WS-5839_20966_CA_RMR_20170711

Excel Civil & Environmental Associates, PLLC
July 11, 2017
Ms. Linda Estkowski
625 Huntsman Court
Gasto ni a, N orth Carolina 28054
NC License No. P-0129
Telephone: [phone]
Facsimile: (704) 853 -3949
1 n t ern e t : www.excelengr.com
NCDEQ I DWM I UST Section
Winston-Salem Regional Office
450 West Hanes Mill Road, Suite 300
Winston-Salem, North Carolina 27105
Re: Monitoring Report -Revised
(Former) Servco No. 01711
850 North Liberty Street
Winston-Salem, North Carolina
Risk Classification: Intermediate
Land Use: INDUSTRIAL/COMMERCIAL
NCDEQ Incident No. 20966
EXCEL Project No. 24090
Dear Ms. Estkowski:
On behalf of Service Distributing Company, Incorporated (Servco), Excel Civil &
Environmental Associates, PLLC (Excel) is pleased to submit a copy of this Active
Remediation Monitoring Report for your approva l. To address your additional email
questions of June 22, 2017 follow:
1. Explain the free product measurement procedure that is being used and its
accuracy as compared to other methods. Free product measurements are made
with an electronic oil-water interface probe with an accuracy of 0.01 feet. This is
industry standard; other free product measurement methods, such as a paste,
offer similar accuracy.
2. Assure that all of the monitoring wells are in a state of good repair (caps present,
screws present and flush with the cap, locks, etc.). Excel will review the condition
of each monitor well during sampling events and make repairs as necessary.
3. Assure that locks are placed on all appropriate equ ipment (vaults, main power
shut off, well heads). Excel will review the condition of secured area during
EXCEL CIVil & ENVIRONMENTAL ASSOCIATES, PllC
www.excelengr.com
Monitoring Report
(Former) Servco No. 01711
Winston-Salem, North Carolin a
SECTION No.
TABLE OF CONTENTS
J Ul y 11 , 2017
Incident No. 20966
Excel No. 24090
PAGE No.
T ABLE OF CONTENTS ........................................ . . . . . . . -. . -. . . . . . . . . . . .. ........................ I
1.0 EXECUTIVE SUMMARy ..... ................................................................. ~ ..... 2
2.0 SITE HISTORY ........................................................................................................ 2
3.0 CURRENT ASSESSMENT INFORMATION ...................................................................... 3
4.0 FREE PRODUCT REMOVAL ....................................................................................... 4
5.0 CONCLUSIONS & R ECOMMENDATIONS ..................................................................... 5
6.0 SUMMARY OF FIELD ACTIVITIES ................................................................................ 8
LIST OF TABLES
TABLE 1 -MONITOR WELL CONSTRUCTION & LIQUID LEVEL DATA
TABLE 2 -SUMMARY OF CURRENT GROUNDWATER ANALYTICAL DATA
TABLE 3-SUMMARY OF HISTORICAL GROUNDWATER ANALYTICAL DATA
TABLE 4 -SUMMARY OF CURRENT SOIL ANALYTICAL DATA
TABLE 5 -GROUNDWATER MONITORING PLAN
LIST OF FIGURES
FIGURE 1 -SITE VICINITY MAP
FIGURE 2 -SITE PLAN
FIGURE 3 -GROUNDWATER CONTOUR MAP
FIGURE 4 -ApPROXIMATE LNAPL EXTENT MAP
FIGURE 5 -GROUNDWATER CONSTITUENTS MAP
FiGURE 6 -SOIL CONSTITUENTS MAP
ApPENDICES
ApPENDIX A -MANN-KENDALL GRAPHS
ApPENDIX B -LABORATORY REPORTS & CHAIN OF CUSTODY FORMS
ApPENDIX C -MAINTENANCE FORMS
APPENDIX 0 -PUBLIC NOTIFICATIONS
EXCEL CiVil & ENVIRONMENTAL ASSOCIATES, PLLC
www.excelengr.com
Monitoring Report
(Former) Servco No. 01711
Winston-Salem, North Carolina
SITE INFORMATION
PRIMARY CONSULTANT:
PROJECT MANAGER:
SITE CONTACT:
SITE HISTORY:
GENERAL GEOLOGY:
REGULATORY INTERACTION
AGENCY:
AGENCY CO NT ACT:
SITE ACTIVITIES:
RISK ASSESSMENT
SENSITIVE RECEPTORS:
CLOSEST POTABLE WELL:
MONITORING
JUly 11, 2017
Incident No. 20966
Excel No_ 24090
Excel Civil & Environmental Associates, PLLC
Mike Stanforth
Robert Gresham
In May 1999, seven steel regulated USTs were
removed from the site (Figure 1, Appendix A).
Samples collected during closure activities by
Wallace-Lee Consultants, llC (WLC) revealed
elevated levels of hydrocarbons. An lSA Report was
completed by WLC in April 2000 with an LSA
Addendum completed by WlC In December 2000,
which concluded that groundwater at the site
contained constituents levels exceeding both NCAC
2l standards and GCls. During LSA activities
conducted by WlC, free phase LNAPL was
discovered at the site in monitoring well MW-2. Free
product recovery efforts reportedly began in February
2000 by monthly site visits for liquid level gauging
and hand bailing.
To date, eight Aggressive Fluid Vapor Recovery
(AFVR) and two 100-hour Mobile Multi-Phase
Extraction (MMPE) events have previously been
conducted at the site by WLC. A vacuum enhanced
free product recovery system was installed
The subject site is located in the Milton Belts of the
Inner Piedmont Geologic Physiographic Province. The
1985 USGS Geologic Map of North Carolina Indicates
that rock in this area is commonly characterized by
inequigranular and megacrystic biotite gneiss and
schist.
NCOEQ, WSRO, DWM, UST Section
Linda Estkowski
Monthly O&M site visits, free product recovery checks
and semiannual groundwater sampling of select wells
Underground utilities on-site and within RfWs of North
Liberty Street and Chestnut Street; adjacent museum.
Water supply wells were not identified within 1,500
feet of the site.
LIQUID LEVEL GAUGING FREQUENCY: As requested
As requested GROUNDWATER SAMPLING METHOD:
EXCEL CIVIL & ENVIRONMENTAL AsSOCIATES, PlLC
www.eKcelengr.com
Monitoring Report
(Former) $ervco No. 01711
Wlnston·Salem, North Ca rolina
EXECUTIVE SUMMARY
July 11 , 2017
Incident No. 20966
Excel No. 24090
The (Former) Servco No . 01711 facility is located at 850 North Liberty Street in Winston-Salem,
Forsyth Counly, North Carolina. As proposed in the revised Corrective Action Plan completed
by Excel dated March 23, 2013, the onsite remediation system was placed into operation in
January of 2015 . The vacuum enhanced free product recovery system is comprised of two
vapor extraction wells and two free product skimmer pumps. A summary of the field activities
associated with the monthly operation and maintenance is given in subsequent sections of this
report.
Operation of the remediation system has resulted in a reduction of lNAPL in MW-2 from a
maximum thickness of 0.44 feet measured in April of 2015 to a current thickness of 0.17 feel
during Ihe reporting period. LNAPL in MW-4 is observed to have remained at a thickness of
0.02 feet (refer to Table 1 and Figure 4). The goal of the remediation system is to eliminate
free product utilizing vacuum enhanced pneumatic skimmers within the source area. The stated
milestone of removing free product has not yet been completed and has been delayed due to
property accessibility issues caused by the current property owner.
Based upon a review of the current analytical data from March 2017, the estimated size of the
area of elevated benzene and MTBE exceeding GCl Standards is approximately 3,900 and
7,500 square feet (MTBE plume), primarily located on the subject property and spanning
beneath the former crown building south to the former UST tank pit.
Results of past receptor surveys completed by Excel during assessment activities indicate that
supply wells were not identified within 1,500 feet of the property. Additionally, according to the
USGS Topographical Map no surface water bodies are located within 1,500 feet of the source
area.
SITE HISTORY
The (former) Servco No. 0171 1 facility is located at 850 North Liberty Street within the city of
Winston-Salem, Forsyth County, North Carolina (refer to Figure 1). A site map of the facility
detailing former structures and monitoring well locations is provided as Figure 2. Various
assessment activities have been conducted at the (former) Servco No. 0171 1 facility following
UST Closure Assessment activities conducted by Service Distributing Company, Incorporated
(Servco) in August 1999 completed by Wallace-Lee Consultants, LLC (WLC) of Wilmington,
North Carolina. During the assessment activities, seven regulated UST's were removed as part
of one excavation during the closure activities. Following removal of the USTs, reportedly no
additional soils were excavated with excavated soils returned to the UST basin. A total of 32 soil
samples were collected from the UST basins, beneath the product lines and dispenser islands
and analyzed for Total Petroleum Hydrocarbons (TPH) by EPA Methods 5030 and 3550
(Gasoline and Diesel Range OrganiCS, respectively). Based on review of the report submitted to
the NCDEQ on August 17. 1999, analytical results revealed elevated levels of petroleum
hydrocarbons in multiple soil samples collected from beneath the UST system.
At the request of the North Carolina Department of Environmental Quality (NCDEQ). Winston-
Salem Regional Office (WsRO), Division of Waste Management, UST Section, a LSA was
EXCEL CtVIL & ENVIRONMENTAL AsSOCIATES, PLlC
www.excelengr.com
Monitoring Report
(Former) Servco No. 01711
Winston-Salem, North Carolina
July 11, 2017
Incident No. 20966
Excel No. 24090
completed for the subject property. Servco contracted Wl C to complete the LSA, which
included the installation of five Type II monitoring wells, a potable well survey, soil and
groundwater sampling with associated laboratory analysis and the completion of the LSA report.
The soil samples collected at the location of MW-1 were found to be above the Soil-Io-Water
Maximum Soil Contaminant Concentrations (MSCC) for various constituents as detailed in the
January 2, 1998 Groundwater Section Guidelines as amended. None of the samples collected
revealed hydrocarbon levels above applicable Industrial/Commercial MSCCs. The laboratory
results of the groundwater samples collected from MW-1, MW-3 and MW-4 were found to
exceed Gross Contam ination levels (GCLs) for benzene as detailed in the January 2, 1998
Groundwater Section Guidelines as amended. During the LSA activities, free product was
encountered in monitoring well MW-2 with a measured thickness of approximately 2.64-feel.
To date, Excel and others have conducted multiple free product recovery events incorporating
both aggressive and passive techniques since February 2000. Eight Aggressive Fluid-Vapor
Recovery (AFVR) events were conducted by WLC reportedly yielding a collective approximate
315-gallons of product. In addition, WLC conducted two 100-hour Mobile Multi-Phase Extraction
(MMPE) events and Excel completed one 100-hour MMPE event recovering a total of 830-
gallons of producUwater mixture from the location of MW-2. At the request of the NCDEQ, a
Free Product Recovery Specification Report was completed by Excel on April 15, 2010.
Activities included the installation of two additional monitoring wells MW-6 and MW-7 and the
completion of a free product evaluation at the location of MW-2. Results of the field evaluation
revealed no free product in the newly installed monitoring wells and that the true free product
thickness at MW-2 was measured at 0.04-feet with an expected recovery rate of O.4-gallons per
hour, Excel recommended the implementation of a free product recovery system at the site.
As directed by the NCDEQ, one additional downgradient monitoring well (MW-13) and two
vapor extraction wells (SVE-1 and SVE-2) were installed on November 24,2014. Replacement
monitoring well MW-2R was installed January 15, 20 15.
The onsite remediation system, utilizing vacuum enhanced free product recovery was placed
into operation in Ja nuary of 2015. The soil vapor extraction system is comprised of two vapor
extraction wells. A summary of the field activities associated wi th the monthly operation and
maintenance is given in subsequent sections of this report.
Site access was denied to ECEA by the property owner in June of 2016 and ECEA was not
granted access to return to the property until March of 2017. During the interim, the free
product recovery system maintenance could not be completed. The lack of site access has
delayed site cleanup activities by the responsible party.
Cleanup levels (soil) for the site would be the lesser of the Industrial/Commercial Maximum Soil
Contaminant Concentrations (MSCCs) or the Soil-la-Water Maximum Soil Contaminant
Concentrations (MSCCs). This CAP proposed the res tora tion of groundwater quality to a site-
specific aclion levels approximating Gross Contamination Levels (GCls) for the applicable
standards developed for this site. Following achievement of the site-specific action level, the site
risk classification can be reduced to "Low" and active grou ndwater remediation can be
EXCEl CIVil & ENVIRONMENTAL ASSOCIATES, PllC
www.excelengr.com
Monitoring Report July 11 , 2017
Incident No. 20966
Excel No. 24090
(Former) Servco No. 01711
Win ston-Salem, North Carolina
suspended. Once risk reduction has occurred, the applicable soil cleanup levels for the site
wou ld be Industrial/Commercial.
CURRENT ASSESSMENT INFORMATION
•
•
•
•
•
•
Groundwater quality samples were collected from eight monitor wells on March 24, 2017
and laboratory analyzed for full range volatile organic compounds (VOCs) by EPA Method
6200B. It is Excel's standard operating procedure not to gauge monitoring wells with an oil·
water interface probe prior to sampling if said well has not historically shown free product.
Static water levels were collected with a decontaminated water level indicator at locations
where free product has not previously been encountered.
Groundwater quality samples were collected from monitoring wells MW-1, MW-6, MW-7,
MW-8, MW-9, MW-10, MW-11, and MW-13 on March 24, 2017. Monitoring wells MW-2R
and MW-4 were not sampled due to the presence of free product: monitoring wells MW-3,
MW-5 and MW-12 could not be located. A map depicting the estimated extent of free
product is provided as Figure 4.
The results of the laboratory data for the groundwater samples collected were compared
against the Gross Contamination levels (GCls). The analytical data presented for the
constituents detected was determined based on the highest result from the various EPA
Methods described above. A review of the laboratory analytical results indicated the
following constituents were above applicable regulatory standards:
> Benzene
• GCl: MW-1 and MW-7
~ Methyl-tert-butyl-ether (MTBE)
• GCl: MW-1, MW-6 and MW-7
Based upon a review of the current analytical data, the estimated size of the area of
elevated benzene and MTBE exceeding GCl Standards is approximately 3,900 and 7,500
square feet (MTBE plume), primarily located on the subject property and spanning beneath
the former crown building south to th e former UST tank pit. The elevated benzene and
MTBE levels exceeding NCAC 2l levels were observed to be spanning offsite onto the
adjacent properties to the south and east. The remaining constituents are a minor portion of
the benzene and MTBE plumes. Some seasonal fluctuations were observed in the
groundwater quality data from select wells.
The onsite remediation system was placed into operation in January of 2015. The soil vapor
extraction system is comprised of two vapor extraction wells. A summary of the field
activities associated with the monthly operation and maintenance is given in subsequent
sections of this report. A copy of the system maintenance form is included in Appendix D.
Soil samples were collected at the site from four soil boring locations, in accordance with an
agreement with the property owner. Soil samples were collected at depths ranging from 3-
fbgl to B-fbgl on March 24, 2017. Table 4 summarizes the soil results from the onsite
samples collected during the current assessment activities conducted by Excel. Soil
EXCEL CIVIL & ENVIRONMENTAL ASSOCIATES, Pll C
www.excetengr.com
Monitoring Report
(Former) Servco No. 01711
Winston-Salem, North Carolina
July 11, 2017
Incident No. 20966
Excel No. 24090
samples were collected in laboratory provided containers and analyzed by Environmental
Science Corporation of Mt. Juliet, Tennessee for the following parameters: Volatile Organics
by EPA Method 8260; Semivolatile Organics by EPA Method 8270; Total Petroleum
Hydrocarbons, Diesel Range Organics by EPA Method 5030; and MADEP Volatile
Petroleum Hydrocarbons (VPH). A review of soils data collected by Excel during the March
2017 sampling event does not indicate impacted soil levels which exceed
Industrial/Commercial MSCCs. Figure 6 in Appendix B depicts select groundwater
constituents. A complete copy of the laboratory analytical data is located in Appendix B.
• Based on the liquid level data collected, groundwater flow is estimated to be to the south. A
groundwater contour map is included in Appendix B, Figure 3.
• Results of past receptor surveys completed by Excel during assessment activities indicate
that supply wells were not identified within 1,500 feet of the property. Additionally, according
to the USGS Topographical Map no surface water bodies are located within 1,500 feet of
the source area.
FREE PRODUCT REMOVAL
• Based upon a review of the current analytical data, the estimated size of the LNAPL is
approximately 500 square feet, primarily located to the south of the former Crown building.
• Operation of the remediation system has resulted in a reduction of LNAPL in MW-2 from a
maximum thickness of 0.44 feet measured in April of 2015 to a current thickness of 0.17 feet
during the report ing period. LNAPL in MW-4 is observed to have remained at a thickness of
0.02 feet (refer to Table 1 and Figure 4). The free product collection tank was recorded to
contain approximately 12.53 gallons of producUwater mix on May 30, 2017.
CONCLUSIONS & RECOMMENDATIONS
• In summary, current laboratory analytical data indicates that overall dissolved phase
hydrocarbon constituents (primarily BTEX and MTBE) continues to occur at the site and are
decreasing with some seasonal fluctuations. Remaining cons tituent levels exceed the GCL
and NCAC 2L Standards at multiple locations for various constituents.
• Mann-Kendall graphs are provided in Appendix A. The graphs showing concentration
trends for Monitoring Wells MW-1, MW-3, MW-6, MW-7 and MW-8. The concentration
trends for benzene and MTBE show decreasing or no trend for all wells with the exception of
MW-7. MW-7 is located adjacent to the LNAPL and should begin to decrease once the free
product has been removed from that area.
• At this time and based on the information in this report, we recommend continued operation
of the vacuum enhanced free product recovery, free product recovery efforts at monitoring
wells MW-2R and MW-4, and continuing semiannu al groundwater sampling of select wells.
EXCEL CIVIL & ENVIRONMENTAL ASSOCIATES, PllC
www.excelengr.com
Moniloring Report July 11 , 2017
Incident No. 20966
Excel No. 24090
(Former) Servco No. 01711
Winston-Salem, North Carolina
1 Enter t he date the monitoring report \\'lIS due. 7/1512017 W ill this report be submitted YES
after the established due date?
2 Was lilly required information from th e above template mi ss ing f,'om this report? YES
IF the answer to question II I or# 2 is "YES", please provide additional information in this cell to explain
what was missing and why.
3 If applicable, will any of the pmposed attenuation milestones under the schedule YES
approved in the Corrective Action I'lan not be met? (within a re(lsonable IIImgill of errOl)
IF the answer to question #3 is "NO", skip to the certification under #8 below.
IF the ;mswer 10 question #3 is "YES", please generally describe in this ceilihe possible reason(s) and
outline proposed remedies. (This sho uld be described in more detail in the re port text above.)
4 Docs an}' known or suspected source zone soil contamination or free product remain YES
o."tsid e of tile assessed area that could be inhibiting natural attenuation?
5 Has there been an un expected increase in co ntaminant mass sufficient to suggest a YES
potential new release from a separate onsite or offsite source?
IF the answer to either question #4 or #5 is "YES", genemlly describe in this cell any actions
recommended to further assess or clean up this known or suspected source. (This should be described in
more detail in the report text above.)
6 CCI·tifieation:
NO
NO
NO
NO
NO
I, Michael Stanforth, a Professional Engineer for Excel Civil & Environmental Associates, PLLC, do certify
that the information contained in this report is correct and accurate to the best of my knowlcdge.
\\\\\11111/11/
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'//t 1 ::;<:," ~-.: ,~"", . ;.' : l' ., . •
Excel Civil & Environmental Associates, PLLC is licensed to practice engineering in North Carolina.
certification number of the company or corporation is P-O 129.
EKen Cl VtL & ENVIRQNMENTALAsSQCIATES, PLlC
www.excelengr.com
The
Active Remediation Monitoring Report
(Former) Servco No. 01711
Winston-Salem. North Carolina
July 11, 2017
Incident No. 20966
Excel No. 24090
SUMMARY OF FIELD ACTIVI TIES
3/24/17: Excel conducted a regularly scheduled monitoring and maintenance site visit to
perform routine 0 & M. Upon arriva l, the system was down. A new timer relay and
air compressor was installed and the system restarted . Free product recovery
skimmers and associated thicknesses were adjusted in MW-2 and MW-4. The
system was operational at departure.
EXCEL CiVIL & ENVIRONMENTAL ASSOCIATES, PlLC
www.excelengr.com
Monitoring Report
(Former) Servco No. 01711
Winston-Salem, North Carolina
July 11, 2017
Incident No. 20966
Excel No. 24090
Site History UST/AST System and Other Release Information
Description
Tank of Date USTID Current/last Previous Capacity Construction Dimensions associated tank Number Contents Contents (galions) Details
1 Kerosene
2 Diesel
3 Gasoline
4 Gasoline
5 Gasoline
6 Gasoline
7 Gasoline
USTID Current/last
Number Contents
1 Kerosene
2 Diesel
3 Gasoline
4 Gasoline
5 Gasoline
6 Gasoline
7 Gasoline
(Approx)
None 10,000 Steel 18' x 10'
None 10,000 Steel 1S' x 10'
None 4,000 Steel 24' x 64"
None 2,000 Steel S'3"x 12'
None 5,000 Steel 13'6"x8'
None 20,000 Steel 30' x 10' 6"
None 20,000 Steel 30' x 10' 6"
Was
Capacity Status of release Incident associated (gallons) UST with UST Number
system
10,000 Removed Yes 513199
10,000 Removed Ye, 513199
4,000 Removed Ye, 513199
Removed 20966 2,000 513199 Ye,
5,000 Removed Ye, 513199
20,000 Removed Ye, 514199
20,000 Removed Ye, 514199
EXCEL CiVil & ENVIRONMENTAL ASSOCIATES, PLl C
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pipings installed
and pumps
Unknown 05115/49
Unknown 05114154
Unknown 05108177
Unknown 05109174
Unknown 05114154
Unknown 05115149
Unknown 05/15/49
Material Description
Released of Release
Former UST
Gasoline system -
discovered
5199
Monitoring Report
(Former) Servco No. 0171 1
Winston-Salem. North Ca rolina
July 11, 2017
Incident No. 20966
Excel No. 24090
Site History -UST Owner/Operator and Other Responsible Party Inform ation
UST 10 Number Facility 10 Incident # 20966 Number
Name of Owner Dates of Operation (mmldd/yy to
mm/dd/yy)
Service
Distributing 5115149 to 5/3199
Company
Street Address
P.O. Box 310
City Slate Zip Telephone Number
Albemarle North 28001 [phone] Carolina
Name of Operator Dates of Operation
Service Distributing Company 5/15/49 to 5/3199
Street Address
Street Address
110 North Second Street
City State Zip Telephone Number
North Albemarle Carolina 28001 [phone]
Incident Number 20966
Name of other Responsible Date of Release {mm/dd/yy to
Party
Same as owner
City
mm/dd/yy
513/99
Street Address
State Zip Telephone Number
EXCEL CIVIL & ENVIRONMENTAL ASSOCIATES, PLLC
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TABLES
Table 1 -Monitoring Well Construction and Liquid Level Data
Table 2 -Summary of Current Groundwater Analytical Data
Table 3 -Summary of Historical Groundwater Analytical Data
Table 4 -Summary of Current Soil Analytical Data
Table 5 -Groundwater Monitoring Plan
EXCELClVlt& ENVIRONMENTAL ASSOCIATES, PLlC
www.excelengr.com
~~:; -~ .. ,-.
1!iII'ii;, ~"",",. ___
MW1 -02/01/00
MW-2 02/02/00
MW-3 02/02/00
MW-4 02/01/00
MW-5 02/01/00
MW-6 02/24/10
MW-7 02/24/10
MW-8 05/11/11
MW-9 05/11/11
MW-l0 05/11/11
MW-11 05/11/11
MW-12 05/11/11
MW-13 11/24/14
NOTES:
All data presented in feet
---
Table 1
Monitoring Well Construction and liquid Level Data
(Former) SERVCO No. 01711
----,
850 North Liberty Street
Winston-Salem, North Carolina
NCDENR Incident No. 20966
Excel Project No. 24090
---". ---~ --_. .-. --, -. , -~ ~-...,,--.. -,. ---> --'l . _ ~. -, '. 'j . --. . .
~'_~~Jj:.---, . " "_ " \ ..... _ ' h~ __ ,_""...,. .v.;", ",':( ... .,,' __ ~~:'1 _ ~.:!.. ____ --, .... ~ •. ~ ... ".:t.~ ... .: ~~ -'--~~
47 37 47 -9944 --3731 --L 6213
47 37 -47 98.65 3603 36.20 I 0.17 I 62.58
47 37 -47 9856 NOT LOCATED
48 38 -48 98.44 37.70 I 37.72 I 0.02 I 60.74
49 39 -49 100.00 NOT LOCATED -ASSUMED DESTROYED
45 25 -45 98.20 --36.38 --61 .82
45 25 -45 99.27 --37.49 --61.78
45 25 -45 100.15 --38.03 --62.12
45 25 -45 96.92 --3602 --60.90
45 25 -45 98.28 --38.09 --60.19
45 25 -45 97.19 --37.22 --59.97
45 25 -45 99.38 NOT LOCATED
45 25 -45 97.56 --36.46 I --I 61.10
Water level data collected on March 24. 2017
FIGURES
Figure 1 -Site Vicinity
Figure 2 -Site Plan
Figure 3 -Groundwater Contour Map
Figure 4 -Approximate LNAPL Extent Map
Figure 5 -Groundwater Constituents Map
Figure 6 -Soils Constituents Map
EXCEl CIVIL & ENVIRONMENTAL ASSOCIATES, Pl lC
www.excelengr.com
APPENDIX A -MANN·KENDALL GRAPHS
EXCEl CiVil & ENVIRONMENTAL ASSOCIATES, PLLC
www.excelengr.com
APPENDIX B -LABORATORY ANALYSES & CHAIN OF CUSTODY FORM
EXCEL CIVIL & ENVIRONMENTAL ASSOCIATES, PllC
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ANALYTICAL REPORT
April 07, 2017
Excel Civil & Environmental Associates
Sample Delivery Group:L898293
Samples Received:03/25/2017
Project Number:24090
Description:Servco 01711 - Winston-Salem # 1
Site:WINSTON-SALEM, NC
Report To:Mr. Mike Stanforth
PO Box 6172
Gastonia, NC 28056-6000
Entire Report Reviewed By:
April 07, 2017
[Preliminary Report]
Jimmy Hunt
Technical Service Representative
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by ESC is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304.
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.esclabsciences.com
April 07, 2017
Jimmy Hunt
Technical Service Representative
ONE LAB. NATIONWIDE.TABLE OF CONTENTS
¹Cp: Cover Page 1
²Tc: Table of Contents 2
³Ss: Sample Summary 3
⁴Cn: Case Narrative 5
⁵Sr: Sample Results 6
MW-1 L898293-01 6
MW-6 L898293-02 8
MW-7 L898293-03 10
MW-8 L898293-04 12
MW-9 L898293-05 14
MW-10 L898293-06 16
MW-11 L898293-07 18
MW-13 L898293-08 20
TRIPBLANK L898293-09 22
B-1 L898293-10 24
B-2 L898293-11 27
B-3 L898293-12 30
B-4 L898293-13 33
⁶Qc: Quality Control Summary 37
Total Solids by Method 2540 G-2011 37
Volatile Petroleum Hydrocarbons by Method MADEPV 39
Volatile Organic Compounds (GC/MS) by Method 6200B-1997 40
Volatile Organic Compounds (GC/MS) by Method 8260B 49
Semi Volatile Organic Compounds (GC/MS) by Method 8270D 53
⁷Gl: Glossary of Terms 59
⁸Al: Accreditations & Locations 60
⁹Sc: Chain of Custody 61
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-1 L898293-01 GW C DeVane 03/24/17 09:35 03/25/17 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-1997 WG964562 20000 04/04/17 07:57 04/04/17 07:57 ACG
Volatile Organic Compounds (GC/MS) by Method 6200B-1997 WG964562 500 04/01/17 19:01 04/01/17 19:01 DWR
Collected by Collected date/time Received date/time
MW-6 L898293-02 GW C DeVane 03/24/17 09:48 03/25/17 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-1997 WG964562 100 04/01/17 19:24 04/01/17 19:24 DWR
Volatile Organic Compounds (GC/MS) by Method 6200B-1997 WG964562 1000 04/04/17 07:44 04/04/17 07:44 ACG
Collected by Collected date/time Received date/time
MW-7 L898293-03 GW C DeVane 03/24/17 10:00 03/25/17 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-1997 WG964562 100 04/01/17 19:47 04/01/17 19:47 DWR
Volatile Organic Compounds (GC/MS) by Method 6200B-1997 WG964562 1000 04/04/17 07:30 04/04/17 07:30 ACG
Collected by Collected date/time Received date/time
MW-8 L898293-04 GW C DeVane 03/24/17 09:20 03/25/17 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-1997 WG964562 5 04/01/17 20:10 04/01/17 20:10 DWR
Volatile Organic Compounds (GC/MS) by Method 6200B-1997 WG964562 500 04/04/17 07:17 04/04/17 07:17 ACG
Collected by Collected date/time Received date/time
MW-9 L898293-05 GW C DeVane 03/24/17 10:15 03/25/17 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-1997 WG964562 50 04/01/17 20:33 04/01/17 20:33 DWR
Volatile Organic Compounds (GC/MS) by Method 6200B-1997 WG964562 50 04/04/17 07:03 04/04/17 07:03 ACG
Collected by Collected date/time Received date/time
MW-10 L898293-06 GW C DeVane 03/24/17 10:27 03/25/17 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-1997 WG964562 1 04/01/17 17:06 04/01/17 17:06 DWR
Collected by Collected date/time Received date/time
MW-11 L898293-07 GW C DeVane 03/24/17 10:54 03/25/17 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-1997 WG964562 1 04/01/17 17:29 04/01/17 17:29 DWR
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-13 L898293-08 GW C DeVane 03/24/17 10:41 03/25/17 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-1997 WG964562 1 04/01/17 17:52 04/01/17 17:52 DWR
Collected by Collected date/time Received date/time
TRIPBLANK L898293-09 GW C DeVane 03/24/17 00:00 03/25/17 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-1997 WG964562 1 04/01/17 18:15 04/01/17 18:15 DWR
Collected by Collected date/time Received date/time
B-1 L898293-10 Solid C DeVane 03/24/17 11:15 03/25/17 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Total Solids by Method 2540 G-2011 WG965406 1 03/30/17 10:42 03/30/17 10:49 KDW
Volatile Petroleum Hydrocarbons by Method MADEPV WG965869 55.5 03/31/17 01:38 03/31/17 01:38 JAH
Volatile Organic Compounds (GC/MS) by Method 8260B WG965859 1 03/24/17 11:15 03/31/17 11:56 JHH
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG965361 1 03/30/17 08:56 03/30/17 15:09 KMP
Collected by Collected date/time Received date/time
B-2 L898293-11 Solid C DeVane 03/24/17 12:18 03/25/17 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Total Solids by Method 2540 G-2011 WG965706 1 03/30/17 14:55 03/30/17 15:02 KDW
Volatile Petroleum Hydrocarbons by Method MADEPV WG965869 56.5 03/31/17 02:10 03/31/17 02:10 JAH
Volatile Organic Compounds (GC/MS) by Method 8260B WG965859 1 03/24/17 12:18 03/31/17 12:16 JHH
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG965361 1 03/30/17 08:56 03/30/17 18:03 KMP
Collected by Collected date/time Received date/time
B-3 L898293-12 Solid C DeVane 03/24/17 11:48 03/25/17 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Total Solids by Method 2540 G-2011 WG965706 1 03/30/17 14:55 03/30/17 15:02 KDW
Volatile Petroleum Hydrocarbons by Method MADEPV WG965869 50 03/31/17 02:43 03/31/17 02:43 JAH
Volatile Organic Compounds (GC/MS) by Method 8260B WG965859 1 03/24/17 11:48 03/31/17 12:39 JHH
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG965361 1 03/30/17 08:56 03/30/17 18:28 KMP
Collected by Collected date/time Received date/time
B-4 L898293-13 Solid C DeVane 03/24/17 11:35 03/25/17 09:00
Method Batch Dilution Preparation Analysis Analyst
date/time date/time
Total Solids by Method 2540 G-2011 WG965706 1 03/30/17 14:55 03/30/17 15:02 KDW
Volatile Petroleum Hydrocarbons by Method MADEPV WG965869 1100 04/06/17 14:15 04/06/17 14:15 LRL
Volatile Petroleum Hydrocarbons by Method MADEPV WG965869 550 04/04/17 22:08 04/04/17 22:08 LRL
Volatile Organic Compounds (GC/MS) by Method 8260B WG965859 1.03 03/24/17 11:35 03/31/17 13:00 JHH
Volatile Organic Compounds (GC/MS) by Method 8260B WG965859 275 03/24/17 11:35 04/04/17 13:23 JHH
Volatile Organic Compounds (GC/MS) by Method 8260B WG965859 2750 03/24/17 11:35 04/04/17 17:00 LRL
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG965361 1 03/30/17 08:56 03/30/17 16:49 KMP
Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG965361 20 03/30/17 08:56 03/31/17 18:57 KMP
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times. All MDL (LOD) and RDL (LOQ)
values reported for environmental samples have been corrected for the dilution factor used in the
analysis. All Method and Batch Quality Control are within established criteria except where addressed
in this case narrative, a non-conformance form or properly qualified within the sample results. By my
digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the
laboratory as having the potential to affect the quality of the data have been identified by the
laboratory, and no information or data have been knowingly withheld that would affect the quality of the
data.
[Preliminary Report]
Jimmy Hunt
Technical Service Representative
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Jimmy Hunt
Technical Service Representative
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L898293
MW-1
Collected date/time: 03/24/17 09:35
Volatile Organic Compounds (GC/MS) by Method 6200B-1997
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acetone U 5000 25000 500 04/01/2017 19:01 WG964562
Acrolein U J4 4440 25000 500 04/01/2017 19:01 WG964562
Acrylonitrile U 935 5000 500 04/01/2017 19:01 WG964562
Benzene 18200 166 500 500 04/01/2017 19:01 WG964562
Bromobenzene U 176 500 500 04/01/2017 19:01 WG964562
Bromodichloromethane U 190 500 500 04/01/2017 19:01 WG964562
Bromoform U 234 500 500 04/01/2017 19:01 WG964562
Bromomethane U J3 433 2500 500 04/01/2017 19:01 WG964562
n-Butylbenzene U 180 500 500 04/01/2017 19:01 WG964562
sec-Butylbenzene U 182 500 500 04/01/2017 19:01 WG964562
tert-Butylbenzene U 200 500 500 04/01/2017 19:01 WG964562
Carbon tetrachloride U 190 500 500 04/01/2017 19:01 WG964562
Chlorobenzene U 174 500 500 04/01/2017 19:01 WG964562
Chlorodibromomethane U 164 500 500 04/01/2017 19:01 WG964562
Chloroethane U 226 2500 500 04/01/2017 19:01 WG964562
Chloroform U 162 2500 500 04/01/2017 19:01 WG964562
Chloromethane U 138 1250 500 04/01/2017 19:01 WG964562
2-Chlorotoluene U 188 500 500 04/01/2017 19:01 WG964562
4-Chlorotoluene U 176 500 500 04/01/2017 19:01 WG964562
1,2-Dibromo-3-Chloropropane U 665 2500 500 04/01/2017 19:01 WG964562
1,2-Dibromoethane U 190 500 500 04/01/2017 19:01 WG964562
Dibromomethane U 173 500 500 04/01/2017 19:01 WG964562
1,2-Dichlorobenzene U 174 500 500 04/01/2017 19:01 WG964562
1,3-Dichlorobenzene U 110 500 500 04/01/2017 19:01 WG964562
1,4-Dichlorobenzene U 137 500 500 04/01/2017 19:01 WG964562
Dichlorodifluoromethane U 276 2500 500 04/01/2017 19:01 WG964562
1,1-Dichloroethane U 130 500 500 04/01/2017 19:01 WG964562
1,2-Dichloroethane U 180 500 500 04/01/2017 19:01 WG964562
1,1-Dichloroethene U 199 500 500 04/01/2017 19:01 WG964562
cis-1,2-Dichloroethene U 130 500 500 04/01/2017 19:01 WG964562
trans-1,2-Dichloroethene U 198 500 500 04/01/2017 19:01 WG964562
1,2-Dichloropropane U 153 500 500 04/01/2017 19:01 WG964562
1,1-Dichloropropene U 176 500 500 04/01/2017 19:01 WG964562
1,3-Dichloropropane U 183 500 500 04/01/2017 19:01 WG964562
2,2-Dichloropropane U 160 500 500 04/01/2017 19:01 WG964562
Di-isopropyl ether 977 160 500 500 04/01/2017 19:01 WG964562
Ethylbenzene 3620 192 500 500 04/01/2017 19:01 WG964562
Hexachloro-1,3-butadiene U 128 500 500 04/01/2017 19:01 WG964562
Isopropylbenzene U 163 500 500 04/01/2017 19:01 WG964562
p-Isopropyltoluene U 175 500 500 04/01/2017 19:01 WG964562
2-Butanone (MEK)U 1960 5000 500 04/01/2017 19:01 WG964562
Methylene Chloride U 500 2500 500 04/01/2017 19:01 WG964562
4-Methyl-2-pentanone (MIBK)U 1070 5000 500 04/01/2017 19:01 WG964562
Methyl tert-butyl ether 633000 7340 20000 20000 04/04/2017 07:57 WG964562
Naphthalene U 500 2500 500 04/01/2017 19:01 WG964562
n-Propylbenzene 351 J 174 500 500 04/01/2017 19:01 WG964562
Styrene U 154 500 500 04/01/2017 19:01 WG964562
1,1,1,2-Tetrachloroethane U 192 500 500 04/01/2017 19:01 WG964562
1,1,2,2-Tetrachloroethane U 65.0 500 500 04/01/2017 19:01 WG964562
Tetrachloroethene U 186 500 500 04/01/2017 19:01 WG964562
Toluene 52300 206 500 500 04/01/2017 19:01 WG964562
1,2,3-Trichlorobenzene U 115 500 500 04/01/2017 19:01 WG964562
1,2,4-Trichlorobenzene U 178 500 500 04/01/2017 19:01 WG964562
1,1,1-Trichloroethane U 160 500 500 04/01/2017 19:01 WG964562
1,1,2-Trichloroethane U 192 500 500 04/01/2017 19:01 WG964562
Trichloroethene U 199 500 500 04/01/2017 19:01 WG964562
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L898293
MW-1
Collected date/time: 03/24/17 09:35
Volatile Organic Compounds (GC/MS) by Method 6200B-1997
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Trichlorofluoromethane U 600 2500 500 04/01/2017 19:01 WG964562
1,2,3-Trichloropropane U 404 1250 500 04/01/2017 19:01 WG964562
1,2,4-Trimethylbenzene 2870 186 500 500 04/01/2017 19:01 WG964562
1,3,5-Trimethylbenzene 992 194 500 500 04/01/2017 19:01 WG964562
Vinyl chloride U J3 130 500 500 04/01/2017 19:01 WG964562
o-Xylene 7560 170 500 500 04/01/2017 19:01 WG964562
m&p-Xylenes 14600 360 1000 500 04/01/2017 19:01 WG964562
(S) Toluene-d8 98.9 80.0-120 04/04/2017 07:57 WG964562
(S) Toluene-d8 103 80.0-120 04/01/2017 19:01 WG964562
(S) Dibromofluoromethane 96.9 76.0-123 04/04/2017 07:57 WG964562
(S) Dibromofluoromethane 108 76.0-123 04/01/2017 19:01 WG964562
(S) a,a,a-Trifluorotoluene 92.7 80.0-120 04/04/2017 07:57 WG964562
(S) a,a,a-Trifluorotoluene 101 80.0-120 04/01/2017 19:01 WG964562
(S) 4-Bromofluorobenzene 88.0 80.0-120 04/04/2017 07:57 WG964562
(S) 4-Bromofluorobenzene 101 80.0-120 04/01/2017 19:01 WG964562
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L898293
MW-6
Collected date/time: 03/24/17 09:48
Volatile Organic Compounds (GC/MS) by Method 6200B-1997
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acetone U 1000 5000 100 04/01/2017 19:24 WG964562
Acrolein U J4 887 5000 100 04/01/2017 19:24 WG964562
Acrylonitrile U 187 1000 100 04/01/2017 19:24 WG964562
Benzene 3530 33.1 100 100 04/01/2017 19:24 WG964562
Bromobenzene U 35.2 100 100 04/01/2017 19:24 WG964562
Bromodichloromethane U 38.0 100 100 04/01/2017 19:24 WG964562
Bromoform U 46.9 100 100 04/01/2017 19:24 WG964562
Bromomethane U J3 86.6 500 100 04/01/2017 19:24 WG964562
n-Butylbenzene U 36.1 100 100 04/01/2017 19:24 WG964562
sec-Butylbenzene U 36.5 100 100 04/01/2017 19:24 WG964562
tert-Butylbenzene U 39.9 100 100 04/01/2017 19:24 WG964562
Carbon tetrachloride U 37.9 100 100 04/01/2017 19:24 WG964562
Chlorobenzene U 34.8 100 100 04/01/2017 19:24 WG964562
Chlorodibromomethane U 32.7 100 100 04/01/2017 19:24 WG964562
Chloroethane U 45.3 500 100 04/01/2017 19:24 WG964562
Chloroform U 32.4 500 100 04/01/2017 19:24 WG964562
Chloromethane U 27.6 250 100 04/01/2017 19:24 WG964562
2-Chlorotoluene U 37.5 100 100 04/01/2017 19:24 WG964562
4-Chlorotoluene U 35.1 100 100 04/01/2017 19:24 WG964562
1,2-Dibromo-3-Chloropropane U 133 500 100 04/01/2017 19:24 WG964562
1,2-Dibromoethane 290 38.1 100 100 04/01/2017 19:24 WG964562
Dibromomethane U 34.6 100 100 04/01/2017 19:24 WG964562
1,2-Dichlorobenzene U 34.9 100 100 04/01/2017 19:24 WG964562
1,3-Dichlorobenzene U 22.0 100 100 04/01/2017 19:24 WG964562
1,4-Dichlorobenzene U 27.4 100 100 04/01/2017 19:24 WG964562
Dichlorodifluoromethane U 55.1 500 100 04/01/2017 19:24 WG964562
1,1-Dichloroethane U 25.9 100 100 04/01/2017 19:24 WG964562
1,2-Dichloroethane 165 36.1 100 100 04/01/2017 19:24 WG964562
1,1-Dichloroethene U 39.8 100 100 04/01/2017 19:24 WG964562
cis-1,2-Dichloroethene U 26.0 100 100 04/01/2017 19:24 WG964562
trans-1,2-Dichloroethene U 39.6 100 100 04/01/2017 19:24 WG964562
1,2-Dichloropropane U 30.6 100 100 04/01/2017 19:24 WG964562
1,1-Dichloropropene U 35.2 100 100 04/01/2017 19:24 WG964562
1,3-Dichloropropane U 36.6 100 100 04/01/2017 19:24 WG964562
2,2-Dichloropropane U 32.1 100 100 04/01/2017 19:24 WG964562
Di-isopropyl ether 216 32.0 100 100 04/01/2017 19:24 WG964562
Ethylbenzene 1020 38.4 100 100 04/01/2017 19:24 WG964562
Hexachloro-1,3-butadiene U 25.6 100 100 04/01/2017 19:24 WG964562
Isopropylbenzene 43.9 J 32.6 100 100 04/01/2017 19:24 WG964562
p-Isopropyltoluene U 35.0 100 100 04/01/2017 19:24 WG964562
2-Butanone (MEK)U 393 1000 100 04/01/2017 19:24 WG964562
Methylene Chloride U 100 500 100 04/01/2017 19:24 WG964562
4-Methyl-2-pentanone (MIBK)291 J 214 1000 100 04/01/2017 19:24 WG964562
Methyl tert-butyl ether 33700 367 1000 1000 04/04/2017 07:44 WG964562
Naphthalene 301 J 100 500 100 04/01/2017 19:24 WG964562
n-Propylbenzene 114 34.9 100 100 04/01/2017 19:24 WG964562
Styrene U 30.7 100 100 04/01/2017 19:24 WG964562
1,1,1,2-Tetrachloroethane U 38.5 100 100 04/01/2017 19:24 WG964562
1,1,2,2-Tetrachloroethane U 13.0 100 100 04/01/2017 19:24 WG964562
Tetrachloroethene U 37.2 100 100 04/01/2017 19:24 WG964562
Toluene 12100 41.2 100 100 04/01/2017 19:24 WG964562
1,2,3-Trichlorobenzene U 23.0 100 100 04/01/2017 19:24 WG964562
1,2,4-Trichlorobenzene U 35.5 100 100 04/01/2017 19:24 WG964562
1,1,1-Trichloroethane U 31.9 100 100 04/01/2017 19:24 WG964562
1,1,2-Trichloroethane U 38.3 100 100 04/01/2017 19:24 WG964562
Trichloroethene U 39.8 100 100 04/01/2017 19:24 WG964562
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L898293
MW-6
Collected date/time: 03/24/17 09:48
Volatile Organic Compounds (GC/MS) by Method 6200B-1997
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Trichlorofluoromethane U 120 500 100 04/01/2017 19:24 WG964562
1,2,3-Trichloropropane U 80.7 250 100 04/01/2017 19:24 WG964562
1,2,4-Trimethylbenzene 1110 37.3 100 100 04/01/2017 19:24 WG964562
1,3,5-Trimethylbenzene 340 38.7 100 100 04/01/2017 19:24 WG964562
Vinyl chloride U J3 25.9 100 100 04/01/2017 19:24 WG964562
o-Xylene 2790 34.1 100 100 04/01/2017 19:24 WG964562
m&p-Xylenes 4900 71.9 200 100 04/01/2017 19:24 WG964562
(S) Toluene-d8 100 80.0-120 04/04/2017 07:44 WG964562
(S) Toluene-d8 104 80.0-120 04/01/2017 19:24 WG964562
(S) Dibromofluoromethane 98.7 76.0-123 04/04/2017 07:44 WG964562
(S) Dibromofluoromethane 108 76.0-123 04/01/2017 19:24 WG964562
(S) a,a,a-Trifluorotoluene 93.2 80.0-120 04/04/2017 07:44 WG964562
(S) a,a,a-Trifluorotoluene 100 80.0-120 04/01/2017 19:24 WG964562
(S) 4-Bromofluorobenzene 88.5 80.0-120 04/04/2017 07:44 WG964562
(S) 4-Bromofluorobenzene 105 80.0-120 04/01/2017 19:24 WG964562
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L898293
MW-7
Collected date/time: 03/24/17 10:00
Volatile Organic Compounds (GC/MS) by Method 6200B-1997
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acetone U 1000 5000 100 04/01/2017 19:47 WG964562
Acrolein U J4 887 5000 100 04/01/2017 19:47 WG964562
Acrylonitrile U 187 1000 100 04/01/2017 19:47 WG964562
Benzene 5250 33.1 100 100 04/01/2017 19:47 WG964562
Bromobenzene U 35.2 100 100 04/01/2017 19:47 WG964562
Bromodichloromethane U 38.0 100 100 04/01/2017 19:47 WG964562
Bromoform U 46.9 100 100 04/01/2017 19:47 WG964562
Bromomethane U J3 86.6 500 100 04/01/2017 19:47 WG964562
n-Butylbenzene U 36.1 100 100 04/01/2017 19:47 WG964562
sec-Butylbenzene U 36.5 100 100 04/01/2017 19:47 WG964562
tert-Butylbenzene U 39.9 100 100 04/01/2017 19:47 WG964562
Carbon tetrachloride U 37.9 100 100 04/01/2017 19:47 WG964562
Chlorobenzene U 34.8 100 100 04/01/2017 19:47 WG964562
Chlorodibromomethane U 32.7 100 100 04/01/2017 19:47 WG964562
Chloroethane U 45.3 500 100 04/01/2017 19:47 WG964562
Chloroform U 32.4 500 100 04/01/2017 19:47 WG964562
Chloromethane U 27.6 250 100 04/01/2017 19:47 WG964562
2-Chlorotoluene U 37.5 100 100 04/01/2017 19:47 WG964562
4-Chlorotoluene U 35.1 100 100 04/01/2017 19:47 WG964562
1,2-Dibromo-3-Chloropropane U 133 500 100 04/01/2017 19:47 WG964562
1,2-Dibromoethane U 38.1 100 100 04/01/2017 19:47 WG964562
Dibromomethane U 34.6 100 100 04/01/2017 19:47 WG964562
1,2-Dichlorobenzene U 34.9 100 100 04/01/2017 19:47 WG964562
1,3-Dichlorobenzene U 22.0 100 100 04/01/2017 19:47 WG964562
1,4-Dichlorobenzene U 27.4 100 100 04/01/2017 19:47 WG964562
Dichlorodifluoromethane U 55.1 500 100 04/01/2017 19:47 WG964562
1,1-Dichloroethane U 25.9 100 100 04/01/2017 19:47 WG964562
1,2-Dichloroethane U 36.1 100 100 04/01/2017 19:47 WG964562
1,1-Dichloroethene U 39.8 100 100 04/01/2017 19:47 WG964562
cis-1,2-Dichloroethene U 26.0 100 100 04/01/2017 19:47 WG964562
trans-1,2-Dichloroethene U 39.6 100 100 04/01/2017 19:47 WG964562
1,2-Dichloropropane U 30.6 100 100 04/01/2017 19:47 WG964562
1,1-Dichloropropene U 35.2 100 100 04/01/2017 19:47 WG964562
1,3-Dichloropropane U 36.6 100 100 04/01/2017 19:47 WG964562
2,2-Dichloropropane U 32.1 100 100 04/01/2017 19:47 WG964562
Di-isopropyl ether 144 32.0 100 100 04/01/2017 19:47 WG964562
Ethylbenzene 386 38.4 100 100 04/01/2017 19:47 WG964562
Hexachloro-1,3-butadiene U 25.6 100 100 04/01/2017 19:47 WG964562
Isopropylbenzene 56.9 J 32.6 100 100 04/01/2017 19:47 WG964562
p-Isopropyltoluene U 35.0 100 100 04/01/2017 19:47 WG964562
2-Butanone (MEK)U 393 1000 100 04/01/2017 19:47 WG964562
Methylene Chloride U 100 500 100 04/01/2017 19:47 WG964562
4-Methyl-2-pentanone (MIBK)U 214 1000 100 04/01/2017 19:47 WG964562
Methyl tert-butyl ether 53700 367 1000 1000 04/04/2017 07:30 WG964562
Naphthalene 111 J 100 500 100 04/01/2017 19:47 WG964562
n-Propylbenzene 92.5 J 34.9 100 100 04/01/2017 19:47 WG964562
Styrene U 30.7 100 100 04/01/2017 19:47 WG964562
1,1,1,2-Tetrachloroethane U 38.5 100 100 04/01/2017 19:47 WG964562
1,1,2,2-Tetrachloroethane U 13.0 100 100 04/01/2017 19:47 WG964562
Tetrachloroethene U 37.2 100 100 04/01/2017 19:47 WG964562
Toluene 7430 41.2 100 100 04/01/2017 19:47 WG964562
1,2,3-Trichlorobenzene U 23.0 100 100 04/01/2017 19:47 WG964562
1,2,4-Trichlorobenzene U 35.5 100 100 04/01/2017 19:47 WG964562
1,1,1-Trichloroethane U 31.9 100 100 04/01/2017 19:47 WG964562
1,1,2-Trichloroethane U 38.3 100 100 04/01/2017 19:47 WG964562
Trichloroethene U 39.8 100 100 04/01/2017 19:47 WG964562
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L898293
MW-7
Collected date/time: 03/24/17 10:00
Volatile Organic Compounds (GC/MS) by Method 6200B-1997
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Trichlorofluoromethane U 120 500 100 04/01/2017 19:47 WG964562
1,2,3-Trichloropropane U 80.7 250 100 04/01/2017 19:47 WG964562
1,2,4-Trimethylbenzene 939 37.3 100 100 04/01/2017 19:47 WG964562
1,3,5-Trimethylbenzene 223 38.7 100 100 04/01/2017 19:47 WG964562
Vinyl chloride U J3 25.9 100 100 04/01/2017 19:47 WG964562
o-Xylene 1390 34.1 100 100 04/01/2017 19:47 WG964562
m&p-Xylenes 3510 71.9 200 100 04/01/2017 19:47 WG964562
(S) Toluene-d8 98.4 80.0-120 04/04/2017 07:30 WG964562
(S) Toluene-d8 103 80.0-120 04/01/2017 19:47 WG964562
(S) Dibromofluoromethane 100 76.0-123 04/04/2017 07:30 WG964562
(S) Dibromofluoromethane 107 76.0-123 04/01/2017 19:47 WG964562
(S) a,a,a-Trifluorotoluene 94.4 80.0-120 04/04/2017 07:30 WG964562
(S) a,a,a-Trifluorotoluene 99.0 80.0-120 04/01/2017 19:47 WG964562
(S) 4-Bromofluorobenzene 87.7 80.0-120 04/04/2017 07:30 WG964562
(S) 4-Bromofluorobenzene 102 80.0-120 04/01/2017 19:47 WG964562
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Excel Civil & Environmental Associates 24090 L898293 04/07/17 10:15 11 of 62
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04
L898293
MW-8
Collected date/time: 03/24/17 09:20
Volatile Organic Compounds (GC/MS) by Method 6200B-1997
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acetone U 50.0 250 5 04/01/2017 20:10 WG964562
Acrolein U J4 44.4 250 5 04/01/2017 20:10 WG964562
Acrylonitrile U 9.35 50.0 5 04/01/2017 20:10 WG964562
Benzene U 1.66 5.00 5 04/01/2017 20:10 WG964562
Bromobenzene U 1.76 5.00 5 04/01/2017 20:10 WG964562
Bromodichloromethane U 1.90 5.00 5 04/01/2017 20:10 WG964562
Bromoform U 2.34 5.00 5 04/01/2017 20:10 WG964562
Bromomethane U J3 4.33 25.0 5 04/01/2017 20:10 WG964562
n-Butylbenzene U 1.80 5.00 5 04/01/2017 20:10 WG964562
sec-Butylbenzene U 1.82 5.00 5 04/01/2017 20:10 WG964562
tert-Butylbenzene U 2.00 5.00 5 04/01/2017 20:10 WG964562
Carbon tetrachloride U 1.90 5.00 5 04/01/2017 20:10 WG964562
Chlorobenzene U 1.74 5.00 5 04/01/2017 20:10 WG964562
Chlorodibromomethane U 1.64 5.00 5 04/01/2017 20:10 WG964562
Chloroethane U 2.26 25.0 5 04/01/2017 20:10 WG964562
Chloroform U 1.62 25.0 5 04/01/2017 20:10 WG964562
Chloromethane U 1.38 12.5 5 04/01/2017 20:10 WG964562
2-Chlorotoluene U 1.88 5.00 5 04/01/2017 20:10 WG964562
4-Chlorotoluene U 1.76 5.00 5 04/01/2017 20:10 WG964562
1,2-Dibromo-3-Chloropropane U 6.65 25.0 5 04/01/2017 20:10 WG964562
1,2-Dibromoethane U 1.90 5.00 5 04/01/2017 20:10 WG964562
Dibromomethane U 1.73 5.00 5 04/01/2017 20:10 WG964562
1,2-Dichlorobenzene U 1.74 5.00 5 04/01/2017 20:10 WG964562
1,3-Dichlorobenzene U 1.10 5.00 5 04/01/2017 20:10 WG964562
1,4-Dichlorobenzene U 1.37 5.00 5 04/01/2017 20:10 WG964562
Dichlorodifluoromethane U 2.76 25.0 5 04/01/2017 20:10 WG964562
1,1-Dichloroethane U 1.30 5.00 5 04/01/2017 20:10 WG964562
1,2-Dichloroethane U 1.80 5.00 5 04/01/2017 20:10 WG964562
1,1-Dichloroethene U 1.99 5.00 5 04/01/2017 20:10 WG964562
cis-1,2-Dichloroethene U 1.30 5.00 5 04/01/2017 20:10 WG964562
trans-1,2-Dichloroethene U 1.98 5.00 5 04/01/2017 20:10 WG964562
1,2-Dichloropropane U 1.53 5.00 5 04/01/2017 20:10 WG964562
1,1-Dichloropropene U 1.76 5.00 5 04/01/2017 20:10 WG964562
1,3-Dichloropropane U 1.83 5.00 5 04/01/2017 20:10 WG964562
2,2-Dichloropropane U 1.60 5.00 5 04/01/2017 20:10 WG964562
Di-isopropyl ether 23.4 1.60 5.00 5 04/01/2017 20:10 WG964562
Ethylbenzene U 1.92 5.00 5 04/01/2017 20:10 WG964562
Hexachloro-1,3-butadiene U 1.28 5.00 5 04/01/2017 20:10 WG964562
Isopropylbenzene U 1.63 5.00 5 04/01/2017 20:10 WG964562
p-Isopropyltoluene U 1.75 5.00 5 04/01/2017 20:10 WG964562
2-Butanone (MEK)U 19.6 50.0 5 04/01/2017 20:10 WG964562
Methylene Chloride U 5.00 25.0 5 04/01/2017 20:10 WG964562
4-Methyl-2-pentanone (MIBK)U 10.7 50.0 5 04/01/2017 20:10 WG964562
Methyl tert-butyl ether 17100 184 500 500 04/04/2017 07:17 WG964562
Naphthalene U 5.00 25.0 5 04/01/2017 20:10 WG964562
n-Propylbenzene U 1.74 5.00 5 04/01/2017 20:10 WG964562
Styrene U 1.54 5.00 5 04/01/2017 20:10 WG964562
1,1,1,2-Tetrachloroethane U 1.92 5.00 5 04/01/2017 20:10 WG964562
1,1,2,2-Tetrachloroethane U 0.650 5.00 5 04/01/2017 20:10 WG964562
Tetrachloroethene U 1.86 5.00 5 04/01/2017 20:10 WG964562
Toluene U 2.06 5.00 5 04/01/2017 20:10 WG964562
1,2,3-Trichlorobenzene U 1.15 5.00 5 04/01/2017 20:10 WG964562
1,2,4-Trichlorobenzene U 1.78 5.00 5 04/01/2017 20:10 WG964562
1,1,1-Trichloroethane U 1.60 5.00 5 04/01/2017 20:10 WG964562
1,1,2-Trichloroethane U 1.92 5.00 5 04/01/2017 20:10 WG964562
Trichloroethene U 1.99 5.00 5 04/01/2017 20:10 WG964562
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Excel Civil & Environmental Associates 24090 L898293 04/07/17 10:15 12 of 62
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04
L898293
MW-8
Collected date/time: 03/24/17 09:20
Volatile Organic Compounds (GC/MS) by Method 6200B-1997
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Trichlorofluoromethane U 6.00 25.0 5 04/01/2017 20:10 WG964562
1,2,3-Trichloropropane U 4.04 12.5 5 04/01/2017 20:10 WG964562
1,2,4-Trimethylbenzene U 1.86 5.00 5 04/01/2017 20:10 WG964562
1,3,5-Trimethylbenzene U 1.94 5.00 5 04/01/2017 20:10 WG964562
Vinyl chloride U J3 1.30 5.00 5 04/01/2017 20:10 WG964562
o-Xylene U 1.70 5.00 5 04/01/2017 20:10 WG964562
m&p-Xylenes U 3.60 10.0 5 04/01/2017 20:10 WG964562
(S) Toluene-d8 96.7 80.0-120 04/04/2017 07:17 WG964562
(S) Toluene-d8 103 80.0-120 04/01/2017 20:10 WG964562
(S) Dibromofluoromethane 98.9 76.0-123 04/04/2017 07:17 WG964562
(S) Dibromofluoromethane 108 76.0-123 04/01/2017 20:10 WG964562
(S) a,a,a-Trifluorotoluene 94.7 80.0-120 04/04/2017 07:17 WG964562
(S) a,a,a-Trifluorotoluene 100 80.0-120 04/01/2017 20:10 WG964562
(S) 4-Bromofluorobenzene 85.6 80.0-120 04/04/2017 07:17 WG964562
(S) 4-Bromofluorobenzene 100 80.0-120 04/01/2017 20:10 WG964562
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Excel Civil & Environmental Associates 24090 L898293 04/07/17 10:15 13 of 62
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 05
L898293
MW-9
Collected date/time: 03/24/17 10:15
Volatile Organic Compounds (GC/MS) by Method 6200B-1997
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acetone U 500 2500 50 04/01/2017 20:33 WG964562
Acrolein U J4 444 2500 50 04/01/2017 20:33 WG964562
Acrylonitrile U 93.5 500 50 04/01/2017 20:33 WG964562
Benzene 4450 16.6 50.0 50 04/01/2017 20:33 WG964562
Bromobenzene U 17.6 50.0 50 04/01/2017 20:33 WG964562
Bromodichloromethane U 19.0 50.0 50 04/01/2017 20:33 WG964562
Bromoform U 23.4 50.0 50 04/01/2017 20:33 WG964562
Bromomethane U J3 43.3 250 50 04/01/2017 20:33 WG964562
n-Butylbenzene U 18.0 50.0 50 04/01/2017 20:33 WG964562
sec-Butylbenzene U 18.2 50.0 50 04/01/2017 20:33 WG964562
tert-Butylbenzene U 20.0 50.0 50 04/01/2017 20:33 WG964562
Carbon tetrachloride U 19.0 50.0 50 04/01/2017 20:33 WG964562
Chlorobenzene U 17.4 50.0 50 04/01/2017 20:33 WG964562
Chlorodibromomethane U 16.4 50.0 50 04/01/2017 20:33 WG964562
Chloroethane U 22.6 250 50 04/01/2017 20:33 WG964562
Chloroform 19.4 J 16.2 250 50 04/01/2017 20:33 WG964562
Chloromethane 51.2 J 13.8 125 50 04/01/2017 20:33 WG964562
2-Chlorotoluene U 18.8 50.0 50 04/01/2017 20:33 WG964562
4-Chlorotoluene U 17.6 50.0 50 04/01/2017 20:33 WG964562
1,2-Dibromo-3-Chloropropane U 66.5 250 50 04/01/2017 20:33 WG964562
1,2-Dibromoethane U 19.0 50.0 50 04/01/2017 20:33 WG964562
Dibromomethane U 17.3 50.0 50 04/01/2017 20:33 WG964562
1,2-Dichlorobenzene U 17.4 50.0 50 04/01/2017 20:33 WG964562
1,3-Dichlorobenzene U 11.0 50.0 50 04/01/2017 20:33 WG964562
1,4-Dichlorobenzene U 13.7 50.0 50 04/01/2017 20:33 WG964562
Dichlorodifluoromethane U 27.6 250 50 04/01/2017 20:33 WG964562
1,1-Dichloroethane U 13.0 50.0 50 04/01/2017 20:33 WG964562
1,2-Dichloroethane U 18.0 50.0 50 04/01/2017 20:33 WG964562
1,1-Dichloroethene U 19.9 50.0 50 04/01/2017 20:33 WG964562
cis-1,2-Dichloroethene U 13.0 50.0 50 04/01/2017 20:33 WG964562
trans-1,2-Dichloroethene U 19.8 50.0 50 04/01/2017 20:33 WG964562
1,2-Dichloropropane U 15.3 50.0 50 04/01/2017 20:33 WG964562
1,1-Dichloropropene U 17.6 50.0 50 04/01/2017 20:33 WG964562
1,3-Dichloropropane U 18.3 50.0 50 04/01/2017 20:33 WG964562
2,2-Dichloropropane U 16.0 50.0 50 04/01/2017 20:33 WG964562
Di-isopropyl ether U 16.0 50.0 50 04/01/2017 20:33 WG964562
Ethylbenzene 153 19.2 50.0 50 04/01/2017 20:33 WG964562
Hexachloro-1,3-butadiene U 12.8 50.0 50 04/01/2017 20:33 WG964562
Isopropylbenzene 24.0 J 16.3 50.0 50 04/01/2017 20:33 WG964562
p-Isopropyltoluene U 17.5 50.0 50 04/01/2017 20:33 WG964562
2-Butanone (MEK)U 196 500 50 04/01/2017 20:33 WG964562
Methylene Chloride U 50.0 250 50 04/01/2017 20:33 WG964562
4-Methyl-2-pentanone (MIBK)U 107 500 50 04/01/2017 20:33 WG964562
Methyl tert-butyl ether U 18.4 50.0 50 04/04/2017 07:03 WG964562
Naphthalene 65.7 J 50.0 250 50 04/01/2017 20:33 WG964562
n-Propylbenzene 21.5 J 17.4 50.0 50 04/01/2017 20:33 WG964562
Styrene U 15.4 50.0 50 04/01/2017 20:33 WG964562
1,1,1,2-Tetrachloroethane U 19.2 50.0 50 04/01/2017 20:33 WG964562
1,1,2,2-Tetrachloroethane U 6.50 50.0 50 04/01/2017 20:33 WG964562
Tetrachloroethene U 18.6 50.0 50 04/01/2017 20:33 WG964562
Toluene 87.6 20.6 50.0 50 04/01/2017 20:33 WG964562
1,2,3-Trichlorobenzene U 11.5 50.0 50 04/01/2017 20:33 WG964562
1,2,4-Trichlorobenzene U 17.8 50.0 50 04/01/2017 20:33 WG964562
1,1,1-Trichloroethane U 16.0 50.0 50 04/01/2017 20:33 WG964562
1,1,2-Trichloroethane U 19.2 50.0 50 04/01/2017 20:33 WG964562
Trichloroethene U 19.9 50.0 50 04/01/2017 20:33 WG964562
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Excel Civil & Environmental Associates 24090 L898293 04/07/17 10:15 14 of 62
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 05
L898293
MW-9
Collected date/time: 03/24/17 10:15
Volatile Organic Compounds (GC/MS) by Method 6200B-1997
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Trichlorofluoromethane U 60.0 250 50 04/01/2017 20:33 WG964562
1,2,3-Trichloropropane U 40.4 125 50 04/01/2017 20:33 WG964562
1,2,4-Trimethylbenzene 175 18.6 50.0 50 04/01/2017 20:33 WG964562
1,3,5-Trimethylbenzene 52.3 19.4 50.0 50 04/01/2017 20:33 WG964562
Vinyl chloride U J3 13.0 50.0 50 04/01/2017 20:33 WG964562
o-Xylene 506 17.0 50.0 50 04/01/2017 20:33 WG964562
m&p-Xylenes 975 36.0 100 50 04/01/2017 20:33 WG964562
(S) Toluene-d8 100 80.0-120 04/04/2017 07:03 WG964562
(S) Toluene-d8 103 80.0-120 04/01/2017 20:33 WG964562
(S) Dibromofluoromethane 95.2 76.0-123 04/04/2017 07:03 WG964562
(S) Dibromofluoromethane 107 76.0-123 04/01/2017 20:33 WG964562
(S) a,a,a-Trifluorotoluene 93.8 80.0-120 04/04/2017 07:03 WG964562
(S) a,a,a-Trifluorotoluene 100 80.0-120 04/01/2017 20:33 WG964562
(S) 4-Bromofluorobenzene 89.1 80.0-120 04/04/2017 07:03 WG964562
(S) 4-Bromofluorobenzene 102 80.0-120 04/01/2017 20:33 WG964562
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Excel Civil & Environmental Associates 24090 L898293 04/07/17 09:00 15 of 62
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Excel Civil & Environmental Associates 24090 L898293 04/07/17 10:15 15 of 62
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 06
L898293
MW-10
Collected date/time: 03/24/17 10:27
Volatile Organic Compounds (GC/MS) by Method 6200B-1997
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acetone U 10.0 50.0 1 04/01/2017 17:06 WG964562
Acrolein U J4 8.87 50.0 1 04/01/2017 17:06 WG964562
Acrylonitrile U 1.87 10.0 1 04/01/2017 17:06 WG964562
Benzene 80.0 0.331 1.00 1 04/01/2017 17:06 WG964562
Bromobenzene U 0.352 1.00 1 04/01/2017 17:06 WG964562
Bromodichloromethane U 0.380 1.00 1 04/01/2017 17:06 WG964562
Bromoform U 0.469 1.00 1 04/01/2017 17:06 WG964562
Bromomethane U J3 0.866 5.00 1 04/01/2017 17:06 WG964562
n-Butylbenzene 0.596 J 0.361 1.00 1 04/01/2017 17:06 WG964562
sec-Butylbenzene 0.548 J 0.365 1.00 1 04/01/2017 17:06 WG964562
tert-Butylbenzene U 0.399 1.00 1 04/01/2017 17:06 WG964562
Carbon tetrachloride U 0.379 1.00 1 04/01/2017 17:06 WG964562
Chlorobenzene U 0.348 1.00 1 04/01/2017 17:06 WG964562
Chlorodibromomethane U 0.327 1.00 1 04/01/2017 17:06 WG964562
Chloroethane U 0.453 5.00 1 04/01/2017 17:06 WG964562
Chloroform U 0.324 5.00 1 04/01/2017 17:06 WG964562
Chloromethane U 0.276 2.50 1 04/01/2017 17:06 WG964562
2-Chlorotoluene U 0.375 1.00 1 04/01/2017 17:06 WG964562
4-Chlorotoluene U 0.351 1.00 1 04/01/2017 17:06 WG964562
1,2-Dibromo-3-Chloropropane U 1.33 5.00 1 04/01/2017 17:06 WG964562
1,2-Dibromoethane U 0.381 1.00 1 04/01/2017 17:06 WG964562
Dibromomethane U 0.346 1.00 1 04/01/2017 17:06 WG964562
1,2-Dichlorobenzene U 0.349 1.00 1 04/01/2017 17:06 WG964562
1,3-Dichlorobenzene U 0.220 1.00 1 04/01/2017 17:06 WG964562
1,4-Dichlorobenzene U 0.274 1.00 1 04/01/2017 17:06 WG964562
Dichlorodifluoromethane U 0.551 5.00 1 04/01/2017 17:06 WG964562
1,1-Dichloroethane U 0.259 1.00 1 04/01/2017 17:06 WG964562
1,2-Dichloroethane 3.04 0.361 1.00 1 04/01/2017 17:06 WG964562
1,1-Dichloroethene U 0.398 1.00 1 04/01/2017 17:06 WG964562
cis-1,2-Dichloroethene U 0.260 1.00 1 04/01/2017 17:06 WG964562
trans-1,2-Dichloroethene U 0.396 1.00 1 04/01/2017 17:06 WG964562
1,2-Dichloropropane U 0.306 1.00 1 04/01/2017 17:06 WG964562
1,1-Dichloropropene U 0.352 1.00 1 04/01/2017 17:06 WG964562
1,3-Dichloropropane U 0.366 1.00 1 04/01/2017 17:06 WG964562
2,2-Dichloropropane U 0.321 1.00 1 04/01/2017 17:06 WG964562
Di-isopropyl ether 10.1 0.320 1.00 1 04/01/2017 17:06 WG964562
Ethylbenzene 12.7 0.384 1.00 1 04/01/2017 17:06 WG964562
Hexachloro-1,3-butadiene U 0.256 1.00 1 04/01/2017 17:06 WG964562
Isopropylbenzene 3.04 0.326 1.00 1 04/01/2017 17:06 WG964562
p-Isopropyltoluene 0.563 J 0.350 1.00 1 04/01/2017 17:06 WG964562
2-Butanone (MEK)U 3.93 10.0 1 04/01/2017 17:06 WG964562
Methylene Chloride U 1.00 5.00 1 04/01/2017 17:06 WG964562
4-Methyl-2-pentanone (MIBK)U 2.14 10.0 1 04/01/2017 17:06 WG964562
Methyl tert-butyl ether 183 0.367 1.00 1 04/01/2017 17:06 WG964562
Naphthalene 18.5 1.00 5.00 1 04/01/2017 17:06 WG964562
n-Propylbenzene 2.11 0.349 1.00 1 04/01/2017 17:06 WG964562
Styrene U 0.307 1.00 1 04/01/2017 17:06 WG964562
1,1,1,2-Tetrachloroethane U 0.385 1.00 1 04/01/2017 17:06 WG964562
1,1,2,2-Tetrachloroethane U 0.130 1.00 1 04/01/2017 17:06 WG964562
Tetrachloroethene 0.610 J 0.372 1.00 1 04/01/2017 17:06 WG964562
Toluene 1.73 0.412 1.00 1 04/01/2017 17:06 WG964562
1,2,3-Trichlorobenzene U 0.230 1.00 1 04/01/2017 17:06 WG964562
1,2,4-Trichlorobenzene U 0.355 1.00 1 04/01/2017 17:06 WG964562
1,1,1-Trichloroethane U 0.319 1.00 1 04/01/2017 17:06 WG964562
1,1,2-Trichloroethane U 0.383 1.00 1 04/01/2017 17:06 WG964562
Trichloroethene U 0.398 1.00 1 04/01/2017 17:06 WG964562
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 06
L898293
MW-10
Collected date/time: 03/24/17 10:27
Volatile Organic Compounds (GC/MS) by Method 6200B-1997
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Trichlorofluoromethane U 1.20 5.00 1 04/01/2017 17:06 WG964562
1,2,3-Trichloropropane U 0.807 2.50 1 04/01/2017 17:06 WG964562
1,2,4-Trimethylbenzene 30.6 0.373 1.00 1 04/01/2017 17:06 WG964562
1,3,5-Trimethylbenzene 17.0 0.387 1.00 1 04/01/2017 17:06 WG964562
Vinyl chloride U J3 0.259 1.00 1 04/01/2017 17:06 WG964562
o-Xylene 61.5 0.341 1.00 1 04/01/2017 17:06 WG964562
m&p-Xylenes 88.6 0.719 2.00 1 04/01/2017 17:06 WG964562
(S) Toluene-d8 105 80.0-120 04/01/2017 17:06 WG964562
(S) Dibromofluoromethane 105 76.0-123 04/01/2017 17:06 WG964562
(S) a,a,a-Trifluorotoluene 99.3 80.0-120 04/01/2017 17:06 WG964562
(S) 4-Bromofluorobenzene 103 80.0-120 04/01/2017 17:06 WG964562
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Excel Civil & Environmental Associates 24090 L898293 04/07/17 10:15 17 of 62
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 07
L898293
MW-11
Collected date/time: 03/24/17 10:54
Volatile Organic Compounds (GC/MS) by Method 6200B-1997
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acetone U 10.0 50.0 1 04/01/2017 17:29 WG964562
Acrolein U J4 8.87 50.0 1 04/01/2017 17:29 WG964562
Acrylonitrile U 1.87 10.0 1 04/01/2017 17:29 WG964562
Benzene U 0.331 1.00 1 04/01/2017 17:29 WG964562
Bromobenzene U 0.352 1.00 1 04/01/2017 17:29 WG964562
Bromodichloromethane U 0.380 1.00 1 04/01/2017 17:29 WG964562
Bromoform U 0.469 1.00 1 04/01/2017 17:29 WG964562
Bromomethane U J3 0.866 5.00 1 04/01/2017 17:29 WG964562
n-Butylbenzene U 0.361 1.00 1 04/01/2017 17:29 WG964562
sec-Butylbenzene U 0.365 1.00 1 04/01/2017 17:29 WG964562
tert-Butylbenzene U 0.399 1.00 1 04/01/2017 17:29 WG964562
Carbon tetrachloride U 0.379 1.00 1 04/01/2017 17:29 WG964562
Chlorobenzene U 0.348 1.00 1 04/01/2017 17:29 WG964562
Chlorodibromomethane U 0.327 1.00 1 04/01/2017 17:29 WG964562
Chloroethane U 0.453 5.00 1 04/01/2017 17:29 WG964562
Chloroform U 0.324 5.00 1 04/01/2017 17:29 WG964562
Chloromethane U 0.276 2.50 1 04/01/2017 17:29 WG964562
2-Chlorotoluene U 0.375 1.00 1 04/01/2017 17:29 WG964562
4-Chlorotoluene U 0.351 1.00 1 04/01/2017 17:29 WG964562
1,2-Dibromo-3-Chloropropane U 1.33 5.00 1 04/01/2017 17:29 WG964562
1,2-Dibromoethane U 0.381 1.00 1 04/01/2017 17:29 WG964562
Dibromomethane U 0.346 1.00 1 04/01/2017 17:29 WG964562
1,2-Dichlorobenzene U 0.349 1.00 1 04/01/2017 17:29 WG964562
1,3-Dichlorobenzene U 0.220 1.00 1 04/01/2017 17:29 WG964562
1,4-Dichlorobenzene U 0.274 1.00 1 04/01/2017 17:29 WG964562
Dichlorodifluoromethane U 0.551 5.00 1 04/01/2017 17:29 WG964562
1,1-Dichloroethane U 0.259 1.00 1 04/01/2017 17:29 WG964562
1,2-Dichloroethane U 0.361 1.00 1 04/01/2017 17:29 WG964562
1,1-Dichloroethene U 0.398 1.00 1 04/01/2017 17:29 WG964562
cis-1,2-Dichloroethene U 0.260 1.00 1 04/01/2017 17:29 WG964562
trans-1,2-Dichloroethene U 0.396 1.00 1 04/01/2017 17:29 WG964562
1,2-Dichloropropane U 0.306 1.00 1 04/01/2017 17:29 WG964562
1,1-Dichloropropene U 0.352 1.00 1 04/01/2017 17:29 WG964562
1,3-Dichloropropane U 0.366 1.00 1 04/01/2017 17:29 WG964562
2,2-Dichloropropane U 0.321 1.00 1 04/01/2017 17:29 WG964562
Di-isopropyl ether U 0.320 1.00 1 04/01/2017 17:29 WG964562
Ethylbenzene U 0.384 1.00 1 04/01/2017 17:29 WG964562
Hexachloro-1,3-butadiene U 0.256 1.00 1 04/01/2017 17:29 WG964562
Isopropylbenzene U 0.326 1.00 1 04/01/2017 17:29 WG964562
p-Isopropyltoluene U 0.350 1.00 1 04/01/2017 17:29 WG964562
2-Butanone (MEK)U 3.93 10.0 1 04/01/2017 17:29 WG964562
Methylene Chloride U 1.00 5.00 1 04/01/2017 17:29 WG964562
4-Methyl-2-pentanone (MIBK)U 2.14 10.0 1 04/01/2017 17:29 WG964562
Methyl tert-butyl ether U 0.367 1.00 1 04/01/2017 17:29 WG964562
Naphthalene U 1.00 5.00 1 04/01/2017 17:29 WG964562
n-Propylbenzene U 0.349 1.00 1 04/01/2017 17:29 WG964562
Styrene U 0.307 1.00 1 04/01/2017 17:29 WG964562
1,1,1,2-Tetrachloroethane U 0.385 1.00 1 04/01/2017 17:29 WG964562
1,1,2,2-Tetrachloroethane U 0.130 1.00 1 04/01/2017 17:29 WG964562
Tetrachloroethene U 0.372 1.00 1 04/01/2017 17:29 WG964562
Toluene U 0.412 1.00 1 04/01/2017 17:29 WG964562
1,2,3-Trichlorobenzene U 0.230 1.00 1 04/01/2017 17:29 WG964562
1,2,4-Trichlorobenzene U 0.355 1.00 1 04/01/2017 17:29 WG964562
1,1,1-Trichloroethane U 0.319 1.00 1 04/01/2017 17:29 WG964562
1,1,2-Trichloroethane U 0.383 1.00 1 04/01/2017 17:29 WG964562
Trichloroethene U 0.398 1.00 1 04/01/2017 17:29 WG964562
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 07
L898293
MW-11
Collected date/time: 03/24/17 10:54
Volatile Organic Compounds (GC/MS) by Method 6200B-1997
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Trichlorofluoromethane U 1.20 5.00 1 04/01/2017 17:29 WG964562
1,2,3-Trichloropropane U 0.807 2.50 1 04/01/2017 17:29 WG964562
1,2,4-Trimethylbenzene U 0.373 1.00 1 04/01/2017 17:29 WG964562
1,3,5-Trimethylbenzene U 0.387 1.00 1 04/01/2017 17:29 WG964562
Vinyl chloride U J3 0.259 1.00 1 04/01/2017 17:29 WG964562
o-Xylene U 0.341 1.00 1 04/01/2017 17:29 WG964562
m&p-Xylenes U 0.719 2.00 1 04/01/2017 17:29 WG964562
(S) Toluene-d8 104 80.0-120 04/01/2017 17:29 WG964562
(S) Dibromofluoromethane 108 76.0-123 04/01/2017 17:29 WG964562
(S) a,a,a-Trifluorotoluene 99.3 80.0-120 04/01/2017 17:29 WG964562
(S) 4-Bromofluorobenzene 103 80.0-120 04/01/2017 17:29 WG964562
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Excel Civil & Environmental Associates 24090 L898293 04/07/17 10:15 19 of 62
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 08
L898293
MW-13
Collected date/time: 03/24/17 10:41
Volatile Organic Compounds (GC/MS) by Method 6200B-1997
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acetone U 10.0 50.0 1 04/01/2017 17:52 WG964562
Acrolein U J4 8.87 50.0 1 04/01/2017 17:52 WG964562
Acrylonitrile U 1.87 10.0 1 04/01/2017 17:52 WG964562
Benzene U 0.331 1.00 1 04/01/2017 17:52 WG964562
Bromobenzene U 0.352 1.00 1 04/01/2017 17:52 WG964562
Bromodichloromethane U 0.380 1.00 1 04/01/2017 17:52 WG964562
Bromoform U 0.469 1.00 1 04/01/2017 17:52 WG964562
Bromomethane U J3 0.866 5.00 1 04/01/2017 17:52 WG964562
n-Butylbenzene U 0.361 1.00 1 04/01/2017 17:52 WG964562
sec-Butylbenzene U 0.365 1.00 1 04/01/2017 17:52 WG964562
tert-Butylbenzene U 0.399 1.00 1 04/01/2017 17:52 WG964562
Carbon tetrachloride U 0.379 1.00 1 04/01/2017 17:52 WG964562
Chlorobenzene U 0.348 1.00 1 04/01/2017 17:52 WG964562
Chlorodibromomethane U 0.327 1.00 1 04/01/2017 17:52 WG964562
Chloroethane U 0.453 5.00 1 04/01/2017 17:52 WG964562
Chloroform U 0.324 5.00 1 04/01/2017 17:52 WG964562
Chloromethane U 0.276 2.50 1 04/01/2017 17:52 WG964562
2-Chlorotoluene U 0.375 1.00 1 04/01/2017 17:52 WG964562
4-Chlorotoluene U 0.351 1.00 1 04/01/2017 17:52 WG964562
1,2-Dibromo-3-Chloropropane U 1.33 5.00 1 04/01/2017 17:52 WG964562
1,2-Dibromoethane U 0.381 1.00 1 04/01/2017 17:52 WG964562
Dibromomethane U 0.346 1.00 1 04/01/2017 17:52 WG964562
1,2-Dichlorobenzene U 0.349 1.00 1 04/01/2017 17:52 WG964562
1,3-Dichlorobenzene U 0.220 1.00 1 04/01/2017 17:52 WG964562
1,4-Dichlorobenzene U 0.274 1.00 1 04/01/2017 17:52 WG964562
Dichlorodifluoromethane U 0.551 5.00 1 04/01/2017 17:52 WG964562
1,1-Dichloroethane U 0.259 1.00 1 04/01/2017 17:52 WG964562
1,2-Dichloroethane U 0.361 1.00 1 04/01/2017 17:52 WG964562
1,1-Dichloroethene U 0.398 1.00 1 04/01/2017 17:52 WG964562
cis-1,2-Dichloroethene U 0.260 1.00 1 04/01/2017 17:52 WG964562
trans-1,2-Dichloroethene U 0.396 1.00 1 04/01/2017 17:52 WG964562
1,2-Dichloropropane U 0.306 1.00 1 04/01/2017 17:52 WG964562
1,1-Dichloropropene U 0.352 1.00 1 04/01/2017 17:52 WG964562
1,3-Dichloropropane U 0.366 1.00 1 04/01/2017 17:52 WG964562
2,2-Dichloropropane U 0.321 1.00 1 04/01/2017 17:52 WG964562
Di-isopropyl ether U 0.320 1.00 1 04/01/2017 17:52 WG964562
Ethylbenzene U 0.384 1.00 1 04/01/2017 17:52 WG964562
Hexachloro-1,3-butadiene U 0.256 1.00 1 04/01/2017 17:52 WG964562
Isopropylbenzene U 0.326 1.00 1 04/01/2017 17:52 WG964562
p-Isopropyltoluene U 0.350 1.00 1 04/01/2017 17:52 WG964562
2-Butanone (MEK)U 3.93 10.0 1 04/01/2017 17:52 WG964562
Methylene Chloride U 1.00 5.00 1 04/01/2017 17:52 WG964562
4-Methyl-2-pentanone (MIBK)U 2.14 10.0 1 04/01/2017 17:52 WG964562
Methyl tert-butyl ether U 0.367 1.00 1 04/01/2017 17:52 WG964562
Naphthalene U 1.00 5.00 1 04/01/2017 17:52 WG964562
n-Propylbenzene U 0.349 1.00 1 04/01/2017 17:52 WG964562
Styrene U 0.307 1.00 1 04/01/2017 17:52 WG964562
1,1,1,2-Tetrachloroethane U 0.385 1.00 1 04/01/2017 17:52 WG964562
1,1,2,2-Tetrachloroethane U 0.130 1.00 1 04/01/2017 17:52 WG964562
Tetrachloroethene U 0.372 1.00 1 04/01/2017 17:52 WG964562
Toluene U 0.412 1.00 1 04/01/2017 17:52 WG964562
1,2,3-Trichlorobenzene U 0.230 1.00 1 04/01/2017 17:52 WG964562
1,2,4-Trichlorobenzene U 0.355 1.00 1 04/01/2017 17:52 WG964562
1,1,1-Trichloroethane U 0.319 1.00 1 04/01/2017 17:52 WG964562
1,1,2-Trichloroethane U 0.383 1.00 1 04/01/2017 17:52 WG964562
Trichloroethene U 0.398 1.00 1 04/01/2017 17:52 WG964562
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Excel Civil & Environmental Associates 24090 L898293 04/07/17 10:15 20 of 62
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 08
L898293
MW-13
Collected date/time: 03/24/17 10:41
Volatile Organic Compounds (GC/MS) by Method 6200B-1997
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Trichlorofluoromethane U 1.20 5.00 1 04/01/2017 17:52 WG964562
1,2,3-Trichloropropane U 0.807 2.50 1 04/01/2017 17:52 WG964562
1,2,4-Trimethylbenzene U 0.373 1.00 1 04/01/2017 17:52 WG964562
1,3,5-Trimethylbenzene U 0.387 1.00 1 04/01/2017 17:52 WG964562
Vinyl chloride U J3 0.259 1.00 1 04/01/2017 17:52 WG964562
o-Xylene U 0.341 1.00 1 04/01/2017 17:52 WG964562
m&p-Xylenes U 0.719 2.00 1 04/01/2017 17:52 WG964562
(S) Toluene-d8 104 80.0-120 04/01/2017 17:52 WG964562
(S) Dibromofluoromethane 108 76.0-123 04/01/2017 17:52 WG964562
(S) a,a,a-Trifluorotoluene 101 80.0-120 04/01/2017 17:52 WG964562
(S) 4-Bromofluorobenzene 103 80.0-120 04/01/2017 17:52 WG964562
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Excel Civil & Environmental Associates 24090 L898293 04/07/17 10:15 21 of 62
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 09
L898293
TRIPBLANK
Collected date/time: 03/24/17 00:00
Volatile Organic Compounds (GC/MS) by Method 6200B-1997
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acetone U 10.0 50.0 1 04/01/2017 18:15 WG964562
Acrolein U J4 8.87 50.0 1 04/01/2017 18:15 WG964562
Acrylonitrile U 1.87 10.0 1 04/01/2017 18:15 WG964562
Benzene U 0.331 1.00 1 04/01/2017 18:15 WG964562
Bromobenzene U 0.352 1.00 1 04/01/2017 18:15 WG964562
Bromodichloromethane U 0.380 1.00 1 04/01/2017 18:15 WG964562
Bromoform U 0.469 1.00 1 04/01/2017 18:15 WG964562
Bromomethane U J3 0.866 5.00 1 04/01/2017 18:15 WG964562
n-Butylbenzene U 0.361 1.00 1 04/01/2017 18:15 WG964562
sec-Butylbenzene U 0.365 1.00 1 04/01/2017 18:15 WG964562
tert-Butylbenzene U 0.399 1.00 1 04/01/2017 18:15 WG964562
Carbon tetrachloride U 0.379 1.00 1 04/01/2017 18:15 WG964562
Chlorobenzene U 0.348 1.00 1 04/01/2017 18:15 WG964562
Chlorodibromomethane U 0.327 1.00 1 04/01/2017 18:15 WG964562
Chloroethane U 0.453 5.00 1 04/01/2017 18:15 WG964562
Chloroform U 0.324 5.00 1 04/01/2017 18:15 WG964562
Chloromethane U 0.276 2.50 1 04/01/2017 18:15 WG964562
2-Chlorotoluene U 0.375 1.00 1 04/01/2017 18:15 WG964562
4-Chlorotoluene U 0.351 1.00 1 04/01/2017 18:15 WG964562
1,2-Dibromo-3-Chloropropane U 1.33 5.00 1 04/01/2017 18:15 WG964562
1,2-Dibromoethane U 0.381 1.00 1 04/01/2017 18:15 WG964562
Dibromomethane U 0.346 1.00 1 04/01/2017 18:15 WG964562
1,2-Dichlorobenzene U 0.349 1.00 1 04/01/2017 18:15 WG964562
1,3-Dichlorobenzene U 0.220 1.00 1 04/01/2017 18:15 WG964562
1,4-Dichlorobenzene U 0.274 1.00 1 04/01/2017 18:15 WG964562
Dichlorodifluoromethane U 0.551 5.00 1 04/01/2017 18:15 WG964562
1,1-Dichloroethane U 0.259 1.00 1 04/01/2017 18:15 WG964562
1,2-Dichloroethane U 0.361 1.00 1 04/01/2017 18:15 WG964562
1,1-Dichloroethene U 0.398 1.00 1 04/01/2017 18:15 WG964562
cis-1,2-Dichloroethene U 0.260 1.00 1 04/01/2017 18:15 WG964562
trans-1,2-Dichloroethene U 0.396 1.00 1 04/01/2017 18:15 WG964562
1,2-Dichloropropane U 0.306 1.00 1 04/01/2017 18:15 WG964562
1,1-Dichloropropene U 0.352 1.00 1 04/01/2017 18:15 WG964562
1,3-Dichloropropane U 0.366 1.00 1 04/01/2017 18:15 WG964562
2,2-Dichloropropane U 0.321 1.00 1 04/01/2017 18:15 WG964562
Di-isopropyl ether U 0.320 1.00 1 04/01/2017 18:15 WG964562
Ethylbenzene U 0.384 1.00 1 04/01/2017 18:15 WG964562
Hexachloro-1,3-butadiene U 0.256 1.00 1 04/01/2017 18:15 WG964562
Isopropylbenzene U 0.326 1.00 1 04/01/2017 18:15 WG964562
p-Isopropyltoluene U 0.350 1.00 1 04/01/2017 18:15 WG964562
2-Butanone (MEK)U 3.93 10.0 1 04/01/2017 18:15 WG964562
Methylene Chloride U 1.00 5.00 1 04/01/2017 18:15 WG964562
4-Methyl-2-pentanone (MIBK)U 2.14 10.0 1 04/01/2017 18:15 WG964562
Methyl tert-butyl ether U 0.367 1.00 1 04/01/2017 18:15 WG964562
Naphthalene U 1.00 5.00 1 04/01/2017 18:15 WG964562
n-Propylbenzene U 0.349 1.00 1 04/01/2017 18:15 WG964562
Styrene U 0.307 1.00 1 04/01/2017 18:15 WG964562
1,1,1,2-Tetrachloroethane U 0.385 1.00 1 04/01/2017 18:15 WG964562
1,1,2,2-Tetrachloroethane U 0.130 1.00 1 04/01/2017 18:15 WG964562
Tetrachloroethene U 0.372 1.00 1 04/01/2017 18:15 WG964562
Toluene U 0.412 1.00 1 04/01/2017 18:15 WG964562
1,2,3-Trichlorobenzene U 0.230 1.00 1 04/01/2017 18:15 WG964562
1,2,4-Trichlorobenzene U 0.355 1.00 1 04/01/2017 18:15 WG964562
1,1,1-Trichloroethane U 0.319 1.00 1 04/01/2017 18:15 WG964562
1,1,2-Trichloroethane U 0.383 1.00 1 04/01/2017 18:15 WG964562
Trichloroethene U 0.398 1.00 1 04/01/2017 18:15 WG964562
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 09
L898293
TRIPBLANK
Collected date/time: 03/24/17 00:00
Volatile Organic Compounds (GC/MS) by Method 6200B-1997
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Trichlorofluoromethane U 1.20 5.00 1 04/01/2017 18:15 WG964562
1,2,3-Trichloropropane U 0.807 2.50 1 04/01/2017 18:15 WG964562
1,2,4-Trimethylbenzene U 0.373 1.00 1 04/01/2017 18:15 WG964562
1,3,5-Trimethylbenzene U 0.387 1.00 1 04/01/2017 18:15 WG964562
Vinyl chloride U J3 0.259 1.00 1 04/01/2017 18:15 WG964562
o-Xylene U 0.341 1.00 1 04/01/2017 18:15 WG964562
m&p-Xylenes U 0.719 2.00 1 04/01/2017 18:15 WG964562
(S) Toluene-d8 104 80.0-120 04/01/2017 18:15 WG964562
(S) Dibromofluoromethane 109 76.0-123 04/01/2017 18:15 WG964562
(S) a,a,a-Trifluorotoluene 101 80.0-120 04/01/2017 18:15 WG964562
(S) 4-Bromofluorobenzene 100 80.0-120 04/01/2017 18:15 WG964562
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 10
L898293
B-1
Collected date/time: 03/24/17 11:15
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 84.3 1 03/30/2017 10:49 WG965406
Volatile Petroleum Hydrocarbons by Method MADEPV
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Unadjusted C5-C8 Aliphatics 4.38 J 2.19 6.58 55.5 03/31/2017 01:38 WG965869
Unadjusted C9-C12 Aliphatics U 2.19 6.58 55.5 03/31/2017 01:38 WG965869
Unadjusted C9-C10 Aromatics 2.62 J 2.19 6.58 55.5 03/31/2017 01:38 WG965869
Total VPH 7.01 2.19 6.58 55.5 03/31/2017 01:38 WG965869
(S) 2,5-Dibromotoluene(FID)96.0 70.0-130 03/31/2017 01:38 WG965869
(S) 2,5-Dibromotoluene(PID)83.8 70.0-130 03/31/2017 01:38 WG965869
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone 0.0229 J 0.0119 0.0593 1 03/31/2017 11:56 WG965859
Acrylonitrile U 0.00212 0.0119 1 03/31/2017 11:56 WG965859
Benzene U 0.000320 0.00119 1 03/31/2017 11:56 WG965859
Bromobenzene U 0.000337 0.00119 1 03/31/2017 11:56 WG965859
Bromodichloromethane U 0.000301 0.00119 1 03/31/2017 11:56 WG965859
Bromoform U 0.000503 0.00119 1 03/31/2017 11:56 WG965859
Bromomethane U 0.00159 0.00593 1 03/31/2017 11:56 WG965859
n-Butylbenzene 0.000544 J 0.000306 0.00119 1 03/31/2017 11:56 WG965859
sec-Butylbenzene U 0.000238 0.00119 1 03/31/2017 11:56 WG965859
tert-Butylbenzene U 0.000244 0.00119 1 03/31/2017 11:56 WG965859
Carbon tetrachloride U 0.000389 0.00119 1 03/31/2017 11:56 WG965859
Chlorobenzene U 0.000251 0.00119 1 03/31/2017 11:56 WG965859
Chlorodibromomethane U 0.000442 0.00119 1 03/31/2017 11:56 WG965859
Chloroethane U 0.00112 0.00593 1 03/31/2017 11:56 WG965859
2-Chloroethyl vinyl ether U 0.00278 0.0593 1 03/31/2017 11:56 WG965859
Chloroform U 0.000272 0.00593 1 03/31/2017 11:56 WG965859
Chloromethane U 0.000445 0.00297 1 03/31/2017 11:56 WG965859
2-Chlorotoluene U 0.000357 0.00119 1 03/31/2017 11:56 WG965859
4-Chlorotoluene U 0.000285 0.00119 1 03/31/2017 11:56 WG965859
1,2-Dibromo-3-Chloropropane U J4 0.00125 0.00593 1 03/31/2017 11:56 WG965859
1,2-Dibromoethane U 0.000407 0.00119 1 03/31/2017 11:56 WG965859
Dibromomethane U 0.000453 0.00119 1 03/31/2017 11:56 WG965859
1,2-Dichlorobenzene U 0.000362 0.00119 1 03/31/2017 11:56 WG965859
1,3-Dichlorobenzene U 0.000283 0.00119 1 03/31/2017 11:56 WG965859
1,4-Dichlorobenzene U 0.000268 0.00119 1 03/31/2017 11:56 WG965859
Dichlorodifluoromethane U 0.000846 0.00593 1 03/31/2017 11:56 WG965859
1,1-Dichloroethane U 0.000236 0.00119 1 03/31/2017 11:56 WG965859
1,2-Dichloroethane U 0.000314 0.00119 1 03/31/2017 11:56 WG965859
1,1-Dichloroethene U 0.000359 0.00119 1 03/31/2017 11:56 WG965859
cis-1,2-Dichloroethene U 0.000279 0.00119 1 03/31/2017 11:56 WG965859
trans-1,2-Dichloroethene U 0.000313 0.00119 1 03/31/2017 11:56 WG965859
1,2-Dichloropropane U 0.000425 0.00119 1 03/31/2017 11:56 WG965859
1,1-Dichloropropene U 0.000376 0.00119 1 03/31/2017 11:56 WG965859
1,3-Dichloropropane U 0.000246 0.00119 1 03/31/2017 11:56 WG965859
cis-1,3-Dichloropropene U 0.000311 0.00119 1 03/31/2017 11:56 WG965859
trans-1,3-Dichloropropene U 0.000317 0.00119 1 03/31/2017 11:56 WG965859
2,2-Dichloropropane U 0.000331 0.00119 1 03/31/2017 11:56 WG965859
Di-isopropyl ether U 0.000294 0.00119 1 03/31/2017 11:56 WG965859
Ethylbenzene 0.00143 0.000352 0.00119 1 03/31/2017 11:56 WG965859
Hexachloro-1,3-butadiene U 0.000406 0.00119 1 03/31/2017 11:56 WG965859
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 10
L898293
B-1
Collected date/time: 03/24/17 11:15
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Isopropylbenzene U 0.000288 0.00119 1 03/31/2017 11:56 WG965859
p-Isopropyltoluene U 0.000242 0.00119 1 03/31/2017 11:56 WG965859
2-Butanone (MEK)U J3 0.00555 0.0119 1 03/31/2017 11:56 WG965859
Methylene Chloride U 0.00119 0.00593 1 03/31/2017 11:56 WG965859
4-Methyl-2-pentanone (MIBK)U J3 J4 0.00223 0.0119 1 03/31/2017 11:56 WG965859
Methyl tert-butyl ether U 0.000251 0.00119 1 03/31/2017 11:56 WG965859
Naphthalene 0.00712 0.00119 0.00593 1 03/31/2017 11:56 WG965859
n-Propylbenzene 0.00113 J 0.000244 0.00119 1 03/31/2017 11:56 WG965859
Styrene U 0.000278 0.00119 1 03/31/2017 11:56 WG965859
1,1,1,2-Tetrachloroethane U 0.000313 0.00119 1 03/31/2017 11:56 WG965859
1,1,2,2-Tetrachloroethane U 0.000433 0.00119 1 03/31/2017 11:56 WG965859
Tetrachloroethene U 0.000327 0.00119 1 03/31/2017 11:56 WG965859
Toluene 0.000788 B J 0.000515 0.00593 1 03/31/2017 11:56 WG965859
1,2,3-Trichlorobenzene U 0.000363 0.00119 1 03/31/2017 11:56 WG965859
1,2,4-Trichlorobenzene U 0.000460 0.00119 1 03/31/2017 11:56 WG965859
1,1,1-Trichloroethane U 0.000339 0.00119 1 03/31/2017 11:56 WG965859
1,1,2-Trichloroethane U 0.000329 0.00119 1 03/31/2017 11:56 WG965859
Trichloroethene U 0.000331 0.00119 1 03/31/2017 11:56 WG965859
Trichlorofluoromethane U 0.000453 0.00593 1 03/31/2017 11:56 WG965859
1,2,3-Trichloropropane U 0.000879 0.00297 1 03/31/2017 11:56 WG965859
1,2,4-Trimethylbenzene 0.0148 0.000250 0.00119 1 03/31/2017 11:56 WG965859
1,3,5-Trimethylbenzene 0.00389 0.000316 0.00119 1 03/31/2017 11:56 WG965859
Vinyl chloride U 0.000345 0.00119 1 03/31/2017 11:56 WG965859
Xylenes, Total 0.0158 0.000828 0.00356 1 03/31/2017 11:56 WG965859
(S) Toluene-d8 97.5 80.0-120 03/31/2017 11:56 WG965859
(S) Dibromofluoromethane 95.9 74.0-131 03/31/2017 11:56 WG965859
(S) 4-Bromofluorobenzene 95.2 64.0-132 03/31/2017 11:56 WG965859
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00761 0.0391 1 03/30/2017 15:09 WG965361
Acenaphthylene U 0.00796 0.0391 1 03/30/2017 15:09 WG965361
Anthracene U 0.00750 0.0391 1 03/30/2017 15:09 WG965361
Atrazine U 0.111 0.395 1 03/30/2017 15:09 WG965361
Benzaldehyde U 0.0631 0.395 1 03/30/2017 15:09 WG965361
Benzo(a)anthracene U 0.00508 0.0391 1 03/30/2017 15:09 WG965361
Benzo(b)fluoranthene U 0.00824 0.0391 1 03/30/2017 15:09 WG965361
Benzo(k)fluoranthene U 0.00690 0.0391 1 03/30/2017 15:09 WG965361
Benzo(g,h,i)perylene U J3 0.00855 0.0391 1 03/30/2017 15:09 WG965361
Benzo(a)pyrene U 0.00650 0.0391 1 03/30/2017 15:09 WG965361
Biphenyl U 0.00697 0.395 1 03/30/2017 15:09 WG965361
Bis(2-chlorethoxy)methane U 0.00913 0.395 1 03/30/2017 15:09 WG965361
Bis(2-chloroethyl)ether U 0.0106 0.395 1 03/30/2017 15:09 WG965361
Bis(2-chloroisopropyl)ether U 0.00901 0.395 1 03/30/2017 15:09 WG965361
4-Bromophenyl-phenylether U 0.0135 0.395 1 03/30/2017 15:09 WG965361
Caprolactam U 0.123 0.395 1 03/30/2017 15:09 WG965361
Carbazole U 0.00622 0.395 1 03/30/2017 15:09 WG965361
2-Chloronaphthalene U 0.00758 0.0391 1 03/30/2017 15:09 WG965361
4-Chlorophenyl-phenylether U 0.00744 0.395 1 03/30/2017 15:09 WG965361
Chrysene U 0.00658 0.0391 1 03/30/2017 15:09 WG965361
Dibenz(a,h)anthracene U 0.00974 0.0391 1 03/30/2017 15:09 WG965361
3,3-Dichlorobenzidine U 0.0942 0.395 1 03/30/2017 15:09 WG965361
2,4-Dinitrotoluene U 0.00720 0.395 1 03/30/2017 15:09 WG965361
2,6-Dinitrotoluene U 0.00874 0.395 1 03/30/2017 15:09 WG965361
Fluoranthene U 0.00588 0.0391 1 03/30/2017 15:09 WG965361
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 10
L898293
B-1
Collected date/time: 03/24/17 11:15
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Fluorene U 0.00809 0.0391 1 03/30/2017 15:09 WG965361
Hexachlorobenzene U 0.0102 0.395 1 03/30/2017 15:09 WG965361
Hexachloro-1,3-butadiene U 0.0119 0.395 1 03/30/2017 15:09 WG965361
Hexachlorocyclopentadiene U 0.0696 0.395 1 03/30/2017 15:09 WG965361
Hexachloroethane U 0.0159 0.395 1 03/30/2017 15:09 WG965361
Indeno(1,2,3-cd)pyrene U J3 0.00916 0.0391 1 03/30/2017 15:09 WG965361
Isophorone U 0.00619 0.395 1 03/30/2017 15:09 WG965361
Naphthalene U 0.0105 0.0391 1 03/30/2017 15:09 WG965361
Nitrobenzene U 0.00824 0.395 1 03/30/2017 15:09 WG965361
n-Nitrosodiphenylamine U 0.00705 0.395 1 03/30/2017 15:09 WG965361
n-Nitrosodi-n-propylamine U 0.0107 0.395 1 03/30/2017 15:09 WG965361
Phenanthrene U 0.00626 0.0391 1 03/30/2017 15:09 WG965361
Benzylbutyl phthalate U 0.0122 0.395 1 03/30/2017 15:09 WG965361
Bis(2-ethylhexyl)phthalate U 0.0142 0.395 1 03/30/2017 15:09 WG965361
Di-n-butyl phthalate U 0.0129 0.395 1 03/30/2017 15:09 WG965361
Diethyl phthalate U 0.00820 0.395 1 03/30/2017 15:09 WG965361
Dimethyl phthalate U 0.00641 0.395 1 03/30/2017 15:09 WG965361
Di-n-octyl phthalate U 0.0108 0.395 1 03/30/2017 15:09 WG965361
Pyrene U 0.0146 0.0391 1 03/30/2017 15:09 WG965361
4-Chloroaniline U 0.0418 0.395 1 03/30/2017 15:09 WG965361
4-Chloro-3-methylphenol U 0.00566 0.395 1 03/30/2017 15:09 WG965361
2-Chlorophenol U 0.00986 0.395 1 03/30/2017 15:09 WG965361
Dibenzofuran U 0.00614 0.395 1 03/30/2017 15:09 WG965361
2,4-Dichlorophenol U 0.00885 0.395 1 03/30/2017 15:09 WG965361
2,4-Dimethylphenol U 0.0559 0.395 1 03/30/2017 15:09 WG965361
4,6-Dinitro-2-methylphenol U 0.147 0.395 1 03/30/2017 15:09 WG965361
2,4-Dinitrophenol U 0.116 0.395 1 03/30/2017 15:09 WG965361
2-Methylnaphthalene U 0.0102 0.0391 1 03/30/2017 15:09 WG965361
2-Methylphenol U 0.0117 0.395 1 03/30/2017 15:09 WG965361
3&4-Methyl Phenol U 0.00929 0.395 1 03/30/2017 15:09 WG965361
2-Nitroaniline U 0.00896 0.395 1 03/30/2017 15:09 WG965361
3-Nitroaniline U 0.0101 0.395 1 03/30/2017 15:09 WG965361
4-Nitroaniline U 0.00758 0.395 1 03/30/2017 15:09 WG965361
2-Nitrophenol U 0.0154 0.395 1 03/30/2017 15:09 WG965361
4-Nitrophenol U 0.0623 0.395 1 03/30/2017 15:09 WG965361
Pentachlorophenol U 0.0569 0.395 1 03/30/2017 15:09 WG965361
Phenol U 0.00824 0.395 1 03/30/2017 15:09 WG965361
2,4,6-Trichlorophenol U 0.00924 0.395 1 03/30/2017 15:09 WG965361
Acetophenone U 0.0892 0.395 1 03/30/2017 15:09 WG965361
1,2,4,5-Tetrachlorobenzene U 0.0904 0.395 1 03/30/2017 15:09 WG965361
2,4,5-Trichlorophenol U 0.0123 0.395 1 03/30/2017 15:09 WG965361
2,3,4,6-Tetrachlorophenol U 0.144 0.395 1 03/30/2017 15:09 WG965361
(S) 2-Fluorophenol 56.5 20.0-120 03/30/2017 15:09 WG965361
(S) Phenol-d5 56.5 20.0-120 03/30/2017 15:09 WG965361
(S) Nitrobenzene-d5 55.7 18.0-125 03/30/2017 15:09 WG965361
(S) 2-Fluorobiphenyl 67.6 28.0-120 03/30/2017 15:09 WG965361
(S) 2,4,6-Tribromophenol 73.5 17.0-137 03/30/2017 15:09 WG965361
(S) p-Terphenyl-d14 83.2 13.0-131 03/30/2017 15:09 WG965361
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 11
L898293
B-2
Collected date/time: 03/24/17 12:18
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 86.5 1 03/30/2017 15:02 WG965706
Volatile Petroleum Hydrocarbons by Method MADEPV
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Unadjusted C5-C8 Aliphatics U 2.17 6.53 56.5 03/31/2017 02:10 WG965869
Unadjusted C9-C12 Aliphatics U 2.17 6.53 56.5 03/31/2017 02:10 WG965869
Unadjusted C9-C10 Aromatics U 2.17 6.53 56.5 03/31/2017 02:10 WG965869
Total VPH U 2.17 6.53 56.5 03/31/2017 02:10 WG965869
(S) 2,5-Dibromotoluene(FID)95.2 70.0-130 03/31/2017 02:10 WG965869
(S) 2,5-Dibromotoluene(PID)82.5 70.0-130 03/31/2017 02:10 WG965869
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone 0.0397 J 0.0116 0.0578 1 03/31/2017 12:16 WG965859
Acrylonitrile U 0.00207 0.0116 1 03/31/2017 12:16 WG965859
Benzene U 0.000312 0.00116 1 03/31/2017 12:16 WG965859
Bromobenzene U 0.000328 0.00116 1 03/31/2017 12:16 WG965859
Bromodichloromethane U 0.000294 0.00116 1 03/31/2017 12:16 WG965859
Bromoform U 0.000490 0.00116 1 03/31/2017 12:16 WG965859
Bromomethane U 0.00155 0.00578 1 03/31/2017 12:16 WG965859
n-Butylbenzene U 0.000298 0.00116 1 03/31/2017 12:16 WG965859
sec-Butylbenzene U 0.000232 0.00116 1 03/31/2017 12:16 WG965859
tert-Butylbenzene U 0.000238 0.00116 1 03/31/2017 12:16 WG965859
Carbon tetrachloride U 0.000379 0.00116 1 03/31/2017 12:16 WG965859
Chlorobenzene U 0.000245 0.00116 1 03/31/2017 12:16 WG965859
Chlorodibromomethane U 0.000431 0.00116 1 03/31/2017 12:16 WG965859
Chloroethane U 0.00109 0.00578 1 03/31/2017 12:16 WG965859
2-Chloroethyl vinyl ether U 0.00271 0.0578 1 03/31/2017 12:16 WG965859
Chloroform U 0.000265 0.00578 1 03/31/2017 12:16 WG965859
Chloromethane U 0.000434 0.00289 1 03/31/2017 12:16 WG965859
2-Chlorotoluene U 0.000348 0.00116 1 03/31/2017 12:16 WG965859
4-Chlorotoluene U 0.000277 0.00116 1 03/31/2017 12:16 WG965859
1,2-Dibromo-3-Chloropropane U J4 0.00121 0.00578 1 03/31/2017 12:16 WG965859
1,2-Dibromoethane U 0.000397 0.00116 1 03/31/2017 12:16 WG965859
Dibromomethane U 0.000442 0.00116 1 03/31/2017 12:16 WG965859
1,2-Dichlorobenzene U 0.000353 0.00116 1 03/31/2017 12:16 WG965859
1,3-Dichlorobenzene U 0.000276 0.00116 1 03/31/2017 12:16 WG965859
1,4-Dichlorobenzene U 0.000261 0.00116 1 03/31/2017 12:16 WG965859
Dichlorodifluoromethane U 0.000824 0.00578 1 03/31/2017 12:16 WG965859
1,1-Dichloroethane U 0.000230 0.00116 1 03/31/2017 12:16 WG965859
1,2-Dichloroethane U 0.000306 0.00116 1 03/31/2017 12:16 WG965859
1,1-Dichloroethene U 0.000350 0.00116 1 03/31/2017 12:16 WG965859
cis-1,2-Dichloroethene U 0.000272 0.00116 1 03/31/2017 12:16 WG965859
trans-1,2-Dichloroethene U 0.000305 0.00116 1 03/31/2017 12:16 WG965859
1,2-Dichloropropane U 0.000414 0.00116 1 03/31/2017 12:16 WG965859
1,1-Dichloropropene U 0.000367 0.00116 1 03/31/2017 12:16 WG965859
1,3-Dichloropropane U 0.000239 0.00116 1 03/31/2017 12:16 WG965859
cis-1,3-Dichloropropene U 0.000303 0.00116 1 03/31/2017 12:16 WG965859
trans-1,3-Dichloropropene U 0.000309 0.00116 1 03/31/2017 12:16 WG965859
2,2-Dichloropropane U 0.000323 0.00116 1 03/31/2017 12:16 WG965859
Di-isopropyl ether U 0.000287 0.00116 1 03/31/2017 12:16 WG965859
Ethylbenzene U 0.000343 0.00116 1 03/31/2017 12:16 WG965859
Hexachloro-1,3-butadiene U 0.000395 0.00116 1 03/31/2017 12:16 WG965859
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 11
L898293
B-2
Collected date/time: 03/24/17 12:18
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Isopropylbenzene U 0.000281 0.00116 1 03/31/2017 12:16 WG965859
p-Isopropyltoluene U 0.000236 0.00116 1 03/31/2017 12:16 WG965859
2-Butanone (MEK)0.00996 J J3 0.00541 0.0116 1 03/31/2017 12:16 WG965859
Methylene Chloride U 0.00116 0.00578 1 03/31/2017 12:16 WG965859
4-Methyl-2-pentanone (MIBK)U J3 J4 0.00217 0.0116 1 03/31/2017 12:16 WG965859
Methyl tert-butyl ether U 0.000245 0.00116 1 03/31/2017 12:16 WG965859
Naphthalene U 0.00116 0.00578 1 03/31/2017 12:16 WG965859
n-Propylbenzene U 0.000238 0.00116 1 03/31/2017 12:16 WG965859
Styrene U 0.000271 0.00116 1 03/31/2017 12:16 WG965859
1,1,1,2-Tetrachloroethane U 0.000305 0.00116 1 03/31/2017 12:16 WG965859
1,1,2,2-Tetrachloroethane U 0.000422 0.00116 1 03/31/2017 12:16 WG965859
Tetrachloroethene U 0.000319 0.00116 1 03/31/2017 12:16 WG965859
Toluene U 0.000502 0.00578 1 03/31/2017 12:16 WG965859
1,2,3-Trichlorobenzene U 0.000354 0.00116 1 03/31/2017 12:16 WG965859
1,2,4-Trichlorobenzene U 0.000449 0.00116 1 03/31/2017 12:16 WG965859
1,1,1-Trichloroethane U 0.000331 0.00116 1 03/31/2017 12:16 WG965859
1,1,2-Trichloroethane U 0.000320 0.00116 1 03/31/2017 12:16 WG965859
Trichloroethene U 0.000323 0.00116 1 03/31/2017 12:16 WG965859
Trichlorofluoromethane U 0.000442 0.00578 1 03/31/2017 12:16 WG965859
1,2,3-Trichloropropane U 0.000857 0.00289 1 03/31/2017 12:16 WG965859
1,2,4-Trimethylbenzene U 0.000244 0.00116 1 03/31/2017 12:16 WG965859
1,3,5-Trimethylbenzene U 0.000308 0.00116 1 03/31/2017 12:16 WG965859
Vinyl chloride U 0.000336 0.00116 1 03/31/2017 12:16 WG965859
Xylenes, Total U 0.000807 0.00347 1 03/31/2017 12:16 WG965859
(S) Toluene-d8 97.4 80.0-120 03/31/2017 12:16 WG965859
(S) Dibromofluoromethane 94.6 74.0-131 03/31/2017 12:16 WG965859
(S) 4-Bromofluorobenzene 93.9 64.0-132 03/31/2017 12:16 WG965859
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00742 0.0382 1 03/30/2017 18:03 WG965361
Acenaphthylene U 0.00776 0.0382 1 03/30/2017 18:03 WG965361
Anthracene U 0.00731 0.0382 1 03/30/2017 18:03 WG965361
Atrazine U 0.108 0.385 1 03/30/2017 18:03 WG965361
Benzaldehyde U 0.0615 0.385 1 03/30/2017 18:03 WG965361
Benzo(a)anthracene U 0.00495 0.0382 1 03/30/2017 18:03 WG965361
Benzo(b)fluoranthene U 0.00804 0.0382 1 03/30/2017 18:03 WG965361
Benzo(k)fluoranthene U 0.00673 0.0382 1 03/30/2017 18:03 WG965361
Benzo(g,h,i)perylene U J3 0.00834 0.0382 1 03/30/2017 18:03 WG965361
Benzo(a)pyrene U 0.00634 0.0382 1 03/30/2017 18:03 WG965361
Biphenyl U 0.00680 0.385 1 03/30/2017 18:03 WG965361
Bis(2-chlorethoxy)methane U 0.00890 0.385 1 03/30/2017 18:03 WG965361
Bis(2-chloroethyl)ether U 0.0104 0.385 1 03/30/2017 18:03 WG965361
Bis(2-chloroisopropyl)ether U 0.00879 0.385 1 03/30/2017 18:03 WG965361
4-Bromophenyl-phenylether U 0.0132 0.385 1 03/30/2017 18:03 WG965361
Caprolactam U 0.120 0.385 1 03/30/2017 18:03 WG965361
Carbazole U 0.00606 0.385 1 03/30/2017 18:03 WG965361
2-Chloronaphthalene U 0.00739 0.0382 1 03/30/2017 18:03 WG965361
4-Chlorophenyl-phenylether U 0.00725 0.385 1 03/30/2017 18:03 WG965361
Chrysene U 0.00642 0.0382 1 03/30/2017 18:03 WG965361
Dibenz(a,h)anthracene U 0.00949 0.0382 1 03/30/2017 18:03 WG965361
3,3-Dichlorobenzidine U 0.0918 0.385 1 03/30/2017 18:03 WG965361
2,4-Dinitrotoluene U 0.00702 0.385 1 03/30/2017 18:03 WG965361
2,6-Dinitrotoluene U 0.00852 0.385 1 03/30/2017 18:03 WG965361
Fluoranthene U 0.00573 0.0382 1 03/30/2017 18:03 WG965361
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 11
L898293
B-2
Collected date/time: 03/24/17 12:18
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Fluorene U 0.00789 0.0382 1 03/30/2017 18:03 WG965361
Hexachlorobenzene U 0.00990 0.385 1 03/30/2017 18:03 WG965361
Hexachloro-1,3-butadiene U 0.0116 0.385 1 03/30/2017 18:03 WG965361
Hexachlorocyclopentadiene U 0.0679 0.385 1 03/30/2017 18:03 WG965361
Hexachloroethane U 0.0155 0.385 1 03/30/2017 18:03 WG965361
Indeno(1,2,3-cd)pyrene U J3 0.00893 0.0382 1 03/30/2017 18:03 WG965361
Isophorone U 0.00604 0.385 1 03/30/2017 18:03 WG965361
Naphthalene U 0.0103 0.0382 1 03/30/2017 18:03 WG965361
Nitrobenzene U 0.00804 0.385 1 03/30/2017 18:03 WG965361
n-Nitrosodiphenylamine U 0.00687 0.385 1 03/30/2017 18:03 WG965361
n-Nitrosodi-n-propylamine U 0.0105 0.385 1 03/30/2017 18:03 WG965361
Phenanthrene U 0.00610 0.0382 1 03/30/2017 18:03 WG965361
Benzylbutyl phthalate U 0.0119 0.385 1 03/30/2017 18:03 WG965361
Bis(2-ethylhexyl)phthalate U 0.0139 0.385 1 03/30/2017 18:03 WG965361
Di-n-butyl phthalate U 0.0126 0.385 1 03/30/2017 18:03 WG965361
Diethyl phthalate U 0.00799 0.385 1 03/30/2017 18:03 WG965361
Dimethyl phthalate U 0.00624 0.385 1 03/30/2017 18:03 WG965361
Di-n-octyl phthalate U 0.0105 0.385 1 03/30/2017 18:03 WG965361
Pyrene U 0.0142 0.0382 1 03/30/2017 18:03 WG965361
4-Chloroaniline U 0.0407 0.385 1 03/30/2017 18:03 WG965361
4-Chloro-3-methylphenol U 0.00552 0.385 1 03/30/2017 18:03 WG965361
2-Chlorophenol U 0.00961 0.385 1 03/30/2017 18:03 WG965361
Dibenzofuran U 0.00599 0.385 1 03/30/2017 18:03 WG965361
2,4-Dichlorophenol U 0.00863 0.385 1 03/30/2017 18:03 WG965361
2,4-Dimethylphenol U 0.0545 0.385 1 03/30/2017 18:03 WG965361
4,6-Dinitro-2-methylphenol U 0.143 0.385 1 03/30/2017 18:03 WG965361
2,4-Dinitrophenol U 0.113 0.385 1 03/30/2017 18:03 WG965361
2-Methylnaphthalene U 0.00996 0.0382 1 03/30/2017 18:03 WG965361
2-Methylphenol U 0.0114 0.385 1 03/30/2017 18:03 WG965361
3&4-Methyl Phenol U 0.00905 0.385 1 03/30/2017 18:03 WG965361
2-Nitroaniline U 0.00873 0.385 1 03/30/2017 18:03 WG965361
3-Nitroaniline U 0.00983 0.385 1 03/30/2017 18:03 WG965361
4-Nitroaniline U 0.00739 0.385 1 03/30/2017 18:03 WG965361
2-Nitrophenol U 0.0150 0.385 1 03/30/2017 18:03 WG965361
4-Nitrophenol U 0.0607 0.385 1 03/30/2017 18:03 WG965361
Pentachlorophenol U 0.0555 0.385 1 03/30/2017 18:03 WG965361
Phenol U 0.00804 0.385 1 03/30/2017 18:03 WG965361
2,4,6-Trichlorophenol U 0.00901 0.385 1 03/30/2017 18:03 WG965361
Acetophenone U 0.0869 0.385 1 03/30/2017 18:03 WG965361
1,2,4,5-Tetrachlorobenzene U 0.0881 0.385 1 03/30/2017 18:03 WG965361
2,4,5-Trichlorophenol U 0.0120 0.385 1 03/30/2017 18:03 WG965361
2,3,4,6-Tetrachlorophenol U 0.140 0.385 1 03/30/2017 18:03 WG965361
(S) 2-Fluorophenol 64.0 20.0-120 03/30/2017 18:03 WG965361
(S) Phenol-d5 66.6 20.0-120 03/30/2017 18:03 WG965361
(S) Nitrobenzene-d5 64.8 18.0-125 03/30/2017 18:03 WG965361
(S) 2-Fluorobiphenyl 81.2 28.0-120 03/30/2017 18:03 WG965361
(S) 2,4,6-Tribromophenol 88.6 17.0-137 03/30/2017 18:03 WG965361
(S) p-Terphenyl-d14 84.4 13.0-131 03/30/2017 18:03 WG965361
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 12
L898293
B-3
Collected date/time: 03/24/17 11:48
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 87.5 1 03/30/2017 15:02 WG965706
Volatile Petroleum Hydrocarbons by Method MADEPV
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Unadjusted C5-C8 Aliphatics 1.91 J 1.90 5.71 50 03/31/2017 02:43 WG965869
Unadjusted C9-C12 Aliphatics 2.99 J 1.90 5.71 50 03/31/2017 02:43 WG965869
Unadjusted C9-C10 Aromatics U 1.90 5.71 50 03/31/2017 02:43 WG965869
Total VPH 4.90 J 1.90 5.71 50 03/31/2017 02:43 WG965869
(S) 2,5-Dibromotoluene(FID)97.8 70.0-130 03/31/2017 02:43 WG965869
(S) 2,5-Dibromotoluene(PID)84.3 70.0-130 03/31/2017 02:43 WG965869
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone 0.0500 J 0.0114 0.0571 1 03/31/2017 12:39 WG965859
Acrylonitrile U 0.00205 0.0114 1 03/31/2017 12:39 WG965859
Benzene 0.00892 0.000309 0.00114 1 03/31/2017 12:39 WG965859
Bromobenzene U 0.000325 0.00114 1 03/31/2017 12:39 WG965859
Bromodichloromethane U 0.000290 0.00114 1 03/31/2017 12:39 WG965859
Bromoform U 0.000485 0.00114 1 03/31/2017 12:39 WG965859
Bromomethane U 0.00153 0.00571 1 03/31/2017 12:39 WG965859
n-Butylbenzene 0.000364 J 0.000295 0.00114 1 03/31/2017 12:39 WG965859
sec-Butylbenzene U 0.000230 0.00114 1 03/31/2017 12:39 WG965859
tert-Butylbenzene U 0.000235 0.00114 1 03/31/2017 12:39 WG965859
Carbon tetrachloride U 0.000375 0.00114 1 03/31/2017 12:39 WG965859
Chlorobenzene U 0.000242 0.00114 1 03/31/2017 12:39 WG965859
Chlorodibromomethane U 0.000426 0.00114 1 03/31/2017 12:39 WG965859
Chloroethane U 0.00108 0.00571 1 03/31/2017 12:39 WG965859
2-Chloroethyl vinyl ether U 0.00267 0.0571 1 03/31/2017 12:39 WG965859
Chloroform U 0.000262 0.00571 1 03/31/2017 12:39 WG965859
Chloromethane U 0.000429 0.00286 1 03/31/2017 12:39 WG965859
2-Chlorotoluene U 0.000344 0.00114 1 03/31/2017 12:39 WG965859
4-Chlorotoluene U 0.000274 0.00114 1 03/31/2017 12:39 WG965859
1,2-Dibromo-3-Chloropropane U J4 0.00120 0.00571 1 03/31/2017 12:39 WG965859
1,2-Dibromoethane U 0.000392 0.00114 1 03/31/2017 12:39 WG965859
Dibromomethane U 0.000437 0.00114 1 03/31/2017 12:39 WG965859
1,2-Dichlorobenzene U 0.000349 0.00114 1 03/31/2017 12:39 WG965859
1,3-Dichlorobenzene U 0.000273 0.00114 1 03/31/2017 12:39 WG965859
1,4-Dichlorobenzene U 0.000258 0.00114 1 03/31/2017 12:39 WG965859
Dichlorodifluoromethane U 0.000815 0.00571 1 03/31/2017 12:39 WG965859
1,1-Dichloroethane U 0.000227 0.00114 1 03/31/2017 12:39 WG965859
1,2-Dichloroethane U 0.000303 0.00114 1 03/31/2017 12:39 WG965859
1,1-Dichloroethene U 0.000346 0.00114 1 03/31/2017 12:39 WG965859
cis-1,2-Dichloroethene U 0.000269 0.00114 1 03/31/2017 12:39 WG965859
trans-1,2-Dichloroethene U 0.000302 0.00114 1 03/31/2017 12:39 WG965859
1,2-Dichloropropane U 0.000409 0.00114 1 03/31/2017 12:39 WG965859
1,1-Dichloropropene U 0.000362 0.00114 1 03/31/2017 12:39 WG965859
1,3-Dichloropropane U 0.000237 0.00114 1 03/31/2017 12:39 WG965859
cis-1,3-Dichloropropene U 0.000299 0.00114 1 03/31/2017 12:39 WG965859
trans-1,3-Dichloropropene U 0.000305 0.00114 1 03/31/2017 12:39 WG965859
2,2-Dichloropropane U 0.000319 0.00114 1 03/31/2017 12:39 WG965859
Di-isopropyl ether U 0.000283 0.00114 1 03/31/2017 12:39 WG965859
Ethylbenzene 0.00335 0.000339 0.00114 1 03/31/2017 12:39 WG965859
Hexachloro-1,3-butadiene U 0.000391 0.00114 1 03/31/2017 12:39 WG965859
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 12
L898293
B-3
Collected date/time: 03/24/17 11:48
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Isopropylbenzene U 0.000278 0.00114 1 03/31/2017 12:39 WG965859
p-Isopropyltoluene U 0.000233 0.00114 1 03/31/2017 12:39 WG965859
2-Butanone (MEK)0.00646 J J3 0.00535 0.0114 1 03/31/2017 12:39 WG965859
Methylene Chloride U 0.00114 0.00571 1 03/31/2017 12:39 WG965859
4-Methyl-2-pentanone (MIBK)U J3 J4 0.00215 0.0114 1 03/31/2017 12:39 WG965859
Methyl tert-butyl ether 0.000418 J 0.000242 0.00114 1 03/31/2017 12:39 WG965859
Naphthalene 0.00296 J 0.00114 0.00571 1 03/31/2017 12:39 WG965859
n-Propylbenzene 0.00134 0.000235 0.00114 1 03/31/2017 12:39 WG965859
Styrene U 0.000267 0.00114 1 03/31/2017 12:39 WG965859
1,1,1,2-Tetrachloroethane U 0.000302 0.00114 1 03/31/2017 12:39 WG965859
1,1,2,2-Tetrachloroethane U 0.000417 0.00114 1 03/31/2017 12:39 WG965859
Tetrachloroethene U 0.000315 0.00114 1 03/31/2017 12:39 WG965859
Toluene 0.00170 B J 0.000496 0.00571 1 03/31/2017 12:39 WG965859
1,2,3-Trichlorobenzene U 0.000350 0.00114 1 03/31/2017 12:39 WG965859
1,2,4-Trichlorobenzene U 0.000443 0.00114 1 03/31/2017 12:39 WG965859
1,1,1-Trichloroethane U 0.000327 0.00114 1 03/31/2017 12:39 WG965859
1,1,2-Trichloroethane U 0.000317 0.00114 1 03/31/2017 12:39 WG965859
Trichloroethene U 0.000319 0.00114 1 03/31/2017 12:39 WG965859
Trichlorofluoromethane U 0.000437 0.00571 1 03/31/2017 12:39 WG965859
1,2,3-Trichloropropane U 0.000847 0.00286 1 03/31/2017 12:39 WG965859
1,2,4-Trimethylbenzene 0.0106 0.000241 0.00114 1 03/31/2017 12:39 WG965859
1,3,5-Trimethylbenzene 0.00316 0.000304 0.00114 1 03/31/2017 12:39 WG965859
Vinyl chloride U 0.000333 0.00114 1 03/31/2017 12:39 WG965859
Xylenes, Total 0.0219 0.000798 0.00343 1 03/31/2017 12:39 WG965859
(S) Toluene-d8 95.5 80.0-120 03/31/2017 12:39 WG965859
(S) Dibromofluoromethane 96.0 74.0-131 03/31/2017 12:39 WG965859
(S) 4-Bromofluorobenzene 92.7 64.0-132 03/31/2017 12:39 WG965859
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene U 0.00734 0.0377 1 03/30/2017 18:28 WG965361
Acenaphthylene U 0.00767 0.0377 1 03/30/2017 18:28 WG965361
Anthracene U 0.00722 0.0377 1 03/30/2017 18:28 WG965361
Atrazine U 0.107 0.381 1 03/30/2017 18:28 WG965361
Benzaldehyde U 0.0608 0.381 1 03/30/2017 18:28 WG965361
Benzo(a)anthracene U 0.00489 0.0377 1 03/30/2017 18:28 WG965361
Benzo(b)fluoranthene U 0.00794 0.0377 1 03/30/2017 18:28 WG965361
Benzo(k)fluoranthene U 0.00665 0.0377 1 03/30/2017 18:28 WG965361
Benzo(g,h,i)perylene U J3 0.00824 0.0377 1 03/30/2017 18:28 WG965361
Benzo(a)pyrene U 0.00626 0.0377 1 03/30/2017 18:28 WG965361
Biphenyl U 0.00672 0.381 1 03/30/2017 18:28 WG965361
Bis(2-chlorethoxy)methane U 0.00880 0.381 1 03/30/2017 18:28 WG965361
Bis(2-chloroethyl)ether U 0.0102 0.381 1 03/30/2017 18:28 WG965361
Bis(2-chloroisopropyl)ether U 0.00869 0.381 1 03/30/2017 18:28 WG965361
4-Bromophenyl-phenylether U 0.0130 0.381 1 03/30/2017 18:28 WG965361
Caprolactam U 0.119 0.381 1 03/30/2017 18:28 WG965361
Carbazole U 0.00599 0.381 1 03/30/2017 18:28 WG965361
2-Chloronaphthalene U 0.00730 0.0377 1 03/30/2017 18:28 WG965361
4-Chlorophenyl-phenylether U 0.00717 0.381 1 03/30/2017 18:28 WG965361
Chrysene U 0.00634 0.0377 1 03/30/2017 18:28 WG965361
Dibenz(a,h)anthracene U 0.00938 0.0377 1 03/30/2017 18:28 WG965361
3,3-Dichlorobenzidine U 0.0908 0.381 1 03/30/2017 18:28 WG965361
2,4-Dinitrotoluene U 0.00694 0.381 1 03/30/2017 18:28 WG965361
2,6-Dinitrotoluene U 0.00842 0.381 1 03/30/2017 18:28 WG965361
Fluoranthene U 0.00567 0.0377 1 03/30/2017 18:28 WG965361
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 12
L898293
B-3
Collected date/time: 03/24/17 11:48
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Fluorene U 0.00780 0.0377 1 03/30/2017 18:28 WG965361
Hexachlorobenzene U 0.00978 0.381 1 03/30/2017 18:28 WG965361
Hexachloro-1,3-butadiene U 0.0114 0.381 1 03/30/2017 18:28 WG965361
Hexachlorocyclopentadiene U 0.0671 0.381 1 03/30/2017 18:28 WG965361
Hexachloroethane U 0.0153 0.381 1 03/30/2017 18:28 WG965361
Indeno(1,2,3-cd)pyrene U J3 0.00882 0.0377 1 03/30/2017 18:28 WG965361
Isophorone U 0.00597 0.381 1 03/30/2017 18:28 WG965361
Naphthalene 0.138 0.0102 0.0377 1 03/30/2017 18:28 WG965361
Nitrobenzene U 0.00794 0.381 1 03/30/2017 18:28 WG965361
n-Nitrosodiphenylamine U 0.00679 0.381 1 03/30/2017 18:28 WG965361
n-Nitrosodi-n-propylamine U 0.0104 0.381 1 03/30/2017 18:28 WG965361
Phenanthrene 0.00755 J 0.00604 0.0377 1 03/30/2017 18:28 WG965361
Benzylbutyl phthalate U 0.0118 0.381 1 03/30/2017 18:28 WG965361
Bis(2-ethylhexyl)phthalate U 0.0137 0.381 1 03/30/2017 18:28 WG965361
Di-n-butyl phthalate U 0.0125 0.381 1 03/30/2017 18:28 WG965361
Diethyl phthalate U 0.00790 0.381 1 03/30/2017 18:28 WG965361
Dimethyl phthalate U 0.00617 0.381 1 03/30/2017 18:28 WG965361
Di-n-octyl phthalate U 0.0104 0.381 1 03/30/2017 18:28 WG965361
Pyrene U 0.0141 0.0377 1 03/30/2017 18:28 WG965361
4-Chloroaniline U 0.0402 0.381 1 03/30/2017 18:28 WG965361
4-Chloro-3-methylphenol U 0.00545 0.381 1 03/30/2017 18:28 WG965361
2-Chlorophenol U 0.00950 0.381 1 03/30/2017 18:28 WG965361
Dibenzofuran U 0.00592 0.381 1 03/30/2017 18:28 WG965361
2,4-Dichlorophenol U 0.00853 0.381 1 03/30/2017 18:28 WG965361
2,4-Dimethylphenol U 0.0538 0.381 1 03/30/2017 18:28 WG965361
4,6-Dinitro-2-methylphenol U 0.142 0.381 1 03/30/2017 18:28 WG965361
2,4-Dinitrophenol U 0.112 0.381 1 03/30/2017 18:28 WG965361
2-Methylnaphthalene 0.111 0.00984 0.0377 1 03/30/2017 18:28 WG965361
2-Methylphenol U 0.0113 0.381 1 03/30/2017 18:28 WG965361
3&4-Methyl Phenol U 0.00895 0.381 1 03/30/2017 18:28 WG965361
2-Nitroaniline U 0.00863 0.381 1 03/30/2017 18:28 WG965361
3-Nitroaniline U 0.00972 0.381 1 03/30/2017 18:28 WG965361
4-Nitroaniline U 0.00730 0.381 1 03/30/2017 18:28 WG965361
2-Nitrophenol U 0.0149 0.381 1 03/30/2017 18:28 WG965361
4-Nitrophenol U 0.0600 0.381 1 03/30/2017 18:28 WG965361
Pentachlorophenol U 0.0549 0.381 1 03/30/2017 18:28 WG965361
Phenol U 0.00794 0.381 1 03/30/2017 18:28 WG965361
2,4,6-Trichlorophenol U 0.00890 0.381 1 03/30/2017 18:28 WG965361
Acetophenone U 0.0860 0.381 1 03/30/2017 18:28 WG965361
1,2,4,5-Tetrachlorobenzene U 0.0871 0.381 1 03/30/2017 18:28 WG965361
2,4,5-Trichlorophenol U 0.0119 0.381 1 03/30/2017 18:28 WG965361
2,3,4,6-Tetrachlorophenol U 0.138 0.381 1 03/30/2017 18:28 WG965361
(S) 2-Fluorophenol 60.1 20.0-120 03/30/2017 18:28 WG965361
(S) Phenol-d5 61.1 20.0-120 03/30/2017 18:28 WG965361
(S) Nitrobenzene-d5 58.3 18.0-125 03/30/2017 18:28 WG965361
(S) 2-Fluorobiphenyl 65.6 28.0-120 03/30/2017 18:28 WG965361
(S) 2,4,6-Tribromophenol 68.1 17.0-137 03/30/2017 18:28 WG965361
(S) p-Terphenyl-d14 65.0 13.0-131 03/30/2017 18:28 WG965361
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 13
L898293
B-4
Collected date/time: 03/24/17 11:35
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 82.9 1 03/30/2017 15:02 WG965706
Volatile Petroleum Hydrocarbons by Method MADEPV
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Unadjusted C5-C8 Aliphatics 109 22.1 66.4 550 04/04/2017 22:08 WG965869
Unadjusted C9-C12 Aliphatics 2730 22.1 66.4 550 04/04/2017 22:08 WG965869
Unadjusted C9-C10 Aromatics 891 44.2 133 1100 04/06/2017 14:15 WG965869
Total VPH 2840 22.1 66.4 550 04/04/2017 22:08 WG965869
(S) 2,5-Dibromotoluene(FID)91.5 70.0-130 04/06/2017 14:15 WG965869
(S) 2,5-Dibromotoluene(FID)97.3 70.0-130 04/04/2017 22:08 WG965869
(S) 2,5-Dibromotoluene(PID)71.9 70.0-130 04/06/2017 14:15 WG965869
(S) 2,5-Dibromotoluene(PID)74.8 70.0-130 04/04/2017 22:08 WG965869
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acetone 0.104 0.0124 0.0621 1.03 03/31/2017 13:00 WG965859
Acrylonitrile U 0.00222 0.0124 1.03 03/31/2017 13:00 WG965859
Benzene U 0.000335 0.00124 1.03 03/31/2017 13:00 WG965859
Bromobenzene U 0.000352 0.00124 1.03 03/31/2017 13:00 WG965859
Bromodichloromethane U 0.000316 0.00124 1.03 03/31/2017 13:00 WG965859
Bromoform U 0.000527 0.00124 1.03 03/31/2017 13:00 WG965859
Bromomethane U 0.00166 0.00621 1.03 03/31/2017 13:00 WG965859
n-Butylbenzene 12.8 0.0857 0.332 275 04/04/2017 13:23 WG965859
sec-Butylbenzene 0.169 V3 0.000250 0.00124 1.03 03/31/2017 13:00 WG965859
tert-Butylbenzene 0.00596 V3 0.000256 0.00124 1.03 03/31/2017 13:00 WG965859
Carbon tetrachloride U 0.000408 0.00124 1.03 03/31/2017 13:00 WG965859
Chlorobenzene U 0.000263 0.00124 1.03 03/31/2017 13:00 WG965859
Chlorodibromomethane U 0.000463 0.00124 1.03 03/31/2017 13:00 WG965859
Chloroethane U 0.00118 0.00621 1.03 03/31/2017 13:00 WG965859
2-Chloroethyl vinyl ether U 0.00291 0.0621 1.03 03/31/2017 13:00 WG965859
Chloroform U 0.000285 0.00621 1.03 03/31/2017 13:00 WG965859
Chloromethane U 0.000466 0.00311 1.03 03/31/2017 13:00 WG965859
2-Chlorotoluene U 0.000374 0.00124 1.03 03/31/2017 13:00 WG965859
4-Chlorotoluene U 0.000298 0.00124 1.03 03/31/2017 13:00 WG965859
1,2-Dibromo-3-Chloropropane U J4 0.00130 0.00621 1.03 03/31/2017 13:00 WG965859
1,2-Dibromoethane U 0.000426 0.00124 1.03 03/31/2017 13:00 WG965859
Dibromomethane U 0.000474 0.00124 1.03 03/31/2017 13:00 WG965859
1,2-Dichlorobenzene U 0.000379 0.00124 1.03 03/31/2017 13:00 WG965859
1,3-Dichlorobenzene U 0.000297 0.00124 1.03 03/31/2017 13:00 WG965859
1,4-Dichlorobenzene U 0.000281 0.00124 1.03 03/31/2017 13:00 WG965859
Dichlorodifluoromethane U 0.000886 0.00621 1.03 03/31/2017 13:00 WG965859
1,1-Dichloroethane U 0.000247 0.00124 1.03 03/31/2017 13:00 WG965859
1,2-Dichloroethane U 0.000329 0.00124 1.03 03/31/2017 13:00 WG965859
1,1-Dichloroethene U 0.000376 0.00124 1.03 03/31/2017 13:00 WG965859
cis-1,2-Dichloroethene U 0.000292 0.00124 1.03 03/31/2017 13:00 WG965859
trans-1,2-Dichloroethene U 0.000328 0.00124 1.03 03/31/2017 13:00 WG965859
1,2-Dichloropropane U 0.000445 0.00124 1.03 03/31/2017 13:00 WG965859
1,1-Dichloropropene U 0.000393 0.00124 1.03 03/31/2017 13:00 WG965859
1,3-Dichloropropane U 0.000257 0.00124 1.03 03/31/2017 13:00 WG965859
cis-1,3-Dichloropropene U 0.000326 0.00124 1.03 03/31/2017 13:00 WG965859
trans-1,3-Dichloropropene U 0.000332 0.00124 1.03 03/31/2017 13:00 WG965859
2,2-Dichloropropane U 0.000346 0.00124 1.03 03/31/2017 13:00 WG965859
Di-isopropyl ether U 0.000308 0.00124 1.03 03/31/2017 13:00 WG965859
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 13
L898293
B-4
Collected date/time: 03/24/17 11:35
Volatile Organic Compounds (GC/MS) by Method 8260B
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Ethylbenzene 12.9 0.0986 0.332 275 04/04/2017 13:23 WG965859
Hexachloro-1,3-butadiene U 0.000425 0.00124 1.03 03/31/2017 13:00 WG965859
Isopropylbenzene 3.53 0.0806 0.332 275 04/04/2017 13:23 WG965859
p-Isopropyltoluene 0.0880 V3 0.000253 0.00124 1.03 03/31/2017 13:00 WG965859
2-Butanone (MEK)0.0325 J3 0.00581 0.0124 1.03 03/31/2017 13:00 WG965859
Methylene Chloride U 0.00124 0.00621 1.03 03/31/2017 13:00 WG965859
4-Methyl-2-pentanone (MIBK)U J3 J4 0.00234 0.0124 1.03 03/31/2017 13:00 WG965859
Methyl tert-butyl ether U 0.000263 0.00124 1.03 03/31/2017 13:00 WG965859
Naphthalene 67.3 3.32 16.6 2750 04/04/2017 17:00 WG965859
n-Propylbenzene 21.3 0.0683 0.332 275 04/04/2017 13:23 WG965859
Styrene U 0.000291 0.00124 1.03 03/31/2017 13:00 WG965859
1,1,1,2-Tetrachloroethane U 0.000328 0.00124 1.03 03/31/2017 13:00 WG965859
1,1,2,2-Tetrachloroethane U 0.000454 0.00124 1.03 03/31/2017 13:00 WG965859
Tetrachloroethene U 0.000343 0.00124 1.03 03/31/2017 13:00 WG965859
Toluene 2.51 B 0.144 1.66 275 04/04/2017 13:23 WG965859
1,2,3-Trichlorobenzene U 0.000380 0.00124 1.03 03/31/2017 13:00 WG965859
1,2,4-Trichlorobenzene U 0.000483 0.00124 1.03 03/31/2017 13:00 WG965859
1,1,1-Trichloroethane U 0.000355 0.00124 1.03 03/31/2017 13:00 WG965859
1,1,2-Trichloroethane U 0.000344 0.00124 1.03 03/31/2017 13:00 WG965859
Trichloroethene U 0.000346 0.00124 1.03 03/31/2017 13:00 WG965859
Trichlorofluoromethane U 0.000474 0.00621 1.03 03/31/2017 13:00 WG965859
1,2,3-Trichloropropane U 0.000920 0.00311 1.03 03/31/2017 13:00 WG965859
1,2,4-Trimethylbenzene 265 0.700 3.32 2750 04/04/2017 17:00 WG965859
1,3,5-Trimethylbenzene 81.2 0.883 3.32 2750 04/04/2017 17:00 WG965859
Vinyl chloride U 0.000362 0.00124 1.03 03/31/2017 13:00 WG965859
Xylenes, Total 161 0.232 0.995 275 04/04/2017 13:23 WG965859
(S) Toluene-d8 97.4 80.0-120 03/31/2017 13:00 WG965859
(S) Toluene-d8 107 80.0-120 04/04/2017 13:23 WG965859
(S) Toluene-d8 107 80.0-120 04/04/2017 17:00 WG965859
(S) Dibromofluoromethane 103 74.0-131 03/31/2017 13:00 WG965859
(S) Dibromofluoromethane 99.8 74.0-131 04/04/2017 13:23 WG965859
(S) Dibromofluoromethane 96.3 74.0-131 04/04/2017 17:00 WG965859
(S) 4-Bromofluorobenzene 107 64.0-132 03/31/2017 13:00 WG965859
(S) 4-Bromofluorobenzene 98.7 64.0-132 04/04/2017 13:23 WG965859
(S) 4-Bromofluorobenzene 99.1 64.0-132 04/04/2017 17:00 WG965859
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
Acenaphthene 0.210 J 0.154 0.796 20 03/31/2017 18:57 WG965361
Acenaphthylene U 0.162 0.796 20 03/31/2017 18:57 WG965361
Anthracene 0.0807 0.00762 0.0398 1 03/30/2017 16:49 WG965361
Atrazine U 2.27 8.03 20 03/31/2017 18:57 WG965361
Benzaldehyde U 1.28 8.03 20 03/31/2017 18:57 WG965361
Benzo(a)anthracene 0.0157 J 0.00516 0.0398 1 03/30/2017 16:49 WG965361
Benzo(b)fluoranthene U 0.00838 0.0398 1 03/30/2017 16:49 WG965361
Benzo(k)fluoranthene U 0.00702 0.0398 1 03/30/2017 16:49 WG965361
Benzo(g,h,i)perylene 0.0104 J J3 0.00870 0.0398 1 03/30/2017 16:49 WG965361
Benzo(a)pyrene 0.00663 J 0.00661 0.0398 1 03/30/2017 16:49 WG965361
Biphenyl 0.407 J 0.142 8.03 20 03/31/2017 18:57 WG965361
Bis(2-chlorethoxy)methane U 0.186 8.03 20 03/31/2017 18:57 WG965361
Bis(2-chloroethyl)ether U 0.216 8.03 20 03/31/2017 18:57 WG965361
Bis(2-chloroisopropyl)ether U 0.183 8.03 20 03/31/2017 18:57 WG965361
4-Bromophenyl-phenylether U 0.0138 0.402 1 03/30/2017 16:49 WG965361
Caprolactam U 2.51 8.03 20 03/31/2017 18:57 WG965361
Carbazole U 0.00632 0.402 1 03/30/2017 16:49 WG965361
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 13
L898293
B-4
Collected date/time: 03/24/17 11:35
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
2-Chloronaphthalene U 0.154 0.796 20 03/31/2017 18:57 WG965361
4-Chlorophenyl-phenylether U 0.151 8.03 20 03/31/2017 18:57 WG965361
Chrysene 0.0169 J 0.00670 0.0398 1 03/30/2017 16:49 WG965361
Dibenz(a,h)anthracene U 0.00990 0.0398 1 03/30/2017 16:49 WG965361
3,3-Dichlorobenzidine U 0.0958 0.402 1 03/30/2017 16:49 WG965361
2,4-Dinitrotoluene U 0.146 8.03 20 03/31/2017 18:57 WG965361
2,6-Dinitrotoluene U 0.177 8.03 20 03/31/2017 18:57 WG965361
Fluoranthene 0.0482 0.00598 0.0398 1 03/30/2017 16:49 WG965361
Fluorene 0.230 J 0.164 0.796 20 03/31/2017 18:57 WG965361
Hexachlorobenzene U 0.0103 0.402 1 03/30/2017 16:49 WG965361
Hexachloro-1,3-butadiene U 0.241 8.03 20 03/31/2017 18:57 WG965361
Hexachlorocyclopentadiene U 1.41 8.03 20 03/31/2017 18:57 WG965361
Hexachloroethane U 0.323 8.03 20 03/31/2017 18:57 WG965361
Indeno(1,2,3-cd)pyrene U J3 0.00931 0.0398 1 03/30/2017 16:49 WG965361
Isophorone 0.165 J 0.125 8.03 20 03/31/2017 18:57 WG965361
Naphthalene 23.2 0.215 0.796 20 03/31/2017 18:57 WG965361
Nitrobenzene U 0.168 8.03 20 03/31/2017 18:57 WG965361
n-Nitrosodiphenylamine U 0.00717 0.402 1 03/30/2017 16:49 WG965361
n-Nitrosodi-n-propylamine U 0.218 8.03 20 03/31/2017 18:57 WG965361
Phenanthrene 0.630 0.00637 0.0398 1 03/30/2017 16:49 WG965361
Benzylbutyl phthalate U 0.0124 0.402 1 03/30/2017 16:49 WG965361
Bis(2-ethylhexyl)phthalate 0.0165 J 0.0145 0.402 1 03/30/2017 16:49 WG965361
Di-n-butyl phthalate U 0.0131 0.402 1 03/30/2017 16:49 WG965361
Diethyl phthalate U 0.166 8.03 20 03/31/2017 18:57 WG965361
Dimethyl phthalate U 0.130 8.03 20 03/31/2017 18:57 WG965361
Di-n-octyl phthalate U 0.0109 0.402 1 03/30/2017 16:49 WG965361
Pyrene 0.118 0.0148 0.0398 1 03/30/2017 16:49 WG965361
4-Chloroaniline U 0.849 8.03 20 03/31/2017 18:57 WG965361
4-Chloro-3-methylphenol U 0.115 8.03 20 03/31/2017 18:57 WG965361
2-Chlorophenol U 0.200 8.03 20 03/31/2017 18:57 WG965361
Dibenzofuran U 0.125 8.03 20 03/31/2017 18:57 WG965361
2,4-Dichlorophenol U 0.180 8.03 20 03/31/2017 18:57 WG965361
2,4-Dimethylphenol U 1.14 8.03 20 03/31/2017 18:57 WG965361
4,6-Dinitro-2-methylphenol U 0.150 0.402 1 03/30/2017 16:49 WG965361
2,4-Dinitrophenol U 2.36 8.03 20 03/31/2017 18:57 WG965361
2-Methylnaphthalene 20.6 0.208 0.796 20 03/31/2017 18:57 WG965361
2-Methylphenol U 0.238 8.03 20 03/31/2017 18:57 WG965361
3&4-Methyl Phenol U 0.189 8.03 20 03/31/2017 18:57 WG965361
2-Nitroaniline U 0.182 8.03 20 03/31/2017 18:57 WG965361
3-Nitroaniline U 0.205 8.03 20 03/31/2017 18:57 WG965361
4-Nitroaniline U 0.154 8.03 20 03/31/2017 18:57 WG965361
2-Nitrophenol U 0.314 8.03 20 03/31/2017 18:57 WG965361
4-Nitrophenol U 1.27 8.03 20 03/31/2017 18:57 WG965361
Pentachlorophenol U 0.0579 0.402 1 03/30/2017 16:49 WG965361
Phenol U 0.168 8.03 20 03/31/2017 18:57 WG965361
2,4,6-Trichlorophenol U 0.188 8.03 20 03/31/2017 18:57 WG965361
Acetophenone U 1.81 8.03 20 03/31/2017 18:57 WG965361
1,2,4,5-Tetrachlorobenzene U 1.83 8.03 20 03/31/2017 18:57 WG965361
2,4,5-Trichlorophenol U 0.251 8.03 20 03/31/2017 18:57 WG965361
2,3,4,6-Tetrachlorophenol U 2.92 8.03 20 03/31/2017 18:57 WG965361
(S) 2-Fluorophenol 53.7 20.0-120 03/30/2017 16:49 WG965361
(S) 2-Fluorophenol 51.7 J7 20.0-120 03/31/2017 18:57 WG965361
(S) Phenol-d5 108 20.0-120 03/30/2017 16:49 WG965361
(S) Phenol-d5 90.5 J7 20.0-120 03/31/2017 18:57 WG965361
(S) Nitrobenzene-d5 232 J1 18.0-125 03/30/2017 16:49 WG965361
(S) Nitrobenzene-d5 103 J7 18.0-125 03/31/2017 18:57 WG965361
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 13
L898293
B-4
Collected date/time: 03/24/17 11:35
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Result (dry)Qualifier MDL (dry)RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
(S) 2-Fluorobiphenyl 67.8 28.0-120 03/30/2017 16:49 WG965361
(S) 2-Fluorobiphenyl 59.8 J7 28.0-120 03/31/2017 18:57 WG965361
(S) 2,4,6-Tribromophenol 84.5 17.0-137 03/30/2017 16:49 WG965361
(S) 2,4,6-Tribromophenol 45.7 J7 17.0-137 03/31/2017 18:57 WG965361
(S) p-Terphenyl-d14 77.2 13.0-131 03/30/2017 16:49 WG965361
(S) p-Terphenyl-d14 55.8 J7 13.0-131 03/31/2017 18:57 WG965361
Sample Narrative:
8270D L898293-13 WG965361: IS/SURR failed on lower dilution.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG965406
Total Solids by Method 2540 G-2011 L898293-10
Method Blank (MB)
(MB) R3207279-1 03/30/17 10:49
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.000400
L898188-03 Original Sample (OS) • Duplicate (DUP)
(OS) L898188-03 03/30/17 10:49 • (DUP) R3207279-3 03/30/17 10:49
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte %%%%
Total Solids 88.8 89.1 1 0.232 5
Laboratory Control Sample (LCS)
(LCS) R3207279-2 03/30/17 10:49
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 99.9 85.0-115
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG965706
Total Solids by Method 2540 G-2011 L898293-11,12,13
Method Blank (MB)
(MB) R3207254-1 03/30/17 15:02
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.00100
L898293-11 Original Sample (OS) • Duplicate (DUP)
(OS) L898293-11 03/30/17 15:02 • (DUP) R3207254-3 03/30/17 15:02
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte %%%%
Total Solids 86.5 88.2 1 1.95 5
Laboratory Control Sample (LCS)
(LCS) R3207254-2 03/30/17 15:02
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG965869
Volatile Petroleum Hydrocarbons by Method MADEPV L898293-10,11,12,13
Method Blank (MB)
(MB) R3207850-3 03/30/17 18:10
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Unadjusted C5-C8 Aliphatics U 1.67 5.00
Unadjusted C9-C12 Aliphatics U 1.67 5.00
Unadjusted C9-C10 Aromatics U 1.67 5.00
Total VPH U 1.67 5.00
(S) 2,5-Dibromotoluene(FID)94.7 70.0-130
(S) 2,5-Dibromotoluene(PID)78.5 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3207850-1 03/30/17 16:00 • (LCSD) R3207850-2 03/30/17 16:32
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l %%%%%
Unadjusted C5-C8 Aliphatics 1.20 1.25 1.21 104 101 70.0-130 3.25 25
Unadjusted C9-C12 Aliphatics 1.40 1.59 1.58 114 113 70.0-130 1.14 25
Unadjusted C9-C10 Aromatics 0.200 0.186 0.184 93.0 92.0 70.0-130 1.15 25
Total VPH 2.80 3.03 2.97 108 106 70.0-130 1.73 25
(S) 2,5-Dibromotoluene(FID) 94.7 97.7 70.0-130
(S) 2,5-Dibromotoluene(PID) 82.2 84.0 70.0-130
L898335-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L898335-01 03/30/17 22:22 • (MS) R3207850-4 03/30/17 20:45 • (MSD) R3207850-5 03/30/17 21:17
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/l mg/l mg/l mg/l %%%%%
Unadjusted C5-C8 Aliphatics 1.20 U 58.9 62.6 99.1 105 49.5 70.0-130 6.17 25
Unadjusted C9-C12 Aliphatics 1.40 U 74.1 79.6 107 115 49.5 70.0-130 7.21 25
Unadjusted C9-C10 Aromatics 0.200 U 8.83 9.39 89.2 94.9 49.5 70.0-130 6.18 25
Total VPH 2.80 U 142 152 102 109 49.5 70.0-130 6.65 25
(S) 2,5-Dibromotoluene(FID) 93.4 95.7 70.0-130
(S) 2,5-Dibromotoluene(PID) 81.4 82.5 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG964562
Volatile Organic Compounds (GC/MS) by Method 6200B-1997 L898293-01,02,03,04,05,06,07,08,09
Method Blank (MB)
(MB) R3207501-4 03/31/17 14:54
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Acetone U 10.0 50.0
Acrolein U 8.87 50.0
Acrylonitrile U 1.87 10.0
Benzene U 0.331 1.00
Bromobenzene U 0.352 1.00
Bromodichloromethane U 0.380 1.00
Bromoform U 0.469 1.00
Bromomethane U 0.866 5.00
n-Butylbenzene U 0.361 1.00
sec-Butylbenzene U 0.365 1.00
tert-Butylbenzene U 0.399 1.00
Carbon tetrachloride U 0.379 1.00
Chlorobenzene U 0.348 1.00
Chlorodibromomethane U 0.327 1.00
Chloroethane U 0.453 5.00
Chloroform U 0.324 5.00
Chloromethane U 0.276 2.50
2-Chlorotoluene U 0.375 1.00
4-Chlorotoluene U 0.351 1.00
1,2-Dibromo-3-Chloropropane U 1.33 5.00
1,2-Dibromoethane U 0.381 1.00
Dibromomethane U 0.346 1.00
1,2-Dichlorobenzene U 0.349 1.00
1,3-Dichlorobenzene U 0.220 1.00
1,4-Dichlorobenzene U 0.274 1.00
Dichlorodifluoromethane U 0.551 5.00
1,1-Dichloroethane U 0.259 1.00
1,2-Dichloroethane U 0.361 1.00
1,1-Dichloroethene U 0.398 1.00
cis-1,2-Dichloroethene U 0.260 1.00
trans-1,2-Dichloroethene U 0.396 1.00
1,2-Dichloropropane U 0.306 1.00
1,1-Dichloropropene U 0.352 1.00
1,3-Dichloropropane U 0.366 1.00
2,2-Dichloropropane U 0.321 1.00
Di-isopropyl ether U 0.320 1.00
Ethylbenzene U 0.384 1.00
Hexachloro-1,3-butadiene U 0.256 1.00
2-Butanone (MEK)U 3.93 10.0
Isopropylbenzene U 0.326 1.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG964562
Volatile Organic Compounds (GC/MS) by Method 6200B-1997 L898293-01,02,03,04,05,06,07,08,09
Method Blank (MB)
(MB) R3207501-4 03/31/17 14:54
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
p-Isopropyltoluene U 0.350 1.00
Methylene Chloride U 1.00 5.00
4-Methyl-2-pentanone (MIBK)U 2.14 10.0
Methyl tert-butyl ether U 0.367 1.00
Naphthalene U 1.00 5.00
Styrene U 0.307 1.00
1,1,1,2-Tetrachloroethane U 0.385 1.00
1,1,2,2-Tetrachloroethane U 0.130 1.00
n-Propylbenzene U 0.349 1.00
Tetrachloroethene U 0.372 1.00
Toluene U 0.412 1.00
1,2,4-Trichlorobenzene U 0.355 1.00
1,1,1-Trichloroethane U 0.319 1.00
1,1,2-Trichloroethane U 0.383 1.00
1,2,3-Trichlorobenzene U 0.230 1.00
Trichloroethene U 0.398 1.00
Trichlorofluoromethane U 1.20 5.00
1,2,3-Trichloropropane U 0.807 2.50
1,2,4-Trimethylbenzene U 0.373 1.00
Vinyl chloride U 0.259 1.00
1,3,5-Trimethylbenzene U 0.387 1.00
o-Xylene U 0.341 1.00
m&p-Xylenes U 0.719 2.00
(S) Toluene-d8 103 80.0-120
(S) Dibromofluoromethane 108 76.0-123
(S) a,a,a-Trifluorotoluene 100 80.0-120
(S) 4-Bromofluorobenzene 104 80.0-120
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3207501-1 03/31/17 13:22 • (LCSD) R3207501-6 04/01/17 21:42
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Acetone 125 99.6 114 79.7 91.1 10.0-160 13.4 23
Acetone 125 99.6 117 79.7 94.0 10.0-160 16.5 23
Acrolein 125 562 568 450 454 10.0-160 E J4 E J4 0.960 20
Acrolein 125 562 573 450 459 10.0-160 E J4 E J4 1.89 20
Acrylonitrile 125 140 135 112 108 60.0-142 3.63 20
Acrylonitrile 125 140 147 112 118 60.0-142 4.70 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG964562
Volatile Organic Compounds (GC/MS) by Method 6200B-1997 L898293-01,02,03,04,05,06,07,08,09
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3207501-1 03/31/17 13:22 • (LCSD) R3207501-6 04/01/17 21:42
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Benzene 25.0 24.9 25.0 99.5 100 69.0-123 0.710 20
Benzene 25.0 24.9 25.2 99.5 101 69.0-123 1.19 20
Bromobenzene 25.0 26.0 25.9 104 104 79.0-120 0.220 20
Bromobenzene 25.0 26.0 26.9 104 108 79.0-120 3.48 20
Bromodichloromethane 25.0 26.2 26.2 105 105 76.0-120 0.220 20
Bromodichloromethane 25.0 26.2 26.5 105 106 76.0-120 1.29 20
Bromoform 25.0 23.5 23.5 93.9 93.8 67.0-132 0.0900 20
Bromoform 25.0 23.5 23.9 93.9 95.5 67.0-132 1.64 20
Bromomethane 25.0 24.2 21.2 96.7 84.6 18.0-160 13.4 20
Bromomethane 25.0 24.2 17.1 96.7 68.2 18.0-160 J3 34.6 20
n-Butylbenzene 25.0 23.4 23.2 93.4 92.7 72.0-126 0.790 20
n-Butylbenzene 25.0 23.4 24.4 93.4 97.4 72.0-126 4.18 20
sec-Butylbenzene 25.0 23.0 23.6 91.9 94.4 74.0-121 2.72 20
sec-Butylbenzene 25.0 23.0 22.2 91.9 88.8 74.0-121 3.42 20
tert-Butylbenzene 25.0 21.3 21.1 85.4 84.3 75.0-122 1.21 20
tert-Butylbenzene 25.0 21.3 22.1 85.4 88.4 75.0-122 3.52 20
Carbon tetrachloride 25.0 23.1 23.6 92.5 94.4 63.0-122 2.01 20
Carbon tetrachloride 25.0 23.1 22.4 92.5 89.5 63.0-122 3.38 20
Chlorobenzene 25.0 27.0 27.1 108 108 79.0-121 0.110 20
Chlorobenzene 25.0 27.0 27.4 108 110 79.0-121 1.36 20
Chlorodibromomethane 25.0 26.7 26.9 107 108 75.0-125 0.880 20
Chlorodibromomethane 25.0 26.7 27.5 107 110 75.0-125 3.13 20
Chloroethane 25.0 14.0 14.3 56.2 57.0 47.0-152 1.48 20
Chloroethane 25.0 14.0 12.3 56.2 49.0 47.0-152 13.6 20
Chloroform 25.0 27.2 27.5 109 110 72.0-121 0.850 20
Chloroform 25.0 27.2 27.8 109 111 72.0-121 1.92 20
Chloromethane 25.0 21.1 20.7 84.3 82.9 48.0-139 1.63 20
Chloromethane 25.0 21.1 22.0 84.3 88.0 48.0-139 4.37 20
2-Chlorotoluene 25.0 26.3 26.1 105 104 74.0-122 0.730 20
2-Chlorotoluene 25.0 26.3 26.9 105 107 74.0-122 2.24 20
4-Chlorotoluene 25.0 26.3 25.9 105 103 79.0-120 1.76 20
4-Chlorotoluene 25.0 26.3 27.0 105 108 79.0-120 2.68 20
1,2-Dibromo-3-Chloropropane 25.0 25.6 25.8 102 103 64.0-127 0.770 20
1,2-Dibromo-3-Chloropropane 25.0 25.6 23.4 102 93.6 64.0-127 9.11 20
1,2-Dibromoethane 25.0 27.1 27.5 108 110 77.0-123 1.42 20
1,2-Dibromoethane 25.0 27.1 26.5 108 106 77.0-123 2.37 20
Dibromomethane 25.0 23.1 23.6 92.2 94.3 78.0-120 2.26 20
Dibromomethane 25.0 23.1 23.9 92.2 95.5 78.0-120 3.51 20
1,2-Dichlorobenzene 25.0 27.4 28.1 109 112 80.0-120 2.67 20
1,2-Dichlorobenzene 25.0 27.4 28.3 109 113 80.0-120 3.31 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG964562
Volatile Organic Compounds (GC/MS) by Method 6200B-1997 L898293-01,02,03,04,05,06,07,08,09
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3207501-1 03/31/17 13:22 • (LCSD) R3207501-6 04/01/17 21:42
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
1,3-Dichlorobenzene 25.0 25.8 26.0 103 104 72.0-123 0.480 20
1,3-Dichlorobenzene 25.0 25.8 26.9 103 108 72.0-123 3.99 20
1,4-Dichlorobenzene 25.0 26.8 27.3 107 109 77.0-120 2.02 20
1,4-Dichlorobenzene 25.0 26.8 27.6 107 110 77.0-120 3.14 20
Dichlorodifluoromethane 25.0 30.2 29.8 121 119 49.0-155 1.37 20
Dichlorodifluoromethane 25.0 30.2 27.3 121 109 49.0-155 10.0 20
1,1-Dichloroethane 25.0 27.1 27.1 108 108 70.0-126 0.0800 20
1,1-Dichloroethane 25.0 27.1 27.5 108 110 70.0-126 1.53 20
1,2-Dichloroethane 25.0 25.8 25.7 103 103 67.0-126 0.360 20
1,2-Dichloroethane 25.0 25.8 26.2 103 105 67.0-126 1.38 20
1,1-Dichloroethene 25.0 27.6 28.0 110 112 64.0-129 1.59 20
1,1-Dichloroethene 25.0 27.6 26.5 110 106 64.0-129 4.04 20
cis-1,2-Dichloroethene 25.0 27.7 27.9 111 111 73.0-120 0.760 20
cis-1,2-Dichloroethene 25.0 27.7 28.2 111 113 73.0-120 2.01 20
trans-1,2-Dichloroethene 25.0 26.9 27.2 108 109 71.0-121 1.18 20
trans-1,2-Dichloroethene 25.0 26.9 27.5 108 110 71.0-121 2.09 20
1,2-Dichloropropane 25.0 26.3 26.6 105 106 75.0-125 1.02 20
1,2-Dichloropropane 25.0 26.3 26.7 105 107 75.0-125 1.35 20
1,1-Dichloropropene 25.0 27.6 27.4 111 110 71.0-129 0.660 20
1,1-Dichloropropene 25.0 27.6 28.1 111 113 71.0-129 1.87 20
1,3-Dichloropropane 25.0 27.9 28.4 112 113 80.0-121 1.48 20
1,3-Dichloropropane 25.0 27.9 28.6 112 114 80.0-121 2.29 20
2,2-Dichloropropane 25.0 23.7 24.0 94.8 96.2 60.0-125 1.44 20
2,2-Dichloropropane 25.0 23.7 24.1 94.8 96.2 60.0-125 1.45 20
Di-isopropyl ether 25.0 24.7 24.9 98.7 99.6 59.0-133 0.920 20
Di-isopropyl ether 25.0 24.7 24.9 98.7 99.8 59.0-133 1.06 20
Ethylbenzene 25.0 23.4 23.4 93.7 93.5 77.0-120 0.150 20
Ethylbenzene 25.0 23.4 24.0 93.7 95.9 77.0-120 2.32 20
Hexachloro-1,3-butadiene 25.0 22.6 22.2 90.5 88.7 64.0-131 1.98 20
Hexachloro-1,3-butadiene 25.0 22.6 24.1 90.5 96.3 64.0-131 6.19 20
Isopropylbenzene 25.0 22.4 22.9 89.7 91.8 75.0-120 2.29 20
Isopropylbenzene 25.0 22.4 21.8 89.7 87.4 75.0-120 2.63 20
2-Butanone (MEK)125 131 134 105 107 37.0-158 2.11 20
2-Butanone (MEK)125 131 144 105 115 37.0-158 9.30 20
p-Isopropyltoluene 25.0 24.0 23.4 96.1 93.7 74.0-126 2.50 20
p-Isopropyltoluene 25.0 24.0 24.7 96.1 98.7 74.0-126 2.62 20
Methylene Chloride 25.0 26.2 26.4 105 106 66.0-121 0.580 20
Methylene Chloride 25.0 26.2 26.8 105 107 66.0-121 2.28 20
4-Methyl-2-pentanone (MIBK)125 145 140 116 112 59.0-143 3.33 20
4-Methyl-2-pentanone (MIBK)125 145 150 116 120 59.0-143 3.50 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG964562
Volatile Organic Compounds (GC/MS) by Method 6200B-1997 L898293-01,02,03,04,05,06,07,08,09
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3207501-1 03/31/17 13:22 • (LCSD) R3207501-6 04/01/17 21:42
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Methyl tert-butyl ether 25.0 26.2 26.6 105 106 64.0-123 1.20 20
Methyl tert-butyl ether 25.0 26.2 27.0 105 108 64.0-123 3.01 20
Naphthalene 25.0 23.0 22.4 92.2 89.6 62.0-128 2.88 20
Naphthalene 25.0 23.0 24.0 92.2 95.8 62.0-128 3.89 20
n-Propylbenzene 25.0 23.1 22.7 92.4 90.6 79.0-120 1.97 20
n-Propylbenzene 25.0 23.1 23.6 92.4 94.5 79.0-120 2.24 20
Styrene 25.0 24.6 24.3 98.5 97.3 78.0-124 1.21 20
Styrene 25.0 24.6 24.1 98.5 96.3 78.0-124 2.26 20
1,1,1,2-Tetrachloroethane 25.0 26.5 26.6 106 106 75.0-122 0.270 20
1,1,1,2-Tetrachloroethane 25.0 26.5 26.3 106 105 75.0-122 0.710 20
1,1,2,2-Tetrachloroethane 25.0 25.5 25.5 102 102 71.0-122 0.0400 20
1,1,2,2-Tetrachloroethane 25.0 25.5 25.4 102 102 71.0-122 0.340 20
Tetrachloroethene 25.0 26.3 26.6 105 106 70.0-127 1.12 20
Tetrachloroethene 25.0 26.3 25.6 105 102 70.0-127 2.70 20
Toluene 25.0 23.2 23.3 92.8 93.1 77.0-120 0.280 20
Toluene 25.0 23.2 23.5 92.8 94.0 77.0-120 1.29 20
1,2,3-Trichlorobenzene 25.0 25.4 25.2 102 101 61.0-133 0.870 20
1,2,3-Trichlorobenzene 25.0 25.4 26.6 102 106 61.0-133 4.50 20
1,2,4-Trichlorobenzene 25.0 26.2 26.1 105 104 69.0-129 0.540 20
1,2,4-Trichlorobenzene 25.0 26.2 27.1 105 108 69.0-129 3.31 20
1,1,1-Trichloroethane 25.0 27.4 27.5 110 110 68.0-122 0.390 20
1,1,1-Trichloroethane 25.0 27.4 25.9 110 104 68.0-122 5.57 20
1,1,2-Trichloroethane 25.0 28.0 28.2 112 113 78.0-120 0.770 20
1,1,2-Trichloroethane 25.0 28.0 28.2 112 113 78.0-120 0.900 20
Trichloroethene 25.0 26.6 26.1 106 104 78.0-120 1.76 20
Trichloroethene 25.0 26.6 27.2 106 109 78.0-120 2.41 20
Trichlorofluoromethane 25.0 21.9 19.0 87.7 75.9 56.0-137 14.4 20
Trichlorofluoromethane 25.0 21.9 23.1 87.7 92.4 56.0-137 5.29 20
1,2,3-Trichloropropane 25.0 25.6 25.3 102 101 72.0-124 1.15 20
1,2,3-Trichloropropane 25.0 25.6 26.3 102 105 72.0-124 2.90 20
1,2,4-Trimethylbenzene 25.0 24.8 24.6 99.1 98.4 75.0-120 0.760 20
1,2,4-Trimethylbenzene 25.0 24.8 25.5 99.1 102 75.0-120 2.77 20
1,3,5-Trimethylbenzene 25.0 24.3 23.9 97.3 95.8 75.0-120 1.61 20
1,3,5-Trimethylbenzene 25.0 24.3 25.1 97.3 100 75.0-120 3.02 20
Vinyl chloride 25.0 26.3 20.8 105 83.2 64.0-133 J3 23.2 20
Vinyl chloride 25.0 26.3 27.2 105 109 64.0-133 3.46 20
o-Xylene 25.0 23.6 23.9 94.2 95.6 78.0-120 1.42 20
o-Xylene 25.0 23.6 23.1 94.2 92.3 78.0-120 2.08 20
m&p-Xylenes 50.0 47.1 46.4 94.1 92.7 77.0-120 1.48 20
m&p-Xylenes 50.0 47.1 48.4 94.1 96.9 77.0-120 2.91 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Excel Civil & Environmental Associates 24090 L898293 04/07/17 10:15 44 of 62
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG964562
Volatile Organic Compounds (GC/MS) by Method 6200B-1997 L898293-01,02,03,04,05,06,07,08,09
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3207501-1 03/31/17 13:22 • (LCSD) R3207501-6 04/01/17 21:42
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
(S) Toluene-d8 103 102 80.0-120
(S) Toluene-d8 103 103 80.0-120
(S) Dibromofluoromethane 107 108 76.0-123
(S) Dibromofluoromethane 107 108 76.0-123
(S) a,a,a-Trifluorotoluene 99.1 98.5 80.0-120
(S) a,a,a-Trifluorotoluene 99.1 100 80.0-120
(S) 4-Bromofluorobenzene 101 102 80.0-120
(S) 4-Bromofluorobenzene 101 100 80.0-120
Laboratory Control Sample (LCS)
(LCS) R3207501-5 04/01/17 12:04
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Acetone 125 123 98.7 10.0-160
Acrolein 125 579 464 10.0-160 E J4
Acrylonitrile 125 138 110 60.0-142
Benzene 25.0 25.2 101 69.0-123
Bromobenzene 25.0 26.4 106 79.0-120
Bromodichloromethane 25.0 26.5 106 76.0-120
Bromoform 25.0 23.9 95.7 67.0-132
Bromomethane 25.0 18.2 72.7 18.0-160
n-Butylbenzene 25.0 24.2 96.6 72.0-126
sec-Butylbenzene 25.0 23.0 92.1 74.0-121
tert-Butylbenzene 25.0 21.7 86.6 75.0-122
Carbon tetrachloride 25.0 23.0 92.0 63.0-122
Chlorobenzene 25.0 27.3 109 79.0-121
Chlorodibromomethane 25.0 26.9 108 75.0-125
Chloroethane 25.0 14.2 56.9 47.0-152
Chloroform 25.0 27.2 109 72.0-121
Chloromethane 25.0 23.3 93.4 48.0-139
2-Chlorotoluene 25.0 26.6 106 74.0-122
4-Chlorotoluene 25.0 26.1 104 79.0-120
1,2-Dibromo-3-Chloropropane 25.0 24.5 97.9 64.0-127
1,2-Dibromoethane 25.0 26.8 107 77.0-123
Dibromomethane 25.0 23.8 95.3 78.0-120
1,2-Dichlorobenzene 25.0 27.8 111 80.0-120
1,3-Dichlorobenzene 25.0 26.3 105 72.0-123
1,4-Dichlorobenzene 25.0 27.2 109 77.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG964562
Volatile Organic Compounds (GC/MS) by Method 6200B-1997 L898293-01,02,03,04,05,06,07,08,09
Laboratory Control Sample (LCS)
(LCS) R3207501-5 04/01/17 12:04
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Dichlorodifluoromethane 25.0 33.7 135 49.0-155
1,1-Dichloroethane 25.0 27.4 110 70.0-126
1,2-Dichloroethane 25.0 25.8 103 67.0-126
1,1-Dichloroethene 25.0 28.4 114 64.0-129
cis-1,2-Dichloroethene 25.0 28.0 112 73.0-120
trans-1,2-Dichloroethene 25.0 28.2 113 71.0-121
1,2-Dichloropropane 25.0 26.7 107 75.0-125
1,1-Dichloropropene 25.0 28.3 113 71.0-129
1,3-Dichloropropane 25.0 28.5 114 80.0-121
2,2-Dichloropropane 25.0 24.7 98.7 60.0-125
Di-isopropyl ether 25.0 24.9 99.8 59.0-133
Ethylbenzene 25.0 23.7 94.6 77.0-120
Hexachloro-1,3-butadiene 25.0 24.3 97.1 64.0-131
Isopropylbenzene 25.0 22.4 89.7 75.0-120
2-Butanone (MEK)125 142 114 37.0-158
p-Isopropyltoluene 25.0 24.3 97.3 74.0-126
Methylene Chloride 25.0 26.4 106 66.0-121
4-Methyl-2-pentanone (MIBK)125 146 117 59.0-143
Methyl tert-butyl ether 25.0 26.5 106 64.0-123
Naphthalene 25.0 23.1 92.4 62.0-128
n-Propylbenzene 25.0 23.3 93.2 79.0-120
Styrene 25.0 24.7 98.9 78.0-124
1,1,1,2-Tetrachloroethane 25.0 26.5 106 75.0-122
1,1,2,2-Tetrachloroethane 25.0 25.8 103 71.0-122
Tetrachloroethene 25.0 26.3 105 70.0-127
Toluene 25.0 23.5 94.1 77.0-120
1,2,3-Trichlorobenzene 25.0 25.8 103 61.0-133
1,2,4-Trichlorobenzene 25.0 26.1 104 69.0-129
1,1,1-Trichloroethane 25.0 27.0 108 68.0-122
1,1,2-Trichloroethane 25.0 28.2 113 78.0-120
Trichloroethene 25.0 26.5 106 78.0-120
Trichlorofluoromethane 25.0 26.1 104 56.0-137
1,2,3-Trichloropropane 25.0 25.4 101 72.0-124
1,2,4-Trimethylbenzene 25.0 25.0 100 75.0-120
1,3,5-Trimethylbenzene 25.0 24.4 97.8 75.0-120
Vinyl chloride 25.0 28.1 113 64.0-133
o-Xylene 25.0 23.5 94.0 78.0-120
m&p-Xylenes 50.0 47.6 95.1 77.0-120
(S) Toluene-d8 104 80.0-120
(S) Dibromofluoromethane 107 76.0-123
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG964562
Volatile Organic Compounds (GC/MS) by Method 6200B-1997 L898293-01,02,03,04,05,06,07,08,09
Laboratory Control Sample (LCS)
(LCS) R3207501-5 04/01/17 12:04
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
(S) a,a,a-Trifluorotoluene 100 80.0-120
(S) 4-Bromofluorobenzene 101 80.0-120
L898388-07 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L898388-07 04/02/17 00:59 • (MS) R3207501-7 04/02/17 01:22 • (MSD) R3207501-8 04/02/17 01:45
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Acetone 125 U 2220 2260 71.0 72.4 25 10.0-139 1.97 25
Acrolein 125 U 15600 16700 499 533 25 10.0-160 E J5 E J5 6.66 25
Acrylonitrile 125 U 3460 3730 111 119 25 46.0-159 7.27 23
Benzene 25.0 16.7 793 820 124 129 25 34.0-147 3.37 20
Bromobenzene 25.0 U 695 716 111 115 25 51.0-137 2.95 20
Bromodichloromethane 25.0 U 694 704 111 113 25 52.0-135 1.37 20
Bromoform 25.0 U 666 664 107 106 25 50.0-146 0.320 20
Bromomethane 25.0 U 450 440 71.9 70.4 25 10.0-160 2.21 23
n-Butylbenzene 25.0 U 654 652 105 104 25 50.0-144 0.260 20
sec-Butylbenzene 25.0 U 635 633 102 101 25 48.0-143 0.290 20
tert-Butylbenzene 25.0 U 647 649 103 104 25 50.0-142 0.380 20
Carbon tetrachloride 25.0 U 719 717 115 115 25 41.0-138 0.300 20
Chlorobenzene 25.0 U 708 714 113 114 25 52.0-141 0.750 20
Chlorodibromomethane 25.0 U 675 676 108 108 25 54.0-142 0.0600 20
Chloroethane 25.0 U 389 367 62.2 58.6 25 23.0-160 5.85 20
Chloroform 25.0 U 743 758 119 121 25 50.0-139 2.02 20
Chloromethane 25.0 U 694 739 111 118 25 14.0-151 6.24 20
2-Chlorotoluene 25.0 U 705 705 113 113 25 48.0-142 0.0500 20
4-Chlorotoluene 25.0 U 678 683 108 109 25 52.0-139 0.800 20
1,2-Dibromo-3-Chloropropane 25.0 U 624 698 99.8 112 25 49.0-144 11.2 24
1,2-Dibromoethane 25.0 U 687 690 110 110 25 54.0-140 0.370 20
Dibromomethane 25.0 U 674 693 108 111 25 53.0-138 2.73 20
1,2-Dichlorobenzene 25.0 U 727 743 116 119 25 56.0-139 2.16 20
1,3-Dichlorobenzene 25.0 U 695 688 111 110 25 50.0-141 1.00 20
1,4-Dichlorobenzene 25.0 U 722 729 116 117 25 53.0-136 0.840 20
Dichlorodifluoromethane 25.0 U 948 950 152 152 25 20.0-160 0.150 21
1,1-Dichloroethane 25.0 U 748 771 120 123 25 47.0-143 3.05 20
1,2-Dichloroethane 25.0 U 675 672 108 107 25 47.0-141 0.570 20
1,1-Dichloroethene 25.0 U 781 793 125 127 25 31.0-148 1.56 20
cis-1,2-Dichloroethene 25.0 U 757 778 121 124 25 43.0-142 2.64 20
trans-1,2-Dichloroethene 25.0 U 772 767 124 123 25 36.0-141 0.730 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG964562
Volatile Organic Compounds (GC/MS) by Method 6200B-1997 L898293-01,02,03,04,05,06,07,08,09
L898388-07 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L898388-07 04/02/17 00:59 • (MS) R3207501-7 04/02/17 01:22 • (MSD) R3207501-8 04/02/17 01:45
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
1,2-Dichloropropane 25.0 U 705 743 113 119 25 51.0-141 5.34 20
1,1-Dichloropropene 25.0 U 765 784 122 125 25 42.0-146 2.38 20
1,3-Dichloropropane 25.0 U 727 741 116 119 25 58.0-139 1.88 20
2,2-Dichloropropane 25.0 U 458 462 73.3 74.0 25 43.0-139 1.00 20
Di-isopropyl ether 25.0 U 686 702 110 112 25 44.0-144 2.30 20
Ethylbenzene 25.0 281 1110 1130 133 136 25 42.0-147 1.62 20
Hexachloro-1,3-butadiene 25.0 U 640 676 102 108 25 44.0-146 5.50 21
Isopropylbenzene 25.0 12.1 698 705 110 111 25 48.0-141 1.04 20
2-Butanone (MEK)125 U 3150 3230 101 103 25 12.0-149 2.71 24
p-Isopropyltoluene 25.0 U 643 646 103 103 25 49.0-146 0.550 20
Methylene Chloride 25.0 U 709 734 113 117 25 42.0-135 3.49 20
4-Methyl-2-pentanone (MIBK)125 U 3510 3580 112 114 25 44.0-160 1.75 22
Methyl tert-butyl ether 25.0 U 715 745 114 119 25 42.0-142 4.07 20
Naphthalene 25.0 97.1 784 872 110 124 25 42.0-146 10.7 24
n-Propylbenzene 25.0 32.8 734 732 112 112 25 47.0-144 0.290 20
Styrene 25.0 U 697 682 111 109 25 47.0-147 2.18 20
1,1,1,2-Tetrachloroethane 25.0 U 681 681 109 109 25 52.0-140 0.0200 20
1,1,2,2-Tetrachloroethane 25.0 U 697 706 112 113 25 46.0-149 1.27 20
Tetrachloroethene 25.0 U 693 668 111 107 25 38.0-147 3.67 20
Toluene 25.0 34.7 767 781 117 119 25 42.0-141 1.77 20
1,2,3-Trichlorobenzene 25.0 U 671 722 107 116 25 45.0-145 7.31 22
1,2,4-Trichlorobenzene 25.0 U 678 745 109 119 25 49.0-147 9.38 21
1,1,1-Trichloroethane 25.0 U 760 730 122 117 25 46.0-140 3.92 20
1,1,2-Trichloroethane 25.0 U 722 735 116 118 25 54.0-139 1.72 20
Trichloroethene 25.0 U 702 691 112 110 25 32.0-156 1.69 20
Trichlorofluoromethane 25.0 U 804 688 129 110 25 32.0-152 15.5 20
1,2,3-Trichloropropane 25.0 U 630 640 101 102 25 54.0-143 1.64 21
1,2,4-Trimethylbenzene 25.0 243 999 1020 121 125 25 41.0-146 2.46 20
1,3,5-Trimethylbenzene 25.0 53.3 737 745 109 111 25 44.0-143 1.10 20
Vinyl chloride 25.0 U 794 719 127 115 25 24.0-153 9.97 20
o-Xylene 25.0 26.2 737 754 114 116 25 44.0-146 2.26 20
m&p-Xylenes 50.0 387 1950 1980 125 127 25 41.0-147 1.46 20
(S) Toluene-d8 102 104 80.0-120
(S) Dibromofluoromethane 108 109 76.0-123
(S) a,a,a-Trifluorotoluene 98.9 98.4 80.0-120
(S) 4-Bromofluorobenzene 100 102 80.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG965859
Volatile Organic Compounds (GC/MS) by Method 8260B L898293-10,11,12,13
Method Blank (MB)
(MB) R3207734-3 03/31/17 10:06
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acetone U 0.0100 0.0500
Acrylonitrile U 0.00179 0.0100
Benzene U 0.000270 0.00100
Bromobenzene U 0.000284 0.00100
Bromodichloromethane U 0.000254 0.00100
Bromoform U 0.000424 0.00100
Bromomethane U 0.00134 0.00500
n-Butylbenzene U 0.000258 0.00100
sec-Butylbenzene U 0.000201 0.00100
tert-Butylbenzene U 0.000206 0.00100
Carbon tetrachloride U 0.000328 0.00100
Chlorobenzene U 0.000212 0.00100
Chlorodibromomethane U 0.000373 0.00100
Chloroethane U 0.000946 0.00500
2-Chloroethyl vinyl ether U 0.00234 0.0500
Chloroform U 0.000229 0.00500
Chloromethane U 0.000375 0.00250
2-Chlorotoluene U 0.000301 0.00100
4-Chlorotoluene U 0.000240 0.00100
1,2-Dibromo-3-Chloropropane U 0.00105 0.00500
1,2-Dibromoethane U 0.000343 0.00100
Dibromomethane U 0.000382 0.00100
1,2-Dichlorobenzene U 0.000305 0.00100
1,3-Dichlorobenzene U 0.000239 0.00100
1,4-Dichlorobenzene U 0.000226 0.00100
Dichlorodifluoromethane U 0.000713 0.00500
1,1-Dichloroethane U 0.000199 0.00100
1,2-Dichloroethane U 0.000265 0.00100
1,1-Dichloroethene U 0.000303 0.00100
cis-1,2-Dichloroethene U 0.000235 0.00100
trans-1,2-Dichloroethene U 0.000264 0.00100
1,2-Dichloropropane U 0.000358 0.00100
1,1-Dichloropropene U 0.000317 0.00100
1,3-Dichloropropane U 0.000207 0.00100
cis-1,3-Dichloropropene U 0.000262 0.00100
trans-1,3-Dichloropropene U 0.000267 0.00100
2,2-Dichloropropane U 0.000279 0.00100
Di-isopropyl ether U 0.000248 0.00100
Ethylbenzene U 0.000297 0.00100
Hexachloro-1,3-butadiene U 0.000342 0.00100
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG965859
Volatile Organic Compounds (GC/MS) by Method 8260B L898293-10,11,12,13
Method Blank (MB)
(MB) R3207734-3 03/31/17 10:06
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Isopropylbenzene U 0.000243 0.00100
p-Isopropyltoluene U 0.000204 0.00100
2-Butanone (MEK)U 0.00468 0.0100
Methylene Chloride U 0.00100 0.00500
4-Methyl-2-pentanone (MIBK)U 0.00188 0.0100
Methyl tert-butyl ether U 0.000212 0.00100
Naphthalene U 0.00100 0.00500
n-Propylbenzene U 0.000206 0.00100
Styrene U 0.000234 0.00100
1,1,1,2-Tetrachloroethane U 0.000264 0.00100
1,1,2,2-Tetrachloroethane U 0.000365 0.00100
Tetrachloroethene U 0.000276 0.00100
Toluene 0.00120 J 0.000434 0.00500
1,2,3-Trichlorobenzene U 0.000306 0.00100
1,2,4-Trichlorobenzene U 0.000388 0.00100
1,1,1-Trichloroethane U 0.000286 0.00100
1,1,2-Trichloroethane U 0.000277 0.00100
Trichloroethene U 0.000279 0.00100
Trichlorofluoromethane U 0.000382 0.00500
1,2,3-Trichloropropane U 0.000741 0.00250
1,2,4-Trimethylbenzene U 0.000211 0.00100
1,3,5-Trimethylbenzene U 0.000266 0.00100
Vinyl chloride U 0.000291 0.00100
Xylenes, Total U 0.000698 0.00300
(S) Toluene-d8 95.5 80.0-120
(S) Dibromofluoromethane 89.7 74.0-131
(S) 4-Bromofluorobenzene 96.2 64.0-132
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3207734-1 03/31/17 09:06 • (LCSD) R3207734-2 03/31/17 09:26
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Acetone 0.125 0.120 0.149 96.3 119 11.0-160 21.3 23
Acrylonitrile 0.125 0.126 0.153 101 122 61.0-143 19.3 20
Benzene 0.0250 0.0207 0.0210 82.7 84.0 71.0-124 1.66 20
Bromobenzene 0.0250 0.0256 0.0255 102 102 78.0-120 0.380 20
Bromodichloromethane 0.0250 0.0239 0.0244 95.5 97.8 75.0-120 2.32 20
Bromoform 0.0250 0.0233 0.0254 93.2 102 65.0-133 8.77 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG965859
Volatile Organic Compounds (GC/MS) by Method 8260B L898293-10,11,12,13
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3207734-1 03/31/17 09:06 • (LCSD) R3207734-2 03/31/17 09:26
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Bromomethane 0.0250 0.0209 0.0212 83.6 84.9 26.0-160 1.57 20
n-Butylbenzene 0.0250 0.0281 0.0275 112 110 73.0-126 2.15 20
sec-Butylbenzene 0.0250 0.0279 0.0271 111 108 75.0-121 2.94 20
tert-Butylbenzene 0.0250 0.0254 0.0245 101 98.2 74.0-122 3.28 20
Carbon tetrachloride 0.0250 0.0207 0.0212 82.7 84.8 66.0-123 2.52 20
Chlorobenzene 0.0250 0.0277 0.0270 111 108 79.0-121 2.42 20
Chlorodibromomethane 0.0250 0.0281 0.0283 112 113 74.0-128 0.790 20
Chloroethane 0.0250 0.0215 0.0214 86.2 85.5 51.0-147 0.810 20
2-Chloroethyl vinyl ether 0.125 0.127 0.142 102 113 10.0-160 10.9 22
Chloroform 0.0250 0.0233 0.0232 93.1 92.7 73.0-123 0.450 20
Chloromethane 0.0250 0.0190 0.0192 76.2 76.7 51.0-138 0.720 20
2-Chlorotoluene 0.0250 0.0281 0.0275 112 110 72.0-124 1.95 20
4-Chlorotoluene 0.0250 0.0277 0.0272 111 109 78.0-120 2.02 20
1,2-Dibromo-3-Chloropropane 0.0250 0.0282 0.0337 113 135 65.0-126 J4 17.7 20
1,2-Dibromoethane 0.0250 0.0256 0.0270 102 108 78.0-122 5.50 20
Dibromomethane 0.0250 0.0223 0.0236 89.2 94.5 79.0-120 5.77 20
1,2-Dichlorobenzene 0.0250 0.0289 0.0292 115 117 80.0-120 1.27 20
1,3-Dichlorobenzene 0.0250 0.0272 0.0267 109 107 72.0-123 1.90 20
1,4-Dichlorobenzene 0.0250 0.0268 0.0267 107 107 77.0-120 0.420 20
Dichlorodifluoromethane 0.0250 0.0187 0.0186 74.6 74.4 49.0-155 0.340 20
1,1-Dichloroethane 0.0250 0.0243 0.0245 97.3 97.8 70.0-128 0.570 20
1,2-Dichloroethane 0.0250 0.0235 0.0242 93.9 96.8 69.0-128 3.07 20
1,1-Dichloroethene 0.0250 0.0234 0.0234 93.6 93.4 63.0-131 0.170 20
cis-1,2-Dichloroethene 0.0250 0.0240 0.0239 96.1 95.7 74.0-123 0.470 20
trans-1,2-Dichloroethene 0.0250 0.0228 0.0227 91.3 90.8 72.0-122 0.570 20
1,2-Dichloropropane 0.0250 0.0257 0.0261 103 105 75.0-126 1.52 20
1,1-Dichloropropene 0.0250 0.0242 0.0242 96.7 96.7 72.0-130 0.0600 20
1,3-Dichloropropane 0.0250 0.0267 0.0275 107 110 80.0-121 2.72 20
cis-1,3-Dichloropropene 0.0250 0.0266 0.0274 106 110 80.0-125 3.08 20
trans-1,3-Dichloropropene 0.0250 0.0265 0.0269 106 107 75.0-129 1.37 20
2,2-Dichloropropane 0.0250 0.0225 0.0232 90.2 92.8 60.0-129 2.89 20
Di-isopropyl ether 0.0250 0.0230 0.0239 92.2 95.7 62.0-133 3.79 20
Ethylbenzene 0.0250 0.0244 0.0239 97.7 95.8 77.0-120 2.03 20
Hexachloro-1,3-butadiene 0.0250 0.0295 0.0280 118 112 68.0-128 5.05 20
Isopropylbenzene 0.0250 0.0246 0.0241 98.6 96.3 75.0-120 2.30 20
p-Isopropyltoluene 0.0250 0.0289 0.0279 116 111 74.0-125 3.61 20
2-Butanone (MEK)0.125 0.134 0.172 107 138 37.0-159 J3 24.7 20
Methylene Chloride 0.0250 0.0224 0.0229 89.7 91.6 67.0-123 2.19 20
4-Methyl-2-pentanone (MIBK)0.125 0.152 0.186 122 149 60.0-144 J3 J4 20.2 20
Methyl tert-butyl ether 0.0250 0.0219 0.0239 87.5 95.6 66.0-125 8.85 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG965859
Volatile Organic Compounds (GC/MS) by Method 8260B L898293-10,11,12,13
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3207734-1 03/31/17 09:06 • (LCSD) R3207734-2 03/31/17 09:26
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Naphthalene 0.0250 0.0246 0.0264 98.4 106 64.0-125 7.21 20
n-Propylbenzene 0.0250 0.0248 0.0241 99.2 96.5 78.0-120 2.68 20
Styrene 0.0250 0.0254 0.0256 102 102 78.0-124 0.860 20
1,1,1,2-Tetrachloroethane 0.0250 0.0283 0.0278 113 111 74.0-124 1.79 20
1,1,2,2-Tetrachloroethane 0.0250 0.0245 0.0272 97.9 109 73.0-120 10.6 20
Tetrachloroethene 0.0250 0.0268 0.0260 107 104 70.0-127 2.86 20
Toluene 0.0250 0.0228 0.0231 91.1 92.3 77.0-120 1.27 20
1,2,3-Trichlorobenzene 0.0250 0.0296 0.0294 118 118 68.0-126 0.530 20
1,2,4-Trichlorobenzene 0.0250 0.0299 0.0295 120 118 70.0-127 1.31 20
1,1,1-Trichloroethane 0.0250 0.0232 0.0234 92.8 93.8 69.0-125 0.990 20
1,1,2-Trichloroethane 0.0250 0.0246 0.0250 98.4 100 78.0-120 1.77 20
Trichloroethene 0.0250 0.0252 0.0253 101 101 79.0-120 0.470 20
Trichlorofluoromethane 0.0250 0.0224 0.0229 89.7 91.5 59.0-136 1.93 20
1,2,3-Trichloropropane 0.0250 0.0272 0.0301 109 120 73.0-124 10.1 20
1,2,4-Trimethylbenzene 0.0250 0.0274 0.0271 110 108 75.0-120 1.06 20
1,3,5-Trimethylbenzene 0.0250 0.0273 0.0267 109 107 75.0-120 2.22 20
Vinyl chloride 0.0250 0.0213 0.0212 85.4 84.9 63.0-134 0.550 20
Xylenes, Total 0.0750 0.0732 0.0710 97.6 94.7 77.0-120 3.05 20
(S) Toluene-d8 95.4 96.5 80.0-120
(S) Dibromofluoromethane 92.6 92.4 74.0-131
(S) 4-Bromofluorobenzene 94.8 93.6 64.0-132
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG965361
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L898293-10,11,12,13
Method Blank (MB)
(MB) R3207229-3 03/30/17 14:44
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acenaphthene U 0.00642 0.0330
Acenaphthylene U 0.00671 0.0330
Acetophenone U 0.0752 0.333
Anthracene U 0.00632 0.0330
Atrazine U 0.0938 0.333
Benzaldehyde U 0.0532 0.333
Benzo(a)anthracene U 0.00428 0.0330
Benzo(b)fluoranthene U 0.00695 0.0330
Benzo(k)fluoranthene U 0.00582 0.0330
Benzo(g,h,i)perylene U 0.00721 0.0330
Benzo(a)pyrene U 0.00548 0.0330
Biphenyl U 0.00588 0.333
Bis(2-chlorethoxy)methane U 0.00770 0.333
Bis(2-chloroethyl)ether U 0.00896 0.333
Bis(2-chloroisopropyl)ether U 0.00760 0.333
4-Bromophenyl-phenylether U 0.0114 0.333
Caprolactam U 0.104 0.333
Carbazole U 0.00524 0.333
4-Chloroaniline U 0.0352 0.333
2-Chloronaphthalene U 0.00639 0.0330
4-Chlorophenyl-phenylether U 0.00627 0.333
Chrysene U 0.00555 0.0330
Dibenz(a,h)anthracene U 0.00821 0.0330
Dibenzofuran U 0.00518 0.333
3,3-Dichlorobenzidine U 0.0794 0.333
2,4-Dinitrotoluene U 0.00607 0.333
2,6-Dinitrotoluene U 0.00737 0.333
Fluoranthene U 0.00496 0.0330
Fluorene U 0.00682 0.0330
Hexachlorobenzene U 0.00856 0.333
Hexachloro-1,3-butadiene U 0.0100 0.333
Hexachlorocyclopentadiene U 0.0587 0.333
Hexachloroethane U 0.0134 0.333
Indeno(1,2,3-cd)pyrene U 0.00772 0.0330
Isophorone U 0.00522 0.333
2-Methylnaphthalene U 0.00861 0.0330
Naphthalene U 0.00889 0.0330
2-Nitroaniline U 0.00755 0.333
3-Nitroaniline U 0.00850 0.333
4-Nitroaniline U 0.00639 0.333
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG965361
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L898293-10,11,12,13
Method Blank (MB)
(MB) R3207229-3 03/30/17 14:44
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Nitrobenzene U 0.00695 0.333
n-Nitrosodiphenylamine U 0.00594 0.333
n-Nitrosodi-n-propylamine U 0.00906 0.333
Phenanthrene U 0.00528 0.0330
Benzylbutyl phthalate U 0.0103 0.333
Bis(2-ethylhexyl)phthalate U 0.0120 0.333
Di-n-butyl phthalate U 0.0109 0.333
Diethyl phthalate U 0.00691 0.333
Dimethyl phthalate U 0.00540 0.333
Di-n-octyl phthalate 0.0332 J 0.00907 0.333
Pyrene U 0.0123 0.0330
4-Chloro-3-methylphenol U 0.00477 0.333
2-Chlorophenol U 0.00831 0.333
2-Methylphenol U 0.00986 0.333
3&4-Methyl Phenol U 0.00783 0.333
2,4-Dichlorophenol U 0.00746 0.333
2,4-Dimethylphenol U 0.0471 0.333
4,6-Dinitro-2-methylphenol U 0.124 0.333
2,4-Dinitrophenol U 0.0980 0.333
2-Nitrophenol U 0.0130 0.333
4-Nitrophenol U 0.0525 0.333
Pentachlorophenol U 0.0480 0.333
Phenol U 0.00695 0.333
1,2,4,5-Tetrachlorobenzene U 0.0762 0.333
2,4,5-Trichlorophenol U 0.0104 0.333
2,4,6-Trichlorophenol U 0.00779 0.333
2,3,4,6-Tetrachlorophenol U 0.121 0.333
(S) Nitrobenzene-d5 59.1 18.0-125
(S) 2-Fluorobiphenyl 74.4 28.0-120
(S) p-Terphenyl-d14 92.6 13.0-131
(S) Phenol-d5 58.3 20.0-120
(S) 2-Fluorophenol 56.9 20.0-120
(S) 2,4,6-Tribromophenol 73.6 17.0-137
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG965361
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L898293-10,11,12,13
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3207229-1 03/30/17 13:54 • (LCSD) R3207229-2 03/30/17 14:19
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Acetophenone 0.667 0.464 0.377 69.5 56.5 30.0-120 20.8 26
Atrazine 0.667 0.727 0.643 109 96.4 43.0-127 12.2 22
Benzaldehyde 0.667 0.165 0.124 24.8 18.6 10.0-120 28.7 40
Acenaphthene 0.667 0.609 0.520 91.2 77.9 47.0-120 15.7 21
Acenaphthylene 0.667 0.648 0.560 97.1 83.9 48.0-120 14.6 21
Anthracene 0.667 0.620 0.543 93.0 81.4 46.0-120 13.2 20
Biphenyl 0.667 0.596 0.511 89.3 76.7 42.0-120 15.2 23
Benzo(a)anthracene 0.667 0.617 0.551 92.4 82.6 46.0-120 11.2 20
Benzo(b)fluoranthene 0.667 0.621 0.556 93.1 83.4 45.0-120 11.0 22
Benzo(k)fluoranthene 0.667 0.603 0.546 90.4 81.8 45.0-120 9.96 23
Caprolactam 0.667 0.649 0.572 97.3 85.8 41.0-136 12.6 22
Benzo(g,h,i)perylene 0.667 0.728 0.578 109 86.7 48.0-120 J3 22.9 21
Carbazole 0.667 0.604 0.535 90.5 80.2 41.0-120 12.0 20
4-Chloroaniline 0.667 0.408 0.338 61.1 50.7 27.0-120 18.6 25
Benzo(a)pyrene 0.667 0.641 0.565 96.1 84.7 46.0-120 12.6 21
Bis(2-chlorethoxy)methane 0.667 0.454 0.394 68.1 59.1 41.0-120 14.2 22
Bis(2-chloroethyl)ether 0.667 0.469 0.365 70.3 54.7 28.0-120 25.1 28
Bis(2-chloroisopropyl)ether 0.667 0.542 0.421 81.2 63.1 40.0-120 25.1 27
4-Bromophenyl-phenylether 0.667 0.609 0.544 91.3 81.6 45.0-120 11.2 20
Dibenzofuran 0.667 0.618 0.539 92.7 80.7 43.0-120 13.7 21
2-Chloronaphthalene 0.667 0.589 0.513 88.3 76.9 43.0-120 13.7 22
4-Chlorophenyl-phenylether 0.667 0.626 0.553 93.9 82.9 46.0-120 12.4 21
Chrysene 0.667 0.619 0.548 92.7 82.1 46.0-120 12.2 20
Dibenz(a,h)anthracene 0.667 0.725 0.582 109 87.3 47.0-120 21.8 22
3,3-Dichlorobenzidine 0.667 0.750 0.669 113 100 20.0-130 11.4 24
2,4-Dinitrotoluene 0.667 0.678 0.602 102 90.3 48.0-122 11.9 21
2,6-Dinitrotoluene 0.667 0.639 0.554 95.9 83.1 46.0-120 14.3 21
Fluoranthene 0.667 0.628 0.556 94.1 83.4 46.0-120 12.0 20
2-Methylnaphthalene 0.667 0.466 0.399 69.9 59.8 43.0-120 15.6 22
Fluorene 0.667 0.629 0.545 94.3 81.7 47.0-120 14.2 20
Hexachlorobenzene 0.667 0.611 0.535 91.6 80.3 42.0-120 13.2 20
2-Nitroaniline 0.667 0.662 0.574 99.2 86.1 46.0-125 14.2 21
Hexachloro-1,3-butadiene 0.667 0.485 0.399 72.7 59.9 36.0-120 19.2 26
3-Nitroaniline 0.667 0.591 0.515 88.6 77.2 37.0-120 13.7 22
Hexachlorocyclopentadiene 0.667 0.639 0.541 95.8 81.0 20.0-124 16.8 26
4-Nitroaniline 0.667 0.618 0.559 92.7 83.8 31.0-127 10.1 26
Hexachloroethane 0.667 0.498 0.380 74.7 57.0 32.0-120 27.0 31
Indeno(1,2,3-cd)pyrene 0.667 0.706 0.564 106 84.5 48.0-120 J3 22.4 21
Isophorone 0.667 0.480 0.418 72.0 62.6 42.0-120 14.0 21
Naphthalene 0.667 0.439 0.370 65.8 55.5 41.0-120 16.9 24
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG965361
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L898293-10,11,12,13
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3207229-1 03/30/17 13:54 • (LCSD) R3207229-2 03/30/17 14:19
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Nitrobenzene 0.667 0.432 0.359 64.8 53.8 36.0-120 18.6 24
n-Nitrosodiphenylamine 0.667 0.570 0.496 85.5 74.3 42.0-120 13.9 20
n-Nitrosodi-n-propylamine 0.667 0.520 0.434 77.9 65.0 39.0-120 18.0 23
Phenanthrene 0.667 0.605 0.529 90.7 79.3 45.0-120 13.4 20
Benzylbutyl phthalate 0.667 0.607 0.544 91.0 81.6 41.0-123 10.9 20
Bis(2-ethylhexyl)phthalate 0.667 0.650 0.570 97.5 85.5 41.0-124 13.1 20
Di-n-butyl phthalate 0.667 0.633 0.564 94.8 84.6 44.0-120 11.4 20
Diethyl phthalate 0.667 0.656 0.584 98.4 87.5 46.0-120 11.7 20
Dimethyl phthalate 0.667 0.651 0.579 97.6 86.8 47.0-120 11.7 21
2-Methylphenol 0.667 0.507 0.417 76.1 62.6 41.0-120 19.5 24
Di-n-octyl phthalate 0.667 0.639 0.563 95.9 84.4 40.0-123 12.7 21
3&4-Methyl Phenol 0.667 0.607 0.500 91.0 74.9 47.0-120 19.4 24
Pyrene 0.667 0.598 0.511 89.7 76.6 45.0-120 15.8 21
4-Chloro-3-methylphenol 0.667 0.498 0.433 74.7 64.9 46.0-120 14.0 20
2-Chlorophenol 0.667 0.519 0.408 77.9 61.2 37.0-120 23.9 27
1,2,4,5-Tetrachlorobenzene 0.667 0.712 0.622 107 93.2 40.0-120 13.5 23
2,4-Dichlorophenol 0.667 0.512 0.432 76.8 64.8 45.0-120 16.9 21
2,4,5-Trichlorophenol 0.667 0.625 0.532 93.7 79.7 44.0-120 16.1 22
2,4-Dimethylphenol 0.667 0.449 0.392 67.3 58.8 40.0-120 13.6 22
4,6-Dinitro-2-methylphenol 0.667 0.574 0.500 86.1 74.9 34.0-120 13.8 23
2,4-Dinitrophenol 0.667 0.327 0.289 49.0 43.3 10.0-120 12.4 30
2-Nitrophenol 0.667 0.511 0.419 76.6 62.8 42.0-120 19.8 24
4-Nitrophenol 0.667 0.590 0.518 88.5 77.7 40.0-120 13.0 21
Pentachlorophenol 0.667 0.547 0.481 82.0 72.1 33.0-122 12.8 22
Phenol 0.667 0.520 0.421 78.0 63.2 38.0-120 21.0 25
2,4,6-Trichlorophenol 0.667 0.653 0.559 98.0 83.7 47.0-120 15.7 22
(S) Nitrobenzene-d5 68.6 56.8 18.0-125
(S) 2-Fluorobiphenyl 93.2 78.8 28.0-120
(S) p-Terphenyl-d14 100 86.5 13.0-131
(S) Phenol-d5 79.9 64.0 20.0-120
(S) 2-Fluorophenol 80.3 59.8 20.0-120
(S) 2,4,6-Tribromophenol 95.9 81.2 17.0-137
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG965361
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L898293-10,11,12,13
L898186-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L898186-01 03/31/17 09:18 • (MS) R3207352-1 03/31/17 09:43 • (MSD) R3207352-2 03/31/17 10:09
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Acetophenone 0.744 ND 0.494 0.464 66.5 62.3 1 24.0-120 6.44 21
Atrazine 0.744 ND 0.667 0.639 89.6 86.0 1 42.0-126 4.19 21
Benzaldehyde 0.744 ND 0.313 0.303 42.1 40.7 1 10.0-126 3.22 32
Biphenyl 0.744 ND 0.581 0.572 78.1 76.9 1 37.0-120 1.49 21
Acenaphthene 0.744 ND 0.576 0.582 77.5 78.3 1 37.0-120 0.960 23
Acenaphthylene 0.744 ND 0.604 0.607 81.2 81.6 1 41.0-120 0.420 22
Caprolactam 0.744 ND 0.671 0.657 90.2 88.4 1 27.0-151 2.03 22
Carbazole 0.744 ND 0.613 0.580 82.4 78.0 1 38.0-120 5.49 21
4-Chloroaniline 0.744 ND 0.392 0.376 52.7 50.6 1 21.0-120 4.16 27
Anthracene 0.744 ND 0.585 0.581 78.6 78.1 1 30.0-123 0.680 25
Dibenzofuran 0.744 ND 0.575 0.583 77.3 78.3 1 30.0-120 1.26 22
Benzo(a)anthracene 0.744 ND 0.568 0.546 76.4 73.4 1 21.0-123 4.05 26
Benzo(b)fluoranthene 0.744 ND 0.691 0.679 92.8 91.3 1 20.0-127 1.69 29
Benzo(k)fluoranthene 0.744 ND 0.651 0.716 87.5 96.3 1 22.0-123 9.56 28
Benzo(g,h,i)perylene 0.744 ND 0.257 0.186 34.5 25.0 1 10.0-120 J3 32.1 32
Benzo(a)pyrene 0.744 ND 0.615 0.584 82.7 78.5 1 23.0-120 5.25 27
Bis(2-chlorethoxy)methane 0.744 ND 0.440 0.445 59.2 59.9 1 37.0-120 1.14 22
Bis(2-chloroethyl)ether 0.744 ND 0.520 0.475 69.9 63.9 1 26.0-120 9.01 27
Bis(2-chloroisopropyl)ether 0.744 ND 0.571 0.538 76.8 72.4 1 35.0-120 5.87 25
4-Bromophenyl-phenylether 0.744 ND 0.563 0.544 75.6 73.1 1 34.0-120 3.39 23
2-Chloronaphthalene 0.744 ND 0.564 0.541 75.9 72.8 1 40.0-120 4.17 22
4-Chlorophenyl-phenylether 0.744 ND 0.554 0.544 74.5 73.1 1 37.0-120 1.95 23
2-Methylnaphthalene 0.744 ND 0.432 0.433 58.1 58.2 1 35.0-120 0.210 23
Chrysene 0.744 ND 0.568 0.543 76.4 73.0 1 19.0-127 4.56 27
Dibenz(a,h)anthracene 0.744 ND 0.318 0.248 42.8 33.4 1 10.0-120 24.7 28
2-Nitroaniline 0.744 ND 0.634 0.646 85.3 86.8 1 42.0-125 1.76 22
3-Nitroaniline 0.744 ND 0.504 0.479 67.8 64.4 1 29.0-120 5.10 25
4-Nitroaniline 0.744 ND 0.828 0.731 111 98.3 1 27.0-130 12.4 27
3,3-Dichlorobenzidine 0.744 ND 0.793 0.583 107 78.4 1 10.0-142 J3 30.5 30
2,4-Dinitrotoluene 0.744 ND 0.633 0.632 85.2 85.0 1 37.0-129 0.180 24
2,6-Dinitrotoluene 0.744 ND 0.569 0.563 76.5 75.7 1 40.0-120 1.02 23
Fluoranthene 0.744 ND 0.624 0.579 84.0 77.8 1 20.0-133 7.58 28
Fluorene 0.744 ND 0.590 0.586 79.4 78.7 1 35.0-120 0.810 23
Hexachlorobenzene 0.744 ND 0.531 0.515 71.4 69.2 1 33.0-120 3.12 24
Hexachloro-1,3-butadiene 0.744 ND 0.417 0.405 56.1 54.4 1 33.0-120 3.07 25
Hexachlorocyclopentadiene 0.744 ND ND ND 0.000 0.000 1 10.0-120 J6 J6 0.000 33
Hexachloroethane 0.744 ND 0.450 0.409 60.5 55.0 1 21.0-120 9.60 30
Indeno(1,2,3-cd)pyrene 0.744 ND 0.318 0.243 42.8 32.6 1 10.0-120 27.0 30
Isophorone 0.744 ND 0.453 0.455 60.9 61.2 1 38.0-120 0.340 22
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Excel Civil & Environmental Associates 24090 L898293 04/07/17 10:15 57 of 62
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG965361
Semi Volatile Organic Compounds (GC/MS) by Method 8270D L898293-10,11,12,13
L898186-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L898186-01 03/31/17 09:18 • (MS) R3207352-1 03/31/17 09:43 • (MSD) R3207352-2 03/31/17 10:09
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Naphthalene 0.744 ND 0.450 0.437 60.5 58.8 1 37.0-120 2.88 25
2-Methylphenol 0.744 ND 0.530 0.504 71.2 67.8 1 34.0-120 4.89 26
Nitrobenzene 0.744 ND 0.438 0.430 58.9 57.9 1 32.0-120 1.84 24
3&4-Methyl Phenol 0.744 ND 0.586 0.567 78.8 76.2 1 35.0-120 3.33 25
n-Nitrosodiphenylamine 0.744 ND 0.528 0.531 71.0 71.4 1 20.0-125 0.670 25
n-Nitrosodi-n-propylamine 0.744 ND 0.541 0.527 72.7 70.9 1 34.0-120 2.56 23
Phenanthrene 0.744 ND 0.579 0.565 77.8 75.9 1 24.0-124 2.42 25
Benzylbutyl phthalate 0.744 ND 0.585 0.610 78.6 82.1 1 18.0-130 4.24 27
Bis(2-ethylhexyl)phthalate 0.744 ND 0.597 0.612 78.1 80.2 1 19.0-127 2.56 28
Di-n-butyl phthalate 0.744 ND 0.585 0.563 78.6 75.6 1 29.0-120 3.84 26
Diethyl phthalate 0.744 ND 0.596 0.607 80.1 81.6 1 42.0-121 1.83 23
Dimethyl phthalate 0.744 ND 0.586 0.576 78.9 77.4 1 42.0-120 1.80 23
1,2,4,5-Tetrachlorobenzene 0.744 ND 0.587 0.582 79.0 78.3 1 40.0-120 0.870 22
Di-n-octyl phthalate 0.744 ND 0.596 0.592 80.2 79.6 1 21.0-122 0.660 27
2,4,5-Trichlorophenol 0.744 ND 0.578 0.580 77.7 77.9 1 40.0-126 0.250 24
Pyrene 0.744 ND 0.542 0.566 72.9 76.1 1 19.0-127 4.23 29
4-Chloro-3-methylphenol 0.744 ND 0.465 0.481 62.5 64.6 1 37.0-121 3.34 23
2-Chlorophenol 0.744 ND 0.575 0.522 77.3 70.2 1 34.0-120 9.56 25
2,4-Dichlorophenol 0.744 ND 0.465 0.484 62.5 65.1 1 41.0-120 4.09 22
2,4-Dimethylphenol 0.744 ND 0.425 0.396 57.2 53.2 1 27.0-120 7.20 25
4,6-Dinitro-2-methylphenol 0.744 ND 0.433 0.343 58.2 46.1 1 10.0-131 23.2 29
2,4-Dinitrophenol 0.744 ND 0.118 ND 15.9 0.000 1 10.0-142 J3 J6 200 30
2-Nitrophenol 0.744 ND 0.454 0.446 61.1 60.0 1 34.0-124 1.84 27
4-Nitrophenol 0.744 ND 0.666 0.659 89.6 88.6 1 26.0-133 1.08 25
Pentachlorophenol 0.744 ND 0.486 0.465 65.3 62.6 1 15.0-152 4.30 26
Phenol 0.744 ND 0.558 0.526 75.0 70.7 1 33.0-120 5.90 24
2,4,6-Trichlorophenol 0.744 ND 0.595 0.612 79.9 82.2 1 40.0-125 2.84 24
(S) Nitrobenzene-d5 60.7 59.2 18.0-125
(S) 2-Fluorobiphenyl 75.4 74.9 28.0-120
(S) p-Terphenyl-d14 74.5 74.2 13.0-131
(S) Phenol-d5 75.5 73.7 20.0-120
(S) 2-Fluorophenol 80.3 72.1 20.0-120
(S) 2,4,6-Tribromophenol 74.3 72.9 17.0-137
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.GLOSSARY OF TERMS
Abbreviations and Definitions
SDG Sample Delivery Group.
MDL Method Detection Limit.
RDL Reported Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
U Not detected at the Reporting Limit (or MDL where applicable).
RPD Relative Percent Difference.
(dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry
report basis for soils].
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD)
from a quality control sample. The Original Sample may not be included within the reported SDG.
(S)Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control
Sample/Duplicate and Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring
recovery. Surrogates are not expected to be detected in all environmental media.
Rec.Recovery.
Qualifier Description
B The same analyte is found in the associated blank.
E The analyte concentration exceeds the upper limit of the calibration range of the instrument
established by the initial calibration (ICAL).
J The identification of the analyte is acceptable; the reported value is an estimate.
J1 Surrogate recovery limits have been exceeded; values are outside upper control limits.
J3 The associated batch QC was outside the established quality control range for precision.
J4 The associated batch QC was outside the established quality control range for accuracy.
J5 The sample matrix interfered with the ability to make any accurate determination; spike value is
high.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is
low.
J7 Surrogate recovery cannot be used for control limit evaluation due to dilution.
V3 The internal standard exhibited poor recovery due to sample matrix interference. The analytical
results will be biased high. BDL results will be unaffected.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.ACCREDITATIONS & LOCATIONS
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Our Locations
Alabama 40660
Alaska UST-080
Arizona AZ0612
Arkansas 88-0469
California 01157CA
Colorado TN00003
Conneticut PH-0197
Florida E87487
Georgia NELAP
Georgia 1 923
Idaho TN00003
Illinois 200008
Indiana C-TN-01
Iowa 364
Kansas E-10277
Kentucky 1 90010
Kentucky 2 16
Louisiana AI30792
Maine TN0002
Maryland 324
Massachusetts M-TN003
Michigan 9958
Minnesota 047-999-395
Mississippi TN00003
Missouri 340
Montana CERT0086
Nebraska NE-OS-15-05
Nevada TN-03-2002-34
New Hampshire 2975
New Jersey–NELAP TN002
New Mexico TN00003
New York 11742
North Carolina Env375
North Carolina 1 DW21704
North Carolina 2 41
North Dakota R-140
Ohio–VAP CL0069
Oklahoma 9915
Oregon TN200002
Pennsylvania 68-02979
Rhode Island 221
South Carolina 84004
South Dakota n/a
Tennessee 1 4 2006
Texas T 104704245-07-TX
Texas 5 LAB0152
A2LA – ISO 17025 1461.01
Canada 1461.01
EPA–Crypto TN00003
State Accreditations
Third Party & Federal Accreditations
ESC Lab Sciences is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other
lab is as accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the
network laboratories in our industry. The most significant benefit to our “one location” design is the design of our laboratory campus. The model is conducive to accelerated productivity,
decreasing turn-around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
ESC Lab Sciences has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please
contact our main office. ESC Lab Sciences performs all testing at our central laboratory.
1. Drinking Water 2. Underground Storage Tanks 3. Aquatic Toxicity 4.
Utah 6157585858
Vermont VT2006
Virginia 109
Washington C1915
West Virginia 233
Wisconsin 9980939910
Wyoming A2LA
AIHA-LAP,LLC 100789
DOD 1461.01
USDA S-67674
Chemical/Microbiological 5. Mold n/a Accreditation not applicable
1461.02A2LA – ISO 170255
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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APPENDIX C -MAINTENANCE FORMS
EXCel CIVil & ENVIRONMENTAL ASSOCIATES, PLLC
www.excelengr.com
SCHEDULED/NON-SCHEDULED SYSTEM MAINTENANCE CHECKLIST
Incident Name I Incident Number Date Maintenance Perlonned
SERVCO Winston Salem 20966 March 24, 2017
rield Personnel Name(s) Time Arrived I Time Departed
M. Stanforth Job 24090 830 1330
ACTIVITIES PERFORMIW TIME SPENT
(List Separately) (List in Vi I lour Increments)
The SVE system was down at arrival, the FP system down pending repairs;
Met with electrician -replaced compressor and timer relay
Oil levels were checked in the SVE components, all levels were
found to be normal; SVE system restarted
The system was evaluated, readings were collected, adjustments were made
as necessary and free product levels collected;
The system was operational at departure.
ON-SITE MAINTENANCE TIME TOTAL 5-hrs
3/24/17
rield Personnel Signature Date
Note:
Travel time should not be included in yollt' breakdown of system maintenance activities.
The information required in this form represents the minimum amount of information ncccssnry to justify maintenance
activities conducted. If the required information is not included on the form or in another document, the State Trust Fund will
not be able to reimburse system maintenance activities. Plcase refer to the scope ofwark for guidam:c on \vhich activities are
considered scheduled/non-scheduled maintenance.
TF ·607C (4/510 I)
APPENDIX D -PUBLIC NOTICE NOTIFICATIONS
EXCEL CiVil & ENVIRONMENTAL ASSOCIATES, PllC
www.excelengr.com
Donna Farris
From:
Sent:
To:
Subject:
Attachments:
Donna Farri s <[e-mail]>
Wednesday, April 04, 2012 12:18 PM
Estkowski, Linda ([e-mail])
Servco 01711 Winston-Salem Inciden t 20966
Return Cert Mail Receipts.pdf
Attached are the return receipts for the notices mailed related to the Corrective Action Plan forwarded to you recently
for the referenced site.
Thank you,
Donna Farris
Excel Civil & Environmental Associates, PLLC
625 Huntsman Court, Gastonia, NC 28054
Ph: 704-853-0800
Fax: [phone]
www.excelengr.com
... 4 Please consider the environment before printing this e-mail.
'The problems we face cannot be solved at the same level of thinking with which we created them. ". Albert Einstein
CONFIDENTIALITY NOTICE: The information in this e-mail is confidential. ft is intended so/ely for the addressee. Access to this a-mail by anyone else
is unauthorized. If you are not the intended recipient, any disclosure, copying, distribution or any action taken or omitted to be taken in reliance on it, is
prohibited and may be unlawful. When addressed to our clients, any opinions or advice contained in this e-mail are subject to the terms and conditions
expressed in the governing ECEA client engagement fetter.
Donna Farris
From:
Sent:
Donna Farri s <[e-mail]>
Thursday, Janu ary 07, 2016 10:10 AM
To: Mike Stanforth (mstanforth@exce lengr.com)
Subject:
Attachments:
FW: Servco 01711 Winston-Sa lem Incident 20966
Return Recei pts 7.B.pdf
From: Donna Farri s [mailto:[e-mail]]
Sent: Tues day, July 02, 2013 1:52 PM
To: thomas.moore@ ncdenr.gov
Subject: Servco 01711 Winston-Salem Incident 20966
Attached are copies of the return receipts for the public notices previously mailed to you for the referenced site.
Thank you,
Donna Farris
Excel Civil & Environmental Associates, PLLC
625 Huntsman Court, Gastonia, NC 28054
Ph : 704-853-0800
Fax: [phone]
www.excelengr.com
j..4 Please consider the environment before printing this e·mail.
'The problems we face cannot be solved at the same level 0/ thinking with which we created them. ". Albert Einstein
CONFIDENTIALITY NOTICE: The information in this e-mail is confidential. It is intended solely for the addressee. Access to this a-mail by anyone else
is unauthorized. If you are not the intended recipient, any disclosure, copying, distribution or any action taken or omitted to be taken in reliance on it, is
prohibited and may be unlawful. When addressed to our clients, any opinions or advice contained in this e-mail are subject to the terms and conditions
expressed in the governing ECEA client engagement fetter.
1