WS-9571_44769_CA_LSA_20170217

1818 Perimeter Road • Dawsonville, GA 30534
706-579-1607 PHONE • 1-706-265-4916 FAX • www.millcreekenvironmental.com
February 16, 2017

North Carolina Department of Environment Quality
450 Hanes Mill Road, Suite 300
Winston-Salem, North Carolina 27105

Attn: Ms. Carin Kromm, Regional Supervisor, UST Section
[e-mail]

Subject: Limited Site Assessment
Nick’s Motor Cars
3384 West US Highway 421
Wilkesboro, Wilkes County, North Carolina 28697
Dear Ms. Kromm,
Mill Creek Environmental, LLC (MCE) has completed a Limited Site Assessment (LSA) for the subject
property. The purpose of this LSA is to further characterize the extent and magnitude of a petroleum
release that was detected during the closure of three (3) 4,000 gallon petroleum underground storage tanks
(USTs) in October, 2016. The LSA is being conducted to met the requirements of North Carolina
Department of Environmental Quality Rule 15A NCAC 02L .0505. During the LSA, one (1) soil boring
was completed, soils were screened for volatile organic vapors using a photoionization detector (PID),
and three (3) soil samples were submitted for laboratory analysis. The results of our investigation
revealed the following:
 Groundwater was not encountered in the soil boring;
 Benzene was detected in soil sample SB-1, 48-50’ at a concentration that exceeds the Soil-to-
Water Maximum Contaminant Concentration (MSCC) by 0.0001 milligram per kilogram;
 Soil contamination does not exceed the residential MSCC; and
 The petroleum release does not pose a threat of explosion due the accumulation of vapors in a
confined space nor does the release pose a risk to public health or the environment.
MCE recommends a “No Further Action Required” (NFA) status for this site based on the data collected
during this Limited Site Assessment.
If you have any questions, or if MCE can be of assistance in any other capacity, please don’t hesitate to
call the undersigned at 706-579-1607.
Sincerely,
MILL CREEK ENVIRONMENTAL, LLC

Ryan Phillippie Dan Centofanti, PG, EP
Project Geologist Technical Director

1818 Perimeter Road • Dawsonville, GA 30534
706-579-1607 PHONE • 1-706-265-4916 FAX • www.millcreekenvironmental.com

Limited Site Assessment
of:
Nick’s Motor Cars
3384 West US Highway 421
Wilkesboro, North Carolina 28697

Prepared for:

Nick’s Motor Cars
3384 West US Highway 421
Wilkesboro, North Carolina 28697

Prepared by:

Mill Creek Environmental, LLC
1818 Perimeter Road
Dawsonville, Georgia 30534
MCES Project # NAC-1701-1

Feburary 2017
Limited Site Assessment
Nick’s Motor Cars
3384 West US Highway 421, Wilkesboro, NC
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P:\Nicks Motor Cars\NAC-1701-1\LSA\Report February 16, 2017

TABLE OF CONTENTS

1 CERTIFICATION ............................................................................................................................. 2 
2 INTRODUCTION .............................................................................................................................. 3 
2.1 PURPOSE ........................................................................................................................................... 3 
2.2 SCOPE OF WORK .............................................................................................................................. 3 
2.3 LIMITATIONS .................................................................................................................................... 3 
3 SITE DESCRIPTION ........................................................................................................................ 4 
4 RECEPTOR INFORMATION ......................................................................................................... 4 
4.1 PUBLIC AND PRIVATE WATER SUPPLY WELLS ................................................................................ 4 
4.2 SURFACE WATER ............................................................................................................................. 5 
5 SOILS AND GEOLOGY ................................................................................................................... 5 
6 SUBSURFACE INVESTIGATION PROCEDURES ..................................................................... 5 
6.1 SUBSURFACE INVESTIGATION METHODOLOGY ............................................................................... 5 
6.2 BORING LOCATION RATIONALE....................................................................................................... 5 
6.3 SOIL SAMPLING PROCEDURES ......................................................................................................... 6 
7 SUBSURFACE INVESTIGATION RESULTS ............................................................................... 6 
7.1 SOIL SAMPLE ANALYTICAL RESULTS .............................................................................................. 6 
8 CONCLUSIONS AND RECOMMENDATIONS ........................................................................... 6 

LIST OF FIGURES

Figure 1 Site Vicinity Map
Figure 2 Soil Boring Location and Data Summary Map

LIST OF TABLES

Table 1a: Site History – UST System and Other Release Information
Table 1b: Site History – UST Owner and Responsible Party Information
Table 2 Soil Analytical Results Summary (VOCs)
Table 3 Soil Analytical Results Summary (EPH)

LIST OF APPENDICES

Appendix A Initial Abatement Action Report
Appendix B LSA Risk Classification and Land Use
Appendix C Boring Log
Appendix D Laboratory Analytical Report
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3384 West US Highway 421, Wilkesboro, NC
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1 CERTIFICATION
We have performed this Assessment in accordance with generally accepted environmental practices
and procedures as of the date of this report. We have employed the degree of care and skill
ordinarily exercised under similar circumstances by reputable environmental professionals
practicing in this area. The conclusions contained within this assessment are based upon site
conditions we readily observed or were reasonably ascertainable and present at the time of the site
inspection, reasonably ascertainable regulatory information, and reasonably ascertainable historical
information.
The scope of this assessment does not purport to encompass every report, record, or other form of
documentation relevant to the property being evaluated. To the best of our knowledge, this
subsurface investigation has been performed in compliance with ASTM Standard E1903-11 for
Phase II Environmental Site Assessments.
We declare that we meet the definition of Environmental Professional as defined in §312.10 of
40 CFR 312 and we have the specific qualifications based on education, training, and experience
to assess a property of the nature, history, and setting of the subject property.

Prepared By: Directed and Reviewed By:

Ryan Phillippie Dan Centofanti, PG, EP
Project Geologist Technical Director

Limited Site Assessment
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3384 West US Highway 421, Wilkesboro, NC
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Mill Creek Environmental, LLC (MCE) has completed a Limited Site Assessment (LSA) of the
former gas station located at 3384 West US Highway 421 in Wilkesboro, Wilkes County, North
Carolina. This investigation was performed at the request of Mr. Nick Wehrmann. All tasks
were completed in general accordance with the American Society for Testing and Materials
(ASTM) Standard Practice E 1903-11.
2.1 Purpose
The purpose of this LSA is to further characterize the extent and magnitude of a petroleum
release that was detected during the closure of three (3) 4,000 gallon petroleum underground
storage tanks (USTs) in October, 2016. The LSA is being conducted to met the requirements of
North Carolina Department of Environmental Quality (NDDEQ) Rule 15A NCAC 02L .0505.
2.2 Scope of Work
The scope of this investigation was directed specifically to address the potential for soil or
groundwater contamination resulting from the release identified during the October 2016 tank
closure at the subject property. The following tasks were completed for this investigation:
 TASK 1- One (1) soil boring was completed at the subject property to a depth of 50
feet below ground surface (BGS).
 TASK 2- Headspace vapor analysis was conducted on soil samples from the
borehole at five-foot intervals from 0 to 30 feet and at two-foot intervals
from 30 to 50 feet to determine if volatile organic vapors were present;
 TASK 3- Soil samples were collected from the soil boring and submitted for
laboratory analysis; and,
 TASK 4- This report was prepared to document MCE’s findings and offer
recommendations for further action as needed to address site conditions.
All work was completed under the direction of a North Carolina Professional Geologist.
2.3 Limitations
The report and any other information which MCE prepared and submitted to Mr. Nick
Wehrmann of Nick Motor Cars, (the user), in connection with this project (the “Report”), are for
the sole use and benefit of the user and may not be used or relied upon by any other person or
entity without the prior written consent of the user and MCE, except as provided for specifically
in the agreement. Any such consent given by MCE will be deemed to be and will be subject to
the terms and conditions as MCE may reasonably require, including without limitation a
monetary limit to MCE’ liability to any person granted such consent (the “Grantee”), and any
such Grantee will be deemed to have agreed to such terms and conditions by its use and reliance
2 INTRODUCTION
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3384 West US Highway 421, Wilkesboro, NC
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on the Report. The use or re-use of this document or the findings, conclusions, or
recommendations presented herein, by any other party or parties is at the sole risk of said users.
MCE and the user agree that (1) the information in the Report relates only to the property
specifically described in the Report and was presented in accordance with and subject to the
scope of work described in the Report or specifically agreed to by MCE and the user; (2) the
information and conclusions provided in the Report apply only to the subject property as it
existed at the time of MCE’s site examination. Should site use or conditions change or should
there be changes in applicable laws, standards, or technology, the information and conclusions in
the Report may no longer apply; (3) MCE makes no representations regarding the value or
marketability of this property or its suitability for any particular use, and none should be inferred
based on the Report; (4) the Report is intended to be used in its entirety and no excerpts may be
taken to be representative of the findings of this investigation; and (5) environmental land-use
issues and constraints of possible relevance (e.g., wetland surveys, sensitive habitats, radon, lead
paint, asbestos, etc.), were not included in this scope of services.
3 SITE DESCRIPTION
The subject property is located in a residential and commercial area of Wilkesboro, North
Carolina. The Wilkes County Tax Assessors Office identifies the subject property as Parcel ID
1505745, totaling 1.25-acres. Ground cover at the subject property is concrete, asphalt, gravel,
and bare soil. The subject property is currently a Meineke auto shop. Three (3) steel 4,000 gallon
petroleum USTs were removed from the subject property by Seramur & Associates between
October 11 and October 13, 2016. During removal of the USTs, small holes were observed on
the bottoms and sides of the tanks. Gasoline and diesel range organic compounds were detected
in the soils beneath each tank. According to an Initial Abatement Action Report completed by
Seramur & Associates, the USTs removed from the subject property were installed as early as
the 1950s and were not registered. A Site Location Map is provided as Figure 1. A summary of
the site history is presented in Table 1a and 1b. The Initial Abatement Action Report for the
release is provided in Appendix A.
4 RECEPTOR INFORMATION
4.1 Public and Private Water Supply Wells
MCE conducted a well survey to identify public and private water supply wells within 1,500 feet
of the subject property. MCE identified one (1) private water supply well located approximately
425 feet to the northwest of the subject property. The well is located at a private residence at
2154 Congo Road. Due to the distance and topographically up-gradient position of the well from
the subject property, the probability this water supply well being impacted by the release at the
subject property is low. MCE also searched the United States Geological Survey National Water
Information System and found no ground water wells within 1,500 feet of the subject property.
All residents and businesses within the surveyed area are supplied with municipal water.
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4.2 Surface Water
Two (2) surface waters are located within 1,500 feet of the subject property. Millers Creek is
located approximately 1,060 feet to the northeast of the subject property and unnamed tributary
to Yadkin River is located approximately 1,270 feet to the southwest of the subject property.
Due to the distance from the subject property, the release is unlikely to impact these waters.
A Risk Classification and Land Use Form is provided in Appendix B.
5 SITE GEOLOGY AND HYDROGEOLOGY
The subject property is situated in the Piedmont Physiographic Province of North Carolina.
Rock types of the Piedmont generally include gneiss, schist, granite, and amphibolite. These
rocks weather to form a reddish-brown soil called residuum, which consists of various amounts
of sand, clay, and silt mixtures.
The upper boundary of the Piedmont groundwater system is formed by the water table. The
water table is usually situated within the residuum, although it can be found within the bedrock
in areas where the residuum is thin. The configuration of the water table is usually a subdued
replica of the site topography. Generally, groundwater in the Piedmont flows from highlands to
lowlands and discharges to streams, lakes, or wetlands. The direction of groundwater flow at the
subject property is unknown, but based on the topography of the subject property the general
direction of groundwater flow in the area is estimated to be to the northeast.
6 SUBSURFACE INVESTIGATION PROCEDURES
MCE conducted the subsurface investigation at the subject property on January 18, 2017. The
following sections include a summary of the activities completed and a discussion of the results
of our investigation.
6.1 Subsurface Investigation Methodology
On January 18, 2017, a Geoprobe 7822DT drill rig was used to advance a 2.25-inch diameter
boring in one (1) location (SB-1) at the subject property. Continuous soil samples were collected
at five-foot intervals from 0 to 30 feet with a dual-tube sampler and at two-foot intervals from 30
to 50 feet with a split spoon sampler.
6.2 Boring Location Rationale
SB-1 This boring location was chosen to assess conditions in the vicinity of the former
UST basin. Ground cover at this location was concrete and soils in this boring
were primarily classified as clayey fill material grading to banded saprolite.
Soil boring locations are shown on Figure 2. Boring logs are included in Appendix C.
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6.3 Soil Sampling Procedures
A headspace vapor analysis for volatile organic vapors was conducted for each sample interval.
Soil samples were collected for laboratory analysis from the sample intervals based on the
highest PID readings. Based on the absence of groundwater within the boring, an additional soil
sample was collected from the deepest interval within the boring.
Upon completion of the boring, soil samples were placed into laboratory-provided containers,
sealed, labeled, packed on ice, and delivered to Pace Analytical in Huntersville, North Carolina
under standard chain of custody procedures. The soil samples collected were analyzed for
extractable petroleum hydrocarbons (EPH) by Massachusetts Department of Environmental
Protection (MADEP) method EPH, volatile petroleum hydrocarbons by MADEP method VPH,
volatile organic compounds (VOCs) by EPA Method 8260, and semi-volatile organic
compounds (SVOCs) by EPA Method 8270. A total of three (3) soil samples were submitted for
analysis.
7 SUBSURFACE INVESTIGATION RESULTS
7.1 Soil Sample Analytical Results
Laboratory analytical data indicated that the VOC constituent benzene was detected in soil
sample SB-1, 48-50’ at a concentration of 0.0057 milligrams per kilogram (mg/kg). This
concentration exceeds the NCDEQ Maximum Soil Contaminant Concentration (MSCC) levels’
Soil-to-Water Maximum Contaminant Concentration of 0.0056 mg/kg. The VOC constituents
ethylbenzene, n-propylbenzene, toluene, 1,2,4-trimethylbenzene, 1,3,5-trimethylebenzene, and
xylenes were detected in soil sample SB-1, 48-50’ at concentrations below their applicable
MSCC level.
The VOC constituents ethylbenzene, methyl-tert-butyl ether, napthalene, toluene, 1,2,4-
trimethylbenzene, 1,3,5-trimethylebenzene, and xylenes were detected in soil sample SB-1, 38-
40’ at concentrations below their applicable MSCC level.
The EPH constituent aliphatic (C19-C36) was detected in soil sample SB-1, 48-50’ at a
concentration below the applicable MSCC level. Summaries of the VOC and EPH detections
are included in Table 2 and 3. The Laboratory Analytical Report is provided in Appendix D.
MCE has developed the following conclusions based on the results of the LSA investigation:
 Groundwater was not encountered in the soil boring;
 Benzene was detected in soil sample SB-1, 48-50’ at a concentration that exceeds the
Soil-to-Water Maximum Contaminant Concentration by 0.0001 milligram per kilogram;
 Soil contamination does not exceed the residential MSCC; and
8 CONCLUSIONS AND RECOMMENDATIONS
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3384 West US Highway 421, Wilkesboro, NC
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 The petroleum release does not pose a threat of explosion due the accumulation of vapors
in a confined space nor does the release pose a risk to public health or the environment.
MCE recommends a “No Further Action Required” (NFA) status for this site based on the data
collected during this Limited Site Assessment.

Figures

Tables

Table 1a 1 2/16/2017 Table 1a: Site History – UST System and Other Release Information Revision Date: 2/3/2017 Incident Number and Name: Nick’s Motor Cars UST ID Number Current/Last Contents * Previous Contents * Capacity (in gallons) Construction Details Tank Dimensions Description of Associated Piping and Pumps Date Tank Installed Status of UST Was release associated with the UST System? UST 1 Gasoline/ Diesel Gasoline/ Diesel 4,000 Steel 24.0’ x 5.3’ Steel product lines Unknown (1950’s ?) Closed by removal on 10/12/16 Yes UST 2 Gasoline/ Diesel Gasoline/ Diesel 4,000 Steel 24.0’ x 5.3’ Steel product lines Unknown (1950’s ?) Closed by removal on 10/12/16 Yes UST 3 Gasoline/ Diesel Gasoline/ Diesel 4,000 Steel 24.0’ x 5.3’ Steel product lines Unknown (1950’s ?) Closed by removal on 10/13/16 Yes Incident Number Material Released Date of Release Description of Release Unknown Gasoline/ Diesel Discovered 10/11/2016 Petroleum was observed in soil removed from sides and under USTs
Table 1b 2 2/16/2017 Table 1b: Site History - UST Owner and Responsible Party Information Revision Date: 2/3/2016 Incident Number and Name: Nick’s Motor Cars UST ID Number Unregistered Facility ID Number Not Registered Name of Owner: Dates of Operation Unknown. Approx 1950 to 1970 Nicholas J. Wehrmann Not Known Street Address 3357 W. US Highway 421 City State Zip Telephone Number Wilkesboro NC 28697 [phone] Name of Operator Dates of Operation (mm/dd/yy to mm/dd/yy) Tommy Turner (Deceased) Not Known Street Address Not Known City State Zip Telephone Number Not Known NC Not Known Not Known Incident Number N/A Name of Other Responsible Party Dates of Release(s) (mm/dd/yy to mm/dd/yy) N/A N/A Street Address N/A City State Zip Telephone Number N/A N/A N/A N/A
Sample IDDepth (ft/BGS)Benzene (mg/kg)Ethylbenzene (mg/kg)Methyl-tert-butyl ether (mg/kg)Napthalene (mg/kg)n-Propylbenzene (mg/kg)Toluene (mg/kg)1,2,4-Trimethylbenzene (mg/kg)1,3,5-Trimethylebenzene (mg/kg)Total Xylenes (mg/kg)SB-1, 20-25' 20-25 BRL BRL BRL BRL BRL BRL BRL BRL BRLSB-1, 38-40' 38-40 BRL 0.0075 0.0057 0.0066 BRL 0.0223 0.0162 BRL 0.0700SB-1, 48-50' 48-500.00570.0488 BRL BRL 0.0142 0.0723 0.0992 0.0374 0.36600.0056 4.9 0.091 0.16 0.17 4.3 8.5 8.3 4.618 1,560 350 313 626 1,200 782 782 3,129164 40,000 3,100 8,176 16,350 32,000 20,440 20,440 81,760NOTE: VOCs = Volatile Organic Compoundsmg/kg = Milligrams Per KilogramBRL = Below Laboratory Reporting Limitft/BGS = Feet Below Ground Surface TABLE 2: SOIL ANALYTICAL RESULTS SUMMARYNick's Motor Cars3384 West US Highway 421Wilkesboro, North Carolina 28697Industrial / Commerical CLApplicable Standards: NCDEQ Maximum Soil Contaminant Concentration Levels Bold numbers represent a detection in exceedence of applicible standard. Volatile Organic Compounds (VOCs)Date Sampled1/18/2017Soil-to-Water Maximum Contaminant Concentration Residential CL1/18/20171/18/2017Table 2 (VOCs) 1 of 22/17/2017
Sample ID Depth
(ft/BGS)
Aliphatic
(C19-C36)
(mg/kg)
SB-1, 20-25' 20-25 BRL
SB-1, 38-40' 38-40 BRL
SB-1, 48-50' 48-50 74.5
#
31,000
810,000
NOTE: VOCs = Volatile Organic Compounds
mg/kg = Milligrams Per Kilogram
BRL = Below Laboratory Reporting Limit
ft/BGS = Feet Below Ground Surface
# = Health based level > 100%
Bold numbers represent a detection in exceedence of
applicible standard.
1/18/2017
1/18/2017
1/18/2017
Soil-to-Water Maximum
Contaminant Concentration
Residential CL
Industrial / Commerical CL
Applicable Standards:
NCDEQ Maximum Soil
Contaminant
Concentration Levels
TABLE 3: SOIL ANALYTICAL RESULTS SUMMARY
Extractable Petroleum Hydrocarbons
Nick's Motor Cars
3384 West US Highway 421
Wilkesboro, North Carolina 28697
Date Sampled
Table 3 (EPH) 2 of 2 2/17/2017

Appendix A
Initial Abatement Action Report

1
Initial Abatement Action Report

In addition to reporting initial response and abatement actions and assessment actions and presenting initial site
characterization, this newly-created Initial Abatement Action Report must fulfill the requirements, when a release
has been discovered, for the following individual reports: Check the applicable report(s).
__ Site Check Report (Section C)
_X_ UST Closure Report (UST-12) with UST-2 Form (Section D)
_X_ Post-Excavation Soil Contamination Assessment Report (Section H)
___ Free Product Recovery Report (Section E)

A. Site Information
1. Site Identification
Date of Report: 11-11-16
Facility I.D.: Not Registered UST Incident Number (if known): Not Known
Site Name: Nick’s Motor Cars
Site Street Address: 3384 W. US Hwy. 421
City/Town: Wilkesboro Zip Code: 28697 County: Wilkes
Description of Geographical Data Point (e.g., diesel fill port): Building
Location Method (GPS, topographical map, other): Google Earth
Latitude (decimal degrees): 36.150110° N Longitude (decimal degrees): 81.218895 ° W

2. Information about Contacts Associated with the Leaking UST System (Addresses must include street, city,
state, zip code and mailing address, if different)
UST Owner/Operator: Nicholas J. Wehrmann
Address: 3384 W. US Hwy. 421, Wilkesboro, NC 28697 Tel.: [phone]
Property Owner: Same
Address: Same Tel.: Same
Property Occupant: Nicholas J. Wehrmann / Nick’s Motor Cars
Consultant/Contractor: Seramur & Associates, PC
Address: 165 Knoll Drive, Boone, NC 28607 Tel: [phone]
Analytical Laboratory: Prism Labs, Inc. State Certification No. 275
Address: 449 Springbrook Road Charlotte, NC 28217 Tel: [phone]

3. Information about Release
Date Discovered: October 11, 2016
Estimated Quantity of Release: Unknown
Cause of Release: Tank corrosion
Source of Release (Dispenser/Piping/UST): UST System
Sizes and contents of UST system(s) from which the release occurred): Three 4,000 Gallon Petroleum
USTs
4. Certification
I, Keith C. Seramur, a Licensed Geologist for Seramur & Associates,
PC, do certify that the information contained in this report is correct and accurate to the best of my knowledge.

Seramur & Associates, PC.__ is licensed to practice geology in North Carolina. The certification number of the
company or corporation is _C310_________________.
2
B. Site History and Characterization
1. Site History
Table B-2 shows UST Owner/Operator Information.

Table B-2: Site History - UST/AST Owner/Operator and Other Responsible Party Information
Revision Date: 10/21/16 Incident Number and Name: Nick’s Motor Cars

UST ID Number UST 1, UST 2, UST 3 Facility ID Number Not Registered
Name of Owner Dates of Operation
(mm/dd/yy to mm/dd/yy)
Nicholas J. Wehrmann Not Known
Street Address
3384 W. US Hwy. 421
City State Zip Telephone Number
Wilkesboro NC 28697 [phone]
Name of Operator Dates of Operation
(mm/dd/yy to mm/dd/yy)
Tommy Turner (Deceased) Not Known
Street Address
Not Known
City State Zip Telephone Number
Not Known NC Not Known Not Known
Incident Number N/A
Name of Other Responsible Party Dates of Release(s)
(mm/dd/yy to mm/dd/yy)
N/A N/A
Street Address
N/A
City State Zip Telephone Number
N/A N/A N/A N/A

3
2. Site History – UST/AST System and Other Release Information

Table B-1 lists information about the former UST systems.

Table B-1: Site History – UST/AST System and Other Release Information
Revision Date: 10/21/16 Incident Number and Name: Nick’s Motor Cars

UST ID
Number

Current/Last
Contents *

Previous
Contents *

Capacity
(in
gallons)

Construction
Details **

Tank
Dimensions
Description
of
Associated
Piping and
Pumps

Date
Tank
Installed

Status of
UST ***

Was
release
associated
with the
UST
System?
UST 1 Gasoline/
Diesel
Gasoline/
Diesel 4,000 Steel 24.0’ x 5.3’ Steel
product lines
Unknown
(1950’s?)
Closed by
removal
on
10/12/16
yes
UST 2 Gasoline/
Diesel
Gasoline/
Diesel 4,000 Steel 24.0’ x 5.3’ Steel
product lines
Unknown
(1950’s?)
Closed by
removal
on
10/12/16
yes
UST 3 Gasoline/
Diesel
Gasoline/
Diesel 4,000 Steel 24.0’ x 5.3’ Steel
product lines
Unknown
(1950’s?)
Closed by
removal
on
10/13/16
yes

Incident
Number
Material
Released
Date of
Release Description of Release
Unknown Gasoline/
Diesel
Discovered
10/11/16
Petroleum was observed in soil removed from sides and under
USTs

The recently closed petroleum USTs 1, 2 and 3 were located on the south side of the property (Figure 2).

The three USTs (1, 2 and 3) were previously used at the property by Tommy Turner as early as the 1950’s.
These were three 4,000 gallon petroleum (gasoline or diesel) USTs. A review of the UST database showed
that these USTs were never registered because they were taken out of service reportedly at some time in the
1970’s according to local informants. No release incident number has been associated with these tanks.

3. There are no known spills or releases from non-UST sources at the subject property prior to the release
discovered 10/11/16.

4. Provide a comprehensive description of the release, including date discovered, cause and source (including tank identification number and contents), and the relationship of historical UST releases, non-UST releases, and off-site releases (indicate incident number) to contamination from current release.

The USTs were permanently closed by removal between October 11 and October 13, 2016. During
removal of the tanks, it was noted that there were small holes in several spots on the tanks on the bottoms
and sides. Petroleum odors and staining were observed on the sides of the tanks and under the tanks.
Gasoline range organics and diesel range organics were detected under each tank. Diesel range organics
were found in all three samples under the middle tank (UST 2) and it is suspected that this was the diesel
storage tank.

Seramur & Associates is not aware of any non-UST releases or off-site releases that could be contributing
to contamination from current release.
4

5. Provide a brief description of site characteristics (including status of facility (active or inactive), land use of site and surrounding area, water supply, topography, vegetation, surface water, wells, buildings, surface cover, soil type, depth to and nature of bedrock, depth to groundwater, direction of groundwater flow, etc.)
The USTs were taken out of service reportedly at some time in the 1970’s according to local informants.
The property is currently used as a body shop/auto restoration facility. Surrounding land use is commercial
and residential. A public water supply is available to some properties in the area and a water supply well
was observed on at least one nearby property. Groundwater was not observed in the UST excavations.

The property is located between two ridges and adjacent to a valley that slopes to the east (Figure 1).
Miller’s Creek runs in a northwest to southeast direction in a valley east of the property. The creek is
approximately 1,000 feet from the UST excavation at its closest point. There is very little vegetation on the
property apart from grass near the highway and brush along the backside of the property. Roots were
observed in the tank pit, some as large as tree roots. The soil consists of sandy silt in the source area.
Bedrock was not encountered and depth to bedrock is unknown. Bedrock in this area is mapped as the
Ashe Formation, primarily a mica schist interbedded with a gneiss (Rankin, D.W., Espenshade, G.H., and
Neuman, R.B., 1972, Geologic Map of the West Half of the Winston-Salem Quadrangle, North Carolina,
Virginia, and Tennessee. Misc. Geol. Invest. Map I-709-A Dept. of the Interior, U.S. Geol. Surv.,
Washington D.C., 1 Map.).

6. Summarize initial abatement actions, assessment activities, and corrective actions performed to date and list all reports previously submitted.

The USTs were permanently closed by removal between October 11 and October 13, 2016. Each trackhoe
bucket of soil removed from the two UST excavations was screened in the field for petroleum vapors with
a Photocheck 100 photoionization detector. Approximately 42 cubic yards of contaminated soil was
removed from around the USTs. Soil contamination appeared to be primarily limited to the area around
and under the tanks. Contaminated soil was transported to Environmental Soils, Inc. in Lattimore, NC.

Soil consisted of sandy silt to a depth of about 9 feet.

Three soil samples were collected from below each of the three USTs (Figure 4). Another composite
sample was collected from the two piles of contaminated soil. All soil samples were analyzed for gasoline
range organics and diesel range organics (EPA Method 8015C, TPH GRO/TPH DRO).

The only previous report prepared for NCDENR was the 24-Hour UST-61 Report.

C. Site Check Report
A site check report has not been completed.

D. UST Closure Report
The UST-2 form is included in Appendix A.

1. Describe preparations for closure including steps taken to notify authorities, permits obtained, and steps
taken to clean and purge the tanks.

A Utility locate request was made to NC One-Call. Seramur & Associates personnel made site visits to
mark the proposed excavation area. The atmosphere in the USTs was checked for explosive vapors with an
Explosimeter. The Lower Explosive Limit (LEL) readings for the gasoline USTs were below 10%. The
atmosphere inside the USTs were rendered inert with carbon dioxide by placing dry ice (1.5 lbs./100
gallons) in the tanks on October 12 and 13, 2016. A UST closure permit was obtained from the County
Fire Marshal. A Health and Safety Plan was prepared for the closure work and a safety meeting was
conducted in the morning prior to commencing work.

5
Residual liquids (water w/some fuel) were removed from UST 3 by Petroserve, Inc. prior to the closures.
973 gallons of a gasoline/water mix were removed from the tank. UST 1 and UST 2 were empty.

The tanks were excavated and removed from the excavation. Fred Reeves Construction transported the
three tanks to their construction yard for cleaning and preparation for recycling.

2. Describe the closure procedure referencing site and sampling location maps and cross-sections presented in Section J of this report. Clearly state how the selection of sample types and locations was influenced by the nature of the stored substance, the type of initial alarm or cause for suspicion, the type of backfill, the depth to groundwater, and other factors appropriate for identifying the presence and source of a release. If presence of groundwater or bedrock require the installation and sampling of monitoring well(s), describe
the process.

Soil was excavated from the sides and one end of each UST. The USTs were then removed from the
excavation using chains and the trackhoe. Soil samples were collected from below each UST (Figures 4
and 5). One additional composite soil sample was collected from the contaminated soil stockpiles. These
soil samples were analyzed for gasoline range organics and diesel range organics (EPA Method 8015B,
TPH GRO/TPH DRO).

Soil samples from the excavation were collected using both the trackhoe bucket and decontaminated hand
auger buckets. The extent of the excavation and locations of soil samples are shown on Figures 3, 4 and 5.
All soil samples were collected while wearing a new pair of disposable Nitrile gloves. The soil samples
were placed in containers provided by the lab, labeled and placed on ice. A chain of custody was initiated
and the samples were transported to Prism Labs Inc. in Charlotte, NC for analysis.

The selection of sample types and locations was not influenced by the nature of the stored substance.
Depth to groundwater is not known. There was no evidence of groundwater in the excavation. The UST
excavation was backfilled with clean soil from the excavation as well as clean fill obtained by Fred Reeves
Construction.

3. Note the amount of residual material pumped from the tank and describe the storage, sampling and disposal of the residual material and the disposal of the tank, pumps and piping.

Residual fuel was removed from UST 3 by Petroserve, Inc. prior to the closures. 973 gallons of a
gasoline/water mix were removed from the tank. UST 1 and UST 2 were empty.

The tanks were excavated and removed from the excavation. Fred Reeves Construction transported the
three tanks to their construction yard for cleaning and preparation for recycling.

4. If a release is determined, document initial response actions.

A petroleum odor and staining was noted around the tanks for the three USTs. Soil excavation was limited
to the volume of soil that was necessary to remove the USTs from the ground. Three USTs were closed
and removed from the site. Contaminated soil associated with the leakage from the tanks was stockpiled
onsite. Approximately 42 cubic yards of contaminated soil was stockpiled onsite and later transported to
Environmental Soils, Inc. in Lattimore, NC.

Elevated concentrations of gasoline range organics and diesel range organics were detected in samples S-1
and S-4. Gasoline range organics were detected above the NCDENR action level in all samples collected
from under the tanks except for S-8 and S-10. Diesel range organics were detected above the NCDENR
action level only in samples S-1, S-4 and S-9.

A 24-hour report was prepared for NC DENR.

5. Document any soil excavation activities.

6
Soil was excavated from the sides and one end of each UST. The USTs were then removed from the
excavation using chains and the trackhoe. If petroleum vapors were detected in soil removed from the
excavation, it was stockpiled onsite and later transported to a remediation facility.

6. Document site investigation.

The trackhoe buckets of soil removed from the UST excavation were screened in the field for petroleum
vapors with a Photocheck 100 photoionization detector. The photoionization detector is calibrated with a
100-ppm isobutylene calibration gas mixture. Soil containing petroleum vapors was stockpiled onsite.

Soil consisted of sandy silt to a depth of about 9 feet.

Soil sample locations are shown on Figures 4 and 5. North-South and East-West cross-sections of the UST
system are shown in Figure 5. Soil samples were collected on October 12 and 13, 2016. The sample time
is listed on the Chain of Custody Record.

Depth to groundwater is not known. There was no evidence of groundwater in the excavation. The UST
excavation was backfilled with clean fill from the tank pit and clean fill obtained by Fred Reeves
Construction.

The hand auger buckets were decontaminated with non-phosphate detergent, distilled water and
isopropanol. Horizontal location and depth of the soil samples was measured with a fiberglass tape,
estimating right angles and referencing site features.

Soil samples were stored on ice and shipped to Prism Labs in Charlotte, NC via Federal Express.

Elevated concentrations of gasoline range organics and diesel range organics were detected in samples S-1
and S-4. Gasoline range organics were detected above the NCDENR action level in all samples collected
from under the tanks except for S-8 and S-10. Diesel range organics were detected above the NCDENR
action level only in samples S-1, S-4 and S-9.

7. Present conclusions and recommendations, referencing maps

The source of soil contamination was the three USTs. Petroleum constituents were detected at
concentrations above the NCDENR action levels in the base of the UST excavation.

Elevated concentrations of gasoline range organics and diesel range organics were detected in samples S-1
and S-4. Gasoline range organics were detected above the NCDENR action level in all samples collected
from under the tanks except for S-8 and S-10. Diesel range organics were detected above the NCDENR
action level only in samples S-1, S-4 and S-9.

Free product has not been encountered at the site. The next assessment phase required by NCDEQ would
be an LSA report.

E. Free Product Investigation and Recovery Report
Free product was not observed during the UST closure.

F. Groundwater and Surface Water Investigation
There was no groundwater or surface water investigation completed during the UST closure.

G. Initial Response and Abatement Action
Contaminated soil associated with the release from the USTs was stockpiled onsite. Approximately 40
cubic yards of contaminated soil was stockpiled. Nine soil samples (S-1 through S-6 and S-8 through S-10)
were collected from within the excavation for TPH GRO/DRO analysis. One additional composite sample
was collected from the soil stockpiles. A 24-hour report was prepared for NCDENR.

7
H. Excavation of Contaminated Soil
A petroleum odor and staining was noted around the tanks for the three USTs. Soil excavation was limited
to the volume of soil that was necessary to remove the USTs from the ground. The three USTs were
collected and removed from the site. Contaminated soil associated with the leakage from the tanks was
stockpiled onsite. Approximately 40 cubic yards of contaminated soil was stockpiled onsite.

Petroleum constituents were detected in soil samples collected from below the USTs. Very high
concentrations of gasoline range organics and diesel range organics were detected in samples S-1 and S-4.
All samples collected from under the tanks except for S-8 and S-10 had gasoline range organics detected
above the NCDENR action level. Only samples S-1, S-4 and S-9 had gasoline range organics detected
above the NCDENR action level.

I. Conclusions
Very high concentrations of gasoline range organics and diesel range organics were detected in samples S-1
and S-4. All samples collected from under the tanks except for S-8 and S-10 had gasoline range organics
detected above the NCDENR action level. Only samples S-1, S-4 and S-9 had gasoline range organics
detected above the NCDENR action level.

Free product has not been encountered at the site. The next assessment phase required by NCDEQ would
be an LSA report.

J. Table B-3 and Figures

8
Table B-3: Summary of Soil Sampling Results
Revision Date: 10/26/16 Incident Number and Name: Nick’s Motor Cars Facility ID#: Not Registered
Analytical Method (e.g., VOC by EPA 8260)
 8015C 8015C
Contaminant of Concern  TPH GRO (mg/kg) TPH DRO (mg/kg) Sample ID Date Collected (mm/dd/yy) Source Area (eg. Tank pit 1) Sample Depth (ft BGS) Incident Phase (Closure , etc) S-1 10/12/16 UST 1 8.6 ft Closure 14,000 2,900
S-2 10/12/16 UST 1 8.6 ft Closure 80 31
S-3 10/12/16 UST 1 8.6 ft Closure 64 ND
S-4 10/12/16 UST 2 8.6 ft Closure 3,200 1,700
S-5 10/12/16 UST 2 8.6 ft Closure 160 39
S-6 10/12/16 UST 2 8.6 ft Closure 400 15
S-7 10/12/16 Stockpile N/A Closure 12 13
S-8 10/13/16 UST 3 8.6 ft Closure 38 ND
S-9 10/13/16 UST 3 8.6 ft Closure 190 750
S-10 10/13/16 UST 3 8.6 ft Closure ND ND
NCDENR Action Level 50 100
ft. BGS = feet below ground surface
ND = Petroleum Constituents Below Reporting Limit or Not Detected

9

10

11

12

13

14
Appendix A – UST-2 Form

15
Appendix B

Laboratory Reports and Chain of Custody

This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Case Narrative
10/26/2016
Keith C. Seramur PGPC
Keith Seramur
165 Knoll Dr.
Boone, NC 28607
Project: Nick’s Motor Cars
Lab Submittal Date: 10/19/2016
Prism Work Order: 6100377
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
DATA SUBJECT TO CHANGE
Reviewed ByDRAFT REPORT DRAFT REPORT
VP Laboratory Services
Data Qualifiers Key Reference:
A Surrogate recovery below range due to sample matrix. Matrix interference suspected.
DO Surrogates diluted out.
M Matrix spike outside of the control limits.
RLM Sample container suspected to have low methanol content. Results possibly biased high.
SR Surrogate recovery outside the QC limits.
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 18
Sample Receipt Summary
10/26/2016
Prism Work Order: 6100377
Client Sample ID MatrixLab Sample ID Date Sampled Date Received
6100377-01 10/12/16S-1 10/19/16Solid
6100377-02 10/12/16S-2 10/19/16Solid
6100377-03 10/12/16S-3 10/19/16Solid
6100377-04 10/12/16S-4 10/19/16Solid
6100377-05 10/12/16S-5 10/19/16Solid
6100377-06 10/12/16S-6 10/19/16Solid
6100377-07 10/12/16S-7 10/19/16Solid
6100377-08 10/13/16S-8 10/19/16Solid
6100377-09 10/13/16S-9 10/19/16Solid
6100377-10 10/13/16S-10 10/19/16Solid
Samples were received in good condition at 5.2 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 18
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 6100377
10/26/2016
Summary of Detections
2900 mg/kg dry6100377-01 S-1 Diesel Range Organics *8015C
14000 mg/kg dry6100377-01 S-1 Gasoline Range Organics *8015C
31 mg/kg dry6100377-02 S-2 Diesel Range Organics *8015C
80 mg/kg dry6100377-02 S-2 Gasoline Range Organics *8015C
64 mg/kg dry6100377-03 S-3 Gasoline Range Organics *8015C
1700 mg/kg dry6100377-04 S-4 Diesel Range Organics *8015C
3200 mg/kg dry6100377-04 S-4 Gasoline Range Organics *8015C
39 mg/kg dry6100377-05 S-5 Diesel Range Organics *8015C
160 mg/kg dry6100377-05 S-5 Gasoline Range Organics *8015C
15 mg/kg dry6100377-06 S-6 Diesel Range Organics *8015C
400 mg/kg dry6100377-06 S-6 Gasoline Range Organics *8015C
13 mg/kg dry6100377-07 S-7 Diesel Range Organics *8015C
12 mg/kg dry6100377-07 S-7 Gasoline Range Organics *8015C
38 mg/kg dry6100377-08 S-8 Gasoline Range Organics *8015C
750 mg/kg dry6100377-09 S-9 Diesel Range Organics *8015C
190 mg/kg dry6100377-09 S-9 Gasoline Range Organics *8015C
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 18
Laboratory Report
10/26/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
165 Knoll Dr.
Project: Nick’s Motor CarsKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Sample Matrix: Solid
Client Sample ID: S-1
Prism Sample ID: 6100377-01
Prism Work Order: 6100377
Time Collected: 10/12/16 14:56
Time Submitted: 10/19/16 11:58
Diesel Range Organics by GC/FID
2900 *8015C P6J03755042010/21/16 23:46 ZRCmg/kg dry 97Diesel Range Organics
Surrogate Recovery Control Limits
49-1240 %o-Terphenyl DO
Gasoline Range Organics by GC/FID
14000 *8015C P6J0410500093010/25/16 12:09 ANGmg/kg dry 140Gasoline Range Organics
Surrogate Recovery Control Limits
50-1370 %a,a,a-Trifluorotoluene DO
General Chemistry Parameters
82.4 *SM2540 G P6J037710.100 10/20/16 16:45 JLB% by
Weight
0.100% Solids
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 18
Laboratory Report
10/26/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
165 Knoll Dr.
Project: Nick’s Motor CarsKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Sample Matrix: Solid
Client Sample ID: S-2
Prism Sample ID: 6100377-02
Prism Work Order: 6100377
Time Collected: 10/12/16 14:59
Time Submitted: 10/19/16 11:58
Diesel Range Organics by GC/FID
31 *8015C P6J037518.7 10/21/16 16:58 ZRCmg/kg dry 2.0Diesel Range Organics
Surrogate Recovery Control Limits
49-12463 %o-Terphenyl
Gasoline Range Organics by GC/FID RLM
80 *8015C P6J0410508.9 10/24/16 22:45 ANGmg/kg dry 1.3Gasoline Range Organics
Surrogate Recovery Control Limits
50-137154 %a,a,a-Trifluorotoluene SR
General Chemistry Parameters
80.6 *SM2540 G P6J037710.100 10/20/16 16:45 JLB% by
Weight
0.100% Solids
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 18
Laboratory Report
10/26/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
165 Knoll Dr.
Project: Nick’s Motor CarsKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Sample Matrix: Solid
Client Sample ID: S-3
Prism Sample ID: 6100377-03
Prism Work Order: 6100377
Time Collected: 10/12/16 15:05
Time Submitted: 10/19/16 11:58
Diesel Range Organics by GC/FID
BRL *8015C P6J037511010/21/16 17:35 ZRCmg/kg dry 2.3Diesel Range Organics
Surrogate Recovery Control Limits
49-12482 %o-Terphenyl
Gasoline Range Organics by GC/FID
64 *8015C P6J0410507.1 10/24/16 23:13 ANGmg/kg dry 1.1Gasoline Range Organics
Surrogate Recovery Control Limits
50-137119 %a,a,a-Trifluorotoluene
General Chemistry Parameters
68.9 *SM2540 G P6J037710.100 10/20/16 16:45 JLB% by
Weight
0.100% Solids
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 18
Laboratory Report
10/26/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
165 Knoll Dr.
Project: Nick’s Motor CarsKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Sample Matrix: Solid
Client Sample ID: S-4
Prism Sample ID: 6100377-04
Prism Work Order: 6100377
Time Collected: 10/12/16 16:50
Time Submitted: 10/19/16 11:58
Diesel Range Organics by GC/FID
1700 *8015C P6J03755050010/22/16 0:23 ZRCmg/kg dry 110Diesel Range Organics
Surrogate Recovery Control Limits
49-1240 %o-Terphenyl DO
Gasoline Range Organics by GC/FID
3200 *8015C P6J0410100016010/25/16 2:28 ANGmg/kg dry 25Gasoline Range Organics
Surrogate Recovery Control Limits
50-137100 %a,a,a-Trifluorotoluene
General Chemistry Parameters
69.8 *SM2540 G P6J037710.100 10/20/16 16:45 JLB% by
Weight
0.100% Solids
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 18
Laboratory Report
10/26/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
165 Knoll Dr.
Project: Nick’s Motor CarsKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Sample Matrix: Solid
Client Sample ID: S-5
Prism Sample ID: 6100377-05
Prism Work Order: 6100377
Time Collected: 10/12/16 17:00
Time Submitted: 10/19/16 11:58
Diesel Range Organics by GC/FID
39 *8015C P6J037518.9 10/21/16 18:12 ZRCmg/kg dry 2.0Diesel Range Organics
Surrogate Recovery Control Limits
49-12479 %o-Terphenyl
Gasoline Range Organics by GC/FID
160 *8015C P6J0410505.8 10/25/16 1:04 ANGmg/kg dry 0.87Gasoline Range Organics
Surrogate Recovery Control Limits
50-137116 %a,a,a-Trifluorotoluene
General Chemistry Parameters
78.6 *SM2540 G P6J037710.100 10/20/16 16:45 JLB% by
Weight
0.100% Solids
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 18
Laboratory Report
10/26/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
165 Knoll Dr.
Project: Nick’s Motor CarsKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Sample Matrix: Solid
Client Sample ID: S-6
Prism Sample ID: 6100377-06
Prism Work Order: 6100377
Time Collected: 10/12/16 17:15
Time Submitted: 10/19/16 11:58
Diesel Range Organics by GC/FID
15 *8015C P6J037519.4 10/21/16 18:49 ZRCmg/kg dry 2.1Diesel Range Organics
Surrogate Recovery Control Limits
49-12478 %o-Terphenyl
Gasoline Range Organics by GC/FID RLM
400 *8015C P6J0410509.8 10/25/16 1:32 ANGmg/kg dry 1.5Gasoline Range Organics
Surrogate Recovery Control Limits
50-137140 %a,a,a-Trifluorotoluene SR
General Chemistry Parameters
74.7 *SM2540 G P6J037710.100 10/20/16 16:45 JLB% by
Weight
0.100% Solids
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 18
Laboratory Report
10/26/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
165 Knoll Dr.
Project: Nick’s Motor CarsKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Sample Matrix: Solid
Client Sample ID: S-7
Prism Sample ID: 6100377-07
Prism Work Order: 6100377
Time Collected: 10/12/16 18:08
Time Submitted: 10/19/16 11:58
Diesel Range Organics by GC/FID
13 *8015C P6J037519.2 10/21/16 19:26 ZRCmg/kg dry 2.1Diesel Range Organics
Surrogate Recovery Control Limits
49-12476 %o-Terphenyl
Gasoline Range Organics by GC/FID
12 *8015C P6J0410507.5 10/24/16 23:41 ANGmg/kg dry 1.1Gasoline Range Organics
Surrogate Recovery Control Limits
50-137124 %a,a,a-Trifluorotoluene
General Chemistry Parameters
76.2 *SM2540 G P6J040710.100 10/21/16 16:42 JLB% by
Weight
0.100% Solids
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 18
Laboratory Report
10/26/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
165 Knoll Dr.
Project: Nick’s Motor CarsKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Sample Matrix: Solid
Client Sample ID: S-8
Prism Sample ID: 6100377-08
Prism Work Order: 6100377
Time Collected: 10/13/16 13:15
Time Submitted: 10/19/16 11:58
Diesel Range Organics by GC/FID
BRL *8015C P6J037519.0 10/21/16 20:04 ZRCmg/kg dry 2.1Diesel Range Organics
Surrogate Recovery Control Limits
49-12488 %o-Terphenyl
Gasoline Range Organics by GC/FID
38 *8015C P6J0410506.6 10/25/16 0:09 ANGmg/kg dry 0.99Gasoline Range Organics
Surrogate Recovery Control Limits
50-137114 %a,a,a-Trifluorotoluene
General Chemistry Parameters
77.0 *SM2540 G P6J037710.100 10/20/16 16:45 JLB% by
Weight
0.100% Solids
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 18
Laboratory Report
10/26/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
165 Knoll Dr.
Project: Nick’s Motor CarsKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Sample Matrix: Solid
Client Sample ID: S-9
Prism Sample ID: 6100377-09
Prism Work Order: 6100377
Time Collected: 10/13/16 13:22
Time Submitted: 10/19/16 11:58
Diesel Range Organics by GC/FID
750 *8015C P6J0375109610/24/16 11:05 ZRCmg/kg dry 22Diesel Range Organics
Surrogate Recovery Control Limits
49-12494 %o-Terphenyl
Gasoline Range Organics by GC/FID
190 *8015C P6J04102503410/25/16 2:00 ANGmg/kg dry 5.2Gasoline Range Organics
Surrogate Recovery Control Limits
50-137130 %a,a,a-Trifluorotoluene
General Chemistry Parameters
73.2 *SM2540 G P6J037710.100 10/20/16 16:45 JLB% by
Weight
0.100% Solids
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 18
Laboratory Report
10/26/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
165 Knoll Dr.
Project: Nick’s Motor CarsKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Sample Matrix: Solid
Client Sample ID: S-10
Prism Sample ID: 6100377-10
Prism Work Order: 6100377
Time Collected: 10/13/16 13:35
Time Submitted: 10/19/16 11:58
Diesel Range Organics by GC/FID
BRL *8015C P6J037518.7 10/21/16 21:18 ZRCmg/kg dry 2.0Diesel Range Organics
Surrogate Recovery Control Limits
49-12445 %o-Terphenyl A
Gasoline Range Organics by GC/FID
BRL *8015C P6J0410508.2 10/25/16 0:37 ANGmg/kg dry 1.2Gasoline Range Organics
Surrogate Recovery Control Limits
50-137136 %a,a,a-Trifluorotoluene
General Chemistry Parameters
80.2 *SM2540 G P6J037710.100 10/20/16 16:45 JLB% by
Weight
0.100% Solids
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 18
10/26/16
Level II QC Report
165 Knoll Dr.
Project: Nick’s Motor CarsKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Prism Work Order: 6100377
Time Submitted: 10/19/2016 11:58:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Gasoline Range Organics by GC/FID - Quality Control
Batch P6J0410 - 5035
Blank (P6J0410-BLK1)Prepared & Analyzed: 10/24/16
Gasoline Range Organics mg/kg wetBRL5.0
mg/kg wet 5.000 50-137Surrogate: a,a,a-Trifluorotoluene 1085.40
LCS (P6J0410-BS1)Prepared & Analyzed: 10/24/16
Gasoline Range Organics mg/kg wet54.3 5.0 41-138
mg/kg wet 5.000 50-137Surrogate: a,a,a-Trifluorotoluene 964.80
LCS Dup (P6J0410-BSD1)Prepared & Analyzed: 10/24/16
Gasoline Range Organics mg/kg wet59.8 5.0 2041-138 10
mg/kg wet 5.000 50-137Surrogate: a,a,a-Trifluorotoluene 994.95
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 18
10/26/16
Level II QC Report
165 Knoll Dr.
Project: Nick’s Motor CarsKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Prism Work Order: 6100377
Time Submitted: 10/19/2016 11:58:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Diesel Range Organics by GC/FID - Quality Control
Batch P6J0375 - 3546
Blank (P6J0375-BLK1)Prepared & Analyzed: 10/21/16
Diesel Range Organics mg/kg wetBRL7.0
mg/kg wet 1.332 49-124Surrogate: o-Terphenyl 761.01
LCS (P6J0375-BS1)Prepared & Analyzed: 10/21/16
Diesel Range Organics mg/kg wet55.6 7.0 66.67 55-10983
mg/kg wet 1.333 49-124Surrogate: o-Terphenyl 811.08
LCS Dup (P6J0375-BSD1)Prepared & Analyzed: 10/21/16
Diesel Range Organics mg/kg wet51.7 7.0 66.67 2055-10978 7
mg/kg wet 1.333 49-124Surrogate: o-Terphenyl 761.01
Matrix Spike (P6J0375-MS1)Prepared & Analyzed: 10/21/16 Source: 6100377-10
Diesel Range Organics mg/kg dry55.3 8.7 83.07 2.42 50-11764
mg/kg dry 1.661 49-124Surrogate: o-Terphenyl 621.03
Matrix Spike Dup (P6J0375-MSD1)Prepared & Analyzed: 10/21/16 Source: 6100377-10
Diesel Range Organics mg/kg dry42.3 8.7 83.01 2.42 24 M50-11748 27
mg/kg dry 1.660 A49-124Surrogate: o-Terphenyl 450.751
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 18
10/26/16
Level II QC Report
165 Knoll Dr.
Project: Nick’s Motor CarsKeith C. Seramur PGPC
Boone, NC 28607
Attn: Keith Seramur
Prism Work Order: 6100377
Time Submitted: 10/19/2016 11:58:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
General Chemistry Parameters - Quality Control
Batch P6J0377 - Solids, Dry Weight
Duplicate (P6J0377-DUP3)Prepared & Analyzed: 10/20/16 Source: 6100377-01
% Solids % by Weight82.4 0.100 82.4 200.07
Duplicate (P6J0377-DUP4)Prepared & Analyzed: 10/20/16 Source: 6100377-10
% Solids % by Weight79.8 0.100 80.2 200.5
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 18
Sample Extraction Data
Prep Method: 3546
Lab Number Batch Date/TimeInitialFinal
P6J03756100377-01 10/21/16 9:2530.01 1g mL
P6J03756100377-02 10/21/16 9:2530.04 1g mL
P6J03756100377-03 10/21/16 9:2530.02 1g mL
P6J03756100377-04 10/21/16 9:2530.07 1g mL
P6J03756100377-05 10/21/16 9:2530.06 1g mL
P6J03756100377-06 10/21/16 9:2530.06 1g mL
P6J03756100377-07 10/21/16 9:2530.01 1g mL
P6J03756100377-08 10/21/16 9:2530.16 1g mL
P6J03756100377-09 10/21/16 9:2530.04 1g mL
P6J03756100377-10 10/21/16 9:2530.08 1g mL
Prep Method: 5035
Lab Number Batch Date/TimeInitialFinal
P6J04106100377-01 10/24/16 13:373.26 5g mL
P6J04106100377-02 10/24/16 13:373.47 5g mL
P6J04106100377-03 10/24/16 13:375.13 5g mL
P6J04106100377-04 10/24/16 13:374.39 5g mL
P6J04106100377-05 10/24/16 13:375.48 5g mL
P6J04106100377-06 10/24/16 13:373.42 5g mL
P6J04106100377-07 10/24/16 13:374.38 5g mL
P6J04106100377-08 10/24/16 13:374.93 5g mL
P6J04106100377-09 10/24/16 13:374.98 5g mL
P6J04106100377-10 10/24/16 13:373.81 5g mL
Prep Method: Solids, Dry Weight
Lab Number Batch Date/TimeInitialFinal
P6J03776100377-01 10/20/16 16:4530 30g g
P6J03776100377-02 10/20/16 16:4530 30g g
P6J03776100377-03 10/20/16 16:4530 30g g
P6J03776100377-04 10/20/16 16:4530 30g g
P6J03776100377-05 10/20/16 16:4530 30g g
P6J03776100377-06 10/20/16 16:4530 30g g
P6J04076100377-07 10/21/16 16:4230 30g g
P6J03776100377-08 10/20/16 16:4530 30g g
P6J03776100377-09 10/20/16 16:4530 30g g
P6J03776100377-10 10/20/16 16:4530 30g g
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 18
Page 18 of 18
16
Appendix C

Standard Operating Procedures

The atmosphere in the USTs was checked for explosive vapors with an Explosimeter. The Lower Explosive Limit
(LEL) readings for the gasoline USTs were below 10%. The atmosphere inside the USTs were rendered inert with
carbon dioxide by placing dry ice (1.5 lbs./100 gallons) in the tanks on October 12 and 13, 2016. A Health and
Safety Plan was prepared for the closure work. A safety meeting was conducted prior to commencing work.

Soil samples collected from the excavation were collected out of the trackhoe bucket and with decontaminated hand
auger buckets. The hand auger buckets were decontaminated with non-phosphate detergent and distilled water and
isopropanol rinses.

Soil samples collected for laboratory analysis were placed in laboratory sample jars with Teflon-lined lids; chilled
and Chain-of-Custody record was initiated. Soil samples were transported to Prism Labs Inc. in Charlotte, North
Carolina for analyses. A new pair of disposable Nitrile gloves was worn while collecting each sample. The depth
and horizontal locations of the soil samples were identified by measuring with a fiberglass tape, estimating right
angles and referencing site features.

17
Appendix D

Disposal Manifests

18

19

20

Appendix B
LSA Risk Classification and Land Use

Limited Site Assessment Report

A. Site Information
1. Site Identification
Date of Report: 2/15/2017
Facility I.D.: Not Registered Incident Number: N/A Site Risk: Low
Site Name: Nick’s Auto Cars
Site Street Address: 3384 West US Highway 421
City/Town: Wilkesboro Zip Code: 28697 County: Wilkes
Description of Geographical Data Point (e.g., dispenser): Building
Location Method (GPS, topographical map, other): Google Earth
Latitude (decimal degrees): 36.1502° N Longitude (decimal degrees): 81.2189° W

2. Information about Contacts Associated with the Release
UST/AST Owner: Nicholas J. Whermann
Address: 3384 West US Highway 421, Wilkesboro, NC 28697 Tel: [phone]
Property Owner: Nicholas J. Whermann
Address: 3384 West US Highway 421, Wilkesboro, NC 28697 Tel: [phone]
Consultant/Contractor: Mill Creek Environmental, LLC
Address: 1818 Perimeter Road, Dawsonville, GA 30534 Tel: [phone]
Analytical Laboratory: Pace Analytical State Certification No. 37706
Address: 9800 Kincey Ave # 100, Huntersville, NC 28078 Tel: [phone]

3. Information about Release
Date Discovered: October 11, 2016
Estimated Quantity of Release: Unknown
Cause of Release: Tank corrosion
Source of Release: UST system
Sizes and Contents of Tank or Other Containment from which the Release Occurred: Three 4,000
Gallon Petroleum USTs

4. Certification

I, Dan Centofanti, a Licensed Geologist for Mill Creek Environmental, LLC do certify that the information
contained in this report is correct and accurate to the best of my knowledge.

Mill Creek Environmental, LLC is licensed to practice geology in North Carolina. The certification number of
the company or corporation is C-505.

Dan Centofanti, PG, EP
Technical Director
Limited Site Assessment Risk Classification and Land Use Form

Part I – Groundwater/Surface Water/Vapor Impacts
High Risk
1. Has the release contaminated any water supply well including any well used for non-drinking purposes? NO
2. Is a water supply well used for drinking water located within 1,000 feet of the source area of the release? YES
Note: This well is located at 2154 Congo Road and is topographically up-gradient from the site.
3. Is a water supply well not used for drinking water (e.g., irrigation, washing cars, industrial cooling water,
filling swimming pools) located within 250 feet of the source area of the release? NO
4. Does groundwater within 500 feet of the source area of the release have the potential for future use (there is
no other source of water supply other than the groundwater)? NO
5. Do vapors from the release pose a threat of explosion because of accumulation of the vapors in a confined
space or pose any other serious threat to public health, public safety or the environment? NO
If yes, describe.
______________________________________________________________________________________
6. Are there any other factors that would cause the release to pose an imminent danger to public health, public
safety, or the environment? NO
If yes, describe.
______________________________________________________________________________________

Intermediate Risk
7. Is a surface water body located within 500 feet of the source area of the release?
NO
If YES, does the maximum groundwater contaminant concentration exceed the surface water quality
standards and criteria found in 15A NCAC 2B .0200 by a factor of 10? NO
8. Is the source area of the release located within a approved or planned wellhead protection area as defined in 42
USC 300h-7(e)? NO
If yes, describe.
______________________________________________________________________________________
9. Is the release located in the Coastal Plain physiographic region as designated on a map entitled “Geology of
North Carolina” published by the Department in 1985? NO
______________________________________________________________________________________
If YES, is the source area of the release located in an area in which there is recharge to an unconfined or
semi-confined deeper aquifer that is being used or may be used as a source of drinking water? NO
If YES, describe.
______________________________________________________________________________________
10. Do the levels of groundwater contamination for any contaminant exceed the gross contamination levels (See
Table 2.) established by the Department? NO

Part II - Land Use
Property Containing Source Area of Release
The questions below pertain to the property containing the source area of the release.
1. Does the property contain one or more primary or secondary residences (permanent or temporary)? NO
Describe.
___________________________________________________________________________________
_____________________________________________________________________
2. Does the property contain a school, daycare center, hospital, playground, park, recreation area, church,
nursing home, or other place of public assembly? NO
Describe.
__________________________________________________________________________________
____________________________________________________________________
3. Does the property contain a commercial (e.g., retail, warehouse, office/business space, etc.) or industrial
(e.g., manufacturing, utilities, industrial research and development, chemical/petroleum bulk storage, etc.)
enterprise, an inactive commercial or industrial enterprise, or is the land undeveloped? YES
Describe.

The subject property is currently a Midas auto shop

4. Do children visit the property? YES
Explain.

Children under supervision of customers of the auto shop may visit the subject property for short
periods of time in the customer waiting room. Children would not be exposed to contaminated soil
while at the subject property.

Is access to the property reliably restricted consistent with its use (e.g., by fences, security personnel or
both)? NO
Explain.
______________________________________________________________________________________
______________________________________________________________________
5. Do pavement, buildings, or other structures cap the contaminated soil? YES
Describe.

The contaminated soil is capped by a concrete and asphalt parking lot.

If yes, what mechanisms are in place or can be put into place to ensure that the contaminated soil will
remain capped in the foreseeable future?
______________________________________________________________________________________
______________________________________________________________________
6. What is the zoning status of the property? Commercial

7. Is the use of the property likely to change in the next 20 years? NO
Explain.
______________________________________________________________________________________
______________________________________________________________________

Property Surrounding Source Area of Release
The questions below pertain to the area within 1,500 feet of the source area of the release (excludes property
containing source area of the release):

1. What is the distance from the source area of the release to the nearest primary or secondary residence
(permanent or temporary)?

Permanent residence, 2154 Congo Road - 360 feet to the northwest, up-gradient.

2. What is the distance from the source area of the release to the nearest school, daycare center, hospital,
playground, park, recreation area, church, nursing home or other place of public assembly?

Pleasant Valley Baptist Church, 100 Buck Road - 400 feet to the northwest, up-gradient.

3. What is the zoning status of properties in the surrounding area? Residential and Commercial

4. Briefly characterize the use and activities of the land in the surrounding area.

North: Residential
East: Marathon gas station
South: Residential
West: Residential and commercial

Appendix C
Boring Log

LOG OF SOIL BORING
Page 1 of 2
Client: Nick's Auto Cars Boring No.: SB-1
Mill Creek Job No.: NAC-1701-1 Well Number: N/A
Environmental Services Job Name: Well Depth: N/A
1818 Perimeter Road Date Installed: 1/18/2017 Well Diam.: N/A
Dawsonville, Georgia 30534 Installed By: Dan Centofanti, P.G. Screen Length: N/A
Drilling Company: EDPS Screen Material: N/A
Boring Depth: 50 ft bgs Slot Size: N/A
Boring Diam.: 2.25 inches GW Level: N/A
Drilling Method: DPT + split-spoons TOC Elev.: N/A
DEPTH SAMPLE USCS BLOW COUNTS PID %
(feet)INTERVAL LITHOLOGIC DESCRIPTION CLASS 0-6 6-12 12-18 18-24 (ppm) REC(feet)6" 12" 18" 24"
FL 103 90
CL

5
CL 225 80

10
CL 40 60
DIAGRAM
Nick's Motor Cars LSA
1818 Perimeter Road
Dawsonville, GA 30534
MONITORING
WELL
Concrete, minor gravel.
Clay, red with tan and yellow mottles, soft, moist, some sand,
roots. (fill)
Clay, some sand, round gravel, red--mottled with tan, yellow
and brown, moist, dry areas, soft, fine mica. (fill)
Clay, minor silt and sand, soft, loose, mottled red, tan, white,
and pink kaolin layers, much mica, some coarse.

15
CL 359 80

20
CL 782 90
25
CL 569 80
30
Screen Interval: Locking Cap: N/A
Casing Interval: N/A Bottom Cap:
Sand Interval: N/A Type of Cover:
Bentonite Interval: N/A Water Level at 24 Hours: N/A
Grout Interval: N/A REMARKS:
Bags Sand: N/A
Bags Bentonite: N/A
Bags Cement: N/A
Installation Observed By: Dan Centofanti, P.G.
No groundwater encountered above 50' bgs.
N/A
N/A
N/A
Same as above.
Clay + sand + silt with minor gravel, dry, folded, mottled.
(saprolite)
Some banding. (saprolite)
Clay with fine sand and silt, very soft, dry, tan-pink-yellowish
mottled with bands of gray and with spots, vertical banding,
gneisic, mica and kalolin. (saprolite)
Same as above with increasing gray, increasing sand, minor
gravel, vertical foliation. (saprolite)
Texture of gneissic parent rock.
Boring Logs.xlsx
LOG OF SOIL BORING
Page 2 of 2
Client: Nick's Auto Cars Boring No.: SB-1
Mill Creek Job No.: NAC-1701-1 Well Number: N/A
Environmental Services Job Name: Well Depth: N/A
1818 Perimeter Road Date Installed: 1/18/2017 Well Diam.: N/A
Dawsonville, Georgia 30534 Installed By: Dan Centofanti, P.G. Screen Length: N/A
Drilling Company: EDPS Screen Material: N/A
Boring Depth: 50 ft bgs Slot Size: N/A
Boring Diam.: 2.25 inches GW Level: N/A
Drilling Method: DPT + split-spoons TOC Elev.: N/A
DEPTH SAMPLE USCS BLOW COUNTS PID %
(feet)INTERVAL LITHOLOGIC DESCRIPTION CLASS 0-6 6-12 12-18 18-24 (ppm) REC(feet)6" 12" 18" 24"
CL 58 100
32
CL 69 100
34
CL 49 100
36
CL 41 100
38
CL 17 100
40
CL 39 100
42
CL 33 100
DIAGRAM
Nick's Motor Cars LSA
1818 Perimeter Road
Dawsonville, GA 30534
MONITORING
WELL
Clay, white kaolinite, red stringers, quartz sand layers, some
mica, brown folliated layers, moist to dry, firm. (saprolite)
Clay, firm, banded, dry to moist, interlayered, foliated, geissic
with brown micasious layers + white kaolinte layers, red
stringers, gray pots, variable coloration, bands + foliation
Clay, firm, banded, moist, brown, white, tan, inter;ayered and
banded saprolite, much quartz and mica, red spots, gneissic
(saprolite)
Clay, hard, banded, multi-layered, red-white-gray-brown layers,
dry, black stringers, quartz and mica throughout, gneissic.
(saprolite)
Same as above. Beautiful saprolite. Banded, multi-colored.
Sam as above. Brown-tan-red.
Same as above. Moist.
44
CL 19 100
46
CL 24 100
48
CL 4 100
50
Screen Interval: Locking Cap: N/A
Casing Interval: N/A Bottom Cap:
Sand Interval: N/A Type of Cover:
Bentonite Interval: N/A Water Level at 24 Hours: N/A
Grout Interval: N/A REMARKS:
Bags Sand: N/A
Bags Bentonite: N/A
Bags Cement: N/A
Installation Observed By: Dan Centofanti, P.G.
N/A
No groundwater encountered above 50' bgs.
N/A
N/A
Same as above. Hard. Moist.
Same as above.
Clay, very hard, moist, banded brown with white layers, black
sringers, much foliation, gneissic. (saporolite)
Boring Logs.xlsx

Appendix D
Laboratory Analytical Report

#=CL#
January 27, 2017
LIMS USE: FR - DAN CENTOFANTI
LIMS OBJECT ID: 92326841
92326841
Project:
Pace Project No.:
RE:
Dan Centofanti
Mill Creek Environmental
1818 Perimeter Rd
Dawsonville, GA 30534
NICUS AUTO CARS NAC-1701-1
Dear Dan Centofanti:
Enclosed are the analytical results for sample(s) received by the laboratory on January 18, 2017.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
Report revised 1/27/17 to remove MDLs.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 44
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92326841
NICUS AUTO CARS NAC-1701-1
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 44
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92326841
NICUS AUTO CARS NAC-1701-1
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92326841001 SB-1, 20-25'MADEP EPH 7 PASI-CPKS
MADEP VPH 5 PASI-CWDV
EPA 8270 74 PASI-CRES
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92326841002 SB-1, 38-40'MADEP EPH 7 PASI-CPKS
MADEP VPH 5 PASI-CWDV
EPA 8270 74 PASI-CRES
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92326841003 SB-1, 48-50'MADEP EPH 7 PASI-CPKS
MADEP VPH 5 PASI-CWDV
EPA 8270 74 PASI-CRES
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92326841
NICUS AUTO CARS NAC-1701-1
Sample:SB-1, 20-25'Lab ID:92326841001 Collected:01/18/17 12:04 Received:01/18/17 18:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 01/24/17 22:06 N201/20/17 11:3010.7 1
Aliphatic (C19-C36)ND mg/kg 01/24/17 22:06 N201/20/17 11:3010.7 1
Aromatic (C11-C22)ND mg/kg 01/24/17 22:06 N201/20/17 11:3010.7 1
Surrogates
Nonatriacontane (S)47 %01/24/17 22:06 7194-86-701/20/17 11:3040-140 1
o-Terphenyl (S)62 %01/24/17 22:06 84-15-101/20/17 11:3040-140 1
2-Fluorobiphenyl (S)101 %01/24/17 22:06 321-60-801/20/17 11:3040-140 1
2-Bromonaphthalene (S)89 %01/24/17 22:06 580-13-201/20/17 11:3040-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)ND mg/kg 01/23/17 20:55 N201/23/17 08:372.1 1
Aliphatic (C09-C12)ND mg/kg 01/23/17 20:55 N201/23/17 08:372.1 1
Aromatic (C09-C10)ND mg/kg 01/23/17 20:55 N201/23/17 08:372.1 1
Surrogates
4-Bromofluorobenzene (FID) (S)95 %01/23/17 20:55 460-00-401/23/17 08:3770-130 1
4-Bromofluorobenzene (PID) (S)92 %01/23/17 20:55 460-00-401/23/17 08:3770-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 01/23/17 17:44 83-32-901/19/17 15:003541
Acenaphthylene ND ug/kg 01/23/17 17:44 208-96-801/19/17 15:003541
Aniline ND ug/kg 01/23/17 17:44 62-53-301/19/17 15:003541
Anthracene ND ug/kg 01/23/17 17:44 120-12-701/19/17 15:003541
Benzo(a)anthracene ND ug/kg 01/23/17 17:44 56-55-301/19/17 15:003541
Benzo(a)pyrene ND ug/kg 01/23/17 17:44 50-32-801/19/17 15:003541
Benzo(b)fluoranthene ND ug/kg 01/23/17 17:44 205-99-201/19/17 15:003541
Benzo(g,h,i)perylene ND ug/kg 01/23/17 17:44 191-24-201/19/17 15:003541
Benzo(k)fluoranthene ND ug/kg 01/23/17 17:44 207-08-901/19/17 15:003541
Benzoic Acid ND ug/kg 01/23/17 17:44 65-85-0 L2,M001/19/17 15:0017701
Benzyl alcohol ND ug/kg 01/23/17 17:44 100-51-601/19/17 15:007081
4-Bromophenylphenyl ether ND ug/kg 01/23/17 17:44 101-55-301/19/17 15:003541
Butylbenzylphthalate ND ug/kg 01/23/17 17:44 85-68-701/19/17 15:003541
4-Chloro-3-methylphenol ND ug/kg 01/23/17 17:44 59-50-701/19/17 15:007081
4-Chloroaniline ND ug/kg 01/23/17 17:44 106-47-801/19/17 15:0017701
bis(2-Chloroethoxy)methane ND ug/kg 01/23/17 17:44 111-91-101/19/17 15:003541
bis(2-Chloroethyl) ether ND ug/kg 01/23/17 17:44 111-44-401/19/17 15:003541
2-Chloronaphthalene ND ug/kg 01/23/17 17:44 91-58-701/19/17 15:003541
2-Chlorophenol ND ug/kg 01/23/17 17:44 95-57-801/19/17 15:003541
4-Chlorophenylphenyl ether ND ug/kg 01/23/17 17:44 7005-72-301/19/17 15:003541
Chrysene ND ug/kg 01/23/17 17:44 218-01-901/19/17 15:003541
Dibenz(a,h)anthracene ND ug/kg 01/23/17 17:44 53-70-301/19/17 15:003541
Dibenzofuran ND ug/kg 01/23/17 17:44 132-64-9 M101/19/17 15:003541
1,2-Dichlorobenzene ND ug/kg 01/23/17 17:44 95-50-1 M101/19/17 15:003541
1,3-Dichlorobenzene ND ug/kg 01/23/17 17:44 541-73-1 L201/19/17 15:003541
1,4-Dichlorobenzene ND ug/kg 01/23/17 17:44 106-46-701/19/17 15:003541
3,3'-Dichlorobenzidine ND ug/kg 01/23/17 17:44 91-94-101/19/17 15:0017701
2,4-Dichlorophenol ND ug/kg 01/23/17 17:44 120-83-201/19/17 15:003541
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92326841
NICUS AUTO CARS NAC-1701-1
Sample:SB-1, 20-25'Lab ID:92326841001 Collected:01/18/17 12:04 Received:01/18/17 18:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Diethylphthalate ND ug/kg 01/23/17 17:44 84-66-201/19/17 15:003541
2,4-Dimethylphenol ND ug/kg 01/23/17 17:44 105-67-901/19/17 15:003541
Dimethylphthalate ND ug/kg 01/23/17 17:44 131-11-301/19/17 15:003541
Di-n-butylphthalate ND ug/kg 01/23/17 17:44 84-74-201/19/17 15:003541
4,6-Dinitro-2-methylphenol ND ug/kg 01/23/17 17:44 534-52-101/19/17 15:007081
2,4-Dinitrophenol ND ug/kg 01/23/17 17:44 51-28-5 L201/19/17 15:0017701
2,4-Dinitrotoluene ND ug/kg 01/23/17 17:44 121-14-2 M101/19/17 15:003541
2,6-Dinitrotoluene ND ug/kg 01/23/17 17:44 606-20-201/19/17 15:003541
Di-n-octylphthalate ND ug/kg 01/23/17 17:44 117-84-001/19/17 15:003541
bis(2-Ethylhexyl)phthalate ND ug/kg 01/23/17 17:44 117-81-701/19/17 15:003541
Fluoranthene ND ug/kg 01/23/17 17:44 206-44-001/19/17 15:003541
Fluorene ND ug/kg 01/23/17 17:44 86-73-701/19/17 15:003541
Hexachloro-1,3-butadiene ND ug/kg 01/23/17 17:44 87-68-301/19/17 15:003541
Hexachlorobenzene ND ug/kg 01/23/17 17:44 118-74-101/19/17 15:003541
Hexachlorocyclopentadiene ND ug/kg 01/23/17 17:44 77-47-401/19/17 15:003541
Hexachloroethane ND ug/kg 01/23/17 17:44 67-72-101/19/17 15:003541
Indeno(1,2,3-cd)pyrene ND ug/kg 01/23/17 17:44 193-39-501/19/17 15:003541
Isophorone ND ug/kg 01/23/17 17:44 78-59-101/19/17 15:003541
1-Methylnaphthalene ND ug/kg 01/23/17 17:44 90-12-001/19/17 15:003541
2-Methylnaphthalene ND ug/kg 01/23/17 17:44 91-57-601/19/17 15:003541
2-Methylphenol(o-Cresol)ND ug/kg 01/23/17 17:44 95-48-701/19/17 15:003541
3&4-Methylphenol(m&p Cresol)ND ug/kg 01/23/17 17:4401/19/17 15:003541
Naphthalene ND ug/kg 01/23/17 17:44 91-20-301/19/17 15:003541
2-Nitroaniline ND ug/kg 01/23/17 17:44 88-74-401/19/17 15:0017701
3-Nitroaniline ND ug/kg 01/23/17 17:44 99-09-201/19/17 15:0017701
4-Nitroaniline ND ug/kg 01/23/17 17:44 100-01-601/19/17 15:007081
Nitrobenzene ND ug/kg 01/23/17 17:44 98-95-301/19/17 15:003541
2-Nitrophenol ND ug/kg 01/23/17 17:44 88-75-501/19/17 15:003541
4-Nitrophenol ND ug/kg 01/23/17 17:44 100-02-701/19/17 15:0017701
N-Nitrosodimethylamine ND ug/kg 01/23/17 17:44 62-75-901/19/17 15:003541
N-Nitroso-di-n-propylamine ND ug/kg 01/23/17 17:44 621-64-701/19/17 15:003541
N-Nitrosodiphenylamine ND ug/kg 01/23/17 17:44 86-30-601/19/17 15:003541
2,2'-Oxybis(1-chloropropane)ND ug/kg 01/23/17 17:44 108-60-1 M101/19/17 15:003541
Pentachlorophenol ND ug/kg 01/23/17 17:44 87-86-501/19/17 15:0017701
Phenanthrene ND ug/kg 01/23/17 17:44 85-01-801/19/17 15:003541
Phenol ND ug/kg 01/23/17 17:4401/19/17 15:003541
Pyrene ND ug/kg 01/23/17 17:44 129-00-001/19/17 15:003541
1,2,4-Trichlorobenzene ND ug/kg 01/23/17 17:44 120-82-101/19/17 15:003541
2,4,5-Trichlorophenol ND ug/kg 01/23/17 17:44 95-95-401/19/17 15:003541
2,4,6-Trichlorophenol ND ug/kg 01/23/17 17:44 88-06-201/19/17 15:003541
Surrogates
Nitrobenzene-d5 (S)44 %01/23/17 17:44 4165-60-001/19/17 15:0023-110 1
2-Fluorobiphenyl (S)42 %01/23/17 17:44 321-60-801/19/17 15:0030-110 1
Terphenyl-d14 (S)58 %01/23/17 17:44 1718-51-001/19/17 15:0028-110 1
Phenol-d6 (S)40 %01/23/17 17:44 13127-88-301/19/17 15:0022-110 1
2-Fluorophenol (S)41 %01/23/17 17:44 367-12-401/19/17 15:0013-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92326841
NICUS AUTO CARS NAC-1701-1
Sample:SB-1, 20-25'Lab ID:92326841001 Collected:01/18/17 12:04 Received:01/18/17 18:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
2,4,6-Tribromophenol (S)43 %01/23/17 17:44 118-79-601/19/17 15:0027-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 01/20/17 19:53 67-64-196.0 1
Benzene ND ug/kg 01/20/17 19:53 71-43-24.8 1
Bromobenzene ND ug/kg 01/20/17 19:53 108-86-14.8 1
Bromochloromethane ND ug/kg 01/20/17 19:53 74-97-54.8 1
Bromodichloromethane ND ug/kg 01/20/17 19:53 75-27-44.8 1
Bromoform ND ug/kg 01/20/17 19:53 75-25-24.8 1
Bromomethane ND ug/kg 01/20/17 19:53 74-83-99.6 1
2-Butanone (MEK)ND ug/kg 01/20/17 19:53 78-93-396.0 1
n-Butylbenzene ND ug/kg 01/20/17 19:53 104-51-84.8 1
sec-Butylbenzene ND ug/kg 01/20/17 19:53 135-98-84.8 1
tert-Butylbenzene ND ug/kg 01/20/17 19:53 98-06-64.8 1
Carbon tetrachloride ND ug/kg 01/20/17 19:53 56-23-54.8 1
Chlorobenzene ND ug/kg 01/20/17 19:53 108-90-74.8 1
Chloroethane ND ug/kg 01/20/17 19:53 75-00-39.6 1
Chloroform ND ug/kg 01/20/17 19:53 67-66-34.8 1
Chloromethane ND ug/kg 01/20/17 19:53 74-87-39.6 1
2-Chlorotoluene ND ug/kg 01/20/17 19:53 95-49-84.8 1
4-Chlorotoluene ND ug/kg 01/20/17 19:53 106-43-44.8 1
1,2-Dibromo-3-chloropropane ND ug/kg 01/20/17 19:53 96-12-84.8 1
Dibromochloromethane ND ug/kg 01/20/17 19:53 124-48-14.8 1
1,2-Dibromoethane (EDB)ND ug/kg 01/20/17 19:53 106-93-44.8 1
Dibromomethane ND ug/kg 01/20/17 19:53 74-95-34.8 1
1,2-Dichlorobenzene ND ug/kg 01/20/17 19:53 95-50-14.8 1
1,3-Dichlorobenzene ND ug/kg 01/20/17 19:53 541-73-14.8 1
1,4-Dichlorobenzene ND ug/kg 01/20/17 19:53 106-46-74.8 1
Dichlorodifluoromethane ND ug/kg 01/20/17 19:53 75-71-89.6 1
1,1-Dichloroethane ND ug/kg 01/20/17 19:53 75-34-34.8 1
1,2-Dichloroethane ND ug/kg 01/20/17 19:53 107-06-24.8 1
1,1-Dichloroethene ND ug/kg 01/20/17 19:53 75-35-44.8 1
cis-1,2-Dichloroethene ND ug/kg 01/20/17 19:53 156-59-24.8 1
trans-1,2-Dichloroethene ND ug/kg 01/20/17 19:53 156-60-54.8 1
1,2-Dichloropropane ND ug/kg 01/20/17 19:53 78-87-54.8 1
1,3-Dichloropropane ND ug/kg 01/20/17 19:53 142-28-94.8 1
2,2-Dichloropropane ND ug/kg 01/20/17 19:53 594-20-74.8 1
1,1-Dichloropropene ND ug/kg 01/20/17 19:53 563-58-64.8 1
cis-1,3-Dichloropropene ND ug/kg 01/20/17 19:53 10061-01-54.8 1
trans-1,3-Dichloropropene ND ug/kg 01/20/17 19:53 10061-02-64.8 1
Diisopropyl ether ND ug/kg 01/20/17 19:53 108-20-34.8 1
Ethylbenzene ND ug/kg 01/20/17 19:53 100-41-44.8 1
Hexachloro-1,3-butadiene ND ug/kg 01/20/17 19:53 87-68-34.8 1
2-Hexanone ND ug/kg 01/20/17 19:53 591-78-648.0 1
Isopropylbenzene (Cumene)ND ug/kg 01/20/17 19:53 98-82-84.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92326841
NICUS AUTO CARS NAC-1701-1
Sample:SB-1, 20-25'Lab ID:92326841001 Collected:01/18/17 12:04 Received:01/18/17 18:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
p-Isopropyltoluene ND ug/kg 01/20/17 19:53 99-87-64.8 1
Methylene Chloride ND ug/kg 01/20/17 19:53 75-09-219.2 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 01/20/17 19:53 108-10-148.0 1
Methyl-tert-butyl ether ND ug/kg 01/20/17 19:53 1634-04-44.8 1
Naphthalene ND ug/kg 01/20/17 19:53 91-20-34.8 1
n-Propylbenzene ND ug/kg 01/20/17 19:53 103-65-14.8 1
Styrene ND ug/kg 01/20/17 19:53 100-42-54.8 1
1,1,1,2-Tetrachloroethane ND ug/kg 01/20/17 19:53 630-20-64.8 1
1,1,2,2-Tetrachloroethane ND ug/kg 01/20/17 19:53 79-34-54.8 1
Tetrachloroethene ND ug/kg 01/20/17 19:53 127-18-4 L34.8 1
Toluene ND ug/kg 01/20/17 19:53 108-88-34.8 1
1,2,3-Trichlorobenzene ND ug/kg 01/20/17 19:53 87-61-64.8 1
1,2,4-Trichlorobenzene ND ug/kg 01/20/17 19:53 120-82-14.8 1
1,1,1-Trichloroethane ND ug/kg 01/20/17 19:53 71-55-64.8 1
1,1,2-Trichloroethane ND ug/kg 01/20/17 19:53 79-00-54.8 1
Trichloroethene ND ug/kg 01/20/17 19:53 79-01-64.8 1
Trichlorofluoromethane ND ug/kg 01/20/17 19:53 75-69-44.8 1
1,2,3-Trichloropropane ND ug/kg 01/20/17 19:53 96-18-44.8 1
1,2,4-Trimethylbenzene ND ug/kg 01/20/17 19:53 95-63-64.8 1
1,3,5-Trimethylbenzene ND ug/kg 01/20/17 19:53 108-67-84.8 1
Vinyl acetate ND ug/kg 01/20/17 19:53 108-05-448.0 1
Vinyl chloride ND ug/kg 01/20/17 19:53 75-01-49.6 1
Xylene (Total)ND ug/kg 01/20/17 19:53 1330-20-79.6 1
m&p-Xylene ND ug/kg 01/20/17 19:53 179601-23-19.6 1
o-Xylene ND ug/kg 01/20/17 19:53 95-47-64.8 1
Surrogates
Toluene-d8 (S)99 %01/20/17 19:53 2037-26-570-130 1
4-Bromofluorobenzene (S)98 %01/20/17 19:53 460-00-470-130 1
1,2-Dichloroethane-d4 (S)88 %01/20/17 19:53 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 6.8 %01/19/17 08:360.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92326841
NICUS AUTO CARS NAC-1701-1
Sample:SB-1, 38-40'Lab ID:92326841002 Collected:01/18/17 13:55 Received:01/18/17 18:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 01/24/17 22:34 N201/20/17 11:3012.4 1
Aliphatic (C19-C36)ND mg/kg 01/24/17 22:34 N201/20/17 11:3012.4 1
Aromatic (C11-C22)ND mg/kg 01/24/17 22:34 N201/20/17 11:3012.4 1
Surrogates
Nonatriacontane (S)49 %01/24/17 22:34 7194-86-701/20/17 11:3040-140 1
o-Terphenyl (S)45 %01/24/17 22:34 84-15-101/20/17 11:3040-140 1
2-Fluorobiphenyl (S)77 %01/24/17 22:34 321-60-801/20/17 11:3040-140 1
2-Bromonaphthalene (S)58 %01/24/17 22:34 580-13-201/20/17 11:3040-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)ND mg/kg 01/23/17 21:23 N201/23/17 08:373.0 1
Aliphatic (C09-C12)ND mg/kg 01/23/17 21:23 N201/23/17 08:373.0 1
Aromatic (C09-C10)ND mg/kg 01/23/17 21:23 N201/23/17 08:373.0 1
Surrogates
4-Bromofluorobenzene (FID) (S)104 %01/23/17 21:23 460-00-401/23/17 08:3770-130 1
4-Bromofluorobenzene (PID) (S)101 %01/23/17 21:23 460-00-401/23/17 08:3770-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 01/23/17 18:44 83-32-901/19/17 15:004091
Acenaphthylene ND ug/kg 01/23/17 18:44 208-96-801/19/17 15:004091
Aniline ND ug/kg 01/23/17 18:44 62-53-301/19/17 15:004091
Anthracene ND ug/kg 01/23/17 18:44 120-12-701/19/17 15:004091
Benzo(a)anthracene ND ug/kg 01/23/17 18:44 56-55-301/19/17 15:004091
Benzo(a)pyrene ND ug/kg 01/23/17 18:44 50-32-801/19/17 15:004091
Benzo(b)fluoranthene ND ug/kg 01/23/17 18:44 205-99-201/19/17 15:004091
Benzo(g,h,i)perylene ND ug/kg 01/23/17 18:44 191-24-201/19/17 15:004091
Benzo(k)fluoranthene ND ug/kg 01/23/17 18:44 207-08-901/19/17 15:004091
Benzoic Acid ND ug/kg 01/23/17 18:44 65-85-0 L201/19/17 15:0020501
Benzyl alcohol ND ug/kg 01/23/17 18:44 100-51-601/19/17 15:008191
4-Bromophenylphenyl ether ND ug/kg 01/23/17 18:44 101-55-301/19/17 15:004091
Butylbenzylphthalate ND ug/kg 01/23/17 18:44 85-68-701/19/17 15:004091
4-Chloro-3-methylphenol ND ug/kg 01/23/17 18:44 59-50-701/19/17 15:008191
4-Chloroaniline ND ug/kg 01/23/17 18:44 106-47-801/19/17 15:0020501
bis(2-Chloroethoxy)methane ND ug/kg 01/23/17 18:44 111-91-101/19/17 15:004091
bis(2-Chloroethyl) ether ND ug/kg 01/23/17 18:44 111-44-401/19/17 15:004091
2-Chloronaphthalene ND ug/kg 01/23/17 18:44 91-58-701/19/17 15:004091
2-Chlorophenol ND ug/kg 01/23/17 18:44 95-57-801/19/17 15:004091
4-Chlorophenylphenyl ether ND ug/kg 01/23/17 18:44 7005-72-301/19/17 15:004091
Chrysene ND ug/kg 01/23/17 18:44 218-01-901/19/17 15:004091
Dibenz(a,h)anthracene ND ug/kg 01/23/17 18:44 53-70-301/19/17 15:004091
Dibenzofuran ND ug/kg 01/23/17 18:44 132-64-901/19/17 15:004091
1,2-Dichlorobenzene ND ug/kg 01/23/17 18:44 95-50-101/19/17 15:004091
1,3-Dichlorobenzene ND ug/kg 01/23/17 18:44 541-73-1 L201/19/17 15:004091
1,4-Dichlorobenzene ND ug/kg 01/23/17 18:44 106-46-701/19/17 15:004091
3,3'-Dichlorobenzidine ND ug/kg 01/23/17 18:44 91-94-101/19/17 15:0020501
2,4-Dichlorophenol ND ug/kg 01/23/17 18:44 120-83-201/19/17 15:004091
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92326841
NICUS AUTO CARS NAC-1701-1
Sample:SB-1, 38-40'Lab ID:92326841002 Collected:01/18/17 13:55 Received:01/18/17 18:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Diethylphthalate ND ug/kg 01/23/17 18:44 84-66-201/19/17 15:004091
2,4-Dimethylphenol ND ug/kg 01/23/17 18:44 105-67-901/19/17 15:004091
Dimethylphthalate ND ug/kg 01/23/17 18:44 131-11-301/19/17 15:004091
Di-n-butylphthalate ND ug/kg 01/23/17 18:44 84-74-201/19/17 15:004091
4,6-Dinitro-2-methylphenol ND ug/kg 01/23/17 18:44 534-52-101/19/17 15:008191
2,4-Dinitrophenol ND ug/kg 01/23/17 18:44 51-28-5 L201/19/17 15:0020501
2,4-Dinitrotoluene ND ug/kg 01/23/17 18:44 121-14-201/19/17 15:004091
2,6-Dinitrotoluene ND ug/kg 01/23/17 18:44 606-20-201/19/17 15:004091
Di-n-octylphthalate ND ug/kg 01/23/17 18:44 117-84-001/19/17 15:004091
bis(2-Ethylhexyl)phthalate ND ug/kg 01/23/17 18:44 117-81-701/19/17 15:004091
Fluoranthene ND ug/kg 01/23/17 18:44 206-44-001/19/17 15:004091
Fluorene ND ug/kg 01/23/17 18:44 86-73-701/19/17 15:004091
Hexachloro-1,3-butadiene ND ug/kg 01/23/17 18:44 87-68-301/19/17 15:004091
Hexachlorobenzene ND ug/kg 01/23/17 18:44 118-74-101/19/17 15:004091
Hexachlorocyclopentadiene ND ug/kg 01/23/17 18:44 77-47-401/19/17 15:004091
Hexachloroethane ND ug/kg 01/23/17 18:44 67-72-101/19/17 15:004091
Indeno(1,2,3-cd)pyrene ND ug/kg 01/23/17 18:44 193-39-501/19/17 15:004091
Isophorone ND ug/kg 01/23/17 18:44 78-59-101/19/17 15:004091
1-Methylnaphthalene ND ug/kg 01/23/17 18:44 90-12-001/19/17 15:004091
2-Methylnaphthalene ND ug/kg 01/23/17 18:44 91-57-601/19/17 15:004091
2-Methylphenol(o-Cresol)ND ug/kg 01/23/17 18:44 95-48-701/19/17 15:004091
3&4-Methylphenol(m&p Cresol)ND ug/kg 01/23/17 18:4401/19/17 15:004091
Naphthalene ND ug/kg 01/23/17 18:44 91-20-301/19/17 15:004091
2-Nitroaniline ND ug/kg 01/23/17 18:44 88-74-401/19/17 15:0020501
3-Nitroaniline ND ug/kg 01/23/17 18:44 99-09-201/19/17 15:0020501
4-Nitroaniline ND ug/kg 01/23/17 18:44 100-01-601/19/17 15:008191
Nitrobenzene ND ug/kg 01/23/17 18:44 98-95-301/19/17 15:004091
2-Nitrophenol ND ug/kg 01/23/17 18:44 88-75-501/19/17 15:004091
4-Nitrophenol ND ug/kg 01/23/17 18:44 100-02-701/19/17 15:0020501
N-Nitrosodimethylamine ND ug/kg 01/23/17 18:44 62-75-901/19/17 15:004091
N-Nitroso-di-n-propylamine ND ug/kg 01/23/17 18:44 621-64-701/19/17 15:004091
N-Nitrosodiphenylamine ND ug/kg 01/23/17 18:44 86-30-601/19/17 15:004091
2,2'-Oxybis(1-chloropropane)ND ug/kg 01/23/17 18:44 108-60-101/19/17 15:004091
Pentachlorophenol ND ug/kg 01/23/17 18:44 87-86-501/19/17 15:0020501
Phenanthrene ND ug/kg 01/23/17 18:44 85-01-801/19/17 15:004091
Phenol ND ug/kg 01/23/17 18:4401/19/17 15:004091
Pyrene ND ug/kg 01/23/17 18:44 129-00-001/19/17 15:004091
1,2,4-Trichlorobenzene ND ug/kg 01/23/17 18:44 120-82-101/19/17 15:004091
2,4,5-Trichlorophenol ND ug/kg 01/23/17 18:44 95-95-401/19/17 15:004091
2,4,6-Trichlorophenol ND ug/kg 01/23/17 18:44 88-06-201/19/17 15:004091
Surrogates
Nitrobenzene-d5 (S)44 %01/23/17 18:44 4165-60-001/19/17 15:0023-110 1
2-Fluorobiphenyl (S)40 %01/23/17 18:44 321-60-801/19/17 15:0030-110 1
Terphenyl-d14 (S)58 %01/23/17 18:44 1718-51-001/19/17 15:0028-110 1
Phenol-d6 (S)43 %01/23/17 18:44 13127-88-301/19/17 15:0022-110 1
2-Fluorophenol (S)45 %01/23/17 18:44 367-12-401/19/17 15:0013-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92326841
NICUS AUTO CARS NAC-1701-1
Sample:SB-1, 38-40'Lab ID:92326841002 Collected:01/18/17 13:55 Received:01/18/17 18:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
2,4,6-Tribromophenol (S)40 %01/23/17 18:44 118-79-601/19/17 15:0027-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 01/19/17 19:00 67-64-190.4 1
Benzene ND ug/kg 01/19/17 19:00 71-43-24.5 1
Bromobenzene ND ug/kg 01/19/17 19:00 108-86-14.5 1
Bromochloromethane ND ug/kg 01/19/17 19:00 74-97-54.5 1
Bromodichloromethane ND ug/kg 01/19/17 19:00 75-27-44.5 1
Bromoform ND ug/kg 01/19/17 19:00 75-25-24.5 1
Bromomethane ND ug/kg 01/19/17 19:00 74-83-99.0 1
2-Butanone (MEK)ND ug/kg 01/19/17 19:00 78-93-390.4 1
n-Butylbenzene ND ug/kg 01/19/17 19:00 104-51-84.5 1
sec-Butylbenzene ND ug/kg 01/19/17 19:00 135-98-84.5 1
tert-Butylbenzene ND ug/kg 01/19/17 19:00 98-06-64.5 1
Carbon tetrachloride ND ug/kg 01/19/17 19:00 56-23-54.5 1
Chlorobenzene ND ug/kg 01/19/17 19:00 108-90-74.5 1
Chloroethane ND ug/kg 01/19/17 19:00 75-00-39.0 1
Chloroform ND ug/kg 01/19/17 19:00 67-66-34.5 1
Chloromethane ND ug/kg 01/19/17 19:00 74-87-39.0 1
2-Chlorotoluene ND ug/kg 01/19/17 19:00 95-49-84.5 1
4-Chlorotoluene ND ug/kg 01/19/17 19:00 106-43-44.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 01/19/17 19:00 96-12-84.5 1
Dibromochloromethane ND ug/kg 01/19/17 19:00 124-48-14.5 1
1,2-Dibromoethane (EDB)ND ug/kg 01/19/17 19:00 106-93-44.5 1
Dibromomethane ND ug/kg 01/19/17 19:00 74-95-34.5 1
1,2-Dichlorobenzene ND ug/kg 01/19/17 19:00 95-50-14.5 1
1,3-Dichlorobenzene ND ug/kg 01/19/17 19:00 541-73-14.5 1
1,4-Dichlorobenzene ND ug/kg 01/19/17 19:00 106-46-74.5 1
Dichlorodifluoromethane ND ug/kg 01/19/17 19:00 75-71-89.0 1
1,1-Dichloroethane ND ug/kg 01/19/17 19:00 75-34-34.5 1
1,2-Dichloroethane ND ug/kg 01/19/17 19:00 107-06-24.5 1
1,1-Dichloroethene ND ug/kg 01/19/17 19:00 75-35-44.5 1
cis-1,2-Dichloroethene ND ug/kg 01/19/17 19:00 156-59-24.5 1
trans-1,2-Dichloroethene ND ug/kg 01/19/17 19:00 156-60-54.5 1
1,2-Dichloropropane ND ug/kg 01/19/17 19:00 78-87-54.5 1
1,3-Dichloropropane ND ug/kg 01/19/17 19:00 142-28-94.5 1
2,2-Dichloropropane ND ug/kg 01/19/17 19:00 594-20-74.5 1
1,1-Dichloropropene ND ug/kg 01/19/17 19:00 563-58-64.5 1
cis-1,3-Dichloropropene ND ug/kg 01/19/17 19:00 10061-01-54.5 1
trans-1,3-Dichloropropene ND ug/kg 01/19/17 19:00 10061-02-64.5 1
Diisopropyl ether ND ug/kg 01/19/17 19:00 108-20-34.5 1
Ethylbenzene 7.5 ug/kg 01/19/17 19:00 100-41-44.5 1
Hexachloro-1,3-butadiene ND ug/kg 01/19/17 19:00 87-68-34.5 1
2-Hexanone ND ug/kg 01/19/17 19:00 591-78-645.2 1
Isopropylbenzene (Cumene)ND ug/kg 01/19/17 19:00 98-82-84.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92326841
NICUS AUTO CARS NAC-1701-1
Sample:SB-1, 38-40'Lab ID:92326841002 Collected:01/18/17 13:55 Received:01/18/17 18:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
p-Isopropyltoluene ND ug/kg 01/19/17 19:00 99-87-64.5 1
Methylene Chloride ND ug/kg 01/19/17 19:00 75-09-2 B18.1 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 01/19/17 19:00 108-10-145.2 1
Methyl-tert-butyl ether 5.7 ug/kg 01/19/17 19:00 1634-04-44.5 1
Naphthalene 6.6 ug/kg 01/19/17 19:00 91-20-34.5 1
n-Propylbenzene ND ug/kg 01/19/17 19:00 103-65-14.5 1
Styrene ND ug/kg 01/19/17 19:00 100-42-54.5 1
1,1,1,2-Tetrachloroethane ND ug/kg 01/19/17 19:00 630-20-64.5 1
1,1,2,2-Tetrachloroethane ND ug/kg 01/19/17 19:00 79-34-54.5 1
Tetrachloroethene ND ug/kg 01/19/17 19:00 127-18-4 L34.5 1
Toluene 22.3 ug/kg 01/19/17 19:00 108-88-34.5 1
1,2,3-Trichlorobenzene ND ug/kg 01/19/17 19:00 87-61-64.5 1
1,2,4-Trichlorobenzene ND ug/kg 01/19/17 19:00 120-82-14.5 1
1,1,1-Trichloroethane ND ug/kg 01/19/17 19:00 71-55-64.5 1
1,1,2-Trichloroethane ND ug/kg 01/19/17 19:00 79-00-54.5 1
Trichloroethene ND ug/kg 01/19/17 19:00 79-01-64.5 1
Trichlorofluoromethane ND ug/kg 01/19/17 19:00 75-69-44.5 1
1,2,3-Trichloropropane ND ug/kg 01/19/17 19:00 96-18-44.5 1
1,2,4-Trimethylbenzene 16.2 ug/kg 01/19/17 19:00 95-63-64.5 1
1,3,5-Trimethylbenzene ND ug/kg 01/19/17 19:00 108-67-84.5 1
Vinyl acetate ND ug/kg 01/19/17 19:00 108-05-445.2 1
Vinyl chloride ND ug/kg 01/19/17 19:00 75-01-49.0 1
Xylene (Total)70.0 ug/kg 01/19/17 19:00 1330-20-79.0 1
m&p-Xylene 41.9 ug/kg 01/19/17 19:00 179601-23-19.0 1
o-Xylene 28.1 ug/kg 01/19/17 19:00 95-47-64.5 1
Surrogates
Toluene-d8 (S)98 %01/19/17 19:00 2037-26-570-130 1
4-Bromofluorobenzene (S)100 %01/19/17 19:00 460-00-470-130 1
1,2-Dichloroethane-d4 (S)80 %01/19/17 19:00 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 19.4 %01/19/17 08:370.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92326841
NICUS AUTO CARS NAC-1701-1
Sample:SB-1, 48-50'Lab ID:92326841003 Collected:01/18/17 15:20 Received:01/18/17 18:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 01/25/17 21:01 N201/20/17 11:3026.3 2
Aliphatic (C19-C36)74.5 mg/kg 01/25/17 21:01 N201/20/17 11:3026.3 2
Aromatic (C11-C22)ND mg/kg 01/25/17 21:01 N201/20/17 11:3013.1 1
Surrogates
Nonatriacontane (S)49 %01/25/17 21:01 7194-86-701/20/17 11:3040-140 2
o-Terphenyl (S)55 %01/25/17 21:01 84-15-101/20/17 11:3040-140 1
2-Fluorobiphenyl (S)85 %01/25/17 21:01 321-60-801/20/17 11:3040-140 1
2-Bromonaphthalene (S)74 %01/25/17 21:01 580-13-201/20/17 11:3040-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)ND mg/kg 01/23/17 21:51 N201/23/17 08:372.8 1
Aliphatic (C09-C12)ND mg/kg 01/23/17 21:51 N201/23/17 08:372.8 1
Aromatic (C09-C10)ND mg/kg 01/23/17 21:51 N201/23/17 08:372.8 1
Surrogates
4-Bromofluorobenzene (FID) (S)100 %01/23/17 21:51 460-00-401/23/17 08:3770-130 1
4-Bromofluorobenzene (PID) (S)97 %01/23/17 21:51 460-00-401/23/17 08:3770-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 01/23/17 19:45 83-32-901/19/17 15:004341
Acenaphthylene ND ug/kg 01/23/17 19:45 208-96-801/19/17 15:004341
Aniline ND ug/kg 01/23/17 19:45 62-53-301/19/17 15:004341
Anthracene ND ug/kg 01/23/17 19:45 120-12-701/19/17 15:004341
Benzo(a)anthracene ND ug/kg 01/23/17 19:45 56-55-301/19/17 15:004341
Benzo(a)pyrene ND ug/kg 01/23/17 19:45 50-32-801/19/17 15:004341
Benzo(b)fluoranthene ND ug/kg 01/23/17 19:45 205-99-201/19/17 15:004341
Benzo(g,h,i)perylene ND ug/kg 01/23/17 19:45 191-24-201/19/17 15:004341
Benzo(k)fluoranthene ND ug/kg 01/23/17 19:45 207-08-901/19/17 15:004341
Benzoic Acid ND ug/kg 01/23/17 19:45 65-85-0 L201/19/17 15:0021701
Benzyl alcohol ND ug/kg 01/23/17 19:45 100-51-601/19/17 15:008671
4-Bromophenylphenyl ether ND ug/kg 01/23/17 19:45 101-55-301/19/17 15:004341
Butylbenzylphthalate ND ug/kg 01/23/17 19:45 85-68-701/19/17 15:004341
4-Chloro-3-methylphenol ND ug/kg 01/23/17 19:45 59-50-701/19/17 15:008671
4-Chloroaniline ND ug/kg 01/23/17 19:45 106-47-801/19/17 15:0021701
bis(2-Chloroethoxy)methane ND ug/kg 01/23/17 19:45 111-91-101/19/17 15:004341
bis(2-Chloroethyl) ether ND ug/kg 01/23/17 19:45 111-44-401/19/17 15:004341
2-Chloronaphthalene ND ug/kg 01/23/17 19:45 91-58-701/19/17 15:004341
2-Chlorophenol ND ug/kg 01/23/17 19:45 95-57-801/19/17 15:004341
4-Chlorophenylphenyl ether ND ug/kg 01/23/17 19:45 7005-72-301/19/17 15:004341
Chrysene ND ug/kg 01/23/17 19:45 218-01-901/19/17 15:004341
Dibenz(a,h)anthracene ND ug/kg 01/23/17 19:45 53-70-301/19/17 15:004341
Dibenzofuran ND ug/kg 01/23/17 19:45 132-64-901/19/17 15:004341
1,2-Dichlorobenzene ND ug/kg 01/23/17 19:45 95-50-101/19/17 15:004341
1,3-Dichlorobenzene ND ug/kg 01/23/17 19:45 541-73-1 L201/19/17 15:004341
1,4-Dichlorobenzene ND ug/kg 01/23/17 19:45 106-46-701/19/17 15:004341
3,3'-Dichlorobenzidine ND ug/kg 01/23/17 19:45 91-94-101/19/17 15:0021701
2,4-Dichlorophenol ND ug/kg 01/23/17 19:45 120-83-201/19/17 15:004341
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92326841
NICUS AUTO CARS NAC-1701-1
Sample:SB-1, 48-50'Lab ID:92326841003 Collected:01/18/17 15:20 Received:01/18/17 18:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Diethylphthalate ND ug/kg 01/23/17 19:45 84-66-201/19/17 15:004341
2,4-Dimethylphenol ND ug/kg 01/23/17 19:45 105-67-901/19/17 15:004341
Dimethylphthalate ND ug/kg 01/23/17 19:45 131-11-301/19/17 15:004341
Di-n-butylphthalate ND ug/kg 01/23/17 19:45 84-74-201/19/17 15:004341
4,6-Dinitro-2-methylphenol ND ug/kg 01/23/17 19:45 534-52-101/19/17 15:008671
2,4-Dinitrophenol ND ug/kg 01/23/17 19:45 51-28-5 L201/19/17 15:0021701
2,4-Dinitrotoluene ND ug/kg 01/23/17 19:45 121-14-201/19/17 15:004341
2,6-Dinitrotoluene ND ug/kg 01/23/17 19:45 606-20-201/19/17 15:004341
Di-n-octylphthalate ND ug/kg 01/23/17 19:45 117-84-001/19/17 15:004341
bis(2-Ethylhexyl)phthalate ND ug/kg 01/23/17 19:45 117-81-701/19/17 15:004341
Fluoranthene ND ug/kg 01/23/17 19:45 206-44-001/19/17 15:004341
Fluorene ND ug/kg 01/23/17 19:45 86-73-701/19/17 15:004341
Hexachloro-1,3-butadiene ND ug/kg 01/23/17 19:45 87-68-301/19/17 15:004341
Hexachlorobenzene ND ug/kg 01/23/17 19:45 118-74-101/19/17 15:004341
Hexachlorocyclopentadiene ND ug/kg 01/23/17 19:45 77-47-401/19/17 15:004341
Hexachloroethane ND ug/kg 01/23/17 19:45 67-72-101/19/17 15:004341
Indeno(1,2,3-cd)pyrene ND ug/kg 01/23/17 19:45 193-39-501/19/17 15:004341
Isophorone ND ug/kg 01/23/17 19:45 78-59-101/19/17 15:004341
1-Methylnaphthalene ND ug/kg 01/23/17 19:45 90-12-001/19/17 15:004341
2-Methylnaphthalene ND ug/kg 01/23/17 19:45 91-57-601/19/17 15:004341
2-Methylphenol(o-Cresol)ND ug/kg 01/23/17 19:45 95-48-701/19/17 15:004341
3&4-Methylphenol(m&p Cresol)ND ug/kg 01/23/17 19:4501/19/17 15:004341
Naphthalene ND ug/kg 01/23/17 19:45 91-20-301/19/17 15:004341
2-Nitroaniline ND ug/kg 01/23/17 19:45 88-74-401/19/17 15:0021701
3-Nitroaniline ND ug/kg 01/23/17 19:45 99-09-201/19/17 15:0021701
4-Nitroaniline ND ug/kg 01/23/17 19:45 100-01-601/19/17 15:008671
Nitrobenzene ND ug/kg 01/23/17 19:45 98-95-301/19/17 15:004341
2-Nitrophenol ND ug/kg 01/23/17 19:45 88-75-501/19/17 15:004341
4-Nitrophenol ND ug/kg 01/23/17 19:45 100-02-701/19/17 15:0021701
N-Nitrosodimethylamine ND ug/kg 01/23/17 19:45 62-75-901/19/17 15:004341
N-Nitroso-di-n-propylamine ND ug/kg 01/23/17 19:45 621-64-701/19/17 15:004341
N-Nitrosodiphenylamine ND ug/kg 01/23/17 19:45 86-30-601/19/17 15:004341
2,2'-Oxybis(1-chloropropane)ND ug/kg 01/23/17 19:45 108-60-101/19/17 15:004341
Pentachlorophenol ND ug/kg 01/23/17 19:45 87-86-501/19/17 15:0021701
Phenanthrene ND ug/kg 01/23/17 19:45 85-01-801/19/17 15:004341
Phenol ND ug/kg 01/23/17 19:4501/19/17 15:004341
Pyrene ND ug/kg 01/23/17 19:45 129-00-001/19/17 15:004341
1,2,4-Trichlorobenzene ND ug/kg 01/23/17 19:45 120-82-101/19/17 15:004341
2,4,5-Trichlorophenol ND ug/kg 01/23/17 19:45 95-95-401/19/17 15:004341
2,4,6-Trichlorophenol ND ug/kg 01/23/17 19:45 88-06-201/19/17 15:004341
Surrogates
Nitrobenzene-d5 (S)54 %01/23/17 19:45 4165-60-001/19/17 15:0023-110 1
2-Fluorobiphenyl (S)36 %01/23/17 19:45 321-60-801/19/17 15:0030-110 1
Terphenyl-d14 (S)55 %01/23/17 19:45 1718-51-001/19/17 15:0028-110 1
Phenol-d6 (S)29 %01/23/17 19:45 13127-88-301/19/17 15:0022-110 1
2-Fluorophenol (S)29 %01/23/17 19:45 367-12-401/19/17 15:0013-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92326841
NICUS AUTO CARS NAC-1701-1
Sample:SB-1, 48-50'Lab ID:92326841003 Collected:01/18/17 15:20 Received:01/18/17 18:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
2,4,6-Tribromophenol (S)25 %01/23/17 19:45 118-79-6 S001/19/17 15:0027-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 01/19/17 19:21 67-64-11081
Benzene 5.7 ug/kg 01/19/17 19:21 71-43-25.4 1
Bromobenzene ND ug/kg 01/19/17 19:21 108-86-15.4 1
Bromochloromethane ND ug/kg 01/19/17 19:21 74-97-55.4 1
Bromodichloromethane ND ug/kg 01/19/17 19:21 75-27-45.4 1
Bromoform ND ug/kg 01/19/17 19:21 75-25-25.4 1
Bromomethane ND ug/kg 01/19/17 19:21 74-83-910.8 1
2-Butanone (MEK)ND ug/kg 01/19/17 19:21 78-93-31081
n-Butylbenzene ND ug/kg 01/19/17 19:21 104-51-85.4 1
sec-Butylbenzene ND ug/kg 01/19/17 19:21 135-98-85.4 1
tert-Butylbenzene ND ug/kg 01/19/17 19:21 98-06-65.4 1
Carbon tetrachloride ND ug/kg 01/19/17 19:21 56-23-55.4 1
Chlorobenzene ND ug/kg 01/19/17 19:21 108-90-75.4 1
Chloroethane ND ug/kg 01/19/17 19:21 75-00-310.8 1
Chloroform ND ug/kg 01/19/17 19:21 67-66-35.4 1
Chloromethane ND ug/kg 01/19/17 19:21 74-87-310.8 1
2-Chlorotoluene ND ug/kg 01/19/17 19:21 95-49-85.4 1
4-Chlorotoluene ND ug/kg 01/19/17 19:21 106-43-45.4 1
1,2-Dibromo-3-chloropropane ND ug/kg 01/19/17 19:21 96-12-85.4 1
Dibromochloromethane ND ug/kg 01/19/17 19:21 124-48-15.4 1
1,2-Dibromoethane (EDB)ND ug/kg 01/19/17 19:21 106-93-45.4 1
Dibromomethane ND ug/kg 01/19/17 19:21 74-95-35.4 1
1,2-Dichlorobenzene ND ug/kg 01/19/17 19:21 95-50-15.4 1
1,3-Dichlorobenzene ND ug/kg 01/19/17 19:21 541-73-15.4 1
1,4-Dichlorobenzene ND ug/kg 01/19/17 19:21 106-46-75.4 1
Dichlorodifluoromethane ND ug/kg 01/19/17 19:21 75-71-810.8 1
1,1-Dichloroethane ND ug/kg 01/19/17 19:21 75-34-35.4 1
1,2-Dichloroethane ND ug/kg 01/19/17 19:21 107-06-25.4 1
1,1-Dichloroethene ND ug/kg 01/19/17 19:21 75-35-45.4 1
cis-1,2-Dichloroethene ND ug/kg 01/19/17 19:21 156-59-25.4 1
trans-1,2-Dichloroethene ND ug/kg 01/19/17 19:21 156-60-55.4 1
1,2-Dichloropropane ND ug/kg 01/19/17 19:21 78-87-55.4 1
1,3-Dichloropropane ND ug/kg 01/19/17 19:21 142-28-95.4 1
2,2-Dichloropropane ND ug/kg 01/19/17 19:21 594-20-75.4 1
1,1-Dichloropropene ND ug/kg 01/19/17 19:21 563-58-65.4 1
cis-1,3-Dichloropropene ND ug/kg 01/19/17 19:21 10061-01-55.4 1
trans-1,3-Dichloropropene ND ug/kg 01/19/17 19:21 10061-02-65.4 1
Diisopropyl ether ND ug/kg 01/19/17 19:21 108-20-35.4 1
Ethylbenzene 48.8 ug/kg 01/19/17 19:21 100-41-45.4 1
Hexachloro-1,3-butadiene ND ug/kg 01/19/17 19:21 87-68-35.4 1
2-Hexanone ND ug/kg 01/19/17 19:21 591-78-654.1 1
Isopropylbenzene (Cumene)ND ug/kg 01/19/17 19:21 98-82-85.4 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/27/2017 09:20 AM
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Page 14 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92326841
NICUS AUTO CARS NAC-1701-1
Sample:SB-1, 48-50'Lab ID:92326841003 Collected:01/18/17 15:20 Received:01/18/17 18:10 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
p-Isopropyltoluene ND ug/kg 01/19/17 19:21 99-87-65.4 1
Methylene Chloride ND ug/kg 01/19/17 19:21 75-09-2 B21.7 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 01/19/17 19:21 108-10-154.1 1
Methyl-tert-butyl ether ND ug/kg 01/19/17 19:21 1634-04-45.4 1
Naphthalene ND ug/kg 01/19/17 19:21 91-20-35.4 1
n-Propylbenzene 14.2 ug/kg 01/19/17 19:21 103-65-15.4 1
Styrene ND ug/kg 01/19/17 19:21 100-42-55.4 1
1,1,1,2-Tetrachloroethane ND ug/kg 01/19/17 19:21 630-20-65.4 1
1,1,2,2-Tetrachloroethane ND ug/kg 01/19/17 19:21 79-34-55.4 1
Tetrachloroethene ND ug/kg 01/19/17 19:21 127-18-4 L35.4 1
Toluene 72.3 ug/kg 01/19/17 19:21 108-88-35.4 1
1,2,3-Trichlorobenzene ND ug/kg 01/19/17 19:21 87-61-65.4 1
1,2,4-Trichlorobenzene ND ug/kg 01/19/17 19:21 120-82-15.4 1
1,1,1-Trichloroethane ND ug/kg 01/19/17 19:21 71-55-65.4 1
1,1,2-Trichloroethane ND ug/kg 01/19/17 19:21 79-00-55.4 1
Trichloroethene ND ug/kg 01/19/17 19:21 79-01-65.4 1
Trichlorofluoromethane ND ug/kg 01/19/17 19:21 75-69-45.4 1
1,2,3-Trichloropropane ND ug/kg 01/19/17 19:21 96-18-45.4 1
1,2,4-Trimethylbenzene 99.2 ug/kg 01/19/17 19:21 95-63-65.4 1
1,3,5-Trimethylbenzene 37.4 ug/kg 01/19/17 19:21 108-67-85.4 1
Vinyl acetate ND ug/kg 01/19/17 19:21 108-05-454.1 1
Vinyl chloride ND ug/kg 01/19/17 19:21 75-01-410.8 1
Xylene (Total)366 ug/kg 01/19/17 19:21 1330-20-710.8 1
m&p-Xylene 259 ug/kg 01/19/17 19:21 179601-23-110.8 1
o-Xylene 107 ug/kg 01/19/17 19:21 95-47-65.4 1
Surrogates
Toluene-d8 (S)100 %01/19/17 19:21 2037-26-570-130 1
4-Bromofluorobenzene (S)96 %01/19/17 19:21 460-00-470-130 1
1,2-Dichloroethane-d4 (S)80 %01/19/17 19:21 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 23.9 %01/19/17 08:370.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/27/2017 09:20 AM
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Page 15 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92326841
NICUS AUTO CARS NAC-1701-1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
345240
MADEP VPH
MADEP VPH
VPH NC Soil
Associated Lab Samples:92326841001, 92326841002, 92326841003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1915486
Associated Lab Samples:92326841001, 92326841002, 92326841003
Matrix:Solid
Analyzed
Aliphatic (C05-C08)mg/kg ND 2.5 N201/23/17 16:13
Aliphatic (C09-C12)mg/kg ND 2.5 N201/23/17 16:13
Aromatic (C09-C10)mg/kg ND 2.5 N201/23/17 16:13
4-Bromofluorobenzene (FID) (S)%94 70-130 01/23/17 16:13
4-Bromofluorobenzene (PID) (S)%92 70-130 01/23/17 16:13
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1915487LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1915488
Aliphatic (C05-C08)mg/kg 15.4 N21510370-13010015.1 2 25
Aliphatic (C09-C12)mg/kg 14.2 N2159430-13010015.0 6 25
Aromatic (C09-C10)mg/kg 4.7 N259370-130934.6 0 25
4-Bromofluorobenzene (FID) (S)%97 70-130103
4-Bromofluorobenzene (PID) (S)%94 70-130100
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/27/2017 09:20 AM
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Page 16 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92326841
NICUS AUTO CARS NAC-1701-1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
344891
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:92326841002, 92326841003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1913606
Associated Lab Samples:92326841002, 92326841003
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 11.0 01/19/17 13:54
1,1,1-Trichloroethane ug/kg ND 11.0 01/19/17 13:54
1,1,2,2-Tetrachloroethane ug/kg ND 11.0 01/19/17 13:54
1,1,2-Trichloroethane ug/kg ND 11.0 01/19/17 13:54
1,1-Dichloroethane ug/kg ND 11.0 01/19/17 13:54
1,1-Dichloroethene ug/kg ND 11.0 01/19/17 13:54
1,1-Dichloropropene ug/kg ND 11.0 01/19/17 13:54
1,2,3-Trichlorobenzene ug/kg ND 11.0 01/19/17 13:54
1,2,3-Trichloropropane ug/kg ND 11.0 01/19/17 13:54
1,2,4-Trichlorobenzene ug/kg ND 11.0 01/19/17 13:54
1,2,4-Trimethylbenzene ug/kg ND 11.0 01/19/17 13:54
1,2-Dibromo-3-chloropropane ug/kg ND 11.0 01/19/17 13:54
1,2-Dibromoethane (EDB)ug/kg ND 11.0 01/19/17 13:54
1,2-Dichlorobenzene ug/kg ND 11.0 01/19/17 13:54
1,2-Dichloroethane ug/kg ND 11.0 01/19/17 13:54
1,2-Dichloropropane ug/kg ND 11.0 01/19/17 13:54
1,3,5-Trimethylbenzene ug/kg ND 11.0 01/19/17 13:54
1,3-Dichlorobenzene ug/kg ND 11.0 01/19/17 13:54
1,3-Dichloropropane ug/kg ND 11.0 01/19/17 13:54
1,4-Dichlorobenzene ug/kg ND 11.0 01/19/17 13:54
2,2-Dichloropropane ug/kg ND 11.0 01/19/17 13:54
2-Butanone (MEK)ug/kg ND 219 01/19/17 13:54
2-Chlorotoluene ug/kg ND 11.0 01/19/17 13:54
2-Hexanone ug/kg ND 110 01/19/17 13:54
4-Chlorotoluene ug/kg ND 11.0 01/19/17 13:54
4-Methyl-2-pentanone (MIBK)ug/kg ND 110 01/19/17 13:54
Acetone ug/kg ND 219 01/19/17 13:54
Benzene ug/kg ND 11.0 01/19/17 13:54
Bromobenzene ug/kg ND 11.0 01/19/17 13:54
Bromochloromethane ug/kg ND 11.0 01/19/17 13:54
Bromodichloromethane ug/kg ND 11.0 01/19/17 13:54
Bromoform ug/kg ND 11.0 01/19/17 13:54
Bromomethane ug/kg ND 21.9 01/19/17 13:54
Carbon tetrachloride ug/kg ND 11.0 01/19/17 13:54
Chlorobenzene ug/kg ND 11.0 01/19/17 13:54
Chloroethane ug/kg ND 21.9 01/19/17 13:54
Chloroform ug/kg ND 11.0 01/19/17 13:54
Chloromethane ug/kg ND 21.9 01/19/17 13:54
cis-1,2-Dichloroethene ug/kg ND 11.0 01/19/17 13:54
cis-1,3-Dichloropropene ug/kg ND 11.0 01/19/17 13:54
Dibromochloromethane ug/kg ND 11.0 01/19/17 13:54
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/27/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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[phone]
Page 17 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92326841
NICUS AUTO CARS NAC-1701-1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1913606
Associated Lab Samples:92326841002, 92326841003
Matrix:Solid
Analyzed
Dibromomethane ug/kg ND 11.0 01/19/17 13:54
Dichlorodifluoromethane ug/kg ND 21.9 01/19/17 13:54
Diisopropyl ether ug/kg ND 11.0 01/19/17 13:54
Ethylbenzene ug/kg ND 11.0 01/19/17 13:54
Hexachloro-1,3-butadiene ug/kg ND 11.0 01/19/17 13:54
Isopropylbenzene (Cumene)ug/kg ND 11.0 01/19/17 13:54
m&p-Xylene ug/kg ND 21.9 01/19/17 13:54
Methyl-tert-butyl ether ug/kg ND 11.0 01/19/17 13:54
Methylene Chloride ug/kg ND 43.9 01/19/17 13:54
n-Butylbenzene ug/kg ND 11.0 01/19/17 13:54
n-Propylbenzene ug/kg ND 11.0 01/19/17 13:54
Naphthalene ug/kg ND 11.0 01/19/17 13:54
o-Xylene ug/kg ND 11.0 01/19/17 13:54
p-Isopropyltoluene ug/kg ND 11.0 01/19/17 13:54
sec-Butylbenzene ug/kg ND 11.0 01/19/17 13:54
Styrene ug/kg ND 11.0 01/19/17 13:54
tert-Butylbenzene ug/kg ND 11.0 01/19/17 13:54
Tetrachloroethene ug/kg ND 11.0 01/19/17 13:54
Toluene ug/kg ND 11.0 01/19/17 13:54
trans-1,2-Dichloroethene ug/kg ND 11.0 01/19/17 13:54
trans-1,3-Dichloropropene ug/kg ND 11.0 01/19/17 13:54
Trichloroethene ug/kg ND 11.0 01/19/17 13:54
Trichlorofluoromethane ug/kg ND 11.0 01/19/17 13:54
Vinyl acetate ug/kg ND 110 01/19/17 13:54
Vinyl chloride ug/kg ND 21.9 01/19/17 13:54
Xylene (Total)ug/kg ND 21.9 01/19/17 13:54
1,2-Dichloroethane-d4 (S)%98 70-132 01/19/17 13:54
4-Bromofluorobenzene (S)%104 70-130 01/19/17 13:54
Toluene-d8 (S)%102 70-130 01/19/17 13:54
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1913607LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 76.971.2 108 74-137
1,1,1-Trichloroethane ug/kg 68.571.2 96 67-140
1,1,2,2-Tetrachloroethane ug/kg 71.371.2 100 72-141
1,1,2-Trichloroethane ug/kg 75.871.2 106 78-138
1,1-Dichloroethane ug/kg 65.671.2 92 69-134
1,1-Dichloroethene ug/kg 65.971.2 93 67-138
1,1-Dichloropropene ug/kg 72.371.2 102 69-139
1,2,3-Trichlorobenzene ug/kg 83.271.2 117 70-146
1,2,3-Trichloropropane ug/kg 77.871.2 109 69-144
1,2,4-Trichlorobenzene ug/kg 82.071.2 115 68-148
1,2,4-Trimethylbenzene ug/kg 75.671.2 106 74-137
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/27/2017 09:20 AM
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Huntersville, NC 28078
[phone]
Page 18 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92326841
NICUS AUTO CARS NAC-1701-1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1913607LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/kg 82.971.2 116 65-140
1,2-Dibromoethane (EDB)ug/kg 75.371.2 106 77-135
1,2-Dichlorobenzene ug/kg 79.871.2 112 77-141
1,2-Dichloroethane ug/kg 68.571.2 96 65-137
1,2-Dichloropropane ug/kg 72.771.2 102 72-136
1,3,5-Trimethylbenzene ug/kg 74.471.2 104 76-133
1,3-Dichlorobenzene ug/kg 77.671.2 109 74-138
1,3-Dichloropropane ug/kg 77.371.2 108 71-139
1,4-Dichlorobenzene ug/kg 76.971.2 108 76-138
2,2-Dichloropropane ug/kg 67.771.2 95 68-137
2-Butanone (MEK)ug/kg 143142 100 58-147
2-Chlorotoluene ug/kg 75.671.2 106 73-139
2-Hexanone ug/kg 171142 120 62-145
4-Chlorotoluene ug/kg 76.371.2 107 76-141
4-Methyl-2-pentanone (MIBK)ug/kg 160142 113 64-149
Acetone ug/kg 137J142 96 53-153
Benzene ug/kg 72.871.2 102 73-135
Bromobenzene ug/kg 77.471.2 109 75-133
Bromochloromethane ug/kg 69.771.2 98 73-134
Bromodichloromethane ug/kg 76.271.2 107 71-135
Bromoform ug/kg 84.671.2 119 66-141
Bromomethane ug/kg 69.371.2 97 53-160
Carbon tetrachloride ug/kg 70.471.2 99 60-145
Chlorobenzene ug/kg 73.771.2 103 78-130
Chloroethane ug/kg 69.871.2 98 64-149
Chloroform ug/kg 67.571.2 95 70-134
Chloromethane ug/kg 72.671.2 102 52-150
cis-1,2-Dichloroethene ug/kg 67.671.2 95 70-133
cis-1,3-Dichloropropene ug/kg 75.971.2 107 68-134
Dibromochloromethane ug/kg 80.871.2 113 71-138
Dibromomethane ug/kg 69.871.2 98 74-130
Dichlorodifluoromethane ug/kg 59.871.2 84 40-160
Diisopropyl ether ug/kg 71.071.2 100 69-141
Ethylbenzene ug/kg 72.171.2 101 75-133
Hexachloro-1,3-butadiene ug/kg 82.771.2 116 68-143
Isopropylbenzene (Cumene)ug/kg 73.671.2 103 76-143
m&p-Xylene ug/kg 141142 99 75-136
Methyl-tert-butyl ether ug/kg 74.971.2 105 68-144
Methylene Chloride ug/kg 73.071.2 102 45-154
n-Butylbenzene ug/kg 76.271.2 107 72-137
n-Propylbenzene ug/kg 75.471.2 106 76-136
Naphthalene ug/kg 87.171.2 122 68-151
o-Xylene ug/kg 73.371.2 103 76-141
p-Isopropyltoluene ug/kg 73.171.2 103 76-140
sec-Butylbenzene ug/kg 75.871.2 106 79-139
Styrene ug/kg 77.771.2 109 79-137
tert-Butylbenzene ug/kg 69.671.2 98 74-143
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/27/2017 09:20 AM
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Page 19 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92326841
NICUS AUTO CARS NAC-1701-1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1913607LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/kg 117 L071.2 165 71-138
Toluene ug/kg 69.971.2 98 74-131
trans-1,2-Dichloroethene ug/kg 67.971.2 95 67-135
trans-1,3-Dichloropropene ug/kg 77.871.2 109 65-146
Trichloroethene ug/kg 79.871.2 112 67-135
Trichlorofluoromethane ug/kg 72.071.2 101 59-144
Vinyl acetate ug/kg 77.8142 55 40-160
Vinyl chloride ug/kg 56.871.2 80 56-141
Xylene (Total)ug/kg 215214 100 76-137
1,2-Dichloroethane-d4 (S)%97 70-132
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1914183MATRIX SPIKE SAMPLE:
MSSpike
Result
92326842005
1,1,1,2-Tetrachloroethane ug/kg 17.719.6 90 70-130ND
1,1,1-Trichloroethane ug/kg 18.519.6 94 70-130ND
1,1,2,2-Tetrachloroethane ug/kg 16.819.6 85 70-130ND
1,1,2-Trichloroethane ug/kg 17.619.6 90 70-130ND
1,1-Dichloroethane ug/kg 17.719.6 90 70-130ND
1,1-Dichloroethene ug/kg 19.019.6 97 49-180ND
1,1-Dichloropropene ug/kg 19.519.6 99 70-130ND
1,2,3-Trichlorobenzene ug/kg 17.119.6 87 70-130ND
1,2,3-Trichloropropane ug/kg 15.919.6 81 70-130ND
1,2,4-Trichlorobenzene ug/kg 17.019.6 86 70-130ND
1,2,4-Trimethylbenzene ug/kg 19.519.6 100 70-130ND
1,2-Dibromo-3-chloropropane ug/kg 16.019.6 81 70-130ND
1,2-Dibromoethane (EDB)ug/kg 17.619.6 90 70-130ND
1,2-Dichlorobenzene ug/kg 19.019.6 97 70-130ND
1,2-Dichloroethane ug/kg 18.219.6 92 70-130ND
1,2-Dichloropropane ug/kg 19.619.6 100 70-130ND
1,3,5-Trimethylbenzene ug/kg 20.019.6 102 70-130ND
1,3-Dichlorobenzene ug/kg 19.119.6 97 70-130ND
1,3-Dichloropropane ug/kg 17.419.6 89 70-130ND
1,4-Dichlorobenzene ug/kg 19.019.6 97 70-130ND
2,2-Dichloropropane ug/kg 17.519.6 89 70-130ND
2-Butanone (MEK)ug/kg 31.4J39.2 80 70-130ND
2-Chlorotoluene ug/kg 21.019.6 107 70-130ND
2-Hexanone ug/kg 33.8J39.2 86 70-130ND
4-Chlorotoluene ug/kg 20.119.6 102 70-130ND
4-Methyl-2-pentanone (MIBK)ug/kg 33.8J39.2 86 70-130ND
Acetone ug/kg 40.6J39.2 103 70-130ND
Benzene ug/kg 19.919.6 102 50-166ND
Bromobenzene ug/kg 20.119.6 102 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/27/2017 09:20 AM
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Page 20 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92326841
NICUS AUTO CARS NAC-1701-1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1914183MATRIX SPIKE SAMPLE:
MSSpike
Result
92326842005
Bromochloromethane ug/kg 17.119.6 87 70-130ND
Bromodichloromethane ug/kg 18.719.6 95 70-130ND
Bromoform ug/kg 15.319.6 78 70-130ND
Bromomethane ug/kg 18.219.6 93 70-130ND
Carbon tetrachloride ug/kg 20.019.6 102 70-130ND
Chlorobenzene ug/kg 19.719.6 100 43-169ND
Chloroethane ug/kg 20.519.6 104 70-130ND
Chloroform ug/kg 18.419.6 94 70-130ND
Chloromethane ug/kg 21.819.6 111 70-130ND
cis-1,2-Dichloroethene ug/kg 19.119.6 97 70-130ND
cis-1,3-Dichloropropene ug/kg 16.919.6 86 70-130ND
Dibromochloromethane ug/kg 16.419.6 84 70-130ND
Dibromomethane ug/kg 17.019.6 86 70-130ND
Dichlorodifluoromethane ug/kg 13.919.6 71 70-130ND
Diisopropyl ether ug/kg 19.319.6 98 70-130ND
Ethylbenzene ug/kg 19.819.6 101 70-130ND
Hexachloro-1,3-butadiene ug/kg 19.619.6 100 70-130ND
Isopropylbenzene (Cumene)ug/kg 19.819.6 101 70-130ND
m&p-Xylene ug/kg 40.239.2 102 70-130ND
Methyl-tert-butyl ether ug/kg 16.319.6 83 70-130ND
Methylene Chloride ug/kg 24.619.6 105 70-130ND
n-Butylbenzene ug/kg 19.319.6 98 70-130ND
n-Propylbenzene ug/kg 20.719.6 105 70-130ND
Naphthalene ug/kg 18.119.6 88 70-130ND
o-Xylene ug/kg 19.319.6 99 70-130ND
p-Isopropyltoluene ug/kg 19.419.6 99 70-130ND
sec-Butylbenzene ug/kg 20.719.6 105 70-130ND
Styrene ug/kg 18.719.6 95 70-130ND
tert-Butylbenzene ug/kg 19.119.6 97 70-130ND
Tetrachloroethene ug/kg 18.019.6 92 70-130ND
Toluene ug/kg 19.919.6 101 52-163ND
trans-1,2-Dichloroethene ug/kg 19.519.6 99 70-130ND
trans-1,3-Dichloropropene ug/kg 16.819.6 85 70-130ND
Trichloroethene ug/kg 18.619.6 95 49-167ND
Trichlorofluoromethane ug/kg 20.419.6 104 70-130ND
Vinyl acetate ug/kg 33.4J39.2 85 70-130ND
Vinyl chloride ug/kg 16.519.6 84 70-130ND
1,2-Dichloroethane-d4 (S)%89 70-132
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92326678001
1914182SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/27/2017 09:20 AM
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Page 21 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92326841
NICUS AUTO CARS NAC-1701-1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92326678001
1914182SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg NDND
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK)ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg NDND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK)ug/kg NDND
Acetone ug/kg 41.8JND
Benzene ug/kg NDND
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg NDND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg NDND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg NDND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg NDND
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene)ug/kg NDND
m&p-Xylene ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92326841
NICUS AUTO CARS NAC-1701-1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92326678001
1914182SAMPLE DUPLICATE:
Methyl-tert-butyl ether ug/kg NDND
Methylene Chloride ug/kg 14.6JND
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg NDND
Naphthalene ug/kg NDND
o-Xylene ug/kg NDND
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg NDND
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg NDND
Toluene ug/kg NDND
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg NDND
Xylene (Total)ug/kg NDND
1,2-Dichloroethane-d4 (S)%84 886
4-Bromofluorobenzene (S)%96 898
Toluene-d8 (S)%99 599
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92326841
NICUS AUTO CARS NAC-1701-1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
345098
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:92326841001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1914766
Associated Lab Samples:92326841001
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 01/20/17 15:06
1,1,1-Trichloroethane ug/kg ND 5.0 01/20/17 15:06
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 01/20/17 15:06
1,1,2-Trichloroethane ug/kg ND 5.0 01/20/17 15:06
1,1-Dichloroethane ug/kg ND 5.0 01/20/17 15:06
1,1-Dichloroethene ug/kg ND 5.0 01/20/17 15:06
1,1-Dichloropropene ug/kg ND 5.0 01/20/17 15:06
1,2,3-Trichlorobenzene ug/kg ND 5.0 01/20/17 15:06
1,2,3-Trichloropropane ug/kg ND 5.0 01/20/17 15:06
1,2,4-Trichlorobenzene ug/kg ND 5.0 01/20/17 15:06
1,2,4-Trimethylbenzene ug/kg ND 5.0 01/20/17 15:06
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 01/20/17 15:06
1,2-Dibromoethane (EDB)ug/kg ND 5.0 01/20/17 15:06
1,2-Dichlorobenzene ug/kg ND 5.0 01/20/17 15:06
1,2-Dichloroethane ug/kg ND 5.0 01/20/17 15:06
1,2-Dichloropropane ug/kg ND 5.0 01/20/17 15:06
1,3,5-Trimethylbenzene ug/kg ND 5.0 01/20/17 15:06
1,3-Dichlorobenzene ug/kg ND 5.0 01/20/17 15:06
1,3-Dichloropropane ug/kg ND 5.0 01/20/17 15:06
1,4-Dichlorobenzene ug/kg ND 5.0 01/20/17 15:06
2,2-Dichloropropane ug/kg ND 5.0 01/20/17 15:06
2-Butanone (MEK)ug/kg ND 99.8 01/20/17 15:06
2-Chlorotoluene ug/kg ND 5.0 01/20/17 15:06
2-Hexanone ug/kg ND 49.9 01/20/17 15:06
4-Chlorotoluene ug/kg ND 5.0 01/20/17 15:06
4-Methyl-2-pentanone (MIBK)ug/kg ND 49.9 01/20/17 15:06
Acetone ug/kg ND 99.8 01/20/17 15:06
Benzene ug/kg ND 5.0 01/20/17 15:06
Bromobenzene ug/kg ND 5.0 01/20/17 15:06
Bromochloromethane ug/kg ND 5.0 01/20/17 15:06
Bromodichloromethane ug/kg ND 5.0 01/20/17 15:06
Bromoform ug/kg ND 5.0 01/20/17 15:06
Bromomethane ug/kg ND 10 01/20/17 15:06
Carbon tetrachloride ug/kg ND 5.0 01/20/17 15:06
Chlorobenzene ug/kg ND 5.0 01/20/17 15:06
Chloroethane ug/kg ND 10 01/20/17 15:06
Chloroform ug/kg ND 5.0 01/20/17 15:06
Chloromethane ug/kg ND 10 01/20/17 15:06
cis-1,2-Dichloroethene ug/kg ND 5.0 01/20/17 15:06
cis-1,3-Dichloropropene ug/kg ND 5.0 01/20/17 15:06
Dibromochloromethane ug/kg ND 5.0 01/20/17 15:06
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92326841
NICUS AUTO CARS NAC-1701-1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1914766
Associated Lab Samples:92326841001
Matrix:Solid
Analyzed
Dibromomethane ug/kg ND 5.0 01/20/17 15:06
Dichlorodifluoromethane ug/kg ND 10 01/20/17 15:06
Diisopropyl ether ug/kg ND 5.0 01/20/17 15:06
Ethylbenzene ug/kg ND 5.0 01/20/17 15:06
Hexachloro-1,3-butadiene ug/kg ND 5.0 01/20/17 15:06
Isopropylbenzene (Cumene)ug/kg ND 5.0 01/20/17 15:06
m&p-Xylene ug/kg ND 10 01/20/17 15:06
Methyl-tert-butyl ether ug/kg ND 5.0 01/20/17 15:06
Methylene Chloride ug/kg ND 20.0 01/20/17 15:06
n-Butylbenzene ug/kg ND 5.0 01/20/17 15:06
n-Propylbenzene ug/kg ND 5.0 01/20/17 15:06
Naphthalene ug/kg ND 5.0 01/20/17 15:06
o-Xylene ug/kg ND 5.0 01/20/17 15:06
p-Isopropyltoluene ug/kg ND 5.0 01/20/17 15:06
sec-Butylbenzene ug/kg ND 5.0 01/20/17 15:06
Styrene ug/kg ND 5.0 01/20/17 15:06
tert-Butylbenzene ug/kg ND 5.0 01/20/17 15:06
Tetrachloroethene ug/kg ND 5.0 01/20/17 15:06
Toluene ug/kg ND 5.0 01/20/17 15:06
trans-1,2-Dichloroethene ug/kg ND 5.0 01/20/17 15:06
trans-1,3-Dichloropropene ug/kg ND 5.0 01/20/17 15:06
Trichloroethene ug/kg ND 5.0 01/20/17 15:06
Trichlorofluoromethane ug/kg ND 5.0 01/20/17 15:06
Vinyl acetate ug/kg ND 49.9 01/20/17 15:06
Vinyl chloride ug/kg ND 10 01/20/17 15:06
Xylene (Total)ug/kg ND 10 01/20/17 15:06
1,2-Dichloroethane-d4 (S)%88 70-132 01/20/17 15:06
4-Bromofluorobenzene (S)%102 70-130 01/20/17 15:06
Toluene-d8 (S)%100 70-130 01/20/17 15:06
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1914767LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 60.658.3 104 74-137
1,1,1-Trichloroethane ug/kg 54.658.3 94 67-140
1,1,2,2-Tetrachloroethane ug/kg 50.158.3 86 72-141
1,1,2-Trichloroethane ug/kg 60.858.3 104 78-138
1,1-Dichloroethane ug/kg 51.858.3 89 69-134
1,1-Dichloroethene ug/kg 58.858.3 101 67-138
1,1-Dichloropropene ug/kg 56.558.3 97 69-139
1,2,3-Trichlorobenzene ug/kg 59.758.3 102 70-146
1,2,3-Trichloropropane ug/kg 56.658.3 97 69-144
1,2,4-Trichlorobenzene ug/kg 57.958.3 99 68-148
1,2,4-Trimethylbenzene ug/kg 58.158.3 100 74-137
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92326841
NICUS AUTO CARS NAC-1701-1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1914767LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/kg 57.758.3 99 65-140
1,2-Dibromoethane (EDB)ug/kg 58.258.3 100 77-135
1,2-Dichlorobenzene ug/kg 58.758.3 101 77-141
1,2-Dichloroethane ug/kg 56.958.3 98 65-137
1,2-Dichloropropane ug/kg 61.758.3 106 72-136
1,3,5-Trimethylbenzene ug/kg 57.458.3 99 76-133
1,3-Dichlorobenzene ug/kg 58.858.3 101 74-138
1,3-Dichloropropane ug/kg 60.758.3 104 71-139
1,4-Dichlorobenzene ug/kg 56.858.3 97 76-138
2,2-Dichloropropane ug/kg 54.358.3 93 68-137
2-Butanone (MEK)ug/kg 133117 114 58-147
2-Chlorotoluene ug/kg 60.558.3 104 73-139
2-Hexanone ug/kg 143117 122 62-145
4-Chlorotoluene ug/kg 58.358.3 100 76-141
4-Methyl-2-pentanone (MIBK)ug/kg 137117 118 64-149
Acetone ug/kg 124117 107 53-153
Benzene ug/kg 60.758.3 104 73-135
Bromobenzene ug/kg 61.158.3 105 75-133
Bromochloromethane ug/kg 56.858.3 97 73-134
Bromodichloromethane ug/kg 60.158.3 103 71-135
Bromoform ug/kg 50.658.3 87 66-141
Bromomethane ug/kg 54.058.3 93 53-160
Carbon tetrachloride ug/kg 56.258.3 96 60-145
Chlorobenzene ug/kg 59.758.3 102 78-130
Chloroethane ug/kg 57.858.3 99 64-149
Chloroform ug/kg 55.058.3 94 70-134
Chloromethane ug/kg 63.358.3 109 52-150
cis-1,2-Dichloroethene ug/kg 57.258.3 98 70-133
cis-1,3-Dichloropropene ug/kg 56.758.3 97 68-134
Dibromochloromethane ug/kg 56.758.3 97 71-138
Dibromomethane ug/kg 57.458.3 98 74-130
Dichlorodifluoromethane ug/kg 45.358.3 78 40-160
Diisopropyl ether ug/kg 62.958.3 108 69-141
Ethylbenzene ug/kg 58.558.3 100 75-133
Hexachloro-1,3-butadiene ug/kg 57.758.3 99 68-143
Isopropylbenzene (Cumene)ug/kg 56.658.3 97 76-143
m&p-Xylene ug/kg 114117 98 75-136
Methyl-tert-butyl ether ug/kg 59.058.3 101 68-144
Methylene Chloride ug/kg 63.658.3 109 45-154
n-Butylbenzene ug/kg 56.958.3 98 72-137
n-Propylbenzene ug/kg 58.758.3 101 76-136
Naphthalene ug/kg 63.158.3 108 68-151
o-Xylene ug/kg 57.158.3 98 76-141
p-Isopropyltoluene ug/kg 56.858.3 97 76-140
sec-Butylbenzene ug/kg 58.258.3 100 79-139
Styrene ug/kg 58.458.3 100 79-137
tert-Butylbenzene ug/kg 54.158.3 93 74-143
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92326841
NICUS AUTO CARS NAC-1701-1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1914767LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/kg 94.1 L058.3 161 71-138
Toluene ug/kg 58.858.3 101 74-131
trans-1,2-Dichloroethene ug/kg 57.358.3 98 67-135
trans-1,3-Dichloropropene ug/kg 60.458.3 104 65-146
Trichloroethene ug/kg 65.558.3 112 67-135
Trichlorofluoromethane ug/kg 55.158.3 94 59-144
Vinyl acetate ug/kg 53J117 45 40-160
Vinyl chloride ug/kg 49.358.3 85 56-141
Xylene (Total)ug/kg 171175 98 76-137
1,2-Dichloroethane-d4 (S)%98 70-132
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1915768MATRIX SPIKE SAMPLE:
MSSpike
Result
92326841001
1,1,1,2-Tetrachloroethane ug/kg 18.820.4 92 70-130ND
1,1,1-Trichloroethane ug/kg 19.320.4 95 70-130ND
1,1,2,2-Tetrachloroethane ug/kg 19.720.4 97 70-130ND
1,1,2-Trichloroethane ug/kg 19.820.4 97 70-130ND
1,1-Dichloroethane ug/kg 20.420.4 100 70-130ND
1,1-Dichloroethene ug/kg 20.620.4 101 49-180ND
1,1-Dichloropropene ug/kg 20.020.4 98 70-130ND
1,2,3-Trichlorobenzene ug/kg 18.120.4 89 70-130ND
1,2,3-Trichloropropane ug/kg 18.520.4 90 70-130ND
1,2,4-Trichlorobenzene ug/kg 17.620.4 86 70-130ND
1,2,4-Trimethylbenzene ug/kg 21.120.4 100 70-130ND
1,2-Dibromo-3-chloropropane ug/kg 21.520.4 105 70-130ND
1,2-Dibromoethane (EDB)ug/kg 18.120.4 89 70-130ND
1,2-Dichlorobenzene ug/kg 19.620.4 96 70-130ND
1,2-Dichloroethane ug/kg 20.220.4 99 70-130ND
1,2-Dichloropropane ug/kg 20.020.4 98 70-130ND
1,3,5-Trimethylbenzene ug/kg 19.420.4 94 70-130ND
1,3-Dichlorobenzene ug/kg 19.120.4 94 70-130ND
1,3-Dichloropropane ug/kg 19.620.4 96 70-130ND
1,4-Dichlorobenzene ug/kg 19.120.4 94 70-130ND
2,2-Dichloropropane ug/kg 19.320.4 94 70-130ND
2-Butanone (MEK)ug/kg 44.6J40.8 109 70-130ND
2-Chlorotoluene ug/kg 19.920.4 98 70-130ND
2-Hexanone ug/kg 39.6J40.8 97 70-130ND
4-Chlorotoluene ug/kg 19.820.4 97 70-130ND
4-Methyl-2-pentanone (MIBK)ug/kg 41.3J40.8 101 70-130ND
Acetone ug/kg 56J40.8 115 70-130ND
Benzene ug/kg 20.320.4 100 50-166ND
Bromobenzene ug/kg 20.320.4 100 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92326841
NICUS AUTO CARS NAC-1701-1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1915768MATRIX SPIKE SAMPLE:
MSSpike
Result
92326841001
Bromochloromethane ug/kg 19.720.4 97 70-130ND
Bromodichloromethane ug/kg 20.420.4 100 70-130ND
Bromoform ug/kg 17.120.4 84 70-130ND
Bromomethane ug/kg 19.920.4 97 70-130ND
Carbon tetrachloride ug/kg 20.320.4 100 70-130ND
Chlorobenzene ug/kg 19.920.4 98 43-169ND
Chloroethane ug/kg 22.820.4 112 70-130ND
Chloroform ug/kg 20.020.4 98 70-130ND
Chloromethane ug/kg 22.920.4 112 70-130ND
cis-1,2-Dichloroethene ug/kg 19.720.4 97 70-130ND
cis-1,3-Dichloropropene ug/kg 19.920.4 97 70-130ND
Dibromochloromethane ug/kg 18.420.4 90 70-130ND
Dibromomethane ug/kg 19.520.4 96 70-130ND
Dichlorodifluoromethane ug/kg 20.020.4 98 70-130ND
Diisopropyl ether ug/kg 19.720.4 97 70-130ND
Ethylbenzene ug/kg 20.220.4 98 70-130ND
Hexachloro-1,3-butadiene ug/kg 15.720.4 77 70-130ND
Isopropylbenzene (Cumene)ug/kg 19.420.4 95 70-130ND
m&p-Xylene ug/kg 39.940.8 96 70-130ND
Methyl-tert-butyl ether ug/kg 20.820.4 102 70-130ND
Methylene Chloride ug/kg 28.620.4 101 70-130ND
n-Butylbenzene ug/kg 17.820.4 87 70-130ND
n-Propylbenzene ug/kg 19.820.4 97 70-130ND
Naphthalene ug/kg 21.120.4 97 70-130ND
o-Xylene ug/kg 20.120.4 96 70-130ND
p-Isopropyltoluene ug/kg 18.220.4 89 70-130ND
sec-Butylbenzene ug/kg 19.420.4 95 70-130ND
Styrene ug/kg 19.120.4 94 70-130ND
tert-Butylbenzene ug/kg 19.520.4 96 70-130ND
Tetrachloroethene ug/kg 18.320.4 90 70-130ND
Toluene ug/kg 20.420.4 99 52-163ND
trans-1,2-Dichloroethene ug/kg 21.520.4 106 70-130ND
trans-1,3-Dichloropropene ug/kg 19.720.4 97 70-130ND
Trichloroethene ug/kg 19.620.4 96 49-167ND
Trichlorofluoromethane ug/kg 23.420.4 115 70-130ND
Vinyl acetate ug/kg 49.9J40.8 122 70-130ND
Vinyl chloride ug/kg 18.420.4 90 70-130ND
1,2-Dichloroethane-d4 (S)%105 70-132
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%102 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92326875003
1915357SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92326841
NICUS AUTO CARS NAC-1701-1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92326875003
1915357SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/kg ND
1,1,2,2-Tetrachloroethane ug/kg ND
1,1,2-Trichloroethane ug/kg ND
1,1-Dichloroethane ug/kg ND
1,1-Dichloroethene ug/kg ND
1,1-Dichloropropene ug/kg ND
1,2,3-Trichlorobenzene ug/kg ND
1,2,3-Trichloropropane ug/kg ND
1,2,4-Trichlorobenzene ug/kg ND
1,2,4-Trimethylbenzene ug/kg ND
1,2-Dibromo-3-chloropropane ug/kg ND
1,2-Dibromoethane (EDB)ug/kg ND
1,2-Dichlorobenzene ug/kg ND
1,2-Dichloroethane ug/kg ND
1,2-Dichloropropane ug/kg ND
1,3,5-Trimethylbenzene ug/kg ND
1,3-Dichlorobenzene ug/kg ND
1,3-Dichloropropane ug/kg ND
1,4-Dichlorobenzene ug/kg ND
2,2-Dichloropropane ug/kg ND
2-Butanone (MEK)ug/kg ND
2-Chlorotoluene ug/kg ND
2-Hexanone ug/kg ND
4-Chlorotoluene ug/kg ND
4-Methyl-2-pentanone (MIBK)ug/kg ND
Acetone ug/kg ND
Benzene ug/kg NDND
Bromobenzene ug/kg ND
Bromochloromethane ug/kg ND
Bromodichloromethane ug/kg ND
Bromoform ug/kg ND
Bromomethane ug/kg ND
Carbon tetrachloride ug/kg ND
Chlorobenzene ug/kg ND
Chloroethane ug/kg ND
Chloroform ug/kg ND
Chloromethane ug/kg ND
cis-1,2-Dichloroethene ug/kg ND
cis-1,3-Dichloropropene ug/kg ND
Dibromochloromethane ug/kg ND
Dibromomethane ug/kg ND
Dichlorodifluoromethane ug/kg ND
Diisopropyl ether ug/kg ND
Ethylbenzene ug/kg NDND
Hexachloro-1,3-butadiene ug/kg ND
Isopropylbenzene (Cumene)ug/kg ND
m&p-Xylene ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92326841
NICUS AUTO CARS NAC-1701-1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92326875003
1915357SAMPLE DUPLICATE:
Methyl-tert-butyl ether ug/kg NDND
Methylene Chloride ug/kg 3.8J
n-Butylbenzene ug/kg ND
n-Propylbenzene ug/kg ND
Naphthalene ug/kg ND
o-Xylene ug/kg NDND
p-Isopropyltoluene ug/kg ND
sec-Butylbenzene ug/kg ND
Styrene ug/kg ND
tert-Butylbenzene ug/kg ND
Tetrachloroethene ug/kg ND
Toluene ug/kg NDND
trans-1,2-Dichloroethene ug/kg ND
trans-1,3-Dichloropropene ug/kg ND
Trichloroethene ug/kg ND
Trichlorofluoromethane ug/kg ND
Vinyl acetate ug/kg ND
Vinyl chloride ug/kg ND
Xylene (Total)ug/kg NDND
1,2-Dichloroethane-d4 (S)%93 1187
4-Bromofluorobenzene (S)%99 599
Toluene-d8 (S)%102 899
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92326841
NICUS AUTO CARS NAC-1701-1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
344906
EPA 3546
EPA 8270
8270 Solid MSSV Microwave
Associated Lab Samples:92326841001, 92326841002, 92326841003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1913683
Associated Lab Samples:92326841001, 92326841002, 92326841003
Matrix:Solid
Analyzed
1,2,4-Trichlorobenzene ug/kg ND 330 01/20/17 09:48
1,2-Dichlorobenzene ug/kg ND 330 01/20/17 09:48
1,3-Dichlorobenzene ug/kg ND 330 01/20/17 09:48
1,4-Dichlorobenzene ug/kg ND 330 01/20/17 09:48
1-Methylnaphthalene ug/kg ND 330 01/20/17 09:48
2,2'-Oxybis(1-chloropropane)ug/kg ND 330 01/20/17 09:48
2,4,5-Trichlorophenol ug/kg ND 330 01/20/17 09:48
2,4,6-Trichlorophenol ug/kg ND 330 01/20/17 09:48
2,4-Dichlorophenol ug/kg ND 330 01/20/17 09:48
2,4-Dimethylphenol ug/kg ND 330 01/20/17 09:48
2,4-Dinitrophenol ug/kg ND 1650 01/20/17 09:48
2,4-Dinitrotoluene ug/kg ND 330 01/20/17 09:48
2,6-Dinitrotoluene ug/kg ND 330 01/20/17 09:48
2-Chloronaphthalene ug/kg ND 330 01/20/17 09:48
2-Chlorophenol ug/kg ND 330 01/20/17 09:48
2-Methylnaphthalene ug/kg ND 330 01/20/17 09:48
2-Methylphenol(o-Cresol)ug/kg ND 330 01/20/17 09:48
2-Nitroaniline ug/kg ND 1650 01/20/17 09:48
2-Nitrophenol ug/kg ND 330 01/20/17 09:48
3&4-Methylphenol(m&p Cresol)ug/kg ND 330 01/20/17 09:48
3,3'-Dichlorobenzidine ug/kg ND 1650 01/20/17 09:48
3-Nitroaniline ug/kg ND 1650 01/20/17 09:48
4,6-Dinitro-2-methylphenol ug/kg ND 660 01/20/17 09:48
4-Bromophenylphenyl ether ug/kg ND 330 01/20/17 09:48
4-Chloro-3-methylphenol ug/kg ND 660 01/20/17 09:48
4-Chloroaniline ug/kg ND 1650 01/20/17 09:48
4-Chlorophenylphenyl ether ug/kg ND 330 01/20/17 09:48
4-Nitroaniline ug/kg ND 660 01/20/17 09:48
4-Nitrophenol ug/kg ND 1650 01/20/17 09:48
Acenaphthene ug/kg ND 330 01/20/17 09:48
Acenaphthylene ug/kg ND 330 01/20/17 09:48
Aniline ug/kg ND 330 01/20/17 09:48
Anthracene ug/kg ND 330 01/20/17 09:48
Benzo(a)anthracene ug/kg ND 330 01/20/17 09:48
Benzo(a)pyrene ug/kg ND 330 01/20/17 09:48
Benzo(b)fluoranthene ug/kg ND 330 01/20/17 09:48
Benzo(g,h,i)perylene ug/kg ND 330 01/20/17 09:48
Benzo(k)fluoranthene ug/kg ND 330 01/20/17 09:48
Benzoic Acid ug/kg ND 1650 01/20/17 09:48
Benzyl alcohol ug/kg ND 660 01/20/17 09:48
bis(2-Chloroethoxy)methane ug/kg ND 330 01/20/17 09:48
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92326841
NICUS AUTO CARS NAC-1701-1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1913683
Associated Lab Samples:92326841001, 92326841002, 92326841003
Matrix:Solid
Analyzed
bis(2-Chloroethyl) ether ug/kg ND 330 01/20/17 09:48
bis(2-Ethylhexyl)phthalate ug/kg ND 330 01/20/17 09:48
Butylbenzylphthalate ug/kg ND 330 01/20/17 09:48
Chrysene ug/kg ND 330 01/20/17 09:48
Di-n-butylphthalate ug/kg ND 330 01/20/17 09:48
Di-n-octylphthalate ug/kg ND 330 01/20/17 09:48
Dibenz(a,h)anthracene ug/kg ND 330 01/20/17 09:48
Dibenzofuran ug/kg ND 330 01/20/17 09:48
Diethylphthalate ug/kg ND 330 01/20/17 09:48
Dimethylphthalate ug/kg ND 330 01/20/17 09:48
Fluoranthene ug/kg ND 330 01/20/17 09:48
Fluorene ug/kg ND 330 01/20/17 09:48
Hexachloro-1,3-butadiene ug/kg ND 330 01/20/17 09:48
Hexachlorobenzene ug/kg ND 330 01/20/17 09:48
Hexachlorocyclopentadiene ug/kg ND 330 01/20/17 09:48
Hexachloroethane ug/kg ND 330 01/20/17 09:48
Indeno(1,2,3-cd)pyrene ug/kg ND 330 01/20/17 09:48
Isophorone ug/kg ND 330 01/20/17 09:48
N-Nitroso-di-n-propylamine ug/kg ND 330 01/20/17 09:48
N-Nitrosodimethylamine ug/kg ND 330 01/20/17 09:48
N-Nitrosodiphenylamine ug/kg ND 330 01/20/17 09:48
Naphthalene ug/kg ND 330 01/20/17 09:48
Nitrobenzene ug/kg ND 330 01/20/17 09:48
Pentachlorophenol ug/kg ND 1650 01/20/17 09:48
Phenanthrene ug/kg ND 330 01/20/17 09:48
Phenol ug/kg ND 330 01/20/17 09:48
Pyrene ug/kg ND 330 01/20/17 09:48
2,4,6-Tribromophenol (S)%51 27-110 01/20/17 09:48
2-Fluorobiphenyl (S)%52 30-110 01/20/17 09:48
2-Fluorophenol (S)%57 13-110 01/20/17 09:48
Nitrobenzene-d5 (S)%53 23-110 01/20/17 09:48
Phenol-d6 (S)%58 22-110 01/20/17 09:48
Terphenyl-d14 (S)%69 28-110 01/20/17 09:48
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1913684LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 10901670 65 36-120
1,2-Dichlorobenzene ug/kg 10701670 64 41-120
1,3-Dichlorobenzene ug/kg 1080 L016706566-120
1,4-Dichlorobenzene ug/kg 10401670 62 42-120
1-Methylnaphthalene ug/kg 10801670 65 40-120
2,2'-Oxybis(1-chloropropane)ug/kg 12001670 72 17-120
2,4,5-Trichlorophenol ug/kg 10601670 64 37-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92326841
NICUS AUTO CARS NAC-1701-1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1913684LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,6-Trichlorophenol ug/kg 12601670 75 40-120
2,4-Dichlorophenol ug/kg 12801670 77 33-120
2,4-Dimethylphenol ug/kg 13601670 82 36-120
2,4-Dinitrophenol ug/kg 1300J L083301622-121
2,4-Dinitrotoluene ug/kg 11701670 70 60-120
2,6-Dinitrotoluene ug/kg 12201670 73 54-120
2-Chloronaphthalene ug/kg 11301670 68 41-120
2-Chlorophenol ug/kg 12801670 77 39-120
2-Methylnaphthalene ug/kg 11401670 68 26-120
2-Methylphenol(o-Cresol)ug/kg 11601670 70 41-120
2-Nitroaniline ug/kg 26503330 80 45-120
2-Nitrophenol ug/kg 12301670 74 35-120
3&4-Methylphenol(m&p Cresol)ug/kg 11901670 71 35-120
3,3'-Dichlorobenzidine ug/kg 22803330 68 16-125
3-Nitroaniline ug/kg 26403330 79 45-120
4,6-Dinitro-2-methylphenol ug/kg 19603330 59 46-120
4-Bromophenylphenyl ether ug/kg 10801670 65 36-120
4-Chloro-3-methylphenol ug/kg 27403330 82 37-120
4-Chloroaniline ug/kg 23403330 70 35-120
4-Chlorophenylphenyl ether ug/kg 11001670 66 30-120
4-Nitroaniline ug/kg 27003330 81 48-120
4-Nitrophenol ug/kg 69408330 83 43-120
Acenaphthene ug/kg 11301670 68 46-120
Acenaphthylene ug/kg 11801670 71 46-120
Aniline ug/kg 10201670 61 33-120
Anthracene ug/kg 11501670 69 63-120
Benzo(a)anthracene ug/kg 11801670 71 61-120
Benzo(a)pyrene ug/kg 11901670 71 59-120
Benzo(b)fluoranthene ug/kg 12301670 74 55-120
Benzo(g,h,i)perylene ug/kg 11501670 69 57-120
Benzo(k)fluoranthene ug/kg 12301670 74 56-120
Benzoic Acid ug/kg 682J L08330813-120
Benzyl alcohol ug/kg 24003330 72 34-120
bis(2-Chloroethoxy)methane ug/kg 11101670 67 21-120
bis(2-Chloroethyl) ether ug/kg 10901670 65 25-120
bis(2-Ethylhexyl)phthalate ug/kg 13101670 79 56-123
Butylbenzylphthalate ug/kg 12601670 76 57-120
Chrysene ug/kg 11501670 69 64-120
Di-n-butylphthalate ug/kg 12801670 77 58-120
Di-n-octylphthalate ug/kg 13701670 82 47-121
Dibenz(a,h)anthracene ug/kg 12301670 74 56-120
Dibenzofuran ug/kg 11001670 66 43-120
Diethylphthalate ug/kg 13101670 78 55-120
Dimethylphthalate ug/kg 12501670 75 54-120
Fluoranthene ug/kg 11901670 71 61-120
Fluorene ug/kg 11801670 71 51-120
Hexachloro-1,3-butadiene ug/kg 10701670 64 22-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92326841
NICUS AUTO CARS NAC-1701-1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1913684LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachlorobenzene ug/kg 11301670 68 53-120
Hexachlorocyclopentadiene ug/kg 10301670 62 18-150
Hexachloroethane ug/kg 10801670 65 39-120
Indeno(1,2,3-cd)pyrene ug/kg 12101670 72 58-120
Isophorone ug/kg 11501670 69 38-120
N-Nitroso-di-n-propylamine ug/kg 12301670 74 30-120
N-Nitrosodimethylamine ug/kg 11501670 69 32-120
N-Nitrosodiphenylamine ug/kg 11401670 68 50-120
Naphthalene ug/kg 11201670 67 38-120
Nitrobenzene ug/kg 11601670 70 37-120
Pentachlorophenol ug/kg 26303330 79 10-120
Phenanthrene ug/kg 11801670 71 62-120
Phenol ug/kg 11901670 71 37-120
Pyrene ug/kg 11001670 66 63-120
2,4,6-Tribromophenol (S)%72 27-110
2-Fluorobiphenyl (S)%67 30-110
2-Fluorophenol (S)%76 13-110
Nitrobenzene-d5 (S)%69 23-110
Phenol-d6 (S)%75 22-110
Terphenyl-d14 (S)%73 28-110
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1913685MATRIX SPIKE SAMPLE:
MSSpike
Result
92326841001
1,2,4-Trichlorobenzene ug/kg 5561790 31 18-119ND
1,2-Dichlorobenzene ug/kg 638 M117903650-110ND
1,3-Dichlorobenzene ug/kg 6261790 35 27-110ND
1,4-Dichlorobenzene ug/kg 6011790 34 28-110ND
1-Methylnaphthalene ug/kg 5241790 29 24-116ND
2,2'-Oxybis(1-chloropropane)ug/kg 816 M117904650-150ND
2,4,5-Trichlorophenol ug/kg 5601790 31 28-110ND
2,4,6-Trichlorophenol ug/kg 6221790 35 17-117ND
2,4-Dichlorophenol ug/kg 5991790 34 21-128ND
2,4-Dimethylphenol ug/kg 5771790 32 10-120ND
2,4-Dinitrophenol ug/kg 22908940 26 10-107ND
2,4-Dinitrotoluene ug/kg 598 M117903336-109ND
2,6-Dinitrotoluene ug/kg 5901790 33 32-110ND
2-Chloronaphthalene ug/kg 5891790 33 30-107ND
2-Chlorophenol ug/kg 6371790 36 14-106ND
2-Methylnaphthalene ug/kg 5201790 29 10-135ND
2-Methylphenol(o-Cresol)ug/kg 5581790 31 10-124ND
2-Nitroaniline ug/kg 1530J3570 43 26-116ND
2-Nitrophenol ug/kg 5331790 30 28-103ND
3&4-Methylphenol(m&p Cresol)ug/kg 5331790 30 10-109ND
3,3'-Dichlorobenzidine ug/kg 1000J3570 28 10-150ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92326841
NICUS AUTO CARS NAC-1701-1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1913685MATRIX SPIKE SAMPLE:
MSSpike
Result
92326841001
3-Nitroaniline ug/kg 1150J3570 32 22-110ND
4,6-Dinitro-2-methylphenol ug/kg 10703570 30 13-121ND
4-Bromophenylphenyl ether ug/kg 6091790 34 31-109ND
4-Chloro-3-methylphenol ug/kg 14603570 41 13-128ND
4-Chloroaniline ug/kg 1050J3570 29 18-102ND
4-Chlorophenylphenyl ether ug/kg 5971790 33 29-112ND
4-Nitroaniline ug/kg 10603570 30 16-111ND
4-Nitrophenol ug/kg 34508940 39 14-135ND
Acenaphthene ug/kg 5771790 32 26-114ND
Acenaphthylene ug/kg 5941790 33 32-108ND
Aniline ug/kg 4771790 27 10-107ND
Anthracene ug/kg 5881790 33 32-111ND
Benzo(a)anthracene ug/kg 5881790 33 25-117ND
Benzo(a)pyrene ug/kg 5831790 33 25-106ND
Benzo(b)fluoranthene ug/kg 5921790 33 24-110ND
Benzo(g,h,i)perylene ug/kg 5191790 29 19-112ND
Benzo(k)fluoranthene ug/kg 6111790 34 24-114ND
Benzoic Acid ug/kg 751J M08940810-110ND
Benzyl alcohol ug/kg 10603570 30 24-106ND
bis(2-Chloroethoxy)methane ug/kg 4951790 28 13-119ND
bis(2-Chloroethyl) ether ug/kg 5211790 29 10-134ND
bis(2-Ethylhexyl)phthalate ug/kg 6761790 38 10-125ND
Butylbenzylphthalate ug/kg 6521790 36 18-110ND
Chrysene ug/kg 6151790 34 30-110ND
Di-n-butylphthalate ug/kg 6781790 38 19-112ND
Di-n-octylphthalate ug/kg 6581790 37 17-105ND
Dibenz(a,h)anthracene ug/kg 5261790 29 23-111ND
Dibenzofuran ug/kg 550 M117903135-103ND
Diethylphthalate ug/kg 7041790 39 27-113ND
Dimethylphthalate ug/kg 6721790 38 26-111ND
Fluoranthene ug/kg 6301790 35 33-109ND
Fluorene ug/kg 5921790 33 32-113ND
Hexachloro-1,3-butadiene ug/kg 6861790 38 16-116ND
Hexachlorobenzene ug/kg 5951790 33 27-120ND
Hexachlorocyclopentadiene ug/kg 4101790 23 10-108ND
Hexachloroethane ug/kg 7181790 40 10-117ND
Indeno(1,2,3-cd)pyrene ug/kg 5541790 31 10-122ND
Isophorone ug/kg 5721790 32 28-114ND
N-Nitroso-di-n-propylamine ug/kg 6111790 34 27-113ND
N-Nitrosodimethylamine ug/kg 6011790 34 10-109ND
N-Nitrosodiphenylamine ug/kg 5891790 33 10-128ND
Naphthalene ug/kg 5601790 27 25-110ND
Nitrobenzene ug/kg 5291790 30 18-114ND
Pentachlorophenol ug/kg 803J3570 22 10-122ND
Phenanthrene ug/kg 5821790 33 30-114ND
Phenol ug/kg 5441790 30 11-102ND
Pyrene ug/kg 5901790 33 25-116ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92326841
NICUS AUTO CARS NAC-1701-1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1913685MATRIX SPIKE SAMPLE:
MSSpike
Result
92326841001
2,4,6-Tribromophenol (S)%36 27-110
2-Fluorobiphenyl (S)%33 30-110
2-Fluorophenol (S)%34 13-110
Nitrobenzene-d5 (S)%34 23-110
Phenol-d6 (S)%35 22-110
Terphenyl-d14 (S)%40 28-110
Parameter Units
Dup
Result QualifiersRPDResult
92326841002
1913686SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
1-Methylnaphthalene ug/kg NDND
2,2'-Oxybis(1-chloropropane)ug/kg NDND
2,4,5-Trichlorophenol ug/kg NDND
2,4,6-Trichlorophenol ug/kg NDND
2,4-Dichlorophenol ug/kg NDND
2,4-Dimethylphenol ug/kg NDND
2,4-Dinitrophenol ug/kg NDND
2,4-Dinitrotoluene ug/kg NDND
2,6-Dinitrotoluene ug/kg NDND
2-Chloronaphthalene ug/kg NDND
2-Chlorophenol ug/kg NDND
2-Methylnaphthalene ug/kg NDND
2-Methylphenol(o-Cresol)ug/kg NDND
2-Nitroaniline ug/kg NDND
2-Nitrophenol ug/kg NDND
3&4-Methylphenol(m&p Cresol)ug/kg NDND
3,3'-Dichlorobenzidine ug/kg NDND
3-Nitroaniline ug/kg NDND
4,6-Dinitro-2-methylphenol ug/kg NDND
4-Bromophenylphenyl ether ug/kg NDND
4-Chloro-3-methylphenol ug/kg NDND
4-Chloroaniline ug/kg NDND
4-Chlorophenylphenyl ether ug/kg NDND
4-Nitroaniline ug/kg NDND
4-Nitrophenol ug/kg NDND
Acenaphthene ug/kg NDND
Acenaphthylene ug/kg NDND
Aniline ug/kg NDND
Anthracene ug/kg NDND
Benzo(a)anthracene ug/kg NDND
Benzo(a)pyrene ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92326841
NICUS AUTO CARS NAC-1701-1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92326841002
1913686SAMPLE DUPLICATE:
Benzo(b)fluoranthene ug/kg NDND
Benzo(g,h,i)perylene ug/kg NDND
Benzo(k)fluoranthene ug/kg NDND
Benzoic Acid ug/kg NDND
Benzyl alcohol ug/kg NDND
bis(2-Chloroethoxy)methane ug/kg NDND
bis(2-Chloroethyl) ether ug/kg NDND
bis(2-Ethylhexyl)phthalate ug/kg NDND
Butylbenzylphthalate ug/kg NDND
Chrysene ug/kg NDND
Di-n-butylphthalate ug/kg NDND
Di-n-octylphthalate ug/kg NDND
Dibenz(a,h)anthracene ug/kg NDND
Dibenzofuran ug/kg NDND
Diethylphthalate ug/kg NDND
Dimethylphthalate ug/kg NDND
Fluoranthene ug/kg NDND
Fluorene ug/kg NDND
Hexachloro-1,3-butadiene ug/kg NDND
Hexachlorobenzene ug/kg NDND
Hexachlorocyclopentadiene ug/kg NDND
Hexachloroethane ug/kg NDND
Indeno(1,2,3-cd)pyrene ug/kg NDND
Isophorone ug/kg NDND
N-Nitroso-di-n-propylamine ug/kg NDND
N-Nitrosodimethylamine ug/kg NDND
N-Nitrosodiphenylamine ug/kg NDND
Naphthalene ug/kg NDND
Nitrobenzene ug/kg NDND
Pentachlorophenol ug/kg NDND
Phenanthrene ug/kg NDND
Phenol ug/kg NDND
Pyrene ug/kg NDND
2,4,6-Tribromophenol (S)%37 740
2-Fluorobiphenyl (S)%36 1240
2-Fluorophenol (S)%40 1345
Nitrobenzene-d5 (S)%36 1944
Phenol-d6 (S)%37 1743
Terphenyl-d14 (S)%64 958
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92326841
NICUS AUTO CARS NAC-1701-1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
345053
MADEP EPH
MADEP EPH
MADEP EPH NC Soil
Associated Lab Samples:92326841001, 92326841002, 92326841003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1914325
Associated Lab Samples:92326841001, 92326841002, 92326841003
Matrix:Solid
Analyzed
Aliphatic (C09-C18)mg/kg ND 10.0 N201/24/17 20:44
Aliphatic (C19-C36)mg/kg ND 10.0 N201/24/17 20:44
Aromatic (C11-C22)mg/kg ND 10.0 N201/24/17 20:44
2-Bromonaphthalene (S)%79 40-140 01/24/17 20:44
2-Fluorobiphenyl (S)%93 40-140 01/24/17 20:44
Nonatriacontane (S)%66 40-140 01/24/17 20:44
o-Terphenyl (S)%78 40-140 01/24/17 20:44
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1914326LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1914327
Aliphatic (C09-C18)mg/kg ND N2105340-14054ND 50
Aliphatic (C19-C36)mg/kg ND N213.3 64 40-14059ND 50
Aromatic (C11-C22)mg/kg 20.3 N228.3 72 40-1406719.1 6 50
2-Bromonaphthalene (S)%77 40-14074
2-Fluorobiphenyl (S)%83 40-14081
Nonatriacontane (S)%59 40-14060
o-Terphenyl (S)%70 40-14068
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92326841
NICUS AUTO CARS NAC-1701-1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
344800
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92326841001, 92326841002, 92326841003
Parameter Units
Dup
Result QualifiersRPDResult
92326835009
1913171SAMPLE DUPLICATE:
Percent Moisture %14.8 614.0
Parameter Units
Dup
Result QualifiersRPDResult
92326842005
1913172SAMPLE DUPLICATE:
Percent Moisture %19.7 119.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 44
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92326841
NICUS AUTO CARS NAC-1701-1
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.B
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples.L3
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold NELAC/TNI accreditation for this parameter.N2
Surrogate recovery outside laboratory control limits.S0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 44
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92326841
NICUS AUTO CARS NAC-1701-1
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92326841001 345053 345546SB-1, 20-25'MADEP EPH MADEP EPH
92326841002 345053 345546SB-1, 38-40'MADEP EPH MADEP EPH
92326841003 345053 345546SB-1, 48-50'MADEP EPH MADEP EPH
92326841001 345240 345409SB-1, 20-25'MADEP VPH MADEP VPH
92326841002 345240 345409SB-1, 38-40'MADEP VPH MADEP VPH
92326841003 345240 345409SB-1, 48-50'MADEP VPH MADEP VPH
92326841001 344906 345043SB-1, 20-25'EPA 3546 EPA 8270
92326841002 344906 345043SB-1, 38-40'EPA 3546 EPA 8270
92326841003 344906 345043SB-1, 48-50'EPA 3546 EPA 8270
92326841001 345098SB-1, 20-25'EPA 8260
92326841002 344891SB-1, 38-40'EPA 8260
92326841003 344891SB-1, 48-50'EPA 8260
92326841001 344800SB-1, 20-25'ASTM D2974-87
92326841002 344800SB-1, 38-40'ASTM D2974-87
92326841003 344800SB-1, 48-50'ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2017 09:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 44
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