WS-9507_44719_CA_LSA_20170607

05/09/17
Technical Report for
GRI (Geological Resources Inc.)
Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
4236
SGS Accutest Job Number: FA43510
Sampling Date: 04/26/17
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
[e-mail]; [e-mail];
[e-mail]; [e-mail]
ATTN: Corey Buchanan
Total number of pages in report:
Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(L-A-B L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AK, AR, GA, IA, KY, MA, NV, OK, OR, UT, WA
This report shall not be reproduced, except in its entirety, without the written approval of SGS Accutest.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone] • http://www.accutest.com
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Norm Farmer
Technical Director
Southeast 05/09/17
e-Hardcopy 2.0
Automated Report
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SGS Accutest is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
Review standard terms at: http://www.sgs.com/en/terms-and-conditions
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FA43510
Table of Contents
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Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................6
3.1: FA43510-1: MW-1 (18') ...............................................................................................7
3.2: FA43510-2: MW-2 (28') ...............................................................................................13
Section 4: Misc. Forms ............................................................................................................19
4.1: Chain of Custody ...........................................................................................................20
Section 5: GC/MS Volatiles - QC Data Summaries ..............................................................23
5.1: Method Blank Summary ................................................................................................24
5.2: Blank Spike Summary ...................................................................................................26
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................28
Section 6: GC/MS Semi-volatiles - QC Data Summaries .....................................................30
6.1: Method Blank Summary ................................................................................................31
6.2: Blank Spike Summary ...................................................................................................33
6.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................35
Section 7: GC Volatiles - QC Data Summaries .....................................................................37
7.1: Method Blank Summary ................................................................................................38
7.2: Blank Spike/Blank Spike Duplicate Summary ..............................................................39
7.3: Duplicate Summary .......................................................................................................40
Section 8: GC Semi-volatiles - QC Data Summaries ............................................................41
8.1: Method Blank Summary ................................................................................................42
8.2: Blank Spike/Blank Spike Duplicate Summary ..............................................................43
8.3: Duplicate Summary .......................................................................................................45 123456782 of 45
FA43510
SGS Accutest
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA43510
Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Project No: 4236
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA43510-1 04/26/17 16:18 AR 04/28/17 SO Soil MW-1 (18')
FA43510-2 04/26/17 16:31 AR 04/28/17 SO Soil MW-2 (28')
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
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FA435101
Summary of Hits Page 1 of 2
Job Number:FA43510
Account:GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Collected:04/26/17
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA43510-1 MW-1 (18')
n-Butylbenzene 3.51 0.39 0.078 mg/kg SW846 8260B
Cyclohexane 0.0991 J 0.39 0.098 mg/kg SW846 8260B
Ethylbenzene 1.05 0.39 0.078 mg/kg SW846 8260B
Isopropylbenzene 1.90 0.39 0.078 mg/kg SW846 8260B
Methylcyclohexane 0.419 0.39 0.13 mg/kg SW846 8260B
Methylene Chloride a 0.499 JB 0.78 0.31 mg/kg SW846 8260B
Naphthalene 21.6 3.9 1.6 mg/kg SW846 8260B
n-Propylbenzene 2.79 0.39 0.078 mg/kg SW846 8260B
Toluene 0.236 J 0.39 0.078 mg/kg SW846 8260B
1,2,4-Trimethylbenzene 11.4 0.39 0.078 mg/kg SW846 8260B
1,3,5-Trimethylbenzene 4.06 0.39 0.078 mg/kg SW846 8260B
Xylene (total)6.38 1.2 0.16 mg/kg SW846 8260B
Acenaphthene b 2.73 2.0 0.22 mg/kg SW846 8270D
Fluorene b 3.49 2.0 0.22 mg/kg SW846 8270D
1-Methylnaphthalene b 19.0 2.0 0.20 mg/kg SW846 8270D
2-Methylnaphthalene b 24.3 2.0 0.20 mg/kg SW846 8270D
Naphthalene b 4.24 2.0 0.20 mg/kg SW846 8270D
Phenanthrene b 9.08 2.0 0.20 mg/kg SW846 8270D
Pyrene b 2.27 2.0 0.24 mg/kg SW846 8270D
Ethylbenzene 1.33 0.16 0.082 mg/kg MADEP VPH REV 1.1
Naphthalene 68.4 8.2 4.9 mg/kg MADEP VPH REV 1.1
Toluene 0.264 0.16 0.082 mg/kg MADEP VPH REV 1.1
m,p-Xylene 2.88 0.33 0.16 mg/kg MADEP VPH REV 1.1
o-Xylene 2.92 0.16 0.082 mg/kg MADEP VPH REV 1.1
C5- C8 Aliphatics (Unadj.)15.4 8.2 2.9 mg/kg MADEP VPH REV 1.1
C9- C12 Aliphatics (Unadj.)299 160 57 mg/kg MADEP VPH REV 1.1
C9- C10 Aromatics (Unadj.)462 160 57 mg/kg MADEP VPH REV 1.1
C5- C8 Aliphatics 15.0 8.2 2.9 mg/kg MADEP VPH REV 1.1
C9- C12 Aliphatics 287 160 57 mg/kg MADEP VPH REV 1.1
C9- C10 Aromatics 462 160 57 mg/kg MADEP VPH REV 1.1
2-Methylnaphthalene c 40.9 12 6.1 mg/kg MADEP EPH REV 1.1
Phenanthrene c 15.7 12 6.1 mg/kg MADEP EPH REV 1.1
C11-C22 Aromatics (Unadj.) c 1750 610 250 mg/kg MADEP EPH REV 1.1
C11-C22 Aromatics c 1670 610 250 mg/kg MADEP EPH REV 1.1
C9-C18 Aliphatics c 3390 610 150 mg/kg MADEP EPH REV 1.1
C19-C36 Aliphatics c 645 610 150 mg/kg MADEP EPH REV 1.1
FA43510-2 MW-2 (28')
n-Butylbenzene 3.67 0.57 0.11 mg/kg SW846 8260B
Ethylbenzene 1.16 0.57 0.11 mg/kg SW846 8260B
Isopropylbenzene 2.10 0.57 0.11 mg/kg SW846 8260B
Methylcyclohexane 0.308 J 0.57 0.20 mg/kg SW846 8260B
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FA435102
Summary of Hits Page 2 of 2
Job Number:FA43510
Account:GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Collected:04/26/17
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
Methylene Chloride a 0.855 JB 1.1 0.46 mg/kg SW846 8260B
Methyl Tert Butyl Ether 0.348 J 0.57 0.11 mg/kg SW846 8260B
Naphthalene 28.5 5.7 2.3 mg/kg SW846 8260B
n-Propylbenzene 3.18 0.57 0.11 mg/kg SW846 8260B
Toluene 0.261 J 0.57 0.11 mg/kg SW846 8260B
1,2,4-Trimethylbenzene 14.6 0.57 0.11 mg/kg SW846 8260B
1,3,5-Trimethylbenzene 4.85 0.57 0.11 mg/kg SW846 8260B
Xylene (total)7.21 1.7 0.24 mg/kg SW846 8260B
Fluorene b 4.16 2.6 0.28 mg/kg SW846 8270D
1-Methylnaphthalene b 23.0 2.6 0.26 mg/kg SW846 8270D
2-Methylnaphthalene b 30.4 2.6 0.26 mg/kg SW846 8270D
Naphthalene b 5.31 2.6 0.26 mg/kg SW846 8270D
Phenanthrene b 10.8 2.6 0.26 mg/kg SW846 8270D
Ethylbenzene 1.16 0.19 0.094 mg/kg MADEP VPH REV 1.1
Methyl Tert Butyl Ether 0.242 0.19 0.094 mg/kg MADEP VPH REV 1.1
Naphthalene 26.4 0.47 0.28 mg/kg MADEP VPH REV 1.1
Toluene 0.228 0.19 0.094 mg/kg MADEP VPH REV 1.1
m,p-Xylene 2.50 0.38 0.19 mg/kg MADEP VPH REV 1.1
o-Xylene 3.23 0.19 0.094 mg/kg MADEP VPH REV 1.1
C5- C8 Aliphatics (Unadj.)20.9 9.4 3.3 mg/kg MADEP VPH REV 1.1
C9- C12 Aliphatics (Unadj.)312 190 66 mg/kg MADEP VPH REV 1.1
C9- C10 Aromatics (Unadj.)426 190 66 mg/kg MADEP VPH REV 1.1
C5- C8 Aliphatics 20.4 9.4 3.3 mg/kg MADEP VPH REV 1.1
C9- C12 Aliphatics 300 190 66 mg/kg MADEP VPH REV 1.1
C9- C10 Aromatics 426 190 66 mg/kg MADEP VPH REV 1.1
2-Methylnaphthalene c 39.4 15 7.7 mg/kg MADEP EPH REV 1.1
Phenanthrene c 14.7 J 15 7.7 mg/kg MADEP EPH REV 1.1
C11-C22 Aromatics (Unadj.) c 1610 770 310 mg/kg MADEP EPH REV 1.1
C11-C22 Aromatics c 1540 770 310 mg/kg MADEP EPH REV 1.1
C9-C18 Aliphatics c 3580 770 190 mg/kg MADEP EPH REV 1.1
C19-C36 Aliphatics c 675 J 770 190 mg/kg MADEP EPH REV 1.1
(a) Suspected laboratory contaminant.
(b) Dilution required due to matrix interference (internal standard failure).
(c) Dilution required due to matrix interference.
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FA435102
SGS Accutest
Sample Results
Report of Analysis
Southeast
Section 3
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FA435103
SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID:MW-1 (18')
Lab Sample ID:FA43510-1 Date Sampled:04/26/17
Matrix:SO - Soil Date Received:04/28/17
Method:SW846 8260B Percent Solids:80.6
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 C0122022.D 1 05/01/17 EP n/a n/a VC4830
Run #2 C0122023.D 1 05/01/17 EP n/a n/a VC4830
Initial Weight Final Volume Methanol Aliquot
Run #1 4.70 g 5.0 ml 100 ul
Run #2 4.70 g 5.0 ml 10.0 ul
VOA Special List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 3.9 0.78 mg/kg
71-43-2 Benzene ND 0.39 0.095 mg/kg
75-27-4 Bromodichloromethane ND 0.39 0.078 mg/kg
75-25-2 Bromoform ND 0.39 0.078 mg/kg
78-93-3 2-Butanone (MEK)ND 2.0 0.57 mg/kg
104-51-8 n-Butylbenzene 3.51 0.39 0.078 mg/kg
75-15-0 Carbon Disulfide ND 0.39 0.078 mg/kg
56-23-5 Carbon Tetrachloride ND 0.39 0.080 mg/kg
108-90-7 Chlorobenzene ND 0.39 0.078 mg/kg
75-00-3 Chloroethane ND 0.39 0.16 mg/kg
67-66-3 Chloroform ND 0.39 0.10 mg/kg
110-82-7 Cyclohexane 0.0991 0.39 0.098 mg/kg J
124-48-1 Dibromochloromethane ND 0.39 0.078 mg/kg
96-12-8 1,2-Dibromo-3-chloropropane ND 0.39 0.15 mg/kg
106-93-4 1,2-Dibromoethane ND 0.39 0.078 mg/kg
75-71-8 Dichlorodifluoromethane ND 0.39 0.16 mg/kg
95-50-1 1,2-Dichlorobenzene ND 0.39 0.078 mg/kg
541-73-1 1,3-Dichlorobenzene ND 0.39 0.078 mg/kg
106-46-7 1,4-Dichlorobenzene ND 0.39 0.090 mg/kg
75-34-3 1,1-Dichloroethane ND 0.39 0.14 mg/kg
107-06-2 1,2-Dichloroethane ND 0.39 0.078 mg/kg
75-35-4 1,1-Dichloroethylene ND 0.39 0.078 mg/kg
156-59-2 cis-1,2-Dichloroethylene ND 0.39 0.11 mg/kg
156-60-5 trans-1,2-Dichloroethylene ND 0.39 0.078 mg/kg
78-87-5 1,2-Dichloropropane ND 0.39 0.078 mg/kg
10061-01-5 cis-1,3-Dichloropropene ND 0.39 0.078 mg/kg
10061-02-6 trans-1,3-Dichloropropene ND 0.39 0.078 mg/kg
100-41-4 Ethylbenzene 1.05 0.39 0.078 mg/kg
591-78-6 2-Hexanone ND 2.0 0.59 mg/kg
98-82-8 Isopropylbenzene 1.90 0.39 0.078 mg/kg
79-20-9 Methyl Acetate ND 2.0 0.70 mg/kg
74-83-9 Methyl Bromide ND 0.39 0.16 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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FA4351033.1
SGS Accutest
Report of Analysis Page 2 of 2
Client Sample ID:MW-1 (18')
Lab Sample ID:FA43510-1 Date Sampled:04/26/17
Matrix:SO - Soil Date Received:04/28/17
Method:SW846 8260B Percent Solids:80.6
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
VOA Special List
CAS No.Compound Result RL MDL Units Q
74-87-3 Methyl Chloride ND 0.39 0.16 mg/kg
108-87-2 Methylcyclohexane 0.419 0.39 0.13 mg/kg
75-09-2 Methylene Chloride a 0.499 0.78 0.31 mg/kg JB
108-10-1 4-Methyl-2-pentanone (MIBK)ND 2.0 0.59 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.39 0.078 mg/kg
91-20-3 Naphthalene 21.6 b 3.9 1.6 mg/kg
103-65-1 n-Propylbenzene 2.79 0.39 0.078 mg/kg
100-42-5 Styrene ND 0.39 0.078 mg/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 0.39 0.078 mg/kg
127-18-4 Tetrachloroethylene ND 0.39 0.10 mg/kg
108-88-3 Toluene 0.236 0.39 0.078 mg/kg J
120-82-1 1,2,4-Trichlorobenzene ND 0.39 0.078 mg/kg
71-55-6 1,1,1-Trichloroethane ND 0.39 0.078 mg/kg
79-00-5 1,1,2-Trichloroethane ND 0.39 0.078 mg/kg
79-01-6 Trichloroethylene ND 0.39 0.078 mg/kg
75-69-4 Trichlorofluoromethane ND 0.39 0.16 mg/kg
95-63-6 1,2,4-Trimethylbenzene 11.4 0.39 0.078 mg/kg
108-67-8 1,3,5-Trimethylbenzene 4.06 0.39 0.078 mg/kg
75-01-4 Vinyl Chloride ND 0.39 0.078 mg/kg
1330-20-7 Xylene (total)6.38 1.2 0.16 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 110%110%75-124%
17060-07-0 1,2-Dichloroethane-D4 108%109%72-135%
2037-26-5 Toluene-D8 102%98%75-126%
460-00-4 4-Bromofluorobenzene 97%96%71-133%
(a) Suspected laboratory contaminant.
(b) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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FA4351033.1
SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID:MW-1 (18')
Lab Sample ID:FA43510-1 Date Sampled:04/26/17
Matrix:SO - Soil Date Received:04/28/17
Method:SW846 8270D SW846 3550C Percent Solids:80.6
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a X053806.D 10 05/04/17 NG 05/02/17 OP64869 SX2276
Run #2
Initial Weight Final Volume
Run #1 30.3 g 1.0 ml
Run #2
ABN Special List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 10 2.0 mg/kg
59-50-7 4-Chloro-3-methyl Phenol ND 2.0 0.23 mg/kg
95-57-8 2-Chlorophenol ND 2.0 0.25 mg/kg
120-83-2 2,4-Dichlorophenol ND 2.0 0.24 mg/kg
105-67-9 2,4-Dimethylphenol ND 2.0 0.54 mg/kg
51-28-5 2,4-Dinitrophenol ND 10 2.0 mg/kg
534-52-1 4,6-Dinitro-o-cresol ND 4.1 0.82 mg/kg
95-48-7 2-Methylphenol ND 2.0 0.25 mg/kg
3&4-Methylphenol ND 2.0 0.34 mg/kg
88-75-5 2-Nitrophenol ND 2.0 0.22 mg/kg
100-02-7 4-Nitrophenol ND 10 2.0 mg/kg
87-86-5 Pentachlorophenol ND 10 2.0 mg/kg
108-95-2 Phenol ND 2.0 0.20 mg/kg
88-06-2 2,4,6-Trichlorophenol ND 2.0 0.24 mg/kg
83-32-9 Acenaphthene 2.73 2.0 0.22 mg/kg
208-96-8 Acenaphthylene ND 2.0 0.20 mg/kg
120-12-7 Anthracene ND 2.0 0.23 mg/kg
56-55-3 Benzo(a)anthracene ND 2.0 0.20 mg/kg
50-32-8 Benzo(a)pyrene ND 2.0 0.24 mg/kg
205-99-2 Benzo(b)fluoranthene ND 2.0 0.22 mg/kg
191-24-2 Benzo(g,h,i)perylene ND 2.0 0.21 mg/kg
207-08-9 Benzo(k)fluoranthene ND 2.0 0.27 mg/kg
101-55-3 4-Bromophenyl phenyl ether ND 2.0 0.21 mg/kg
85-68-7 Butyl benzyl phthalate ND 2.0 0.41 mg/kg
106-47-8 4-Chloroaniline ND 2.0 0.52 mg/kg
111-91-1 bis(2-Chloroethoxy)methane ND 2.0 0.20 mg/kg
111-44-4 bis(2-Chloroethyl)ether ND 2.0 0.24 mg/kg
108-60-1 bis(2-Chloroisopropyl)ether ND 2.0 0.26 mg/kg
91-58-7 2-Chloronaphthalene ND 2.0 0.20 mg/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 2.0 0.20 mg/kg
218-01-9 Chrysene ND 2.0 0.21 mg/kg
53-70-3 Dibenzo(a,h)anthracene ND 2.0 0.26 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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FA4351033.1
SGS Accutest
Report of Analysis Page 2 of 2
Client Sample ID:MW-1 (18')
Lab Sample ID:FA43510-1 Date Sampled:04/26/17
Matrix:SO - Soil Date Received:04/28/17
Method:SW846 8270D SW846 3550C Percent Solids:80.6
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
ABN Special List
CAS No.Compound Result RL MDL Units Q
132-64-9 Dibenzofuran ND 2.0 0.20 mg/kg
91-94-1 3,3'-Dichlorobenzidine ND 2.0 0.49 mg/kg
84-66-2 Diethyl Phthalate ND 4.1 0.41 mg/kg
131-11-3 Dimethyl Phthalate ND 2.0 0.41 mg/kg
117-84-0 Di-n-octyl Phthalate ND 2.0 0.41 mg/kg
84-74-2 Di-n-butyl Phthalate ND 4.1 0.82 mg/kg
121-14-2 2,4-Dinitrotoluene ND 2.0 0.20 mg/kg
606-20-2 2,6-Dinitrotoluene ND 2.0 0.26 mg/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 4.1 0.41 mg/kg
206-44-0 Fluoranthene ND 2.0 0.20 mg/kg
86-73-7 Fluorene 3.49 2.0 0.22 mg/kg
118-74-1 Hexachlorobenzene ND 2.0 0.21 mg/kg
87-68-3 Hexachlorobutadiene ND 2.0 0.21 mg/kg
77-47-4 Hexachlorocyclopentadiene ND 2.0 0.41 mg/kg
67-72-1 Hexachloroethane ND 2.0 0.24 mg/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 2.0 0.25 mg/kg
78-59-1 Isophorone ND 2.0 0.20 mg/kg
90-12-0 1-Methylnaphthalene 19.0 2.0 0.20 mg/kg
91-57-6 2-Methylnaphthalene 24.3 2.0 0.20 mg/kg
91-20-3 Naphthalene 4.24 2.0 0.20 mg/kg
98-95-3 Nitrobenzene ND 2.0 0.20 mg/kg
621-64-7 N-Nitrosodi-n-propylamine ND 2.0 0.20 mg/kg
86-30-6 N-Nitrosodiphenylamine ND 2.0 0.22 mg/kg
85-01-8 Phenanthrene 9.08 2.0 0.20 mg/kg
129-00-0 Pyrene 2.27 2.0 0.24 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 54%40-102%
4165-62-2 Phenol-d5 53%41-100%
118-79-6 2,4,6-Tribromophenol 57%42-108%
4165-60-0 Nitrobenzene-d5 78%40-105%
321-60-8 2-Fluorobiphenyl 60%43-107%
1718-51-0 Terphenyl-d14 62%45-119%
(a) Dilution required due to matrix interference (internal standard failure).
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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FA4351033.1
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Report of Analysis Page 1 of 1
Client Sample ID:MW-1 (18')
Lab Sample ID:FA43510-1 Date Sampled:04/26/17
Matrix:SO - Soil Date Received:04/28/17
Method:MADEP VPH REV 1.1 Percent Solids:80.6
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 UU020264.D 1 05/05/17 AJC n/a n/a GUU1064
Run #2 UU020263.D 1 05/05/17 AJC n/a n/a GUU1064
Initial Weight Final Volume Methanol Aliquot
Run #1 4.52 g 5.1 ml 100 ul
Run #2 4.52 g 5.1 ml 5.0 ul
MADEP VPH List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.082 0.082 mg/kg
100-41-4 Ethylbenzene 1.33 0.16 0.082 mg/kg
91-20-3 Naphthalene 68.4 a 8.2 4.9 mg/kg
108-88-3 Toluene 0.264 0.16 0.082 mg/kg
m,p-Xylene 2.88 0.33 0.16 mg/kg
95-47-6 o-Xylene 2.92 0.16 0.082 mg/kg
C5- C8 Aliphatics (Unadj.)15.4 8.2 2.9 mg/kg
C9- C12 Aliphatics (Unadj.)299 a 160 57 mg/kg
C9- C10 Aromatics (Unadj.)462 a 160 57 mg/kg
C5- C8 Aliphatics 15.0 8.2 2.9 mg/kg
C9- C12 Aliphatics 287 a 160 57 mg/kg
C9- C10 Aromatics 462 a 160 57 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 BFB 127%0% b 70-130%
460-00-4 BFB 98%0% b 70-130%
(a) Result is from Run# 2
(b) Outside control limits due to dilution.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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FA4351033.1
SGS Accutest
Report of Analysis Page 1 of 1
Client Sample ID:MW-1 (18')
Lab Sample ID:FA43510-1 Date Sampled:04/26/17
Matrix:SO - Soil Date Received:04/28/17
Method:MADEP EPH REV 1.1 SW846 3546 Percent Solids:80.6
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a NN018649.D 50 05/08/17 MG 05/01/17 OP64856 GNN934
Run #2
Initial Weight Final Volume
Run #1 20.2 g 2.0 ml
Run #2
MAEPH List
CAS No.Compound Result RL MDL Units Q
83-32-9 Acenaphthene ND 12 6.1 mg/kg
208-96-8 Acenaphthylene ND 12 6.1 mg/kg
120-12-7 Anthracene ND 12 6.1 mg/kg
56-55-3 Benzo(a)anthracene ND 12 6.1 mg/kg
50-32-8 Benzo(a)pyrene ND 12 6.1 mg/kg
205-99-2 Benzo(b)fluoranthene ND 12 6.1 mg/kg
191-24-2 Benzo(g,h,i)perylene ND 12 6.1 mg/kg
207-08-9 Benzo(k)fluoranthene ND 12 6.1 mg/kg
218-01-9 Chrysene ND 12 6.1 mg/kg
53-70-3 Dibenzo(a,h)anthracene ND 12 6.1 mg/kg
206-44-0 Fluoranthene ND 12 6.1 mg/kg
86-73-7 Fluorene ND 12 6.1 mg/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 12 6.1 mg/kg
91-57-6 2-Methylnaphthalene 40.9 12 6.1 mg/kg
91-20-3 Naphthalene ND 12 6.1 mg/kg
85-01-8 Phenanthrene 15.7 12 6.1 mg/kg
129-00-0 Pyrene ND 12 6.1 mg/kg
C11-C22 Aromatics (Unadj.)1750 610 250 mg/kg
C11-C22 Aromatics 1670 610 250 mg/kg
C9-C18 Aliphatics 3390 610 150 mg/kg
C19-C36 Aliphatics 645 610 150 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
3386-33-2 1-Chlorooctadecane 0% b 40-140%
580-13-2 2-Bromonaphthalene 0% b 40-140%
84-15-1 o-Terphenyl 0% b 40-140%
321-60-8 2-Fluorobiphenyl 0% b 40-140%
(a) Dilution required due to matrix interference.
(b) Outside control limits due to dilution.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 45
FA4351033.1
SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID:MW-2 (28')
Lab Sample ID:FA43510-2 Date Sampled:04/26/17
Matrix:SO - Soil Date Received:04/28/17
Method:SW846 8260B Percent Solids:63.9
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 C0122024.D 1 05/01/17 EP n/a n/a VC4830
Run #2 C0122025.D 1 05/01/17 EP n/a n/a VC4830
Initial Weight Final Volume Methanol Aliquot
Run #1 4.51 g 5.0 ml 100 ul
Run #2 4.51 g 5.0 ml 10.0 ul
VOA Special List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 5.7 1.1 mg/kg
71-43-2 Benzene ND 0.57 0.14 mg/kg
75-27-4 Bromodichloromethane ND 0.57 0.11 mg/kg
75-25-2 Bromoform ND 0.57 0.11 mg/kg
78-93-3 2-Butanone (MEK)ND 2.9 0.84 mg/kg
104-51-8 n-Butylbenzene 3.67 0.57 0.11 mg/kg
75-15-0 Carbon Disulfide ND 0.57 0.11 mg/kg
56-23-5 Carbon Tetrachloride ND 0.57 0.12 mg/kg
108-90-7 Chlorobenzene ND 0.57 0.11 mg/kg
75-00-3 Chloroethane ND 0.57 0.23 mg/kg
67-66-3 Chloroform ND 0.57 0.15 mg/kg
110-82-7 Cyclohexane ND 0.57 0.14 mg/kg
124-48-1 Dibromochloromethane ND 0.57 0.11 mg/kg
96-12-8 1,2-Dibromo-3-chloropropane ND 0.57 0.22 mg/kg
106-93-4 1,2-Dibromoethane ND 0.57 0.11 mg/kg
75-71-8 Dichlorodifluoromethane ND 0.57 0.23 mg/kg
95-50-1 1,2-Dichlorobenzene ND 0.57 0.11 mg/kg
541-73-1 1,3-Dichlorobenzene ND 0.57 0.11 mg/kg
106-46-7 1,4-Dichlorobenzene ND 0.57 0.13 mg/kg
75-34-3 1,1-Dichloroethane ND 0.57 0.20 mg/kg
107-06-2 1,2-Dichloroethane ND 0.57 0.11 mg/kg
75-35-4 1,1-Dichloroethylene ND 0.57 0.11 mg/kg
156-59-2 cis-1,2-Dichloroethylene ND 0.57 0.16 mg/kg
156-60-5 trans-1,2-Dichloroethylene ND 0.57 0.11 mg/kg
78-87-5 1,2-Dichloropropane ND 0.57 0.11 mg/kg
10061-01-5 cis-1,3-Dichloropropene ND 0.57 0.11 mg/kg
10061-02-6 trans-1,3-Dichloropropene ND 0.57 0.11 mg/kg
100-41-4 Ethylbenzene 1.16 0.57 0.11 mg/kg
591-78-6 2-Hexanone ND 2.9 0.86 mg/kg
98-82-8 Isopropylbenzene 2.10 0.57 0.11 mg/kg
79-20-9 Methyl Acetate ND 2.9 1.0 mg/kg
74-83-9 Methyl Bromide ND 0.57 0.23 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
13 of 45
FA4351033.2
SGS Accutest
Report of Analysis Page 2 of 2
Client Sample ID:MW-2 (28')
Lab Sample ID:FA43510-2 Date Sampled:04/26/17
Matrix:SO - Soil Date Received:04/28/17
Method:SW846 8260B Percent Solids:63.9
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
VOA Special List
CAS No.Compound Result RL MDL Units Q
74-87-3 Methyl Chloride ND 0.57 0.23 mg/kg
108-87-2 Methylcyclohexane 0.308 0.57 0.20 mg/kg J
75-09-2 Methylene Chloride a 0.855 1.1 0.46 mg/kg JB
108-10-1 4-Methyl-2-pentanone (MIBK)ND 2.9 0.86 mg/kg
1634-04-4 Methyl Tert Butyl Ether 0.348 0.57 0.11 mg/kg J
91-20-3 Naphthalene 28.5 b 5.7 2.3 mg/kg
103-65-1 n-Propylbenzene 3.18 0.57 0.11 mg/kg
100-42-5 Styrene ND 0.57 0.11 mg/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 0.57 0.11 mg/kg
127-18-4 Tetrachloroethylene ND 0.57 0.15 mg/kg
108-88-3 Toluene 0.261 0.57 0.11 mg/kg J
120-82-1 1,2,4-Trichlorobenzene ND 0.57 0.11 mg/kg
71-55-6 1,1,1-Trichloroethane ND 0.57 0.11 mg/kg
79-00-5 1,1,2-Trichloroethane ND 0.57 0.11 mg/kg
79-01-6 Trichloroethylene ND 0.57 0.11 mg/kg
75-69-4 Trichlorofluoromethane ND 0.57 0.23 mg/kg
95-63-6 1,2,4-Trimethylbenzene 14.6 0.57 0.11 mg/kg
108-67-8 1,3,5-Trimethylbenzene 4.85 0.57 0.11 mg/kg
75-01-4 Vinyl Chloride ND 0.57 0.11 mg/kg
1330-20-7 Xylene (total)7.21 1.7 0.24 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 108%109%75-124%
17060-07-0 1,2-Dichloroethane-D4 108%106%72-135%
2037-26-5 Toluene-D8 98%99%75-126%
460-00-4 4-Bromofluorobenzene 98%95%71-133%
(a) Suspected laboratory contaminant.
(b) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
14 of 45
FA4351033.2
SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID:MW-2 (28')
Lab Sample ID:FA43510-2 Date Sampled:04/26/17
Matrix:SO - Soil Date Received:04/28/17
Method:SW846 8270D SW846 3550C Percent Solids:63.9
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a X053807.D 10 05/04/17 NG 05/02/17 OP64869 SX2276
Run #2
Initial Weight Final Volume
Run #1 30.4 g 1.0 ml
Run #2
ABN Special List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 13 2.6 mg/kg
59-50-7 4-Chloro-3-methyl Phenol ND 2.6 0.29 mg/kg
95-57-8 2-Chlorophenol ND 2.6 0.32 mg/kg
120-83-2 2,4-Dichlorophenol ND 2.6 0.30 mg/kg
105-67-9 2,4-Dimethylphenol ND 2.6 0.68 mg/kg
51-28-5 2,4-Dinitrophenol ND 13 2.6 mg/kg
534-52-1 4,6-Dinitro-o-cresol ND 5.1 1.0 mg/kg
95-48-7 2-Methylphenol ND 2.6 0.31 mg/kg
3&4-Methylphenol ND 2.6 0.42 mg/kg
88-75-5 2-Nitrophenol ND 2.6 0.28 mg/kg
100-02-7 4-Nitrophenol ND 13 2.6 mg/kg
87-86-5 Pentachlorophenol ND 13 2.6 mg/kg
108-95-2 Phenol ND 2.6 0.26 mg/kg
88-06-2 2,4,6-Trichlorophenol ND 2.6 0.30 mg/kg
83-32-9 Acenaphthene ND 2.6 0.27 mg/kg
208-96-8 Acenaphthylene ND 2.6 0.26 mg/kg
120-12-7 Anthracene ND 2.6 0.29 mg/kg
56-55-3 Benzo(a)anthracene ND 2.6 0.26 mg/kg
50-32-8 Benzo(a)pyrene ND 2.6 0.30 mg/kg
205-99-2 Benzo(b)fluoranthene ND 2.6 0.28 mg/kg
191-24-2 Benzo(g,h,i)perylene ND 2.6 0.27 mg/kg
207-08-9 Benzo(k)fluoranthene ND 2.6 0.34 mg/kg
101-55-3 4-Bromophenyl phenyl ether ND 2.6 0.27 mg/kg
85-68-7 Butyl benzyl phthalate ND 2.6 0.51 mg/kg
106-47-8 4-Chloroaniline ND 2.6 0.65 mg/kg
111-91-1 bis(2-Chloroethoxy)methane ND 2.6 0.26 mg/kg
111-44-4 bis(2-Chloroethyl)ether ND 2.6 0.30 mg/kg
108-60-1 bis(2-Chloroisopropyl)ether ND 2.6 0.32 mg/kg
91-58-7 2-Chloronaphthalene ND 2.6 0.26 mg/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 2.6 0.26 mg/kg
218-01-9 Chrysene ND 2.6 0.26 mg/kg
53-70-3 Dibenzo(a,h)anthracene ND 2.6 0.32 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
15 of 45
FA4351033.2
SGS Accutest
Report of Analysis Page 2 of 2
Client Sample ID:MW-2 (28')
Lab Sample ID:FA43510-2 Date Sampled:04/26/17
Matrix:SO - Soil Date Received:04/28/17
Method:SW846 8270D SW846 3550C Percent Solids:63.9
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
ABN Special List
CAS No.Compound Result RL MDL Units Q
132-64-9 Dibenzofuran ND 2.6 0.26 mg/kg
91-94-1 3,3'-Dichlorobenzidine ND 2.6 0.61 mg/kg
84-66-2 Diethyl Phthalate ND 5.1 0.51 mg/kg
131-11-3 Dimethyl Phthalate ND 2.6 0.51 mg/kg
117-84-0 Di-n-octyl Phthalate ND 2.6 0.51 mg/kg
84-74-2 Di-n-butyl Phthalate ND 5.1 1.0 mg/kg
121-14-2 2,4-Dinitrotoluene ND 2.6 0.26 mg/kg
606-20-2 2,6-Dinitrotoluene ND 2.6 0.33 mg/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 5.1 0.51 mg/kg
206-44-0 Fluoranthene ND 2.6 0.26 mg/kg
86-73-7 Fluorene 4.16 2.6 0.28 mg/kg
118-74-1 Hexachlorobenzene ND 2.6 0.26 mg/kg
87-68-3 Hexachlorobutadiene ND 2.6 0.26 mg/kg
77-47-4 Hexachlorocyclopentadiene ND 2.6 0.51 mg/kg
67-72-1 Hexachloroethane ND 2.6 0.30 mg/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 2.6 0.31 mg/kg
78-59-1 Isophorone ND 2.6 0.26 mg/kg
90-12-0 1-Methylnaphthalene 23.0 2.6 0.26 mg/kg
91-57-6 2-Methylnaphthalene 30.4 2.6 0.26 mg/kg
91-20-3 Naphthalene 5.31 2.6 0.26 mg/kg
98-95-3 Nitrobenzene ND 2.6 0.26 mg/kg
621-64-7 N-Nitrosodi-n-propylamine ND 2.6 0.26 mg/kg
86-30-6 N-Nitrosodiphenylamine ND 2.6 0.28 mg/kg
85-01-8 Phenanthrene 10.8 2.6 0.26 mg/kg
129-00-0 Pyrene ND 2.6 0.30 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 82%40-102%
4165-62-2 Phenol-d5 85%41-100%
118-79-6 2,4,6-Tribromophenol 92%42-108%
4165-60-0 Nitrobenzene-d5 109% b 40-105%
321-60-8 2-Fluorobiphenyl 98%43-107%
1718-51-0 Terphenyl-d14 98%45-119%
(a) Dilution required due to matrix interference (internal standard failure).
(b) Outside control limits due to dilution.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
16 of 45
FA4351033.2
SGS Accutest
Report of Analysis Page 1 of 1
Client Sample ID:MW-2 (28')
Lab Sample ID:FA43510-2 Date Sampled:04/26/17
Matrix:SO - Soil Date Received:04/28/17
Method:MADEP VPH REV 1.1 Percent Solids:63.9
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 UU020267.D 1 05/05/17 AJC n/a n/a GUU1064
Run #2 UU020266.D 1 05/05/17 AJC n/a n/a GUU1064
Initial Weight Final Volume Methanol Aliquot
Run #1 6.07 g 5.1 ml 100 ul
Run #2 6.07 g 5.1 ml 5.0 ul
MADEP VPH List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.094 0.094 mg/kg
100-41-4 Ethylbenzene 1.16 0.19 0.094 mg/kg
1634-04-4 Methyl Tert Butyl Ether 0.242 0.19 0.094 mg/kg
91-20-3 Naphthalene 26.4 0.47 0.28 mg/kg
108-88-3 Toluene 0.228 0.19 0.094 mg/kg
m,p-Xylene 2.50 0.38 0.19 mg/kg
95-47-6 o-Xylene 3.23 0.19 0.094 mg/kg
C5- C8 Aliphatics (Unadj.)20.9 9.4 3.3 mg/kg
C9- C12 Aliphatics (Unadj.)312 a 190 66 mg/kg
C9- C10 Aromatics (Unadj.)426 a 190 66 mg/kg
C5- C8 Aliphatics 20.4 9.4 3.3 mg/kg
C9- C12 Aliphatics 300 a 190 66 mg/kg
C9- C10 Aromatics 426 a 190 66 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 BFB 155%0% b 70-130%
460-00-4 BFB 113%0% b 70-130%
(a) Result is from Run# 2
(b) Outside control limits due to dilution.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
17 of 45
FA4351033.2
SGS Accutest
Report of Analysis Page 1 of 1
Client Sample ID:MW-2 (28')
Lab Sample ID:FA43510-2 Date Sampled:04/26/17
Matrix:SO - Soil Date Received:04/28/17
Method:MADEP EPH REV 1.1 SW846 3546 Percent Solids:63.9
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a NN018651.D 50 05/08/17 MG 05/01/17 OP64856 GNN934
Run #2
Initial Weight Final Volume
Run #1 20.4 g 2.0 ml
Run #2
MAEPH List
CAS No.Compound Result RL MDL Units Q
83-32-9 Acenaphthene ND 15 7.7 mg/kg
208-96-8 Acenaphthylene ND 15 7.7 mg/kg
120-12-7 Anthracene ND 15 7.7 mg/kg
56-55-3 Benzo(a)anthracene ND 15 7.7 mg/kg
50-32-8 Benzo(a)pyrene ND 15 7.7 mg/kg
205-99-2 Benzo(b)fluoranthene ND 15 7.7 mg/kg
191-24-2 Benzo(g,h,i)perylene ND 15 7.7 mg/kg
207-08-9 Benzo(k)fluoranthene ND 15 7.7 mg/kg
218-01-9 Chrysene ND 15 7.7 mg/kg
53-70-3 Dibenzo(a,h)anthracene ND 15 7.7 mg/kg
206-44-0 Fluoranthene ND 15 7.7 mg/kg
86-73-7 Fluorene ND 15 7.7 mg/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 15 7.7 mg/kg
91-57-6 2-Methylnaphthalene 39.4 15 7.7 mg/kg
91-20-3 Naphthalene ND 15 7.7 mg/kg
85-01-8 Phenanthrene 14.7 15 7.7 mg/kg J
129-00-0 Pyrene ND 15 7.7 mg/kg
C11-C22 Aromatics (Unadj.)1610 770 310 mg/kg
C11-C22 Aromatics 1540 770 310 mg/kg
C9-C18 Aliphatics 3580 770 190 mg/kg
C19-C36 Aliphatics 675 770 190 mg/kg J
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
3386-33-2 1-Chlorooctadecane 0% b 40-140%
580-13-2 2-Bromonaphthalene 0% b 40-140%
84-15-1 o-Terphenyl 0% b 40-140%
321-60-8 2-Fluorobiphenyl 0% b 40-140%
(a) Dilution required due to matrix interference.
(b) Outside control limits due to dilution.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
18 of 45
FA4351033.2
SGS Accutest
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Southeast
Section 4
19 of 45
FA435104
FA43510: Chain of Custody
Page 1 of 3
20 of 45
FA4351044.1
FA43510: Chain of Custody
Page 2 of 3
21 of 45
FA4351044.1
FA43510: Chain of Custody
Page 3 of 3
22 of 45
FA4351044.1
SGS Accutest
GC/MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Southeast
Section 5
23 of 45
FA435105
Method Blank Summary Page 1 of 2
Job Number:FA43510
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VC4830-MB C0122013.D 1 05/01/17 EP n/a n/a VC4830
The QC reported here applies to the following samples:Method: SW846 8260B
FA43510-1, FA43510-2
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 50 10 ug/kg
71-43-2 Benzene ND 5.0 1.2 ug/kg
75-27-4 Bromodichloromethane ND 5.0 1.0 ug/kg
75-25-2 Bromoform ND 5.0 1.0 ug/kg
78-93-3 2-Butanone (MEK)ND 25 7.3 ug/kg
104-51-8 n-Butylbenzene ND 5.0 1.0 ug/kg
75-15-0 Carbon Disulfide ND 5.0 1.0 ug/kg
56-23-5 Carbon Tetrachloride ND 5.0 1.0 ug/kg
108-90-7 Chlorobenzene ND 5.0 1.0 ug/kg
75-00-3 Chloroethane ND 5.0 2.0 ug/kg
67-66-3 Chloroform ND 5.0 1.3 ug/kg
110-82-7 Cyclohexane ND 5.0 1.3 ug/kg
124-48-1 Dibromochloromethane ND 5.0 1.0 ug/kg
96-12-8 1,2-Dibromo-3-chloropropane ND 5.0 1.9 ug/kg
106-93-4 1,2-Dibromoethane ND 5.0 1.0 ug/kg
75-71-8 Dichlorodifluoromethane ND 5.0 2.0 ug/kg
95-50-1 1,2-Dichlorobenzene ND 5.0 1.0 ug/kg
541-73-1 1,3-Dichlorobenzene ND 5.0 1.0 ug/kg
106-46-7 1,4-Dichlorobenzene ND 5.0 1.2 ug/kg
75-34-3 1,1-Dichloroethane ND 5.0 1.8 ug/kg
107-06-2 1,2-Dichloroethane ND 5.0 1.0 ug/kg
75-35-4 1,1-Dichloroethylene ND 5.0 1.0 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.4 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.0 ug/kg
78-87-5 1,2-Dichloropropane ND 5.0 1.0 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.0 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.0 ug/kg
100-41-4 Ethylbenzene ND 5.0 1.0 ug/kg
591-78-6 2-Hexanone ND 25 7.5 ug/kg
98-82-8 Isopropylbenzene ND 5.0 1.0 ug/kg
79-20-9 Methyl Acetate ND 25 8.9 ug/kg
74-83-9 Methyl Bromide ND 5.0 2.0 ug/kg
74-87-3 Methyl Chloride ND 5.0 2.0 ug/kg
108-87-2 Methylcyclohexane ND 5.0 1.7 ug/kg
75-09-2 Methylene Chloride 6.3 10 4.0 ug/kg J
108-10-1 4-Methyl-2-pentanone (MIBK)ND 25 7.5 ug/kg
24 of 45
FA4351055.1.1
Method Blank Summary Page 2 of 2
Job Number:FA43510
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VC4830-MB C0122013.D 1 05/01/17 EP n/a n/a VC4830
The QC reported here applies to the following samples:Method: SW846 8260B
FA43510-1, FA43510-2
CAS No.Compound Result RL MDL Units Q
1634-04-4 Methyl Tert Butyl Ether ND 5.0 1.0 ug/kg
91-20-3 Naphthalene ND 5.0 2.0 ug/kg
103-65-1 n-Propylbenzene ND 5.0 1.0 ug/kg
100-42-5 Styrene ND 5.0 1.0 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 1.0 ug/kg
127-18-4 Tetrachloroethylene ND 5.0 1.3 ug/kg
108-88-3 Toluene ND 5.0 1.0 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.0 ug/kg
71-55-6 1,1,1-Trichloroethane ND 5.0 1.0 ug/kg
79-00-5 1,1,2-Trichloroethane ND 5.0 1.0 ug/kg
79-01-6 Trichloroethylene ND 5.0 1.0 ug/kg
75-69-4 Trichlorofluoromethane ND 5.0 2.0 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 5.0 1.0 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 5.0 1.0 ug/kg
75-01-4 Vinyl Chloride ND 5.0 1.0 ug/kg
1330-20-7 Xylene (total)ND 15 2.1 ug/kg
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 107%75-124%
17060-07-0 1,2-Dichloroethane-D4 106%72-135%
2037-26-5 Toluene-D8 102%75-126%
460-00-4 4-Bromofluorobenzene 96%71-133%
25 of 45
FA4351055.1.1
Blank Spike Summary Page 1 of 2
Job Number:FA43510
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VC4830-BS C0122021.D 1 05/01/17 EP n/a n/a VC4830
The QC reported here applies to the following samples:Method: SW846 8260B
FA43510-1, FA43510-2
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
67-64-1 Acetone 250 274 110 61-152
71-43-2 Benzene 50 56.7 113 76-126
75-27-4 Bromodichloromethane 50 52.3 105 74-130
75-25-2 Bromoform 50 51.8 104 76-127
78-93-3 2-Butanone (MEK)250 284 114 75-137
104-51-8 n-Butylbenzene 50 50.6 101 71-128
75-15-0 Carbon Disulfide 50 51.0 102 72-122
56-23-5 Carbon Tetrachloride 50 51.4 103 78-133
108-90-7 Chlorobenzene 50 51.6 103 81-129
75-00-3 Chloroethane 50 48.2 96 68-133
67-66-3 Chloroform 50 52.7 105 72-123
110-82-7 Cyclohexane 50 51.3 103 73-126
124-48-1 Dibromochloromethane 50 53.8 108 76-127
96-12-8 1,2-Dibromo-3-chloropropane 50 52.5 105 70-137
106-93-4 1,2-Dibromoethane 50 50.5 101 77-126
75-71-8 Dichlorodifluoromethane 50 62.4 125 68-168
95-50-1 1,2-Dichlorobenzene 50 51.8 104 80-129
541-73-1 1,3-Dichlorobenzene 50 49.4 99 81-129
106-46-7 1,4-Dichlorobenzene 50 47.8 96 76-130
75-34-3 1,1-Dichloroethane 50 55.7 111 73-125
107-06-2 1,2-Dichloroethane 50 54.7 109 74-128
75-35-4 1,1-Dichloroethylene 50 52.2 104 81-136
156-59-2 cis-1,2-Dichloroethylene 50 54.3 109 74-126
156-60-5 trans-1,2-Dichloroethylene 50 54.3 109 70-127
78-87-5 1,2-Dichloropropane 50 51.3 103 74-125
10061-01-5 cis-1,3-Dichloropropene 50 48.5 97 80-123
10061-02-6 trans-1,3-Dichloropropene 50 52.4 105 75-131
100-41-4 Ethylbenzene 50 54.7 109 77-123
591-78-6 2-Hexanone 250 270 108 72-133
98-82-8 Isopropylbenzene 50 54.5 109 80-136
79-20-9 Methyl Acetate 250 271 108 67-137
74-83-9 Methyl Bromide 50 52.1 104 65-139
74-87-3 Methyl Chloride 50 53.8 108 71-144
108-87-2 Methylcyclohexane 50 51.9 104 75-128
75-09-2 Methylene Chloride 50 58.2 116 74-137
108-10-1 4-Methyl-2-pentanone (MIBK)250 290 116 76-132
* = Outside of Control Limits.
26 of 45
FA4351055.2.1
Blank Spike Summary Page 2 of 2
Job Number:FA43510
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VC4830-BS C0122021.D 1 05/01/17 EP n/a n/a VC4830
The QC reported here applies to the following samples:Method: SW846 8260B
FA43510-1, FA43510-2
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
1634-04-4 Methyl Tert Butyl Ether 50 54.2 108 77-120
91-20-3 Naphthalene 50 62.2 124 79-129
103-65-1 n-Propylbenzene 50 49.9 100 80-135
100-42-5 Styrene 50 54.2 108 78-125
79-34-5 1,1,2,2-Tetrachloroethane 50 51.9 104 71-126
127-18-4 Tetrachloroethylene 50 53.9 108 79-130
108-88-3 Toluene 50 56.6 113 76-124
120-82-1 1,2,4-Trichlorobenzene 50 53.5 107 78-130
71-55-6 1,1,1-Trichloroethane 50 49.8 100 70-129
79-00-5 1,1,2-Trichloroethane 50 52.4 105 74-124
79-01-6 Trichloroethylene 50 51.9 104 75-128
75-69-4 Trichlorofluoromethane 50 52.8 106 73-145
95-63-6 1,2,4-Trimethylbenzene 50 54.7 109 74-123
108-67-8 1,3,5-Trimethylbenzene 50 54.1 108 73-122
75-01-4 Vinyl Chloride 50 52.8 106 76-141
1330-20-7 Xylene (total)150 158 105 80-129
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 104%75-124%
17060-07-0 1,2-Dichloroethane-D4 103%72-135%
2037-26-5 Toluene-D8 105%75-126%
460-00-4 4-Bromofluorobenzene 98%71-133%
* = Outside of Control Limits.
27 of 45
FA4351055.2.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA43510
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA43422-1MS C0122016.D 1 05/01/17 EP n/a n/a VC4830
FA43422-1MSD C0122017.D 1 05/01/17 EP n/a n/a VC4830
FA43422-1 a C0122015.D 1 05/01/17 EP n/a n/a VC4830
The QC reported here applies to the following samples:Method: SW846 8260B
FA43510-1, FA43510-2
FA43422-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
67-64-1 Acetone 17.6 J 329 299 85 330 270 76 10 61-152/27
71-43-2 Benzene ND 65.8 63.8 97 66 61.5 93 4 76-126/26
75-27-4 Bromodichloromethane ND 65.8 60.4 92 66 63.1 96 4 74-130/25
75-25-2 Bromoform ND 65.8 64.2 98 66 64.8 98 1 76-127/26
78-93-3 2-Butanone (MEK)ND 329 288 87 330 313 95 8 75-137/25
104-51-8 n-Butylbenzene ND 65.8 66.4 101 66 60.8 92 9 71-128/35
75-15-0 Carbon Disulfide ND 65.8 59.5 90 66 49.4 75 19 72-122/29
56-23-5 Carbon Tetrachloride ND 65.8 59.0 90 66 51.4 78 14 78-133/29
108-90-7 Chlorobenzene ND 65.8 63.7 97 66 63.0 95 1 81-129/29
75-00-3 Chloroethane ND 65.8 53.3 81 66 46.5 70 14 68-133/29
67-66-3 Chloroform ND 65.8 62.9 96 66 56.4 85 11 72-123/26
110-82-7 Cyclohexane ND 65.8 52.4 80 66 44.7 68*16 73-126/32
124-48-1 Dibromochloromethane ND 65.8 63.8 97 66 66.0 100 3 76-127/27
96-12-8 1,2-Dibromo-3-chloropropane ND 65.8 63.7 97 66 56.5 86 12 70-137/29
106-93-4 1,2-Dibromoethane ND 65.8 60.3 92 66 67.0 102 11 77-126/26
75-71-8 Dichlorodifluoromethane ND 65.8 57.7 88 66 45.7 69 23 68-168/29
95-50-1 1,2-Dichlorobenzene ND 65.8 65.6 100 66 60.3 91 8 80-129/32
541-73-1 1,3-Dichlorobenzene ND 65.8 65.9 100 66 64.4 98 2 81-129/33
106-46-7 1,4-Dichlorobenzene ND 65.8 65.3 99 66 64.1 97 2 76-130/32
75-34-3 1,1-Dichloroethane ND 65.8 64.0 97 66 55.9 85 14 73-125/27
107-06-2 1,2-Dichloroethane ND 65.8 64.0 97 66 64.2 97 0 74-128/23
75-35-4 1,1-Dichloroethylene ND 65.8 60.3 92 66 50.3 76*18 81-136/28
156-59-2 cis-1,2-Dichloroethylene ND 65.8 64.7 98 66 56.2 85 14 74-126/26
156-60-5 trans-1,2-Dichloroethylene ND 65.8 64.1 97 66 53.8 82 17 70-127/27
78-87-5 1,2-Dichloropropane ND 65.8 60.8 92 66 61.9 94 2 74-125/25
10061-01-5 cis-1,3-Dichloropropene ND 65.8 55.9 85 66 67.1 102 18 80-123/26
10061-02-6 trans-1,3-Dichloropropene ND 65.8 59.8 91 66 70.9 107 17 75-131/28
100-41-4 Ethylbenzene ND 65.8 66.3 101 66 61.4 93 8 77-123/31
591-78-6 2-Hexanone ND 329 225 68*330 237 72 5 72-133/26
98-82-8 Isopropylbenzene ND 65.8 66.6 101 66 57.1 87 15 80-136/32
79-20-9 Methyl Acetate ND 329 312 95 330 303 92 3 67-137/30
74-83-9 Methyl Bromide ND 65.8 61.6 94 66 50.3 76 20 65-139/31
74-87-3 Methyl Chloride ND 65.8 61.5 93 66 50.7 77 19 71-144/27
108-87-2 Methylcyclohexane ND 65.8 51.2 78 66 44.3 67*14 75-128/31
75-09-2 Methylene Chloride 6.3 JB 65.8 66.6 92 66 54.6 73*20 74-137/28
108-10-1 4-Methyl-2-pentanone (MIBK)ND 329 324 98 330 299 91 8 76-132/26
* = Outside of Control Limits.
28 of 45
FA4351055.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA43510
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA43422-1MS C0122016.D 1 05/01/17 EP n/a n/a VC4830
FA43422-1MSD C0122017.D 1 05/01/17 EP n/a n/a VC4830
FA43422-1 a C0122015.D 1 05/01/17 EP n/a n/a VC4830
The QC reported here applies to the following samples:Method: SW846 8260B
FA43510-1, FA43510-2
FA43422-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
1634-04-4 Methyl Tert Butyl Ether ND 65.8 67.6 103 66 57.2 87 17 77-120/24
91-20-3 Naphthalene ND 65.8 72.1 110 66 55.0 83 27 79-129/33
103-65-1 n-Propylbenzene ND 65.8 62.7 95 66 58.6 89 7 80-135/33
100-42-5 Styrene ND 65.8 66.7 101 66 66.7 101 0 78-125/30
79-34-5 1,1,2,2-Tetrachloroethane ND 65.8 60.4 92 66 59.7 90 1 71-126/30
127-18-4 Tetrachloroethylene ND 65.8 72.9 111 66 71.9 109 1 79-130/31
108-88-3 Toluene ND 65.8 66.1 100 66 61.8 94 7 76-124/30
120-82-1 1,2,4-Trichlorobenzene ND 65.8 72.9 111 66 54.4 82 29 78-130/34
71-55-6 1,1,1-Trichloroethane ND 65.8 58.8 89 66 50.7 77 15 70-129/27
79-00-5 1,1,2-Trichloroethane ND 65.8 61.7 94 66 64.9 98 5 74-124/28
79-01-6 Trichloroethylene ND 65.8 60.6 92 66 61.7 93 2 75-128/27
75-69-4 Trichlorofluoromethane ND 65.8 56.3 86 66 47.4 72*17 73-145/31
95-63-6 1,2,4-Trimethylbenzene ND 65.8 67.8 103 66 62.4 95 8 74-123/34
108-67-8 1,3,5-Trimethylbenzene ND 65.8 65.4 99 66 60.6 92 8 73-122/33
75-01-4 Vinyl Chloride ND 65.8 59.2 90 66 48.3 73*20 76-141/27
1330-20-7 Xylene (total)ND 198 197 100 198 178 90 10 80-129/30
CAS No.Surrogate Recoveries MS MSD FA43422-1 Limits
1868-53-7 Dibromofluoromethane 105%95%93%75-124%
17060-07-0 1,2-Dichloroethane-D4 97%98%105%72-135%
2037-26-5 Toluene-D8 105%98%94%75-126%
460-00-4 4-Bromofluorobenzene 96%104%115%71-133%
(a) Sample was prepared from a bulk container.
* = Outside of Control Limits.
29 of 45
FA4351055.3.1
SGS Accutest
GC/MS Semi-volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Southeast
Section 6
30 of 45
FA435106
Method Blank Summary Page 1 of 2
Job Number:FA43510
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP64869-MB X053786.D 1 05/04/17 NG 05/02/17 OP64869 SX2276
The QC reported here applies to the following samples:Method: SW846 8270D
FA43510-1, FA43510-2
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 830 170 ug/kg
59-50-7 4-Chloro-3-methyl Phenol ND 170 19 ug/kg
95-57-8 2-Chlorophenol ND 170 20 ug/kg
120-83-2 2,4-Dichlorophenol ND 170 19 ug/kg
105-67-9 2,4-Dimethylphenol ND 170 44 ug/kg
51-28-5 2,4-Dinitrophenol ND 830 170 ug/kg
534-52-1 4,6-Dinitro-o-cresol ND 330 67 ug/kg
95-48-7 2-Methylphenol ND 170 20 ug/kg
3&4-Methylphenol ND 170 27 ug/kg
88-75-5 2-Nitrophenol ND 170 18 ug/kg
100-02-7 4-Nitrophenol ND 830 170 ug/kg
87-86-5 Pentachlorophenol ND 830 170 ug/kg
108-95-2 Phenol ND 170 17 ug/kg
88-06-2 2,4,6-Trichlorophenol ND 170 19 ug/kg
83-32-9 Acenaphthene ND 170 18 ug/kg
208-96-8 Acenaphthylene ND 170 17 ug/kg
120-12-7 Anthracene ND 170 19 ug/kg
56-55-3 Benzo(a)anthracene ND 170 17 ug/kg
50-32-8 Benzo(a)pyrene ND 170 20 ug/kg
205-99-2 Benzo(b)fluoranthene ND 170 18 ug/kg
191-24-2 Benzo(g,h,i)perylene ND 170 17 ug/kg
207-08-9 Benzo(k)fluoranthene ND 170 22 ug/kg
101-55-3 4-Bromophenyl phenyl ether ND 170 17 ug/kg
85-68-7 Butyl benzyl phthalate ND 170 33 ug/kg
106-47-8 4-Chloroaniline ND 170 42 ug/kg
111-91-1 bis(2-Chloroethoxy)methane ND 170 17 ug/kg
111-44-4 bis(2-Chloroethyl)ether ND 170 19 ug/kg
108-60-1 bis(2-Chloroisopropyl)ether ND 170 21 ug/kg
91-58-7 2-Chloronaphthalene ND 170 17 ug/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 170 17 ug/kg
218-01-9 Chrysene ND 170 17 ug/kg
53-70-3 Dibenzo(a,h)anthracene ND 170 21 ug/kg
132-64-9 Dibenzofuran ND 170 17 ug/kg
91-94-1 3,3'-Dichlorobenzidine ND 170 40 ug/kg
84-66-2 Diethyl Phthalate ND 330 33 ug/kg
131-11-3 Dimethyl Phthalate ND 170 33 ug/kg
31 of 45
FA4351066.1.1
Method Blank Summary Page 2 of 2
Job Number:FA43510
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP64869-MB X053786.D 1 05/04/17 NG 05/02/17 OP64869 SX2276
The QC reported here applies to the following samples:Method: SW846 8270D
FA43510-1, FA43510-2
CAS No.Compound Result RL MDL Units Q
117-84-0 Di-n-octyl Phthalate ND 170 33 ug/kg
84-74-2 Di-n-butyl Phthalate ND 330 67 ug/kg
121-14-2 2,4-Dinitrotoluene ND 170 17 ug/kg
606-20-2 2,6-Dinitrotoluene ND 170 21 ug/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 330 33 ug/kg
206-44-0 Fluoranthene ND 170 17 ug/kg
86-73-7 Fluorene ND 170 18 ug/kg
118-74-1 Hexachlorobenzene ND 170 17 ug/kg
87-68-3 Hexachlorobutadiene ND 170 17 ug/kg
77-47-4 Hexachlorocyclopentadiene ND 170 33 ug/kg
67-72-1 Hexachloroethane ND 170 20 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 170 20 ug/kg
78-59-1 Isophorone ND 170 17 ug/kg
90-12-0 1-Methylnaphthalene ND 170 17 ug/kg
91-57-6 2-Methylnaphthalene ND 170 17 ug/kg
91-20-3 Naphthalene ND 170 17 ug/kg
98-95-3 Nitrobenzene ND 170 17 ug/kg
621-64-7 N-Nitrosodi-n-propylamine ND 170 17 ug/kg
86-30-6 N-Nitrosodiphenylamine ND 170 18 ug/kg
85-01-8 Phenanthrene ND 170 17 ug/kg
129-00-0 Pyrene ND 170 19 ug/kg
CAS No.Surrogate Recoveries Limits
367-12-4 2-Fluorophenol 76%40-102%
4165-62-2 Phenol-d5 78%41-100%
118-79-6 2,4,6-Tribromophenol 92%42-108%
4165-60-0 Nitrobenzene-d5 82%40-105%
321-60-8 2-Fluorobiphenyl 81%43-107%
1718-51-0 Terphenyl-d14 86%45-119%
32 of 45
FA4351066.1.1
Blank Spike Summary Page 1 of 2
Job Number:FA43510
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP64869-BS X053785.D 1 05/04/17 NG 05/02/17 OP64869 SX2276
The QC reported here applies to the following samples:Method: SW846 8270D
FA43510-1, FA43510-2
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
65-85-0 Benzoic Acid 3330 3090 93 36-118
59-50-7 4-Chloro-3-methyl Phenol 1670 1460 88 52-108
95-57-8 2-Chlorophenol 1670 1400 84 48-104
120-83-2 2,4-Dichlorophenol 1670 1470 88 51-105
105-67-9 2,4-Dimethylphenol 1670 1380 83 43-96
51-28-5 2,4-Dinitrophenol 3330 2710 81 40-119
534-52-1 4,6-Dinitro-o-cresol 3330 3370 101 64-121
95-48-7 2-Methylphenol 1670 1320 79 46-107
3&4-Methylphenol 3330 2710 81 44-111
88-75-5 2-Nitrophenol 1670 1450 87 49-104
100-02-7 4-Nitrophenol 3330 2720 82 56-116
87-86-5 Pentachlorophenol 3330 3040 91 61-114
108-95-2 Phenol 1670 1400 84 45-110
88-06-2 2,4,6-Trichlorophenol 1670 1580 95 56-109
83-32-9 Acenaphthene 1670 1410 85 56-109
208-96-8 Acenaphthylene 1670 1480 89 56-106
120-12-7 Anthracene 1670 1410 85 61-110
56-55-3 Benzo(a)anthracene 1670 1520 91 66-111
50-32-8 Benzo(a)pyrene 1670 1550 93 59-104
205-99-2 Benzo(b)fluoranthene 1670 1550 93 67-113
191-24-2 Benzo(g,h,i)perylene 1670 1560 94 67-113
207-08-9 Benzo(k)fluoranthene 1670 1540 92 67-114
101-55-3 4-Bromophenyl phenyl ether 1670 1570 94 62-110
85-68-7 Butyl benzyl phthalate 1670 1500 90 65-113
106-47-8 4-Chloroaniline 1670 1460 88 30-115
111-91-1 bis(2-Chloroethoxy)methane 1670 1370 82 48-105
111-44-4 bis(2-Chloroethyl)ether 1670 1350 81 46-103
108-60-1 bis(2-Chloroisopropyl)ether 1670 1280 77 40-110
91-58-7 2-Chloronaphthalene 1670 1410 85 53-106
7005-72-3 4-Chlorophenyl phenyl ether 1670 1430 86 58-106
218-01-9 Chrysene 1670 1450 87 65-112
53-70-3 Dibenzo(a,h)anthracene 1670 1720 103 68-115
132-64-9 Dibenzofuran 1670 1430 86 57-108
91-94-1 3,3'-Dichlorobenzidine 1670 1600 96 36-114
84-66-2 Diethyl Phthalate 1670 1360 82 61-109
131-11-3 Dimethyl Phthalate 1670 1420 85 59-108
* = Outside of Control Limits.
33 of 45
FA4351066.2.1
Blank Spike Summary Page 2 of 2
Job Number:FA43510
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP64869-BS X053785.D 1 05/04/17 NG 05/02/17 OP64869 SX2276
The QC reported here applies to the following samples:Method: SW846 8270D
FA43510-1, FA43510-2
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
117-84-0 Di-n-octyl Phthalate 1670 1630 98 64-119
84-74-2 Di-n-butyl Phthalate 1670 1490 89 63-108
121-14-2 2,4-Dinitrotoluene 1670 1530 92 59-109
606-20-2 2,6-Dinitrotoluene 1670 1480 89 61-107
117-81-7 bis(2-Ethylhexyl)phthalate 1670 1570 94 64-115
206-44-0 Fluoranthene 1670 1440 86 60-108
86-73-7 Fluorene 1670 1470 88 58-109
118-74-1 Hexachlorobenzene 1670 1490 89 59-111
87-68-3 Hexachlorobutadiene 1670 1360 82 41-108
77-47-4 Hexachlorocyclopentadiene 1670 1510 91 49-110
67-72-1 Hexachloroethane 1670 1230 74 40-105
193-39-5 Indeno(1,2,3-cd)pyrene 1670 1740 104 66-116
78-59-1 Isophorone 1670 1420 85 42-89
90-12-0 1-Methylnaphthalene 1670 1460 88 49-106
91-57-6 2-Methylnaphthalene 1670 1390 83 47-106
91-20-3 Naphthalene 1670 1380 83 44-104
98-95-3 Nitrobenzene 1670 1370 82 43-108
621-64-7 N-Nitrosodi-n-propylamine 1670 1360 82 48-108
86-30-6 N-Nitrosodiphenylamine 1670 1540 92 62-110
85-01-8 Phenanthrene 1670 1500 90 63-111
129-00-0 Pyrene 1670 1480 89 65-115
CAS No.Surrogate Recoveries BSP Limits
367-12-4 2-Fluorophenol 77%40-102%
4165-62-2 Phenol-d5 81%41-100%
118-79-6 2,4,6-Tribromophenol 93%42-108%
4165-60-0 Nitrobenzene-d5 83%40-105%
321-60-8 2-Fluorobiphenyl 85%43-107%
1718-51-0 Terphenyl-d14 92%45-119%
* = Outside of Control Limits.
34 of 45
FA4351066.2.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA43510
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP64869-MS X053790.D 1 05/04/17 NG 05/02/17 OP64869 SX2276
OP64869-MSD X053791.D 1 05/04/17 NG 05/02/17 OP64869 SX2276
FA43456-2 X053789.D 1 05/04/17 NG 05/02/17 OP64869 SX2276
The QC reported here applies to the following samples:Method: SW846 8270D
FA43510-1, FA43510-2
FA43456-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
65-85-0 Benzoic Acid 960 U 3800 232 6*3790 300 8*26 36-118/41
59-50-7 4-Chloro-3-methyl Phenol 190 U 1900 1520 80 1890 1310 69 15 52-108/21
95-57-8 2-Chlorophenol 190 U 1900 1410 74 1890 1200 63 16 48-104/26
120-83-2 2,4-Dichlorophenol 190 U 1900 1530 81 1890 1310 69 15 51-105/27
105-67-9 2,4-Dimethylphenol 190 U 1900 1440 76 1890 1240 66 15 43-96/23
51-28-5 2,4-Dinitrophenol 960 U 3800 405 11*3790 424 11*5 40-119/32
534-52-1 4,6-Dinitro-o-cresol 380 U 3800 1570 41*3790 1480 39*6 64-121/29
95-48-7 2-Methylphenol 190 U 1900 1410 74 1890 1200 63 16 46-107/24
3&4-Methylphenol 190 U 3800 2820 74 3790 2440 64 14 44-111/24
88-75-5 2-Nitrophenol 190 U 1900 1490 78 1890 1310 69 13 49-104/27
100-02-7 4-Nitrophenol 960 U 3800 2570 68 3790 2350 62 9 56-116/23
87-86-5 Pentachlorophenol 960 U 3800 1730 46*3790 1810 48*5 61-114/23
108-95-2 Phenol 190 U 1900 1410 74 1890 1230 65 14 45-110/24
88-06-2 2,4,6-Trichlorophenol 190 U 1900 1610 85 1890 1370 72 16 56-109/25
83-32-9 Acenaphthene 190 U 1900 1510 80 1890 1260 67 18 56-109/23
208-96-8 Acenaphthylene 34.3 I 1900 1620 84 1890 1340 69 19 56-106/23
120-12-7 Anthracene 61.6 I 1900 1510 76 1890 1300 65 15 61-110/21
56-55-3 Benzo(a)anthracene 185 I 1900 1770 83 1890 1470 68 19 66-111/23
50-32-8 Benzo(a)pyrene 160 I 1900 1760 84 1890 1450 68 19 59-104/23
205-99-2 Benzo(b)fluoranthene 168 I 1900 1900 91 1890 1610 76 17 67-113/24
191-24-2 Benzo(g,h,i)perylene 95.4 I 1900 1720 86 1890 1460 72 16 67-113/21
207-08-9 Benzo(k)fluoranthene 120 I 1900 1620 79 1890 1370 66*17 67-114/22
101-55-3 4-Bromophenyl phenyl ether 190 U 1900 1660 87 1890 1440 76 14 62-110/21
85-68-7 Butyl benzyl phthalate 190 U 1900 1680 88 1890 1610 85 4 65-113/20
106-47-8 4-Chloroaniline 190 U 1900 1540 81 1890 1360 72 12 30-115/30
111-91-1 bis(2-Chloroethoxy)methane 190 U 1900 1430 75 1890 1220 64 16 48-105/24
111-44-4 bis(2-Chloroethyl)ether 190 U 1900 1350 71 1890 1160 61 15 46-103/27
108-60-1 bis(2-Chloroisopropyl)ether 190 U 1900 1380 73 1890 1180 62 16 40-110/25
91-58-7 2-Chloronaphthalene 190 U 1900 1520 80 1890 1290 68 16 53-106/23
7005-72-3 4-Chlorophenyl phenyl ether 190 U 1900 1510 80 1890 1280 68 16 58-106/21
218-01-9 Chrysene 190 1900 1680 78 1890 1360 62*21 65-112/25
53-70-3 Dibenzo(a,h)anthracene 34.3 I 1900 1830 95 1890 1610 83 13 68-115/23
132-64-9 Dibenzofuran 190 U 1900 1530 81 1890 1320 70 15 57-108/22
91-94-1 3,3'-Dichlorobenzidine 190 U 1900 1680 88 1890 1480 78 13 36-114/28
84-66-2 Diethyl Phthalate 380 U 1900 1520 80 1890 1290 68 16 61-109/20
131-11-3 Dimethyl Phthalate 190 U 1900 1510 80 1890 1270 67 17 59-108/20
* = Outside of Control Limits.
35 of 45
FA4351066.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA43510
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP64869-MS X053790.D 1 05/04/17 NG 05/02/17 OP64869 SX2276
OP64869-MSD X053791.D 1 05/04/17 NG 05/02/17 OP64869 SX2276
FA43456-2 X053789.D 1 05/04/17 NG 05/02/17 OP64869 SX2276
The QC reported here applies to the following samples:Method: SW846 8270D
FA43510-1, FA43510-2
FA43456-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
117-84-0 Di-n-octyl Phthalate 190 U 1900 1870 98 1890 1780 94 5 64-119/21
84-74-2 Di-n-butyl Phthalate 380 U 1900 1570 83 1890 1390 73 12 63-108/19
121-14-2 2,4-Dinitrotoluene 190 U 1900 1560 82 1890 1340 71 15 59-109/20
606-20-2 2,6-Dinitrotoluene 190 U 1900 1540 81 1890 1340 71 14 61-107/22
117-81-7 bis(2-Ethylhexyl)phthalate 82.5 I 1900 1790 90 1890 1670 84 7 64-115/23
206-44-0 Fluoranthene 321 1900 1670 71 1890 1290 51*26*60-108/25
86-73-7 Fluorene 190 U 1900 1550 82 1890 1300 69 18 58-109/21
118-74-1 Hexachlorobenzene 190 U 1900 1550 82 1890 1330 70 15 59-111/21
87-68-3 Hexachlorobutadiene 190 U 1900 1410 74 1890 1190 63 17 41-108/27
77-47-4 Hexachlorocyclopentadiene 190 U 1900 1240 65 1890 963 51 25 49-110/31
67-72-1 Hexachloroethane 190 U 1900 1240 65 1890 1050 55 17 40-105/32
193-39-5 Indeno(1,2,3-cd)pyrene 122 I 1900 1900 94 1890 1640 80 15 66-116/22
78-59-1 Isophorone 190 U 1900 1450 76 1890 1220 64 17 42-89/22
90-12-0 1-Methylnaphthalene 190 U 1900 1520 80 1890 1270 67 18 49-106/26
91-57-6 2-Methylnaphthalene 190 U 1900 1400 74 1890 1240 66 12 47-106/27
91-20-3 Naphthalene 190 U 1900 1420 75 1890 1190 63 18 44-104/27
98-95-3 Nitrobenzene 190 U 1900 1400 74 1890 1190 63 16 43-108/25
621-64-7 N-Nitrosodi-n-propylamine 190 U 1900 1400 74 1890 1230 65 13 48-108/27
86-30-6 N-Nitrosodiphenylamine 190 U 1900 1670 88 1890 1450 77 14 62-110/21
85-01-8 Phenanthrene 214 1900 1690 78 1890 1360 61*22 63-111/22
129-00-0 Pyrene 251 1900 1880 86 1890 1650 74 13 65-115/25
CAS No.Surrogate Recoveries MS MSD FA43456-2 Limits
367-12-4 2-Fluorophenol 68%61%66%40-102%
4165-62-2 Phenol-d5 72%63%67%41-100%
118-79-6 2,4,6-Tribromophenol 83%74%81%42-108%
4165-60-0 Nitrobenzene-d5 74%65%69%40-105%
321-60-8 2-Fluorobiphenyl 79%69%73%43-107%
1718-51-0 Terphenyl-d14 88%89%78%45-119%
* = Outside of Control Limits.
36 of 45
FA4351066.3.1
SGS Accutest
GC Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Southeast
Section 7
37 of 45
FA435107
Method Blank Summary Page 1 of 1
Job Number:FA43510
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
GUU1064-MB UU020253.D 1 05/05/17 AJC n/a n/a GUU1064
The QC reported here applies to the following samples:Method: MADEP VPH REV 1.1
FA43510-1, FA43510-2
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 51 51 ug/kg
100-41-4 Ethylbenzene ND 100 51 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 100 51 ug/kg
91-20-3 Naphthalene ND 260 150 ug/kg
108-88-3 Toluene ND 100 51 ug/kg
m,p-Xylene ND 200 100 ug/kg
95-47-6 o-Xylene ND 100 51 ug/kg
C5- C8 Aliphatics (Unadj.)ND 5100 1800 ug/kg
C9- C12 Aliphatics (Unadj.)ND 5100 1800 ug/kg
C9- C10 Aromatics (Unadj.)ND 5100 1800 ug/kg
CAS No.Surrogate Recoveries Limits
460-00-4 BFB 97%70-130%
460-00-4 BFB 89%70-130%
38 of 45
FA4351077.1.1
Blank Spike/Blank Spike Duplicate Summary Page 1 of 1
Job Number:FA43510
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
GUU1064-BS UU020252.D 1 05/05/17 AJC n/a n/a GUU1064
GUU1064-BSD UU020251.D 1 05/05/17 AJC n/a n/a GUU1064
The QC reported here applies to the following samples:Method: MADEP VPH REV 1.1
FA43510-1, FA43510-2
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/kg ug/kg %ug/kg %RPD Rec/RPD
71-43-2 Benzene 4160 4200 101 4230 102 1 70-130/25
100-41-4 Ethylbenzene 4160 4170 100 4200 101 1 70-130/25
1634-04-4 Methyl Tert Butyl Ether 4160 4470 107 4390 105 2 70-130/25
91-20-3 Naphthalene 4160 3270 79 3250 78 1 70-130/25
108-88-3 Toluene 4160 4250 102 4270 103 0 70-130/25
m,p-Xylene 8320 8390 101 8460 102 1 70-130/25
95-47-6 o-Xylene 4160 4080 98 4100 99 0 70-130/25
C5- C8 Aliphatics (Unadj.)12500 16100 129 16600 133*3 70-130/25
C9- C12 Aliphatics (Unadj.)8320 8790 106 8850 106 1 70-130/25
C9- C10 Aromatics (Unadj.)4160 3900 94 3670 88 6 70-130/25
CAS No.Surrogate Recoveries BSP BSD Limits
460-00-4 BFB 87%90%70-130%
460-00-4 BFB 81%84%70-130%
* = Outside of Control Limits.
39 of 45
FA4351077.2.1
Duplicate Summary Page 1 of 1
Job Number:FA43510
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA43638-1DUP UU020255.D 1 05/05/17 AJC n/a n/a GUU1064
FA43638-1 UU020254.D 1 05/05/17 AJC n/a n/a GUU1064
The QC reported here applies to the following samples:Method: MADEP VPH REV 1.1
FA43510-1, FA43510-2
FA43638-1 DUP
CAS No.Compound ug/kg Q ug/kg Q RPD Limits
71-43-2 Benzene ND ND nc 50
100-41-4 Ethylbenzene ND ND nc 50
1634-04-4 Methyl Tert Butyl Ether ND ND nc 50
91-20-3 Naphthalene ND ND nc 50
108-88-3 Toluene ND ND nc 50
m,p-Xylene ND ND nc 50
95-47-6 o-Xylene ND ND nc 50
C5- C8 Aliphatics (Unadj.)ND ND nc 50
C9- C12 Aliphatics (Unadj.)ND ND nc 50
C9- C10 Aromatics (Unadj.)ND ND nc 50
C5- C8 Aliphatics ND ND nc 50
C9- C12 Aliphatics ND ND nc 50
C9- C10 Aromatics ND ND nc 50
CAS No.Surrogate Recoveries DUP FA43638-1 Limits
460-00-4 BFB 101%105%70-130%
460-00-4 BFB 91%95%70-130%
* = Outside of Control Limits.
40 of 45
FA4351077.3.1
SGS Accutest
GC Semi-volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Southeast
Section 8
41 of 45
FA435108
Method Blank Summary Page 1 of 1
Job Number:FA43510
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP64856-MB NN018625.D 1 05/06/17 MG 05/01/17 OP64856 GNN933
The QC reported here applies to the following samples:Method: MADEP EPH REV 1.1
FA43510-1, FA43510-2
CAS No.Compound Result RL MDL Units Q
83-32-9 Acenaphthene ND 200 100 ug/kg
208-96-8 Acenaphthylene ND 200 100 ug/kg
120-12-7 Anthracene ND 200 100 ug/kg
56-55-3 Benzo(a)anthracene ND 200 100 ug/kg
50-32-8 Benzo(a)pyrene ND 200 100 ug/kg
205-99-2 Benzo(b)fluoranthene ND 200 100 ug/kg
191-24-2 Benzo(g,h,i)perylene ND 200 100 ug/kg
207-08-9 Benzo(k)fluoranthene ND 200 100 ug/kg
218-01-9 Chrysene ND 200 100 ug/kg
53-70-3 Dibenzo(a,h)anthracene ND 200 100 ug/kg
206-44-0 Fluoranthene ND 200 100 ug/kg
86-73-7 Fluorene ND 200 100 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 200 100 ug/kg
91-57-6 2-Methylnaphthalene ND 200 100 ug/kg
91-20-3 Naphthalene ND 200 100 ug/kg
85-01-8 Phenanthrene ND 200 100 ug/kg
129-00-0 Pyrene ND 200 100 ug/kg
C11-C22 Aromatics (Unadj.)ND 10000 4000 ug/kg
C11-C22 Aromatics ND 10000 4000 ug/kg
C9-C18 Aliphatics ND 10000 2500 ug/kg
C19-C36 Aliphatics ND 10000 2500 ug/kg
CAS No.Surrogate Recoveries Limits
3386-33-2 1-Chlorooctadecane 75%40-140%
580-13-2 2-Bromonaphthalene 96%40-140%
84-15-1 o-Terphenyl 73%40-140%
321-60-8 2-Fluorobiphenyl 94%40-140%
42 of 45
FA4351088.1.1
Blank Spike/Blank Spike Duplicate Summary Page 1 of 2
Job Number:FA43510
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP64856-BS NN018626.D 1 05/06/17 MG 05/01/17 OP64856 GNN933
OP64856-BSD NN018627.D 1 05/06/17 MG 05/01/17 OP64856 GNN933
The QC reported here applies to the following samples:Method: MADEP EPH REV 1.1
FA43510-1, FA43510-2
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/kg ug/kg %ug/kg %RPD Rec/RPD
83-32-9 Acenaphthene 5000 3650 73 3090 62 17 40-140/30
208-96-8 Acenaphthylene 5000 3540 71 2990 60 17 40-140/30
120-12-7 Anthracene 5000 4020 80 3690 74 9 40-140/30
56-55-3 Benzo(a)anthracene 5000 4020 80 3790 76 6 40-140/30
50-32-8 Benzo(a)pyrene 5000 3890 78 3610 72 7 40-140/30
205-99-2 Benzo(b)fluoranthene 5000 4000 80 3740 75 7 40-140/30
191-24-2 Benzo(g,h,i)perylene 5000 3860 77 3610 72 7 40-140/30
207-08-9 Benzo(k)fluoranthene 5000 4070 81 3780 76 7 40-140/30
218-01-9 Chrysene 5000 4130 83 3880 78 6 40-140/30
53-70-3 Dibenzo(a,h)anthracene 5000 4040 81 3760 75 7 40-140/30
206-44-0 Fluoranthene 5000 4020 80 3820 76 5 40-140/30
86-73-7 Fluorene 5000 3770 75 3250 65 15 40-140/30
193-39-5 Indeno(1,2,3-cd)pyrene 5000 3920 78 3640 73 7 40-140/30
91-57-6 2-Methylnaphthalene 5000 3200 64 2670 53 18 40-140/30
91-20-3 Naphthalene 5000 2990 60 2470 49 19 40-140/30
85-01-8 Phenanthrene 5000 3900 78 3540 71 10 40-140/30
129-00-0 Pyrene 5000 4110 82 3910 78 5 40-140/30
C11-C22 Aromatics (Unadj.)85000 58800 69 53700 63 9 40-140/30
C11-C22 Aromatics 85000 ND 0*ND 0*nc 50-150/30 a
C9-C18 Aliphatics 30000 22200 74 22100 74 0 40-140/30
C19-C36 Aliphatics 40000 38700 97 37200 93 4 40-140/30
CAS No.Surrogate Recoveries BSP BSD Limits
3386-33-2 1-Chlorooctadecane 83%78%40-140%
580-13-2 2-Bromonaphthalene 106%78%40-140%
84-15-1 o-Terphenyl 77%71%40-140%
321-60-8 2-Fluorobiphenyl 101%74%40-140%
Sample Compound Col #1 Col #2 Breakthrough Limit
OP64856-BS 2-Methylnaphthalene 3200 ND 0.0%5.0
OP64856-BS Naphthalene 2990 ND 0.0%5.0
OP64856-BSD 2-Methylnaphthalene 2670 ND 0.0%5.0
OP64856-BSD Naphthalene 2470 ND 0.0%5.0
* = Outside of Control Limits.
43 of 45
FA4351088.2.1
Blank Spike/Blank Spike Duplicate Summary Page 2 of 2
Job Number:FA43510
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP64856-BS NN018626.D 1 05/06/17 MG 05/01/17 OP64856 GNN933
OP64856-BSD NN018627.D 1 05/06/17 MG 05/01/17 OP64856 GNN933
The QC reported here applies to the following samples:Method: MADEP EPH REV 1.1
FA43510-1, FA43510-2
(a) Advisory control limits.
* = Outside of Control Limits.
44 of 45
FA4351088.2.1
Duplicate Summary Page 1 of 1
Job Number:FA43510
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP64856-DUP a NN018650.D 50 05/08/17 MG 05/01/17 OP64856 GNN934
FA43510-1 a NN018649.D 50 05/08/17 MG 05/01/17 OP64856 GNN934
The QC reported here applies to the following samples:Method: MADEP EPH REV 1.1
FA43510-1, FA43510-2
FA43510-1 DUP
CAS No.Compound ug/kg Q ug/kg Q RPD Limits
83-32-9 Acenaphthene ND ND nc 30 b
208-96-8 Acenaphthylene ND ND nc 30 b
120-12-7 Anthracene ND ND nc 30 b
56-55-3 Benzo(a)anthracene ND ND nc 30 b
50-32-8 Benzo(a)pyrene ND ND nc 30 b
205-99-2 Benzo(b)fluoranthene ND ND nc 30 b
191-24-2 Benzo(g,h,i)perylene ND ND nc 30 b
207-08-9 Benzo(k)fluoranthene ND ND nc 30 b
218-01-9 Chrysene ND ND nc 30 b
53-70-3 Dibenzo(a,h)anthracene ND ND nc 30 b
206-44-0 Fluoranthene ND ND nc 30 b
86-73-7 Fluorene ND ND nc 30 b
193-39-5 Indeno(1,2,3-cd)pyrene ND ND nc 30 b
91-57-6 2-Methylnaphthalene 40900 53400 27 30 b
91-20-3 Naphthalene ND 6900 J 200*30 b
85-01-8 Phenanthrene 15700 20000 24 30 b
129-00-0 Pyrene ND 6120 J 200*30 b
C11-C22 Aromatics (Unadj.)1750000 2140000 20 30 b
C11-C22 Aromatics 1670000 2040000 20 30 b
C9-C18 Aliphatics 3390000 4450000 27 30 b
C19-C36 Aliphatics 645000 896000 33*30 b
CAS No.Surrogate Recoveries DUP FA43510-1 Limits
3386-33-2 1-Chlorooctadecane 0%* c 0%* c 40-140%
580-13-2 2-Bromonaphthalene 0%* c 0%* c 40-140%
84-15-1 o-Terphenyl 0%* c 0%* c 40-140%
321-60-8 2-Fluorobiphenyl 0%* c 0%* c 40-140%
(a) Dilution required due to matrix interference.
(b) Advisory control limits.
(c) Outside control limits due to dilution.
* = Outside of Control Limits.
45 of 45
FA4351088.3.1