WS-4752_15492_CA_LAB_20191120

SHEALY ENVIRONMENTAL SERVICES,INC.
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced,except in its entirety,without the written approval of Shealy Environmental Services,Inc.
Shealy Environmental Services,Inc.
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax [phone] www.shealylab.com
Report of Analysis
DEQ DWM
217 West Jones St.
Raleigh,NC 27603
Attention:Linda Estlowski
Project Name:Steelmain's Fabric Shop
Project Number:15492
Lot Number:UK07086
Date Completed:11/20/2019
11/20/2019 4:26 PM
Approved and released by:
Project Manager:Nisreen Saikaly
Page 1 of 28
SHEALY ENVIRONMENTAL SERVICES,INC.
SC DHEC No:32010001 NELAC No:E87653 NC DENR No:329 NC Field Parameters No:5639
Shealy Environmental Services,Inc.
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax [phone] www.shealylab.com
Case Narrative
DEQ DWM
Lot Number:UK07086
This Report of Analysis contains the analytical result(s)for the sample(s)listed on the Sample Summary
following this Case Narrative.The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt,sample analysis,and data review have been performed in accordance with the most
current approved NELAC standards,the Shealy Environmental Services,Inc.("Shealy")Quality
Assurance Management Plan (QAMP),standard operating procedures (SOPs),and Shealy policies.Any
exceptions to the NELAC standards,the QAMP,SOPs or policies are qualified on the results page or
discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the
cover page.
Page 2 of 28
SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
DEQ DWM
Lot Number: UK07086

Sample Number Sample ID Matrix Date Sampled Date Received
001 11/06/2019 0900Trip Blank Aqueous 11/07/2019
002 11/06/2019 113010205 US 421S/Green Aqueous 11/07/2019
003 11/06/2019 1040186 Howard Steelman Dr/Style Aqueous 11/07/2019
004 11/06/2019 1045212 Howard Steelman Dr/McNeil Aqueous 11/07/2019
005 11/06/2019 1145132 VL Moretz Rd/Duke Aqueous 11/07/2019
006 11/06/2019 1055212 Howard Steelman-before filter Aqueous 11/07/2019
007 11/06/2019 1200161 VL Moretz Aqueous 11/07/2019
(7 samples)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 3 of 28
SHEALY ENVIRONMENTAL SERVICES, INC.
Detection Summary
DEQ DWM
Lot Number: UK07086

Sample Sample ID Matrix Parameter Method Result Q Units Page
001 Trip Blank Aqueous 1,4-Dichlorobenzene SM 6200B-0.87 ug/L 5
(1 detection)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 4 of 28
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
DEQ DWM
Trip Blank
UK07086-001
11/06/2019 0900
11/07/2019
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 1 11/14/2019 1031 TML 35674
2 SM 6200B-SM 6200B-2011 1 11/15/2019 2319 JTH 35945
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
Benzene 71-43-2 SM 6200B-ND 1ug/L0.50
Bromobenzene 108-86-1 SM 6200B-ND 1ug/L0.50
Bromochloromethane 74-97-5 SM 6200B-ND 1ug/L0.50
Bromodichloromethane 75-27-4 SM 6200B-ND 1ug/L0.50
Bromoform 75-25-2 SM 6200B-ND 1ug/L0.50
Bromomethane (Methyl bromide)74-83-9 SM 6200B-ND 1ug/L0.50
n-Butylbenzene 104-51-8 SM 6200B-ND 1ug/L0.50
sec-Butylbenzene 135-98-8 SM 6200B-ND 1ug/L0.50
tert-Butylbenzene 98-06-6 SM 6200B-ND 1ug/L0.50
Carbon tetrachloride 56-23-5 SM 6200B-ND 1ug/L0.50
Chlorobenzene 108-90-7 SM 6200B-ND 1ug/L0.50
Chloroethane 75-00-3 SM 6200B-ND 1ug/L0.50
Chloroform 67-66-3 SM 6200B-ND 1ug/L0.50
Chloromethane (Methyl chloride)74-87-3 SM 6200B-ND 1ug/L0.50
2-Chlorotoluene 95-49-8 SM 6200B-ND 1ug/L0.50
4-Chlorotoluene 106-43-4 SM 6200B-ND 1ug/L0.50
Dibromochloromethane 124-48-1 SM 6200B-ND 1ug/L0.50
1,2-Dibromoethane (EDB)106-93-4 SM 6200B-ND 1ug/L0.50
Dibromomethane (Methylene bromide)74-95-3 SM 6200B-ND 1ug/L0.50
1,2-Dichlorobenzene 95-50-1 SM 6200B-ND 1ug/L0.50
1,3-Dichlorobenzene 541-73-1 SM 6200B-ND 1ug/L0.50
1,4-Dichlorobenzene 106-46-7 SM 6200B-0.87 2ug/L0.50
Dichlorodifluoromethane 75-71-8 SM 6200B-ND 1ug/L0.50
1,1-Dichloroethane 75-34-3 SM 6200B-ND 1ug/L0.50
1,2-Dichloroethane 107-06-2 SM 6200B-ND 1ug/L0.50
1,1-Dichloroethene 75-35-4 SM 6200B-ND 1ug/L0.50
cis-1,2-Dichloroethene 156-59-2 SM 6200B-ND 1ug/L0.50
trans-1,2-Dichloroethene 156-60-5 SM 6200B-ND 1ug/L0.50
1,2-Dichloropropane 78-87-5 SM 6200B-ND 1ug/L0.50
1,3-Dichloropropane 142-28-9 SM 6200B-ND 1ug/L0.50
2,2-Dichloropropane 594-20-7 SM 6200B-ND 1ug/L0.50
1,1-Dichloropropene 563-58-6 SM 6200B-ND 1ug/L0.50
cis-1,3-Dichloropropene 10061-01-5 SM 6200B-ND 1ug/L0.50
trans-1,3-Dichloropropene 10061-02-6 SM 6200B-ND 1ug/L0.50
Diisopropyl ether (IPE)108-20-3 SM 6200B-ND 1ug/L0.50
Ethylbenzene 100-41-4 SM 6200B-ND 1ug/L0.50
Hexachlorobutadiene 87-68-3 SM 6200B-ND 1ug/L0.50
Isopropylbenzene (Cumene)98-82-8 SM 6200B-ND 1ug/L0.50
p-Isopropyltoluene (p-Cymene)99-87-6 SM 6200B-ND 1ug/L0.50
Methyl tertiary butyl ether (MTBE)1634-04-4 SM 6200B-ND 1ug/L0.50
Methylene chloride 75-09-2 SM 6200B-ND 1ug/L0.50
Naphthalene 91-20-3 SM 6200B-ND 1ug/L0.50
n-Propylbenzene 103-65-1 SM 6200B-ND 1ug/L0.50
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 5 of 28
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
DEQ DWM
Trip Blank
UK07086-001
11/06/2019 0900
11/07/2019
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 1 11/14/2019 1031 TML 35674
2 SM 6200B-SM 6200B-2011 1 11/15/2019 2319 JTH 35945
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
Styrene 100-42-5 SM 6200B-ND 1ug/L0.50
1,1,1,2-Tetrachloroethane 630-20-6 SM 6200B-ND 1ug/L0.50
1,1,2,2-Tetrachloroethane 79-34-5 SM 6200B-ND 1ug/L0.50
Tetrachloroethene 127-18-4 SM 6200B-ND 1ug/L0.50
Toluene 108-88-3 SM 6200B-ND 1ug/L0.50
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 SM 6200B-ND 1ug/L0.50
1,2,3-Trichlorobenzene 87-61-6 SM 6200B-ND 1ug/L0.50
1,2,4-Trichlorobenzene 120-82-1 SM 6200B-ND 1ug/L0.50
1,1,1-Trichloroethane 71-55-6 SM 6200B-ND 1ug/L0.50
1,1,2-Trichloroethane 79-00-5 SM 6200B-ND 1ug/L0.50
Trichloroethene 79-01-6 SM 6200B-ND 1ug/L0.50
Trichlorofluoromethane 75-69-4 SM 6200B-ND 1ug/L0.50
1,2,3-Trichloropropane 96-18-4 SM 6200B-ND 1ug/L0.50
1,3,5-Trimethylbenzene (Mesitylene)108-67-8 SM 6200B-ND 1ug/L0.50
1,2,4-Trimethylbenzene 95-63-6 SM 6200B-ND 1ug/L0.50
Vinyl chloride 75-01-4 SM 6200B-ND 1ug/L0.50
m+p - Xylenes 179601-23-1 SM 6200B-ND 1ug/L0.50
o - Xylenes 95-47-6 SM 6200B-ND 1ug/L0.50
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
1,2-Dichloroethane-d4 100 70-130 109 70-130
Bromofluorobenzene 94 70-130 88 70-130
Toluene-d8 101 70-130 100 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 6 of 28
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
DEQ DWM
10205 US 421S/Green
UK07086-002
11/06/2019 1130
11/07/2019
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 1 11/14/2019 1055 TML 35674
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
Benzene 71-43-2 SM 6200B-ND 1ug/L0.50
Bromobenzene 108-86-1 SM 6200B-ND 1ug/L0.50
Bromochloromethane 74-97-5 SM 6200B-ND 1ug/L0.50
Bromodichloromethane 75-27-4 SM 6200B-ND 1ug/L0.50
Bromoform 75-25-2 SM 6200B-ND 1ug/L0.50
Bromomethane (Methyl bromide)74-83-9 SM 6200B-ND 1ug/L0.50
n-Butylbenzene 104-51-8 SM 6200B-ND 1ug/L0.50
sec-Butylbenzene 135-98-8 SM 6200B-ND 1ug/L0.50
tert-Butylbenzene 98-06-6 SM 6200B-ND 1ug/L0.50
Carbon tetrachloride 56-23-5 SM 6200B-ND 1ug/L0.50
Chlorobenzene 108-90-7 SM 6200B-ND 1ug/L0.50
Chloroethane 75-00-3 SM 6200B-ND 1ug/L0.50
Chloroform 67-66-3 SM 6200B-ND 1ug/L0.50
Chloromethane (Methyl chloride)74-87-3 SM 6200B-ND 1ug/L0.50
2-Chlorotoluene 95-49-8 SM 6200B-ND 1ug/L0.50
4-Chlorotoluene 106-43-4 SM 6200B-ND 1ug/L0.50
Dibromochloromethane 124-48-1 SM 6200B-ND 1ug/L0.50
1,2-Dibromoethane (EDB)106-93-4 SM 6200B-ND 1ug/L0.50
Dibromomethane (Methylene bromide)74-95-3 SM 6200B-ND 1ug/L0.50
1,2-Dichlorobenzene 95-50-1 SM 6200B-ND 1ug/L0.50
1,3-Dichlorobenzene 541-73-1 SM 6200B-ND 1ug/L0.50
1,4-Dichlorobenzene 106-46-7 SM 6200B-ND 1ug/L0.50
Dichlorodifluoromethane 75-71-8 SM 6200B-ND 1ug/L0.50
1,1-Dichloroethane 75-34-3 SM 6200B-ND 1ug/L0.50
1,2-Dichloroethane 107-06-2 SM 6200B-ND 1ug/L0.50
1,1-Dichloroethene 75-35-4 SM 6200B-ND 1ug/L0.50
cis-1,2-Dichloroethene 156-59-2 SM 6200B-ND 1ug/L0.50
trans-1,2-Dichloroethene 156-60-5 SM 6200B-ND 1ug/L0.50
1,2-Dichloropropane 78-87-5 SM 6200B-ND 1ug/L0.50
1,3-Dichloropropane 142-28-9 SM 6200B-ND 1ug/L0.50
2,2-Dichloropropane 594-20-7 SM 6200B-ND 1ug/L0.50
1,1-Dichloropropene 563-58-6 SM 6200B-ND 1ug/L0.50
cis-1,3-Dichloropropene 10061-01-5 SM 6200B-ND 1ug/L0.50
trans-1,3-Dichloropropene 10061-02-6 SM 6200B-ND 1ug/L0.50
Diisopropyl ether (IPE)108-20-3 SM 6200B-ND 1ug/L0.50
Ethylbenzene 100-41-4 SM 6200B-ND 1ug/L0.50
Hexachlorobutadiene 87-68-3 SM 6200B-ND 1ug/L0.50
Isopropylbenzene (Cumene)98-82-8 SM 6200B-ND 1ug/L0.50
p-Isopropyltoluene (p-Cymene)99-87-6 SM 6200B-ND 1ug/L0.50
Methyl tertiary butyl ether (MTBE)1634-04-4 SM 6200B-ND 1ug/L0.50
Methylene chloride 75-09-2 SM 6200B-ND 1ug/L0.50
Naphthalene 91-20-3 SM 6200B-ND 1ug/L0.50
n-Propylbenzene 103-65-1 SM 6200B-ND 1ug/L0.50
Styrene 100-42-5 SM 6200B-ND 1ug/L0.50
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 7 of 28
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
DEQ DWM
10205 US 421S/Green
UK07086-002
11/06/2019 1130
11/07/2019
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 1 11/14/2019 1055 TML 35674
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
1,1,1,2-Tetrachloroethane 630-20-6 SM 6200B-ND 1ug/L0.50
1,1,2,2-Tetrachloroethane 79-34-5 SM 6200B-ND 1ug/L0.50
Tetrachloroethene 127-18-4 SM 6200B-ND 1ug/L0.50
Toluene 108-88-3 SM 6200B-ND 1ug/L0.50
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 SM 6200B-ND 1ug/L0.50
1,2,3-Trichlorobenzene 87-61-6 SM 6200B-ND 1ug/L0.50
1,2,4-Trichlorobenzene 120-82-1 SM 6200B-ND 1ug/L0.50
1,1,1-Trichloroethane 71-55-6 SM 6200B-ND 1ug/L0.50
1,1,2-Trichloroethane 79-00-5 SM 6200B-ND 1ug/L0.50
Trichloroethene 79-01-6 SM 6200B-ND 1ug/L0.50
Trichlorofluoromethane 75-69-4 SM 6200B-ND 1ug/L0.50
1,2,3-Trichloropropane 96-18-4 SM 6200B-ND 1ug/L0.50
1,3,5-Trimethylbenzene (Mesitylene)108-67-8 SM 6200B-ND 1ug/L0.50
1,2,4-Trimethylbenzene 95-63-6 SM 6200B-ND 1ug/L0.50
Vinyl chloride 75-01-4 SM 6200B-ND 1ug/L0.50
m+p - Xylenes 179601-23-1 SM 6200B-ND 1ug/L0.50
o - Xylenes 95-47-6 SM 6200B-ND 1ug/L0.50
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 101 70-130
Bromofluorobenzene 95 70-130
Toluene-d8 100 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 8 of 28
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
DEQ DWM
186 Howard Steelman Dr/Style
UK07086-003
11/06/2019 1040
11/07/2019
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 1 11/14/2019 1120 TML 35674
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
Benzene 71-43-2 SM 6200B-ND 1ug/L0.50
Bromobenzene 108-86-1 SM 6200B-ND 1ug/L0.50
Bromochloromethane 74-97-5 SM 6200B-ND 1ug/L0.50
Bromodichloromethane 75-27-4 SM 6200B-ND 1ug/L0.50
Bromoform 75-25-2 SM 6200B-ND 1ug/L0.50
Bromomethane (Methyl bromide)74-83-9 SM 6200B-ND 1ug/L0.50
n-Butylbenzene 104-51-8 SM 6200B-ND 1ug/L0.50
sec-Butylbenzene 135-98-8 SM 6200B-ND 1ug/L0.50
tert-Butylbenzene 98-06-6 SM 6200B-ND 1ug/L0.50
Carbon tetrachloride 56-23-5 SM 6200B-ND 1ug/L0.50
Chlorobenzene 108-90-7 SM 6200B-ND 1ug/L0.50
Chloroethane 75-00-3 SM 6200B-ND 1ug/L0.50
Chloroform 67-66-3 SM 6200B-ND 1ug/L0.50
Chloromethane (Methyl chloride)74-87-3 SM 6200B-ND 1ug/L0.50
2-Chlorotoluene 95-49-8 SM 6200B-ND 1ug/L0.50
4-Chlorotoluene 106-43-4 SM 6200B-ND 1ug/L0.50
Dibromochloromethane 124-48-1 SM 6200B-ND 1ug/L0.50
1,2-Dibromoethane (EDB)106-93-4 SM 6200B-ND 1ug/L0.50
Dibromomethane (Methylene bromide)74-95-3 SM 6200B-ND 1ug/L0.50
1,2-Dichlorobenzene 95-50-1 SM 6200B-ND 1ug/L0.50
1,3-Dichlorobenzene 541-73-1 SM 6200B-ND 1ug/L0.50
1,4-Dichlorobenzene 106-46-7 SM 6200B-ND 1ug/L0.50
Dichlorodifluoromethane 75-71-8 SM 6200B-ND 1ug/L0.50
1,1-Dichloroethane 75-34-3 SM 6200B-ND 1ug/L0.50
1,2-Dichloroethane 107-06-2 SM 6200B-ND 1ug/L0.50
1,1-Dichloroethene 75-35-4 SM 6200B-ND 1ug/L0.50
cis-1,2-Dichloroethene 156-59-2 SM 6200B-ND 1ug/L0.50
trans-1,2-Dichloroethene 156-60-5 SM 6200B-ND 1ug/L0.50
1,2-Dichloropropane 78-87-5 SM 6200B-ND 1ug/L0.50
1,3-Dichloropropane 142-28-9 SM 6200B-ND 1ug/L0.50
2,2-Dichloropropane 594-20-7 SM 6200B-ND 1ug/L0.50
1,1-Dichloropropene 563-58-6 SM 6200B-ND 1ug/L0.50
cis-1,3-Dichloropropene 10061-01-5 SM 6200B-ND 1ug/L0.50
trans-1,3-Dichloropropene 10061-02-6 SM 6200B-ND 1ug/L0.50
Diisopropyl ether (IPE)108-20-3 SM 6200B-ND 1ug/L0.50
Ethylbenzene 100-41-4 SM 6200B-ND 1ug/L0.50
Hexachlorobutadiene 87-68-3 SM 6200B-ND 1ug/L0.50
Isopropylbenzene (Cumene)98-82-8 SM 6200B-ND 1ug/L0.50
p-Isopropyltoluene (p-Cymene)99-87-6 SM 6200B-ND 1ug/L0.50
Methyl tertiary butyl ether (MTBE)1634-04-4 SM 6200B-ND 1ug/L0.50
Methylene chloride 75-09-2 SM 6200B-ND 1ug/L0.50
Naphthalene 91-20-3 SM 6200B-ND 1ug/L0.50
n-Propylbenzene 103-65-1 SM 6200B-ND 1ug/L0.50
Styrene 100-42-5 SM 6200B-ND 1ug/L0.50
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 9 of 28
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
DEQ DWM
186 Howard Steelman Dr/Style
UK07086-003
11/06/2019 1040
11/07/2019
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 1 11/14/2019 1120 TML 35674
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
1,1,1,2-Tetrachloroethane 630-20-6 SM 6200B-ND 1ug/L0.50
1,1,2,2-Tetrachloroethane 79-34-5 SM 6200B-ND 1ug/L0.50
Tetrachloroethene 127-18-4 SM 6200B-ND 1ug/L0.50
Toluene 108-88-3 SM 6200B-ND 1ug/L0.50
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 SM 6200B-ND 1ug/L0.50
1,2,3-Trichlorobenzene 87-61-6 SM 6200B-ND 1ug/L0.50
1,2,4-Trichlorobenzene 120-82-1 SM 6200B-ND 1ug/L0.50
1,1,1-Trichloroethane 71-55-6 SM 6200B-ND 1ug/L0.50
1,1,2-Trichloroethane 79-00-5 SM 6200B-ND 1ug/L0.50
Trichloroethene 79-01-6 SM 6200B-ND 1ug/L0.50
Trichlorofluoromethane 75-69-4 SM 6200B-ND 1ug/L0.50
1,2,3-Trichloropropane 96-18-4 SM 6200B-ND 1ug/L0.50
1,3,5-Trimethylbenzene (Mesitylene)108-67-8 SM 6200B-ND 1ug/L0.50
1,2,4-Trimethylbenzene 95-63-6 SM 6200B-ND 1ug/L0.50
Vinyl chloride 75-01-4 SM 6200B-ND 1ug/L0.50
m+p - Xylenes 179601-23-1 SM 6200B-ND 1ug/L0.50
o - Xylenes 95-47-6 SM 6200B-ND 1ug/L0.50
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 99 70-130
Bromofluorobenzene 86 70-130
Toluene-d8 97 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 10 of 28
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
DEQ DWM
212 Howard Steelman Dr/McNeil
UK07086-004
11/06/2019 1045
11/07/2019
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 1 11/14/2019 1144 TML 35674
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
Benzene 71-43-2 SM 6200B-ND 1ug/L0.50
Bromobenzene 108-86-1 SM 6200B-ND 1ug/L0.50
Bromochloromethane 74-97-5 SM 6200B-ND 1ug/L0.50
Bromodichloromethane 75-27-4 SM 6200B-ND 1ug/L0.50
Bromoform 75-25-2 SM 6200B-ND 1ug/L0.50
Bromomethane (Methyl bromide)74-83-9 SM 6200B-ND 1ug/L0.50
n-Butylbenzene 104-51-8 SM 6200B-ND 1ug/L0.50
sec-Butylbenzene 135-98-8 SM 6200B-ND 1ug/L0.50
tert-Butylbenzene 98-06-6 SM 6200B-ND 1ug/L0.50
Carbon tetrachloride 56-23-5 SM 6200B-ND 1ug/L0.50
Chlorobenzene 108-90-7 SM 6200B-ND 1ug/L0.50
Chloroethane 75-00-3 SM 6200B-ND 1ug/L0.50
Chloroform 67-66-3 SM 6200B-ND 1ug/L0.50
Chloromethane (Methyl chloride)74-87-3 SM 6200B-ND 1ug/L0.50
2-Chlorotoluene 95-49-8 SM 6200B-ND 1ug/L0.50
4-Chlorotoluene 106-43-4 SM 6200B-ND 1ug/L0.50
Dibromochloromethane 124-48-1 SM 6200B-ND 1ug/L0.50
1,2-Dibromoethane (EDB)106-93-4 SM 6200B-ND 1ug/L0.50
Dibromomethane (Methylene bromide)74-95-3 SM 6200B-ND 1ug/L0.50
1,2-Dichlorobenzene 95-50-1 SM 6200B-ND 1ug/L0.50
1,3-Dichlorobenzene 541-73-1 SM 6200B-ND 1ug/L0.50
1,4-Dichlorobenzene 106-46-7 SM 6200B-ND 1ug/L0.50
Dichlorodifluoromethane 75-71-8 SM 6200B-ND 1ug/L0.50
1,1-Dichloroethane 75-34-3 SM 6200B-ND 1ug/L0.50
1,2-Dichloroethane 107-06-2 SM 6200B-ND 1ug/L0.50
1,1-Dichloroethene 75-35-4 SM 6200B-ND 1ug/L0.50
cis-1,2-Dichloroethene 156-59-2 SM 6200B-ND 1ug/L0.50
trans-1,2-Dichloroethene 156-60-5 SM 6200B-ND 1ug/L0.50
1,2-Dichloropropane 78-87-5 SM 6200B-ND 1ug/L0.50
1,3-Dichloropropane 142-28-9 SM 6200B-ND 1ug/L0.50
2,2-Dichloropropane 594-20-7 SM 6200B-ND 1ug/L0.50
1,1-Dichloropropene 563-58-6 SM 6200B-ND 1ug/L0.50
cis-1,3-Dichloropropene 10061-01-5 SM 6200B-ND 1ug/L0.50
trans-1,3-Dichloropropene 10061-02-6 SM 6200B-ND 1ug/L0.50
Diisopropyl ether (IPE)108-20-3 SM 6200B-ND 1ug/L0.50
Ethylbenzene 100-41-4 SM 6200B-ND 1ug/L0.50
Hexachlorobutadiene 87-68-3 SM 6200B-ND 1ug/L0.50
Isopropylbenzene (Cumene)98-82-8 SM 6200B-ND 1ug/L0.50
p-Isopropyltoluene (p-Cymene)99-87-6 SM 6200B-ND 1ug/L0.50
Methyl tertiary butyl ether (MTBE)1634-04-4 SM 6200B-ND 1ug/L0.50
Methylene chloride 75-09-2 SM 6200B-ND 1ug/L0.50
Naphthalene 91-20-3 SM 6200B-ND 1ug/L0.50
n-Propylbenzene 103-65-1 SM 6200B-ND 1ug/L0.50
Styrene 100-42-5 SM 6200B-ND 1ug/L0.50
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 11 of 28
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
DEQ DWM
212 Howard Steelman Dr/McNeil
UK07086-004
11/06/2019 1045
11/07/2019
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 1 11/14/2019 1144 TML 35674
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
1,1,1,2-Tetrachloroethane 630-20-6 SM 6200B-ND 1ug/L0.50
1,1,2,2-Tetrachloroethane 79-34-5 SM 6200B-ND 1ug/L0.50
Tetrachloroethene 127-18-4 SM 6200B-ND 1ug/L0.50
Toluene 108-88-3 SM 6200B-ND 1ug/L0.50
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 SM 6200B-ND 1ug/L0.50
1,2,3-Trichlorobenzene 87-61-6 SM 6200B-ND 1ug/L0.50
1,2,4-Trichlorobenzene 120-82-1 SM 6200B-ND 1ug/L0.50
1,1,1-Trichloroethane 71-55-6 SM 6200B-ND 1ug/L0.50
1,1,2-Trichloroethane 79-00-5 SM 6200B-ND 1ug/L0.50
Trichloroethene 79-01-6 SM 6200B-ND 1ug/L0.50
Trichlorofluoromethane 75-69-4 SM 6200B-ND 1ug/L0.50
1,2,3-Trichloropropane 96-18-4 SM 6200B-ND 1ug/L0.50
1,3,5-Trimethylbenzene (Mesitylene)108-67-8 SM 6200B-ND 1ug/L0.50
1,2,4-Trimethylbenzene 95-63-6 SM 6200B-ND 1ug/L0.50
Vinyl chloride 75-01-4 SM 6200B-ND 1ug/L0.50
m+p - Xylenes 179601-23-1 SM 6200B-ND 1ug/L0.50
o - Xylenes 95-47-6 SM 6200B-ND 1ug/L0.50
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 102 70-130
Bromofluorobenzene 93 70-130
Toluene-d8 101 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 12 of 28
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
DEQ DWM
132 VL Moretz Rd/Duke
UK07086-005
11/06/2019 1145
11/07/2019
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 1 11/14/2019 1209 TML 35674
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
Benzene 71-43-2 SM 6200B-ND 1ug/L0.50
Bromobenzene 108-86-1 SM 6200B-ND 1ug/L0.50
Bromochloromethane 74-97-5 SM 6200B-ND 1ug/L0.50
Bromodichloromethane 75-27-4 SM 6200B-ND 1ug/L0.50
Bromoform 75-25-2 SM 6200B-ND 1ug/L0.50
Bromomethane (Methyl bromide)74-83-9 SM 6200B-ND 1ug/L0.50
n-Butylbenzene 104-51-8 SM 6200B-ND 1ug/L0.50
sec-Butylbenzene 135-98-8 SM 6200B-ND 1ug/L0.50
tert-Butylbenzene 98-06-6 SM 6200B-ND 1ug/L0.50
Carbon tetrachloride 56-23-5 SM 6200B-ND 1ug/L0.50
Chlorobenzene 108-90-7 SM 6200B-ND 1ug/L0.50
Chloroethane 75-00-3 SM 6200B-ND 1ug/L0.50
Chloroform 67-66-3 SM 6200B-ND 1ug/L0.50
Chloromethane (Methyl chloride)74-87-3 SM 6200B-ND 1ug/L0.50
2-Chlorotoluene 95-49-8 SM 6200B-ND 1ug/L0.50
4-Chlorotoluene 106-43-4 SM 6200B-ND 1ug/L0.50
Dibromochloromethane 124-48-1 SM 6200B-ND 1ug/L0.50
1,2-Dibromoethane (EDB)106-93-4 SM 6200B-ND 1ug/L0.50
Dibromomethane (Methylene bromide)74-95-3 SM 6200B-ND 1ug/L0.50
1,2-Dichlorobenzene 95-50-1 SM 6200B-ND 1ug/L0.50
1,3-Dichlorobenzene 541-73-1 SM 6200B-ND 1ug/L0.50
1,4-Dichlorobenzene 106-46-7 SM 6200B-ND 1ug/L0.50
Dichlorodifluoromethane 75-71-8 SM 6200B-ND 1ug/L0.50
1,1-Dichloroethane 75-34-3 SM 6200B-ND 1ug/L0.50
1,2-Dichloroethane 107-06-2 SM 6200B-ND 1ug/L0.50
1,1-Dichloroethene 75-35-4 SM 6200B-ND 1ug/L0.50
cis-1,2-Dichloroethene 156-59-2 SM 6200B-ND 1ug/L0.50
trans-1,2-Dichloroethene 156-60-5 SM 6200B-ND 1ug/L0.50
1,2-Dichloropropane 78-87-5 SM 6200B-ND 1ug/L0.50
1,3-Dichloropropane 142-28-9 SM 6200B-ND 1ug/L0.50
2,2-Dichloropropane 594-20-7 SM 6200B-ND 1ug/L0.50
1,1-Dichloropropene 563-58-6 SM 6200B-ND 1ug/L0.50
cis-1,3-Dichloropropene 10061-01-5 SM 6200B-ND 1ug/L0.50
trans-1,3-Dichloropropene 10061-02-6 SM 6200B-ND 1ug/L0.50
Diisopropyl ether (IPE)108-20-3 SM 6200B-ND 1ug/L0.50
Ethylbenzene 100-41-4 SM 6200B-ND 1ug/L0.50
Hexachlorobutadiene 87-68-3 SM 6200B-ND 1ug/L0.50
Isopropylbenzene (Cumene)98-82-8 SM 6200B-ND 1ug/L0.50
p-Isopropyltoluene (p-Cymene)99-87-6 SM 6200B-ND 1ug/L0.50
Methyl tertiary butyl ether (MTBE)1634-04-4 SM 6200B-ND 1ug/L0.50
Methylene chloride 75-09-2 SM 6200B-ND 1ug/L0.50
Naphthalene 91-20-3 SM 6200B-ND 1ug/L0.50
n-Propylbenzene 103-65-1 SM 6200B-ND 1ug/L0.50
Styrene 100-42-5 SM 6200B-ND 1ug/L0.50
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 13 of 28
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
DEQ DWM
132 VL Moretz Rd/Duke
UK07086-005
11/06/2019 1145
11/07/2019
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 1 11/14/2019 1209 TML 35674
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
1,1,1,2-Tetrachloroethane 630-20-6 SM 6200B-ND 1ug/L0.50
1,1,2,2-Tetrachloroethane 79-34-5 SM 6200B-ND 1ug/L0.50
Tetrachloroethene 127-18-4 SM 6200B-ND 1ug/L0.50
Toluene 108-88-3 SM 6200B-ND 1ug/L0.50
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 SM 6200B-ND 1ug/L0.50
1,2,3-Trichlorobenzene 87-61-6 SM 6200B-ND 1ug/L0.50
1,2,4-Trichlorobenzene 120-82-1 SM 6200B-ND 1ug/L0.50
1,1,1-Trichloroethane 71-55-6 SM 6200B-ND 1ug/L0.50
1,1,2-Trichloroethane 79-00-5 SM 6200B-ND 1ug/L0.50
Trichloroethene 79-01-6 SM 6200B-ND 1ug/L0.50
Trichlorofluoromethane 75-69-4 SM 6200B-ND 1ug/L0.50
1,2,3-Trichloropropane 96-18-4 SM 6200B-ND 1ug/L0.50
1,3,5-Trimethylbenzene (Mesitylene)108-67-8 SM 6200B-ND 1ug/L0.50
1,2,4-Trimethylbenzene 95-63-6 SM 6200B-ND 1ug/L0.50
Vinyl chloride 75-01-4 SM 6200B-ND 1ug/L0.50
m+p - Xylenes 179601-23-1 SM 6200B-ND 1ug/L0.50
o - Xylenes 95-47-6 SM 6200B-ND 1ug/L0.50
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 92 70-130
Bromofluorobenzene 81 70-130
Toluene-d8 91 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 14 of 28
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
DEQ DWM
212 Howard Steelman-before filter
UK07086-006
11/06/2019 1055
11/07/2019
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 1 11/14/2019 1233 TML 35674
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
Benzene 71-43-2 SM 6200B-ND 1ug/L0.50
Bromobenzene 108-86-1 SM 6200B-ND 1ug/L0.50
Bromochloromethane 74-97-5 SM 6200B-ND 1ug/L0.50
Bromodichloromethane 75-27-4 SM 6200B-ND 1ug/L0.50
Bromoform 75-25-2 SM 6200B-ND 1ug/L0.50
Bromomethane (Methyl bromide)74-83-9 SM 6200B-ND 1ug/L0.50
n-Butylbenzene 104-51-8 SM 6200B-ND 1ug/L0.50
sec-Butylbenzene 135-98-8 SM 6200B-ND 1ug/L0.50
tert-Butylbenzene 98-06-6 SM 6200B-ND 1ug/L0.50
Carbon tetrachloride 56-23-5 SM 6200B-ND 1ug/L0.50
Chlorobenzene 108-90-7 SM 6200B-ND 1ug/L0.50
Chloroethane 75-00-3 SM 6200B-ND 1ug/L0.50
Chloroform 67-66-3 SM 6200B-ND 1ug/L0.50
Chloromethane (Methyl chloride)74-87-3 SM 6200B-ND 1ug/L0.50
2-Chlorotoluene 95-49-8 SM 6200B-ND 1ug/L0.50
4-Chlorotoluene 106-43-4 SM 6200B-ND 1ug/L0.50
Dibromochloromethane 124-48-1 SM 6200B-ND 1ug/L0.50
1,2-Dibromoethane (EDB)106-93-4 SM 6200B-ND 1ug/L0.50
Dibromomethane (Methylene bromide)74-95-3 SM 6200B-ND 1ug/L0.50
1,2-Dichlorobenzene 95-50-1 SM 6200B-ND 1ug/L0.50
1,3-Dichlorobenzene 541-73-1 SM 6200B-ND 1ug/L0.50
1,4-Dichlorobenzene 106-46-7 SM 6200B-ND 1ug/L0.50
Dichlorodifluoromethane 75-71-8 SM 6200B-ND 1ug/L0.50
1,1-Dichloroethane 75-34-3 SM 6200B-ND 1ug/L0.50
1,2-Dichloroethane 107-06-2 SM 6200B-ND 1ug/L0.50
1,1-Dichloroethene 75-35-4 SM 6200B-ND 1ug/L0.50
cis-1,2-Dichloroethene 156-59-2 SM 6200B-ND 1ug/L0.50
trans-1,2-Dichloroethene 156-60-5 SM 6200B-ND 1ug/L0.50
1,2-Dichloropropane 78-87-5 SM 6200B-ND 1ug/L0.50
1,3-Dichloropropane 142-28-9 SM 6200B-ND 1ug/L0.50
2,2-Dichloropropane 594-20-7 SM 6200B-ND 1ug/L0.50
1,1-Dichloropropene 563-58-6 SM 6200B-ND 1ug/L0.50
cis-1,3-Dichloropropene 10061-01-5 SM 6200B-ND 1ug/L0.50
trans-1,3-Dichloropropene 10061-02-6 SM 6200B-ND 1ug/L0.50
Diisopropyl ether (IPE)108-20-3 SM 6200B-ND 1ug/L0.50
Ethylbenzene 100-41-4 SM 6200B-ND 1ug/L0.50
Hexachlorobutadiene 87-68-3 SM 6200B-ND 1ug/L0.50
Isopropylbenzene (Cumene)98-82-8 SM 6200B-ND 1ug/L0.50
p-Isopropyltoluene (p-Cymene)99-87-6 SM 6200B-ND 1ug/L0.50
Methyl tertiary butyl ether (MTBE)1634-04-4 SM 6200B-ND 1ug/L0.50
Methylene chloride 75-09-2 SM 6200B-ND 1ug/L0.50
Naphthalene 91-20-3 SM 6200B-ND 1ug/L0.50
n-Propylbenzene 103-65-1 SM 6200B-ND 1ug/L0.50
Styrene 100-42-5 SM 6200B-ND 1ug/L0.50
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 15 of 28
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
DEQ DWM
212 Howard Steelman-before filter
UK07086-006
11/06/2019 1055
11/07/2019
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 1 11/14/2019 1233 TML 35674
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
1,1,1,2-Tetrachloroethane 630-20-6 SM 6200B-ND 1ug/L0.50
1,1,2,2-Tetrachloroethane 79-34-5 SM 6200B-ND 1ug/L0.50
Tetrachloroethene 127-18-4 SM 6200B-ND 1ug/L0.50
Toluene 108-88-3 SM 6200B-ND 1ug/L0.50
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 SM 6200B-ND 1ug/L0.50
1,2,3-Trichlorobenzene 87-61-6 SM 6200B-ND 1ug/L0.50
1,2,4-Trichlorobenzene 120-82-1 SM 6200B-ND 1ug/L0.50
1,1,1-Trichloroethane 71-55-6 SM 6200B-ND 1ug/L0.50
1,1,2-Trichloroethane 79-00-5 SM 6200B-ND 1ug/L0.50
Trichloroethene 79-01-6 SM 6200B-ND 1ug/L0.50
Trichlorofluoromethane 75-69-4 SM 6200B-ND 1ug/L0.50
1,2,3-Trichloropropane 96-18-4 SM 6200B-ND 1ug/L0.50
1,3,5-Trimethylbenzene (Mesitylene)108-67-8 SM 6200B-ND 1ug/L0.50
1,2,4-Trimethylbenzene 95-63-6 SM 6200B-ND 1ug/L0.50
Vinyl chloride 75-01-4 SM 6200B-ND 1ug/L0.50
m+p - Xylenes 179601-23-1 SM 6200B-ND 1ug/L0.50
o - Xylenes 95-47-6 SM 6200B-ND 1ug/L0.50
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 101 70-130
Bromofluorobenzene 88 70-130
Toluene-d8 97 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 16 of 28
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
DEQ DWM
161 VL Moretz
UK07086-007
11/06/2019 1200
11/07/2019
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 1 11/14/2019 1258 TML 35674
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
Benzene 71-43-2 SM 6200B-ND 1ug/L0.50
Bromobenzene 108-86-1 SM 6200B-ND 1ug/L0.50
Bromochloromethane 74-97-5 SM 6200B-ND 1ug/L0.50
Bromodichloromethane 75-27-4 SM 6200B-ND 1ug/L0.50
Bromoform 75-25-2 SM 6200B-ND 1ug/L0.50
Bromomethane (Methyl bromide)74-83-9 SM 6200B-ND 1ug/L0.50
n-Butylbenzene 104-51-8 SM 6200B-ND 1ug/L0.50
sec-Butylbenzene 135-98-8 SM 6200B-ND 1ug/L0.50
tert-Butylbenzene 98-06-6 SM 6200B-ND 1ug/L0.50
Carbon tetrachloride 56-23-5 SM 6200B-ND 1ug/L0.50
Chlorobenzene 108-90-7 SM 6200B-ND 1ug/L0.50
Chloroethane 75-00-3 SM 6200B-ND 1ug/L0.50
Chloroform 67-66-3 SM 6200B-ND 1ug/L0.50
Chloromethane (Methyl chloride)74-87-3 SM 6200B-ND 1ug/L0.50
2-Chlorotoluene 95-49-8 SM 6200B-ND 1ug/L0.50
4-Chlorotoluene 106-43-4 SM 6200B-ND 1ug/L0.50
Dibromochloromethane 124-48-1 SM 6200B-ND 1ug/L0.50
1,2-Dibromoethane (EDB)106-93-4 SM 6200B-ND 1ug/L0.50
Dibromomethane (Methylene bromide)74-95-3 SM 6200B-ND 1ug/L0.50
1,2-Dichlorobenzene 95-50-1 SM 6200B-ND 1ug/L0.50
1,3-Dichlorobenzene 541-73-1 SM 6200B-ND 1ug/L0.50
1,4-Dichlorobenzene 106-46-7 SM 6200B-ND 1ug/L0.50
Dichlorodifluoromethane 75-71-8 SM 6200B-ND 1ug/L0.50
1,1-Dichloroethane 75-34-3 SM 6200B-ND 1ug/L0.50
1,2-Dichloroethane 107-06-2 SM 6200B-ND 1ug/L0.50
1,1-Dichloroethene 75-35-4 SM 6200B-ND 1ug/L0.50
cis-1,2-Dichloroethene 156-59-2 SM 6200B-ND 1ug/L0.50
trans-1,2-Dichloroethene 156-60-5 SM 6200B-ND 1ug/L0.50
1,2-Dichloropropane 78-87-5 SM 6200B-ND 1ug/L0.50
1,3-Dichloropropane 142-28-9 SM 6200B-ND 1ug/L0.50
2,2-Dichloropropane 594-20-7 SM 6200B-ND 1ug/L0.50
1,1-Dichloropropene 563-58-6 SM 6200B-ND 1ug/L0.50
cis-1,3-Dichloropropene 10061-01-5 SM 6200B-ND 1ug/L0.50
trans-1,3-Dichloropropene 10061-02-6 SM 6200B-ND 1ug/L0.50
Diisopropyl ether (IPE)108-20-3 SM 6200B-ND 1ug/L0.50
Ethylbenzene 100-41-4 SM 6200B-ND 1ug/L0.50
Hexachlorobutadiene 87-68-3 SM 6200B-ND 1ug/L0.50
Isopropylbenzene (Cumene)98-82-8 SM 6200B-ND 1ug/L0.50
p-Isopropyltoluene (p-Cymene)99-87-6 SM 6200B-ND 1ug/L0.50
Methyl tertiary butyl ether (MTBE)1634-04-4 SM 6200B-ND 1ug/L0.50
Methylene chloride 75-09-2 SM 6200B-ND 1ug/L0.50
Naphthalene 91-20-3 SM 6200B-ND 1ug/L0.50
n-Propylbenzene 103-65-1 SM 6200B-ND 1ug/L0.50
Styrene 100-42-5 SM 6200B-ND 1ug/L0.50
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 17 of 28
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
DEQ DWM
161 VL Moretz
UK07086-007
11/06/2019 1200
11/07/2019
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 1 11/14/2019 1258 TML 35674
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
1,1,1,2-Tetrachloroethane 630-20-6 SM 6200B-ND 1ug/L0.50
1,1,2,2-Tetrachloroethane 79-34-5 SM 6200B-ND 1ug/L0.50
Tetrachloroethene 127-18-4 SM 6200B-ND 1ug/L0.50
Toluene 108-88-3 SM 6200B-ND 1ug/L0.50
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 SM 6200B-ND 1ug/L0.50
1,2,3-Trichlorobenzene 87-61-6 SM 6200B-ND 1ug/L0.50
1,2,4-Trichlorobenzene 120-82-1 SM 6200B-ND 1ug/L0.50
1,1,1-Trichloroethane 71-55-6 SM 6200B-ND 1ug/L0.50
1,1,2-Trichloroethane 79-00-5 SM 6200B-ND 1ug/L0.50
Trichloroethene 79-01-6 SM 6200B-ND 1ug/L0.50
Trichlorofluoromethane 75-69-4 SM 6200B-ND 1ug/L0.50
1,2,3-Trichloropropane 96-18-4 SM 6200B-ND 1ug/L0.50
1,3,5-Trimethylbenzene (Mesitylene)108-67-8 SM 6200B-ND 1ug/L0.50
1,2,4-Trimethylbenzene 95-63-6 SM 6200B-ND 1ug/L0.50
Vinyl chloride 75-01-4 SM 6200B-ND 1ug/L0.50
m+p - Xylenes 179601-23-1 SM 6200B-ND 1ug/L0.50
o - Xylenes 95-47-6 SM 6200B-ND 1ug/L0.50
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 98 70-130
Bromofluorobenzene 93 70-130
Toluene-d8 99 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
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Page 18 of 28
QC Summary
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Page 19 of 28
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:UQ35674-001
35674 SM 6200B-2011
Analytical Method:SM 6200B-2011
Matrix:Aqueous
Parameter Result Q LOQ Units Analysis DateDil
Benzene ND 11/14/2019 09520.50 ug/L1
Bromobenzene ND 11/14/2019 09520.50 ug/L1
Bromochloromethane ND 11/14/2019 09520.50 ug/L1
Bromodichloromethane ND 11/14/2019 09520.50 ug/L1
Bromoform ND 11/14/2019 09520.50 ug/L1
Bromomethane (Methyl bromide)ND 11/14/2019 09520.50 ug/L1
n-Butylbenzene ND 11/14/2019 09520.50 ug/L1
sec-Butylbenzene ND 11/14/2019 09520.50 ug/L1
tert-Butylbenzene ND 11/14/2019 09520.50 ug/L1
Carbon tetrachloride ND 11/14/2019 09520.50 ug/L1
Chlorobenzene ND 11/14/2019 09520.50 ug/L1
Chloroethane ND 11/14/2019 09520.50 ug/L1
Chloroform ND 11/14/2019 09520.50 ug/L1
Chloromethane (Methyl chloride)ND 11/14/2019 09520.50 ug/L1
2-Chlorotoluene ND 11/14/2019 09520.50 ug/L1
4-Chlorotoluene ND 11/14/2019 09520.50 ug/L1
Dibromochloromethane ND 11/14/2019 09520.50 ug/L1
1,2-Dibromoethane (EDB)ND 11/14/2019 09520.50 ug/L1
Dibromomethane (Methylene bromide)ND 11/14/2019 09520.50 ug/L1
1,2-Dichlorobenzene ND 11/14/2019 09520.50 ug/L1
1,3-Dichlorobenzene ND 11/14/2019 09520.50 ug/L1
1,4-Dichlorobenzene ND 11/14/2019 09520.50 ug/L1
Dichlorodifluoromethane ND 11/14/2019 09520.50 ug/L1
1,1-Dichloroethane ND 11/14/2019 09520.50 ug/L1
1,2-Dichloroethane ND 11/14/2019 09520.50 ug/L1
1,1-Dichloroethene ND 11/14/2019 09520.50 ug/L1
cis-1,2-Dichloroethene ND 11/14/2019 09520.50 ug/L1
trans-1,2-Dichloroethene ND 11/14/2019 09520.50 ug/L1
1,2-Dichloropropane ND 11/14/2019 09520.50 ug/L1
1,3-Dichloropropane ND 11/14/2019 09520.50 ug/L1
2,2-Dichloropropane ND 11/14/2019 09520.50 ug/L1
1,1-Dichloropropene ND 11/14/2019 09520.50 ug/L1
cis-1,3-Dichloropropene ND 11/14/2019 09520.50 ug/L1
trans-1,3-Dichloropropene ND 11/14/2019 09520.50 ug/L1
Diisopropyl ether (IPE)ND 11/14/2019 09520.50 ug/L1
Ethylbenzene ND 11/14/2019 09520.50 ug/L1
Hexachlorobutadiene ND 11/14/2019 09520.50 ug/L1
Isopropylbenzene (Cumene)ND 11/14/2019 09520.50 ug/L1
p-Isopropyltoluene (p-Cymene)ND 11/14/2019 09520.50 ug/L1
Methyl tertiary butyl ether (MTBE)ND 11/14/2019 09520.50 ug/L1
Methylene chloride ND 11/14/2019 09520.50 ug/L1
Naphthalene ND 11/14/2019 09520.50 ug/L1
n-Propylbenzene ND 11/14/2019 09520.50 ug/L1
Styrene ND 11/14/2019 09520.50 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the LOQ
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
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Shealy Environmental Services, Inc.

Page 20 of 28
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:UQ35674-001
35674 SM 6200B-2011
Analytical Method:SM 6200B-2011
Matrix:Aqueous
Parameter Result Q LOQ Units Analysis DateDil
1,1,1,2-Tetrachloroethane ND 11/14/2019 09520.50 ug/L1
1,1,2,2-Tetrachloroethane ND 11/14/2019 09520.50 ug/L1
Tetrachloroethene ND 11/14/2019 09520.50 ug/L1
Toluene ND 11/14/2019 09520.50 ug/L1
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 11/14/2019 09520.50 ug/L1
1,2,3-Trichlorobenzene ND 11/14/2019 09520.50 ug/L1
1,2,4-Trichlorobenzene ND 11/14/2019 09520.50 ug/L1
1,1,1-Trichloroethane ND 11/14/2019 09520.50 ug/L1
1,1,2-Trichloroethane ND 11/14/2019 09520.50 ug/L1
Trichloroethene ND 11/14/2019 09520.50 ug/L1
Trichlorofluoromethane ND 11/14/2019 09520.50 ug/L1
1,2,3-Trichloropropane ND 11/14/2019 09520.50 ug/L1
1,3,5-Trimethylbenzene (Mesitylene)ND 11/14/2019 09520.50 ug/L1
1,2,4-Trimethylbenzene ND 11/14/2019 09520.50 ug/L1
Vinyl chloride ND 11/14/2019 09520.50 ug/L1
m+p - Xylenes ND 11/14/2019 09520.50 ug/L1
o - Xylenes ND 11/14/2019 09520.50 ug/L1
Surrogate Q % Rec Acceptance
Limit
1,2-Dichloroethane-d4 101 70-130
Bromofluorobenzene 96 70-130
Toluene-d8 100 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the LOQ
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
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Shealy Environmental Services, Inc.

Page 21 of 28
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:UQ35674-002
35674 SM 6200B-2011
Analytical Method:SM 6200B-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Benzene 48 11/14/2019 0840975070-1301
Bromobenzene 48 11/14/2019 0840975070-1301
Bromochloromethane 45 11/14/2019 0840895070-1301
Bromodichloromethane 48 11/14/2019 0840955070-1301
Bromoform 45 11/14/2019 0840895070-1301
Bromomethane (Methyl bromide)55 11/14/2019 08401095060-1401
n-Butylbenzene 50 11/14/2019 0840995070-1301
sec-Butylbenzene 53 11/14/2019 08401065070-1301
tert-Butylbenzene 50 11/14/2019 08401015070-1301
Carbon tetrachloride 47 11/14/2019 0840935070-1301
Chlorobenzene 45 11/14/2019 0840905070-1301
Chloroethane 49 11/14/2019 0840985042-1631
Chloroform 46 11/14/2019 0840935070-1301
Chloromethane (Methyl chloride)50 11/14/2019 08401005020-1581
2-Chlorotoluene 49 11/14/2019 0840985070-1301
4-Chlorotoluene 47 11/14/2019 0840935070-1301
Dibromochloromethane 45 11/14/2019 0840905070-1301
1,2-Dibromoethane (EDB)45 11/14/2019 0840915070-1301
Dibromomethane (Methylene bromide)47 11/14/2019 0840945070-1301
1,2-Dichlorobenzene 46 11/14/2019 0840935070-1301
1,3-Dichlorobenzene 46 11/14/2019 0840925070-1301
1,4-Dichlorobenzene 46 11/14/2019 0840915070-1301
Dichlorodifluoromethane 36 11/14/2019 0840715060-1401
1,1-Dichloroethane 46 11/14/2019 0840935070-1301
1,2-Dichloroethane 48 11/14/2019 0840965070-1301
1,1-Dichloroethene 44 11/14/2019 0840885070-1301
cis-1,2-Dichloroethene 46 11/14/2019 0840935070-1301
trans-1,2-Dichloroethene 44 11/14/2019 0840885070-1301
1,2-Dichloropropane 48 11/14/2019 0840955070-1301
1,3-Dichloropropane 46 11/14/2019 0840925070-1301
2,2-Dichloropropane 52 11/14/2019 08401045070-1301
1,1-Dichloropropene 45 11/14/2019 0840895070-1301
cis-1,3-Dichloropropene 47 11/14/2019 0840955070-1301
trans-1,3-Dichloropropene 48 11/14/2019 0840965070-1301
Diisopropyl ether (IPE)47 11/14/2019 0840945070-1301
Ethylbenzene 47 11/14/2019 0840935070-1301
Hexachlorobutadiene 54 11/14/2019 08401095070-1301
Isopropylbenzene (Cumene)48 11/14/2019 0840975070-1301
p-Isopropyltoluene (p-Cymene)52 11/14/2019 08401045070-1301
Methyl tertiary butyl ether (MTBE)49 11/14/2019 0840985070-1301
Methylene chloride 48 11/14/2019 0840975070-1301
Naphthalene 38 11/14/2019 0840765050-1401
n-Propylbenzene 50 11/14/2019 08401005070-1301
Styrene 48 11/14/2019 0840965070-1301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the LOQ
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
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Shealy Environmental Services, Inc.

Page 22 of 28
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:UQ35674-002
35674 SM 6200B-2011
Analytical Method:SM 6200B-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
1,1,1,2-Tetrachloroethane 47 11/14/2019 0840945070-1301
1,1,2,2-Tetrachloroethane 49 11/14/2019 0840985070-1301
Tetrachloroethene 45 11/14/2019 0840905070-1301
Toluene 46 11/14/2019 0840915070-1301
1,1,2-Trichloro-1,2,2-Trifluoroethane 46 11/14/2019 0840935070-1301
1,2,3-Trichlorobenzene 36 11/14/2019 0840735070-1301
1,2,4-Trichlorobenzene 38 11/14/2019 0840775070-1301
1,1,1-Trichloroethane 48 11/14/2019 0840965070-1301
1,1,2-Trichloroethane 46 11/14/2019 0840925070-1301
Trichloroethene 45 11/14/2019 0840905070-1301
Trichlorofluoromethane 46 11/14/2019 0840925060-1401
1,2,3-Trichloropropane 47 11/14/2019 0840945070-1301
1,3,5-Trimethylbenzene (Mesitylene)51 11/14/2019 08401025070-1301
1,2,4-Trimethylbenzene 52 11/14/2019 08401045070-1301
Vinyl chloride 48 11/14/2019 0840975060-1401
m+p - Xylenes 46 11/14/2019 0840935070-1301
o - Xylenes 47 11/14/2019 0840945070-1301
Surrogate Q % Rec Acceptance
Limit
1,2-Dichloroethane-d4 99 70-130
Bromofluorobenzene 90 70-130
Toluene-d8 92 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the LOQ
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
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Shealy Environmental Services, Inc.

Page 23 of 28
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:UQ35945-001
35945 SM 6200B-2011
Analytical Method:SM 6200B-2011
Matrix:Aqueous
Parameter Result Q LOQ Units Analysis DateDil
1,4-Dichlorobenzene ND 11/15/2019 22300.50 ug/L1
Surrogate Q % Rec
Acceptance
Limit
1,2-Dichloroethane-d4 117 70-130
Bromofluorobenzene 95 70-130
Toluene-d8 110 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the LOQ
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
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Shealy Environmental Services, Inc.

Page 24 of 28
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:UQ35945-002
35945 SM 6200B-2011
Analytical Method:SM 6200B-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
1,4-Dichlorobenzene 51 11/15/2019 21031025070-1301
Surrogate Q % Rec
Acceptance
Limit
1,2-Dichloroethane-d4 108 70-130
Bromofluorobenzene 101 70-130
Toluene-d8 100 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the LOQ
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
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Shealy Environmental Services, Inc.

Page 25 of 28
Chain of Custody
and
Miscellaneous Documents
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Shealy Environmental Services, Inc.

Page 26 of 28
SHEALY ENVIRONMENTAL SERVICES, INC.

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 27 of 28
SHEALY ENVIRONMENTAL SERVICES, INC.

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 28 of 28