WS-9913_45093_CA_SCH_20180822

609A Piner Road., Suite 115
Wilmington, North Carolina 28409
Telephone [phone]
Fax [phone]
www.atcgroupservices.com
August 21, 2018
Ms. Mindy Lepard
North Carolina Department of Environmental Quality
Winston-Salem Regional Office
Division of Waste Management – UST Section
450 West Hanes Mill Road, Suite 300
Winston-Salem, North Carolina 27105
RE: SITE CHECK REPORT
Pilot Travel Center No. 6955
1044 Jimmie Kerr Road
Haw River, Alamance County, North Carolina
NCDEQ Facility ID #00-0-0000035045
ATC Project No.: PT00695501
Dear Ms. Lepard:
ATC Associates of North Carolina, LLC (ATC), on behalf of Pilot Travel Centers, LLC (Pilot), is
submitting this Site Check Report for the referenced facility.
If you have any questions regarding this submittal, please contact Joey Cupp of Pilot at
865.474.2826, or Maureen Jackson of ATC at 919.871.0999.
Sincerely,
ATC ASSOCIATES OF NORTH CAROLINA, LLC
Maureen Jackson, P.G.Max Burmeister
Senior Project Manager Program Manager
cc:Pilot Travel Centers, LLC
UST CLOSURE REPORT
PILOT TRAVEL CENTER NO. 6955
1044 JIMMIE KERR ROAD
HAW RIVER, ALAMANCE COUNTY, NORTH CAROLINA
FACILITY ID NO. 00-0-0000035045
ATC PROJECT NO. PT00695501
August 21, 2018
Prepared for:
Pilot Travel Center
5508 Lonas Drive
Knoxville, Tennessee 37909
Prepared by:
ATC Associates of North Carolina, P.C.
609A Piner Road, Suite 115
Wilmington, North Carolina 28409
Pilot Site No. 6955 August 21, 2018
NCDEQ Facility ID #00-0-0000035045 Site Check Report
ATC Associates of North Carolina
B. SITE HISTORY
1.Provide UST Owner and Operator Information:
See Table 1.
2.Provide UST Information:
See Table 2.
3.Provide Non-UST Information:
No ASTs or Surface Spills are known to exist at the site.
4.Describe relation of location of current UST system to historical UST releases:
No historical UST releases have been identified for the site.
5.Provide a Brief Description of Site Characteristics:
The subject property consists of one convenience store building, two fast food restaurants,
and petroleum fueling equipment. The subject property and surrounding area are fairly level.
The subject property is located in a light commercial area in proximity to Interstate-85/40 of
Haw River. Public water is supplied to the area. A topographic map and site map are
attached as Figures 1 and 2, respectively.
C. SITE CHECK PROCEDURES
1.UST System Testing:
On July 12, 2018, approximately 2 inches of diesel product was identified in the submersible
turbine pump (STP) sump for diesel tank #3, and the sump was in need of repair or
replacement. On July 13, 2018, ATC personnel submitted a UST-17A UST Suspected
Release 24 Hour Notice on behalf of Pilot Travel Centers, LLC (Pilot). On July 20, 2018, a
UST-17B UST Suspected Release 7 Day Notice was submitted by ATC personnel. On
August 16, 2018, upon receipt of the soil analytical results, ATC personnel submitted a UST-
61 24-Hour Release and UST Leak Reporting Form to NCDEQ Winston-Salem Regional
Office.
Copies of the referenced notifications are provided in Attachment I.
2.Site Check Procedure:
On August 13, 2018, ATC personnel contracted with Geologic Exploration to hand auger a
borehole 5 feet below ground surface (bgs) in proximity to the diesel tank #3 STP sump. ATC
personnel collected a soil sample at the 5-foot bgs interval for laboratory analysis. The
location of the soil sample is provided on Figure 2.
3.Soil Excavation Activities:
Soil excavation was not performed, as part of this site check.
Pilot Site No. 6955 August 21, 2018
NCDEQ Facility ID #00-0-0000035045 Site Check Report
ATC Associates of North Carolina
D. SITE INVESTIGATION
1.Field Screening:
Soil sample SB-1was not screened at the time of collection.
2.Soil Sampling Information:
Soil sample SB-1 was collected at an interval of approximately 5 feet bgs, on August 13,
2018. The soil encountered consisted of brown/green/grey silty sand at a depth of
approximately 5 feet bgs. Groundwater was not encountered in this boring to the termination
depth of 5 feet bgs. The boring log for SB-1 is provided in Attachment II.
The soil samples were shipped to a N.C. certified laboratory in a chilled cooler, following
proper chain-of-custody procedures to be analyzed by Environmental Protection Agency
(EPA) Method for 8260B, EPA Method 8270D, Massachusetts Department of Environmental
Protection (MADEP) Method for Volatile Petroleum Hydrocarbons (VPH), and MADEP Method
for Extractable Petroleum Hydrocarbons (EPH).
3.Groundwater and Surface Sampling Information:
Groundwater samples and surface water samples were not collected.
4.Quality Control Measures:
The soil samples were placed in laboratory provided jars and vials. Samples were
immediately placed on ice and contained in a cooler during transportation. Samples were
transported by courier under a chain-of-custody to the laboratory for analysis.
5.Investigation Results:
Laboratory analytical results of the soil sample collected adjacent to the diesel tank #3 STP
sump detected a C9-C22 Aromatics concentration above its established Soil-to-Groundwater
(STGW) Maximum Contaminant Concentrations (MSCCs). The results are shown in Table 3.
A copy of the laboratory report and chain-of-custody documents are provided in Attachment
III.
E. CONCLUSION AND RECOMMENDATIONS
Laboratory analytical results of the soil sample collected adjacent to the diesel tank #3 STP
sump detected a C9-C22 Aromatics concentration above its established STGW-MSCCs.
Based on the soil analytical data, it appears a release of petroleum has occurred from the
diesel tank #3 STP sump.
F. FIGURES
Figure 1 – Topographic Map
Figure 2 – Site Map with Boring Location
Pilot Site No. 6955 August 21, 2018
NCDEQ Facility ID #00-0-0000035045 Site Check Report
ATC Associates of North Carolina
G. TABLES
Table 1 – UST Owner and Operator Information
Table 2 – UST/AST System Information
Table 3 – Soil Analytical Results
H. ATTACHMENTS
I – Notifications and Testing Results
II – Boring Log
III – Soil Laboratory Report and Chain-of-Custody Documents
FIGURES

FIGURES

TABLES
TABLE 1
UST OWNER AND OPERATOR INFORMATION
PILOT STORE #6955
1044 JIMMIE KERR ROAD
HAW RIVER, ALAMANCE COUNTY, NORTH CAROLINA
Revision Date:8/17/2018 Incident Number and Name:Pilot Store #6955
UST ID Number All Facility ID Number 00-0-0000035045
City State Zip Telephone Number
Knoxville TN 37909 865-474-3106
City State Zip Telephone Number
Dates of Operation (MM/DD/YY to MM/DD/YY)Name of Owner
Dates of Operation (MM/DD/YY to MM/DD/YY)Name of Operator
5508 Lonas Road
Pilot Travel Centers, LLC 5/24/1996 to Present
Street Address
As Above
Street Address
TABLE 2
UST/AST SYSTEM INFORMATION
PILOT STORE #6955
1044 JIMMIE KERR ROAD
HAW RIVER, ALAMANCE COUNTY, NORTH CAROLINA
Revision Date:8/17/2018
UST ID Number
Current/Last
Contents
Previous
Contents
Capacity
(gallons)
Construction
Details
Tank
Dimensions
Description of
Associated
Piping and
Pumps
Date Tank
Installed Status of UST
Was Release
Associates with
the UST System?
1 Gasoline None 15,000 Steel Unknown Unknown 05/24/96 Active No
2 Gasoline None 10,000 Steel Unknown Unknown 05/24/96 Active No
3 Diesel None 25,000 Steel Unknown Unknown 05/24/96 Active Yes
4 Diesel None 25,000 Steel Unknown Unknown 05/24/96 Active Yes
AST ID Number
Current/Last
Contents
Previous
Contents
Capacity
(gallons)
Construction
Details
Tank
Dimensions
Description of
Associated
Piping and
Pumps
Date Tank
Installed Status of AST
Was Release
Associates with
the AST System?
Incident Number and Name:Pilot Store #6955
None associated with this site
TABLE 3
SOIL ANALYTICAL RESULTS
PILOT STORE #6955
1044 JIMMIE KERR ROAD
HAW RIVER, ALAMANCE COUNTY, NORTH CAROLINA
EPA
Method
8270D
SB-1 5 8/13/2018 0.080J <11 406 130 193
270 68 540 NE 31
469 939 1,500 31,000 469
12,264 24528 40,000 810,000 12,264
Notes:
1. Concentrations reported in milligrams per kilogram (mg/kg).
2. MSCC = Maximum Soil Contaminant Concentration.
3. Bold indicates concentrations above NCDEQ Soil-to-Groundwater MSCC.
4. J denotes value estimated by the laboratory.
Soil-to-Groundwater MSCC
Residential MSCC
Industrial/Commerical MSCC
Analytical Method MADEP Method EPH/VPH
Sample Depth (feet)Date Sampled PyreneC5-C8 AliphaticsC9-C18 AliphaticsC19-C36 AliphaticsC9-C22 Aromatics

ATTACHMENT I

DEQ Notifications

UST-17A UST Suspected Release 24 Hour Notice
Do not use this form to report a 24 hour notice of a Pollution Incident. You must use form UST-61, 24 Hour Release and UST Leak
Reporting Form.
 This form must be used to report to DEQ, within 24 hours of discovery, a Suspected Release from any of the following:
a) Failed or inconclusive leak detection or tightness test results. This includes positive test results, such as “Increase”, which
indicates the level in the UST system has increased more than 0.2 gph.
b) Unusual operating conditions which can include, but are not limited to: the erratic behavior of dispensing equipment; the
unexplained presence of water in the tank; the presence of fuel in containment sumps or interstitial spaces; or the degradation of
any equipment or element of an underground storage tank system to the point where that equipment or element can not reasonably
be expected to perform its intended function.
c) Internal inspection results such as, perforations, corrosion holes, weld failures, or other similar defects that indicate a release
could have occurred.
 If you have more than four UST systems to report suspected releases, then attach additional sheets of the UST-17A form. You only
need to list the UST systems at your site that have suspected releases.
 Within 7 days of discovery, submit a UST-17B form to document the response activities taken to investigate the suspected release.
 Please submit this form to: NCDEQ/DWM, UST Section
1646 Mail Service Center
Raleigh, North Carolina 27699-1646
OR
Fax to [phone] OR [e-mail]
I. UST OWNER II. UST FACILITY
Name:

Name:

Facility ID:

Address:

Address:

City:

State:

Zip:

City:

County:

Person Reporting:

Title of Person Reporting:

Telephone Number:
( )
III. UST INFORMATION
Tank Number / Size: / / / /
Product Stored:
Location and/or source of
suspected release:
(check all that apply)
Tank
Piping
Tank Sump
Dispenser Sump
Spill Bucket
Internal Inspection
Other (Explain in
comments)
Tank
Piping
Tank Sump
Dispenser Sump
Spill Bucket
Internal Inspection
Other (Explain in
comments)
Tank
Piping
Tank Sump
Dispenser Sump
Spill Bucket
Internal Inspection
Other (Explain in
comments)
Tank
Piping
Tank Sump
Dispenser Sump
Spill Bucket
Internal Inspection
Other (Explain in
comments)
Leak detection method or
other observation that
indicates a suspected
release. (e.g., ATG, SIR,
visual contamination, fuel
in sump, etc.):

Failed/Inconclusive date or
date that leak detection
method suspected release
discovered:

IV. COMMENTS

UST-17A Revised 10/2015 http://www.wastenotnc.org/web/wm/

UST-17B UST Suspected Release 7 Day Notice
 This form must be used to report to DEQ, within 7 days of discovery, the investigation results for a Suspected Release from any of the following:
a) Failed or inconclusive leak detection or tightness test results. This includes positive test results, such as “Increase”, which indicates the level in the
UST system has increased more than 0.2 gph.
b) Unusual operating conditions which can include, but are not limited to, the erratic behavior of dispensing equipment; the unexplained presence of
water in the tank; the presence of fuel in containment sumps or interstitial spaces; or the degradation of any equipment or element of an underground
storage tank system to the point where that equipment or element can not reasonably be expected to perform its intended function.
c) Internal inspection results such as, perforations, corrosion holes, weld failures, or other similar defects that indicate a release could have occurred.
 If you have more than four UST systems to report suspected release investigations, then attach additional sheets of the UST-17B form.
 Please submit this form along with the supporting documentation to:
NCDEQ/DWM, UST Section
1646 Mail Service Center
Raleigh, North Carolina 27699-1646
OR
Fax to [phone] OR [e-mail]
I. UST OWNER II. UST FACILITY
Name:

Name:

Facility ID:

Address:

Address:

City:

State:

Zip:

City:

County:

Person Reporting:

Title of Person Reporting:

Telephone Number:
( )
III. INVESTIGATION RESULTS
Tank Number / Size: / / / /
Product Stored:
Reason for Suspected
Release Investigation
(Check all that apply):

You must attach the
supporting documentation
specified in the footnote for
the reason(s) selected.
Data entry error 1
Dispensing fuel while
test is being conducted 2
Faulty equipment 3
Incorrect stick or meter
reading 1
Incorrect tank chart 4
Internal Inspection 5
Meter not calibrated 6
Other (Attach
explanation)1
Tank/Dispenser
containment sump contains liquid 7
Tilted tank 8
Unknown 1
Data entry error 1
Dispensing fuel while
test is being conducted 2
Faulty equipment 3
Incorrect stick or meter
reading 1
Incorrect tank chart 4
Internal Inspection 5
Meter not calibrated 6
Other (Attach
explanation)1
Tank/Dispenser
containment sump contains liquid 7
Tilted tank 8
Unknown 1
Data entry error 1
Dispensing fuel while
test is being conducted 2
Faulty equipment 3
Incorrect stick or meter
reading 1
Incorrect tank chart 4
Internal Inspection 5
Meter not calibrated 6
Other (Attach
explanation)1
Tank/Dispenser
containment sump contains liquid 7
Tilted tank 8
Unknown 1
Data entry error 1
Dispensing fuel while
test is being conducted 2
Faulty equipment 3
Incorrect stick or meter
reading 1
Incorrect tank chart 4
Internal Inspection 5
Meter not calibrated 6
Other (Attach
explanation)1
Tank/Dispenser
containment sump contains liquid 7
Tilted tank 8
Unknown 1
1 Conduct a tank and/or line tightness test and attach the results, along with all of the supporting data sheets for the test method, to this form for submittal.
The summary page listing the results by itself is not acceptable. If the tightness test results are fail, then you must repair or replace your UST system and
conduct a site check in accordance with 15A NCAC 2N .0603.
2 Provide sales receipts or other comparable documentation that shows fuel was being dispensed from the UST during the test.
3 Provide invoices (with a description of the work completed) or other documentation that shows the equipment has been repaired.
4 Correct your leak detection results using the correct tank chart and submit copies with this form.
5 Repair the UST in accordance with the manufacturer’s instructions or a national standard (e.g., PEI API 1631) and conduct a site check in accordance with
15A NCAC 2N .0603. If the UST is not repaired, then it must be permanently closed in accordance with the latest version of the UST Sections Guidelines
for Tank Closure.
6 Correct your leak detection results using the amount your meter was adjusted following calibration and submit copies of the meter calibration and leak
detection results with this form.
7 Conduct a tightness test (e.g., hydrostatic test) of the sump and submit the test result along with this form. If the test results are fail, then you must repair
or replace the containment sump and conduct a site check in accordance with 15A NCAC 2N .0603.
8 Submit documentation from your UST equipment contractor explaining how they determined the UST was tilted. Correct your leak detection results using a
tank chart adjusted for the tilt and submit with this form.
Note: Tank, piping, spill bucket and containment sump replacements must be done in accordance with 15A NCAC 2N .0900
UST-17B Revised 10/2015 http://www.wastenotnc.org/web/wm/

ATTACHMENT II

Boring Log

08-17-2018 S:\Enviro\Pilot\6955 - Haw River\Boring Logs\SB-1.borClient: Pilot
Project #: PT00695501
Haw River, Alamance County, NC
1044 Jimmie Kerr Road
Pilot #5955
BORING LOG: SB-1
(Page 1 of 1)
Date(s) Drilled : 08/13/18
Drilling Contractor : GEX
Drilling Method : Hand Auger
Boring Diameter : 2 inches
Sampling Method : NA
Sampling Interval : NA
Logged By : Robert Winfield
Depth In Feet (BGS)0
1
2
3
4
5 USCSGRAPHICDESCRIPTION
AR
SM
SM
SM
Asphalt
Brown; Silty SAND with some rock fragments
Brown; Silty SAND with pockets of green silty sand mixed in; Petroleum odor present
Brown, green, and grey; Silty SAND; Petroleum odor present
BGS - below ground surface
Boring terminated at 5 feet bgs.

ATTACHMENT III

Soil Analytical Report

39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
August 16, 2018
Maureen Jackson
ATC Group Services LLC - Raleigh NC
2725 East Millbrook Road, Ste 121
Raleigh, NC 27604
Project Location: Haw River, NC
Client Job Number:
Project Number: PT00695501
Laboratory Work Order Number: 18H0706
Enclosed are results of analyses for samples received by the laboratory on August 15, 2018. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Kerry K. McGee
Project Manager
Page 1 of 39
Table of Contents
Table of Contents
Sample Summary 3
Hits Only Report 4
Case Narrative 5
Sample Results 7
18H0706-01 7
Sample Preparation Information 14
QC Data 15
Volatile Organic Compounds by GC/MS 15
B210357 15
Semivolatile Organic Compounds by GC/MS 20
B210345 20
Petroleum Hydrocarbons Analyses - EPH 25
B210344 25
Petroleum Hydrocarbons Analyses - VPH 28
B209997 28
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) 30
B210372 30
Flag/Qualifier Summary 31
Certifications 32
Chain of Custody/Sample Receipt 37
Page 2 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
8/16/2018
ATC Group Services LLC - Raleigh NC
2725 East Millbrook Road, Ste 121
Raleigh, NC 27604
ATTN: Maureen Jackson
PT00695501
18H0706
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Haw River, NC
SB-1 18H0706-01 Soil MADEP-EPH-04-1.1
MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
SW-846 8260B
SW-846 8270D
[TOC_1]Sample Summary[TOC]
Page 3 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
[TOC_1]Hits Only Report[TOC]EXECUTIVE SUMMARY
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
18H0706-01SB-1
DL
Pyrene 0.080 0.20 mg/Kg dry SW-846 8270DJ0.065
C11-C22 Aromatics 160 12 mg/Kg dry MADEP-EPH-04-1.1
C19-C36 Aliphatics 130 12 mg/Kg dry MADEP-EPH-04-1.1
C9-C18 Aliphatics 380 58 mg/Kg dry MADEP-EPH-04-1.1
Unadjusted C11-C22 Aromatics 160 12 mg/Kg dry MADEP-EPH-04-1.1
C9-C10 Aromatics 33 11 mg/Kg dry MADEP-VPH-Feb 2018 Rev 2.11.6
C9-C12 Aliphatics 26 11 mg/Kg dry MADEP-VPH-Feb 2018 Rev 2.12.3
Unadjusted C9-C12 Aliphatics 59 11 mg/Kg dry MADEP-VPH-Feb 2018 Rev 2.12.3
% Solids 86.3 % Wt SM 2540G
Con-Test does not accept liability for the consequences of any actions taken solely on the basis of the information provided in the Executive Summary
section of this report. Users must review this report in its entirety to determine data usability and assessment.
Page 4 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
For method MA VPH only hydrocarbon ranges were requested and reported.
For method MA EPH, only hydrocarbon ranges were requested and reported.
[TOC_1]Case Narrative[TOC]
SW-846 8270D
Qualifications:
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD
between the two LFB/LCS results is within method specified criteria.
Analyte & Samples(s) Qualified:
L-07
Hexachlorocyclopentadiene
B210345-BS1
Initial calibration did not meet method specifications. Compound was calibrated using a response factor where %RSD is outside of method
specified criteria. Reported result is estimated.
Analyte & Samples(s) Qualified:
V-04
Benzidine
18H0706-01[SB-1], B210345-BLK1, B210345-BS1, B210345-BSD1
Continuing calibration did not meet method specifications and was biased on the low side for this compound. Reported result is estimated.
Analyte & Samples(s) Qualified:
V-05
Hexachlorocyclopentadiene
18H0706-01[SB-1], B210345-BLK1, B210345-BS1, B210345-BSD1
Continuing calibration did not meet method specifications and was biased on the high side for this compound. Reported result is estimated.
Analyte & Samples(s) Qualified:
V-06
Benzidine
B210345-BS1, B210345-BSD1
Continuing calibration did not meet method specifications and was biased on the high side. Data validation is not affected since sample result
was "not detected" for this compound.
Analyte & Samples(s) Qualified:
V-20
Benzidine
18H0706-01[SB-1], B210345-BLK1
Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this compound. Reported result is
estimated.
Analyte & Samples(s) Qualified:
V-34
3,3-Dichlorobenzidine
18H0706-01[SB-1], B210345-BLK1, B210345-BS1, B210345-BSD1
3-Nitroaniline
18H0706-01[SB-1], B210345-BLK1, B210345-BS1, B210345-BSD1
4-Chloroaniline
18H0706-01[SB-1], B210345-BLK1, B210345-BS1, B210345-BSD1
Aniline
18H0706-01[SB-1], B210345-BLK1, B210345-BS1, B210345-BSD1
Page 5 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
MADEP-EPH-04-1.1
SPE cartridge contamination with non-petroleum compounds, if present, is verified by GC/MS in each method blank per extraction batch and excluded from C 11-C22 aromatic
range fraction in all samples in the batch. No significant modifications were made to the method.
MADEP-VPH-Feb 2018 Rev 2.1
Analytical column used for VPH analysis is Restek, Rtx-502.2, 105meter, 0.53mmID, 3um df. Trap used for VPH analysis is Carbopack B/CarboSieveS-III.
No significant modifications were made to the method. All VPH samples were received preserved properly in methanol with a soil/methanol ratio of 1:1 +/- 25% completely
covered by methanol in the proper containers specified on the chain-of-custody form unless specified in this narrative.
The results of analyses reported only relate to samples submitted to the Con-Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Daren J. Damboragian
Director of Operations
Page 6 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 8/15/2018
Work Order: 18H0706Sample Description:Project Location: Haw River, NC
Sample ID: 18H0706-01
Field Sample #: SB-1
Sample Matrix: Soil
Sampled: 8/13/2018 17:00
[TOC_2]18H0706-01[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 2.8 8/15/18 12:22 MFFmg/Kg dry0.55 8/15/18SW-846 8260B1Acetone
ND 0.28 8/15/18 12:22 MFFmg/Kg dry0.033 8/15/18SW-846 8260B1Acrylonitrile
ND 0.028 8/15/18 12:22 MFFmg/Kg dry0.0060 8/15/18SW-846 8260B1tert-Amyl Methyl Ether (TAME)
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0068 8/15/18SW-846 8260B1Benzene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0085 8/15/18SW-846 8260B1Bromobenzene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.013 8/15/18SW-846 8260B1Bromochloromethane
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.017 8/15/18SW-846 8260B1Bromodichloromethane
ND 0.11 8/15/18 12:22 MFFmg/Kg dry0.012 8/15/18SW-846 8260B1Bromoform
ND 0.11 8/15/18 12:22 MFFmg/Kg dry0.054 8/15/18SW-846 8260B1Bromomethane
ND 1.1 8/15/18 12:22 MFFmg/Kg dry0.13 8/15/18SW-846 8260B12-Butanone (MEK)
ND 1.1 8/15/18 12:22 MFFmg/Kg dry0.12 8/15/18SW-846 8260B1tert-Butyl Alcohol (TBA)
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0085 8/15/18SW-846 8260B1n-Butylbenzene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0074 8/15/18SW-846 8260B1sec-Butylbenzene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0069 8/15/18SW-846 8260B1tert-Butylbenzene
ND 0.028 8/15/18 12:22 MFFmg/Kg dry0.0054 8/15/18SW-846 8260B1tert-Butyl Ethyl Ether (TBEE)
ND 0.17 8/15/18 12:22 MFFmg/Kg dry0.058 8/15/18SW-846 8260B1Carbon Disulfide
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.014 8/15/18SW-846 8260B1Carbon Tetrachloride
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0091 8/15/18SW-846 8260B1Chlorobenzene
ND 0.028 8/15/18 12:22 MFFmg/Kg dry0.0059 8/15/18SW-846 8260B1Chlorodibromomethane
ND 0.11 8/15/18 12:22 MFFmg/Kg dry0.016 8/15/18SW-846 8260B1Chloroethane
ND 0.11 8/15/18 12:22 MFFmg/Kg dry0.013 8/15/18SW-846 8260B1Chloroform
ND 0.11 8/15/18 12:22 MFFmg/Kg dry0.031 8/15/18SW-846 8260B1Chloromethane
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0068 8/15/18SW-846 8260B12-Chlorotoluene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0080 8/15/18SW-846 8260B14-Chlorotoluene
ND 0.28 8/15/18 12:22 MFFmg/Kg dry0.021 8/15/18SW-846 8260B11,2-Dibromo-3-chloropropane (DBCP)
ND 0.028 8/15/18 12:22 MFFmg/Kg dry0.0084 8/15/18SW-846 8260B11,2-Dibromoethane (EDB)
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0091 8/15/18SW-846 8260B1Dibromomethane
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0097 8/15/18SW-846 8260B11,2-Dichlorobenzene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0097 8/15/18SW-846 8260B11,3-Dichlorobenzene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0085 8/15/18SW-846 8260B11,4-Dichlorobenzene
ND 0.11 8/15/18 12:22 MFFmg/Kg dry0.018 8/15/18SW-846 8260B1trans-1,4-Dichloro-2-butene
ND 0.11 8/15/18 12:22 MFFmg/Kg dry0.016 8/15/18SW-846 8260B1Dichlorodifluoromethane (Freon 12)
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0090 8/15/18SW-846 8260B11,1-Dichloroethane
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.011 8/15/18SW-846 8260B11,2-Dichloroethane
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.012 8/15/18SW-846 8260B11,1-Dichloroethylene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0084 8/15/18SW-846 8260B1cis-1,2-Dichloroethylene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0085 8/15/18SW-846 8260B1trans-1,2-Dichloroethylene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0074 8/15/18SW-846 8260B11,2-Dichloropropane
ND 0.028 8/15/18 12:22 MFFmg/Kg dry0.0074 8/15/18SW-846 8260B11,3-Dichloropropane
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.012 8/15/18SW-846 8260B12,2-Dichloropropane
ND 0.11 8/15/18 12:22 MFFmg/Kg dry0.0073 8/15/18SW-846 8260B11,1-Dichloropropene
ND 0.028 8/15/18 12:22 MFFmg/Kg dry0.0068 8/15/18SW-846 8260B1cis-1,3-Dichloropropene
ND 0.028 8/15/18 12:22 MFFmg/Kg dry0.0064 8/15/18SW-846 8260B1trans-1,3-Dichloropropene
ND 0.11 8/15/18 12:22 MFFmg/Kg dry0.013 8/15/18SW-846 8260B1Diethyl Ether
[TOC_1]Sample Results[TOC]
Page 7 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 8/15/2018
Work Order: 18H0706Sample Description:Project Location: Haw River, NC
Sample ID: 18H0706-01
Field Sample #: SB-1
Sample Matrix: Soil
Sampled: 8/13/2018 17:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.028 8/15/18 12:22 MFFmg/Kg dry0.010 8/15/18SW-846 8260B1Diisopropyl Ether (DIPE)
ND 2.8 8/15/18 12:22 MFFmg/Kg dry1.5 8/15/18SW-846 8260B11,4-Dioxane
ND 11 8/15/18 12:22 MFFmg/Kg dry1.6 8/15/18SW-846 8260B1Ethanol
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0074 8/15/18SW-846 8260B1Ethylbenzene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.034 8/15/18SW-846 8260B1Hexachlorobutadiene
ND 0.57 8/15/18 12:22 MFFmg/Kg dry0.087 8/15/18SW-846 8260B12-Hexanone (MBK)
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0068 8/15/18SW-846 8260B1Isopropylbenzene (Cumene)
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0085 8/15/18SW-846 8260B1p-Isopropyltoluene (p-Cymene)
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0051 8/15/18SW-846 8260B1Methyl tert-Butyl Ether (MTBE)
ND 0.28 8/15/18 12:22 MFFmg/Kg dry0.18 8/15/18SW-846 8260B1Methylene Chloride
ND 0.57 8/15/18 12:22 MFFmg/Kg dry0.084 8/15/18SW-846 8260B14-Methyl-2-pentanone (MIBK)
ND 0.11 8/15/18 12:22 MFFmg/Kg dry0.0069 8/15/18SW-846 8260B1Naphthalene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0074 8/15/18SW-846 8260B1n-Propylbenzene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0085 8/15/18SW-846 8260B1Styrene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0068 8/15/18SW-846 8260B11,1,1,2-Tetrachloroethane
ND 0.028 8/15/18 12:22 MFFmg/Kg dry0.0091 8/15/18SW-846 8260B11,1,2,2-Tetrachloroethane
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.015 8/15/18SW-846 8260B1Tetrachloroethylene
ND 0.57 8/15/18 12:22 MFFmg/Kg dry0.061 8/15/18SW-846 8260B1Tetrahydrofuran
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0097 8/15/18SW-846 8260B1Toluene
ND 0.28 8/15/18 12:22 MFFmg/Kg dry0.0080 8/15/18SW-846 8260B11,2,3-Trichlorobenzene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.011 8/15/18SW-846 8260B11,2,4-Trichlorobenzene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0097 8/15/18SW-846 8260B11,3,5-Trichlorobenzene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0075 8/15/18SW-846 8260B11,1,1-Trichloroethane
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.013 8/15/18SW-846 8260B11,1,2-Trichloroethane
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.011 8/15/18SW-846 8260B1Trichloroethylene
ND 0.11 8/15/18 12:22 MFFmg/Kg dry0.0084 8/15/18SW-846 8260B1Trichlorofluoromethane (Freon 11)
ND 0.11 8/15/18 12:22 MFFmg/Kg dry0.012 8/15/18SW-846 8260B11,2,3-Trichloropropane
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.011 8/15/18SW-846 8260B11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.010 8/15/18SW-846 8260B11,2,4-Trimethylbenzene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0074 8/15/18SW-846 8260B11,3,5-Trimethylbenzene
ND 0.11 8/15/18 12:22 MFFmg/Kg dry0.0076 8/15/18SW-846 8260B1Vinyl Chloride
ND 0.11 8/15/18 12:22 MFFmg/Kg dry0.015 8/15/18SW-846 8260B1m+p Xylene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0075 8/15/18SW-846 8260B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 91.2 8/15/18 12:2270-130
Toluene-d8 97.7 8/15/18 12:2270-130
4-Bromofluorobenzene 102 8/15/18 12:2270-130
Page 8 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 8/15/2018
Work Order: 18H0706Sample Description:Project Location: Haw River, NC
Sample ID: 18H0706-01
Field Sample #: SB-1
Sample Matrix: Soil
Sampled: 8/13/2018 17:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.059 8/15/18SW-846 8270D1Acenaphthene
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.066 8/15/18SW-846 8270D1Acenaphthylene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.077 8/15/18SW-846 8270D1Acetophenone
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.11 8/15/18SW-846 8270D1V-34Aniline
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.057 8/15/18SW-846 8270D1Anthracene
ND 0.76 8/15/18 15:01 CDTmg/Kg dry0.49 8/15/18SW-846 8270D1V-04, V-20Benzidine
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.052 8/15/18SW-846 8270D1Benzo(a)anthracene
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.061 8/15/18SW-846 8270D1Benzo(a)pyrene
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.055 8/15/18SW-846 8270D1Benzo(b)fluoranthene
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.087 8/15/18SW-846 8270D1Benzo(g,h,i)perylene
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.061 8/15/18SW-846 8270D1Benzo(k)fluoranthene
ND 1.2 8/15/18 15:01 CDTmg/Kg dry0.21 8/15/18SW-846 8270D1Benzoic Acid
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.075 8/15/18SW-846 8270D1Bis(2-chloroethoxy)methane
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.077 8/15/18SW-846 8270D1Bis(2-chloroethyl)ether
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.084 8/15/18SW-846 8270D1Bis(2-chloroisopropyl)ether
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.15 8/15/18SW-846 8270D1Bis(2-Ethylhexyl)phthalate
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.066 8/15/18SW-846 8270D14-Bromophenylphenylether
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.094 8/15/18SW-846 8270D1Butylbenzylphthalate
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.051 8/15/18SW-846 8270D1Carbazole
ND 0.76 8/15/18 15:01 CDTmg/Kg dry0.090 8/15/18SW-846 8270D1V-344-Chloroaniline
ND 0.76 8/15/18 15:01 CDTmg/Kg dry0.084 8/15/18SW-846 8270D14-Chloro-3-methylphenol
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.074 8/15/18SW-846 8270D12-Chloronaphthalene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.070 8/15/18SW-846 8270D12-Chlorophenol
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.066 8/15/18SW-846 8270D14-Chlorophenylphenylether
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.061 8/15/18SW-846 8270D1Chrysene
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.12 8/15/18SW-846 8270D1Dibenz(a,h)anthracene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.068 8/15/18SW-846 8270D1Dibenzofuran
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.085 8/15/18SW-846 8270D1Di-n-butylphthalate
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.069 8/15/18SW-846 8270D11,2-Dichlorobenzene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.067 8/15/18SW-846 8270D11,3-Dichlorobenzene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.070 8/15/18SW-846 8270D11,4-Dichlorobenzene
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.060 8/15/18SW-846 8270D1V-343,3-Dichlorobenzidine
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.067 8/15/18SW-846 8270D12,4-Dichlorophenol
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.070 8/15/18SW-846 8270D1Diethylphthalate
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.073 8/15/18SW-846 8270D12,4-Dimethylphenol
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.069 8/15/18SW-846 8270D1Dimethylphthalate
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.37 8/15/18SW-846 8270D14,6-Dinitro-2-methylphenol
ND 0.76 8/15/18 15:01 CDTmg/Kg dry0.22 8/15/18SW-846 8270D12,4-Dinitrophenol
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.064 8/15/18SW-846 8270D12,4-Dinitrotoluene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.069 8/15/18SW-846 8270D12,6-Dinitrotoluene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.21 8/15/18SW-846 8270D1Di-n-octylphthalate
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.064 8/15/18SW-846 8270D11,2-Diphenylhydrazine (as Azobenzene)
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.065 8/15/18SW-846 8270D1Fluoranthene
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.064 8/15/18SW-846 8270D1Fluorene
Page 9 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 8/15/2018
Work Order: 18H0706Sample Description:Project Location: Haw River, NC
Sample ID: 18H0706-01
Field Sample #: SB-1
Sample Matrix: Soil
Sampled: 8/13/2018 17:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.069 8/15/18SW-846 8270D1Hexachlorobenzene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.069 8/15/18SW-846 8270D1Hexachlorobutadiene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.083 8/15/18SW-846 8270D1V-05Hexachlorocyclopentadiene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.079 8/15/18SW-846 8270D1Hexachloroethane
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.14 8/15/18SW-846 8270D1Indeno(1,2,3-cd)pyrene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.076 8/15/18SW-846 8270D1Isophorone
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.075 8/15/18SW-846 8270D11-Methylnaphthalene
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.068 8/15/18SW-846 8270D12-Methylnaphthalene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.098 8/15/18SW-846 8270D12-Methylphenol
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.12 8/15/18SW-846 8270D13/4-Methylphenol
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.10 8/15/18SW-846 8270D1Naphthalene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.066 8/15/18SW-846 8270D12-Nitroaniline
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.057 8/15/18SW-846 8270D1V-343-Nitroaniline
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.066 8/15/18SW-846 8270D14-Nitroaniline
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.074 8/15/18SW-846 8270D1Nitrobenzene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.10 8/15/18SW-846 8270D12-Nitrophenol
ND 0.76 8/15/18 15:01 CDTmg/Kg dry0.085 8/15/18SW-846 8270D14-Nitrophenol
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.25 8/15/18SW-846 8270D1N-Nitrosodimethylamine
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.081 8/15/18SW-846 8270D1N-Nitrosodiphenylamine
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.081 8/15/18SW-846 8270D1N-Nitrosodi-n-propylamine
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.094 8/15/18SW-846 8270D1Pentachloronitrobenzene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.095 8/15/18SW-846 8270D1Pentachlorophenol
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.10 8/15/18SW-846 8270D1Phenanthrene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.067 8/15/18SW-846 8270D1Phenol
0.080 0.20 8/15/18 15:01 CDTmg/Kg dry0.065 8/15/18SW-846 8270D1JPyrene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.064 8/15/18SW-846 8270D1Pyridine
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.070 8/15/18SW-846 8270D11,2,4,5-Tetrachlorobenzene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.070 8/15/18SW-846 8270D11,2,4-Trichlorobenzene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.089 8/15/18SW-846 8270D12,4,5-Trichlorophenol
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.066 8/15/18SW-846 8270D12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 63.7 8/15/18 15:0130-130
Phenol-d6 64.5 8/15/18 15:0130-130
Nitrobenzene-d5 63.4 8/15/18 15:0130-130
2-Fluorobiphenyl 72.7 8/15/18 15:0130-130
2,4,6-Tribromophenol 62.0 8/15/18 15:0130-130
p-Terphenyl-d14 76.4 8/15/18 15:0130-130
Page 10 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 8/15/2018
Work Order: 18H0706Sample Description:Project Location: Haw River, NC
Sample ID: 18H0706-01
Field Sample #: SB-1
Sample Matrix: Soil
Sampled: 8/13/2018 17:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - EPH
380 58 8/16/18 9:36 RMWmg/Kg dry 8/15/18MADEP-EPH-04-1.15C9-C18 Aliphatics
130 12 8/16/18 4:45 RMWmg/Kg dry 8/15/18MADEP-EPH-04-1.11C19-C36 Aliphatics
160 12 8/16/18 4:45 RMWmg/Kg dry 8/15/18MADEP-EPH-04-1.11Unadjusted C11-C22 Aromatics
160 12 8/16/18 4:45 RMWmg/Kg dry 8/15/18MADEP-EPH-04-1.11C11-C22 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD)74.5 8/16/18 4:4540-140
o-Terphenyl (OTP)74.4 8/16/18 4:4540-140
2-Bromonaphthalene 94.2 8/16/18 4:4540-140
2-Fluorobiphenyl 81.0 8/16/18 4:4540-140
Page 11 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 8/15/2018
Work Order: 18H0706Sample Description:Project Location: Haw River, NC
Sample ID: 18H0706-01
Field Sample #: SB-1
Sample Matrix: Soil
Sampled: 8/13/2018 17:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Soil/Methanol Preservation Ratio: 1.17
Petroleum Hydrocarbons Analyses - VPH
ND 11 8/15/18 11:27 EEHmg/Kg dry 8/15/18MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 11 8/15/18 11:27 EEHmg/Kg dry 8/15/18MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
59 11 8/15/18 11:27 EEHmg/Kg dry 8/15/18MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
26 11 8/15/18 11:27 EEHmg/Kg dry 8/15/18MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
33 11 8/15/18 11:27 EEHmg/Kg dry 8/15/18MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)80.4 8/15/18 11:2770-130
2,5-Dibromotoluene (PID)80.1 8/15/18 11:2770-130
Page 12 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 8/15/2018
Work Order: 18H0706Sample Description:Project Location: Haw River, NC
Sample ID: 18H0706-01
Field Sample #: SB-1
Sample Matrix: Soil
Sampled: 8/13/2018 17:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
86.3 8/15/18 17:56 JFC% Wt 8/15/18SM 2540G1% Solids
Page 13 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: SW-846 3546-MADEP-EPH-04-1.1
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B210344 08/15/1820.0 2.0018H0706-01 [SB-1]
Prep Method: MA VPH-MADEP-VPH-Feb 2018 Rev 2.1
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B209997 08/15/185.90 5.8018H0706-01 [SB-1]
Prep Method: % Solids-SM 2540G
Lab Number [Field ID]Batch Date
B210372 08/15/1818H0706-01 [SB-1]
Prep Method: SW-846 5035/5030B-SW-846 8260B
Lab Number [Field ID]Batch
Sample
Amount(g)
Methanol
Volume(mL)
Methanol
Aliquot(mL)
Final
Volume(mL)Date
18H0706-01 [SB-1]B210357 5.90 5.80 1 50 08/15/18
Prep Method: SW-846 3546-SW-846 8270D
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B210345 08/15/1830.1 1.0018H0706-01 [SB-1]
[TOC_1]Sample Preparation Information[TOC]
Page 14 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Volatile Organic Compounds by GC/MS[TOC]
Batch B210357 - SW-846 5035/5030B
[TOC_3]B210357[TOC]
Blank (B210357-BLK1) Prepared & Analyzed: 08/15/18
Acetone mg/Kg wet2.5ND
Acrylonitrile mg/Kg wet0.25ND
tert-Amyl Methyl Ether (TAME)mg/Kg wet0.025ND
Benzene mg/Kg wet0.050ND
Bromobenzene mg/Kg wet0.050ND
Bromochloromethane mg/Kg wet0.050ND
Bromodichloromethane mg/Kg wet0.050ND
Bromoform mg/Kg wet0.10ND
Bromomethane mg/Kg wet0.10ND
2-Butanone (MEK)mg/Kg wet1.0ND
tert-Butyl Alcohol (TBA)mg/Kg wet1.0ND
n-Butylbenzene mg/Kg wet0.050ND
sec-Butylbenzene mg/Kg wet0.050ND
tert-Butylbenzene mg/Kg wet0.050ND
tert-Butyl Ethyl Ether (TBEE)mg/Kg wet0.025ND
Carbon Disulfide mg/Kg wet0.15ND
Carbon Tetrachloride mg/Kg wet0.050ND
Chlorobenzene mg/Kg wet0.050ND
Chlorodibromomethane mg/Kg wet0.025ND
Chloroethane mg/Kg wet0.10ND
Chloroform mg/Kg wet0.10ND
Chloromethane mg/Kg wet0.10ND
2-Chlorotoluene mg/Kg wet0.050ND
4-Chlorotoluene mg/Kg wet0.050ND
1,2-Dibromo-3-chloropropane (DBCP)mg/Kg wet0.25ND
1,2-Dibromoethane (EDB)mg/Kg wet0.025ND
Dibromomethane mg/Kg wet0.050ND
1,2-Dichlorobenzene mg/Kg wet0.050ND
1,3-Dichlorobenzene mg/Kg wet0.050ND
1,4-Dichlorobenzene mg/Kg wet0.050ND
trans-1,4-Dichloro-2-butene mg/Kg wet0.10ND
Dichlorodifluoromethane (Freon 12)mg/Kg wet0.10ND
1,1-Dichloroethane mg/Kg wet0.050ND
1,2-Dichloroethane mg/Kg wet0.050ND
1,1-Dichloroethylene mg/Kg wet0.050ND
cis-1,2-Dichloroethylene mg/Kg wet0.050ND
trans-1,2-Dichloroethylene mg/Kg wet0.050ND
1,2-Dichloropropane mg/Kg wet0.050ND
1,3-Dichloropropane mg/Kg wet0.025ND
2,2-Dichloropropane mg/Kg wet0.050ND
1,1-Dichloropropene mg/Kg wet0.10ND
cis-1,3-Dichloropropene mg/Kg wet0.025ND
trans-1,3-Dichloropropene mg/Kg wet0.025ND
Diethyl Ether mg/Kg wet0.10ND
Diisopropyl Ether (DIPE)mg/Kg wet0.025ND
1,4-Dioxane mg/Kg wet2.5ND
Ethanol mg/Kg wet0.20ND
Ethylbenzene mg/Kg wet0.050ND
Hexachlorobutadiene mg/Kg wet0.050ND
2-Hexanone (MBK)mg/Kg wet0.50ND
Isopropylbenzene (Cumene)mg/Kg wet0.050ND
p-Isopropyltoluene (p-Cymene)mg/Kg wet0.050ND
[TOC_1]QC Data[TOC]
Page 15 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B210357 - SW-846 5035/5030B
Blank (B210357-BLK1) Prepared & Analyzed: 08/15/18
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.050ND
Methylene Chloride mg/Kg wet0.25ND
4-Methyl-2-pentanone (MIBK)mg/Kg wet0.50ND
Naphthalene mg/Kg wet0.10ND
n-Propylbenzene mg/Kg wet0.050ND
Styrene mg/Kg wet0.050ND
1,1,1,2-Tetrachloroethane mg/Kg wet0.050ND
1,1,2,2-Tetrachloroethane mg/Kg wet0.025ND
Tetrachloroethylene mg/Kg wet0.050ND
Tetrahydrofuran mg/Kg wet0.50ND
Toluene mg/Kg wet0.050ND
1,2,3-Trichlorobenzene mg/Kg wet0.25ND
1,2,4-Trichlorobenzene mg/Kg wet0.050ND
1,3,5-Trichlorobenzene mg/Kg wet0.050ND
1,1,1-Trichloroethane mg/Kg wet0.050ND
1,1,2-Trichloroethane mg/Kg wet0.050ND
Trichloroethylene mg/Kg wet0.050ND
Trichlorofluoromethane (Freon 11)mg/Kg wet0.10ND
1,2,3-Trichloropropane mg/Kg wet0.10ND
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
mg/Kg wet0.050ND
1,2,4-Trimethylbenzene mg/Kg wet0.050ND
1,3,5-Trimethylbenzene mg/Kg wet0.050ND
Vinyl Chloride mg/Kg wet0.10ND
m+p Xylene mg/Kg wet0.10ND
o-Xylene mg/Kg wet0.050ND
mg/Kg wet 0.0250 70-130Surrogate: 1,2-Dichloroethane-d4 89.00.0222
mg/Kg wet 0.0250 70-130Surrogate: Toluene-d8 97.20.0243
mg/Kg wet 0.0250 70-130Surrogate: 4-Bromofluorobenzene 95.60.0239
LCS (B210357-BS1) Prepared & Analyzed: 08/15/18
Acetone mg/Kg wet0.057 0.113 70-16091.40.104
Acrylonitrile mg/Kg wet0.0057 0.0113 70-13086.70.00983
tert-Amyl Methyl Ether (TAME)mg/Kg wet0.00057 0.0113 70-13089.50.0101
Benzene mg/Kg wet0.0011 0.0113 70-13092.90.0105
Bromobenzene mg/Kg wet0.0011 0.0113 70-13098.20.0111
Bromochloromethane mg/Kg wet0.0011 0.0113 70-13095.80.0109
Bromodichloromethane mg/Kg wet0.0011 0.0113 70-13097.20.0110
Bromoform mg/Kg wet0.0023 0.0113 70-1301000.0113
Bromomethane mg/Kg wet0.0023 0.0113 40-13087.80.00995
2-Butanone (MEK)mg/Kg wet0.023 0.113 70-16077.10.0874
tert-Butyl Alcohol (TBA)mg/Kg wet0.023 0.113 40-13098.40.112
n-Butylbenzene mg/Kg wet0.0011 0.0113 70-1301030.0116
sec-Butylbenzene mg/Kg wet0.0011 0.0113 70-1301060.0120
tert-Butylbenzene mg/Kg wet0.0011 0.0113 70-1601030.0117
tert-Butyl Ethyl Ether (TBEE)mg/Kg wet0.00057 0.0113 70-13080.90.00917
Carbon Disulfide mg/Kg wet0.0034 0.0113 70-1301130.0128
Carbon Tetrachloride mg/Kg wet0.0011 0.0113 70-13091.60.0104
Chlorobenzene mg/Kg wet0.0011 0.0113 70-1301020.0115
Chlorodibromomethane mg/Kg wet0.00057 0.0113 70-1301030.0117
Chloroethane mg/Kg wet0.0023 0.0113 70-13093.90.0106
Chloroform mg/Kg wet0.0023 0.0113 70-13098.60.0112
Chloromethane mg/Kg wet0.0023 0.0113 70-13074.90.00849
Page 16 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B210357 - SW-846 5035/5030B
LCS (B210357-BS1) Prepared & Analyzed: 08/15/18
2-Chlorotoluene mg/Kg wet0.0011 0.0113 70-1301000.0113
4-Chlorotoluene mg/Kg wet0.0011 0.0113 70-13099.40.0113
1,2-Dibromo-3-chloropropane (DBCP)mg/Kg wet0.0057 0.0113 70-13097.90.0111
1,2-Dibromoethane (EDB)mg/Kg wet0.00057 0.0113 70-1301050.0119
Dibromomethane mg/Kg wet0.0011 0.0113 70-1301050.0119
1,2-Dichlorobenzene mg/Kg wet0.0011 0.0113 70-1301030.0117
1,3-Dichlorobenzene mg/Kg wet0.0011 0.0113 70-1301070.0121
1,4-Dichlorobenzene mg/Kg wet0.0011 0.0113 70-13098.60.0112
trans-1,4-Dichloro-2-butene mg/Kg wet0.0023 0.0113 70-13082.90.00940
Dichlorodifluoromethane (Freon 12)mg/Kg wet0.0023 0.0113 40-16084.00.00952
1,1-Dichloroethane mg/Kg wet0.0011 0.0113 70-13092.20.0104
1,2-Dichloroethane mg/Kg wet0.0011 0.0113 70-13088.20.0100
1,1-Dichloroethylene mg/Kg wet0.0011 0.0113 70-1301010.0115
cis-1,2-Dichloroethylene mg/Kg wet0.0011 0.0113 70-13087.30.00989
trans-1,2-Dichloroethylene mg/Kg wet0.0011 0.0113 70-13091.50.0104
1,2-Dichloropropane mg/Kg wet0.0011 0.0113 70-13095.90.0109
1,3-Dichloropropane mg/Kg wet0.00057 0.0113 70-13087.80.00995
2,2-Dichloropropane mg/Kg wet0.0011 0.0113 70-13083.40.00945
1,1-Dichloropropene mg/Kg wet0.0023 0.0113 70-13089.10.0101
cis-1,3-Dichloropropene mg/Kg wet0.00057 0.0113 70-13093.00.0105
trans-1,3-Dichloropropene mg/Kg wet0.00057 0.0113 70-13093.90.0106
Diethyl Ether mg/Kg wet0.0023 0.0113 70-13094.90.0108
Diisopropyl Ether (DIPE)mg/Kg wet0.00057 0.0113 70-13075.80.00859
1,4-Dioxane mg/Kg wet0.057 0.113 40-16098.00.111
Ethylbenzene mg/Kg wet0.0011 0.0113 70-1301040.0118
Hexachlorobutadiene mg/Kg wet0.0011 0.0113 70-1601120.0127
2-Hexanone (MBK)mg/Kg wet0.011 0.113 70-16083.10.0942
Isopropylbenzene (Cumene)mg/Kg wet0.0011 0.0113 70-1301100.0125
p-Isopropyltoluene (p-Cymene)mg/Kg wet0.0011 0.0113 70-1301050.0119
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.0011 0.0113 70-13096.20.0109
Methylene Chloride mg/Kg wet0.0057 0.0113 40-16090.20.0102
4-Methyl-2-pentanone (MIBK)mg/Kg wet0.011 0.113 70-16082.50.0935
Naphthalene mg/Kg wet0.0023 0.0113 40-1301040.0118
n-Propylbenzene mg/Kg wet0.0011 0.0113 70-1301030.0117
Styrene mg/Kg wet0.0011 0.0113 70-1301040.0118
1,1,1,2-Tetrachloroethane mg/Kg wet0.0011 0.0113 70-1301090.0124
1,1,2,2-Tetrachloroethane mg/Kg wet0.00057 0.0113 70-1301050.0119
Tetrachloroethylene mg/Kg wet0.0011 0.0113 70-1301050.0119
Tetrahydrofuran mg/Kg wet0.011 0.0113 J70-13078.90.00894
Toluene mg/Kg wet0.0011 0.0113 70-1301020.0116
1,2,3-Trichlorobenzene mg/Kg wet0.0057 0.0113 70-1301040.0118
1,2,4-Trichlorobenzene mg/Kg wet0.0011 0.0113 70-13099.60.0113
1,3,5-Trichlorobenzene mg/Kg wet0.0011 0.0113 70-13099.90.0113
1,1,1-Trichloroethane mg/Kg wet0.0011 0.0113 70-13098.40.0112
1,1,2-Trichloroethane mg/Kg wet0.0011 0.0113 70-1301040.0117
Trichloroethylene mg/Kg wet0.0011 0.0113 70-1301020.0116
Trichlorofluoromethane (Freon 11)mg/Kg wet0.0023 0.0113 70-13099.00.0112
1,2,3-Trichloropropane mg/Kg wet0.0023 0.0113 70-13075.90.00860
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
mg/Kg wet0.0011 0.0113 70-1301120.0127
1,2,4-Trimethylbenzene mg/Kg wet0.0011 0.0113 70-13098.60.0112
1,3,5-Trimethylbenzene mg/Kg wet0.0011 0.0113 70-13099.80.0113
Page 17 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B210357 - SW-846 5035/5030B
LCS (B210357-BS1) Prepared & Analyzed: 08/15/18
Vinyl Chloride mg/Kg wet0.0023 0.0113 40-13086.80.00984
m+p Xylene mg/Kg wet0.0023 0.0227 70-1301010.0230
o-Xylene mg/Kg wet0.0011 0.0113 70-1301020.0115
mg/Kg wet 0.0283 70-130Surrogate: 1,2-Dichloroethane-d4 89.00.0252
mg/Kg wet 0.0283 70-130Surrogate: Toluene-d8 99.70.0283
mg/Kg wet 0.0283 70-130Surrogate: 4-Bromofluorobenzene 96.90.0274
LCS Dup (B210357-BSD1) Prepared & Analyzed: 08/15/18
Acetone mg/Kg wet0.057 0.113 2570-16089.9 1.620.102
Acrylonitrile mg/Kg wet0.0057 0.0113 2570-13081.4 6.310.00923
tert-Amyl Methyl Ether (TAME)mg/Kg wet0.00057 0.0113 2570-13088.5 1.120.0100
Benzene mg/Kg wet0.0011 0.0113 2570-13092.3 0.6480.0105
Bromobenzene mg/Kg wet0.0011 0.0113 2570-13099.5 1.320.0113
Bromochloromethane mg/Kg wet0.0011 0.0113 2570-13095.3 0.5230.0108
Bromodichloromethane mg/Kg wet0.0011 0.0113 2570-13094.6 2.710.0107
Bromoform mg/Kg wet0.0023 0.0113 2570-130104 3.730.0118
Bromomethane mg/Kg wet0.0023 0.0113 2540-130104 16.70.0118
2-Butanone (MEK)mg/Kg wet0.023 0.113 2570-16074.6 3.340.0845
tert-Butyl Alcohol (TBA)mg/Kg wet0.023 0.113 2540-13090.3 8.640.102
n-Butylbenzene mg/Kg wet0.0011 0.0113 2570-130102 0.1950.0116
sec-Butylbenzene mg/Kg wet0.0011 0.0113 2570-130105 0.7610.0119
tert-Butylbenzene mg/Kg wet0.0011 0.0113 2570-160101 2.550.0114
tert-Butyl Ethyl Ether (TBEE)mg/Kg wet0.00057 0.0113 2570-13080.9 0.000.00917
Carbon Disulfide mg/Kg wet0.0034 0.0113 2570-130105 7.890.0119
Carbon Tetrachloride mg/Kg wet0.0011 0.0113 2570-13090.3 1.430.0102
Chlorobenzene mg/Kg wet0.0011 0.0113 2570-130103 0.9800.0116
Chlorodibromomethane mg/Kg wet0.00057 0.0113 2570-130103 0.1950.0116
Chloroethane mg/Kg wet0.0023 0.0113 2570-13091.6 2.480.0104
Chloroform mg/Kg wet0.0023 0.0113 2570-13098.2 0.4070.0111
Chloromethane mg/Kg wet0.0023 0.0113 2570-13073.8 1.480.00836
2-Chlorotoluene mg/Kg wet0.0011 0.0113 2570-13097.2 2.840.0110
4-Chlorotoluene mg/Kg wet0.0011 0.0113 2570-13097.4 2.030.0110
1,2-Dibromo-3-chloropropane (DBCP)mg/Kg wet0.0057 0.0113 2570-13087.0 11.80.00986
1,2-Dibromoethane (EDB)mg/Kg wet0.00057 0.0113 2570-130100 4.960.0114
Dibromomethane mg/Kg wet0.0011 0.0113 2570-130105 0.4750.0119
1,2-Dichlorobenzene mg/Kg wet0.0011 0.0113 2570-130102 1.070.0115
1,3-Dichlorobenzene mg/Kg wet0.0011 0.0113 2570-130107 0.09360.0121
1,4-Dichlorobenzene mg/Kg wet0.0011 0.0113 2570-13096.8 1.840.0110
trans-1,4-Dichloro-2-butene mg/Kg wet0.0023 0.0113 2570-13078.2 5.830.00886
Dichlorodifluoromethane (Freon 12)mg/Kg wet0.0023 0.0113 2540-16084.9 1.070.00962
1,1-Dichloroethane mg/Kg wet0.0011 0.0113 2570-13091.4 0.8710.0104
1,2-Dichloroethane mg/Kg wet0.0011 0.0113 2570-13088.9 0.7900.0101
1,1-Dichloroethylene mg/Kg wet0.0011 0.0113 2570-13098.0 3.210.0111
cis-1,2-Dichloroethylene mg/Kg wet0.0011 0.0113 2570-13085.4 2.200.00968
trans-1,2-Dichloroethylene mg/Kg wet0.0011 0.0113 2570-13090.1 1.540.0102
1,2-Dichloropropane mg/Kg wet0.0011 0.0113 2570-13094.2 1.790.0107
1,3-Dichloropropane mg/Kg wet0.00057 0.0113 2570-13089.6 2.030.0102
2,2-Dichloropropane mg/Kg wet0.0011 0.0113 2570-13081.7 2.060.00926
1,1-Dichloropropene mg/Kg wet0.0023 0.0113 2570-13090.2 1.230.0102
cis-1,3-Dichloropropene mg/Kg wet0.00057 0.0113 2570-13091.4 1.740.0104
trans-1,3-Dichloropropene mg/Kg wet0.00057 0.0113 2570-13093.4 0.5340.0106
Diethyl Ether mg/Kg wet0.0023 0.0113 2570-13093.5 1.490.0106
Page 18 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B210357 - SW-846 5035/5030B
LCS Dup (B210357-BSD1) Prepared & Analyzed: 08/15/18
Diisopropyl Ether (DIPE)mg/Kg wet0.00057 0.0113 2570-13075.3 0.6620.00853
1,4-Dioxane mg/Kg wet0.057 0.113 5040-16093.2 5.040.106
Ethylbenzene mg/Kg wet0.0011 0.0113 2570-130106 1.810.0120
Hexachlorobutadiene mg/Kg wet0.0011 0.0113 2570-160109 2.630.0123
2-Hexanone (MBK)mg/Kg wet0.011 0.113 2570-16079.4 4.620.0900
Isopropylbenzene (Cumene)mg/Kg wet0.0011 0.0113 2570-130110 0.2720.0125
p-Isopropyltoluene (p-Cymene)mg/Kg wet0.0011 0.0113 2570-130104 1.150.0117
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.0011 0.0113 2570-13094.7 1.570.0107
Methylene Chloride mg/Kg wet0.0057 0.0113 2540-16089.7 0.5560.0102
4-Methyl-2-pentanone (MIBK)mg/Kg wet0.011 0.113 2570-16080.5 2.450.0913
Naphthalene mg/Kg wet0.0023 0.0113 2540-130102 1.840.0116
n-Propylbenzene mg/Kg wet0.0011 0.0113 2570-130101 1.960.0114
Styrene mg/Kg wet0.0011 0.0113 2570-130106 1.530.0120
1,1,1,2-Tetrachloroethane mg/Kg wet0.0011 0.0113 2570-130103 6.040.0117
1,1,2,2-Tetrachloroethane mg/Kg wet0.00057 0.0113 2570-130104 0.6680.0118
Tetrachloroethylene mg/Kg wet0.0011 0.0113 2570-130107 1.510.0121
Tetrahydrofuran mg/Kg wet0.011 0.0113 25 J70-13072.4 8.590.00821
Toluene mg/Kg wet0.0011 0.0113 2570-130101 1.380.0114
1,2,3-Trichlorobenzene mg/Kg wet0.0057 0.0113 2570-130104 0.09600.0118
1,2,4-Trichlorobenzene mg/Kg wet0.0011 0.0113 2570-130101 1.490.0115
1,3,5-Trichlorobenzene mg/Kg wet0.0011 0.0113 2570-13097.2 2.740.0110
1,1,1-Trichloroethane mg/Kg wet0.0011 0.0113 2570-13097.5 0.9190.0110
1,1,2-Trichloroethane mg/Kg wet0.0011 0.0113 2570-130105 1.250.0119
Trichloroethylene mg/Kg wet0.0011 0.0113 2570-13099.9 2.180.0113
Trichlorofluoromethane (Freon 11)mg/Kg wet0.0023 0.0113 2570-13096.4 2.660.0109
1,2,3-Trichloropropane mg/Kg wet0.0023 0.0113 2570-13077.8 2.470.00882
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
mg/Kg wet0.0011 0.0113 2570-130107 4.830.0121
1,2,4-Trimethylbenzene mg/Kg wet0.0011 0.0113 2570-13096.7 1.950.0110
1,3,5-Trimethylbenzene mg/Kg wet0.0011 0.0113 2570-13098.7 1.110.0112
Vinyl Chloride mg/Kg wet0.0023 0.0113 2540-13085.9 1.040.00974
m+p Xylene mg/Kg wet0.0023 0.0227 2570-130102 0.2460.0231
o-Xylene mg/Kg wet0.0011 0.0113 2570-130102 0.1960.0116
mg/Kg wet 0.0283 70-130Surrogate: 1,2-Dichloroethane-d4 88.90.0252
mg/Kg wet 0.0283 70-130Surrogate: Toluene-d8 98.80.0280
mg/Kg wet 0.0283 70-130Surrogate: 4-Bromofluorobenzene 96.50.0273
Page 19 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Semivolatile Organic Compounds by GC/MS[TOC]
Batch B210345 - SW-846 3546
[TOC_3]B210345[TOC]
Blank (B210345-BLK1) Prepared & Analyzed: 08/15/18
Acenaphthene mg/Kg wet0.17ND
Acenaphthylene mg/Kg wet0.17ND
Acetophenone mg/Kg wet0.34ND
Aniline mg/Kg wet0.34 V-34ND
Anthracene mg/Kg wet0.17ND
Benzidine mg/Kg wet0.66 V-04, V-20ND
Benzo(a)anthracene mg/Kg wet0.17ND
Benzo(a)pyrene mg/Kg wet0.17ND
Benzo(b)fluoranthene mg/Kg wet0.17ND
Benzo(g,h,i)perylene mg/Kg wet0.17ND
Benzo(k)fluoranthene mg/Kg wet0.17ND
Benzoic Acid mg/Kg wet1.0ND
Bis(2-chloroethoxy)methane mg/Kg wet0.34ND
Bis(2-chloroethyl)ether mg/Kg wet0.34ND
Bis(2-chloroisopropyl)ether mg/Kg wet0.34ND
Bis(2-Ethylhexyl)phthalate mg/Kg wet0.34ND
4-Bromophenylphenylether mg/Kg wet0.34ND
Butylbenzylphthalate mg/Kg wet0.34ND
Carbazole mg/Kg wet0.17ND
4-Chloroaniline mg/Kg wet0.66 V-34ND
4-Chloro-3-methylphenol mg/Kg wet0.66ND
2-Chloronaphthalene mg/Kg wet0.34ND
2-Chlorophenol mg/Kg wet0.34ND
4-Chlorophenylphenylether mg/Kg wet0.34ND
Chrysene mg/Kg wet0.17ND
Dibenz(a,h)anthracene mg/Kg wet0.17ND
Dibenzofuran mg/Kg wet0.34ND
Di-n-butylphthalate mg/Kg wet0.34ND
1,2-Dichlorobenzene mg/Kg wet0.34ND
1,3-Dichlorobenzene mg/Kg wet0.34ND
1,4-Dichlorobenzene mg/Kg wet0.34ND
3,3-Dichlorobenzidine mg/Kg wet0.17 V-34ND
2,4-Dichlorophenol mg/Kg wet0.34ND
Diethylphthalate mg/Kg wet0.34ND
2,4-Dimethylphenol mg/Kg wet0.34ND
Dimethylphthalate mg/Kg wet0.34ND
4,6-Dinitro-2-methylphenol mg/Kg wet0.34ND
2,4-Dinitrophenol mg/Kg wet0.66ND
2,4-Dinitrotoluene mg/Kg wet0.34ND
2,6-Dinitrotoluene mg/Kg wet0.34ND
Di-n-octylphthalate mg/Kg wet0.34ND
1,2-Diphenylhydrazine (as Azobenzene)mg/Kg wet0.34ND
Fluoranthene mg/Kg wet0.17ND
Fluorene mg/Kg wet0.17ND
Hexachlorobenzene mg/Kg wet0.34ND
Hexachlorobutadiene mg/Kg wet0.34ND
Hexachlorocyclopentadiene mg/Kg wet0.34 V-05ND
Hexachloroethane mg/Kg wet0.34ND
Indeno(1,2,3-cd)pyrene mg/Kg wet0.17ND
Isophorone mg/Kg wet0.34ND
1-Methylnaphthalene mg/Kg wet0.17ND
2-Methylnaphthalene mg/Kg wet0.17ND
Page 20 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B210345 - SW-846 3546
Blank (B210345-BLK1) Prepared & Analyzed: 08/15/18
2-Methylphenol mg/Kg wet0.34ND
3/4-Methylphenol mg/Kg wet0.34ND
Naphthalene mg/Kg wet0.17ND
2-Nitroaniline mg/Kg wet0.34ND
3-Nitroaniline mg/Kg wet0.34 V-34ND
4-Nitroaniline mg/Kg wet0.34ND
Nitrobenzene mg/Kg wet0.34ND
2-Nitrophenol mg/Kg wet0.34ND
4-Nitrophenol mg/Kg wet0.66ND
N-Nitrosodimethylamine mg/Kg wet0.34ND
N-Nitrosodiphenylamine mg/Kg wet0.34ND
N-Nitrosodi-n-propylamine mg/Kg wet0.34ND
Pentachloronitrobenzene mg/Kg wet0.34ND
Pentachlorophenol mg/Kg wet0.34ND
Phenanthrene mg/Kg wet0.17ND
Phenol mg/Kg wet0.34ND
Pyrene mg/Kg wet0.17ND
Pyridine mg/Kg wet0.34ND
1,2,4,5-Tetrachlorobenzene mg/Kg wet0.34ND
1,2,4-Trichlorobenzene mg/Kg wet0.34ND
2,4,5-Trichlorophenol mg/Kg wet0.34ND
2,4,6-Trichlorophenol mg/Kg wet0.34ND
mg/Kg wet 6.67 30-130Surrogate: 2-Fluorophenol 79.25.28
mg/Kg wet 6.67 30-130Surrogate: Phenol-d6 80.25.35
mg/Kg wet 3.33 30-130Surrogate: Nitrobenzene-d5 73.22.44
mg/Kg wet 3.33 30-130Surrogate: 2-Fluorobiphenyl 85.02.83
mg/Kg wet 6.67 30-130Surrogate: 2,4,6-Tribromophenol 76.15.08
mg/Kg wet 3.33 30-130Surrogate: p-Terphenyl-d14 1033.44
LCS (B210345-BS1) Prepared & Analyzed: 08/15/18
Acenaphthene mg/Kg wet0.17 1.67 40-14073.01.22
Acenaphthylene mg/Kg wet0.17 1.67 40-14073.11.22
Acetophenone mg/Kg wet0.34 1.67 40-14073.11.22
Aniline mg/Kg wet0.34 1.67 V-3410-14071.71.19
Anthracene mg/Kg wet0.17 1.67 40-14083.01.38
Benzidine mg/Kg wet0.66 1.67 V-04, V-0640-1401382.29
Benzo(a)anthracene mg/Kg wet0.17 1.67 40-14078.41.31
Benzo(a)pyrene mg/Kg wet0.17 1.67 40-14081.11.35
Benzo(b)fluoranthene mg/Kg wet0.17 1.67 40-14070.61.18
Benzo(g,h,i)perylene mg/Kg wet0.17 1.67 40-14077.21.29
Benzo(k)fluoranthene mg/Kg wet0.17 1.67 40-14076.41.27
Benzoic Acid mg/Kg wet1.0 1.67 30-13073.21.22
Bis(2-chloroethoxy)methane mg/Kg wet0.34 1.67 40-14077.51.29
Bis(2-chloroethyl)ether mg/Kg wet0.34 1.67 40-14070.41.17
Bis(2-chloroisopropyl)ether mg/Kg wet0.34 1.67 40-14087.51.46
Bis(2-Ethylhexyl)phthalate mg/Kg wet0.34 1.67 40-14090.21.50
4-Bromophenylphenylether mg/Kg wet0.34 1.67 40-14074.11.24
Butylbenzylphthalate mg/Kg wet0.34 1.67 40-14087.61.46
Carbazole mg/Kg wet0.17 1.67 40-14077.31.29
4-Chloroaniline mg/Kg wet0.66 1.67 V-3410-14060.01.00
4-Chloro-3-methylphenol mg/Kg wet0.66 1.67 30-13081.11.35
2-Chloronaphthalene mg/Kg wet0.34 1.67 40-14063.51.06
Page 21 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B210345 - SW-846 3546
LCS (B210345-BS1) Prepared & Analyzed: 08/15/18
2-Chlorophenol mg/Kg wet0.34 1.67 30-13075.11.25
4-Chlorophenylphenylether mg/Kg wet0.34 1.67 40-14070.91.18
Chrysene mg/Kg wet0.17 1.67 40-14078.91.31
Dibenz(a,h)anthracene mg/Kg wet0.17 1.67 40-14077.41.29
Dibenzofuran mg/Kg wet0.34 1.67 40-14074.31.24
Di-n-butylphthalate mg/Kg wet0.34 1.67 40-14082.21.37
1,2-Dichlorobenzene mg/Kg wet0.34 1.67 40-14070.81.18
1,3-Dichlorobenzene mg/Kg wet0.34 1.67 40-14066.91.12
1,4-Dichlorobenzene mg/Kg wet0.34 1.67 40-14067.21.12
3,3-Dichlorobenzidine mg/Kg wet0.17 1.67 V-3420-14069.81.16
2,4-Dichlorophenol mg/Kg wet0.34 1.67 30-13076.01.27
Diethylphthalate mg/Kg wet0.34 1.67 40-14070.51.18
2,4-Dimethylphenol mg/Kg wet0.34 1.67 30-13085.31.42
Dimethylphthalate mg/Kg wet0.34 1.67 40-14072.41.21
4,6-Dinitro-2-methylphenol mg/Kg wet0.34 1.67 30-13074.01.23
2,4-Dinitrophenol mg/Kg wet0.66 1.67 30-13056.80.947
2,4-Dinitrotoluene mg/Kg wet0.34 1.67 40-14074.01.23
2,6-Dinitrotoluene mg/Kg wet0.34 1.67 40-14080.51.34
Di-n-octylphthalate mg/Kg wet0.34 1.67 40-14090.21.50
1,2-Diphenylhydrazine (as Azobenzene)mg/Kg wet0.34 1.67 40-14080.41.34
Fluoranthene mg/Kg wet0.17 1.67 40-14076.91.28
Fluorene mg/Kg wet0.17 1.67 40-14072.31.20
Hexachlorobenzene mg/Kg wet0.34 1.67 40-14071.81.20
Hexachlorobutadiene mg/Kg wet0.34 1.67 40-14069.51.16
Hexachlorocyclopentadiene mg/Kg wet0.34 1.67 L-07, V-0540-14038.4 *0.640
Hexachloroethane mg/Kg wet0.34 1.67 40-14067.01.12
Indeno(1,2,3-cd)pyrene mg/Kg wet0.17 1.67 40-14073.31.22
Isophorone mg/Kg wet0.34 1.67 40-14077.81.30
1-Methylnaphthalene mg/Kg wet0.17 1.67 40-14081.71.36
2-Methylnaphthalene mg/Kg wet0.17 1.67 40-14082.41.37
2-Methylphenol mg/Kg wet0.34 1.67 30-13071.01.18
3/4-Methylphenol mg/Kg wet0.34 1.67 30-13084.81.41
Naphthalene mg/Kg wet0.17 1.67 40-14074.11.23
2-Nitroaniline mg/Kg wet0.34 1.67 40-14070.71.18
3-Nitroaniline mg/Kg wet0.34 1.67 V-3430-14071.11.19
4-Nitroaniline mg/Kg wet0.34 1.67 40-14074.71.24
Nitrobenzene mg/Kg wet0.34 1.67 40-14069.21.15
2-Nitrophenol mg/Kg wet0.34 1.67 30-13080.01.33
4-Nitrophenol mg/Kg wet0.66 1.67 30-13076.11.27
N-Nitrosodimethylamine mg/Kg wet0.34 1.67 40-14064.71.08
N-Nitrosodiphenylamine mg/Kg wet0.34 1.67 40-14098.31.64
N-Nitrosodi-n-propylamine mg/Kg wet0.34 1.67 40-14069.01.15
Pentachloronitrobenzene mg/Kg wet0.34 1.67 40-14072.21.20
Pentachlorophenol mg/Kg wet0.34 1.67 30-13061.81.03
Phenanthrene mg/Kg wet0.17 1.67 40-14081.51.36
Phenol mg/Kg wet0.34 1.67 30-13075.21.25
Pyrene mg/Kg wet0.17 1.67 40-14082.81.38
Pyridine mg/Kg wet0.34 1.67 30-14045.40.757
1,2,4,5-Tetrachlorobenzene mg/Kg wet0.34 1.67 40-14066.11.10
1,2,4-Trichlorobenzene mg/Kg wet0.34 1.67 40-14072.51.21
2,4,5-Trichlorophenol mg/Kg wet0.34 1.67 30-13073.71.23
2,4,6-Trichlorophenol mg/Kg wet0.34 1.67 30-13073.81.23
Page 22 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B210345 - SW-846 3546
LCS (B210345-BS1) Prepared & Analyzed: 08/15/18
mg/Kg wet 6.67 30-130Surrogate: 2-Fluorophenol 77.85.19
mg/Kg wet 6.67 30-130Surrogate: Phenol-d6 82.55.50
mg/Kg wet 3.33 30-130Surrogate: Nitrobenzene-d5 75.12.50
mg/Kg wet 3.33 30-130Surrogate: 2-Fluorobiphenyl 85.72.86
mg/Kg wet 6.67 30-130Surrogate: 2,4,6-Tribromophenol 70.14.67
mg/Kg wet 3.33 30-130Surrogate: p-Terphenyl-d14 97.23.24
LCS Dup (B210345-BSD1) Prepared & Analyzed: 08/15/18
Acenaphthene mg/Kg wet0.17 1.67 3040-14071.4 2.221.19
Acenaphthylene mg/Kg wet0.17 1.67 3040-14072.5 0.7421.21
Acetophenone mg/Kg wet0.34 1.67 3040-14070.9 3.141.18
Aniline mg/Kg wet0.34 1.67 50 V-3410-14057.8 21.40.963
Anthracene mg/Kg wet0.17 1.67 3040-14081.5 1.871.36
Benzidine mg/Kg wet0.66 1.67 30 V-04, V-0640-140114 18.31.91
Benzo(a)anthracene mg/Kg wet0.17 1.67 3040-14077.7 0.9481.30
Benzo(a)pyrene mg/Kg wet0.17 1.67 3040-14080.8 0.4691.35
Benzo(b)fluoranthene mg/Kg wet0.17 1.67 3040-14070.9 0.5371.18
Benzo(g,h,i)perylene mg/Kg wet0.17 1.67 3040-14074.8 3.181.25
Benzo(k)fluoranthene mg/Kg wet0.17 1.67 3040-14077.2 1.121.29
Benzoic Acid mg/Kg wet1.0 1.67 5030-13069.9 4.671.16
Bis(2-chloroethoxy)methane mg/Kg wet0.34 1.67 3040-14073.5 5.251.22
Bis(2-chloroethyl)ether mg/Kg wet0.34 1.67 3040-14065.9 6.611.10
Bis(2-chloroisopropyl)ether mg/Kg wet0.34 1.67 3040-14078.9 10.41.31
Bis(2-Ethylhexyl)phthalate mg/Kg wet0.34 1.67 3040-14085.9 4.881.43
4-Bromophenylphenylether mg/Kg wet0.34 1.67 3040-14074.3 0.2701.24
Butylbenzylphthalate mg/Kg wet0.34 1.67 3040-14084.0 4.291.40
Carbazole mg/Kg wet0.17 1.67 3040-14076.2 1.431.27
4-Chloroaniline mg/Kg wet0.66 1.67 30 V-3410-14045.7 27.10.761
4-Chloro-3-methylphenol mg/Kg wet0.66 1.67 3030-13076.6 5.711.28
2-Chloronaphthalene mg/Kg wet0.34 1.67 3040-14064.0 0.7531.07
2-Chlorophenol mg/Kg wet0.34 1.67 3030-13075.1 0.05321.25
4-Chlorophenylphenylether mg/Kg wet0.34 1.67 3040-14071.3 0.5341.19
Chrysene mg/Kg wet0.17 1.67 3040-14077.8 1.331.30
Dibenz(a,h)anthracene mg/Kg wet0.17 1.67 3040-14075.6 2.381.26
Dibenzofuran mg/Kg wet0.34 1.67 3040-14074.1 0.2431.23
Di-n-butylphthalate mg/Kg wet0.34 1.67 3040-14078.9 4.201.31
1,2-Dichlorobenzene mg/Kg wet0.34 1.67 3040-14071.9 1.631.20
1,3-Dichlorobenzene mg/Kg wet0.34 1.67 3040-14068.9 2.971.15
1,4-Dichlorobenzene mg/Kg wet0.34 1.67 3040-14069.2 2.991.15
3,3-Dichlorobenzidine mg/Kg wet0.17 1.67 50 V-3420-14057.8 18.70.964
2,4-Dichlorophenol mg/Kg wet0.34 1.67 3030-13074.8 1.541.25
Diethylphthalate mg/Kg wet0.34 1.67 3040-14068.6 2.791.14
2,4-Dimethylphenol mg/Kg wet0.34 1.67 3030-13084.4 1.061.41
Dimethylphthalate mg/Kg wet0.34 1.67 3040-14071.0 1.981.18
4,6-Dinitro-2-methylphenol mg/Kg wet0.34 1.67 3030-13072.0 2.661.20
2,4-Dinitrophenol mg/Kg wet0.66 1.67 3030-13056.2 1.030.937
2,4-Dinitrotoluene mg/Kg wet0.34 1.67 3040-14073.5 0.6241.22
2,6-Dinitrotoluene mg/Kg wet0.34 1.67 3040-14079.0 1.911.32
Di-n-octylphthalate mg/Kg wet0.34 1.67 3040-14086.8 3.801.45
1,2-Diphenylhydrazine (as Azobenzene)mg/Kg wet0.34 1.67 3040-14071.2 12.11.19
Fluoranthene mg/Kg wet0.17 1.67 3040-14076.4 0.6791.27
Fluorene mg/Kg wet0.17 1.67 3040-14071.1 1.651.18
Page 23 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B210345 - SW-846 3546
LCS Dup (B210345-BSD1) Prepared & Analyzed: 08/15/18
Hexachlorobenzene mg/Kg wet0.34 1.67 3040-14071.6 0.3351.19
Hexachlorobutadiene mg/Kg wet0.34 1.67 3040-14073.4 5.541.22
Hexachlorocyclopentadiene mg/Kg wet0.34 1.67 30 V-0540-14040.7 5.910.679
Hexachloroethane mg/Kg wet0.34 1.67 3040-14065.7 1.931.09
Indeno(1,2,3-cd)pyrene mg/Kg wet0.17 1.67 3040-14077.0 4.871.28
Isophorone mg/Kg wet0.34 1.67 3040-14073.4 5.871.22
1-Methylnaphthalene mg/Kg wet0.17 1.67 3040-14080.9 0.9351.35
2-Methylnaphthalene mg/Kg wet0.17 1.67 3040-14081.8 0.6821.36
2-Methylphenol mg/Kg wet0.34 1.67 3030-13067.5 5.031.12
3/4-Methylphenol mg/Kg wet0.34 1.67 3030-13080.6 5.151.34
Naphthalene mg/Kg wet0.17 1.67 3040-14075.5 1.901.26
2-Nitroaniline mg/Kg wet0.34 1.67 3040-14065.7 7.361.10
3-Nitroaniline mg/Kg wet0.34 1.67 30 V-3430-14063.8 10.81.06
4-Nitroaniline mg/Kg wet0.34 1.67 3040-14075.0 0.3471.25
Nitrobenzene mg/Kg wet0.34 1.67 3040-14066.5 4.011.11
2-Nitrophenol mg/Kg wet0.34 1.67 3030-13081.3 1.611.35
4-Nitrophenol mg/Kg wet0.66 1.67 5030-13072.3 5.121.21
N-Nitrosodimethylamine mg/Kg wet0.34 1.67 3040-14060.7 6.281.01
N-Nitrosodiphenylamine mg/Kg wet0.34 1.67 3040-14095.3 3.121.59
N-Nitrosodi-n-propylamine mg/Kg wet0.34 1.67 3040-14063.1 8.871.05
Pentachloronitrobenzene mg/Kg wet0.34 1.67 3040-14074.4 3.061.24
Pentachlorophenol mg/Kg wet0.34 1.67 3030-13061.3 0.8771.02
Phenanthrene mg/Kg wet0.17 1.67 3040-14079.5 2.461.32
Phenol mg/Kg wet0.34 1.67 3030-13072.0 4.371.20
Pyrene mg/Kg wet0.17 1.67 3040-14082.1 0.9221.37
Pyridine mg/Kg wet0.34 1.67 3030-14044.3 2.500.738
1,2,4,5-Tetrachlorobenzene mg/Kg wet0.34 1.67 3040-14067.4 1.981.12
1,2,4-Trichlorobenzene mg/Kg wet0.34 1.67 3040-14075.1 3.551.25
2,4,5-Trichlorophenol mg/Kg wet0.34 1.67 3030-13073.4 0.3811.22
2,4,6-Trichlorophenol mg/Kg wet0.34 1.67 3030-13075.4 2.091.26
mg/Kg wet 6.67 30-130Surrogate: 2-Fluorophenol 75.95.06
mg/Kg wet 6.67 30-130Surrogate: Phenol-d6 77.95.19
mg/Kg wet 3.33 30-130Surrogate: Nitrobenzene-d5 71.42.38
mg/Kg wet 3.33 30-130Surrogate: 2-Fluorobiphenyl 84.72.82
mg/Kg wet 6.67 30-130Surrogate: 2,4,6-Tribromophenol 70.64.70
mg/Kg wet 3.33 30-130Surrogate: p-Terphenyl-d14 95.73.19
Page 24 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - EPH - Quality Control
QUALITY CONTROL
[TOC_2]Petroleum Hydrocarbons Analyses - EPH[TOC]
Batch B210344 - SW-846 3546
[TOC_3]B210344[TOC]
Blank (B210344-BLK1) Prepared: 08/15/18 Analyzed: 08/16/18
C9-C18 Aliphatics mg/Kg wet10ND
C19-C36 Aliphatics mg/Kg wet10ND
Unadjusted C11-C22 Aromatics mg/Kg wet10ND
C11-C22 Aromatics mg/Kg wet10ND
Acenaphthene mg/Kg wet0.10ND
Acenaphthylene mg/Kg wet0.10ND
Anthracene mg/Kg wet0.10ND
Benzo(a)anthracene mg/Kg wet0.10ND
Benzo(a)pyrene mg/Kg wet0.10ND
Benzo(b)fluoranthene mg/Kg wet0.10ND
Benzo(g,h,i)perylene mg/Kg wet0.10ND
Benzo(k)fluoranthene mg/Kg wet0.10ND
Chrysene mg/Kg wet0.10ND
Dibenz(a,h)anthracene mg/Kg wet0.10ND
Fluoranthene mg/Kg wet0.10ND
Fluorene mg/Kg wet0.10ND
Indeno(1,2,3-cd)pyrene mg/Kg wet0.10ND
2-Methylnaphthalene mg/Kg wet0.10ND
Naphthalene mg/Kg wet0.10ND
Phenanthrene mg/Kg wet0.10ND
Pyrene mg/Kg wet0.10ND
n-Decane mg/Kg wet0.10ND
n-Docosane mg/Kg wet0.10ND
n-Dodecane mg/Kg wet0.10ND
n-Eicosane mg/Kg wet0.10ND
n-Hexacosane mg/Kg wet0.10ND
n-Hexadecane mg/Kg wet0.10ND
n-Hexatriacontane mg/Kg wet0.10ND
n-Nonadecane mg/Kg wet0.10ND
n-Nonane mg/Kg wet0.10ND
n-Octacosane mg/Kg wet0.10ND
n-Octadecane mg/Kg wet0.10ND
n-Tetracosane mg/Kg wet0.10ND
n-Tetradecane mg/Kg wet0.10ND
n-Triacontane mg/Kg wet0.10ND
Naphthalene-aliphatic fraction mg/Kg wet0.10ND
2-Methylnaphthalene-aliphatic fraction mg/Kg wet0.10ND
mg/Kg wet 5.00 40-140Surrogate: Chlorooctadecane (COD)82.04.10
mg/Kg wet 5.00 40-140Surrogate: o-Terphenyl (OTP)79.23.96
mg/Kg wet 5.00 40-140Surrogate: 2-Bromonaphthalene 93.74.68
mg/Kg wet 5.00 40-140Surrogate: 2-Fluorobiphenyl 87.34.37
LCS (B210344-BS1) Prepared: 08/15/18 Analyzed: 08/16/18
C9-C18 Aliphatics mg/Kg wet10 30.0 40-14080.924.3
C19-C36 Aliphatics mg/Kg wet10 40.0 40-14093.637.5
Acenaphthene mg/Kg wet0.10 5.00 40-14074.53.72
Acenaphthylene mg/Kg wet0.10 5.00 40-14070.33.51
Anthracene mg/Kg wet0.10 5.00 40-14082.94.14
Benzo(a)anthracene mg/Kg wet0.10 5.00 40-14084.14.20
Benzo(a)pyrene mg/Kg wet0.10 5.00 40-14082.64.13
Benzo(b)fluoranthene mg/Kg wet0.10 5.00 40-14083.84.19
Benzo(g,h,i)perylene mg/Kg wet0.10 5.00 40-14082.74.14
Page 25 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - EPH - Quality Control
QUALITY CONTROL
Batch B210344 - SW-846 3546
LCS (B210344-BS1) Prepared: 08/15/18 Analyzed: 08/16/18
Benzo(k)fluoranthene mg/Kg wet0.10 5.00 40-14083.14.15
Chrysene mg/Kg wet0.10 5.00 40-14083.94.19
Dibenz(a,h)anthracene mg/Kg wet0.10 5.00 40-14085.44.27
Fluoranthene mg/Kg wet0.10 5.00 40-14083.64.18
Fluorene mg/Kg wet0.10 5.00 40-14078.73.93
Indeno(1,2,3-cd)pyrene mg/Kg wet0.10 5.00 40-14079.13.96
2-Methylnaphthalene mg/Kg wet0.10 5.00 40-14070.13.51
Naphthalene mg/Kg wet0.10 5.00 40-14063.83.19
Phenanthrene mg/Kg wet0.10 5.00 40-14084.24.21
Pyrene mg/Kg wet0.10 5.00 40-14085.64.28
n-Decane mg/Kg wet0.10 5.00 40-14051.92.60
n-Docosane mg/Kg wet0.10 5.00 40-14090.64.53
n-Dodecane mg/Kg wet0.10 5.00 40-14067.83.39
n-Eicosane mg/Kg wet0.10 5.00 40-14094.64.73
n-Hexacosane mg/Kg wet0.10 5.00 40-14086.54.33
n-Hexadecane mg/Kg wet0.10 5.00 40-14091.54.58
n-Hexatriacontane mg/Kg wet0.10 5.00 40-14080.34.01
n-Nonadecane mg/Kg wet0.10 5.00 40-14092.54.62
n-Nonane mg/Kg wet0.10 5.00 30-14034.71.74
n-Octacosane mg/Kg wet0.10 5.00 40-14082.34.11
n-Octadecane mg/Kg wet0.10 5.00 40-14094.74.74
n-Tetracosane mg/Kg wet0.10 5.00 40-14089.14.45
n-Tetradecane mg/Kg wet0.10 5.00 40-14082.84.14
n-Triacontane mg/Kg wet0.10 5.00 40-14081.64.08
Naphthalene-aliphatic fraction mg/Kg wet0.10 5.00 0-5ND
2-Methylnaphthalene-aliphatic fraction mg/Kg wet0.10 5.00 0-5ND
mg/Kg wet 5.00 40-140Surrogate: Chlorooctadecane (COD)88.34.42
mg/Kg wet 5.00 40-140Surrogate: o-Terphenyl (OTP)86.84.34
mg/Kg wet 5.00 40-140Surrogate: 2-Bromonaphthalene 85.44.27
mg/Kg wet 5.00 40-140Surrogate: 2-Fluorobiphenyl 87.24.36
LCS Dup (B210344-BSD1) Prepared: 08/15/18 Analyzed: 08/16/18
C9-C18 Aliphatics mg/Kg wet10 30.0 2540-14085.8 5.9125.7
C19-C36 Aliphatics mg/Kg wet10 40.0 2540-14095.0 1.4238.0
Acenaphthene mg/Kg wet0.10 5.00 2540-14077.6 4.133.88
Acenaphthylene mg/Kg wet0.10 5.00 2540-14073.3 4.293.67
Anthracene mg/Kg wet0.10 5.00 2540-14085.6 3.264.28
Benzo(a)anthracene mg/Kg wet0.10 5.00 2540-14086.7 3.124.34
Benzo(a)pyrene mg/Kg wet0.10 5.00 2540-14085.5 3.524.28
Benzo(b)fluoranthene mg/Kg wet0.10 5.00 2540-14087.0 3.734.35
Benzo(g,h,i)perylene mg/Kg wet0.10 5.00 2540-14086.8 4.844.34
Benzo(k)fluoranthene mg/Kg wet0.10 5.00 2540-14085.7 3.114.28
Chrysene mg/Kg wet0.10 5.00 2540-14086.4 2.954.32
Dibenz(a,h)anthracene mg/Kg wet0.10 5.00 2540-14089.9 5.174.50
Fluoranthene mg/Kg wet0.10 5.00 2540-14086.4 3.284.32
Fluorene mg/Kg wet0.10 5.00 2540-14081.7 3.784.09
Indeno(1,2,3-cd)pyrene mg/Kg wet0.10 5.00 2540-14082.2 3.794.11
2-Methylnaphthalene mg/Kg wet0.10 5.00 2540-14072.8 3.803.64
Naphthalene mg/Kg wet0.10 5.00 2540-14066.7 4.513.34
Phenanthrene mg/Kg wet0.10 5.00 2540-14087.2 3.404.36
Pyrene mg/Kg wet0.10 5.00 2540-14088.4 3.184.42
n-Decane mg/Kg wet0.10 5.00 2540-14055.8 7.222.79
Page 26 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - EPH - Quality Control
QUALITY CONTROL
Batch B210344 - SW-846 3546
LCS Dup (B210344-BSD1) Prepared: 08/15/18 Analyzed: 08/16/18
n-Docosane mg/Kg wet0.10 5.00 2540-14091.8 1.334.59
n-Dodecane mg/Kg wet0.10 5.00 2540-14071.7 5.593.58
n-Eicosane mg/Kg wet0.10 5.00 2540-14094.0 0.5984.70
n-Hexacosane mg/Kg wet0.10 5.00 2540-14088.2 1.874.41
n-Hexadecane mg/Kg wet0.10 5.00 2540-14093.8 2.524.69
n-Hexatriacontane mg/Kg wet0.10 5.00 2540-14082.3 2.514.12
n-Nonadecane mg/Kg wet0.10 5.00 2540-14093.8 1.424.69
n-Nonane mg/Kg wet0.10 5.00 2530-14037.6 8.001.88
n-Octacosane mg/Kg wet0.10 5.00 2540-14084.0 2.034.20
n-Octadecane mg/Kg wet0.10 5.00 2540-14096.5 1.914.83
n-Tetracosane mg/Kg wet0.10 5.00 2540-14090.5 1.614.53
n-Tetradecane mg/Kg wet0.10 5.00 2540-14085.8 3.574.29
n-Triacontane mg/Kg wet0.10 5.00 2540-14083.5 2.354.17
Naphthalene-aliphatic fraction mg/Kg wet0.10 5.00 0-5ND
2-Methylnaphthalene-aliphatic fraction mg/Kg wet0.10 5.00 0-5ND
mg/Kg wet 5.00 40-140Surrogate: Chlorooctadecane (COD)88.54.42
mg/Kg wet 5.00 40-140Surrogate: o-Terphenyl (OTP)88.24.41
mg/Kg wet 5.00 40-140Surrogate: 2-Bromonaphthalene 84.04.20
mg/Kg wet 5.00 40-140Surrogate: 2-Fluorobiphenyl 87.94.40
Page 27 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - VPH - Quality Control
QUALITY CONTROL
[TOC_2]Petroleum Hydrocarbons Analyses - VPH[TOC]
Batch B209997 - MA VPH
[TOC_3]B209997[TOC]
Blank (B209997-BLK1) Prepared: 08/10/18 Analyzed: 08/14/18
Unadjusted C5-C8 Aliphatics mg/Kg wet10ND
C5-C8 Aliphatics mg/Kg wet10ND
Unadjusted C9-C12 Aliphatics mg/Kg wet10ND
C9-C12 Aliphatics mg/Kg wet10ND
C9-C10 Aromatics mg/Kg wet10ND
Benzene mg/Kg wet0.050ND
Butylcyclohexane mg/Kg wet0.050ND
Decane mg/Kg wet0.050ND
Ethylbenzene mg/Kg wet0.050ND
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.050ND
2-Methylpentane mg/Kg wet0.050ND
Naphthalene mg/Kg wet0.50ND
Nonane mg/Kg wet0.050ND
Pentane mg/Kg wet0.050ND
Toluene mg/Kg wet0.050ND
1,2,4-Trimethylbenzene mg/Kg wet0.050ND
2,2,4-Trimethylpentane mg/Kg wet0.050ND
m+p Xylene mg/Kg wet0.10ND
o-Xylene mg/Kg wet0.050ND
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)93.137.3
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)86.334.5
LCS (B209997-BS1) Prepared: 08/10/18 Analyzed: 08/14/18
Benzene mg/Kg wet0.0010 0.100 70-1301070.107
Butylcyclohexane mg/Kg wet0.0010 0.100 70-13089.50.0895
Decane mg/Kg wet0.0010 0.100 70-13093.00.0930
Ethylbenzene mg/Kg wet0.0010 0.100 70-1301080.108
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.0010 0.100 70-1301090.109
2-Methylpentane mg/Kg wet0.0010 0.100 70-1301190.119
Naphthalene mg/Kg wet0.010 0.100 70-1301030.103
Nonane mg/Kg wet0.0010 0.100 30-13088.20.0882
Pentane mg/Kg wet0.0010 0.100 70-1301210.121
Toluene mg/Kg wet0.0010 0.100 70-1301070.107
1,2,4-Trimethylbenzene mg/Kg wet0.0010 0.100 70-1301090.109
2,2,4-Trimethylpentane mg/Kg wet0.0010 0.100 70-1301110.111
m+p Xylene mg/Kg wet0.0020 0.200 70-1301100.219
o-Xylene mg/Kg wet0.0010 0.100 70-1301070.107
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)94.237.7
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)87.735.1
LCS Dup (B209997-BSD1) Prepared: 08/10/18 Analyzed: 08/14/18
Benzene mg/Kg wet0.0010 0.100 2570-130106 0.5780.106
Butylcyclohexane mg/Kg wet0.0010 0.100 2570-13089.6 0.1520.0896
Decane mg/Kg wet0.0010 0.100 2570-13094.5 1.530.0945
Ethylbenzene mg/Kg wet0.0010 0.100 2570-130107 0.6420.107
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.0010 0.100 2570-130107 2.090.107
2-Methylpentane mg/Kg wet0.0010 0.100 2570-130118 0.7560.118
Naphthalene mg/Kg wet0.010 0.100 2570-130101 2.400.101
Nonane mg/Kg wet0.0010 0.100 2530-13088.5 0.2900.0885
Pentane mg/Kg wet0.0010 0.100 2570-130119 1.580.119
Toluene mg/Kg wet0.0010 0.100 2570-130106 0.6500.106
1,2,4-Trimethylbenzene mg/Kg wet0.0010 0.100 2570-130108 0.9920.108
Page 28 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - VPH - Quality Control
QUALITY CONTROL
Batch B209997 - MA VPH
LCS Dup (B209997-BSD1) Prepared: 08/10/18 Analyzed: 08/14/18
2,2,4-Trimethylpentane mg/Kg wet0.0010 0.100 2570-130108 2.970.108
m+p Xylene mg/Kg wet0.0020 0.200 2570-130109 0.7790.217
o-Xylene mg/Kg wet0.0010 0.100 2570-130106 0.8960.106
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)95.238.1
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)87.735.1
Page 29 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) - Quality Control
QUALITY CONTROL
[TOC_2]Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)[TOC]
Batch B210372 - % Solids
[TOC_3]B210372[TOC]
Duplicate (B210372-DUP1) Prepared & Analyzed: 08/15/18 Source: 18H0706-01
% Solids % Wt 200.10386.4 86.3
Page 30 of 39
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
FLAG/QUALIFIER SUMMARY
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
J
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but
the other is within limits. RPD between the two LFB/LCS results is within method specified criteria.
L-07
Initial calibration did not meet method specifications. Compound was calibrated using a response factor where
%RSD is outside of method specified criteria. Reported result is estimated.
V-04
Continuing calibration did not meet method specifications and was biased on the low side for this compound.
Reported result is estimated.
V-05
Continuing calibration did not meet method specifications and was biased on the high side for this compound.
Reported result is estimated.
V-06
Continuing calibration did not meet method specifications and was biased on the high side. Data validation is not
affected since sample result was "not detected" for this compound.
V-20
Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this
compound. Reported result is estimated.
V-34
[TOC_1]Flag/Qualifier Summary[TOC]
Page 31 of 39
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
MADEP-EPH-04-1.1 in Soil
CT,NC,ME,NH-PC9-C18 Aliphatics
CT,NC,ME,NH-PC19-C36 Aliphatics
CT,NC,ME,NH-PUnadjusted C11-C22 Aromatics
CT,NC,ME,NH-PC11-C22 Aromatics
CT,NC,ME,NH-PAcenaphthene
CT,NC,ME,NH-PAcenaphthylene
CT,NC,ME,NH-PAnthracene
CT,NC,ME,NH-PBenzo(a)anthracene
CT,NC,ME,NH-PBenzo(a)pyrene
CT,NC,ME,NH-PBenzo(b)fluoranthene
CT,NC,ME,NH-PBenzo(g,h,i)perylene
CT,NC,ME,NH-PBenzo(k)fluoranthene
CT,NC,ME,NH-PChrysene
CT,NC,ME,NH-PDibenz(a,h)anthracene
CT,NC,ME,NH-PFluoranthene
CT,NC,MEFluorene
CT,NC,ME,NH-PIndeno(1,2,3-cd)pyrene
CT,NC,ME2-Methylnaphthalene
CT,NC,ME,NH-PNaphthalene
CT,NC,ME,NH-PPhenanthrene
CT,NC,ME,NH-PPyrene
MADEP-VPH-Feb 2018 Rev 2.1 in Soil
CT,NC,ME,NH-PUnadjusted C5-C8 Aliphatics
CT,NC,ME,NH-PC5-C8 Aliphatics
CT,NC,ME,NH-PUnadjusted C9-C12 Aliphatics
CT,NC,ME,NH-PC9-C12 Aliphatics
CT,NC,ME,NH-PC9-C10 Aromatics
CT,NC,ME,NH-PBenzene
CT,NC,ME,NH-PEthylbenzene
CT,NC,ME,NH-PMethyl tert-Butyl Ether (MTBE)
CT,NC,ME,NH-PNaphthalene
CT,NC,ME,NH-PToluene
CT,NC,ME,NH-Pm+p Xylene
CT,NC,ME,NH-Po-Xylene
SW-846 8260B in Soil
NCAcetone
NCAcrylonitrile
NCtert-Amyl Methyl Ether (TAME)
NCBenzene
NCBromobenzene
NCBromochloromethane
NCBromodichloromethane
NCBromoform
NCBromomethane
NC2-Butanone (MEK)
NCtert-Butyl Alcohol (TBA)
[TOC_1]Certifications[TOC]
Page 32 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 8260B in Soil
NCn-Butylbenzene
NCsec-Butylbenzene
NCtert-Butylbenzene
NCtert-Butyl Ethyl Ether (TBEE)
NCCarbon Disulfide
NCCarbon Tetrachloride
NCChlorobenzene
NCChlorodibromomethane
NCChloroethane
NCChloroform
NCChloromethane
NC2-Chlorotoluene
NC4-Chlorotoluene
NC1,2-Dibromo-3-chloropropane (DBCP)
NC1,2-Dibromoethane (EDB)
NCDibromomethane
NC1,2-Dichlorobenzene
NC1,3-Dichlorobenzene
NC1,4-Dichlorobenzene
NCtrans-1,4-Dichloro-2-butene
NCDichlorodifluoromethane (Freon 12)
NC1,1-Dichloroethane
NC1,2-Dichloroethane
NC1,1-Dichloroethylene
NCcis-1,2-Dichloroethylene
NCtrans-1,2-Dichloroethylene
NC1,2-Dichloropropane
NC1,3-Dichloropropane
NC2,2-Dichloropropane
NC1,1-Dichloropropene
NCcis-1,3-Dichloropropene
NCtrans-1,3-Dichloropropene
NCDiethyl Ether
NCDiisopropyl Ether (DIPE)
NC1,4-Dioxane
NCEthylbenzene
NCHexachlorobutadiene
NC2-Hexanone (MBK)
NCIsopropylbenzene (Cumene)
NCp-Isopropyltoluene (p-Cymene)
NCMethyl tert-Butyl Ether (MTBE)
NCMethylene Chloride
NC4-Methyl-2-pentanone (MIBK)
NCNaphthalene
NCn-Propylbenzene
NCStyrene
NC1,1,1,2-Tetrachloroethane
Page 33 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 8260B in Soil
NC1,1,2,2-Tetrachloroethane
NCTetrachloroethylene
NCTetrahydrofuran
NCToluene
NC1,2,3-Trichlorobenzene
NC1,2,4-Trichlorobenzene
NC1,3,5-Trichlorobenzene
NC1,1,1-Trichloroethane
NC1,1,2-Trichloroethane
NCTrichloroethylene
NCTrichlorofluoromethane (Freon 11)
NC1,2,3-Trichloropropane
NC1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
NC1,2,4-Trimethylbenzene
NC1,3,5-Trimethylbenzene
NCVinyl Chloride
NCm+p Xylene
NCo-Xylene
SW-846 8270D in Soil
CT,NY,NH,ME,NC,VAAcenaphthene
CT,NY,NH,ME,NC,VAAcenaphthylene
NY,NH,ME,NC,VAAcetophenone
NY,NH,ME,NC,VAAniline
CT,NY,NH,ME,NC,VAAnthracene
CT,NY,NH,ME,NC,VABenzidine
CT,NY,NH,ME,NC,VABenzo(a)anthracene
CT,NY,NH,ME,NC,VABenzo(a)pyrene
CT,NY,NH,ME,NC,VABenzo(b)fluoranthene
CT,NY,NH,ME,NC,VABenzo(g,h,i)perylene
CT,NY,NH,ME,NC,VABenzo(k)fluoranthene
NY,NH,ME,NC,VABenzoic Acid
CT,NY,NH,ME,NC,VABis(2-chloroethoxy)methane
CT,NY,NH,ME,NC,VABis(2-chloroethyl)ether
CT,NY,NH,ME,NC,VABis(2-chloroisopropyl)ether
CT,NY,NH,ME,NC,VABis(2-Ethylhexyl)phthalate
CT,NY,NH,ME,NC,VA4-Bromophenylphenylether
CT,NY,NH,ME,NC,VAButylbenzylphthalate
NCCarbazole
CT,NY,NH,ME,NC,VA4-Chloroaniline
CT,NY,NH,ME,NC,VA4-Chloro-3-methylphenol
CT,NY,NH,NC,VA2-Chloronaphthalene
CT,NY,NH,ME,NC,VA2-Chlorophenol
CT,NY,NH,ME,NC,VA4-Chlorophenylphenylether
CT,NY,NH,ME,NC,VAChrysene
CT,NY,NH,ME,NC,VADibenz(a,h)anthracene
CT,NY,NH,ME,NC,VADibenzofuran
Page 34 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 8270D in Soil
CT,NY,NH,ME,NC,VADi-n-butylphthalate
NY,NH,ME,NC,VA1,2-Dichlorobenzene
NY,NH,ME,NC,VA1,3-Dichlorobenzene
NY,NH,ME,NC,VA1,4-Dichlorobenzene
CT,NY,NH,ME,NC,VA3,3-Dichlorobenzidine
CT,NY,NH,ME,NC,VA2,4-Dichlorophenol
CT,NY,NH,ME,NC,VADiethylphthalate
CT,NY,NH,ME,NC,VA2,4-Dimethylphenol
CT,NY,NH,ME,NC,VADimethylphthalate
CT,NY,NH,ME,NC,VA4,6-Dinitro-2-methylphenol
CT,NY,NH,ME,NC,VA2,4-Dinitrophenol
CT,NY,NH,ME,NC,VA2,4-Dinitrotoluene
CT,NY,NH,ME,NC,VA2,6-Dinitrotoluene
CT,NY,NH,ME,NC,VADi-n-octylphthalate
NY,NH,ME,NC,VA1,2-Diphenylhydrazine (as Azobenzene)
CT,NY,NH,ME,NC,VAFluoranthene
NY,NH,ME,NC,VAFluorene
CT,NY,NH,ME,NC,VAHexachlorobenzene
CT,NY,NH,ME,NC,VAHexachlorobutadiene
CT,NY,NH,ME,NC,VAHexachlorocyclopentadiene
CT,NY,NH,ME,NC,VAHexachloroethane
CT,NY,NH,ME,NC,VAIndeno(1,2,3-cd)pyrene
CT,NY,NH,ME,NC,VAIsophorone
NC1-Methylnaphthalene
CT,NY,NH,ME,NC,VA2-Methylnaphthalene
CT,NY,NH,ME,NC,VA2-Methylphenol
CT,NY,NH,ME,NC,VA3/4-Methylphenol
CT,NY,NH,ME,NC,VANaphthalene
CT,NY,NH,ME,NC,VA2-Nitroaniline
CT,NY,NH,ME,NC,VA3-Nitroaniline
CT,NY,NH,ME,NC,VA4-Nitroaniline
CT,NY,NH,ME,NC,VANitrobenzene
CT,NY,NH,ME,NC,VA2-Nitrophenol
CT,NY,NH,ME,NC,VA4-Nitrophenol
CT,NY,NH,ME,NC,VAN-Nitrosodimethylamine
CT,NY,NH,ME,NC,VAN-Nitrosodiphenylamine
CT,NY,NH,ME,NC,VAN-Nitrosodi-n-propylamine
NY,NCPentachloronitrobenzene
CT,NY,NH,ME,NC,VAPentachlorophenol
CT,NY,NH,ME,NC,VAPhenanthrene
CT,NY,NH,ME,NC,VAPhenol
CT,NY,NH,ME,NC,VAPyrene
CT,NY,NH,ME,NC,VAPyridine
NY,NC1,2,4,5-Tetrachlorobenzene
CT,NY,NH,ME,NC,VA1,2,4-Trichlorobenzene
CT,NY,NH,ME,NC,VA2,4,5-Trichlorophenol
CT,NY,NH,ME,NC,VA2,4,6-Trichlorophenol
Page 35 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 8270D in Soil
NC2-Fluorophenol
The CON-TEST Environmental Laboratory operates under the following certifications and accreditations:
Code Description Number Expires
100033AIHA-LAP, LLC - ISO17025:2005AIHA 03/1/2020
M-MA100Massachusetts DEPMA 06/30/2019
PH-0567Connecticut Department of Publilc HealthCT 09/30/2019
10899 NELAPNew York State Department of HealthNY 04/1/2019
2516 NELAPNew Hampshire Environmental LabNH-S 02/5/2019
LAO00112Rhode Island Department of HealthRI 12/30/2018
652North Carolina Div. of Water QualityNC 12/31/2018
MA007 NELAPNew Jersey DEPNJ 06/30/2019
E871027 NELAPFlorida Department of HealthFL 06/30/2019
LL015036Vermont Department of Health Lead LaboratoryVT 07/30/2019
2011028State of MaineME 06/9/2019
460217Commonwealth of VirginiaVA 12/14/2018
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2018
VT-255716Vermont Department of Health Drinking WaterVT-DW 06/12/2019
25703North Carolina Department of HealthNC-DW 07/31/2019
Page 36 of 39
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ATTACHMENT II

08-17-2018 S:\Enviro\Pilot\6955 - Haw River\Boring Logs\SB-1.borClient: Pilot
Project #: PT00695501
Haw River, Alamance County, NC
1044 Jimmie Kerr Road
Pilot #5955
BORING LOG: SB-1
(Page 1 of 1)
Date(s) Drilled : 08/13/18
Drilling Contractor : GEX
Drilling Method : Hand Auger
Boring Diameter : 2 inches
Sampling Method : NA
Sampling Interval : NA
Logged By : Robert Winfield
Depth In Feet (BGS)0
1
2
3
4
5 USCSGRAPHICDESCRIPTION
AR
SM
SM
SM
Asphalt
Brown; Silty SAND with some rock fragments
Brown; Silty SAND with pockets of green silty sand mixed in; Petroleum odor present
Brown, green, and grey; Silty SAND; Petroleum odor present
BGS - below ground surface
Boring terminated at 5 feet bgs.

ATTACHMENT III

39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
August 16, 2018
Maureen Jackson
ATC Group Services LLC - Raleigh NC
2725 East Millbrook Road, Ste 121
Raleigh, NC 27604
Project Location: Haw River, NC
Client Job Number:
Project Number: PT00695501
Laboratory Work Order Number: 18H0706
Enclosed are results of analyses for samples received by the laboratory on August 15, 2018. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Kerry K. McGee
Project Manager
Page 1 of 39
Table of Contents
Table of Contents
Sample Summary 3
Hits Only Report 4
Case Narrative 5
Sample Results 7
18H0706-01 7
Sample Preparation Information 14
QC Data 15
Volatile Organic Compounds by GC/MS 15
B210357 15
Semivolatile Organic Compounds by GC/MS 20
B210345 20
Petroleum Hydrocarbons Analyses - EPH 25
B210344 25
Petroleum Hydrocarbons Analyses - VPH 28
B209997 28
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) 30
B210372 30
Flag/Qualifier Summary 31
Certifications 32
Chain of Custody/Sample Receipt 37
Page 2 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
8/16/2018
ATC Group Services LLC - Raleigh NC
2725 East Millbrook Road, Ste 121
Raleigh, NC 27604
ATTN: Maureen Jackson
PT00695501
18H0706
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Haw River, NC
SB-1 18H0706-01 Soil MADEP-EPH-04-1.1
MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
SW-846 8260B
SW-846 8270D
[TOC_1]Sample Summary[TOC]
Page 3 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
[TOC_1]Hits Only Report[TOC]EXECUTIVE SUMMARY
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
18H0706-01SB-1
DL
Pyrene 0.080 0.20 mg/Kg dry SW-846 8270DJ0.065
C11-C22 Aromatics 160 12 mg/Kg dry MADEP-EPH-04-1.1
C19-C36 Aliphatics 130 12 mg/Kg dry MADEP-EPH-04-1.1
C9-C18 Aliphatics 380 58 mg/Kg dry MADEP-EPH-04-1.1
Unadjusted C11-C22 Aromatics 160 12 mg/Kg dry MADEP-EPH-04-1.1
C9-C10 Aromatics 33 11 mg/Kg dry MADEP-VPH-Feb 2018 Rev 2.11.6
C9-C12 Aliphatics 26 11 mg/Kg dry MADEP-VPH-Feb 2018 Rev 2.12.3
Unadjusted C9-C12 Aliphatics 59 11 mg/Kg dry MADEP-VPH-Feb 2018 Rev 2.12.3
% Solids 86.3 % Wt SM 2540G
Con-Test does not accept liability for the consequences of any actions taken solely on the basis of the information provided in the Executive Summary
section of this report. Users must review this report in its entirety to determine data usability and assessment.
Page 4 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
For method MA VPH only hydrocarbon ranges were requested and reported.
For method MA EPH, only hydrocarbon ranges were requested and reported.
[TOC_1]Case Narrative[TOC]
SW-846 8270D
Qualifications:
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD
between the two LFB/LCS results is within method specified criteria.
Analyte & Samples(s) Qualified:
L-07
Hexachlorocyclopentadiene
B210345-BS1
Initial calibration did not meet method specifications. Compound was calibrated using a response factor where %RSD is outside of method
specified criteria. Reported result is estimated.
Analyte & Samples(s) Qualified:
V-04
Benzidine
18H0706-01[SB-1], B210345-BLK1, B210345-BS1, B210345-BSD1
Continuing calibration did not meet method specifications and was biased on the low side for this compound. Reported result is estimated.
Analyte & Samples(s) Qualified:
V-05
Hexachlorocyclopentadiene
18H0706-01[SB-1], B210345-BLK1, B210345-BS1, B210345-BSD1
Continuing calibration did not meet method specifications and was biased on the high side for this compound. Reported result is estimated.
Analyte & Samples(s) Qualified:
V-06
Benzidine
B210345-BS1, B210345-BSD1
Continuing calibration did not meet method specifications and was biased on the high side. Data validation is not affected since sample result
was "not detected" for this compound.
Analyte & Samples(s) Qualified:
V-20
Benzidine
18H0706-01[SB-1], B210345-BLK1
Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this compound. Reported result is
estimated.
Analyte & Samples(s) Qualified:
V-34
3,3-Dichlorobenzidine
18H0706-01[SB-1], B210345-BLK1, B210345-BS1, B210345-BSD1
3-Nitroaniline
18H0706-01[SB-1], B210345-BLK1, B210345-BS1, B210345-BSD1
4-Chloroaniline
18H0706-01[SB-1], B210345-BLK1, B210345-BS1, B210345-BSD1
Aniline
18H0706-01[SB-1], B210345-BLK1, B210345-BS1, B210345-BSD1
Page 5 of 39
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
MADEP-EPH-04-1.1
SPE cartridge contamination with non-petroleum compounds, if present, is verified by GC/MS in each method blank per extraction batch and excluded from C 11-C22 aromatic
range fraction in all samples in the batch. No significant modifications were made to the method.
MADEP-VPH-Feb 2018 Rev 2.1
Analytical column used for VPH analysis is Restek, Rtx-502.2, 105meter, 0.53mmID, 3um df. Trap used for VPH analysis is Carbopack B/CarboSieveS-III.
No significant modifications were made to the method. All VPH samples were received preserved properly in methanol with a soil/methanol ratio of 1:1 +/- 25% completely
covered by methanol in the proper containers specified on the chain-of-custody form unless specified in this narrative.
The results of analyses reported only relate to samples submitted to the Con-Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Daren J. Damboragian
Director of Operations
Page 6 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 8/15/2018
Work Order: 18H0706Sample Description:Project Location: Haw River, NC
Sample ID: 18H0706-01
Field Sample #: SB-1
Sample Matrix: Soil
Sampled: 8/13/2018 17:00
[TOC_2]18H0706-01[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 2.8 8/15/18 12:22 MFFmg/Kg dry0.55 8/15/18SW-846 8260B1Acetone
ND 0.28 8/15/18 12:22 MFFmg/Kg dry0.033 8/15/18SW-846 8260B1Acrylonitrile
ND 0.028 8/15/18 12:22 MFFmg/Kg dry0.0060 8/15/18SW-846 8260B1tert-Amyl Methyl Ether (TAME)
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0068 8/15/18SW-846 8260B1Benzene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0085 8/15/18SW-846 8260B1Bromobenzene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.013 8/15/18SW-846 8260B1Bromochloromethane
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.017 8/15/18SW-846 8260B1Bromodichloromethane
ND 0.11 8/15/18 12:22 MFFmg/Kg dry0.012 8/15/18SW-846 8260B1Bromoform
ND 0.11 8/15/18 12:22 MFFmg/Kg dry0.054 8/15/18SW-846 8260B1Bromomethane
ND 1.1 8/15/18 12:22 MFFmg/Kg dry0.13 8/15/18SW-846 8260B12-Butanone (MEK)
ND 1.1 8/15/18 12:22 MFFmg/Kg dry0.12 8/15/18SW-846 8260B1tert-Butyl Alcohol (TBA)
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0085 8/15/18SW-846 8260B1n-Butylbenzene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0074 8/15/18SW-846 8260B1sec-Butylbenzene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0069 8/15/18SW-846 8260B1tert-Butylbenzene
ND 0.028 8/15/18 12:22 MFFmg/Kg dry0.0054 8/15/18SW-846 8260B1tert-Butyl Ethyl Ether (TBEE)
ND 0.17 8/15/18 12:22 MFFmg/Kg dry0.058 8/15/18SW-846 8260B1Carbon Disulfide
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.014 8/15/18SW-846 8260B1Carbon Tetrachloride
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0091 8/15/18SW-846 8260B1Chlorobenzene
ND 0.028 8/15/18 12:22 MFFmg/Kg dry0.0059 8/15/18SW-846 8260B1Chlorodibromomethane
ND 0.11 8/15/18 12:22 MFFmg/Kg dry0.016 8/15/18SW-846 8260B1Chloroethane
ND 0.11 8/15/18 12:22 MFFmg/Kg dry0.013 8/15/18SW-846 8260B1Chloroform
ND 0.11 8/15/18 12:22 MFFmg/Kg dry0.031 8/15/18SW-846 8260B1Chloromethane
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0068 8/15/18SW-846 8260B12-Chlorotoluene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0080 8/15/18SW-846 8260B14-Chlorotoluene
ND 0.28 8/15/18 12:22 MFFmg/Kg dry0.021 8/15/18SW-846 8260B11,2-Dibromo-3-chloropropane (DBCP)
ND 0.028 8/15/18 12:22 MFFmg/Kg dry0.0084 8/15/18SW-846 8260B11,2-Dibromoethane (EDB)
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0091 8/15/18SW-846 8260B1Dibromomethane
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0097 8/15/18SW-846 8260B11,2-Dichlorobenzene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0097 8/15/18SW-846 8260B11,3-Dichlorobenzene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0085 8/15/18SW-846 8260B11,4-Dichlorobenzene
ND 0.11 8/15/18 12:22 MFFmg/Kg dry0.018 8/15/18SW-846 8260B1trans-1,4-Dichloro-2-butene
ND 0.11 8/15/18 12:22 MFFmg/Kg dry0.016 8/15/18SW-846 8260B1Dichlorodifluoromethane (Freon 12)
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0090 8/15/18SW-846 8260B11,1-Dichloroethane
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.011 8/15/18SW-846 8260B11,2-Dichloroethane
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.012 8/15/18SW-846 8260B11,1-Dichloroethylene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0084 8/15/18SW-846 8260B1cis-1,2-Dichloroethylene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0085 8/15/18SW-846 8260B1trans-1,2-Dichloroethylene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0074 8/15/18SW-846 8260B11,2-Dichloropropane
ND 0.028 8/15/18 12:22 MFFmg/Kg dry0.0074 8/15/18SW-846 8260B11,3-Dichloropropane
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.012 8/15/18SW-846 8260B12,2-Dichloropropane
ND 0.11 8/15/18 12:22 MFFmg/Kg dry0.0073 8/15/18SW-846 8260B11,1-Dichloropropene
ND 0.028 8/15/18 12:22 MFFmg/Kg dry0.0068 8/15/18SW-846 8260B1cis-1,3-Dichloropropene
ND 0.028 8/15/18 12:22 MFFmg/Kg dry0.0064 8/15/18SW-846 8260B1trans-1,3-Dichloropropene
ND 0.11 8/15/18 12:22 MFFmg/Kg dry0.013 8/15/18SW-846 8260B1Diethyl Ether
[TOC_1]Sample Results[TOC]
Page 7 of 39
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 8/15/2018
Work Order: 18H0706Sample Description:Project Location: Haw River, NC
Sample ID: 18H0706-01
Field Sample #: SB-1
Sample Matrix: Soil
Sampled: 8/13/2018 17:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.028 8/15/18 12:22 MFFmg/Kg dry0.010 8/15/18SW-846 8260B1Diisopropyl Ether (DIPE)
ND 2.8 8/15/18 12:22 MFFmg/Kg dry1.5 8/15/18SW-846 8260B11,4-Dioxane
ND 11 8/15/18 12:22 MFFmg/Kg dry1.6 8/15/18SW-846 8260B1Ethanol
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0074 8/15/18SW-846 8260B1Ethylbenzene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.034 8/15/18SW-846 8260B1Hexachlorobutadiene
ND 0.57 8/15/18 12:22 MFFmg/Kg dry0.087 8/15/18SW-846 8260B12-Hexanone (MBK)
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0068 8/15/18SW-846 8260B1Isopropylbenzene (Cumene)
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0085 8/15/18SW-846 8260B1p-Isopropyltoluene (p-Cymene)
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0051 8/15/18SW-846 8260B1Methyl tert-Butyl Ether (MTBE)
ND 0.28 8/15/18 12:22 MFFmg/Kg dry0.18 8/15/18SW-846 8260B1Methylene Chloride
ND 0.57 8/15/18 12:22 MFFmg/Kg dry0.084 8/15/18SW-846 8260B14-Methyl-2-pentanone (MIBK)
ND 0.11 8/15/18 12:22 MFFmg/Kg dry0.0069 8/15/18SW-846 8260B1Naphthalene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0074 8/15/18SW-846 8260B1n-Propylbenzene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0085 8/15/18SW-846 8260B1Styrene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0068 8/15/18SW-846 8260B11,1,1,2-Tetrachloroethane
ND 0.028 8/15/18 12:22 MFFmg/Kg dry0.0091 8/15/18SW-846 8260B11,1,2,2-Tetrachloroethane
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.015 8/15/18SW-846 8260B1Tetrachloroethylene
ND 0.57 8/15/18 12:22 MFFmg/Kg dry0.061 8/15/18SW-846 8260B1Tetrahydrofuran
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0097 8/15/18SW-846 8260B1Toluene
ND 0.28 8/15/18 12:22 MFFmg/Kg dry0.0080 8/15/18SW-846 8260B11,2,3-Trichlorobenzene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.011 8/15/18SW-846 8260B11,2,4-Trichlorobenzene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0097 8/15/18SW-846 8260B11,3,5-Trichlorobenzene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0075 8/15/18SW-846 8260B11,1,1-Trichloroethane
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.013 8/15/18SW-846 8260B11,1,2-Trichloroethane
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.011 8/15/18SW-846 8260B1Trichloroethylene
ND 0.11 8/15/18 12:22 MFFmg/Kg dry0.0084 8/15/18SW-846 8260B1Trichlorofluoromethane (Freon 11)
ND 0.11 8/15/18 12:22 MFFmg/Kg dry0.012 8/15/18SW-846 8260B11,2,3-Trichloropropane
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.011 8/15/18SW-846 8260B11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.010 8/15/18SW-846 8260B11,2,4-Trimethylbenzene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0074 8/15/18SW-846 8260B11,3,5-Trimethylbenzene
ND 0.11 8/15/18 12:22 MFFmg/Kg dry0.0076 8/15/18SW-846 8260B1Vinyl Chloride
ND 0.11 8/15/18 12:22 MFFmg/Kg dry0.015 8/15/18SW-846 8260B1m+p Xylene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0075 8/15/18SW-846 8260B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 91.2 8/15/18 12:2270-130
Toluene-d8 97.7 8/15/18 12:2270-130
4-Bromofluorobenzene 102 8/15/18 12:2270-130
Page 8 of 39
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 8/15/2018
Work Order: 18H0706Sample Description:Project Location: Haw River, NC
Sample ID: 18H0706-01
Field Sample #: SB-1
Sample Matrix: Soil
Sampled: 8/13/2018 17:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.059 8/15/18SW-846 8270D1Acenaphthene
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.066 8/15/18SW-846 8270D1Acenaphthylene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.077 8/15/18SW-846 8270D1Acetophenone
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.11 8/15/18SW-846 8270D1V-34Aniline
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.057 8/15/18SW-846 8270D1Anthracene
ND 0.76 8/15/18 15:01 CDTmg/Kg dry0.49 8/15/18SW-846 8270D1V-04, V-20Benzidine
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.052 8/15/18SW-846 8270D1Benzo(a)anthracene
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.061 8/15/18SW-846 8270D1Benzo(a)pyrene
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.055 8/15/18SW-846 8270D1Benzo(b)fluoranthene
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.087 8/15/18SW-846 8270D1Benzo(g,h,i)perylene
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.061 8/15/18SW-846 8270D1Benzo(k)fluoranthene
ND 1.2 8/15/18 15:01 CDTmg/Kg dry0.21 8/15/18SW-846 8270D1Benzoic Acid
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.075 8/15/18SW-846 8270D1Bis(2-chloroethoxy)methane
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.077 8/15/18SW-846 8270D1Bis(2-chloroethyl)ether
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.084 8/15/18SW-846 8270D1Bis(2-chloroisopropyl)ether
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.15 8/15/18SW-846 8270D1Bis(2-Ethylhexyl)phthalate
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.066 8/15/18SW-846 8270D14-Bromophenylphenylether
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.094 8/15/18SW-846 8270D1Butylbenzylphthalate
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.051 8/15/18SW-846 8270D1Carbazole
ND 0.76 8/15/18 15:01 CDTmg/Kg dry0.090 8/15/18SW-846 8270D1V-344-Chloroaniline
ND 0.76 8/15/18 15:01 CDTmg/Kg dry0.084 8/15/18SW-846 8270D14-Chloro-3-methylphenol
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.074 8/15/18SW-846 8270D12-Chloronaphthalene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.070 8/15/18SW-846 8270D12-Chlorophenol
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.066 8/15/18SW-846 8270D14-Chlorophenylphenylether
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.061 8/15/18SW-846 8270D1Chrysene
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.12 8/15/18SW-846 8270D1Dibenz(a,h)anthracene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.068 8/15/18SW-846 8270D1Dibenzofuran
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.085 8/15/18SW-846 8270D1Di-n-butylphthalate
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.069 8/15/18SW-846 8270D11,2-Dichlorobenzene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.067 8/15/18SW-846 8270D11,3-Dichlorobenzene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.070 8/15/18SW-846 8270D11,4-Dichlorobenzene
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.060 8/15/18SW-846 8270D1V-343,3-Dichlorobenzidine
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.067 8/15/18SW-846 8270D12,4-Dichlorophenol
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.070 8/15/18SW-846 8270D1Diethylphthalate
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.073 8/15/18SW-846 8270D12,4-Dimethylphenol
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.069 8/15/18SW-846 8270D1Dimethylphthalate
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.37 8/15/18SW-846 8270D14,6-Dinitro-2-methylphenol
ND 0.76 8/15/18 15:01 CDTmg/Kg dry0.22 8/15/18SW-846 8270D12,4-Dinitrophenol
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.064 8/15/18SW-846 8270D12,4-Dinitrotoluene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.069 8/15/18SW-846 8270D12,6-Dinitrotoluene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.21 8/15/18SW-846 8270D1Di-n-octylphthalate
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.064 8/15/18SW-846 8270D11,2-Diphenylhydrazine (as Azobenzene)
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.065 8/15/18SW-846 8270D1Fluoranthene
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.064 8/15/18SW-846 8270D1Fluorene
Page 9 of 39
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 8/15/2018
Work Order: 18H0706Sample Description:Project Location: Haw River, NC
Sample ID: 18H0706-01
Field Sample #: SB-1
Sample Matrix: Soil
Sampled: 8/13/2018 17:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.069 8/15/18SW-846 8270D1Hexachlorobenzene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.069 8/15/18SW-846 8270D1Hexachlorobutadiene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.083 8/15/18SW-846 8270D1V-05Hexachlorocyclopentadiene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.079 8/15/18SW-846 8270D1Hexachloroethane
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.14 8/15/18SW-846 8270D1Indeno(1,2,3-cd)pyrene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.076 8/15/18SW-846 8270D1Isophorone
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.075 8/15/18SW-846 8270D11-Methylnaphthalene
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.068 8/15/18SW-846 8270D12-Methylnaphthalene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.098 8/15/18SW-846 8270D12-Methylphenol
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.12 8/15/18SW-846 8270D13/4-Methylphenol
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.10 8/15/18SW-846 8270D1Naphthalene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.066 8/15/18SW-846 8270D12-Nitroaniline
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.057 8/15/18SW-846 8270D1V-343-Nitroaniline
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.066 8/15/18SW-846 8270D14-Nitroaniline
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.074 8/15/18SW-846 8270D1Nitrobenzene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.10 8/15/18SW-846 8270D12-Nitrophenol
ND 0.76 8/15/18 15:01 CDTmg/Kg dry0.085 8/15/18SW-846 8270D14-Nitrophenol
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.25 8/15/18SW-846 8270D1N-Nitrosodimethylamine
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.081 8/15/18SW-846 8270D1N-Nitrosodiphenylamine
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.081 8/15/18SW-846 8270D1N-Nitrosodi-n-propylamine
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.094 8/15/18SW-846 8270D1Pentachloronitrobenzene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.095 8/15/18SW-846 8270D1Pentachlorophenol
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.10 8/15/18SW-846 8270D1Phenanthrene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.067 8/15/18SW-846 8270D1Phenol
0.080 0.20 8/15/18 15:01 CDTmg/Kg dry0.065 8/15/18SW-846 8270D1JPyrene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.064 8/15/18SW-846 8270D1Pyridine
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.070 8/15/18SW-846 8270D11,2,4,5-Tetrachlorobenzene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.070 8/15/18SW-846 8270D11,2,4-Trichlorobenzene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.089 8/15/18SW-846 8270D12,4,5-Trichlorophenol
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.066 8/15/18SW-846 8270D12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 63.7 8/15/18 15:0130-130
Phenol-d6 64.5 8/15/18 15:0130-130
Nitrobenzene-d5 63.4 8/15/18 15:0130-130
2-Fluorobiphenyl 72.7 8/15/18 15:0130-130
2,4,6-Tribromophenol 62.0 8/15/18 15:0130-130
p-Terphenyl-d14 76.4 8/15/18 15:0130-130
Page 10 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 8/15/2018
Work Order: 18H0706Sample Description:Project Location: Haw River, NC
Sample ID: 18H0706-01
Field Sample #: SB-1
Sample Matrix: Soil
Sampled: 8/13/2018 17:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - EPH
380 58 8/16/18 9:36 RMWmg/Kg dry 8/15/18MADEP-EPH-04-1.15C9-C18 Aliphatics
130 12 8/16/18 4:45 RMWmg/Kg dry 8/15/18MADEP-EPH-04-1.11C19-C36 Aliphatics
160 12 8/16/18 4:45 RMWmg/Kg dry 8/15/18MADEP-EPH-04-1.11Unadjusted C11-C22 Aromatics
160 12 8/16/18 4:45 RMWmg/Kg dry 8/15/18MADEP-EPH-04-1.11C11-C22 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD)74.5 8/16/18 4:4540-140
o-Terphenyl (OTP)74.4 8/16/18 4:4540-140
2-Bromonaphthalene 94.2 8/16/18 4:4540-140
2-Fluorobiphenyl 81.0 8/16/18 4:4540-140
Page 11 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 8/15/2018
Work Order: 18H0706Sample Description:Project Location: Haw River, NC
Sample ID: 18H0706-01
Field Sample #: SB-1
Sample Matrix: Soil
Sampled: 8/13/2018 17:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Soil/Methanol Preservation Ratio: 1.17
Petroleum Hydrocarbons Analyses - VPH
ND 11 8/15/18 11:27 EEHmg/Kg dry 8/15/18MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 11 8/15/18 11:27 EEHmg/Kg dry 8/15/18MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
59 11 8/15/18 11:27 EEHmg/Kg dry 8/15/18MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
26 11 8/15/18 11:27 EEHmg/Kg dry 8/15/18MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
33 11 8/15/18 11:27 EEHmg/Kg dry 8/15/18MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)80.4 8/15/18 11:2770-130
2,5-Dibromotoluene (PID)80.1 8/15/18 11:2770-130
Page 12 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 8/15/2018
Work Order: 18H0706Sample Description:Project Location: Haw River, NC
Sample ID: 18H0706-01
Field Sample #: SB-1
Sample Matrix: Soil
Sampled: 8/13/2018 17:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
86.3 8/15/18 17:56 JFC% Wt 8/15/18SM 2540G1% Solids
Page 13 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: SW-846 3546-MADEP-EPH-04-1.1
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B210344 08/15/1820.0 2.0018H0706-01 [SB-1]
Prep Method: MA VPH-MADEP-VPH-Feb 2018 Rev 2.1
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B209997 08/15/185.90 5.8018H0706-01 [SB-1]
Prep Method: % Solids-SM 2540G
Lab Number [Field ID]Batch Date
B210372 08/15/1818H0706-01 [SB-1]
Prep Method: SW-846 5035/5030B-SW-846 8260B
Lab Number [Field ID]Batch
Sample
Amount(g)
Methanol
Volume(mL)
Methanol
Aliquot(mL)
Final
Volume(mL)Date
18H0706-01 [SB-1]B210357 5.90 5.80 1 50 08/15/18
Prep Method: SW-846 3546-SW-846 8270D
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B210345 08/15/1830.1 1.0018H0706-01 [SB-1]
[TOC_1]Sample Preparation Information[TOC]
Page 14 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Volatile Organic Compounds by GC/MS[TOC]
Batch B210357 - SW-846 5035/5030B
[TOC_3]B210357[TOC]
Blank (B210357-BLK1) Prepared & Analyzed: 08/15/18
Acetone mg/Kg wet2.5ND
Acrylonitrile mg/Kg wet0.25ND
tert-Amyl Methyl Ether (TAME)mg/Kg wet0.025ND
Benzene mg/Kg wet0.050ND
Bromobenzene mg/Kg wet0.050ND
Bromochloromethane mg/Kg wet0.050ND
Bromodichloromethane mg/Kg wet0.050ND
Bromoform mg/Kg wet0.10ND
Bromomethane mg/Kg wet0.10ND
2-Butanone (MEK)mg/Kg wet1.0ND
tert-Butyl Alcohol (TBA)mg/Kg wet1.0ND
n-Butylbenzene mg/Kg wet0.050ND
sec-Butylbenzene mg/Kg wet0.050ND
tert-Butylbenzene mg/Kg wet0.050ND
tert-Butyl Ethyl Ether (TBEE)mg/Kg wet0.025ND
Carbon Disulfide mg/Kg wet0.15ND
Carbon Tetrachloride mg/Kg wet0.050ND
Chlorobenzene mg/Kg wet0.050ND
Chlorodibromomethane mg/Kg wet0.025ND
Chloroethane mg/Kg wet0.10ND
Chloroform mg/Kg wet0.10ND
Chloromethane mg/Kg wet0.10ND
2-Chlorotoluene mg/Kg wet0.050ND
4-Chlorotoluene mg/Kg wet0.050ND
1,2-Dibromo-3-chloropropane (DBCP)mg/Kg wet0.25ND
1,2-Dibromoethane (EDB)mg/Kg wet0.025ND
Dibromomethane mg/Kg wet0.050ND
1,2-Dichlorobenzene mg/Kg wet0.050ND
1,3-Dichlorobenzene mg/Kg wet0.050ND
1,4-Dichlorobenzene mg/Kg wet0.050ND
trans-1,4-Dichloro-2-butene mg/Kg wet0.10ND
Dichlorodifluoromethane (Freon 12)mg/Kg wet0.10ND
1,1-Dichloroethane mg/Kg wet0.050ND
1,2-Dichloroethane mg/Kg wet0.050ND
1,1-Dichloroethylene mg/Kg wet0.050ND
cis-1,2-Dichloroethylene mg/Kg wet0.050ND
trans-1,2-Dichloroethylene mg/Kg wet0.050ND
1,2-Dichloropropane mg/Kg wet0.050ND
1,3-Dichloropropane mg/Kg wet0.025ND
2,2-Dichloropropane mg/Kg wet0.050ND
1,1-Dichloropropene mg/Kg wet0.10ND
cis-1,3-Dichloropropene mg/Kg wet0.025ND
trans-1,3-Dichloropropene mg/Kg wet0.025ND
Diethyl Ether mg/Kg wet0.10ND
Diisopropyl Ether (DIPE)mg/Kg wet0.025ND
1,4-Dioxane mg/Kg wet2.5ND
Ethanol mg/Kg wet0.20ND
Ethylbenzene mg/Kg wet0.050ND
Hexachlorobutadiene mg/Kg wet0.050ND
2-Hexanone (MBK)mg/Kg wet0.50ND
Isopropylbenzene (Cumene)mg/Kg wet0.050ND
p-Isopropyltoluene (p-Cymene)mg/Kg wet0.050ND
[TOC_1]QC Data[TOC]
Page 15 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B210357 - SW-846 5035/5030B
Blank (B210357-BLK1) Prepared & Analyzed: 08/15/18
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.050ND
Methylene Chloride mg/Kg wet0.25ND
4-Methyl-2-pentanone (MIBK)mg/Kg wet0.50ND
Naphthalene mg/Kg wet0.10ND
n-Propylbenzene mg/Kg wet0.050ND
Styrene mg/Kg wet0.050ND
1,1,1,2-Tetrachloroethane mg/Kg wet0.050ND
1,1,2,2-Tetrachloroethane mg/Kg wet0.025ND
Tetrachloroethylene mg/Kg wet0.050ND
Tetrahydrofuran mg/Kg wet0.50ND
Toluene mg/Kg wet0.050ND
1,2,3-Trichlorobenzene mg/Kg wet0.25ND
1,2,4-Trichlorobenzene mg/Kg wet0.050ND
1,3,5-Trichlorobenzene mg/Kg wet0.050ND
1,1,1-Trichloroethane mg/Kg wet0.050ND
1,1,2-Trichloroethane mg/Kg wet0.050ND
Trichloroethylene mg/Kg wet0.050ND
Trichlorofluoromethane (Freon 11)mg/Kg wet0.10ND
1,2,3-Trichloropropane mg/Kg wet0.10ND
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
mg/Kg wet0.050ND
1,2,4-Trimethylbenzene mg/Kg wet0.050ND
1,3,5-Trimethylbenzene mg/Kg wet0.050ND
Vinyl Chloride mg/Kg wet0.10ND
m+p Xylene mg/Kg wet0.10ND
o-Xylene mg/Kg wet0.050ND
mg/Kg wet 0.0250 70-130Surrogate: 1,2-Dichloroethane-d4 89.00.0222
mg/Kg wet 0.0250 70-130Surrogate: Toluene-d8 97.20.0243
mg/Kg wet 0.0250 70-130Surrogate: 4-Bromofluorobenzene 95.60.0239
LCS (B210357-BS1) Prepared & Analyzed: 08/15/18
Acetone mg/Kg wet0.057 0.113 70-16091.40.104
Acrylonitrile mg/Kg wet0.0057 0.0113 70-13086.70.00983
tert-Amyl Methyl Ether (TAME)mg/Kg wet0.00057 0.0113 70-13089.50.0101
Benzene mg/Kg wet0.0011 0.0113 70-13092.90.0105
Bromobenzene mg/Kg wet0.0011 0.0113 70-13098.20.0111
Bromochloromethane mg/Kg wet0.0011 0.0113 70-13095.80.0109
Bromodichloromethane mg/Kg wet0.0011 0.0113 70-13097.20.0110
Bromoform mg/Kg wet0.0023 0.0113 70-1301000.0113
Bromomethane mg/Kg wet0.0023 0.0113 40-13087.80.00995
2-Butanone (MEK)mg/Kg wet0.023 0.113 70-16077.10.0874
tert-Butyl Alcohol (TBA)mg/Kg wet0.023 0.113 40-13098.40.112
n-Butylbenzene mg/Kg wet0.0011 0.0113 70-1301030.0116
sec-Butylbenzene mg/Kg wet0.0011 0.0113 70-1301060.0120
tert-Butylbenzene mg/Kg wet0.0011 0.0113 70-1601030.0117
tert-Butyl Ethyl Ether (TBEE)mg/Kg wet0.00057 0.0113 70-13080.90.00917
Carbon Disulfide mg/Kg wet0.0034 0.0113 70-1301130.0128
Carbon Tetrachloride mg/Kg wet0.0011 0.0113 70-13091.60.0104
Chlorobenzene mg/Kg wet0.0011 0.0113 70-1301020.0115
Chlorodibromomethane mg/Kg wet0.00057 0.0113 70-1301030.0117
Chloroethane mg/Kg wet0.0023 0.0113 70-13093.90.0106
Chloroform mg/Kg wet0.0023 0.0113 70-13098.60.0112
Chloromethane mg/Kg wet0.0023 0.0113 70-13074.90.00849
Page 16 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B210357 - SW-846 5035/5030B
LCS (B210357-BS1) Prepared & Analyzed: 08/15/18
2-Chlorotoluene mg/Kg wet0.0011 0.0113 70-1301000.0113
4-Chlorotoluene mg/Kg wet0.0011 0.0113 70-13099.40.0113
1,2-Dibromo-3-chloropropane (DBCP)mg/Kg wet0.0057 0.0113 70-13097.90.0111
1,2-Dibromoethane (EDB)mg/Kg wet0.00057 0.0113 70-1301050.0119
Dibromomethane mg/Kg wet0.0011 0.0113 70-1301050.0119
1,2-Dichlorobenzene mg/Kg wet0.0011 0.0113 70-1301030.0117
1,3-Dichlorobenzene mg/Kg wet0.0011 0.0113 70-1301070.0121
1,4-Dichlorobenzene mg/Kg wet0.0011 0.0113 70-13098.60.0112
trans-1,4-Dichloro-2-butene mg/Kg wet0.0023 0.0113 70-13082.90.00940
Dichlorodifluoromethane (Freon 12)mg/Kg wet0.0023 0.0113 40-16084.00.00952
1,1-Dichloroethane mg/Kg wet0.0011 0.0113 70-13092.20.0104
1,2-Dichloroethane mg/Kg wet0.0011 0.0113 70-13088.20.0100
1,1-Dichloroethylene mg/Kg wet0.0011 0.0113 70-1301010.0115
cis-1,2-Dichloroethylene mg/Kg wet0.0011 0.0113 70-13087.30.00989
trans-1,2-Dichloroethylene mg/Kg wet0.0011 0.0113 70-13091.50.0104
1,2-Dichloropropane mg/Kg wet0.0011 0.0113 70-13095.90.0109
1,3-Dichloropropane mg/Kg wet0.00057 0.0113 70-13087.80.00995
2,2-Dichloropropane mg/Kg wet0.0011 0.0113 70-13083.40.00945
1,1-Dichloropropene mg/Kg wet0.0023 0.0113 70-13089.10.0101
cis-1,3-Dichloropropene mg/Kg wet0.00057 0.0113 70-13093.00.0105
trans-1,3-Dichloropropene mg/Kg wet0.00057 0.0113 70-13093.90.0106
Diethyl Ether mg/Kg wet0.0023 0.0113 70-13094.90.0108
Diisopropyl Ether (DIPE)mg/Kg wet0.00057 0.0113 70-13075.80.00859
1,4-Dioxane mg/Kg wet0.057 0.113 40-16098.00.111
Ethylbenzene mg/Kg wet0.0011 0.0113 70-1301040.0118
Hexachlorobutadiene mg/Kg wet0.0011 0.0113 70-1601120.0127
2-Hexanone (MBK)mg/Kg wet0.011 0.113 70-16083.10.0942
Isopropylbenzene (Cumene)mg/Kg wet0.0011 0.0113 70-1301100.0125
p-Isopropyltoluene (p-Cymene)mg/Kg wet0.0011 0.0113 70-1301050.0119
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.0011 0.0113 70-13096.20.0109
Methylene Chloride mg/Kg wet0.0057 0.0113 40-16090.20.0102
4-Methyl-2-pentanone (MIBK)mg/Kg wet0.011 0.113 70-16082.50.0935
Naphthalene mg/Kg wet0.0023 0.0113 40-1301040.0118
n-Propylbenzene mg/Kg wet0.0011 0.0113 70-1301030.0117
Styrene mg/Kg wet0.0011 0.0113 70-1301040.0118
1,1,1,2-Tetrachloroethane mg/Kg wet0.0011 0.0113 70-1301090.0124
1,1,2,2-Tetrachloroethane mg/Kg wet0.00057 0.0113 70-1301050.0119
Tetrachloroethylene mg/Kg wet0.0011 0.0113 70-1301050.0119
Tetrahydrofuran mg/Kg wet0.011 0.0113 J70-13078.90.00894
Toluene mg/Kg wet0.0011 0.0113 70-1301020.0116
1,2,3-Trichlorobenzene mg/Kg wet0.0057 0.0113 70-1301040.0118
1,2,4-Trichlorobenzene mg/Kg wet0.0011 0.0113 70-13099.60.0113
1,3,5-Trichlorobenzene mg/Kg wet0.0011 0.0113 70-13099.90.0113
1,1,1-Trichloroethane mg/Kg wet0.0011 0.0113 70-13098.40.0112
1,1,2-Trichloroethane mg/Kg wet0.0011 0.0113 70-1301040.0117
Trichloroethylene mg/Kg wet0.0011 0.0113 70-1301020.0116
Trichlorofluoromethane (Freon 11)mg/Kg wet0.0023 0.0113 70-13099.00.0112
1,2,3-Trichloropropane mg/Kg wet0.0023 0.0113 70-13075.90.00860
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
mg/Kg wet0.0011 0.0113 70-1301120.0127
1,2,4-Trimethylbenzene mg/Kg wet0.0011 0.0113 70-13098.60.0112
1,3,5-Trimethylbenzene mg/Kg wet0.0011 0.0113 70-13099.80.0113
Page 17 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B210357 - SW-846 5035/5030B
LCS (B210357-BS1) Prepared & Analyzed: 08/15/18
Vinyl Chloride mg/Kg wet0.0023 0.0113 40-13086.80.00984
m+p Xylene mg/Kg wet0.0023 0.0227 70-1301010.0230
o-Xylene mg/Kg wet0.0011 0.0113 70-1301020.0115
mg/Kg wet 0.0283 70-130Surrogate: 1,2-Dichloroethane-d4 89.00.0252
mg/Kg wet 0.0283 70-130Surrogate: Toluene-d8 99.70.0283
mg/Kg wet 0.0283 70-130Surrogate: 4-Bromofluorobenzene 96.90.0274
LCS Dup (B210357-BSD1) Prepared & Analyzed: 08/15/18
Acetone mg/Kg wet0.057 0.113 2570-16089.9 1.620.102
Acrylonitrile mg/Kg wet0.0057 0.0113 2570-13081.4 6.310.00923
tert-Amyl Methyl Ether (TAME)mg/Kg wet0.00057 0.0113 2570-13088.5 1.120.0100
Benzene mg/Kg wet0.0011 0.0113 2570-13092.3 0.6480.0105
Bromobenzene mg/Kg wet0.0011 0.0113 2570-13099.5 1.320.0113
Bromochloromethane mg/Kg wet0.0011 0.0113 2570-13095.3 0.5230.0108
Bromodichloromethane mg/Kg wet0.0011 0.0113 2570-13094.6 2.710.0107
Bromoform mg/Kg wet0.0023 0.0113 2570-130104 3.730.0118
Bromomethane mg/Kg wet0.0023 0.0113 2540-130104 16.70.0118
2-Butanone (MEK)mg/Kg wet0.023 0.113 2570-16074.6 3.340.0845
tert-Butyl Alcohol (TBA)mg/Kg wet0.023 0.113 2540-13090.3 8.640.102
n-Butylbenzene mg/Kg wet0.0011 0.0113 2570-130102 0.1950.0116
sec-Butylbenzene mg/Kg wet0.0011 0.0113 2570-130105 0.7610.0119
tert-Butylbenzene mg/Kg wet0.0011 0.0113 2570-160101 2.550.0114
tert-Butyl Ethyl Ether (TBEE)mg/Kg wet0.00057 0.0113 2570-13080.9 0.000.00917
Carbon Disulfide mg/Kg wet0.0034 0.0113 2570-130105 7.890.0119
Carbon Tetrachloride mg/Kg wet0.0011 0.0113 2570-13090.3 1.430.0102
Chlorobenzene mg/Kg wet0.0011 0.0113 2570-130103 0.9800.0116
Chlorodibromomethane mg/Kg wet0.00057 0.0113 2570-130103 0.1950.0116
Chloroethane mg/Kg wet0.0023 0.0113 2570-13091.6 2.480.0104
Chloroform mg/Kg wet0.0023 0.0113 2570-13098.2 0.4070.0111
Chloromethane mg/Kg wet0.0023 0.0113 2570-13073.8 1.480.00836
2-Chlorotoluene mg/Kg wet0.0011 0.0113 2570-13097.2 2.840.0110
4-Chlorotoluene mg/Kg wet0.0011 0.0113 2570-13097.4 2.030.0110
1,2-Dibromo-3-chloropropane (DBCP)mg/Kg wet0.0057 0.0113 2570-13087.0 11.80.00986
1,2-Dibromoethane (EDB)mg/Kg wet0.00057 0.0113 2570-130100 4.960.0114
Dibromomethane mg/Kg wet0.0011 0.0113 2570-130105 0.4750.0119
1,2-Dichlorobenzene mg/Kg wet0.0011 0.0113 2570-130102 1.070.0115
1,3-Dichlorobenzene mg/Kg wet0.0011 0.0113 2570-130107 0.09360.0121
1,4-Dichlorobenzene mg/Kg wet0.0011 0.0113 2570-13096.8 1.840.0110
trans-1,4-Dichloro-2-butene mg/Kg wet0.0023 0.0113 2570-13078.2 5.830.00886
Dichlorodifluoromethane (Freon 12)mg/Kg wet0.0023 0.0113 2540-16084.9 1.070.00962
1,1-Dichloroethane mg/Kg wet0.0011 0.0113 2570-13091.4 0.8710.0104
1,2-Dichloroethane mg/Kg wet0.0011 0.0113 2570-13088.9 0.7900.0101
1,1-Dichloroethylene mg/Kg wet0.0011 0.0113 2570-13098.0 3.210.0111
cis-1,2-Dichloroethylene mg/Kg wet0.0011 0.0113 2570-13085.4 2.200.00968
trans-1,2-Dichloroethylene mg/Kg wet0.0011 0.0113 2570-13090.1 1.540.0102
1,2-Dichloropropane mg/Kg wet0.0011 0.0113 2570-13094.2 1.790.0107
1,3-Dichloropropane mg/Kg wet0.00057 0.0113 2570-13089.6 2.030.0102
2,2-Dichloropropane mg/Kg wet0.0011 0.0113 2570-13081.7 2.060.00926
1,1-Dichloropropene mg/Kg wet0.0023 0.0113 2570-13090.2 1.230.0102
cis-1,3-Dichloropropene mg/Kg wet0.00057 0.0113 2570-13091.4 1.740.0104
trans-1,3-Dichloropropene mg/Kg wet0.00057 0.0113 2570-13093.4 0.5340.0106
Diethyl Ether mg/Kg wet0.0023 0.0113 2570-13093.5 1.490.0106
Page 18 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B210357 - SW-846 5035/5030B
LCS Dup (B210357-BSD1) Prepared & Analyzed: 08/15/18
Diisopropyl Ether (DIPE)mg/Kg wet0.00057 0.0113 2570-13075.3 0.6620.00853
1,4-Dioxane mg/Kg wet0.057 0.113 5040-16093.2 5.040.106
Ethylbenzene mg/Kg wet0.0011 0.0113 2570-130106 1.810.0120
Hexachlorobutadiene mg/Kg wet0.0011 0.0113 2570-160109 2.630.0123
2-Hexanone (MBK)mg/Kg wet0.011 0.113 2570-16079.4 4.620.0900
Isopropylbenzene (Cumene)mg/Kg wet0.0011 0.0113 2570-130110 0.2720.0125
p-Isopropyltoluene (p-Cymene)mg/Kg wet0.0011 0.0113 2570-130104 1.150.0117
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.0011 0.0113 2570-13094.7 1.570.0107
Methylene Chloride mg/Kg wet0.0057 0.0113 2540-16089.7 0.5560.0102
4-Methyl-2-pentanone (MIBK)mg/Kg wet0.011 0.113 2570-16080.5 2.450.0913
Naphthalene mg/Kg wet0.0023 0.0113 2540-130102 1.840.0116
n-Propylbenzene mg/Kg wet0.0011 0.0113 2570-130101 1.960.0114
Styrene mg/Kg wet0.0011 0.0113 2570-130106 1.530.0120
1,1,1,2-Tetrachloroethane mg/Kg wet0.0011 0.0113 2570-130103 6.040.0117
1,1,2,2-Tetrachloroethane mg/Kg wet0.00057 0.0113 2570-130104 0.6680.0118
Tetrachloroethylene mg/Kg wet0.0011 0.0113 2570-130107 1.510.0121
Tetrahydrofuran mg/Kg wet0.011 0.0113 25 J70-13072.4 8.590.00821
Toluene mg/Kg wet0.0011 0.0113 2570-130101 1.380.0114
1,2,3-Trichlorobenzene mg/Kg wet0.0057 0.0113 2570-130104 0.09600.0118
1,2,4-Trichlorobenzene mg/Kg wet0.0011 0.0113 2570-130101 1.490.0115
1,3,5-Trichlorobenzene mg/Kg wet0.0011 0.0113 2570-13097.2 2.740.0110
1,1,1-Trichloroethane mg/Kg wet0.0011 0.0113 2570-13097.5 0.9190.0110
1,1,2-Trichloroethane mg/Kg wet0.0011 0.0113 2570-130105 1.250.0119
Trichloroethylene mg/Kg wet0.0011 0.0113 2570-13099.9 2.180.0113
Trichlorofluoromethane (Freon 11)mg/Kg wet0.0023 0.0113 2570-13096.4 2.660.0109
1,2,3-Trichloropropane mg/Kg wet0.0023 0.0113 2570-13077.8 2.470.00882
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
mg/Kg wet0.0011 0.0113 2570-130107 4.830.0121
1,2,4-Trimethylbenzene mg/Kg wet0.0011 0.0113 2570-13096.7 1.950.0110
1,3,5-Trimethylbenzene mg/Kg wet0.0011 0.0113 2570-13098.7 1.110.0112
Vinyl Chloride mg/Kg wet0.0023 0.0113 2540-13085.9 1.040.00974
m+p Xylene mg/Kg wet0.0023 0.0227 2570-130102 0.2460.0231
o-Xylene mg/Kg wet0.0011 0.0113 2570-130102 0.1960.0116
mg/Kg wet 0.0283 70-130Surrogate: 1,2-Dichloroethane-d4 88.90.0252
mg/Kg wet 0.0283 70-130Surrogate: Toluene-d8 98.80.0280
mg/Kg wet 0.0283 70-130Surrogate: 4-Bromofluorobenzene 96.50.0273
Page 19 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Semivolatile Organic Compounds by GC/MS[TOC]
Batch B210345 - SW-846 3546
[TOC_3]B210345[TOC]
Blank (B210345-BLK1) Prepared & Analyzed: 08/15/18
Acenaphthene mg/Kg wet0.17ND
Acenaphthylene mg/Kg wet0.17ND
Acetophenone mg/Kg wet0.34ND
Aniline mg/Kg wet0.34 V-34ND
Anthracene mg/Kg wet0.17ND
Benzidine mg/Kg wet0.66 V-04, V-20ND
Benzo(a)anthracene mg/Kg wet0.17ND
Benzo(a)pyrene mg/Kg wet0.17ND
Benzo(b)fluoranthene mg/Kg wet0.17ND
Benzo(g,h,i)perylene mg/Kg wet0.17ND
Benzo(k)fluoranthene mg/Kg wet0.17ND
Benzoic Acid mg/Kg wet1.0ND
Bis(2-chloroethoxy)methane mg/Kg wet0.34ND
Bis(2-chloroethyl)ether mg/Kg wet0.34ND
Bis(2-chloroisopropyl)ether mg/Kg wet0.34ND
Bis(2-Ethylhexyl)phthalate mg/Kg wet0.34ND
4-Bromophenylphenylether mg/Kg wet0.34ND
Butylbenzylphthalate mg/Kg wet0.34ND
Carbazole mg/Kg wet0.17ND
4-Chloroaniline mg/Kg wet0.66 V-34ND
4-Chloro-3-methylphenol mg/Kg wet0.66ND
2-Chloronaphthalene mg/Kg wet0.34ND
2-Chlorophenol mg/Kg wet0.34ND
4-Chlorophenylphenylether mg/Kg wet0.34ND
Chrysene mg/Kg wet0.17ND
Dibenz(a,h)anthracene mg/Kg wet0.17ND
Dibenzofuran mg/Kg wet0.34ND
Di-n-butylphthalate mg/Kg wet0.34ND
1,2-Dichlorobenzene mg/Kg wet0.34ND
1,3-Dichlorobenzene mg/Kg wet0.34ND
1,4-Dichlorobenzene mg/Kg wet0.34ND
3,3-Dichlorobenzidine mg/Kg wet0.17 V-34ND
2,4-Dichlorophenol mg/Kg wet0.34ND
Diethylphthalate mg/Kg wet0.34ND
2,4-Dimethylphenol mg/Kg wet0.34ND
Dimethylphthalate mg/Kg wet0.34ND
4,6-Dinitro-2-methylphenol mg/Kg wet0.34ND
2,4-Dinitrophenol mg/Kg wet0.66ND
2,4-Dinitrotoluene mg/Kg wet0.34ND
2,6-Dinitrotoluene mg/Kg wet0.34ND
Di-n-octylphthalate mg/Kg wet0.34ND
1,2-Diphenylhydrazine (as Azobenzene)mg/Kg wet0.34ND
Fluoranthene mg/Kg wet0.17ND
Fluorene mg/Kg wet0.17ND
Hexachlorobenzene mg/Kg wet0.34ND
Hexachlorobutadiene mg/Kg wet0.34ND
Hexachlorocyclopentadiene mg/Kg wet0.34 V-05ND
Hexachloroethane mg/Kg wet0.34ND
Indeno(1,2,3-cd)pyrene mg/Kg wet0.17ND
Isophorone mg/Kg wet0.34ND
1-Methylnaphthalene mg/Kg wet0.17ND
2-Methylnaphthalene mg/Kg wet0.17ND
Page 20 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B210345 - SW-846 3546
Blank (B210345-BLK1) Prepared & Analyzed: 08/15/18
2-Methylphenol mg/Kg wet0.34ND
3/4-Methylphenol mg/Kg wet0.34ND
Naphthalene mg/Kg wet0.17ND
2-Nitroaniline mg/Kg wet0.34ND
3-Nitroaniline mg/Kg wet0.34 V-34ND
4-Nitroaniline mg/Kg wet0.34ND
Nitrobenzene mg/Kg wet0.34ND
2-Nitrophenol mg/Kg wet0.34ND
4-Nitrophenol mg/Kg wet0.66ND
N-Nitrosodimethylamine mg/Kg wet0.34ND
N-Nitrosodiphenylamine mg/Kg wet0.34ND
N-Nitrosodi-n-propylamine mg/Kg wet0.34ND
Pentachloronitrobenzene mg/Kg wet0.34ND
Pentachlorophenol mg/Kg wet0.34ND
Phenanthrene mg/Kg wet0.17ND
Phenol mg/Kg wet0.34ND
Pyrene mg/Kg wet0.17ND
Pyridine mg/Kg wet0.34ND
1,2,4,5-Tetrachlorobenzene mg/Kg wet0.34ND
1,2,4-Trichlorobenzene mg/Kg wet0.34ND
2,4,5-Trichlorophenol mg/Kg wet0.34ND
2,4,6-Trichlorophenol mg/Kg wet0.34ND
mg/Kg wet 6.67 30-130Surrogate: 2-Fluorophenol 79.25.28
mg/Kg wet 6.67 30-130Surrogate: Phenol-d6 80.25.35
mg/Kg wet 3.33 30-130Surrogate: Nitrobenzene-d5 73.22.44
mg/Kg wet 3.33 30-130Surrogate: 2-Fluorobiphenyl 85.02.83
mg/Kg wet 6.67 30-130Surrogate: 2,4,6-Tribromophenol 76.15.08
mg/Kg wet 3.33 30-130Surrogate: p-Terphenyl-d14 1033.44
LCS (B210345-BS1) Prepared & Analyzed: 08/15/18
Acenaphthene mg/Kg wet0.17 1.67 40-14073.01.22
Acenaphthylene mg/Kg wet0.17 1.67 40-14073.11.22
Acetophenone mg/Kg wet0.34 1.67 40-14073.11.22
Aniline mg/Kg wet0.34 1.67 V-3410-14071.71.19
Anthracene mg/Kg wet0.17 1.67 40-14083.01.38
Benzidine mg/Kg wet0.66 1.67 V-04, V-0640-1401382.29
Benzo(a)anthracene mg/Kg wet0.17 1.67 40-14078.41.31
Benzo(a)pyrene mg/Kg wet0.17 1.67 40-14081.11.35
Benzo(b)fluoranthene mg/Kg wet0.17 1.67 40-14070.61.18
Benzo(g,h,i)perylene mg/Kg wet0.17 1.67 40-14077.21.29
Benzo(k)fluoranthene mg/Kg wet0.17 1.67 40-14076.41.27
Benzoic Acid mg/Kg wet1.0 1.67 30-13073.21.22
Bis(2-chloroethoxy)methane mg/Kg wet0.34 1.67 40-14077.51.29
Bis(2-chloroethyl)ether mg/Kg wet0.34 1.67 40-14070.41.17
Bis(2-chloroisopropyl)ether mg/Kg wet0.34 1.67 40-14087.51.46
Bis(2-Ethylhexyl)phthalate mg/Kg wet0.34 1.67 40-14090.21.50
4-Bromophenylphenylether mg/Kg wet0.34 1.67 40-14074.11.24
Butylbenzylphthalate mg/Kg wet0.34 1.67 40-14087.61.46
Carbazole mg/Kg wet0.17 1.67 40-14077.31.29
4-Chloroaniline mg/Kg wet0.66 1.67 V-3410-14060.01.00
4-Chloro-3-methylphenol mg/Kg wet0.66 1.67 30-13081.11.35
2-Chloronaphthalene mg/Kg wet0.34 1.67 40-14063.51.06
Page 21 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B210345 - SW-846 3546
LCS (B210345-BS1) Prepared & Analyzed: 08/15/18
2-Chlorophenol mg/Kg wet0.34 1.67 30-13075.11.25
4-Chlorophenylphenylether mg/Kg wet0.34 1.67 40-14070.91.18
Chrysene mg/Kg wet0.17 1.67 40-14078.91.31
Dibenz(a,h)anthracene mg/Kg wet0.17 1.67 40-14077.41.29
Dibenzofuran mg/Kg wet0.34 1.67 40-14074.31.24
Di-n-butylphthalate mg/Kg wet0.34 1.67 40-14082.21.37
1,2-Dichlorobenzene mg/Kg wet0.34 1.67 40-14070.81.18
1,3-Dichlorobenzene mg/Kg wet0.34 1.67 40-14066.91.12
1,4-Dichlorobenzene mg/Kg wet0.34 1.67 40-14067.21.12
3,3-Dichlorobenzidine mg/Kg wet0.17 1.67 V-3420-14069.81.16
2,4-Dichlorophenol mg/Kg wet0.34 1.67 30-13076.01.27
Diethylphthalate mg/Kg wet0.34 1.67 40-14070.51.18
2,4-Dimethylphenol mg/Kg wet0.34 1.67 30-13085.31.42
Dimethylphthalate mg/Kg wet0.34 1.67 40-14072.41.21
4,6-Dinitro-2-methylphenol mg/Kg wet0.34 1.67 30-13074.01.23
2,4-Dinitrophenol mg/Kg wet0.66 1.67 30-13056.80.947
2,4-Dinitrotoluene mg/Kg wet0.34 1.67 40-14074.01.23
2,6-Dinitrotoluene mg/Kg wet0.34 1.67 40-14080.51.34
Di-n-octylphthalate mg/Kg wet0.34 1.67 40-14090.21.50
1,2-Diphenylhydrazine (as Azobenzene)mg/Kg wet0.34 1.67 40-14080.41.34
Fluoranthene mg/Kg wet0.17 1.67 40-14076.91.28
Fluorene mg/Kg wet0.17 1.67 40-14072.31.20
Hexachlorobenzene mg/Kg wet0.34 1.67 40-14071.81.20
Hexachlorobutadiene mg/Kg wet0.34 1.67 40-14069.51.16
Hexachlorocyclopentadiene mg/Kg wet0.34 1.67 L-07, V-0540-14038.4 *0.640
Hexachloroethane mg/Kg wet0.34 1.67 40-14067.01.12
Indeno(1,2,3-cd)pyrene mg/Kg wet0.17 1.67 40-14073.31.22
Isophorone mg/Kg wet0.34 1.67 40-14077.81.30
1-Methylnaphthalene mg/Kg wet0.17 1.67 40-14081.71.36
2-Methylnaphthalene mg/Kg wet0.17 1.67 40-14082.41.37
2-Methylphenol mg/Kg wet0.34 1.67 30-13071.01.18
3/4-Methylphenol mg/Kg wet0.34 1.67 30-13084.81.41
Naphthalene mg/Kg wet0.17 1.67 40-14074.11.23
2-Nitroaniline mg/Kg wet0.34 1.67 40-14070.71.18
3-Nitroaniline mg/Kg wet0.34 1.67 V-3430-14071.11.19
4-Nitroaniline mg/Kg wet0.34 1.67 40-14074.71.24
Nitrobenzene mg/Kg wet0.34 1.67 40-14069.21.15
2-Nitrophenol mg/Kg wet0.34 1.67 30-13080.01.33
4-Nitrophenol mg/Kg wet0.66 1.67 30-13076.11.27
N-Nitrosodimethylamine mg/Kg wet0.34 1.67 40-14064.71.08
N-Nitrosodiphenylamine mg/Kg wet0.34 1.67 40-14098.31.64
N-Nitrosodi-n-propylamine mg/Kg wet0.34 1.67 40-14069.01.15
Pentachloronitrobenzene mg/Kg wet0.34 1.67 40-14072.21.20
Pentachlorophenol mg/Kg wet0.34 1.67 30-13061.81.03
Phenanthrene mg/Kg wet0.17 1.67 40-14081.51.36
Phenol mg/Kg wet0.34 1.67 30-13075.21.25
Pyrene mg/Kg wet0.17 1.67 40-14082.81.38
Pyridine mg/Kg wet0.34 1.67 30-14045.40.757
1,2,4,5-Tetrachlorobenzene mg/Kg wet0.34 1.67 40-14066.11.10
1,2,4-Trichlorobenzene mg/Kg wet0.34 1.67 40-14072.51.21
2,4,5-Trichlorophenol mg/Kg wet0.34 1.67 30-13073.71.23
2,4,6-Trichlorophenol mg/Kg wet0.34 1.67 30-13073.81.23
Page 22 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B210345 - SW-846 3546
LCS (B210345-BS1) Prepared & Analyzed: 08/15/18
mg/Kg wet 6.67 30-130Surrogate: 2-Fluorophenol 77.85.19
mg/Kg wet 6.67 30-130Surrogate: Phenol-d6 82.55.50
mg/Kg wet 3.33 30-130Surrogate: Nitrobenzene-d5 75.12.50
mg/Kg wet 3.33 30-130Surrogate: 2-Fluorobiphenyl 85.72.86
mg/Kg wet 6.67 30-130Surrogate: 2,4,6-Tribromophenol 70.14.67
mg/Kg wet 3.33 30-130Surrogate: p-Terphenyl-d14 97.23.24
LCS Dup (B210345-BSD1) Prepared & Analyzed: 08/15/18
Acenaphthene mg/Kg wet0.17 1.67 3040-14071.4 2.221.19
Acenaphthylene mg/Kg wet0.17 1.67 3040-14072.5 0.7421.21
Acetophenone mg/Kg wet0.34 1.67 3040-14070.9 3.141.18
Aniline mg/Kg wet0.34 1.67 50 V-3410-14057.8 21.40.963
Anthracene mg/Kg wet0.17 1.67 3040-14081.5 1.871.36
Benzidine mg/Kg wet0.66 1.67 30 V-04, V-0640-140114 18.31.91
Benzo(a)anthracene mg/Kg wet0.17 1.67 3040-14077.7 0.9481.30
Benzo(a)pyrene mg/Kg wet0.17 1.67 3040-14080.8 0.4691.35
Benzo(b)fluoranthene mg/Kg wet0.17 1.67 3040-14070.9 0.5371.18
Benzo(g,h,i)perylene mg/Kg wet0.17 1.67 3040-14074.8 3.181.25
Benzo(k)fluoranthene mg/Kg wet0.17 1.67 3040-14077.2 1.121.29
Benzoic Acid mg/Kg wet1.0 1.67 5030-13069.9 4.671.16
Bis(2-chloroethoxy)methane mg/Kg wet0.34 1.67 3040-14073.5 5.251.22
Bis(2-chloroethyl)ether mg/Kg wet0.34 1.67 3040-14065.9 6.611.10
Bis(2-chloroisopropyl)ether mg/Kg wet0.34 1.67 3040-14078.9 10.41.31
Bis(2-Ethylhexyl)phthalate mg/Kg wet0.34 1.67 3040-14085.9 4.881.43
4-Bromophenylphenylether mg/Kg wet0.34 1.67 3040-14074.3 0.2701.24
Butylbenzylphthalate mg/Kg wet0.34 1.67 3040-14084.0 4.291.40
Carbazole mg/Kg wet0.17 1.67 3040-14076.2 1.431.27
4-Chloroaniline mg/Kg wet0.66 1.67 30 V-3410-14045.7 27.10.761
4-Chloro-3-methylphenol mg/Kg wet0.66 1.67 3030-13076.6 5.711.28
2-Chloronaphthalene mg/Kg wet0.34 1.67 3040-14064.0 0.7531.07
2-Chlorophenol mg/Kg wet0.34 1.67 3030-13075.1 0.05321.25
4-Chlorophenylphenylether mg/Kg wet0.34 1.67 3040-14071.3 0.5341.19
Chrysene mg/Kg wet0.17 1.67 3040-14077.8 1.331.30
Dibenz(a,h)anthracene mg/Kg wet0.17 1.67 3040-14075.6 2.381.26
Dibenzofuran mg/Kg wet0.34 1.67 3040-14074.1 0.2431.23
Di-n-butylphthalate mg/Kg wet0.34 1.67 3040-14078.9 4.201.31
1,2-Dichlorobenzene mg/Kg wet0.34 1.67 3040-14071.9 1.631.20
1,3-Dichlorobenzene mg/Kg wet0.34 1.67 3040-14068.9 2.971.15
1,4-Dichlorobenzene mg/Kg wet0.34 1.67 3040-14069.2 2.991.15
3,3-Dichlorobenzidine mg/Kg wet0.17 1.67 50 V-3420-14057.8 18.70.964
2,4-Dichlorophenol mg/Kg wet0.34 1.67 3030-13074.8 1.541.25
Diethylphthalate mg/Kg wet0.34 1.67 3040-14068.6 2.791.14
2,4-Dimethylphenol mg/Kg wet0.34 1.67 3030-13084.4 1.061.41
Dimethylphthalate mg/Kg wet0.34 1.67 3040-14071.0 1.981.18
4,6-Dinitro-2-methylphenol mg/Kg wet0.34 1.67 3030-13072.0 2.661.20
2,4-Dinitrophenol mg/Kg wet0.66 1.67 3030-13056.2 1.030.937
2,4-Dinitrotoluene mg/Kg wet0.34 1.67 3040-14073.5 0.6241.22
2,6-Dinitrotoluene mg/Kg wet0.34 1.67 3040-14079.0 1.911.32
Di-n-octylphthalate mg/Kg wet0.34 1.67 3040-14086.8 3.801.45
1,2-Diphenylhydrazine (as Azobenzene)mg/Kg wet0.34 1.67 3040-14071.2 12.11.19
Fluoranthene mg/Kg wet0.17 1.67 3040-14076.4 0.6791.27
Fluorene mg/Kg wet0.17 1.67 3040-14071.1 1.651.18
Page 23 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B210345 - SW-846 3546
LCS Dup (B210345-BSD1) Prepared & Analyzed: 08/15/18
Hexachlorobenzene mg/Kg wet0.34 1.67 3040-14071.6 0.3351.19
Hexachlorobutadiene mg/Kg wet0.34 1.67 3040-14073.4 5.541.22
Hexachlorocyclopentadiene mg/Kg wet0.34 1.67 30 V-0540-14040.7 5.910.679
Hexachloroethane mg/Kg wet0.34 1.67 3040-14065.7 1.931.09
Indeno(1,2,3-cd)pyrene mg/Kg wet0.17 1.67 3040-14077.0 4.871.28
Isophorone mg/Kg wet0.34 1.67 3040-14073.4 5.871.22
1-Methylnaphthalene mg/Kg wet0.17 1.67 3040-14080.9 0.9351.35
2-Methylnaphthalene mg/Kg wet0.17 1.67 3040-14081.8 0.6821.36
2-Methylphenol mg/Kg wet0.34 1.67 3030-13067.5 5.031.12
3/4-Methylphenol mg/Kg wet0.34 1.67 3030-13080.6 5.151.34
Naphthalene mg/Kg wet0.17 1.67 3040-14075.5 1.901.26
2-Nitroaniline mg/Kg wet0.34 1.67 3040-14065.7 7.361.10
3-Nitroaniline mg/Kg wet0.34 1.67 30 V-3430-14063.8 10.81.06
4-Nitroaniline mg/Kg wet0.34 1.67 3040-14075.0 0.3471.25
Nitrobenzene mg/Kg wet0.34 1.67 3040-14066.5 4.011.11
2-Nitrophenol mg/Kg wet0.34 1.67 3030-13081.3 1.611.35
4-Nitrophenol mg/Kg wet0.66 1.67 5030-13072.3 5.121.21
N-Nitrosodimethylamine mg/Kg wet0.34 1.67 3040-14060.7 6.281.01
N-Nitrosodiphenylamine mg/Kg wet0.34 1.67 3040-14095.3 3.121.59
N-Nitrosodi-n-propylamine mg/Kg wet0.34 1.67 3040-14063.1 8.871.05
Pentachloronitrobenzene mg/Kg wet0.34 1.67 3040-14074.4 3.061.24
Pentachlorophenol mg/Kg wet0.34 1.67 3030-13061.3 0.8771.02
Phenanthrene mg/Kg wet0.17 1.67 3040-14079.5 2.461.32
Phenol mg/Kg wet0.34 1.67 3030-13072.0 4.371.20
Pyrene mg/Kg wet0.17 1.67 3040-14082.1 0.9221.37
Pyridine mg/Kg wet0.34 1.67 3030-14044.3 2.500.738
1,2,4,5-Tetrachlorobenzene mg/Kg wet0.34 1.67 3040-14067.4 1.981.12
1,2,4-Trichlorobenzene mg/Kg wet0.34 1.67 3040-14075.1 3.551.25
2,4,5-Trichlorophenol mg/Kg wet0.34 1.67 3030-13073.4 0.3811.22
2,4,6-Trichlorophenol mg/Kg wet0.34 1.67 3030-13075.4 2.091.26
mg/Kg wet 6.67 30-130Surrogate: 2-Fluorophenol 75.95.06
mg/Kg wet 6.67 30-130Surrogate: Phenol-d6 77.95.19
mg/Kg wet 3.33 30-130Surrogate: Nitrobenzene-d5 71.42.38
mg/Kg wet 3.33 30-130Surrogate: 2-Fluorobiphenyl 84.72.82
mg/Kg wet 6.67 30-130Surrogate: 2,4,6-Tribromophenol 70.64.70
mg/Kg wet 3.33 30-130Surrogate: p-Terphenyl-d14 95.73.19
Page 24 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - EPH - Quality Control
QUALITY CONTROL
[TOC_2]Petroleum Hydrocarbons Analyses - EPH[TOC]
Batch B210344 - SW-846 3546
[TOC_3]B210344[TOC]
Blank (B210344-BLK1) Prepared: 08/15/18 Analyzed: 08/16/18
C9-C18 Aliphatics mg/Kg wet10ND
C19-C36 Aliphatics mg/Kg wet10ND
Unadjusted C11-C22 Aromatics mg/Kg wet10ND
C11-C22 Aromatics mg/Kg wet10ND
Acenaphthene mg/Kg wet0.10ND
Acenaphthylene mg/Kg wet0.10ND
Anthracene mg/Kg wet0.10ND
Benzo(a)anthracene mg/Kg wet0.10ND
Benzo(a)pyrene mg/Kg wet0.10ND
Benzo(b)fluoranthene mg/Kg wet0.10ND
Benzo(g,h,i)perylene mg/Kg wet0.10ND
Benzo(k)fluoranthene mg/Kg wet0.10ND
Chrysene mg/Kg wet0.10ND
Dibenz(a,h)anthracene mg/Kg wet0.10ND
Fluoranthene mg/Kg wet0.10ND
Fluorene mg/Kg wet0.10ND
Indeno(1,2,3-cd)pyrene mg/Kg wet0.10ND
2-Methylnaphthalene mg/Kg wet0.10ND
Naphthalene mg/Kg wet0.10ND
Phenanthrene mg/Kg wet0.10ND
Pyrene mg/Kg wet0.10ND
n-Decane mg/Kg wet0.10ND
n-Docosane mg/Kg wet0.10ND
n-Dodecane mg/Kg wet0.10ND
n-Eicosane mg/Kg wet0.10ND
n-Hexacosane mg/Kg wet0.10ND
n-Hexadecane mg/Kg wet0.10ND
n-Hexatriacontane mg/Kg wet0.10ND
n-Nonadecane mg/Kg wet0.10ND
n-Nonane mg/Kg wet0.10ND
n-Octacosane mg/Kg wet0.10ND
n-Octadecane mg/Kg wet0.10ND
n-Tetracosane mg/Kg wet0.10ND
n-Tetradecane mg/Kg wet0.10ND
n-Triacontane mg/Kg wet0.10ND
Naphthalene-aliphatic fraction mg/Kg wet0.10ND
2-Methylnaphthalene-aliphatic fraction mg/Kg wet0.10ND
mg/Kg wet 5.00 40-140Surrogate: Chlorooctadecane (COD)82.04.10
mg/Kg wet 5.00 40-140Surrogate: o-Terphenyl (OTP)79.23.96
mg/Kg wet 5.00 40-140Surrogate: 2-Bromonaphthalene 93.74.68
mg/Kg wet 5.00 40-140Surrogate: 2-Fluorobiphenyl 87.34.37
LCS (B210344-BS1) Prepared: 08/15/18 Analyzed: 08/16/18
C9-C18 Aliphatics mg/Kg wet10 30.0 40-14080.924.3
C19-C36 Aliphatics mg/Kg wet10 40.0 40-14093.637.5
Acenaphthene mg/Kg wet0.10 5.00 40-14074.53.72
Acenaphthylene mg/Kg wet0.10 5.00 40-14070.33.51
Anthracene mg/Kg wet0.10 5.00 40-14082.94.14
Benzo(a)anthracene mg/Kg wet0.10 5.00 40-14084.14.20
Benzo(a)pyrene mg/Kg wet0.10 5.00 40-14082.64.13
Benzo(b)fluoranthene mg/Kg wet0.10 5.00 40-14083.84.19
Benzo(g,h,i)perylene mg/Kg wet0.10 5.00 40-14082.74.14
Page 25 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - EPH - Quality Control
QUALITY CONTROL
Batch B210344 - SW-846 3546
LCS (B210344-BS1) Prepared: 08/15/18 Analyzed: 08/16/18
Benzo(k)fluoranthene mg/Kg wet0.10 5.00 40-14083.14.15
Chrysene mg/Kg wet0.10 5.00 40-14083.94.19
Dibenz(a,h)anthracene mg/Kg wet0.10 5.00 40-14085.44.27
Fluoranthene mg/Kg wet0.10 5.00 40-14083.64.18
Fluorene mg/Kg wet0.10 5.00 40-14078.73.93
Indeno(1,2,3-cd)pyrene mg/Kg wet0.10 5.00 40-14079.13.96
2-Methylnaphthalene mg/Kg wet0.10 5.00 40-14070.13.51
Naphthalene mg/Kg wet0.10 5.00 40-14063.83.19
Phenanthrene mg/Kg wet0.10 5.00 40-14084.24.21
Pyrene mg/Kg wet0.10 5.00 40-14085.64.28
n-Decane mg/Kg wet0.10 5.00 40-14051.92.60
n-Docosane mg/Kg wet0.10 5.00 40-14090.64.53
n-Dodecane mg/Kg wet0.10 5.00 40-14067.83.39
n-Eicosane mg/Kg wet0.10 5.00 40-14094.64.73
n-Hexacosane mg/Kg wet0.10 5.00 40-14086.54.33
n-Hexadecane mg/Kg wet0.10 5.00 40-14091.54.58
n-Hexatriacontane mg/Kg wet0.10 5.00 40-14080.34.01
n-Nonadecane mg/Kg wet0.10 5.00 40-14092.54.62
n-Nonane mg/Kg wet0.10 5.00 30-14034.71.74
n-Octacosane mg/Kg wet0.10 5.00 40-14082.34.11
n-Octadecane mg/Kg wet0.10 5.00 40-14094.74.74
n-Tetracosane mg/Kg wet0.10 5.00 40-14089.14.45
n-Tetradecane mg/Kg wet0.10 5.00 40-14082.84.14
n-Triacontane mg/Kg wet0.10 5.00 40-14081.64.08
Naphthalene-aliphatic fraction mg/Kg wet0.10 5.00 0-5ND
2-Methylnaphthalene-aliphatic fraction mg/Kg wet0.10 5.00 0-5ND
mg/Kg wet 5.00 40-140Surrogate: Chlorooctadecane (COD)88.34.42
mg/Kg wet 5.00 40-140Surrogate: o-Terphenyl (OTP)86.84.34
mg/Kg wet 5.00 40-140Surrogate: 2-Bromonaphthalene 85.44.27
mg/Kg wet 5.00 40-140Surrogate: 2-Fluorobiphenyl 87.24.36
LCS Dup (B210344-BSD1) Prepared: 08/15/18 Analyzed: 08/16/18
C9-C18 Aliphatics mg/Kg wet10 30.0 2540-14085.8 5.9125.7
C19-C36 Aliphatics mg/Kg wet10 40.0 2540-14095.0 1.4238.0
Acenaphthene mg/Kg wet0.10 5.00 2540-14077.6 4.133.88
Acenaphthylene mg/Kg wet0.10 5.00 2540-14073.3 4.293.67
Anthracene mg/Kg wet0.10 5.00 2540-14085.6 3.264.28
Benzo(a)anthracene mg/Kg wet0.10 5.00 2540-14086.7 3.124.34
Benzo(a)pyrene mg/Kg wet0.10 5.00 2540-14085.5 3.524.28
Benzo(b)fluoranthene mg/Kg wet0.10 5.00 2540-14087.0 3.734.35
Benzo(g,h,i)perylene mg/Kg wet0.10 5.00 2540-14086.8 4.844.34
Benzo(k)fluoranthene mg/Kg wet0.10 5.00 2540-14085.7 3.114.28
Chrysene mg/Kg wet0.10 5.00 2540-14086.4 2.954.32
Dibenz(a,h)anthracene mg/Kg wet0.10 5.00 2540-14089.9 5.174.50
Fluoranthene mg/Kg wet0.10 5.00 2540-14086.4 3.284.32
Fluorene mg/Kg wet0.10 5.00 2540-14081.7 3.784.09
Indeno(1,2,3-cd)pyrene mg/Kg wet0.10 5.00 2540-14082.2 3.794.11
2-Methylnaphthalene mg/Kg wet0.10 5.00 2540-14072.8 3.803.64
Naphthalene mg/Kg wet0.10 5.00 2540-14066.7 4.513.34
Phenanthrene mg/Kg wet0.10 5.00 2540-14087.2 3.404.36
Pyrene mg/Kg wet0.10 5.00 2540-14088.4 3.184.42
n-Decane mg/Kg wet0.10 5.00 2540-14055.8 7.222.79
Page 26 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - EPH - Quality Control
QUALITY CONTROL
Batch B210344 - SW-846 3546
LCS Dup (B210344-BSD1) Prepared: 08/15/18 Analyzed: 08/16/18
n-Docosane mg/Kg wet0.10 5.00 2540-14091.8 1.334.59
n-Dodecane mg/Kg wet0.10 5.00 2540-14071.7 5.593.58
n-Eicosane mg/Kg wet0.10 5.00 2540-14094.0 0.5984.70
n-Hexacosane mg/Kg wet0.10 5.00 2540-14088.2 1.874.41
n-Hexadecane mg/Kg wet0.10 5.00 2540-14093.8 2.524.69
n-Hexatriacontane mg/Kg wet0.10 5.00 2540-14082.3 2.514.12
n-Nonadecane mg/Kg wet0.10 5.00 2540-14093.8 1.424.69
n-Nonane mg/Kg wet0.10 5.00 2530-14037.6 8.001.88
n-Octacosane mg/Kg wet0.10 5.00 2540-14084.0 2.034.20
n-Octadecane mg/Kg wet0.10 5.00 2540-14096.5 1.914.83
n-Tetracosane mg/Kg wet0.10 5.00 2540-14090.5 1.614.53
n-Tetradecane mg/Kg wet0.10 5.00 2540-14085.8 3.574.29
n-Triacontane mg/Kg wet0.10 5.00 2540-14083.5 2.354.17
Naphthalene-aliphatic fraction mg/Kg wet0.10 5.00 0-5ND
2-Methylnaphthalene-aliphatic fraction mg/Kg wet0.10 5.00 0-5ND
mg/Kg wet 5.00 40-140Surrogate: Chlorooctadecane (COD)88.54.42
mg/Kg wet 5.00 40-140Surrogate: o-Terphenyl (OTP)88.24.41
mg/Kg wet 5.00 40-140Surrogate: 2-Bromonaphthalene 84.04.20
mg/Kg wet 5.00 40-140Surrogate: 2-Fluorobiphenyl 87.94.40
Page 27 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - VPH - Quality Control
QUALITY CONTROL
[TOC_2]Petroleum Hydrocarbons Analyses - VPH[TOC]
Batch B209997 - MA VPH
[TOC_3]B209997[TOC]
Blank (B209997-BLK1) Prepared: 08/10/18 Analyzed: 08/14/18
Unadjusted C5-C8 Aliphatics mg/Kg wet10ND
C5-C8 Aliphatics mg/Kg wet10ND
Unadjusted C9-C12 Aliphatics mg/Kg wet10ND
C9-C12 Aliphatics mg/Kg wet10ND
C9-C10 Aromatics mg/Kg wet10ND
Benzene mg/Kg wet0.050ND
Butylcyclohexane mg/Kg wet0.050ND
Decane mg/Kg wet0.050ND
Ethylbenzene mg/Kg wet0.050ND
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.050ND
2-Methylpentane mg/Kg wet0.050ND
Naphthalene mg/Kg wet0.50ND
Nonane mg/Kg wet0.050ND
Pentane mg/Kg wet0.050ND
Toluene mg/Kg wet0.050ND
1,2,4-Trimethylbenzene mg/Kg wet0.050ND
2,2,4-Trimethylpentane mg/Kg wet0.050ND
m+p Xylene mg/Kg wet0.10ND
o-Xylene mg/Kg wet0.050ND
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)93.137.3
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)86.334.5
LCS (B209997-BS1) Prepared: 08/10/18 Analyzed: 08/14/18
Benzene mg/Kg wet0.0010 0.100 70-1301070.107
Butylcyclohexane mg/Kg wet0.0010 0.100 70-13089.50.0895
Decane mg/Kg wet0.0010 0.100 70-13093.00.0930
Ethylbenzene mg/Kg wet0.0010 0.100 70-1301080.108
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.0010 0.100 70-1301090.109
2-Methylpentane mg/Kg wet0.0010 0.100 70-1301190.119
Naphthalene mg/Kg wet0.010 0.100 70-1301030.103
Nonane mg/Kg wet0.0010 0.100 30-13088.20.0882
Pentane mg/Kg wet0.0010 0.100 70-1301210.121
Toluene mg/Kg wet0.0010 0.100 70-1301070.107
1,2,4-Trimethylbenzene mg/Kg wet0.0010 0.100 70-1301090.109
2,2,4-Trimethylpentane mg/Kg wet0.0010 0.100 70-1301110.111
m+p Xylene mg/Kg wet0.0020 0.200 70-1301100.219
o-Xylene mg/Kg wet0.0010 0.100 70-1301070.107
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)94.237.7
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)87.735.1
LCS Dup (B209997-BSD1) Prepared: 08/10/18 Analyzed: 08/14/18
Benzene mg/Kg wet0.0010 0.100 2570-130106 0.5780.106
Butylcyclohexane mg/Kg wet0.0010 0.100 2570-13089.6 0.1520.0896
Decane mg/Kg wet0.0010 0.100 2570-13094.5 1.530.0945
Ethylbenzene mg/Kg wet0.0010 0.100 2570-130107 0.6420.107
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.0010 0.100 2570-130107 2.090.107
2-Methylpentane mg/Kg wet0.0010 0.100 2570-130118 0.7560.118
Naphthalene mg/Kg wet0.010 0.100 2570-130101 2.400.101
Nonane mg/Kg wet0.0010 0.100 2530-13088.5 0.2900.0885
Pentane mg/Kg wet0.0010 0.100 2570-130119 1.580.119
Toluene mg/Kg wet0.0010 0.100 2570-130106 0.6500.106
1,2,4-Trimethylbenzene mg/Kg wet0.0010 0.100 2570-130108 0.9920.108
Page 28 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - VPH - Quality Control
QUALITY CONTROL
Batch B209997 - MA VPH
LCS Dup (B209997-BSD1) Prepared: 08/10/18 Analyzed: 08/14/18
2,2,4-Trimethylpentane mg/Kg wet0.0010 0.100 2570-130108 2.970.108
m+p Xylene mg/Kg wet0.0020 0.200 2570-130109 0.7790.217
o-Xylene mg/Kg wet0.0010 0.100 2570-130106 0.8960.106
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)95.238.1
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)87.735.1
Page 29 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) - Quality Control
QUALITY CONTROL
[TOC_2]Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)[TOC]
Batch B210372 - % Solids
[TOC_3]B210372[TOC]
Duplicate (B210372-DUP1) Prepared & Analyzed: 08/15/18 Source: 18H0706-01
% Solids % Wt 200.10386.4 86.3
Page 30 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
FLAG/QUALIFIER SUMMARY
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
J
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but
the other is within limits. RPD between the two LFB/LCS results is within method specified criteria.
L-07
Initial calibration did not meet method specifications. Compound was calibrated using a response factor where
%RSD is outside of method specified criteria. Reported result is estimated.
V-04
Continuing calibration did not meet method specifications and was biased on the low side for this compound.
Reported result is estimated.
V-05
Continuing calibration did not meet method specifications and was biased on the high side for this compound.
Reported result is estimated.
V-06
Continuing calibration did not meet method specifications and was biased on the high side. Data validation is not
affected since sample result was "not detected" for this compound.
V-20
Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this
compound. Reported result is estimated.
V-34
[TOC_1]Flag/Qualifier Summary[TOC]
Page 31 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
MADEP-EPH-04-1.1 in Soil
CT,NC,ME,NH-PC9-C18 Aliphatics
CT,NC,ME,NH-PC19-C36 Aliphatics
CT,NC,ME,NH-PUnadjusted C11-C22 Aromatics
CT,NC,ME,NH-PC11-C22 Aromatics
CT,NC,ME,NH-PAcenaphthene
CT,NC,ME,NH-PAcenaphthylene
CT,NC,ME,NH-PAnthracene
CT,NC,ME,NH-PBenzo(a)anthracene
CT,NC,ME,NH-PBenzo(a)pyrene
CT,NC,ME,NH-PBenzo(b)fluoranthene
CT,NC,ME,NH-PBenzo(g,h,i)perylene
CT,NC,ME,NH-PBenzo(k)fluoranthene
CT,NC,ME,NH-PChrysene
CT,NC,ME,NH-PDibenz(a,h)anthracene
CT,NC,ME,NH-PFluoranthene
CT,NC,MEFluorene
CT,NC,ME,NH-PIndeno(1,2,3-cd)pyrene
CT,NC,ME2-Methylnaphthalene
CT,NC,ME,NH-PNaphthalene
CT,NC,ME,NH-PPhenanthrene
CT,NC,ME,NH-PPyrene
MADEP-VPH-Feb 2018 Rev 2.1 in Soil
CT,NC,ME,NH-PUnadjusted C5-C8 Aliphatics
CT,NC,ME,NH-PC5-C8 Aliphatics
CT,NC,ME,NH-PUnadjusted C9-C12 Aliphatics
CT,NC,ME,NH-PC9-C12 Aliphatics
CT,NC,ME,NH-PC9-C10 Aromatics
CT,NC,ME,NH-PBenzene
CT,NC,ME,NH-PEthylbenzene
CT,NC,ME,NH-PMethyl tert-Butyl Ether (MTBE)
CT,NC,ME,NH-PNaphthalene
CT,NC,ME,NH-PToluene
CT,NC,ME,NH-Pm+p Xylene
CT,NC,ME,NH-Po-Xylene
SW-846 8260B in Soil
NCAcetone
NCAcrylonitrile
NCtert-Amyl Methyl Ether (TAME)
NCBenzene
NCBromobenzene
NCBromochloromethane
NCBromodichloromethane
NCBromoform
NCBromomethane
NC2-Butanone (MEK)
NCtert-Butyl Alcohol (TBA)
[TOC_1]Certifications[TOC]
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SW-846 8260B in Soil
NCn-Butylbenzene
NCsec-Butylbenzene
NCtert-Butylbenzene
NCtert-Butyl Ethyl Ether (TBEE)
NCCarbon Disulfide
NCCarbon Tetrachloride
NCChlorobenzene
NCChlorodibromomethane
NCChloroethane
NCChloroform
NCChloromethane
NC2-Chlorotoluene
NC4-Chlorotoluene
NC1,2-Dibromo-3-chloropropane (DBCP)
NC1,2-Dibromoethane (EDB)
NCDibromomethane
NC1,2-Dichlorobenzene
NC1,3-Dichlorobenzene
NC1,4-Dichlorobenzene
NCtrans-1,4-Dichloro-2-butene
NCDichlorodifluoromethane (Freon 12)
NC1,1-Dichloroethane
NC1,2-Dichloroethane
NC1,1-Dichloroethylene
NCcis-1,2-Dichloroethylene
NCtrans-1,2-Dichloroethylene
NC1,2-Dichloropropane
NC1,3-Dichloropropane
NC2,2-Dichloropropane
NC1,1-Dichloropropene
NCcis-1,3-Dichloropropene
NCtrans-1,3-Dichloropropene
NCDiethyl Ether
NCDiisopropyl Ether (DIPE)
NC1,4-Dioxane
NCEthylbenzene
NCHexachlorobutadiene
NC2-Hexanone (MBK)
NCIsopropylbenzene (Cumene)
NCp-Isopropyltoluene (p-Cymene)
NCMethyl tert-Butyl Ether (MTBE)
NCMethylene Chloride
NC4-Methyl-2-pentanone (MIBK)
NCNaphthalene
NCn-Propylbenzene
NCStyrene
NC1,1,1,2-Tetrachloroethane
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NC1,1,2,2-Tetrachloroethane
NCTetrachloroethylene
NCTetrahydrofuran
NCToluene
NC1,2,3-Trichlorobenzene
NC1,2,4-Trichlorobenzene
NC1,3,5-Trichlorobenzene
NC1,1,1-Trichloroethane
NC1,1,2-Trichloroethane
NCTrichloroethylene
NCTrichlorofluoromethane (Freon 11)
NC1,2,3-Trichloropropane
NC1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
NC1,2,4-Trimethylbenzene
NC1,3,5-Trimethylbenzene
NCVinyl Chloride
NCm+p Xylene
NCo-Xylene
SW-846 8270D in Soil
CT,NY,NH,ME,NC,VAAcenaphthene
CT,NY,NH,ME,NC,VAAcenaphthylene
NY,NH,ME,NC,VAAcetophenone
NY,NH,ME,NC,VAAniline
CT,NY,NH,ME,NC,VAAnthracene
CT,NY,NH,ME,NC,VABenzidine
CT,NY,NH,ME,NC,VABenzo(a)anthracene
CT,NY,NH,ME,NC,VABenzo(a)pyrene
CT,NY,NH,ME,NC,VABenzo(b)fluoranthene
CT,NY,NH,ME,NC,VABenzo(g,h,i)perylene
CT,NY,NH,ME,NC,VABenzo(k)fluoranthene
NY,NH,ME,NC,VABenzoic Acid
CT,NY,NH,ME,NC,VABis(2-chloroethoxy)methane
CT,NY,NH,ME,NC,VABis(2-chloroethyl)ether
CT,NY,NH,ME,NC,VABis(2-chloroisopropyl)ether
CT,NY,NH,ME,NC,VABis(2-Ethylhexyl)phthalate
CT,NY,NH,ME,NC,VA4-Bromophenylphenylether
CT,NY,NH,ME,NC,VAButylbenzylphthalate
NCCarbazole
CT,NY,NH,ME,NC,VA4-Chloroaniline
CT,NY,NH,ME,NC,VA4-Chloro-3-methylphenol
CT,NY,NH,NC,VA2-Chloronaphthalene
CT,NY,NH,ME,NC,VA2-Chlorophenol
CT,NY,NH,ME,NC,VA4-Chlorophenylphenylether
CT,NY,NH,ME,NC,VAChrysene
CT,NY,NH,ME,NC,VADibenz(a,h)anthracene
CT,NY,NH,ME,NC,VADibenzofuran
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SW-846 8270D in Soil
CT,NY,NH,ME,NC,VADi-n-butylphthalate
NY,NH,ME,NC,VA1,2-Dichlorobenzene
NY,NH,ME,NC,VA1,3-Dichlorobenzene
NY,NH,ME,NC,VA1,4-Dichlorobenzene
CT,NY,NH,ME,NC,VA3,3-Dichlorobenzidine
CT,NY,NH,ME,NC,VA2,4-Dichlorophenol
CT,NY,NH,ME,NC,VADiethylphthalate
CT,NY,NH,ME,NC,VA2,4-Dimethylphenol
CT,NY,NH,ME,NC,VADimethylphthalate
CT,NY,NH,ME,NC,VA4,6-Dinitro-2-methylphenol
CT,NY,NH,ME,NC,VA2,4-Dinitrophenol
CT,NY,NH,ME,NC,VA2,4-Dinitrotoluene
CT,NY,NH,ME,NC,VA2,6-Dinitrotoluene
CT,NY,NH,ME,NC,VADi-n-octylphthalate
NY,NH,ME,NC,VA1,2-Diphenylhydrazine (as Azobenzene)
CT,NY,NH,ME,NC,VAFluoranthene
NY,NH,ME,NC,VAFluorene
CT,NY,NH,ME,NC,VAHexachlorobenzene
CT,NY,NH,ME,NC,VAHexachlorobutadiene
CT,NY,NH,ME,NC,VAHexachlorocyclopentadiene
CT,NY,NH,ME,NC,VAHexachloroethane
CT,NY,NH,ME,NC,VAIndeno(1,2,3-cd)pyrene
CT,NY,NH,ME,NC,VAIsophorone
NC1-Methylnaphthalene
CT,NY,NH,ME,NC,VA2-Methylnaphthalene
CT,NY,NH,ME,NC,VA2-Methylphenol
CT,NY,NH,ME,NC,VA3/4-Methylphenol
CT,NY,NH,ME,NC,VANaphthalene
CT,NY,NH,ME,NC,VA2-Nitroaniline
CT,NY,NH,ME,NC,VA3-Nitroaniline
CT,NY,NH,ME,NC,VA4-Nitroaniline
CT,NY,NH,ME,NC,VANitrobenzene
CT,NY,NH,ME,NC,VA2-Nitrophenol
CT,NY,NH,ME,NC,VA4-Nitrophenol
CT,NY,NH,ME,NC,VAN-Nitrosodimethylamine
CT,NY,NH,ME,NC,VAN-Nitrosodiphenylamine
CT,NY,NH,ME,NC,VAN-Nitrosodi-n-propylamine
NY,NCPentachloronitrobenzene
CT,NY,NH,ME,NC,VAPentachlorophenol
CT,NY,NH,ME,NC,VAPhenanthrene
CT,NY,NH,ME,NC,VAPhenol
CT,NY,NH,ME,NC,VAPyrene
CT,NY,NH,ME,NC,VAPyridine
NY,NC1,2,4,5-Tetrachlorobenzene
CT,NY,NH,ME,NC,VA1,2,4-Trichlorobenzene
CT,NY,NH,ME,NC,VA2,4,5-Trichlorophenol
CT,NY,NH,ME,NC,VA2,4,6-Trichlorophenol
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CERTIFICATIONS
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SW-846 8270D in Soil
NC2-Fluorophenol
The CON-TEST Environmental Laboratory operates under the following certifications and accreditations:
Code Description Number Expires
100033AIHA-LAP, LLC - ISO17025:2005AIHA 03/1/2020
M-MA100Massachusetts DEPMA 06/30/2019
PH-0567Connecticut Department of Publilc HealthCT 09/30/2019
10899 NELAPNew York State Department of HealthNY 04/1/2019
2516 NELAPNew Hampshire Environmental LabNH-S 02/5/2019
LAO00112Rhode Island Department of HealthRI 12/30/2018
652North Carolina Div. of Water QualityNC 12/31/2018
MA007 NELAPNew Jersey DEPNJ 06/30/2019
E871027 NELAPFlorida Department of HealthFL 06/30/2019
LL015036Vermont Department of Health Lead LaboratoryVT 07/30/2019
2011028State of MaineME 06/9/2019
460217Commonwealth of VirginiaVA 12/14/2018
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2018
VT-255716Vermont Department of Health Drinking WaterVT-DW 06/12/2019
25703North Carolina Department of HealthNC-DW 07/31/2019
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