WS-7005_30505_CA_MRP_20230203

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]

February 3, 2023

Mr. Ryan Bond
NCDEQ-UST Section
Winston-Salem Regional Office
450 W. Hanes Mill Road
Suite 300
Winston-Salem, NC 27105

Re: Ground Water Monitoring Report
January 2023
Reedy Creek Food Mart
3778 NC Highway 150
Lexington, Davidson County
North Carolina
Facility ID Number: 00-0-0000011589
Incident Number: 30505
GRI Project Number: 6328

Dear Mr. Bond,

Please find enclosed the referenced report for the above mentioned site.
If you have any questions, please contact Scott Ball at 704-845-4010.

Sincerely,
Geological Resources, Inc.

Leslie Maxtone-Graham
Administrative Assistant

Enclosure

Cc: Mr. Lewis Efird; United Oil of the Carolinas, file

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
Engineering Certification: C-2727 • Geology Certification: C-127
Ground Water Monitoring Report
January 2023
Reedy Creek Food Mart
3778 North Carolina Highway 150
Lexington, Davidson County
North Carolina 27295
Facility ID Number: 00-0-0000011589
Incident Number: 30505
GRI Project Number: 6328

February 3, 2023

W. Scott Ball, Q.E.P.
Project Manager
Xavier T. Farmer, G.I.T.
Report Writer
Prepared for:
Mr. Lewis Efird
United Oil of the Carolinas
Post Office Box 68
Gastonia, North Carolina 28054-0068

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: February 3, 2023 Reedy Creek Food Mart
Project Manager: W. Scott Ball, Q.E.P. GRI Project No. 6328
i
EXECUTIVE SUMMARY
Reedy Creek Food Mart is located at 3778 North Carolina Highway 150 in Lexington, Davidson County,
North Carolina. The site is currently owned by Hanif Malik Et. Als. and is operated by M. Malik, Inc. as a
petroleum retail facility and convenience store. Soil sampling results after tank removal activities in 2004
confirmed a release at the site. Currently, one 10,000-gallon gasoline, two 4,000-gallon gasoline and one
2,000-gallon kerosene USTs are active at the site. The adjoining properties are a mixture of rural
agricultural, and commercial properties. According to the information determined during receptor survey
activities, six water supply wells were identified within 1,500 feet of the site. There is one well within
1,000 feet of the site, however, it is inactive, and the property is connected to municipal water. Public
water is available to the site and some surrounding properties within a 1,500-foot radius of the site.

On January 11, 2023, three monitoring wells and one telescoping well were gauged, purged and/or
sampled. Monitoring wells MW-4 and MW-7 could not be located, MW-2 is presumed to have been
covered in asphalt, and MW-5 is presumed destroyed. Free product was not observed at the site. The
concentrations of BTEX constituents, MTBE, naphthalene, acetone, tert-amyl alcohol (TAA), 2-butanone,
tert-butyl alcohol (TBA), 1,2-dibromoethane (EDB), 1,2-dicholorethane (1,2-DCA), ethanol, 2-hexanone,
isopropylbenzene, di-isopropyl ether, methyl isobutyl ketone (MIBK), n-propylbenzene, 1,2,4-
trimethylbenzne, 1,3,5-trimethylbenzene, lead, C5-C12 aliphatics and/or C9-C10 aromatics reported in
the ground water samples collected from MW-1, MW-3, MW-6, and/or VMW-1 exceeded the MACs. The
concentrations of benzene, TAA, EDB, and 1,2-DCA in MW-1 exceeded the GCLs.

Based on this information, the risk classification for the site should be lowered to intermediate risk. An
attempt should be made to locate and confirm the status of monitoring wells MW-2, MW-4, MW-5 and
MW-7. If these wells are not found, they should be replaced with new wells in order to assess
contamination more accurately at the site. Regular ground water monitoring should be continued at the
site. A MMPE event should be conducted at monitoring well MW-1 in order to reduce the concentrations
of dissolved phase contaminants reported in that well.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: February 3, 2023 Reedy Creek Food Mart
Project Manager: W. Scott Ball, Q.E.P. GRI Project No. 6328
ii
SITE INFORMATION
1. Site Identification
 Reedy Creek Food Mart (Facility ID 00-0-0000011589)
 Incident Number 30505 – High Risk (H135D)
 Location of Source Area: 3778 North Carolina Highway 150
Lexington, NC 27295
Davidson County
35.900594°N, 80.322970°W (Topographical Map)
2. Information about Contacts Associated with the Leaking UST System

UST/AST Owner
M. Malik, Inc.
4756 Pliney Farlow Rd.,
Trinity, NC 27370-7450
Email Unknown
Phone No. Unknown

UST/AST Operator
M. Malik, Inc.
4756 Pliney Farlow Rd.,
Trinity, NC 27370-7450
Email Unknown
Phone No. Unknown

3. Information about Release
 Release was discovered on November 3, 2004
 An unknown amount of product was released from the leaking UST system.
 One 10,000-gallon gasoline, two 4,000-gallon gasoline, and one 2,000-gallon kerosene USTs and
associated pumps and product piping are active at the site
Consultant/Contractor
Geological Resources, Inc.
3502 Hayes Road
Monroe, NC 28110
[e-mail]
704-845-4010
Property Owner
Hanif Malik Et Als
3778 N NC Hwy 150
Lexington, NC 27295
Email Unknown
Phone No. Unknown
Property Occupant
Reedy Creek Food Mart, Vape
& Glass Shop
3778 N NC Hwy 150
Lexington, NC 27295
Email Unknown
Phone No. Unknown
Analytical Laboratory
Waypoint Analytical, LLC
449 Spirngbrook Road
Charlotte, NC 28217
State Certification No. 37735 and
402
704-529-6364

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: February 3, 2023 Reedy Creek Food Mart
Project Manager: W. Scott Ball, Q.E.P. GRI Project No. 6328
iii
ACRONYMS
ACM: Asbestos Containing Materials
AFVR: Aggressive Fluid-Vapor Recovery
ARR: Acknowledgement of Report Receipt
AS: Air Sparging
AST: Aboveground Storage Tank
ASTM: American Society for Testing and
Materials
BGS: Below Ground Surface
CAP: Corrective Action Plan
CFR: Code of Federal Regulations
CSA: Comprehensive Site Assessment
DPE: Dual Phase Extraction
DRO: Total Petroleum Hydrocarbons Diesel
Range Organics
DWM: Division of Waste Management
DWR: Department of Water Resources
EPA: Environmental Protection Agency
EPH: Extractible Petroleum Hydrocarbons
ESA: Environmental Site Assessment
GCL: Gross Contamination Level
GRI: Geological Resources, Inc.
GRO: Total Petroleum Hydrocarbons
Gasoline Range Organics
LSA: Limited Site Assessment
MAC: Maximum Allowable Concentration as
specified in T15A NCAC 2L.0202
MADEP: Massachusetts Department of
Environmental Protection
MCC: Maximum Contaminant Concentrations
MMPE: Mobile Multi-Phase Extraction
NAPL: Non-Aqueous Phase Liquid, “Free
Product”
NCDEQ: North Carolina Department of
Environmental Quality
NCDOT: North Carolina Department of
Transportation
NFA: Notice of No Further Action
NORR: Notice of Regulatory Requirements
NOV: Notice of Violation
NPDES: National Pollutant Discharge
Elimination System
NRP: Notice of Residual Petroleum
O&M: Operation and Maintenance
PAHs: Polynuclear Aromatic Hydrocarbons
PCA: Pre-Construction Assessment
RAL: Regulatory Action Level
SCLs: Soil Cleanup Level
SPCC: Spill Prevention Control and
Countermeasures
SVE: Soil Vapor Extraction
SVOCs: Semi-Volatile Organic Compounds
SWPPP: Stormwater Pollution Prevention Plan
TCLP: Toxicity Characteristic Leaching
Procedure (EPA Method SW-846 1311)
TOC: Top of Casing
TPH: Total Petroleum Hydrocarbons
USGS: United States Geological Survey
UST: Underground Storage Tank
UVF: Ultraviolet Fluorescence
VOCs: Volatile Organic Compounds
VPH: Volatile Petroleum Hydrocarbons

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: February 3, 2023 Reedy Creek Food Mart
Project Manager: W. Scott Ball, Q.E.P. GRI Project No. 6328
TABLE OF CONTENTS
EXECUTIVE SUMMARY ....................................................................................................................... i
SITE INFORMATION ............................................................................................................................ ii
ACRONYMS ....................................................................................................................................... iii
1.0 SITE HISTORY AND CHARACTERIZATION ...................................................................................1
2.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL
ASSESSMENT INFORMATION ...................................................................................................2
3.0 FREE PRODUCT REMOVAL ........................................................................................................3
4.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS ..................................3
5.0 CONCLUSIONS .........................................................................................................................4
6.0 LIMITATIONS ...........................................................................................................................4
7.0 STATEMENTS AND CERTIFICATION ...........................................................................................4

FIGURES
Figure 1: Site Location Map
Figure 2A: Site Vicinity Map
Figure 2B: Zoning Map
Figure 3: Site Map
Figure 4: Water Table Surface Map
Figure 5: Ground Water Quality Map

TABLES
Table 1: UST Owner and Operator Information
Table 2: UST System Information
Table 3: Adjacent Property Owner Information
Table 4: Updated Receptor Survey Information
Table 5: Well Construction and Gauging Information
Table 6: Summary of Ground Water Sample Analytical Results

APPENDICES
Appendix A: State Correspondence
Appendix B: Land Use Information
Appendix C: Laboratory Analytical Report

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: February 3, 2023 Reedy Creek Food Mart
Project Manager: W. Scott Ball, Q.E.P. GRI Project No. 6328
1
1.0 SITE HISTORY AND CHARACTERIZATION
GRI presents the results of the January 2023 ground water sampling event at the Reedy Creek Food Mart
site; located at 3778 North Carolina Highway 150 in Lexington, Davidson County, North Carolina. A
topographic map showing the general site location and the surrounding area is included as Figure 1. These
activities were conducted in accordance with GRI Proposal No. 22-897, which was submitted to the
NCDEQ and was approved as Task Authorization No. 30505-4 on December 16, 2022. State
correspondence is included as Appendix A.

The site is currently owned by Hanif Malik Et. Als. and is operated by M. Malik, Inc. as a petroleum retail
facility and convenience store. Concentrations of TPH-GRO and TPH-DRO taken from beneath the
dispensers and product piping during tank closure in 2004 indicated a release at the site. Currently, one
10,000-gallon gasoline, two 4,000-gallon gasoline, and one 2,000-gallon kerosene USTs are active at the
site. UST owner/operator information and UST system information are included as Tables 1 and 2,
respectively. The Registered Tank Report is shown below:

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: February 3, 2023 Reedy Creek Food Mart
Project Manager: W. Scott Ball, Q.E.P. GRI Project No. 6328
2
The site and surrounding area is a mixture of rural agricultural, and commercial properties. The site
contains one building (the store and restaurant) and is primarily capped with concrete and asphalt. The
overall topography at the site is relatively flat. No surface water bodies were identified within a 500-foot
radius of the site. Seven Type II monitoring wells (MW-1 through MW-7) and one Type III monitoring well
(VMW-1) were installed at the site during previous ground water assessment activities. A Site Map
showing the locations of the monitoring wells and the structures on-site is included as Figure 2.

On January 11, 2023, GRI personnel conducted a receptor survey at the site. Six water supply wells were
identified within a 1,500-foot radius of the site. One Water Supply Well was identified within 1,000 feet
of the site, however the property is connected to municipal water and the well is inactive. Three potable
and two inactive water supply wells were identified between 1,000 and 1,500 feet from the site.
Municipal water is available to the site and some surrounding properties. Adjacent property owner
information is presented in Table 3. A Site Vicinity Map showing the adjacent properties has been
included as Figure 3. The information gathered during the updated receptor survey is included as Table
4. Land use information has been summarized in Appendix B.

S&ME, Inc. submitted a CAP on July 24, 2015, that proposed to reduce contaminant concentrations to at
or below GCLs at site by limited excavation of contaminated soils, as well as the installation of a vapor
extraction and air sparging remediation system at the site. Based on available information, the CAP was
not implemented.
2.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL
ASSESSMENT INFORMATION
On January 11, 2023, three Type II monitoring wells (MW-1, MW-3, and MW-6) and one telescoping well
(VMW-1) were gauged, purged and/or sampled in accordance with the NCDEQ guidelines. Monitoring
wells MW-4 and MW-7 could not be located, MW-2 is presumed to have been covered in asphalt, and
MW-5 is presumed destroyed. Free product was not observed at the site. Depths to ground water in the
Type II monitoring wells ranged from 32.31 feet to 32.98 feet. Ground water elevations in the Type II
monitoring wells ranged from 67.02 feet to 68.32 feet. Ground water flow was divergent around MW-1
flowing northeast and southwest with horizontal gradients of approximately 0.01 feet per foot northeast,
and approximately 0.001 feet per foot southwest. The vertical gradient between paired wells MW-1 and
VMW-1 was approximately 0.005 feet per foot in the downward direction. Well construction and gauging
information is presented in Table 5. A Water Table Surface Map based on the January 11, 2023 gauging
data of the Type II monitoring wells is included as Figure 4. A summary of the current ground water
gauging data is shown below:
Well ID
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(feet)
Free
Product
Thickness
(ft.)
Ground
Water
Elevation
(ft.)
MW-1 30 - 45 45 101.03 32.71 --- 68.32
MW-2 27 - 42 42 101.05 NM --- NM
MW-3 30 - 45 45 100.00 32.98 --- 67.02
MW-4 30 - 45 45 100.10 NM --- NM

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: February 3, 2023 Reedy Creek Food Mart
Project Manager: W. Scott Ball, Q.E.P. GRI Project No. 6328
3
MW-5 25 - 40 40 100.57 NM --- NM
MW-6 34 - 44 44 100.53 32.31 --- 68.22
MW-7 33 - 43 43 100.62 NM --- NM
VMW-1 70 - 75 75 101.09 32.95 --- 68.14

Ground water samples collected from the monitoring wells were submitted for laboratory analyses using
EPA Method 6200B plus oxygenates, VPH by the MADEP method, and lead by method 6010. The
concentrations of BTEX constituents, MTBE, naphthalene, acetone, tert-amyl alcohol (TAA), 2-butanone,
tert-butyl alcohol (TBA), 1,2-dibromoethane (EDB), 1,2-dicholorethane (1,2-DCA), ethanol, 2-hexanone,
isopropylbenzene, di-isopropyl ether, methyl isobutyl ketone (MIBK), n-propylbenzene, 1,2,4-
trimethylbenzne, 1,3,5-trimethylbenzene, lead, C5-C12 aliphatics and/or C9-C10 aromatics reported in
the ground water samples collected from MW-1, MW-3, MW-6, and/or VMW-1 exceeded the MACs. The
concentrations of benzene, TAA, EDB, and 1,2-DCA in MW-1 exceeded the GCLs. A summary of the
analytical results for ground water samples collected on January 11, 2023, is presented in Table 6. A
Ground Water Quality Map based on the January 2023 data is included as Figure 5. A complete report of
laboratory analyses of the ground water samples collected from the monitoring wells during the January
2023 sampling event has been included as Appendix C. A summary of the current ground water analytical
data is shown below:

Contaminant
of Concern → Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene Lead C5-C8 Aliphatics C9-C12 Aliphatics C9-C10 Aromatics Well
ID
MACs (μg/l) 1 600 600 500 20 6 15 400 700 200
GCL (μg/l) 5,000 260,000 80,000 50,000 20,000 6,000 15,000 NE NE NE
MW-1 24,600 46,600 3,170 15,600 15,500 631 634 65,800 18,700 8,370
MW-2 NS NS NS NS NS NS NS NS NS NS
MW-3 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 15 <11.5 <25.8 <4.02
MW-4 NS NS NS NS NS NS NS NS NS NS
MW-5 NS NS NS NS NS NS NS NS NS NS
MW-6 <1.80 5.45 2.22 J 12.2 J 103 21.4 14 88 <25.8 7.67 J
MW-7 NS NS NS NS NS NS NS NS NS NS
VMW-1 1.67 8.52 1.27 15.9 0.786 J 1.93 <6.60 <11.5 71.0 J 24.8 J

The site is not located in the Coastal Plain Physiographic Province of North Carolina. The water table has
a seasonal high depth to water of approximately thirty-two feet BGS.
3.0 FREE PRODUCT REMOVAL
Free product has not historically been present in at the site.
4.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS
Due to the site being in the active remediation phase, no natural attenuation monitoring plan is currently
in place at the site.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: February 3, 2023 Reedy Creek Food Mart
Project Manager: W. Scott Ball, Q.E.P. GRI Project No. 6328
4
5.0 CONCLUSIONS
• On January 11, 2023, three Type II monitoring wells and one telescoping well were gauged, purged
and/or sampled. Monitoring wells MW-4, and MW-7 could not be found, MW-2 is presumed to
be covered by asphalt, and MW-5 is presumed destroyed. Ground water flow was generally
divergent to the northeast and southwest with a horizontal gradient of approximately 0.01 feet
per foot northeast, and approximately 0.001 feet per foot southwest. The vertical gradient
between paired wells MW-1 and VMW-1 was approximately 0.005 feet per foot in the downward
direction.
• The concentrations of BTEX constituents, MTBE, naphthalene, acetone, tert-amyl alcohol (TAA),
2-butanone, tert-butyl alcohol (TBA), 1,2-dibromoethane (EDB), 1,2-dicholorethane (1,2-DCA),
ethanol, 2-hexanone, isopropylbenzene, di-isopropyl ether, methyl isobutyl ketone (MIBK), n-
propylbenzene, 1,2,4-trimethylbenzne, 1,3,5-trimethylbenzene, lead, C5-C12 aliphatics and/or
C9-C10 aromatics reported in the ground water samples collected from MW-1, MW-3, MW-6,
and/or VMW-1 exceeded the MACs. The concentrations of benzene, TAA, EDB, and 1,2-DCA in
MW-1 exceeded the GCLs.
• Based on this information, the risk classification for the site should be reduced to intermediate
risk. An attempt should be made to locate monitoring wells MW-2, MW-4, MW-5, and MW-7. If
these wells are not found, they should be replaced with new wells in order to assess
contamination more accurately at the site. Regular ground water monitoring should be continued
at the site.
• A MMPE event should be conducted at monitoring well MW-1 in order to reduce the
concentrations of dissolved phase contaminants reported in that well.
6.0 LIMITATIONS
This report has been prepared for the exclusive use of United Oil of the Carolinas for specific application
to the referenced site in Davidson County, North Carolina. The assessment was conducted based on the
scope of work and level of effort desired by the NCDEQ and with resources adequate only for that scope
of work. Our findings have been developed in accordance with generally accepted standards of
environmental practices in the State of North Carolina, available information, and our professional
judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would
be interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data.
7.0 STATEMENTS AND CERTIFICATION
1 Enter the date the monitoring report was due. n/a Will this report be submitted after the
established due date?
YES NO
2 Was any required information from the above template missing from this report? YES NO

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: February 3, 2023 Reedy Creek Food Mart
Project Manager: W. Scott Ball, Q.E.P. GRI Project No. 6328
5
IF the answer to question #1 or# 2 is “YES”, please provide additional information in this cell to explain
what was missing and why.
3 If applicable, will any of the proposed attenuation milestones under the schedule approved
in the Corrective Action Plan not be met? (within a reasonable margin of error)
YES NO
IF the answer to question #3 is “NO”, skip to the certification under #8 below.
IF the answer to question #3 is “YES”, please generally describe in this cell the possible reason(s) and
outline proposed remedies. (This should be described in more detail in the report text above.)

N/A
4 Does any known or suspected source zone soil contamination or free product remain
outside of the assessed area that could be inhibiting natural attenuation?
YES NO
5 Has there been an unexpected increase in contaminant mass sufficient to suggest a
potential new release from a separate onsite or offsite source?
YES NO
IF the answer to either question #4 or #5 is “YES”, generally describe in this cell any actions
recommended to further assess or clean up this known or suspected source. (This should be described
in more detail in the report text above.)

6 Certification:
I, Samuel L. McKay, III, a Licensed Geologist for Geological Resources, Inc., do certify that the information
contained in this report is correct and accurate to the best of my knowledge.

Geological Resources, Inc. is licensed to practice engineering and geology in North Carolina. The
certification number of the company or corporation is C-2727/C-127.

FIGURES
SITE LOCATIONFigure 1 Site Location Reedy Creek Food Mart3778 North Highway 150Lexington, North CarolinaDavidson CountyIncident No. 30505GRI Project No. 6328500 M2000 FTDate: 01/04/2023Location: 35.900594° N -80.322970° W Dad
"J
"J
"J
"J
"J
"J
SITE
6708-04-94-2882
6708-02-75-4739
6708-04-64-9449
6708-02-65-7255
6708-02-75-2316
6708-02-85-4636
6708-02-85-6027
6708-04-74-32286708-02-85-33316708-04-74-52276708-02-85-5358
6708-02-85-5253
6708-04-74-9156
6708-04-74-4724
6708-02-85-0296
WSW-6
WSW-5
WSW-4
WSW-3
WSW-2
WSW-1
North Carolina Highway 150 Perrell Lane
Butterfly Drive
St ell a Driv e
H e rita g e D riv e
Baby Bear Lane
Lenox Court
FIGURE 2A: SITE VICINITY MAPREEDY CREEK FOOD MART3778 NC HIGHWAY 150LEXINGTON, DAVIDSON COUNTYNORTH CAROLINAINCIDENT NO. 30505GRI PROJECT NO. 6328
PREPARED BY:GEOLOGICAL RESOURCES, INC.FEBRUARY 2, 2023
³
0 300150Feet
1 inch = 300 feet
1,500-FOOT RADIUS
1,000-FOOT RADIUS
250-FOOT RADIUS
500-FOOT RADIUS
LEGEND
"J Water Supply Well
Centerlines
hydrography
Well Owners and Adjacent Properties
Parcels
"J
"J
"J
"J
"J
"J
SITE
WSW-6
WSW-5
WSW-4
WSW-3
WSW-2
WSW-1
North Carolina Highway 150 Perrell Lane
Butterfly Drive
St ell a Driv e
H e rita g e D riv e
Baby Bear Lane
Lenox Court
FIGURE 2B: ZONING MAPREEDY CREEK FOOD MART3778 NC HIGHWAY 150LEXINGTON, DAVIDSON COUNTYNORTH CAROLINAINCIDENT NO. 30505GRI PROJECT NO. 6328
PREPARED BY:GEOLOGICAL RESOURCES, INC.FEBRUARY 2, 2023
³
0 300150Feet
1 inch = 300 feet
1,500-FOOT RADIUS
1,000-FOOT RADIUS
250-FOOT RADIUS
500-FOOT RADIUS
LEGEND
ZONING - RA-3
ZONING - RC
ZONING - HC
"J Water Supply Well
Centerlines
hydrography
Parcels

TABLES
UST ID Number A1 - A4 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number A1 - A4 Facility ID Number
Owner or Operator?
Owner
UST ID Number A1 - A4 Facility ID Number
Owner or Operator?
Owner
Telephone Number
0-011589
Name of Owner or Operator Dates of Ownership / Operation
Address Telephone Number
0-011589
[phone]
Unknown Unknown
0-011589
Name of Owner or Operator Dates of Ownership / Operation
M. Malik, Inc.09/08/2006 - Current
Address
Holding Bros., Inc.05/05/1986 - 09/08/2006
Name of Owner or Operator Dates of Ownership / Operation
Address
United Oil of the Carolinas, Inc.01/11/2002 - 09/08/2006
P.O. Box 68, Gastonia, NC 28053
4756 Pliney Farlow Road, Trinity, NC 27370-7450 Unknown
Telephone Number
TABLE 1
UST OWNER/OPERATOR INFORMATION
REEDY CREEK FOOD MART (INCIDENT NO. 30505)
Page 1 of 1
Date: 01/13/23
Was Release
Associated
with UST
System?
(Yes / No)
1 Kerosene NA 1,000 4/22/1970 Single Wall Steel 46" x 12'Single Wall Steel Removed No
2 Gasoline NA 4,000 4/22/1970 Single Wall Steel 5' 4" x 24'Other Removed Yes
3 Gasoline NA 4,000 4/22/1970 Single Wall Steel 5' 4" x 24'Other Removed Yes
4 Gasoline NA 4,000 4/22/1970 Single Wall Steel 5' 4" x 24'Other Removed Yes
A1 Gasoline NA 10,000 9/8/2006 Double Wall Steel 8' x 26' 8"Single Wall FRP Current No
A2 Gasoline NA 4,000 9/8/2006 Double Wall Steel 5' 4" x 24'Other Current No
A3 Gasoline NA 4,000 9/8/2006 Double Wall Steel 5' 4" x 24'Other Current No
A4 Kerosene NA 2,000 9/8/2006 Double Wall Steel 5' 4" x 12'Single Wall FRP Current No
Notes:
• FRP: Fiberglass reinforced plastic.
TABLE 2
UST SYSTEM INFORMATION
REEDY CREEK FOOD MART (INCIDENT NO. 30505)
Facility ID # : 0-011589
Status
of
UST
UST
ID
No.
Current
or Most
Recent
Contents
Previous
Contents
Capacity
(gallons)
Date
Installed
Construction
Details
Tank
Dimensions
Description of
Associated
Product Piping
and
Pumps
Page 1 of 1
Date: 01/13/23 Facility ID # : 0-011589
Parcel Number Owner Name Address
6708-02-85-3331 (Site)Malik Hanifand 3778 North NC Highway 150
Lexington, NC 27295
6708-02-85-4636 Harry Lee Hill 3880 North NC Highway 150
Lexington, NC 27295
6708-02-85-5358 McCullough-Stokes Properties, LLC 153 Lenox Court
Lexington, NC 27295
6708-02-85-5253 Chaney Lane Sheffield 194 Lenox Court
Lexington, NC 27295
6708-02-85-6027 David and Lisa Koonts 3768 North NC Highway 150
Lexington, NC 27295
6708-02-85-0296 Russell Palmer Freedle, Jr.3771 North NC Highway 150
Lexington, NC 27295
6708-02-85-7255 Russell Palmer Freedle, Jr.3729 North NC Highway 150
Lexington, NC 27295
6708-02-85-0491 CG2 Homes, Inc.111 Salter Path
Lexington, NC 27295
6708-02-85-1615 CG2 Homes, Inc.110 Salter Path
Lexington, NC 27295
Note:
• Properties are keyed to Figure 3.
TABLE 3
ADJACENT PROPERTY OWNER INFORMATION
REEDY CREEK FOOD MART (INCIDENT NO. 30505)
Page 1 of 1
Facility ID # : 0-011589
Well ID.Parcel ID No.Well Owner Mailing Address Well Address Well Status
(Active/In-Active)
Well Use
(Potable / Non-
Potable
etc.)
Municpal
Water
Available
Yes/No
Connected
to
Municipal
Water
Yes/No
Distance
from
source area
of release
(ft.)
WSW-1 6708-04-74-4724 Danny & Scarlet Link 234 Baby Bear Lane
Lexington, NC 27295
234 Baby Bear Lane
Lexington, NC 27295 Active Potable Unknown No ~1050' SW
WSW-2 6708-04-74-3228 Justin & Rachel Lanier 290 Baby Bear Lane
Lexington, NC 27295
290 Baby Bear Lane
Lexington, NC 27295 Inactive Non-Potable
Inactive Yes Yes ~1400' SW
WSW-3 6708-04-74-5227 Nickolas & Kayla Fritts 289 Baby Bear Lane
Lexington, NC 27295
289 Baby Bear Lane
Lexington, NC 27295 Inactive Non-Potable
Inactive Yes Yes ~1,350' SW
WSW-4 6837-43-2387 John Perrell 213 Baby Bear Lane
Lexington, NC 27295
213 Baby Bear Lane
Lexington, NC 27295 Active Potable Unknown No ~1,300' SW
WSW-5 6708-04-74-9156 Wanda Turner & Marjorie Holder 1800 Meadow Glen Lane
Winston Salem, NC 27127
3559 North NC Highway 150
Lexington, NC 27295 Active Potable Unknown No ~1,300' S
WSW-6 6708-04-94-2882 Patsy Perrell 133 Perrell Lane
Lexington, NC 27295
133 Perrell Lane
Lexington, NC 27295 Inactive Non-Potable
Inactive Yes Yes ~650' SE
Notes:
• Receptors are shown on Figure 3.
• n/a: not applicable.
Unknown
TABLE 4
RECEPTOR INFORMATION
REEDY CREEK FOOD MART (INCIDENT NO. 30505)
Date: 01/25/23
Well Construction Details
(Depth, Screened Interval, Type of Well, ect.)
51' bored well; 24' - 51' screened interval
Unknown
Unknown
Unknown
62' bored well
Page 1 of 1
Date: 01/13/23
Well ID
Date
Installed
(m/dd/yy)
Date Water
Level
Measured
(m/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(feet)
Free Product
Thickness
(ft.)
Ground
Water
Elevation (ft.)
Comments
MW-1 01/28/05 01/11/23 30 30 - 45 45 101.03 32.71 ---68.32
MW-2 01/28/05 01/11/23 27 27 - 42 42 101.05 NM ---NM covered w/ asphalt
MW-3 03/30/05 01/11/23 30 30 - 45 45 100.00 32.98 ---67.02
MW-4 03/30/05 01/11/23 30 30 - 45 45 100.10 NM ---NM not found
MW-5 03/30/05 01/11/23 25 25 - 40 40 100.57 NM ---NM destroyed
MW-6 10/21/09 01/11/23 34 34 - 44 44 100.53 32.31 ---68.22
MW-7 10/21/09 01/11/23 33 33 - 43 43 100.62 NM ---NM not found
VMW-1 03/31/05 01/11/23 70 70 - 75 75 101.09 32.95 ---68.14
Notes:
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
REEDY CREEK FOOD MART (INCIDENT NO. 30505)
Facility ID # : 0-011589
• ft BGS : feet below ground surface.
• NM : Not measured.
• Elevation relative to mean sea level.
Page 1 of 1
EPA
Method
6010/303
0C
Well
ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 6,000 40 4,000 10 0.02 0.4 4,000 40 70 70 100 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,000,000 40,000 4,000,000 10,000 50 400 4,000,000 40,000 30,500 70,000 100,000 26,100 28,500 25,000 15,000 NE NE NE
MW-1 01/11/23 24,600 46,600 3,170 15,600 15,500 631 44,000 48,000 23,000 9,000 1,040 2,080 14500 J 4,230 143 9,360 1,280 440 3,730 1,010 634 65,800 18,700 8,370
MW-2 01/11/23 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
MW-3 01/11/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <1.80 <1.90 <0.710 7.00 J <0.200 <0.150 <42.0 <0.380 <0.180 <0.500 <0.078 <0.190 <0.190 <0.180 15.1 <11.5 <25.8 <4.02
MW-4 01/11/23 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
MW-5 01/11/23 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
MW-6 01/11/23 <1.80 5.45 2.22 J 12.2 J 103 21.4 <18.0 338 <7.10 266 <2.00 <0.150 <420 <3.80 <1.80 17.6 <0.780 <1.90 4.41 J <1.80 14.1 88.2 <25.8 7.67 J
MW-7 01/11/23 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
VMW-1 01/11/23 1.67 8.52 1.27 15.9 0.786 J 1.93 22.3 16.9 4.53 J 10.4 <0.200 <0.150 <42.0 0.807 J 0.207 J 0.890 1.04 0.777 11.1 4.65 <6.60 <11.5 71.0 J 24.8 J
Trip Blank 01/11/23 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <1.80 NM <0.710 NM <0.200 <0.150 <42.0 <0.380 <0.180 <0.500 <0.078 <0.190 <0.190 <0.180 NM NM NM NM
Notes:
• For other compounds reported which did not exceed the MACs, refer to the laboratory reports.
• Concentrations in italics indicate the GCLs were below the reported concentrations.
• Concentrations in bold face type indicate the MACs were below the reported concentrations.
• J: Estimated value.tert-Butyl alcohol(TBA)2-Butanone(MEK)2-HexanoneEthanol1,2-Dichloroethane1,2-Dibromoethane(EDB)n-PropylbenzeneMethyl isobutyl ketone (MIBK) (4-Methyl-2-PentanoneDi-isopropyl etherIsopropylbenzene• Results reported in µg/l (micrograms per liter)
• MAC: Maximum Allowable Concenration as specified in T15A NCAC 2L.0202.
• GCL: Gross contamination level.
• NE: Standard not established.
• < : Less than the method detection limit specified in the laboratory report.
MACs (μg/l)
GCL (μg/l)NaphthaleneAcetonetert-Amyl alcohol(TAA)Contaminant of Concern
→BenzeneTolueneEthylbenzeneXylenesMTBETABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
REEDY CREEK FOOD MART (INCIDENT NO. 30505)
Date: 01/31/23 Facility ID #: 0-011589
Analytical Method
→EPA Method 6200B MADEP Method VPH
C9-C12 AliphaticsC9-C10 Aromatics1,2,4-TrimethylbenzeneLeadC5-C8 Aliphatics1,3,5-TrimethylbenzenePage 1 of 1

APPENDICES

APPENDIX A
State Correspondence
6328 Received DEC 28 2022
Site Name City / County /Davidson Incident #30505
Resp Pty Name / Contact Incident Mgr Region WS
RP Type (Owner/Operator / Landowner / Attny-in-fact)Change Order?Prev. TA #3
Consultant / Project Mgr /Scott Ball
Telephone / Fax Number /Task Authorization Number:4 ChangeOrd:
Project Mgr Email Site Risk / Rank / Abatement:H-135-D RRA Date:5/11/2005
Proposal# / Scope Dates /% Commercial (C=100%, NC=0%, Both=1%-99%)
Has STF Eligibility Been Determined? (Y/N)Site Status (Active or NFA Date)
With Claim: [ ] All Main Consultant/Contractor invoices attached?[ ] Proof of payment attached directly to the front of each invoice?
 Important: The date of reimbursement is dependent on the Trust Fund balance. There may be a delay in the reimbursement of claims for work under this ePATA.3rd Pty Ded?Task #Lab /
SubCode
RO IM AuthProposed
Rate/Price
(Consultant)RO Supv. AuthProposed Task
Subtotal
(Consultant)
Final
Preapproved
Subtotal
(UST Section)
Claimed
Amount3
(Consultant)
1.010 1 /site y $500.00 Y $500.00 $500.00 /
1.025 1 /site y $740.00 Y $740.00 $740.00 /
1.050 1 /agreement y $300.00 Y $300.00 $300.00 /
4.031 7 /wells y $110.00 Y $770.00 $770.00 /
4.090 #240 8 /samples y $94.00 Y $752.00 $752.00 /
4.090 #330 7 /samples y $14.00 Y $98.00 $98.00 /
4.090 #341 7 /samples y $56.00 Y $392.00 $392.00 /
4.091 1 /shipment y $60.00 Y $60.00 $60.00 /
6.090 1 /report y $1,125.00 Y $1,125.00 $1,125.00 /
12.050 1 /trip y $250.00 Y $250.00 $250.00 /
12.055 1 /trip y $50.00 Y $50.00 $50.00 /
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
Requested Preapproved Claimed 3
TOTAL:$5,037.00 $5,037.00 TOTAL:
Total Standard Costs (Not Third Party)$5,037.00 $5,037.00 Total Standard Costs
Total applied as Third Party Deductible/Damage Costs $0.00 $0.00 Total Third Pty Costs
Process Tracking (Date)
TA Submittal:12/15/22 by:(PM)(Reserved for RO)
RO Review:12/15/22 by:(IM)Joint UST Preapproval Confirmed By:Date1 12/16/2022
RO Supv. Review:12/16/22 by:(STF)RP or Designee Receipt Confirmation By:Date 4
1 - This ePATA expires one year from the Joint UST Preapproval date. This does not extend, alter, or supersede any regulatory deadlines (e.g., NORR's, NOV's, Enforcements, etc.)
2 - THE ONE YEAR STATUTE OF LIMITATIONS APPLIES TO EACH INDIVIDUAL TASK. Costs must be claimed within one year of completion of that task to be reimbursable.
3 - Only Tasks included on this ePATA may be claimed. Do not include other Tasks or claimed costs (i.e., Claim preparation) that were not preapproved or the claim will be returned.
4 - Preapproval is not valid (i.e., claimable) until receipt is signed as 'Confirmed' by the RP or their designee within a week of approval. The signed pre-approval must be submitted
in the submitted claim. Signature indicates acknowledgement of the tasks and amounts approved. Any objections/appeals must be submitted via Change Order prior to work
proceeding. Scope/cost negotiations do not supersede other regulatory deadlines as described in #1 above. Also, any ePATA that has been signed as 'Confirmed' by both the
UST Section and RP is not to be modified without written consent by all signatories.
5 - Tasks approved on Directed - CAB Only ePATAs must be performed in accordance with all applicable rules, statutes, and RRD Task Scopes of Work to be reimbursed in full.
DWM/UST ePATA 4/1/2022
SB
Proposed
Units / Type
(Consultant)
Ryan Bond
Active
22-897 ecember 2022-January 202
704-845-4012
Dates of Work
(Consultant)
Started1 / Completed2
FINAL REIMBURSEMENT
[e-mail]
United Oil of the Carolinas Lewis Efird
Geological Resources, Inc.
DIRECTED - CAB ONLY
Lexington
(Must Complete with Claim Submittal)(See Instructions / RRD for Tasks requiring Preapproval / Task Authorization)
Owner/Operator
704-845-4010
(Reserved for Incident Manager)
PREAPPROVAL / TASK AUTHORIZATION
Reedy Creek Food Mart
Note:This Electronic Preapproval Task Authorization (ePATA)shall be used to receive preapproval from the UST Section.A proposal,including maps and figures,must be
attached to elaborate on the costs for the tasks listed below that describes the scope of work and the rationale for the proposed activities.If,following completion of this ePATA,you discover that unexpected tasks must be performed, incurring costs for tasks not originally included with this form,you must complete and submit a separate ePATA request
designated as a "Change Order" in the provided space above prior to conducting those tasks.Include a copy of the prior ePATA form for confirmation.Please attach this form to
the cover of the corresponding claim when requesting reimbursement.IMPORTANT:Only one claim may be submitted per ePATA and all work on the ePATA must have beencompletedwithin12monthsofthecompletiondateoftheFIRSTcompletedtasktoremainwithintheStatuteofLimitations.All ePATAs submittedwithin aclaim are closed with thatclaim,and may not be re-used in a separate submittal,even for costs or tasks that were not originally claimed.Final reimbursement of costs associated with the Total Claimed
amount below may be affected by the eligibility status of the site (i.e.,deductibles,apportionment,etc.),and the documentary validation of incurred costs as reasonable and
necessary expenses per 15A NCAC 2P .0402 and .0404.
RAB
JWB
(Initials)
ELECTRONIC PREAPPROVAL TASK AUTHORIZATION FORMDept of Environmental Quality -Division of Waste Management
Changed analytical method #272 to #240. -RAB
12/20/2022
6328 Received DEC 20 2022

APPENDIX B
Land Use Information
Date: 01/25/23 Facility ID # : 00-0-0000011589
Map ID No.Land Use Feature Zoning Description Address
Distance from
Source Area
(feet)
n/a RA-3 Rural Agricultural
District n/a n/a
n/a HC Highway Commercial
District n/a n/a
n/a RC Rural Commercial
District n/a n/a
Note:
• Properties are keyed to Figure 2B.
APPENDIX B
LAND USE INFORMATION
REEDY CREEK FOOD MART (INCIDENT NO. 30505)
Page 1 of 1

APPENDIX C
Laboratory Analytical Report

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

1/24/2023
Geological Resources, Inc. Scott Ball
3502 Hayes Road Monroe, NC, 28110
Ref: Analytical Testing
Lab Report Number: 23-011-0103 Client Project Description: Reedy Creek Food Mart
GRI # 6328
Dear Scott Ball:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 1/11/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love Project Manager
Page 1 of 61
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202337735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202399012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Page 1 of 1 00016/23-011-0103
Page 2 of 61
Report Number:
Sample Summary Table
Client Project Description:
23-011-0103
Reedy Creek Food Mart
GRI # 6328
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
01/11/2023 08:50Aqueous 97297 MW-1 01/11/2023 15:04
01/11/2023 08:50Aqueous 97297 MW-1 01/11/2023 15:04 6010D Eurofins -
01/11/2023 09:20Aqueous 97298 MW-3 01/11/2023 15:04
01/11/2023 09:20Aqueous 97298 MW-3 01/11/2023 15:04 6010D Eurofins -
01/11/2023 08:40Aqueous 97299 MW-6 01/11/2023 15:04
01/11/2023 08:40Aqueous 97299 MW-6 01/11/2023 15:04 6010D Eurofins -
01/11/2023 09:05Aqueous 97300 VMW-1 01/11/2023 15:04
01/11/2023 09:05Aqueous 97300 VMW-1 01/11/2023 15:04 6010D Eurofins -
01/11/2023Aqueous 97301 TB 01/11/2023 15:04
Eurofins - Savannah: Eurofins Environmental Testing Southeast, Savannah, Savannah, GA
Page 3 of 61
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-011-0103
Report Limit
Project:Reedy Creek Food Mart
V 97297MW-1
See Attached6010DLead mg/L
44000 01/24/2023 08:316200BAcetoneµg/L 1800
24600 01/24/2023 08:316200BBenzeneµg/L 180
J28.8 01/19/2023 11:306200Bn-Butylbenzene µg/L 18.0
J23.6 01/19/2023 11:306200Bsec-Butyl benzene µg/L 20.0
9360 01/19/2023 11:306200BDi-Isopropyl Ether (DIPE)µg/L 50.0
1040 01/19/2023 11:306200B1,2-Dibromoethane µg/L 20.0
2080 01/19/2023 11:306200B1,2-Dichloroethane µg/L 15.0
J1450001/19/2023 11:306200BEthanolµg/L 4200
3170 01/19/2023 11:306200BEthylbenzeneµg/L 17.0
4230 01/19/2023 11:306200B2-Hexanone µg/L 38.0
143 01/19/2023 11:306200BIsopropylbenzeneµg/L 18.0
23000 01/24/2023 08:316200BMethyl Ethyl Ketone (MEK)µg/L 710
15500 01/24/2023 08:316200BMethyl tert-butyl ether (MTBE)µg/L 140
1280 01/19/2023 11:306200B4-Methyl-2-Pentanone µg/L 7.80
631 01/19/2023 11:306200BNaphthaleneµg/L 47.0
440 01/19/2023 11:306200Bn-Propylbenzene µg/L 19.0
9000 01/19/2023 11:306200Btert-Butyl Alcohol (TBA)µg/L 160
48000 01/24/2023 08:316200Btert-Amyl Alcohol (TAA)µg/L 1900
J89.0 01/19/2023 11:306200Btert-Amyl Methyl Ether (TAME)µg/L 28.0
46600 01/24/2023 08:316200BTolueneµg/L 220
3730 01/19/2023 11:306200B1,2,4-Trimethylbenzene µg/L 19.0
1010 01/19/2023 11:306200B1,3,5-Trimethylbenzene µg/L 18.0
5540 01/19/2023 11:306200Bo-Xylene µg/L 21.0
10100 01/19/2023 11:306200Bm,p-Xylene µg/L 42.0
15600 01/19/2023 11:306200BXylene (Total)µg/L 21.0
65800 01/13/2023 10:10CALCULATIONAliphatic C5-C8 (Adjusted)µg/L 5750
18700 01/12/2023 15:27CALCULATIONAliphatics C9-C12 (Adjusted)µg/L 2580
8370 01/12/2023 15:27CALCULATIONAromatic C9-C10 (Adjusted)µg/L 402
137000 01/13/2023 10:10MADEP-VPH Aliphatic C5-C8 µg/L 5750
45900 01/12/2023 15:27MADEP-VPH Aliphatic C9-C12 µg/L 2580
8370 01/12/2023 15:27MADEP-VPH Aromatic C9-C10 µg/L 402
V 97298MW-3
See Attached6010DLead mg/L
J7.00 01/19/2023 06:046200Btert-Butyl Alcohol (TBA)µg/L 1.60
Page 4 of 61
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-011-0103
Report Limit
Project:Reedy Creek Food Mart
V 97299MW-6
See Attached6010DLead mg/L
17.6 01/19/2023 10:406200BDi-Isopropyl Ether (DIPE)µg/L 5.00
J2.22 01/19/2023 10:406200BEthylbenzeneµg/L 1.70
103 01/19/2023 10:406200BMethyl tert-butyl ether (MTBE)µg/L 1.40
21.4 01/19/2023 10:406200BNaphthaleneµg/L 4.70
266 01/19/2023 10:406200Btert-Butyl Alcohol (TBA)µg/L 16.0
338 01/19/2023 10:406200Btert-Amyl Alcohol (TAA)µg/L 19.0
5.45 01/19/2023 10:406200BTolueneµg/L 2.20
J4.41 01/19/2023 10:406200B1,2,4-Trimethylbenzene µg/L 1.90
J3.73 01/19/2023 10:406200Bo-Xylene µg/L 2.10
J8.44 01/19/2023 10:406200Bm,p-Xylene µg/L 4.20
J12.2 01/19/2023 10:406200BXylene (Total)µg/L 2.10
88.2 01/12/2023 12:15CALCULATIONAliphatic C5-C8 (Adjusted)µg/L 11.5
J7.67 01/12/2023 12:15CALCULATIONAromatic C9-C10 (Adjusted)µg/L 4.02
93.6 01/12/2023 12:15MADEP-VPH Aliphatic C5-C8 µg/L 11.5
J29.0 01/12/2023 12:15MADEP-VPH Aliphatic C9-C12 µg/L 25.8
J7.67 01/12/2023 12:15MADEP-VPH Aromatic C9-C10 µg/L 4.02
V 97300VMW-1
See Attached6010DLead mg/L
22.3 01/19/2023 06:296200BAcetoneµg/L 1.80
1.67 01/19/2023 06:296200BBenzeneµg/L 0.180
J0.235 01/19/2023 06:296200Bn-Butylbenzene µg/L 0.180
0.890 01/19/2023 06:296200BDi-Isopropyl Ether (DIPE)µg/L 0.500
1.27 01/19/2023 06:296200BEthylbenzeneµg/L 0.170
J0.807 01/19/2023 06:296200B2-Hexanone µg/L 0.380
J0.207 01/19/2023 06:296200BIsopropylbenzeneµg/L 0.180
J4.53 01/19/2023 06:296200BMethyl Ethyl Ketone (MEK)µg/L 0.710
J0.786 01/19/2023 06:296200BMethyl tert-butyl ether (MTBE)µg/L 0.140
1.04 01/19/2023 06:296200B4-Methyl-2-Pentanone µg/L 0.078
1.93 01/19/2023 06:296200BNaphthaleneµg/L 0.470
0.777 01/19/2023 06:296200Bn-Propylbenzene µg/L 0.190
10.4 01/19/2023 06:296200Btert-Butyl Alcohol (TBA)µg/L 1.60
16.9 01/19/2023 06:296200Btert-Amyl Alcohol (TAA)µg/L 1.90
8.52 01/19/2023 06:296200BTolueneµg/L 0.220
11.1 01/19/2023 06:296200B1,2,4-Trimethylbenzene µg/L 0.190
4.65 01/19/2023 06:296200B1,3,5-Trimethylbenzene µg/L 0.180
Page 5 of 61
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-011-0103
Report Limit
Project:Reedy Creek Food Mart
V 97300VMW-1
6.65 01/19/2023 06:296200Bo-Xylene µg/L 0.210
9.26 01/19/2023 06:296200Bm,p-Xylene µg/L 0.420
15.9 01/19/2023 06:296200BXylene (Total)µg/L 0.210
J71.0 01/13/2023 11:35CALCULATIONAliphatics C9-C12 (Adjusted)µg/L 25.8
J24.8 01/13/2023 11:35CALCULATIONAromatic C9-C10 (Adjusted)µg/L 4.02
J12.1 01/13/2023 11:35MADEP-VPH Aliphatic C5-C8 µg/L 11.5
113 01/13/2023 11:35MADEP-VPH Aliphatic C9-C12 µg/L 25.8
J24.8 01/13/2023 11:35MADEP-VPH Aromatic C9-C10 µg/L 4.02
Page 6 of 61

Client: Geological Resources, Inc. CASE NARRATIVE
Project: Reedy Creek Food Mart Lab Report Number: 23-011-0103
Date: 1/24/2023
Volatile Organic Compounds - GC/MS Method 6200B Analyte: 1,2-Dibromo-3-chloropropane QC Batch No: V29119/V29020
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Analyte: Naphthalene QC Batch No: V29119/V29020
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.

Page 7 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-011-0103
00087
Geological Resources, Inc.
3502 Hayes Road
Scott Ball
Monroe
Danyale Love
Project Manager
GRI # 6328 Received : 01/11/2023
Reedy Creek Food Mart
Report Date : 01/24/2023
Sample ID :
Lab No :
Sampled:MW-1
97297 Matrix:
1/11/2023 8:50
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<100 µg/L 100 10003,3-Dimethyl-1-butanol 100 01/19/23 11:30 6200BMSA
See Attached mg/L 0.006Lead 1 6010DBKN
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 8 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-011-0103
00087
Geological Resources, Inc.
3502 Hayes Road
Scott Ball
Monroe
Danyale Love
Project Manager
GRI # 6328 Received : 01/11/2023
Reedy Creek Food Mart
Report Date : 01/24/2023
Sample ID :
Lab No :
Sampled:MW-1
97297 Matrix:
1/11/2023 8:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29020 01/18/23 14:00 V29118 01/23/23 14:00
44000 µg/L 1800 10000Acetone 1000 01/24/23 08:31 V29119MSA
24600 µg/L 180 500Benzene 1000 01/24/23 08:31 V29119MSA
<21.0 µg/L 21.0 50.0Bromobenzene 100 01/19/23 11:30 V29021MSA
<42.0 µg/L 42.0 100Bromochloromethane 100 01/19/23 11:30 V29021MSA
<16.0 µg/L 16.0 50.0Bromodichloromethane 100 01/19/23 11:30 V29021MSA
<150 µg/L 150 500Bromoform 100 01/19/23 11:30 V29021MSA
<28.0 µg/L 28.0 100Bromomethane 100 01/19/23 11:30 V29021MSA
28.8 J µg/L 18.0 50.0n-Butylbenzene 100 01/19/23 11:30 V29021MSA
23.6 J
µg/L 20.0 50.0
sec-Butyl benzene 100 01/19/23 11:30 V29021MSA
<92.0 µg/L 92.0 200tert-Butyl benzene 100 01/19/23 11:30 V29021MSA
<18.0 µg/L 18.0 50.0Carbon Tetrachloride 100 01/19/23 11:30 V29021MSA
<19.0 µg/L 19.0 50.0Chlorobenzene 100 01/19/23 11:30 V29021MSA
<19.0 µg/L 19.0 50.0Chlorodibromomethane 100 01/19/23 11:30 V29021MSA
<43.0 µg/L 43.0 100Chloroethane 100 01/19/23 11:30 V29021MSA
<22.0 µg/L 22.0 50.0Chloroform 100 01/19/23 11:30 V29021MSA
<22.0 µg/L 22.0 50.0
Chloromethane 100 01/19/23 11:30 V29021MSA
<20.0 µg/L 20.0 50.02-Chlorotoluene 100 01/19/23 11:30 V29021MSA
<20.0 µg/L 20.0 50.04-Chlorotoluene 100 01/19/23 11:30 V29021MSA
9360 µg/L 50.0 50.0Di-Isopropyl Ether (DIPE)100 01/19/23 11:30 V29021MSA
<110 µg/L 110 2001,2-Dibromo-3-Chloropropane 100 01/19/23 11:30 V29021MSA
1040 µg/L 20.0 50.01,2-Dibromoethane 100 01/19/23 11:30 V29021MSA
<23.0 µg/L 23.0 50.0Dibromomethane 100 01/19/23 11:30 V29021MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 9 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-011-0103
00087
Geological Resources, Inc.
3502 Hayes Road
Scott Ball
Monroe
Danyale Love
Project Manager
GRI # 6328 Received : 01/11/2023
Reedy Creek Food Mart
Report Date : 01/24/2023
Sample ID :
Lab No :
Sampled:MW-1
97297 Matrix:
1/11/2023 8:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29020 01/18/23 14:00 V29118 01/23/23 14:00
<22.0 µg/L 22.0 50.01,2-Dichlorobenzene 100 01/19/23 11:30 V29021MSA
<19.0 µg/L 19.0 50.01,3-Dichlorobenzene 100 01/19/23 11:30 V29021MSA
<21.0 µg/L 21.0 50.01,4-Dichlorobenzene 100 01/19/23 11:30 V29021MSA
<120 µg/L 120 500Dichlorodifluoromethane 100 01/19/23 11:30 V29021MSA
<24.0 µg/L 24.0 50.01,1-Dichloroethane 100 01/19/23 11:30 V29021MSA
2080 µg/L 15.0 50.01,2-Dichloroethane 100 01/19/23 11:30 V29021MSA
<15.0 µg/L 15.0 50.01,1-Dichloroethene 100 01/19/23 11:30 V29021MSA
<20.0 µg/L 20.0 50.0cis-1,2-Dichloroethene 100 01/19/23 11:30 V29021MSA
<18.0 µg/L 18.0 50.0
trans-1,2-Dichloroethene 100 01/19/23 11:30 V29021MSA
<19.0 µg/L 19.0 50.01,2-Dichloropropane 100 01/19/23 11:30 V29021MSA
<13.0 µg/L 13.0 50.01,3-Dichloropropane 100 01/19/23 11:30 V29021MSA
<21.0 µg/L 21.0 2002,2-Dichloropropane 100 01/19/23 11:30 V29021MSA
<20.0 µg/L 20.0 50.01,1-Dichloropropene 100 01/19/23 11:30 V29021MSA
<21.0 µg/L 21.0 50.0cis-1,3-Dichloropropene 100 01/19/23 11:30 V29021MSA
<15.0 µg/L 15.0 50.0trans-1,3-Dichloropropene 100 01/19/23 11:30 V29021MSA
14500 J
µg/L 4200 20000
Ethanol 100 01/19/23 11:30 V29021MSA
3170 µg/L 17.0 50.0Ethylbenzene 100 01/19/23 11:30 V29021MSA
<35.0 µg/L 35.0 300Hexachlorobutadiene 100 01/19/23 11:30 V29021MSA
4230 µg/L 38.0 1002-Hexanone 100 01/19/23 11:30 V29021MSA
143 µg/L 18.0 50.0Isopropylbenzene 100 01/19/23 11:30 V29021MSA
<8.90 µg/L 8.90 50.04-Isopropyl toluene 100 01/19/23 11:30 V29021MSA
23000 µg/L 710 5000Methyl Ethyl Ketone (MEK)1000 01/24/23 08:31 V29119MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 10 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-011-0103
00087
Geological Resources, Inc.
3502 Hayes Road
Scott Ball
Monroe
Danyale Love
Project Manager
GRI # 6328 Received : 01/11/2023
Reedy Creek Food Mart
Report Date : 01/24/2023
Sample ID :
Lab No :
Sampled:MW-1
97297 Matrix:
1/11/2023 8:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29020 01/18/23 14:00 V29118 01/23/23 14:00
15500 µg/L 140 1000Methyl tert-butyl ether (MTBE)1000 01/24/23 08:31 V29119MSA
1280 µg/L 7.80 1004-Methyl-2-Pentanone 100 01/19/23 11:30 V29021MSA
<33.0 µg/L 33.0 200Methylene Chloride 100 01/19/23 11:30 V29021MSA
631 µg/L 47.0 100Naphthalene 100 01/19/23 11:30 V29021MSA
440 µg/L 19.0 50.0n-Propylbenzene 100 01/19/23 11:30 V29021MSA
<22.0 µg/L 22.0 50.0Styrene 100 01/19/23 11:30 V29021MSA
9000 µg/L 160 1000tert-Butyl Alcohol (TBA)100 01/19/23 11:30 V29021MSA
<35.0 µg/L 35.0 1000tert-Butyl formate (TBF)100 01/19/23 11:30 V29021MSA
48000 µg/L 1900 10000
tert-Amyl Alcohol (TAA)1000 01/24/23 08:31 V29119MSA
89.0 J µg/L 28.0 1000tert-Amyl Methyl Ether (TAME)100 01/19/23 11:30 V29021MSA
<16.0 µg/L 16.0 50.01,1,1,2-Tetrachloroethane 100 01/19/23 11:30 V29021MSA
<16.0 µg/L 16.0 50.01,1,2,2-Tetrachloroethane 100 01/19/23 11:30 V29021MSA
<22.0 µg/L 22.0 50.0Tetrachloroethene 100 01/19/23 11:30 V29021MSA
46600 µg/L 220 500Toluene 1000 01/24/23 08:31 V29119MSA
<38.0 µg/L 38.0 50.01,2,3-Trichlorobenzene 100 01/19/23 11:30 V29021MSA
<31.0 µg/L 31.0 50.0
1,2,4-Trichlorobenzene 100 01/19/23 11:30 V29021MSA
<16.0 µg/L 16.0 50.01,1,1-Trichloroethane 100 01/19/23 11:30 V29021MSA
<9.60 µg/L 9.60 50.01,1,2-Trichloroethane 100 01/19/23 11:30 V29021MSA
<18.0 µg/L 18.0 50.0Trichloroethene 100 01/19/23 11:30 V29021MSA
<18.0 µg/L 18.0 50.0Trichlorofluoromethane 100 01/19/23 11:30 V29021MSA
<27.0 µg/L 27.0 50.01,2,3-Trichloropropane 100 01/19/23 11:30 V29021MSA
3730 µg/L 19.0 50.01,2,4-Trimethylbenzene 100 01/19/23 11:30 V29021MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 11 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-011-0103
00087
Geological Resources, Inc.
3502 Hayes Road
Scott Ball
Monroe
Danyale Love
Project Manager
GRI # 6328 Received : 01/11/2023
Reedy Creek Food Mart
Report Date : 01/24/2023
Sample ID :
Lab No :
Sampled:MW-1
97297 Matrix:
1/11/2023 8:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29020 01/18/23 14:00 V29118 01/23/23 14:00
1010 µg/L 18.0 50.01,3,5-Trimethylbenzene 100 01/19/23 11:30 V29021MSA
<100 µg/L 100 500Vinyl Acetate 100 01/19/23 11:30 V29021MSA
<17.0 µg/L 17.0 50.0Vinyl Chloride 100 01/19/23 11:30 V29021MSA
5540 µg/L 21.0 50.0o-Xylene 100 01/19/23 11:30 V29021MSA
10100 µg/L 42.0 100m,p-Xylene 100 01/19/23 11:30 V29021MSA
15600 µg/L 21.0 50.0Xylene (Total)100 01/19/23 11:30 V29021
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%01/19/23 11:30100 MSA V29021
Surrogate: Dibromofluoromethane 89.4 Limits: 70-130%01/19/23 11:30100 MSA V29021
Surrogate: 1,2-Dichloroethane - d4 96.6 Limits: 70-130%01/19/23 11:30100 MSA V29021
Surrogate: Toluene-d8 102 Limits: 70-130%01/19/23 11:30100 MSA V29021
Surrogate: 4-Bromofluorobenzene 109 Limits: 70-130%01/24/23 08:311000 MSA V29119
Surrogate: Dibromofluoromethane 86.8 Limits: 70-130%01/24/23 08:311000 MSA V29119
Surrogate: 1,2-Dichloroethane - d4 89.8 Limits: 70-130%01/24/23 08:311000 MSA V29119
Surrogate: Toluene-d8 95.8 Limits: 70-130%01/24/23 08:311000 MSA V29119
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 12 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-011-0103
00087
Geological Resources, Inc.
3502 Hayes Road
Scott Ball
Monroe
Danyale Love
Project Manager
GRI # 6328 Received : 01/11/2023
Reedy Creek Food Mart
Report Date : 01/24/2023
Sample ID :
Lab No :
Sampled:MW-1
97297 Matrix:
1/11/2023 8:50
Aqueous
Analytical Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
CALCULATION
65800 µg/L 5750 25000Aliphatic C5-C8 (Adjusted)1000 01/13/23 10:10
18700 µg/L 2580 5000Aliphatics C9-C12 (Adjusted)100 01/12/23 15:27
8370 µg/L 402 5000Aromatic C9-C10 (Adjusted)100 01/12/23 15:27
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V28854 01/13/23 08:00
137000 µg/L 5750 25000Aliphatic C5-C8 500 01/13/23 10:10 V28855TBL
45900 µg/L 2580 5000Aliphatic C9-C12 100 01/12/23 15:27 V28855TBL
8370 µg/L 402 5000Aromatic C9-C10 100 01/12/23 15:27 V28855TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)84.5 Limits: 70-130%01/12/23 15:27100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)79.7 Limits: 70-130%01/12/23 15:27100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)81.1 Limits: 70-130%01/13/23 10:10500 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)76.7 Limits: 70-130%01/13/23 10:10500 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 13 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-011-0103
00087
Geological Resources, Inc.
3502 Hayes Road
Scott Ball
Monroe
Danyale Love
Project Manager
GRI # 6328 Received : 01/11/2023
Reedy Creek Food Mart
Report Date : 01/24/2023
Sample ID :
Lab No :
Sampled:MW-3
97298 Matrix:
1/11/2023 9:20
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 01/19/23 06:04 6200BMSA
See Attached mg/L 0.006Lead 1 6010DBKN
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 14 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-011-0103
00087
Geological Resources, Inc.
3502 Hayes Road
Scott Ball
Monroe
Danyale Love
Project Manager
GRI # 6328 Received : 01/11/2023
Reedy Creek Food Mart
Report Date : 01/24/2023
Sample ID :
Lab No :
Sampled:MW-3
97298 Matrix:
1/11/2023 9:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29020 01/18/23 14:00
<1.80 µg/L 1.80 10.0Acetone 1 01/19/23 06:04 V29021MSA
<0.180 µg/L 0.180 0.500Benzene 1 01/19/23 06:04 V29021MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 01/19/23 06:04 V29021MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 01/19/23 06:04 V29021MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 01/19/23 06:04 V29021MSA
<1.50 µg/L 1.50 5.00Bromoform 1 01/19/23 06:04 V29021MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 01/19/23 06:04 V29021MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 01/19/23 06:04 V29021MSA
<0.200 µg/L 0.200 0.500
sec-Butyl benzene 1 01/19/23 06:04 V29021MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 01/19/23 06:04 V29021MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 01/19/23 06:04 V29021MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 01/19/23 06:04 V29021MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 01/19/23 06:04 V29021MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 01/19/23 06:04 V29021MSA
<0.220 µg/L 0.220 0.500Chloroform 1 01/19/23 06:04 V29021MSA
<0.220 µg/L 0.220 0.500
Chloromethane 1 01/19/23 06:04 V29021MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 01/19/23 06:04 V29021MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 01/19/23 06:04 V29021MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 01/19/23 06:04 V29021MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 01/19/23 06:04 V29021MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 01/19/23 06:04 V29021MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 01/19/23 06:04 V29021MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 15 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-011-0103
00087
Geological Resources, Inc.
3502 Hayes Road
Scott Ball
Monroe
Danyale Love
Project Manager
GRI # 6328 Received : 01/11/2023
Reedy Creek Food Mart
Report Date : 01/24/2023
Sample ID :
Lab No :
Sampled:MW-3
97298 Matrix:
1/11/2023 9:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29020 01/18/23 14:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 01/19/23 06:04 V29021MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 01/19/23 06:04 V29021MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 01/19/23 06:04 V29021MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 01/19/23 06:04 V29021MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 01/19/23 06:04 V29021MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 01/19/23 06:04 V29021MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 01/19/23 06:04 V29021MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 01/19/23 06:04 V29021MSA
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 01/19/23 06:04 V29021MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 01/19/23 06:04 V29021MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 01/19/23 06:04 V29021MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 01/19/23 06:04 V29021MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 01/19/23 06:04 V29021MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 01/19/23 06:04 V29021MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 01/19/23 06:04 V29021MSA
<42.0 µg/L 42.0 200
Ethanol 1 01/19/23 06:04 V29021MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 01/19/23 06:04 V29021MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 01/19/23 06:04 V29021MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 01/19/23 06:04 V29021MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 01/19/23 06:04 V29021MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 01/19/23 06:04 V29021MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 01/19/23 06:04 V29021MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 16 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-011-0103
00087
Geological Resources, Inc.
3502 Hayes Road
Scott Ball
Monroe
Danyale Love
Project Manager
GRI # 6328 Received : 01/11/2023
Reedy Creek Food Mart
Report Date : 01/24/2023
Sample ID :
Lab No :
Sampled:MW-3
97298 Matrix:
1/11/2023 9:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29020 01/18/23 14:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 01/19/23 06:04 V29021MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 01/19/23 06:04 V29021MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 01/19/23 06:04 V29021MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 01/19/23 06:04 V29021MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 01/19/23 06:04 V29021MSA
<0.220 µg/L 0.220 0.500Styrene 1 01/19/23 06:04 V29021MSA
7.00 J µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 01/19/23 06:04 V29021MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 01/19/23 06:04 V29021MSA
<1.90 µg/L 1.90 10.0
tert-Amyl Alcohol (TAA)1 01/19/23 06:04 V29021MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 01/19/23 06:04 V29021MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 01/19/23 06:04 V29021MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 01/19/23 06:04 V29021MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 01/19/23 06:04 V29021MSA
<0.220 µg/L 0.220 0.500Toluene 1 01/19/23 06:04 V29021MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 01/19/23 06:04 V29021MSA
<0.310 µg/L 0.310 0.500
1,2,4-Trichlorobenzene 1 01/19/23 06:04 V29021MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 01/19/23 06:04 V29021MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 01/19/23 06:04 V29021MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 01/19/23 06:04 V29021MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 01/19/23 06:04 V29021MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 01/19/23 06:04 V29021MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 01/19/23 06:04 V29021MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 17 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-011-0103
00087
Geological Resources, Inc.
3502 Hayes Road
Scott Ball
Monroe
Danyale Love
Project Manager
GRI # 6328 Received : 01/11/2023
Reedy Creek Food Mart
Report Date : 01/24/2023
Sample ID :
Lab No :
Sampled:MW-3
97298 Matrix:
1/11/2023 9:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29020 01/18/23 14:00
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 01/19/23 06:04 V29021MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 01/19/23 06:04 V29021MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 01/19/23 06:04 V29021MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 01/19/23 06:04 V29021MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 01/19/23 06:04 V29021MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 01/19/23 06:04 V29021KCC
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%01/19/23 06:041 MSA V29021
Surrogate: Dibromofluoromethane 93.6 Limits: 70-130%01/19/23 06:041 MSA V29021
Surrogate: 1,2-Dichloroethane - d4 95.0 Limits: 70-130%01/19/23 06:041 MSA V29021
Surrogate: Toluene-d8 99.6 Limits: 70-130%01/19/23 06:041 MSA V29021
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 18 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-011-0103
00087
Geological Resources, Inc.
3502 Hayes Road
Scott Ball
Monroe
Danyale Love
Project Manager
GRI # 6328 Received : 01/11/2023
Reedy Creek Food Mart
Report Date : 01/24/2023
Sample ID :
Lab No :
Sampled:MW-3
97298 Matrix:
1/11/2023 9:20
Aqueous
Analytical Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
CALCULATION
<11.5 µg/L 11.5 50.0Aliphatic C5-C8 (Adjusted)1 01/12/23 11:51
<25.8 µg/L 25.8 50.0Aliphatics C9-C12 (Adjusted)1 01/12/23 11:51
<4.02 µg/L 4.02 50.0Aromatic C9-C10 (Adjusted)1 01/12/23 11:51
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V28854 01/13/23 08:00
<11.5 µg/L 11.5 50.0Aliphatic C5-C8 1 01/12/23 11:51 V28855TBL
<25.8 µg/L 25.8 50.0Aliphatic C9-C12 1 01/12/23 11:51 V28855TBL
<4.02 µg/L 4.02 50.0Aromatic C9-C10 1 01/12/23 11:51 V28855TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)81.2 Limits: 70-130%01/12/23 11:511 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)77.1 Limits: 70-130%01/12/23 11:511 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 19 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-011-0103
00087
Geological Resources, Inc.
3502 Hayes Road
Scott Ball
Monroe
Danyale Love
Project Manager
GRI # 6328 Received : 01/11/2023
Reedy Creek Food Mart
Report Date : 01/24/2023
Sample ID :
Lab No :
Sampled:MW-6
97299 Matrix:
1/11/2023 8:40
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<10.0 µg/L 10.0 1003,3-Dimethyl-1-butanol 10 01/19/23 10:40 6200BMSA
See Attached mg/L 0.006Lead 1 6010DBKN
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 20 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-011-0103
00087
Geological Resources, Inc.
3502 Hayes Road
Scott Ball
Monroe
Danyale Love
Project Manager
GRI # 6328 Received : 01/11/2023
Reedy Creek Food Mart
Report Date : 01/24/2023
Sample ID :
Lab No :
Sampled:MW-6
97299 Matrix:
1/11/2023 8:40
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29020 01/18/23 14:00
<18.0 µg/L 18.0 100Acetone 10 01/19/23 10:40 V29021MSA
<1.80 µg/L 1.80 5.00Benzene 10 01/19/23 10:40 V29021MSA
<2.10 µg/L 2.10 5.00Bromobenzene 10 01/19/23 10:40 V29021MSA
<4.20 µg/L 4.20 10.0Bromochloromethane 10 01/19/23 10:40 V29021MSA
<1.60 µg/L 1.60 5.00Bromodichloromethane 10 01/19/23 10:40 V29021MSA
<15.0 µg/L 15.0 50.0Bromoform 10 01/19/23 10:40 V29021MSA
<2.80 µg/L 2.80 10.0Bromomethane 10 01/19/23 10:40 V29021MSA
<1.80 µg/L 1.80 5.00n-Butylbenzene 10 01/19/23 10:40 V29021MSA
<2.00 µg/L 2.00 5.00
sec-Butyl benzene 10 01/19/23 10:40 V29021MSA
<9.20 µg/L 9.20 20.0tert-Butyl benzene 10 01/19/23 10:40 V29021MSA
<1.80 µg/L 1.80 5.00Carbon Tetrachloride 10 01/19/23 10:40 V29021MSA
<1.90 µg/L 1.90 5.00Chlorobenzene 10 01/19/23 10:40 V29021MSA
<1.90 µg/L 1.90 5.00Chlorodibromomethane 10 01/19/23 10:40 V29021MSA
<4.30 µg/L 4.30 10.0Chloroethane 10 01/19/23 10:40 V29021MSA
<2.20 µg/L 2.20 5.00Chloroform 10 01/19/23 10:40 V29021MSA
<2.20 µg/L 2.20 5.00
Chloromethane 10 01/19/23 10:40 V29021MSA
<2.00 µg/L 2.00 5.002-Chlorotoluene 10 01/19/23 10:40 V29021MSA
<2.00 µg/L 2.00 5.004-Chlorotoluene 10 01/19/23 10:40 V29021MSA
17.6 µg/L 5.00 5.00Di-Isopropyl Ether (DIPE)10 01/19/23 10:40 V29021MSA
<11.0 µg/L 11.0 20.01,2-Dibromo-3-Chloropropane 10 01/19/23 10:40 V29021MSA
<2.00 µg/L 2.00 5.001,2-Dibromoethane 10 01/19/23 10:40 V29021MSA
<2.30 µg/L 2.30 5.00Dibromomethane 10 01/19/23 10:40 V29021MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 21 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-011-0103
00087
Geological Resources, Inc.
3502 Hayes Road
Scott Ball
Monroe
Danyale Love
Project Manager
GRI # 6328 Received : 01/11/2023
Reedy Creek Food Mart
Report Date : 01/24/2023
Sample ID :
Lab No :
Sampled:MW-6
97299 Matrix:
1/11/2023 8:40
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29020 01/18/23 14:00
<2.20 µg/L 2.20 5.001,2-Dichlorobenzene 10 01/19/23 10:40 V29021MSA
<1.90 µg/L 1.90 5.001,3-Dichlorobenzene 10 01/19/23 10:40 V29021MSA
<2.10 µg/L 2.10 5.001,4-Dichlorobenzene 10 01/19/23 10:40 V29021MSA
<12.0 µg/L 12.0 50.0Dichlorodifluoromethane 10 01/19/23 10:40 V29021MSA
<2.40 µg/L 2.40 5.001,1-Dichloroethane 10 01/19/23 10:40 V29021MSA
<1.50 µg/L 1.50 5.001,2-Dichloroethane 10 01/19/23 10:40 V29021MSA
<1.50 µg/L 1.50 5.001,1-Dichloroethene 10 01/19/23 10:40 V29021MSA
<2.00 µg/L 2.00 5.00cis-1,2-Dichloroethene 10 01/19/23 10:40 V29021MSA
<1.80 µg/L 1.80 5.00
trans-1,2-Dichloroethene 10 01/19/23 10:40 V29021MSA
<1.90 µg/L 1.90 5.001,2-Dichloropropane 10 01/19/23 10:40 V29021MSA
<1.30 µg/L 1.30 5.001,3-Dichloropropane 10 01/19/23 10:40 V29021MSA
<2.10 µg/L 2.10 20.02,2-Dichloropropane 10 01/19/23 10:40 V29021MSA
<2.00 µg/L 2.00 5.001,1-Dichloropropene 10 01/19/23 10:40 V29021MSA
<2.10 µg/L 2.10 5.00cis-1,3-Dichloropropene 10 01/19/23 10:40 V29021MSA
<1.50 µg/L 1.50 5.00trans-1,3-Dichloropropene 10 01/19/23 10:40 V29021MSA
<420 µg/L 420 2000
Ethanol 10 01/19/23 10:40 V29021MSA
2.22 J µg/L 1.70 5.00Ethylbenzene 10 01/19/23 10:40 V29021MSA
<3.50 µg/L 3.50 30.0Hexachlorobutadiene 10 01/19/23 10:40 V29021MSA
<3.80 µg/L 3.80 10.02-Hexanone 10 01/19/23 10:40 V29021MSA
<1.80 µg/L 1.80 5.00Isopropylbenzene 10 01/19/23 10:40 V29021MSA
<0.890 µg/L 0.890 5.004-Isopropyl toluene 10 01/19/23 10:40 V29021MSA
<7.10 µg/L 7.10 50.0Methyl Ethyl Ketone (MEK)10 01/19/23 10:40 V29021MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 22 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-011-0103
00087
Geological Resources, Inc.
3502 Hayes Road
Scott Ball
Monroe
Danyale Love
Project Manager
GRI # 6328 Received : 01/11/2023
Reedy Creek Food Mart
Report Date : 01/24/2023
Sample ID :
Lab No :
Sampled:MW-6
97299 Matrix:
1/11/2023 8:40
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29020 01/18/23 14:00
103 µg/L 1.40 10.0Methyl tert-butyl ether (MTBE)10 01/19/23 10:40 V29021MSA
<0.780 µg/L 0.780 10.04-Methyl-2-Pentanone 10 01/19/23 10:40 V29021MSA
<3.30 µg/L 3.30 20.0Methylene Chloride 10 01/19/23 10:40 V29021MSA
21.4 µg/L 4.70 10.0Naphthalene 10 01/19/23 10:40 V29021MSA
<1.90 µg/L 1.90 5.00n-Propylbenzene 10 01/19/23 10:40 V29021MSA
<2.20 µg/L 2.20 5.00Styrene 10 01/19/23 10:40 V29021MSA
266 µg/L 16.0 100tert-Butyl Alcohol (TBA)10 01/19/23 10:40 V29021MSA
<3.50 µg/L 3.50 100tert-Butyl formate (TBF)10 01/19/23 10:40 V29021MSA
338 µg/L 19.0 100
tert-Amyl Alcohol (TAA)10 01/19/23 10:40 V29021MSA
<2.80 µg/L 2.80 100tert-Amyl Methyl Ether (TAME)10 01/19/23 10:40 V29021MSA
<1.60 µg/L 1.60 5.001,1,1,2-Tetrachloroethane 10 01/19/23 10:40 V29021MSA
<1.60 µg/L 1.60 5.001,1,2,2-Tetrachloroethane 10 01/19/23 10:40 V29021MSA
<2.20 µg/L 2.20 5.00Tetrachloroethene 10 01/19/23 10:40 V29021MSA
5.45 µg/L 2.20 5.00Toluene 10 01/19/23 10:40 V29021MSA
<3.80 µg/L 3.80 5.001,2,3-Trichlorobenzene 10 01/19/23 10:40 V29021MSA
<3.10 µg/L 3.10 5.00
1,2,4-Trichlorobenzene 10 01/19/23 10:40 V29021MSA
<1.60 µg/L 1.60 5.001,1,1-Trichloroethane 10 01/19/23 10:40 V29021MSA
<0.960 µg/L 0.960 5.001,1,2-Trichloroethane 10 01/19/23 10:40 V29021MSA
<1.80 µg/L 1.80 5.00Trichloroethene 10 01/19/23 10:40 V29021MSA
<1.80 µg/L 1.80 5.00Trichlorofluoromethane 10 01/19/23 10:40 V29021MSA
<2.70 µg/L 2.70 5.001,2,3-Trichloropropane 10 01/19/23 10:40 V29021MSA
4.41 J µg/L 1.90 5.001,2,4-Trimethylbenzene 10 01/19/23 10:40 V29021MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 23 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-011-0103
00087
Geological Resources, Inc.
3502 Hayes Road
Scott Ball
Monroe
Danyale Love
Project Manager
GRI # 6328 Received : 01/11/2023
Reedy Creek Food Mart
Report Date : 01/24/2023
Sample ID :
Lab No :
Sampled:MW-6
97299 Matrix:
1/11/2023 8:40
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29020 01/18/23 14:00
<1.80 µg/L 1.80 5.001,3,5-Trimethylbenzene 10 01/19/23 10:40 V29021MSA
<10.0 µg/L 10.0 50.0Vinyl Acetate 10 01/19/23 10:40 V29021MSA
<1.70 µg/L 1.70 5.00Vinyl Chloride 10 01/19/23 10:40 V29021MSA
3.73 J µg/L 2.10 5.00o-Xylene 10 01/19/23 10:40 V29021MSA
8.44 J µg/L 4.20 10.0m,p-Xylene 10 01/19/23 10:40 V29021MSA
12.2 J µg/L 2.10 5.00Xylene (Total)10 01/19/23 10:40 V29021KCC
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%01/19/23 10:4010 MSA V29021
Surrogate: Dibromofluoromethane 95.4 Limits: 70-130%01/19/23 10:4010 MSA V29021
Surrogate: 1,2-Dichloroethane - d4 93.4 Limits: 70-130%01/19/23 10:4010 MSA V29021
Surrogate: Toluene-d8 95.8 Limits: 70-130%01/19/23 10:4010 MSA V29021
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 24 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-011-0103
00087
Geological Resources, Inc.
3502 Hayes Road
Scott Ball
Monroe
Danyale Love
Project Manager
GRI # 6328 Received : 01/11/2023
Reedy Creek Food Mart
Report Date : 01/24/2023
Sample ID :
Lab No :
Sampled:MW-6
97299 Matrix:
1/11/2023 8:40
Aqueous
Analytical Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
CALCULATION
88.2 µg/L 11.5 50.0Aliphatic C5-C8 (Adjusted)1 01/12/23 12:15
<25.8 µg/L 25.8 50.0Aliphatics C9-C12 (Adjusted)1 01/12/23 12:15
7.67 J µg/L 4.02 50.0Aromatic C9-C10 (Adjusted)1 01/12/23 12:15
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V28854 01/13/23 08:00
93.6 µg/L 11.5 50.0Aliphatic C5-C8 1 01/12/23 12:15 V28855TBL
29.0 J µg/L 25.8 50.0Aliphatic C9-C12 1 01/12/23 12:15 V28855TBL
7.67 J µg/L 4.02 50.0Aromatic C9-C10 1 01/12/23 12:15 V28855TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)86.4 Limits: 70-130%01/12/23 12:151 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)81.7 Limits: 70-130%01/12/23 12:151 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 25 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-011-0103
00087
Geological Resources, Inc.
3502 Hayes Road
Scott Ball
Monroe
Danyale Love
Project Manager
GRI # 6328 Received : 01/11/2023
Reedy Creek Food Mart
Report Date : 01/24/2023
Sample ID :
Lab No :
Sampled:VMW-1
97300 Matrix:
1/11/2023 9:05
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 01/19/23 06:29 6200BMSA
See Attached mg/L 0.006Lead 1 6010DBKN
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 26 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-011-0103
00087
Geological Resources, Inc.
3502 Hayes Road
Scott Ball
Monroe
Danyale Love
Project Manager
GRI # 6328 Received : 01/11/2023
Reedy Creek Food Mart
Report Date : 01/24/2023
Sample ID :
Lab No :
Sampled:VMW-1
97300 Matrix:
1/11/2023 9:05
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29020 01/18/23 14:00
22.3 µg/L 1.80 10.0Acetone 1 01/19/23 06:29 V29021MSA
1.67 µg/L 0.180 0.500Benzene 1 01/19/23 06:29 V29021MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 01/19/23 06:29 V29021MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 01/19/23 06:29 V29021MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 01/19/23 06:29 V29021MSA
<1.50 µg/L 1.50 5.00Bromoform 1 01/19/23 06:29 V29021MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 01/19/23 06:29 V29021MSA
0.235 J µg/L 0.180 0.500n-Butylbenzene 1 01/19/23 06:29 V29021MSA
<0.200 µg/L 0.200 0.500
sec-Butyl benzene 1 01/19/23 06:29 V29021MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 01/19/23 06:29 V29021MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 01/19/23 06:29 V29021MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 01/19/23 06:29 V29021MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 01/19/23 06:29 V29021MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 01/19/23 06:29 V29021MSA
<0.220 µg/L 0.220 0.500Chloroform 1 01/19/23 06:29 V29021MSA
<0.220 µg/L 0.220 0.500
Chloromethane 1 01/19/23 06:29 V29021MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 01/19/23 06:29 V29021MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 01/19/23 06:29 V29021MSA
0.890 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 01/19/23 06:29 V29021MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 01/19/23 06:29 V29021MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 01/19/23 06:29 V29021MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 01/19/23 06:29 V29021MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 27 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-011-0103
00087
Geological Resources, Inc.
3502 Hayes Road
Scott Ball
Monroe
Danyale Love
Project Manager
GRI # 6328 Received : 01/11/2023
Reedy Creek Food Mart
Report Date : 01/24/2023
Sample ID :
Lab No :
Sampled:VMW-1
97300 Matrix:
1/11/2023 9:05
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29020 01/18/23 14:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 01/19/23 06:29 V29021MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 01/19/23 06:29 V29021MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 01/19/23 06:29 V29021MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 01/19/23 06:29 V29021MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 01/19/23 06:29 V29021MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 01/19/23 06:29 V29021MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 01/19/23 06:29 V29021MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 01/19/23 06:29 V29021MSA
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 01/19/23 06:29 V29021MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 01/19/23 06:29 V29021MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 01/19/23 06:29 V29021MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 01/19/23 06:29 V29021MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 01/19/23 06:29 V29021MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 01/19/23 06:29 V29021MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 01/19/23 06:29 V29021MSA
<42.0 µg/L 42.0 200
Ethanol 1 01/19/23 06:29 V29021MSA
1.27 µg/L 0.170 0.500Ethylbenzene 1 01/19/23 06:29 V29021MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 01/19/23 06:29 V29021MSA
0.807 J µg/L 0.380 1.002-Hexanone 1 01/19/23 06:29 V29021MSA
0.207 J µg/L 0.180 0.500Isopropylbenzene 1 01/19/23 06:29 V29021MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 01/19/23 06:29 V29021MSA
4.53 J µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 01/19/23 06:29 V29021MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 28 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-011-0103
00087
Geological Resources, Inc.
3502 Hayes Road
Scott Ball
Monroe
Danyale Love
Project Manager
GRI # 6328 Received : 01/11/2023
Reedy Creek Food Mart
Report Date : 01/24/2023
Sample ID :
Lab No :
Sampled:VMW-1
97300 Matrix:
1/11/2023 9:05
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29020 01/18/23 14:00
0.786 J µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 01/19/23 06:29 V29021MSA
1.04 µg/L 0.078 1.004-Methyl-2-Pentanone 1 01/19/23 06:29 V29021MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 01/19/23 06:29 V29021MSA
1.93 µg/L 0.470 1.00Naphthalene 1 01/19/23 06:29 V29021MSA
0.777 µg/L 0.190 0.500n-Propylbenzene 1 01/19/23 06:29 V29021MSA
<0.220 µg/L 0.220 0.500Styrene 1 01/19/23 06:29 V29021MSA
10.4 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 01/19/23 06:29 V29021MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 01/19/23 06:29 V29021MSA
16.9 µg/L 1.90 10.0
tert-Amyl Alcohol (TAA)1 01/19/23 06:29 V29021MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 01/19/23 06:29 V29021MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 01/19/23 06:29 V29021MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 01/19/23 06:29 V29021MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 01/19/23 06:29 V29021MSA
8.52 µg/L 0.220 0.500Toluene 1 01/19/23 06:29 V29021MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 01/19/23 06:29 V29021MSA
<0.310 µg/L 0.310 0.500
1,2,4-Trichlorobenzene 1 01/19/23 06:29 V29021MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 01/19/23 06:29 V29021MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 01/19/23 06:29 V29021MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 01/19/23 06:29 V29021MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 01/19/23 06:29 V29021MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 01/19/23 06:29 V29021MSA
11.1 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 01/19/23 06:29 V29021MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 29 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-011-0103
00087
Geological Resources, Inc.
3502 Hayes Road
Scott Ball
Monroe
Danyale Love
Project Manager
GRI # 6328 Received : 01/11/2023
Reedy Creek Food Mart
Report Date : 01/24/2023
Sample ID :
Lab No :
Sampled:VMW-1
97300 Matrix:
1/11/2023 9:05
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29020 01/18/23 14:00
4.65 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 01/19/23 06:29 V29021MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 01/19/23 06:29 V29021MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 01/19/23 06:29 V29021MSA
6.65 µg/L 0.210 0.500o-Xylene 1 01/19/23 06:29 V29021MSA
9.26 µg/L 0.420 1.00m,p-Xylene 1 01/19/23 06:29 V29021MSA
15.9 µg/L 0.210 0.500Xylene (Total)1 01/19/23 06:29 V29021KCC
Surrogate: 4-Bromofluorobenzene 97.4 Limits: 70-130%01/19/23 06:291 MSA V29021
Surrogate: Dibromofluoromethane 93.0 Limits: 70-130%01/19/23 06:291 MSA V29021
Surrogate: 1,2-Dichloroethane - d4 93.8 Limits: 70-130%01/19/23 06:291 MSA V29021
Surrogate: Toluene-d8 96.4 Limits: 70-130%01/19/23 06:291 MSA V29021
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 30 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-011-0103
00087
Geological Resources, Inc.
3502 Hayes Road
Scott Ball
Monroe
Danyale Love
Project Manager
GRI # 6328 Received : 01/11/2023
Reedy Creek Food Mart
Report Date : 01/24/2023
Sample ID :
Lab No :
Sampled:VMW-1
97300 Matrix:
1/11/2023 9:05
Aqueous
Analytical Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
CALCULATION
<11.5 µg/L 11.5 50.0Aliphatic C5-C8 (Adjusted)1 01/13/23 11:35
71.0 J µg/L 25.8 50.0Aliphatics C9-C12 (Adjusted)1 01/13/23 11:35
24.8 J µg/L 4.02 50.0Aromatic C9-C10 (Adjusted)1 01/13/23 11:35
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V28854 01/13/23 08:00
12.1 J µg/L 11.5 50.0Aliphatic C5-C8 1 01/13/23 11:35 V28855TBL
113 µg/L 25.8 50.0Aliphatic C9-C12 1 01/13/23 11:35 V28855TBL
24.8 J µg/L 4.02 50.0Aromatic C9-C10 1 01/13/23 11:35 V28855TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)81.4 Limits: 70-130%01/13/23 11:351 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)77.1 Limits: 70-130%01/13/23 11:351 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 31 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-011-0103
00087
Geological Resources, Inc.
3502 Hayes Road
Scott Ball
Monroe
Danyale Love
Project Manager
GRI # 6328 Received : 01/11/2023
Reedy Creek Food Mart
Report Date : 01/24/2023
Sample ID :
Lab No :
Sampled:TB
97301 Matrix:
1/11/2023 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29020 01/18/23 14:00
<1.80 µg/L 1.80 10.0Acetone 1 01/19/23 05:14 V29021MSA
<0.180 µg/L 0.180 0.500Benzene 1 01/19/23 05:14 V29021MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 01/19/23 05:14 V29021MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 01/19/23 05:14 V29021MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 01/19/23 05:14 V29021MSA
<1.50 µg/L 1.50 5.00Bromoform 1 01/19/23 05:14 V29021MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 01/19/23 05:14 V29021MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 01/19/23 05:14 V29021MSA
<0.200 µg/L 0.200 0.500
sec-Butyl benzene 1 01/19/23 05:14 V29021MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 01/19/23 05:14 V29021MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 01/19/23 05:14 V29021MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 01/19/23 05:14 V29021MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 01/19/23 05:14 V29021MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 01/19/23 05:14 V29021MSA
<0.220 µg/L 0.220 0.500Chloroform 1 01/19/23 05:14 V29021MSA
<0.220 µg/L 0.220 0.500
Chloromethane 1 01/19/23 05:14 V29021MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 01/19/23 05:14 V29021MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 01/19/23 05:14 V29021MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 01/19/23 05:14 V29021MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 01/19/23 05:14 V29021MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 01/19/23 05:14 V29021MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 01/19/23 05:14 V29021MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 32 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-011-0103
00087
Geological Resources, Inc.
3502 Hayes Road
Scott Ball
Monroe
Danyale Love
Project Manager
GRI # 6328 Received : 01/11/2023
Reedy Creek Food Mart
Report Date : 01/24/2023
Sample ID :
Lab No :
Sampled:TB
97301 Matrix:
1/11/2023 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29020 01/18/23 14:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 01/19/23 05:14 V29021MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 01/19/23 05:14 V29021MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 01/19/23 05:14 V29021MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 01/19/23 05:14 V29021MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 01/19/23 05:14 V29021MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 01/19/23 05:14 V29021MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 01/19/23 05:14 V29021MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 01/19/23 05:14 V29021MSA
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 01/19/23 05:14 V29021MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 01/19/23 05:14 V29021MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 01/19/23 05:14 V29021MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 01/19/23 05:14 V29021MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 01/19/23 05:14 V29021MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 01/19/23 05:14 V29021MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 01/19/23 05:14 V29021MSA
<42.0 µg/L 42.0 200
Ethanol 1 01/19/23 05:14 V29021MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 01/19/23 05:14 V29021MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 01/19/23 05:14 V29021MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 01/19/23 05:14 V29021MSA
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 01/19/23 05:14 V29021MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 01/19/23 05:14 V29021MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 01/19/23 05:14 V29021MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 33 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-011-0103
00087
Geological Resources, Inc.
3502 Hayes Road
Scott Ball
Monroe
Danyale Love
Project Manager
GRI # 6328 Received : 01/11/2023
Reedy Creek Food Mart
Report Date : 01/24/2023
Sample ID :
Lab No :
Sampled:TB
97301 Matrix:
1/11/2023 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29020 01/18/23 14:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 01/19/23 05:14 V29021MSA
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 01/19/23 05:14 V29021MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 01/19/23 05:14 V29021MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 01/19/23 05:14 V29021MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 01/19/23 05:14 V29021MSA
<0.220 µg/L 0.220 0.500Styrene 1 01/19/23 05:14 V29021MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 01/19/23 05:14 V29021MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 01/19/23 05:14 V29021MSA
<0.220 µg/L 0.220 0.500
Tetrachloroethene 1 01/19/23 05:14 V29021MSA
<0.220 µg/L 0.220 0.500Toluene 1 01/19/23 05:14 V29021MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 01/19/23 05:14 V29021MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 01/19/23 05:14 V29021MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 01/19/23 05:14 V29021MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 01/19/23 05:14 V29021MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 01/19/23 05:14 V29021MSA
<0.180 µg/L 0.180 0.500
Trichlorofluoromethane 1 01/19/23 05:14 V29021MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 01/19/23 05:14 V29021MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 01/19/23 05:14 V29021MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 01/19/23 05:14 V29021MSA
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 01/19/23 05:14 V29021MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 01/19/23 05:14 V29021MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 01/19/23 05:14 V29021MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 34 of 61
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
23-011-0103
00087
Geological Resources, Inc.
3502 Hayes Road
Scott Ball
Monroe
Danyale Love
Project Manager
GRI # 6328 Received : 01/11/2023
Reedy Creek Food Mart
Report Date : 01/24/2023
Sample ID :
Lab No :
Sampled:TB
97301 Matrix:
1/11/2023 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V29020 01/18/23 14:00
<0.420 µg/L 0.420 1.00m,p-Xylene 1 01/19/23 05:14 V29021MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 01/19/23 05:14 V29021
Surrogate: 4-Bromofluorobenzene 106 Limits: 70-130%01/19/23 05:141 MSA V29021
Surrogate: Dibromofluoromethane 98.2 Limits: 70-130%01/19/23 05:141 MSA V29021
Surrogate: 1,2-Dichloroethane - d4 97.0 Limits: 70-130%01/19/23 05:141 MSA V29021
Surrogate: Toluene-d8 99.8 Limits: 70-130%01/19/23 05:141 MSA V29021
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 35 of 61
ANALYTICAL REPORT
PREPARED FOR
Attn: PM Group NC
Waypoint Analytical, Inc.
449 Springbrook Road
Charlotte, North Carolina 28217
Generated 1/20/2023 2:43:05 PM
JOB DESCRIPTION
23-011-0103
JOB NUMBER
680-229208-1
See page two for job notes and contact information.
Savannah GA 31404
5102 LaRoche Avenue
Eurofins Savannah
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Eurofins Savannah
Eurofins Savannah is a laboratory within Eurofins Environment Testing Southeast, LLC, a company within Eurofins Environment Testing Group of Companies
Job Notes
The test results in this report meet NELAP requirements for parameters for which accreditation is required or available. Any
exceptions to the NELAP requirements are noted. Results pertain only to samples listed in this report. This report may not be
reproduced, except in full, without the written approval of the laboratory. Questions should be directed to the person who
signed this report.
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins Environment Testing Southeast, LLC Project
Manager.
Authorization
Generated
1/20/2023 2:43:05 PM
Authorized for release by
John Andros, Project Manager I
[e-mail]
[phone]
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Definitions/Glossary
Job ID: 680-229208-1Client: Waypoint Analytical, Inc.
Project/Site: 23-011-0103
Glossary
These commonly used abbreviations may or may not be present in this report.
¤ Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins Savannah
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Page 38 of 61
Sample Summary
Client: Waypoint Analytical, Inc.Job ID: 680-229208-1
Project/Site: 23-011-0103
Lab Sample ID Client Sample ID Matrix Collected Received
680-229208-1 MW-1 / 97297 Water 01/11/23 08:50 01/17/23 10:00
680-229208-2 MW-3 / 97298 Water 01/11/23 09:20 01/17/23 10:00
680-229208-3 MW-6 / 97299 Water 01/11/23 08:40 01/17/23 10:00
680-229208-4 VMW-1 / 97300 Water 01/11/23 09:05 01/17/23 10:00
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Page 39 of 61
Case Narrative
Client: Waypoint Analytical, Inc.Job ID: 680-229208-1
Project/Site: 23-011-0103
Job ID: 680-229208-1
Laboratory: Eurofins Savannah
Narrative
Job Narrative
680-229208-1
Receipt
The samples were received on 1/17/2023 10:00 AM. Unless otherwise noted below, the samples arrived in good condition, and, where
required, properly preserved and on ice. The temperature of the cooler at receipt time was 16.3°C
Metals
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
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Page 40 of 61
Client Sample Results
Job ID: 680-229208-1Client: Waypoint Analytical, Inc.
Project/Site: 23-011-0103
Lab Sample ID: 680-229208-1Client Sample ID: MW-1 / 97297
Matrix: WaterDate Collected: 01/11/23 08:50
Date Received: 01/17/23 10:00
Method: SW846 6010D - Metals (ICP) - Total Recoverable
RL MDL
634 10.0 6.60 ug/L 01/18/23 05:47 01/19/23 14:48 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Lead
Eurofins Savannah
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Client Sample Results
Job ID: 680-229208-1Client: Waypoint Analytical, Inc.
Project/Site: 23-011-0103
Lab Sample ID: 680-229208-2Client Sample ID: MW-3 / 97298
Matrix: WaterDate Collected: 01/11/23 09:20
Date Received: 01/17/23 10:00
Method: SW846 6010D - Metals (ICP) - Total Recoverable
RL MDL
15.1 10.0 6.60 ug/L 01/18/23 05:47 01/19/23 14:45 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Lead
Eurofins Savannah
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Client Sample Results
Job ID: 680-229208-1Client: Waypoint Analytical, Inc.
Project/Site: 23-011-0103
Lab Sample ID: 680-229208-3Client Sample ID: MW-6 / 97299
Matrix: WaterDate Collected: 01/11/23 08:40
Date Received: 01/17/23 10:00
Method: SW846 6010D - Metals (ICP) - Total Recoverable
RL MDL
14.1 10.0 6.60 ug/L 01/18/23 05:47 01/19/23 14:36 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Lead
Eurofins Savannah
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Client Sample Results
Job ID: 680-229208-1Client: Waypoint Analytical, Inc.
Project/Site: 23-011-0103
Lab Sample ID: 680-229208-4Client Sample ID: VMW-1 / 97300
Matrix: WaterDate Collected: 01/11/23 09:05
Date Received: 01/17/23 10:00
Method: SW846 6010D - Metals (ICP) - Total Recoverable
RL MDL
ND 10.0 6.60 ug/L 01/18/23 05:47 01/19/23 14:39 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Lead
Eurofins Savannah
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QC Sample Results
Job ID: 680-229208-1Client: Waypoint Analytical, Inc.
Project/Site: 23-011-0103
Method: 6010D - Metals (ICP)
Client Sample ID: Method BlankLab Sample ID: MB 680-759436/1-A
Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 759797 Prep Batch: 759436
RL MDL
Lead ND 10.0 6.60 ug/L 01/18/23 05:47 01/19/23 14:03 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-759436/2-A
Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 759797 Prep Batch: 759436
Lead 505 516.4 ug/L 102 80-120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
Client Sample ID: Matrix SpikeLab Sample ID: 680-229237-F-1-B MS
Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 759797 Prep Batch: 759436
Lead ND 505 499.5 ug/L 99 75-125
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 680-229237-F-1-C MSD
Matrix: Water Prep Type: Total Recoverable
Analysis Batch: 759797 Prep Batch: 759436
Lead ND 505 515.3 ug/L 102 75-125 3 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
Eurofins Savannah
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QC Association Summary
Job ID: 680-229208-1Client: Waypoint Analytical, Inc.
Project/Site: 23-011-0103
Metals
Prep Batch: 759436
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3005A680-229208-1 MW-1 / 97297 Total Recoverable
Water 3005A680-229208-2 MW-3 / 97298 Total Recoverable
Water 3005A680-229208-3 MW-6 / 97299 Total Recoverable
Water 3005A680-229208-4 VMW-1 / 97300 Total Recoverable
Water 3005AMB 680-759436/1-A Method Blank Total Recoverable
Water 3005ALCS 680-759436/2-A Lab Control Sample Total Recoverable
Water 3005A680-229237-F-1-B MS Matrix Spike Total Recoverable
Water 3005A680-229237-F-1-C MSD Matrix Spike Duplicate Total Recoverable
Analysis Batch: 759797
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6010D 759436680-229208-1 MW-1 / 97297 Total Recoverable
Water 6010D 759436680-229208-2 MW-3 / 97298 Total Recoverable
Water 6010D 759436680-229208-3 MW-6 / 97299 Total Recoverable
Water 6010D 759436680-229208-4 VMW-1 / 97300 Total Recoverable
Water 6010D 759436MB 680-759436/1-A Method Blank Total Recoverable
Water 6010D 759436LCS 680-759436/2-A Lab Control Sample Total Recoverable
Water 6010D 759436680-229237-F-1-B MS Matrix Spike Total Recoverable
Water 6010D 759436680-229237-F-1-C MSD Matrix Spike Duplicate Total Recoverable
Eurofins Savannah
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Page 46 of 61
Lab Chronicle
Client: Waypoint Analytical, Inc.Job ID: 680-229208-1
Project/Site: 23-011-0103
Client Sample ID: MW-1 / 97297 Lab Sample ID: 680-229208-1
Matrix: WaterDate Collected: 01/11/23 08:50
Date Received: 01/17/23 10:00
Prep 3005A RR01/18/23 05:47 EET SAV759436
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total Recoverable 50 mL 50 mL
Analysis 6010D 1 759797 01/19/23 14:48 BCB EET SAVTotal Recoverable
ICPHInstrument ID:
Client Sample ID: MW-3 / 97298 Lab Sample ID: 680-229208-2
Matrix: WaterDate Collected: 01/11/23 09:20
Date Received: 01/17/23 10:00
Prep 3005A RR01/18/23 05:47 EET SAV759436
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total Recoverable 50 mL 50 mL
Analysis 6010D 1 759797 01/19/23 14:45 BCB EET SAVTotal Recoverable
ICPHInstrument ID:
Client Sample ID: MW-6 / 97299 Lab Sample ID: 680-229208-3
Matrix: WaterDate Collected: 01/11/23 08:40
Date Received: 01/17/23 10:00
Prep 3005A RR01/18/23 05:47 EET SAV759436
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total Recoverable 50 mL 50 mL
Analysis 6010D 1 759797 01/19/23 14:36 BCB EET SAVTotal Recoverable
ICPHInstrument ID:
Client Sample ID: VMW-1 / 97300 Lab Sample ID: 680-229208-4
Matrix: WaterDate Collected: 01/11/23 09:05
Date Received: 01/17/23 10:00
Prep 3005A RR01/18/23 05:47 EET SAV759436
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total Recoverable 50 mL 50 mL
Analysis 6010D 1 759797 01/19/23 14:39 BCB EET SAVTotal Recoverable
ICPHInstrument ID:
Laboratory References:
EET SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins Savannah
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Accreditation/Certification Summary
Client: Waypoint Analytical, Inc.Job ID: 680-229208-1
Project/Site: 23-011-0103
Laboratory: Eurofins Savannah
The accreditations/certifications listed below are applicable to this report.
Authority Program Identification Number Expiration Date
North Carolina (WW/SW) State 269 12-31-23
South Carolina State 98001 06-30-23
Eurofins Savannah
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Method Summary
Job ID: 680-229208-1Client: Waypoint Analytical, Inc.
Project/Site: 23-011-0103
Method Method Description LaboratoryProtocol
SW8466010D Metals (ICP)EET SAV
SW8463005A Preparation, Total Recoverable or Dissolved Metals EET SAV
Protocol References:
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
EET SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins Savannah
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Login Sample Receipt Checklist
Client: Waypoint Analytical, Inc.Job Number: 680-229208-1
Login Number: 229208
Question Answer Comment
Creator: Sims, Robert D
List Source: Eurofins Savannah
List Number: 1
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
FalseSamples were received on ice.Thermal preservation not required.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
N/AContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins Savannah
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Page 51 of 61
Quality Control Data
23-011-0103Report No:
Project Description:
Client ID:Geological Resources, Inc.
Reedy Creek Food Mart
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V29021QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V29020
Associated Lab Samples: 97297, 97298, 97299, 97300, 97301
LRB-V29020 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
01/19/23 03:5810.01.80<1.80µg/LAcetone
01/19/23 03:580.5000.180<0.180µg/LBenzene
01/19/23 03:580.5000.210<0.210µg/LBromobenzene
01/19/23 03:581.000.420<0.420µg/LBromochloromethane
01/19/23 03:580.5000.160<0.160µg/LBromodichloromethane
01/19/23 03:585.001.50<1.50µg/LBromoform
01/19/23 03:581.000.280<0.280µg/LBromomethane
01/19/23 03:580.5000.180<0.180µg/Ln-Butylbenzene
01/19/23 03:580.5000.200<0.200µg/Lsec-Butyl benzene
01/19/23 03:582.000.920<0.920µg/Ltert-Butyl benzene
01/19/23 03:580.5000.180<0.180µg/LCarbon Tetrachloride
01/19/23 03:580.5000.190<0.190µg/LChlorobenzene
01/19/23 03:580.5000.190<0.190µg/LChlorodibromomethane
01/19/23 03:581.000.430<0.430µg/LChloroethane
01/19/23 03:580.5000.220<0.220µg/LChloroform
01/19/23 03:580.5000.220<0.220µg/LChloromethane
01/19/23 03:580.5000.200<0.200µg/L2-Chlorotoluene
01/19/23 03:580.5000.200<0.200µg/L4-Chlorotoluene
01/19/23 03:580.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
01/19/23 03:582.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
01/19/23 03:580.5000.200<0.200µg/L1,2-Dibromoethane
01/19/23 03:580.5000.230<0.230µg/LDibromomethane
01/19/23 03:580.5000.220<0.220µg/L1,2-Dichlorobenzene
01/19/23 03:580.5000.190<0.190µg/L1,3-Dichlorobenzene
01/19/23 03:580.5000.210<0.210µg/L1,4-Dichlorobenzene
01/19/23 03:585.001.20<1.20µg/LDichlorodifluoromethane
01/19/23 03:580.5000.240<0.240µg/L1,1-Dichloroethane
Page 1 of 8Date:01/24/2023 04:30 PM
Page 52 of 61
Quality Control Data
23-011-0103Report No:
Project Description:
Client ID:Geological Resources, Inc.
Reedy Creek Food Mart
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V29021QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V29020
Associated Lab Samples: 97297, 97298, 97299, 97300, 97301
LRB-V29020 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
01/19/23 03:580.5000.150<0.150µg/L1,2-Dichloroethane
01/19/23 03:580.5000.150<0.150µg/L1,1-Dichloroethene
01/19/23 03:580.5000.200<0.200µg/Lcis-1,2-Dichloroethene
01/19/23 03:580.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
01/19/23 03:580.5000.190<0.190µg/L1,2-Dichloropropane
01/19/23 03:580.5000.130<0.130µg/L1,3-Dichloropropane
01/19/23 03:582.000.210<0.210µg/L2,2-Dichloropropane
01/19/23 03:580.5000.200<0.200µg/L1,1-Dichloropropene
01/19/23 03:580.5000.210<0.210µg/Lcis-1,3-Dichloropropene
01/19/23 03:580.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
01/19/23 03:5820042.0<42.0µg/LEthanol
01/19/23 03:580.5000.170<0.170µg/LEthylbenzene
01/19/23 03:583.000.350<0.350µg/LHexachlorobutadiene
01/19/23 03:581.000.380<0.380µg/L2-Hexanone
01/19/23 03:580.5000.180<0.180µg/LIsopropylbenzene
01/19/23 03:580.5000.089<0.089µg/L4-Isopropyl toluene
01/19/23 03:585.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
01/19/23 03:581.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
01/19/23 03:581.000.078<0.078µg/L4-Methyl-2-Pentanone
01/19/23 03:582.000.330<0.330µg/LMethylene Chloride
01/19/23 03:581.000.470<0.470µg/LNaphthalene
01/19/23 03:580.5000.190<0.190µg/Ln-Propylbenzene
01/19/23 03:580.5000.220<0.220µg/LStyrene
01/19/23 03:5810.01.60<1.60µg/Ltert-Butyl Alcohol (TBA)
01/19/23 03:5810.00.350<0.350µg/Ltert-Butyl formate (TBF)
01/19/23 03:5810.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
01/19/23 03:5810.00.280<0.280µg/Ltert-Amyl Methyl Ether (TAME)
Page 2 of 8Date:01/24/2023 04:30 PM
Page 53 of 61
Quality Control Data
23-011-0103Report No:
Project Description:
Client ID:Geological Resources, Inc.
Reedy Creek Food Mart
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V29021QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V29020
Associated Lab Samples: 97297, 97298, 97299, 97300, 97301
LRB-V29020 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
01/19/23 03:580.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
01/19/23 03:580.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
01/19/23 03:580.5000.220<0.220µg/LTetrachloroethene
01/19/23 03:580.5000.220<0.220µg/LToluene
01/19/23 03:580.5000.380<0.380µg/L1,2,3-Trichlorobenzene
01/19/23 03:580.5000.310<0.310µg/L1,2,4-Trichlorobenzene
01/19/23 03:580.5000.160<0.160µg/L1,1,1-Trichloroethane
01/19/23 03:580.5000.096<0.096µg/L1,1,2-Trichloroethane
01/19/23 03:580.5000.180<0.180µg/LTrichloroethene
01/19/23 03:580.5000.180<0.180µg/LTrichlorofluoromethane
01/19/23 03:580.5000.270<0.270µg/L1,2,3-Trichloropropane
01/19/23 03:580.5000.190<0.190µg/L1,2,4-Trimethylbenzene
01/19/23 03:580.5000.180<0.180µg/L1,3,5-Trimethylbenzene
01/19/23 03:585.001.00<1.00µg/LVinyl Acetate
01/19/23 03:580.5000.170<0.170µg/LVinyl Chloride
01/19/23 03:580.5000.210<0.210µg/Lo-Xylene
01/19/23 03:581.000.420<0.420µg/Lm,p-Xylene
01/19/23 03:5810.01.00<1.00µg/L3,3-Dimethyl-1-butanol
01/19/23 03:584-Bromofluorobenzene (S)123 70-130
01/19/23 03:58Dibromofluoromethane (S)93.0 70-130
01/19/23 03:581,2-Dichloroethane - d4 (S)97.0 70-130
01/19/23 03:58Toluene-d8 (S)95.4 70-130
Page 3 of 8Date:01/24/2023 04:30 PM
Page 54 of 61
Quality Control Data
23-011-0103Report No:
Project Description:
Client ID:Geological Resources, Inc.
Reedy Creek Food Mart
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V29021QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V29020
LCS-V29020 LCSD-V29020Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
24.2 60.562.525.040.0µg/LAcetone 40-160 3.2 20.0
19.3 96.599.019.820.0µg/LBenzene 70-130 2.5 20.0
20.4 10210621.220.0µg/LBromobenzene 70-130 3.8 20.0
20.3 10210220.320.0µg/LBromochloromethane 70-130 0.0 20.0
19.6 98.099.019.820.0µg/LBromodichloromethane 70-130 1.0 20.0
18.1 90.598.519.720.0µg/LBromoform 70-130 8.4 20.0
17.8 89.087.017.420.0µg/LBromomethane 60-140 2.2 20.0
20.1 10110521.020.0µg/Ln-Butylbenzene 70-130 4.3 20.0
19.8 99.010220.420.0µg/Lsec-Butyl benzene 70-130 2.9 20.0
19.7 98.510320.620.0µg/Ltert-Butyl benzene 70-130 4.4 20.0
18.8 94.096.019.220.0µg/LCarbon Tetrachloride 70-130 2.1 20.0
20.3 10210821.620.0µg/LChlorobenzene 70-130 6.2 20.0
18.3 91.591.018.220.0µg/LChlorodibromomethane 70-130 0.5 20.0
20.8 10410520.920.0µg/LChloroethane 60-140 0.4 20.0
20.1 10110320.520.0µg/LChloroform 70-130 1.9 20.0
18.9 94.597.019.420.0µg/LChloromethane 60-140 2.6 20.0
20.1 10110420.820.0µg/L2-Chlorotoluene 70-130 3.4 20.0
19.8 99.010520.920.0µg/L4-Chlorotoluene 70-130 5.4 20.0
19.2 96.010020.020.0µg/LDi-Isopropyl Ether (DIPE)70-130 4.0 20.0
18.6 93.085.517.120.0µg/L1,2-Dibromo-3-Chloropropane 70-130 8.4 20.0
19.4 97.010020.020.0µg/L1,2-Dibromoethane 70-130 3.0 20.0
19.7 98.594.518.920.0µg/LDibromomethane 70-130 4.1 20.0
19.7 98.510420.820.0µg/L1,2-Dichlorobenzene 70-130 5.4 20.0
19.5 97.510521.020.0µg/L1,3-Dichlorobenzene 70-130 7.4 20.0
19.4 97.010420.720.0µg/L1,4-Dichlorobenzene 70-130 6.4 20.0
21.8 10910621.220.0µg/LDichlorodifluoromethane 60-140 2.7 20.0
Page 4 of 8Date:01/24/2023 04:30 PM
Page 55 of 61
Quality Control Data
23-011-0103Report No:
Project Description:
Client ID:Geological Resources, Inc.
Reedy Creek Food Mart
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V29021QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V29020
LCS-V29020 LCSD-V29020Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
19.8 99.010420.720.0µg/L1,1-Dichloroethane 70-130 4.4 20.0
19.4 97.097.019.420.0µg/L1,2-Dichloroethane 70-130 0.0 20.0
19.5 97.510220.320.0µg/L1,1-Dichloroethene 70-130 4.0 20.0
19.5 97.510520.920.0µg/Lcis-1,2-Dichloroethene 70-130 6.9 20.0
20.8 10410721.320.0µg/Ltrans-1,2-Dichloroethene 70-130 2.3 20.0
20.1 10110320.620.0µg/L1,2-Dichloropropane 70-130 2.4 20.0
19.2 96.099.019.820.0µg/L1,3-Dichloropropane 70-130 3.0 20.0
17.9 89.589.017.820.0µg/L2,2-Dichloropropane 70-130 0.5 20.0
20.6 10310220.420.0µg/L1,1-Dichloropropene 70-130 0.9 20.0
19.9 99.596.019.220.0µg/Lcis-1,3-Dichloropropene 70-130 3.5 20.0
19.7 98.595.019.020.0µg/Ltrans-1,3-Dichloropropene 70-130 3.6 20.0
388 77.677.4387500µg/LEthanol 60-140 0.2 20.0
19.3 96.510621.120.0µg/LEthylbenzene 70-130 8.9 20.0
20.5 10396.019.220.0µg/LHexachlorobutadiene 70-130 6.5 20.0
14.9 74.578.515.720.0µg/L2-Hexanone 60-140 5.2 20.0
21.1 10611022.020.0µg/LIsopropylbenzene 70-130 4.1 20.0
20.0 10010320.620.0µg/L4-Isopropyl toluene 70-130 2.9 20.0
15.7 78.570.014.020.0µg/LMethyl Ethyl Ketone (MEK)60-140 11.4 20.0
18.6 93.094.518.920.0µg/LMethyl tert-butyl ether (MTBE)70-130 1.6 20.0
15.6 78.078.515.720.0µg/L4-Methyl-2-Pentanone 60-140 0.6 20.0
20.1 10110220.320.0µg/LMethylene Chloride 70-130 0.9 20.0
19.8 99.010420.720.0µg/LNaphthalene 70-130 4.4 20.0
20.4 10210621.220.0µg/Ln-Propylbenzene 70-130 3.8 20.0
18.7 93.510621.120.0µg/LStyrene 70-130 12.0 20.0
27.6 69.071.528.640.0µg/Ltert-Butyl Alcohol (TBA)40-140 3.5 20.0
35.2 88.075.230.140.0µg/Ltert-Butyl formate (TBF)40-140 15.6 20.0
Page 5 of 8Date:01/24/2023 04:30 PM
Page 56 of 61
Quality Control Data
23-011-0103Report No:
Project Description:
Client ID:Geological Resources, Inc.
Reedy Creek Food Mart
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V29021QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V29020
LCS-V29020 LCSD-V29020Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
15.6 78.068.513.720.0µg/Ltert-Amyl Alcohol (TAA)40-140 12.9 20.0
38.8 97.095.738.340.0µg/Ltert-Amyl Methyl Ether (TAME)40-140 1.2 20.0
21.3 10711122.220.0µg/L1,1,1,2-Tetrachloroethane 70-130 4.1 20.0
18.2 91.093.018.620.0µg/L1,1,2,2-Tetrachloroethane 70-130 2.1 20.0
21.3 10711222.420.0µg/LTetrachloroethene 70-130 5.0 20.0
20.4 10298.019.620.0µg/LToluene 70-130 4.0 20.0
23.3 11711122.120.0µg/L1,2,3-Trichlorobenzene 70-130 5.2 20.0
21.4 10710821.620.0µg/L1,2,4-Trichlorobenzene 70-130 0.9 20.0
20.2 10110120.220.0µg/L1,1,1-Trichloroethane 70-130 0.0 20.0
19.2 96.094.018.820.0µg/L1,1,2-Trichloroethane 70-130 2.1 20.0
20.2 10110520.920.0µg/LTrichloroethene 70-130 3.4 20.0
20.0 10010020.020.0µg/LTrichlorofluoromethane 60-140 0.0 20.0
17.5 87.590.018.020.0µg/L1,2,3-Trichloropropane 70-130 2.8 20.0
20.3 10210621.120.0µg/L1,2,4-Trimethylbenzene 70-130 3.8 20.0
20.2 10110721.320.0µg/L1,3,5-Trimethylbenzene 70-130 5.3 20.0
15.8 79.070.514.120.0µg/LVinyl Acetate 60-140 11.3 20.0
20.7 10410621.120.0µg/LVinyl Chloride 60-140 1.9 20.0
19.3 96.510521.020.0µg/Lo-Xylene 70-130 8.4 20.0
40.1 10010943.540.0µg/Lm,p-Xylene 70-130 8.1 20.0
17.1 85.580.016.020.0µg/L3,3-Dimethyl-1-butanol 70-130 6.6 20.0
98.61034-Bromofluorobenzene (S)70-130
98.096.2Dibromofluoromethane (S)70-130
97.296.21,2-Dichloroethane - d4 (S)70-130
101104Toluene-d8 (S)70-130
Page 6 of 8Date:01/24/2023 04:30 PM
Page 57 of 61
Quality Control Data
23-011-0103Report No:
Project Description:
Client ID:Geological Resources, Inc.
Reedy Creek Food Mart
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V29119QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V29118
Associated Lab Samples: 97297
LRB-V29118 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
01/24/23 01:0110.01.80<1.80µg/LAcetone
01/24/23 01:010.5000.180<0.180µg/LBenzene
01/24/23 01:015.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
01/24/23 01:011.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
01/24/23 01:0110.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
01/24/23 01:010.5000.220<0.220µg/LToluene
01/24/23 01:014-Bromofluorobenzene (S)92.8 70-130
01/24/23 01:01Dibromofluoromethane (S)93.4 70-130
01/24/23 01:011,2-Dichloroethane - d4 (S)95.8 70-130
01/24/23 01:01Toluene-d8 (S)105 70-130
LCS-V29118 LCSD-V29118Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
32.9 82.283.733.540.0µg/LAcetone 40-160 1.8 20.0
18.3 91.510320.620.0µg/LBenzene 70-130 11.8 20.0
19.4 97.091.018.220.0µg/LMethyl Ethyl Ketone (MEK)60-140 6.3 20.0
17.6 88.093.018.620.0µg/LMethyl tert-butyl ether (MTBE)70-130 5.5 20.0
20.6 10310220.320.0µg/Ltert-Amyl Alcohol (TAA)40-140 1.4 20.0
18.2 91.096.519.320.0µg/LToluene 70-130 5.8 20.0
1051004-Bromofluorobenzene (S)70-130
92.496.2Dibromofluoromethane (S)70-130
92.299.21,2-Dichloroethane - d4 (S)70-130
100103Toluene-d8 (S)70-130
Page 7 of 8Date:01/24/2023 04:30 PM
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Quality Control Data
23-011-0103Report No:
Project Description:
Client ID:Geological Resources, Inc.
Reedy Creek Food Mart
QC Prep Batch Method:
Massachusetts VPH
MADEP-VPH
V28855QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAVPH (Prep)
QC Prep:V28854
Associated Lab Samples: 97297, 97298, 97299, 97300
LRB-V28854 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
01/12/23 11:2750.011.5<11.5µg/LAliphatic C5-C8
01/12/23 11:2750.025.8<25.8µg/LAliphatic C9-C12
01/12/23 11:2750.04.02<4.02µg/LAromatic C9-C10
01/12/23 11:272,5-Dibromotoluene (FID) (S)79.1 70-130
01/12/23 11:272,5-Dibromotoluene (PID) (S)77.3 70-130
LCS-V28854 LCSD-V28854Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
306 10297.3292300µg/LAliphatic C5-C8 70-130 4.6 50.0
371 124122367300µg/LAliphatic C9-C12 70-130 1.0 50.0
110 110107107100µg/LAromatic C9-C10 70-130 2.7 50.0
80.678.32,5-Dibromotoluene (FID) (S)70-130
77.575.92,5-Dibromotoluene (PID) (S)70-130
Page 8 of 8Date:01/24/2023 04:30 PM
Page 59 of 61
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-011-0103
Geological Resources, Inc.
00087
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 2.3C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angela D Overcash Date & Time:01/11/2023 16:27:29
Special precautions or instructions included?
Comments:
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