WS-10181_45313_CA_LSA_20210215

PHASE I LIMITED SITE ASSESSMENT REPORT
WEST 70 CURB MARKET SITE
110 WOODLAWN ROAD
MEBANE, ALAMANCE COUNTY, NORTH CAROLINA
INCIDENT NO. 45313
FACILITY ID No. 00-0-000023230
Prepared For:
Mr. Michael Tompkins
McLeod Oil Company, Inc.
P.O. Box 100
Mebane, North Carolina 27302
Prepared By:
Progress Environmental Group, Inc.
P.O. Box 5884
Winston-Salem, North Carolina 27113
Progress Project No. 1021014.001
February 9, 2021
P.O. Box 5884
Winston-Salem, North Carolina 27113
p. 336.722.9999 f. 336.722.9998
www.progressenvironmental.com
February 9, 2021
Ms. Karen J. Hall
North Carolina Department of Environmental Quality
UST Section
450 West Hanes Mill Road, Suite 300
Winston-Salem, North Carolina 27105
Subject: Phase I Limited Site Assessment Report
West 70 Curb Market Site
110 Woodlawn Road
Mebane, Alamance County, North Carolina
Progress Project No. 1021014.001
Incident No. 45313
Dear Ms. Hall:
On behalf of McLeod Oil Company, Inc., Progress Environmental Group, Inc. (Progress) is submitting
this Phase I Limited Site Assessment Report for the subject site. Included in this report is a description
of the field activities, the results obtained, and our conclusions and recommendations.
This Phase I Limited Site Assessment Report has been prepared in general accordance with the
Underground Storage Tank Limited Site Assessment guidelines presented in the NCDEQ Guidelines
for Assessment and Corrective Action dated January 19, 2021.
We appreciate your consideration and cooperation in the submission of this report. If you have any
questions concerning this report please feel free to contact us at [phone].
Sincerely,
PROGRESS ENVIRONMENTAL GROUP, INC.
Joseph S. Lawson III Jeffrey A. Ballsieper
Director of Ecological Services Director of Environmental Services
Licensed NC 1653
Attachments
cc: Mr. Michael Tompkins, McLeod Oil Company, Inc.
P.O. Box 5884
Winston-Salem, North Carolina 27113
p. 336.722.9999 f. 336.722.9998
www.progressenvironmental.com
February 6, 2021
Mr. Michael Tompkins
McLeod Oil Company, Inc.
P.O. Box 100
Mebane, North Carolina 27302
Subject: Phase I Limited Site Assessment Report
West 70 Curb Market Site
110 Woodlawn Road
Mebane, Alamance County, North Carolina
Progress Project No. 1021014.001
Incident N0. 45313
Dear Mr. Tompkins:
Progress Environmental Group, Inc. (Progress) is pleased to submit this Phase I Limited Site
Assessment Report for the West 70 Curb Market Site in Mebane, North Carolina. The objective of the
assessment was to assess the potential risks to human health and the environment, and recommend
whether additional assessment may be necessary at the site.
This report is intended for the use of McLeod Oil Company, Inc., only. The contents should not be
relied upon by other parties without the express written consent of Progress. The findings are relevant
to the dates of our site work and should not be relied upon to represent site conditions on other dates.
Progress appreciates the opportunity to provide our environmental services. If you have any questions
or if we may be of further service, please contact the undersigned at [phone].
Sincerely,
PROGRESS ENVIRONMENTAL GROUP, INC.
Joseph S. Lawson III Jeffrey A. Ballsieper
Director of Ecological Services Director of Environmental Services
Licensed NC 1653
Attachment: Phase I Limited Site Assessment Report and Appendices
Phase I Limited Site Assessment
West 70 Curb Market Site
110 Woodlawn Road
Mebane, North Carolina
Progress Project No. 1021014.001
February 6, 2021
i
TABLE OF CONTENTS
A SITE IDENTIFICATION ....................................................................................................................... 1
B SITE HISTORY AND CHARACTERIZATION .................................................................................. 2
C RISK CHARACTERIZATION .............................................................................................................. 3
1 GROUNDWATER/SURFACE WATER/VAPOR IMPACTS .............................................................................. 3
2 LAND USE ............................................................................................................................................... 4
D RECEPTOR INFORMATION ............................................................................................................... 5
1 WATER-SUPPLY WELLS .......................................................................................................................... 5
2 PUBLIC WATER SUPPLIES ....................................................................................................................... 6
3 SURFACE WATER .................................................................................................................................... 6
4 WELLHEAD PROTECTION AREAS ........................................................................................................... 6
5 DEEP AQUIFERS IN THE COASTAL PLAIN PHYSIOGRAPHIC REGION ........................................................ 6
6 SUBSURFACE STRUCTURES ..................................................................................................................... 6
7 PROPERTY OWNERS AND OCCUPANTS .................................................................................................... 7
E SITE GEOLOGY AND HYDROGEOLOGY ....................................................................................... 7
F SAMPLING RESULTS ........................................................................................................................... 7
1 SOIL ........................................................................................................................................................ 7
2 GROUNDWATER ...................................................................................................................................... 8
G CONCLUSIONS AND RECOMMENDATIONS ................................................................................. 8
H FREE PRODUCT INVESTIGATION/RECOVERY ........................................................................... 9
I REFERENCES ......................................................................................................................................... 9
FIGURES
Figure 1 – Topographic Site Map
Figure 2 – Site Map
Figure 3 – Surrounding Property Owners Map
Figure 4 – Water-Supply Well Location Map
Figure 5 – Zoning Map
TABLES
Table B-1 – Site History, UST/AST System Information
Table B-2 – Site History, UST Owner/Operator Information
Table B-4 – Summary of Detected Groundwater Analytical Results
Table B-5 – Water Supply Well Information
Table B-6 – Surrounding Property Owners
Table B-7 – Well Construction Information
APPENDICES
Appendix A – Standard Sampling Procedures
Appendix B – Sampling Sheet/Boring Log/Well Construction Record
Appendix C – Returned Water-Supply Questionnaires
Appendix D – Laboratory Test Reports and Chains-of-Custody
Phase I Limited Site Assessment
West 70 Curb Market Site
110 Woodlawn Road
Mebane, North Carolina
Progress Project No. 1021014.001
February 9, 2021
1
Phase I Limited Site Assessment Report
A SITE IDENTIFICATION
Date of Report: February 9, 2021
Facility I.D.: 00-0-0000023230
UST Incident Number (if known): 45313
Site Name: West 70 Curb Market Site
Site Location: 110 Woodlawn Road, Mebane, North Carolina 27302
Nearest City/Town: Mebane, North Carolina County: Alamance
UST Owner/Operator: McLeod Oil Company, Inc.
Address: P.O. Box 100, Mebane, North Carolina 27302 Phone: [phone]
Property Owner: McLeod Oil Company, Inc.
Address: P.O. Box 100, Mebane, North Carolina 27302 Phone: [phone]
Property Occupant: Unoccupied
Address: P.O. Box 100, Mebane, North Carolina 27302 Phone: [phone]
Consultant/Contractor: Progress Environmental Group, Inc.
Address: P.O. Box 5884, Winston-Salem, North Carolina 27113 Phone: [phone]
Attention: Mr. Jeffrey A. Ballsieper, L.G.
Analytical Laboratory: Pace Analytical Laboratories, LLC
Address: 9800 Kincey Avenue, Huntersville, North Carolina 27284 Phone: [phone]
Release Information
Date Discovered: August 23, 2019
Latitude: N 36.098609 Longitude: W 79.283000
Estimated Quantity of Release: Unknown
Cause of Release: Unknown
Source of Release (e.g., Piping/UST): Gasoline USTs
Sizes and contents of UST system(s) from which the release occurred): One 4,000-gallon gasoline UST and one
1,000-gallon gasoline UST (Table B-1).
Risk Classification: Undetermined
Land Use Category: Industrial/Commercial
I, Jeffrey A. Ballsieper, a Licensed Geologist for Progress Environmental Group, Inc., do certify that the
information contained in this report is correct and accurate to the best of my knowledge.
_____________________________________
Jeffrey A. Ballsieper, L.G.
Director of Environmental Services
Progress Environmental Group, Inc. is licensed to practice geology in North Carolina. The certification
number of the corporation is C-552.
Phase I Limited Site Assessment
West 70 Curb Market Site
110 Woodlawn Road
Mebane, North Carolina
Progress Project No. 1021014.001
February 9, 2021
2
B SITE HISTORY AND CHARACTERIZATION
Progress Environmental Group, Inc. (Progress) was contracted by McLeod Oil Company, Inc. to
conduct underground storage tank (UST) closure activities at the West 70 Curb Market located at
110 Woodlawn Road in Mebane, Alamance County, North Carolina (Figure 1). The site consists of
a former convenience store which stored petroleum products in USTs for retail sale. At the time of
the removal the site was undergoing remodeling, and the USTs had not been used to store petroleum
product since 2005. The site is located in a mixed use area of Mebane, including commercial,
residential, and industrial uses.It is likely that the surrounding properties are served by the Town of
Mebane municipal water-supply system. The closure activities included the removal of one 1,000-
gallon gasoline UST and one 4,000-gallon gasoline UST and associated piping. Information
regarding the on-site USTs is presented below:
Table B-1
Site History, UST/AST System Information
Tank
No.
Installation
Date
Capacity
(gallons)
Construction
Materials
Dimensions
(inches)
Removal
Date
Previous
Contents
1 Unknown 1,000 Steel 46” x 144” 8/8/19 Gasoline
2 Unknown 4,000 Steel 64” x 285” 8/8/19 Gasoline
Table B-2
Site History, UST Owner/Operator Information
Owner’s Name Address Phone Number Dates of
Ownership
McLeod Oil Company, Inc. P.O. Box 100,
Mebane, NC 27302 [phone] 1974-2019
Based on the results of the initial abatement activities, Progress concluded the following:
Progress supervised the removal of one 1,000-gallon gasoline UST and one 4,000-gallon UST, and
associated fuel dispensing lines from the subject site.
Progress collected a total of five soil samples beneath the gasoline USTs (S-1 through S-5).
Laboratory analysis of soil samples S-3 (23,500 mg/Kg) and S-4 (3,720 mg/Kg) collected beneath
the USTs indicated Total Petroleum Hydrocarbons as Gasoline (TPH-G) concentrations in excess
of the North Carolina Action Level.
Progress collected a total of two soil samples beneath the dispensers (S-6 and S-7). Laboratory
analysis of soil sample S-6 (1,720 mg/Kg) collected from beneath the northernmost dispenser
indicated TPH-G concentrations in excess of the North Carolina Action Level.
Progress collected one soil sample beneath the fuel distribution lines (S-8). Laboratory analysis of
soil sample S-8 (2,740 mg/Kg) collected from beneath the fuel distribution lines indicated TPH-G
concentrations in excess of the North Carolina Action Level.
Based on the presence of notably contaminated soil, Progress supervised the over-excavation of
contaminated soil beneath the USTs. Soil samples were screened using Redlabs mobile laboratory
to complete the guided excavation. Approximately 484.07 tons of petroleum-impacted soil were
excavated from the site and transported to an off-site permitted disposal facility.
Phase I Limited Site Assessment
West 70 Curb Market Site
110 Woodlawn Road
Mebane, North Carolina
Progress Project No. 1021014.001
February 9, 2021
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Following the over-excavation of the contaminated soil, Progress screened the soil samples from
the sidewalls of the excavation via Redlabs mobile laboratory. Each of the soil samples selected
for laboratory analysis did not exhibit TPH as gasoline at concentrations exceeding the North
Carolina Action Level when analyzed using the UVF Method. Progress collected confirmation
soil samples from the sidewalls and base of the over-excavation. Prior to collecting the soil samples
laboratory analysis of soil samples SW-1 and SW-6 collected from the sidewalls of the over-
excavation did not detect targeted compounds above their respective Soil-to-Groundwater
Maximum Soil Contaminant Concentrations (MSCCs) or Residential Soil Cleanup Levels.
Laboratory analysis of soil samples SW-2 through SW-5 and SW-7 through SW-12 collected from
the sidewalls and soil samples B-1 through B-4 collected from the base of the over-excavation
detected at least one targeted compound above its respective Soil-to-Groundwater MSCC. C9-C10
Aromatics were detected in soil sample B-3 at a concentration that exceeds its Residential Soil
Cleanup Level.
C RISK CHARACTERIZATION
1 Groundwater/Surface Water/Vapor Impacts
High Risk
1. Has the release contaminated any water-supply well including any well used for non-
drinking purposes? UNKNOWN
2.Is a water-supply well used for drinking water located within 1,500 feet of the source area
of the discharge or release? NO
3.Is a water-supply well not used for drinking water (e.g. irrigation, washing cars, industrial
cooling water, filling swimming pools) located within 250 feet of the source area of the
release? NO
4. Does groundwater within 500 feet of the source area of the release have the potential for
future use (there is no other source of water supply other than groundwater)? NO
Public water is available in the vicinity of the site.
5.Do vapors from the release pose a threat of explosion because of accumulation of the vapors
in a confined space or pose any other serious threat to public health, public safety, or the
environment? UNKNOWN
6.Are there any other factors that would cause the release to pose an imminent danger to public
health, public safety, or the environment? NO
Intermediate Risk
7.Is a surface water body located within 500 feet of the source area of the release? NO
If yes, does the maximum groundwater contaminant concentration exceed the surface water
quality standards and criteria found in 15A NCAC 2B .0200 by a factor of 10?
Phase I Limited Site Assessment
West 70 Curb Market Site
110 Woodlawn Road
Mebane, North Carolina
Progress Project No. 1021014.001
February 9, 2021
4
8. Is the source area or release located within an approved or planned wellhead protection area
as defined in 42 USC 300h-7(e)? NO
9.Is the release located in the Coastal Plain physiographic region as designated on a map
entitled “Geology of North Carolina” published by the Department in 1985? NO
10.Do the levels of groundwater contamination for any contaminants exceed the gross
contaminant levels (GCL) (see Table 9 of the New Guidelines) established by the
Department? NO
2 Land Use
Property Containing Source Area of Release
The questions below pertain to the property containing the source area of the release.
1. Does the property contain one or more primary or secondary residences (permanent or
temporary)? NO
Describe. The property is developed with a two story building that is currently unoccupied
(Figure 2).
2. Does the property contain a school, daycare center, hospital, playground, park, recreation
area, church, nursing home, or other place of public assembly? NO
Describe. The property is developed with a two story building that is currently unoccupied.
3. Does the property contain a commercial (e.g., retail, warehouse, office/business space, etc.)
or industrial (e.g., manufacturing, utilities, industrial research and development,
chemical/petroleum bulk storage, etc.) enterprise, an inactive commercial or industrial
enterprise, or is the land undeveloped? YES
Describe. The property is developed with a two story commercial building that is currently
unoccupied.
4.Do children visit the property? NO
Explain. The property is developed with a two story building that is currently unoccupied
therefore, Progress would not expect children to visit the property regularly.
4.Is access to the property reliably restricted consistent with its use (e.g., fences, security
personnel or both)? NO
Explain. Access restrictions are not deemed necessary.
5.Do pavement, buildings, or other structures cap the contaminated soil? NO
If yes, explain what mechanisms are in place or can be put into place to ensure that the
contaminated soil will remain capped in the foreseeable future.
Phase I Limited Site Assessment
West 70 Curb Market Site
110 Woodlawn Road
Mebane, North Carolina
Progress Project No. 1021014.001
February 9, 2021
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The contaminated soil is beneath an area that was uncovered during the UST closure activities.
The disturbed area was formerly covered in asphalt pavement.
6. What is the zoning status of the property?
The subject site is zoned General Business (B-2) (Figure 5).
7. Is the use of the property likely to change in the next 20 years? UNKNOWN
Explain. Progress does not have knowledge of future development plans associated with the
site.
Property Surrounding Source Area of Release
The questions below pertain to the area within 1,500 feet of the source area of the release (excludes
property containing source area of the release).
1. What is the distance from the source area of the release to the nearest primary or secondary
residence (permanent or temporary)? The nearest occupied residence is located
approximately 1,040 feet to the north-northwest of the source area.
2. What is the distance from the source area of the release to the nearest school, daycare center,
hospital, playground, park, recreation area, church, nursing home or other place of public
assembly? Progress identified the Mebane United Presbyterian Church located
approximately 1,100 feet south of the site.
3. What is the zoning status of properties in the surrounding area? The surrounding properties
in the area are predominately zoned as General Business (B-2), Residential (R-20), and
Heavy Manufacturing (M-1), and Light Manufacturing (M-2).
5.Briefly characterize the use and activities of the land in the surrounding area.
Land uses in the surrounding areas are commercial and rural residential.
D RECEPTOR INFORMATION
1 Water-Supply Wells
Progress mailed 73 water-supply well questionnaires to the property owners within a 1,000-
foot radius of the site. 17 of the questionnaires have been completed and returned at the time
of this report. Progress also completed a visual reconnaissance within 1,500 feet of the site.
Progress identified evidence of two water-supply wells during the reconnaissance of
accessible properties within 1,000 feet of the site or based on the returned questionnaires.
One well located at 145 Woodlawn Road does not appear to be utilized for drinking and the
property was confirmed to be connected to the Alamance-Orange Water System; however,
a questionnaire was not returned from the owner of this property. A second well identified
Phase I Limited Site Assessment
West 70 Curb Market Site
110 Woodlawn Road
Mebane, North Carolina
Progress Project No. 1021014.001
February 9, 2021
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at 168 Woodlawn Road was confirmed via conversation with the property owner to be used
for irrigation and livestock watering. Each of the identified water-supply wells are located
more than 500 feet from the source area. An additional out of use well was identified more
than 1,000 feet from the source area and, therefore, was not included on Figure 4 or in Table
B-5. Copies of the returned water-supply well questionnaires are included in Appendix D.
Progress understands that public water is available in the vicinity of the site.
2 Public Water Supplies
Are public water supplies available within 1,500 feet of the source are of the release? YES
If yes, where is the location of the nearest public water line and the source(s) of the public
water supply? The public water lines are located within the adjacent rights-of-way. Please
note, properties proximal to the site are provided water by either the City of Mebane or the
Alamance-Orange Water System. The source of drinking water in the City of Mebane is
from the Graham-Mebane Reservoir (surface water supply). The Orange-Alamance Water
System include Corporation Lake, four water-supply wells, and purchased water from the City
of Burlington through the Town of Haw River. Lake Orange provides additional water during
drought conditions. The water-supply wells associated with the Alamance-Orange water
supply do not appear to be located proximal to the site.
3 Surface Water
According to the USGS topographic map, an unnamed pond is located approximately 1,400
feet to the west-northwest of the source area.
4 Wellhead Protection Areas
The source area is not located within an established wellhead protection area according to
the North Carolina Well Head Protection Areas Map
(https://www.arcgis.com/home/webmap/viewer.html?webmap=7492e0fe11874ccca699679
d03bc0751).
5 Deep Aquifers in the Coastal Plain Physiographic Region
The subject site is located in the Piedmont Physiographic Province.
6 Subsurface Structures
Overhead electrical and phone utility lines are located at the subject site. Subsurface water
and septic lines are located at the site. Subsurface utilities (power and communication lines)
were not identified proximal to the UST system.
Phase I Limited Site Assessment
West 70 Curb Market Site
110 Woodlawn Road
Mebane, North Carolina
Progress Project No. 1021014.001
February 9, 2021
7
7 Property Owners and Occupants
MACMOM, LLC. currently owns the subject property. Adjacent properties are developed
as commercial properties or are undeveloped. The names and addresses of the adjacent
property owners are provided in Table B-6.
E SITE GEOLOGY AND HYDROGEOLOGY
According to the Geologic Map of North Carolina (1985), the subject property is situated in
the Carolina Slate Belt of the Piedmont Physiographic Province of North Carolina. The site is
located in an area underlain by intermediate metavolcanic rock characterized by
metamorphosed andesitic tuffs and flows. In the Piedmont Physiographic Province,
groundwater generally occurs under water-table conditions and is stored in the pore space
between individual grains of residual soil and in the fractures within the underlying parent
rock. Due to the intense shearing associated with the thrust faulting in the area, it can be
expected that the fractures play a major role in the flow of groundwater in the subsurface.
Recharge to the water table is primarily by precipitation infiltrating the upper soils and
percolating downward, under the influence of gravity, to the groundwater table. Typically, the
water table is not a level surface, but a subdued reflection of the land surface. However, the
depth to the water table is not constant, and depends on many factors, which include the amount
of rainfall, the permeability of the soil, and the amount of groundwater being pumped in the
area.
Based on our review of the topographic map and on-site observation, the site is located on a
ridge. Groundwater generally flows in directions sub-parallel to the ground surface slopes
and under the influence of gravity toward points of discharge such as creeks, swamps,
drainage swales, or pumped groundwater wells. Based on topographic inference,
groundwater beneath the site most likely flows to the west.
Soil encountered during the UST removal included fine sandy silt. During the advancement
of the soil boring to install the monitoring well, Progress consistently encountered fine sandy
silt beneath the imported fill material (21 feet bls). Bedrock was not encountered during
drilling activities. Groundwater was encountered at an approximate depth of 18 feet bls in
the monitoring well installed on site. Groundwater flow beneath the site appears to be
migrating to the west. An unnamed pond is located approximately 1,400 feet to the west of
the source area (Figure 1).
F SAMPLING RESULTS
1 Soil
Based on the depth to groundwater being identified shallower than the former excavation of
contaminated soil, Progress did not collect a soil sample for laboratory analysis as part of
this assessment.
Phase I Limited Site Assessment
West 70 Curb Market Site
110 Woodlawn Road
Mebane, North Carolina
Progress Project No. 1021014.001
February 9, 2021
8
2 Groundwater
On January 15, 2021 3D Environmental Investigations, LLC installed one, two-inch
monitoring well (MW-1) to an approximate depth of 30 feet bls with 15 feet of 0.01 slotted
Schedule 40 PVC screen using the hollow stem auger drilling method. Following proper
well development and purging, Progress collected a groundwater sample from the
monitoring well using a disposable bailer and new length of cord and transferred to the
laboratory containers into a cooler packed with ice. The groundwater sample collected from
monitoring well MW-1 was analyzed for volatile organic compounds (VOCs) using
Standard Method 6200B, for ethylene dibromide using EPA Method 504.1, for lead using
the Standard Method, and for volatile petroleum hydrocarbons using the Massachusetts
Department of Environmental Protection (MADEP) Method.
Laboratory analysis of the groundwater sample collected from monitoring well MW-1
detected benzene (4,380 µg/L), chloroform (78.5 µg/L), ethylbenzene (1,410 µg/L), di-
isopropyl ether (317 µg/L), methyl tert-butyl ether (18,900 µg/L), toluene (14,300 µg/L),
1,2,4-trimethylbenzene (1,440 µg/L), total xylenes (7,660 µg/L), ethylene dibromide (1.1
µg/L), C5-C8 Aliphatics (57,100 µg/L), C9-C12 Aliphatics (22,000 µg/L), and C9-C10
Aromatics (6,350 µg/L) at concentrations exceeding their respective North Carolina 2L
Groundwater Quality Standards (NC2LGWQS). Please note, none of the detected
concentrations exceed the applicable Gross Contamination Levels (GCLs).
Copies of the laboratory data sheet and chain-of-custody record are included in the Appendix
D. The groundwater sample was collected using the methods described in Appendix A.
G CONCLUSIONS AND RECOMMENDATIONS
Based on the results of the receptor survey and groundwater sampling activities, Progress
makes the following conclusions:
1.The site meets the criteria for a Low Risk site based on the absence of active water-supply
wells being identified within 1,000 feet of the source area. The site is not located within a
wellhead protection area.
2.Based on the depth to groundwater being identified shallower than the former excavation of
contaminated soil, Progress did not collect a soil sample for laboratory analysis as part of
this assessment.
3.Laboratory analysis of the groundwater sample collected from monitoring well MW-1
detected benzene (4,380 µg/L), chloroform (78.5 µg/L), ethylbenzene (1,410 µg/L), di-
isopropyl ether (317 µg/L), methyl tert-butyl ether (18,900 µg/L), toluene (14,300 µg/L),
1,2,4-trimethylbenzene (1,440 µg/L), total xylenes (7,660 µg/L), ethylene dibromide (1.1
µg/L), C5-C8 Aliphatics (57,100 µg/L), C9-C12 Aliphatics (22,000 µg/L), and C9-C10
Aromatics (6,350 µg/L) at concentrations exceeding their respective NC2LGWQS. Please
note, none of the detected concentrations exceed the applicable GCLs.
Phase I Limited Site Assessment
West 70 Curb Market Site
110 Woodlawn Road
Mebane, North Carolina
Progress Project No. 1021014.001
February 9, 2021
9
Progress recommends providing a copy of this report to the Winston-Salem Regional Office
of the NCDEQ, Division of Waste Management, UST Section.
H FREE PRODUCT INVESTIGATION/RECOVERY
Free product was not detected in the monitoring well during the October 2020 sampling
event.
I REFERENCES
North Carolina Department of Natural Resources and Community Development Geologic Map of
North Carolina published 1985.
Underground Storage Tank Section, North Carolina Department of Environment and Natural
Resources, Guidelines for Assessment and Corrective Action for UST Releases, Effective
January 19, 2021.
UST Closure and Initial Abatement Action Report, prepared by Progress Environmental Group, Inc.
and dated October 15, 2019.
FIGURES
Figure 1
Topographic Site Map
West 70 Curb Market
110 Woodlawn Road
Mebane, North Carolina
P.O. Box 5884
Winston-Salem, NC 27113
Telephone: [phone]
Fax: [phone]
www.progressenvironmental.com
Mebane, N.C.
Date: 2019
United States Department of the Interior
United States Geological Survey
7.5 Minute Series Topographic Map
Contour Interval: 10 feet
Approximate Scale: 1:24,000
Project: West 70 Curb Market
Client: McLeod Oil
Progress Job #: 1021014.001
Date: February 2021
Site
UST LOCATION
ESTIMATED PRODUCT LINE LOCATION
SOIL SAMPLING LOCATION
1
2
3
4
5
86
7Former Dispenser
Former Dispenser 4,000-Gallon
Gasoline UST
1,000-Gallon
Gasoline UST
Limits of Excavation
15 ProgressENVIRONMENTAL GROUP, INC.JSLFEB 2021JABAS SHOWNFEB 2021Figure 2.SKFP.O. Box 5884WINSTON-SALEM, NORTH CAROLINA 27113PHONE [phone] FAX [phone]FIGURE 2SITE MAPWEST 70 CURB MARKET110 WOODLAWN ROADMEBANE, NORTH CAROLINAPROJECT1021014.001MW-1
Figure 3
Surrounding Property Owners Map
West 70 Curb Market
110 Woodlawn Road
Mebane, North Carolina
P.O. Box 5884
Winston-Salem, NC 27113
Telephone: [phone]
Fax: [phone]
www.progressenvironmental.com
Mebane, N.C.
Date: 2021
Alamance County GIS
https://apps.alamance-
nc.com/CountyGISMap/default.aspx
Approximate Scale: Not to Scale
Project: West 70 Curb Market
Client: McLeod Oil
Progress Job #: 1021014.001
Date: February 2021
Site
ProgressENVIRONMENTAL GROUP, INC.JSL1021014.001FEB 2021JABAS SHOWNFEB 2021Figure 4.SKFP.O. Box 5884WINSTON-SALEM, NORTH CAROLINA 27113PHONE [phone] FAX [phone]FIGURE 4WATER SUPPLY WELL LOCATION MAPWEST 70 CURB MARKET110 WOODLAWN ROADMEBANE, NORTH CAROLINAPROJECTWS-2 Approximate location of water-supply well not active
WS-1
WS-2
Approximate location of water-supply well not used for drinkingWS-1
Location of an area of public assembly
Figure 5
Zoning Map
West 70 Curb Market
110 Woodlawn Road
Mebane, North Carolina
B-2 R-20 M-1 M-2
P.O. Box 5884
Winston-Salem, NC 27113
Telephone: [phone]
Fax: [phone]
www.progressenvironmental.com
Mebane, N.C.
Date: 2021
Alamance County GIS
https://apps.alamance-
nc.com/CountyGISMap/default.aspx
Approximate Scale: Not to Scale
Project: West 70 Curb Market
Client: McLeod Oil
Progress Job #: 1021014.001
Date: February 2021
Site
TABLES
Lead EDB
Well Number Sampling Date
MW-1 01/02/21 4,380 78.5 1,410 317 18,900 14,300 1,440 7,660 5.5 1.1 57,100 22,000 6,350
1 70 600 70 20 600 400 500 15 0.02 400 700 200
5,000 70,000 84,500 70,000 20,000 260,000 28,500 85,500 15,000 50 NS NS NS
Notes:
= Exceeds North Carolina 2L Groundwater Quality Standards (NC2LGWQS)
= Exceeds Gross Contamination Levels (GCLs)
Contaminant concentrations are reported in micrograms per liter (µg/L)
NE = Not Established
BQL = Below Quantitation Limts
NT = Not Tested
NS No Standard LeadEDBC5-C8 AliphaticsGCLs BenzeneContaminant of Concern
NC2LGWQS IsopropyletherEthylbenzeneChloroformMethyl tert butyl etherMEBANE, ALAMANCE COUNTY, NORTH CAROLINA
INCIDENT NO. 45313
TABLE B-4
SUMMARY OF DETECTED GROUNDWATER ANALYTICAL RESULTS
PHASE I LSA REPORT
WEST 70 CURB MARKET
110 WOODLAWN ROAD
MADEP Method VPHAnalytical Method
Toluene1,2,4-TrimethylbenzeneC9-C12 AliphaticsC9-C10 AromaticsTotal Xylenes
MAP ID OWNER NAME SITE ADDRESS MAILING ADDRESS WELL USE CONNECTED TO PUBLIC
WATER
PUBLIC WATER
AVAILABLE TO
PROPERTY
APPROXIMATE
DISTANCE OF WELL
FROM SOURCE AREA
(FT.)
168 Woodlawn Road
Mebane, North Carolina 27302
145 Woodlawn Road
Wilmington, North Carolina 28405
Locations of water-suply wells are depicted on Figure 4
YES
YES
YESSandra Cook et al 140 Woodlawn Road Not For Drinking 510'
WS-1 Joseph Combs 168 Woodlawn Road Irrigation/Livestock
WS-2
YES
MEBANE, ALAMANCE COUNTY, NORTH CAROLINA
TABLE B-5
WATER-SUPPLY WELL INFORMATION - JANUARY 2021
PHASE I LIMITED SITE ASSESSMENT REPORT
WEST 70 CURB MARKET
815'
110 WOODLAWN ROAD
Map ID Name Property Address Mailing Address
Map ID numbers are referenced to Figure 3
HOLT STREETYADKIN PRESY OF UN PRESBY CH
P O BOX 557
MEBANE, NC 27302
P O BOX 100
MEBANE, NC 27302-010US HIGHWAY 70
528 N CARR ST
MEBANE, NC 27302
133 WOODLAWN ROAD
MEBANE, NC 27302
6630 NC 62 NORTH
BURLINGTON, NC 27217
833 CENTER STREET
MEBANE, NC 27302
PO BOX 88
MADISON, NC 27055
NOT PROVIDED
110 WOODLAWN ROAD
MEBANE, NC 27302
165435 COOK ROY K III
H & J MANAGEMENT INC165434
165403 MCLEOD OIL CO INC
165421 MEBANE FIRST PRESBYTERIAN CH
165424
HOLT STREET
Site (165431)MACMOM, LLC
INCIDENT NO. 45313
TABLE B-6
SURROUNDING PROPERTY OWNERS
PHASE I LIMITED SITE ASSESSMENT REPORT
WEST 70 CURB MARKET
110 WOODLAWN ROAD
MEBANE, ALAMANCE COUNTY, NORTH CAROLINA
Well Screened Total Depth to Relative Groundwater
Monitoring Well Installation Diameter Interval Depth to Water Elevation Elevation
ID Date (inches)(feet)(feet)(feet TOC) (feet TOC )**(feet)
1/15/2021
MW-1 1/15/2021 2 15-30 30 18.92 100.00 81.08
TABLE B-7
WELL CONSTRUCTION INFORMATION
WEST 70 CURB MARKET
NCDEQ INCIDENT NO.: 45313
PHASE I LIMITED SITE ASSESSMENT
APPENDIX A
STANDARD SAMPLING PROCEDURES
EXHIBIT A
Procedures for Developing the Monitoring Wells
Well development will be performed no sooner than 24 hours after well construction is completed.
Wells will be developed by bailing or pumping a minimum of five well-volumes of groundwater
from the well.
The turbidity, pH, specific conductivity, dissolved oxygen and temperature of the development
water will be measured and recorded, and used as an indicator parameter to determine the
completion of the development process.
EXHIBIT B
Procedures for Collecting Groundwater Samples
Each well will be purged of three standing well volumes prior to sample collection to remove
stagnant water from the well and well bore in an effort to collect samples that are representative of
the water quality in the formation surrounding each well.
Chemical preservatives, if applicable, will be added to sample bottles by the laboratory.
Sample bottles will be labeled prior to sample collection.
Sample bottles will be filled directly from the Teflon or disposable bailer. Volatile organic samples
will be collected first.
The pH, temperature, and specific conductance of the sample will be measured and recorded.
These measurements will be taken from a sample deposited in a separate container. Visual
characteristics of the sample, including insoluble materials, will be recorded.
Caps will be secured on bottles, bottle will be placed in plastic bags and the bags will be sealed.
Documentation, including Chain-of-Custody Record and laboratory analytical request form, will
be completed for all samples.
Samples will be packed in coolers with "bubble wrap" and ice packs for shipment.
Chain-of-Custody Record and analytical request form will be placed inside cooler sealed with
security tape.
Samples will be shipped via overnight express to the analytical laboratory within 24 hours
following collection.
Laboratory will be advised of each sample shipment.
APPENDIX B
SAMPLING SHEET/BORING LOG/WELL CONSTRUCTION RECORD
Remarks:
Project Manager: J. Ballsieper
Casing Diameter:
Hole Diameter: 6.25"Start Date: 1/15/21
Date: February 2021
Location: Jonesville, NC
Project: West 70 Curb Market
Job No.: 1021014.001
Boring/Well ID:
Geologist:
60
50
40
30
Drilling Method: Geoprobe - SSA
20
10
Sample
ID
Complete Date: 1/15/21
(feet)DepthRec/Adv(ppm)Blows (in)PIDGeologic Description
LithologyWater TablePage 1 of 1
30
40
20
10
Well Diagram
MW-1
60
50
Monitoring Well Installed to 30 feet bls
120 Fayette StreetWinston-Salem, North Carolina 27101(336) 722-9999
Gravel
Ground Surface
(17.0') #2Quartz Sand(15.0') 2"PVC Screen
(15.0') 2"PVC Casing
(4.0') GroutFill Material
(9.0') Bentonite
Orange brown finesandy silt (Petroleum Odors)
APPENDIX C
RETURNED WATER-SUPPLY WELL QUESTIONNAIRES
APPENDIX D
LABORATORY TEST REPORTS AND CHAINS-OF-CUSTODY
#=CL#
February 02, 2021
LIMS USE: FR - JEFF BALLSIEPER
LIMS OBJECT ID: 92516967
92516967
Project:
Pace Project No.:
RE:
Jeff Ballsieper
Progress Environmental, Inc.
120 Fayette St.
Winston Salem, NC 27101
West 70 Curb Market
Dear Jeff Ballsieper:
Enclosed are the analytical results for sample(s) received by the laboratory on January 15, 2021. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Stephanie Knott
[e-mail]
Project Manager
336-996-2841
Enclosures
cc:Jay Lawson, Progressive Environmental Group
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
106 Short St.
Kernersville, NC 27284
336-996-2841
Page 1 of 17
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92516967
West 70 Curb Market
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
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DOD Certification: #1461.01
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Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
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Kentucky Certification #: 90010
Louisiana Certification #: AI30792
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Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: VT2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
106 Short St.
Kernersville, NC 27284
336-996-2841
Page 2 of 17
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92516967
West 70 Curb Market
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92516967001 MW-1 EPA 504.1 4 PASI-CJMS1
MADEP VPH 6 PANACG
EPA 200.7 Rev 4.4 1994 1 PASI-ABG2
SM 6200B 69 PASI-CPM1
PAN = Pace National - Mt. Juliet
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
106 Short St.
Kernersville, NC 27284
336-996-2841
Page 3 of 17
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92516967
West 70 Curb Market
Sample:MW-1 Lab ID:92516967001 Collected:01/15/21 11:45 Received:01/15/21 16:29 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 504.1 Preparation Method: EPA 504.1
Pace Analytical Services - Charlotte
504 GCS EDB and DBCP
1,2-Dibromo-3-chloropropane ND ug/L 01/21/21 11:32 96-12-801/20/21 09:220.10 2
1,2-Dibromoethane (EDB)1.1 ug/L 01/21/21 11:32 106-93-401/20/21 09:220.042 2
1,2,3-Trichloropropane ND ug/L 01/21/21 11:32 96-18-401/20/21 09:220.10 2
Surrogates
1-Chloro-2-bromopropane (S)134 %01/21/21 11:32 301-79-56 S501/20/21 09:2270-130 2
Analytical Method: MADEP VPH Preparation Method: MADEPV
Pace National - Mt. Juliet
MADEPV
Aliphatic (C05-C08)57100 ug/L 01/27/21 22:4801/27/21 22:48100010
Aliphatic (C09-C12)22000 ug/L 01/27/21 22:4801/27/21 22:48100010
Aromatic (C09-C10),Unadjusted 6350 ug/L 01/27/21 22:48 TPHC9C10A01/27/21 22:48100010
Total VPH 85500 ug/L 01/27/21 22:48 VPH01/27/21 22:48100010
Surrogates
2,5-Dibromotoluene (FID)96.7 %01/27/21 22:48 615-59-8FID01/27/21 22:4870.0-130 10
2,5-Dibromotoluene (PID)87.1 %01/27/21 22:48 615-59-8PID01/27/21 22:4870.0-130 10
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
200.7 MET ICP
Lead 5.5 ug/L 01/21/21 16:15 7439-92-101/21/21 01:565.0 1
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 01/22/21 18:15 75-85-412500125
tert-Amylmethyl ether ND ug/L 01/22/21 18:15 994-05-81250125
Benzene 4380 ug/L 01/22/21 18:15 71-43-262.5 125
Bromobenzene ND ug/L 01/22/21 18:15 108-86-162.5 125
Bromochloromethane ND ug/L 01/22/21 18:15 74-97-562.5 125
Bromodichloromethane ND ug/L 01/22/21 18:15 75-27-462.5 125
Bromoform ND ug/L 01/22/21 18:15 75-25-262.5 125
Bromomethane ND ug/L 01/22/21 18:15 74-83-9625125
tert-Butyl Alcohol ND ug/L 01/22/21 18:15 75-65-02500125
n-Butylbenzene ND ug/L 01/22/21 18:15 104-51-862.5 125
sec-Butylbenzene ND ug/L 01/22/21 18:15 135-98-862.5 125
tert-Butylbenzene ND ug/L 01/22/21 18:15 98-06-662.5 125
tert-Butyl Formate ND ug/L 01/22/21 18:15 762-75-42500125
Carbon tetrachloride ND ug/L 01/22/21 18:15 56-23-562.5 125
Chlorobenzene ND ug/L 01/22/21 18:15 108-90-762.5 125
Chloroethane ND ug/L 01/22/21 18:15 75-00-3125125
Chloroform 78.5 ug/L 01/22/21 18:15 67-66-362.5 125
Chloromethane ND ug/L 01/22/21 18:15 74-87-3125125
2-Chlorotoluene ND ug/L 01/22/21 18:15 95-49-862.5 125
4-Chlorotoluene ND ug/L 01/22/21 18:15 106-43-462.5 125
1,2-Dibromo-3-chloropropane ND ug/L 01/22/21 18:15 96-12-8125125
Dibromochloromethane ND ug/L 01/22/21 18:15 124-48-162.5 125
1,2-Dibromoethane (EDB)ND ug/L 01/22/21 18:15 106-93-462.5 125
Dibromomethane ND ug/L 01/22/21 18:15 74-95-362.5 125
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/02/2021 06:39 PM
Pace Analytical Services, LLC
106 Short St.
Kernersville, NC 27284
336-996-2841
Page 4 of 17
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92516967
West 70 Curb Market
Sample:MW-1 Lab ID:92516967001 Collected:01/15/21 11:45 Received:01/15/21 16:29 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,2-Dichlorobenzene ND ug/L 01/22/21 18:15 95-50-162.5 125
1,3-Dichlorobenzene ND ug/L 01/22/21 18:15 541-73-162.5 125
1,4-Dichlorobenzene ND ug/L 01/22/21 18:15 106-46-762.5 125
Dichlorodifluoromethane ND ug/L 01/22/21 18:15 75-71-862.5 125
1,1-Dichloroethane ND ug/L 01/22/21 18:15 75-34-362.5 125
1,2-Dichloroethane ND ug/L 01/22/21 18:15 107-06-262.5 125
1,1-Dichloroethene ND ug/L 01/22/21 18:15 75-35-462.5 125
cis-1,2-Dichloroethene ND ug/L 01/22/21 18:15 156-59-262.5 125
trans-1,2-Dichloroethene ND ug/L 01/22/21 18:15 156-60-562.5 125
1,2-Dichloropropane ND ug/L 01/22/21 18:15 78-87-562.5 125
1,3-Dichloropropane ND ug/L 01/22/21 18:15 142-28-962.5 125
2,2-Dichloropropane ND ug/L 01/22/21 18:15 594-20-762.5 125
1,1-Dichloropropene ND ug/L 01/22/21 18:15 563-58-662.5 125
cis-1,3-Dichloropropene ND ug/L 01/22/21 18:15 10061-01-562.5 125
trans-1,3-Dichloropropene ND ug/L 01/22/21 18:15 10061-02-662.5 125
Diisopropyl ether 317 ug/L 01/22/21 18:15 108-20-362.5 125
Ethanol ND ug/L 01/22/21 18:15 64-17-525000125
Ethylbenzene 1410 ug/L 01/22/21 18:15 100-41-462.5 125
Ethyl-tert-butyl ether ND ug/L 01/22/21 18:15 637-92-31250125
Hexachloro-1,3-butadiene ND ug/L 01/22/21 18:15 87-68-3250125
Isopropylbenzene (Cumene)ND ug/L 01/22/21 18:15 98-82-862.5 125
Methylene Chloride ND ug/L 01/22/21 18:15 75-09-2250125
Methyl-tert-butyl ether 18900 ug/L 01/22/21 18:15 1634-04-462.5 125
Naphthalene ND ug/L 01/22/21 18:15 91-20-3250125
n-Propylbenzene ND ug/L 01/22/21 18:15 103-65-162.5 125
Styrene ND ug/L 01/22/21 18:15 100-42-562.5 125
1,1,1,2-Tetrachloroethane ND ug/L 01/22/21 18:15 630-20-662.5 125
1,1,2,2-Tetrachloroethane ND ug/L 01/22/21 18:15 79-34-562.5 125
Tetrachloroethene ND ug/L 01/22/21 18:15 127-18-462.5 125
Toluene 14300 ug/L 01/22/21 18:15 108-88-362.5 125
1,2,3-Trichlorobenzene ND ug/L 01/22/21 18:15 87-61-6250125
1,2,4-Trichlorobenzene ND ug/L 01/22/21 18:15 120-82-1250125
1,1,1-Trichloroethane ND ug/L 01/22/21 18:15 71-55-662.5 125
1,1,2-Trichloroethane ND ug/L 01/22/21 18:15 79-00-562.5 125
Trichloroethene ND ug/L 01/22/21 18:15 79-01-662.5 125
Trichlorofluoromethane ND ug/L 01/22/21 18:15 75-69-4125125
1,2,3-Trichloropropane ND ug/L 01/22/21 18:15 96-18-462.5 125
1,2,4-Trimethylbenzene 1440 ug/L 01/22/21 18:15 95-63-662.5 125
1,3,5-Trimethylbenzene ND ug/L 01/22/21 18:15 108-67-862.5 125
Vinyl chloride ND ug/L 01/22/21 18:15 75-01-4125125
m&p-Xylene 4760 ug/L 01/22/21 18:15 179601-23-1125125
o-Xylene 2900 ug/L 01/22/21 18:15 95-47-662.5 125
Surrogates
1,2-Dichloroethane-d4 (S)91 %01/22/21 18:15 17060-07-070-130 125
4-Bromofluorobenzene (S)93 %01/22/21 18:15 460-00-470-130 125
Toluene-d8 (S)100 %01/22/21 18:15 2037-26-570-130 125
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/02/2021 06:39 PM
Pace Analytical Services, LLC
106 Short St.
Kernersville, NC 27284
336-996-2841
Page 5 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92516967
West 70 Curb Market
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1611496
MADEPV
MADEP VPH
MADEPV
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92516967001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3616425-3
Associated Lab Samples:92516967001
Matrix:Water
Analyzed
Aliphatic (C05-C08)ug/L ND 100 01/26/21 13:38
Aliphatic (C09-C12)ug/L ND 100 01/26/21 13:38
Aromatic (C09-C10),Unadjusted ug/L ND 100 01/26/21 13:38
Total VPH ug/L ND 100 01/26/21 13:38
2,5-Dibromotoluene (FID)%79.9 70.0-130 01/26/21 13:38
2,5-Dibromotoluene (PID)%70.7 70.0-130 01/26/21 13:38
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3616425-1LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3616425-2
Aliphatic (C05-C08)ug/L 12201200 102 70.0-1301021220 0.00 25
Aliphatic (C09-C12)ug/L 14601400 104 70.0-1301041450 0.687 25
Aromatic (C09-C10),Unadjusted ug/L 185200 92.5 70.0-13092.5185 0.00 25
Total VPH ug/L 28702800 103 70.0-1301022860 0.349 25
2,5-Dibromotoluene (FID)%86.2 70.0-13084.8
2,5-Dibromotoluene (PID)%76.9 70.0-13075.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/02/2021 06:39 PM
Pace Analytical Services, LLC
106 Short St.
Kernersville, NC 27284
336-996-2841
Page 6 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92516967
West 70 Curb Market
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
594211
EPA 200.7 Rev 4.4 1994
EPA 200.7 Rev 4.4 1994
200.7 MET
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92516967001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3135373
Associated Lab Samples:92516967001
Matrix:Water
Analyzed
Lead ug/L ND 5.0 01/21/21 15:59
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3135374LABORATORY CONTROL SAMPLE:
LCSSpike
Lead ug/L 475500 95 85-115
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3135375MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92517248001
3135376
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Lead ug/L 500 100 70-130101 2500ND500509
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3135377MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92517313002
3135378
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Lead ug/L 500 102 70-130102 0500ND510512
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/02/2021 06:39 PM
Pace Analytical Services, LLC
106 Short St.
Kernersville, NC 27284
336-996-2841
Page 7 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92516967
West 70 Curb Market
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
594725
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92516967001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3137739
Associated Lab Samples:92516967001
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 01/22/21 13:13
1,1,1-Trichloroethane ug/L ND 0.50 01/22/21 13:13
1,1,2,2-Tetrachloroethane ug/L ND 0.50 01/22/21 13:13
1,1,2-Trichloroethane ug/L ND 0.50 01/22/21 13:13
1,1-Dichloroethane ug/L ND 0.50 01/22/21 13:13
1,1-Dichloroethene ug/L ND 0.50 01/22/21 13:13
1,1-Dichloropropene ug/L ND 0.50 01/22/21 13:13
1,2,3-Trichlorobenzene ug/L ND 2.0 01/22/21 13:13
1,2,3-Trichloropropane ug/L ND 0.50 01/22/21 13:13
1,2,4-Trichlorobenzene ug/L ND 2.0 01/22/21 13:13
1,2,4-Trimethylbenzene ug/L ND 0.50 01/22/21 13:13
1,2-Dibromo-3-chloropropane ug/L ND 1.0 01/22/21 13:13
1,2-Dibromoethane (EDB)ug/L ND 0.50 01/22/21 13:13
1,2-Dichlorobenzene ug/L ND 0.50 01/22/21 13:13
1,2-Dichloroethane ug/L ND 0.50 01/22/21 13:13
1,2-Dichloropropane ug/L ND 0.50 01/22/21 13:13
1,3,5-Trimethylbenzene ug/L ND 0.50 01/22/21 13:13
1,3-Dichlorobenzene ug/L ND 0.50 01/22/21 13:13
1,3-Dichloropropane ug/L ND 0.50 01/22/21 13:13
1,4-Dichlorobenzene ug/L ND 0.50 01/22/21 13:13
2,2-Dichloropropane ug/L ND 0.50 01/22/21 13:13
2-Chlorotoluene ug/L ND 0.50 01/22/21 13:13
4-Chlorotoluene ug/L ND 0.50 01/22/21 13:13
Benzene ug/L ND 0.50 01/22/21 13:13
Bromobenzene ug/L ND 0.50 01/22/21 13:13
Bromochloromethane ug/L ND 0.50 01/22/21 13:13
Bromodichloromethane ug/L ND 0.50 01/22/21 13:13
Bromoform ug/L ND 0.50 01/22/21 13:13
Bromomethane ug/L ND 5.0 01/22/21 13:13
Carbon tetrachloride ug/L ND 0.50 01/22/21 13:13
Chlorobenzene ug/L ND 0.50 01/22/21 13:13
Chloroethane ug/L ND 1.0 01/22/21 13:13
Chloroform ug/L ND 0.50 01/22/21 13:13
Chloromethane ug/L ND 1.0 01/22/21 13:13
cis-1,2-Dichloroethene ug/L ND 0.50 01/22/21 13:13
cis-1,3-Dichloropropene ug/L ND 0.50 01/22/21 13:13
Dibromochloromethane ug/L ND 0.50 01/22/21 13:13
Dibromomethane ug/L ND 0.50 01/22/21 13:13
Dichlorodifluoromethane ug/L ND 0.50 01/22/21 13:13
Diisopropyl ether ug/L ND 0.50 01/22/21 13:13
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/02/2021 06:39 PM
Pace Analytical Services, LLC
106 Short St.
Kernersville, NC 27284
336-996-2841
Page 8 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92516967
West 70 Curb Market
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3137739
Associated Lab Samples:92516967001
Matrix:Water
Analyzed
Ethanol ug/L ND 200 01/22/21 13:13
Ethyl-tert-butyl ether ug/L ND 10.0 01/22/21 13:13
Ethylbenzene ug/L ND 0.50 01/22/21 13:13
Hexachloro-1,3-butadiene ug/L ND 2.0 01/22/21 13:13
Isopropylbenzene (Cumene)ug/L ND 0.50 01/22/21 13:13
m&p-Xylene ug/L ND 1.0 01/22/21 13:13
Methyl-tert-butyl ether ug/L ND 0.50 01/22/21 13:13
Methylene Chloride ug/L ND 2.0 01/22/21 13:13
n-Butylbenzene ug/L ND 0.50 01/22/21 13:13
n-Propylbenzene ug/L ND 0.50 01/22/21 13:13
Naphthalene ug/L ND 2.0 01/22/21 13:13
o-Xylene ug/L ND 0.50 01/22/21 13:13
sec-Butylbenzene ug/L ND 0.50 01/22/21 13:13
Styrene ug/L ND 0.50 01/22/21 13:13
tert-Amyl Alcohol ug/L ND 100 01/22/21 13:13
tert-Amylmethyl ether ug/L ND 10.0 01/22/21 13:13
tert-Butyl Alcohol ug/L ND 20.0 01/22/21 13:13
tert-Butyl Formate ug/L ND 20.0 01/22/21 13:13
tert-Butylbenzene ug/L ND 0.50 01/22/21 13:13
Tetrachloroethene ug/L ND 0.50 01/22/21 13:13
Toluene ug/L ND 0.50 01/22/21 13:13
trans-1,2-Dichloroethene ug/L ND 0.50 01/22/21 13:13
trans-1,3-Dichloropropene ug/L ND 0.50 01/22/21 13:13
Trichloroethene ug/L ND 0.50 01/22/21 13:13
Trichlorofluoromethane ug/L ND 1.0 01/22/21 13:13
Vinyl chloride ug/L ND 1.0 01/22/21 13:13
1,2-Dichloroethane-d4 (S)%95 70-130 01/22/21 13:13
4-Bromofluorobenzene (S)%102 70-130 01/22/21 13:13
Toluene-d8 (S)%102 70-130 01/22/21 13:13
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3137740LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 52.350 105 60-140
1,1,1-Trichloroethane ug/L 46.050 92 60-140
1,1,2,2-Tetrachloroethane ug/L 47.750 95 60-140
1,1,2-Trichloroethane ug/L 49.450 99 60-140
1,1-Dichloroethane ug/L 44.250 88 60-140
1,1-Dichloroethene ug/L 44.450 89 60-140
1,1-Dichloropropene ug/L 45.850 92 60-140
1,2,3-Trichlorobenzene ug/L 56.550 113 60-140
1,2,3-Trichloropropane ug/L 47.750 95 60-140
1,2,4-Trichlorobenzene ug/L 56.250 112 60-140
1,2,4-Trimethylbenzene ug/L 51.050 102 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/02/2021 06:39 PM
Pace Analytical Services, LLC
106 Short St.
Kernersville, NC 27284
336-996-2841
Page 9 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92516967
West 70 Curb Market
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3137740LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/L 54.750 109 60-140
1,2-Dibromoethane (EDB)ug/L 47.850 96 60-140
1,2-Dichlorobenzene ug/L 59.550 119 60-140
1,2-Dichloroethane ug/L 45.550 91 60-140
1,2-Dichloropropane ug/L 46.650 93 60-140
1,3,5-Trimethylbenzene ug/L 51.250 102 60-140
1,3-Dichlorobenzene ug/L 50.550 101 60-140
1,3-Dichloropropane ug/L 45.450 91 60-140
1,4-Dichlorobenzene ug/L 49.550 99 60-140
2,2-Dichloropropane ug/L 48.150 96 60-140
2-Chlorotoluene ug/L 53.450 107 60-140
4-Chlorotoluene ug/L 48.750 97 60-140
Benzene ug/L 47.050 94 60-140
Bromobenzene ug/L 59.650 119 60-140
Bromochloromethane ug/L 43.150 86 60-140
Bromodichloromethane ug/L 45.950 92 60-140
Bromoform ug/L 46.950 94 60-140
Bromomethane ug/L 49.850 100 60-140
Carbon tetrachloride ug/L 48.750 97 60-140
Chlorobenzene ug/L 49.950 100 60-140
Chloroethane ug/L 41.150 82 60-140
Chloroform ug/L 45.350 91 60-140
Chloromethane ug/L 36.150 72 60-140
cis-1,2-Dichloroethene ug/L 41.950 84 60-140
cis-1,3-Dichloropropene ug/L 48.050 96 60-140
Dibromochloromethane ug/L 49.050 98 60-140
Dibromomethane ug/L 47.150 94 60-140
Dichlorodifluoromethane ug/L 42.550 85 60-140
Diisopropyl ether ug/L 41.750 83 60-140
Ethanol ug/L 18002000 90 60-140
Ethyl-tert-butyl ether ug/L 97.8100 98 60-140
Ethylbenzene ug/L 50.450 101 60-140
Hexachloro-1,3-butadiene ug/L 52.650 105 60-140
Isopropylbenzene (Cumene)ug/L 46.250 92 60-140
m&p-Xylene ug/L 95.0100 95 60-140
Methyl-tert-butyl ether ug/L 46.750 93 60-140
Methylene Chloride ug/L 41.450 83 60-140
n-Butylbenzene ug/L 54.250 108 60-140
n-Propylbenzene ug/L 52.850 106 60-140
Naphthalene ug/L 56.950 114 60-140
o-Xylene ug/L 42.650 85 60-140
sec-Butylbenzene ug/L 51.950 104 60-140
Styrene ug/L 43.350 87 60-140
tert-Amyl Alcohol ug/L 10801000 108 60-140
tert-Amylmethyl ether ug/L 102100 102 60-140
tert-Butyl Alcohol ug/L 476500 95 60-140
tert-Butyl Formate ug/L 424400 106 60-140
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/02/2021 06:39 PM
Pace Analytical Services, LLC
106 Short St.
Kernersville, NC 27284
336-996-2841
Page 10 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92516967
West 70 Curb Market
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3137740LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/L 44.250 88 60-140
Tetrachloroethene ug/L 46.550 93 60-140
Toluene ug/L 44.650 89 60-140
trans-1,2-Dichloroethene ug/L 44.250 88 60-140
trans-1,3-Dichloropropene ug/L 50.550 101 60-140
Trichloroethene ug/L 46.150 92 60-140
Trichlorofluoromethane ug/L 41.150 82 60-140
Vinyl chloride ug/L 36.650 73 60-140
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%107 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3137741MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92517919008
3137742
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 4000 112 60-140115 34000ND44704590
1,1,1-Trichloroethane ug/L 4000 92 60-14090 34000ND36903580
1,1,2,2-Tetrachloroethane ug/L 4000 110 60-140108 24000ND44104330
1,1,2-Trichloroethane ug/L 4000 100 60-140103 34000ND40204140
1,1-Dichloroethane ug/L 4000 83 60-14084 14000ND33403370
1,1-Dichloroethene ug/L 4000 64 60-14065 24000ND25702620
1,1-Dichloropropene ug/L 4000 82 60-14083 14000ND32803310
1,2,3-Trichlorobenzene ug/L 4000 108 60-140113 54000ND43104520
1,2,3-Trichloropropane ug/L 4000 105 60-140106 04000ND42204230
1,2,4-Trichlorobenzene ug/L 4000 106 60-140109 34000ND42504370
1,2,4-Trimethylbenzene ug/L 4000 112 60-140117 34000122057105890
1,2-Dibromo-3-chloropropane ug/L 4000 110 60-140115 44000ND44204620
1,2-Dibromoethane (EDB)ug/L 4000 110 60-140110 0400013645404540
1,2-Dichlorobenzene ug/L 4000 114 60-140116 24000ND45504640
1,2-Dichloroethane ug/L 4000 90 60-14092 2400029539103990
1,2-Dichloropropane ug/L 4000 98 60-14098 04000ND39403940
1,3,5-Trimethylbenzene ug/L 4000 118 60-140119 14000ND47204760
1,3-Dichlorobenzene ug/L 4000 110 60-140111 14000ND44004450
1,3-Dichloropropane ug/L 4000 105 60-140105 04000ND41804190
1,4-Dichlorobenzene ug/L 4000 109 60-140111 24000ND43604440
2,2-Dichloropropane ug/L M140002060-14018 124000ND820731
2-Chlorotoluene ug/L 4000 111 60-140115 44000ND44204590
4-Chlorotoluene ug/L 4000 108 60-140110 14000ND43404390
Benzene ug/L 4000 90 60-140116 54000166002020021300
Bromobenzene ug/L 4000 114 60-140114 04000ND45704560
Bromochloromethane ug/L 4000 90 60-14087 34000ND36003480
Bromodichloromethane ug/L 4000 99 60-14098 14000ND39603930
Bromoform ug/L 4000 112 60-140115 34000ND44804600
Bromomethane ug/L M140004860-14041 164000ND19401650
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/02/2021 06:39 PM
Pace Analytical Services, LLC
106 Short St.
Kernersville, NC 27284
336-996-2841
Page 11 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92516967
West 70 Curb Market
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3137741MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92517919008
3137742
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Carbon tetrachloride ug/L 4000 98 60-14092 74000ND39303670
Chlorobenzene ug/L 4000 109 60-140109 04000ND43704370
Chloroethane ug/L M140003860-14040 64000ND15301610
Chloroform ug/L 4000 90 60-14088 24000ND36103520
Chloromethane ug/L M140001860-14017 54000ND708672
cis-1,2-Dichloroethene ug/L 4000 88 60-14086 24000ND35203440
cis-1,3-Dichloropropene ug/L 4000 80 60-14079 14000ND32003160
Dibromochloromethane ug/L 4000 114 60-140115 24000ND45504610
Dibromomethane ug/L 4000 101 60-140100 14000ND40204000
Dichlorodifluoromethane ug/L M14000060-14014000NDNDND
Diisopropyl ether ug/L 4000 86 60-14087 14000ND34603490
Ethanol ug/L 160000 81 60-14075 7160000ND129000121000
Ethyl-tert-butyl ether ug/L 8000 94 60-14094 08000ND75307550
Ethylbenzene ug/L 4000 111 60-140116 34000188063306520
Hexachloro-1,3-butadiene ug/L 4000 100 60-140100 04000ND40104000
Isopropylbenzene (Cumene)ug/L 4000 113 60-140114 24000ND45004570
m&p-Xylene ug/L 8000 114 60-140124 5800057001490015600
Methyl-tert-butyl ether ug/L 4000 88 60-14085 44000ND35303390
Methylene Chloride ug/L 4000 77 60-14076 24000ND30803030
n-Butylbenzene ug/L 4000 101 60-140102 14000ND40304080
n-Propylbenzene ug/L 4000 109 60-140112 24000ND43704470
Naphthalene ug/L 4000 113 60-140119 5400058551205360
o-Xylene ug/L 4000 120 60-140127 44000312079108210
sec-Butylbenzene ug/L 4000 108 60-140112 44000ND43104490
Styrene ug/L 4000 115 60-140114 14000ND46204560
tert-Amyl Alcohol ug/L 80000 109 60-140114 48000013200J100000105000
tert-Amylmethyl ether ug/L 8000 98 60-14096 28000ND78607690
tert-Butyl Alcohol ug/L 40000 102 60-140105 340000ND4100042100
tert-Butyl Formate ug/L 32000 92 60-14090 232000ND2930028800
tert-Butylbenzene ug/L 4000 96 60-14099 34000ND38503980
Tetrachloroethene ug/L 4000 103 60-140100 34000ND41203980
Toluene ug/L M1400010360-140144 64000245002860030300
trans-1,2-Dichloroethene ug/L 4000 75 60-14075 04000ND30003010
trans-1,3-Dichloropropene ug/L 4000 78 60-14081 34000ND31203220
Trichloroethene ug/L 4000 98 60-14094 44000ND39203770
Trichlorofluoromethane ug/L M140004760-14049 44000ND19001960
Vinyl chloride ug/L M140001660-14016 34000ND623640
1,2-Dichloroethane-d4 (S)%101 70-13099
4-Bromofluorobenzene (S)%99 70-130100
Toluene-d8 (S)%99 70-13097
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/02/2021 06:39 PM
Pace Analytical Services, LLC
106 Short St.
Kernersville, NC 27284
336-996-2841
Page 12 of 17
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92516967
West 70 Curb Market
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
593942
EPA 504.1
EPA 504.1
GCS 504 EDB DBCP
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92516967001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3133834
Associated Lab Samples:92516967001
Matrix:Water
Analyzed
1,2,3-Trichloropropane ug/L ND 0.050 01/20/21 11:07
1,2-Dibromo-3-chloropropane ug/L ND 0.050 01/20/21 11:07
1,2-Dibromoethane (EDB)ug/L ND 0.020 01/20/21 11:07
1-Chloro-2-bromopropane (S)%94 70-130 01/20/21 11:07
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3133835LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
3133836
1,2,3-Trichloropropane ug/L 0.320.25 128 70-1301120.28 13 20
1,2-Dibromo-3-chloropropane ug/L 0.260.25 105 70-130970.24 8 20
1,2-Dibromoethane (EDB)ug/L 0.230.25 94 70-130940.23 0 20
1-Chloro-2-bromopropane (S)%98 70-13093
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3133838MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92517285009
3133839
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,2,3-Trichloropropane ug/L M10.25 246 65-135257 40.25<14.7 0.62 0.65
1,2-Dibromo-3-chloropropane ug/L M10.25 1440 65-1351470 20.25<50.7 3.6 3.7
1,2-Dibromoethane (EDB)ug/L M10.25 -80700 65-135-81700 00.25806 603 601
1-Chloro-2-bromopropane (S)%S244470-130441
Parameter Units
Dup
Result QualifiersRPDResult
92515931001
3133837SAMPLE DUPLICATE:
1,2,3-Trichloropropane ug/L NDND
1,2-Dibromo-3-chloropropane ug/L NDND
1,2-Dibromoethane (EDB)ug/L NDND
1-Chloro-2-bromopropane (S)%112121
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/02/2021 06:39 PM
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106 Short St.
Kernersville, NC 27284
336-996-2841
Page 13 of 17
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92516967
West 70 Curb Market
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample
re-analysis).S2
Surrogate recovery outside control limits due to matrix interferences (not confirmed by re-analysis).S5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/02/2021 06:39 PM
Pace Analytical Services, LLC
106 Short St.
Kernersville, NC 27284
336-996-2841
Page 14 of 17
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92516967
West 70 Curb Market
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92516967001 593942 594020MW-1 EPA 504.1 EPA 504.1
92516967001 1611496 1611496MW-1 MADEPV MADEP VPH
92516967001 594211 594252MW-1 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994
92516967001 594725MW-1 SM 6200B
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/02/2021 06:39 PM
Pace Analytical Services, LLC
106 Short St.
Kernersville, NC 27284
336-996-2841
Page 15 of 17
Page 16 of 17
Page 17 of 17