WS-28517_47857_CA_IAR_20230124

Initial Abatement Action Report

Former Brown School
1125 Highland Avenue
Winston-Salem, North Carolina

DEQ UST Section Incident No. 47857
H&H Job No. MBS-001
January 24, 2023

C-1269 Engineering
#C-245 Geology
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Initial Abatement Action Report

A. Site Information
1. Site Identification
Date of Report: January 24, 2023
Facility ID: 00-0-0000035148 UST Incident Number: 47857
Site Name: Former Brown School
Site Street Address: 1125 Highland Avenue
City, Town: Winston-Salem_Zip Code: 27101 County: Forsyth
Description of Geographical Data Point: Former UST location
Location Method: Google Earth
Latitude: 36.1086 N Longitude: -80.2321 W
2. Information about Contacts Associated with the Leaking UST System
UST Owner: Shilohian-St. Peters Childcare
Address: Unknown Tel.: Unknown
UST Operator: same as above
Address: Tel.:
Property Owner: Housing Authority of Winston-Salem
Address: 500 W. 4th Street, Winston-Salem, NC 27101 Tel.: [phone]
Property Occupant: Vacant Address: Tel.:
Consultant/Contractor: Hart & Hickman, PC
Address: 2923 South Tryon Street, Suite 100, Charlotte, NC 28203
Tel.: [phone] (Attn: Bo Cappleman, PG)
Analytical Laboratory: Pace Analytical Services, LLC State Cert. No. 375
Address: 9800 Kinsey Ave, Suite 100, Huntersville, NC Tel.: [phone]
3. Information About Release
Date Discovered: March 10, 2014
Estimated Quantity of Release: Unknown
Cause of Release: Unknown
Source of Release: UST
Sizes and contents of UST system: One 20,000-gallon fuel oil UST
4. Certification
I, Robert Cappleman, PG, a Licensed Geologist at Hart & Hickman, PC, do certify that
the information contained in this report is correct and accurate to the best of my
knowledge.
Hart & Hickman, PC is licensed to practice geology/engineering in North Carolina. The
certification numbers of the company are C-245/C-1269.

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B. Site History and Characterization
1. UST Owner and Operator Information:
UST/AST ID No. UST-1 Facility ID Number 00-0-0000035148
Name of Owner Dates of Ownership
Shilohian-St. Peters Childcare Unknown
Street Address
Unknown
City State Zip Telephone Number
Winston-Salem NC Unknown Unknown
Name of Operator Dates of Operation
Same as above
Street Address

City State Zip Telephone Number

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3. Non-UST/AST spills at the site:
No non-underground storage tank (UST)/aboveground storage tank (AST)
petroleum spills are known to have occurred at the site.

4. Description of release:
In 2014, ECS Carolinas, LLP, performed a soil assessment to evaluate potential
impacts at the former 20,000-gallon fuel oil underground storage tank (UST) and
associated product piping. A petroleum release was confirmed on March 10,
2014, upon receipt of laboratory analytical data. Diesel-range total petroleum
hydrocarbons (TPH-DRO) were identified in samples GP-2 (15 ft) and GP-8 (5 ft)
at concentrations of 395 mg/kg and 416 mg/kg, respectively, which exceed the
current North Carolina Department of Environmental Quality (DEQ) UST Section
Action Level of 100 mg/kg. TPH-DRO was also detected in sample GP-7 at a
concentration of 14.1 mg/kg, which exceeded the former Action Level of
10 mg/kg but is below the current Action Level. No gasoline-range total
petroleum hydrocarbons (TPH-GRO) were detected in the soil samples collected
by ECS. The April 2014 Limited Soil Sampling Report prepared by ECS is
included in Appendix A, analytical data for samples GP-2, GP-7, and GP-8 are
included in Table 1, and the GP-2, GP-7, and GP-8 sample locations are shown on
Figure 3.

In March 2021, H&H performed Phase II Environmental Site Assessment (ESA)
activities to further evaluate soil impacts adjacent to the former UST basin and
associated the product line to the north of the UST. Soil samples SB-5 (5-6 ft)
and SB-5 (9-10 ft) were collected adjacent to the former product line, and soil
samples SB-6 (15-16 ft) and SB-6 (20-21 ft) were collected adjacent to the former
UST basin near prior sample GP-2. TPH-DRO and TPH-GRO were not detected
above the Action Levels in soil samples SB-5 or SB-6. Multiple polynuclear
aromatic hydrocarbons (PAHs) were detected in sample SB-5 (5-6 ft).
Specifically, benzo(a)pyrene (0.954 mg/kg) was detected above the Residential
Maximum Soil Contaminant Concentration (MSCC) of 0.66 mg/kg, and
benzo(a)anthracene (1.01 mg/kg), benzo(b)fluoranthene (1.14 mg/kg), 1-
methylnaphthalene (0.103 mg/kg), and naphthalene (0.203 mg/kg) were detected
above the respective Soil-to-Water MSCCs. Soil data for samples SB-5 and SB-6
are presented in Table 1, and SB-5 and SB-6 sample locations are shown on
Figure 3.

In June 2021, a 24-Hour Release and UST Leak Reporting Form (UST-61) was
submitted to the DEQ UST Section. DEQ established Incident No. 47857 for the
on-site fuel oil release. Subsequently, a Notice of Intent: UST Permanent Closure
or Change-in-Service (UST-3) form was submitted on July 13, 2022. Copies of
these forms are provided in Appendix B.

In July 2022, the 20,000-gallon fuel oil UST, the associated product line, and
petroleum-impacted soil near the UST system were removed from the subject
property. UST closure methodology, closure soil sampling results, impacted soil

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excavation, and post-excavation soil sampling results are described below.

5. Site characteristics:
The site is approximately 4.46 acres and was formerly developed with several
school buildings that were demolished in July 2022. The site is currently
comprised of cleared/graded land that is under development for a multi-family
residential complex. A site location map is presented as Figure 1, and a site map
is presented as Figure 2.

The subject site is located in the Milton Belt of the Piedmont Physiographic
Province of North Carolina. The area land surface is generally characterized as
gently sloping, which may become moderately steep where intersected by
streams. In the site area, underlying bedrock is comprised of predominantly
biotite gneiss and schist. In the Piedmont, the bedrock is overlain by a mantle of
weathered rock termed saprolite or residuum. The saprolite consists of
unconsolidated clay, silt, and sand with lesser amounts of rock fragments. Due to
the range of parent rock types and their variable susceptibility to weathering, the
saprolite ranges widely in color, texture, and thickness. Generally, the saprolite is
thickest near interstream divides and thins toward streambeds. In profile, the
saprolite normally grades from clayey soils near the land surface to highly
weathered rock above the competent bedrock.

The occurrence and movement of groundwater in the Piedmont is typically within
two separate but interconnected water-bearing zones. A shallow water-bearing
zone occurs within the saprolite, and a deeper water-bearing zone occurs within
the underlying bedrock. Groundwater in the shallow saprolite zone occurs in the
interstitial pore spaces between the grains comprising the saprolite soils.
Groundwater in this zone is typically under water table or unconfined conditions.
In general, groundwater migrates laterally from recharge areas to small streams
that serve as localized discharge points.

The occurrence and movement of groundwater in the underlying water-bearing
zone within the crystalline bedrock is controlled by secondary joints, fractures,
faults, and dikes within the bedrock. On a regional scale, the direction of
groundwater flow is typically from uplands to major streams and groundwater
sinks. The saprolite has a higher porosity than the bedrock and serves as a
reservoir that supplies water to a network of fractures in the bedrock.

Based on data collected by H&H during Phase II ESA field activities in February
2021, the water table at the Site is approximately 25 to 35 ft below ground surface
(bgs), and shallow groundwater flows to the southeast towards an unnamed
tributary of Brushy Fork. Groundwater was not encountered during UST closure
or over-excavation activities.

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6. Initial abatement actions, assessment activities, and corrective actions
performed to date:

As noted above, ECS and H&H identified petroleum-related soil impacts
adjacent to the UST basin and associated product line during assessment activities
in 2014 and 2021.

In July 2022, one 20,000-gallon fuel oil UST (UST-1) and the associated product
line were removed from the subject property by EVO Corporation (EVO) of
Winston-Salem, North Carolina. Based on the results of prior soil assessment at
the site and field evidence of impacted soils at the time of closure, soil over-
excavation activities were initiated following the UST system removal in
accordance with DEQ guidance. UST closure and soil over-excavation activities
are discussed further in Section D below.

C. Site Check Report
Not applicable.

D. UST Closure Report following UST-12 format and Site Investigation Report
for Permanent Closure or Change-in-Service of UST (UST-2 Form)

1. Preparations for closure including the steps taken to notify authorities,
permits obtained and the steps taken to clean and purge the tanks:
Prior to UST closure activities, EVO obtained a permit authorizing the UST
removal from the Winton-Salem Fire Marshal’s Office.

Prior to removal, residual #2 fuel oil was removed from the UST and associated
product piping using a vacuum truck. The interior of the UST was triple rinsed
using a pressure washer, and the rinse water was removed with a vacuum truck.
Approximately 115 total gallons of residual fluids and wash water were removed
from the UST and associated product piping.

Following residual fluids removal, the UST was purged of combustible vapors
with dry ice and tested with a combustible gas indicator to confirm that
potentially combustible vapors had dissipated.

2. Closure procedures:
Initially, soil was removed from the top and sides of the UST with a track hoe so
that the tank could be removed from the ground. Soils encountered during the
excavation were evaluated in the field for the presence of odors, staining, and
organic vapor readings with a calibrated photo-ionization detector (PID). The
PID was calibrated prior to its use against an isobutylene standard. Based on field
screening results, soil was either stockpiled for future haul-off to the EVO facility
or segregated for use as backfill.

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During UST removal, H&H observed that the UST was situated on a subgrade
concrete pad. No obvious damage or oil staining was observed on the concrete
pad. The UST was inspected for holes or other signs of structural damage. The
UST was single-walled and constructed of steel, and corrosion was observed on
the base and sides of the UST.

Subsurface product piping connected to the UST was also removed for proper
disposal. Product piping associated with the UST was constructed of steel. H&H
did not observe obvious visual evidence of damage to the underground product
piping.

3. Note the amount of residual material pumped from the tank and describes
the storage, sampling and disposal of the residual material and the disposal
of the tank, pumps and piping:
As stated above, EVO removed approximately 115 total gallons of residual fluids
and wash water from the UST and associated product piping. The fluids were
treated at the HOH Corporation facility in Winston-Salem, North Carolina. The
non-hazardous material manifest for the residual fluids is included in Appendix C.

The UST and product piping were transported off-site by EVO for recycling at
Foss Recycling in Winston-Salem, North Carolina. The tank disposal certificate
for the UST is included in Appendix C.

4. Initial response actions and initial abatement actions:
Initial response and abatement actions are discussed in the following section.

5. Soil excavation and Site Investigation activities:
After removal of the UST and product piping, twelve closure soil samples (T-1
through T-12) were collected from the perimeter of the subgrade concrete pad,
and three soil samples (PL-1 through PL-3) were collected below the former
product line in accordance with DEQ guidelines. The closure samples were
analyzed for TPH-GRO and TPH-DRO by EPA Method 8015C.

The analytical results for the closure soil samples indicated the presence of TPH-
DRO above the DEQ Action Level of 100 mg/kg in sample T-9 (221 mg/kg),
which was collected from the southeastern portion of the UST excavation. TPH-
GRO was not detected above the laboratory method detection limits in any of the
UST closure samples.

Due to the identification of soil impacts, approximately 244.57 tons of impacted
soil were excavated from below the UST and product piping. The excavated soil
was transported to EVO’s treatment facility in Winston-Salem, North Carolina. A
copy of the certificate of disposal, non-hazardous waste manifests, and certified
weight tickets for the excavated soil are provided in Appendix C.

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Field evidence of petroleum-related soil impacts was observed adjacent to the
east, south, and west of the southern portion of the UST and associated concrete
pad. Field evidence of petroleum-related soil impacts was also observed along
the north-central portion of the product piping. Therefore, impacted soil was
excavated from these areas. Due to the presence of the concrete pad beneath the
UST, no soil impacts were identified in soil beneath the pad.

Following over-excavation activities along the southern portion of the UST basin,
four base samples and three sidewall samples were collected from the excavation.
The excavation along the southern portion of the UST basin sloped from north to
south based on field screening results. Due to the negligible depth of excavation
on the north side of the UST excavation area, no sidewall samples were collected
from the north side of the excavation. In addition, one base sample and four
sidewall samples were collected from the piping excavation. In accordance with
DEQ guidance, the post-excavation soil samples were analyzed for volatile
organic compounds (VOCs) by EPA Method 8260D, semi-VOCs (SVOCs) by
EPA Method 8270E, and extractable petroleum hydrocarbons (EPH) and volatile
petroleum hydrocarbons (VPH) using the Massachusetts Department of
Environmental Protection (MADEP) Methods.

EPH and at least one VOC were detected in all post-excavation soil samples.
However, the detected concentrations are below the DEQ Soil-to-Water,
Residential, and Industrial/Commercial MSCCs. VPH and SVOCs were not
detected above laboratory detection limits in any post-excavation soil samples.

UST closure and post-excavation soil sampling results are presented in Tables 1
and 2, respectively. UST closure soil sample locations are depicted on Figure 3,
and the excavation areas and post-excavation soil sample locations are depicted
on Figure 4. Laboratory analytical sheets are included in Appendix D.

Following soil removal, the excavations were backfilled with imported backfill
material from the Vulcan Materials North Quarry in Winston-Salem, North
Carolina and excess soil generated during on-site grading activities. The imported
backfill material consisted primarily of brown sandy silts.

E. Free Product Investigation and Recovery Report
Not applicable.

F. Groundwater and Surface Water Investigation
Not applicable.

G. Initial Response and Abatement Activities
See Section B.

H. Excavation of Contaminated Soil
See Section D.

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I. Conclusions and Recommendations:
In July 2022, one 20,000-gallon fuel oil UST and associated product piping were
removed from the subject property. Approximately 244.57 total tons of petroleum-
impacted soils were excavated from below the tank and product piping.

Results of post-excavation confirmation soil sampling did not indicate the presence
of VOCs, SVOCs, EPH, or VPH at concentrations above the DEQ Soil-to-Water,
Residential, or Industrial/Commercial MSCCs.

Based on the results of the Initial Abatement Action activities, impacted soil has
been adequately removed from along the former UST basin and associated product
line. As such, H&H recommends that DEQ issue a Notice of No Further Action for
the release incident.

Table 1Summary of Soil Analytical Results - Due Diligence and UST Closure SamplesFormer Brown School1125 Highland AvenueWinston-Salem, North CarolinaH&H Job No. MBS-001Sample ID GP-2 GP-7 GP-8 PL-1 PL-2 PL-3Sample Location UST BasinDepth (ft bgs) 15 5 5 5-6 9-10 15-16 20-21 1 - 1.5 1 - 1.5 1 - 1.5Date 3/5/2014 3/5/2014 3/5/2014 7/19/2022 7/19/2022 7/19/2022TPH (8015C)Diesel Range Organics (C10-C28)39514.14165.89 J 3.16 J 4.51 J 2.64 J5.3 J 18.3 13.8 100 -- -- --Gasoline Range Organics (C6-C10) <10 <10 <10 0.440 J 0.494 J 0.461 J 0.336 J<1.7 <1.9 <1.750 -- -- --VOCs (8260D)-- -- --- --SVOCs (8270E/8270C SIM)AcenaphtheneNA NA NA0.234 J<0.020 <0.018 <0.017NA NA NA--8.3 93014,000AnthraceneNA NA NA0.394 J<0.010 <0.008 <0.008NA NA NA--640 4,60070,000Benzo(a)anthraceneNA NA NA1.01<0.010 <0.009 <0.009NA NA NA--0.17 6.632Benzo(a)pyreneNA NA NA0.954<0.008 <0.007 <0.006NA NA NA--0.058 0.663.2Benzo(b)fluorantheneNA NA NA1.14<0.008 <0.007 <0.007NA NA NA--0.6 6.632Benzo(g,h,i)peryleneNA NA NA0.466 J<0.008 <0.007 <0.007NA NA NA--7,600 4697,000Benzo(k)fluorantheneNA NA NA0.484 J<0.009 <0.008 <0.008NA NA NA--5.8 66327ChryseneNA NA NA1.09<0.010 <0.009 <0.009NA NA NA--18 6633,270Dibenz(a,h)anthraceneNA NA NA0.038 J<0.026 <0.023 <0.022NA NA NA--0.19 0.6603.27DibenzofuranNA NA NA0.234 J<0.024 <0.021 <0.021NA NA NA--5.2 15.6233FluorantheneNA NA NA2.68<0.0010 <0.009 <0.008NA NA NA--330 6259,340FluoreneNA NA NA0.267 J<0.019 <0.017 <0.017NA NA NA--55 6259,340Indeno(1,2,3-cd)pyreneNA NA NA0.538 J<0.025 <0.022 <0.021NA NA NA--1.9 6.6332.71-MethylnaphthaleneNA NA NA0.103 J<0.013 <0.012 <0.011NA NA NA--0.054 22.81122-MethylnaphthaleneNA NA NA0.109 J<0.017 <0.015 <0.015NA NA NA--1.5 62.5934NaphthaleneNA NA NA0.203 J<0.019 <0.017 <0.016NA NA NA--0.2 5.527PhenanthreneNA NA NA2.77<0.009 <0.008 <0.008NA NA NA--64 4697,000PyreneNA NA NA2.30<0.013 <0.011 <0.011NA NA NA--210 4697,000EPH/VPH (MADEP)C5-C8 Aliphatics (VPH)NA NA NA<2.01 <2.53 <1.94 <1.87NA NA NA--68 6259,340C9-C12 Aliphatics (VPH)NA NA NA<0.895 <1.12 <0.865 <0.832NA NA NA--NE NENEC9-C18 Aliphatics (EPH)NA NA NA<3.09 <3.34 <3.06 <2.92NA NA NA--540 1,56023,300Total C9-C18 Aliphatics NA NA NA<3.09 <3.34 <3.06 <2.92NA NA NA--540 1,56023,300C9-C10 Aromatics (VPH)NA NA NA<0.956 <1.20 <0.924 <0.888NA NA NA--NE NENEC11-C22 Aromatics (EPH)NA NA NA<16.8 <18.2 <16.7 <16.0NA NA NA--NE NENETotal C9-C22 Aromatics NA NA NA<17.8 <19.4 <17.6 <16.9NA NA NA--31 4697,000C19-C36 Aliphatics (EPH)NA NA NA<10.4 <11.2 11.9 J <9.82NA NA NA--Immobile 31,200467,000Notes:1) NC Department of Environmental Quality (DEQ) Division of Waste Management (DWM) Underground Storage Tank (UST) Section Action Levels (July 2016)2) DEQ UST Section Maximum Soil Contaminant Concentrations (MSCCs) dated October 2021Soil concentrations are reported in milligrams per kilogram (mg/kg).Compound concentrations are reported to the laboratory method detection limits.Bold values exceed a DEQ Action Level or Soil-to-Water MSCC.Underlined values exceed the DEQ Residential MSCC.Only those compounds detected in at least one sample shown aboveLaboratory analytical methods are shown in parenthesesSamples GP-2, GP-7, and GP-8 were collected during a soil assessment performed by ECS Southeast, LLP in March 2014.Samples SB-5 and SB-6 were collected during a Phase II Environmental Site Assessment performed by H&H in February 2021.UST = underground storage tank; TPH = total petroleum hydrocarbons; ft bgs= feet below ground surface;J = Estimated concentration that is above the laboratory method detection limit but below the laboratory reporting limitSB-6SB-5All Below Laboratory Method Detection LimitsAction Level (1)Soil-to-Water MSCCs (2)Residential MSCCs (2)Industrial/ Commercial MSCCs (2)Product Line UST BasinProduct Line2/26/2021 2/25/2021Product Linehttps://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/McCormack Baron Salazar (MBS)/MBS‐001 Brown School/Task 9 ‐ UST Removal and Soil Excavation/Initial Abatement Action Report/Data Table_ABM11/21/2022Table 1 (Page 1 of 2)Hart & Hickman, PC
Table 1Summary of Soil Analytical Results - Due Diligence and UST Closure SamplesFormer Brown School1125 Highland AvenueWinston-Salem, North CarolinaH&H Job No. MBS-001Sample ID T-1 T-2 T-3 T-4 T-5 T-6 T-7 T-8 T-9 T-10 T-11 T-12Sample LocationDepth (ft bgs) 151515151515151515151515Date 7/20/2022 7/20/2022 7/20/2022 7/20/2022 7/20/2022 7/20/2022 7/20/2022 7/20/2022 7/20/2022 7/20/2022 7/20/2022 7/20/2022TPH (8015C)Diesel Range Organics (C10-C28)5.8<4.4 <4.2 <4.4 <4.8 <5.3 <4.3 <4.422110.5 4.5 J<4.3100 -- -- --Gasoline Range Organics (C6-C10)<2.2 <3.0 <2.4<2.8 <3.0 <2.9<2.6 <2.6 <2.2<2.3 <2.5 <2.750 -- -- --VOCs (8260D)-- -- --- --SVOCs (8270E/8270C SIM)AcenaphtheneNA NA NA NA NA NA NA NA NA NA NA NA--8.3 93014,000AnthraceneNA NA NA NA NA NA NA NA NA NA NA NA--640 4,60070,000Benzo(a)anthraceneNA NA NA NA NA NA NA NA NA NA NA NA--0.17 6.632Benzo(a)pyreneNA NA NA NA NA NA NA NA NA NA NA NA--0.058 0.663.2Benzo(b)fluorantheneNA NA NA NA NA NA NA NA NA NA NA NA--0.6 6.632Benzo(g,h,i)peryleneNA NA NA NA NA NA NA NA NA NA NA NA--7,600 4697,000Benzo(k)fluorantheneNA NA NA NA NA NA NA NA NA NA NA NA--5.8 66327ChryseneNA NA NA NA NA NA NA NA NA NA NA NA--18 6633,270Dibenz(a,h)anthraceneNA NA NA NA NA NA NA NA NA NA NA NA--0.19 0.6603.27DibenzofuranNA NA NA NA NA NA NA NA NA NA NA NA--5.2 15.6233FluorantheneNA NA NA NA NA NA NA NA NA NA NA NA--330 6259,340FluoreneNA NA NA NA NA NA NA NA NA NA NA NA--55 6259,340Indeno(1,2,3-cd)pyreneNA NA NA NA NA NA NA NA NA NA NA NA--1.9 6.6332.71-MethylnaphthaleneNA NA NA NA NA NA NA NA NA NA NA NA--0.054 22.81122-MethylnaphthaleneNA NA NA NA NA NA NA NA NA NA NA NA--1.5 62.5934NaphthaleneNA NA NA NA NA NA NA NA NA NA NA NA--0.2 5.527PhenanthreneNA NA NA NA NA NA NA NA NA NA NA NA--64 4697,000PyreneNA NA NA NA NA NA NA NA NA NA NA NA--210 4697,000EPH/VPH (MADEP)C5-C8 Aliphatics (VPH)NA NA NA NA NANANA NA NA NA NANA--68 6259,340C9-C12 Aliphatics (VPH)NA NA NA NA NANANA NA NA NA NANA--NE NENEC9-C18 Aliphatics (EPH)NA NA NA NA NANANA NA NA NA NANA--540 1,56023,300Total C9-C18 Aliphatics NA NA NA NA NANANA NA NA NA NANA--540 1,56023,300C9-C10 Aromatics (VPH)NA NA NA NA NANANA NA NA NA NANA--NE NENEC11-C22 Aromatics (EPH)NA NA NA NA NANANA NA NA NA NANA--NE NENETotal C9-C22 Aromatics NA NA NA NA NANANA NA NA NA NANA--31 4697,000C19-C36 Aliphatics (EPH)NA NA NA NA NANANA NA NA NA NANA--Immobile 31,200467,000Notes:1) NC Department of Environmental Quality (DEQ) Division of Waste Management (DWM) Underground Storage Tank (UST) Section Action Levels (July 2016)2) DEQ UST Section Maximum Soil Contaminant Concentrations (MSCCs) dated October 2021Soil concentrations are reported in milligrams per kilogram (mg/kg).Compound concentrations are reported to the laboratory method detection limits.Bold values exceed a DEQ Action Level or Soil-to-Water MSCC.Underlined values exceed the DEQ Residential MSCC.Only those compounds detected in at least one sample shown aboveLaboratory analytical methods are shown in parenthesesSamples GP-2, GP-7, and GP-8 were collected during a soil assessment performed by ECS Southeast, LLP in March 2014.Samples SB-5 and SB-6 were collected during a Phase II Environmental Site Assessment performed by H&H in February 2021.UST = underground storage tank; TPH = total petroleum hydrocarbons; ft bgs= feet below ground surface;J = Estimated concentration that is above the laboratory method detection limit but below the laboratory reporting limitAll Below Laboratory Method Detection LimitsUnderground Storage TankAction Level (1)Soil-to-Water MSCCs (2)Residential MSCCs (2)Industrial/ Commercial MSCCs (2)https://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/McCormack Baron Salazar (MBS)/MBS‐001 Brown School/Task 9 ‐ UST Removal and Soil Excavation/Initial Abatement Action Report/Data Table_ABM11/21/2022Table 1 (Page 2 of 2)Hart & Hickman, PC
Table 2Summary of UST Risk-Based Analytical ResultsFormer Brown School1125 Highland AvenueWinston-Salem, North CarolinaH&H Job No. MBS-001Sample ID PL-BASE PL-N PL-E PL-S PL-W EXC-BASE-1 EXC-BASE-2 EXC-BASE-3 EXC-BASE-4 EXC-SIDE-1 EXC-SIDE-2 EXC-SIDE-3Sample LocationProduct Line Excavation - BaseProduct Line Excavation - North SidewallProduct Line Excavation - East SidewallProduct Line Excavation - South SidewallProduct Line Excavation - West SidewallUST Excavation - Base NorthwestUST Excavation - Base NortheastUST Excavation - Base SouthwestUST Excavation - Base SoutheastUST Excavation - West SidewallUST Excavation - East SidewallUST Excavation - South SidewallDepth (ft bgs) 121212121217171717141414Date 7/19/2022 7/19/2022 7/19/2022 7/19/2022 7/19/2022 7/20/2022 7/20/2022 7/20/2022 7/20/2022 7/20/2022 7/20/2022 7/20/2022EPH/VPH by MADEP MethodC5-C8 Aliphatics (VPH)<3.0 <2.7 <2.6<2.6 <3.0 <3.0<3.1 <2.9 <2.9<3.5 <3.3 <3.168 625 9,340C9-C12 Aliphatics (VPH)<3.0 <2.7 <2.6<2.6 <3.0 <3.0<3.1 <2.9 <2.9<3.5 <3.3 <3.1NE NE NEC9-C18 Aliphatics (EPH)<3.02 <3.05 <2.64 <3.20 <3.052.84 J<2.9417.8<2.70 <3.31 <3.09 <2.86540 1,560 23,300Total C9-C18 AliphaticsND ND ND ND ND2.84 JND17.8ND ND ND ND540 1,560 23,300C19-C36 Aliphatics (EPH)3.54 J 3.29 J 3.50 J 3.45 J 5.69 J<2.835.46 J 10.4 3.20 J 4.91 J 4.40 J 4.05 J NE 31,200 467,000C9-C10 Aromatics (VPH)<3.0 <2.7 <2.6<2.6 <3.0 <3.0<3.1 <2.9 <2.9<3.5 <3.3 <3.1NE NE NEC11-C22 Aromatics (EPH)3.49 J 3.65 J 3.95 J<3.204.80 J 4.13 J 3.05 J 10.1 2.97 J 3.84 J 4.68 J 3.84 J NE NE NETotal C9-C22 Aromatics 3.49 J 3.65 J 3.95 JND4.80 J 4.13 J 3.05 J 10.1 2.97 J 3.84 J 4.68 J 3.84 J 31 469 7,000C19-C36 Aliphatics (EPH)3.54 J 3.29 J 3.50 J 3.45 J 5.69 J<2.835.46 J 10.4 3.20 J 4.91 J 4.40 J 4.05 J Immobile 31,200 467,000VOCs by EPA Method 8260DAcetoneND ND ND519ND<0.0602<0.0461<0.0435 <0.0417 <0.0474 <0.0462 <0.046124 14,000 210,0002-Butanone (MEK) 0.055 J 0.069 J 0.0476 J 1.46 0.0752 J0.0966 J0.0789 J 0.0880 J 0.0702 J 0.0792 J 0.0776 J 0.0809 J 16 9,380 140,000EthylbenzeneND0.004 J 0.0042 J 0.0052 J 0.0060 J<0.0044<0.0033 <0.0332 <0.0030 <0.0034 <0.0034 <0.00338 60.3 297TolueneND ND0.0068ND ND<0.0027<0.0020 <0.0019 <0.0018 <0.0021 <0.0020 <0.00205.4 1,250 18,600m&p-XyleneND0.0070 J 0.0105 JND0.0078 J<0.0064<0.0049 <0.0046 <0.0044 <0.0050 <0.0049 <0.00496 3,120 46,700o-XyleneND0.0062 J 0.0082 0.0055 J 0.0092<0.0041<0.0032 <0.0030 <0.0029 <0.0033 <0.0032 <0.00326 3,120 46,700SVOCs by EPA Method 8270EAll BDL All BDL All BDL All BDL All BDL All BDL All BDL All BDL All BDL All BDL All BDL All BDL-- -- --Notes:1) North Carolina Department of Environmental Quality (DEQ) Underground Storage Tank (UST) Maximum Soil Contaminant Concentrations (MSCCs) dated October 2021.Soil concentrations are reported in milligrams per kilogram (mg/kg).Compound concentrations are reported to the laboratory method detection limits.Only VOC compounds detected in at least one sample are shown above.EPH = extractable petroleum hydrocarbons; VPH = volatile petroleum hydrocarbons; MADEP = Massachusetts Department of Environmental ProtectionVOCs = volatile organic compounds; SVOCs = semi-volatile organic compoundsft bgs= feet below ground surface; NE = not established; BDL = below laboratory method detection limits; ND = not detected; -- = not applicableJ = Estimated concentration that is above the laboratory method detection limit but below the laboratory reporting limit Residential MSCCs (1)Soil-to-Water MSCCs (1)Industrial MSCCs (1)https://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/McCormack Baron Salazar (MBS)/MBS‐001 Brown School/Task 9 ‐ UST Removal and Soil Excavation/Initial Abatement Action Report/Data Table_ABM11/21/2022Table 2 (Page 1 of 1)Hart & Hickman, PC
USGS The National Map: National Boundaries Dataset, 3DEP ElevationProgram, Geographic Names Information System, National HydrographyDataset, National Land Cover Database, National Structures Dataset,and National Transportation Dataset; USGS Global Ecosystems; U.S.Census Bureau TIGER/Line data; USFS Road Data; Natural Earth Data;U.S. Department of State Humanitarian Information Unit; and NOAANational Centers for Environmental Information, U.S. Coastal ReliefModel. Data refreshed May, 2020.
SITE LOCATION MAP
FORMER BROWN SCHOOL1125 HIGHLAND AVENUEWINSTON-SALEM, NORTH CAROLINA
DATE: 12-8-20
JOB NO: MBS-001
REVISION NO: 0
FIGURE NO: 1
2923 South Tryon Street - Suite 100Charlotte, North Carolina 28203704-586-0007 (p) 704-586-0373 (f)License # C-1269 / # C-245 Geology
TITLE
PROJECT
0 2,000 4,000
SCALE IN FEET
SITE
Path: \\HHFS01\Redirectedfolders\sperry\My Documents\ArcGIS\PROJECTS\MBS-001\Figure-1_ArcMap.mxdN
U.S.G.S. QUADRANGLE MAP
WINSTON-SALEM EAST, NORTH CAROLINA 2013
QUADRANGLE7.5 MINUTE SERIES (TOPOGRAPHIC)
REVISION NO. 0
JOB NO. MBS-001
DATE: 12-8-20
FIGURE NO. 2
FORMER BROWN SCHOOL
1125 HIGHLAND AVENUE
WINSTON-SALEM, NORTH CAROLINA
SITE MAP
LEGEND
SITE PROPERTY BOUNDARY
PARCEL BOUNDARY
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 Geology
EAST 11TH STREET
EAST 12TH STREET
HIGHLAND AVENUENORTH CLEVELAND AVENUEFORMER CLASSROOM BUILDING(DEMOLISHED 2022)
FORMER CLASSROOM TRAILERS
(DEMOLISHED 2022)
NOTES:
1. PARCEL DATA OBTAINED FROM FORSYTH COUNTY
GIS, 2020.
2. AERIAL IMAGERY OBTAINED FROM NC ONEMAP, 2019.
APARTMENTS
(1151 E. 11TH STREET)
ST. JOHNS BAPTIST CHURCH
(1200 N. CLEVELAND AVENUE)
RESIDENTIAL RESIDENTIALVACANT LAND
AND PARKING LOT
SHILOH BAPTIST CHURCH
(916 E. 12TH STREET)
PARKING
LOT
JOHN F. KENNEDY HIGH SCHOOL
(890 E. 11TH STREET)
BEST CHOICE CENTER
(1031 HIGHLAND AVENUE)
APARTMENTS
(1070 E. 11TH STREET)S:\AAA-Master Projects\McCormack Baron Salazar (MBS)\Task 1 - Phase I ESA\Figures\SITE MAP.dwg, FIG.2, 12/8/2020 1:05:42 PM, sperryFORMER WOODLAND AVENUE NEFORMER 20-000-GALLON FUEL OIL UST
SB-5
FORMER WOODLAND AVENUE NEGP-7
GP-8 PL-3
PL-2
PL-1
T-4
T-3
T-2
T-1
T-7
T-6T-5
T-8
T-9
T-10
T-12 T-11
GP-2
REVISION NO. 0
JOB NO. MBS-001
DATE: 10-26-22
FIGURE NO. 3
FORMER BROWN SCHOOL
1125 HIGHLAND AVENUE
WINSTON-SALEM, NORTH CAROLINA
DUE DILIGENCE AND UST CLOSURE
SAMPLE LOCATION MAP
LEGEND
SITE PROPERTY BOUNDARY
PARCEL BOUNDARY
APPROXIMATE LOCATION OF
BURNED SCHOOL BUILDINGS
CHAIN-LINK FENCE
APPROXIMATE UST LOCATION
APPROXIMATE LOCATION OF
FORMER PRODUCT PIPING
UST CLOSURE SOIL SAMPLES
DUE DILIGENCE SOIL SAMPLES
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
NOTES:
1. PARCEL DATA OBTAINED FROM FORSYTH COUNTY GIS, 2020.
2. AERIAL IMAGERY OBTAINED FROM NC ONEMAP, 2019.
3. UST = UNDERGROUND STORAGE TANK
4. SB-5 SOIL SAMPLE COLLECTED DURING FEBRUARY AND
MARCH, 2021 PHASE II ESA PERFORMED BY H&H. GP-2, GP-7,
AND GP-8 COLLECTED DURING APRIL 2014 LIMITED SOIL
SAMPLING PERFORMED BY ECS CARLINAS, LLP.S:\AAA-Master Projects\McCormack Baron Salazar (MBS)\MBS-001 Brown School\Task 9 - UST Removal and Soil Excavation\Figures\SITE MAP 20221025.dwg, UST FIG 3, 11/9/2022 10:41:02 AM, shaynesSB-6
PL-W
PL-S
PL-N
PL-E
PL-BASE
EXC-SIDE-1
EXC-BASE-1 EXC-BASE-2
EXC-SIDE-3
EXC-BASE-4EXC-BASE-3
EXC-SIDE-2
REVISION NO. 0
JOB NO. MBS-001
DATE: 10-26-22
FIGURE NO. 4
FORMER BROWN SCHOOL
1125 HIGHLAND AVENUE
WINSTON-SALEM, NORTH CAROLINA
POST-EXCAVATION SAMPLE LOCATION MAP
LEGEND
SITE PROPERTY BOUNDARY
PARCEL BOUNDARY
APPROXIMATE LOCATION OF
BURNED SCHOOL BUILDINGS
CHAIN-LINK FENCE
APPROXIMATE UST LOCATION
APPROXIMATE LOCATION OF
FORMER PRODUCT PIPING
UST AND PRODUCT LINE
EXCAVATION AREA
AREA OF OVER-EXCAVATION
POST-EXCAVATION SOIL
SAMPLES
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
NOTES:
1. PARCEL DATA OBTAINED FROM FORSYTH COUNTY GIS, 2020.
2. AERIAL IMAGERY OBTAINED FROM NC ONEMAP, 2019.
3. UST = UNDERGROUND STORAGE TANK
FORMER WOODLAND AVENUE NES:\AAA-Master Projects\McCormack Baron Salazar (MBS)\MBS-001 Brown School\Task 9 - UST Removal and Soil Excavation\Figures\SITE MAP 20221025.dwg, UST FIG 4, 11/9/2022 11:08:49 AM, shaynes

Appendix A

Report of Limited Soil Sampling prepared by ECS Carolinas, LLP
(April 14, 2014)

Appendix B

24-Hour Release and UST Leak Reporting form (UST-61)
UST-61 24-Hour Release and UST Leak Reporting Form.
For Releases
in NC
This form should be completed and submitted to the UST Section’s regional office following a known or suspected release from
an underground storage tank (UST) system. This form is required to be submitted within 24 hours of discovery of a known or
suspected release
(DWM USE ONLY)
Incident # ________ Risk (H,I,L,U)_______
Received On ________ Received By ________
Reported by (circle one): Phone, Fax or Report
Region _______
Suspected Contamination? (Y/N) ________
Confirmed GW Contamination? (Y/N) ______
Confirmed Soil Contamination ?(Y/N) ______
Samples Taken?(Y/N) ______
Free Product? (Y/N) _____ If Yes, State Greatest
Thickness ______________
Facility ID Number ______________
Date Leak Discovered ___________
Comm/Non-Commercial? ________
Reg/Non-regulated? _____________
INCIDENT DESCRIPTION
Incident Name:
Address: County:
City/Town: Zip Code: Regional Office (circle one): Asheville, Mooresville, Fayetteville,
Raleigh, Washington, Wilmington, Winston-Salem
Latitude (decimal degrees): Longitude (decimal degrees) : Obtained by:
Briefly describe suspected or confirmed release: (including but not limited to: nature of release, date of release, amount
of release, amount of free product present and recovery efforts, initial responses conducted, impacts to receptors)  GPS
 Topographic map
 GIS Address matching
 Other
 Unknown
Describe location:
HOW RELEASE WAS DISCOVERED (Release Code)
(Check one)
 Release Detection Equipment or Methods
 During UST Closure/Removal
 Property Transfer
 Visual/Odor
 Water in Tank
 Water Supply Well Contamination
 Groundwater Contamination
 Surface Water Contamination
 Other (specify) _______________
SOURCE OF CONTAMINATION
Source of Release (Check primary source) Cause of Release (Check primary cause) Type of Release (Check one) Product Type Released (Check primary product type released)
 Tank
 Piping
 Dispenser
 Submersible Turbine Pump
 Delivery Problem
 Spill Bucket
 Other
 Unknown
Definitions presented on reverse
 Spill
 Overfill
 Corrosion
 Physical/Mechanical
Damage
 Install Problem
 Other
 Unknown
Definitions presented on reverse
 Petroleum
 Non-Petroleum
 Both
Location
(Check one)
 Facility
 Residence
 Other
 Gasoline/ Diesel/
Kerosene
 Heating Oil
 Other Petroleum
Products
 Metals
 Other Inorganics
 Other Organics
 Diesel/Veg. Oil
Blend
 Vegetable Oil 100%
 E10 – E20
 E21 – E84
 E85 – E99
 Ethanol 100%
 E01 – E09
Ownership
1. Municipal 2. Military 3. Unknown 4. Private 5. Federal 6. County 7. State
Operation Type
1. Public Service 2. Agricultural 3. Residential 4. Education/Relig. 5. Industrial 6. Commercial 7. Mining
UST Form 61 (02/19) Page 1 of 2
(Former)
IMPACT ON DRINKING WATER SUPPLIES
Water Supply Wells Affected? 1. Yes 2. No 3. Unknown
Number of Water Supply Wells Affected __________________
Water Supply Wells Contaminated: (Include Users Names, Addresses and Phone Numbers. Attach additional sheet if necessary)
1.
2.
3.
UST SYSTEM OWNER
UST Owner/Company
Point of Contact Address
City State Zip Code Telephone Number
UST SYSTEM OPERATOR
UST Operator/Company Address
City State Zip Code Telephone Number
LANDOWNER AT LOCATION OF UST INCIDENT
Landowner Address
City State Zip Code Telephone Number
Draw Sketch of Area (showing two major road intersections) or Attach Map
Person Reporting Incident Company Telephone Number
Title Address Date
UST Form 61 (02/19) Page 2 of 2
Definitions of Sources Tank: means the tank that stores the product and is part of the underground storage tank system Piping: means the piping and connectors running from the tank or submersible turbine pump to the dispenser or other end-use equipment (Vent, vapor recovery, or fill lines are excluded.) Dispenser: includes the dispenser and the equipment used to connect the dispenser to the piping (e.g., a release from a suction pump or from components located above the shear valve) Submersible Turbine Pump (STP) Area includes the submersible turbine pump head (typically located in the tank sump), the line leak detector, and the piping that connects the submersible turbine pump to the tank Delivery Problem: identifies releases that occurred during product delivery to the tank. (Typical causes associated with this source are spills and overfills.)
Other: serves as the option to use when the release source is known but does not fit into one of the preceding categories (e.g., for releases from vent lines, vapor recovery lines, and fill lines) Unknown: identifies releases for which the source has not been determined
Definitions of Causes
Spill: use this cause when a spill occurs (e.g., when the delivery hose is disconnected from the tank fill pipe or when the nozzle is removed from the dispenser) Overfill: use when an overfill occurs (e.g., overfills may occur from the fill pipe at the tank or when the nozzle fails to shut off at the dispenser) Physical or Mechanical Damage: use for all types of physical or mechanical damage, except corrosion (e.g., puncture of tank or piping, loose fittings, broken components, and components that have changed dimension) Corrosion: use when a metal tank, piping, or other component has a release due to corrosion (e.g., for steel, corrosion takes the form of rust) Installation Problem: use when the problem is determined to have occurred specifically because the UST system was not installed properly Other: use this option when the cause is known but does not fit into one of the preceding categories (e.g., putting regulated substances into monitoring wells) Unknown: use when the cause has not been determined
UST-3 Notice of Intent: UST Permanent Closure or Change-in-Service
Return completed form to:
The DWM Regional Office located in the area where the facility is located. Also send a copy to the Central Office in Raleigh.
SEE MAP ON THE BACK OF THIS FORM FOR THE CENTRAL AND REGIONAL OFFICE ADDRESSES.
STATE USE ONLY
I.D. #_____________________
Date Received______________
INSTRUCTIONS (READ THIS FIRST)
Complete and return a UST-3 form at least thirty (30) days prior to closure or change-in-service activities.
Completed UST closure or change-in-service site assessment reports, along with a copy of the UST-2A and/or 2B forms, should be submitted
to the appropriate Division of Waste Management (DWM) Regional Office within thirty (30) days following closure activities. The UST-2 form
should also be submitted to the Central Office in Raleigh so that the status of the tanks may be changed to permanently closed and your
tank fee account can be closed out.Note: Tank fees may be due for unregistered tanks.
UST closure and change-in-service site assessments must be completed in accordance with the latest version of the Guidelines for Site
Checks, Tank Closure and Initial Response. The guidelines can be obtained at https://deq.nc.gov/about/divisions/waste-management/ust.
Note: To close tanks in place you must obtain prior approval from the DWM Regional office located in the region where the facility is located.
You must make sure that USTs removed from your property are disposed of properly. When choosing a closure contractor, ask where the
tank(s) will be taken for disposal. Usually, USTs are cleaned and cut up for scrap metal. This is dangerous work and must be performed
by a qualified company. Tanks disposed of illegally in fields or other dumpsites can leak petroleum products and sludge into the environment.
If your tanks are disposed of improperly, you could be held responsible for the cleanup of any environmental damage that occurs.
I. OWNERSHIP OF TANKS II. LOCATION
Owner Name (Corporation, Individual, Public Agency, or Other Entity) Facility Name or Company
Street Address Facility ID # (If known)
City County Street Address
State Zip Code City County Zip Code
Phone Number Email Phone Number
III. CONTACT PERSONNEL
Name:Company Name:Job Title: Phone Number:
IV. TANK REMOVAL, CLOSURE IN PLACE, CHANGE-IN SERVICE
1.Contact local fire marshal.
2.Plan entire closure event.
3.Conduct Site Soil Assessment.
4. If removing tanks or closing in place, refer to
API Publication 2015 Cleaning Petroleum
Storage Tanks and 1604 Removal and
Disposal of Used Underground Petroleum
Storage Tanks.
5.Provide a sketch locating piping, tanks and
soil sampling locations.
6. Submit a closure report in the format of UST-
12 (including the form UST-2) within thirty
(30) days following the site investigation.
7. If a release from the tanks has occurred, the
site assessment portion of the tank closure
must be conducted under the supervision of
a P.E. or L.G., with all closure site assessment
reports bearing the signature and seal of the
P.E. or L.G. If a release has not occurred, the
supervision, signature or seal of a P.E. or L.G.
is not required.
8.Keep closure records for three (3) years.
V. WORK TO BE PERFORMED BY
Contractor Name:Contractor Company Name:
Address:State: Zip Code:Phone No:
Primary Consultant Name:Primary Consultant Company Name:Consultant Phone No:
VI. TANKS SCHEDULED FOR CLOSURE OR CHANGE-IN-SERVICE
Tank ID No.Size in Gallons Last Contents
Proposed Activity
Closure Change-In-Service
Removal Abandonment in Place *New Contents Stored
*Prior written approval to abandon a tank in place must be received from a DWM Regional Office.
VII. OWNER OR OWNER’S AUTHORIZED REPRESENTATIVE
Has a release from a UST system occurred at this location? Yes No Unknown
I understand that I can be held responsible for environmental damage resulting from the improper disposal of my USTs.
Print name and official title:
Signature Date Signed SCHEDULED REMOVAL DATE Notify your DWM Regional Office
48 hours before this date if
scheduled removal date changes
UST-3 Rev 2/2021
e and official title:
evvvvvvvvvvvvvvvvvvvvvvvvvvvvvvvvvv 2222222222/20211111
Shilohian St. Peters Childcare
Unknown
Unknown Unknown
Unknown
Unknown Unknown
Former Brown School
00-0-0000035148
1125 Highland Avenue
Winston-Salem Guilford 27101
N/A
Bo Cappleman Project ManagerHart & Hickman, PC 704-586-0007
Tony Disher Evo Corporation
1703 Vargrave Street 27107 877-725-5844
Bo Cappleman Hart & Hickman, PC
NC
704-586-0007
1 20,000 fuel oil ■
Jerry Stone, Vice President; WS CNI Phase 1, LP; By: WS CNI Phase 1 MBS GP, Inc., its General Partner
7/13/2022 7/18/2022
■

Appendix C

Certificate of Disposal and Non-Hazardous Waste Manifests, and Weight Tickets

Appendix D

Laboratory Analytical Report
#=CL#
August 10, 2022
LIMS USE: FR - BO CAPPLEMAN
LIMS OBJECT ID: 92616378
92616378
Project:
Pace Project No.:
RE:
Bo Cappleman
Hart & Hickman
2923 South Tryon Street
Charlotte, NC 28203
MBS.001
Dear Bo Cappleman:
Enclosed are the analytical results for sample(s) received by the laboratory on July 22, 2022. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Charlotte
Report revised 8/10/22 to include EPH re-run results for PL-S (12).
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
1(704)875-9092
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 125
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92616378
MBS.001
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Virginia Certification #: VT2006
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 125
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92616378
MBS.001
Lab ID Sample ID Matrix Date Collected Date Received
92616378001 PL-1 (1-1.5)Solid 07/19/22 11:25 07/22/22 08:40
92616378002 PL-2 (1-1.5)Solid 07/19/22 11:30 07/22/22 08:40
92616378003 PL-3 (1-1.5)Solid 07/19/22 11:35 07/22/22 08:40
92616378004 T-1 (15)Solid 07/20/22 14:30 07/22/22 08:40
92616378005 T-2 (15)Solid 07/20/22 14:55 07/22/22 08:40
92616378006 T-3 (15)Solid 07/20/22 14:20 07/22/22 08:40
92616378007 T-4 (15)Solid 07/20/22 16:40 07/22/22 08:40
92616378008 T-5 (15)Solid 07/20/22 17:05 07/22/22 08:40
92616378009 T-6 (15)Solid 07/20/22 16:58 07/22/22 08:40
92616378010 T-7 (15)Solid 07/20/22 16:48 07/22/22 08:40
92616378011 T-8 (15)Solid 07/20/22 14:15 07/22/22 08:40
92616378012 T-9 (15)Solid 07/20/22 14:50 07/22/22 08:40
92616378013 T-10 (15)Solid 07/20/22 14:25 07/22/22 08:40
92616378014 T-11 (15)Solid 07/20/22 14:35 07/22/22 08:40
92616378015 T-12 (15)Solid 07/20/22 14:45 07/22/22 08:40
92616378016 EXC-BASE-1 Solid 07/20/22 15:55 07/22/22 08:40
92616378017 EXC-BASE-2 Solid 07/20/22 16:02 07/22/22 08:40
92616378018 EXC-BASE-3 Solid 07/20/22 16:08 07/22/22 08:40
92616378019 EXC-BASE-4 Solid 07/20/22 16:16 07/22/22 08:40
92616378020 EXC-SIDE-1 Solid 07/20/22 16:22 07/22/22 08:40
92616378021 EXC-SIDE-2 Solid 07/20/22 16:30 07/22/22 08:40
92616378022 EXC-SIDE-3 Solid 07/20/22 16:37 07/22/22 08:40
92616378023 PL-BASE (12)Solid 07/19/22 16:45 07/22/22 08:40
92616378024 PL-N (12)Solid 07/19/22 16:30 07/22/22 08:40
92616378025 PL-S (12)Solid 07/19/22 16:35 07/22/22 08:40
92616378026 PL-E (12)Solid 07/19/22 16:40 07/22/22 08:40
92616378027 PL-W (12)Solid 07/19/22 16:40 07/22/22 08:40
92616378028 EXTRA T-2 (15)Solid 07/19/22 14:20 07/22/22 08:40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 125
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92616378
MBS.001
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92616378001 PL-1 (1-1.5)EPA 8015C 2 PASI-CAP2
EPA 8015C 2 PASI-CCL
SW-846 1 PASI-CKDF
92616378002 PL-2 (1-1.5)EPA 8015C 2 PASI-CAP2
EPA 8015C 2 PASI-CCL
SW-846 1 PASI-CKDF
92616378003 PL-3 (1-1.5)EPA 8015C 2 PASI-CAP2
EPA 8015C 2 PASI-CCL
SW-846 1 PASI-CKDF
92616378004 T-1 (15)EPA 8015C 2 PASI-CAP2
EPA 8015C 2 PASI-CCL
SW-846 1 PASI-CKDF
92616378005 T-2 (15)EPA 8015C 2 PASI-CAP2
EPA 8015C 2 PASI-CCL
SW-846 1 PASI-CKDF
92616378006 T-3 (15)EPA 8015C 2 PASI-CAP2
EPA 8015C 2 PASI-CCL
SW-846 1 PASI-CKDF
92616378007 T-4 (15)EPA 8015C 2 PASI-CAP2
EPA 8015C 2 PASI-CCL
SW-846 1 PASI-CKDF
92616378008 T-5 (15)EPA 8015C 2 PASI-CAP2
EPA 8015C 2 PASI-CCL
SW-846 1 PASI-CKDF
92616378009 T-6 (15)EPA 8015C 2 PASI-CAP2
EPA 8015C 2 PASI-CCL
SW-846 1 PASI-CKDF
92616378010 T-7 (15)EPA 8015C 2 PASI-CAP2
EPA 8015C 2 PASI-CCL
SW-846 1 PASI-CKDF
92616378011 T-8 (15)EPA 8015C 2 PASI-CAP2
EPA 8015C 2 PASI-CCL
SW-846 1 PASI-CKDF
92616378012 T-9 (15)EPA 8015C 2 PASI-CAP2
EPA 8015C 2 PASI-CCL
SW-846 1 PASI-CKDF
92616378013 T-10 (15)EPA 8015C 2 PASI-CAP2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 125
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92616378
MBS.001
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 8015C 2 PASI-CCL
SW-846 1 PASI-CKDF
92616378014 T-11 (15)EPA 8015C 2 PASI-CAP2
EPA 8015C 2 PASI-CCL
SW-846 1 PASI-CKDF
92616378015 T-12 (15)EPA 8015C 2 PASI-CAP2
EPA 8015C 2 PASI-CTEG
SW-846 1 PASI-CKDF
92616378016 EXC-BASE-1 MADEP EPH 8 PANDMG
MADEP VPH 5 PASI-CTEG
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
92616378017 EXC-BASE-2 MADEP EPH 8 PANDMG
MADEP VPH 5 PASI-CTEG
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
92616378018 EXC-BASE-3 MADEP EPH 8 PANDMG
MADEP VPH 5 PASI-CTEG
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
92616378019 EXC-BASE-4 MADEP EPH 8 PANDMG
MADEP VPH 5 PASI-CTEG
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
92616378020 EXC-SIDE-1 MADEP EPH 8 PANDMG
MADEP VPH 5 PASI-CTEG
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 125
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92616378
MBS.001
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
SM 2540G 1 PANCMK
92616378021 EXC-SIDE-2 MADEP EPH 8 PANDMG
MADEP VPH 5 PASI-CTEG
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
92616378022 EXC-SIDE-3 MADEP EPH 8 PANDMG
MADEP VPH 5 PASI-CTEG
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
92616378023 PL-BASE (12)MADEP EPH 8 PANDMG
MADEP VPH 5 PASI-CTEG
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
92616378024 PL-N (12)MADEP EPH 8 PANDMG
MADEP VPH 5 PASI-CTEG
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
92616378025 PL-S (12)MADEP EPH 8 PANDMG
MADEP VPH 5 PASI-CTEG
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
92616378026 PL-E (12)MADEP EPH 8 PANDMG
MADEP VPH 5 PASI-CTEG
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 125
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92616378
MBS.001
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92616378027 PL-W (12)MADEP EPH 8 PANDMG
MADEP VPH 5 PASI-CTEG
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
PAN = Pace National - Mt. Juliet
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:PL-1 (1-1.5)Lab ID:92616378001 Collected:07/19/22 11:25 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)5.3J mg/kg 07/27/22 13:4207/27/22 03:495.5 3.9 1
Surrogates
n-Pentacosane (S)80 %07/27/22 13:42 629-99-207/27/22 03:4910-130 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 07/25/22 16:4107/25/22 12:296.0 1.7 1
Surrogates
4-Bromofluorobenzene (S)105 %07/25/22 16:41 460-00-407/25/22 12:2966-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 10.1 %07/25/22 14:35 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:PL-2 (1-1.5)Lab ID:92616378002 Collected:07/19/22 11:30 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)18.3 mg/kg 07/27/22 13:4207/27/22 03:495.7 4.0 1
Surrogates
n-Pentacosane (S)74 %07/27/22 13:42 629-99-207/27/22 03:4910-130 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 07/25/22 17:3307/25/22 12:296.7 1.9 1
Surrogates
4-Bromofluorobenzene (S)104 %07/25/22 17:33 460-00-407/25/22 12:2966-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 12.1 %07/25/22 14:35 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:PL-3 (1-1.5)Lab ID:92616378003 Collected:07/19/22 11:35 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)13.8 mg/kg 07/27/22 13:5907/27/22 03:495.5 3.9 1
Surrogates
n-Pentacosane (S)77 %07/27/22 13:59 629-99-207/27/22 03:4910-130 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 07/25/22 17:5907/25/22 12:296.1 1.7 1
Surrogates
4-Bromofluorobenzene (S)104 %07/25/22 17:59 460-00-407/25/22 12:2966-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 9.4 %07/25/22 14:35 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:T-1 (15)Lab ID:92616378004 Collected:07/20/22 14:30 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)5.8 mg/kg 07/27/22 13:5907/27/22 03:495.6 4.0 1
Surrogates
n-Pentacosane (S)64 %07/27/22 13:59 629-99-207/27/22 03:4910-130 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 07/25/22 18:2407/25/22 12:297.8 2.2 1
Surrogates
4-Bromofluorobenzene (S)103 %07/25/22 18:24 460-00-407/25/22 12:2966-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 11.6 %07/25/22 14:35 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:T-2 (15)Lab ID:92616378005 Collected:07/20/22 14:55 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 07/27/22 14:1707/27/22 03:496.2 4.4 1
Surrogates
n-Pentacosane (S)60 %07/27/22 14:17 629-99-207/27/22 03:4910-130 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 07/25/22 18:5007/25/22 12:2910.8 3.0 1
Surrogates
4-Bromofluorobenzene (S)104 %07/25/22 18:50 460-00-407/25/22 12:2966-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 19.9 %07/25/22 14:35 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:T-3 (15)Lab ID:92616378006 Collected:07/20/22 14:20 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 07/27/22 14:1707/27/22 03:495.9 4.2 1
Surrogates
n-Pentacosane (S)60 %07/27/22 14:17 629-99-207/27/22 03:4910-130 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 07/25/22 19:1607/25/22 12:298.5 2.4 1
Surrogates
4-Bromofluorobenzene (S)104 %07/25/22 19:16 460-00-407/25/22 12:2966-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 16.7 %07/25/22 14:35 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:T-4 (15)Lab ID:92616378007 Collected:07/20/22 16:40 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 07/27/22 14:3407/27/22 03:496.2 4.4 1
Surrogates
n-Pentacosane (S)59 %07/27/22 14:34 629-99-207/27/22 03:4910-130 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 07/25/22 19:4207/25/22 12:2910.1 2.8 1
Surrogates
4-Bromofluorobenzene (S)105 %07/25/22 19:42 460-00-407/25/22 12:2966-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 20.1 %07/25/22 14:51 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:T-5 (15)Lab ID:92616378008 Collected:07/20/22 17:05 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 07/27/22 14:3407/27/22 03:496.8 4.8 1
Surrogates
n-Pentacosane (S)62 %07/27/22 14:34 629-99-207/27/22 03:4910-130 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 07/25/22 20:0707/25/22 12:2910.8 3.0 1
Surrogates
4-Bromofluorobenzene (S)105 %07/25/22 20:07 460-00-407/25/22 12:2966-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 27.1 %07/25/22 14:51 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:T-6 (15)Lab ID:92616378009 Collected:07/20/22 16:58 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 07/27/22 14:5207/27/22 03:497.4 5.3 1
Surrogates
n-Pentacosane (S)72 %07/27/22 14:52 629-99-207/27/22 03:4910-130 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 07/25/22 20:3307/25/22 12:2910.5 2.9 1
Surrogates
4-Bromofluorobenzene (S)105 %07/25/22 20:33 460-00-407/25/22 12:2966-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 32.7 %07/25/22 14:51 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:T-7 (15)Lab ID:92616378010 Collected:07/20/22 16:48 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 07/27/22 14:5207/27/22 03:496.1 4.3 1
Surrogates
n-Pentacosane (S)67 %07/27/22 14:52 629-99-207/27/22 03:4910-130 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 07/25/22 20:5907/25/22 12:299.6 2.6 1
Surrogates
4-Bromofluorobenzene (S)102 %07/25/22 20:59 460-00-407/25/22 12:2966-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 18.5 %07/25/22 14:51 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:T-8 (15)Lab ID:92616378011 Collected:07/20/22 14:15 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 07/27/22 15:1007/27/22 03:496.3 4.4 1
Surrogates
n-Pentacosane (S)65 %07/27/22 15:10 629-99-207/27/22 03:4910-130 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 07/25/22 21:2407/25/22 12:299.5 2.6 1
Surrogates
4-Bromofluorobenzene (S)108 %07/25/22 21:24 460-00-407/25/22 12:2966-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 20.3 %07/25/22 14:51 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:T-9 (15)Lab ID:92616378012 Collected:07/20/22 14:50 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)221 mg/kg 07/27/22 15:1007/27/22 03:495.8 4.1 1
Surrogates
n-Pentacosane (S)66 %07/27/22 15:10 629-99-207/27/22 03:4910-130 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 07/25/22 21:5007/25/22 12:297.9 2.2 1
Surrogates
4-Bromofluorobenzene (S)104 %07/25/22 21:50 460-00-407/25/22 12:2966-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 14.0 %07/25/22 14:51 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:T-10 (15)Lab ID:92616378013 Collected:07/20/22 14:25 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)10.5 mg/kg 07/27/22 15:2807/27/22 03:496.0 4.3 1
Surrogates
n-Pentacosane (S)57 %07/27/22 15:28 629-99-207/27/22 03:4910-130 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 07/25/22 22:1607/25/22 12:298.5 2.3 1
Surrogates
4-Bromofluorobenzene (S)103 %07/25/22 22:16 460-00-407/25/22 12:2966-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 17.0 %07/25/22 14:52 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:T-11 (15)Lab ID:92616378014 Collected:07/20/22 14:35 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)4.5J mg/kg 07/27/22 15:2807/27/22 03:496.0 4.3 1
Surrogates
n-Pentacosane (S)64 %07/27/22 15:28 629-99-207/27/22 03:4910-130 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 07/25/22 22:4207/25/22 12:299.1 2.5 1
Surrogates
4-Bromofluorobenzene (S)106 %07/25/22 22:42 460-00-407/25/22 12:2966-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 17.7 %07/25/22 14:52 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:T-12 (15)Lab ID:92616378015 Collected:07/20/22 14:45 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 07/27/22 15:4607/27/22 03:496.0 4.3 1
Surrogates
n-Pentacosane (S)65 %07/27/22 15:46 629-99-207/27/22 03:4910-130 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 07/27/22 18:2607/27/22 13:389.6 2.7 1
Surrogates
4-Bromofluorobenzene (S)111 %07/27/22 18:26 460-00-407/27/22 13:3866-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 17.4 %07/25/22 14:52 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:EXC-BASE-1 Lab ID:92616378016 Collected:07/20/22 15:55 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP EPH Preparation Method: MA DEP/NJ DEP
Pace National - Mt. Juliet
TPH by Method MADEPE
Aliphatic (C09-C18)2.84J mg/kg 08/04/22 18:56 B,J08/02/22 15:258.47 2.83 1
Aliphatic (C19-C36)ND mg/kg 08/04/22 18:5608/02/22 15:258.47 2.83 1
Aromatic (C11-C22)4.13J mg/kg 08/04/22 21:32 B,J08/02/22 15:258.47 2.83 1
Total Extractable Hydrocarbons 6.97J mg/kg 08/04/22 21:32 TPH-TEH B,J08/02/22 15:258.47 2.83 1
Surrogates
o-Terphenyl (S)64.8 %08/04/22 21:32 84-15-108/02/22 15:2540.0-140 1
1-Chloro-octadecane (S)57.6 %08/04/22 18:56 3386-33-208/02/22 15:2540.0-140 1
2-Fluorobiphenyl (S)81.6 %08/04/22 21:32 321-60-808/02/22 15:2540.0-140 1
2-Bromonaphthalene (S)78.2 %08/04/22 21:32 580-13-208/02/22 15:2540.0-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Pace Analytical Services - Charlotte
VPH NC Soil
Aliphatic (C05-C08)ND mg/kg 07/23/22 00:53 N207/22/22 18:223.0 3.0 1
Aliphatic(C09-C12) Adjusted ND mg/kg 07/23/22 00:53 N207/22/22 18:223.0 3.0 1
Aromatic (C09-C10)ND mg/kg 07/23/22 00:53 N207/22/22 18:223.0 3.0 1
Surrogates
4-Bromofluorobenzene (FID) (S)102 %07/23/22 00:53 460-00-407/22/22 18:2270-130 1
4-Bromofluorobenzene (PID) (S)89 %07/23/22 00:53 460-00-407/22/22 18:2270-130 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 07/28/22 09:49 83-32-907/27/22 03:473871361
Acenaphthylene ND ug/kg 07/28/22 09:49 208-96-807/27/22 03:473871361
Aniline ND ug/kg 07/28/22 09:49 62-53-307/27/22 03:473871511
Anthracene ND ug/kg 07/28/22 09:49 120-12-707/27/22 03:473871271
Benzo(a)anthracene ND ug/kg 07/28/22 09:49 56-55-307/27/22 03:473871291
Benzo(a)pyrene ND ug/kg 07/28/22 09:49 50-32-807/27/22 03:473871341
Benzo(b)fluoranthene ND ug/kg 07/28/22 09:49 205-99-207/27/22 03:473871291
Benzo(g,h,i)perylene ND ug/kg 07/28/22 09:49 191-24-207/27/22 03:473871501
Benzo(k)fluoranthene ND ug/kg 07/28/22 09:49 207-08-907/27/22 03:473871361
Benzoic Acid ND ug/kg 07/28/22 09:49 65-85-007/27/22 03:4719308311
Benzyl alcohol ND ug/kg 07/28/22 09:49 100-51-607/27/22 03:477742931
4-Bromophenylphenyl ether ND ug/kg 07/28/22 09:49 101-55-307/27/22 03:473871491
Butylbenzylphthalate ND ug/kg 07/28/22 09:49 85-68-707/27/22 03:473871631
4-Chloro-3-methylphenol ND ug/kg 07/28/22 09:49 59-50-707/27/22 03:477742721
4-Chloroaniline ND ug/kg 07/28/22 09:49 106-47-807/27/22 03:477743041
bis(2-Chloroethoxy)methane ND ug/kg 07/28/22 09:49 111-91-107/27/22 03:473871611
bis(2-Chloroethyl) ether ND ug/kg 07/28/22 09:49 111-44-407/27/22 03:473871451
2-Chloronaphthalene ND ug/kg 07/28/22 09:49 91-58-707/27/22 03:473871541
2-Chlorophenol ND ug/kg 07/28/22 09:49 95-57-807/27/22 03:473871451
4-Chlorophenylphenyl ether ND ug/kg 07/28/22 09:49 7005-72-307/27/22 03:473871441
Chrysene ND ug/kg 07/28/22 09:49 218-01-907/27/22 03:473871411
Dibenz(a,h)anthracene ND ug/kg 07/28/22 09:49 53-70-307/27/22 03:473871491
Dibenzofuran ND ug/kg 07/28/22 09:49 132-64-907/27/22 03:473871391
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:EXC-BASE-1 Lab ID:92616378016 Collected:07/20/22 15:55 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
1,2-Dichlorobenzene ND ug/kg 07/28/22 09:49 95-50-107/27/22 03:473871391
1,3-Dichlorobenzene ND ug/kg 07/28/22 09:49 541-73-107/27/22 03:473871371
1,4-Dichlorobenzene ND ug/kg 07/28/22 09:49 106-46-707/27/22 03:473871481
3,3'-Dichlorobenzidine ND ug/kg 07/28/22 09:49 91-94-107/27/22 03:477742611
2,4-Dichlorophenol ND ug/kg 07/28/22 09:49 120-83-207/27/22 03:473871511
Diethylphthalate ND ug/kg 07/28/22 09:49 84-66-207/27/22 03:473871421
2,4-Dimethylphenol ND ug/kg 07/28/22 09:49 105-67-907/27/22 03:473871611
Dimethylphthalate ND ug/kg 07/28/22 09:49 131-11-307/27/22 03:473871411
Di-n-butylphthalate ND ug/kg 07/28/22 09:49 84-74-207/27/22 03:473871301
4,6-Dinitro-2-methylphenol ND ug/kg 07/28/22 09:49 534-52-107/27/22 03:477743611
2,4-Dinitrophenol ND ug/kg 07/28/22 09:49 51-28-507/27/22 03:47193012001
2,4-Dinitrotoluene ND ug/kg 07/28/22 09:49 121-14-207/27/22 03:473871491
2,6-Dinitrotoluene ND ug/kg 07/28/22 09:49 606-20-207/27/22 03:473871421
Di-n-octylphthalate ND ug/kg 07/28/22 09:49 117-84-007/27/22 03:473871521
bis(2-Ethylhexyl)phthalate ND ug/kg 07/28/22 09:49 117-81-707/27/22 03:473871501
Fluoranthene ND ug/kg 07/28/22 09:49 206-44-007/27/22 03:473871321
Fluorene ND ug/kg 07/28/22 09:49 86-73-707/27/22 03:473871361
Hexachloro-1,3-butadiene ND ug/kg 07/28/22 09:49 87-68-307/27/22 03:473871681
Hexachlorobenzene ND ug/kg 07/28/22 09:49 118-74-107/27/22 03:473871511
Hexachlorocyclopentadiene ND ug/kg 07/28/22 09:49 77-47-407/27/22 03:473872221
Hexachloroethane ND ug/kg 07/28/22 09:49 67-72-107/27/22 03:473871481
Indeno(1,2,3-cd)pyrene ND ug/kg 07/28/22 09:49 193-39-507/27/22 03:473871521
Isophorone ND ug/kg 07/28/22 09:49 78-59-107/27/22 03:473871721
1-Methylnaphthalene ND ug/kg 07/28/22 09:49 90-12-007/27/22 03:473871361
2-Methylnaphthalene ND ug/kg 07/28/22 09:49 91-57-607/27/22 03:473871551
2-Methylphenol(o-Cresol)ND ug/kg 07/28/22 09:49 95-48-707/27/22 03:473871581
3&4-Methylphenol(m&p Cresol)ND ug/kg 07/28/22 09:49 15831-10-407/27/22 03:473871561
Naphthalene ND ug/kg 07/28/22 09:49 91-20-307/27/22 03:473871311
2-Nitroaniline ND ug/kg 07/28/22 09:49 88-74-407/27/22 03:4719303161
3-Nitroaniline ND ug/kg 07/28/22 09:49 99-09-207/27/22 03:4719303041
4-Nitroaniline ND ug/kg 07/28/22 09:49 100-01-607/27/22 03:477742941
Nitrobenzene ND ug/kg 07/28/22 09:49 98-95-307/27/22 03:473871791
2-Nitrophenol ND ug/kg 07/28/22 09:49 88-75-507/27/22 03:473871681
4-Nitrophenol ND ug/kg 07/28/22 09:49 100-02-707/27/22 03:4719307481
N-Nitrosodimethylamine ND ug/kg 07/28/22 09:49 62-75-907/27/22 03:473871301
N-Nitroso-di-n-propylamine ND ug/kg 07/28/22 09:49 621-64-707/27/22 03:473871451
N-Nitrosodiphenylamine ND ug/kg 07/28/22 09:49 86-30-607/27/22 03:473871371
2,2'-Oxybis(1-chloropropane)ND ug/kg 07/28/22 09:49 108-60-107/27/22 03:473871841
Pentachlorophenol ND ug/kg 07/28/22 09:49 87-86-507/27/22 03:477743791
Phenanthrene ND ug/kg 07/28/22 09:49 85-01-807/27/22 03:473871271
Phenol ND ug/kg 07/28/22 09:49 108-95-207/27/22 03:473871721
Pyrene ND ug/kg 07/28/22 09:49 129-00-007/27/22 03:473871571
Pyridine ND ug/kg 07/28/22 09:49 110-86-107/27/22 03:473871221
1,2,4-Trichlorobenzene ND ug/kg 07/28/22 09:49 120-82-107/27/22 03:473871521
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:EXC-BASE-1 Lab ID:92616378016 Collected:07/20/22 15:55 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,4,5-Trichlorophenol ND ug/kg 07/28/22 09:49 95-95-407/27/22 03:473871771
2,4,6-Trichlorophenol ND ug/kg 07/28/22 09:49 88-06-207/27/22 03:473871591
Surrogates
Nitrobenzene-d5 (S)61 %07/28/22 09:49 4165-60-007/27/22 03:4721-130 1
2-Fluorobiphenyl (S)58 %07/28/22 09:49 321-60-807/27/22 03:4719-130 1
Terphenyl-d14 (S)76 %07/28/22 09:49 1718-51-007/27/22 03:4715-130 1
Phenol-d6 (S)58 %07/28/22 09:49 13127-88-307/27/22 03:4718-130 1
2-Fluorophenol (S)60 %07/28/22 09:49 367-12-407/27/22 03:4718-130 1
2,4,6-Tribromophenol (S)69 %07/28/22 09:49 118-79-607/27/22 03:4718-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 07/26/22 16:19 67-64-107/25/22 16:0018860.2 1
Benzene ND ug/kg 07/26/22 16:19 71-43-207/25/22 16:009.4 3.7 1
Bromobenzene ND ug/kg 07/26/22 16:19 108-86-107/25/22 16:009.4 3.1 1
Bromochloromethane ND ug/kg 07/26/22 16:19 74-97-507/25/22 16:009.4 2.8 1
Bromodichloromethane ND ug/kg 07/26/22 16:19 75-27-407/25/22 16:009.4 3.6 1
Bromoform ND ug/kg 07/26/22 16:19 75-25-207/25/22 16:009.4 3.3 1
Bromomethane ND ug/kg 07/26/22 16:19 74-83-9 IK,v107/25/22 16:0018.8 14.8 1
2-Butanone (MEK)96.6J ug/kg 07/26/22 16:19 78-93-3 C707/25/22 16:0018845.0 1
n-Butylbenzene ND ug/kg 07/26/22 16:19 104-51-807/25/22 16:009.4 4.4 1
sec-Butylbenzene ND ug/kg 07/26/22 16:19 135-98-807/25/22 16:009.4 4.1 1
tert-Butylbenzene ND ug/kg 07/26/22 16:19 98-06-607/25/22 16:009.4 3.3 1
Carbon tetrachloride ND ug/kg 07/26/22 16:19 56-23-507/25/22 16:009.4 3.5 1
Chlorobenzene ND ug/kg 07/26/22 16:19 108-90-707/25/22 16:009.4 1.8 1
Chloroethane ND ug/kg 07/26/22 16:19 75-00-307/25/22 16:0018.8 7.2 1
Chloroform ND ug/kg 07/26/22 16:19 67-66-307/25/22 16:009.4 5.7 1
Chloromethane ND ug/kg 07/26/22 16:19 74-87-307/25/22 16:0018.8 7.9 1
2-Chlorotoluene ND ug/kg 07/26/22 16:19 95-49-807/25/22 16:009.4 3.3 1
4-Chlorotoluene ND ug/kg 07/26/22 16:19 106-43-407/25/22 16:009.4 1.7 1
1,2-Dibromo-3-chloropropane ND ug/kg 07/26/22 16:19 96-12-8 IK07/25/22 16:009.4 3.6 1
Dibromochloromethane ND ug/kg 07/26/22 16:19 124-48-107/25/22 16:009.4 5.3 1
1,2-Dibromoethane (EDB)ND ug/kg 07/26/22 16:19 106-93-407/25/22 16:009.4 4.1 1
Dibromomethane ND ug/kg 07/26/22 16:19 74-95-307/25/22 16:009.4 2.0 1
1,2-Dichlorobenzene ND ug/kg 07/26/22 16:19 95-50-107/25/22 16:009.4 3.4 1
1,3-Dichlorobenzene ND ug/kg 07/26/22 16:19 541-73-107/25/22 16:009.4 2.9 1
1,4-Dichlorobenzene ND ug/kg 07/26/22 16:19 106-46-707/25/22 16:009.4 2.4 1
Dichlorodifluoromethane ND ug/kg 07/26/22 16:19 75-71-8 IH07/25/22 16:0018.8 4.1 1
1,1-Dichloroethane ND ug/kg 07/26/22 16:19 75-34-307/25/22 16:009.4 3.9 1
1,2-Dichloroethane ND ug/kg 07/26/22 16:19 107-06-207/25/22 16:009.4 6.2 1
1,1-Dichloroethene ND ug/kg 07/26/22 16:19 75-35-407/25/22 16:009.4 3.9 1
cis-1,2-Dichloroethene ND ug/kg 07/26/22 16:19 156-59-207/25/22 16:009.4 3.2 1
trans-1,2-Dichloroethene ND ug/kg 07/26/22 16:19 156-60-507/25/22 16:009.4 3.3 1
1,2-Dichloropropane ND ug/kg 07/26/22 16:19 78-87-507/25/22 16:009.4 2.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:EXC-BASE-1 Lab ID:92616378016 Collected:07/20/22 15:55 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,3-Dichloropropane ND ug/kg 07/26/22 16:19 142-28-907/25/22 16:009.4 2.9 1
2,2-Dichloropropane ND ug/kg 07/26/22 16:19 594-20-7 v207/25/22 16:009.4 3.1 1
1,1-Dichloropropene ND ug/kg 07/26/22 16:19 563-58-607/25/22 16:009.4 4.5 1
cis-1,3-Dichloropropene ND ug/kg 07/26/22 16:19 10061-01-507/25/22 16:009.4 2.6 1
trans-1,3-Dichloropropene ND ug/kg 07/26/22 16:19 10061-02-607/25/22 16:009.4 3.2 1
Diisopropyl ether ND ug/kg 07/26/22 16:19 108-20-307/25/22 16:009.4 2.5 1
Ethylbenzene ND ug/kg 07/26/22 16:19 100-41-407/25/22 16:009.4 4.4 1
Hexachloro-1,3-butadiene ND ug/kg 07/26/22 16:19 87-68-307/25/22 16:0018.8 15.3 1
2-Hexanone ND ug/kg 07/26/22 16:19 591-78-607/25/22 16:0093.8 9.0 1
Isopropylbenzene (Cumene)ND ug/kg 07/26/22 16:19 98-82-807/25/22 16:009.4 3.2 1
p-Isopropyltoluene ND ug/kg 07/26/22 16:19 99-87-607/25/22 16:009.4 4.6 1
Methylene Chloride ND ug/kg 07/26/22 16:19 75-09-207/25/22 16:0037.5 25.7 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 07/26/22 16:19 108-10-107/25/22 16:0093.8 9.0 1
Methyl-tert-butyl ether ND ug/kg 07/26/22 16:19 1634-04-407/25/22 16:009.4 3.5 1
Naphthalene ND ug/kg 07/26/22 16:19 91-20-3 v207/25/22 16:009.4 4.9 1
n-Propylbenzene ND ug/kg 07/26/22 16:19 103-65-107/25/22 16:009.4 3.3 1
Styrene ND ug/kg 07/26/22 16:19 100-42-507/25/22 16:009.4 2.5 1
1,1,1,2-Tetrachloroethane ND ug/kg 07/26/22 16:19 630-20-607/25/22 16:009.4 3.6 1
1,1,2,2-Tetrachloroethane ND ug/kg 07/26/22 16:19 79-34-507/25/22 16:009.4 2.5 1
Tetrachloroethene ND ug/kg 07/26/22 16:19 127-18-407/25/22 16:009.4 3.0 1
Toluene ND ug/kg 07/26/22 16:19 108-88-307/25/22 16:009.4 2.7 1
1,2,3-Trichlorobenzene ND ug/kg 07/26/22 16:19 87-61-6 IK,v207/25/22 16:009.4 7.6 1
1,2,4-Trichlorobenzene ND ug/kg 07/26/22 16:19 120-82-107/25/22 16:009.4 7.9 1
1,1,1-Trichloroethane ND ug/kg 07/26/22 16:19 71-55-607/25/22 16:009.4 4.9 1
1,1,2-Trichloroethane ND ug/kg 07/26/22 16:19 79-00-507/25/22 16:009.4 3.1 1
Trichloroethene ND ug/kg 07/26/22 16:19 79-01-607/25/22 16:009.4 2.4 1
Trichlorofluoromethane ND ug/kg 07/26/22 16:19 75-69-407/25/22 16:009.4 5.2 1
1,2,3-Trichloropropane ND ug/kg 07/26/22 16:19 96-18-407/25/22 16:009.4 4.7 1
1,2,4-Trimethylbenzene ND ug/kg 07/26/22 16:19 95-63-607/25/22 16:009.4 2.6 1
1,3,5-Trimethylbenzene ND ug/kg 07/26/22 16:19 108-67-807/25/22 16:009.4 3.2 1
Vinyl acetate ND ug/kg 07/26/22 16:19 108-05-407/25/22 16:0093.8 6.8 1
Vinyl chloride ND ug/kg 07/26/22 16:19 75-01-407/25/22 16:0018.8 4.8 1
Xylene (Total)ND ug/kg 07/26/22 16:19 1330-20-707/25/22 16:0018.8 5.3 1
m&p-Xylene ND ug/kg 07/26/22 16:19 179601-23-107/25/22 16:0018.8 6.4 1
o-Xylene ND ug/kg 07/26/22 16:19 95-47-607/25/22 16:009.4 4.1 1
Surrogates
Toluene-d8 (S)100 %07/26/22 16:19 2037-26-507/25/22 16:0070-130 1
4-Bromofluorobenzene (S)98 %07/26/22 16:19 460-00-407/25/22 16:0069-134 1
1,2-Dichloroethane-d4 (S)107 %07/26/22 16:19 17060-07-007/25/22 16:0070-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 15.3 %07/25/22 14:52 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:EXC-BASE-1 Lab ID:92616378016 Collected:07/20/22 15:55 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 76.7 %08/03/22 11:0608/03/22 10:591
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:EXC-BASE-2 Lab ID:92616378017 Collected:07/20/22 16:02 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP EPH Preparation Method: MA DEP/NJ DEP
Pace National - Mt. Juliet
TPH by Method MADEPE
Aliphatic (C09-C18)ND mg/kg 08/04/22 19:1808/02/22 15:258.81 2.94 1
Aliphatic (C19-C36)5.46J mg/kg 08/04/22 19:18 B,J08/02/22 15:258.81 2.94 1
Aromatic (C11-C22)3.05J mg/kg 08/04/22 21:09 B,J08/02/22 15:258.81 2.94 1
Total Extractable Hydrocarbons 8.51J mg/kg 08/04/22 21:09 TPH-TEH B,J08/02/22 15:258.81 2.94 1
Surrogates
o-Terphenyl (S)61.7 %08/04/22 21:09 84-15-108/02/22 15:2540.0-140 1
1-Chloro-octadecane (S)52.7 %08/04/22 19:18 3386-33-208/02/22 15:2540.0-140 1
2-Fluorobiphenyl (S)82.4 %08/04/22 21:09 321-60-808/02/22 15:2540.0-140 1
2-Bromonaphthalene (S)79.2 %08/04/22 21:09 580-13-208/02/22 15:2540.0-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Pace Analytical Services - Charlotte
VPH NC Soil
Aliphatic (C05-C08)ND mg/kg 07/23/22 01:22 N207/22/22 18:223.1 3.1 1
Aliphatic(C09-C12) Adjusted ND mg/kg 07/23/22 01:22 N207/22/22 18:223.1 3.1 1
Aromatic (C09-C10)ND mg/kg 07/23/22 01:22 N207/22/22 18:223.1 3.1 1
Surrogates
4-Bromofluorobenzene (FID) (S)96 %07/23/22 01:22 460-00-407/22/22 18:2270-130 1
4-Bromofluorobenzene (PID) (S)85 %07/23/22 01:22 460-00-407/22/22 18:2270-130 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 07/28/22 10:17 83-32-907/27/22 03:473791331
Acenaphthylene ND ug/kg 07/28/22 10:17 208-96-807/27/22 03:473791331
Aniline ND ug/kg 07/28/22 10:17 62-53-307/27/22 03:473791481
Anthracene ND ug/kg 07/28/22 10:17 120-12-707/27/22 03:473791241
Benzo(a)anthracene ND ug/kg 07/28/22 10:17 56-55-307/27/22 03:473791261
Benzo(a)pyrene ND ug/kg 07/28/22 10:17 50-32-807/27/22 03:473791311
Benzo(b)fluoranthene ND ug/kg 07/28/22 10:17 205-99-207/27/22 03:473791261
Benzo(g,h,i)perylene ND ug/kg 07/28/22 10:17 191-24-207/27/22 03:473791471
Benzo(k)fluoranthene ND ug/kg 07/28/22 10:17 207-08-907/27/22 03:473791331
Benzoic Acid ND ug/kg 07/28/22 10:17 65-85-007/27/22 03:4718908141
Benzyl alcohol ND ug/kg 07/28/22 10:17 100-51-607/27/22 03:477582871
4-Bromophenylphenyl ether ND ug/kg 07/28/22 10:17 101-55-307/27/22 03:473791461
Butylbenzylphthalate ND ug/kg 07/28/22 10:17 85-68-707/27/22 03:473791601
4-Chloro-3-methylphenol ND ug/kg 07/28/22 10:17 59-50-707/27/22 03:477582661
4-Chloroaniline ND ug/kg 07/28/22 10:17 106-47-807/27/22 03:477582971
bis(2-Chloroethoxy)methane ND ug/kg 07/28/22 10:17 111-91-107/27/22 03:473791571
bis(2-Chloroethyl) ether ND ug/kg 07/28/22 10:17 111-44-407/27/22 03:473791421
2-Chloronaphthalene ND ug/kg 07/28/22 10:17 91-58-707/27/22 03:473791501
2-Chlorophenol ND ug/kg 07/28/22 10:17 95-57-807/27/22 03:473791421
4-Chlorophenylphenyl ether ND ug/kg 07/28/22 10:17 7005-72-307/27/22 03:473791411
Chrysene ND ug/kg 07/28/22 10:17 218-01-907/27/22 03:473791381
Dibenz(a,h)anthracene ND ug/kg 07/28/22 10:17 53-70-307/27/22 03:473791461
Dibenzofuran ND ug/kg 07/28/22 10:17 132-64-907/27/22 03:473791371
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:EXC-BASE-2 Lab ID:92616378017 Collected:07/20/22 16:02 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
1,2-Dichlorobenzene ND ug/kg 07/28/22 10:17 95-50-107/27/22 03:473791371
1,3-Dichlorobenzene ND ug/kg 07/28/22 10:17 541-73-107/27/22 03:473791341
1,4-Dichlorobenzene ND ug/kg 07/28/22 10:17 106-46-707/27/22 03:473791451
3,3'-Dichlorobenzidine ND ug/kg 07/28/22 10:17 91-94-107/27/22 03:477582561
2,4-Dichlorophenol ND ug/kg 07/28/22 10:17 120-83-207/27/22 03:473791481
Diethylphthalate ND ug/kg 07/28/22 10:17 84-66-207/27/22 03:473791391
2,4-Dimethylphenol ND ug/kg 07/28/22 10:17 105-67-907/27/22 03:473791571
Dimethylphthalate ND ug/kg 07/28/22 10:17 131-11-307/27/22 03:473791381
Di-n-butylphthalate ND ug/kg 07/28/22 10:17 84-74-207/27/22 03:473791271
4,6-Dinitro-2-methylphenol ND ug/kg 07/28/22 10:17 534-52-107/27/22 03:477583541
2,4-Dinitrophenol ND ug/kg 07/28/22 10:17 51-28-507/27/22 03:47189011701
2,4-Dinitrotoluene ND ug/kg 07/28/22 10:17 121-14-207/27/22 03:473791461
2,6-Dinitrotoluene ND ug/kg 07/28/22 10:17 606-20-207/27/22 03:473791391
Di-n-octylphthalate ND ug/kg 07/28/22 10:17 117-84-007/27/22 03:473791491
bis(2-Ethylhexyl)phthalate ND ug/kg 07/28/22 10:17 117-81-707/27/22 03:473791471
Fluoranthene ND ug/kg 07/28/22 10:17 206-44-007/27/22 03:473791301
Fluorene ND ug/kg 07/28/22 10:17 86-73-707/27/22 03:473791331
Hexachloro-1,3-butadiene ND ug/kg 07/28/22 10:17 87-68-307/27/22 03:473791641
Hexachlorobenzene ND ug/kg 07/28/22 10:17 118-74-107/27/22 03:473791481
Hexachlorocyclopentadiene ND ug/kg 07/28/22 10:17 77-47-407/27/22 03:473792171
Hexachloroethane ND ug/kg 07/28/22 10:17 67-72-107/27/22 03:473791451
Indeno(1,2,3-cd)pyrene ND ug/kg 07/28/22 10:17 193-39-507/27/22 03:473791491
Isophorone ND ug/kg 07/28/22 10:17 78-59-107/27/22 03:473791691
1-Methylnaphthalene ND ug/kg 07/28/22 10:17 90-12-007/27/22 03:473791331
2-Methylnaphthalene ND ug/kg 07/28/22 10:17 91-57-607/27/22 03:473791521
2-Methylphenol(o-Cresol)ND ug/kg 07/28/22 10:17 95-48-707/27/22 03:473791551
3&4-Methylphenol(m&p Cresol)ND ug/kg 07/28/22 10:17 15831-10-407/27/22 03:473791531
Naphthalene ND ug/kg 07/28/22 10:17 91-20-307/27/22 03:473791291
2-Nitroaniline ND ug/kg 07/28/22 10:17 88-74-407/27/22 03:4718903101
3-Nitroaniline ND ug/kg 07/28/22 10:17 99-09-207/27/22 03:4718902971
4-Nitroaniline ND ug/kg 07/28/22 10:17 100-01-607/27/22 03:477582881
Nitrobenzene ND ug/kg 07/28/22 10:17 98-95-307/27/22 03:473791761
2-Nitrophenol ND ug/kg 07/28/22 10:17 88-75-507/27/22 03:473791641
4-Nitrophenol ND ug/kg 07/28/22 10:17 100-02-707/27/22 03:4718907321
N-Nitrosodimethylamine ND ug/kg 07/28/22 10:17 62-75-907/27/22 03:473791271
N-Nitroso-di-n-propylamine ND ug/kg 07/28/22 10:17 621-64-707/27/22 03:473791421
N-Nitrosodiphenylamine ND ug/kg 07/28/22 10:17 86-30-607/27/22 03:473791341
2,2'-Oxybis(1-chloropropane)ND ug/kg 07/28/22 10:17 108-60-107/27/22 03:473791801
Pentachlorophenol ND ug/kg 07/28/22 10:17 87-86-507/27/22 03:477583711
Phenanthrene ND ug/kg 07/28/22 10:17 85-01-807/27/22 03:473791241
Phenol ND ug/kg 07/28/22 10:17 108-95-207/27/22 03:473791691
Pyrene ND ug/kg 07/28/22 10:17 129-00-007/27/22 03:473791541
Pyridine ND ug/kg 07/28/22 10:17 110-86-107/27/22 03:473791191
1,2,4-Trichlorobenzene ND ug/kg 07/28/22 10:17 120-82-107/27/22 03:473791491
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:EXC-BASE-2 Lab ID:92616378017 Collected:07/20/22 16:02 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,4,5-Trichlorophenol ND ug/kg 07/28/22 10:17 95-95-407/27/22 03:473791731
2,4,6-Trichlorophenol ND ug/kg 07/28/22 10:17 88-06-207/27/22 03:473791561
Surrogates
Nitrobenzene-d5 (S)61 %07/28/22 10:17 4165-60-007/27/22 03:4721-130 1
2-Fluorobiphenyl (S)60 %07/28/22 10:17 321-60-807/27/22 03:4719-130 1
Terphenyl-d14 (S)79 %07/28/22 10:17 1718-51-007/27/22 03:4715-130 1
Phenol-d6 (S)61 %07/28/22 10:17 13127-88-307/27/22 03:4718-130 1
2-Fluorophenol (S)62 %07/28/22 10:17 367-12-407/27/22 03:4718-130 1
2,4,6-Tribromophenol (S)76 %07/28/22 10:17 118-79-607/27/22 03:4718-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 07/26/22 16:38 67-64-107/25/22 16:0014446.1 1
Benzene ND ug/kg 07/26/22 16:38 71-43-207/25/22 16:007.2 2.9 1
Bromobenzene ND ug/kg 07/26/22 16:38 108-86-107/25/22 16:007.2 2.3 1
Bromochloromethane ND ug/kg 07/26/22 16:38 74-97-507/25/22 16:007.2 2.1 1
Bromodichloromethane ND ug/kg 07/26/22 16:38 75-27-407/25/22 16:007.2 2.8 1
Bromoform ND ug/kg 07/26/22 16:38 75-25-207/25/22 16:007.2 2.5 1
Bromomethane ND ug/kg 07/26/22 16:38 74-83-9 IK,v107/25/22 16:0014.4 11.4 1
2-Butanone (MEK)78.9J ug/kg 07/26/22 16:38 78-93-3 C707/25/22 16:0014434.5 1
n-Butylbenzene ND ug/kg 07/26/22 16:38 104-51-807/25/22 16:007.2 3.4 1
sec-Butylbenzene ND ug/kg 07/26/22 16:38 135-98-807/25/22 16:007.2 3.2 1
tert-Butylbenzene ND ug/kg 07/26/22 16:38 98-06-607/25/22 16:007.2 2.6 1
Carbon tetrachloride ND ug/kg 07/26/22 16:38 56-23-507/25/22 16:007.2 2.7 1
Chlorobenzene ND ug/kg 07/26/22 16:38 108-90-707/25/22 16:007.2 1.4 1
Chloroethane ND ug/kg 07/26/22 16:38 75-00-307/25/22 16:0014.4 5.5 1
Chloroform ND ug/kg 07/26/22 16:38 67-66-307/25/22 16:007.2 4.4 1
Chloromethane ND ug/kg 07/26/22 16:38 74-87-307/25/22 16:0014.4 6.0 1
2-Chlorotoluene ND ug/kg 07/26/22 16:38 95-49-807/25/22 16:007.2 2.5 1
4-Chlorotoluene ND ug/kg 07/26/22 16:38 106-43-407/25/22 16:007.2 1.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 07/26/22 16:38 96-12-8 IK07/25/22 16:007.2 2.8 1
Dibromochloromethane ND ug/kg 07/26/22 16:38 124-48-107/25/22 16:007.2 4.0 1
1,2-Dibromoethane (EDB)ND ug/kg 07/26/22 16:38 106-93-407/25/22 16:007.2 3.2 1
Dibromomethane ND ug/kg 07/26/22 16:38 74-95-307/25/22 16:007.2 1.5 1
1,2-Dichlorobenzene ND ug/kg 07/26/22 16:38 95-50-107/25/22 16:007.2 2.6 1
1,3-Dichlorobenzene ND ug/kg 07/26/22 16:38 541-73-107/25/22 16:007.2 2.2 1
1,4-Dichlorobenzene ND ug/kg 07/26/22 16:38 106-46-707/25/22 16:007.2 1.9 1
Dichlorodifluoromethane ND ug/kg 07/26/22 16:38 75-71-8 IH07/25/22 16:0014.4 3.1 1
1,1-Dichloroethane ND ug/kg 07/26/22 16:38 75-34-307/25/22 16:007.2 3.0 1
1,2-Dichloroethane ND ug/kg 07/26/22 16:38 107-06-207/25/22 16:007.2 4.8 1
1,1-Dichloroethene ND ug/kg 07/26/22 16:38 75-35-407/25/22 16:007.2 3.0 1
cis-1,2-Dichloroethene ND ug/kg 07/26/22 16:38 156-59-207/25/22 16:007.2 2.5 1
trans-1,2-Dichloroethene ND ug/kg 07/26/22 16:38 156-60-507/25/22 16:007.2 2.5 1
1,2-Dichloropropane ND ug/kg 07/26/22 16:38 78-87-507/25/22 16:007.2 2.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:EXC-BASE-2 Lab ID:92616378017 Collected:07/20/22 16:02 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,3-Dichloropropane ND ug/kg 07/26/22 16:38 142-28-907/25/22 16:007.2 2.2 1
2,2-Dichloropropane ND ug/kg 07/26/22 16:38 594-20-7 v207/25/22 16:007.2 2.3 1
1,1-Dichloropropene ND ug/kg 07/26/22 16:38 563-58-607/25/22 16:007.2 3.4 1
cis-1,3-Dichloropropene ND ug/kg 07/26/22 16:38 10061-01-507/25/22 16:007.2 2.0 1
trans-1,3-Dichloropropene ND ug/kg 07/26/22 16:38 10061-02-607/25/22 16:007.2 2.5 1
Diisopropyl ether ND ug/kg 07/26/22 16:38 108-20-307/25/22 16:007.2 1.9 1
Ethylbenzene ND ug/kg 07/26/22 16:38 100-41-407/25/22 16:007.2 3.3 1
Hexachloro-1,3-butadiene ND ug/kg 07/26/22 16:38 87-68-307/25/22 16:0014.4 11.8 1
2-Hexanone ND ug/kg 07/26/22 16:38 591-78-607/25/22 16:0071.9 6.9 1
Isopropylbenzene (Cumene)ND ug/kg 07/26/22 16:38 98-82-807/25/22 16:007.2 2.4 1
p-Isopropyltoluene ND ug/kg 07/26/22 16:38 99-87-607/25/22 16:007.2 3.5 1
Methylene Chloride ND ug/kg 07/26/22 16:38 75-09-207/25/22 16:0028.7 19.7 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 07/26/22 16:38 108-10-107/25/22 16:0071.9 6.9 1
Methyl-tert-butyl ether ND ug/kg 07/26/22 16:38 1634-04-407/25/22 16:007.2 2.7 1
Naphthalene ND ug/kg 07/26/22 16:38 91-20-3 v207/25/22 16:007.2 3.8 1
n-Propylbenzene ND ug/kg 07/26/22 16:38 103-65-107/25/22 16:007.2 2.6 1
Styrene ND ug/kg 07/26/22 16:38 100-42-507/25/22 16:007.2 1.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 07/26/22 16:38 630-20-607/25/22 16:007.2 2.8 1
1,1,2,2-Tetrachloroethane ND ug/kg 07/26/22 16:38 79-34-507/25/22 16:007.2 1.9 1
Tetrachloroethene ND ug/kg 07/26/22 16:38 127-18-407/25/22 16:007.2 2.3 1
Toluene ND ug/kg 07/26/22 16:38 108-88-307/25/22 16:007.2 2.0 1
1,2,3-Trichlorobenzene ND ug/kg 07/26/22 16:38 87-61-6 IK,v207/25/22 16:007.2 5.8 1
1,2,4-Trichlorobenzene ND ug/kg 07/26/22 16:38 120-82-107/25/22 16:007.2 6.0 1
1,1,1-Trichloroethane ND ug/kg 07/26/22 16:38 71-55-607/25/22 16:007.2 3.7 1
1,1,2-Trichloroethane ND ug/kg 07/26/22 16:38 79-00-507/25/22 16:007.2 2.4 1
Trichloroethene ND ug/kg 07/26/22 16:38 79-01-607/25/22 16:007.2 1.9 1
Trichlorofluoromethane ND ug/kg 07/26/22 16:38 75-69-407/25/22 16:007.2 4.0 1
1,2,3-Trichloropropane ND ug/kg 07/26/22 16:38 96-18-407/25/22 16:007.2 3.6 1
1,2,4-Trimethylbenzene ND ug/kg 07/26/22 16:38 95-63-607/25/22 16:007.2 2.0 1
1,3,5-Trimethylbenzene ND ug/kg 07/26/22 16:38 108-67-807/25/22 16:007.2 2.4 1
Vinyl acetate ND ug/kg 07/26/22 16:38 108-05-407/25/22 16:0071.9 5.2 1
Vinyl chloride ND ug/kg 07/26/22 16:38 75-01-407/25/22 16:0014.4 3.7 1
Xylene (Total)ND ug/kg 07/26/22 16:38 1330-20-707/25/22 16:0014.4 4.1 1
m&p-Xylene ND ug/kg 07/26/22 16:38 179601-23-107/25/22 16:0014.4 4.9 1
o-Xylene ND ug/kg 07/26/22 16:38 95-47-607/25/22 16:007.2 3.2 1
Surrogates
Toluene-d8 (S)101 %07/26/22 16:38 2037-26-507/25/22 16:0070-130 1
4-Bromofluorobenzene (S)99 %07/26/22 16:38 460-00-407/25/22 16:0069-134 1
1,2-Dichloroethane-d4 (S)110 %07/26/22 16:38 17060-07-007/25/22 16:0070-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 14.0 %07/25/22 14:52 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:EXC-BASE-2 Lab ID:92616378017 Collected:07/20/22 16:02 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 73.8 %08/03/22 11:0608/03/22 10:591
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:EXC-BASE-3 Lab ID:92616378018 Collected:07/20/22 16:08 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP EPH Preparation Method: MA DEP/NJ DEP
Pace National - Mt. Juliet
TPH by Method MADEPE
Aliphatic (C09-C18)17.8 mg/kg 08/04/22 19:41 B08/02/22 15:259.16 3.06 1
Aliphatic (C19-C36)10.4 mg/kg 08/04/22 19:41 B08/02/22 15:259.16 3.06 1
Aromatic (C11-C22)10.1 mg/kg 08/04/22 20:47 B08/02/22 15:259.16 3.06 1
Total Extractable Hydrocarbons 38.3 mg/kg 08/04/22 20:47 TPH-TEH B08/02/22 15:259.16 3.06 1
Surrogates
o-Terphenyl (S)71.8 %08/04/22 20:47 84-15-108/02/22 15:2540.0-140 1
1-Chloro-octadecane (S)69.2 %08/04/22 19:41 3386-33-208/02/22 15:2540.0-140 1
2-Fluorobiphenyl (S)84.4 %08/04/22 20:47 321-60-808/02/22 15:2540.0-140 1
2-Bromonaphthalene (S)81.6 %08/04/22 20:47 580-13-208/02/22 15:2540.0-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Pace Analytical Services - Charlotte
VPH NC Soil
Aliphatic (C05-C08)ND mg/kg 07/23/22 01:50 N207/22/22 18:222.9 2.9 1
Aliphatic(C09-C12) Adjusted ND mg/kg 07/23/22 01:50 N207/22/22 18:222.9 2.9 1
Aromatic (C09-C10)ND mg/kg 07/23/22 01:50 N207/22/22 18:222.9 2.9 1
Surrogates
4-Bromofluorobenzene (FID) (S)102 %07/23/22 01:50 460-00-407/22/22 18:2270-130 1
4-Bromofluorobenzene (PID) (S)90 %07/23/22 01:50 460-00-407/22/22 18:2270-130 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 07/28/22 10:45 83-32-907/27/22 03:473971401
Acenaphthylene ND ug/kg 07/28/22 10:45 208-96-807/27/22 03:473971401
Aniline ND ug/kg 07/28/22 10:45 62-53-307/27/22 03:473971551
Anthracene ND ug/kg 07/28/22 10:45 120-12-707/27/22 03:473971301
Benzo(a)anthracene ND ug/kg 07/28/22 10:45 56-55-307/27/22 03:473971321
Benzo(a)pyrene ND ug/kg 07/28/22 10:45 50-32-807/27/22 03:473971371
Benzo(b)fluoranthene ND ug/kg 07/28/22 10:45 205-99-207/27/22 03:473971321
Benzo(g,h,i)perylene ND ug/kg 07/28/22 10:45 191-24-207/27/22 03:473971541
Benzo(k)fluoranthene ND ug/kg 07/28/22 10:45 207-08-907/27/22 03:473971401
Benzoic Acid ND ug/kg 07/28/22 10:45 65-85-007/27/22 03:4719808531
Benzyl alcohol ND ug/kg 07/28/22 10:45 100-51-607/27/22 03:477943011
4-Bromophenylphenyl ether ND ug/kg 07/28/22 10:45 101-55-307/27/22 03:473971531
Butylbenzylphthalate ND ug/kg 07/28/22 10:45 85-68-707/27/22 03:473971671
4-Chloro-3-methylphenol ND ug/kg 07/28/22 10:45 59-50-707/27/22 03:477942791
4-Chloroaniline ND ug/kg 07/28/22 10:45 106-47-807/27/22 03:477943111
bis(2-Chloroethoxy)methane ND ug/kg 07/28/22 10:45 111-91-107/27/22 03:473971651
bis(2-Chloroethyl) ether ND ug/kg 07/28/22 10:45 111-44-407/27/22 03:473971491
2-Chloronaphthalene ND ug/kg 07/28/22 10:45 91-58-707/27/22 03:473971581
2-Chlorophenol ND ug/kg 07/28/22 10:45 95-57-807/27/22 03:473971491
4-Chlorophenylphenyl ether ND ug/kg 07/28/22 10:45 7005-72-307/27/22 03:473971481
Chrysene ND ug/kg 07/28/22 10:45 218-01-907/27/22 03:473971441
Dibenz(a,h)anthracene ND ug/kg 07/28/22 10:45 53-70-307/27/22 03:473971531
Dibenzofuran ND ug/kg 07/28/22 10:45 132-64-907/27/22 03:473971431
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:EXC-BASE-3 Lab ID:92616378018 Collected:07/20/22 16:08 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
1,2-Dichlorobenzene ND ug/kg 07/28/22 10:45 95-50-107/27/22 03:473971431
1,3-Dichlorobenzene ND ug/kg 07/28/22 10:45 541-73-107/27/22 03:473971411
1,4-Dichlorobenzene ND ug/kg 07/28/22 10:45 106-46-707/27/22 03:473971521
3,3'-Dichlorobenzidine ND ug/kg 07/28/22 10:45 91-94-107/27/22 03:477942681
2,4-Dichlorophenol ND ug/kg 07/28/22 10:45 120-83-207/27/22 03:473971551
Diethylphthalate ND ug/kg 07/28/22 10:45 84-66-207/27/22 03:473971461
2,4-Dimethylphenol ND ug/kg 07/28/22 10:45 105-67-907/27/22 03:473971651
Dimethylphthalate ND ug/kg 07/28/22 10:45 131-11-307/27/22 03:473971441
Di-n-butylphthalate ND ug/kg 07/28/22 10:45 84-74-207/27/22 03:473971331
4,6-Dinitro-2-methylphenol ND ug/kg 07/28/22 10:45 534-52-107/27/22 03:477943701
2,4-Dinitrophenol ND ug/kg 07/28/22 10:45 51-28-507/27/22 03:47198012301
2,4-Dinitrotoluene ND ug/kg 07/28/22 10:45 121-14-207/27/22 03:473971531
2,6-Dinitrotoluene ND ug/kg 07/28/22 10:45 606-20-207/27/22 03:473971461
Di-n-octylphthalate ND ug/kg 07/28/22 10:45 117-84-007/27/22 03:473971561
bis(2-Ethylhexyl)phthalate ND ug/kg 07/28/22 10:45 117-81-707/27/22 03:473971541
Fluoranthene ND ug/kg 07/28/22 10:45 206-44-007/27/22 03:473971361
Fluorene ND ug/kg 07/28/22 10:45 86-73-707/27/22 03:473971401
Hexachloro-1,3-butadiene ND ug/kg 07/28/22 10:45 87-68-307/27/22 03:473971721
Hexachlorobenzene ND ug/kg 07/28/22 10:45 118-74-107/27/22 03:473971551
Hexachlorocyclopentadiene ND ug/kg 07/28/22 10:45 77-47-407/27/22 03:473972271
Hexachloroethane ND ug/kg 07/28/22 10:45 67-72-107/27/22 03:473971521
Indeno(1,2,3-cd)pyrene ND ug/kg 07/28/22 10:45 193-39-507/27/22 03:473971561
Isophorone ND ug/kg 07/28/22 10:45 78-59-107/27/22 03:473971771
1-Methylnaphthalene ND ug/kg 07/28/22 10:45 90-12-007/27/22 03:473971401
2-Methylnaphthalene ND ug/kg 07/28/22 10:45 91-57-607/27/22 03:473971591
2-Methylphenol(o-Cresol)ND ug/kg 07/28/22 10:45 95-48-707/27/22 03:473971621
3&4-Methylphenol(m&p Cresol)ND ug/kg 07/28/22 10:45 15831-10-407/27/22 03:473971601
Naphthalene ND ug/kg 07/28/22 10:45 91-20-307/27/22 03:473971351
2-Nitroaniline ND ug/kg 07/28/22 10:45 88-74-407/27/22 03:4719803251
3-Nitroaniline ND ug/kg 07/28/22 10:45 99-09-207/27/22 03:4719803111
4-Nitroaniline ND ug/kg 07/28/22 10:45 100-01-607/27/22 03:477943021
Nitrobenzene ND ug/kg 07/28/22 10:45 98-95-307/27/22 03:473971841
2-Nitrophenol ND ug/kg 07/28/22 10:45 88-75-507/27/22 03:473971721
4-Nitrophenol ND ug/kg 07/28/22 10:45 100-02-707/27/22 03:4719807671
N-Nitrosodimethylamine ND ug/kg 07/28/22 10:45 62-75-907/27/22 03:473971331
N-Nitroso-di-n-propylamine ND ug/kg 07/28/22 10:45 621-64-707/27/22 03:473971491
N-Nitrosodiphenylamine ND ug/kg 07/28/22 10:45 86-30-607/27/22 03:473971411
2,2'-Oxybis(1-chloropropane)ND ug/kg 07/28/22 10:45 108-60-107/27/22 03:473971891
Pentachlorophenol ND ug/kg 07/28/22 10:45 87-86-507/27/22 03:477943881
Phenanthrene ND ug/kg 07/28/22 10:45 85-01-807/27/22 03:473971301
Phenol ND ug/kg 07/28/22 10:45 108-95-207/27/22 03:473971771
Pyrene ND ug/kg 07/28/22 10:45 129-00-007/27/22 03:473971611
Pyridine ND ug/kg 07/28/22 10:45 110-86-107/27/22 03:473971251
1,2,4-Trichlorobenzene ND ug/kg 07/28/22 10:45 120-82-107/27/22 03:473971561
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:EXC-BASE-3 Lab ID:92616378018 Collected:07/20/22 16:08 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,4,5-Trichlorophenol ND ug/kg 07/28/22 10:45 95-95-407/27/22 03:473971821
2,4,6-Trichlorophenol ND ug/kg 07/28/22 10:45 88-06-207/27/22 03:473971641
Surrogates
Nitrobenzene-d5 (S)56 %07/28/22 10:45 4165-60-007/27/22 03:4721-130 1
2-Fluorobiphenyl (S)55 %07/28/22 10:45 321-60-807/27/22 03:4719-130 1
Terphenyl-d14 (S)72 %07/28/22 10:45 1718-51-007/27/22 03:4715-130 1
Phenol-d6 (S)55 %07/28/22 10:45 13127-88-307/27/22 03:4718-130 1
2-Fluorophenol (S)54 %07/28/22 10:45 367-12-407/27/22 03:4718-130 1
2,4,6-Tribromophenol (S)65 %07/28/22 10:45 118-79-607/27/22 03:4718-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 07/26/22 16:57 67-64-107/25/22 16:0013543.5 1
Benzene ND ug/kg 07/26/22 16:57 71-43-207/25/22 16:006.8 2.7 1
Bromobenzene ND ug/kg 07/26/22 16:57 108-86-107/25/22 16:006.8 2.2 1
Bromochloromethane ND ug/kg 07/26/22 16:57 74-97-507/25/22 16:006.8 2.0 1
Bromodichloromethane ND ug/kg 07/26/22 16:57 75-27-407/25/22 16:006.8 2.6 1
Bromoform ND ug/kg 07/26/22 16:57 75-25-207/25/22 16:006.8 2.4 1
Bromomethane ND ug/kg 07/26/22 16:57 74-83-9 IK,v107/25/22 16:0013.5 10.7 1
2-Butanone (MEK)88.0J ug/kg 07/26/22 16:57 78-93-3 C707/25/22 16:0013532.5 1
n-Butylbenzene ND ug/kg 07/26/22 16:57 104-51-807/25/22 16:006.8 3.2 1
sec-Butylbenzene ND ug/kg 07/26/22 16:57 135-98-807/25/22 16:006.8 3.0 1
tert-Butylbenzene ND ug/kg 07/26/22 16:57 98-06-607/25/22 16:006.8 2.4 1
Carbon tetrachloride ND ug/kg 07/26/22 16:57 56-23-507/25/22 16:006.8 2.5 1
Chlorobenzene ND ug/kg 07/26/22 16:57 108-90-707/25/22 16:006.8 1.3 1
Chloroethane ND ug/kg 07/26/22 16:57 75-00-307/25/22 16:0013.5 5.2 1
Chloroform ND ug/kg 07/26/22 16:57 67-66-307/25/22 16:006.8 4.1 1
Chloromethane ND ug/kg 07/26/22 16:57 74-87-307/25/22 16:0013.5 5.7 1
2-Chlorotoluene ND ug/kg 07/26/22 16:57 95-49-807/25/22 16:006.8 2.4 1
4-Chlorotoluene ND ug/kg 07/26/22 16:57 106-43-407/25/22 16:006.8 1.2 1
1,2-Dibromo-3-chloropropane ND ug/kg 07/26/22 16:57 96-12-8 IK07/25/22 16:006.8 2.6 1
Dibromochloromethane ND ug/kg 07/26/22 16:57 124-48-107/25/22 16:006.8 3.8 1
1,2-Dibromoethane (EDB)ND ug/kg 07/26/22 16:57 106-93-407/25/22 16:006.8 3.0 1
Dibromomethane ND ug/kg 07/26/22 16:57 74-95-307/25/22 16:006.8 1.4 1
1,2-Dichlorobenzene ND ug/kg 07/26/22 16:57 95-50-107/25/22 16:006.8 2.4 1
1,3-Dichlorobenzene ND ug/kg 07/26/22 16:57 541-73-107/25/22 16:006.8 2.1 1
1,4-Dichlorobenzene ND ug/kg 07/26/22 16:57 106-46-707/25/22 16:006.8 1.8 1
Dichlorodifluoromethane ND ug/kg 07/26/22 16:57 75-71-8 IH07/25/22 16:0013.5 2.9 1
1,1-Dichloroethane ND ug/kg 07/26/22 16:57 75-34-307/25/22 16:006.8 2.8 1
1,2-Dichloroethane ND ug/kg 07/26/22 16:57 107-06-207/25/22 16:006.8 4.5 1
1,1-Dichloroethene ND ug/kg 07/26/22 16:57 75-35-407/25/22 16:006.8 2.8 1
cis-1,2-Dichloroethene ND ug/kg 07/26/22 16:57 156-59-207/25/22 16:006.8 2.3 1
trans-1,2-Dichloroethene ND ug/kg 07/26/22 16:57 156-60-507/25/22 16:006.8 2.4 1
1,2-Dichloropropane ND ug/kg 07/26/22 16:57 78-87-507/25/22 16:006.8 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:EXC-BASE-3 Lab ID:92616378018 Collected:07/20/22 16:08 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,3-Dichloropropane ND ug/kg 07/26/22 16:57 142-28-907/25/22 16:006.8 2.1 1
2,2-Dichloropropane ND ug/kg 07/26/22 16:57 594-20-7 v207/25/22 16:006.8 2.2 1
1,1-Dichloropropene ND ug/kg 07/26/22 16:57 563-58-607/25/22 16:006.8 3.3 1
cis-1,3-Dichloropropene ND ug/kg 07/26/22 16:57 10061-01-507/25/22 16:006.8 1.8 1
trans-1,3-Dichloropropene ND ug/kg 07/26/22 16:57 10061-02-607/25/22 16:006.8 2.3 1
Diisopropyl ether ND ug/kg 07/26/22 16:57 108-20-307/25/22 16:006.8 1.8 1
Ethylbenzene ND ug/kg 07/26/22 16:57 100-41-407/25/22 16:006.8 3.2 1
Hexachloro-1,3-butadiene ND ug/kg 07/26/22 16:57 87-68-307/25/22 16:0013.5 11.1 1
2-Hexanone ND ug/kg 07/26/22 16:57 591-78-607/25/22 16:0067.7 6.5 1
Isopropylbenzene (Cumene)ND ug/kg 07/26/22 16:57 98-82-807/25/22 16:006.8 2.3 1
p-Isopropyltoluene ND ug/kg 07/26/22 16:57 99-87-607/25/22 16:006.8 3.3 1
Methylene Chloride ND ug/kg 07/26/22 16:57 75-09-207/25/22 16:0027.1 18.6 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 07/26/22 16:57 108-10-107/25/22 16:0067.7 6.5 1
Methyl-tert-butyl ether ND ug/kg 07/26/22 16:57 1634-04-407/25/22 16:006.8 2.5 1
Naphthalene ND ug/kg 07/26/22 16:57 91-20-3 v207/25/22 16:006.8 3.6 1
n-Propylbenzene ND ug/kg 07/26/22 16:57 103-65-107/25/22 16:006.8 2.4 1
Styrene ND ug/kg 07/26/22 16:57 100-42-507/25/22 16:006.8 1.8 1
1,1,1,2-Tetrachloroethane ND ug/kg 07/26/22 16:57 630-20-607/25/22 16:006.8 2.6 1
1,1,2,2-Tetrachloroethane ND ug/kg 07/26/22 16:57 79-34-507/25/22 16:006.8 1.8 1
Tetrachloroethene ND ug/kg 07/26/22 16:57 127-18-407/25/22 16:006.8 2.1 1
Toluene ND ug/kg 07/26/22 16:57 108-88-307/25/22 16:006.8 1.9 1
1,2,3-Trichlorobenzene ND ug/kg 07/26/22 16:57 87-61-6 IK,v207/25/22 16:006.8 5.5 1
1,2,4-Trichlorobenzene ND ug/kg 07/26/22 16:57 120-82-107/25/22 16:006.8 5.7 1
1,1,1-Trichloroethane ND ug/kg 07/26/22 16:57 71-55-607/25/22 16:006.8 3.5 1
1,1,2-Trichloroethane ND ug/kg 07/26/22 16:57 79-00-507/25/22 16:006.8 2.2 1
Trichloroethene ND ug/kg 07/26/22 16:57 79-01-607/25/22 16:006.8 1.7 1
Trichlorofluoromethane ND ug/kg 07/26/22 16:57 75-69-407/25/22 16:006.8 3.7 1
1,2,3-Trichloropropane ND ug/kg 07/26/22 16:57 96-18-407/25/22 16:006.8 3.4 1
1,2,4-Trimethylbenzene ND ug/kg 07/26/22 16:57 95-63-607/25/22 16:006.8 1.9 1
1,3,5-Trimethylbenzene ND ug/kg 07/26/22 16:57 108-67-807/25/22 16:006.8 2.3 1
Vinyl acetate ND ug/kg 07/26/22 16:57 108-05-407/25/22 16:0067.7 4.9 1
Vinyl chloride ND ug/kg 07/26/22 16:57 75-01-407/25/22 16:0013.5 3.4 1
Xylene (Total)ND ug/kg 07/26/22 16:57 1330-20-707/25/22 16:0013.5 3.9 1
m&p-Xylene ND ug/kg 07/26/22 16:57 179601-23-107/25/22 16:0013.5 4.6 1
o-Xylene ND ug/kg 07/26/22 16:57 95-47-607/25/22 16:006.8 3.0 1
Surrogates
Toluene-d8 (S)100 %07/26/22 16:57 2037-26-507/25/22 16:0070-130 1
4-Bromofluorobenzene (S)96 %07/26/22 16:57 460-00-407/25/22 16:0069-134 1
1,2-Dichloroethane-d4 (S)104 %07/26/22 16:57 17060-07-007/25/22 16:0070-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 17.1 %07/25/22 14:52 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:EXC-BASE-3 Lab ID:92616378018 Collected:07/20/22 16:08 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 71.0 %08/03/22 11:0608/03/22 10:591
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:EXC-BASE-4 Lab ID:92616378019 Collected:07/20/22 16:16 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP EPH Preparation Method: MA DEP/NJ DEP
Pace National - Mt. Juliet
TPH by Method MADEPE
Aliphatic (C09-C18)ND mg/kg 08/04/22 20:0308/02/22 15:258.09 2.70 1
Aliphatic (C19-C36)3.20J mg/kg 08/04/22 20:03 B,J08/02/22 15:258.09 2.70 1
Aromatic (C11-C22)2.97J mg/kg 08/04/22 20:25 B,J08/02/22 15:258.09 2.70 1
Total Extractable Hydrocarbons 6.17J mg/kg 08/04/22 20:25 TPH-TEH B,J08/02/22 15:258.09 2.70 1
Surrogates
o-Terphenyl (S)61.8 %08/04/22 20:25 84-15-108/02/22 15:2540.0-140 1
1-Chloro-octadecane (S)57.1 %08/04/22 20:03 3386-33-208/02/22 15:2540.0-140 1
2-Fluorobiphenyl (S)76.5 %08/04/22 20:25 321-60-808/02/22 15:2540.0-140 1
2-Bromonaphthalene (S)73.5 %08/04/22 20:25 580-13-208/02/22 15:2540.0-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Pace Analytical Services - Charlotte
VPH NC Soil
Aliphatic (C05-C08)ND mg/kg 07/23/22 02:18 N207/22/22 18:222.9 2.9 1
Aliphatic(C09-C12) Adjusted ND mg/kg 07/23/22 02:18 N207/22/22 18:222.9 2.9 1
Aromatic (C09-C10)ND mg/kg 07/23/22 02:18 N207/22/22 18:222.9 2.9 1
Surrogates
4-Bromofluorobenzene (FID) (S)104 %07/23/22 02:18 460-00-407/22/22 18:2270-130 1
4-Bromofluorobenzene (PID) (S)89 %07/23/22 02:18 460-00-407/22/22 18:2270-130 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 07/28/22 11:13 83-32-907/27/22 03:473771321
Acenaphthylene ND ug/kg 07/28/22 11:13 208-96-807/27/22 03:473771321
Aniline ND ug/kg 07/28/22 11:13 62-53-307/27/22 03:473771471
Anthracene ND ug/kg 07/28/22 11:13 120-12-707/27/22 03:473771231
Benzo(a)anthracene ND ug/kg 07/28/22 11:13 56-55-307/27/22 03:473771261
Benzo(a)pyrene ND ug/kg 07/28/22 11:13 50-32-807/27/22 03:473771301
Benzo(b)fluoranthene ND ug/kg 07/28/22 11:13 205-99-207/27/22 03:473771261
Benzo(g,h,i)perylene ND ug/kg 07/28/22 11:13 191-24-207/27/22 03:473771461
Benzo(k)fluoranthene ND ug/kg 07/28/22 11:13 207-08-907/27/22 03:473771321
Benzoic Acid ND ug/kg 07/28/22 11:13 65-85-007/27/22 03:4718808101
Benzyl alcohol ND ug/kg 07/28/22 11:13 100-51-607/27/22 03:477542861
4-Bromophenylphenyl ether ND ug/kg 07/28/22 11:13 101-55-307/27/22 03:473771451
Butylbenzylphthalate ND ug/kg 07/28/22 11:13 85-68-707/27/22 03:473771591
4-Chloro-3-methylphenol ND ug/kg 07/28/22 11:13 59-50-707/27/22 03:477542651
4-Chloroaniline ND ug/kg 07/28/22 11:13 106-47-807/27/22 03:477542961
bis(2-Chloroethoxy)methane ND ug/kg 07/28/22 11:13 111-91-107/27/22 03:473771561
bis(2-Chloroethyl) ether ND ug/kg 07/28/22 11:13 111-44-407/27/22 03:473771421
2-Chloronaphthalene ND ug/kg 07/28/22 11:13 91-58-707/27/22 03:473771501
2-Chlorophenol ND ug/kg 07/28/22 11:13 95-57-807/27/22 03:473771421
4-Chlorophenylphenyl ether ND ug/kg 07/28/22 11:13 7005-72-307/27/22 03:473771401
Chrysene ND ug/kg 07/28/22 11:13 218-01-907/27/22 03:473771371
Dibenz(a,h)anthracene ND ug/kg 07/28/22 11:13 53-70-307/27/22 03:473771451
Dibenzofuran ND ug/kg 07/28/22 11:13 132-64-907/27/22 03:473771361
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:EXC-BASE-4 Lab ID:92616378019 Collected:07/20/22 16:16 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
1,2-Dichlorobenzene ND ug/kg 07/28/22 11:13 95-50-107/27/22 03:473771361
1,3-Dichlorobenzene ND ug/kg 07/28/22 11:13 541-73-107/27/22 03:473771341
1,4-Dichlorobenzene ND ug/kg 07/28/22 11:13 106-46-707/27/22 03:473771441
3,3'-Dichlorobenzidine ND ug/kg 07/28/22 11:13 91-94-107/27/22 03:477542551
2,4-Dichlorophenol ND ug/kg 07/28/22 11:13 120-83-207/27/22 03:473771471
Diethylphthalate ND ug/kg 07/28/22 11:13 84-66-207/27/22 03:473771381
2,4-Dimethylphenol ND ug/kg 07/28/22 11:13 105-67-907/27/22 03:473771561
Dimethylphthalate ND ug/kg 07/28/22 11:13 131-11-307/27/22 03:473771371
Di-n-butylphthalate ND ug/kg 07/28/22 11:13 84-74-207/27/22 03:473771271
4,6-Dinitro-2-methylphenol ND ug/kg 07/28/22 11:13 534-52-107/27/22 03:477543521
2,4-Dinitrophenol ND ug/kg 07/28/22 11:13 51-28-507/27/22 03:47188011701
2,4-Dinitrotoluene ND ug/kg 07/28/22 11:13 121-14-207/27/22 03:473771451
2,6-Dinitrotoluene ND ug/kg 07/28/22 11:13 606-20-207/27/22 03:473771381
Di-n-octylphthalate ND ug/kg 07/28/22 11:13 117-84-007/27/22 03:473771481
bis(2-Ethylhexyl)phthalate ND ug/kg 07/28/22 11:13 117-81-707/27/22 03:473771461
Fluoranthene ND ug/kg 07/28/22 11:13 206-44-007/27/22 03:473771291
Fluorene ND ug/kg 07/28/22 11:13 86-73-707/27/22 03:473771321
Hexachloro-1,3-butadiene ND ug/kg 07/28/22 11:13 87-68-307/27/22 03:473771631
Hexachlorobenzene ND ug/kg 07/28/22 11:13 118-74-107/27/22 03:473771471
Hexachlorocyclopentadiene ND ug/kg 07/28/22 11:13 77-47-407/27/22 03:473772161
Hexachloroethane ND ug/kg 07/28/22 11:13 67-72-107/27/22 03:473771441
Indeno(1,2,3-cd)pyrene ND ug/kg 07/28/22 11:13 193-39-507/27/22 03:473771481
Isophorone ND ug/kg 07/28/22 11:13 78-59-107/27/22 03:473771681
1-Methylnaphthalene ND ug/kg 07/28/22 11:13 90-12-007/27/22 03:473771321
2-Methylnaphthalene ND ug/kg 07/28/22 11:13 91-57-607/27/22 03:473771511
2-Methylphenol(o-Cresol)ND ug/kg 07/28/22 11:13 95-48-707/27/22 03:473771541
3&4-Methylphenol(m&p Cresol)ND ug/kg 07/28/22 11:13 15831-10-407/27/22 03:473771521
Naphthalene ND ug/kg 07/28/22 11:13 91-20-307/27/22 03:473771281
2-Nitroaniline ND ug/kg 07/28/22 11:13 88-74-407/27/22 03:4718803081
3-Nitroaniline ND ug/kg 07/28/22 11:13 99-09-207/27/22 03:4718802961
4-Nitroaniline ND ug/kg 07/28/22 11:13 100-01-607/27/22 03:477542871
Nitrobenzene ND ug/kg 07/28/22 11:13 98-95-307/27/22 03:473771751
2-Nitrophenol ND ug/kg 07/28/22 11:13 88-75-507/27/22 03:473771631
4-Nitrophenol ND ug/kg 07/28/22 11:13 100-02-707/27/22 03:4718807291
N-Nitrosodimethylamine ND ug/kg 07/28/22 11:13 62-75-907/27/22 03:473771271
N-Nitroso-di-n-propylamine ND ug/kg 07/28/22 11:13 621-64-707/27/22 03:473771421
N-Nitrosodiphenylamine ND ug/kg 07/28/22 11:13 86-30-607/27/22 03:473771341
2,2'-Oxybis(1-chloropropane)ND ug/kg 07/28/22 11:13 108-60-107/27/22 03:473771791
Pentachlorophenol ND ug/kg 07/28/22 11:13 87-86-507/27/22 03:477543691
Phenanthrene ND ug/kg 07/28/22 11:13 85-01-807/27/22 03:473771231
Phenol ND ug/kg 07/28/22 11:13 108-95-207/27/22 03:473771681
Pyrene ND ug/kg 07/28/22 11:13 129-00-007/27/22 03:473771531
Pyridine ND ug/kg 07/28/22 11:13 110-86-107/27/22 03:473771191
1,2,4-Trichlorobenzene ND ug/kg 07/28/22 11:13 120-82-107/27/22 03:473771481
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:EXC-BASE-4 Lab ID:92616378019 Collected:07/20/22 16:16 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,4,5-Trichlorophenol ND ug/kg 07/28/22 11:13 95-95-407/27/22 03:473771721
2,4,6-Trichlorophenol ND ug/kg 07/28/22 11:13 88-06-207/27/22 03:473771551
Surrogates
Nitrobenzene-d5 (S)63 %07/28/22 11:13 4165-60-007/27/22 03:4721-130 1
2-Fluorobiphenyl (S)61 %07/28/22 11:13 321-60-807/27/22 03:4719-130 1
Terphenyl-d14 (S)79 %07/28/22 11:13 1718-51-007/27/22 03:4715-130 1
Phenol-d6 (S)65 %07/28/22 11:13 13127-88-307/27/22 03:4718-130 1
2-Fluorophenol (S)66 %07/28/22 11:13 367-12-407/27/22 03:4718-130 1
2,4,6-Tribromophenol (S)77 %07/28/22 11:13 118-79-607/27/22 03:4718-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 07/26/22 17:15 67-64-107/25/22 16:0013041.7 1
Benzene ND ug/kg 07/26/22 17:15 71-43-207/25/22 16:006.5 2.6 1
Bromobenzene ND ug/kg 07/26/22 17:15 108-86-107/25/22 16:006.5 2.1 1
Bromochloromethane ND ug/kg 07/26/22 17:15 74-97-507/25/22 16:006.5 1.9 1
Bromodichloromethane ND ug/kg 07/26/22 17:15 75-27-407/25/22 16:006.5 2.5 1
Bromoform ND ug/kg 07/26/22 17:15 75-25-207/25/22 16:006.5 2.3 1
Bromomethane ND ug/kg 07/26/22 17:15 74-83-9 IK,v107/25/22 16:0013.0 10.3 1
2-Butanone (MEK)70.2J ug/kg 07/26/22 17:15 78-93-3 C707/25/22 16:0013031.1 1
n-Butylbenzene ND ug/kg 07/26/22 17:15 104-51-807/25/22 16:006.5 3.1 1
sec-Butylbenzene ND ug/kg 07/26/22 17:15 135-98-807/25/22 16:006.5 2.9 1
tert-Butylbenzene ND ug/kg 07/26/22 17:15 98-06-607/25/22 16:006.5 2.3 1
Carbon tetrachloride ND ug/kg 07/26/22 17:15 56-23-507/25/22 16:006.5 2.4 1
Chlorobenzene ND ug/kg 07/26/22 17:15 108-90-707/25/22 16:006.5 1.2 1
Chloroethane ND ug/kg 07/26/22 17:15 75-00-307/25/22 16:0013.0 5.0 1
Chloroform ND ug/kg 07/26/22 17:15 67-66-307/25/22 16:006.5 3.9 1
Chloromethane ND ug/kg 07/26/22 17:15 74-87-307/25/22 16:0013.0 5.5 1
2-Chlorotoluene ND ug/kg 07/26/22 17:15 95-49-807/25/22 16:006.5 2.3 1
4-Chlorotoluene ND ug/kg 07/26/22 17:15 106-43-407/25/22 16:006.5 1.1 1
1,2-Dibromo-3-chloropropane ND ug/kg 07/26/22 17:15 96-12-8 IK07/25/22 16:006.5 2.5 1
Dibromochloromethane ND ug/kg 07/26/22 17:15 124-48-107/25/22 16:006.5 3.6 1
1,2-Dibromoethane (EDB)ND ug/kg 07/26/22 17:15 106-93-407/25/22 16:006.5 2.9 1
Dibromomethane ND ug/kg 07/26/22 17:15 74-95-307/25/22 16:006.5 1.4 1
1,2-Dichlorobenzene ND ug/kg 07/26/22 17:15 95-50-107/25/22 16:006.5 2.3 1
1,3-Dichlorobenzene ND ug/kg 07/26/22 17:15 541-73-107/25/22 16:006.5 2.0 1
1,4-Dichlorobenzene ND ug/kg 07/26/22 17:15 106-46-707/25/22 16:006.5 1.7 1
Dichlorodifluoromethane ND ug/kg 07/26/22 17:15 75-71-8 IH07/25/22 16:0013.0 2.8 1
1,1-Dichloroethane ND ug/kg 07/26/22 17:15 75-34-307/25/22 16:006.5 2.7 1
1,2-Dichloroethane ND ug/kg 07/26/22 17:15 107-06-207/25/22 16:006.5 4.3 1
1,1-Dichloroethene ND ug/kg 07/26/22 17:15 75-35-407/25/22 16:006.5 2.7 1
cis-1,2-Dichloroethene ND ug/kg 07/26/22 17:15 156-59-207/25/22 16:006.5 2.2 1
trans-1,2-Dichloroethene ND ug/kg 07/26/22 17:15 156-60-507/25/22 16:006.5 2.3 1
1,2-Dichloropropane ND ug/kg 07/26/22 17:15 78-87-507/25/22 16:006.5 1.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:EXC-BASE-4 Lab ID:92616378019 Collected:07/20/22 16:16 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,3-Dichloropropane ND ug/kg 07/26/22 17:15 142-28-907/25/22 16:006.5 2.0 1
2,2-Dichloropropane ND ug/kg 07/26/22 17:15 594-20-7 v207/25/22 16:006.5 2.1 1
1,1-Dichloropropene ND ug/kg 07/26/22 17:15 563-58-607/25/22 16:006.5 3.1 1
cis-1,3-Dichloropropene ND ug/kg 07/26/22 17:15 10061-01-507/25/22 16:006.5 1.8 1
trans-1,3-Dichloropropene ND ug/kg 07/26/22 17:15 10061-02-607/25/22 16:006.5 2.2 1
Diisopropyl ether ND ug/kg 07/26/22 17:15 108-20-307/25/22 16:006.5 1.8 1
Ethylbenzene ND ug/kg 07/26/22 17:15 100-41-407/25/22 16:006.5 3.0 1
Hexachloro-1,3-butadiene ND ug/kg 07/26/22 17:15 87-68-307/25/22 16:0013.0 10.6 1
2-Hexanone ND ug/kg 07/26/22 17:15 591-78-607/25/22 16:0064.9 6.3 1
Isopropylbenzene (Cumene)ND ug/kg 07/26/22 17:15 98-82-807/25/22 16:006.5 2.2 1
p-Isopropyltoluene ND ug/kg 07/26/22 17:15 99-87-607/25/22 16:006.5 3.2 1
Methylene Chloride ND ug/kg 07/26/22 17:15 75-09-207/25/22 16:0026.0 17.8 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 07/26/22 17:15 108-10-107/25/22 16:0064.9 6.3 1
Methyl-tert-butyl ether ND ug/kg 07/26/22 17:15 1634-04-407/25/22 16:006.5 2.4 1
Naphthalene ND ug/kg 07/26/22 17:15 91-20-3 v207/25/22 16:006.5 3.4 1
n-Propylbenzene ND ug/kg 07/26/22 17:15 103-65-107/25/22 16:006.5 2.3 1
Styrene ND ug/kg 07/26/22 17:15 100-42-507/25/22 16:006.5 1.7 1
1,1,1,2-Tetrachloroethane ND ug/kg 07/26/22 17:15 630-20-607/25/22 16:006.5 2.5 1
1,1,2,2-Tetrachloroethane ND ug/kg 07/26/22 17:15 79-34-507/25/22 16:006.5 1.7 1
Tetrachloroethene ND ug/kg 07/26/22 17:15 127-18-407/25/22 16:006.5 2.1 1
Toluene ND ug/kg 07/26/22 17:15 108-88-307/25/22 16:006.5 1.8 1
1,2,3-Trichlorobenzene ND ug/kg 07/26/22 17:15 87-61-6 IK,v207/25/22 16:006.5 5.2 1
1,2,4-Trichlorobenzene ND ug/kg 07/26/22 17:15 120-82-107/25/22 16:006.5 5.5 1
1,1,1-Trichloroethane ND ug/kg 07/26/22 17:15 71-55-607/25/22 16:006.5 3.4 1
1,1,2-Trichloroethane ND ug/kg 07/26/22 17:15 79-00-507/25/22 16:006.5 2.2 1
Trichloroethene ND ug/kg 07/26/22 17:15 79-01-607/25/22 16:006.5 1.7 1
Trichlorofluoromethane ND ug/kg 07/26/22 17:15 75-69-407/25/22 16:006.5 3.6 1
1,2,3-Trichloropropane ND ug/kg 07/26/22 17:15 96-18-407/25/22 16:006.5 3.3 1
1,2,4-Trimethylbenzene ND ug/kg 07/26/22 17:15 95-63-607/25/22 16:006.5 1.8 1
1,3,5-Trimethylbenzene ND ug/kg 07/26/22 17:15 108-67-807/25/22 16:006.5 2.2 1
Vinyl acetate ND ug/kg 07/26/22 17:15 108-05-407/25/22 16:0064.9 4.7 1
Vinyl chloride ND ug/kg 07/26/22 17:15 75-01-407/25/22 16:0013.0 3.3 1
Xylene (Total)ND ug/kg 07/26/22 17:15 1330-20-707/25/22 16:0013.0 3.7 1
m&p-Xylene ND ug/kg 07/26/22 17:15 179601-23-107/25/22 16:0013.0 4.4 1
o-Xylene ND ug/kg 07/26/22 17:15 95-47-607/25/22 16:006.5 2.9 1
Surrogates
Toluene-d8 (S)99 %07/26/22 17:15 2037-26-507/25/22 16:0070-130 1
4-Bromofluorobenzene (S)98 %07/26/22 17:15 460-00-407/25/22 16:0069-134 1
1,2-Dichloroethane-d4 (S)108 %07/26/22 17:15 17060-07-007/25/22 16:0070-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 13.6 %07/25/22 14:52 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:EXC-BASE-4 Lab ID:92616378019 Collected:07/20/22 16:16 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 80.4 %08/03/22 11:0608/03/22 10:591
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:EXC-SIDE-1 Lab ID:92616378020 Collected:07/20/22 16:22 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP EPH Preparation Method: MA DEP/NJ DEP
Pace National - Mt. Juliet
TPH by Method MADEPE
Aliphatic (C09-C18)ND mg/kg 08/04/22 23:0008/02/22 15:259.92 3.31 1
Aliphatic (C19-C36)4.91J mg/kg 08/04/22 23:00 B,J08/02/22 15:259.92 3.31 1
Aromatic (C11-C22)3.84J mg/kg 08/05/22 02:20 B,J08/02/22 15:259.92 3.31 1
Total Extractable Hydrocarbons 8.76J mg/kg 08/05/22 02:20 TPH-TEH B,J08/02/22 15:259.92 3.31 1
Surrogates
o-Terphenyl (S)67.6 %08/05/22 02:20 84-15-108/02/22 15:2540.0-140 1
1-Chloro-octadecane (S)60.0 %08/04/22 23:00 3386-33-208/02/22 15:2540.0-140 1
2-Fluorobiphenyl (S)83.3 %08/05/22 02:20 321-60-808/02/22 15:2540.0-140 1
2-Bromonaphthalene (S)79.7 %08/05/22 02:20 580-13-208/02/22 15:2540.0-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Pace Analytical Services - Charlotte
VPH NC Soil
Aliphatic (C05-C08)ND mg/kg 07/23/22 02:46 N207/22/22 18:223.5 3.5 1
Aliphatic(C09-C12) Adjusted ND mg/kg 07/23/22 02:46 N207/22/22 18:223.5 3.5 1
Aromatic (C09-C10)ND mg/kg 07/23/22 02:46 N207/22/22 18:223.5 3.5 1
Surrogates
4-Bromofluorobenzene (FID) (S)100 %07/23/22 02:46 460-00-407/22/22 18:2270-130 1
4-Bromofluorobenzene (PID) (S)88 %07/23/22 02:46 460-00-407/22/22 18:2270-130 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 07/28/22 11:41 83-32-907/27/22 03:474081441
Acenaphthylene ND ug/kg 07/28/22 11:41 208-96-807/27/22 03:474081441
Aniline ND ug/kg 07/28/22 11:41 62-53-307/27/22 03:474081601
Anthracene ND ug/kg 07/28/22 11:41 120-12-707/27/22 03:474081341
Benzo(a)anthracene ND ug/kg 07/28/22 11:41 56-55-307/27/22 03:474081361
Benzo(a)pyrene ND ug/kg 07/28/22 11:41 50-32-807/27/22 03:474081411
Benzo(b)fluoranthene ND ug/kg 07/28/22 11:41 205-99-207/27/22 03:474081361
Benzo(g,h,i)perylene ND ug/kg 07/28/22 11:41 191-24-207/27/22 03:474081581
Benzo(k)fluoranthene ND ug/kg 07/28/22 11:41 207-08-907/27/22 03:474081441
Benzoic Acid ND ug/kg 07/28/22 11:41 65-85-007/27/22 03:4720408771
Benzyl alcohol ND ug/kg 07/28/22 11:41 100-51-607/27/22 03:478173091
4-Bromophenylphenyl ether ND ug/kg 07/28/22 11:41 101-55-307/27/22 03:474081571
Butylbenzylphthalate ND ug/kg 07/28/22 11:41 85-68-707/27/22 03:474081721
4-Chloro-3-methylphenol ND ug/kg 07/28/22 11:41 59-50-707/27/22 03:478172871
4-Chloroaniline ND ug/kg 07/28/22 11:41 106-47-807/27/22 03:478173211
bis(2-Chloroethoxy)methane ND ug/kg 07/28/22 11:41 111-91-107/27/22 03:474081701
bis(2-Chloroethyl) ether ND ug/kg 07/28/22 11:41 111-44-407/27/22 03:474081531
2-Chloronaphthalene ND ug/kg 07/28/22 11:41 91-58-707/27/22 03:474081621
2-Chlorophenol ND ug/kg 07/28/22 11:41 95-57-807/27/22 03:474081531
4-Chlorophenylphenyl ether ND ug/kg 07/28/22 11:41 7005-72-307/27/22 03:474081521
Chrysene ND ug/kg 07/28/22 11:41 218-01-907/27/22 03:474081491
Dibenz(a,h)anthracene ND ug/kg 07/28/22 11:41 53-70-307/27/22 03:474081571
Dibenzofuran ND ug/kg 07/28/22 11:41 132-64-907/27/22 03:474081471
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:EXC-SIDE-1 Lab ID:92616378020 Collected:07/20/22 16:22 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
1,2-Dichlorobenzene ND ug/kg 07/28/22 11:41 95-50-107/27/22 03:474081471
1,3-Dichlorobenzene ND ug/kg 07/28/22 11:41 541-73-107/27/22 03:474081451
1,4-Dichlorobenzene ND ug/kg 07/28/22 11:41 106-46-707/27/22 03:474081561
3,3'-Dichlorobenzidine ND ug/kg 07/28/22 11:41 91-94-107/27/22 03:478172761
2,4-Dichlorophenol ND ug/kg 07/28/22 11:41 120-83-207/27/22 03:474081601
Diethylphthalate ND ug/kg 07/28/22 11:41 84-66-207/27/22 03:474081501
2,4-Dimethylphenol ND ug/kg 07/28/22 11:41 105-67-907/27/22 03:474081701
Dimethylphthalate ND ug/kg 07/28/22 11:41 131-11-307/27/22 03:474081491
Di-n-butylphthalate ND ug/kg 07/28/22 11:41 84-74-207/27/22 03:474081371
4,6-Dinitro-2-methylphenol ND ug/kg 07/28/22 11:41 534-52-107/27/22 03:478173811
2,4-Dinitrophenol ND ug/kg 07/28/22 11:41 51-28-507/27/22 03:47204012601
2,4-Dinitrotoluene ND ug/kg 07/28/22 11:41 121-14-207/27/22 03:474081571
2,6-Dinitrotoluene ND ug/kg 07/28/22 11:41 606-20-207/27/22 03:474081501
Di-n-octylphthalate ND ug/kg 07/28/22 11:41 117-84-007/27/22 03:474081611
bis(2-Ethylhexyl)phthalate ND ug/kg 07/28/22 11:41 117-81-707/27/22 03:474081581
Fluoranthene ND ug/kg 07/28/22 11:41 206-44-007/27/22 03:474081401
Fluorene ND ug/kg 07/28/22 11:41 86-73-707/27/22 03:474081441
Hexachloro-1,3-butadiene ND ug/kg 07/28/22 11:41 87-68-307/27/22 03:474081771
Hexachlorobenzene ND ug/kg 07/28/22 11:41 118-74-107/27/22 03:474081601
Hexachlorocyclopentadiene ND ug/kg 07/28/22 11:41 77-47-407/27/22 03:474082341
Hexachloroethane ND ug/kg 07/28/22 11:41 67-72-107/27/22 03:474081561
Indeno(1,2,3-cd)pyrene ND ug/kg 07/28/22 11:41 193-39-507/27/22 03:474081611
Isophorone ND ug/kg 07/28/22 11:41 78-59-107/27/22 03:474081821
1-Methylnaphthalene ND ug/kg 07/28/22 11:41 90-12-007/27/22 03:474081441
2-Methylnaphthalene ND ug/kg 07/28/22 11:41 91-57-607/27/22 03:474081631
2-Methylphenol(o-Cresol)ND ug/kg 07/28/22 11:41 95-48-707/27/22 03:474081671
3&4-Methylphenol(m&p Cresol)ND ug/kg 07/28/22 11:41 15831-10-407/27/22 03:474081651
Naphthalene ND ug/kg 07/28/22 11:41 91-20-307/27/22 03:474081391
2-Nitroaniline ND ug/kg 07/28/22 11:41 88-74-407/27/22 03:4720403341
3-Nitroaniline ND ug/kg 07/28/22 11:41 99-09-207/27/22 03:4720403211
4-Nitroaniline ND ug/kg 07/28/22 11:41 100-01-607/27/22 03:478173111
Nitrobenzene ND ug/kg 07/28/22 11:41 98-95-307/27/22 03:474081891
2-Nitrophenol ND ug/kg 07/28/22 11:41 88-75-507/27/22 03:474081771
4-Nitrophenol ND ug/kg 07/28/22 11:41 100-02-707/27/22 03:4720407901
N-Nitrosodimethylamine ND ug/kg 07/28/22 11:41 62-75-907/27/22 03:474081371
N-Nitroso-di-n-propylamine ND ug/kg 07/28/22 11:41 621-64-707/27/22 03:474081531
N-Nitrosodiphenylamine ND ug/kg 07/28/22 11:41 86-30-607/27/22 03:474081451
2,2'-Oxybis(1-chloropropane)ND ug/kg 07/28/22 11:41 108-60-107/27/22 03:474081941
Pentachlorophenol ND ug/kg 07/28/22 11:41 87-86-507/27/22 03:478174001
Phenanthrene ND ug/kg 07/28/22 11:41 85-01-807/27/22 03:474081341
Phenol ND ug/kg 07/28/22 11:41 108-95-207/27/22 03:474081821
Pyrene ND ug/kg 07/28/22 11:41 129-00-007/27/22 03:474081661
Pyridine ND ug/kg 07/28/22 11:41 110-86-107/27/22 03:474081291
1,2,4-Trichlorobenzene ND ug/kg 07/28/22 11:41 120-82-107/27/22 03:474081611
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:EXC-SIDE-1 Lab ID:92616378020 Collected:07/20/22 16:22 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,4,5-Trichlorophenol ND ug/kg 07/28/22 11:41 95-95-407/27/22 03:474081871
2,4,6-Trichlorophenol ND ug/kg 07/28/22 11:41 88-06-207/27/22 03:474081681
Surrogates
Nitrobenzene-d5 (S)68 %07/28/22 11:41 4165-60-007/27/22 03:4721-130 1
2-Fluorobiphenyl (S)68 %07/28/22 11:41 321-60-807/27/22 03:4719-130 1
Terphenyl-d14 (S)93 %07/28/22 11:41 1718-51-007/27/22 03:4715-130 1
Phenol-d6 (S)72 %07/28/22 11:41 13127-88-307/27/22 03:4718-130 1
2-Fluorophenol (S)72 %07/28/22 11:41 367-12-407/27/22 03:4718-130 1
2,4,6-Tribromophenol (S)94 %07/28/22 11:41 118-79-607/27/22 03:4718-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 07/26/22 17:34 67-64-107/25/22 16:0014847.4 1
Benzene ND ug/kg 07/26/22 17:34 71-43-207/25/22 16:007.4 2.9 1
Bromobenzene ND ug/kg 07/26/22 17:34 108-86-107/25/22 16:007.4 2.4 1
Bromochloromethane ND ug/kg 07/26/22 17:34 74-97-507/25/22 16:007.4 2.2 1
Bromodichloromethane ND ug/kg 07/26/22 17:34 75-27-407/25/22 16:007.4 2.8 1
Bromoform ND ug/kg 07/26/22 17:34 75-25-207/25/22 16:007.4 2.6 1
Bromomethane ND ug/kg 07/26/22 17:34 74-83-9 IK,v107/25/22 16:0014.8 11.7 1
2-Butanone (MEK)79.2J ug/kg 07/26/22 17:34 78-93-3 C707/25/22 16:0014835.4 1
n-Butylbenzene ND ug/kg 07/26/22 17:34 104-51-807/25/22 16:007.4 3.5 1
sec-Butylbenzene ND ug/kg 07/26/22 17:34 135-98-807/25/22 16:007.4 3.2 1
tert-Butylbenzene ND ug/kg 07/26/22 17:34 98-06-607/25/22 16:007.4 2.6 1
Carbon tetrachloride ND ug/kg 07/26/22 17:34 56-23-507/25/22 16:007.4 2.8 1
Chlorobenzene ND ug/kg 07/26/22 17:34 108-90-707/25/22 16:007.4 1.4 1
Chloroethane ND ug/kg 07/26/22 17:34 75-00-307/25/22 16:0014.8 5.7 1
Chloroform ND ug/kg 07/26/22 17:34 67-66-307/25/22 16:007.4 4.5 1
Chloromethane ND ug/kg 07/26/22 17:34 74-87-307/25/22 16:0014.8 6.2 1
2-Chlorotoluene ND ug/kg 07/26/22 17:34 95-49-807/25/22 16:007.4 2.6 1
4-Chlorotoluene ND ug/kg 07/26/22 17:34 106-43-407/25/22 16:007.4 1.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 07/26/22 17:34 96-12-8 IK07/25/22 16:007.4 2.9 1
Dibromochloromethane ND ug/kg 07/26/22 17:34 124-48-107/25/22 16:007.4 4.1 1
1,2-Dibromoethane (EDB)ND ug/kg 07/26/22 17:34 106-93-407/25/22 16:007.4 3.2 1
Dibromomethane ND ug/kg 07/26/22 17:34 74-95-307/25/22 16:007.4 1.6 1
1,2-Dichlorobenzene ND ug/kg 07/26/22 17:34 95-50-107/25/22 16:007.4 2.7 1
1,3-Dichlorobenzene ND ug/kg 07/26/22 17:34 541-73-107/25/22 16:007.4 2.3 1
1,4-Dichlorobenzene ND ug/kg 07/26/22 17:34 106-46-707/25/22 16:007.4 1.9 1
Dichlorodifluoromethane ND ug/kg 07/26/22 17:34 75-71-8 IH07/25/22 16:0014.8 3.2 1
1,1-Dichloroethane ND ug/kg 07/26/22 17:34 75-34-307/25/22 16:007.4 3.0 1
1,2-Dichloroethane ND ug/kg 07/26/22 17:34 107-06-207/25/22 16:007.4 4.9 1
1,1-Dichloroethene ND ug/kg 07/26/22 17:34 75-35-407/25/22 16:007.4 3.0 1
cis-1,2-Dichloroethene ND ug/kg 07/26/22 17:34 156-59-207/25/22 16:007.4 2.5 1
trans-1,2-Dichloroethene ND ug/kg 07/26/22 17:34 156-60-507/25/22 16:007.4 2.6 1
1,2-Dichloropropane ND ug/kg 07/26/22 17:34 78-87-507/25/22 16:007.4 2.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:EXC-SIDE-1 Lab ID:92616378020 Collected:07/20/22 16:22 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,3-Dichloropropane ND ug/kg 07/26/22 17:34 142-28-907/25/22 16:007.4 2.3 1
2,2-Dichloropropane ND ug/kg 07/26/22 17:34 594-20-7 v207/25/22 16:007.4 2.4 1
1,1-Dichloropropene ND ug/kg 07/26/22 17:34 563-58-607/25/22 16:007.4 3.5 1
cis-1,3-Dichloropropene ND ug/kg 07/26/22 17:34 10061-01-507/25/22 16:007.4 2.0 1
trans-1,3-Dichloropropene ND ug/kg 07/26/22 17:34 10061-02-607/25/22 16:007.4 2.5 1
Diisopropyl ether ND ug/kg 07/26/22 17:34 108-20-307/25/22 16:007.4 2.0 1
Ethylbenzene ND ug/kg 07/26/22 17:34 100-41-407/25/22 16:007.4 3.4 1
Hexachloro-1,3-butadiene ND ug/kg 07/26/22 17:34 87-68-307/25/22 16:0014.8 12.1 1
2-Hexanone ND ug/kg 07/26/22 17:34 591-78-607/25/22 16:0073.8 7.1 1
Isopropylbenzene (Cumene)ND ug/kg 07/26/22 17:34 98-82-807/25/22 16:007.4 2.5 1
p-Isopropyltoluene ND ug/kg 07/26/22 17:34 99-87-607/25/22 16:007.4 3.6 1
Methylene Chloride ND ug/kg 07/26/22 17:34 75-09-207/25/22 16:0029.5 20.2 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 07/26/22 17:34 108-10-107/25/22 16:0073.8 7.1 1
Methyl-tert-butyl ether ND ug/kg 07/26/22 17:34 1634-04-407/25/22 16:007.4 2.8 1
Naphthalene ND ug/kg 07/26/22 17:34 91-20-3 v207/25/22 16:007.4 3.9 1
n-Propylbenzene ND ug/kg 07/26/22 17:34 103-65-107/25/22 16:007.4 2.6 1
Styrene ND ug/kg 07/26/22 17:34 100-42-507/25/22 16:007.4 1.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 07/26/22 17:34 630-20-607/25/22 16:007.4 2.8 1
1,1,2,2-Tetrachloroethane ND ug/kg 07/26/22 17:34 79-34-507/25/22 16:007.4 1.9 1
Tetrachloroethene ND ug/kg 07/26/22 17:34 127-18-407/25/22 16:007.4 2.3 1
Toluene ND ug/kg 07/26/22 17:34 108-88-307/25/22 16:007.4 2.1 1
1,2,3-Trichlorobenzene ND ug/kg 07/26/22 17:34 87-61-6 IK,v207/25/22 16:007.4 6.0 1
1,2,4-Trichlorobenzene ND ug/kg 07/26/22 17:34 120-82-107/25/22 16:007.4 6.2 1
1,1,1-Trichloroethane ND ug/kg 07/26/22 17:34 71-55-607/25/22 16:007.4 3.8 1
1,1,2-Trichloroethane ND ug/kg 07/26/22 17:34 79-00-507/25/22 16:007.4 2.4 1
Trichloroethene ND ug/kg 07/26/22 17:34 79-01-607/25/22 16:007.4 1.9 1
Trichlorofluoromethane ND ug/kg 07/26/22 17:34 75-69-407/25/22 16:007.4 4.1 1
1,2,3-Trichloropropane ND ug/kg 07/26/22 17:34 96-18-407/25/22 16:007.4 3.7 1
1,2,4-Trimethylbenzene ND ug/kg 07/26/22 17:34 95-63-607/25/22 16:007.4 2.0 1
1,3,5-Trimethylbenzene ND ug/kg 07/26/22 17:34 108-67-807/25/22 16:007.4 2.5 1
Vinyl acetate ND ug/kg 07/26/22 17:34 108-05-407/25/22 16:0073.8 5.4 1
Vinyl chloride ND ug/kg 07/26/22 17:34 75-01-407/25/22 16:0014.8 3.7 1
Xylene (Total)ND ug/kg 07/26/22 17:34 1330-20-707/25/22 16:0014.8 4.2 1
m&p-Xylene ND ug/kg 07/26/22 17:34 179601-23-107/25/22 16:0014.8 5.0 1
o-Xylene ND ug/kg 07/26/22 17:34 95-47-607/25/22 16:007.4 3.3 1
Surrogates
Toluene-d8 (S)100 %07/26/22 17:34 2037-26-507/25/22 16:0070-130 1
4-Bromofluorobenzene (S)99 %07/26/22 17:34 460-00-407/25/22 16:0069-134 1
1,2-Dichloroethane-d4 (S)113 %07/26/22 17:34 17060-07-007/25/22 16:0070-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 19.5 %07/25/22 14:53 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:EXC-SIDE-1 Lab ID:92616378020 Collected:07/20/22 16:22 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 65.6 %08/03/22 11:0608/03/22 10:591
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:EXC-SIDE-2 Lab ID:92616378021 Collected:07/20/22 16:30 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP EPH Preparation Method: MA DEP/NJ DEP
Pace National - Mt. Juliet
TPH by Method MADEPE
Aliphatic (C09-C18)ND mg/kg 08/04/22 23:2308/02/22 15:259.26 3.09 1
Aliphatic (C19-C36)4.40J mg/kg 08/04/22 23:23 B,J08/02/22 15:259.26 3.09 1
Aromatic (C11-C22)4.68J mg/kg 08/05/22 01:58 B,J08/02/22 15:259.26 3.09 1
Total Extractable Hydrocarbons 9.08J mg/kg 08/05/22 01:58 TPH-TEH B,J08/02/22 15:259.26 3.09 1
Surrogates
o-Terphenyl (S)67.5 %08/05/22 01:58 84-15-108/02/22 15:2540.0-140 1
1-Chloro-octadecane (S)67.9 %08/04/22 23:23 3386-33-208/02/22 15:2540.0-140 1
2-Fluorobiphenyl (S)76.7 %08/05/22 01:58 321-60-808/02/22 15:2540.0-140 1
2-Bromonaphthalene (S)73.3 %08/05/22 01:58 580-13-208/02/22 15:2540.0-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Pace Analytical Services - Charlotte
VPH NC Soil
Aliphatic (C05-C08)ND mg/kg 07/23/22 03:14 N207/22/22 18:223.3 3.3 1
Aliphatic(C09-C12) Adjusted ND mg/kg 07/23/22 03:14 N207/22/22 18:223.3 3.3 1
Aromatic (C09-C10)ND mg/kg 07/23/22 03:14 N207/22/22 18:223.3 3.3 1
Surrogates
4-Bromofluorobenzene (FID) (S)98 %07/23/22 03:14 460-00-407/22/22 18:2270-130 1
4-Bromofluorobenzene (PID) (S)86 %07/23/22 03:14 460-00-407/22/22 18:2270-130 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 07/28/22 12:09 83-32-907/27/22 03:474031421
Acenaphthylene ND ug/kg 07/28/22 12:09 208-96-807/27/22 03:474031421
Aniline ND ug/kg 07/28/22 12:09 62-53-307/27/22 03:474031581
Anthracene ND ug/kg 07/28/22 12:09 120-12-707/27/22 03:474031321
Benzo(a)anthracene ND ug/kg 07/28/22 12:09 56-55-307/27/22 03:474031341
Benzo(a)pyrene ND ug/kg 07/28/22 12:09 50-32-807/27/22 03:474031391
Benzo(b)fluoranthene ND ug/kg 07/28/22 12:09 205-99-207/27/22 03:474031341
Benzo(g,h,i)perylene ND ug/kg 07/28/22 12:09 191-24-207/27/22 03:474031561
Benzo(k)fluoranthene ND ug/kg 07/28/22 12:09 207-08-907/27/22 03:474031421
Benzoic Acid ND ug/kg 07/28/22 12:09 65-85-007/27/22 03:4720208671
Benzyl alcohol ND ug/kg 07/28/22 12:09 100-51-607/27/22 03:478073061
4-Bromophenylphenyl ether ND ug/kg 07/28/22 12:09 101-55-307/27/22 03:474031551
Butylbenzylphthalate ND ug/kg 07/28/22 12:09 85-68-707/27/22 03:474031701
4-Chloro-3-methylphenol ND ug/kg 07/28/22 12:09 59-50-707/27/22 03:478072841
4-Chloroaniline ND ug/kg 07/28/22 12:09 106-47-807/27/22 03:478073171
bis(2-Chloroethoxy)methane ND ug/kg 07/28/22 12:09 111-91-107/27/22 03:474031671
bis(2-Chloroethyl) ether ND ug/kg 07/28/22 12:09 111-44-407/27/22 03:474031521
2-Chloronaphthalene ND ug/kg 07/28/22 12:09 91-58-707/27/22 03:474031601
2-Chlorophenol ND ug/kg 07/28/22 12:09 95-57-807/27/22 03:474031521
4-Chlorophenylphenyl ether ND ug/kg 07/28/22 12:09 7005-72-307/27/22 03:474031501
Chrysene ND ug/kg 07/28/22 12:09 218-01-907/27/22 03:474031471
Dibenz(a,h)anthracene ND ug/kg 07/28/22 12:09 53-70-307/27/22 03:474031551
Dibenzofuran ND ug/kg 07/28/22 12:09 132-64-907/27/22 03:474031451
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:EXC-SIDE-2 Lab ID:92616378021 Collected:07/20/22 16:30 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
1,2-Dichlorobenzene ND ug/kg 07/28/22 12:09 95-50-107/27/22 03:474031451
1,3-Dichlorobenzene ND ug/kg 07/28/22 12:09 541-73-107/27/22 03:474031431
1,4-Dichlorobenzene ND ug/kg 07/28/22 12:09 106-46-707/27/22 03:474031541
3,3'-Dichlorobenzidine ND ug/kg 07/28/22 12:09 91-94-107/27/22 03:478072731
2,4-Dichlorophenol ND ug/kg 07/28/22 12:09 120-83-207/27/22 03:474031581
Diethylphthalate ND ug/kg 07/28/22 12:09 84-66-207/27/22 03:474031481
2,4-Dimethylphenol ND ug/kg 07/28/22 12:09 105-67-907/27/22 03:474031671
Dimethylphthalate ND ug/kg 07/28/22 12:09 131-11-307/27/22 03:474031471
Di-n-butylphthalate ND ug/kg 07/28/22 12:09 84-74-207/27/22 03:474031361
4,6-Dinitro-2-methylphenol ND ug/kg 07/28/22 12:09 534-52-107/27/22 03:478073761
2,4-Dinitrophenol ND ug/kg 07/28/22 12:09 51-28-507/27/22 03:47202012501
2,4-Dinitrotoluene ND ug/kg 07/28/22 12:09 121-14-207/27/22 03:474031551
2,6-Dinitrotoluene ND ug/kg 07/28/22 12:09 606-20-207/27/22 03:474031481
Di-n-octylphthalate ND ug/kg 07/28/22 12:09 117-84-007/27/22 03:474031591
bis(2-Ethylhexyl)phthalate ND ug/kg 07/28/22 12:09 117-81-707/27/22 03:474031561
Fluoranthene ND ug/kg 07/28/22 12:09 206-44-007/27/22 03:474031381
Fluorene ND ug/kg 07/28/22 12:09 86-73-707/27/22 03:474031421
Hexachloro-1,3-butadiene ND ug/kg 07/28/22 12:09 87-68-307/27/22 03:474031751
Hexachlorobenzene ND ug/kg 07/28/22 12:09 118-74-107/27/22 03:474031581
Hexachlorocyclopentadiene ND ug/kg 07/28/22 12:09 77-47-407/27/22 03:474032311
Hexachloroethane ND ug/kg 07/28/22 12:09 67-72-107/27/22 03:474031541
Indeno(1,2,3-cd)pyrene ND ug/kg 07/28/22 12:09 193-39-507/27/22 03:474031591
Isophorone ND ug/kg 07/28/22 12:09 78-59-107/27/22 03:474031801
1-Methylnaphthalene ND ug/kg 07/28/22 12:09 90-12-007/27/22 03:474031421
2-Methylnaphthalene ND ug/kg 07/28/22 12:09 91-57-607/27/22 03:474031611
2-Methylphenol(o-Cresol)ND ug/kg 07/28/22 12:09 95-48-707/27/22 03:474031651
3&4-Methylphenol(m&p Cresol)ND ug/kg 07/28/22 12:09 15831-10-407/27/22 03:474031631
Naphthalene ND ug/kg 07/28/22 12:09 91-20-307/27/22 03:474031371
2-Nitroaniline ND ug/kg 07/28/22 12:09 88-74-407/27/22 03:4720203301
3-Nitroaniline ND ug/kg 07/28/22 12:09 99-09-207/27/22 03:4720203171
4-Nitroaniline ND ug/kg 07/28/22 12:09 100-01-607/27/22 03:478073071
Nitrobenzene ND ug/kg 07/28/22 12:09 98-95-307/27/22 03:474031871
2-Nitrophenol ND ug/kg 07/28/22 12:09 88-75-507/27/22 03:474031751
4-Nitrophenol ND ug/kg 07/28/22 12:09 100-02-707/27/22 03:4720207801
N-Nitrosodimethylamine ND ug/kg 07/28/22 12:09 62-75-907/27/22 03:474031361
N-Nitroso-di-n-propylamine ND ug/kg 07/28/22 12:09 621-64-707/27/22 03:474031521
N-Nitrosodiphenylamine ND ug/kg 07/28/22 12:09 86-30-607/27/22 03:474031431
2,2'-Oxybis(1-chloropropane)ND ug/kg 07/28/22 12:09 108-60-107/27/22 03:474031921
Pentachlorophenol ND ug/kg 07/28/22 12:09 87-86-507/27/22 03:478073951
Phenanthrene ND ug/kg 07/28/22 12:09 85-01-807/27/22 03:474031321
Phenol ND ug/kg 07/28/22 12:09 108-95-207/27/22 03:474031801
Pyrene ND ug/kg 07/28/22 12:09 129-00-007/27/22 03:474031641
Pyridine ND ug/kg 07/28/22 12:09 110-86-107/27/22 03:474031271
1,2,4-Trichlorobenzene ND ug/kg 07/28/22 12:09 120-82-107/27/22 03:474031591
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:EXC-SIDE-2 Lab ID:92616378021 Collected:07/20/22 16:30 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,4,5-Trichlorophenol ND ug/kg 07/28/22 12:09 95-95-407/27/22 03:474031851
2,4,6-Trichlorophenol ND ug/kg 07/28/22 12:09 88-06-207/27/22 03:474031661
Surrogates
Nitrobenzene-d5 (S)44 %07/28/22 12:09 4165-60-007/27/22 03:4721-130 1
2-Fluorobiphenyl (S)45 %07/28/22 12:09 321-60-807/27/22 03:4719-130 1
Terphenyl-d14 (S)79 %07/28/22 12:09 1718-51-007/27/22 03:4715-130 1
Phenol-d6 (S)48 %07/28/22 12:09 13127-88-307/27/22 03:4718-130 1
2-Fluorophenol (S)46 %07/28/22 12:09 367-12-407/27/22 03:4718-130 1
2,4,6-Tribromophenol (S)76 %07/28/22 12:09 118-79-607/27/22 03:4718-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 07/27/22 02:36 67-64-107/25/22 23:2014446.2 1
Benzene ND ug/kg 07/27/22 02:36 71-43-207/25/22 23:207.2 2.9 1
Bromobenzene ND ug/kg 07/27/22 02:36 108-86-107/25/22 23:207.2 2.3 1
Bromochloromethane ND ug/kg 07/27/22 02:36 74-97-507/25/22 23:207.2 2.1 1
Bromodichloromethane ND ug/kg 07/27/22 02:36 75-27-407/25/22 23:207.2 2.8 1
Bromoform ND ug/kg 07/27/22 02:36 75-25-207/25/22 23:207.2 2.5 1
Bromomethane ND ug/kg 07/27/22 02:36 74-83-9 IK,L1,v107/25/22 23:2014.4 11.4 1
2-Butanone (MEK)77.6J ug/kg 07/27/22 02:36 78-93-3 C707/25/22 23:2014434.5 1
n-Butylbenzene ND ug/kg 07/27/22 02:36 104-51-807/25/22 23:207.2 3.4 1
sec-Butylbenzene ND ug/kg 07/27/22 02:36 135-98-807/25/22 23:207.2 3.2 1
tert-Butylbenzene ND ug/kg 07/27/22 02:36 98-06-607/25/22 23:207.2 2.6 1
Carbon tetrachloride ND ug/kg 07/27/22 02:36 56-23-507/25/22 23:207.2 2.7 1
Chlorobenzene ND ug/kg 07/27/22 02:36 108-90-707/25/22 23:207.2 1.4 1
Chloroethane ND ug/kg 07/27/22 02:36 75-00-307/25/22 23:2014.4 5.6 1
Chloroform ND ug/kg 07/27/22 02:36 67-66-307/25/22 23:207.2 4.4 1
Chloromethane ND ug/kg 07/27/22 02:36 74-87-307/25/22 23:2014.4 6.0 1
2-Chlorotoluene ND ug/kg 07/27/22 02:36 95-49-807/25/22 23:207.2 2.5 1
4-Chlorotoluene ND ug/kg 07/27/22 02:36 106-43-407/25/22 23:207.2 1.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 07/27/22 02:36 96-12-8 IK07/25/22 23:207.2 2.8 1
Dibromochloromethane ND ug/kg 07/27/22 02:36 124-48-107/25/22 23:207.2 4.0 1
1,2-Dibromoethane (EDB)ND ug/kg 07/27/22 02:36 106-93-407/25/22 23:207.2 3.2 1
Dibromomethane ND ug/kg 07/27/22 02:36 74-95-307/25/22 23:207.2 1.5 1
1,2-Dichlorobenzene ND ug/kg 07/27/22 02:36 95-50-107/25/22 23:207.2 2.6 1
1,3-Dichlorobenzene ND ug/kg 07/27/22 02:36 541-73-107/25/22 23:207.2 2.2 1
1,4-Dichlorobenzene ND ug/kg 07/27/22 02:36 106-46-707/25/22 23:207.2 1.9 1
Dichlorodifluoromethane ND ug/kg 07/27/22 02:36 75-71-8 IH07/25/22 23:2014.4 3.1 1
1,1-Dichloroethane ND ug/kg 07/27/22 02:36 75-34-307/25/22 23:207.2 3.0 1
1,2-Dichloroethane ND ug/kg 07/27/22 02:36 107-06-207/25/22 23:207.2 4.8 1
1,1-Dichloroethene ND ug/kg 07/27/22 02:36 75-35-407/25/22 23:207.2 3.0 1
cis-1,2-Dichloroethene ND ug/kg 07/27/22 02:36 156-59-207/25/22 23:207.2 2.5 1
trans-1,2-Dichloroethene ND ug/kg 07/27/22 02:36 156-60-507/25/22 23:207.2 2.5 1
1,2-Dichloropropane ND ug/kg 07/27/22 02:36 78-87-507/25/22 23:207.2 2.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:EXC-SIDE-2 Lab ID:92616378021 Collected:07/20/22 16:30 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,3-Dichloropropane ND ug/kg 07/27/22 02:36 142-28-907/25/22 23:207.2 2.2 1
2,2-Dichloropropane ND ug/kg 07/27/22 02:36 594-20-707/25/22 23:207.2 2.3 1
1,1-Dichloropropene ND ug/kg 07/27/22 02:36 563-58-607/25/22 23:207.2 3.5 1
cis-1,3-Dichloropropene ND ug/kg 07/27/22 02:36 10061-01-507/25/22 23:207.2 2.0 1
trans-1,3-Dichloropropene ND ug/kg 07/27/22 02:36 10061-02-607/25/22 23:207.2 2.5 1
Diisopropyl ether ND ug/kg 07/27/22 02:36 108-20-307/25/22 23:207.2 1.9 1
Ethylbenzene ND ug/kg 07/27/22 02:36 100-41-407/25/22 23:207.2 3.4 1
Hexachloro-1,3-butadiene ND ug/kg 07/27/22 02:36 87-68-307/25/22 23:2014.4 11.8 1
2-Hexanone ND ug/kg 07/27/22 02:36 591-78-607/25/22 23:2071.9 6.9 1
Isopropylbenzene (Cumene)ND ug/kg 07/27/22 02:36 98-82-807/25/22 23:207.2 2.4 1
p-Isopropyltoluene ND ug/kg 07/27/22 02:36 99-87-607/25/22 23:207.2 3.5 1
Methylene Chloride ND ug/kg 07/27/22 02:36 75-09-207/25/22 23:2028.8 19.7 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 07/27/22 02:36 108-10-107/25/22 23:2071.9 6.9 1
Methyl-tert-butyl ether ND ug/kg 07/27/22 02:36 1634-04-407/25/22 23:207.2 2.7 1
Naphthalene ND ug/kg 07/27/22 02:36 91-20-3 v207/25/22 23:207.2 3.8 1
n-Propylbenzene ND ug/kg 07/27/22 02:36 103-65-107/25/22 23:207.2 2.6 1
Styrene ND ug/kg 07/27/22 02:36 100-42-507/25/22 23:207.2 1.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 07/27/22 02:36 630-20-607/25/22 23:207.2 2.8 1
1,1,2,2-Tetrachloroethane ND ug/kg 07/27/22 02:36 79-34-507/25/22 23:207.2 1.9 1
Tetrachloroethene ND ug/kg 07/27/22 02:36 127-18-407/25/22 23:207.2 2.3 1
Toluene ND ug/kg 07/27/22 02:36 108-88-307/25/22 23:207.2 2.0 1
1,2,3-Trichlorobenzene ND ug/kg 07/27/22 02:36 87-61-6 IK,v207/25/22 23:207.2 5.8 1
1,2,4-Trichlorobenzene ND ug/kg 07/27/22 02:36 120-82-107/25/22 23:207.2 6.0 1
1,1,1-Trichloroethane ND ug/kg 07/27/22 02:36 71-55-607/25/22 23:207.2 3.7 1
1,1,2-Trichloroethane ND ug/kg 07/27/22 02:36 79-00-507/25/22 23:207.2 2.4 1
Trichloroethene ND ug/kg 07/27/22 02:36 79-01-607/25/22 23:207.2 1.9 1
Trichlorofluoromethane ND ug/kg 07/27/22 02:36 75-69-407/25/22 23:207.2 4.0 1
1,2,3-Trichloropropane ND ug/kg 07/27/22 02:36 96-18-407/25/22 23:207.2 3.6 1
1,2,4-Trimethylbenzene ND ug/kg 07/27/22 02:36 95-63-607/25/22 23:207.2 2.0 1
1,3,5-Trimethylbenzene ND ug/kg 07/27/22 02:36 108-67-807/25/22 23:207.2 2.4 1
Vinyl acetate ND ug/kg 07/27/22 02:36 108-05-407/25/22 23:2071.9 5.2 1
Vinyl chloride ND ug/kg 07/27/22 02:36 75-01-407/25/22 23:2014.4 3.7 1
Xylene (Total)ND ug/kg 07/27/22 02:36 1330-20-707/25/22 23:2014.4 4.1 1
m&p-Xylene ND ug/kg 07/27/22 02:36 179601-23-107/25/22 23:2014.4 4.9 1
o-Xylene ND ug/kg 07/27/22 02:36 95-47-607/25/22 23:207.2 3.2 1
Surrogates
Toluene-d8 (S)100 %07/27/22 02:36 2037-26-507/25/22 23:2070-130 1
4-Bromofluorobenzene (S)97 %07/27/22 02:36 460-00-407/25/22 23:2069-134 1
1,2-Dichloroethane-d4 (S)105 %07/27/22 02:36 17060-07-007/25/22 23:2070-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 18.4 %07/25/22 14:53 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:EXC-SIDE-2 Lab ID:92616378021 Collected:07/20/22 16:30 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 70.2 %08/03/22 11:0608/03/22 10:591
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:EXC-SIDE-3 Lab ID:92616378022 Collected:07/20/22 16:37 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP EPH Preparation Method: MA DEP/NJ DEP
Pace National - Mt. Juliet
TPH by Method MADEPE
Aliphatic (C09-C18)ND mg/kg 08/04/22 23:4508/02/22 15:258.57 2.86 1
Aliphatic (C19-C36)4.05J mg/kg 08/04/22 23:45 B,J08/02/22 15:258.57 2.86 1
Aromatic (C11-C22)3.84J mg/kg 08/05/22 01:36 B,J08/02/22 15:258.57 2.86 1
Total Extractable Hydrocarbons 7.89J mg/kg 08/05/22 01:36 TPH-TEH B,J08/02/22 15:258.57 2.86 1
Surrogates
o-Terphenyl (S)63.3 %08/05/22 01:36 84-15-108/02/22 15:2540.0-140 1
1-Chloro-octadecane (S)61.9 %08/04/22 23:45 3386-33-208/02/22 15:2540.0-140 1
2-Fluorobiphenyl (S)84.3 %08/05/22 01:36 321-60-808/02/22 15:2540.0-140 1
2-Bromonaphthalene (S)80.7 %08/05/22 01:36 580-13-208/02/22 15:2540.0-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Pace Analytical Services - Charlotte
VPH NC Soil
Aliphatic (C05-C08)ND mg/kg 07/23/22 03:43 N207/22/22 18:223.1 3.1 1
Aliphatic(C09-C12) Adjusted ND mg/kg 07/23/22 03:43 N207/22/22 18:223.1 3.1 1
Aromatic (C09-C10)ND mg/kg 07/23/22 03:43 N207/22/22 18:223.1 3.1 1
Surrogates
4-Bromofluorobenzene (FID) (S)98 %07/23/22 03:43 460-00-407/22/22 18:2270-130 1
4-Bromofluorobenzene (PID) (S)86 %07/23/22 03:43 460-00-407/22/22 18:2270-130 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 07/28/22 12:38 83-32-907/27/22 03:474171471
Acenaphthylene ND ug/kg 07/28/22 12:38 208-96-807/27/22 03:474171471
Aniline ND ug/kg 07/28/22 12:38 62-53-307/27/22 03:474171631
Anthracene ND ug/kg 07/28/22 12:38 120-12-707/27/22 03:474171371
Benzo(a)anthracene ND ug/kg 07/28/22 12:38 56-55-307/27/22 03:474171391
Benzo(a)pyrene ND ug/kg 07/28/22 12:38 50-32-807/27/22 03:474171441
Benzo(b)fluoranthene ND ug/kg 07/28/22 12:38 205-99-207/27/22 03:474171391
Benzo(g,h,i)perylene ND ug/kg 07/28/22 12:38 191-24-207/27/22 03:474171621
Benzo(k)fluoranthene ND ug/kg 07/28/22 12:38 207-08-907/27/22 03:474171471
Benzoic Acid ND ug/kg 07/28/22 12:38 65-85-007/27/22 03:4720908961
Benzyl alcohol ND ug/kg 07/28/22 12:38 100-51-607/27/22 03:478353161
4-Bromophenylphenyl ether ND ug/kg 07/28/22 12:38 101-55-307/27/22 03:474171611
Butylbenzylphthalate ND ug/kg 07/28/22 12:38 85-68-707/27/22 03:474171761
4-Chloro-3-methylphenol ND ug/kg 07/28/22 12:38 59-50-707/27/22 03:478352931
4-Chloroaniline ND ug/kg 07/28/22 12:38 106-47-807/27/22 03:478353271
bis(2-Chloroethoxy)methane ND ug/kg 07/28/22 12:38 111-91-107/27/22 03:474171731
bis(2-Chloroethyl) ether ND ug/kg 07/28/22 12:38 111-44-407/27/22 03:474171571
2-Chloronaphthalene ND ug/kg 07/28/22 12:38 91-58-707/27/22 03:474171661
2-Chlorophenol ND ug/kg 07/28/22 12:38 95-57-807/27/22 03:474171571
4-Chlorophenylphenyl ether ND ug/kg 07/28/22 12:38 7005-72-307/27/22 03:474171561
Chrysene ND ug/kg 07/28/22 12:38 218-01-907/27/22 03:474171521
Dibenz(a,h)anthracene ND ug/kg 07/28/22 12:38 53-70-307/27/22 03:474171611
Dibenzofuran ND ug/kg 07/28/22 12:38 132-64-907/27/22 03:474171501
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:EXC-SIDE-3 Lab ID:92616378022 Collected:07/20/22 16:37 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
1,2-Dichlorobenzene ND ug/kg 07/28/22 12:38 95-50-107/27/22 03:474171501
1,3-Dichlorobenzene ND ug/kg 07/28/22 12:38 541-73-107/27/22 03:474171481
1,4-Dichlorobenzene ND ug/kg 07/28/22 12:38 106-46-707/27/22 03:474171591
3,3'-Dichlorobenzidine ND ug/kg 07/28/22 12:38 91-94-107/27/22 03:478352821
2,4-Dichlorophenol ND ug/kg 07/28/22 12:38 120-83-207/27/22 03:474171631
Diethylphthalate ND ug/kg 07/28/22 12:38 84-66-207/27/22 03:474171531
2,4-Dimethylphenol ND ug/kg 07/28/22 12:38 105-67-907/27/22 03:474171731
Dimethylphthalate ND ug/kg 07/28/22 12:38 131-11-307/27/22 03:474171521
Di-n-butylphthalate ND ug/kg 07/28/22 12:38 84-74-207/27/22 03:474171401
4,6-Dinitro-2-methylphenol ND ug/kg 07/28/22 12:38 534-52-107/27/22 03:478353891
2,4-Dinitrophenol ND ug/kg 07/28/22 12:38 51-28-507/27/22 03:47209012901
2,4-Dinitrotoluene ND ug/kg 07/28/22 12:38 121-14-207/27/22 03:474171611
2,6-Dinitrotoluene ND ug/kg 07/28/22 12:38 606-20-207/27/22 03:474171531
Di-n-octylphthalate ND ug/kg 07/28/22 12:38 117-84-007/27/22 03:474171641
bis(2-Ethylhexyl)phthalate ND ug/kg 07/28/22 12:38 117-81-707/27/22 03:474171621
Fluoranthene ND ug/kg 07/28/22 12:38 206-44-007/27/22 03:474171431
Fluorene ND ug/kg 07/28/22 12:38 86-73-707/27/22 03:474171471
Hexachloro-1,3-butadiene ND ug/kg 07/28/22 12:38 87-68-307/27/22 03:474171811
Hexachlorobenzene ND ug/kg 07/28/22 12:38 118-74-107/27/22 03:474171631
Hexachlorocyclopentadiene ND ug/kg 07/28/22 12:38 77-47-407/27/22 03:474172391
Hexachloroethane ND ug/kg 07/28/22 12:38 67-72-107/27/22 03:474171591
Indeno(1,2,3-cd)pyrene ND ug/kg 07/28/22 12:38 193-39-507/27/22 03:474171641
Isophorone ND ug/kg 07/28/22 12:38 78-59-107/27/22 03:474171861
1-Methylnaphthalene ND ug/kg 07/28/22 12:38 90-12-007/27/22 03:474171471
2-Methylnaphthalene ND ug/kg 07/28/22 12:38 91-57-607/27/22 03:474171671
2-Methylphenol(o-Cresol)ND ug/kg 07/28/22 12:38 95-48-707/27/22 03:474171711
3&4-Methylphenol(m&p Cresol)ND ug/kg 07/28/22 12:38 15831-10-407/27/22 03:474171681
Naphthalene ND ug/kg 07/28/22 12:38 91-20-307/27/22 03:474171421
2-Nitroaniline ND ug/kg 07/28/22 12:38 88-74-407/27/22 03:4720903411
3-Nitroaniline ND ug/kg 07/28/22 12:38 99-09-207/27/22 03:4720903271
4-Nitroaniline ND ug/kg 07/28/22 12:38 100-01-607/27/22 03:478353171
Nitrobenzene ND ug/kg 07/28/22 12:38 98-95-307/27/22 03:474171931
2-Nitrophenol ND ug/kg 07/28/22 12:38 88-75-507/27/22 03:474171811
4-Nitrophenol ND ug/kg 07/28/22 12:38 100-02-707/27/22 03:4720908071
N-Nitrosodimethylamine ND ug/kg 07/28/22 12:38 62-75-907/27/22 03:474171401
N-Nitroso-di-n-propylamine ND ug/kg 07/28/22 12:38 621-64-707/27/22 03:474171571
N-Nitrosodiphenylamine ND ug/kg 07/28/22 12:38 86-30-607/27/22 03:474171481
2,2'-Oxybis(1-chloropropane)ND ug/kg 07/28/22 12:38 108-60-107/27/22 03:474171991
Pentachlorophenol ND ug/kg 07/28/22 12:38 87-86-507/27/22 03:478354081
Phenanthrene ND ug/kg 07/28/22 12:38 85-01-807/27/22 03:474171371
Phenol ND ug/kg 07/28/22 12:38 108-95-207/27/22 03:474171861
Pyrene ND ug/kg 07/28/22 12:38 129-00-007/27/22 03:474171691
Pyridine ND ug/kg 07/28/22 12:38 110-86-107/27/22 03:474171321
1,2,4-Trichlorobenzene ND ug/kg 07/28/22 12:38 120-82-107/27/22 03:474171641
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:EXC-SIDE-3 Lab ID:92616378022 Collected:07/20/22 16:37 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,4,5-Trichlorophenol ND ug/kg 07/28/22 12:38 95-95-407/27/22 03:474171911
2,4,6-Trichlorophenol ND ug/kg 07/28/22 12:38 88-06-207/27/22 03:474171721
Surrogates
Nitrobenzene-d5 (S)63 %07/28/22 12:38 4165-60-007/27/22 03:4721-130 1
2-Fluorobiphenyl (S)64 %07/28/22 12:38 321-60-807/27/22 03:4719-130 1
Terphenyl-d14 (S)84 %07/28/22 12:38 1718-51-007/27/22 03:4715-130 1
Phenol-d6 (S)65 %07/28/22 12:38 13127-88-307/27/22 03:4718-130 1
2-Fluorophenol (S)66 %07/28/22 12:38 367-12-407/27/22 03:4718-130 1
2,4,6-Tribromophenol (S)79 %07/28/22 12:38 118-79-607/27/22 03:4718-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 07/27/22 02:54 67-64-107/25/22 23:2014446.1 1
Benzene ND ug/kg 07/27/22 02:54 71-43-207/25/22 23:207.2 2.9 1
Bromobenzene ND ug/kg 07/27/22 02:54 108-86-107/25/22 23:207.2 2.3 1
Bromochloromethane ND ug/kg 07/27/22 02:54 74-97-507/25/22 23:207.2 2.1 1
Bromodichloromethane ND ug/kg 07/27/22 02:54 75-27-407/25/22 23:207.2 2.8 1
Bromoform ND ug/kg 07/27/22 02:54 75-25-207/25/22 23:207.2 2.5 1
Bromomethane ND ug/kg 07/27/22 02:54 74-83-9 IK,L1,v107/25/22 23:2014.4 11.4 1
2-Butanone (MEK)80.9J ug/kg 07/27/22 02:54 78-93-3 C707/25/22 23:2014434.5 1
n-Butylbenzene ND ug/kg 07/27/22 02:54 104-51-807/25/22 23:207.2 3.4 1
sec-Butylbenzene ND ug/kg 07/27/22 02:54 135-98-807/25/22 23:207.2 3.2 1
tert-Butylbenzene ND ug/kg 07/27/22 02:54 98-06-607/25/22 23:207.2 2.6 1
Carbon tetrachloride ND ug/kg 07/27/22 02:54 56-23-507/25/22 23:207.2 2.7 1
Chlorobenzene ND ug/kg 07/27/22 02:54 108-90-707/25/22 23:207.2 1.4 1
Chloroethane ND ug/kg 07/27/22 02:54 75-00-307/25/22 23:2014.4 5.5 1
Chloroform ND ug/kg 07/27/22 02:54 67-66-307/25/22 23:207.2 4.4 1
Chloromethane ND ug/kg 07/27/22 02:54 74-87-3 M107/25/22 23:2014.4 6.0 1
2-Chlorotoluene ND ug/kg 07/27/22 02:54 95-49-807/25/22 23:207.2 2.5 1
4-Chlorotoluene ND ug/kg 07/27/22 02:54 106-43-407/25/22 23:207.2 1.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 07/27/22 02:54 96-12-8 IK07/25/22 23:207.2 2.8 1
Dibromochloromethane ND ug/kg 07/27/22 02:54 124-48-107/25/22 23:207.2 4.0 1
1,2-Dibromoethane (EDB)ND ug/kg 07/27/22 02:54 106-93-407/25/22 23:207.2 3.2 1
Dibromomethane ND ug/kg 07/27/22 02:54 74-95-307/25/22 23:207.2 1.5 1
1,2-Dichlorobenzene ND ug/kg 07/27/22 02:54 95-50-107/25/22 23:207.2 2.6 1
1,3-Dichlorobenzene ND ug/kg 07/27/22 02:54 541-73-107/25/22 23:207.2 2.2 1
1,4-Dichlorobenzene ND ug/kg 07/27/22 02:54 106-46-707/25/22 23:207.2 1.9 1
Dichlorodifluoromethane ND ug/kg 07/27/22 02:54 75-71-8 IH,M107/25/22 23:2014.4 3.1 1
1,1-Dichloroethane ND ug/kg 07/27/22 02:54 75-34-307/25/22 23:207.2 3.0 1
1,2-Dichloroethane ND ug/kg 07/27/22 02:54 107-06-207/25/22 23:207.2 4.8 1
1,1-Dichloroethene ND ug/kg 07/27/22 02:54 75-35-407/25/22 23:207.2 3.0 1
cis-1,2-Dichloroethene ND ug/kg 07/27/22 02:54 156-59-207/25/22 23:207.2 2.5 1
trans-1,2-Dichloroethene ND ug/kg 07/27/22 02:54 156-60-507/25/22 23:207.2 2.5 1
1,2-Dichloropropane ND ug/kg 07/27/22 02:54 78-87-507/25/22 23:207.2 2.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:EXC-SIDE-3 Lab ID:92616378022 Collected:07/20/22 16:37 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,3-Dichloropropane ND ug/kg 07/27/22 02:54 142-28-907/25/22 23:207.2 2.2 1
2,2-Dichloropropane ND ug/kg 07/27/22 02:54 594-20-707/25/22 23:207.2 2.3 1
1,1-Dichloropropene ND ug/kg 07/27/22 02:54 563-58-607/25/22 23:207.2 3.4 1
cis-1,3-Dichloropropene ND ug/kg 07/27/22 02:54 10061-01-507/25/22 23:207.2 2.0 1
trans-1,3-Dichloropropene ND ug/kg 07/27/22 02:54 10061-02-607/25/22 23:207.2 2.5 1
Diisopropyl ether ND ug/kg 07/27/22 02:54 108-20-307/25/22 23:207.2 1.9 1
Ethylbenzene ND ug/kg 07/27/22 02:54 100-41-407/25/22 23:207.2 3.3 1
Hexachloro-1,3-butadiene ND ug/kg 07/27/22 02:54 87-68-307/25/22 23:2014.4 11.8 1
2-Hexanone ND ug/kg 07/27/22 02:54 591-78-607/25/22 23:2071.8 6.9 1
Isopropylbenzene (Cumene)ND ug/kg 07/27/22 02:54 98-82-807/25/22 23:207.2 2.4 1
p-Isopropyltoluene ND ug/kg 07/27/22 02:54 99-87-607/25/22 23:207.2 3.5 1
Methylene Chloride ND ug/kg 07/27/22 02:54 75-09-207/25/22 23:2028.7 19.7 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 07/27/22 02:54 108-10-107/25/22 23:2071.8 6.9 1
Methyl-tert-butyl ether ND ug/kg 07/27/22 02:54 1634-04-407/25/22 23:207.2 2.7 1
Naphthalene ND ug/kg 07/27/22 02:54 91-20-3 v207/25/22 23:207.2 3.8 1
n-Propylbenzene ND ug/kg 07/27/22 02:54 103-65-107/25/22 23:207.2 2.6 1
Styrene ND ug/kg 07/27/22 02:54 100-42-507/25/22 23:207.2 1.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 07/27/22 02:54 630-20-607/25/22 23:207.2 2.8 1
1,1,2,2-Tetrachloroethane ND ug/kg 07/27/22 02:54 79-34-507/25/22 23:207.2 1.9 1
Tetrachloroethene ND ug/kg 07/27/22 02:54 127-18-407/25/22 23:207.2 2.3 1
Toluene ND ug/kg 07/27/22 02:54 108-88-307/25/22 23:207.2 2.0 1
1,2,3-Trichlorobenzene ND ug/kg 07/27/22 02:54 87-61-6 IK,v207/25/22 23:207.2 5.8 1
1,2,4-Trichlorobenzene ND ug/kg 07/27/22 02:54 120-82-107/25/22 23:207.2 6.0 1
1,1,1-Trichloroethane ND ug/kg 07/27/22 02:54 71-55-607/25/22 23:207.2 3.7 1
1,1,2-Trichloroethane ND ug/kg 07/27/22 02:54 79-00-507/25/22 23:207.2 2.4 1
Trichloroethene ND ug/kg 07/27/22 02:54 79-01-607/25/22 23:207.2 1.9 1
Trichlorofluoromethane ND ug/kg 07/27/22 02:54 75-69-407/25/22 23:207.2 4.0 1
1,2,3-Trichloropropane ND ug/kg 07/27/22 02:54 96-18-407/25/22 23:207.2 3.6 1
1,2,4-Trimethylbenzene ND ug/kg 07/27/22 02:54 95-63-607/25/22 23:207.2 2.0 1
1,3,5-Trimethylbenzene ND ug/kg 07/27/22 02:54 108-67-807/25/22 23:207.2 2.4 1
Vinyl acetate ND ug/kg 07/27/22 02:54 108-05-407/25/22 23:2071.8 5.2 1
Vinyl chloride ND ug/kg 07/27/22 02:54 75-01-407/25/22 23:2014.4 3.6 1
Xylene (Total)ND ug/kg 07/27/22 02:54 1330-20-707/25/22 23:2014.4 4.1 1
m&p-Xylene ND ug/kg 07/27/22 02:54 179601-23-107/25/22 23:2014.4 4.9 1
o-Xylene ND ug/kg 07/27/22 02:54 95-47-607/25/22 23:207.2 3.2 1
Surrogates
Toluene-d8 (S)101 %07/27/22 02:54 2037-26-507/25/22 23:2070-130 1
4-Bromofluorobenzene (S)98 %07/27/22 02:54 460-00-407/25/22 23:2069-134 1
1,2-Dichloroethane-d4 (S)109 %07/27/22 02:54 17060-07-007/25/22 23:2070-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 21.2 %07/25/22 14:53 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:EXC-SIDE-3 Lab ID:92616378022 Collected:07/20/22 16:37 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 75.8 %08/03/22 11:0608/03/22 10:591
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:PL-BASE (12)Lab ID:92616378023 Collected:07/19/22 16:45 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP EPH Preparation Method: MA DEP/NJ DEP
Pace National - Mt. Juliet
TPH by Method MADEPE
Aliphatic (C09-C18)ND mg/kg 08/05/22 00:0708/02/22 15:259.03 3.02 1
Aliphatic (C19-C36)3.54J mg/kg 08/05/22 00:07 B,J08/02/22 15:259.03 3.02 1
Aromatic (C11-C22)3.49J mg/kg 08/05/22 01:14 B,J08/02/22 15:259.03 3.02 1
Total Extractable Hydrocarbons 7.03J mg/kg 08/05/22 01:14 TPH-TEH B,J08/02/22 15:259.03 3.02 1
Surrogates
o-Terphenyl (S)68.0 %08/05/22 01:14 84-15-108/02/22 15:2540.0-140 1
1-Chloro-octadecane (S)63.6 %08/05/22 00:07 3386-33-208/02/22 15:2540.0-140 1
2-Fluorobiphenyl (S)83.0 %08/05/22 01:14 321-60-808/02/22 15:2540.0-140 1
2-Bromonaphthalene (S)79.4 %08/05/22 01:14 580-13-208/02/22 15:2540.0-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Pace Analytical Services - Charlotte
VPH NC Soil
Aliphatic (C05-C08)ND mg/kg 07/23/22 04:11 N207/22/22 18:223.0 3.0 1
Aliphatic(C09-C12) Adjusted ND mg/kg 07/23/22 04:11 N207/22/22 18:223.0 3.0 1
Aromatic (C09-C10)ND mg/kg 07/23/22 04:11 N207/22/22 18:223.0 3.0 1
Surrogates
4-Bromofluorobenzene (FID) (S)98 %07/23/22 04:11 460-00-407/22/22 18:2270-130 1
4-Bromofluorobenzene (PID) (S)85 %07/23/22 04:11 460-00-407/22/22 18:2270-130 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 07/28/22 13:06 83-32-907/27/22 03:474161461
Acenaphthylene ND ug/kg 07/28/22 13:06 208-96-807/27/22 03:474161461
Aniline ND ug/kg 07/28/22 13:06 62-53-307/27/22 03:474161631
Anthracene ND ug/kg 07/28/22 13:06 120-12-707/27/22 03:474161361
Benzo(a)anthracene ND ug/kg 07/28/22 13:06 56-55-307/27/22 03:474161391
Benzo(a)pyrene ND ug/kg 07/28/22 13:06 50-32-807/27/22 03:474161441
Benzo(b)fluoranthene ND ug/kg 07/28/22 13:06 205-99-207/27/22 03:474161391
Benzo(g,h,i)perylene ND ug/kg 07/28/22 13:06 191-24-207/27/22 03:474161621
Benzo(k)fluoranthene ND ug/kg 07/28/22 13:06 207-08-907/27/22 03:474161461
Benzoic Acid ND ug/kg 07/28/22 13:06 65-85-007/27/22 03:4720808951
Benzyl alcohol ND ug/kg 07/28/22 13:06 100-51-607/27/22 03:478333151
4-Bromophenylphenyl ether ND ug/kg 07/28/22 13:06 101-55-307/27/22 03:474161601
Butylbenzylphthalate ND ug/kg 07/28/22 13:06 85-68-707/27/22 03:474161751
4-Chloro-3-methylphenol ND ug/kg 07/28/22 13:06 59-50-707/27/22 03:478332931
4-Chloroaniline ND ug/kg 07/28/22 13:06 106-47-807/27/22 03:478333271
bis(2-Chloroethoxy)methane ND ug/kg 07/28/22 13:06 111-91-107/27/22 03:474161731
bis(2-Chloroethyl) ether ND ug/kg 07/28/22 13:06 111-44-407/27/22 03:474161561
2-Chloronaphthalene ND ug/kg 07/28/22 13:06 91-58-707/27/22 03:474161651
2-Chlorophenol ND ug/kg 07/28/22 13:06 95-57-807/27/22 03:474161561
4-Chlorophenylphenyl ether ND ug/kg 07/28/22 13:06 7005-72-307/27/22 03:474161551
Chrysene ND ug/kg 07/28/22 13:06 218-01-907/27/22 03:474161511
Dibenz(a,h)anthracene ND ug/kg 07/28/22 13:06 53-70-307/27/22 03:474161601
Dibenzofuran ND ug/kg 07/28/22 13:06 132-64-907/27/22 03:474161501
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:PL-BASE (12)Lab ID:92616378023 Collected:07/19/22 16:45 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
1,2-Dichlorobenzene ND ug/kg 07/28/22 13:06 95-50-107/27/22 03:474161501
1,3-Dichlorobenzene ND ug/kg 07/28/22 13:06 541-73-107/27/22 03:474161481
1,4-Dichlorobenzene ND ug/kg 07/28/22 13:06 106-46-707/27/22 03:474161591
3,3'-Dichlorobenzidine ND ug/kg 07/28/22 13:06 91-94-107/27/22 03:478332811
2,4-Dichlorophenol ND ug/kg 07/28/22 13:06 120-83-207/27/22 03:474161631
Diethylphthalate ND ug/kg 07/28/22 13:06 84-66-207/27/22 03:474161531
2,4-Dimethylphenol ND ug/kg 07/28/22 13:06 105-67-907/27/22 03:474161731
Dimethylphthalate ND ug/kg 07/28/22 13:06 131-11-307/27/22 03:474161511
Di-n-butylphthalate ND ug/kg 07/28/22 13:06 84-74-207/27/22 03:474161401
4,6-Dinitro-2-methylphenol ND ug/kg 07/28/22 13:06 534-52-107/27/22 03:478333891
2,4-Dinitrophenol ND ug/kg 07/28/22 13:06 51-28-507/27/22 03:47208012901
2,4-Dinitrotoluene ND ug/kg 07/28/22 13:06 121-14-207/27/22 03:474161601
2,6-Dinitrotoluene ND ug/kg 07/28/22 13:06 606-20-207/27/22 03:474161531
Di-n-octylphthalate ND ug/kg 07/28/22 13:06 117-84-007/27/22 03:474161641
bis(2-Ethylhexyl)phthalate ND ug/kg 07/28/22 13:06 117-81-707/27/22 03:474161621
Fluoranthene ND ug/kg 07/28/22 13:06 206-44-007/27/22 03:474161431
Fluorene ND ug/kg 07/28/22 13:06 86-73-707/27/22 03:474161461
Hexachloro-1,3-butadiene ND ug/kg 07/28/22 13:06 87-68-307/27/22 03:474161801
Hexachlorobenzene ND ug/kg 07/28/22 13:06 118-74-107/27/22 03:474161631
Hexachlorocyclopentadiene ND ug/kg 07/28/22 13:06 77-47-407/27/22 03:474162381
Hexachloroethane ND ug/kg 07/28/22 13:06 67-72-107/27/22 03:474161591
Indeno(1,2,3-cd)pyrene ND ug/kg 07/28/22 13:06 193-39-507/27/22 03:474161641
Isophorone ND ug/kg 07/28/22 13:06 78-59-107/27/22 03:474161851
1-Methylnaphthalene ND ug/kg 07/28/22 13:06 90-12-007/27/22 03:474161461
2-Methylnaphthalene ND ug/kg 07/28/22 13:06 91-57-607/27/22 03:474161671
2-Methylphenol(o-Cresol)ND ug/kg 07/28/22 13:06 95-48-707/27/22 03:474161701
3&4-Methylphenol(m&p Cresol)ND ug/kg 07/28/22 13:06 15831-10-407/27/22 03:474161681
Naphthalene ND ug/kg 07/28/22 13:06 91-20-307/27/22 03:474161411
2-Nitroaniline ND ug/kg 07/28/22 13:06 88-74-407/27/22 03:4720803411
3-Nitroaniline ND ug/kg 07/28/22 13:06 99-09-207/27/22 03:4720803271
4-Nitroaniline ND ug/kg 07/28/22 13:06 100-01-607/27/22 03:478333171
Nitrobenzene ND ug/kg 07/28/22 13:06 98-95-307/27/22 03:474161931
2-Nitrophenol ND ug/kg 07/28/22 13:06 88-75-507/27/22 03:474161801
4-Nitrophenol ND ug/kg 07/28/22 13:06 100-02-707/27/22 03:4720808051
N-Nitrosodimethylamine ND ug/kg 07/28/22 13:06 62-75-907/27/22 03:474161401
N-Nitroso-di-n-propylamine ND ug/kg 07/28/22 13:06 621-64-707/27/22 03:474161561
N-Nitrosodiphenylamine ND ug/kg 07/28/22 13:06 86-30-607/27/22 03:474161481
2,2'-Oxybis(1-chloropropane)ND ug/kg 07/28/22 13:06 108-60-107/27/22 03:474161981
Pentachlorophenol ND ug/kg 07/28/22 13:06 87-86-507/27/22 03:478334081
Phenanthrene ND ug/kg 07/28/22 13:06 85-01-807/27/22 03:474161361
Phenol ND ug/kg 07/28/22 13:06 108-95-207/27/22 03:474161851
Pyrene ND ug/kg 07/28/22 13:06 129-00-007/27/22 03:474161691
Pyridine ND ug/kg 07/28/22 13:06 110-86-107/27/22 03:474161311
1,2,4-Trichlorobenzene ND ug/kg 07/28/22 13:06 120-82-107/27/22 03:474161641
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:PL-BASE (12)Lab ID:92616378023 Collected:07/19/22 16:45 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,4,5-Trichlorophenol ND ug/kg 07/28/22 13:06 95-95-407/27/22 03:474161911
2,4,6-Trichlorophenol ND ug/kg 07/28/22 13:06 88-06-207/27/22 03:474161721
Surrogates
Nitrobenzene-d5 (S)67 %07/28/22 13:06 4165-60-007/27/22 03:4721-130 1
2-Fluorobiphenyl (S)68 %07/28/22 13:06 321-60-807/27/22 03:4719-130 1
Terphenyl-d14 (S)86 %07/28/22 13:06 1718-51-007/27/22 03:4715-130 1
Phenol-d6 (S)68 %07/28/22 13:06 13127-88-307/27/22 03:4718-130 1
2-Fluorophenol (S)71 %07/28/22 13:06 367-12-407/27/22 03:4718-130 1
2,4,6-Tribromophenol (S)83 %07/28/22 13:06 118-79-607/27/22 03:4718-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 07/27/22 03:13 67-64-107/25/22 23:2014747.2 1
Benzene ND ug/kg 07/27/22 03:13 71-43-207/25/22 23:207.4 2.9 1
Bromobenzene ND ug/kg 07/27/22 03:13 108-86-107/25/22 23:207.4 2.4 1
Bromochloromethane ND ug/kg 07/27/22 03:13 74-97-507/25/22 23:207.4 2.2 1
Bromodichloromethane ND ug/kg 07/27/22 03:13 75-27-407/25/22 23:207.4 2.8 1
Bromoform ND ug/kg 07/27/22 03:13 75-25-207/25/22 23:207.4 2.6 1
Bromomethane ND ug/kg 07/27/22 03:13 74-83-9 IK,L1,v107/25/22 23:2014.7 11.6 1
2-Butanone (MEK)55.0J ug/kg 07/27/22 03:13 78-93-3 C707/25/22 23:2014735.3 1
n-Butylbenzene ND ug/kg 07/27/22 03:13 104-51-807/25/22 23:207.4 3.5 1
sec-Butylbenzene ND ug/kg 07/27/22 03:13 135-98-807/25/22 23:207.4 3.2 1
tert-Butylbenzene ND ug/kg 07/27/22 03:13 98-06-607/25/22 23:207.4 2.6 1
Carbon tetrachloride ND ug/kg 07/27/22 03:13 56-23-507/25/22 23:207.4 2.8 1
Chlorobenzene ND ug/kg 07/27/22 03:13 108-90-707/25/22 23:207.4 1.4 1
Chloroethane ND ug/kg 07/27/22 03:13 75-00-307/25/22 23:2014.7 5.7 1
Chloroform ND ug/kg 07/27/22 03:13 67-66-307/25/22 23:207.4 4.5 1
Chloromethane ND ug/kg 07/27/22 03:13 74-87-307/25/22 23:2014.7 6.2 1
2-Chlorotoluene ND ug/kg 07/27/22 03:13 95-49-807/25/22 23:207.4 2.6 1
4-Chlorotoluene ND ug/kg 07/27/22 03:13 106-43-407/25/22 23:207.4 1.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 07/27/22 03:13 96-12-8 IK07/25/22 23:207.4 2.9 1
Dibromochloromethane ND ug/kg 07/27/22 03:13 124-48-107/25/22 23:207.4 4.1 1
1,2-Dibromoethane (EDB)ND ug/kg 07/27/22 03:13 106-93-407/25/22 23:207.4 3.2 1
Dibromomethane ND ug/kg 07/27/22 03:13 74-95-307/25/22 23:207.4 1.6 1
1,2-Dichlorobenzene ND ug/kg 07/27/22 03:13 95-50-107/25/22 23:207.4 2.6 1
1,3-Dichlorobenzene ND ug/kg 07/27/22 03:13 541-73-107/25/22 23:207.4 2.3 1
1,4-Dichlorobenzene ND ug/kg 07/27/22 03:13 106-46-707/25/22 23:207.4 1.9 1
Dichlorodifluoromethane ND ug/kg 07/27/22 03:13 75-71-8 IH07/25/22 23:2014.7 3.2 1
1,1-Dichloroethane ND ug/kg 07/27/22 03:13 75-34-307/25/22 23:207.4 3.0 1
1,2-Dichloroethane ND ug/kg 07/27/22 03:13 107-06-207/25/22 23:207.4 4.9 1
1,1-Dichloroethene ND ug/kg 07/27/22 03:13 75-35-407/25/22 23:207.4 3.0 1
cis-1,2-Dichloroethene ND ug/kg 07/27/22 03:13 156-59-207/25/22 23:207.4 2.5 1
trans-1,2-Dichloroethene ND ug/kg 07/27/22 03:13 156-60-507/25/22 23:207.4 2.6 1
1,2-Dichloropropane ND ug/kg 07/27/22 03:13 78-87-507/25/22 23:207.4 2.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:PL-BASE (12)Lab ID:92616378023 Collected:07/19/22 16:45 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,3-Dichloropropane ND ug/kg 07/27/22 03:13 142-28-907/25/22 23:207.4 2.3 1
2,2-Dichloropropane ND ug/kg 07/27/22 03:13 594-20-707/25/22 23:207.4 2.4 1
1,1-Dichloropropene ND ug/kg 07/27/22 03:13 563-58-607/25/22 23:207.4 3.5 1
cis-1,3-Dichloropropene ND ug/kg 07/27/22 03:13 10061-01-507/25/22 23:207.4 2.0 1
trans-1,3-Dichloropropene ND ug/kg 07/27/22 03:13 10061-02-607/25/22 23:207.4 2.5 1
Diisopropyl ether ND ug/kg 07/27/22 03:13 108-20-307/25/22 23:207.4 2.0 1
Ethylbenzene ND ug/kg 07/27/22 03:13 100-41-407/25/22 23:207.4 3.4 1
Hexachloro-1,3-butadiene ND ug/kg 07/27/22 03:13 87-68-307/25/22 23:2014.7 12.0 1
2-Hexanone ND ug/kg 07/27/22 03:13 591-78-607/25/22 23:2073.5 7.1 1
Isopropylbenzene (Cumene)ND ug/kg 07/27/22 03:13 98-82-807/25/22 23:207.4 2.5 1
p-Isopropyltoluene ND ug/kg 07/27/22 03:13 99-87-607/25/22 23:207.4 3.6 1
Methylene Chloride ND ug/kg 07/27/22 03:13 75-09-207/25/22 23:2029.4 20.1 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 07/27/22 03:13 108-10-107/25/22 23:2073.5 7.1 1
Methyl-tert-butyl ether ND ug/kg 07/27/22 03:13 1634-04-407/25/22 23:207.4 2.8 1
Naphthalene ND ug/kg 07/27/22 03:13 91-20-3 v207/25/22 23:207.4 3.9 1
n-Propylbenzene ND ug/kg 07/27/22 03:13 103-65-107/25/22 23:207.4 2.6 1
Styrene ND ug/kg 07/27/22 03:13 100-42-507/25/22 23:207.4 1.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 07/27/22 03:13 630-20-607/25/22 23:207.4 2.8 1
1,1,2,2-Tetrachloroethane ND ug/kg 07/27/22 03:13 79-34-507/25/22 23:207.4 1.9 1
Tetrachloroethene ND ug/kg 07/27/22 03:13 127-18-407/25/22 23:207.4 2.3 1
Toluene ND ug/kg 07/27/22 03:13 108-88-307/25/22 23:207.4 2.1 1
1,2,3-Trichlorobenzene ND ug/kg 07/27/22 03:13 87-61-6 IK,v207/25/22 23:207.4 5.9 1
1,2,4-Trichlorobenzene ND ug/kg 07/27/22 03:13 120-82-107/25/22 23:207.4 6.2 1
1,1,1-Trichloroethane ND ug/kg 07/27/22 03:13 71-55-607/25/22 23:207.4 3.8 1
1,1,2-Trichloroethane ND ug/kg 07/27/22 03:13 79-00-507/25/22 23:207.4 2.4 1
Trichloroethene ND ug/kg 07/27/22 03:13 79-01-607/25/22 23:207.4 1.9 1
Trichlorofluoromethane ND ug/kg 07/27/22 03:13 75-69-407/25/22 23:207.4 4.0 1
1,2,3-Trichloropropane ND ug/kg 07/27/22 03:13 96-18-407/25/22 23:207.4 3.7 1
1,2,4-Trimethylbenzene ND ug/kg 07/27/22 03:13 95-63-607/25/22 23:207.4 2.0 1
1,3,5-Trimethylbenzene ND ug/kg 07/27/22 03:13 108-67-807/25/22 23:207.4 2.5 1
Vinyl acetate ND ug/kg 07/27/22 03:13 108-05-407/25/22 23:2073.5 5.4 1
Vinyl chloride ND ug/kg 07/27/22 03:13 75-01-407/25/22 23:2014.7 3.7 1
Xylene (Total)ND ug/kg 07/27/22 03:13 1330-20-707/25/22 23:2014.7 4.2 1
m&p-Xylene ND ug/kg 07/27/22 03:13 179601-23-107/25/22 23:2014.7 5.0 1
o-Xylene ND ug/kg 07/27/22 03:13 95-47-607/25/22 23:207.4 3.3 1
Surrogates
Toluene-d8 (S)100 %07/27/22 03:13 2037-26-507/25/22 23:2070-130 1
4-Bromofluorobenzene (S)97 %07/27/22 03:13 460-00-407/25/22 23:2069-134 1
1,2-Dichloroethane-d4 (S)107 %07/27/22 03:13 17060-07-007/25/22 23:2070-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 21.0 %07/25/22 14:53 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 61 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:PL-BASE (12)Lab ID:92616378023 Collected:07/19/22 16:45 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 72.0 %08/03/22 11:0608/03/22 10:591
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 62 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:PL-N (12)Lab ID:92616378024 Collected:07/19/22 16:30 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP EPH Preparation Method: MA DEP/NJ DEP
Pace National - Mt. Juliet
TPH by Method MADEPE
Aliphatic (C09-C18)ND mg/kg 08/05/22 00:2908/02/22 15:259.14 3.05 1
Aliphatic (C19-C36)3.29J mg/kg 08/05/22 00:29 B,J08/02/22 15:259.14 3.05 1
Aromatic (C11-C22)3.65J mg/kg 08/05/22 00:51 B,J08/02/22 15:259.14 3.05 1
Total Extractable Hydrocarbons 6.94J mg/kg 08/05/22 00:51 TPH-TEH B,J08/02/22 15:259.14 3.05 1
Surrogates
o-Terphenyl (S)66.0 %08/05/22 00:51 84-15-108/02/22 15:2540.0-140 1
1-Chloro-octadecane (S)65.3 %08/05/22 00:29 3386-33-208/02/22 15:2540.0-140 1
2-Fluorobiphenyl (S)76.9 %08/05/22 00:51 321-60-808/02/22 15:2540.0-140 1
2-Bromonaphthalene (S)73.7 %08/05/22 00:51 580-13-208/02/22 15:2540.0-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Pace Analytical Services - Charlotte
VPH NC Soil
Aliphatic (C05-C08)ND mg/kg 07/23/22 04:39 N207/22/22 18:222.7 2.7 1
Aliphatic(C09-C12) Adjusted ND mg/kg 07/23/22 04:39 N207/22/22 18:222.7 2.7 1
Aromatic (C09-C10)ND mg/kg 07/23/22 04:39 N207/22/22 18:222.7 2.7 1
Surrogates
4-Bromofluorobenzene (FID) (S)99 %07/23/22 04:39 460-00-407/22/22 18:2270-130 1
4-Bromofluorobenzene (PID) (S)87 %07/23/22 04:39 460-00-407/22/22 18:2270-130 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 07/28/22 13:34 83-32-907/27/22 03:474241491
Acenaphthylene ND ug/kg 07/28/22 13:34 208-96-807/27/22 03:474241491
Aniline ND ug/kg 07/28/22 13:34 62-53-307/27/22 03:474241661
Anthracene ND ug/kg 07/28/22 13:34 120-12-707/27/22 03:474241391
Benzo(a)anthracene ND ug/kg 07/28/22 13:34 56-55-307/27/22 03:474241411
Benzo(a)pyrene ND ug/kg 07/28/22 13:34 50-32-807/27/22 03:474241471
Benzo(b)fluoranthene ND ug/kg 07/28/22 13:34 205-99-207/27/22 03:474241411
Benzo(g,h,i)perylene ND ug/kg 07/28/22 13:34 191-24-207/27/22 03:474241651
Benzo(k)fluoranthene ND ug/kg 07/28/22 13:34 207-08-907/27/22 03:474241491
Benzoic Acid ND ug/kg 07/28/22 13:34 65-85-007/27/22 03:4721209111
Benzyl alcohol ND ug/kg 07/28/22 13:34 100-51-607/27/22 03:478483211
4-Bromophenylphenyl ether ND ug/kg 07/28/22 13:34 101-55-307/27/22 03:474241631
Butylbenzylphthalate ND ug/kg 07/28/22 13:34 85-68-707/27/22 03:474241791
4-Chloro-3-methylphenol ND ug/kg 07/28/22 13:34 59-50-707/27/22 03:478482981
4-Chloroaniline ND ug/kg 07/28/22 13:34 106-47-807/27/22 03:478483331
bis(2-Chloroethoxy)methane ND ug/kg 07/28/22 13:34 111-91-107/27/22 03:474241761
bis(2-Chloroethyl) ether ND ug/kg 07/28/22 13:34 111-44-407/27/22 03:474241591
2-Chloronaphthalene ND ug/kg 07/28/22 13:34 91-58-707/27/22 03:474241681
2-Chlorophenol ND ug/kg 07/28/22 13:34 95-57-807/27/22 03:474241591
4-Chlorophenylphenyl ether ND ug/kg 07/28/22 13:34 7005-72-307/27/22 03:474241581
Chrysene ND ug/kg 07/28/22 13:34 218-01-907/27/22 03:474241541
Dibenz(a,h)anthracene ND ug/kg 07/28/22 13:34 53-70-307/27/22 03:474241631
Dibenzofuran ND ug/kg 07/28/22 13:34 132-64-907/27/22 03:474241531
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 63 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:PL-N (12)Lab ID:92616378024 Collected:07/19/22 16:30 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
1,2-Dichlorobenzene ND ug/kg 07/28/22 13:34 95-50-107/27/22 03:474241531
1,3-Dichlorobenzene ND ug/kg 07/28/22 13:34 541-73-107/27/22 03:474241501
1,4-Dichlorobenzene ND ug/kg 07/28/22 13:34 106-46-707/27/22 03:474241621
3,3'-Dichlorobenzidine ND ug/kg 07/28/22 13:34 91-94-107/27/22 03:478482871
2,4-Dichlorophenol ND ug/kg 07/28/22 13:34 120-83-207/27/22 03:474241661
Diethylphthalate ND ug/kg 07/28/22 13:34 84-66-207/27/22 03:474241561
2,4-Dimethylphenol ND ug/kg 07/28/22 13:34 105-67-907/27/22 03:474241761
Dimethylphthalate ND ug/kg 07/28/22 13:34 131-11-307/27/22 03:474241541
Di-n-butylphthalate ND ug/kg 07/28/22 13:34 84-74-207/27/22 03:474241431
4,6-Dinitro-2-methylphenol ND ug/kg 07/28/22 13:34 534-52-107/27/22 03:478483961
2,4-Dinitrophenol ND ug/kg 07/28/22 13:34 51-28-507/27/22 03:47212013101
2,4-Dinitrotoluene ND ug/kg 07/28/22 13:34 121-14-207/27/22 03:474241631
2,6-Dinitrotoluene ND ug/kg 07/28/22 13:34 606-20-207/27/22 03:474241561
Di-n-octylphthalate ND ug/kg 07/28/22 13:34 117-84-007/27/22 03:474241671
bis(2-Ethylhexyl)phthalate ND ug/kg 07/28/22 13:34 117-81-707/27/22 03:474241651
Fluoranthene ND ug/kg 07/28/22 13:34 206-44-007/27/22 03:474241451
Fluorene ND ug/kg 07/28/22 13:34 86-73-707/27/22 03:474241491
Hexachloro-1,3-butadiene ND ug/kg 07/28/22 13:34 87-68-307/27/22 03:474241841
Hexachlorobenzene ND ug/kg 07/28/22 13:34 118-74-107/27/22 03:474241661
Hexachlorocyclopentadiene ND ug/kg 07/28/22 13:34 77-47-407/27/22 03:474242431
Hexachloroethane ND ug/kg 07/28/22 13:34 67-72-107/27/22 03:474241621
Indeno(1,2,3-cd)pyrene ND ug/kg 07/28/22 13:34 193-39-507/27/22 03:474241671
Isophorone ND ug/kg 07/28/22 13:34 78-59-107/27/22 03:474241891
1-Methylnaphthalene ND ug/kg 07/28/22 13:34 90-12-007/27/22 03:474241491
2-Methylnaphthalene ND ug/kg 07/28/22 13:34 91-57-607/27/22 03:474241701
2-Methylphenol(o-Cresol)ND ug/kg 07/28/22 13:34 95-48-707/27/22 03:474241741
3&4-Methylphenol(m&p Cresol)ND ug/kg 07/28/22 13:34 15831-10-407/27/22 03:474241711
Naphthalene ND ug/kg 07/28/22 13:34 91-20-307/27/22 03:474241441
2-Nitroaniline ND ug/kg 07/28/22 13:34 88-74-407/27/22 03:4721203471
3-Nitroaniline ND ug/kg 07/28/22 13:34 99-09-207/27/22 03:4721203331
4-Nitroaniline ND ug/kg 07/28/22 13:34 100-01-607/27/22 03:478483231
Nitrobenzene ND ug/kg 07/28/22 13:34 98-95-307/27/22 03:474241971
2-Nitrophenol ND ug/kg 07/28/22 13:34 88-75-507/27/22 03:474241841
4-Nitrophenol ND ug/kg 07/28/22 13:34 100-02-707/27/22 03:4721208201
N-Nitrosodimethylamine ND ug/kg 07/28/22 13:34 62-75-907/27/22 03:474241431
N-Nitroso-di-n-propylamine ND ug/kg 07/28/22 13:34 621-64-707/27/22 03:474241591
N-Nitrosodiphenylamine ND ug/kg 07/28/22 13:34 86-30-607/27/22 03:474241501
2,2'-Oxybis(1-chloropropane)ND ug/kg 07/28/22 13:34 108-60-107/27/22 03:474242021
Pentachlorophenol ND ug/kg 07/28/22 13:34 87-86-507/27/22 03:478484151
Phenanthrene ND ug/kg 07/28/22 13:34 85-01-807/27/22 03:474241391
Phenol ND ug/kg 07/28/22 13:34 108-95-207/27/22 03:474241891
Pyrene ND ug/kg 07/28/22 13:34 129-00-007/27/22 03:474241721
Pyridine ND ug/kg 07/28/22 13:34 110-86-107/27/22 03:474241341
1,2,4-Trichlorobenzene ND ug/kg 07/28/22 13:34 120-82-107/27/22 03:474241671
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 64 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:PL-N (12)Lab ID:92616378024 Collected:07/19/22 16:30 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,4,5-Trichlorophenol ND ug/kg 07/28/22 13:34 95-95-407/27/22 03:474241941
2,4,6-Trichlorophenol ND ug/kg 07/28/22 13:34 88-06-207/27/22 03:474241751
Surrogates
Nitrobenzene-d5 (S)71 %07/28/22 13:34 4165-60-007/27/22 03:4721-130 1
2-Fluorobiphenyl (S)71 %07/28/22 13:34 321-60-807/27/22 03:4719-130 1
Terphenyl-d14 (S)88 %07/28/22 13:34 1718-51-007/27/22 03:4715-130 1
Phenol-d6 (S)72 %07/28/22 13:34 13127-88-307/27/22 03:4718-130 1
2-Fluorophenol (S)75 %07/28/22 13:34 367-12-407/27/22 03:4718-130 1
2,4,6-Tribromophenol (S)88 %07/28/22 13:34 118-79-607/27/22 03:4718-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 07/27/22 03:32 67-64-107/25/22 23:2014446.4 1
Benzene ND ug/kg 07/27/22 03:32 71-43-207/25/22 23:207.2 2.9 1
Bromobenzene ND ug/kg 07/27/22 03:32 108-86-107/25/22 23:207.2 2.4 1
Bromochloromethane ND ug/kg 07/27/22 03:32 74-97-507/25/22 23:207.2 2.1 1
Bromodichloromethane ND ug/kg 07/27/22 03:32 75-27-407/25/22 23:207.2 2.8 1
Bromoform ND ug/kg 07/27/22 03:32 75-25-207/25/22 23:207.2 2.5 1
Bromomethane ND ug/kg 07/27/22 03:32 74-83-9 IK,L1,v107/25/22 23:2014.4 11.4 1
2-Butanone (MEK)69.0J ug/kg 07/27/22 03:32 78-93-3 C707/25/22 23:2014434.7 1
n-Butylbenzene ND ug/kg 07/27/22 03:32 104-51-807/25/22 23:207.2 3.4 1
sec-Butylbenzene ND ug/kg 07/27/22 03:32 135-98-807/25/22 23:207.2 3.2 1
tert-Butylbenzene ND ug/kg 07/27/22 03:32 98-06-607/25/22 23:207.2 2.6 1
Carbon tetrachloride ND ug/kg 07/27/22 03:32 56-23-507/25/22 23:207.2 2.7 1
Chlorobenzene ND ug/kg 07/27/22 03:32 108-90-707/25/22 23:207.2 1.4 1
Chloroethane ND ug/kg 07/27/22 03:32 75-00-307/25/22 23:2014.4 5.6 1
Chloroform ND ug/kg 07/27/22 03:32 67-66-307/25/22 23:207.2 4.4 1
Chloromethane ND ug/kg 07/27/22 03:32 74-87-307/25/22 23:2014.4 6.1 1
2-Chlorotoluene ND ug/kg 07/27/22 03:32 95-49-807/25/22 23:207.2 2.6 1
4-Chlorotoluene ND ug/kg 07/27/22 03:32 106-43-407/25/22 23:207.2 1.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 07/27/22 03:32 96-12-8 IK07/25/22 23:207.2 2.8 1
Dibromochloromethane ND ug/kg 07/27/22 03:32 124-48-107/25/22 23:207.2 4.1 1
1,2-Dibromoethane (EDB)ND ug/kg 07/27/22 03:32 106-93-407/25/22 23:207.2 3.2 1
Dibromomethane ND ug/kg 07/27/22 03:32 74-95-307/25/22 23:207.2 1.5 1
1,2-Dichlorobenzene ND ug/kg 07/27/22 03:32 95-50-107/25/22 23:207.2 2.6 1
1,3-Dichlorobenzene ND ug/kg 07/27/22 03:32 541-73-107/25/22 23:207.2 2.2 1
1,4-Dichlorobenzene ND ug/kg 07/27/22 03:32 106-46-707/25/22 23:207.2 1.9 1
Dichlorodifluoromethane ND ug/kg 07/27/22 03:32 75-71-8 IH07/25/22 23:2014.4 3.1 1
1,1-Dichloroethane ND ug/kg 07/27/22 03:32 75-34-307/25/22 23:207.2 3.0 1
1,2-Dichloroethane ND ug/kg 07/27/22 03:32 107-06-207/25/22 23:207.2 4.8 1
1,1-Dichloroethene ND ug/kg 07/27/22 03:32 75-35-407/25/22 23:207.2 3.0 1
cis-1,2-Dichloroethene ND ug/kg 07/27/22 03:32 156-59-207/25/22 23:207.2 2.5 1
trans-1,2-Dichloroethene ND ug/kg 07/27/22 03:32 156-60-507/25/22 23:207.2 2.5 1
1,2-Dichloropropane ND ug/kg 07/27/22 03:32 78-87-507/25/22 23:207.2 2.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 65 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:PL-N (12)Lab ID:92616378024 Collected:07/19/22 16:30 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,3-Dichloropropane ND ug/kg 07/27/22 03:32 142-28-907/25/22 23:207.2 2.3 1
2,2-Dichloropropane ND ug/kg 07/27/22 03:32 594-20-707/25/22 23:207.2 2.4 1
1,1-Dichloropropene ND ug/kg 07/27/22 03:32 563-58-607/25/22 23:207.2 3.5 1
cis-1,3-Dichloropropene ND ug/kg 07/27/22 03:32 10061-01-507/25/22 23:207.2 2.0 1
trans-1,3-Dichloropropene ND ug/kg 07/27/22 03:32 10061-02-607/25/22 23:207.2 2.5 1
Diisopropyl ether ND ug/kg 07/27/22 03:32 108-20-307/25/22 23:207.2 2.0 1
Ethylbenzene 4.0J ug/kg 07/27/22 03:32 100-41-407/25/22 23:207.2 3.4 1
Hexachloro-1,3-butadiene ND ug/kg 07/27/22 03:32 87-68-307/25/22 23:2014.4 11.8 1
2-Hexanone ND ug/kg 07/27/22 03:32 591-78-607/25/22 23:2072.2 7.0 1
Isopropylbenzene (Cumene)ND ug/kg 07/27/22 03:32 98-82-807/25/22 23:207.2 2.5 1
p-Isopropyltoluene ND ug/kg 07/27/22 03:32 99-87-607/25/22 23:207.2 3.6 1
Methylene Chloride ND ug/kg 07/27/22 03:32 75-09-207/25/22 23:2028.9 19.8 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 07/27/22 03:32 108-10-107/25/22 23:2072.2 7.0 1
Methyl-tert-butyl ether ND ug/kg 07/27/22 03:32 1634-04-407/25/22 23:207.2 2.7 1
Naphthalene ND ug/kg 07/27/22 03:32 91-20-3 v207/25/22 23:207.2 3.8 1
n-Propylbenzene ND ug/kg 07/27/22 03:32 103-65-107/25/22 23:207.2 2.6 1
Styrene ND ug/kg 07/27/22 03:32 100-42-507/25/22 23:207.2 1.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 07/27/22 03:32 630-20-607/25/22 23:207.2 2.8 1
1,1,2,2-Tetrachloroethane ND ug/kg 07/27/22 03:32 79-34-507/25/22 23:207.2 1.9 1
Tetrachloroethene ND ug/kg 07/27/22 03:32 127-18-407/25/22 23:207.2 2.3 1
Toluene ND ug/kg 07/27/22 03:32 108-88-307/25/22 23:207.2 2.1 1
1,2,3-Trichlorobenzene ND ug/kg 07/27/22 03:32 87-61-6 IK,v207/25/22 23:207.2 5.8 1
1,2,4-Trichlorobenzene ND ug/kg 07/27/22 03:32 120-82-107/25/22 23:207.2 6.1 1
1,1,1-Trichloroethane ND ug/kg 07/27/22 03:32 71-55-607/25/22 23:207.2 3.8 1
1,1,2-Trichloroethane ND ug/kg 07/27/22 03:32 79-00-507/25/22 23:207.2 2.4 1
Trichloroethene ND ug/kg 07/27/22 03:32 79-01-607/25/22 23:207.2 1.9 1
Trichlorofluoromethane ND ug/kg 07/27/22 03:32 75-69-407/25/22 23:207.2 4.0 1
1,2,3-Trichloropropane ND ug/kg 07/27/22 03:32 96-18-407/25/22 23:207.2 3.7 1
1,2,4-Trimethylbenzene ND ug/kg 07/27/22 03:32 95-63-607/25/22 23:207.2 2.0 1
1,3,5-Trimethylbenzene ND ug/kg 07/27/22 03:32 108-67-807/25/22 23:207.2 2.4 1
Vinyl acetate ND ug/kg 07/27/22 03:32 108-05-407/25/22 23:2072.2 5.3 1
Vinyl chloride ND ug/kg 07/27/22 03:32 75-01-407/25/22 23:2014.4 3.7 1
Xylene (Total)13.2J ug/kg 07/27/22 03:32 1330-20-707/25/22 23:2014.4 4.1 1
m&p-Xylene 7.0J ug/kg 07/27/22 03:32 179601-23-107/25/22 23:2014.4 4.9 1
o-Xylene 6.2J ug/kg 07/27/22 03:32 95-47-607/25/22 23:207.2 3.2 1
Surrogates
Toluene-d8 (S)101 %07/27/22 03:32 2037-26-507/25/22 23:2070-130 1
4-Bromofluorobenzene (S)98 %07/27/22 03:32 460-00-407/25/22 23:2069-134 1
1,2-Dichloroethane-d4 (S)109 %07/27/22 03:32 17060-07-007/25/22 23:2070-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 21.4 %07/25/22 14:53 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 66 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:PL-N (12)Lab ID:92616378024 Collected:07/19/22 16:30 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 71.1 %08/03/22 11:0608/03/22 10:591
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 67 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:PL-S (12)Lab ID:92616378025 Collected:07/19/22 16:35 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP EPH Preparation Method: MA DEP/NJ DEP
Pace National - Mt. Juliet
TPH by Method MADEPE
Aliphatic (C09-C18)3.20J mg/kg 08/05/22 03:49 J08/02/22 15:259.59 3.20 1
Aliphatic (C09-C18)ND mg/kg 08/09/22 21:21 H108/08/22 15:199.59 3.20 1
Aliphatic (C19-C36)6.18J mg/kg 08/05/22 03:49 B,J08/02/22 15:259.59 3.20 1
Aliphatic (C19-C36)3.45J mg/kg 08/09/22 21:21 H1,J08/08/22 15:199.59 3.20 1
Aromatic (C11-C22)24.6 mg/kg 08/05/22 06:46 B08/02/22 15:259.59 3.20 1
Aromatic (C11-C22)ND mg/kg 08/09/22 21:44 H108/08/22 15:199.59 3.20 1
Total Extractable Hydrocarbons 34.1 mg/kg 08/05/22 06:46 TPH-TEH B08/02/22 15:259.59 3.20 1
Total Extractable Hydrocarbons 3.45J mg/kg 08/09/22 21:21 TPH-TEH H1,J08/08/22 15:199.59 3.20 1
Surrogates
o-Terphenyl (S)66.4 %08/05/22 06:46 84-15-108/02/22 15:2540.0-140 1
o-Terphenyl (S)68.2 %08/09/22 21:44 84-15-108/08/22 15:1940.0-140 1
1-Chloro-octadecane (S)61.8 %08/05/22 03:49 3386-33-208/02/22 15:2540.0-140 1
1-Chloro-octadecane (S)60.8 %08/09/22 21:21 3386-33-208/08/22 15:1940.0-140 1
2-Fluorobiphenyl (S)82.5 %08/05/22 06:46 321-60-808/02/22 15:2540.0-140 1
2-Fluorobiphenyl (S)81.8 %08/09/22 21:44 321-60-808/08/22 15:1940.0-140 1
2-Bromonaphthalene (S)78.8 %08/05/22 06:46 580-13-208/02/22 15:2540.0-140 1
2-Bromonaphthalene (S)81.4 %08/09/22 21:44 580-13-208/08/22 15:1940.0-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Pace Analytical Services - Charlotte
VPH NC Soil
Aliphatic (C05-C08)ND mg/kg 07/23/22 05:07 N207/22/22 18:222.6 2.6 1
Aliphatic(C09-C12) Adjusted ND mg/kg 07/23/22 05:07 N207/22/22 18:222.6 2.6 1
Aromatic (C09-C10)ND mg/kg 07/23/22 05:07 N207/22/22 18:222.6 2.6 1
Surrogates
4-Bromofluorobenzene (FID) (S)98 %07/23/22 05:07 460-00-407/22/22 18:2270-130 1
4-Bromofluorobenzene (PID) (S)86 %07/23/22 05:07 460-00-407/22/22 18:2270-130 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 07/28/22 14:02 83-32-907/27/22 03:473951391
Acenaphthylene ND ug/kg 07/28/22 14:02 208-96-807/27/22 03:473951391
Aniline ND ug/kg 07/28/22 14:02 62-53-307/27/22 03:473951551
Anthracene ND ug/kg 07/28/22 14:02 120-12-707/27/22 03:473951291
Benzo(a)anthracene ND ug/kg 07/28/22 14:02 56-55-307/27/22 03:473951321
Benzo(a)pyrene ND ug/kg 07/28/22 14:02 50-32-807/27/22 03:473951371
Benzo(b)fluoranthene ND ug/kg 07/28/22 14:02 205-99-207/27/22 03:473951321
Benzo(g,h,i)perylene ND ug/kg 07/28/22 14:02 191-24-207/27/22 03:473951531
Benzo(k)fluoranthene ND ug/kg 07/28/22 14:02 207-08-907/27/22 03:473951391
Benzoic Acid ND ug/kg 07/28/22 14:02 65-85-007/27/22 03:4719808491
Benzyl alcohol ND ug/kg 07/28/22 14:02 100-51-607/27/22 03:477902991
4-Bromophenylphenyl ether ND ug/kg 07/28/22 14:02 101-55-307/27/22 03:473951521
Butylbenzylphthalate ND ug/kg 07/28/22 14:02 85-68-707/27/22 03:473951661
4-Chloro-3-methylphenol ND ug/kg 07/28/22 14:02 59-50-707/27/22 03:477902781
4-Chloroaniline ND ug/kg 07/28/22 14:02 106-47-807/27/22 03:477903101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 68 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:PL-S (12)Lab ID:92616378025 Collected:07/19/22 16:35 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
bis(2-Chloroethoxy)methane ND ug/kg 07/28/22 14:02 111-91-107/27/22 03:473951641
bis(2-Chloroethyl) ether ND ug/kg 07/28/22 14:02 111-44-407/27/22 03:473951491
2-Chloronaphthalene ND ug/kg 07/28/22 14:02 91-58-707/27/22 03:473951571
2-Chlorophenol ND ug/kg 07/28/22 14:02 95-57-807/27/22 03:473951491
4-Chlorophenylphenyl ether ND ug/kg 07/28/22 14:02 7005-72-307/27/22 03:473951471
Chrysene ND ug/kg 07/28/22 14:02 218-01-907/27/22 03:473951441
Dibenz(a,h)anthracene ND ug/kg 07/28/22 14:02 53-70-307/27/22 03:473951521
Dibenzofuran ND ug/kg 07/28/22 14:02 132-64-907/27/22 03:473951431
1,2-Dichlorobenzene ND ug/kg 07/28/22 14:02 95-50-107/27/22 03:473951431
1,3-Dichlorobenzene ND ug/kg 07/28/22 14:02 541-73-107/27/22 03:473951401
1,4-Dichlorobenzene ND ug/kg 07/28/22 14:02 106-46-707/27/22 03:473951511
3,3'-Dichlorobenzidine ND ug/kg 07/28/22 14:02 91-94-107/27/22 03:477902671
2,4-Dichlorophenol ND ug/kg 07/28/22 14:02 120-83-207/27/22 03:473951551
Diethylphthalate ND ug/kg 07/28/22 14:02 84-66-207/27/22 03:473951451
2,4-Dimethylphenol ND ug/kg 07/28/22 14:02 105-67-907/27/22 03:473951641
Dimethylphthalate ND ug/kg 07/28/22 14:02 131-11-307/27/22 03:473951441
Di-n-butylphthalate ND ug/kg 07/28/22 14:02 84-74-207/27/22 03:473951331
4,6-Dinitro-2-methylphenol ND ug/kg 07/28/22 14:02 534-52-107/27/22 03:477903691
2,4-Dinitrophenol ND ug/kg 07/28/22 14:02 51-28-507/27/22 03:47198012201
2,4-Dinitrotoluene ND ug/kg 07/28/22 14:02 121-14-207/27/22 03:473951521
2,6-Dinitrotoluene ND ug/kg 07/28/22 14:02 606-20-207/27/22 03:473951451
Di-n-octylphthalate ND ug/kg 07/28/22 14:02 117-84-007/27/22 03:473951561
bis(2-Ethylhexyl)phthalate ND ug/kg 07/28/22 14:02 117-81-707/27/22 03:473951531
Fluoranthene ND ug/kg 07/28/22 14:02 206-44-007/27/22 03:473951351
Fluorene ND ug/kg 07/28/22 14:02 86-73-707/27/22 03:473951391
Hexachloro-1,3-butadiene ND ug/kg 07/28/22 14:02 87-68-307/27/22 03:473951711
Hexachlorobenzene ND ug/kg 07/28/22 14:02 118-74-107/27/22 03:473951551
Hexachlorocyclopentadiene ND ug/kg 07/28/22 14:02 77-47-407/27/22 03:473952261
Hexachloroethane ND ug/kg 07/28/22 14:02 67-72-107/27/22 03:473951511
Indeno(1,2,3-cd)pyrene ND ug/kg 07/28/22 14:02 193-39-507/27/22 03:473951561
Isophorone ND ug/kg 07/28/22 14:02 78-59-107/27/22 03:473951761
1-Methylnaphthalene ND ug/kg 07/28/22 14:02 90-12-007/27/22 03:473951391
2-Methylnaphthalene ND ug/kg 07/28/22 14:02 91-57-607/27/22 03:473951581
2-Methylphenol(o-Cresol)ND ug/kg 07/28/22 14:02 95-48-707/27/22 03:473951621
3&4-Methylphenol(m&p Cresol)ND ug/kg 07/28/22 14:02 15831-10-407/27/22 03:473951591
Naphthalene ND ug/kg 07/28/22 14:02 91-20-307/27/22 03:473951341
2-Nitroaniline ND ug/kg 07/28/22 14:02 88-74-407/27/22 03:4719803231
3-Nitroaniline ND ug/kg 07/28/22 14:02 99-09-207/27/22 03:4719803101
4-Nitroaniline ND ug/kg 07/28/22 14:02 100-01-607/27/22 03:477903011
Nitrobenzene ND ug/kg 07/28/22 14:02 98-95-307/27/22 03:473951831
2-Nitrophenol ND ug/kg 07/28/22 14:02 88-75-507/27/22 03:473951711
4-Nitrophenol ND ug/kg 07/28/22 14:02 100-02-707/27/22 03:4719807641
N-Nitrosodimethylamine ND ug/kg 07/28/22 14:02 62-75-907/27/22 03:473951331
N-Nitroso-di-n-propylamine ND ug/kg 07/28/22 14:02 621-64-707/27/22 03:473951491
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 69 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:PL-S (12)Lab ID:92616378025 Collected:07/19/22 16:35 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
N-Nitrosodiphenylamine ND ug/kg 07/28/22 14:02 86-30-607/27/22 03:473951401
2,2'-Oxybis(1-chloropropane)ND ug/kg 07/28/22 14:02 108-60-107/27/22 03:473951881
Pentachlorophenol ND ug/kg 07/28/22 14:02 87-86-507/27/22 03:477903871
Phenanthrene ND ug/kg 07/28/22 14:02 85-01-807/27/22 03:473951291
Phenol ND ug/kg 07/28/22 14:02 108-95-207/27/22 03:473951761
Pyrene ND ug/kg 07/28/22 14:02 129-00-007/27/22 03:473951601
Pyridine ND ug/kg 07/28/22 14:02 110-86-107/27/22 03:473951251
1,2,4-Trichlorobenzene ND ug/kg 07/28/22 14:02 120-82-107/27/22 03:473951561
2,4,5-Trichlorophenol ND ug/kg 07/28/22 14:02 95-95-407/27/22 03:473951811
2,4,6-Trichlorophenol ND ug/kg 07/28/22 14:02 88-06-207/27/22 03:473951631
Surrogates
Nitrobenzene-d5 (S)61 %07/28/22 14:02 4165-60-007/27/22 03:4721-130 1
2-Fluorobiphenyl (S)65 %07/28/22 14:02 321-60-807/27/22 03:4719-130 1
Terphenyl-d14 (S)98 %07/28/22 14:02 1718-51-007/27/22 03:4715-130 1
Phenol-d6 (S)65 %07/28/22 14:02 13127-88-307/27/22 03:4718-130 1
2-Fluorophenol (S)66 %07/28/22 14:02 367-12-407/27/22 03:4718-130 1
2,4,6-Tribromophenol (S)90 %07/28/22 14:02 118-79-607/27/22 03:4718-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone 519 ug/kg 07/27/22 03:50 67-64-1 C707/25/22 23:2017957.6 1
Benzene ND ug/kg 07/27/22 03:50 71-43-207/25/22 23:209.0 3.6 1
Bromobenzene ND ug/kg 07/27/22 03:50 108-86-107/25/22 23:209.0 2.9 1
Bromochloromethane ND ug/kg 07/27/22 03:50 74-97-507/25/22 23:209.0 2.7 1
Bromodichloromethane ND ug/kg 07/27/22 03:50 75-27-407/25/22 23:209.0 3.5 1
Bromoform ND ug/kg 07/27/22 03:50 75-25-207/25/22 23:209.0 3.2 1
Bromomethane ND ug/kg 07/27/22 03:50 74-83-9 IK,L1,v107/25/22 23:2017.9 14.2 1
2-Butanone (MEK)1460 ug/kg 07/27/22 03:50 78-93-3 C707/25/22 23:2017943.1 1
n-Butylbenzene ND ug/kg 07/27/22 03:50 104-51-807/25/22 23:209.0 4.2 1
sec-Butylbenzene ND ug/kg 07/27/22 03:50 135-98-807/25/22 23:209.0 3.9 1
tert-Butylbenzene ND ug/kg 07/27/22 03:50 98-06-607/25/22 23:209.0 3.2 1
Carbon tetrachloride ND ug/kg 07/27/22 03:50 56-23-507/25/22 23:209.0 3.4 1
Chlorobenzene ND ug/kg 07/27/22 03:50 108-90-707/25/22 23:209.0 1.7 1
Chloroethane ND ug/kg 07/27/22 03:50 75-00-307/25/22 23:2017.9 6.9 1
Chloroform ND ug/kg 07/27/22 03:50 67-66-307/25/22 23:209.0 5.5 1
Chloromethane ND ug/kg 07/27/22 03:50 74-87-307/25/22 23:2017.9 7.5 1
2-Chlorotoluene ND ug/kg 07/27/22 03:50 95-49-807/25/22 23:209.0 3.2 1
4-Chlorotoluene ND ug/kg 07/27/22 03:50 106-43-407/25/22 23:209.0 1.6 1
1,2-Dibromo-3-chloropropane ND ug/kg 07/27/22 03:50 96-12-8 IK07/25/22 23:209.0 3.5 1
Dibromochloromethane ND ug/kg 07/27/22 03:50 124-48-107/25/22 23:209.0 5.0 1
1,2-Dibromoethane (EDB)ND ug/kg 07/27/22 03:50 106-93-407/25/22 23:209.0 3.9 1
Dibromomethane ND ug/kg 07/27/22 03:50 74-95-307/25/22 23:209.0 1.9 1
1,2-Dichlorobenzene ND ug/kg 07/27/22 03:50 95-50-107/25/22 23:209.0 3.2 1
1,3-Dichlorobenzene ND ug/kg 07/27/22 03:50 541-73-107/25/22 23:209.0 2.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 70 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:PL-S (12)Lab ID:92616378025 Collected:07/19/22 16:35 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,4-Dichlorobenzene ND ug/kg 07/27/22 03:50 106-46-707/25/22 23:209.0 2.3 1
Dichlorodifluoromethane ND ug/kg 07/27/22 03:50 75-71-8 IH07/25/22 23:2017.9 3.9 1
1,1-Dichloroethane ND ug/kg 07/27/22 03:50 75-34-307/25/22 23:209.0 3.7 1
1,2-Dichloroethane ND ug/kg 07/27/22 03:50 107-06-207/25/22 23:209.0 5.9 1
1,1-Dichloroethene ND ug/kg 07/27/22 03:50 75-35-407/25/22 23:209.0 3.7 1
cis-1,2-Dichloroethene ND ug/kg 07/27/22 03:50 156-59-207/25/22 23:209.0 3.1 1
trans-1,2-Dichloroethene ND ug/kg 07/27/22 03:50 156-60-507/25/22 23:209.0 3.1 1
1,2-Dichloropropane ND ug/kg 07/27/22 03:50 78-87-507/25/22 23:209.0 2.7 1
1,3-Dichloropropane ND ug/kg 07/27/22 03:50 142-28-907/25/22 23:209.0 2.8 1
2,2-Dichloropropane ND ug/kg 07/27/22 03:50 594-20-707/25/22 23:209.0 2.9 1
1,1-Dichloropropene ND ug/kg 07/27/22 03:50 563-58-607/25/22 23:209.0 4.3 1
cis-1,3-Dichloropropene ND ug/kg 07/27/22 03:50 10061-01-507/25/22 23:209.0 2.4 1
trans-1,3-Dichloropropene ND ug/kg 07/27/22 03:50 10061-02-607/25/22 23:209.0 3.1 1
Diisopropyl ether ND ug/kg 07/27/22 03:50 108-20-307/25/22 23:209.0 2.4 1
Ethylbenzene 5.2J ug/kg 07/27/22 03:50 100-41-407/25/22 23:209.0 4.2 1
Hexachloro-1,3-butadiene ND ug/kg 07/27/22 03:50 87-68-307/25/22 23:2017.9 14.7 1
2-Hexanone ND ug/kg 07/27/22 03:50 591-78-607/25/22 23:2089.7 8.7 1
Isopropylbenzene (Cumene)ND ug/kg 07/27/22 03:50 98-82-807/25/22 23:209.0 3.1 1
p-Isopropyltoluene ND ug/kg 07/27/22 03:50 99-87-607/25/22 23:209.0 4.4 1
Methylene Chloride ND ug/kg 07/27/22 03:50 75-09-207/25/22 23:2035.9 24.6 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 07/27/22 03:50 108-10-107/25/22 23:2089.7 8.7 1
Methyl-tert-butyl ether ND ug/kg 07/27/22 03:50 1634-04-407/25/22 23:209.0 3.4 1
Naphthalene ND ug/kg 07/27/22 03:50 91-20-3 v207/25/22 23:209.0 4.7 1
n-Propylbenzene ND ug/kg 07/27/22 03:50 103-65-107/25/22 23:209.0 3.2 1
Styrene ND ug/kg 07/27/22 03:50 100-42-507/25/22 23:209.0 2.4 1
1,1,1,2-Tetrachloroethane ND ug/kg 07/27/22 03:50 630-20-607/25/22 23:209.0 3.4 1
1,1,2,2-Tetrachloroethane ND ug/kg 07/27/22 03:50 79-34-507/25/22 23:209.0 2.4 1
Tetrachloroethene ND ug/kg 07/27/22 03:50 127-18-407/25/22 23:209.0 2.8 1
Toluene ND ug/kg 07/27/22 03:50 108-88-307/25/22 23:209.0 2.5 1
1,2,3-Trichlorobenzene ND ug/kg 07/27/22 03:50 87-61-6 IK,v207/25/22 23:209.0 7.3 1
1,2,4-Trichlorobenzene ND ug/kg 07/27/22 03:50 120-82-107/25/22 23:209.0 7.5 1
1,1,1-Trichloroethane ND ug/kg 07/27/22 03:50 71-55-607/25/22 23:209.0 4.7 1
1,1,2-Trichloroethane ND ug/kg 07/27/22 03:50 79-00-507/25/22 23:209.0 3.0 1
Trichloroethene ND ug/kg 07/27/22 03:50 79-01-607/25/22 23:209.0 2.3 1
Trichlorofluoromethane ND ug/kg 07/27/22 03:50 75-69-407/25/22 23:209.0 4.9 1
1,2,3-Trichloropropane ND ug/kg 07/27/22 03:50 96-18-407/25/22 23:209.0 4.5 1
1,2,4-Trimethylbenzene ND ug/kg 07/27/22 03:50 95-63-607/25/22 23:209.0 2.5 1
1,3,5-Trimethylbenzene ND ug/kg 07/27/22 03:50 108-67-807/25/22 23:209.0 3.0 1
Vinyl acetate ND ug/kg 07/27/22 03:50 108-05-407/25/22 23:2089.7 6.5 1
Vinyl chloride ND ug/kg 07/27/22 03:50 75-01-407/25/22 23:2017.9 4.6 1
Xylene (Total)5.5J ug/kg 07/27/22 03:50 1330-20-707/25/22 23:2017.9 5.1 1
m&p-Xylene ND ug/kg 07/27/22 03:50 179601-23-107/25/22 23:2017.9 6.1 1
o-Xylene 5.5J ug/kg 07/27/22 03:50 95-47-607/25/22 23:209.0 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 71 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:PL-S (12)Lab ID:92616378025 Collected:07/19/22 16:35 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Surrogates
Toluene-d8 (S)100 %07/27/22 03:50 2037-26-507/25/22 23:2070-130 1
4-Bromofluorobenzene (S)98 %07/27/22 03:50 460-00-407/25/22 23:2069-134 1
1,2-Dichloroethane-d4 (S)104 %07/27/22 03:50 17060-07-007/25/22 23:2070-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 16.5 %07/25/22 14:53 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 67.8 %08/03/22 11:0608/03/22 10:591
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 72 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:PL-E (12)Lab ID:92616378026 Collected:07/19/22 16:40 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP EPH Preparation Method: MA DEP/NJ DEP
Pace National - Mt. Juliet
TPH by Method MADEPE
Aliphatic (C09-C18)ND mg/kg 08/05/22 04:1108/02/22 15:257.90 2.64 1
Aliphatic (C19-C36)3.50J mg/kg 08/05/22 04:11 B,J08/02/22 15:257.90 2.64 1
Aromatic (C11-C22)3.95J mg/kg 08/05/22 06:24 B,J08/02/22 15:257.90 2.64 1
Total Extractable Hydrocarbons 7.45J mg/kg 08/05/22 06:24 TPH-TEH B,J08/02/22 15:257.90 2.64 1
Surrogates
o-Terphenyl (S)67.9 %08/05/22 06:24 84-15-108/02/22 15:2540.0-140 1
1-Chloro-octadecane (S)63.9 %08/05/22 04:11 3386-33-208/02/22 15:2540.0-140 1
2-Fluorobiphenyl (S)82.7 %08/05/22 06:24 321-60-808/02/22 15:2540.0-140 1
2-Bromonaphthalene (S)79.3 %08/05/22 06:24 580-13-208/02/22 15:2540.0-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Pace Analytical Services - Charlotte
VPH NC Soil
Aliphatic (C05-C08)ND mg/kg 07/23/22 05:35 N207/22/22 18:222.6 2.6 1
Aliphatic(C09-C12) Adjusted ND mg/kg 07/23/22 05:35 N207/22/22 18:222.6 2.6 1
Aromatic (C09-C10)ND mg/kg 07/23/22 05:35 N207/22/22 18:222.6 2.6 1
Surrogates
4-Bromofluorobenzene (FID) (S)98 %07/23/22 05:35 460-00-407/22/22 18:2270-130 1
4-Bromofluorobenzene (PID) (S)86 %07/23/22 05:35 460-00-407/22/22 18:2270-130 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 07/28/22 15:44 83-32-907/27/22 03:473901371
Acenaphthylene ND ug/kg 07/28/22 15:44 208-96-807/27/22 03:473901371
Aniline ND ug/kg 07/28/22 15:44 62-53-307/27/22 03:473901531
Anthracene ND ug/kg 07/28/22 15:44 120-12-707/27/22 03:473901281
Benzo(a)anthracene ND ug/kg 07/28/22 15:44 56-55-307/27/22 03:473901301
Benzo(a)pyrene ND ug/kg 07/28/22 15:44 50-32-807/27/22 03:473901351
Benzo(b)fluoranthene ND ug/kg 07/28/22 15:44 205-99-207/27/22 03:473901301
Benzo(g,h,i)perylene ND ug/kg 07/28/22 15:44 191-24-207/27/22 03:473901511
Benzo(k)fluoranthene ND ug/kg 07/28/22 15:44 207-08-907/27/22 03:473901371
Benzoic Acid ND ug/kg 07/28/22 15:44 65-85-007/27/22 03:4719508391
Benzyl alcohol ND ug/kg 07/28/22 15:44 100-51-607/27/22 03:477812961
4-Bromophenylphenyl ether ND ug/kg 07/28/22 15:44 101-55-307/27/22 03:473901501
Butylbenzylphthalate ND ug/kg 07/28/22 15:44 85-68-707/27/22 03:473901641
4-Chloro-3-methylphenol ND ug/kg 07/28/22 15:44 59-50-707/27/22 03:477812741
4-Chloroaniline ND ug/kg 07/28/22 15:44 106-47-807/27/22 03:477813061
bis(2-Chloroethoxy)methane ND ug/kg 07/28/22 15:44 111-91-107/27/22 03:473901621
bis(2-Chloroethyl) ether ND ug/kg 07/28/22 15:44 111-44-407/27/22 03:473901471
2-Chloronaphthalene ND ug/kg 07/28/22 15:44 91-58-707/27/22 03:473901551
2-Chlorophenol ND ug/kg 07/28/22 15:44 95-57-807/27/22 03:473901471
4-Chlorophenylphenyl ether ND ug/kg 07/28/22 15:44 7005-72-307/27/22 03:473901451
Chrysene ND ug/kg 07/28/22 15:44 218-01-907/27/22 03:473901421
Dibenz(a,h)anthracene ND ug/kg 07/28/22 15:44 53-70-307/27/22 03:473901501
Dibenzofuran ND ug/kg 07/28/22 15:44 132-64-907/27/22 03:473901411
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 73 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:PL-E (12)Lab ID:92616378026 Collected:07/19/22 16:40 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
1,2-Dichlorobenzene ND ug/kg 07/28/22 15:44 95-50-107/27/22 03:473901411
1,3-Dichlorobenzene ND ug/kg 07/28/22 15:44 541-73-107/27/22 03:473901381
1,4-Dichlorobenzene ND ug/kg 07/28/22 15:44 106-46-707/27/22 03:473901491
3,3'-Dichlorobenzidine ND ug/kg 07/28/22 15:44 91-94-107/27/22 03:477812641
2,4-Dichlorophenol ND ug/kg 07/28/22 15:44 120-83-207/27/22 03:473901531
Diethylphthalate ND ug/kg 07/28/22 15:44 84-66-207/27/22 03:473901431
2,4-Dimethylphenol ND ug/kg 07/28/22 15:44 105-67-907/27/22 03:473901621
Dimethylphthalate ND ug/kg 07/28/22 15:44 131-11-307/27/22 03:473901421
Di-n-butylphthalate ND ug/kg 07/28/22 15:44 84-74-207/27/22 03:473901311
4,6-Dinitro-2-methylphenol ND ug/kg 07/28/22 15:44 534-52-107/27/22 03:477813641
2,4-Dinitrophenol ND ug/kg 07/28/22 15:44 51-28-507/27/22 03:47195012101
2,4-Dinitrotoluene ND ug/kg 07/28/22 15:44 121-14-207/27/22 03:473901501
2,6-Dinitrotoluene ND ug/kg 07/28/22 15:44 606-20-207/27/22 03:473901431
Di-n-octylphthalate ND ug/kg 07/28/22 15:44 117-84-0 v107/27/22 03:473901541
bis(2-Ethylhexyl)phthalate ND ug/kg 07/28/22 15:44 117-81-707/27/22 03:473901511
Fluoranthene ND ug/kg 07/28/22 15:44 206-44-007/27/22 03:473901341
Fluorene ND ug/kg 07/28/22 15:44 86-73-707/27/22 03:473901371
Hexachloro-1,3-butadiene ND ug/kg 07/28/22 15:44 87-68-307/27/22 03:473901691
Hexachlorobenzene ND ug/kg 07/28/22 15:44 118-74-107/27/22 03:473901531
Hexachlorocyclopentadiene ND ug/kg 07/28/22 15:44 77-47-407/27/22 03:473902241
Hexachloroethane ND ug/kg 07/28/22 15:44 67-72-107/27/22 03:473901491
Indeno(1,2,3-cd)pyrene ND ug/kg 07/28/22 15:44 193-39-507/27/22 03:473901541
Isophorone ND ug/kg 07/28/22 15:44 78-59-107/27/22 03:473901741
1-Methylnaphthalene ND ug/kg 07/28/22 15:44 90-12-007/27/22 03:473901371
2-Methylnaphthalene ND ug/kg 07/28/22 15:44 91-57-607/27/22 03:473901561
2-Methylphenol(o-Cresol)ND ug/kg 07/28/22 15:44 95-48-707/27/22 03:473901601
3&4-Methylphenol(m&p Cresol)ND ug/kg 07/28/22 15:44 15831-10-407/27/22 03:473901571
Naphthalene ND ug/kg 07/28/22 15:44 91-20-307/27/22 03:473901321
2-Nitroaniline ND ug/kg 07/28/22 15:44 88-74-407/27/22 03:4719503191
3-Nitroaniline ND ug/kg 07/28/22 15:44 99-09-207/27/22 03:4719503061
4-Nitroaniline ND ug/kg 07/28/22 15:44 100-01-607/27/22 03:477812971
Nitrobenzene ND ug/kg 07/28/22 15:44 98-95-307/27/22 03:473901811
2-Nitrophenol ND ug/kg 07/28/22 15:44 88-75-507/27/22 03:473901691
4-Nitrophenol ND ug/kg 07/28/22 15:44 100-02-707/27/22 03:4719507551
N-Nitrosodimethylamine ND ug/kg 07/28/22 15:44 62-75-907/27/22 03:473901311
N-Nitroso-di-n-propylamine ND ug/kg 07/28/22 15:44 621-64-707/27/22 03:473901471
N-Nitrosodiphenylamine ND ug/kg 07/28/22 15:44 86-30-607/27/22 03:473901381
2,2'-Oxybis(1-chloropropane)ND ug/kg 07/28/22 15:44 108-60-107/27/22 03:473901861
Pentachlorophenol ND ug/kg 07/28/22 15:44 87-86-507/27/22 03:477813821
Phenanthrene ND ug/kg 07/28/22 15:44 85-01-807/27/22 03:473901281
Phenol ND ug/kg 07/28/22 15:44 108-95-207/27/22 03:473901741
Pyrene ND ug/kg 07/28/22 15:44 129-00-007/27/22 03:473901591
Pyridine ND ug/kg 07/28/22 15:44 110-86-107/27/22 03:473901231
1,2,4-Trichlorobenzene ND ug/kg 07/28/22 15:44 120-82-107/27/22 03:473901541
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 74 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:PL-E (12)Lab ID:92616378026 Collected:07/19/22 16:40 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,4,5-Trichlorophenol ND ug/kg 07/28/22 15:44 95-95-407/27/22 03:473901791
2,4,6-Trichlorophenol ND ug/kg 07/28/22 15:44 88-06-207/27/22 03:473901611
Surrogates
Nitrobenzene-d5 (S)70 %07/28/22 15:44 4165-60-007/27/22 03:4721-130 1
2-Fluorobiphenyl (S)65 %07/28/22 15:44 321-60-807/27/22 03:4719-130 1
Terphenyl-d14 (S)79 %07/28/22 15:44 1718-51-007/27/22 03:4715-130 1
Phenol-d6 (S)69 %07/28/22 15:44 13127-88-307/27/22 03:4718-130 1
2-Fluorophenol (S)66 %07/28/22 15:44 367-12-407/27/22 03:4718-130 1
2,4,6-Tribromophenol (S)76 %07/28/22 15:44 118-79-607/27/22 03:4718-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 07/27/22 04:09 67-64-107/25/22 23:2012640.4 1
Benzene ND ug/kg 07/27/22 04:09 71-43-207/25/22 23:206.3 2.5 1
Bromobenzene ND ug/kg 07/27/22 04:09 108-86-107/25/22 23:206.3 2.0 1
Bromochloromethane ND ug/kg 07/27/22 04:09 74-97-507/25/22 23:206.3 1.9 1
Bromodichloromethane ND ug/kg 07/27/22 04:09 75-27-407/25/22 23:206.3 2.4 1
Bromoform ND ug/kg 07/27/22 04:09 75-25-207/25/22 23:206.3 2.2 1
Bromomethane ND ug/kg 07/27/22 04:09 74-83-9 IK,L1,v107/25/22 23:2012.6 9.9 1
2-Butanone (MEK)47.6J ug/kg 07/27/22 04:09 78-93-3 C707/25/22 23:2012630.2 1
n-Butylbenzene ND ug/kg 07/27/22 04:09 104-51-807/25/22 23:206.3 3.0 1
sec-Butylbenzene ND ug/kg 07/27/22 04:09 135-98-807/25/22 23:206.3 2.8 1
tert-Butylbenzene ND ug/kg 07/27/22 04:09 98-06-607/25/22 23:206.3 2.2 1
Carbon tetrachloride ND ug/kg 07/27/22 04:09 56-23-507/25/22 23:206.3 2.4 1
Chlorobenzene ND ug/kg 07/27/22 04:09 108-90-707/25/22 23:206.3 1.2 1
Chloroethane ND ug/kg 07/27/22 04:09 75-00-307/25/22 23:2012.6 4.9 1
Chloroform ND ug/kg 07/27/22 04:09 67-66-307/25/22 23:206.3 3.8 1
Chloromethane ND ug/kg 07/27/22 04:09 74-87-307/25/22 23:2012.6 5.3 1
2-Chlorotoluene ND ug/kg 07/27/22 04:09 95-49-807/25/22 23:206.3 2.2 1
4-Chlorotoluene ND ug/kg 07/27/22 04:09 106-43-407/25/22 23:206.3 1.1 1
1,2-Dibromo-3-chloropropane ND ug/kg 07/27/22 04:09 96-12-8 IK07/25/22 23:206.3 2.4 1
Dibromochloromethane ND ug/kg 07/27/22 04:09 124-48-107/25/22 23:206.3 3.5 1
1,2-Dibromoethane (EDB)ND ug/kg 07/27/22 04:09 106-93-407/25/22 23:206.3 2.8 1
Dibromomethane ND ug/kg 07/27/22 04:09 74-95-307/25/22 23:206.3 1.3 1
1,2-Dichlorobenzene ND ug/kg 07/27/22 04:09 95-50-107/25/22 23:206.3 2.3 1
1,3-Dichlorobenzene ND ug/kg 07/27/22 04:09 541-73-107/25/22 23:206.3 1.9 1
1,4-Dichlorobenzene ND ug/kg 07/27/22 04:09 106-46-707/25/22 23:206.3 1.6 1
Dichlorodifluoromethane ND ug/kg 07/27/22 04:09 75-71-8 IH07/25/22 23:2012.6 2.7 1
1,1-Dichloroethane ND ug/kg 07/27/22 04:09 75-34-307/25/22 23:206.3 2.6 1
1,2-Dichloroethane ND ug/kg 07/27/22 04:09 107-06-207/25/22 23:206.3 4.2 1
1,1-Dichloroethene ND ug/kg 07/27/22 04:09 75-35-407/25/22 23:206.3 2.6 1
cis-1,2-Dichloroethene ND ug/kg 07/27/22 04:09 156-59-207/25/22 23:206.3 2.2 1
trans-1,2-Dichloroethene ND ug/kg 07/27/22 04:09 156-60-507/25/22 23:206.3 2.2 1
1,2-Dichloropropane ND ug/kg 07/27/22 04:09 78-87-507/25/22 23:206.3 1.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 75 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:PL-E (12)Lab ID:92616378026 Collected:07/19/22 16:40 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,3-Dichloropropane ND ug/kg 07/27/22 04:09 142-28-907/25/22 23:206.3 2.0 1
2,2-Dichloropropane ND ug/kg 07/27/22 04:09 594-20-707/25/22 23:206.3 2.0 1
1,1-Dichloropropene ND ug/kg 07/27/22 04:09 563-58-607/25/22 23:206.3 3.0 1
cis-1,3-Dichloropropene ND ug/kg 07/27/22 04:09 10061-01-507/25/22 23:206.3 1.7 1
trans-1,3-Dichloropropene ND ug/kg 07/27/22 04:09 10061-02-607/25/22 23:206.3 2.2 1
Diisopropyl ether ND ug/kg 07/27/22 04:09 108-20-307/25/22 23:206.3 1.7 1
Ethylbenzene 4.2J ug/kg 07/27/22 04:09 100-41-407/25/22 23:206.3 2.9 1
Hexachloro-1,3-butadiene ND ug/kg 07/27/22 04:09 87-68-307/25/22 23:2012.6 10.3 1
2-Hexanone ND ug/kg 07/27/22 04:09 591-78-607/25/22 23:2062.9 6.1 1
Isopropylbenzene (Cumene)ND ug/kg 07/27/22 04:09 98-82-807/25/22 23:206.3 2.1 1
p-Isopropyltoluene ND ug/kg 07/27/22 04:09 99-87-607/25/22 23:206.3 3.1 1
Methylene Chloride ND ug/kg 07/27/22 04:09 75-09-207/25/22 23:2025.2 17.2 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 07/27/22 04:09 108-10-107/25/22 23:2062.9 6.1 1
Methyl-tert-butyl ether ND ug/kg 07/27/22 04:09 1634-04-407/25/22 23:206.3 2.4 1
Naphthalene ND ug/kg 07/27/22 04:09 91-20-3 v207/25/22 23:206.3 3.3 1
n-Propylbenzene ND ug/kg 07/27/22 04:09 103-65-107/25/22 23:206.3 2.2 1
Styrene ND ug/kg 07/27/22 04:09 100-42-507/25/22 23:206.3 1.7 1
1,1,1,2-Tetrachloroethane ND ug/kg 07/27/22 04:09 630-20-607/25/22 23:206.3 2.4 1
1,1,2,2-Tetrachloroethane ND ug/kg 07/27/22 04:09 79-34-507/25/22 23:206.3 1.7 1
Tetrachloroethene ND ug/kg 07/27/22 04:09 127-18-407/25/22 23:206.3 2.0 1
Toluene 6.8 ug/kg 07/27/22 04:09 108-88-307/25/22 23:206.3 1.8 1
1,2,3-Trichlorobenzene ND ug/kg 07/27/22 04:09 87-61-6 IK,v207/25/22 23:206.3 5.1 1
1,2,4-Trichlorobenzene ND ug/kg 07/27/22 04:09 120-82-107/25/22 23:206.3 5.3 1
1,1,1-Trichloroethane ND ug/kg 07/27/22 04:09 71-55-607/25/22 23:206.3 3.3 1
1,1,2-Trichloroethane ND ug/kg 07/27/22 04:09 79-00-507/25/22 23:206.3 2.1 1
Trichloroethene ND ug/kg 07/27/22 04:09 79-01-607/25/22 23:206.3 1.6 1
Trichlorofluoromethane ND ug/kg 07/27/22 04:09 75-69-407/25/22 23:206.3 3.5 1
1,2,3-Trichloropropane ND ug/kg 07/27/22 04:09 96-18-407/25/22 23:206.3 3.2 1
1,2,4-Trimethylbenzene ND ug/kg 07/27/22 04:09 95-63-607/25/22 23:206.3 1.7 1
1,3,5-Trimethylbenzene ND ug/kg 07/27/22 04:09 108-67-807/25/22 23:206.3 2.1 1
Vinyl acetate ND ug/kg 07/27/22 04:09 108-05-407/25/22 23:2062.9 4.6 1
Vinyl chloride ND ug/kg 07/27/22 04:09 75-01-407/25/22 23:2012.6 3.2 1
Xylene (Total)18.7 ug/kg 07/27/22 04:09 1330-20-707/25/22 23:2012.6 3.6 1
m&p-Xylene 10.5J ug/kg 07/27/22 04:09 179601-23-107/25/22 23:2012.6 4.3 1
o-Xylene 8.2 ug/kg 07/27/22 04:09 95-47-607/25/22 23:206.3 2.8 1
Surrogates
Toluene-d8 (S)101 %07/27/22 04:09 2037-26-507/25/22 23:2070-130 1
4-Bromofluorobenzene (S)99 %07/27/22 04:09 460-00-407/25/22 23:2069-134 1
1,2-Dichloroethane-d4 (S)106 %07/27/22 04:09 17060-07-007/25/22 23:2070-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 15.2 %07/25/22 14:53 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 76 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:PL-E (12)Lab ID:92616378026 Collected:07/19/22 16:40 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 82.3 %08/03/22 12:5308/03/22 12:431
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 77 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:PL-W (12)Lab ID:92616378027 Collected:07/19/22 16:40 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP EPH Preparation Method: MA DEP/NJ DEP
Pace National - Mt. Juliet
TPH by Method MADEPE
Aliphatic (C09-C18)ND mg/kg 08/05/22 04:3308/02/22 15:259.13 3.05 1
Aliphatic (C19-C36)5.69J mg/kg 08/05/22 04:33 B,J08/02/22 15:259.13 3.05 1
Aromatic (C11-C22)4.80J mg/kg 08/05/22 06:02 B,J08/02/22 15:259.13 3.05 1
Total Extractable Hydrocarbons 10.5 mg/kg 08/05/22 06:02 TPH-TEH B08/02/22 15:259.13 3.05 1
Surrogates
o-Terphenyl (S)69.8 %08/05/22 06:02 84-15-108/02/22 15:2540.0-140 1
1-Chloro-octadecane (S)67.1 %08/05/22 04:33 3386-33-208/02/22 15:2540.0-140 1
2-Fluorobiphenyl (S)83.3 %08/05/22 06:02 321-60-808/02/22 15:2540.0-140 1
2-Bromonaphthalene (S)79.8 %08/05/22 06:02 580-13-208/02/22 15:2540.0-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Pace Analytical Services - Charlotte
VPH NC Soil
Aliphatic (C05-C08)ND mg/kg 07/23/22 06:04 N207/22/22 18:223.0 3.0 1
Aliphatic(C09-C12) Adjusted ND mg/kg 07/23/22 06:04 N207/22/22 18:223.0 3.0 1
Aromatic (C09-C10)ND mg/kg 07/23/22 06:04 N207/22/22 18:223.0 3.0 1
Surrogates
4-Bromofluorobenzene (FID) (S)99 %07/23/22 06:04 460-00-407/22/22 18:2270-130 1
4-Bromofluorobenzene (PID) (S)86 %07/23/22 06:04 460-00-407/22/22 18:2270-130 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 07/28/22 16:12 83-32-907/27/22 03:473971401
Acenaphthylene ND ug/kg 07/28/22 16:12 208-96-807/27/22 03:473971401
Aniline ND ug/kg 07/28/22 16:12 62-53-307/27/22 03:473971551
Anthracene ND ug/kg 07/28/22 16:12 120-12-707/27/22 03:473971301
Benzo(a)anthracene ND ug/kg 07/28/22 16:12 56-55-307/27/22 03:473971321
Benzo(a)pyrene ND ug/kg 07/28/22 16:12 50-32-807/27/22 03:473971371
Benzo(b)fluoranthene ND ug/kg 07/28/22 16:12 205-99-207/27/22 03:473971321
Benzo(g,h,i)perylene ND ug/kg 07/28/22 16:12 191-24-207/27/22 03:473971541
Benzo(k)fluoranthene ND ug/kg 07/28/22 16:12 207-08-907/27/22 03:473971401
Benzoic Acid ND ug/kg 07/28/22 16:12 65-85-007/27/22 03:4719908531
Benzyl alcohol ND ug/kg 07/28/22 16:12 100-51-607/27/22 03:477943011
4-Bromophenylphenyl ether ND ug/kg 07/28/22 16:12 101-55-307/27/22 03:473971531
Butylbenzylphthalate ND ug/kg 07/28/22 16:12 85-68-707/27/22 03:473971671
4-Chloro-3-methylphenol ND ug/kg 07/28/22 16:12 59-50-707/27/22 03:477942791
4-Chloroaniline ND ug/kg 07/28/22 16:12 106-47-807/27/22 03:477943121
bis(2-Chloroethoxy)methane ND ug/kg 07/28/22 16:12 111-91-107/27/22 03:473971651
bis(2-Chloroethyl) ether ND ug/kg 07/28/22 16:12 111-44-407/27/22 03:473971491
2-Chloronaphthalene ND ug/kg 07/28/22 16:12 91-58-707/27/22 03:473971581
2-Chlorophenol ND ug/kg 07/28/22 16:12 95-57-807/27/22 03:473971491
4-Chlorophenylphenyl ether ND ug/kg 07/28/22 16:12 7005-72-307/27/22 03:473971481
Chrysene ND ug/kg 07/28/22 16:12 218-01-907/27/22 03:473971441
Dibenz(a,h)anthracene ND ug/kg 07/28/22 16:12 53-70-307/27/22 03:473971531
Dibenzofuran ND ug/kg 07/28/22 16:12 132-64-907/27/22 03:473971431
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 78 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:PL-W (12)Lab ID:92616378027 Collected:07/19/22 16:40 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
1,2-Dichlorobenzene ND ug/kg 07/28/22 16:12 95-50-107/27/22 03:473971431
1,3-Dichlorobenzene ND ug/kg 07/28/22 16:12 541-73-107/27/22 03:473971411
1,4-Dichlorobenzene ND ug/kg 07/28/22 16:12 106-46-707/27/22 03:473971521
3,3'-Dichlorobenzidine ND ug/kg 07/28/22 16:12 91-94-107/27/22 03:477942681
2,4-Dichlorophenol ND ug/kg 07/28/22 16:12 120-83-207/27/22 03:473971551
Diethylphthalate ND ug/kg 07/28/22 16:12 84-66-207/27/22 03:473971461
2,4-Dimethylphenol ND ug/kg 07/28/22 16:12 105-67-907/27/22 03:473971651
Dimethylphthalate ND ug/kg 07/28/22 16:12 131-11-307/27/22 03:473971441
Di-n-butylphthalate ND ug/kg 07/28/22 16:12 84-74-207/27/22 03:473971341
4,6-Dinitro-2-methylphenol ND ug/kg 07/28/22 16:12 534-52-107/27/22 03:477943711
2,4-Dinitrophenol ND ug/kg 07/28/22 16:12 51-28-507/27/22 03:47199012301
2,4-Dinitrotoluene ND ug/kg 07/28/22 16:12 121-14-207/27/22 03:473971531
2,6-Dinitrotoluene ND ug/kg 07/28/22 16:12 606-20-207/27/22 03:473971461
Di-n-octylphthalate ND ug/kg 07/28/22 16:12 117-84-0 v107/27/22 03:473971561
bis(2-Ethylhexyl)phthalate ND ug/kg 07/28/22 16:12 117-81-707/27/22 03:473971541
Fluoranthene ND ug/kg 07/28/22 16:12 206-44-007/27/22 03:473971361
Fluorene ND ug/kg 07/28/22 16:12 86-73-707/27/22 03:473971401
Hexachloro-1,3-butadiene ND ug/kg 07/28/22 16:12 87-68-307/27/22 03:473971721
Hexachlorobenzene ND ug/kg 07/28/22 16:12 118-74-107/27/22 03:473971551
Hexachlorocyclopentadiene ND ug/kg 07/28/22 16:12 77-47-407/27/22 03:473972271
Hexachloroethane ND ug/kg 07/28/22 16:12 67-72-107/27/22 03:473971521
Indeno(1,2,3-cd)pyrene ND ug/kg 07/28/22 16:12 193-39-507/27/22 03:473971561
Isophorone ND ug/kg 07/28/22 16:12 78-59-107/27/22 03:473971771
1-Methylnaphthalene ND ug/kg 07/28/22 16:12 90-12-007/27/22 03:473971401
2-Methylnaphthalene ND ug/kg 07/28/22 16:12 91-57-607/27/22 03:473971591
2-Methylphenol(o-Cresol)ND ug/kg 07/28/22 16:12 95-48-707/27/22 03:473971621
3&4-Methylphenol(m&p Cresol)ND ug/kg 07/28/22 16:12 15831-10-407/27/22 03:473971601
Naphthalene ND ug/kg 07/28/22 16:12 91-20-307/27/22 03:473971351
2-Nitroaniline ND ug/kg 07/28/22 16:12 88-74-407/27/22 03:4719903251
3-Nitroaniline ND ug/kg 07/28/22 16:12 99-09-207/27/22 03:4719903121
4-Nitroaniline ND ug/kg 07/28/22 16:12 100-01-607/27/22 03:477943021
Nitrobenzene ND ug/kg 07/28/22 16:12 98-95-307/27/22 03:473971841
2-Nitrophenol ND ug/kg 07/28/22 16:12 88-75-507/27/22 03:473971721
4-Nitrophenol ND ug/kg 07/28/22 16:12 100-02-707/27/22 03:4719907681
N-Nitrosodimethylamine ND ug/kg 07/28/22 16:12 62-75-907/27/22 03:473971341
N-Nitroso-di-n-propylamine ND ug/kg 07/28/22 16:12 621-64-707/27/22 03:473971491
N-Nitrosodiphenylamine ND ug/kg 07/28/22 16:12 86-30-607/27/22 03:473971411
2,2'-Oxybis(1-chloropropane)ND ug/kg 07/28/22 16:12 108-60-107/27/22 03:473971891
Pentachlorophenol ND ug/kg 07/28/22 16:12 87-86-507/27/22 03:477943891
Phenanthrene ND ug/kg 07/28/22 16:12 85-01-807/27/22 03:473971301
Phenol ND ug/kg 07/28/22 16:12 108-95-207/27/22 03:473971771
Pyrene ND ug/kg 07/28/22 16:12 129-00-007/27/22 03:473971611
Pyridine ND ug/kg 07/28/22 16:12 110-86-107/27/22 03:473971251
1,2,4-Trichlorobenzene ND ug/kg 07/28/22 16:12 120-82-107/27/22 03:473971561
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 79 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:PL-W (12)Lab ID:92616378027 Collected:07/19/22 16:40 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,4,5-Trichlorophenol ND ug/kg 07/28/22 16:12 95-95-407/27/22 03:473971821
2,4,6-Trichlorophenol ND ug/kg 07/28/22 16:12 88-06-207/27/22 03:473971641
Surrogates
Nitrobenzene-d5 (S)60 %07/28/22 16:12 4165-60-007/27/22 03:4721-130 1
2-Fluorobiphenyl (S)58 %07/28/22 16:12 321-60-807/27/22 03:4719-130 1
Terphenyl-d14 (S)74 %07/28/22 16:12 1718-51-007/27/22 03:4715-130 1
Phenol-d6 (S)62 %07/28/22 16:12 13127-88-307/27/22 03:4718-130 1
2-Fluorophenol (S)60 %07/28/22 16:12 367-12-407/27/22 03:4718-130 1
2,4,6-Tribromophenol (S)66 %07/28/22 16:12 118-79-607/27/22 03:4718-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 07/27/22 04:28 67-64-107/25/22 23:2017556.0 1
Benzene ND ug/kg 07/27/22 04:28 71-43-207/25/22 23:208.7 3.5 1
Bromobenzene ND ug/kg 07/27/22 04:28 108-86-107/25/22 23:208.7 2.8 1
Bromochloromethane ND ug/kg 07/27/22 04:28 74-97-507/25/22 23:208.7 2.6 1
Bromodichloromethane ND ug/kg 07/27/22 04:28 75-27-407/25/22 23:208.7 3.4 1
Bromoform ND ug/kg 07/27/22 04:28 75-25-207/25/22 23:208.7 3.1 1
Bromomethane ND ug/kg 07/27/22 04:28 74-83-9 IK,L1,v107/25/22 23:2017.5 13.8 1
2-Butanone (MEK)75.2J ug/kg 07/27/22 04:28 78-93-3 C707/25/22 23:2017541.9 1
n-Butylbenzene ND ug/kg 07/27/22 04:28 104-51-807/25/22 23:208.7 4.1 1
sec-Butylbenzene ND ug/kg 07/27/22 04:28 135-98-807/25/22 23:208.7 3.8 1
tert-Butylbenzene ND ug/kg 07/27/22 04:28 98-06-607/25/22 23:208.7 3.1 1
Carbon tetrachloride ND ug/kg 07/27/22 04:28 56-23-507/25/22 23:208.7 3.3 1
Chlorobenzene ND ug/kg 07/27/22 04:28 108-90-707/25/22 23:208.7 1.7 1
Chloroethane ND ug/kg 07/27/22 04:28 75-00-307/25/22 23:2017.5 6.7 1
Chloroform ND ug/kg 07/27/22 04:28 67-66-307/25/22 23:208.7 5.3 1
Chloromethane ND ug/kg 07/27/22 04:28 74-87-307/25/22 23:2017.5 7.3 1
2-Chlorotoluene ND ug/kg 07/27/22 04:28 95-49-807/25/22 23:208.7 3.1 1
4-Chlorotoluene ND ug/kg 07/27/22 04:28 106-43-407/25/22 23:208.7 1.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 07/27/22 04:28 96-12-8 IK07/25/22 23:208.7 3.4 1
Dibromochloromethane ND ug/kg 07/27/22 04:28 124-48-107/25/22 23:208.7 4.9 1
1,2-Dibromoethane (EDB)ND ug/kg 07/27/22 04:28 106-93-407/25/22 23:208.7 3.8 1
Dibromomethane ND ug/kg 07/27/22 04:28 74-95-307/25/22 23:208.7 1.9 1
1,2-Dichlorobenzene ND ug/kg 07/27/22 04:28 95-50-107/25/22 23:208.7 3.1 1
1,3-Dichlorobenzene ND ug/kg 07/27/22 04:28 541-73-107/25/22 23:208.7 2.7 1
1,4-Dichlorobenzene ND ug/kg 07/27/22 04:28 106-46-707/25/22 23:208.7 2.3 1
Dichlorodifluoromethane ND ug/kg 07/27/22 04:28 75-71-8 IH07/25/22 23:2017.5 3.8 1
1,1-Dichloroethane ND ug/kg 07/27/22 04:28 75-34-307/25/22 23:208.7 3.6 1
1,2-Dichloroethane ND ug/kg 07/27/22 04:28 107-06-207/25/22 23:208.7 5.8 1
1,1-Dichloroethene ND ug/kg 07/27/22 04:28 75-35-407/25/22 23:208.7 3.6 1
cis-1,2-Dichloroethene ND ug/kg 07/27/22 04:28 156-59-207/25/22 23:208.7 3.0 1
trans-1,2-Dichloroethene ND ug/kg 07/27/22 04:28 156-60-507/25/22 23:208.7 3.1 1
1,2-Dichloropropane ND ug/kg 07/27/22 04:28 78-87-507/25/22 23:208.7 2.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 80 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:PL-W (12)Lab ID:92616378027 Collected:07/19/22 16:40 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,3-Dichloropropane ND ug/kg 07/27/22 04:28 142-28-907/25/22 23:208.7 2.7 1
2,2-Dichloropropane ND ug/kg 07/27/22 04:28 594-20-707/25/22 23:208.7 2.8 1
1,1-Dichloropropene ND ug/kg 07/27/22 04:28 563-58-607/25/22 23:208.7 4.2 1
cis-1,3-Dichloropropene ND ug/kg 07/27/22 04:28 10061-01-507/25/22 23:208.7 2.4 1
trans-1,3-Dichloropropene ND ug/kg 07/27/22 04:28 10061-02-607/25/22 23:208.7 3.0 1
Diisopropyl ether ND ug/kg 07/27/22 04:28 108-20-307/25/22 23:208.7 2.4 1
Ethylbenzene 6.0J ug/kg 07/27/22 04:28 100-41-407/25/22 23:208.7 4.1 1
Hexachloro-1,3-butadiene ND ug/kg 07/27/22 04:28 87-68-307/25/22 23:2017.5 14.3 1
2-Hexanone ND ug/kg 07/27/22 04:28 591-78-607/25/22 23:2087.3 8.4 1
Isopropylbenzene (Cumene)ND ug/kg 07/27/22 04:28 98-82-807/25/22 23:208.7 3.0 1
p-Isopropyltoluene ND ug/kg 07/27/22 04:28 99-87-607/25/22 23:208.7 4.3 1
Methylene Chloride ND ug/kg 07/27/22 04:28 75-09-207/25/22 23:2034.9 23.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 07/27/22 04:28 108-10-107/25/22 23:2087.3 8.4 1
Methyl-tert-butyl ether ND ug/kg 07/27/22 04:28 1634-04-407/25/22 23:208.7 3.3 1
Naphthalene ND ug/kg 07/27/22 04:28 91-20-3 v207/25/22 23:208.7 4.6 1
n-Propylbenzene ND ug/kg 07/27/22 04:28 103-65-107/25/22 23:208.7 3.1 1
Styrene ND ug/kg 07/27/22 04:28 100-42-507/25/22 23:208.7 2.3 1
1,1,1,2-Tetrachloroethane ND ug/kg 07/27/22 04:28 630-20-607/25/22 23:208.7 3.4 1
1,1,2,2-Tetrachloroethane ND ug/kg 07/27/22 04:28 79-34-507/25/22 23:208.7 2.3 1
Tetrachloroethene ND ug/kg 07/27/22 04:28 127-18-407/25/22 23:208.7 2.8 1
Toluene ND ug/kg 07/27/22 04:28 108-88-307/25/22 23:208.7 2.5 1
1,2,3-Trichlorobenzene ND ug/kg 07/27/22 04:28 87-61-6 IK,v207/25/22 23:208.7 7.1 1
1,2,4-Trichlorobenzene ND ug/kg 07/27/22 04:28 120-82-107/25/22 23:208.7 7.3 1
1,1,1-Trichloroethane ND ug/kg 07/27/22 04:28 71-55-607/25/22 23:208.7 4.5 1
1,1,2-Trichloroethane ND ug/kg 07/27/22 04:28 79-00-507/25/22 23:208.7 2.9 1
Trichloroethene ND ug/kg 07/27/22 04:28 79-01-607/25/22 23:208.7 2.3 1
Trichlorofluoromethane ND ug/kg 07/27/22 04:28 75-69-407/25/22 23:208.7 4.8 1
1,2,3-Trichloropropane ND ug/kg 07/27/22 04:28 96-18-407/25/22 23:208.7 4.4 1
1,2,4-Trimethylbenzene ND ug/kg 07/27/22 04:28 95-63-607/25/22 23:208.7 2.4 1
1,3,5-Trimethylbenzene ND ug/kg 07/27/22 04:28 108-67-807/25/22 23:208.7 2.9 1
Vinyl acetate ND ug/kg 07/27/22 04:28 108-05-407/25/22 23:2087.3 6.4 1
Vinyl chloride ND ug/kg 07/27/22 04:28 75-01-407/25/22 23:2017.5 4.4 1
Xylene (Total)17.0J ug/kg 07/27/22 04:28 1330-20-707/25/22 23:2017.5 5.0 1
m&p-Xylene 7.8J ug/kg 07/27/22 04:28 179601-23-107/25/22 23:2017.5 6.0 1
o-Xylene 9.2 ug/kg 07/27/22 04:28 95-47-607/25/22 23:208.7 3.9 1
Surrogates
Toluene-d8 (S)101 %07/27/22 04:28 2037-26-507/25/22 23:2070-130 1
4-Bromofluorobenzene (S)98 %07/27/22 04:28 460-00-407/25/22 23:2069-134 1
1,2-Dichloroethane-d4 (S)110 %07/27/22 04:28 17060-07-007/25/22 23:2070-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 17.2 %07/25/22 15:16 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 81 of 125
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92616378
MBS.001
Sample:PL-W (12)Lab ID:92616378027 Collected:07/19/22 16:40 Received:07/22/22 08:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 71.2 %08/03/22 12:5308/03/22 12:431
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 82 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616378
MBS.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1904880
MA DEP/NJ DEP
MADEP EPH
TPH by Method MADEPE
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92616378016, 92616378017, 92616378018, 92616378019, 92616378020, 92616378021, 92616378022,
92616378023, 92616378024, 92616378025, 92616378026, 92616378027
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3822434-1
Associated Lab Samples:92616378016, 92616378017, 92616378018, 92616378019, 92616378020, 92616378021, 92616378022,
92616378023, 92616378024, 92616378025, 92616378026, 92616378027
Matrix:Solid
AnalyzedMDL
Aliphatic (C09-C18)mg/kg 2.97J 6.50 J08/03/22 21:082.17
Aliphatic (C19-C36)mg/kg 2.90J 6.50 J08/03/22 21:082.17
Total Extractable Hydrocarbons mg/kg 5.87J 6.50 J08/03/22 21:082.17
1-Chloro-octadecane (S)%78 40.0-140 08/03/22 21:08
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3822434-4
Associated Lab Samples:92616378016, 92616378017, 92616378018, 92616378019, 92616378020, 92616378021, 92616378022,
92616378023, 92616378024, 92616378025, 92616378026, 92616378027
Matrix:Solid
AnalyzedMDL
Aromatic (C11-C22)mg/kg 3.51J 6.50 J08/03/22 22:182.17
Total Extractable Hydrocarbons mg/kg 3.51J 6.50 J08/03/22 22:182.17
o-Terphenyl (S)%80.3 40.0-140 08/03/22 22:18
2-Fluorobiphenyl (S)%86.8 40.0-140 08/03/22 22:18
2-Bromonaphthalene (S)%86.5 40.0-140 08/03/22 22:18
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3822434-2LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3822434-3
Aliphatic (C09-C18)mg/kg 26.639.9 66.7 40.0-14069.427.7 4.05 25
Aliphatic (C19-C36)mg/kg 42.853.2 80.5 40.0-14085.045.2 5.45 25
1-Chloro-octadecane (S)%73.5 40.0-14075.9
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3822434-5LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3822434-6
Aromatic (C11-C22)mg/kg 93.8113 83.0 40.0-14078.889.0 5.25 25
o-Terphenyl (S)%81.8 40.0-14076.7
2-Fluorobiphenyl (S)%86.1 40.0-14083.5
2-Bromonaphthalene (S)%85.7 40.0-14082.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 83 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616378
MBS.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3822434-7MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1517877-05
R3822434-8
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Aliphatic (C09-C18)mg/kg P648.1 0.00 40.0-1400.00 32.2 5048.1247 168 232
Aliphatic (C19-C36)mg/kg 64.2 54.2 40.0-14059.7 5.28 5064.230.3 65.0 68.5
1-Chloro-octadecane (S)%75.9 40.0-14070.6
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3822434-9MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1517877-05
R3822434-10
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Aromatic (C11-C22)mg/kg 136 56.8 40.0-14079.1 17.9 5013677.1 154 185
o-Terphenyl (S)%83.7 40.0-14084.3
2-Fluorobiphenyl (S)%91.1 40.0-14096.2
2-Bromonaphthalene (S)%88.4 40.0-14092.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 84 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616378
MBS.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1907676
MA DEP/NJ DEP
MADEP EPH
TPH by Method MADEPE
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92616378025
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3824521-1
Associated Lab Samples:92616378025
Matrix:Solid
AnalyzedMDL
Aliphatic (C09-C18)mg/kg ND 6.50 08/09/22 09:582.17
Aliphatic (C19-C36)mg/kg ND 6.50 08/09/22 09:582.17
Total Extractable Hydrocarbons mg/kg ND 6.50 08/09/22 09:582.17
1-Chloro-octadecane (S)%63 40.0-140 08/09/22 09:58
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3824521-4
Associated Lab Samples:92616378025
Matrix:Solid
AnalyzedMDL
Aromatic (C11-C22)mg/kg ND 6.50 08/09/22 11:082.17
Total Extractable Hydrocarbons mg/kg ND 6.50 08/09/22 11:082.17
o-Terphenyl (S)%77.1 40.0-140 08/09/22 11:08
2-Fluorobiphenyl (S)%85 40.0-140 08/09/22 11:08
2-Bromonaphthalene (S)%84.6 40.0-140 08/09/22 11:08
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3824521-2LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3824521-3
Aliphatic (C09-C18)mg/kg 23.039.9 57.6 40.0-14055.422.1 3.99 25
Aliphatic (C19-C36)mg/kg 35.653.2 66.9 40.0-14062.433.2 6.98 25
1-Chloro-octadecane (S)%64.5 40.0-14059.2
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3824521-5LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3824521-6
Aromatic (C11-C22)mg/kg 74.8113 66.2 40.0-14063.772.0 3.81 25
o-Terphenyl (S)%67.3 40.0-14064.5
2-Fluorobiphenyl (S)%83.3 40.0-14083.5
2-Bromonaphthalene (S)%83.5 40.0-14083.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 85 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616378
MBS.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3824521-7MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1519992-05
R3824521-8
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Aliphatic (C09-C18)mg/kg MH44.7 173 40.0-140105 18.4 5044.0109 186 155
Aliphatic (C19-C36)mg/kg P659.6 248 40.0-140227 3.26 5058.7306 454 439
1-Chloro-octadecane (S)%53.4 40.0-14063.2
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3824521-9MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1519992-05
R3824521-10
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Aromatic (C11-C22)mg/kg MH12715040.0-140103 18.1 50124188379316
o-Terphenyl (S)%69.7 40.0-14066.2
2-Fluorobiphenyl (S)%100 40.0-14082.4
2-Bromonaphthalene (S)%100 40.0-14081.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 86 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616378
MBS.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
712637
EPA 5030B
EPA 8015C
Gasoline Range Organics
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92616378001, 92616378002, 92616378003, 92616378004, 92616378005, 92616378006, 92616378007,
92616378008, 92616378009, 92616378010, 92616378011, 92616378012, 92616378013, 92616378014
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3715799
Associated Lab Samples:92616378001, 92616378002, 92616378003, 92616378004, 92616378005, 92616378006, 92616378007,
92616378008, 92616378009, 92616378010, 92616378011, 92616378012, 92616378013, 92616378014
Matrix:Solid
AnalyzedMDL
Gas Range Organics (C6-C10)mg/kg ND 6.0 07/25/22 15:491.7
4-Bromofluorobenzene (S)%104 66-130 07/25/22 15:49
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3715800LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10)mg/kg 50.249.8 101 70-130
4-Bromofluorobenzene (S)%104 66-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3715802MATRIX SPIKE SAMPLE:
MSSpike
Result
92616378002
Gas Range Organics (C6-C10)mg/kg 48.356.1 84 65-146ND
4-Bromofluorobenzene (S)%105 66-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92616378001
3715801SAMPLE DUPLICATE:
Gas Range Organics (C6-C10)mg/kg ND 30ND
4-Bromofluorobenzene (S)%105105
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 87 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616378
MBS.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
713150
EPA 5030B
EPA 8015C
Gasoline Range Organics
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92616378015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3718315
Associated Lab Samples:92616378015
Matrix:Solid
AnalyzedMDL
Gas Range Organics (C6-C10)mg/kg ND 6.0 07/27/22 18:001.7
4-Bromofluorobenzene (S)%108 66-130 07/27/22 18:00
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3718316LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10)mg/kg 46.449.7 93 70-130
4-Bromofluorobenzene (S)%110 66-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3719717MATRIX SPIKE SAMPLE:
MSSpike
Result
92616565004
Gas Range Organics (C6-C10)mg/kg 79.875.7 104 65-146ND
4-Bromofluorobenzene (S)%109 66-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92616378015
3719531SAMPLE DUPLICATE:
Gas Range Organics (C6-C10)mg/kg ND 30ND
4-Bromofluorobenzene (S)%110111
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 88 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616378
MBS.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
712441
MADEP VPH
MADEP VPH
VPH NC Soil
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92616378016, 92616378017, 92616378018, 92616378019, 92616378020, 92616378021, 92616378022,
92616378023, 92616378024, 92616378025, 92616378026, 92616378027
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3714904
Associated Lab Samples:92616378016, 92616378017, 92616378018, 92616378019, 92616378020, 92616378021, 92616378022,
92616378023, 92616378024, 92616378025, 92616378026, 92616378027
Matrix:Solid
AnalyzedMDL
Aliphatic (C05-C08)mg/kg ND 2.5 N207/22/22 20:402.5
Aromatic (C09-C10)mg/kg ND 2.5 N207/22/22 20:402.5
4-Bromofluorobenzene (FID) (S)%98 70-130 07/22/22 20:40
4-Bromofluorobenzene (PID) (S)%87 70-130 07/22/22 20:40
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3714905LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
3714906
Aliphatic (C05-C08)mg/kg 14.6 N215.2 96 70-1309213.9 5 25
Aromatic (C09-C10)mg/kg 4.9 N25.1 97 70-130944.7 3 25
4-Bromofluorobenzene (FID) (S)%102 70-130101
4-Bromofluorobenzene (PID) (S)%93 70-13091
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 89 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616378
MBS.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
712702
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92616378016, 92616378017, 92616378018, 92616378019, 92616378020
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3716267
Associated Lab Samples:92616378016, 92616378017, 92616378018, 92616378019, 92616378020
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 07/26/22 13:501.9
1,1,1-Trichloroethane ug/kg ND 5.0 07/26/22 13:502.6
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 07/26/22 13:501.3
1,1,2-Trichloroethane ug/kg ND 5.0 07/26/22 13:501.7
1,1-Dichloroethane ug/kg ND 5.0 07/26/22 13:502.1
1,1-Dichloroethene ug/kg ND 5.0 07/26/22 13:502.1
1,1-Dichloropropene ug/kg ND 5.0 07/26/22 13:502.4
1,2,3-Trichlorobenzene ug/kg ND 5.0 IK,v207/26/22 13:504.0
1,2,3-Trichloropropane ug/kg ND 5.0 07/26/22 13:502.5
1,2,4-Trichlorobenzene ug/kg ND 5.0 07/26/22 13:504.2
1,2,4-Trimethylbenzene ug/kg ND 5.0 07/26/22 13:501.4
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 IK07/26/22 13:501.9
1,2-Dibromoethane (EDB)ug/kg ND 5.0 07/26/22 13:502.2
1,2-Dichlorobenzene ug/kg ND 5.0 07/26/22 13:501.8
1,2-Dichloroethane ug/kg ND 5.0 07/26/22 13:503.3
1,2-Dichloropropane ug/kg ND 5.0 07/26/22 13:501.5
1,3,5-Trimethylbenzene ug/kg ND 5.0 07/26/22 13:501.7
1,3-Dichlorobenzene ug/kg ND 5.0 07/26/22 13:501.6
1,3-Dichloropropane ug/kg ND 5.0 07/26/22 13:501.6
1,4-Dichlorobenzene ug/kg ND 5.0 07/26/22 13:501.3
2,2-Dichloropropane ug/kg ND 5.0 v207/26/22 13:501.6
2-Butanone (MEK)ug/kg ND 100 07/26/22 13:5024.0
2-Chlorotoluene ug/kg ND 5.0 07/26/22 13:501.8
2-Hexanone ug/kg ND 50.0 07/26/22 13:504.8
4-Chlorotoluene ug/kg ND 5.0 07/26/22 13:500.88
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 07/26/22 13:504.8
Acetone ug/kg ND 100 07/26/22 13:5032.1
Benzene ug/kg ND 5.0 07/26/22 13:502.0
Bromobenzene ug/kg ND 5.0 07/26/22 13:501.6
Bromochloromethane ug/kg ND 5.0 07/26/22 13:501.5
Bromodichloromethane ug/kg ND 5.0 07/26/22 13:501.9
Bromoform ug/kg ND 5.0 07/26/22 13:501.8
Bromomethane ug/kg ND 10.0 IK,v107/26/22 13:507.9
Carbon tetrachloride ug/kg ND 5.0 07/26/22 13:501.9
Chlorobenzene ug/kg ND 5.0 07/26/22 13:500.96
Chloroethane ug/kg ND 10.0 07/26/22 13:503.9
Chloroform ug/kg 5.0 5.0 07/26/22 13:503.0
Chloromethane ug/kg ND 10.0 07/26/22 13:504.2
cis-1,2-Dichloroethene ug/kg ND 5.0 07/26/22 13:501.7
cis-1,3-Dichloropropene ug/kg ND 5.0 07/26/22 13:501.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 90 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616378
MBS.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3716267
Associated Lab Samples:92616378016, 92616378017, 92616378018, 92616378019, 92616378020
Matrix:Solid
AnalyzedMDL
Dibromochloromethane ug/kg ND 5.0 07/26/22 13:502.8
Dibromomethane ug/kg ND 5.0 07/26/22 13:501.1
Dichlorodifluoromethane ug/kg ND 10.0 IH07/26/22 13:502.2
Diisopropyl ether ug/kg ND 5.0 07/26/22 13:501.4
Ethylbenzene ug/kg ND 5.0 07/26/22 13:502.3
Hexachloro-1,3-butadiene ug/kg ND 10.0 07/26/22 13:508.2
Isopropylbenzene (Cumene)ug/kg ND 5.0 07/26/22 13:501.7
m&p-Xylene ug/kg ND 10.0 07/26/22 13:503.4
Methyl-tert-butyl ether ug/kg ND 5.0 07/26/22 13:501.9
Methylene Chloride ug/kg ND 20.0 07/26/22 13:5013.7
n-Butylbenzene ug/kg ND 5.0 07/26/22 13:502.4
n-Propylbenzene ug/kg ND 5.0 07/26/22 13:501.8
Naphthalene ug/kg ND 5.0 v207/26/22 13:502.6
o-Xylene ug/kg ND 5.0 07/26/22 13:502.2
p-Isopropyltoluene ug/kg ND 5.0 07/26/22 13:502.5
sec-Butylbenzene ug/kg ND 5.0 07/26/22 13:502.2
Styrene ug/kg ND 5.0 07/26/22 13:501.3
tert-Butylbenzene ug/kg ND 5.0 07/26/22 13:501.8
Tetrachloroethene ug/kg ND 5.0 07/26/22 13:501.6
Toluene ug/kg ND 5.0 07/26/22 13:501.4
trans-1,2-Dichloroethene ug/kg ND 5.0 07/26/22 13:501.8
trans-1,3-Dichloropropene ug/kg ND 5.0 07/26/22 13:501.7
Trichloroethene ug/kg ND 5.0 07/26/22 13:501.3
Trichlorofluoromethane ug/kg ND 5.0 07/26/22 13:502.8
Vinyl acetate ug/kg ND 50.0 07/26/22 13:503.6
Vinyl chloride ug/kg ND 10.0 07/26/22 13:502.5
Xylene (Total)ug/kg ND 10.0 07/26/22 13:502.8
1,2-Dichloroethane-d4 (S)%112 70-130 07/26/22 13:50
4-Bromofluorobenzene (S)%96 69-134 07/26/22 13:50
Toluene-d8 (S)%100 70-130 07/26/22 13:50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3716268LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 12501250 100 70-130
1,1,1-Trichloroethane ug/kg 11201250 89 70-130
1,1,2,2-Tetrachloroethane ug/kg 11701250 94 70-130
1,1,2-Trichloroethane ug/kg 11601250 93 70-130
1,1-Dichloroethane ug/kg 11701250 94 70-130
1,1-Dichloroethene ug/kg 12001250 96 70-130
1,1-Dichloropropene ug/kg 11801250 94 70-130
1,2,3-Trichlorobenzene ug/kg 841 IK,v312506765-130
1,2,3-Trichloropropane ug/kg 11801250 94 70-130
1,2,4-Trichlorobenzene ug/kg 10901250 87 68-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 91 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616378
MBS.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3716268LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 12901250 103 70-130
1,2-Dibromo-3-chloropropane ug/kg 1070 IK12508670-130
1,2-Dibromoethane (EDB)ug/kg 12601250 101 70-130
1,2-Dichlorobenzene ug/kg 12201250 97 70-130
1,2-Dichloroethane ug/kg 11901250 96 63-130
1,2-Dichloropropane ug/kg 12101250 97 70-130
1,3,5-Trimethylbenzene ug/kg 12801250 102 70-130
1,3-Dichlorobenzene ug/kg 12301250 98 70-130
1,3-Dichloropropane ug/kg 12701250 102 70-130
1,4-Dichlorobenzene ug/kg 12601250 101 70-130
2,2-Dichloropropane ug/kg 864 v312506966-130
2-Butanone (MEK)ug/kg 20702500 83 70-130
2-Chlorotoluene ug/kg 12801250 102 70-130
2-Hexanone ug/kg 23502500 94 70-130
4-Chlorotoluene ug/kg 12801250 102 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 22702500 91 70-130
Acetone ug/kg 24002500 96 69-130
Benzene ug/kg 11101250 89 70-130
Bromobenzene ug/kg 12601250 101 70-130
Bromochloromethane ug/kg 11401250 91 70-130
Bromodichloromethane ug/kg 12101250 97 69-130
Bromoform ug/kg 12401250 99 70-130
Bromomethane ug/kg 1630 IK,v1125013052-130
Carbon tetrachloride ug/kg 10901250 87 70-130
Chlorobenzene ug/kg 12701250 102 70-130
Chloroethane ug/kg 13701250 110 65-130
Chloroform ug/kg 11301250 90 70-130
Chloromethane ug/kg 13801250 110 55-130
cis-1,2-Dichloroethene ug/kg 12101250 96 70-130
cis-1,3-Dichloropropene ug/kg 11701250 94 70-130
Dibromochloromethane ug/kg 12501250 100 70-130
Dibromomethane ug/kg 11501250 92 70-130
Dichlorodifluoromethane ug/kg 1470 IH125011745-156
Diisopropyl ether ug/kg 12501250 100 70-130
Ethylbenzene ug/kg 11501250 92 70-130
Hexachloro-1,3-butadiene ug/kg 10401250 83 66-130
Isopropylbenzene (Cumene)ug/kg 12001250 96 70-130
m&p-Xylene ug/kg 24802500 99 70-130
Methyl-tert-butyl ether ug/kg 11301250 91 70-130
Methylene Chloride ug/kg 12201250 97 65-130
n-Butylbenzene ug/kg 12401250 99 67-130
n-Propylbenzene ug/kg 12701250 101 70-130
Naphthalene ug/kg 952 v312507670-130
o-Xylene ug/kg 11801250 95 70-130
p-Isopropyltoluene ug/kg 12801250 102 67-130
sec-Butylbenzene ug/kg 12301250 99 69-130
Styrene ug/kg 12501250 100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 92 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616378
MBS.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3716268LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 12401250 100 67-130
Tetrachloroethene ug/kg 12401250 99 70-130
Toluene ug/kg 10701250 86 70-130
trans-1,2-Dichloroethene ug/kg 11801250 95 70-130
trans-1,3-Dichloropropene ug/kg 11801250 94 68-130
Trichloroethene ug/kg 11301250 91 70-130
Trichlorofluoromethane ug/kg 11801250 94 70-130
Vinyl acetate ug/kg 26402500 105 70-130
Vinyl chloride ug/kg 14001250 112 61-130
Xylene (Total)ug/kg 36603750 98 70-130
1,2-Dichloroethane-d4 (S)%105 70-130
4-Bromofluorobenzene (S)%100 69-134
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3716269MATRIX SPIKE SAMPLE:
MSSpike
Result
92616337001
1,1,1,2-Tetrachloroethane ug/kg 1030819 125 70-131ND
1,1,1-Trichloroethane ug/kg 1060819 130 65-133ND
1,1,2,2-Tetrachloroethane ug/kg 969819 118 66-130ND
1,1,2-Trichloroethane ug/kg 940819 115 66-133ND
1,1-Dichloroethane ug/kg 1050819 128 65-130ND
1,1-Dichloroethene ug/kg 1170819 143 10-158ND
1,1-Dichloropropene ug/kg 1120 M181913768-133ND
1,2,3-Trichlorobenzene ug/kg 439 IK,v38195427-138ND
1,2,3-Trichloropropane ug/kg 940819 115 67-130ND
1,2,4-Trichlorobenzene ug/kg 829819 101 51-134ND
1,2,4-Trimethylbenzene ug/kg 1080819 132 63-136ND
1,2-Dibromo-3-chloropropane ug/kg 811 IK8199932-130ND
1,2-Dibromoethane (EDB)ug/kg 1000819 122 70-130ND
1,2-Dichlorobenzene ug/kg 1030819 125 69-130ND
1,2-Dichloroethane ug/kg 992819 121 59-130ND
1,2-Dichloropropane ug/kg 1060819 130 70-130ND
1,3,5-Trimethylbenzene ug/kg 1100819 134 65-137ND
1,3-Dichlorobenzene ug/kg 1040819 127 70-130ND
1,3-Dichloropropane ug/kg 1020819 125 70-130ND
1,4-Dichlorobenzene ug/kg 1050819 128 68-130ND
2,2-Dichloropropane ug/kg 693 v38198532-130ND
2-Butanone (MEK)ug/kg 16401640 94 10-136109J
2-Chlorotoluene ug/kg 1090819 133 69-141ND
2-Hexanone ug/kg 18201640 111 10-144ND
4-Chlorotoluene ug/kg 1070819 131 70-132ND
4-Methyl-2-pentanone (MIBK)ug/kg 18201640 111 25-143ND
Acetone ug/kg 16801640 103 10-130ND
Benzene ug/kg 1010819 124 67-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 93 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616378
MBS.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3716269MATRIX SPIKE SAMPLE:
MSSpike
Result
92616337001
Bromobenzene ug/kg 1010819 124 70-130ND
Bromochloromethane ug/kg 916819 112 69-134ND
Bromodichloromethane ug/kg 986819 120 64-130ND
Bromoform ug/kg 924819 113 62-130ND
Bromomethane ug/kg 330 IK,v18194020-176ND
Carbon tetrachloride ug/kg 1010819 123 65-140ND
Chlorobenzene ug/kg 1070 M181913170-130ND
Chloroethane ug/kg 203819 24 10-130ND
Chloroform ug/kg 947819 116 63-130ND
Chloromethane ug/kg 1350 M181916558-130ND
cis-1,2-Dichloroethene ug/kg 1060819 129 66-130ND
cis-1,3-Dichloropropene ug/kg 948819 116 67-130ND
Dibromochloromethane ug/kg 958819 117 67-130ND
Dibromomethane ug/kg 920819 112 63-131ND
Dichlorodifluoromethane ug/kg 1710 IH,M181920944-180ND
Diisopropyl ether ug/kg 1090 M181913363-130ND
Ethylbenzene ug/kg 1020819 124 66-130ND
Hexachloro-1,3-butadiene ug/kg 1050819 128 64-150ND
Isopropylbenzene (Cumene)ug/kg 1070819 131 69-135ND
m&p-Xylene ug/kg 21901640 133 60-133ND
Methyl-tert-butyl ether ug/kg 901819 110 65-130ND
Methylene Chloride ug/kg 1040819 127 61-130ND
n-Butylbenzene ug/kg 1090819 134 65-140ND
n-Propylbenzene ug/kg 1090819 133 67-140ND
Naphthalene ug/kg 454 v38195515-145ND
o-Xylene ug/kg 1020819 124 66-133ND
p-Isopropyltoluene ug/kg 1130819 138 56-147ND
sec-Butylbenzene ug/kg 1120819 137 65-139ND
Styrene ug/kg 1030819 126 70-132ND
tert-Butylbenzene ug/kg 1100819 134 62-135ND
Tetrachloroethene ug/kg 1040819 127 70-135ND
Toluene ug/kg 973819 119 67-130ND
trans-1,2-Dichloroethene ug/kg 1090 M181913469-130ND
trans-1,3-Dichloropropene ug/kg 936819 114 62-130ND
Trichloroethene ug/kg 1050819 128 70-135ND
Trichlorofluoromethane ug/kg 246819 30 10-130ND
Vinyl acetate ug/kg 20101640 122 53-130ND
Vinyl chloride ug/kg 1280 M181915761-148ND
Xylene (Total)ug/kg 32002450 130 63-132ND
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%99 69-134
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 94 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616378
MBS.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92616337002
3716270SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND IK,v230ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND IK30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND v230ND
2-Butanone (MEK)ug/kg ND 3055.1J
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg ND 30ND
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND IK,v130ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND IH30ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 95 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616378
MBS.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92616337002
3716270SAMPLE DUPLICATE:
m&p-Xylene ug/kg ND 30ND
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg ND 30ND
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg ND v230ND
o-Xylene ug/kg ND 30ND
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg ND 30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
Xylene (Total)ug/kg ND 30ND
1,2-Dichloroethane-d4 (S)%108109
4-Bromofluorobenzene (S)%9898
Toluene-d8 (S)%101101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 96 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616378
MBS.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
712764
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92616378021, 92616378022, 92616378023, 92616378024, 92616378025, 92616378026, 92616378027
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3716618
Associated Lab Samples:92616378021, 92616378022, 92616378023, 92616378024, 92616378025, 92616378026, 92616378027
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 07/27/22 02:171.9
1,1,1-Trichloroethane ug/kg ND 5.0 07/27/22 02:172.6
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 07/27/22 02:171.3
1,1,2-Trichloroethane ug/kg ND 5.0 07/27/22 02:171.7
1,1-Dichloroethane ug/kg ND 5.0 07/27/22 02:172.1
1,1-Dichloroethene ug/kg ND 5.0 07/27/22 02:172.1
1,1-Dichloropropene ug/kg ND 5.0 07/27/22 02:172.4
1,2,3-Trichlorobenzene ug/kg ND 5.0 IK,v207/27/22 02:174.0
1,2,3-Trichloropropane ug/kg ND 5.0 07/27/22 02:172.5
1,2,4-Trichlorobenzene ug/kg ND 5.0 07/27/22 02:174.2
1,2,4-Trimethylbenzene ug/kg ND 5.0 07/27/22 02:171.4
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 IK07/27/22 02:171.9
1,2-Dibromoethane (EDB)ug/kg ND 5.0 07/27/22 02:172.2
1,2-Dichlorobenzene ug/kg ND 5.0 07/27/22 02:171.8
1,2-Dichloroethane ug/kg ND 5.0 07/27/22 02:173.3
1,2-Dichloropropane ug/kg ND 5.0 07/27/22 02:171.5
1,3,5-Trimethylbenzene ug/kg ND 5.0 07/27/22 02:171.7
1,3-Dichlorobenzene ug/kg ND 5.0 07/27/22 02:171.6
1,3-Dichloropropane ug/kg ND 5.0 07/27/22 02:171.6
1,4-Dichlorobenzene ug/kg ND 5.0 07/27/22 02:171.3
2,2-Dichloropropane ug/kg ND 5.0 07/27/22 02:171.6
2-Butanone (MEK)ug/kg ND 100 07/27/22 02:1724.0
2-Chlorotoluene ug/kg ND 5.0 07/27/22 02:171.8
2-Hexanone ug/kg ND 50.0 07/27/22 02:174.8
4-Chlorotoluene ug/kg ND 5.0 07/27/22 02:170.88
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 07/27/22 02:174.8
Acetone ug/kg ND 100 07/27/22 02:1732.1
Benzene ug/kg ND 5.0 07/27/22 02:172.0
Bromobenzene ug/kg ND 5.0 07/27/22 02:171.6
Bromochloromethane ug/kg ND 5.0 07/27/22 02:171.5
Bromodichloromethane ug/kg ND 5.0 07/27/22 02:171.9
Bromoform ug/kg ND 5.0 07/27/22 02:171.8
Bromomethane ug/kg ND 10.0 IK,v107/27/22 02:177.9
Carbon tetrachloride ug/kg ND 5.0 07/27/22 02:171.9
Chlorobenzene ug/kg ND 5.0 07/27/22 02:170.96
Chloroethane ug/kg ND 10.0 07/27/22 02:173.9
Chloroform ug/kg 5.0J 5.0 07/27/22 02:173.0
Chloromethane ug/kg ND 10.0 07/27/22 02:174.2
cis-1,2-Dichloroethene ug/kg ND 5.0 07/27/22 02:171.7
cis-1,3-Dichloropropene ug/kg ND 5.0 07/27/22 02:171.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 97 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616378
MBS.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3716618
Associated Lab Samples:92616378021, 92616378022, 92616378023, 92616378024, 92616378025, 92616378026, 92616378027
Matrix:Solid
AnalyzedMDL
Dibromochloromethane ug/kg ND 5.0 07/27/22 02:172.8
Dibromomethane ug/kg ND 5.0 07/27/22 02:171.1
Dichlorodifluoromethane ug/kg ND 10.0 IH07/27/22 02:172.2
Diisopropyl ether ug/kg ND 5.0 07/27/22 02:171.4
Ethylbenzene ug/kg ND 5.0 07/27/22 02:172.3
Hexachloro-1,3-butadiene ug/kg ND 10.0 07/27/22 02:178.2
Isopropylbenzene (Cumene)ug/kg ND 5.0 07/27/22 02:171.7
m&p-Xylene ug/kg ND 10.0 07/27/22 02:173.4
Methyl-tert-butyl ether ug/kg ND 5.0 07/27/22 02:171.9
Methylene Chloride ug/kg ND 20.0 07/27/22 02:1713.7
n-Butylbenzene ug/kg ND 5.0 07/27/22 02:172.4
n-Propylbenzene ug/kg ND 5.0 07/27/22 02:171.8
Naphthalene ug/kg ND 5.0 v207/27/22 02:172.6
o-Xylene ug/kg ND 5.0 07/27/22 02:172.2
p-Isopropyltoluene ug/kg ND 5.0 07/27/22 02:172.5
sec-Butylbenzene ug/kg ND 5.0 07/27/22 02:172.2
Styrene ug/kg ND 5.0 07/27/22 02:171.3
tert-Butylbenzene ug/kg ND 5.0 07/27/22 02:171.8
Tetrachloroethene ug/kg ND 5.0 07/27/22 02:171.6
Toluene ug/kg ND 5.0 07/27/22 02:171.4
trans-1,2-Dichloroethene ug/kg ND 5.0 07/27/22 02:171.8
trans-1,3-Dichloropropene ug/kg ND 5.0 07/27/22 02:171.7
Trichloroethene ug/kg ND 5.0 07/27/22 02:171.3
Trichlorofluoromethane ug/kg ND 5.0 07/27/22 02:172.8
Vinyl acetate ug/kg ND 50.0 07/27/22 02:173.6
Vinyl chloride ug/kg ND 10.0 07/27/22 02:172.5
Xylene (Total)ug/kg ND 10.0 07/27/22 02:172.8
1,2-Dichloroethane-d4 (S)%111 70-130 07/27/22 02:17
4-Bromofluorobenzene (S)%94 69-134 07/27/22 02:17
Toluene-d8 (S)%100 70-130 07/27/22 02:17
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3716619LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 12901250 103 70-130
1,1,1-Trichloroethane ug/kg 11901250 95 70-130
1,1,2,2-Tetrachloroethane ug/kg 12301250 98 70-130
1,1,2-Trichloroethane ug/kg 12301250 98 70-130
1,1-Dichloroethane ug/kg 12601250 100 70-130
1,1-Dichloroethene ug/kg 13101250 105 70-130
1,1-Dichloropropene ug/kg 12601250 101 70-130
1,2,3-Trichlorobenzene ug/kg 931 IK,v312507565-130
1,2,3-Trichloropropane ug/kg 12601250 101 70-130
1,2,4-Trichlorobenzene ug/kg 11201250 90 68-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 98 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616378
MBS.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3716619LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 13601250 108 70-130
1,2-Dibromo-3-chloropropane ug/kg 1130 IK12509170-130
1,2-Dibromoethane (EDB)ug/kg 13001250 104 70-130
1,2-Dichlorobenzene ug/kg 12601250 101 70-130
1,2-Dichloroethane ug/kg 12501250 100 63-130
1,2-Dichloropropane ug/kg 12901250 103 70-130
1,3,5-Trimethylbenzene ug/kg 13401250 107 70-130
1,3-Dichlorobenzene ug/kg 12801250 103 70-130
1,3-Dichloropropane ug/kg 13001250 104 70-130
1,4-Dichlorobenzene ug/kg 12701250 102 70-130
2,2-Dichloropropane ug/kg 11301250 91 66-130
2-Butanone (MEK)ug/kg 22602500 90 70-130
2-Chlorotoluene ug/kg 13201250 106 70-130
2-Hexanone ug/kg 24802500 99 70-130
4-Chlorotoluene ug/kg 13401250 107 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 24302500 97 70-130
Acetone ug/kg 24502500 98 69-130
Benzene ug/kg 11901250 96 70-130
Bromobenzene ug/kg 13001250 104 70-130
Bromochloromethane ug/kg 12001250 96 70-130
Bromodichloromethane ug/kg 12801250 103 69-130
Bromoform ug/kg 12601250 101 70-130
Bromomethane ug/kg 1750 IK,L1,v1125014052-130
Carbon tetrachloride ug/kg 11901250 95 70-130
Chlorobenzene ug/kg 13201250 105 70-130
Chloroethane ug/kg 14801250 119 65-130
Chloroform ug/kg 12201250 97 70-130
Chloromethane ug/kg 15001250 120 55-130
cis-1,2-Dichloroethene ug/kg 12901250 103 70-130
cis-1,3-Dichloropropene ug/kg 12901250 103 70-130
Dibromochloromethane ug/kg 12801250 102 70-130
Dibromomethane ug/kg 12001250 96 70-130
Dichlorodifluoromethane ug/kg 1720 IH125013845-156
Diisopropyl ether ug/kg 13001250 104 70-130
Ethylbenzene ug/kg 12101250 96 70-130
Hexachloro-1,3-butadiene ug/kg 11301250 91 66-130
Isopropylbenzene (Cumene)ug/kg 12701250 101 70-130
m&p-Xylene ug/kg 26002500 104 70-130
Methyl-tert-butyl ether ug/kg 11701250 93 70-130
Methylene Chloride ug/kg 13201250 105 65-130
n-Butylbenzene ug/kg 13301250 107 67-130
n-Propylbenzene ug/kg 13401250 107 70-130
Naphthalene ug/kg 1050 v312508470-130
o-Xylene ug/kg 12401250 99 70-130
p-Isopropyltoluene ug/kg 13601250 109 67-130
sec-Butylbenzene ug/kg 13101250 105 69-130
Styrene ug/kg 13101250 105 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 99 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616378
MBS.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3716619LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 13801250 110 67-130
Tetrachloroethene ug/kg 12701250 102 70-130
Toluene ug/kg 11501250 92 70-130
trans-1,2-Dichloroethene ug/kg 12801250 102 70-130
trans-1,3-Dichloropropene ug/kg 12801250 103 68-130
Trichloroethene ug/kg 12401250 99 70-130
Trichlorofluoromethane ug/kg 13601250 109 70-130
Vinyl acetate ug/kg 28202500 113 70-130
Vinyl chloride ug/kg 15201250 122 61-130
Xylene (Total)ug/kg 38503750 103 70-130
1,2-Dichloroethane-d4 (S)%105 70-130
4-Bromofluorobenzene (S)%99 69-134
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3718293MATRIX SPIKE SAMPLE:
MSSpike
Result
92616378022
1,1,1,2-Tetrachloroethane ug/kg 837718 116 70-131ND
1,1,1-Trichloroethane ug/kg 866718 121 65-133ND
1,1,2,2-Tetrachloroethane ug/kg 764718 106 66-130ND
1,1,2-Trichloroethane ug/kg 761718 106 66-133ND
1,1-Dichloroethane ug/kg 859718 120 65-130ND
1,1-Dichloroethene ug/kg 918718 128 10-158ND
1,1-Dichloropropene ug/kg 923718 129 68-133ND
1,2,3-Trichlorobenzene ug/kg 529 IK,v37187427-138ND
1,2,3-Trichloropropane ug/kg 764718 106 67-130ND
1,2,4-Trichlorobenzene ug/kg 762718 106 51-134ND
1,2,4-Trimethylbenzene ug/kg 871718 121 63-136ND
1,2-Dibromo-3-chloropropane ug/kg 668 IK7189332-130ND
1,2-Dibromoethane (EDB)ug/kg 790718 110 70-130ND
1,2-Dichlorobenzene ug/kg 827718 115 69-130ND
1,2-Dichloroethane ug/kg 818718 114 59-130ND
1,2-Dichloropropane ug/kg 844718 117 70-130ND
1,3,5-Trimethylbenzene ug/kg 881718 123 65-137ND
1,3-Dichlorobenzene ug/kg 863718 120 70-130ND
1,3-Dichloropropane ug/kg 815718 113 70-130ND
1,4-Dichlorobenzene ug/kg 829718 115 68-130ND
2,2-Dichloropropane ug/kg 765 v371810732-130ND
2-Butanone (MEK)ug/kg 13001430 85 10-13680.9J
2-Chlorotoluene ug/kg 882718 123 69-141ND
2-Hexanone ug/kg 14001430 98 10-144ND
4-Chlorotoluene ug/kg 867718 121 70-132ND
4-Methyl-2-pentanone (MIBK)ug/kg 14101430 98 25-143ND
Acetone ug/kg 13101430 91 10-130ND
Benzene ug/kg 801718 112 67-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 100 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616378
MBS.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3718293MATRIX SPIKE SAMPLE:
MSSpike
Result
92616378022
Bromobenzene ug/kg 819718 114 70-130ND
Bromochloromethane ug/kg 729718 102 69-134ND
Bromodichloromethane ug/kg 794718 111 64-130ND
Bromoform ug/kg 731718 102 62-130ND
Bromomethane ug/kg 274 IK,v17183820-176ND
Carbon tetrachloride ug/kg 803718 112 65-140ND
Chlorobenzene ug/kg 877718 122 70-130ND
Chloroethane ug/kg 117718 16 10-130ND
Chloroform ug/kg 789718 110 63-130ND
Chloromethane ug/kg 1110 M171815458-130ND
cis-1,2-Dichloroethene ug/kg 861718 120 66-130ND
cis-1,3-Dichloropropene ug/kg 806718 112 67-130ND
Dibromochloromethane ug/kg 775718 108 67-130ND
Dibromomethane ug/kg 724718 101 63-131ND
Dichlorodifluoromethane ug/kg 1390 IH,M171819344-180ND
Diisopropyl ether ug/kg 879718 122 63-130ND
Ethylbenzene ug/kg 816718 114 66-130ND
Hexachloro-1,3-butadiene ug/kg 970718 135 64-150ND
Isopropylbenzene (Cumene)ug/kg 862718 120 69-135ND
m&p-Xylene ug/kg 17401430 121 60-133ND
Methyl-tert-butyl ether ug/kg 755718 105 65-130ND
Methylene Chloride ug/kg 912718 127 61-130ND
n-Butylbenzene ug/kg 934718 130 65-140ND
n-Propylbenzene ug/kg 887718 124 67-140ND
Naphthalene ug/kg 519 v37187215-145ND
o-Xylene ug/kg 809718 113 66-133ND
p-Isopropyltoluene ug/kg 930718 129 56-147ND
sec-Butylbenzene ug/kg 913718 127 65-139ND
Styrene ug/kg 836718 116 70-132ND
tert-Butylbenzene ug/kg 871718 121 62-135ND
Tetrachloroethene ug/kg 837718 117 70-135ND
Toluene ug/kg 781718 109 67-130ND
trans-1,2-Dichloroethene ug/kg 898718 125 69-130ND
trans-1,3-Dichloropropene ug/kg 792718 110 62-130ND
Trichloroethene ug/kg 839718 117 70-135ND
Trichlorofluoromethane ug/kg 181718 25 10-130ND
Vinyl acetate ug/kg 17201430 120 53-130ND
Vinyl chloride ug/kg 1050718 146 61-148ND
Xylene (Total)ug/kg 25502160 118 63-132ND
1,2-Dichloroethane-d4 (S)%106 70-130
4-Bromofluorobenzene (S)%99 69-134
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 101 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616378
MBS.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92616378021
3718292SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND IK,v230ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND IK30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND v230ND
2-Butanone (MEK)ug/kg 80.3J 3077.6J
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg ND 30ND
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND IK,v130ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg 5.1J 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND IH30ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg 3.6J 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 102 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616378
MBS.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92616378021
3718292SAMPLE DUPLICATE:
m&p-Xylene ug/kg ND 30ND
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg ND 30ND
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg ND v230ND
o-Xylene ug/kg ND 30ND
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg ND 30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
Xylene (Total)ug/kg ND 30ND
1,2-Dichloroethane-d4 (S)%112105
4-Bromofluorobenzene (S)%10097
Toluene-d8 (S)%101100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 103 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616378
MBS.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
713049
EPA 3546
EPA 8015C
8015 Solid GCSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92616378001, 92616378002, 92616378003, 92616378004, 92616378005, 92616378006, 92616378007,
92616378008, 92616378009, 92616378010, 92616378011, 92616378012, 92616378013, 92616378014,
92616378015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3717994
Associated Lab Samples:92616378001, 92616378002, 92616378003, 92616378004, 92616378005, 92616378006, 92616378007,
92616378008, 92616378009, 92616378010, 92616378011, 92616378012, 92616378013, 92616378014,
92616378015
Matrix:Solid
AnalyzedMDL
Diesel Range Organics(C10-C28)mg/kg ND 4.9 07/27/22 12:313.5
n-Pentacosane (S)%73 10-130 07/27/22 12:31
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3717995LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Range Organics(C10-C28)mg/kg 48.066 73 44-130
n-Pentacosane (S)%81 10-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3717996MATRIX SPIKE SAMPLE:
MSSpike
Result
92615889001
Diesel Range Organics(C10-C28)mg/kg 43.566 60 10-130ND
n-Pentacosane (S)%69 10-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92615892001
3717997SAMPLE DUPLICATE:
Diesel Range Organics(C10-C28)mg/kg ND 30ND
n-Pentacosane (S)%7167
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 104 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616378
MBS.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
713046
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92616378016, 92616378017, 92616378018, 92616378019, 92616378020, 92616378021, 92616378022,
92616378023, 92616378024, 92616378025, 92616378026, 92616378027
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3717980
Associated Lab Samples:92616378016, 92616378017, 92616378018, 92616378019, 92616378020, 92616378021, 92616378022,
92616378023, 92616378024, 92616378025, 92616378026, 92616378027
Matrix:Solid
AnalyzedMDL
1,2,4-Trichlorobenzene ug/kg ND 326 07/27/22 12:49128
1,2-Dichlorobenzene ug/kg ND 326 07/27/22 12:49117
1,3-Dichlorobenzene ug/kg ND 326 07/27/22 12:49115
1,4-Dichlorobenzene ug/kg ND 326 07/27/22 12:49124
1-Methylnaphthalene ug/kg ND 326 07/27/22 12:49114
2,2'-Oxybis(1-chloropropane)ug/kg ND 326 07/27/22 12:49155
2,4,5-Trichlorophenol ug/kg ND 326 07/27/22 12:49149
2,4,6-Trichlorophenol ug/kg ND 326 07/27/22 12:49134
2,4-Dichlorophenol ug/kg ND 326 07/27/22 12:49127
2,4-Dimethylphenol ug/kg ND 326 07/27/22 12:49135
2,4-Dinitrophenol ug/kg ND 1630 07/27/22 12:491010
2,4-Dinitrotoluene ug/kg ND 326 07/27/22 12:49125
2,6-Dinitrotoluene ug/kg ND 326 07/27/22 12:49119
2-Chloronaphthalene ug/kg ND 326 07/27/22 12:49129
2-Chlorophenol ug/kg ND 326 07/27/22 12:49122
2-Methylnaphthalene ug/kg ND 326 07/27/22 12:49130
2-Methylphenol(o-Cresol)ug/kg ND 326 07/27/22 12:49133
2-Nitroaniline ug/kg ND 1630 07/27/22 12:49266
2-Nitrophenol ug/kg ND 326 07/27/22 12:49141
3&4-Methylphenol(m&p Cresol)ug/kg ND 326 07/27/22 12:49131
3,3'-Dichlorobenzidine ug/kg ND 651 07/27/22 12:49220
3-Nitroaniline ug/kg ND 1630 07/27/22 12:49256
4,6-Dinitro-2-methylphenol ug/kg ND 651 07/27/22 12:49304
4-Bromophenylphenyl ether ug/kg ND 326 07/27/22 12:49125
4-Chloro-3-methylphenol ug/kg ND 651 07/27/22 12:49229
4-Chloroaniline ug/kg ND 651 07/27/22 12:49256
4-Chlorophenylphenyl ether ug/kg ND 326 07/27/22 12:49121
4-Nitroaniline ug/kg ND 651 07/27/22 12:49248
4-Nitrophenol ug/kg ND 1630 07/27/22 12:49630
Acenaphthene ug/kg ND 326 07/27/22 12:49114
Acenaphthylene ug/kg ND 326 07/27/22 12:49114
Aniline ug/kg ND 326 07/27/22 12:49127
Anthracene ug/kg ND 326 07/27/22 12:49107
Benzo(a)anthracene ug/kg ND 326 07/27/22 12:49109
Benzo(a)pyrene ug/kg ND 326 07/27/22 12:49112
Benzo(b)fluoranthene ug/kg ND 326 07/27/22 12:49109
Benzo(g,h,i)perylene ug/kg ND 326 07/27/22 12:49126
Benzo(k)fluoranthene ug/kg ND 326 07/27/22 12:49114
Benzoic Acid ug/kg ND 1630 07/27/22 12:49700
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 105 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616378
MBS.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3717980
Associated Lab Samples:92616378016, 92616378017, 92616378018, 92616378019, 92616378020, 92616378021, 92616378022,
92616378023, 92616378024, 92616378025, 92616378026, 92616378027
Matrix:Solid
AnalyzedMDL
Benzyl alcohol ug/kg ND 651 07/27/22 12:49247
bis(2-Chloroethoxy)methane ug/kg ND 326 07/27/22 12:49135
bis(2-Chloroethyl) ether ug/kg ND 326 07/27/22 12:49122
bis(2-Ethylhexyl)phthalate ug/kg ND 326 v107/27/22 12:49126
Butylbenzylphthalate ug/kg ND 326 07/27/22 12:49137
Chrysene ug/kg ND 326 07/27/22 12:49118
Di-n-butylphthalate ug/kg ND 326 07/27/22 12:49110
Di-n-octylphthalate ug/kg ND 326 v107/27/22 12:49128
Dibenz(a,h)anthracene ug/kg ND 326 07/27/22 12:49125
Dibenzofuran ug/kg ND 326 07/27/22 12:49117
Diethylphthalate ug/kg ND 326 07/27/22 12:49119
Dimethylphthalate ug/kg ND 326 07/27/22 12:49118
Fluoranthene ug/kg ND 326 07/27/22 12:49112
Fluorene ug/kg ND 326 07/27/22 12:49114
Hexachloro-1,3-butadiene ug/kg ND 326 07/27/22 12:49141
Hexachlorobenzene ug/kg ND 326 07/27/22 12:49127
Hexachlorocyclopentadiene ug/kg ND 326 07/27/22 12:49187
Hexachloroethane ug/kg ND 326 07/27/22 12:49124
Indeno(1,2,3-cd)pyrene ug/kg ND 326 07/27/22 12:49128
Isophorone ug/kg ND 326 07/27/22 12:49145
N-Nitroso-di-n-propylamine ug/kg ND 326 07/27/22 12:49122
N-Nitrosodimethylamine ug/kg ND 326 07/27/22 12:49110
N-Nitrosodiphenylamine ug/kg ND 326 07/27/22 12:49115
Naphthalene ug/kg ND 326 07/27/22 12:49111
Nitrobenzene ug/kg ND 326 07/27/22 12:49151
Pentachlorophenol ug/kg ND 651 07/27/22 12:49319
Phenanthrene ug/kg ND 326 07/27/22 12:49107
Phenol ug/kg ND 326 07/27/22 12:49145
Pyrene ug/kg ND 326 07/27/22 12:49132
Pyridine ug/kg ND 326 07/27/22 12:49103
2,4,6-Tribromophenol (S)%73 18-130 07/27/22 12:49
2-Fluorobiphenyl (S)%61 19-130 07/27/22 12:49
2-Fluorophenol (S)%63 18-130 07/27/22 12:49
Nitrobenzene-d5 (S)%63 21-130 07/27/22 12:49
Phenol-d6 (S)%64 18-130 07/27/22 12:49
Terphenyl-d14 (S)%85 15-130 07/27/22 12:49
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3717981LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 11101640 67 47-130
1,2-Dichlorobenzene ug/kg 10901640 66 49-130
1,3-Dichlorobenzene ug/kg 10701640 65 48-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 106 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616378
MBS.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3717981LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dichlorobenzene ug/kg 10701640 65 49-130
1-Methylnaphthalene ug/kg 12301640 75 54-130
2,2'-Oxybis(1-chloropropane)ug/kg 11301640 69 38-130
2,4,5-Trichlorophenol ug/kg 13201640 80 49-130
2,4,6-Trichlorophenol ug/kg 14201640 86 50-130
2,4-Dichlorophenol ug/kg 12001640 73 51-130
2,4-Dimethylphenol ug/kg 13101640 79 53-130
2,4-Dinitrophenol ug/kg 76708220 93 39-130
2,4-Dinitrotoluene ug/kg 14801640 90 53-130
2,6-Dinitrotoluene ug/kg 14801640 90 55-130
2-Chloronaphthalene ug/kg 12801640 78 48-130
2-Chlorophenol ug/kg 11401640 69 54-130
2-Methylnaphthalene ug/kg 12001640 73 57-130
2-Methylphenol(o-Cresol)ug/kg 11101640 67 50-130
2-Nitroaniline ug/kg 27903290 85 49-130
2-Nitrophenol ug/kg 13301640 81 50-130
3&4-Methylphenol(m&p Cresol)ug/kg 11301640 69 50-130
3,3'-Dichlorobenzidine ug/kg 26303290 80 47-130
3-Nitroaniline ug/kg 27903290 85 45-130
4,6-Dinitro-2-methylphenol ug/kg 33003290 100 50-142
4-Bromophenylphenyl ether ug/kg 14501640 88 55-130
4-Chloro-3-methylphenol ug/kg 27203290 83 52-130
4-Chloroaniline ug/kg 25003290 76 49-130
4-Chlorophenylphenyl ether ug/kg 13301640 81 53-130
4-Nitroaniline ug/kg 28003290 85 51-130
4-Nitrophenol ug/kg 72208220 88 40-130
Acenaphthene ug/kg 13801640 84 56-130
Acenaphthylene ug/kg 14901640 90 58-130
Aniline ug/kg 10301640 63 44-130
Anthracene ug/kg 13601640 83 60-130
Benzo(a)anthracene ug/kg 14801640 90 59-130
Benzo(a)pyrene ug/kg 18601640 113 57-130
Benzo(b)fluoranthene ug/kg 17501640 107 54-130
Benzo(g,h,i)perylene ug/kg 15901640 96 59-130
Benzo(k)fluoranthene ug/kg 17001640 104 54-130
Benzoic Acid ug/kg 42108220 51 19-130
Benzyl alcohol ug/kg 23803290 72 50-130
bis(2-Chloroethoxy)methane ug/kg 11601640 70 55-130
bis(2-Chloroethyl) ether ug/kg 10701640 65 53-130
bis(2-Ethylhexyl)phthalate ug/kg 1660 v1164010158-130
Butylbenzylphthalate ug/kg 15801640 96 46-138
Chrysene ug/kg 14401640 88 57-130
Di-n-butylphthalate ug/kg 15201640 93 57-130
Di-n-octylphthalate ug/kg 1670 v1164010157-130
Dibenz(a,h)anthracene ug/kg 15701640 95 60-130
Dibenzofuran ug/kg 13901640 85 54-130
Diethylphthalate ug/kg 14001640 85 55-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616378
MBS.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3717981LABORATORY CONTROL SAMPLE:
LCSSpike
Dimethylphthalate ug/kg 13801640 84 57-130
Fluoranthene ug/kg 14701640 90 57-130
Fluorene ug/kg 14201640 86 56-130
Hexachloro-1,3-butadiene ug/kg 9971640 61 41-130
Hexachlorobenzene ug/kg 14001640 85 53-130
Hexachlorocyclopentadiene ug/kg 11801640 72 23-130
Hexachloroethane ug/kg 10401640 63 48-130
Indeno(1,2,3-cd)pyrene ug/kg 15901640 97 61-130
Isophorone ug/kg 12001640 73 49-130
N-Nitroso-di-n-propylamine ug/kg 11301640 69 52-130
N-Nitrosodimethylamine ug/kg 10501640 64 45-130
N-Nitrosodiphenylamine ug/kg 14701640 89 56-130
Naphthalene ug/kg 11701640 71 56-130
Nitrobenzene ug/kg 11701640 71 50-130
Pentachlorophenol ug/kg 31503290 96 33-130
Phenanthrene ug/kg 14601640 89 60-130
Phenol ug/kg 12601640 76 54-130
Pyrene ug/kg 15401640 94 61-130
Pyridine ug/kg 8701640 53 35-130
2,4,6-Tribromophenol (S)%91 18-130
2-Fluorobiphenyl (S)%70 19-130
2-Fluorophenol (S)%66 18-130
Nitrobenzene-d5 (S)%67 21-130
Phenol-d6 (S)%68 18-130
Terphenyl-d14 (S)%87 15-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3717982MATRIX SPIKE SAMPLE:
MSSpike
Result
92615898001
1,2,4-Trichlorobenzene ug/kg 16002210 73 22-130ND
1,2-Dichlorobenzene ug/kg 15402210 70 23-130ND
1,3-Dichlorobenzene ug/kg 15402210 70 26-130ND
1,4-Dichlorobenzene ug/kg 15202210 69 27-130ND
1-Methylnaphthalene ug/kg 16302210 74 30-130ND
2,2'-Oxybis(1-chloropropane)ug/kg 15602210 70 30-130ND
2,4,5-Trichlorophenol ug/kg 16502210 75 26-130ND
2,4,6-Trichlorophenol ug/kg 17902210 81 23-130ND
2,4-Dichlorophenol ug/kg 16702210 76 29-130ND
2,4-Dimethylphenol ug/kg 15402210 70 13-130ND
2,4-Dinitrophenol ug/kg 944011000 85 10-131ND
2,4-Dinitrotoluene ug/kg 17202210 78 28-130ND
2,6-Dinitrotoluene ug/kg 18402210 83 36-130ND
2-Chloronaphthalene ug/kg 17202210 78 27-130ND
2-Chlorophenol ug/kg 16602210 75 29-130ND
2-Methylnaphthalene ug/kg 16002210 72 29-130ND
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616378
MBS.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3717982MATRIX SPIKE SAMPLE:
MSSpike
Result
92615898001
2-Methylphenol(o-Cresol)ug/kg 14502210 66 20-130ND
2-Nitroaniline ug/kg 33404410 76 29-130ND
2-Nitrophenol ug/kg 19002210 86 26-130ND
3&4-Methylphenol(m&p Cresol)ug/kg 14402210 65 10-176ND
3,3'-Dichlorobenzidine ug/kg 32604410 74 15-130ND
3-Nitroaniline ug/kg 33404410 76 28-130ND
4,6-Dinitro-2-methylphenol ug/kg 41704410 94 15-132ND
4-Bromophenylphenyl ether ug/kg 18502210 84 35-130ND
4-Chloro-3-methylphenol ug/kg 32804410 74 30-130ND
4-Chloroaniline ug/kg 31104410 70 28-130ND
4-Chlorophenylphenyl ether ug/kg 15902210 72 32-130ND
4-Nitroaniline ug/kg 31504410 71 30-130ND
4-Nitrophenol ug/kg 814011000 74 17-130ND
Acenaphthene ug/kg 17502210 79 29-130ND
Acenaphthylene ug/kg 18802210 85 31-130ND
Aniline ug/kg 7882210 36 10-130ND
Anthracene ug/kg 16902210 76 33-130ND
Benzo(a)anthracene ug/kg 19002210 86 32-130ND
Benzo(a)pyrene ug/kg 23202210 105 32-130ND
Benzo(b)fluoranthene ug/kg 22102210 100 33-130ND
Benzo(g,h,i)perylene ug/kg 19202210 87 28-130ND
Benzo(k)fluoranthene ug/kg 21402210 97 31-130ND
Benzoic Acid ug/kg 357011000 32 10-130ND
Benzyl alcohol ug/kg 31404410 71 31-130ND
bis(2-Chloroethoxy)methane ug/kg 15702210 71 30-130ND
bis(2-Chloroethyl) ether ug/kg 15202210 69 68-130ND
bis(2-Ethylhexyl)phthalate ug/kg 2030 v122109240-130ND
Butylbenzylphthalate ug/kg 19802210 90 40-130ND
Chrysene ug/kg 18402210 83 30-130ND
Di-n-butylphthalate ug/kg 17602210 80 41-130ND
Di-n-octylphthalate ug/kg 2010 v122109142-130ND
Dibenz(a,h)anthracene ug/kg 19502210 88 27-130ND
Dibenzofuran ug/kg 17202210 78 32-130ND
Diethylphthalate ug/kg 16302210 74 40-130ND
Dimethylphthalate ug/kg 16402210 74 37-130ND
Fluoranthene ug/kg 16702210 76 26-130ND
Fluorene ug/kg 16502210 75 31-130ND
Hexachloro-1,3-butadiene ug/kg 14002210 63 20-130ND
Hexachlorobenzene ug/kg 17402210 79 29-130ND
Hexachlorocyclopentadiene ug/kg 17402210 79 10-130ND
Hexachloroethane ug/kg 14902210 67 21-130ND
Indeno(1,2,3-cd)pyrene ug/kg 19102210 87 28-130ND
Isophorone ug/kg 14902210 68 32-130ND
N-Nitroso-di-n-propylamine ug/kg 14202210 64 31-130ND
N-Nitrosodimethylamine ug/kg 14602210 66 20-130ND
N-Nitrosodiphenylamine ug/kg 18502210 84 32-130ND
Naphthalene ug/kg 16602210 75 30-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
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Huntersville, NC 28078
[phone]
Page 109 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616378
MBS.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3717982MATRIX SPIKE SAMPLE:
MSSpike
Result
92615898001
Nitrobenzene ug/kg 16502210 75 25-130ND
Pentachlorophenol ug/kg 38204410 87 10-130ND
Phenanthrene ug/kg 18002210 82 34-130ND
Phenol ug/kg 16502210 75 14-130ND
Pyrene ug/kg 20602210 93 31-130ND
Pyridine ug/kg 215J2210 10 10-130ND
2,4,6-Tribromophenol (S)%83 18-130
2-Fluorobiphenyl (S)%74 19-130
2-Fluorophenol (S)%71 18-130
Nitrobenzene-d5 (S)%74 21-130
Phenol-d6 (S)%73 18-130
Terphenyl-d14 (S)%89 15-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92615898002
3717983SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
1-Methylnaphthalene ug/kg ND 30ND
2,2'-Oxybis(1-chloropropane)ug/kg ND 30ND
2,4,5-Trichlorophenol ug/kg ND 30ND
2,4,6-Trichlorophenol ug/kg ND 30ND
2,4-Dichlorophenol ug/kg ND 30ND
2,4-Dimethylphenol ug/kg ND 30ND
2,4-Dinitrophenol ug/kg ND 30ND
2,4-Dinitrotoluene ug/kg ND 30ND
2,6-Dinitrotoluene ug/kg ND 30ND
2-Chloronaphthalene ug/kg ND 30ND
2-Chlorophenol ug/kg ND 30ND
2-Methylnaphthalene ug/kg ND 30ND
2-Methylphenol(o-Cresol)ug/kg ND 30ND
2-Nitroaniline ug/kg ND 30ND
2-Nitrophenol ug/kg ND 30ND
3&4-Methylphenol(m&p Cresol)ug/kg ND 30ND
3,3'-Dichlorobenzidine ug/kg ND 30ND
3-Nitroaniline ug/kg ND 30ND
4,6-Dinitro-2-methylphenol ug/kg ND 30ND
4-Bromophenylphenyl ether ug/kg ND 30ND
4-Chloro-3-methylphenol ug/kg ND 30ND
4-Chloroaniline ug/kg ND 30ND
4-Chlorophenylphenyl ether ug/kg ND 30ND
4-Nitroaniline ug/kg ND 30ND
4-Nitrophenol ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
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Page 110 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616378
MBS.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92615898002
3717983SAMPLE DUPLICATE:
Acenaphthene ug/kg ND 30ND
Acenaphthylene ug/kg ND 30ND
Aniline ug/kg ND 30ND
Anthracene ug/kg ND 30ND
Benzo(a)anthracene ug/kg ND 30ND
Benzo(a)pyrene ug/kg ND 30ND
Benzo(b)fluoranthene ug/kg ND 30ND
Benzo(g,h,i)perylene ug/kg ND 30ND
Benzo(k)fluoranthene ug/kg ND 30ND
Benzoic Acid ug/kg ND 30ND
Benzyl alcohol ug/kg ND 30ND
bis(2-Chloroethoxy)methane ug/kg ND 30ND
bis(2-Chloroethyl) ether ug/kg ND 30ND
bis(2-Ethylhexyl)phthalate ug/kg ND v130ND
Butylbenzylphthalate ug/kg ND 30ND
Chrysene ug/kg ND 30ND
Di-n-butylphthalate ug/kg ND 30ND
Di-n-octylphthalate ug/kg ND v130ND
Dibenz(a,h)anthracene ug/kg ND 30ND
Dibenzofuran ug/kg ND 30ND
Diethylphthalate ug/kg ND 30ND
Dimethylphthalate ug/kg ND 30ND
Fluoranthene ug/kg ND 30ND
Fluorene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Hexachlorobenzene ug/kg ND 30ND
Hexachlorocyclopentadiene ug/kg ND 30ND
Hexachloroethane ug/kg ND 30ND
Indeno(1,2,3-cd)pyrene ug/kg ND 30ND
Isophorone ug/kg ND 30ND
N-Nitroso-di-n-propylamine ug/kg ND 30ND
N-Nitrosodimethylamine ug/kg ND 30ND
N-Nitrosodiphenylamine ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
Nitrobenzene ug/kg ND 30ND
Pentachlorophenol ug/kg ND 30ND
Phenanthrene ug/kg ND 30ND
Phenol ug/kg ND 30ND
Pyrene ug/kg ND 30ND
Pyridine ug/kg ND 30ND
2,4,6-Tribromophenol (S)%6368
2-Fluorobiphenyl (S)%5870
2-Fluorophenol (S)%5161
Nitrobenzene-d5 (S)%6172
Phenol-d6 (S)%5970
Terphenyl-d14 (S)%8188
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 111 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616378
MBS.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
712674
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92616378001, 92616378002, 92616378003, 92616378004, 92616378005, 92616378006
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92616220001
3716008SAMPLE DUPLICATE:
Percent Moisture %12.7 N222512.9
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92616378006
3716009SAMPLE DUPLICATE:
Percent Moisture %16.4 N222516.7
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 112 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616378
MBS.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
712675
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92616378007, 92616378008, 92616378009, 92616378010, 92616378011, 92616378012, 92616378013,
92616378014, 92616378015, 92616378016, 92616378017, 92616378018, 92616378019, 92616378020,
92616378021, 92616378022, 92616378023, 92616378024, 92616378025, 92616378026
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92616378007
3716025SAMPLE DUPLICATE:
Percent Moisture %21.2 N252520.1
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92616378026
3716026SAMPLE DUPLICATE:
Percent Moisture %14.9 N222515.2
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 113 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616378
MBS.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
712690
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92616378027
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92615341001
3716161SAMPLE DUPLICATE:
Percent Moisture %20.2 N262521.4
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92616356001
3716162SAMPLE DUPLICATE:
Percent Moisture %77.3 N202577.5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 114 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616378
MBS.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1904154
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92616378016, 92616378017, 92616378018, 92616378019, 92616378020, 92616378021, 92616378022,
92616378023, 92616378024, 92616378025
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3822497-1
Associated Lab Samples:92616378016, 92616378017, 92616378018, 92616378019, 92616378020, 92616378021, 92616378022,
92616378023, 92616378024, 92616378025
Matrix:Solid
AnalyzedMDL
Total Solids %ND 08/03/22 11:06
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3822497-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92616378023
R3822497-3SAMPLE DUPLICATE:
Total Solids %72.4 0.552 1072.0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 115 of 125
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92616378
MBS.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1904155
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92616378026, 92616378027
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3822671-1
Associated Lab Samples:92616378026, 92616378027
Matrix:Solid
AnalyzedMDL
Total Solids %0.00100 08/03/22 12:53
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3822671-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1519968-15
R3822671-3SAMPLE DUPLICATE:
Total Solids %90.2 2.27 1092.2
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
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Page 116 of 125
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92616378
MBS.001
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
WORKORDER QUALIFIERS
WO: 92616378
[1]
SAMPLE QUALIFIERS
Sample: 92616378018
TPH by Method MADEPE - Duplicate Analysis performed due to QC failure. Results confirm; reporting in hold data[1]
Sample: 92616378025
TPH by Method MADEPE - Duplicate Analysis performed due to QC failure. Results don't confirm; both analyses reported[1]
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.B
Analyte is a possible laboratory contaminant (not present in method blank).C7
Analysis conducted outside the recognized method holding time.H1
This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.IH
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
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Page 117 of 125
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92616378
MBS.001
ANALYTE QUALIFIERS
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.IK
Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.J
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike recovery and/or matrix spike duplicate recovery was above laboratory control limits. Result may be biased
high.MH
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
Matrix spike recovery was outside laboratory control limits due to a parent sample concentration notably higher than the
spike level.P6
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 118 of 125
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92616378
MBS.001
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92616378016 1904880 1904880EXC-BASE-1 MA DEP/NJ DEP MADEP EPH
92616378017 1904880 1904880EXC-BASE-2 MA DEP/NJ DEP MADEP EPH
92616378018 1904880 1904880EXC-BASE-3 MA DEP/NJ DEP MADEP EPH
92616378019 1904880 1904880EXC-BASE-4 MA DEP/NJ DEP MADEP EPH
92616378020 1904880 1904880EXC-SIDE-1 MA DEP/NJ DEP MADEP EPH
92616378021 1904880 1904880EXC-SIDE-2 MA DEP/NJ DEP MADEP EPH
92616378022 1904880 1904880EXC-SIDE-3 MA DEP/NJ DEP MADEP EPH
92616378023 1904880 1904880PL-BASE (12)MA DEP/NJ DEP MADEP EPH
92616378024 1904880 1904880PL-N (12)MA DEP/NJ DEP MADEP EPH
92616378025 1904880 1904880PL-S (12)MA DEP/NJ DEP MADEP EPH
92616378025 1907676 1907676PL-S (12)MA DEP/NJ DEP MADEP EPH
92616378026 1904880 1904880PL-E (12)MA DEP/NJ DEP MADEP EPH
92616378027 1904880 1904880PL-W (12)MA DEP/NJ DEP MADEP EPH
92616378001 713049 713206PL-1 (1-1.5)EPA 3546 EPA 8015C
92616378002 713049 713206PL-2 (1-1.5)EPA 3546 EPA 8015C
92616378003 713049 713206PL-3 (1-1.5)EPA 3546 EPA 8015C
92616378004 713049 713206T-1 (15)EPA 3546 EPA 8015C
92616378005 713049 713206T-2 (15)EPA 3546 EPA 8015C
92616378006 713049 713206T-3 (15)EPA 3546 EPA 8015C
92616378007 713049 713206T-4 (15)EPA 3546 EPA 8015C
92616378008 713049 713206T-5 (15)EPA 3546 EPA 8015C
92616378009 713049 713206T-6 (15)EPA 3546 EPA 8015C
92616378010 713049 713206T-7 (15)EPA 3546 EPA 8015C
92616378011 713049 713206T-8 (15)EPA 3546 EPA 8015C
92616378012 713049 713206T-9 (15)EPA 3546 EPA 8015C
92616378013 713049 713206T-10 (15)EPA 3546 EPA 8015C
92616378014 713049 713206T-11 (15)EPA 3546 EPA 8015C
92616378015 713049 713206T-12 (15)EPA 3546 EPA 8015C
92616378001 712637 712652PL-1 (1-1.5)EPA 5030B EPA 8015C
92616378002 712637 712652PL-2 (1-1.5)EPA 5030B EPA 8015C
92616378003 712637 712652PL-3 (1-1.5)EPA 5030B EPA 8015C
92616378004 712637 712652T-1 (15)EPA 5030B EPA 8015C
92616378005 712637 712652T-2 (15)EPA 5030B EPA 8015C
92616378006 712637 712652T-3 (15)EPA 5030B EPA 8015C
92616378007 712637 712652T-4 (15)EPA 5030B EPA 8015C
92616378008 712637 712652T-5 (15)EPA 5030B EPA 8015C
92616378009 712637 712652T-6 (15)EPA 5030B EPA 8015C
92616378010 712637 712652T-7 (15)EPA 5030B EPA 8015C
92616378011 712637 712652T-8 (15)EPA 5030B EPA 8015C
92616378012 712637 712652T-9 (15)EPA 5030B EPA 8015C
92616378013 712637 712652T-10 (15)EPA 5030B EPA 8015C
92616378014 712637 712652T-11 (15)EPA 5030B EPA 8015C
92616378015 713150 713236T-12 (15)EPA 5030B EPA 8015C
92616378016 712441 712448EXC-BASE-1 MADEP VPH MADEP VPH
92616378017 712441 712448EXC-BASE-2 MADEP VPH MADEP VPH
92616378018 712441 712448EXC-BASE-3 MADEP VPH MADEP VPH
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 119 of 125
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92616378
MBS.001
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92616378019 712441 712448EXC-BASE-4 MADEP VPH MADEP VPH
92616378020 712441 712448EXC-SIDE-1 MADEP VPH MADEP VPH
92616378021 712441 712448EXC-SIDE-2 MADEP VPH MADEP VPH
92616378022 712441 712448EXC-SIDE-3 MADEP VPH MADEP VPH
92616378023 712441 712448PL-BASE (12)MADEP VPH MADEP VPH
92616378024 712441 712448PL-N (12)MADEP VPH MADEP VPH
92616378025 712441 712448PL-S (12)MADEP VPH MADEP VPH
92616378026 712441 712448PL-E (12)MADEP VPH MADEP VPH
92616378027 712441 712448PL-W (12)MADEP VPH MADEP VPH
92616378016 713046 713165EXC-BASE-1 EPA 3546 EPA 8270E
92616378017 713046 713165EXC-BASE-2 EPA 3546 EPA 8270E
92616378018 713046 713165EXC-BASE-3 EPA 3546 EPA 8270E
92616378019 713046 713165EXC-BASE-4 EPA 3546 EPA 8270E
92616378020 713046 713165EXC-SIDE-1 EPA 3546 EPA 8270E
92616378021 713046 713165EXC-SIDE-2 EPA 3546 EPA 8270E
92616378022 713046 713165EXC-SIDE-3 EPA 3546 EPA 8270E
92616378023 713046 713165PL-BASE (12)EPA 3546 EPA 8270E
92616378024 713046 713165PL-N (12)EPA 3546 EPA 8270E
92616378025 713046 713165PL-S (12)EPA 3546 EPA 8270E
92616378026 713046 713165PL-E (12)EPA 3546 EPA 8270E
92616378027 713046 713165PL-W (12)EPA 3546 EPA 8270E
92616378016 712702 712875EXC-BASE-1 EPA 5035A/5030B EPA 8260D
92616378017 712702 712875EXC-BASE-2 EPA 5035A/5030B EPA 8260D
92616378018 712702 712875EXC-BASE-3 EPA 5035A/5030B EPA 8260D
92616378019 712702 712875EXC-BASE-4 EPA 5035A/5030B EPA 8260D
92616378020 712702 712875EXC-SIDE-1 EPA 5035A/5030B EPA 8260D
92616378021 712764 712877EXC-SIDE-2 EPA 5035A/5030B EPA 8260D
92616378022 712764 712877EXC-SIDE-3 EPA 5035A/5030B EPA 8260D
92616378023 712764 712877PL-BASE (12)EPA 5035A/5030B EPA 8260D
92616378024 712764 712877PL-N (12)EPA 5035A/5030B EPA 8260D
92616378025 712764 712877PL-S (12)EPA 5035A/5030B EPA 8260D
92616378026 712764 712877PL-E (12)EPA 5035A/5030B EPA 8260D
92616378027 712764 712877PL-W (12)EPA 5035A/5030B EPA 8260D
92616378001 712674PL-1 (1-1.5)SW-846
92616378002 712674PL-2 (1-1.5)SW-846
92616378003 712674PL-3 (1-1.5)SW-846
92616378004 712674T-1 (15)SW-846
92616378005 712674T-2 (15)SW-846
92616378006 712674T-3 (15)SW-846
92616378007 712675T-4 (15)SW-846
92616378008 712675T-5 (15)SW-846
92616378009 712675T-6 (15)SW-846
92616378010 712675T-7 (15)SW-846
92616378011 712675T-8 (15)SW-846
92616378012 712675T-9 (15)SW-846
92616378013 712675T-10 (15)SW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 120 of 125
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92616378
MBS.001
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92616378014 712675T-11 (15)SW-846
92616378015 712675T-12 (15)SW-846
92616378016 712675EXC-BASE-1 SW-846
92616378017 712675EXC-BASE-2 SW-846
92616378018 712675EXC-BASE-3 SW-846
92616378019 712675EXC-BASE-4 SW-846
92616378020 712675EXC-SIDE-1 SW-846
92616378021 712675EXC-SIDE-2 SW-846
92616378022 712675EXC-SIDE-3 SW-846
92616378023 712675PL-BASE (12)SW-846
92616378024 712675PL-N (12)SW-846
92616378025 712675PL-S (12)SW-846
92616378026 712675PL-E (12)SW-846
92616378027 712690PL-W (12)SW-846
92616378016 1904154 1904154EXC-BASE-1 SM 2540 G SM 2540G
92616378017 1904154 1904154EXC-BASE-2 SM 2540 G SM 2540G
92616378018 1904154 1904154EXC-BASE-3 SM 2540 G SM 2540G
92616378019 1904154 1904154EXC-BASE-4 SM 2540 G SM 2540G
92616378020 1904154 1904154EXC-SIDE-1 SM 2540 G SM 2540G
92616378021 1904154 1904154EXC-SIDE-2 SM 2540 G SM 2540G
92616378022 1904154 1904154EXC-SIDE-3 SM 2540 G SM 2540G
92616378023 1904154 1904154PL-BASE (12)SM 2540 G SM 2540G
92616378024 1904154 1904154PL-N (12)SM 2540 G SM 2540G
92616378025 1904154 1904154PL-S (12)SM 2540 G SM 2540G
92616378026 1904155 1904155PL-E (12)SM 2540 G SM 2540G
92616378027 1904155 1904155PL-W (12)SM 2540 G SM 2540G
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/10/2022 03:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 121 of 125
Page 122 of 125
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