WS-9385_44606_CA_LSA_20191126

TABLE OF CONTENTS 

1.0 INTRODUCTION .................................................................................. 1 
2.0 SITE HISTORY ...................................................................................... 2 
2.1 UNDERGROUND STORAGE TANK INFORMATION ............................................... 2 
2.2 SITE HISTORY ........................................................................................... 3 
3.0 RISK CHARACTERIZATION ................................................................... 3 
4.0 RECEPTOR INFORMATION .................................................................. 4 
4.1 WATER SUPPLY WELLS ............................................................................... 4 
4.2 PUBLIC WATER SUPPLIES ............................................................................ 4 
4.3 SURFACE WATER ...................................................................................... 4 
4.4 WELLHEAD PROTECTION AREAS ................................................................... 4 
4.5 DEEP AQUIFERS IN THE COASTAL PLAIN PHYSIOGRAPHIC REGION ........................ 5 
4.6 SUBSURFACE STRUCTURES .......................................................................... 5 
4.7 LAND USE ............................................................................................... 5 
5.0 SITE GEOLOGY & HYDROGEOLOGY ..................................................... 5 
6.0 SOIL INVESTIGATION .......................................................................... 5 
7.0 GROUNDWATER INVESTIGATION ....................................................... 6 
7.1 MONITORING WELL INSTALLATION ............................................................... 6 
7.2 MONITORING WELL SAMPLING & LABORATORY ANALYSES ................................ 7 
7.3 GROUNDWATER FLOW DIRECTION ................................................................ 8 
7.4 GROUNDWATER ANALYTICAL RESULTS ........................................................... 8 
8.0 ASSESSMENT SUMMARY .................................................................... 9 
9.0 LIMITATIONS .................................................................................... 11 

Page  I

TABLE OF CONTENTS 
(Continued) 

FIGURES: 

1. USGS Topographic Map 
2. Site Map 
3. Receptor Survey Map 
4. Potentiometric Surface Map (10‐24‐2019) 
5. Benzene Isoconcentration Map (10‐24‐2019) 
6. MTBE Isoconcentration Map (10‐24‐2019) 
7. Naphthalene Isoconcentration Map (10‐24‐2019) 

TABLES: 

1. UST Information (page 2) 
2. Surrounding Properties within 1,000 ft. of Source Area  
3. Risk‐Based Soil Analytical Results 
4. Monitoring Well Construction Data 
5. Groundwater Gauging Data 
6. Groundwater Analytical Results 

APPENDICES: 

A. Notice of Regulatory Requirements 
B. LSA Risk Classification & Land Use Form 
C. Completed Well Survey Forms 
D. Standard Field Procedures  
E. Boring Logs & Well Construction Records  
F. Laboratory Report for Soil  
G. Laboratory Report for Groundwater Samples 

Page II

Alamance Oil Company, Inc. – Limited Site Assessment (LSA II) 1
Pyramid Project # 2019-210 11/27/2019
PHASE II  
LIMITED SITE ASSESSMENT REPORT 
ALAMANCE OIL  
GAS STATION SITE 

1.0 INTRODUCTION 

On behalf of T.A.C. Inc. and Alamance Oil Company, Pyramid Environmental & 
Engineering P.C. (Pyramid) has completed the Phase II Limited Site Assessment (LSA II) 
for the Alamance Oil Gasoline Station site. The site is located at 1525 W. Webb Avenue 
in Burlington, Alamance County, North Carolina, and is the site of a petroleum 
underground storage tank (UST) release. The location of the site is shown on Figure 1, a 
portion of the Burlington, NC, USGS topographic map. 

The gasoline station was constructed in the 1960s with three 2,000‐gallon gasoline 
Underground Storage Tanks (USTs) and one 550‐gallon UST. The site map is shown as 
Figure 2.  These tanks have been upgraded through the years to maintain compliance 
with UST requirements and operability. In 2016, the NC Department of Environmental 
Quality (NCDEQ) found a diesel dispenser leak at the main pump island during a UST 
compliance inspection. As part of the remediation efforts, Pyramid removed 
contaminated soil below the diesel pump using an Air‐Knife and vacuum unit. The 
removal of several drums of soil was able to remediate the localized diesel spill. 

In 2018, the NCDEQ again inspected the site, and another diesel fuel release was 
detected at the same dispenser location. After cleanup, the soil was tested for Risk‐
Based compounds, and the results were sent to the NCDEQ. A Notice of Regulatory 
Requirements (NORR) was sent to Alamance Oil requiring a Limited Site Assessment 
(LSA) for diesel release DEQ # 44606‐B. 

Groundwater Incident #: 44606 
Site Name: Alamance Oil Gas Station  
Site Address: 1525 W. Webb Ave., Burlington,  NC 27217 
County: Alamance County, NC 
Describe GPS release area: Active Gasoline Station 
Source of GPS location: Google Earth 
Latitude/Longitude of Source: N Lat.  36.106063°   W Long. ‐ 79.457246° 

UST Owner / UST Operator: T.A.C., Inc. 
 2200 E. Bessemer Ave., Greensboro, NC 

Alamance Oil Company, Inc. – Limited Site Assessment (LSA II) 2
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Responsible Party: T.A.C., Inc. 
 2200 E. Bessemer Avenue, Greensboro, NC 
Property Owner: Alamance Oil Company  
Property Occupant: Active Alamance Oil Gasoline Station 

Consultant Contractor: Mike Jones, Operations Manager 
 Pyramid Environmental & Engineering, PC 
 503 Industrial Ave., Greensboro, NC 27406 
 (336) 335‐3174 
 [e-mail] 

Analytical Laboratory: Pace Analytical Services, LLC 
 9800 Kincey Ave., Suite 300 
 Huntersville, NC 28078 
 (615) 258‐5858 

2.0 SITE HISTORY 

2.1 Underground Storage Tank Information 
As described earlier, the gasoline station has been in operation since the 1960s, and has 
been regularly upgraded to maintain compliance with NCDEQ UST requirements.  
Details of the USTs are included in Table 1. 

Table 1  ‐  UST Information 

Tank 
No. 
Installation 
Date 
Size in 
Gallons 
Tank 
Dimensions 
Last 
Contents 
Date 
Removed 
1 1960s 2,000 64" diam. x 12 ft. long Gasoline Active 
2 1960s 2,000 64" diam. x 12 ft. long Gasoline Active 
3 1960s 2,000 64" diam. x 12 ft. long Gasoline Active 
4 1960s 550 42" diam. x 92” long Diesel Active 

The site plan showing the UST locations of the Alamance Oil gas station site is presented 
as Figure 2.  Based on the DEQ UST registration database, the USTs were single walled 
steel USTs installed in the late 1960s. 

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2.2 Site History 
The Alamance Oil Gasoline Station was constructed in the 1960s with three 2,000‐gallon 
gasoline USTs and one 550‐gallon diesel UST. These tanks have been upgraded through 
the years to maintain compliance with UST requirements and operability. 

In 2016, the NC Department of Environmental Quality (NCDEQ) found a diesel dispenser 
leak at the pump island during a compliance inspection.  As part of the remediation 
efforts, Pyramid removed contaminated soil below the diesel pump using an Air‐Knife 
and vacuum unit. The removal of several drums of soil was able to remediate the 
localized diesel spill. 

In 2018, the NCDEQ again inspected the site, and another diesel fuel release was 
detected at the same location. After a second soil cleanup under the dispenser, the soil 
was tested for Risk‐Based compounds, and the results were sent to the NCDEQ.  A 
Notice of Regulatory Requirements (NORR) was sent to Alamance Oil requiring a Limited 
Site Assessment (LSA). The diesel release is DEQ # 44606‐B.  The NCDEQ letter dated 
June 11, 2019 is presented as Appendix A.  

3.0 RISK CHARACTERIZATION 

To provide the information for Risk Ranking at the site, Pyramid researched the 
surrounding properties within 1000 feet of the site. In total there were over 160 
properties. Pyramid sent over 160 fliers to the surrounding property owners to see who 
is on City water, and if there were any wells. Pyramid also performed a driving and 
walking survey of the area looking for water supply wells. The LSA Risk Classification and 
Land Use Form was completed by Pyramid and is presented as Appendix B.  

The receptors survey did not reveal any active water supply wells within 1,500 feet of 
the gasoline UST. The area is supplied with drinking water by the City of Burlington.  

The results of the receptor survey indicate that there are no active water supply wells 
located within 1,000 feet of the source area (the Gas Station dispenser island).       
Surface water from the site drains to ditches and into an intermittent tributary to an 
unnamed stream about 3,500 feet south of the site. This unnamed creek flows south 
into the Little Alamance Creek located approximately a mile south of the site. There is 
no surface water within 500 feet of the site.  

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4.0 RECEPTOR INFORMATION 

A search for supply wells was conducted by walking and driving the surrounding area, 
and the water supply well locations within 1,500 feet of the site are shown on the aerial 
map presented as Figure 3. Additional information was acquired from discussions with 
local residents and business owners, and the data are reflected in Table 2. 

Pyramid completed a receptor survey for the Alamance Oil Gas Station site. The site is in 
the City of Burlington, and the City provides municipal water to all properties within 
1000 feet of the site.  Over 160 supply well surveys were sent to property owners within 
1,000 feet of the site. The property owner information is included in Table 2. 
Approximately 10 percent of the surveys mailed were completed and returned after a 
45‐day time period. Copies of the completed well surveys are included as Appendix C. 
These surveys and the interviews with local businesses confirm that properties are 
connected to municipal water supply for all uses. The locations of surrounding 
properties within 1,500 feet of the source area are shown on Figure 3. The property 
owner and supply well information for the properties within approximately 1,000 feet 
are provided in Table 2. 

4.1 Water Supply Wells 
As shown on Figure 3, no water active water supply wells were identified within 1,000 
feet of the site. One abandoned well was located east of the site and at a 
topographically higher elevation. This old abandoned well was filled with rocks and had 
no well pump. Another old, unused water supply well was found in an open field about 
1,300 feet north of the site.  

4.2 Public Water Supplies  
The subject site and all properties within 1,000 feet of the site rely on municipal water 
provided by the City of Burlington. 

4.3 Surface Water 
Surface water from the site drains to ditches and into an intermittent tributary to an 
unnamed stream about 3,500 feet south of the site. This unnamed creek flows south 
into the Little Alamance Creek located approximately a mile south of the site. There is 
no surface water within 500 feet of the site.  

4.4 Wellhead Protection Areas 
There are no designated wellhead protection areas within a 1,500‐foot radius of the 
site. 

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4.5 Deep Aquifers in the Coastal Plain Physiographic Region 
This site is not in the Coastal Plain; therefore, this section does not apply to this site. 

4.6 Subsurface Structures 
No shallow subsurface utilities are present in the source area that could act to spread 
contamination. 

4.7 Land Use 
The area on the north side of Webb Avenue is all commercial businesses. The railroad 
track is located about 300 feet north of Webb Avenue.  On the south side of West Webb 
Avenue are mostly residential properties with some commercial businesses to the 
southwest of the site.  

5.0 SITE GEOLOGY & HYDROGEOLOGY  
Pyramid’s review of the 1985 Geologic Map of North Carolina yielded information 
concerning local geology and hydrogeology. Based on this review, the site is in the 
Carolina Slate Belt of North Carolina. The surface geology consists of regional soils 
created by the weathering of the underlying bedrock. According to the 1985 Geologic 
Map of North Carolina, the underlying bedrock beneath the site includes 
metamorphosed granitic rock, map symbol CZg. 

In general, both surface and groundwater flow directions are controlled by topographic 
contours of landforms, with flow occurring perpendicular to the contours from high to 
low elevations. The site elevation is approximately 680 feet above mean sea‐level. 
Surface run‐off from the site generally flows in ditches to the southwest. An unnamed 
intermittent stream flows to an unnamed tributary to Little Alamance Creek about a 
mile from the site. The location of the site relative to surface water is shown in Figure 1. 

6.0 SOIL INVESTIGATION  

For the LSA, the initial soil boring at MW‐1 was used to assess soil near the petroleum 
release location at the off‐road diesel dispenser.  The soil samples were collected using a 
Geoprobe® direct‐push rig and the standard field procedures detailed in Appendix D.   

On October 1, 2019, the soil boring at the location of MW‐1 (B‐1) was completed and 
soil samples were collected using stainless steel macro‐core samplers with clean 
disposable polyethylene  sleeves. Soil samples were selected from various depths for 
field screening with a calibrated Photo‐Ionization Detector (PID). Based on the field 

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screening results and the depth to groundwater in the well, soil samples were preserved 
for laboratory analyses.  The soil description and PID readings are shown on the Boring 
Logs in Appendix E. 

Soil samples were collected from B‐1 at depths of 3‐5 feet, 8‐10 feet, and 10‐13 feet 
below land surface (BLS) for laboratory analysis.  The depth to groundwater measured in 
MW‐1 was 15.1 feet. The soil samples were immediately preserved in laboratory 
containers for analysis at Pace Analytical Service in Huntersville, NC. The analytical 
methods were: 

 EPA Method 8260 for Volatile Organic Compounds (VOCs) 
 EPA Method 8270 for Semi‐Volatile Organic compounds (SVOCs) 
 Massachusetts DEP (MADEP) Method for Volatile Petroleum Hydrocarbons (VPH) 
 MADEP Method for Extractable Petroleum Hydrocarbons (VPH) 

The soil analytical results showed no detections in the 3‐5 foot sample, and results 
greater than the Maximum Soil Contaminant Concentrations (MSCCs) for Soil‐to‐
Groundwater (STGW) regulatory levels in the 8‐10 foot and 10‐13 foot soil samples. 
Although the results were not elevated to the residential MSCC levels, there were 
multiple petroleum compounds detected in soil. Results from the Risk‐Based soil 
sampling are summarized on Table 3, and the Pace Analytical report is presented in 
Appendix F. 

7.0 GROUNDWATER INVESTIGATION 

7.1 Monitoring Well Installation 
To investigate groundwater in the UST area, Pyramid installed one 2‐inch diameter 
monitoring well on October 1, 2019 (MW‐1).  The well was installed to a depth of 30 
feet below land surface (BLS), and the location is shown on Figure 2.  MW‐1 was drilled 
under the pump island canopy using a track‐mounted Geoprobe® and installed with 
solid stem augers. This well was constructed using 20 feet of 2‐inch diameter schedule‐
40 PVC 0.010‐inch slotted screen, and the remaining portion of the well was constructed 
of schedule 40 PVC solid well casing. The well construction data for MW‐1, is included in 
Table 4 and a copy of the well construction record is presented in Appendix E.  

After the groundwater samples from MW‐1 were analyzed by the laboratory, the result 
showed concentrations of benzene above the Gross Contaminant Levels (GCLs). The 
NCDEQ requires the assessment to continue with the completion of an LSA II.  

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On October 24, 2019, Pyramid installed three (3) additional 2‐inch diameter monitoring 
wells. Two down‐gradient monitoring wells (MW‐2 and MW‐3) were installed at the 
southern property boundary along West Webb Avenue. The up‐gradient monitoring well 
(MW‐4) was installed on the northern edge of the gas station site. The well locations are 
shown on Figure 2, and the wells were installed using a track‐mounted Geoprobe® and 
installed with solid stem augers to a depth of 30 feet BLS.  The wells were constructed 
using 20 feet of 2‐inch diameter schedule‐40 PVC 0.010‐inch slotted screen, and the 
remaining portion was constructed of schedule 40 PVC well casing. The well 
construction data for MW‐2, 3 & 4 are included in Table 4 and a copy of the well logs 
and well construction records are presented in Appendix E.  

7.2 Monitoring Well Sampling & Laboratory Analyses 
On October 2, 2019, groundwater samples were collected from monitoring well MW‐1 
for laboratory analyses. Prior to sampling, MW‐1 was gauged to record the depth to 
groundwater and checked for free‐phase petroleum product (free‐product).  No free 
product was detected in MW‐1 and the depth to groundwater measured 15.1 feet 
below the top of the casing. To purge stagnant water and develop each monitoring well, 
approximately 10 gallons of water was removed from the well using a disposable bailer. 
The standard field procedures used by Pyramid are presented as Appendix D. 

The groundwater samples were collected using the disposable bailer and placed in 
laboratory prepared containers, packed in ice, and prepared for shipment to Pace 
Analytical Services in Huntersville, NC. The groundwater samples were analyzed for 
volatile and semi‐volatile organic compounds using: 

 EPA Methods 6200B for Volatile Organic Compounds (VOCs)  
 EPA Method 625 + 10 Peaks for Semi‐volatile Organic Compounds (SVOCs) 
 EPA Method 504.1 for Ethylene Dibromide (EDB 
 MADEP Volatile Petroleum Hydrocarbons (VPH) 
 MADEP Extractable Petroleum Hydrocarbons (EPH) 
 EPA Method 6010 for lead (Pb)  

The results from MW‐1 were evaluated and showed benzene concentrations in the 
groundwater above the Gross Contaminant Levels (GCLs) established by the NCDEQ. 
Based on these results, the NCDEQ requires additional assessment at the site.  

On October 28, 2019, groundwater samples were collected from monitoring wells MW‐
1, 2, 3, & 4, for laboratory analyses. Prior to collecting the groundwater samples, the 
monitoring wells were gauged to record the depth to groundwater and check for free 
product.  No free product was detected in any of the monitoring wells. The depth to 

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groundwater ranged from 14.86 feet to 16.84 feet below the top of the casing. The 
standard field procedures used by Pyramid are presented as Appendix D. The 
groundwater samples collected from MW‐2, 3, and 4 were analyzed for the same 
compounds as before.  Previous sample containers from MW‐1 had been broken during 
shipment, and MW‐1 was resampled for EPA Method 625 analysis.   

7.3 Groundwater Flow Direction 
On October 28, 2019, Pyramid conducted an elevation survey to establish the relative 
top of casing (TOC) elevations for the monitoring wells. Groundwater elevation data 
recorded in the field with the calculated TOC elevations of the monitoring wells are 
presented in Table 5.  The TOC elevation data from the survey was used in conjunction 
with depth‐to‐groundwater measurements to determine the groundwater elevation at 
each monitoring well.  Using the calculated groundwater elevation data for the Type II 
monitoring wells, a potentiometric surface map was prepared for the site and in 
presented as Figure 4. Based on the estimated groundwater surface contours, the 
shallow groundwater flow is to the southwest which agrees with the local topography 
and stream flow observed in the area. 

7.4 Groundwater Analytical Results 
The groundwater analytical results from the four wells showed petroleum contaminant 
concentrations above the North Carolina Administrative Code (NCAC) 2L Groundwater 
Standards. The groundwater concentrations detected are summarized on Table 6 and 
the laboratory reports are presented in Appendix G. The data are reported in 
Micrograms per liter (µg/l). The results of the groundwater sampling are summarized 
below.  

 Monitor well MW‐1 is in the source area and contained elevated concentrations 
of benzene toluene, ethylbenzene, and total xylenes (BTEX). The benzene 
concentrations in this well was greater than the benzene GCL, and many 
compounds were above the NCAC 2L Groundwater Standards. 

 In addition, MW‐1 also contained oxygenates which indicate a gasoline release. 
Methyl tert‐butyl ether (MTBE), isopropyl ether (IPE), Tert‐Amyl Alcohol (TAA), 
and Tert‐Butyl Alcohol (TBA) were detected in MW‐1 at elevated concentrations. 
The oxygenate compounds indicate a gasoline release since these compounds 
are not found in diesel fuel.  

 The lead (Pb), Ethylene Dibromide (EDB), and 1,2‐Dichloroethane (1,2‐DCA) 
normally associated with leaded gasoline releases were not detected in any of 
the monitoring wells.  

Alamance Oil Company, Inc. – Limited Site Assessment (LSA II) 9
Pyramid Project # 2019-210 11/27/2019

 Naphthalene although it was detected at concentrations higher than the NCAC 
2L Groundwater Standard, the levels detected were less than 700 ug/l.  The low 
naphthalene concentrations detected in the source area further indicate a 
gasoline release at the site, as a significant diesel release would be expected to 
have higher naphthalene concentrations.   

 The results of the groundwater sampling indicate that the source area has 
elevated concentrations of petroleum compounds in exceedance of the NCAC 2L 
Groundwater Standards. Benzene was detected above the Gross Contaminant 
Levels (GCLs) in MW‐1 and  MW‐2.  

The laboratory results for the groundwater samples collected in October 2019 are 
summarized on Table 6 and a copy of the laboratory reports and chains of custody is 
presented as Appendix G. Groundwater concentration contours were prepared for 
benzene, MTBE, and naphthalene and are presented as Figures 6, 7, and 8, respectively.  
These analytical data and concentration contours indicate groundwater migration 
downgradient to the southwest in the direction of Webb Avenue. 

8.0 ASSESSMENT SUMMARY  
As requested by T.A.C., Inc., Pyramid has completed the Phase II Limited Site 
Assessment (LSA II) for the Alamance Oil Company Gas Station Site.  A summary of the 
assessment results is presented below.  

 On June 11, 2019, the NCDEQ issued a NORR to Alamance Oil requiring the 
completion of a Limited Site Assessment for the gas station site. 

 In  October 2019, Pyramid completed a receptor survey for the property. No 
active water supply wells were observed within a 1,000‐foot radius of the site. 
Responses from fliers mailed to all properties within 1,000 feet of the site (>160 
fliers) indicate no water supply wells are present and all properties are served by 
municipal water by the City of Burlington.  The risk evaluation showed that the 
entire area surrounding the site relies on municipal water supply.  

 The nearest surface water is approximately 3,500 feet south of the site, and no 
surface water is located within 500 feet of the site. An unnamed intermittent 
stream is located southwest of the site, and surface water flows in the 
intermittent stream to the Little Alamance Creek about a mile south of  the site.  

Alamance Oil Company, Inc. – Limited Site Assessment (LSA II) 10
Pyramid Project # 2019-210 11/27/2019
 The initial groundwater samples in MW‐1 in the source area showed benzene 
concentrations above the GCLs.  No free product was detected in MW‐1.  

 On October 24, monitoring wells MW‐2, MW‐3, & MW‐4 were installed in the 
source area to a depth of 30 feet to assess the groundwater gradient and 
contaminant migration. No free product was detected in the monitoring wells.  

 Monitor well MW‐1 is in the source area and contained elevated concentrations 
of benzene toluene, ethylbenzene, and total xylenes (BTEX). The benzene 
concentrations in this well was greater than the benzene GCL, and many 
compounds were above the NCAC 2L Groundwater Standards. 

 In addition, MW‐1 also contained oxygenates which indicate a gasoline release. 
Methyl tert‐butyl ether (MTBE), isopropyl ether (IPE), Tert‐Amyl Alcohol (TAA), 
and Tert‐Butyl Alcohol (TBA) were detected in MW‐1 at elevated concentrations 
in MW‐1. The oxygenate compounds indicate a gasoline release since these 
compounds are not found in diesel fuel.  

 The lead (Pb), Ethylene Dibromide (EDB), and 1,2‐Dichloroethane (1,2‐DCA) 
normally associated with leaded gasoline releases were not detected in any of 
the monitoring wells.  

 Naphthalene although it was detected at concentrations higher than the NCAC 
2L Groundwater Standard, the levels detected were less than 700 ug/l.  The low 
naphthalene concentrations detected in the source area further indicate a 
gasoline release at the site, as a significant diesel release would be expected to 
have higher naphthalene concentrations.   

 The results of the groundwater sampling indicate that the source area has 
elevated concentrations of petroleum compounds in exceedance of the NCAC 2L 
Groundwater Standards. Benzene was detected above the Gross Contaminant 
Levels (GCLs) in MW‐1 and  MW‐2.  

 The risk classification of the incident should be “intermediate Risk”. 

Based on the findings of this LSA II, the concentrations detected in the monitoring wells 
are above GCL groundwater standards and the plume appears to be migrating to the 
southwest. 

Alamance Oil Company, Inc. – Limited Site Assessment (LSA II) 11
Pyramid Project # 2019-210 11/27/2019

9.0 LIMITATIONS 

This report is prepared for, and made available solely for the use of Alamance Oil 
Company, Inc. and the NCDEQ.  The contents thereof may not be used or relied upon by 
any other person without the express written consent and authorization of Pyramid 
Environmental & Engineering, P.C. (Pyramid). The scope of services for this 
environmental report relies on documented environmental data provided by others. 
The NCDEQ accepted the previous environmental investigations; therefore, these 
reports are counted as reliable in providing historical data for the evaluations in the LSA  
report. The subsurface is inherently heterogeneous and subsurface heterogeneities not 
identified in this limited study may influence COCs in unpredicted ways. Subsurface 
conditions such as groundwater flow, groundwater elevations, and water quality will 
vary over time. The opinions and conclusions in this report are in accordance with 
industry accepted geologic and hydrogeologic practices used at the time and location 
where the report was prepared.  The observations, conclusions, and recommendations 
documented in this report are based on site conditions and information reviewed at the 
time of Pyramid's investigation. Pyramid appreciates the opportunity to provide this 
environmental service. 

FIGURES 

Alamance
Alamance County GIS
Heavy Industrial Development Applicants
APPLIED FOR PERMIT
PERMIT APPROVED
UNDER CONSTRUCTION
October 1, 2019

Owner Name:BERICO FUELS INC
76-334-578865570816GREENSBORO, NC 27405-73422200 E BESSEMER AVENUE
GPIN:PID:
DISCLAIMER:The datasets and maps available are not survey grade or a legal document. They are a best approximation of what is on the ground, but do contain errors. The data comes from various sources nationally, the state of North Carolina, and here in Alamance County. Alamance County will not be held responsible for the misuse, misrepresentation, or misinterpretation of the data or maps. These maps and data are a service provided for the benefit for Alamance County citizens. We constantly strive to improve the quality and expand the amount of data and maps available.
ALAMANCE CO UNTY shall assume no liability for any errors, omissions, or inaccuracies in the information provided regardless of how caused; or any decision made or action taken or not taken by user in reliance upon any information or data furnished hereunder. The user knowingly waives any and all claims for damages against any and all of the entities comprising the Alamance County GIS System that may arise from the mapping data.Date: 10/1/2019
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TABLES 

Table 2  Properties Within 1,000 FeetAlamance Oil Co.1525 W. Webb AvenueBurlington, NC 27217Property IDProperty PIN Owner NameOwner AddressOwner CityOwner State Owner Zip Property AddressSW Yes/No City Water Y/N Distance To Well Comments71‐313‐22584229 PARK AVENUE CHURCH OF CHRIST438 DODSON RDMEBANENC27302 0.7 ACRES ON BROOKLYN ST71‐311‐39670790 CITY OF BURLINGTON ENGINEERING DEPARTMENT425 S LEXINGTON AVEBURLINGTONNC27215 1351 N PARK AVENOYNA71‐315‐6680203 CALTOCAR PROPERTIES LLC102 TURNBURY PLACEELONNC27244 1407‐1417 GRIMES ST74‐326‐100388163 J A LOWE MEMORIAL CHURCH1712 W WEBB AVEBURLINGTONNC27217 1712 W. Webb Street76‐333‐101 471979 IGLESIA DE RESTAURACION ELIM2732 BLANCHE DRBURLINGTONNC27215 1648 W WEBB AVE76‐333‐102 474970 BARBER PROPERTIES OF ALAMANCE3100 LOWE RDELONNC27244 BL 1620 W WEBB AVE76‐333‐133 476768 KATSOUDAS OLYMPIA T1522 SHERWOOD DRBURLINGTONNC27215 1552 & 1546 W WEBB AVE76‐333‐104 477782 KATSOUDAS TRIANTAFILOS G1522 SHERWOOD DRIVEBURLINGTONNC27215 1542 W WEBB AVE76‐333‐127 478639 ANDREWS PROPERTIES OF THEPO BOX 6ALTAMAHAWNC27201 1538 W WEBB AVE76‐333‐128 478676 MOORE SANDRA M1324 KIRPATRICK RDBURLINGTONNC27215 1534 W WEBB AVENOYNA76‐334‐52478928 BESSEMER GROUP INC2200 E BESSEMER AVEGREENSBORONC27405 BL 1549 W WEBB AVE76‐333‐106 479633 BLAND CATHY ELIZABETH1528 WEST WEBB AVENUEBURLINGTONNC27217 1549 W WEBB AVE76‐333‐107 479680 LOPEZ LAURA PATRICIA VAZQUEZ1522 W WEBB AVEBURLINGTONNC272171522 W WEBB AVE76‐333‐100 481002 K C MART INC3002 S MEBANE STBURLINGTONNC27215 1654 W WEBB AVE76‐334‐50482380 RED CAPITAL HOLDINGS LLC1912 ROCKGLEN LNGREENSBORONC27410 BL 1637 W WEBB AVE76‐334‐51486038 LYNCH OIL CO INC1609 WEBB AVEBURLINGTONNC27217 1605 W WEBB AVENOYNA76‐333‐108 570546 JOHNSON INGRID E E1516 W WEBB AVEBURLINGTONNC27215 1516 W WEBB AVE76‐334‐57570816 BERICO FUELS INC2200 E BESSEMER AVENUEGREENSBORONC27405 1525 W WEBB AVENOYNAConfirmed on Site76‐333‐109 571522 IBARRA PABLO I1506 W WEBB AVEBURLINGTONNC27217 1506 W WEBB AVE78‐337‐86572454 SIMPSON DOROTHY P FAMILY TRST*300 TRAIL ONEBURLINGTONNC27215 1436 W WEBB AVENOYNA76‐334‐54572706 BESSEMER GROUP INC2200 EAST BESSEMER AVEGREENSBORONC27405 1511 W WEBB AVE78‐337‐88573122 MOORE DONALD LEE3634 STONEY CREEK CHURCH RDELONNC27244 1418 W WEBB AVE78‐337‐87573410 JIMENEZ REYMUNDO F GARCIA1430 WEST WEBB AVENUEBURLINGTONNC27217 1430 W WEBB AVE76‐334‐55573628 PARKER TIMOTHY DBA JDP ENTERPPO BOX 684BURLINGTONNC27216 1439 W WEBB AVENOYNA78‐337‐89574269 POTEAT PHILLIP ANDREW1412 W WEBB AVENUEBURLINGTONNC27217 HBL 1412 W WEBB AVE77‐335‐200 574631 BARBER SANDRA1410 CAPPOQUIN WAYBURLINGTONNC27215 BL 1421 W WEBB AVE78‐337‐90575225 PATTERSON CAROLYN GOLDSTON1404 W WEBB AVEBURLINGTONNC27217 1404 W WEBB AVE77‐335‐201 575565 B AND H CURB MARKETSP O BOX 2479BURLINGTONNC27216 1417 W WEBB AVE77‐336‐229 576189 PERINIS ANDREW N1313 RIDGECREST AVEBURLINGTONNC27215 1310 & 1316 W WEBB AVE77‐335‐202 576488 YOUNG THOMAS PHILIP400 E HARDEN STGRAHAMNC27253 1403 W WEBB AVE77‐336‐217 577096 PERINIS ELENA E1423 RIDGECREST AVEBURLINGTONNC27215 HBL 1246 W WEBB AVE77‐336‐150 577116 PERINIS ANDREW N1313 RIDGECREST AVEBURLINGTONNC27215 1302 W WEBB AVE77‐335‐205 579269 ANP INC1313 RIDGECREST AVEBURLINGTONNC27215 1247 W WEBB AVE72‐319‐112 488594 JIST INVESTMENTS LLC4699 BOYD WRIGHT ROADBURLINGTONNC27215 1703 N PARK AVE76‐332‐139 379668 WILLIAMS JEFFREY1916 SOMERSET HILLS CTRALEIGHNC27604 HL 310 SOMERS AVE78‐338‐63464916 SUMNER BARRY1012 GARFIELD RDBURLINGTONNC27215 1012 GARFIELD RD78‐338‐62464991 JORDAN H BARNEY1854 JIMMIE KERR RDHAW RIVERNC27258 HL 1543 WICKHAM STNOYNA78‐338‐61B 465847 QUALLS VAN B & KATHY M2183 WALKER AVEBURLINGTONNC27215 HL 1535 & 1539 WICKHAM ST78‐338‐61466716 YARBOROUGH CYNTHIA DAWN1533 WICKHAM STBURLINGTONNC27215 HL 1533 WICKHAM ST78‐338‐74466795 DICICCO DONALD APO BOX 4216BURLINGTONNC27215 HL 1531 WICKHAM ST78‐338‐68A 466949 UPCHURCH PHYLLIS VICTORIA HILL707 N NC 87BURLINGTONNC272171516 & 1518 MELODY LN78‐338‐75467628 CHRISTOPHER JO ANN203 NEW CASTLE DRBURLINGTONNC27215 1527 WICKHAM ST78‐338‐69467869 JEFFERSON GARRY F & CYNTHIA S1510 MELODY LNBURLINGTONNC27215 1510 MELODY LN78‐338‐71468890 METCALF RANDOLPH ALAN405 HAWTHORNE LNBURLINGTONNC27215 HBL 405 HAWTHORNE LN78‐338‐70469807 METCALF RANDOLPH ALAN SR403 HAWTHORNE LANEBURLINGTONNC27215 403 HAWTHORNE LN76‐332‐113 469958 MASSEY BOBBY K & MARGARET4209 BIRCH BRIDGE RDBURLINGTONNC27217313 HAWTHORNE LN76‐332‐126 470537 BLATCHLEY CYNTHIA L1627 MELODY LANEBURLINGTONNC27215 1627 MELODY LN76‐332‐100 470717 CARBAJAL PROPERTIES LLC228 SOUTH MELVILLE STGRAHAMNC27253 302 SOMERS AVE75‐331‐123 471276 ZANGOTSIS JOHN S2211 CANTERBURY DRIVEBURLINGTONNC27215 HL 1614 MELODY LANE75‐331‐115 471300 TYRRELL PAUL D & CAROLINE1618 MELODY CTBURLINGTONNC27215 1618 MELODY LN76‐332‐123 471498 SMITH JUDY P1015 S RIDGE RDBURLINGTONNC272171617 MELODY LN76‐332‐125 471504 KING LARRY APO BOX 579PLEASANT GARDENNC27312 1623 MELODY LN76‐332‐124 471550 GOODMAN PAULA DOZIER1619 MELODY LANEBURLINGTONNC27215 1619 MELODY LN76‐332‐102 471687 FREEMAN ALBERT L & LORI R1065 DUNMORE DRBURLINGTONNC27215 1552 ALBRIGHT AVE76‐332‐101 471711 HERNANDEZ EMANUEL2416 BERKLEY RDBURLINGTONNC27217 1556 ALBRIGHT AVE75‐331‐120 472150 TAYLOR YVONNE V1602 MELODY LNBURLINGTONNC27215 1009 GARFIELD RD
Table 2  Properties Within 1,000 FeetAlamance Oil Co.1525 W. Webb AvenueBurlington, NC 2721775‐331‐116 472243 MANER TIFFANY Y1608 MELODY LANEBURLINGTONNC27215 1608 MELODY LN75‐331‐122 472290 BAUGESS BOYD D & BETSY E412 GLENWOOD AVEBURLINGTONNC27215 HL 1606 MELODY LANE76‐332‐122 472445 ANDREWS HOWARD L SRPO BOX 25BURLINGTONNC27216 1615 MELODY LN76‐332‐103 472634 STOCKWELL RICHARD JAMES1548 ALBRIGHT AVEBURLINGTONNC27215 1548 ALBRIGHT AVE76‐332‐142 472681 LEWIS ROBERT M & ASSOC INC404 GREENFERN COURTBURLINGTONNC27215 1546 ALBRIGHT AVE75‐331‐121473157 TAYLOR YVONNE V1602 MELODY LNBURLINGTONNC27215 1602 MELODY LN76‐332‐120 473377 PATE BRITTANY N1607 MELODY LANEBURLINGTONNC27215 1607 MELODY LN76‐332‐121 473401 JJ LLC1001 BROOKVIEW DRIVEELONNC27244 1611 MELODY LN76‐332‐134 473528 K E P ASSOCIATES LLCATTN:JERRY PITTS JR &KIM PITTS BURLINGTONNC27216 1542 ALBRIGHT AVE76‐332‐135 473585 NARTATEZ ESTRELLA I1540 ALBRIGHT AVEBURLINGTONNC27215 1540 ALBRIGHT AVE76‐333‐129 473787 STRICKLING RAYMOND MICHAEL1545 ALBRIGHT AVEBURLINGTONNC27215 1545 ALBRIGHT AVE76‐333‐119 473802 BAYLIFF JERRY GREEN JR103 LOCHRIDGE DRROXBORONC27573 HBL ALBRIGHT78‐338‐64474052 TATE LORINIA H1008 GARFIELD RDBURLINGTONNC27215 HBL 1008 GARFIELD RD78‐338‐65474086 SLAVIN DAWN ELIZABETH1006 GARFIELD ROADBURLINGTONNC27215 BROOKWOOD SUBD BLK G76‐332‐119 474352 EDWARDS KEITH A219 COLLINWOOD DRBURLINGTONNC27215 1549 ALBRIGHT AVE76‐332‐106 474489 JAYNE MICHAEL1534 ALBRIGHT AVEBURLINGTONNC27215 1534 ALBRIGHT AVE76‐332‐105 474532 RIFE PHILIP D1536 ALBRIGHT AVEBURLINGTONNC27215 1536 ALBRIGHT AVE76‐333‐130 474744 MULLINS JAMES R II3012 TRUITT DRBURLINGTONNC27215 1541 ALBRIGHT AVE78‐338‐67475082 CARNES ROBIN FRANCES1522 MELODY LNBURLINGTONNC27215 1522 MELODY LN78‐338‐66475111 WARNER DARREN DAVID1634 DONCASTER LANEBURLINGTONNC27217 HL 1004 GARFIELD DR76‐332‐140 475219 DUPREE TERESA LOUISE STEELE1531 MELODY LANEBURLINGTONNC27215 HL 1531 MELODY LANE76‐332‐141 475266 OAKLEY NELL PRESNELL LIFE EST1033 RAINEY STBURLINGTONNC27217 1527 MELODY LNNOYN/A76‐333‐125475657 NANCE JAMES D & BOBBIE J1535 ALBRIGHT AVENUEBURLINGTONNC27215 HL 1535 ALBRIGHT AVE76‐333‐117 475700 TERRELL TERRIE1537 ALBRIGHT AVBURLINGTONNC27215 HBL 1537 ALBRIGHT AVE76‐332‐141A 476231 JONES NANCY F1523 MELODY LANEBURLINGTONNC27215 1523 MELODY LN76‐332‐128 476450 MOORE FRANKLIN K & VICKI SP O BOX 352BURLINGTONNC27216 1524 ALBRIGHT AVE76‐333‐126 476614 LYNTHACUM ELVIN WAYNE & LAURA1416 MANCHESTER LNBURLINGTONNC27215 HBL 1531 ALBRIGHT AVE76‐332‐133 477117 HAMLETT MICAH SHAWN1519 MELODY LANEBURLINGTONNC27215 1519 MELODY LN76‐332‐116 477174 ADAMS RENTALS LLC1203 BELMONT STBURLINGTONNC27215 1515 MELODY LN76‐332‐108 477334 KIER LAURIN ROGERS1520 ALBRIGHT AVEBURLINGTONNC27215 HBL 1520 ALBRIGHT AVE76‐332‐132 477390 RDC REAL ESTATE SOLUTIONS INCPO BOX 19511GREENSBORONC27419 1516 ALBRIGHT AVENOYN/A76‐333‐114 477546 GUAMAN JORGE ROBERTO1523 ALBRIGHT AVEBURLINGTONNC27215 HBL 1523 ALBRIGHT AVE76‐332‐114478067 WYNN MICHAEL1509 MELODY LANEBURLINGTONNC272151509 MELODY LN76‐332‐115 478121 ADAMS RENTALS LLC1203 BELMONT STBURLINGTONNC27215 1513 MELODY LN76‐332‐130 478257 RIVERS BONNIE S1512 ALBRIGHT AVEBURLINGTONNC27215 1512 ALBRIGHT AVE76‐333‐131 478497 TRIPLE L PROPERTIES LLCPO BOX 1454GRAHAMNC27273 1517 ALBRIGHT AVE76‐333‐113 478521 SHEPANSKI KAITLYN1519 ALBRIGHT AVEBURLINGTONNC27215 1519 ALBRIGHT AVE76‐332‐112A 479065 TREI LLC5709 GATE CITY BLVD SUITE 202GREENSBORONC27407 311 HAWTHORNE LNNOYN/ACalled in 10/1/1976‐332‐112 479170 MCMASTERS HOWARD LEE & DONNA R307 HAWTHORNE LANEBURLINGTONNC27215 307 HAWTHORNE LN76‐332‐131 479204 HAVERLAND RONALD MPO BOX 1567BURLINGTONNC27216 1510 ALBRIGHT AVENOYN/A76‐332‐110 479251 MASSEY JEAN HEIRS15004 NEW LIGHT RDWAKE FORESTNC27587 1506 ALBRIGHT AVE76‐333‐132 479463 C & C VENTURES11715 S 53 AVEPAPILLIONNE68133 1511 ALBRIGHT AVE78‐337‐116 560784 OKEY EDNA EUGENIA406 HAWTHORNE LANEBURLINGTONNC27215 406 HAWTHORNE LNNOYN/ACalled in 10/1/1978‐337‐80561778 COYNER LIBBY M402 HAWTHORNE LANEBURLINGTONNC27215 402 HAWTHORNE LN78‐337‐81561922 THOMAS JOHN G1772 ROUTH RDBURLINGTONNC27217 314 HAWTHORNE LN78‐337‐96563769 THOMPSON VERNON LEE307 KERNODLE DRBURLINGTONNC27215 307 KERNODLE DR78‐337‐114 563884 TETER DIANA DRU305 KERNODLE DRIVEBURLINGTONNC27215 305 KERNODLE DR78‐337‐115 564902 HOWARD STEPHEN V1405 WILLOW OAK DRBURLINGTONNC27215 221 KERNODLE DR78‐337‐94564918 GRAY MARC C219 KERNODLE DRBURLINGTONNC27215 219 KERNODLE DR77‐336‐91566902 CLAYTON JONATHAN BRAD220 KERNODLE DRIVEBURLINGTONNC27215 220 KERNODLE DR77‐336‐94566927 SMITH DAVID MATTHEW157 SYLVAN SCHOOL RDSNOW CAMPNC27349 HBL 216 KERNODLE DR76‐332‐111 570127 OAKLEY RICKY LPO BOX 10622GREENSBORONC27404 1504 ALBRIGHT AVE76‐333‐124 570333 WALL FAYE B711 E HANOVER RDGRAHAMNC27253 215 HAWTHORNE LN76‐333‐123 570357 DUNNAGAN CHRISTOPHER TPO BOX 27NEWLANDNC28657 211 HAWTHORNE LN76‐333‐110 570473 BREWER BRANDON S1707 PINECREST STBURLINGTONNC27215 209 HAWTHORNE LN78‐337‐82571053 BRITT HUBERT L310 HAWTHORNE LNBURLINGTONNC27215 310 HAWTHORNE LN78‐337‐83571183 JACOBO TEODORO VALERIO ETUX304 HAWTHORNE LANEBURLINGTONNC27215 304 HAWTHORNE
Table 2  Properties Within 1,000 FeetAlamance Oil Co.1525 W. Webb AvenueBurlington, NC 2721778‐337‐84572214 PRICE JOSEPH B214 HAWTHORNE LANEBURLINGTONNC27215 214 HAWTHORNE LN78‐337‐93574033 MOON PAUL RP O BOX 27ELONNC27244 217 KERNODLE DRNOYN/A78‐337‐92574047 ANDREWS VICTOR S & KATHY W6703 FRIEDEN CHURCH RDGIBSONVILLENC27249 213 KERNODLE DR78‐337‐91574154 APPLE RITA LANE5944 MT ZION RDSNOW CAMPNC27349 211 KERNODLE DR77‐336‐96576032 EULISS PATRICIA A214 KERNODLE DRBURLINGTONNC27215 HL 214 KERNODLE DR77‐336‐98576048 PERINIS MINA1428 RIDGECREST AVEBURLINGTONNC27215 HBL 210 KERNODLE DR76‐332‐143 470717 CARBAJAL PROPERTIES LLC228 SOUTH MELVILLE STGRAHAMNC27253 306 SOMERS AVE76‐332‐144 470717 CARBAJAL PROPERTIES LLC228 SOUTH MELVILLE STGRAHAMNC27253 1560 ALBRIGHT AVE73‐320‐131 483684 VINSON JAMES EDWARD ETALPO BOX 463MEBANENC27302 1711 N PARK AVE73‐320‐132 485600 VINSON JAMES EDWARD ETALPO BOX 463MEBANENC27302 1707 N PARK AVE73‐320‐105 486936 CURRY AUDREY BANKS LEA & ETALC/O HUGHES CRISP JRCHARLOTTENC282621.66 ACRES OFF FLORENCE ST72‐319‐124 487732 VIVAR GILDARDO VIDAL1652 ELM STREETBURLINGTONNC27215 1652 ELM ST72‐319‐123 487792 CUNNINGHAM GAIL R1648 ELM STBURLINGTONNC27217 HL 1648 ELM ST71‐314‐25488355 PICHARDO FELIPE JULIAN1637 N PARK AVEBURLINGTONNC27217 1637 N PARK AVE72‐319‐122 488742 LOPEZ JONATHAN J4021 FORBES WAYBURLINGTONNC27215 1644 ELM ST71‐314‐26489352 FAUCETTE AUDREY130 FAUCETTE AVEBURLINGTONNC27215 HL 1615 N PARK AVE72‐319‐121 489702 NGUYEN THUYLAN THI1640 ELM STBURLINGTONNC27217 HL 1640 ELM ST72‐319‐120489782 ARMSTRONG MARGARET P1634 ELM STBURLINGTONNC27217HL 1634 ELM ST71‐312‐34576936 PINNIX REUBIN JR1413 NORTH PARK AVEBURLINGTONNC27217 1413 N PARK AVE71‐312‐35576992 KHALID ABDUL SHAKOOR1500 EGLANTYNE COURTRALEIGHNC27613 1425 N PARK AVE71‐312‐36577868 VITAL JUAN & MA DEL R1419 N PARK AVEBURLINGTONNC27217 1419 N PARK AVE71‐312‐37578825 DEGRAFFENRIED WILMA S LIFE EST310 HIGHLAND AVENUEBURLINGTONNC27217 1411 N PARK AVE71‐312‐38578891 VERA CANDELARIO MERCEDES1309 JACKSON STBURLINGTONNC27217 1403 N PARK AVE71‐312‐14579987 SMITH TODD ALLEN110 B SOUTH MAPLE STGRAHAMNC27253 1406 GRIMES ST71‐314‐27580228 COUSINS SIGNORA MOORE HEIRS419 DOGETT DRGRAHAMNC27253 1621 N PARK AVE72‐319‐119 580763 ALVAREZ JUAN M & MARIA A1630 ELM STBURLINGTONNC27217 HL 1630 ELM ST71‐314‐29581251 GRAVES BRENDA JEAN1535 N PARK AVEBURLINGTONNC27217 1535 N PARK AVENoYNACalled in 10//17/1971‐314‐24581383 MEBANE MARK E305 BROOKLYN STBURLINGTONNC27217 0.44 ACRES ON BROOKLYN ST72‐319‐118 581715 SMITH TRACY LYNN1626 ELM STBURLINGTONNC27217 HL 1626 ELM ST72‐319‐117 581831 URIG LEONA CAROL1620 ELM STBURLINGTONNC27217 HL 1620 ELM ST72‐319‐112B 582465 GRAVES VAN LEE302 BROOKLYN STBURLINGTONNC27217 302 BROOKLYN ST72‐319‐112C 582562 INGRAM PAMELA L306 BROOKLYN STBURLINGTONNC27217 306 BROOKLYN ST72‐319‐112D 582569 CARRANZA JOSE A308 BROOKLYN STREETBURLINGTONNC27217 308 BROOKLYN ST72‐319‐112E 582665 GARCIA LUCIA LOPEZ312 BROOKLYN STBURLINGTONNC27217 HBL 312 BROOKLYN ST72‐319‐111A 582761 RICHMOND ROY314 BROOKLYN STBURLINGTONNC27217 314 BROOKLYN ST71‐313‐30583105 PARK AVENUE CHURCH OF CHRIST438 DODSON RDMEBANENC27302 1531 N PARK AVE71‐313‐32584066 STUTTS ANSEL RAY2410 W FRONT STBURLINGTONNC27215 N PARK AVE72‐317‐116584431 MEBANE MARK EDWARD305 BROOKLYN STBURLINGTONNC27217301 & 305 BROOKLYN AVE72‐317‐122 584544 GOLDSTEIN MICHAEL V309 BROOKLYN STREETBURLINGTONNC27215 309 BROOKLYN ST72‐317‐114 584663 BIGELOW LEA A311 BROOKLYN STBRULINGTONNC27217 HL 311 BROOKLYN ST72‐317‐113C 584752 WATKINS OSTELLA HEIRS315 BROOKLYN STBURLINGTONNC27217 315 BROOKLYN ST71‐313‐33585042 QUALLS HARVEY KEITHPO BOX 1209GRAHAMNC27253 1505 N PARK AVENoYNA71‐313‐19585165 BREWER JOHN LEE2751 WOODBURY DRBURLINGTONNC27217 120 CASWELL ST71‐313‐20585283 GUTHRIE JEANETTE Y HEIRS6180 CANE CREEK COURTSNOW CAMPNC27349 HBL 139 CASWELL ST71‐313‐21585392 CARSON LAURA MCDANIEL6195 TWIN OAKS DR NWOCEAN ISL BCHNC28469 HBL 202 CASWELL ST72‐317‐129 585482 WYRICK LORI ANN306 CASWELL STBURLINGTONNC27217 306 CASWELL ST72‐317‐128A 585581 FLINCHUM TINA LOUISE BROWN3631 BRICK CH RDBURLINGTONNC27215 HL 308 CASWELL ST72‐317‐128585596 SHIELDS ROGERPO BOX 1352MEBANENC27302 310 CASWELL ST72‐317‐130 586611 RODRIGUEZ DORIS E LEON DE3527 GARDEN RDBURLINGTONNC27215 312 CASWELL ST71‐312‐16A 587088 DAVIS SONDRA MARIE1424 GRIMES STBURLINGTONNC27217 1424 GRIMES ST71‐312‐18587113 HERNANDEZ FRANCISCO MENDOZA123 CASWELL STBURLINGTONNC27217 123 CASWELL ST71‐315‐1587370 SHUE KATHY ANN201 CASWELL STBURLINGTONNC27217 HBL 201 CASWELL ST71‐312‐16588054 R & R PROPERTIES OF ELON LLC2967 AMICK RDELONNC27244 1420 GRIMES ST71‐315‐5588278 GENTRY EDDIE WAYNE2540 HUTCHINS MILL LANEHAW RIVERNC27258 1429 GRIMES ST72‐316‐110 588400 EULISS DENNIS H524 W ELM STGRAHAMNC27253 305 & 307 CASWELL ST71‐312‐15589011 SMITH TODD ALLEN110 B SOUTH MAPLE STGRAHAMNC27253 1408 GRIMES ST71‐311‐10671886 BCITY OF BURLINGTON ENGINEERING DEPARTMENT 425 S LEXINGTON AVEBURLINGTONNC27215 1.29 ACRES ON MITCHELL STNoYNA
Industrial Soil to
B-1 3-5 B-1 8-10 B-1 10-13 Commercial Residential Groundwater
Sample Date:10/1/2019 10/1/2019 10/1/2019 MSCC MSCC MSCC
Sample Depth (feet):3-5' 8-10' 10-13' (mg/kg) (mg/kg) (mg/kg)
C5-C8 Aliphatics (x)VPH ND 613 3.6 24,528 939 68
C9-C12 Aliphatics (a)VPH ND 1,020 3.6
C9-C18 Aliphatics (b)EPH ND 21.5 151 4,000 1,500 540
C9-C18 Aliphatics (a-c)+b Sum ND ND ND
C19-C36 Aliphatics (y)EPH ND ND ND 81,000 31,000 CI
C9-C10 Aromatics (c)VPH ND 503 ND
C11-C22 Aromatics (d)EPH ND 20.4 42.3 12,264 469 31
C9-C22 Aromatics (c+d)Sum ND ND ND
Acetone 8260 ND ND ND 360,000 14000 24
Benzene 8260 ND 2.28 0.0275 164 18 0.0056
Bromobenzene 8260 ND ND ND No MSCC No MSCC No MSCC
2-Butanone 8260 ND ND ND No MSCC No MSCC No MSCC
n-Butylbenzene 8260 ND 11.7 ND 16,350 626 4.3
sec-Butylbenzene 8260 ND ND ND 16,350 626 3.3
tert-Butylbenzene 8260 ND ND ND 16,350 626 3.4
Carbon disulfide 8260 ND ND ND 40,880 1564 4.3
4-Chlorotoluene 8260 ND ND ND No MSCC No MSCC No MSCC
Ethylbenzene 8260 ND 48.4 0.0149 40,000 1560 4.9
2-Hexanone 8260 ND ND ND 16,000 6200 1.9
Isopropylbenzene 8260 ND 4.27 ND 40,880 1564 1.7
p-Isopropyltoluene 8260 ND ND ND No MSCC No MSCC No MSCC
Iodomethane 8260 ND ND ND No MSCC No MSCC No MSCC
4-methyl 2-pentanone 8260 ND ND ND No MSCC No MSCC No MSCC
Naphthalene 8260 ND 47.8 0.0093 8,176 313 0.16
n-Propylbenzene 8260 ND 24.2 0.0038 16,350 626 1.7
Styrene 8260 ND 3.13 ND 81,760 3,128 1.5
Trichlorofluromethane 8260 ND ND ND 122,640 4692 29
1,2,3-Tricloropropane 8260 ND 2.33 ND No MSCC No MSCC No MSCC
Toluene 8260 ND 71.6 0.0838 32,000 1200 4.3
1,2,4-Trimethylbenzene 8260 ND 163 0.03 20,440 782 8.5
1,3,5-Trimethylbenzene 8260 ND 54.2 0.0081 20,440 782 8.3
Total Xylenes 8260 0.0132 229 0.0754 81,760 3129 4.6
MTBE 8260 ND ND ND 3100 350 0.091
All Other 8260 Parameters 8260 ND ND ND NA NA NA
Benzo[b]fluoranthene 8270 ND ND ND 8 0.88 1.2
Bis(2-ethylhexyl)phthalate 8270 ND ND ND 410 46 6.6
Chrysene 8270 ND ND ND 780 88 39
Fluoranthene 8270 ND ND ND 16,400 620 290
Fluorene 8270 ND ND ND 16,400 620 47
2-Methyl naphthalene 8270 ND ND ND 1,635 63 3.6
Acenaphtylene 8270 ND ND ND 12,264 469 11
Dibenzofuran 8270 ND ND ND 1,635 62 4.7
Naphthalene 8270 ND ND ND 8,176 313 0.16
Phenanthrene 8270 ND ND ND 12,264 469 56
Pyrene 8270 ND ND ND 12,264 469 270
All Other 8270 Parameters 8270 ND ND ND NA NA NA
Total Chromium 6010 ND ND ND ND 47 1226
Total Lead 6010 ND ND ND ND 400 400
mg/kg = parts per million (ppm).ND = Not detected above the Laboratory Quantitative Limits
BOLD values exceed the Soil to GW MSCCs NAP = Not Analzyed for this parameter
MSCC = Maximum Soil Contaminant Concentratio
CI = Considered Immobile
EPA Method 8270 (mg/kg)
NA = Not Applicable
EPA Method 6010 (mg/kg)
Analytical Parameter Method
Pyramid Job #2019‐210
TABLE 3
 Risk‐Based Soil Analytical Results 
1525 W. Webb Ave,Burlington , NC
Sample Number
EPA Method 8260 (mg/kg)
VPH & EPH (mg/kg)
Pyramid Environmental
Job Number #2019-210
Monitoring Well Well Riser Screen Grout Bentonite Sand Date
Well Depth Diameter Interval Interval Interval Interval Interval Constructed
(feet) (inches) (feet) (feet) (feet) (feet) (feet)
MW-1 30 2 0-10 10-30 0-3 3-4 4-30 10/01/19
MW-2 30 2 0-10 10-30 0-3 3-4 4-30 10/29/19
MW-3 30 2 0-10 10-30 0-3 3-4 4-30 10/29/19
MW-4 30 2 0-10 10-30 0-3 3-3.5 4-30 10/29/19
TABLE 4
Monitoring Well Construction Details
Alamance Oil Company
Burlington, North Carolina
1525 W. Webb Ave.
TOP OF DEPTH TO FREE- FREE- ADJUSTED
WELL CASING DATE DEPTH TO FREE- PRODUCT PRODUCT DEPTH TO GROUNDWATER
NUMBER ELEVATION MEASURED WATER PRODUCT THICKNESS ADJUSTMENT GROUNDWATER ELEVATION(Feet)(Feet) (Feet) (Feet) (Feet)(Feet)(Feet)
10/28/2019 15.59 0.00 0.00 0.00 15.59 84.41
10/28/2019 14.86 Dry 0.00 0.00 14.86 83.91
10/28/2019 14.58 0.00 0.00 0.00 14.58 84.91
10/28/2019 89.43 0.00 0.00 0.00 89.43 16.84
NG = Not Gauged
Datum is top of casing elevation at MW-1 which is set at elevation = 100.00'.
TABLE 5
GROUNDWATER ELEVATION DATA
Alamance Oil Company
1525 W. Webb Avenue, Burlingon, NC
NCDEQ Incident #44606
MW-4 106.27
MW-1 100.00
MW-2 98.77
MW-3 99.49
Page 1 of 1
NCAC 2L
PARAMETER UNITS DATE Groundwater GCLs
MW-1 MW-2 MW-3 MW-4
Standards
EPA Method 6200B
10-02-19 17,100 --- --- ---
Benzene ug/l 10-28-19 NS 14,200 394 614 1 5,000

10-02-19 26,600 --- --- ---
Toluene ug/l 10-28-19 NS 36,500 42.6 59.2 600 260,000
10-02-19 1,930 --- --- ---
Ethylbenzene ug/l 10-28-19 NS 2,210 22.4 551 600 84,500
10-02-19 8,480 --- --- ---
Total Xylenes ug/l 10-28-19 NS 11,410 196.4 1,373 500 85,500
10-02-19 54,110 --- --- ---
Total BTEX ug/l 10-28-19 NS 64,320 655 2,597 NO NO

MTBE 10-02-19 17,100 --- --- ---
Methyl Tert -ug/l 10-28-19 NS 790 248 126 20 20,000
Butyl Ether
10-28-19 ND --- --- ---
Bromodicloromethane ug/l 10-28-19 NS ND ND 38.3 0.6 600

(IPE)10-02-19 5,730 --- --- ---
Isopropyl Ether ug/l 10-28-19 NS 1,330 22.7 31.8 70 70,000
(Diisopropyl ether)
10-02-19 ND ---------
Dibromocloromethane ug/l 10-28-19 NS ND ND 22.4 0.4 400
10-02-19 577 --- --- ---
Naphthalene ug/l 10-28-19 NS 665 33 439 6 6,000
10-02-19 ND --- --- ---
1,2- Dichloroethane ug/l 10-28-19 NS ND ND ND 0.4 400
10-02-19 1,130 ---------
1,2,4-trimethylbenzene ug/l 10-28-19 NS 1,280 64.3 1,100 400 28,500
10-02-19 ND ---------
1,3,5-trimethylbenzene ug/l 10-28-19 NS 284 13 263 400 28,500
10-02-19 ND --- --- ---
Methylene Chlordie ug/l 10-28-19 NS NS ND 30.2 5 5,000
10-02-19 ND ---------
n-Propylbenzene ug/l 10-28-19 NS 145 10.9 89.4 70 30,000
10-02-19 ND --- --- ---
Ethylene Dibromide ug/l 10-28-19 NS ND ND ND 0.02 50
(EDB)
10-02-19 ND ---------
Chloroform ug/l 10-28-19 NS 389 ND 132 70 70,000
Monitoring Well Groundwater Analytical Results
TABLE 6
Alamance Oil
MONITORING WELLS
Page 1 of 2
NCAC 2L
PARAMETER UNITS DATE Groundwater GCLs
MW-1 MW-2 MW-3 MW-4
Standards
Monitoring Well Groundwater Analytical Results
TABLE 6
Alamance Oil
MONITORING WELLS
Oxygenates
10-02-19 ND --- --- ---
Ethanol ug/l 10-28-19 NS ND ND ND 4000 4000000
10-02-19 89,900 --- --- ---
tert-Amyl Alcohol ug/l 10-28-19 NS ND ND ND 40 40000
(TAA)
10-02-19 ND --- --- ---
tert-Amyl Methyl Ether ug/l 10-28-19 NS ND ND ND 128 128000
(TAME)
10-02-19 6,260 --- --- ---
tert-Butyl Alcohol ug/l 10-28-19 NS ND ND ND 10 10000
(TBA
10-02-19 ND --- --- ---
All other ug/l 10-28-19 NS ND ND ND NO NO
6200B Compounds
EPA Method 504.1
10-02-19 ND ---------1,2-Dibromomethane
(EDB)ug/l 10-28-19 NS ND ND ND NO NO
MADEP EPH
10-02-19 ND --- --- ---
Aliphatic (C09-C18)ug/l 10-28-19 NS ND ND ND NO NO
10-02-19 ND --- --- ---
Aliphatic (C9-C36)ug/l 10-28-19 NS ND ND ND NO NO
10-02-19 535 --- --- ---
Aromatic C11-C22 ug/l 10-28-19 NS 444 134 731 NO NO
MADEP VPH
10-02-19 125,000 --- --- ---
Aliphatic (C05-C08)ug/l 10-28-19 NS 113,000 2,490 1,960 NO NO
10-02-19 24,600 --- --- ---
Aliphatic (C9-C12)ug/l 10-28-19 NS 30,800 648 6,770 NO NO
10-02-19 8,910 --- --- ---
Aromatic C09-C10 ug/l 10-28-19 NS 12,000 323 3,520 NO NO
EPA Method 601D
10-02-19 ND --- --- ---
Lead ug/l 10-28-19 NS ND ND ND 15 15000
EPA Method 625.1
10-02-19 --- --- ---
Phenol ug/l 10-28-19 ND 11.8 ND ND 30 30,000
10-02-19 --- --- ---
Napthalene ug/l 10-28-19 NS 350 18.4 143 6 6,000
*All other 625.1 compounds were below MDLs
NS #NAME?
BRL / ND = Not Detected
--- = Well was not installed.
Page 2 of 2

APPENDIX   A 

Notice of Regulatory Requirements 

June 11, 2019

Alamance Oil Company
Attention: Ms. Kim McKinney
1525 West Webb Avenue
Burlington, North Carolina 27217

Re: Notice of Regulatory Requirements
15A NCAC 2L .0405
Risk-based Assessment and Corrective Action for
Petroleum Underground Storage Tanks

Alamance Oil Company Store-B
1525 West Webb Avenue, Burlington
Alamance County
Incident number:44606
Risk Classification: Unknown

Dear Ms. McKinney:

The Soil Excavation/ Initial Abatement Action Report received by the UST Section, Division of Waste
Management, Winston-Salem Regional Office on April 23, 2018 has been reviewed. The report indicates
that soil contamination exceeds the lower of the residential or soil-to-groundwater maximum soil
contaminant concentrations (MSCCs) established in Title 15A NCAC 2L .0411. Therefore, the UST
Section hereby confirms that you must comply with assessment and reporting requirements of Title 15A
NCAC 2L .0405.

The requirements of Title 15A NCAC 2L .0405 include the preparation and submittal of a Limited Site
Assessment (LSA) Report, in accordance with the rule and the most recent version of the Guidelines for Assessment and Corrective Action for UST Releases, within 120 days of discovery of the release.

Because a release or discharge has been confirmed, a Licensed Geologist or a Professional Engineer,
certified by the State of North Carolina, is required to prepare and certify all reports submitted to the
Department of Environmental Quality in accordance with Title 15A NCAC 2L .0103(e) and 2L .0111(b).

Please note that before you sell, transfer, or request a “No Further Action” determination for a property that
has not been remediated to below “unrestricted use” standards, you must file a Notice of Residual Petroleum
("Notice") with the Register of Deeds in the county where the property is located (NCGS 143B-279.9 and
143B-279.11).

Failure to comply with the State's rules in the manner and time specified may result in the assessment of
civil penalties and/or the use of other enforcement mechanisms.

If you have any questions regarding trust fund eligibility or reimbursement from the Commercial or
Noncommercial Leaking Petroleum Underground Storage Tank Cleanup Funds, please contact the UST
Section Trust Fund Branch at [phone]. If you have any questions regarding the actions that must
be taken or the rules mentioned in this letter, please contact me at the address or telephone number listed
below.

Sincerely,

Mindy Lepard
Hydrogeologist
Winston-Salem Regional Office
UST Section, Division of Waste Management, NCDEQ

cc: Alamance County Health Department
Mr. Michael Jones, Pyramid Environmental, via email

Winston-Salem Regional Office | 450 West Hanes Mill Road | Suite 300 | Winston-Salem, NC 27105 | [phone]

APPENDIX   B 

Limited Site Assessment Report

________________________________________________________________________________________________________
LSA – Alamance Oil – 1525 W. Webb Ave, Greensboro, NC Page 1
PYRAMID ENVIRONMENTAL & ENGINEERING, P.C. 11/27/19

Limited Site Assessment Risk Classification and Land Use Form

Part I – Groundwater/Surface Water/Vapor Impacts
High Risk
1. Has the discharge or release contaminated any water supply well including any used for
non-drinking purposes? YES/NO
If yes, explain.

No active supply wells were located within 1000 feet. All properties within 1,500 feet are
provided with water from the City of Burlington.

2. Is a water supply well used for drinking water located within 1000 feet of the source area
of the discharge or release? YES/NO

3. Is a water supply well used for any purpose (e.g., irrigation, washing cars, industrial
cooling water, filling swimming pools) located within 250 feet of the source area of the
release or discharge? YES/NO

4. Does groundwater within 500 feet of the source area of the discharge or release have the
potential for future use in that there is no other source of water supply other than the
groundwater? YES/ NO
Explain.
All property around the site are provided water from the City of Burlington.

5. Do vapors from the discharge or release pose a threat of explosion because of
accumulation of the vapors in a confined space or pose any other serious threat to public
health, public safety, or the environment? YES/NO
If yes, explain.

6. Are there any other factors that would cause the discharge or release to pose an imminent
danger to public health, public safety, or the environment? YES/NO
If yes, explain.

Limited Site Assessment Report

________________________________________________________________________________________________________
LSA – Alamance Oil – 1525 W. Webb Ave, Greensboro, NC Page 2
PYRAMID ENVIRONMENTAL & ENGINEERING, P.C. 11/27/19

Intermediate Risk

7. Is a surface water body located within 500 feet of the source area of the discharge or
release? YES/ NO
A small intermittent stream is located 370 feet southwest of the site. The intermittent stream
lead to an unnamed stream at about 3,500 feet south of the site. This stream flows to Little
Alamance Creek about 1 mile from the site.

If yes, does the maximum groundwater contaminant concentration exceed the surface
water quality standards and criteria found in 15A NCAC 2B .0200 by a factor of 10?
YES/NO
Not applicable

8. Is the source area of the discharge or release located within a designated wellhead
protection area as defined in 42 USC 300h-7(e)? YES/NO
If yes, explain.

9. Is the discharge or release located in the Coastal Plain physiographic region as designated
on a map entitled “Geology of North Carolina” published by the Department in 1985?
YES/NO

If yes, is the source area of the discharge or release located in an area in which there is
recharge to an unconfined or semi-confined deeper aquifer that is being used or may be
used as a source of drinking water? YES/NO
If yes, explain.
Not applicable.

10. Do the levels of groundwater contamination for any contaminant exceed the gross
contamination levels established (see Table 7) by the Department. YES/NO

Limited Site Assessment Report

________________________________________________________________________________________________________
LSA – Alamance Oil – 1525 W. Webb Ave, Greensboro, NC Page 3
PYRAMID ENVIRONMENTAL & ENGINEERING, P.C. 11/27/19

Part II - Land Use
Property Containing Source Area of Discharge or Release
The questions below pertain to the property containing the source area of the release.
1. Does the property contain one or more primary or secondary residences (permanent or
temporary)? YES/NO
Explain.

2. Does the property contain a school, daycare center, hospital, playground, park, recreation
area, church, nursing home, or other place of public assembly? YES/NO
Explain.

3. Does the property contain a commercial (e.g., retail, warehouse, office/business space,
etc.) or industrial (e.g., manufacturing, utilities, industrial research, and development,
chemical/petroleum bulk storage, etc.) enterprise, an inactive commercial or industrial
enterprise, or is the land undeveloped? YES/NO
Explain.

4. Do children visit the property? YES/NO
Explain.

The back part of the property is restricted by fencing . The gas station access is
unrestricted and is concrete paved. Children can visit the gas station area.

5. Is access to the property reliably restricted consistent with its use (e.g., by fences, security
personnel or both)? YES/NO
Explain.

The back part of the property is surrounded by fences and gates and is paved. The gas
station in the front is concrete paved.

6. Do pavement, buildings, or other structures cap the contaminated soil? YES/ NO
Explain.
The source area near the USTs and dispenser island is capped with concrete.

If yes, what mechanisms are in place or can be put into place to ensure that the
contaminated soil will remain capped in the foreseeable future?
The contaminated soil is under concrete.

Limited Site Assessment Report

________________________________________________________________________________________________________
LSA – Alamance Oil – 1525 W. Webb Ave, Greensboro, NC Page 4
PYRAMID ENVIRONMENTAL & ENGINEERING, P.C. 11/27/19

7. What is the zoning status of the property?

The property is zoned “Commercial”

8. Is the use of the property likely to change in the next 20 years? YES/NO
Explain.
NO

Property Surrounding Source Area of Discharge or Release
The questions below pertain to the area within 1500 feet of the source area of the discharge or
release (excludes property containing source area of the release):

11. What is the distance from the source area of the release to the nearest primary or
secondary residence (permanent or temporary)?

Source area is approx. 115 feet from a house across Webb Avenue.

12. What is the distance from the source area of the release to the nearest school, daycare
center, hospital, playground, park, recreation area, church, nursing home or other place of
public assembly?

A church is located approximately 0.1 miles southeast of the site.

13. What is the zoning status of properties in the surrounding area?
The zoning is all commercial along the north side of N. Webb Avenue. The zoning
is residential and commercial on the south side W. Webb Avenue

14. Briefly characterize the use and activities of the land in the surrounding area.

Commercial businesses are located to the west, north, and east of the gas station site.
Residential properties are located to the south across Webb Avenue.

APPENDIX   C 

APPENDIX   D 

Standard Field Procedures: Revision 10.3 Page 1
Pyramid Environmental & Engineering, P.C. Revision date 11-11-2016
Standard Field Procedures
Pyramid Environmental & Engineering, P.C.
________________________________________________________________________
1.0 Equipment Decontamination Equipment decontamination is essential to assure representative environmental samples are collected and to eliminate the potential for cross-contamination between sample points. Pyramid strives to clean all field equipment prior to leaving the office; however, field decontamination is still required on most projects. The procedures for decontamination of water level probes, hand augers, sampling probes, trowels, and other field equipment are listed below.

1.1 EPA Region IV Decontamination Procedures Drilling and soil sampling equipment is decontaminated prior to each use using a pressure washer or steam cleaner. Reusable sampling equipment (hand augers, sampling probes,
trowels, split spoon samplers, water sampling equipment, etc.…) are decontaminated using the general procedure described below.
 Wash with non-phosphate detergent and water, brush to remove particulate matter
 Rinse with tap water
 Rinse with 10 percent nitric acid solution (only if sampling for metals)
 Rinse with de-ionized water
 Rinse with pesticide-grade isopropyl alcohol
 Rinse with de-ionized water
 Air-dry as long as possible The level of decontamination used is appropriate to the analytical parameters selected and the material of the sampling device being used for sampling. For example, if metals analyses are required, then the 10 % nitric acid solution is used for decontamination of stainless-steel equipment. Pyramid uses de-ionized or distilled water for decontamination. Equipment that is not used immediately after decontamination is wrapped in aluminum foil prior to storage.

2.0 Soil Borings & Sampling

2.1 Soil Borings Soil borings are used by Pyramid to characterize the subsurface at many sites. The borings provide information concerning soil types and density, depth to refusal, depth to bedrock, organic vapors that may be present, and can be used to obtain samples for laboratory analysis. Pyramid conducts borings in several different ways, using hand augers, direct-push equipment (Geoprobe), sample probes, split-spoon samplers (ASTM D 1586-84), auger
drilling, air drilling, and Vibro-Core. The following procedures are used by Pyramid Environmental when performing soil borings: 1. Soil boring locations are chosen, and the utility locating service is called to mark all
public utilities. Pyramid also locates private utilities at many project sites using Pyramid locating equipment or a private utility locating service.
Standard Field Procedures: Revision 10.3 Page 2
Pyramid Environmental & Engineering, P.C. Revision date 11-11-2016
2. Down hole drilling equipment is cleaned prior to use and between borings using
pressure washing or steam cleaning. Additional decontamination procedures in Section 1.1 are used for quality assurance for sampling tools such as split spoons or direct-push points. 3. Soil borings are advanced using direct-push, drilling rigs, hand augers, or other appropriate means. 4. Soil samples are normally collected at a minimum of 5-foot intervals. Each sample is divided into two parts. Soil samples for laboratory analyses are jarred from the initial sample volume. The remaining soil is stored in a sealed container for headspace analysis with an organic vapor analyzer (OVA). 5. After screening the soil with the field instruments, each soil sample is described by the field geologist and a geologic description is recorded in project documentation.
6. Soils are typically described in the field by the project geologist or soil scientist and are classified according to the Unified Soil Classification System (ASTM D 2488-84).
7. Soil samples selected for laboratory analysis are placed in properly prepared, laboratory supplied containers and immediately packed in a cooler on ice. Sample
custody is maintained using standard chain-of-custody procedures through delivery to the analytical laboratory. 8. Soil borings, which are not completed as monitoring wells, are grouted using a Portland cement, bentonite, or backfilled with soil cuttings. 9. Where appropriate, soil cuttings are spread near the soil boring or well site in most instances. In rare instances, drill cuttings will be containerized and disposed off-site after waste determination has been made.
2.2 Headspace Screening Soil samples are routinely screened for volatile organic compounds (VOCs) which may be an indication of organic or petroleum hydrocarbon contamination. The typical screening procedure includes immediately transferring the soil from the sampling devices to a sealed container (sealed plastic bag). The soil container is filled approximately halfway with soil and sealed. This creates headspace above the soil in which VOCs may accumulate. The container is allowed to stand for 5 to 15 minutes for the VOCs to equilibrate in the headspace of the container. The headspace of the container is then screened using a calibrated organic vapor analyzer (PID or FID). The screening is conducted by cracking the seal only enough to allow insertion of the probe into the headspace so as not to dilute the sample. In most cases where the contaminant of concern includes volatile organics, the highest or “Peak“ field-screening result is documented for each sample. The soil samples showing the highest reading from each boring are typically selected for laboratory analysis.

Standard Field Procedures: Revision 10.3 Page 3
Pyramid Environmental & Engineering, P.C. Revision date 11-11-2016
2.3 Soil Sample Collection for Laboratory Analysis After the targeted depth has been reached, soil samples are collected using a variety of
sampling devices. Soil sample devices used include split-spoons, stainless-steel hand augers, stainless-steel sampling scoops, and directly from the center of the excavator bucket. The sample technician uses appropriate disposable sampling gloves, which are changed between samples to avoid cross-contamination of samples. Each sampling device is decontaminated prior to use. Only laboratory provided containers are used for sample collection. Samples are collected in accordance with the preservation methods required by
the requested analytical method. Samples are handled as little as possible and preserved in the field as specified for the analytical method. The samples are stored and transported to the laboratory in an insulated cooler chilled to approximately 4 degrees centigrade. The samples are labeled with a minimum of the following information: project name or number, sampler name, date collected, sample number, and analysis requested. Sample custody is maintained using standard chain-of-custody procedures through delivery to the analytical
laboratory. Notes of the sampling events are recorded in bound field notebooks.

2.4 Sediment Sample Collection for Laboratory Analysis Near surface sediment may be present in a surface water stream or dry intermittent stream
bed. Sediment samples are typically soil related samples and may be collected with a variety of sampling tools. Pyramid will use stainless-steel samplers which have been decontaminated according to the procedure detailed in section 1.1 of this document. After
the sediment samples are collected, the location, depth, conditions, and sample composition are documented in the project records. The samples will be screened in the field to detect volatile organic vapors and visually examined for contamination. Sediment samples will be
preserved in laboratory prepared containers in accordance with sample preservation recommendation of the analytical laboratory. Samples are handled as little as possible and preserved in the field as specified for the analytical method. The samples are stored and transported in an insulated cooler chilled to approximately 4 degrees centigrade. The samples are labeled with a minimum of the following information: project name or number, sampler name, date collected, sample number, and analysis requested. Sample custody is maintained using standard chain-of-custody procedures through delivery to the analytical laboratory. Documentation of the sampling events are recorded in bound field notebooks.

3.0 Direct-Push Sampling Procedures Direct-push sampling techniques have been used at many sites to collect soil and groundwater samples rapidly and inexpensively. Track-mounted, direct-push rigs can access hard to reach areas and allow borings and monitoring wells to be installed. Pyramid has used this technology to the benefit of our clients at many project sites. For soil sampling, typically, the direct-push steel drive tube is decontaminated using a pressure washer, and a new plastic sample liner is inserted in the steel drive tube to collect soil samples. If necessary, the stainless-steel sampling tube is decontaminated using Region IV decontamination procedures presented in Section 1.1. The soil samples are collected in
new polyethylene sample tubes within the steel drive tube. The soil samples are then extracted from the polyethylene liner and preserved as required for the appropriate laboratory analysis.
Standard Field Procedures: Revision 10.3 Page 4
Pyramid Environmental & Engineering, P.C. Revision date 11-11-2016
For Groundwater sampling, a steel probe with a retractable screen section and tubing are driven to depth and the screened section is opened to allow groundwater to enter the tubing.
The water samples are withdrawn using new polyethylene tubing with either a decontaminated stainless-steel check ball, or peristaltic pump. The groundwater sample is placed directly into the appropriate laboratory containers and sealed immediately. To prevent cross-contamination of samples, new disposable tubing is used for each groundwater sample point. Disposable nitrile gloves are worn by field personnel during development and groundwater sampling, and gloves are changed between samples. Groundwater sampling procedures are detailed more in Section 5.0, as appropriate for each analytical method.

4.0 Monitoring Well Installation Groundwater monitoring wells are installed in many subsurface environments; sedimentary, Piedmont saprolite, and mountain terrains to list a few. Formations encountered include
unconsolidated and consolidated sediments, saprolitic and weathered rock formations, and bedrock. Groundwater monitoring wells provide a stable sampling point at discrete intervals within the confined or unconfined aquifers. Monitoring wells are installed for a number of reasons, and are typically installed as 1-inch, 2-inch, 4-inch, or 6-inch diameter wells. Construction may be of PVC or other appropriate materials. The following procedures are used by Pyramid when performing borings and monitoring well installations.
 If required, monitoring well permits are obtained from the State, County, or City.
 Boring and monitoring well locations are chosen, and utilities are marked by the public utility locating company. As needed, the drill locations may also be scanned for utilities using a private utility locating company.
 In selecting a drill site, care is taken to avoid overhead power lines, and subsurface
utilities whenever possible.
 Down hole drilling equipment is decontaminated prior to use and between borings.
 Borings are advanced using direct-push, drilling rigs, hand augers, solid-stem augers, hollow-stem augers, air rotary drilling, or air hammer drilling.
 Soil samples are normally collected at a minimum of 5-foot intervals. Each sample is divided into two parts. Soil samples for laboratory analyses are jarred from the initial sample volume. The remaining soil is stored in a sealed container for headspace analysis with an organic vapor analyzer (OVA).
 After screening the soil with the field instruments, each soil sample is described by the field geologist and a geologic description is recorded in the field notes.
Type II monitoring wells are usually installed using 2-inch diameter schedule 40 PVC riser and 2-inch, 0.010-inch machine slotted well screen. The screened interval varies with the purpose of the well, and well details are presented with the boring logs.
Type III wells are usually installed as double-cased wells to monitor the deeper portions of the aquifer. The first casing is usually a 6-inch diameter casing drilled to bedrock or an
appropriate depth within the saprolite. The 6-inch diameter casing is then set and grouted in the borehole. After the cement grout has set for 12 to 24-hours, the borehole is completed to the desired depth using air rotary or an air hammer drilling. The Type III monitoring well is
usually constructed of 2-inch diameter SCH 40 PVC casing and 2-inch diameter SCH 40 PVC 0.010-inch slotted well screen.
Standard Field Procedures: Revision 10.3 Page 5
Pyramid Environmental & Engineering, P.C. Revision date 11-11-2016
In most applications, a sand filter pack of #2 well sand (or appropriately sized well sand) is typically installed to a level of 2 feet above the top of the screen in each well. A minimum 2-
foot thick bentonite seal is usually placed on top of the filter pack and hydrated with de-ionized or distilled water. The remaining annular space of a typical well is backfilled to grade with a Portland cement/bentonite grout. In monitoring wells where the water table is close to surface, the amount of sand above the screen and bentonite will be reduced to allow for a minimum of 2–3 feet of cement grout in the well bore. At the surface, each well is usually secured with a locking cap and a steel well protector set in a 2 by 2 foot concrete pad. In some cases, stick-up well protectors are used to secure the well and allow the well to be more easily located in wooded or open areas. Each groundwater monitoring well is developed by surging, pumping, or bailing to remove sediment before sampling. Water removed during development is managed according to regulatory standards.

5.0 Water Sampling Procedures Pyramid relies on water sampling as a primary method for assessment of subsurface conditions. Water sampling typically includes sampling groundwater from monitoring wells, supply wells, surface water bodies, waste pits, sumps, etc. The following provides typical
sampling procedures for the major sample types.

5.1 Monitoring Wells Prior to sampling each monitoring well, depth to product/groundwater and total well depth are measured using a properly decontaminated electric interface probe. This information is recorded in the field record and the volume of the water in the well casing is calculated. To purge stagnant water from each monitoring well, five well casing volumes of water are removed from each well, or until the field parameters pH, conductivity, dissolved oxygen, and temperature have stabilized. If the water in the monitoring well is removed until the well is dry, then the well is sampled thereafter. Water removed from wells during purging is managed in accordance with regulatory guidance. Depending on project requirements, temperature, pH, specific conductance, dissolved oxygen, and other parameters may be measured prior to sampling.
Groundwater samples are typically collected using a new disposable polyethylene bailer and a new length of nylon cord. To prevent cross-contamination of samples between wells, a
new disposable bailer is used for each well. A new pair of disposable gloves is worn by field personnel during purging and sampling, and is changed between wells. In the case of small diameter monitoring wells or direct-push water samples, water samples may be collected
using a peristaltic pump and new polyethylene tubing. Another method is to use a segment of new polyethylene tubing and a stainless-steel check ball to create a “Tube Bailer”.
Groundwater samples selected for laboratory analysis are placed in properly prepared, laboratory supplied containers and immediately preserved in a cooler on ice. Samples are maintained under standard chain-of-custody procedures from sample collection through laboratory analysis.
Standard Field Procedures: Revision 10.3 Page 6
Pyramid Environmental & Engineering, P.C. Revision date 11-11-2016
5.2 Water Supply Well Sampling Procedures Prior to sampling each water supply well, the well owner is contacted to provide access to
the well. The well owner is interviewed to find the faucet closest to the well for sampling. If there are no faucets located on the well, then water from an outside faucet is usually sampled. If there are no outside faucets available, then the water samples are collected from an inside faucet. The location of the sample is recorded in the field book. The owner is interviewed to see if there is a chlorination system on the well, or if the well has
been recently chlorinated. Recent chlorination could affect the laboratory detection limits. In most cases, the samples are preserved using sodium thiosulfate or ascorbic acid to remove the interactions of chlorine, which may be present in the samples. To purge stagnant water from the water supply well system, the faucet is allowed to run on full stream for a minimum of 15 minutes. The aerator is removed from the tap if one is
present. Water removed from wells during purging is managed according to regulatory standards. Supply well samples are collected using appropriate laboratory prepared containers for each analysis. The analytical methods selected will vary with the contaminant of interest. To prevent cross-contamination of samples between wells, disposable latex gloves are worn by field personnel during purging and sampling and are changed between wells. It is possible that samples may be required at several places within the water supply system. The samples
will be collected accordingly and labeled to show the source and location sampled. Supply well samples selected for laboratory analysis are placed in properly prepared, laboratory supplied containers and immediately packed in a cooler on wet ice, and chilled to approximately 4 degrees Celsius. Samples are maintained under strict control using standard chain-of-custody procedures through laboratory analysis.

5.3 Surface Water Sampling Surface water samples are obtained using several techniques including use of sample bailers, sample scoops, from boats, bridges, or wading into a stream. Caution should always be used when sampling surface water to ensure that the water collected is representative of the conditions. Since stream or open water sampling is transient, careful documentation of the site conditions is required.
In many studies, additional samples from upstream and downstream of the desired sample point are required. Surface water sampling must be planned to reflect the desired conditions
during sampling. The general procedures are similar to the supply well sampling procedures detailed above. Appropriate laboratory prepared containers are used for each analysis. The analytical methods selected will vary with the contaminant of interest.
To prevent cross-contamination of samples between samples, disposable latex gloves are worn by field personnel during purging and sampling and are changed between samples. It
is possible that samples may be required at several places along the stream to check for influences of up-stream facilities.
Standard Field Procedures: Revision 10.3 Page 7
Pyramid Environmental & Engineering, P.C. Revision date 11-11-2016
The samples will be collected accordingly and labeled to show the source and location sampled. Sample will always be collected upstream of the area disturbed by the person
sampling the stream. Surface water samples selected for laboratory analysis are placed in properly prepared, laboratory supplied containers and immediately packed in a cooler on ice. Samples are maintained under strict control using standard chain-of-custody procedures through laboratory analysis.

6.0 Quality Assurance / Quality Control The decontamination procedures listed above have been implemented on many sites with excellent results. The procedures are often verified by an appropriate use of the following environmental sample “Blanks.”
Trip Blanks
The Trip Blank (or travel blanks) are often used to verify that the sample containers are not impacted during shipping, and verify that the source of the glassware is not the source of contamination. The trip blanks are preserved de-ionized water, collected in the laboratory, and shipped with the sample containers to the site. The trip blank remains in the cooler and is shipped back to the laboratory with the environmental samples. The trip blank is usually analyzed for volatile organics, which correspond to the target analyses.
Field Blanks
Field Blanks are quality assurance samples which are collected in the field to represent the conditions present at the time the samples are collected. For water samples, the laboratory containers are opened and filled in the field using de-ionized (or distilled) water from a known source. The samples then travel to the laboratory with the other samples for analysis.
Equipment Blanks
Equipment Blanks are used to verify whether the decontamination procedures used for the sample equipment or the new equipment added any contaminants to the sample during collection. If a non-disposable sampling device is used (such as a sampling treir, scoop,
hand auger, Teflon bailer, etc…), then the decontamination of the sampling device is usually verified using an equipment blank. The equipment blank is collected using de-ionized (or distilled) water from a known source. The equipment is cleaned, and allowed to dry, the water
is poured over or through the equipment, and collected in the appropriate sample containers. The equipment blank samples are preserved with the other environmental samples, and shipped for analyses for the target parameters.
Duplicate Samples
Duplicate Samples are used to verify the sampling procedures and laboratory analysis variability. The duplicate samples may be collected from waste streams, soil, or groundwater. These samples are collected and sent to the laboratory as a blind sample to have maximum effectiveness. Samples are generally analyzed for the same analytical methods as the actual environmental sample for direct comparison. Duplicate samples may also be split between two different laboratories to provide verification of laboratory detection limits or quality process verification.

APPENDIX   E 

APPENDIX   F 

#=CL#
October 11, 2019
LIMS USE: FR - MIKE JONES
LIMS OBJECT ID: 92447918
92447918
Project:
Pace Project No.:
RE:
Mr. Mike Jones
Pyramid Environmental
P.O. Box 16265
503 Industrial Avenue
Greensboro, NC 27416
Alamance 2019-210
Dear Mr. Jones:
Enclosed are the analytical results for sample(s) received by the laboratory on October 02, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Amanda Payne
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 46
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92447918
Alamance 2019-210
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 46
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92447918
Alamance 2019-210
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92447918001 B-1 3-5 MADEP EPH 7 PASI-CSEM
MADEP VPH 6 PASI-CLMB
EPA 8270D 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
ASTM D2974-87 1 PASI-CKDF
92447918002 B-1 8-10 MADEP EPH 7 PASI-CSEM
MADEP VPH 6 PASI-CLMB
EPA 8270D 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
ASTM D2974-87 1 PASI-CKDF
92447918003 B-1 10-13 MADEP EPH 7 PASI-CSEM
MADEP VPH 6 PASI-CLMB
EPA 8270D 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
ASTM D2974-87 1 PASI-CKDF
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92447918
Alamance 2019-210
Sample: B-1 3-5 Lab ID: 92447918001 Collected: 10/01/19 10:15 Received: 10/02/19 09:48 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 10/07/19 21:39 N210/03/19 09:5011.4 1
Aliphatic (C19-C36)ND mg/kg 10/07/19 21:39 N210/03/19 09:5011.4 1
Aromatic (C11-C22)ND mg/kg 10/07/19 21:39 N210/03/19 09:5011.4 1
Surrogates
Nonatriacontane (S)60 %10/07/19 21:39 7194-86-710/03/19 09:5040-140 1
o-Terphenyl (S)70 %10/07/19 21:39 84-15-110/03/19 09:5040-140 1
2-Fluorobiphenyl (S)94 %10/07/19 21:39 321-60-810/03/19 09:5040-140 1
2-Bromonaphthalene (S)70 %10/07/19 21:39 580-13-210/03/19 09:5040-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)ND mg/kg 10/03/19 17:01 N210/03/19 13:222.4 1
Aliphatic (C09-C12)ND mg/kg 10/03/19 17:01 N210/03/19 13:222.4 1
Aliphatic(C09-C12) Adjusted ND mg/kg 10/03/19 17:01 N210/03/19 13:222.4 1
Aromatic (C09-C10)ND mg/kg 10/03/19 17:01 N210/03/19 13:222.4 1
Surrogates
4-Bromofluorobenzene (FID) (S)89 %10/03/19 17:01 460-00-410/03/19 13:2270-130 1
4-Bromofluorobenzene (PID) (S)92 %10/03/19 17:01 460-00-410/03/19 13:2270-130 1
Analytical Method: EPA 8270D Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 10/08/19 12:34 83-32-910/07/19 18:59375 1
Acenaphthylene ND ug/kg 10/08/19 12:34 208-96-810/07/19 18:59375 1
Aniline ND ug/kg 10/08/19 12:34 62-53-310/07/19 18:59375 1
Anthracene ND ug/kg 10/08/19 12:34 120-12-710/07/19 18:59375 1
Benzo(a)anthracene ND ug/kg 10/08/19 12:34 56-55-310/07/19 18:59375 1
Benzo(a)pyrene ND ug/kg 10/08/19 12:34 50-32-810/07/19 18:59375 1
Benzo(b)fluoranthene ND ug/kg 10/08/19 12:34 205-99-210/07/19 18:59375 1
Benzo(g,h,i)perylene ND ug/kg 10/08/19 12:34 191-24-210/07/19 18:59375 1
Benzo(k)fluoranthene ND ug/kg 10/08/19 12:34 207-08-910/07/19 18:59375 1
Benzoic Acid ND ug/kg 10/08/19 12:34 65-85-010/07/19 18:591880 1
Benzyl alcohol ND ug/kg 10/08/19 12:34 100-51-610/07/19 18:59750 1
4-Bromophenylphenyl ether ND ug/kg 10/08/19 12:34 101-55-310/07/19 18:59375 1
Butylbenzylphthalate ND ug/kg 10/08/19 12:34 85-68-710/07/19 18:59375 1
4-Chloro-3-methylphenol ND ug/kg 10/08/19 12:34 59-50-710/07/19 18:59750 1
4-Chloroaniline ND ug/kg 10/08/19 12:34 106-47-810/07/19 18:591880 1
bis(2-Chloroethoxy)methane ND ug/kg 10/08/19 12:34 111-91-110/07/19 18:59375 1
bis(2-Chloroethyl) ether ND ug/kg 10/08/19 12:34 111-44-410/07/19 18:59375 1
2-Chloronaphthalene ND ug/kg 10/08/19 12:34 91-58-710/07/19 18:59375 1
2-Chlorophenol ND ug/kg 10/08/19 12:34 95-57-810/07/19 18:59375 1
4-Chlorophenylphenyl ether ND ug/kg 10/08/19 12:34 7005-72-310/07/19 18:59375 1
Chrysene ND ug/kg 10/08/19 12:34 218-01-910/07/19 18:59375 1
Dibenz(a,h)anthracene ND ug/kg 10/08/19 12:34 53-70-310/07/19 18:59375 1
Dibenzofuran ND ug/kg 10/08/19 12:34 132-64-910/07/19 18:59375 1
1,2-Dichlorobenzene ND ug/kg 10/08/19 12:34 95-50-110/07/19 18:59375 1
1,3-Dichlorobenzene ND ug/kg 10/08/19 12:34 541-73-110/07/19 18:59375 1
1,4-Dichlorobenzene ND ug/kg 10/08/19 12:34 106-46-710/07/19 18:59375 1
3,3'-Dichlorobenzidine ND ug/kg 10/08/19 12:34 91-94-110/07/19 18:591880 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/11/2019 05:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92447918
Alamance 2019-210
Sample: B-1 3-5 Lab ID: 92447918001 Collected: 10/01/19 10:15 Received: 10/02/19 09:48 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270D Preparation Method: EPA 35468270 MSSV Microwave
2,4-Dichlorophenol ND ug/kg 10/08/19 12:34 120-83-210/07/19 18:59375 1
Diethylphthalate ND ug/kg 10/08/19 12:34 84-66-210/07/19 18:59375 1
2,4-Dimethylphenol ND ug/kg 10/08/19 12:34 105-67-910/07/19 18:59375 1
Dimethylphthalate ND ug/kg 10/08/19 12:34 131-11-310/07/19 18:59375 1
Di-n-butylphthalate ND ug/kg 10/08/19 12:34 84-74-210/07/19 18:59375 1
4,6-Dinitro-2-methylphenol ND ug/kg 10/08/19 12:34 534-52-110/07/19 18:59750 1
2,4-Dinitrophenol ND ug/kg 10/08/19 12:34 51-28-5 R110/07/19 18:591880 1
2,4-Dinitrotoluene ND ug/kg 10/08/19 12:34 121-14-210/07/19 18:59375 1
2,6-Dinitrotoluene ND ug/kg 10/08/19 12:34 606-20-210/07/19 18:59375 1
Di-n-octylphthalate ND ug/kg 10/08/19 12:34 117-84-010/07/19 18:59375 1
bis(2-Ethylhexyl)phthalate ND ug/kg 10/08/19 12:34 117-81-710/07/19 18:59375 1
Fluoranthene ND ug/kg 10/08/19 12:34 206-44-010/07/19 18:59375 1
Fluorene ND ug/kg 10/08/19 12:34 86-73-710/07/19 18:59375 1
Hexachloro-1,3-butadiene ND ug/kg 10/08/19 12:34 87-68-310/07/19 18:59375 1
Hexachlorobenzene ND ug/kg 10/08/19 12:34 118-74-110/07/19 18:59375 1
Hexachlorocyclopentadiene ND ug/kg 10/08/19 12:34 77-47-410/07/19 18:59375 1
Hexachloroethane ND ug/kg 10/08/19 12:34 67-72-110/07/19 18:59375 1
Indeno(1,2,3-cd)pyrene ND ug/kg 10/08/19 12:34 193-39-510/07/19 18:59375 1
Isophorone ND ug/kg 10/08/19 12:34 78-59-110/07/19 18:59375 1
1-Methylnaphthalene ND ug/kg 10/08/19 12:34 90-12-010/07/19 18:59375 1
2-Methylnaphthalene ND ug/kg 10/08/19 12:34 91-57-610/07/19 18:59375 1
2-Methylphenol(o-Cresol)ND ug/kg 10/08/19 12:34 95-48-710/07/19 18:59375 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 10/08/19 12:34 15831-10-410/07/19 18:59375 1
Naphthalene ND ug/kg 10/08/19 12:34 91-20-310/07/19 18:59375 1
2-Nitroaniline ND ug/kg 10/08/19 12:34 88-74-410/07/19 18:591880 1
3-Nitroaniline ND ug/kg 10/08/19 12:34 99-09-210/07/19 18:591880 1
4-Nitroaniline ND ug/kg 10/08/19 12:34 100-01-610/07/19 18:59750 1
Nitrobenzene ND ug/kg 10/08/19 12:34 98-95-310/07/19 18:59375 1
2-Nitrophenol ND ug/kg 10/08/19 12:34 88-75-510/07/19 18:59375 1
4-Nitrophenol ND ug/kg 10/08/19 12:34 100-02-710/07/19 18:591880 1
N-Nitrosodimethylamine ND ug/kg 10/08/19 12:34 62-75-910/07/19 18:59375 1
N-Nitroso-di-n-propylamine ND ug/kg 10/08/19 12:34 621-64-710/07/19 18:59375 1
N-Nitrosodiphenylamine ND ug/kg 10/08/19 12:34 86-30-610/07/19 18:59375 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 10/08/19 12:34 108-60-110/07/19 18:59375 1
Pentachlorophenol ND ug/kg 10/08/19 12:34 87-86-510/07/19 18:591880 1
Phenanthrene ND ug/kg 10/08/19 12:34 85-01-810/07/19 18:59375 1
Phenol ND ug/kg 10/08/19 12:34 108-95-210/07/19 18:59375 1
Pyrene ND ug/kg 10/08/19 12:34 129-00-010/07/19 18:59375 1
Pyridine ND ug/kg 10/08/19 12:34 110-86-110/07/19 18:59375 1
1,2,4-Trichlorobenzene ND ug/kg 10/08/19 12:34 120-82-110/07/19 18:59375 1
2,4,5-Trichlorophenol ND ug/kg 10/08/19 12:34 95-95-410/07/19 18:59375 1
2,4,6-Trichlorophenol ND ug/kg 10/08/19 12:34 88-06-210/07/19 18:59375 1
Surrogates
Nitrobenzene-d5 (S)59 %10/08/19 12:34 4165-60-010/07/19 18:5923-110 1
2-Fluorobiphenyl (S)69 %10/08/19 12:34 321-60-810/07/19 18:5930-110 1
Terphenyl-d14 (S)88 %10/08/19 12:34 1718-51-010/07/19 18:5928-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/11/2019 05:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92447918
Alamance 2019-210
Sample: B-1 3-5 Lab ID: 92447918001 Collected: 10/01/19 10:15 Received: 10/02/19 09:48 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270D Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
Phenol-d6 (S)64 %10/08/19 12:34 13127-88-310/07/19 18:5922-110 1
2-Fluorophenol (S)64 %10/08/19 12:34 367-12-410/07/19 18:5913-110 1
2,4,6-Tribromophenol (S)73 %10/08/19 12:34 118-79-610/07/19 18:5927-110 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND ug/kg 10/08/19 06:30 67-64-110/07/19 14:0480.6 1
Benzene ND ug/kg 10/08/19 06:30 71-43-210/07/19 14:044.0 1
Bromobenzene ND ug/kg 10/08/19 06:30 108-86-110/07/19 14:044.0 1
Bromochloromethane ND ug/kg 10/08/19 06:30 74-97-510/07/19 14:044.0 1
Bromodichloromethane ND ug/kg 10/08/19 06:30 75-27-410/07/19 14:044.0 1
Bromoform ND ug/kg 10/08/19 06:30 75-25-210/07/19 14:044.0 1
Bromomethane ND ug/kg 10/08/19 06:30 74-83-910/07/19 14:048.1 1
2-Butanone (MEK)ND ug/kg 10/08/19 06:30 78-93-310/07/19 14:0480.6 1
n-Butylbenzene ND ug/kg 10/08/19 06:30 104-51-810/07/19 14:044.0 1
sec-Butylbenzene ND ug/kg 10/08/19 06:30 135-98-810/07/19 14:044.0 1
tert-Butylbenzene ND ug/kg 10/08/19 06:30 98-06-610/07/19 14:044.0 1
Carbon tetrachloride ND ug/kg 10/08/19 06:30 56-23-510/07/19 14:044.0 1
Chlorobenzene ND ug/kg 10/08/19 06:30 108-90-710/07/19 14:044.0 1
Chloroethane ND ug/kg 10/08/19 06:30 75-00-310/07/19 14:048.1 1
Chloroform ND ug/kg 10/08/19 06:30 67-66-310/07/19 14:044.0 1
Chloromethane ND ug/kg 10/08/19 06:30 74-87-310/07/19 14:048.1 1
2-Chlorotoluene ND ug/kg 10/08/19 06:30 95-49-810/07/19 14:044.0 1
4-Chlorotoluene ND ug/kg 10/08/19 06:30 106-43-410/07/19 14:044.0 1
1,2-Dibromo-3-chloropropane ND ug/kg 10/08/19 06:30 96-12-8 v110/07/19 14:044.0 1
Dibromochloromethane ND ug/kg 10/08/19 06:30 124-48-110/07/19 14:044.0 1
1,2-Dibromoethane (EDB)ND ug/kg 10/08/19 06:30 106-93-410/07/19 14:044.0 1
Dibromomethane ND ug/kg 10/08/19 06:30 74-95-310/07/19 14:044.0 1
1,2-Dichlorobenzene ND ug/kg 10/08/19 06:30 95-50-110/07/19 14:044.0 1
1,3-Dichlorobenzene ND ug/kg 10/08/19 06:30 541-73-110/07/19 14:044.0 1
1,4-Dichlorobenzene ND ug/kg 10/08/19 06:30 106-46-710/07/19 14:044.0 1
Dichlorodifluoromethane ND ug/kg 10/08/19 06:30 75-71-810/07/19 14:048.1 1
1,1-Dichloroethane ND ug/kg 10/08/19 06:30 75-34-310/07/19 14:044.0 1
1,2-Dichloroethane ND ug/kg 10/08/19 06:30 107-06-210/07/19 14:044.0 1
1,1-Dichloroethene ND ug/kg 10/08/19 06:30 75-35-410/07/19 14:044.0 1
cis-1,2-Dichloroethene ND ug/kg 10/08/19 06:30 156-59-210/07/19 14:044.0 1
trans-1,2-Dichloroethene ND ug/kg 10/08/19 06:30 156-60-510/07/19 14:044.0 1
1,2-Dichloropropane ND ug/kg 10/08/19 06:30 78-87-510/07/19 14:044.0 1
1,3-Dichloropropane ND ug/kg 10/08/19 06:30 142-28-910/07/19 14:044.0 1
2,2-Dichloropropane ND ug/kg 10/08/19 06:30 594-20-710/07/19 14:044.0 1
1,1-Dichloropropene ND ug/kg 10/08/19 06:30 563-58-610/07/19 14:044.0 1
cis-1,3-Dichloropropene ND ug/kg 10/08/19 06:30 10061-01-510/07/19 14:044.0 1
trans-1,3-Dichloropropene ND ug/kg 10/08/19 06:30 10061-02-610/07/19 14:044.0 1
Diisopropyl ether ND ug/kg 10/08/19 06:30 108-20-310/07/19 14:044.0 1
Ethylbenzene ND ug/kg 10/08/19 06:30 100-41-410/07/19 14:044.0 1
Hexachloro-1,3-butadiene ND ug/kg 10/08/19 06:30 87-68-310/07/19 14:044.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/11/2019 05:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92447918
Alamance 2019-210
Sample: B-1 3-5 Lab ID: 92447918001 Collected: 10/01/19 10:15 Received: 10/02/19 09:48 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
2-Hexanone ND ug/kg 10/08/19 06:30 591-78-610/07/19 14:0440.3 1
Isopropylbenzene (Cumene)ND ug/kg 10/08/19 06:30 98-82-810/07/19 14:044.0 1
p-Isopropyltoluene ND ug/kg 10/08/19 06:30 99-87-610/07/19 14:044.0 1
Methylene Chloride ND ug/kg 10/08/19 06:30 75-09-210/07/19 14:0416.1 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 10/08/19 06:30 108-10-110/07/19 14:0440.3 1
Methyl-tert-butyl ether ND ug/kg 10/08/19 06:30 1634-04-410/07/19 14:044.0 1
Naphthalene ND ug/kg 10/08/19 06:30 91-20-310/07/19 14:044.0 1
n-Propylbenzene ND ug/kg 10/08/19 06:30 103-65-110/07/19 14:044.0 1
Styrene ND ug/kg 10/08/19 06:30 100-42-510/07/19 14:044.0 1
1,1,1,2-Tetrachloroethane ND ug/kg 10/08/19 06:30 630-20-610/07/19 14:044.0 1
1,1,2,2-Tetrachloroethane ND ug/kg 10/08/19 06:30 79-34-510/07/19 14:044.0 1
Tetrachloroethene ND ug/kg 10/08/19 06:30 127-18-410/07/19 14:044.0 1
Toluene 13.2 ug/kg 10/08/19 06:30 108-88-310/07/19 14:044.0 1
1,2,3-Trichlorobenzene ND ug/kg 10/08/19 06:30 87-61-610/07/19 14:044.0 1
1,2,4-Trichlorobenzene ND ug/kg 10/08/19 06:30 120-82-110/07/19 14:044.0 1
1,1,1-Trichloroethane ND ug/kg 10/08/19 06:30 71-55-610/07/19 14:044.0 1
1,1,2-Trichloroethane ND ug/kg 10/08/19 06:30 79-00-510/07/19 14:044.0 1
Trichloroethene ND ug/kg 10/08/19 06:30 79-01-610/07/19 14:044.0 1
Trichlorofluoromethane ND ug/kg 10/08/19 06:30 75-69-410/07/19 14:044.0 1
1,2,3-Trichloropropane ND ug/kg 10/08/19 06:30 96-18-410/07/19 14:044.0 1
1,2,4-Trimethylbenzene ND ug/kg 10/08/19 06:30 95-63-610/07/19 14:044.0 1
1,3,5-Trimethylbenzene ND ug/kg 10/08/19 06:30 108-67-810/07/19 14:044.0 1
Vinyl acetate ND ug/kg 10/08/19 06:30 108-05-4 IK,v210/07/19 14:0440.3 1
Vinyl chloride ND ug/kg 10/08/19 06:30 75-01-410/07/19 14:048.1 1
Xylene (Total)13.2 ug/kg 10/08/19 06:30 1330-20-710/07/19 14:048.1 1
m&p-Xylene 9.0 ug/kg 10/08/19 06:30 179601-23-110/07/19 14:048.1 1
o-Xylene 4.2 ug/kg 10/08/19 06:30 95-47-610/07/19 14:044.0 1
Surrogates
Toluene-d8 (S)104 %10/08/19 06:30 2037-26-510/07/19 14:0470-130 1
4-Bromofluorobenzene (S)99 %10/08/19 06:30 460-00-410/07/19 14:0470-130 1
1,2-Dichloroethane-d4 (S)96 %10/08/19 06:30 17060-07-010/07/19 14:0470-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 12.3 %10/02/19 17:030.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/11/2019 05:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92447918
Alamance 2019-210
Sample: B-1 8-10 Lab ID: 92447918002 Collected: 10/01/19 10:20 Received: 10/02/19 09:48 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)21.5 mg/kg 10/07/19 22:07 N210/03/19 09:5012.1 1
Aliphatic (C19-C36)ND mg/kg 10/07/19 22:07 N210/03/19 09:5012.1 1
Aromatic (C11-C22)ND mg/kg 10/07/19 22:07 N210/03/19 09:5012.1 1
Surrogates
Nonatriacontane (S)67 %10/07/19 22:07 7194-86-710/03/19 09:5040-140 1
o-Terphenyl (S)79 %10/07/19 22:07 84-15-110/03/19 09:5040-140 1
2-Fluorobiphenyl (S)104 %10/07/19 22:07 321-60-810/03/19 09:5040-140 1
2-Bromonaphthalene (S)72 %10/07/19 22:07 580-13-210/03/19 09:5040-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)613 mg/kg 10/04/19 16:38 N210/03/19 13:2213.6 4
Aliphatic (C09-C12)1020 mg/kg 10/04/19 16:38 N210/03/19 13:2213.6 4
Aliphatic(C09-C12) Adjusted 518 mg/kg 10/04/19 16:38 N210/03/19 13:2213.6 4
Aromatic (C09-C10)503 mg/kg 10/04/19 16:38 N210/03/19 13:2213.6 4
Surrogates
4-Bromofluorobenzene (FID) (S)141 %10/04/19 16:38 460-00-4 S210/03/19 13:2270-130 4
4-Bromofluorobenzene (PID) (S)101 %10/04/19 16:38 460-00-410/03/19 13:2270-130 4
Analytical Method: EPA 8270D Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 10/08/19 13:57 83-32-910/07/19 18:59395 1
Acenaphthylene ND ug/kg 10/08/19 13:57 208-96-810/07/19 18:59395 1
Aniline ND ug/kg 10/08/19 13:57 62-53-310/07/19 18:59395 1
Anthracene ND ug/kg 10/08/19 13:57 120-12-710/07/19 18:59395 1
Benzo(a)anthracene ND ug/kg 10/08/19 13:57 56-55-310/07/19 18:59395 1
Benzo(a)pyrene ND ug/kg 10/08/19 13:57 50-32-810/07/19 18:59395 1
Benzo(b)fluoranthene ND ug/kg 10/08/19 13:57 205-99-210/07/19 18:59395 1
Benzo(g,h,i)perylene ND ug/kg 10/08/19 13:57 191-24-210/07/19 18:59395 1
Benzo(k)fluoranthene ND ug/kg 10/08/19 13:57 207-08-910/07/19 18:59395 1
Benzoic Acid ND ug/kg 10/08/19 13:57 65-85-010/07/19 18:591980 1
Benzyl alcohol ND ug/kg 10/08/19 13:57 100-51-610/07/19 18:59790 1
4-Bromophenylphenyl ether ND ug/kg 10/08/19 13:57 101-55-310/07/19 18:59395 1
Butylbenzylphthalate ND ug/kg 10/08/19 13:57 85-68-710/07/19 18:59395 1
4-Chloro-3-methylphenol ND ug/kg 10/08/19 13:57 59-50-710/07/19 18:59790 1
4-Chloroaniline ND ug/kg 10/08/19 13:57 106-47-810/07/19 18:591980 1
bis(2-Chloroethoxy)methane ND ug/kg 10/08/19 13:57 111-91-110/07/19 18:59395 1
bis(2-Chloroethyl) ether ND ug/kg 10/08/19 13:57 111-44-410/07/19 18:59395 1
2-Chloronaphthalene ND ug/kg 10/08/19 13:57 91-58-710/07/19 18:59395 1
2-Chlorophenol ND ug/kg 10/08/19 13:57 95-57-810/07/19 18:59395 1
4-Chlorophenylphenyl ether ND ug/kg 10/08/19 13:57 7005-72-310/07/19 18:59395 1
Chrysene ND ug/kg 10/08/19 13:57 218-01-910/07/19 18:59395 1
Dibenz(a,h)anthracene ND ug/kg 10/08/19 13:57 53-70-310/07/19 18:59395 1
Dibenzofuran ND ug/kg 10/08/19 13:57 132-64-910/07/19 18:59395 1
1,2-Dichlorobenzene ND ug/kg 10/08/19 13:57 95-50-110/07/19 18:59395 1
1,3-Dichlorobenzene ND ug/kg 10/08/19 13:57 541-73-110/07/19 18:59395 1
1,4-Dichlorobenzene ND ug/kg 10/08/19 13:57 106-46-710/07/19 18:59395 1
3,3'-Dichlorobenzidine ND ug/kg 10/08/19 13:57 91-94-110/07/19 18:591980 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/11/2019 05:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92447918
Alamance 2019-210
Sample: B-1 8-10 Lab ID: 92447918002 Collected: 10/01/19 10:20 Received: 10/02/19 09:48 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270D Preparation Method: EPA 35468270 MSSV Microwave
2,4-Dichlorophenol ND ug/kg 10/08/19 13:57 120-83-210/07/19 18:59395 1
Diethylphthalate ND ug/kg 10/08/19 13:57 84-66-210/07/19 18:59395 1
2,4-Dimethylphenol ND ug/kg 10/08/19 13:57 105-67-910/07/19 18:59395 1
Dimethylphthalate ND ug/kg 10/08/19 13:57 131-11-310/07/19 18:59395 1
Di-n-butylphthalate ND ug/kg 10/08/19 13:57 84-74-210/07/19 18:59395 1
4,6-Dinitro-2-methylphenol ND ug/kg 10/08/19 13:57 534-52-110/07/19 18:59790 1
2,4-Dinitrophenol ND ug/kg 10/08/19 13:57 51-28-510/07/19 18:591980 1
2,4-Dinitrotoluene ND ug/kg 10/08/19 13:57 121-14-210/07/19 18:59395 1
2,6-Dinitrotoluene ND ug/kg 10/08/19 13:57 606-20-210/07/19 18:59395 1
Di-n-octylphthalate ND ug/kg 10/08/19 13:57 117-84-010/07/19 18:59395 1
bis(2-Ethylhexyl)phthalate ND ug/kg 10/08/19 13:57 117-81-710/07/19 18:59395 1
Fluoranthene ND ug/kg 10/08/19 13:57 206-44-010/07/19 18:59395 1
Fluorene ND ug/kg 10/08/19 13:57 86-73-710/07/19 18:59395 1
Hexachloro-1,3-butadiene ND ug/kg 10/08/19 13:57 87-68-310/07/19 18:59395 1
Hexachlorobenzene ND ug/kg 10/08/19 13:57 118-74-110/07/19 18:59395 1
Hexachlorocyclopentadiene ND ug/kg 10/08/19 13:57 77-47-410/07/19 18:59395 1
Hexachloroethane ND ug/kg 10/08/19 13:57 67-72-110/07/19 18:59395 1
Indeno(1,2,3-cd)pyrene ND ug/kg 10/08/19 13:57 193-39-510/07/19 18:59395 1
Isophorone ND ug/kg 10/08/19 13:57 78-59-110/07/19 18:59395 1
1-Methylnaphthalene ND ug/kg 10/08/19 13:57 90-12-010/07/19 18:59395 1
2-Methylnaphthalene ND ug/kg 10/08/19 13:57 91-57-610/07/19 18:59395 1
2-Methylphenol(o-Cresol)ND ug/kg 10/08/19 13:57 95-48-710/07/19 18:59395 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 10/08/19 13:57 15831-10-410/07/19 18:59395 1
Naphthalene ND ug/kg 10/08/19 13:57 91-20-310/07/19 18:59395 1
2-Nitroaniline ND ug/kg 10/08/19 13:57 88-74-410/07/19 18:591980 1
3-Nitroaniline ND ug/kg 10/08/19 13:57 99-09-210/07/19 18:591980 1
4-Nitroaniline ND ug/kg 10/08/19 13:57 100-01-610/07/19 18:59790 1
Nitrobenzene ND ug/kg 10/08/19 13:57 98-95-310/07/19 18:59395 1
2-Nitrophenol ND ug/kg 10/08/19 13:57 88-75-510/07/19 18:59395 1
4-Nitrophenol ND ug/kg 10/08/19 13:57 100-02-710/07/19 18:591980 1
N-Nitrosodimethylamine ND ug/kg 10/08/19 13:57 62-75-910/07/19 18:59395 1
N-Nitroso-di-n-propylamine ND ug/kg 10/08/19 13:57 621-64-710/07/19 18:59395 1
N-Nitrosodiphenylamine ND ug/kg 10/08/19 13:57 86-30-610/07/19 18:59395 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 10/08/19 13:57 108-60-110/07/19 18:59395 1
Pentachlorophenol ND ug/kg 10/08/19 13:57 87-86-510/07/19 18:591980 1
Phenanthrene ND ug/kg 10/08/19 13:57 85-01-810/07/19 18:59395 1
Phenol ND ug/kg 10/08/19 13:57 108-95-210/07/19 18:59395 1
Pyrene ND ug/kg 10/08/19 13:57 129-00-010/07/19 18:59395 1
Pyridine ND ug/kg 10/08/19 13:57 110-86-110/07/19 18:59395 1
1,2,4-Trichlorobenzene ND ug/kg 10/08/19 13:57 120-82-110/07/19 18:59395 1
2,4,5-Trichlorophenol ND ug/kg 10/08/19 13:57 95-95-410/07/19 18:59395 1
2,4,6-Trichlorophenol ND ug/kg 10/08/19 13:57 88-06-210/07/19 18:59395 1
Surrogates
Nitrobenzene-d5 (S)48 %10/08/19 13:57 4165-60-010/07/19 18:5923-110 1
2-Fluorobiphenyl (S)56 %10/08/19 13:57 321-60-810/07/19 18:5930-110 1
Terphenyl-d14 (S)68 %10/08/19 13:57 1718-51-010/07/19 18:5928-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/11/2019 05:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92447918
Alamance 2019-210
Sample: B-1 8-10 Lab ID: 92447918002 Collected: 10/01/19 10:20 Received: 10/02/19 09:48 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270D Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
Phenol-d6 (S)51 %10/08/19 13:57 13127-88-310/07/19 18:5922-110 1
2-Fluorophenol (S)53 %10/08/19 13:57 367-12-410/07/19 18:5913-110 1
2,4,6-Tribromophenol (S)63 %10/08/19 13:57 118-79-610/07/19 18:5927-110 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND ug/kg 10/08/19 18:44 67-64-110/08/19 13:2439900 250
Benzene 2280 ug/kg 10/08/19 18:44 71-43-210/08/19 13:241990 250
Bromobenzene ND ug/kg 10/08/19 18:44 108-86-110/08/19 13:241990 250
Bromochloromethane ND ug/kg 10/08/19 18:44 74-97-510/08/19 13:241990 250
Bromodichloromethane ND ug/kg 10/08/19 18:44 75-27-410/08/19 13:241990 250
Bromoform ND ug/kg 10/08/19 18:44 75-25-210/08/19 13:241990 250
Bromomethane ND ug/kg 10/08/19 18:44 74-83-910/08/19 13:243990 250
2-Butanone (MEK)ND ug/kg 10/08/19 18:44 78-93-310/08/19 13:2439900 250
n-Butylbenzene 11700 ug/kg 10/08/19 18:44 104-51-810/08/19 13:241990 250
sec-Butylbenzene ND ug/kg 10/08/19 18:44 135-98-810/08/19 13:241990 250
tert-Butylbenzene ND ug/kg 10/08/19 18:44 98-06-610/08/19 13:241990 250
Carbon tetrachloride ND ug/kg 10/08/19 18:44 56-23-510/08/19 13:241990 250
Chlorobenzene ND ug/kg 10/08/19 18:44 108-90-710/08/19 13:241990 250
Chloroethane ND ug/kg 10/08/19 18:44 75-00-3 v110/08/19 13:243990 250
Chloroform ND ug/kg 10/08/19 18:44 67-66-310/08/19 13:241990 250
Chloromethane ND ug/kg 10/08/19 18:44 74-87-310/08/19 13:243990 250
2-Chlorotoluene ND ug/kg 10/08/19 18:44 95-49-810/08/19 13:241990 250
4-Chlorotoluene ND ug/kg 10/08/19 18:44 106-43-410/08/19 13:241990 250
1,2-Dibromo-3-chloropropane ND ug/kg 10/08/19 18:44 96-12-810/08/19 13:241990 250
Dibromochloromethane ND ug/kg 10/08/19 18:44 124-48-110/08/19 13:241990 250
1,2-Dibromoethane (EDB)ND ug/kg 10/08/19 18:44 106-93-410/08/19 13:241990 250
Dibromomethane ND ug/kg 10/08/19 18:44 74-95-310/08/19 13:241990 250
1,2-Dichlorobenzene ND ug/kg 10/08/19 18:44 95-50-110/08/19 13:241990 250
1,3-Dichlorobenzene ND ug/kg 10/08/19 18:44 541-73-110/08/19 13:241990 250
1,4-Dichlorobenzene ND ug/kg 10/08/19 18:44 106-46-710/08/19 13:241990 250
Dichlorodifluoromethane ND ug/kg 10/08/19 18:44 75-71-810/08/19 13:243990 250
1,1-Dichloroethane ND ug/kg 10/08/19 18:44 75-34-310/08/19 13:241990 250
1,2-Dichloroethane ND ug/kg 10/08/19 18:44 107-06-210/08/19 13:241990 250
1,1-Dichloroethene ND ug/kg 10/08/19 18:44 75-35-410/08/19 13:241990 250
cis-1,2-Dichloroethene ND ug/kg 10/08/19 18:44 156-59-210/08/19 13:241990 250
trans-1,2-Dichloroethene ND ug/kg 10/08/19 18:44 156-60-510/08/19 13:241990 250
1,2-Dichloropropane ND ug/kg 10/08/19 18:44 78-87-510/08/19 13:241990 250
1,3-Dichloropropane ND ug/kg 10/08/19 18:44 142-28-910/08/19 13:241990 250
2,2-Dichloropropane ND ug/kg 10/08/19 18:44 594-20-710/08/19 13:241990 250
1,1-Dichloropropene ND ug/kg 10/08/19 18:44 563-58-610/08/19 13:241990 250
cis-1,3-Dichloropropene ND ug/kg 10/08/19 18:44 10061-01-510/08/19 13:241990 250
trans-1,3-Dichloropropene ND ug/kg 10/08/19 18:44 10061-02-610/08/19 13:241990 250
Diisopropyl ether ND ug/kg 10/08/19 18:44 108-20-310/08/19 13:241990 250
Ethylbenzene 48400 ug/kg 10/08/19 18:44 100-41-410/08/19 13:241990 250
Hexachloro-1,3-butadiene ND ug/kg 10/08/19 18:44 87-68-310/08/19 13:241990 250
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/11/2019 05:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92447918
Alamance 2019-210
Sample: B-1 8-10 Lab ID: 92447918002 Collected: 10/01/19 10:20 Received: 10/02/19 09:48 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
2-Hexanone ND ug/kg 10/08/19 18:44 591-78-610/08/19 13:2419900 250
Isopropylbenzene (Cumene)4270 ug/kg 10/08/19 18:44 98-82-810/08/19 13:241990 250
p-Isopropyltoluene ND ug/kg 10/08/19 18:44 99-87-610/08/19 13:241990 250
Methylene Chloride ND ug/kg 10/08/19 18:44 75-09-210/08/19 13:247980 250
4-Methyl-2-pentanone (MIBK)ND ug/kg 10/08/19 18:44 108-10-110/08/19 13:2419900 250
Methyl-tert-butyl ether ND ug/kg 10/08/19 18:44 1634-04-410/08/19 13:241990 250
Naphthalene 47800 ug/kg 10/08/19 18:44 91-20-310/08/19 13:241990 250
n-Propylbenzene 24200 ug/kg 10/08/19 18:44 103-65-110/08/19 13:241990 250
Styrene 3130 ug/kg 10/08/19 18:44 100-42-510/08/19 13:241990 250
1,1,1,2-Tetrachloroethane ND ug/kg 10/08/19 18:44 630-20-610/08/19 13:241990 250
1,1,2,2-Tetrachloroethane ND ug/kg 10/08/19 18:44 79-34-510/08/19 13:241990 250
Tetrachloroethene ND ug/kg 10/08/19 18:44 127-18-410/08/19 13:241990 250
Toluene 71600 ug/kg 10/09/19 16:15 108-88-310/08/19 13:247980 1000
1,2,3-Trichlorobenzene ND ug/kg 10/08/19 18:44 87-61-610/08/19 13:241990 250
1,2,4-Trichlorobenzene ND ug/kg 10/08/19 18:44 120-82-110/08/19 13:241990 250
1,1,1-Trichloroethane ND ug/kg 10/08/19 18:44 71-55-610/08/19 13:241990 250
1,1,2-Trichloroethane ND ug/kg 10/08/19 18:44 79-00-510/08/19 13:241990 250
Trichloroethene ND ug/kg 10/08/19 18:44 79-01-610/08/19 13:241990 250
Trichlorofluoromethane ND ug/kg 10/08/19 18:44 75-69-410/08/19 13:241990 250
1,2,3-Trichloropropane 2330 ug/kg 10/08/19 18:44 96-18-410/08/19 13:241990 250
1,2,4-Trimethylbenzene 163000 ug/kg 10/09/19 16:15 95-63-610/08/19 13:247980 1000
1,3,5-Trimethylbenzene 54200 ug/kg 10/08/19 18:44 108-67-810/08/19 13:241990 250
Vinyl acetate ND ug/kg 10/08/19 18:44 108-05-4 IK10/08/19 13:2419900 250
Vinyl chloride ND ug/kg 10/08/19 18:44 75-01-410/08/19 13:243990 250
Xylene (Total)229000 ug/kg 10/09/19 16:15 1330-20-710/08/19 13:2416000 1000
m&p-Xylene 156000 ug/kg 10/09/19 16:15 179601-23-110/08/19 13:2416000 1000
o-Xylene 73200 ug/kg 10/08/19 18:44 95-47-610/08/19 13:241990 250
Surrogates
Toluene-d8 (S)102 %10/08/19 18:44 2037-26-510/08/19 13:2470-130 250
4-Bromofluorobenzene (S)96 %10/08/19 18:44 460-00-410/08/19 13:2470-130 250
1,2-Dichloroethane-d4 (S)93 %10/08/19 18:44 17060-07-010/08/19 13:2470-132 250
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 17.3 %10/02/19 17:040.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/11/2019 05:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92447918
Alamance 2019-210
Sample: B-1 10-13 Lab ID: 92447918003 Collected: 10/01/19 10:25 Received: 10/02/19 09:48 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)151 mg/kg 10/08/19 12:55 N210/03/19 09:5047.7 4
Aliphatic (C19-C36)ND mg/kg 10/08/19 12:55 N210/03/19 09:5047.7 4
Aromatic (C11-C22)42.3 mg/kg 10/07/19 22:34 N210/03/19 09:5011.9 1
Surrogates
Nonatriacontane (S)58 %10/08/19 12:55 7194-86-710/03/19 09:5040-140 4
o-Terphenyl (S)98 %10/07/19 22:34 84-15-110/03/19 09:5040-140 1
2-Fluorobiphenyl (S)105 %10/07/19 22:34 321-60-810/03/19 09:5040-140 1
2-Bromonaphthalene (S)100 %10/07/19 22:34 580-13-210/03/19 09:5040-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)3.6 mg/kg 10/03/19 17:30 N210/03/19 13:223.2 1
Aliphatic (C09-C12)3.6 mg/kg 10/03/19 17:30 N210/03/19 13:223.2 1
Aliphatic(C09-C12) Adjusted ND mg/kg 10/03/19 17:30 N210/03/19 13:223.2 1
Aromatic (C09-C10)ND mg/kg 10/03/19 17:30 N210/03/19 13:223.2 1
Surrogates
4-Bromofluorobenzene (FID) (S)89 %10/03/19 17:30 460-00-410/03/19 13:2270-130 1
4-Bromofluorobenzene (PID) (S)91 %10/03/19 17:30 460-00-410/03/19 13:2270-130 1
Analytical Method: EPA 8270D Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 10/08/19 14:25 83-32-910/07/19 18:59390 1
Acenaphthylene ND ug/kg 10/08/19 14:25 208-96-810/07/19 18:59390 1
Aniline ND ug/kg 10/08/19 14:25 62-53-310/07/19 18:59390 1
Anthracene ND ug/kg 10/08/19 14:25 120-12-710/07/19 18:59390 1
Benzo(a)anthracene ND ug/kg 10/08/19 14:25 56-55-310/07/19 18:59390 1
Benzo(a)pyrene ND ug/kg 10/08/19 14:25 50-32-810/07/19 18:59390 1
Benzo(b)fluoranthene ND ug/kg 10/08/19 14:25 205-99-210/07/19 18:59390 1
Benzo(g,h,i)perylene ND ug/kg 10/08/19 14:25 191-24-210/07/19 18:59390 1
Benzo(k)fluoranthene ND ug/kg 10/08/19 14:25 207-08-910/07/19 18:59390 1
Benzoic Acid ND ug/kg 10/08/19 14:25 65-85-010/07/19 18:591950 1
Benzyl alcohol ND ug/kg 10/08/19 14:25 100-51-610/07/19 18:59779 1
4-Bromophenylphenyl ether ND ug/kg 10/08/19 14:25 101-55-310/07/19 18:59390 1
Butylbenzylphthalate ND ug/kg 10/08/19 14:25 85-68-710/07/19 18:59390 1
4-Chloro-3-methylphenol ND ug/kg 10/08/19 14:25 59-50-710/07/19 18:59779 1
4-Chloroaniline ND ug/kg 10/08/19 14:25 106-47-810/07/19 18:591950 1
bis(2-Chloroethoxy)methane ND ug/kg 10/08/19 14:25 111-91-110/07/19 18:59390 1
bis(2-Chloroethyl) ether ND ug/kg 10/08/19 14:25 111-44-410/07/19 18:59390 1
2-Chloronaphthalene ND ug/kg 10/08/19 14:25 91-58-710/07/19 18:59390 1
2-Chlorophenol ND ug/kg 10/08/19 14:25 95-57-810/07/19 18:59390 1
4-Chlorophenylphenyl ether ND ug/kg 10/08/19 14:25 7005-72-310/07/19 18:59390 1
Chrysene ND ug/kg 10/08/19 14:25 218-01-910/07/19 18:59390 1
Dibenz(a,h)anthracene ND ug/kg 10/08/19 14:25 53-70-310/07/19 18:59390 1
Dibenzofuran ND ug/kg 10/08/19 14:25 132-64-910/07/19 18:59390 1
1,2-Dichlorobenzene ND ug/kg 10/08/19 14:25 95-50-110/07/19 18:59390 1
1,3-Dichlorobenzene ND ug/kg 10/08/19 14:25 541-73-110/07/19 18:59390 1
1,4-Dichlorobenzene ND ug/kg 10/08/19 14:25 106-46-710/07/19 18:59390 1
3,3'-Dichlorobenzidine ND ug/kg 10/08/19 14:25 91-94-110/07/19 18:591950 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/11/2019 05:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92447918
Alamance 2019-210
Sample: B-1 10-13 Lab ID: 92447918003 Collected: 10/01/19 10:25 Received: 10/02/19 09:48 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270D Preparation Method: EPA 35468270 MSSV Microwave
2,4-Dichlorophenol ND ug/kg 10/08/19 14:25 120-83-210/07/19 18:59390 1
Diethylphthalate ND ug/kg 10/08/19 14:25 84-66-210/07/19 18:59390 1
2,4-Dimethylphenol ND ug/kg 10/08/19 14:25 105-67-910/07/19 18:59390 1
Dimethylphthalate ND ug/kg 10/08/19 14:25 131-11-310/07/19 18:59390 1
Di-n-butylphthalate ND ug/kg 10/08/19 14:25 84-74-210/07/19 18:59390 1
4,6-Dinitro-2-methylphenol ND ug/kg 10/08/19 14:25 534-52-110/07/19 18:59779 1
2,4-Dinitrophenol ND ug/kg 10/08/19 14:25 51-28-510/07/19 18:591950 1
2,4-Dinitrotoluene ND ug/kg 10/08/19 14:25 121-14-210/07/19 18:59390 1
2,6-Dinitrotoluene ND ug/kg 10/08/19 14:25 606-20-210/07/19 18:59390 1
Di-n-octylphthalate ND ug/kg 10/08/19 14:25 117-84-010/07/19 18:59390 1
bis(2-Ethylhexyl)phthalate ND ug/kg 10/08/19 14:25 117-81-710/07/19 18:59390 1
Fluoranthene ND ug/kg 10/08/19 14:25 206-44-010/07/19 18:59390 1
Fluorene ND ug/kg 10/08/19 14:25 86-73-710/07/19 18:59390 1
Hexachloro-1,3-butadiene ND ug/kg 10/08/19 14:25 87-68-310/07/19 18:59390 1
Hexachlorobenzene ND ug/kg 10/08/19 14:25 118-74-110/07/19 18:59390 1
Hexachlorocyclopentadiene ND ug/kg 10/08/19 14:25 77-47-410/07/19 18:59390 1
Hexachloroethane ND ug/kg 10/08/19 14:25 67-72-110/07/19 18:59390 1
Indeno(1,2,3-cd)pyrene ND ug/kg 10/08/19 14:25 193-39-510/07/19 18:59390 1
Isophorone ND ug/kg 10/08/19 14:25 78-59-110/07/19 18:59390 1
1-Methylnaphthalene ND ug/kg 10/08/19 14:25 90-12-010/07/19 18:59390 1
2-Methylnaphthalene ND ug/kg 10/08/19 14:25 91-57-610/07/19 18:59390 1
2-Methylphenol(o-Cresol)ND ug/kg 10/08/19 14:25 95-48-710/07/19 18:59390 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 10/08/19 14:25 15831-10-410/07/19 18:59390 1
Naphthalene ND ug/kg 10/08/19 14:25 91-20-310/07/19 18:59390 1
2-Nitroaniline ND ug/kg 10/08/19 14:25 88-74-410/07/19 18:591950 1
3-Nitroaniline ND ug/kg 10/08/19 14:25 99-09-210/07/19 18:591950 1
4-Nitroaniline ND ug/kg 10/08/19 14:25 100-01-610/07/19 18:59779 1
Nitrobenzene ND ug/kg 10/08/19 14:25 98-95-310/07/19 18:59390 1
2-Nitrophenol ND ug/kg 10/08/19 14:25 88-75-510/07/19 18:59390 1
4-Nitrophenol ND ug/kg 10/08/19 14:25 100-02-710/07/19 18:591950 1
N-Nitrosodimethylamine ND ug/kg 10/08/19 14:25 62-75-910/07/19 18:59390 1
N-Nitroso-di-n-propylamine ND ug/kg 10/08/19 14:25 621-64-710/07/19 18:59390 1
N-Nitrosodiphenylamine ND ug/kg 10/08/19 14:25 86-30-610/07/19 18:59390 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 10/08/19 14:25 108-60-110/07/19 18:59390 1
Pentachlorophenol ND ug/kg 10/08/19 14:25 87-86-510/07/19 18:591950 1
Phenanthrene ND ug/kg 10/08/19 14:25 85-01-810/07/19 18:59390 1
Phenol ND ug/kg 10/08/19 14:25 108-95-210/07/19 18:59390 1
Pyrene ND ug/kg 10/08/19 14:25 129-00-010/07/19 18:59390 1
Pyridine ND ug/kg 10/08/19 14:25 110-86-110/07/19 18:59390 1
1,2,4-Trichlorobenzene ND ug/kg 10/08/19 14:25 120-82-110/07/19 18:59390 1
2,4,5-Trichlorophenol ND ug/kg 10/08/19 14:25 95-95-410/07/19 18:59390 1
2,4,6-Trichlorophenol ND ug/kg 10/08/19 14:25 88-06-210/07/19 18:59390 1
Surrogates
Nitrobenzene-d5 (S)55 %10/08/19 14:25 4165-60-010/07/19 18:5923-110 1
2-Fluorobiphenyl (S)64 %10/08/19 14:25 321-60-810/07/19 18:5930-110 1
Terphenyl-d14 (S)75 %10/08/19 14:25 1718-51-010/07/19 18:5928-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/11/2019 05:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92447918
Alamance 2019-210
Sample: B-1 10-13 Lab ID: 92447918003 Collected: 10/01/19 10:25 Received: 10/02/19 09:48 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8270D Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
Phenol-d6 (S)56 %10/08/19 14:25 13127-88-310/07/19 18:5922-110 1
2-Fluorophenol (S)52 %10/08/19 14:25 367-12-410/07/19 18:5913-110 1
2,4,6-Tribromophenol (S)50 %10/08/19 14:25 118-79-610/07/19 18:5927-110 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND ug/kg 10/10/19 17:24 67-64-110/10/19 15:5672.3 1
Benzene 27.5 ug/kg 10/10/19 17:24 71-43-210/10/19 15:563.6 1
Bromobenzene ND ug/kg 10/10/19 17:24 108-86-110/10/19 15:563.6 1
Bromochloromethane ND ug/kg 10/10/19 17:24 74-97-510/10/19 15:563.6 1
Bromodichloromethane ND ug/kg 10/10/19 17:24 75-27-410/10/19 15:563.6 1
Bromoform ND ug/kg 10/10/19 17:24 75-25-210/10/19 15:563.6 1
Bromomethane ND ug/kg 10/10/19 17:24 74-83-910/10/19 15:567.2 1
2-Butanone (MEK)ND ug/kg 10/10/19 17:24 78-93-310/10/19 15:5672.3 1
n-Butylbenzene ND ug/kg 10/10/19 17:24 104-51-810/10/19 15:563.6 1
sec-Butylbenzene ND ug/kg 10/10/19 17:24 135-98-810/10/19 15:563.6 1
tert-Butylbenzene ND ug/kg 10/10/19 17:24 98-06-610/10/19 15:563.6 1
Carbon tetrachloride ND ug/kg 10/10/19 17:24 56-23-510/10/19 15:563.6 1
Chlorobenzene ND ug/kg 10/10/19 17:24 108-90-710/10/19 15:563.6 1
Chloroethane ND ug/kg 10/10/19 17:24 75-00-310/10/19 15:567.2 1
Chloroform ND ug/kg 10/10/19 17:24 67-66-310/10/19 15:563.6 1
Chloromethane ND ug/kg 10/10/19 17:24 74-87-310/10/19 15:567.2 1
2-Chlorotoluene ND ug/kg 10/10/19 17:24 95-49-810/10/19 15:563.6 1
4-Chlorotoluene ND ug/kg 10/10/19 17:24 106-43-410/10/19 15:563.6 1
1,2-Dibromo-3-chloropropane ND ug/kg 10/10/19 17:24 96-12-810/10/19 15:563.6 1
Dibromochloromethane ND ug/kg 10/10/19 17:24 124-48-110/10/19 15:563.6 1
1,2-Dibromoethane (EDB)ND ug/kg 10/10/19 17:24 106-93-410/10/19 15:563.6 1
Dibromomethane ND ug/kg 10/10/19 17:24 74-95-310/10/19 15:563.6 1
1,2-Dichlorobenzene ND ug/kg 10/10/19 17:24 95-50-110/10/19 15:563.6 1
1,3-Dichlorobenzene ND ug/kg 10/10/19 17:24 541-73-110/10/19 15:563.6 1
1,4-Dichlorobenzene ND ug/kg 10/10/19 17:24 106-46-710/10/19 15:563.6 1
Dichlorodifluoromethane ND ug/kg 10/10/19 17:24 75-71-810/10/19 15:567.2 1
1,1-Dichloroethane ND ug/kg 10/10/19 17:24 75-34-310/10/19 15:563.6 1
1,2-Dichloroethane ND ug/kg 10/10/19 17:24 107-06-210/10/19 15:563.6 1
1,1-Dichloroethene ND ug/kg 10/10/19 17:24 75-35-410/10/19 15:563.6 1
cis-1,2-Dichloroethene ND ug/kg 10/10/19 17:24 156-59-210/10/19 15:563.6 1
trans-1,2-Dichloroethene ND ug/kg 10/10/19 17:24 156-60-510/10/19 15:563.6 1
1,2-Dichloropropane ND ug/kg 10/10/19 17:24 78-87-510/10/19 15:563.6 1
1,3-Dichloropropane ND ug/kg 10/10/19 17:24 142-28-910/10/19 15:563.6 1
2,2-Dichloropropane ND ug/kg 10/10/19 17:24 594-20-710/10/19 15:563.6 1
1,1-Dichloropropene ND ug/kg 10/10/19 17:24 563-58-610/10/19 15:563.6 1
cis-1,3-Dichloropropene ND ug/kg 10/10/19 17:24 10061-01-510/10/19 15:563.6 1
trans-1,3-Dichloropropene ND ug/kg 10/10/19 17:24 10061-02-610/10/19 15:563.6 1
Diisopropyl ether ND ug/kg 10/10/19 17:24 108-20-310/10/19 15:563.6 1
Ethylbenzene 14.9 ug/kg 10/10/19 17:24 100-41-410/10/19 15:563.6 1
Hexachloro-1,3-butadiene ND ug/kg 10/10/19 17:24 87-68-310/10/19 15:563.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/11/2019 05:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 46
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92447918
Alamance 2019-210
Sample: B-1 10-13 Lab ID: 92447918003 Collected: 10/01/19 10:25 Received: 10/02/19 09:48 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
2-Hexanone ND ug/kg 10/10/19 17:24 591-78-610/10/19 15:5636.2 1
Isopropylbenzene (Cumene)ND ug/kg 10/10/19 17:24 98-82-810/10/19 15:563.6 1
p-Isopropyltoluene ND ug/kg 10/10/19 17:24 99-87-610/10/19 15:563.6 1
Methylene Chloride ND ug/kg 10/10/19 17:24 75-09-210/10/19 15:5614.5 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 10/10/19 17:24 108-10-110/10/19 15:5636.2 1
Methyl-tert-butyl ether ND ug/kg 10/10/19 17:24 1634-04-410/10/19 15:563.6 1
Naphthalene 9.3 ug/kg 10/10/19 17:24 91-20-310/10/19 15:563.6 1
n-Propylbenzene 3.8 ug/kg 10/10/19 17:24 103-65-110/10/19 15:563.6 1
Styrene ND ug/kg 10/10/19 17:24 100-42-510/10/19 15:563.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 10/10/19 17:24 630-20-610/10/19 15:563.6 1
1,1,2,2-Tetrachloroethane ND ug/kg 10/10/19 17:24 79-34-510/10/19 15:563.6 1
Tetrachloroethene ND ug/kg 10/10/19 17:24 127-18-410/10/19 15:563.6 1
Toluene 83.8 ug/kg 10/10/19 17:24 108-88-310/10/19 15:563.6 1
1,2,3-Trichlorobenzene ND ug/kg 10/10/19 17:24 87-61-610/10/19 15:563.6 1
1,2,4-Trichlorobenzene ND ug/kg 10/10/19 17:24 120-82-110/10/19 15:563.6 1
1,1,1-Trichloroethane ND ug/kg 10/10/19 17:24 71-55-610/10/19 15:563.6 1
1,1,2-Trichloroethane ND ug/kg 10/10/19 17:24 79-00-510/10/19 15:563.6 1
Trichloroethene ND ug/kg 10/10/19 17:24 79-01-610/10/19 15:563.6 1
Trichlorofluoromethane ND ug/kg 10/10/19 17:24 75-69-410/10/19 15:563.6 1
1,2,3-Trichloropropane ND ug/kg 10/10/19 17:24 96-18-410/10/19 15:563.6 1
1,2,4-Trimethylbenzene 30.0 ug/kg 10/10/19 17:24 95-63-610/10/19 15:563.6 1
1,3,5-Trimethylbenzene 8.1 ug/kg 10/10/19 17:24 108-67-810/10/19 15:563.6 1
Vinyl acetate ND ug/kg 10/10/19 17:24 108-05-410/10/19 15:5636.2 1
Vinyl chloride ND ug/kg 10/10/19 17:24 75-01-410/10/19 15:567.2 1
Xylene (Total)75.4 ug/kg 10/10/19 17:24 1330-20-710/10/19 15:567.2 1
m&p-Xylene 48.3 ug/kg 10/10/19 17:24 179601-23-110/10/19 15:567.2 1
o-Xylene 27.2 ug/kg 10/10/19 17:24 95-47-610/10/19 15:563.6 1
Surrogates
Toluene-d8 (S)103 %10/10/19 17:24 2037-26-510/10/19 15:5670-130 1
4-Bromofluorobenzene (S)104 %10/10/19 17:24 460-00-410/10/19 15:5670-130 1
1,2-Dichloroethane-d4 (S)102 %10/10/19 17:24 17060-07-010/10/19 15:5670-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 16.1 %10/02/19 17:040.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/11/2019 05:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92447918
Alamance 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
501510
MADEP VPH
MADEP VPH
VPH NC Soil
Associated Lab Samples: 92447918001, 92447918002, 92447918003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2697168
Associated Lab Samples:92447918001, 92447918002, 92447918003
Matrix: Solid
Analyzed
Aliphatic (C05-C08)mg/kg ND 2.5 N210/03/19 15:32
Aliphatic (C09-C12)mg/kg ND 2.5 N210/03/19 15:32
Aromatic (C09-C10)mg/kg ND 2.5 N210/03/19 15:32
4-Bromofluorobenzene (FID) (S)%90 70-130 10/03/19 15:32
4-Bromofluorobenzene (PID) (S)%94 70-130 10/03/19 15:32
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2697169LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2697170
Aliphatic (C05-C08)mg/kg 15.4 N215.1 102 70-13010015.1 2 25
Aliphatic (C09-C12)mg/kg 15.7 N215.1 104 30-13010215.5 1 25
Aromatic (C09-C10)mg/kg 5.1 N2510170-130984.9 3 25
4-Bromofluorobenzene (FID) (S)%103 70-13093
4-Bromofluorobenzene (PID) (S)%105 70-13095
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/11/2019 05:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92447918
Alamance 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
501852
EPA 5035A
EPA 8260D
8260D MSV 5035A Volatile Organics
Associated Lab Samples: 92447918001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2698776
Associated Lab Samples:92447918001
Matrix: Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 10/08/19 00:52
1,1,1-Trichloroethane ug/kg ND 5.0 10/08/19 00:52
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 10/08/19 00:52
1,1,2-Trichloroethane ug/kg ND 5.0 10/08/19 00:52
1,1-Dichloroethane ug/kg ND 5.0 10/08/19 00:52
1,1-Dichloroethene ug/kg ND 5.0 10/08/19 00:52
1,1-Dichloropropene ug/kg ND 5.0 10/08/19 00:52
1,2,3-Trichlorobenzene ug/kg ND 5.0 10/08/19 00:52
1,2,3-Trichloropropane ug/kg ND 5.0 10/08/19 00:52
1,2,4-Trichlorobenzene ug/kg ND 5.0 10/08/19 00:52
1,2,4-Trimethylbenzene ug/kg ND 5.0 10/08/19 00:52
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 v110/08/19 00:52
1,2-Dibromoethane (EDB)ug/kg ND 5.0 10/08/19 00:52
1,2-Dichlorobenzene ug/kg ND 5.0 10/08/19 00:52
1,2-Dichloroethane ug/kg ND 5.0 10/08/19 00:52
1,2-Dichloropropane ug/kg ND 5.0 10/08/19 00:52
1,3,5-Trimethylbenzene ug/kg ND 5.0 10/08/19 00:52
1,3-Dichlorobenzene ug/kg ND 5.0 10/08/19 00:52
1,3-Dichloropropane ug/kg ND 5.0 10/08/19 00:52
1,4-Dichlorobenzene ug/kg ND 5.0 10/08/19 00:52
2,2-Dichloropropane ug/kg ND 5.0 10/08/19 00:52
2-Butanone (MEK)ug/kg ND 100 10/08/19 00:52
2-Chlorotoluene ug/kg ND 5.0 10/08/19 00:52
2-Hexanone ug/kg ND 50.0 10/08/19 00:52
4-Chlorotoluene ug/kg ND 5.0 10/08/19 00:52
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 10/08/19 00:52
Acetone ug/kg ND 100 10/08/19 00:52
Benzene ug/kg ND 5.0 10/08/19 00:52
Bromobenzene ug/kg ND 5.0 10/08/19 00:52
Bromochloromethane ug/kg ND 5.0 10/08/19 00:52
Bromodichloromethane ug/kg ND 5.0 10/08/19 00:52
Bromoform ug/kg ND 5.0 10/08/19 00:52
Bromomethane ug/kg ND 10.0 10/08/19 00:52
Carbon tetrachloride ug/kg ND 5.0 10/08/19 00:52
Chlorobenzene ug/kg ND 5.0 10/08/19 00:52
Chloroethane ug/kg ND 10.0 10/08/19 00:52
Chloroform ug/kg ND 5.0 10/08/19 00:52
Chloromethane ug/kg ND 10.0 10/08/19 00:52
cis-1,2-Dichloroethene ug/kg ND 5.0 10/08/19 00:52
cis-1,3-Dichloropropene ug/kg ND 5.0 10/08/19 00:52
Dibromochloromethane ug/kg ND 5.0 10/08/19 00:52
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/11/2019 05:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92447918
Alamance 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2698776
Associated Lab Samples:92447918001
Matrix: Solid
Analyzed
Dibromomethane ug/kg ND 5.0 10/08/19 00:52
Dichlorodifluoromethane ug/kg ND 10.0 10/08/19 00:52
Diisopropyl ether ug/kg ND 5.0 10/08/19 00:52
Ethylbenzene ug/kg ND 5.0 10/08/19 00:52
Hexachloro-1,3-butadiene ug/kg ND 5.0 10/08/19 00:52
Isopropylbenzene (Cumene)ug/kg ND 5.0 10/08/19 00:52
m&p-Xylene ug/kg ND 10.0 10/08/19 00:52
Methyl-tert-butyl ether ug/kg ND 5.0 10/08/19 00:52
Methylene Chloride ug/kg ND 20.0 10/08/19 00:52
n-Butylbenzene ug/kg ND 5.0 10/08/19 00:52
n-Propylbenzene ug/kg ND 5.0 10/08/19 00:52
Naphthalene ug/kg ND 5.0 10/08/19 00:52
o-Xylene ug/kg ND 5.0 10/08/19 00:52
p-Isopropyltoluene ug/kg ND 5.0 10/08/19 00:52
sec-Butylbenzene ug/kg ND 5.0 10/08/19 00:52
Styrene ug/kg ND 5.0 10/08/19 00:52
tert-Butylbenzene ug/kg ND 5.0 10/08/19 00:52
Tetrachloroethene ug/kg ND 5.0 10/08/19 00:52
Toluene ug/kg ND 5.0 10/08/19 00:52
trans-1,2-Dichloroethene ug/kg ND 5.0 10/08/19 00:52
trans-1,3-Dichloropropene ug/kg ND 5.0 10/08/19 00:52
Trichloroethene ug/kg ND 5.0 10/08/19 00:52
Trichlorofluoromethane ug/kg ND 5.0 10/08/19 00:52
Vinyl acetate ug/kg ND 50.0 IK,v210/08/19 00:52
Vinyl chloride ug/kg ND 10.0 10/08/19 00:52
Xylene (Total)ug/kg ND 10.0 10/08/19 00:52
1,2-Dichloroethane-d4 (S)%94 70-132 10/08/19 00:52
4-Bromofluorobenzene (S)%100 70-130 10/08/19 00:52
Toluene-d8 (S)%107 70-130 10/08/19 00:52
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2698777LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 54.950 110 70-130
1,1,1-Trichloroethane ug/kg 47.550 95 70-130
1,1,2,2-Tetrachloroethane ug/kg 57.850 116 55-130
1,1,2-Trichloroethane ug/kg 52.750 105 70-130
1,1-Dichloroethane ug/kg 49.850 100 68-130
1,1-Dichloroethene ug/kg 50.350 101 70-130
1,1-Dichloropropene ug/kg 49.650 99 70-130
1,2,3-Trichlorobenzene ug/kg 53.250 106 70-130
1,2,3-Trichloropropane ug/kg 60.950 122 70-130
1,2,4-Trichlorobenzene ug/kg 49.650 99 70-130
1,2,4-Trimethylbenzene ug/kg 53.150 106 69-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/11/2019 05:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92447918
Alamance 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2698777LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/kg 65.1 v150130 57-141
1,2-Dibromoethane (EDB)ug/kg 57.950 116 70-130
1,2-Dichlorobenzene ug/kg 52.250 104 70-130
1,2-Dichloroethane ug/kg 49.350 99 70-130
1,2-Dichloropropane ug/kg 51.950 104 70-130
1,3,5-Trimethylbenzene ug/kg 51.850 104 70-130
1,3-Dichlorobenzene ug/kg 50.950 102 70-130
1,3-Dichloropropane ug/kg 60.650 121 70-130
1,4-Dichlorobenzene ug/kg 51.550 103 70-130
2,2-Dichloropropane ug/kg 46.850 94 70-130
2-Butanone (MEK)ug/kg 118100 118 60-130
2-Chlorotoluene ug/kg 51.150 102 70-130
2-Hexanone ug/kg 124100 124 70-132
4-Chlorotoluene ug/kg 51.250 102 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 112100 112 69-130
Acetone ug/kg 122100 122 49-148
Benzene ug/kg 51.250 102 70-130
Bromobenzene ug/kg 52.650 105 70-130
Bromochloromethane ug/kg 50.650 101 70-130
Bromodichloromethane ug/kg 51.550 103 70-130
Bromoform ug/kg 58.150 116 68-136
Bromomethane ug/kg 53.050 106 60-140
Carbon tetrachloride ug/kg 46.450 93 70-130
Chlorobenzene ug/kg 51.350 103 70-130
Chloroethane ug/kg 60.850 122 51-147
Chloroform ug/kg 48.850 98 70-130
Chloromethane ug/kg 50.450 101 48-130
cis-1,2-Dichloroethene ug/kg 48.050 96 70-130
cis-1,3-Dichloropropene ug/kg 54.850 110 70-130
Dibromochloromethane ug/kg 57.250 114 70-130
Dibromomethane ug/kg 49.750 99 70-130
Dichlorodifluoromethane ug/kg 50.850 102 49-130
Diisopropyl ether ug/kg 52.150 104 66-130
Ethylbenzene ug/kg 50.950 102 70-130
Hexachloro-1,3-butadiene ug/kg 50.050 100 70-130
Isopropylbenzene (Cumene)ug/kg 51.750 103 70-130
m&p-Xylene ug/kg 105100 105 70-130
Methyl-tert-butyl ether ug/kg 54.850 110 70-130
Methylene Chloride ug/kg 44.350 89 50-137
n-Butylbenzene ug/kg 50.850 102 70-130
n-Propylbenzene ug/kg 52.250 104 70-130
Naphthalene ug/kg 59.050 118 70-131
o-Xylene ug/kg 52.850 106 70-130
p-Isopropyltoluene ug/kg 52.850 106 70-130
sec-Butylbenzene ug/kg 53.450 107 70-130
Styrene ug/kg 52.950 106 70-130
tert-Butylbenzene ug/kg 47.250 94 69-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/11/2019 05:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92447918
Alamance 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2698777LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/kg 49.450 99 56-130
Toluene ug/kg 46.650 93 70-130
trans-1,2-Dichloroethene ug/kg 48.350 97 70-130
trans-1,3-Dichloropropene ug/kg 52.650 105 70-130
Trichloroethene ug/kg 50.850 102 70-141
Trichlorofluoromethane ug/kg 49.650 99 67-130
Vinyl acetate ug/kg 82.5 IK,v310083 10-136
Vinyl chloride ug/kg 53.350 107 67-130
Xylene (Total)ug/kg 158150 105 70-130
1,2-Dichloroethane-d4 (S)%103 70-132
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%96 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2701039MATRIX SPIKE SAMPLE:
MSSpike
Result
92448206003
1,1,1,2-Tetrachloroethane ug/kg 16.720.3 83 52-133ND
1,1,1-Trichloroethane ug/kg 18.920.3 93 49-137ND
1,1,2,2-Tetrachloroethane ug/kg 16.720.3 83 39-150ND
1,1,2-Trichloroethane ug/kg 17.520.3 87 48-140ND
1,1-Dichloroethane ug/kg 19.320.3 96 46-135ND
1,1-Dichloroethene ug/kg 21.420.3 106 38-149ND
1,1-Dichloropropene ug/kg 17.220.3 85 41-140ND
1,2,3-Trichlorobenzene ug/kg 9.220.3 45 10-158ND
1,2,3-Trichloropropane ug/kg 18.420.3 91 33-157ND
1,2,4-Trichlorobenzene ug/kg 9.620.3 47 10-155ND
1,2,4-Trimethylbenzene ug/kg 14.520.3 72 24-154ND
1,2-Dibromo-3-chloropropane ug/kg 16.8 v120.3 83 33-158ND
1,2-Dibromoethane (EDB)ug/kg 17.220.3 85 40-136ND
1,2-Dichlorobenzene ug/kg 13.820.3 68 27-146ND
1,2-Dichloroethane ug/kg 17.520.3 87 49-140ND
1,2-Dichloropropane ug/kg 17.420.3 86 44-143ND
1,3,5-Trimethylbenzene ug/kg 15.520.3 77 40-144ND
1,3-Dichlorobenzene ug/kg 13.120.3 65 33-140ND
1,3-Dichloropropane ug/kg 18.8 v120.3 93 47-147ND
1,4-Dichlorobenzene ug/kg 13.320.3 66 35-139ND
2,2-Dichloropropane ug/kg 18.320.3 91 41-140ND
2-Butanone (MEK)ug/kg 32.7J40.5 81 10-181ND
2-Chlorotoluene ug/kg 15.920.3 78 38-147ND
2-Hexanone ug/kg 22.3J40.5 55 18-169ND
4-Chlorotoluene ug/kg 15.020.3 74 36-145ND
4-Methyl-2-pentanone (MIBK)ug/kg 31.9J40.5 79 16-175ND
Acetone ug/kg 62.3J40.5 154 10-200ND
Benzene ug/kg 19.020.3 94 46-136ND
Bromobenzene ug/kg 15.720.3 77 38-149ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/11/2019 05:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92447918
Alamance 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2701039MATRIX SPIKE SAMPLE:
MSSpike
Result
92448206003
Bromochloromethane ug/kg 17.920.3 89 44-142ND
Bromodichloromethane ug/kg 17.120.3 85 41-140ND
Bromoform ug/kg 15.420.3 76 34-145ND
Bromomethane ug/kg 18.320.3 90 14-162ND
Carbon tetrachloride ug/kg 18.620.3 92 44-141ND
Chlorobenzene ug/kg 16.020.3 79 39-141ND
Chloroethane ug/kg 25.1 v120.3 124 10-182ND
Chloroform ug/kg 17.620.3 87 45-140ND
Chloromethane ug/kg 20.520.3 101 19-149ND
cis-1,2-Dichloroethene ug/kg 17.820.3 88 38-150ND
cis-1,3-Dichloropropene ug/kg 14.920.3 74 30-144ND
Dibromochloromethane ug/kg 15.9 v120.3 79 36-145ND
Dibromomethane ug/kg 17.720.3 88 41-145ND
Dichlorodifluoromethane ug/kg 21.620.3 107 16-146ND
Diisopropyl ether ug/kg 18.320.3 91 41-143ND
Ethylbenzene ug/kg 17.520.3 86 35-144ND
Hexachloro-1,3-butadiene ug/kg 12.620.3 62 10-160ND
Isopropylbenzene (Cumene)ug/kg 17.220.3 85 30-152ND
m&p-Xylene ug/kg 34.540.5 85 33-145ND
Methyl-tert-butyl ether ug/kg 16.220.3 80 49-140ND
Methylene Chloride ug/kg 17.7J20.3 87 10-174ND
n-Butylbenzene ug/kg 14.420.3 71 10-160ND
n-Propylbenzene ug/kg 17.520.3 87 24-159ND
Naphthalene ug/kg 10.420.3 52 10-171ND
o-Xylene ug/kg 16.920.3 83 31-150ND
p-Isopropyltoluene ug/kg 15.720.3 78 21-154ND
sec-Butylbenzene ug/kg 17.620.3 87 19-159ND
Styrene ug/kg 14.320.3 71 15-152ND
tert-Butylbenzene ug/kg 15.820.3 78 31-141ND
Tetrachloroethene ug/kg 16.820.3 83 19-141ND
Toluene ug/kg 17.520.3 87 31-146ND
trans-1,2-Dichloroethene ug/kg 19.420.3 96 28-157ND
trans-1,3-Dichloropropene ug/kg 14.420.3 71 25-146ND
Trichloroethene ug/kg 17.920.3 88 34-149ND
Trichlorofluoromethane ug/kg 23.820.3 117 10-167ND
Vinyl acetate ug/kg 18.3J IK,v240.5 45 10-200ND
Vinyl chloride ug/kg 21.820.3 108 36-155ND
Xylene (Total)ug/kg 51.460.7 85 29-148ND
1,2-Dichloroethane-d4 (S)%108 70-132
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/11/2019 05:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92447918
Alamance 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92448206002
2701038SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg NDND
1,2-Dibromo-3-chloropropane ug/kg ND v1ND
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
1,3-Dichloropropane ug/kg ND v1ND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK)ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg NDND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK)ug/kg NDND
Acetone ug/kg NDND
Benzene ug/kg NDND
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg NDND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg ND v1ND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg ND v1ND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg NDND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg NDND
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene)ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/11/2019 05:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92447918
Alamance 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92448206002
2701038SAMPLE DUPLICATE:
m&p-Xylene ug/kg NDND
Methyl-tert-butyl ether ug/kg NDND
Methylene Chloride ug/kg NDND
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg NDND
Naphthalene ug/kg NDND
o-Xylene ug/kg NDND
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg NDND
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg NDND
Toluene ug/kg NDND
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg ND IK,v2ND
Vinyl chloride ug/kg NDND
Xylene (Total)ug/kg NDND
1,2-Dichloroethane-d4 (S)%9899
4-Bromofluorobenzene (S)%99100
Toluene-d8 (S)%104104
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/11/2019 05:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92447918
Alamance 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
502304
EPA 5035A
EPA 8260D
8260D MSV 5035A Volatile Organics
Associated Lab Samples: 92447918002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2700586
Associated Lab Samples:92447918002
Matrix: Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 10/08/19 13:04
1,1,1-Trichloroethane ug/kg ND 5.0 10/08/19 13:04
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 10/08/19 13:04
1,1,2-Trichloroethane ug/kg ND 5.0 10/08/19 13:04
1,1-Dichloroethane ug/kg ND 5.0 10/08/19 13:04
1,1-Dichloroethene ug/kg ND 5.0 10/08/19 13:04
1,1-Dichloropropene ug/kg ND 5.0 10/08/19 13:04
1,2,3-Trichlorobenzene ug/kg ND 5.0 10/08/19 13:04
1,2,3-Trichloropropane ug/kg ND 5.0 10/08/19 13:04
1,2,4-Trichlorobenzene ug/kg ND 5.0 10/08/19 13:04
1,2,4-Trimethylbenzene ug/kg ND 5.0 v110/08/19 13:04
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 10/08/19 13:04
1,2-Dibromoethane (EDB)ug/kg ND 5.0 10/08/19 13:04
1,2-Dichlorobenzene ug/kg ND 5.0 10/08/19 13:04
1,2-Dichloroethane ug/kg ND 5.0 10/08/19 13:04
1,2-Dichloropropane ug/kg ND 5.0 10/08/19 13:04
1,3,5-Trimethylbenzene ug/kg ND 5.0 10/08/19 13:04
1,3-Dichlorobenzene ug/kg ND 5.0 10/08/19 13:04
1,3-Dichloropropane ug/kg ND 5.0 10/08/19 13:04
1,4-Dichlorobenzene ug/kg ND 5.0 10/08/19 13:04
2,2-Dichloropropane ug/kg ND 5.0 10/08/19 13:04
2-Butanone (MEK)ug/kg ND 100 10/08/19 13:04
2-Chlorotoluene ug/kg ND 5.0 10/08/19 13:04
2-Hexanone ug/kg ND 50.0 10/08/19 13:04
4-Chlorotoluene ug/kg ND 5.0 10/08/19 13:04
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 10/08/19 13:04
Acetone ug/kg ND 100 10/08/19 13:04
Benzene ug/kg ND 5.0 10/08/19 13:04
Bromobenzene ug/kg ND 5.0 10/08/19 13:04
Bromochloromethane ug/kg ND 5.0 10/08/19 13:04
Bromodichloromethane ug/kg ND 5.0 10/08/19 13:04
Bromoform ug/kg ND 5.0 10/08/19 13:04
Bromomethane ug/kg ND 10.0 10/08/19 13:04
Carbon tetrachloride ug/kg ND 5.0 10/08/19 13:04
Chlorobenzene ug/kg ND 5.0 10/08/19 13:04
Chloroethane ug/kg ND 10.0 v110/08/19 13:04
Chloroform ug/kg ND 5.0 10/08/19 13:04
Chloromethane ug/kg ND 10.0 10/08/19 13:04
cis-1,2-Dichloroethene ug/kg ND 5.0 10/08/19 13:04
cis-1,3-Dichloropropene ug/kg ND 5.0 10/08/19 13:04
Dibromochloromethane ug/kg ND 5.0 10/08/19 13:04
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/11/2019 05:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92447918
Alamance 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2700586
Associated Lab Samples:92447918002
Matrix: Solid
Analyzed
Dibromomethane ug/kg ND 5.0 10/08/19 13:04
Dichlorodifluoromethane ug/kg ND 10.0 10/08/19 13:04
Diisopropyl ether ug/kg ND 5.0 10/08/19 13:04
Ethylbenzene ug/kg ND 5.0 10/08/19 13:04
Hexachloro-1,3-butadiene ug/kg ND 5.0 10/08/19 13:04
Isopropylbenzene (Cumene)ug/kg ND 5.0 10/08/19 13:04
m&p-Xylene ug/kg ND 10.0 10/08/19 13:04
Methyl-tert-butyl ether ug/kg ND 5.0 10/08/19 13:04
Methylene Chloride ug/kg ND 20.0 10/08/19 13:04
n-Butylbenzene ug/kg ND 5.0 10/08/19 13:04
n-Propylbenzene ug/kg ND 5.0 10/08/19 13:04
Naphthalene ug/kg ND 5.0 10/08/19 13:04
o-Xylene ug/kg ND 5.0 10/08/19 13:04
p-Isopropyltoluene ug/kg ND 5.0 10/08/19 13:04
sec-Butylbenzene ug/kg ND 5.0 10/08/19 13:04
Styrene ug/kg ND 5.0 10/08/19 13:04
tert-Butylbenzene ug/kg ND 5.0 10/08/19 13:04
Tetrachloroethene ug/kg ND 5.0 10/08/19 13:04
Toluene ug/kg ND 5.0 10/08/19 13:04
trans-1,2-Dichloroethene ug/kg ND 5.0 10/08/19 13:04
trans-1,3-Dichloropropene ug/kg ND 5.0 10/08/19 13:04
Trichloroethene ug/kg ND 5.0 10/08/19 13:04
Trichlorofluoromethane ug/kg ND 5.0 10/08/19 13:04
Vinyl acetate ug/kg ND 50.0 IK10/08/19 13:04
Vinyl chloride ug/kg ND 10.0 10/08/19 13:04
Xylene (Total)ug/kg ND 10.0 10/08/19 13:04
1,2-Dichloroethane-d4 (S)%95 70-132 10/08/19 13:04
4-Bromofluorobenzene (S)%103 70-130 10/08/19 13:04
Toluene-d8 (S)%106 70-130 10/08/19 13:04
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2700587LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 52.850 106 70-130
1,1,1-Trichloroethane ug/kg 47.950 96 70-130
1,1,2,2-Tetrachloroethane ug/kg 54.750 109 55-130
1,1,2-Trichloroethane ug/kg 52.150 104 70-130
1,1-Dichloroethane ug/kg 49.950 100 68-130
1,1-Dichloroethene ug/kg 51.450 103 70-130
1,1-Dichloropropene ug/kg 51.750 103 70-130
1,2,3-Trichlorobenzene ug/kg 55.950 112 70-130
1,2,3-Trichloropropane ug/kg 57.850 116 70-130
1,2,4-Trichlorobenzene ug/kg 53.250 106 70-130
1,2,4-Trimethylbenzene ug/kg 58.2 v150116 69-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/11/2019 05:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92447918
Alamance 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2700587LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/kg 64.550 129 57-141
1,2-Dibromoethane (EDB)ug/kg 55.850 112 70-130
1,2-Dichlorobenzene ug/kg 53.150 106 70-130
1,2-Dichloroethane ug/kg 47.150 94 70-130
1,2-Dichloropropane ug/kg 51.650 103 70-130
1,3,5-Trimethylbenzene ug/kg 54.150 108 70-130
1,3-Dichlorobenzene ug/kg 52.350 105 70-130
1,3-Dichloropropane ug/kg 58.050 116 70-130
1,4-Dichlorobenzene ug/kg 52.650 105 70-130
2,2-Dichloropropane ug/kg 48.750 97 70-130
2-Butanone (MEK)ug/kg 115100 115 60-130
2-Chlorotoluene ug/kg 51.750 103 70-130
2-Hexanone ug/kg 121100 121 70-132
4-Chlorotoluene ug/kg 52.950 106 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 110100 110 69-130
Acetone ug/kg 115100 115 49-148
Benzene ug/kg 51.450 103 70-130
Bromobenzene ug/kg 53.650 107 70-130
Bromochloromethane ug/kg 50.750 101 70-130
Bromodichloromethane ug/kg 49.850 100 70-130
Bromoform ug/kg 54.450 109 68-136
Bromomethane ug/kg 50.750 101 60-140
Carbon tetrachloride ug/kg 46.150 92 70-130
Chlorobenzene ug/kg 50.550 101 70-130
Chloroethane ug/kg 58.8 v150118 51-147
Chloroform ug/kg 47.750 95 70-130
Chloromethane ug/kg 51.750 103 48-130
cis-1,2-Dichloroethene ug/kg 48.650 97 70-130
cis-1,3-Dichloropropene ug/kg 53.950 108 70-130
Dibromochloromethane ug/kg 54.550 109 70-130
Dibromomethane ug/kg 50.250 100 70-130
Dichlorodifluoromethane ug/kg 49.750 99 49-130
Diisopropyl ether ug/kg 52.850 106 66-130
Ethylbenzene ug/kg 52.350 105 70-130
Hexachloro-1,3-butadiene ug/kg 54.250 108 70-130
Isopropylbenzene (Cumene)ug/kg 52.950 106 70-130
m&p-Xylene ug/kg 106100 106 70-130
Methyl-tert-butyl ether ug/kg 53.850 108 70-130
Methylene Chloride ug/kg 44.450 89 50-137
n-Butylbenzene ug/kg 55.550 111 70-130
n-Propylbenzene ug/kg 55.250 110 70-130
Naphthalene ug/kg 60.950 122 70-131
o-Xylene ug/kg 53.250 106 70-130
p-Isopropyltoluene ug/kg 55.350 111 70-130
sec-Butylbenzene ug/kg 56.150 112 70-130
Styrene ug/kg 52.650 105 70-130
tert-Butylbenzene ug/kg 48.350 97 69-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/11/2019 05:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92447918
Alamance 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2700587LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/kg 50.150 100 56-130
Toluene ug/kg 46.850 94 70-130
trans-1,2-Dichloroethene ug/kg 49.050 98 70-130
trans-1,3-Dichloropropene ug/kg 52.250 104 70-130
Trichloroethene ug/kg 51.750 103 70-141
Trichlorofluoromethane ug/kg 52.150 104 67-130
Vinyl acetate ug/kg 91.4 IK10091 10-136
Vinyl chloride ug/kg 52.650 105 67-130
Xylene (Total)ug/kg 160150 106 70-130
1,2-Dichloroethane-d4 (S)%107 70-132
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%95 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2700588MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92447960002
2700589
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/kg 811 92 52-13393 1811ND748 757
1,1,1-Trichloroethane ug/kg 811 102 49-137102 0811ND830 829
1,1,2,2-Tetrachloroethane ug/kg 811 108 39-150111 3811ND872 898
1,1,2-Trichloroethane ug/kg 811 104 48-140107 2811ND846 867
1,1-Dichloroethane ug/kg 811 105 46-135109 4811ND854 886
1,1-Dichloroethene ug/kg 811 52 38-14956 8811ND418 453
1,1-Dichloropropene ug/kg 811 102 41-140103 1811ND831 836
1,2,3-Trichlorobenzene ug/kg 811 108 10-158112 3811ND875 904
1,2,3-Trichloropropane ug/kg 811 110 33-157112 1811ND896 909
1,2,4-Trichlorobenzene ug/kg 811 113 10-155112 1811ND918 911
1,2,4-Trimethylbenzene ug/kg v181110624-154106 0811ND930 929
1,2-Dibromo-3-chloropropane ug/kg 811 99 33-158102 2811ND806 824
1,2-Dibromoethane (EDB)ug/kg 811 101 40-136107 5811ND822 867
1,2-Dichlorobenzene ug/kg 811 108 27-146110 2811ND873 892
1,2-Dichloroethane ug/kg 811 103 49-140107 3811ND838 864
1,2-Dichloropropane ug/kg 811 105 44-143110 5811ND853 895
1,3,5-Trimethylbenzene ug/kg 811 104 40-144107 3811ND841 867
1,3-Dichlorobenzene ug/kg 811 104 33-140106 2811ND844 861
1,3-Dichloropropane ug/kg 811 112 47-147112 0811ND908 907
1,4-Dichlorobenzene ug/kg 811 104 35-139110 5811ND844 891
2,2-Dichloropropane ug/kg 811 103 41-140106 2811ND838 856
2-Butanone (MEK)ug/kg 1620 107 10-1811111620ND1740J 1790J
2-Chlorotoluene ug/kg 811 103 38-147108 5811ND834 878
2-Hexanone ug/kg 1620 91 18-169931620ND1470J 1520J
4-Chlorotoluene ug/kg 811 105 36-145109 4811ND852 885
4-Methyl-2-pentanone (MIBK) ug/kg 1620 105 16-1751041620ND1700J 1690J
Acetone ug/kg 1620 73 10-200881620ND1190J 1420J
Benzene ug/kg 811 107 46-136111 3811ND869 900
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/11/2019 05:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92447918
Alamance 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2700588MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92447960002
2700589
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Bromobenzene ug/kg 811 105 38-149111 5811ND851 899
Bromochloromethane ug/kg 811 107 44-142109 1811ND869 881
Bromodichloromethane ug/kg 811 95 41-14097 2811ND768 787
Bromoform ug/kg 811 83 34-14582 1811ND672 667
Bromomethane ug/kg 811 104 14-162107 3811ND842 870
Carbon tetrachloride ug/kg 811 88 44-14190 2811ND715 732
Chlorobenzene ug/kg 811 100 39-141105 5811ND814 854
Chloroethane ug/kg v18116410-18268 6811ND523 554
Chloroform ug/kg 811 104 45-140107 3811ND842 867
Chloromethane ug/kg 811 117 19-149115 2811ND952 934
cis-1,2-Dichloroethene ug/kg 811 109 38-150108 1811ND885 879
cis-1,3-Dichloropropene ug/kg 811 104 30-144106 2811ND840 857
Dibromochloromethane ug/kg 811 89 36-14589 0811ND720 721
Dibromomethane ug/kg 811 101 41-145104 3811ND820 842
Dichlorodifluoromethane ug/kg 811 106 16-146110 4811ND863 896
Diisopropyl ether ug/kg 811 97 41-143100 3811ND789 811
Ethylbenzene ug/kg 811 106 35-144109 3811ND861 886
Hexachloro-1,3-butadiene ug/kg 811 104 10-160111 7811ND840 897
Isopropylbenzene (Cumene) ug/kg 811 105 30-152110 4811ND850 889
m&p-Xylene ug/kg 1620 104 33-145109 41620ND1770 1830
Methyl-tert-butyl ether ug/kg 811 105 49-14097 8811ND852 786
Methylene Chloride ug/kg 811 105 10-174106 1811ND847 856
n-Butylbenzene ug/kg 811 109 10-160112 3811ND880 911
n-Propylbenzene ug/kg 811 107 24-159111 4811ND868 903
Naphthalene ug/kg 811 107 10-171112 4811ND948 990
o-Xylene ug/kg 811 104 31-150108 381148.5J 895 927
p-Isopropyltoluene ug/kg 811 108 21-154113 5811ND876 916
sec-Butylbenzene ug/kg 811 110 19-159115 4811ND889 929
Styrene ug/kg 811 105 15-152108 2811ND855 874
tert-Butylbenzene ug/kg 811 94 31-14198 4811ND760 793
Tetrachloroethene ug/kg 811 96 19-14198 2811ND778 792
Toluene ug/kg 811 93 31-14698 5811ND804 849
trans-1,2-Dichloroethene ug/kg 811 102 28-157112 9811ND830 912
trans-1,3-Dichloropropene ug/kg 811 99 25-146100 1811ND803 813
Trichloroethene ug/kg 811 138 34-149113 781117002820 2620
Trichlorofluoromethane ug/kg 811 48 10-16748 0811ND392 391
Vinyl acetate ug/kg IK162011710-2001161620ND1900J 1890J
Vinyl chloride ug/kg 811 111 36-155115 4811ND898 932
Xylene (Total)ug/kg 2430 109 29-148113 42430ND2660 2760
1,2-Dichloroethane-d4 (S)%115 70-132113
4-Bromofluorobenzene (S)%99 70-130100
Toluene-d8 (S)%100 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/11/2019 05:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92447918
Alamance 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
502890
EPA 5035A
EPA 8260D
8260D MSV 5035A Volatile Organics
Associated Lab Samples: 92447918003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2703286
Associated Lab Samples:92447918003
Matrix: Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 10/10/19 16:59
1,1,1-Trichloroethane ug/kg ND 5.0 10/10/19 16:59
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 10/10/19 16:59
1,1,2-Trichloroethane ug/kg ND 5.0 10/10/19 16:59
1,1-Dichloroethane ug/kg ND 5.0 10/10/19 16:59
1,1-Dichloroethene ug/kg ND 5.0 10/10/19 16:59
1,1-Dichloropropene ug/kg ND 5.0 10/10/19 16:59
1,2,3-Trichlorobenzene ug/kg ND 5.0 10/10/19 16:59
1,2,3-Trichloropropane ug/kg ND 5.0 10/10/19 16:59
1,2,4-Trichlorobenzene ug/kg ND 5.0 10/10/19 16:59
1,2,4-Trimethylbenzene ug/kg ND 5.0 10/10/19 16:59
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 10/10/19 16:59
1,2-Dibromoethane (EDB)ug/kg ND 5.0 10/10/19 16:59
1,2-Dichlorobenzene ug/kg ND 5.0 10/10/19 16:59
1,2-Dichloroethane ug/kg ND 5.0 10/10/19 16:59
1,2-Dichloropropane ug/kg ND 5.0 10/10/19 16:59
1,3,5-Trimethylbenzene ug/kg ND 5.0 10/10/19 16:59
1,3-Dichlorobenzene ug/kg ND 5.0 10/10/19 16:59
1,3-Dichloropropane ug/kg ND 5.0 10/10/19 16:59
1,4-Dichlorobenzene ug/kg ND 5.0 10/10/19 16:59
2,2-Dichloropropane ug/kg ND 5.0 10/10/19 16:59
2-Butanone (MEK)ug/kg ND 100 10/10/19 16:59
2-Chlorotoluene ug/kg ND 5.0 10/10/19 16:59
2-Hexanone ug/kg ND 50.0 10/10/19 16:59
4-Chlorotoluene ug/kg ND 5.0 10/10/19 16:59
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 10/10/19 16:59
Acetone ug/kg ND 100 10/10/19 16:59
Benzene ug/kg ND 5.0 10/10/19 16:59
Bromobenzene ug/kg ND 5.0 10/10/19 16:59
Bromochloromethane ug/kg ND 5.0 10/10/19 16:59
Bromodichloromethane ug/kg ND 5.0 10/10/19 16:59
Bromoform ug/kg ND 5.0 10/10/19 16:59
Bromomethane ug/kg ND 10.0 10/10/19 16:59
Carbon tetrachloride ug/kg ND 5.0 10/10/19 16:59
Chlorobenzene ug/kg ND 5.0 10/10/19 16:59
Chloroethane ug/kg ND 10.0 10/10/19 16:59
Chloroform ug/kg ND 5.0 10/10/19 16:59
Chloromethane ug/kg ND 10.0 10/10/19 16:59
cis-1,2-Dichloroethene ug/kg ND 5.0 10/10/19 16:59
cis-1,3-Dichloropropene ug/kg ND 5.0 10/10/19 16:59
Dibromochloromethane ug/kg ND 5.0 10/10/19 16:59
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/11/2019 05:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92447918
Alamance 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2703286
Associated Lab Samples:92447918003
Matrix: Solid
Analyzed
Dibromomethane ug/kg ND 5.0 10/10/19 16:59
Dichlorodifluoromethane ug/kg ND 10.0 10/10/19 16:59
Diisopropyl ether ug/kg ND 5.0 10/10/19 16:59
Ethylbenzene ug/kg ND 5.0 10/10/19 16:59
Hexachloro-1,3-butadiene ug/kg ND 5.0 10/10/19 16:59
Isopropylbenzene (Cumene)ug/kg ND 5.0 10/10/19 16:59
m&p-Xylene ug/kg ND 10.0 10/10/19 16:59
Methyl-tert-butyl ether ug/kg ND 5.0 10/10/19 16:59
Methylene Chloride ug/kg ND 20.0 10/10/19 16:59
n-Butylbenzene ug/kg ND 5.0 10/10/19 16:59
n-Propylbenzene ug/kg ND 5.0 10/10/19 16:59
Naphthalene ug/kg ND 5.0 10/10/19 16:59
o-Xylene ug/kg ND 5.0 10/10/19 16:59
p-Isopropyltoluene ug/kg ND 5.0 10/10/19 16:59
sec-Butylbenzene ug/kg ND 5.0 10/10/19 16:59
Styrene ug/kg ND 5.0 10/10/19 16:59
tert-Butylbenzene ug/kg ND 5.0 10/10/19 16:59
Tetrachloroethene ug/kg ND 5.0 10/10/19 16:59
Toluene ug/kg ND 5.0 10/10/19 16:59
trans-1,2-Dichloroethene ug/kg ND 5.0 10/10/19 16:59
trans-1,3-Dichloropropene ug/kg ND 5.0 10/10/19 16:59
Trichloroethene ug/kg ND 5.0 10/10/19 16:59
Trichlorofluoromethane ug/kg ND 5.0 10/10/19 16:59
Vinyl acetate ug/kg ND 50.0 10/10/19 16:59
Vinyl chloride ug/kg ND 10.0 10/10/19 16:59
Xylene (Total)ug/kg ND 10.0 10/10/19 16:59
1,2-Dichloroethane-d4 (S)%95 70-132 10/10/19 16:59
4-Bromofluorobenzene (S)%102 70-130 10/10/19 16:59
Toluene-d8 (S)%102 70-130 10/10/19 16:59
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2703287LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 52.050 104 70-130
1,1,1-Trichloroethane ug/kg 50.450 101 70-130
1,1,2,2-Tetrachloroethane ug/kg 52.050 104 55-130
1,1,2-Trichloroethane ug/kg 50.650 101 70-130
1,1-Dichloroethane ug/kg 51.750 103 68-130
1,1-Dichloroethene ug/kg 55.850 112 70-130
1,1-Dichloropropene ug/kg 49.150 98 70-130
1,2,3-Trichlorobenzene ug/kg 49.150 98 70-130
1,2,3-Trichloropropane ug/kg 53.050 106 70-130
1,2,4-Trichlorobenzene ug/kg 46.250 92 70-130
1,2,4-Trimethylbenzene ug/kg 47.750 95 69-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/11/2019 05:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92447918
Alamance 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2703287LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/kg 51.850 104 57-141
1,2-Dibromoethane (EDB)ug/kg 53.750 107 70-130
1,2-Dichlorobenzene ug/kg 49.350 99 70-130
1,2-Dichloroethane ug/kg 51.550 103 70-130
1,2-Dichloropropane ug/kg 51.350 103 70-130
1,3,5-Trimethylbenzene ug/kg 49.650 99 70-130
1,3-Dichlorobenzene ug/kg 47.650 95 70-130
1,3-Dichloropropane ug/kg 53.650 107 70-130
1,4-Dichlorobenzene ug/kg 47.850 96 70-130
2,2-Dichloropropane ug/kg 51.850 104 70-130
2-Butanone (MEK)ug/kg 95.2J100 95 60-130
2-Chlorotoluene ug/kg 48.250 96 70-130
2-Hexanone ug/kg 98.2100 98 70-132
4-Chlorotoluene ug/kg 48.550 97 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 98.0100 98 69-130
Acetone ug/kg 97.1J100 97 49-148
Benzene ug/kg 52.450 105 70-130
Bromobenzene ug/kg 48.350 97 70-130
Bromochloromethane ug/kg 52.750 105 70-130
Bromodichloromethane ug/kg 51.950 104 70-130
Bromoform ug/kg 53.350 107 68-136
Bromomethane ug/kg 53.050 106 60-140
Carbon tetrachloride ug/kg 48.750 97 70-130
Chlorobenzene ug/kg 49.850 100 70-130
Chloroethane ug/kg 53.450 107 51-147
Chloroform ug/kg 52.350 105 70-130
Chloromethane ug/kg 55.550 111 48-130
cis-1,2-Dichloroethene ug/kg 53.250 106 70-130
cis-1,3-Dichloropropene ug/kg 55.550 111 70-130
Dibromochloromethane ug/kg 51.450 103 70-130
Dibromomethane ug/kg 48.350 97 70-130
Dichlorodifluoromethane ug/kg 54.550 109 49-130
Diisopropyl ether ug/kg 54.850 110 66-130
Ethylbenzene ug/kg 51.250 102 70-130
Hexachloro-1,3-butadiene ug/kg 48.250 96 70-130
Isopropylbenzene (Cumene)ug/kg 51.850 104 70-130
m&p-Xylene ug/kg 101100 101 70-130
Methyl-tert-butyl ether ug/kg 51.750 103 70-130
Methylene Chloride ug/kg 49.250 98 50-137
n-Butylbenzene ug/kg 48.350 97 70-130
n-Propylbenzene ug/kg 49.550 99 70-130
Naphthalene ug/kg 48.950 98 70-131
o-Xylene ug/kg 51.550 103 70-130
p-Isopropyltoluene ug/kg 50.250 100 70-130
sec-Butylbenzene ug/kg 50.450 101 70-130
Styrene ug/kg 49.750 99 70-130
tert-Butylbenzene ug/kg 44.450 89 69-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/11/2019 05:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92447918
Alamance 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2703287LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/kg 50.150 100 56-130
Toluene ug/kg 49.150 98 70-130
trans-1,2-Dichloroethene ug/kg 53.050 106 70-130
trans-1,3-Dichloropropene ug/kg 50.150 100 70-130
Trichloroethene ug/kg 50.550 101 70-141
Trichlorofluoromethane ug/kg 52.450 105 67-130
Vinyl acetate ug/kg 88.7100 89 10-136
Vinyl chloride ug/kg 53.150 106 67-130
Xylene (Total)ug/kg 153150 102 70-130
1,2-Dichloroethane-d4 (S)%102 70-132
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%95 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2703288MATRIX SPIKE SAMPLE:
MSSpike
Result
92448136001
1,1,1,2-Tetrachloroethane ug/kg 13.320.4 65 52-133ND
1,1,1-Trichloroethane ug/kg 17.420.4 85 49-137ND
1,1,2,2-Tetrachloroethane ug/kg ND M120.4 0 39-150ND
1,1,2-Trichloroethane ug/kg 9.5 M120.4 47 48-140ND
1,1-Dichloroethane ug/kg 21.720.4 106 46-135ND
1,1-Dichloroethene ug/kg 31.3 M120.4 153 38-149ND
1,1-Dichloropropene ug/kg 15.120.4 74 41-140ND
1,2,3-Trichlorobenzene ug/kg 5.720.4 28 10-158ND
1,2,3-Trichloropropane ug/kg 16.020.4 78 33-157ND
1,2,4-Trichlorobenzene ug/kg 5.520.4 27 10-155ND
1,2,4-Trimethylbenzene ug/kg 11.420.4 56 24-154ND
1,2-Dibromo-3-chloropropane ug/kg 9.420.4 46 33-158ND
1,2-Dibromoethane (EDB)ug/kg 17.820.4 87 40-136ND
1,2-Dichlorobenzene ug/kg 10.320.4 50 27-146ND
1,2-Dichloroethane ug/kg 20.320.4 100 49-140ND
1,2-Dichloropropane ug/kg 18.020.4 88 44-143ND
1,3,5-Trimethylbenzene ug/kg 10.220.4 50 40-144ND
1,3-Dichlorobenzene ug/kg 1020.4 49 33-140ND
1,3-Dichloropropane ug/kg 19.620.4 96 47-147ND
1,4-Dichlorobenzene ug/kg 10.120.4 50 35-139ND
2,2-Dichloropropane ug/kg 19.020.4 93 41-140ND
2-Butanone (MEK)ug/kg 40.9J40.8 72 10-181ND
2-Chlorotoluene ug/kg 11.520.4 57 38-147ND
2-Hexanone ug/kg 39.2J40.8 96 18-169ND
4-Chlorotoluene ug/kg 12.120.4 59 36-145ND
4-Methyl-2-pentanone (MIBK)ug/kg 38.2J40.8 77 16-175ND
Acetone ug/kg 10940.8 26 10-200ND
Benzene ug/kg 18.720.4 91 46-136ND
Bromobenzene ug/kg 13.420.4 66 38-149ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/11/2019 05:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92447918
Alamance 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2703288MATRIX SPIKE SAMPLE:
MSSpike
Result
92448136001
Bromochloromethane ug/kg 23.120.4 113 44-142ND
Bromodichloromethane ug/kg 16.020.4 79 41-140ND
Bromoform ug/kg 13.520.4 66 34-145ND
Bromomethane ug/kg 25.620.4 125 14-162ND
Carbon tetrachloride ug/kg 16.120.4 79 44-141ND
Chlorobenzene ug/kg 14.420.4 70 39-141ND
Chloroethane ug/kg 31.820.4 156 10-182ND
Chloroform ug/kg 20.820.4 102 45-140ND
Chloromethane ug/kg 30.120.4 147 19-149ND
cis-1,2-Dichloroethene ug/kg 21.720.4 106 38-150ND
cis-1,3-Dichloropropene ug/kg 17.720.4 87 30-144ND
Dibromochloromethane ug/kg 14.520.4 71 36-145ND
Dibromomethane ug/kg 20.320.4 99 41-145ND
Dichlorodifluoromethane ug/kg 24.620.4 121 16-146ND
Diisopropyl ether ug/kg 19.320.4 95 41-143ND
Ethylbenzene ug/kg 13.020.4 64 35-144ND
Hexachloro-1,3-butadiene ug/kg 4.1J20.4 20 10-160ND
Isopropylbenzene (Cumene)ug/kg 10.920.4 53 30-152ND
m&p-Xylene ug/kg 26.440.8 65 33-145ND
Methyl-tert-butyl ether ug/kg 17.320.4 85 49-140ND
Methylene Chloride ug/kg 32.620.4 143 10-174ND
n-Butylbenzene ug/kg 8.320.4 41 10-160ND
n-Propylbenzene ug/kg 13.120.4 64 24-159ND
Naphthalene ug/kg 9.920.4 49 10-171ND
o-Xylene ug/kg 12.720.4 62 31-150ND
p-Isopropyltoluene ug/kg 8.420.4 41 21-154ND
sec-Butylbenzene ug/kg 9.320.4 46 19-159ND
Styrene ug/kg 13.020.4 64 15-152ND
tert-Butylbenzene ug/kg 8.420.4 41 31-141ND
Tetrachloroethene ug/kg 12.520.4 61 19-141ND
Toluene ug/kg 15.120.4 74 31-146ND
trans-1,2-Dichloroethene ug/kg 21.320.4 104 28-157ND
trans-1,3-Dichloropropene ug/kg 16.720.4 82 25-146ND
Trichloroethene ug/kg 27.220.4 133 34-149ND
Trichlorofluoromethane ug/kg 21.920.4 107 10-167ND
Vinyl acetate ug/kg 20.8J40.8 51 10-200ND
Vinyl chloride ug/kg 27.920.4 137 36-155ND
Xylene (Total)ug/kg 39.261.3 64 29-148ND
1,2-Dichloroethane-d4 (S)%103 70-132
4-Bromofluorobenzene (S)%95 70-130
Toluene-d8 (S)%94 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/11/2019 05:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92447918
Alamance 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92448222013
2704364SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg NDND
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK)ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg NDND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK)ug/kg NDND
Acetone ug/kg NDND
Benzene ug/kg NDND
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg NDND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg NDND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg NDND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg NDND
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene)ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/11/2019 05:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92447918
Alamance 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92448222013
2704364SAMPLE DUPLICATE:
m&p-Xylene ug/kg NDND
Methyl-tert-butyl ether ug/kg NDND
Methylene Chloride ug/kg NDND
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg NDND
Naphthalene ug/kg NDND
o-Xylene ug/kg NDND
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg NDND
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg NDND
Toluene ug/kg NDND
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg NDND
Xylene (Total)ug/kg NDND
1,2-Dichloroethane-d4 (S)%138 S3105
4-Bromofluorobenzene (S)%107100
Toluene-d8 (S)%106102
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/11/2019 05:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92447918
Alamance 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
502058
EPA 3546
EPA 8270D
8270 Solid MSSV Microwave
Associated Lab Samples: 92447918001, 92447918002, 92447918003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2699595
Associated Lab Samples:92447918001, 92447918002, 92447918003
Matrix: Solid
Analyzed
1,2,4-Trichlorobenzene ug/kg ND 326 10/08/19 11:38
1,2-Dichlorobenzene ug/kg ND 326 10/08/19 11:38
1,3-Dichlorobenzene ug/kg ND 326 10/08/19 11:38
1,4-Dichlorobenzene ug/kg ND 326 10/08/19 11:38
1-Methylnaphthalene ug/kg ND 326 10/08/19 11:38
2,2'-Oxybis(1-chloropropane)ug/kg ND 326 10/08/19 11:38
2,4,5-Trichlorophenol ug/kg ND 326 10/08/19 11:38
2,4,6-Trichlorophenol ug/kg ND 326 10/08/19 11:38
2,4-Dichlorophenol ug/kg ND 326 10/08/19 11:38
2,4-Dimethylphenol ug/kg ND 326 10/08/19 11:38
2,4-Dinitrophenol ug/kg ND 1630 10/08/19 11:38
2,4-Dinitrotoluene ug/kg ND 326 10/08/19 11:38
2,6-Dinitrotoluene ug/kg ND 326 10/08/19 11:38
2-Chloronaphthalene ug/kg ND 326 10/08/19 11:38
2-Chlorophenol ug/kg ND 326 10/08/19 11:38
2-Methylnaphthalene ug/kg ND 326 10/08/19 11:38
2-Methylphenol(o-Cresol)ug/kg ND 326 10/08/19 11:38
2-Nitroaniline ug/kg ND 1630 10/08/19 11:38
2-Nitrophenol ug/kg ND 326 10/08/19 11:38
3&4-Methylphenol(m&p Cresol)ug/kg ND 326 10/08/19 11:38
3,3'-Dichlorobenzidine ug/kg ND 1630 10/08/19 11:38
3-Nitroaniline ug/kg ND 1630 10/08/19 11:38
4,6-Dinitro-2-methylphenol ug/kg ND 651 10/08/19 11:38
4-Bromophenylphenyl ether ug/kg ND 326 10/08/19 11:38
4-Chloro-3-methylphenol ug/kg ND 651 10/08/19 11:38
4-Chloroaniline ug/kg ND 1630 10/08/19 11:38
4-Chlorophenylphenyl ether ug/kg ND 326 10/08/19 11:38
4-Nitroaniline ug/kg ND 651 10/08/19 11:38
4-Nitrophenol ug/kg ND 1630 10/08/19 11:38
Acenaphthene ug/kg ND 326 10/08/19 11:38
Acenaphthylene ug/kg ND 326 10/08/19 11:38
Aniline ug/kg ND 326 10/08/19 11:38
Anthracene ug/kg ND 326 10/08/19 11:38
Benzo(a)anthracene ug/kg ND 326 10/08/19 11:38
Benzo(a)pyrene ug/kg ND 326 10/08/19 11:38
Benzo(b)fluoranthene ug/kg ND 326 10/08/19 11:38
Benzo(g,h,i)perylene ug/kg ND 326 10/08/19 11:38
Benzo(k)fluoranthene ug/kg ND 326 10/08/19 11:38
Benzoic Acid ug/kg ND 1630 10/08/19 11:38
Benzyl alcohol ug/kg ND 651 10/08/19 11:38
bis(2-Chloroethoxy)methane ug/kg ND 326 10/08/19 11:38
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/11/2019 05:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92447918
Alamance 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2699595
Associated Lab Samples:92447918001, 92447918002, 92447918003
Matrix: Solid
Analyzed
bis(2-Chloroethyl) ether ug/kg ND 326 10/08/19 11:38
bis(2-Ethylhexyl)phthalate ug/kg ND 326 10/08/19 11:38
Butylbenzylphthalate ug/kg ND 326 10/08/19 11:38
Chrysene ug/kg ND 326 10/08/19 11:38
Di-n-butylphthalate ug/kg ND 326 10/08/19 11:38
Di-n-octylphthalate ug/kg ND 326 10/08/19 11:38
Dibenz(a,h)anthracene ug/kg ND 326 10/08/19 11:38
Dibenzofuran ug/kg ND 326 10/08/19 11:38
Diethylphthalate ug/kg ND 326 10/08/19 11:38
Dimethylphthalate ug/kg ND 326 10/08/19 11:38
Fluoranthene ug/kg ND 326 10/08/19 11:38
Fluorene ug/kg ND 326 10/08/19 11:38
Hexachloro-1,3-butadiene ug/kg ND 326 10/08/19 11:38
Hexachlorobenzene ug/kg ND 326 10/08/19 11:38
Hexachlorocyclopentadiene ug/kg ND 326 10/08/19 11:38
Hexachloroethane ug/kg ND 326 10/08/19 11:38
Indeno(1,2,3-cd)pyrene ug/kg ND 326 10/08/19 11:38
Isophorone ug/kg ND 326 10/08/19 11:38
N-Nitroso-di-n-propylamine ug/kg ND 326 10/08/19 11:38
N-Nitrosodimethylamine ug/kg ND 326 10/08/19 11:38
N-Nitrosodiphenylamine ug/kg ND 326 10/08/19 11:38
Naphthalene ug/kg ND 326 10/08/19 11:38
Nitrobenzene ug/kg ND 326 10/08/19 11:38
Pentachlorophenol ug/kg ND 1630 10/08/19 11:38
Phenanthrene ug/kg ND 326 10/08/19 11:38
Phenol ug/kg ND 326 10/08/19 11:38
Pyrene ug/kg ND 326 10/08/19 11:38
Pyridine ug/kg ND 326 10/08/19 11:38
2,4,6-Tribromophenol (S)%82 27-110 10/08/19 11:38
2-Fluorobiphenyl (S)%71 30-110 10/08/19 11:38
2-Fluorophenol (S)%66 13-110 10/08/19 11:38
Nitrobenzene-d5 (S)%57 23-110 10/08/19 11:38
Phenol-d6 (S)%65 22-110 10/08/19 11:38
Terphenyl-d14 (S)%96 28-110 10/08/19 11:38
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2699596LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 12501670 75 52-130
1,2-Dichlorobenzene ug/kg 12501670 75 51-130
1,3-Dichlorobenzene ug/kg 12501670 75 50-130
1,4-Dichlorobenzene ug/kg 12401670 74 49-130
1-Methylnaphthalene ug/kg 13701670 82 55-130
2,2'-Oxybis(1-chloropropane)ug/kg 13101670 79 30-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/11/2019 05:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92447918
Alamance 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2699596LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,5-Trichlorophenol ug/kg 13001670 78 55-130
2,4,6-Trichlorophenol ug/kg 13601670 81 57-130
2,4-Dichlorophenol ug/kg 12801670 77 56-130
2,4-Dimethylphenol ug/kg 12901670 77 51-130
2,4-Dinitrophenol ug/kg 66408360 79 27-133
2,4-Dinitrotoluene ug/kg 11801670 70 61-130
2,6-Dinitrotoluene ug/kg 13401670 80 60-130
2-Chloronaphthalene ug/kg 12901670 77 52-130
2-Chlorophenol ug/kg 13401670 80 54-130
2-Methylnaphthalene ug/kg 14301670 86 54-130
2-Methylphenol(o-Cresol)ug/kg 13101670 78 51-130
2-Nitroaniline ug/kg 23803340 71 51-130
2-Nitrophenol ug/kg 14401670 86 49-130
3&4-Methylphenol(m&p Cresol)ug/kg 13301670 80 11-163
3,3'-Dichlorobenzidine ug/kg 25403340 76 10-132
3-Nitroaniline ug/kg 25603340 77 55-130
4,6-Dinitro-2-methylphenol ug/kg 33903340 101 47-142
4-Bromophenylphenyl ether ug/kg 16401670 98 59-130
4-Chloro-3-methylphenol ug/kg 24003340 72 55-130
4-Chloroaniline ug/kg 27703340 83 54-130
4-Chlorophenylphenyl ether ug/kg 12901670 77 58-130
4-Nitroaniline ug/kg 24703340 74 54-130
4-Nitrophenol ug/kg 42508360 51 48-130
Acenaphthene ug/kg 14001670 84 60-130
Acenaphthylene ug/kg 14301670 86 60-130
Aniline ug/kg 11501670 69 43-130
Anthracene ug/kg 16101670 96 63-130
Benzo(a)anthracene ug/kg 16501670 98 59-130
Benzo(a)pyrene ug/kg 16001670 96 57-130
Benzo(b)fluoranthene ug/kg 15401670 92 54-130
Benzo(g,h,i)perylene ug/kg 17201670 103 59-130
Benzo(k)fluoranthene ug/kg 16601670 99 54-130
Benzoic Acid ug/kg 41408360 50 19-130
Benzyl alcohol ug/kg 24403340 73 50-130
bis(2-Chloroethoxy)methane ug/kg 13801670 83 54-130
bis(2-Chloroethyl) ether ug/kg 13701670 82 48-130
bis(2-Ethylhexyl)phthalate ug/kg 16901670 101 45-134
Butylbenzylphthalate ug/kg 17001670 102 46-138
Chrysene ug/kg 16901670 101 58-130
Di-n-butylphthalate ug/kg 14701670 88 60-130
Di-n-octylphthalate ug/kg 16301670 97 53-130
Dibenz(a,h)anthracene ug/kg 17301670 103 59-130
Dibenzofuran ug/kg 12801670 76 60-130
Diethylphthalate ug/kg 12101670 73 60-130
Dimethylphthalate ug/kg 13501670 81 60-130
Fluoranthene ug/kg 14301670 86 65-130
Fluorene ug/kg 12801670 77 63-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/11/2019 05:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92447918
Alamance 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2699596LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachloro-1,3-butadiene ug/kg 11401670 68 46-130
Hexachlorobenzene ug/kg 14701670 88 58-130
Hexachlorocyclopentadiene ug/kg 12101670 73 23-130
Hexachloroethane ug/kg 11601670 70 47-130
Indeno(1,2,3-cd)pyrene ug/kg 16701670 100 60-130
Isophorone ug/kg 11301670 68 49-130
N-Nitroso-di-n-propylamine ug/kg 12401670 74 47-130
N-Nitrosodimethylamine ug/kg 13101670 78 45-130
N-Nitrosodiphenylamine ug/kg 17101670 103 59-130
Naphthalene ug/kg 14401670 86 55-130
Nitrobenzene ug/kg 10901670 65 49-130
Pentachlorophenol ug/kg 28803340 86 10-132
Phenanthrene ug/kg 16001670 96 62-130
Phenol ug/kg 13001670 78 46-130
Pyrene ug/kg 18601670 111 53-130
Pyridine ug/kg 10401670 62 37-130
2,4,6-Tribromophenol (S)%97 27-110
2-Fluorobiphenyl (S)%78 30-110
2-Fluorophenol (S)%75 13-110
Nitrobenzene-d5 (S)%66 23-110
Phenol-d6 (S)%73 22-110
Terphenyl-d14 (S)%102 28-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2699597MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92447918001
2699598
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/kg 1870 74 18-13072 11920ND1380 1370
1,2-Dichlorobenzene ug/kg 1870 73 14-13071 11920ND1370 1360
1,3-Dichlorobenzene ug/kg 1870 72 12-13070 11920ND1350 1340
1,4-Dichlorobenzene ug/kg 1870 72 10-13070 11920ND1350 1340
1-Methylnaphthalene ug/kg 1870 80 12-13077 11920ND1490 1480
2,2'-Oxybis(1-chloropropane) ug/kg 1870 76 10-13075 01920ND1430 1430
2,4,5-Trichlorophenol ug/kg 1870 77 13-13072 41920ND1430 1380
2,4,6-Trichlorophenol ug/kg 1870 80 17-13071 91920ND1500 1370
2,4-Dichlorophenol ug/kg 1870 78 10-13074 21920ND1450 1420
2,4-Dimethylphenol ug/kg 1870 76 10-13073 21920ND1420 1400
2,4-Dinitrophenol ug/kg R193507610-13052 349600ND7100 5030
2,4-Dinitrotoluene ug/kg 1870 72 24-13069 11920ND1350 1330
2,6-Dinitrotoluene ug/kg 1870 81 23-13078 11920ND1510 1490
2-Chloronaphthalene ug/kg 1870 76 19-13073 11920ND1420 1400
2-Chlorophenol ug/kg 1870 78 10-13074 21920ND1450 1430
2-Methylnaphthalene ug/kg 1870 83 18-13080 11920ND1560 1540
2-Methylphenol(o-Cresol)ug/kg 1870 74 10-13073 01920ND1390 1390
2-Nitroaniline ug/kg 3740 71 17-13070 13840ND2650 2670
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/11/2019 05:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92447918
Alamance 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2699597MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92447918001
2699598
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
2-Nitrophenol ug/kg 1870 86 10-13082 21920ND1610 1580
3&4-Methylphenol(m&p
Cresol)ug/kg 1870 75 10-13074 11920ND1410 1420
3,3'-Dichlorobenzidine ug/kg 3740 81 10-13080 13840ND3040 3060
3-Nitroaniline ug/kg 3740 79 24-13077 03840ND2960 2970
4,6-Dinitro-2-methylphenol ug/kg 3740 101 10-15282 183840ND3780 3160
4-Bromophenylphenyl ether ug/kg 1870 96 29-13093 11920ND1790 1780
4-Chloro-3-methylphenol ug/kg 3740 70 17-13069 13840ND2620 2640
4-Chloroaniline ug/kg 3740 82 14-13080 03840ND3050 3060
4-Chlorophenylphenyl ether ug/kg 1870 74 25-13072 01920ND1390 1380
4-Nitroaniline ug/kg 3740 75 22-13073 13840ND2790 2810
4-Nitrophenol ug/kg 9350 50 10-13043 149600ND4690 4100
Acenaphthene ug/kg 1870 81 20-13079 01920ND1520 1520
Acenaphthylene ug/kg 1870 84 25-13082 01920ND1570 1570
Aniline ug/kg 1870 66 10-13065 11920ND1240 1250
Anthracene ug/kg 1870 94 29-13092 01920ND1770 1770
Benzo(a)anthracene ug/kg 1870 95 19-13090 21920ND1780 1730
Benzo(a)pyrene ug/kg 1870 91 12-13088 21920ND1710 1680
Benzo(b)fluoranthene ug/kg 1870 87 14-13083 21920ND1630 1600
Benzo(g,h,i)perylene ug/kg 1870 95 10-13091 21920ND1770 1740
Benzo(k)fluoranthene ug/kg 1870 93 14-13090 01920ND1740 1730
Benzoic Acid ug/kg 9350 27 10-130169600ND2560 1500J
Benzyl alcohol ug/kg 3740 69 13-13067 03840ND2580 2570
bis(2-Chloroethoxy)methane ug/kg 1870 81 16-13078 21920ND1520 1490
bis(2-Chloroethyl) ether ug/kg 1870 80 11-13078 01920ND1500 1510
bis(2-Ethylhexyl)phthalate ug/kg 1870 95 21-13090 31920ND1780 1730
Butylbenzylphthalate ug/kg 1870 96 23-13092 21920ND1800 1770
Chrysene ug/kg 1870 99 22-13093 41920ND1850 1790
Di-n-butylphthalate ug/kg 1870 84 30-13082 11920ND1580 1570
Di-n-octylphthalate ug/kg 1870 94 23-14288 41920ND1760 1680
Dibenz(a,h)anthracene ug/kg 1870 97 10-13092 31920ND1820 1770
Dibenzofuran ug/kg 1870 75 24-13073 01920ND1410 1400
Diethylphthalate ug/kg 1870 73 26-13071 01920ND1360 1350
Dimethylphthalate ug/kg 1870 82 22-13079 11920ND1530 1520
Fluoranthene ug/kg 1870 85 33-13081 21920ND1580 1560
Fluorene ug/kg 1870 74 22-13073 11920ND1390 1390
Hexachloro-1,3-butadiene ug/kg 1870 67 13-13064 21920ND1250 1230
Hexachlorobenzene ug/kg 1870 84 29-13082 01920ND1580 1570
Hexachlorocyclopentadiene ug/kg 1870 72 10-13068 41920ND1350 1300
Hexachloroethane ug/kg 1870 68 10-13065 21920ND1280 1250
Indeno(1,2,3-cd)pyrene ug/kg 1870 93 10-13088 31920ND1740 1690
Isophorone ug/kg 1870 66 13-13064 11920ND1240 1230
N-Nitroso-di-n-propylamine ug/kg 1870 71 12-13070 11920ND1320 1340
N-Nitrosodimethylamine ug/kg 1870 74 11-13070 21920ND1380 1350
N-Nitrosodiphenylamine ug/kg 1870 104 15-130101 01920ND1940 1940
Naphthalene ug/kg 1870 84 15-13082 01920ND1570 1580
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/11/2019 05:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92447918
Alamance 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2699597MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92447918001
2699598
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrobenzene ug/kg 1870 65 12-13063 01920ND1210 1210
Pentachlorophenol ug/kg 3740 81 10-13064 203840ND3010 2460
Phenanthrene ug/kg 1870 94 27-13091 01920ND1760 1750
Phenol ug/kg 1870 73 10-13071 01920ND1370 1370
Pyrene ug/kg 1870 104 19-130100 11920ND1940 1910
Pyridine ug/kg 1870 43 10-13045 81920ND802 867
2,4,6-Tribromophenol (S)%97 27-11092
2-Fluorobiphenyl (S)%75 30-11075
2-Fluorophenol (S)%71 13-11071
Nitrobenzene-d5 (S)%65 23-11066
Phenol-d6 (S)%68 22-11069
Terphenyl-d14 (S)%93 28-11093
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/11/2019 05:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92447918
Alamance 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
501379
MADEP EPH
MADEP EPH
MADEP EPH NC Soil
Associated Lab Samples: 92447918001, 92447918002, 92447918003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2696480
Associated Lab Samples:92447918001, 92447918002, 92447918003
Matrix: Solid
Analyzed
Aliphatic (C09-C18)mg/kg ND 10.0 N210/03/19 16:14
Aliphatic (C19-C36)mg/kg ND 10.0 N210/03/19 16:14
Aromatic (C11-C22)mg/kg ND 10.0 N210/03/19 16:14
2-Bromonaphthalene (S)%103 40-140 10/03/19 16:14
2-Fluorobiphenyl (S)%104 40-140 10/03/19 16:14
Nonatriacontane (S)%73 40-140 10/03/19 16:14
o-Terphenyl (S)%82 40-140 10/03/19 16:14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2696481LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2696482
Aliphatic (C09-C18)mg/kg ND N2104940-14052ND 50
Aliphatic (C19-C36)mg/kg ND N213.3 65 40-14066ND 50
Aromatic (C11-C22)mg/kg 22.5 N228.3 79 40-1407421.0 7 50
2-Bromonaphthalene (S)%105 40-14085
2-Fluorobiphenyl (S)%105 40-14088
Nonatriacontane (S)%67 40-14063
o-Terphenyl (S)%88 40-14083
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/11/2019 05:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 46
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92447918
Alamance 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
501297
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples: 92447918001, 92447918002, 92447918003
Parameter Units
Dup
Result QualifiersRPDResult
92447591001
2696194SAMPLE DUPLICATE:
Percent Moisture %22.5 323.3
Parameter Units
Dup
Result QualifiersRPDResult
92447918003
2696195SAMPLE DUPLICATE:
Percent Moisture %14.5 1116.1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/11/2019 05:06 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 46
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92447918
Alamance 2019-210
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.IK
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
RPD value was outside control limits.R1
Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample
re-analysis).S2
Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample.S3
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in theassociated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/11/2019 05:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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Page 44 of 46
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92447918
Alamance 2019-210
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92447918001 501379 501703B-1 3-5 MADEP EPH MADEP EPH
92447918002 501379 501703B-1 8-10 MADEP EPH MADEP EPH
92447918003 501379 501703B-1 10-13 MADEP EPH MADEP EPH
92447918001 501510 501599B-1 3-5 MADEP VPH MADEP VPH
92447918002 501510 501599B-1 8-10 MADEP VPH MADEP VPH
92447918003 501510 501599B-1 10-13 MADEP VPH MADEP VPH
92447918001 502058 502333B-1 3-5 EPA 3546 EPA 8270D
92447918002 502058 502333B-1 8-10 EPA 3546 EPA 8270D
92447918003 502058 502333B-1 10-13 EPA 3546 EPA 8270D
92447918001 501852 501857B-1 3-5 EPA 5035A EPA 8260D
92447918002 502304 502318B-1 8-10 EPA 5035A EPA 8260D
92447918003 502890 502913B-1 10-13 EPA 5035A EPA 8260D
92447918001 501297B-1 3-5 ASTM D2974-87
92447918002 501297B-1 8-10 ASTM D2974-87
92447918003 501297B-1 10-13 ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/11/2019 05:06 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 45 of 46
Page 46 of 46

APPENDIX   G 

#=CL#
October 16, 2019
LIMS USE: FR - MIKE JONES
LIMS OBJECT ID: 92448122
92448122
Project:
Pace Project No.:
RE:
Mr. Mike Jones
Pyramid Environmental
P.O. Box 16265
503 Industrial Avenue
Greensboro, NC 27416
Alamance Oil 2019-210
Dear Mr. Jones:
Enclosed are the analytical results for sample(s) received by the laboratory on October 03, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
Due to a laboratory error, the 625 fraction of the project is unable to be reported. Per client request,
all other analytical results have been reported.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Amanda Payne
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
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[phone]
Page 1 of 19
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92448122
Alamance Oil 2019-210
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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Huntersville, NC 28078
[phone]
Page 2 of 19
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92448122
Alamance Oil 2019-210
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92448122001 MW-1 EPA 504.1 4 PASI-CBAJ
MADEP EPH 7 PASI-CSEM
MADEP VPH 6 PASI-CLMB
EPA 6010D 1 PASI-ASH1
SM 6200B 69 PASI-CGAW
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Huntersville, NC 28078
[phone]
Page 3 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92448122
Alamance Oil 2019-210
Sample: MW-1 Lab ID: 92448122001 Collected: 10/02/19 13:00 Received: 10/03/19 09:13 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 504.1 Preparation Method: EPA 504.1504 GCS EDB and DBCP
1,2-Dibromo-3-chloropropane ND ug/L 10/08/19 18:39 96-12-810/08/19 09:090.047 1
1,2-Dibromoethane (EDB)ND ug/L 10/08/19 18:39 106-93-410/08/19 09:090.019 1
1,2,3-Trichloropropane ND ug/L 10/08/19 18:39 96-18-410/08/19 09:090.047 1
Surrogates
1-Chloro-2-bromopropane (S)103 %10/08/19 18:39 301-79-5610/08/19 09:0970-130 1
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Water
Aliphatic (C09-C18)ND ug/L 10/07/19 15:43 N210/05/19 10:5396.2 1
Aliphatic (C19-C36)ND ug/L 10/07/19 15:43 N210/05/19 10:5396.2 1
Aromatic (C11-C22)535 ug/L 10/07/19 15:43 N210/05/19 10:5396.2 1
Surrogates
Nonatriacontane (S)67 %10/07/19 15:43 7194-86-710/05/19 10:5340-140 1
o-Terphenyl (S)79 %10/07/19 15:43 84-15-110/05/19 10:5340-140 1
2-Fluorobiphenyl (S)90 %10/07/19 15:43 321-60-810/05/19 10:5340-140 1
2-Bromonaphthalene (S)94 %10/07/19 15:43 580-13-210/05/19 10:5340-140 1
Analytical Method: MADEP VPHVPH NC Water
Aliphatic (C05-C08)125000 ug/L 10/04/19 17:07 N22500 50
Aliphatic (C09-C12)24600 ug/L 10/04/19 17:07 N22500 50
Aliphatic(C09-C12) Adjusted 15700 ug/L 10/04/19 17:07 N22500 50
Aromatic (C09-C10)8910 ug/L 10/04/19 17:07 N22500 50
Surrogates
4-Bromofluorobenzene (FID) (S)88 %10/04/19 17:07 460-00-470-130 50
4-Bromofluorobenzene (PID) (S)92 %10/04/19 17:07 460-00-470-130 50
Analytical Method: EPA 6010D Preparation Method: EPA 3010A6010 MET ICP
Lead ND ug/L 10/10/19 19:21 7439-92-110/08/19 23:455.0 1
Analytical Method: SM 6200B6200B MSV
tert-Amyl Alcohol 89900 ug/L 10/14/19 22:51 75-85-420000 200
tert-Amylmethyl ether ND ug/L 10/14/19 22:51 994-05-82000 200
Benzene 17100 ug/L 10/14/19 22:51 71-43-2100 200
Bromobenzene ND ug/L 10/14/19 22:51 108-86-1100 200
Bromochloromethane ND ug/L 10/14/19 22:51 74-97-5100 200
Bromodichloromethane ND ug/L 10/14/19 22:51 75-27-4100 200
Bromoform ND ug/L 10/14/19 22:51 75-25-2100 200
Bromomethane ND ug/L 10/14/19 22:51 74-83-91000 200
tert-Butyl Alcohol 6260 ug/L 10/14/19 22:51 75-65-02000 200
n-Butylbenzene ND ug/L 10/14/19 22:51 104-51-8100 200
sec-Butylbenzene ND ug/L 10/14/19 22:51 135-98-8100 200
tert-Butylbenzene ND ug/L 10/14/19 22:51 98-06-6100 200
tert-Butyl Formate ND ug/L 10/14/19 22:51 762-75-4 L14000 200
Carbon tetrachloride ND ug/L 10/14/19 22:51 56-23-5100 200
Chlorobenzene ND ug/L 10/14/19 22:51 108-90-7100 200
Chloroethane ND ug/L 10/14/19 22:51 75-00-3200 200
Chloroform ND ug/L 10/14/19 22:51 67-66-31000 200
REPORT OF LABORATORY ANALYSIS
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Page 4 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92448122
Alamance Oil 2019-210
Sample: MW-1 Lab ID: 92448122001 Collected: 10/02/19 13:00 Received: 10/03/19 09:13 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B6200B MSV
Chloromethane ND ug/L 10/14/19 22:51 74-87-3200 200
2-Chlorotoluene ND ug/L 10/14/19 22:51 95-49-8100 200
4-Chlorotoluene ND ug/L 10/14/19 22:51 106-43-4100 200
1,2-Dibromo-3-chloropropane ND ug/L 10/14/19 22:51 96-12-8200 200
Dibromochloromethane ND ug/L 10/14/19 22:51 124-48-1100 200
1,2-Dibromoethane (EDB)ND ug/L 10/14/19 22:51 106-93-4100 200
Dibromomethane ND ug/L 10/14/19 22:51 74-95-3100 200
1,2-Dichlorobenzene ND ug/L 10/14/19 22:51 95-50-1100 200
1,3-Dichlorobenzene ND ug/L 10/14/19 22:51 541-73-1100 200
1,4-Dichlorobenzene ND ug/L 10/14/19 22:51 106-46-7100 200
Dichlorodifluoromethane ND ug/L 10/14/19 22:51 75-71-8100 200
1,1-Dichloroethane ND ug/L 10/14/19 22:51 75-34-3100 200
1,2-Dichloroethane ND ug/L 10/14/19 22:51 107-06-2100 200
1,1-Dichloroethene ND ug/L 10/14/19 22:51 75-35-4100 200
cis-1,2-Dichloroethene ND ug/L 10/14/19 22:51 156-59-2100 200
trans-1,2-Dichloroethene ND ug/L 10/14/19 22:51 156-60-5100 200
1,2-Dichloropropane ND ug/L 10/14/19 22:51 78-87-5100 200
1,3-Dichloropropane ND ug/L 10/14/19 22:51 142-28-9100 200
2,2-Dichloropropane ND ug/L 10/14/19 22:51 594-20-7100 200
1,1-Dichloropropene ND ug/L 10/14/19 22:51 563-58-6100 200
cis-1,3-Dichloropropene ND ug/L 10/14/19 22:51 10061-01-5100 200
trans-1,3-Dichloropropene ND ug/L 10/14/19 22:51 10061-02-6100 200
Diisopropyl ether 5730 ug/L 10/14/19 22:51 108-20-3100 200
Ethanol ND ug/L 10/14/19 22:51 64-17-540000 200
Ethylbenzene 1930 ug/L 10/14/19 22:51 100-41-4100 200
Ethyl-tert-butyl ether ND ug/L 10/14/19 22:51 637-92-32000 200
Hexachloro-1,3-butadiene ND ug/L 10/14/19 22:51 87-68-3400 200
Isopropylbenzene (Cumene)ND ug/L 10/14/19 22:51 98-82-8100 200
Methylene Chloride ND ug/L 10/14/19 22:51 75-09-2400 200
Methyl-tert-butyl ether 17100 ug/L 10/14/19 22:51 1634-04-4100 200
Naphthalene 577 ug/L 10/14/19 22:51 91-20-3400 200
n-Propylbenzene ND ug/L 10/14/19 22:51 103-65-1100 200
Styrene 107 ug/L 10/14/19 22:51 100-42-5100 200
1,1,1,2-Tetrachloroethane ND ug/L 10/14/19 22:51 630-20-6100 200
1,1,2,2-Tetrachloroethane ND ug/L 10/14/19 22:51 79-34-5100 200
Tetrachloroethene ND ug/L 10/14/19 22:51 127-18-4100 200
Toluene 26600 ug/L 10/14/19 22:51 108-88-3100 200
1,2,3-Trichlorobenzene ND ug/L 10/14/19 22:51 87-61-6400 200
1,2,4-Trichlorobenzene ND ug/L 10/14/19 22:51 120-82-1400 200
1,1,1-Trichloroethane ND ug/L 10/14/19 22:51 71-55-6100 200
1,1,2-Trichloroethane ND ug/L 10/14/19 22:51 79-00-5100 200
Trichloroethene ND ug/L 10/14/19 22:51 79-01-6100 200
Trichlorofluoromethane ND ug/L 10/14/19 22:51 75-69-4200 200
1,2,3-Trichloropropane ND ug/L 10/14/19 22:51 96-18-4100 200
1,2,4-Trimethylbenzene 1130 ug/L 10/14/19 22:51 95-63-6100 200
1,3,5-Trimethylbenzene ND ug/L 10/14/19 22:51 108-67-8100 200
Vinyl chloride ND ug/L 10/14/19 22:51 75-01-4200 200
REPORT OF LABORATORY ANALYSIS
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Page 5 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92448122
Alamance Oil 2019-210
Sample: MW-1 Lab ID: 92448122001 Collected: 10/02/19 13:00 Received: 10/03/19 09:13 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B6200B MSV
m&p-Xylene 5650 ug/L 10/14/19 22:51 179601-23-1200 200
o-Xylene 2830 ug/L 10/14/19 22:51 95-47-6100 200
Surrogates
1,2-Dichloroethane-d4 (S)103 %10/14/19 22:51 17060-07-070-130 200
4-Bromofluorobenzene (S)98 %10/14/19 22:51 460-00-470-130 200
Toluene-d8 (S)101 %10/14/19 22:51 2037-26-570-130 200
REPORT OF LABORATORY ANALYSIS
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Page 6 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92448122
Alamance Oil 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
501820
MADEP VPH
MADEP VPH
VPH NC Water
Associated Lab Samples: 92448122001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2698512
Associated Lab Samples:92448122001
Matrix: Water
Analyzed
Aliphatic (C05-C08)ug/L ND 50.0 N210/04/19 14:39
Aliphatic (C09-C12)ug/L ND 50.0 N210/04/19 14:39
Aromatic (C09-C10)ug/L ND 50.0 N210/04/19 14:39
4-Bromofluorobenzene (FID) (S)%88 70-130 10/04/19 14:39
4-Bromofluorobenzene (PID) (S)%92 70-130 10/04/19 14:39
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2698513LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2698514
Aliphatic (C05-C08)ug/L 318 N230010670-130107321 1 25
Aliphatic (C09-C12)ug/L 315 N230010530-130107322 2 25
Aromatic (C09-C10)ug/L 103 N210010370-130104104 1 25
4-Bromofluorobenzene (FID) (S)%98 70-13098
4-Bromofluorobenzene (PID) (S)%101 70-130100
REPORT OF LABORATORY ANALYSIS
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Page 7 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92448122
Alamance Oil 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
502441
EPA 3010A
EPA 6010D
6010 MET
Associated Lab Samples: 92448122001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2701189
Associated Lab Samples:92448122001
Matrix: Water
Analyzed
Lead ug/L ND 5.0 10/10/19 18:03
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2701190LABORATORY CONTROL SAMPLE:
LCSSpike
Lead ug/L 483500 97 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2701191MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92448261001
2701192
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Lead ug/L 500 89 75-12589 050029.9 477 475
REPORT OF LABORATORY ANALYSIS
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Page 8 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92448122
Alamance Oil 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
503388
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples: 92448122001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2705775
Associated Lab Samples:92448122001
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 10/14/19 17:47
1,1,1-Trichloroethane ug/L ND 0.50 10/14/19 17:47
1,1,2,2-Tetrachloroethane ug/L ND 0.50 10/14/19 17:47
1,1,2-Trichloroethane ug/L ND 0.50 10/14/19 17:47
1,1-Dichloroethane ug/L ND 0.50 10/14/19 17:47
1,1-Dichloroethene ug/L ND 0.50 10/14/19 17:47
1,1-Dichloropropene ug/L ND 0.50 10/14/19 17:47
1,2,3-Trichlorobenzene ug/L ND 2.0 10/14/19 17:47
1,2,3-Trichloropropane ug/L ND 0.50 10/14/19 17:47
1,2,4-Trichlorobenzene ug/L ND 2.0 10/14/19 17:47
1,2,4-Trimethylbenzene ug/L ND 0.50 10/14/19 17:47
1,2-Dibromo-3-chloropropane ug/L ND 1.0 10/14/19 17:47
1,2-Dibromoethane (EDB)ug/L ND 0.50 10/14/19 17:47
1,2-Dichlorobenzene ug/L ND 0.50 10/14/19 17:47
1,2-Dichloroethane ug/L ND 0.50 10/14/19 17:47
1,2-Dichloropropane ug/L ND 0.50 10/14/19 17:47
1,3,5-Trimethylbenzene ug/L ND 0.50 10/14/19 17:47
1,3-Dichlorobenzene ug/L ND 0.50 10/14/19 17:47
1,3-Dichloropropane ug/L ND 0.50 10/14/19 17:47
1,4-Dichlorobenzene ug/L ND 0.50 10/14/19 17:47
2,2-Dichloropropane ug/L ND 0.50 10/14/19 17:47
2-Chlorotoluene ug/L ND 0.50 10/14/19 17:47
4-Chlorotoluene ug/L ND 0.50 10/14/19 17:47
Benzene ug/L ND 0.50 10/14/19 17:47
Bromobenzene ug/L ND 0.50 10/14/19 17:47
Bromochloromethane ug/L ND 0.50 10/14/19 17:47
Bromodichloromethane ug/L ND 0.50 10/14/19 17:47
Bromoform ug/L ND 0.50 10/14/19 17:47
Bromomethane ug/L ND 5.0 10/14/19 17:47
Carbon tetrachloride ug/L ND 0.50 10/14/19 17:47
Chlorobenzene ug/L ND 0.50 10/14/19 17:47
Chloroethane ug/L ND 1.0 10/14/19 17:47
Chloroform ug/L ND 5.0 10/14/19 17:47
Chloromethane ug/L ND 1.0 10/14/19 17:47
cis-1,2-Dichloroethene ug/L ND 0.50 10/14/19 17:47
cis-1,3-Dichloropropene ug/L ND 0.50 10/14/19 17:47
Dibromochloromethane ug/L ND 0.50 10/14/19 17:47
Dibromomethane ug/L ND 0.50 10/14/19 17:47
Dichlorodifluoromethane ug/L ND 0.50 10/14/19 17:47
Diisopropyl ether ug/L ND 0.50 10/14/19 17:47
Ethanol ug/L ND 200 10/14/19 17:47
REPORT OF LABORATORY ANALYSIS
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Page 9 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92448122
Alamance Oil 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2705775
Associated Lab Samples:92448122001
Matrix: Water
Analyzed
Ethyl-tert-butyl ether ug/L ND 10.0 10/14/19 17:47
Ethylbenzene ug/L ND 0.50 10/14/19 17:47
Hexachloro-1,3-butadiene ug/L ND 2.0 10/14/19 17:47
Isopropylbenzene (Cumene)ug/L ND 0.50 10/14/19 17:47
m&p-Xylene ug/L ND 1.0 10/14/19 17:47
Methyl-tert-butyl ether ug/L ND 0.50 10/14/19 17:47
Methylene Chloride ug/L ND 2.0 10/14/19 17:47
n-Butylbenzene ug/L ND 0.50 10/14/19 17:47
n-Propylbenzene ug/L ND 0.50 10/14/19 17:47
Naphthalene ug/L ND 2.0 10/14/19 17:47
o-Xylene ug/L ND 0.50 10/14/19 17:47
sec-Butylbenzene ug/L ND 0.50 10/14/19 17:47
Styrene ug/L ND 0.50 10/14/19 17:47
tert-Amyl Alcohol ug/L ND 100 10/14/19 17:47
tert-Amylmethyl ether ug/L ND 10.0 10/14/19 17:47
tert-Butyl Alcohol ug/L ND 10.0 10/14/19 17:47
tert-Butyl Formate ug/L ND 20.0 10/14/19 17:47
tert-Butylbenzene ug/L ND 0.50 10/14/19 17:47
Tetrachloroethene ug/L ND 0.50 10/14/19 17:47
Toluene ug/L ND 0.50 10/14/19 17:47
trans-1,2-Dichloroethene ug/L ND 0.50 10/14/19 17:47
trans-1,3-Dichloropropene ug/L ND 0.50 10/14/19 17:47
Trichloroethene ug/L ND 0.50 10/14/19 17:47
Trichlorofluoromethane ug/L ND 1.0 10/14/19 17:47
Vinyl chloride ug/L ND 1.0 10/14/19 17:47
1,2-Dichloroethane-d4 (S)%100 70-130 10/14/19 17:47
4-Bromofluorobenzene (S)%97 70-130 10/14/19 17:47
Toluene-d8 (S)%100 70-130 10/14/19 17:47
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2705776LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 54.550 109 60-140
1,1,1-Trichloroethane ug/L 59.250 118 60-140
1,1,2,2-Tetrachloroethane ug/L 51.650 103 60-140
1,1,2-Trichloroethane ug/L 57.250 114 60-140
1,1-Dichloroethane ug/L 57.750 115 60-140
1,1-Dichloroethene ug/L 58.650 117 60-140
1,1-Dichloropropene ug/L 59.650 119 60-140
1,2,3-Trichlorobenzene ug/L 53.350 107 60-140
1,2,3-Trichloropropane ug/L 52.550 105 60-140
1,2,4-Trichlorobenzene ug/L 51.350 103 60-140
1,2,4-Trimethylbenzene ug/L 52.050 104 60-140
1,2-Dibromo-3-chloropropane ug/L 53.050 106 60-140
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/16/2019 05:04 PM
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Page 10 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92448122
Alamance Oil 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2705776LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromoethane (EDB)ug/L 56.050 112 60-140
1,2-Dichlorobenzene ug/L 52.350 105 60-140
1,2-Dichloroethane ug/L 54.250 108 60-140
1,2-Dichloropropane ug/L 55.350 111 60-140
1,3,5-Trimethylbenzene ug/L 52.950 106 60-140
1,3-Dichlorobenzene ug/L 51.650 103 60-140
1,3-Dichloropropane ug/L 55.150 110 60-140
1,4-Dichlorobenzene ug/L 51.250 102 60-140
2,2-Dichloropropane ug/L 64.050 128 60-140
2-Chlorotoluene ug/L 51.950 104 60-140
4-Chlorotoluene ug/L 51.150 102 60-140
Benzene ug/L 55.350 111 60-140
Bromobenzene ug/L 51.850 104 60-140
Bromochloromethane ug/L 58.850 118 60-140
Bromodichloromethane ug/L 58.850 118 60-140
Bromoform ug/L 55.950 112 60-140
Bromomethane ug/L 51.250 102 60-140
Carbon tetrachloride ug/L 56.550 113 60-140
Chlorobenzene ug/L 52.150 104 60-140
Chloroethane ug/L 50.050 100 60-140
Chloroform ug/L 57.250 114 60-140
Chloromethane ug/L 46.150 92 60-140
cis-1,2-Dichloroethene ug/L 57.750 115 60-140
cis-1,3-Dichloropropene ug/L 60.650 121 60-140
Dibromochloromethane ug/L 55.150 110 60-140
Dibromomethane ug/L 58.050 116 60-140
Dichlorodifluoromethane ug/L 60.650 121 60-140
Diisopropyl ether ug/L 56.950 114 60-140
Ethanol ug/L 18602000 93 60-140
Ethyl-tert-butyl ether ug/L 114100 114 60-140
Ethylbenzene ug/L 53.350 107 60-140
Hexachloro-1,3-butadiene ug/L 52.250 104 60-140
Isopropylbenzene (Cumene)ug/L 54.050 108 60-140
m&p-Xylene ug/L 107100 107 60-140
Methyl-tert-butyl ether ug/L 62.450 125 60-140
Methylene Chloride ug/L 55.250 110 60-140
n-Butylbenzene ug/L 52.750 105 60-140
n-Propylbenzene ug/L 52.050 104 60-140
Naphthalene ug/L 52.350 105 60-140
o-Xylene ug/L 55.150 110 60-140
sec-Butylbenzene ug/L 54.250 108 60-140
Styrene ug/L 53.750 107 60-140
tert-Amyl Alcohol ug/L 11501000 115 60-140
tert-Amylmethyl ether ug/L 115100 115 60-140
tert-Butyl Alcohol ug/L 592500 118 60-140
tert-Butyl Formate ug/L 611 L1400153 60-140
tert-Butylbenzene ug/L 46.450 93 60-140
REPORT OF LABORATORY ANALYSIS
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Page 11 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92448122
Alamance Oil 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2705776LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/L 55.150 110 60-140
Toluene ug/L 53.950 108 60-140
trans-1,2-Dichloroethene ug/L 57.850 116 60-140
trans-1,3-Dichloropropene ug/L 58.850 118 60-140
Trichloroethene ug/L 57.450 115 60-140
Trichlorofluoromethane ug/L 59.550 119 60-140
Vinyl chloride ug/L 58.350 117 60-140
1,2-Dichloroethane-d4 (S)%107 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2705777MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92447981003
2705778
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 2000 109 60-140112 32000ND2180 2250
1,1,1-Trichloroethane ug/L 2000 115 60-140122 62000ND2300 2440
1,1,2,2-Tetrachloroethane ug/L 2000 103 60-140108 52000ND2060 2160
1,1,2-Trichloroethane ug/L 2000 112 60-140116 42000ND2230 2320
1,1-Dichloroethane ug/L 2000 114 60-140116 22000ND2290 2330
1,1-Dichloroethene ug/L 2000 117 60-140120 32000ND2330 2400
1,1-Dichloropropene ug/L 2000 117 60-140119 22000ND2340 2380
1,2,3-Trichlorobenzene ug/L 2000 97 60-140104 72000ND1940 2080
1,2,3-Trichloropropane ug/L 2000 103 60-140105 22000ND2060 2100
1,2,4-Trichlorobenzene ug/L 2000 95 60-140104 92000ND1900 2080
1,2,4-Trimethylbenzene ug/L 2000 126 60-140132 52000ND2520 2650
1,2-Dibromo-3-chloropropane ug/L 2000 101 60-140108 62000ND2030 2160
1,2-Dibromoethane (EDB)ug/L 2000 106 60-140110 42000ND2120 2200
1,2-Dichlorobenzene ug/L 2000 103 60-140109 62000ND2060 2190
1,2-Dichloroethane ug/L 2000 104 60-140109 52000ND2090 2180
1,2-Dichloropropane ug/L 2000 109 60-140113 42000ND2180 2260
1,3,5-Trimethylbenzene ug/L 2000 112 60-140118 52000ND2250 2360
1,3-Dichlorobenzene ug/L 2000 102 60-140107 52000ND2030 2140
1,3-Dichloropropane ug/L 2000 107 60-140110 32000ND2130 2190
1,4-Dichlorobenzene ug/L 2000 101 60-140107 62000ND2020 2140
2,2-Dichloropropane ug/L 2000 117 60-140121 32000ND2340 2420
2-Chlorotoluene ug/L 2000 106 60-140107 22000ND2110 2150
4-Chlorotoluene ug/L 2000 103 60-140108 52000ND2050 2170
Benzene ug/L M1200056160-140563 02000ND11200 11300
Bromobenzene ug/L 2000 105 60-140110 52000ND2090 2190
Bromochloromethane ug/L 2000 112 60-140113 12000ND2250 2260
Bromodichloromethane ug/L 2000 117 60-140122 52000ND2330 2450
Bromoform ug/L 2000 109 60-140113 42000ND2180 2270
Bromomethane ug/L 2000 68 60-14082 182000ND1370 1630
Carbon tetrachloride ug/L 2000 118 60-140122 32000ND2370 2430
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92448122
Alamance Oil 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2705777MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92447981003
2705778
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Chlorobenzene ug/L 2000 106 60-140110 42000ND2120 2200
Chloroethane ug/L 2000 110 60-140115 42000ND2210 2310
Chloroform ug/L 2000 111 60-140112 12000ND2220 2230
Chloromethane ug/L 2000 90 60-14096 62000ND1800 1920
cis-1,2-Dichloroethene ug/L 2000 111 60-140114 32000ND2220 2280
cis-1,3-Dichloropropene ug/L 2000 118 60-140122 42000ND2360 2450
Dibromochloromethane ug/L 2000 109 60-140113 42000ND2170 2270
Dibromomethane ug/L 2000 111 60-140116 42000ND2230 2320
Dichlorodifluoromethane ug/L 2000 111 60-140110 12000ND2220 2200
Diisopropyl ether ug/L M1200018960-140195 32000ND3790 3910
Ethanol ug/L 80000 92 60-14095 380000ND73400 76000
Ethyl-tert-butyl ether ug/L 4000 103 60-140110 74000ND4100 4390
Ethylbenzene ug/L M1200014960-140152 22000ND2980 3030
Hexachloro-1,3-butadiene ug/L 2000 102 60-140108 62000ND2030 2150
Isopropylbenzene (Cumene) ug/L 2000 111 60-140116 42000ND2210 2310
m&p-Xylene ug/L M1400018660-140188 14000ND7460 7510
Methyl-tert-butyl ether ug/L 2000 113 60-140119 52000ND2260 2380
Methylene Chloride ug/L 2000 104 60-140108 42000ND2090 2170
n-Butylbenzene ug/L 2000 100 60-140109 92000ND2010 2190
n-Propylbenzene ug/L 2000 107 60-140112 52000ND2130 2250
Naphthalene ug/L 2000 103 60-140110 72000ND2060 2200
o-Xylene ug/L M1200014760-140149 12000ND2940 2970
sec-Butylbenzene ug/L 2000 109 60-140115 62000ND2170 2300
Styrene ug/L 2000 109 60-140112 32000ND2180 2240
tert-Amyl Alcohol ug/L M14000021360-140220 340000ND85300 87900
tert-Amylmethyl ether ug/L 4000 106 60-140114 84000ND4230 4570
tert-Butyl Alcohol ug/L 20000 108 60-140120 1020000ND21600 24000
tert-Butyl Formate ug/L 16000 128 60-140135 616000ND20500 21700
tert-Butylbenzene ug/L 2000 93 60-14099 72000ND1850 1980
Tetrachloroethene ug/L 2000 110 60-140113 32000ND2200 2260
Toluene ug/L M1200043160-140427 12000ND8620 8550
trans-1,2-Dichloroethene ug/L 2000 112 60-140118 52000ND2240 2350
trans-1,3-Dichloropropene ug/L 2000 113 60-140117 42000ND2260 2350
Trichloroethene ug/L 2000 118 60-140120 22000ND2360 2400
Trichlorofluoromethane ug/L 2000 122 60-140124 22000ND2430 2480
Vinyl chloride ug/L 2000 118 60-140119 12000ND2350 2390
1,2-Dichloroethane-d4 (S)%100 70-130102
4-Bromofluorobenzene (S)%101 70-130101
Toluene-d8 (S)%99 70-130100
REPORT OF LABORATORY ANALYSIS
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Page 13 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92448122
Alamance Oil 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
502244
EPA 504.1
EPA 504.1
GCS 504 EDB DBCP
Associated Lab Samples: 92448122001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2700271
Associated Lab Samples:92448122001
Matrix: Water
Analyzed
1,2,3-Trichloropropane ug/L ND 0.050 10/08/19 13:41
1,2-Dibromo-3-chloropropane ug/L ND 0.050 10/08/19 13:41
1,2-Dibromoethane (EDB)ug/L ND 0.020 10/08/19 13:41
1-Chloro-2-bromopropane (S)%99 70-130 10/08/19 13:41
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2700272LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2700273
1,2,3-Trichloropropane ug/L 0.290.25 116 70-1301100.28 5 20
1,2-Dibromo-3-chloropropane ug/L 0.210.25 85 70-130860.22 1 20
1,2-Dibromoethane (EDB)ug/L 0.240.25 97 70-130950.24 2 20
1-Chloro-2-bromopropane (S)%105 70-130104
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2700275MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92447912002
2700276
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,2,3-Trichloropropane ug/L 0.25 105 65-135101 60.25ND 0.27 0.25
1,2-Dibromo-3-chloropropane ug/L 0.25 108 65-135105 40.25ND 0.27 0.26
1,2-Dibromoethane (EDB)ug/L 0.25 107 65-135102 70.25ND 0.27 0.25
1-Chloro-2-bromopropane (S) %109 70-130106
Parameter Units
Dup
Result QualifiersRPDResult
92447894003
2700274SAMPLE DUPLICATE:
1,2,3-Trichloropropane ug/L NDND
1,2-Dibromo-3-chloropropane ug/L NDND
1,2-Dibromoethane (EDB)ug/L NDND
1-Chloro-2-bromopropane (S)%114102
REPORT OF LABORATORY ANALYSIS
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Page 14 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92448122
Alamance Oil 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
501922
MADEP EPH
MADEP EPH
MADEP EPH NC Water
Associated Lab Samples: 92448122001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2699001
Associated Lab Samples:92448122001
Matrix: Water
Analyzed
Aliphatic (C09-C18)ug/L ND 100 N210/07/19 13:53
Aliphatic (C19-C36)ug/L ND 100 N210/07/19 13:53
Aromatic (C11-C22)ug/L ND 100 N210/07/19 13:53
2-Bromonaphthalene (S)%101 40-140 10/07/19 13:53
2-Fluorobiphenyl (S)%101 40-140 10/07/19 13:53
Nonatriacontane (S)%71 40-140 10/07/19 13:53
o-Terphenyl (S)%82 40-140 10/07/19 13:53
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2699002LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2699003
Aliphatic (C09-C18)ug/L 138 N23004640-14041124 11 50
Aliphatic (C19-C36)ug/L 234 N24005840-14065260 11 50
Aromatic (C11-C22)ug/L 595 N28507040-14086734 21 50
2-Bromonaphthalene (S)%98 40-14091
2-Fluorobiphenyl (S)%97 40-140107
Nonatriacontane (S)%60 40-14067
o-Terphenyl (S)%81 40-140101
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/16/2019 05:04 PM
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Page 15 of 19
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92448122
Alamance Oil 2019-210
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
REPORT OF LABORATORY ANALYSIS
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Page 16 of 19
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92448122
Alamance Oil 2019-210
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92448122001 502244 502315MW-1 EPA 504.1 EPA 504.1
92448122001 501922 502134MW-1 MADEP EPH MADEP EPH
92448122001 501820MW-1 MADEP VPH
92448122001 502441 502519MW-1 EPA 3010A EPA 6010D
92448122001 503388MW-1 SM 6200B
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/16/2019 05:04 PM
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Page 17 of 19
Page 18 of 19
Page 19 of 19
#=CL#
November 08, 2019
LIMS USE: FR - MIKE JONES
LIMS OBJECT ID: 92451374
92451374
Project:
Pace Project No.:
RE:
Mr. Mike Jones
Pyramid Environmental
P.O. Box 16265
503 Industrial Avenue
Greensboro, NC 27416
ALAMANCE OIL 2019-210
Dear Mr. Jones:
Enclosed are the analytical results for sample(s) received by the laboratory on October 29, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Amanda Payne
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 1 of 42
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92451374
ALAMANCE OIL 2019-210
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 2 of 42
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92451374
ALAMANCE OIL 2019-210
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92451374001 MW-1 EPA 625.1 57 PASI-CPKS
92451374002 MW-2 EPA 504.1 2 PASI-CBAJ
MADEP EPH 7 PASI-CBAJ
MADEP VPH 6 PASI-CLMB
EPA 6010D 1 PASI-ASH1
EPA 625.1 57 PASI-CPKS
SM 6200B 63 PASI-CCL
92451374003 MW-3 EPA 504.1 2 PASI-CBAJ
MADEP EPH 7 PASI-CBAJ
MADEP VPH 6 PASI-CLMB
EPA 6010D 1 PASI-ASH1
EPA 625.1 57 PASI-CPKS
SM 6200B 63 PASI-CCL
92451374004 MW-4 EPA 504.1 2 PASI-CBAJ
MADEP EPH 7 PASI-CBAJ
MADEP VPH 6 PASI-CLMB
EPA 6010D 1 PASI-ASH1
EPA 625.1 57 PASI-CPKS
SM 6200B 63 PASI-CCL
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 3 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92451374
ALAMANCE OIL 2019-210
Sample: MW-1 Lab ID: 92451374001 Collected: 10/28/19 11:55 Received: 10/29/19 10:35 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1625 RVE
Acenaphthene ND ug/L 11/04/19 18:25 83-32-911/01/19 16:185.0 1
Acenaphthylene ND ug/L 11/04/19 18:25 208-96-811/01/19 16:185.0 1
Anthracene ND ug/L 11/04/19 18:25 120-12-711/01/19 16:185.0 1
Benzo(a)anthracene ND ug/L 11/04/19 18:25 56-55-311/01/19 16:185.0 1
Benzo(a)pyrene ND ug/L 11/04/19 18:25 50-32-811/01/19 16:185.0 1
Benzo(b)fluoranthene ND ug/L 11/04/19 18:25 205-99-211/01/19 16:185.0 1
Benzo(g,h,i)perylene ND ug/L 11/04/19 18:25 191-24-211/01/19 16:185.0 1
Benzo(k)fluoranthene ND ug/L 11/04/19 18:25 207-08-911/01/19 16:185.0 1
4-Bromophenylphenyl ether ND ug/L 11/04/19 18:25 101-55-311/01/19 16:185.0 1
Butylbenzylphthalate ND ug/L 11/04/19 18:25 85-68-711/01/19 16:185.0 1
4-Chloro-3-methylphenol ND ug/L 11/04/19 18:25 59-50-711/01/19 16:185.0 1
bis(2-Chloroethoxy)methane ND ug/L 11/04/19 18:25 111-91-111/01/19 16:1810.0 1
bis(2-Chloroethyl) ether ND ug/L 11/04/19 18:25 111-44-411/01/19 16:185.0 1
2-Chloronaphthalene ND ug/L 11/04/19 18:25 91-58-711/01/19 16:185.0 1
2-Chlorophenol ND ug/L 11/04/19 18:25 95-57-811/01/19 16:185.0 1
4-Chlorophenylphenyl ether ND ug/L 11/04/19 18:25 7005-72-311/01/19 16:185.0 1
Chrysene ND ug/L 11/04/19 18:25 218-01-911/01/19 16:185.0 1
Dibenz(a,h)anthracene ND ug/L 11/04/19 18:25 53-70-311/01/19 16:185.0 1
3,3'-Dichlorobenzidine ND ug/L 11/04/19 18:25 91-94-111/01/19 16:1825.0 1
2,4-Dichlorophenol ND ug/L 11/04/19 18:25 120-83-211/01/19 16:185.0 1
Diethylphthalate ND ug/L 11/04/19 18:25 84-66-211/01/19 16:185.0 1
2,4-Dimethylphenol ND ug/L 11/04/19 18:25 105-67-911/01/19 16:1810.0 1
Dimethylphthalate ND ug/L 11/04/19 18:25 131-11-311/01/19 16:185.0 1
Di-n-butylphthalate ND ug/L 11/04/19 18:25 84-74-211/01/19 16:185.0 1
4,6-Dinitro-2-methylphenol ND ug/L 11/04/19 18:25 534-52-111/01/19 16:1820.0 1
2,4-Dinitrophenol ND ug/L 11/04/19 18:25 51-28-511/01/19 16:1850.0 1
2,4-Dinitrotoluene ND ug/L 11/04/19 18:25 121-14-211/01/19 16:185.0 1
2,6-Dinitrotoluene ND ug/L 11/04/19 18:25 606-20-211/01/19 16:185.0 1
Di-n-octylphthalate ND ug/L 11/04/19 18:25 117-84-011/01/19 16:185.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 11/04/19 18:25 117-81-711/01/19 16:185.0 1
Fluoranthene ND ug/L 11/04/19 18:25 206-44-011/01/19 16:185.0 1
Fluorene ND ug/L 11/04/19 18:25 86-73-711/01/19 16:185.0 1
Hexachloro-1,3-butadiene ND ug/L 11/04/19 18:25 87-68-311/01/19 16:185.0 1
Hexachlorobenzene ND ug/L 11/04/19 18:25 118-74-111/01/19 16:185.0 1
Hexachlorocyclopentadiene ND ug/L 11/04/19 18:25 77-47-411/01/19 16:1810.0 1
Hexachloroethane ND ug/L 11/04/19 18:25 67-72-111/01/19 16:185.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 11/04/19 18:25 193-39-511/01/19 16:185.0 1
Isophorone ND ug/L 11/04/19 18:25 78-59-111/01/19 16:1810.0 1
Naphthalene 362 ug/L 11/05/19 20:48 91-20-311/01/19 16:1820.0 4
Nitrobenzene ND ug/L 11/04/19 18:25 98-95-311/01/19 16:185.0 1
2-Nitrophenol ND ug/L 11/04/19 18:25 88-75-511/01/19 16:185.0 1
4-Nitrophenol ND ug/L 11/04/19 18:25 100-02-711/01/19 16:1850.0 1
N-Nitrosodimethylamine ND ug/L 11/04/19 18:25 62-75-911/01/19 16:185.0 1
N-Nitroso-di-n-propylamine ND ug/L 11/04/19 18:25 621-64-711/01/19 16:185.0 1
N-Nitrosodiphenylamine ND ug/L 11/04/19 18:25 86-30-611/01/19 16:1810.0 1
Pentachlorophenol ND ug/L 11/04/19 18:25 87-86-511/01/19 16:1810.0 1
Phenanthrene ND ug/L 11/04/19 18:25 85-01-811/01/19 16:185.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/08/2019 03:47 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
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Page 4 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92451374
ALAMANCE OIL 2019-210
Sample: MW-1 Lab ID: 92451374001 Collected: 10/28/19 11:55 Received: 10/29/19 10:35 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1625 RVE
Phenol 27.5 ug/L 11/04/19 18:25 108-95-211/01/19 16:185.0 1
Pyrene ND ug/L 11/04/19 18:25 129-00-011/01/19 16:185.0 1
1,2,4-Trichlorobenzene ND ug/L 11/04/19 18:25 120-82-111/01/19 16:185.0 1
2,4,6-Trichlorophenol ND ug/L 11/04/19 18:25 88-06-211/01/19 16:1810.0 1
Surrogates
Nitrobenzene-d5 (S)92 %11/04/19 18:25 4165-60-011/01/19 16:1810-120 1
2-Fluorobiphenyl (S)52 %11/04/19 18:25 321-60-811/01/19 16:1815-120 1
Terphenyl-d14 (S)93 %11/04/19 18:25 1718-51-011/01/19 16:1811-131 1
Phenol-d6 (S)63 %11/04/19 18:25 13127-88-311/01/19 16:1810-120 1
2-Fluorophenol (S)75 %11/04/19 18:25 367-12-411/01/19 16:1810-120 1
2,4,6-Tribromophenol (S)123 %11/04/19 18:25 118-79-611/01/19 16:1810-137 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/08/2019 03:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92451374
ALAMANCE OIL 2019-210
Sample: MW-2 Lab ID: 92451374002 Collected: 10/28/19 11:50 Received: 10/29/19 10:35 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 504.1 Preparation Method: EPA 504.1504 GCS EDB and DBCP
1,2-Dibromoethane (EDB)ND ug/L 11/02/19 01:18 106-93-411/01/19 08:510.019 1
Surrogates
1-Chloro-2-bromopropane (S)116 %11/02/19 01:18 301-79-5611/01/19 08:5170-130 1
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Water
Aliphatic (C09-C18)ND ug/L 11/04/19 17:11 N211/01/19 12:1196.2 1
Aliphatic (C19-C36)ND ug/L 11/04/19 17:11 N211/01/19 12:1196.2 1
Aromatic (C11-C22)444 ug/L 11/04/19 17:11 N211/01/19 12:1196.2 1
Surrogates
Nonatriacontane (S)66 %11/04/19 17:11 7194-86-711/01/19 12:1140-140 1
o-Terphenyl (S)74 %11/04/19 17:11 84-15-111/01/19 12:1140-140 1
2-Fluorobiphenyl (S)103 %11/04/19 17:11 321-60-811/01/19 12:1140-140 1
2-Bromonaphthalene (S)102 %11/04/19 17:11 580-13-211/01/19 12:1140-140 1
Analytical Method: MADEP VPHVPH NC Water
Aliphatic (C05-C08)113000 ug/L 10/30/19 18:19 N25000 100
Aliphatic (C09-C12)30800 ug/L 10/30/19 18:19 N25000 100
Aliphatic(C09-C12) Adjusted 18900 ug/L 10/30/19 18:19 N25000 100
Aromatic (C09-C10)12000 ug/L 10/30/19 18:19 N25000 100
Surrogates
4-Bromofluorobenzene (FID) (S)94 %10/30/19 18:19 460-00-470-130 100
4-Bromofluorobenzene (PID) (S)98 %10/30/19 18:19 460-00-470-130 100
Analytical Method: EPA 6010D Preparation Method: EPA 3010A6010 MET ICP
Lead ND ug/L 11/06/19 19:21 7439-92-111/01/19 21:555.0 1
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1625 RVE
Acenaphthene ND ug/L 11/04/19 18:51 83-32-911/01/19 16:185.0 1
Acenaphthylene ND ug/L 11/04/19 18:51 208-96-811/01/19 16:185.0 1
Anthracene ND ug/L 11/04/19 18:51 120-12-711/01/19 16:185.0 1
Benzo(a)anthracene ND ug/L 11/04/19 18:51 56-55-311/01/19 16:185.0 1
Benzo(a)pyrene ND ug/L 11/04/19 18:51 50-32-811/01/19 16:185.0 1
Benzo(b)fluoranthene ND ug/L 11/04/19 18:51 205-99-211/01/19 16:185.0 1
Benzo(g,h,i)perylene ND ug/L 11/04/19 18:51 191-24-211/01/19 16:185.0 1
Benzo(k)fluoranthene ND ug/L 11/04/19 18:51 207-08-911/01/19 16:185.0 1
4-Bromophenylphenyl ether ND ug/L 11/04/19 18:51 101-55-311/01/19 16:185.0 1
Butylbenzylphthalate ND ug/L 11/04/19 18:51 85-68-711/01/19 16:185.0 1
4-Chloro-3-methylphenol ND ug/L 11/04/19 18:51 59-50-711/01/19 16:185.0 1
bis(2-Chloroethoxy)methane ND ug/L 11/04/19 18:51 111-91-111/01/19 16:1810.0 1
bis(2-Chloroethyl) ether ND ug/L 11/04/19 18:51 111-44-411/01/19 16:185.0 1
2-Chloronaphthalene ND ug/L 11/04/19 18:51 91-58-711/01/19 16:185.0 1
2-Chlorophenol ND ug/L 11/04/19 18:51 95-57-811/01/19 16:185.0 1
4-Chlorophenylphenyl ether ND ug/L 11/04/19 18:51 7005-72-311/01/19 16:185.0 1
Chrysene ND ug/L 11/04/19 18:51 218-01-911/01/19 16:185.0 1
Dibenz(a,h)anthracene ND ug/L 11/04/19 18:51 53-70-311/01/19 16:185.0 1
3,3'-Dichlorobenzidine ND ug/L 11/04/19 18:51 91-94-111/01/19 16:1825.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/08/2019 03:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92451374
ALAMANCE OIL 2019-210
Sample: MW-2 Lab ID: 92451374002 Collected: 10/28/19 11:50 Received: 10/29/19 10:35 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1625 RVE
2,4-Dichlorophenol ND ug/L 11/04/19 18:51 120-83-211/01/19 16:185.0 1
Diethylphthalate ND ug/L 11/04/19 18:51 84-66-211/01/19 16:185.0 1
2,4-Dimethylphenol ND ug/L 11/04/19 18:51 105-67-911/01/19 16:1810.0 1
Dimethylphthalate ND ug/L 11/04/19 18:51 131-11-311/01/19 16:185.0 1
Di-n-butylphthalate ND ug/L 11/04/19 18:51 84-74-211/01/19 16:185.0 1
4,6-Dinitro-2-methylphenol ND ug/L 11/04/19 18:51 534-52-111/01/19 16:1820.0 1
2,4-Dinitrophenol ND ug/L 11/04/19 18:51 51-28-511/01/19 16:1850.0 1
2,4-Dinitrotoluene ND ug/L 11/04/19 18:51 121-14-211/01/19 16:185.0 1
2,6-Dinitrotoluene ND ug/L 11/04/19 18:51 606-20-211/01/19 16:185.0 1
Di-n-octylphthalate ND ug/L 11/04/19 18:51 117-84-011/01/19 16:185.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 11/04/19 18:51 117-81-711/01/19 16:185.0 1
Fluoranthene ND ug/L 11/04/19 18:51 206-44-011/01/19 16:185.0 1
Fluorene ND ug/L 11/04/19 18:51 86-73-711/01/19 16:185.0 1
Hexachloro-1,3-butadiene ND ug/L 11/04/19 18:51 87-68-311/01/19 16:185.0 1
Hexachlorobenzene ND ug/L 11/04/19 18:51 118-74-111/01/19 16:185.0 1
Hexachlorocyclopentadiene ND ug/L 11/04/19 18:51 77-47-411/01/19 16:1810.0 1
Hexachloroethane ND ug/L 11/04/19 18:51 67-72-111/01/19 16:185.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 11/04/19 18:51 193-39-511/01/19 16:185.0 1
Isophorone ND ug/L 11/04/19 18:51 78-59-111/01/19 16:1810.0 1
Naphthalene 350 ug/L 11/05/19 20:18 91-20-311/01/19 16:1820.0 4
Nitrobenzene ND ug/L 11/04/19 18:51 98-95-311/01/19 16:185.0 1
2-Nitrophenol ND ug/L 11/04/19 18:51 88-75-511/01/19 16:185.0 1
4-Nitrophenol ND ug/L 11/04/19 18:51 100-02-711/01/19 16:1850.0 1
N-Nitrosodimethylamine ND ug/L 11/04/19 18:51 62-75-911/01/19 16:185.0 1
N-Nitroso-di-n-propylamine ND ug/L 11/04/19 18:51 621-64-711/01/19 16:185.0 1
N-Nitrosodiphenylamine ND ug/L 11/04/19 18:51 86-30-611/01/19 16:1810.0 1
Pentachlorophenol ND ug/L 11/04/19 18:51 87-86-511/01/19 16:1810.0 1
Phenanthrene ND ug/L 11/04/19 18:51 85-01-811/01/19 16:185.0 1
Phenol 11.8 ug/L 11/04/19 18:51 108-95-211/01/19 16:185.0 1
Pyrene ND ug/L 11/04/19 18:51 129-00-011/01/19 16:185.0 1
1,2,4-Trichlorobenzene ND ug/L 11/04/19 18:51 120-82-111/01/19 16:185.0 1
2,4,6-Trichlorophenol ND ug/L 11/04/19 18:51 88-06-211/01/19 16:1810.0 1
Surrogates
Nitrobenzene-d5 (S)67 %11/04/19 18:51 4165-60-011/01/19 16:1810-120 1
2-Fluorobiphenyl (S)40 %11/04/19 18:51 321-60-811/01/19 16:1815-120 1
Terphenyl-d14 (S)80 %11/04/19 18:51 1718-51-011/01/19 16:1811-131 1
Phenol-d6 (S)51 %11/04/19 18:51 13127-88-311/01/19 16:1810-120 1
2-Fluorophenol (S)65 %11/04/19 18:51 367-12-411/01/19 16:1810-120 1
2,4,6-Tribromophenol (S)106 %11/04/19 18:51 118-79-611/01/19 16:1810-137 1
Analytical Method: SM 6200B6200B MSV
Benzene 14200 ug/L 11/06/19 16:39 71-43-2125 250
Bromobenzene ND ug/L 11/06/19 16:39 108-86-1125 250
Bromochloromethane ND ug/L 11/06/19 16:39 74-97-5125 250
Bromodichloromethane ND ug/L 11/06/19 16:39 75-27-4125 250
Bromoform ND ug/L 11/06/19 16:39 75-25-2125 250
Bromomethane ND ug/L 11/06/19 16:39 74-83-91250 250
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/08/2019 03:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92451374
ALAMANCE OIL 2019-210
Sample: MW-2 Lab ID: 92451374002 Collected: 10/28/19 11:50 Received: 10/29/19 10:35 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B6200B MSV
n-Butylbenzene ND ug/L 11/06/19 16:39 104-51-8125 250
sec-Butylbenzene ND ug/L 11/06/19 16:39 135-98-8125 250
tert-Butylbenzene ND ug/L 11/06/19 16:39 98-06-6125 250
Carbon tetrachloride ND ug/L 11/06/19 16:39 56-23-5125 250
Chlorobenzene ND ug/L 11/06/19 16:39 108-90-7125 250
Chloroethane ND ug/L 11/06/19 16:39 75-00-3250 250
Chloroform 389 ug/L 11/06/19 16:39 67-66-3 B,C9125 250
Chloromethane ND ug/L 11/06/19 16:39 74-87-3250 250
2-Chlorotoluene ND ug/L 11/06/19 16:39 95-49-8125 250
4-Chlorotoluene ND ug/L 11/06/19 16:39 106-43-4125 250
1,2-Dibromo-3-chloropropane ND ug/L 11/06/19 16:39 96-12-8250 250
Dibromochloromethane ND ug/L 11/06/19 16:39 124-48-1125 250
1,2-Dibromoethane (EDB)ND ug/L 11/06/19 16:39 106-93-4125 250
Dibromomethane ND ug/L 11/06/19 16:39 74-95-3125 250
1,2-Dichlorobenzene ND ug/L 11/06/19 16:39 95-50-1125 250
1,3-Dichlorobenzene ND ug/L 11/06/19 16:39 541-73-1125 250
1,4-Dichlorobenzene ND ug/L 11/06/19 16:39 106-46-7125 250
Dichlorodifluoromethane ND ug/L 11/06/19 16:39 75-71-8125 250
1,1-Dichloroethane ND ug/L 11/06/19 16:39 75-34-3125 250
1,2-Dichloroethane ND ug/L 11/06/19 16:39 107-06-2125 250
1,1-Dichloroethene ND ug/L 11/06/19 16:39 75-35-4125 250
cis-1,2-Dichloroethene ND ug/L 11/06/19 16:39 156-59-2125 250
trans-1,2-Dichloroethene ND ug/L 11/06/19 16:39 156-60-5125 250
1,2-Dichloropropane ND ug/L 11/06/19 16:39 78-87-5125 250
1,3-Dichloropropane ND ug/L 11/06/19 16:39 142-28-9125 250
2,2-Dichloropropane ND ug/L 11/06/19 16:39 594-20-7125 250
1,1-Dichloropropene ND ug/L 11/06/19 16:39 563-58-6125 250
cis-1,3-Dichloropropene ND ug/L 11/06/19 16:39 10061-01-5125 250
trans-1,3-Dichloropropene ND ug/L 11/06/19 16:39 10061-02-6125 250
Diisopropyl ether 1330 ug/L 11/06/19 16:39 108-20-3125 250
Ethylbenzene 2210 ug/L 11/06/19 16:39 100-41-4125 250
Hexachloro-1,3-butadiene ND ug/L 11/06/19 16:39 87-68-3500 250
Isopropylbenzene (Cumene)ND ug/L 11/06/19 16:39 98-82-8125 250
Methylene Chloride ND ug/L 11/06/19 16:39 75-09-2500 250
Methyl-tert-butyl ether 790 ug/L 11/06/19 16:39 1634-04-4125 250
Naphthalene 665 ug/L 11/06/19 16:39 91-20-3500 250
n-Propylbenzene 145 ug/L 11/06/19 16:39 103-65-1125 250
Styrene 185 ug/L 11/06/19 16:39 100-42-5125 250
1,1,1,2-Tetrachloroethane ND ug/L 11/06/19 16:39 630-20-6125 250
1,1,2,2-Tetrachloroethane ND ug/L 11/06/19 16:39 79-34-5125 250
Tetrachloroethene ND ug/L 11/06/19 16:39 127-18-4125 250
Toluene 36500 ug/L 11/06/19 16:39 108-88-3125 250
1,2,3-Trichlorobenzene ND ug/L 11/06/19 16:39 87-61-6500 250
1,2,4-Trichlorobenzene ND ug/L 11/06/19 16:39 120-82-1500 250
1,1,1-Trichloroethane ND ug/L 11/06/19 16:39 71-55-6125 250
1,1,2-Trichloroethane ND ug/L 11/06/19 16:39 79-00-5125 250
Trichloroethene ND ug/L 11/06/19 16:39 79-01-6125 250
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/08/2019 03:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92451374
ALAMANCE OIL 2019-210
Sample: MW-2 Lab ID: 92451374002 Collected: 10/28/19 11:50 Received: 10/29/19 10:35 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B6200B MSV
Trichlorofluoromethane ND ug/L 11/06/19 16:39 75-69-4250 250
1,2,3-Trichloropropane ND ug/L 11/06/19 16:39 96-18-4125 250
1,2,4-Trimethylbenzene 1280 ug/L 11/06/19 16:39 95-63-6125 250
1,3,5-Trimethylbenzene 284 ug/L 11/06/19 16:39 108-67-8125 250
Vinyl chloride ND ug/L 11/06/19 16:39 75-01-4250 250
m&p-Xylene 7320 ug/L 11/06/19 16:39 179601-23-1250 250
o-Xylene 4090 ug/L 11/06/19 16:39 95-47-6125 250
Surrogates
1,2-Dichloroethane-d4 (S)96 %11/06/19 16:39 17060-07-070-130 250
4-Bromofluorobenzene (S)108 %11/06/19 16:39 460-00-470-130 250
Toluene-d8 (S)98 %11/06/19 16:39 2037-26-570-130 250
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/08/2019 03:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92451374
ALAMANCE OIL 2019-210
Sample: MW-3 Lab ID: 92451374003 Collected: 10/28/19 11:25 Received: 10/29/19 10:35 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 504.1 Preparation Method: EPA 504.1504 GCS EDB and DBCP
1,2-Dibromoethane (EDB)ND ug/L 11/07/19 16:40 106-93-411/07/19 08:500.020 1
Surrogates
1-Chloro-2-bromopropane (S)93 %11/07/19 16:40 301-79-5611/07/19 08:5070-130 1
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Water
Aliphatic (C09-C18)ND ug/L 11/04/19 17:38 N211/01/19 12:1197.1 1
Aliphatic (C19-C36)ND ug/L 11/04/19 17:38 N211/01/19 12:1197.1 1
Aromatic (C11-C22)134 ug/L 11/04/19 17:38 N211/01/19 12:1197.1 1
Surrogates
Nonatriacontane (S)89 %11/04/19 17:38 7194-86-711/01/19 12:1140-140 1
o-Terphenyl (S)87 %11/04/19 17:38 84-15-111/01/19 12:1140-140 1
2-Fluorobiphenyl (S)101 %11/04/19 17:38 321-60-811/01/19 12:1140-140 1
2-Bromonaphthalene (S)102 %11/04/19 17:38 580-13-211/01/19 12:1140-140 1
Analytical Method: MADEP VPHVPH NC Water
Aliphatic (C05-C08)2490 ug/L 10/30/19 20:17 N250.0 1
Aliphatic (C09-C12)648 ug/L 10/30/19 20:17 N250.0 1
Aliphatic(C09-C12) Adjusted 325 ug/L 10/30/19 20:17 N250.0 1
Aromatic (C09-C10)323 ug/L 10/30/19 20:17 N250.0 1
Surrogates
4-Bromofluorobenzene (FID) (S)96 %10/30/19 20:17 460-00-470-130 1
4-Bromofluorobenzene (PID) (S)97 %10/30/19 20:17 460-00-470-130 1
Analytical Method: EPA 6010D Preparation Method: EPA 3010A6010 MET ICP
Lead ND ug/L 11/06/19 19:24 7439-92-111/01/19 21:555.0 1
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1625 RVE
Acenaphthene ND ug/L 11/04/19 19:16 83-32-911/01/19 16:185.0 1
Acenaphthylene ND ug/L 11/04/19 19:16 208-96-811/01/19 16:185.0 1
Anthracene ND ug/L 11/04/19 19:16 120-12-711/01/19 16:185.0 1
Benzo(a)anthracene ND ug/L 11/04/19 19:16 56-55-311/01/19 16:185.0 1
Benzo(a)pyrene ND ug/L 11/04/19 19:16 50-32-811/01/19 16:185.0 1
Benzo(b)fluoranthene ND ug/L 11/04/19 19:16 205-99-211/01/19 16:185.0 1
Benzo(g,h,i)perylene ND ug/L 11/04/19 19:16 191-24-211/01/19 16:185.0 1
Benzo(k)fluoranthene ND ug/L 11/04/19 19:16 207-08-911/01/19 16:185.0 1
4-Bromophenylphenyl ether ND ug/L 11/04/19 19:16 101-55-311/01/19 16:185.0 1
Butylbenzylphthalate ND ug/L 11/04/19 19:16 85-68-711/01/19 16:185.0 1
4-Chloro-3-methylphenol ND ug/L 11/04/19 19:16 59-50-711/01/19 16:185.0 1
bis(2-Chloroethoxy)methane ND ug/L 11/04/19 19:16 111-91-111/01/19 16:1810.0 1
bis(2-Chloroethyl) ether ND ug/L 11/04/19 19:16 111-44-411/01/19 16:185.0 1
2-Chloronaphthalene ND ug/L 11/04/19 19:16 91-58-711/01/19 16:185.0 1
2-Chlorophenol ND ug/L 11/04/19 19:16 95-57-811/01/19 16:185.0 1
4-Chlorophenylphenyl ether ND ug/L 11/04/19 19:16 7005-72-311/01/19 16:185.0 1
Chrysene ND ug/L 11/04/19 19:16 218-01-911/01/19 16:185.0 1
Dibenz(a,h)anthracene ND ug/L 11/04/19 19:16 53-70-311/01/19 16:185.0 1
3,3'-Dichlorobenzidine ND ug/L 11/04/19 19:16 91-94-111/01/19 16:1825.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/08/2019 03:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92451374
ALAMANCE OIL 2019-210
Sample: MW-3 Lab ID: 92451374003 Collected: 10/28/19 11:25 Received: 10/29/19 10:35 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1625 RVE
2,4-Dichlorophenol ND ug/L 11/04/19 19:16 120-83-211/01/19 16:185.0 1
Diethylphthalate ND ug/L 11/04/19 19:16 84-66-211/01/19 16:185.0 1
2,4-Dimethylphenol ND ug/L 11/04/19 19:16 105-67-911/01/19 16:1810.0 1
Dimethylphthalate ND ug/L 11/04/19 19:16 131-11-311/01/19 16:185.0 1
Di-n-butylphthalate ND ug/L 11/04/19 19:16 84-74-211/01/19 16:185.0 1
4,6-Dinitro-2-methylphenol ND ug/L 11/04/19 19:16 534-52-111/01/19 16:1820.0 1
2,4-Dinitrophenol ND ug/L 11/04/19 19:16 51-28-511/01/19 16:1850.0 1
2,4-Dinitrotoluene ND ug/L 11/04/19 19:16 121-14-211/01/19 16:185.0 1
2,6-Dinitrotoluene ND ug/L 11/04/19 19:16 606-20-211/01/19 16:185.0 1
Di-n-octylphthalate ND ug/L 11/04/19 19:16 117-84-011/01/19 16:185.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 11/04/19 19:16 117-81-711/01/19 16:185.0 1
Fluoranthene ND ug/L 11/04/19 19:16 206-44-011/01/19 16:185.0 1
Fluorene ND ug/L 11/04/19 19:16 86-73-711/01/19 16:185.0 1
Hexachloro-1,3-butadiene ND ug/L 11/04/19 19:16 87-68-311/01/19 16:185.0 1
Hexachlorobenzene ND ug/L 11/04/19 19:16 118-74-111/01/19 16:185.0 1
Hexachlorocyclopentadiene ND ug/L 11/04/19 19:16 77-47-411/01/19 16:1810.0 1
Hexachloroethane ND ug/L 11/04/19 19:16 67-72-111/01/19 16:185.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 11/04/19 19:16 193-39-511/01/19 16:185.0 1
Isophorone ND ug/L 11/04/19 19:16 78-59-111/01/19 16:1810.0 1
Naphthalene 18.4 ug/L 11/04/19 19:16 91-20-311/01/19 16:185.0 1
Nitrobenzene ND ug/L 11/04/19 19:16 98-95-311/01/19 16:185.0 1
2-Nitrophenol ND ug/L 11/04/19 19:16 88-75-511/01/19 16:185.0 1
4-Nitrophenol ND ug/L 11/04/19 19:16 100-02-711/01/19 16:1850.0 1
N-Nitrosodimethylamine ND ug/L 11/04/19 19:16 62-75-911/01/19 16:185.0 1
N-Nitroso-di-n-propylamine ND ug/L 11/04/19 19:16 621-64-711/01/19 16:185.0 1
N-Nitrosodiphenylamine ND ug/L 11/04/19 19:16 86-30-611/01/19 16:1810.0 1
Pentachlorophenol ND ug/L 11/04/19 19:16 87-86-511/01/19 16:1810.0 1
Phenanthrene ND ug/L 11/04/19 19:16 85-01-811/01/19 16:185.0 1
Phenol ND ug/L 11/04/19 19:16 108-95-211/01/19 16:185.0 1
Pyrene ND ug/L 11/04/19 19:16 129-00-011/01/19 16:185.0 1
1,2,4-Trichlorobenzene ND ug/L 11/04/19 19:16 120-82-111/01/19 16:185.0 1
2,4,6-Trichlorophenol ND ug/L 11/04/19 19:16 88-06-211/01/19 16:1810.0 1
Surrogates
Nitrobenzene-d5 (S)69 %11/04/19 19:16 4165-60-011/01/19 16:1810-120 1
2-Fluorobiphenyl (S)61 %11/04/19 19:16 321-60-811/01/19 16:1815-120 1
Terphenyl-d14 (S)66 %11/04/19 19:16 1718-51-011/01/19 16:1811-131 1
Phenol-d6 (S)35 %11/04/19 19:16 13127-88-311/01/19 16:1810-120 1
2-Fluorophenol (S)42 %11/04/19 19:16 367-12-411/01/19 16:1810-120 1
2,4,6-Tribromophenol (S)76 %11/04/19 19:16 118-79-611/01/19 16:1810-137 1
Analytical Method: SM 6200B6200B MSV
Benzene 394 ug/L 11/06/19 14:33 71-43-21.2 2.5
Bromobenzene ND ug/L 11/06/19 14:33 108-86-11.2 2.5
Bromochloromethane ND ug/L 11/06/19 14:33 74-97-51.2 2.5
Bromodichloromethane ND ug/L 11/06/19 14:33 75-27-41.2 2.5
Bromoform ND ug/L 11/06/19 14:33 75-25-21.2 2.5
Bromomethane ND ug/L 11/06/19 14:33 74-83-912.5 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/08/2019 03:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92451374
ALAMANCE OIL 2019-210
Sample: MW-3 Lab ID: 92451374003 Collected: 10/28/19 11:25 Received: 10/29/19 10:35 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B6200B MSV
n-Butylbenzene 5.0 ug/L 11/06/19 14:33 104-51-81.2 2.5
sec-Butylbenzene ND ug/L 11/06/19 14:33 135-98-81.2 2.5
tert-Butylbenzene ND ug/L 11/06/19 14:33 98-06-61.2 2.5
Carbon tetrachloride ND ug/L 11/06/19 14:33 56-23-51.2 2.5
Chlorobenzene ND ug/L 11/06/19 14:33 108-90-71.2 2.5
Chloroethane ND ug/L 11/06/19 14:33 75-00-32.5 2.5
Chloroform ND ug/L 11/06/19 14:33 67-66-31.2 2.5
Chloromethane ND ug/L 11/06/19 14:33 74-87-32.5 2.5
2-Chlorotoluene ND ug/L 11/06/19 14:33 95-49-81.2 2.5
4-Chlorotoluene ND ug/L 11/06/19 14:33 106-43-41.2 2.5
1,2-Dibromo-3-chloropropane ND ug/L 11/06/19 14:33 96-12-82.5 2.5
Dibromochloromethane ND ug/L 11/06/19 14:33 124-48-11.2 2.5
1,2-Dibromoethane (EDB)ND ug/L 11/06/19 14:33 106-93-41.2 2.5
Dibromomethane ND ug/L 11/06/19 14:33 74-95-31.2 2.5
1,2-Dichlorobenzene ND ug/L 11/06/19 14:33 95-50-11.2 2.5
1,3-Dichlorobenzene ND ug/L 11/06/19 14:33 541-73-11.2 2.5
1,4-Dichlorobenzene ND ug/L 11/06/19 14:33 106-46-71.2 2.5
Dichlorodifluoromethane ND ug/L 11/06/19 14:33 75-71-81.2 2.5
1,1-Dichloroethane ND ug/L 11/06/19 14:33 75-34-31.2 2.5
1,2-Dichloroethane ND ug/L 11/06/19 14:33 107-06-21.2 2.5
1,1-Dichloroethene ND ug/L 11/06/19 14:33 75-35-41.2 2.5
cis-1,2-Dichloroethene ND ug/L 11/06/19 14:33 156-59-21.2 2.5
trans-1,2-Dichloroethene ND ug/L 11/06/19 14:33 156-60-51.2 2.5
1,2-Dichloropropane ND ug/L 11/06/19 14:33 78-87-51.2 2.5
1,3-Dichloropropane ND ug/L 11/06/19 14:33 142-28-91.2 2.5
2,2-Dichloropropane ND ug/L 11/06/19 14:33 594-20-71.2 2.5
1,1-Dichloropropene ND ug/L 11/06/19 14:33 563-58-61.2 2.5
cis-1,3-Dichloropropene ND ug/L 11/06/19 14:33 10061-01-51.2 2.5
trans-1,3-Dichloropropene ND ug/L 11/06/19 14:33 10061-02-61.2 2.5
Diisopropyl ether 22.7 ug/L 11/06/19 14:33 108-20-31.2 2.5
Ethylbenzene 22.4 ug/L 11/06/19 14:33 100-41-41.2 2.5
Hexachloro-1,3-butadiene ND ug/L 11/06/19 14:33 87-68-35.0 2.5
Isopropylbenzene (Cumene)6.4 ug/L 11/06/19 14:33 98-82-81.2 2.5
Methylene Chloride ND ug/L 11/06/19 14:33 75-09-25.0 2.5
Methyl-tert-butyl ether 248 ug/L 11/06/19 14:33 1634-04-41.2 2.5
Naphthalene 33.0 ug/L 11/06/19 14:33 91-20-35.0 2.5
n-Propylbenzene 10.9 ug/L 11/06/19 14:33 103-65-11.2 2.5
Styrene ND ug/L 11/06/19 14:33 100-42-51.2 2.5
1,1,1,2-Tetrachloroethane ND ug/L 11/06/19 14:33 630-20-61.2 2.5
1,1,2,2-Tetrachloroethane ND ug/L 11/06/19 14:33 79-34-51.2 2.5
Tetrachloroethene ND ug/L 11/06/19 14:33 127-18-41.2 2.5
Toluene 42.6 ug/L 11/06/19 14:33 108-88-31.2 2.5
1,2,3-Trichlorobenzene ND ug/L 11/06/19 14:33 87-61-65.0 2.5
1,2,4-Trichlorobenzene ND ug/L 11/06/19 14:33 120-82-15.0 2.5
1,1,1-Trichloroethane ND ug/L 11/06/19 14:33 71-55-61.2 2.5
1,1,2-Trichloroethane ND ug/L 11/06/19 14:33 79-00-51.2 2.5
Trichloroethene ND ug/L 11/06/19 14:33 79-01-61.2 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/08/2019 03:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92451374
ALAMANCE OIL 2019-210
Sample: MW-3 Lab ID: 92451374003 Collected: 10/28/19 11:25 Received: 10/29/19 10:35 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B6200B MSV
Trichlorofluoromethane ND ug/L 11/06/19 14:33 75-69-42.5 2.5
1,2,3-Trichloropropane ND ug/L 11/06/19 14:33 96-18-41.2 2.5
1,2,4-Trimethylbenzene 64.3 ug/L 11/06/19 14:33 95-63-61.2 2.5
1,3,5-Trimethylbenzene 13.0 ug/L 11/06/19 14:33 108-67-81.2 2.5
Vinyl chloride ND ug/L 11/06/19 14:33 75-01-42.5 2.5
m&p-Xylene 114 ug/L 11/06/19 14:33 179601-23-12.5 2.5
o-Xylene 82.4 ug/L 11/06/19 14:33 95-47-61.2 2.5
Surrogates
1,2-Dichloroethane-d4 (S)93 %11/06/19 14:33 17060-07-070-130 2.5
4-Bromofluorobenzene (S)98 %11/06/19 14:33 460-00-470-130 2.5
Toluene-d8 (S)100 %11/06/19 14:33 2037-26-570-130 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/08/2019 03:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92451374
ALAMANCE OIL 2019-210
Sample: MW-4 Lab ID: 92451374004 Collected: 10/28/19 11:20 Received: 10/29/19 10:35 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 504.1 Preparation Method: EPA 504.1504 GCS EDB and DBCP
1,2-Dibromoethane (EDB)ND ug/L 11/07/19 16:52 106-93-411/07/19 08:500.020 1
Surrogates
1-Chloro-2-bromopropane (S)154 %11/07/19 16:52 301-79-56 S511/07/19 08:5070-130 1
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Water
Aliphatic (C09-C18)ND ug/L 11/04/19 18:05 N211/01/19 12:1196.2 1
Aliphatic (C19-C36)ND ug/L 11/04/19 18:05 N211/01/19 12:1196.2 1
Aromatic (C11-C22)731 ug/L 11/04/19 18:05 N211/01/19 12:1196.2 1
Surrogates
Nonatriacontane (S)85 %11/04/19 18:05 7194-86-711/01/19 12:1140-140 1
o-Terphenyl (S)89 %11/04/19 18:05 84-15-111/01/19 12:1140-140 1
2-Fluorobiphenyl (S)96 %11/04/19 18:05 321-60-811/01/19 12:1140-140 1
2-Bromonaphthalene (S)103 %11/04/19 18:05 580-13-211/01/19 12:1140-140 1
Analytical Method: MADEP VPHVPH NC Water
Aliphatic (C05-C08)1960 ug/L 10/30/19 18:48 N2125 2.5
Aliphatic (C09-C12)6770 ug/L 10/30/19 18:48 N2125 2.5
Aliphatic(C09-C12) Adjusted 3250 ug/L 10/30/19 18:48 N2125 2.5
Aromatic (C09-C10)3520 ug/L 10/30/19 18:48 N2125 2.5
Surrogates
4-Bromofluorobenzene (FID) (S)93 %10/30/19 18:48 460-00-470-130 2.5
4-Bromofluorobenzene (PID) (S)97 %10/30/19 18:48 460-00-470-130 2.5
Analytical Method: EPA 6010D Preparation Method: EPA 3010A6010 MET ICP
Lead ND ug/L 11/06/19 19:27 7439-92-111/01/19 21:555.0 1
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1625 RVE
Acenaphthene ND ug/L 11/04/19 19:41 83-32-911/01/19 16:185.0 1
Acenaphthylene ND ug/L 11/04/19 19:41 208-96-811/01/19 16:185.0 1
Anthracene ND ug/L 11/04/19 19:41 120-12-711/01/19 16:185.0 1
Benzo(a)anthracene ND ug/L 11/04/19 19:41 56-55-311/01/19 16:185.0 1
Benzo(a)pyrene ND ug/L 11/04/19 19:41 50-32-811/01/19 16:185.0 1
Benzo(b)fluoranthene ND ug/L 11/04/19 19:41 205-99-211/01/19 16:185.0 1
Benzo(g,h,i)perylene ND ug/L 11/04/19 19:41 191-24-211/01/19 16:185.0 1
Benzo(k)fluoranthene ND ug/L 11/04/19 19:41 207-08-911/01/19 16:185.0 1
4-Bromophenylphenyl ether ND ug/L 11/04/19 19:41 101-55-311/01/19 16:185.0 1
Butylbenzylphthalate ND ug/L 11/04/19 19:41 85-68-711/01/19 16:185.0 1
4-Chloro-3-methylphenol ND ug/L 11/04/19 19:41 59-50-711/01/19 16:185.0 1
bis(2-Chloroethoxy)methane ND ug/L 11/04/19 19:41 111-91-111/01/19 16:1810.0 1
bis(2-Chloroethyl) ether ND ug/L 11/04/19 19:41 111-44-411/01/19 16:185.0 1
2-Chloronaphthalene ND ug/L 11/04/19 19:41 91-58-711/01/19 16:185.0 1
2-Chlorophenol ND ug/L 11/04/19 19:41 95-57-811/01/19 16:185.0 1
4-Chlorophenylphenyl ether ND ug/L 11/04/19 19:41 7005-72-311/01/19 16:185.0 1
Chrysene ND ug/L 11/04/19 19:41 218-01-911/01/19 16:185.0 1
Dibenz(a,h)anthracene ND ug/L 11/04/19 19:41 53-70-311/01/19 16:185.0 1
3,3'-Dichlorobenzidine ND ug/L 11/04/19 19:41 91-94-111/01/19 16:1825.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/08/2019 03:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92451374
ALAMANCE OIL 2019-210
Sample: MW-4 Lab ID: 92451374004 Collected: 10/28/19 11:20 Received: 10/29/19 10:35 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1625 RVE
2,4-Dichlorophenol ND ug/L 11/04/19 19:41 120-83-211/01/19 16:185.0 1
Diethylphthalate ND ug/L 11/04/19 19:41 84-66-211/01/19 16:185.0 1
2,4-Dimethylphenol ND ug/L 11/04/19 19:41 105-67-911/01/19 16:1810.0 1
Dimethylphthalate ND ug/L 11/04/19 19:41 131-11-311/01/19 16:185.0 1
Di-n-butylphthalate ND ug/L 11/04/19 19:41 84-74-211/01/19 16:185.0 1
4,6-Dinitro-2-methylphenol ND ug/L 11/04/19 19:41 534-52-111/01/19 16:1820.0 1
2,4-Dinitrophenol ND ug/L 11/04/19 19:41 51-28-511/01/19 16:1850.0 1
2,4-Dinitrotoluene ND ug/L 11/04/19 19:41 121-14-211/01/19 16:185.0 1
2,6-Dinitrotoluene ND ug/L 11/04/19 19:41 606-20-211/01/19 16:185.0 1
Di-n-octylphthalate ND ug/L 11/04/19 19:41 117-84-011/01/19 16:185.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 11/04/19 19:41 117-81-711/01/19 16:185.0 1
Fluoranthene ND ug/L 11/04/19 19:41 206-44-011/01/19 16:185.0 1
Fluorene ND ug/L 11/04/19 19:41 86-73-711/01/19 16:185.0 1
Hexachloro-1,3-butadiene ND ug/L 11/04/19 19:41 87-68-311/01/19 16:185.0 1
Hexachlorobenzene ND ug/L 11/04/19 19:41 118-74-111/01/19 16:185.0 1
Hexachlorocyclopentadiene ND ug/L 11/04/19 19:41 77-47-411/01/19 16:1810.0 1
Hexachloroethane ND ug/L 11/04/19 19:41 67-72-111/01/19 16:185.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 11/04/19 19:41 193-39-511/01/19 16:185.0 1
Isophorone ND ug/L 11/04/19 19:41 78-59-111/01/19 16:1810.0 1
Naphthalene 143 ug/L 11/04/19 19:41 91-20-311/01/19 16:185.0 1
Nitrobenzene ND ug/L 11/04/19 19:41 98-95-311/01/19 16:185.0 1
2-Nitrophenol ND ug/L 11/04/19 19:41 88-75-511/01/19 16:185.0 1
4-Nitrophenol ND ug/L 11/04/19 19:41 100-02-711/01/19 16:1850.0 1
N-Nitrosodimethylamine ND ug/L 11/04/19 19:41 62-75-911/01/19 16:185.0 1
N-Nitroso-di-n-propylamine ND ug/L 11/04/19 19:41 621-64-711/01/19 16:185.0 1
N-Nitrosodiphenylamine ND ug/L 11/04/19 19:41 86-30-611/01/19 16:1810.0 1
Pentachlorophenol ND ug/L 11/04/19 19:41 87-86-511/01/19 16:1810.0 1
Phenanthrene ND ug/L 11/04/19 19:41 85-01-811/01/19 16:185.0 1
Phenol ND ug/L 11/04/19 19:41 108-95-211/01/19 16:185.0 1
Pyrene ND ug/L 11/04/19 19:41 129-00-011/01/19 16:185.0 1
1,2,4-Trichlorobenzene ND ug/L 11/04/19 19:41 120-82-111/01/19 16:185.0 1
2,4,6-Trichlorophenol ND ug/L 11/04/19 19:41 88-06-211/01/19 16:1810.0 1
Surrogates
Nitrobenzene-d5 (S)52 %11/04/19 19:41 4165-60-011/01/19 16:1810-120 1
2-Fluorobiphenyl (S)33 %11/04/19 19:41 321-60-811/01/19 16:1815-120 1
Terphenyl-d14 (S)61 %11/04/19 19:41 1718-51-011/01/19 16:1811-131 1
Phenol-d6 (S)37 %11/04/19 19:41 13127-88-311/01/19 16:1810-120 1
2-Fluorophenol (S)43 %11/04/19 19:41 367-12-411/01/19 16:1810-120 1
2,4,6-Tribromophenol (S)53 %11/04/19 19:41 118-79-611/01/19 16:1810-137 1
Analytical Method: SM 6200B6200B MSV
Benzene 614 ug/L 11/07/19 14:54 71-43-25.0 10
Bromobenzene ND ug/L 11/07/19 14:54 108-86-15.0 10
Bromochloromethane ND ug/L 11/07/19 14:54 74-97-55.0 10
Bromodichloromethane 38.3 ug/L 11/07/19 14:54 75-27-45.0 10
Bromoform ND ug/L 11/07/19 14:54 75-25-25.0 10
Bromomethane ND ug/L 11/07/19 14:54 74-83-950.0 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/08/2019 03:47 PM
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Page 15 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92451374
ALAMANCE OIL 2019-210
Sample: MW-4 Lab ID: 92451374004 Collected: 10/28/19 11:20 Received: 10/29/19 10:35 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B6200B MSV
n-Butylbenzene 15.5 ug/L 11/07/19 14:54 104-51-85.0 10
sec-Butylbenzene ND ug/L 11/07/19 14:54 135-98-85.0 10
tert-Butylbenzene ND ug/L 11/07/19 14:54 98-06-65.0 10
Carbon tetrachloride ND ug/L 11/07/19 14:54 56-23-55.0 10
Chlorobenzene ND ug/L 11/07/19 14:54 108-90-75.0 10
Chloroethane ND ug/L 11/07/19 14:54 75-00-310.0 10
Chloroform 132 ug/L 11/07/19 14:54 67-66-35.0 10
Chloromethane ND ug/L 11/07/19 14:54 74-87-310.0 10
2-Chlorotoluene ND ug/L 11/07/19 14:54 95-49-85.0 10
4-Chlorotoluene ND ug/L 11/07/19 14:54 106-43-45.0 10
1,2-Dibromo-3-chloropropane ND ug/L 11/07/19 14:54 96-12-810.0 10
Dibromochloromethane 22.4 ug/L 11/07/19 14:54 124-48-15.0 10
1,2-Dibromoethane (EDB)ND ug/L 11/07/19 14:54 106-93-45.0 10
Dibromomethane ND ug/L 11/07/19 14:54 74-95-35.0 10
1,2-Dichlorobenzene ND ug/L 11/07/19 14:54 95-50-15.0 10
1,3-Dichlorobenzene ND ug/L 11/07/19 14:54 541-73-15.0 10
1,4-Dichlorobenzene ND ug/L 11/07/19 14:54 106-46-75.0 10
Dichlorodifluoromethane ND ug/L 11/07/19 14:54 75-71-85.0 10
1,1-Dichloroethane ND ug/L 11/07/19 14:54 75-34-35.0 10
1,2-Dichloroethane ND ug/L 11/07/19 14:54 107-06-25.0 10
1,1-Dichloroethene ND ug/L 11/07/19 14:54 75-35-45.0 10
cis-1,2-Dichloroethene ND ug/L 11/07/19 14:54 156-59-25.0 10
trans-1,2-Dichloroethene ND ug/L 11/07/19 14:54 156-60-55.0 10
1,2-Dichloropropane ND ug/L 11/07/19 14:54 78-87-55.0 10
1,3-Dichloropropane ND ug/L 11/07/19 14:54 142-28-95.0 10
2,2-Dichloropropane ND ug/L 11/07/19 14:54 594-20-75.0 10
1,1-Dichloropropene ND ug/L 11/07/19 14:54 563-58-65.0 10
cis-1,3-Dichloropropene ND ug/L 11/07/19 14:54 10061-01-55.0 10
trans-1,3-Dichloropropene ND ug/L 11/07/19 14:54 10061-02-65.0 10
Diisopropyl ether 31.8 ug/L 11/07/19 14:54 108-20-35.0 10
Ethylbenzene 551 ug/L 11/07/19 14:54 100-41-45.0 10
Hexachloro-1,3-butadiene ND ug/L 11/07/19 14:54 87-68-320.0 10
Isopropylbenzene (Cumene)29.4 ug/L 11/07/19 14:54 98-82-85.0 10
Methylene Chloride 30.2 ug/L 11/07/19 14:54 75-09-2 C920.0 10
Methyl-tert-butyl ether 126 ug/L 11/07/19 14:54 1634-04-45.0 10
Naphthalene 439 ug/L 11/07/19 14:54 91-20-320.0 10
n-Propylbenzene 89.4 ug/L 11/07/19 14:54 103-65-15.0 10
Styrene ND ug/L 11/07/19 14:54 100-42-55.0 10
1,1,1,2-Tetrachloroethane ND ug/L 11/07/19 14:54 630-20-65.0 10
1,1,2,2-Tetrachloroethane ND ug/L 11/07/19 14:54 79-34-55.0 10
Tetrachloroethene ND ug/L 11/07/19 14:54 127-18-45.0 10
Toluene 59.2 ug/L 11/07/19 14:54 108-88-35.0 10
1,2,3-Trichlorobenzene ND ug/L 11/07/19 14:54 87-61-620.0 10
1,2,4-Trichlorobenzene ND ug/L 11/07/19 14:54 120-82-120.0 10
1,1,1-Trichloroethane ND ug/L 11/07/19 14:54 71-55-65.0 10
1,1,2-Trichloroethane ND ug/L 11/07/19 14:54 79-00-55.0 10
Trichloroethene ND ug/L 11/07/19 14:54 79-01-65.0 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/08/2019 03:47 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 16 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92451374
ALAMANCE OIL 2019-210
Sample: MW-4 Lab ID: 92451374004 Collected: 10/28/19 11:20 Received: 10/29/19 10:35 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B6200B MSV
Trichlorofluoromethane ND ug/L 11/07/19 14:54 75-69-410.0 10
1,2,3-Trichloropropane 8.6 ug/L 11/07/19 14:54 96-18-45.0 10
1,2,4-Trimethylbenzene 1100 ug/L 11/07/19 14:54 95-63-65.0 10
1,3,5-Trimethylbenzene 263 ug/L 11/07/19 14:54 108-67-85.0 10
Vinyl chloride ND ug/L 11/07/19 14:54 75-01-410.0 10
m&p-Xylene 837 ug/L 11/07/19 14:54 179601-23-110.0 10
o-Xylene 536 ug/L 11/07/19 14:54 95-47-65.0 10
Surrogates
1,2-Dichloroethane-d4 (S)96 %11/07/19 14:54 17060-07-070-130 10
4-Bromofluorobenzene (S)98 %11/07/19 14:54 460-00-470-130 10
Toluene-d8 (S)104 %11/07/19 14:54 2037-26-570-130 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/08/2019 03:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92451374
ALAMANCE OIL 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
506718
MADEP VPH
MADEP VPH
VPH NC Water
Associated Lab Samples: 92451374002, 92451374003, 92451374004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2720955
Associated Lab Samples:92451374002, 92451374003, 92451374004
Matrix: Water
Analyzed
Aliphatic (C05-C08)ug/L ND 50.0 N210/30/19 15:22
Aliphatic (C09-C12)ug/L ND 50.0 N210/30/19 15:22
Aromatic (C09-C10)ug/L ND 50.0 N210/30/19 15:22
4-Bromofluorobenzene (FID) (S)%97 70-130 10/30/19 15:22
4-Bromofluorobenzene (PID) (S)%98 70-130 10/30/19 15:22
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2720956LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2720957
Aliphatic (C05-C08)ug/L 315 N230010570-13098293 7 25
Aliphatic (C09-C12)ug/L 301 N230010030-13094282 7 25
Aromatic (C09-C10)ug/L 100 N210010070-1309493.9 7 25
4-Bromofluorobenzene (FID) (S)%103 70-130102
4-Bromofluorobenzene (PID) (S)%103 70-130102
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/08/2019 03:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92451374
ALAMANCE OIL 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
507236
EPA 3010A
EPA 6010D
6010 MET
Associated Lab Samples: 92451374002, 92451374003, 92451374004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2723514
Associated Lab Samples:92451374002, 92451374003, 92451374004
Matrix: Water
Analyzed
Lead ug/L ND 5.0 11/06/19 19:03
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2723515LABORATORY CONTROL SAMPLE:
LCSSpike
Lead ug/L 473500 95 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2723516MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92451814001
2723517
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Lead ug/L 500 94 75-12592 25003.0J 473 463
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/08/2019 03:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92451374
ALAMANCE OIL 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
507868
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples: 92451374002, 92451374003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2726324
Associated Lab Samples:92451374002, 92451374003
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 11/06/19 11:17
1,1,1-Trichloroethane ug/L ND 0.50 11/06/19 11:17
1,1,2,2-Tetrachloroethane ug/L ND 0.50 11/06/19 11:17
1,1,2-Trichloroethane ug/L ND 0.50 11/06/19 11:17
1,1-Dichloroethane ug/L ND 0.50 11/06/19 11:17
1,1-Dichloroethene ug/L ND 0.50 11/06/19 11:17
1,1-Dichloropropene ug/L ND 0.50 11/06/19 11:17
1,2,3-Trichlorobenzene ug/L ND 2.0 11/06/19 11:17
1,2,3-Trichloropropane ug/L ND 0.50 11/06/19 11:17
1,2,4-Trichlorobenzene ug/L ND 2.0 11/06/19 11:17
1,2,4-Trimethylbenzene ug/L ND 0.50 11/06/19 11:17
1,2-Dibromo-3-chloropropane ug/L ND 1.0 11/06/19 11:17
1,2-Dibromoethane (EDB)ug/L ND 0.50 11/06/19 11:17
1,2-Dichlorobenzene ug/L ND 0.50 11/06/19 11:17
1,2-Dichloroethane ug/L ND 0.50 11/06/19 11:17
1,2-Dichloropropane ug/L ND 0.50 11/06/19 11:17
1,3,5-Trimethylbenzene ug/L ND 0.50 11/06/19 11:17
1,3-Dichlorobenzene ug/L ND 0.50 11/06/19 11:17
1,3-Dichloropropane ug/L ND 0.50 11/06/19 11:17
1,4-Dichlorobenzene ug/L ND 0.50 11/06/19 11:17
2,2-Dichloropropane ug/L ND 0.50 11/06/19 11:17
2-Chlorotoluene ug/L ND 0.50 11/06/19 11:17
4-Chlorotoluene ug/L ND 0.50 11/06/19 11:17
Benzene ug/L ND 0.50 11/06/19 11:17
Bromobenzene ug/L ND 0.50 11/06/19 11:17
Bromochloromethane ug/L ND 0.50 11/06/19 11:17
Bromodichloromethane ug/L ND 0.50 11/06/19 11:17
Bromoform ug/L ND 0.50 11/06/19 11:17
Bromomethane ug/L ND 5.0 11/06/19 11:17
Carbon tetrachloride ug/L ND 0.50 11/06/19 11:17
Chlorobenzene ug/L ND 0.50 11/06/19 11:17
Chloroethane ug/L ND 1.0 11/06/19 11:17
Chloroform ug/L 1.5 0.50 11/06/19 11:17
Chloromethane ug/L ND 1.0 11/06/19 11:17
cis-1,2-Dichloroethene ug/L ND 0.50 11/06/19 11:17
cis-1,3-Dichloropropene ug/L ND 0.50 11/06/19 11:17
Dibromochloromethane ug/L ND 0.50 11/06/19 11:17
Dibromomethane ug/L ND 0.50 11/06/19 11:17
Dichlorodifluoromethane ug/L ND 0.50 11/06/19 11:17
Diisopropyl ether ug/L ND 0.50 11/06/19 11:17
Ethylbenzene ug/L ND 0.50 11/06/19 11:17
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/08/2019 03:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92451374
ALAMANCE OIL 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2726324
Associated Lab Samples:92451374002, 92451374003
Matrix: Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 2.0 11/06/19 11:17
Isopropylbenzene (Cumene)ug/L ND 0.50 11/06/19 11:17
m&p-Xylene ug/L ND 1.0 11/06/19 11:17
Methyl-tert-butyl ether ug/L ND 0.50 11/06/19 11:17
Methylene Chloride ug/L ND 2.0 11/06/19 11:17
n-Butylbenzene ug/L ND 0.50 11/06/19 11:17
n-Propylbenzene ug/L ND 0.50 11/06/19 11:17
Naphthalene ug/L ND 2.0 11/06/19 11:17
o-Xylene ug/L ND 0.50 11/06/19 11:17
sec-Butylbenzene ug/L ND 0.50 11/06/19 11:17
Styrene ug/L ND 0.50 11/06/19 11:17
tert-Butylbenzene ug/L ND 0.50 11/06/19 11:17
Tetrachloroethene ug/L ND 0.50 11/06/19 11:17
Toluene ug/L ND 0.50 11/06/19 11:17
trans-1,2-Dichloroethene ug/L ND 0.50 11/06/19 11:17
trans-1,3-Dichloropropene ug/L ND 0.50 11/06/19 11:17
Trichloroethene ug/L ND 0.50 11/06/19 11:17
Trichlorofluoromethane ug/L ND 1.0 11/06/19 11:17
Vinyl chloride ug/L ND 1.0 11/06/19 11:17
1,2-Dichloroethane-d4 (S)%94 70-130 11/06/19 11:17
4-Bromofluorobenzene (S)%99 70-130 11/06/19 11:17
Toluene-d8 (S)%101 70-130 11/06/19 11:17
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2726325LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 53.050 106 60-140
1,1,1-Trichloroethane ug/L 49.950 100 60-140
1,1,2,2-Tetrachloroethane ug/L 50.650 101 60-140
1,1,2-Trichloroethane ug/L 52.150 104 60-140
1,1-Dichloroethane ug/L 54.350 109 60-140
1,1-Dichloroethene ug/L 55.850 112 60-140
1,1-Dichloropropene ug/L 49.850 100 60-140
1,2,3-Trichlorobenzene ug/L 57.850 116 60-140
1,2,3-Trichloropropane ug/L 50.350 101 60-140
1,2,4-Trichlorobenzene ug/L 57.750 115 60-140
1,2,4-Trimethylbenzene ug/L 50.950 102 60-140
1,2-Dibromo-3-chloropropane ug/L 61.650 123 60-140
1,2-Dibromoethane (EDB)ug/L 52.850 106 60-140
1,2-Dichlorobenzene ug/L 51.250 102 60-140
1,2-Dichloroethane ug/L 45.250 90 60-140
1,2-Dichloropropane ug/L 56.650 113 60-140
1,3,5-Trimethylbenzene ug/L 50.850 102 60-140
1,3-Dichlorobenzene ug/L 49.450 99 60-140
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/08/2019 03:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92451374
ALAMANCE OIL 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2726325LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 53.650 107 60-140
1,4-Dichlorobenzene ug/L 49.650 99 60-140
2,2-Dichloropropane ug/L 55.650 111 60-140
2-Chlorotoluene ug/L 49.750 99 60-140
4-Chlorotoluene ug/L 49.750 99 60-140
Benzene ug/L 51.650 103 60-140
Bromobenzene ug/L 52.350 105 60-140
Bromochloromethane ug/L 53.550 107 60-140
Bromodichloromethane ug/L 54.650 109 60-140
Bromoform ug/L 52.550 105 60-140
Bromomethane ug/L 48.750 97 60-140
Carbon tetrachloride ug/L 50.950 102 60-140
Chlorobenzene ug/L 50.050 100 60-140
Chloroethane ug/L 50.050 100 60-140
Chloroform ug/L 54.750 109 60-140
Chloromethane ug/L 35.650 71 60-140
cis-1,2-Dichloroethene ug/L 54.150 108 60-140
cis-1,3-Dichloropropene ug/L 65.450 131 60-140
Dibromochloromethane ug/L 53.150 106 60-140
Dibromomethane ug/L 57.150 114 60-140
Dichlorodifluoromethane ug/L 44.150 88 60-140
Diisopropyl ether ug/L 56.150 112 60-140
Ethylbenzene ug/L 50.550 101 60-140
Hexachloro-1,3-butadiene ug/L 57.850 116 60-140
Isopropylbenzene (Cumene)ug/L 52.950 106 60-140
m&p-Xylene ug/L 102100 102 60-140
Methyl-tert-butyl ether ug/L 59.150 118 60-140
Methylene Chloride ug/L 54.450 109 60-140
n-Butylbenzene ug/L 52.150 104 60-140
n-Propylbenzene ug/L 50.650 101 60-140
Naphthalene ug/L 57.250 114 60-140
o-Xylene ug/L 52.050 104 60-140
sec-Butylbenzene ug/L 51.650 103 60-140
Styrene ug/L 52.550 105 60-140
tert-Butylbenzene ug/L 42.950 86 60-140
Tetrachloroethene ug/L 57.250 114 60-140
Toluene ug/L 57.450 115 60-140
trans-1,2-Dichloroethene ug/L 55.550 111 60-140
trans-1,3-Dichloropropene ug/L 54.950 110 60-140
Trichloroethene ug/L 51.850 104 60-140
Trichlorofluoromethane ug/L 52.750 105 60-140
Vinyl chloride ug/L 46.150 92 60-140
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%113 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/08/2019 03:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92451374
ALAMANCE OIL 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2726326MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92451820004
2726327
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 1000 111 60-140108 21000<21.1 1110 1080
1,1,1-Trichloroethane ug/L 1000 118 60-140111 51000<13.9 1180 1110
1,1,2,2-Tetrachloroethane ug/L 1000 105 60-14099 61000<9.6 1050 988
1,1,2-Trichloroethane ug/L 1000 119 60-140113 51000<11.6 1190 1130
1,1-Dichloroethane ug/L 1000 118 60-140108 91000<12.2 1180 1080
1,1-Dichloroethene ug/L 1000 126 60-140116 81000<10.9 1260 1160
1,1-Dichloropropene ug/L 1000 117 60-140112 51000<17.4 1170 1120
1,2,3-Trichlorobenzene ug/L 1000 96 60-140110 141000<39.0 958 1100
1,2,3-Trichloropropane ug/L 1000 113 60-140103 91000<13.6 1130 1030
1,2,4-Trichlorobenzene ug/L 1000 101 60-140107 61000<21.8 1010 1070
1,2,4-Trimethylbenzene ug/L 1000 119 60-14099 8100014802670 2470
1,2-Dibromo-3-chloropropane ug/L 1000 110 60-140114 31000<19.2 1100 1140
1,2-Dibromoethane (EDB)ug/L 1000 111 60-140109 21000<11.6 1110 1090
1,2-Dichlorobenzene ug/L 1000 106 60-140102 41000<12.0 1060 1020
1,2-Dichloroethane ug/L 1000 106 60-14098 81000<13.2 1060 980
1,2-Dichloropropane ug/L 1000 115 60-140115 01000<9.2 1150 1150
1,3,5-Trimethylbenzene ug/L 1000 115 60-14096 1410003831540 1340
1,3-Dichlorobenzene ug/L 1000 104 60-140101 31000<12.5 1040 1010
1,3-Dichloropropane ug/L 1000 112 60-140110 21000<17.0 1120 1100
1,4-Dichlorobenzene ug/L 1000 102 60-14099 41000<12.4 1020 985
2,2-Dichloropropane ug/L 1000 106 60-140100 61000<14.0 1060 1000
2-Chlorotoluene ug/L 1000 114 60-140103 101000<10.4 1140 1030
4-Chlorotoluene ug/L 1000 105 60-14098 71000<10.3 1050 980
Benzene ug/L 1000 118 60-140109 510005161690 1610
Bromobenzene ug/L 1000 115 60-140105 91000<10.8 1150 1050
Bromochloromethane ug/L 1000 110 60-140104 61000<12.9 1100 1040
Bromodichloromethane ug/L 1000 122 60-140118 31000<9.2 1220 1180
Bromoform ug/L 1000 113 60-140107 51000<20.2 1130 1070
Bromomethane ug/L 1000 69 60-14069 01000<86.0 691 692
Carbon tetrachloride ug/L 1000 116 60-140113 21000<11.6 1160 1130
Chlorobenzene ug/L 1000 108 60-140105 31000<11.2 1080 1050
Chloroethane ug/L 1000 123 60-140114 71000<29.2 1230 1140
Chloroform ug/L 1000 116 60-140106 8100096.6 1260 1160
Chloromethane ug/L 1000 101 60-140100 11000<20.8 1010 998
cis-1,2-Dichloroethene ug/L 1000 116 60-140107 81000<10.4 1160 1070
cis-1,3-Dichloropropene ug/L 1000 120 60-140112 71000<17.8 1200 1120
Dibromochloromethane ug/L 1000 117 60-140113 31000<20.1 1170 1130
Dibromomethane ug/L 1000 111 60-140106 41000<15.5 1110 1060
Dichlorodifluoromethane ug/L 1000 124 60-140103 181000<14.2 1240 1030
Diisopropyl ether ug/L 1000 112 60-140103 91000<16.7 1120 1030
Ethylbenzene ug/L 1000 106 60-14096 5100010902150 2050
Hexachloro-1,3-butadiene ug/L 1000 108 60-140105 31000<60.0 1080 1050
Isopropylbenzene (Cumene) ug/L 1000 119 60-140106 11100059.3 1250 1120
m&p-Xylene ug/L 2000 102 60-14087 5200041606190 5910
Methyl-tert-butyl ether ug/L 1000 109 60-140108 11000<22.2 1090 1080
Methylene Chloride ug/L 1000 103 60-14095 81000<75.0 1030 948
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/08/2019 03:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92451374
ALAMANCE OIL 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2726326MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92451820004
2726327
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L 1000 110 60-140109 11000<17.6 1100 1090
n-Propylbenzene ug/L 1000 114 60-14099 1210001821320 1170
Naphthalene ug/L 1000 96 60-140107 810003711330 1440
o-Xylene ug/L 1000 99 60-14079 7100019702960 2760
sec-Butylbenzene ug/L 1000 113 60-140111 31000<12.3 1130 1110
Styrene ug/L 1000 114 60-140106 81000<12.8 1140 1060
tert-Butylbenzene ug/L 1000 93 60-14099 61000<12.5 933 993
Tetrachloroethene ug/L 1000 116 60-140114 21000<11.6 1160 1140
Toluene ug/L M110009760-14055 6100058506820 6400
trans-1,2-Dichloroethene ug/L 1000 108 60-140105 31000<12.8 1080 1050
trans-1,3-Dichloropropene ug/L 1000 109 60-140111 21000<19.7 1090 1110
Trichloroethene ug/L 1000 120 60-140114 51000<11.6 1200 1140
Trichlorofluoromethane ug/L 1000 127 60-140120 51000<16.8 1270 1200
Vinyl chloride ug/L 1000 125 60-140116 81000<20.4 1250 1160
1,2-Dichloroethane-d4 (S)%93 70-13098
4-Bromofluorobenzene (S)%105 70-13098
Toluene-d8 (S)%99 70-13097
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/08/2019 03:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92451374
ALAMANCE OIL 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
508198
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples: 92451374004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2728046
Associated Lab Samples:92451374004
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 11/07/19 11:38
1,1,1-Trichloroethane ug/L ND 0.50 11/07/19 11:38
1,1,2,2-Tetrachloroethane ug/L ND 0.50 11/07/19 11:38
1,1,2-Trichloroethane ug/L ND 0.50 11/07/19 11:38
1,1-Dichloroethane ug/L ND 0.50 11/07/19 11:38
1,1-Dichloroethene ug/L ND 0.50 11/07/19 11:38
1,1-Dichloropropene ug/L ND 0.50 11/07/19 11:38
1,2,3-Trichlorobenzene ug/L ND 2.0 11/07/19 11:38
1,2,3-Trichloropropane ug/L ND 0.50 11/07/19 11:38
1,2,4-Trichlorobenzene ug/L ND 2.0 11/07/19 11:38
1,2,4-Trimethylbenzene ug/L ND 0.50 11/07/19 11:38
1,2-Dibromo-3-chloropropane ug/L ND 1.0 11/07/19 11:38
1,2-Dibromoethane (EDB)ug/L ND 0.50 11/07/19 11:38
1,2-Dichlorobenzene ug/L ND 0.50 11/07/19 11:38
1,2-Dichloroethane ug/L ND 0.50 11/07/19 11:38
1,2-Dichloropropane ug/L ND 0.50 11/07/19 11:38
1,3,5-Trimethylbenzene ug/L ND 0.50 11/07/19 11:38
1,3-Dichlorobenzene ug/L ND 0.50 11/07/19 11:38
1,3-Dichloropropane ug/L ND 0.50 11/07/19 11:38
1,4-Dichlorobenzene ug/L ND 0.50 11/07/19 11:38
2,2-Dichloropropane ug/L ND 0.50 11/07/19 11:38
2-Chlorotoluene ug/L ND 0.50 11/07/19 11:38
4-Chlorotoluene ug/L ND 0.50 11/07/19 11:38
Benzene ug/L ND 0.50 11/07/19 11:38
Bromobenzene ug/L ND 0.50 11/07/19 11:38
Bromochloromethane ug/L ND 0.50 11/07/19 11:38
Bromodichloromethane ug/L ND 0.50 11/07/19 11:38
Bromoform ug/L ND 0.50 11/07/19 11:38
Bromomethane ug/L ND 5.0 11/07/19 11:38
Carbon tetrachloride ug/L ND 0.50 11/07/19 11:38
Chlorobenzene ug/L ND 0.50 11/07/19 11:38
Chloroethane ug/L ND 1.0 11/07/19 11:38
Chloroform ug/L ND 0.50 11/07/19 11:38
Chloromethane ug/L ND 1.0 11/07/19 11:38
cis-1,2-Dichloroethene ug/L ND 0.50 11/07/19 11:38
cis-1,3-Dichloropropene ug/L ND 0.50 11/07/19 11:38
Dibromochloromethane ug/L ND 0.50 11/07/19 11:38
Dibromomethane ug/L ND 0.50 11/07/19 11:38
Dichlorodifluoromethane ug/L ND 0.50 11/07/19 11:38
Diisopropyl ether ug/L ND 0.50 11/07/19 11:38
Ethylbenzene ug/L ND 0.50 11/07/19 11:38
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/08/2019 03:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92451374
ALAMANCE OIL 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2728046
Associated Lab Samples:92451374004
Matrix: Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 2.0 11/07/19 11:38
Isopropylbenzene (Cumene)ug/L ND 0.50 11/07/19 11:38
m&p-Xylene ug/L ND 1.0 11/07/19 11:38
Methyl-tert-butyl ether ug/L ND 0.50 11/07/19 11:38
Methylene Chloride ug/L ND 2.0 11/07/19 11:38
n-Butylbenzene ug/L ND 0.50 11/07/19 11:38
n-Propylbenzene ug/L ND 0.50 11/07/19 11:38
Naphthalene ug/L ND 2.0 11/07/19 11:38
o-Xylene ug/L ND 0.50 11/07/19 11:38
sec-Butylbenzene ug/L ND 0.50 11/07/19 11:38
Styrene ug/L ND 0.50 11/07/19 11:38
tert-Butylbenzene ug/L ND 0.50 11/07/19 11:38
Tetrachloroethene ug/L ND 0.50 11/07/19 11:38
Toluene ug/L ND 0.50 11/07/19 11:38
trans-1,2-Dichloroethene ug/L ND 0.50 11/07/19 11:38
trans-1,3-Dichloropropene ug/L ND 0.50 11/07/19 11:38
Trichloroethene ug/L ND 0.50 11/07/19 11:38
Trichlorofluoromethane ug/L ND 1.0 11/07/19 11:38
Vinyl chloride ug/L ND 1.0 11/07/19 11:38
1,2-Dichloroethane-d4 (S)%93 70-130 11/07/19 11:38
4-Bromofluorobenzene (S)%91 70-130 11/07/19 11:38
Toluene-d8 (S)%104 70-130 11/07/19 11:38
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2728047LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 52.350 105 60-140
1,1,1-Trichloroethane ug/L 56.350 113 60-140
1,1,2,2-Tetrachloroethane ug/L 48.350 97 60-140
1,1,2-Trichloroethane ug/L 57.650 115 60-140
1,1-Dichloroethane ug/L 54.250 108 60-140
1,1-Dichloroethene ug/L 56.950 114 60-140
1,1-Dichloropropene ug/L 60.350 121 60-140
1,2,3-Trichlorobenzene ug/L 60.150 120 60-140
1,2,3-Trichloropropane ug/L 50.150 100 60-140
1,2,4-Trichlorobenzene ug/L 58.150 116 60-140
1,2,4-Trimethylbenzene ug/L 50.050 100 60-140
1,2-Dibromo-3-chloropropane ug/L 62.550 125 60-140
1,2-Dibromoethane (EDB)ug/L 55.750 111 60-140
1,2-Dichlorobenzene ug/L 51.350 103 60-140
1,2-Dichloroethane ug/L 46.650 93 60-140
1,2-Dichloropropane ug/L 57.750 115 60-140
1,3,5-Trimethylbenzene ug/L 51.150 102 60-140
1,3-Dichlorobenzene ug/L 49.750 99 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/08/2019 03:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92451374
ALAMANCE OIL 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2728047LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 56.850 114 60-140
1,4-Dichlorobenzene ug/L 49.050 98 60-140
2,2-Dichloropropane ug/L 58.150 116 60-140
2-Chlorotoluene ug/L 50.450 101 60-140
4-Chlorotoluene ug/L 50.050 100 60-140
Benzene ug/L 51.350 103 60-140
Bromobenzene ug/L 52.150 104 60-140
Bromochloromethane ug/L 54.450 109 60-140
Bromodichloromethane ug/L 59.950 120 60-140
Bromoform ug/L 51.750 103 60-140
Bromomethane ug/L 45.050 90 60-140
Carbon tetrachloride ug/L 54.350 109 60-140
Chlorobenzene ug/L 49.950 100 60-140
Chloroethane ug/L 51.250 102 60-140
Chloroform ug/L 56.050 112 60-140
Chloromethane ug/L 38.150 76 60-140
cis-1,2-Dichloroethene ug/L 56.450 113 60-140
cis-1,3-Dichloropropene ug/L 56.950 114 60-140
Dibromochloromethane ug/L 55.150 110 60-140
Dibromomethane ug/L 57.950 116 60-140
Dichlorodifluoromethane ug/L 47.450 95 60-140
Diisopropyl ether ug/L 52.850 106 60-140
Ethylbenzene ug/L 49.950 100 60-140
Hexachloro-1,3-butadiene ug/L 61.750 123 60-140
Isopropylbenzene (Cumene)ug/L 51.150 102 60-140
m&p-Xylene ug/L 99.3100 99 60-140
Methyl-tert-butyl ether ug/L 54.150 108 60-140
Methylene Chloride ug/L 45.350 91 60-140
n-Butylbenzene ug/L 53.950 108 60-140
n-Propylbenzene ug/L 50.750 101 60-140
Naphthalene ug/L 60.050 120 60-140
o-Xylene ug/L 50.850 102 60-140
sec-Butylbenzene ug/L 51.950 104 60-140
Styrene ug/L 50.550 101 60-140
tert-Butylbenzene ug/L 43.550 87 60-140
Tetrachloroethene ug/L 54.750 109 60-140
Toluene ug/L 48.250 96 60-140
trans-1,2-Dichloroethene ug/L 49.850 100 60-140
trans-1,3-Dichloropropene ug/L 52.850 106 60-140
Trichloroethene ug/L 56.350 113 60-140
Trichlorofluoromethane ug/L 57.650 115 60-140
Vinyl chloride ug/L 53.050 106 60-140
1,2-Dichloroethane-d4 (S)%96 70-130
4-Bromofluorobenzene (S)%96 70-130
Toluene-d8 (S)%93 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/08/2019 03:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92451374
ALAMANCE OIL 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2728048MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92451954003
2728049
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 5000 105 60-140107 15000ND5270 5350
1,1,1-Trichloroethane ug/L 5000 122 60-140106 145000ND6090 5320
1,1,2,2-Tetrachloroethane ug/L 5000 96 60-140100 45000ND4800 4980
1,1,2-Trichloroethane ug/L 5000 102 60-140106 45000ND5090 5280
1,1-Dichloroethane ug/L 5000 114 60-140102 115000ND5690 5100
1,1-Dichloroethene ug/L 5000 119 60-14099 195000ND5970 4930
1,1-Dichloropropene ug/L 5000 115 60-140106 85000ND5730 5310
1,2,3-Trichlorobenzene ug/L 5000 99 60-14089 115000ND4960 4460
1,2,3-Trichloropropane ug/L 5000 99 60-140102 35000ND4940 5110
1,2,4-Trichlorobenzene ug/L 5000 104 60-14089 165000ND5220 4450
1,2,4-Trimethylbenzene ug/L 5000 98 60-14084 11500016306540 5850
1,2-Dibromo-3-chloropropane ug/L 5000 104 60-14091 145000ND5210 4550
1,2-Dibromoethane (EDB)ug/L 5000 108 60-140112 350005465930 6140
1,2-Dichlorobenzene ug/L 5000 101 60-140101 05000ND5030 5030
1,2-Dichloroethane ug/L 5000 95 60-14092 350002795030 4870
1,2-Dichloropropane ug/L 5000 96 60-14092 55000ND4810 4600
1,3,5-Trimethylbenzene ug/L 5000 98 60-14088 1050004055280 4790
1,3-Dichlorobenzene ug/L 5000 97 60-14091 65000ND4830 4530
1,3-Dichloropropane ug/L 5000 110 60-140110 05000ND5520 5510
1,4-Dichlorobenzene ug/L 5000 96 60-14097 25000ND4790 4870
2,2-Dichloropropane ug/L 5000 100 60-14092 85000ND4990 4620
2-Chlorotoluene ug/L 5000 100 60-14089 125000ND4990 4440
4-Chlorotoluene ug/L 5000 97 60-14087 115000ND4860 4340
Benzene ug/L 5000 66 60-140126 235000867011900 15000
Bromobenzene ug/L 5000 101 60-14089 125000ND5030 4450
Bromochloromethane ug/L 5000 111 60-140101 95000ND5530 5040
Bromodichloromethane ug/L 5000 103 60-140100 25000ND5130 5010
Bromoform ug/L 5000 102 60-140108 55000ND5120 5380
Bromomethane ug/L M150004060-14044 85000ND2000 2180
Carbon tetrachloride ug/L 5000 115 60-140120 45000ND5740 5980
Chlorobenzene ug/L 5000 100 60-140101 25000ND4980 5060
Chloroethane ug/L 5000 104 60-14099 55000ND5210 4950
Chloroform ug/L 5000 109 60-140101 75000ND5470 5070
Chloromethane ug/L M150006860-14057 175000ND3400 2870
cis-1,2-Dichloroethene ug/L 5000 104 60-140101 35000ND5190 5060
cis-1,3-Dichloropropene ug/L 5000 115 60-14098 165000ND5770 4890
Dibromochloromethane ug/L 5000 116 60-140114 15000ND5790 5710
Dibromomethane ug/L 5000 99 60-14093 65000ND4940 4650
Dichlorodifluoromethane ug/L 5000 99 60-14085 155000ND4940 4250
Diisopropyl ether ug/L 5000 114 60-14085 295000ND5700 4240
Ethylbenzene ug/L 5000 97 60-140101 3500017106580 6750
Hexachloro-1,3-butadiene ug/L 5000 108 60-14095 135000ND5410 4770
Isopropylbenzene (Cumene) ug/L 5000 106 60-140110 45000ND5290 5500
m&p-Xylene ug/L 10000 97 60-140102 310000733017000 17500
Methyl-tert-butyl ether ug/L 5000 105 60-14090 165000ND5270 4480
Methylene Chloride ug/L 5000 104 60-14084 195000ND5540 4570
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/08/2019 03:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92451374
ALAMANCE OIL 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2728048MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92451954003
2728049
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L 5000 98 60-14088 105000ND4900 4420
n-Propylbenzene ug/L 5000 98 60-14086 1250002225100 4520
Naphthalene ug/L 5000 96 60-14094 25000ND5020 4910
o-Xylene ug/L 5000 99 60-140105 3500044809430 9730
sec-Butylbenzene ug/L 5000 103 60-14095 95000ND5160 4740
Styrene ug/L 5000 101 60-140106 45000ND5070 5280
tert-Butylbenzene ug/L 5000 86 60-14077 105000ND4290 3860
Tetrachloroethene ug/L 5000 122 60-140110 105000ND6090 5510
Toluene ug/L M1500012260-140-10 1850003390040000 33400
trans-1,2-Dichloroethene ug/L 5000 104 60-14089 155000ND5180 4460
trans-1,3-Dichloropropene ug/L 5000 101 60-14094 75000ND5060 4710
Trichloroethene ug/L 5000 104 60-140114 95000ND5210 5690
Trichlorofluoromethane ug/L 5000 123 60-140104 175000ND6160 5220
Vinyl chloride ug/L 5000 105 60-14090 155000ND5230 4490
1,2-Dichloroethane-d4 (S)%96 70-13098
4-Bromofluorobenzene (S)%99 70-130102
Toluene-d8 (S)%103 70-13090
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/08/2019 03:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92451374
ALAMANCE OIL 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
507098
EPA 504.1
EPA 504.1
GCS 504 EDB DBCP
Associated Lab Samples: 92451374002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2722740
Associated Lab Samples:92451374002
Matrix: Water
Analyzed
1,2-Dibromoethane (EDB)ug/L ND 0.020 11/01/19 20:23
1-Chloro-2-bromopropane (S)%99 70-130 11/01/19 20:23
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2722741LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2722742
1,2-Dibromoethane (EDB)ug/L 0.230.25 93 70-130970.24 4 20
1-Chloro-2-bromopropane (S)%97 70-13099
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2722744MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92451221002
2722745
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,2-Dibromoethane (EDB)ug/L 0.24 97 65-13595 10.24ND 0.23 0.23
1-Chloro-2-bromopropane (S) %101 70-13099
Parameter Units
Dup
Result QualifiersRPDResult
92451221001
2722743SAMPLE DUPLICATE:
1,2-Dibromoethane (EDB)ug/L NDND
1-Chloro-2-bromopropane (S)%10796
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/08/2019 03:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92451374
ALAMANCE OIL 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
508141
EPA 504.1
EPA 504.1
GCS 504 EDB DBCP
Associated Lab Samples: 92451374003, 92451374004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2727759
Associated Lab Samples:92451374003, 92451374004
Matrix: Water
Analyzed
1,2-Dibromoethane (EDB)ug/L ND 0.020 11/07/19 14:06
1-Chloro-2-bromopropane (S)%98 70-130 11/07/19 14:06
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2727760LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2727761
1,2-Dibromoethane (EDB)ug/L 0.230.25 94 70-130960.24 3 20
1-Chloro-2-bromopropane (S)%94 70-13096
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2727763MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92452094004
2727764
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,2-Dibromoethane (EDB)ug/L 0.26 95 65-13599 10.25ND 0.24 0.25
1-Chloro-2-bromopropane (S) %94 70-13098
Parameter Units
Dup
Result QualifiersRPDResult
92452094003
2727762SAMPLE DUPLICATE:
1,2-Dibromoethane (EDB)ug/L NDND
1-Chloro-2-bromopropane (S)%96104
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/08/2019 03:47 PM
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Page 31 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92451374
ALAMANCE OIL 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
507167
EPA 625.1
EPA 625.1
625 MSS
Associated Lab Samples: 92451374001, 92451374002, 92451374003, 92451374004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2722988
Associated Lab Samples:92451374001, 92451374002, 92451374003, 92451374004
Matrix: Water
Analyzed
1,2,4-Trichlorobenzene ug/L ND 5.0 11/04/19 10:01
2,4,6-Trichlorophenol ug/L ND 10.0 11/04/19 10:01
2,4-Dichlorophenol ug/L ND 5.0 11/04/19 10:01
2,4-Dimethylphenol ug/L ND 10.0 11/04/19 10:01
2,4-Dinitrophenol ug/L ND 50.0 11/04/19 10:01
2,4-Dinitrotoluene ug/L ND 5.0 11/04/19 10:01
2,6-Dinitrotoluene ug/L ND 5.0 11/04/19 10:01
2-Chloronaphthalene ug/L ND 5.0 11/04/19 10:01
2-Chlorophenol ug/L ND 5.0 11/04/19 10:01
2-Nitrophenol ug/L ND 5.0 11/04/19 10:01
3,3'-Dichlorobenzidine ug/L ND 25.0 11/04/19 10:01
4,6-Dinitro-2-methylphenol ug/L ND 20.0 11/04/19 10:01
4-Bromophenylphenyl ether ug/L ND 5.0 11/04/19 10:01
4-Chloro-3-methylphenol ug/L ND 5.0 11/04/19 10:01
4-Chlorophenylphenyl ether ug/L ND 5.0 11/04/19 10:01
4-Nitrophenol ug/L ND 50.0 11/04/19 10:01
Acenaphthene ug/L ND 5.0 11/04/19 10:01
Acenaphthylene ug/L ND 5.0 11/04/19 10:01
Anthracene ug/L ND 5.0 11/04/19 10:01
Benzo(a)anthracene ug/L ND 5.0 11/04/19 10:01
Benzo(a)pyrene ug/L ND 5.0 11/04/19 10:01
Benzo(b)fluoranthene ug/L ND 5.0 11/04/19 10:01
Benzo(g,h,i)perylene ug/L ND 5.0 11/04/19 10:01
Benzo(k)fluoranthene ug/L ND 5.0 11/04/19 10:01
bis(2-Chloroethoxy)methane ug/L ND 10.0 11/04/19 10:01
bis(2-Chloroethyl) ether ug/L ND 5.0 11/04/19 10:01
bis(2-Ethylhexyl)phthalate ug/L ND 5.0 11/04/19 10:01
Butylbenzylphthalate ug/L ND 5.0 11/04/19 10:01
Chrysene ug/L ND 5.0 11/04/19 10:01
Di-n-butylphthalate ug/L ND 5.0 11/04/19 10:01
Di-n-octylphthalate ug/L ND 5.0 11/04/19 10:01
Dibenz(a,h)anthracene ug/L ND 5.0 11/04/19 10:01
Diethylphthalate ug/L ND 5.0 11/04/19 10:01
Dimethylphthalate ug/L ND 5.0 11/04/19 10:01
Fluoranthene ug/L ND 5.0 11/04/19 10:01
Fluorene ug/L ND 5.0 11/04/19 10:01
Hexachloro-1,3-butadiene ug/L ND 5.0 11/04/19 10:01
Hexachlorobenzene ug/L ND 5.0 11/04/19 10:01
Hexachlorocyclopentadiene ug/L ND 10.0 11/04/19 10:01
Hexachloroethane ug/L ND 5.0 11/04/19 10:01
Indeno(1,2,3-cd)pyrene ug/L ND 5.0 11/04/19 10:01
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/08/2019 03:47 PM
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Huntersville, NC 28078
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Page 32 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92451374
ALAMANCE OIL 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2722988
Associated Lab Samples:92451374001, 92451374002, 92451374003, 92451374004
Matrix: Water
Analyzed
Isophorone ug/L ND 10.0 11/04/19 10:01
N-Nitroso-di-n-propylamine ug/L ND 5.0 11/04/19 10:01
N-Nitrosodimethylamine ug/L ND 5.0 11/04/19 10:01
N-Nitrosodiphenylamine ug/L ND 10.0 11/04/19 10:01
Naphthalene ug/L ND 5.0 11/04/19 10:01
Nitrobenzene ug/L ND 5.0 11/04/19 10:01
Pentachlorophenol ug/L ND 10.0 11/04/19 10:01
Phenanthrene ug/L ND 5.0 11/04/19 10:01
Phenol ug/L ND 5.0 11/04/19 10:01
Pyrene ug/L ND 5.0 11/04/19 10:01
2,4,6-Tribromophenol (S)%66 10-137 11/04/19 10:01
2-Fluorobiphenyl (S)%60 15-120 11/04/19 10:01
2-Fluorophenol (S)%64 10-120 11/04/19 10:01
Nitrobenzene-d5 (S)%58 10-120 11/04/19 10:01
Phenol-d6 (S)%66 10-120 11/04/19 10:01
Terphenyl-d14 (S)%64 11-131 11/04/19 10:01
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2722989LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 36.950 74 44-142
2,4,6-Trichlorophenol ug/L 38.650 77 37-144
2,4-Dichlorophenol ug/L 39.650 79 1-191
2,4-Dimethylphenol ug/L 30.750 61 32-119
2,4-Dinitrophenol ug/L 332250 133 1-181
2,4-Dinitrotoluene ug/L 55.850 112 39-139
2,6-Dinitrotoluene ug/L 50.950 102 50-158
2-Chloronaphthalene ug/L 40.050 80 60-118
2-Chlorophenol ug/L 40.450 81 23-134
2-Nitrophenol ug/L 47.550 95 29-182
3,3'-Dichlorobenzidine ug/L 52.9100 53 1-262
4,6-Dinitro-2-methylphenol ug/L 140100 140 1-181
4-Bromophenylphenyl ether ug/L 44.150 88 53-127
4-Chloro-3-methylphenol ug/L 79.2100 79 22-147
4-Chlorophenylphenyl ether ug/L 41.750 83 25-158
4-Nitrophenol ug/L 184250 74 1-132
Acenaphthene ug/L 40.650 81 47-145
Acenaphthylene ug/L 44.450 89 33-145
Anthracene ug/L 46.250 92 1-166
Benzo(a)anthracene ug/L 50.550 101 33-143
Benzo(a)pyrene ug/L 49.650 99 17-163
Benzo(b)fluoranthene ug/L 54.350 109 24-159
Benzo(g,h,i)perylene ug/L 51.450 103 1-219
Benzo(k)fluoranthene ug/L 56.150 112 11-162
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/08/2019 03:47 PM
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Huntersville, NC 28078
[phone]
Page 33 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92451374
ALAMANCE OIL 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2722989LABORATORY CONTROL SAMPLE:
LCSSpike
bis(2-Chloroethoxy)methane ug/L 40.750 81 33-184
bis(2-Chloroethyl) ether ug/L 41.650 83 12-158
bis(2-Ethylhexyl)phthalate ug/L 52.750 105 8-158
Butylbenzylphthalate ug/L 51.650 103 1-152
Chrysene ug/L 49.250 98 17-168
Di-n-butylphthalate ug/L 51.850 104 1-118
Di-n-octylphthalate ug/L 53.450 107 4-146
Dibenz(a,h)anthracene ug/L 52.150 104 1-227
Diethylphthalate ug/L 49.650 99 1-114
Dimethylphthalate ug/L 46.650 93 1-112
Fluoranthene ug/L 52.950 106 26-137
Fluorene ug/L 45.850 92 59-121
Hexachloro-1,3-butadiene ug/L 34.850 70 24-116
Hexachlorobenzene ug/L 46.250 92 1-152
Hexachlorocyclopentadiene ug/L 41.650 83 25-150
Hexachloroethane ug/L 35.150 70 40-113
Indeno(1,2,3-cd)pyrene ug/L 51.550 103 1-171
Isophorone ug/L 40.950 82 21-196
N-Nitroso-di-n-propylamine ug/L 41.550 83 1-230
N-Nitrosodimethylamine ug/L 36.150 72 25-150
N-Nitrosodiphenylamine ug/L 19.450 39 25-150
Naphthalene ug/L 41.450 83 21-133
Nitrobenzene ug/L 43.850 88 35-180
Pentachlorophenol ug/L 94.6100 95 14-176
Phenanthrene ug/L 50.650 101 54-120
Phenol ug/L 25.850 52 5-112
Pyrene ug/L 50.550 101 52-115
2,4,6-Tribromophenol (S)%96 10-137
2-Fluorobiphenyl (S)%75 15-120
2-Fluorophenol (S)%67 10-120
Nitrobenzene-d5 (S)%77 10-120
Phenol-d6 (S)%51 10-120
Terphenyl-d14 (S)%85 11-131
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2722990MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92448559013
2722991
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L 50 62 44-14266 650ND30.8 32.8
2,4,6-Trichlorophenol ug/L 50 86 37-14472 1750ND43.1 36.2
2,4-Dichlorophenol ug/L 50 83 1-19174 1250ND41.6 36.8
2,4-Dimethylphenol ug/L 50 79 32-11971 1150ND39.6 35.6
2,4-Dinitrophenol ug/L 250 108 1-1816250ND271 ND
2,4-Dinitrotoluene ug/L 50 100 39-13984 1750ND50.1 42.2
2,6-Dinitrotoluene ug/L 50 94 50-15884 1150ND47.0 42.0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/08/2019 03:47 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92451374
ALAMANCE OIL 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2722990MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92448559013
2722991
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
2-Chloronaphthalene ug/L 50 77 60-11871 750ND38.4 35.6
2-Chlorophenol ug/L 50 81 23-13474 950ND40.5 36.9
2-Nitrophenol ug/L 50 92 29-18282 1250ND46.2 41.0
3,3'-Dichlorobenzidine ug/L 100 89 1-26279 11100ND88.6 79.4
4,6-Dinitro-2-methylphenol ug/L R11001241-18151 83100ND124 51.5
4-Bromophenylphenyl ether ug/L 50 81 53-12772 1150ND40.3 36.1
4-Chloro-3-methylphenol ug/L 100 87 22-14777 12100ND86.5 77.1
4-Chlorophenylphenyl ether ug/L 50 81 25-15872 1250ND40.5 35.9
4-Nitrophenol ug/L R1250591-13221 97250ND147 51.3
Acenaphthene ug/L 50 83 47-14574 1150ND41.5 37.2
Acenaphthylene ug/L 50 87 33-14579 1150ND43.7 39.3
Anthracene ug/L 50 95 1-16684 1350ND47.4 41.8
Benzo(a)anthracene ug/L 50 93 33-14383 1150ND46.7 41.7
Benzo(a)pyrene ug/L 50 101 17-16388 1450ND50.6 44.1
Benzo(b)fluoranthene ug/L 50 99 24-15987 1350ND49.5 43.5
Benzo(g,h,i)perylene ug/L 50 101 1-21983 1950ND50.5 41.7
Benzo(k)fluoranthene ug/L 50 103 11-16291 1250ND51.6 45.7
bis(2-Chloroethoxy)methane ug/L 50 79 33-18470 1350ND39.6 34.8
bis(2-Chloroethyl) ether ug/L 50 79 12-15871 1150ND39.6 35.5
bis(2-Ethylhexyl)phthalate ug/L 50 97 8-15888 1050ND48.6 43.8
Butylbenzylphthalate ug/L 50 95 1-15286 1050ND47.3 42.9
Chrysene ug/L 50 89 17-16879 1250ND44.7 39.6
Di-n-butylphthalate ug/L 50 94 1-11882 1350ND46.8 41.2
Di-n-octylphthalate ug/L 50 98 4-14688 1150ND49.1 44.0
Dibenz(a,h)anthracene ug/L 50 100 1-22784 1850ND50.0 42.0
Diethylphthalate ug/L 50 89 1-11477 1550ND44.7 38.6
Dimethylphthalate ug/L 50 85 1-11274 1450ND42.5 37.1
Fluoranthene ug/L 50 93 26-13781 1450ND46.6 40.7
Fluorene ug/L 50 87 59-12177 1250ND43.7 38.6
Hexachloro-1,3-butadiene ug/L 50 60 24-11664 650ND30.0 31.9
Hexachlorobenzene ug/L 50 85 1-15276 1250ND42.6 37.9
Hexachlorocyclopentadiene ug/L 50 79 25-15080 250ND39.3 40.2
Hexachloroethane ug/L 50 57 40-11363 1050ND28.5 31.6
Indeno(1,2,3-cd)pyrene ug/L 50 99 1-17184 1750ND49.7 41.8
Isophorone ug/L 50 82 21-19672 1350ND41.2 36.2
N-Nitroso-di-n-propylamine ug/L 50 81 1-23074 1050ND40.6 36.8
N-Nitrosodimethylamine ug/L 50 68 25-15063 850ND34.1 31.5
N-Nitrosodiphenylamine ug/L 50 85 25-15075 1250ND42.4 37.5
Naphthalene ug/L 50 71 21-13372 050ND35.6 35.8
Nitrobenzene ug/L 50 82 35-18075 1050ND41.1 37.3
Pentachlorophenol ug/L R11009514-17666 36100ND95.4 66.1
Phenanthrene ug/L 50 91 54-12079 1450ND45.3 39.6
Phenol ug/L 50 49 5-11247 550ND24.6 23.3
Pyrene ug/L 50 95 52-11585 1150ND47.4 42.4
2,4,6-Tribromophenol (S)%99 10-13795
2-Fluorobiphenyl (S)%56 15-12069
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/08/2019 03:47 PM
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Huntersville, NC 28078
[phone]
Page 35 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92451374
ALAMANCE OIL 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2722990MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92448559013
2722991
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
2-Fluorophenol (S)%63 10-12064
Nitrobenzene-d5 (S)%70 10-12073
Phenol-d6 (S)%47 10-12049
Terphenyl-d14 (S)%76 11-13176
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/08/2019 03:47 PM
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Huntersville, NC 28078
[phone]
Page 36 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92451374
ALAMANCE OIL 2019-210
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
507107
MADEP EPH
MADEP EPH
MADEP EPH NC Water
Associated Lab Samples: 92451374002, 92451374003, 92451374004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2722755
Associated Lab Samples:92451374002, 92451374003, 92451374004
Matrix: Water
Analyzed
Aliphatic (C09-C18)ug/L ND 100 N211/04/19 15:21
Aliphatic (C19-C36)ug/L ND 100 N211/04/19 15:21
Aromatic (C11-C22)ug/L ND 100 N211/04/19 15:21
2-Bromonaphthalene (S)%106 40-140 11/04/19 15:21
2-Fluorobiphenyl (S)%108 40-140 11/04/19 15:21
Nonatriacontane (S)%91 40-140 11/04/19 15:21
o-Terphenyl (S)%95 40-140 11/04/19 15:21
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2722756LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2722757
Aliphatic (C09-C18)ug/L 182 N23006140-14053160 13 50
Aliphatic (C19-C36)ug/L 303 N24007640-14065261 15 50
Aromatic (C11-C22)ug/L 740 N28508740-14074631 16 50
2-Bromonaphthalene (S)%105 40-14095
2-Fluorobiphenyl (S)%106 40-140103
Nonatriacontane (S)%86 40-14075
o-Terphenyl (S)%105 40-14088
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/08/2019 03:47 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 42
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92451374
ALAMANCE OIL 2019-210
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.B
Common Laboratory Contaminant.C9
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
RPD value was outside control limits.R1
Surrogate recovery outside control limits due to matrix interferences (not confirmed by re-analysis).S5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/08/2019 03:47 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 38 of 42
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92451374
ALAMANCE OIL 2019-210
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92451374002 507098 507225MW-2 EPA 504.1 EPA 504.1
92451374003 508141 508236MW-3 EPA 504.1 EPA 504.1
92451374004 508141 508236MW-4 EPA 504.1 EPA 504.1
92451374002 507107 507465MW-2 MADEP EPH MADEP EPH
92451374003 507107 507465MW-3 MADEP EPH MADEP EPH
92451374004 507107 507465MW-4 MADEP EPH MADEP EPH
92451374002 506718MW-2 MADEP VPH
92451374003 506718MW-3 MADEP VPH
92451374004 506718MW-4 MADEP VPH
92451374002 507236 507268MW-2 EPA 3010A EPA 6010D
92451374003 507236 507268MW-3 EPA 3010A EPA 6010D
92451374004 507236 507268MW-4 EPA 3010A EPA 6010D
92451374001 507167 507376MW-1 EPA 625.1 EPA 625.1
92451374002 507167 507376MW-2 EPA 625.1 EPA 625.1
92451374003 507167 507376MW-3 EPA 625.1 EPA 625.1
92451374004 507167 507376MW-4 EPA 625.1 EPA 625.1
92451374002 507868MW-2 SM 6200B
92451374003 507868MW-3 SM 6200B
92451374004 508198MW-4 SM 6200B
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/08/2019 03:47 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 42
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