WS-9913_45093_CA_LSA_20200311

609A Piner Road, Suite 115
Wilmington, North Carolina 28409
Telephone [phone]
Fax [phone]
www.atcgroupservices.com

March 11, 2020

Ms. Mindy Lepard
North Carolina Department of Environmental Quality
Winston-Salem Regional Office
Division of Waste Management - UST Section
450 West Hanes Mill Road, Suite 300
Winston-Salem, North Carolina 27105

RE: Phase I Limited Site Assessment
Pilot Travel Center #6955
1044 Jimmie Kerr Road
Haw River, Alamance County, North Carolina
NCDEQ Facility ID #00-0-0000035045
NCDEQ Incident No. 45093
ATC Project No. PT00695504

Dear Ms. Lepard:

ATC Associates of North Carolina, P.C., on behalf of Pilot Travel Centers, LLC, is submitting this
Phase I Limited Site Assessment Report for the Pilot Travel Center #6955 located in Haw River,
North Carolina. This report documents limited site assessment activities conducted per the Notice of
Regulatory Requirements issued by the North Carolina Department of Environmental Quality dated
November 21, 2019 and included the installation of one monitoring well and subsequent
groundwater sampling event in January 2020 and the laboratory analytical results.

If you have any questions or require additional information, please contact our office at (919)
871-0999.

Sincerely,

ATC Associates of North Carolina, P.C.
Maureen Jackson, P.G. Max Burmeister
Senior Project Manager Program Manager

cc: Joey Cupp, Pilot Travel Centers, LLC
Phase I Limited Site Assessment Report March 11, 2020
Pilot Travel Center #6955 (Incident #45093) ATC Project No. PT00695504
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TABLE OF CONTENTS

1.0 SITE IDENTIFICATION .................................................................................3
2.0 SITE HISTORY AND CHARACTERIZATION ...........................................4
2.1 UST Owner and Operator Information ....................................................4
2.2 UST Information ......................................................................................4
2.3 AST Information ......................................................................................4
2.4 Site Characteristics...................................................................................4
2.5 Release Information .................................................................................4
3.0 LIMITED SITE ASSESSMENT RISK CLASSIFICATION AND LAND USE
..............................................................................................................................5
4.0 RECEPTOR PATHWAY INFORMATION ...................................................8
4.1 Water Supply Wells .................................................................................8
4.2 Public Water Supplies ..............................................................................9
4.3 Surface Water Bodies ..............................................................................9
4.4 Wellhead Protection Areas ......................................................................9
4.5 Regional Geology and Hydrogeology .....................................................9
4.6 Subsurface Structures...............................................................................10
4.7 Land Use ..................................................................................................10
5.0 LIMITED SITE ASSESSMENT ACTIVITIES ..............................................10
5.1 Soil Sampling ...........................................................................................10
5.2 Monitoring Well Installation....................................................................10
5.3 Groundwater Sampling ............................................................................11
6.0 SITE GEOLOGY AND HYDROGEOLOGY.................................................11
6.1 Description of Shallow Subsurface Geology ...........................................11
6.2 Groundwater Occurrence .........................................................................12
6.3 Groundwater Flow Direction ...................................................................12
7.0 ANALYTICAL RESULTS ...............................................................................12
7.1 Soil Analytical Results .............................................................................12
7.2 Groundwater Analytical Results ..............................................................12
8.0 CONCLUSIONS AND RECOMMENDATIONS ...........................................12
8.1 Conclusions ..............................................................................................12
8.2 Recommendations ....................................................................................13

Phase I Limited Site Assessment Report March 11, 2020
Pilot Travel Center #6955 (Incident #45093) ATC Project No. PT00695504
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TABLES

Table 1 Water Supply Well Information
Table 2 Adjacent Property Owner Information
Table 3 Monitoring Well Construction Details
Table 4 Soil Analytical Results
Table 5 Groundwater Analytical Results

FIGURES

Figure 1 Topographic Map
Figure 2 Site Map
Figure 3 Potential Receptor Map
Figure 4 Groundwater Analytical Map

APPENDICES

Appendix A Soil Boring Log and Well Construction Record
Appendix B Laboratory Analytical Results

Phase I Limited Site Assessment Report March 11, 2020
Pilot Travel Center #6955 (Incident #45093) ATC Project No. PT00695504
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2.0 SITE HISTORY AND CHARACTERIZATION
2.1 UST Owner and Operator Information
One 15,000-gallon gasoline, one 10,000-gallon gasoline, and two 25,000-gallon diesel underground
storage tanks (USTs) were installed at the referenced facility on May 24, 1996. The USTs and their
appurtenances are owned by Pilot Travel Centers, LLC of Knoxville, Tennessee. Information regarding
each of the tanks is provided below.

2.2 UST Information
UST
ID PRODUCT CAPACITY
(gals.) MATERIALS INSTALLATION
DATE
UST
STATUS
RELEASE
ASSOCIATED
(Yes/No)

T1 Gasoline 15,000 Steel 05-24-1996 Active No
T2 Gasoline 10,000 Steel 05-24-1996 Active No
T3 Diesel 25,000 Steel 05-24-1996 Active Yes
T4 Diesel 25,000 Steel 05-24-1996 Active Yes

Figure 1 is a topographical map of the site and surrounding area. Figure 2 is a site map, which depicts
the site and pertinent structures, including the location of the USTs and appurtenances.

2.3 AST Information
ASTs were not observed on the property.

2.4 Site Characteristics
The subject property consists of one convenience store building, two fast food restaurants, and several
gasoline and diesel dispenser islands, and other petroleum fueling equipment. The subject property and
surrounding area are fairly level. The subject property is located in a light commercial area in proximity
to Interstate-85/40 (off Exit 150). Municipal water is available in the site vicinity.

2.5 Release Information
On June 12, 2018, during on-site testing of the UST system, it was determined that there was diesel
product in the submersible turbine pump (STP) sump for diesel tank #3, and the sump was in need of
repair or replacement. On June 13, 2018, Pilot Travel Centers, LLC (Pilot) personnel submitted a UST
17A UST Suspected Release 24 Hour Notice. On June 20, 2018, Pilot personnel submitted a UST-17B
UST Suspected Release 7 Day Notice. As part of the site check activities, ATC personnel contracted with
Geologic Exploration to hand auger a borehole to 5 feet below ground surface (bgs) in proximity to the
Phase I Limited Site Assessment Report March 11, 2020
Pilot Travel Center #6955 (Incident #45093) ATC Project No. PT00695504
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diesel tank #3 STP sump. The soil sample collected during the site check activities (SB-1 5’) indicated
C9-C22 aromatics above the Soil-to-Groundwater Maximum Soil Contaminant Concentrations
(STGW-MSCCs). On August 16, 2018, upon receipt of the soil analytical results, ATC personnel
submitted a UST-61 24-Hour Release and UST Leak Reporting Form to the North Carolina Department
of Environmental Quality (NCDEQ) Winston-Salem Regional Office. The results of the site check
activities are documented in a Site Check Report submitted by ATC on August 21, 2018.

On November 21, 2019, NCDEQ issued a Notice of Regulatory Requirements (NORR) for the
performance of a Phase I Limited Site Assessment (LSA).

3.0 LIMITED SITE ASSESSMENT RISK CLASSIFICATION AND LAND USE
In order to evaluate the following, a review of available site-specific, local and regional data was
performed to include:
 A well survey within a 1,500-foot radius of the subject facility, including a record inquiry.
 Identification of wellhead protection areas.
 Researching geology and hydrogeology of the region, including topography, soil types, and
surface water drainage patterns.
 Identification of surface waters within a 1,500-foot radius of the subject facility.
 Land use observations (site reconnaissance) and zoning classifications.
 A visual survey for subsurface structures and potential impacts from the source area.
 Gathering information on adjacent property owners and occupants.

Part I – Groundwater/Surface Water/Vapor Impacts
High Risk:
1. Has the discharge or release contaminated any water supply well including any used for
non-drinking purposes? NO

2. Is a water supply well used for drinking water located within 1,000 feet of the source area of the
discharge or release? NO

According to the City of Graham Water and Sewer Department, public water is supplied to the
site and adjacent properties and municipal water is available in the site vicinity. During the water
supply well survey, one water supply well was identified approximately 800 feet north of the
source area. It was confirmed that this property is connected to the municipal water supply and
has an active water account; therefore, it is assumed the water supply well is used for non-potable
purposes.

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Pilot Travel Center #6955 (Incident #45093) ATC Project No. PT00695504
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3. Is a water supply well used for any purpose (e.g. irrigation, washing cars, industrial cooling
water, filling swimming pools) located within 250 feet of the source area of the release or
discharge? NO

4. Does groundwater within 500 feet of the source area of the discharge or release have the
potential for future use in that there is no other source of water supply other than the
groundwater? NO

5. Do vapors from the discharge or release pose a threat of explosion because of accumulation of
the vapors in a confined space or pose any other serious threat to public health, public safety, or
the environment? NO

6. Are there any other factors that would cause the discharge or release to pose an imminent danger
to public health, public safety, or the environment? NO

At the time of this report, factors have not been identified that would appear to pose an imminent
danger to public health, public safety, or the environment.

Intermediate Risk:
7. Is a surface water body located within 500 feet of the source area of the discharge or release?
NO

An unnamed pond is located approximately 1,100 feet west of the site. The Haw River is located
approximately 2,400 feet west of the site.

If yes, does the maximum groundwater contaminant concentration exceed the surface water
quality standards and criteria found in 15A NCAC 2B .0200 by a factor of 10? NA

8. Is the source area of the discharge or release located within a designated wellhead protection
area as defined in 42 USC 300h-7(e)? NO

ATC reviewed the list of wellhead protection areas for municipalities and no wellhead protection
areas were identified in the site vicinity.

9. Is the discharge or release located in the Coastal Plain Physiographic Region as designated on a
map entitled “Geology of North Carolina” published by the Department in 1985? NO

If yes, is the source area of the discharge or release located in an area in which there is recharge
to an unconfirmed or semi-confined aquifer that is being used or may be used as a source of
drinking water? NA

10. Do the levels of groundwater contamination for any contaminant exceed the gross contamination
levels (GCLs) established by the Department? NO

Part II – Land Use
Property Containing Source Area of Discharge or Release:
The questions below pertain to the property containing the source area of the release.
1. Does the property contain one or more primary or secondary (permanent or temporary)
residences? NO

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2. Does the property contain a school, daycare center, hospital, playground, park, recreation area,
church, nursing home, or other place of public assembly? NO

The property is a travel center with retail petroleum sales.

3. Does the property contain a commercial (e.g., retail, warehouse, office/business space, etc.) or
industrial (e.g., manufacturing, utilities, industrial research and development,
chemical/petroleum bulk storage, etc.) enterprise, and inactive commercial or industrial
enterprise, or is the land undeveloped? YES

The property is an active travel center with retail petroleum sales.

4. Do children visit the property? YES

Children visit the property consistent with its use.

5. Is access to the property reliably restricted consistent with its use (e.g., by fences, security
personnel or both)? NO

The site is not restricted.

6. Do pavement, building, or other structures cap the contaminated soil? YES

The area is covered by asphalt in the driveways and parking areas. The UST basin and beneath
the canopies is concrete

If yes, what mechanisms are in place or can be put into place to ensure that the contaminated soil
will remain capped in the foreseeable future?

The property will likely remain commercial for the foreseeable future.

7. What is the zoning status of the property?

The site is zoned General Business (B-2).

8. Is the use of the property likely to change in the next 20 years? NO
ATC personnel are not aware of any plans to change the use of the property by the current
property owner.

Property Surrounding Source Area of Discharge or Release:
The questions below pertain to the area within 1,500 feet of the source area of the discharge or release
(excludes property containing source area of the release):

9. What is the distance from the source area of the release to the nearest primary or secondary
residence (permanent or temporary)?
The nearest residence was identified approximately 750 feet north of the source area.
Phase I Limited Site Assessment Report March 11, 2020
Pilot Travel Center #6955 (Incident #45093) ATC Project No. PT00695504
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10. What is the distance from the source area of the release to the nearest school, daycare center,
hospital, playground, park, recreation area, church, nursing home, or other place of public
assembly?
Alamance Community College is located approximately 1,500 feet southwest of the source area.
No other places of public assembly were identified within 1,500 feet of the source area.

11. What is the zoning status of properties in the surrounding area?
Properties surrounding the subject facility are zoned Light Industrial (I-1). The zoning status of
the subject facility is General Business (B-2). Commercial, industrial, and wooded, undeveloped
properties characterize the surrounding area.

12. Briefly characterize the use and activities of the land in the surrounding area.
The site is bordered to the north by Blue Beacon Truck Wash, to the east by vacant industrial
land, to the west by Jimmie Kerr Road, and south by Interstate-85/40 with industrial and vacant
land beyond. Agricultural and wooded land surround the area.

4.0 RECEPTOR PATHWAY INFORMATION
As defined by NCDEQ, a receptor is “any human, plant, or animal that is or has the potential to be
adversely affected by the release or migration of contaminants”. With respect to the subject facility, the
following sections present information regarding potential receptor pathways for the migration of
contaminants and pathway relationships to the facility.

In an effort to efficiently gather complete and accurate data, ATC personnel performed a receptor survey
of the area. Activities included a visual reconnaissance survey within 1,500 feet radial distance of the site
and obtaining utility information from the City of Graham Water and Sewer Department. The results of
the survey, regarding the potential identification of water wells located within 1,500 feet of the site, are
summarized below.

4.1 Water Supply Wells
ATC conducted a water supply well survey in the surrounding vicinity of the site. As part of the survey,
ATC performed the following:
 ATC conducted a visual reconnaissance on February 24, 2020. The reconnaissance was performed
by driving and/or walking throughout the surrounding area and visually assessing the individual
parcels of land for evidence of water supply wells, well houses, and/or water meters within a radius
of 1,500 feet from the source area.
 ATC contacted the City of Graham Water and Sewer Department, to determine which properties
within 1,500 feet of the source area were connected to the county water system.
Phase I Limited Site Assessment Report March 11, 2020
Pilot Travel Center #6955 (Incident #45093) ATC Project No. PT00695504
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 ATC utilized the Alamance County Geographic Information System website Wells database, to
determine if known wells were identified within 1,500 feet of the source area.

Based on ATC’s findings, there is one water supply well located approximately 800 feet north of the source
area. According to the City of Graham, this property has an active water account. Information regarding this
water supply well is included in Table 1 and the location of the water supply well is depicted on Figure 3.

4.2 Public Water Supplies
Public water supply to the area is provided by the City of Graham Water and Sewer Department.

4.3 Surface Water Bodies
As shown on Figure 1, an unnamed pond is located approximately 1,100 feet west of the site. The Haw
River is located approximately 2,400 feet west of the site.

4.4 Wellhead Protection Areas
ATC reviewed the list of wellhead protection areas and no wellhead protection areas were identified in
the site vicinity.

4.5 Regional Geology and Hydrogeology
The site is located in the Piedmont Physiographic Region comprised of intermediate metavolcanic rock of
the Cambrian/Late Proterozoic consisting of metamorphosed andesitic tuffs and flows and minor felsic
and mafic metavolcanic rock.

The occurrence and movement of groundwater in the Piedmont is within two separate, but interconnected,
water-bearing zones. A shallow water-bearing zone occurs within the surficial soils and a deeper zone
occurs within the underlying bedrock. Groundwater in the shallow soil zone occurs in the interstitial pore
spaces between the grains comprising the surficial soils. Groundwater in this zone is typically
unconfined. Groundwater movement is generally lateral from recharge areas to small streams that serve
as localized discharge points. The occurrence and movement of groundwater in the underlying water-
bearing zone within the crystalline bedrock is controlled by secondary joints, fractures, and faults within
the bedrock. On a regional scale, the direction of groundwater flow is typically from uplands to major
streams and groundwater sinks.

Phase I Limited Site Assessment Report March 11, 2020
Pilot Travel Center #6955 (Incident #45093) ATC Project No. PT00695504
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4.6 Subsurface Structures
Subsurface structures identified at the subject facility include municipal water and sewer lines. A water
meter and sewer manholes were observed on-site. Other utilities may be present.

ATC reviewed tax property cards available on the Alamance County Tax Administration webpage, to
determine the presence of subsurface structures at the site or on adjacent properties. Based on the survey,
structures at the site or properties within 1,500 feet do not appear to extend beneath the subsurface (i.e.
basements).

4.7 Land Use
The properties surrounding the site are commercial, industrial, or wooded. The nearest residence is
located approximately 750 feet north of the site. Adjacent property use is summarized in Table 2.

5.0 LIMITED SITE ASSESSMENT ACTIVITIES
The limited site assessment activities performed to collect data for this report included researching
site-specific, local and regional data, performing soil and groundwater sampling, and submitting soil and
groundwater samples for analytical testing. Information was also obtained from prior reports, prepared by
ATC. The following sections discuss specific methodologies used in conducting these limited site
assessment activities.

5.1 Soil Sampling
Three soil samples, MW-1 (5-6’), MW-1 (10-11’), and MW-1 (15-16’) were collected during the
installation of monitoring well MW-1, using hollow stem augers on January 16, 2020. These samples
were collected into laboratory-approved containers, packed in ice, and delivered under chain-of-custody
to Pace Analytical, for analyses. Soil samples MW-1 (5-6’) and MW-1 (15-16’) were requested to be
analyzed by Environmental Protection Agency (EPA) Methods 8260 and 8270 and Massachusetts
Department of Environmental Protection (MADEP) Methods for Extractable Petroleum Hydrocarbons
(EPH) and Volatile Petroleum Hydrocarbons (VPH). Soil sample MW-1 (10-11’) was requested to be
analyzed for MADEP EPH and VPH. The boring log is presented in Appendix A.

5.2 Monitoring Well Installation
On January 20, 2020, monitoring well MW-1 was installed by personnel with IET using air rotary
drilling, during the Phase I Limited Site Assessment activities. The location of the monitoring well is
depicted on Figure 2.
Phase I Limited Site Assessment Report March 11, 2020
Pilot Travel Center #6955 (Incident #45093) ATC Project No. PT00695504
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Monitoring well MW-1 was installed to a depth of approximately 29 feet below ground surface (bgs).
The well was installed using air rotary and constructed of two-inch diameter well casing made of
flush-joint, threaded schedule-40 poly vinyl chloride (PVC) pipe. The PVC well screen is 0.010-inch slot
with a screened interval of 10 feet. A coarse sand pack (filter pack) was used to backfill the well annulus
to a depth of approximately one foot above the well screen. A one-foot thick bentonite seal was placed
above the filter pack, and neat cement was used to fill the remainder of the well annulus to ground
surface. The well was installed as flush-mounted and was provided with a sealing and locking cap. A
protective, steel-traffic bearing cover was placed over the well upon completion. The boring log and well
construction record are presented in Appendix A.

5.3 Groundwater Sampling
On January 31, 2020, a groundwater sample was collected from monitoring well MW-1. The water level
was recorded from the well utilizing an oil/water interface probe (12.81 feet bgs). Prior to sample
collection, the respective well volume was calculated, and a minimum of three well volumes were purged
from the well column, to ensure replacement of stagnant water with representative formation water.

The groundwater sample was collected into laboratory-approved containers, packed in ice, and delivered
under chain-of-custody to Pace in Mount Juliet, Tennessee for analyses. The sample was analyzed by EPA
Method 602, EPA Method 625, and MADEP Methods for EPH and VPH.

6.0 SITE GEOLOGY AND HYDROGEOLOGY

6.1 Description of Shallow Subsurface Geology
According to the United States Department of Agriculture Natural Resources Conservation Services Web
Soil Survey, the site is underlain by the Urban land (Ur), defined as impervious layers over
human-transported material.

Soil encountered during the installation of monitoring well MW-1 generally consisted of brown silty sand
to 4 feet bgs; brown, green, and gray silty sand to 8 feet bgs; and light brown clay to 13 feet bgs. Refusal
was encountered at 13 feet bgs. Due to the use of an air rotary drill rig, no lithology was recorded below
13 feet bgs. The boring log and well construction record for MW-1 are provided in Appendix A.

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Pilot Travel Center #6955 (Incident #45093) ATC Project No. PT00695504
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6.2 Groundwater Occurrence
During the groundwater sampling event on January 31, 2020, ATC personnel obtained a groundwater
measurement and groundwater sample from monitoring well MW-1. At the time of sample collection, the
depth-to-groundwater measurement was 12.81 feet below the well top of casing. Table 3 provides a
summary of well construction and depth-to-groundwater measurement.

6.3 Groundwater Flow Direction
Based on information obtained from the topographic map of the area, it appears groundwater flow would be
to the west towards the Haw River located approximately 2,400 feet to the west of the source area.

7.0 ANALYTICAL RESULTS

7.1 Soil Analytical Results
Laboratory analytical results for the soil samples, MW-1 (5-6’), MW-1 (10-11’), and MW-1 (15-16’)
collected from the borehole of monitoring well MW-1 did not indicate the presence of compounds
exceeding the STGW-MSCCs. The soil sample collected during the site check activities (SB-1 5’)
indicated C9-C22 aromatics above the STGW-MSCCs. The soil analytical results obtained during the site
check and monitoring well installation activities are summarized in Table 4. A copy of the laboratory
report and chain-of-custody documents are included in Appendix B. The results of the site check
activities were documented in the August 21, 2018, Site Check Report.

7.2 Groundwater Analytical Results
Laboratory analytical results of the groundwater sample collected from monitoring well MW-1 detected a
dissolved C9-C22 aromatics concentration above its established 2L Standard.

Other dissolved target compound concentrations were detected above laboratory-method detection limits
(MDLs); but, below established 2L Standards. A summary of the groundwater analytical data is
presented in Table 5. Figure 4 depicts contaminants in groundwater exceeding the 2L Standards. A
copy of the laboratory analytical report is included as Appendix B.

8.0 CONCLUSIONS AND RECOMMENDATIONS
8.1 Conclusions
Based on the information obtained during this LSA, it appears the site has been impacted from a
petroleum release.
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Pilot Travel Center #6955 (Incident #45093) ATC Project No. PT00695504
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 The subject facility is connected to the public water supply provided by the City of
Graham Water and Sewer Department.
 The subject facility is not located within an approved Wellhead Protection Area.
 The nearest surface water body was identified as an unnamed pond located approximately
1,100 feet west of the site.
 One water supply well (assumed to be used for non-potable purposes) is located within
1,500 feet of the site. The property was confirmed to be connected to the City of Graham
municipal water supply.
 Laboratory analytical results for the soil samples, MW-1 (5-6’), MW-1 (10-11’), and
MW-1 (15-16’) collected from the borehole of monitoring well MW-1 did not indicate
the presence of compounds exceeding the STGW MSCCs. The soil sample collected
during the site check activities (SB-1 5’) indicated C9-C22 aromatics above the
STGW-MSCCs.
 Light non-aqueous phase liquid was not detected in monitoring well MW-1.
 Laboratory analytical results of the groundwater sample collected from monitoring well
MW-1 detected a dissolved C9-C22 aromatics concentration exceeding its 2L Standard.
Other dissolved target compound concentrations were detected above laboratory MDLs
but below established 2L Standards.

8.2 Recommendations
The results of the LSA activities indicate that the subject facility meets the criteria for Low Risk
classification. ATC recommends no further action.

TABLES
TABLE 1
WATER SUPPLY WELL INFORMATION
PILOT TRAVEL CENTER #6599
1044 JIMMIE KERR ROAD
HAW RIVER, ALAMANCE COUNTY, NORTH CAROLINA
NCDEQ INCIDENT # 45093
Water Supply Well Property Owner(s)Property Address Distance from
Source (feet)
Method of
Identification
Connected to
Municipal Water
Water Supply
Well Usage
WSW-1
L&E Enterprises I LLP
1843H NC Highway 49
Burlington, NC 27217-9145
908 Jimmie Kerr Road 800 feet North Visual during Receptor
Survey Yes Unknown
Notes:
1. Information obtained from the City of Graham and Alamance County GIS systems.
TABLE 2
ADJACENT PROPERTY OWNER INFORMATION
PILOT TRAVEL CENTER #6599
1044 JIMMIE KERR ROAD
HAW RIVER, ALAMANCE COUNTY, NORTH CAROLINA
NCDEQ INCIDENT # 45093
Zoning Classification
Parcel Identification Number
Observed Land Use
Site PFJ Southeast LLC General Business District (B-2)
Pilot Travel Centers #6599 c/o Intax Store 152897
1044 Jimmie Kerr Road P.O. Box 54710 Travel Center with Petroleum Sales
Haw River, North Carolina Lexington, KY 40555
North of the Site Blue Beacon International, Inc.Light Industrial District (I-1)
Blue Beacon Truck Wash P.O. Box 856 152898
950 Jimmie Kerr Road Salina, KS 67402 Truck Wash
Haw River, North Carolina
Northwest of the Site (across Jimmie Kerr Road)PFJ Southeast LLC Light Industrial District (I-1)
Flying J Travel Center c/o Intax Store 152823
1043 Jimmie Kerr Road P.O. Box 54710 Gas Station
Haw River, North Carolina Lexington, KY 40555
Southwest of the Site (across Jimmie Kerr Road)CFJ Properties Light Industrial District (I-1)
Vacant Land Attn Flying J C/O Rash #287, Store #682 152823
Unaddressed P.O. Box 54710 Wooded
Haw River, North Carolina Lexington, KY 40555
Southwest of the Site (across Interstate I-85/40)Rodos Inc.Light Industrial District (I-1)
Wooded c/o Peter Manis 152821
Unaddressed 800 N. Ocean Drive Wooded
Haw River, North Carolina Hollywood, FL 33019
Southeast of the Site (across Interstate I-85/40)I N F Properties LLC Light Industrial District (I-1)
Wooded Interstate Narrow Fabrics 152893
Porter Ave P.O. Box 746 Manufacturing/Warehouse
Haw River, North Carolina Graham, NC 27253
East of the Site I 40 Drive In LLC Light Industrial District (I-1)
Vacant Land P.O. Box 872 173630
Kronberg Court Graham, NC 27253 Cleared and Wooded
Haw River, North Carolina
Property Location and Address Owner's Name and Address
TABLE 3
MONITORING WELL CONSTRUCTION DETAILS
PILOT TRAVEL CENTER #6599
1044 JIMMIE KERR ROAD
HAW RIVER, ALAMANCE COUNTY, NORTH CAROLINA
NCDEQ INCIDENT # 45093
Depth of
Water (feet)
Depth to
Product (feet)
Groundwater
Elevation (feet)
MW-1 01/20/20 2 19-29 29.0 100.00 12.81 --87.19
Notes:
1. Elevation is referenced to an arbitrary on-site benchmark of 100.00 feet.
2. Total well depth measured from top of casing.
Date Measured: 1/31/2020
Monitoring
Well ID
Date
Installed
Well
Casing
Diameter
(Inches)
Screened
Interval
(feet)
Depth of Well
(feet)
Top of Casing
(feet)
TABLE 4
SOIL ANALYTICAL RESULTS
PILOT TRAVEL CENTER #6599
1044 JIMMIE KERR ROAD
HAW RIVER, ALAMANCE COUNTY, NORTH CAROLINA
NCDEQ INCIDENT # 45093
EPA
Method
8270D
Sample
Depth (feet
below ground
surface)
Date
Sampled
PyreneC5-C8 AliphaticsC9-C18 AliphaticsC19-C36 AliphaticsC9-C22 AromaticsSB-1 5 08/13/18 0.080J <11 406 130 193
MW-1 (5-6)5-6 01/16/20 <0.0378 <5.68 ND 12.6 9.84
MW-1 (10-11)10-11 01/16/20 NA <5.73 ND <7.45 ND
MW-1 (15-16)15-16 01/16/20 <0.0361 <5.42 10.5 7.94 9.40
270 68 540 NE 31
469 939 1,500 31,000 469
12,264 24528 40,000 810,000 12,264
Notes:
1. Concentrations reported in milligrams per kilogram (mg/kg).
2. MSCC = Maximum Soil Contaminant Concentration.
3. Bold indicates concentrations above NCDEQ Soil-to-Groundwater MSCC.
4. J denotes value estimated by the laboratory.
5. NA = Not Analyzed.
6. ND = Not Detected.
Soil-to-Groundwater MSCC
Residential MSCC
Industrial/Commercial MSCC
Analytical Method MADEP Method EPH/VPH
TABLE 5
GROUNDWATER ANALYTICAL RESULTS
PILOT TRAVEL CENTER #6599
1044 JIMMIE KERR ROAD
HAW RIVER, ALAMANCE COUNTY, NORTH CAROLINA
NCDEQ INCIDENT # 45093
EPA
METHOD
625
Sample ID Date Sampled
BenzeneTolueneEthylbenzeneTotal XylenesMTBEIPENaphthaleneC5-C8 AliphaticsC9-C18 AliphaticsC19-C36 AliphaticsC9-C22 AromaticsMW-1 01/31/20 <1 <1 <1 <3 <1 <1 <1 <100 104 <100 511
1 600 600 500 20 70 6 400 700 10,000 200
5,000 260,000 84,500 85,500 20,000 70,000 6,000 NE NE NE NE
Notes:
1. Concentrations reported in micrograms per liter (ug/L).
2. NE = Not established.
3. Bold text indicates concentrations above NCAC 2L Groundwater Quality Standard.
4. Final C9-C18 Aliphatics values are equal to C9-C12 Aliphatics plus C9-C18 Aliphatics as reported in the laboratory report.
5. Final C9-C22 Aromatics are equal to C9-C10 Aromatics plus C11-C22 Aromatics as reported in the laboratory analytical report.
NCAC 2L Groundwater
Quality Standards (ug/L)
Gross Contaminant Level
(ug/L)
ANALYTICAL METHOD EPA METHOD 602 MADEP METHODS for VPH
and EPH

FIGURES

APPENDIX A
SOIL BORING LOG AND
WELL CONSTRUCTION RECORD

03-02-2020 S:\Enviro\Pilot\Pilot 6955 - Haw River\Boring Logs\MW-1.borClient: Pilot
ATC Project No. PT00695504
Haw River, Alamance County, North Carolina
1044 Jimmie Kerr Road
Pilot #6955
-Boring was hand cleared to 5 feet below ground surface (bgs).
-Refusal at 13 feet bgs with Hollow Stem Auger (HSA). Continued with Air Rig
to 29 feet bgs. Unable to record lithology due to the use of Air Rig.
-Depth to water at 22 feet bgs.
BORING LOG: MW-1
(Page 1 of 1)
Date(s) Drilled : 01/16/2020
Drilling Contractor : IET
Drilling Method : Hand Auger/ HSA, Air Rotary
Boring Diameter : 8.5 Inches
Sampling Method : Macrocore With DPT
Sampling Interval : NA
Logged By : Cory Nobles
Depth In Feet0
5
10
15
20
25
30 USCSGRAPHICDESCRIPTION VOCs
(ppm)
17.5
36.2
16.2
Well: MW-1
Grout
Bentonite
Sand Pack
Casing
Screen
AR
SM
SM
CL
F0
Asphalt
Brown, Silty SAND with rock fragments
Brown, green, and gray, Silty SAND, mild petroleum odor present
light brown, Silty CLAY, dry, no odor
No Lithology Recorded
End Of Boring

WELL CONSTRUCTION RECORD (GW-1) For Internal Use Only:

Form GW-1 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1. Well Contractor Information:

Well Contractor Name

NC Well Contractor Certification Number

Company Name

2. Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.)

3. Well Use (check well use):
Water Supply Well:
□Agricultural □Municipal/Public
□Geothermal (Heating/Cooling Supply) □Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared)
□Irrigation
Non-Water Supply Well:
□Monitoring □Recovery
Injection Well:
□Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier
□Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop) □Tracer
□Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks)

4. Date Well(s) Completed: Well ID#
5a. Well Location:

Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip

County Parcel Identification No. (PIN)

5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)

N W

6. Is(are) the well(s): □Permanent or □Temporary

7. Is this a repair to an existing well: □Yes or □No
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.

8. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
construction, only 1 GW-1 is needed. Indicate TOTAL NUMBER of wells
drilled:

9. Total well depth below land surface: (ft.)
For multiple wells list all depths if different (example- 3@200’ and 2@100′)

10. Static water level below top of casing: (ft.)
If water level is above casing, use “+”
11. Borehole diameter: (in.)

12. Well construction method:
(i.e. auger, rotary, cable, direct push, etc.)

FOR WATER SUPPLY WELLS ONLY:

13a. Yield (gpm) Method of test:
13b. Disinfection type: Amount:

14. WATER ZONES
FROM TO DESCRIPTION
ft. ft.
ft. ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable)
FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
17. SCREEN
FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
18. GROUT
FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
ft. ft.
ft. ft.
ft. ft.
19. SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
ft. ft.
ft. ft.
20. DRILLING LOG (attach additional sheets if necessary)
FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
21. REMARKS

22. Certification:

Signature of Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a
copy of this record has been provided to the well owner.
23. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
construction details. You may also attach additional pages if necessary.

SUBMITTAL INSTRUCTIONS

24a. For All Wells: Submit this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells: In addition to sending the form to the address in 24a
above, also submit one copy of this form within 30 days of completion of well
construction to the following:

Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells: In addition to sending the form to
the address(es) above, also submit one copy of this form within 30 days of
completion of well construction to the county health department of the county
where constructed.
Mike Tynan
2725-A
IET
Jan 20, 2020 MW-1
Pilot #6955
1044 Jimmie Kerr Rd, Haw River 27258
Alamance
36 04 16.44 79 21 04.85
30
~22
8.5
auger, rotary
2/13/2020
22 30 pwr
0 20 2 Sch40 PVC
10 30 2 0.010 Sch40 PVC
0
0.5
15
18
0.5
15
18
40
concrete
neat cement
bentonite
#2 silica sand pour through augers
pour
See Report
MW completed at surface with flush well cover and 2'x2'
concrete pad.
Print Form
pour
pour

APPENDIX B
LABORATORY ANALYTICAL RESULTS

39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
August 16, 2018
Maureen Jackson
ATC Group Services LLC - Raleigh NC
2725 East Millbrook Road, Ste 121
Raleigh, NC 27604
Project Location: Haw River, NC
Client Job Number:
Project Number: PT00695501
Laboratory Work Order Number: 18H0706
Enclosed are results of analyses for samples received by the laboratory on August 15, 2018. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Kerry K. McGee
Project Manager
Page 1 of 39
Table of Contents
Table of Contents
Sample Summary 3
Hits Only Report 4
Case Narrative 5
Sample Results 7
18H0706-01 7
Sample Preparation Information 14
QC Data 15
Volatile Organic Compounds by GC/MS 15
B210357 15
Semivolatile Organic Compounds by GC/MS 20
B210345 20
Petroleum Hydrocarbons Analyses - EPH 25
B210344 25
Petroleum Hydrocarbons Analyses - VPH 28
B209997 28
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) 30
B210372 30
Flag/Qualifier Summary 31
Certifications 32
Chain of Custody/Sample Receipt 37
Page 2 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
8/16/2018
ATC Group Services LLC - Raleigh NC
2725 East Millbrook Road, Ste 121
Raleigh, NC 27604
ATTN: Maureen Jackson
PT00695501
18H0706
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Haw River, NC
SB-1 18H0706-01 Soil MADEP-EPH-04-1.1
MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
SW-846 8260B
SW-846 8270D
[TOC_1]Sample Summary[TOC]
Page 3 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
[TOC_1]Hits Only Report[TOC]EXECUTIVE SUMMARY
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
18H0706-01SB-1
DL
Pyrene 0.080 0.20 mg/Kg dry SW-846 8270DJ0.065
C11-C22 Aromatics 160 12 mg/Kg dry MADEP-EPH-04-1.1
C19-C36 Aliphatics 130 12 mg/Kg dry MADEP-EPH-04-1.1
C9-C18 Aliphatics 380 58 mg/Kg dry MADEP-EPH-04-1.1
Unadjusted C11-C22 Aromatics 160 12 mg/Kg dry MADEP-EPH-04-1.1
C9-C10 Aromatics 33 11 mg/Kg dry MADEP-VPH-Feb 2018 Rev 2.11.6
C9-C12 Aliphatics 26 11 mg/Kg dry MADEP-VPH-Feb 2018 Rev 2.12.3
Unadjusted C9-C12 Aliphatics 59 11 mg/Kg dry MADEP-VPH-Feb 2018 Rev 2.12.3
% Solids 86.3 % Wt SM 2540G
Con-Test does not accept liability for the consequences of any actions taken solely on the basis of the information provided in the Executive Summary
section of this report. Users must review this report in its entirety to determine data usability and assessment.
Page 4 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
For method MA VPH only hydrocarbon ranges were requested and reported.
For method MA EPH, only hydrocarbon ranges were requested and reported.
[TOC_1]Case Narrative[TOC]
SW-846 8270D
Qualifications:
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD
between the two LFB/LCS results is within method specified criteria.
Analyte & Samples(s) Qualified:
L-07
Hexachlorocyclopentadiene
B210345-BS1
Initial calibration did not meet method specifications. Compound was calibrated using a response factor where %RSD is outside of method
specified criteria. Reported result is estimated.
Analyte & Samples(s) Qualified:
V-04
Benzidine
18H0706-01[SB-1], B210345-BLK1, B210345-BS1, B210345-BSD1
Continuing calibration did not meet method specifications and was biased on the low side for this compound. Reported result is estimated.
Analyte & Samples(s) Qualified:
V-05
Hexachlorocyclopentadiene
18H0706-01[SB-1], B210345-BLK1, B210345-BS1, B210345-BSD1
Continuing calibration did not meet method specifications and was biased on the high side for this compound. Reported result is estimated.
Analyte & Samples(s) Qualified:
V-06
Benzidine
B210345-BS1, B210345-BSD1
Continuing calibration did not meet method specifications and was biased on the high side. Data validation is not affected since sample result
was "not detected" for this compound.
Analyte & Samples(s) Qualified:
V-20
Benzidine
18H0706-01[SB-1], B210345-BLK1
Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this compound. Reported result is
estimated.
Analyte & Samples(s) Qualified:
V-34
3,3-Dichlorobenzidine
18H0706-01[SB-1], B210345-BLK1, B210345-BS1, B210345-BSD1
3-Nitroaniline
18H0706-01[SB-1], B210345-BLK1, B210345-BS1, B210345-BSD1
4-Chloroaniline
18H0706-01[SB-1], B210345-BLK1, B210345-BS1, B210345-BSD1
Aniline
18H0706-01[SB-1], B210345-BLK1, B210345-BS1, B210345-BSD1
Page 5 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
MADEP-EPH-04-1.1
SPE cartridge contamination with non-petroleum compounds, if present, is verified by GC/MS in each method blank per extraction batch and excluded from C 11-C22 aromatic
range fraction in all samples in the batch. No significant modifications were made to the method.
MADEP-VPH-Feb 2018 Rev 2.1
Analytical column used for VPH analysis is Restek, Rtx-502.2, 105meter, 0.53mmID, 3um df. Trap used for VPH analysis is Carbopack B/CarboSieveS-III.
No significant modifications were made to the method. All VPH samples were received preserved properly in methanol with a soil/methanol ratio of 1:1 +/- 25% completely
covered by methanol in the proper containers specified on the chain-of-custody form unless specified in this narrative.
The results of analyses reported only relate to samples submitted to the Con-Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Daren J. Damboragian
Director of Operations
Page 6 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 8/15/2018
Work Order: 18H0706Sample Description:Project Location: Haw River, NC
Sample ID: 18H0706-01
Field Sample #: SB-1
Sample Matrix: Soil
Sampled: 8/13/2018 17:00
[TOC_2]18H0706-01[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 2.8 8/15/18 12:22 MFFmg/Kg dry0.55 8/15/18SW-846 8260B1Acetone
ND 0.28 8/15/18 12:22 MFFmg/Kg dry0.033 8/15/18SW-846 8260B1Acrylonitrile
ND 0.028 8/15/18 12:22 MFFmg/Kg dry0.0060 8/15/18SW-846 8260B1tert-Amyl Methyl Ether (TAME)
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0068 8/15/18SW-846 8260B1Benzene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0085 8/15/18SW-846 8260B1Bromobenzene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.013 8/15/18SW-846 8260B1Bromochloromethane
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.017 8/15/18SW-846 8260B1Bromodichloromethane
ND 0.11 8/15/18 12:22 MFFmg/Kg dry0.012 8/15/18SW-846 8260B1Bromoform
ND 0.11 8/15/18 12:22 MFFmg/Kg dry0.054 8/15/18SW-846 8260B1Bromomethane
ND 1.1 8/15/18 12:22 MFFmg/Kg dry0.13 8/15/18SW-846 8260B12-Butanone (MEK)
ND 1.1 8/15/18 12:22 MFFmg/Kg dry0.12 8/15/18SW-846 8260B1tert-Butyl Alcohol (TBA)
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0085 8/15/18SW-846 8260B1n-Butylbenzene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0074 8/15/18SW-846 8260B1sec-Butylbenzene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0069 8/15/18SW-846 8260B1tert-Butylbenzene
ND 0.028 8/15/18 12:22 MFFmg/Kg dry0.0054 8/15/18SW-846 8260B1tert-Butyl Ethyl Ether (TBEE)
ND 0.17 8/15/18 12:22 MFFmg/Kg dry0.058 8/15/18SW-846 8260B1Carbon Disulfide
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.014 8/15/18SW-846 8260B1Carbon Tetrachloride
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0091 8/15/18SW-846 8260B1Chlorobenzene
ND 0.028 8/15/18 12:22 MFFmg/Kg dry0.0059 8/15/18SW-846 8260B1Chlorodibromomethane
ND 0.11 8/15/18 12:22 MFFmg/Kg dry0.016 8/15/18SW-846 8260B1Chloroethane
ND 0.11 8/15/18 12:22 MFFmg/Kg dry0.013 8/15/18SW-846 8260B1Chloroform
ND 0.11 8/15/18 12:22 MFFmg/Kg dry0.031 8/15/18SW-846 8260B1Chloromethane
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0068 8/15/18SW-846 8260B12-Chlorotoluene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0080 8/15/18SW-846 8260B14-Chlorotoluene
ND 0.28 8/15/18 12:22 MFFmg/Kg dry0.021 8/15/18SW-846 8260B11,2-Dibromo-3-chloropropane (DBCP)
ND 0.028 8/15/18 12:22 MFFmg/Kg dry0.0084 8/15/18SW-846 8260B11,2-Dibromoethane (EDB)
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0091 8/15/18SW-846 8260B1Dibromomethane
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0097 8/15/18SW-846 8260B11,2-Dichlorobenzene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0097 8/15/18SW-846 8260B11,3-Dichlorobenzene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0085 8/15/18SW-846 8260B11,4-Dichlorobenzene
ND 0.11 8/15/18 12:22 MFFmg/Kg dry0.018 8/15/18SW-846 8260B1trans-1,4-Dichloro-2-butene
ND 0.11 8/15/18 12:22 MFFmg/Kg dry0.016 8/15/18SW-846 8260B1Dichlorodifluoromethane (Freon 12)
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0090 8/15/18SW-846 8260B11,1-Dichloroethane
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.011 8/15/18SW-846 8260B11,2-Dichloroethane
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.012 8/15/18SW-846 8260B11,1-Dichloroethylene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0084 8/15/18SW-846 8260B1cis-1,2-Dichloroethylene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0085 8/15/18SW-846 8260B1trans-1,2-Dichloroethylene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0074 8/15/18SW-846 8260B11,2-Dichloropropane
ND 0.028 8/15/18 12:22 MFFmg/Kg dry0.0074 8/15/18SW-846 8260B11,3-Dichloropropane
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.012 8/15/18SW-846 8260B12,2-Dichloropropane
ND 0.11 8/15/18 12:22 MFFmg/Kg dry0.0073 8/15/18SW-846 8260B11,1-Dichloropropene
ND 0.028 8/15/18 12:22 MFFmg/Kg dry0.0068 8/15/18SW-846 8260B1cis-1,3-Dichloropropene
ND 0.028 8/15/18 12:22 MFFmg/Kg dry0.0064 8/15/18SW-846 8260B1trans-1,3-Dichloropropene
ND 0.11 8/15/18 12:22 MFFmg/Kg dry0.013 8/15/18SW-846 8260B1Diethyl Ether
[TOC_1]Sample Results[TOC]
Page 7 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 8/15/2018
Work Order: 18H0706Sample Description:Project Location: Haw River, NC
Sample ID: 18H0706-01
Field Sample #: SB-1
Sample Matrix: Soil
Sampled: 8/13/2018 17:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.028 8/15/18 12:22 MFFmg/Kg dry0.010 8/15/18SW-846 8260B1Diisopropyl Ether (DIPE)
ND 2.8 8/15/18 12:22 MFFmg/Kg dry1.5 8/15/18SW-846 8260B11,4-Dioxane
ND 11 8/15/18 12:22 MFFmg/Kg dry1.6 8/15/18SW-846 8260B1Ethanol
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0074 8/15/18SW-846 8260B1Ethylbenzene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.034 8/15/18SW-846 8260B1Hexachlorobutadiene
ND 0.57 8/15/18 12:22 MFFmg/Kg dry0.087 8/15/18SW-846 8260B12-Hexanone (MBK)
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0068 8/15/18SW-846 8260B1Isopropylbenzene (Cumene)
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0085 8/15/18SW-846 8260B1p-Isopropyltoluene (p-Cymene)
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0051 8/15/18SW-846 8260B1Methyl tert-Butyl Ether (MTBE)
ND 0.28 8/15/18 12:22 MFFmg/Kg dry0.18 8/15/18SW-846 8260B1Methylene Chloride
ND 0.57 8/15/18 12:22 MFFmg/Kg dry0.084 8/15/18SW-846 8260B14-Methyl-2-pentanone (MIBK)
ND 0.11 8/15/18 12:22 MFFmg/Kg dry0.0069 8/15/18SW-846 8260B1Naphthalene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0074 8/15/18SW-846 8260B1n-Propylbenzene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0085 8/15/18SW-846 8260B1Styrene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0068 8/15/18SW-846 8260B11,1,1,2-Tetrachloroethane
ND 0.028 8/15/18 12:22 MFFmg/Kg dry0.0091 8/15/18SW-846 8260B11,1,2,2-Tetrachloroethane
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.015 8/15/18SW-846 8260B1Tetrachloroethylene
ND 0.57 8/15/18 12:22 MFFmg/Kg dry0.061 8/15/18SW-846 8260B1Tetrahydrofuran
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0097 8/15/18SW-846 8260B1Toluene
ND 0.28 8/15/18 12:22 MFFmg/Kg dry0.0080 8/15/18SW-846 8260B11,2,3-Trichlorobenzene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.011 8/15/18SW-846 8260B11,2,4-Trichlorobenzene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0097 8/15/18SW-846 8260B11,3,5-Trichlorobenzene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0075 8/15/18SW-846 8260B11,1,1-Trichloroethane
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.013 8/15/18SW-846 8260B11,1,2-Trichloroethane
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.011 8/15/18SW-846 8260B1Trichloroethylene
ND 0.11 8/15/18 12:22 MFFmg/Kg dry0.0084 8/15/18SW-846 8260B1Trichlorofluoromethane (Freon 11)
ND 0.11 8/15/18 12:22 MFFmg/Kg dry0.012 8/15/18SW-846 8260B11,2,3-Trichloropropane
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.011 8/15/18SW-846 8260B11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.010 8/15/18SW-846 8260B11,2,4-Trimethylbenzene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0074 8/15/18SW-846 8260B11,3,5-Trimethylbenzene
ND 0.11 8/15/18 12:22 MFFmg/Kg dry0.0076 8/15/18SW-846 8260B1Vinyl Chloride
ND 0.11 8/15/18 12:22 MFFmg/Kg dry0.015 8/15/18SW-846 8260B1m+p Xylene
ND 0.057 8/15/18 12:22 MFFmg/Kg dry0.0075 8/15/18SW-846 8260B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 91.2 8/15/18 12:2270-130
Toluene-d8 97.7 8/15/18 12:2270-130
4-Bromofluorobenzene 102 8/15/18 12:2270-130
Page 8 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 8/15/2018
Work Order: 18H0706Sample Description:Project Location: Haw River, NC
Sample ID: 18H0706-01
Field Sample #: SB-1
Sample Matrix: Soil
Sampled: 8/13/2018 17:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.059 8/15/18SW-846 8270D1Acenaphthene
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.066 8/15/18SW-846 8270D1Acenaphthylene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.077 8/15/18SW-846 8270D1Acetophenone
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.11 8/15/18SW-846 8270D1V-34Aniline
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.057 8/15/18SW-846 8270D1Anthracene
ND 0.76 8/15/18 15:01 CDTmg/Kg dry0.49 8/15/18SW-846 8270D1V-04, V-20Benzidine
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.052 8/15/18SW-846 8270D1Benzo(a)anthracene
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.061 8/15/18SW-846 8270D1Benzo(a)pyrene
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.055 8/15/18SW-846 8270D1Benzo(b)fluoranthene
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.087 8/15/18SW-846 8270D1Benzo(g,h,i)perylene
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.061 8/15/18SW-846 8270D1Benzo(k)fluoranthene
ND 1.2 8/15/18 15:01 CDTmg/Kg dry0.21 8/15/18SW-846 8270D1Benzoic Acid
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.075 8/15/18SW-846 8270D1Bis(2-chloroethoxy)methane
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.077 8/15/18SW-846 8270D1Bis(2-chloroethyl)ether
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.084 8/15/18SW-846 8270D1Bis(2-chloroisopropyl)ether
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.15 8/15/18SW-846 8270D1Bis(2-Ethylhexyl)phthalate
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.066 8/15/18SW-846 8270D14-Bromophenylphenylether
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.094 8/15/18SW-846 8270D1Butylbenzylphthalate
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.051 8/15/18SW-846 8270D1Carbazole
ND 0.76 8/15/18 15:01 CDTmg/Kg dry0.090 8/15/18SW-846 8270D1V-344-Chloroaniline
ND 0.76 8/15/18 15:01 CDTmg/Kg dry0.084 8/15/18SW-846 8270D14-Chloro-3-methylphenol
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.074 8/15/18SW-846 8270D12-Chloronaphthalene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.070 8/15/18SW-846 8270D12-Chlorophenol
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.066 8/15/18SW-846 8270D14-Chlorophenylphenylether
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.061 8/15/18SW-846 8270D1Chrysene
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.12 8/15/18SW-846 8270D1Dibenz(a,h)anthracene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.068 8/15/18SW-846 8270D1Dibenzofuran
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.085 8/15/18SW-846 8270D1Di-n-butylphthalate
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.069 8/15/18SW-846 8270D11,2-Dichlorobenzene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.067 8/15/18SW-846 8270D11,3-Dichlorobenzene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.070 8/15/18SW-846 8270D11,4-Dichlorobenzene
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.060 8/15/18SW-846 8270D1V-343,3-Dichlorobenzidine
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.067 8/15/18SW-846 8270D12,4-Dichlorophenol
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.070 8/15/18SW-846 8270D1Diethylphthalate
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.073 8/15/18SW-846 8270D12,4-Dimethylphenol
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.069 8/15/18SW-846 8270D1Dimethylphthalate
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.37 8/15/18SW-846 8270D14,6-Dinitro-2-methylphenol
ND 0.76 8/15/18 15:01 CDTmg/Kg dry0.22 8/15/18SW-846 8270D12,4-Dinitrophenol
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.064 8/15/18SW-846 8270D12,4-Dinitrotoluene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.069 8/15/18SW-846 8270D12,6-Dinitrotoluene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.21 8/15/18SW-846 8270D1Di-n-octylphthalate
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.064 8/15/18SW-846 8270D11,2-Diphenylhydrazine (as Azobenzene)
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.065 8/15/18SW-846 8270D1Fluoranthene
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.064 8/15/18SW-846 8270D1Fluorene
Page 9 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 8/15/2018
Work Order: 18H0706Sample Description:Project Location: Haw River, NC
Sample ID: 18H0706-01
Field Sample #: SB-1
Sample Matrix: Soil
Sampled: 8/13/2018 17:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.069 8/15/18SW-846 8270D1Hexachlorobenzene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.069 8/15/18SW-846 8270D1Hexachlorobutadiene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.083 8/15/18SW-846 8270D1V-05Hexachlorocyclopentadiene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.079 8/15/18SW-846 8270D1Hexachloroethane
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.14 8/15/18SW-846 8270D1Indeno(1,2,3-cd)pyrene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.076 8/15/18SW-846 8270D1Isophorone
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.075 8/15/18SW-846 8270D11-Methylnaphthalene
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.068 8/15/18SW-846 8270D12-Methylnaphthalene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.098 8/15/18SW-846 8270D12-Methylphenol
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.12 8/15/18SW-846 8270D13/4-Methylphenol
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.10 8/15/18SW-846 8270D1Naphthalene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.066 8/15/18SW-846 8270D12-Nitroaniline
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.057 8/15/18SW-846 8270D1V-343-Nitroaniline
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.066 8/15/18SW-846 8270D14-Nitroaniline
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.074 8/15/18SW-846 8270D1Nitrobenzene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.10 8/15/18SW-846 8270D12-Nitrophenol
ND 0.76 8/15/18 15:01 CDTmg/Kg dry0.085 8/15/18SW-846 8270D14-Nitrophenol
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.25 8/15/18SW-846 8270D1N-Nitrosodimethylamine
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.081 8/15/18SW-846 8270D1N-Nitrosodiphenylamine
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.081 8/15/18SW-846 8270D1N-Nitrosodi-n-propylamine
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.094 8/15/18SW-846 8270D1Pentachloronitrobenzene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.095 8/15/18SW-846 8270D1Pentachlorophenol
ND 0.20 8/15/18 15:01 CDTmg/Kg dry0.10 8/15/18SW-846 8270D1Phenanthrene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.067 8/15/18SW-846 8270D1Phenol
0.080 0.20 8/15/18 15:01 CDTmg/Kg dry0.065 8/15/18SW-846 8270D1JPyrene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.064 8/15/18SW-846 8270D1Pyridine
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.070 8/15/18SW-846 8270D11,2,4,5-Tetrachlorobenzene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.070 8/15/18SW-846 8270D11,2,4-Trichlorobenzene
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.089 8/15/18SW-846 8270D12,4,5-Trichlorophenol
ND 0.39 8/15/18 15:01 CDTmg/Kg dry0.066 8/15/18SW-846 8270D12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 63.7 8/15/18 15:0130-130
Phenol-d6 64.5 8/15/18 15:0130-130
Nitrobenzene-d5 63.4 8/15/18 15:0130-130
2-Fluorobiphenyl 72.7 8/15/18 15:0130-130
2,4,6-Tribromophenol 62.0 8/15/18 15:0130-130
p-Terphenyl-d14 76.4 8/15/18 15:0130-130
Page 10 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 8/15/2018
Work Order: 18H0706Sample Description:Project Location: Haw River, NC
Sample ID: 18H0706-01
Field Sample #: SB-1
Sample Matrix: Soil
Sampled: 8/13/2018 17:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - EPH
380 58 8/16/18 9:36 RMWmg/Kg dry 8/15/18MADEP-EPH-04-1.15C9-C18 Aliphatics
130 12 8/16/18 4:45 RMWmg/Kg dry 8/15/18MADEP-EPH-04-1.11C19-C36 Aliphatics
160 12 8/16/18 4:45 RMWmg/Kg dry 8/15/18MADEP-EPH-04-1.11Unadjusted C11-C22 Aromatics
160 12 8/16/18 4:45 RMWmg/Kg dry 8/15/18MADEP-EPH-04-1.11C11-C22 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD)74.5 8/16/18 4:4540-140
o-Terphenyl (OTP)74.4 8/16/18 4:4540-140
2-Bromonaphthalene 94.2 8/16/18 4:4540-140
2-Fluorobiphenyl 81.0 8/16/18 4:4540-140
Page 11 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 8/15/2018
Work Order: 18H0706Sample Description:Project Location: Haw River, NC
Sample ID: 18H0706-01
Field Sample #: SB-1
Sample Matrix: Soil
Sampled: 8/13/2018 17:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Soil/Methanol Preservation Ratio: 1.17
Petroleum Hydrocarbons Analyses - VPH
ND 11 8/15/18 11:27 EEHmg/Kg dry 8/15/18MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 11 8/15/18 11:27 EEHmg/Kg dry 8/15/18MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
59 11 8/15/18 11:27 EEHmg/Kg dry 8/15/18MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
26 11 8/15/18 11:27 EEHmg/Kg dry 8/15/18MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
33 11 8/15/18 11:27 EEHmg/Kg dry 8/15/18MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)80.4 8/15/18 11:2770-130
2,5-Dibromotoluene (PID)80.1 8/15/18 11:2770-130
Page 12 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 8/15/2018
Work Order: 18H0706Sample Description:Project Location: Haw River, NC
Sample ID: 18H0706-01
Field Sample #: SB-1
Sample Matrix: Soil
Sampled: 8/13/2018 17:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
86.3 8/15/18 17:56 JFC% Wt 8/15/18SM 2540G1% Solids
Page 13 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: SW-846 3546-MADEP-EPH-04-1.1
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B210344 08/15/1820.0 2.0018H0706-01 [SB-1]
Prep Method: MA VPH-MADEP-VPH-Feb 2018 Rev 2.1
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B209997 08/15/185.90 5.8018H0706-01 [SB-1]
Prep Method: % Solids-SM 2540G
Lab Number [Field ID]Batch Date
B210372 08/15/1818H0706-01 [SB-1]
Prep Method: SW-846 5035/5030B-SW-846 8260B
Lab Number [Field ID]Batch
Sample
Amount(g)
Methanol
Volume(mL)
Methanol
Aliquot(mL)
Final
Volume(mL)Date
18H0706-01 [SB-1]B210357 5.90 5.80 1 50 08/15/18
Prep Method: SW-846 3546-SW-846 8270D
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B210345 08/15/1830.1 1.0018H0706-01 [SB-1]
[TOC_1]Sample Preparation Information[TOC]
Page 14 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Volatile Organic Compounds by GC/MS[TOC]
Batch B210357 - SW-846 5035/5030B
[TOC_3]B210357[TOC]
Blank (B210357-BLK1) Prepared & Analyzed: 08/15/18
Acetone mg/Kg wet2.5ND
Acrylonitrile mg/Kg wet0.25ND
tert-Amyl Methyl Ether (TAME)mg/Kg wet0.025ND
Benzene mg/Kg wet0.050ND
Bromobenzene mg/Kg wet0.050ND
Bromochloromethane mg/Kg wet0.050ND
Bromodichloromethane mg/Kg wet0.050ND
Bromoform mg/Kg wet0.10ND
Bromomethane mg/Kg wet0.10ND
2-Butanone (MEK)mg/Kg wet1.0ND
tert-Butyl Alcohol (TBA)mg/Kg wet1.0ND
n-Butylbenzene mg/Kg wet0.050ND
sec-Butylbenzene mg/Kg wet0.050ND
tert-Butylbenzene mg/Kg wet0.050ND
tert-Butyl Ethyl Ether (TBEE)mg/Kg wet0.025ND
Carbon Disulfide mg/Kg wet0.15ND
Carbon Tetrachloride mg/Kg wet0.050ND
Chlorobenzene mg/Kg wet0.050ND
Chlorodibromomethane mg/Kg wet0.025ND
Chloroethane mg/Kg wet0.10ND
Chloroform mg/Kg wet0.10ND
Chloromethane mg/Kg wet0.10ND
2-Chlorotoluene mg/Kg wet0.050ND
4-Chlorotoluene mg/Kg wet0.050ND
1,2-Dibromo-3-chloropropane (DBCP)mg/Kg wet0.25ND
1,2-Dibromoethane (EDB)mg/Kg wet0.025ND
Dibromomethane mg/Kg wet0.050ND
1,2-Dichlorobenzene mg/Kg wet0.050ND
1,3-Dichlorobenzene mg/Kg wet0.050ND
1,4-Dichlorobenzene mg/Kg wet0.050ND
trans-1,4-Dichloro-2-butene mg/Kg wet0.10ND
Dichlorodifluoromethane (Freon 12)mg/Kg wet0.10ND
1,1-Dichloroethane mg/Kg wet0.050ND
1,2-Dichloroethane mg/Kg wet0.050ND
1,1-Dichloroethylene mg/Kg wet0.050ND
cis-1,2-Dichloroethylene mg/Kg wet0.050ND
trans-1,2-Dichloroethylene mg/Kg wet0.050ND
1,2-Dichloropropane mg/Kg wet0.050ND
1,3-Dichloropropane mg/Kg wet0.025ND
2,2-Dichloropropane mg/Kg wet0.050ND
1,1-Dichloropropene mg/Kg wet0.10ND
cis-1,3-Dichloropropene mg/Kg wet0.025ND
trans-1,3-Dichloropropene mg/Kg wet0.025ND
Diethyl Ether mg/Kg wet0.10ND
Diisopropyl Ether (DIPE)mg/Kg wet0.025ND
1,4-Dioxane mg/Kg wet2.5ND
Ethanol mg/Kg wet0.20ND
Ethylbenzene mg/Kg wet0.050ND
Hexachlorobutadiene mg/Kg wet0.050ND
2-Hexanone (MBK)mg/Kg wet0.50ND
Isopropylbenzene (Cumene)mg/Kg wet0.050ND
p-Isopropyltoluene (p-Cymene)mg/Kg wet0.050ND
[TOC_1]QC Data[TOC]
Page 15 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B210357 - SW-846 5035/5030B
Blank (B210357-BLK1) Prepared & Analyzed: 08/15/18
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.050ND
Methylene Chloride mg/Kg wet0.25ND
4-Methyl-2-pentanone (MIBK)mg/Kg wet0.50ND
Naphthalene mg/Kg wet0.10ND
n-Propylbenzene mg/Kg wet0.050ND
Styrene mg/Kg wet0.050ND
1,1,1,2-Tetrachloroethane mg/Kg wet0.050ND
1,1,2,2-Tetrachloroethane mg/Kg wet0.025ND
Tetrachloroethylene mg/Kg wet0.050ND
Tetrahydrofuran mg/Kg wet0.50ND
Toluene mg/Kg wet0.050ND
1,2,3-Trichlorobenzene mg/Kg wet0.25ND
1,2,4-Trichlorobenzene mg/Kg wet0.050ND
1,3,5-Trichlorobenzene mg/Kg wet0.050ND
1,1,1-Trichloroethane mg/Kg wet0.050ND
1,1,2-Trichloroethane mg/Kg wet0.050ND
Trichloroethylene mg/Kg wet0.050ND
Trichlorofluoromethane (Freon 11)mg/Kg wet0.10ND
1,2,3-Trichloropropane mg/Kg wet0.10ND
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
mg/Kg wet0.050ND
1,2,4-Trimethylbenzene mg/Kg wet0.050ND
1,3,5-Trimethylbenzene mg/Kg wet0.050ND
Vinyl Chloride mg/Kg wet0.10ND
m+p Xylene mg/Kg wet0.10ND
o-Xylene mg/Kg wet0.050ND
mg/Kg wet 0.0250 70-130Surrogate: 1,2-Dichloroethane-d4 89.00.0222
mg/Kg wet 0.0250 70-130Surrogate: Toluene-d8 97.20.0243
mg/Kg wet 0.0250 70-130Surrogate: 4-Bromofluorobenzene 95.60.0239
LCS (B210357-BS1) Prepared & Analyzed: 08/15/18
Acetone mg/Kg wet0.057 0.113 70-16091.40.104
Acrylonitrile mg/Kg wet0.0057 0.0113 70-13086.70.00983
tert-Amyl Methyl Ether (TAME)mg/Kg wet0.00057 0.0113 70-13089.50.0101
Benzene mg/Kg wet0.0011 0.0113 70-13092.90.0105
Bromobenzene mg/Kg wet0.0011 0.0113 70-13098.20.0111
Bromochloromethane mg/Kg wet0.0011 0.0113 70-13095.80.0109
Bromodichloromethane mg/Kg wet0.0011 0.0113 70-13097.20.0110
Bromoform mg/Kg wet0.0023 0.0113 70-1301000.0113
Bromomethane mg/Kg wet0.0023 0.0113 40-13087.80.00995
2-Butanone (MEK)mg/Kg wet0.023 0.113 70-16077.10.0874
tert-Butyl Alcohol (TBA)mg/Kg wet0.023 0.113 40-13098.40.112
n-Butylbenzene mg/Kg wet0.0011 0.0113 70-1301030.0116
sec-Butylbenzene mg/Kg wet0.0011 0.0113 70-1301060.0120
tert-Butylbenzene mg/Kg wet0.0011 0.0113 70-1601030.0117
tert-Butyl Ethyl Ether (TBEE)mg/Kg wet0.00057 0.0113 70-13080.90.00917
Carbon Disulfide mg/Kg wet0.0034 0.0113 70-1301130.0128
Carbon Tetrachloride mg/Kg wet0.0011 0.0113 70-13091.60.0104
Chlorobenzene mg/Kg wet0.0011 0.0113 70-1301020.0115
Chlorodibromomethane mg/Kg wet0.00057 0.0113 70-1301030.0117
Chloroethane mg/Kg wet0.0023 0.0113 70-13093.90.0106
Chloroform mg/Kg wet0.0023 0.0113 70-13098.60.0112
Chloromethane mg/Kg wet0.0023 0.0113 70-13074.90.00849
Page 16 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B210357 - SW-846 5035/5030B
LCS (B210357-BS1) Prepared & Analyzed: 08/15/18
2-Chlorotoluene mg/Kg wet0.0011 0.0113 70-1301000.0113
4-Chlorotoluene mg/Kg wet0.0011 0.0113 70-13099.40.0113
1,2-Dibromo-3-chloropropane (DBCP)mg/Kg wet0.0057 0.0113 70-13097.90.0111
1,2-Dibromoethane (EDB)mg/Kg wet0.00057 0.0113 70-1301050.0119
Dibromomethane mg/Kg wet0.0011 0.0113 70-1301050.0119
1,2-Dichlorobenzene mg/Kg wet0.0011 0.0113 70-1301030.0117
1,3-Dichlorobenzene mg/Kg wet0.0011 0.0113 70-1301070.0121
1,4-Dichlorobenzene mg/Kg wet0.0011 0.0113 70-13098.60.0112
trans-1,4-Dichloro-2-butene mg/Kg wet0.0023 0.0113 70-13082.90.00940
Dichlorodifluoromethane (Freon 12)mg/Kg wet0.0023 0.0113 40-16084.00.00952
1,1-Dichloroethane mg/Kg wet0.0011 0.0113 70-13092.20.0104
1,2-Dichloroethane mg/Kg wet0.0011 0.0113 70-13088.20.0100
1,1-Dichloroethylene mg/Kg wet0.0011 0.0113 70-1301010.0115
cis-1,2-Dichloroethylene mg/Kg wet0.0011 0.0113 70-13087.30.00989
trans-1,2-Dichloroethylene mg/Kg wet0.0011 0.0113 70-13091.50.0104
1,2-Dichloropropane mg/Kg wet0.0011 0.0113 70-13095.90.0109
1,3-Dichloropropane mg/Kg wet0.00057 0.0113 70-13087.80.00995
2,2-Dichloropropane mg/Kg wet0.0011 0.0113 70-13083.40.00945
1,1-Dichloropropene mg/Kg wet0.0023 0.0113 70-13089.10.0101
cis-1,3-Dichloropropene mg/Kg wet0.00057 0.0113 70-13093.00.0105
trans-1,3-Dichloropropene mg/Kg wet0.00057 0.0113 70-13093.90.0106
Diethyl Ether mg/Kg wet0.0023 0.0113 70-13094.90.0108
Diisopropyl Ether (DIPE)mg/Kg wet0.00057 0.0113 70-13075.80.00859
1,4-Dioxane mg/Kg wet0.057 0.113 40-16098.00.111
Ethylbenzene mg/Kg wet0.0011 0.0113 70-1301040.0118
Hexachlorobutadiene mg/Kg wet0.0011 0.0113 70-1601120.0127
2-Hexanone (MBK)mg/Kg wet0.011 0.113 70-16083.10.0942
Isopropylbenzene (Cumene)mg/Kg wet0.0011 0.0113 70-1301100.0125
p-Isopropyltoluene (p-Cymene)mg/Kg wet0.0011 0.0113 70-1301050.0119
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.0011 0.0113 70-13096.20.0109
Methylene Chloride mg/Kg wet0.0057 0.0113 40-16090.20.0102
4-Methyl-2-pentanone (MIBK)mg/Kg wet0.011 0.113 70-16082.50.0935
Naphthalene mg/Kg wet0.0023 0.0113 40-1301040.0118
n-Propylbenzene mg/Kg wet0.0011 0.0113 70-1301030.0117
Styrene mg/Kg wet0.0011 0.0113 70-1301040.0118
1,1,1,2-Tetrachloroethane mg/Kg wet0.0011 0.0113 70-1301090.0124
1,1,2,2-Tetrachloroethane mg/Kg wet0.00057 0.0113 70-1301050.0119
Tetrachloroethylene mg/Kg wet0.0011 0.0113 70-1301050.0119
Tetrahydrofuran mg/Kg wet0.011 0.0113 J70-13078.90.00894
Toluene mg/Kg wet0.0011 0.0113 70-1301020.0116
1,2,3-Trichlorobenzene mg/Kg wet0.0057 0.0113 70-1301040.0118
1,2,4-Trichlorobenzene mg/Kg wet0.0011 0.0113 70-13099.60.0113
1,3,5-Trichlorobenzene mg/Kg wet0.0011 0.0113 70-13099.90.0113
1,1,1-Trichloroethane mg/Kg wet0.0011 0.0113 70-13098.40.0112
1,1,2-Trichloroethane mg/Kg wet0.0011 0.0113 70-1301040.0117
Trichloroethylene mg/Kg wet0.0011 0.0113 70-1301020.0116
Trichlorofluoromethane (Freon 11)mg/Kg wet0.0023 0.0113 70-13099.00.0112
1,2,3-Trichloropropane mg/Kg wet0.0023 0.0113 70-13075.90.00860
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
mg/Kg wet0.0011 0.0113 70-1301120.0127
1,2,4-Trimethylbenzene mg/Kg wet0.0011 0.0113 70-13098.60.0112
1,3,5-Trimethylbenzene mg/Kg wet0.0011 0.0113 70-13099.80.0113
Page 17 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B210357 - SW-846 5035/5030B
LCS (B210357-BS1) Prepared & Analyzed: 08/15/18
Vinyl Chloride mg/Kg wet0.0023 0.0113 40-13086.80.00984
m+p Xylene mg/Kg wet0.0023 0.0227 70-1301010.0230
o-Xylene mg/Kg wet0.0011 0.0113 70-1301020.0115
mg/Kg wet 0.0283 70-130Surrogate: 1,2-Dichloroethane-d4 89.00.0252
mg/Kg wet 0.0283 70-130Surrogate: Toluene-d8 99.70.0283
mg/Kg wet 0.0283 70-130Surrogate: 4-Bromofluorobenzene 96.90.0274
LCS Dup (B210357-BSD1) Prepared & Analyzed: 08/15/18
Acetone mg/Kg wet0.057 0.113 2570-16089.9 1.620.102
Acrylonitrile mg/Kg wet0.0057 0.0113 2570-13081.4 6.310.00923
tert-Amyl Methyl Ether (TAME)mg/Kg wet0.00057 0.0113 2570-13088.5 1.120.0100
Benzene mg/Kg wet0.0011 0.0113 2570-13092.3 0.6480.0105
Bromobenzene mg/Kg wet0.0011 0.0113 2570-13099.5 1.320.0113
Bromochloromethane mg/Kg wet0.0011 0.0113 2570-13095.3 0.5230.0108
Bromodichloromethane mg/Kg wet0.0011 0.0113 2570-13094.6 2.710.0107
Bromoform mg/Kg wet0.0023 0.0113 2570-130104 3.730.0118
Bromomethane mg/Kg wet0.0023 0.0113 2540-130104 16.70.0118
2-Butanone (MEK)mg/Kg wet0.023 0.113 2570-16074.6 3.340.0845
tert-Butyl Alcohol (TBA)mg/Kg wet0.023 0.113 2540-13090.3 8.640.102
n-Butylbenzene mg/Kg wet0.0011 0.0113 2570-130102 0.1950.0116
sec-Butylbenzene mg/Kg wet0.0011 0.0113 2570-130105 0.7610.0119
tert-Butylbenzene mg/Kg wet0.0011 0.0113 2570-160101 2.550.0114
tert-Butyl Ethyl Ether (TBEE)mg/Kg wet0.00057 0.0113 2570-13080.9 0.000.00917
Carbon Disulfide mg/Kg wet0.0034 0.0113 2570-130105 7.890.0119
Carbon Tetrachloride mg/Kg wet0.0011 0.0113 2570-13090.3 1.430.0102
Chlorobenzene mg/Kg wet0.0011 0.0113 2570-130103 0.9800.0116
Chlorodibromomethane mg/Kg wet0.00057 0.0113 2570-130103 0.1950.0116
Chloroethane mg/Kg wet0.0023 0.0113 2570-13091.6 2.480.0104
Chloroform mg/Kg wet0.0023 0.0113 2570-13098.2 0.4070.0111
Chloromethane mg/Kg wet0.0023 0.0113 2570-13073.8 1.480.00836
2-Chlorotoluene mg/Kg wet0.0011 0.0113 2570-13097.2 2.840.0110
4-Chlorotoluene mg/Kg wet0.0011 0.0113 2570-13097.4 2.030.0110
1,2-Dibromo-3-chloropropane (DBCP)mg/Kg wet0.0057 0.0113 2570-13087.0 11.80.00986
1,2-Dibromoethane (EDB)mg/Kg wet0.00057 0.0113 2570-130100 4.960.0114
Dibromomethane mg/Kg wet0.0011 0.0113 2570-130105 0.4750.0119
1,2-Dichlorobenzene mg/Kg wet0.0011 0.0113 2570-130102 1.070.0115
1,3-Dichlorobenzene mg/Kg wet0.0011 0.0113 2570-130107 0.09360.0121
1,4-Dichlorobenzene mg/Kg wet0.0011 0.0113 2570-13096.8 1.840.0110
trans-1,4-Dichloro-2-butene mg/Kg wet0.0023 0.0113 2570-13078.2 5.830.00886
Dichlorodifluoromethane (Freon 12)mg/Kg wet0.0023 0.0113 2540-16084.9 1.070.00962
1,1-Dichloroethane mg/Kg wet0.0011 0.0113 2570-13091.4 0.8710.0104
1,2-Dichloroethane mg/Kg wet0.0011 0.0113 2570-13088.9 0.7900.0101
1,1-Dichloroethylene mg/Kg wet0.0011 0.0113 2570-13098.0 3.210.0111
cis-1,2-Dichloroethylene mg/Kg wet0.0011 0.0113 2570-13085.4 2.200.00968
trans-1,2-Dichloroethylene mg/Kg wet0.0011 0.0113 2570-13090.1 1.540.0102
1,2-Dichloropropane mg/Kg wet0.0011 0.0113 2570-13094.2 1.790.0107
1,3-Dichloropropane mg/Kg wet0.00057 0.0113 2570-13089.6 2.030.0102
2,2-Dichloropropane mg/Kg wet0.0011 0.0113 2570-13081.7 2.060.00926
1,1-Dichloropropene mg/Kg wet0.0023 0.0113 2570-13090.2 1.230.0102
cis-1,3-Dichloropropene mg/Kg wet0.00057 0.0113 2570-13091.4 1.740.0104
trans-1,3-Dichloropropene mg/Kg wet0.00057 0.0113 2570-13093.4 0.5340.0106
Diethyl Ether mg/Kg wet0.0023 0.0113 2570-13093.5 1.490.0106
Page 18 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B210357 - SW-846 5035/5030B
LCS Dup (B210357-BSD1) Prepared & Analyzed: 08/15/18
Diisopropyl Ether (DIPE)mg/Kg wet0.00057 0.0113 2570-13075.3 0.6620.00853
1,4-Dioxane mg/Kg wet0.057 0.113 5040-16093.2 5.040.106
Ethylbenzene mg/Kg wet0.0011 0.0113 2570-130106 1.810.0120
Hexachlorobutadiene mg/Kg wet0.0011 0.0113 2570-160109 2.630.0123
2-Hexanone (MBK)mg/Kg wet0.011 0.113 2570-16079.4 4.620.0900
Isopropylbenzene (Cumene)mg/Kg wet0.0011 0.0113 2570-130110 0.2720.0125
p-Isopropyltoluene (p-Cymene)mg/Kg wet0.0011 0.0113 2570-130104 1.150.0117
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.0011 0.0113 2570-13094.7 1.570.0107
Methylene Chloride mg/Kg wet0.0057 0.0113 2540-16089.7 0.5560.0102
4-Methyl-2-pentanone (MIBK)mg/Kg wet0.011 0.113 2570-16080.5 2.450.0913
Naphthalene mg/Kg wet0.0023 0.0113 2540-130102 1.840.0116
n-Propylbenzene mg/Kg wet0.0011 0.0113 2570-130101 1.960.0114
Styrene mg/Kg wet0.0011 0.0113 2570-130106 1.530.0120
1,1,1,2-Tetrachloroethane mg/Kg wet0.0011 0.0113 2570-130103 6.040.0117
1,1,2,2-Tetrachloroethane mg/Kg wet0.00057 0.0113 2570-130104 0.6680.0118
Tetrachloroethylene mg/Kg wet0.0011 0.0113 2570-130107 1.510.0121
Tetrahydrofuran mg/Kg wet0.011 0.0113 25 J70-13072.4 8.590.00821
Toluene mg/Kg wet0.0011 0.0113 2570-130101 1.380.0114
1,2,3-Trichlorobenzene mg/Kg wet0.0057 0.0113 2570-130104 0.09600.0118
1,2,4-Trichlorobenzene mg/Kg wet0.0011 0.0113 2570-130101 1.490.0115
1,3,5-Trichlorobenzene mg/Kg wet0.0011 0.0113 2570-13097.2 2.740.0110
1,1,1-Trichloroethane mg/Kg wet0.0011 0.0113 2570-13097.5 0.9190.0110
1,1,2-Trichloroethane mg/Kg wet0.0011 0.0113 2570-130105 1.250.0119
Trichloroethylene mg/Kg wet0.0011 0.0113 2570-13099.9 2.180.0113
Trichlorofluoromethane (Freon 11)mg/Kg wet0.0023 0.0113 2570-13096.4 2.660.0109
1,2,3-Trichloropropane mg/Kg wet0.0023 0.0113 2570-13077.8 2.470.00882
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
mg/Kg wet0.0011 0.0113 2570-130107 4.830.0121
1,2,4-Trimethylbenzene mg/Kg wet0.0011 0.0113 2570-13096.7 1.950.0110
1,3,5-Trimethylbenzene mg/Kg wet0.0011 0.0113 2570-13098.7 1.110.0112
Vinyl Chloride mg/Kg wet0.0023 0.0113 2540-13085.9 1.040.00974
m+p Xylene mg/Kg wet0.0023 0.0227 2570-130102 0.2460.0231
o-Xylene mg/Kg wet0.0011 0.0113 2570-130102 0.1960.0116
mg/Kg wet 0.0283 70-130Surrogate: 1,2-Dichloroethane-d4 88.90.0252
mg/Kg wet 0.0283 70-130Surrogate: Toluene-d8 98.80.0280
mg/Kg wet 0.0283 70-130Surrogate: 4-Bromofluorobenzene 96.50.0273
Page 19 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Semivolatile Organic Compounds by GC/MS[TOC]
Batch B210345 - SW-846 3546
[TOC_3]B210345[TOC]
Blank (B210345-BLK1) Prepared & Analyzed: 08/15/18
Acenaphthene mg/Kg wet0.17ND
Acenaphthylene mg/Kg wet0.17ND
Acetophenone mg/Kg wet0.34ND
Aniline mg/Kg wet0.34 V-34ND
Anthracene mg/Kg wet0.17ND
Benzidine mg/Kg wet0.66 V-04, V-20ND
Benzo(a)anthracene mg/Kg wet0.17ND
Benzo(a)pyrene mg/Kg wet0.17ND
Benzo(b)fluoranthene mg/Kg wet0.17ND
Benzo(g,h,i)perylene mg/Kg wet0.17ND
Benzo(k)fluoranthene mg/Kg wet0.17ND
Benzoic Acid mg/Kg wet1.0ND
Bis(2-chloroethoxy)methane mg/Kg wet0.34ND
Bis(2-chloroethyl)ether mg/Kg wet0.34ND
Bis(2-chloroisopropyl)ether mg/Kg wet0.34ND
Bis(2-Ethylhexyl)phthalate mg/Kg wet0.34ND
4-Bromophenylphenylether mg/Kg wet0.34ND
Butylbenzylphthalate mg/Kg wet0.34ND
Carbazole mg/Kg wet0.17ND
4-Chloroaniline mg/Kg wet0.66 V-34ND
4-Chloro-3-methylphenol mg/Kg wet0.66ND
2-Chloronaphthalene mg/Kg wet0.34ND
2-Chlorophenol mg/Kg wet0.34ND
4-Chlorophenylphenylether mg/Kg wet0.34ND
Chrysene mg/Kg wet0.17ND
Dibenz(a,h)anthracene mg/Kg wet0.17ND
Dibenzofuran mg/Kg wet0.34ND
Di-n-butylphthalate mg/Kg wet0.34ND
1,2-Dichlorobenzene mg/Kg wet0.34ND
1,3-Dichlorobenzene mg/Kg wet0.34ND
1,4-Dichlorobenzene mg/Kg wet0.34ND
3,3-Dichlorobenzidine mg/Kg wet0.17 V-34ND
2,4-Dichlorophenol mg/Kg wet0.34ND
Diethylphthalate mg/Kg wet0.34ND
2,4-Dimethylphenol mg/Kg wet0.34ND
Dimethylphthalate mg/Kg wet0.34ND
4,6-Dinitro-2-methylphenol mg/Kg wet0.34ND
2,4-Dinitrophenol mg/Kg wet0.66ND
2,4-Dinitrotoluene mg/Kg wet0.34ND
2,6-Dinitrotoluene mg/Kg wet0.34ND
Di-n-octylphthalate mg/Kg wet0.34ND
1,2-Diphenylhydrazine (as Azobenzene)mg/Kg wet0.34ND
Fluoranthene mg/Kg wet0.17ND
Fluorene mg/Kg wet0.17ND
Hexachlorobenzene mg/Kg wet0.34ND
Hexachlorobutadiene mg/Kg wet0.34ND
Hexachlorocyclopentadiene mg/Kg wet0.34 V-05ND
Hexachloroethane mg/Kg wet0.34ND
Indeno(1,2,3-cd)pyrene mg/Kg wet0.17ND
Isophorone mg/Kg wet0.34ND
1-Methylnaphthalene mg/Kg wet0.17ND
2-Methylnaphthalene mg/Kg wet0.17ND
Page 20 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B210345 - SW-846 3546
Blank (B210345-BLK1) Prepared & Analyzed: 08/15/18
2-Methylphenol mg/Kg wet0.34ND
3/4-Methylphenol mg/Kg wet0.34ND
Naphthalene mg/Kg wet0.17ND
2-Nitroaniline mg/Kg wet0.34ND
3-Nitroaniline mg/Kg wet0.34 V-34ND
4-Nitroaniline mg/Kg wet0.34ND
Nitrobenzene mg/Kg wet0.34ND
2-Nitrophenol mg/Kg wet0.34ND
4-Nitrophenol mg/Kg wet0.66ND
N-Nitrosodimethylamine mg/Kg wet0.34ND
N-Nitrosodiphenylamine mg/Kg wet0.34ND
N-Nitrosodi-n-propylamine mg/Kg wet0.34ND
Pentachloronitrobenzene mg/Kg wet0.34ND
Pentachlorophenol mg/Kg wet0.34ND
Phenanthrene mg/Kg wet0.17ND
Phenol mg/Kg wet0.34ND
Pyrene mg/Kg wet0.17ND
Pyridine mg/Kg wet0.34ND
1,2,4,5-Tetrachlorobenzene mg/Kg wet0.34ND
1,2,4-Trichlorobenzene mg/Kg wet0.34ND
2,4,5-Trichlorophenol mg/Kg wet0.34ND
2,4,6-Trichlorophenol mg/Kg wet0.34ND
mg/Kg wet 6.67 30-130Surrogate: 2-Fluorophenol 79.25.28
mg/Kg wet 6.67 30-130Surrogate: Phenol-d6 80.25.35
mg/Kg wet 3.33 30-130Surrogate: Nitrobenzene-d5 73.22.44
mg/Kg wet 3.33 30-130Surrogate: 2-Fluorobiphenyl 85.02.83
mg/Kg wet 6.67 30-130Surrogate: 2,4,6-Tribromophenol 76.15.08
mg/Kg wet 3.33 30-130Surrogate: p-Terphenyl-d14 1033.44
LCS (B210345-BS1) Prepared & Analyzed: 08/15/18
Acenaphthene mg/Kg wet0.17 1.67 40-14073.01.22
Acenaphthylene mg/Kg wet0.17 1.67 40-14073.11.22
Acetophenone mg/Kg wet0.34 1.67 40-14073.11.22
Aniline mg/Kg wet0.34 1.67 V-3410-14071.71.19
Anthracene mg/Kg wet0.17 1.67 40-14083.01.38
Benzidine mg/Kg wet0.66 1.67 V-04, V-0640-1401382.29
Benzo(a)anthracene mg/Kg wet0.17 1.67 40-14078.41.31
Benzo(a)pyrene mg/Kg wet0.17 1.67 40-14081.11.35
Benzo(b)fluoranthene mg/Kg wet0.17 1.67 40-14070.61.18
Benzo(g,h,i)perylene mg/Kg wet0.17 1.67 40-14077.21.29
Benzo(k)fluoranthene mg/Kg wet0.17 1.67 40-14076.41.27
Benzoic Acid mg/Kg wet1.0 1.67 30-13073.21.22
Bis(2-chloroethoxy)methane mg/Kg wet0.34 1.67 40-14077.51.29
Bis(2-chloroethyl)ether mg/Kg wet0.34 1.67 40-14070.41.17
Bis(2-chloroisopropyl)ether mg/Kg wet0.34 1.67 40-14087.51.46
Bis(2-Ethylhexyl)phthalate mg/Kg wet0.34 1.67 40-14090.21.50
4-Bromophenylphenylether mg/Kg wet0.34 1.67 40-14074.11.24
Butylbenzylphthalate mg/Kg wet0.34 1.67 40-14087.61.46
Carbazole mg/Kg wet0.17 1.67 40-14077.31.29
4-Chloroaniline mg/Kg wet0.66 1.67 V-3410-14060.01.00
4-Chloro-3-methylphenol mg/Kg wet0.66 1.67 30-13081.11.35
2-Chloronaphthalene mg/Kg wet0.34 1.67 40-14063.51.06
Page 21 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B210345 - SW-846 3546
LCS (B210345-BS1) Prepared & Analyzed: 08/15/18
2-Chlorophenol mg/Kg wet0.34 1.67 30-13075.11.25
4-Chlorophenylphenylether mg/Kg wet0.34 1.67 40-14070.91.18
Chrysene mg/Kg wet0.17 1.67 40-14078.91.31
Dibenz(a,h)anthracene mg/Kg wet0.17 1.67 40-14077.41.29
Dibenzofuran mg/Kg wet0.34 1.67 40-14074.31.24
Di-n-butylphthalate mg/Kg wet0.34 1.67 40-14082.21.37
1,2-Dichlorobenzene mg/Kg wet0.34 1.67 40-14070.81.18
1,3-Dichlorobenzene mg/Kg wet0.34 1.67 40-14066.91.12
1,4-Dichlorobenzene mg/Kg wet0.34 1.67 40-14067.21.12
3,3-Dichlorobenzidine mg/Kg wet0.17 1.67 V-3420-14069.81.16
2,4-Dichlorophenol mg/Kg wet0.34 1.67 30-13076.01.27
Diethylphthalate mg/Kg wet0.34 1.67 40-14070.51.18
2,4-Dimethylphenol mg/Kg wet0.34 1.67 30-13085.31.42
Dimethylphthalate mg/Kg wet0.34 1.67 40-14072.41.21
4,6-Dinitro-2-methylphenol mg/Kg wet0.34 1.67 30-13074.01.23
2,4-Dinitrophenol mg/Kg wet0.66 1.67 30-13056.80.947
2,4-Dinitrotoluene mg/Kg wet0.34 1.67 40-14074.01.23
2,6-Dinitrotoluene mg/Kg wet0.34 1.67 40-14080.51.34
Di-n-octylphthalate mg/Kg wet0.34 1.67 40-14090.21.50
1,2-Diphenylhydrazine (as Azobenzene)mg/Kg wet0.34 1.67 40-14080.41.34
Fluoranthene mg/Kg wet0.17 1.67 40-14076.91.28
Fluorene mg/Kg wet0.17 1.67 40-14072.31.20
Hexachlorobenzene mg/Kg wet0.34 1.67 40-14071.81.20
Hexachlorobutadiene mg/Kg wet0.34 1.67 40-14069.51.16
Hexachlorocyclopentadiene mg/Kg wet0.34 1.67 L-07, V-0540-14038.4 *0.640
Hexachloroethane mg/Kg wet0.34 1.67 40-14067.01.12
Indeno(1,2,3-cd)pyrene mg/Kg wet0.17 1.67 40-14073.31.22
Isophorone mg/Kg wet0.34 1.67 40-14077.81.30
1-Methylnaphthalene mg/Kg wet0.17 1.67 40-14081.71.36
2-Methylnaphthalene mg/Kg wet0.17 1.67 40-14082.41.37
2-Methylphenol mg/Kg wet0.34 1.67 30-13071.01.18
3/4-Methylphenol mg/Kg wet0.34 1.67 30-13084.81.41
Naphthalene mg/Kg wet0.17 1.67 40-14074.11.23
2-Nitroaniline mg/Kg wet0.34 1.67 40-14070.71.18
3-Nitroaniline mg/Kg wet0.34 1.67 V-3430-14071.11.19
4-Nitroaniline mg/Kg wet0.34 1.67 40-14074.71.24
Nitrobenzene mg/Kg wet0.34 1.67 40-14069.21.15
2-Nitrophenol mg/Kg wet0.34 1.67 30-13080.01.33
4-Nitrophenol mg/Kg wet0.66 1.67 30-13076.11.27
N-Nitrosodimethylamine mg/Kg wet0.34 1.67 40-14064.71.08
N-Nitrosodiphenylamine mg/Kg wet0.34 1.67 40-14098.31.64
N-Nitrosodi-n-propylamine mg/Kg wet0.34 1.67 40-14069.01.15
Pentachloronitrobenzene mg/Kg wet0.34 1.67 40-14072.21.20
Pentachlorophenol mg/Kg wet0.34 1.67 30-13061.81.03
Phenanthrene mg/Kg wet0.17 1.67 40-14081.51.36
Phenol mg/Kg wet0.34 1.67 30-13075.21.25
Pyrene mg/Kg wet0.17 1.67 40-14082.81.38
Pyridine mg/Kg wet0.34 1.67 30-14045.40.757
1,2,4,5-Tetrachlorobenzene mg/Kg wet0.34 1.67 40-14066.11.10
1,2,4-Trichlorobenzene mg/Kg wet0.34 1.67 40-14072.51.21
2,4,5-Trichlorophenol mg/Kg wet0.34 1.67 30-13073.71.23
2,4,6-Trichlorophenol mg/Kg wet0.34 1.67 30-13073.81.23
Page 22 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B210345 - SW-846 3546
LCS (B210345-BS1) Prepared & Analyzed: 08/15/18
mg/Kg wet 6.67 30-130Surrogate: 2-Fluorophenol 77.85.19
mg/Kg wet 6.67 30-130Surrogate: Phenol-d6 82.55.50
mg/Kg wet 3.33 30-130Surrogate: Nitrobenzene-d5 75.12.50
mg/Kg wet 3.33 30-130Surrogate: 2-Fluorobiphenyl 85.72.86
mg/Kg wet 6.67 30-130Surrogate: 2,4,6-Tribromophenol 70.14.67
mg/Kg wet 3.33 30-130Surrogate: p-Terphenyl-d14 97.23.24
LCS Dup (B210345-BSD1) Prepared & Analyzed: 08/15/18
Acenaphthene mg/Kg wet0.17 1.67 3040-14071.4 2.221.19
Acenaphthylene mg/Kg wet0.17 1.67 3040-14072.5 0.7421.21
Acetophenone mg/Kg wet0.34 1.67 3040-14070.9 3.141.18
Aniline mg/Kg wet0.34 1.67 50 V-3410-14057.8 21.40.963
Anthracene mg/Kg wet0.17 1.67 3040-14081.5 1.871.36
Benzidine mg/Kg wet0.66 1.67 30 V-04, V-0640-140114 18.31.91
Benzo(a)anthracene mg/Kg wet0.17 1.67 3040-14077.7 0.9481.30
Benzo(a)pyrene mg/Kg wet0.17 1.67 3040-14080.8 0.4691.35
Benzo(b)fluoranthene mg/Kg wet0.17 1.67 3040-14070.9 0.5371.18
Benzo(g,h,i)perylene mg/Kg wet0.17 1.67 3040-14074.8 3.181.25
Benzo(k)fluoranthene mg/Kg wet0.17 1.67 3040-14077.2 1.121.29
Benzoic Acid mg/Kg wet1.0 1.67 5030-13069.9 4.671.16
Bis(2-chloroethoxy)methane mg/Kg wet0.34 1.67 3040-14073.5 5.251.22
Bis(2-chloroethyl)ether mg/Kg wet0.34 1.67 3040-14065.9 6.611.10
Bis(2-chloroisopropyl)ether mg/Kg wet0.34 1.67 3040-14078.9 10.41.31
Bis(2-Ethylhexyl)phthalate mg/Kg wet0.34 1.67 3040-14085.9 4.881.43
4-Bromophenylphenylether mg/Kg wet0.34 1.67 3040-14074.3 0.2701.24
Butylbenzylphthalate mg/Kg wet0.34 1.67 3040-14084.0 4.291.40
Carbazole mg/Kg wet0.17 1.67 3040-14076.2 1.431.27
4-Chloroaniline mg/Kg wet0.66 1.67 30 V-3410-14045.7 27.10.761
4-Chloro-3-methylphenol mg/Kg wet0.66 1.67 3030-13076.6 5.711.28
2-Chloronaphthalene mg/Kg wet0.34 1.67 3040-14064.0 0.7531.07
2-Chlorophenol mg/Kg wet0.34 1.67 3030-13075.1 0.05321.25
4-Chlorophenylphenylether mg/Kg wet0.34 1.67 3040-14071.3 0.5341.19
Chrysene mg/Kg wet0.17 1.67 3040-14077.8 1.331.30
Dibenz(a,h)anthracene mg/Kg wet0.17 1.67 3040-14075.6 2.381.26
Dibenzofuran mg/Kg wet0.34 1.67 3040-14074.1 0.2431.23
Di-n-butylphthalate mg/Kg wet0.34 1.67 3040-14078.9 4.201.31
1,2-Dichlorobenzene mg/Kg wet0.34 1.67 3040-14071.9 1.631.20
1,3-Dichlorobenzene mg/Kg wet0.34 1.67 3040-14068.9 2.971.15
1,4-Dichlorobenzene mg/Kg wet0.34 1.67 3040-14069.2 2.991.15
3,3-Dichlorobenzidine mg/Kg wet0.17 1.67 50 V-3420-14057.8 18.70.964
2,4-Dichlorophenol mg/Kg wet0.34 1.67 3030-13074.8 1.541.25
Diethylphthalate mg/Kg wet0.34 1.67 3040-14068.6 2.791.14
2,4-Dimethylphenol mg/Kg wet0.34 1.67 3030-13084.4 1.061.41
Dimethylphthalate mg/Kg wet0.34 1.67 3040-14071.0 1.981.18
4,6-Dinitro-2-methylphenol mg/Kg wet0.34 1.67 3030-13072.0 2.661.20
2,4-Dinitrophenol mg/Kg wet0.66 1.67 3030-13056.2 1.030.937
2,4-Dinitrotoluene mg/Kg wet0.34 1.67 3040-14073.5 0.6241.22
2,6-Dinitrotoluene mg/Kg wet0.34 1.67 3040-14079.0 1.911.32
Di-n-octylphthalate mg/Kg wet0.34 1.67 3040-14086.8 3.801.45
1,2-Diphenylhydrazine (as Azobenzene)mg/Kg wet0.34 1.67 3040-14071.2 12.11.19
Fluoranthene mg/Kg wet0.17 1.67 3040-14076.4 0.6791.27
Fluorene mg/Kg wet0.17 1.67 3040-14071.1 1.651.18
Page 23 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B210345 - SW-846 3546
LCS Dup (B210345-BSD1) Prepared & Analyzed: 08/15/18
Hexachlorobenzene mg/Kg wet0.34 1.67 3040-14071.6 0.3351.19
Hexachlorobutadiene mg/Kg wet0.34 1.67 3040-14073.4 5.541.22
Hexachlorocyclopentadiene mg/Kg wet0.34 1.67 30 V-0540-14040.7 5.910.679
Hexachloroethane mg/Kg wet0.34 1.67 3040-14065.7 1.931.09
Indeno(1,2,3-cd)pyrene mg/Kg wet0.17 1.67 3040-14077.0 4.871.28
Isophorone mg/Kg wet0.34 1.67 3040-14073.4 5.871.22
1-Methylnaphthalene mg/Kg wet0.17 1.67 3040-14080.9 0.9351.35
2-Methylnaphthalene mg/Kg wet0.17 1.67 3040-14081.8 0.6821.36
2-Methylphenol mg/Kg wet0.34 1.67 3030-13067.5 5.031.12
3/4-Methylphenol mg/Kg wet0.34 1.67 3030-13080.6 5.151.34
Naphthalene mg/Kg wet0.17 1.67 3040-14075.5 1.901.26
2-Nitroaniline mg/Kg wet0.34 1.67 3040-14065.7 7.361.10
3-Nitroaniline mg/Kg wet0.34 1.67 30 V-3430-14063.8 10.81.06
4-Nitroaniline mg/Kg wet0.34 1.67 3040-14075.0 0.3471.25
Nitrobenzene mg/Kg wet0.34 1.67 3040-14066.5 4.011.11
2-Nitrophenol mg/Kg wet0.34 1.67 3030-13081.3 1.611.35
4-Nitrophenol mg/Kg wet0.66 1.67 5030-13072.3 5.121.21
N-Nitrosodimethylamine mg/Kg wet0.34 1.67 3040-14060.7 6.281.01
N-Nitrosodiphenylamine mg/Kg wet0.34 1.67 3040-14095.3 3.121.59
N-Nitrosodi-n-propylamine mg/Kg wet0.34 1.67 3040-14063.1 8.871.05
Pentachloronitrobenzene mg/Kg wet0.34 1.67 3040-14074.4 3.061.24
Pentachlorophenol mg/Kg wet0.34 1.67 3030-13061.3 0.8771.02
Phenanthrene mg/Kg wet0.17 1.67 3040-14079.5 2.461.32
Phenol mg/Kg wet0.34 1.67 3030-13072.0 4.371.20
Pyrene mg/Kg wet0.17 1.67 3040-14082.1 0.9221.37
Pyridine mg/Kg wet0.34 1.67 3030-14044.3 2.500.738
1,2,4,5-Tetrachlorobenzene mg/Kg wet0.34 1.67 3040-14067.4 1.981.12
1,2,4-Trichlorobenzene mg/Kg wet0.34 1.67 3040-14075.1 3.551.25
2,4,5-Trichlorophenol mg/Kg wet0.34 1.67 3030-13073.4 0.3811.22
2,4,6-Trichlorophenol mg/Kg wet0.34 1.67 3030-13075.4 2.091.26
mg/Kg wet 6.67 30-130Surrogate: 2-Fluorophenol 75.95.06
mg/Kg wet 6.67 30-130Surrogate: Phenol-d6 77.95.19
mg/Kg wet 3.33 30-130Surrogate: Nitrobenzene-d5 71.42.38
mg/Kg wet 3.33 30-130Surrogate: 2-Fluorobiphenyl 84.72.82
mg/Kg wet 6.67 30-130Surrogate: 2,4,6-Tribromophenol 70.64.70
mg/Kg wet 3.33 30-130Surrogate: p-Terphenyl-d14 95.73.19
Page 24 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - EPH - Quality Control
QUALITY CONTROL
[TOC_2]Petroleum Hydrocarbons Analyses - EPH[TOC]
Batch B210344 - SW-846 3546
[TOC_3]B210344[TOC]
Blank (B210344-BLK1) Prepared: 08/15/18 Analyzed: 08/16/18
C9-C18 Aliphatics mg/Kg wet10ND
C19-C36 Aliphatics mg/Kg wet10ND
Unadjusted C11-C22 Aromatics mg/Kg wet10ND
C11-C22 Aromatics mg/Kg wet10ND
Acenaphthene mg/Kg wet0.10ND
Acenaphthylene mg/Kg wet0.10ND
Anthracene mg/Kg wet0.10ND
Benzo(a)anthracene mg/Kg wet0.10ND
Benzo(a)pyrene mg/Kg wet0.10ND
Benzo(b)fluoranthene mg/Kg wet0.10ND
Benzo(g,h,i)perylene mg/Kg wet0.10ND
Benzo(k)fluoranthene mg/Kg wet0.10ND
Chrysene mg/Kg wet0.10ND
Dibenz(a,h)anthracene mg/Kg wet0.10ND
Fluoranthene mg/Kg wet0.10ND
Fluorene mg/Kg wet0.10ND
Indeno(1,2,3-cd)pyrene mg/Kg wet0.10ND
2-Methylnaphthalene mg/Kg wet0.10ND
Naphthalene mg/Kg wet0.10ND
Phenanthrene mg/Kg wet0.10ND
Pyrene mg/Kg wet0.10ND
n-Decane mg/Kg wet0.10ND
n-Docosane mg/Kg wet0.10ND
n-Dodecane mg/Kg wet0.10ND
n-Eicosane mg/Kg wet0.10ND
n-Hexacosane mg/Kg wet0.10ND
n-Hexadecane mg/Kg wet0.10ND
n-Hexatriacontane mg/Kg wet0.10ND
n-Nonadecane mg/Kg wet0.10ND
n-Nonane mg/Kg wet0.10ND
n-Octacosane mg/Kg wet0.10ND
n-Octadecane mg/Kg wet0.10ND
n-Tetracosane mg/Kg wet0.10ND
n-Tetradecane mg/Kg wet0.10ND
n-Triacontane mg/Kg wet0.10ND
Naphthalene-aliphatic fraction mg/Kg wet0.10ND
2-Methylnaphthalene-aliphatic fraction mg/Kg wet0.10ND
mg/Kg wet 5.00 40-140Surrogate: Chlorooctadecane (COD)82.04.10
mg/Kg wet 5.00 40-140Surrogate: o-Terphenyl (OTP)79.23.96
mg/Kg wet 5.00 40-140Surrogate: 2-Bromonaphthalene 93.74.68
mg/Kg wet 5.00 40-140Surrogate: 2-Fluorobiphenyl 87.34.37
LCS (B210344-BS1) Prepared: 08/15/18 Analyzed: 08/16/18
C9-C18 Aliphatics mg/Kg wet10 30.0 40-14080.924.3
C19-C36 Aliphatics mg/Kg wet10 40.0 40-14093.637.5
Acenaphthene mg/Kg wet0.10 5.00 40-14074.53.72
Acenaphthylene mg/Kg wet0.10 5.00 40-14070.33.51
Anthracene mg/Kg wet0.10 5.00 40-14082.94.14
Benzo(a)anthracene mg/Kg wet0.10 5.00 40-14084.14.20
Benzo(a)pyrene mg/Kg wet0.10 5.00 40-14082.64.13
Benzo(b)fluoranthene mg/Kg wet0.10 5.00 40-14083.84.19
Benzo(g,h,i)perylene mg/Kg wet0.10 5.00 40-14082.74.14
Page 25 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - EPH - Quality Control
QUALITY CONTROL
Batch B210344 - SW-846 3546
LCS (B210344-BS1) Prepared: 08/15/18 Analyzed: 08/16/18
Benzo(k)fluoranthene mg/Kg wet0.10 5.00 40-14083.14.15
Chrysene mg/Kg wet0.10 5.00 40-14083.94.19
Dibenz(a,h)anthracene mg/Kg wet0.10 5.00 40-14085.44.27
Fluoranthene mg/Kg wet0.10 5.00 40-14083.64.18
Fluorene mg/Kg wet0.10 5.00 40-14078.73.93
Indeno(1,2,3-cd)pyrene mg/Kg wet0.10 5.00 40-14079.13.96
2-Methylnaphthalene mg/Kg wet0.10 5.00 40-14070.13.51
Naphthalene mg/Kg wet0.10 5.00 40-14063.83.19
Phenanthrene mg/Kg wet0.10 5.00 40-14084.24.21
Pyrene mg/Kg wet0.10 5.00 40-14085.64.28
n-Decane mg/Kg wet0.10 5.00 40-14051.92.60
n-Docosane mg/Kg wet0.10 5.00 40-14090.64.53
n-Dodecane mg/Kg wet0.10 5.00 40-14067.83.39
n-Eicosane mg/Kg wet0.10 5.00 40-14094.64.73
n-Hexacosane mg/Kg wet0.10 5.00 40-14086.54.33
n-Hexadecane mg/Kg wet0.10 5.00 40-14091.54.58
n-Hexatriacontane mg/Kg wet0.10 5.00 40-14080.34.01
n-Nonadecane mg/Kg wet0.10 5.00 40-14092.54.62
n-Nonane mg/Kg wet0.10 5.00 30-14034.71.74
n-Octacosane mg/Kg wet0.10 5.00 40-14082.34.11
n-Octadecane mg/Kg wet0.10 5.00 40-14094.74.74
n-Tetracosane mg/Kg wet0.10 5.00 40-14089.14.45
n-Tetradecane mg/Kg wet0.10 5.00 40-14082.84.14
n-Triacontane mg/Kg wet0.10 5.00 40-14081.64.08
Naphthalene-aliphatic fraction mg/Kg wet0.10 5.00 0-5ND
2-Methylnaphthalene-aliphatic fraction mg/Kg wet0.10 5.00 0-5ND
mg/Kg wet 5.00 40-140Surrogate: Chlorooctadecane (COD)88.34.42
mg/Kg wet 5.00 40-140Surrogate: o-Terphenyl (OTP)86.84.34
mg/Kg wet 5.00 40-140Surrogate: 2-Bromonaphthalene 85.44.27
mg/Kg wet 5.00 40-140Surrogate: 2-Fluorobiphenyl 87.24.36
LCS Dup (B210344-BSD1) Prepared: 08/15/18 Analyzed: 08/16/18
C9-C18 Aliphatics mg/Kg wet10 30.0 2540-14085.8 5.9125.7
C19-C36 Aliphatics mg/Kg wet10 40.0 2540-14095.0 1.4238.0
Acenaphthene mg/Kg wet0.10 5.00 2540-14077.6 4.133.88
Acenaphthylene mg/Kg wet0.10 5.00 2540-14073.3 4.293.67
Anthracene mg/Kg wet0.10 5.00 2540-14085.6 3.264.28
Benzo(a)anthracene mg/Kg wet0.10 5.00 2540-14086.7 3.124.34
Benzo(a)pyrene mg/Kg wet0.10 5.00 2540-14085.5 3.524.28
Benzo(b)fluoranthene mg/Kg wet0.10 5.00 2540-14087.0 3.734.35
Benzo(g,h,i)perylene mg/Kg wet0.10 5.00 2540-14086.8 4.844.34
Benzo(k)fluoranthene mg/Kg wet0.10 5.00 2540-14085.7 3.114.28
Chrysene mg/Kg wet0.10 5.00 2540-14086.4 2.954.32
Dibenz(a,h)anthracene mg/Kg wet0.10 5.00 2540-14089.9 5.174.50
Fluoranthene mg/Kg wet0.10 5.00 2540-14086.4 3.284.32
Fluorene mg/Kg wet0.10 5.00 2540-14081.7 3.784.09
Indeno(1,2,3-cd)pyrene mg/Kg wet0.10 5.00 2540-14082.2 3.794.11
2-Methylnaphthalene mg/Kg wet0.10 5.00 2540-14072.8 3.803.64
Naphthalene mg/Kg wet0.10 5.00 2540-14066.7 4.513.34
Phenanthrene mg/Kg wet0.10 5.00 2540-14087.2 3.404.36
Pyrene mg/Kg wet0.10 5.00 2540-14088.4 3.184.42
n-Decane mg/Kg wet0.10 5.00 2540-14055.8 7.222.79
Page 26 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - EPH - Quality Control
QUALITY CONTROL
Batch B210344 - SW-846 3546
LCS Dup (B210344-BSD1) Prepared: 08/15/18 Analyzed: 08/16/18
n-Docosane mg/Kg wet0.10 5.00 2540-14091.8 1.334.59
n-Dodecane mg/Kg wet0.10 5.00 2540-14071.7 5.593.58
n-Eicosane mg/Kg wet0.10 5.00 2540-14094.0 0.5984.70
n-Hexacosane mg/Kg wet0.10 5.00 2540-14088.2 1.874.41
n-Hexadecane mg/Kg wet0.10 5.00 2540-14093.8 2.524.69
n-Hexatriacontane mg/Kg wet0.10 5.00 2540-14082.3 2.514.12
n-Nonadecane mg/Kg wet0.10 5.00 2540-14093.8 1.424.69
n-Nonane mg/Kg wet0.10 5.00 2530-14037.6 8.001.88
n-Octacosane mg/Kg wet0.10 5.00 2540-14084.0 2.034.20
n-Octadecane mg/Kg wet0.10 5.00 2540-14096.5 1.914.83
n-Tetracosane mg/Kg wet0.10 5.00 2540-14090.5 1.614.53
n-Tetradecane mg/Kg wet0.10 5.00 2540-14085.8 3.574.29
n-Triacontane mg/Kg wet0.10 5.00 2540-14083.5 2.354.17
Naphthalene-aliphatic fraction mg/Kg wet0.10 5.00 0-5ND
2-Methylnaphthalene-aliphatic fraction mg/Kg wet0.10 5.00 0-5ND
mg/Kg wet 5.00 40-140Surrogate: Chlorooctadecane (COD)88.54.42
mg/Kg wet 5.00 40-140Surrogate: o-Terphenyl (OTP)88.24.41
mg/Kg wet 5.00 40-140Surrogate: 2-Bromonaphthalene 84.04.20
mg/Kg wet 5.00 40-140Surrogate: 2-Fluorobiphenyl 87.94.40
Page 27 of 39
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - VPH - Quality Control
QUALITY CONTROL
[TOC_2]Petroleum Hydrocarbons Analyses - VPH[TOC]
Batch B209997 - MA VPH
[TOC_3]B209997[TOC]
Blank (B209997-BLK1) Prepared: 08/10/18 Analyzed: 08/14/18
Unadjusted C5-C8 Aliphatics mg/Kg wet10ND
C5-C8 Aliphatics mg/Kg wet10ND
Unadjusted C9-C12 Aliphatics mg/Kg wet10ND
C9-C12 Aliphatics mg/Kg wet10ND
C9-C10 Aromatics mg/Kg wet10ND
Benzene mg/Kg wet0.050ND
Butylcyclohexane mg/Kg wet0.050ND
Decane mg/Kg wet0.050ND
Ethylbenzene mg/Kg wet0.050ND
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.050ND
2-Methylpentane mg/Kg wet0.050ND
Naphthalene mg/Kg wet0.50ND
Nonane mg/Kg wet0.050ND
Pentane mg/Kg wet0.050ND
Toluene mg/Kg wet0.050ND
1,2,4-Trimethylbenzene mg/Kg wet0.050ND
2,2,4-Trimethylpentane mg/Kg wet0.050ND
m+p Xylene mg/Kg wet0.10ND
o-Xylene mg/Kg wet0.050ND
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)93.137.3
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)86.334.5
LCS (B209997-BS1) Prepared: 08/10/18 Analyzed: 08/14/18
Benzene mg/Kg wet0.0010 0.100 70-1301070.107
Butylcyclohexane mg/Kg wet0.0010 0.100 70-13089.50.0895
Decane mg/Kg wet0.0010 0.100 70-13093.00.0930
Ethylbenzene mg/Kg wet0.0010 0.100 70-1301080.108
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.0010 0.100 70-1301090.109
2-Methylpentane mg/Kg wet0.0010 0.100 70-1301190.119
Naphthalene mg/Kg wet0.010 0.100 70-1301030.103
Nonane mg/Kg wet0.0010 0.100 30-13088.20.0882
Pentane mg/Kg wet0.0010 0.100 70-1301210.121
Toluene mg/Kg wet0.0010 0.100 70-1301070.107
1,2,4-Trimethylbenzene mg/Kg wet0.0010 0.100 70-1301090.109
2,2,4-Trimethylpentane mg/Kg wet0.0010 0.100 70-1301110.111
m+p Xylene mg/Kg wet0.0020 0.200 70-1301100.219
o-Xylene mg/Kg wet0.0010 0.100 70-1301070.107
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)94.237.7
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)87.735.1
LCS Dup (B209997-BSD1) Prepared: 08/10/18 Analyzed: 08/14/18
Benzene mg/Kg wet0.0010 0.100 2570-130106 0.5780.106
Butylcyclohexane mg/Kg wet0.0010 0.100 2570-13089.6 0.1520.0896
Decane mg/Kg wet0.0010 0.100 2570-13094.5 1.530.0945
Ethylbenzene mg/Kg wet0.0010 0.100 2570-130107 0.6420.107
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.0010 0.100 2570-130107 2.090.107
2-Methylpentane mg/Kg wet0.0010 0.100 2570-130118 0.7560.118
Naphthalene mg/Kg wet0.010 0.100 2570-130101 2.400.101
Nonane mg/Kg wet0.0010 0.100 2530-13088.5 0.2900.0885
Pentane mg/Kg wet0.0010 0.100 2570-130119 1.580.119
Toluene mg/Kg wet0.0010 0.100 2570-130106 0.6500.106
1,2,4-Trimethylbenzene mg/Kg wet0.0010 0.100 2570-130108 0.9920.108
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - VPH - Quality Control
QUALITY CONTROL
Batch B209997 - MA VPH
LCS Dup (B209997-BSD1) Prepared: 08/10/18 Analyzed: 08/14/18
2,2,4-Trimethylpentane mg/Kg wet0.0010 0.100 2570-130108 2.970.108
m+p Xylene mg/Kg wet0.0020 0.200 2570-130109 0.7790.217
o-Xylene mg/Kg wet0.0010 0.100 2570-130106 0.8960.106
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)95.238.1
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)87.735.1
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) - Quality Control
QUALITY CONTROL
[TOC_2]Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)[TOC]
Batch B210372 - % Solids
[TOC_3]B210372[TOC]
Duplicate (B210372-DUP1) Prepared & Analyzed: 08/15/18 Source: 18H0706-01
% Solids % Wt 200.10386.4 86.3
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
FLAG/QUALIFIER SUMMARY
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
J
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but
the other is within limits. RPD between the two LFB/LCS results is within method specified criteria.
L-07
Initial calibration did not meet method specifications. Compound was calibrated using a response factor where
%RSD is outside of method specified criteria. Reported result is estimated.
V-04
Continuing calibration did not meet method specifications and was biased on the low side for this compound.
Reported result is estimated.
V-05
Continuing calibration did not meet method specifications and was biased on the high side for this compound.
Reported result is estimated.
V-06
Continuing calibration did not meet method specifications and was biased on the high side. Data validation is not
affected since sample result was "not detected" for this compound.
V-20
Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this
compound. Reported result is estimated.
V-34
[TOC_1]Flag/Qualifier Summary[TOC]
Page 31 of 39
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CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
MADEP-EPH-04-1.1 in Soil
CT,NC,ME,NH-PC9-C18 Aliphatics
CT,NC,ME,NH-PC19-C36 Aliphatics
CT,NC,ME,NH-PUnadjusted C11-C22 Aromatics
CT,NC,ME,NH-PC11-C22 Aromatics
CT,NC,ME,NH-PAcenaphthene
CT,NC,ME,NH-PAcenaphthylene
CT,NC,ME,NH-PAnthracene
CT,NC,ME,NH-PBenzo(a)anthracene
CT,NC,ME,NH-PBenzo(a)pyrene
CT,NC,ME,NH-PBenzo(b)fluoranthene
CT,NC,ME,NH-PBenzo(g,h,i)perylene
CT,NC,ME,NH-PBenzo(k)fluoranthene
CT,NC,ME,NH-PChrysene
CT,NC,ME,NH-PDibenz(a,h)anthracene
CT,NC,ME,NH-PFluoranthene
CT,NC,MEFluorene
CT,NC,ME,NH-PIndeno(1,2,3-cd)pyrene
CT,NC,ME2-Methylnaphthalene
CT,NC,ME,NH-PNaphthalene
CT,NC,ME,NH-PPhenanthrene
CT,NC,ME,NH-PPyrene
MADEP-VPH-Feb 2018 Rev 2.1 in Soil
CT,NC,ME,NH-PUnadjusted C5-C8 Aliphatics
CT,NC,ME,NH-PC5-C8 Aliphatics
CT,NC,ME,NH-PUnadjusted C9-C12 Aliphatics
CT,NC,ME,NH-PC9-C12 Aliphatics
CT,NC,ME,NH-PC9-C10 Aromatics
CT,NC,ME,NH-PBenzene
CT,NC,ME,NH-PEthylbenzene
CT,NC,ME,NH-PMethyl tert-Butyl Ether (MTBE)
CT,NC,ME,NH-PNaphthalene
CT,NC,ME,NH-PToluene
CT,NC,ME,NH-Pm+p Xylene
CT,NC,ME,NH-Po-Xylene
SW-846 8260B in Soil
NCAcetone
NCAcrylonitrile
NCtert-Amyl Methyl Ether (TAME)
NCBenzene
NCBromobenzene
NCBromochloromethane
NCBromodichloromethane
NCBromoform
NCBromomethane
NC2-Butanone (MEK)
NCtert-Butyl Alcohol (TBA)
[TOC_1]Certifications[TOC]
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CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 8260B in Soil
NCn-Butylbenzene
NCsec-Butylbenzene
NCtert-Butylbenzene
NCtert-Butyl Ethyl Ether (TBEE)
NCCarbon Disulfide
NCCarbon Tetrachloride
NCChlorobenzene
NCChlorodibromomethane
NCChloroethane
NCChloroform
NCChloromethane
NC2-Chlorotoluene
NC4-Chlorotoluene
NC1,2-Dibromo-3-chloropropane (DBCP)
NC1,2-Dibromoethane (EDB)
NCDibromomethane
NC1,2-Dichlorobenzene
NC1,3-Dichlorobenzene
NC1,4-Dichlorobenzene
NCtrans-1,4-Dichloro-2-butene
NCDichlorodifluoromethane (Freon 12)
NC1,1-Dichloroethane
NC1,2-Dichloroethane
NC1,1-Dichloroethylene
NCcis-1,2-Dichloroethylene
NCtrans-1,2-Dichloroethylene
NC1,2-Dichloropropane
NC1,3-Dichloropropane
NC2,2-Dichloropropane
NC1,1-Dichloropropene
NCcis-1,3-Dichloropropene
NCtrans-1,3-Dichloropropene
NCDiethyl Ether
NCDiisopropyl Ether (DIPE)
NC1,4-Dioxane
NCEthylbenzene
NCHexachlorobutadiene
NC2-Hexanone (MBK)
NCIsopropylbenzene (Cumene)
NCp-Isopropyltoluene (p-Cymene)
NCMethyl tert-Butyl Ether (MTBE)
NCMethylene Chloride
NC4-Methyl-2-pentanone (MIBK)
NCNaphthalene
NCn-Propylbenzene
NCStyrene
NC1,1,1,2-Tetrachloroethane
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 8260B in Soil
NC1,1,2,2-Tetrachloroethane
NCTetrachloroethylene
NCTetrahydrofuran
NCToluene
NC1,2,3-Trichlorobenzene
NC1,2,4-Trichlorobenzene
NC1,3,5-Trichlorobenzene
NC1,1,1-Trichloroethane
NC1,1,2-Trichloroethane
NCTrichloroethylene
NCTrichlorofluoromethane (Freon 11)
NC1,2,3-Trichloropropane
NC1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
NC1,2,4-Trimethylbenzene
NC1,3,5-Trimethylbenzene
NCVinyl Chloride
NCm+p Xylene
NCo-Xylene
SW-846 8270D in Soil
CT,NY,NH,ME,NC,VAAcenaphthene
CT,NY,NH,ME,NC,VAAcenaphthylene
NY,NH,ME,NC,VAAcetophenone
NY,NH,ME,NC,VAAniline
CT,NY,NH,ME,NC,VAAnthracene
CT,NY,NH,ME,NC,VABenzidine
CT,NY,NH,ME,NC,VABenzo(a)anthracene
CT,NY,NH,ME,NC,VABenzo(a)pyrene
CT,NY,NH,ME,NC,VABenzo(b)fluoranthene
CT,NY,NH,ME,NC,VABenzo(g,h,i)perylene
CT,NY,NH,ME,NC,VABenzo(k)fluoranthene
NY,NH,ME,NC,VABenzoic Acid
CT,NY,NH,ME,NC,VABis(2-chloroethoxy)methane
CT,NY,NH,ME,NC,VABis(2-chloroethyl)ether
CT,NY,NH,ME,NC,VABis(2-chloroisopropyl)ether
CT,NY,NH,ME,NC,VABis(2-Ethylhexyl)phthalate
CT,NY,NH,ME,NC,VA4-Bromophenylphenylether
CT,NY,NH,ME,NC,VAButylbenzylphthalate
NCCarbazole
CT,NY,NH,ME,NC,VA4-Chloroaniline
CT,NY,NH,ME,NC,VA4-Chloro-3-methylphenol
CT,NY,NH,NC,VA2-Chloronaphthalene
CT,NY,NH,ME,NC,VA2-Chlorophenol
CT,NY,NH,ME,NC,VA4-Chlorophenylphenylether
CT,NY,NH,ME,NC,VAChrysene
CT,NY,NH,ME,NC,VADibenz(a,h)anthracene
CT,NY,NH,ME,NC,VADibenzofuran
Page 34 of 39
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 8270D in Soil
CT,NY,NH,ME,NC,VADi-n-butylphthalate
NY,NH,ME,NC,VA1,2-Dichlorobenzene
NY,NH,ME,NC,VA1,3-Dichlorobenzene
NY,NH,ME,NC,VA1,4-Dichlorobenzene
CT,NY,NH,ME,NC,VA3,3-Dichlorobenzidine
CT,NY,NH,ME,NC,VA2,4-Dichlorophenol
CT,NY,NH,ME,NC,VADiethylphthalate
CT,NY,NH,ME,NC,VA2,4-Dimethylphenol
CT,NY,NH,ME,NC,VADimethylphthalate
CT,NY,NH,ME,NC,VA4,6-Dinitro-2-methylphenol
CT,NY,NH,ME,NC,VA2,4-Dinitrophenol
CT,NY,NH,ME,NC,VA2,4-Dinitrotoluene
CT,NY,NH,ME,NC,VA2,6-Dinitrotoluene
CT,NY,NH,ME,NC,VADi-n-octylphthalate
NY,NH,ME,NC,VA1,2-Diphenylhydrazine (as Azobenzene)
CT,NY,NH,ME,NC,VAFluoranthene
NY,NH,ME,NC,VAFluorene
CT,NY,NH,ME,NC,VAHexachlorobenzene
CT,NY,NH,ME,NC,VAHexachlorobutadiene
CT,NY,NH,ME,NC,VAHexachlorocyclopentadiene
CT,NY,NH,ME,NC,VAHexachloroethane
CT,NY,NH,ME,NC,VAIndeno(1,2,3-cd)pyrene
CT,NY,NH,ME,NC,VAIsophorone
NC1-Methylnaphthalene
CT,NY,NH,ME,NC,VA2-Methylnaphthalene
CT,NY,NH,ME,NC,VA2-Methylphenol
CT,NY,NH,ME,NC,VA3/4-Methylphenol
CT,NY,NH,ME,NC,VANaphthalene
CT,NY,NH,ME,NC,VA2-Nitroaniline
CT,NY,NH,ME,NC,VA3-Nitroaniline
CT,NY,NH,ME,NC,VA4-Nitroaniline
CT,NY,NH,ME,NC,VANitrobenzene
CT,NY,NH,ME,NC,VA2-Nitrophenol
CT,NY,NH,ME,NC,VA4-Nitrophenol
CT,NY,NH,ME,NC,VAN-Nitrosodimethylamine
CT,NY,NH,ME,NC,VAN-Nitrosodiphenylamine
CT,NY,NH,ME,NC,VAN-Nitrosodi-n-propylamine
NY,NCPentachloronitrobenzene
CT,NY,NH,ME,NC,VAPentachlorophenol
CT,NY,NH,ME,NC,VAPhenanthrene
CT,NY,NH,ME,NC,VAPhenol
CT,NY,NH,ME,NC,VAPyrene
CT,NY,NH,ME,NC,VAPyridine
NY,NC1,2,4,5-Tetrachlorobenzene
CT,NY,NH,ME,NC,VA1,2,4-Trichlorobenzene
CT,NY,NH,ME,NC,VA2,4,5-Trichlorophenol
CT,NY,NH,ME,NC,VA2,4,6-Trichlorophenol
Page 35 of 39
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 8270D in Soil
NC2-Fluorophenol
The CON-TEST Environmental Laboratory operates under the following certifications and accreditations:
Code Description Number Expires
100033AIHA-LAP, LLC - ISO17025:2005AIHA 03/1/2020
M-MA100Massachusetts DEPMA 06/30/2019
PH-0567Connecticut Department of Publilc HealthCT 09/30/2019
10899 NELAPNew York State Department of HealthNY 04/1/2019
2516 NELAPNew Hampshire Environmental LabNH-S 02/5/2019
LAO00112Rhode Island Department of HealthRI 12/30/2018
652North Carolina Div. of Water QualityNC 12/31/2018
MA007 NELAPNew Jersey DEPNJ 06/30/2019
E871027 NELAPFlorida Department of HealthFL 06/30/2019
LL015036Vermont Department of Health Lead LaboratoryVT 07/30/2019
2011028State of MaineME 06/9/2019
460217Commonwealth of VirginiaVA 12/14/2018
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2018
VT-255716Vermont Department of Health Drinking WaterVT-DW 06/12/2019
25703North Carolina Department of HealthNC-DW 07/31/2019
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ANALYTICAL REPORT
February 13, 2020
ATC Group Services - NC Pilot
Sample Delivery Group:L1185652
Samples Received:02/04/2020
Project Number:6955-605-13
Description:Pilot 6955
Report To:Maureen Jackson
609A Piner Road Suite 115
Wilmington, NC 28409
Entire Report Reviewed By:
February 13, 2020
[Preliminary Report]
Jeff Carr
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received.
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
ATC Group Services - NC Pilot 6955-605-13 L1185652 02/13/20 17:46 1 of 17
February 13, 2020
Jeff Carr
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
ATC Group Services - NC Pilot 6955-605-13 L1185652 02/13/20 17:57 1 of 17
ONE LAB. NATIONWIDE.TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
MW-1 L1185652-01 5
Qc: Quality Control Summary 7
Volatile Petroleum Hydrocarbons by Method MADEPV 7
Volatile Organic Compounds (GC/MS) by Method 602MS 8
TPH by Method MADEPE 9
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 10
Gl: Glossary of Terms 14
Al: Accreditations & Locations 15
Sc: Sample Chain of Custody 16
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
ATC Group Services - NC Pilot 6955-605-13 L1185652 02/13/20 17:46 2 of 17
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
ATC Group Services - NC Pilot 6955-605-13 L1185652 02/13/20 17:57 2 of 17
ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-1 L1185652-01 GW Cory Nobles 01/31/20 12:30 02/04/20 08:30
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Petroleum Hydrocarbons by Method MADEPV WG1423777 1 02/06/20 20:11 02/06/20 20:11 BMB Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 602MS WG1423144 1 02/05/20 20:22 02/05/20 20:22 JHH Mt. Juliet, TN
TPH by Method MADEPE WG1426382 1 02/12/20 05:39 02/12/20 15:04 CLG Mt. Juliet, TN
TPH by Method MADEPE WG1426382 1 02/12/20 05:39 02/12/20 15:28 CLG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1424380 1 02/07/20 15:11 02/09/20 12:24 LEA Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
ATC Group Services - NC Pilot 6955-605-13 L1185652 02/13/20 17:46 3 of 17
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
ATC Group Services - NC Pilot 6955-605-13 L1185652 02/13/20 17:57 3 of 17
ONE LAB. NATIONWIDE.CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Jeff Carr
Project Manager
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
ATC Group Services - NC Pilot 6955-605-13 L1185652 02/13/20 17:46 4 of 17
Jeff Carr
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
ATC Group Services - NC Pilot 6955-605-13 L1185652 02/13/20 17:57 4 of 17
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L1185652
MW-1
Collected date/time: 01/31/20 12:30
Volatile Petroleum Hydrocarbons by Method MADEPV
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Unadjusted C5-C8 Aliphatics ND 0.100 1 02/06/2020 20:11 WG1423777
Unadjusted C9-C12 Aliphatics 0.104 0.100 1 02/06/2020 20:11 WG1423777
Unadjusted C9-C10 Aromatics 0.194 0.100 1 02/06/2020 20:11 WG1423777
Total VPH 0.298 0.100 1 02/06/2020 20:11 WG1423777
(S) 2,5-Dibromotoluene(FID)85.2 70.0-130 02/06/2020 20:11 WG1423777
(S) 2,5-Dibromotoluene(PID)90.3 70.0-130 02/06/2020 20:11 WG1423777
Volatile Organic Compounds (GC/MS) by Method 602MS
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Benzene ND 0.00100 1 02/05/2020 20:22 WG1423144
Toluene ND 0.00100 1 02/05/2020 20:22 WG1423144
Ethylbenzene ND 0.00100 1 02/05/2020 20:22 WG1423144
Total Xylenes ND 0.00300 1 02/05/2020 20:22 WG1423144
Methyl tert-butyl ether ND 0.00100 1 02/05/2020 20:22 WG1423144
Di-isopropyl ether ND 0.00100 1 02/05/2020 20:22 WG1423144
(S) Toluene-d8 102 80.0-120 02/05/2020 20:22 WG1423144
(S) 4-Bromofluorobenzene 101 77.0-126 02/05/2020 20:22 WG1423144
(S) 1,2-Dichloroethane-d4 99.1 70.0-130 02/05/2020 20:22 WG1423144
TPH by Method MADEPE
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Unadjusted C9-C18 Aliphatics ND 0.100 1 02/12/2020 15:04 WG1426382
Unadjusted C19-C36 Aliphatics ND 0.100 1 02/12/2020 15:04 WG1426382
Unadjusted C11-C22 Aromatics 0.313 0.100 1 02/12/2020 15:28 WG1426382
Unadjusted Total Petroleum
Hydrocarbons 0.350 0.100 1 02/12/2020 15:28 WG1426382
(S) o-Terphenyl 46.0 40.0-140 02/12/2020 15:28 WG1426382
(S) 1-Chloro-octadecane 23.6 J2 40.0-140 02/12/2020 15:04 WG1426382
(S) 2-Fluorobiphenyl 88.5 40.0-140 02/12/2020 15:28 WG1426382
(S) 2-Bromonaphthalene 87.0 40.0-140 02/12/2020 15:28 WG1426382
Sample Narrative:
L1185652-01 WG1426382: Duplicate Analysis performed due to surrogate failure. Results confirm; reporting in hold data
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Acenaphthene ND 0.00100 1 02/09/2020 12:24 WG1424380
Acenaphthylene ND 0.00100 1 02/09/2020 12:24 WG1424380
Anthracene ND 0.00100 1 02/09/2020 12:24 WG1424380
Benzidine ND J3 0.0100 1 02/09/2020 12:24 WG1424380
Benzo(a)anthracene ND 0.00100 1 02/09/2020 12:24 WG1424380
Benzo(b)fluoranthene ND 0.00100 1 02/09/2020 12:24 WG1424380
Benzo(k)fluoranthene ND 0.00100 1 02/09/2020 12:24 WG1424380
Benzo(g,h,i)perylene ND 0.00100 1 02/09/2020 12:24 WG1424380
Benzo(a)pyrene ND 0.00100 1 02/09/2020 12:24 WG1424380
Bis(2-chlorethoxy)methane ND 0.0100 1 02/09/2020 12:24 WG1424380
Bis(2-chloroethyl)ether ND 0.0100 1 02/09/2020 12:24 WG1424380
2,2-Oxybis(1-Chloropropane)ND 0.0100 1 02/09/2020 12:24 WG1424380
4-Bromophenyl-phenylether ND 0.0100 1 02/09/2020 12:24 WG1424380
2-Chloronaphthalene ND 0.00100 1 02/09/2020 12:24 WG1424380
4-Chlorophenyl-phenylether ND 0.0100 1 02/09/2020 12:24 WG1424380
Chrysene ND 0.00100 1 02/09/2020 12:24 WG1424380
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L1185652
MW-1
Collected date/time: 01/31/20 12:30
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/l mg/l date / time
Dibenz(a,h)anthracene ND 0.00100 1 02/09/2020 12:24 WG1424380
3,3-Dichlorobenzidine ND 0.0100 1 02/09/2020 12:24 WG1424380
2,4-Dinitrotoluene ND 0.0100 1 02/09/2020 12:24 WG1424380
2,6-Dinitrotoluene ND 0.0100 1 02/09/2020 12:24 WG1424380
Fluoranthene ND 0.00100 1 02/09/2020 12:24 WG1424380
Fluorene ND 0.00100 1 02/09/2020 12:24 WG1424380
Hexachlorobenzene ND 0.00100 1 02/09/2020 12:24 WG1424380
Hexachloro-1,3-butadiene ND 0.0100 1 02/09/2020 12:24 WG1424380
Hexachlorocyclopentadiene ND 0.0100 1 02/09/2020 12:24 WG1424380
Hexachloroethane ND 0.0100 1 02/09/2020 12:24 WG1424380
Indeno(1,2,3-cd)pyrene ND 0.00100 1 02/09/2020 12:24 WG1424380
Isophorone ND 0.0100 1 02/09/2020 12:24 WG1424380
Naphthalene ND 0.00100 1 02/09/2020 12:24 WG1424380
Nitrobenzene ND 0.0100 1 02/09/2020 12:24 WG1424380
n-Nitrosodimethylamine ND 0.0100 1 02/09/2020 12:24 WG1424380
n-Nitrosodiphenylamine ND 0.0100 1 02/09/2020 12:24 WG1424380
n-Nitrosodi-n-propylamine ND 0.0100 1 02/09/2020 12:24 WG1424380
Phenanthrene ND 0.00100 1 02/09/2020 12:24 WG1424380
Benzylbutyl phthalate ND 0.00300 1 02/09/2020 12:24 WG1424380
Bis(2-ethylhexyl)phthalate ND 0.00300 1 02/09/2020 12:24 WG1424380
Di-n-butyl phthalate ND 0.00300 1 02/09/2020 12:24 WG1424380
Diethyl phthalate ND 0.00300 1 02/09/2020 12:24 WG1424380
Dimethyl phthalate ND 0.00300 1 02/09/2020 12:24 WG1424380
Di-n-octyl phthalate ND 0.00300 1 02/09/2020 12:24 WG1424380
Pyrene ND 0.00100 1 02/09/2020 12:24 WG1424380
1,2,4-Trichlorobenzene ND 0.0100 1 02/09/2020 12:24 WG1424380
4-Chloro-3-methylphenol ND 0.0100 1 02/09/2020 12:24 WG1424380
2-Chlorophenol ND 0.0100 1 02/09/2020 12:24 WG1424380
2,4-Dichlorophenol ND 0.0100 1 02/09/2020 12:24 WG1424380
2,4-Dimethylphenol ND 0.0100 1 02/09/2020 12:24 WG1424380
4,6-Dinitro-2-methylphenol ND 0.0100 1 02/09/2020 12:24 WG1424380
2,4-Dinitrophenol ND 0.0100 1 02/09/2020 12:24 WG1424380
2-Nitrophenol ND 0.0100 1 02/09/2020 12:24 WG1424380
4-Nitrophenol ND 0.0100 1 02/09/2020 12:24 WG1424380
Pentachlorophenol ND 0.0100 1 02/09/2020 12:24 WG1424380
Phenol ND 0.0100 1 02/09/2020 12:24 WG1424380
2,4,6-Trichlorophenol ND 0.0100 1 02/09/2020 12:24 WG1424380
(S) Nitrobenzene-d5 47.1 15.0-314 02/09/2020 12:24 WG1424380
(S) 2-Fluorobiphenyl 50.0 22.0-127 02/09/2020 12:24 WG1424380
(S) p-Terphenyl-d14 60.8 29.0-141 02/09/2020 12:24 WG1424380
(S) Phenol-d5 17.4 8.00-424 02/09/2020 12:24 WG1424380
(S) 2-Fluorophenol 27.0 10.0-120 02/09/2020 12:24 WG1424380
(S) 2,4,6-Tribromophenol 114 10.0-153 02/09/2020 12:24 WG1424380
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1423777
Volatile Petroleum Hydrocarbons by Method MADEPV L1185652-01
Method Blank (MB)
(MB) R3498486-3 02/06/20 18:50
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Unadjusted C5-C8 Aliphatics U 0.0333 0.100
Unadjusted C9-C12 Aliphatics U 0.0333 0.100
Unadjusted C9-C10 Aromatics U 0.0333 0.100
Total VPH U 0.0333 0.100
(S) 2,5-Dibromotoluene(FID)86.1 70.0-130
(S) 2,5-Dibromotoluene(PID)87.2 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3498486-1 02/06/20 10:18 • (LCSD) R3498486-2 02/06/20 10:51
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Unadjusted C5-C8 Aliphatics 1.20 1.30 1.30 108 108 70.0-130 0.000 25
Unadjusted C9-C12 Aliphatics 1.40 1.71 1.71 122 122 70.0-130 0.000 25
Unadjusted C9-C10 Aromatics 0.200 0.243 0.243 122 122 70.0-130 0.000 25
Total VPH 2.80 3.25 3.25 116 116 70.0-130 0.000 25
(S) 2,5-Dibromotoluene(FID) 93.1 95.0 70.0-130
(S) 2,5-Dibromotoluene(PID) 95.5 96.9 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1423144
Volatile Organic Compounds (GC/MS) by Method 602MS L1185652-01
Method Blank (MB)
(MB) R3497406-2 02/05/20 16:17
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Benzene U 0.000331 0.00100
Di-isopropyl ether U 0.000320 0.00100
Ethylbenzene U 0.000384 0.00100
Methyl tert-butyl ether U 0.000367 0.00100
Toluene U 0.000412 0.00100
Xylenes, Total U 0.00106 0.00300
(S) Toluene-d8 103 80.0-120
(S) 4-Bromofluorobenzene 99.4 77.0-126
(S) 1,2-Dichloroethane-d4 99.2 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3497406-1 02/05/20 15:36
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/l mg/l %%
Benzene 0.00500 0.00477 95.4 70.0-123
Di-isopropyl ether 0.00500 0.00405 81.0 58.0-138
Ethylbenzene 0.00500 0.00484 96.8 79.0-123
Methyl tert-butyl ether 0.00500 0.00484 96.8 68.0-125
Toluene 0.00500 0.00481 96.2 79.0-120
Xylenes, Total 0.0150 0.0149 99.3 79.0-123
(S) Toluene-d8 102 80.0-120
(S) 4-Bromofluorobenzene 99.7 77.0-126
(S) 1,2-Dichloroethane-d4 99.3 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1426382
TPH by Method MADEPE L1185652-01
Method Blank (MB)
(MB) R3499672-1 02/12/20 12:41
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Unadjusted C9-C18 Aliphatics 0.0333 J 0.0333 0.100
Unadjusted C19-C36 Aliphatics U 0.0333 0.100
(S) 1-Chloro-octadecane 48.6 40.0-140
Method Blank (MB)
(MB) R3499672-4 02/12/20 13:52
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Unadjusted C11-C22 Aromatics U 0.0333 0.100
(S) o-Terphenyl 71.3 40.0-140
(S) 2-Fluorobiphenyl 86.6 40.0-140
(S) 2-Bromonaphthalene 81.0 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3499672-2 02/12/20 13:05 • (LCSD) R3499672-3 02/12/20 13:28
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Unadjusted C9-C18 Aliphatics 0.600 0.333 0.309 55.5 51.5 40.0-140 7.48 25
Unadjusted C19-C36 Aliphatics 0.800 0.541 0.510 67.6 63.7 40.0-140 5.90 25
(S) 1-Chloro-octadecane 44.9 43.1 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3499672-5 02/12/20 14:16 • (LCSD) R3499672-6 02/12/20 14:40
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Unadjusted C11-C22 Aromatics 1.70 1.10 1.22 64.7 71.8 40.0-140 10.3 25
(S) o-Terphenyl 63.2 67.9 40.0-140
(S) 2-Fluorobiphenyl 83.6 95.1 40.0-140
(S) 2-Bromonaphthalene 77.3 88.6 40.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1424380
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1185652-01
Method Blank (MB)
(MB) R3498145-3 02/08/20 13:11
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Acenaphthene U 0.000316 0.00100
Acenaphthylene U 0.000309 0.00100
Anthracene U 0.000291 0.00100
Benzidine U 0.00432 0.0100
Benzo(a)anthracene U 0.0000975 0.00100
Benzo(b)fluoranthene U 0.0000896 0.00100
Benzo(k)fluoranthene U 0.000355 0.00100
Benzo(g,h,i)perylene U 0.000161 0.00100
Benzo(a)pyrene U 0.000340 0.00100
Bis(2-chlorethoxy)methane U 0.000329 0.0100
Bis(2-chloroethyl)ether U 0.00162 0.0100
2,2-oxybis(1-chloropropane)U 0.000445 0.0100
4-Bromophenyl-phenylether U 0.000335 0.0100
2-Chloronaphthalene U 0.000330 0.00100
4-Chlorophenyl-phenylether U 0.000303 0.0100
Chrysene U 0.000332 0.00100
Dibenz(a,h)anthracene U 0.000279 0.00100
3,3-Dichlorobenzidine U 0.00202 0.0100
2,4-Dinitrotoluene U 0.00165 0.0100
2,6-Dinitrotoluene U 0.000279 0.0100
Fluoranthene U 0.000310 0.00100
Fluorene U 0.000323 0.00100
Hexachlorobenzene U 0.000341 0.00100
Hexachloro-1,3-butadiene U 0.000329 0.0100
Hexachlorocyclopentadiene U 0.00233 0.0100
Hexachloroethane U 0.000365 0.0100
Indeno(1,2,3-cd)pyrene U 0.000279 0.00100
Isophorone U 0.000272 0.0100
Naphthalene U 0.000372 0.00100
Nitrobenzene U 0.000367 0.0100
n-Nitrosodimethylamine U 0.00126 0.0100
n-Nitrosodiphenylamine U 0.00119 0.0100
n-Nitrosodi-n-propylamine U 0.000403 0.0100
Phenanthrene U 0.000366 0.00100
Benzylbutyl phthalate U 0.000275 0.00300
Bis(2-ethylhexyl)phthalate U 0.000709 0.00300
Di-n-butyl phthalate U 0.000266 0.00300
Diethyl phthalate U 0.000282 0.00300
Dimethyl phthalate U 0.000283 0.00300
Di-n-octyl phthalate U 0.000278 0.00300
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1424380
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1185652-01
Method Blank (MB)
(MB) R3498145-3 02/08/20 13:11
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mg/l mg/l
Pyrene U 0.000330 0.00100
1,2,4-Trichlorobenzene U 0.000355 0.0100
4-Chloro-3-methylphenol U 0.000263 0.0100
2-Chlorophenol U 0.000283 0.0100
2-Nitrophenol U 0.000320 0.0100
4-Nitrophenol U 0.00201 0.0100
Pentachlorophenol U 0.000313 0.0100
Phenol U 0.000334 0.0100
2,4,6-Trichlorophenol U 0.000297 0.0100
2,4-Dichlorophenol U 0.000284 0.0100
2,4-Dimethylphenol U 0.000624 0.0100
4,6-Dinitro-2-methylphenol U 0.00262 0.0100
2,4-Dinitrophenol U 0.00325 0.0100
(S) Nitrobenzene-d5 62.5 15.0-314
(S) 2-Fluorobiphenyl 66.0 22.0-127
(S) p-Terphenyl-d14 87.2 29.0-141
(S) Phenol-d5 22.7 8.00-424
(S) 2-Fluorophenol 37.8 10.0-120
(S) 2,4,6-Tribromophenol 121 10.0-153
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3498145-1 02/08/20 12:29 • (LCSD) R3498145-2 02/08/20 12:50
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Acenaphthene 0.0500 0.0299 0.0359 59.8 71.8 47.0-145 18.2 48
Acenaphthylene 0.0500 0.0322 0.0388 64.4 77.6 33.0-145 18.6 74
Anthracene 0.0500 0.0333 0.0397 66.6 79.4 27.0-133 17.5 66
Benzidine 0.100 0.0193 0.0284 19.3 28.4 1.00-120 J3 38.2 36
Benzo(a)anthracene 0.0500 0.0368 0.0430 73.6 86.0 33.0-143 15.5 53
Benzo(b)fluoranthene 0.0500 0.0353 0.0422 70.6 84.4 24.0-159 17.8 71
Benzo(k)fluoranthene 0.0500 0.0362 0.0409 72.4 81.8 11.0-162 12.2 63
Benzo(g,h,i)perylene 0.0500 0.0347 0.0401 69.4 80.2 1.00-219 14.4 97
Benzo(a)pyrene 0.0500 0.0379 0.0443 75.8 88.6 17.0-163 15.6 72
Bis(2-chlorethoxy)methane 0.0500 0.0272 0.0326 54.4 65.2 1.00-219 18.1 54
Bis(2-chloroethyl)ether 0.0500 0.0277 0.0346 55.4 69.2 33.0-185 22.2 108
2,2-oxybis(1-chloropropane)0.0500 0.0294 0.0365 58.8 73.0 36.0-166 21.5 76
4-Bromophenyl-phenylether 0.0500 0.0369 0.0462 73.8 92.4 53.0-127 22.4 43
2-Chloronaphthalene 0.0500 0.0305 0.0371 61.0 74.2 60.0-120 19.5 24
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ATC Group Services - NC Pilot 6955-605-13 L1185652 02/13/20 17:57 11 of 17
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1424380
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1185652-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3498145-1 02/08/20 12:29 • (LCSD) R3498145-2 02/08/20 12:50
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
4-Chlorophenyl-phenylether 0.0500 0.0322 0.0388 64.4 77.6 25.0-158 18.6 61
Chrysene 0.0500 0.0349 0.0412 69.8 82.4 17.0-168 16.6 87
Dibenz(a,h)anthracene 0.0500 0.0376 0.0437 75.2 87.4 1.00-227 15.0 126
3,3-Dichlorobenzidine 0.100 0.0647 0.0777 64.7 77.7 1.00-262 18.3 108
2,4-Dinitrotoluene 0.0500 0.0349 0.0402 69.8 80.4 39.0-139 14.1 42
2,6-Dinitrotoluene 0.0500 0.0325 0.0387 65.0 77.4 50.0-158 17.4 48
Fluoranthene 0.0500 0.0351 0.0405 70.2 81.0 26.0-137 14.3 66
Fluorene 0.0500 0.0319 0.0378 63.8 75.6 59.0-121 16.9 38
Hexachlorobenzene 0.0500 0.0377 0.0457 75.4 91.4 1.00-152 19.2 55
Hexachloro-1,3-butadiene 0.0500 0.0280 0.0341 56.0 68.2 24.0-120 19.6 62
Hexachlorocyclopentadiene 0.0500 0.0225 0.0290 45.0 58.0 10.0-120 25.2 31
Hexachloroethane 0.0500 0.0266 0.0335 53.2 67.0 40.0-120 23.0 52
Indeno(1,2,3-cd)pyrene 0.0500 0.0371 0.0429 74.2 85.8 1.00-171 14.5 99
Isophorone 0.0500 0.0279 0.0330 55.8 66.0 21.0-196 16.7 93
Naphthalene 0.0500 0.0262 0.0311 52.4 62.2 21.0-133 17.1 65
Nitrobenzene 0.0500 0.0257 0.0308 51.4 61.6 35.0-180 18.1 62
n-Nitrosodimethylamine 0.0500 0.0164 0.0213 32.8 42.6 10.0-120 26.0 34
n-Nitrosodiphenylamine 0.0500 0.0330 0.0402 66.0 80.4 44.0-120 19.7 21
n-Nitrosodi-n-propylamine 0.0500 0.0313 0.0387 62.6 77.4 1.00-230 21.1 87
Phenanthrene 0.0500 0.0330 0.0397 66.0 79.4 54.0-120 18.4 39
Benzylbutyl phthalate 0.0500 0.0377 0.0447 75.4 89.4 1.00-152 17.0 60
Bis(2-ethylhexyl)phthalate 0.0500 0.0358 0.0424 71.6 84.8 8.00-158 16.9 82
Di-n-butyl phthalate 0.0500 0.0391 0.0465 78.2 93.0 1.00-120 17.3 47
Diethyl phthalate 0.0500 0.0350 0.0410 70.0 82.0 1.00-120 15.8 100
Dimethyl phthalate 0.0500 0.0337 0.0398 67.4 79.6 1.00-120 16.6 183
Di-n-octyl phthalate 0.0500 0.0367 0.0445 73.4 89.0 4.00-146 19.2 69
Pyrene 0.0500 0.0390 0.0451 78.0 90.2 52.0-120 14.5 49
1,2,4-Trichlorobenzene 0.0500 0.0268 0.0323 53.6 64.6 44.0-142 18.6 50
4-Chloro-3-methylphenol 0.0500 0.0265 0.0308 53.0 61.6 22.0-147 15.0 73
2-Chlorophenol 0.0500 0.0255 0.0331 51.0 66.2 23.0-134 25.9 61
2,4-Dichlorophenol 0.0500 0.0266 0.0318 53.2 63.6 39.0-135 17.8 50
2,4-Dimethylphenol 0.0500 0.0201 0.0241 40.2 48.2 32.0-120 18.1 58
4,6-Dinitro-2-methylphenol 0.0500 0.0362 0.0417 72.4 83.4 1.00-181 14.1 203
2,4-Dinitrophenol 0.0500 0.0338 0.0387 67.6 77.4 1.00-191 13.5 132
2-Nitrophenol 0.0500 0.0261 0.0310 52.2 62.0 29.0-182 17.2 55
4-Nitrophenol 0.0500 0.0142 0.0167 28.4 33.4 1.00-132 16.2 131
Pentachlorophenol 0.0500 0.0419 0.0471 83.8 94.2 14.0-176 11.7 86
Phenol 0.0500 0.0112 0.0146 22.4 29.2 5.00-120 26.4 64
2,4,6-Trichlorophenol 0.0500 0.0331 0.0402 66.2 80.4 37.0-144 19.4 58
(S) Nitrobenzene-d5 48.5 58.6 15.0-314
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
ATC Group Services - NC Pilot 6955-605-13 L1185652 02/13/20 17:46 12 of 17
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
ATC Group Services - NC Pilot 6955-605-13 L1185652 02/13/20 17:57 12 of 17
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1424380
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1185652-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3498145-1 02/08/20 12:29 • (LCSD) R3498145-2 02/08/20 12:50
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
(S) 2-Fluorobiphenyl 58.9 72.6 22.0-127
(S) p-Terphenyl-d14 75.3 87.6 29.0-141
(S) Phenol-d5 20.7 27.7 8.00-424
(S) 2-Fluorophenol 33.1 44.1 10.0-120
(S) 2,4,6-Tribromophenol 121 133 10.0-153
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
J The identification of the analyte is acceptable; the reported value is an estimate.
J2 Surrogate recovery limits have been exceeded; values are outside lower control limits.
J3 The associated batch QC was outside the established quality control range for precision.
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ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing
turn-around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National.

State Accreditations
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN-03-2002-34
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹n/a
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶90010 South Carolina 84004
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana ¹LA180010 Texas T104704245-18-15
Maine TN0002 Texas ⁵LAB0152
Maryland 324 Utah TN00003
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 460132
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 9980939910
Montana CERT0086 Wyoming A2LA

Third Party Federal Accreditations
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable

Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contactour main office. Pace National performs all testing at our central laboratory.
1 Cp
2Tc
3Ss
4Cn
5Sr
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ANALYTICAL REPORT
January 27, 2020
ATC Group Services - NC Pilot
Sample Delivery Group:L1181391
Samples Received:01/21/2020
Project Number:6955-605-13
Description:Pilot 6955
Report To:Maureen Jackson
609A Piner Road Suite 115
Wilmington, NC 28409
Entire Report Reviewed By:
January 27, 2020
[Preliminary Report]
Jeff Carr
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received.
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2Tc
3Ss
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January 28, 2020
Jeff Carr
Project Manager
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ONE LAB. NATIONWIDE.TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
MW-1 (5-6) L1181391-01 5
MW-1 (15-16) L1181391-02 8
MW-1 (10-11) L1181391-03 11
Qc: Quality Control Summary 12
Total Solids by Method 2540 G-2011 12
Volatile Petroleum Hydrocarbons by Method MADEPV 13
Volatile Organic Compounds (GC/MS) by Method 8260D 14
TPH by Method MADEPE 20
Semi Volatile Organic Compounds (GC/MS) by Method 8270E 22
Gl: Glossary of Terms 26
Al: Accreditations & Locations 27
Sc: Sample Chain of Custody 28
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-1 (5-6) L1181391-01 Solid Cory Nobles 01/16/20 16:00 01/21/20 08:30
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1415317 1 01/23/20 18:44 01/23/20 19:10 KDW Mt. Juliet, TN
Volatile Petroleum Hydrocarbons by Method MADEPV WG1415331 1 01/16/20 16:00 01/22/20 14:22 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG1415264 1 01/16/20 16:00 01/22/20 16:20 DWR Mt. Juliet, TN
TPH by Method MADEPE WG1415374 1 01/22/20 11:46 01/23/20 20:46 SHG Mt. Juliet, TN
TPH by Method MADEPE WG1415374 1 01/22/20 11:46 01/24/20 00:20 SHG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1416103 1 01/23/20 20:46 01/24/20 02:57 JNJ Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-1 (15-16) L1181391-02 Solid Cory Nobles 01/16/20 18:00 01/21/20 08:30
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1415317 1 01/23/20 18:44 01/23/20 19:10 KDW Mt. Juliet, TN
Volatile Petroleum Hydrocarbons by Method MADEPV WG1415331 1 01/16/20 18:00 01/22/20 14:55 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG1415264 1 01/16/20 18:00 01/22/20 16:40 DWR Mt. Juliet, TN
TPH by Method MADEPE WG1415374 1 01/22/20 11:46 01/23/20 21:57 SHG Mt. Juliet, TN
TPH by Method MADEPE WG1415374 1 01/22/20 11:46 01/23/20 23:08 SHG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1416103 1 01/23/20 20:46 01/24/20 02:37 JNJ Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-1 (10-11) L1181391-03 Solid Cory Nobles 01/16/20 17:00 01/21/20 08:30
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1415317 1 01/23/20 18:44 01/23/20 19:10 KDW Mt. Juliet, TN
Volatile Petroleum Hydrocarbons by Method MADEPV WG1415331 1 01/16/20 17:00 01/22/20 15:28 ACG Mt. Juliet, TN
TPH by Method MADEPE WG1415374 1 01/22/20 11:46 01/23/20 22:21 SHG Mt. Juliet, TN
TPH by Method MADEPE WG1415374 1 01/22/20 11:46 01/23/20 22:45 SHG Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Jeff Carr
Project Manager
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Jeff Carr
Project Manager
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L1181391
MW-1 (5-6)
Collected date/time: 01/16/20 16:00
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 88.0 1 01/23/2020 19:10 WG1415317
Volatile Petroleum Hydrocarbons by Method MADEPV
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Unadjusted C5-C8 Aliphatics ND 5.68 1 01/22/2020 14:22 WG1415331
Unadjusted C9-C12 Aliphatics ND 5.68 1 01/22/2020 14:22 WG1415331
Unadjusted C9-C10 Aromatics ND 5.68 1 01/22/2020 14:22 WG1415331
Total VPH ND 5.68 1 01/22/2020 14:22 WG1415331
(S) 2,5-Dibromotoluene(FID)88.5 70.0-130 01/22/2020 14:22 WG1415331
(S) 2,5-Dibromotoluene(PID)85.8 70.0-130 01/22/2020 14:22 WG1415331
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND J3 0.0284 1 01/22/2020 16:20 WG1415264
Acrylonitrile ND 0.0142 1 01/22/2020 16:20 WG1415264
Benzene ND 0.00114 1 01/22/2020 16:20 WG1415264
Bromobenzene ND 0.0142 1 01/22/2020 16:20 WG1415264
Bromodichloromethane ND 0.00284 1 01/22/2020 16:20 WG1415264
Bromoform ND 0.0284 1 01/22/2020 16:20 WG1415264
Bromomethane ND 0.0142 1 01/22/2020 16:20 WG1415264
n-Butylbenzene ND 0.0142 1 01/22/2020 16:20 WG1415264
sec-Butylbenzene ND 0.0142 1 01/22/2020 16:20 WG1415264
tert-Butylbenzene ND 0.00568 1 01/22/2020 16:20 WG1415264
Carbon tetrachloride ND 0.00568 1 01/22/2020 16:20 WG1415264
Chlorobenzene ND 0.00284 1 01/22/2020 16:20 WG1415264
Chlorodibromomethane ND 0.00284 1 01/22/2020 16:20 WG1415264
Chloroethane ND 0.00568 1 01/22/2020 16:20 WG1415264
Chloroform ND 0.00284 1 01/22/2020 16:20 WG1415264
Chloromethane ND 0.0142 1 01/22/2020 16:20 WG1415264
2-Chlorotoluene ND 0.00284 1 01/22/2020 16:20 WG1415264
4-Chlorotoluene ND 0.00568 1 01/22/2020 16:20 WG1415264
1,2-Dibromo-3-Chloropropane ND 0.0284 1 01/22/2020 16:20 WG1415264
1,2-Dibromoethane ND 0.00284 1 01/22/2020 16:20 WG1415264
Dibromomethane ND 0.00568 1 01/22/2020 16:20 WG1415264
1,2-Dichlorobenzene ND 0.00568 1 01/22/2020 16:20 WG1415264
1,3-Dichlorobenzene ND 0.00568 1 01/22/2020 16:20 WG1415264
1,4-Dichlorobenzene ND 0.00568 1 01/22/2020 16:20 WG1415264
Dichlorodifluoromethane ND 0.00284 1 01/22/2020 16:20 WG1415264
1,1-Dichloroethane ND 0.00284 1 01/22/2020 16:20 WG1415264
1,2-Dichloroethane ND 0.00284 1 01/22/2020 16:20 WG1415264
1,1-Dichloroethene ND 0.00284 1 01/22/2020 16:20 WG1415264
cis-1,2-Dichloroethene ND 0.00284 1 01/22/2020 16:20 WG1415264
trans-1,2-Dichloroethene ND 0.00568 1 01/22/2020 16:20 WG1415264
1,2-Dichloropropane ND 0.00568 1 01/22/2020 16:20 WG1415264
1,1-Dichloropropene ND 0.00284 1 01/22/2020 16:20 WG1415264
1,3-Dichloropropane ND 0.00568 1 01/22/2020 16:20 WG1415264
cis-1,3-Dichloropropene ND 0.00284 1 01/22/2020 16:20 WG1415264
trans-1,3-Dichloropropene ND 0.00568 1 01/22/2020 16:20 WG1415264
2,2-Dichloropropane ND 0.00284 1 01/22/2020 16:20 WG1415264
Di-isopropyl ether ND 0.00114 1 01/22/2020 16:20 WG1415264
Ethylbenzene ND 0.00284 1 01/22/2020 16:20 WG1415264
Hexachloro-1,3-butadiene ND 0.0284 1 01/22/2020 16:20 WG1415264
Isopropylbenzene ND 0.00284 1 01/22/2020 16:20 WG1415264
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L1181391
MW-1 (5-6)
Collected date/time: 01/16/20 16:00
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
p-Isopropyltoluene ND 0.00568 1 01/22/2020 16:20 WG1415264
2-Butanone (MEK)ND 0.0284 1 01/22/2020 16:20 WG1415264
Methylene Chloride ND 0.0284 1 01/22/2020 16:20 WG1415264
4-Methyl-2-pentanone (MIBK)ND 0.0284 1 01/22/2020 16:20 WG1415264
Methyl tert-butyl ether ND 0.00114 1 01/22/2020 16:20 WG1415264
Naphthalene ND 0.0142 1 01/22/2020 16:20 WG1415264
n-Propylbenzene ND 0.00568 1 01/22/2020 16:20 WG1415264
Styrene ND 0.0142 1 01/22/2020 16:20 WG1415264
1,1,1,2-Tetrachloroethane ND 0.00284 1 01/22/2020 16:20 WG1415264
1,1,2,2-Tetrachloroethane ND 0.00284 1 01/22/2020 16:20 WG1415264
1,1,2-Trichlorotrifluoroethane ND 0.00284 1 01/22/2020 16:20 WG1415264
Tetrachloroethene ND 0.00284 1 01/22/2020 16:20 WG1415264
Toluene ND 0.00568 1 01/22/2020 16:20 WG1415264
1,2,3-Trichlorobenzene ND 0.0142 1 01/22/2020 16:20 WG1415264
1,2,4-Trichlorobenzene ND 0.0142 1 01/22/2020 16:20 WG1415264
1,1,1-Trichloroethane ND 0.00284 1 01/22/2020 16:20 WG1415264
1,1,2-Trichloroethane ND 0.00284 1 01/22/2020 16:20 WG1415264
Trichloroethene ND 0.00114 1 01/22/2020 16:20 WG1415264
Trichlorofluoromethane ND 0.00284 1 01/22/2020 16:20 WG1415264
1,2,3-Trichloropropane ND 0.0142 1 01/22/2020 16:20 WG1415264
1,2,4-Trimethylbenzene ND 0.00568 1 01/22/2020 16:20 WG1415264
1,2,3-Trimethylbenzene ND 0.00568 1 01/22/2020 16:20 WG1415264
Vinyl chloride ND 0.00284 1 01/22/2020 16:20 WG1415264
1,3,5-Trimethylbenzene ND 0.00568 1 01/22/2020 16:20 WG1415264
Xylenes, Total ND 0.00739 1 01/22/2020 16:20 WG1415264
(S) Toluene-d8 99.3 75.0-131 01/22/2020 16:20 WG1415264
(S) 4-Bromofluorobenzene 98.9 67.0-138 01/22/2020 16:20 WG1415264
(S) 1,2-Dichloroethane-d4 95.6 70.0-130 01/22/2020 16:20 WG1415264
TPH by Method MADEPE
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Unadjusted C9-C18 Aliphatics ND 7.39 1 01/23/2020 20:46 WG1415374
Unadjusted C19-C36 Aliphatics 12.6 J6 7.39 1 01/23/2020 20:46 WG1415374
Unadjusted C11-C22 Aromatics 9.84 7.39 1 01/24/2020 00:20 WG1415374
Unadjusted Total Petroleum
Hydrocarbons 22.5 7.39 1 01/24/2020 00:20 WG1415374
(S) o-Terphenyl 73.1 40.0-140 01/24/2020 00:20 WG1415374
(S) 1-Chloro-octadecane 80.5 40.0-140 01/23/2020 20:46 WG1415374
(S) 2-Fluorobiphenyl 90.2 40.0-140 01/24/2020 00:20 WG1415374
(S) 2-Bromonaphthalene 85.0 40.0-140 01/24/2020 00:20 WG1415374
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0378 1 01/24/2020 02:57 WG1416103
Acenaphthylene ND 0.0378 1 01/24/2020 02:57 WG1416103
Anthracene ND 0.0378 1 01/24/2020 02:57 WG1416103
Benzidine ND 0.378 1 01/24/2020 02:57 WG1416103
Benzo(a)anthracene ND 0.0378 1 01/24/2020 02:57 WG1416103
Benzo(b)fluoranthene ND 0.0378 1 01/24/2020 02:57 WG1416103
Benzo(k)fluoranthene ND 0.0378 1 01/24/2020 02:57 WG1416103
Benzo(g,h,i)perylene ND 0.0378 1 01/24/2020 02:57 WG1416103
Benzo(a)pyrene ND 0.0378 1 01/24/2020 02:57 WG1416103
Bis(2-chlorethoxy)methane ND 0.378 1 01/24/2020 02:57 WG1416103
Bis(2-chloroethyl)ether ND 0.378 1 01/24/2020 02:57 WG1416103
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L1181391
MW-1 (5-6)
Collected date/time: 01/16/20 16:00
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
2,2-Oxybis(1-Chloropropane)ND 0.378 1 01/24/2020 02:57 WG1416103
4-Bromophenyl-phenylether ND 0.378 1 01/24/2020 02:57 WG1416103
2-Chloronaphthalene ND 0.0378 1 01/24/2020 02:57 WG1416103
4-Chlorophenyl-phenylether ND 0.378 1 01/24/2020 02:57 WG1416103
Chrysene ND 0.0378 1 01/24/2020 02:57 WG1416103
Dibenz(a,h)anthracene ND 0.0378 1 01/24/2020 02:57 WG1416103
3,3-Dichlorobenzidine ND 0.378 1 01/24/2020 02:57 WG1416103
2,4-Dinitrotoluene ND 0.378 1 01/24/2020 02:57 WG1416103
2,6-Dinitrotoluene ND 0.378 1 01/24/2020 02:57 WG1416103
Fluoranthene ND 0.0378 1 01/24/2020 02:57 WG1416103
Fluorene ND 0.0378 1 01/24/2020 02:57 WG1416103
Hexachlorobenzene ND 0.378 1 01/24/2020 02:57 WG1416103
Hexachloro-1,3-butadiene ND 0.378 1 01/24/2020 02:57 WG1416103
Hexachlorocyclopentadiene ND 0.378 1 01/24/2020 02:57 WG1416103
Hexachloroethane ND 0.378 1 01/24/2020 02:57 WG1416103
Indeno(1,2,3-cd)pyrene ND 0.0378 1 01/24/2020 02:57 WG1416103
Isophorone ND 0.378 1 01/24/2020 02:57 WG1416103
Naphthalene ND 0.0378 1 01/24/2020 02:57 WG1416103
Nitrobenzene ND 0.378 1 01/24/2020 02:57 WG1416103
n-Nitrosodimethylamine ND 0.378 1 01/24/2020 02:57 WG1416103
n-Nitrosodiphenylamine ND 0.378 1 01/24/2020 02:57 WG1416103
n-Nitrosodi-n-propylamine ND 0.378 1 01/24/2020 02:57 WG1416103
Phenanthrene ND 0.0378 1 01/24/2020 02:57 WG1416103
Benzylbutyl phthalate ND 0.378 1 01/24/2020 02:57 WG1416103
Bis(2-ethylhexyl)phthalate ND 0.378 1 01/24/2020 02:57 WG1416103
Di-n-butyl phthalate ND 0.378 1 01/24/2020 02:57 WG1416103
Diethyl phthalate ND 0.378 1 01/24/2020 02:57 WG1416103
Dimethyl phthalate ND 0.378 1 01/24/2020 02:57 WG1416103
Di-n-octyl phthalate ND 0.378 1 01/24/2020 02:57 WG1416103
Pyrene ND 0.0378 1 01/24/2020 02:57 WG1416103
1,2,4-Trichlorobenzene ND 0.378 1 01/24/2020 02:57 WG1416103
4-Chloro-3-methylphenol ND 0.378 1 01/24/2020 02:57 WG1416103
2-Chlorophenol ND 0.378 1 01/24/2020 02:57 WG1416103
2,4-Dichlorophenol ND 0.378 1 01/24/2020 02:57 WG1416103
2,4-Dimethylphenol ND 0.378 1 01/24/2020 02:57 WG1416103
4,6-Dinitro-2-methylphenol ND 0.378 1 01/24/2020 02:57 WG1416103
2,4-Dinitrophenol ND 0.378 1 01/24/2020 02:57 WG1416103
2-Nitrophenol ND 0.378 1 01/24/2020 02:57 WG1416103
4-Nitrophenol ND 0.378 1 01/24/2020 02:57 WG1416103
Pentachlorophenol ND 0.378 1 01/24/2020 02:57 WG1416103
Phenol ND 0.378 1 01/24/2020 02:57 WG1416103
2,4,6-Trichlorophenol ND 0.378 1 01/24/2020 02:57 WG1416103
(S) 2-Fluorophenol 66.1 12.0-120 01/24/2020 02:57 WG1416103
(S) Phenol-d5 64.8 10.0-120 01/24/2020 02:57 WG1416103
(S) Nitrobenzene-d5 45.8 10.0-122 01/24/2020 02:57 WG1416103
(S) 2-Fluorobiphenyl 46.7 15.0-120 01/24/2020 02:57 WG1416103
(S) 2,4,6-Tribromophenol 67.6 10.0-127 01/24/2020 02:57 WG1416103
(S) p-Terphenyl-d14 57.2 10.0-120 01/24/2020 02:57 WG1416103
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L1181391
MW-1 (15-16)
Collected date/time: 01/16/20 18:00
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 92.3 1 01/23/2020 19:10 WG1415317
Volatile Petroleum Hydrocarbons by Method MADEPV
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Unadjusted C5-C8 Aliphatics ND 5.42 1 01/22/2020 14:55 WG1415331
Unadjusted C9-C12 Aliphatics ND 5.42 1 01/22/2020 14:55 WG1415331
Unadjusted C9-C10 Aromatics ND 5.42 1 01/22/2020 14:55 WG1415331
Total VPH ND 5.42 1 01/22/2020 14:55 WG1415331
(S) 2,5-Dibromotoluene(FID)90.5 70.0-130 01/22/2020 14:55 WG1415331
(S) 2,5-Dibromotoluene(PID)89.1 70.0-130 01/22/2020 14:55 WG1415331
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND J3 0.0271 1 01/22/2020 16:40 WG1415264
Acrylonitrile ND 0.0135 1 01/22/2020 16:40 WG1415264
Benzene ND 0.00108 1 01/22/2020 16:40 WG1415264
Bromobenzene ND 0.0135 1 01/22/2020 16:40 WG1415264
Bromodichloromethane ND 0.00271 1 01/22/2020 16:40 WG1415264
Bromoform ND 0.0271 1 01/22/2020 16:40 WG1415264
Bromomethane ND 0.0135 1 01/22/2020 16:40 WG1415264
n-Butylbenzene ND 0.0135 1 01/22/2020 16:40 WG1415264
sec-Butylbenzene ND 0.0135 1 01/22/2020 16:40 WG1415264
tert-Butylbenzene ND 0.00542 1 01/22/2020 16:40 WG1415264
Carbon tetrachloride ND 0.00542 1 01/22/2020 16:40 WG1415264
Chlorobenzene ND 0.00271 1 01/22/2020 16:40 WG1415264
Chlorodibromomethane ND 0.00271 1 01/22/2020 16:40 WG1415264
Chloroethane ND 0.00542 1 01/22/2020 16:40 WG1415264
Chloroform ND 0.00271 1 01/22/2020 16:40 WG1415264
Chloromethane ND 0.0135 1 01/22/2020 16:40 WG1415264
2-Chlorotoluene ND 0.00271 1 01/22/2020 16:40 WG1415264
4-Chlorotoluene ND 0.00542 1 01/22/2020 16:40 WG1415264
1,2-Dibromo-3-Chloropropane ND 0.0271 1 01/22/2020 16:40 WG1415264
1,2-Dibromoethane ND 0.00271 1 01/22/2020 16:40 WG1415264
Dibromomethane ND 0.00542 1 01/22/2020 16:40 WG1415264
1,2-Dichlorobenzene ND 0.00542 1 01/22/2020 16:40 WG1415264
1,3-Dichlorobenzene ND 0.00542 1 01/22/2020 16:40 WG1415264
1,4-Dichlorobenzene ND 0.00542 1 01/22/2020 16:40 WG1415264
Dichlorodifluoromethane ND 0.00271 1 01/22/2020 16:40 WG1415264
1,1-Dichloroethane ND 0.00271 1 01/22/2020 16:40 WG1415264
1,2-Dichloroethane ND 0.00271 1 01/22/2020 16:40 WG1415264
1,1-Dichloroethene ND 0.00271 1 01/22/2020 16:40 WG1415264
cis-1,2-Dichloroethene ND 0.00271 1 01/22/2020 16:40 WG1415264
trans-1,2-Dichloroethene ND 0.00542 1 01/22/2020 16:40 WG1415264
1,2-Dichloropropane ND 0.00542 1 01/22/2020 16:40 WG1415264
1,1-Dichloropropene ND 0.00271 1 01/22/2020 16:40 WG1415264
1,3-Dichloropropane ND 0.00542 1 01/22/2020 16:40 WG1415264
cis-1,3-Dichloropropene ND 0.00271 1 01/22/2020 16:40 WG1415264
trans-1,3-Dichloropropene ND 0.00542 1 01/22/2020 16:40 WG1415264
2,2-Dichloropropane ND 0.00271 1 01/22/2020 16:40 WG1415264
Di-isopropyl ether ND 0.00108 1 01/22/2020 16:40 WG1415264
Ethylbenzene ND 0.00271 1 01/22/2020 16:40 WG1415264
Hexachloro-1,3-butadiene ND 0.0271 1 01/22/2020 16:40 WG1415264
Isopropylbenzene ND 0.00271 1 01/22/2020 16:40 WG1415264
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L1181391
MW-1 (15-16)
Collected date/time: 01/16/20 18:00
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
p-Isopropyltoluene ND 0.00542 1 01/22/2020 16:40 WG1415264
2-Butanone (MEK)ND 0.0271 1 01/22/2020 16:40 WG1415264
Methylene Chloride ND 0.0271 1 01/22/2020 16:40 WG1415264
4-Methyl-2-pentanone (MIBK)ND 0.0271 1 01/22/2020 16:40 WG1415264
Methyl tert-butyl ether ND 0.00108 1 01/22/2020 16:40 WG1415264
Naphthalene ND 0.0135 1 01/22/2020 16:40 WG1415264
n-Propylbenzene ND 0.00542 1 01/22/2020 16:40 WG1415264
Styrene ND 0.0135 1 01/22/2020 16:40 WG1415264
1,1,1,2-Tetrachloroethane ND 0.00271 1 01/22/2020 16:40 WG1415264
1,1,2,2-Tetrachloroethane ND 0.00271 1 01/22/2020 16:40 WG1415264
1,1,2-Trichlorotrifluoroethane ND 0.00271 1 01/22/2020 16:40 WG1415264
Tetrachloroethene ND 0.00271 1 01/22/2020 16:40 WG1415264
Toluene ND 0.00542 1 01/22/2020 16:40 WG1415264
1,2,3-Trichlorobenzene ND 0.0135 1 01/22/2020 16:40 WG1415264
1,2,4-Trichlorobenzene ND 0.0135 1 01/22/2020 16:40 WG1415264
1,1,1-Trichloroethane ND 0.00271 1 01/22/2020 16:40 WG1415264
1,1,2-Trichloroethane ND 0.00271 1 01/22/2020 16:40 WG1415264
Trichloroethene ND 0.00108 1 01/22/2020 16:40 WG1415264
Trichlorofluoromethane ND 0.00271 1 01/22/2020 16:40 WG1415264
1,2,3-Trichloropropane ND 0.0135 1 01/22/2020 16:40 WG1415264
1,2,4-Trimethylbenzene ND 0.00542 1 01/22/2020 16:40 WG1415264
1,2,3-Trimethylbenzene ND 0.00542 1 01/22/2020 16:40 WG1415264
Vinyl chloride ND 0.00271 1 01/22/2020 16:40 WG1415264
1,3,5-Trimethylbenzene ND 0.00542 1 01/22/2020 16:40 WG1415264
Xylenes, Total ND 0.00704 1 01/22/2020 16:40 WG1415264
(S) Toluene-d8 98.4 75.0-131 01/22/2020 16:40 WG1415264
(S) 4-Bromofluorobenzene 102 67.0-138 01/22/2020 16:40 WG1415264
(S) 1,2-Dichloroethane-d4 93.6 70.0-130 01/22/2020 16:40 WG1415264
TPH by Method MADEPE
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Unadjusted C9-C18 Aliphatics 10.5 7.04 1 01/23/2020 21:57 WG1415374
Unadjusted C19-C36 Aliphatics 7.94 7.04 1 01/23/2020 21:57 WG1415374
Unadjusted C11-C22 Aromatics 9.40 7.04 1 01/23/2020 23:08 WG1415374
Unadjusted Total Petroleum
Hydrocarbons 27.9 7.04 1 01/23/2020 23:08 WG1415374
(S) o-Terphenyl 75.8 40.0-140 01/23/2020 23:08 WG1415374
(S) 1-Chloro-octadecane 81.6 40.0-140 01/23/2020 21:57 WG1415374
(S) 2-Fluorobiphenyl 92.9 40.0-140 01/23/2020 23:08 WG1415374
(S) 2-Bromonaphthalene 88.5 40.0-140 01/23/2020 23:08 WG1415374
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0361 1 01/24/2020 02:37 WG1416103
Acenaphthylene ND 0.0361 1 01/24/2020 02:37 WG1416103
Anthracene ND 0.0361 1 01/24/2020 02:37 WG1416103
Benzidine ND 0.361 1 01/24/2020 02:37 WG1416103
Benzo(a)anthracene ND 0.0361 1 01/24/2020 02:37 WG1416103
Benzo(b)fluoranthene ND 0.0361 1 01/24/2020 02:37 WG1416103
Benzo(k)fluoranthene ND 0.0361 1 01/24/2020 02:37 WG1416103
Benzo(g,h,i)perylene ND 0.0361 1 01/24/2020 02:37 WG1416103
Benzo(a)pyrene ND 0.0361 1 01/24/2020 02:37 WG1416103
Bis(2-chlorethoxy)methane ND 0.361 1 01/24/2020 02:37 WG1416103
Bis(2-chloroethyl)ether ND 0.361 1 01/24/2020 02:37 WG1416103
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
ATC Group Services - NC Pilot 6955-605-13 L1181391 01/28/20 08:24 9 of 28
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L1181391
MW-1 (15-16)
Collected date/time: 01/16/20 18:00
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
2,2-Oxybis(1-Chloropropane)ND 0.361 1 01/24/2020 02:37 WG1416103
4-Bromophenyl-phenylether ND 0.361 1 01/24/2020 02:37 WG1416103
2-Chloronaphthalene ND 0.0361 1 01/24/2020 02:37 WG1416103
4-Chlorophenyl-phenylether ND 0.361 1 01/24/2020 02:37 WG1416103
Chrysene ND 0.0361 1 01/24/2020 02:37 WG1416103
Dibenz(a,h)anthracene ND 0.0361 1 01/24/2020 02:37 WG1416103
3,3-Dichlorobenzidine ND 0.361 1 01/24/2020 02:37 WG1416103
2,4-Dinitrotoluene ND 0.361 1 01/24/2020 02:37 WG1416103
2,6-Dinitrotoluene ND 0.361 1 01/24/2020 02:37 WG1416103
Fluoranthene ND 0.0361 1 01/24/2020 02:37 WG1416103
Fluorene ND 0.0361 1 01/24/2020 02:37 WG1416103
Hexachlorobenzene ND 0.361 1 01/24/2020 02:37 WG1416103
Hexachloro-1,3-butadiene ND 0.361 1 01/24/2020 02:37 WG1416103
Hexachlorocyclopentadiene ND 0.361 1 01/24/2020 02:37 WG1416103
Hexachloroethane ND 0.361 1 01/24/2020 02:37 WG1416103
Indeno(1,2,3-cd)pyrene ND 0.0361 1 01/24/2020 02:37 WG1416103
Isophorone ND 0.361 1 01/24/2020 02:37 WG1416103
Naphthalene ND 0.0361 1 01/24/2020 02:37 WG1416103
Nitrobenzene ND 0.361 1 01/24/2020 02:37 WG1416103
n-Nitrosodimethylamine ND 0.361 1 01/24/2020 02:37 WG1416103
n-Nitrosodiphenylamine ND 0.361 1 01/24/2020 02:37 WG1416103
n-Nitrosodi-n-propylamine ND 0.361 1 01/24/2020 02:37 WG1416103
Phenanthrene ND 0.0361 1 01/24/2020 02:37 WG1416103
Benzylbutyl phthalate ND 0.361 1 01/24/2020 02:37 WG1416103
Bis(2-ethylhexyl)phthalate ND 0.361 1 01/24/2020 02:37 WG1416103
Di-n-butyl phthalate ND 0.361 1 01/24/2020 02:37 WG1416103
Diethyl phthalate ND 0.361 1 01/24/2020 02:37 WG1416103
Dimethyl phthalate ND 0.361 1 01/24/2020 02:37 WG1416103
Di-n-octyl phthalate ND 0.361 1 01/24/2020 02:37 WG1416103
Pyrene ND 0.0361 1 01/24/2020 02:37 WG1416103
1,2,4-Trichlorobenzene ND 0.361 1 01/24/2020 02:37 WG1416103
4-Chloro-3-methylphenol ND 0.361 1 01/24/2020 02:37 WG1416103
2-Chlorophenol ND 0.361 1 01/24/2020 02:37 WG1416103
2,4-Dichlorophenol ND 0.361 1 01/24/2020 02:37 WG1416103
2,4-Dimethylphenol ND 0.361 1 01/24/2020 02:37 WG1416103
4,6-Dinitro-2-methylphenol ND 0.361 1 01/24/2020 02:37 WG1416103
2,4-Dinitrophenol ND 0.361 1 01/24/2020 02:37 WG1416103
2-Nitrophenol ND 0.361 1 01/24/2020 02:37 WG1416103
4-Nitrophenol ND 0.361 1 01/24/2020 02:37 WG1416103
Pentachlorophenol ND 0.361 1 01/24/2020 02:37 WG1416103
Phenol ND 0.361 1 01/24/2020 02:37 WG1416103
2,4,6-Trichlorophenol ND 0.361 1 01/24/2020 02:37 WG1416103
(S) 2-Fluorophenol 59.6 12.0-120 01/24/2020 02:37 WG1416103
(S) Phenol-d5 54.8 10.0-120 01/24/2020 02:37 WG1416103
(S) Nitrobenzene-d5 45.2 10.0-122 01/24/2020 02:37 WG1416103
(S) 2-Fluorobiphenyl 47.7 15.0-120 01/24/2020 02:37 WG1416103
(S) 2,4,6-Tribromophenol 53.1 10.0-127 01/24/2020 02:37 WG1416103
(S) p-Terphenyl-d14 46.4 10.0-120 01/24/2020 02:37 WG1416103
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L1181391
MW-1 (10-11)
Collected date/time: 01/16/20 17:00
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 87.3 1 01/23/2020 19:10 WG1415317
Volatile Petroleum Hydrocarbons by Method MADEPV
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Unadjusted C5-C8 Aliphatics ND 5.73 1 01/22/2020 15:28 WG1415331
Unadjusted C9-C12 Aliphatics ND 5.73 1 01/22/2020 15:28 WG1415331
Unadjusted C9-C10 Aromatics ND 5.73 1 01/22/2020 15:28 WG1415331
Total VPH ND 5.73 1 01/22/2020 15:28 WG1415331
(S) 2,5-Dibromotoluene(FID)91.2 70.0-130 01/22/2020 15:28 WG1415331
(S) 2,5-Dibromotoluene(PID)89.6 70.0-130 01/22/2020 15:28 WG1415331
TPH by Method MADEPE
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Unadjusted C9-C18 Aliphatics ND 7.45 1 01/23/2020 22:21 WG1415374
Unadjusted C19-C36 Aliphatics ND 7.45 1 01/23/2020 22:21 WG1415374
Unadjusted C11-C22 Aromatics ND 7.45 1 01/23/2020 22:45 WG1415374
Unadjusted Total Petroleum
Hydrocarbons ND 7.45 1 01/23/2020 22:21 WG1415374
(S) o-Terphenyl 65.8 40.0-140 01/23/2020 22:45 WG1415374
(S) 1-Chloro-octadecane 71.2 40.0-140 01/23/2020 22:21 WG1415374
(S) 2-Fluorobiphenyl 96.2 40.0-140 01/23/2020 22:45 WG1415374
(S) 2-Bromonaphthalene 91.0 40.0-140 01/23/2020 22:45 WG1415374
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1415317
Total Solids by Method 2540 G-2011 L1181391-01,02,03
Method Blank (MB)
(MB) R3493709-1 01/23/20 19:10
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.000
L1181365-04 Original Sample (OS) • Duplicate (DUP)
(OS) L1181365-04 01/23/20 19:10 • (DUP) R3493709-3 01/23/20 19:10
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 88.8 89.6 1 0.862 10
Laboratory Control Sample (LCS)
(LCS) R3493709-2 01/23/20 19:10
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 49.9 99.9 85.0-115
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1415331
Volatile Petroleum Hydrocarbons by Method MADEPV L1181391-01,02,03
Method Blank (MB)
(MB) R3494411-3 01/22/20 13:31
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Unadjusted C5-C8 Aliphatics 1.88 J 1.67 5.00
Unadjusted C9-C12 Aliphatics U 1.67 5.00
Unadjusted C9-C10 Aromatics U 1.67 5.00
Total VPH U 1.67 5.00
(S) 2,5-Dibromotoluene(FID)80.6 70.0-130
(S) 2,5-Dibromotoluene(PID)79.3 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3494411-1 01/22/20 09:58 • (LCSD) R3494411-2 01/22/20 10:32
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Unadjusted C5-C8 Aliphatics 60.0 58.6 57.4 97.7 95.7 70.0-130 2.07 25
Unadjusted C9-C12 Aliphatics 70.0 80.7 77.8 115 111 70.0-130 3.66 25
Unadjusted C9-C10 Aromatics 10.0 11.4 11.2 114 112 70.0-130 1.77 25
Total VPH 140 151 146 108 104 70.0-130 3.37 25
(S) 2,5-Dibromotoluene(FID) 96.7 103 70.0-130
(S) 2,5-Dibromotoluene(PID) 96.3 102 70.0-130
L1181391-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1181391-03 01/22/20 15:28 • (MS) R3494411-4 01/22/20 17:07 • (MSD) R3494411-5 01/22/20 17:39
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Unadjusted C5-C8 Aliphatics 58.4 ND 56.7 64.4 97.1 110 1 70.0-130 12.7 25
Unadjusted C9-C12 Aliphatics 68.2 ND 58.0 66.7 85.0 97.8 1 70.0-130 14.0 25
Unadjusted C9-C10 Aromatics 9.74 ND 7.33 8.89 75.3 91.3 1 70.0-130 19.2 25
Total VPH 136 ND 123 140 89.9 103 1 70.0-130 13.1 25
(S) 2,5-Dibromotoluene(FID) 96.9 95.3 70.0-130
(S) 2,5-Dibromotoluene(PID) 95.3 93.8 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1415264
Volatile Organic Compounds (GC/MS) by Method 8260D L1181391-01,02
Method Blank (MB)
(MB) R3493249-3 01/22/20 10:49
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acetone U 0.0137 0.0250
Acrylonitrile U 0.00190 0.0125
Benzene U 0.000400 0.00100
Bromobenzene U 0.00105 0.0125
Bromodichloromethane U 0.000788 0.00250
Bromoform U 0.00598 0.0250
Bromomethane U 0.00370 0.0125
n-Butylbenzene U 0.00384 0.0125
sec-Butylbenzene U 0.00253 0.0125
tert-Butylbenzene U 0.00155 0.00500
Carbon tetrachloride U 0.00108 0.00500
Chlorobenzene U 0.000573 0.00250
Chlorodibromomethane U 0.000450 0.00250
Chloroethane U 0.00108 0.00500
Chloroform U 0.000415 0.00250
Chloromethane U 0.00139 0.0125
2-Chlorotoluene U 0.000920 0.00250
4-Chlorotoluene U 0.00113 0.00500
1,2-Dibromo-3-Chloropropane U 0.00510 0.0250
1,2-Dibromoethane U 0.000525 0.00250
Dibromomethane U 0.00100 0.00500
1,2-Dichlorobenzene U 0.00145 0.00500
1,3-Dichlorobenzene U 0.00170 0.00500
1,4-Dichlorobenzene U 0.00197 0.00500
Dichlorodifluoromethane U 0.000818 0.00250
1,1-Dichloroethane U 0.000575 0.00250
1,2-Dichloroethane U 0.000475 0.00250
1,1-Dichloroethene U 0.000500 0.00250
cis-1,2-Dichloroethene U 0.000690 0.00250
trans-1,2-Dichloroethene U 0.00143 0.00500
1,2-Dichloropropane U 0.00127 0.00500
1,1-Dichloropropene U 0.000700 0.00250
1,3-Dichloropropane U 0.00175 0.00500
cis-1,3-Dichloropropene U 0.000678 0.00250
trans-1,3-Dichloropropene U 0.00153 0.00500
2,2-Dichloropropane U 0.000793 0.00250
Di-isopropyl ether U 0.000350 0.00100
Ethylbenzene U 0.000530 0.00250
Hexachloro-1,3-butadiene U 0.0127 0.0250
Isopropylbenzene U 0.000863 0.00250
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1415264
Volatile Organic Compounds (GC/MS) by Method 8260D L1181391-01,02
Method Blank (MB)
(MB) R3493249-3 01/22/20 10:49
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
p-Isopropyltoluene U 0.00233 0.00500
2-Butanone (MEK)0.0222 J 0.0125 0.0250
Methylene Chloride U 0.00664 0.0250
4-Methyl-2-pentanone (MIBK)U 0.0100 0.0250
Methyl tert-butyl ether U 0.000295 0.00100
Naphthalene U 0.00312 0.0125
n-Propylbenzene U 0.00118 0.00500
Styrene U 0.00273 0.0125
1,1,1,2-Tetrachloroethane U 0.000500 0.00250
1,1,2,2-Tetrachloroethane U 0.000390 0.00250
Tetrachloroethene U 0.000700 0.00250
Toluene U 0.00125 0.00500
1,1,2-Trichlorotrifluoroethane U 0.000675 0.00250
1,2,3-Trichlorobenzene U 0.000625 0.0125
1,2,4-Trichlorobenzene U 0.00482 0.0125
1,1,1-Trichloroethane U 0.000275 0.00250
1,1,2-Trichloroethane U 0.000883 0.00250
Trichloroethene U 0.000400 0.00100
Trichlorofluoromethane U 0.000500 0.00250
1,2,3-Trichloropropane U 0.00510 0.0125
1,2,3-Trimethylbenzene U 0.00115 0.00500
1,2,4-Trimethylbenzene U 0.00116 0.00500
1,3,5-Trimethylbenzene U 0.00108 0.00500
Vinyl chloride U 0.000683 0.00250
Xylenes, Total U 0.00478 0.00650
(S) Toluene-d8 98.8 75.0-131
(S) 4-Bromofluorobenzene 99.7 67.0-138
(S) 1,2-Dichloroethane-d4 92.8 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3493249-1 01/22/20 09:31 • (LCSD) R3493249-2 01/22/20 09:51
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Acetone 0.625 0.386 0.544 61.8 87.0 10.0-160 J3 34.0 31
Acrylonitrile 0.625 0.695 0.560 111 89.6 45.0-153 21.5 22
Benzene 0.125 0.136 0.138 109 110 70.0-123 1.46 20
Bromobenzene 0.125 0.123 0.122 98.4 97.6 73.0-121 0.816 20
Bromodichloromethane 0.125 0.133 0.131 106 105 73.0-121 1.52 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1415264
Volatile Organic Compounds (GC/MS) by Method 8260D L1181391-01,02
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3493249-1 01/22/20 09:31 • (LCSD) R3493249-2 01/22/20 09:51
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Bromoform 0.125 0.116 0.116 92.8 92.8 64.0-132 0.000 20
Bromomethane 0.125 0.106 0.104 84.8 83.2 56.0-147 1.90 20
n-Butylbenzene 0.125 0.148 0.146 118 117 68.0-135 1.36 20
sec-Butylbenzene 0.125 0.133 0.134 106 107 74.0-130 0.749 20
tert-Butylbenzene 0.125 0.132 0.129 106 103 75.0-127 2.30 20
Carbon tetrachloride 0.125 0.125 0.119 100 95.2 66.0-128 4.92 20
Chlorobenzene 0.125 0.126 0.126 101 101 76.0-128 0.000 20
Chlorodibromomethane 0.125 0.119 0.120 95.2 96.0 74.0-127 0.837 20
Chloroethane 0.125 0.0916 0.0959 73.3 76.7 61.0-134 4.59 20
Chloroform 0.125 0.126 0.128 101 102 72.0-123 1.57 20
Chloromethane 0.125 0.110 0.109 88.0 87.2 51.0-138 0.913 20
2-Chlorotoluene 0.125 0.129 0.129 103 103 75.0-124 0.000 20
4-Chlorotoluene 0.125 0.135 0.135 108 108 75.0-124 0.000 20
1,2-Dibromo-3-Chloropropane 0.125 0.105 0.105 84.0 84.0 59.0-130 0.000 20
1,2-Dibromoethane 0.125 0.130 0.134 104 107 74.0-128 3.03 20
Dibromomethane 0.125 0.135 0.126 108 101 75.0-122 6.90 20
1,2-Dichlorobenzene 0.125 0.126 0.126 101 101 76.0-124 0.000 20
1,3-Dichlorobenzene 0.125 0.140 0.134 112 107 76.0-125 4.38 20
1,4-Dichlorobenzene 0.125 0.129 0.129 103 103 77.0-121 0.000 20
Dichlorodifluoromethane 0.125 0.138 0.137 110 110 43.0-156 0.727 20
1,1-Dichloroethane 0.125 0.113 0.113 90.4 90.4 70.0-127 0.000 20
1,2-Dichloroethane 0.125 0.133 0.132 106 106 65.0-131 0.755 20
1,1-Dichloroethene 0.125 0.118 0.116 94.4 92.8 65.0-131 1.71 20
cis-1,2-Dichloroethene 0.125 0.106 0.109 84.8 87.2 73.0-125 2.79 20
trans-1,2-Dichloroethene 0.125 0.117 0.120 93.6 96.0 71.0-125 2.53 20
1,2-Dichloropropane 0.125 0.126 0.126 101 101 74.0-125 0.000 20
1,1-Dichloropropene 0.125 0.124 0.119 99.2 95.2 73.0-125 4.12 20
1,3-Dichloropropane 0.125 0.117 0.121 93.6 96.8 80.0-125 3.36 20
cis-1,3-Dichloropropene 0.125 0.126 0.129 101 103 76.0-127 2.35 20
trans-1,3-Dichloropropene 0.125 0.142 0.144 114 115 73.0-127 1.40 20
2,2-Dichloropropane 0.125 0.106 0.102 84.8 81.6 59.0-135 3.85 20
Di-isopropyl ether 0.125 0.112 0.112 89.6 89.6 60.0-136 0.000 20
Ethylbenzene 0.125 0.121 0.120 96.8 96.0 74.0-126 0.830 20
Hexachloro-1,3-butadiene 0.125 0.139 0.144 111 115 57.0-150 3.53 20
Isopropylbenzene 0.125 0.124 0.124 99.2 99.2 72.0-127 0.000 20
p-Isopropyltoluene 0.125 0.147 0.146 118 117 72.0-133 0.683 20
2-Butanone (MEK)0.625 0.540 0.431 86.4 69.0 30.0-160 22.5 24
Methylene Chloride 0.125 0.110 0.117 88.0 93.6 68.0-123 6.17 20
4-Methyl-2-pentanone (MIBK)0.625 0.632 0.619 101 99.0 56.0-143 2.08 20
Methyl tert-butyl ether 0.125 0.131 0.130 105 104 66.0-132 0.766 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1415264
Volatile Organic Compounds (GC/MS) by Method 8260D L1181391-01,02
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3493249-1 01/22/20 09:31 • (LCSD) R3493249-2 01/22/20 09:51
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Naphthalene 0.125 0.115 0.110 92.0 88.0 59.0-130 4.44 20
n-Propylbenzene 0.125 0.130 0.130 104 104 74.0-126 0.000 20
Styrene 0.125 0.118 0.119 94.4 95.2 72.0-127 0.844 20
1,1,1,2-Tetrachloroethane 0.125 0.116 0.119 92.8 95.2 74.0-129 2.55 20
1,1,2,2-Tetrachloroethane 0.125 0.117 0.114 93.6 91.2 68.0-128 2.60 20
Tetrachloroethene 0.125 0.125 0.124 100 99.2 70.0-136 0.803 20
Toluene 0.125 0.114 0.116 91.2 92.8 75.0-121 1.74 20
1,1,2-Trichlorotrifluoroethane 0.125 0.134 0.130 107 104 61.0-139 3.03 20
1,2,3-Trichlorobenzene 0.125 0.109 0.108 87.2 86.4 59.0-139 0.922 20
1,2,4-Trichlorobenzene 0.125 0.127 0.125 102 100 62.0-137 1.59 20
1,1,1-Trichloroethane 0.125 0.124 0.125 99.2 100 69.0-126 0.803 20
1,1,2-Trichloroethane 0.125 0.120 0.121 96.0 96.8 78.0-123 0.830 20
Trichloroethene 0.125 0.131 0.129 105 103 76.0-126 1.54 20
Trichlorofluoromethane 0.125 0.119 0.119 95.2 95.2 61.0-142 0.000 20
1,2,3-Trichloropropane 0.125 0.110 0.109 88.0 87.2 67.0-129 0.913 20
1,2,3-Trimethylbenzene 0.125 0.115 0.114 92.0 91.2 74.0-124 0.873 20
1,2,4-Trimethylbenzene 0.125 0.131 0.131 105 105 70.0-126 0.000 20
1,3,5-Trimethylbenzene 0.125 0.129 0.130 103 104 73.0-127 0.772 20
Vinyl chloride 0.125 0.113 0.109 90.4 87.2 63.0-134 3.60 20
Xylenes, Total 0.375 0.376 0.376 100 100 72.0-127 0.000 20
(S) Toluene-d8 96.3 97.7 75.0-131
(S) 4-Bromofluorobenzene 99.9 100 67.0-138
(S) 1,2-Dichloroethane-d4 102 99.3 70.0-130
L1181569-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1181569-01 01/22/20 19:14 • (MS) R3493249-4 01/22/20 20:13 • (MSD) R3493249-5 01/22/20 20:32
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Acetone 0.962 U 1.59 1.03 165 107 1 10.0-160 J5 J3 42.8 40
Acrylonitrile 0.962 U 1.27 1.36 132 141 1 10.0-160 6.79 40
Benzene 0.192 U 0.162 0.246 84.0 128 1 10.0-149 J3 41.5 37
Bromobenzene 0.192 U 0.149 0.202 77.2 105 1 10.0-156 30.3 38
Bromodichloromethane 0.192 U 0.169 0.223 88.0 116 1 10.0-143 27.5 37
Bromoform 0.192 U 0.172 0.197 89.6 102 1 10.0-146 13.3 36
Bromomethane 0.192 U 0.115 0.175 59.8 91.2 1 10.0-149 J3 41.7 38
n-Butylbenzene 0.192 U 0.175 0.243 91.2 126 1 10.0-160 32.4 40
sec-Butylbenzene 0.192 U 0.162 0.228 84.0 118 1 10.0-159 34.0 39
tert-Butylbenzene 0.192 U 0.152 0.217 79.0 113 1 10.0-156 35.2 39
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1415264
Volatile Organic Compounds (GC/MS) by Method 8260D L1181391-01,02
L1181569-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1181569-01 01/22/20 19:14 • (MS) R3493249-4 01/22/20 20:13 • (MSD) R3493249-5 01/22/20 20:32
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Carbon tetrachloride 0.192 U 0.153 0.243 79.4 126 1 10.0-145 J3 45.6 37
Chlorobenzene 0.192 U 0.152 0.215 79.1 112 1 10.0-152 34.4 39
Chlorodibromomethane 0.192 U 0.157 0.191 81.6 99.2 1 10.0-146 19.5 37
Chloroethane 0.192 U 0.0980 0.163 51.0 84.8 1 10.0-146 J3 49.9 40
Chloroform 0.192 U 0.163 0.231 84.8 120 1 10.0-146 34.4 37
Chloromethane 0.192 U 0.135 0.219 70.3 114 1 10.0-159 J3 47.1 37
2-Chlorotoluene 0.192 U 0.149 0.219 77.4 114 1 10.0-159 38.0 38
4-Chlorotoluene 0.192 U 0.159 0.228 82.4 118 1 10.0-155 35.9 39
1,2-Dibromo-3-Chloropropane 0.192 U 0.165 0.183 85.6 95.2 1 10.0-151 10.6 39
1,2-Dibromoethane 0.192 U 0.189 0.219 98.4 114 1 10.0-148 14.3 34
Dibromomethane 0.192 U 0.186 0.219 96.8 114 1 10.0-147 16.0 35
1,2-Dichlorobenzene 0.192 U 0.163 0.212 84.8 110 1 10.0-155 26.2 37
1,3-Dichlorobenzene 0.192 U 0.165 0.229 85.6 119 1 10.0-153 32.8 38
1,4-Dichlorobenzene 0.192 U 0.154 0.211 80.0 110 1 10.0-151 31.2 38
Dichlorodifluoromethane 0.192 U 0.166 0.289 86.4 150 1 10.0-160 J3 54.1 35
1,1-Dichloroethane 0.192 U 0.135 0.212 70.3 110 1 10.0-147 J3 44.4 37
1,2-Dichloroethane 0.192 U 0.182 0.223 94.4 116 1 10.0-148 20.5 35
1,1-Dichloroethene 0.192 U 0.129 0.222 67.0 115 1 10.0-155 J3 53.0 37
cis-1,2-Dichloroethene 0.192 U 0.140 0.197 72.6 102 1 10.0-149 34.0 37
trans-1,2-Dichloroethene 0.192 U 0.143 0.225 74.3 117 1 10.0-150 J3 44.5 37
1,2-Dichloropropane 0.192 U 0.155 0.222 80.8 115 1 10.0-148 35.1 37
1,1-Dichloropropene 0.192 U 0.135 0.223 70.3 116 1 10.0-153 J3 49.0 35
1,3-Dichloropropane 0.192 U 0.155 0.197 80.8 102 1 10.0-154 23.6 35
cis-1,3-Dichloropropene 0.192 U 0.151 0.205 78.7 106 1 10.0-151 29.9 37
trans-1,3-Dichloropropene 0.192 U 0.174 0.222 90.4 115 1 10.0-148 24.1 37
2,2-Dichloropropane 0.192 U 0.144 0.226 74.6 118 1 10.0-138 J3 44.7 36
Di-isopropyl ether 0.192 U 0.152 0.194 79.2 101 1 10.0-147 24.0 36
Ethylbenzene 0.192 U 0.148 0.219 76.9 114 1 10.0-160 J3 38.6 38
Hexachloro-1,3-butadiene 0.192 U 0.165 0.211 85.6 110 1 10.0-160 24.6 40
Isopropylbenzene 0.192 U 0.153 0.223 79.4 116 1 10.0-155 37.4 38
p-Isopropyltoluene 0.192 U 0.179 0.246 92.8 128 1 10.0-160 31.9 40
2-Butanone (MEK)0.962 0.0286 0.934 1.12 94.1 114 1 10.0-160 18.3 40
Methylene Chloride 0.192 U 0.153 0.223 79.6 116 1 10.0-141 J3 37.2 37
4-Methyl-2-pentanone (MIBK)0.962 U 1.07 1.13 111 117 1 10.0-160 5.05 35
Methyl tert-butyl ether 0.192 U 0.203 0.239 106 124 1 11.0-147 16.0 35
Naphthalene 0.192 U 0.169 0.191 88.0 99.2 1 10.0-160 12.0 36
n-Propylbenzene 0.192 U 0.150 0.220 78.2 114 1 10.0-158 37.6 38
Styrene 0.192 U 0.145 0.202 75.6 105 1 10.0-160 32.4 40
1,1,1,2-Tetrachloroethane 0.192 U 0.155 0.203 80.8 106 1 10.0-149 26.6 39
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1415264
Volatile Organic Compounds (GC/MS) by Method 8260D L1181391-01,02
L1181569-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1181569-01 01/22/20 19:14 • (MS) R3493249-4 01/22/20 20:13 • (MSD) R3493249-5 01/22/20 20:32
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
1,1,2,2-Tetrachloroethane 0.192 U 0.172 0.199 89.6 103 1 10.0-160 14.1 35
Tetrachloroethene 0.192 U 0.137 0.215 71.2 112 1 10.0-156 J3 44.5 39
Toluene 0.192 U 0.130 0.197 67.8 102 1 10.0-156 J3 40.7 38
1,1,2-Trichlorotrifluoroethane 0.192 U 0.165 0.279 85.6 145 1 10.0-160 J3 51.4 36
1,2,3-Trichlorobenzene 0.192 U 0.142 0.182 73.8 94.4 1 10.0-160 24.5 40
1,2,4-Trichlorobenzene 0.192 U 0.162 0.206 84.0 107 1 10.0-160 24.3 40
1,1,1-Trichloroethane 0.192 U 0.150 0.234 78.0 122 1 10.0-144 J3 43.7 35
1,1,2-Trichloroethane 0.192 U 0.159 0.197 82.4 102 1 10.0-160 21.6 35
Trichloroethene 0.192 U 0.153 0.232 79.4 121 1 10.0-156 J3 41.4 38
Trichlorofluoromethane 0.192 U 0.132 0.235 68.4 122 1 10.0-160 J3 56.6 40
1,2,3-Trichloropropane 0.192 U 0.172 0.191 89.6 99.2 1 10.0-156 10.2 35
1,2,3-Trimethylbenzene 0.192 U 0.141 0.189 73.2 98.4 1 10.0-160 29.4 36
1,2,4-Trimethylbenzene 0.192 U 0.160 0.223 83.2 116 1 10.0-160 32.9 36
1,3,5-Trimethylbenzene 0.192 U 0.151 0.217 78.7 113 1 10.0-160 35.6 38
Vinyl chloride 0.192 U 0.140 0.225 72.6 117 1 10.0-160 J3 46.6 37
Xylenes, Total 0.577 U 0.457 0.666 79.2 115 1 10.0-160 37.3 38
(S) Toluene-d8 96.6 96.5 75.0-131
(S) 4-Bromofluorobenzene 106 104 67.0-138
(S) 1,2-Dichloroethane-d4 106 104 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1415374
TPH by Method MADEPE L1181391-01,02,03
Method Blank (MB)
(MB) R3493902-1 01/23/20 18:23
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Unadjusted C9-C18 Aliphatics U 2.17 6.50
Unadjusted C19-C36 Aliphatics U 2.17 6.50
Unadjusted Total Petroleum
Hydrocarbons U 2.17 6.50
(S) 1-Chloro-octadecane 67.9 40.0-140
Method Blank (MB)
(MB) R3493902-4 01/23/20 19:35
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Unadjusted C11-C22 Aromatics U 2.17 6.50
Unadjusted Total Petroleum
Hydrocarbons U 2.17 6.50
(S) o-Terphenyl 62.0 40.0-140
(S) 2-Fluorobiphenyl 82.0 40.0-140
(S) 2-Bromonaphthalene 77.4 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3493902-2 01/23/20 18:47 • (LCSD) R3493902-3 01/23/20 19:11
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Unadjusted C9-C18 Aliphatics 39.9 24.2 22.9 60.7 57.4 40.0-140 5.52 25
Unadjusted C19-C36 Aliphatics 53.2 33.2 33.0 62.4 62.0 40.0-140 0.604 25
(S) 1-Chloro-octadecane 68.8 64.5 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3493902-5 01/23/20 19:58 • (LCSD) R3493902-6 01/23/20 20:22
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Unadjusted C11-C22 Aromatics 113 71.5 85.7 63.3 75.8 40.0-140 18.1 25
(S) o-Terphenyl 62.0 73.1 40.0-140
(S) 2-Fluorobiphenyl 89.5 93.4 40.0-140
(S) 2-Bromonaphthalene 84.2 88.0 40.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1415374
TPH by Method MADEPE L1181391-01,02,03
L1181391-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1181391-01 01/23/20 20:46 • (MS) R3493902-7 01/23/20 21:10 • (MSD) R3493902-8 01/23/20 21:33
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Unadjusted C9-C18 Aliphatics 45.3 ND 24.8 26.9 54.6 59.4 1 40.0-140 8.35 50
Unadjusted C19-C36 Aliphatics 60.5 12.6 36.6 42.0 39.7 48.7 1 40.0-140 J6 13.9 50
(S) 1-Chloro-octadecane 59.8 64.5 40.0-140
L1181391-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1181391-01 01/23/20 20:46 • (MS) R3493902-10 01/23/20 23:56 • (MSD) R3493902-9 01/23/20 23:32
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Unadjusted C11-C22 Aromatics 128 9.84 73.9 103 49.9 72.9 1 40.0-140 33.3 50
(S) o-Terphenyl 52.8 72.9 40.0-140
(S) 2-Fluorobiphenyl 86.3 102 40.0-140
(S) 2-Bromonaphthalene 81.0 95.5 40.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1416103
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1181391-01,02
Method Blank (MB)
(MB) R3493819-2 01/24/20 01:01
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acenaphthene U 0.00642 0.0333
Acenaphthylene U 0.00671 0.0333
Anthracene U 0.00632 0.0333
Benzidine U 0.0637 0.333
Benzo(a)anthracene U 0.00428 0.0333
Benzo(b)fluoranthene U 0.00695 0.0333
Benzo(k)fluoranthene U 0.00582 0.0333
Benzo(g,h,i)perylene U 0.00721 0.0333
Benzo(a)pyrene U 0.00548 0.0333
Bis(2-chlorethoxy)methane U 0.00770 0.333
Bis(2-chloroethyl)ether U 0.00896 0.333
2,2-oxybis(1-chloropropane)U 0.00760 0.333
4-Bromophenyl-phenylether U 0.0114 0.333
2-Chloronaphthalene U 0.00639 0.0333
4-Chlorophenyl-phenylether U 0.00627 0.333
Chrysene U 0.00555 0.0333
Dibenz(a,h)anthracene U 0.00821 0.0333
3,3-Dichlorobenzidine U 0.0794 0.333
2,4-Dinitrotoluene U 0.00607 0.333
2,6-Dinitrotoluene U 0.00737 0.333
Fluoranthene U 0.00496 0.0333
Fluorene U 0.00682 0.0333
Hexachlorobenzene U 0.00856 0.333
Hexachloro-1,3-butadiene U 0.0100 0.333
Hexachlorocyclopentadiene U 0.0587 0.333
Hexachloroethane U 0.0134 0.333
Indeno(1,2,3-cd)pyrene U 0.00772 0.0333
Isophorone U 0.00522 0.333
Naphthalene U 0.00889 0.0333
Nitrobenzene U 0.00695 0.333
n-Nitrosodimethylamine U 0.0647 0.333
n-Nitrosodiphenylamine U 0.0900 0.333
n-Nitrosodi-n-propylamine U 0.00906 0.333
Phenanthrene U 0.00528 0.0333
Benzylbutyl phthalate U 0.0103 0.333
Bis(2-ethylhexyl)phthalate U 0.0120 0.333
Di-n-butyl phthalate U 0.0109 0.333
Diethyl phthalate U 0.00691 0.333
Dimethyl phthalate U 0.00540 0.333
Di-n-octyl phthalate U 0.00907 0.333
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1416103
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1181391-01,02
Method Blank (MB)
(MB) R3493819-2 01/24/20 01:01
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Pyrene U 0.0123 0.0333
1,2,4-Trichlorobenzene U 0.00876 0.333
4-Chloro-3-methylphenol U 0.00477 0.333
2-Chlorophenol U 0.00831 0.333
2,4-Dichlorophenol U 0.00746 0.333
2,4-Dimethylphenol U 0.0471 0.333
4,6-Dinitro-2-methylphenol U 0.124 0.333
2,4-Dinitrophenol U 0.0980 0.333
2-Nitrophenol U 0.0130 0.333
4-Nitrophenol U 0.0525 0.333
Pentachlorophenol U 0.0480 0.333
Phenol U 0.00695 0.333
2,4,6-Trichlorophenol U 0.00779 0.333
(S) Nitrobenzene-d5 55.6 10.0-122
(S) 2-Fluorobiphenyl 58.6 15.0-120
(S) p-Terphenyl-d14 61.6 10.0-120
(S) Phenol-d5 59.2 10.0-120
(S) 2-Fluorophenol 64.0 12.0-120
(S) 2,4,6-Tribromophenol 62.9 10.0-127
Laboratory Control Sample (LCS)
(LCS) R3493819-1 01/24/20 00:42
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Acenaphthene 0.666 0.336 50.5 38.0-120
Acenaphthylene 0.666 0.355 53.3 40.0-120
Anthracene 0.666 0.345 51.8 42.0-120
Benzidine 1.33 0.194 14.6 10.0-120
Benzo(a)anthracene 0.666 0.372 55.9 44.0-120
Benzo(b)fluoranthene 0.666 0.350 52.6 43.0-120
Benzo(k)fluoranthene 0.666 0.350 52.6 44.0-120
Benzo(g,h,i)perylene 0.666 0.349 52.4 43.0-120
Benzo(a)pyrene 0.666 0.374 56.2 45.0-120
Bis(2-chlorethoxy)methane 0.666 0.283 42.5 20.0-120
Bis(2-chloroethyl)ether 0.666 0.340 51.1 16.0-120
2,2-Oxybis(1-Chloropropane)0.666 0.320 48.0 23.0-120
4-Bromophenyl-phenylether 0.666 0.360 54.1 40.0-120
2-Chloronaphthalene 0.666 0.338 50.8 35.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1416103
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1181391-01,02
Laboratory Control Sample (LCS)
(LCS) R3493819-1 01/24/20 00:42
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
4-Chlorophenyl-phenylether 0.666 0.359 53.9 40.0-120
Chrysene 0.666 0.345 51.8 43.0-120
Dibenz(a,h)anthracene 0.666 0.350 52.6 44.0-120
3,3-Dichlorobenzidine 1.33 0.627 47.1 28.0-120
2,4-Dinitrotoluene 0.666 0.374 56.2 45.0-120
2,6-Dinitrotoluene 0.666 0.380 57.1 42.0-120
Fluoranthene 0.666 0.348 52.3 44.0-120
Fluorene 0.666 0.349 52.4 41.0-120
Hexachlorobenzene 0.666 0.353 53.0 39.0-120
Hexachloro-1,3-butadiene 0.666 0.294 44.1 15.0-120
Hexachlorocyclopentadiene 0.666 0.336 50.5 15.0-120
Hexachloroethane 0.666 0.311 46.7 17.0-120
Indeno(1,2,3-cd)pyrene 0.666 0.364 54.7 45.0-120
Isophorone 0.666 0.284 42.6 23.0-120
Naphthalene 0.666 0.280 42.0 18.0-120
Nitrobenzene 0.666 0.292 43.8 17.0-120
n-Nitrosodimethylamine 0.666 0.297 44.6 10.0-125
n-Nitrosodiphenylamine 0.666 0.358 53.8 40.0-120
n-Nitrosodi-n-propylamine 0.666 0.322 48.3 26.0-120
Phenanthrene 0.666 0.337 50.6 42.0-120
Benzylbutyl phthalate 0.666 0.402 60.4 40.0-120
Bis(2-ethylhexyl)phthalate 0.666 0.392 58.9 41.0-120
Di-n-butyl phthalate 0.666 0.365 54.8 43.0-120
Diethyl phthalate 0.666 0.366 55.0 43.0-120
Dimethyl phthalate 0.666 0.355 53.3 43.0-120
Di-n-octyl phthalate 0.666 0.414 62.2 40.0-120
Pyrene 0.666 0.359 53.9 41.0-120
1,2,4-Trichlorobenzene 0.666 0.284 42.6 17.0-120
4-Chloro-3-methylphenol 0.666 0.338 50.8 28.0-120
2-Chlorophenol 0.666 0.358 53.8 28.0-120
2,4-Dichlorophenol 0.666 0.329 49.4 25.0-120
2,4-Dimethylphenol 0.666 0.301 45.2 15.0-120
4,6-Dinitro-2-methylphenol 0.666 0.306 45.9 16.0-120
2,4-Dinitrophenol 0.666 0.200 30.0 10.0-120
2-Nitrophenol 0.666 0.351 52.7 20.0-120
4-Nitrophenol 0.666 0.349 52.4 27.0-120
Pentachlorophenol 0.666 0.285 42.8 29.0-120
Phenol 0.666 0.349 52.4 28.0-120
2,4,6-Trichlorophenol 0.666 0.409 61.4 37.0-120
(S) Nitrobenzene-d5 42.6 10.0-122
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1416103
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1181391-01,02
Laboratory Control Sample (LCS)
(LCS) R3493819-1 01/24/20 00:42
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
(S) 2-Fluorobiphenyl 52.3 15.0-120
(S) p-Terphenyl-d14 53.5 10.0-120
(S) Phenol-d5 54.1 10.0-120
(S) 2-Fluorophenol 58.3 12.0-120
(S) 2,4,6-Tribromophenol 60.7 10.0-127
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
(dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils].
MDL Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
RDL (dry)Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
J The identification of the analyte is acceptable; the reported value is an estimate.
J3 The associated batch QC was outside the established quality control range for precision.
J5 The sample matrix interfered with the ability to make any accurate determination; spike value is high.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing
turn-around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National.

State Accreditations
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN-03-2002-34
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹n/a
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶90010 South Carolina 84004
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana ¹LA180010 Texas T104704245-18-15
Maine TN0002 Texas ⁵LAB0152
Maryland 324 Utah TN00003
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 460132
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 9980939910
Montana CERT0086 Wyoming A2LA

Third Party Federal Accreditations
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable

Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contactour main office. Pace National performs all testing at our central laboratory.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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