WS-9507_44719_CA_IAR_20160829

08/10/16
Technical Report for
GRI (Geological Resources Inc.)
Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
4236
SGS Accutest Job Number: FA35839
Sampling Date: 08/01/16
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
[e-mail]; [e-mail];
[e-mail]; [e-mail]
ATTN: Corey Buchanan
Total number of pages in report:
Certifications: FL (E83510), LA (03051), KS (E-10327), IA (366), IL (200063), NC (573), NJ (FL002), SC (96038001)
DoD ELAP (L-A-B L2229), CA (2937), TX (T104704404), PA (68-03573), VA (460177),
AK, AR, GA, KY, MA, NV, OK, UT, WA
This report shall not be reproduced, except in its entirety, without the written approval of SGS Accutest.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone] • http://www.accutest.com
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Norm Farmer
Technical Director
Southeast 08/10/16
e-Hardcopy 2.0
Automated Report
35
SGS Accutest is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
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FA35839
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................5
3.1: FA35839-1: DI-1 (3') ....................................................................................................6
3.2: FA35839-2: SP-1 (0-200) .............................................................................................8
3.3: FA35839-3: UST-1-1 (10') ............................................................................................10
3.4: FA35839-4: UST-1-2 (10') ............................................................................................12
3.5: FA35839-5: SW-N (11') ................................................................................................14
3.6: FA35839-6: SW-E (11') ................................................................................................15
3.7: FA35839-7: SW-S (11') .................................................................................................16
3.8: FA35839-8: SW-W (11') ...............................................................................................17
3.9: FA35839-9: BOTTOM (13') .........................................................................................18
Section 4: Misc. Forms ............................................................................................................19
4.1: Chain of Custody ...........................................................................................................20
Section 5: GC Volatiles - QC Data Summaries .....................................................................24
5.1: Method Blank Summary ................................................................................................25
5.2: Blank Spike Summary ...................................................................................................27
5.3: Matrix Spike Summary ..................................................................................................29
5.4: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................30
5.5: Duplicate Summary .......................................................................................................31
Section 6: GC Semi-volatiles - QC Data Summaries ............................................................32
6.1: Method Blank Summary ................................................................................................33
6.2: Blank Spike Summary ...................................................................................................34
6.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................35 1234562 of 35
FA35839
SGS Accutest
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA35839
Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Project No: 4236
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA35839-1 08/01/16 10:01 CB 08/03/16 SO Soil DI-1 (3')
FA35839-2 08/01/16 10:37 CB 08/03/16 SO Soil SP-1 (0-200)
FA35839-3 08/01/16 12:37 CB 08/03/16 SO Soil UST-1-1 (10')
FA35839-4 08/01/16 12:41 CB 08/03/16 SO Soil UST-1-2 (10')
FA35839-5 08/01/16 12:50 CB 08/03/16 SO Soil SW-N (11')
FA35839-6 08/01/16 12:53 CB 08/03/16 SO Soil SW-E (11')
FA35839-7 08/01/16 12:59 CB 08/03/16 SO Soil SW-S (11')
FA35839-8 08/01/16 12:55 CB 08/03/16 SO Soil SW-W (11')
FA35839-9 08/01/16 13:01 CB 08/03/16 SO Soil BOTTOM (13')
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
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FA358391
Summary of Hits Page 1 of 1
Job Number:FA35839
Account:GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Collected:08/01/16
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA35839-1 DI-1 (3')
TPH-GRO (C6-C10)22.4 7.2 3.6 mg/kg SW846 8015C
TPH (C10-C28)1860 81 48 mg/kg SW846 8015C
FA35839-2 SP-1 (0-200)
TPH-GRO (C6-C10)73.2 9.3 4.7 mg/kg SW846 8015C
TPH (C10-C28)954 95 57 mg/kg SW846 8015C
FA35839-3 UST-1-1 (10')
TPH-GRO (C6-C10)164 18 8.9 mg/kg SW846 8015C
TPH (C10-C28)20000 940 560 mg/kg SW846 8015C
FA35839-4 UST-1-2 (10')
No hits reported in this sample.
FA35839-5 SW-N (11')
No hits reported in this sample.
FA35839-6 SW-E (11')
No hits reported in this sample.
FA35839-7 SW-S (11')
No hits reported in this sample.
FA35839-8 SW-W (11')
No hits reported in this sample.
FA35839-9 BOTTOM (13')
No hits reported in this sample.
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FA358392
SGS Accutest
Sample Results
Report of Analysis
Southeast
Section 3
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FA358393
SGS Accutest
Report of Analysis Page 1 of 1
Client Sample ID:DI-1 (3')
Lab Sample ID:FA35839-1 Date Sampled:08/01/16
Matrix:SO - Soil Date Received:08/03/16
Method:SW846 8015C Percent Solids:78.2
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 UV075123.D 1 08/03/16 AH n/a n/a GUV3995
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 5.48 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)22.4 7.2 3.6 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 83%56-149%
98-08-8 aaa-Trifluorotoluene 97%66-132%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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FA3583933.1
SGS Accutest
Report of Analysis Page 1 of 1
Client Sample ID:DI-1 (3')
Lab Sample ID:FA35839-1 Date Sampled:08/01/16
Matrix:SO - Soil Date Received:08/03/16
Method:SW846 8015C SW846 3546 Percent Solids:78.2
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 WR11729.D 10 08/09/16 SJL 08/04/16 OP61336 GWR447
Run #2
Initial Weight Final Volume
Run #1 19.8 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)1860 81 48 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 95%56-122%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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FA3583933.1
SGS Accutest
Report of Analysis Page 1 of 1
Client Sample ID:SP-1 (0-200)
Lab Sample ID:FA35839-2 Date Sampled:08/01/16
Matrix:SO - Soil Date Received:08/03/16
Method:SW846 8015C Percent Solids:65.9
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 UV075124.D 1 08/03/16 AH n/a n/a GUV3995
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 5.61 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)73.2 9.3 4.7 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 89%56-149%
98-08-8 aaa-Trifluorotoluene 97%66-132%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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FA3583933.2
SGS Accutest
Report of Analysis Page 1 of 1
Client Sample ID:SP-1 (0-200)
Lab Sample ID:FA35839-2 Date Sampled:08/01/16
Matrix:SO - Soil Date Received:08/03/16
Method:SW846 8015C SW846 3546 Percent Solids:65.9
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 WR11758.D 10 08/10/16 SJL 08/04/16 OP61336 GWR448
Run #2
Initial Weight Final Volume
Run #1 19.9 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)954 95 57 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 83%56-122%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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FA3583933.2
SGS Accutest
Report of Analysis Page 1 of 1
Client Sample ID:UST-1-1 (10')
Lab Sample ID:FA35839-3 Date Sampled:08/01/16
Matrix:SO - Soil Date Received:08/03/16
Method:SW846 8015C Percent Solids:67.1
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 UV075143.D 1 08/04/16 AH n/a n/a GUV3996
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 5.81 g 5.0 ml 50.0 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)164 18 8.9 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 84%56-149%
98-08-8 aaa-Trifluorotoluene 110%66-132%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 35
FA3583933.3
SGS Accutest
Report of Analysis Page 1 of 1
Client Sample ID:UST-1-1 (10')
Lab Sample ID:FA35839-3 Date Sampled:08/01/16
Matrix:SO - Soil Date Received:08/03/16
Method:SW846 8015C SW846 3546 Percent Solids:67.1
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 WR11759.D 100 08/10/16 SJL 08/04/16 OP61336 GWR448
Run #2
Initial Weight Final Volume
Run #1 19.9 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)20000 940 560 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 0% a 56-122%
(a) Outside control limits due to dilution.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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FA3583933.3
SGS Accutest
Report of Analysis Page 1 of 1
Client Sample ID:UST-1-2 (10')
Lab Sample ID:FA35839-4 Date Sampled:08/01/16
Matrix:SO - Soil Date Received:08/03/16
Method:SW846 8015C Percent Solids:57.8
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 UV075128.D 1 08/04/16 AH n/a n/a GUV3995
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 5.31 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 12 5.9 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 101%56-149%
98-08-8 aaa-Trifluorotoluene 98%66-132%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 35
FA3583933.4
SGS Accutest
Report of Analysis Page 1 of 1
Client Sample ID:UST-1-2 (10')
Lab Sample ID:FA35839-4 Date Sampled:08/01/16
Matrix:SO - Soil Date Received:08/03/16
Method:SW846 8015C SW846 3546 Percent Solids:57.8
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 WR11750.D 1 08/09/16 SJL 08/04/16 OP61336 GWR447
Run #2
Initial Weight Final Volume
Run #1 20.8 g 1.0 ml
Run #2
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)ND 10 6.2 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 87%56-122%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
13 of 35
FA3583933.4
SGS Accutest
Report of Analysis Page 1 of 1
Client Sample ID:SW-N (11')
Lab Sample ID:FA35839-5 Date Sampled:08/01/16
Matrix:SO - Soil Date Received:08/03/16
Percent Solids:85.9
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Solids, Percent 85.9 %1 08/03/16 16:47 ZC SM19 2540G
RL = Reporting Limit
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FA3583933.5
SGS Accutest
Report of Analysis Page 1 of 1
Client Sample ID:SW-E (11')
Lab Sample ID:FA35839-6 Date Sampled:08/01/16
Matrix:SO - Soil Date Received:08/03/16
Percent Solids:68.3
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Solids, Percent 68.3 %1 08/03/16 16:47 ZC SM19 2540G
RL = Reporting Limit
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FA3583933.6
SGS Accutest
Report of Analysis Page 1 of 1
Client Sample ID:SW-S (11')
Lab Sample ID:FA35839-7 Date Sampled:08/01/16
Matrix:SO - Soil Date Received:08/03/16
Percent Solids:63.0
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Solids, Percent 63 %1 08/03/16 16:47 ZC SM19 2540G
RL = Reporting Limit
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FA3583933.7
SGS Accutest
Report of Analysis Page 1 of 1
Client Sample ID:SW-W (11')
Lab Sample ID:FA35839-8 Date Sampled:08/01/16
Matrix:SO - Soil Date Received:08/03/16
Percent Solids:69.6
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Solids, Percent 69.6 %1 08/03/16 16:47 ZC SM19 2540G
RL = Reporting Limit
17 of 35
FA3583933.8
SGS Accutest
Report of Analysis Page 1 of 1
Client Sample ID:BOTTOM (13')
Lab Sample ID:FA35839-9 Date Sampled:08/01/16
Matrix:SO - Soil Date Received:08/03/16
Percent Solids:71.5
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Solids, Percent 71.5 %1 08/03/16 16:49 ZC SM19 2540G
RL = Reporting Limit
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FA3583933.9
SGS Accutest
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Southeast
Section 4
19 of 35
FA358394
FA35839: Chain of Custody
Page 1 of 4
20 of 35
FA3583944.1
FA35839: Chain of Custody
Page 2 of 4
21 of 35
FA3583944.1
FA35839: Chain of Custody
Page 3 of 4
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FA3583944.1
Job Change FA35839
Requested Date: 8/9/2016 Received Date: 8/3/2016
Account Name: GRI (Geological Resources Inc.) Due Date: 8/10/2016
Project Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC Deliverable: COMMB
CSR: MunaM TAT (Days): 7
============================================================================================================= Sample #: FA35839-1 thru 4 Change:
Per client request analyze samples for V8260BTX.
=============================================================================================================
Above Changes Per: Corey Buchanan Date/Time: 8/9/2016 10:01:13 AM
This Change Order is confirmation of the revisions, previously discussed with the SGS Accutest Client Service Representative.
Page 1 of 1
FA35839: Chain of Custody
Page 4 of 4
23 of 35
FA3583944.1
SGS Accutest
GC Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Southeast
Section 5
24 of 35
FA358395
Method Blank Summary Page 1 of 1
Job Number:FA35839
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
GUV3995-MB UV075122.D 1 08/03/16 AH n/a n/a GUV3995
The QC reported here applies to the following samples:Method: SW846 8015C
FA35839-1, FA35839-2, FA35839-4
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 5.0 2.5 mg/kg
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 101%56-149%
98-08-8 aaa-Trifluorotoluene 98%66-132%
25 of 35
FA3583955.1.1
Method Blank Summary Page 1 of 1
Job Number:FA35839
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
GUV3996-MB UV075142.D 1 08/04/16 AH n/a n/a GUV3996
The QC reported here applies to the following samples:Method: SW846 8015C
FA35839-3
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 5.0 2.5 mg/kg
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 101%56-149%
98-08-8 aaa-Trifluorotoluene 98%66-132%
26 of 35
FA3583955.1.2
Blank Spike Summary Page 1 of 1
Job Number:FA35839
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
GUV3995-BS UV075118.D 1 08/03/16 AH n/a n/a GUV3995
The QC reported here applies to the following samples:Method: SW846 8015C
FA35839-1, FA35839-2, FA35839-4
Spike BSP BSP
CAS No.Compound mg/kg mg/kg %Limits
TPH-GRO (C6-C10)20 17.6 88 74-128
CAS No.Surrogate Recoveries BSP Limits
460-00-4 4-Bromofluorobenzene 108%56-149%
98-08-8 aaa-Trifluorotoluene 103%66-132%
* = Outside of Control Limits.
27 of 35
FA3583955.2.1
Blank Spike Summary Page 1 of 1
Job Number:FA35839
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
GUV3996-BS UV075141.D 1 08/04/16 AH n/a n/a GUV3996
The QC reported here applies to the following samples:Method: SW846 8015C
FA35839-3
Spike BSP BSP
CAS No.Compound mg/kg mg/kg %Limits
TPH-GRO (C6-C10)20 17.4 87 74-128
CAS No.Surrogate Recoveries BSP Limits
460-00-4 4-Bromofluorobenzene 105%56-149%
98-08-8 aaa-Trifluorotoluene 102%66-132%
* = Outside of Control Limits.
28 of 35
FA3583955.2.2
Matrix Spike Summary Page 1 of 1
Job Number:FA35839
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA35839-3MS UV075145.D 1 08/04/16 AH n/a n/a GUV3996
FA35839-3 UV075143.D 1 08/04/16 AH n/a n/a GUV3996
The QC reported here applies to the following samples:Method: SW846 8015C
FA35839-3
FA35839-3 Spike MS MS
CAS No.Compound mg/kg Q mg/kg mg/kg %Limits
TPH-GRO (C6-C10)164 70.9 218 76 74-128
CAS No.Surrogate Recoveries MS FA35839-3 Limits
460-00-4 4-Bromofluorobenzene 87%84%56-149%
98-08-8 aaa-Trifluorotoluene 113%110%66-132%
* = Outside of Control Limits.
29 of 35
FA3583955.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1
Job Number:FA35839
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA35839-4MS UV075129.D 1 08/04/16 AH n/a n/a GUV3995
FA35839-4MSD UV075130.D 1 08/04/16 AH n/a n/a GUV3995
FA35839-4 UV075128.D 1 08/04/16 AH n/a n/a GUV3995
The QC reported here applies to the following samples:Method: SW846 8015C
FA35839-1, FA35839-2, FA35839-4
FA35839-4 Spike MS MS Spike MSD MSD Limits
CAS No.Compound mg/kg Q mg/kg mg/kg %mg/kg mg/kg %RPD Rec/RPD
TPH-GRO (C6-C10)ND 47.2 32.4 69*47.2 31.0 66*4 74-128/17
CAS No.Surrogate Recoveries MS MSD FA35839-4 Limits
460-00-4 4-Bromofluorobenzene 105%107%101%56-149%
98-08-8 aaa-Trifluorotoluene 101%102%98%66-132%
* = Outside of Control Limits.
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FA3583955.4.1
Duplicate Summary Page 1 of 1
Job Number:FA35839
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA35839-3DUP UV075144.D 1 08/04/16 AH n/a n/a GUV3996
FA35839-3 UV075143.D 1 08/04/16 AH n/a n/a GUV3996
The QC reported here applies to the following samples:Method: SW846 8015C
FA35839-3
FA35839-3 DUP
CAS No.Compound mg/kg Q mg/kg Q RPD Limits
TPH-GRO (C6-C10)164 163 1 17
CAS No.Surrogate Recoveries DUP FA35839-3 Limits
460-00-4 4-Bromofluorobenzene 102%84%56-149%
98-08-8 aaa-Trifluorotoluene 109%110%66-132%
* = Outside of Control Limits.
31 of 35
FA3583955.5.1
SGS Accutest
GC Semi-volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Southeast
Section 6
32 of 35
FA358396
Method Blank Summary Page 1 of 1
Job Number:FA35839
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP61336-MB WR11725.D 1 08/09/16 SJL 08/04/16 OP61336 GWR447
The QC reported here applies to the following samples:Method: SW846 8015C
FA35839-1, FA35839-2, FA35839-3, FA35839-4
CAS No.Compound Result RL MDL Units Q
TPH (C10-C28)ND 6.3 3.8 mg/kg
CAS No.Surrogate Recoveries Limits
84-15-1 o-Terphenyl 82%56-122%
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FA3583966.1.1
Blank Spike Summary Page 1 of 1
Job Number:FA35839
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP61336-BS WR11724.D 1 08/09/16 SJL 08/04/16 OP61336 GWR447
The QC reported here applies to the following samples:Method: SW846 8015C
FA35839-1, FA35839-2, FA35839-3, FA35839-4
Spike BSP BSP
CAS No.Compound mg/kg mg/kg %Limits
TPH (C10-C28)50 42.9 86 62-116
CAS No.Surrogate Recoveries BSP Limits
84-15-1 o-Terphenyl 94%56-122%
* = Outside of Control Limits.
34 of 35
FA3583966.2.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1
Job Number:FA35839
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP61336-MS WR11730.D 10 08/09/16 SJL 08/04/16 OP61336 GWR447
OP61336-MSD WR11731.D 10 08/09/16 SJL 08/04/16 OP61336 GWR447
FA35839-1 WR11729.D 10 08/09/16 SJL 08/04/16 OP61336 GWR447
The QC reported here applies to the following samples:Method: SW846 8015C
FA35839-1, FA35839-2, FA35839-3, FA35839-4
FA35839-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound mg/kg Q mg/kg mg/kg %mg/kg mg/kg %RPD Rec/RPD
TPH (C10-C28)1860 62.4 1860 0* a 64.3 1100 -1183* a51*62-116/35
CAS No.Surrogate Recoveries MS MSD FA35839-1 Limits
84-15-1 o-Terphenyl 115%109%95%56-122%
(a) Outside control limits due to high level in sample relative to spike amount.
* = Outside of Control Limits.
35 of 35
FA3583966.3.1
08/10/16
Technical Report for
GRI (Geological Resources Inc.)
Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
4236
SGS Accutest Job Number: FA35839R
Sampling Date: 08/01/16
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
[e-mail]; [e-mail];
[e-mail]; [e-mail]
ATTN: Corey Buchanan
Total number of pages in report:
Certifications: FL (E83510), LA (03051), KS (E-10327), IA (366), IL (200063), NC (573), NJ (FL002), SC (96038001)
DoD ELAP (L-A-B L2229), CA (2937), TX (T104704404), PA (68-03573), VA (460177),
AK, AR, GA, KY, MA, NV, OK, UT, WA
This report shall not be reproduced, except in its entirety, without the written approval of SGS Accutest.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone] • http://www.accutest.com
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Norm Farmer
Technical Director
Southeast 08/10/16
e-Hardcopy 2.0
Automated Report
18
SGS Accutest is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
1 of 18
FA35839R
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................5
3.1: FA35839-1R: DI-1 (3') ..................................................................................................6
3.2: FA35839-2R: SP-1 (0-200) ...........................................................................................7
3.3: FA35839-3R: UST-1-1 (10') .........................................................................................8
3.4: FA35839-4R: UST-1-2 (10') .........................................................................................9
Section 4: Misc. Forms ............................................................................................................10
4.1: Chain of Custody ...........................................................................................................11
Section 5: GC/MS Volatiles - QC Data Summaries ..............................................................15
5.1: Method Blank Summary ................................................................................................16
5.2: Blank Spike Summary ...................................................................................................17
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................18 123452 of 18
FA35839R
SGS Accutest
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA35839R
Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Project No: 4236
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA35839-1R 08/01/16 10:01 CB 08/03/16 SO Soil DI-1 (3')
FA35839-2R 08/01/16 10:37 CB 08/03/16 SO Soil SP-1 (0-200)
FA35839-3R 08/01/16 12:37 CB 08/03/16 SO Soil UST-1-1 (10')
FA35839-4R 08/01/16 12:41 CB 08/03/16 SO Soil UST-1-2 (10')
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
3 of 18
FA35839R1
Summary of Hits Page 1 of 1
Job Number:FA35839R
Account:GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Collected:08/01/16
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA35839-1R DI-1 (3')
No hits reported in this sample.
FA35839-2R SP-1 (0-200)
No hits reported in this sample.
FA35839-3R UST-1-1 (10')
No hits reported in this sample.
FA35839-4R UST-1-2 (10')
No hits reported in this sample.
4 of 18
FA35839R2
SGS Accutest
Sample Results
Report of Analysis
Southeast
Section 3
5 of 18
FA35839R3
SGS Accutest
Report of Analysis Page 1 of 1
Client Sample ID:DI-1 (3')
Lab Sample ID:FA35839-1R Date Sampled:08/01/16
Matrix:SO - Soil Date Received:08/03/16
Method:SW846 8260B Percent Solids:78.2
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 Y30388.D 1 08/09/16 AD n/a n/a VY1224
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 6.09 g 5.0 ml 100 ul
Run #2
Purgeable Aromatics
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.33 0.084 mg/kg
108-88-3 Toluene ND 0.33 0.075 mg/kg
100-41-4 Ethylbenzene ND 0.33 0.072 mg/kg
1330-20-7 Xylene (total)ND 1.0 0.19 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 105%75-124%
17060-07-0 1,2-Dichloroethane-D4 111%72-135%
2037-26-5 Toluene-D8 94%75-126%
460-00-4 4-Bromofluorobenzene 96%71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
6 of 18
FA35839R33.1
SGS Accutest
Report of Analysis Page 1 of 1
Client Sample ID:SP-1 (0-200)
Lab Sample ID:FA35839-2R Date Sampled:08/01/16
Matrix:SO - Soil Date Received:08/03/16
Method:SW846 8260B Percent Solids:65.9
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 Y30389.D 1 08/09/16 AD n/a n/a VY1224
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 6.33 g 5.0 ml 100 ul
Run #2
Purgeable Aromatics
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.43 0.11 mg/kg
108-88-3 Toluene ND 0.43 0.097 mg/kg
100-41-4 Ethylbenzene ND 0.43 0.094 mg/kg
1330-20-7 Xylene (total)ND 1.3 0.24 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 107%75-124%
17060-07-0 1,2-Dichloroethane-D4 108%72-135%
2037-26-5 Toluene-D8 99%75-126%
460-00-4 4-Bromofluorobenzene 93%71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
7 of 18
FA35839R33.2
SGS Accutest
Report of Analysis Page 1 of 1
Client Sample ID:UST-1-1 (10')
Lab Sample ID:FA35839-3R Date Sampled:08/01/16
Matrix:SO - Soil Date Received:08/03/16
Method:SW846 8260B Percent Solids:67.1
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 Y30390.D 1 08/09/16 AD n/a n/a VY1224
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 5.89 g 5.0 ml 100 ul
Run #2
Purgeable Aromatics
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.44 0.11 mg/kg
108-88-3 Toluene ND 0.44 0.099 mg/kg
100-41-4 Ethylbenzene ND 0.44 0.096 mg/kg
1330-20-7 Xylene (total)ND 1.3 0.25 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 103%75-124%
17060-07-0 1,2-Dichloroethane-D4 106%72-135%
2037-26-5 Toluene-D8 96%75-126%
460-00-4 4-Bromofluorobenzene 92%71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
8 of 18
FA35839R33.3
SGS Accutest
Report of Analysis Page 1 of 1
Client Sample ID:UST-1-2 (10')
Lab Sample ID:FA35839-4R Date Sampled:08/01/16
Matrix:SO - Soil Date Received:08/03/16
Method:SW846 8260B Percent Solids:57.8
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 Y30392.D 1 08/09/16 AD n/a n/a VY1224
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 5.93 g 5.0 ml 100 ul
Run #2
Purgeable Aromatics
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.55 0.14 mg/kg
108-88-3 Toluene ND 0.55 0.12 mg/kg
100-41-4 Ethylbenzene ND 0.55 0.12 mg/kg
1330-20-7 Xylene (total)ND 1.6 0.31 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%75-124%
17060-07-0 1,2-Dichloroethane-D4 98%72-135%
2037-26-5 Toluene-D8 98%75-126%
460-00-4 4-Bromofluorobenzene 98%71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
9 of 18
FA35839R33.4
SGS Accutest
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Southeast
Section 4
10 of 18
FA35839R4
FA35839R: Chain of Custody
Page 1 of 4
11 of 18
FA35839R44.1
FA35839R: Chain of Custody
Page 2 of 4
12 of 18
FA35839R44.1
FA35839R: Chain of Custody
Page 3 of 4
13 of 18
FA35839R44.1
Job Change FA35839
Requested Date: 8/9/2016 Received Date: 8/3/2016
Account Name: GRI (Geological Resources Inc.) Due Date: 8/10/2016
Project Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC Deliverable: COMMB
CSR: MunaM TAT (Days): 7
============================================================================================================= Sample #: FA35839-1 thru 4 Change:
Per client request analyze samples for V8260BTX.
=============================================================================================================
Above Changes Per: Corey Buchanan Date/Time: 8/9/2016 10:01:13 AM
This Change Order is confirmation of the revisions, previously discussed with the SGS Accutest Client Service Representative.
Page 1 of 1
FA35839R: Chain of Custody
Page 4 of 4
14 of 18
FA35839R44.1
SGS Accutest
GC/MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Southeast
Section 5
15 of 18
FA35839R5
Method Blank Summary Page 1 of 1
Job Number:FA35839R
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VY1224-MB Y30383.D 1 08/09/16 AD n/a n/a VY1224
The QC reported here applies to the following samples:Method: SW846 8260B
FA35839-1R, FA35839-2R, FA35839-3R, FA35839-4R
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 5.0 1.3 ug/kg
100-41-4 Ethylbenzene ND 5.0 1.1 ug/kg
108-88-3 Toluene ND 5.0 1.1 ug/kg
1330-20-7 Xylene (total)ND 15 2.9 ug/kg
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 102%75-124%
17060-07-0 1,2-Dichloroethane-D4 112%72-135%
2037-26-5 Toluene-D8 104%75-126%
460-00-4 4-Bromofluorobenzene 99%71-133%
16 of 18
FA35839R55.1.1
Blank Spike Summary Page 1 of 1
Job Number:FA35839R
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VY1224-BS Y30382.D 1 08/09/16 AD n/a n/a VY1224
The QC reported here applies to the following samples:Method: SW846 8260B
FA35839-1R, FA35839-2R, FA35839-3R, FA35839-4R
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
71-43-2 Benzene 50 52.7 105 76-126
100-41-4 Ethylbenzene 50 51.9 104 77-123
108-88-3 Toluene 50 54.2 108 76-124
1330-20-7 Xylene (total)150 158 105 80-129
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 99%75-124%
17060-07-0 1,2-Dichloroethane-D4 107%72-135%
2037-26-5 Toluene-D8 99%75-126%
460-00-4 4-Bromofluorobenzene 100%71-133%
* = Outside of Control Limits.
17 of 18
FA35839R55.2.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1
Job Number:FA35839R
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA35950-4MS Y30386.D 1 08/09/16 AD n/a n/a VY1224
FA35950-4MSD Y30387.D 1 08/09/16 AD n/a n/a VY1224
FA35950-4 Y30385.D 1 08/09/16 AD n/a n/a VY1224
The QC reported here applies to the following samples:Method: SW846 8260B
FA35839-1R, FA35839-2R, FA35839-3R, FA35839-4R
FA35950-4 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
71-43-2 Benzene 4.3 U 70.9 61.9 87 72 55.2 77 11 76-126/26
100-41-4 Ethylbenzene 4.3 U 70.9 57.7 81 72 42.2 59*31 77-123/31
108-88-3 Toluene 4.3 U 70.9 67.9 96 72 53.7 75*23 76-124/30
1330-20-7 Xylene (total)13 U 213 176 83 216 130 60*30 80-129/30
CAS No.Surrogate Recoveries MS MSD FA35950-4 Limits
1868-53-7 Dibromofluoromethane 105%105%114%75-124%
17060-07-0 1,2-Dichloroethane-D4 109%110%118%72-135%
2037-26-5 Toluene-D8 103%98%103%75-126%
460-00-4 4-Bromofluorobenzene 107%100%116%71-133%
* = Outside of Control Limits.
18 of 18
FA35839R55.3.1
08/18/16
Technical Report for
GRI (Geological Resources Inc.)
Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
4236
SGS Accutest Job Number: FA35839T
Sampling Date: 08/01/16
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
[e-mail]; [e-mail];
[e-mail]; [e-mail]
ATTN: Corey Buchanan
Total number of pages in report:
Certifications: FL (E83510), LA (03051), KS (E-10327), IA (366), IL (200063), NC (573), NJ (FL002), SC (96038001)
DoD ELAP (L-A-B L2229), CA (2937), TX (T104704404), PA (68-03573), VA (460177),
AK, AR, GA, KY, MA, NV, OK, UT, WA
This report shall not be reproduced, except in its entirety, without the written approval of SGS Accutest.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone] • http://www.accutest.com
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Norm Farmer
Technical Director
Southeast 08/18/16
e-Hardcopy 2.0
Automated Report
66
SGS Accutest is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
1 of 66
FA35839T
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................5
3.1: FA35839-5T: SW-N (11') ..............................................................................................6
3.2: FA35839-6T: SW-E (11') ..............................................................................................12
3.3: FA35839-7T: SW-S (11') ..............................................................................................18
3.4: FA35839-9T: BOTTOM (13') .......................................................................................24
Section 4: Misc. Forms ............................................................................................................30
4.1: Chain of Custody ...........................................................................................................31
Section 5: GC/MS Volatiles - QC Data Summaries ..............................................................36
5.1: Method Blank Summary ................................................................................................37
5.2: Blank Spike Summary ...................................................................................................41
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................45
Section 6: GC/MS Semi-volatiles - QC Data Summaries .....................................................49
6.1: Method Blank Summary ................................................................................................50
6.2: Blank Spike Summary ...................................................................................................52
6.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................54
Section 7: GC Volatiles - QC Data Summaries .....................................................................56
7.1: Method Blank Summary ................................................................................................57
7.2: Blank Spike/Blank Spike Duplicate Summary ..............................................................59
7.3: Duplicate Summary .......................................................................................................61
Section 8: GC Semi-volatiles - QC Data Summaries ............................................................63
8.1: Method Blank Summary ................................................................................................64
8.2: Blank Spike/Blank Spike Duplicate Summary ..............................................................65
8.3: Duplicate Summary .......................................................................................................66 123456782 of 66
FA35839T
SGS Accutest
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA35839T
Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Project No: 4236
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA35839-5T 08/01/16 12:50 CB 08/03/16 SO Soil SW-N (11')
FA35839-6T 08/01/16 12:53 CB 08/03/16 SO Soil SW-E (11')
FA35839-7T 08/01/16 12:59 CB 08/03/16 SO Soil SW-S (11')
FA35839-9T 08/01/16 13:01 CB 08/03/16 SO Soil BOTTOM (13')
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
3 of 66
FA35839T1
Summary of Hits Page 1 of 1
Job Number:FA35839T
Account:GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Collected:08/01/16
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA35839-5T SW-N (11')
Acetone 0.0186 J 0.053 0.011 mg/kg SW846 8260B
FA35839-6T SW-E (11')
Acetone 0.271 0.062 0.013 mg/kg SW846 8260B
Benzene 0.0040 J 0.0062 0.0016 mg/kg SW846 8260B
Cyclohexane 0.0142 0.0062 0.0015 mg/kg SW846 8260B
Methylcyclohexane 0.0171 0.0062 0.0012 mg/kg SW846 8260B
Naphthalene 0.0361 0.0062 0.0025 mg/kg SW846 8260B
1,2,4-Trimethylbenzene 0.0082 0.0062 0.0012 mg/kg SW846 8260B
1,3,5-Trimethylbenzene 0.0207 0.0062 0.0012 mg/kg SW846 8260B
Xylene (total)0.0083 J 0.018 0.0035 mg/kg SW846 8260B
Acenaphthene 0.0985 J 0.24 0.032 mg/kg SW846 8270D
Fluoranthene 0.0490 J 0.24 0.030 mg/kg SW846 8270D
Fluorene 0.129 J 0.24 0.031 mg/kg SW846 8270D
1-Methylnaphthalene 0.242 0.24 0.038 mg/kg SW846 8270D
2-Methylnaphthalene 0.214 J 0.24 0.028 mg/kg SW846 8270D
Phenanthrene 0.515 0.24 0.030 mg/kg SW846 8270D
Pyrene 0.294 0.24 0.046 mg/kg SW846 8270D
Methyl Tert Butyl Ether 0.102 J 0.20 0.10 mg/kg MADEP VPH REV 1.1
Naphthalene 3.55 0.50 0.30 mg/kg MADEP VPH REV 1.1
o-Xylene 0.115 J 0.20 0.10 mg/kg MADEP VPH REV 1.1
C5- C8 Aliphatics (Unadj.)5.54 J 10 3.5 mg/kg MADEP VPH REV 1.1
C9- C12 Aliphatics (Unadj.)95.7 40 14 mg/kg MADEP VPH REV 1.1
C9- C10 Aromatics (Unadj.)64.3 40 14 mg/kg MADEP VPH REV 1.1
C5- C8 Aliphatics 5.44 J 10 3.5 mg/kg MADEP VPH REV 1.1
C9- C12 Aliphatics 95.5 40 14 mg/kg MADEP VPH REV 1.1
C9- C10 Aromatics 64.3 40 14 mg/kg MADEP VPH REV 1.1
C11-C22 Aromatics (Unadj.) a 170 59 44 mg/kg MADEP EPH REV 1.1
C11-C22 Aromatics a 170 59 44 mg/kg MADEP EPH REV 1.1
C9-C18 Aliphatics a 574 59 30 mg/kg MADEP EPH REV 1.1
C19-C36 Aliphatics a 79.3 59 30 mg/kg MADEP EPH REV 1.1
FA35839-7T SW-S (11')
Acetone 0.0225 J 0.064 0.013 mg/kg SW846 8260B
FA35839-9T BOTTOM (13')
No hits reported in this sample.
(a) Dilution required due to matrix interference.
4 of 66
FA35839T2
SGS Accutest
Sample Results
Report of Analysis
Southeast
Section 3
5 of 66
FA35839T3
SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID:SW-N (11')
Lab Sample ID:FA35839-5T Date Sampled:08/01/16
Matrix:SO - Soil Date Received:08/03/16
Method:SW846 8260B Percent Solids:85.9
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 F0078941.D 1 08/03/16 EP n/a n/a VF2712
Run #2
Initial Weight Final Volume
Run #1 5.47 g 5.0 ml
Run #2
VOA Special List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 0.0186 0.053 0.011 mg/kg J
71-43-2 Benzene ND 0.0053 0.0013 mg/kg
75-27-4 Bromodichloromethane ND 0.0053 0.0011 mg/kg
75-25-2 Bromoform ND 0.0053 0.0011 mg/kg
78-93-3 2-Butanone (MEK)ND 0.027 0.0097 mg/kg
104-51-8 n-Butylbenzene ND 0.0053 0.0011 mg/kg
75-15-0 Carbon Disulfide ND 0.0053 0.0011 mg/kg
56-23-5 Carbon Tetrachloride ND 0.0053 0.0019 mg/kg
108-90-7 Chlorobenzene ND 0.0053 0.0011 mg/kg
75-00-3 Chloroethane ND 0.0053 0.0021 mg/kg
67-66-3 Chloroform ND 0.0053 0.0013 mg/kg
110-82-7 Cyclohexane ND 0.0053 0.0013 mg/kg
124-48-1 Dibromochloromethane ND 0.0053 0.0011 mg/kg
96-12-8 1,2-Dibromo-3-chloropropane ND 0.0053 0.0024 mg/kg
106-93-4 1,2-Dibromoethane ND 0.0053 0.0011 mg/kg
75-71-8 Dichlorodifluoromethane ND 0.0053 0.0026 mg/kg
95-50-1 1,2-Dichlorobenzene ND 0.0053 0.0011 mg/kg
541-73-1 1,3-Dichlorobenzene ND 0.0053 0.0011 mg/kg
106-46-7 1,4-Dichlorobenzene ND 0.0053 0.0011 mg/kg
75-34-3 1,1-Dichloroethane ND 0.0053 0.0018 mg/kg
107-06-2 1,2-Dichloroethane ND 0.0053 0.0011 mg/kg
75-35-4 1,1-Dichloroethylene ND 0.0053 0.0011 mg/kg
156-59-2 cis-1,2-Dichloroethylene ND 0.0053 0.0013 mg/kg
156-60-5 trans-1,2-Dichloroethylene ND 0.0053 0.0016 mg/kg
78-87-5 1,2-Dichloropropane ND 0.0053 0.0017 mg/kg
10061-01-5 cis-1,3-Dichloropropene ND 0.0053 0.0020 mg/kg
10061-02-6 trans-1,3-Dichloropropene ND 0.0053 0.0011 mg/kg
100-41-4 Ethylbenzene ND 0.0053 0.0012 mg/kg
591-78-6 2-Hexanone ND 0.027 0.0093 mg/kg
98-82-8 Isopropylbenzene ND 0.0053 0.0015 mg/kg
79-20-9 Methyl Acetate ND 0.027 0.0091 mg/kg
74-83-9 Methyl Bromide ND 0.0053 0.0027 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
6 of 66
FA35839T33.1
SGS Accutest
Report of Analysis Page 2 of 2
Client Sample ID:SW-N (11')
Lab Sample ID:FA35839-5T Date Sampled:08/01/16
Matrix:SO - Soil Date Received:08/03/16
Method:SW846 8260B Percent Solids:85.9
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
VOA Special List
CAS No.Compound Result RL MDL Units Q
74-87-3 Methyl Chloride ND 0.0053 0.0026 mg/kg
108-87-2 Methylcyclohexane ND 0.0053 0.0011 mg/kg
75-09-2 Methylene Chloride ND 0.011 0.0043 mg/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 0.027 0.011 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.0053 0.0012 mg/kg
91-20-3 Naphthalene ND 0.0053 0.0021 mg/kg
103-65-1 n-Propylbenzene ND 0.0053 0.0013 mg/kg
100-42-5 Styrene ND 0.0053 0.0011 mg/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 0.0053 0.0024 mg/kg
127-18-4 Tetrachloroethylene ND 0.0053 0.0014 mg/kg
108-88-3 Toluene ND 0.0053 0.0012 mg/kg
120-82-1 1,2,4-Trichlorobenzene ND 0.0053 0.0016 mg/kg
71-55-6 1,1,1-Trichloroethane ND 0.0053 0.0011 mg/kg
79-00-5 1,1,2-Trichloroethane ND 0.0053 0.0019 mg/kg
79-01-6 Trichloroethylene ND 0.0053 0.0012 mg/kg
75-69-4 Trichlorofluoromethane ND 0.0053 0.0020 mg/kg
95-63-6 1,2,4-Trimethylbenzene ND 0.0053 0.0011 mg/kg
108-67-8 1,3,5-Trimethylbenzene ND 0.0053 0.0011 mg/kg
75-01-4 Vinyl Chloride ND 0.0053 0.0018 mg/kg
1330-20-7 Xylene (total)ND 0.016 0.0030 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 106%75-124%
17060-07-0 1,2-Dichloroethane-D4 104%72-135%
2037-26-5 Toluene-D8 94%75-126%
460-00-4 4-Bromofluorobenzene 110%71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
7 of 66
FA35839T33.1
SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID:SW-N (11')
Lab Sample ID:FA35839-5T Date Sampled:08/01/16
Matrix:SO - Soil Date Received:08/03/16
Method:SW846 8270D SW846 3550C Percent Solids:85.9
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 X048314.D 1 08/12/16 MV 08/11/16 OP61449 SX2101
Run #2
Initial Weight Final Volume
Run #1 30.5 g 1.0 ml
Run #2
ABN Special List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 0.95 0.19 mg/kg
59-50-7 4-Chloro-3-methyl Phenol ND 0.19 0.029 mg/kg
95-57-8 2-Chlorophenol ND 0.19 0.024 mg/kg
120-83-2 2,4-Dichlorophenol ND 0.19 0.027 mg/kg
105-67-9 2,4-Dimethylphenol ND 0.19 0.023 mg/kg
51-28-5 2,4-Dinitrophenol ND 0.95 0.19 mg/kg
534-52-1 4,6-Dinitro-o-cresol ND 0.38 0.076 mg/kg
95-48-7 2-Methylphenol ND 0.19 0.020 mg/kg
3&4-Methylphenol ND 0.19 0.045 mg/kg
88-75-5 2-Nitrophenol ND 0.19 0.024 mg/kg
100-02-7 4-Nitrophenol ND 0.95 0.15 mg/kg
87-86-5 Pentachlorophenol ND 0.95 0.15 mg/kg
108-95-2 Phenol ND 0.19 0.023 mg/kg
88-06-2 2,4,6-Trichlorophenol ND 0.19 0.023 mg/kg
83-32-9 Acenaphthene ND 0.19 0.025 mg/kg
208-96-8 Acenaphthylene ND 0.19 0.024 mg/kg
120-12-7 Anthracene ND 0.19 0.028 mg/kg
56-55-3 Benzo(a)anthracene ND 0.19 0.022 mg/kg
50-32-8 Benzo(a)pyrene ND 0.19 0.020 mg/kg
205-99-2 Benzo(b)fluoranthene ND 0.19 0.024 mg/kg
191-24-2 Benzo(g,h,i)perylene ND 0.19 0.019 mg/kg
207-08-9 Benzo(k)fluoranthene ND 0.19 0.027 mg/kg
101-55-3 4-Bromophenyl phenyl ether ND 0.19 0.022 mg/kg
85-68-7 Butyl benzyl phthalate ND 0.19 0.038 mg/kg
106-47-8 4-Chloroaniline ND 0.19 0.027 mg/kg
111-91-1 bis(2-Chloroethoxy)methane ND 0.19 0.029 mg/kg
111-44-4 bis(2-Chloroethyl)ether ND 0.19 0.034 mg/kg
108-60-1 bis(2-Chloroisopropyl)ether ND 0.19 0.028 mg/kg
91-58-7 2-Chloronaphthalene ND 0.19 0.026 mg/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 0.19 0.024 mg/kg
218-01-9 Chrysene ND 0.19 0.026 mg/kg
53-70-3 Dibenzo(a,h)anthracene ND 0.19 0.020 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
8 of 66
FA35839T33.1
SGS Accutest
Report of Analysis Page 2 of 2
Client Sample ID:SW-N (11')
Lab Sample ID:FA35839-5T Date Sampled:08/01/16
Matrix:SO - Soil Date Received:08/03/16
Method:SW846 8270D SW846 3550C Percent Solids:85.9
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
ABN Special List
CAS No.Compound Result RL MDL Units Q
132-64-9 Dibenzofuran ND 0.19 0.024 mg/kg
91-94-1 3,3'-Dichlorobenzidine ND 0.19 0.021 mg/kg
84-66-2 Diethyl Phthalate ND 0.38 0.038 mg/kg
131-11-3 Dimethyl Phthalate ND 0.19 0.038 mg/kg
117-84-0 Di-n-octyl Phthalate ND 0.19 0.038 mg/kg
84-74-2 Di-n-butyl Phthalate ND 0.38 0.076 mg/kg
121-14-2 2,4-Dinitrotoluene ND 0.19 0.019 mg/kg
606-20-2 2,6-Dinitrotoluene ND 0.19 0.024 mg/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 0.38 0.038 mg/kg
206-44-0 Fluoranthene ND 0.19 0.023 mg/kg
86-73-7 Fluorene ND 0.19 0.024 mg/kg
118-74-1 Hexachlorobenzene ND 0.19 0.024 mg/kg
87-68-3 Hexachlorobutadiene ND 0.19 0.021 mg/kg
77-47-4 Hexachlorocyclopentadiene a ND 0.19 0.038 mg/kg
67-72-1 Hexachloroethane ND 0.19 0.022 mg/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 0.19 0.029 mg/kg
78-59-1 Isophorone ND 0.19 0.020 mg/kg
90-12-0 1-Methylnaphthalene ND 0.19 0.030 mg/kg
91-57-6 2-Methylnaphthalene ND 0.19 0.021 mg/kg
91-20-3 Naphthalene ND 0.19 0.029 mg/kg
98-95-3 Nitrobenzene ND 0.19 0.025 mg/kg
621-64-7 N-Nitrosodi-n-propylamine ND 0.19 0.020 mg/kg
86-30-6 N-Nitrosodiphenylamine ND 0.19 0.036 mg/kg
85-01-8 Phenanthrene ND 0.19 0.023 mg/kg
129-00-0 Pyrene ND 0.19 0.036 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 66%40-102%
4165-62-2 Phenol-d5 73%41-100%
118-79-6 2,4,6-Tribromophenol 77%42-108%
4165-60-0 Nitrobenzene-d5 74%40-105%
321-60-8 2-Fluorobiphenyl 79%43-107%
1718-51-0 Terphenyl-d14 80%45-119%
(a) Associated CCV outside control limits.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
9 of 66
FA35839T33.1
SGS Accutest
Report of Analysis Page 1 of 1
Client Sample ID:SW-N (11')
Lab Sample ID:FA35839-5T Date Sampled:08/01/16
Matrix:SO - Soil Date Received:08/03/16
Method:MADEP VPH REV 1.1 Percent Solids:85.9
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 UU016740.D 1 08/03/16 AH n/a n/a GUU853
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 5.20 g 5.1 ml 100 ul
Run #2
MADEP VPH List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.065 0.065 mg/kg
100-41-4 Ethylbenzene ND 0.13 0.065 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.13 0.065 mg/kg
91-20-3 Naphthalene ND 0.33 0.20 mg/kg
108-88-3 Toluene ND 0.13 0.065 mg/kg
m,p-Xylene ND 0.26 0.13 mg/kg
95-47-6 o-Xylene ND 0.13 0.065 mg/kg
C5- C8 Aliphatics (Unadj.)ND 6.5 2.3 mg/kg
C9- C12 Aliphatics (Unadj.)ND 6.5 2.3 mg/kg
C9- C10 Aromatics (Unadj.)ND 6.5 2.3 mg/kg
C5- C8 Aliphatics ND 6.5 2.3 mg/kg
C9- C12 Aliphatics ND 6.5 2.3 mg/kg
C9- C10 Aromatics ND 6.5 2.3 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 BFB 88%70-130%
460-00-4 BFB 90%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 66
FA35839T33.1
SGS Accutest
Report of Analysis Page 1 of 1
Client Sample ID:SW-N (11')
Lab Sample ID:FA35839-5T Date Sampled:08/01/16
Matrix:SO - Soil Date Received:08/03/16
Method:MADEP EPH REV 1.1 SW846 3546 Percent Solids:85.9
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 NN015928.D 1 08/17/16 FS 08/11/16 OP61448 GNN787
Run #2
Initial Weight Final Volume
Run #1 20.0 g 2.0 ml
Run #2
MAEPH List
CAS No.Compound Result RL MDL Units Q
83-32-9 Acenaphthene ND 0.23 0.12 mg/kg
208-96-8 Acenaphthylene ND 0.23 0.12 mg/kg
120-12-7 Anthracene ND 0.23 0.12 mg/kg
56-55-3 Benzo(a)anthracene ND 0.23 0.12 mg/kg
50-32-8 Benzo(a)pyrene ND 0.23 0.12 mg/kg
205-99-2 Benzo(b)fluoranthene ND 0.23 0.12 mg/kg
191-24-2 Benzo(g,h,i)perylene ND 0.23 0.12 mg/kg
207-08-9 Benzo(k)fluoranthene ND 0.23 0.12 mg/kg
218-01-9 Chrysene ND 0.23 0.12 mg/kg
53-70-3 Dibenzo(a,h)anthracene ND 0.23 0.12 mg/kg
206-44-0 Fluoranthene ND 0.23 0.12 mg/kg
86-73-7 Fluorene ND 0.23 0.12 mg/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 0.23 0.12 mg/kg
91-57-6 2-Methylnaphthalene ND 0.23 0.12 mg/kg
91-20-3 Naphthalene ND 0.23 0.12 mg/kg
85-01-8 Phenanthrene ND 0.23 0.12 mg/kg
129-00-0 Pyrene ND 0.23 0.12 mg/kg
C11-C22 Aromatics (Unadj.)ND 12 8.7 mg/kg
C11-C22 Aromatics ND 12 8.7 mg/kg
C9-C18 Aliphatics ND 12 5.8 mg/kg
C19-C36 Aliphatics ND 12 5.8 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
3386-33-2 1-Chlorooctadecane 61%40-140%
580-13-2 2-Bromonaphthalene 88%40-140%
84-15-1 o-Terphenyl 63%40-140%
321-60-8 2-Fluorobiphenyl 78%40-140%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 66
FA35839T33.1
SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID:SW-E (11')
Lab Sample ID:FA35839-6T Date Sampled:08/01/16
Matrix:SO - Soil Date Received:08/03/16
Method:SW846 8260B Percent Solids:68.3
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 F0078942.D 1 08/03/16 EP n/a n/a VF2712
Run #2
Initial Weight Final Volume
Run #1 5.94 g 5.0 ml
Run #2
VOA Special List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 0.271 0.062 0.013 mg/kg
71-43-2 Benzene 0.0040 0.0062 0.0016 mg/kg J
75-27-4 Bromodichloromethane ND 0.0062 0.0012 mg/kg
75-25-2 Bromoform ND 0.0062 0.0012 mg/kg
78-93-3 2-Butanone (MEK)ND 0.031 0.011 mg/kg
104-51-8 n-Butylbenzene ND 0.0062 0.0012 mg/kg
75-15-0 Carbon Disulfide ND 0.0062 0.0012 mg/kg
56-23-5 Carbon Tetrachloride ND 0.0062 0.0022 mg/kg
108-90-7 Chlorobenzene ND 0.0062 0.0012 mg/kg
75-00-3 Chloroethane ND 0.0062 0.0025 mg/kg
67-66-3 Chloroform ND 0.0062 0.0015 mg/kg
110-82-7 Cyclohexane 0.0142 0.0062 0.0015 mg/kg
124-48-1 Dibromochloromethane ND 0.0062 0.0012 mg/kg
96-12-8 1,2-Dibromo-3-chloropropane ND 0.0062 0.0027 mg/kg
106-93-4 1,2-Dibromoethane ND 0.0062 0.0012 mg/kg
75-71-8 Dichlorodifluoromethane ND 0.0062 0.0031 mg/kg
95-50-1 1,2-Dichlorobenzene ND 0.0062 0.0012 mg/kg
541-73-1 1,3-Dichlorobenzene ND 0.0062 0.0012 mg/kg
106-46-7 1,4-Dichlorobenzene ND 0.0062 0.0013 mg/kg
75-34-3 1,1-Dichloroethane ND 0.0062 0.0021 mg/kg
107-06-2 1,2-Dichloroethane ND 0.0062 0.0012 mg/kg
75-35-4 1,1-Dichloroethylene ND 0.0062 0.0012 mg/kg
156-59-2 cis-1,2-Dichloroethylene ND 0.0062 0.0015 mg/kg
156-60-5 trans-1,2-Dichloroethylene ND 0.0062 0.0019 mg/kg
78-87-5 1,2-Dichloropropane ND 0.0062 0.0020 mg/kg
10061-01-5 cis-1,3-Dichloropropene ND 0.0062 0.0023 mg/kg
10061-02-6 trans-1,3-Dichloropropene ND 0.0062 0.0012 mg/kg
100-41-4 Ethylbenzene ND 0.0062 0.0013 mg/kg
591-78-6 2-Hexanone ND 0.031 0.011 mg/kg
98-82-8 Isopropylbenzene ND 0.0062 0.0017 mg/kg
79-20-9 Methyl Acetate ND 0.031 0.011 mg/kg
74-83-9 Methyl Bromide ND 0.0062 0.0032 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 66
FA35839T33.2
SGS Accutest
Report of Analysis Page 2 of 2
Client Sample ID:SW-E (11')
Lab Sample ID:FA35839-6T Date Sampled:08/01/16
Matrix:SO - Soil Date Received:08/03/16
Method:SW846 8260B Percent Solids:68.3
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
VOA Special List
CAS No.Compound Result RL MDL Units Q
74-87-3 Methyl Chloride ND 0.0062 0.0030 mg/kg
108-87-2 Methylcyclohexane 0.0171 0.0062 0.0012 mg/kg
75-09-2 Methylene Chloride ND 0.012 0.0049 mg/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 0.031 0.013 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.0062 0.0014 mg/kg
91-20-3 Naphthalene 0.0361 0.0062 0.0025 mg/kg
103-65-1 n-Propylbenzene ND 0.0062 0.0015 mg/kg
100-42-5 Styrene ND 0.0062 0.0012 mg/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 0.0062 0.0027 mg/kg
127-18-4 Tetrachloroethylene ND 0.0062 0.0016 mg/kg
108-88-3 Toluene ND 0.0062 0.0014 mg/kg
120-82-1 1,2,4-Trichlorobenzene ND 0.0062 0.0018 mg/kg
71-55-6 1,1,1-Trichloroethane ND 0.0062 0.0012 mg/kg
79-00-5 1,1,2-Trichloroethane ND 0.0062 0.0022 mg/kg
79-01-6 Trichloroethylene ND 0.0062 0.0014 mg/kg
75-69-4 Trichlorofluoromethane ND 0.0062 0.0023 mg/kg
95-63-6 1,2,4-Trimethylbenzene 0.0082 0.0062 0.0012 mg/kg
108-67-8 1,3,5-Trimethylbenzene 0.0207 0.0062 0.0012 mg/kg
75-01-4 Vinyl Chloride ND 0.0062 0.0021 mg/kg
1330-20-7 Xylene (total)0.0083 0.018 0.0035 mg/kg J
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 113%75-124%
17060-07-0 1,2-Dichloroethane-D4 107%72-135%
2037-26-5 Toluene-D8 95%75-126%
460-00-4 4-Bromofluorobenzene 117%71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
13 of 66
FA35839T33.2
SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID:SW-E (11')
Lab Sample ID:FA35839-6T Date Sampled:08/01/16
Matrix:SO - Soil Date Received:08/03/16
Method:SW846 8270D SW846 3550C Percent Solids:68.3
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 X048315.D 1 08/12/16 MV 08/11/16 OP61449 SX2101
Run #2
Initial Weight Final Volume
Run #1 29.9 g 1.0 ml
Run #2
ABN Special List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 1.2 0.24 mg/kg
59-50-7 4-Chloro-3-methyl Phenol ND 0.24 0.037 mg/kg
95-57-8 2-Chlorophenol ND 0.24 0.031 mg/kg
120-83-2 2,4-Dichlorophenol ND 0.24 0.034 mg/kg
105-67-9 2,4-Dimethylphenol ND 0.24 0.030 mg/kg
51-28-5 2,4-Dinitrophenol ND 1.2 0.24 mg/kg
534-52-1 4,6-Dinitro-o-cresol ND 0.49 0.098 mg/kg
95-48-7 2-Methylphenol ND 0.24 0.026 mg/kg
3&4-Methylphenol ND 0.24 0.058 mg/kg
88-75-5 2-Nitrophenol ND 0.24 0.030 mg/kg
100-02-7 4-Nitrophenol ND 1.2 0.20 mg/kg
87-86-5 Pentachlorophenol ND 1.2 0.20 mg/kg
108-95-2 Phenol ND 0.24 0.029 mg/kg
88-06-2 2,4,6-Trichlorophenol ND 0.24 0.030 mg/kg
83-32-9 Acenaphthene 0.0985 0.24 0.032 mg/kg J
208-96-8 Acenaphthylene ND 0.24 0.031 mg/kg
120-12-7 Anthracene ND 0.24 0.036 mg/kg
56-55-3 Benzo(a)anthracene ND 0.24 0.028 mg/kg
50-32-8 Benzo(a)pyrene ND 0.24 0.026 mg/kg
205-99-2 Benzo(b)fluoranthene ND 0.24 0.031 mg/kg
191-24-2 Benzo(g,h,i)perylene ND 0.24 0.024 mg/kg
207-08-9 Benzo(k)fluoranthene ND 0.24 0.034 mg/kg
101-55-3 4-Bromophenyl phenyl ether ND 0.24 0.029 mg/kg
85-68-7 Butyl benzyl phthalate ND 0.24 0.049 mg/kg
106-47-8 4-Chloroaniline ND 0.24 0.034 mg/kg
111-91-1 bis(2-Chloroethoxy)methane ND 0.24 0.037 mg/kg
111-44-4 bis(2-Chloroethyl)ether ND 0.24 0.044 mg/kg
108-60-1 bis(2-Chloroisopropyl)ether ND 0.24 0.036 mg/kg
91-58-7 2-Chloronaphthalene ND 0.24 0.034 mg/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 0.24 0.031 mg/kg
218-01-9 Chrysene ND 0.24 0.033 mg/kg
53-70-3 Dibenzo(a,h)anthracene ND 0.24 0.026 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
14 of 66
FA35839T33.2
SGS Accutest
Report of Analysis Page 2 of 2
Client Sample ID:SW-E (11')
Lab Sample ID:FA35839-6T Date Sampled:08/01/16
Matrix:SO - Soil Date Received:08/03/16
Method:SW846 8270D SW846 3550C Percent Solids:68.3
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
ABN Special List
CAS No.Compound Result RL MDL Units Q
132-64-9 Dibenzofuran ND 0.24 0.031 mg/kg
91-94-1 3,3'-Dichlorobenzidine ND 0.24 0.027 mg/kg
84-66-2 Diethyl Phthalate ND 0.49 0.049 mg/kg
131-11-3 Dimethyl Phthalate ND 0.24 0.049 mg/kg
117-84-0 Di-n-octyl Phthalate ND 0.24 0.049 mg/kg
84-74-2 Di-n-butyl Phthalate ND 0.49 0.098 mg/kg
121-14-2 2,4-Dinitrotoluene ND 0.24 0.024 mg/kg
606-20-2 2,6-Dinitrotoluene ND 0.24 0.031 mg/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 0.49 0.049 mg/kg
206-44-0 Fluoranthene 0.0490 0.24 0.030 mg/kg J
86-73-7 Fluorene 0.129 0.24 0.031 mg/kg J
118-74-1 Hexachlorobenzene ND 0.24 0.030 mg/kg
87-68-3 Hexachlorobutadiene ND 0.24 0.028 mg/kg
77-47-4 Hexachlorocyclopentadiene a ND 0.24 0.049 mg/kg
67-72-1 Hexachloroethane ND 0.24 0.028 mg/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 0.24 0.038 mg/kg
78-59-1 Isophorone ND 0.24 0.025 mg/kg
90-12-0 1-Methylnaphthalene 0.242 0.24 0.038 mg/kg
91-57-6 2-Methylnaphthalene 0.214 0.24 0.028 mg/kg J
91-20-3 Naphthalene ND 0.24 0.037 mg/kg
98-95-3 Nitrobenzene ND 0.24 0.032 mg/kg
621-64-7 N-Nitrosodi-n-propylamine ND 0.24 0.026 mg/kg
86-30-6 N-Nitrosodiphenylamine ND 0.24 0.047 mg/kg
85-01-8 Phenanthrene 0.515 0.24 0.030 mg/kg
129-00-0 Pyrene 0.294 0.24 0.046 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 71%40-102%
4165-62-2 Phenol-d5 79%41-100%
118-79-6 2,4,6-Tribromophenol 88%42-108%
4165-60-0 Nitrobenzene-d5 81%40-105%
321-60-8 2-Fluorobiphenyl 81%43-107%
1718-51-0 Terphenyl-d14 82%45-119%
(a) Associated CCV outside control limits.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
15 of 66
FA35839T33.2
SGS Accutest
Report of Analysis Page 1 of 1
Client Sample ID:SW-E (11')
Lab Sample ID:FA35839-6T Date Sampled:08/01/16
Matrix:SO - Soil Date Received:08/03/16
Method:MADEP VPH REV 1.1 Percent Solids:68.3
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 UU016742.D 1 08/03/16 AH n/a n/a GUU853
Run #2 UU016783.D 1 08/04/16 AH n/a n/a GUU855
Initial Weight Final Volume Methanol Aliquot
Run #1 4.82 g 5.1 ml 100 ul
Run #2 4.82 g 5.1 ml 25.0 ul
MADEP VPH List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.10 0.10 mg/kg
100-41-4 Ethylbenzene ND 0.20 0.10 mg/kg
1634-04-4 Methyl Tert Butyl Ether 0.102 0.20 0.10 mg/kg J
91-20-3 Naphthalene 3.55 0.50 0.30 mg/kg
108-88-3 Toluene ND 0.20 0.10 mg/kg
m,p-Xylene ND 0.40 0.20 mg/kg
95-47-6 o-Xylene 0.115 0.20 0.10 mg/kg J
C5- C8 Aliphatics (Unadj.)5.54 10 3.5 mg/kg J
C9- C12 Aliphatics (Unadj.)95.7 a 40 14 mg/kg
C9- C10 Aromatics (Unadj.)64.3 a 40 14 mg/kg
C5- C8 Aliphatics 5.44 10 3.5 mg/kg J
C9- C12 Aliphatics 95.5 a 40 14 mg/kg
C9- C10 Aromatics 64.3 a 40 14 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 BFB 103%99%70-130%
460-00-4 BFB 99%99%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
16 of 66
FA35839T33.2
SGS Accutest
Report of Analysis Page 1 of 1
Client Sample ID:SW-E (11')
Lab Sample ID:FA35839-6T Date Sampled:08/01/16
Matrix:SO - Soil Date Received:08/03/16
Method:MADEP EPH REV 1.1 SW846 3546 Percent Solids:68.3
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a NN015932.D 4 08/17/16 FS 08/11/16 OP61448 GNN787
Run #2
Initial Weight Final Volume
Run #1 19.8 g 2.0 ml
Run #2
MAEPH List
CAS No.Compound Result RL MDL Units Q
83-32-9 Acenaphthene ND 1.2 0.59 mg/kg
208-96-8 Acenaphthylene ND 1.2 0.59 mg/kg
120-12-7 Anthracene ND 1.2 0.59 mg/kg
56-55-3 Benzo(a)anthracene ND 1.2 0.59 mg/kg
50-32-8 Benzo(a)pyrene ND 1.2 0.59 mg/kg
205-99-2 Benzo(b)fluoranthene ND 1.2 0.59 mg/kg
191-24-2 Benzo(g,h,i)perylene ND 1.2 0.59 mg/kg
207-08-9 Benzo(k)fluoranthene ND 1.2 0.59 mg/kg
218-01-9 Chrysene ND 1.2 0.59 mg/kg
53-70-3 Dibenzo(a,h)anthracene ND 1.2 0.59 mg/kg
206-44-0 Fluoranthene ND 1.2 0.59 mg/kg
86-73-7 Fluorene ND 1.2 0.59 mg/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 1.2 0.59 mg/kg
91-57-6 2-Methylnaphthalene ND 1.2 0.59 mg/kg
91-20-3 Naphthalene ND 1.2 0.59 mg/kg
85-01-8 Phenanthrene ND 1.2 0.59 mg/kg
129-00-0 Pyrene ND 1.2 0.59 mg/kg
C11-C22 Aromatics (Unadj.)170 59 44 mg/kg
C11-C22 Aromatics 170 59 44 mg/kg
C9-C18 Aliphatics 574 59 30 mg/kg
C19-C36 Aliphatics 79.3 59 30 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
3386-33-2 1-Chlorooctadecane 48%40-140%
580-13-2 2-Bromonaphthalene 91%40-140%
84-15-1 o-Terphenyl 69%40-140%
321-60-8 2-Fluorobiphenyl 77%40-140%
(a) Dilution required due to matrix interference.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
17 of 66
FA35839T33.2
SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID:SW-S (11')
Lab Sample ID:FA35839-7T Date Sampled:08/01/16
Matrix:SO - Soil Date Received:08/03/16
Method:SW846 8260B Percent Solids:63.0
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 Y30284.D 1 08/03/16 AD n/a n/a VY1220
Run #2
Initial Weight Final Volume
Run #1 6.16 g 5.0 ml
Run #2
VOA Special List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 0.0225 0.064 0.013 mg/kg J
71-43-2 Benzene ND 0.0064 0.0016 mg/kg
75-27-4 Bromodichloromethane ND 0.0064 0.0013 mg/kg
75-25-2 Bromoform ND 0.0064 0.0013 mg/kg
78-93-3 2-Butanone (MEK)ND 0.032 0.012 mg/kg
104-51-8 n-Butylbenzene ND 0.0064 0.0013 mg/kg
75-15-0 Carbon Disulfide ND 0.0064 0.0013 mg/kg
56-23-5 Carbon Tetrachloride ND 0.0064 0.0023 mg/kg
108-90-7 Chlorobenzene ND 0.0064 0.0013 mg/kg
75-00-3 Chloroethane ND 0.0064 0.0026 mg/kg
67-66-3 Chloroform ND 0.0064 0.0016 mg/kg
110-82-7 Cyclohexane ND 0.0064 0.0016 mg/kg
124-48-1 Dibromochloromethane ND 0.0064 0.0013 mg/kg
96-12-8 1,2-Dibromo-3-chloropropane ND 0.0064 0.0029 mg/kg
106-93-4 1,2-Dibromoethane ND 0.0064 0.0013 mg/kg
75-71-8 Dichlorodifluoromethane ND 0.0064 0.0032 mg/kg
95-50-1 1,2-Dichlorobenzene ND 0.0064 0.0013 mg/kg
541-73-1 1,3-Dichlorobenzene ND 0.0064 0.0013 mg/kg
106-46-7 1,4-Dichlorobenzene ND 0.0064 0.0013 mg/kg
75-34-3 1,1-Dichloroethane ND 0.0064 0.0022 mg/kg
107-06-2 1,2-Dichloroethane ND 0.0064 0.0013 mg/kg
75-35-4 1,1-Dichloroethylene ND 0.0064 0.0013 mg/kg
156-59-2 cis-1,2-Dichloroethylene ND 0.0064 0.0015 mg/kg
156-60-5 trans-1,2-Dichloroethylene ND 0.0064 0.0020 mg/kg
78-87-5 1,2-Dichloropropane ND 0.0064 0.0020 mg/kg
10061-01-5 cis-1,3-Dichloropropene ND 0.0064 0.0024 mg/kg
10061-02-6 trans-1,3-Dichloropropene ND 0.0064 0.0013 mg/kg
100-41-4 Ethylbenzene ND 0.0064 0.0014 mg/kg
591-78-6 2-Hexanone ND 0.032 0.011 mg/kg
98-82-8 Isopropylbenzene ND 0.0064 0.0018 mg/kg
79-20-9 Methyl Acetate ND 0.032 0.011 mg/kg
74-83-9 Methyl Bromide ND 0.0064 0.0033 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
18 of 66
FA35839T33.3
SGS Accutest
Report of Analysis Page 2 of 2
Client Sample ID:SW-S (11')
Lab Sample ID:FA35839-7T Date Sampled:08/01/16
Matrix:SO - Soil Date Received:08/03/16
Method:SW846 8260B Percent Solids:63.0
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
VOA Special List
CAS No.Compound Result RL MDL Units Q
74-87-3 Methyl Chloride ND 0.0064 0.0031 mg/kg
108-87-2 Methylcyclohexane ND 0.0064 0.0013 mg/kg
75-09-2 Methylene Chloride ND 0.013 0.0052 mg/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 0.032 0.014 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.0064 0.0014 mg/kg
91-20-3 Naphthalene ND 0.0064 0.0026 mg/kg
103-65-1 n-Propylbenzene ND 0.0064 0.0016 mg/kg
100-42-5 Styrene ND 0.0064 0.0013 mg/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 0.0064 0.0028 mg/kg
127-18-4 Tetrachloroethylene ND 0.0064 0.0017 mg/kg
108-88-3 Toluene ND 0.0064 0.0015 mg/kg
120-82-1 1,2,4-Trichlorobenzene ND 0.0064 0.0019 mg/kg
71-55-6 1,1,1-Trichloroethane ND 0.0064 0.0013 mg/kg
79-00-5 1,1,2-Trichloroethane ND 0.0064 0.0023 mg/kg
79-01-6 Trichloroethylene ND 0.0064 0.0015 mg/kg
75-69-4 Trichlorofluoromethane ND 0.0064 0.0024 mg/kg
95-63-6 1,2,4-Trimethylbenzene ND 0.0064 0.0013 mg/kg
108-67-8 1,3,5-Trimethylbenzene ND 0.0064 0.0013 mg/kg
75-01-4 Vinyl Chloride ND 0.0064 0.0022 mg/kg
1330-20-7 Xylene (total)ND 0.019 0.0037 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 103%75-124%
17060-07-0 1,2-Dichloroethane-D4 114%72-135%
2037-26-5 Toluene-D8 95%75-126%
460-00-4 4-Bromofluorobenzene 101%71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
19 of 66
FA35839T33.3
SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID:SW-S (11')
Lab Sample ID:FA35839-7T Date Sampled:08/01/16
Matrix:SO - Soil Date Received:08/03/16
Method:SW846 8270D SW846 3550C Percent Solids:63.0
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 X048316.D 1 08/12/16 MV 08/11/16 OP61449 SX2101
Run #2
Initial Weight Final Volume
Run #1 30.1 g 1.0 ml
Run #2
ABN Special List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 1.3 0.26 mg/kg
59-50-7 4-Chloro-3-methyl Phenol ND 0.26 0.040 mg/kg
95-57-8 2-Chlorophenol ND 0.26 0.033 mg/kg
120-83-2 2,4-Dichlorophenol ND 0.26 0.037 mg/kg
105-67-9 2,4-Dimethylphenol ND 0.26 0.032 mg/kg
51-28-5 2,4-Dinitrophenol ND 1.3 0.26 mg/kg
534-52-1 4,6-Dinitro-o-cresol ND 0.53 0.11 mg/kg
95-48-7 2-Methylphenol ND 0.26 0.028 mg/kg
3&4-Methylphenol ND 0.26 0.062 mg/kg
88-75-5 2-Nitrophenol ND 0.26 0.033 mg/kg
100-02-7 4-Nitrophenol ND 1.3 0.21 mg/kg
87-86-5 Pentachlorophenol ND 1.3 0.21 mg/kg
108-95-2 Phenol ND 0.26 0.031 mg/kg
88-06-2 2,4,6-Trichlorophenol ND 0.26 0.032 mg/kg
83-32-9 Acenaphthene ND 0.26 0.034 mg/kg
208-96-8 Acenaphthylene ND 0.26 0.033 mg/kg
120-12-7 Anthracene ND 0.26 0.038 mg/kg
56-55-3 Benzo(a)anthracene ND 0.26 0.030 mg/kg
50-32-8 Benzo(a)pyrene ND 0.26 0.028 mg/kg
205-99-2 Benzo(b)fluoranthene ND 0.26 0.033 mg/kg
191-24-2 Benzo(g,h,i)perylene ND 0.26 0.026 mg/kg
207-08-9 Benzo(k)fluoranthene ND 0.26 0.037 mg/kg
101-55-3 4-Bromophenyl phenyl ether ND 0.26 0.031 mg/kg
85-68-7 Butyl benzyl phthalate ND 0.26 0.053 mg/kg
106-47-8 4-Chloroaniline ND 0.26 0.037 mg/kg
111-91-1 bis(2-Chloroethoxy)methane ND 0.26 0.040 mg/kg
111-44-4 bis(2-Chloroethyl)ether ND 0.26 0.047 mg/kg
108-60-1 bis(2-Chloroisopropyl)ether ND 0.26 0.038 mg/kg
91-58-7 2-Chloronaphthalene ND 0.26 0.036 mg/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 0.26 0.033 mg/kg
218-01-9 Chrysene ND 0.26 0.036 mg/kg
53-70-3 Dibenzo(a,h)anthracene ND 0.26 0.028 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
20 of 66
FA35839T33.3
SGS Accutest
Report of Analysis Page 2 of 2
Client Sample ID:SW-S (11')
Lab Sample ID:FA35839-7T Date Sampled:08/01/16
Matrix:SO - Soil Date Received:08/03/16
Method:SW846 8270D SW846 3550C Percent Solids:63.0
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
ABN Special List
CAS No.Compound Result RL MDL Units Q
132-64-9 Dibenzofuran ND 0.26 0.033 mg/kg
91-94-1 3,3'-Dichlorobenzidine ND 0.26 0.029 mg/kg
84-66-2 Diethyl Phthalate ND 0.53 0.053 mg/kg
131-11-3 Dimethyl Phthalate ND 0.26 0.053 mg/kg
117-84-0 Di-n-octyl Phthalate ND 0.26 0.053 mg/kg
84-74-2 Di-n-butyl Phthalate ND 0.53 0.11 mg/kg
121-14-2 2,4-Dinitrotoluene ND 0.26 0.026 mg/kg
606-20-2 2,6-Dinitrotoluene ND 0.26 0.034 mg/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 0.53 0.053 mg/kg
206-44-0 Fluoranthene ND 0.26 0.032 mg/kg
86-73-7 Fluorene ND 0.26 0.034 mg/kg
118-74-1 Hexachlorobenzene ND 0.26 0.033 mg/kg
87-68-3 Hexachlorobutadiene ND 0.26 0.030 mg/kg
77-47-4 Hexachlorocyclopentadiene a ND 0.26 0.053 mg/kg
67-72-1 Hexachloroethane ND 0.26 0.031 mg/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 0.26 0.041 mg/kg
78-59-1 Isophorone ND 0.26 0.027 mg/kg
90-12-0 1-Methylnaphthalene ND 0.26 0.041 mg/kg
91-57-6 2-Methylnaphthalene ND 0.26 0.030 mg/kg
91-20-3 Naphthalene ND 0.26 0.040 mg/kg
98-95-3 Nitrobenzene ND 0.26 0.035 mg/kg
621-64-7 N-Nitrosodi-n-propylamine ND 0.26 0.028 mg/kg
86-30-6 N-Nitrosodiphenylamine ND 0.26 0.050 mg/kg
85-01-8 Phenanthrene ND 0.26 0.032 mg/kg
129-00-0 Pyrene ND 0.26 0.049 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 55%40-102%
4165-62-2 Phenol-d5 65%41-100%
118-79-6 2,4,6-Tribromophenol 64%42-108%
4165-60-0 Nitrobenzene-d5 60%40-105%
321-60-8 2-Fluorobiphenyl 60%43-107%
1718-51-0 Terphenyl-d14 74%45-119%
(a) Associated CCV outside control limits.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
21 of 66
FA35839T33.3
SGS Accutest
Report of Analysis Page 1 of 1
Client Sample ID:SW-S (11')
Lab Sample ID:FA35839-7T Date Sampled:08/01/16
Matrix:SO - Soil Date Received:08/03/16
Method:MADEP VPH REV 1.1 Percent Solids:63.0
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 UU016743.D 1 08/03/16 AH n/a n/a GUU853
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 5.15 g 5.1 ml 100 ul
Run #2
MADEP VPH List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.11 0.11 mg/kg
100-41-4 Ethylbenzene ND 0.22 0.11 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.22 0.11 mg/kg
91-20-3 Naphthalene ND 0.54 0.32 mg/kg
108-88-3 Toluene ND 0.22 0.11 mg/kg
m,p-Xylene ND 0.43 0.22 mg/kg
95-47-6 o-Xylene ND 0.22 0.11 mg/kg
C5- C8 Aliphatics (Unadj.)ND 11 3.8 mg/kg
C9- C12 Aliphatics (Unadj.)ND 11 3.8 mg/kg
C9- C10 Aromatics (Unadj.)ND 11 3.8 mg/kg
C5- C8 Aliphatics ND 11 3.8 mg/kg
C9- C12 Aliphatics ND 11 3.8 mg/kg
C9- C10 Aromatics ND 11 3.8 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 BFB 115%70-130%
460-00-4 BFB 119%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
22 of 66
FA35839T33.3
SGS Accutest
Report of Analysis Page 1 of 1
Client Sample ID:SW-S (11')
Lab Sample ID:FA35839-7T Date Sampled:08/01/16
Matrix:SO - Soil Date Received:08/03/16
Method:MADEP EPH REV 1.1 SW846 3546 Percent Solids:63.0
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 NN015933.D 1 08/17/16 FS 08/11/16 OP61448 GNN787
Run #2
Initial Weight Final Volume
Run #1 19.9 g 2.0 ml
Run #2
MAEPH List
CAS No.Compound Result RL MDL Units Q
83-32-9 Acenaphthene ND 0.32 0.16 mg/kg
208-96-8 Acenaphthylene ND 0.32 0.16 mg/kg
120-12-7 Anthracene ND 0.32 0.16 mg/kg
56-55-3 Benzo(a)anthracene ND 0.32 0.16 mg/kg
50-32-8 Benzo(a)pyrene ND 0.32 0.16 mg/kg
205-99-2 Benzo(b)fluoranthene ND 0.32 0.16 mg/kg
191-24-2 Benzo(g,h,i)perylene ND 0.32 0.16 mg/kg
207-08-9 Benzo(k)fluoranthene ND 0.32 0.16 mg/kg
218-01-9 Chrysene ND 0.32 0.16 mg/kg
53-70-3 Dibenzo(a,h)anthracene ND 0.32 0.16 mg/kg
206-44-0 Fluoranthene ND 0.32 0.16 mg/kg
86-73-7 Fluorene ND 0.32 0.16 mg/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 0.32 0.16 mg/kg
91-57-6 2-Methylnaphthalene ND 0.32 0.16 mg/kg
91-20-3 Naphthalene ND 0.32 0.16 mg/kg
85-01-8 Phenanthrene ND 0.32 0.16 mg/kg
129-00-0 Pyrene ND 0.32 0.16 mg/kg
C11-C22 Aromatics (Unadj.)ND 16 12 mg/kg
C11-C22 Aromatics ND 16 12 mg/kg
C9-C18 Aliphatics ND 16 8.0 mg/kg
C19-C36 Aliphatics ND 16 8.0 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
3386-33-2 1-Chlorooctadecane 63%40-140%
580-13-2 2-Bromonaphthalene 88%40-140%
84-15-1 o-Terphenyl 62%40-140%
321-60-8 2-Fluorobiphenyl 78%40-140%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
23 of 66
FA35839T33.3
SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID:BOTTOM (13')
Lab Sample ID:FA35839-9T Date Sampled:08/01/16
Matrix:SO - Soil Date Received:08/03/16
Method:SW846 8260B Percent Solids:71.5
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 Y30283.D 1 08/03/16 AD n/a n/a VY1220
Run #2
Initial Weight Final Volume
Run #1 5.50 g 5.0 ml
Run #2
VOA Special List
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 0.064 0.013 mg/kg
71-43-2 Benzene ND 0.0064 0.0016 mg/kg
75-27-4 Bromodichloromethane ND 0.0064 0.0013 mg/kg
75-25-2 Bromoform ND 0.0064 0.0013 mg/kg
78-93-3 2-Butanone (MEK)ND 0.032 0.012 mg/kg
104-51-8 n-Butylbenzene ND 0.0064 0.0013 mg/kg
75-15-0 Carbon Disulfide ND 0.0064 0.0013 mg/kg
56-23-5 Carbon Tetrachloride ND 0.0064 0.0023 mg/kg
108-90-7 Chlorobenzene ND 0.0064 0.0013 mg/kg
75-00-3 Chloroethane ND 0.0064 0.0025 mg/kg
67-66-3 Chloroform ND 0.0064 0.0016 mg/kg
110-82-7 Cyclohexane ND 0.0064 0.0016 mg/kg
124-48-1 Dibromochloromethane ND 0.0064 0.0013 mg/kg
96-12-8 1,2-Dibromo-3-chloropropane ND 0.0064 0.0028 mg/kg
106-93-4 1,2-Dibromoethane ND 0.0064 0.0013 mg/kg
75-71-8 Dichlorodifluoromethane ND 0.0064 0.0032 mg/kg
95-50-1 1,2-Dichlorobenzene ND 0.0064 0.0013 mg/kg
541-73-1 1,3-Dichlorobenzene ND 0.0064 0.0013 mg/kg
106-46-7 1,4-Dichlorobenzene ND 0.0064 0.0013 mg/kg
75-34-3 1,1-Dichloroethane ND 0.0064 0.0021 mg/kg
107-06-2 1,2-Dichloroethane ND 0.0064 0.0013 mg/kg
75-35-4 1,1-Dichloroethylene ND 0.0064 0.0013 mg/kg
156-59-2 cis-1,2-Dichloroethylene ND 0.0064 0.0015 mg/kg
156-60-5 trans-1,2-Dichloroethylene ND 0.0064 0.0019 mg/kg
78-87-5 1,2-Dichloropropane ND 0.0064 0.0020 mg/kg
10061-01-5 cis-1,3-Dichloropropene ND 0.0064 0.0024 mg/kg
10061-02-6 trans-1,3-Dichloropropene ND 0.0064 0.0013 mg/kg
100-41-4 Ethylbenzene ND 0.0064 0.0014 mg/kg
591-78-6 2-Hexanone ND 0.032 0.011 mg/kg
98-82-8 Isopropylbenzene ND 0.0064 0.0018 mg/kg
79-20-9 Methyl Acetate ND 0.032 0.011 mg/kg
74-83-9 Methyl Bromide ND 0.0064 0.0033 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:BOTTOM (13')
Lab Sample ID:FA35839-9T Date Sampled:08/01/16
Matrix:SO - Soil Date Received:08/03/16
Method:SW846 8260B Percent Solids:71.5
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
VOA Special List
CAS No.Compound Result RL MDL Units Q
74-87-3 Methyl Chloride ND 0.0064 0.0031 mg/kg
108-87-2 Methylcyclohexane ND 0.0064 0.0013 mg/kg
75-09-2 Methylene Chloride ND 0.013 0.0051 mg/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 0.032 0.014 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.0064 0.0014 mg/kg
91-20-3 Naphthalene ND 0.0064 0.0025 mg/kg
103-65-1 n-Propylbenzene ND 0.0064 0.0016 mg/kg
100-42-5 Styrene ND 0.0064 0.0013 mg/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 0.0064 0.0028 mg/kg
127-18-4 Tetrachloroethylene ND 0.0064 0.0017 mg/kg
108-88-3 Toluene ND 0.0064 0.0014 mg/kg
120-82-1 1,2,4-Trichlorobenzene ND 0.0064 0.0019 mg/kg
71-55-6 1,1,1-Trichloroethane ND 0.0064 0.0013 mg/kg
79-00-5 1,1,2-Trichloroethane ND 0.0064 0.0023 mg/kg
79-01-6 Trichloroethylene ND 0.0064 0.0015 mg/kg
75-69-4 Trichlorofluoromethane ND 0.0064 0.0024 mg/kg
95-63-6 1,2,4-Trimethylbenzene ND 0.0064 0.0013 mg/kg
108-67-8 1,3,5-Trimethylbenzene ND 0.0064 0.0013 mg/kg
75-01-4 Vinyl Chloride ND 0.0064 0.0021 mg/kg
1330-20-7 Xylene (total)ND 0.019 0.0036 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 103%75-124%
17060-07-0 1,2-Dichloroethane-D4 116%72-135%
2037-26-5 Toluene-D8 98%75-126%
460-00-4 4-Bromofluorobenzene 100%71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 2
Client Sample ID:BOTTOM (13')
Lab Sample ID:FA35839-9T Date Sampled:08/01/16
Matrix:SO - Soil Date Received:08/03/16
Method:SW846 8270D SW846 3550C Percent Solids:71.5
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 X048317.D 1 08/12/16 MV 08/11/16 OP61449 SX2101
Run #2
Initial Weight Final Volume
Run #1 30.3 g 1.0 ml
Run #2
ABN Special List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 1.2 0.23 mg/kg
59-50-7 4-Chloro-3-methyl Phenol ND 0.23 0.035 mg/kg
95-57-8 2-Chlorophenol ND 0.23 0.029 mg/kg
120-83-2 2,4-Dichlorophenol ND 0.23 0.032 mg/kg
105-67-9 2,4-Dimethylphenol ND 0.23 0.028 mg/kg
51-28-5 2,4-Dinitrophenol ND 1.2 0.23 mg/kg
534-52-1 4,6-Dinitro-o-cresol ND 0.46 0.092 mg/kg
95-48-7 2-Methylphenol ND 0.23 0.025 mg/kg
3&4-Methylphenol ND 0.23 0.054 mg/kg
88-75-5 2-Nitrophenol ND 0.23 0.029 mg/kg
100-02-7 4-Nitrophenol ND 1.2 0.18 mg/kg
87-86-5 Pentachlorophenol ND 1.2 0.18 mg/kg
108-95-2 Phenol ND 0.23 0.027 mg/kg
88-06-2 2,4,6-Trichlorophenol ND 0.23 0.028 mg/kg
83-32-9 Acenaphthene ND 0.23 0.030 mg/kg
208-96-8 Acenaphthylene ND 0.23 0.029 mg/kg
120-12-7 Anthracene ND 0.23 0.033 mg/kg
56-55-3 Benzo(a)anthracene ND 0.23 0.027 mg/kg
50-32-8 Benzo(a)pyrene ND 0.23 0.025 mg/kg
205-99-2 Benzo(b)fluoranthene ND 0.23 0.029 mg/kg
191-24-2 Benzo(g,h,i)perylene ND 0.23 0.023 mg/kg
207-08-9 Benzo(k)fluoranthene ND 0.23 0.032 mg/kg
101-55-3 4-Bromophenyl phenyl ether ND 0.23 0.027 mg/kg
85-68-7 Butyl benzyl phthalate ND 0.23 0.046 mg/kg
106-47-8 4-Chloroaniline ND 0.23 0.032 mg/kg
111-91-1 bis(2-Chloroethoxy)methane ND 0.23 0.035 mg/kg
111-44-4 bis(2-Chloroethyl)ether ND 0.23 0.041 mg/kg
108-60-1 bis(2-Chloroisopropyl)ether ND 0.23 0.033 mg/kg
91-58-7 2-Chloronaphthalene ND 0.23 0.032 mg/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 0.23 0.029 mg/kg
218-01-9 Chrysene ND 0.23 0.031 mg/kg
53-70-3 Dibenzo(a,h)anthracene ND 0.23 0.025 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:BOTTOM (13')
Lab Sample ID:FA35839-9T Date Sampled:08/01/16
Matrix:SO - Soil Date Received:08/03/16
Method:SW846 8270D SW846 3550C Percent Solids:71.5
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
ABN Special List
CAS No.Compound Result RL MDL Units Q
132-64-9 Dibenzofuran ND 0.23 0.029 mg/kg
91-94-1 3,3'-Dichlorobenzidine ND 0.23 0.025 mg/kg
84-66-2 Diethyl Phthalate ND 0.46 0.046 mg/kg
131-11-3 Dimethyl Phthalate ND 0.23 0.046 mg/kg
117-84-0 Di-n-octyl Phthalate ND 0.23 0.046 mg/kg
84-74-2 Di-n-butyl Phthalate ND 0.46 0.092 mg/kg
121-14-2 2,4-Dinitrotoluene ND 0.23 0.023 mg/kg
606-20-2 2,6-Dinitrotoluene ND 0.23 0.029 mg/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 0.46 0.046 mg/kg
206-44-0 Fluoranthene ND 0.23 0.028 mg/kg
86-73-7 Fluorene ND 0.23 0.029 mg/kg
118-74-1 Hexachlorobenzene ND 0.23 0.028 mg/kg
87-68-3 Hexachlorobutadiene ND 0.23 0.026 mg/kg
77-47-4 Hexachlorocyclopentadiene a ND 0.23 0.046 mg/kg
67-72-1 Hexachloroethane ND 0.23 0.027 mg/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 0.23 0.036 mg/kg
78-59-1 Isophorone ND 0.23 0.024 mg/kg
90-12-0 1-Methylnaphthalene ND 0.23 0.036 mg/kg
91-57-6 2-Methylnaphthalene ND 0.23 0.026 mg/kg
91-20-3 Naphthalene ND 0.23 0.035 mg/kg
98-95-3 Nitrobenzene ND 0.23 0.030 mg/kg
621-64-7 N-Nitrosodi-n-propylamine ND 0.23 0.024 mg/kg
86-30-6 N-Nitrosodiphenylamine ND 0.23 0.044 mg/kg
85-01-8 Phenanthrene ND 0.23 0.028 mg/kg
129-00-0 Pyrene ND 0.23 0.043 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 70%40-102%
4165-62-2 Phenol-d5 82%41-100%
118-79-6 2,4,6-Tribromophenol 76%42-108%
4165-60-0 Nitrobenzene-d5 75%40-105%
321-60-8 2-Fluorobiphenyl 74%43-107%
1718-51-0 Terphenyl-d14 89%45-119%
(a) Associated CCV outside control limits.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 1
Client Sample ID:BOTTOM (13')
Lab Sample ID:FA35839-9T Date Sampled:08/01/16
Matrix:SO - Soil Date Received:08/03/16
Method:MADEP VPH REV 1.1 Percent Solids:71.5
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 UU016745.D 1 08/03/16 AH n/a n/a GUU853
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 5.15 g 5.1 ml 100 ul
Run #2
MADEP VPH List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.089 0.089 mg/kg
100-41-4 Ethylbenzene ND 0.18 0.089 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.18 0.089 mg/kg
91-20-3 Naphthalene ND 0.45 0.27 mg/kg
108-88-3 Toluene ND 0.18 0.089 mg/kg
m,p-Xylene ND 0.36 0.18 mg/kg
95-47-6 o-Xylene ND 0.18 0.089 mg/kg
C5- C8 Aliphatics (Unadj.)ND 8.9 3.1 mg/kg
C9- C12 Aliphatics (Unadj.)ND 8.9 3.1 mg/kg
C9- C10 Aromatics (Unadj.)ND 8.9 3.1 mg/kg
C5- C8 Aliphatics ND 8.9 3.1 mg/kg
C9- C12 Aliphatics ND 8.9 3.1 mg/kg
C9- C10 Aromatics ND 8.9 3.1 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 BFB 129%70-130%
460-00-4 BFB 132% a 70-130%
(a) Outside control limits; however, sample is ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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FA35839T33.4
SGS Accutest
Report of Analysis Page 1 of 1
Client Sample ID:BOTTOM (13')
Lab Sample ID:FA35839-9T Date Sampled:08/01/16
Matrix:SO - Soil Date Received:08/03/16
Method:MADEP EPH REV 1.1 SW846 3546 Percent Solids:71.5
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 NN015934.D 1 08/17/16 FS 08/11/16 OP61448 GNN787
Run #2
Initial Weight Final Volume
Run #1 19.9 g 2.0 ml
Run #2
MAEPH List
CAS No.Compound Result RL MDL Units Q
83-32-9 Acenaphthene ND 0.28 0.14 mg/kg
208-96-8 Acenaphthylene ND 0.28 0.14 mg/kg
120-12-7 Anthracene ND 0.28 0.14 mg/kg
56-55-3 Benzo(a)anthracene ND 0.28 0.14 mg/kg
50-32-8 Benzo(a)pyrene ND 0.28 0.14 mg/kg
205-99-2 Benzo(b)fluoranthene ND 0.28 0.14 mg/kg
191-24-2 Benzo(g,h,i)perylene ND 0.28 0.14 mg/kg
207-08-9 Benzo(k)fluoranthene ND 0.28 0.14 mg/kg
218-01-9 Chrysene ND 0.28 0.14 mg/kg
53-70-3 Dibenzo(a,h)anthracene ND 0.28 0.14 mg/kg
206-44-0 Fluoranthene ND 0.28 0.14 mg/kg
86-73-7 Fluorene ND 0.28 0.14 mg/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 0.28 0.14 mg/kg
91-57-6 2-Methylnaphthalene ND 0.28 0.14 mg/kg
91-20-3 Naphthalene ND 0.28 0.14 mg/kg
85-01-8 Phenanthrene ND 0.28 0.14 mg/kg
129-00-0 Pyrene ND 0.28 0.14 mg/kg
C11-C22 Aromatics (Unadj.)ND 14 11 mg/kg
C11-C22 Aromatics ND 14 11 mg/kg
C9-C18 Aliphatics ND 14 7.0 mg/kg
C19-C36 Aliphatics ND 14 7.0 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
3386-33-2 1-Chlorooctadecane 66%40-140%
580-13-2 2-Bromonaphthalene 95%40-140%
84-15-1 o-Terphenyl 68%40-140%
321-60-8 2-Fluorobiphenyl 84%40-140%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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SGS Accutest
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Southeast
Section 4
30 of 66
FA35839T4
FA35839T: Chain of Custody
Page 1 of 5
31 of 66
FA35839T44.1
FA35839T: Chain of Custody
Page 2 of 5
32 of 66
FA35839T44.1
FA35839T: Chain of Custody
Page 3 of 5
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FA35839T44.1
Job Change FA35839
Requested Date: 8/9/2016 Received Date: 8/3/2016
Account Name: GRI (Geological Resources Inc.) Due Date: 8/10/2016
Project Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC Deliverable: COMMB
CSR: MunaM TAT (Days): 7
============================================================================================================= Sample #: FA35839-1 thru 4 Change:
Per client request analyze samples for V8260BTX.
=============================================================================================================
Above Changes Per: Corey Buchanan Date/Time: 8/9/2016 10:01:13 AM
This Change Order is confirmation of the revisions, previously discussed with the SGS Accutest Client Service Representative.
Page 1 of 1
FA35839T: Chain of Custody
Page 4 of 5
34 of 66
FA35839T44.1
Job Change FA35839
Requested Date: 8/9/2016 Received Date: 8/3/2016
Account Name: GRI (Geological Resources Inc.) Due Date: 8/10/2016
Project Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC Deliverable: COMMB
CSR: MunaM TAT (Days): 7
============================================================================================================= Sample #: FA35839-5, 6, 7, 9 Change:
Per client request analyze samples for V8260SL, VMAVPH,
AB8270SL and BMAEPH.
=============================================================================================================
Above Changes Per: Corey Buchanan Date/Time: 8/10/2016 3:03:57 PM
This Change Order is confirmation of the revisions, previously discussed with the SGS Accutest Client Service Representative.
Page 1 of 1
FA35839T: Chain of Custody
Page 5 of 5
35 of 66
FA35839T44.1
SGS Accutest
GC/MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Southeast
Section 5
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FA35839T5
Method Blank Summary Page 1 of 2
Job Number:FA35839T
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VY1220-MB Y30276.D 1 08/03/16 AD n/a n/a VY1220
The QC reported here applies to the following samples:Method: SW846 8260B
FA35839-7T, FA35839-9T
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 50 10 ug/kg
71-43-2 Benzene ND 5.0 1.3 ug/kg
75-27-4 Bromodichloromethane ND 5.0 1.0 ug/kg
75-25-2 Bromoform ND 5.0 1.0 ug/kg
78-93-3 2-Butanone (MEK)ND 25 9.1 ug/kg
104-51-8 n-Butylbenzene ND 5.0 1.0 ug/kg
75-15-0 Carbon Disulfide ND 5.0 1.0 ug/kg
56-23-5 Carbon Tetrachloride ND 5.0 1.8 ug/kg
108-90-7 Chlorobenzene ND 5.0 1.0 ug/kg
75-00-3 Chloroethane ND 5.0 2.0 ug/kg
67-66-3 Chloroform ND 5.0 1.2 ug/kg
110-82-7 Cyclohexane ND 5.0 1.2 ug/kg
124-48-1 Dibromochloromethane ND 5.0 1.0 ug/kg
96-12-8 1,2-Dibromo-3-chloropropane ND 5.0 2.2 ug/kg
106-93-4 1,2-Dibromoethane ND 5.0 1.0 ug/kg
75-71-8 Dichlorodifluoromethane ND 5.0 2.5 ug/kg
95-50-1 1,2-Dichlorobenzene ND 5.0 1.0 ug/kg
541-73-1 1,3-Dichlorobenzene ND 5.0 1.0 ug/kg
106-46-7 1,4-Dichlorobenzene ND 5.0 1.0 ug/kg
75-34-3 1,1-Dichloroethane ND 5.0 1.7 ug/kg
107-06-2 1,2-Dichloroethane ND 5.0 1.0 ug/kg
75-35-4 1,1-Dichloroethylene ND 5.0 1.0 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.2 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.5 ug/kg
78-87-5 1,2-Dichloropropane ND 5.0 1.6 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.9 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.0 ug/kg
100-41-4 Ethylbenzene ND 5.0 1.1 ug/kg
591-78-6 2-Hexanone ND 25 8.7 ug/kg
98-82-8 Isopropylbenzene ND 5.0 1.4 ug/kg
79-20-9 Methyl Acetate ND 25 8.6 ug/kg
74-83-9 Methyl Bromide ND 5.0 2.6 ug/kg
74-87-3 Methyl Chloride ND 5.0 2.4 ug/kg
108-87-2 Methylcyclohexane ND 5.0 1.0 ug/kg
75-09-2 Methylene Chloride 7.7 10 4.0 ug/kg J
108-10-1 4-Methyl-2-pentanone (MIBK)ND 25 11 ug/kg
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FA35839T55.1.1
Method Blank Summary Page 2 of 2
Job Number:FA35839T
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VY1220-MB Y30276.D 1 08/03/16 AD n/a n/a VY1220
The QC reported here applies to the following samples:Method: SW846 8260B
FA35839-7T, FA35839-9T
CAS No.Compound Result RL MDL Units Q
1634-04-4 Methyl Tert Butyl Ether ND 5.0 1.1 ug/kg
91-20-3 Naphthalene ND 5.0 2.0 ug/kg
103-65-1 n-Propylbenzene ND 5.0 1.2 ug/kg
100-42-5 Styrene ND 5.0 1.0 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 2.2 ug/kg
127-18-4 Tetrachloroethylene ND 5.0 1.3 ug/kg
108-88-3 Toluene ND 5.0 1.1 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.5 ug/kg
71-55-6 1,1,1-Trichloroethane ND 5.0 1.0 ug/kg
79-00-5 1,1,2-Trichloroethane ND 5.0 1.8 ug/kg
79-01-6 Trichloroethylene ND 5.0 1.2 ug/kg
75-69-4 Trichlorofluoromethane ND 5.0 1.9 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 5.0 1.0 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 5.0 1.0 ug/kg
75-01-4 Vinyl Chloride ND 5.0 1.7 ug/kg
1330-20-7 Xylene (total)ND 15 2.9 ug/kg
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 108%75-124%
17060-07-0 1,2-Dichloroethane-D4 111%72-135%
2037-26-5 Toluene-D8 100%75-126%
460-00-4 4-Bromofluorobenzene 98%71-133%
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FA35839T55.1.1
Method Blank Summary Page 1 of 2
Job Number:FA35839T
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VF2712-MB F0078935.D 1 08/03/16 EP n/a n/a VF2712
The QC reported here applies to the following samples:Method: SW846 8260B
FA35839-5T, FA35839-6T
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 50 10 ug/kg
71-43-2 Benzene ND 5.0 1.3 ug/kg
75-27-4 Bromodichloromethane ND 5.0 1.0 ug/kg
75-25-2 Bromoform ND 5.0 1.0 ug/kg
78-93-3 2-Butanone (MEK)ND 25 9.1 ug/kg
104-51-8 n-Butylbenzene ND 5.0 1.0 ug/kg
75-15-0 Carbon Disulfide ND 5.0 1.0 ug/kg
56-23-5 Carbon Tetrachloride ND 5.0 1.8 ug/kg
108-90-7 Chlorobenzene ND 5.0 1.0 ug/kg
75-00-3 Chloroethane ND 5.0 2.0 ug/kg
67-66-3 Chloroform ND 5.0 1.2 ug/kg
110-82-7 Cyclohexane ND 5.0 1.2 ug/kg
124-48-1 Dibromochloromethane ND 5.0 1.0 ug/kg
96-12-8 1,2-Dibromo-3-chloropropane ND 5.0 2.2 ug/kg
106-93-4 1,2-Dibromoethane ND 5.0 1.0 ug/kg
75-71-8 Dichlorodifluoromethane ND 5.0 2.5 ug/kg
95-50-1 1,2-Dichlorobenzene ND 5.0 1.0 ug/kg
541-73-1 1,3-Dichlorobenzene ND 5.0 1.0 ug/kg
106-46-7 1,4-Dichlorobenzene ND 5.0 1.0 ug/kg
75-34-3 1,1-Dichloroethane ND 5.0 1.7 ug/kg
107-06-2 1,2-Dichloroethane ND 5.0 1.0 ug/kg
75-35-4 1,1-Dichloroethylene ND 5.0 1.0 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.2 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.5 ug/kg
78-87-5 1,2-Dichloropropane ND 5.0 1.6 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.9 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.0 ug/kg
100-41-4 Ethylbenzene ND 5.0 1.1 ug/kg
591-78-6 2-Hexanone ND 25 8.7 ug/kg
98-82-8 Isopropylbenzene ND 5.0 1.4 ug/kg
79-20-9 Methyl Acetate ND 25 8.6 ug/kg
74-83-9 Methyl Bromide ND 5.0 2.6 ug/kg
74-87-3 Methyl Chloride ND 5.0 2.4 ug/kg
108-87-2 Methylcyclohexane ND 5.0 1.0 ug/kg
75-09-2 Methylene Chloride 7.5 10 4.0 ug/kg J
108-10-1 4-Methyl-2-pentanone (MIBK)ND 25 11 ug/kg
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FA35839T55.1.2
Method Blank Summary Page 2 of 2
Job Number:FA35839T
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VF2712-MB F0078935.D 1 08/03/16 EP n/a n/a VF2712
The QC reported here applies to the following samples:Method: SW846 8260B
FA35839-5T, FA35839-6T
CAS No.Compound Result RL MDL Units Q
1634-04-4 Methyl Tert Butyl Ether ND 5.0 1.1 ug/kg
91-20-3 Naphthalene ND 5.0 2.0 ug/kg
103-65-1 n-Propylbenzene ND 5.0 1.2 ug/kg
100-42-5 Styrene ND 5.0 1.0 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 2.2 ug/kg
127-18-4 Tetrachloroethylene ND 5.0 1.3 ug/kg
108-88-3 Toluene ND 5.0 1.1 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.5 ug/kg
71-55-6 1,1,1-Trichloroethane ND 5.0 1.0 ug/kg
79-00-5 1,1,2-Trichloroethane ND 5.0 1.8 ug/kg
79-01-6 Trichloroethylene ND 5.0 1.2 ug/kg
75-69-4 Trichlorofluoromethane ND 5.0 1.9 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 5.0 1.0 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 5.0 1.0 ug/kg
75-01-4 Vinyl Chloride ND 5.0 1.7 ug/kg
1330-20-7 Xylene (total)ND 15 2.9 ug/kg
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 104%75-124%
17060-07-0 1,2-Dichloroethane-D4 107%72-135%
2037-26-5 Toluene-D8 99%75-126%
460-00-4 4-Bromofluorobenzene 101%71-133%
40 of 66
FA35839T55.1.2
Blank Spike Summary Page 1 of 2
Job Number:FA35839T
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VY1220-BS Y30275.D 1 08/03/16 AD n/a n/a VY1220
The QC reported here applies to the following samples:Method: SW846 8260B
FA35839-7T, FA35839-9T
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
67-64-1 Acetone 250 239 96 61-152
71-43-2 Benzene 50 53.0 106 76-126
75-27-4 Bromodichloromethane 50 56.8 114 74-130
75-25-2 Bromoform 50 55.3 111 76-127
78-93-3 2-Butanone (MEK)250 234 94 75-137
104-51-8 n-Butylbenzene 50 49.2 98 71-128
75-15-0 Carbon Disulfide 50 48.1 96 72-122
56-23-5 Carbon Tetrachloride 50 56.7 113 78-133
108-90-7 Chlorobenzene 50 56.0 112 81-129
75-00-3 Chloroethane 50 49.6 99 68-133
67-66-3 Chloroform 50 54.0 108 72-123
110-82-7 Cyclohexane 50 49.4 99 73-126
124-48-1 Dibromochloromethane 50 56.7 113 76-127
96-12-8 1,2-Dibromo-3-chloropropane 50 51.4 103 70-137
106-93-4 1,2-Dibromoethane 50 56.2 112 77-126
75-71-8 Dichlorodifluoromethane 50 41.4 83 68-168
95-50-1 1,2-Dichlorobenzene 50 53.2 106 80-129
541-73-1 1,3-Dichlorobenzene 50 52.7 105 81-129
106-46-7 1,4-Dichlorobenzene 50 53.1 106 76-130
75-34-3 1,1-Dichloroethane 50 56.4 113 73-125
107-06-2 1,2-Dichloroethane 50 54.9 110 74-128
75-35-4 1,1-Dichloroethylene 50 55.3 111 81-136
156-59-2 cis-1,2-Dichloroethylene 50 52.3 105 74-126
156-60-5 trans-1,2-Dichloroethylene 50 58.6 117 70-127
78-87-5 1,2-Dichloropropane 50 54.5 109 74-125
10061-01-5 cis-1,3-Dichloropropene 50 55.6 111 80-123
10061-02-6 trans-1,3-Dichloropropene 50 61.5 123 75-131
100-41-4 Ethylbenzene 50 52.0 104 77-123
591-78-6 2-Hexanone 250 248 99 72-133
98-82-8 Isopropylbenzene 50 52.6 105 80-136
79-20-9 Methyl Acetate 250 251 100 67-137
74-83-9 Methyl Bromide 50 47.8 96 65-139
74-87-3 Methyl Chloride 50 45.0 90 71-144
108-87-2 Methylcyclohexane 50 50.5 101 75-128
75-09-2 Methylene Chloride 50 62.3 125 74-137
108-10-1 4-Methyl-2-pentanone (MIBK)250 254 102 76-132
* = Outside of Control Limits.
41 of 66
FA35839T55.2.1
Blank Spike Summary Page 2 of 2
Job Number:FA35839T
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VY1220-BS Y30275.D 1 08/03/16 AD n/a n/a VY1220
The QC reported here applies to the following samples:Method: SW846 8260B
FA35839-7T, FA35839-9T
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
1634-04-4 Methyl Tert Butyl Ether 50 53.1 106 77-120
91-20-3 Naphthalene 50 57.3 115 79-129
103-65-1 n-Propylbenzene 50 53.5 107 80-135
100-42-5 Styrene 50 56.3 113 78-125
79-34-5 1,1,2,2-Tetrachloroethane 50 50.2 100 71-126
127-18-4 Tetrachloroethylene 50 54.4 109 79-130
108-88-3 Toluene 50 53.3 107 76-124
120-82-1 1,2,4-Trichlorobenzene 50 50.8 102 78-130
71-55-6 1,1,1-Trichloroethane 50 51.7 103 70-129
79-00-5 1,1,2-Trichloroethane 50 54.3 109 74-124
79-01-6 Trichloroethylene 50 51.6 103 75-128
75-69-4 Trichlorofluoromethane 50 49.9 100 73-145
95-63-6 1,2,4-Trimethylbenzene 50 51.8 104 74-123
108-67-8 1,3,5-Trimethylbenzene 50 50.8 102 73-122
75-01-4 Vinyl Chloride 50 44.6 89 76-141
1330-20-7 Xylene (total)150 157 105 80-129
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 103%75-124%
17060-07-0 1,2-Dichloroethane-D4 109%72-135%
2037-26-5 Toluene-D8 99%75-126%
460-00-4 4-Bromofluorobenzene 98%71-133%
* = Outside of Control Limits.
42 of 66
FA35839T55.2.1
Blank Spike Summary Page 1 of 2
Job Number:FA35839T
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VF2712-BS F0078934.D 1 08/03/16 EP n/a n/a VF2712
The QC reported here applies to the following samples:Method: SW846 8260B
FA35839-5T, FA35839-6T
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
67-64-1 Acetone 250 245 98 61-152
71-43-2 Benzene 50 53.6 107 76-126
75-27-4 Bromodichloromethane 50 56.9 114 74-130
75-25-2 Bromoform 50 55.9 112 76-127
78-93-3 2-Butanone (MEK)250 272 109 75-137
104-51-8 n-Butylbenzene 50 52.8 106 71-128
75-15-0 Carbon Disulfide 50 45.6 91 72-122
56-23-5 Carbon Tetrachloride 50 52.9 106 78-133
108-90-7 Chlorobenzene 50 53.3 107 81-129
75-00-3 Chloroethane 50 49.8 100 68-133
67-66-3 Chloroform 50 53.9 108 72-123
110-82-7 Cyclohexane 50 51.7 103 73-126
124-48-1 Dibromochloromethane 50 55.6 111 76-127
96-12-8 1,2-Dibromo-3-chloropropane 50 58.8 118 70-137
106-93-4 1,2-Dibromoethane 50 53.8 108 77-126
75-71-8 Dichlorodifluoromethane 50 45.6 91 68-168
95-50-1 1,2-Dichlorobenzene 50 54.4 109 80-129
541-73-1 1,3-Dichlorobenzene 50 54.3 109 81-129
106-46-7 1,4-Dichlorobenzene 50 52.1 104 76-130
75-34-3 1,1-Dichloroethane 50 57.2 114 73-125
107-06-2 1,2-Dichloroethane 50 59.1 118 74-128
75-35-4 1,1-Dichloroethylene 50 51.7 103 81-136
156-59-2 cis-1,2-Dichloroethylene 50 49.8 100 74-126
156-60-5 trans-1,2-Dichloroethylene 50 57.1 114 70-127
78-87-5 1,2-Dichloropropane 50 55.9 112 74-125
10061-01-5 cis-1,3-Dichloropropene 50 59.1 118 80-123
10061-02-6 trans-1,3-Dichloropropene 50 62.1 124 75-131
100-41-4 Ethylbenzene 50 52.3 105 77-123
591-78-6 2-Hexanone 250 272 109 72-133
98-82-8 Isopropylbenzene 50 55.4 111 80-136
79-20-9 Methyl Acetate 250 266 106 67-137
74-83-9 Methyl Bromide 50 49.4 99 65-139
74-87-3 Methyl Chloride 50 48.5 97 71-144
108-87-2 Methylcyclohexane 50 50.9 102 75-128
75-09-2 Methylene Chloride 50 64.0 128 74-137
108-10-1 4-Methyl-2-pentanone (MIBK)250 292 117 76-132
* = Outside of Control Limits.
43 of 66
FA35839T55.2.2
Blank Spike Summary Page 2 of 2
Job Number:FA35839T
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VF2712-BS F0078934.D 1 08/03/16 EP n/a n/a VF2712
The QC reported here applies to the following samples:Method: SW846 8260B
FA35839-5T, FA35839-6T
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
1634-04-4 Methyl Tert Butyl Ether 50 55.7 111 77-120
91-20-3 Naphthalene 50 56.6 113 79-129
103-65-1 n-Propylbenzene 50 51.4 103 80-135
100-42-5 Styrene 50 54.7 109 78-125
79-34-5 1,1,2,2-Tetrachloroethane 50 57.3 115 71-126
127-18-4 Tetrachloroethylene 50 50.4 101 79-130
108-88-3 Toluene 50 53.1 106 76-124
120-82-1 1,2,4-Trichlorobenzene 50 42.4 85 78-130
71-55-6 1,1,1-Trichloroethane 50 49.5 99 70-129
79-00-5 1,1,2-Trichloroethane 50 57.1 114 74-124
79-01-6 Trichloroethylene 50 52.5 105 75-128
75-69-4 Trichlorofluoromethane 50 48.6 97 73-145
95-63-6 1,2,4-Trimethylbenzene 50 54.1 108 74-123
108-67-8 1,3,5-Trimethylbenzene 50 54.5 109 73-122
75-01-4 Vinyl Chloride 50 45.5 91 76-141
1330-20-7 Xylene (total)150 157 105 80-129
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 103%75-124%
17060-07-0 1,2-Dichloroethane-D4 105%72-135%
2037-26-5 Toluene-D8 98%75-126%
460-00-4 4-Bromofluorobenzene 99%71-133%
* = Outside of Control Limits.
44 of 66
FA35839T55.2.2
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA35839T
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA35831-8MS F0078939.D 1 08/03/16 EP n/a n/a VF2712
FA35831-8MSD F0078940.D 1 08/03/16 EP n/a n/a VF2712
FA35831-8 F0078936.D 1 08/03/16 EP n/a n/a VF2712
The QC reported here applies to the following samples:Method: SW846 8260B
FA35839-5T, FA35839-6T
FA35831-8 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
67-64-1 Acetone 7100 U 35300 33700 95 35300 32000 91 5 61-152/27
71-43-2 Benzene 710 U 7060 6590 93 7060 6610 94 0 76-126/26
75-27-4 Bromodichloromethane 710 U 7060 6770 96 7060 6740 95 0 74-130/25
75-25-2 Bromoform 710 U 7060 7750 110 7060 7930 112 2 76-127/26
78-93-3 2-Butanone (MEK)3500 U 35300 33000 93 35300 31800 90 4 75-137/25
104-51-8 n-Butylbenzene 1230 7060 7640 91 7060 7470 88 2 71-128/35
75-15-0 Carbon Disulfide 710 U 7060 5840 83 7060 5710 81 2 72-122/29
56-23-5 Carbon Tetrachloride 710 U 7060 6220 88 7060 6200 88 0 78-133/29
108-90-7 Chlorobenzene 710 U 7060 6930 98 7060 6970 99 1 81-129/29
75-00-3 Chloroethane 710 U 7060 3380 48*7060 3130 44*8 68-133/29
67-66-3 Chloroform 710 U 7060 6870 97 7060 6560 93 5 72-123/26
110-82-7 Cyclohexane 710 U 7060 5580 79 7060 5610 79 1 73-126/32
124-48-1 Dibromochloromethane 710 U 7060 7260 103 7060 7280 103 0 76-127/27
96-12-8 1,2-Dibromo-3-chloropropane 710 U 7060 7230 102 7060 6800 96 6 70-137/29
106-93-4 1,2-Dibromoethane 710 U 7060 6960 99 7060 6900 98 1 77-126/26
75-71-8 Dichlorodifluoromethane 710 U 7060 5340 76 7060 4830 68 10 68-168/29
95-50-1 1,2-Dichlorobenzene 710 U 7060 7210 102 7060 7330 104 2 80-129/32
541-73-1 1,3-Dichlorobenzene 710 U 7060 7570 107 7060 7480 106 1 81-129/33
106-46-7 1,4-Dichlorobenzene 710 U 7060 7370 104 7060 7560 107 3 76-130/32
75-34-3 1,1-Dichloroethane 710 U 7060 6690 95 7060 6420 91 4 73-125/27
107-06-2 1,2-Dichloroethane 710 U 7060 6910 98 7060 6570 93 5 74-128/23
75-35-4 1,1-Dichloroethylene 710 U 7060 6230 88 7060 5870 83 6 81-136/28
156-59-2 cis-1,2-Dichloroethylene 710 U 7060 6650 94 7060 6750 96 1 74-126/26
156-60-5 trans-1,2-Dichloroethylene 710 U 7060 6930 98 7060 6590 93 5 70-127/27
78-87-5 1,2-Dichloropropane 710 U 7060 6560 93 7060 6560 93 0 74-125/25
10061-01-5 cis-1,3-Dichloropropene 710 U 7060 6810 96 7060 6800 96 0 80-123/26
10061-02-6 trans-1,3-Dichloropropene 710 U 7060 6910 98 7060 6750 96 2 75-131/28
100-41-4 Ethylbenzene 710 U 7060 6940 98 7060 6820 97 2 77-123/31
591-78-6 2-Hexanone 3500 U 35300 32300 91 35300 29900 85 8 72-133/26
98-82-8 Isopropylbenzene 267 I 7060 7440 102 7060 7300 100 2 80-136/32
79-20-9 Methyl Acetate 3500 U 35300 45400 129 35300 41900 119 8 67-137/30
74-83-9 Methyl Bromide 710 U 7060 6470 92 7060 6320 90 2 65-139/31
74-87-3 Methyl Chloride 710 U 7060 5590 79 7060 5450 77 3 71-144/27
108-87-2 Methylcyclohexane 710 U 7060 5740 81 7060 5860 83 2 75-128/31
75-09-2 Methylene Chloride 1040 IV 7060 7520 92 7060 7430 91 1 74-137/28
108-10-1 4-Methyl-2-pentanone (MIBK)3500 U 35300 34600 98 35300 32000 91 8 76-132/26
* = Outside of Control Limits.
45 of 66
FA35839T55.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA35839T
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA35831-8MS F0078939.D 1 08/03/16 EP n/a n/a VF2712
FA35831-8MSD F0078940.D 1 08/03/16 EP n/a n/a VF2712
FA35831-8 F0078936.D 1 08/03/16 EP n/a n/a VF2712
The QC reported here applies to the following samples:Method: SW846 8260B
FA35839-5T, FA35839-6T
FA35831-8 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
1634-04-4 Methyl Tert Butyl Ether 710 U 7060 7630 108 7060 7380 105 3 77-120/24
91-20-3 Naphthalene 17900 7060 17700 -3* a 7060 17000 -13* a 4 79-129/33
103-65-1 n-Propylbenzene 709 I 7060 6750 86 7060 6600 83 2 80-135/33
100-42-5 Styrene 710 U 7060 7550 107 7060 7440 105 1 78-125/30
79-34-5 1,1,2,2-Tetrachloroethane 710 U 7060 7400 105 7060 7440 105 1 71-126/30
127-18-4 Tetrachloroethylene 710 U 7060 6990 99 7060 7140 101 2 79-130/31
108-88-3 Toluene 710 U 7060 6510 92 7060 6440 91 1 76-124/30
120-82-1 1,2,4-Trichlorobenzene 710 U 7060 7550 107 7060 7220 102 4 78-130/34
71-55-6 1,1,1-Trichloroethane 710 U 7060 6160 87 7060 5970 85 3 70-129/27
79-00-5 1,1,2-Trichloroethane 710 U 7060 7700 109 7060 7360 104 5 74-124/28
79-01-6 Trichloroethylene 710 U 7060 6710 95 7060 6820 97 2 75-128/27
75-69-4 Trichlorofluoromethane 710 U 7060 5040 71*7060 4680 66*7 73-145/31
95-63-6 1,2,4-Trimethylbenzene 710 U 7060 6970 99 7060 6910 98 1 74-123/34
108-67-8 1,3,5-Trimethylbenzene 710 U 7060 6800 96 7060 6440 91 5 73-122/33
75-01-4 Vinyl Chloride 710 U 7060 5590 79 7060 5550 79 1 76-141/27
1330-20-7 Xylene (total)2100 U 21200 20600 97 21200 19700 93 4 80-129/30
CAS No.Surrogate Recoveries MS MSD FA35831-8 Limits
1868-53-7 Dibromofluoromethane 106%103%107%75-124%
17060-07-0 1,2-Dichloroethane-D4 99%91%117%72-135%
2037-26-5 Toluene-D8 98%95%98%75-126%
460-00-4 4-Bromofluorobenzene 106%110%98%71-133%
(a) Outside control limits due to high level in sample relative to spike amount.
* = Outside of Control Limits.
46 of 66
FA35839T55.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA35839T
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA35843-1MS Y30287.D 1 08/03/16 AD n/a n/a VY1220
FA35843-1MSD Y30288.D 1 08/03/16 AD n/a n/a VY1220
FA35843-1 a Y30281.D 1 08/03/16 AD n/a n/a VY1220
FA35843-1 Y30282.D 1 08/03/16 AD n/a n/a VY1220
The QC reported here applies to the following samples:Method: SW846 8260B
FA35839-7T, FA35839-9T
FA35843-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
67-64-1 Acetone ND b 1680000 73400 4*1680000 1620000 96 183*61-152/27
71-43-2 Benzene 7300 c 336000 317000 92 336000 325000 95 2 76-126/26
75-27-4 Bromodichloromethane ND b 336000 300000 89 336000 311000 93 4 74-130/25
75-25-2 Bromoform ND b 336000 292000 87 336000 316000 94 8 76-127/26
78-93-3 2-Butanone (MEK)ND b 1680000 1500000 89 1680000 1660000 99 10 75-137/25
104-51-8 n-Butylbenzene 38100 b 336000 375000 100 336000 382000 102 2 71-128/35
75-15-0 Carbon Disulfide ND b 336000 260000 77 336000 274000 82 5 72-122/29
56-23-5 Carbon Tetrachloride ND b 336000 272000 81 336000 276000 82 1 78-133/29
108-90-7 Chlorobenzene ND b 336000 335000 100 336000 339000 101 1 81-129/29
75-00-3 Chloroethane ND b 336000 254000 76 336000 266000 79 5 68-133/29
67-66-3 Chloroform ND b 336000 302000 90 336000 312000 93 3 72-123/26
110-82-7 Cyclohexane 11500 b J 336000 265000 75 336000 270000 77 2 73-126/32
124-48-1 Dibromochloromethane ND b 336000 310000 92 336000 335000 100 8 76-127/27
96-12-8 1,2-Dibromo-3-chloropropane ND b 336000 332000 99 336000 348000 104 5 70-137/29
106-93-4 1,2-Dibromoethane ND b 336000 332000 99 336000 334000 99 1 77-126/26
75-71-8 Dichlorodifluoromethane ND b 336000 207000 62*336000 205000 61*1 68-168/29
95-50-1 1,2-Dichlorobenzene ND b 336000 335000 100 336000 353000 105 5 80-129/32
541-73-1 1,3-Dichlorobenzene ND b 336000 339000 101 336000 360000 107 6 81-129/33
106-46-7 1,4-Dichlorobenzene ND b 336000 349000 104 336000 359000 107 3 76-130/32
75-34-3 1,1-Dichloroethane ND b 336000 305000 91 336000 314000 94 3 73-125/27
107-06-2 1,2-Dichloroethane ND b 336000 315000 94 336000 322000 96 2 74-128/23
75-35-4 1,1-Dichloroethylene ND b 336000 278000 83 336000 289000 86 4 81-136/28
156-59-2 cis-1,2-Dichloroethylene ND b 336000 304000 91 336000 304000 91 0 74-126/26
156-60-5 trans-1,2-Dichloroethylene ND b 336000 303000 90 336000 317000 94 5 70-127/27
78-87-5 1,2-Dichloropropane ND b 336000 317000 94 336000 318000 95 0 74-125/25
10061-01-5 cis-1,3-Dichloropropene ND b 336000 324000 96 336000 332000 99 2 80-123/26
10061-02-6 trans-1,3-Dichloropropene ND b 336000 340000 101 336000 359000 107 5 75-131/28
100-41-4 Ethylbenzene 121000 c 336000 438000 94 336000 450000 98 3 77-123/31
591-78-6 2-Hexanone ND b 1680000 1530000 91 1680000 1660000 99 8 72-133/26
98-82-8 Isopropylbenzene 19600 b J 336000 347000 97 336000 350000 98 1 80-136/32
79-20-9 Methyl Acetate ND b 1680000 1570000 94 1680000 1660000 99 6 67-137/30
74-83-9 Methyl Bromide ND b 336000 278000 83 336000 288000 86 4 65-139/31
74-87-3 Methyl Chloride ND b 336000 260000 77 336000 261000 78 0 71-144/27
108-87-2 Methylcyclohexane 69100 b 336000 329000 77 336000 333000 79 1 75-128/31
75-09-2 Methylene Chloride 41400 b JB 336000 340000 89 336000 353000 93 4 74-137/28
108-10-1 4-Methyl-2-pentanone (MIBK)ND b 1680000 1640000 98 1680000 1740000 104 6 76-132/26
* = Outside of Control Limits.
47 of 66
FA35839T55.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA35839T
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA35843-1MS Y30287.D 1 08/03/16 AD n/a n/a VY1220
FA35843-1MSD Y30288.D 1 08/03/16 AD n/a n/a VY1220
FA35843-1 a Y30281.D 1 08/03/16 AD n/a n/a VY1220
FA35843-1 Y30282.D 1 08/03/16 AD n/a n/a VY1220
The QC reported here applies to the following samples:Method: SW846 8260B
FA35839-7T, FA35839-9T
FA35843-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
1634-04-4 Methyl Tert Butyl Ether ND b 336000 317000 94 336000 327000 97 3 77-120/24
91-20-3 Naphthalene 118000 b 336000 471000 105 336000 509000 116 8 79-129/33
103-65-1 n-Propylbenzene 66900 b 336000 385000 95 336000 411000 102 7 80-135/33
100-42-5 Styrene ND b 336000 343000 102 336000 356000 106 4 78-125/30
79-34-5 1,1,2,2-Tetrachloroethane ND b 336000 310000 92 336000 338000 101 9 71-126/30
127-18-4 Tetrachloroethylene ND b 336000 321000 96 336000 329000 98 2 79-130/31
108-88-3 Toluene 282000 b 336000 583000 90 336000 613000 99 5 76-124/30
120-82-1 1,2,4-Trichlorobenzene ND b 336000 377000 112 336000 389000 116 3 78-130/34
71-55-6 1,1,1-Trichloroethane ND b 336000 262000 78 336000 270000 80 3 70-129/27
79-00-5 1,1,2-Trichloroethane ND b 336000 447000 133*336000 470000 140*5 74-124/28
79-01-6 Trichloroethylene ND b 336000 292000 87 336000 300000 89 3 75-128/27
75-69-4 Trichlorofluoromethane ND b 336000 211000 63*336000 226000 67*7 73-145/31
95-63-6 1,2,4-Trimethylbenzene 807000 b 336000 956000 44* d 336000 1050000 72* d 9 74-123/34
108-67-8 1,3,5-Trimethylbenzene 282000 b 336000 566000 85 336000 616000 99 8 73-122/33
75-01-4 Vinyl Chloride ND b 336000 248000 74*336000 257000 77 4 76-141/27
1330-20-7 Xylene (total)1540000 b 1010000 2510000 96 1010000 2700000 115 7 80-129/30
CAS No.Surrogate Recoveries MS MSD FA35843-1 FA35843-1 Limits
1868-53-7 Dibromofluoromethane 99%102%59%* e 90%75-124%
17060-07-0 1,2-Dichloroethane-D4 95%97%57%* e 105%72-135%
2037-26-5 Toluene-D8 101%100%106%101%75-126%
460-00-4 4-Bromofluorobenzene 96%101%111%105%71-133%
(a) Confirmation run for internal standard areas.
(b) Result is from Run #3.
(c) Result is from Run #2.
(d) Outside control limits due to high level in sample relative to spike amount.
(e) Outside control limits due to matrix interference.
* = Outside of Control Limits.
48 of 66
FA35839T55.3.2
SGS Accutest
GC/MS Semi-volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Southeast
Section 6
49 of 66
FA35839T6
Method Blank Summary Page 1 of 2
Job Number:FA35839T
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP61449-MB X048305.D 1 08/12/16 MV 08/11/16 OP61449 SX2101
The QC reported here applies to the following samples:Method: SW846 8270D
FA35839-5T, FA35839-6T, FA35839-7T, FA35839-9T
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 830 170 ug/kg
59-50-7 4-Chloro-3-methyl Phenol ND 170 25 ug/kg
95-57-8 2-Chlorophenol ND 170 21 ug/kg
120-83-2 2,4-Dichlorophenol ND 170 23 ug/kg
105-67-9 2,4-Dimethylphenol ND 170 20 ug/kg
51-28-5 2,4-Dinitrophenol ND 830 170 ug/kg
534-52-1 4,6-Dinitro-o-cresol ND 330 67 ug/kg
95-48-7 2-Methylphenol ND 170 18 ug/kg
3&4-Methylphenol ND 170 39 ug/kg
88-75-5 2-Nitrophenol ND 170 21 ug/kg
100-02-7 4-Nitrophenol ND 830 130 ug/kg
87-86-5 Pentachlorophenol ND 830 130 ug/kg
108-95-2 Phenol ND 170 20 ug/kg
88-06-2 2,4,6-Trichlorophenol ND 170 20 ug/kg
83-32-9 Acenaphthene ND 170 21 ug/kg
208-96-8 Acenaphthylene ND 170 21 ug/kg
120-12-7 Anthracene ND 170 24 ug/kg
56-55-3 Benzo(a)anthracene ND 170 19 ug/kg
50-32-8 Benzo(a)pyrene ND 170 18 ug/kg
205-99-2 Benzo(b)fluoranthene ND 170 21 ug/kg
191-24-2 Benzo(g,h,i)perylene ND 170 17 ug/kg
207-08-9 Benzo(k)fluoranthene ND 170 23 ug/kg
101-55-3 4-Bromophenyl phenyl ether ND 170 19 ug/kg
85-68-7 Butyl benzyl phthalate ND 170 33 ug/kg
106-47-8 4-Chloroaniline ND 170 23 ug/kg
111-91-1 bis(2-Chloroethoxy)methane ND 170 25 ug/kg
111-44-4 bis(2-Chloroethyl)ether ND 170 30 ug/kg
108-60-1 bis(2-Chloroisopropyl)ether ND 170 24 ug/kg
91-58-7 2-Chloronaphthalene ND 170 23 ug/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 170 21 ug/kg
218-01-9 Chrysene ND 170 22 ug/kg
53-70-3 Dibenzo(a,h)anthracene ND 170 18 ug/kg
132-64-9 Dibenzofuran ND 170 21 ug/kg
91-94-1 3,3'-Dichlorobenzidine ND 170 18 ug/kg
84-66-2 Diethyl Phthalate ND 330 33 ug/kg
131-11-3 Dimethyl Phthalate ND 170 33 ug/kg
50 of 66
FA35839T66.1.1
Method Blank Summary Page 2 of 2
Job Number:FA35839T
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP61449-MB X048305.D 1 08/12/16 MV 08/11/16 OP61449 SX2101
The QC reported here applies to the following samples:Method: SW846 8270D
FA35839-5T, FA35839-6T, FA35839-7T, FA35839-9T
CAS No.Compound Result RL MDL Units Q
117-84-0 Di-n-octyl Phthalate ND 170 33 ug/kg
84-74-2 Di-n-butyl Phthalate ND 330 67 ug/kg
121-14-2 2,4-Dinitrotoluene ND 170 17 ug/kg
606-20-2 2,6-Dinitrotoluene ND 170 21 ug/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 330 33 ug/kg
206-44-0 Fluoranthene ND 170 20 ug/kg
86-73-7 Fluorene ND 170 21 ug/kg
118-74-1 Hexachlorobenzene ND 170 21 ug/kg
87-68-3 Hexachlorobutadiene ND 170 19 ug/kg
77-47-4 Hexachlorocyclopentadiene ND 170 33 ug/kg
67-72-1 Hexachloroethane ND 170 19 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 170 26 ug/kg
78-59-1 Isophorone ND 170 17 ug/kg
90-12-0 1-Methylnaphthalene ND 170 26 ug/kg
91-57-6 2-Methylnaphthalene ND 170 19 ug/kg
91-20-3 Naphthalene ND 170 25 ug/kg
98-95-3 Nitrobenzene ND 170 22 ug/kg
621-64-7 N-Nitrosodi-n-propylamine ND 170 18 ug/kg
86-30-6 N-Nitrosodiphenylamine ND 170 32 ug/kg
85-01-8 Phenanthrene ND 170 20 ug/kg
129-00-0 Pyrene ND 170 31 ug/kg
CAS No.Surrogate Recoveries Limits
367-12-4 2-Fluorophenol 63%40-102%
4165-62-2 Phenol-d5 73%41-100%
118-79-6 2,4,6-Tribromophenol 64%42-108%
4165-60-0 Nitrobenzene-d5 67%40-105%
321-60-8 2-Fluorobiphenyl 66%43-107%
1718-51-0 Terphenyl-d14 72%45-119%
51 of 66
FA35839T66.1.1
Blank Spike Summary Page 1 of 2
Job Number:FA35839T
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP61449-BS X048304.D 1 08/12/16 MV 08/11/16 OP61449 SX2101
The QC reported here applies to the following samples:Method: SW846 8270D
FA35839-5T, FA35839-6T, FA35839-7T, FA35839-9T
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
65-85-0 Benzoic Acid 3330 2560 77 36-118
59-50-7 4-Chloro-3-methyl Phenol 1670 1260 76 52-108
95-57-8 2-Chlorophenol 1670 1190 71 48-104
120-83-2 2,4-Dichlorophenol 1670 1300 78 51-105
105-67-9 2,4-Dimethylphenol 1670 1280 77 43-96
51-28-5 2,4-Dinitrophenol 3330 2250 68 40-119
534-52-1 4,6-Dinitro-o-cresol 3330 2810 84 64-121
95-48-7 2-Methylphenol 1670 1150 69 46-107
3&4-Methylphenol 3330 2290 69 44-111
88-75-5 2-Nitrophenol 1670 1280 77 49-104
100-02-7 4-Nitrophenol 3330 2180 65 56-116
87-86-5 Pentachlorophenol 3330 2740 82 61-114
108-95-2 Phenol 1670 1200 72 45-110
88-06-2 2,4,6-Trichlorophenol 1670 1370 82 56-109
83-32-9 Acenaphthene 1670 1360 82 56-109
208-96-8 Acenaphthylene 1670 1310 79 56-106
120-12-7 Anthracene 1670 1380 83 61-110
56-55-3 Benzo(a)anthracene 1670 1410 85 66-111
50-32-8 Benzo(a)pyrene 1670 1420 85 59-104
205-99-2 Benzo(b)fluoranthene 1670 1480 89 67-113
191-24-2 Benzo(g,h,i)perylene 1670 1440 86 67-113
207-08-9 Benzo(k)fluoranthene 1670 1460 88 67-114
101-55-3 4-Bromophenyl phenyl ether 1670 1540 92 62-110
85-68-7 Butyl benzyl phthalate 1670 1570 94 65-113
106-47-8 4-Chloroaniline 1670 1250 75 30-115
111-91-1 bis(2-Chloroethoxy)methane 1670 1320 79 48-105
111-44-4 bis(2-Chloroethyl)ether 1670 1180 71 46-103
108-60-1 bis(2-Chloroisopropyl)ether 1670 1350 81 40-110
91-58-7 2-Chloronaphthalene 1670 1340 80 53-106
7005-72-3 4-Chlorophenyl phenyl ether 1670 1340 80 58-106
218-01-9 Chrysene 1670 1490 89 65-112
53-70-3 Dibenzo(a,h)anthracene 1670 1400 84 68-115
132-64-9 Dibenzofuran 1670 1310 79 57-108
91-94-1 3,3'-Dichlorobenzidine 1670 1240 74 36-114
84-66-2 Diethyl Phthalate 1670 1310 79 61-109
131-11-3 Dimethyl Phthalate 1670 1340 80 59-108
* = Outside of Control Limits.
52 of 66
FA35839T66.2.1
Blank Spike Summary Page 2 of 2
Job Number:FA35839T
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP61449-BS X048304.D 1 08/12/16 MV 08/11/16 OP61449 SX2101
The QC reported here applies to the following samples:Method: SW846 8270D
FA35839-5T, FA35839-6T, FA35839-7T, FA35839-9T
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
117-84-0 Di-n-octyl Phthalate 1670 1710 103 64-119
84-74-2 Di-n-butyl Phthalate 1670 1440 86 63-108
121-14-2 2,4-Dinitrotoluene 1670 1320 79 59-109
606-20-2 2,6-Dinitrotoluene 1670 1270 76 61-107
117-81-7 bis(2-Ethylhexyl)phthalate 1670 1650 99 64-115
206-44-0 Fluoranthene 1670 1260 76 60-108
86-73-7 Fluorene 1670 1280 77 58-109
118-74-1 Hexachlorobenzene 1670 1480 89 59-111
87-68-3 Hexachlorobutadiene 1670 1280 77 41-108
77-47-4 Hexachlorocyclopentadiene 1670 1710 103 49-110
67-72-1 Hexachloroethane 1670 1150 69 40-105
193-39-5 Indeno(1,2,3-cd)pyrene 1670 1420 85 66-116
78-59-1 Isophorone 1670 1330 80 42-89
90-12-0 1-Methylnaphthalene 1670 1300 78 49-106
91-57-6 2-Methylnaphthalene 1670 1290 77 47-106
91-20-3 Naphthalene 1670 1210 73 44-104
98-95-3 Nitrobenzene 1670 1320 79 43-108
621-64-7 N-Nitrosodi-n-propylamine 1670 1230 74 48-108
86-30-6 N-Nitrosodiphenylamine 1670 1500 90 62-110
85-01-8 Phenanthrene 1670 1400 84 63-111
129-00-0 Pyrene 1670 1570 94 65-115
CAS No.Surrogate Recoveries BSP Limits
367-12-4 2-Fluorophenol 65%40-102%
4165-62-2 Phenol-d5 73%41-100%
118-79-6 2,4,6-Tribromophenol 83%42-108%
4165-60-0 Nitrobenzene-d5 75%40-105%
321-60-8 2-Fluorobiphenyl 77%43-107%
1718-51-0 Terphenyl-d14 91%45-119%
* = Outside of Control Limits.
53 of 66
FA35839T66.2.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA35839T
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP61449-MS X048307.D 1 08/12/16 MV 08/11/16 OP61449 SX2101
OP61449-MSD X048308.D 1 08/12/16 MV 08/11/16 OP61449 SX2101
FA35953-1 X048306.D 1 08/12/16 MV 08/11/16 OP61449 SX2101
The QC reported here applies to the following samples:Method: SW846 8270D
FA35839-5T, FA35839-6T, FA35839-7T, FA35839-9T
FA35953-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
65-85-0 Benzoic Acid 890 U 3510 2660 76 3510 2350 67 12 36-118/41
59-50-7 4-Chloro-3-methyl Phenol 180 U 1750 1330 76 1750 1180 67 12 52-108/21
95-57-8 2-Chlorophenol 180 U 1750 1250 71 1750 1130 64 10 48-104/26
120-83-2 2,4-Dichlorophenol 180 U 1750 1380 79 1750 1220 70 12 51-105/27
105-67-9 2,4-Dimethylphenol 180 U 1750 1370 78 1750 1220 70 12 43-96/23
51-28-5 2,4-Dinitrophenol 890 U 3510 2310 66 3510 1980 56 15 40-119/32
534-52-1 4,6-Dinitro-o-cresol 350 U 3510 2940 84 3510 2590 74 13 64-121/29
95-48-7 2-Methylphenol 180 U 1750 1210 69 1750 1090 62 10 46-107/24
3&4-Methylphenol 180 U 3510 2390 68 3510 2150 61 11 44-111/24
88-75-5 2-Nitrophenol 180 U 1750 1380 79 1750 1240 71 11 49-104/27
100-02-7 4-Nitrophenol 890 U 3510 2290 65 3510 1920 55*18 56-116/23
87-86-5 Pentachlorophenol 890 U 3510 2960 84 3510 2530 72 16 61-114/23
108-95-2 Phenol 180 U 1750 1260 72 1750 1130 64 11 45-110/24
88-06-2 2,4,6-Trichlorophenol 180 U 1750 1470 84 1750 1280 73 14 56-109/25
83-32-9 Acenaphthene 180 U 1750 1450 83 1750 1260 72 14 56-109/23
208-96-8 Acenaphthylene 180 U 1750 1390 79 1750 1210 69 14 56-106/23
120-12-7 Anthracene 180 U 1750 1470 84 1750 1260 72 15 61-110/21
56-55-3 Benzo(a)anthracene 180 U 1750 1470 84 1750 1260 72 15 66-111/23
50-32-8 Benzo(a)pyrene 180 U 1750 1470 84 1750 1270 72 15 59-104/23
205-99-2 Benzo(b)fluoranthene 180 U 1750 1480 84 1750 1290 74 14 67-113/24
191-24-2 Benzo(g,h,i)perylene 180 U 1750 1510 86 1750 1260 72 18 67-113/21
207-08-9 Benzo(k)fluoranthene 180 U 1750 1570 90 1750 1350 77 15 67-114/22
101-55-3 4-Bromophenyl phenyl ether 180 U 1750 1580 90 1750 1390 79 13 62-110/21
85-68-7 Butyl benzyl phthalate 180 U 1750 1640 94 1750 1450 83 12 65-113/20
106-47-8 4-Chloroaniline 180 U 1750 1290 74 1750 1110 63 15 30-115/30
111-91-1 bis(2-Chloroethoxy)methane 180 U 1750 1410 80 1750 1260 72 11 48-105/24
111-44-4 bis(2-Chloroethyl)ether 180 U 1750 1250 71 1750 1140 65 9 46-103/27
108-60-1 bis(2-Chloroisopropyl)ether 180 U 1750 1390 79 1750 1270 72 9 40-110/25
91-58-7 2-Chloronaphthalene 180 U 1750 1430 82 1750 1260 72 13 53-106/23
7005-72-3 4-Chlorophenyl phenyl ether 180 U 1750 1410 80 1750 1210 69 15 58-106/21
218-01-9 Chrysene 180 U 1750 1600 91 1750 1370 78 15 65-112/25
53-70-3 Dibenzo(a,h)anthracene 180 U 1750 1520 87 1750 1220 70 22 68-115/23
132-64-9 Dibenzofuran 180 U 1750 1400 80 1750 1200 68 15 57-108/22
91-94-1 3,3'-Dichlorobenzidine 180 U 1750 1230 70 1750 1060 60 15 36-114/28
84-66-2 Diethyl Phthalate 350 U 1750 1360 78 1750 1180 67 14 61-109/20
131-11-3 Dimethyl Phthalate 180 U 1750 1420 81 1750 1210 69 16 59-108/20
* = Outside of Control Limits.
54 of 66
FA35839T66.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA35839T
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP61449-MS X048307.D 1 08/12/16 MV 08/11/16 OP61449 SX2101
OP61449-MSD X048308.D 1 08/12/16 MV 08/11/16 OP61449 SX2101
FA35953-1 X048306.D 1 08/12/16 MV 08/11/16 OP61449 SX2101
The QC reported here applies to the following samples:Method: SW846 8270D
FA35839-5T, FA35839-6T, FA35839-7T, FA35839-9T
FA35953-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
117-84-0 Di-n-octyl Phthalate 180 U 1750 1710 98 1750 1580 90 8 64-119/21
84-74-2 Di-n-butyl Phthalate 350 U 1750 1510 86 1750 1320 75 13 63-108/19
121-14-2 2,4-Dinitrotoluene 180 U 1750 1380 79 1750 1200 68 14 59-109/20
606-20-2 2,6-Dinitrotoluene 180 U 1750 1330 76 1750 1130 64 16 61-107/22
117-81-7 bis(2-Ethylhexyl)phthalate 350 U 1750 1720 98 1750 1520 87 12 64-115/23
206-44-0 Fluoranthene 180 U 1750 1310 75 1750 1120 64 16 60-108/25
86-73-7 Fluorene 180 U 1750 1350 77 1750 1160 66 15 58-109/21
118-74-1 Hexachlorobenzene 180 U 1750 1540 88 1750 1350 77 13 59-111/21
87-68-3 Hexachlorobutadiene 180 U 1750 1390 79 1750 1220 70 13 41-108/27
77-47-4 Hexachlorocyclopentadiene 180 U 1750 1850 106 1750 1600 91 14 49-110/31
67-72-1 Hexachloroethane 180 U 1750 1170 67 1750 1100 63 6 40-105/32
193-39-5 Indeno(1,2,3-cd)pyrene 180 U 1750 1480 84 1750 1240 71 18 66-116/22
78-59-1 Isophorone 180 U 1750 1400 80 1750 1260 72 11 42-89/22
90-12-0 1-Methylnaphthalene 180 U 1750 1370 78 1750 1210 69 12 49-106/26
91-57-6 2-Methylnaphthalene 180 U 1750 1400 80 1750 1230 70 13 47-106/27
91-20-3 Naphthalene 180 U 1750 1300 74 1750 1160 66 11 44-104/27
98-95-3 Nitrobenzene 180 U 1750 1410 80 1750 1270 72 10 43-108/25
621-64-7 N-Nitrosodi-n-propylamine 180 U 1750 1280 73 1750 1160 66 10 48-108/27
86-30-6 N-Nitrosodiphenylamine 180 U 1750 1600 91 1750 1390 79 14 62-110/21
85-01-8 Phenanthrene 180 U 1750 1480 84 1750 1290 74 14 63-111/22
129-00-0 Pyrene 180 U 1750 1660 95 1750 1480 84 11 65-115/25
CAS No.Surrogate Recoveries MS MSD FA35953-1 Limits
367-12-4 2-Fluorophenol 66%59%72%40-102%
4165-62-2 Phenol-d5 73%66%81%41-100%
118-79-6 2,4,6-Tribromophenol 86%74%91%42-108%
4165-60-0 Nitrobenzene-d5 76%69%82%40-105%
321-60-8 2-Fluorobiphenyl 80%70%84%43-107%
1718-51-0 Terphenyl-d14 91%79%101%45-119%
* = Outside of Control Limits.
55 of 66
FA35839T66.3.1
SGS Accutest
GC Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Southeast
Section 7
56 of 66
FA35839T7
Method Blank Summary Page 1 of 1
Job Number:FA35839T
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
GUU853-MB UU016739.D 1 08/03/16 AH n/a n/a GUU853
The QC reported here applies to the following samples:Method: MADEP VPH REV 1.1
FA35839-5T, FA35839-6T, FA35839-7T, FA35839-9T
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 51 51 ug/kg
100-41-4 Ethylbenzene ND 100 51 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 100 51 ug/kg
91-20-3 Naphthalene ND 260 150 ug/kg
108-88-3 Toluene ND 100 51 ug/kg
m,p-Xylene ND 200 100 ug/kg
95-47-6 o-Xylene ND 100 51 ug/kg
C5- C8 Aliphatics (Unadj.)ND 5100 1800 ug/kg
C9- C12 Aliphatics (Unadj.)ND 5100 1800 ug/kg
C9- C10 Aromatics (Unadj.)ND 5100 1800 ug/kg
CAS No.Surrogate Recoveries Limits
460-00-4 BFB 82%70-130%
460-00-4 BFB 84%70-130%
57 of 66
FA35839T77.1.1
Method Blank Summary Page 1 of 1
Job Number:FA35839T
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
GUU855-MB UU016776.D 1 08/04/16 AH n/a n/a GUU855
The QC reported here applies to the following samples:Method: MADEP VPH REV 1.1
FA35839-6T
CAS No.Compound Result RL MDL Units Q
C9- C12 Aliphatics (Unadj.)ND 5100 1800 ug/kg
C9- C10 Aromatics (Unadj.)ND 5100 1800 ug/kg
CAS No.Surrogate Recoveries Limits
460-00-4 BFB 85%70-130%
460-00-4 BFB 88%70-130%
58 of 66
FA35839T77.1.2
Blank Spike/Blank Spike Duplicate Summary Page 1 of 1
Job Number:FA35839T
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
GUU853-BS UU016737.D 1 08/03/16 AH n/a n/a GUU853
GUU853-BSD UU016738.D 1 08/03/16 AH n/a n/a GUU853
The QC reported here applies to the following samples:Method: MADEP VPH REV 1.1
FA35839-5T, FA35839-6T, FA35839-7T, FA35839-9T
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/kg ug/kg %ug/kg %RPD Rec/RPD
71-43-2 Benzene 4160 4030 97 4040 97 0 70-130/25
100-41-4 Ethylbenzene 4160 4070 98 4080 98 0 70-130/25
1634-04-4 Methyl Tert Butyl Ether 4160 3980 96 4000 96 1 70-130/25
91-20-3 Naphthalene 4160 3640 87 3690 89 1 70-130/25
108-88-3 Toluene 4160 4020 97 4030 97 0 70-130/25
m,p-Xylene 8320 7930 95 7910 95 0 70-130/25
95-47-6 o-Xylene 4160 4010 96 4010 96 0 70-130/25
C5- C8 Aliphatics (Unadj.)12500 14000 112 14100 113 1 70-130/25
C9- C12 Aliphatics (Unadj.)8320 8970 108 8780 105 2 70-130/25
C9- C10 Aromatics (Unadj.)4160 4330 104 4470 107 3 70-130/25
CAS No.Surrogate Recoveries BSP BSD Limits
460-00-4 BFB 85%85%70-130%
460-00-4 BFB 86%85%70-130%
* = Outside of Control Limits.
59 of 66
FA35839T77.2.1
Blank Spike/Blank Spike Duplicate Summary Page 1 of 1
Job Number:FA35839T
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
GUU855-BS UU016774.D 1 08/04/16 AH n/a n/a GUU855
GUU855-BSD UU016775.D 1 08/04/16 AH n/a n/a GUU855
The QC reported here applies to the following samples:Method: MADEP VPH REV 1.1
FA35839-6T
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/kg ug/kg %ug/kg %RPD Rec/RPD
C9- C12 Aliphatics (Unadj.)8320 8240 99 8970 108 8 70-130/25
C9- C10 Aromatics (Unadj.)4160 4030 97 4300 103 6 70-130/25
CAS No.Surrogate Recoveries BSP BSD Limits
460-00-4 BFB 89%90%70-130%
460-00-4 BFB 90%90%70-130%
* = Outside of Control Limits.
60 of 66
FA35839T77.2.2
Duplicate Summary Page 1 of 1
Job Number:FA35839T
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA35839-5TDUP UU016741.D 1 08/03/16 AH n/a n/a GUU853
FA35839-5T UU016740.D 1 08/03/16 AH n/a n/a GUU853
The QC reported here applies to the following samples:Method: MADEP VPH REV 1.1
FA35839-5T, FA35839-6T, FA35839-7T, FA35839-9T
FA35839-5T DUP
CAS No.Compound ug/kg Q ug/kg Q RPD Limits
71-43-2 Benzene ND ND nc 50
100-41-4 Ethylbenzene ND ND nc 50
1634-04-4 Methyl Tert Butyl Ether ND ND nc 50
91-20-3 Naphthalene ND ND nc 50
108-88-3 Toluene ND ND nc 50
m,p-Xylene ND ND nc 50
95-47-6 o-Xylene ND ND nc 50
C5- C8 Aliphatics (Unadj.)ND ND nc 50
C9- C12 Aliphatics (Unadj.)ND ND nc 50
C9- C10 Aromatics (Unadj.)ND ND nc 50
C5- C8 Aliphatics ND ND nc 50
C9- C12 Aliphatics ND ND nc 50
C9- C10 Aromatics ND ND nc 50
CAS No.Surrogate Recoveries DUP FA35839-5T Limits
460-00-4 BFB 90%88%70-130%
460-00-4 BFB 92%90%70-130%
* = Outside of Control Limits.
61 of 66
FA35839T77.3.1
Duplicate Summary Page 1 of 1
Job Number:FA35839T
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA35842-4DUP UU016779.D 1 08/04/16 AH n/a n/a GUU855
FA35842-4 UU016778.D 1 08/04/16 AH n/a n/a GUU855
The QC reported here applies to the following samples:Method: MADEP VPH REV 1.1
FA35839-6T
FA35842-4 DUP
CAS No.Compound ug/kg Q ug/kg Q RPD Limits
C9- C12 Aliphatics (Unadj.)45100 J 46400 J 3 50
C9- C10 Aromatics (Unadj.)129000 126000 2 50
C9- C12 Aliphatics ND ND nc 50
C9- C10 Aromatics 129000 126000 2 50
CAS No.Surrogate Recoveries DUP FA35842-4 Limits
460-00-4 BFB 112%116%70-130%
460-00-4 BFB 103%101%70-130%
* = Outside of Control Limits.
62 of 66
FA35839T77.3.2
SGS Accutest
GC Semi-volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Southeast
Section 8
63 of 66
FA35839T8
Method Blank Summary Page 1 of 1
Job Number:FA35839T
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP61448-MB NN015921.D 1 08/17/16 FS 08/11/16 OP61448 GNN787
The QC reported here applies to the following samples:Method: MADEP EPH REV 1.1
FA35839-5T, FA35839-6T, FA35839-7T, FA35839-9T
CAS No.Compound Result RL MDL Units Q
83-32-9 Acenaphthene ND 200 100 ug/kg
208-96-8 Acenaphthylene ND 200 100 ug/kg
120-12-7 Anthracene ND 200 100 ug/kg
56-55-3 Benzo(a)anthracene ND 200 100 ug/kg
50-32-8 Benzo(a)pyrene ND 200 100 ug/kg
205-99-2 Benzo(b)fluoranthene ND 200 100 ug/kg
191-24-2 Benzo(g,h,i)perylene ND 200 100 ug/kg
207-08-9 Benzo(k)fluoranthene ND 200 100 ug/kg
218-01-9 Chrysene ND 200 100 ug/kg
53-70-3 Dibenzo(a,h)anthracene ND 200 100 ug/kg
206-44-0 Fluoranthene ND 200 100 ug/kg
86-73-7 Fluorene ND 200 100 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 200 100 ug/kg
91-57-6 2-Methylnaphthalene ND 200 100 ug/kg
91-20-3 Naphthalene ND 200 100 ug/kg
85-01-8 Phenanthrene ND 200 100 ug/kg
129-00-0 Pyrene ND 200 100 ug/kg
C11-C22 Aromatics (Unadj.)ND 10000 7500 ug/kg
C11-C22 Aromatics ND 10000 7500 ug/kg
C9-C18 Aliphatics ND 10000 5000 ug/kg
C19-C36 Aliphatics ND 10000 5000 ug/kg
CAS No.Surrogate Recoveries Limits
3386-33-2 1-Chlorooctadecane 59%40-140%
580-13-2 2-Bromonaphthalene 87%40-140%
84-15-1 o-Terphenyl 60%40-140%
321-60-8 2-Fluorobiphenyl 80%40-140%
64 of 66
FA35839T88.1.1
Blank Spike/Blank Spike Duplicate Summary Page 1 of 1
Job Number:FA35839T
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP61448-BS NN015922.D 1 08/17/16 FS 08/11/16 OP61448 GNN787
OP61448-BSD NN015923.D 1 08/17/16 FS 08/11/16 OP61448 GNN787
The QC reported here applies to the following samples:Method: MADEP EPH REV 1.1
FA35839-5T, FA35839-6T, FA35839-7T, FA35839-9T
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/kg ug/kg %ug/kg %RPD Rec/RPD
83-32-9 Acenaphthene 5000 2930 59 3320 66 12 40-140/30
208-96-8 Acenaphthylene 5000 3040 61 3460 69 13 40-140/30
120-12-7 Anthracene 5000 3210 64 3660 73 13 40-140/30
56-55-3 Benzo(a)anthracene 5000 3480 70 3990 80 14 40-140/30
50-32-8 Benzo(a)pyrene 5000 3440 69 3950 79 14 40-140/30
205-99-2 Benzo(b)fluoranthene 5000 3640 73 4190 84 14 40-140/30
191-24-2 Benzo(g,h,i)perylene 5000 3700 74 4160 83 12 40-140/30
207-08-9 Benzo(k)fluoranthene 5000 3410 68 3900 78 13 40-140/30
218-01-9 Chrysene 5000 3490 70 3980 80 13 40-140/30
53-70-3 Dibenzo(a,h)anthracene 5000 3750 75 4260 85 13 40-140/30
206-44-0 Fluoranthene 5000 3390 68 3890 78 14 40-140/30
86-73-7 Fluorene 5000 3120 62 3530 71 12 40-140/30
193-39-5 Indeno(1,2,3-cd)pyrene 5000 3650 73 4170 83 13 40-140/30
91-57-6 2-Methylnaphthalene 5000 2830 57 3230 65 13 40-140/30
91-20-3 Naphthalene 5000 2460 49 2830 57 14 40-140/30
85-01-8 Phenanthrene 5000 3420 68 3920 78 14 40-140/30
129-00-0 Pyrene 5000 3500 70 4000 80 13 40-140/30
C11-C22 Aromatics (Unadj.)85000 54000 64 61500 72 13 40-140/30
C9-C18 Aliphatics 30000 17500 58 20600 69 16 40-140/30
C19-C36 Aliphatics 40000 28200 71 32200 81 13 40-140/30
CAS No.Surrogate Recoveries BSP BSD Limits
3386-33-2 1-Chlorooctadecane 56%67%40-140%
580-13-2 2-Bromonaphthalene 81%97%40-140%
84-15-1 o-Terphenyl 60%68%40-140%
321-60-8 2-Fluorobiphenyl 74%88%40-140%
Sample Compound Col #1 Col #2 Breakthrough Limit
OP61448-BS 2-Methylnaphthalene 2830 ND 0.0%5.0
OP61448-BS Naphthalene 2460 ND 0.0%5.0
OP61448-BSD 2-Methylnaphthalene 3230 ND 0.0%5.0
OP61448-BSD Naphthalene 2830 ND 0.0%5.0
* = Outside of Control Limits.
65 of 66
FA35839T88.2.1
Duplicate Summary Page 1 of 1
Job Number:FA35839T
Account:GRINCC GRI (Geological Resources Inc.)
Project:Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP61448-DUP NN015935.D 1 08/17/16 FS 08/11/16 OP61448 GNN787
FA35839-9T NN015934.D 1 08/17/16 FS 08/11/16 OP61448 GNN787
The QC reported here applies to the following samples:Method: MADEP EPH REV 1.1
FA35839-5T, FA35839-6T, FA35839-7T, FA35839-9T
FA35839-9T DUP
CAS No.Compound ug/kg Q ug/kg Q RPD Limits
83-32-9 Acenaphthene ND ND nc 30 a
208-96-8 Acenaphthylene ND ND nc 30 a
120-12-7 Anthracene ND ND nc 30 a
56-55-3 Benzo(a)anthracene ND ND nc 30 a
50-32-8 Benzo(a)pyrene ND ND nc 30 a
205-99-2 Benzo(b)fluoranthene ND ND nc 30 a
191-24-2 Benzo(g,h,i)perylene ND ND nc 30 a
207-08-9 Benzo(k)fluoranthene ND ND nc 30 a
218-01-9 Chrysene ND ND nc 30 a
53-70-3 Dibenzo(a,h)anthracene ND ND nc 30 a
206-44-0 Fluoranthene ND ND nc 30 a
86-73-7 Fluorene ND ND nc 30 a
193-39-5 Indeno(1,2,3-cd)pyrene ND ND nc 30 a
91-57-6 2-Methylnaphthalene ND ND nc 30 a
91-20-3 Naphthalene ND ND nc 30 a
85-01-8 Phenanthrene ND ND nc 30 a
129-00-0 Pyrene ND ND nc 30 a
C11-C22 Aromatics (Unadj.)ND ND nc 30 a
C11-C22 Aromatics ND ND nc 30 a
C9-C18 Aliphatics ND ND nc 30 a
C19-C36 Aliphatics ND ND nc 30 a
CAS No.Surrogate Recoveries DUP FA35839-9T Limits
3386-33-2 1-Chlorooctadecane 69%66%40-140%
580-13-2 2-Bromonaphthalene 82%95%40-140%
84-15-1 o-Terphenyl 61%68%40-140%
321-60-8 2-Fluorobiphenyl 73%84%40-140%
(a) Advisory control limits.
* = Outside of Control Limits.
66 of 66
FA35839T88.3.1