WS-29721_48843_CA_O_20220916_EnvironmentalAssessmentReport

ECS Southeast, LLP
Environmental Site Assessment Report Mount Hope Church Road Site
1763 Mt. Hope Church Road
McLeansville, Guilford County, North Carolina

ECS Project No. 49:17856-B
September 16, 2022

September 16, 2022
Mr. Hank Niblock
Craige Jenkins Liipfert & Walker, LLP
110 Oakwood Drive
Suite 300
Winston-Salem, North Carolina 27103

Reference: Environmental Site Assessment Report
Mount Hope Church Road Site
1763 Mt. Hope Church Road
McLeansville, Guilford County, North Carolina
ECS Project No. 49:1856-B Dear Mr. Niblock, ECS Southeast, LLP (ECS) is pleased to provide Craige Jenkins Liipfert & Walker, LLP with the results of our environmental site assessment for the above-referenced site. ECS’s services were provided in accordance with ECS proposal No. 49:32781P dated July 28, 2022 and authorized on August 11, 2022. ECS appreciates the opportunity to provide our services to you. If there are questions regarding this report, or a need for further information, please contact us. Respectfully submitted, ECS SOUTHEAST, LLP

Ron Navarro Scott M. Werley, P.G.
Environmental Staff Project Manager Environmental Principal
[e-mail] [e-mail]
919-861-9910 984-297-7285

Environmental Site Assessment Report Mt. Hope Church Road Site
1763 Mt. Hope Church Road, McLeansville, North Carolina ECS Project No. 49:17856-B September 16, 2022

i

TABLE OF CONTENTS 1.0 PROJECT INFORMATION .................................................................................................................... 1
2.0 SCOPE OF SERVICES ............................................................................................................................ 1
3.0 RESULTS .............................................................................................................................................. 3
4.0 FINDINGS AND CONCLUSIONS ........................................................................................................... 4
5.0 RECOMENDATIONS ............................................................................................................................ 4
6.0 QUALIFICATIONS OF REPORT ............................................................................................................. 5
FIGURES Figure 1 Site Topographic Map Figure 2 Aerial Site Map and Sample Location Map TABLE Table 1 Summary Groundwater Analytical Results Table 2 Summary of VOC/SVOC Soil Analytical Results APPENDICES Appendix A Site Photograph Log Appendix B Well Permit Information Appendix C Boring Logs Appendix D Laboratory Data Sheets and Chain-of-Custody Records

Environmental Site Assessment Report Mt. Hope Church Road Site
1763 Mt. Hope Church Road, McLeansville, North Carolina ECS Project No. 49:17856-B September 16, 2022
Page | 1

1.0 PROJECT INFORMATION

The subject property is located at 1763 Mt. Hope Church Road in McLeansville, North Carolina (Figure 1).
According to the Guilford County Online GIS website, the subject property is identified as Parcel
Identification Number (PIN) 8804327039, consists of 5.84 acres, and is owned by Thomas and Janice
Hancock. Based on the available information, the subject property is developed with an approximate
2,816 square foot building reportedly constructed in 1960. ECS previously conducted a Phase I
Environmental Site Assessment (Phase I ESA) at the site, documented in a report dated July 25, 2022 (ECS
Project No. 49:17856). The results of the Phase I ESA revealed the following recognized environmental
conditions (RECs) in connection with the subject property:

• The discarded 55-gallon drums and other containers in the wooded land around the barn
represent a REC due to the potential release of solvents and other petroleum compounds.
• The suspect UST piping located adjacent to the outbuilding represents a REC.
• The historical use of the eastern adjoining property as an automotive repair facility for
approximately 50 years represents a REC.

Based upon the results of the revised Phase I ESA, ECS was requested to conduct additional Environmental
Assessment Services at the subject property in an effort to evaluate the if the identified RECs have
impacted the subject property. This evaluation included the collection and laboratory analysis of soil and
groundwater quality samples from the subject property. These activities are summarized in this report.

2.0 SCOPE OF SERVICES

The field activities were conducted by ECS on August 29 and August 30, 2022. ECS contracted with Ground
Zero Environmental (GZE) to drill and abandon borings on August 30, 2022. Field activities on August 29,
2022 consisted of the collection of four hand auger soil samples in the vicinity of the discarded drums
identified in the Phase I ESA. Field activities on August 30, 2022 consisted of the collection of one soil
sample via a Direct Push Technology (DPT) drill rig, the installation of three temporary wells along the
eastern boundary of the subject property, the collection of three groundwater samples from the
temporary wells for laboratory analysis, and abandonment of the temporary wells. ECS provided an
environmental professional to observe and document soil boring activities and collect soil and
groundwater samples. Photo documentation of field activities is provided in Appendix A.

2.1 Monitoring Well Permit

ECS procured a monitoring well construction permit from the North Carolina Department of
Environmental Quality (NCDEQ) (No. WM0401836). A copy of the permit is included in Appendix B.

2.2 Utility Locate Services

Prior to commencing with field activities, ECS contacted North Carolina One-Call to locate/mark public
utilities at the site. ECS additionally contracted with KCI Technologies (KCI), to conduct Ground Penetrating
Radar (GPR) and private utility locating services at the site. Required separation distances between
Environmental Site Assessment Report Mt. Hope Church Road Site
1763 Mt. Hope Church Road, McLeansville, North Carolina ECS Project No. 49:17856-B September 16, 2022
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subsurface activities and marked utilities (typically 30-inches) were maintained during the field activities.
KCI also attempted to locate the possible UST near the outbuilding on the subject property, as identified
in the Phase I ESA. Evidence of a current or former UST was not encountered near the building using
GPR/EM technology, however, an unused AST was discovered in the vicinity of the vent piping near the
outbuilding.

2.3 Groundwater Sampling Activities

ECS contracted with GZE to advance three (3) soil borings for the installation of three (3) groundwater
temporary wells (one per boring) to assess the groundwater for impacts associated with the RECs
identified during the Phase I ESA. The temporary wells were constructed per North Carolina
Administrative Code (NCAC) 2C well construction standards utilizing 1-inch diameter 0.010-inch slotted
PVC well screen and riser pipe set with screen to straddle the water table based upon indications of
groundwater observed during the advancement of the borings. TW-1 and TW-3 were drilled to depths of
30 feet below ground surface (ft bgs) and TW-1 was drilled to a depth of approximately 25 ft bgs. The
approximate static water level below ground surface was measured at 22.7 ft bgs in TW-1, 24.25 ft bgs in
TW-2, and 20.25 ft bgs in TW-3. The approximate groundwater sample locations are depicted on Figure 2. Boring logs are available in Appendix C. Groundwater samples were collected from TW-1 through TW-
3 utilizing a peristaltic pump and new dedicated disposable polyethylene tubing. Prior to sampling, the
sampling points were developed/purged using the pump and tubing to remove sand, silt, and other fine
sediments which may have entered the screen during drilling, and to promote communication between
the surrounding formation and the screened interval. Groundwater samples were then collected from
TW-1 through TW-3 by pumping groundwater directly into laboratory supplied/preserved sample
containers. The groundwater sample containers were labeled and placed into a cooler with ice to maintain
the samples at approximately 4° Celsius (°C). The samples were submitted to Pace Analytical Services, LLC
(Pace) located in Huntersville, North Carolina (North Carolina Certification # 12) to be analyzed for Volatile
Organic Compounds (VOCs) by EPA Method 8260 and Semi-volatile Organic Compounds (SVOCs) by EPA
method 8270. ECS maintained proper chain-of-custody (COC) procedures throughout the sample collection
and transportation process. Copies of the laboratory report and COC are included in Appendix D. Following
the completion of the groundwater sampling activities, the temporary monitor wells were abandoned by
GZE.

2.4 Soil Sampling Activities

ECS observed and documented the advancement of one (1) soil boring by GZE at the subject property to
collect a soil sample in the vicinity of the AST near the outbuilding on the subject property. The boring, labeled
SB-1, was drilled to a depth of approximately 20 ft bgs using the DPT rig by driving a macro-core soil sampler
equipped with a new disposable liner. Soils were collected continuously from the ground surface to the
termination of the soil borings within the sampler. Upon retrieval of the sampler, the liner was removed and
cut open to expose the soils, where they were screened in the field for volatile organic vapors using a flame
ionization detector (FID). The soil core was screened at five (5) foot intervals. The soil interval exhibiting the
highest FID reading or other evidence of apparent impacts (staining, odors, etc.) from the boring was collected
and submitted for laboratory analysis. Due to the FID readings and petroleum odors recorded in the field for
the soil interval between 5-10 ft bgs, the sample was obtained from the 5-10 ft soil interval. The sample was
submitted to Pace to be analyzed for VOCs by EPA Method 8260D, SVOCs by method 8270, volatile
Environmental Site Assessment Report Mt. Hope Church Road Site
1763 Mt. Hope Church Road, McLeansville, North Carolina ECS Project No. 49:17856-B September 16, 2022
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petroleum hydrocarbons (VPH) by the Massachusetts Department of Environmental Protection (MADEP)
VPH method, and extractable petroleum hydrocarbons (EPH) by the MADEPH EPH method. ECS
maintained proper COC procedures throughout the sample collection and transportation process. Copies of
the laboratory report and COC are included in Appendix D. The soil borings were backfilled with the soil
cuttings generated during the boring activities and capped appropriately.

In addition to the soil sample collected near the possible UST in the vicinity of the outbuilding on the subject
property, ECS also collected four (4) soil samples in the vicinity of the discarded drums identified in the Phase
I ESA. The soil samples were collected from borings advanced via hand auger, to depths of approximately 5 ft
bgs at each location. The hand auger was decontaminated between each boring location to reduce the
potential for cross-contamination between sample locations. The soil samples were appropriately packaged
and submitted to Pace to be analyzed for VOCs by EPA Method 8260 and SVOCS by EPA Method 8270. The
approximate soil sample locations are illustrated on Figure 2.

3.0 RESULTS
3.1 Groundwater Results

According to the laboratory analytical report submitted by Pace, no VOC or SVOC constituents were detected
above laboratory reporting limits in the three groundwater samples collected and submitted for analysis. A
summary of the groundwater analytical results is provided in Table 1. Laboratory reports and COC
documentation are provided in Appendix D.

3.2 Soil Results

The analytical results for the soil samples collected via hand auger near the discarded drums on the subject
property (HA-1 through HA-4) have been compared to NCDEQ Preliminary Site Remediation Goals (PSRGs),
which are applicable to potential contaminant sources of this type. The analytical results for SB-1, which was
collected to assess a potential UST release, has been compared to NCDEQ Maximum Soil Contaminant
Concentrations (MSCCs), which are applicable to UST assessments.

According to the laboratory analytical report submitted by Pace, C9-C18 aliphatic petroleum
hydrocarbons, and C9-C22 aromatic petroleum hydrocarbons were detected at concentrations above
NCDEQ Division of Waste Management (DWM) Soil to Groundwater MSCCs in the soil sample identified
as SB-1, which was obtained from the vicinity of the possible UST near the outbuilding on the subject
property. P-isopropytoluene, naphthalene, 1,3,5-trimethylbenzene, 1-methylnaphthalene, and 2-
methylnaphthalene were also identified at concentrations above their respective NCDEQ Soil to
Groundwater MSCCs. No other VOC, SVOC, EPH, or VPH constituents except for those described above
were detected above laboratory reporting limits (RLs) in the soil sample identified as SB-1 collected from
5-10 ft bgs.

O-xylene was detected above laboratory RLs, but below its respective Protection of Groundwater PSRG in
the four hand auger soil samples (identified as HA-1 through HA-4) collected in the vicinity of the drums
Environmental Site Assessment Report Mt. Hope Church Road Site
1763 Mt. Hope Church Road, McLeansville, North Carolina ECS Project No. 49:17856-B September 16, 2022
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on the subject property. No other VOC or SVOC constituents were detected above laboratory RLs in the
four hand auger soil samples collected.

A summary of the soil analytical results for VOCs and SVOCs is available in Table 2. A summary of the soil
analytical results for EPH and VPH is available in Table 3. Laboratory reports and COC documentation are
provided in Appendix D.

4.0 FINDINGS AND CONCLUSIONS

Based on the results of the environmental assessment, ECS concludes the following:
• C9-C18 aliphatics and C9-C22 aromatics were detected above their respective Soil-to-
Groundwater MSCCs in the soil sample SB-1 collected from 5-10 ft bgs.
• P-isopropytoluene, naphthalene, 1,3,5-trimethylbenzene, 1-methylnaphthalene, and 2-
methylnaphthalene were detected above their respective Soil to Groundwater MSCCs in soil
sample SB-1 when analyzed for VOCs and SVOCs by EPA Method 8260 and 8270, respectively.
• The occurrence of EPH, VPH, VOC, and SVOC constituents above regulatory standards in the soil
sample SB-1 at 5-10 ft bgs is likely attributed to a petroleum release from the suspect UST
reported to potentially be present near the outbuilding on the subject property. Soil quality
comparison criteria for UST related assessments are the NCDEQ MSCCs.
• No VOC or SVOC constituents were detected above their applicable regulatory standards in the
hand auger soil samples identified as HA-1 through HA-4.
• No VOC or SVOC constituents were detected above their applicable regulatory standards in the
three groundwater samples collected on the subject property and identified as TW-1 through TW-
3.

5.0 RECOMMENDATIONS

Based on the results of the environmental assessment, ECS recommends the following:
• Based on the detection of EPH, VPH, VOC, and SVOCs at concentrations greater than its regulatory
guidance levels in site soil assessed by sample SB-1, ECS recommends that further assessment be
performed in the vicinity of the potential former UST to delineate the extent of impacted soil. ECS
also recommends that a groundwater sample be taken from the vicinity of the area in which SB-
1 was collected in an effort to confirm or deny if the release has impacted site groundwater.
• A copy of this report be kept in your records for future reference.

Environmental Site Assessment Report Mt. Hope Church Road Site
1763 Mt. Hope Church Road, McLeansville, North Carolina ECS Project No. 49:17856-B September 16, 2022
Page | 5

6.0 QUALIFICATIONS OF REPORT

The activities and evaluative approaches used in this assessment are consistent with those normally
employed in environmental assessment projects of this type. Our evaluation of site conditions has been
based on our understanding of the site project information and the data obtained during our field
activities. This report was prepared for the express use of Craige Jenkins Liipfert & Walker, LLP . Use of this report by other individuals or companies implies their acceptance of the General Conditions of Service of the original contract.

Environmental Site Assessment Report Mt. Hope Church Road Site
1763 Mt. Hope Church Road, McLeansville, North Carolina ECS Project No. 49:17856-B September 16, 2022
Page | 6

FIGURES

SOURCE:
ECS PHASE I (July 2022)
SCALE SHOWN ABOVE
FIGURE 1
SITE TOPOGRAPHIC MAP
1763 Mt. Hope Church Road
McLeansville, NC
ECS Project Number: 49:17856-B
SOURCE:
ECS PHASE I (July 2022)
2020 IMAGERY
SCALE SHOWN ABOVE
FIGURE 2
SITE AERIAL AND SAMPLE LOCATION MAP
1763 Mt. Hope Church Road
McLeansville, NC
ECS Project Number: 49:17856-B
Approximate Temporary
Monitoring Well Location
Legend
Approximate Hand Auger Soil
Boring Location
2
2
1 Suspect UST pipes -REC
2 Discarded Drums -REC
HA-1
HA-2
HA-3
HA-4
SB-1
TW-1
TW-2
TW-3
Approximate DPT Rig Soil Boring Location
Environmental Site Assessment Report Mt. Hope Church Road Site
1763 Mt. Hope Church Road, McLeansville, North Carolina ECS Project No. 49:17856-B September 16, 2022
Page | 7

TABLES

PARAMETER SCREENING LEVEL
Sample ID TW-1 TW-2 TW-3
Collection Date
All SVOCs ND ND ND Various
All VOCs ND ND ND Various
Notes:Results are presented in micrograms per Liter (ug/L), analogous to parts per billion (ppb).NC2LGWQS = North Carolina 2L Groundwater Quality Standard as of April 1, 2022
NS = No StandardND = Not detected at or above adjusted reporting limit.
TABLE 1: SUMMARY OF GROUNDWATER ANALYTICAL RESULTS
MOUNT HOPE CHURCH ROAD SITE
1763 MOUNT HOPE CHURCH ROAD
McLEANSVILLE, GUILFORD COUNTY, NORTH CAROLINA
ECS PROJECT NO. 49-17856-B
Volatile Organic Compounds (VOCs) By EPA Method 8260
8/31/2022
ANALYTICAL RESULTS
NC2LGWQS
Semi-Volatile Organic Compounds (SVOCs) By EPA Method 8270
Sample ID HA-1 HA-2 HA-3 HA-4 SB-1
Sample Depth (ft)0-5 0-5 0-5 0-5 5-10
Collection Date
p-Isopropyltoluene <0.39 <0.39 <0.39 <0.39 2.8 NS NS NS 0.12 1560 23330
Naphthalene <0.39 <0.39 <0.39 <0.39 3.6 0.39 2.1 8.8 0.2 5.5 27
1,2,4-Trimethylbenzene <0.39 <0.39 <0.39 <0.39 7.4 12 63 370 6.6 156 23301,3,5-Trimethylbenzene <0.39 <0.39 <0.39 <0.39 4.6 11 56 320 6.6 156 2330
o-Xylene 0.0094 0.0079 0.0074 0.0055 0.5 9.8 140 590 6 3120 46700
1-Methylnapthalene <0.41 <0.41 <0.41 <0.41 3.2 0.11 18 73 0.054 22.8 112
2-Methylnapthalene <0.83 <0.83 <0.83 <0.83 3.7 3.1 48 600 1.5 62.5 934Naphthalene<0.41 <0.41 <0.41 <0.41 1.3 0.39 2.1 8.8 0.2 5.5 27
Aliphatic (C5-C8) NA NA NA NA 27.8 NS NS NS 68 625 93,400
Aliphatic (C9-C18)
(C9-C12 + C9-C18)NA NA NA NA 1,198 NS NS NS 540 1,560 23,300
Aliphatic (C19-C36)NA NA NA NA <125 NS NS NS NS 31,200 467,000Aromatic (C9-C22)
(C9-C10 + C11-C22)NA NA NA NA 441 NS NS NS 31 469 7,000
Notes:
Results are presented in milligrams per Kilogram (mg/Kg), analogous to parts per million (ppm).
Only those constituents detected in at least one sample are listed above. For complete results, refer to laboratory report.Soil sample results for HA-1 trhough HA-4 are compared to the NCDEQ PSRGs dated July 2022Soil sample results for SB-1 are compared to the NCDEQ MSCCs dated September 2022
NCDEQ = North Carolina Department of Environmental Quality
PSRG = Preliminary Site Remediation GoalMSCC = Maximum Soil Contaminant ConcentrationEPH = Extractable Petroleum Hydrocarbons
VPH = Volatile Petroleum Hydrocarbons
MADEP = Massachussets Departmetn of Environmental ProtectionNA = Not AnalyzedBold denotes concentration is equal to or in exceedance of the soil-to-water MSCC
VOC = Volatile Organic Compounds
SVOC = Semi-Volatile Organic Compounds
Parameter
8/29/2022
COMPARISON CRITERIA
Soil to Groundwater MSCCs
Residential MSCCs
Industrial/ Commercial MSCCs
TABLE 2: SUMMARY OF SOIL ANALYTICAL RESULTSMOUNT HOPE CHURCH ROAD SITE
1763 MOUNT HOPE CHURCH ROADMcLEANSVILLE, GUILFORD COUNTY, NORTH CAROLINA
ECS PROJECT NO. 49-17856-B
Protection of Groundwater PSRG Residential Health Based PSRG
Industrial/ Commercial Health Based PSRG
Volatile Organic Compounds (VOCs) by EPA Method 8260
Semi-Volatile Organic Compounds (SVOCs) by EPA Method 8270
MADEP EPH & VPH NC SOIL
ANALYTICAL RESULTS NCDEQ PSRGs NCDEQ MSCCs
Environmental Site Assessment Report Mt. Hope Church Road Site
1763 Mt. Hope Church Road, McLeansville, North Carolina ECS Project No. 49:17856-B September 16, 2022
Page | 8

APPENDIX A SITE PHOTOGRAPH LOG

PHOTOGRAPH LOG
Mt. Hope Church Road Site
1763 Mt. Hope Church Road
McLeansville, Guilford County, NC
ECS Project Number: 49-17856-N
Photograph 1: UST piping near outbuilding
Photograph 2: AST Near outbuilding
PHOTOGRAPH LOG
Mt. Hope Church Road Site
1763 Mt. Hope Church Road
McLeansville, Guilford County, NC
ECS Project Number: 49-17856-N
Photograph 3: Collecting hand auger soil sample from soil beneath drums
Photograph 2: Drilling SS-1 with hand auger
Photograph 4: Drilling temporary well for groundwater sampling
PHOTOGRAPH LOG
Mt. Hope Church Road Site
1763 Mt. Hope Church Road
McLeansville, Guilford County, NC
ECS Project Number: 49-17856-N
Photograph 5: Temporary well after installation
Photograph 6: Drilling SB-1 near AST by outbuilding
PHOTOGRAPH LOG
Mt. Hope Church Road Site
1763 Mt. Hope Church Road
McLeansville, Guilford County, NC
ECS Project Number: 49-17856-N
Photograph 7: Collecting groundwater sample from temporary well
Environmental Site Assessment Report Mt. Hope Church Road Site
1763 Mt. Hope Church Road, McLeansville, North Carolina ECS Project No. 49:17856-B September 16, 2022
Page | 9

APPENDIX B WELL PERMIT INFORMATION

North Carolina Department of Environmental Quality | Division of Water Resources
Winston-Salem Regional Office | 450 W. Hanes Mill Rd, Suite 300 | Winston-Salem, North Carolina 27105
336.776.9800

August 22, 2022
Mr. Hank Niblock
Craige Jenkins Liipfert & Walker, LLP
110 Oakwood Drive, Suite 300
Winston-Salem, North Carolina 27103

SUBJECT: MONITORING WELL CONSTRUCTION
PERMIT NO. WM0401386
COUNTY: Guilford
FILE NAME: 1763 Mt. Hope Church Road

Dear Mr. Niblock:

In accordance with your application received on August 17, 2022, we are forwarding herewith:

1. Monitoring Well Construction Permit No. WM0401386 for the construction of four (4)
temporary monitoring wells at 1763 Mt. Hope Church Road in McLeansville in Guilford
County.

Henceforth, correspondence and data relating to this well shall be designated as specified in the
subject heading above. This Permit will be effective from the date of issuance and shall be subject
to the conditions and limitations as specified therein. If you have any questions regarding this
permit, please contact me or Jim Gonsiewski at [phone].

Sincerely,

Lon T. Snider
Regional Supervisor
Water Quality Regional Operations Section
Division of Water Resources, NCDEQ – WSRO

cc: Thomas and Janice Hancock
Ron Navarro – ECS Southeast, LLP (Electronic Copy)
WSRO Electronic Files
Laserfiche Files

North Carolina Department of Environmental Quality | Division of Water Resources
Winston-Salem Regional Office | 450 W. Hanes Mill Rd, Suite 300 | Raleigh, North Carolina 27105
336.776.9800

NORTH CAROLINA
DEPARTMENT OF ENVIRONMENTAL QUALITY
DIVISION OF WATER RESOURCES – WATER QUALITY REGIONAL OPERATIONS
SECTION

PERMIT FOR THE CONSTRUCTION OF A MONITORING WELL

In accordance with the provisions of Article 7, Chapter 87, North Carolina General Statutes, and
other applicable Laws, Rules and Regulations.

PERMISSION IS HEREBY GRANTED TO

Craige Jenkins Liipfert & Walker, LLP

FOR THE CONSTRUCTION OF A MONITOR WELL SYSTEM consisting of four (4)
temporary monitoring wells owned by Craige Jenkins Liipfert & Walker, LLP. The wells will be
located at 1763 Mt. Hope Church Road in McLeansville, North Carolina, in Guilford County. This
Permit is issued in accordance with the application received on August 17, 2022 in conformity
with specifications and supporting data, all of which are filed with the Department of
Environmental Quality and are considered integral parts of this Permit.

This Permit is for well construction only, and does not waive any provision or requirement of any
other applicable law or regulation. Construction of any well under this Permit shall be in strict
compliance with the North Carolina Well Construction Regulations and Standards (15A NCAC
02C .0100), and other State and Local Laws and regulations pertaining to well construction.

If any requirements or limitations specified in this Permit are unacceptable, you have a right to an
adjudicatory hearing upon written request within 30 days of receipt of this Permit. The request
must be in the form of a written petition conforming to Chapter 150B of the North Carolina General
Statutes and filed with the Office of Administrative Hearings, 6714 Mail Service Center, Raleigh,
North Carolina 27699-6714. Unless such a demand is made, this Permit is final and binding.

This Permit will be effective for one year from the date of its issuance and shall be subject to other
specified conditions, limitations, or exceptions as follows:

North Carolina Department of Environmental Quality | Division of Water Resources
Winston-Salem Regional Office | 450 W. Hanes Mill Rd, Suite 300 | Raleigh, North Carolina 27105
336.776.9800

1. Issuance of this Permit does not obligate reimbursement from State trust funds, if these
wells are being installed as part of an investigation for contamination from an underground
storage tank or dry cleaner incident.
2. Issuance of this Permit does not supersede any other agreement, permit, or requirement
issued by another agency.
3. The well(s) shall be located and constructed as shown on the attachments submitted as part
of the Permit application.
4. Each well shall have a Well Contractor Identification Plate in accordance with 15A NCAC
02C .0108(o).
5. Well construction records (GW-1) for each well shall be submitted to the Division of Water
Resources’ Information Processing Unit within 30 days of the well completion.
6. When the well is discontinued or abandoned, it shall be abandoned in accordance with 15A
NCAC 02C .0113 and a well abandonment record (GW-30) shall be submitted to the
Division of Water Resources’ Information Processing Unit within 30 days of the well
abandonment.
7. The County Health Department may require a county monitoring well construction permit.
Please contact the health department for their requirements.

Permit issued the 22nd day of August, 2022

FOR THE NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION

_______________________________________________
Lon T. Snider, Regional Supervisor
Water Quality Regional Operations Section
Division of Water Resources, NCDEQ - WSRO

By Authority of the Environmental Management Commission

Permit No. # WM0401386
Environmental Site Assessment Report Mt. Hope Church Road Site
1763 Mt. Hope Church Road, McLeansville, North Carolina ECS Project No. 49:17856-B September 16, 2022
Page | 10

APPENDIX C BORING LOGS
Depth/
5
10
15
20
25
30
ElevaƟon
-5
-10
-15
-20
-25
-30 PID Reading258.0
321.0
285.0
43.5 Sample NumberSB-1 Sample Recovery (in)Graphic LogSoil ClassiĮcaƟon
SC
SC
ML
ML
DescripƟon
Red/Brown Clayey Silt
Red/Brown Clayey Silt
Brown/Tan Silt PHC
Red/Brown Silt PHC, Moist
END OF DRILLING AT 20.0 FT
Project Name:Mount Hope Church Road Site
Client:
Site LocaƟon:1763 Mt. Hope Church Rd. McLeansville, NC
27301
LaƟtude/Longitude:
Sheet:1 of 1 Boring No:SB-1
Project No.:49:17856-B
Driller:Ground Zero Drill Rig:GeoProbe
WL (First Encountered)Boring Started:Aug 31 2022
WL (CompleƟon)Boring Completed:Aug 31 2022
Remarks:Logged By:
Principal Engineer/
Responsible PG:
Randy Cavillier
Joe Nestor
Depth/
5
10
15
20
25
30
ElevaƟon
-5
-10
-15
-20
-25
-30 PID ReadingSample NumberTW-1 Sample Recovery (in)Graphic LogSoil ClassiĮcaƟon
SC
SC
ML
ML
ML
ML
DescripƟon
Red Brown Clayey Silt
Tan/Red Clayey Silt
Brown Silt
Brown Silt, Moist
Brown Silt, Wet at 23' BLS
Brown Silt, Wet
END OF DRILLING AT 30.0 FT
WELL CONSTRUCTION
1" Diameter Sch. 40
PVC Riser
1" Diameter Sch. 40
PVC Screen
Project Name:Mount Hope Church Road Site
Client:
Site LocaƟon:1763 Mt. Hope Church Rd. McLeansville, NC
27301
LaƟtude/Longitude:
Sheet:1 of 1 Boring No:TW-1
Project No.:49:17856-B
Driller:Ground Zero Drill Rig:GeoProbe
ElevaƟon:
WL (First Encountered)Boring Started:Aug 31 2022
WL (CompleƟon)Boring Completed:Aug 31 2022
Remarks:Logged By:
Principal Engineer/
Responsible PG:
Randy Cavillier
Joe Nestor
Depth/
5
10
15
20
25
30
ElevaƟon
-5
-10
-15
-20
-25
-30 PID ReadingSample NumberTW-2 Sample Recovery (in)Graphic LogSoil ClassiĮcaƟon
SC
SC
ML
ML
ML
DescripƟon
Red/Brown Clayey Silt
Red/Brown Clayey Silt
Red/Brown Silt
Red/Brown Silt, Wet
Red/Brown Silt, Wet
END OF DRILLING AT 25.0 FT
WELL CONSTRUCTION
1" Diameter Sch. 40
PVC Riser
1" Diameter Sch. 40
Screen
Project Name:Mount Hope Church Road Site
Client:
Site LocaƟon:1763 Mt. Hope Church Rd. McLeansville, NC
27301
LaƟtude/Longitude:
Sheet:1 of 1 Boring No:TW-2
Project No.:49:17856-B
Driller:Ground Zero Drill Rig:GeoProbe
ElevaƟon:
WL (First Encountered)Boring Started:Aug 31 2022
WL (CompleƟon)Boring Completed:Aug 31 2022
Remarks:Logged By:
Principal Engineer/
Responsible PG:
Randy Cavillier
Joe Nestor
Depth/
5
10
15
20
25
30
ElevaƟon
-5
-10
-15
-20
-25
-30 PID ReadingSample NumberTW-3 Sample Recovery (in)Graphic LogSoil ClassiĮcaƟon
SC
SC
ML
ML
ML
ML
DescripƟon
Red/Brown Clayey Silt
Red/Brown Clayey Silt
Red/Tan Silt
Red/Tan Silt, Moist
Red/Tan Silt, Moist
Red/Tan Silt, Moist
END OF DRILLING AT 30.0 FT
WELL CONSTRUCTION
1" Diameter Sch. 40
PVC Riser
1" Diameter Sch. 40
PVC Screen
Project Name:Mount Hope Church Road Site
Client:
Site LocaƟon:1763 Mt. Hope Church Rd. McLeansville, NC
27301
LaƟtude/Longitude:
Sheet:1 of 1 Boring No:TW-3
Project No.:49:17856-B
Driller:Ground Zero Drill Rig:GeoProbe
ElevaƟon:
WL (First Encountered)Boring Started:Aug 31 2022
WL (CompleƟon)Boring Completed:Aug 31 2022
Remarks:Logged By:
Principal Engineer/
Responsible PG:
Randy Cavillier
Joe Nestor
Environmental Site Assessment Report Mt. Hope Church Road Site
1763 Mt. Hope Church Road, McLeansville, North Carolina ECS Project No. 49:17856-B September 16, 2022
Page | 11

APPENDIX D LABORATORY DATA SHEETS AND CHAIN-OF-CUSTODY RECORD
#=CL#
September 12, 2022
LIMS USE: FR - RANDY CAVALLIER
LIMS OBJECT ID: 92623480
92623480
Project:
Pace Project No.:
RE:
Mr. Randy Cavallier
ECS Southeast, LLP
4811 Koger Blvd.
Greensboro, NC 27407
MT. HOPE CHURCH ROAD, MCLEANSV
Dear Mr. Cavallier:
Enclosed are the analytical results for sample(s) received by the laboratory on September 01, 2022. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
[phone]
Enclosures
cc:ECS Southeast Reporting, ECS Southeast
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 71
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 71
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92623480001 HA-1 EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
92623480002 HA-2 EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
92623480003 HA-3 EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
92623480004 HA-4 EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
92623480005 SB-1 MADEP EPH 7 PASI-CBAJ
MADEP VPH 5 PASI-CTEG
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
92623480006 TW-1 EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CSAS
92623480007 TW-2 EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CSAS
92623480008 TW-3 EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CSAS
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Sample:HA-1 Lab ID:92623480001 Collected:08/29/22 13:20 Received:09/01/22 10:05 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 09/06/22 17:26 83-32-909/03/22 23:210.40 1
Acenaphthylene ND mg/kg 09/06/22 17:26 208-96-809/03/22 23:210.40 1
Aniline ND mg/kg 09/06/22 17:26 62-53-309/03/22 23:210.40 1
Anthracene ND mg/kg 09/06/22 17:26 120-12-709/03/22 23:210.40 1
Benzo(a)anthracene ND mg/kg 09/06/22 17:26 56-55-309/03/22 23:210.40 1
Benzo(a)pyrene ND mg/kg 09/06/22 17:26 50-32-809/03/22 23:210.40 1
Benzo(b)fluoranthene ND mg/kg 09/06/22 17:26 205-99-209/03/22 23:210.40 1
Benzo(g,h,i)perylene ND mg/kg 09/06/22 17:26 191-24-209/03/22 23:210.40 1
Benzo(k)fluoranthene ND mg/kg 09/06/22 17:26 207-08-909/03/22 23:210.40 1
Benzoic Acid ND mg/kg 09/06/22 17:26 65-85-009/03/22 23:212.0 1
Benzyl alcohol ND mg/kg 09/06/22 17:26 100-51-609/03/22 23:210.80 1
4-Bromophenylphenyl ether ND mg/kg 09/06/22 17:26 101-55-309/03/22 23:210.40 1
Butylbenzylphthalate ND mg/kg 09/06/22 17:26 85-68-709/03/22 23:210.40 1
4-Chloro-3-methylphenol ND mg/kg 09/06/22 17:26 59-50-709/03/22 23:210.80 1
4-Chloroaniline ND mg/kg 09/06/22 17:26 106-47-809/03/22 23:210.80 1
bis(2-Chloroethoxy)methane ND mg/kg 09/06/22 17:26 111-91-109/03/22 23:210.40 1
bis(2-Chloroethyl) ether ND mg/kg 09/06/22 17:26 111-44-409/03/22 23:210.40 1
2-Chloronaphthalene ND mg/kg 09/06/22 17:26 91-58-709/03/22 23:210.40 1
2-Chlorophenol ND mg/kg 09/06/22 17:26 95-57-809/03/22 23:210.40 1
4-Chlorophenylphenyl ether ND mg/kg 09/06/22 17:26 7005-72-309/03/22 23:210.40 1
Chrysene ND mg/kg 09/06/22 17:26 218-01-909/03/22 23:210.40 1
Dibenz(a,h)anthracene ND mg/kg 09/06/22 17:26 53-70-309/03/22 23:210.40 1
Dibenzofuran ND mg/kg 09/06/22 17:26 132-64-909/03/22 23:210.40 1
1,2-Dichlorobenzene ND mg/kg 09/06/22 17:26 95-50-109/03/22 23:210.40 1
1,3-Dichlorobenzene ND mg/kg 09/06/22 17:26 541-73-109/03/22 23:210.40 1
1,4-Dichlorobenzene ND mg/kg 09/06/22 17:26 106-46-709/03/22 23:210.40 1
3,3'-Dichlorobenzidine ND mg/kg 09/06/22 17:26 91-94-109/03/22 23:210.80 1
2,4-Dichlorophenol ND mg/kg 09/06/22 17:26 120-83-209/03/22 23:210.40 1
Diethylphthalate ND mg/kg 09/06/22 17:26 84-66-209/03/22 23:210.40 1
2,4-Dimethylphenol ND mg/kg 09/06/22 17:26 105-67-909/03/22 23:210.40 1
Dimethylphthalate ND mg/kg 09/06/22 17:26 131-11-309/03/22 23:210.40 1
Di-n-butylphthalate ND mg/kg 09/06/22 17:26 84-74-209/03/22 23:210.40 1
4,6-Dinitro-2-methylphenol ND mg/kg 09/06/22 17:26 534-52-109/03/22 23:210.80 1
2,4-Dinitrophenol ND mg/kg 09/06/22 17:26 51-28-509/03/22 23:212.0 1
2,4-Dinitrotoluene ND mg/kg 09/06/22 17:26 121-14-209/03/22 23:210.40 1
2,6-Dinitrotoluene ND mg/kg 09/06/22 17:26 606-20-209/03/22 23:210.40 1
Di-n-octylphthalate ND mg/kg 09/06/22 17:26 117-84-009/03/22 23:210.40 1
bis(2-Ethylhexyl)phthalate ND mg/kg 09/06/22 17:26 117-81-7 v209/03/22 23:210.40 1
Fluoranthene ND mg/kg 09/06/22 17:26 206-44-009/03/22 23:210.40 1
Fluorene ND mg/kg 09/06/22 17:26 86-73-709/03/22 23:210.40 1
Hexachloro-1,3-butadiene ND mg/kg 09/06/22 17:26 87-68-309/03/22 23:210.40 1
Hexachlorobenzene ND mg/kg 09/06/22 17:26 118-74-109/03/22 23:210.40 1
Hexachlorocyclopentadiene ND mg/kg 09/06/22 17:26 77-47-409/03/22 23:210.40 1
Hexachloroethane ND mg/kg 09/06/22 17:26 67-72-109/03/22 23:210.40 1
Indeno(1,2,3-cd)pyrene ND mg/kg 09/06/22 17:26 193-39-509/03/22 23:210.40 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Sample:HA-1 Lab ID:92623480001 Collected:08/29/22 13:20 Received:09/01/22 10:05 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Isophorone ND mg/kg 09/06/22 17:26 78-59-109/03/22 23:210.40 1
1-Methylnaphthalene ND mg/kg 09/06/22 17:26 90-12-009/03/22 23:210.40 1
2-Methylnaphthalene ND mg/kg 09/06/22 17:26 91-57-609/03/22 23:210.40 1
2-Methylphenol(o-Cresol)ND mg/kg 09/06/22 17:26 95-48-709/03/22 23:210.40 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 09/06/22 17:26 15831-10-409/03/22 23:210.40 1
Naphthalene ND mg/kg 09/06/22 17:26 91-20-309/03/22 23:210.40 1
2-Nitroaniline ND mg/kg 09/06/22 17:26 88-74-409/03/22 23:212.0 1
3-Nitroaniline ND mg/kg 09/06/22 17:26 99-09-209/03/22 23:212.0 1
4-Nitroaniline ND mg/kg 09/06/22 17:26 100-01-609/03/22 23:210.80 1
Nitrobenzene ND mg/kg 09/06/22 17:26 98-95-309/03/22 23:210.40 1
2-Nitrophenol ND mg/kg 09/06/22 17:26 88-75-509/03/22 23:210.40 1
4-Nitrophenol ND mg/kg 09/06/22 17:26 100-02-709/03/22 23:212.0 1
N-Nitrosodimethylamine ND mg/kg 09/06/22 17:26 62-75-909/03/22 23:210.40 1
N-Nitroso-di-n-propylamine ND mg/kg 09/06/22 17:26 621-64-709/03/22 23:210.40 1
N-Nitrosodiphenylamine ND mg/kg 09/06/22 17:26 86-30-609/03/22 23:210.40 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 09/06/22 17:26 108-60-109/03/22 23:210.40 1
Pentachlorophenol ND mg/kg 09/06/22 17:26 87-86-509/03/22 23:210.80 1
Phenanthrene ND mg/kg 09/06/22 17:26 85-01-809/03/22 23:210.40 1
Phenol ND mg/kg 09/06/22 17:26 108-95-209/03/22 23:210.40 1
Pyrene ND mg/kg 09/06/22 17:26 129-00-009/03/22 23:210.40 1
Pyridine ND mg/kg 09/06/22 17:26 110-86-109/03/22 23:210.40 1
1,2,4-Trichlorobenzene ND mg/kg 09/06/22 17:26 120-82-109/03/22 23:210.40 1
2,4,5-Trichlorophenol ND mg/kg 09/06/22 17:26 95-95-409/03/22 23:210.40 1
2,4,6-Trichlorophenol ND mg/kg 09/06/22 17:26 88-06-209/03/22 23:210.40 1
Surrogates
Nitrobenzene-d5 (S)40 %09/06/22 17:26 4165-60-009/03/22 23:2121-130 1
2-Fluorobiphenyl (S)34 %09/06/22 17:26 321-60-809/03/22 23:2119-130 1
Terphenyl-d14 (S)75 %09/06/22 17:26 1718-51-009/03/22 23:2115-130 1
Phenol-d6 (S)39 %09/06/22 17:26 13127-88-309/03/22 23:2118-130 1
2-Fluorophenol (S)42 %09/06/22 17:26 367-12-409/03/22 23:2118-130 1
2,4,6-Tribromophenol (S)63 %09/06/22 17:26 118-79-609/03/22 23:2118-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 09/02/22 20:02 67-64-1 v209/02/22 15:410.16 1
Benzene ND mg/kg 09/02/22 20:02 71-43-209/02/22 15:410.0081 1
Bromobenzene ND mg/kg 09/02/22 20:02 108-86-109/02/22 15:410.0081 1
Bromochloromethane ND mg/kg 09/02/22 20:02 74-97-509/02/22 15:410.0081 1
Bromodichloromethane ND mg/kg 09/02/22 20:02 75-27-409/02/22 15:410.0081 1
Bromoform ND mg/kg 09/02/22 20:02 75-25-209/02/22 15:410.0081 1
Bromomethane ND mg/kg 09/02/22 20:02 74-83-909/02/22 15:410.016 1
2-Butanone (MEK)ND mg/kg 09/02/22 20:02 78-93-3 v209/02/22 15:410.16 1
n-Butylbenzene ND mg/kg 09/02/22 20:02 104-51-809/02/22 15:410.0081 1
sec-Butylbenzene ND mg/kg 09/02/22 20:02 135-98-809/02/22 15:410.0081 1
tert-Butylbenzene ND mg/kg 09/02/22 20:02 98-06-609/02/22 15:410.0081 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Sample:HA-1 Lab ID:92623480001 Collected:08/29/22 13:20 Received:09/01/22 10:05 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Carbon tetrachloride ND mg/kg 09/02/22 20:02 56-23-509/02/22 15:410.0081 1
Chlorobenzene ND mg/kg 09/02/22 20:02 108-90-709/02/22 15:410.0081 1
Chloroethane ND mg/kg 09/02/22 20:02 75-00-309/02/22 15:410.016 1
Chloroform ND mg/kg 09/02/22 20:02 67-66-309/02/22 15:410.0081 1
Chloromethane ND mg/kg 09/02/22 20:02 74-87-309/02/22 15:410.016 1
2-Chlorotoluene ND mg/kg 09/02/22 20:02 95-49-809/02/22 15:410.0081 1
4-Chlorotoluene ND mg/kg 09/02/22 20:02 106-43-409/02/22 15:410.0081 1
1,2-Dibromo-3-chloropropane ND mg/kg 09/02/22 20:02 96-12-809/02/22 15:410.0081 1
Dibromochloromethane ND mg/kg 09/02/22 20:02 124-48-109/02/22 15:410.0081 1
1,2-Dibromoethane (EDB)ND mg/kg 09/02/22 20:02 106-93-409/02/22 15:410.0081 1
Dibromomethane ND mg/kg 09/02/22 20:02 74-95-309/02/22 15:410.0081 1
1,2-Dichlorobenzene ND mg/kg 09/02/22 20:02 95-50-109/02/22 15:410.0081 1
1,3-Dichlorobenzene ND mg/kg 09/02/22 20:02 541-73-109/02/22 15:410.0081 1
1,4-Dichlorobenzene ND mg/kg 09/02/22 20:02 106-46-709/02/22 15:410.0081 1
Dichlorodifluoromethane ND mg/kg 09/02/22 20:02 75-71-809/02/22 15:410.016 1
1,1-Dichloroethane ND mg/kg 09/02/22 20:02 75-34-309/02/22 15:410.0081 1
1,2-Dichloroethane ND mg/kg 09/02/22 20:02 107-06-209/02/22 15:410.0081 1
1,1-Dichloroethene ND mg/kg 09/02/22 20:02 75-35-409/02/22 15:410.0081 1
cis-1,2-Dichloroethene ND mg/kg 09/02/22 20:02 156-59-209/02/22 15:410.0081 1
trans-1,2-Dichloroethene ND mg/kg 09/02/22 20:02 156-60-509/02/22 15:410.0081 1
1,2-Dichloropropane ND mg/kg 09/02/22 20:02 78-87-509/02/22 15:410.0081 1
1,3-Dichloropropane ND mg/kg 09/02/22 20:02 142-28-909/02/22 15:410.0081 1
2,2-Dichloropropane ND mg/kg 09/02/22 20:02 594-20-7 v209/02/22 15:410.0081 1
1,1-Dichloropropene ND mg/kg 09/02/22 20:02 563-58-609/02/22 15:410.0081 1
cis-1,3-Dichloropropene ND mg/kg 09/02/22 20:02 10061-01-509/02/22 15:410.0081 1
trans-1,3-Dichloropropene ND mg/kg 09/02/22 20:02 10061-02-609/02/22 15:410.0081 1
Diisopropyl ether ND mg/kg 09/02/22 20:02 108-20-3 v209/02/22 15:410.0081 1
Ethylbenzene ND mg/kg 09/02/22 20:02 100-41-409/02/22 15:410.0081 1
Hexachloro-1,3-butadiene ND mg/kg 09/02/22 20:02 87-68-3 IK09/02/22 15:410.016 1
2-Hexanone ND mg/kg 09/02/22 20:02 591-78-609/02/22 15:410.081 1
Isopropylbenzene (Cumene)ND mg/kg 09/02/22 20:02 98-82-809/02/22 15:410.0081 1
p-Isopropyltoluene ND mg/kg 09/02/22 20:02 99-87-609/02/22 15:410.0081 1
Methylene Chloride ND mg/kg 09/02/22 20:02 75-09-2 L2,v209/02/22 15:410.032 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 09/02/22 20:02 108-10-109/02/22 15:410.081 1
Methyl-tert-butyl ether ND mg/kg 09/02/22 20:02 1634-04-409/02/22 15:410.0081 1
Naphthalene ND mg/kg 09/02/22 20:02 91-20-309/02/22 15:410.0081 1
n-Propylbenzene ND mg/kg 09/02/22 20:02 103-65-109/02/22 15:410.0081 1
Styrene ND mg/kg 09/02/22 20:02 100-42-509/02/22 15:410.0081 1
1,1,1,2-Tetrachloroethane ND mg/kg 09/02/22 20:02 630-20-609/02/22 15:410.0081 1
1,1,2,2-Tetrachloroethane ND mg/kg 09/02/22 20:02 79-34-509/02/22 15:410.0081 1
Tetrachloroethene ND mg/kg 09/02/22 20:02 127-18-4 IK09/02/22 15:410.0081 1
Toluene ND mg/kg 09/02/22 20:02 108-88-309/02/22 15:410.0081 1
1,2,3-Trichlorobenzene ND mg/kg 09/02/22 20:02 87-61-609/02/22 15:410.0081 1
1,2,4-Trichlorobenzene ND mg/kg 09/02/22 20:02 120-82-109/02/22 15:410.0081 1
1,1,1-Trichloroethane ND mg/kg 09/02/22 20:02 71-55-609/02/22 15:410.0081 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Sample:HA-1 Lab ID:92623480001 Collected:08/29/22 13:20 Received:09/01/22 10:05 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,1,2-Trichloroethane ND mg/kg 09/02/22 20:02 79-00-509/02/22 15:410.0081 1
Trichloroethene ND mg/kg 09/02/22 20:02 79-01-609/02/22 15:410.0081 1
Trichlorofluoromethane ND mg/kg 09/02/22 20:02 75-69-409/02/22 15:410.0081 1
1,2,3-Trichloropropane ND mg/kg 09/02/22 20:02 96-18-409/02/22 15:410.0081 1
1,2,4-Trimethylbenzene ND mg/kg 09/02/22 20:02 95-63-609/02/22 15:410.0081 1
1,3,5-Trimethylbenzene ND mg/kg 09/02/22 20:02 108-67-809/02/22 15:410.0081 1
Vinyl acetate ND mg/kg 09/02/22 20:02 108-05-409/02/22 15:410.081 1
Vinyl chloride ND mg/kg 09/02/22 20:02 75-01-409/02/22 15:410.016 1
Xylene (Total)ND mg/kg 09/02/22 20:02 1330-20-709/02/22 15:410.016 1
m&p-Xylene ND mg/kg 09/02/22 20:02 179601-23-109/02/22 15:410.016 1
o-Xylene 0.0094 mg/kg 09/02/22 20:02 95-47-609/02/22 15:410.0081 1
Surrogates
Toluene-d8 (S)97 %09/02/22 20:02 2037-26-509/02/22 15:4170-130 1
4-Bromofluorobenzene (S)100 %09/02/22 20:02 460-00-409/02/22 15:4170-130 1
1,2-Dichloroethane-d4 (S)88 %09/02/22 20:02 17060-07-009/02/22 15:4170-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 18.8 %09/01/22 17:31 N20.10 1
Sample:HA-2 Lab ID:92623480002 Collected:08/29/22 13:40 Received:09/01/22 10:05 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 09/06/22 17:54 83-32-909/03/22 23:210.39 1
Acenaphthylene ND mg/kg 09/06/22 17:54 208-96-809/03/22 23:210.39 1
Aniline ND mg/kg 09/06/22 17:54 62-53-309/03/22 23:210.39 1
Anthracene ND mg/kg 09/06/22 17:54 120-12-709/03/22 23:210.39 1
Benzo(a)anthracene ND mg/kg 09/06/22 17:54 56-55-309/03/22 23:210.39 1
Benzo(a)pyrene ND mg/kg 09/06/22 17:54 50-32-809/03/22 23:210.39 1
Benzo(b)fluoranthene ND mg/kg 09/06/22 17:54 205-99-209/03/22 23:210.39 1
Benzo(g,h,i)perylene ND mg/kg 09/06/22 17:54 191-24-209/03/22 23:210.39 1
Benzo(k)fluoranthene ND mg/kg 09/06/22 17:54 207-08-909/03/22 23:210.39 1
Benzoic Acid ND mg/kg 09/06/22 17:54 65-85-009/03/22 23:212.0 1
Benzyl alcohol ND mg/kg 09/06/22 17:54 100-51-609/03/22 23:210.79 1
4-Bromophenylphenyl ether ND mg/kg 09/06/22 17:54 101-55-309/03/22 23:210.39 1
Butylbenzylphthalate ND mg/kg 09/06/22 17:54 85-68-709/03/22 23:210.39 1
4-Chloro-3-methylphenol ND mg/kg 09/06/22 17:54 59-50-709/03/22 23:210.79 1
4-Chloroaniline ND mg/kg 09/06/22 17:54 106-47-809/03/22 23:210.79 1
bis(2-Chloroethoxy)methane ND mg/kg 09/06/22 17:54 111-91-109/03/22 23:210.39 1
bis(2-Chloroethyl) ether ND mg/kg 09/06/22 17:54 111-44-409/03/22 23:210.39 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Sample:HA-2 Lab ID:92623480002 Collected:08/29/22 13:40 Received:09/01/22 10:05 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2-Chloronaphthalene ND mg/kg 09/06/22 17:54 91-58-709/03/22 23:210.39 1
2-Chlorophenol ND mg/kg 09/06/22 17:54 95-57-809/03/22 23:210.39 1
4-Chlorophenylphenyl ether ND mg/kg 09/06/22 17:54 7005-72-309/03/22 23:210.39 1
Chrysene ND mg/kg 09/06/22 17:54 218-01-909/03/22 23:210.39 1
Dibenz(a,h)anthracene ND mg/kg 09/06/22 17:54 53-70-309/03/22 23:210.39 1
Dibenzofuran ND mg/kg 09/06/22 17:54 132-64-909/03/22 23:210.39 1
1,2-Dichlorobenzene ND mg/kg 09/06/22 17:54 95-50-109/03/22 23:210.39 1
1,3-Dichlorobenzene ND mg/kg 09/06/22 17:54 541-73-109/03/22 23:210.39 1
1,4-Dichlorobenzene ND mg/kg 09/06/22 17:54 106-46-709/03/22 23:210.39 1
3,3'-Dichlorobenzidine ND mg/kg 09/06/22 17:54 91-94-109/03/22 23:210.79 1
2,4-Dichlorophenol ND mg/kg 09/06/22 17:54 120-83-209/03/22 23:210.39 1
Diethylphthalate ND mg/kg 09/06/22 17:54 84-66-209/03/22 23:210.39 1
2,4-Dimethylphenol ND mg/kg 09/06/22 17:54 105-67-909/03/22 23:210.39 1
Dimethylphthalate ND mg/kg 09/06/22 17:54 131-11-309/03/22 23:210.39 1
Di-n-butylphthalate ND mg/kg 09/06/22 17:54 84-74-209/03/22 23:210.39 1
4,6-Dinitro-2-methylphenol ND mg/kg 09/06/22 17:54 534-52-109/03/22 23:210.79 1
2,4-Dinitrophenol ND mg/kg 09/06/22 17:54 51-28-509/03/22 23:212.0 1
2,4-Dinitrotoluene ND mg/kg 09/06/22 17:54 121-14-209/03/22 23:210.39 1
2,6-Dinitrotoluene ND mg/kg 09/06/22 17:54 606-20-209/03/22 23:210.39 1
Di-n-octylphthalate ND mg/kg 09/06/22 17:54 117-84-009/03/22 23:210.39 1
bis(2-Ethylhexyl)phthalate ND mg/kg 09/06/22 17:54 117-81-7 v209/03/22 23:210.39 1
Fluoranthene ND mg/kg 09/06/22 17:54 206-44-009/03/22 23:210.39 1
Fluorene ND mg/kg 09/06/22 17:54 86-73-709/03/22 23:210.39 1
Hexachloro-1,3-butadiene ND mg/kg 09/06/22 17:54 87-68-309/03/22 23:210.39 1
Hexachlorobenzene ND mg/kg 09/06/22 17:54 118-74-109/03/22 23:210.39 1
Hexachlorocyclopentadiene ND mg/kg 09/06/22 17:54 77-47-409/03/22 23:210.39 1
Hexachloroethane ND mg/kg 09/06/22 17:54 67-72-109/03/22 23:210.39 1
Indeno(1,2,3-cd)pyrene ND mg/kg 09/06/22 17:54 193-39-509/03/22 23:210.39 1
Isophorone ND mg/kg 09/06/22 17:54 78-59-109/03/22 23:210.39 1
1-Methylnaphthalene ND mg/kg 09/06/22 17:54 90-12-009/03/22 23:210.39 1
2-Methylnaphthalene ND mg/kg 09/06/22 17:54 91-57-609/03/22 23:210.39 1
2-Methylphenol(o-Cresol)ND mg/kg 09/06/22 17:54 95-48-709/03/22 23:210.39 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 09/06/22 17:54 15831-10-409/03/22 23:210.39 1
Naphthalene ND mg/kg 09/06/22 17:54 91-20-309/03/22 23:210.39 1
2-Nitroaniline ND mg/kg 09/06/22 17:54 88-74-409/03/22 23:212.0 1
3-Nitroaniline ND mg/kg 09/06/22 17:54 99-09-209/03/22 23:212.0 1
4-Nitroaniline ND mg/kg 09/06/22 17:54 100-01-609/03/22 23:210.79 1
Nitrobenzene ND mg/kg 09/06/22 17:54 98-95-309/03/22 23:210.39 1
2-Nitrophenol ND mg/kg 09/06/22 17:54 88-75-509/03/22 23:210.39 1
4-Nitrophenol ND mg/kg 09/06/22 17:54 100-02-709/03/22 23:212.0 1
N-Nitrosodimethylamine ND mg/kg 09/06/22 17:54 62-75-909/03/22 23:210.39 1
N-Nitroso-di-n-propylamine ND mg/kg 09/06/22 17:54 621-64-709/03/22 23:210.39 1
N-Nitrosodiphenylamine ND mg/kg 09/06/22 17:54 86-30-609/03/22 23:210.39 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 09/06/22 17:54 108-60-109/03/22 23:210.39 1
Pentachlorophenol ND mg/kg 09/06/22 17:54 87-86-509/03/22 23:210.79 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Sample:HA-2 Lab ID:92623480002 Collected:08/29/22 13:40 Received:09/01/22 10:05 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Phenanthrene ND mg/kg 09/06/22 17:54 85-01-809/03/22 23:210.39 1
Phenol ND mg/kg 09/06/22 17:54 108-95-209/03/22 23:210.39 1
Pyrene ND mg/kg 09/06/22 17:54 129-00-009/03/22 23:210.39 1
Pyridine ND mg/kg 09/06/22 17:54 110-86-109/03/22 23:210.39 1
1,2,4-Trichlorobenzene ND mg/kg 09/06/22 17:54 120-82-109/03/22 23:210.39 1
2,4,5-Trichlorophenol ND mg/kg 09/06/22 17:54 95-95-409/03/22 23:210.39 1
2,4,6-Trichlorophenol ND mg/kg 09/06/22 17:54 88-06-209/03/22 23:210.39 1
Surrogates
Nitrobenzene-d5 (S)55 %09/06/22 17:54 4165-60-009/03/22 23:2121-130 1
2-Fluorobiphenyl (S)49 %09/06/22 17:54 321-60-809/03/22 23:2119-130 1
Terphenyl-d14 (S)72 %09/06/22 17:54 1718-51-009/03/22 23:2115-130 1
Phenol-d6 (S)53 %09/06/22 17:54 13127-88-309/03/22 23:2118-130 1
2-Fluorophenol (S)57 %09/06/22 17:54 367-12-409/03/22 23:2118-130 1
2,4,6-Tribromophenol (S)73 %09/06/22 17:54 118-79-609/03/22 23:2118-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 09/02/22 20:19 67-64-1 v209/02/22 15:410.15 1
Benzene ND mg/kg 09/02/22 20:19 71-43-209/02/22 15:410.0076 1
Bromobenzene ND mg/kg 09/02/22 20:19 108-86-109/02/22 15:410.0076 1
Bromochloromethane ND mg/kg 09/02/22 20:19 74-97-509/02/22 15:410.0076 1
Bromodichloromethane ND mg/kg 09/02/22 20:19 75-27-409/02/22 15:410.0076 1
Bromoform ND mg/kg 09/02/22 20:19 75-25-209/02/22 15:410.0076 1
Bromomethane ND mg/kg 09/02/22 20:19 74-83-909/02/22 15:410.015 1
2-Butanone (MEK)ND mg/kg 09/02/22 20:19 78-93-3 v209/02/22 15:410.15 1
n-Butylbenzene ND mg/kg 09/02/22 20:19 104-51-809/02/22 15:410.0076 1
sec-Butylbenzene ND mg/kg 09/02/22 20:19 135-98-809/02/22 15:410.0076 1
tert-Butylbenzene ND mg/kg 09/02/22 20:19 98-06-609/02/22 15:410.0076 1
Carbon tetrachloride ND mg/kg 09/02/22 20:19 56-23-509/02/22 15:410.0076 1
Chlorobenzene ND mg/kg 09/02/22 20:19 108-90-709/02/22 15:410.0076 1
Chloroethane ND mg/kg 09/02/22 20:19 75-00-309/02/22 15:410.015 1
Chloroform ND mg/kg 09/02/22 20:19 67-66-309/02/22 15:410.0076 1
Chloromethane ND mg/kg 09/02/22 20:19 74-87-309/02/22 15:410.015 1
2-Chlorotoluene ND mg/kg 09/02/22 20:19 95-49-809/02/22 15:410.0076 1
4-Chlorotoluene ND mg/kg 09/02/22 20:19 106-43-409/02/22 15:410.0076 1
1,2-Dibromo-3-chloropropane ND mg/kg 09/02/22 20:19 96-12-809/02/22 15:410.0076 1
Dibromochloromethane ND mg/kg 09/02/22 20:19 124-48-109/02/22 15:410.0076 1
1,2-Dibromoethane (EDB)ND mg/kg 09/02/22 20:19 106-93-409/02/22 15:410.0076 1
Dibromomethane ND mg/kg 09/02/22 20:19 74-95-309/02/22 15:410.0076 1
1,2-Dichlorobenzene ND mg/kg 09/02/22 20:19 95-50-109/02/22 15:410.0076 1
1,3-Dichlorobenzene ND mg/kg 09/02/22 20:19 541-73-109/02/22 15:410.0076 1
1,4-Dichlorobenzene ND mg/kg 09/02/22 20:19 106-46-709/02/22 15:410.0076 1
Dichlorodifluoromethane ND mg/kg 09/02/22 20:19 75-71-809/02/22 15:410.015 1
1,1-Dichloroethane ND mg/kg 09/02/22 20:19 75-34-309/02/22 15:410.0076 1
1,2-Dichloroethane ND mg/kg 09/02/22 20:19 107-06-209/02/22 15:410.0076 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Sample:HA-2 Lab ID:92623480002 Collected:08/29/22 13:40 Received:09/01/22 10:05 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,1-Dichloroethene ND mg/kg 09/02/22 20:19 75-35-409/02/22 15:410.0076 1
cis-1,2-Dichloroethene ND mg/kg 09/02/22 20:19 156-59-209/02/22 15:410.0076 1
trans-1,2-Dichloroethene ND mg/kg 09/02/22 20:19 156-60-509/02/22 15:410.0076 1
1,2-Dichloropropane ND mg/kg 09/02/22 20:19 78-87-509/02/22 15:410.0076 1
1,3-Dichloropropane ND mg/kg 09/02/22 20:19 142-28-909/02/22 15:410.0076 1
2,2-Dichloropropane ND mg/kg 09/02/22 20:19 594-20-7 v209/02/22 15:410.0076 1
1,1-Dichloropropene ND mg/kg 09/02/22 20:19 563-58-609/02/22 15:410.0076 1
cis-1,3-Dichloropropene ND mg/kg 09/02/22 20:19 10061-01-509/02/22 15:410.0076 1
trans-1,3-Dichloropropene ND mg/kg 09/02/22 20:19 10061-02-609/02/22 15:410.0076 1
Diisopropyl ether ND mg/kg 09/02/22 20:19 108-20-3 v209/02/22 15:410.0076 1
Ethylbenzene ND mg/kg 09/02/22 20:19 100-41-409/02/22 15:410.0076 1
Hexachloro-1,3-butadiene ND mg/kg 09/02/22 20:19 87-68-3 IK09/02/22 15:410.015 1
2-Hexanone ND mg/kg 09/02/22 20:19 591-78-609/02/22 15:410.076 1
Isopropylbenzene (Cumene)ND mg/kg 09/02/22 20:19 98-82-809/02/22 15:410.0076 1
p-Isopropyltoluene ND mg/kg 09/02/22 20:19 99-87-609/02/22 15:410.0076 1
Methylene Chloride ND mg/kg 09/02/22 20:19 75-09-2 L2,v209/02/22 15:410.030 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 09/02/22 20:19 108-10-109/02/22 15:410.076 1
Methyl-tert-butyl ether ND mg/kg 09/02/22 20:19 1634-04-409/02/22 15:410.0076 1
Naphthalene ND mg/kg 09/02/22 20:19 91-20-309/02/22 15:410.0076 1
n-Propylbenzene ND mg/kg 09/02/22 20:19 103-65-109/02/22 15:410.0076 1
Styrene ND mg/kg 09/02/22 20:19 100-42-509/02/22 15:410.0076 1
1,1,1,2-Tetrachloroethane ND mg/kg 09/02/22 20:19 630-20-609/02/22 15:410.0076 1
1,1,2,2-Tetrachloroethane ND mg/kg 09/02/22 20:19 79-34-509/02/22 15:410.0076 1
Tetrachloroethene ND mg/kg 09/02/22 20:19 127-18-4 IK09/02/22 15:410.0076 1
Toluene ND mg/kg 09/02/22 20:19 108-88-309/02/22 15:410.0076 1
1,2,3-Trichlorobenzene ND mg/kg 09/02/22 20:19 87-61-609/02/22 15:410.0076 1
1,2,4-Trichlorobenzene ND mg/kg 09/02/22 20:19 120-82-109/02/22 15:410.0076 1
1,1,1-Trichloroethane ND mg/kg 09/02/22 20:19 71-55-609/02/22 15:410.0076 1
1,1,2-Trichloroethane ND mg/kg 09/02/22 20:19 79-00-509/02/22 15:410.0076 1
Trichloroethene ND mg/kg 09/02/22 20:19 79-01-609/02/22 15:410.0076 1
Trichlorofluoromethane ND mg/kg 09/02/22 20:19 75-69-409/02/22 15:410.0076 1
1,2,3-Trichloropropane ND mg/kg 09/02/22 20:19 96-18-409/02/22 15:410.0076 1
1,2,4-Trimethylbenzene ND mg/kg 09/02/22 20:19 95-63-609/02/22 15:410.0076 1
1,3,5-Trimethylbenzene ND mg/kg 09/02/22 20:19 108-67-809/02/22 15:410.0076 1
Vinyl acetate ND mg/kg 09/02/22 20:19 108-05-409/02/22 15:410.076 1
Vinyl chloride ND mg/kg 09/02/22 20:19 75-01-409/02/22 15:410.015 1
Xylene (Total)ND mg/kg 09/02/22 20:19 1330-20-709/02/22 15:410.015 1
m&p-Xylene ND mg/kg 09/02/22 20:19 179601-23-109/02/22 15:410.015 1
o-Xylene 0.0079 mg/kg 09/02/22 20:19 95-47-609/02/22 15:410.0076 1
Surrogates
Toluene-d8 (S)98 %09/02/22 20:19 2037-26-509/02/22 15:4170-130 1
4-Bromofluorobenzene (S)98 %09/02/22 20:19 460-00-409/02/22 15:4170-130 1
1,2-Dichloroethane-d4 (S)88 %09/02/22 20:19 17060-07-009/02/22 15:4170-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Sample:HA-2 Lab ID:92623480002 Collected:08/29/22 13:40 Received:09/01/22 10:05 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 15.9 %09/01/22 17:31 N20.10 1
Sample:HA-3 Lab ID:92623480003 Collected:08/29/22 14:30 Received:09/01/22 10:05 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 09/06/22 18:22 83-32-909/03/22 23:210.35 1
Acenaphthylene ND mg/kg 09/06/22 18:22 208-96-809/03/22 23:210.35 1
Aniline ND mg/kg 09/06/22 18:22 62-53-309/03/22 23:210.35 1
Anthracene ND mg/kg 09/06/22 18:22 120-12-709/03/22 23:210.35 1
Benzo(a)anthracene ND mg/kg 09/06/22 18:22 56-55-309/03/22 23:210.35 1
Benzo(a)pyrene ND mg/kg 09/06/22 18:22 50-32-809/03/22 23:210.35 1
Benzo(b)fluoranthene ND mg/kg 09/06/22 18:22 205-99-209/03/22 23:210.35 1
Benzo(g,h,i)perylene ND mg/kg 09/06/22 18:22 191-24-209/03/22 23:210.35 1
Benzo(k)fluoranthene ND mg/kg 09/06/22 18:22 207-08-909/03/22 23:210.35 1
Benzoic Acid ND mg/kg 09/06/22 18:22 65-85-009/03/22 23:211.8 1
Benzyl alcohol ND mg/kg 09/06/22 18:22 100-51-609/03/22 23:210.71 1
4-Bromophenylphenyl ether ND mg/kg 09/06/22 18:22 101-55-309/03/22 23:210.35 1
Butylbenzylphthalate ND mg/kg 09/06/22 18:22 85-68-709/03/22 23:210.35 1
4-Chloro-3-methylphenol ND mg/kg 09/06/22 18:22 59-50-709/03/22 23:210.71 1
4-Chloroaniline ND mg/kg 09/06/22 18:22 106-47-809/03/22 23:210.71 1
bis(2-Chloroethoxy)methane ND mg/kg 09/06/22 18:22 111-91-109/03/22 23:210.35 1
bis(2-Chloroethyl) ether ND mg/kg 09/06/22 18:22 111-44-409/03/22 23:210.35 1
2-Chloronaphthalene ND mg/kg 09/06/22 18:22 91-58-709/03/22 23:210.35 1
2-Chlorophenol ND mg/kg 09/06/22 18:22 95-57-809/03/22 23:210.35 1
4-Chlorophenylphenyl ether ND mg/kg 09/06/22 18:22 7005-72-309/03/22 23:210.35 1
Chrysene ND mg/kg 09/06/22 18:22 218-01-909/03/22 23:210.35 1
Dibenz(a,h)anthracene ND mg/kg 09/06/22 18:22 53-70-309/03/22 23:210.35 1
Dibenzofuran ND mg/kg 09/06/22 18:22 132-64-909/03/22 23:210.35 1
1,2-Dichlorobenzene ND mg/kg 09/06/22 18:22 95-50-109/03/22 23:210.35 1
1,3-Dichlorobenzene ND mg/kg 09/06/22 18:22 541-73-109/03/22 23:210.35 1
1,4-Dichlorobenzene ND mg/kg 09/06/22 18:22 106-46-709/03/22 23:210.35 1
3,3'-Dichlorobenzidine ND mg/kg 09/06/22 18:22 91-94-109/03/22 23:210.71 1
2,4-Dichlorophenol ND mg/kg 09/06/22 18:22 120-83-209/03/22 23:210.35 1
Diethylphthalate ND mg/kg 09/06/22 18:22 84-66-209/03/22 23:210.35 1
2,4-Dimethylphenol ND mg/kg 09/06/22 18:22 105-67-909/03/22 23:210.35 1
Dimethylphthalate ND mg/kg 09/06/22 18:22 131-11-309/03/22 23:210.35 1
Di-n-butylphthalate ND mg/kg 09/06/22 18:22 84-74-209/03/22 23:210.35 1
4,6-Dinitro-2-methylphenol ND mg/kg 09/06/22 18:22 534-52-109/03/22 23:210.71 1
2,4-Dinitrophenol ND mg/kg 09/06/22 18:22 51-28-509/03/22 23:211.8 1
2,4-Dinitrotoluene ND mg/kg 09/06/22 18:22 121-14-209/03/22 23:210.35 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Sample:HA-3 Lab ID:92623480003 Collected:08/29/22 14:30 Received:09/01/22 10:05 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,6-Dinitrotoluene ND mg/kg 09/06/22 18:22 606-20-209/03/22 23:210.35 1
Di-n-octylphthalate ND mg/kg 09/06/22 18:22 117-84-009/03/22 23:210.35 1
bis(2-Ethylhexyl)phthalate ND mg/kg 09/06/22 18:22 117-81-7 v209/03/22 23:210.35 1
Fluoranthene ND mg/kg 09/06/22 18:22 206-44-009/03/22 23:210.35 1
Fluorene ND mg/kg 09/06/22 18:22 86-73-709/03/22 23:210.35 1
Hexachloro-1,3-butadiene ND mg/kg 09/06/22 18:22 87-68-309/03/22 23:210.35 1
Hexachlorobenzene ND mg/kg 09/06/22 18:22 118-74-109/03/22 23:210.35 1
Hexachlorocyclopentadiene ND mg/kg 09/06/22 18:22 77-47-409/03/22 23:210.35 1
Hexachloroethane ND mg/kg 09/06/22 18:22 67-72-109/03/22 23:210.35 1
Indeno(1,2,3-cd)pyrene ND mg/kg 09/06/22 18:22 193-39-509/03/22 23:210.35 1
Isophorone ND mg/kg 09/06/22 18:22 78-59-109/03/22 23:210.35 1
1-Methylnaphthalene ND mg/kg 09/06/22 18:22 90-12-009/03/22 23:210.35 1
2-Methylnaphthalene ND mg/kg 09/06/22 18:22 91-57-609/03/22 23:210.35 1
2-Methylphenol(o-Cresol)ND mg/kg 09/06/22 18:22 95-48-709/03/22 23:210.35 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 09/06/22 18:22 15831-10-409/03/22 23:210.35 1
Naphthalene ND mg/kg 09/06/22 18:22 91-20-309/03/22 23:210.35 1
2-Nitroaniline ND mg/kg 09/06/22 18:22 88-74-409/03/22 23:211.8 1
3-Nitroaniline ND mg/kg 09/06/22 18:22 99-09-209/03/22 23:211.8 1
4-Nitroaniline ND mg/kg 09/06/22 18:22 100-01-609/03/22 23:210.71 1
Nitrobenzene ND mg/kg 09/06/22 18:22 98-95-309/03/22 23:210.35 1
2-Nitrophenol ND mg/kg 09/06/22 18:22 88-75-509/03/22 23:210.35 1
4-Nitrophenol ND mg/kg 09/06/22 18:22 100-02-709/03/22 23:211.8 1
N-Nitrosodimethylamine ND mg/kg 09/06/22 18:22 62-75-909/03/22 23:210.35 1
N-Nitroso-di-n-propylamine ND mg/kg 09/06/22 18:22 621-64-709/03/22 23:210.35 1
N-Nitrosodiphenylamine ND mg/kg 09/06/22 18:22 86-30-609/03/22 23:210.35 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 09/06/22 18:22 108-60-109/03/22 23:210.35 1
Pentachlorophenol ND mg/kg 09/06/22 18:22 87-86-509/03/22 23:210.71 1
Phenanthrene ND mg/kg 09/06/22 18:22 85-01-809/03/22 23:210.35 1
Phenol ND mg/kg 09/06/22 18:22 108-95-209/03/22 23:210.35 1
Pyrene ND mg/kg 09/06/22 18:22 129-00-009/03/22 23:210.35 1
Pyridine ND mg/kg 09/06/22 18:22 110-86-109/03/22 23:210.35 1
1,2,4-Trichlorobenzene ND mg/kg 09/06/22 18:22 120-82-109/03/22 23:210.35 1
2,4,5-Trichlorophenol ND mg/kg 09/06/22 18:22 95-95-409/03/22 23:210.35 1
2,4,6-Trichlorophenol ND mg/kg 09/06/22 18:22 88-06-209/03/22 23:210.35 1
Surrogates
Nitrobenzene-d5 (S)38 %09/06/22 18:22 4165-60-009/03/22 23:2121-130 1
2-Fluorobiphenyl (S)42 %09/06/22 18:22 321-60-809/03/22 23:2119-130 1
Terphenyl-d14 (S)62 %09/06/22 18:22 1718-51-009/03/22 23:2115-130 1
Phenol-d6 (S)39 %09/06/22 18:22 13127-88-309/03/22 23:2118-130 1
2-Fluorophenol (S)40 %09/06/22 18:22 367-12-409/03/22 23:2118-130 1
2,4,6-Tribromophenol (S)63 %09/06/22 18:22 118-79-609/03/22 23:2118-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 09/02/22 20:55 67-64-1 v209/02/22 15:410.14 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Sample:HA-3 Lab ID:92623480003 Collected:08/29/22 14:30 Received:09/01/22 10:05 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Benzene ND mg/kg 09/02/22 20:55 71-43-209/02/22 15:410.0072 1
Bromobenzene ND mg/kg 09/02/22 20:55 108-86-109/02/22 15:410.0072 1
Bromochloromethane ND mg/kg 09/02/22 20:55 74-97-509/02/22 15:410.0072 1
Bromodichloromethane ND mg/kg 09/02/22 20:55 75-27-409/02/22 15:410.0072 1
Bromoform ND mg/kg 09/02/22 20:55 75-25-209/02/22 15:410.0072 1
Bromomethane ND mg/kg 09/02/22 20:55 74-83-909/02/22 15:410.014 1
2-Butanone (MEK)ND mg/kg 09/02/22 20:55 78-93-3 v209/02/22 15:410.14 1
n-Butylbenzene ND mg/kg 09/02/22 20:55 104-51-809/02/22 15:410.0072 1
sec-Butylbenzene ND mg/kg 09/02/22 20:55 135-98-809/02/22 15:410.0072 1
tert-Butylbenzene ND mg/kg 09/02/22 20:55 98-06-609/02/22 15:410.0072 1
Carbon tetrachloride ND mg/kg 09/02/22 20:55 56-23-509/02/22 15:410.0072 1
Chlorobenzene ND mg/kg 09/02/22 20:55 108-90-709/02/22 15:410.0072 1
Chloroethane ND mg/kg 09/02/22 20:55 75-00-309/02/22 15:410.014 1
Chloroform ND mg/kg 09/02/22 20:55 67-66-309/02/22 15:410.0072 1
Chloromethane ND mg/kg 09/02/22 20:55 74-87-309/02/22 15:410.014 1
2-Chlorotoluene ND mg/kg 09/02/22 20:55 95-49-809/02/22 15:410.0072 1
4-Chlorotoluene ND mg/kg 09/02/22 20:55 106-43-409/02/22 15:410.0072 1
1,2-Dibromo-3-chloropropane ND mg/kg 09/02/22 20:55 96-12-809/02/22 15:410.0072 1
Dibromochloromethane ND mg/kg 09/02/22 20:55 124-48-109/02/22 15:410.0072 1
1,2-Dibromoethane (EDB)ND mg/kg 09/02/22 20:55 106-93-409/02/22 15:410.0072 1
Dibromomethane ND mg/kg 09/02/22 20:55 74-95-309/02/22 15:410.0072 1
1,2-Dichlorobenzene ND mg/kg 09/02/22 20:55 95-50-109/02/22 15:410.0072 1
1,3-Dichlorobenzene ND mg/kg 09/02/22 20:55 541-73-109/02/22 15:410.0072 1
1,4-Dichlorobenzene ND mg/kg 09/02/22 20:55 106-46-709/02/22 15:410.0072 1
Dichlorodifluoromethane ND mg/kg 09/02/22 20:55 75-71-809/02/22 15:410.014 1
1,1-Dichloroethane ND mg/kg 09/02/22 20:55 75-34-309/02/22 15:410.0072 1
1,2-Dichloroethane ND mg/kg 09/02/22 20:55 107-06-209/02/22 15:410.0072 1
1,1-Dichloroethene ND mg/kg 09/02/22 20:55 75-35-409/02/22 15:410.0072 1
cis-1,2-Dichloroethene ND mg/kg 09/02/22 20:55 156-59-209/02/22 15:410.0072 1
trans-1,2-Dichloroethene ND mg/kg 09/02/22 20:55 156-60-509/02/22 15:410.0072 1
1,2-Dichloropropane ND mg/kg 09/02/22 20:55 78-87-509/02/22 15:410.0072 1
1,3-Dichloropropane ND mg/kg 09/02/22 20:55 142-28-909/02/22 15:410.0072 1
2,2-Dichloropropane ND mg/kg 09/02/22 20:55 594-20-7 v209/02/22 15:410.0072 1
1,1-Dichloropropene ND mg/kg 09/02/22 20:55 563-58-609/02/22 15:410.0072 1
cis-1,3-Dichloropropene ND mg/kg 09/02/22 20:55 10061-01-509/02/22 15:410.0072 1
trans-1,3-Dichloropropene ND mg/kg 09/02/22 20:55 10061-02-609/02/22 15:410.0072 1
Diisopropyl ether ND mg/kg 09/02/22 20:55 108-20-3 v209/02/22 15:410.0072 1
Ethylbenzene ND mg/kg 09/02/22 20:55 100-41-409/02/22 15:410.0072 1
Hexachloro-1,3-butadiene ND mg/kg 09/02/22 20:55 87-68-3 IK09/02/22 15:410.014 1
2-Hexanone ND mg/kg 09/02/22 20:55 591-78-609/02/22 15:410.072 1
Isopropylbenzene (Cumene)ND mg/kg 09/02/22 20:55 98-82-809/02/22 15:410.0072 1
p-Isopropyltoluene ND mg/kg 09/02/22 20:55 99-87-609/02/22 15:410.0072 1
Methylene Chloride ND mg/kg 09/02/22 20:55 75-09-2 L2,v209/02/22 15:410.029 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 09/02/22 20:55 108-10-109/02/22 15:410.072 1
Methyl-tert-butyl ether ND mg/kg 09/02/22 20:55 1634-04-409/02/22 15:410.0072 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Sample:HA-3 Lab ID:92623480003 Collected:08/29/22 14:30 Received:09/01/22 10:05 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Naphthalene ND mg/kg 09/02/22 20:55 91-20-309/02/22 15:410.0072 1
n-Propylbenzene ND mg/kg 09/02/22 20:55 103-65-109/02/22 15:410.0072 1
Styrene ND mg/kg 09/02/22 20:55 100-42-509/02/22 15:410.0072 1
1,1,1,2-Tetrachloroethane ND mg/kg 09/02/22 20:55 630-20-609/02/22 15:410.0072 1
1,1,2,2-Tetrachloroethane ND mg/kg 09/02/22 20:55 79-34-509/02/22 15:410.0072 1
Tetrachloroethene ND mg/kg 09/02/22 20:55 127-18-4 IK09/02/22 15:410.0072 1
Toluene ND mg/kg 09/02/22 20:55 108-88-309/02/22 15:410.0072 1
1,2,3-Trichlorobenzene ND mg/kg 09/02/22 20:55 87-61-609/02/22 15:410.0072 1
1,2,4-Trichlorobenzene ND mg/kg 09/02/22 20:55 120-82-109/02/22 15:410.0072 1
1,1,1-Trichloroethane ND mg/kg 09/02/22 20:55 71-55-609/02/22 15:410.0072 1
1,1,2-Trichloroethane ND mg/kg 09/02/22 20:55 79-00-509/02/22 15:410.0072 1
Trichloroethene ND mg/kg 09/02/22 20:55 79-01-609/02/22 15:410.0072 1
Trichlorofluoromethane ND mg/kg 09/02/22 20:55 75-69-409/02/22 15:410.0072 1
1,2,3-Trichloropropane ND mg/kg 09/02/22 20:55 96-18-409/02/22 15:410.0072 1
1,2,4-Trimethylbenzene ND mg/kg 09/02/22 20:55 95-63-609/02/22 15:410.0072 1
1,3,5-Trimethylbenzene ND mg/kg 09/02/22 20:55 108-67-809/02/22 15:410.0072 1
Vinyl acetate ND mg/kg 09/02/22 20:55 108-05-409/02/22 15:410.072 1
Vinyl chloride ND mg/kg 09/02/22 20:55 75-01-409/02/22 15:410.014 1
Xylene (Total)ND mg/kg 09/02/22 20:55 1330-20-709/02/22 15:410.014 1
m&p-Xylene ND mg/kg 09/02/22 20:55 179601-23-109/02/22 15:410.014 1
o-Xylene 0.0074 mg/kg 09/02/22 20:55 95-47-609/02/22 15:410.0072 1
Surrogates
Toluene-d8 (S)96 %09/02/22 20:55 2037-26-509/02/22 15:4170-130 1
4-Bromofluorobenzene (S)98 %09/02/22 20:55 460-00-409/02/22 15:4170-130 1
1,2-Dichloroethane-d4 (S)86 %09/02/22 20:55 17060-07-009/02/22 15:4170-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 8.1 %09/01/22 17:31 N20.10 1
Sample:HA-4 Lab ID:92623480004 Collected:08/29/22 15:30 Received:09/01/22 10:05 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 09/06/22 18:50 83-32-909/03/22 23:210.36 1
Acenaphthylene ND mg/kg 09/06/22 18:50 208-96-809/03/22 23:210.36 1
Aniline ND mg/kg 09/06/22 18:50 62-53-309/03/22 23:210.36 1
Anthracene ND mg/kg 09/06/22 18:50 120-12-709/03/22 23:210.36 1
Benzo(a)anthracene ND mg/kg 09/06/22 18:50 56-55-309/03/22 23:210.36 1
Benzo(a)pyrene ND mg/kg 09/06/22 18:50 50-32-809/03/22 23:210.36 1
Benzo(b)fluoranthene ND mg/kg 09/06/22 18:50 205-99-209/03/22 23:210.36 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Sample:HA-4 Lab ID:92623480004 Collected:08/29/22 15:30 Received:09/01/22 10:05 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Benzo(g,h,i)perylene ND mg/kg 09/06/22 18:50 191-24-209/03/22 23:210.36 1
Benzo(k)fluoranthene ND mg/kg 09/06/22 18:50 207-08-909/03/22 23:210.36 1
Benzoic Acid ND mg/kg 09/06/22 18:50 65-85-009/03/22 23:211.8 1
Benzyl alcohol ND mg/kg 09/06/22 18:50 100-51-609/03/22 23:210.71 1
4-Bromophenylphenyl ether ND mg/kg 09/06/22 18:50 101-55-309/03/22 23:210.36 1
Butylbenzylphthalate ND mg/kg 09/06/22 18:50 85-68-709/03/22 23:210.36 1
4-Chloro-3-methylphenol ND mg/kg 09/06/22 18:50 59-50-709/03/22 23:210.71 1
4-Chloroaniline ND mg/kg 09/06/22 18:50 106-47-809/03/22 23:210.71 1
bis(2-Chloroethoxy)methane ND mg/kg 09/06/22 18:50 111-91-109/03/22 23:210.36 1
bis(2-Chloroethyl) ether ND mg/kg 09/06/22 18:50 111-44-409/03/22 23:210.36 1
2-Chloronaphthalene ND mg/kg 09/06/22 18:50 91-58-709/03/22 23:210.36 1
2-Chlorophenol ND mg/kg 09/06/22 18:50 95-57-809/03/22 23:210.36 1
4-Chlorophenylphenyl ether ND mg/kg 09/06/22 18:50 7005-72-309/03/22 23:210.36 1
Chrysene ND mg/kg 09/06/22 18:50 218-01-909/03/22 23:210.36 1
Dibenz(a,h)anthracene ND mg/kg 09/06/22 18:50 53-70-309/03/22 23:210.36 1
Dibenzofuran ND mg/kg 09/06/22 18:50 132-64-909/03/22 23:210.36 1
1,2-Dichlorobenzene ND mg/kg 09/06/22 18:50 95-50-109/03/22 23:210.36 1
1,3-Dichlorobenzene ND mg/kg 09/06/22 18:50 541-73-109/03/22 23:210.36 1
1,4-Dichlorobenzene ND mg/kg 09/06/22 18:50 106-46-709/03/22 23:210.36 1
3,3'-Dichlorobenzidine ND mg/kg 09/06/22 18:50 91-94-109/03/22 23:210.71 1
2,4-Dichlorophenol ND mg/kg 09/06/22 18:50 120-83-209/03/22 23:210.36 1
Diethylphthalate ND mg/kg 09/06/22 18:50 84-66-209/03/22 23:210.36 1
2,4-Dimethylphenol ND mg/kg 09/06/22 18:50 105-67-909/03/22 23:210.36 1
Dimethylphthalate ND mg/kg 09/06/22 18:50 131-11-309/03/22 23:210.36 1
Di-n-butylphthalate ND mg/kg 09/06/22 18:50 84-74-209/03/22 23:210.36 1
4,6-Dinitro-2-methylphenol ND mg/kg 09/06/22 18:50 534-52-109/03/22 23:210.71 1
2,4-Dinitrophenol ND mg/kg 09/06/22 18:50 51-28-509/03/22 23:211.8 1
2,4-Dinitrotoluene ND mg/kg 09/06/22 18:50 121-14-209/03/22 23:210.36 1
2,6-Dinitrotoluene ND mg/kg 09/06/22 18:50 606-20-209/03/22 23:210.36 1
Di-n-octylphthalate ND mg/kg 09/06/22 18:50 117-84-009/03/22 23:210.36 1
bis(2-Ethylhexyl)phthalate ND mg/kg 09/06/22 18:50 117-81-7 v209/03/22 23:210.36 1
Fluoranthene ND mg/kg 09/06/22 18:50 206-44-009/03/22 23:210.36 1
Fluorene ND mg/kg 09/06/22 18:50 86-73-709/03/22 23:210.36 1
Hexachloro-1,3-butadiene ND mg/kg 09/06/22 18:50 87-68-309/03/22 23:210.36 1
Hexachlorobenzene ND mg/kg 09/06/22 18:50 118-74-109/03/22 23:210.36 1
Hexachlorocyclopentadiene ND mg/kg 09/06/22 18:50 77-47-409/03/22 23:210.36 1
Hexachloroethane ND mg/kg 09/06/22 18:50 67-72-109/03/22 23:210.36 1
Indeno(1,2,3-cd)pyrene ND mg/kg 09/06/22 18:50 193-39-509/03/22 23:210.36 1
Isophorone ND mg/kg 09/06/22 18:50 78-59-109/03/22 23:210.36 1
1-Methylnaphthalene ND mg/kg 09/06/22 18:50 90-12-009/03/22 23:210.36 1
2-Methylnaphthalene ND mg/kg 09/06/22 18:50 91-57-609/03/22 23:210.36 1
2-Methylphenol(o-Cresol)ND mg/kg 09/06/22 18:50 95-48-709/03/22 23:210.36 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 09/06/22 18:50 15831-10-409/03/22 23:210.36 1
Naphthalene ND mg/kg 09/06/22 18:50 91-20-309/03/22 23:210.36 1
2-Nitroaniline ND mg/kg 09/06/22 18:50 88-74-409/03/22 23:211.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Sample:HA-4 Lab ID:92623480004 Collected:08/29/22 15:30 Received:09/01/22 10:05 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
3-Nitroaniline ND mg/kg 09/06/22 18:50 99-09-209/03/22 23:211.8 1
4-Nitroaniline ND mg/kg 09/06/22 18:50 100-01-609/03/22 23:210.71 1
Nitrobenzene ND mg/kg 09/06/22 18:50 98-95-309/03/22 23:210.36 1
2-Nitrophenol ND mg/kg 09/06/22 18:50 88-75-509/03/22 23:210.36 1
4-Nitrophenol ND mg/kg 09/06/22 18:50 100-02-709/03/22 23:211.8 1
N-Nitrosodimethylamine ND mg/kg 09/06/22 18:50 62-75-909/03/22 23:210.36 1
N-Nitroso-di-n-propylamine ND mg/kg 09/06/22 18:50 621-64-709/03/22 23:210.36 1
N-Nitrosodiphenylamine ND mg/kg 09/06/22 18:50 86-30-609/03/22 23:210.36 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 09/06/22 18:50 108-60-109/03/22 23:210.36 1
Pentachlorophenol ND mg/kg 09/06/22 18:50 87-86-509/03/22 23:210.71 1
Phenanthrene ND mg/kg 09/06/22 18:50 85-01-809/03/22 23:210.36 1
Phenol ND mg/kg 09/06/22 18:50 108-95-209/03/22 23:210.36 1
Pyrene ND mg/kg 09/06/22 18:50 129-00-009/03/22 23:210.36 1
Pyridine ND mg/kg 09/06/22 18:50 110-86-109/03/22 23:210.36 1
1,2,4-Trichlorobenzene ND mg/kg 09/06/22 18:50 120-82-109/03/22 23:210.36 1
2,4,5-Trichlorophenol ND mg/kg 09/06/22 18:50 95-95-409/03/22 23:210.36 1
2,4,6-Trichlorophenol ND mg/kg 09/06/22 18:50 88-06-209/03/22 23:210.36 1
Surrogates
Nitrobenzene-d5 (S)41 %09/06/22 18:50 4165-60-009/03/22 23:2121-130 1
2-Fluorobiphenyl (S)40 %09/06/22 18:50 321-60-809/03/22 23:2119-130 1
Terphenyl-d14 (S)46 %09/06/22 18:50 1718-51-009/03/22 23:2115-130 1
Phenol-d6 (S)42 %09/06/22 18:50 13127-88-309/03/22 23:2118-130 1
2-Fluorophenol (S)44 %09/06/22 18:50 367-12-409/03/22 23:2118-130 1
2,4,6-Tribromophenol (S)43 %09/06/22 18:50 118-79-609/03/22 23:2118-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 09/02/22 21:12 67-64-1 v209/02/22 15:410.11 1
Benzene ND mg/kg 09/02/22 21:12 71-43-209/02/22 15:410.0055 1
Bromobenzene ND mg/kg 09/02/22 21:12 108-86-109/02/22 15:410.0055 1
Bromochloromethane ND mg/kg 09/02/22 21:12 74-97-509/02/22 15:410.0055 1
Bromodichloromethane ND mg/kg 09/02/22 21:12 75-27-409/02/22 15:410.0055 1
Bromoform ND mg/kg 09/02/22 21:12 75-25-209/02/22 15:410.0055 1
Bromomethane ND mg/kg 09/02/22 21:12 74-83-909/02/22 15:410.011 1
2-Butanone (MEK)ND mg/kg 09/02/22 21:12 78-93-3 v209/02/22 15:410.11 1
n-Butylbenzene ND mg/kg 09/02/22 21:12 104-51-809/02/22 15:410.0055 1
sec-Butylbenzene ND mg/kg 09/02/22 21:12 135-98-809/02/22 15:410.0055 1
tert-Butylbenzene ND mg/kg 09/02/22 21:12 98-06-609/02/22 15:410.0055 1
Carbon tetrachloride ND mg/kg 09/02/22 21:12 56-23-509/02/22 15:410.0055 1
Chlorobenzene ND mg/kg 09/02/22 21:12 108-90-709/02/22 15:410.0055 1
Chloroethane ND mg/kg 09/02/22 21:12 75-00-309/02/22 15:410.011 1
Chloroform ND mg/kg 09/02/22 21:12 67-66-309/02/22 15:410.0055 1
Chloromethane ND mg/kg 09/02/22 21:12 74-87-309/02/22 15:410.011 1
2-Chlorotoluene ND mg/kg 09/02/22 21:12 95-49-809/02/22 15:410.0055 1
4-Chlorotoluene ND mg/kg 09/02/22 21:12 106-43-409/02/22 15:410.0055 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Sample:HA-4 Lab ID:92623480004 Collected:08/29/22 15:30 Received:09/01/22 10:05 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2-Dibromo-3-chloropropane ND mg/kg 09/02/22 21:12 96-12-809/02/22 15:410.0055 1
Dibromochloromethane ND mg/kg 09/02/22 21:12 124-48-109/02/22 15:410.0055 1
1,2-Dibromoethane (EDB)ND mg/kg 09/02/22 21:12 106-93-409/02/22 15:410.0055 1
Dibromomethane ND mg/kg 09/02/22 21:12 74-95-309/02/22 15:410.0055 1
1,2-Dichlorobenzene ND mg/kg 09/02/22 21:12 95-50-109/02/22 15:410.0055 1
1,3-Dichlorobenzene ND mg/kg 09/02/22 21:12 541-73-109/02/22 15:410.0055 1
1,4-Dichlorobenzene ND mg/kg 09/02/22 21:12 106-46-709/02/22 15:410.0055 1
Dichlorodifluoromethane ND mg/kg 09/02/22 21:12 75-71-809/02/22 15:410.011 1
1,1-Dichloroethane ND mg/kg 09/02/22 21:12 75-34-309/02/22 15:410.0055 1
1,2-Dichloroethane ND mg/kg 09/02/22 21:12 107-06-209/02/22 15:410.0055 1
1,1-Dichloroethene ND mg/kg 09/02/22 21:12 75-35-409/02/22 15:410.0055 1
cis-1,2-Dichloroethene ND mg/kg 09/02/22 21:12 156-59-209/02/22 15:410.0055 1
trans-1,2-Dichloroethene ND mg/kg 09/02/22 21:12 156-60-509/02/22 15:410.0055 1
1,2-Dichloropropane ND mg/kg 09/02/22 21:12 78-87-509/02/22 15:410.0055 1
1,3-Dichloropropane ND mg/kg 09/02/22 21:12 142-28-909/02/22 15:410.0055 1
2,2-Dichloropropane ND mg/kg 09/02/22 21:12 594-20-7 v209/02/22 15:410.0055 1
1,1-Dichloropropene ND mg/kg 09/02/22 21:12 563-58-609/02/22 15:410.0055 1
cis-1,3-Dichloropropene ND mg/kg 09/02/22 21:12 10061-01-509/02/22 15:410.0055 1
trans-1,3-Dichloropropene ND mg/kg 09/02/22 21:12 10061-02-609/02/22 15:410.0055 1
Diisopropyl ether ND mg/kg 09/02/22 21:12 108-20-3 v209/02/22 15:410.0055 1
Ethylbenzene ND mg/kg 09/02/22 21:12 100-41-409/02/22 15:410.0055 1
Hexachloro-1,3-butadiene ND mg/kg 09/02/22 21:12 87-68-3 IK09/02/22 15:410.011 1
2-Hexanone ND mg/kg 09/02/22 21:12 591-78-609/02/22 15:410.055 1
Isopropylbenzene (Cumene)ND mg/kg 09/02/22 21:12 98-82-809/02/22 15:410.0055 1
p-Isopropyltoluene ND mg/kg 09/02/22 21:12 99-87-609/02/22 15:410.0055 1
Methylene Chloride ND mg/kg 09/02/22 21:12 75-09-2 L2,v209/02/22 15:410.022 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 09/02/22 21:12 108-10-109/02/22 15:410.055 1
Methyl-tert-butyl ether ND mg/kg 09/02/22 21:12 1634-04-409/02/22 15:410.0055 1
Naphthalene ND mg/kg 09/02/22 21:12 91-20-309/02/22 15:410.0055 1
n-Propylbenzene ND mg/kg 09/02/22 21:12 103-65-109/02/22 15:410.0055 1
Styrene ND mg/kg 09/02/22 21:12 100-42-509/02/22 15:410.0055 1
1,1,1,2-Tetrachloroethane ND mg/kg 09/02/22 21:12 630-20-609/02/22 15:410.0055 1
1,1,2,2-Tetrachloroethane ND mg/kg 09/02/22 21:12 79-34-509/02/22 15:410.0055 1
Tetrachloroethene ND mg/kg 09/02/22 21:12 127-18-4 IK09/02/22 15:410.0055 1
Toluene ND mg/kg 09/02/22 21:12 108-88-309/02/22 15:410.0055 1
1,2,3-Trichlorobenzene ND mg/kg 09/02/22 21:12 87-61-609/02/22 15:410.0055 1
1,2,4-Trichlorobenzene ND mg/kg 09/02/22 21:12 120-82-109/02/22 15:410.0055 1
1,1,1-Trichloroethane ND mg/kg 09/02/22 21:12 71-55-609/02/22 15:410.0055 1
1,1,2-Trichloroethane ND mg/kg 09/02/22 21:12 79-00-509/02/22 15:410.0055 1
Trichloroethene ND mg/kg 09/02/22 21:12 79-01-609/02/22 15:410.0055 1
Trichlorofluoromethane ND mg/kg 09/02/22 21:12 75-69-409/02/22 15:410.0055 1
1,2,3-Trichloropropane ND mg/kg 09/02/22 21:12 96-18-409/02/22 15:410.0055 1
1,2,4-Trimethylbenzene ND mg/kg 09/02/22 21:12 95-63-609/02/22 15:410.0055 1
1,3,5-Trimethylbenzene ND mg/kg 09/02/22 21:12 108-67-809/02/22 15:410.0055 1
Vinyl acetate ND mg/kg 09/02/22 21:12 108-05-409/02/22 15:410.055 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Sample:HA-4 Lab ID:92623480004 Collected:08/29/22 15:30 Received:09/01/22 10:05 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Vinyl chloride ND mg/kg 09/02/22 21:12 75-01-409/02/22 15:410.011 1
Xylene (Total)ND mg/kg 09/02/22 21:12 1330-20-709/02/22 15:410.011 1
m&p-Xylene ND mg/kg 09/02/22 21:12 179601-23-109/02/22 15:410.011 1
o-Xylene 0.0055 mg/kg 09/02/22 21:12 95-47-609/02/22 15:410.0055 1
Surrogates
Toluene-d8 (S)98 %09/02/22 21:12 2037-26-509/02/22 15:4170-130 1
4-Bromofluorobenzene (S)99 %09/02/22 21:12 460-00-409/02/22 15:4170-130 1
1,2-Dichloroethane-d4 (S)85 %09/02/22 21:12 17060-07-009/02/22 15:4170-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 6.1 %09/01/22 17:32 N20.10 1
Sample:SB-1 Lab ID:92623480005 Collected:08/31/22 14:15 Received:09/01/22 10:05 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Soil
Aliphatic (C09-C18)914 mg/kg 09/12/22 13:51 N209/09/22 11:3812510
Aliphatic (C19-C36)ND mg/kg 09/12/22 13:51 N209/09/22 11:3812510
Aromatic (C11-C22)129 mg/kg 09/12/22 12:18 N209/09/22 11:3812.5 1
Surrogates
1-Chlorooctadecane (S)0 %09/12/22 13:51 3386-33-2 S409/09/22 11:3840-140 10
o-Terphenyl (S)70 %09/12/22 12:18 84-15-109/09/22 11:3840-140 1
2-Fluorobiphenyl (S)188 %09/12/22 12:18 321-60-8 S509/09/22 11:3840-140 1
2-Bromonaphthalene (S)166 %09/12/22 12:18 580-13-2 S509/09/22 11:3840-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Pace Analytical Services - Charlotte
VPH NC Soil
Aliphatic (C05-C08)27.8 mg/kg 09/03/22 00:12 N209/02/22 11:324.3 1
Aliphatic(C09-C12) Adjusted 284 mg/kg 09/03/22 00:12 N209/02/22 11:324.3 1
Aromatic (C09-C10)312 mg/kg 09/03/22 00:12 N209/02/22 11:324.3 1
Surrogates
4-Bromofluorobenzene (FID) (S)344 %09/03/22 00:12 460-00-4 S509/02/22 11:3270-130 1
4-Bromofluorobenzene (PID) (S)156 %09/03/22 00:12 460-00-4 S509/02/22 11:3270-130 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 09/06/22 19:18 83-32-909/03/22 23:210.41 1
Acenaphthylene ND mg/kg 09/06/22 19:18 208-96-809/03/22 23:210.41 1
Aniline ND mg/kg 09/06/22 19:18 62-53-309/03/22 23:210.41 1
Anthracene ND mg/kg 09/06/22 19:18 120-12-709/03/22 23:210.41 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Sample:SB-1 Lab ID:92623480005 Collected:08/31/22 14:15 Received:09/01/22 10:05 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Benzo(a)anthracene ND mg/kg 09/06/22 19:18 56-55-309/03/22 23:210.41 1
Benzo(a)pyrene ND mg/kg 09/06/22 19:18 50-32-809/03/22 23:210.41 1
Benzo(b)fluoranthene ND mg/kg 09/06/22 19:18 205-99-209/03/22 23:210.41 1
Benzo(g,h,i)perylene ND mg/kg 09/06/22 19:18 191-24-209/03/22 23:210.41 1
Benzo(k)fluoranthene ND mg/kg 09/06/22 19:18 207-08-909/03/22 23:210.41 1
Benzoic Acid ND mg/kg 09/06/22 19:18 65-85-009/03/22 23:212.1 1
Benzyl alcohol ND mg/kg 09/06/22 19:18 100-51-609/03/22 23:210.83 1
4-Bromophenylphenyl ether ND mg/kg 09/06/22 19:18 101-55-309/03/22 23:210.41 1
Butylbenzylphthalate ND mg/kg 09/06/22 19:18 85-68-709/03/22 23:210.41 1
4-Chloro-3-methylphenol ND mg/kg 09/06/22 19:18 59-50-709/03/22 23:210.83 1
4-Chloroaniline ND mg/kg 09/06/22 19:18 106-47-809/03/22 23:210.83 1
bis(2-Chloroethoxy)methane ND mg/kg 09/06/22 19:18 111-91-109/03/22 23:210.41 1
bis(2-Chloroethyl) ether ND mg/kg 09/06/22 19:18 111-44-409/03/22 23:210.41 1
2-Chloronaphthalene ND mg/kg 09/06/22 19:18 91-58-709/03/22 23:210.41 1
2-Chlorophenol ND mg/kg 09/06/22 19:18 95-57-809/03/22 23:210.41 1
4-Chlorophenylphenyl ether ND mg/kg 09/06/22 19:18 7005-72-309/03/22 23:210.41 1
Chrysene ND mg/kg 09/06/22 19:18 218-01-909/03/22 23:210.41 1
Dibenz(a,h)anthracene ND mg/kg 09/06/22 19:18 53-70-309/03/22 23:210.41 1
Dibenzofuran ND mg/kg 09/06/22 19:18 132-64-909/03/22 23:210.41 1
1,2-Dichlorobenzene ND mg/kg 09/06/22 19:18 95-50-109/03/22 23:210.41 1
1,3-Dichlorobenzene ND mg/kg 09/06/22 19:18 541-73-109/03/22 23:210.41 1
1,4-Dichlorobenzene ND mg/kg 09/06/22 19:18 106-46-709/03/22 23:210.41 1
3,3'-Dichlorobenzidine ND mg/kg 09/06/22 19:18 91-94-109/03/22 23:210.83 1
2,4-Dichlorophenol ND mg/kg 09/06/22 19:18 120-83-209/03/22 23:210.41 1
Diethylphthalate ND mg/kg 09/06/22 19:18 84-66-209/03/22 23:210.41 1
2,4-Dimethylphenol ND mg/kg 09/06/22 19:18 105-67-909/03/22 23:210.41 1
Dimethylphthalate ND mg/kg 09/06/22 19:18 131-11-309/03/22 23:210.41 1
Di-n-butylphthalate ND mg/kg 09/06/22 19:18 84-74-209/03/22 23:210.41 1
4,6-Dinitro-2-methylphenol ND mg/kg 09/06/22 19:18 534-52-109/03/22 23:210.83 1
2,4-Dinitrophenol ND mg/kg 09/06/22 19:18 51-28-509/03/22 23:212.1 1
2,4-Dinitrotoluene ND mg/kg 09/06/22 19:18 121-14-209/03/22 23:210.41 1
2,6-Dinitrotoluene ND mg/kg 09/06/22 19:18 606-20-209/03/22 23:210.41 1
Di-n-octylphthalate ND mg/kg 09/06/22 19:18 117-84-009/03/22 23:210.41 1
bis(2-Ethylhexyl)phthalate ND mg/kg 09/06/22 19:18 117-81-7 v209/03/22 23:210.41 1
Fluoranthene ND mg/kg 09/06/22 19:18 206-44-009/03/22 23:210.41 1
Fluorene ND mg/kg 09/06/22 19:18 86-73-709/03/22 23:210.41 1
Hexachloro-1,3-butadiene ND mg/kg 09/06/22 19:18 87-68-309/03/22 23:210.41 1
Hexachlorobenzene ND mg/kg 09/06/22 19:18 118-74-109/03/22 23:210.41 1
Hexachlorocyclopentadiene ND mg/kg 09/06/22 19:18 77-47-409/03/22 23:210.41 1
Hexachloroethane ND mg/kg 09/06/22 19:18 67-72-109/03/22 23:210.41 1
Indeno(1,2,3-cd)pyrene ND mg/kg 09/06/22 19:18 193-39-509/03/22 23:210.41 1
Isophorone ND mg/kg 09/06/22 19:18 78-59-109/03/22 23:210.41 1
1-Methylnaphthalene 3.2 mg/kg 09/06/22 19:18 90-12-009/03/22 23:210.41 1
2-Methylnaphthalene 3.7 mg/kg 09/08/22 09:36 91-57-609/03/22 23:210.83 2
2-Methylphenol(o-Cresol)ND mg/kg 09/06/22 19:18 95-48-709/03/22 23:210.41 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Sample:SB-1 Lab ID:92623480005 Collected:08/31/22 14:15 Received:09/01/22 10:05 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
3&4-Methylphenol(m&p Cresol)ND mg/kg 09/06/22 19:18 15831-10-409/03/22 23:210.41 1
Naphthalene 1.3 mg/kg 09/06/22 19:18 91-20-309/03/22 23:210.41 1
2-Nitroaniline ND mg/kg 09/06/22 19:18 88-74-409/03/22 23:212.1 1
3-Nitroaniline ND mg/kg 09/06/22 19:18 99-09-209/03/22 23:212.1 1
4-Nitroaniline ND mg/kg 09/06/22 19:18 100-01-609/03/22 23:210.83 1
Nitrobenzene ND mg/kg 09/06/22 19:18 98-95-309/03/22 23:210.41 1
2-Nitrophenol ND mg/kg 09/06/22 19:18 88-75-509/03/22 23:210.41 1
4-Nitrophenol ND mg/kg 09/06/22 19:18 100-02-709/03/22 23:212.1 1
N-Nitrosodimethylamine ND mg/kg 09/06/22 19:18 62-75-909/03/22 23:210.41 1
N-Nitroso-di-n-propylamine ND mg/kg 09/06/22 19:18 621-64-709/03/22 23:210.41 1
N-Nitrosodiphenylamine ND mg/kg 09/06/22 19:18 86-30-609/03/22 23:210.41 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 09/06/22 19:18 108-60-109/03/22 23:210.41 1
Pentachlorophenol ND mg/kg 09/06/22 19:18 87-86-509/03/22 23:210.83 1
Phenanthrene ND mg/kg 09/06/22 19:18 85-01-809/03/22 23:210.41 1
Phenol ND mg/kg 09/06/22 19:18 108-95-209/03/22 23:210.41 1
Pyrene ND mg/kg 09/06/22 19:18 129-00-009/03/22 23:210.41 1
Pyridine ND mg/kg 09/06/22 19:18 110-86-109/03/22 23:210.41 1
1,2,4-Trichlorobenzene ND mg/kg 09/06/22 19:18 120-82-109/03/22 23:210.41 1
2,4,5-Trichlorophenol ND mg/kg 09/06/22 19:18 95-95-409/03/22 23:210.41 1
2,4,6-Trichlorophenol ND mg/kg 09/06/22 19:18 88-06-209/03/22 23:210.41 1
Surrogates
Nitrobenzene-d5 (S)71 %09/06/22 19:18 4165-60-009/03/22 23:2121-130 1
2-Fluorobiphenyl (S)68 %09/06/22 19:18 321-60-809/03/22 23:2119-130 1
Terphenyl-d14 (S)73 %09/06/22 19:18 1718-51-009/03/22 23:2115-130 1
Phenol-d6 (S)57 %09/06/22 19:18 13127-88-309/03/22 23:2118-130 1
2-Fluorophenol (S)60 %09/06/22 19:18 367-12-409/03/22 23:2118-130 1
2,4,6-Tribromophenol (S)81 %09/06/22 19:18 118-79-609/03/22 23:2118-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 09/03/22 04:00 67-64-1 v209/02/22 15:417.8 50
Benzene ND mg/kg 09/03/22 04:00 71-43-209/02/22 15:410.39 50
Bromobenzene ND mg/kg 09/03/22 04:00 108-86-109/02/22 15:410.39 50
Bromochloromethane ND mg/kg 09/03/22 04:00 74-97-509/02/22 15:410.39 50
Bromodichloromethane ND mg/kg 09/03/22 04:00 75-27-409/02/22 15:410.39 50
Bromoform ND mg/kg 09/03/22 04:00 75-25-209/02/22 15:410.39 50
Bromomethane ND mg/kg 09/03/22 04:00 74-83-909/02/22 15:410.78 50
2-Butanone (MEK)ND mg/kg 09/03/22 04:00 78-93-3 v209/02/22 15:417.8 50
n-Butylbenzene ND mg/kg 09/03/22 04:00 104-51-809/02/22 15:410.39 50
sec-Butylbenzene ND mg/kg 09/03/22 04:00 135-98-809/02/22 15:410.39 50
tert-Butylbenzene ND mg/kg 09/03/22 04:00 98-06-609/02/22 15:410.39 50
Carbon tetrachloride ND mg/kg 09/03/22 04:00 56-23-509/02/22 15:410.39 50
Chlorobenzene ND mg/kg 09/03/22 04:00 108-90-709/02/22 15:410.39 50
Chloroethane ND mg/kg 09/03/22 04:00 75-00-309/02/22 15:410.78 50
Chloroform ND mg/kg 09/03/22 04:00 67-66-309/02/22 15:410.39 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Sample:SB-1 Lab ID:92623480005 Collected:08/31/22 14:15 Received:09/01/22 10:05 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Chloromethane ND mg/kg 09/03/22 04:00 74-87-309/02/22 15:410.78 50
2-Chlorotoluene ND mg/kg 09/03/22 04:00 95-49-809/02/22 15:410.39 50
4-Chlorotoluene ND mg/kg 09/03/22 04:00 106-43-409/02/22 15:410.39 50
1,2-Dibromo-3-chloropropane ND mg/kg 09/03/22 04:00 96-12-809/02/22 15:410.39 50
Dibromochloromethane ND mg/kg 09/03/22 04:00 124-48-109/02/22 15:410.39 50
1,2-Dibromoethane (EDB)ND mg/kg 09/03/22 04:00 106-93-409/02/22 15:410.39 50
Dibromomethane ND mg/kg 09/03/22 04:00 74-95-309/02/22 15:410.39 50
1,2-Dichlorobenzene ND mg/kg 09/03/22 04:00 95-50-109/02/22 15:410.39 50
1,3-Dichlorobenzene ND mg/kg 09/03/22 04:00 541-73-109/02/22 15:410.39 50
1,4-Dichlorobenzene ND mg/kg 09/03/22 04:00 106-46-709/02/22 15:410.39 50
Dichlorodifluoromethane ND mg/kg 09/03/22 04:00 75-71-809/02/22 15:410.78 50
1,1-Dichloroethane ND mg/kg 09/03/22 04:00 75-34-309/02/22 15:410.39 50
1,2-Dichloroethane ND mg/kg 09/03/22 04:00 107-06-209/02/22 15:410.39 50
1,1-Dichloroethene ND mg/kg 09/03/22 04:00 75-35-409/02/22 15:410.39 50
cis-1,2-Dichloroethene ND mg/kg 09/03/22 04:00 156-59-209/02/22 15:410.39 50
trans-1,2-Dichloroethene ND mg/kg 09/03/22 04:00 156-60-509/02/22 15:410.39 50
1,2-Dichloropropane ND mg/kg 09/03/22 04:00 78-87-509/02/22 15:410.39 50
1,3-Dichloropropane ND mg/kg 09/03/22 04:00 142-28-909/02/22 15:410.39 50
2,2-Dichloropropane ND mg/kg 09/03/22 04:00 594-20-7 v209/02/22 15:410.39 50
1,1-Dichloropropene ND mg/kg 09/03/22 04:00 563-58-609/02/22 15:410.39 50
cis-1,3-Dichloropropene ND mg/kg 09/03/22 04:00 10061-01-509/02/22 15:410.39 50
trans-1,3-Dichloropropene ND mg/kg 09/03/22 04:00 10061-02-609/02/22 15:410.39 50
Diisopropyl ether ND mg/kg 09/03/22 04:00 108-20-3 v209/02/22 15:410.39 50
Ethylbenzene ND mg/kg 09/03/22 04:00 100-41-409/02/22 15:410.39 50
Hexachloro-1,3-butadiene ND mg/kg 09/03/22 04:00 87-68-3 IK09/02/22 15:410.78 50
2-Hexanone ND mg/kg 09/03/22 04:00 591-78-609/02/22 15:413.9 50
Isopropylbenzene (Cumene)ND mg/kg 09/03/22 04:00 98-82-809/02/22 15:410.39 50
p-Isopropyltoluene 2.8 mg/kg 09/03/22 04:00 99-87-609/02/22 15:410.39 50
Methylene Chloride ND mg/kg 09/03/22 04:00 75-09-2 L2,v209/02/22 15:411.6 50
4-Methyl-2-pentanone (MIBK)ND mg/kg 09/03/22 04:00 108-10-109/02/22 15:413.9 50
Methyl-tert-butyl ether ND mg/kg 09/03/22 04:00 1634-04-409/02/22 15:410.39 50
Naphthalene 3.6 mg/kg 09/03/22 04:00 91-20-309/02/22 15:410.39 50
n-Propylbenzene ND mg/kg 09/03/22 04:00 103-65-109/02/22 15:410.39 50
Styrene ND mg/kg 09/03/22 04:00 100-42-509/02/22 15:410.39 50
1,1,1,2-Tetrachloroethane ND mg/kg 09/03/22 04:00 630-20-609/02/22 15:410.39 50
1,1,2,2-Tetrachloroethane ND mg/kg 09/03/22 04:00 79-34-509/02/22 15:410.39 50
Tetrachloroethene ND mg/kg 09/03/22 04:00 127-18-4 IK09/02/22 15:410.39 50
Toluene ND mg/kg 09/03/22 04:00 108-88-309/02/22 15:410.39 50
1,2,3-Trichlorobenzene ND mg/kg 09/03/22 04:00 87-61-609/02/22 15:410.39 50
1,2,4-Trichlorobenzene ND mg/kg 09/03/22 04:00 120-82-109/02/22 15:410.39 50
1,1,1-Trichloroethane ND mg/kg 09/03/22 04:00 71-55-609/02/22 15:410.39 50
1,1,2-Trichloroethane ND mg/kg 09/03/22 04:00 79-00-509/02/22 15:410.39 50
Trichloroethene ND mg/kg 09/03/22 04:00 79-01-609/02/22 15:410.39 50
Trichlorofluoromethane ND mg/kg 09/03/22 04:00 75-69-409/02/22 15:410.39 50
1,2,3-Trichloropropane ND mg/kg 09/03/22 04:00 96-18-409/02/22 15:410.39 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Sample:SB-1 Lab ID:92623480005 Collected:08/31/22 14:15 Received:09/01/22 10:05 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2,4-Trimethylbenzene 7.4 mg/kg 09/03/22 04:00 95-63-609/02/22 15:410.39 50
1,3,5-Trimethylbenzene 4.6 mg/kg 09/03/22 04:00 108-67-809/02/22 15:410.39 50
Vinyl acetate ND mg/kg 09/03/22 04:00 108-05-409/02/22 15:413.9 50
Vinyl chloride ND mg/kg 09/03/22 04:00 75-01-409/02/22 15:410.78 50
Xylene (Total)ND mg/kg 09/03/22 04:00 1330-20-709/02/22 15:410.78 50
m&p-Xylene ND mg/kg 09/03/22 04:00 179601-23-109/02/22 15:410.78 50
o-Xylene 0.50 mg/kg 09/03/22 04:00 95-47-609/02/22 15:410.39 50
Surrogates
Toluene-d8 (S)95 %09/03/22 04:00 2037-26-509/02/22 15:4170-130 50
4-Bromofluorobenzene (S)104 %09/03/22 04:00 460-00-409/02/22 15:4170-130 50
1,2-Dichloroethane-d4 (S)82 %09/03/22 04:00 17060-07-009/02/22 15:4170-130 50
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 20.2 %09/01/22 17:32 N20.10 1
Sample:TW-1 Lab ID:92623480006 Collected:08/31/22 09:45 Received:09/01/22 10:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 09/06/22 21:16 83-32-909/06/22 12:008.3 1
Acenaphthylene ND ug/L 09/06/22 21:16 208-96-809/06/22 12:008.3 1
Aniline ND ug/L 09/06/22 21:16 62-53-309/06/22 12:008.3 1
Anthracene ND ug/L 09/06/22 21:16 120-12-709/06/22 12:008.3 1
Benzo(a)anthracene ND ug/L 09/06/22 21:16 56-55-309/06/22 12:008.3 1
Benzo(a)pyrene ND ug/L 09/06/22 21:16 50-32-809/06/22 12:008.3 1
Benzo(b)fluoranthene ND ug/L 09/06/22 21:16 205-99-209/06/22 12:008.3 1
Benzo(g,h,i)perylene ND ug/L 09/06/22 21:16 191-24-209/06/22 12:008.3 1
Benzo(k)fluoranthene ND ug/L 09/06/22 21:16 207-08-909/06/22 12:008.3 1
Benzoic Acid ND ug/L 09/06/22 21:16 65-85-009/06/22 12:0041.7 1
Benzyl alcohol ND ug/L 09/06/22 21:16 100-51-609/06/22 12:0016.7 1
4-Bromophenylphenyl ether ND ug/L 09/06/22 21:16 101-55-309/06/22 12:008.3 1
Butylbenzylphthalate ND ug/L 09/06/22 21:16 85-68-709/06/22 12:008.3 1
4-Chloro-3-methylphenol ND ug/L 09/06/22 21:16 59-50-709/06/22 12:008.3 1
4-Chloroaniline ND ug/L 09/06/22 21:16 106-47-809/06/22 12:0016.7 1
bis(2-Chloroethoxy)methane ND ug/L 09/06/22 21:16 111-91-109/06/22 12:008.3 1
bis(2-Chloroethyl) ether ND ug/L 09/06/22 21:16 111-44-409/06/22 12:008.3 1
2-Chloronaphthalene ND ug/L 09/06/22 21:16 91-58-709/06/22 12:008.3 1
2-Chlorophenol ND ug/L 09/06/22 21:16 95-57-809/06/22 12:008.3 1
4-Chlorophenylphenyl ether ND ug/L 09/06/22 21:16 7005-72-309/06/22 12:008.3 1
Chrysene ND ug/L 09/06/22 21:16 218-01-909/06/22 12:008.3 1
Dibenz(a,h)anthracene ND ug/L 09/06/22 21:16 53-70-309/06/22 12:008.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Sample:TW-1 Lab ID:92623480006 Collected:08/31/22 09:45 Received:09/01/22 10:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Dibenzofuran ND ug/L 09/06/22 21:16 132-64-909/06/22 12:008.3 1
1,2-Dichlorobenzene ND ug/L 09/06/22 21:16 95-50-109/06/22 12:008.3 1
1,3-Dichlorobenzene ND ug/L 09/06/22 21:16 541-73-109/06/22 12:008.3 1
1,4-Dichlorobenzene ND ug/L 09/06/22 21:16 106-46-709/06/22 12:008.3 1
3,3'-Dichlorobenzidine ND ug/L 09/06/22 21:16 91-94-109/06/22 12:0016.7 1
2,4-Dichlorophenol ND ug/L 09/06/22 21:16 120-83-209/06/22 12:008.3 1
Diethylphthalate ND ug/L 09/06/22 21:16 84-66-209/06/22 12:008.3 1
2,4-Dimethylphenol ND ug/L 09/06/22 21:16 105-67-909/06/22 12:008.3 1
Dimethylphthalate ND ug/L 09/06/22 21:16 131-11-309/06/22 12:008.3 1
Di-n-butylphthalate ND ug/L 09/06/22 21:16 84-74-209/06/22 12:008.3 1
4,6-Dinitro-2-methylphenol ND ug/L 09/06/22 21:16 534-52-109/06/22 12:0016.7 1
2,4-Dinitrophenol ND ug/L 09/06/22 21:16 51-28-509/06/22 12:0041.7 1
2,4-Dinitrotoluene ND ug/L 09/06/22 21:16 121-14-209/06/22 12:008.3 1
2,6-Dinitrotoluene ND ug/L 09/06/22 21:16 606-20-209/06/22 12:008.3 1
Di-n-octylphthalate ND ug/L 09/06/22 21:16 117-84-009/06/22 12:008.3 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/06/22 21:16 117-81-709/06/22 12:005.0 1
Fluoranthene ND ug/L 09/06/22 21:16 206-44-009/06/22 12:008.3 1
Fluorene ND ug/L 09/06/22 21:16 86-73-709/06/22 12:008.3 1
Hexachloro-1,3-butadiene ND ug/L 09/06/22 21:16 87-68-309/06/22 12:008.3 1
Hexachlorobenzene ND ug/L 09/06/22 21:16 118-74-109/06/22 12:008.3 1
Hexachlorocyclopentadiene ND ug/L 09/06/22 21:16 77-47-409/06/22 12:008.3 1
Hexachloroethane ND ug/L 09/06/22 21:16 67-72-109/06/22 12:008.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/06/22 21:16 193-39-509/06/22 12:008.3 1
Isophorone ND ug/L 09/06/22 21:16 78-59-109/06/22 12:008.3 1
1-Methylnaphthalene ND ug/L 09/06/22 21:16 90-12-009/06/22 12:008.3 1
2-Methylnaphthalene ND ug/L 09/06/22 21:16 91-57-609/06/22 12:008.3 1
2-Methylphenol(o-Cresol)ND ug/L 09/06/22 21:16 95-48-709/06/22 12:008.3 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/06/22 21:16 15831-10-409/06/22 12:008.3 1
Naphthalene ND ug/L 09/06/22 21:16 91-20-309/06/22 12:008.3 1
2-Nitroaniline ND ug/L 09/06/22 21:16 88-74-409/06/22 12:0016.7 1
3-Nitroaniline ND ug/L 09/06/22 21:16 99-09-209/06/22 12:0016.7 1
4-Nitroaniline ND ug/L 09/06/22 21:16 100-01-609/06/22 12:0016.7 1
Nitrobenzene ND ug/L 09/06/22 21:16 98-95-309/06/22 12:008.3 1
2-Nitrophenol ND ug/L 09/06/22 21:16 88-75-509/06/22 12:008.3 1
4-Nitrophenol ND ug/L 09/06/22 21:16 100-02-709/06/22 12:0041.7 1
N-Nitrosodimethylamine ND ug/L 09/06/22 21:16 62-75-909/06/22 12:008.3 1
N-Nitroso-di-n-propylamine ND ug/L 09/06/22 21:16 621-64-709/06/22 12:008.3 1
N-Nitrosodiphenylamine ND ug/L 09/06/22 21:16 86-30-609/06/22 12:008.3 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/06/22 21:16 108-60-109/06/22 12:008.3 1
Pentachlorophenol ND ug/L 09/06/22 21:16 87-86-509/06/22 12:0016.7 1
Phenanthrene ND ug/L 09/06/22 21:16 85-01-809/06/22 12:008.3 1
Phenol ND ug/L 09/06/22 21:16 108-95-209/06/22 12:008.3 1
Pyrene ND ug/L 09/06/22 21:16 129-00-009/06/22 12:008.3 1
1,2,4-Trichlorobenzene ND ug/L 09/06/22 21:16 120-82-109/06/22 12:008.3 1
2,4,5-Trichlorophenol ND ug/L 09/06/22 21:16 95-95-409/06/22 12:008.3 1
2,4,6-Trichlorophenol ND ug/L 09/06/22 21:16 88-06-209/06/22 12:008.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Sample:TW-1 Lab ID:92623480006 Collected:08/31/22 09:45 Received:09/01/22 10:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Surrogates
Nitrobenzene-d5 (S)53 %09/06/22 21:16 4165-60-009/06/22 12:0010-144 1
2-Fluorobiphenyl (S)35 %09/06/22 21:16 321-60-809/06/22 12:0010-130 1
Terphenyl-d14 (S)105 %09/06/22 21:16 1718-51-009/06/22 12:0034-163 1
Phenol-d6 (S)30 %09/06/22 21:16 13127-88-309/06/22 12:0010-130 1
2-Fluorophenol (S)22 %09/06/22 21:16 367-12-409/06/22 12:0010-130 1
2,4,6-Tribromophenol (S)42 %09/06/22 21:16 118-79-609/06/22 12:0010-144 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 09/08/22 19:24 67-64-125.0 1
Benzene ND ug/L 09/08/22 19:24 71-43-21.0 1
Bromobenzene ND ug/L 09/08/22 19:24 108-86-11.0 1
Bromochloromethane ND ug/L 09/08/22 19:24 74-97-51.0 1
Bromodichloromethane ND ug/L 09/08/22 19:24 75-27-41.0 1
Bromoform ND ug/L 09/08/22 19:24 75-25-21.0 1
Bromomethane ND ug/L 09/08/22 19:24 74-83-92.0 1
2-Butanone (MEK)ND ug/L 09/08/22 19:24 78-93-35.0 1
Carbon tetrachloride ND ug/L 09/08/22 19:24 56-23-51.0 1
Chlorobenzene ND ug/L 09/08/22 19:24 108-90-71.0 1
Chloroethane ND ug/L 09/08/22 19:24 75-00-31.0 1
Chloroform ND ug/L 09/08/22 19:24 67-66-31.0 1
Chloromethane ND ug/L 09/08/22 19:24 74-87-31.0 1
2-Chlorotoluene ND ug/L 09/08/22 19:24 95-49-81.0 1
4-Chlorotoluene ND ug/L 09/08/22 19:24 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 09/08/22 19:24 96-12-82.0 1
Dibromochloromethane ND ug/L 09/08/22 19:24 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 09/08/22 19:24 106-93-41.0 1
Dibromomethane ND ug/L 09/08/22 19:24 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 09/08/22 19:24 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 09/08/22 19:24 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 09/08/22 19:24 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 09/08/22 19:24 75-71-81.0 1
1,1-Dichloroethane ND ug/L 09/08/22 19:24 75-34-31.0 1
1,2-Dichloroethane ND ug/L 09/08/22 19:24 107-06-21.0 1
1,1-Dichloroethene ND ug/L 09/08/22 19:24 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 09/08/22 19:24 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 09/08/22 19:24 156-60-51.0 1
1,2-Dichloropropane ND ug/L 09/08/22 19:24 78-87-51.0 1
1,3-Dichloropropane ND ug/L 09/08/22 19:24 142-28-91.0 1
2,2-Dichloropropane ND ug/L 09/08/22 19:24 594-20-71.0 1
1,1-Dichloropropene ND ug/L 09/08/22 19:24 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 09/08/22 19:24 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 09/08/22 19:24 10061-02-61.0 1
Diisopropyl ether ND ug/L 09/08/22 19:24 108-20-31.0 1
Ethylbenzene ND ug/L 09/08/22 19:24 100-41-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Sample:TW-1 Lab ID:92623480006 Collected:08/31/22 09:45 Received:09/01/22 10:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Hexachloro-1,3-butadiene ND ug/L 09/08/22 19:24 87-68-32.0 1
2-Hexanone ND ug/L 09/08/22 19:24 591-78-65.0 1
p-Isopropyltoluene ND ug/L 09/08/22 19:24 99-87-61.0 1
Methylene Chloride ND ug/L 09/08/22 19:24 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/08/22 19:24 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 09/08/22 19:24 1634-04-41.0 1
Naphthalene ND ug/L 09/08/22 19:24 91-20-31.0 1
Styrene ND ug/L 09/08/22 19:24 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 09/08/22 19:24 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 09/08/22 19:24 79-34-51.0 1
Tetrachloroethene ND ug/L 09/08/22 19:24 127-18-41.0 1
Toluene ND ug/L 09/08/22 19:24 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 09/08/22 19:24 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 09/08/22 19:24 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 09/08/22 19:24 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 09/08/22 19:24 79-00-51.0 1
Trichloroethene ND ug/L 09/08/22 19:24 79-01-61.0 1
Trichlorofluoromethane ND ug/L 09/08/22 19:24 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 09/08/22 19:24 96-18-41.0 1
Vinyl acetate ND ug/L 09/08/22 19:24 108-05-4 IK2.0 1
Vinyl chloride ND ug/L 09/08/22 19:24 75-01-41.0 1
Xylene (Total)ND ug/L 09/08/22 19:24 1330-20-71.0 1
m&p-Xylene ND ug/L 09/08/22 19:24 179601-23-12.0 1
o-Xylene ND ug/L 09/08/22 19:24 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)106 %09/08/22 19:24 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %09/08/22 19:24 17060-07-070-130 1
Toluene-d8 (S)105 %09/08/22 19:24 2037-26-570-130 1
Sample:TW-2 Lab ID:92623480007 Collected:08/31/22 10:30 Received:09/01/22 10:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 09/06/22 21:42 83-32-909/06/22 12:008.3 1
Acenaphthylene ND ug/L 09/06/22 21:42 208-96-809/06/22 12:008.3 1
Aniline ND ug/L 09/06/22 21:42 62-53-309/06/22 12:008.3 1
Anthracene ND ug/L 09/06/22 21:42 120-12-709/06/22 12:008.3 1
Benzo(a)anthracene ND ug/L 09/06/22 21:42 56-55-309/06/22 12:008.3 1
Benzo(a)pyrene ND ug/L 09/06/22 21:42 50-32-809/06/22 12:008.3 1
Benzo(b)fluoranthene ND ug/L 09/06/22 21:42 205-99-209/06/22 12:008.3 1
Benzo(g,h,i)perylene ND ug/L 09/06/22 21:42 191-24-209/06/22 12:008.3 1
Benzo(k)fluoranthene ND ug/L 09/06/22 21:42 207-08-909/06/22 12:008.3 1
Benzoic Acid ND ug/L 09/06/22 21:42 65-85-009/06/22 12:0041.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Sample:TW-2 Lab ID:92623480007 Collected:08/31/22 10:30 Received:09/01/22 10:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Benzyl alcohol ND ug/L 09/06/22 21:42 100-51-609/06/22 12:0016.7 1
4-Bromophenylphenyl ether ND ug/L 09/06/22 21:42 101-55-309/06/22 12:008.3 1
Butylbenzylphthalate ND ug/L 09/06/22 21:42 85-68-709/06/22 12:008.3 1
4-Chloro-3-methylphenol ND ug/L 09/06/22 21:42 59-50-709/06/22 12:008.3 1
4-Chloroaniline ND ug/L 09/06/22 21:42 106-47-809/06/22 12:0016.7 1
bis(2-Chloroethoxy)methane ND ug/L 09/06/22 21:42 111-91-109/06/22 12:008.3 1
bis(2-Chloroethyl) ether ND ug/L 09/06/22 21:42 111-44-409/06/22 12:008.3 1
2-Chloronaphthalene ND ug/L 09/06/22 21:42 91-58-709/06/22 12:008.3 1
2-Chlorophenol ND ug/L 09/06/22 21:42 95-57-809/06/22 12:008.3 1
4-Chlorophenylphenyl ether ND ug/L 09/06/22 21:42 7005-72-309/06/22 12:008.3 1
Chrysene ND ug/L 09/06/22 21:42 218-01-909/06/22 12:008.3 1
Dibenz(a,h)anthracene ND ug/L 09/06/22 21:42 53-70-309/06/22 12:008.3 1
Dibenzofuran ND ug/L 09/06/22 21:42 132-64-909/06/22 12:008.3 1
1,2-Dichlorobenzene ND ug/L 09/06/22 21:42 95-50-109/06/22 12:008.3 1
1,3-Dichlorobenzene ND ug/L 09/06/22 21:42 541-73-109/06/22 12:008.3 1
1,4-Dichlorobenzene ND ug/L 09/06/22 21:42 106-46-709/06/22 12:008.3 1
3,3'-Dichlorobenzidine ND ug/L 09/06/22 21:42 91-94-109/06/22 12:0016.7 1
2,4-Dichlorophenol ND ug/L 09/06/22 21:42 120-83-209/06/22 12:008.3 1
Diethylphthalate ND ug/L 09/06/22 21:42 84-66-209/06/22 12:008.3 1
2,4-Dimethylphenol ND ug/L 09/06/22 21:42 105-67-909/06/22 12:008.3 1
Dimethylphthalate ND ug/L 09/06/22 21:42 131-11-309/06/22 12:008.3 1
Di-n-butylphthalate ND ug/L 09/06/22 21:42 84-74-209/06/22 12:008.3 1
4,6-Dinitro-2-methylphenol ND ug/L 09/06/22 21:42 534-52-109/06/22 12:0016.7 1
2,4-Dinitrophenol ND ug/L 09/06/22 21:42 51-28-509/06/22 12:0041.7 1
2,4-Dinitrotoluene ND ug/L 09/06/22 21:42 121-14-209/06/22 12:008.3 1
2,6-Dinitrotoluene ND ug/L 09/06/22 21:42 606-20-209/06/22 12:008.3 1
Di-n-octylphthalate ND ug/L 09/06/22 21:42 117-84-009/06/22 12:008.3 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/06/22 21:42 117-81-709/06/22 12:005.0 1
Fluoranthene ND ug/L 09/06/22 21:42 206-44-009/06/22 12:008.3 1
Fluorene ND ug/L 09/06/22 21:42 86-73-709/06/22 12:008.3 1
Hexachloro-1,3-butadiene ND ug/L 09/06/22 21:42 87-68-309/06/22 12:008.3 1
Hexachlorobenzene ND ug/L 09/06/22 21:42 118-74-109/06/22 12:008.3 1
Hexachlorocyclopentadiene ND ug/L 09/06/22 21:42 77-47-409/06/22 12:008.3 1
Hexachloroethane ND ug/L 09/06/22 21:42 67-72-109/06/22 12:008.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/06/22 21:42 193-39-509/06/22 12:008.3 1
Isophorone ND ug/L 09/06/22 21:42 78-59-109/06/22 12:008.3 1
1-Methylnaphthalene ND ug/L 09/06/22 21:42 90-12-009/06/22 12:008.3 1
2-Methylnaphthalene ND ug/L 09/06/22 21:42 91-57-609/06/22 12:008.3 1
2-Methylphenol(o-Cresol)ND ug/L 09/06/22 21:42 95-48-709/06/22 12:008.3 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/06/22 21:42 15831-10-409/06/22 12:008.3 1
Naphthalene ND ug/L 09/06/22 21:42 91-20-309/06/22 12:008.3 1
2-Nitroaniline ND ug/L 09/06/22 21:42 88-74-409/06/22 12:0016.7 1
3-Nitroaniline ND ug/L 09/06/22 21:42 99-09-209/06/22 12:0016.7 1
4-Nitroaniline ND ug/L 09/06/22 21:42 100-01-609/06/22 12:0016.7 1
Nitrobenzene ND ug/L 09/06/22 21:42 98-95-309/06/22 12:008.3 1
2-Nitrophenol ND ug/L 09/06/22 21:42 88-75-509/06/22 12:008.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Sample:TW-2 Lab ID:92623480007 Collected:08/31/22 10:30 Received:09/01/22 10:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
4-Nitrophenol ND ug/L 09/06/22 21:42 100-02-709/06/22 12:0041.7 1
N-Nitrosodimethylamine ND ug/L 09/06/22 21:42 62-75-909/06/22 12:008.3 1
N-Nitroso-di-n-propylamine ND ug/L 09/06/22 21:42 621-64-709/06/22 12:008.3 1
N-Nitrosodiphenylamine ND ug/L 09/06/22 21:42 86-30-609/06/22 12:008.3 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/06/22 21:42 108-60-109/06/22 12:008.3 1
Pentachlorophenol ND ug/L 09/06/22 21:42 87-86-509/06/22 12:0016.7 1
Phenanthrene ND ug/L 09/06/22 21:42 85-01-809/06/22 12:008.3 1
Phenol ND ug/L 09/06/22 21:42 108-95-209/06/22 12:008.3 1
Pyrene ND ug/L 09/06/22 21:42 129-00-009/06/22 12:008.3 1
1,2,4-Trichlorobenzene ND ug/L 09/06/22 21:42 120-82-109/06/22 12:008.3 1
2,4,5-Trichlorophenol ND ug/L 09/06/22 21:42 95-95-409/06/22 12:008.3 1
2,4,6-Trichlorophenol ND ug/L 09/06/22 21:42 88-06-209/06/22 12:008.3 1
Surrogates
Nitrobenzene-d5 (S)68 %09/06/22 21:42 4165-60-009/06/22 12:0010-144 1
2-Fluorobiphenyl (S)54 %09/06/22 21:42 321-60-809/06/22 12:0010-130 1
Terphenyl-d14 (S)128 %09/06/22 21:42 1718-51-009/06/22 12:0034-163 1
Phenol-d6 (S)54 %09/06/22 21:42 13127-88-309/06/22 12:0010-130 1
2-Fluorophenol (S)55 %09/06/22 21:42 367-12-409/06/22 12:0010-130 1
2,4,6-Tribromophenol (S)104 %09/06/22 21:42 118-79-609/06/22 12:0010-144 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 09/08/22 19:42 67-64-125.0 1
Benzene ND ug/L 09/08/22 19:42 71-43-21.0 1
Bromobenzene ND ug/L 09/08/22 19:42 108-86-11.0 1
Bromochloromethane ND ug/L 09/08/22 19:42 74-97-51.0 1
Bromodichloromethane ND ug/L 09/08/22 19:42 75-27-41.0 1
Bromoform ND ug/L 09/08/22 19:42 75-25-21.0 1
Bromomethane ND ug/L 09/08/22 19:42 74-83-92.0 1
2-Butanone (MEK)ND ug/L 09/08/22 19:42 78-93-35.0 1
Carbon tetrachloride ND ug/L 09/08/22 19:42 56-23-51.0 1
Chlorobenzene ND ug/L 09/08/22 19:42 108-90-71.0 1
Chloroethane ND ug/L 09/08/22 19:42 75-00-31.0 1
Chloroform ND ug/L 09/08/22 19:42 67-66-31.0 1
Chloromethane ND ug/L 09/08/22 19:42 74-87-31.0 1
2-Chlorotoluene ND ug/L 09/08/22 19:42 95-49-81.0 1
4-Chlorotoluene ND ug/L 09/08/22 19:42 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 09/08/22 19:42 96-12-82.0 1
Dibromochloromethane ND ug/L 09/08/22 19:42 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 09/08/22 19:42 106-93-41.0 1
Dibromomethane ND ug/L 09/08/22 19:42 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 09/08/22 19:42 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 09/08/22 19:42 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 09/08/22 19:42 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 09/08/22 19:42 75-71-81.0 1
1,1-Dichloroethane ND ug/L 09/08/22 19:42 75-34-31.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Sample:TW-2 Lab ID:92623480007 Collected:08/31/22 10:30 Received:09/01/22 10:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,2-Dichloroethane ND ug/L 09/08/22 19:42 107-06-21.0 1
1,1-Dichloroethene ND ug/L 09/08/22 19:42 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 09/08/22 19:42 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 09/08/22 19:42 156-60-51.0 1
1,2-Dichloropropane ND ug/L 09/08/22 19:42 78-87-51.0 1
1,3-Dichloropropane ND ug/L 09/08/22 19:42 142-28-91.0 1
2,2-Dichloropropane ND ug/L 09/08/22 19:42 594-20-71.0 1
1,1-Dichloropropene ND ug/L 09/08/22 19:42 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 09/08/22 19:42 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 09/08/22 19:42 10061-02-61.0 1
Diisopropyl ether ND ug/L 09/08/22 19:42 108-20-31.0 1
Ethylbenzene ND ug/L 09/08/22 19:42 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 09/08/22 19:42 87-68-32.0 1
2-Hexanone ND ug/L 09/08/22 19:42 591-78-65.0 1
p-Isopropyltoluene ND ug/L 09/08/22 19:42 99-87-61.0 1
Methylene Chloride ND ug/L 09/08/22 19:42 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/08/22 19:42 108-10-15.0 1
Methyl-tert-butyl ether 197 ug/L 09/08/22 19:42 1634-04-41.0 1
Naphthalene ND ug/L 09/08/22 19:42 91-20-31.0 1
Styrene ND ug/L 09/08/22 19:42 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 09/08/22 19:42 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 09/08/22 19:42 79-34-51.0 1
Tetrachloroethene ND ug/L 09/08/22 19:42 127-18-41.0 1
Toluene ND ug/L 09/08/22 19:42 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 09/08/22 19:42 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 09/08/22 19:42 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 09/08/22 19:42 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 09/08/22 19:42 79-00-51.0 1
Trichloroethene ND ug/L 09/08/22 19:42 79-01-61.0 1
Trichlorofluoromethane ND ug/L 09/08/22 19:42 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 09/08/22 19:42 96-18-41.0 1
Vinyl acetate ND ug/L 09/08/22 19:42 108-05-4 IK2.0 1
Vinyl chloride ND ug/L 09/08/22 19:42 75-01-41.0 1
Xylene (Total)ND ug/L 09/08/22 19:42 1330-20-71.0 1
m&p-Xylene ND ug/L 09/08/22 19:42 179601-23-12.0 1
o-Xylene ND ug/L 09/08/22 19:42 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)103 %09/08/22 19:42 460-00-470-130 1
1,2-Dichloroethane-d4 (S)95 %09/08/22 19:42 17060-07-070-130 1
Toluene-d8 (S)101 %09/08/22 19:42 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Sample:TW-3 Lab ID:92623480008 Collected:08/31/22 11:10 Received:09/01/22 10:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 09/07/22 13:27 83-32-909/06/22 16:001001
Acenaphthylene ND ug/L 09/07/22 13:27 208-96-809/06/22 16:001001
Aniline ND ug/L 09/07/22 13:27 62-53-309/06/22 16:001001
Anthracene ND ug/L 09/07/22 13:27 120-12-709/06/22 16:001001
Benzo(a)anthracene ND ug/L 09/07/22 13:27 56-55-309/06/22 16:001001
Benzo(a)pyrene ND ug/L 09/07/22 13:27 50-32-809/06/22 16:001001
Benzo(b)fluoranthene ND ug/L 09/07/22 13:27 205-99-209/06/22 16:001001
Benzo(g,h,i)perylene ND ug/L 09/07/22 13:27 191-24-209/06/22 16:001001
Benzo(k)fluoranthene ND ug/L 09/07/22 13:27 207-08-909/06/22 16:001001
Benzoic Acid ND ug/L 09/07/22 13:27 65-85-009/06/22 16:005001
Benzyl alcohol ND ug/L 09/07/22 13:27 100-51-609/06/22 16:002001
4-Bromophenylphenyl ether ND ug/L 09/07/22 13:27 101-55-309/06/22 16:001001
Butylbenzylphthalate ND ug/L 09/07/22 13:27 85-68-709/06/22 16:001001
4-Chloro-3-methylphenol ND ug/L 09/07/22 13:27 59-50-709/06/22 16:001001
4-Chloroaniline ND ug/L 09/07/22 13:27 106-47-809/06/22 16:002001
bis(2-Chloroethoxy)methane ND ug/L 09/07/22 13:27 111-91-109/06/22 16:001001
bis(2-Chloroethyl) ether ND ug/L 09/07/22 13:27 111-44-409/06/22 16:001001
2-Chloronaphthalene ND ug/L 09/07/22 13:27 91-58-709/06/22 16:001001
2-Chlorophenol ND ug/L 09/07/22 13:27 95-57-809/06/22 16:001001
4-Chlorophenylphenyl ether ND ug/L 09/07/22 13:27 7005-72-309/06/22 16:001001
Chrysene ND ug/L 09/07/22 13:27 218-01-909/06/22 16:001001
Dibenz(a,h)anthracene ND ug/L 09/07/22 13:27 53-70-309/06/22 16:001001
Dibenzofuran ND ug/L 09/07/22 13:27 132-64-909/06/22 16:001001
1,2-Dichlorobenzene ND ug/L 09/07/22 13:27 95-50-109/06/22 16:001001
1,3-Dichlorobenzene ND ug/L 09/07/22 13:27 541-73-109/06/22 16:001001
1,4-Dichlorobenzene ND ug/L 09/07/22 13:27 106-46-709/06/22 16:001001
3,3'-Dichlorobenzidine ND ug/L 09/07/22 13:27 91-94-109/06/22 16:002001
2,4-Dichlorophenol ND ug/L 09/07/22 13:27 120-83-209/06/22 16:001001
Diethylphthalate ND ug/L 09/07/22 13:27 84-66-209/06/22 16:001001
2,4-Dimethylphenol ND ug/L 09/07/22 13:27 105-67-909/06/22 16:001001
Dimethylphthalate ND ug/L 09/07/22 13:27 131-11-309/06/22 16:001001
Di-n-butylphthalate ND ug/L 09/07/22 13:27 84-74-209/06/22 16:001001
4,6-Dinitro-2-methylphenol ND ug/L 09/07/22 13:27 534-52-109/06/22 16:002001
2,4-Dinitrophenol ND ug/L 09/07/22 13:27 51-28-509/06/22 16:005001
2,4-Dinitrotoluene ND ug/L 09/07/22 13:27 121-14-209/06/22 16:001001
2,6-Dinitrotoluene ND ug/L 09/07/22 13:27 606-20-209/06/22 16:001001
Di-n-octylphthalate ND ug/L 09/07/22 13:27 117-84-009/06/22 16:001001
bis(2-Ethylhexyl)phthalate ND ug/L 09/07/22 13:27 117-81-709/06/22 16:0060.0 1
Fluoranthene ND ug/L 09/07/22 13:27 206-44-009/06/22 16:001001
Fluorene ND ug/L 09/07/22 13:27 86-73-709/06/22 16:001001
Hexachloro-1,3-butadiene ND ug/L 09/07/22 13:27 87-68-309/06/22 16:001001
Hexachlorobenzene ND ug/L 09/07/22 13:27 118-74-109/06/22 16:001001
Hexachlorocyclopentadiene ND ug/L 09/07/22 13:27 77-47-409/06/22 16:001001
Hexachloroethane ND ug/L 09/07/22 13:27 67-72-109/06/22 16:001001
Indeno(1,2,3-cd)pyrene ND ug/L 09/07/22 13:27 193-39-509/06/22 16:001001
Isophorone ND ug/L 09/07/22 13:27 78-59-109/06/22 16:001001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Sample:TW-3 Lab ID:92623480008 Collected:08/31/22 11:10 Received:09/01/22 10:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
1-Methylnaphthalene ND ug/L 09/07/22 13:27 90-12-009/06/22 16:001001
2-Methylnaphthalene ND ug/L 09/07/22 13:27 91-57-609/06/22 16:001001
2-Methylphenol(o-Cresol)ND ug/L 09/07/22 13:27 95-48-709/06/22 16:001001
3&4-Methylphenol(m&p Cresol)ND ug/L 09/07/22 13:27 15831-10-409/06/22 16:001001
Naphthalene ND ug/L 09/07/22 13:27 91-20-309/06/22 16:001001
2-Nitroaniline ND ug/L 09/07/22 13:27 88-74-409/06/22 16:002001
3-Nitroaniline ND ug/L 09/07/22 13:27 99-09-209/06/22 16:002001
4-Nitroaniline ND ug/L 09/07/22 13:27 100-01-609/06/22 16:002001
Nitrobenzene ND ug/L 09/07/22 13:27 98-95-309/06/22 16:001001
2-Nitrophenol ND ug/L 09/07/22 13:27 88-75-509/06/22 16:001001
4-Nitrophenol ND ug/L 09/07/22 13:27 100-02-709/06/22 16:005001
N-Nitrosodimethylamine ND ug/L 09/07/22 13:27 62-75-909/06/22 16:001001
N-Nitroso-di-n-propylamine ND ug/L 09/07/22 13:27 621-64-709/06/22 16:001001
N-Nitrosodiphenylamine ND ug/L 09/07/22 13:27 86-30-609/06/22 16:001001
2,2'-Oxybis(1-chloropropane)ND ug/L 09/07/22 13:27 108-60-109/06/22 16:001001
Pentachlorophenol ND ug/L 09/07/22 13:27 87-86-509/06/22 16:002001
Phenanthrene ND ug/L 09/07/22 13:27 85-01-809/06/22 16:001001
Phenol ND ug/L 09/07/22 13:27 108-95-209/06/22 16:001001
Pyrene ND ug/L 09/07/22 13:27 129-00-009/06/22 16:001001
1,2,4-Trichlorobenzene ND ug/L 09/07/22 13:27 120-82-109/06/22 16:001001
2,4,5-Trichlorophenol ND ug/L 09/07/22 13:27 95-95-409/06/22 16:001001
2,4,6-Trichlorophenol ND ug/L 09/07/22 13:27 88-06-209/06/22 16:001001
Surrogates
Nitrobenzene-d5 (S)61 %09/07/22 13:27 4165-60-009/06/22 16:0010-144 1
2-Fluorobiphenyl (S)45 %09/07/22 13:27 321-60-809/06/22 16:0010-130 1
Terphenyl-d14 (S)91 %09/07/22 13:27 1718-51-009/06/22 16:0034-163 1
Phenol-d6 (S)37 %09/07/22 13:27 13127-88-309/06/22 16:0010-130 1
2-Fluorophenol (S)51 %09/07/22 13:27 367-12-409/06/22 16:0010-130 1
2,4,6-Tribromophenol (S)71 %09/07/22 13:27 118-79-609/06/22 16:0010-144 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 09/08/22 20:00 67-64-125.0 1
Benzene ND ug/L 09/08/22 20:00 71-43-21.0 1
Bromobenzene ND ug/L 09/08/22 20:00 108-86-11.0 1
Bromochloromethane ND ug/L 09/08/22 20:00 74-97-51.0 1
Bromodichloromethane ND ug/L 09/08/22 20:00 75-27-41.0 1
Bromoform ND ug/L 09/08/22 20:00 75-25-21.0 1
Bromomethane ND ug/L 09/08/22 20:00 74-83-92.0 1
2-Butanone (MEK)ND ug/L 09/08/22 20:00 78-93-35.0 1
Carbon tetrachloride ND ug/L 09/08/22 20:00 56-23-51.0 1
Chlorobenzene ND ug/L 09/08/22 20:00 108-90-71.0 1
Chloroethane ND ug/L 09/08/22 20:00 75-00-31.0 1
Chloroform ND ug/L 09/08/22 20:00 67-66-31.0 1
Chloromethane ND ug/L 09/08/22 20:00 74-87-31.0 1
2-Chlorotoluene ND ug/L 09/08/22 20:00 95-49-81.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Sample:TW-3 Lab ID:92623480008 Collected:08/31/22 11:10 Received:09/01/22 10:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
4-Chlorotoluene ND ug/L 09/08/22 20:00 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 09/08/22 20:00 96-12-82.0 1
Dibromochloromethane ND ug/L 09/08/22 20:00 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 09/08/22 20:00 106-93-41.0 1
Dibromomethane ND ug/L 09/08/22 20:00 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 09/08/22 20:00 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 09/08/22 20:00 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 09/08/22 20:00 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 09/08/22 20:00 75-71-81.0 1
1,1-Dichloroethane ND ug/L 09/08/22 20:00 75-34-31.0 1
1,2-Dichloroethane ND ug/L 09/08/22 20:00 107-06-21.0 1
1,1-Dichloroethene ND ug/L 09/08/22 20:00 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 09/08/22 20:00 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 09/08/22 20:00 156-60-51.0 1
1,2-Dichloropropane ND ug/L 09/08/22 20:00 78-87-51.0 1
1,3-Dichloropropane ND ug/L 09/08/22 20:00 142-28-91.0 1
2,2-Dichloropropane ND ug/L 09/08/22 20:00 594-20-71.0 1
1,1-Dichloropropene ND ug/L 09/08/22 20:00 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 09/08/22 20:00 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 09/08/22 20:00 10061-02-61.0 1
Diisopropyl ether ND ug/L 09/08/22 20:00 108-20-31.0 1
Ethylbenzene ND ug/L 09/08/22 20:00 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 09/08/22 20:00 87-68-32.0 1
2-Hexanone ND ug/L 09/08/22 20:00 591-78-65.0 1
p-Isopropyltoluene ND ug/L 09/08/22 20:00 99-87-61.0 1
Methylene Chloride ND ug/L 09/08/22 20:00 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/08/22 20:00 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 09/08/22 20:00 1634-04-41.0 1
Naphthalene ND ug/L 09/08/22 20:00 91-20-31.0 1
Styrene ND ug/L 09/08/22 20:00 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 09/08/22 20:00 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 09/08/22 20:00 79-34-51.0 1
Tetrachloroethene ND ug/L 09/08/22 20:00 127-18-41.0 1
Toluene ND ug/L 09/08/22 20:00 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 09/08/22 20:00 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 09/08/22 20:00 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 09/08/22 20:00 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 09/08/22 20:00 79-00-51.0 1
Trichloroethene ND ug/L 09/08/22 20:00 79-01-61.0 1
Trichlorofluoromethane ND ug/L 09/08/22 20:00 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 09/08/22 20:00 96-18-41.0 1
Vinyl acetate ND ug/L 09/08/22 20:00 108-05-4 IK2.0 1
Vinyl chloride ND ug/L 09/08/22 20:00 75-01-41.0 1
Xylene (Total)ND ug/L 09/08/22 20:00 1330-20-71.0 1
m&p-Xylene ND ug/L 09/08/22 20:00 179601-23-12.0 1
o-Xylene ND ug/L 09/08/22 20:00 95-47-61.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 71
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Sample:TW-3 Lab ID:92623480008 Collected:08/31/22 11:10 Received:09/01/22 10:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Surrogates
4-Bromofluorobenzene (S)104 %09/08/22 20:00 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %09/08/22 20:00 17060-07-070-130 1
Toluene-d8 (S)101 %09/08/22 20:00 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
721251
MADEP VPH
MADEP VPH
VPH NC Soil
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92623480005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3757971
Associated Lab Samples:92623480005
Matrix:Solid
Analyzed
Aliphatic (C05-C08)mg/kg ND 2.5 N209/02/22 16:41
Aromatic (C09-C10)mg/kg ND 2.5 N209/02/22 16:41
4-Bromofluorobenzene (FID) (S)%108 70-130 09/02/22 16:41
4-Bromofluorobenzene (PID) (S)%96 70-130 09/02/22 16:41
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3757972LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
3757973
Aliphatic (C05-C08)mg/kg 13.9 N2159370-1309514.2 2 25
Aromatic (C09-C10)mg/kg 4.8 N259770-130944.7 2 25
4-Bromofluorobenzene (FID) (S)%105 70-130106
4-Bromofluorobenzene (PID) (S)%94 70-13096
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
721351
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92623480001, 92623480002, 92623480003, 92623480004, 92623480005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3758599
Associated Lab Samples:92623480001, 92623480002, 92623480003, 92623480004, 92623480005
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane mg/kg ND 0.0050 09/02/22 19:44
1,1,1-Trichloroethane mg/kg ND 0.0050 09/02/22 19:44
1,1,2,2-Tetrachloroethane mg/kg ND 0.0050 09/02/22 19:44
1,1,2-Trichloroethane mg/kg ND 0.0050 09/02/22 19:44
1,1-Dichloroethane mg/kg ND 0.0050 09/02/22 19:44
1,1-Dichloroethene mg/kg ND 0.0050 09/02/22 19:44
1,1-Dichloropropene mg/kg ND 0.0050 09/02/22 19:44
1,2,3-Trichlorobenzene mg/kg ND 0.0050 09/02/22 19:44
1,2,3-Trichloropropane mg/kg ND 0.0050 09/02/22 19:44
1,2,4-Trichlorobenzene mg/kg ND 0.0050 09/02/22 19:44
1,2,4-Trimethylbenzene mg/kg ND 0.0050 09/02/22 19:44
1,2-Dibromo-3-chloropropane mg/kg ND 0.0050 09/02/22 19:44
1,2-Dibromoethane (EDB)mg/kg ND 0.0050 09/02/22 19:44
1,2-Dichlorobenzene mg/kg ND 0.0050 09/02/22 19:44
1,2-Dichloroethane mg/kg ND 0.0050 09/02/22 19:44
1,2-Dichloropropane mg/kg ND 0.0050 09/02/22 19:44
1,3,5-Trimethylbenzene mg/kg ND 0.0050 09/02/22 19:44
1,3-Dichlorobenzene mg/kg ND 0.0050 09/02/22 19:44
1,3-Dichloropropane mg/kg ND 0.0050 09/02/22 19:44
1,4-Dichlorobenzene mg/kg ND 0.0050 09/02/22 19:44
2,2-Dichloropropane mg/kg ND 0.0050 v209/02/22 19:44
2-Butanone (MEK)mg/kg ND 0.10 v209/02/22 19:44
2-Chlorotoluene mg/kg ND 0.0050 09/02/22 19:44
2-Hexanone mg/kg ND 0.050 09/02/22 19:44
4-Chlorotoluene mg/kg ND 0.0050 09/02/22 19:44
4-Methyl-2-pentanone (MIBK)mg/kg ND 0.050 09/02/22 19:44
Acetone mg/kg ND 0.10 v209/02/22 19:44
Benzene mg/kg ND 0.0050 09/02/22 19:44
Bromobenzene mg/kg ND 0.0050 09/02/22 19:44
Bromochloromethane mg/kg ND 0.0050 09/02/22 19:44
Bromodichloromethane mg/kg ND 0.0050 09/02/22 19:44
Bromoform mg/kg ND 0.0050 09/02/22 19:44
Bromomethane mg/kg ND 0.010 09/02/22 19:44
Carbon tetrachloride mg/kg ND 0.0050 09/02/22 19:44
Chlorobenzene mg/kg ND 0.0050 09/02/22 19:44
Chloroethane mg/kg ND 0.010 09/02/22 19:44
Chloroform mg/kg ND 0.0050 09/02/22 19:44
Chloromethane mg/kg ND 0.010 09/02/22 19:44
cis-1,2-Dichloroethene mg/kg ND 0.0050 09/02/22 19:44
cis-1,3-Dichloropropene mg/kg ND 0.0050 09/02/22 19:44
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3758599
Associated Lab Samples:92623480001, 92623480002, 92623480003, 92623480004, 92623480005
Matrix:Solid
Analyzed
Dibromochloromethane mg/kg ND 0.0050 09/02/22 19:44
Dibromomethane mg/kg ND 0.0050 09/02/22 19:44
Dichlorodifluoromethane mg/kg ND 0.010 09/02/22 19:44
Diisopropyl ether mg/kg ND 0.0050 v209/02/22 19:44
Ethylbenzene mg/kg ND 0.0050 09/02/22 19:44
Hexachloro-1,3-butadiene mg/kg ND 0.010 IK09/02/22 19:44
Isopropylbenzene (Cumene)mg/kg ND 0.0050 09/02/22 19:44
m&p-Xylene mg/kg ND 0.010 09/02/22 19:44
Methyl-tert-butyl ether mg/kg ND 0.0050 09/02/22 19:44
Methylene Chloride mg/kg ND 0.020 v209/02/22 19:44
n-Butylbenzene mg/kg ND 0.0050 09/02/22 19:44
n-Propylbenzene mg/kg ND 0.0050 09/02/22 19:44
Naphthalene mg/kg ND 0.0050 09/02/22 19:44
o-Xylene mg/kg ND 0.0050 09/02/22 19:44
p-Isopropyltoluene mg/kg ND 0.0050 09/02/22 19:44
sec-Butylbenzene mg/kg ND 0.0050 09/02/22 19:44
Styrene mg/kg ND 0.0050 09/02/22 19:44
tert-Butylbenzene mg/kg ND 0.0050 09/02/22 19:44
Tetrachloroethene mg/kg ND 0.0050 IK09/02/22 19:44
Toluene mg/kg ND 0.0050 09/02/22 19:44
trans-1,2-Dichloroethene mg/kg ND 0.0050 09/02/22 19:44
trans-1,3-Dichloropropene mg/kg ND 0.0050 09/02/22 19:44
Trichloroethene mg/kg ND 0.0050 09/02/22 19:44
Trichlorofluoromethane mg/kg ND 0.0050 09/02/22 19:44
Vinyl acetate mg/kg ND 0.050 09/02/22 19:44
Vinyl chloride mg/kg ND 0.010 09/02/22 19:44
Xylene (Total)mg/kg ND 0.010 09/02/22 19:44
1,2-Dichloroethane-d4 (S)%85 70-130 09/02/22 19:44
4-Bromofluorobenzene (S)%96 70-130 09/02/22 19:44
Toluene-d8 (S)%96 70-130 09/02/22 19:44
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3758600LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane mg/kg 1.21.2 99 70-130
1,1,1-Trichloroethane mg/kg 1.11.2 89 70-130
1,1,2,2-Tetrachloroethane mg/kg 1.11.2 89 70-130
1,1,2-Trichloroethane mg/kg 1.21.2 93 70-130
1,1-Dichloroethane mg/kg 1.01.2 80 70-130
1,1-Dichloroethene mg/kg 1.11.2 86 70-130
1,1-Dichloropropene mg/kg 1.11.2 89 70-130
1,2,3-Trichlorobenzene mg/kg 1.31.2 101 70-130
1,2,3-Trichloropropane mg/kg 1.01.2 83 70-130
1,2,4-Trichlorobenzene mg/kg 1.21.2 99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3758600LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene mg/kg 1.21.2 93 70-130
1,2-Dibromo-3-chloropropane mg/kg 1.31.2 102 67-130
1,2-Dibromoethane (EDB)mg/kg 1.21.2 93 70-130
1,2-Dichlorobenzene mg/kg 1.21.2 96 70-130
1,2-Dichloroethane mg/kg 1.01.2 83 70-130
1,2-Dichloropropane mg/kg 1.11.2 87 70-130
1,3,5-Trimethylbenzene mg/kg 1.21.2 97 70-130
1,3-Dichlorobenzene mg/kg 1.21.2 95 70-130
1,3-Dichloropropane mg/kg 1.11.2 86 70-130
1,4-Dichlorobenzene mg/kg 1.21.2 93 70-130
2,2-Dichloropropane mg/kg 0.86 v31.2 69 67-130
2-Butanone (MEK)mg/kg 1.8 v32.5 74 66-130
2-Chlorotoluene mg/kg 1.11.2 89 70-130
2-Hexanone mg/kg 2.22.5 87 70-130
4-Chlorotoluene mg/kg 1.11.2 91 70-130
4-Methyl-2-pentanone (MIBK)mg/kg 2.22.5 88 70-130
Acetone mg/kg 1.9 v32.5 76 67-130
Benzene mg/kg 1.01.2 83 70-130
Bromobenzene mg/kg 1.21.2 95 70-130
Bromochloromethane mg/kg 1.21.2 95 70-130
Bromodichloromethane mg/kg 1.11.2 90 70-130
Bromoform mg/kg 1.31.2 102 70-130
Bromomethane mg/kg 1.21.2 94 53-175
Carbon tetrachloride mg/kg 1.21.2 99 70-130
Chlorobenzene mg/kg 1.21.2 92 70-130
Chloroethane mg/kg 1.11.2 90 70-135
Chloroform mg/kg 1.11.2 85 70-130
Chloromethane mg/kg 1.11.2 85 64-130
cis-1,2-Dichloroethene mg/kg 1.01.2 82 70-130
cis-1,3-Dichloropropene mg/kg 1.11.2 90 70-130
Dibromochloromethane mg/kg 1.21.2 97 70-130
Dibromomethane mg/kg 1.21.2 100 70-130
Dichlorodifluoromethane mg/kg 1.01.2 82 63-145
Diisopropyl ether mg/kg 0.99 v31.2 79 68-130
Ethylbenzene mg/kg 1.11.2 87 70-130
Hexachloro-1,3-butadiene mg/kg 1.2 IK1.2 93 70-130
Isopropylbenzene (Cumene)mg/kg 1.21.2 96 70-130
m&p-Xylene mg/kg 2.32.5 94 70-130
Methyl-tert-butyl ether mg/kg 1.01.2 84 70-130
Methylene Chloride mg/kg 0.81 L2,v31.2 64 67-130
n-Butylbenzene mg/kg 1.11.2 90 70-130
n-Propylbenzene mg/kg 1.11.2 90 70-130
Naphthalene mg/kg 1.31.2 100 70-130
o-Xylene mg/kg 1.21.2 94 70-130
p-Isopropyltoluene mg/kg 1.21.2 98 70-130
sec-Butylbenzene mg/kg 1.21.2 92 70-130
Styrene mg/kg 1.21.2 99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3758600LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene mg/kg 1.21.2 97 64-130
Tetrachloroethene mg/kg 1.2 IK1.2 95 70-130
Toluene mg/kg 1.11.2 90 70-130
trans-1,2-Dichloroethene mg/kg 1.01.2 82 70-130
trans-1,3-Dichloropropene mg/kg 1.11.2 91 70-130
Trichloroethene mg/kg 1.31.2 102 70-130
Trichlorofluoromethane mg/kg 1.11.2 85 70-130
Vinyl acetate mg/kg 2.12.5 86 70-134
Vinyl chloride mg/kg 1.11.2 86 68-130
Xylene (Total)mg/kg 3.53.8 94 70-130
1,2-Dichloroethane-d4 (S)%87 70-130
4-Bromofluorobenzene (S)%96 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3758601MATRIX SPIKE SAMPLE:
MSSpike
Result
92623480001
1,1,1,2-Tetrachloroethane mg/kg 1.00.81 127 58-140ND
1,1,1-Trichloroethane mg/kg 0.960.81 119 58-144ND
1,1,2,2-Tetrachloroethane mg/kg 0.860.81 106 52-139ND
1,1,2-Trichloroethane mg/kg 0.930.81 115 56-140ND
1,1-Dichloroethane mg/kg 0.810.81 100 58-145ND
1,1-Dichloroethene mg/kg 0.990.81 123 57-158ND
1,1-Dichloropropene mg/kg 0.950.81 118 58-151ND
1,2,3-Trichlorobenzene mg/kg 0.500.81 62 48-149ND
1,2,3-Trichloropropane mg/kg 0.820.81 101 54-132ND
1,2,4-Trichlorobenzene mg/kg 0.850.81 105 51-151ND
1,2,4-Trimethylbenzene mg/kg 0.960.81 119 38-170ND
1,2-Dibromo-3-chloropropane mg/kg 0.820.81 101 44-134ND
1,2-Dibromoethane (EDB)mg/kg 0.930.81 114 60-138ND
1,2-Dichlorobenzene mg/kg 1.00.81 127 59-147ND
1,2-Dichloroethane mg/kg 0.820.81 101 57-139ND
1,2-Dichloropropane mg/kg 0.880.81 109 62-145ND
1,3,5-Trimethylbenzene mg/kg 1.00.81 125 47-159ND
1,3-Dichlorobenzene mg/kg 1.00.81 126 58-144ND
1,3-Dichloropropane mg/kg 0.880.81 109 60-142ND
1,4-Dichlorobenzene mg/kg 0.980.81 121 57-143ND
2,2-Dichloropropane mg/kg 0.84 v30.81 103 37-144ND
2-Butanone (MEK)mg/kg 1.2 v31.6 72 28-146ND
2-Chlorotoluene mg/kg 0.900.81 111 55-158ND
2-Hexanone mg/kg 1.51.6 90 44-141ND
4-Chlorotoluene mg/kg 0.940.81 116 55-146ND
4-Methyl-2-pentanone (MIBK)mg/kg 1.41.6 88 50-138ND
Acetone mg/kg 1.3 v31.6 80 20-136ND
Benzene mg/kg 0.870.81 108 60-145ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3758601MATRIX SPIKE SAMPLE:
MSSpike
Result
92623480001
Bromobenzene mg/kg 0.950.81 117 59-145ND
Bromochloromethane mg/kg 0.910.81 112 57-143ND
Bromodichloromethane mg/kg 0.870.81 108 53-133ND
Bromoform mg/kg 0.950.81 117 48-133ND
Bromomethane mg/kg 1.00.81 127 10-167ND
Carbon tetrachloride mg/kg 1.10.81 138 57-147ND
Chlorobenzene mg/kg 1.00.81 123 61-144ND
Chloroethane mg/kg 0.850.81 105 10-153ND
Chloroform mg/kg 0.870.81 108 58-141ND
Chloromethane mg/kg 0.780.81 96 54-165ND
cis-1,2-Dichloroethene mg/kg 0.870.81 107 59-144ND
cis-1,3-Dichloropropene mg/kg 0.920.81 113 56-137ND
Dibromochloromethane mg/kg 0.950.81 118 53-139ND
Dibromomethane mg/kg 1.00.81 127 60-136ND
Dichlorodifluoromethane mg/kg 0.930.81 115 49-177ND
Diisopropyl ether mg/kg 0.77 v30.81 95 53-136ND
Ethylbenzene mg/kg 0.950.81 117 53-150ND
Hexachloro-1,3-butadiene mg/kg 1.1 IK0.81 138 42-186ND
Isopropylbenzene (Cumene)mg/kg 1.10.81 137 62-154ND
m&p-Xylene mg/kg 2.01.6 125 49-156ND
Methyl-tert-butyl ether mg/kg 0.840.81 103 54-133ND
Methylene Chloride mg/kg 0.53 v30.81 66 50-153ND
n-Butylbenzene mg/kg 1.00.81 128 44-174ND
n-Propylbenzene mg/kg 0.960.81 119 52-157ND
Naphthalene mg/kg 0.530.81 65 37-150ND
o-Xylene mg/kg 1.00.81 127 54-1500.0094
p-Isopropyltoluene mg/kg 1.10.81 138 50-164ND
sec-Butylbenzene mg/kg 1.00.81 129 58-161ND
Styrene mg/kg 1.10.81 131 60-148ND
tert-Butylbenzene mg/kg 1.00.81 128 44-151ND
Tetrachloroethene mg/kg 1.0 IK0.81 127 53-151ND
Toluene mg/kg 0.970.81 119 52-148ND
trans-1,2-Dichloroethene mg/kg 0.900.81 111 60-148ND
trans-1,3-Dichloropropene mg/kg 0.880.81 109 55-133ND
Trichloroethene mg/kg 1.10.81 141 60-148ND
Trichlorofluoromethane mg/kg 0.860.81 106 10-154ND
Vinyl acetate mg/kg 1.51.6 94 50-149ND
Vinyl chloride mg/kg 1.00.81 123 57-157ND
Xylene (Total)mg/kg 3.12.5 126 52-153ND
1,2-Dichloroethane-d4 (S)%83 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%97 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92623480002
3758602SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane mg/kg NDND
1,1,1-Trichloroethane mg/kg NDND
1,1,2,2-Tetrachloroethane mg/kg NDND
1,1,2-Trichloroethane mg/kg NDND
1,1-Dichloroethane mg/kg NDND
1,1-Dichloroethene mg/kg NDND
1,1-Dichloropropene mg/kg NDND
1,2,3-Trichlorobenzene mg/kg NDND
1,2,3-Trichloropropane mg/kg NDND
1,2,4-Trichlorobenzene mg/kg NDND
1,2,4-Trimethylbenzene mg/kg NDND
1,2-Dibromo-3-chloropropane mg/kg NDND
1,2-Dibromoethane (EDB)mg/kg NDND
1,2-Dichlorobenzene mg/kg NDND
1,2-Dichloroethane mg/kg NDND
1,2-Dichloropropane mg/kg NDND
1,3,5-Trimethylbenzene mg/kg NDND
1,3-Dichlorobenzene mg/kg NDND
1,3-Dichloropropane mg/kg NDND
1,4-Dichlorobenzene mg/kg NDND
2,2-Dichloropropane mg/kg ND v2ND
2-Butanone (MEK)mg/kg ND v2ND
2-Chlorotoluene mg/kg NDND
2-Hexanone mg/kg NDND
4-Chlorotoluene mg/kg NDND
4-Methyl-2-pentanone (MIBK)mg/kg NDND
Acetone mg/kg ND v2ND
Benzene mg/kg NDND
Bromobenzene mg/kg NDND
Bromochloromethane mg/kg NDND
Bromodichloromethane mg/kg NDND
Bromoform mg/kg NDND
Bromomethane mg/kg NDND
Carbon tetrachloride mg/kg NDND
Chlorobenzene mg/kg .0046JND
Chloroethane mg/kg NDND
Chloroform mg/kg NDND
Chloromethane mg/kg NDND
cis-1,2-Dichloroethene mg/kg NDND
cis-1,3-Dichloropropene mg/kg NDND
Dibromochloromethane mg/kg NDND
Dibromomethane mg/kg NDND
Dichlorodifluoromethane mg/kg NDND
Diisopropyl ether mg/kg ND v2ND
Ethylbenzene mg/kg NDND
Hexachloro-1,3-butadiene mg/kg ND IKND
Isopropylbenzene (Cumene)mg/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92623480002
3758602SAMPLE DUPLICATE:
m&p-Xylene mg/kg NDND
Methyl-tert-butyl ether mg/kg NDND
Methylene Chloride mg/kg ND v2ND
n-Butylbenzene mg/kg NDND
n-Propylbenzene mg/kg NDND
Naphthalene mg/kg NDND
o-Xylene mg/kg ND0.0079
p-Isopropyltoluene mg/kg NDND
sec-Butylbenzene mg/kg NDND
Styrene mg/kg NDND
tert-Butylbenzene mg/kg NDND
Tetrachloroethene mg/kg ND IKND
Toluene mg/kg NDND
trans-1,2-Dichloroethene mg/kg NDND
trans-1,3-Dichloropropene mg/kg NDND
Trichloroethene mg/kg NDND
Trichlorofluoromethane mg/kg NDND
Vinyl acetate mg/kg NDND
Vinyl chloride mg/kg NDND
Xylene (Total)mg/kg NDND
1,2-Dichloroethane-d4 (S)%8788
4-Bromofluorobenzene (S)%10098
Toluene-d8 (S)%9798
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
722095
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92623480006, 92623480007, 92623480008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3762325
Associated Lab Samples:92623480006, 92623480007, 92623480008
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 09/08/22 15:47
1,1,1-Trichloroethane ug/L ND 1.0 09/08/22 15:47
1,1,2,2-Tetrachloroethane ug/L ND 1.0 09/08/22 15:47
1,1,2-Trichloroethane ug/L ND 1.0 09/08/22 15:47
1,1-Dichloroethane ug/L ND 1.0 09/08/22 15:47
1,1-Dichloroethene ug/L ND 1.0 09/08/22 15:47
1,1-Dichloropropene ug/L ND 1.0 09/08/22 15:47
1,2,3-Trichlorobenzene ug/L ND 1.0 09/08/22 15:47
1,2,3-Trichloropropane ug/L ND 1.0 09/08/22 15:47
1,2,4-Trichlorobenzene ug/L ND 1.0 09/08/22 15:47
1,2-Dibromo-3-chloropropane ug/L ND 2.0 09/08/22 15:47
1,2-Dibromoethane (EDB)ug/L ND 1.0 09/08/22 15:47
1,2-Dichlorobenzene ug/L ND 1.0 09/08/22 15:47
1,2-Dichloroethane ug/L ND 1.0 09/08/22 15:47
1,2-Dichloropropane ug/L ND 1.0 09/08/22 15:47
1,3-Dichlorobenzene ug/L ND 1.0 09/08/22 15:47
1,3-Dichloropropane ug/L ND 1.0 09/08/22 15:47
1,4-Dichlorobenzene ug/L ND 1.0 09/08/22 15:47
2,2-Dichloropropane ug/L ND 1.0 09/08/22 15:47
2-Butanone (MEK)ug/L ND 5.0 09/08/22 15:47
2-Chlorotoluene ug/L ND 1.0 09/08/22 15:47
2-Hexanone ug/L ND 5.0 09/08/22 15:47
4-Chlorotoluene ug/L ND 1.0 09/08/22 15:47
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 09/08/22 15:47
Acetone ug/L ND 25.0 09/08/22 15:47
Benzene ug/L ND 1.0 09/08/22 15:47
Bromobenzene ug/L ND 1.0 09/08/22 15:47
Bromochloromethane ug/L ND 1.0 09/08/22 15:47
Bromodichloromethane ug/L ND 1.0 09/08/22 15:47
Bromoform ug/L ND 1.0 09/08/22 15:47
Bromomethane ug/L ND 2.0 09/08/22 15:47
Carbon tetrachloride ug/L ND 1.0 09/08/22 15:47
Chlorobenzene ug/L ND 1.0 09/08/22 15:47
Chloroethane ug/L ND 1.0 09/08/22 15:47
Chloroform ug/L ND 1.0 09/08/22 15:47
Chloromethane ug/L ND 1.0 09/08/22 15:47
cis-1,2-Dichloroethene ug/L ND 1.0 09/08/22 15:47
cis-1,3-Dichloropropene ug/L ND 1.0 09/08/22 15:47
Dibromochloromethane ug/L ND 1.0 09/08/22 15:47
Dibromomethane ug/L ND 1.0 09/08/22 15:47
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3762325
Associated Lab Samples:92623480006, 92623480007, 92623480008
Matrix:Water
Analyzed
Dichlorodifluoromethane ug/L ND 1.0 09/08/22 15:47
Diisopropyl ether ug/L ND 1.0 09/08/22 15:47
Ethylbenzene ug/L ND 1.0 09/08/22 15:47
Hexachloro-1,3-butadiene ug/L ND 2.0 09/08/22 15:47
m&p-Xylene ug/L ND 2.0 09/08/22 15:47
Methyl-tert-butyl ether ug/L ND 1.0 09/08/22 15:47
Methylene Chloride ug/L ND 5.0 09/08/22 15:47
Naphthalene ug/L ND 1.0 09/08/22 15:47
o-Xylene ug/L ND 1.0 09/08/22 15:47
p-Isopropyltoluene ug/L ND 1.0 09/08/22 15:47
Styrene ug/L ND 1.0 09/08/22 15:47
Tetrachloroethene ug/L ND 1.0 09/08/22 15:47
Toluene ug/L ND 1.0 09/08/22 15:47
trans-1,2-Dichloroethene ug/L ND 1.0 09/08/22 15:47
trans-1,3-Dichloropropene ug/L ND 1.0 09/08/22 15:47
Trichloroethene ug/L ND 1.0 09/08/22 15:47
Trichlorofluoromethane ug/L ND 1.0 09/08/22 15:47
Vinyl acetate ug/L ND 2.0 IK09/08/22 15:47
Vinyl chloride ug/L ND 1.0 09/08/22 15:47
Xylene (Total)ug/L ND 1.0 09/08/22 15:47
1,2-Dichloroethane-d4 (S)%104 70-130 09/08/22 15:47
4-Bromofluorobenzene (S)%103 70-130 09/08/22 15:47
Toluene-d8 (S)%101 70-130 09/08/22 15:47
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3762326LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 52.050 104 70-130
1,1,1-Trichloroethane ug/L 47.550 95 70-130
1,1,2,2-Tetrachloroethane ug/L 47.750 95 70-130
1,1,2-Trichloroethane ug/L 45.950 92 70-130
1,1-Dichloroethane ug/L 46.750 93 70-130
1,1-Dichloroethene ug/L 47.550 95 70-130
1,1-Dichloropropene ug/L 53.250 106 70-130
1,2,3-Trichlorobenzene ug/L 46.650 93 70-130
1,2,3-Trichloropropane ug/L 49.550 99 70-130
1,2,4-Trichlorobenzene ug/L 46.450 93 70-130
1,2-Dibromo-3-chloropropane ug/L 45.050 90 70-131
1,2-Dibromoethane (EDB)ug/L 48.950 98 70-130
1,2-Dichlorobenzene ug/L 47.850 96 70-130
1,2-Dichloroethane ug/L 48.350 97 70-130
1,2-Dichloropropane ug/L 53.550 107 70-130
1,3-Dichlorobenzene ug/L 46.950 94 70-130
1,3-Dichloropropane ug/L 51.550 103 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3762326LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dichlorobenzene ug/L 45.550 91 70-130
2,2-Dichloropropane ug/L 46.350 93 68-135
2-Butanone (MEK)ug/L 95.3100 95 70-134
2-Chlorotoluene ug/L 47.350 95 70-130
2-Hexanone ug/L 117100 117 70-131
4-Chlorotoluene ug/L 45.850 92 70-130
4-Methyl-2-pentanone (MIBK)ug/L 101100 101 70-130
Acetone ug/L 80.3100 80 70-133
Benzene ug/L 43.550 87 70-130
Bromobenzene ug/L 43.550 87 70-130
Bromochloromethane ug/L 44.350 89 70-130
Bromodichloromethane ug/L 49.750 99 70-130
Bromoform ug/L 51.050 102 70-130
Bromomethane ug/L 39.750 79 45-151
Carbon tetrachloride ug/L 46.650 93 70-130
Chlorobenzene ug/L 49.150 98 70-130
Chloroethane ug/L 48.650 97 39-152
Chloroform ug/L 45.750 91 70-130
Chloromethane ug/L 51.250 102 58-130
cis-1,2-Dichloroethene ug/L 47.250 94 70-130
cis-1,3-Dichloropropene ug/L 51.050 102 70-130
Dibromochloromethane ug/L 53.150 106 70-130
Dibromomethane ug/L 43.750 87 70-130
Dichlorodifluoromethane ug/L 52.650 105 54-133
Diisopropyl ether ug/L 49.250 98 70-130
Ethylbenzene ug/L 49.850 100 70-130
Hexachloro-1,3-butadiene ug/L 48.050 96 70-135
m&p-Xylene ug/L 98.6100 99 70-130
Methyl-tert-butyl ether ug/L 44.650 89 70-130
Methylene Chloride ug/L 45.450 91 66-130
Naphthalene ug/L 49.150 98 70-130
o-Xylene ug/L 48.950 98 70-130
p-Isopropyltoluene ug/L 49.650 99 70-130
Styrene ug/L 50.750 101 70-130
Tetrachloroethene ug/L 48.250 96 70-130
Toluene ug/L 44.850 90 70-130
trans-1,2-Dichloroethene ug/L 43.450 87 70-130
trans-1,3-Dichloropropene ug/L 49.050 98 70-130
Trichloroethene ug/L 50.050 100 70-130
Trichlorofluoromethane ug/L 45.250 90 62-130
Vinyl acetate ug/L 98.1 IK1009870-144
Vinyl chloride ug/L 52.950 106 62-130
Xylene (Total)ug/L 147150 98 70-130
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%105 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3762327MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92623960002
3762328
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 98 70-141103 420ND19.6 20.5
1,1,1-Trichloroethane ug/L 20 102 70-150111 920ND20.3 22.1
1,1,2,2-Tetrachloroethane ug/L 20 95 69-14297 220ND19.0 19.4
1,1,2-Trichloroethane ug/L 20 92 70-13899 820ND18.4 19.9
1,1-Dichloroethane ug/L 20 102 70-150113 1020ND20.5 22.5
1,1-Dichloroethene ug/L 20 110 70-156115 420ND22.1 22.9
1,1-Dichloropropene ug/L 20 112 70-150121 820ND22.4 24.3
1,2,3-Trichlorobenzene ug/L 20 103 70-148106 320ND20.7 21.3
1,2,3-Trichloropropane ug/L 20 88 70-14094 620ND17.7 18.8
1,2,4-Trichlorobenzene ug/L 20 100 70-146100 020ND19.9 20.0
1,2-Dibromo-3-chloropropane ug/L 20 82 68-14693 1320ND16.3 18.6
1,2-Dibromoethane (EDB)ug/L 20 90 70-13887 320ND18.0 17.3
1,2-Dichlorobenzene ug/L 20 101 70-141106 520ND20.1 21.1
1,2-Dichloroethane ug/L 20 97 69-143104 720ND19.5 20.9
1,2-Dichloropropane ug/L 20 112 68-156109 320ND22.3 21.7
1,3-Dichlorobenzene ug/L 20 102 70-143104 320ND20.3 20.9
1,3-Dichloropropane ug/L 20 97 70-138100 320ND19.4 20.0
1,4-Dichlorobenzene ug/L 20 96 70-14299 320ND19.3 19.8
2,2-Dichloropropane ug/L 20 102 52-170109 620ND20.5 21.7
2-Butanone (MEK)ug/L 40 91 60-157103 1240ND36.5 41.3
2-Chlorotoluene ug/L 20 98 70-14799 120ND19.6 19.7
2-Hexanone ug/L 40 104 68-146109 440ND41.6 43.5
4-Chlorotoluene ug/L 20 96 70-14299 320ND19.3 19.9
4-Methyl-2-pentanone (MIBK)ug/L 40 96 70-141103 740ND38.5 41.3
Acetone ug/L 40 83 58-157101 1940ND33.2 40.2
Benzene ug/L 20 94 70-14295 120ND18.8 19.0
Bromobenzene ug/L 20 96 70-143101 620ND19.1 20.3
Bromochloromethane ug/L 20 91 70-146100 920ND18.2 19.9
Bromodichloromethane ug/L 20 106 70-139107 120ND21.3 21.4
Bromoform ug/L 20 90 64-14097 820ND18.0 19.5
Bromomethane ug/L 20 99 28-192104 520ND19.8 20.8
Carbon tetrachloride ug/L 20 105 70-14899 620ND21.0 19.8
Chlorobenzene ug/L 20 103 70-141102 120ND20.6 20.4
Chloroethane ug/L 20 122 58-191125 320ND24.4 25.1
Chloroform ug/L 20 94 70-148104 10200.50J 19.2 21.3
Chloromethane ug/L 20 126 43-162125 020ND25.1 25.1
cis-1,2-Dichloroethene ug/L 20 106 68-151113 620ND21.2 22.6
cis-1,3-Dichloropropene ug/L 20 103 70-139104 120ND20.6 20.8
Dibromochloromethane ug/L 20 100 70-14496 420ND20.0 19.2
Dibromomethane ug/L 20 97 70-13995 220ND19.3 19.0
Dichlorodifluoromethane ug/L 20 106 39-171110 420ND21.2 22.0
Diisopropyl ether ug/L 20 97 67-142106 920ND19.3 21.2
Ethylbenzene ug/L 20 103 70-143105 220ND20.6 21.0
Hexachloro-1,3-butadiene ug/L 20 121 64-163115 520ND24.2 23.1
m&p-Xylene ug/L 40 105 70-144105 040ND41.9 42.0
Methyl-tert-butyl ether ug/L 20 85 65-14391 820ND16.9 18.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3762327MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92623960002
3762328
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Methylene Chloride ug/L 20 109 62-149113 420ND21.7 22.7
Naphthalene ug/L 20 97 67-147103 620ND19.4 20.6
o-Xylene ug/L 20 100 70-145104 520ND20.0 20.9
p-Isopropyltoluene ug/L 20 108 70-147109 220ND21.5 21.9
Styrene ug/L 20 101 70-143104 320ND20.2 20.8
Tetrachloroethene ug/L 20 100 70-14598 220ND19.9 19.6
Toluene ug/L 20 101 70-14298 320ND20.1 19.6
trans-1,2-Dichloroethene ug/L 20 99 70-151104 520ND19.8 20.8
trans-1,3-Dichloropropene ug/L 20 94 70-13998 420ND18.8 19.5
Trichloroethene ug/L 20 115 62-146123 6203.5 26.5 28.1
Trichlorofluoromethane ug/L 20 105 63-153112 620ND21.0 22.4
Vinyl acetate ug/L IK409261-162101 940ND36.8 40.4
Vinyl chloride ug/L 20 127 61-163134 620ND25.4 26.8
Xylene (Total)ug/L 60 103 70-143105 260ND61.8 62.9
1,2-Dichloroethane-d4 (S)%97 70-130108
4-Bromofluorobenzene (S)%100 70-130100
Toluene-d8 (S)%98 70-13098
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
721495
EPA 3510C
EPA 8270E
8270E Water MSSV RVE
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92623480006, 92623480007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3759169
Associated Lab Samples:92623480006, 92623480007
Matrix:Water
Analyzed
1,2,4-Trichlorobenzene ug/L ND 10.0 09/06/22 15:12
1,2-Dichlorobenzene ug/L ND 10.0 09/06/22 15:12
1,3-Dichlorobenzene ug/L ND 10.0 09/06/22 15:12
1,4-Dichlorobenzene ug/L ND 10.0 09/06/22 15:12
1-Methylnaphthalene ug/L ND 10.0 09/06/22 15:12
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 09/06/22 15:12
2,4,5-Trichlorophenol ug/L ND 10.0 09/06/22 15:12
2,4,6-Trichlorophenol ug/L ND 10.0 09/06/22 15:12
2,4-Dichlorophenol ug/L ND 10.0 09/06/22 15:12
2,4-Dimethylphenol ug/L ND 10.0 09/06/22 15:12
2,4-Dinitrophenol ug/L ND 50.0 09/06/22 15:12
2,4-Dinitrotoluene ug/L ND 10.0 09/06/22 15:12
2,6-Dinitrotoluene ug/L ND 10.0 09/06/22 15:12
2-Chloronaphthalene ug/L ND 10.0 09/06/22 15:12
2-Chlorophenol ug/L ND 10.0 09/06/22 15:12
2-Methylnaphthalene ug/L ND 10.0 09/06/22 15:12
2-Methylphenol(o-Cresol)ug/L ND 10.0 09/06/22 15:12
2-Nitroaniline ug/L ND 20.0 09/06/22 15:12
2-Nitrophenol ug/L ND 10.0 09/06/22 15:12
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 09/06/22 15:12
3,3'-Dichlorobenzidine ug/L ND 20.0 09/06/22 15:12
3-Nitroaniline ug/L ND 20.0 09/06/22 15:12
4,6-Dinitro-2-methylphenol ug/L ND 20.0 09/06/22 15:12
4-Bromophenylphenyl ether ug/L ND 10.0 09/06/22 15:12
4-Chloro-3-methylphenol ug/L ND 10.0 09/06/22 15:12
4-Chloroaniline ug/L ND 20.0 09/06/22 15:12
4-Chlorophenylphenyl ether ug/L ND 10.0 09/06/22 15:12
4-Nitroaniline ug/L ND 20.0 09/06/22 15:12
4-Nitrophenol ug/L ND 50.0 09/06/22 15:12
Acenaphthene ug/L ND 10.0 09/06/22 15:12
Acenaphthylene ug/L ND 10.0 09/06/22 15:12
Aniline ug/L ND 10.0 09/06/22 15:12
Anthracene ug/L ND 10.0 09/06/22 15:12
Benzo(a)anthracene ug/L ND 10.0 09/06/22 15:12
Benzo(a)pyrene ug/L ND 10.0 09/06/22 15:12
Benzo(b)fluoranthene ug/L ND 10.0 09/06/22 15:12
Benzo(g,h,i)perylene ug/L ND 10.0 09/06/22 15:12
Benzo(k)fluoranthene ug/L ND 10.0 09/06/22 15:12
Benzoic Acid ug/L ND 50.0 09/06/22 15:12
Benzyl alcohol ug/L ND 20.0 09/06/22 15:12
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3759169
Associated Lab Samples:92623480006, 92623480007
Matrix:Water
Analyzed
bis(2-Chloroethoxy)methane ug/L ND 10.0 09/06/22 15:12
bis(2-Chloroethyl) ether ug/L ND 10.0 09/06/22 15:12
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 09/06/22 15:12
Butylbenzylphthalate ug/L ND 10.0 09/06/22 15:12
Chrysene ug/L ND 10.0 09/06/22 15:12
Di-n-butylphthalate ug/L ND 10.0 09/06/22 15:12
Di-n-octylphthalate ug/L ND 10.0 09/06/22 15:12
Dibenz(a,h)anthracene ug/L ND 10.0 09/06/22 15:12
Dibenzofuran ug/L ND 10.0 09/06/22 15:12
Diethylphthalate ug/L ND 10.0 09/06/22 15:12
Dimethylphthalate ug/L ND 10.0 09/06/22 15:12
Fluoranthene ug/L ND 10.0 09/06/22 15:12
Fluorene ug/L ND 10.0 09/06/22 15:12
Hexachloro-1,3-butadiene ug/L ND 10.0 09/06/22 15:12
Hexachlorobenzene ug/L ND 10.0 09/06/22 15:12
Hexachlorocyclopentadiene ug/L ND 10.0 09/06/22 15:12
Hexachloroethane ug/L ND 10.0 09/06/22 15:12
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 09/06/22 15:12
Isophorone ug/L ND 10.0 09/06/22 15:12
N-Nitroso-di-n-propylamine ug/L ND 10.0 09/06/22 15:12
N-Nitrosodimethylamine ug/L ND 10.0 09/06/22 15:12
N-Nitrosodiphenylamine ug/L ND 10.0 09/06/22 15:12
Naphthalene ug/L ND 10.0 09/06/22 15:12
Nitrobenzene ug/L ND 10.0 09/06/22 15:12
Pentachlorophenol ug/L ND 20.0 09/06/22 15:12
Phenanthrene ug/L ND 10.0 09/06/22 15:12
Phenol ug/L ND 10.0 09/06/22 15:12
Pyrene ug/L ND 10.0 09/06/22 15:12
2,4,6-Tribromophenol (S)%71 10-144 09/06/22 15:12
2-Fluorobiphenyl (S)%68 10-130 09/06/22 15:12
2-Fluorophenol (S)%61 10-130 09/06/22 15:12
Nitrobenzene-d5 (S)%90 10-144 09/06/22 15:12
Phenol-d6 (S)%54 10-130 09/06/22 15:12
Terphenyl-d14 (S)%129 34-163 09/06/22 15:12
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3759170LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 21.750 43 18-130
1,2-Dichlorobenzene ug/L 18.050 36 20-130
1,3-Dichlorobenzene ug/L 15.350 31 18-130
1,4-Dichlorobenzene ug/L 16.150 32 18-130
1-Methylnaphthalene ug/L 27.350 55 29-130
2,2'-Oxybis(1-chloropropane)ug/L 20.850 42 28-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3759170LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,5-Trichlorophenol ug/L 24.750 49 35-130
2,4,6-Trichlorophenol ug/L 23.650 47 31-130
2,4-Dichlorophenol ug/L 24.950 50 35-130
2,4-Dimethylphenol ug/L 29.950 60 34-130
2,4-Dinitrophenol ug/L 80.2250 32 10-153
2,4-Dinitrotoluene ug/L 31.050 62 37-136
2,6-Dinitrotoluene ug/L 29.650 59 33-136
2-Chloronaphthalene ug/L 27.250 54 26-130
2-Chlorophenol ug/L 23.650 47 37-130
2-Methylnaphthalene ug/L 26.850 54 29-130
2-Methylphenol(o-Cresol)ug/L 23.350 47 35-130
2-Nitroaniline ug/L 47.9100 48 37-130
2-Nitrophenol ug/L 23.450 47 32-130
3&4-Methylphenol(m&p Cresol)ug/L 22.550 45 34-130
3,3'-Dichlorobenzidine ug/L 56.1100 56 34-136
3-Nitroaniline ug/L 58.6100 59 37-138
4,6-Dinitro-2-methylphenol ug/L 43.9100 44 21-157
4-Bromophenylphenyl ether ug/L 27.950 56 38-130
4-Chloro-3-methylphenol ug/L 52.1100 52 37-130
4-Chloroaniline ug/L 54.6100 55 38-130
4-Chlorophenylphenyl ether ug/L 27.250 54 33-130
4-Nitroaniline ug/L 58.9100 59 42-137
4-Nitrophenol ug/L 53.0250 21 10-130
Acenaphthene ug/L 28.450 57 33-130
Acenaphthylene ug/L 28.050 56 35-130
Aniline ug/L 22.050 44 22-130
Anthracene ug/L 27.150 54 48-130
Benzo(a)anthracene ug/L 29.050 58 48-137
Benzo(a)pyrene ug/L 30.350 61 49-138
Benzo(b)fluoranthene ug/L 31.450 63 52-138
Benzo(g,h,i)perylene ug/L 33.150 66 48-140
Benzo(k)fluoranthene ug/L 31.350 63 48-139
Benzoic Acid ug/L 59.0250 24 10-130
Benzyl alcohol ug/L 48.0100 48 35-130
bis(2-Chloroethoxy)methane ug/L 27.050 54 34-130
bis(2-Chloroethyl) ether ug/L 26.350 53 36-130
bis(2-Ethylhexyl)phthalate ug/L 29.950 60 32-165
Butylbenzylphthalate ug/L 29.150 58 34-161
Chrysene ug/L 30.050 60 47-131
Di-n-butylphthalate ug/L 27.850 56 39-144
Di-n-octylphthalate ug/L 29.850 60 30-170
Dibenz(a,h)anthracene ug/L 32.350 65 49-138
Dibenzofuran ug/L 28.550 57 33-130
Diethylphthalate ug/L 29.050 58 38-131
Dimethylphthalate ug/L 29.250 58 37-130
Fluoranthene ug/L 30.950 62 46-137
Fluorene ug/L 29.650 59 37-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3759170LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachloro-1,3-butadiene ug/L 18.150 36 11-130
Hexachlorobenzene ug/L 27.650 55 38-130
Hexachlorocyclopentadiene ug/L 18.150 36 10-130
Hexachloroethane ug/L 14.550 29 14-130
Indeno(1,2,3-cd)pyrene ug/L 33.450 67 41-130
Isophorone ug/L 26.950 54 33-130
N-Nitroso-di-n-propylamine ug/L 26.350 53 36-130
N-Nitrosodimethylamine ug/L 21.650 43 34-130
N-Nitrosodiphenylamine ug/L 29.850 60 37-130
Naphthalene ug/L 23.950 48 30-130
Nitrobenzene ug/L 25.350 51 36-130
Pentachlorophenol ug/L 43.5100 44 23-149
Phenanthrene ug/L 30.550 61 44-130
Phenol ug/L 16.550 33 18-130
Pyrene ug/L 30.550 61 47-134
2,4,6-Tribromophenol (S)%63 10-144
2-Fluorobiphenyl (S)%56 10-130
2-Fluorophenol (S)%39 10-130
Nitrobenzene-d5 (S)%54 10-144
Phenol-d6 (S)%35 10-130
Terphenyl-d14 (S)%62 34-163
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3759198MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92623694001
3759199
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L 50 29 10-13024 2150ND14.6 11.8
1,2-Dichlorobenzene ug/L 50 16 10-1301350ND8.1J 6.4J
1,3-Dichlorobenzene ug/L 50 11 10-1301050ND5.6J 4.8J
1,4-Dichlorobenzene ug/L 50 13 10-1301150ND6.5J 5.5J
1-Methylnaphthalene ug/L 50 69 10-13060 1450ND34.5 30.2
2,2'-Oxybis(1-chloropropane)ug/L 50 54 12-14246 1650ND27.0 22.9
2,4,5-Trichlorophenol ug/L 50 74 10-14360 2150ND37.0 30.1
2,4,6-Trichlorophenol ug/L 50 56 10-14753 750ND28.2 26.4
2,4-Dichlorophenol ug/L 50 75 10-13866 1250ND37.5 33.1
2,4-Dimethylphenol ug/L 50 103 25-13090 1450ND51.4 44.8
2,4-Dinitrophenol ug/L 250 28 10-16537 26250ND70.5 91.6
2,4-Dinitrotoluene ug/L 50 113 29-14899 1450ND56.6 49.4
2,6-Dinitrotoluene ug/L 50 113 26-14695 1750ND56.4 47.4
2-Chloronaphthalene ug/L 50 82 11-13075 950ND41.0 37.4
2-Chlorophenol ug/L 50 61 10-13354 1350ND30.7 26.9
2-Methylnaphthalene ug/L 50 63 13-13056 1150ND31.4 28.2
2-Methylphenol(o-Cresol)ug/L 50 79 20-13067 1750ND39.4 33.3
2-Nitroaniline ug/L 100 95 24-13682 15100ND95.4 82.0
2-Nitrophenol ug/L 50 66 10-15358 1250ND32.9 29.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3759198MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92623694001
3759199
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
3&4-Methylphenol(m&p
Cresol)ug/L 50 79 16-13068 1550ND39.5 33.8
3,3'-Dichlorobenzidine ug/L 100 105 10-15389 17100ND10588.7
3-Nitroaniline ug/L 100 114 22-15198 15100ND11497.6
4,6-Dinitro-2-methylphenol ug/L 100 43 10-18050 15100ND42.7 49.6
4-Bromophenylphenyl ether ug/L 50 104 25-13088 1750ND52.2 44.0
4-Chloro-3-methylphenol ug/L 100 97 25-13382 17100ND97.1 81.7
4-Chloroaniline ug/L 100 96 14-13284 14100ND96.4 84.1
4-Chlorophenylphenyl ether ug/L 50 97 19-13084 1450ND48.4 41.9
4-Nitroaniline ug/L 100 109 29-15095 14100ND10994.9
4-Nitrophenol ug/L 250 17 10-13023250ND42.3J 57.8
Acenaphthene ug/L 50 97 16-13086 1250ND48.3 42.9
Acenaphthylene ug/L 50 95 15-13784 1350ND47.6 41.8
Aniline ug/L 50 69 10-13058 1850ND34.5 28.8
Anthracene ug/L 50 103 37-13686 1750ND51.3 43.1
Benzo(a)anthracene ug/L 50 111 40-14594 1750ND55.6 47.0
Benzo(a)pyrene ug/L 50 115 41-14698 1650ND57.3 49.0
Benzo(b)fluoranthene ug/L 50 115 39-15198 1650ND57.6 49.2
Benzo(g,h,i)perylene ug/L 50 119 40-147103 1550ND59.4 51.3
Benzo(k)fluoranthene ug/L 50 120 40-146101 1750ND59.9 50.3
Benzoic Acid ug/L 250 25 10-13027 7250ND62.2 66.4
Benzyl alcohol ug/L 100 86 25-13071 19100ND86.3 71.5
bis(2-Chloroethoxy)methane ug/L 50 89 23-13074 1850ND44.4 37.2
bis(2-Chloroethyl) ether ug/L 50 77 25-13066 1550ND38.6 33.1
bis(2-Ethylhexyl)phthalate ug/L 50 119 28-166102 1550ND59.3 51.1
Butylbenzylphthalate ug/L 50 120 33-165102 1650ND60.1 51.0
Chrysene ug/L 50 111 38-14196 1450ND55.4 48.2
Di-n-butylphthalate ug/L 50 111 32-15392 1850ND55.4 46.2
Di-n-octylphthalate ug/L 50 123 30-175104 1650ND61.4 52.1
Dibenz(a,h)anthracene ug/L 50 119 39-148102 1550ND59.7 51.1
Dibenzofuran ug/L 50 101 20-13087 1450ND50.4 43.7
Diethylphthalate ug/L 50 108 28-14293 1450ND53.8 46.6
Dimethylphthalate ug/L 50 107 26-13692 1550ND53.3 46.0
Fluoranthene ug/L 50 113 39-14397 1650ND56.6 48.5
Fluorene ug/L 50 105 24-13292 1450ND52.5 45.8
Hexachloro-1,3-butadiene ug/L 50 13 10-1301050ND6.3J 5J
Hexachlorobenzene ug/L 50 106 29-13088 1950ND52.9 43.8
Hexachlorocyclopentadiene ug/L 50 34 10-13030 1250ND16.9 15.0
Hexachloroethane ug/L M150710-130550ND3.3J 2.3J
Indeno(1,2,3-cd)pyrene ug/L 50 120 39-148104 1450ND59.9 51.9
Isophorone ug/L 50 96 23-13083 1550ND48.0 41.3
N-Nitroso-di-n-propylamine ug/L 50 89 25-13075 1750ND44.3 37.3
N-Nitrosodimethylamine ug/L 50 69 22-13059 1550ND34.3 29.6
N-Nitrosodiphenylamine ug/L 50 110 26-13492 1850ND54.9 45.8
Naphthalene ug/L 50 44 14-13036 2150ND22.2 18.0
Nitrobenzene ug/L 50 74 25-13065 1450ND37.1 32.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3759198MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92623694001
3759199
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Pentachlorophenol ug/L 100 40 10-17541 3100ND39.5 40.9
Phenanthrene ug/L 50 112 36-13396 1650ND56.2 47.9
Phenol ug/L 50 49 10-13043 1450ND24.5 21.3
Pyrene ug/L 50 114 40-14398 1650ND57.2 48.9
2,4,6-Tribromophenol (S)%82 10-14465
2-Fluorobiphenyl (S)%72 10-13058
2-Fluorophenol (S)%39 10-13038
Nitrobenzene-d5 (S)%80 10-14469
Phenol-d6 (S)%48 10-13039
Terphenyl-d14 (S)%124 34-163103
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
721579
EPA 3510C
EPA 8270E
8270E Water MSSV RVE
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92623480008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3759571
Associated Lab Samples:92623480008
Matrix:Water
Analyzed
1,2,4-Trichlorobenzene ug/L ND 10.0 09/06/22 16:56
1,2-Dichlorobenzene ug/L ND 10.0 09/06/22 16:56
1,3-Dichlorobenzene ug/L ND 10.0 09/06/22 16:56
1,4-Dichlorobenzene ug/L ND 10.0 09/06/22 16:56
1-Methylnaphthalene ug/L ND 10.0 09/06/22 16:56
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 09/06/22 16:56
2,4,5-Trichlorophenol ug/L ND 10.0 09/06/22 16:56
2,4,6-Trichlorophenol ug/L ND 10.0 09/06/22 16:56
2,4-Dichlorophenol ug/L ND 10.0 09/06/22 16:56
2,4-Dimethylphenol ug/L ND 10.0 09/06/22 16:56
2,4-Dinitrophenol ug/L ND 50.0 09/06/22 16:56
2,4-Dinitrotoluene ug/L ND 10.0 09/06/22 16:56
2,6-Dinitrotoluene ug/L ND 10.0 09/06/22 16:56
2-Chloronaphthalene ug/L ND 10.0 09/06/22 16:56
2-Chlorophenol ug/L ND 10.0 09/06/22 16:56
2-Methylnaphthalene ug/L ND 10.0 09/06/22 16:56
2-Methylphenol(o-Cresol)ug/L ND 10.0 09/06/22 16:56
2-Nitroaniline ug/L ND 20.0 09/06/22 16:56
2-Nitrophenol ug/L ND 10.0 09/06/22 16:56
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 09/06/22 16:56
3,3'-Dichlorobenzidine ug/L ND 20.0 09/06/22 16:56
3-Nitroaniline ug/L ND 20.0 09/06/22 16:56
4,6-Dinitro-2-methylphenol ug/L ND 20.0 09/06/22 16:56
4-Bromophenylphenyl ether ug/L ND 10.0 09/06/22 16:56
4-Chloro-3-methylphenol ug/L ND 10.0 09/06/22 16:56
4-Chloroaniline ug/L ND 20.0 09/06/22 16:56
4-Chlorophenylphenyl ether ug/L ND 10.0 09/06/22 16:56
4-Nitroaniline ug/L ND 20.0 09/06/22 16:56
4-Nitrophenol ug/L ND 50.0 09/06/22 16:56
Acenaphthene ug/L ND 10.0 09/06/22 16:56
Acenaphthylene ug/L ND 10.0 09/06/22 16:56
Aniline ug/L ND 10.0 09/06/22 16:56
Anthracene ug/L ND 10.0 09/06/22 16:56
Benzo(a)anthracene ug/L ND 10.0 09/06/22 16:56
Benzo(a)pyrene ug/L ND 10.0 09/06/22 16:56
Benzo(b)fluoranthene ug/L ND 10.0 09/06/22 16:56
Benzo(g,h,i)perylene ug/L ND 10.0 09/06/22 16:56
Benzo(k)fluoranthene ug/L ND 10.0 09/06/22 16:56
Benzoic Acid ug/L ND 50.0 09/06/22 16:56
Benzyl alcohol ug/L ND 20.0 09/06/22 16:56
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3759571
Associated Lab Samples:92623480008
Matrix:Water
Analyzed
bis(2-Chloroethoxy)methane ug/L ND 10.0 09/06/22 16:56
bis(2-Chloroethyl) ether ug/L ND 10.0 09/06/22 16:56
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 09/06/22 16:56
Butylbenzylphthalate ug/L ND 10.0 09/06/22 16:56
Chrysene ug/L ND 10.0 09/06/22 16:56
Di-n-butylphthalate ug/L ND 10.0 09/06/22 16:56
Di-n-octylphthalate ug/L ND 10.0 09/06/22 16:56
Dibenz(a,h)anthracene ug/L ND 10.0 09/06/22 16:56
Dibenzofuran ug/L ND 10.0 09/06/22 16:56
Diethylphthalate ug/L ND 10.0 09/06/22 16:56
Dimethylphthalate ug/L ND 10.0 09/06/22 16:56
Fluoranthene ug/L ND 10.0 09/06/22 16:56
Fluorene ug/L ND 10.0 09/06/22 16:56
Hexachloro-1,3-butadiene ug/L ND 10.0 09/06/22 16:56
Hexachlorobenzene ug/L ND 10.0 09/06/22 16:56
Hexachlorocyclopentadiene ug/L ND 10.0 09/06/22 16:56
Hexachloroethane ug/L ND 10.0 09/06/22 16:56
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 09/06/22 16:56
Isophorone ug/L ND 10.0 09/06/22 16:56
N-Nitroso-di-n-propylamine ug/L ND 10.0 09/06/22 16:56
N-Nitrosodimethylamine ug/L ND 10.0 09/06/22 16:56
N-Nitrosodiphenylamine ug/L ND 10.0 09/06/22 16:56
Naphthalene ug/L ND 10.0 09/06/22 16:56
Nitrobenzene ug/L ND 10.0 09/06/22 16:56
Pentachlorophenol ug/L ND 20.0 09/06/22 16:56
Phenanthrene ug/L ND 10.0 09/06/22 16:56
Phenol ug/L ND 10.0 09/06/22 16:56
Pyrene ug/L ND 10.0 09/06/22 16:56
2,4,6-Tribromophenol (S)%72 10-144 09/06/22 16:56
2-Fluorobiphenyl (S)%46 10-130 09/06/22 16:56
2-Fluorophenol (S)%49 10-130 09/06/22 16:56
Nitrobenzene-d5 (S)%61 10-144 09/06/22 16:56
Phenol-d6 (S)%42 10-130 09/06/22 16:56
Terphenyl-d14 (S)%98 34-163 09/06/22 16:56
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3759572LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 30.650 61 18-130
1,2-Dichlorobenzene ug/L 23.750 47 20-130
1,3-Dichlorobenzene ug/L 19.950 40 18-130
1,4-Dichlorobenzene ug/L 21.150 42 18-130
1-Methylnaphthalene ug/L 41.350 83 29-130
2,2'-Oxybis(1-chloropropane)ug/L 28.650 57 28-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3759572LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,5-Trichlorophenol ug/L 45.550 91 35-130
2,4,6-Trichlorophenol ug/L 44.450 89 31-130
2,4-Dichlorophenol ug/L 41.650 83 35-130
2,4-Dimethylphenol ug/L 46.050 92 34-130
2,4-Dinitrophenol ug/L 184250 74 10-153
2,4-Dinitrotoluene ug/L 48.050 96 37-136
2,6-Dinitrotoluene ug/L 47.750 95 33-136
2-Chloronaphthalene ug/L 43.650 87 26-130
2-Chlorophenol ug/L 36.350 73 37-130
2-Methylnaphthalene ug/L 39.950 80 29-130
2-Methylphenol(o-Cresol)ug/L 36.650 73 35-130
2-Nitroaniline ug/L 80.2100 80 37-130
2-Nitrophenol ug/L 38.750 77 32-130
3&4-Methylphenol(m&p Cresol)ug/L 36.950 74 34-130
3,3'-Dichlorobenzidine ug/L 92.0100 92 34-136
3-Nitroaniline ug/L 96.7100 97 37-138
4,6-Dinitro-2-methylphenol ug/L 92.9100 93 21-157
4-Bromophenylphenyl ether ug/L 46.450 93 38-130
4-Chloro-3-methylphenol ug/L 83.1100 83 37-130
4-Chloroaniline ug/L 86.6100 87 38-130
4-Chlorophenylphenyl ether ug/L 42.550 85 33-130
4-Nitroaniline ug/L 93.5100 94 42-137
4-Nitrophenol ug/L 117250 47 10-130
Acenaphthene ug/L 44.850 90 33-130
Acenaphthylene ug/L 44.550 89 35-130
Aniline ug/L 33.750 67 22-130
Anthracene ug/L 43.650 87 48-130
Benzo(a)anthracene ug/L 47.050 94 48-137
Benzo(a)pyrene ug/L 49.050 98 49-138
Benzo(b)fluoranthene ug/L 50.250 100 52-138
Benzo(g,h,i)perylene ug/L 50.050 100 48-140
Benzo(k)fluoranthene ug/L 51.150 102 48-139
Benzoic Acid ug/L 120250 48 10-130
Benzyl alcohol ug/L 78.3100 78 35-130
bis(2-Chloroethoxy)methane ug/L 40.350 81 34-130
bis(2-Chloroethyl) ether ug/L 36.250 72 36-130
bis(2-Ethylhexyl)phthalate ug/L 51.050 102 32-165
Butylbenzylphthalate ug/L 51.150 102 34-161
Chrysene ug/L 47.650 95 47-131
Di-n-butylphthalate ug/L 46.650 93 39-144
Di-n-octylphthalate ug/L 50.050 100 30-170
Dibenz(a,h)anthracene ug/L 49.950 100 49-138
Dibenzofuran ug/L 44.750 89 33-130
Diethylphthalate ug/L 45.650 91 38-131
Dimethylphthalate ug/L 45.150 90 37-130
Fluoranthene ug/L 48.050 96 46-137
Fluorene ug/L 45.850 92 37-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3759572LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachloro-1,3-butadiene ug/L 24.050 48 11-130
Hexachlorobenzene ug/L 45.650 91 38-130
Hexachlorocyclopentadiene ug/L 30.550 61 10-130
Hexachloroethane ug/L 18.650 37 14-130
Indeno(1,2,3-cd)pyrene ug/L 51.050 102 41-130
Isophorone ug/L 42.850 86 33-130
N-Nitroso-di-n-propylamine ug/L 40.150 80 36-130
N-Nitrosodimethylamine ug/L 31.550 63 34-130
N-Nitrosodiphenylamine ug/L 49.450 99 37-130
Naphthalene ug/L 34.750 69 30-130
Nitrobenzene ug/L 35.950 72 36-130
Pentachlorophenol ug/L 91.1100 91 23-149
Phenanthrene ug/L 48.750 97 44-130
Phenol ug/L 26.950 54 18-130
Pyrene ug/L 50.850 102 47-134
2,4,6-Tribromophenol (S)%109 10-144
2-Fluorobiphenyl (S)%86 10-130
2-Fluorophenol (S)%64 10-130
Nitrobenzene-d5 (S)%79 10-144
Phenol-d6 (S)%56 10-130
Terphenyl-d14 (S)%109 34-163
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3759573MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92613441020
3759574
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L 50 22 10-1302050ND10.8 9.8J
1,2-Dichlorobenzene ug/L 50 12 10-1301250ND6.1J 6.2J
1,3-Dichlorobenzene ug/L M150710-130750ND3.3J 3.6J
1,4-Dichlorobenzene ug/L M150910-130950ND4.4J 4.4J
1-Methylnaphthalene ug/L 50 44 10-13044 150ND22.0 21.8
2,2'-Oxybis(1-chloropropane)ug/L 50 34 12-14236 750ND16.9 18.1
2,4,5-Trichlorophenol ug/L 50 43 10-14353 1950ND21.7 26.3
2,4,6-Trichlorophenol ug/L 50 27 10-14733 2050ND13.6 16.6
2,4-Dichlorophenol ug/L 50 51 10-13855 750ND25.6 27.4
2,4-Dimethylphenol ug/L 50 81 25-13079 250ND40.3 39.5
2,4-Dinitrophenol ug/L 250 11 10-16511250ND27.7J 28.4J
2,4-Dinitrotoluene ug/L 50 73 29-14882 1250ND36.4 41.1
2,6-Dinitrotoluene ug/L 50 76 26-14680 550ND38.2 40.1
2-Chloronaphthalene ug/L 50 51 11-13053 350ND25.5 26.4
2-Chlorophenol ug/L 50 38 10-13339 550ND18.8 19.7
2-Methylnaphthalene ug/L 50 42 13-13042 150ND20.9 21.0
2-Methylphenol(o-Cresol)ug/L 50 52 20-13052 050ND26.0 26.1
2-Nitroaniline ug/L 100 57 24-13663 10100ND57.1 62.9
2-Nitrophenol ug/L v1504910-15353 850ND24.3 26.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3759573MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92613441020
3759574
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
3&4-Methylphenol(m&p
Cresol)ug/L 50 56 16-13054 550ND28.2 26.8
3,3'-Dichlorobenzidine ug/L 100 50 10-15358 16100ND50.0 58.5
3-Nitroaniline ug/L 100 44 22-15146 4100ND44.3 46.3
4,6-Dinitro-2-methylphenol ug/L 100 13 10-18015100ND12.7J 14.7J
4-Bromophenylphenyl ether ug/L 50 71 25-13082 1450ND35.5 40.9
4-Chloro-3-methylphenol ug/L 100 66 25-13373 9100ND66.5 72.5
4-Chloroaniline ug/L 100 45 14-13246 2100ND45.3 46.5
4-Chlorophenylphenyl ether ug/L 50 62 19-13071 1250ND31.1 35.3
4-Nitroaniline ug/L 100 38 29-15038 1100ND37.6 38.1
4-Nitrophenol ug/L M1250310-1305250NDND12.4J
Acenaphthene ug/L 50 56 16-13060 750ND28.1 30.2
Acenaphthylene ug/L 50 58 15-13761 550ND28.9 30.4
Aniline ug/L 50 38 10-13037 150ND18.9 18.7
Anthracene ug/L 50 64 37-13674 1550ND31.8 36.9
Benzo(a)anthracene ug/L 50 78 40-14595 1950ND39.0 47.4
Benzo(a)pyrene ug/L 50 80 41-14699 2150ND39.9 49.5
Benzo(b)fluoranthene ug/L 50 80 39-15198 2050ND40.1 48.9
Benzo(g,h,i)perylene ug/L 50 86 40-147102 1750ND42.9 50.8
Benzo(k)fluoranthene ug/L 50 79 40-14695 1850ND39.5 47.5
Benzoic Acid ug/L M1250010-1300250NDNDND
Benzyl alcohol ug/L 100 57 25-13054 6100ND57.2 53.7
bis(2-Chloroethoxy)methane ug/L 50 55 23-13054 150ND27.4 27.2
bis(2-Chloroethyl) ether ug/L 50 44 25-13046 550ND21.9 23.1
bis(2-Ethylhexyl)phthalate ug/L 50 88 28-166116 2850ND44.0 58.1
Butylbenzylphthalate ug/L v1509733-165122 2350ND48.5 60.8
Chrysene ug/L 50 76 38-14192 1950ND38.0 46.0
Di-n-butylphthalate ug/L 50 82 32-153100 2050ND40.8 50.1
Di-n-octylphthalate ug/L 50 79 30-175105 2850ND39.5 52.5
Dibenz(a,h)anthracene ug/L 50 81 39-148102 2450ND40.5 51.2
Dibenzofuran ug/L 50 61 20-13066 850ND30.4 33.1
Diethylphthalate ug/L 50 69 28-14279 1450ND34.5 39.6
Dimethylphthalate ug/L 50 68 26-13674 950ND33.8 36.9
Fluoranthene ug/L 50 73 39-14389 2050ND36.6 44.6
Fluorene ug/L 50 62 24-13269 1050ND31.2 34.4
Hexachloro-1,3-butadiene ug/L 50 13 10-1301150ND6.5J 5.6J
Hexachlorobenzene ug/L 50 67 29-13080 1850ND33.5 39.9
Hexachlorocyclopentadiene ug/L 50 24 10-13025 250ND12.0 12.3
Hexachloroethane ug/L M150610-130550ND3J2.6J
Indeno(1,2,3-cd)pyrene ug/L 50 87 39-148101 1550ND43.7 50.6
Isophorone ug/L 50 66 23-13064 350ND32.9 32.0
N-Nitroso-di-n-propylamine ug/L 50 59 25-13056 550ND29.7 28.2
N-Nitrosodimethylamine ug/L 50 45 22-13045 150ND22.7 22.4
N-Nitrosodiphenylamine ug/L 50 70 26-13484 1750ND35.2 41.9
Naphthalene ug/L 50 27 14-13027 250ND13.3 13.6
Nitrobenzene ug/L 50 60 25-13064 750ND29.8 31.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3759573MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92613441020
3759574
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Pentachlorophenol ug/L M1100510-1754100ND4.5J 4.3J
Phenanthrene ug/L 50 69 36-13380 1550ND34.6 40.2
Phenol ug/L 50 37 10-13035 550ND18.3 17.4
Pyrene ug/L 50 84 40-143103 2050ND42.1 51.5
2,4,6-Tribromophenol (S)%39 10-14449
2-Fluorobiphenyl (S)%41 10-13045
2-Fluorophenol (S)%28 10-13028
Nitrobenzene-d5 (S)%54 10-14453
Phenol-d6 (S)%37 10-13035
Terphenyl-d14 (S)%89 34-163115
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
721423
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92623480001, 92623480002, 92623480003, 92623480004, 92623480005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3758895
Associated Lab Samples:92623480001, 92623480002, 92623480003, 92623480004, 92623480005
Matrix:Solid
Analyzed
1,2,4-Trichlorobenzene mg/kg ND 0.32 09/06/22 12:43
1,2-Dichlorobenzene mg/kg ND 0.32 09/06/22 12:43
1,3-Dichlorobenzene mg/kg ND 0.32 09/06/22 12:43
1,4-Dichlorobenzene mg/kg ND 0.32 09/06/22 12:43
1-Methylnaphthalene mg/kg ND 0.32 09/06/22 12:43
2,2'-Oxybis(1-chloropropane)mg/kg ND 0.32 09/06/22 12:43
2,4,5-Trichlorophenol mg/kg ND 0.32 09/06/22 12:43
2,4,6-Trichlorophenol mg/kg ND 0.32 09/06/22 12:43
2,4-Dichlorophenol mg/kg ND 0.32 09/06/22 12:43
2,4-Dimethylphenol mg/kg ND 0.32 09/06/22 12:43
2,4-Dinitrophenol mg/kg ND 1.6 09/06/22 12:43
2,4-Dinitrotoluene mg/kg ND 0.32 09/06/22 12:43
2,6-Dinitrotoluene mg/kg ND 0.32 09/06/22 12:43
2-Chloronaphthalene mg/kg ND 0.32 09/06/22 12:43
2-Chlorophenol mg/kg ND 0.32 09/06/22 12:43
2-Methylnaphthalene mg/kg ND 0.32 09/06/22 12:43
2-Methylphenol(o-Cresol)mg/kg ND 0.32 09/06/22 12:43
2-Nitroaniline mg/kg ND 1.6 09/06/22 12:43
2-Nitrophenol mg/kg ND 0.32 09/06/22 12:43
3&4-Methylphenol(m&p Cresol)mg/kg ND 0.32 09/06/22 12:43
3,3'-Dichlorobenzidine mg/kg ND 0.65 09/06/22 12:43
3-Nitroaniline mg/kg ND 1.6 09/06/22 12:43
4,6-Dinitro-2-methylphenol mg/kg ND 0.65 09/06/22 12:43
4-Bromophenylphenyl ether mg/kg ND 0.32 09/06/22 12:43
4-Chloro-3-methylphenol mg/kg ND 0.65 09/06/22 12:43
4-Chloroaniline mg/kg ND 0.65 09/06/22 12:43
4-Chlorophenylphenyl ether mg/kg ND 0.32 09/06/22 12:43
4-Nitroaniline mg/kg ND 0.65 09/06/22 12:43
4-Nitrophenol mg/kg ND 1.6 09/06/22 12:43
Acenaphthene mg/kg ND 0.32 09/06/22 12:43
Acenaphthylene mg/kg ND 0.32 09/06/22 12:43
Aniline mg/kg ND 0.32 09/06/22 12:43
Anthracene mg/kg ND 0.32 09/06/22 12:43
Benzo(a)anthracene mg/kg ND 0.32 09/06/22 12:43
Benzo(a)pyrene mg/kg ND 0.32 09/06/22 12:43
Benzo(b)fluoranthene mg/kg ND 0.32 09/06/22 12:43
Benzo(g,h,i)perylene mg/kg ND 0.32 09/06/22 12:43
Benzo(k)fluoranthene mg/kg ND 0.32 09/06/22 12:43
Benzoic Acid mg/kg ND 1.6 09/06/22 12:43
Benzyl alcohol mg/kg ND 0.65 09/06/22 12:43
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3758895
Associated Lab Samples:92623480001, 92623480002, 92623480003, 92623480004, 92623480005
Matrix:Solid
Analyzed
bis(2-Chloroethoxy)methane mg/kg ND 0.32 09/06/22 12:43
bis(2-Chloroethyl) ether mg/kg ND 0.32 09/06/22 12:43
bis(2-Ethylhexyl)phthalate mg/kg ND 0.32 v209/06/22 12:43
Butylbenzylphthalate mg/kg ND 0.32 09/06/22 12:43
Chrysene mg/kg ND 0.32 09/06/22 12:43
Di-n-butylphthalate mg/kg ND 0.32 09/06/22 12:43
Di-n-octylphthalate mg/kg ND 0.32 09/06/22 12:43
Dibenz(a,h)anthracene mg/kg ND 0.32 09/06/22 12:43
Dibenzofuran mg/kg ND 0.32 09/06/22 12:43
Diethylphthalate mg/kg ND 0.32 09/06/22 12:43
Dimethylphthalate mg/kg ND 0.32 09/06/22 12:43
Fluoranthene mg/kg ND 0.32 09/06/22 12:43
Fluorene mg/kg ND 0.32 09/06/22 12:43
Hexachloro-1,3-butadiene mg/kg ND 0.32 09/06/22 12:43
Hexachlorobenzene mg/kg ND 0.32 09/06/22 12:43
Hexachlorocyclopentadiene mg/kg ND 0.32 09/06/22 12:43
Hexachloroethane mg/kg ND 0.32 09/06/22 12:43
Indeno(1,2,3-cd)pyrene mg/kg ND 0.32 09/06/22 12:43
Isophorone mg/kg ND 0.32 09/06/22 12:43
N-Nitroso-di-n-propylamine mg/kg ND 0.32 09/06/22 12:43
N-Nitrosodimethylamine mg/kg ND 0.32 09/06/22 12:43
N-Nitrosodiphenylamine mg/kg ND 0.32 09/06/22 12:43
Naphthalene mg/kg ND 0.32 09/06/22 12:43
Nitrobenzene mg/kg ND 0.32 09/06/22 12:43
Pentachlorophenol mg/kg ND 0.65 09/06/22 12:43
Phenanthrene mg/kg ND 0.32 09/06/22 12:43
Phenol mg/kg ND 0.32 09/06/22 12:43
Pyrene mg/kg ND 0.32 09/06/22 12:43
Pyridine mg/kg ND 0.32 09/06/22 12:43
2,4,6-Tribromophenol (S)%70 18-130 09/06/22 12:43
2-Fluorobiphenyl (S)%49 19-130 09/06/22 12:43
2-Fluorophenol (S)%52 18-130 09/06/22 12:43
Nitrobenzene-d5 (S)%51 21-130 09/06/22 12:43
Phenol-d6 (S)%52 18-130 09/06/22 12:43
Terphenyl-d14 (S)%79 15-130 09/06/22 12:43
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3758896LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene mg/kg 1.21.7 72 47-130
1,2-Dichlorobenzene mg/kg 1.11.7 67 49-130
1,3-Dichlorobenzene mg/kg 1.11.7 68 48-130
1,4-Dichlorobenzene mg/kg 1.11.7 67 49-130
1-Methylnaphthalene mg/kg 1.31.7 77 54-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 59 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3758896LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)mg/kg 1.21.7 71 38-130
2,4,5-Trichlorophenol mg/kg 1.51.7 87 49-130
2,4,6-Trichlorophenol mg/kg 1.41.7 82 50-130
2,4-Dichlorophenol mg/kg 1.31.7 78 51-130
2,4-Dimethylphenol mg/kg 1.51.7 89 53-130
2,4-Dinitrophenol mg/kg 4.18.4 48 39-130
2,4-Dinitrotoluene mg/kg 1.41.7 85 53-130
2,6-Dinitrotoluene mg/kg 1.51.7 87 55-130
2-Chloronaphthalene mg/kg 1.31.7 77 48-130
2-Chlorophenol mg/kg 1.21.7 73 54-130
2-Methylnaphthalene mg/kg 1.21.7 74 57-130
2-Methylphenol(o-Cresol)mg/kg 1.21.7 71 50-130
2-Nitroaniline mg/kg 3.03.4 88 49-130
2-Nitrophenol mg/kg 1.41.7 83 50-130
3&4-Methylphenol(m&p Cresol)mg/kg 1.11.7 67 50-130
3,3'-Dichlorobenzidine mg/kg 2.53.4 74 47-130
3-Nitroaniline mg/kg 2.93.4 87 45-130
4,6-Dinitro-2-methylphenol mg/kg 2.23.4 67 50-142
4-Bromophenylphenyl ether mg/kg 1.51.7 91 55-130
4-Chloro-3-methylphenol mg/kg 2.93.4 85 52-130
4-Chloroaniline mg/kg 2.53.4 73 49-130
4-Chlorophenylphenyl ether mg/kg 1.41.7 81 53-130
4-Nitroaniline mg/kg 2.83.4 83 51-130
4-Nitrophenol mg/kg 6.58.4 78 40-130
Acenaphthene mg/kg 1.31.7 76 56-130
Acenaphthylene mg/kg 1.41.7 86 58-130
Aniline mg/kg 1.21.7 69 44-130
Anthracene mg/kg 1.31.7 75 60-130
Benzo(a)anthracene mg/kg 1.41.7 81 59-130
Benzo(a)pyrene mg/kg 1.61.7 96 57-130
Benzo(b)fluoranthene mg/kg 1.61.7 96 54-130
Benzo(g,h,i)perylene mg/kg 1.61.7 97 59-130
Benzo(k)fluoranthene mg/kg 1.41.7 86 54-130
Benzoic Acid mg/kg 2.88.4 33 19-130
Benzyl alcohol mg/kg 2.53.4 73 50-130
bis(2-Chloroethoxy)methane mg/kg 1.21.7 74 55-130
bis(2-Chloroethyl) ether mg/kg 1.21.7 69 53-130
bis(2-Ethylhexyl)phthalate mg/kg 1.2 v31.7 69 58-130
Butylbenzylphthalate mg/kg 1.41.7 86 46-138
Chrysene mg/kg 1.51.7 89 57-130
Di-n-butylphthalate mg/kg 1.31.7 76 57-130
Di-n-octylphthalate mg/kg 1.61.7 93 57-130
Dibenz(a,h)anthracene mg/kg 1.61.7 95 60-130
Dibenzofuran mg/kg 1.41.7 81 54-130
Diethylphthalate mg/kg 1.41.7 81 55-130
Dimethylphthalate mg/kg 1.41.7 82 57-130
Fluoranthene mg/kg 1.51.7 89 57-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3758896LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene mg/kg 1.41.7 81 56-130
Hexachloro-1,3-butadiene mg/kg 1.21.7 74 41-130
Hexachlorobenzene mg/kg 1.41.7 86 53-130
Hexachlorocyclopentadiene mg/kg 1.11.7 65 23-130
Hexachloroethane mg/kg 1.11.7 65 48-130
Indeno(1,2,3-cd)pyrene mg/kg 1.61.7 97 61-130
Isophorone mg/kg 1.31.7 78 49-130
N-Nitroso-di-n-propylamine mg/kg 1.11.7 66 52-130
N-Nitrosodimethylamine mg/kg 0.931.7 55 45-130
N-Nitrosodiphenylamine mg/kg 1.31.7 78 56-130
Naphthalene mg/kg 1.21.7 72 56-130
Nitrobenzene mg/kg 1.31.7 77 50-130
Pentachlorophenol mg/kg 2.43.4 71 33-130
Phenanthrene mg/kg 1.41.7 83 60-130
Phenol mg/kg 1.41.7 84 54-130
Pyrene mg/kg 1.51.7 89 61-130
Pyridine mg/kg 0.821.7 49 35-130
2,4,6-Tribromophenol (S)%87 18-130
2-Fluorobiphenyl (S)%74 19-130
2-Fluorophenol (S)%77 18-130
Nitrobenzene-d5 (S)%76 21-130
Phenol-d6 (S)%77 18-130
Terphenyl-d14 (S)%86 15-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3758897MATRIX SPIKE SAMPLE:
MSSpike
Result
92623068001
1,2,4-Trichlorobenzene mg/kg 1.12 56 22-130ND
1,2-Dichlorobenzene mg/kg 1.02 54 23-130ND
1,3-Dichlorobenzene mg/kg 1.12 55 26-130ND
1,4-Dichlorobenzene mg/kg 1.02 55 27-130ND
1-Methylnaphthalene mg/kg 1.12 58 30-130ND
2,2'-Oxybis(1-chloropropane)mg/kg 1.12 58 30-130ND
2,4,5-Trichlorophenol mg/kg 1.42 74 26-130ND
2,4,6-Trichlorophenol mg/kg 1.32 69 23-130ND
2,4-Dichlorophenol mg/kg 1.22 63 29-130ND
2,4-Dimethylphenol mg/kg 1.42 71 13-130ND
2,4-Dinitrophenol mg/kg 6.59.6 68 10-131ND
2,4-Dinitrotoluene mg/kg 1.42 75 28-130ND
2,6-Dinitrotoluene mg/kg 1.52 76 36-130ND
2-Chloronaphthalene mg/kg 1.12 59 27-130ND
2-Chlorophenol mg/kg 1.22 61 29-130ND
2-Methylnaphthalene mg/kg 1.12 56 29-130ND
2-Methylphenol(o-Cresol)mg/kg 1.12 56 20-130ND
2-Nitroaniline mg/kg 3.03.8 79 29-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
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[phone]
Page 61 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3758897MATRIX SPIKE SAMPLE:
MSSpike
Result
92623068001
2-Nitrophenol mg/kg 1.32 67 26-130ND
3&4-Methylphenol(m&p Cresol)mg/kg 1.02 53 10-176ND
3,3'-Dichlorobenzidine mg/kg 2.43.8 62 15-130ND
3-Nitroaniline mg/kg 3.03.8 79 28-130ND
4,6-Dinitro-2-methylphenol mg/kg 2.63.8 69 15-132ND
4-Bromophenylphenyl ether mg/kg 1.42 71 35-130ND
4-Chloro-3-methylphenol mg/kg 2.73.8 70 30-130ND
4-Chloroaniline mg/kg 2.33.8 60 28-130ND
4-Chlorophenylphenyl ether mg/kg 1.22 64 32-130ND
4-Nitroaniline mg/kg 2.83.8 74 30-130ND
4-Nitrophenol mg/kg 6.99.6 73 17-130ND
Acenaphthene mg/kg 1.12 60 29-130ND
Acenaphthylene mg/kg 1.32 67 31-130ND
Aniline mg/kg 1.02 55 10-130ND
Anthracene mg/kg 1.22 61 33-130ND
Benzo(a)anthracene mg/kg 1.32 66 32-130ND
Benzo(a)pyrene mg/kg 1.52 79 32-130ND
Benzo(b)fluoranthene mg/kg 1.52 78 33-130ND
Benzo(g,h,i)perylene mg/kg 1.52 79 28-130ND
Benzo(k)fluoranthene mg/kg 1.32 71 31-130ND
Benzoic Acid mg/kg 5.99.6 62 10-130ND
Benzyl alcohol mg/kg 2.33.8 59 31-130ND
bis(2-Chloroethoxy)methane mg/kg 1.22 62 30-130ND
bis(2-Chloroethyl) ether mg/kg 1.1 M125868-130ND
bis(2-Ethylhexyl)phthalate mg/kg 1.1 v325640-130ND
Butylbenzylphthalate mg/kg 1.32 70 40-130ND
Chrysene mg/kg 1.42 72 30-130ND
Di-n-butylphthalate mg/kg 1.22 62 41-130ND
Di-n-octylphthalate mg/kg 1.52 76 42-130ND
Dibenz(a,h)anthracene mg/kg 1.52 78 27-130ND
Dibenzofuran mg/kg 1.22 65 32-130ND
Diethylphthalate mg/kg 1.32 69 40-130ND
Dimethylphthalate mg/kg 1.42 74 37-130ND
Fluoranthene mg/kg 1.42 74 26-130ND
Fluorene mg/kg 1.32 65 31-130ND
Hexachloro-1,3-butadiene mg/kg 1.12 56 20-130ND
Hexachlorobenzene mg/kg 1.32 69 29-130ND
Hexachlorocyclopentadiene mg/kg 0.882 46 10-130ND
Hexachloroethane mg/kg 0.982 51 21-130ND
Indeno(1,2,3-cd)pyrene mg/kg 1.52 80 28-130ND
Isophorone mg/kg 1.22 63 32-130ND
N-Nitroso-di-n-propylamine mg/kg 1.02 53 31-130ND
N-Nitrosodimethylamine mg/kg 0.892 47 20-130ND
N-Nitrosodiphenylamine mg/kg 1.22 63 32-130ND
Naphthalene mg/kg 1.12 57 30-130ND
Nitrobenzene mg/kg 1.22 64 25-130ND
Pentachlorophenol mg/kg 2.53.8 65 10-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 62 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3758897MATRIX SPIKE SAMPLE:
MSSpike
Result
92623068001
Phenanthrene mg/kg 1.32 68 34-130ND
Phenol mg/kg 1.32 67 14-130ND
Pyrene mg/kg 1.42 72 31-130ND
Pyridine mg/kg ND2 20 10-130ND
2,4,6-Tribromophenol (S)%71 18-130
2-Fluorobiphenyl (S)%51 19-130
2-Fluorophenol (S)%61 18-130
Nitrobenzene-d5 (S)%60 21-130
Phenol-d6 (S)%59 18-130
Terphenyl-d14 (S)%65 15-130
Parameter Units
Dup
Result QualifiersRPDResult
92623540001
3758898SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene mg/kg NDND
1,2-Dichlorobenzene mg/kg NDND
1,3-Dichlorobenzene mg/kg NDND
1,4-Dichlorobenzene mg/kg NDND
1-Methylnaphthalene mg/kg NDND
2,2'-Oxybis(1-chloropropane)mg/kg NDND
2,4,5-Trichlorophenol mg/kg NDND
2,4,6-Trichlorophenol mg/kg NDND
2,4-Dichlorophenol mg/kg NDND
2,4-Dimethylphenol mg/kg NDND
2,4-Dinitrophenol mg/kg NDND
2,4-Dinitrotoluene mg/kg NDND
2,6-Dinitrotoluene mg/kg NDND
2-Chloronaphthalene mg/kg NDND
2-Chlorophenol mg/kg NDND
2-Methylnaphthalene mg/kg NDND
2-Methylphenol(o-Cresol)mg/kg NDND
2-Nitroaniline mg/kg NDND
2-Nitrophenol mg/kg NDND
3&4-Methylphenol(m&p Cresol)mg/kg NDND
3,3'-Dichlorobenzidine mg/kg NDND
3-Nitroaniline mg/kg NDND
4,6-Dinitro-2-methylphenol mg/kg NDND
4-Bromophenylphenyl ether mg/kg NDND
4-Chloro-3-methylphenol mg/kg NDND
4-Chloroaniline mg/kg NDND
4-Chlorophenylphenyl ether mg/kg NDND
4-Nitroaniline mg/kg NDND
4-Nitrophenol mg/kg NDND
Acenaphthene mg/kg NDND
Acenaphthylene mg/kg NDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 63 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92623540001
3758898SAMPLE DUPLICATE:
Aniline mg/kg NDND
Anthracene mg/kg NDND
Benzo(a)anthracene mg/kg NDND
Benzo(a)pyrene mg/kg NDND
Benzo(b)fluoranthene mg/kg NDND
Benzo(g,h,i)perylene mg/kg NDND
Benzo(k)fluoranthene mg/kg NDND
Benzoic Acid mg/kg NDND
Benzyl alcohol mg/kg NDND
bis(2-Chloroethoxy)methane mg/kg NDND
bis(2-Chloroethyl) ether mg/kg NDND
bis(2-Ethylhexyl)phthalate mg/kg ND v2ND
Butylbenzylphthalate mg/kg NDND
Chrysene mg/kg NDND
Di-n-butylphthalate mg/kg NDND
Di-n-octylphthalate mg/kg NDND
Dibenz(a,h)anthracene mg/kg NDND
Dibenzofuran mg/kg NDND
Diethylphthalate mg/kg NDND
Dimethylphthalate mg/kg NDND
Fluoranthene mg/kg NDND
Fluorene mg/kg NDND
Hexachloro-1,3-butadiene mg/kg NDND
Hexachlorobenzene mg/kg NDND
Hexachlorocyclopentadiene mg/kg NDND
Hexachloroethane mg/kg NDND
Indeno(1,2,3-cd)pyrene mg/kg NDND
Isophorone mg/kg NDND
N-Nitroso-di-n-propylamine mg/kg NDND
N-Nitrosodimethylamine mg/kg NDND
N-Nitrosodiphenylamine mg/kg NDND
Naphthalene mg/kg NDND
Nitrobenzene mg/kg NDND
Pentachlorophenol mg/kg NDND
Phenanthrene mg/kg NDND
Phenol mg/kg NDND
Pyrene mg/kg NDND
Pyridine mg/kg NDND
2,4,6-Tribromophenol (S)%6966
2-Fluorobiphenyl (S)%4644
2-Fluorophenol (S)%5251
Nitrobenzene-d5 (S)%5251
Phenol-d6 (S)%5049
Terphenyl-d14 (S)%7672
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 64 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
722163
MADEP EPH
MADEP EPH
MADEP EPH NC Soil
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92623480005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3762670
Associated Lab Samples:92623480005
Matrix:Solid
Analyzed
Aliphatic (C09-C18)mg/kg ND 10.1 N209/12/22 07:54
Aliphatic (C19-C36)mg/kg ND 10.1 N209/12/22 07:54
Aromatic (C11-C22)mg/kg ND 10.1 N209/12/22 07:54
1-Chlorooctadecane (S)%59 40-140 09/12/22 07:54
2-Bromonaphthalene (S)%80 40-140 09/12/22 07:54
2-Fluorobiphenyl (S)%74 40-140 09/12/22 07:54
o-Terphenyl (S)%68 40-140 09/12/22 07:54
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3762671LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
3762672
Aliphatic (C09-C18)mg/kg ND N210.2 49 40-14055ND 50
Aliphatic (C19-C36)mg/kg ND N213.6 68 40-14058ND 50
Aromatic (C11-C22)mg/kg 21.7 N228.8 75 40-1407521.1 3 50
1-Chlorooctadecane (S)%71 40-14084
2-Bromonaphthalene (S)%83 40-14083
2-Fluorobiphenyl (S)%84 40-14082
o-Terphenyl (S)%81 40-14076
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
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Huntersville, NC 28078
[phone]
Page 65 of 71
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
721106
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92623480001, 92623480002, 92623480003, 92623480004, 92623480005
Parameter Units
Dup
Result QualifiersRPDResult
92623288015
3757594SAMPLE DUPLICATE:
Percent Moisture %16.8 N21118.8
Parameter Units
Dup
Result QualifiersRPDResult
92623509001
3757595SAMPLE DUPLICATE:
Percent Moisture %20.8 N2221.3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
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Page 66 of 71
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.IK
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
Surrogate recovery not evaluated against control limits due to sample dilution.S4
Surrogate recovery outside control limits due to matrix interferences (not confirmed by re-analysis).S5
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
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Huntersville, NC 28078
[phone]
Page 67 of 71
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92623480
MT. HOPE CHURCH ROAD, MCLEANSV
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92623480005 722163 722602SB-1 MADEP EPH MADEP EPH
92623480005 721251 721287SB-1 MADEP VPH MADEP VPH
92623480006 721495 721583TW-1 EPA 3510C EPA 8270E
92623480007 721495 721583TW-2 EPA 3510C EPA 8270E
92623480008 721579 721754TW-3 EPA 3510C EPA 8270E
92623480001 721423 721487HA-1 EPA 3546 EPA 8270E
92623480002 721423 721487HA-2 EPA 3546 EPA 8270E
92623480003 721423 721487HA-3 EPA 3546 EPA 8270E
92623480004 721423 721487HA-4 EPA 3546 EPA 8270E
92623480005 721423 721487SB-1 EPA 3546 EPA 8270E
92623480001 721351 721544HA-1 EPA 5035A/5030B EPA 8260D
92623480002 721351 721544HA-2 EPA 5035A/5030B EPA 8260D
92623480003 721351 721544HA-3 EPA 5035A/5030B EPA 8260D
92623480004 721351 721544HA-4 EPA 5035A/5030B EPA 8260D
92623480005 721351 721544SB-1 EPA 5035A/5030B EPA 8260D
92623480006 722095TW-1 EPA 8260D
92623480007 722095TW-2 EPA 8260D
92623480008 722095TW-3 EPA 8260D
92623480001 721106HA-1 SW-846
92623480002 721106HA-2 SW-846
92623480003 721106HA-3 SW-846
92623480004 721106HA-4 SW-846
92623480005 721106SB-1 SW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/12/2022 03:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
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