WS-3667_11700_CA_CAP_20040610_MNAProposal

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DUKE
POWER
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Mr. IL
DUKE POWER
Proposal fo r
Monitored Natural Attenuation (MNA)
BURLINGTON MANUFACTURED
GAS PLANT
Prepared by :
Duke Power
MGP Site Management Group
Mail Code EC 12 ZB
526 South Church Street (28202-1802)
PO Box 100 6
Charlotte, North Carolina 28201-1006
Wilk-o r~W
Duke DUKE POWER
PabPowere 526 South Church St.
P .0 .Box 1006ADuke Energy Company Charlotte,NC 28202-1006
June 10,2004
Mr . Peter L . Doom
Superfund Section
Division of Waste Management
401 Oberlin Road, Suite 150
Raleigh,NC 27699-164 6
Subject : Burlington MGP Site
Proposal for Monitored Natural Attenuation
Dear Mr . Doom :
Please find attached two copies of the Proposal for Monitored Natural Attenuation (MNA)document for
the Burlington MGP site .
The objectives of this report are to present groundwater assessment data, provide an evaluation of NINA,
and propose a long-term groundwater monitoring program for the Burlington MGP site . The data
collected to date allows a thorough review of the groundwater conditions at the Burlington MGP site .
The groundwater data was evaluated using a lines of evidence approach to determine the effectiveness
and feasibility of Monitored Natural Attenuation for the Burlington MGP site . Several key conclusions
are evident from review of the available groundwater data :
•The contaminant concentrations are stable or decreasing .
•The overburden and saprolite groundwater contamination is contained on-site .
•The bedrock contamination extends off-site, but is bounded in downgradient direction by PMWL-
BR and the side gradient movement is likely limited beyond Piedmont Way .
Periodic groundwater sampling is necessary to verify that site groundwater conditions do not
change significantly.
If you have questions concerning the report, please contact me at rebaker@duke-energy .com or
980 .373 .7889 .After your review of this report and the recently submitted Interim Remedial Measures
proposal, please contact me to discuss future work efforts at the site .I appreciate all of your efforts in
working with Duke on this site .
Sincerely,
Richard E .Baker Jr ., P .E .
Duke Powe r
Attachments
xc :Ralph Roberts
Tim Hunsucke r
John Powers (w/out attachments)
www, duke -energy. Com
Burlington MGP Site
Proposal fo r
Monitored Natural Attenuation (MNA)
Richard E .Baker, Jr ., P .E .
Prepared by :
Duke Powe r
MGP Site Management Group
Mail Code : EC12Z B
526 S .Church St .
Charlotte NC 28202
TABLE OF CONTENT S
1 .0 INTRODUCTION . . . . . . . . ... . . . . . . . . ... . . .. . ... ... . . . . . . . ..... . . . . . ... . . . . . ... . . . . . ... ....... . ... . . . . . .. 1
2 .0 REPORT OBJECTIVES . . . . . . . . . . . . ..... . . . . . . . . . . ... . . . . . . . . . . . . . . ... . . . . . ... . . . . . . . . ... . . . ....... 1
3 .0 MONITORED NATURAL ATTENUATION ... . . . . . . . . . ..... . . . . . ... ... . . . ..... .... . . ... . ..2
4 .0 SITE HISTORY . . . . . . . . . . . . . . . . ..... ... . .. ..... . . . ... . ... . . . . . . . . ... . . . ... . ... . . ... . . . ... ... . . . . . ... . . . . .2
5 .0 SITE CHARACTERIZATION . ... ... . . ... . . .... ... . ... . . ... . . . . ..... . ... . . ... ... ... . . . . . . . . . . . .... 3
5.1 Soil Contamination . .. .. ..... .. ........... .. .. .. .. .. .... ........... .. . ...... .. .. ... ... . .. .... . .... .. .. ........... ..... ... .... ...... .... .. ... 3
5.2 Groundwater Contamination ......... .. .. .......... .. .. .. .. . .. ..... ...... . ... .. .. . .. .. ... .. ........ .. .. .. .. .. .. .. . .. ..... .. . .. .. ... ..4
5 .2 .1 Shallow Overburden.... ..... . . . . ... . . . ....... . . . ..... . . . . . . . . . . ... . . . . ... . .. .... ... ........ ............ . . . ........... ....... . ..... . . ... .5
5 .2 .2 Saprolite ..... . . . . . . . . . . ....... ..... . . . . . . . . . . . . ..... . . . ....... . . . ..... ... ... . . . . . ... ... ... ... . ..... . . ............... . . . ..... . . ... . . . . . ... .. ....5
5 .2 .3 Shallow Bedrock . . ........ ........ . . . ..... . . . . . . . . . . . . ........... . . . ..... ...... . ....... . . ..... . . ... . . . . . ..... . . . . . ..... . . ... ..... . . . ...... 6
5 .2 .4 General Contamination Trends ...... . ... . . . . . . ..... . ... . ... . . . . . . ..... .......... . ..... . . . . . ... . . . . . . . . . . . . ..... . . . ................7
5 .3 Groundwater Movement .. .. .. .. .. .. .. ..... .......... .. .. .. .. .. . .. ... ...... .. .... .. ..... .. ..... ... .. ... .. ........ .. .. ...... .. .. ........ .7
6 .0 MNA DEMONSTRATION APPROACH . . ... . . ... .... . . . . . . . . . . . . . . . . . . ... ... . . . . . . . . . . . ... 8
7 .0 EVALUATION OF MNA (VALIDATION MONITORING).. . . . . . . . . . . . . . . ... . . . . . . .. 9
7.1 Primary Lines of Evidence (PLOE).... .. .. .... ....... .. .. ... ...... .. ... ... . .. .. .. ... .. .. .... .. .. .. .... .. .. ..... ..... ..... .. ...... 9
7 .2 Secondary Lines of Evidence (SLOE)........ .. .. .. .. .. . .. . .. .. .... .. . ... .. . .. .... ... ..... ..... .. .. .......... ...... .. .. .. .. ... 10
7 .3 Other Lines of Evidence (OLOE).. ... ....... .. . .. .. .. .. .. .. . ... ... .. . .. .. .... ......... .... .. .. .. .. .. ........ ... .. .. ... ... .. .... . 1 1
8 .0 SUMMARY OF CURRENT STATE EVALUATION . ... . . . ... . . ... . . . . . . ... ... . . . ... 11
9 .0 PROPOSAL FOR LONG-TERM MONITORING . ... . . . . . ... . . ... . ... ... ..... . ..... .. 11
9 .1 Groundwater Sampling .. .. .. ........... .. .. .. ........ .. .. .. .. .. ... ..... .... .. ...... .. ..... .. ...... .. .. . ..... .. .... ..... .. ... .. ... ..... 11
9 .2 Lab Analyses . ... ...... .. .. ...... ....... .. .. .. .. .. .... .... .. ........ .. . .. . .. .. .. .. .. . .. ...... ...... . .... .. .... .. .. ........ .. .. .. .. .. .. .. .. .. ..12
9.3 Reporting of Analytical Results . .... .. .. ...... .. .. .. .. .. .. .. . .. . .. ...... .. .... .. ..... .. ...... .. .. .. ........ .. .. ... .. ..............1 2
10 .0 REFERENCES .. . . . ... . . . . . . . ... . . ... . ... ... . . . . . ....... ... . . ...... . . ..... . . . . ..... . ... ..... ... . . . .... 13
LIST OF TABLES
Table I MNA Well s
Table 2 Summary of Shallow Overburden Analytical Data
Table 3 Summary of Saprolite Analytical Dat a
Table 4 Summary of Shallow Bedrock Analytical Data
Table 5 Shallow Overburden Groundwater Elevations
Table 6 Saprolite Analytical Groundwater Elevations
Table 7 Shallow Bedrock Groundwater Elevations
Table 8 Summary of Shallow Overburden MNA Indicator Data
Table 9 Summary of Saprolite MNA Indicator Data
Table 10 Summary of Shallow Bedrock MNA Indicator Data
Table I I Proposed Groundwater Sampling Schedul e
Table 12 Proposed Analytical Methods
Table 13 Proposed Reporting Schedul e
LIST OF FIGURES
Figure I Site Location
Figure 2 Groundwater Monitoring Well Location s
Figure 3 April 2004 Shallow Overburden Groundwater Monitoring Results
Figure 4 April 2004 Saprolite Groundwater Monitoring Result s
Figure 5 April 2004 Shallow Bedrock Groundwater Monitoring Results
Figure 6 Shallow Overburden Groundwater Contour Map -LTRS
Figure 7 Saprolite Groundwater Contour Map - LJR S
Figure 8 Shallow Bedrock Groundwater Contour Map - UR S
Figure 9 Shallow Overburden Groundwater Contaminant Trends -Benzene
Figure 10 Shallow Overburden Groundwater Contaminant Trends -Naphthalene
Figure I I Saprolite Groundwater Monitoring Contaminant Trends -Benzene
Figure 12 Saprolite Groundwater Monitoring Contaminant Trends -Naphthalene
Figure 13 Shallow Bedrock Groundwater Monitoring Contaminant Trends -Benzene
Figure 14 Shallow Bedrock Groundwater Monitoring Contaminant Trends -Naphthalene
Figure 15 April 2004 Shallow Overburden Benzene and Naphthalene Concentrations as a
Function of Distanc e
Figure 16 April 2004 Saprolite Benzene and Naphthalene Concentrations as a Function of
Distance
Figure 17 April 2004 Shallow Bedrock Benzene and Naphthalene Concentrations as a
Function of Distance
APPENDICES
APPENDIX A SITE INVESTIGATIO N
Table A-1 Soil Samples -Field Screening and Sampling Summary (by
depth interval )
Table A-2 Soil Samples -Method 8270 Analytical Results Surnmary
Table A-3 Soil Samples -Method 8020/8260 Analytical Results Summary
Figure A-1 Site Plan
Figure A-2 1929 Sanborn Map
Figure A-3 Historical MGP Site Facilities
Figure A-4 Soil Sampling Locations
APPENDIX B GROUNDWATER ANALYTICAL LAB REPORTS
June 2003
October 2003
January 2004
April 2004
Burlington MGP Site -Proposal for Monitored Natural Attenuation (MNA)
1 .0 INTRODUCTIO N
The former Burlington MGP site is located at 1205 North Church Street in the city of
Burlington, North Carolina. The site location is shown on Figure 1 .The site
encompasses approximately 10 acres of land and currently serves as an operations center
for Duke electric utility line operations and maintenance group .
The subsurface soils at the site have been impacted by volatile organic compounds
(VOCs) and polycyclic aromatic hydrocarbons (PAHs) from historical operations in
certain areas of the site as described in previous site assessment reports (Duke,1999 ;
Duke, 2002 ;URS,2002 ; LTRS,2003).The site is presently and will remain for the
foreseeable future, a Duke Power Operations Center. Risk assessments (Corporate
Environmental Solutions, January 2004) completed for the current site use concluded that
current risk levels were acceptable . Excavation and removal of impacted soils on the site
is not planned at this time .
Groundwater is present at the site under unconfined conditions at depths between 4 and
17 feet bgs . The groundwater elevation data indicates that shallow and deep overburden
groundwater converges from the east and west towards Dry Creek, which flows across
the Site while shallow bedrock groundwater flows across the Site to the northeast towards
monitoring well PMWL-S/D/BR .All three groundwater zones have been impacted by
VOCs and PAHs from historical operations on the site while analytical results for surface
water samples were below NCDENR regulatory standards .
Because down gradient receptors are supplied with municipal water, the bedrock
contamination does not appear to pose unacceptable risk to off-site receptors or
properties . Additionally, analytical results from off-site well cluster PMWL and MW-9
located northeast of the site were all below laboratory reporting limits and NCDENR
regulatory standards.
This report includes analytical sample results from groundwater sampling events that
began as early as February 1999 for some of the monitoring wells installed at the site .
The most recent well installations at the site occurred in April 2003 and were sampled for
the fifth time in April 2004 . The data collected to date allows a thorough review of the
groundwater conditions at the Burlington MGP site .
2 .0 REPORT OBJECTIVES
The objectives of this report are to
•Present groundwater assessment data
•Provide an evaluation of NIN A
•Propose a long-term groundwater monitoring program
for the Burlington MGP site .
3 .0 MONITORED NATURAL ATTENUATIO N
Natural attenuation processes affect the fate and transport of organic compounds in all
hydrologic systems . Natural Attenuation is defined as the reduction in mass or
concentration of a chemical of concern over time or distance from the source of a
chemical of concern due to naturally occurring physical, chemical and biological
processes, such as biodegradation, dispersion, dilution, adsorption, and volatilization .
Monitored Natural Attenuation (MNA)is defined as the use of natural attenuation within
the context of a careftilly controlled and monitored response action to achieve protective
concentration levels at the point of exposure .
According to the EPA (1998)there are three types of environmental monitoring required
to implement and validate a MNA program :
1)Site Characterization (i .e., baseline monitoring) to describe the disposition of
contamination and predict its ftiture behavior;
2) Validation monitoring to determine if predictions based on site characterization
are accurate; and
3)Long-term monitoring to ensure that the behavior of the contaminant plume does
not change .
4 .0 SITE HISTORY
The Burlington Manufactured Gas Plant site is located at 1205 North Church Street in
Burlington, North Carolina (see Figure A-1)at the approximate coordinates of north
latitude 360-51-49"and west longitude 79'-25'-6". A MGP facility operated at this site
beginning in 1925 and into the 1950s producing gas using the water gas process . The
MGP facilities were demolished at some point during the late 1950s to mid 1960s
timeframe . The site originally served as an electric power plant and trolley facility . The
site currently serves as an operations center for Duke Power utility line operations and
maintenance, and also contains an electric substation . The current boundaries for the
Duke property were established in 1962 and consist of approximately 10 acres .
Site features including historical and current site facilities are shown on Figure A-1 in
Appendix A .The gas plant facilities (gas plant building, gasholders, scrubbers, tar tanks,
etc .) were initially indicated on the 1929 Sanborn map (see Figure A-2).The Sanborn
Map also provides information on historical upgradient industrial facilities that include
textile processing facilities, oil company storage facilities, lumber milling facilities, auto
repair shops, motor freight facilities, a laundry, and a railway car bam .
Duke Power converted the power plant building into a trolley facility and later into an
operations center. Duke Power sold the gas franchise along with 3 .06 acres of the
property to Piedmont Natural Gas Company in 195 1 .Duke repurchased 0 .8 acres from
Pidemont in 1962 to expand the operations center facility . At some point during the
1950's and/or 1960's timeframe, the MGP facilities were demolished and the coolin g
2
water pond (see Figure A-3)was filled in to provide additional area for an operations
center storage yard and electrical substation .
The Burlington MGP site lies in a commercial/residential area approximately one mile
east of downtown Burlington. The site is bordered by North Church Street on the north,
Piedmont Way Street on the east, Holly Street on the west, and by Piedmont Natural Gas
Company property as well as Rainey Street on the south. Residential properties are
located directly adjacent to the site along the east and west property boundaries .
Perimeter security fencing restricts public access to the site .A stream flows from south
to north through the eastern area of the site and through the area of the former cooling
water pond . The stream originates approximately 4000 feet south of the site . The
operations center building, other structures, and asphalt paving cover the central area of
the site . The southeastern area of the site along and on both sides of the stream, and the
western area of the site located in the vicinity of Holly Street, are gravel surfaced .
A walking survey conducted during the site assessment effort confirmed that all
properties within 1500 feet were supplied drinking water by the City of Burlington
municipal water supply system . The groundwater at the site is not currently used for any
purpose and there are no associated exposures . The stream flowing through the site flows
through a highly urbanized area and eventually discharges into Dry Creek located
approximately 6500 feet northeast of the site . Dry Creek discharges into the Haw River
located 1 .6 miles to the northeast .
There are no sensitive environmental areas located within a I mile radius of the
Burlington MGP site .
5 .0 SITE CHARACTERIZATIO N
Extensive site characterization has been performed at the Burlington MGP Site .
The results of the Burlington MGP site investigations have been presented to NCDENR
in various reports (Duke,1999 ;Duke, 2002 ;URS,2002 ;URS, 2003).Information
presented in these reports relevant to implementation of this MNA proposal is
summarized in the following sections .
5.1 Soil Contamination
Characterization of soils at the Burlington MGP Site was conducted using Geoprobeo
direct-push sampling techniques. Soil samples were obtained from the nodal points of a
50'grid system covering suspected areas of MGP related contamination as shown in
Figure A-4 . Soil samples were collected in continuous 4'depth intervals until the extent
of contamination had been established or until refusal was encountered. The soil samples
were collected at 1 12 locations with samples collected at multiple depths .A total of 387
soil samples were collected and field screened using a inummoassay technology (SDI-
Rapid Assay@ for carcinogenic PAHs and a photoionization detector PID for VOCs .
3
Fifty-six of the samples collected were submitted for laboratory analyses . Table A-1
provides a summary of all sample coordinate locations, sample depth intervals, sampling
dates, RaPID Assay@ field screen results, PID screen results, PCB screen results, and a
listing of which samples were submitted for laboratory analyses . The levels of Polycyclic
Aromatic Hydrocarbons (PAHs) were analyzed using EPA Method 8270 and are
summarized in Table A-2 .Boring number suffixes indicate sample depth intervals as
follows :
Suffix Depth Interva l
A Surface to 4'
B 41 to 8 1
C TWIT
D 12'to 16'
E and F > 16 '
Total concentrations of carcinogenic PAH compounds as benzo(a)pyrene equivalents (see
Table A-2)were determined by summing the products of individual compound
concentrations and associated relative carcinogenic potency factors (CPF) as specified in
the DENR guidance . For the determination of concentration sums in each contaminant
classification category, one-half of the laboratory detection limit was assumed for soil
samples exhibiting non-detects . The maximum carcinogenic PAR concentration detected
was 88 ppm .
Concentrations of volatile organic compounds in soil were determined by EPA Methods
8020 or 8260 and are summarized in Table A-3 .For the determination of Total BTEX,
one-half of the laboratory detection limit was assumed for soil samples exhibiting non-
detects . As indicated in Table A-3,BTEX compounds were only detected in 18%of 56
soil samples submitted for Methods 8020/8260 analyses . The maximum Total BTEX
concentration detected was 237 ppm . Naphthalene was also detected in the Methods
8020/8260 analyses in 43% of the 56 soil samples submitted with a maximum
concentration of 480 ppm .
5.2 Groundwater Contaminatio n
Installation and sampling of 56 groundwater monitoring wells (see Figure 2) during site
investigations indicate that the site is underlain by three geostratigraphic units (URS,
2002). These units include from ground surface downward : shallow overburden
consisting of residual (native) soils and fill (e .g ., concrete, brick, wood) ranging from I to
20 feet in thickness, weathered decomposed rock (saprolite) ranging from I to 4 feet in
thickness, and shallow bedrock. Based upon observations of bedrock cores and hydraulic
conductivity testing data, bedrock becomes more competent and less permeable very
quickly with depth (i .e ., within 5 to 10 feet of the bedrock surface). Groundwater in each
of the three geostratigraphic units has been impacted by PA.Hs and MGP-related VOC s
4
(i .e ., predominantly benzene and naphthalene) with the highest concentrations detected in
groundwater between the operations center and Dry Creek.
Twenty-two wells were selected for use in the NINA evaluation effort (see Table 1).
Tables 24 present historical data for the 22 wells . The most recent analytical results
from April 2004 are shown in Figures 3-5 for each of the three layers at the site .A
number of observations can be made using the data and previous evaluation efforts
completed .
5 .2 .1 Shallow Overburde n
The extent of benzene and naphthalene in excess of the corresponding NCDENR
groundwater standards in shallow overburden groundwater is well defined and does not
extend off-site . As shown in Table 2 and Figure 3,the off-site well MW-9 and the two
overburden wells near the property boundary, MW-5 and PMWM-S, did not have
detectable concentrations of benzene or naphthalene during the April 2004 sample event .
No detectable contamination has been observed at MW-9 and PMWM-S as noted in
Table 2 except for low levels of toluene in the most recent (April 2004) sampling event
with levels less than 3 ~Lg/l .No benzene contamination was observed at MW-5 while the
naphthalene concentrations were 120 pg/I in February 1999 and 48 gg/I in June 2002
before decreasing to levels below the 21 lig/I DENR 2L standard in April 2003 .Benzene
and naphthalene concentrations in PMWC-S remained stable between June 2002 and
April 2004 . Contaminant concentrations in the primary plume areas as evaluated using
PMWB-S and P-IS have decreased when compared to maximum observed concentration
levels . In summary, the data indicates that the shallow overburden contamination is
contained on-site and is decreasing in magnitude .
5 .2 .2 Saprolite
The extent of benzene and naphthalene in excess of the corresponding NCDENR
groundwater standards in saprolite groundwater is well defined and does not extend off-
site. As shown in Table 3,no benzene or naphthalene contamination was observed at the
downgradient saprolite well (PMWL-D) or the sidegradient saprolite well PMWI in
January 2004 . However, in April 2004 (see Figure 4),1 .3 Pg/I of toluene was detected at
PMWL-D and 4 .9 ~Lg/l of naphthalene was detected at PMWI . No benzene or
naphthalene contamination has ever been observed at the downgradient well PMWL-D
while low concentrations of both benzene and naphthalene were observed in well PMWI
during some of the first few sampling events . However, the concentrations were never
greater than the DENR 2L standards .
The PMWG-D concentrations are within the DENR 2L standards . In April 2004,
benzene was detected in well PMWG-D at a concentration of 0 .63 jLg/I while naphthalene
was detected at a concentration of 9 .2 pg/l .The naphthalene concentration in PMWG-D
5
has decreased significantly since the initial February 2002 sample event result of 150
Pg/l .
Naphthalene concentrations in PMWF-D, PMWC-D, and PMWB-D remain above the
DENR standard, but the concentrations have decreased significantly as compared to the
maximum observed concentrations . Benzene in these three wells also remains above the
2L standard, but again reductions in contaminant levels in these wells have occurred .
The increased benzene concentration in PMV*rF-D for the April 2004 sampling event was
due to an elevated laboratory detection limit arising from an elevated naphthalene
concentration. However, there was no corresponding increase in the concentration of
ethylbenzene which remained consistent with historical values . Additionally, there was
no increase in benzene concentration in wells PMWC-D (upgradient) or PMWI
(downgradient). For these reasons, the increase in benzene concentration in monitoring
well PMVVF-D is likely overstated .
In summary, the data indicates that the saprolite contamination is contained on-site and is
decreasing in magnitude .
5 .2.3 Shallow Bedroc k
In contract with overburden and saprolite groundwater wells, groundwater with
concentrations of benzene and naphthalene exceeding NCDENR groundwater standards
in shallow bedrock groundwater likely extends off-site to the north of the Site beyond
North Church Street .
The two bedrock wells closest to the property lines along North Church Street are
PMWH-BR and PMWI-BR. As shown in Table 4, The PMWH-BR naphthalene
concentration was 1600 pg/l in June 2002, decreased to 730 gg/l in January 2004, and
increased to 1400 Vg/l in April 2004. Similarly, the PMWl-BR naphthalene
concentration decreased from 2000 Itg/l in June 2002 to 5 1 0 lig/l in January 2004 before
increasing to 1400 gg/l in April 2004 . In PMVrH-BR, the benzene concentration was
less than 5 gg/l for 4 out of 5 sampling events prior to increasing to 54 [Lg/l during the
April 2004 sampling event . The PMWI-BR benzene concentrations stayed relatively
stable with a 150 gg/i concentration in June 2002 compared to 120 gg/l in January 2004
before increasing to 760 gg/l in April 2004 .
Naphthalene at the side gradient bedrock monitoring well PMWM-BR was detected at
300 gg/l during the initial April 2003 sample event and 180 Ag/I during the most recent
sample event (see Table 4 and Figure 5).Both of these concentrations are above the
corresponding NCDENR groundwater standard . The naphthalene concentrations appear
to be decreasing at this location . Naphthalene has been detected once at th e
downgradient bedrock monitoring location PMVY'L-BR while the last three sample events
conducted during October 2003,January 2004, and April 2004 did not result in the
detection of any benzene or naphthalene contamination . Benzene has never been
6
detected in either PMWM-BR or PMWL-BR . However, 2 .1 pg/I toluene was detected in
PMWL-BR during the April 2004 sample event .
This data along with the flow direction in shallow bedrock indicates that the lateral extent
of naphthalene exceeding the corresponding NCDENR groundwater standard may extend
east across Piedmont Way, but does not extend to the furthest downgradient bedrock
monitoring well (i .e ., PMWL-BR). In contrast, benzene was not detected in monitoring
wells PMWM-BR which indicates that the lateral gradient extent of benzene in shallow
bedrock may not extend beyond Site boundaries . Based on the PMWI-BR results, the
benzene contamination may extend beyond Church Street .
5 .2 .4 General Contamination Trend s
A review of the data in Tables 2-4 indicates some increases in concentrations of benzene
and naphthalene . The wells exhibiting increases are generally located in the plume areas
while wells located near the downgradient boundary of impacted groundwater show
decreasing trends . Few of the wells downgradient of the PMWC cluster have shown
increases . PMWF-D indicated an increase in the April 2003 sampling event but
decreased in the two following sample events until the January 2004 sampling event
when the contaminant concentrations increased again . PMWM-BR which is a
sidegradient well near Piedmont Way has shown alternating decreases and increases
since its initial sampling in April 2003 .PMWI-BR has also shown some increasing and
decreasing trends in concentrations .
Groundwater contaminant concentrations in impacted areas and downgradient of
impacted areas have shown both increasing and decreasing trends since monitoring
began . Given that impacted materials arising from MGP operations have been in place
for 50 to 75 years and groundwater contamination is primarily contained inside site
boundaries, it appears that natural attenuation processes have and should continue to be
effective in controlling the contaminated plume .
5.3 Groundwater Movemen t
Nine rounds of comprehensive water level measurements were collected from the site
monitoring wells from November 2001 through April 2004 . Tables 5-7 provide the
historic groundwater elevations for each of the groundwater zones at the site . The most
extensive review of groundwater movement at the site was completed during preparation
of the URS 2002 report .
In-situ hydraulic tests (i .e ., slug tests) were performed on 12 monitoring wells and two
piezometers to obtain estimates of the horizontal hydraulic conductivities of fill soils,
saprolite, and bedrock at the site . The wells tested were selected to provide an adequate
assessment of the hydraulic conductivity distribution in shallow overburden, saprolite,
and bedrock in areas impacted by MGP related constituents . Estimated horizontal
hydraulic conductivity values for monitoring wells completed in the overburden fil l
7
ranges from 0.31 ft/day to 1 .14 ft/day with a geometric mean of 0 .5 ft/day. The estimated
horizontal hydraulic conductivity of the saprolite ranges from 0 .01 ft/day to 0 .77 ft/day
with a geometric mean of 0 . 18 ft/day . Horizontal conductivities for fractured shallow
bedrock range from 0 .39 ft/day to 7 .51 ft/day with a geometric mean of 1 .2 ft/day . Two
monitoring wells that were installed in deeper competent bedrock exhibited low hydraulic
conductivities of 0 .02 ft/day and 0 .05 ft/day, indicating that bedrock becomes less
permeable and more competent with depth .
URS used water elevation data collected during a groundwater monitoring event
completed in June 2002 to develop groundwater contour maps (URS,2002) for the
shallow overburden, saprolite and fractured shallow bedrock flow systems . The
evaluation included the conclusions noted below :
•Groundwater elevations in shallow overburden are highest along the west side of
the site and lowest immediately adjacent to Dry Creek . Shallow overburden
groundwater is interpreted to flow towards Dry Creek with a portion of the
shallow overburden groundwater discharging to the creek.
•Groundwater elevations in saprolite generally decreased in a downstream
direction . Similar to shallow overburden groundwater, groundwater in the
saprolite flows toward and converges on Dry Creek with a portion of the
groundwater contained in the saprolite discharging to the creek .
•Groundwater in fractured shallow bedrock flows in a northeasterly direction
parallel to Dry Creek and towards the downstream end of the local drainage basin
for the creek. This suggests that bedrock groundwater discharges either to Dry
creek downstream of the site or ultimately to the Haw River, which is interpreted
to be a regional groundwater discharge point for deeper groundwater from the site
area .
URS performed additional technical analyses during preparation of the August 2003
report . The report evaluated additional data collected and provided a review of the 2002
report findings . The 2003 URS report findings included :
•The shallow and deep overburden groundwater converges from the east and west
towards Dry Creek, which flows across the Site, whereas shallow bedrock
groundwater flows across the Site to the northeast towards monitoring well cluster
PMWL-S/D/BR (see Figures 6 - 8 )
•Upward hydraulic gradients were consistently observed at three monitoring well
couplets (i .e ., monitoring wells PMWA-S/D, PMWC-S/D/BR, and PMWI/PMWI-
BR) located closest to Dry Creek, which flows across the Site . These data indicate
that shallow and deeper overburden groundwater as well as a portion of shallow
bedrock groundwater at the Site discharges to the creek (see Figure 8).
6 .0 MNA DEMONSTRATION APPROAC H
A demonstration that MNA is an effective remedy can be made using a lines of evidence
(LOE)approach . There are three lines of evidence (TNRCC, 2001) that can be used :
8
1 .Primary lines of evidence (PLOE). Relies on use of historical groundwater data
that demonstrate a clear trend of stable or decreasing contaminants of concem
(COC)concentrations over time and with distance away from the source at
appropriate monitoring or sampling points .
2 . Secondary lines of evidence (SLOE).Uses geochcmical indicators to document
certain geochernical signatures or "footprints" in the groundwater that
demonstrate (indirectly) the type of natural attenuation process(es) occurring at
the affected property and the destruction of COCs or uses distance-based /time-
based biodegradation rate calculations to demonstrate attenuation .
3 .Other lines of evidence (OLOE).Most often consists of predictive modeling
studies and other lab/field studies that demonstrate an understanding of the natural
attenuation process(es) occurring at the affected property and their effectiveness
in controlling protective concentration limit exceedence zone migration and
decreasing COC concentrations . These approaches are recommended in cases
where predictive modeling may be used to demonstrate plume stability if PLOE
data collected over four consecutive quarters fails to provide a clear trend of
stable or decreasing COC concentrations .
7 .0 EVALUATION OF MNA (VALIDATION MONITORING )
An evaluation of the three lines of evidence described in Section 6 .0 is provided in this
section .
7.1 Pritnafy Lines of Evidence (PLOE )
Historical groundwater data for the NINA wells is presented in Tables 2-4 and the most
recent data (April 2004) is graphically illustrated in Figures 3-5 .Another set of figures
(Figures 9-14) show long-term contaminant trends for benzene and naphthalene over
time in each hydraulic zone of the site . Figures 15-17 provide a review of the April 2004
benzene and naphthalene concentrations as a function of distance moving away from the
primary areas of contamination .
All of the monitoring wells have been sampled at least 5 times beginning in April 2003
while a portion of the wells have been sampled 7-8 times . This data is adequate to make
the following observations regarding the contaminant trends at the site .
•The contaminant concentrations have decreased in magnitude over time .
•The contaminant concentrations generally decrease in a downgradient direction .
(Some increases in contamination concentrations between PMWC-BR and
PMWI-BR/PMVv'H-BR were observed in January 2004 and April 2004 .)
The data indicates that the contaminant plumes in all three hydraulic zones are in a
controlled condition and the plumes are not expanding . Although, there have been some
9
increases in contaminant concentrations, the concentrations near the downgradient edge
of impact show decreases in magnitude . The results meet the intent of the reviewed
guidance (EPA, 1999 ;EPRI, 2002 ; TNRCC, 200 1)regarding MNA -the contaminant
concentrations are either stable or decreasing .
7.2 Secondary Lines of Evidence (SLOE)
Geochernical indicator parameters collected at the Burlington site provide substantial
evidence that natural attenuation processes are occurring in the groundwater contaminant
plumes . Information provided in Tables 8-10,the URS 2002 report and the URS 2003
report was reviewed to evaluate the potential effectiveness of natural attenuation
processes at the Burlington MGP site . Suitable populations of microorganisms to achieve
degradation of benzene and naphthalene were observed at the site in testing performed
during boring of monitoring wells at PMWA-S, PMW-D, and PMWC-D (URS,2002).
Additionally,pH measurements observed in all three zones (shallow overburden,
saprolite, and fractured bedrock) are suitable for growth of indigenous microorganisms
capable of degrading benzene and naphthalene . Other observations from the site data
related to naturally occurring biodegradation are summarized below .
Indicator Expected Trend Observed Result s
Impacted Area Nonimpacted Area
Dissolved Oxygen is consumed a s
Oxygen organic contaminants are
(ppm)biodegraded. Therefore,
oxygen should be lower in
impacted areas .
Shallow 0 .23 (PMWB-S) 4 .0 (PMWM-S)
Saprolite 0.2(PMWB-D) 2 .4 (PMWI)
Bedrock 0. 17 (DMW-2)0 .45 (DMW-1 )
Redox Potential As oxygen is consumed Redox values are Redox values are positive
during biodegradation of negative or lower than or higher than in impacted
organics, redox potential in nonimpacted wells wells
decreases .
Alkalinity As organic compounds Concentrations range < 1 meq/L in upgradient
are degraded, alkalinity from 2 -10 meq/L wells DMW-1 and MW-3
may increase as a result o f
C02 formation .
Electron After oxygen is consumed Fluctuate with DO and Generally stable
Acceptors in the biodegradation contaminant concentrations in
Nitrate process, other electron concentrations upgradient well s
acceptors are utilized .
Sulfate
No additional geochernical data collection for the site is proposed because of the effective
demonstration using the data collected to date .
10
7.3 Other Lines of Evidence (OLOE)
Predictive modeling may be used to demonstrate plume stability if PLOE data collected
over four consecutive quarters fails to provide a clear trend of stable or decreasing COC
concentrations . However, due to the effectiveness of the primary and secondary lines of
evidence, no modeling efforts are planned for the site .
8 .0 SUMMARY OF CURRENT STATE EVALUATIO N
Several quarters of groundwater data allow for a good analysis of the site contamination .
Several key conclusions are evident from review of the available data :
•The contaminant concentrations are stable or decreasing .
•The overburden and saprolite groundwater contamination is contained on-site .
•The bedrock contamination extends off-site, but is bounded in downgradient
direction by PMWL-BR and the side gradient movement is likely limited beyond
Piedmont Way.
•The geochernical parameters provide good information regarding secondary
indicators and indicate that effective biodegradation is occurring at the site .
•No modeling is necessary based on the effectiveness of the primary and secondary
indicators .
0 Periodic groundwater sampling is necessary to verify that site groundwater
conditions do not change significantly . The proposal for future NfNA sampling is
provided in the next section .
9 .0 PROPOSAL FOR LONG-TERM MONITORIN G
In order to verify that site groundwater conditions do not change significantly at the
Burlington MGP site, Duke Power proposes a long-term groundwater monitoring
program be implemented . The program is described in this section .
9.1 Groundwater Samplin g
The groundwater monitoring wells will be sampled twice per year according to the
proposed schedule in Table 11 .Duke will use low flow sampling techniques to sample
the groundwater wells . Prior to purging, the water levels will be gauged using an
electronic interface probe . Each well will be purged using a peristaltic pump with
dedicated tubing . The pump rate will be adjusted to stabilize drawdown (usually to less
than one foot) and purge water will be passed through a flow cell attached to a
Hydrolab@ water quality instrument to measure temperature,pH,oxidation-reduction
potential (ORP), dissolved oxygen (DO),and specific conductance . Purge water will be
collected into suitable containers for proper disposal . Purging will be deemed complet e
I I
when three consecutive measurements taken at three to five minute intervals are found to
be within the following criteria :
•Temperature is not varying more than one degree Celsius (*C):
• pH is not varying by more than 0 . 1 standard pH unit ; an d
•Specific conductance is not varying by more than 10 percent .
When field indicator parameters are stabilized, the pump discharge line will be
disconnected from the flow cell and samples will be collected directly from the pump
discharge line into the appropriate sample containers provided by the laboratory.
Following collection, samples will be logged on a chain-of-custody form and stored with
ice in a cooler for shipment to the laboratory .
Each well sampling will be completed within three hours after final purge . Prior to
sampling VOCs, the pumping rate will be reduced to 50-ml per minute to minimize the
loss of VOCs through sample aeration . Appropriate preservatives will be added to
samples, custody sheet documentation will be completed, and samples will be stored on
ice at VC until delivery to the laboratory .
9 .2 Lab Analyses
The groundwater samples will be analyzed as described in Table 12 . Analysis of field
parameters and EPA Method 8260 (BTEX +naphthalene) will be performed for each
sampling event . The use of the EPA 8260 analysis for BTEX and naphthalene is
proposed as the only analytical test to be used for long-term organic monitoring at the
site . Based on the analytical results observed to date, this analysis should allow effective
evaluation and trending of the site groundwater contamination.
The sample analyses will be performed by the Duke Energy Analytical Laboratory
located in Huntersville,NC (SCDHEC Laboratory Certification 499005) or other North
Carolina certified labs . These lab analyses should allow effective long-term evaluation of
the site groundwater.
9.3 Reporting of Analytical Results
As noted in Table 13,Duke will submit an annual report that provides an analysis of the
year of groundwater data and any recommendations for changes in the sampling program .
During the sampling event between annual reports, a summary data table along with
figures showing benzene, naphthalene, and groundwater elevation contours will be
provided to DENR .
12
10 .0 REFERENCE S
Air Force Center for Environmental Excellence,Designing Monitoring Programs to
Effectively Evaluate the Performance of Natural Attenuation .
Corporate Environmental Solutions, 2004 . "Baseline Risk Assessment for Duke
Property." January 2004 .
Corporate Environmental Solutions, 2004 . "Baseline Risk Assessment for Piedmont
Property." January 2004 .
Duke Engineering Services,1999 ."Duke Power Company, Burlington Manufactured
Gas Plant Site, Investigation and Site Assessment Report ." October 1999 .
Duke Energy, December 2002 . "Responses to DENR Technical Review Comments
Burlington Manufactured Gas Plant Site ."
EPA, 1998,Monitored Natural Attenuationfor Groundwater:EPA/625/K-98/00 1 .
EPA, 1999,Use ofMonitored Natural Attenuation at Superfund, RCRA Corrective
Action, and Underground Storage Tank Sites :OSWER Directive Number 9200 .4-
17P .
EPRI, Guidance for the Selection of Monitored Natural Attenuation as a Remedial
Measure,July 2002,1005306 .
TNRCC, Monitored Natural Demonstrations,October 2001, RG-366/TRRP-33 .
URS,2002 . "Supplemental Site Characterization Report Former Burlington
Manufactured Gas Plant Site Burlington ,North Carolina ." November 2002 .
URS, 2003 ."Phase 11 Supplemental Site Characterization Report Addendum Former
Burlington Manufactured Gas Plant Site Burlington, North Carolina ." August 2003 .
13
03r,mU)
MNA Wells
Monitoring Well Information
Shallow Overburden Wells
TotalDepth Waterl-eyel Elevation Top Elevation Bottom Hydraulic Average
Location fit bg$)Reference Ground Surface Bedrock Screen Slot Screen Screen Intemal Screen interval Screen Length Conductivity GW Velocity
I Elevation (0)Elevation (ft)Elevation (ft)Size (in) Material ffn (ft)(ft)(tils")(l MY,
MW-3 22 .6 607.48 607 .65 585.05 0.01 PVC 595 .65 585 .65 io
P-2S 14 592.9,1 593 .99 no 0.01 PVC 589.99 679 .99 10
PMWB-S 14 589.14 589 .19 no 0.01 PVC 585.19 575 .19 10 3.54E-06 3.10E-01
P-IS 12.1 590.63 590 .68 ne 0.01 PVC 588.58 578 .58 10 1 .63E-05 1 .41E~00
PMWC-S 21 .5 690.96 591 her 0.01 Pvc 684 .5 569 .5 15 4 .90E .06 4 .20E-01 18 .3
MW-5 13 .9 585.91 586 .14 572.24 0.01 PVC 582.24 57Z24 1 0
Mw.p 7 576.64 574 .14 567 .14 0.01 PVC 572.14 567.14 5
PMWM-S 13 588.53 588 .83 NE oel PVC 582.83 576 .33 Es
PMW -S 10 576.24 1 576 .~ 1 NE 1 0.01 1 PVC 1 574.04 1 569Z4 1 5
Saprolite Well s
Total Depth Water Le~el Elevation Top EWation Bottom Hydraulic Average
Location (it b9s)Reference Gmund Surface Bedrock Screen Slot Screen Screen Inter,,al Screen Intenyal Screen Length Conduc&ity GW Velocity
Ele~ation (it)Elevation (ft)Elevation (ft)Size ~in) Material (ft)Of (ft)(fvsec) (I'lldayl, 0w)
PMWB-D 18 .7 689.31 589 .35 570 .65 0.01 PVC 672.35 570.85 1 .5 4 .28E-06 3 .70E-0 1
PWWC-D 25 .5 591 .41 691 .46 565.96 0~01 PVC 567 .46 665.96 1 .6
PMWF-D 17 .6 586,99 507 .16 569 .53 0 .01 PVC 571 .91 569.91 2 7 .3
PMWG-D 20 590.32 590 .49 570 .49 0.01 PVC 573.82 571 .16 2.66
PMWI 17 .3 556.013 586 .1 569 .8 pelf PVC 571 .6 569~6 2 13011-07 1 .001E-02
PMWL-D 10 1 576.93 576,23 NE 0 .01 PVC 1 567 .23 566.23
Shallow Fractured Bedrock Wells
Total Depth Water 1.9~01 Elevalton Top of Elevation Bottom of Hydraulic Average
Location (ft b9s) Reference Ground Surface Bectroa Screen Slot Screen Sown Intmal Screen Interval Screen Lergth Conductivity GW Ve"
Elevabon (ft)Ele~afion (ft)Elevalbon (ft)Size (in) Material (ft)(ft) (ft) (fvsoc)(fuday)(fvyr)
DMW.1 29.8 591 .24 591 .46 577 .46 0 .01 PVC 574 .46 562 .16 12.3
DMW-2 32.3 589 .78 589 .92 671 .42 0 .01 Pvc 567 .72 557 .72 10 4 .55E-06 3 .90E41
PMWC-BF 36 591 .61 591 .69 565 .69 0 .01 PVC 564 .69 555 .69 9 9 .33EA)6 8AGE-01 2878
PlAWH-BF 22.5 684 .49 554 .57 571 .07 0 .01 PVC 564 .47 563 .47 1 1 .79E-05 1 .55E+00
PMWl-BR 38 .5 586 .03 686 .13 568 .63 0 .01 PVC 556 .63 547 .63 a a .69E-05 7 .511E+0 0
24 ::588 .75 589.05 574 .75 0 .01 PVC 573 .05 569 .55 3.6
3, 1 576 .27 1 676 .57 1 565 .57 1 0 .01 PVC 561 .67 1 551+67 10
Table IBurlingtonMGP Site
Summary of Shallow Overburden Wells
Analytical Dat a
Lo~fion Sample Benzene Ethylbenzenil Naphthalene Toluene m-p-Xylem o-Xylene Total Xylem ToMIOTEX
Date NO (Ug/1) (u9n)Owl (ugil)(UgA)(u9A)(U9A)
MW-3 2/2SM999 (1 .00) (1 .00)(2 .00)(1 .00)(2.00)(1 .00)(2.00) (2 .00)
4/28/2003 (0.5) (1 .0)(2.0)(1 .0)(2.0)(1 .0 )
7/2512DO3 (0.5) (1 .0) (10) (1 .0)(2.0)(1 .0)
1012312DO3 (0.5) (1 .0)(2.0)(1 .0)(2.0)(1 .0)
1121/2004 (0.5) (1 .0)(2.0)(1 .0)(2.0)(1 .0)
4/2712OD4 (0.5) (1 .0)(2.0) 2 .20 (2.0)(1 .0 )
PMWB-S 101312001 140 .00 170 .DO 1700 .00 56.00 91 .00 56.00 147 .00 513.00
6/1212002 140 .00 290 .00 440 .00 100 .00 na M 260 .00 730.00
5/1/2003 100 .00 300 .00 36M .00 (100)(200)(1013)
712412003 190 .00 340 .00 2600 .00 130 .00 140 .00 100 .00
10/21M03 140 .00 290 .00 2500 .00 93 .00 120 .00 86.00
1121/2004 120 .00 250 .00 1700 .00 83 .00 100 .00 77.00
4/27/20134 140 .00 250 .00 2700 .00 98 .00 82.00 79.00
PAS 6/1312002 55 .00 130 .00 1900 .00 16 .00 M M 110 .00 311 .00
4/29/2DO3 2.90 (2 .0) 120 .00 (2 .0) (4 .0)7 .0 0
7/25/2003 0 .53 (1 .0) (10) (1 .0)(2.0)(1 .0)2.00
10121/2003 2.10 2 .80 17 .00 (1 .0)(2.0) 5 .20
1121/2004 18 .00 41 .00 70 .00 2 .30 11 .00 44 .00
412812DO4 30 .00 110.00 820 .00 &80 33.DO 76.00
PMWC-S iO/212DOI (1 .0)2 .10 190.00 (1 .0)(2.0)1 .80 1.80 3.90
6112/2002 4 .40 2 .80 120 .00 (1 .0) M M 5 .90 13.1D
511r"3 2 .80 (2 .0)13D.00 (2 .0) (4 .0) 4 .20
712212D03 2 .70 2 .00 57 .00 (1 .0)(2 .0) 4 .10
1012112003 3 .40 2 * 10 90 .00 (1 .0)(2 .0) 4 .40
1120/2004 3 .30 2 .00 110.00 (1 .0)(2 .0) 4 .20
4/2612004 4 .80 2 .60 120.00 (1 .0)2 .50 510
MW.6 V2511999 nd rid 120.00 rid rid rid nd
6114r2GO2 (0 .50) 1 .80 48 .00 (1 .0) ne M (30) 1 .80
4130/2003 (0 .5) (1 .0) 19 .00 (1 .0)(2 .0)(1 .0)
7/22r2003 (0 .5) (1 .0) (10) (1 .0)(2 .0)(1 .0)
10/2D/2003 (0 .5) (1 .0) 6 .00 (1 .0)(2 .0)(1 .0)
MMD04 (0 .5) (1 .0)(2 .0)(1 .0)(2 .0)(1 .0)
4/2712OD4 (0 .5) (1 .0)(2 .0)2.70 (2 .0)(1 .0)
MW-9 6121/2D02 nd nd (10.0)nd nd rid nd rid
51112003 (0 .5) (1 .0)(2 .0)(1 .0)(2 .0)(1 .0)
7/l/2003 NS NS NS NS NS NS
1012212003 (0 .5) (1 .0)(2.0)(1 .0)(2 .0)(1 .0)
IM12004 (05) (1 .0)(2.0)(1 .0)(2 .0)(1 .0)
4 .28/04 (0.5) (1 .0)(2.0)(1 .0)(2 .0)(1 .0 )
PMWM-S 413012003 (0.5) (1 .0)(2.0)(1 .0)(2.0)(1 .0)
712112003 (0.5) (1 .0) (10 .0) (1 .0)(2.0)(1 .0)
1012012003 (0.5) (1 .0)(2.0)(1 .0)(2.0)(1 .0)
1/19/2004 (0.5) (1 .0)(2.0)(1 .0)(2 .0)(1 .0)
4126/2004 (0.5) (1 .0)(2.0) 2 .00 (2 .0)(1 .0 )
PMWL-S 5/l/2003 (0.5) (1 .0)(2 .0)(1 .0)(2 .0)(1 .0)
7124r2OO3 (0 .5) (1 .0) (10 .0) (1 .0)(2 .0)(1 .0)
1012=003 (0 .5) (1 .0)(2 .0)(1 .0)(2 .0)(1 .0)
1/2012004 (0 .5) (1 .0)(2 .0)(1 .0)(2 .0)(1 .0)
4/2812DD4 (0 .5) (1 .0)(2 .0)(1 .0)(2.0)(1 .0)
Note. Values in panmtheses indicate less than labmtory detection
Table 2
Bunington MGP Ske
Summary of Saprolite Wells
Analytical Dat a
Location Sample Benzene Ethylbenzene Naphthalene Toluene m-p-Xulene o-Xylene Total Xylene Total BTEX
Date (ug/1) (ug/1) (ugil)(ugn) (ugA)(UgA)(UgA)
PMWB-D 10/2/2001 71 .00 40 .00 1100 .00 (10 .00)(20.00)25 .00 25 .00 136.00
6/1212002 54 .00 25.00 980 .00 (5.00)na na 28 .00 107.00
412912003 4 .70 2.20 950 .00 (2.0) (4.0) (2 .0 )
7124/2003 52 .00 24 .00 270 .00 1 .90 10.00 16.00
10/2112003 20 .00 (10) 230 .00 (10)(20)(10)
1/21/2004 35.00 9.00 300.00 1 .40 6.70 10.00
4/28/2004 50.00 (25) 720.00 (25) (50) (25 )
PMWC .D 10/312001 30.00 210 .00 7600.00 18 .00 54 .00 55.00 109 .00 367 .00
6/1212002 11 .00 87 .00 3100.00 10 .00 na na 62 .00 170 .00
a/27/2002 13.00 84 .00 1500.00 12 .00 29 .00 31 .00 60.00 169.00
4/29/2003 11 .00 93 .00 3300.00 10 .00 35 .00 37 .00
7/24/2D03 11 .00 69 .00 1100.00 (20) (40)28 .00
10/21/2003 (5) 37.00 530 .00 (10)(20)13 .00
1/20/2004 10 .00 86.00 1500.00 9.80 33 .00 37 .00
4/2612004 (13)54.00 1800 .00 (25) (50) (25 )
PMWF-D 2/l/2002 (13 .00) 30 .00 2100 .00 (13.00) (26M)(13.00)(26.00) 30.00
6114/2002 (5 .00) 16.00 1300 .00 (10 .00)na he (30.00) 16 .00
812712002 1 .40 19 .00 1300 .00 3.80 13.00 11 .00 24.00 48 .20
4/2912003 (2 .0)29 .00 2500 .00 5.00 14.00 16.00
7/22/2003 0 .82 30 .00 1200 .00 5 .60 13.00 16.00
10121/2003 0 .55 26 .00 320.00 4 .60 MOO 13.00
1/20/2004 0.71 27 .00 11DO.00 5 .70 17.00 21 .00
4/2812004 (13) 27 .00 1200 .00 (25) (50) (25 )
PMWG-D 2/112002 1 .90 2 .30 150.00 (1 .00)(2 .00)(1 .00)(2,00) 4 .20
6114/2002 0.89 (1 .00) 33 .00 (1 .00)na na (3.00) 0 .89
4/30/2003 (0 .5) 1 .60 45 .00 (1 .0)(2 .0)2 .30
7/22/2003 0 .54 1 .20 15 .00 (1 .0)(2 .0) 2 .20
10/2012003 0 .52 1 .00 8 .90 (1-0)(2.0)1 .80
1119/2004 (0 .5) (1 .0) 2 .90 (1 .0)(2.0) 1 .40
4129/2004 0 .63 1 .40 9 .20 (1 .0)(2.0) 2 .20
PMWI 6/14/2002 0 .59 (1 .00) 10.00 (1 .00) ne he (3 .00) 0.59
4130/2003 (0-5) (1 .0) 3 .20 (1 .0)(2.0)(1 .0 )
7/21/2003 (0.5) (1 .0) (10) (1 .0)(2 .0)(1 .0)
10120/2003 (0.5) (1 .0)(2 .0)(1 .0)(2 .0)(1 .0)
1119/2004 (0.5) (1 .0)(2 .0)(1 .0)(2 .0)(1 .0)
4/27/2OD4 (0-5) (1 .0)4.90 (1 .0)(2 .0)(1 .0 )
PMWL-D 4/3012003 (0 .5) (1 .0)(2 .0)(1 .0)(2 .0)(l - 0)
7/24/2003 (0-5) (1 .0) (10) (1 .0)(2 .0)(1 .0)
10122/2003 (0 .5) (1 .0)(2 .0)(1 .0)(2 .0)(1 .0)
1/2112004 (0 .5) (1 .0)(2.0)(1 .0)(2 .0)(1 .0)
4128/2004 (0.5) (1 .0)(2.0)1 .30 (2 .0)(1 .0 )
I I I I I I I I
Note : Values in parentheses indicate less than laboratory detection
Burlington MGP Site Table 3
Summary of Shallow Bedrock Wells
Analytical Data
Location Sample Benzene Ethypenzene Naphthalene Toluene m-p-Xulene o-Xylene Total Xylene Total BTEX
Date (ug/1)NO)(ug/1)(Ugn)(UgA)(UgA)(ugn)(ug/1)DMW-1 2125/1999 (1 .00) (1 .00)(2 .00)(1 .00)(2.00)(1 .00)(2 .00) (2.00 )
611712002 (0.50) (1 .00) (3 .00) (1 .00)na na (3 .00) (3 .00)
4/2112003 (0 .5) (1 .0)(2 .0)(1 .0)(2 .0)(1 .0 )
7125/2003 (0 .5) (1 .0) (10 .0) (1 .0)(2 .0)(1 .0)
10/23/2003 (0 .5) (1 .0)(2 .0)(1 .0)(2 .0)(1 .0)
1121/2004 (0 .5) (1 .0)(2 .0)(1 .0)(2 .0)(1 .0)
4/28/2004 (0 .5) (1 .0)(2.0)(1 .0)(2 .0)(1 .0 )
OMW.2 2/25/2002 85 .00 110 .00 2600.00 (50 .00) (100.00) 65 .00 65 .00 21,60.00
6/1312002 76 .00 91 .00 1800.00 6.50 ne na 64 .00 237.50
4129/2003 77 .00 110 .00 2700 .00 (20) (40)37 .00
7124/2003 85.00 130 .00 900 .00 9.70 43 .00 47 .00
1012112003 43.00 61 .00 580 .00 (10)20 .00 19 .00
1/2112DO4 79.00 93 .00 110O .Go (10)34 .00 35 .00
4/28/20134 580.00 710 .00 2600 .00 69 .00 250 .00 250 .00
PMWC-BR 10/312001 7.90 18 .00 850 .00 2 .80 9 .80 22.00 31 .80 60.50
611212002 9 .60 15 .00 340 .00 4 .40 na na 24.00 53.110
8/27/2002 1 I .Go 46 .00 970.00 17 .00 44.00 33.00 77M 151 .00
4/29/2003 5 .00 14 .00 360M 3 .60 8 .80 12 .00
7122J2003 5 .30 11 .00 160.00 (5.0) (10) 10 .00
1012112003 6 .10 13 .00 380.00 3 .20 8.40 11 .00
1/2012OD4 8 .20 16 .00 220.00 (10)(20) 12 .00
4/26/2004 8 .00 14.00 330.00 (5.0) (10) 13 .00
PMWH-BR 6114/2002 (5 .00)40.00 1600.00 11 .00 na na 53.00 104 .00
8/2712002 1 .80 53.00 1500.00 13.00 36 .00 31 .00 67 .00 134 .00
4/30/2003 8.00 41 .00 1200 .00 6 .00 25 .00 20.0 0
712212003 4.50 38 .00 980 .00 6 .10 2100 22.00
10/2212003 4.00 26 .00 730 .00 (5) 16.00 13.00
1/2012004 (5) 19 .00 730 .00 (10)14.DO 14 .00
412712004 54.00 220 .00 14GO .00 29 .00 120 .00 110 .00
I I I I
PMWl-BR 611412002 150 .00 130 .00 1600 .00 29.00 re na 150.00 459 .00
812712002 150 .00 160 .DO 2000.00 28.00 55 .00 120.00 175.00 513.00
4/30/2003 110 .00 120M 1200 .00 (40 .0)(80 .0) 73 .00
7/21/2003 150 .00 180.00 1100 .00 5.20 30 .00 97.00
10120/2003 89 .00 95.00 390.00 (10)(20)38 .00
1/19/2004 120.00 110.00 510 .00 (10) 26.00 55 .00
4/27/2004 760.00 830 .00 1400 .GO (25) 110 .00 350 .00
PMWM-BR 413012003 (2.0)3 .00 300 .00 (2 .0)10 .00 4 .80
7/21/2003 (0 .5) 2 .30 170.00 (1 .0) 8 .00 4 .00
10/20/2003 (0 .5) 2 .30 200.00 (1 .0) 7 .20 3 .60
1/1912004 (0 .5) 1 .70 130.00 (1 .0) 5 .10 2.70
4/26/2004 (2-5)(5 .0) 180.00 (5.0) (10) (5.0 )
PMWL-BR 4'30'20()3 (0 O~
(2 .0)(1 .0)(2.0)(1 .0)
712412003
(0.:)) 1 :0 1 3
.00 (1 .0)(2 .0)(1 .0)
10/2212003 (0.5) (1 .0)(2 .0)(1 .0)(2 .0)(1 .0)
1/2012004
(0
(2.0)(1 .0)(2 .0)(1 .0)
4/2812004 (0 (2.0)2.10 (2 .0)(1 .0)
Note: Values in parenthases indicate less than laboratory defection
Burlington MGP Site Table 4
Summary of Shallow Overburden Wells
Groundwater Elevation s
lr,,taltatioe Meast;rahrert Depth to Water Ler,el Ghouh~ter
Locatim Date Date Water Reference Elchration
Ele,taUon (ft)
MW4 Molina 212WIM 13,95 607.48 $053
812611999 14,08 693A
11113r"l NS -
211/2002 NS -
6/612002 NS -
7111/2002 NS -
412~3 11 .65 595M
7125/2003 11A 596,08
ID/23/2003 12,39 595 .09
1r2Ir2004 1367 59181
4127120N U75 593 .73
PMWB.S 91612DO1 11/13(2001 9,01 589.14 58C)A3
211/2002 82 5M~
&arM2 8.7 680'"
711 112002 8,6`1 580.6
51112D03 7,64 581 .6
71241=3 7 .42 $81 .72
1012112003 7 .97 581 .17
1121)2004 8 .37 580.77
4r27WN 806 01 .08
P-Is M12001 1111312001 8,99 590.63 581 .641
2JIaOO2 6 .64 581 .99
662002 8,69 581 .94
7/11/2002 9 581 .0
412W003 6,~ ~.og
7/34103 659 584,04
IMI/2003 7 .35 5821.28
1/21/2004 8 .08 582.!55
4/28aOU a N 582,%
PMM .S W12001 iVI3&00l 1150 500.06 577.38
211r2002 1222 578J4
602002 1327 577.69
7/11/2002 13,45 sn,51
&112003 11 .47 57949
7Q2r.W3 11 .39 579.67
IM112003 12.37 57859
V2012004 13,08 577.88
412612004 12,U S78,1 2
MW4 9/2WIN8 MWING 6,67 5135.91 579,24
812611999 7.65 578.26
11113r2001 7.64 578.37
211/2002 6.37 570.U
6WO02 7.38 578.53
7111r"2 7.61 578A
4MM03 5.63 t580 .28
7122r"3 5,51 580,4
10/2012003 0.36 579 .65
IQ012004 6.78 579 .13
4r2712004 6 INI 1 579 .07
MW4 W12JIM 6421/1999 7.45 576 .64 569,19
M611M 6,12 57052
IIA~001 NS -
21112002 NS -
6WO02 NS -
7111)2002 NS -
W112003 5.96 670,68
711f2003 NS -
10/2=3 Ov6 569.68
V2112004 642 570.22
4r2812004 6,47 670,1 7
PM".5 411 1r2003 ~012003 9,72 588 .53 578,81
7121~10.29 678 .24
10/2012DO 11 .28 577 .25
1/19/2004 11 .38 577A5
4/26/2004 10.97 577,56
Pm~-s 4912003 WI/2003 2.72 576.24 573,52
7/2412DO3 2.011 573.26
1012=003 3.91 572.33
1r2M004 3,23 573.01
4Qw~3 17 57307
B~Hirgtoh MGP Site Table 5
Summary of Saprolite Wells
Groundwater Elevation s
Installation Depth to Water Level Groundwater
Localon Date Date Water Reference Elevation
(ft)Elevation (ft) (ft )
PMWB .D 916r"I 1111312001 8.61 689.31 590.7
211=02 8." 580 .87
6/6/2002 8.78 580 .53
7111rM2 8.84 5W .47
4129/2003 7.67 581 .64
7/2412003 7.56 581 .75
1012112OD3 8.01 581 .3
1121r2004 8.34 580 .97
4r2ar2004 8.07 581 .24
PMWC-D 917/2001 1 111ar"I 13 .15 691 .41 578 .26
VI/2002 12 .78 678 .63
(11MIM2 13 .66 5TT75
7111/2002 13 .75 677 .66
4129r&'DD3 11 .31 SBO.1
7122P"3 12 .7 678 .71
1012112003 13 .47 577.94
112012004 15 .55 576.86
4r26/2OD4 15 .27 576A 4
PMWF-D 1118/2002 V1/2002 8.74 586 .99 578.25
M2002 9.36 5TT64
711112002 9.85 577.34
CMD03 7 .3 579.69
7/22/2003 7.47 579.52
1012112D03 7.51 579.48
1/20/2004 8.59 578 .4
4/28/2DO4 9.06 577.93
PMWG-D 1/212002 2/1M)02 10 .13 590 .32 580.19
6/612002 10 .81 579.51
7/1112002 7 583.32
43012003 8 .45 681 .87
7/2212D03 8 .54 58IJ8
IDIM2003 9 .12 581 .2
IIIW2004 9 .58 650.74
1 412712004 9 .88 580.44
PMWI 61512002 602002 12 .1 5116.06 573.96
7/1112002 12 .26 573 .78
413=003 9 .6 576.46
7121r2OM 11 .32 574 .74
101=2003 10 .71 575 .35
1119r2OG4 11 .39 574 .67
412712004 11 .29 4 .2 2
51 19PMWL-D 4/8/2003 VJOr"3 3 .74 575.93 ;72
712412003 2 .96 672 .98
1Qr2Zf2D03 3 .89 572 .04
1/2112004 4 .47 571 .46
412a/2004 3 ."572 .49
Burlington MGP Sfe Table 6
Summary of Shallow Bedrock Wells
Groundwater Elevation s
Installation Depth to Water Level Grounchvater
Location Date Date Water Reference Elevation Elevation
(Iftt) (feet)TOC (feet )
DMW-1 1111111998 2125/1999 5.52 591 .24 585.72
at26/1999 6.71 584 .53
1111312001 7.4 583 .84
211rM2 5.82 555 .42
6/612002 7.24 584
711112002 7 .48 683 .76
4/2112003 5 .3 585 .94
7125/2003 5 .22 5W .02
10123/2003 6 .24 585 .00
1121/2004 6 .71 SUM
4/2812004 6 .4 584 .84
DMW-2 11/1811998 2/25/19N T21 W9 .78 582 .57
OFM1999 7 .55 582 .23
11113/2001 8 .72 581 .06
21V2002 835 581 .43
616/2002 8 .26 581 .52
7/11/2D02 8 .88 580.9
4123/2003 6 .62 583.16
7124/2003 6 .63 683.15
10121/2003 7 .29 582.49
112M2004 7 .95 581 .83
4/2812004 7 .85 1 581 .93
PMWC-BR 902001 11/13r"2 13 .62 591.61 577.99
7JI/2002 12.52 579.09
616/2002 13 .52 578.09
7111/2002 13 .87 677.74
4123/2003 11 .21 580 .4
7rM2003 11 .3 5W .31
1012112003 12 .43 579 .18
1/2012004 13 .17 578 ."
412612004 13 .01 578.6
PMWH-BR 614/2002 6/612002 9.23 584 .49 675 .26
7/11/2002 9.39 675.1
4rM2D03 7.87 576 .62
7/2212003 7.78 676 .71
10122r"3 8 .1 576 .39
1/20/2004 8 .45 676.04
4127/2004 8 .68 575.8 1
PMWI-BR 6/312002 6181:2W2 12 586.03 574.03
7111/2002 11 .49 574.54
CJW2003 9 .64 576.39
7/2112003 9 .58 576.45
10120/2003 10.19 575.84
1/19/2OD4 10.32 575.71
412M4004 10.35 575 .68
PMWM-BR VIV2003 4/3012003 9.9 588 .65 678 .76
7/21/2003 10.49 578 .16
10/2Gr2M 11 .29 577 .36
1/1912004 11 .52 577 .13
V26/2004 11 .19 MA S
PMWL-BR 4/10/2003 4130/2003 4.95 578.27 571 .32
7/24/2003 4.96 571 .31
1CV22r"3 5.31 670 .46
1/20/2004 5 .61 570 .66
4/2W2004 5 .35 570 .92
Burlington MGP Site Table 7
Summary Of Shallow Overburden
MNA IndiGator Data
Total
Location Sample N03 S04 Total Fe Fe-2 Mn PH Ccmd DO ALK REDOX Turbidity
Date (mg/1)(mg1t)(mg/1)(Mg/1)(m9A)(Sid . Units) (umhosfcm)(mgA)(meqIL)l Priv~ (NTU)
MW-3 4/28/2003 0 .73 11 .00 0A0 5 .56 121 .00 0.05 426.60
712512003 2 .75 12.75 0.51 0.03 5 .60 126.00 0.25 6 .04 421 .00 29.00
10/2312003 2 .81 12.07 0.54 0.03 6 .80 127 .00 0.16 0 .74 348 .00 29.00
1/21/2004 2 .85 11 .90 0.74 0.06 5.70 119 .00 0.27 0 .76 na 14 .00
4/281'2004 (0.1) 26.27 0.16 0.21 5.70 117 .00 0.39 0 .74 138 .00 5 .30
PMWB-S 101312001 (0,02) 54 .00 12 .0 0
6112r2002 7.90 731 .00 0 .10 na 5 .50
5/112003 6.91 690 .00 0 .49 .176.20
7124/2003 1 .25 6.01 30 .30 0 .22 6.80 788 .00 0 .04 6 .04 64 .00 3 .00
1012112D03 (0.1) 1 .66 29.50 0 .19 6 .80 826 .00 0 .05 7.00 74 .00 8 .10
1/21/20134 0.82 22 .90 28.50 0 .18 7 .10 830 .DO 0 .19 6 .63 77.00 2.90
4127/2OD4 1 .70 11 .09 20.77 0 .17 6 .60 706 .00 0 .23 5 .69 -85 34 .00
P-IS 611312002 6 .70 635.00 0 .20 na 12 .00
U2912003 6 .34 764.00 0.19 63.70
7/2512003 (0 .1) 52 .30 0 .69 1 .77 6 .50 912.00 0.05 7 .50 225 .00 2 .60
10121/2003 (0 .1) 35 .35 2 .79 2.28 6 .50 1017 .00 0.04 7 .94 180 .00 12 .00
1121/2004 (0 .1)20 .20 13.20 2.72 7 .00 770.00 0.07 6 .61 96.00 6 .80
4/28/2004 (0 .1) 16 .08 17 .96 2.95 6 .60 692 .00 0.15 6.31 -93 4 .00
1 1 11 1 1 1PMWC-S 1002001 na 36.00 17 .00 6.60 671 .00 2.60 -97 .00 30:00
6/1212003 7.60 4114 .00 0 .20 5 .20
511/2003 6.50 404 .00 0 .37 -101 .30
712212003 (0,11 1,59 20,00 2,M 6,50 458,00 0,05 319 89,DO 6,30
10M/2003 (0.1) 0 .85 24 .70 2 .70 6.60 481 .00 0 .08 3 .92 101 .00 6.10
1/2012004 (0 .1) 0 .15 23 .20 2 .50 7 .00 484 .00 0 .13 3 .95 16 .00 3 .605C26`21)04 0.30 0 .25 25.12 2 .71 6 .15D 512 .00 0 .29 4 .07 -75 4 .20
MW.5 2125/1999 ~0 .02 32 .20 10198 .00
611412002 7 .20 643 .00 0.40 na 3 .10
4/30/2003 7 .10 895 .00 0 .31 -58 .20
7=003 (0 .1)45 .40 4 .48 0 .53 7 .00 994 .00 0 .33 9 .37 94 .00 3 .10
10120/2003 (0 .1)24 .81 4 .62 0.60 6.80 948 .00 0 .09 9.27 93.00 5.90
112012004 (0~1) 31 .90 5 .08 0 53 7.10 837 .00 0 .29 9.25 na 19 .00
4127r2004,0 .19 39.47 4 .14 0.50 7.10 921 .00 0 .22 9.38 -93 7.70
1 1 1 1 1
MW-9 612111999 ns ns n s
Mr2W3 6.70 564.00 0 .99 -&50
7/1/2003
10/2212003 2 .99 49 .7 0 .34 0 .08 6.2 643 0.22 5 .69 264 33.00
1/21/2004 7 .05 53 .3 0 .087 0 .011 5 .4 9
4128r2004 9 .87 62 .42 0 .397 0 .021 6.5 658 0.41 5 .58 137 7 .10
PWWM .S 413012DO3 1 .20 6 .00 0 .10 5 .00 110 .00 2 .07 377.70
712M2003 6 .35 11 .80 0.04 0.03 5.40 121 .00 1 .68 0 .33 522 .00 0 .67
10/2012003 4.36 15 .93 0.54 0 .10 5 .50 142 .00 0 .70 0.39 430 .00 15 .00
1/1912004 4.27 18 .14 0 .09 0 .04 5 .50 148.00 1 .20 0.04 406 .00 3 .30
412612DO4 8.65 17 .96 0 .07 0 .01 5 .30 126.OD 4 .00 0.37 193 .00 2.8 0
1 1 1 1
PMWL-S 5/112003 0.10 17 .00 2 .70 6 .27 453.00 3.10 2~2 0
712412003 (0 .1)21 .10 30.00 1 .99 6.30 453 .00 0.17 3 .70 ;547
00
9 .40
l0aM003 (0 .1)24.37 35.84 1 .99 6.10 554 .00 0.40 4 .39 159.00 12 .00
1120/2004 0 .11 14.49 53.30 2.07 6.60 539 .00 0 .21 1 .50
4128120D4 0 .17 21 .95 39 .42 2.04 6 .50 520 .00 0 .21 370
Note: Values in parentheses indicate less than laboratory detection
Burlington MGP Site Table 8
Summary Of Saprolite
MNA Indicator Data
0-
Total
Location Sample N03 S04 Total Fe Fe+2 Mn pH Cond DO ALK REDOX Turbidity
Date (MgA) (mg/1) (mg/1) (mg/1) (mgll)(Std . Units) (umhos/cm)(mg")(meq/1)(MV) (NTU )
PMWB-D 10/2/2001 (0 .02) (2.00)6 .60 547 .00 2 .40 -79 .00 22 .00
611212002 na na 7 .40 368 .00 0 .20 na 2 .80
412WO03 0 .10 5.00 7.50 6 .12 341 .00 0 .22 -43 .70
7124/2003 (0 .1) (0 .1) 19 .90 4 .00 6 .40 339 .00 0 .05 3 .28 127 .00 0 .82
1012IM03 (0 .1) 0 .11 18 .67 3 .78 6 .40 388 .00 0 .05 3 .56 147 .00 4 .60
1121/2004 (0 .1) (0 .1) 13 .97 3 .60 6 .70 371 .00 0 .21 3 .26 156.00 3 .80
412812004 0 .17 0 .23 18 .25 3 .67 6 .30 376 .00 0 .20 3 .51 -67 7 .4 0
PMWC-D 10/3/2001 0 .02 9 .00 7 .10 86 .00 3 .30 -331 .00 19 .00
6/12/2002 na na 7 .70 556 .00 020 na 1 .90
812712002
412912003 0 .10 5 .00 5 .20 6 .26 470 .00 0 .20 -40 .70
7124/2003 (0 .1) (0 .1) 9 .80 8 .40 6 .50 520 .00 0 .09 4 .84 122 .00 0 .48
10/2112003 (0 .1) 0 .10 9 .79 8 .53 6 .60 543 .00 0 .13 5 .09 149 .00 4 .50
1120/20(34 (0 .1) (0 .1) 9 .68 8 .45 6 .80 534.00 0 .17 69 .00 1 .60
4126/2004 0.31 0 .25 8 .52 8 .48 6 .50 537.00 0 .28 5.04 -47 57.0 0
MWF-D 21112002 na na na 6 .50 2 .70 -94 .00 40 .00
6/14/2002 na na na 7 .10 867.00 5 .90 na 125 .00
8/27/2002 na na na
4/29/2003 0.10 11 .00 0.20 6 .52 889.00 1 .02 -15 .70
7/22/2003 (0 .1)4 .89 13 .00 6 .9D 1009 .00 0.19 9.72 52.00 12 .40
10/21M03 (0 .1)0 .43 12 .84 4 .79 6 .70 952.00 0.06 10 .09 79.00 9 .10
1/2012004 (0 .1) 0 .66 12 .38 4 .66 6 .90 928.00 0.30 10 .01 na 5 .50
412812004 0.17 0 .73 11 .34 4 .52 6 .90 741 .00 2.80 9 .54 -52 22 .00
PMWG-D 2/l/2002 na na na 6 .20 1 .80 -56.00 410 .00
6/1412002 na na na 6 .40 487 .00 0.20 29 .10
4/30/2003 0 .96 20.00 0 .28 6 .27 497 .00 0.42 100 .70
7/2212003 3 .24 23.00 0 .45 2 .49 6 .4D 538 .00 0.08 4 .27 211 .00 1 .10
10120/2003 3 .42 20.60 0 .43 2 .46 6 .10 518 .00 0.06 4 .08 191 .00 3.00
1/1912004 3 .43 19.10 0 .13 1 .58 6 .20 457 .00 0 .33 3 .50 na 2.20
4129/2004 3 .44 20 .06 0 .53 2 .59 6 .40 530 .00 0 .94 4 .07 15 .00 3 .70
PMWl 611412002 na na na 6.80 291 .00 0 .60 na 237 .00
4/30/2003 0 .10 5.00 0.10 6.97 373 .00 0 .83 -70 .10
7/21/2003 (0 .1) 6 .81 5.23 0.94 7.00 417 .00 1 .20 3 .64 100.00 5 .10
1012012003 (0 .1)9 .02 9.92 1 .15 6.80 411 .00 0 .33 3 .09 92 .00 4 .20
1/1912004 0 .15 7 .68 0.58 0.23 7 .00 366 .00 1 .90 3 .32 240.00 3 .20
4127/2004 0 .27 8.63 3 .35 0.75 6 .90 254 .00 2 .40 3 .0 1
PMWL-D 4/3012003 0.10 30 .00 0 .10 6 .17 275.00 0.62 4 .60
7/24/2003 (0.1) 30-20 1 .61 0 .18 6 .20 265.00 0.29 2 .07 261 .00 4.50
10/22/2003 (0.1) 30.62 26 .74 0 .67 6 .00 302.00 0.78 2 .06 268 .00 13 .90
1121/2004 (0 .1) 25.66 0 .45 0 .23 6.50 352 .00 3.70 2.79 na 5.30
4/2812004 (0 .1) 26.27 0 .16 0 .21 6.40 342 .00 1 .50 2.65 114 .00 2 .00
Note : Values in parentheses indicate less then laboratory detectio n
Burlington MGP Site Table 9
Summary Of Shallow Bedrock
MNA Indicator Data
Total
Location Sample N03 S04 Total Fe Fe-2 Min pH Cond DO ALK REDOX Turbidity
Date (mgA)(mgA)(mgm)(mgA)(MgA)(Std . Units)(umhos/cm)(ri (meqfi)(mv) (NTU)
DMW~l 2125/1999 0.10 23 .80 1032 .00
611712002 na na, na 6 .20 140 .DO 0 .20 na 3.00
412112003 0 .31 10 .00 0.10 5 .80 96 .00 0 .30 215 .00
712512003 0 .68 9 .86 0 .38 0 .22 6 .00 107.00 0 .06 0.74 320 .00 2.60
10/23/2003 0 .25 9 .97 2 .58 0 .29 6 .00 123.00 0 .13 0 .87 242 .00 11 .00
1/2112DO4 0 .12 9 .12 3 .12 0 .19 6 .20 106.00 0 .53 0 .82 na 11 .00
4128120G4 0 .45 12.10 1 .75 0 .26 6 .20 106.00 0 .45 0 .84 72 .00 6.60
Dill 2/2512002 (0 .02)6675 .00
6/13r"2 na na na 6 .40 466.00 0.10 na 0 .40
4/29/2003 0 .10 5 .00 2 .40 6 .32 420.DO 0.01 47 .80
7/24/2003 (0.1) 1 .01 (0 .1) 7.47 6 .40 412.00 0.04 4 .52 153.00 1 .10
10/21/2003 (0.1) (0.1) 7 .26 6.92 6 .40 475.00 0.04 4 .54 168.00 8 .10
1/21/2OG4 (0.1)0.20 6 .10 6.46 6.40 412 .00 0.14 4 .16 na 0 .30
4/28/2004 (0.1)0 .20 7 .011 6.59 6.40 452 .00 0.17 4 .56 -62 5 .4 0
PMWC-BR 10/3/2001 (0 .02)5.00 6.60 64 .00 1 .80 -1D4 .00 12 .00
6/12/2D02 na na,M 7.60 474 .00 0.40 ns 2.20
8/2712002 na na na
4/2912003 0.10 5 .00 12.00 6.18 Q9 .00 0 .14 -54 .00
712212W3 (0.1)2 .02 14 .50 3.36 6.50 460 .00 0 .07 3 .94 118 .00 2.00
10121/2003 (0 .1) 1 .28 14 .50 3 .73 6.50 461 .00 0 .05 4.27 110 .00 11 .00
1/20/2004 0.12 1 .13 13 .29 3 .54 7 .00 473 .00 0 .21 4.15 12 .00 2 .20
4r2612004 0,07 0,80 13,89 3,76 6,50 511,00 0,57 4,26 .62 2,50
PMWH-BR 611412002 na na na 6 .70 478.00 0 .30 na 1 .90
8/27/2002 na na na na
4/3012003 0.10 5 .00 2.70 6 .57 439 .00 0 .27 -27 .70
7122/2003 (0 .1) 0 .16 4.60 3 .97 6 .60 464 .00 0 .03 4 .01 67 .00 0 .8 2
10122rM3 (0 .1) 0 .18 4 .72 4 .02 6 .30 461 .00 0 .05 4 .09 110.00 11 .00
1/20120134 0 .10 0 .48 4 .58 4 .14 630 427 .00 0 .23 4 .05 na 0.20
4r2712004 (0 .1) 0.36 4 .45 3 .85 6 .70 456 .00 0.23 3 .91 .77 2.70
PMWl-SR 6114r2W2 na na na 5.80 496 .00 0 .20 na 5.80
8/2712002 na na na na
413=003 0 .10 28.00 0 .40 6.52 573 .00 0 .27 2.00
712112003 (0.1) 15.90 2 .77 4.11 6.70 586 .00 0 .03 5 .32 128 .00 0 .93
1012ORM (0.1) 10.60 3.98 6.60 555 .130 0 .03 5 .33 86 .00 2 .40
1/19/2004 (0.1) 35 .26 1 .97 2.58 7.70 681 .00 0 .67 5.91 .18 .00 2 .10
4/27/2004 0 .18 23 .30 1 .93 2.82 6.80 576.00 0 .20 5.37 .78 1 .20
1 1 1 1 1 1 1
PMWK4 .BR 4/30/2003 0.50 30 .00 0.29 5 .45 239.00 0.42 342.20
7MP2003 2 .67 24 .40 0 .96 0 .86 5 .90 231 .00 0.06 1 .01 286.00 1 A0
1012ORW3 1 .82 25 .92 1 .43 1 .04 6 .00 241 .00 0.17 1 .15 210.00 2.30
1/19/2004 1 .78 24 .72 0.62 1 .06 5 .90 226 .00 1 .00 1 .07 na 3.40
412612004 18 .75 25 .96 0.31 0 .97 5 .80 142 .00 1 .70 1 .07 37.00 0.80
PMWL-BR 4M/2003 0 .10 15 .00 0 .17 6 .39 321 .00 0 .27 115.20
7124/2003 (0 .1) 17 .20 0.37 0 .38 6.50 301 .00 0 .04 2 .62 228 .00 0 .71
1 M 2r"3 (0 .1) 16 .59 0.33 0 .34 6.30 326 .00 0 .25 2 .59 231 .00 2 .40
1120/2004 (0.1) 20 .78 0 .19 0 .23 6 .30 234.00 0 .24 2.03 na 1 .50
4121112004 (0.1) 23 .00 0 .19 0 .23 6 .20 234.00 0 .21 1 .95 119 .00 1 .50
Note: Values in parentheses indicate less than laboratory defectio n
Burfington MGP Site Table 10
Proposed Groundwater Sampling Schedule
Year Sample Field EPA 8260 (BTEX +
Event Parameters Naphthalene)
2004 Oct-04 x x
Apr-05 x x
2005
Oct-05 x x
Apr-06 x x
2006
Oct-06 x x
2007 Oct-07
x x
Table 11
PROPOSED ANALYTICAL METHODS
BURLINGTON MG1P
REPORTING
PARAMETERS UNIT METHOD
-.------.IN-SITU ANALYSES --- -------------
pH Note 1 su Hydrolab
Specific Conductance Note 1 urnho/cm Hydrolab
Disolved Oxygen (DO)Note 1 mgA Hydrolab
ORP Note I mg/l HydrolabTemperature Note I deg .C HydrolabWater/Product Level Note 1 ft .Probe
Evacuation Volume Note I gallons CaIc.
--------ORGANIC ANALYSES------ - -----
Volatile Organics Notes 2,3,4 ug/I 8260-MGP (BTEX +naphthalene)
Notes :
'In-situ parameters (pH,cond, temp,DO,ORP) to be collected in flow-thorugh cell
2 Low Flow sampling -minimize /stabilize drawdow n
3 EPA 8260 -Analyses to be BTEX extended to include Naphthalene4DO NOT collect samples if free product is ;->O .l ft .
Table 12
Proposed Reporting Schedule
Summary Information -data tableYear Sample Event Formal Report Report Contents along with figures showing benzene
and naphthalene -Will likely match
Tables 1-7 and Figures 9-1 7
2004 Oct-04 no report x
Review of Previous Year of
Apr-05 x Groundwater Sampling Results and
2005 Recommendations for Changes in
Next Year
Oct-05 no report x
Review of Previous Year of
Apr-06 x Groundwater Sampling Results and2006Recommendations for Changes in
Next Yea r
Oct-06 no report x
Review of Previous Year o f2007Oct-07 x Groundwater Sampling Results and
Recommendations for Changes in
Next Yea r
Table 13
3
Dud lay St
Shep he Sk Knolhvood O r~tlsx~0 Evans St W,7kjrW,'/G~Efizabot Crestview D r4Q'00 (W0rnfnjg,,d,
'0--w C 3Hatcl) St C5, 0 0 cc
V~dU)- -E 0 ~:. &0 zQ 9 7~Holland AveC
zRolfu~q, Rd N
0
A Hilton Rd Rudd S t
GljRde Ct lvaV M -"ieg"~Ii3 A
70 IF ftayon S,
N Man St Sancbre 0 Martin Sjeyz
OL
0 IPlb -1401RalineyStcn ~2 .. -(n I x
Grace Ave ~> '* I Hedge St>Cn ILI 0.1 10 ~P'ff Cn N Moban(St121~Harris St P.
00.
V 't4 Mebane St St J>0 klahoma Ave
P'k -61
.
3n '
t
Grahan) s~.ElwOod St PiedmOnl rjay
0
S t87 C~oveTdO&s 51
O-Parkar St
DUKEPOWER
BURLINGTON MGP SITE
SITE LOCATION
FIGURE : 1-
N3P,FH MAIN STREET
p A
S~ITCHYMD z
BURLINGTON WGP SITE
GROUNDWATER MONITORING
WELL LOCATIONS
FIGURE :2
c \DG~..d.n W0212004 01 46 17 PIA
NOR
NORTH MA~N STREET UYcij S
LD AmA
T
IN a IN
SW17C~YARD
BURUNGTON MOP SITE
APRIL 20014
SHALLOW OVERBURDEN
GROUNDWATER
A.MONITORING RESULTS
/----7 DG FIGURr:3
c,0GN%budmda don 0W2tlDD4 02 13 18 PM
NORTH MAN STREFT
OL,
PIT"10
l2w
OPI ~AT 4
2 ~ENE
70WEP
im 0 a
S~IT~HY~)
I SURLINVO=MOP SITE
>APRIL2004
SAPROLITE'OLE ~ACK GROUNDWATER
MONITORING RESULTS
OLD FIGURE:4
c TGN~.d ... d..W/DMOD4 03 08,35 RIM
-----------------------------------------
NORTH MAIN STREET Cl,
P.
put'.On
01E~l~ Vs
A
nwu
12 100 fO o 100
SWITCHYWD
BURLINGTON MOPSITE
>APRIL2004
POLE PACK SHALLOWBEDROC K
GROUNDWATER
MONITORING RESULTS
FIGURE :8
O.0GNloudmoa don 06/04M04 D8 :53 46 AM
p --s
D ~UNDWATER ~ATON"Nol .1.42 1.,A'~Pl..11 d20D3 (FT ~Sl)
.-I SUI R FINATIO.dll 1 . MTAI 1`~.2 .d (~ Gl)
--M~G-UNI -ON GO-F977n,Pmwv-s INFERRED GROUN"ATERPm.c_s mo 31 Id .TI .NJ
P_ls
PROPEEW UNE WPROXWTE)
E GP.1-S ~NE (FEET NET
Z2 EDGE Or PAVEME4T
S RFMC ~EN
Or .R ON OF FO ._G D' u Ev
8709 vIl ..G
d ..E~STOR~
FdCl N .TEG~~EW W~QNS EXTENDING FRON!DRYE..'....1 NEG.HMCH STREET ME MPNOYIN~TE,
P.-
581 do,r I!,7
Gi .~
582 do.'.91
r
DIJIKEPOMIRBURLINGTONMGP SITE
0 140 0
M S DG_ DUKE ENERGY SHALLOW OVERBURDENURSCorparationSHOWN I -6MIER MANUFACTURED GAS PLANT SITE GROUNDWATER CONTOUR MAP ~ URS'~ULYD 2.11.3 BURLINGTON,NORTH CAROLINA477C~rddd,VOwf,SI M,~,~ddod SCALE, FEE
A Tir N STT~'ET -om"
FWA,GRCILNEWAA~ER F~Ar"-~Rt-15 .2.3 (FT .31 )
GROVNIDWAIP ELENATKA co~cu.-IU
A,EARE...VERDIFECIIO~
'501ERTY J .E (APPROXNATE)
P COMFOUR UNE (M-1 M)'0"~L~Ems EDGE OF
I S RFACE WATER
il'l O:CTOI,OF1~0 40
STORM ORAN
SOMMART 10CA"ONS E.%~~ FRO~MP.D~D~CREEx C.Na 40~OF WMC'URC.STFEET ARE AFIAO~IFATEL
A' 10.
J
`~~.VjrRrkl
DUIQH F ~
13URLINGTON MGP SITE
0 140 210 866-007 CURE ENERGY SAPROUTE GROUNDWATERURS Corporation --FORMER MANUFACTURED GAS PI-ANT SITE CONTOUR MAP - URS
427CWgrM8 StrVed. SaifI ~&Ind,RW,O,SCALE,FEET MILS .-NGTON .NORTH IPirURE 7
P"I-SR
571'N,
CROUNMRTER, eu~m N.11 1!, ~ (TT NSL )
I ORMNOWTER EUENATON CONTWR
578 .84 NFERNRED MUMOYMTEROIREOT.
PROI`E~JNE WPRO%RNATE)
PENCE
W~ ~ (FEET wERj
-DN .O~EWE 01 RAA.ENT
D ..-3 m.-E cu~`E'T`SM~.TER
NREC71ON Of VTN
UVLOI.0
-W-~. O .N
MRT ~TONS EXTENDING FRO.OWOREN ~NgL NORTH OF NOHTHCMRCH~EET ME ~ROXIRAM
DW-1
cu
-A
HON I . DUINJE P ~
BURLINGTON MGP SITE
1=NO, 46866-007 DUKE ENERG SHALLOW BEDROC KURS Corporation 0 140 210 280 MLS AS SH6wN GROUNDWATER CONTOUR MAP - URS-!!mmsm~
-
I FORMER MANUFACTURED GAS PLANT SITE
7 ~9- ~4 ~ft 3A SCALE,FEET BURLINGTON,NORTH CAROUNA7-~lil=zmu r.-MUS I I IGURE : 8
Shallow Overburden Groundwater Contaminant Trends
Benzene
MW-3
060
0,400 ~O
00 F~
Sa~W DW.
PMWB~s P-is
2000 6OW
N N O NW, 4
50M 201W
ON O,W
DW. U .VW e m
PMWc .s
I N
200 1
O .W
M-5 PMWMIs
0 60 1 3 0
.40 .200
20 0 1 0
0 W 0 W
F~
ON
040
020
PMwL-s
0 30
0200
0 10
J.
Figure 9
~ing~ MGP s~
Shallow Overburden Groundwater Contaminant Trends
Naphthalene
16,0000 mw~
~2 W
000 0
J~
SaWle Dam
PMwB-s P-Is
40M W 20M M3000,00 DO2000W
7z
00Q
000
I-al ~3 ja~
Sawl. ON.SaWl .Dads
Pmwc~s
2W00
w
0,00
la,m
U.PW Data
MW4 PMwM-s
M 00 6 0
W 00 4 W 10,
W DO 2 W
0 W 010 L . ...
F~ ~2 .3 1~ J. ja~
U .P1 .Dat.Sawl . Daft
MW-9
6 0
0
I M
i2w i1 11",.
0,
J . aa,~
Sam,looda
PMWL~
60 0
400
2
0 W
&.P'. Data
B.din,W MGP SlIa Figure 10
Saprolite Groundwater Contaminant Trends
Benzen e
060
DMW-I
0 a
020
0 DO
sa .p .Data
PMWB-D
800 0
40,00 'A",
am
je~ ~.te
Data
PMWC-D
4o w
30M
0 2 .
,
low
000 .1 J-a~
S.MW Data
PMWF-D PMWG-D
2.00
6001 , W I
-
~Ioo4am201.DOO
Semple Date Satt,lla Data
P~
1 800
WSo4a
0
20
am
~02
sa.pa. Data
PMWL-D
0300
200 to
0 DD
San,ft Data
~,e,aoe Mop Ste Figure 11
Saprolite Groundwater Contaminant Trends
Naphthalene
DMW .I
6M
F~
PMWB-D
:5M W
WOMI
5m
PMWC.D
BON N
NNW
4WO W2OWW
wt.
~Naphftl~
PMWF-D PMG-D
300000 2WW
2:0.0 1*1 5000 i
50
000 ON
1.~ J~
U,.M. D.
PMWI
5M
00
ON
Sa~l.
PMWL-D
0 0
002.0
am
lawl . D .t.
B.dm&~MGP S".Figure 12
Shallow Bedrock Groundwater Contaminant Trends
Benzen e
ON
DMW-I
0,0
000 1 1~02
sample Date
DMW-2
0000
00 00 i
4W .W
2DO M
ON
sane"Dad.
PMWC-BR
500
N
DO
0 M
S."to Mae
PMMaR
8NDO
6N
:W
400 W
20000 00 ja~
sampia eata
PMWH-BR PMWM-BR
6000
40M
20M
ON ODO [
ja~ ja~
Samplai D. sampia oaa
PMWL.B R
0 30
.200
'10
0 W
simple mi .
Su&,W MGP &te Figure 13
Shallow Bedrock Groundwater Contaminant Trends
Naphthalen e
DMW-I
6
W
S
S..Vi.D .I.
DMW-2
3"M
OM
F~2 J~ ~~.1
Sa .PI .D.W
PMWC43 R
am
PMW~BR
3~W
2MW
imm
O,W
Ow.
P~-BR PMWM-BR
4WW
=W
000
PMWL-BR
O.W
U .PI. DO.
D~ing~ MGP Ve Figure 14
Overburden Wells Apr. 2004 Benzene Conc .
1000 .00
PMWB-S
100.00
P-I S
30 .00
10
.00 PMwC-S04.80
1 .00
MW-3 190 390 MW-5 590 PMwM-S 790 990
0 .25 MW-9 PMwL-S
0 .25 0.25 025 0.25
0 .10 -
Distance (it)from MW-3
Overburden Wells /Apr. 2004 Naphthalene Conc .
100000 .0 0
10000 .00
PMWB-S
1000.00 P-1 S 2700 .00
820 .00
PMwC-s
100.00 f7hZV.UV
10 .00
-MW-3 MW-5 PMwM-S MW-9 PMwL-S
1 .00 1 .00 1 .00 1 .00 100
1 .00 ,
-11 490 990
0 .101,
Distance (ft)from MW-3
Figure 15
Saprolite Wells Apr. 2004 Benzene Conc .
1000 .00
PMW[3-D
50.00100.00
PMWC-D
6 .50
tM 10 .00
(90 PMWF-D
6 .50
PMWG-D
1 .00 :.0-6.3 . ~.. I I . I .
190 390 0 590 790 990
DMW-1 PMwI-I PMWL-D
0 .10 025 0 .25 0 .25 0
Distance (ft)from DMW-1
Saprolite Wells Apr. 2004 Naphthalene Conc .
10000 .00
PMWB-D
720 .00
1000 .00
MWF-D
PMWC-D 1200-DO
1800.00
100 .00
PMWG-D
9 .20
10 .00 :PMW14
4.90
DMW-1 PMWL-D
1 .00 ..... .g .UU 190 390 590 790 990
0101
Distance (ft)from DMW-1
16
Figure 16
Shallow Bedrock Wells /Apr . 2004 Benzene Conc .
1000.00
PMWI-BRDMW-2
580.00 U 760.00
100.00 -
PMWH-BR
54 .00
10.00
PMWC-BR
8.00 PMWM-BR
1 .2 5
1 .00
. . .. . .-m DMW-1 190 390 590 790 990
0 .25 PMWL-B R
0 .25
0.1011
Distance (ft)from DMW-I
Shallow Bedrock Wells I Apr. 2004 Naphthalene Conc .
100()0 .()0
DMW-2 PMWH-BR
1400.00260D.00 'I":
1000 .00
MWI-BR
100 .00 :-1400M
PMWM-B RPMWC-BR 180.00330.0D
10 .00
DMW-1 PMWL-BR
1 .00 1 .00 1 .00
0AY 190 390 59D 790 990
Distance (ft)from DMW-I
is
Figure 17
APPENDIX A
SITE INVESTIGATION
BURLINGTON MGP SIT E
Field Screening and Sampling Summary
Depth Interval: Surface to 4'
SAMPLING DESCRIPTION FIELD SCREEN LABORATORY SAMPLE SUMBITTED
RESULTS
Boring Sampling Sample Sampling Refusal CPAH PID PCB
No .Grid Date Depth Depth
Coordinate Interval Conc --i
(feet]Locatm are a0h W
detects M a0 0 2 F,
(<2 ppm) 0 0 z z 0
co Q. w 0 12 0 0. 0 w
North East From To (ppm] [ppm] Ippm]
BOIA 0 280 lQfl3(S8 0 4 4 .2 0 X X
802A so 300 10113W 0 4 27A 0.7
603A 100 32S 10113tSB 0 4 2 .6 0 .6 x x
804A ISO 350 1CY13/98 0 4 7 .4 0 .3
B05A 100 300 10113/98 0 4 7 1 .1 x x
B06A 200 350 I(Y13/98 0 A 12 .2 0 .2 x x x x x x x x x x x x x x'-x
B07A 627 271 10115198 0 4 2.8 0 .9 x x I
SORA 502 2S4 10115M 0 4 17.8 1 x x
809A 436 274 10115198 0 4 20.6 2 .2
BIOA 485 1 304 1 10/15198 0 4 38.2 2
B11A 498 1 285 1 10/15198 0 1 4 119 .2 26 .4
B12A 4T7 1 230 1 10115M 0 4 2 .4 3 .9 x x
B13A 456 1 250 1 10115/98 0 4 35 .6 2 .9 x x
B14A 0 1 250 1 10/19M 0 4 1 0 .2
BISA 0 1 200 1 10119/98 0 4 1 0 .5
BIGA so 200 10119198 0 4 4 16 .2 0.4
817A so 250 1DI19IS8 0 3 .3 3.3 126 0.4 x x x x x x x x x x x x x x x
B18A 100 200 10119/98 0 4 68 .2 2 .5
B19A 100 250 10/19198 0 4 114.6 2.5
B20A ISO 250 10119198 0 2 .5 2 .5 1 2 .2 10 .5-1 .0
B21A 200 250 10/19/98 0 4 2S.6 2 .7 1
B22A 200 300 10M9198 0 4 32.6 2 .8 1
B23A 200 385 10119/98 0 4 33 .2 2 .5 x x
B24A 250 300 10121198 0 4 *16 .2 15 .7
B2SA 250 350 1=1198 0 4 14 .8 4 .7
B26A 250 1 400 10121/98 0 4 37 2 .2
B27A 300 1 300 10121/98 0 4 is 3.9
B28A 300 350 IQt2l/98 0 4 45.6 6.7
B29A 300 400 10/21/98 0 4 U .4 1 .2
830A 350 438 10t27/98 0 4 8 0A
B31A 350 400 10/27198 0 4 3.4 0
B32A 350 350 10127198 0 1 4 28 1 0 0 .5-1 .0
833A 350 300 10127/98 0 4 263 10 .4
B34A 400 450 10/211/98 0 4 27 .4 0 .3
B35A 4GO 400 1W28198 0 4 12.4 0
836A 400 350 10128/98 0 4 31 .8 0 .5
837A 400 300 10/28198 0 4 3 0
B38A 450 450 10/28198 0 4 20.6 0.2
B39A 450 487 10/29198 0 4 16.2 1 .2
840A 4W 400 1OV29198 0 4 24 .2 1 .2
B41A 450 350 1 Of29/98 0 4 23 .4 1 .1
B42A 500 450 10t29198 0 4 17 .2 ,1 .2
B43A 500 400 10129/98 0 4 70 1 .7
S"A Soo 500 11 f2/98 0 4 4 .4 0 .3
WA sso Soo 1 1 098 0 4 1 0 .3
IF4~A --SW-450 11/2t98 0 4 1 -0
B47A 550 395 1112/98 0 4 8 .8 0
B48A Soo 355 1112M 0 4 1 3
.3 - - - - - - - - -
B49A 556 271 11/3t98 0 4 1 I S
B50A 520 1 245 1113/98 0 4 24 .4 0.3 x Ix
Table V.D.4-1
I of3
Table A-1
BURLINGTON IVIGP SIT E
Field Screening and Sampling Summary
Depth Interval : Surface to 4-
SAMPLING DESCRIPTION FIELD SCREEN LABORATORY SAMPLE SUMBiTTED
RESULTS
Boring Sampling Sample Sampling Refinial CPAH PID PC B
No .Grid Date Depth Depth
C~rdinate Interval
are non <Location Pact]wdatecisM2 z 0 0 2 FrZ 04<2 pp-) 0 0 to x 0 w00 0 xco 0 0. w 0 0 .
North East From To (ppm) Ippm] Ippm ]
SSIA 4S4 214 11/3198 0 4 1 1 0 1 1 1 1B52A478 214 11/3198 0 4 1 0
B53A 434 300 115198 0 4 2 .4 0 .7 1
as" 358 228 1114198 0 4 62 .8 2 .2 1B65A389 179 11/4198 0 4 3 .8 31 1
B56A 400 200 1114198 0 A 33 .2 4.1
BWA 400 250 1114198 0 4 18 .2 S3
B58A 434 208 1114198 0 4 22.6 1 .8
BSIA 480 330 11/sw 0 4 27 8.5
B62A 440 1 170 1 11/5= 0 4 1 0 .4
863A 10 550 1119198 0 1 4 1 1 0 .9 x x x x x x x x x
B64A so sw 1119198 0 4 1 0
865A 10 Soo 1119198 0 4 4.5 17.2 0
866A 300 250 1119W 0 4 ss.8 0 .5
867A 250 2SO 11098 0 4 3 0
B68A 250 200 11 IV98 0 4 2 .2 11 1 Note : concrete pad encountered at 3 .6v
B69A 200 200 11/9198 0 4 1 1 6
B70A 150 200 11/9/98 0 4 1 0.2
B?IA 200 150 1119M 0 4 2.6 0
872A 300 200 IIM95 0 4 17 .0 4 .3
B73A 320 215 1 11/W98 0 4 1 7 5 .5
1374A 350 ISO 1 1119198 0 4 1 95
875A 350 Joe 11/9/98 0 4 1 5 .8
076A 250 ISO 11110f9a 0 4 6 2 .9 x x x x -X x xK[ X677A 300 ISO 11110198 0 4 6 3 1
B78A 375 125 11110/98 0 4 1 3.2 x x x x x x x x xX
879A Soo 550 11/11/98 a 4 1 .4 1 .3 1
0
K X [X
B80A Soo 600 11/11/98 0 4 1 2.4
BUIA so sw 11111198 0 4 1 0 .2
882A 550 600 11/11198 0 4 2.6 03
883A sw 650 11/11198 0 4 1 0 .40000B84A600 650 11/11198 0 4 3.2 0 .6
B85A 600 600 11111198 0 4 102 0 .9 x x x x x x x x x
B86A 600 sw 11111/98 0 4 1 1 .8
B89A 650 650 11/12198 0 4 UA 1 .2
1XI
B87A 650 550 11111/98 0 4 15 .8 1 .3
B88A 650 600 11/11198 0 4 1 is DA
890A 700 650 11/12M 0 4 46 .8 0.2 x x x x x x x x x
B91A 700 600 11112tS8 0 4 5 .6 0.6
B92A 700 550 5112/98 0 4 4 .4 0
893A 750 600 11/30t98 0 4 6 .2 0.1000 XXr~
x [894A 600 450 W30198 0 4 1 0 .4
B95A 600 500 11/30198 0 4 2 .4 3 .4
496A650 Soo 11 rM98 0 1 .6 1 .4
0
A
897A 650 1 11/30/98 0 4 4
B99A 600 410 12/1/98 0 4 .4
-T2/1 198
0
699A 650 400 12/1 r98 0 4 1
B
m I -ffxx x1 100A so Soo 1211198 0 4 30.4 1
Table V.D .4-1
2 of 3
Table A- I
BURLINGTON IVIGP SIT E
Field Screening and Sampling Summary
Depth Interval : Surface to 4'
SAMPLING DESCRIPTION FIELD SCREEN LABORATORY SAMPLE SUMBITTED
RESULTS
Boring sampling Sample Sampling Refusal CPAH PID PC B
No. Grid Date Depth Depth
Coordinate Intenral 0<Location Ifeeti an, non wdetactsILI w w C3e0 0 M F~(<2 pp-) z < z z o. 01-0 0North East Ftom To LpPmI (PPm1 Ippm l
8101A so 470 1211/98 0 4 1 .6 0.7
B'102A 0 410 12/1=0 4 0 .8 4.5
8103A so 400 11211198 0 4 3 .2 2.3
B104A 100 Soo 3122199 0 4 1 0 .4
8105A 100 450 3122199 0 4 4 07
B106A 248 559 3r22/99 0 4 1 0 .3
B107A 2" 540 =2199 0 4 1 0 .4
B108A 1142 526 W22199 0 4 1 0 .3
B109A 150 450 3123t99 0 4 6.8 3 .3
B110A 329 512 3t23t99 0 4 '11 .2 0 .2
:111A M? 2_~M311999 4 1 08
-J-
11iA 1 4i8 3r23 9 0
4 1 iflFl I
Table V.D .41-1
3 of 3
Table A-1
BURLINGTON MGP SIT E
Field Screening and Sampling Summary
Depth Interval : 4~ to r
SAMPLING DESCRIPTION FIELD SCREEN LABORATORY SAMPLE SUMBITTED
RESULTS
Boring Sampling Sample Sampling Rahtsal CPAH PID Pc e
No. Grid Date Depth Depth
Coordinate Interval coflC-_1 < <
Location (feet] we Von 0 w
detects Of w 00 0 2 re(~2 ppm)0 M
a
w 0z Q. 0L)z 00 L)00 C . 0 Q 1-0 0 . 1- 0 03
North East From To IPPM)(Ppm)IPPmI
Sale a 280 10113198 4 8 1 0 1
B028 so 300 10113/98 4 a 49.4 0.2 x x I
B038 '100 325 10/131S8 4 8 2.8 0.2 1B04B '150 350 10/13198 4 a 28 .2 0 x X1 I IBOSS100 300 i0/l3fS8 4 6 6 1 1 .2 1 11
Base 200 350 10113198 4 a 28 0
SOTS 527 271 10115198 4 a 1 1 .3
S08B 502 254 10115198 4 a 1 0
Bose 435 274 10/151911 4 8 3 2
BIOS 485 304 1 10115t98 4 8 16.8 1 .4
Bile 498 285 1 10115fS8 4 1 8 172A 59 .5 x x1xi XXXXXX,x x x x x X1
612B 4T7 230 101151%4 8 1 1 1813B456250 10/15198 4 a 1 4.2
B14B 0 251)10119/98 4 a a 1 0.5
B15B 0 200 10119198 4 6 .5 6 .5 2 .4 0.5
xBias10020010/19198 4 a 1`16,4 1 .2 x x x x x x x x x x x
BASS 100 250 10/19/98 4 5.4 5.4 33 .6 1 .8
B218 200 250 10/19/98 4 4.9 4 .9 67 .8 3 .1
B22B 200 300 10119/98 4 6.2 6.2 30 2 .6
B23B 200 385 10119tsa 4 a 35.8 2 .4
B248 260 300 10/21/W 4 8 4.2 6 .4 1 1 1 1825B250 3SO 10121198 4 6 .5 6 .5 5 3 .7 <0 .5 1 1 1826825040010121/98 4 8 39.6 1 .3 x I x I x XIX x X, X,X,X x x x x x
B27B 300 300 10121/98 4 8 43.2 23 .4 x x x x x x x x x x x x x X-X
8288 300 350 IW21198 4 8 57.4 11 .5 x x I IB29B300400101211984ais 2 .2 Q.5 I630B354)438 IW27198 4 8 16 .2 0 .5
031B 350 "0 10127/98 4 8 1 0 .2
B328 350 350 10/27M 4 a 9 0
833B 350 300 10f27/98 4 8 297 2 .6
B348 400 4W 10/28/98 4 8 13 0 .4 1 1 1 1 1836B40035010128M 4 a 3S4 10 x x x x x x x x x I x I x I x x x
B37B 400 300 1012&98 1 4 8 171 20 .3 1 1 15388450 450 10128M 4 a 6A 0
B39B 450 487 1 (V29198 4 8 76-2 1 .7 <0 .5 1 1 1 1 1 1Sao450 400 10129/98 4 8 175 21 .6 1 1 1B4iB 450 350 1W29/98 4 a 6 .4 3.3
B428 Soo 460 1=9198 4 8 153 9 .9 x X1 x I x I x x x x x I I
B43B Soo 400 1=9198 4 8 4 1 .3
S"B 500 500 11098 4 a 22.8 0 .1
B45B 550 Soo 11/2/98 4 8 1
B46B sw 450 11f2f98 4 8 68.4 0 x x x x X
B47B 560 395 11 4 1 8 1 0 .6
B48B Soo 355
1122 1 1 1 a
7.2 381 x x x x x x x
B49B 556 271 lirSI98 4 1 a i n 7
520 1 245 11/3/98B50B
Table V.D.4-2
I of3
Table A-1
BURLINGTON MGP SIT E
Field Screening and Sampling Summary
Depth Interval : 4'to 8 '
SAMPLING DESCRIPTION FIELD SCREEN LABORATORY SAMPLE SUMBITTED
RESULTS
Boring Sampling Sample Sampling Rehtsal CPAH PID PC B
No . Grid Date Depth Depth
Coordinate Interval canc-1 <
Location [feet)are ran w wdetects0 0 2z z a. c .04<2 ppm) 0 M z x 0 wn 0 Q 0 0
North East From To Lopm]IPP-1 IPP-1
B518 494 1 214 1 1 rJ/98 4 1 8 1 1 1 0
8526 478 1 214 11rim 4 1 8 1 1 0 1
BS38 4U 1 300 1113198 4 1 8 1 1 6 .4
111,V98 4 8 66 .8 10 .8
1 9 1114198 4 8 490 153 x x x xix xix xixixlx . x x x x
8668 400 200 1114198 4 8 1 3 .3 1 1 1 1
ORB 400 1 250 1114IS8 4 8 83 .2 3.3 1 1 1
B588 434 208 1114/98 4 8 2.2 1 .5
B61B 480 330 1115/98 4 8 1 13 2.2
B628 440 170 1115W 4 8 1 1 0.2
B638 10 sw 1119/98 4 8 1 0.8 0 .3
B64B 50 550 1119/98 4 8 3.6 0
856B 300 250 1119/98 4 8 2 .4 14 .8 x x x x x A x x x XIX x x x x
B6?B 250 260 1119/98 4 7 .3 T3 1 2 .5 x x x x x x x x
868B 250 200 1119M A a I a I
B698 200 1 200 1119W 4 8 8 1 2 .4 1
B70B 150 200 1119/98 4 8 1 0
B71B 200 150 IIf9198 4 8 1 a
B72B 300 0 1119M 4 8 1 4 .5 1 x x x
B73B 320 215 11/9198 4 8 1 4 .8
B748 350 150 1 11/9/98 4 8 511 158 x X1 x x x x x x x
B75B 350 100 1 1119198 4 8 1 4 .6
B76B 2SO 150 11110f98 4 a 1 3.1
BTTB 300 i5l)11110IN 4 8 1 2 .4
878S 376_L_125 1111Qf98 4 8 1 3.1
-'97-9B 50-0-1 5-50 11/11M 4 1 8 159 1 .2
B80B 600 600 11/11/98 4 a 1 0 .9 1
B81B SW SW 11111/98 4 8 1 0 1
B82B Sw 600 11/11198 4 TA 7 .4 4 0 .8 X X XXXXIXXX
B83B 550 6SO 11111198 4 8 3 .2 1
B84B 600 650 11/11198 4 8 19 1 .1
B858 600 600 li/11198 4 8 14.2 0.2
B86B 600 6150 11/11/98 4 6 32 0 .9
-7FM-TB --j-50- 560 11111198 4 8 18.4 0 .5
jjg-8 6-5-0 600 11111198 4 8 22 0 .6
en-e- --is-o- -iwo -Ti-/i2/w- -4 8 26 1 .8
--ffigS --TOO--650 11112/98 4 1 8 22 .4 1 0 .3
B91B 700 1 600 11112/98 4 8 3 .4 0
892B 700 1 550 11112198 4 8 9 .2 0 X X X X XIX X X X
B93B 7W 600 11130198 4 8 7 .6 0.6
30198B94BSoo4SO111
k
4 8 9.6 0.5
8958 600 500 1 1 W98 4 8 1 0 1
B96B
6so 500 11tXV98 4 8 7 1 .3
8978 650 450 llr"98 4 8 8.3 5.8 3 .210013B95" !EB988
600 410 1211 198 4 8 1 5
B998
650 400 12/1/98 4 8 1 .4 01211W.0
LB 50 500 12/1198 4 5 .8 5 .8 - -
Table V.D.4-2
2 of 3
Table A-1
BURLINGTON MGP SITE
Field Screening and Sampling Summary
Depth Interval: 4'tog '
SAMPUNG DESCRIPTION FIELD SCREEN LABORATORY SAMPLE SUMBITTED
RESULTS
Boring Sampling Sample Sampling Refusal CPAH PID PCB
No.Grid Date Depth Depth
Coordinate Interval 0)conC--I <[feet)<Location are I'lon 0 1- w
detects of w w w 13
n 93 0 0 2 ,-2 ppm)0
0 >w Q 0. 1- 1- 1- 1, 0 InNorth Fast From To EPpm1 101-1 IPPM]
B101B 50 470 12/1198 4 a 1 1 7 4 .2 1B1028041012/l/98 4 8 2 .4 4
8103B so 400 12/1/98 4 a 8 .2 B-7
B1048 100 500 3122/99 4 8 8 0 .5 x x x x x x x x x
81058 100 450 3/22/99 4 6 6 15 .2 0 .1
Sloss 248 559 W22199 4 7 7 2.2 0 .6
B107B 204 60 W22/99 4 6 .6 6.6 1 0 .2
Sloss 142 526 3/22/99 4 6 6 1 1 .8
8,10913 150 460 3123199 4 8 1 1 .2
8110B 329 612 3f23f99 4 8 110.4 1 .3
B111B 1 3112 572 3231QW199 4 1 1 .2
4`18 3123/99 4 8 214 3545 3=2
Table V.D.4-2
3 of 3
Table A-1
BURLINGTON IVIGP SIT E
Field Screening and Sampling Summary
Depth Interval : Il'to 12 '
SAMPLING DESCRIPTION FIELD SCREEN LABORATORY SAMPLE SUMBITTED
RESULTS
Boring Sampling Sample Sampling Refusal CPAH PID PC B
No. Grid Date Depth Depth
Coordinate Interval Conc=1
Location [fed] afe non wdetectsw ar w 000 0 2 reJ<2 pprn)w z < z z c.o.0
() I.) ,0to 1- 0 . 1- 1- 1- w 0 wNorth East From To (Ppm) IM-1 IPP"1 1
BOIC 0 280 10/13198 8 9 9 1 0
B02C so 300 10/13M 8 11 11 1 0.9
603C 100 325 10113198 8 11 .5 11 .5 1 0.2
BW ISO 3so 10113M a 11 .5 11 .5 2 0.1
S06C 200 350 10/13MB 8 12 12 .3 IA 0
1307C $27 271 10/15M 8 12 1
NBC 602 264 10115GS 8 12 4.8 0
Boric 435 274 10115(98 8 12 7A 20
BIOC 485 304 101151911 8 12 2 0 .7
611C 498 285 1 10115198 8 12 154 .8 24 .5
B'12C 4T7 230 1 10/15198 8 1 12 1 1 3
013C 456 1 250 1 10/15tU 11 .51 12.51 1 .2 07
Bisc 100 1 200 1 10/19198 8 1 9.6 1 9.6 9.8 1 .7
B23C 200 1 385 1 10/19198 5 12 18.2 1 .1
B24C 250 1 300 10/21fill) 8 11 .6 11 .6 is 104 x x
B26C 250 400 10/21/98 8 12 20.6 3.2
027C 300 300 10121/98 8 12 11 .4 3.4 1 .1-4 .0 x
B28C 300 350 l0f2l198 8 12 2 .8 2.5
829C 300 400 10121/98 8 12 76.2 1 .1 x x
B30C 350 438 10127/98 8 12 42.6 0 .6--<0 .5B31C350400 10127198 8 12 No Sam
B32C 350 350 10127198 8 12 lu 23 .6 x x x x x x x x x
833C 350 300 1Qf271W 8 12 238 12 x x x x x x x x xB34C 400 450 1012a/so 8 12 73A 0 .2
B36C 400 1 350 10128198 8 12 3.8 1 .3
837C 400 1 300 10128f98 8 12 136 26.7
838C 450 1 450 lQt28/98 8 11 .4 11 .4 152 35
B39C 4W 1 487 10/29t98 8 12 20.4 2 .9
B40C 450 1 400 10/291-98 8 12 220 38.2B41C450350 10/29/98 8 12 3 .6 4 .6
B42C Soo 460 lOr29198 8 12 12 87 3 .2 0.5-1 .0
B43C Soo 400 10129M 8 12 2 .4 3 .4
B44C Soo 500 11/2/98 8 12 1 2 .8 0
B46C 550 Soo 11098 8 12 1 a
846C sw 450 11098 8 12 2.2 0
B47C sw 395 l1r2198 8 12 1 5
B48C Soo 355 11098 8 12 159 78
049C sw 271 1113198 8 12 1 0.4
B50C S20 1 245 1113198 8 12 1 1 .5
B51C 494 214 11ral9a 8 12 1 1-2
852C 478 214 W3198 a 12 1 0 .1
B63C 434 300 11/3198 8 12 1 22.1 x x x x x x xxx
854C 358 228 11/4198 8 12 56A 18 x Ix I IB&-C 389 179 111W98 8 12 94 24 .2
BS6C 400 200 11/4M a 12 3 .2 3 .7867C400 250 1114M 8 12 iss 63
8580 434 208 1114198 8 12 12-2 1 9
B61C 480 330 1115/98 8 12 37 .6 135 .4 X X X X X X X X X
B62C "0 170 1115198 8 12 1 0.2B63C 10 550 1119/98 8 12 1 0.1
B64C 1 50 550 1119198 8 11 11 1 0.5BGSC1 300 250 1119/98 8 12 , 1 22-3
Table V.D .4-3
IoI2
Table A-1
BURLINGTON WIGP SITE
Field Screening and Sampling Summary
Depth Interval : Vto 12'
SAMPLING DESCRIPTION FIELD SCREEN LABORATORY SAMPLE SUMBITTED
RESULTS
Boring Sampling Sample Sampling Rehnal CPAH PID PC B
No.Grid Date Depth Depth L)Coordinate Interval E 0Conc-I <am non w 0 wLocation [fed]<
detawts of w M of w 0, 9 z 0 0
0
0 7
J-*plan), I < z 00 to x
a
w 0Q. 0North East From To [ppmI [Ppm] (Ppm]
868C 250 200 11/9= 8 12 1 1 69.4 0 1 x Xi I it I I I 1 1BTOCISO2001119/98 8 12 1 0
B71C 200 ISO 1119198 a 12 1 0
872C 300 200 11/9198 a 12 14 8 .1
073C 320 215 1119198 8 12 91 .2 S5-6
874C 350 ISO 11/9198 8 12 147 45 .8
B76C 350 100 11/91w 8 10 .7 10.7 1 4.1
876C 250 150 11110/98 8 10 .2 10.2 1 2.7
677C 300 ISO II/I0f98 a 12 2 .4 1 .8
1378C 376 125 11/10/98 8 12 1 2-6
879C 500 6W 1 11/11/98 8 12 1 1-3
B80C 500 600 1 11111/98 8 12 1 0.3
BBIC 550 660 11/11198 8 12 1 0 .2
883C sw 650 11/1I/s8 8 12 1 0 .7
884C 600 650 1111ilga 8 12 2 01
685C Soo Soo II/II/S8 8 12 32.8 0
886C Soo 550 11111198 8 12 25 .4 0 .8
687C 650 550 11111/ss 8 12 22 .8 0 .2
sac 650 600 11111198 8 12 37 .8 31
889C 660 650 11/12/98 a 12 7 .6 1 .9
Bsoc 700 650 11112/98 8 12 62 .6 0.1
891C 700 600 11/12/98 8 12 7.6 2 .3
892C 700 550 11112M 8 12 1 0
893C 750 600 11rJOIS8 a 12 12 1 .6 0 2
894C 600 450 llr3w98 8 12 339 25 .4 x x x x x x x x x
695C 600 600 lIr30198 8 11 .6 11 .6 1 1 .9
896C 1 650 Soo lir"98 a 12 1 0 .8 1 Ix I
898C 600 410 1211/98 8 12 1 4 .4 x x X,X,X x x x x
899C 650 400 12/l/SB 8 12 30.4 0 x x xjxIx x x x x
BIOIC 50 470 1211198 8 12 6 .8 4 .6
B'102C 0 410 12/1198 a 11 .1 11 .1 8 .4 3 .2
8103C so 400 12iliss 8 12 10 6
B104C 100 500 W22/99 8 1 &3 1 8 .3 2 .4 0.7
B109C ISO 450 3r23f99 8 11 .5 11 .5 1 1 0 3
8110C 329 612 3f23/99 11 12 1 ~~8 19 X X X XxBIIIC312 572 3123M 8 1 ;
B112C 418 545 3/23/99 8 iS.4 1 2 .8 x X .
Table V.D.4-3
2 of 2
Table A-1
BURLINGTON MGP SITE
Field Screening and Sampling Summary
Depth Interval : 12' to 16'
SAMPLING DESCRIPTION FIELD SCREEN LABORATORY SAMPLE SUMBITTED
RESULTS
Boring Sampling Sample, Sampling Reftnal CPAH PID PC B
No.Grid Date Depth Depth toCoordinate Intenpal coacc l
Location [feet) are non
delacts w wIn0 0 2 R.0
Q.Q . 0z z(<2 pp 0 0 w
0
. x 0 U ~(o u 0 inQNorth Fast From To (Ppm] Ippml Ipp-I
8070 527 271 10/15(98 12 1 15 CAVED 1 2 .9
808D 502 2S4 10115M 12 1 15 15 1 0 .1
B09D 435 274 110115198 12 16 26A 48 .1 x X1 x X1 xlx x x xlxixlxl x
SiOD 486 304 10115198 12 is 35 .6 34 x xjx xIxlx x x x1XI xjxjx x x
BliD 498 285 10115M 12 Is 1 3.9 1 1 1823D200385 10119198 12 16 1 2 1 1 1026D2SO400101211981216 17A 4 .4
B27D 300 300 10/21198 12 14 14 7 .8 2-3
B28D 300 350 10/21/98 12 12 .5 12.5 0 2
029D 300 400 10/21198 12 14 .6 14 .6 34A 1 .6
B30D 350 438 l(V27/98 12 14 14 67A 0
83110 350 400 l0f27/98 12 16 77.8 1 .2
B32D 350 350 1 10127198 12 15.2 15 .2 37.2 5.2
B33D 350 300 1 10/27198 12 14 14 4 .2 0
B34D 400 450 10128t98 12 16 1123 3.8 x xi
B36D 400 350 110128198 12 16 16 11 .4 0
637D 400 1 300 1 =11198 12 16 112A 2~8
B39D 460 1 487 lQt29/SB 12 16 159.2 8 .6 x x 11
B"D 450 400 10129/98 12 15 .9 15.9 71 .8 13 .4
8410 450 350 W29198 12 16 4 1 .2
B43D Soo 400 11=9198 12 is 21 1 .5
B"D Soo 500 111098 1 12 1 16 1 16.4 0 .2
B46D 550 500 1 If2198 12 1 16 1 1 0
B46D 550 450 11/2/98 12 13 13 1 0
B4'1D 550 395 111098 12 16 1 0.5
B48D Soo 355 1112198 12 16 1 0.2
B53D 434 300 11/3198 12 16 1 8.4
S55D 389 17S 1114/98 12 16 1 12 9
657D 400 250 1114/98 12 16 229 45 .7 x XIX x x x x X1 x
B58D 4u 208 1114M 12 16 1 1 .2 1
B61D 480 330 1115198 12 16 1 3 .6 1
B620 440 170 1115198 12 15.3 15 .3 1 0
S66D 300 250 1 1119198 12 12 .8 12 .8 1 0 .7
B72D 300 200 ii/Siga 12 14 14 13 .8 6-8
B73D 320 2115 1119198 12 13 .1 13.1 26 .8 8 .8
874D 360 ISO 1 1 t9fos 12 13 13 6.4 13.1
B77D 300 150 11/10198 12 16 4.4 2
BTSO 376 125 11110M 12 13 .4 13 .4 1 .6 1A
B79D 500 550 11/11198 12 16 2 1-6
8800 500 600 11111/98 12 16 110.4 0 .4
B81D 550 SH 11/11198 12 15.5 15 .5 1 1 .1
883D sso 650 11111/98 12 16 1 0.6
884D 600 660 11/11198 12 16 2 .4 0
885D 600 600 111/111198 12 16 4 0
886D Soo 550 111/111M 12 16 46 1 1
887D 650 550 11/11/98 12 14 .5 145 72 .6 2 x x x x x x x x x
S881)650 600 11111198 12 16 38 2 .5
B89D V50 650 11T12iga 12 16 28 .8 0
700 650 1 iTi-2/-9s -12-jtff 13 .2 10 .6 0B90D
Table V .D .44
I of 2
Table A-1
BURLINGTON MGP SITE
Field Screening and Sampling Summary
Depth Interval : 12'to 16 '
SAMPUNG DESCRIPTION FIELD SCREEN LABORATORY SAMPLE SUMBITTED
RESULTS
Boring Sampling Sample Sampling Reb~al CPAH PID PC B
No .Grid Date Depth Depth
Coowdmate Interval Conc=l < zLocationtfwlareRan < <
detects M w w 010 0 M EE(~2 ppm)< z o. 0 00 ~z0 0North East From To Ippm) [Ppm] Ippm]
891D 700 600 11/12198 12 16 4.2 05 1 1 1 1B92D700 SW 11/12/98 12 16 6.6 0B94D60045011/30/98 12 16 lee 29896D650 Soo 111/30198 12 15-41 1 3 .4B98D60041012/1198
12 it 15 .4
1 4 .2899D650400 12/1/98 12 16 1 0810111)so 470 12JI198 12 12 .1 12 .1 no ~~M-Ple ad!B103D so 400 12JI198 12 12 .3 12 .3 1 V15578101)329 512 3123t99 12 13 .9 13 .9 1 1 2 18112D41815451 3123/99 12 12 .4 12 .4
Table V.D.44
2 of 2
Table A-1
BURLINGTON MGIP SIT E
Field Screening and Sampling Summary
Depth Interval :> 16 '
SAMPLING DESCRIPTION FIELD SCREEN LABORATORY SAMPLE SUMBITTED
RESULTS
Boring Sampling Sample Sampling Refusal CPAH Pit PCB a)No. Grid Date Depth Depth 2 0Coordinate Interval conc-I
Location [feet)areoW w w
detects 0 0 M R(~2 ppm) 0 z z 00x
North East From To [pp.] Ippm) [PP-]
609K 1 IN ~74
1 12115198,16 , 19 7 .4 1 12.4
810E 48i 304 101151981 16 1 19 38.6 30 .8
831E 3SO 400 1 10/27tS8 16 20 6.4 0.7
NE
400 450 1 10r28198 16
16
.51 16 .5 1149 0.9
837E 400 300 10/2af98 16 20 2 .2 0.1
B39E 450 487 1 W29198 16 17.1 1 17 .1 1193 18 .6
B"E Soo 500 11r219a 16 20"198 --9-3-xw20
54SE 1 550 500 jjt2W 16 20 1 0 .2
B53E 434 300 lIrJ1S8 16 20 1 1 2 .7
B57E 400 250 1114/98 16 20 146 14.6 1 1 1
330 11 6 0 29 .2 1 22.681
-aO SW 15 .9711-19-8 16 2 234
:X:
:*x X X X X,X X X X X X X
OE 600 11111/98 16 no sample collected--aO-
ME 600 600 11111/98 16 16 .2 16.2 no sample collected
B86E Soo SW 11/11198 16 16 .3 16.3 4`1 .8 0 .5
E so Soo ilyll/98 16 16-5 16 .5 87.8 0 .6
i iE
700 600
111ga
16 16.8 168 86.4 2 .3 x X16E
B92F 700 550 11112198 16 18.8 18a 6 .8 0 .3
BS4E Soo 450 1 113019B 16 17 .5 V .5 3.6 1 .7
NB98E Soo 440 1211198 16 185 18.5 1
B99E 650 400 12/1/98 16 20 1
18
r'
IS 51 1 LJ 1 .12
0
23 5 23 5
X
BB10F485 304 10/15198 19 22 39.8 2 722 TJ_-
BSIF 480 330 11/5198 20 23.5 23 .5 25.2 3 .3 x X 1
650
""M8 B
I B79F Soo 550 11111W 20 21
Table V .D-4-5
I Of i
Tabic A-1
BURLINGTON MGP SITE
Method 8270 Analytical Results Summary
Depth Interval :ALL DEPTH S
NON-CARCINOGENS CARCINOGENS
Cc 26 Lu
ut
cPAH a t , z211 -C MO 02 =0 g 6 SC 0 _0 L. a 'i 00 wCvrripvurid;3~ M M E 2 -6 00M
z B -6 -6 L)X0c:c000 20 U
B(a)P Equiv NA NA NA NA NA NA NA NANA NA 0.1 0001 0 1CPF;I I I I I
Sample Concentrations in ppm Non-detects Included at
Location Detects In bold text, Non-detacts in plain text at one-half the detection limit ons-haff the direction limit
B01A 0165 0165 0165 0165 o165 0 165 0.165 0165 0165 0165 0.165 0165 0165 0,165 0185 0.165 0.165'2 .81 I'le 0 .5
B02B 0 175 0175 0 .72 0 175 0 .41 2 .3 0175 3 .1 12 3 .5 3 .9 3 .9 0175 1 .4 4.2 3 .8 2.1 50 .21 27.48 7.17
803A Ole Ols 0 is a Is Dis 018 Ole 018 Ole 018 Ole 018 cis 0 .36 o .ia cis did 3 .24 1 .44 0.42
B04B 017 0 17 0 .17 0 .17 0 17 046 0 17 0 .73 1 .5 017 0 .35 0 .47 017 0 .77 0 .38 017 017 6 .36 2 .48 0.63
BOSA 0 155 0155 0155 0155 0155 0155 0 .155 0 .6 1 .2 0 .72 0.36 0.7 0155 1 .7 0 .37 0 .54 0155 7 .58 3 .97 0.65
B06A 0 17 017 o 1-7 -6-17 o-17- __6 3-5 __01_7 0 .44 _f_3 -ol_7 0.38 0 .43 7 1_7 0 .44 0,17 0.17 0 V 5 .21 1 .93 0.42
B07A 09 09 09 09 09 09 0 .9 0 .9 09 0.9 09 09 09 0 .9 09 09 0 .9 15 .30 6.30 2 .08
B08A 0,17 0 17 0,17 0 17 0 17 0 .58 017 0.81 3 .3 0.53 0.6 0.77 0.17 1 .3 0 .56 0 .46 0.17 10.27 4 .03 0 .87
B09D 3 .4 11 1 7 1 .7 11 3 .6 1 7 13 13 1 7 1 7 11 1 .7 1 .7 1 .7 1.7 1 .7 41 .70 11 .90 3 .93
SIOD 6 .1 25 205 205 2.05 5 .5 2o5 2 05 2,05 205 2 05 205 2 .05 205 205 2,05 205 65.301 14 .35 4 .74
BIIB 270 260 22 22 56 190 44 62 75 22 22 22 22 22 22 22 22 1,176.00 154 .00 60 .84
B12A 0 165 0 165 0165 0165 0 .165 D 165 0165 0 165 0165 0165 0165 0165 0,165 0165 0165 0,165 0165 2.81 1 .16 0 .38
B13A 0165 OA65 0,165 0 .165 0,165 1 0.34 1 .6 2.9 0.78 1 .3 1 .5 0,165 2 1 .2 0.7 0.165 14.48 7.03 1 .60
B17A 0155 0 iSS 0 155 0,155 0155 0,155 0,155 0,155 OA55 0155 0 .155 0155 0.155 0.67 0.155 0.155 0155 3 .16 1 .60 0 .36
Bias 1 6 1 6 16 1,6 16 1 6 1 .6 IS 16 16 16 16 lZ 1,6 1 .6 i's Is 27.20 11 .201 3 .701
o-4-__B23A 09 0,9 09 0,9 09 3 .8 9 .5 15 2 .5 3 .5 4 .7 oe 7.3 3.7 2.5 og 54 .70 23.50 5 .37
B24C 09 09 09 01 09 1 .8 09 1 .8 3 .2 09 01 09 09 1 .8 09 09 0.9 20 .30 7 .20 2 .09
B26B 095 095 095 095 0 .95 4.2 2 .6 6.7 26 3 .2 5 .4 6 .6 0,95 9.3 5.6 3 .3 o .95 78 .45 32.10 7 .61
B27B 09 3 .1 og 1 .9 2 3 .4 o,g 09 2 09 0 .9 09 0.9 0,9 0.9 09 09 23 .20 6.30 2 .08
B288 09 09 09 09 09 09 09 09 09 09 0~9 09 09 0,9 01 09 0.9 15 .30 6.30 2 .08
B29C 2 8 2 8 7 18 5 .6 9 .9 19 2 .2 5.4 5 .4 2 5 .7 3 .8 2 .4 2 108 .40 28 .7o 6 .84
B32C 79 89 51 10 .5 26 79 23 25 33 105 105 105 105 10,5 105 105 10 .5 499 .50 7350 24 .27
833C 20 68 95 95 39 160 20 59 98 95 34 31 95 35 21 9 .5 95 642 .00 149 .50 36.18
B368 10 .6 27 22 41 170 390 52 110 230 105 65 60 10 .5 56 27 io5 io .5 1,302 .50 239 .50
"."834D 30 22 11 34 25 47 11 11 22 11 11 11 11 11 11 11 11 301 .00
77 .00,
2!1.421
Table V.D .4-6
1 of 3
Table A-2
0
BURLINGTON MGP SITE
Method 8270 Analytical Results Summary
Depth Interval :ALL DEPTHS
NON-CARCINOGENS CARCINOGEN S
0 62 cc Cc cc L)E z
UE or202!
PAH a Q.UCompound:Z Lu 1K 100zWU
UIr<
B(s)P Equiv NA NA NA NA NA NA NA NA NA NA 01 0.001 0 .1 LLCPF1I I I I I I I I I I I I o 'To of 71 1
Sample Concentrations in ppm Non-datects Included at
Location Detects in bold text, Non-detecis in plain text at one-half the detection limit on"aff the detection limit
939D 320 490 44 350 340 710 250 200 350 17 .5 17.5 17 .5 175 so 64 17.5 17.5 3,303.00 231 .50 87 .57
B42B 32 42 21 29 38 99 25 31 56 9 .5 9,5 95 95 S5 as 95 9 .5 449 .00 68 .50 21 .95
B44E 9 5 56 9,5 50 41 81 22 21 32 95 9 .5 95 95 SS 95 95 9 .5 398 .00 6850 21 .95
8468 10 5 10 .5 105 to 5 105 105 105 10's 23 to,5 10,5 105 105 10 .5 105 105 10.5 191 .00 73 .50 24.27
B48B 12 15 0 .48 0 .58 0 .73 1 .8 0 .43 0.46 0.92 022 022 022 022 022 0,22 022 022 34 .15 1 .54 0.51
B50A 10 10 10 10 10 10 10 10 10 10 10 11 10 10 10 10 10 170 .00 7000 2311
B53C 95 47 95 95 23 43 95 95 95 95 95 95 S5 95 95 SS 9 .5 248 .00 66 .50 21 .9!
B55B 520 730 62 220 200 460 140 170 330 27 83 77 laS 74 62 25 lo5 3,201 .00 342.00 86 .17
857D 53 100 10 10 32 78 20 23 35 10 10 10 10 10 10 10 10 4411 .00 70.00 23 .11
B61C 5 .9 to 11 11 3 .6 6 .4 1 029 oil 1 1
11 0,19 0 1 IQ 0 1 159
.80 77,001 25 .42
861F 0,19 019 1 019 1 019 13,19 0 19 1 19 0.19 0 .19 0 1 9 ~1, 1 119 1 3.23 1 .33 0 .44
B63A 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 170 .00 70.00 23.11
866C 0195 0195 0 .195 0195 0195 0 195 0 195 0,195 0 .195 0.195 OA95 0,195 0195 0 195 0,195 0196 0 .195 3 .32 1 .37 OAS
B67B 020 020 020 020 020 020 020 020 0,20 020 0,20 020 0 .20 0,20 0.20 020 0,20 3 .40 1 .40 0.46
869C 1 15 1 is 1 .15 1 is 1 .15 1.15 1.15 1 .15 1,15 1 .15 1,15 1 15 1 .15 1 .15 115 115 115 19 .55 8.05 2 .66
B76A 10 10 10 10 10 10 to 10 10 10 10 10 to 10 10 10 10 170 .00 70 .1)0 203 .4191
B711A 021 021 021 021 021 021 021 021 021 021 0,21 021 0.21 021 0 .21 0,21 021 3.57 14 7
B82B 1 9 1 9 1 9 1 .9 1~9 1 9 1 .9 1.9 1.9 1 .9 1.9 1.9 1.9 1.9 1 .9 1 .9 1 .9 32 .30 13 .30 4 .39
BSSA 95 95 95 95 95 23 9 .5 19 19 95 9S 95 9,5 95 S5 9.5 9.5 194 .00 66.50 21 .95
Table V .D.4-6
2o(3
Table A-2
BURLINGTON MGP SITE
Method 8270 Analytical Results Summary
Depth Interval ;ALL DEPTHS
NON-CARCINOGENS CARCINOGENS
ccJI?c c w129a 0
zPAHz z c L)a C, 0 IF jc~ wCompound:A g BEcIZ0z'6 8 Q.ON .0 z< c c
to to We c
B(&IP E W NA NA NA I NA NA I NA NA FNAJ 1 .1 boot 0 '~ 0 .11 1 0.1 1CPF7u NA NA i i i I
Sample Concentrations in pprn Non.deted$ Included at
Location Detects In bold text, Non-detects in plain ted at one-half the detection limit orte-half the detedlon limit
8870 11 11 11 11 11 11 11 11 it 11 11 1 1 11 it 11 1 1 if 187.00 77.00 26 .42
890A 95 95 95 95 95 95 95 95 9's 95 95 as 95 93 95 95 93 161 .50 66 .50 21 .95
891E 1 9 1 9 1 .9 1 9 1 .9 10 1 .9 3 .9 4 .2 1 .9 1,9 1 9 1 .9 1 .9 IS 1 .9 1 .9 44.70 13 .30 4.39
B928 20 20 2 0 20 ]20 20 20 20 70 20 20 2,0 20 2 .0 20 2
0
2o 34.00 14 .00 4.82
B94C 300 400 11 160 120 280 70 61 110 11 31 26 11 23 22 11 11 1 1 .650 .00 135.00 38.56
B98C 023 023 023 023 023 023 023 023 023 023 023 023 023 023 0.23 0,23 023 3.91 1 .61 0.53
899C 021 021 021 021 021 021 021 021 021 021 021 0 .21 021 0 .21 021 011 0.21 3.57 1 .47 0.4
13100A 0,95 095 095 0.95 0.95 2 .1 095 3.1 4.4 2 .6 2 2 .3 o,95 4.8 2.8 2.3 0 .95 34 .00 16.10 4.33
B104B 205 205 2.05 205 2,05 2 .05 206 4.6 8 .7 205 205 2 .05 205 10 4.3 2 .05 2 .05 $4,15 24.55 7 .07
B110C 225 2,26 225 2 .25 2 .25 14 225 14 1 19 225 6 .5 8 .3 1 2.25 11 6 .3 2,26 2 .25 101 .60 38 .85 9 .77
B112C 2 .4 2 .5 2.5 2 .5 2S 2 .5 25 5 11 25 5 5 .6 2 .5 8.4 5 21 2 .5 67 .30 31 .40 8 .69
B112D 1 .85 1 .85 11 6 .9 20 130 41 44 84 1 4.9 1 26 1 22 1 .85 20 1 16 1 5 .6 1 .85 438 .80 93 .30 21 .42
4601 221 801 641 25 2
2212.4991 4061 1 .0721 I .E lei 2851 4751 2551 5411 4321 284 72i57
%Total PAHs :1 10.8%.5%1 17 .8%1 5.1%1 6 .0%1 ID . 1 .5%1 3 .3%1 2 .6%1 1 .7%1 1
.6%1
TOTAL PAH9 for ALL DEPTHS -
S!TOTAL CARCINOGENIC PAHs for ALL DEP -2,703
%Carcinogenic PAH9 - 1 16.4%
TOTAL CARCINOGENIC PAH& as B(a)P Equiv for ALL DEPTHS -
Table V .D.4-6
3 of 3
Table A-2
BURLINGTON MGP SIT E
Method 8020/8260 Analytical Results Summary
Depth Interval :ALL DEPTHS
c C
C XWNNa W c QLUUj C (1)
M 3~r 2 :2 _jCompound:4,M
a JQ >5 '51 W00 96 E E CLCLF_2 5 00 E a Jl~z0 Q. th v e
C6 C4
Sample Concentrations in pipm
Location Detects In bold text, Non-detects in plain text, shown at one-half the detection limit
0~.101 010 7BOIAU07 0,007 0.007 0.007 0 .007 0.014 0.007 0.007 0.007 0.007 0 .007 0.007 0 0.042
B028 0009 0,009 0.009 0,009 0.009 0,018 0.009 0 .009 0.009 0.009 0.009 0
.009 0~ 0~oos
0,054
B03A 0 .008 0 .008 0.008 0 .008 0.008 0,017 0.008 0 .008 0 .008 0,008 0 .008 0 .008 0.008 0 .008 0 .049
B04B 0 .006 0,006 0,006 0 .006 0.006 0 .013 0.006 0 .006 0.006 0.006 0.006 0.006 0 .0156 0 .006 0,037
B05A 0006 0 .006 0 .006 0.006 0.006 0 .013 0006 0 .006 0,006 0 .006 0 .006 0 0.006 0 .037
_0 14 007 .007 .007 .007 .007 0 .007 0 .007 0,007 0 .042----6 .007 0 .007 .007 007 OM7 .01306A06
807A 0 .006 0.006 0 .006 0,006 0 .006 0.013 0 .006 OM6 0.006 0.006 0,006 0 .006 0.006 0 .006 0 .037
B08A 0 .006 0.006 0 .006 0,006 0 .006 0.011 0.006 0.006 0.006 0.006 0 .006 0 .006 OoDe 0 .006 0 .035
B09D 0,9 0.9 0~9 0 .9 0 .9 1 .8 09 0,9 O's 0.9 0 .9 0 .9 0.9 3 .6 5 .4
810D 0 .95 0.95 0 .95 0 .95 0~95 1 .9 0 .95 0.95 0.95 0 .95 0.95 1 .4 0 .95 4.8 5 .7
B11B 4 .1 4 .1 4 .1 4 .1 4 .1 6 .5 4 .1 4 .1 4.1 4 .1 4.1 11 4 .1 480 24 .9
B12A 0,006 0,006 0 .006 0.006 0,006 0 .01 0 .006 OMS 0 .006 0 .006 0.006 0 .006 0.006 30 0 .034
B13A 0,005 0.005 0.005 0 .005 0 .005 0 .01 0 .005 0 .005 0.005 0 .005 0.006 0 .005 0.006 0 .005 0.03
B17A 0,004 0 .004 0 .004 0,004 0,004 0.008 0 .004 GoN 0 .004 0 .004 0o04 0 .004 0,004 O .OD4 0 .024
BIBS 0.004 0.004 0.004 0 .004 OM4 0.008 0 .004 0 .004 0 .004 0 .004 D.004 0.004 0 .004 0,004 0,024
D6B23A0.006 0.006 0.006 0 .006 .006 0.011 006 006 006 .006 0.006 0.006 0 .006 00 0 .035
824C 0,006 0.006 0.006 0 .006 OM6 0.012 0 .006 0 .006 0.006 0.006 0 .006 0,006 0 .06 0 .006 0 .036
B26B 0.006 0 .006 0,006 0 .006 0 .006 0 .013 0,006 0 .006 0.006 0.006 0 .006 0 .006 0,006 0 .006 0 .037
B278 0,028 0 .028 0 .028 0 .028 0 .028 0,055 0.028 0.028 0 .028 0,028 0 .028 0 .028 0 .028 0.21 0 .167
B288 0~95 0 .95 O~95 0 .95 095 1 .9 095 0 .95 0.95 0.95 0 .95 0 .95 0 .95 3.4 5 .7
B29C 2 .2 2.2 2 .2 Z2 2 .2 4.4 2 .2 2.2 2.2 2.2 2.2 2.2 2 .2 20 13 .
B32C 0 37 1 0 37 1 0 .37 0 .37 3 .3 1 .6 1 0 .7 1 0 .62 O~37 1 0 .37 1 1 .1 1 2.6 0 .37 1 71 6.24
Table V .D .4-1 3
i of 3
Table A-3
BURLINGTON MGP SITE
Method 8020/8260 Analytical Results Summary
Depth Interval :ALL DEPTH S
:S NUjr4)C C a)
MCompound:
2a 0 0 to E E CL C L
0 a 2 0 M 0W 0 zCC6cli
Sample Concentrations in pp m
Location Detects In bold text, Non-detects in plain text, shown at one-half the detection limi t
B33C 0.17 0.17 0 .17 0 17 0.6 0 .345 017 0 .17 0 17 0 1 0 .17 0.42 0.17 9.1 1 .455
B36B 0 .032 0.032 0 .032 0,032 0.34 0 .065 0.032 0 .032 0 .032 0.032 0.032 0 .097 0 .032 0 .69 0.501
B34D 0A 0 .4 0A 04 0 .76 0 .8 04 04 04 04 0 .64 1 .6 0.4 54 2.76
B39D 0 .4 0 .4 0 .4 0 .4 3 .9 2 .5 1 .2 0 .4 0.4 0.4 0 .92 2.6 0 .4 17 8.4
B42B 0 .175 0 175 0 .175 0 .175 0.42 0 .36 0 .26 0,175 0 .175 0.175 0 .28 0.66 0 .175 29 1 .39
____ff_4_4E 0 .7 0 .7 0 .7 -0 7 0-7 1 .4 0.7 -0 7 - 03 0_7 0-7 0-7 0 .7 Is 4 .2
846B 0005 0 .005 0 .005 0005 0 .005 0.01 0 .01 0 .005 0 .005 0 .005 0,005 0 .005 0 .005 0 .017 0 .03 5
B48B 0 .25 0.25 0 .25 0 .78 4 .1 22 11 0 .25 2.5 1 .4 it 34 0 .25 57 38.13
1350A 0.005 0.005 0.005 0.005 0 .005 0 .01 0.005 DM5 oo05 0 .005 0.005 0 .005 0 .006 0 .005 0 .03
B63C 0 .005 0.005 0 .005 0,005 0 .005 0 .01 0.005 0 .005 0=5 0 .005 1 0 .005 0,005 1 0 .005 0 .005 0 .03
B65B 0.75 0.75 0 .29 Is 87 89 45 8 .1 075 0 .75 23 as 9.8 210 236 .90
B57D 034 D .34 O~34 0 .34 0 .57 0 .7 0 .34 0 .34 0 .34 0 .34 1 2 .5 0 .34 88 2 .29
561 C 0,26 0 .26 1 .1 0 .26 8 .1 6.6 3 .3 0.47 0 .26 0 .26 1 .2 3 .1 0 .62 9 .1 19 .36
B61 F 0 .005 0 .005 0,005 OM5 0,005 0 .01 0 .005 0,005 0,005 0 .005 0,005 0 .005 0.005 0 .005 0.03
863A 0,005 0 .005 0,005 0 .005 0005 .005 0.005 0 .005 0 .005 0.005 1 0 .005 0.03
018 is 0.01 :B66C 0 .018 0 .0T8 001 018 0,618 0'2.60~14 0,0 8 0 .018 0~018 0 .018 .018 0.018 0 .11 0 .10600
B68C 0 .006 0,006 0.00 0,0112 O .OD6 0.006 0 .006 0.006 0 .006 0 .006 0.006 0 .006 0,036
876A 0.005 0,005 0 .00 0 1 0 .005 0 .005 1 0 .005 0.005 0.005 0.005 0 0 .005 0 .0 3
Table V.D.4-13
2 of 3
Table A-3
BURLINGTON MGP SITE
Method 802018260 Analytical Results Summary
Depth Interval :ALL DEPTHS
a C4)0 0C X
r 4)4)C U .1
uj W c N 0 C S!
M :2 MCompound::E
2 2 2 c
a M 0 2 E E CL
0 JM E 2 ZO 0ui0
Sample Concentrations in pp m
Location Detects in bold text, Non-detects in plain text, shown at one-half the detection limi t
B78A 0,006 0 .006 0 .006 0,006 0 .006 0.011 0 .006 0,006 0 .006 0.006 0.006 0.006 0 .008 0.006 0,035
B828 0 .006 0 .006 0,006 0.006 0,006 0 .011 0.008 0 .006 0,006 0.006 0,006 0 .006 0 .006 0.006 0.035
885A 0 .006 0,006 0 .006 0006 OM6 0 .012 0 .006 0.006 0.006 0.006 0.006 0 .006 0 .006 0 .12 0,036
B87D 0 .009 0 .009 0 .009 0 .009 0 .009 G.M 0,009 0.009 0.009 0.009 0.009 0.009 0 .009 0 .009 0.064
B90A 0,006 0006 0 .006 0,006 0.006 0,011 0.006 0,006 0,006 0,006 0 .006 0.006 0.008 0 .006 0 .035
B91E 0,012 0.012 0 .012 0,012 O~012 0.023 0.012 0.012 0.012 0 .012 0 .012 0.012 0 .012 0.12 0 .071
B928 0 .006 0.006 0 .006 0.006 0,006 O~012 0.006 0,006 0.006 0 .006 0.006 0 .006 0.006 0 .006 0 .036
B94C 3 .4 3 .4 3A 3 .4 3 .4 7 3 .4 3 .4 3.4 3.4 3 .4 4.8 3 .4 300 20 .6
B98C 0006 0 .006 0 .006 OMS 0.006 0 .012 0006 0 .006 0.006 0,006 0,006 0 .006 0.006 0,006 0 .036
B99C 0 .004 0 .004 0 .004 0 .004 0,004 0 .008 0 .004 OoD4 0 .004 0 .004 0.004 0 .004 0.004 0
.
004 0.024
B100A 0 .006 0 .006 0,006 0 .006 0,006 0,012 0 .006 0.006 0.006 0.006 0.006 0 .006 0.006 0.006 0.036
8104B 0 .002 0.002 0.002 0 .002 0 .002 0 .0035 0 .002 0.0035 0.0115
B110C 0,0015 0,0015 0 .0015 0.0015 0 .0015 0o035 0 .0015 0 .0035 0.0095
B112C 0 .002 0 .002 0 .002 0 .002 0.002 0.004 0 .002 0 .004 0.012
B112D 0 .002 0 .002 0 .002 0 .002 0 .002 0 .0045 0 .002 0 .08 0,0125
B114C 0.004 0.004 0 .004 0.004 0 .008 0.004 0,004 0 .008 0 .024
Total Number of Samples =F__7561
Number of Non-Detects = 1 321
%Non-Detects = f-5-7-17-/.
Table V .D .4-1 3
3 of 3
Table A-3
PI~M~WAY
r ---- ---------------- -- -
44 lit
if
------------
JEFFRIES HI
opkau,
JOE5 E) cms
COLLI 5.4TNL'DT
NORTH ~A3N STREET
V% ~j
OPERATIMBUM
Lr
JJ
Z TZE
D~ER-IT
/f
UNEV%W~U~Ml)~W
N I
PIEDWO INATURk'GAS Ico N 0
,"BLDG/I,BLDG/ 0 -
&
QUIGEF~R/6LN BURUNGTON MGP SITE
HISTORICAL MGP
SITE FACILITIE S
APPROXIMATE LOCATIONS
PAII4 Y STKET rigure A-3
z
PIEDMONT WAY
JT
CDm
ax
m
APPENDIX B
GROUNDWATER ANALYTICAL LAB REPORTS
Burlington MGP
July 2003 Groundwate r
Field Analytical Data
Field Calibration Fornis
Groundwater Monitoring Data Sheet s
Chain Of Custody Records
Laboratory Analytical Data
Burlington MNA Proposal /Appendix B
BURLINGTON OPEO INS CENTER -MGP SITE
GROUNDWATER N .-MTORING FIELD DATA
SAPROLITE WELLS
AVG
WELL DEPTH TO PROD PUMP WELL EVAC WELL EVAC SPECIFICWELL DEPTH WATER LEVEL RATE -VOL VOL VOL VOL EVAC TEMP PH CONDUCTANCE DO ORP TURDDATE- NO .(fact) ffeei) (rect) ODOR (entlenin) (liters)(lit'.) (go,) (go') Oasl .o) (d,g Q DmIts)(trenhods.) (mg/1)(mV) INTO)7124/03 PMWB-D 18.18 7.56 NONE MINOR 165 6.56 9 .46 ).73 2 .50 NO 20.4,20.3, 20 .3 6.4, 6.4.6 .4 339,340,339 0 .05,0.07.0,05 128,128,127 0.93, 0 .95,0.827/22/03 PMWC-D 25 .20 12~70 NONE NONE 91 7.72 9,46 2 .04 2,50 NO 22 .1,221.22 .2 6.5 .6 .5,6.5 519,519,520 0 . 10, 0.08, ll 122,122, 122 0 .68,0 .38,0.48W221103 PMWF-D 16.32 7.47 NONE MINOR 287 5 .46 5,69 L" 1 .50 YES 18 .3,18 .5 6 .9,6 .9 1010. Hm 0 .46 .0 .19 52,52 61,12A7/22103 PMWG-D 19.07 8.54 NONE NONE 161 6 .50 10 .41 1 .72 2 .75 NO 19 .7,19.7,19.6 6.4.6 .4,64 536,540.538 0 .10,0.09,0 .08 216,213,211 0 .98,1 .3,1 .1712U03PMWI 16.12 11 .32 NONE NONE 55 2 .96 4.60 0 .78 1 .22 NO 25 .0,25 .2.25 .2 7.0, 7 .0, 7 .0 412,415,417 1 .47,1 .29,1 .16 109,103,100 3.8,4.7,5 .17/24/03 PMWL-D 9 .70 2 .95 NONE NONE 103 4 .17 8.52 1 .10 2 .25 NO 22 .0,22 .0 6,2,6 .2 2M,265 0 .16,0 .29 261 .261 4 .9,4,5
OVERBURDEN WELLS
AVGWELL DEPTH TO PROD PUMP WELL EVAC WELL EVAC SPECIFICWELL DEPTH WATER LEVEL RATE -VOL VOL VOL VOL EVAC TEMP FEE CONDUCTANCE DO ORP TUR11DATENO.(feel)(feet)(feet)ODOR DaVol (liters) (liters)(go[) (go')(ye~no)(d,g Q (units)Durnholcin) (rit (mv) (NTU)7/2903 MWA 22 .24 11 .40 NONE NONE 270 6 .69 11 .36 t .77 3.00 NO 19 .0, 19.0, 19.1 5.6.5 .6,5~6 126,126.126 0 .25, 0.25, 0 .25 414,416,421 34,30,297/22/03 MW-5 13 .54 5 .51 NONE NONE 63 4 .96 6.62 1 .31 1 .75 NO 22 .7, 22 .8, 22 .9 7 .0, 7 .0, 7 .0 993,994,994 0 .68,IL46 .0 .33 96,95,94 4 .2,3.9,3 .17/24103 MW-9 9 .50 NOTE I NOTE I NOTE I NOTE I NOTE I NOTE I NOTE[ NOTEI NOTEI NOTEI NOTEI NOTEI NOTEI NOTE) NOTE]7124103 PMWTI-S 13 .58 7 .42 NONE MINOR 55 3 .80 568 I .W 1 .50 NO 25 4 . 24 .9, 24.2 61,61,6.8 790,792,789 0 .08,0 05,0,04 67 .66, ~ 3 .5,107122103PMWC-S 21 ~09 11 .39 NONE NONE 156 5,99 11 .36 1 .58 3,00 NO 21 .1, 21 .2,21 .2 6~5 . 6 .5,6.5 452,457,459 0 .05,0.04,0 .05 92,90,89 7 .4,5.4,6,37124103 PMWL-S 7 .60 2 .98 NONE MINOR 63 2 .85 6 .62 0 .75 1,75 NO 243 . 24 .3, 24.3 63,63 . 6.3 463,456,453 0 .19,0,17,0 .17 143, 145,147 11 5 .9,5,9,4712;/03 PMWM-S 12,68 10 .29 NONE NONE 271 1 .48 T57 0.39 2,00 NO 19 7,19,7,19.6 SA, 5 .4, 5 .4 120,121,121 1 .70,1 .67,1 .68 523,522,522 1 .2,OS2, 0o77124103p-I S 11,7[ 6 .59 NONE NONE 103 3 .16 3 .50 0,84 0 92 NO 26 .6,26 .7, 26.6 65,6,5,6.5 911, 912, 912 0 .07 .0 06,0 .05 222,224,225 4 .7,2 8,2o
SHALLOW FRACTURED BEDROCK WELLS
AVG
WELL DEPTH TO PROD PUMP WELL EVAC WELL EVAC SPECIFICWELL DEPTH WATER LEVEL RATE VOL VOL VOL VOL EVAC TEMP pH CONDUCTANCE DO ORP THEIRDATE NO .(feet) (real)(feet)ODOR (liters)(liters)(go,) (go') (Y'.1 .0) (dag Q (tarth.)Durnho/cm)(mg/1)(-V) (NTU)7/25103 DMW-1 29 .02 5 .22 NONE NONE 480 14,69 20 .82 3 .88 5.50 NO 18 .7,18 .6,18 .6 6.0.6.0, 6 .0 107,107~ 107 0.09,0.06, 0 .06 322,320 .320 3 .0,2.8,2o7/24/03 DMW-2 32 .08 6 .63 NONE NONE 223 15.71 19 .87 4 .15 5.25 NO 20 .7,20.8,20.8 6.4,6.4.6 .4 408,408,412 O~N, 0.05, ON 154,154,153 1 .4,1 .17/22/03 PMWC-E1R 36 .00 11 .30 NONE MINOR 843 15.25 28 .39 4 .03 7.50 NO 19 .1, 19 .1, 19 .0 6.5 .6.5,6 .5 462,460,460 0.06,0.06, 0 .07 121 .119,118 4.9 .2.7,207122/03 PMWH-BR 20 .72 7 .78 NONE NONE 253 7 .99 13 .25 2 .11 3 .50 NO 17 .9, 17 .8, 17 .8 6 .5,6.6,6 .6 466,464,464 0.03,0 .05, 0.03 71,69 .67 0.43,0 .29, 0 827/21/03 PMWI-BR 38 .07 9 .58 NONE NONE 329 17.59 24 .60 4~65 6,50 NO 19.6,19 .7, 19 .6 6 .7,6.7 .6 .7 5%,587,586 0.03, 0 .02,0.03 126,128,128 1 .5 .0 .97,0 .937/24/03 PMWL-BR 24 .46 4 .96 NONE NONE 388 12 .N 17.03 3 .18 4 .50 NO 19.4.19 .3, 19 .3 6 .5, 6.5,6 .5 297,302,301 0.04, 0 .05,0.04 230,229,228 0,83, O~71, 0.717/21/03 PMWM-BR 19 .16 10 .49 NONE NONE 163 5 .35 7.57 1 .41 2 .00 NO 20.4, 20.4, 20 .4 5 .9,5 .9,5 .9 233, 231,231 0.07,0 .08,0.06 277,282,286 1 .4,1 .1, 1 .4
COMMENTS :
Water levels and well depths are merenceti to top of PVC casing ,
-Avg pumping rate used to minimin or stabilim drawdow, while removing me well volume and stabilizing indicator parameters Samples were collected at or v, 100 m1main.NOTE 1)Well was inaccessible due to 4 rs of overgrowth, fallen treas and "all dumping in the area.
FIELD SAMPLING CALIBRATION DATA FORM
STUDY ;DQXt.~GTO(-J my-XC4
DATE:03-WEATHER CONDMONS,-7 0 -2,~OFI,ralpr~
COLLECTORS: O-UL"~SURFACE UNrr READER
:
HYDROLAD SERIAL 8:3 42 46 COMPUTER:
OTHERrouiPMENT : IrMW (UNX4Z'V%V-TEM-- SURVEYOR SERIAL
Procedure Number 3210 .1
Calibration Time Time 0 .5(0 Time 0 S", 0 Tim e
Barometric
mmHg mmHgPressure? 5 -7 .~!mmH g
Instrument Standard Instrument Standard Instrument Standard7~~Value Value Value Value Value Value
Thermomete r
No .yj
TEM P
(deg C)
W
DO W
(mgA)W
AW >
pH B 0 >7 .00 '?eO 7.00 >7 .00
(units) B C~O >4 .00 0 4 .00 >4 .00
8 > 10.00 10 .00 > 10.00
SPCOND SS 01 .0 > 0 .00 0 .00 > 0 .00
(US/Cm) SS g;; q?.> 6 >
SS > >
ORP SS y;?O >;6zo Cf ;2,>
(MV) SS >>
TURBIDITY SS
t-1 t-14 > 0 .00 tj 0 .00 > 0 .00
(ntu)SS
>
>
KEY:8 =Buffer W =Winkler NA Not Applicable
SS =Standard Solution AW =Average Winkle r
> =Adjusted To -- / -- > =Not Adjusted To
FIELD SAMPLING CALIBRATION DATA FORM
STUDY :'pJvx~-Z'tJ ceyo-j M C.,-P
DATE, -1 1 ;t-t (LT 3 WEATHER CONDMONS :4ok ,CA-Car-V ct a
COLLECTORS:%2z~o N&6c~SURFACE UNff READER: L-~C,
HYDROLAS SERIAL #:73 %C)COMPUTER :
OTHER EQUIPMENT:R15 (,LJ `TVN6Z0""Td& SURVEYOR SERIAL #:
Procedure Number 3210.1
Calibration Time Time 0 Qi RD Time Time
Barometri c
Pressure mmHg mmHg mmHg
Parameter Calib . Instrument Standard Instrument Standard Instrument Standard
I Value Value Value Value Value Value
Thermometer
No .JJ
TEMP > > >
(deg C) > > >
W -,5,s
DO W
(mv)W
AW > > >
pH 8 > 7 .00 > 7 .00 > 7.00
(units) B >4.00 >4 .00 >4 .00
B > 10 .00 > 10 .00 >10 .00
SPCOND SS 0 .0 > 0 .00 > 0 .00 > 0 .00
(US/CM) SS ----> > ->
SS > > >
ORP SS 1-124 >Y :Zo >>
(mv) SS - > > > -
TURBIDITY SS tj tA->0 .00 > 0 .00 >0.00
(ntu)SS >
KEY : B ~Buller W =Winkler NA Not Applicable
SS =Standard Solution AW =Average Winkle r
-- -- > =Adjusted To -- / -- > =Not Adjusted To
FIELD SAMPLING CALIBRATION DATA FORM
STUDY:ibu&,-~fj C;'TOIJ r-,/A a P
DATE :-2-9-1 n 3-WEATHER CONDMONS : at Z) lz>K-Cly A~Xuy CA-0 --D
COLLECTORS:SURFACE UNIT READER : 'La C-
HYDROLAB SERIAL #:COMPUTER:J~D C-
OTHER EQUIPMENT :SURVEYOR SERIAL-kAr
Procedure Number 3210 .1
Calibration Time Time t>J 0'0 Time -?30 Time
Barometri c
Pressure mmHg q 5',9 mmHg mmHg
Parameter Calib . Instrument Standard Instrument Standard Instrument Standard
I Value Value Value Value Value Value
Thermomete r
No .tj
TEMP >
(deg C) >>
W Li
DO IN
(MgA)IN
AW 4 . A,3 >6-5 >
pH B , 7 .00 7.7 .00 > 7 .00
>4 .00 >4 .00 >4 .00(units) B
> 10 .00 > 10 .00 > 10 .00
SPCOND SS >0 .00 (D ,> 0.00 > 0 .0 0
(US/CM) SS -211S >-7j-s~7;z2( ->7 .) o >-
SS > >
ORP SS -Yi 8 >!yzo >Z19 >
(mv) SS > ->
TURBIDITY SS (A- > 0 .00 0 .00 > 0.00
(n1u)SS
KEY :B ~Butler W =Winkler NA Not Applicable
SS =Standard S0lUti0r1 AW =Average Winkle r
-- -- > =Adjusted To -- / -- > =Not Adjusted To
FIELD SAMPLING CALIBRATION DATA FORM
STUDY :0,i'l-L-l"i C-k U-J
DATE: C,WEATHER CONDITIONS :VA-rW CLD--&y
COLLECTORS :SURFACE UNIT READER :
HYDROLAB SERIAL COMPUTER :kZC q
OTHER EOUIPMENT :SURVEYOR SERIAL C
Procedure Number 3210 .1
Calibration Time Time 0 :j I Time Time
Barometri c
Pressure 75 mmHg mmHg mmHg
Parameter Calib . Instrument Standard Instrument Standard Instrument Standard
I Value Value Value Value Value Value
Thermomete r
No .rJJ A
TEMP > > >
(deg C) > >
W 0101
DO W
(mg,l)W
AW >01 >
pH B > 7 .00 > 7 .00 > 7 .00
(units) B cl
> -
4 .00 >4 .00 >4 .00
B > 10 .00 > 10.00 >10 .00
SPCOND SS > 0 .00 > 0.00 > 0.00
(US/Cm) SS ~,t 0 0,> > ->
SS > > >
ORP SS Vc_ > >
(mv) SS
4/,2_C>__/> _ >>
TURBIDITY SS > 0 .00 >0.00
(ntu)SS ----> >
KEY: B =Buffer W =Winkler NA Not Applicable
SS =Standard Solution AW =Average Winkle r
> =Adjusted To -- / -- > =Not Adjusted To
DUKE POWER COMPAN Y
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
ILOCATIoN TON, NC PROC NO :
IPROJECTN ME:IBURLINGTON MGP .LSAPROLITE WELLS)FIELD CREW :
SAMPLING DATE: 24-Jul-0 3
MONITORING WELL NO .PMWB-0
WATER LEVEL METER SIN :N/A
PID READING
M
PRODUCT LEVEL METER SIN :Vk-tE,I
METHOD (Pump /Ball)IPERiSTALTIL:P~Ump TIME /INITIALS OF COLLECTED SAMPLE:
WELL VOLUME CALCULATION:
WELL WELL WAT CONVERSION F WELL7
ICOLUMN ft X FACTOR aAajlDIAMDEPTH(ft)OL_
2-18 .18 0 X 0 .163 1
X
lions X 3 .785 N/A liters
k L
D DETECTED ODORS FREE PRODUCT MEASUREMENT
68 ft .TYPE*-14K, DEPTH TO WATER :
STRONG :DEPTH TO PRODUCT :--- v 0 fj tE (ft)
MIN,PRODUCT TI (ft)
PUMP INTAKE NONE!DON'T SAMPLE IF THICKNESS >OR =TO 0 . 1 FT !
AT START AT iND
17.5 It ft.
pH ORP DISSOLVEDWA Tff FLOWRATE TEMP SPEC TURBIDIT Y
TIME LEVEL COND OXYGEN
(hh :mm :ss)(ft)(ml/m n)(deg C) (US/cm)(ntu) (unit)(Mv)(mqA)
ci .(.-? 1-5?,k -') 5- 1^ 1 ~ tj
F- C-AeJ L~UG kiE
w-A-:)L ck,69 IG c F?.-33 cl . 4 o,ck3 4,39 /;,9 005
1 ~l 1 05 12, 1- q ~-?t2O aO,Z5 3-31,9 0,95'4,?g (-~-g I 0-cf?
i It%(;Z,53 9,15 9-34 .4 0 -16 ;L G,39 (2-1 c-). o 5
A-,L-*w 'A
ELECTRONIC FILENAME -fn V-)c
COMMENTS=P Ab 4m(-
tjo-\,C-l -t?JAA z4uy
\jJtA A -c um~r~n,\-
NOTE :WATER LEVEL,PRODUCT LEVEL,AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
DUKE POWER COMPAN Y
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
JILOCATION :BURLINGTON, NC PROC NO :3500 .1
PROJECT NAME :BURLINGTON rLP!nOfE WELLS)FIELD CREW :LDC,RLW
SAMPLING DATE:-24-4uFeOr
22
~-u
MONITORING WELL NO .
PMWC-D WATER LEVEL METER SIN :N/A
PID READING fit lk.-PPM PRODUCT LEVEL METER S/N :
METHOD (Pump I Ball)JPERISTALTIC PUMP I TIME / INITIALS OF COLLECT PLE :,L 12C_9 C
WELL VOLUME CALCULATION :
R ft lRftl C oTO WATEIR cowi~SIONJ WELLWELL WELL T TO WATER CONVERSION WEL
DIAM DEPTH (ft)WAZ
)LUMN ft X
FAC TFDEm !~fP ~COLUMN (ft)OR VOL al
2-25.20 X
X
gallons X 3 .785
SCREEN INTERVA L
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
2 24 .0 Ift TYPE : EPTH TO WATER :i
STRONG :EPTH TO PRODUCT :---kjL)14t~00
DDUCTTHICKNESS : (ft)
Pump INTAKEI NONE : IDON'T SAMPLE IF THICKNESS >OR =TO 0 .1 FT !
AT START AT EN D
25 .0 ft 1~-j I
WATER FLOWRATE TEMP SPEC TURBIDITY PH ORP DISSOLVED
TIME LEVEL COND OXYGE N
(hh :mm :ss)(ft)(m in) (deg C) (us/cm)(ntu)(unit)(mv)(mgA)
9
----------
fS : SO',35 14 qs Cl C)6,-s o
(5,,57~51 -!(.,c(!;lo ;La, 2.0 -5 6'so 12 .-)-0, oe
3 (o r7 .00 Cl 1 --4 --2,- -"A -5,(cl .9 0 . q 3 6 . 5-1 0 .07
-toTA L v Qk-(Lcoavv~D X . 5-1
I
-I'V L &n tcoil ;7 ZT--l-/- 3 -,b
ELECTRONIC FILENAME -
COMMENTS :C, \ -
T L)U r-'r-F ~-rj
e ErA AA i~n 1 .4
NOTE :WATER LEVEL, PRODUCT LEVEL,AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
DUKE POWER COMPAN Y
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
ILOCATION :BURLINGTON,NC PROC NO : 3500 .1j
S MPLI T Ju,,,,[[PROJECT~NAME:BURLINGTON
P-
'SAP1,10fE WELLS)FIELDCREWJ LDC,R
SAMPLING DATE :r222 u0TM
MONITORING WELL NO .:71
c-
WATER LEVEL METER SfN:
PID READING L rd In PRODUCT LEVEL METER S/N ;
METHOD (Pump /Ball)PERISTALTIC PUMP TIME / INITIALS OF COLLECTED SAMPLE :
WELL VOLUME CALCULATION :
WELL WELL DEPTH TO WATER CONVER ION W EEL LVolL 'al
ISI '!DIAM DEPTH (ft)WATER ft COLUMN (ft)X FFACTOR L
I.,
2-16 .32 X 0 .163 1
X paq
gallons X 3 .785 liters
SCREENINTERVAL
FP IM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
1 14 .32 ft .TYPE :DEPTH TO WATER :
STRONG :DEPTH TO PRODUCT :.4 1 Pi %E (tt)
MINOR :PRODUCT THICKNESS : (ft)
PUMP INTAKE NONE: DON'T SAMPLE IF THICKNESS >OR =TO 0 .1 FT !
AT START AT EN D
A&.57- ft .1 ,
I t.3 2,rT I to .5~v t
WATEK FLOWRATE TEMP SPEC TURBIDITY PH ORP LV
TIME LEVEL COND OXYGEN
(hh :mm :ss)(ft)(ml in) (deg C) (us/cm)(ntu)(unit)(M,)(mgA)
N-P-vt;-~r 4,-o xxr,
r Z4~c-v\Y ~css N-1 3cvz~-~J-~Iclf-ly *a k - - 0:;, b - ~-Y\5
cNJ A c-~ A T L ft T mliq :ol I-iA-s 7 --1 71- -1( 1 o4 ,
1-3,23 ft
5 A-&x P Lz-')A T
LQ~ t-ol'.~kj 0 If
A'V -r- n-
bc -TTL -2-
ELECTRONIC FILENAME -qMWEL CA P
COMMENTS :
LEVEL, PRODUCT LEVEL .AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
L~---C
D j ~T,IZ A C ~ A M41 nt~4114 GlEr"c'
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLIN G
ILOCATION :I BURLINGTON, NC PROC NO:El~~
I PROJECT NAME : IBURLINGTON MGP (SAPROLITE WELLS)FIELDCREW :j LDC,RLW
ISAMPLING DATE:.24-~1 22-Jul-03 I
%-9 f.L4
MONITORING WELL NO .PMWG-D
WATER LEVEL METER SfN :N/A
PID READING >;L~PPM PRODUCT LEVEL METER S/N :
METHOD (Pump /Bail)IPERISTALTIC PUMP TIME / INITIAL'S OF COLLECTED SAMPLE :
WELL VOLUME CALCULATION :
ION~SIONWELL WELL FDEPTH TO WATER COIN~VERSI WEL L
DIAM DEPTH (ft)[_.WATER (ft)COLUMN (11)X FACTOR I VOL (gal)I
2-19 .07 1 10-5~X
F X
gallons X 3 .785 liters
SCREENINTERVA L
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
19 .07 16 .57 Ift TYPE : 1DEPTHTOWATER :I
STRONG :DEPTH TO PRODUCT :--- fjo :,,E (ft)
MINOR PRODUCT THICKNESS : (ft)
Pump INTAKE NONE: IDON7 SAMPLE IF THICKNESS>OR =TO 0 .1 FT !
AT START AT END
At-.ff- it.%%-n
WATER FLOWRATE TEMP SPEC TURBIDITY PH ORP DISSOLVED
TIME LEVEL COND OXYGEN
(hh :mm :ss)(ft)(ml/min) (deg C) (USICM)(ntu) (unit)(mv)(mgA )
b -7 % , -)-y 4 h , A1q3~1 0
l9c
C,7-cr.;k3 ci o S~o xo-io 503 5-0 kl)3-2-a1c,013
kr-36,39 9,u ~G cl 1 11 X -~ Ay>kx~ 1 6, 3' ~A a 6, Ig,
It"gI, !sLA -k ~oa-i L r-, ~cA ~A 53L 0 11~ 9 I-L ((. 0 ~I L)
9 .03 L C,(4-Gy -5*-39, y ~,3-3 3c,;L k 3 0, r,9
i 1 ',5 4'.~L 5-cl ~OA IL 5-1 ot, >7 5~3 k t-13 -3 L Lk k c A
yo "L k-YvXC V C
Aiv,,~I~ 5 S-S-ks N1
ELECTRONIC FILENAME -
COMMENTS : 6 b -r-* r,-L-; %c-~Aq
P OF WELL CASING .
DUKE POWER COMPAN Y
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
ILOCATION : BURLINGTON, NC PROC NO :3500 1
1PROJECT NAME : BURLINGTON MGP (SAPROLITE WELLS)FIELDCREWd LDC,RLW
ISAMPLING DATE:21 -J,1-03
MONITORING WELL NO .PMWI
WATER LEVEL METER SIN : N/A
PID READING %r4k-*Tx-'ppm PRODUCT LEVEL METER S/N :kooi~~- I
METHOD (Pump I Ball)IPERISTALTIC PUMP I TIME / INITIALS OF COLLECTED SAMPLE:Lj_L,7-t
WELL VOLUME CALCULATION :
CONVERSIONWELLWELL F DEPTH TO r WATER CONVERSION WELLR
DIAM DEPTH (ft)WATER Lf~COLUMN (tt)X FACTO R
2-16 .12 x 0.1631
X r7
M .-)R gallons X 3 .785 lit.rs
SCREENINTERVA L
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
1 14 .12 ft.TYPE : IDEPTHTOWATER:i
STRO~G~ IDEPTH TO PRODUCT :--- ~jo"c (ft)
MINOR~I PRODUCT THICKNESS : (ft)
PUMP INTAKE NONF-V IDON'T SAMPLE IF THICKNESS >OR =TO 0 .1 Fr !
AT START ATEND
15 .5 ft
WATER FLOWRATE TEMP SPEC TURBIDITY PH ORP DISSOLVED
TIME LEVEL COND OXYGEN
(hh :mm :ss)(ft)(mllmin) (deg C) (us/cm)(ntu) (unit)(mv)(mqA)
12L .-Ill-lio XTA ~M~Z~e-li P -,-4 mw vj
?0c>0 "-Q
b%tCm,A%kc6 A,.t %tN 164PA"%,-%Ak ~,k
&,t~ke~,l ~,%A',~e)Aj %F 4 Od ",~,j J~uQ~J
%~t- LIS,Atlh b NZ41 zvA-,qT L 0 x 1,,~l cc-c~ 0 "or &Vf-I
It :'i %A 51A .,5'1 & 0 Z Lf . 2.1.tj 6 1 . &3A-5 (v -CU t72,A-09
I ~i,50 :264 ~5 L 2 1 - 5-1-yu Ir-5 3-53 c .9 V III 1~79
Lt',sL ,4 0 ;iy G X ZY . IA-3 3A 6 . A 10 V,-'.I ~l
6'. 0%,.S-5
(. SY
5-8 (1 Li .C 4-L5 .12 10 3
J&,15-6-z!) - Xt ql 4 -'1 S-11 ot a,I too
I
0 t-L"4 0-0
ELECTRONIC FILENAME-
COMMENTS :
-T-A c- 11
NOTE :WATER LEVEL,PRODUCT LEVEL,AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
DUKE POWER COMPAN Y
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
PROC NO : 3500.1
PROJECT NAME : BURLINGTON MGP (SAPROLITE WELLS)FIELD CREW :LDC,RLW
ISAMPLING DATE:,Rj d .1-ea Pe dul 2t:h=!!±tt=I 24-J,1-0 3
MONITORING WELL NO .PMWL-D
WATER LEVEL METER SIN :N/A
PID READING m PRODUCT LEVEL METER S/N :
METHOD (Pump/ Ball)PUMP TIME / INITIALS OF COLLECTED SAMPLE :
WELL VOLUME CALCULATION : SAN'N'j.
WATER CONVER IONCoWELL WELL DEPTH TO
ISI
F-WELL
DIAM DEPTH (ft)
ILUMN ft X
FACTOR VOL (gal)
2-o X 0 .163 1
X
qallons 3 .785X liters
SCREENINTERVAL
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENTft.
TYPE : EPTH TO WATER :I
STRONG : I DEPTH TO PRODUCT~?J 0 ~~tF (ft
MINOR : ]PRODUCT THICKNESS : (ft)Pump INTAKE NONE : IDON'T SAMPLE IF THICKNESS >OR TO 0 .1 FT !
AT START ATEN
(L k:--VVkQ ~,j CLL- U L- c.).9A k
%,nc Af-b oLr-v%,j slks~~lc w c c %~CftC-4Lt blvv~,)o1wiWATER FLOWHATE TEMP SPEC TURBIDITY pH ORP DIS OLVEDTIME LEVEL COND OXYGEN(hh nnss)(ft)(milmin)(dea C) (uS/cm)(nlu) (unit)(mv) (mg/1)
T~r~,45-L !a 1~ 1,%4-7 1
SS G (,"I-l (Lk Y --3 . C( -8 -
09 00 (4 Tt f-7 3%Lit 1 :1
%19 Qs -?- k '7,Z. 1 1 7- ri 44-1-s
69 1-3 ;,rk-3 4 9 0
09 15 1?-
r39 Z;lzi -I li 33 94 ki 5
09 11-5 712S 911 S7,t k --a
t9 Zo -7kal
'+--73'7 tf'z~
'I ~t I x k -11 "1 1 AL L(-a 1 4-1cl k 0 .
09's-12,441 \4 2-q 0 220A !xf,5 .2.cf .,c;4-ki a(.k o".1-1
I
ELECTRONIC FILENAME -PMW~b .(A F
COMMENTS:s IDIE tZbocc-cs-vir FX3~"Z
G -4
NOTE :WATER LEVEL, PRODUCT LEVEL,AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
-IL--- -1
~,cvv\
DUKE POWER COMPAN Y
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
,.JILOCATION : [BURLINGTON, NC PROC NO :3500 .1
PROJECT NAME : BURLINGTON MGP (OVERBURDEN WELLS)FIELDCREW :LDC,RLW
ISAMPLING DATE:_ZLJdq~~~ 24-Jul-0 3
MONITORING WELL NO . P-lS 77:7~~I
WATER LEVEL METER SM:N/A
PID READING Lr-xn~-1~m PRODUCT LEVEL METER S
METHOD (Pump/ Ball)IPERISTALTIC Pump TIME / INITIALS OF COLLECTED SAMPLE :13-5-Q
WELL VOLUME CALCULATION :
ER IONWELL WELL --DEPTH TO WAT CONVERSI F-WELL
DIAM DEPTH (ft)WATER ft COLUMN ft X FACTOR VOL (gal)_]I
2-11 .71 X 0 .1631
X
gallons X 3 .785 -liters
SCREENINTERVA L
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
11 .71 1 .71 ft.TYPE :DEPTH TO WATER :
STRONG :DEPTH TO PRODUCT :--- NAF (tt)
MINOR
.
PRODUCT THICKNESS :(ft)
Pump INTAKE NONE : DONT SAMPLE IF THICKNESS >OR =TO 0 .1 FT !
AT START A l
11 .21 ft.t %Xk ft .
WATER FLOWRATE TEMP SPEC TURBIDITY pH ORP DISSOLVED
TIME LEVEL COND OXYGEN
(hh :mm :ss) (mllmin) (deg C) (USICM)(ntu) (unit)~Mv (mqA)
15'3-5^*-06 r--'V)tw-L-o 3-)-Oo li,k AD AJ
----------------------- - - - ------
a 0 ;L6, co I .,I q .4-3 tj o .or)
4 9kj .~;- I k~-75 (a . OC
15'LIL' 3R 10%l a6 .4 .z Q%I,~.2Z5,0, Q-s
TOTAL-VOL,X<v%xQ-N-tj 5-06
SAM P c-%~4 1,
ELECTRONIC FILENAME - ks -CA P
Z~OMMENTS :c A IN C-
0 -Tj7u-fA A L-Jt LA-ic,T-
~NOTE :WATER LEVEL, PRODUCT LEVEL .AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
DUKE POWER COMPAN Y
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
LOCATION :PROC NO : 1 3500
1PROJECT NAME : BURLINGTON MGP (OVERBURDEN WELLS)FIELD CREW :L LDG, Ew~
SAMPLING DATE :
MONITORING WELL NO .MW-3
WATER LEVEL METER S/N :
PID READING PPM PRODUCT LEVEL METER S/N :
METHOD (Pump/ Bail)1PERISTALTIC PUMP TIME / INITIALS OF COLLECTED SAMPLE :h0w
WELL VOLUME CALCULATION :
WELL WELL EPTH TO WATER CONVERS1 WELLCo)LUMN tt Vo l
DIAM DEPTH (11)WATER (ft) COLUMN (ft)
X L Jai
2-22 .24 X
X
N/A gallons X 3.785 NIA
SCREENINTERVA L
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
ft 1-Zo ft . TYPE : !DEPTH TO WATER:ISTRONG:DEPTH TO PRODUCT:_ Tj 0 .4,L--(ft)
MINOR~ PRODUCT THICKNESS :
F----PUMP INT!j~ NONE : IDON7 SAMPLE IFTHICKNESS >OR=TOO .l FTI
AT START ATEND .1
1*7 .0 ft
WATER FLOWRATE TEMP SPEC I TURBIDITY pH ORP DISSOL ETIME LEVEL COND OXYGEN
(hh :mm :ss)_ (tt) (mi/min) (deg C) (US/cm)(ntu) (unit)(mv)(matl )
5 4 -5' UD) X710 101,oc,124-3 3-1 .0 S,q t((4 0~;k5
n-V 5q ; I< 11 . 9-'20 1 ct ils',8 3 0 -;L-5, 4-Lf (4 0 .2.57
Tat-ILQV~-
ELECTRONIC FILENAME -
COMMENTS :(.L,I-NA&14 L.I
f-ore P .T5 MIA T U I-L -T
~OTE :WATER LEVEL,PRODUCT LEVEL,AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
11
DUKE POWER COMPAN Y
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
ILOCATION : BURLINGTON, NC PROC NO : I 3SO0.1
I PROJECT NAME :BU RLINGTON
GP
VERBURDEN WELLS1 FIELDCREW :j LDC,RL
ISAMPLING DATE:--1~r 2,
MONITORING WELL NO.MW-,5
WATER LEVEL METER SIN :N/A
PID READING PRODUCT LEVEL METER S/N :
METHOD (Pump /Ball)JPERISTALTIC :~PUMP M TIME/INITIALS OF COLLECTED SAMPLE :
WELL VOLUME CALCULATION:
WELL WELL DEPTH TO WATER CONVERSI WELL
DIAM DEPTH (ft)WATER (ft)COLUMN ft X VOL(gal)
2-13 .54 5-5 L X
X
gallons X 3.785 liters
SCREENINTERVAL
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
1 3 .54 It .TYPE : EPTH TO WATER :
STRONG :EPTH TO PRODUCT:---(ft;
ODUCTTHICKNESS :
_NPUMPINTAKDE NONE: IDON7 SAMPLE IF THICKNESS >OR =TO 0 .1 FT 1
AT START Al
10.5 ft. 1 (
WATER FLOWRATE TEMP SPEC TURBIDITY pH ORP DISSOLVEDTIME LEVEL COND OXYGEN(hh :mm:ss)(ft)(mVmin) (deg C) (us/cm)(ntu) (unit)(mv)(mgA )
U -Xc~'70 -SM8 eoz-LZ-7-4 D N,"~0~rj IN Jo t-~4 'i -w-b
4 rj jfS L
9,.,tct,.53 j,,,1-cr -7 ~f 9X-4-)Qj ga .5'5-4-7 03 9 ~7 1114
cl',54',33 (,. -7- 1 5 (1 2 :L-5L I gqo .g q,54 7-01 1 cl -? OA9
9"5cl,
-
1~1 4-Al -/, q Al -,>a q 9,z .c V, 9 (e 0-(R
ko-~ds-.04 6 2-1 5'9 AX~82,993 .8 2~),q 4 q_y-0,,f4
5-(.,2 ;L -91 o 1139 3,oC 7 .o 1 -33
1b 1 .
<Aj,~-P-I~svn c)% ~bc -7 t=X/2~
ELECTRONIC FILENAME -rv\ LJ C a
COMMENTS :r C-0 ?Ah /%,Awst- 'TAG,
JV8 \~0-,L-
ODUCT LEVEL,AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
DUKE POWER COMPAN Y
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
ILOCATION :IBURLINGTON, NC PROC NO :3500 .1
1PROJECT NAME : BURLINGTON MGP (OVERBURDEN WELLS)FIELDCREW : LDC,RLW
ISAMPLING DATE:;-4 -A r+-22,VG~~I 24-Jul-03
MONITORING WELL NO .MW-9 I
WATER LEVEL METER SIN : NIA
PID READING ppm PRODUCT LEVEL METER SIN :
METHOD (Pump /Ball)PUMP TIME / INITIALS OF COLLECTED SAMPLE :
WELL VOLUME CALCULATION :
WELL WELL DEPTH TO CONVERSIONF WATER CONVERSION WELLR
DIAM DEPTH (ft)WATER_ff~X I FACTOR I VOL(gal)
2-9 .50 X
X
gallons X 1 3 .785
SCREENINTERVAL
FROM id TO DETECTED ODORS FREE PRODUCT MEASUREMENT
tit TYPE~I IDEPTH TO WATER,
STRONG, I IDEPTH TO PRODUCT~---I (ft)
MINOR~I I PRODUCT THICKNESS : = I (ft)
Pump INTAKEI NONE : I IDON7 SAMPLE IFTHICKNESS >OR =TO 0.1 FT !
ft
. ft .
AT START AT EN D
WATER FLOWRATE TEMP SPEC TURBIDITY PH ORP DISSOL ED
TIME LEVEL COND OXYGEN
(hh :mm :~)(ft)(mi/min)(deg C) (US/cm)(ntu) (unit)(mv)(mqA)
ELECTRONIC FILENAME -
COMMENTS: 5~L ~,k~ 6 F c-r-A L-rj I xjc-
.Vf urt~-%- lCrJAcf-e-TstLLC (o"vQ>-iAt-mo-J L,,ZNw
NKS UCC3~01L-A
-
ml~- %.-kjerviz so~tbmq-CL-tA~,
hr"-%ws:-"t O.FJ-Lxt-
1,NOTE:WATER LEVEL, PRODUCT LEVEL,AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
DUKE POWER COMPAN Y
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
ILOCATION : IBURLINGTON, NC PROC NO : 1 3500.1
1PROJECT NAME : BURLINGTON MGP (OVERBURDEN WELLS)FIELDCREW :j LDC,RL
ISAMPLING DATE :24-J11-03
MONITORING WELL NO.PMWB-S
WATER LEVEL METER SIN :N/A
PID READING PPMI PRODUCT LEVEL METER SfN :
METHOD (Pump/ Ball)kPERlSTALTIC PUMP TIME / INITIALS OF COLLECTED SAMPLE :1 1136 L-br.-I
WELL VOLUME CALCULATION :
WATER0lLUMN IIIflWELL WELL --D~EPTH TT06 WAT CONVERSION
E IDIAM DEPTH (ft)WATER ft X FACTOR
2-13.58 r7 ,A x XX
gallons X 3 .785 liters
SCREENINTERVA L
FF30M TO DETECTED ODORS FREE PRODUCT MEASUREMENT
14 .0 4 .0 ft,TYPE : II;At.JA^IDEPTHTOWATER :
STRON&DEPTH TO PRODUCT:---I a cj,~-00
MINOR~ PRODUCT THICKNESS: = I (ft)
I PUMP INTAKE NONE : I IDON'T SAMPLE IF THICKNESS >OR =TO 0.1 FT
AT START A7 :ND
WATER FLOWRATE TEMP SPEC TURBIDITY PH ORP DISSOLVED
TIME LEVEL COND OXYGEN
(hh :mm :ss)(ft)(ml/min)(deg C) (us/cm)(ntu) (unit)(mv)(mgA )
3-%-~ovx~;b 1 . c~Pr T 3 sk-o ;~t-b F-L4 W AA Tv~
TO ~A
s-1- I a3,,(,i 6 -2 -21 C),
3o Lo,;L 4 .--) 4 3~X 4 ct C70 o q
(3'1 1 1.og 11, ~A ri -3%aS-,i4 -),Yo,3 -C --~4 6;-2 C9 , os*
3, 1-): 5-3 9 .1,0 A4-10 71A -D 3,A -7 e.4 0 .05
I 3--AS' 3~q , 12--7 U a 4, a. 2L,J1;19 231 7-2 4 4
T-0 7 \) a v--eo s 1 5-
5
v+-
- ()
-
?txi
ELECTRONIC FILENAME -~IMWB 5 C A P
COMMENTS:b .4 flAA
NOTE :WATER LEVEL, PRODUCT LEVEL,AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
DUKE POWER COMPAN Y
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
LOCATION :BURLINGTON, NC PROC NO :3500.1
PROJECT NAME : BURLINGTON MqP~OVEDBIRDEN WELLS)FIELDCREW :l LDC,RLW
SAMPLING DATE:-24-60H31
22_jul_03
5IR -1-1 AA
MONITORING WELL NO. PMWC-s
WATER LEVEL METER S/N : N/A
PID READING PJO-M L PRODUCT LEVEL METER SIN :
METHOD (Pump /Ball)1PERISTALTIC PUMP I TIME / INITIALS OF COLLECTED SAMPLE :\-f
WELL VOLUME CALCULATION :
Co~LUMN ftCoWELL WELL WATER CONVERSION WELL)LUMN OR Vol
0 1 1DIAM DEPTH (ft)X FACTOR
L lal
2-21 .09 X 0 .163 10
i X
gallons X 3 .785 ~fiters
SCREENINTERVA L
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
2 6.5 TYPE : EPTH TO WATER :
STRONG :EPTH TO PRODUCT:---gj')'4~E (ft)
ODUCTTHICKNESS : = (ft)
E KE~]NONE : IDON'T SAMPLE IF THICKNESS >OR =TO 0.1 FT!Pump INT8K
:AT START AT :NDN
17 .0 ft. 1'7 ~ 0
ft
WATER FLOWRATE TEMP SPEC TURBIDITY pH ORP DISSOLVEDTIME LEVEL COND OXYGEN(hh :mm :ss)(ft)(ml/min) (deg C) (uS/cm)(ntu) (unit)(mv)-(mgA)
:IL.-5 1 oo
b A
----------
-A-A ', 53 111-53 /S-q -X I -if I &1 (2- 1 ;L(-S 4 1A.10-1 0 .
IZ-59 /58 -11 . 6 L 1~2-5-~L I ict .9 (.~ v '~( ) 0 k r),0
13'.3q-,4~3 1 .2 -IY4 -Z 1 .ys clW 97 0, r-
3 9 : 5q 0~4 a I. C, 9L 1,33 29-:Z - q cl,o~;t -Lel ~r
13'.&tf '. 39 1.
a-70 154 2 1 1-3 y5A .I ~? -L'Cl 4, Le~~90-6 1
t3~51'~2-4 12'--) 1 kL ~i 3- X,),6 5440 6 q9 I a 0 . C)q
ll~,. 5-7 :54 4 (L t .2 :2-kj57 . g L .3 3' 6 . It I 8cf 0~05-
C4 4
IA4-,PLC-i t 5,Zp C L-
LC> %AA L~~%E3 S
I t4A_ t,~C-11-A-C t i,I) N-
ELECTRONIC FILENAME -CA P
COMMENTS : CA Pit TLIS I,,<fj
6-6 0 t,TVP!4r fA b
Ask
NOTE :WATER LEVEL, PRODUCT LEVEL,AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
DUKE POWER COMPAN Y
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
ILOCATION :BURLINGTON, NC PROC NO : 1 3500 .
1 PROJECT NAME, BURLINGTON MGP (OVERBURDEN WELLS) FIELDCREWd LDC,R
JSAMPLING DATE : 21-Jul-03 =40~~~-~-j -0 c-
MONITORING WELL NO.PMWM-S -71
WATER LEVEL METER S/N :N/A
PID READING tiorz I PPM PRODUCT LEVEL METER S/N :at Li's -1
METHOD (Pump /Ball)Pump TIME i INITIALS OF COLLECTED SAMPLE :
WELL VOLUME CALCULATION :
W Itj 0 [COXNVERSiI3~)LUMN tt VolCoWELL WELL D=TfO WATEIRI,,CONVERSION Wl ELLETHT~_ L al
DIAM DEPTH (Ift)
)LUMN X
FACTOR al
2'
X
57631
_ 36
X 0 .1
0 .4%gallons X 3 .785 1 .14 ~fiters
SCREENINTERVAL
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
%;k .!s ft .1 Ift TYPE, DEPTH TO WATER :
STRONG~DEPTH TO PRODIJCT~---0 1~00
MINOR, PRODUCT THICKNESS, =00
Pump INTAKEJ NONE : I V~IDON'T SAMPLE IF THICKNESS >OR =TO 0.1 FT !
AT START ATEND
jj,j
It
.
WATER FLOWRATE TFMP SPEC TURBIDITY pH I ORP DISSOLVED
TIME LEVEL COND OXYGEN
(hh :mm :ss) (ft)(ml/min)(deg C) (uslcm)(ntu) (unit)(mv)(mqA )
:5 -r "r-C7 ittl)&A w b 0 IllJ -puevtco (5 a b ej
wvL crity-1
16%201'j,%GL .vk%t "05 2 .301 -5 .40 5-A 2~1-1711
to .'71 2.60 1 kat-.L 5t I~LO-A I 1-;04 S-39 SA3 1 1-70
v% 2J ', k3 go 0 _t%4v) txo .-)0 -Va.5 .'t 0 3 2z 1 . c -?
~v.xcv.%-k to .1%;040 19 .L 17.0 .9 0 -L-) 5-41 _5';L 2-1 .1.2
.4~ A4vP LF 0 1/%r it 1 <, %,a c_ M Li 0,2
ELECTRONIC FILENAME -PVV\VJeV\5 .C-Arr
COMMENTS :IlLrj=gAmrE'Sn~~;6 Pif-tk I 0-Y CA ve-A ij a A-A
ey C-Dol!k LAv-%_4_VAh blo n~k&g_
If
NOTE :WATER LEVEL, PRODUCT LEVEL,AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING-
DUKE POWER COMPAN Y
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
ILOCATION :BURLIN TON, NC I PROC NO: 1 3500 .1
1PROJECT NAME : BURLINGTON MGP (OVERBURDEN WELLS FIELDCREWd LDC,RL
ISAMPLING DATE:24-Jul-03
MONITORING WELL NO .PMWL-S
WATER LEVEL METER SfN :
PID READING Sin PRODUCT LEVEL METER S/N :
METHOD (Pump I Bail)P, Pump TIME/INITIALS OF COLLECTED SAMPLE :
WELL VOLUME CALCULATION :
ft Co)LUMN ft VolWELL WELL
DEPT
RT~ WATER CONVERSION W1 ELl-L a l
DIAM DEPTH (11)WAZ COLUMN (it)X VOL al
2- r).4,>x
X
gallons X 3.785 lit,,s
SCREENINTERVA L
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
it .0 it.TYPE :DEPTH TO WATER :I
STRONG :DEPTH TO PRODUCT:---1 ovo"C (ft)
TINOR :ve-PRODUCT THICKNESS :.=I (it)
Pump INTAKEI NONE : DON'T SAMPLE IF THICKNESS >OR =TO 0 .1 Fr !
AT START I AT END
4-7~ 1-6
7-5:Lbc
WAILH FLOWRATE TEMP SPEC TURBIDITY pH ORP DISSOLVED
TIME LEVEL COND OXYGEN
(hh :mm :ss)(ft)(ml in)(deg C) (US/CM)(ntu) (und)(my)(m-qA)
,t,ztm -10 s-,,A%x%.-Zzc -S-m .- 1AAb is'T so;ct4.
Mg L cX-6,41^Wlik tA-f 0 N NW244 C. 0 -Jm f~,fz,~f-ot-T --I x
4ft-z--Ior~
n-A--s E Xv 0 Z4%-r!S:S:.kz %-A Alr Olt,
o-)3 ~>- -
(-tt &VGI 64 41A c 140 k em
kf6)- Mj-lea ;ej OAk S .-NViE 0AA-Dt"fJ
To (. 't &0-:5 ~~C,5'P*Q-
0 4 .5o 1 22 vo- .7- 10-3 4 .-3er 12-~2 0-2-1
j3 ~) *.!I t~:'-V ly . -5 :~s 50 3 .tq I 1,!A ~67 b-120 0,2.%j
0-?4 1,v,L ;t,;24 .%-7 q115 4,?(.k34 0 ~-X -A,
3 13( 0,13o-7 : 5-7 : It e 6 IS .3
091 .OLC,01C,E41 .0 2x-I Y, 5~41 -Z
091.all 04 -Y, -) -7 41 'Im')5 33 1144 0-1
Ost . 7-0 t,>-3 Lf,v,.t 104 .11J~3
tt~5
6-32-1'(2 0 .11'y (.A
,5 .CAPELECTRONIC FILENAME -
COMMENTS : C, I - 'T
c,ef1b P ;;;T
411NOTE : ATER LEVEL, PRODUCT LEVEL,AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
MQJ L
-k C-0 -t
to rr .3 2,04
'ct ;L 4,IS— 5 cl 3 4-3 1
-SAN?LO a c b-I It, 3
3 -5-
jo-, vo P-t~CNMV ~--b
DUKE POWER COMPAN Y
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
ILOCATION :IBURLINGTON . NC PROC NO : 1 3500.1
1PROJECT NAME: IBURLINGTON MGP (SHAL FRACT BR WELLS) FIELDCREW :j LDC,RL
gob,ISAMPLING DATE:I
MONITORING WELL NO .DMW-1 71 r7 I t o 3
WATER LEVEL METER SIN : N/A
PID READING NO TV-,ppm PRODUCT LEVEL METER SIN :
METHOD (Pump/ Bail)IPERISTALTIC PUMP I TIME / INITIALS OF COLLECTED SAMPLE :
WELL VOLUME CALCULATION:
CZ14 ~RSIONWELL WELL f-6i~TH T07 TE RCOILUMN ftCODEPWA CONVERSION
DIAM DEPTH (ft)WATER (ft)
ILUMN (ft X
FACTORFACTORI
2-29 .02 5 X
X
N/A g,lio,s X 3.785 N/A ~Ijters
SCREENINTERVA L
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
29 nP ft . 16 .72 ft .TYPE~ DEPTH TO WATER :
STRONG :DEPTH TO PRODUCT:--- %E (ft)
MINOR : PRODUCT THICKNESS :(ft)
PUMP INTAKE NONE : 7~-DON`T SAMPLE IF THICKNESS >OR =TO 0 .1 FT !
AT START AT END
24 .0 ft XLJ,0 ft .
WATER FLOWRATE TEMP SPEC TURBIDITY pH ORP DISSOLVED
TIME LEVEL COND OXYGEN
(hh :mm :ss)(ft)(mVmin) (deg C) (US/cm)(ntu) (unit)(mv) (mco)
q ISO (L fV10,10) 4.0 gal A,,o A --cAd ~-o
.2-cl 1.Ll a 5-ilq ~Asc)k9,4 rl ks0-4 3-01 e .OQ 3 ;2- '1-0,n
3(o',119 s%J4 LAgo kg .44 ( 0'j . a -2 .1 4. 51~t 9 1 ~1-0 0 .0k
M, 4 Ali ~,Aq I Lt scu kA,4 4 1 tw..9 X -Lx S .9s,1 32 o 0,0(.1
To-%yv%.-~,cyvko '%* !~-;91~k
Av~? t-iz 0 -7 /2-51113 %Z 4-011- q'l'
ELECTRONIC FILENAME - C,A
COMMENTS :Ck --f-In 1Z.ff%A VW (-W,-eJ
C'~O~W -111661'4 lsj ;:~Ll-.1 2 Ah,
D T, X-7 a
DUKE POWER COMPAN Y
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
ILOCATION :BURLINGTON, NC PROC NO :3500 .1
1PROJECT~NAME: BURLINGTON MGP (SHAL FRACT EIR WELLS) FIELDCREW :j LDC,RLW
T 24-Jul-03FISAMPLINGDAE
MONITORING WELL NO.DMW-2
WATER LEVEL METER SIN : N/A
PID READING Noic I ppm!PRODUCT LEVEL METER SIN :~(5 -I,
METHOD (Pump/ Ball)SUB Pump TIME / INITIALS OF COLLECTED SAMPLE :e
WELL VOLUME CALCULATION :
)LU VolCoCo)LUMN ftWELL WELL F DEPTH TO WATER CONVERSION WELL
DIAM DEPTH (141)WATER (ft)MN ft X FAC~OR L a
2-32.08 X 0.163 1
X
gallons X 3 .785 liters
I SCREENINTERVA L
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
32 nn ft 22 .08 ft.TYPE :DEPTH TO WATER :i
STRONG :DEPTH TO PRODUCT :---MONC (ft)
MINOR: PRODUCT THICKNESS : (ft)
Pump INTAKE NONE : -C~rz DON'T SAMPLE IF THICKNESS >OR =TO 0.1 FT !
AT START AT END
27.0 ft .ZID It
WATER FLOWRATE TEMP SPEC TURBIDITY PH ORP DISSOLVED-
TIME LEVEL COND OXYGEN
(hh :mm :ss) (ft)(mllmin)(dog C) (Us/cm)(ntu) (unit)(mv)(mgA)
sn4k I
k Al 0 .0 1
lyc%-'i 1 .12 6, 3-?ts Li
cs . I I ;L I I C . IS3
(2-t ."va 5 .
JL ;c)L~)<-
ELECTRONIC FILENAME -;L C
COMMENTS:
I LEVEL.PRODUCT LEVEL,AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
DUKE POWER COMPAN Y
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
1LOCATION :BURLINGTON, NC PROC NO : 1 3500 .1
1PROJECT NAME : BURLINGTON BR WELLS)FIELDCREWd LDC,RLW2_~,2t_jVr.63 r2P (SHAL FIACT
n3ISAMPLING DATE:
U1 .03
o g
~L'~-D c-
MONITORING WELL NO.[~C-BR
WATER LEVEL METER SIN :N/A
PID READING I pk-vvt I ppml PRODUCT LEVEL METER S/N:
METHOD (Pump/ Ball)I URSSUB Pump TIME / INITIALS OF COLLECTED SAMPLE :
WELL VOLUME CALCULATION :
- I SlOdCo)LUMN tt VOLWELL WELL DEPTH TO WATER CONVERSION WELL
0 1 1DIAM DEPTH (ft)WATER (ft) COLUMN (tt)X 7FACTORI
2 36 .00 63X0.1631 4 . Q
X
gallons X 3 .785 lite's
SCREENINTERVA L
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
3 27 .0 Ift TYPE : C4*A\.j*,p-DEPTH TO WATER:i
STRONG~iDEPTH TO PRODUCT :...
PRODUCT THICKNESS : = I (ft)
Pump INTAKE NONE : I JDON-r SAMPLE IF THICKNESS>OR =TO 0 .1 FT !
AT START ATEN D
34 .5 ft 34
6 ft.
WATER FLOWRATE TEMP SPEC TURBIDITY pH ORP DISSOLVED
TIME LEVEL COND OXYGEN
(hh :mm:ss)(ft) (m min) (deg C) (US/CM)(ntu) (unit)(Mv)(mqA)
L 12)6-0,
k L 3 6 (S,30 950 (9~~x li ~ In LA - b-s Li 6 1-2-(
",q 0 ig,3-2 2 .7,0 1 (cl 0 q~;,?, 5-L'-) 4 -)
Is,Lilg ed,2-o (&,I I qdd-L-k 1 3-0 .
0 \-o -7
-1~ A-I AZ
ELECTRONIC FILENAME fm~,jc-BrZ-C-Af
COMMENTS :e-1 0
G-00 43 TYA-G -4 we"Il It "
NOTE :WATER LEVEL, PRODUCT LEVEL,AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
DUKE POWER COMPAN Y
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
LOCATION : IBURLINGTON, NC I PROC NO: 3500 .
PROJECT NAME, BURLINGTON MGP (SHAL FRACT Brt WELLS)FIELD CREW :LDC,R
ISAMPLING DATE : -9UAd-.(l3 . I 22-Jul-03 I 23-Zl.-03 ~24-001-03'1
MONITORING WELL NO .PMWH-BR
WATER LEVEL METER SIN:N/A
PID READING 2-0 wo PPM PRODUCT LEVEL METER S/N :kot'is-k
METHOD (Pump /Ball)1PERISTALTIC PUMP TIME / INITIALS OF COLLECTED SAMPLE :o-,-so 2,(-
WELL VOLUME CALCULATION:
CONVERSION IELLC 0~LUMN ft V L lalWATERWELL WELL FDEPTH TO CONVERSION0WATER[Eo-~DIAM DEPTH (ft)WATER (ft)
~LUMN ft X
FACTOR
2-20.72 vof x 0 .1631
X
gallons X 3 .78S liters
SCREENINTERVA L
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
20.72
It.
19 .72 ft
.
TYPE : EPTH TO WATER :
STRONG :EPTH TO PRODUCT :---(ft)
MINOR~ PRODUCT THICKNESS : (ft)
Pump INTAKE NONE : DONT SAMPLE IF THICRNESS OR =TO 0 .1 FT 1
AT START AT END
20 .0 ft.aO .0 ft.
WATER FLOWRATE TEMP SPEC TURBIDITY pH ORP DISSOLVED
TIME LEVEL COND OXYGEN
(hh :mm :ss)(ft)(mVmin)(deg C) (US/cm)(ntu) (unit)(mv)(mgA)
s .L4L 2.51-t 5 -% A 5,% %.,r t ir-
T (A cri E%~A#-4 1-~cb rev 4-%C
2 .41 a5li 1 11 .1 0 -43 6,5"4 o,-I A 1 0 - ol
cl 2.5 . A.0 ff-41 -'L 17 .%2~4(,g .I o .,Xck 4-sy to 9 6 .05
q,. 2-ALi L 17 .9-3 q~ 3 .0 .03
0900 ~,XQ-
ELECTRONIC FILENAME -trnw\iga . c-A P
COMMENTS : E:l %~L",- -,t-~roG,
qNOTE~ WATER LEVEL, PRODUCT LEVEL .AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
DUKE POWER COMPAN Y
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
JLOCATION :I BURLINGTON,NC PROC NO:
1PROJECT NAME : IBURLINGTON MGP (SHAL FRACT BR WELLS)FIELD CREW :
ISAMPLING DATE :.21-Jul-0 3
MONITORING WELL No .PMWI-13R
WATER LEVEL METER SIN:N/A
PID READING ppm PRODUCT LEVEL METER SIN:
METHOD (Pump /Ball)Pump TIME/INITIALS OF COLLECTED SAMPLE:
WELL VOLUME CALCULATION :
WATER CONVERSIONlLUMN ftWELL WELL DEPTH TO Co WELL
DIAM DEPTH (ft)WATER (ft) COLUMN ft X FACTO R
X 0.16312-38 .07 1 .58 -1 .
gallons X 3 .785 I~Iters
SCREEN INTERVAL
DETECTE ODORS FREE PRODUCT MEASUREMENT
TYPE :IDEPTH TO WATER :i
STRONG :DEPTH TO PRODUCT:---fjodL,(ft)
MINOR :PRODUCT THICKNESS :
Pump INTAKE NONE:V IDON'T SAMPLE IF THICKNESS >OR =TO 0 .1 FT 1
AT START I AT EN D
33 .0 ILI 33 .0 It
WATER FLOWRATE TEMP SPEC TURBIDITY P ORP DISSOLVED
TIME LEVEL COND OXYGEN
(hh :mm :ss)(ft)(mllmln) (deg C)(uS/=) (ntu) (unit)(mv)(MgA)
ts ..3oi 3 41tt-r-zl )PL
Tt^
3 :1 4Aq 1 9 -5'~ S'9 o .3 1 .51 4 - ? Lf I
is"uttr. A-4 1,0 .2,R 33o 11-49 'S ZM -I O,ct-)C -7 Li (.2-ok
1(6, -~53* -A. k to . 34 33lk,121-1 %1 S&S-9 (D -ci 3 4-?4 Iz 1?0 .0
-roT /w- I, ~Ac--c'b 1 4
SAC-A "70 1 63 17 :Lco
ELECTRONIC FILENAME -C41 LP 14
COMMENTS :7 rA c-4 PAD
TU 6 C-jc~
WNOTE : WATER LEVEL, PRODUCT LEVEL,AN6%L D-E-PJTLH4AE REFERENCED TO THE TOP OF WELL CASING .
DUKE POWER COMPAN Y
F GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
ILOCATION ;I BURLINGTON, NC PROC NO: 1 3500 .
1PROJECT NAME : 113URLINGTON MGP ISHAL FRACT BR WELLS) FIELDCREW :j LDC,R
SAMPLING DATE : I --"~~.~ I 24-Jul-0 3
MONITORING WELL NO.PMWL-BR IAK
WATER LEVEL METER S/N :
PID READING PRODUCT LEVEL METER SIN :
METHOD (Pump /Ball)PU TIME / INITIALS OF COLLECTED SAMPLE :
WELL VOLUME CALCULATION :
)LUMN ft0'n)LUMMN%WELL WELL TO WATER CONVERSION WELL
DEPT" ftl Co IDIAMDEPTH(ft)WATE
1] X
FACTOR VOL (gal)
2-X
I-L"X
gallons X 3 .785 ~lltels
SCREENINTERVA L
FROM TO DETECTE ODORS FREE PRODUCT MEASUREMENT
;14-0 ft .1 4 .o Ift TYPE :2EPTH TO WATER :
STRONG :!DEPTH TO PRODUCT::,13 vi ko~00MINORODUCTTHICKNESS: (ft)Pump INTAKEI NONE : IDONT SAMPLE IF THICKNESS>OR =TO 0 .1 FT !
AT START AT END
),0 - 0 ft . 10 .0 ft
.
-WATER FLOWRATE TEMP SPEC TURBIDITY pH ORP DISSOLVED
TIME LEVEL COND OXYGEN
(hh :mm :ss)(ft)(mllmln) (deg C) (US/cm)(ntu) (unit)(mv)(Mqn )
0 32 4 380 9-2 .2-5,SAX -1 -4-e5 1'.,
32 ri,ri 1 3 8Q tl~~4o xct 7 .1 .130 0,04
Li'?-? ~ 9 Li -39o 11 1 3 o 30%. -)0 -1 4 S I I ;L 2-9 0 ~ 05 , I
0 :-is LtoD 101--IL 3o%.%i o .1 1 axg, 0,04
-4
:5 At~Ltr 1 : ~~,q ?-4 f 4 -3
ELECTRONIC FILENAME -CA P
COMMENTS : -r-
c-,'oo ?v%z -1-4 c-
INOTE~WATER LEVEL, PRODUCT LEVEL,AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
DUKE POWER COMPAN Y
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
L2C~I,TION:IBURLINGTON, N C~R;j J_C PROC NO :3500 .1'T
NAME :BURLINGTON MGP (SHAL FRACT BR WELLS)FIELD CREW :
SAMPLING DATE:21-Jul_03 0A Pa J11 98 1 -24-3 LD C-
MONITORING WELL NO.PMWM-13R
WATER LEVEL METER SIN :NIA
PID READING x-nnm PRODUCT LEVEL METER SIN :om5 -~
METHOD (Pump /Ball)Pump TIME / INITIALS OF COLLECTED SAMPLE :cs~ ,L%-
WELL VOLUME CALCULATION :
WATERWELL WELL DEPTH TO CONVERSION F WELLCo
DIAM DEPTH ft WATER (ft)
)LUMN ft X
FACTOR VOL (gal)
2- X 0.163 1
X
gallons X 3 .785
SCREENINTERVA L
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
lot %(,.0 Ift TYPE : IDEPTHTOWATER:ISTRONG:EPTH TO PRODUCT*---1 00
MINOR: tPRODUCT THICKNESS : = I (ft)
Pump INTAKE NONE V~JDON7 SAMPLE IFTHICKNESS >OR =TOO .l FT !
AT START,.AT iND -
It.
WATER FLOWRATE TEMP SPEC TURBIDITY PH ORP DISSOLVE DTIME LEVEL COND OXYGEN(hh :mm :ss)(ft)(ml/min) (deg C) (us/cm)(ntu)(mv (mqA)
%-41CEL"V'40 .4 iY:AP-j 4SIC4-v~-ll~- Nm~o I "M
7.1. %to 1.xit L0 1 .')l 5.72.-z-2 :?
11-5111, 1-50 1 ;L-Ok38 Q ;L, It 1,21 ~'211 1 0 .
11 .4,o 11 o 2-0-3 OL-2.31 .3 1 .05 5-11 .7- v 0-op
51 1 L -0 ,ko .3.5-tlbbw 2. os t . 3 .,;.41 o _,III 0 . oc
ELECTRONIC FILENAME -PAWfn6(2-
,ZTS :COMM 5 A"b Q P we I-%.- CASZc~*-V-CA ~JA Iv IF ko%,%C~zv NZ
r
C, I (is 4~,oo h If PAO r4O A G
NOTE:WATER LEVEL, PRODUCT LEVEL .AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
CHAIN OF CUSTODY RECOVAND ANALYSIS REQUEST FORM 0
Analytical Laboratory Services iDuke--------- ---------"Page -L oiMail Code MG03A2 (Building 7405)DISTRIBUTION13339Hagers Ferry R dPowEnergy.FX~-,ORIGINAL lo LAB ,
For Detailed Instructions, see : Huntersville,N. C . 28078 1,1rPf!OGRAM,-: COPY to CLIENT(704) 875~5245 bb,Wiite~http ://devwv1essenv1coc1 Fax :7;L4j .§Lkjq.................L jk ............
I)Project Name 2)Phone No: a7b~5257
SURUNGTON MGP (OVERBURDEN WELLS)FU
E 3)CIISAI C .Campbell/ R . Roberts 4)Fax No ;875 .5032 5p sem.:I=C
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i Desktop N pie Description or ID Date Time 19 z 2 111 w U 1
C23 0 1 TRIP BLANK 3 n/a 3*11,11-3 a43~PA&W X
W ?X 1 1 3 1 6M-3 03
6.2 PMWB-S 0 (330 X I 1 3
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'Add .Cost Will Apply
CHAIN OF CUSTODY RECOR4,kND ANALYSIS REQUEST FOR M5M --------
ices I 01FRDukeMail Code MG03A2 (Building 7405) L sampla Cie "Page Of
DISTRIBUTION0 lql~a l,,~4j!~~Ip tPoftEnergy,13339 Hagers Ferry Rd
7~
V Moil Frow ORIGINAL to LAB,Date&itFor Detailed instructions, see : Huntersville,N. C . 28078 ll.opjgay~~[phone] &~VSAMPLE PROGRAJM~ COPY to CLIENT~4,,~~Glcund Water ,httlil/de~Iessenv/coct F a-M.: 7M -~q.Q:L DIMAS;-------------.12 5 8 -------------74 ~l, ~,w
I)Project Name 2)Phone No :875-5257 We r..t-'~Drlnldlng Water I
BURLINGTON MGP (OVERBURDEN WELLS)4,
-C olerTe 6(RCRkWaste-~-.f,NO
3)CIlent C .Campbell/ R . Roberts 4)Fax ND :875-5032 Pr a C
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I "Lob ID i Desktop No . "Sample Description or ID L)0Signature C.D,teTT,m,z
023 0 i TRIP BLANK ie,%-.Iq~x 3 We 3
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E PMWL-S x 1 1 3 1 6
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2
QC SAMPLE (WELL P-1 S)x n/a 1
Customer to sign &date below
21)RellNd DetafTtra A ea .8Z--3-o 2)PZ
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nlAnalytical Laboratory Services ;I=.Duke ------------- - ----------'[LIM "Page otMail Code MG03A2 (Building 7405)R!DISTRIBUTION13339Hagers Ferry Rd ZgIMH~WIRg~b~,PtkrEnergy..I I ORIGINAL to LAS,Huntersiville,N . C. 28078 I LFor Detailed Instmcrions, we : [phone] COPY to CLIENT
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I)Project Name 2)Phone No :075-5257
BURLINGTON MGP (OVERBURDEN WELLS)
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PMWC-S x 1 1 3 1 6
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0 MIN-9 x I 1 3 1
PMWM-S x 1 1 3 1 6
PMWL-S x 1 1 3 1 6E0UIFIELDBLANKx 1 1 3 1 n/a 6a
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Customer to sign &date below
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August 13, 2003 5 :29:19 PM Page #1 of 1
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Duke Trace Metals
OvkEnergy.Case Narrativ e
(This dommeat must accompany release of Analytiml Data)
---- - ------- -------- -
03-JUL-0337
LIMS Job #03-JUL-0338
03-JUL-0339dW
Worklist #03-JUL-071 9
0 iron was analyzed in the method blank by ICP above the reporting limit . The
concentration of Fe was 0 .054 mg/L compared to the reporting limit of 0 .010
mg/L .
• All other QC associated with this data set is acceptable .
•The concentration of iron in Sample #23024518 is between 5 and 10 times
that contained in the blank . Therefore, this result should be considered an
upper limit of the true concentration and should be used with caution .
•For sample 23024535,the concentration of iron in the sample is at a level
below 5 times that contained in the blank . This result must be considered to
be suspect .
• All other samples contain iron in concentrations greater than 10 times that
contained in the blank . Therefore, those results are acceptable .
•The data may be reported to the client with the above qualifications .
Itl~ ----------
-%iaj rr, Scientist
-------------------------------------------------------------------------------------Duke Energy Analytical Laboratory Service s
Environment, Health &Safety Services Environmental Center - MG03A2
Phone:[phone] Hagers Ferry Road
FAX [phone] Humersville NC 28078-7929
Duke Duke Energy Analytical Laborator y
Phone .[phone] Fax :[phone]PoEnergy.13339 Hagers Ferry Road Huntersville,NC28078-7929
McGuire Nudear Complex - MG03A 2
C4ertiflcata 4of Aknalynis
New York State Department of Health Certification # 11717Oldahoma Department of Environmental Quality Certification # 9930
Kansas Department of Health and Environment Certificate # E-1031 1
North Carolina Department of Health &Human Services Certification #37804
South Carolina (DHEC)Laboratory ID # 99OD5 North Carolina (DENR) Certification #248
Station Name :BURLINGTON Job Number :03-JUL-0339
Sample ID #23024529 Desktop 9 Customer ID :RALPH ROBERTS
Sample Description : MW-3 (OVERBURDEN WELLS )
Collection Date : 25-Jul-03 08 :05 :00 Date Retceived in Laboratory : 14-Jul-03 TypeofSample :MGPSITE
ReferenceMethod:EPA310 .11SM2320B Data Posted :8110=0323 :48:5 0
ALKALINITY fTOTAL INFLECTION POINT)ALKALINITY 0.73 rn-ieq/L .
Reference Method:EPA 200.7/6010B Data Posted :7/3012003 16 :30:2 5
IRON BY ICP (DIGESTEDL_IRON 0 .512 mguF1-_
Reference Method:EPA 200.7/6010B Data Posted :7130/2003 16 :30:2 5
MANGANESE BY ICIP (DIGESTED)MANGANESE 0 .031 nngfl,
Reference Method,EPA 300.0 Data Posted 713112003 11 35 1 0
MG-NIL BY CALCULATION -NITRATE _R._62 mg-NIL
Reference Method:EPA 300.0 Data Posted :7/30/2003 13 :58:3 5
NITRATE IC)NITRATE 2 .75 mg/L
Reference Method:EPA 300.0 Data Posted :713012003 13 :58:3 5
SULFATE SULFATE 12 .75
Reference Method: Data Posted :8/26/2003 15 :29 :44
VARIOUS SAMPLE TYPES SUBMITTED TO PACE PACE TESTCOMPLETED
J
Sample ID #:23024530 Desktop #Customer ID :RALPH ROBERT S
Sample Description : PMWB-S (OVERBURDEN WELLS)
Collection Date : 24-Jul-03 13 :30 :00 Date Received in Laboratory : 14-Jul-03 TypeofSampie :MGPSITE
Reference Method :EPA310.1/SM2320B Data Posted 8/10/2003 23 48 50
ALKALINITY (TOTAL INFLECTION POINT)ALKALINITY 6 .04 mq_q/L
ReferenceMethod :EPA200 .7/601013 Data Posted :7/3012003 1&30 :26
.-IRON BY ICP (DIGESTED)IRON 30 .267 mgII
ReferenceMethod EPA200 .7/6010B Data Posted 7130/2003 16 30 :26
MANGANESE BY ICP (DIGESTED)_MANGANESE 0 .215 mg/L
Reference Method :EPA 300 .0 Data Posted:713112003 11 :35 :1 2
MG.-N/L.BY CALCULATION NITRA TE 0.28 mg-N/L
Reference Method :EPA 300o Data Posted 7/3012003 13 59 0 6
NITRATE (IC)NITRATE 1 .25 mg/L
ReferenceMethod :EPA300 .0 Data Posted :7130/2003 13 59 0 6
SULFATE (C)SULFATE 6 .01 mg/L
vml "'g~ lh~ hw,~No .1I&Min Goiemwd 812 -12003 09.42 .41 http ://dewww/cssenv/Iah-srv/P~Ig .
Duke Duke Energy Analytical Laborator y
Phone [phone] Fax [phone]Nnergy.13339 Hagers Ferry Road Huntersville,INC 28078-7929
McGuire Nuclear Complex - MG03A 2
Certificate of AV&nxkiysi!s
New York State Department of Health Certification # 11717Oklahoma Department of Environmental Quality Certification # 9930Kansas Department of Health and Environment Certificate #E4031 1North Carolina Depannnent of Health &Human Services Certlicaton ft 37804
South Carolina (DHEC)Laboratory ID # 99006 North Carolina (DENR) CerDfication A 248
Station Name:BURLINGTON Job Number:03-JUL-0339
Sample ID #:23024530 Desktop #Customer ID RALPH ROBERTS
Sample Description : PMWB-S (OVERBURDEN WELLS )
Collection Date: 24-Jul-03 13 :30 :00 Date Received in Laboratory: 14-Jul-03 TypeofSample :MGPSITE
E
Reference Method : Data Posted:8126/2003 15 :29 48
VARIOUS SAMPLE TYPES SUBMITTED TO PACE PACE TEST COMPLETED
Sample ID #:23024531 Desktop #Customer ID :RALPH ROBERTS
Sample Description :P-IS (OVERBURDEN WELLS )
Collection Date : 26-Jul-0315 :50 :00 Date Received in Laboratory : 14-Jul~03 Type of Sample MGP SITE
ReferenceMethod:EPA310.1/SM2320B Data Posted :811012003 23 :48 :50
__ALKALINITY (TO ALKALINITY 7 .60 rneqIL.
Reference Method :EPA 200 .7/60108 Data Posted :7/3012003 16 :30 2 6
[RON BY ICP_(PIGEqTED)_IRON 0 .686 mqII
ReferenceMethod :EPA2007/601013 Data Posted:7/30/2003 16 30 2 6
MANGANESE BY ICPDIGESTEDI MANGANESE 1 .767 m9IL
Reference Method :EPA 300 .0 Data Posted :7/31/2003 11 35 1 5
MG-N/L BY CALCULATION NITRATE <0 .02 mg-NIL
Reference Method EPA 300 .0 Data Posted :7/3012003 13 59 30
NITRATEACJ,NITRATE < 0 .10 mg/L
Reference Method :EPA 300o Data Posted :713012003 13 59 30
SULFATE (IP)_ -SULFA TE 52 .32 mg/L
Reference Method Data Posted :8/26/2003 15 :29 :5 2
VARIOUS SAMPLE TYPES SUBMITTED TO PACE PACE TEST COMPLETED
Sample ID #:23024532 Desktop #Customer ID RALPH ROBERTS
Sample Description : PMWC-S (OVERBURDEN WELLS )
Collection Date : 224ul-03 15 :00 :00 Date Received in Laboratory : 14-jul-03 TypeofSample :MGPSITE
ReferenceMethod :EPA310 .1/SM2320B Data Posted 8/1012003 23 48 50
ALKALINITY (TOTAL INFLECTION POINT)ALKALINITY 3 .59 meq/L
ReferenceMethod EPA200,7160108 Data Posted :8/12/2003 08 :00 :3 0
IRON BY ICP (DIGESTED)IRON 20.053 ring/I
Reference Method :EPA200.7/6010B Data Posted 8/1212003 08 00 3 0
MANGANESE BY ICP (DIGESTED)MANGANESE 2 .383 mg/L
V,,ii . ... . .. lh~lw,.Noa t.........I N12-12003 09 42 41 IMP //dcwww/cseziv/lal,_srv/
Duke Duke Energy Analytical Laboratory
Phone:[phone] Fax :[phone]
13339 Hagers Ferry Road Huntersville .NC28078-7929
McGuire Nuclear Complex - MG03A 2
c 4B rt i f i o-- a t e~a f Aftna-slysis
New York State Department of Health Certification 9 1171T
Oldahoma Department of Environmental QualAy Certification 9 9930
Kansas Department of Health and Environment Certificate # E-1031 1
North Carolina Department of Health &Human Services Certification #3T8D4
South Carolina QHEC)Laboratory ID # 99005 North Carolina (DENR) Certification #248
Station Name :BURLINGTON Job Number :03-JUL-0339
Sample ID #:23024532 Desktop #Customer ID :RALPH ROBERTS
Sample Description : P11i (OVERBURDEN WELLS )
Collection Date : 22~.Iul-03 15 :00 :00 Date Received in Laboratory: 144ul-03 Type of Sample :MGP SITE
Reference Method :EPA 300 .0 Data Posted:7128/2003 1 1 :27 :3 6
MG-N/1.BY CALCULATION NITRATE <0 .02 mg-NIL
Refereroe Method :EPA 300 .0 Data Posted: 7t24/2003 15:58 :0 3
NITRATE IC)NITRATE -< 0.10 mgLL__
Reference Method :EPA 300.0 Data Posted :712512003 11 :23 :25
SULFATE (IC)__SULFATE I .S9
Reference Method: Data Posted : 7/31t2003 13 :18 :1 3
VARIOUS SAMPLE TYPES SUBMITTED TO PACE PACE TEST COMPLETED
Sample ID #:23024533 Desktop #Customer ID :RALPH ROBERTS
Sample Description : MW-5 (OVERBURDEN WELLS )
Collection Date : 22-Jul-03 10:15 :00 Date Received in Laboratory : 14-Jul-03 TypeofSample MGPSITE
ReferenceMethDd :EPA310 .11SM2320B Data Posted :8110/2003 23 :48 :5 0
, ALISALINITY(TOTA~INFLECTION POINT)_______ALKALINITY 9 .37 ni
Reference Method :EPA 200.716010B Data Posted:8/121200308 :00:3 0
IRON BY ICP (DIGESTED) -IRON 4 .483 ringti
ReferenoeMethod:EPA200.7/6010B Data Posted!8/1212003 08 :00:3 1
_?ESTED),MANGANESE-0 .531 mg/LMANGANESEBYICPffjIC
Reference Method :EPA 300 0 Data Posted :7/2812003 11 :27 :37
MG-NIL BY CALCULATION NITRATE <0 .02 nni
ReferenceMethDd :EPA 300 .0 Data Posted : 7124/2003 15 :58 :24
NITRATE (IC)NITRATE < 0 .10 ri
Refefence, Method :EPA 300~O Data Posted 7/2512003 11 :23 :26
SULFATE [C)SULFATE 45 .42 mg/L
Reference Method : Data Posted :7/3112003 13:18 :1 3
VARIOUS SAMPLE TYPES SUBMITTED TO PACE PACE TEST COMPLETED
Vm,. ... ..
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je,,,H G.... .....I N12-120030 42 41 http I/dL..,vv/csscnv/IaI,-.,rv/
Duke Duke Energy Analytical Ublorator y
Phone [phone] Fax :704-87~,5038Nnerg.13339 Hagers Ferry Road Huntersville,NC 28078-7929
McGuire Nuclear Complex - MG03A2
Certificata 4of fflLnzalyais
New York State Department of Health Certification #11717
Oklahoma Department of Environmental Quality Certification # 9930
Kansas Department of Health and Environment Certificate # E-1D31 1
North Carolina Department of Health &Human SeNces Certification # 37804
South Carolina (DHEC)Laboratory ID # 99006 North Carolina (DENR) Certification 248
-Station Name :BURLINGTON 03--JUL-0339
Sample ID 23024535 Desktop #Customer ID :RALPH ROBERTS
Sample Description : PIMW`M-S (OVERBURDEN WELLS )
CollectionDate : 211,1ul-031111 :35 :00 Date Received in Laboratory : 14-Jul-03 TypeofSample :MGPSITE
ReferenceMethod :EPA310 .11SM232013 Data Posted:8/10/2003 23:48 :50
-ALKALINITY (TOTAL INFLECTION POI"T ALKALINITY 0 .33 megIL
ReferenceMethod :EPA200.7/6010B Data Posted 811212003 08 00 3 1
IRON BY ICIP DIGESTED)IRON 0 .035 mg/I ......
Reference Method :EPA 200 .7/601 OB Data Posted 8/1212003 08:00 3 1
MANGANESE BY ICP (DIGESTED)MANGANESE 0 .028 mgAL
Reference Method :EPA 300 .0 DataPosted 7/25/200310271 0
MG-NIL BY CALCULATION NITRATE 1 .43 mg-NIL
Refenence Method :EPA 300 .0 Data Posted : 7124/2003 14 :54 :2 1
NITRATE [IC)NITRATE 6.35 Mg/L .
Reference Method :EPA 300 .0 Data Posted 7124/2003 14 :20 :44
SULFATEJIC).. . ....SULFATE .11 .80 mg/L .
Reference Method : Data Posted 7131/2003 13 :18 :1 3
VARIOUS SAMPLE TYPES SUBMITTED TO PACE PACE TEST COMPLETED
Sample ID 23024536 Desktop #Customer ID :RALPH ROBERTS
Sample Description : PIMWL-S (OVERBURDEN WELLS )
Collection Date : 24-Jul-03 08 :35:00 Date Received in Laboratory : 14-Jul-03 TypeofSample :MGPSITE
Referencelviethod :EPA310 .1/SM2320B Data Posted :8/10/2003 23 :48:5 0
ALKALINITY (TOTAL INFLECJION POINT),____ALKALINITY 3 .70 rrreq/L
ReferenmMethod:EPA200,71601013 Data Posted :7130/2003 16 30:2 6
IRON BY ICP (DIGESTED)IRON 30 .033 mg/I
ReferenceMethod:EPA200.716010B Data Posted .7/30/2003 16 :30,2 6
MANGANESE BY ICP (DIGESTED)MANGANESE 1 .987 mg/L
Reference Method:EPA 300,0 Data Posted 7131/2003 11 35:1 7
MG-N/L BY CALCULATION NITRATE <0 .02 mg-N/L
Reference Method:EPA 300 0 Data Posted 7/30/2003 14 :00.0 3
NITRATE [IC)NITRATE < 0.10 mg/L
Reference Method EPA 300o Data Posted 7/30/2003 14 :00:0 3
SULFATE (IC)SULFATE 21 .10 mg/L
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Duke Duke Energy Analytical Laboratory
Phone [phone] Fax:[phone]
13339 Hagers Ferry Road Huntersville .NC 28078-7929
McGuire Nuclear Complex - MG03A 2Cartificata at Aetnaly-sis,
NewYork State Department of Health Certification 9 11717
OWahoma Department of Environmental Quality Certification If 9930
Kansas Department of Health and Environment Certificate # E-1031 1
North Carolina Department of Health &Human Services Certification # 378D4
South Carolina (DHEC)Laboratory ID 99005 North Carolina (DENR) Certification 248
Station Name :BURLINGTON Job Number:03-JUL-0339
L
Sample ID #: 23024536 Desktop #Customer ID:RALPH ROBERTS
Sample Description : PMWL-S (OVERBURDEN WELLS )
Collection Date : 24-Jul-03 08 :35 :00 Date Received in Laboratory: 14~.Iu"3 TypeofSample :MGPSITE
Reference Method : Data Posted :8/26/2003 15 :29 :58
VARIOUS SAMPLE TYPES SUBMITTED TO PACE PACE TEST COMPLETED
Sample ID #: 23024537 Desktop #Customer ID :RALPH ROBERTS
Sample Description :FIELD BLANK (OVERBURDEN WELLS )
Collection Date : 26-Jul-03 08 :35 :00 Date Received in Laboratory : 14-Ju"3 TypeofSample :MGPSITE
ReferenceMethod :EPA310 .1/SM2320B Data Posted :811012003 23:48 :5 0
ALKALINITY (TOTAL INFLECTION POINT)ALKALINITY <meq/L
RefenenoeMethod :EPA200 .7/60108 Data Posted!7130/2003 16:30 :2 7
IRON BYjCP (DIGESTED)IRON 0 .019 M I
ReferenceMethod :EPA200 .7/6010B Data Posted :7/3012003 16 :30:2 7
MANGANESE BY ICP (MG IESTED _ _ _MANGANESE < 0 .005 mg/L.
Referenoe Method :EPA 300 .0 Data Posted :TM/2003 11 :35:2 0
MG-NIL.BY CALCULATION NITRATE <0 .02 mg-N/L
Reference Method :EPA 300 .0 Data Posted :7/3012003 14 :00 :3 0
NITRATE (IC)NITRATE < 0 .10 mg/L.
Reference Method :EPA 300d Data Posted 7/3012003 14 :00 :3 0
SULFATE (IC), -SULFATE-<.0 .10 mgLL
Reference Method : Data Posted 812612003 15 :30 :03
VARIOUS SAMPLE TYPES SUBMITTED TO PACE PACE TEST COMPLETED
I VenhWan0APMVed8y. Date
V"i .'-1, lh~ hw~No wJeep)"(;v)jemeeIX/2-/2()0J Dr) 42 41 htip ://dww~/essenv/ki1h-srv/
Duke Duke Energy Analytical Laborator y
Phone:[phone] Fax :[phone]PoEneily.13339 Hagers Ferry Road Huntersville,NC 28078-7929
McGuire Nuclear Complex - MG03A 2
Certificata of Analysis
New York State Department of Health Certif ication # 11717Oklahoma Department of Environmental Quality Certification # 9930Kansas Department of Health and Environment Certificate # E-1031 1
North Carolina Department of Health &Human Services Certification # 37804South Carolina (DHEC)Laboratory ID # 99ODS North Carolina (DENR) Certification #248
SampleiD#: 23024528 Job#:03-JUL-033 9
Sample Description :TRIP BLANK (OVERBURDEN WELLS )
Collection Date : 2Wul-03 04 :30 :00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
OG IXARAMETERS;IN WATER BY GCIMS - 8260
Test Code : MS8260MGPW Test Method : SW-846 503013/8260B Date Posted :07128103
Resuft Flag
Benzene < 0.60 jg/L 0 .50 Vg/L 0
Toluene < 1 .0 uglL 1 .0 1 .9/1- 0
Ethylbemene < 1 .0 pg/L 1 .0 pg/L a
m-p-Xylene <2 .0 pg/L 2.0 ug/L 0
o-Xylene < 1 .0 pg/L 1 .0 pglL 0
Sample ID #:23024529 Job#:03,JUL-033 9
,,Sample Description :MW-3 (OVERBURDEN WELLS )
'llection Date : 25-Jul-03 08:05:00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
MGP PARAMETERS IN WATER BY GC/MS - 8260
Test Code : MS8260MGPW Test Method : SW-846 5030B18260B Date Posted :07128/03
Result -_ReportmgjLmut Fla g
Benzene < 0 .50 pg/L 0 .50 ug/L 0
Toluene < 1 .0 pg/L 1 .0 P91 0
Ethylbenzene < 1 .0 pg/L 1 .0 P911-0
m-p-Xylene <2 .0 pg/L 2.0 pg/L 0
o-Xylene < 1 .0 pg/L 1 .0 Pg/L 0
Sample ID #:23024530 Job#:03-JUL-033 9
Sample Description :PMWB-S (OVERBURDEN WELLS )
Collection Date: 24-Jul-03 13 :30:00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
77
iAGP PARAMETERS IN WATER BY GC/MS - 826 0
Test Code : MS8260MGPW Test Method : SW-846 5030B/8260B Date Posted :07/28103
Result Reportmg Limit Flag
Benzene 190 pg/L 2 .5 pg/L 0
Toluene 130 Vg/L 5 .0 jglL 0
Ethylbenzene 340 pg/L 5 .0 jg/l . 0
m-p .Xylene 140 pg/L 10 ug/L 0
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Duke Duke Energy Analytical Laborator y
PI 704-875-5245 Fax :[phone]ftergy.13339 Hagers Ferry Road Huntersville .NC 28078-7929
McGuire Nuclear Complex - MG03A 2
Certificalbe of Analysis
New York State Department of Health Certification # 11717Oklahoma Department of Environmental Quality CerlificatiOn # 9930Kansas Department of Health and Environment Cerfifical #E4D31 1North Carolina Department of Health &Human Services Certification #37804
South Carolina (DHEC)Laboratory ID# 99005 North Carolina (DENR) Certification 9 248
FERRUZZI ~': ~i i 1 1! 1 11 ''1 11 i I I i I I ii i 1 1 1 11 1:11!i i ~i i 111 1i1111 iI i1 111
SamplI 23024530 Job#:03-JUL-0339
Sample Description :PMWB-S (OVERBURDEN WELLS )
Collection Date : 24-Ju"3 13 :30:00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
OGP PARAMETERS IN WATER BY GC/MIS - 826 0
Test Code. MS8260MGPW Test Method : SW-846 5030B/8260B Date Posted :07128103
Result Reporting Limit Fla g
o-Xylene 100 pg/L 5 .0 pg/L 0
Sairl 23024531 JoI 03-JUL-0339
Sample Description :PAS (OVERBURDEN WELLS )
Collection Date: 25~Jul-03 15 :50:00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
&
AgIVW ARAMETERS IN WATER BY GC/MS -826 0
W-Testc-od-e-: MS8260MGPW Test Method : SW-846 503OB18260B Date Posted :07/28/03
Result Reporting Limit Flag
Benzene 0 .53 pill 0 .50 pg/L 0
Toluene < 1 .0 pg/L 1 .0 pgtL 0
Ethylbenzene < 1 .0 pl 1 .0 pg/L 0
m-p-Xylene <2 .0 pg/L 2.0 ug/L 0
o-Xylene 2 .0 pg/L 1 .0 pg/L 0
~imgmsL~
Samphill 23024532 Job#: 03-JUL-033 9
Sample Description :PMWI (OVERBURDEN WELLS )
Collection Date : 22-Jul-03 15 :00 :00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
MGP PARAMETERS IN WATER BY GCIMS - 8260
Test Code MS8260MGPW Test Method : SW-846 50306/8260B Date Posted :07128/03
Result Reporting Limit Fla g
Benzene 2 .7 pglL 0.50 pg/L 0
Toluene 1 .0 pg/L 1 .0 pg/L 0
Ethylbenzene 2 .0 pg/L 1 .0 Vg/L 0
m-p-Xylene <2 .0 poll 2 .0 pg/L 0
o-Xylene 4 .1 il 1 .0 pg/L 0
Visit as rat the IntraNct a tR',......... ....d 112 W111 1 ", 15 21 htip ://dcw .w/cise .iv/lab-srv/
Duke Duke Energy Analytical Uboratior y
Phone:[phone] Fax :[phone]
13339 Hagers Ferry Road Huntersville .NC28078-7929
McGuire Nuclear Complex - MG03A 2
Cartificate of Analysis
New York State Department of Health Certif ication # 11717Oklahoma Department of Environmental Quality Certification # 9930Kansas Department of Health and Environment Certificate # E-1031 1
North Carolina Department of Health &Human Services Certification #37804
South Carolina (DHEQ Laboratory I D # 99006 North Carolina (DENR) Certification #248
SamplelD#: 23024533 Job#:03-JUL-0339
Sample Description : MW-5 (OVERBURDEN WELLS )
Collection Date : 22-Ju"3 10 :15:00 Site :BURLINGTON Sample Type: MGP SITE Desktop #
OGP PARAMETERS IN WATER BY GCIMS - 826 0
Test Code: MS8260MGPW Test Method : SW-846 6030B18260B Date Posted :07/28/03
Result Repo Limit Flag
Benzene < 0 .50 lig/L 0.50 pg/L 0
Toluene < 1 .0 pg/L 1 .0 pg/L 0
Ethylbenzene < 1 .0 pg/L 1 .0 pg/L 0
m-p-xylene <2 .0 pglL 2 .0 pg/L 0
o-Xylene < 1 .0 pg/L 1 .0 pg/L 0
SamplelD#: 23024535 Job#:03~JIJL-033 9
,,Sample Description :PMWM-S (OVERBURDEN WELLS )
,liection Date : 21-Jul-0311 :35 :00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
GP PARAMETERS IN WATER BY GC/MS - 8260
Test Code : MS8260MGPW Test Method : SW-8465030B/8260B Date Posted :07/28103
-fe~ -lKe.-mungrLimit Fla g
Benzene < 0 .50 pg/L 0 .50 pg/L 0
Toluene < 1 .0 pg/L 1 .0 pg/L 0
Ethylbenzene < 1 .0 pg/L 1 .0 pg/L 0
m-p-Xylene <2 .0 pg/L 2.0 Vg/L 0
o-Xylene < 1 .0 pg/L 11 .0 VglL 0
7 --mz;,7,72 7
SamplelD#:23024536 Job#:03-JUL-033 9
Sample Description :PMWL-S (OVERBURDEN WELLS )
Collection Date : 24-Jul-03 08 :35:00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
7T -7
iMGP PARAMETERS IN WATER BY G C/MS - 826 0
Test Code : MS8260MGPW Test Method : SW-846 503OB/8260B Date Posted :07/28103
Result Reporting Limit Fla g
Benzene 0 .50 Vg/L 0 .50 Pg/L 0
Toluene < 1 .0 pg/L 1 .0 pg/L 0
Ethylbenzene < 1 .0 pg/L 1 .0 pg/L 0
m-p-Xylene <2 .0 P911 . 2 .0 pglL 0
V,,,I,,s ... I tk lw .No .1hup:/lde%vww/esscnv/lab-srv/
PDuke Duke Energy Analytical Laboratory
anergy.Phone [phone] Fax,704-875.503 8
13339 Hagers Ferry Road Huntersville,NC 28078-7929
McGuire Nuclear Complex - MG03A 2
C4ertificate of Analysis
Now York State Department of Health Certification # 11T17
Oklahoma Department of Environmental Quality Certification 9 9930
Kansas Department of Health and Environment Certificate # E-1031 1
North Carolina Department of Health &Human Services Certification # 3780 4
South Carolina (DHEQ Laboratory ID # 99005 North Carolina (DENR) Certification 248
7--jj
SamplelD#: 23024536 Job #: 03~.JIUL-033 9
Sample Description :PMWL-S (OVERBURDEN WELLS )
Collection Date : 24-Jul-03 08 :35 :00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
~11131P~PAMMETERS IN WATER BY GCIMS - 826 0
Test Code : MS8260MGPW Test Method : SW-846 503013/8260B Date Posted :07128/03
Result ___jRqpoqinZLjrTq_laR-9-
o .Xylene < 1 .0 ug/L 1 .0 pg1L 0
Sample ID #: 23024537 Job#:03-JUL-0339
Sample Description :FIELD BLANK (OVERBURDEN WELLS )
Collection Date : 25-JuW3 08:35:00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
AINJIGIP PARAMETEMS IN WATER BY GCM - 8260
-Te-s-t Code : M-S826-0Mt3P-W- Test-Metho-d :-SW--8-4--6-60--30-B-18-260-B------ -Date Posted :07. /28/03 -
Resuft Reporifing_Lmt Flag
Benzene < 0 .50 pg/L 0 .50 pg/L 0
Toluene < 1 .0 pg/L 1 .0 pg/L 0
Ethylbenzene < 1 .0 pg/L 1 .0 pg/L 0
m-p.Xylene <2 .0 ug/L 2.0 pgIL 0
o-xylene < 1 .0 pg/L 1 .0 pg/L 0
------------------------------------
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4 Rr,.rr Enn" siroauttd due 1.,--d onallts .ed efil .h ..
5 Smssple Results Should or Be U -ed For Regulator, Purpose ,
6 Anal,le dtlers,el below l1bo"tory rePonnna Inult or ~ eshmsue d
7 Reported concentration - h,-b-muon of more th,l one wociar,
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Pace Analytical Services, Inc .
9800 Kincey Avenue, Suite 100ceAnalXicalHuntersville,NC 28078
Phone :[phone]
Fax :[phone]
August 21,200 3
Mr . Paul J .Fitzgerald
Duke Powe r
Mail Code :MG03A.2
13339 Hagers Ferry Road
Huntersville,NC 28078-792 9
RE : Client Project ID : 03-JUL-039/Ml 1356
Pace Project ID : 924779 6
Dear Mr . Fitzgerald :
I am writing in regards to your concerns about the recovery of the acid surrogates in several of the
samples associated with the above referenced project .
1 have reviewed the extraction log and the raw data for these samples and believe that this is an
extraction problem with these samples . Four of the samples (23024532/PMWC-S ;
23024516/PMWC-D ; 23024523/PMWC-BR ; 23024524/PMWH-BR) emulsified during the
extraction process. As stated in the laboratory report, there was insufficient sample volume available
for reextraction and reanalysis of these samples .
LCS 923180525,which was extracted alongside the samples, shows acceptable recoveries for
phenol-d5 and 2-fluorophenol . Other samples analyzed on the same day but not extracted on the
same day show recoveries for these two surrogates in the range of 50-70%recovery . Therefore,I do
not believe that the low recoveries are caused by a problem with the instrumentation .
Our acceptance limits for phenol-d5 and 2-fluorophenol are 10-125%,which are consistent with
EPA data for these surrogates .
If you have any additional questions or need additional information, please contact me at
704-875-9092 Ext .229 .
Sincerely yours,
Mavis Jones
Quality Manager
Pace Anslyfivol Urden Ine
M Kincey Awatat,Svito 100
a Analyfical"Hunkfwlle.AC 28078'Ce Phom 704 875 9092ivim.paoelabs .ocerr Far 704.875.9091
August 28,200 3
Mr .Joy Perkins
Duke Power
13339 Begets Perry Road
MG30k2
Huntersville,VC 2007 6
RE : Lab Project Rumbir:3 924779 6
Client Project ID : 03-JUL-0339/NI1356
Dear Mr . Perkins ;
Enclosed are the analytical results for sample(s) received by the laboratory on July 23, 2003 .Results reported
herein conforse to the asset current NELAC standards, here applicable, iseless othemise narrated in the body of
the report .
If you have any questions concerning this report please feel free to contact me .
sincerely ,
a&.
Kristi Tart
Kristi .Tartlipacelabs .con,
Project Manager
Enclosures
1 aboratory Clurld cefian IDLaboratoryCarlificationIDSREPORT OF LABORATORY ANALYSIS KY Drinking Water 9MRICWastewater 1 2
NC Drinking Water 37706 This report shall not be reproduced, except in full,VA Drinking Water 213
SC 99006 without the written consent of Pam ArieVical Sewices . Inc. FL NELAP E87627
Pace Ana4lical Serwar, Inc.98M Kincey Awnuo, Sub 100
a
11full Hur;Wsvifie,NC 28078CROUMalyfical"Phone [phone]~.paoelabs .com Far M4.875.9091
C,
Lab Project Number :924779 6
Client Project ID : 03-JUL-0339/NI135 6
Lab Sample No :923171987 Project Sample Number ;9247796-001 Date Collected ;07/22/03 15 :00
Client Semple ID :23024532/PNWC-S Matrix : Water Date Received :07/23/03 11 :50
Parameters Results Unito Report Limi Analyzed By CAB No .Goal Roglant
GCIMS Sentivolatiler e
Seadvolatile Organics Prep/Method : EPA 827 0
Acenaphthene 86 . ug/l 10 . 07/29/03 08 :05 BET 83-32-9
Acensylothylone No USA 10 . 07/29/03 08 :05 BET 208-96-6
Aniline No ug/l 10 . 07/29/03 08 :05 BET 62-53-3
Anthracene No ug/l 10 . 07/29/03 08 :05 BET 120-12-7
BesaxoWasithracODO ND ug/l 10 . 07/29/03 06 :05 BET 56-55-3
Beacto(Opyrane No ug/l 10 . 07/29/03 00 :05 BET 50-32-B
Basuto (b) f luoranthone ND ug/l 10 . 07/29/03 00 ;05 BET 205-99-2
smio(g,bli)parylme No ug/l 10 . 07/29/03 08 :05 BET 191-24-2
Sense (k) f luoranthene ND ug/l 10 . 07/29/03 08 :05 BET 207-00-9
Bazzoic acid No ug/l 50 . 07/29/03 08 :05 BET 65-85-0
Bentryl alcohol ND ug/l 20 .07/29/03 08 :05 BET 100-51-6
4-BromophanylphOMY1 Other No ug/l 10 . 07/29/03 0805 BET 101-55-3
Butylbecoxylphthalate No ug/l 10 . 07/29/03 00 :05 BET 85-68-7
4 -Chloro .3 -methylphenol No ug/l 20 .07/29/03 00 :05 BET 59-50-7
4-Chloroarailine No ug/l 20 .07/29/03 08 :05 EST 106-47-8
biz(2-Ch1oro6thoxy)mzthAnO ND USA 10 . 07/29/03 08 :05 BET 111-91-1
bio(2-Chloroothyl) other No Ug/l 10 . 07/29/03 08 :05 BET 111-44-4
bis(2-Chloroisopropyl) other No Ug/l 10 . 07/29/03 08 :05 BET 39630-32-9
2-Chloronaphthalene No Ug/l 10 . 07/29/03 08 :05 BET 91-58-7
2-Chlorophenol No ug/l 10 . 07/29/03 08 :05 BET 95-57-8
4-Chlorophanylphenyl ether No ug/l 10 . 07/29/03 08 :05 BET 7005-72-3
Cbryoeafe ND ug/l 10, 07/29/03 08 :05 BET 218-01-9
Dibenz (a, h) anthracene No ug/l 10 . 07/29/03 08 :05 BET 53-70-3
Dibewzofuran No ug/1 10 . 07/29/03 08 :05 BET 132-64-9
1 .2-Dichlorobartzene No ug/l 10 . 07/29/03 011 :05 BET 95-50-1
1,3-Dichlorobwzene No ug/l 10 . 07/29/03 013 :05 BET 541-73-1
1,41-Dichlorobenzene No ug/l 10 . 07/29/03 08 :05 BET 106-46-7
3,3--Dichlorobanzidine No ug/l 20 .07/29/03 08 :05 BET 91-94-1
2,4-Dichlorophanol ND Ug/l 10 . 07/29/03 08 :05 BET 120-83-2
Diethylphthalate No Ug/l 10 . 07/29/03 08 :05 BET 84-66-2
2,4-DimthylpheuOl ND ug/l 10 . 07/29/03 08 :05 BET 105-67-9
Dimethylphthalate No ug/l 10 . 07/29/03 08 :05 BET 131-11-3
Di-n-butylphthalate No ug/l 10 . 07/29/03 08 :05 BET 84-74-2
4,6-Dinitro-2-mothylph=Ol ND ug/l 50 . 07/29/03 00 :05 BET 534-52-1
2,4-Dinitrophenol No ug/l 50 . 07/29/03 08 :05 BET 51-28-5
2,41-Dinitrotoluene No ug/1 10 . 07/29/03 08 :05 BUT 121~14-2
2,6-Dinitrotolume No ug/1 10 . 07/29/03 08 :05 BET 606-20-2
Date ;00/20/03 Is
l,trontgry Cerlificafign IDS[ftboratorv unification IDs REPORT OF LABORATORY ANALYSIS KY Drinking Water 9MNCWastirvater 1 2
NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213
SC 99M mover the witten consent of Pau Analytical Services.Im FL NELAP E87627
Poce Afflityllool Sariden,Inc.
98M Kincey Avenue, Suite 100
HO&WIle,AC 28078;a5*'UceMq1yqca1`v Phom 704.8759MMM.P80alabs.com AU.704.875.9091
Lab Project Number :924779 6
Cliezut Project ID : 03-JUL-0339/NI135 6
Lab Sawle NO : 923171997 Project Sample Number :9247796-001 Date Collected :07/22/03 15 :00
Clieut Sample ID ; 23024532/PKWC-S Matrix ; Water Date Received ;07/23/03 11 :50
Parameters Results units Rewrt Limi Analyzed By CAB NO,Duel Realis t
Di-n-octylphthalate ED ug/l 10 . 07129/03 08 :05 BET 117-84-0
1,2-Diph=ylhydrazine ED ug/l 20 .07/29/03 08 ;05 BET 122-66-7
bis(2-Ethylhexyl)phtb,alate ED uq/l 10 . 07/29/03 08 :05 BET 117-81-7
Pluorazitheirse ND ug/l 10 . 07/29/03 08 :05 BET 206-44-0
Fluoreae 22 .ug/l 10 . 07/29/03 08 :05 BET 86-73-7
R"achloro-1, 3-butadiane ND ug/1 10 . 07/29/03 08 ;05 BET 87-68-3
Hasachlorobelazene ND ug/l 10 . 07/29/03 080S BET 118-74-1
Hexachlorocycloperstadiernis HD ug/1 10 . 07/29/03 08 ;05 BET 77-47-4
Hemachloroathace ND ug/l 10 . 07/29/03 08 :05 BET 67-72-1
Indeno (1,2,3-cd)pyreue ND ug/1 10 . 07/29/03 08 :05 BET 193-39-5
Isophorme ED ug/1 10 . 07/29/03 08 :05 BET 78-59-1
2-Methyluaphthalinse 21 .ug/l 10 . 07/29/03 08 :05 BET 91-57-6
2-Methylpheuol (0-Cresol)ED ug/l 10 . 07/29/03 08 :05 BET 95-48-7
3&4-Methylphecol ED ug/l 10 . 07/29/03 08 :05 BET
Naphtlaalerse 57 . USA 10 . 07/29/03 08 :05 BET 91-20-3
2-Nitroulusiline ED uq/l 50 . 07/29/03 06 ;05 BET 88-74-4
3-Mitrousuilins,ED ug/l 50 . 07/29/03 08 :05 BET 99-09-2
4-Nitrossailine ND USA so . 07/29/03 08 :05 BIT 100-01-6
Nitrobelazees ND ug/l 10 . 07/29/03 08 :05 BET 98-95-3
2-Nitrophelsol ND ug/l 10 . 07/29/03 08 :05 BET 88-75-5
4-Mitropheniol ND ug/l 50 . 07/29/03 08 :05 BET 100-02-7
M-Nitrosodimethylamine ND ug/l 10 . 07/29/03 08 :05 BET 62-75-9
N-Nitroso-di-n-propylamine ED ug/i 10 . 07/29/03 08 :05 BET 621-64-7
N-Nitrooodiphwylamine ED ug/1 10 . 07/29/03 08 :05 BET 86-30-6
Pautachlorophectol ED ug/l 50 . 07/29/03 08 :05 BIT 87-86-5
Pherfarithrere ED ug/l 10 . 07/29/03 08 :05 BET 85-01-8
Phenol ND ug/l 10 . 07/29/03 06 ;05 BET 108-95-2
Pyrene ND uq/l 10 . 07/29/03 08 :05 BET 129-00-0
1,2,4-Trichloroberizeuse ND ug/l 10 . 07/29/03 08 :05 BET 120-82-1
2,4,5-Trichlomphawl ND ug/l 50 . 07/29/03 08 :05 SET 95-95-4
2,4,15-Trichlorophernol ND ug/l 10 . 07/29/03 08 :05 BET 68-06-2
Nitrobenzace-dS (S) 68 % 07/29/03 08 :05 BET 4165-60-0
2-Fluorobipheuyl (S) 72 % 07/29/03 08 :05 BET 321-60-8
Terphenyl-dl4 (S) so % 07/29/03 08 :05 BET 1718-51-0
Phenol-d5 (S) 1 % 07/29/03 08 :05 BET 4165-62-2 1,2
2-Fluorophemol (S) 3 % 07/29/03 08 :05 BET 367-12-4 1,2
2,4,6-Tribrossophsool (S)21 % 07/29/03 08 :05 BET
Date Extracted 07/25/03 07/25/0 3
Date :08/28/03 Fag.: 2 of 18
I abaratory r.,nificat an IIghorrunry Certification I REPORT OF LABORATORY ANALYSIS KY Drinicing Water 9DO90NCWastewater 1 2
NC Drinking Water 37706 This report shall not heneproduced . except in full, VA Drinking Water 213
Sc gm without the wrften consent of Pace kialytical Services, hic . FL NELAP E87627
Pace AnsWO&I SaWca Ing
98W 10how Asentiv. Sudit 100
HUMM11A NC28078112cemalytical"Phone [phone]W
Fax.,704.875.9091
Lab Project Number :924779 6
Client Project ID : 03-JUL-0339/KI135 6
Lab Sample No :923171995 Project Sample Number :9247796-002 Date Collected :07/22/03 10 :15
Client Sample ID :23024533/NW-5 Katrixt Water Date Received ;07/23/03 11 :50
Parameters Results Unitis Recort Limit Analyzed By CAB No .Dual Recilant
GCIKS Seinivolatile s
Sectivolatile organics Prep/Method :SPA 827 0
kcanaphthene RD ug/l 10 . 07/29/03 O8s42 BET 83-32-9
Acenaphthylexiss ND ug/l 10 . 07/29/03 08 ;42 BET 208-96-8
Aniline ND ug/l 10 . 07/29/03 08 :42 BET 62-53-3
Anthracene ND ug/l 10 . 07/29/03 08 :42 BET 120-12-7
Bentio(a)wthracene ND ug/l 10 . 07/29/03 06i42 BET 56-55-3
Bmzo(&)pyrma ND ug/l 10 . 07/29/03 06j,112 BET 50-32-8
BeatzoWflucirtuathene No ug/l 10 . 07/29/03 08142 BET 205-99-2
Bmzo(g,b .i)peryl=G ND ug/l 10 . 07/29/03 08 :42 BET 191-24-2
Banzo(k)fluoratithene RD ug/l 10 . 07/29/03 08 :42 BET 207-08-9
Beazoic acid ND ug/l 50 . 07/29/03 08 :42 BET 65-85-0
Bmzyl alcohol ND uq/l 20 .07/29/03 08 :42 BET 100-51-6
4-ar-phwylphenyl ether ND ug/l 10 . 07/29/03 08i,112 BET 101-55-3
Butylboasylphthalate ND USA 10 . 07/29/03 08 ;42 BET 85-68-7
4-Chlor*-3-mthylphmol ND ug/l 20 .07/29/03 08 :42 B9T 59-50-7
4-Chierroaniline ND ug/l 20 .07/29/03 08 :42 BET 106-47-8
bio(2-Chlorootboxy) methane No ug/l 10 . 07/29/03 08 :42 BET 111-91-1
bio(2-Chloroothyl) other ND ug/l 10 . 07/29/03 00 ;42 BET 111-44-4
bia(2-Chlaroisopropyl) ether ND ug/l 10 . 07/29/03 08z42 BET 39630-32-9
2-Chloronaphthalene ND ug/l 10 . 07/29/03 08 :42 BET 91-58-7
2-Chlorophenol ND ug/l 10 . 07/29/03 08 :42 BET 95-57-0
4-Chloraphenylphenyl ether No ug/l 10 . 07/29/03 08 ;42 BET 7005-72-3
Chrysten ND ug/l 10 . 07/29/03 08 :42 BET 216-01-9
Dibenz(:,h) anthracene ND USA 10 . 07/29/03 06 ;42 EST 53-70-3
Dibenzofuran ND ug/l 10 . 07/29/03 08 :42 BET 132-64-9
1,2-Dichlorobenzene No uq/l 10 . 07/29/03 00 :42 BET 95-50-1
1,3-Dichlorobeazene ND ug/l 10 . 07/29/03 08:42 BET 541-73-1
1,41-Dichlorobsuizene No ug/l 10 . 07/29/03 08:42 BET 106-46-7
3,31-Dichlorob=zidine ND ug/l 20 .07/29/03 08 :42 BET 91-94-1
2,4-Dichlorophmol No ug/l 10 . 07/29/03 08 :42 BET 120-03-2
Diethylphthalate ND USA 10 . 07/29/03 08 :42 BET 84-66-2
2 .4-Dimethylphmol ND ug/l 10 . 07/29/03 09 :42 BBT 105-67-9
Dizesathylphthalate ND USA 10 . 07/29/03 08 :42 BET 131-11-3
Di-a-butylphthalate ND ug/l 10 . 07/29/03 08 :42 BET 84-74-2
4,6-Dinitro-2-mthylphenol ND ug/l 50 . 07/29/03 08 :42 BET 534-52-1
2,4-Dinitropheaol ND ug/l 50 . 07/29/03 08 :42 BET 51-28-5
2,4-Dinitrotoluens ND ug/l 10 . 07/29/03 08 :42 BET 121-14-2
2,6-Dinitrotoluenre No ug/l 10 . 07/29/03 08 :42 BET 06-20-2
Date :08/20/03 page : 3 Of is
Lawmmlaufi~i AbOfMON GIEWIM1011 IDS REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090NCWastserater 1 2
NC Drinking Water 37706 This imort stall rot be reprodwed, e=P1 in Wis.VA DrL*ng Water 213
SC gm wthoUt ON Witter CO(dent Of Pace klsVelli ServiOm. IM Fi.NELAP E87627
Pace Ans4lical SeMess, /a:.
W KwW Aoxit Suat 100
H&OSWIlk AC 28078aceAnalyfical~Am 704 873 9092mwpacelabs.com Fax.,704.875.9091
Lab Project Number :9247796
Client Project XD ;03-JUL-0339/KI135 6
Lab Sample No :923171995 Project Sample Number :9247796-002 Date collected :07/22/03 10 :15
Client Sample ID : 23024533/KW-5 Matrix : Water Date Received :07/23/03 11 :50
Parameters Resulto Unite Report Limi Analyzed By ChS No .%tAl.RWLMt
Di-n-octylphtbalate ED ug/l 10 . 07/29/03 08 :42 BET 117-84-0
1,2-Diphany1hydrazine ND ug/l 20 .07/29/03 08 :42 BET 122-66-7
bin (2-Ethylbe3cyl)phthalate RD uq/l 10 . 07/29/03 08 :42 BET 117-81-7
Fluorantheae ND ug/l 10 . 07/29/03 08 :42 BET 206-44-0
Pluorens ED USA 10 . 07/29/03 06 ;42 BET 86-73-7
H"achloro-1,3-butadime ED ug/l 10 . 07/29/03 08 :42 BET 07-66-3
Hexachlorobenzwe ND ug/l 10 . 07/29/03 08 ;42 BET 118-74-1
Remixechlorocyclopentadiene RD ug/1 10 . 07/29/03 08A2 BET 77-47-4
Sexachloroethime ED usr/l 10 . 07/29/03 CSA2 BET 67-72-1
Indeno (1,2,3-cd)pyrons ED ug/l 10 . 07/29/03 08 :42 BET 193-39-5
loophoroade ED ug/l 10 . 07/29/03 OBA2 BET 78-59-1
2-Mathy1naphthalene ED ug/l 10 . 07/29/03 08 :42 BET 91-57-6
2-Methylphenol (o-Cresol)ND ug/l 10 . 07/29/03 08 :42 BET 95-48-7
U41-Metbylphanol ED ug/l 10 . 07/29/03 08 :42 BET
Naphthalene,ED ug/l 10 . 07/29/03 08 :42 EST 91-20-3
2-Nitmamiline ND ug/l 50 . 07/29/03 08 :42 BET 08-74-4
3-Nitromailine RD ug/l 50 . 07/29/03 08A2 BET 99-09-2
4-Mitroaniline ND ug/l 50 . 07/29/03 08 .42 BET 100-01 .6
Nitroberazene ED uq/l 10 . 07/29/03 08 :42 BET 98-95-3
2-Nitrophartol ED ug/l 10 . 07/29/03 08 :42 BET 88-75-5
4-Nitrophencl ED ug/l 50 . 07/29/03 08 ;42 BET 100-02-7
N-Nitronodimthylanine ND ug/l 10 . 07/29/03 08 :42 BET 62-75-9
X-Nitroso-di-n-propylmine ND ug/l 10 . 07/29/03 08 :42 BET 621-64-7
N-Mitrosodiphanylamine,ND ug/l 10 . 07/29/03 08 :42 BET 86-30-6
Pentachlorophenol ED ug/l 50 . 07/29/03 08 :42 BET 87-86-5
Pheranthrene ND UB/I 10 . 07/29/03 08 ;42 BET 85-01-8
Phanol ND ug/l 10 . 07/29/03 0BA2 BET 108-95-2
Pyrezue ED ug/l 10 . 07/29/03 08 :42 BET 129-00-0
1,2,41-Trichlorobenzeas ED ug/l 10 . 07/29/03 08 :42 BET 120-62-1
2 . 4,5 -Trichlorophenel ND ug/l 50 . 07/29/03 08:42 BET 95-95-4
2,4,6-Trichlorophanol ND ug/l 10 . 07/29/03 08 :42 BET 06-06-2
Mitrobenzene-d5 (S) 65 07/29/03 08 :42 BET 4165-60-0
2-Fluorobiphanyl (S) 70 07/29/03 06 :42 BET 321-60-6
Terphanyl-d14 (S) 85 07/29/03 08 :42 BET 1718-51-0
Ph*aol-d5 (8) 10 111 07/29/03 08 :42 BET 4165-62-2
2-Fluoraphmol (S) 13 % 07/29/03 08 :42 BET 367-12-4
2,4,6-Tribromphmol (S) 85 11 07/29/03 08 :42 BET
Date Extracted 07/25/03 07/25/0 3
D,it.: 08/20/01
P 4 t I $
i,bo=m Canifficedion IDS
J .bonuo N
NC Wasts"nor 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water gm
NC Drinking Water 37706 Thus report anal not be reproduced, enept in futi, VA Drinking Water 213
sc 9M wittiout ais wrimen consent of Pam Amatirtica]Servicim, Inc . FL NELAP E87627
Pace AnS411081 Services,1w.
9800 KoW Aventat, Suits 100
HLOI&MIle,AIC 28078calcuemalytical'Phone [phone]
Far 704.875.9091
ac,
Lab Project Number :924779 6
Client Project ID : 03-JUL-0339/MI135 6
Lab Sample No :923172001 Project Sample Number :9247796-003 Date Collected :07/21/03 11 ;35
Client Sample ID : 23024535/PKWM-S Matrix : Water Date Received :07/23/03 11 :50
Parattleters, Results Units Ropgric Limit Analyzed BY CAB No . Qua,RtgLat
GCIKS Semivolatile s
Sessivolatile organics Prep/Method : EPA B27 0
kcenaphthents ND ug/l 10 . 07/29/03 09 :20 BET 83-32-9
acenaphthylens,No USA 10 . 07/29/03 09 :20 BET 208-96-8
Aniline HD ug/l 10, 07/29/03 09 :20 BET 62-53-3
Anthraceas No ug/l 10 . 07/29/03 09 :20 BET 120-12-7
Eastern (a)anthracerre ND ug/l 10 . 07/29/03 09 :20 BET 56-55-3
Benzo(Opyreve No ug/l 10 . 07/29/03 09t20 BET 50-32-8
Banzo (b) f luorantheate ND ug/l 10 . 07/29/03 09 :20 BET 205-99-2
Benzo(g,h,Uperylene No ug/l 10 . 07/29/03 09 :20 BET 191-24-2
BenzoWfluorantheire ND ug/l 10 . 07/29/03 09 :20 BET 207-08-9
Benzoic acid ED ug/l 50 . 07/29/03 09s20 BET 65-85-0
Benzyl alcohol ED ug/l 20 .07/29/03 09 ;20 BET 100-51-6
4-Bromoplarmaylphemyl ether No ug/l 10 . 07/29/03 09 :20 BET 101-55-3
Butylberarsylphthalate ND USA 10 . 07/29/03 09 :20 BET 85-66-7
4-Chloro-3-mthylphanol No ug/l 20 .07/29/03 09 :20 BET 59-50-7
4-Chloroaniline ND ug/l 20 .07/29/03 0900 BET 106-47-8
bia(2-Chloroethoxy)msethane No ug/l 10 . 07/29/03 09 :20 BET 111-91-1
bie(2-Chloroethyl) ether ND ug/l 10 . 07/29/03 09 :20 BET 111-44-4
bis(2-Chloroisopropyl) ether ED ug/l 10, 07/29/03 09 :20 BET 39638-32-9
2-Chlormaphthalme ND ug/l 10 . 07/29/03 09 :20 BET 91-56-7
2-Chlorcrybecaol No ug/l 10 . 07/29/03 09 ;20 BET 95-57-8
4-Chloropheirrylphenyl ether ND ug/l 10 . 07/29/03 09 :20 BET 7005-72-3
Cbryaane ND ug/l 10 . 07/29/03 09 :20 BET 218-01-9
Dibenz(a,h)anthracent,ED Ug/l lo . 07/29/03 09 :20 BET 53-70-3
Dibmzofur=ED Ug/l 10 . 07/29/03 09 :20 BET 132-64-9
1,2-Dichlorobeazene No ug/l 10 . 07/29/03 09 :20 BET 95-50-1
1,3-Dichlorobenzene,ND ug/l 10 . 07/29/03 09 ;20 BET 541-73-1
1,4-Dichlortablenzane ND ug/l 10 . 07/29/03 09 :20 BET 106-46-7
3,3--Dichlorobanzidine ED ug/l 20 .07/29/03 09 :20 BET 91-94-1
2 .4-Dichlorophenol ED ug/l 10 . 07/29/03 09 :20 BET 120-83-2
Diethylphthalate ND ug/l 10 . 07/29/03 09 :20 BET 84-66-2
2,4-Dimthylphenol No ug/l 10 . 07/29/03 09 :20 BET 105-67-9
Dimethylphthalate ND ug/l 10 . 07/29/03 09 :20 BET 131-11-3
Di-n-butylphthalate No ug/l 10 . 07/29/03 09 :20 BET 84-74-2
4 .6-Dinitro-2-methylphertol No ug/l 50 . 07/29/03 09 :20 BET 534-52-1
2,4-Dinitrophenol ND ug/l 50 . 07/29/03 09%20 BET 51-28-5
2,41-Dinitrotoluene,ND ug/l 10 . 07/29/03 09 :20 BET 121-14-2
2,6-Dinitrotoluwe ND ug/l 10 . 07/29/03 09 :20 BET 606-20-2
Date ;00/28/03 Page :5 nf 18
1 appralory ren fical an IIthommary rArfif cation 11)REPORT OF LABORATORY ANALYSIS KY Drinking Water QMK Wastseraft, 1 2
NC Drinking Water 37706 This report shall nol be reprodwed, except in tull . VA DrinVing Water 213
SC gm vathout the written consent of Pace AmlYtV21 Services, Inc Fl.NELAP E87627
Pace AnaNUest Sen1m, Inc .
M MAW AMW,Suilis 100
I
HuMMI/A AC28078mAnalyfical"Agile 7048759092
mm.paoialabs.com Far 704.875.9091
ac,
Lab Project Number ;924779 6
Cutest Project ID :03-JUL-0339/KI135 6
Lab Sample NO ; 923172001 Project Sample Number ;9247796-003 Date Collected :07/21/03 11 :35
Cliect Sample ID : 23024535/PXWN-S Wisteria : Water Date Received :07/23/03 11 :50
Results Unitis RepQrt Limit ---AR41y-z9d---21Y-CAS NO -Quall RWL%t
Di-n-octylphthalate ND ug/1 10 . 07/29/03 09 :20 BET 117-84-0
1,2-Diphenyihydrazine ND ug/l 20 .07/29/03 09 :20 BET 122-66-7
bis(2-Ethylhexyl)phtb,alate ED ug/1 10 . 07/29/03 09 :20 BET 117-81-7
Flucrazathreste ED ug/l 10 . 07/29/03 09 :20 BET 206-44-0
Fluoresce RD ug/1 10 . 07/29/03 09 ;20 BET 86-73-7
Heacachloro-1,21-butadiame ND ug/l 10 . 07/29/03 09 :20 BET 87-68-3
Reafachloroberalizents ED ug/l 10 . 07/29/03 09 :20 BET 118-74-1
Sexachlorocrycloprectadiame ED ug/l 10 . 07/29/03 09 :20 BET 77-47-4
geaciscIalortatithaare ED ug/1 10 . 07/29/03 09 :20 BET 67-72-1
Isideneg (l,2,3-cd)Pyrex%e ED ug/l 10 . 07/29/03 09 :20 BET 193-39-5
lacphorone HD ug/l 10 . 07/29/03 09 :20 EST 78-59-1
2-Methyllausplathatleme ED ug/1 10 . 07/29/03 09 :20 BET 91-57-6
2-Kethylphsool (0-Cresol)ED ug/l 10 . 07/29/03 09 :20 BET 95-48-7
311,4-Metlrylphecol ED ug/l 10 . 07/29/03 09 :20 BET
Hisplathalserse ND ug/l 10 . 07/29/03 09 ;20 BET 91-20-3
2-Nitromiline ED ug/1 50 . 07/29/03 09 :20 EST 88-74-4
3-Mitrosuailine ND ug/l 50 . 07/29/03 09 ;20 BET 99-09-2
4-Nitromiline KID ug/l 50 . 07/29/03 09 :20 BET 100-01-6
Nitrobecizene ND ug/1 10 . 07/29/03 09 :20 BET 98-95-3
2-Mitrophatool ED ug/l 10 . 07/29/03 09 :20 BUT 88-75-5
4-Nitrophrensol ED ug/l 50 . 07/29/03 09 :20 BET 100-02-7
N-NitroinadiessathYlamine ED ug/1 10 . 07/29/03 09 :20 BET 62-75-9
N-Nitroso-di-a-propylmine ND ug/l 10 . 07/29/03 09 :20 BET 621-64-7
N-Nitrosodipherrylamine ND ug/l 10 . 07/29/03 09 :20 BET 86-30-6
Pexatachlorophenol ND ug/l 50 . 07/29/03 09 :20 BET 87-86-5
Pheinfuntlexace ED ug/l 10 . 07/29/03 09 :20 BET 85-01-8
Pheriol ND ug/l 10 . 07/29/03 09 :20 BET 108-95-2
Pyrme ED ug/1 10 . 07/29/03 09 :20 ENT 129-00-0
1,2,41-Trichlorobenziuat,ND ug/l 10 . 07/29/03 09 :20 BET 120-92-1
2,4,5-Trichloraphanol ED ug/l 50 . 07/29/03 09 :20 BET 95-95-4
2,4,6-Trichlorophistrol ND ug/l 10 . 07/29/03 09 :20 BET 08-06-2
Nitrobeausece-,15 (8) 63 Is 07/29/03 09 :20 BET 4165-60-0
2-Pluorobiphresayl (S)64 % 07/29/03 09 :20 BET 321-60-8
Terphwyl-dl4 (S) 92 It 07/29/03 09 :20 BET 1718-51-0
Phencl-d5 (S) 25 is 07/29/03 09 :20 BET 4165-62-2
2-Pluorophristril.(S) 32 15 07/29/03 09 :20 BET 367-12-4
2,4,6-Tribrozophatiol (S) 85 Is 07/29/03 09 :20 BE T
Date Extracted 07/25/03 07/25/03
page : 6 of is
I ahnnalon, Carlification iDS REPORT OF LABORATORY ANALYSIS KY Drinking Water 9DD90NCWastewater 1 2
NC Drinking Water 37706 This report shal; not be reprodmed. axontitin tull, VA Drinking Wale,213
Sc 9M without the written consent ol Pace AmMical SerMls.Inc .Fl.NELAP E87527
Pace AR81YUC81 SetWe", Inc.
9M KinoeyAww, Suite 100Hunferwile,AlC 2807850,.Malyfical Phone [phone]livnew.pacelabs.com Far 704.875.9091
Lab Project Number :924779 6
Client Project ID : 03-JUL-0339/KI1356
PARANETER FOOTNOTE S
1wrgastic Net chemistry Analyses were performed at our Pace Asheville laboratory and Organic and Metals
testing was performed at our Pace Charlotte laboratory unless otherwise footnoted .
ND Not detected at or above adjusted reporting limit
NC Not Calculabl e
J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
NDL Adjusted Method Detection Limi t
(S)Surrogate
Ill The surrogate and/or spike recovery was outside acceptance limits .
(2) The sample could not be re-extracted due to limited sample volume .
Vat.:08/28/03 page :7 of is
l,hVrat,m Certification U
NG Wastenvater 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water g0D90
NG Drinking Water 37706 This report shall not be reprodinced. excePt in full VA Drialong Water 213
SC 9M without the written consent of Pau Anahetical Services, Inc FL NELAP E87627
Pace Anablical Services, Inc.
M Kincey Amul Svils 100
01'se!] Hunimpalk AC 28078Gauce mayical-Phone [phone]~.Psowabs .oourf Far 704.875.9091
QUALITY CONTROL DATA
Lab Project Number :924779 6
Client Project ID :03-JUL-0339/NI1356
QC Batch :78376 Analysis Method ; EPA 827 0
QC Batch Method : Analysis Description : Senivolatile organics
Associated Lab Samples :923171987 923171995 92317200 1
NETEDD BLANK :92318051 7
Associated Lab Samples :923171987 923171995 923172001
Blank Reporting
Parameter VqLtA-Result Limit rootnotop
Acensplathene ug/l ND 10 .
Acersaphthylene ug/l No 10 .
Aniline ug/l ND 10 .
Anthracene ug/l ND 10 .
Below (a) anthraceme,ug/l No 10 .
Beaso (a) Pyrene ug/l BID 10 .
Benzo(b)f luorantheate ug/l ND 10 .
Bau%o(9,h,i)P*rylene ug/l RD 10 .
Benzo (k)Iluoranthesua ug/l ND I'*
Banzoic acid ug/l ND 50 .
Beasyl alcohol ug/l ED 20 .
4-Brcalwophenrylphanyl ether ug/l ED 10 .
Butylbenzylphthalate ug/l BID 10 .
4-Chloro-3-methylpbsuml ug/l No 20 .
4-Chloroaxtiline,ug/l ED 20 .
bio(2-Chloroathozy) methane ug/l ND 10 .
bis(2-Chloroethyl) other ug/l No 10 .
bis(2-Chloroisopropyl) ether ug/l ND 10 .
2-Chloronaphthalene ug/l No 10 .
2-Chlorophenol ug/l ND 10 .
41-Cblorophenylphanyl ether ug/l BID 10 .
Chrymens ug/l ND 10 .
Dibenz(a,h)anthracene ug/l ND 10 .
Dibezzofuran ug/l ED 10 .
1,2-Dichlorobenzelce USA ND 10 .
1 .3-Dichlorobenzme ug/l ND 10 .
1,4-Dichlorobarsene ug/l No 10 .
3,3--Dichlorobenzidine ug/l ND 20 .
2,4-Dichlorophataol ug/l No 10 .
Dietbylphthalate ug/l ND 10 .
2,4-Dimethylphenol ug/l ND 10 .
Date :DG/28/03
1 .ben.tn' randke,nn 1
REPORT OF LABORATORY ANALYSIS KY Drinking Water 9wNCWastewter 1 2
NC Drinking Water 37706 This report shall not be reproduced . except in full, VA Drinking Water 213
SC 99M without the written consent Df Pan Analytical Services .Im FL NELAP E87627
Pug A48101cal SorWen,/Ac.
9800 Kincey Averfue, Suito 100
Hfin0wile,NC 28078VUmalyfical"'Phom 70L(8759092
Far 704.875.9091
C,
QUALITY CONTROL DATA
Lab Project Number :9247796
Client Project ID : 03-JUL-0339/MI1356
HMOD BLUM :92318051 7
Associated Lab Samples :923171987 923171995 923172001
Blank Reporting
Parameter Units Result Limit Footnotes
Dimethylphthalace ug/l RD 10 .
Di-n-butylphthalate ug/l ND 10 .
4,6-Dinitro-2-methylpheasol ug/l ND 50 .
2,4-Dinitrophmol ug/l ND 50 .
2,4-Dinitmtolume ug/l ND 10 .
2,6-Dinitratoluene ug/l ND 10 .
Di-n-octylphthalate ug/l ND 10 .
1,2-Diphmylhydrazine ug/l ND 20 .
bia(2-Sthylhexyl)phthalate ug/l ND 10 .
Fluorskathene ug/l ND 10 .
Pluoreas USA ND 10 .
Hertaichloro-1,31-butaidiene ug/l ND 10 .
Sexachlorobenzesse ug/l ND 10 .
Hescachlorwyclopentadietne ug/l HD 10 .
Haxachloroethane ug/l ND 10 .
Indeno (1, 2,3 - cd)pyrwe ug/l ND 10 .
Isophorone ug/l ND 10 .
2-Hathyltausphthalene ug/l ND 10 .
2-Methylphenol (o-Cresol)ug/l ND 10 .
3fi4-Hathylphanol ug/l ND 10 .
Napiathalene ug/l ND 10 .
2-Nitroaniline ug/l ND 50 .
3-Nitromiline ug/l HD 50 .
4-Hitroaniline ug/l ND 50 .
Hitrobenzene ug/l ND 10 .
2-Nitrophanol ug/l ND 10 .
41-Nitrophanol ug/l ND 50 .
N-Nitrosodimethylamine ug/l NO 10 .
N-Nitroso-di-n-propylazine ug/l ND 10 .
N-Nitrosadiphenylamine ug/l ND 10 .
Pentachlorophenol ug/l ND 50 .
Phananthrens ug/l ND 10 .
Phenol ug/l ND 10 .
Pyrene ug/l ND 10 .
1,2,4 .Trichlorobenzene ug/l ND 10 .
2,4,5-Trichlorophenol uq/1 ND 50 .
Data :08/28/03 Page :9 of 18
1,beuat,rv Candecation Me REPORT OF LABORATORY ANALYSIS KY Drinking Water 9OD90NCWasturvater 1 2
NC Din king Water 37706 This report 511all off be reproduced. except in futl. VA Drinking Water 213
Sc 9M vAthoui the written consent of Pace Analytical Services, IM. FL NELAP E87627
Poce Anslyficol SerWe",Ine.
W lUncey Avelitle,Suds 100
I C
baIxioll.HwWwk NC 28078^0t,t'at
Photm 704 875 9092
Fax.,704.875.9091
QUALITY CONTROL DATA
Lab Project Number :924779 6
Client Project ID :03-JUL-0339/MI1356
xzTEDD BLAME :923180517
Associated Lab Samples ;923171987 923171995 923172001
Blank Reporting
Parameter Units Result Limit Footnotes
2,4,6-Trichlorophenol ug/l ED 10 .
lwitrobanwi,ono-dS (S) %6 4
2-Pluorobiphanyl (S) 111 64
Torphwyl-dl4 (S) %84
Phavol-0 (S) % 16
2-Fluomphwol (S) %21
2,4,6-Tribrosallphozol (8) % 77
LASORATORy CONTROL SAMPLE k LCSD: 923171169 92317117 7
Spike LCS LCSD LCS LCSD
Parameter Units Couc .Result Result %Re Roo M Footnotes
kconaphthers ug/l 50 .00 37 .74 37 .20 76 74 1
Acenaphthylene,ug/l 50 .00 37 .28 37 .32 75 75 0
Aniline ug/l 50 .00 22 .18 29 .07 44 60 30
Anthracene ug/l 50 .00 41 .27 40 .10 82 80 3
Bsnzo (a) anthracsse,ug/l 50 .00 41 .87 40 .90 94 82 2
Basso (a) pyrane ug/1 50 .00 43 .80 42 .79 88 86 3
Benzo (b) f luoranthene ug/l 50 .00 44 .46 42 .86 69 86 4
BUD= (91 h I i) perylene ug/l 50 .00 43 .01 42 .37 B6 85 2
Benzo(k)fluoranthene ug/l 50 .00 41 .41 41 .39 83 83 0
Botanic acid ug/l 50 .00 15 .28 22 .35 31 45 38 1
Bansyl alcohol ug/l 50 .00 29 .24 40 .86 58 82 33 1
41-Bromophenylpheuyl other ug/l 50 .00 39 .11 38 .48 78 77 2
Butylbeazylphthalate ug/l 50 .00 92 .59 109 .4 185 219 17 2,3,2,3
4-Chloro-3-mthylPhOwl ug/l 50 .00 24 .72 42 .34 49 95 53 1
4-Chloroamiline ug/l 50 .00 20.20 30 .09 40 60 39 1
bie,12-Chloroethoxy)methaae USA 50 .00 38 .60 37 .08 77 74 4
bis(2-chloroethyl) other ug/l SO .00 34 .34 34 .57 69 69 1
bis(2-Chloroisopropyl) ether ug/l 50 .00 37 .22 36 .56 74 73 2
2-ChloronaphthalOns ug/l 50 .00 35 .46 35 .09 71 70 1
2-Chlorophemol ug/l 50 .00 21 .33 34 .83 43 70 48 1
4-Chlorophenylphenyl ether ug/l 50 .00 38 .66 38 .52 77 77 0
Chryaene ug/l 50 .00 41 .19 40 .46 82 81 2
Dibonz (a,h)anthracene ug/l 50 .00 44 .11 44 .37 88 89 1
Date :00/28/03 Page : 1D f is
"bontary Cartelicatm IIebOMInN fArIffiCatiOn IDS REPORT OF LABORATORY AKALYSIS KY Drinking Water 900510NCWashwater 1 2
NC Drinking Water 37706 This report shall not be reWodu"d, extept in full . VA Drinking Walef 213
Sc 9M Ynthout the witten Consent 01 Pam Analytical Services Int. FL NELAP E87627
Pope Analyffent Sdritw, Inc .
1
9800 ffincty AKYW, Svits too
a
^61 Hilvai AV 28078UVAnalyfical'"RM 704 875 9092
Fat.704.875.9091
C,
QUALITY CONTROL DATA
Lab Project Number ;924779 6
Client Project ID : 03-JUL-0339/MX1356
LKSOR&TORY CONML SAMLE 5,LCSD : 923171169 92317117 7
Spike LCS LCSD LCS LCSD
Parameter Units Conc,Result Result Roo Rec M Pootnotem
Dibenzofuran.ug/l 50 .00 37 .64 37 .19 75 74 1
1,2-Dicblorobenzene ug/l 50 .00 30 .47 28 .89 61 58 5
1,3-Dichlorobenzene ug/l 50 .00 29 .22 28 .19 58 56 4
1,4-Dichlorobenzens ug/l 50 .00 29 .63 28 .19 60 56 6
3,3--Dichlorobenzidine,ug/l 100 .00 41 .14 41 .62 41 42 1
2,4-Dichlorophano 1 ug/l 50 .00 24 .76 37 .97 so 76 42 1
DiethylphthalatO ug/l 50 .00 35 .86 35 .09 72 70 2
2,4-Dimet1sylplantool ug/l 50 .00 24.20 38 .19 48 76 45 1
Dimthylphthalate ug/l 50 .00 23 .33 23 .94 47 48 3
Di-a-butylphthalate ug/l 50 .00 41 .09 39 .66 82 79 4
41,6-Dinitro-2-methylpher,ol ug/l 50 .00 41 .65 45 .36 03 91 9
2,41-Dinitropheluol ug/1 50 .00 34 .81 49 .86 70 100 36 1
2,41-Dinitrotoluene ug/l 50 .00 44 .35 43 .69 89 87 1
2,6-Dinitrotoluene ug/l 50 .00 43 .41 43 .03 87 86 1
0 Di,n-ootylphthalate ug/l 11,00 17*81 47,16 91 15 1
1,3-Diphenylhydrasiae ug/l 50 .00 35 .15 34 .56 70 69 2
bia(2-Ethylhexyl)phthalate ug/l 50 .00 47 .10 46 .53 94 93 1
Fluoranthene ug/l 50 .00 39 .03 38 .98 so 78 2
Pluarene ug/l 50 .00 39 .63 38 .90 79 78 2
Hatfuschloro-1,31-butadiener ug/l 50 .00 28 .82 28 .07 58 56 3
Recaachlorobenzeue ug/l 50 .00 38 .29 37 .68 77 75 2
Hexachlorocyclopentadiene ug/l 50 .00 23 .39 24 .67 47 49 5
Hexachlorcrethaxle uff/l 50 .00 29 .96 211 .59 60 57 5
Indeno(l .2,3-cd)pyrene uq/l 50 .00 43 .69 43 .77 87 88 0
Isophorone ug/l 50 .00 42 .38 41 .51 85 83 2
2-Methy1naphthalene ug/l 50 .00 34 .91 34 .05 70 6B 2
2-Nethylphenol (o-Cresol)ug/l 50 .00 20 .11 33 .42 40 67 50 1
UA-Methylphenol ug/l 50 .00 19 .26 32 .72 38 65 52 1
Naphthalene ug/l 50 .00 33 .71 32 .30 67 65 4
2-Nitromiline ug/l 50 .00 37 .50 37 .96 75 76 1
3-Nitroaniline ug/l 50 .00 31 .60 34 .57 63 69 9
4-Nitro=iline ug/l 50 .00 28 .96 35 .15 58 70 19
Hitrobenzene ug/l 50 .00 36 .30 35 .20 73 70 3
2-Nitrophenol uq/l 50 .00 32 .10 39 .97 64 80 22
4-Nitrophenol ug/l 50 .00 13 .70 20 .22 27 40 38 1
N-Nitrooodimethyl=ine ug/l 50 .00 14 .88 18 .76 30 38 23
N-Nitrooo-di-a-propylamine ug/l 50 .00 41 .01 40 .27 82 80 2
Date ; Oe/28/03 Page ; 11 of to
i awrataN CmMustin lDsIaboralam Cefoloatlan lps REPORT OF UBORATORY ANALYSIS KY Drinking Water 9DO90NCWaSUWW 1 2
NCD ",king WaWr 37706 This report suall not be reprolltud, tntoePt in full . VA Durdung Water 213
Sc 99OD6 without awl witten consent of Pau AwtiOtIl SerAces .IM FIL NELAP E87627
Me Amlyflogit Serfr(cm,toe.MKirxWAmm Suite 100
HuntifMile.A(C 2807872neAnalytical'Johme.,704.875.9092
Fax.[phone]
QUALITY CONTROL DATA
Lab Project Number :924779 6
Client Project ID : 03-JUL-0339/MI1356
LABORATORY CONTROL SAMPLE LCSD : 923171169 92317117 7
Spike LCS LCSD LCS LCSD
Personator MaLts Conc .Result Result I Rao Rec RPD Footnotes
N-Niteemsodiphatrylamine Ug/l 50 .00 38 .29 37.12 77 74 3
Pentachlorophanxtl Ug/l 50 .00 39 .07 40 .47 78 Ill 4
Ph~thrme Ug/l 50 .00 39 .10 38 .34 78 77 2
Phemol ug/l 50 .00 12 .24 16 .90 24 34 32 1
Pyrme ug/l 50 .00 40 .63 39 .69 81 79 2
1,2,4-Trichlorobelizene Ug/l 50 .00 30 .61 29 .60 62 59 4
2,4,5-Trichloropharmol ug/l 50 .00 31 .04 42 .19 62 84 30
2,4,6-Trichlorophmol Ug/l 50 .00 33 .25 41 .66 66 83 22
Nitrobskozemia-d5 (S) 76 75
2-Pluorobiphanyl (S)74 74
Torphmyl-dl4 (S)84 83
phsiamol-tI5 (8)24 34
2-Fluorophamol (S)28 44
2,4,6-Tribrossopharml (S) 09 93
LABORATORY CONTROL SA14PLE :923180525
Spike LCS LCS
Parameter units Conc . Result Rao Footnotes
A ...Phth,c,Ug/l 50 .00 35 .86 72
Acerousplithylenis ug/l 50 .00 35 .53 71
Aniline Ug/l 50 .00 32 .43 65
Anthracene ug/l 50 .00 39 .89 s o
Benzo (a) asathraceme Ug/l 50 .00 39 .12 78
Bansio(a)pyrene ug/l 50 .00 42 .54 B5
B=Zo (b) f luormthene ug/l 50 .00 45 .25 90
Berilic (9,h, i) perylene Ug/l 50 .00 34 .35 69
BanzoMfluoranthere Ug/l 50 .00 39 .35 79
Romanic acid Ug/l 50 .00 10 .31 21
beroxyl alcohol Ug/1 50 .00 32 .60 65
4-8r=phmylphmyl ether Ug/l 50 .00 41 .60 83
leutylbeassylphthalate ug/l 50 .00 74 .08 148 2
4 -Chloro-3 -mmathylphanol Ug/l 50 .00 33 .09 66
4-Chloro=iliue Ug/1 50 .00 34 .44 69
bia(2-Chloroethoxy)methaaue ug/l 50 .00 33 .67 67
bis(2-ChlorGethyl) other ug/l 50 .00 32 .75 6 6
D .t .i 00/28/03 yage :12 of 18
I aboran, rantlicatkin I DIshoratiori Cartiffikat on REPORT OF LABORATORY ANALYSIS KY Drinking Water 9DO90NCWastewater 12
NC Drinking Water 37706 This report shall nor be reproduced, except in full, VA Drinking Water 213
SC 99006 without the written consent of Pace kialyfisal Services, Im Fl.NELAP E87627
Pico Anslyflegil Serolces Inc
9&V Know Awfue, Suite 100
Huffterwile.NC 28078MalXical-PhOIV'7&.875.9092/7;alce mm.pacelabs .conrh Far 704.875.9091
QUALITY CONTROL DATA
Lab Project Number :924779 6
Client Project ID :03-JUL-0339/MI1356
LABORATORY CONTROL SAMPLE : 923180525
Spike LCS LCS
Paranoter Units Conc,Result III Reg Footnotes;
bio(2-Chloroisopropyl) other uq/l 50 .00 32 .56 65
2-Chloronaphthalene ug/l 50 .00 33 .04 66
2-Chlorot,111610,01 ug/l 50 .00 27 .82 56
4-Cblorophonylphenyl ether ug/l 50 .00 40 .14 s o
Chryissaus ug/l 50 .00 40 .62 81
IDibGoz (a,h)SethraCmll ug/l 50 .00 3537 71
Dibmzofur=ug/l 50 .00 36 .40 73
1,2-Dichlorobenzesse uq/1 50 .00 31 .11 62
1,31-Dichlorobenzene ug/l 50 .00 29 .98 60
1,41-DichlorobSELZM411 ug/l 50 .00 29 .76 60
3,31--Dichloroboazidine ug/l 100 .00 50 .02 50
2,4-DiChlorophollol ug/l SO .00 32 .09 64
Diethylphthalate ug/l 50 .00 37 .34 75
2,4-Disisethylphosawl ug/l 50 .00 29 .95 60
Dithylphthlate g/l 51,00 21*18 53
Di-n-butylphthalate uq/l $0 .00 39 .56 79
4, G-Dinitro-2-meathylpheriol ug/l 50 .00 48 .22 96
2,41-Dinitrophenol ug/l 50 .00 38 .05 76
2,4-Dinitrotolume ug/l 50 .00 43 .01 86
2,11-Dinitrotoluene ug/l 50 .00 39 .07 78
Di-n-octylphthalate ug/l 50 .00 41 .74 84
1,2-Diphenylhydrazine ug/1 50 .00 27 .84 56
bia(2-Ethylhoxyl)phthalate ug/l 50 .00 41 .15 82
Fluoranthene ug/l 50 .00 41 .74 84
Pluorene ug/1 50 .00 39 .36 79
Nexachloro-1,21-butadiene,ug/l 50 .00 31 .21 62
Reacischlortabonzene ug/l 50 .00 40 .34 81
Hexachlorocyclopantadiene ug/l 50 .00 22 .33 45
Hexachloroothane ug/1 50 .00 29 .08 58
Indeno (1,2, 3-cd) pyrene ug/1 50 .00 34 .99 70
loophorone ug/l 50 .00 36 .05 72
2-Nothyluaphthalene ug/l 50 .00 31 .89 64
2-Methylphenol (o-Cresol)ug/l 50 .00 26 .20 52
U11-Mothylphenol ug/l 50 .00 23 .90 48
Naphthalene ug/1 50 .00 33 .16 66
2-Nitroaniline ug/l 50 .00 34 .39 69
3-Nitroamiline ug/l 50 .00 36 .09 7 2
Date~08/28/03 page~13 of to
1,honflar,Cenflical,00 IDS REPORT OF LABORATORY ANALYSIS KY Drinking Water 9OD90NCWastirever 1 2
NC Drinking Water 37706 This nmort shelf not be reproduced, excePt in full, VA Driniring; Watef 213
SC 9M whhwt Via wittain consent of Im Anat0oll Servicls .In Ff.NELAP E87627
Page Anslylivol Servi Inc.
M Kirm Awhae.Suits 100
I
Hishlowlie,AC28078ceAnaVical'e Phorie.,704.875.9W~.Paceilabs .corrf Far 704.875.9091
C,
QUALITY CONTROL DATA
Lab Project Number :924779 6
Client Project ID : 03-JUL-0339/KI1356
LABORATORY CONTROL SAMPLE :923180525
Spike ICE LCS
Parameter Units Cone,Result %Rec Footnotes
4-Nitrosadline ug/I 50 .00 40 .21 so
Nitrobesousene ug/l 50 .00 34 .92 70
2-Mitrophainol ug/l 50 .00 32 .67 65
4-Nitrophencl ug/l 50 .00 20 .07 40
N-Mitrooodimthylamine ug/l 50 .00 23 .41 47
X-mitrooo-di-n-propylamine ug/I 50 .00 35 .26 70
N-NitrooodiPh"Yl--i-O ug/l 50 .00 38 .43 77
Pentachlorophenol ug/I 50 .00 39 .14 78
Phexaminthrencle u0/1 50 .00 40 .15 s o
Phenol ug/l 50 .00 13 .82 28
Pyrene ug/l 50 .00 41 .55 03
1,2,4-Trichlorobenzerrue ug/l 50 .00 30 .97 62
2,4,5-Trichlorophenol ug/l 50 .00 36 .47 77
2,4,6-Trichlorophaxiol ug/l 50 .00 37 .02 74
Mitrobenzati (S) 70
2-Fluorobiphanyl (S) 68
Torpbmyl-dl4 (8) 87
Phervol-0 (8) 29
2-Fluoropheavol (S) 38
2,4,45-Tribromophenol (S) 89
MATRIX SPIKE &MATRIX SPIKE DUPLICATE :923171185 92317119 3
923152805 Spike ME MSD ME NE D
Units Result Conc, Relsult Result Iii-Alic %JIiiQ RU P00=06
Acenaphthene ug/l 0 100 .00 73 .40 79 .82 73 80 6
4-Chlorri-3-methylphewl uq/I 0 100 .00 70 .76 75 .74 71 76 7
2-Chlorophenol ug/l 0 100 .00 64 .12 63 .35 64 63 1
1,41-Dichlorobenzene ug/l 1 .001 100 .00 60 .36 60 .58 59 60 0
2,4-Dinitrotoluene ug/l 0 100 .00 86 .10 96 .37 86 96 11
4-Nitrophenol ug/l 0 100 .00 41 .91 42 .25 42 42 1
N-Nitroso-di-n-propylmine ug/l 0 100 .00 79 .00 83 .19 79 83 5
Pentacb1orophentol ug/I 0 100 .00 62 .73 71 .68 63 72 1 3
Phenol ug/I 0 100 .00 29 .85 28 .87 30 29 3
Pyrecie ug/l 0 100 .00 79 .09 87 .81 79 Be 10
1,2,4-Trichlorobenzene ug/l 0 100 .00 59 .09 61 .22 59 61 4
Date ; 011/28103 page :14 of is
lateral," canificalion IIhnriCatiffcallunIDSREPORT OF LABORATORY ANALYSIS KY Drinking Water smNCWastewater 12 Water 213NCDrinking Water 37706 This report shelf nol be reproduced, except in full.VA Drinitin g
Sc 990:16 wthment the wrinen comment of PaU AMMICal SeMCH . IM FL NELAR E07627
Place Anflyfical Sertinfew, Inc.
9800 Kincey Amu,Suite 100
a
GbceAnalXical"HuffIerwile,NC 28078
C,
Phone 704875S092wwwPacelabs.com Far 704.875.9091
QUALITY CONTROL DATA
Lab Project Number :9247796
Client Project ID : 03-JUL-0339/NI1356
MATRIX SPIKE &MATRIX SPIKE DUPLICATE : 923171185 92317119 3
923152805 Spike ME Moo ME KSD
Parameter Units Result Cqnc .Reoult Result Rec Rec RD Footnotes
Nitrobenterene-,15 (S)74 79
2-Fluorobiphanyl (S) 71 7 6
Torphmyl-dl4 (S) 70 73
Phev*l-d5 (S) 32 31
2-Fluorophenol.(S)42 38
2,4,6-Tribromorphatagl (S) 78 90
SAMPLE DUPLICATE :923173918
923152839 DUP
Parameter Units -921alt-Refult RM Footnotes
Acanaplathative ug/l No ND NC
kcamaphthylexie,ug/l No No KC
Aniline ug/l ND No NC
Anthraceze ug/l No No NC
Seraito (a) anthracema ug/l No ND NC
Beizzo(a)pyrene ug/l No No NC
Senwo (b) fluoramthene Uq/l ND ND NC
B=zo(g,h,i)Perylenq ug/l No ND NC
Beazo (k) fluor=th=e ug/l HD ND N C
Benzoic acid Ug/l No ND KC
Bmzyl alcohol Uq/l ED No NC
4-11romophanylphemyl ether ug/l No No NC
Butylbenzylphthalate ug/l No No VC
4-Chloro-3-methylphenol ug/l No No NC
4-Chloroaniline ug/l No No NC
bi8(2-Chloroethoxy)methaue ug/l No No NC
bis(2-chloroethyl) ether ug/l ND No KC
bio(2-Chloroisopropyl) ether ug/l No No NC
2-Chloronaphthalone ug/l ND HD KC
2-Chlorophenol ug/l No ND NC
4-Chlorophenylphenyl ether ug/l No ND KC
Chryaeae ug/l No ND NC
Dibenz (a, h) anthracene Utf/l No ND NC
Dibenzofuran ug/l No ND NC
1,2-Dichlorobenmene ug/l No No NC
Dato~08/20/03 Pago ; 15 Of 18
1 atioratom Carfification lDs 1,baraton, Cetfifa:abon lDs
NC Wastworater 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
NC Drinking Water 37706 Tinis repoif shall not U reproduced, excePt in full,VA Drinking Water 213
SC 99006 ,ghw the witten consent of Pam Analyfia Sewes.Im Fl.NELAP E87627
Pew Anolyticol Swwca,Inc.
9W Kincey Avenue, Suite 100
Hw&W11A A(C 28078ZeAnalydcaf~Phone [phone]
wim.pacelabs .cant, Fax.[phone]
QUALITY CONTROL DATA
Lab Project Number :924779 6
Clierot Project ID :03-JUL-0339/MX1356
SAMPLE DUPLICATEz 923173916
923152839 Dup
P"amatter Units Result Result RPD Pootnotell
1,21-Dichlorobenzene ug/1 RD ND Mc
1,4 -Dichlorobenzene ug/1 ND No NC
3,31-Dichlorobanxidine ug/1 No No NC
2,4-Dichlorophenol ug/1 ED ND Mc
Diethylphthalate uq/1 No ND NC
2,4-Dimethylpheamol ug/1 ND ND NC
Dimethylphthalate ug/1 ND No NC
Di-n-butylphthalate ug/1 ED No KC
4,6-Dinitm-2-mathylphenol ug/1 No ND Kc
2,41-Dinitmphenol Ug/1 No ND Kc
2,4-Dinitrotoluene uq/1 ND ND NC
2,6-Dinitrotoluene ug/1 No No NC
Di-m-octylphthalate ug/1 NO No KC
1,2-Diphenylhydrazine ugli No ND KC
bie(2-My1hexy1)phtha1ate USA ED No NC
Plutorauxthene,ug/1 No No MC
Pluoreze ug/1 No No KC
Hexachloro-1,3-butaldiene USA No ND Kc
Heauschlorobezuesexte ug/1 ED No NC
Hattachlorocyclopentadiene,ug/1 ND ND NC
Sintachloroethane ug/1 No ND NC
1ndeno(1,2,3-cd)pyrer*ug/1 ND NZ)NC
lacphorone,ug/1 No ND NC
2-Mathylnaphthal=e ug/1 ND ND HC
2-Mathylphemol (o-Cresol)ug/1 No ND NC
U41-Methylphanol ug/1 No ND KC
Naphthalene ug/1 No No NC
2-Nitromiline ug/1 No ND NC
3-Nitroaniline ug/1 No ND NC
41-Nitroaziline ug/1 No No NC
Nitrobeezene ug/1 ND ND KC
2-Nitrophenol ug/1 ND No HC
4-Nitrophenol ug/1 ND No NC
N-Nitrosodimethylmine ug/1 No No NC
N-Nitroso-di-n-propylamine ug/1 No ND NC
N-Nitrooodiphonylamine ug/1 No ND KC
Pentachlorophanol ug/1 ED No NC
Date!08/20/03 Pact,16 f 18
langraloN Cadflimllan IDSREPORT OF LABORATORY ANALYSIS KY Druflong Water 9MNGWastewater 1 2NCOMking Water 37706 This relport shall not be reproduceti . except in full VA Dunking Water 213
SC 99M wthout the weten consent of Paw Arlatykal SelVic",111C FL NELAP E87627
Pogo Aa#IWCRI Services, 170.
rincey A vanK Sual;100
HunWidlit NC 280789acemalytical"Phom 704 875 9092minuplioelabs.oom Far 704.875.9091
QUALITY CONTROL DATA
Lab Project Number :9247796
Clieut Project ID ; 03-JUL-0339/MI1356
SAMPLE DUPLICANS :923173918
923152839 DUP
Parameter Units Result Result M Footnotes
Phententhrelple ug/1 ND ND KC
Phenol ug/1 ND ND NC
Pyrelle ug/1 ED ND KC
1,2,4-Trichlorobenzene ug/1 ED ND KC
2,4,5-Trichlorophaeol ug/1 ND ND KC
2,4,6-Trichlorophelux,01 ug/1 ND No Mc
Mitmbenzene-dS iS) 62 5 8
2-Pluorobiplawyl (S) 55 53
Terpheoy1-d14 (8) 81 75
Phemsol-0 4S) 11 19
2-Fluoropheaval (8) 13 26
2,4,6-Tribrostophemol (S) %40 7 8
Date~08/28/03 Peg*: 17 of 10
1,barat,N Gedrficatrun IllsahAMANnerthication Ds REPORT OF LABORATORY ANALYSIS KY Drinking Water 90WNCWastemew 1 2
NC Drinking Wale(37706 This report shall w w replodutj . except in full . VA Drinking Water 213
SC 99DO6 Without the wrillan consent of Pace Analldical Semites . Im Fl .NELAP E87627
Pave Ans4liciff Services,Inc.
M kinctey Avenue, Suits 100
Hunterswile,AC 28078aceAnalyfical"Phone [phone]
wiinm.Pa0e1abS.C0ft1 Fax.'704.875.9091
Lab Project Number :924779 6
client Project ID :03-JUL-0339/KI1356
QUALITY CONTROL DATA PARAMETER FOOTNOTE S
Consistent with EPA guidelines, urrounded concentrations are displayed and have been used to calculate %Rec and RPD values .
LCS (D)Laboratory Control Sample (Duplicate )
MS(D)Matrix Spike (Duplicate)
DUP Sample Duplicat e
ND Not detected at or above adjusted reporting limit
KC Not Calculabl e
J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
KDL Adjusted Method Detection Limi t
RPD Relative Percent Difference
(S)Surrogat e
Ill RPD value was outside control limits, however both percent recoveries were acceptable . Sample results for the
QC batch were accepted based on percent recoveries and completeness of QC data .
E21 Recovery falls outside of QC limits, however, this compound is not found in the associated samples .
[3)Analyte in f ound in the associated blank an well an in the sample (CLP B-Flag).
D&te :08/28/03 Part .: to f I$
5 12boraunm Cert fkat no IDSI~hgratfhni Certification ID REPORT OF LABORATORY ANALYSIS KY Drinking Water 9DO90NCWastewater 12
NC Drinking Water 377D6 This report shall not be reproduced, encept in full .VA Drinting Water 213
SC 99006 without the written consent of Pace linalytical Semcen .Inc Fl.NELAP E87627
CHAIN OF CUSTODY RECORDIND ANALYSIS REQUEST FORM
Ana lic ratory Services im,i~yC .d :=oDuke*--'*-*-* -------LIMS I I....... ...a SO 9PageA2(Building 7405)O f
I DISTRIBUTION(T .4PahwEnergy..13339 Hagrs Ferry Rd i Erom
For Detailed Instructions, see : Hunte ra~il
;.,,
N . C . 28078 'ti. ORIGINAL to LAB,
http :11de~Iessenv/cocI 75-5245 COPY to CLIENT
-------------Fa.x :.(7
I)Prolect Name 2)Phone No :875-5257
BURLINGTON MGP (OVERBURDEN WELLS)
E 3)CIlent C .Campbell R . Roberts 4)Fax No :875-5032
2=H 0. 3=H
5)B ..Ine,sUnIt : 20018 6)Process : 7)ResoTo :0193 C
E 08)Project ID:MGPBURL 9)Activlty to : ALLACTV I O)Mail Code:M-GO3A3
Customer to c mniete :=,,Q)aporoorlateNoN-sHADED are E
-----------14 01 01 u,LASUSEONLY "Chem Collection Information CS C13<.P 0"Lob to I ueSKIOP NO .Sample Description or ID Date Time Signature z 2 w w
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QCSAMPLE(WEL P-IS)x n/a IE
Customer to sign &date below11)Kell R 12Requested Turnaround
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t 14 Days0 M 0Relinquishedby: ~m CDate/Time ::::-I Uay s
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$21111010 'Othe r
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0 0 c?1`7 7qCHAINOFCUSTODYRECORDAND ANALYSIS REQUEST FOR M
~W~I-Y'Jc-ai L~~i;~ratory Services iI ---------------------Duke I LIM "Page -L of1 9 goMail Cod G IA2 (Building 7405)
DISTRIBUTIO NIDEnergy.1 3033M ho rs Ferry Rd
to ORIGINAL to LAB,Huntersville,N . C . 28075
to CLIENTFor Detailed Instructions, see : (704) 875-524 5httpl/de~/essenvlcoc/
-------------Fax :.i279L4)-§L5-.t1R!~............
I)N.j .ct N~rre 2)Phone No :87!5~5257
BURLINGTON MGP (SAFROLITZ WELLS)
E 3)cllent C.Campbell R . Roberts 4)Fax No:875 .5032
04 3=H
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21)Re n u1shed 8 OatefThno A"'B7 "Requested Turnaround
14 Days %/qu by : v -/I r; w 0/TImRelLn ~she~'---(X-t 1/6 1.), I-EDate e
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23)!Received by: E Mw VO0 48 H,at 'Tim U I >,V
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CHAIN OF CUSTODY RECORD AND ANALYSIS REQUEST FOR M
Analytical Laboratory Service s=1L Duke ---------------------- * -------------------51411 SA "Page o fMail Code MG03A2 (Building 7405)lums a s
13339 Hagers Ferry Rd i DISTRIBUTIO NFVVEnergy-Huntersville,N. C . 28078 Er ORIGINAL to LAB,
For Detailed Instructions, see :
hUo/1dew~ww/essenvIcoc/ [phone] COPY to CLIENT
Q k .............-------------Fax :. 7PL4j2L5-AR:L
I)P,oi .ct N .roe 2)Phone No :875-5257
BURLINGTON MGP SHAL FRACT BR WELLS)
L8131PH
E 3)CIlent C .Campbell R . Roberts 4)Fax No :875-5032 .:I= C
3=H
SIB ..ine.s Unit : 20018 6)Process : 7)A ..p .T.: 0193
08)Project]D : MGPBURL 9)ActlMty ID: ALLACTV 10)Mall Code :MG03A3
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appropriate NON
r -------- *,-,*---1 014CO1211 J3Chem llection Information E <LA13USEONLY
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"Lob ID I ueSKIOP NO ."Sample Description or ID 0 0 UUDate Time Signature c: z 2 U.] U.1
c2i3o DMW-1 x 1 1 3 1
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Date/Tune:
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Pace Analytical Services,Inc.
9800 Kincey Averfaill, Smile 100
Hunwone,NC 28078acemalyticarPhone7048759092
w,,Avpaf:elabs .Wm Fu.704.875.9091
August 26,200 3
Mr .Jay Perkins
Duke Power
13339 Sellers Perry Road
XG3Qk2
Hunteraville,NC 2807 0
RE : Lab Project Number :924096 7
Client Project To :03-JUL-0339/11CI1356
Dear Xr, Perkins :
Inclosed are the analytical results for sample(s) received by the laboratory on August 13, 2003 .Results
reported herein conform to the most current ~C standards,where applicable,unless otherwise narrated in the
body of the report .
If you have my questions concerning this report please feel free to contact me .
Sincerely ,
Kristi Tart
Kristi .Tartilipacelabs .cook
Project manager
enclosures
L,thor .toN Carub,210-105 I ationitarv Cgrfibution Dr;
NC Warnewate, 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
NC Dtinbrill Water 37706 This repon shall not be reproduced . excepi in full,VA Drinking Water 213
SC 99DOG Oout the dden consent of Pace Analltical Sentices . Mr . Fl .NELAP E87627
Pace malyrical Sefwm . Inc.
M Kincey Milli Suite 100
Hunfelsville,NC 28078~ZeAnaljdical"Phone.,704.875.9092
wwpacelabs.corn Fax.[phone]
Lab Project Number :9248967
Client Project ID :03-JUL-0339/MI135 6
Lab Sample No : 923239214 Project Sample Number :9248967-001 Date Collected :07/25/03 08 :05
Client Sample ID :23024529/MW-3 Matrix : Water Date Received :08/13/03 12 :05
Parameters Results units Report Limi AnalyAgd By CAS No . Qual ReqLm t
GCIKS Sestivolatile s
Sennivolatile Organics Prep[Method :EPA 827 0
Aceraphthene ND ug/l 10 . 08/20/03 20 :24 BET 83-32-9
Acepaplathylare ED Ug/l 10 . 08/20/03 20 :24 BET 200-96-8
Aniline No Ug/l 10 . 08/20/03 20 :24 BET 62-53-3
Anthracens ND USA 10 . 08/20/03 20 :24 BET 120-12-7
Benzo (a) anthracene No ug/l 10 . 08/20/03 20 :24 BET 56-55-3
Berxo(a)pyrene No Ug/l 10 . 08/20/03 20 :24 BET 50-32-8
Beaten (b) IFluctranthene No USA 10 . 08/20/03 20 :24 BET 205-99-2
Benzo (9,h, i) parylene ND Ug/l 10 . 08/20/03 20 :24 BET 191-24-2
Berazo (k) f lunrantherie No ug/l 10 . 08/20/03 20 :24 BET 207-08-9
Bimazoic acid ND ug/1 50 . 08/20/03 20 :24 BET 65-85-0
Begasyl alcohol No USA 20 .08/20/03 20 :24 BET 100-51-6
4-Bromaphertylphenyl ether KID USA 10 . 08/20/03 20 :24 BET 101-55-3
Butylbanxylphthalate No Ug/l 10 . 08/20/03 20 :24 BET B5-68-7
4-Chloro-3-methylphanol No ug/l 20 .08/20/03 20 :24 BET 59-50-7
4-Chloro"iline No USA 20 .08/20/03 20 :24 BET 106-47-8
bis(2-Chloroethoxy)methane No Ug/l 10 . 08/20/03 20 :24 BET 111-91-1
bis(2-CbloroathYl) ether ND Ug/l 10 . 08/20/03 20 :24 BET 111-44-4
bis(2-Chloroisopropyl) ether No Ug/1 10 . 08/20/03 20 :24 BET 39638-32-9
2-Chloronaphthalene No ug/l 10 . 08/20/03 20 :24 BET 91-58-7
2-Chlorophenol No ug/l 10 . 08/20/03 20 :24 BET 95-57-8
4-Chlorophatrylphenyl ether No USA 10 . 08/20/03 20 :24 BET 7005-72-3
Chrysene RD Ug/l 10 . 08/20/03 20 :24 BET 218-01-9
Dibenz (a, h) amthracene ND USA 10 . 08/20/03 20 :24 BET 53-70-3
Dibertzolturan No USA 10 . 08/20/03 20 :24 BET 132-64-9
1,2-Dichlorrobenzene No ug/1 10 . 08/20/03 20 :24 BET 95-50-1
1,3-Dichlorolpenzene No Ug/l 10 . 08/20/03 20 :24 BET 541-73-1
1,4-Dichlorobenzere No Ug/l 10 . 08/20/03 20 :24 BET 106-46-7
3,3--Dichlorobenzidine ND Ug/l 20 .08/20/03 20 :24 BET 91-94-1
2 .4-Dichlorophenol No ug/l 10 . 08/20/03 20 :24 BET 120-83-2
Diethylphthalate No Ug/l 10 . 08/20/03 20 :24 BET 84-66-2
2,4-Dimethylphenol ND ug/l 10 . 08/20/03 20 :24 BET 105-67-9
Dimethylphthalate No Ug/l 10 . 08/20/03 20 :24 BET 131-11-3
Di-n-butylphthalate ND Ug/l 10 . 08/20/03 20 :24 BET 84-74-2
4,6-Dinitro-2-methylphenol ND Ug/l so . 08/20/03 20 :24 BET 534-52-1
2,4-Dinitrophenol No ug/l 50 . 08/20/03 20 :24 BET 51-28-5
2,4-Dinitrotoluene ND ug/l 10 . 08/20/03 20 :24 BET 121-14-2
2,6-Dinitrotoluene No ug/l 10 . 08/20/03 20 :24 BET 606-20-2
Date :08/26/03 Page ;1 of 19
I aboratow COMO]=0 REPORT OF LABORATORY ANALYSIS KY Drinking Wale,9 MNCWaStereater12
NC Drinking Water 37706 This report shall nut be recioduceo except in lull .VA Drinking Water 213
sc 99DD6 without the written consent of Pace kuthytical Services .Inc .FL NELAP E87627
Pace Analytical Swinfees. Inc.
.98M KhIM AwnK Suite 100
Hunfaiskolle,NC 28078aceAnalXicalPhone-704.875.M
wvAypaoelabs.cons Fax.704875.X91
Lab Project Number :924896 7
Client Project ID :03-JUL_0339/MI135 6
Lab Sample No : 923239214 Project Sample Number :9240967-001 Date Collected :07/25/03 08 :05
Client Sample ID :23024529/KW-3 Matrix : Water Date Received :08/13/03 12 :05
parameters Results Units Repqrt Limi ___AnalyaedB CAB No . Dual Reglant
Di-n-octylphthalate ND ug/l 10 . 08/20/03 20 ;24 BET 117-114-0
1,2-Diph=ylhydrazine ND Ug/l 20 .08/20/03 20 :24 BET 122-66-7
bis(2-Ethylhexyl)phthalate ND ug/1 10 . 08/20/03 20 :24 BET 117-81-7
Pluoranthens ND ug/l 10 . 09/20/03 20z24 BET 206-44-0
Fluoragge KID ug/l 10 . 08120/03 20 :24 BET 86-73-7
B"achloro-1, 3-butadieme KID ug/l 10 . 08/20/03 20 :24 BET 87-68-3
Hexachlorobertzene ND ug/1 10 . 08/20/03 20 :24 BET 118-74-1
Hexachlorocyclopentadiene KID ug/l 10 . 08/20/03 20 :24 BET 77-47-4
Hexacloloroethane KID Ug/l 10 . 08/20/03 20 :24 BET 67-72-1
1ndeno(l,2,3-cd)pyrane KID ug/l 10 . 08/20/03 20 :24 BET 193-39-5
Isophorone ND ug/l 10 . 08/20/03 20 :24 BET 78-59-1
2-Methylouiplathaleme KID ug/l 10 . 08/20/03 20 :24 BET 91-57-6
2-Methylphwol (0-Cresol)No USA 10 . 08/20/03 20 :24 BET 95-48-7
3&4-Methylphenol ND ug/l 10 . 08/20/03 20 :24 BET
Naphthalene ND ug/l 10 . 08/20/03 20 :24 BET 91-20-3
2-Nitroaniliro ND Ug/l 50 . 08/20/03 20 :24 BET 80-74-4
3-Nitromiline No ug/l 50 . 08/20/03 20 :24 BET 99-09-2
4-Nitroaniline ND ug/l 50 . 08/20/03 20 :24 BET 100-01-6
Nitrobenzene ND ug/l 10 . 08/20/03 20:24 BET 98-95-3
2-Nitrophenol KID ug/l 10 . 00/20/03 20:24 BET 88-75-5
4-Nitrophenol ND ug/l 50, 08/20/03 20 :24 BET 100-02-7
N-Nitrooodimethylanine ND ug/l 10 . 08/20/03 20:24 BET 62-75-9
N-Nitrono-di-a-propylaMine No ug/l 10 . 08/20/03 20 :24 BET 621-64-7
N-Nitrooodiphonylassine KID ug/l 10 . 08/20/03 20 :24 BET 86-30-6
Pentachloropherol ND ug/l 50, 08/20/03 20 :24 BET 87-86-5
Pherianthrene ND ug/1 10 . 08/20/03 20 :24 BET 85-01-8
Phenol ND ug/l 10 . 08/20/03 20 :24 BET IOB-95-2
Pyreate KID ug/l 10 . 08/20/03 20 :24 BET 129-00-0
1,2,4-Trichlorobenzene ND Ug/l 10 . 08/20/03 20 :24 BET 120-82-1
2,4,5-Trichlorophenol ND ug/1 50 . 08/20/03 20 :24 BET 95-95-4
2,41,6-Trichloropheriol ND ug/l 10 . 08/20/03 20 :24 BET 88-06-2
Hitrobenzene-d5 (S) 57 % 08/20/03 20 :24 BET 4165-60-0
2-Fluorobipbenyl (S) 59 % 08/20/03 20 :24 BET 321-60-8
Terphenyl-dl4 (S) 101 % 08/20/03 20 :24 BET 1718-51-0
Pbenol-d5 (S)28 % 08/20/03 20 :24 BET 4165-62-2
2-Fluorophenol (S)42 % 08/20/03 20:24 BET 367-12-4
2,4,6-Tribrmophenol (S) 83 15 011/20/03 20 :24 BE T
Date Extracted 08/19/03 08/19/03
Comments ; Saanple received outside of EPA recommended holding time .
Date :08/26/03 Page : 2 of
w-IV5 1 aboialory Ceftificailion It,b,r,toN Clablirgi REPORT OF LABORATORY ANALYSIS Ky Drinking Water 9DD90NCWastewater 1 2
NC Drinking Water 37706 This retiont shall not be recroduceo, excePt in lull,VA Drinking Water 213
Sc 99OD6 without the wiften consent of Pace Aralf,racal Sewices . Inc . Ft-NELAP E87627
Pace Anslythfal SerWees,Ific .M Kh ;W Averfus, Suits 100
Hiluilarsville, W 28078aceAnalXicalPhone.,704.8759W
w"Ay.pacelabs-cont Fair.7048759W
Lab Project Number : 924896 7
Client Project ID : 03-JUL_ 0339/KI135 6
Lab Sample NO : 923239222 Project Sample Number : 924B967-002 Date Collected! 07/24/03 13 :30
Client Sample ID :23024530/PMWB-S Matrix : Water Date Received :08/13/03 12 :05
Parametere __gfflfultS Units Revort Limi Analyzed By CAS No . 011al Recitan t
GC/MS Sentivolatile S
Septivolatile organics Prep/Method :EPA 827 0
AcerulliPlithene 120 ug/l 10 . 08/21/03 14 :48 BET 83-32-9 1
AcoulliPhthYlialull ND ug/l 10, 08/21/03 14 :48 BET 208-96-8
Aniline ND ug/l 10 . 08/21/03 14 :48 BET 62-53-3
Anthracene No ug/l 10 . 08/21/03 14 :48 BET 120-12-7
BM20 (a) anthracene ND ug/l 10 . 08/21/03 14 :48 BET 56-55-3
BaZ1Z0 (a)pyrene ND Ug/l 10 . 08/21/03 14 :48 BET 50-32.8
Benzo (b) f luorantheolue ND ug/l 10 . 08/21/03 14 ;48 BET 205-99-2
BM20(g,h,i)peryl-e ND u9i'l 10 . 08/21/03 14 :48 BET 191-24-2
BenZ0 (k) f luoranthene ND Ug/l 10 . 08/21/03 14 :48 BET 207-08-9
Benzoic acid ND ug/l 50 . 08/21/03 14 :48 BET 65-85-0
Bonlryl alcohol No ug/l 20 .08/21/03 14 :48 BET 100-51-6
4-Br,,,ph,,ylphwyl other ND ug/l 10 . 08/21/03 14 :48 BET 101-55-3
Butylbmzylphthalate ND Ug/l 10 . 08/21/03 14 :40 BET OS-68-7
4 -Chloro-3 -"thylph-01 ND ug/l 01/11/13 14 :11 BET 51-50-7
4-Chloroarfiline No ug/l 20 .08/21/03 14 :48 BET 106-47-8
bin (2 -Chlorcethoxy) methane ND ug/l 10 . 08/21/03 14 :48 BET 111-91-1
bis(2-Chloroothyl) ether MID ug/l 10 . 08/21/03 14 :48 BET 111-44-4
bio(2-Chloroiaoprolyyl) ether No USA 10 . 08/21/03 14 :48 BET 39638-32-9
2-Chloronaphthalene ND ug/l 10 . 08/21/03 14 :48 BET 91-5B-7
2-Chlorophon0l ND ug/l 10 . 08/21/03 14 :48 BET 95-57-8
41-Chlorophanylphanyl ether ND ug/l 10 . 08/21/03 14 :48 BET 7005-72-3
Chrysene ND ug/l 10 . 08/21/03 14 :48 BET 218-01-9
Dibenz (a,h)anthracene ND ug/l 10 .oe/21/03 14 :48 BET 53-70-3
Dibenzofurato 13 . ug/l 10 . 08/21/03 14 :48 BET 132-64-9
1,2-Dichlorobenzene No ug/l 10 . 08/21/03 14 :48 BET 95-50-1
1, 3 -Dichlorobenzene MID ug/l 10 . 08/21/03 14 :48 BET 541-73-1
1,41-Dichlorobacliene ND ug/l 10 .o8/21/03 14 :48 BET 106-46-7
3,3--Dichlorobenzidine ND USA 20 .08/21/03 14 :48 BET 91-94-1
2,4-Dichlorophenol No ug/l 10 . 08/21/03 14 :48 BET 120-83-2
Diethylphthalate No ug/l 10 . 08/21/03 14 :49 BET 84-66-2
2,4-Dimethylphenol No ug/l 10 . 08/21/03 14 :48 BET 105-67-9
Dimethylphthalate ND ug/l 10 . 08/21/03 14 :48 BET 131-11-3
Di-u-butylphthalate ND ug/l 10 . 08/21/03 14 :48 BET 84-74-2
4,6-Dinitro-2-methylphenol No ug/l 50 . 08/21/03 14 :48 BET 534-52-1
2,4-Dinitrophenol No Ug/l 50 . 08/21/03 14 :48 BET 51-28-5
2,4-Dinitrotoluezie No ug/l 10 . 08/21/03 14 :48 BET 121-14-2
2,6-Dinitrotoluene ND ug/l 10 . 08/21/03 14 :48 BET 606-20-2
Page ;3 of 19Date~00/26/03
1 Mouton, Cernfirztepin lDq1a"fatoHCerlfQlQl11Uf5 REPORT OF LABORATORY ANALYSIS KY Drinking Water 9DO90NCWastamber 12 nking Water 213NCDrinking water 37706 This report stuill not be reproduced, except in full,VA On
SC 99OD6 without the "rfn consent of Pace Analytical SerAces .Inc,FL NELAP E87627
Pace malytical Serwess,Inc.
M Pay Averedue, Suite 100
Huntal NC 28078OAnalyfical'Phone [phone]
Pn-AvipacefabS.com AU.,704.875. 9MI
Lab Project Number : 924896 7
Client Project ID : 03-JUL _ 0339/MI135 6
Lab Sample No :923239222 Project Sample Number :9248967-002 Date Collected ; 07/24/03 13 :30
Client Sample ID :23024530/PNWB-S Matrix : Water Date Received :08/13/03 12 :05
Parameters Results Units escort Limit Analyzed By CAB No . Dual Rattles
Di-n-octylphthalate ND ug/l 10 . 08/21/03 14 :48 BET 117-04-0
1,2-Diphwylhydrazine ED ug/l 20 .08/21/03 14 :48 BET 122-66-7
bia(2-Ethylhexyl)pbthalate Be ug/l 10 . 08/21/03 14 :48 BET 117-81-7
Fluorazatheme ND ug/l 10 . 08/21/03 14 :48 BET 206-44-0
Fluorene 37 . ug/l 10 . 08/21/03 14 :48 BET 86-73-7
Heatachloro-1,31-butadiene ND ug/l 10 . 08/21/03 14 :48 BET 87-68-3
Hexachlorobenzens ND ug/l 10 . 08/21/03 14 :48 BET 118-74-1
Emacblorocyclopentadime ND ug/l 10 . 08/21/03 14 :48 BET 77-47-4
Hexachloroethane ND ug/l 10 . 08/21/03 14:48 BET 67-72-1
Ind=o(l,2,3-cd)pyrene Be ug/l 10 . 08/21/03 14 :48 BET 193-39-5
Isophorone KID ug/l 10 . 08/21/03 14 :48 BET 78-59-1
2-Methy1naplathalene 570 ug/l 200 08/21/03 14 :48 BET 91-57-6
2-Methylphescal (0-Cresol)ND USA 10 . 08/21/03 14 :48 BET 95-48-7
3&4-Mothylphawl ND ug/l 10 . 08/21/03 14 :48 BET
Naphthalene 2600 ug/l 400 08/21/03 14 :48 BET 91-20-3
2-Nitroarailine ND ug/l 50 . 08/21/03 14 :48 BET 88-74-4
3-Nitro=iline ED ug/l 50, 08/21/03 14 :48 BET 99-09-2
4-Nitromiline ND ug/l 50 . 08/21/03 14 :48 BET 100-01-6
Nitrobezzwe ND ug/l 10 . 08/21/03 14AB BET 98-95-3
2-Nitrophanol ND ug/l 10 . 08/21/03 14 :46 BET 88-75-5
4-Nitrophenol ND ug/l 50 . 08/21/03 14 :48 BET 100-02-7
N-Nitrosollimethylamine ND ug/l 10 . 08/21/03 14 :48 BET 62-75-9
N-Nitroso-di-n-propylamine BID ug/l 10 . 08/21/03 14 :48 BET 621-64-7
N-Nitrogodiphmylamine ND ug/l 10 . 08/21/03 14 :48 BET 86-30-6
Pentachlorophenol KID ug/l 50 . 08/21/03 14 :48 BET 87-86-5
Phertantlarene 31 . ug/l 10 . 08/21/03 14 :48 BET 85-01-8
Phenol KID ug/l 10 . 08/21/03 14 :48 BET 108-95-2
Pyrene ND ug/l 10 . 08/21/03 14 :48 BET 129-00-0
1,2,4-Trichlorobenzene ND USA 10 . 08/21/03 14 :48 BET 120-82-1
2 .4,5-Trichlorophenol ND ug/l 50 . 08/21/03 14 :48 BUT 95-95-4
2,4,6-Trichlorophenol ND ug/l 10 . 08/21/03 14 :48 BET 88-06-2
Nitrobenzene-d5 (S) 127 % 08/21/03 14 :48 BET 4165-60-0 2
2-Fluorobipbenyl (S) 66 % 08/21/03 14 :48 BET 321-60-8
Terphmyl-dl4 (S) 115 % 08/21/03 14 :48 BET 1718-51-0
Phenol-dS (S)20 % 08/21/03 14 :48 BET 4165-62-2
2-Fluorophenol (S) 23 % 08/21/03 14 :48 BET 367-12-4
2,4,6-Tribrmophenol (S)74 % 08/21/03 14 ;48 BET
Date Extracted 08/19/03 08/19/03
Comments :Sample received outside of EPA recommended holding time .
Date ;08/26/03 Page : 4 of 19
1,13cralory Cartificallon IDS alboratory Cerldficalron IDS
NC ViWearater 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
NC Drinking Water 37706 This report Shall not be reproduced, except in full, VA Drinking Water 213
SC 99DO6 without the written consent of Pace mairtical Semors, Im .K NELAP E87627
ftce Analytical Services, Inc .
WOMAwnue, Suite 100
HunherswIle,NC 28078aceAnalXicaf-Phone.-70f.875.9092
wi"y.pacelabs.com Far 704.875.W
Lab Project Number :924896 7
Client Project ID : 03-JUL-0339/HI135 6
Lab Sample No :923239230 Project Sample Number :9248967-003 Date Collected : 07/24/03 15 :50
Client Sample ID : 23024531/P-IS Matrix : Water Date Received :08/13/03 12 :05
Parameters Results Units ReRort Limit Analyzed By CKS No .Oual ReqLm t
GC/NS Selaivolatile s
Sestivolatile Organics Prop/method : EPA 827 0
Acenaphthene ED ug/l 10 . 08/25/03 18 :00 BET 83-32-9
Acenaphthylerne ND ug/l 10 . 08/25/03 18 :00 BET 208-96-8
Aniline ND ug/l 10 . 08/25/03 18 :00 BET 62-53-3
Anthracene ND ug/l 10 . 08/25/03 18 :00 BET 120-12-7
Benzo(a) anthracene ND ug/l 10 . 08/25/03 18 :00 BET 56-55-3
Bmzo(a)pyr=e ND ug/l 10 . 08/25/03 18 :00 BHT 50-32-8
Benito (b) If lucrantherre ED ug/l 10 . 08/25/03 18 :00 BET 205-99 .2
Benzo(g,h,i)peryleUa ED ug/l 10 . 06/25/03 18 :00 BET 191-24-2
Bwzo (k) f luoranthene ED ug/l 10 . 08/25/03 18 :00 BET 207-08-9
Benzoic acid KID ug/l 50 . 08/25/03 18 :00 BET 65-65-0
Bwzyl alcohol ND ug/l 20 .08/25/03 18 :00 BET 100-51-6
41-Bramopherrylphanyl ether ND ug/l 10 . 08/25/03 18 :00 BET 101-55-3
Butylbenrylphthalate ND ug/l 10 . 08/25/03 19 :00 BET 65-68-7
4-Chloro,3-zethylplenol ND ug/l 21, 01/21/01 l1i10 BET 19-50-7
4-Chloroamiline,MID ug/l 20 .08/25/03 18~00 BET 106-47-8
bis(2-Chloroetholcy)metharce,ED ug/l 10 . 08/25/03 18 :00 BET 111-91-1
bis(2-Chloroethyl) ether ND UST/I 10 . 08/25/03 18 ;00 BET 111-44-4
bis(2-Chloroisopropyl) ether ND ug/l 10 . 08/25/03 18 :00 BET 39638-32-9
2-Chlormaphthalene ND ug/l 10 . 08/25/03 18 :00 BET 91-58-7
2-Chloropherol ND ug/l 10 . 08/25/03 18 :00 BET 95-57-8
4-Chlorophanylphenyl ether ND ug/l 10 . 08/25/03 18 :00 BET 7005-72-3
Claryserns,ND ug/l 10 . 08/25/03 18 :00 BET 218-01-9
Dibenz(a,h)autbracene ED ug/l 10 . 08/25/03 18 :00 BET 53-70-3
Dibenzofurart KID ug/l 10 . 08/25/03 18 :00 BET 132-64-9
1 .2-Dichlorobefuzene ND UR/1 10 . 08/25/03 18 :00 BET 95-50-1
1,3-Dichlorobenzeme,MID ug/l 10 . 08/25/03 18 :00 BET 541-73-1
1,41-Dichlorobenzene ND ug/l 10 . 08/25/03 18 :00 BET 106-46-7
3,3--Dichlorobenzidine ND ug/l 20 .08/25/03 18 :00 BET 91-94-1
2,4-Dichlorophenol ND Ug1l 10 . 08/25/03 18 :00 BET 120-83-2
Diethylphthalate ND ug/l 10 . 08/25/03 18 :00 BET 84-66-2
2 .4-Dimethylphenol ND ug/l 10 . 08/25/03 18 :00 BET 105-67-9
Dimethylphthalate ND ugli 10 . 08/25/03 18 :00 BET 131-11-3
Di-n-butylphthalate ED ug/l 10 . 08/25/03 18 :00 BET 84-74-2
4,46-Dinitro-2-methylphenol RD ug/l 50 . 08/25/03 18 :00 BET 534-52-2
2,4-Dinitrophenol ND ug/l 50 . 08/25/03 18 :00 BET 51-28-5
2,4-Dinitrotoluene ND ug/l 10 . 08/25/03 18 :00 BET 121-14-2
2,6-Dinitrotoluene ND ug/l 10 . 08/25/03 18 :00 BET 606-20-2
Date :08/26/03 Page : 5 of 19
l,bor,[DN Cerlificalum IQ5 REPORT OF LABORATORY ANALYSIS 1~horgb,N Certification I
NG Wasteerane, 12 KY Drinking Water 9OD90
NC Drinking Water 37706 This report shall not be reprock,rced, except in full . VA Drinking Water 213
SC 99006 w0hout the wrinen consent of Pace Auralytical SeNices . Inc . FL NELAP E87627
Pace Analytical Satirical Inc.
MT Kincey Avelibig Suite 100
Huntermile,AfC 28078aceAnalyfical"Phone.-704.875.90.92
wvAy.pacelabs.com Fax.[phone]
Lab Project Number :924896 7
Client Proj act ID : 03-JUL-0339/NI135 6
Lab Sample No :923239230 Project Sample Number :9248967-003 Date Collected : 07/24/03 15 :50
Client Sample ID : 23024531/P .lS Katrix : Water Date Received :08/13/03 12 ;05
Parameters Results, Units Re;gnrt Limit ___AnAlyzed_-By CAB No . Dual Reglant
Di-n-octylphthalate ND ug/l 10 . 08/25/03 18 :00 BET 117-1114-0
1,2-Diphenylbydrazine No ug/l 20 .08/25/03 18 :00 BET 122-66-7
bis(2-Rthylhexyl)phthalate No ug/l 10 . 08/25/03 18 :00 BET 117-81-7
Fluoranthene No ug/l 10 . 08/25/03 Men BET 206-44-0
Fluorene No ug/l 10 . 08/25/03 18 :00 BET 86-73-7
Heacachloro-1,3-buttudiene No ug/l 10 . 08/25/03 18 :00 BET 87-68-3
Heocachloroberazerate No ug/1 10 . 08/25/03 18 :00 BET 118-74-1
Hexachlorocyclopentadiene No ug/1 10 . 08/25/03 18 :00 BET 77-47-4
Hatcachlorcethapare No ug/l 10 . 08/25/03 18 :00 BET 67-72-1
1nd=o(l,2,3-cd)Pyrwe No ug/l 10 . 08/25/03 18 :00 BET 193-39-5
Isophorone ND ug/l 10 . 08/25/03 18 :00 BET 78-59-1
2-Methyltbaplathalene No ug/l 10 . 08/25/03 10 :00 BET 91-57-6
2-Hathylphespol (0-Cresol)No ug/l 10 . 08/25/03 18 :00 BET 95-48-7
3&4-Netlrylphenol No ug/l 10 . 08/25/03 18 :00 BET
Naphthalene No ug/l 10 . 08/25/03 18 :00 BET 91-20-3
1-NItrosalline,No ug/l 50 . 08/25/03 18 :00 BET 88-74-4
3-Nitroaniline No ug/l 50 . 08/25/03 18 ;00 BET 99-09-2
4-Nitroaniline No ug/l 50 . 08/25/03 18 :00 BET 100-01-6
Nitrobenzene No ug/l 10 . 08/25/03 18 :00 BET 98-95-3
2-Nitrophemol No ug/l 10 . 08/25/03 18 :00 BET 88-75-5
4~Nitrophenol ND ug/l 50 . 08/25/03 18 :00 BET 100-02-7
N-Nitrosodimethylamine No ug/l 10 . 08/25/03 18 :00 BET 62-75-9
N-Nitroso-di-n-propylazzatine ND ug/l 10 . 08/25/03 18 :00 BET 621-64-7
N-Nitrosodiphesaylamine ND ug/l 10 . 08/25/03 18 :00 BET 86-30-6
Pentachlorophemol ND ug/l 50 . 08/25/03 18 :00 BET 87-86-5
Phemanthrene No ug/l 10 . 08/25/03 18 :00 BET 85-01-8
Phenol No ug/l 10 . 08/25/03 18 :00 BET 108-95-2
Pyrene No ug/l 10 . 08/25/03 18 :00 BET 129-00-0
1,2,4-Trichlorobenzene No ug/l 10 . 08/25/03 18 :00 BET 120-82-1
2,4,5-Trichlorophmol No ug/l 50 . 08/25/03 18 :00 BET 95-95-4
2,4,6-Trichlorophanol No ug/l 10 . 08/25/03 18 :00 BET 68-06-2
Nitrobenzene-0 (S) 50 It 08/25/03 18 :00 BET 4165-60-0
2-Fluorobipharlyl (S)49 % 08/25/03 18 :00 BET 321-60-8
Terphenyl-dl4 (S) 60 % 08/25/03 18 :00 BET 1718-51-0
Phenol-d5 (S) 11 % 08/25/03 18 :00 BET 4165-62-2
2-Fluorophanol (S)12 % 08/25/03 18 :00 BET 367-12-4
2,4,6-Tribromophenol (S) 26 % 08/25/03 18 :00 BET
Date Extracted 08/19/03 08119/03
Comments :Sample received outside of EPA recommended holding time .
nat,OB/26/03 P-9.: 6 f 19
(,ognthory Cerblicathaft IDS I alongloN Centhution I
NC Wasteenater 12 REPORT OF LABORATORY ANALYSIS KY Dninkurg Water 9DD90
NC Drinking Water 37706 This report sarrall not be reproduced, except in lull,VA Drinking Water 213
SC 9M wrthout the written conwol of Pace Arwattlical Services,In,FL NELAP E87627
Pace Analytical servic",Inc.
9WO Kincify Averful Suite 100
HunterSville,AC 28078aceAna1j&ca1'*Phow 7048759W
wi-Aypacelabs .com Fax.704.875.M
Lab Project Number :924896 7
Client Project ID :03-JUL-0339/14II35 6
Lab Sample NO :923239248 Project Sample Number ; 92411967-004 Date Collected : 07/24/03 08 :35
Client Sample ID :23024536/PMWL-S Matrix : Water Date Received :08/13/03 12 :05
Parameters Results Units Report Limit Analysed By CKS NO . Dual ReorLim
GC/KS Segaivolatile s
Semivolatile Organics Prep/Method : EPA 827 0
Acenaphthearbe ND ug/l 10 . 08/20/03 22 :10 BET 83-32-9
Aceinaplathyleme ND ug/l 10 . 08/20/03 22 :10 BET 208-96-8
Aniline ND ug/l 10 . 08/20/03 22 :10 BET 62-53-3
Arathracerfe ED ug/l 10 . 08/20/03 22 :10 BET 120-12-7
Banco (a) aukthraceirge ED ug/l 10, 08/20/03 22 :10 BET 56-55-3
Banco (a)pyreate ED UE/1 10 . 08/20/03 22 :10 BET 50-32-8
BealazoWfluorarithene ND uq/l 10 . 08/20/03 22 :10 BET 205-99-2
Bemzo(9,h,i)perylene ND ug/l 10, 00/20/03 22 :10 BET 191-24-2
Banco (k) f lucarantheabe ND ug/l 10 . 08/20/03 22 :10 BET 207-08-9
Small acid NO ug/l 50 . 08/20/03 22 :10 BET 65-85-0
Bwzyl alcohol ND Ug/l 20 .08/20/03 22 :10 BET 100-51-6
4-Brobacaphrany1pbearlyl ether ND ug/l 10 . 08/20/03 22 :10 BET 101-55-3
Butylbeaksylphthalate MID ug/l 11). 08/20/03 22 :10 BET 85-68-7
4-Chloro-3-methylphenol ND Ug/l 20 .06/20/03 22 :10 BET 59-50-7
4-Chloroaniline ND ug/l 20 .08/20/03 22 ;10 BET 106-47-8
bia(2-Chloroethozy)metb=e ND ug/l 10 . 08/20/03 22 :10 BET 111-91-1
bia(2-Chloroethyl) ether ND ug/l 10 . 08/20/03 22 :10 BET 111-44-4
bis(2-Chloroisopropyl) ether ND ug/l 10 . 08/20/03 22 :10 BET 39638-32-9
2 -Chloronaphthalene KID ug/l 10 . 08/20/03 22 :10 BHT 91-58-7
2-Chlorophenol.ED ug/l 10 . 08/20/03 22 :10 BET 95-57-8
4-Chlorophisaylphenyl ether ND Ug/l 10 . 08/20/03 22 :10 BET 7005-72-3
Chrysene ND ug/l 10 . 08/20/03 22 :10 BET 218-01-9
Dibenz (a, h) fulthracene ND ug/l 10 . 08/20/03 22 :10 BET 53-70-3
Dibermofuran,ND ug/l 10 . 08/20/03 22 :10 BET 132-64-9
1,2-Dichlorobenzene KID ug/l 10 . 08/20/03 22 :10 BET 95-50-1
1,3-Dichlorobenzerge ND ug/l 10 . 08/20/03 22 :10 BET 541-73-1
1,4-Dichlorobermene ND ug/l 10 . 00/20/03 22 :10 BET 106-46-7
3,3--Dichlorobenzidine ND ug/l 20 .08/20/03 22 :10 BET 91-94-1
2,4-Dichlorophenol KID ug/l 10 . 08/20/03 22 :10 BET 120-83-2
Diethylphthalate ND ug/l 10 . 08/20/03 22 :10 BET 84-66-2
2,4-Dimethylphenol ND ug/l 10 . 09/20/03 22 :10 BET 105-67-9
Dimethylphthalate ND ug/l 10 . 08/20/03 22 :10 BET 131-11-3
Di-n-butylphthalate ND ug/l 10 . 08/20/03 22 :11)BET 84-74-2
4 .6-Dinitro-2-methylphenol ND ug/l so . 08/20/03 22 :10 BET 534-52-1
2,4-Dinitrophenol ND ug/l 50 . 08/20/03 22 :10 BET 51-28-5
2,4-Dinitrotoluene ND ug/l 10 . 08/20/03 22 :10 BET 121-14-2
2 .6-Dinitrotoluene ND ug/l 10 . 08/20/03 22 :10 BET 606-20-2
laate~08/26/113 Page~7 of 19
40
1 apgratore Cartheation Ills REPORT OF LABORATORY ANALYSIS I-aharatioN Certification ID
NC Wasunkatiff 12 KY Drinking Water 90090
NC Drinking Water 377D6 This nation shall not be fewirduced, except in lull,VA Drinking Wale,213
SO 99006 wnhout the written consent of Pace Analifical Serxicers, Inc . FL NELAP E87627
Pace Analytical Serifives, Inc.
M KsnM Awnue, Suite 100
Huntarsville,NC 28078aceAnalXical`Phone.,704.875902
wivwy.pacelabs .conr Fax.704.875.M
Lab Project Number :924896 7
Client Project ID :03-JUL-0339/KI135 6
Lab Sample No : 923239248 Project Sample Number : 9248967-004 Date Collected : 07/24/03 08 :35
Client Sample ID :23024536/PKWL-S Matrix : Water Date Received :08/13/03 12 :05
Parameters Results units Report Lied . Analyzed BY CAB No .Oual ReqLmt
Di-n-octylphthalate No ug/1 10 . 08120/03 22 :10 BET 117-84-0
1,2-Diphenylhydrazine ND ug/l 20 .08/20/03 22 :10 BET 122-66-7
bis(2-Ethylhexyl)pbtbalate ND ug/l 10 . 08/20/03 22 :10 BET 117-81-7
Pluorafrothene,ND ug/l 10 . 08/20/03 22 :10 BET 206-44-0
Fluorene,No ug/l 10 . 08/20/03 22 :10 BET 06-73-7
Rexachloro-1 .3-butadiene ND ug/l 10 . 08/20/03 22 :10 BET 87-68-3
Hexachlorobenzene,ND ug/l 10 . 08/20103 22 :10 BET 118-74-1
Hexachlorocyclopentadiene No ug/l 10 . 08/20/03 22 :10 BET 77-47-4
Hexachlorciethane,No ug/l 10 . 08/20/03 22 :10 BET 67-72-1
1nd=o(1,2,3-cd)pyrens No ug/l 10 . 08/20/03 22 :10 BET 193-39-5
Isophorcut ND USA 10 . 08/20/03 22 :10 BET 78-59-1
2 -Methyllawaplathaleage ND ug/1 10 . 08/20/03 22 :10 BHT 91-57-6
2-Methylphenol (o-Cresol)ND ug/l 10 . 08/20/03 22 :10 BET 95-48-7
U41-Methylpherfol ND ug/l 10 . 08/20/03 22 ;10 BET
Naphthalene No ug/l 10 . 08/20/03 22 :10 BET 91-20-3
2-Nitromiline ND ug/l 50 . 08/20/03 22 :10 BET 88-74-4
3-Nitromiline No ug/l 50 . 08/20/03 22 :10 BET 99-09-2
4-Nitroaniline KID ug/l 50 . 08/20/03 22 :10 BET 100-01-6
elitroberizeme ND ug/l 10 . 08/20/03 22 :10 BET 98-95-3
2-Nitropherrool No ug/l 10 . 08/20/03 22 :10 BET 89-75-5
4-Nitrophanol No ug/l 50 . 08/20/03 22 :10 BET 100-02-7
N-Nitrooodimethylamine No ug/l 10 . 08/20/03 22ilO BET 62-75-9
N-Nitroso-di-n-propylamine No ug/l 10 . 08/20/03 22 :10 BET 621-64-7
N-Nitronodiphanylamire No ug/l 10 . 08/20/03 22 :10 BET 86-30-6
Pentachloropheatol ND ug/1 50 . 08/20/03 22 :10 BET 87-86-5
Phenanthrene No ug/l 10 . 08/20/03 22 :10 BET 85-01-8
Phenol No ugf/l 10 . 08/20/03 22 :10 BET 108-95-2
Pyrene ND ug/l 10 . 08/20/03 22 :10 BET 129-00-0
1,2,4-Trichlorobenzwe No ug/l 10 . 08/20/03 22 :10 BET 120-82-1
2,4,5-Trichlorophenol ND ug/l 50 . 08/20/03 22 :10 BET 95-95-4
2,41,6-Trichlorophencil ND ug/l 10 . 08/20/03 22 :10 BET 88-06-2
Nitrobenlienei (S) 58 % 08/20/03 22 :10 BET 4165-60-0
2-Fluorobiphenyl (S) 58 % 08/20/03 22 :10 BET 321-60-8
Terphenyl-c[14 (S) 99 % 08/20/03 22 :10 BET 1718-51-0
Pheani (S) 0 % 08/20/03 22 :10 BET 4165-62-2 3
2-Pluoropbezol (S) 1 % 08/20/03 22 :10 BET 367-12-4 3
2,4,6-Tribromaphenol (S) 13 % 08/20/03 22 :10 BET 3
Date Extracted 08/19/03 08/19/0 3
Comments : Sample received outside of EPA recommended holding time .
Date ;00/26/03 page : 8 of 19
11105 ahoraitory Unification QsIaboratori, Cedifieceig REPORT OF LABORATORY ANALYSIS KY Drinking Water 9OD90NCWrinearrate, 1 2
NC Drinking Water 37706 This repon Still not be reproduaced, except in full. VA Drinking Water 213
SC 99DD6 without the written consent of Pace Analytical Servicei Inc . FL NELAP E87627
Pace Ana4lical SerWen,hic.
-W Array Areerhae, Suite 100
Hunteiswlht~NO 28078aceAnalyficaf-Phonel 704.875.9092wivwpacelabs.com Far 704.875.M
Lab Project Number :924896 7
Client Project ID : 03-JUL-0339/NI135 6
Lab Sample No :923239255 Project Sample Number :9248967-005 Date Collected :07/25/03 08 :35
Client Sample ID : 23024537/FIELD SLAW Matrix : Water Date Received ;08/13/03 12 :05
Parameters Results Units Revort Lind Analyzed By CAB No . Dual Raglan
GCIMS Segnivolatile s
Semivolatile Organics Prep/method :EPA 827 0
Acenaphthene ED ug/l 10 . 08/20/03 23 :21 BET 83-32-9
Acenaphtlayleclue ND ug/l 10 . 08/20/03 23 :21 BUT 208-96-8
Aniline ND ug/l 10 . 08/20/03 23 :21 BET 62-53-3
Anthracme BID ug/l 10 . 08/20/03 23 :21 BET 120-12-7
BerazoWmatthracents ND ug/l 10 .OB/20/03 23 ;21 BUT 56-55-3
Bmzo(&)pyrme KID ug/l 10 . 08/20/03 23 :21 BET 50-32-8
Began (b) f luorrunthernat ED ug/l 10 . 00/20/03 23 :21 BET 205-99-2
Bmzo(g,b,i)perylme ND ug/l 10 . 00/20/03 23 ;21 BET 191-24-2
Boner,(k) If luorantherte ED ug/l 10 . 08/20/03 23 :21 BET 207-08-9
Henzoic acid ND ug/l 50 . 08/20/03 23 :21 BET 65-85-0
Benzyl alcohol ED ug/l 20 .00/20/03 23 :21 BET 100-51-6
4-Bromopbeitylphenyl other ED ug/l 10 . 08/20/03 23 :21 BET 101-55-3
Butylbenzylphthalate ND ug/l 10 . 08/20/03 23 :21 BET 85-68-7
4-Chloro-3-methylphenol ND ug/l 20 .08/20/03 23 :21 BET 59-50-7
4-Chloroazliline MID ug/l 20 .08/20/03 23 :21 BET 106-47-8
bia(2-Chloroethoxy)methane MD ug/l 10 . 08/20/03 23 :21 BET 111-91-1
bis(2-Chloroethyl) other ND ug/l 10 . 08/20/03 23 :21 BET 111-44-4
bis(2-Chloroisopropyl) ether ND ug/l 10 . 08/20/03 23 :21 BET 39638-32-9
2-Chloronaphthalene ND ug/l 10 . 08/20/03 23 :21 BET 91-58-7
2-Chlorophenol.ND ug/l 10 . 08/20/03 23 :21 BET 95-57-8
4-Chlorophorrylphanyl ether MD ug/l 10 . 08/20/03 23 :21 BET 7005-72-3
Chrysene ND ug/l 10 . 08/20/03 23 :21 BET 218-01-9
Dibenz(a,h) anthracerie ND ug/l 10 . 08/20/03 23 :21 BET 53-70-3
Dibecuselturan ND ug/l 10 . 08/20/03 23 :21 BET 132-64-9
1,2-Dichlorobenzene ND ug/l 10 . 08/20/03 23 :21 BET 95-50-1
1,3-Dichlorobenzener ND ug/l 10 . 08/20/03 23 :21 BET 541-73-1
1,41-Dichlorobenzene ND ug/l 10 . 08/20/03 23 :21 BET 106-46-7
3 .3--Dichlorobenzidine ND ug/l 20 .08/20/03 23 :21 BET 91-94-1
2,41-Dichloropbenol MID ug/l 10 . 08/20/03 23 :21 BET 120-83-2
Diethylpbthalate ND ug/l 10 . 08/20/03 23 ;21 BET 84-66-2
2,4-Dimethylphenol ND ug/l 10 . 08/20/03 23 :21 BET 105-67-9
Dimethylphthalate ND ug/l 10 . 00/20/03 23 :21 BET 131-11-3
Di-n-butylphthalate ND ug/l 10 . 08/20/03 23 :21 BET 84-74-2
4,6-Dititro-2-methylphenol ND ug/l 50 . 08/20/03 23 :21 BET 534-52-1
2,4-Dinitrophmol ND ug/l so . 08/20/03 23 :21 BET 51-28-5
2,4-Dinitrotoluene MID ug/l 10 . 08/20/03 23 :21 BET 121-14-2
2,6-Dinitrotoluene ND ug/l 10 . 08/20/03 23 :21 BET 606-20-2
Date :08/26/03 ftqe~ 9 f,f 15
lamiatoNCtitificationlDs Laboratory Unification I
NC wastenter 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reprokluced . except in full,VA Drinking Water 213
SC 99006 without the written consent ol Pace Analtyl Services, Inc. FL NELAP E87627
Pace Analytical Services, Inc .
9M Kincey Avenue, Suite 100
Hunfetsville,NO 28078aceAnaIjiffiticaf-Phone.,704.875,9092wit,ii,pacaelabS.Com Fa.704.675.9091
Lab Project Number :924896 7
Client Project ID :03-JUL _0339/MI135 6
Lab Sample No :923239255 Project Sample Number ;9248967-005 Date Collected :07/25/03 08 :35
Client Sample ID : 23024537/FIELD BLANK Katrix : Water Date Received :08/13/03 12 :05
Parameters Results- units Report Limi Analyzed BY CAB No .Gual Raglan
Di-n~octylpahthalate ND ug/l 10 . 08/20/03 23 :21 BET 117-84-0
1,2-Diphenylhydrazine ND ug/l 20 .08/20/03 23 :21 BET 122-66-7
bia(2-Ethylhexyl)pbthalate ND ug/I 10 . 08/20/03 23 ;21 BET 117-81-7
Fluoranthene ND ugr/I 10 . 08/20/03 23 :21 BET 206-44-0
Pluorene ND Ug/l 10 . 08/20/03 23 :21 BET 86-73-7
H"achloro-1,3-butadiene ND ug/l 10 . 08/20/03 23 :21 BET 87-68-3
Reccachlorobeduene ND ug/l 10 . 08/20/03 23 :21 BET 118-74-1
Nexachlorocyclopentadiene No ug/l 10 . 08/20/03 23 :21 BET 77-47-4
Hexachloroethane ND ug/l 10 . 08/20/03 23 :21 BET 67-72-1
Jndaco(I,2,3-cd)pyrei No US/' 10 . 08/20/03 23 :21 BET 193-39-5
Isophorone No ug/l 10 . 08/20/03 23M BET 78-59-1
2-Nethyltaphthailene No ug/l 10 . 08/20/03 23 :21 BET 91-57-6
2-Nethylphenol (o-Cresol)No ugr/l 10 . 08/20/03 23 :21 BET 95-48-7
3&4-Nathylphenol ND ug/l 10 . 08/20/03 23 :21 BET
Naphthalene No ug/I 10 . 08/20/03 23 :21 BET 91-20-3
2-Nitromiline No ug/I 50 . 08/20/03 23 :21 BET 88-74-4
3-Nitroaniline No ug/l 50 . 08/20/03 23 :21 BET 99-09-2
4-Nitromiline ND ug/I 50 . 08/20/03 23 :21 BET 100-01-6
Nitrobtanaterse ND ug/l 10 . 08/20/03 23 :21 BET 98-95-3
2-Nitrophenol No uq/l 10 . 08/20/03 23 :21 BET 88-75-5
4-Nitrophenol ND ug/l 50 . 08/20/03 23 :21 BET 100-02-7
N-Nitrooodimethylamine ND ug/l 10 . 08/20/03 23 :21 BET 62-75-9
N-Nitroso-di-n-propylamine No ugf/I 10 . 08/20/03 23 :21 BET 621-64-7
N-Nitrosodipherrylapaine No Ug/l 10 . 08/20/03 23 :21 BET 86-30-6
Prentachlorophearl No ug/l 50 . 08/20/03 23 :21 BET 87-86-5
Pheranthrene No ug/l Ia . 08/20/03 23 :21 BET 85-01-8
Phenol No ugll 10 . 08/20/03 23 :21 BET 108-95-2
Pyrene No Ug/l 10 . 08/20/03 23 :21 BET 129-00-0
1,2,4-Trichlorobenzene No ug/l 10 . 08/20/03 23 :21 BET 120-82-1
2,4,5-Trichlorophenol No ug/l 50 . 08/20/03 23 :21 BET 95-95-4
2,4,6-Trichlorophenol ND ug/l 10 . 08/20/03 23 :21 BET 88-06-2
Nitrobenzene-d5 IS) 65 % 08/20/03 23 :21 BET 4165-60-0
2-Flucirobiphenyl IS)64 % 08/20/03 23 :21 BET 321-60-8
Terphenyl-d14 IS)112 % 08/20/03 23 :21 BET 1718-51-0
Phenol-d5 IS) 30 Sk 08/20/03 23 :21 BET 4165-62-2
2-Fluorophenol IS)44 % 08/20/03 23 :21 BET 367-12-4
2,4,6-Tribromphenol IS)82 08/20/03 23 :21 BET
Date Extracted 08/19/03 08/19/03
Comments :Sample received outside of EPA recommended holding time .
Date ;08/26/03 Page :10 of 19
Ceddlegilon as REPORT OF LABORATORY ANALYSIS LaboraloN CellifiCafiDn i
NC Wastewater 12 KY Drinking Water 9DD90
NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213
SC 99006 without the written consent of Pace Anil Sewices, Irl FL NELAP E87627
Pace Malyfical SerWas, lite .
98W Kincey Anfinue, Suffe 100
Huntarsvifle,NC 28078aceAnaIjfilPhone.,704.875.9092m-Aypacelabs .com Far 7048759091
Lab Project Number :924896 7
Client Project ID :03-JUL-0339/MI1356
PARAMETER FOOTNOTE S
Inorganic Wet Chemistry Analyses were performed at our Pace ksheville laboratory and Organic and Metals
testing was performed at our Pace Charlotte laboratory urfless otherwise footnoted .
No Not detected at or above adjusted reporting limit
NC Not Calculable
J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDL Adjusted Method Detection Limi t
(S)Surrogate
[I]Compound concentration eaceedo the calibration range of the instrument (CLP Z-Flag).
(2) Base/neutral surrogate recovery outside of control limits . The data was accepted based on valid recovery of
r-ining two base/neutral surrogates .
131 Surrogate recovery outside of acceptance window confirmed as a matrix effect by the analysis of a duplicate or
MS/KSD on this sample .
Date :08126/03 Page :11 of 19
litborat,rv Certification 105 Laboratory Unification I
K wastewater 12 REPORT OF LABORA70RY ANALYSIS KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full,VA Drinking Water 213
SC 99006 without the winter, consent of Pace Axiat0cal Services,Inc.FL NELAR E87627
Pace An,1411cal Serinten,/He.
MitinMAkiew, Suite 100
Meltivsville,NC 28076aceAnalytical'Am.-704.875.9092wt-Avpacelabs .cono hu.704.875.X91
QUALITY CONTROL DATA
Lab Project Number :924896 7
Client Project ID : 03-JUL-0339/MI1356
QC Batch :79954 Analysis Method ;EPA 827 0
QC Batch Method : Analysis Description : Sestivolatile Organics
Associated Lab Samples : 923239214 923239222 923239230 923239248 923239255
MEMD BLANK :92325969 1
Associated Lab Samples : 923239214 923239222 923239230 923239248 923239255
Blank Reporting
Parameter Units Result Limit Footnotes
Acenaplathene ug/l ND 10 .
Acenaphithylene ug/l ED 10 .
Aniline ug/l ND 10 .
Anthracene ug/l ND 10,
Benzo(a)anthracerke ug/l ND 10 .
Beezo (a) pyreme ug/l ND 10 .
Bmzo(b)fluor=thane ug/l ND 10 .
Banzo(g,h,i)peryle1ne ng/l ND 10 .
B0mZ0 (k) fluorarathene ug/l ND 10 .
Benzoic acid ug/l ND 51).
Renryl alcohol ug/l ND 20 .
4-Bromacphenylphenyl ether ug/l ND 10 .
Butylbanzylphthalate ug/l ND 10 .
4-Chloro-3-methylphenol ug/l ND 20 .
4-Chloroaniline ug/l ND 2D .
bio(2-Chloroetboxy)meth=e ug/l ND 10 .
bis(2-ChloroethYl) ether ug/l ND 10 .
bis(2-Chloroisopropyl) ether ug/l ND 10 .
2-Chloronaphthalene ug/l ND 10 .
2-Chlorophervol ug/l ND 10 .
4-Chlorophmylphenyl ether ug/l ND 10 .
Chrysene ug/l ND 10 .
Dibenz(a,h)amthracene ugr/l ND 10 .
Dibenzofurats.ug/1 ND 10 .
1,2-Dichlorobenzeme ug/l ND 10 .
1,3-Dichlorobenzene ug/l ND 10 .
1 .4-Dichlorobenzene uq/1 ND 10 .
3,3--Dichlorobenzidine Ug/l ND 20 .
2,4-Dichlorophenol ug/l ND 10 .
Diethylphthalate ug/l ND 10 .
2,4-Dimethylphenol ug/l ND 10 .
Date :08/26/03 Page ; 12 of 19
I aloorancry CertiffalwaJ25 REPORT OF LABORATORY ANALYSIS Laboratory Unification I
NC Wastewate, 12 KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213
Sc 99DO6 wdixten the wiften consent of Pace Arralklacal Services, Inc . FL NELAP E87627
Pace Malytical Serwe",Inc.
M Day Avenue, Suite 100
Hubtarmlle,NC 28078aceAnalXicalPhow704,875.9092
m"v.pacelabs,com Fa.704,875.M
QUALITY CONTROL DATA
Lab Project Number :924896 7
Client Project ID : 03-JUL 0339/NI1356
MMOD BLANK :923259691
Associated Lab Samples : 923239214 923239222 923239230 923239248 923239255
Blank Reporting
Parameter -Units Result Limit Footnotes
Dimethylphthalate ug/l KID 10 .
Di-n-butylphthalate ug/l ND 10 .
4,6-Dinitro-2-methylphenol ug/l ND 50 .
2,4-Dinitropbmol Ug/l ND 50 .
2,4-Dinitrotolume ug/l ND 10 .
2,6-Dinitrotoluene ug/l ND 10 .
Di-n-octylphthalate ug/l NID 10 .
1,2-Diphmylhydrazine ug/l ND 20 .
bis(2-Ethylhexyl)phthalate ug/l ND 10 .
Fluoranthene USA ND 10 .
Pluorene ug/l ND 10 .
H"achloro-1,3-butadiene ug/l ND 10 .
Bearacb1orobenzerne ug/l ND 11,
Harachlorocyclopentadiene,ug/l IND 10 .
Rescachloroetharre ug/l ND 10 .
1rrdemfo(1,2,3-cd)pyrene ug/l ND 10 .
Isophorone ug/l ND 10 .
2-Methyluaphthalene USA NE)10 .
2-Methylphenol (o-Cresol)ug/l ND 10 .
3&4-Methylphenol ug/l ND 10 .
Naphthalene ug/l ND 10 .
2-Nitroaniline ug/l ND 50 .
3-Nitroamiline ug/l ND 50 .
4-Nitroaniline ug/l ND 50 .
Nitrobenzene,ug/l ND 10 .
2-Nitrophenol ug/l ND 10 .
4-Nitrophernol ug/l ND 50 .
N-Nitrosodimethylamine ug/l ND 10 .
N-Nitroso-di-n-propylamine ug/l ND 10 .
N-Nitrosodiphenylamine ug/l ND 10 .
Pentachlorophenol.ug/l ND 50 .
Phtub-othrene,ug/l ND 10 .
Phewl ug/l ND 10 .
Pyrene ug/l ND 10 .
1,2,4-Trichlorobenzene ug/l ND 10 .
2,4,5-Trichlorophenol ug/l ND 50 .
Date :08/26/03 Page ;13 of 19
40
[Lab Laboratory Certilcalion IDIaboratow Cenificatro REPORT OF LABORATORY ANALYSIS KY Drinking Water 9DO90NGWastewater 1 2
NC Drinking Water 37706 This report shelf not be reproduceb, except in full.VA Drinking Water 213
SC 99DD6 without the written c,,mnt,t Pace Anardical Sewices . Inc . FL NELAP E87627
Pace Analyficarf Seivieff, Inc.
W Kincey Avenue, Suite 100
Hunletsville,NC 28078aceAnaljdical"Phone [phone]Mwi-Av.pacatans.com Fm.704.875.M
QUALITY CONTROL DATA
Lab Project Number :924896 7
Client Project ID : 03-JUL-0339/KI1356
METHOD BLANK :92325969 1
Associated Lab Samples : 923239214 923239222 923239230 923239248 923239255
Blank Reporting
Parameter Units Result Limit Footnotes
2,4,6-Trichlorophenol ug/l NO 10 .
Nitrobenzene-d5 (S) % 5 3
2-Fluorobiphelayl (S) % 53
Terphanyl-d14 (S) % 79
Phenol-d5 (S) IS 24
2-Fluorophenol (S) 115 34
2,4,6-Tribroaskophenol (S) %64
LABORATORY CONTROL SAMPLE LCSD : 923259709 92325971 7
Spike LCS ICSD LCS LCSD
Parameter Units -Conc,Result Result Ilk Rao Ill Rao RED Footnotes
Acenaplothene ug/1 50 .00 28 .65 32 .81 57 66 14
Acenaphthylene ug/1 50 .00 213 .33 32 .90 57 66 1 5
Aniline ug/1 50 .00 46 .60 65 .42 93 131 34 1,2
Anthracers ug/l 50 .06 30 .60 35 .09 fil 70 14
BanzoWanthracene uq/l 50 .00 31 .54 34 .98 63 70 10
Benzo(a)pyrene ug/l 50 .00 34 .90 39 .40 70 79 12
Benito (b) f luoranthene ug/l 50 .00 33 .45 34 .93 67 70 4
Benzo(g,h,i)perylene ug/l 50 .00 37 .64 41 .79 75 84 10
BenzoMfluorantheas ug/l 50 .00 40 .56 53 .07 81 106 27
Benzoic acid ug/l 50 .00 6 .259 10 .30 16 21 22
Benzyl alcohol ug/l 50 .00 24 .40 31 .61 49 63 26
4-Bremeophanylphertyl ether ug/l 50 .00 28 .59 32 .89 57 66 14
Butylbenzylphthalate ug/1 50 .00 24 .54 30 .85 49 62 23
4-Chloro-3-methylphenol ug/l 50 .00 24 .97 32 .72 so 65 27
4-Chloromiline ug/l 50 .00 29 .26 36 .23 58 72 21
bia(2-Chloroethoxy)methane uq/l 50 .00 23 .63 26 .81 47 54 13
bis(2-Chloroethyl) ether ug/l 50 .00 21 .53 24 .83 43 50 14
bis(2-Chloroisopropyl) ether ug/l 50 .00 22 .06 25 .51 44 51 14
2-Chlorovaphthalene ug/l 50 .00 29 .46 34 .63 59 69 16
2-Chlorophenol uq/l 50 .00 19 .58 26 .75 39 54 31 3
4-Chlorophenylphenyl ether ug/l 50 .00 28 .18 32 .41 56 65 14
Chrysen ug/l 50 .00 32 .13 35 .38 64 71 10
Dibenz(:,h) anthracene ug/l 50 .00 31 .43 35 .65 63 71 1 3
Date :08/26/03 Page ;14 of 19
1 airgralory Carl fulion IDS REPORT OF LABORATORY ANALYSIS Lahoralon, Certrhuthen ID
NC Wastewater 12 KY Drinking Water 90090
NG Drinkutij Water 37706 Thes report shall not be reproduced, except in lull.VA Drinking Water 213
SC 99OD6 wrinout the widen consent of Pam Anatntical Semites, Inc . FL NELAP E87627
Pace Analytical $eivices, Inc .
MKinmAvenue, Suite 100
Hunhitswile NC28078aceAnalyficalPhone.,704.875,9M
wm.parcelabs .ixim Fall.704.875.9091
QUALITY CONTROL DAT A
Lab Project Number :9248967
Client Project ID :03-JUL_0339/KI1356
LABORATORY CONTROL SAMPLE LCSD ; 923259709 923259717
Spike LCS LCSID LCS LCSID
Parameter Units Conc . Ressult Result ReC It Rec RPD Footnotes
Dibeoizof~an ug/1 50 .00 32 .78 37 .10 66 74 1 2
1 .2 -Dichlorobeauzene ug/1 50 .00 26 .15 29 .96 52 60 14
1,3-Dichlorobesizerte uq/1 50 .00 24 .76 28 .91 50 58 is
1,41-Dichlorobenteene uq/1 SO .00 24 .58 26 .74 49 58 16
3,31-Dichlorobemocidiner ug/1 100 .00 18 .59 19 .58 19 20 5 4
2,4-Dichloropherool ug/1 50 .00 24 .74 30 .09 so 60 19
Diethylphthalate uq/1 50 .00 18 .70 22 .20 37 44 17
2,4-Dimethylph=Ol ug/1 50 .00 21 .82 25 .89 44 52 17
Dimethylphthalate ug/1 50 .00 6 .526 7 .756 13 16 17
Di-n-butylphthalate ug/1 50 .00 23 .77 27 .28 48 55 14
4,15-Dinitro-2-mathylphrecull ug/1 50 .00 32 .44 35 .92 65 72 10
2,4-Dinitrophmol ug/1 50 .00 28 .22 31 .82 56 64 12
2,4-Dinitrotolume ug/1 50 .00 34 .66 39 .56 69 79 13
2,6-11initrotolene g/1 10,10 34,10 39,80 18 80 11
Di-n-octylphthalate ug/1 50 .00 27 .65 31 .27 55 62 12
1,2-Dipheazy1hydrazine,ug/1 50 .00 27 .62 31 .06 55 62 12
bia(2-Ethy1hexy1)Phtha1ate ug/1 50 .00 30 .89 34 .76 62 70 12
Pluoracrithene,ug/1 50 .00 28 .48 32 .34 57 65 13
Fluorene uq/1 50 .00 30 .51 34 .93 61 70 14
H"achloro-1,3-butadiene ug/1 50 .00 26 .05 29 .00 52 58 11
Hersetachlorobeloseenae ug/1 50 .00 35 .05 39 .73 70 80 13
Recicischlorocyclopentactiecue ug/1 50 .00 14 .44 19 .89 29 40 32 3
Heceachloroethazie uff/1 50 .00 24 .18 28 .31 48 57 16
inderno(1,2,21-ccl)pyrecrue ug/1 50 .00 33 .54 38 .16 67 76 13
loophorone ug/1 50 .00 32 .83 36 .53 66 73 11
2-Methyloutplotbalene ug/1 50 .00 28 .79 31 .92 58 64 10
2-Methylphenol (o-Cresol)ug/1 50 .00 17 .84 24 .04 36 48 30
U41-Methylphecool Ug/1 50 .00 15 .57 22 .73 31 46 37 3
Napluthaleme ug/1 50 .00 25 .31 27 .99 51 56 10
2-Nitroakailine ugf/1 50 .00 28 .36 32 .65 57 65 14
3-Nitroaxii1ine ug/1 50 .00 28 .32 35 .48 57 71 22
4-Nitroacrailine ug/1 50 .00 23 .69 30 .19 47 60 24
Nitroberucene,ug/1 50 .00 29 .55 32 .46 59 65 9
2-Nitrophenol ug/1 50 .00 26 .29 28 .92 53 58 10
4-Nitrophmol ug/1 50 .00 10 .56 15 .40 21 31 37 3
N-Nitrosodi-ethylamine ug/1 50 .00 13 .52 16 .85 27 34 22
N-Nitroso-di-a-propylmine ug/1 50 .00 22 .77 26 .52 46 53 1 5
Date ;08/26/03 Page :15 of 19
111b l .bonnoryIahnrAIDN Carl facatio REPORT OF LABORATORY ANALYSIS KY Drinking Water 9DD90NCWastewater 12
NC Drinking Water 37706 This report shall not be reproduced, except in full.VA Dnriking; Water 213
Sc 99006 without the written consent of Pace Analytical Sennoes . Inc. FL NELAP E87627
Pace Analytical SerWeles, Inc .9800 KinveyAwnive, Suite 100
Hunterskille,NC 28078aceAnalXical"Phone.[phone]
WilAirpaCelabs.Com FaK.704.875.9091
QUALITY CONTROL DATA
Lab Project Number :924896 7
Client Project ID : 03-JUL-0339/MI1356
LABORATORY CONTROL SAMPLE LCSD ; 923259709 923259717
Spike LCS LCSD LCS LCSD
Parameter units Conc .Result Result Rec Rei; RPD Footnotes
N-Nitrosodiphenylamine ug/l 50 .00 28 .15 32 .73 56 66 15
Perstachlorophenol ug/l 50 .00 31 .57 35 .69 63 71 12
Phemanthrene ug/l 50 .00 30 .01 34 .50 60 69 14
Phenvol ug/l 50 .00 9 .066 12 .44 is 25 31 3
Pyrene ug/l 50 .00 38 .62 45 .31 77 91 16
1,2,4-Trichlorobenzene ug/i 50 .00 25 .67 29 .26 51 58 13
2,4,5-Trichlorophenol ug/l 50 .00 32 .81 38 .55 66 77 16
2,41,6-Trichlorophenol ug/l 50 .00 29 .83 36 .07 60 72 19
Hitrobenzwe-d5 (S)49 55
2-Fluorobiphenyl (S) 50 58
Terphenyl-dl4 (S)74 85
Phenol-dS (S) is 24
2-Fluorophersol (S)22 33
2,4,6-Tribrcrophenol (S) 67 7 2
MATRIX SPIKE &MATRIX SPIKE DUPLICATE :923259733 92325974 1
923239040 Spike HS KSD MS MS D
Parameter Units Result Conic .Result Result %Rec Rec RPD Footnotes
Acenualphtherfe ug/i 0 50 .00 32 .48 30 .67 65 61 6
4-Chloro-3-methylphenal ug/l 0 50 .00 35 .69 27 .58 71 55 26
2-Chlorophenol ug/l 0 50 .00 27 .70 23.55 55 47 16
1,4-Dichlorobenzene ug/l a 50 .00 26 .16 28 .02 52 56 7
2,4-Dinitrotoluene ug/l 0 50 .00 40 .17 38 .43 80 77 4
4-Nitrophenol ug/l 0 50 .00 17 .76 14 .14 36 28 23
N-Nitroso-di-n-propylannine ug/l 0 50 .00 25 .71 26 .27 51 52 2
Pentachlorophenol ug/l 0 50 .00 36 .03 32.23 72 64 1 1
Phenol ug/I 0 50 .00 12 .99 10 .78 26 22 19
Pyrene ug/l 0 50 .00 46 .11 42 .73 92 86 8
1,2,4-Trichlorobenzene ug/I a 50 .00 28 .05 28 .74 56 58 2
Nitrobenzeri (S)54 55
2-Fluorobiphenyl (S) 57 55
Terphenyl-d14 (S) 88 83
Phefool-d5 (S) 25 21
2-Fluorophertol (S) 35 28
2,4,6-Tribromophenol (S) 75 7 0
Date :00/26/03 page :16 of 19
Laboratory Certification IDS REPORT OF LABORATORY ANALYSIS KY Drinking Water 9OD90NCWastewater 1 2
NC Drinking Water 37706 This annul Shall not be relpfoduced . except in full . VA Drariking Water 213
Sc 99OD6 earthout Me written consent of Pecs AnattliCal Semces, hic. FL NELAP E87627
Pecs Analytical Servicem,Inc.
,QWO Khtel, Awnue, Suite 100
Huntersinifie,AC28078ceAnaljftalPhone: 704 875 9092
WmAv.pacelabs .ccim Fax,704,8759091
QUALITY CONTROL DATA
Lab Project Nicobar :924896 7
Client Project ID :03-JUL_ 0339/MI1356
SAMPLE DUPLICATE :923259725
923239248 DUP
Parmetotr Units, Result Result RPD Footnotes
Aceatimplitheae Ug/l ND ED NC
Acoosphthyleme,US/1 ED ND NC
Aniline ug/l ED ED NC
Anthracerue ug/l ND ND KC
Bremato (a) anthraceme tig/l ND ED NC
Bwzo (a) pyrene ug/l ND ND KC
BeltzoWfluoravathene Uq/l ND ED KC
Benzo (9, la,i) PiarYlallloe Ug/l ND ND MC
Berazo (k)fluoranthene rag/l ED ED KC
Benzoic acid Ug/l ED ND HC
Bearyl alcohol ug/l HD ED NC
4-Br,,phmylphwyl other Ug/l ND ED NC
Butyllbenzy1plothalate ug/l ND ND NC
4-Chloro-3-methylphmol rag/l ED ED KC
4-Chloroaniline rag/l No ND NC
bis(2-Chloroethoxy)methme ug/l ND ED NC
bia(2-Chloroethyl) ether ug/l ND ED NC
bis(2-Chloroisopropyl) ether Ug/l ND ND KC
2-Chloronaphthaleme,Ug/l ED ND NC
2-Chlorophenol ug/l ND ND NC
4-Chlorophenylphenyl other ug/l ND ND NC
Chrysene rag/l ND ND NC
Dibenz (a, h)aumthracerve Ug/l ND ND NC
Dibmzofurm ug/l ND ND NC
1,2-Dichlorobenzene ug/l ND ND NC
1,3-Dictilorolneurizene,Ug/l ND ND NC
1,4-Dichlorolpenzene ug/l ED RD NC
3,21--Dichloroberizidine Ug/l ND ND NC
2,4-Dichlorophenol Ug/l ND ED NC
Diethylphthalate Ug/l ND ED NC
2,4-Dimethylphenol Ug/l ND ND NC
Dimethylphthalate rag/l ND ND KC
Di-n-butylphthalate Ug/l HD ND KC
4,6 .Dinitro-2-methylphenol Ug/l ND ND NC
2,4-Dinitrophenol ug/l ND ND NC
2,41-Dinitrotoluerme Ug/l ND ND NC
2,6-Dinitrotalume ug/l ND ND NC
txate~08/26/03 P .ge :f 19
40
1 Abotaloh, Cerldicahon IIapprabory Unification IN REPORT OF LABORATORY ANALYSIS KY Drinking Water 90MNGWastamter 1 2
NC Drinklog Water 37706 This region shall not be reproduvel, except in full.VA Drinking Water 213
SO 99MG without the written consent of pace Anallfical Semices . Inc FL NELAP E87627
leeve Anaffirfical Serinfees, Inc.
W Kincey Aventur, Suite 100
Hunel NC 28078aceAnalyfical'Phone.,704.875.9M
M-Avidacefigibs.cont Fv.*704.875.9091
QUALITY CONTROL DATA
Lab Project Number :924896 7
Client Project ID :03-JUL_0339/MI1356
SAMPLE DUPLICATE :923259725
923239248 DUT
Parameter Units Result Result gPD Footnotes
Di .n.octyliplathislate ug/1 No No NC
1,2-Dipheary1hYdritzine ug/1 No No NC
bis(2-Ethy1heXY1)phtha1ate ug/l No No NC
Flucraurtheme,ug/1 No ND NC
Fluorites,ug/1 No ND NC
Heicachloro-1,31-butaidieue ug/1 No No NC
H"achlorobeloazemer ug/1 ND No KC
Heacrachlorocycloplontadiencle ug/1 ND No KC
Heasuachloroetharte,ug/1 No No NC
Indemno(l, 2,3-cd)pyrene ug/1 No No NC
Iscaphorodue ug/1 No No NC
2-Methylinaphthaleole ug/1 ND ND NC
2-Metbylphaddial (o-Cresol)ug/1 ND ND KC
3fi4-MGthy1Phed01 ug/1 No No NC
Naphthalsole uq/1 No NI)NC
2-Nitrositailifirs ug/1 No ND NC
3-Nitroarxiline ug/1 ND No NC
4-Nitroariline,ug/1 No No NC
Nitroberizene ug/1 No ND KC
2-Nitropherval ug/1 NU No KC
41-Nitropheal ug/1 No ND KC
N-NitroaxactimethYlamine ug/1 ND ND KC
N-Mitroso-di-n-propylanine ug/1 ND No NC
N-Nitrostodiphertylappine ug/1 No No NC
Pentachlorophenol ug/1 ND ND NC
Phatianthristrue,ug/1 No No NC
Phei ug/1 No ND KC
Pyrene ug/1 No No KC
1,2,4-Trichlorobanzens ug/1 ND No NC
2,4,5-Trichlorophenol ug/1 ND No NC
2,4,6-Trichlorophanol ug/1 ND No NC
Nitrobenzene-ciS (S) % se 6 2
2-Fluorobiphenyl (S) % 58 61
Terphenyl-c114 (S) % 99 9 6
Phenci (S) % 0 0 5
2-Fluarophenol (S) % 1 0 5
2,4,6-Tribrom,cpheriol (S) Is 13 11 5
Date :08/26/03 page :is Of 19
0
1 ingrunry Certification IREPORT OF LABORATORY ANALYSIS KY Drinking Water 90090NCWastewater 1 2
NC Drinking Water 37706 This report shall not be reproduckno, except in full .VA Drinking Water 213
SC 9M whout the widen count of Pace Analytical Serlices, Im FL NELAP E87627
Pace mallincal services,Inc.9&T Kincey Avenue, Suite 100
Huntersville,NC 28078OAnalj&al Phone.,704.875.M
FaK.704.875.9091
Lab Project Number :9248967
Client Project ID : 03-JUL-0339/MI1356
QUALITY CONTROL DATA PARAMETER FOOTNOTE S
Consistent with EPA guidelines, unrounded concentrations are displayed and have been used to calculate %Rec and RPD values .
LCS(D)Laboratory Control sample (Duplicate )
MS(D)Matrix Spike (Duplicate)
DUP Bowls Duplicate
ND Not detected at or above adjusted reporting limit
MC Not Calculabl e
J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
NDL Adjusted Method Detection Limi t
RPD Relative Percent Difference
(S)Surrogate
ill Recovery falls outside of QC limits, however, this compound is not found in the associated samples .
(21 The calculated RPID was outside QC acceptance limits .
[31 R?D value was outside control limits, however both percent recoveries were acceptable . Sample results for the
QC batch were accepted based on percent recoveries and completeness of QC data .
[4) The surrogate and/or spike recovery was outside acceptance limits .
Is)The surrogate recovery was outside QC acceptance limits due to matrix interference .
Date :08/26/03 Page :19 of 1 9
Laboratory Ced ficathur IDs REPORT OF LABORATORY ANALYSIS Labor,t,N Certification 10
MC Wastewater 12 KY Drinking Water 90090
NC Drinking Water 37706 This report shall not be reproduced . except in full.VA Drinking Water 213
&C 99D06 wrthout the written consent of Pace AnaMical SeNices, Inc . FL NELAP E87627
CHAIN OF CUSTODY RECOPAND ANALYSIS REQUEST FORM 0
3611I ~ -7nalyticalLaboratory Services iDuke----------------------!-i~ "Pag eMail Code MG03A2 (Building 7405)--%-0 1
?DwEnergy.13339 Hagers Ferry Rd DISTRIBUTIO N
For Detailed Instructions, see : Hunteraville,N . C. 28078 ORIGINAL to LAB,
[phone] COPY to CLIENT
http://de~1essenv/coc/Fa..............E-IFLDIM~M ............
liProject Name 2)Phome No : 075-5257
BURLINGTON MGP (SAPROLITE WELLS)
E 3)Cliont C .Campbell R . Roberts 4)Fax No:875-503 2
t
C/ 3=
y"=11 a
SiBusiness Unit: 20018 6)Proce"; 7)RiwF,,To:0193 in
010:MGPBURL DiActivity,ID : ALLACTV 10)Mall Code:M003A3 alCustomer t complete all
c r
SI4ADFD Areas .M 2
14CO .0 0 w 0 1
LAB USE ONLY "Chem Ilection Information NE 0 < < 0
i "Labli)i Desktop No . "Sample Description or ID Date Time Signature 0 0 Q.te::2 z 2 w w 01 1.0c23oPMWB-D -7 4 Y103 1 -1 05 0 X 1 1 3 1 6
PMWC-D x 1 1 3 1"7 405,4 60PMWF-D ".a2.2 16 ;L5~x 1 1 3 1 6
! z PM WIr G-D 7 (PL"c 11-55 X x 1 1 3 1 6
1 0
6PMwI431xitaijr-b-C.44IJ x 1 1 3 1
PMWL-D -7/Vf M Oct 1!;-l x 1 1 3 1 6
2
E0
E
customer to sign date below
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............................
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Other
Add .Cost Will Apply
IkDuke Duke Energy Analytical Laboratory
Phone. [phone] ~ax 704-875-5038#Energy.13339 Hagers Ferry Road Huntersville .NC 28078-7929
mcGuire Nuclear Complex - MG03A 2
C4--rtiflcate Of Analysi s
New York State Department of Health Certification 9 11717
Oklahoma Department of Environmental Quality Certification N 9930
Kansas Department of Health and Environment Certificate # E-1031 1
North Carolina Department of Health &Human Services Certification # 378D4
South Carolina (DHEC)Laboratory ID # 991306 North Carolina (DENR) Certification M 248
Z~L
SamptelD#:23024515 Job#:03-JUL-0337
Sample Description :PMWB-D (SAPROLITE WELLS )
~.ollection Date : 24-Jul-0314 :16 :00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
~,EGP:7~,~~METIERS IN WATER BY GCINIS - 826 0
Test Code : MS8260MGPW Test Method: SW-846 603013/826013 Date Posted :07128103
Result Reporting Limit Reg
Benzene 52 pg/L 0.50 P911-0
Toluene 1 .9 pg/L 1 .0 pg/L 0
Ethylbenzene 24 P911.1 .0 pg/L 0
m-p-Xylone 10 Vg/L 2.0 Pall.0
16 pgfL 1 .0 pg/L 0
SamplelD#: 23024516 Job#:03-JUL-033 7
Sample Description :PMWC-D (SAPROLITE WELLS )
on Date :22-Jul-03 16:05 :00 Site : BURLINGTON Sample Type : MGP SITE Desktop #
OGIP PARAMETERS IN WATER BY GCIMS - 8260
Test Code : MS8260MGPW Test Method : SW-846 5030B18260B Date Posted :07/28103
Result Reponting Limit Flag
Benzene 11 pg/L 10 pg1L 0
Toluene <20 Pa 20 pg/L 0
Ethylbenzene 69 pg/L 20 lig[L 0
m-p-Xylene <40 Pg/L 40 pgfL 0
28 $WL 20 pgtL 0
Sample ID #: 23024517 Job#:03-JUL-033 7
Sample Description :PMWF-D (SAPROLITE WELLS )
Collection Date: 22-JuI-03 16 :25 :00 Site :BURLINGTON Sample Type :MGP SITE Desktop #
Test Code : MS8260MGPW Test Method : SW-846 5030B/8260B Date Posted :07128/03
Resuft __~~eporfinq ml Flag
Benzene 0 .82 Vg/L 0 .50 pg1L 0
Toluene 5 .6 pgfL 1 .0 pg/L 0
Ethylbenzene 30 pg/L 1 .0 pg[L 0
is in-It-Xylene 13 pg/L 2.0 pgfL 0
Visit w cin the IntntN4 at
,ps, (;Cwm~www]15:12.0t hffpj/d~/e=nvAab-sin,/P~ 0 1 rj
D
.
uke Duke Energy Analytical Laboratory
Phone .[phone] Fax [phone]Nnerg.13339 Hagers Ferry Road Huntersville,NC 28078-7929
McGuire Nuclear Complex - MG03A 2
Cartificate af Analysi s
New York State Department of Health Certification N 11717
Olklahoma Department of Environmental Quality Cerlificabon 4 993D
Kansas Department of Health and Environment Certificate # E-1031 1
North Carolina Department of Health &Human Services Certification #3780 4
South Carolina (DHEC)Laboratory ID 4 99DOS North Carolina (DENR) Certfication 4 248
SamplelD#:23024517 Job#:03-JUL-033 7
Sample Description :PMWF-D (SAPROLITE WELLS )
Collection Date : 22-Jul-03 16 :25:00 Site :BURLINGTON Sample Type: MGP SITE Desktop #
Test Code : MS8260MGPW Test Method : SW-846 503OB18260B Date Posted :07128/03
Resuft Reporting Limit Fla g
16 Vg/L 1 .0 Vg/L 0
SamplelD#: 23024518 Job#:03-JUL-033 7
Sample Description :PMWG-D (SAPROLITE WELLS )
Collection Date : 22-Jul-03 11 :55 :00 Site :BURLINGTON Sample Type: MGP SITE Desktop #
P PARAMETERS IN WATER BY GCIMS - 8260
st Code: MS8260MGPW Test Method : SW-846 5030B18260B Date Posted :07128103
Result Reporting Limit Fla g
Benene 0.54 pg/L 0.50 WgIL 0
Toluene < 1 .0 pgVL 1 .0 PA 0
Ethylbe=ne I I Vil/l . 1 .0 pg/L 0
M-p-Xylerne <2.0 pg[L 2.0 VgA.0
2.2 pg/L 1 .0 MIL 0
Sarni 23024519 Job#:03-JUL-033 7
Sample Description :PMWI (SAPROLITE WELLS )
Collection Date: 21-Jul-03 16 :25:00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
Test Code : MS8260MGPW Test Method : SW-846 5030B18260B Date Posted :07128103
Remit ReportiN Limit Flag
Bamene < 0.50 pq/L 0 .60 pg1L 0
Toluene < 1 .0 pg/L 1 .0 ptill . 0
Ethylbenzene < 1 .0 pg/L 1 .0 pg1l . 0
m-p-Xylene <2.0 pg/L 2 .0 pgtL 0
O-Xylene < 1 .0 pg/L 1 .0 pg/L 0
Visit us m the ineniNla at P~I 2 .f 3Mwtile) 15:22:M hhp://de~/eswnvAab-srv/
Duke Duke Energy Analytical Laborator y
Phone [phone] ~ay 704-875-5038Nnety.13339 Hagers Ferry Road Huntersville .NC 28078-7929
McGuire Nuclear Complex - MG03A2
CiBirstificate of Analysis
New York State Department of Health Certification Af 11717
Oklahoma Department of Environmental Quality Certification 1) 9930
Kansas Department of Health and Environment Certificate A$ E-1031 1
North Carolina Department of Health &Human Sermces Certification # 37804
South Carolina (DHEC)Laboratory ID # 99006 North Carolina (DENR) Certification #248
SamplelD#: 23024520 Jobif :03-JUL-033 7
Sample Description :PMWL-D (SAPROLITE WELLS )
Collection Date : 24-Jul-03 09 :45 :00 Site BURLINGTON Sample Type : MGP SITE Desktop #
Test Code : MS8260MGPW Test Method: SW-846 5030B18260B Date Posted :07128103
Resuft -Reporting Limit Flag
Benzene < 0 .50 pg/L 0.50 PgIL 0
Toluene < 1 .0 pg/L 1 .0 pVL 0
Ethylbenzene < 1 .0 pq/L 1 .0 pg[L 0
rn-p-Xylene <2 .0 pg/L 2 .0 pg/L 0
o-Xylene < 1 .0 pg/L 1 .0 pg1l. 0
------------------------------------
Qlatscripitian cA Flags :
Aln Analytical ~o-dlur, Wers, Met
se Case Nar'sce .
Estimated Co-centralion .lias Cam Atanswahat
3 -Reinert ~-,. Ele-ted dae, 1. asuff-tere,.-,I ..-nl
4 -Repass ~mit Elevated obso to rec,aired stowlybcal stimics,
5 -Sareple Remits should 2,T.t Be Used For Reaulator, PurposesMs. Case
6 -A.Wa.detested b0asa tswle .esdcs~ reaches ., ]-.1 chartere d
7 -Reported concentration is she combinesion of more that one asoclor .
Rjpjntd attar ne highest can c .ntr .tic. in 'he earlist)_
14
aM Reported B),Dale
Visit us on the IntraNd at
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August 13, 2003 5 :29 :19 PM Page #1 ot'l
Duke Trace Metals
OvkEnergy.Case Narrativ e
(This document must accompany release ofAnalytical Data)
----------------------- -------------------------------- - -------------------------------------------------- - ------------ --------------------------- --------------------------------
03-JUL-0337,0*
LIMS Job #03-JUL-0338
03-JUL-033 9
Worklist #03-JUL-071 9
•Iron was analyzed in the method blank by ICP above the reporting limit . The
concentration of Fe was 0 .054 mg/L compared to the reporting limit of 0 .010
mg/L .
• All other QC associated with this data set is acceptable .
•The concentration of iron in Sample #23024518 is between 5 and 10 times
that contained in the blank . Therefore, this result should be considered an
upper limit of the true concentration and should be used with caution .
•For sample 23024535,the concentration of iron in the sample is at a level
below 5 times that contained in the blank . This result must be considered to
be suspect .
• All other samples contain iron in concentrations greater than 10 times that
contained in the blank . Therefore, those results are acceptable .
•The data may be reported to the client with the above qualifications .
kil ----------
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Laboratory Services---------- D--u--k-e--*E--n,-e- -r-9--y- -A---n-a--1y--t-i c- -a--1 ------------------
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Phone: [phone] Hagers Ferry Road
FAK 704-875-50M Htnitersvile NC 2BO78-7929
0 .0 q
CHAIN OF CUSTODY RECORD AND ANALYSIS REQUEST FORM---------I
nalytical Laboratory Services iDuke--------------------------"'Page k ofMail Code MG03A2 (Building 7405)J-DISTRIBUTIO NIdwrEnergy..13339 Hagers Ferry Rd ORIGINAL to LAB,For Detailed Instructions, see : Hunteraville,N . C. 28078
(704)87S .5245 COPY to CLIENThItpJ/de~/assenv/cocl Far.............. ..C7U4 8L5-.qq:Lk ............
I)Project Name 2)Phone No :075-5257BURLINGTONMGP (SAPROLITE WELLS)Z
E 3)CHeNt C .Campbell R . Roberts 4)Fax No :875-5032 P se".1 .C
2-H 0, 3=H >
4 =
5)BuslnessUnIt : 20018 6)Pr .c.ss:7)Resp .To: 0193 G
S)Pml.~t ID :MGPBURL 9)A .tlsity ID : ALLACTV IO)MallCM@ :MG03A3
te all
cc
0
LAB USE ONLY 12 Chem "Collection Information IE
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1~~)3a3g'7-79 PMWB-D i ~I -t 0;X -10 .- x i 1 3 ~I
-7 /U/O ;~ 0.5-j!'.ja X I I 1 1 3 1 6
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913J 89(D-)-PMVVL-D -7jjqj0-;gq~(C J,'jo~X 1 1 1 1 3 1 00 6
0.
E
3
Customer to sign &date below
2I)Relinquished By Datarl"Tme
uRequested Turnaround
14 Days I/as as
Ea 7 Days
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Other* Add .ost Ill Ap*
CHAIN OF CUSTODY RECORD AND ANALYSIS -REQUEST FORM .-
Analytical Laboratory Services iDuke----- - * -----------------------------
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DISTRIBUTIO NIftdrEnergy.13339 Hagers Fe"Rd ORIGINAL to LAB,Hunteraville,N. C . 2807 8Fof Detailed Instnuctions,see:(704)876-S245 COPY to CLIENT
hUpJ/dew~w/assenv/cocl Fa .(7 4)2LS~jq:L~............
I)Projed Name 2)Phons No :$75-52S7
BURLINGTONMGP(SAPROLITE WELLS)
E 3)Cllent C .Campbell R . Roberts 4)Fax No :37S_S032 P
Zw V,4-n
4.1
SiSusin"s Unit:20018 6)Process : 7)Aesp.To:0193
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13Sa 43 0"Lablo I Desktop No . mple Description or ID Date Time sicinature,1:: z 1 01
PIAWB-D _X 1 1 3 1 6
x 1 1 3 1 6PIVIVVC-D 7 1405, ce~l XPMVVF-D ;Lsr A X I 1 3 1
E PMWG-D X 1 1 3 1 6
PMWI L,~X 1 1 3 1 6
X I 1 6PMWL-D 3
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23)!Received by : BE '48HrDate/Time:'7/~2/oA U it >-a
ILL
Add .Cost Will Apply
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100eacmnalyticalHuntersville,AIC 28078
Phone :[phone]
www.pacelabs.com Fax:[phone]
August 26 . 2003
Mr . Jay Perkins
Duke Powe r
13339 Hagers Ferry Road
MG30A2
Huntersville .NIC 2807 8
RE : Lab Project Number :9248953
Client Project ID : 03-JUL-0337/MI1356
Dear Mr . Perkins :
Enclosed are the analytical results for sample(s) received by the laboratory on August 13 . 2003 .Results
reported herein conform to the most current NELAC standards . where applicable . unless otherwise narrated in the
body of the report .
If you have any questions concerning this report please feel free to contact me .
Sincerely ,
Kristi Tart
Kristi .Tart@pacelabs .com
Project Manager
Enclosures
1 aboratory CertificatiQn ID_~REPORT OF LABORATORY ANALYSIS Labgralory Certification !Ds
NG Wastewater 12 LA Wastewater 04034
NC Drinking Water 37706 This report shall not be reproducea, except in full, VA Drinking Water 213
SG 99006 without the written consent of Pace Analytical Services, Inc Ft-NELAP E87627
Pace Analytical Services, Inc .
9800 Kincey Avenue, Suite 100acmnalyticiHuntersville,NC 28078
Phone:[phone]www.pacelabs .com Lab Project Number :9248953 Fax.[phone]
Client Project ID :03-JUL-0337/MI1356
Lab Sample No :923238778 Project Sample Number :9248953-001 Date Collected : 07/24/03 14 :15
Client Sample ID :23024515/PMWB-D Matrix : Water Date Received :08/13/03 12 :05
Parameters Results Units Report Limit Analyzed By CAS No . Qual ReqLmt
GUMS Semivolatile s
Semivolatile Organics Prep/Method :EPA 8270
Acenaphthene 180 ug/l so . 08/25/03 16 :39 BET 83-32-9
Acenaphthylene NO ug/l 10 . 08125/03 16 :39 BET 208-96-8
Aniline NO ug/l 10 . 08/25/03 16 :39 BET 62-53-3
Anthracene 11 . ug/l 10 . 08/25/03 16 :39 BET 120-12-7
Benzo(a)anthracene NO ug/l 10 . 08/25/03 16 :39 BET 56-55-3
Benzo(a)pyrene NO ug/l 10 . 08/25/03 16 :39 BET 50-32-8
Benzo(b)fluoranthene ND ug/l 10 . 08/25/03 16 :39 BET 205-99-2
Benzo(g,h .i)perylene ND ug/l 10 . 08/25/03 16 :39 BET 191-24-2
Benzo(k)fluoranthene NO ug/1 10 . 08/25/03 16 :39 BET 207-08-9
Benzoic acid ND ug/l 50 . 08/25/03 16 :39 BET 65-85-0
Benzyl alcohol NO ug/l 20 .08/25/03 16 :39 BET 100-51-6
4-Bromophenylphenyl ether NO ug/l 10 . 08/25/03 16 :39 BET 101-55-3
Butylbenzylphthalate NO ug/l 10 . 08/25/03 16 :39 BET 85-68-7
4-Chloro-3-methylphenol NO ug/l 20 .08/25/03 16 :39 BET 59-50-7
4-Chloroaniline NO ug1l 20 .08/25/03 16 :39 BET 106-47-8
bisl2-Clloroethoxylmethane NO ug/l 11, 08/25103 16 :39 BET 111,11,1
bis(2-Chloroethyl) ether NO ug/l 10 . 08/25/03 16 :39 BET 111-44-4
bis(2-Chloroisopropyl) ether IND ug/l 10 . 08/25/03 16 :39 BET 39638-32-9
2-Chloronaphthalene ND ug/l 10 . 08/25/03 16 :39 BET 91-58-7
2-Chlorophenol IND ug/l 10 . 08/25/03 16 :39 BET 95-57-8
4-Chlarophenylphenyl ether NO ug/l 10 . 08/25/03 16 :39 BET 7005-72-3
Chrysene NO ug/l 10 08/25/03 16 :39 BET 218-01-9
Dibenz(a .h)anthracene NO ug/l 10 . 08/25/03 16 :39 BET 53-70-3
Dibenzofuran 17 . ug/l 10 . 08/25/03 16 :39 BET 132-64-9
1 .2-Dichlorobenzene NO ug/l 10 . 08/25/03 16 :39 BET 95-50-1
1 .3-Dichlorobenzene NO ug/l 10 . 08/25/03 16 :39 BET 541-73-1
1,4-Dichlorobenzene NO ug/1 10 . 08/25/03 16 :39 BET 106-46-7
3 .3'-Dichlorobenzidine IND ug/I 20 .08/25/03 16 :39 BET 91-94-1
2 .4-Dichlorophenol ND ug/1 10 . 08/25103 16 :39 BET 120-83-2
Diethylphthalate IND ug/l 10 . 08/25/03 16 :39 BET 84-66-2
2,4-Dimethylphenol IND ug/l 10 . 08/25/03 16 :39 BET 105-67-9
Dimethylphthalate IND ug/1 10 . 08/25/03 16 :39 BET 131-11-3
Di-n-butylphthalate ND ug/l 10 . 08/25/03 16 :39 BET 84-74-2
4 .6-Dinitro-2-methylphenol IND ug/l 50 . 08/25/03 16 :39 BET 534-52-1
2 .4-Dinitrophenol ND ug/l 50 . 08/25/03 16 :39 BET 51-28-5
2,4-Dinitrotoluene ND ug/l 10 . 08/25/03 16 :39 BET 121-14-2
2 .6-Dinitrotoluene ND ug/l 10 . 08/25/03 16 :39 BET 606-20-2
Date 08/26/03 Page :I of 1 3
Laboratory Certification I Ds REPORT OF LABORATORY ANALYSIS Laboratory Ce[tification IDs
NC Wastewater 12 LA Wastewater 04034
NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213
SC 99006 w1hout the written consent of Pace Analytical Services, Inc . FL NFLAP E87627
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
a ceAna al"Huntersville,NC 28078
Wild Phone:[phone]www.pacelabs .com Fax:[phone]Lab Project Number :924895 3
Client Project ID :03-JUL-0337/MI135 6
Lab Sample No :923238778 Project Sample Number :9248953-001 Date Collected : 07/24/03 14 :15
Client Sample ID :23024515/PMWB-D Matrix : Water Date Received :08/13/03 12 :05
Parameters Results Units Report Limit Analyzed By CAS No . Dual ReqLmt
Di-n-octylphthalate ND ug/l 10 . 08/25/03 16 :39 BET 117-84-0
1 .2-Diphenylhydrazine IND ug/l 20 .08/25/03 16 :39 BET 122-66-7
bis(2-Ethylhexyl)phthalate KID ug/l 10 . 08/25/03 16 :39 BET 117-81-7
Fluoranthene RD ug/l 10 . 08/25103 16 :39 BET 206-44-0
Fluorene 39 . ug/l 10 . 08/25/03 16 :39 BET 86-73-7
Hexachloro-1 .3-butadiene ND ug/l 10 . 08/25/03 16 :39 BET 87-613-3
Hexachlorobenzene IND ug/l 10 . 08/25/03 16 :39 BET 118-74-1
Hexachlorocyclopentadiene ND ug/l 10 . 08/25/03 16 :39 BET 77-47-4
Hexachloroethane ND ug/l 10 . 08/25/03 16 :39 SET 67-72-1
Indeno(l .2 .3-cd)pyrene IND ug/l 10 . 08/25/03 16 :39 BET 193-39-5
Isophorone IND ug/l 10 . 08/25/03 16 :39 BET 78-59-1
2-Methylnaphthalene 60 . ug/l 10 . 08/25/03 16 :39 BET 91-57-6
2-Methylphenol (o-Cresol)IND ug/l 10 . 08/25/03 16 :39 BET 95-48-7
3&4-Methylpheriol K) ug/l 10 . 08/25/03 16 :39 BET
Naphthalene 270 ug/l 50 . 08/25/03 16 :39 BET 91-20-3
2-Nitroaniline IND ug/l 50 . 08/25/03 16 :39 BET 88-74-4
3-Nitroaniline IND ug/l 50 . 08/25/03 16 :39 BET 99-09-2
4-Nitroaniline ND ug/l 50 . 08/25/03 16 :39 BET 100-01-6
Nitrobenzene IND ug/l 10 . 08/25/03 16 :39 BET 98-95-3
2-Nitrophenol IND ug/l 10 . 08/25/03 16 :39 BET 88-75-5
4-Nitrophenol IND ug/l 50 . 08/25/03 16 :39 BET 100-02-7
N-Nitrosodimethylamine ND ug/l 10 . 08/25/03 16 :39 BET 62-75-9
N-Nitroso-di-n-propylamine ND ug/l 10 . 08/25/03 16 :39 BET 621-64-7
N-Nitrosodiphenylamine ND ug/l 10 . 08/25/03 16 :39 BET 86-30-6
Pentachlorophenol IND ug/l 50 . 08/25/03 16 :39 BET 87-86-5
Phenanthrene 53 . ug/l 10 . 08/25/03 16 :39 BET 85-01-8
Phenol ND ug/l 10 . 08/25/03 16 :39 BET 108-95-2
Pyrene IND ug/l 10 . 08/25/03 16 :39 BET 129-00-0
1 .2 .4-Trichlorobenzene RD ug/l 10 . 08/25/03 16 :39 BET 120-82-1
2,4 .5-Trichlorophenol ND ug/l 50 . 08/25/03 16 :39 BET 95-95-4
2,4 .6-Trichlorophenol IND ug/l 10 . 08/25/03 16 :39 BET 88-06-2
Nitrobenzene-d5 (S)54 % 08/25/03 16 :39 BET 4165-60-0
2-Fluorobiphenyl (S) 59 % 08/2S/03 16 :39 BET 321-60-8
Terphenyl-c!14 (S)74 % 08/25/03 16 :39 BET 1718-51-0
Phenol-d5 (S) 1 % 08/25/03 16 :39 BET 4165-62-2 1
2-Fluorophenol (S)2 % 08/25/03 16 :39 BET 367-12-4 1
2,4 .6-Tribromophenol (S) 6 % 08/25/03 16 :39 BET I
Date Extracted 08/19/03 08/19/03
Date 08126/03 Page : 2 of 1 3
Laboratory GCrlifi~ajign IDs REPORT OF LABORATORY ANALYSIS Laboratory Q~rtification IDs
NC Wastewater 12 LA Wastewater 04034
NG Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213
SC 99006 without the written consent of Pace Analytical Services . Inc . FL NELAP E87627
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100eaceAnalyficalaHuntersville,NC 28078
www.pacelabs .com Phone :[phone]
Lab Project Number :9248953 Fax.,704 .875 .9091
Client Project ID : 03-JUL-0337/MI135 6
Lab Sample No :923238802 Project Sample Number :9248953-002 Date Collected : 07/24/03 09 :45
Client Sample ID : 23024520/PMWL-D Matrix : Water Date Received :08/13/03 12 :05
Parameters Results Units Report Limit Analyzed By CAS No . Qual ReqLm t
GUMS Setnivolatile s
Searivolatile Organics Prep/Method :EPA 827 0
Acenaphthene ND ug/l 10 . 08/20/03 16 :46 BET 83-32-9
Acenaphthylene ND ug/l 10 . 08/20/03 16 :46 BET 208-96 .8
Aniline NO ug/l 10 . 08/20/03 16 :46 BET 62-53-3
Anthracene NO ug/l 10 . 08/20/03 16 :46 BET 120-12-7
Benzo(a)anthracene NO ug/l 10 . 08/20/03 16 :46 BET 56-55-3
Benzo(a)pyrene ND ug/l 10 . 08/20/03 16 :46 BET 50-32-8
Benzo(b)fluoranthene IND ug/l 10 . 08/20/03 16 :46 BET 205-99-2
Benzo(g .h .i)perylene NO ug/l 10 . 08/20/03 16 :46 BET 191-24-2
Benzo(k)fluoranthene ND ug/l 10 . 08/20/03 16 :46 BET 207-08-9
Benzoic acid ND ug/l 50 . 08/20/03 16 :46 BET 65-85-0
Benzyl alcohol NO ug/l 20 .08/20/03 16 :46 BET 100-51-6
4-Bromophenylphenyl ether NO ug/1 10 . 08/20/03 16 :46 BET 101-55-3
Butylbenzylphthalate NO ug/1 10 . 08/20103 16 :46 BET 85-68-7
4-Chloro-3-methylphenol NO ug/1 20 .08/20/03 16 :46 BET 59-50-7
4-Chloroaniline NO ug/l 20 .08/20/03 16 :46 BET 106-47-8
bis(2-Chloroethoxy)methane NO ug/l 10 . 08/20/03 16 :46 BET 111-91-1
bis(2-Chloroethyl) ether NO ug/l 10 . 08/20/03 16 :46 BET 111-44-4
bis(2-Chloroisopropyl) ether NO ug/1 10 . 08/20/03 16 :46 BET 39638-32-9
2-Chloronaphthalene NO ug/l 10 . 08/20/03 16 :46 BET 91-58-7
2-Chlorophenol NO ug/l 10 . 08/20/03 16 :46 BET 95-57-8
4-Chlorophenylphenyl ether NO ug/l 10 . 08/20/03 16 :46 BET 7005-72-3
Chrysene NO ug/l 10 . 08/20/03 16 :46 BET 218-01-9
Dibenz(a .h)anthracene NO ug/l 10 . 08/20/03 16 :46 BET 53-70-3
Dibenzofuran NO ug/l 10 . 08/20/03 16 :46 BET 132-64 .9
1 .2-Dichlorobenzene NO ug/l 10 . 08/20/03 16 :46 BET 95-50-1
1 .3-Dichlorobenzene NO ug/l 10 . 08/20/03 16 :46 BET 541-73-1
1 .4-Dichlorobenzene NO ug/l 10 . 08/20/03 16 :46 BET 106-46-7
3 .3'-Dichlorobenzidine NO ug/l 20 .08/20/03 16 :46 BET 91-94-1
2 .4-Dichlorophenol NO ug/l 10 . 08/20/03 16 :46 BET 120-83-2
Diethylphthalate NO ug/l 10 . 08/20/03 16 :46 BET 84-66-2
2 .4-Dimethylphenol NO ug/l 10 . 08/20/03 16 :46 BET 105-67-9
Dimethylphthalate NO ug/l 10 . 08/20/03 16 :46 BET 131-11-3
Di-n-butylphthalate NO ug/l 10 . 08/20/03 16 :46 BET 94-74 .2
4 .6-Dinitro-2-methylpheriol NO ug/l 50 . 08/20/03 16 :46 BET 534-52-1
2 .4-Dinitrophenol NO ug/l 50 . 08/20/03 16 :46 BET 51-28-5
2 .4-Dinitrotoluene NO ug/l 10 . 08/20/03 16 :46 BET 121-14-2
2 .6-Dinitrotoluene ND ug/l 10 . 08/20/03 16 :46 BET 606-20-2
Date :08126/03 Page :3 of 1 3
Laboratory Certification ID Laboralgry Certification I
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS _D~
NC Drinking Water 37706 This report shall not be reproduced, except in full,LA Wastewater 04034
VA Drinking Water 21 3SC 99006 without the written consent of Pace Analytical Services, hic, FL NELAP E87627
Pace Analytical Services, Inc .
9800 Kincey Avenue, Suite 1005ceAnalyficaloHuntersville,NO 28078
Phone:[phone]
www.pacelabs.com
Lab Project Number :9248953
Fax:[phone]
Client Project ID :03-JUL-0337/1111356
Lab Sample NO : 923238802 Project Sample Number :9248953-002 Date Collected: 07/24/03 09 :45
Client Sample ID :23024520/PMWL-D Matrix : Water Date Received :08/13/03 12 :05
Parameters Results Units Report Limit Analyzed By CAS No . Qual ReqLm t
Di-n-octylphthalate ND ug/l 10 . 08/20/03 16 :46 BET 117-84-0
1 .2-Diphenylhydrazine NO ug/l 20 .08/20/03 16 :46 BET 122-66-7
bis(2-Ethylhexyl)phthalate ND ug/l 10 . 08/20/03 16 :46 BET 117-81-7
Fluoranthene NO ug/l 10 . 08/20/03 16 :46 BET 206-44-0
Fluorene NO ug/l 10 . 08/20/03 16 :46 BET 86-73-7
Nexachloro-1 .3-butadiene NO ug/l 10 . 08/20/03 16 :46 BET 87-68-3
Hexachlorobenzene ND ug/l 10 . 08/20/03 16 :46 BET 118-74-1
Hexachlorocyclopentadiene ND ug/l 10 . 08/20/03 16 :46 BET 77-47-4
Hexachloroethane NO ug/l 10 . 08/20/03 16 :46 BET 67-72-1
lndeno(I .2 .3-cd)pyrene NO ug/1 10 . 08/20103 16 :46 BET 193-39-5
IsophDrone ND ug/l 10 . 08/20/03 16 :46 BET 78-59-1
2-Methylnaphthalene NO ug/l 10 . 08/20/03 16 :46 BET 91-57-6
2-Methylphenol (o-Cresol)RD ug/l 10 . 08/20/03 16 :46 BET 95-48-7
3&4-Methylphenol ND ug/l 10 . 08/20/03 16:46 BET
Naphthalene NO ug/l 10 . 08/20/03 16:46 BET 91-20-3
2-Nitroaniline NO ug/l 50 . 08/20/03 16 :46 BET 88-74-4
3-Nitroaniline NO ug/l 50 . 08/20/03 16:46 BET 99-09-2
4-Nitroaniline ND ug/l 50 . 08/20/03 16 :46 BET 100-01-6
Nitrobenzene ND ug/l 10 . 08/20/03 16 :46 BET 98-95-3
2-Nitrophenol ND ug/l 10 . 08/20/03 16 :46 BET 88-75-5
4-Nitrophenol NO ug/l 50 . 08/20/03 16 :46 BET 100-02-7
N-Nitrosodimethylamine NO ug/l 10 . 08/20/03 16 :46 BET 62-75-9
N-Nitroso-di-n-propylamine NO ug/l 10 . 08/20/03 16 :46 BET 621-64-7
N-Nitrosodiphenylamine NO ug/l 10 . 08/20/03 16 :46 BET 86-30-6
Pentachlorophenol ND ug/l 50 . 08/20/03 16 :46 BET 87-86-5
Phenanthrene ND ug/l 10 . 08/20/03 16 :46 BET 85-01-8
Phenol NO ug/l 10 . 08/20/03 16 :46 BET 108-95-2
Pyrene NO ug/l 10 . 08/20/03 16 :46 BET 129-00-0
1,2 .4-Trichlorobenzene NO ug/l 10 . 08/20/03 16 :46 BET 120-82-1
2,4 .5-Trichlorophenol NO ug/l 50 . 08/20/03 16 :46 BET 95-95-4
2 .4 .6-Trichlorophenol NO ug/l 10 . 08/20/03 16 :46 BET 88-06-2
Nitrobenzene-d5 (S)49 X 08/20/03 16 :46 BET 4165-60-0
2-Fluorobiphenyl (S) 52 X 08/20/03 16 :46 BET 321-60-8
Terphenyl-dl4 (S) 89 % 08/20/03 16 :46 BET 1718-51-0
Phenol-d5 (S)22 % 08/20/03 16 :46 BET 4165-62-2
2-Fluorophenol (S) 32 % 08/20103 16 :46 BET 367-12-4
2 .4 .6-Tribromophenol (S) 79 % 08/20103 16 :46 BET
Date Extracted 08/19/03 08/19/0 3
Date :08/26103 Page : 4 f 1 3
I aboratory Ccrtifi~ation ID~REPORT OF LABORATORY ANALYSIS Laboratory Qertificalion ID~
NG Wastewater 12 LA Wastewater 04034
NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213
SC 99006 without the written consent of Pace Analytical Seivices . Inc . I'L NELAP E87627
Pace Analytical Services, Inc.
9800 Khocey Avenue, Suite 100acieAnalyfical"Huntersville,NC 28078
Phone :[phone]www.pacelabs.com
Lab Project Number :9248953 Fax.[phone]
Client Project ID : 03-JUL-0337/MI1356
PAPAMETER FOOTNOTES
Inorganic Wet Chemistry Analyses were performed at our Pace Asheville laboratory and Organic and Metals
testing was performed at our Pace Charlotte laboratory unless otherwise footnoted .
NO Not detected at or above adjusted reporting limit
NC Not Calculabl e
j Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MOIL Adjusted Method Detection Limi t
(5)Surrogat e
[I]Low surrogate recovery was confirmed as a matrix effect by a second analysis .
Date 08/26103 Page :5 of 1 3
Laboratory Certification IlDs REPORT OF LABORATORY ANALYSIS Laboratory Certification IDS
NC Wastewater 12 LA Wastewater 04034
NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213
SC 99006 without the written consent of Pace Analytical Services, Inc, Ft NELAP E87627
Pace Analyticai services, Inc .
9800 Kincey Avenue, Suite 100aneAnalyticaloHuntersville,NC 28078
www.pacelahs.com QUALITY CONTROL DATA Phone:[phone]
Fax:[phone]
Lab Project Number :924895 3
Client Project ID : 03-JUL-0337/MI1356
OC Batch :79954 Analysis Method :EPA 8270
QC Batch Method : Analysis Description : Semivolatile Organics
Associated Lab Samples :923238778 92323880 2
METHOD BLANK :92325969 1
Associated Lab Samples :923238778 923238802
Blank Reporting
Parameter Units Result Limit Footnotes
Acenaphthene Ug/l RD 10 .
Acenaphthylene Ug/l ND 10 .
Aniline Ug/l NO 10 .
Anthracene Ug/l NO 10 .
Benzo(a)anthracene Ug/1 NO 10 .
Benzo(a)pyrene ug/l NO 10 .
Benzo(b)fluoranthene ug/l NO 10 .
Benzo(g .h,i)perylene ug/l NO 10 .
Benzo(k)fluoranthene ug/l NO 10 .
Benzoic acid ug/l NO 50 .
Benzyl alcohol ug/l NO 20 .
4-Bromophenylphenyl ether ug/l NO 10 .
Butylbenzylphthalate ug/l NO 10 .
4-Chloro-3-methylphenol ug/1 NO 20 .
4-Chloroaniline ug/l ND 20 .
bis(2-Chloroethoxy)methane Ug/l NO 10 .
bis(2-Chloroethyl) ether ug/1 NO 10 .
bis(2-Chloroisopropyl) ether ug/1 NO 10 .
2-Chloronaphthalene ug/l NO 10-
2-Chlorophenol uq/1 NO 10 .
4-Chlorophenylphenyl ether ug/1 NO 10 .
Chrysene ug/1 NO 10 .
Dibenz(a .h)anthracene ug/1 NO 10 .
Dibenzofuran ug/l NO 10 .
1 .2-Dichlorobenzene Ug/l NO 10 .
1 .3-Dichlorobenzene ug/l NO 10 .
1 .4-Dichlorobenzene Ug/l NO 10 .
3 .3'-Dichlorobenzidine ug/l NO 20 .
2 .4-Dichlorophenol ug/l NO 10 .
Diethylphthalate ug/l NO 10 .
2,4-Dimethylphenol ug/l NO 10 .
Date :011126/03 Pa W :6 of 1 3
Laboratory Genification IN Laboratory Certification KD
INC Wastewater 12 REPORT OF LABORATORY ANALYSIS --5LAWastewater 04034
NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213Sc 99006 without the written consent of Pace Analytical Services, Inc . I'L NELAP E87627
Pace flWalytical Services, Inc.
9800 Kincey Avenue, Suite 100aneAnalyfical'Huntersville,NC 28078
www.pacelabs .com QUALITY CONTROL DATA Phone :[phone]
Fax-704 .875 .9091
Lab Project Number :924895 3
Client Project ID :03-JUL-0337/KI1356
METHOD BLANK :92325969 1
Associated Lab Samples :923238778 92323880 2
Blank Reporting
Parameter Units Result Limit -Footnotes
Dimethylphthalate ug/l ND 10 .
Di-n-butylphthalate ug/l NO 10 .
4,6-Dinitro-2-methylphenol ug/l NO 50 .
2 .4-Dinitrophenol Ug/l NO 50 .
2,4 .Dinitrotoluene ug/l ND 10 .
2 .6-Dinitrotoluene Ug/l NO 10 .
Di-n-octylphthalate ug/l NO 10 .
1,2-Diphenylhydrazine ug/l KID 20 .
bis(2-Ethylbexyl)phthalate Ug/l NO 10 .
Fluoranthene ug/l RD 10 .
Fluorene ug/l ND 10 .
Hexachloro-1 .3-butadiene ug/l NO 10 .
Hexachlorobenzene ug/l ND 10 .
Hexachlorocyclopentadiene ug/l NO 10 .
Hexachloroethane ug/1 ND 10 .
indeno(l .2 .3-cd)pyrene ug/l RD 10 .
Isophorone ug/l RD 10 .
2-Methylnaphthalene ug/l ND 10 .
2-Methylphenol (0-Cresol)ug/l ND 10 .
3&4-Methylphenol ug/l NO 10 .
Naphthalene ug/l NO 10 .
2-Nitroaniline Ug/1 RD 50 .
3-Nitroaniline ug/l NO 50 .
4-Nitroaniline ug/l ND 50 .
Nitrobenzene ug/l NO 10 .
2-Nitrophenol ug/l NO 10 .
4-Nitrophenol ug/l ND 50 .
N-Nitrosoclimethylamine ug/l NO 10 .
N-Nitroso-di-n-propylamine ug/l NO 10 .
N-Nitrosodiphenylamine ug/I NO 10 .
Pentachlorophenol ug/l ND 50 .
Phenanthrene ug/l NO 10 .
Phenol ug/I NO 10 .
Pyrene ug/I ND 10-
1 .2 .4-Trichlorobenzene ug/l ND 10 .
2 .4 .5-Trichlorophenol ug/l NO 50 .
Date 08/26/03 Page :7 of 1 3
Laboratory QertificaliQn ID REPORT OF LABORATORY ANALYSIS Laboratory Certification ID~
NC Wastewater 12 This report shall nor be reproduced . except in full,
LA Wastewater 04034
NC Drinking Water 37706 VA Drinking Water 213
Sc 99006 without the written consent of Pace Analytical Services, Inc . FL NELAP E87627
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100acmnalyticaleHuntersville,NC 28078
www.pacelahs .com QUALITY CONTROL DATA Phone:[phone]
Fax.,704.875.9091
Lab Project Number :924895 3
Client Project ID :03-JUL-0337/MI1356
METHOD BLANK : 92325969 1
Associated Lab Samples :923238778 923238802
Blank Reporting
Parameter-Units Result Limit Footnotes
2 .4 .6-Trichlorophenol ug/I ND 10 .
Nitrobenzene-d5 (S) % 53
2-Fluorobiphenyl (S) % 53
Terphenyl-d14 (S) X 79
Phenol-d5 (S) X 24
2-Fluorophenol (S) %34
2,4 .6-TribromDphenol (S) X 64
LABORATORY CONTROL SAMPLE & LCSD : 923259709 92325971 7
Spike LCS LCSD LCS LCSD
Parameter Units Conc . Result Result Rec X Rec RPD Footnotes
Acenaphthene ug/1 50 .00 28 .65 32 .81 57 66 14
Acenaphthylene ug/l 50 .00 28 .33 32 .90 57 66 1 5
Aniline ug/I 50 .00 46 .60 65 .42 93 131 34 1,2
Anthracene ug/1 50 .00 30 .60 35 .09 61 70 14
Benzo(a)anthracene ug/1 50 .00 31 .54 34 .98 63 70 10
Benzo(a)pyrene ug/1 50 .00 34 .90 39 .40 70 79 12
Benzo(b)fluoranthene ug/l 50 .00 33 .45 34 .93 67 70 4
Benzo(g .h .i)perylene ug/I 50 .00 37 .64 41 .79 75 84 10
Benzo(k)fluoranthene ug/l 50 .00 40 .56 53 .07 81 106 27
Benzoic acid ug/l 50 .00 8 .259 10 .30 16 21 22
Benzyl alcohol ug/l 50 .00 24 .40 31 .61 49 63 26
4-Bromophenylphenyl ether ug/l 50 .00 28 .59 32 .89 57 66 14
Butylbenzylphthalate ug/l 50 .00 24 .54 30 .65 49 62 23
4-Chloro-3-methylphenol ug/l 50 .00 24 .97 32 .72 50 65 27
4-Chloroaniline ug/1 50 .00 29 .26 36 .23 58 72 21
bis(2-Chloroethoxy)methane ug/I 50 .00 23 .63 26 .81 47 54 13
bis(2-Chloroethyl) ether ug/l 50 .00 21 .53 24-83 43 50 14
bis(2-Chloroisopropyl) ether ug/I 50 .00 22 .06 25 .51 44 51 14
2-Chloronaphthalene ug/1 50 .00 29 .46 34 .63 59 69 16
2-Chlorophenol ug/l 50 .00 19 .58 26 .75 39 54 31 3
4-Chlorophenylphenyl ether ug/l 50 .00 28 .18 32 .41 56 65 14
Chrysene ug/l 50 .00 32 .13 35 .38 64 71 10
Dibenz(a .h)anthracene ug/l 50 .00 31~43 35 .65 63 71 1 3
Date ;OB/26/03 Page :8 of 1 3
Laboratory Certification l_D5 Laboratory G~-rtifiCafion ID
NC Wastewater 12 REPORT OF LABORATORY ANALYSIS LA Wastewater 04034
NC Drinking Water 37706 This report shall not be reproduced . except in full, VA Drinking Water 213
Sc 99006 w4hout the written consent of Pace Analytical Services, Inc I'L NELAP E87627
Pace Analytical Services, Inc .
9800 Kincey Avenue, Suite 1 00ceHuntersville,NC 28078;a i Analyfical e
www.pacelabs .com QUALITY CON"OL DATA Phone :[phone]
Fax.[phone]
Lab Project Number :9248953
Client Project ID :03-JUL-0337/MI1356
LABORATORY CONTROL SAMPLE & LCSD : 923259709 92325971 7
Spike LCS LCSD LCS LCSD
Parameter Units Conic .Result Result Rec Z Rec RPD Footnotes
Dibenzofuran ug/l 50 .00 32 .78 37.10 66 74 12
1 .2-Dichlorobenzene ug/l 50 .00 26 .15 29 .96 52 60 14
1 .3-Dichloroberizene ug/l 50 .00 24 .76 28 .91 50 58 15
1 .4-Dichlorobenzene ug/l 50 .00 24 .58 28 .74 49 58 16
3X-Dichlorobenzidine ug/l 100 .00 18 .59 19.58 19 20 5 4
2 .4-Dichlorophenol ug/l 50 .00 24 .74 30 .09 50 60 19
Diethylphthalate ug/l 50 .00 18 .70 22 .20 37 44 17
2,4-Dimethylphenol ug/l 50 .00 21 .82 25 .89 44 52 17
Dimethylphthalate ug/l 50 .00 6 .526 7 .756 13 16 17
Di-n-butylphthalate ug/l 50 .00 23 .77 27 .28 48 55 14
4 .6-Dinitro-2-methylphenol ug/l 50 .00 32 .44 35 .92 65 72 10
2 .4-Dinitrophenol ug/1 50 .00 28 .22 31 .82 56 64 12
2 .4-Dinitrotoluene ug/l 50 .00 34 .66 39 .56 69 79 13
2 .6-Dinitrotoluene ug/l 50 .00 34 .10 39 .80 68 80 15
Di-n-octylphthalate ug/l 50 .00 27 .65 31 .27 55 62 12
1 .2-Diphenylhydrazine ug/l 50 .00 27 .62 31 .06 55 62 12
bis(2-Ethylbexyl)phthalate ug/l 50 .00 30 .89 34 .76 62 70 12
Fluoranthene ug/l 50 .00 28 .48 32 .34 57 65 13
Fluorene ug/l 50 .00 30 .51 34 .93 61 70 14
Hexachloro-1 .3-butadiene ug/l 50 .00 26 .05 29 .00 52 58 11
Hexachlorobenzene ug/l 50 .00 35 .05 39 .73 70 80 13
Hexachlorocyclopentadiene ug/l 50 .00 14 .44 19 .89 29 40 32 3
Hexachloroethane ug/l 50 .00 24 .18 28 .31 48 57 16
lndeno(1,2 .3-cd)pyrene ug/l 50 .00 33 .54 38 .16 67 76 13
lsophorone ug/l 50 .00 32 .83 36 .53 66 73 11
2-Methylnaphthalene ug/l 50 .00 28 .79 31.92 58 64 10
2-Methylphenol (o-Cresol)ug/l 50 .00 17 .94 24 .04 36 48 30
3114-Methylphenol ug/l 50 .00 15 .57 22.73 31 46 37 3
Naphthalene ug/l 50 .00 25 .31 27 .99 51 56 10
2-Nitroaniline ug/l 50 .00 28 .36 32 .65 57 65 14
3-Nitroaniline ug/l 50 .00 28 .32 35 .48 57 71 22
4-Nitroaniline ug/l 50 .00 23 .69 30 .19 47 60 24
Nitrobenzene ug/l 50 .00 29 .55 32 .46 59 65 9
2-Nitrophenol ug/l 50 .00 26 .29 28 .92 53 58 10
4-Nitrophenol ug/I 50 .00 10 .56 15 .40 21 31 37 3
N-Nitrosoclimethylamine ug/I 50 .00 13 .52 16.85 27 34 22
N-Nitroso-di-n-propylamine ug/l 50 .00 22 .77 26 .52 46 53 1 5
Date 08/26/03 Page :9 of 1 3
Laboratory Certification 103 Labg(atQrv Qgrtification LD_5
NG Wastewater 12 REPORT OF LABORATORY ANALYSIS LA Wastewater 04034
NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213
SIC 99006 without the written consent of Pace Analytical Services, Inc . FL NELAP E87627
Pace Analytical Services, Inc .
5neAnal 9800 Kincey Avenue, Suite 1 00ytical"Huntersville,NC 28078
www.pacelabs.com QUALITY CONTROL DATA Phone:[phone]
Fax.,704.875.9091
Lab Project Number : 924895 3
Client Project 10 : 03-JUL-0337/MI1356
LABORATORY CONTROL SAMPLE & LCSD : 923259709 923259717
Spike LCS LCSD LCS LCSD
Parameter Units Conc .. Result Result Rec %Rec RPD Footnotes
N-Nitrosodiphenylamine ug/l 50 .00 28 .15 32 .73 56 66 15
Pentachlorophenol ug/l 50 .00 31 .57 35 .69 63 71 12
Phenanthrene ug/l SO .00 30 .01 34 .50 60 69 1 4
Phenol ug/l 50 .00 9 .068 12 .44 18 25 31 3
Pyrene ug/l 50 .00 38 .62 45 .31 77 91 16
1.2 .4-Trichlorobenzene ug/l 50 .00 25 .67 29 .26 51 58 13
2.4 .5-Trichlorophenol ug/l 50 .00 32 .81 38 .55 66 77 16
2.4 .6-Trichlorophenol ug/l 50 .00 29 .83 36 .07 60 72 19
Nitrobenzene-d5 (S)49 55
2-Fluorobiphenyl (S) 50 58
Terphenyl-d14 (S)74 85
Phenol-d5 (S) 18 24
2-Fluorophenol (S)22 33
2,4 .6-Tribromophenol (S) 67 7 2
MATRIX SPIKE &MATRIX SPIKE DUPLICATE : 923259733 92325974 1
923239040 Spike INS MSD HIS MSO
Parameter Units Result Conc . Result Result Rec X Rec RPD Footnotes
Acenaphthene ug/l 0 50 .00 32 .48 30 .67 65 61 6
4-Chloro-3-methylphenol ug/l 0 50 .00 35 .69 27 .58 71 55 26
2-Chlorophenol ug/l 0 50 .00 27 .70 23 .55 55 47 16
1 .4-Dichlorobenzene ug/l 0 50 .00 26 .16 28 .02 52 56 7
2 .4-Dinitrotoluene ug/l 0 50 .00 40 .17 38 .43 80 77 4
4-Nitropherol ug/l 0 50 .00 17 .76 14 .14 36 28 23
N-Nitroso-di-n-propylamine ug/l 0 50 .00 25 .71 26 .27 51 52 2
Pentachlorophenol ug/l 0 50 .00 36 .03 32 .23 72 64 1 1
Phenol ug/l 0 50 .00 12 .99 10 .78 26 22 19
Pyrene ug/l 0 50 .00 46 .11 42 .73 92 86 8
1 .2 .4-Trichlorobenzene ug/l 0 50 .00 28 .05 28 .74 56 58 2
Nitrobenzene-c!5 (S)54 55
2-Fluorobiphenyl (S) 57 55
Terphenyl-d14 (S) 88 83
Phenol-c!5 (S) 25 21
2-Fluorophenol (5) 35 28
2 .4 .6-Tribromophenol (S) 75 7 0
Date :08/26103 PaW :10 of 1 3
Laboratory Certification las Laboratory Certification IDNCWastewater12REPORT OF LABORATORY ANALYSIS LA Wastewater 04034
NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213SC 99006 without the written consent of Pace Analytical Services, Inc . FL NELAP E87627
Pace Analytical Seirvices, Inc.
9800 Kincey Avenue, Suite 100acieAnalyfical"Huntersville,NC 28078
www.pacelabs.com QUALITY CONTROL DATA Phone:[phone]
Fax.[phone]
Lab Project Number :9248953
Client Project ID : 03-JUL-0337/1411356
SAMPLE DUPLICATE : 923259725
923239248 DU P
Parameter Units Result Result RPD Footnotes
Acenaphthene ug/1 NO NO NC
Acenaphthylene ug/l NO NO NC
Aniline ug/1 NO NO NC
Anthracene ug/I NO NO NC
Benzo(a)anthracene ug/l NO NO NC
Benzo(a)pyrene ug/l NO NO NC
Benzo(b)fluoranthene ug/1 NO NO NC
Benzo(g .h .i)perylene ug/l NO NO NC
Senzo(k)fluoranthene ug/I NO NO NC
Benzoic acid ug/l NO NO NC
Benzyl alcohol ug/l RD NO NC
4-Bromophenylphenyl ether ug/l NO NO NC
Butylbenzylphthalate ug/l NO NO NC
4-Chloro-3-methylphenol ug/I NO NO NC
4-Chloroaniline ug/1 NO NO NC
bis(2-Chloroethoxy)methane ug/l NO NO NC
bis(2-Chloroethyl) ether ug/l NO NO NC
bis(2-Chloroisopropyl) ether ug/l NO NO INC
2-Chloronaphthalene ug/l NO NO NC
2-Chlorophenol ug/l NO NO NC
4-Chlorophenylphenyl ether ug/l NO NO NC
Chrysene ug/l NO NO NC
Dibenz(a,h)anthracene ug/l NO NO NC
Dibenzofuran ug/l NO NO NC
1 .2-Dichlorobenzene ug/l NO NO NC
1 .3-Dichlorobenzene ug/l NO NO NC
1 .4-Dichlorobenzene ug/l NO NO NC
3,3'-Dichlorobenzidine ug/l NO NO NC
2 .4-Dichlorophenol ug/l NO NO NC
Diethylphthalate ug/l NO NO NC
2,4-Dimethylphenol ug/l NO NO NC
Dimethylphthalate ug/l NO ND NC
Di-n-butylphthalate ug/l NO NO NC
4 .6-Dinitro-2-methylphenol ug/l NO NO NC
2,4-Dinitrophenol ug/l NO NO NC
2 .4-Dinitrotoluene ug/l NO NO NC
2 .6-Dinitrotoluene ug/l NO NO IN C
Date :08/26103 Page :11 of 1 3
Laboratory Certification ID5 REPORT OF LABORATORY ANALYSIS Labgratory Certification tDs
NC Wastewater 12 LA Wastewater 04034
NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213
SIC 99006 without the written consent of Pace Analytical Services, Inc . I'L NELAP E87627
Pace Analytical Services, Inc .
9800 Kincey Avenue, Suite 100acieAnalyficaloHuntersville,NC 28078
www.pacelabs .com QUALITY CONTROL DATA Phone:[phone]
Fax.,704 .875.9091
Lab Project Number :924895 3
Client Project ID :03-JUL-0337/MI1356
SAMPLE DUPLICATE : 923259725
923239248 DUP
Parameter Units Result Result RPD Footnotes
Di-n-octylphthalate ug/l ND ND NC
1 .2-Diphenylhydrazine ug/I ND IND NC
bis(2-Ethylhexyl)phthalate ug/l ND IND NC
Fluoranthene ug/l IND ND INC
Fluorene ug/I RD ND NC
Hexachlora-1 .3-butadiene ug/l RD IND NC
Hexachlorobenzene ug/l IND ND NC
Nexachlorocyclopentadiene ug/I ND ND NC
Hexachloroethane ug/1 ND RD K
Indeno(l .2 .3-cd)pyrene ug/l ND ND MC
Isophorone ug/l IND ND NC
2-Methylnaphthalene ug/I ND ND NC
2-Methylphenol (o-Cresol)ug/1 ND ND INC
3&4-Methylphenol ug/l ND ND NC
Naphthalene ug/l RD IND NC
2-Nitroaniline ug/l IND IND NC
3-Nitroaniline ug/1 ND ND INC
4-Nitroaniline ug/I ND ND NC
Nitrobenzene ug/l ND ND NC
2-Nitrophenol ug/l IND ND NC
4-Nitrophenol ug/l ND ND NC
M-Nitrosodimethylamine ug/l ND ND NC
N-Nitroso-di-n-propylamine ug/l ND ND KC
N-Nitrosodiphenylamine ug/I ND ND NC
Pentachlorophenol ug/1 ND ND NC
Phenanthrene ug/l ND ND NC
Phenol ug/l ND ND NC
Pyrene ug/l ND ND NC
1,2 .4-Trichlorobenzene ug/l ND ND NC
2,4 .5-Trichlorophenol ug/l ND ND NC
2 .4 .6-Trichlorophenol ug/l ND ND NC
Nitrobenzene-dS (S) 58 62
2-Fluorobiphenyl (S) 58 61
Terphenyl-dl4 (S) Ir 99 9 6
Phenol-d5 (S) % 0 0 5
2-Fluorophenol (S) 1 0 5
2,4 .6-Tribromphenol (S) 13 11 5
Date 08/26103 Page : 12 of 1 3
Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS Laboratory Certification IDs
NC Wastewater 12 LA Wastewater 04034
NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213
Sc 99006 without the written consent of Pace Analytical Services, lflc . FL NELAP E87627
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100eaneAnalyticaleHuntersville,NC 28078
Phone:[phone]
www.pacelabs.com
Lab Project Number :9248953 Fax.-704.875.9091
Client Project ID :03-JUL-0337/MI1356
QUALITY CONTROL DATA PARAMETER FOOTNOTE S
Consistent with EPA guidelines . unrounded concentrations are displayed and have been used to calculate %Rec and RPD values .
LCS(D)Laboratory Control Sample (Duplicate )
KS(D) Matrix Spike (Duplicate)
CUP Sample Duplicat e
ND Not detected at or above adjusted reporting limit
NC Not Calculabl e
J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
NEIL Adjusted Method Detection Limi t
RPD Relative Percent Difference
(S)Surrogat e
Ill Recovery falls outside of OC limits . however . this compound is not found in the associated samples .
[21 The calculated RPD was outside QC acceptance limits .
[31 RPD value was outside control limits, however both percent recoveries were acceptable . Sample results for the
QC batch were accepted based on percent recoveries and completeness of QC data .
[41 The surrogate and/or spike recovery was outside acceptance limits .
[51 The surrogate recovery was outside QC acceptance limits due to matrix interference .
0
Date 08126/03 Page :13 of 13
is
laboratory Certification IDs REPORT OF LABORATORY ANALYSIS Lgboratory CQrlification I-D5
ING Wastewater 12 LA Wastewater 04034
NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213
SC 99006 without the written consent of Pace Analytical Services, Inc Fl-NELAP 187627
Pace Analytical Services, Inc .
9800 Kincey Avenue, Suite 10 02ceAnalytical"Huntersville,NC 2807 8
i Phone:[phone]
Fax:[phone]
August 21,200 3
Mr . Paul J .Fitzgerald
Duke Powe r
Mail Code :MG03A2
13339 Hagers Ferry Road
Huntersville,NC 28078-792 9
RE : Client Project ID : 03-JUL-039IM11 356
Pace Project ID : 924779 6
Dear Mr. Fitzgerald :
I am writing in regards to your concerns about the recovery of the acid surrogates in several of the
samples associated with the above referenced project .
I have reviewed the extraction log and the raw data for these samples and believe that this is an
extraction problem with these samples . Four of the samples (23024532/PMWC-S ;
23024516/PMWC-D ; 23024523/PMWC-BR ; 23024524[PMWH-BR) emulsified during the
extraction process . As stated in the laboratory report, there was insufficient sample volume available
for reextraction and reanalysis of these samples .
LCS 923180525,which was extracted alongside the samples, shows acceptable recoveries for
phenol-d5 and 2-fluorophenol . Other samples analyzed on the same day but not extracted on the
same day show recoveries for these two surrogates in the range of 50-70%recovery . Therefore,I do
not believe that the low recoveries are caused by a problem with the instrumentation .
Our acceptance limits for phenol-d5 and 2-fluorophenol are 10-125%,which are consistent with
EPA data for these surrogates .
If you have any additional questions or need additional information, please contact me at
704-875-9092 Ext .229 .
Sincerely yours,
Mavis Jones
Quality Manager
Pace Analytical Samices . Inc.
980 Kincey Avenue, Suite 100
I
Huntersville,NC 28078CeAnalyficalPhone 704 875 9W
"M pacelabs.com Far ;104.875."l
August 28,200 3
mr . Jay Parkin,
Duke Powe r
13339 Hagers Perry Road
X930K2
Encteravills,NC 2007 B
RE : Lab Project Numbert 9249793
Client Project ID ; 03-~-0337/]KII356
Dear bbr .Perkins :
Enclosed are the analytical results for G&WIG(4) received by the laboratory on July 23 . 2003 .Result. reported
herein confoon to the mat current NMC st=darda, where applicable,less otherwise narrated in the body of
the report .
If you have any questions CWCG=iug this report please feel free to contact se .
iincerely ,
Awl .
KriNti Tart
KrLsti .Ta,rt*pacel&b8 .c=
Project xanager
Enclosures
1,bomtorv Ceffification INLabwAM Carfificadon ID&REPORT OF LABORATORY ANALYSIS KY ftking WAW MWMCWastewater 12
MCD-11 -VAW ME Thb MW SW ad be rWO&CK WMW in WIL VA WnkkV Wativ 213
SC 9M wifto E,WMen MM of pace kWjcal E,,wlck UM R.NELAP E87627
Pace Analytical Services, Inc .
980 Kifcgykenue, Suite 100
Huntarsville,NC 28078j~~5?6 Analytical "Phone.[phone]~Pawlabs .oonr Far.704.875.9091
Lab Project Number :924979 3
Client Project ID ; 03-JUL-0337/NI135 6
Lab Sample NO : 923172019 Project Sample Number ;9249793-001 Date Collected :07/22/03 16 :05
Client Sample ID :23024516/PKWC-D Matrix : Water Date Received :07/23/03 11 :50
Paronetere Resulto Units Report Limi Analyzed By CAB No . Qual RwLm t
GC/MS Semivolatile s
Semivolatile Organics Prop/Method ; EPA 827 0
Acenaphthene,160 ug/I 100 07/29/03 09 :57 BET 83-32-9
Acenaphthylene 18 . ug/1 10 . 07/29/03 09 :57 BET 208-96-8
Aniline No Ug/l Ia . 07/29/03 09 :57 BET 62-53-3
Anthracene No ug/l 10 . 07/29/03 09 :57 BET 120-12-7
Benno (a) anthracene No ug/l 10 . 07/29/03 09 :57 BET 56-55-3
Bmzo(a)pyrene ND ug/l 10 . 07/29/03 09 :57 BET 50-32-8
Benzo (b) f luormthene,ND ug/I 10 . 07/29/03 09 :57 BET 205-99-2
Bmzo(g,b,i)peryl=*NV ug/l 10 . 07/29/03 09 :57 BET 191-24-2
Benzo (k) f luoranthane No ug/l 10 . 07/29/03 09 :57 BET 207-08-9
Benzoic acid ND ug/l 50 . 07/29/03 09 :57 BET 65-85-0
Bwzyl alcohol ND Ug/l 20 .07/29/03 09 :57 BET 100-51-6
4-BronoPharaylPhereYl other No ug/I 10 . 07/29/03 09 :57 BET 101-55-3
Butylbemxylphthalate No Ug/I 10 . 07/29/03 09 :57 BET 85-68-7
4-Chloro-3-methylphemol No ug/I 20 .07/29/03 09 :57 BET 59-50-7
4-Chloroaniline,No ug/l 20 .07/29/03 09 :57 BET 106-47-6
bin (2-Chloroethoxy)methaue No ug/l 10 . 07/29/03 09 :57 BET 111-91-1
bis(2-Chlaroethyl) other No Ug/l 10 . 07/29/03 09 :57 BET 111-44-4
jis(2-Chloroisopropyl) other ND uq/1 10 . 07/29/03 09 :57 BET 39638-32-9
2-Chloronaphthalene ND ug/1 10 . 07/29/03 09 ;57 BET 91-58-7
2-Chlorophenol ND ug/l 10 . 07/29/03 09-.57 BET 95-57-8
4-Chlorophenylphanyl other ND ug/I 10 . 07/29/03 09 :57 BET 7005-72-3
Chrysens ND ug/l 10 . 07/29103 09 :57 BET 218-01-9
Dibenz(a,h)anthrocene,No ug/1 10 . 07/29/03 09s57 BET 53-70-3
Dibenzofuran 15 . uq/I 10 . 07/29/03 09 :57 BET 132-64-9
1,2-Dichlorobenzone,ED ug/l 10 . 07/29/03 09 :57 BET 95-50-1
1,3-Dichlorobansons,No ug/I 10 . 07/29/03 09%57 BET 541-73-1
1,4-Dichlorob~we HD ug/I 10 . 07/29/03 09 :57 BET 106-46-7
3,31-Dichlorobanzidine No ug/l 20 .07/29/03 09 ;57 BET 91-94-1
2,4-DichlocoPh4a0l ND ug/I 10 . 07/29/03 09 :57 BET 120-63-2
Diethylphthalate ND ug/l 10 . 07/29/03 09 :57 BET 84-66-2
2,4-Dimethylphocal ND uq/1 10 . 07/29/03 D9 :57 BET 105-67-9
Dimsthylpbthalato ND ug/1 10 . 07/29/03 09 :57 BET 131-11-3
Di-A-butYlPhthalAtO ND uq/1 10 . 07/29/03 09 :57 BET 84-74-2
4,6-DiUitr0-2-m*thYlPhan0l ND ug/l $0 . 07/29/03 09 :57 BET 534-52-1
2,4-Dinitrophwol ND uq/I 50 . 07/29/03 09 :57 BET 51-28-5
2,4-Dinitrotolume ND Ug/1 10 . 07/29/03 09i57 BET 121-14-2
2,6-Dinitrotoluene ND ug/1 10 . 07/29/03 09 :57 BET 606-20-2
Data, 08/28/0)Page ; I of 20
l,boratm Carfificatian 11%1,boneor, Carganhon IDS REPORT OF LABORATORY AKALYSIS KY D"M WAK 90090NCWagannow 12
NC Dim ddi W9w 37706 Ibis mW stud not be Mproftex OC01 in fulk VA r I Water 213
sc 99006 wow on wain compat of Pace m*dw SWAM kc R.MMV E87W
Psce An8lyfleol Seffices. Inc.
M Kincey Avenue, Suits 100
HunWswile,AC 28078ceAnalytical"Phone:[phone]
Fax.[phone]ac,
Lab Project Number :924979 3
Client Project ID : 03-JUL-0337/NI135 6
Lab Sample No :923172019 Project Sample Number :9249793-001 Date Collected :07/22/03 16 :05
Client Sample ID : 23024516/PMWC-D Katrix : Water Date Received :07/23/03 11 :50
Parameters Reaults Units Report Limit Analyzed By CAS No . Dual ReqLm t
Di-n-octylphthalate No ug/l 10 . 07/29/03 09 :57 BET 117-84-0
1,2-Diphmylhydrazine No ug/l 20 .07/29/03 09 :57 BET 122-66-7
bis(2-3thylhexyl)phthalate No ug/I 10 . 07/29/03 09 :57 BFT 117-01-7
Fluorantheae No ug/1 10 . 07/29103 09 :57 BRT 206-44-0
Pluorene 30 . ug/I 10 . 07/29/03 09 :57 BET 96-73-7
Hmachloro-1,3-butadime No ug/l 10 . 07/29/03 09 :57 BET 87-68-3
Haxachlorobensene No ug/l 10 . 07/29/03 09 :57 BET 118-74-1
Heanchlorocyclopentadiene No ug/1 10 . 07/29/03 09z57 BET 77-47-4
Raxachloroethane No uq/1 10 . 07129103 09 :57 BET 67-72-1
Imd=o(l,2,3-cd)pyr*ue ND ug/I 10 . 07/29/03 09 ;57 EST 193-39-5
Isophorome No ug/l Ia . 07/29/03 09 :57 BBT 78-59-1
2-Methyluephthalene 370 ug/l 100 07/29/03 09 ;57 BET 91-57-6
2-Methylphenol (o-Cresol)No ug/l 10 . 07/29/03 09 :57 BET 95-48-7
U4-Methylphenol No ug/1 10 . 07/29/03 09 :57 BET
Naphthalene 1100 ug/I 100 07/29/03 09 :57 BBT 91-20-3
2-Nitroaniline No ug/I 50 . 07/29/03 09 :57 BET 90-74-4
3-Nitroaniline No ug/l 50 . 07/29/03 09 :57 BET 99-09-2
.4,Nitroaeiline No ug/i 50 . 07/29/03 09 :57 BET 100-01-6
litrobanzens No ug/I 10 . 07/29/03 09tS7 BET 98-95-3
2-Nitrophanol ND ug/I 10 . 07/29/03 09M DST 08-75-5
4-Nitrophenol No ug/l 50 . 07/29103 09sS7 BET 100-02-7
N-Mitrowdimethylamire ND ug/I 10 . 07/29/03 09 :57 BRT 62-75-9
N-Mitroso-di-n-propylazins No ug/I 10 . 07/29/03 09 :57 BET 621-64-7
N-Nitrosodiphemylamius ND ug/1 10 . 07/29/03 09 ;57 BHT 06-30-6
Pentachlomphanol.No ug/I 50 . 07/29/03 09s57 BET 87-86-5
Phanamthrens,36 . ug/I 10 . 07/29/03 09 :57 BET 85-01-8
Phenol No ug/I 10 . 07/29/03 09 :S7 BET 108-95-2
pyrenf No ug/1 Ia . 07/29/03 09s57 BET 129-00-0
1,2,4-TrichlorobenzenG ND ug/1 10 . 07/29/03 09s57 BET 120-82-1
2,4,5-Trichlorophenol No ug/l 50 . 07/29/03 09 :57 BET 95-95-4
2, 4,6 -Trichlorophamol No ug/I 10 . 07/29/03 09 :57 BET 88-06-2
Nitrobenzens-0 IS) 108 % 07/29/03 09 :57 BET 4165-60-0
2-Fluorobiphanyl IS) 65 % 07/29/03 09 :57 BET 321-60-8
Torpbmyl-dl4 IS) 78 % 07/29/03 09 :57 M 1719-Sl-D
Phenol-0 IS) 1 % 07/29/03 09z57 BET 4165-62-2 1,2
2-Fluorophenol IS) 3 % 07/29/03 09M BET 367-12-4 1,2
2,4,6-Tribrowphanol IS)26 % 07/29/03 09 :57 BET
Date Zxtracted 07/25/03 07/25/0 3
Datel 04/26/03 Pag.,2 of 20
laboralonCerfiflicatiM102i,banaam Cardfladlan 10%REPORT OF LABORATORY ANALYSIS KY DrWft WAu 90090NoWasuwatsr 1 2
No Mwng wdu 3TAX ThW mW 90 ad be Mgwoduved.VOW 10 K VAD&M WUK 213
sc 99006 to Maim conswo od PM NMWM SWVtM hm Ft NELAP Eaw
Pace Analylicol Services, Inc.
9W Kincey Avenue, Suite 100Huntersville,NC 28078ZeAnalyfical"Phow 704 875 902vvivivPacalabscomFax.704.87SX91
Lab Project Number ;924979 3
Client Project ID :03-JUL-0337/MI135 6
Lab Sample No :923172027 Project Sample Number :9249793-002 Date Collected :07/22/03 16 :25
Client Sample ID :23024517/PNWF-D Matrix ; Water Date Received ;07/23/03 11 :50
Parameters Results Units Rqport Limi Analyxed By CAS No .Dual RwLm t
GC/MS Sentivolatile s
Sam,ivolatile Organics Prep/Method : EPA 827 0
Acanaphthene 200 ug/l 100 07/29/03 10 :36 BET 83-32-9
Acenaphthylene 10 . ug/l 10 . 07/29/03 10 :36 BET 206-96-8
Aniline NO ug/l 10 . 07/29/03 10 :36 BET 62-53-3
Anthracene NO ug/l 10 . 07/29/03 10 :36 BUT 120-12-7
Benzo(O anthracene ND ug/I 10 . 07/29/03 10 :36 BET 56-55-3
Benzols)pyrene ND ug/l 10 . 07/29/03 10 :36 BET 50-32-6
Benzo (b) f luoranthene NO ug/l 10 . 07/29/03 10 :36 BET 205-99-2
Bmzo(g,h,i)peryl=e ND ug/l 10 . 07/29/03 10 :36 BET 191-24-2
Benzo (k) f luoranthens NO ug/l 10 . 07/29/03 10 :36 BET 207-08-9
Benzoic acid ND ug/l 50 . 07/39/03 10 :36 BET 65-85-0
Beazyl alcohol ND ug/l 20 .07/29/03 10 :36 BET 100-51-6
4-Bromophenylphenyl ether ND ug/l 10 . 07/29/03 10 :36 BET 101-55-3
Butylbenxylphthalats ND Ug/l 10 . 07/29/03 10 :36 BZT 85-68-7
4-Chloro-3-mathylphenol NO ug/l 20 .07/29/03 10 :36 BUT 59-50-7
4-Chloroauiline ND ug/l 20 .07/29/03 10 :36 BET 106-47-8
w bie(2-Chloroothoxy),sethane ND ug/l 10, 07/29/03 10 :36 BET 111-91-1
iB(2-Chloroothyl) other ND ug/l 10 . 07/29/03 10 :36 BET 111-44-4
bliq(2-Chloroisopropyl) ether ND ug/l 10 . 07/29/03 10 ;36 BET 39638-32-9
2-Chloronaphthalene ND ug/l 10 . 07/29/03 10 :36 RIrr 91-58-7
2-Cblorophmol ND ug/l 10 . 07/29/03 10 ;36 BET 95-57-0
4-ChloropbWlphenyl other NO ug/l 10 . 07/29/03 10 :36 BET 7005-72-3
Chryswe ND ug/l 10 . 07/29/03 10 :36 BET 218-01-9
Dibezz(a,h)wthracene NO ug/l 10 . 07/29/03 10 :36 BET 53-70-3
Dibenzofuran 16 . ug/l 10 . 07/29/03 10 :36 SET 132-64-9
1,2-Dichlorobanzene ND ug/l 10 . 07/29/03 1006 BET 95-50-1
1,3-Dichlorobemsene ND ug/l 10 . 07/29/03 10 :36 BET 541-73-1
1,4-Dichlorobenzaae ND ug/l 10 . 07/29/03 10 :36 BET 106-46-7
3,3--Dichlorobezaidine NO ug/l 20 .07/29/03 10 :36 BET 91-94-1
2,4-Dichlorophencl ND ug/l 10 . 07/29/03 10 :36 BET 120-83-2
Diethylpbthalate No ugli 10 . 07/29/03 1006 BET 94-66-2
2,4-Dimethylphenal,ND ug/l 10 . 07/29/03 10 :36 BET 105-67-9
Dimthylphthalate ND ug/l 10 . 07/29/03 10136 BET 131-11-3
Di-n-butylphtbalate ND ug/l 10 . 07/29/03 10 :36 BIT 84-74-2
4,6-Dinitro-2-methylphenol ND ug/l 50 . 07/29/03 10 :36 BET 534-52-1
2,4-Dinitrophervol,ND ug/l 50 . 07/29/03 10 :36 BET 51-28-5
2,4-Dinitrotolume NO ug/l 10 . 07/29/03 10 :36 BET 121-14-2
2,6-Dinitrotoluene ND ug/l 10 . 07/29/03 1006 BET 606-20-2
Date :08/26/03 ftq.~3 of 20
I -boMM C-rtfficffbM IDSREPORT OF LABORATORY ANALYSIS KYDMftWgu 90090NoWaows* 1 2
k'CftklbvwAuf 3M This few "so,to fwo&xad~ now in fiA VA r WAK 213
Sc 9w womut to wmm owmant of P= kmww Wvkm w FL MELAP E87627
Pace Analytical Services, Inc.
98M K)ncey Avenue, Suits 100
Hussuarsville.NC 28078ZeAnalytical`Phone :704.875,9092
~paoelabscom Fax.[phone]
Lab Project Number : 924979 3
Client Project ID :03-JUL-0337/MI135 6
Lab S mple NO :923172027 Project Sample Number :9249793-002 Date Collected :07/22/03 16 :25
Client Sample ID : 23024517/PMWF-D Matrix : Water Date Received ;07/23/03 11 :50
Paremseters Results Units Report Limi Analyzed By CAB No .Qual ReqLm
Di-n-octylphthalate ND ug/l 10 . 07/29103 10 :36 BET 117-84-0
1,2-Diphany1hydrazine RD ug/l 20 .07/29/03 10 :36 BET 122-66-7
bio(2-Ethylbexyl)phtbalate No ug/l 10 . 07/29/03 10 :36 BET 117-81-7
Pluoranthene No ug/l 10 . 07129/03 10 :36 BET 206-44-0
Fluorene 45 .ug/l 10 . 07/29/03 10 :36 BST 86-73-7
Emachloro-1 .3-butadione No ug/l 10 . 07/29103 10 :36 BET 87-68-3
Rexachlorobanzene,No ug/l 10 . 07/29/03 1006 BXT 118-74-1
Hexachlorocyclopantadiena No ug/l 10 . 07/29/03 10 :36 BET 77-47-4
HwachlorOOthanO ND ug/l 10 . 07/29/03 10 :36 BET 67-72-1
Jndeno(l,2,3-cd)pyrene ND ug/l 10 . 07/29/03 10 :36 BET 193-39-5
loopborone No ug/l 10 . 07/29/03 10 :36 BET 78-59-1
2-Methyluaphthalene 350 ug/l 100 07/29/03 10 :36 BET 91-57-6
2-Methylphenol (0-Cresol)ND ug/l 10 . 07/29/03 10 :36 BET 95-48-7
3&4-Xetbylphaaol ND ug/l 10 . 07/29/03 10 :36 BRT
Naphthalene 1200 ug/l 100 07/29/03 10 :36 BET 91-20-3
2-Mitroaniline No uq/l 50 . 07/29/03 10 :36 BET 08-74-4
3-Nitroaniline ND ug/l 50 . 07/29/03 10 ;36 BET 99-09-2
.4-Mitroanillne HD ug/l 50 . 07/29/03 10 :36 BET 100-01-6
Igitrobsexamse ND Ug/l 10 . 07/29/03 10 :36 BET 90-95-3
I-Nitrophemol. No ug/l 10 . 07/29/03 10 :36 BST 88-75-5
4-Mitr0phen0l No ug/l 50 . 07/29/03 10 :36 BZr 100-02 .7
U-Nitrosodimethylazine No ug/l 10 . 07/29/03 10 :36 BRT 62-75-9
N-Nitroso-di-a-propylamine No ug/I 10 . 07/29/03 10 :36 BET 621-64-7
N-Nitrooodiphenylanine ND ug/l 10 . 07/29/03 10 :36 BRT 86-30-6
Pectachlorophemol HD ug/l 50 . 07/29/03 10 :36 BET 87-86-5
ph...thrage 47 .ug/l 10 . 07/29/03 10 :36 BET 85-01-8
Phenol RD ug/l 10 . 07/29/03 10 :36 BST 108-95-2
Pyrane No ug/l 10 . 07/29/03 lOs36 BIT 129-00-0
1,2,4-Tricb1orobenzene ND ug/l 10 . 07/29/03 10 :36 BET 120-62 .1
2,4,5-Trichloropheno I ED ug/l 50 . 07/29/03 10 :36 BET 95-95-4
2,4,6-Trichlorophenol No ug/l 10 . 07/29/03 1006 BET 88-06 .2
mitrobeazene-0 (S) 106 % 07/29/03 lOs36 BET 4165-60-0
2-Pluorobiphanyl (S) 70 111 07/29/03 10 :36 BET 321-60-8
T6rphmyl-dl4 (9)94 % 07/29/03 10 :36 BET 1718-51-0
Phensol-0 (8) 19 % 07/29/03 10 ;36 BET 4165-62-2
2-Fluorophemol (S) 25 % 07/29/03 10 :36 NET 367-12-4
2,4,6-Tribromophenol (S) 83 % 07/29/03 10 :36 BET
Date Ritracted 07/25/03 07/25/0 3
Dates 0#/20/03 Page ;4 of 20
1,1bontm Cssrfif~tion 10a,borlIM GRIMM IDS REPORT OF UBORATORY AMYSIS KY Drialske Watar gDD9DNCWAsbuder 1 2
NC Dibldna Vhdw 3TM8 This Npod shal nol be reprodumd.WUPt In fuls VA WnIft Watff 213
SO 99Dw without N WHIM mmm of PICS lums"M Ser"Iew Inc FL NEL06P E576V
Pace Analyficsi Services, Inc.
M Kincey Avenue, Suits 100
HunWswile.AC 28078;--;a'ceAna1yfica1'-Phone:704.875,9092vvvnvPace1abS'wM Fax.,704.875.9M
Lab Project Number :924979 3
Client Project ID!03-JUL-0337/KI135 6
Lab Sample NO ; 923172035 Project Sample Number ;9249793-003 Date Collected :07/22/03 11 :55
Client Sample ID :23024518/PMWG-D Matrix : Water Date Received :07/23/03 11 :50
Parametera ReaUlto Units Report Limi Analvxod BY CAB No .Dual RwLm
GC/14S Somivolatilea
Sonivolatile Organics Prep/Method :EPA 827 0
Acenaphthene 51 . ug/I 10 . 07/29/03 11 :14 BET 83-32-9
Acenaphthylene No ug/I 10 . 07/29/03 11 :14 BET 208-96-8
Aniline No ug/l 10 . 07/29/03 11 :14 BET 62-53-3
Anthracene ND ug/l 10 . 07/29/03 11 :14 BET 120-12-7
BenzoWanthracene ED ug/I 10 . 07/29/03 11 :14 BET 56-55-3
Benzo(a)pyrane,No ug/I 10 . 07/29/03 11:14 BUT 50-32-8
BwzQ (b) f luorantbene ED ug/I 10 . 07/29/03 11:14 BET 205-99-2
Benzo(g,h,i)POrylens No ug/l 10 . 07/29/03 11 ;14 BET 191-24-2
Benzo(k)fluorantbene No ug/l 10 . 07/29/03 11:14 BET 207-00-9
Benzoic acid ND ug/l 50 . 07/29/03 11 :14 139T 65-85-0
Benzyl alcohol ND ug/l 20 .07/29/03 11:14 BET 100-51-6
4-Bromcphanylphenyl other No ug/l 10 . 07/29/03 11:14 BET 101-55-3
Butylbonzylphthalate ED ug/I 10 . 07/29/03 11:14 BET 05-68-7
4-Chloro-3-mothylphenol No ug/I 20 .07/29/03 11:14 BET 59-50-7
4-Chloroaniline ED ug/1 20 .07/29/03 11 :14 BET 106-47-8
0 bie(2-Chloroethoxy)meth--o ED ug/l 10 . 07/29/03 11 :14 ENT 111-91-1
)is(2-Chlor"thyl) other ED ug/I 10 . 07/29/03 Iltl4 BIT 111-44-4
'bis(2-Chlorcisopropyl) other ND ug/I 10 . 07/29/03 IItl4 SET 39638-32-9
2-Chloronaphthalene ED ug/I 10 . 07/29/03 11 :14 BET 91-58-7
2-Chlorophaacl.No ug/I 10 . 07/29/03 11 :14 BET 95-57-8
4-Chlorophanylphanyl other ED ug/l 10 . 07/29/03 11 :14 BZT 7005-72-3
cbrysone ED uq/I 10 . 07/29/03 IItI4 BET 210-01-9
Diben,(a, h) anthracene,ED ug/l 10 . 07/29/03 11:14 BET 53-70-3
Dibonzofuran ED ug/I 10 . 07/29/03 11 :14 ENT 132-64-9
1,2-Dichlorobenzone No ug/l 10 . 07/29/03 11 :14 BET 95-50-1
1,3-Dichlorabousene ND ug/I Ia . 07/29/03 Ilzl4 BZT 541-73-1
1,4-Dichlorobenzene No uq/I 10 . 07/29/03 11 :14 BE'r 106-46-7
3,31-Dichlorobeasidine ED ug/l 20 .07/29/03 11 :14 BET 91-94-1
2,4-Dichlorophanol ED ug/l 10 . 07/29/03 11 :14 BET 120-83-2
Dietbylphthalate ND ug/l 10 . 07/29/03 I1zl4 BET 04-66-2
2,4-Dimstbylphonul ED ug/l 10 . 07/29/03 11 :14 Brr 105-67-9
DiwthylphLbalate ND ug/l 10 . 07/29/03 11 :14 BET 131-11-3
Di-n-butylphthalate HD ug/I 10 . 07/29/03 11 :14 BE?84-74-2
4,6-Dinitro-2-mothylphonol ND ug/I 50 . 07/29/03 11 :14 BET 534-52-1
2,4-Dinitraphano 1 No ug/I 50 . 07/29/03 11 :14 BET 51-28-5
2,4-DinitrotolueaO ED ug/l 10 . 07/29/03 11 :14 BIrr 121-14-2
2,6-Dinitrotoluens ED ug/l 10 . 07/29/03 11 :14 BET 606-20-2
Der ., 09/21/03 Page : 5 of 20
1,1bDigm Canftficn Mei.borftry Cedficafien We REPORT OF LABORATORY ANALYSIS KywwdlvwaK Pamw wasbwnv 12
Mcftftwebt VM M Won 04 ad be WoducK =cW in fat VA DwftN Viabo 213
Sc r"~ up widen MRSO of PM ftvdw SKVICIS.keL FL NELQ E8?W
Pace Analytical Services,Inc.
9800 Kincey Avenue, Suite 100
Huntwswile.NC 28078
a eAnalyfical"Phone M4 875 9092
?CI Pacelabs'com Fax.[phone]
Lab Project Number :924979 3
Client Project ID ; 03-JUL-0337/KI135 6
Lab Sample No :923172035 Project Semple Number :9249793-003 Date Collected :07/22/03 11 :55
Client Sample ID :23024518/PMKG-D Katrix : Water Date Received :07/23/03 11 :50
Parameters Ropulto Units Report Limi Analyzed By CAB No .Oval ReqLat
Di-n-octylphthalate No ug/I 10 . 07/29/03 11 :14 Birr 117-84-0
1,2-Dipheny1hydrazine No ug/I 20 .07/29/03 11 :14 BET 122-66-7
bis(2-Bthylhwcyl)phthalate No ug/l 10 . 07129/03 11 :14 BET 117-81-7
Pluoranthena ND ug/l 10 . 07/29103 11 :14 BET 206-44-0
Fluorene No ug/I 10 . 07/29/03 11 :14 BET 86-73-7
Bmachloro-1 .3-butadiene No ug/i 10 . 07/29/03 11 :14 BET 87-68-3
Nexachlorobenzene ND ug/1 10 . 07/29/03 11 ;14 BET 118-74-1
Bexachlorocyclopentadiene ND ug/l 10 . 07/29/03 11 :14 BET 77-47-4
Hazachloroethane ND ug/I 10 . 07/29/03 11 ;14 BET 67-72-1
Ind*ao(l,2,3-cd)pyrene No ug/I 10 . 07/29/03 11 :14 BET 193-39-5
Isophorone ND ug/I 10 . 07/29/03 11 :14 SIM 78-59-1
2-Nothylnaphthalmo ND ug/l 10 . 07/29/03 11 :14 BET 91-57-6
2-Methylphenol (0-Cresol)ND ug/l 10 . 07/29/03 11 :14 BET 95-48-7
364-Methylphezvol No ug/I 10 . 07/29/03 11 :14 BET
Naphthalene 15 . ug/I 10 . 07/29/03 11 :14 BET 91-20-3
2-Nitromiline ND ug/I 50 . 07/29/03 11 :14 BET 88-74-4
3-Nitrowiline ND ug/l 50 . 07/29/03 11 :14 BET 99-09-2
4-Mitroamiline No ug/l 50 . 07/29/03 11 :14 BET 100-01-6
* trobenzene ND ug/I 10 . 07/29/03 11s14 BRT 98-95-3
21 Nit"Phanal ND ug/1 10 . 07/29/03 11 :14 BZr 88-75-5
4-Nitrophmol ND ug/l 50 . 07/29/03 11 :14 BET 100-02-7
N-Nitrosodimethylamine ND ug/I 10 . 07/29/03 11 :14 BET 62-75-9
U-Niticoso-di-n-pirvVylamine ND ug/1 10 . 07/29/03 lltU EST 621-64-7
N-Nitrosodiphanylamine ND ug/I 10 . 07/29/03 1lzl4 BXr 86-30-6
Pentachlorophanol ND ug/1 50 . 07/29/03 21 :14 BRT 87-86-5
Phno-threne 19 . ug/l 10 . 07/29/03 11 :14 BET 85-01-0
Phenol No ug/l 10 . 07/29/03 llzl4 BZT 108-95-2
Pyracm HD ug/I 10 . 07/29/03 lltl4 BET 129-00-0
1,2,4-Trichlorobenzeae HD ug/1 10 . 07/29/03 11 :14 BRT 120-82-1
2,4,5-Trichlorapheriol ND ug/1 50 . 07/29/03 11 :14 SET 95-95-4
2,4,6-Trichlorophenol ND ug/i 10 . 07/29/03 11 :14 BET 88-06-2
Nitrobenzene-6 (0) 75 % 07/29/03 11 ;14 BET 4165-60-0
2-Fluorobiphanyl (S)74 11 07/29/03 11 :14 BET 321-60-8
Terpbanyl-dU (S) 06 % 07/29/03 11 :14 SET 1716-51-0
Phenol-d5 (8)14 % 07/29/03 11-14 BET 4165-62-2
2-Fluorophenol (S) 23 % 07/29/03 11 :24 BET 367-12-4
2,4,6-Tribrowphwol (3) 86 % 07/29/03 11 :14 BET
Date Extracted 07/25/03 07/25/03
Uts,09/28/03 Page : 6 of 10
I bonflon, Carfification IDS..Danong Cardficanon I REPORT OF LABORATORY ANALYSIS KYMdftWav 9DD90NCWaVjwAv12
NC UnkhV water 3TIO6 This Mw Mau not be WWL=d. exceot in hA VA Mr"V WMW 213
SC 99DDS www ON 17411n cons" Is Pace kwAkA Swv~ k~FL NaAP E87827
Pace Aaalyfical Semites, Inc.
980OKinceykenue. Suite 100Huntarsville.AC 28078ZfcconAnalyfical"Phone:[phone]
~.oacelabsxom Fax.[phone]
Lab Project Number :924979 3
client Project ID : 03-JUL-0337/KI135 6
Lab Sample NO : 923172043 Project Sample Number : 9249793-004 Date Collected :07/21/03 16 :25
Client Sample ID : 23024519/PXWI Matrix : Water Date Received :07/23/03 11 :50
Parameters Results Units Rewrt Limit Analysed BY CAB No . Dual Roglai t
GCIKS Sezivolatile s
Semivolatile Organics Prep/Metbod : EPA 827 0
kcanaphthene No USA 10 . 07/29/03 11 ;52 BET 83-32-9
Aconaphthylene ND ug/l 10 . 07/29/03 11 .52 BET 208-96-8
Aniline ED ugil 10 . 07/29/03 11 :52 BET 62-53-3
Anthracene ED ug/l 10 . 07/29/03 11 :52 BET 120-12-7
Benzo(a) anthracens No ug/I 10 . 07/29/03 11 :52 BET 56-55-3
B=zo(a)pyr=e ED ug/I 10 . 07/29/03 Ilt52 BET 50-32-8
BanzoWfluoratithene ED ug/I 10 . 07/29/03 11 :52 BET 205-99-2
Banzo(q,h'i)PerylGne ED uq/l 10 . 07/29/03 11 :52 BET 191-24-2
BoaxoMfluorantheng,ND u9/1 10 . 07/29/03 11t52 BET 207-08-9
Benzoic acid ED ug/l 50 . 07/29/03 11 :52 BET 65-85-0
Bwzyl alcohol ND ug/i 20 .07/29/03 11 :52 BET 100-51-6
4-Bromophanylphanyl other ED ug/l 10 . 07/29/03 11 :52 BET 101-55-3
Butylbeasylphthalate No Ug/l 10 . 07/29/03 11 :52 BET 85-68-7
4-Chloro-3-mthylphwol ED ug/l 20 .07/29/03 11 :52 BET 59-50-7
4-Chloroamiline ND uq/l 20 .07/29/03 11 ;52 BET 106-47-8
,,bin (2-Chlorothoocylowithaza,ED ug/I 10* 17/21/01 11 :52 BET 111-91-1
bis(2-Chlorciotlryl) other No ug/l 10 . 07/29/03 11 .52 BET 111-44-4
,is(2-Chloroisopropyl) other ED ug/l 10 . 07/29/03 lliS2 BET 39638-32-9
2-Chlorianaphithalene ED Ug/l 10 . 07/29/03 11152 BET 91-58-7
2-Chlorophomol ND Uq/I 10 . 07/29/03 11 :52 BET 95-57-8
4-Chlorophanylphonyl other ED USA 10 . 07/29/03 11 :52 BET 7005-72-3
ChryBone ED Ug/i 10 . 07/29/03 IliS2 BET 218-01-9
Dibenz (a,h)anthraceas ED Ug/1 10 . 07/29103 11 :52 BET 53-70-3
Dibenzofuran ED ug/1 10 . 07/29/03 Ils52 BET 132-64-9
1,2-Dichlorobatizene ED Ug/I 10 . 07/29/03 11 :52 BET 95-50-1
1,3-Dichlorobigazone ED Ug/1 10 . 07/29/03 11 :52 BET 541-73-1
1,4-Dichlorobanswe ED Ug/1 10 . 07/29/03 Ilj52 BET 106-46-7
3,31-Dichlorobwzidine ED uq/1 20 .07/29/03 11 :52 BET 91-94-1
2,4-Dichloropb,enol ND ug/I 10 . 07/29/03 11:52 BET 120-83-2
Diothylphthalate ED Ug/l 10 . 07/29/03 11 :52 BET 84-66-2
2,4-Disethylphonol ED Uq/1 10 . 07/29/03 IliS2 Bffr 105-67-9
Dimtbylphthalate ED Uq/1 in . 07/29/03 11 :52 BET 131-11-3
Di-n-butylpbthalate ED ug/1 10 . 07/29/03 11 :52 BET 84-74-2
4,6-Dinitro-2-methylphezol ED ug/l 50 . 07/29/03 11&52 BET 534-52-1
2,4-Dinitrophenol ND ug/I 50 . 07/29/03 11 :52 BET 51-28-5
2,4-Dinitmtolume No ug/l 10 . 07/29/03 Ilt52 BET 121-14-2
2,6-Dinitrotolume ED ug/1 10 . 07/29/03 Ils52 BET 606-20-2
Date . OB/21/03 Page ; 7 of 20
I,boW,mCwfifIcaIipnIDS0REPORT OF LABORATORY ANALYSIS KY DmWng Vistai 9 MNGWaghwadw12
NC Wdft WWK 37106 ThIs mW "I ad be mpioikwk 0=0 ki fiA VA Dik"q Vftter 213
Sc 99006 wmad So wrwen mum 01 Pw Aim"me SWVkK h~FL MELAP EBW
Pace Analyficol Services, Inc.
98M Kincey Avenue, Suite 100
Huntarsvifit NC 28078ceMalytical"Phone [phone]
Fax.[phone]
ac,
Lab Project Number ;924979 3
Client Project ID :03-JUL-0337/MI135 6
Lab Sample No :923172043 Project Sample Number : 9243793-004 Date Collected ;07/21/03 16 :25
Client Sample ID :23024519/PMWI Hatrix : Water Date Recei~ved :07/23/03 11 :50
Parmeters Results Units Report Limi Analyzed BY CAB No .OUAI Regliest
Di-n-Qctylphthalate No ug/l 10 . 07/29/03 11 :52 BET 117-84-0
1,2-Diphmylhydrazine No ug/I 20 .07/29/03 11 :52 BET 122-66-7
bia(2-8thylhexyl)phthalate No ug/l 10 . 07/29/03 11 :52 BUT 117-Bl-7
Fluorantheme ED ug/l 10 . 07/29/03 11 :52 BET 206-44-0
Pluorene No ug/I 10 . 07/29/03 11 ;52 BET 86-73-7
Haxachloro-1,3-butadiene No ug/l 10 . 07/29/03 11 :52 BET 87-68-3
Rexachlorobenzene No ug/I 10 . 07/29/03 11;52 BET 118-74-1
Esexachlorocyclopentadierse ED ug/l 10 . 07/29/03 11 :52 BET 77-47-4
Hexamblornethane ED ug/l 10 . 07/29/03 11 ;52 BET 67-72-1
lnd=o(1,2,3-cd)pyr"e No ug/l 10 . 07/29/03 11 :52 BET 193-39-5
Isophorone No ug/l 10 . 07/29/03 11 ;52 BET 78-59-1
2-Hathylumphthalene No USA 10 . 07/29/03 11 :52 BET 91-57-6
2-Metbylphacol (0-Cresol)No ug/I 10 . 07/29/03 11 :52 BET 95-48-7
U4-Kethylphanol NO ug/I 10 . 07/29/03 11 :52 BET
Naphthalene No ug/I 10 . 07/29/03 11 :52 BET 91-20-3
2-Nitroanilize ED Ug/l 50 . 07/29/03 11 :52 BET 80-74-4
3-Nitroacuiline No ug/l 50 . 07/29/03 11 ;52 BET 99-09-2
4-Mitroaniline ED ug/l 50 . 07/29/03 11 :52 BET 100-01-6
Nitrobenzessue,RD Ug/I 10 . 07/29/03 11 :52 DST 98-95-3
i-Nitrophanol ED Ug/I Ia . 07/29/03 Il :S2 BET 88-75-5
4-Nitrophenol ND Ug/l 50 . 07/29/03 11 :52 BET 100-02-7
N-Nitmacalinathylamine RD Ug/l 10 . 07/29/03 11:52 BET 62-75-9
N-Nitrooo-di-n-propylamine No Ug/l 10 . 07/29/03 11 :52 M 621-64-7
N-Nitrozodiphanylazine No Ug/l 10 . 07/29/03 11M BET 86-30-6
Pentachlorophamol ED Ug/l 50 . 07/29/03 11 :52 BET 87-86-5
Ph....thrm,No Ug/I 10 . 07129/03 II :S2 BET 85-01-8
Pommel ED Ug/l 10 . 07/29/03 11%52 EST 108-95-2
Pyrens,No mg/I 10 . 07/29/03 11 :52 BET 129-00-0
1,2,4-Trichlorobanzene No Ug/I 10 . 07/29/03 11 :52 BET 120-82-1
2,4,5-Trichlorophenol No Ug/l 50 . 07/29/03 11 :52 BET 95-95-4
2,4,6-Trichlorophencs No Ug/I 10 . 07129/03 11 :52 BET 88-06-3
Hitrobenzarse-d.5 (9) 56 % 07/29/03 11 :52 BIT 4165-60-0
2-Fluorobiphanyl (8) 56 07/29/03 12 :52 BET 321-60-8
Tisrphenyl-,114 (3) 78 07/29/03 11 :52 BET 1718-51-0
Phanol-,15 (S) 8 is 07/29/03 Ils52 BET 4165-62-2 3
2-Fluourophecol (S) 11 % 07/29/03 11:52 BET 367-12-4
2,4,6-Tribromophenol (S) 62 111 07/29/03 11:52 BET
Date Extracted 07/25/03 07/25/0 3
Dates 08/26/03 page ; a of 20
1 Abondan, cerfl9caflon 1
NC Wmdres 12 REPORT OF LABORATORY ANALYSIS KY DrMMng Waw 9DM
NC D*&4 Mur 37?06 Thk (Sped OW rat be Woduced.am$In hA,VA 0 11 -VhW 213
Sc VAN Wfthoul an wftm cowmad Of Pace kwykw SwV1cM Inc.FL NELAP EMU
Pace Analytical $ervic", Inc .
9800 Kincey Avenue, Suita 100
Hun0swile,NC 280787cemalyfical-Phone:[phone]
Far 704.875.9091
Lab Project Number ;924979 3
Client Project ID :03-JUL-0337/MI1356
PARAMETER FOOTNOTE S
Inorg=ic Wet Chemistry Analyses were performed at our Pace Asheville laboratory and Organic and Metals
testing was performed at our Pace Charlotte laboratory unless otherwise footnoted .
KD Not detected at or above adjusted reporting limit
NC Not Calculabl e
J Estimated concentration above the adjusted method detection limit and balm the adjusted reporting limit
MDL Adjusted Method Detection Limi t
(S)Surrogat e
(1)The surrogate and/or spike recovery was outside acceptance limits .
[2) The sample could not be re-extracted due to limited sample volume .
[31 Acid surrogate recovery outside of control limits . The data was accepted based on valid recovery of the two
remaining acid surrogates .
Date : OB/20/03 Page :9 of 20
1,boMowCarh1kafion10st abmssn, Cerfificatlan IDS REPORT OF LABORATORY ANALYSIS KY MWM WaW 9MNCWnbwdw 1 2NC NWft Wor 3TM Tbb regain align ro be repa&amd,NCO In hA VAD110 VMK 213
SC 990D8 ~ V1*writhn canuffit of PM k*"SOMM UC R.NELAP E87W
PaCe Analytical Services,Ine .
WKincey Avenue, Suits 100
Hunlarsville.NC 28078ceMalyfical"Phone:[phone]v,vvvvpace4sbs .com Fu.*704.875.9091
ac,
QUALITY CONTROL DATA
Lab Project Number :924979 3
Client Project ID : 03-JUL-0337/MI1356
QC Batch :78376 Analysis Method : EPA 827 0
QC Batch Method : Analysis Description : Seativolatile Organics
Associated Lab Samples :923172019 923172027 923172035 92317204 3
METHOD BLANK ; 923100517
Associated Lab Sasiples :923172019 923172027 923172035 923172043
Blank Reporting
Parameter Units Result Limit Pootngtee
Acenaphtherve ug/l No 10 .
Ac ema phthylene ug/l ND 10 .
Aniline ug/l ND 10 .
Anthracene ug/1 NO 10 .
B=zo (a) anthracene ug/1 NO 10 .
BOILZO(a)pyrene ug/l ED 10 .
Benzo (b)fluoranthene ug/1 No lo .
Bmso(g,h,i)peryl=e ug/l NO 10 .
Bezzo W fluorazttheze ug/l NO 10 .
BenZoic acid ug/1 No 50 .
A111kFzy,1 alcohol ug/1 NO 20 .
w 3rossnphanylphemyl ether ug/1 NO 10 .
autylbenzylphthalate ug/1 No 10 .
4-Chloro-3-mathylpheral ug/l ED 20 .
4-Chloroaniline ug/l ND 20 .
bio(2-Chlor"thozy)mthane ug/l ND 10 .
bia(2-Chloroothyl) other ug/1 No 10 .
bis(2-Chloroisopropyl) other ug/l ND 10 .
2-Chloronaphthaleme uq/1 ED 10 .
2-Chlorophanx,l ug/1 ED 10 .
4-cblorophwylphanyl other ug/1 No 10 .
Chrysene ug/l ND 10 .
Dibeaz (a,b)anthracene ug/l NO 10 .
Dibenzoturan ug/1 ND 10 .
1,2-Dichlorobanzene,ug/1 ND 10 .
1,3-Dichlorobenzene ug/l ED 10 .
1,4-Dichlorobenzwe ug/1 NO 10 .
3,3--Dichlorobemaidins,ug/1 ND 20 .
2,4-Dichlorophson 1 ug/l NO 10 .
Diethylphthalate ug/1 NO 10 .
2,4-Dimethylphanol ug/l ND 10 .
Date ;08/21/03 Pa,*t 10 of 20
tgboratorv Carfir~fipn IDS0L,bonemm Gerfiflabon IDs REPORT OF LABORATORY AIMYSIS KY Odnft W&W MWNCWasftwa* 1 2
Mcpwngwaw 3T= Tift mW &W nol bs rWo&vK wApt In K VA DMft WMK 213
Sc 99005 WbDUI thl Wdbn WNW 00 PWS kfi"W SMVIM ks~FL NELAP E87627
Pace Analytical Samices, Inc.
9800 Kincey Avenue, Suile 100
Hunlarsville,NC 28078;;ZeAnalyficaf-Phone.,704.875.9092~.Pacalsbs .com Far.704.875.9091
QUALITY CONTROL DATA
Lab Project Number :924979 3
Client Project ID : 03-JUL-0337/KI1356
MMOD BLANK :92318051 7
Associated Lab Samplesi 923172019 923172027 923172035 923172043
Blank Reporting
Parameter Units Result Limit FoQtAgtea
Dimethylphthalate ug/I NI)10 .
Di-n-butylphthalate ug/I ND 10 .
4,6-Dinitm-2-mthylphenal ug/I ND 50 .
2,4-Dinitrophenol ug/I HD 50 .
2 .4-Dinitrotolume mall ND 10 .
2,6-Dinitrotolume ug/I NI)10 .
Di-n-octylphthalate ug/1 ND 10 .
1,2-Diphuylhydrazine ug/1 ND 20 .
bis(2-Ethylhexyl)phthalate ug/I ND 10 .
Fluoranthene ug/I ND 10 .
Fluorene ug/l ND 10 .
Hastauchloro-1 .3-butadiene ug/I ND 10 .
Saxachlorobenzene ug/I RD 10 .
HexachlorocyclopentadiSmG ug/1 ND 10 .
bloroatkume ug/I HD 10 .
o(l,2,3-cd)py,reme ug/1 HD Ia .
~-,Pwchoroae ug/l ND 10 .
2-Methy1naphthalene ug/1 ND 10 .
2-Nothylphemol (o-Cresol)ug/1 ND 10 .
3&4-Nothylph emo I Ug/I ND 10 .
Naphthalene Uq/1 RD 10 .
2-Nitroaniline ug/l HD 50 .
3-Nitmanilize Ug/1 ND 50 .
4-Mitroaniline ug/l ND 50 .
Nitrobenzwe Ug/l ND 10 .
2-Nitrophianol Ug/1 HD 10 .
4-Nitrophanal ug/l ND 50 .
N-Nitrooodimthylamine ug/I ND 10 .
N-mitroso-di-n-propylazine Ug/l ND 10 .
N-Nitrosodipbemylamine ug/I HD 10 .
Pentachlomphenvol ug/l MD $0 .
Pham--thrsne ug/1 ND 10 .
Phervol Ug/l ND 10 .
Pyrene ug/1 ND 10 .
1,2,4-Trichlorobeazene ug/I ND 10 .
2,4,5-Trichlorophezvol Ug/1 ND 50 .
Date,08/28/03 Page : 11 of 2 0
REPORT OF LABORATORY ANALYSIS KY WWM WZW 90090NCWaWwabs 12
HC D"M VhW 3TM8 Thb mW Ad ad be Wadu~0=0 h hA VA OrMV W&W 213
Sc am ~IM w1ftn owsent of Pace Ana"W SeW=&h~FL NELAP E87627
Paco Analytical SeNices,Inc.
98W Kincey Avenue, Suits 100
Hunhwsville,NC 28078;2ceAnalXicaf-Phone :[phone]
~Paw)abs .cofn Fax:[phone]
QUALITY CONTROL DAT A
Lab Project Number ;924979 3
client Project ID :03-JUL-0337/MI1356
METHOD BLANK :92318051 7
Associated Lab Samtples : 923172019 923172027 923172035 923172043
Blank Reporting
Paramet Units RGAMIt Limit Pogtngt9a
2,4,6-Trichlorophanol ug/l No 10 .
Hitrobenzano-d5 (S) %6 4
2-Fluorobiphenyl (S) %64
Torphanyl-d14 (S)94
Phemol-d5 (S) 16
2-Fluorophenol (S)21
2,4,6-Tribrouopheruol (S) 77
LABORATORY CONTROL SAMPLE LCSD : 923171169 92317117 7
Spike LCS LCSD LCS LCS D
Parameter Mliitt-Conc,Result Result Rec %Rao RPD Footnotes
Aceamphthene,ug/l 50 .00 37 .74 37.20 76 74 1
Admkk ...hthylene ug/1 50 .00 37 .28 37 .32 75 75 0
w ug/l 50 .00 22 .18 29 .87 44 60 30
anthracene ug/l 50 .00 41 .27 40 .10 82 so 3
Henan (a) "thracene ug/l 50 .00 41 .87 40 .90 84 82 2
Banzo (a) pyreas ug/l 50 .00 43 .88 42 .79 Be 86 3
Banzo (b)fluoranthene ug/l 50 .00 44 .46 42 .86 89 86 4
Bmzo(g,h,i)peryl=e ugil 50 .00 43 .01 42 .37 06 85 2
Boost,W fluorauthene ug/1 50 .00 41 .41 41 .39 83 83 0
Benzoic acid ug/l 50 .00 15 .28 22 .35 31 45 36 1
Bonsyl alcohol ug/1 50 .00 29 .24 40 .86 so 32 33 1
4-BromphanylphODY1 other ug/l 50 .00 39 .11 38 .48 78 77 2
Butylbmsylphthalate ug/l 50 .00 92 .59 109 .4 185 219 17 2,3,2,3
4-Chloro-3-mothylphembi ug/l 50 .00 24 .72 42.34 49 85 53 1
4-Chloroaniline ug/l 50 .00 20 .20 30 .09 40 60 39 1
bio(2-Chloroethoxy)methane ug/1 50 .00 38 .60 37 .08 77 74 4
bis(2-Chlaroethyl) other ug/l 50 .00 34 .34 34 .57 69 69 1
bia(2-Chlomisopropyl) other ug/l 50 .00 37 .22 36 .56 74 73 2
2-Chloronaphth&1=6 ug/l 50 .00 35 .46 35 .09 71 70 1
2-Chlor*ph"Ol ug/l 50 .00 21 .33 34 .83 43 70 48 1
4-Chlorophmylphenyl other ug/l 50 .00 38 .66 36 .52 77 77 0
Chrysozo uq/1 50 .00 41 .19 40.48 82 81 2
Dibeaz (a,h)anthr&cGnG ug/l 50 .00 44 .11 44 .37 Be 89 1
Date~00/20/03 Page ;12 ot 20
9 I abononm CartWocatim I,,borAn ClOW2110D I REPORT OF LABORATORY ANALYSIS KY Making WaW 90090W WuWn* 1 2
NC OdnWW Wage 37706 This mean W not be WockxK VVW In full, VA DMft W&W 213
SC 99006 MMWA tM wft MOM Of P=k*WW SONIM IM FL NELAP E87627
Pace Analytical Services, Inc.
1
9M Kincey Avenue, Suite too
a ce Malyfical Huntetsville,AfC 28078
Phone :[phone]
Far 704.875.9091
C,
QUALITY CONTROL DATA
Lab Project Number :924979 3
Client Project ID : 03-JUL-0337/MI1356
LKBORATORY CONTROL SAMPLE LCSD : 923171169 92317117 7
spike We LCSD LCs LCSD
Parameter Units COUP .Result Result %get %Reg "D Footnotes
Dibenzofur"ug/l 50 .00 37 .64 37.19 75 74 1
1,2 .Dichlorobenzone ug/l 50 .00 30 .47 28 .89 61 58 5
1, 3 -Dichlorobenzeme ug/l 50 .00 29 .22 28 .19 so 56 4
1 .4 -Dichlorobenzerse ug/l 50 .00 29 .83 28 .19 60 56 6
3,31-Dichlorobensidirse ug/l 100 .00 41 .14 41 .62 41 42 1
2,4-Dichlorophen*1 ug/1 50 .00 24 .76 37 .97 so 76 42 1
Diethylphthalate ug/1 50 .00 35 .86 35 .09 72 70 2
2,4-Dimethylphervol ug/l 50 .00 24 .20 38 .19 48 76 45 1
Dimethylphthalate ug/l 50 .00 23 .33 23 .94 47 48 3
Di-n-butylphthalate ug/l 50 .00 41 .09 39 .66 82 79 4
4,6 .Dinitro-2-wthylphenol ug/l 50 .00 41 .65 45 .36 83 91 9
2,4-Dinitrophenol ug/1 50 .00 34 .81 49 .86 70 100 36 1
2,4-Dinitmtolume ug/l 50 .00 44 .35 43 .69 89 87 1
2 .6-Dinitrotolueno ug/l 50 .00 43 .41 43 .03 87 86 1
Di-n-octylphthalate ug/l 50 .00 47 .88 47 .46 96 95 1
1,2-Diphmylhydrazine ug/1 50 .00 35 .15 34 .56 70 69 2
a (2 -Bthylh"yl) phthaslate uq/1 50 .00 47 .10 46 .53 94 93 1
uoramthene ug/l 50 .00 39 .63 38 .98 so 78 2
Fluorene ug/l 50 .00 39 .63 38 .90 79 78 2
Heavachloro-1, 3 -butadieno ug/l 50 .00 26 .82 26 .07 58 56 3
Hentachlorobenzens,ug/l 50 .00 38 .29 37 .68 77 75 2
3. . .chlorocyclopentadiane ug/l 50 .00 23 .39 24 .67 47 49 5
Hexachloroethane ug/1 50 .00 29 .98 2839 60 57 5
Indeno (1 .2,3-c0pyrsame,ug/1 50 .00 43 .69 43 .77 87 Be 0
Isophorosesse ug/l 50 .00 42 .36 41 .51 85 83 2
2-Nothyluaphthalme ug/l 50 .00 34 .91 34 .05 70 60 2
2-Methylphwol (a-Cresol)ug/l 50 .00 20 .11 33 .42 40 67 50 1
3&4-Methylphanol ug/1 50 .00 19 .26 32 .72 38 65 52 1
Haphthaleme ug/l 50 .00 33 .71 32 .30 67 65 4
2-Nitroamiline,ug/1 50 .00 37 .50 37 .96 75 76 1
3-Nitromiline u9/1 50 .00 31 .60 34 .57 63 69 9
4-Nitroaniline ug/l 50 .00 28 .96 35 .15 56 70 19
Nitrobenzene ug/l 50 .00 36 .30 35 .20 73 70 3
2-Nitrophenol ug/l 50 .00 32 .10 39 .97 64 80 22
4-Nitrophezvol ug/l 50 .00 23 .70 20 .22 27 40 36 1
N-Nitromodimet.hylami"ug/l 50 .00 14 .88 18 .76 30 38 23
H-Mitroso-di-n-propylamine uq/1 50 .00 41 .01 40 .27 82 80 2
rates 08/20/03 Pages 13 of 20
Issbonsurv Carfilkabon ID& I nboratm Wfficathan IDs
NCWadewa* U REPORT OF LABORATORY ANALYSIS KY DrkWM Mew 90090
NG Missing Water 37M 7bb Few Stan ad be WOAMA V=M in tulL VA n , -VMK 213
sc 99006 ~119 WFAWn QXMd Of PM kdykgl S@rVkM k~R.NELAP E87627
Pace Analytical Services, Inc.
W Kinogy Avenue, Suite 100
HunAgswile.NC 28076;2ceAnalyfical'Ph"M#8;159Mvv,vvvPac&1abs.coM Aar:M4.875,9091
QUALITY CONTROL DATA
Lab Project Number :924979 3
Client Project ID ;03-JUL-0337/MI1356
LABORATORY CONTROL SAMPLE & LCSD : 923171169 92317117 7
Spike LCS LCSD LCS LCS D
Parameter Units CQAC,Result Result Re %ReC RM Pootagtoa
M-Nitrooodiphenylmine ug/1 50 .00 38 .29 37.12 77 74 3
Pentachlorophazol ug/l 50 .00 39 .07 40 .47 78 81 4
Phemout;hrazu,ug/l 50 .00 39 .10 38 .34 78 77 2
pher,ol ug/l 50 .00 12 .24 16 .90 24 34 32 1
Pyrme ug/l 50 .00 40 .63 39 .69 81 79 2
1,2,4-Trichlorobenzene ug/l 50 .00 30 .81 29 .60 62 59 4
2,4,5-Trichloroph=ol ug/1 50 .00 31 .04 42 .19 62 84 30
2,4,6-Trichlorophmol ug/l 50 .00 33 .25 41 .66 66 83 22
Nitrobextzane-d5 (S) 76 75
2-Pluorobiphenyl (S)74 74
Terphenyl-d14 (S)84 83
Phaoml-0 (S)24 34
2-Fluorophemol (8)28 44
2,4,6-Tribr=phwol (8) 89 93
WIOEAT~Rlf CONTROL SAMPLE : 923180525
Spike LCS WE
Parameter mlita-Conc . Result Rae Footnotes
kcez~aphthwe ug/l 50 .00 35 .86 72
kcacaphthylene ug/1 50 .00 35 .53 71
Aniline ug/l 50 .00 32 .43 65
Anthraceng ug/1 50 .00 39 .89 90
Banzo(Manthracene ug/l 50 .00 39 .12 78
Benso(a)pyrwe ug/l 50 .00 42 .54 8 5
Senzo (b)fluoranthene ug/1 50 .00 45 .25 90
Rattan (g.h, i) perylene ug/l 50 .00 34 .35 69
Benzo (k)fluoranthene ug/l 50 .00 39 .35 79
Benzoic acid uq/l 50 .00 10 .31 21
Beasyl alcohol uq/l 50 .00 32 .60 65
4-Bromophanylphanyl ether ug/l 50 .00 41 .60 93
Rutylbensylphthalate ug/l 50 .00 74 .08 148 2
4-Chloro-3-wthylphowl ug/l 50 .00 33 .09 66
4-Chloroaniline ug/l 50 .00 34 .44 69
big (2-Chlornetboxy)wtharm uq/1 50 .00 33 .67 67
bia(2-Chloroothyl) ether ug/1 50 .00 32 .75 6 6
Data$08/29/03 Page : 14 of 20
0 LJWIAIQ~
WIV016130'aw 12 REPORT OF LABORATORY ANALYSIS KY Onnift Wan 9M
NC Mftq WM 3TM6 nA mW 94 not bs Wo&=d.except in bA VA Wn1ft W4K 213
Sc 9M ~tM WMM compt ot Pm ka"M SerAces,gat FL WELAP E$7627
Poes Anflyflest Sertrien,k7c.
nngWAwl Svftg 100
Haftsid/k,AC 28078ceAnalytical"'ftm 704.8759092mvvPP8ce1abs.oOm Far 704.875.9091
ac,
QUALITY CONTROL DATA
Lab Project Nmber :924979 3
Client Project ID :03-JUL-0337/KI1356
LABORATORY CONTROL SAMPLE : 923180525
Spike LCS L.Cs
Parameter Unito Conc, Reault ROD Footnotes
bis(2-Chlomisopropyl) other ug/l 50 .00 32 .56 65
2-Chloranaphthaleme ug/1 50 .00 33 .04 66
2-Chlorophital us/1 50 .00 27 .82 56
4-Chloropherrylphettlyl other Ug/1 50 .00 40 .14 0 0
Chrysexto urgill 50 .00 40 .62 81
Dibegaz(aMaxithracome ug/1 50 .00 35 .57 71
Dibeastotlaurfur,Ug/1 50 .00 36 .40 73
1,2-Dichlorobeffuzears ug/1 50 .100 31 .11 62
1,3-Dichlombmzme Uq/1 50 .00 29 .98 60
1,4-DiCUO=b=ZMG Ug/1 50 .00 29 .76 60
3,31--Dichlorobefouridiner ug/i 100 .00 50 .02 50
2,4-DiCILlOrOPh~l Ug/1 50 .00 32 .09 64
Diethylphthalate Ug/1 50 .00 37 .34 75
2,4-Dimethylph~l Ug/1 50 .00 29 .95 60
Dimthylphthalate Ugl/1 50 .00 26 .58 53
Di-n-butylphthalate Uq/1 50 .00 39 .56 79
4,6-Dinitm-2-methylphomfol Ug/1 50 .00 48 .22 96
2,4-DinitraPh=l Ug/1 50 .00 3B .05 76
2,4-Dinitrotalume Ug/1 50 .00 43,01 86
2,6-Dinitmtoluwe Ug/1 50 .00 39 .07 78
Di-n-octylphthalate Ug/1 50 .00 41 .74 84
1,2-Diphelay1hydrazine Ug/1 50 .00 27 .84 56
bis(2-gthylhexyl)phthalate Ug/1 50 .00 41 .15 82
Fluorailthoes Ug/1 50,00 41 .74 84
Pluoreme,urg/1 50 .00 39 .36 79
Nexachloro-1,3-butadione Uq/1 50 .00 31 .21 62
Refiechlorobeflizeme Ug/1 50 .00 40 .34 61
Elexachlormyclopwtadiene Ug/1 50 .00 22 .33 45
Hexachloroothatifer Ug/1 50 .00 29 .08 58
1nde,Do(1,2,3-cd)pyroDo Ug/1 50 .00 34 .99 70
loophorone Ug/1 50 .00 36 .05 72
2-Nothyluaphthalene Ug/1 50 .00 31 .89 64
2-Nothylphenal (o-Cresol)Ug/1 50 .00 26 .20 52
364-Mothylphouguol og/1 50 .00 23 .90 48
Naphthalene Ug/1 50 .00 33 .16 66
2-Nitromeniline ug/1 50 .00 34 .39 69
3-Nitroamiline ug/1 50 .00 36 .09 72
Page :15 of 20Date:08/28/0 3
Is
12mratnw C.Arldinfinn IDumm9mrilliliumamREPORT OF LABORATORY ANALYSIS KY Drinking Water 9OD90NCwasts"ter 1 2
NC Drinking Water 37706 Thill snall not De reproduced . excePI in lull VA Drifting Water 213
sc 99005 WIMDUI thir WfIVISA COn"001 Pate ~ly~l Ser"'C'S' tM FL NELAP E87627
Polo AintlyffelliftWen ke
9800 10incey,11ifenoi Suite 100
hforolfirsitille,AC 28078ceAnalydcal'Phone [phone]Mwwwpacelabs.orons Fu.'704.875.9091
a17,
QUALITY CONTROL DATA
Lab Project Number :924979 3
Client Project ID ; 03-JUL-0337/MI1356
LABORATORY CONTROL SAMPLE :923180525
Spike LCS LCS
Parameter Unite Colic .Result %Eric Footalotee
4-Nitroamiliffirs,ug/1 50 .00 40 .21 so
Nitrobetrus;ezer ug/1 $0 .00 34 .92 70
2-Hitropheasol ug/1 50 .00 32 .67 6s
4-Nitrophresual uq/1 50 .00 20 .07 40
le-Nitrozodisawathylamins,ug/1 50 .00 23 .41 47
N-Nitroso-di-n-propylamine US/1 50 .00 35 .26 70
U-Nitrosodiplassurylargrines ug/1 50 .00 38 .43 77
PmtacbLloroph~l ug/1 50 .00 39 .14 7 8
ug/1 50 .00 40 .15 so
Phenol ug/1 50 .00 13 .82 28
Pyrenees,ug/1 50 .00 41 .55 63
1,2,4-Trichlorobismisserre ug/1 50 .00 30 .97 62
2,4,5-Trichlorophreffol ust/1 50 .00 38 .47 77
2,4,6-Trichlorophessiol ug/1 50 .00 37 .02 74
Nitrobegazaii Of 70
2-Fluorobiphearyl (8) 68
Terphernityl-dI4 (S) 87
Phessai (S) 29
2-Fluorophasnol (S) 38
2,41,6-Tribromophersol (S) 89
MATRIX SPIKE fi MATRIX SPIKE DUPLICATE : 923171165 92317119 3
923152805 Spike Me NEU Me KS D
Parmeter Units Result Court . Ressult Result %_Ig_C %_Er& M Footnotes
kcrumplithemns ug/i 0 100 .00 73 .40 79 .82 73 80 0
4-Chloro-3-mathylphanol ug/1 0 100 .00 70 .76 75 .74 71 76 7
2-Chlorophenol ug/1 0 100 .00 64 .12 63 .35 64 63 1
1,4-Dichlorobenzene ug/1 1 .001 100 .00 60 .36 60 .58 59 60 0
2,4-Dinitrotoluene ug/1 0 100 .00 86 .10 96 .37 86 96 11
4-Nitropharsol u9/1 0 100 .00 41 .91 42 .25 42 42 1
N-Nitroso-di-n-propylamine ug/1 0 100 .00 79 .00 83 .19 79 83 5
Pentachloropherrol uq/1 0 100 .00 62 .73 71 .68 63 72 1 3
Plarinsol UT/I 0 100 .00 29 .85 28 .87 30 29 3
Pyrite ug/1 0 100 .00 79 .09 87 .81 79 88 10
1,2,4-Trichlorobenzene ug/1 0 100 .00 59 .09 61 .22 59 61 4
Data :08/28/03 Page ;16 of 20
I aborAtory Garliflution 1 0-blr-'-N CeftNUIM ID REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090NCWa6t,neafte, 1 2
NC Drinking Water 37706 This (soon shall not be reprodieved, except in fail VA Drinking Water 213
SC 99DD6 arthotif the within consent of Pace ""ul SeNa:vs,I%,Ft.NELAP E87627
Psce Ansiolest Services,Inc.
M 16ncey Militia, Slgif 100
HunisAllit AC 26078*(~52oeAnaljftal'Phow W875 9092www.pacelobs .com Fu.704.875.9091
QUALITY CONTROL DATA
Lab Project Number ;9249793
Client Project ID :03-JUL-0337/NI1356
M&TRIX SPIKE &bMTRIX SPIKE DUPLICATE : 923171185 92317119 3
923152805 Spike KS KSD KS KSD
Parameter Units Result Conc .Result Result %-R&c Rec, RPD Footnotes
Nitrobassamosel (S)74 19
2-Flustrobiphisoxyl (S) 71 7 6
Taryhmyl-dl4 (S) 70 73
Phessol-,15 (8) 32 31
2-Pluorophassiol (S)42 38
2,4,6-Tribr bagful (S) 78 90
SAME DUPLICATE : 923173910
923152839 DUP
Parameter units Relault Result M Footructele
Ac~phth~ug/l ED ND NC
kcaussisailastbrylene ug/l ND ND NC
Aniline ug/l ND ND RIC
Allithracrestas ug/l ND ND KC
Benew (a) anthracenes ug/l ND ND KC
Bronsto (a) pyrones ug/l ED ND NC
Sezueo (b) f liforasathespe ug/l ND ND NC
Bmgao(g,h,i)perylone ug/l HD ND Mc
Senzo (k) f luoranthease ug/1 ND ND NC
Bexazoic acid ug/l ND ND KC
Bessiryl alcohol ug/l ND ND He
4-Bromoophessylphanyl other ug/l ND ND NC
Butylbearylphthalate ug/l ND ND NC
4-Chloro-3-mothylphenol ug/l ND ND NC
4-Chloroaniline ug/l ND ND KC
bio(2-Chloroethoxy)methana ug/l ND ND NC
bis(2-Chlomethyl) other ug/1 ND ND NC
bio(2-Chlorcisopropyl) other ug/1 ND ND NC
2-Chloronaphthalone ug/l ND ND NC
2-Chlorophoutacil ug/l ND ND NC
4-Chlorophenylphenyl ether ug/l ND ND NC
Claryorace,ug/l ND ND NC
Diblesiz(a,h),savithracene ug/l ND ND HC
Dibel or=ug/1 ND ND HC
1,2-Dichlorobenterie Ug/1 ND NO NC
Date :00/28/03 Pagt~17 of 20
1 sparingly C."Itification IDSREPORT OF LABORATORY ANALYSIS KY Drinking Water 90090NCwastervater 1 2
NC Drinking Water 37706 This report sJull not pe,eeproduced, except in lull,VA Dnrikung Wale,213
Sc 99(06 vrtriw Uw iviften consent ol Pace Analytical Services,Inic FL NELAP E87627
Pm AwlWal Serview,Inc.
98M 10nay AwrpA Sub 100
HmbWlk, AC 28078C.eAnalytical'a Phom 7MB759092
Fax.704.875,9091
QUALITY CONTROL DATA
Lab Project Numsber :924979 3
Client Project ID ;03-JUL-0337/NI1356
SAME DUPLICATE : 923173918
923152839 DUP
Parrumister -units Result Reoult UD Focatnotel;
1,31-Diclolorrobenzene ug/l ED ED NC
1,4-Dichlombenzene ug/l ED HD KC
3,31--DichlorobtfMaidi-ne,ug/l RD HD NC
2,4-DiCUoroph~l ug/l ED ND KC
Diethylphthalate ug/l ED ED KC
2,4-Dimtktylph~l ug/l ED RD HC
Dimthylphthalate ug/l HD HD KC
Di-n-butylphthalate ug/l RD ED HC
4,45-Dinitm-2-smarthylphearforl ug/l ED HD KC
2,4-Drinitrophionfol.ug/l ED ED NC
2,4 .Dinitmtolume ug/l RD ED TIC
2,6-Dinitrotolualmall,ug/l ED ND NC
Di-n-rotylphthalmate ug/l ED ND KC
1,2-Diphenylhydrazine ug/l RD ED KC
big 12,lthylhyll phtbal8t6 13911 ED ED MC
Fluorazathents ug/l RD ED KC
Fluorene ug/l ED ED NC
R"achloro-1,3-butadiene ug/l ED HD TIC
Hemoschlorobertmene ug/l ED ED NC
Reatatchlorocyclopentadierie ug/l ED HD NC
Hemetchloroethame ug/l HD ND NC
Indeno (1,2 .3 - cd)pyreue,ug/l HD ND N C
Ishophorcrue ug/l ND ND NC
2-NothylMPhthaleas ug/l ED ND TIC
2-MethylP11411101 (o-Cresol)ug/l ED HD NC
3&4-Hathylpheml ug/l ED ND NC
Haplathallext, ug/l ND ND KC
2-Hitroanilizaa,ug/l ND ND NC
3-Nitroamilins,ug/l ED ND NC
4-Nitroarailine ug/l HD ND NC
Nitrobenzene ug/l ED RD NC
2-Nitroplasiol ug/l HD ND NC
4-Nitrophmol ug/l ND ND NC
N-NitroaGdimethylamiae ug/l ND HD NC
N-Nitroso-di-n-propylmine ug/l ND ND NC
M-Nitrosodiphertylamize,ug/1 ND ND HC
Peritachlorophenol ug/l HD HU N C
Date :09/20/03 Page :18 of 20
I Ahnnatory 01fiffifatIQUIDS REPORT OF LABORATORY ANALYSIS KY Drinking Water N MNCWasteanater 1 2
NC Drinking Water 37706 This ieport shalt not Do teprockmed . Mitt In lot VA Dhinlong Water 213
5C 99M wichoul the wrthen, consent of Pace "IYUC21 Se"Icls .Im Fl.NELAP E87627
Paco Anslyffevit SoMm,Inc.
M Vncvy AYM Sudif 100
MOW011A NC 28078ZmAnallytical"a PhM.,704.875.9092wivev.pacelabs.cons Far 704.875.9091
QUALITY CONTROL DATA
Lab Project Number :924979 3
Clieut Project ID : 03-JUL-0337/HX1356
SAMPLE DUPLICKTE :923173918
923152839 DUP
Paripmeter Units Result Result RPD Footnotes
Pheaufacthreme uq/1 ND ND KC
Phenol ug/1 IM ED VC
Pyrenge ug/1 RD ND HC
1,2,411-Trichliprobenzange ug/1 ND ND KC
2,4,5-Trichloropbencl ug/1 HD ND KC
2,4,46-Trichlorophemol ug/1 ND ND KC
Nitrobausualimpus-0 (S) % 62 5 6
2-Fluorobiphetuyl (8) % 55 53
Terphengryl-d14 M % 81 75
Phetaxil-0 (S) % 11 19
2-Fluorophimmull (8) 116 13 26
2,41,15-Tribromarphemol (S) 111 40 7 6
Data ;00/39/03 Page : 19 of 20
C .Md cation I
NC Wastee,ater 12DJUS REPORT OF LABORATORY ANALYSIS Ky Drinking Water 9M
NC Dnr~kiog Wait,37706 This report shall not oP repropuced, except in full,VA Drinking water 213
SIC 9M muw The written consent of Pace AnalYlkal Semcks .firec FL NELAP E87627
PaceAmalyffalSorWees Jac
9800 10now Amp. Suite 100
HwbWlk AC 28D78,('!15c'ie Analj6cal Phiffil 704 875 9092mmPacelabs.cont Fax.[phone]
Lab Project Number :924979 3
Client Project ID : 03-JUL-0337/MI1356
QUALITY CONTROL DATA PARAMET ER FOOTNOTES
Consistent with EPA guidelines, usurounded concentrations are displayed and have been used to calculate 11;Rao and RPD values .
LCS(D)Laboratory Control Sample (Duplicate )
KS(D)Matrix spike (Duplicate)
Dup Sample Duplicat e
ED Not detected at or above adjusted reporting limit
NC Not Calculabl e
J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
XDL Adjusted Method Detection Limit
RPD Relative Percent Difference
(S)S=ogate
Ill RPD value was outside control limits, however both percent recoveries were acceptable . Sample results for the
QC batch were accepted hued on percent recoveries and completeness of QC data .
(21 Recovery falls outside of QC limits, however, this compound is not found in the associated samples .
(31 Analyte in found in the associated blank an well as in the sample (CLP E-Plag).
Dat*z 08/28/03 Pogo :20 of 2 0
CenrfiCatmtuh I
REPORT OF LABORATORY ANALYSIS KY Drinking Water 9DO90NCWastewater 1 2
NC Drinking Water 37706 This repon shall not oe reproduced, excePt in full, VA Drinking Water 213
SC 99DD6 without the witten consent of Pace Analtnical Semces . Inc FL NELAP E87627
CHAIN OF CUSTODY RECOMAND ANALYSIS REQUEST FORM5i Z
Analytical Laboratory Services i Fla iDukeA "Page X-ot-AMail Code MG03A2 (Building 7405)A DISTRIBUTIONI ~iPdftrEnergy..M39 Hagers Ferry Rd mpqss."
1~ 1CF41 - - ORIGINAL to LAS,
For Detailed Instructions, see : Huntereville,N . C. 28078 PCE~~,R , 1 !COPY to CLIENT
http ://devvww/essenv/oocJ (704) 875,5245 n W a
Fa :[phone].............. .E .........................
I)Pmject Name 2)Phone No :875-525 7
BURLINGTON MGP (SHAL FRACT BR WELLS)
E 3)Client C.Campbell R . Roberts 4)Fn No :875-5032
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DMW-1 0-X 1 1 3 1 re 6
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PMVVC-BR 7 A2.103 So x 1 1 3 1 6
C ki),4=iA -E PMWH-BR -7 1.22JO3 09?,q 4 .x 1 1 3 1
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CHAIN OF CUSTODY RECORPAND ANALYSIS REQUEST FORM
Duke Ana'W,~~,Ta X ;RR t
Mail Code MG03A2 (Building 7405)LIMS411 "Page of-A-
13339 Hagers Ferry Rd 9 s DISTRIBUTIONPahvEnergy..
For Detailed Instructions, see : Huntersville,N. C . 28078 B ORIGINAL to LAB,
httpJ/de~/essenv/coc/ [phone] COPY to
CLIENT
Fa :(704)$75-503 8.......................................A
1)PMI"t Name 2)Phone No : 875-5257
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PMWH-BR *7 122-1c,og?o 11,X I 1 3 1
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0 0 0CHAINOFCUSTODYRECORUAND ANALYSIS REQUEST FORM
Analytical Laboratory Services iDuke--------------------- - -----------"Page o fMall Code MG03A2 (Building 7405) -L
13339 Hagers Ferry Rd no DISTRIBUTIO NPakwEnergy.i Fro I to LAB ,Huntersville,N. C . 28078 !D oFor Detailed Instructions, see : [phone] COPY to CLIENThttp:Hde~1essenv1coc/Fa . k ......................... .
I)Prolewt Name 2)Phone Noi 875-5257BURLING TON MGP (SHAL FRA CT BR WELL S)
E 3)Cllent 4)Fax No ;875-5032C.Campbell /R . Roberts I C
2=H 0, 3=H
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C0,111)ProjectlD: MGPBURL 9)Actlvlty to: ALLACTV 10)Mall Code:MG03A3
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LAB USE ONLY 12 Chem "Collection Information o'
US < <-2"Lob 10 i Desktop NO ."Sample Description or ID :D:,:t,=Signature 0 o. 0-z 2 w w L)
DMW-I x 1 1 3 1 1 1 1 6
DMW-2 x 1 1 3 1 6
PMWC-BR x 1 1 3 1 6
E PMWH-BR x 1 1 3 1 6.2.0 PMWI-BR X 1 1 3 1
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August 13, 2003 5:29:19 PM Page #1 0 1
Duke Trace Metals
whEnergy..Case Narrativ e
(Fhis dc~ument must a=mpany release of Analytiml Data)
--- - ----------------
03-JUL-0337
LIMS Job #03-JUL-0338op .
03-JUL-033 9
Worklist #03-JUL-071 9
•Iron was analyzed in the method blank by ICP above the reporting limit . The
concentration of Fe was 0 .054 mg/L compared to the reporting limit of 0 .010
mg/L .
• All other QC associated with this data set is acceptable .
•The concentration of iron in Sample #23024S18 is between 5 and 10 times
that contained in the blank . Therefore, this result should be considered an
upper limit of the true concentration and should be used with caution .
•For sample 23024535,the concentration of iron in the sample is at a level
below 5 times that contained in the blank . This result must be considered to
be suspect .
All other samples contain iron in concentrations greater than 10 times that
contained in the blank . Therefore, those results are acceptable .
The data may be reported to the client with the above qualifications .
rj
.A--4 j
manqr~t-Gd~n-Karr,scie-nt-is*t
-------------------------------------------------------------------------------------
Duke Energy Analytical Laboratory Service s
Environment, Health &Safety Services Environmental Center - MG03A2
Phone:[phone] Hagers Ferry Road
FAX:[phone] Huntersville NC 28078-7929
Duke Duke Energy Analytical Laborator y
Phone :704-875~5245 Fax :[phone]lbergy.13339 Hagers Ferry Road Huntersville .NC 28078-7929
McGuire Nuclear Complex - MG03A2Ciertificalbe arAknaly-si s
New York State Department of Health Certification # 11717Olklahoma Department of Environmental Quality Certification ft 9930
Kansas Department of Health and Environment Cerfificate # E-1031 1
North Carolina Department Of Health &Human Services Certification #37804
South Carolina (DHEC)Laboratory ID # 99005 North Carolina (DENR) Certification #248
Station Name :BURLINGTON Job Number :03-JUL-0338
L --- ---.I
Sample ID #:23024521 Desktop #Customer ID :RALPH ROBERTS
Sample Description : DMW-1 (SHAL FRACT BIR WELLS )
Collection Date : 254ul-03 06 :45:00 Date Received in Laboratory: 14-Jul-03 Type of Sample : MGP SITE
RefenenceMethod :EPA31O .1/SM232OB Data Posted 8/101200323 :48 :50
ALKALINITY TOTAL INFLECTION POINT _ALKALINITY 0 .74 meql!,____
ReterenceMethod :EPA200.71601013 Data Posted :7/30/2003 16 :30 :24
IRON BY ICP (DIGESTED) - -IRON 0 .381 m /I
ReferenoeMethod :EPA200.716010B Data Posted 7/30/2003 16 :30:24
MANGANESE BY ICIP (DIGESTED)MANGANESE 0 .220 mg/L
Reference Method :EPA 300.0 Data Posted 7131/~003 11 35 03
MG-N/L BY CALCULATIO N
Reference Method :EPA 300.0 Data Posted : 713=003 15 :10:30
NITRATE IC)NITRATE 0 .68 mg/L
Reference Method :EPA 300 .0 Data Posted-7/2912003 15 54 4 7
SUILFATEAIC)-SULFATE 9 .86 m%/L---
Reference Method Data Posted 1112612003 15 28 58
VARIOUS SAMPLE TYPES SUBMITTED TO PACE PACE TEST COMPLETED
Sample ID #:23024522 Desktop #Customer ID:RALPH ROBERTS
Sample Description: DMW-2 (SHAL FRACT BIR WELLS )
Collection Date : 24-Jul-03 16:50 :00 Date Received in Laboratory: 144ul-03 TypeofSample :MGPSITE
ReferenceMelhod EPA310 .11SM2320B Data Posted 8110/2003 23 48 50
ALKALINITY (TOTAL INFLECTION POINT)_ALKALINITY 4 .62 meqIL.
Reference Method:EPA 200 .7/6010B Data Posted :7/3012003 13 56 45
IRON BY CID (DIGESTED) -IRON < 0 .100 mg/l
Referen~Method:EPA200.7160108 Data Posted 7130/2003 16 30 2 5
MANGANESE BY ICP (DIGESTED)MANGANESE 7 .471 mg/L.
Reference Method :EPA 300.0 Data Posted 7/3112003 11 35 0 5
MG-N/L.BY CALCULATION NITRATE <0 .02 mg-NIL
Refereni:oMethod EPA300 .0 Data Postedi 7130/2003 13 56 :4 5
NITRATE (IC)NITRATE < 0 .10 mg/L
Reference Method :EPA 300 .0 Data Posted :817/2003 13 :16 :28
SULFATE (IC)SULFATE 1 .01 mg/L
Vi .. . ... .. .ln";.No mG..... . ....1 812 -12003 Hy JA 23 h1Ip ://dc~ww/esse,iv/Iab-srW P.,,I ,,,
Duke Duke Energy Analytical Laborator y
Phone:[phone] Fax :[phone]
13339 Hagers Ferry Road Huntersville .NC 28078-7929
McGuire Nuclear Complex - MG03A 2
Cartificate of Aknaly-sirm
NewYorkState Department ofHealth Certification #11717Olcahoma Department of Environmental Quality Certification # 9930
Kansas Department of Health and Environment Certificate # E-1031 1
North Carolina Department of Health &Human Services Certification ft 37804
South Carolina (DHEQ Laboratory ID # 99005 North Carolina (DENR) Certification 4 24 8
Station Name :BURLINGTON Job Number :03-JUL-0338
Sample ID #23024522 Desktop #Customer 0: RALPH ROBERTS
Sample Description : DMW-2 SHAL FRACT 13R WELLS )
Collection Date : 24-Jul-03 16:50:00 Date Received in Laboratory : 14-Jul-03 TypeofSample :MGPSITE
Reference Method: Data Posted :812612003 15:29 :02
VARIOUS SAMPLE TYPES SUBMITTED TO PACE PACE TEST COMPLETED
Sample ID #:23024523 Desktop #Customer 10 :RALPH ROBERTS
Sample Description : PMWC-BR (SHAL FRACT EIR WELLS )
Collection Date : 22-Jul-03 16 :50 :00 Date Received in Laboratory: I&Jul-03 TypeofSample :MGPSITE
F
Reference Method :EPA310 .1/SM2320B Data Posted :8/10/2003 23 :48 :50
ALKALINITY (TOTAL INFLECTION POINT)ALKALINITY 3 .94 ni
ReferenmMethod :EPA200 .7/6010B Data Posted :8123/2003 11 :45 :45
IRON BY ICP (DIGESTED)--IRON 14.515 ringill
Reference Method :EPA 200 .7/60108 Data Posted :8/23/2003 11 :45 :45
MANGANESE BY ICP PtggSTED MANGANESE 3.361 mg/L
Reference Method :EPA 300b Data Posted :7/2812GO3 11 :27 :34
MG-NIL BY CALCULATION NITRATE <0 .02 mgAll_
Referenoe Method :EPA 300.0 Data Posted 7/2412003 15 :56 :1 6
NITRATE (I NITRATE < DID ni
Reference Method :EPA 300.0 Data Posted : 7t2512003 11 :23 :2 5
SULFATE(IC)_SULFATE 2 .02 mg/L
Reference Method: Data Posted :812612003 15 :29:0 7
VARIOUS SAMPLE TYPES SUBMITTED TO PACE -PACE TESTCOMPLEMED
Sample to #:23024524 Desktop #Customer ID :RALPH ROBERTS
Sample Description: PMWH-BR (SHAL FRACT BIR WELLS)
Collection Date . 22-Jul-03 09 :30 :00 Date Received in Laboratory : 14-Jul-03 Type of Sample MGP SITE
ReferenmMethod :EPA310 .1/SM23208 Data Posted:8110/2003 23 :46 :50
ALKALINITY (TOTAL INFLECTION POINT)ALKALINITY 4 .01 meq/L
ReferenceMethod EPA200 .7/6010B Data Posted:811212003 08 :00 :2 8
IRON BY ICP (DIGESTED)IRON 4 .605 mgll
ReferenceMethod EPA200,716010B Data Posted : 811 212003 08 :00 .2 8
MANGANESE BY ICP (DIGESTED)MANGANESE 3 .969 mg/L
VR,p,d G... . ... ...1 812-12003 01)~36 :23 hur,//d w .ZSSC"V/Iah_srV/P .,
Duke Duke Energy Analytical Laboratory
Phone :[phone] Fax [phone]Nerg.13339 Hagers Ferry Road Huntersville .NC28078-7929
McGuire Nuclear Complex - MG03A 2Certificate 4of fflinaly-ni a
New York State Department of Health Certification # 11717
Oklahoma Department of Environmental Quality Certification # 9930Kansas Department of Health and Environment Certificate # E-1031 1
North Carolina Department of Health &Human Services Cenificaton #37804
South Carolina (DHEC)Laboratory ID # 99MS North Carolina (DENR) Certificatori #248
Station Name :BURLINGTON Job Number :03-JUL-0338
Sample ID #:23024524 Desktop III Customer ID :RALPH ROBERTS
Sample Description : PMWH-BR (SHAL FRACT EIR WELLS )
Collection Date : 22,Jul-03 09 :30 :00 Date Received in Laboratory : 14-Jul-03 TypeofSample :MGPSITE
L
Reference Method :EPA 300 .0 Data Posted :712812003 11 :27 :3 5
MG-NIL BY CALCULATION NITRATE <-0 .02 mg-NIL
Reference Method :EPA 300.0 Data Posted : 7/2412003 15:56 :2 7
NITRATE (I NITRATE <_ 0 .10 mgIL__
Reference Method ;EPA 300.0 Data Posted :712512003 11 :23 :2 5
SULFATE (IC)SULFATE 0.16 L
Reference, Metinod : Data Posted 812612003 15 29 1 1
VARIOUS SAMPLE TYPES SUBMITTED TO PACE PACE TEST COMPLETED
Sample ID 9 : 23024525 Desktop #Customer ID :RALPH ROBERTS
Sample Description: PMWI-EIR (SHAL FRACT BR WELLS)
CollectionDate: 21-Jul-0317 :20 :00 Date Received in Laboratory : 114,1ul-03 TypeofSample :MGPSITE
F-
RefefenceMethod :EPA310 .1/SM2320B Data Posted:8/10/2003 23 :48 50
ALKALINITY110TAL INFL~CTION POINT)___ALKALINITY 5.32 meq/L
ReferenceMethod EPA200.716010B Data Posted:8/1212003 08 :00 :28
- -[RON BY ICP (DIGEVED)____..-I-RON--.2 .770 rin gLI
ReferenceMethod :EPA200.716010B Data Posted 8/1212003 08 00 29
MANGANESE BY ICP(DIGES~TED)MANGANESE 4 .106 mqrL.
Reference Method :EPA 300.0 Data Posted :7/25/2003 10 :27:08
111i BY CALCULATION NITRATE <0.02 mg-NIL
Reference Method :EPA 300 .0 Data Posted : 7/24/2003 14 :55:1 5
-NITRATE (IC)NITRATE < 0 .10 mg/L
Reference Method :EPA 300 .0 Data Posted: 7124/2003 14 :20:4 6
SULFATE (IC)SULFATE 15 .86 mg/L
Reference Method Data Posted :8/26/2003 15 :29 :1 6
VARIOUS SAMPLE TYPES SUBMITTED TO PACE PACE TEST COMPLETED
0
... ...812-12003 U9,34 23 hap //d,www/essenv/lab-,,rv/
Duke Duke Energy Analytical Laboratory
Phone:[phone] Fax :704-87~,5038PeEnergy.13339 Hagers Ferry Road Huntersville .NC28078-7929
McGuire Nuclear Complex - MG03A 2Ciertiflc--ate ar Amnalyr~u s
New York State Department of Health Certification # 11717
Oklahoma Department of Environmental Quality Certification # 9930Kansas Department of Health and Environment Certificate 9 E-1031 1
North Carolina Department of Health &Human Services Certification It 37804
South Carolina (DHEC)Laboratory ID # 99005 North Carolina (DENR) Certification 9 24 8
Station Name :BURLINGTON Job Number:03 -JUL-0338
Sample ID #: 23024526 Desktop At Customer 10:RALPH ROBERTS
Sample Description : PMWM-BR (SHAL FRACT EIR WELLS )
Collection Date : 21-Jul-03 13 :00 :00 Date Received in Laboratory : 14-Jul-03 TypeofSample :MGPSITE
Referencelviethod :EPA310.11SM232013 Data Posted :Bit 012003 23 48 50
ALKALINITY (TOTAL INFLECTION POINT) ALKALINITY 1 .01 me IL
ReferenceMethod :EPA200 .71601013 Data Posted :811212003 08 :00:29
IRON BY ICP (DIGESTED)IRON ---- - -0.959 mg/I
ReferenceMethod :EPA200 .7160110B Data Posted :8/1212003 08 :00:29
MANGANESE BY ICP (DIGESTED)MANGANESE
Reference Method :EPA 300 .0 Data Posted :7/25/2003 10 :27:0 9
Iii BY CALCULATION NITRATE 0 .60 m -N/L
Reference Method :EPA 300.0 Data Posted : 7/24/2003 14 :54 :5 5
NITRATE [IC)NITRATE 2 .67 mg/L
Reference Method :EPA 300~O Data Posted 712412003 14 20 4 5
SULFATE C),SULFATE 24.36 rriIM
Reference Method : Data Posted 8126/2003 15 :29 20
VARIOUS SAMPLE TYPES SUBMITTED TO PACE PACE TEST COMPLETED
Sample ID #: 23024527 Desktop At Customer ID :RALPH ROBERTS
Sample Description : PMWL-BR (SHAL FRACT BR WELLS )
Collection Date : 24-Jul-03 10 :46:00 Date Received in Laboratory : 14-Jul-03 TypeofSample :MGPSITE
ReferenceMethod :EPA310.1/SM2320B Data Posted 8/1012003 23 48 :50
- - -ALKALINITY (TOTAL INFLECTION POINT)___ _____ALKALINITY 2.62 Teq/L
Reference Method :EPA 200.7/6010B Data Posted :7/30/2003 16:30 :2 5
IRON BY ICP (DIGESTED)IRON 0.371 mg/I
Reference Method :EPA 200.7/601 013 Data Posted:713012003 16 :30 :25
MANGANESE BY ICP (DIGESTED)MANGANESE 0.383 mg/L
Reference Method :EPA 300.0 Data Posted 7/3112003 11 35 :08
MG-N/L BY CALCULATION NITRATE <0 .02 mg-N/L
Reference Method EPA 300.0 Data Posted :7130/2003 13 57 :36
NITRATE (C)NITRATE <0.10 mgIL
Reference Method :EPA 300,0 Data Posted 7/30/2003 13 57 :3 6
SULFATE (IC)SULFATE 17 .16 mg/L
Vimiu,.,,Ih,- finmN~,.,K12-12003 09 36 .23 hl1p :/Idewww/essenv/lab-srv/
Duke Duke Energy Analytical Laborator y
Phone:[phone] Pax :704-875-5038PoEnergy.13339 Hagers Ferry Road Huntersville .NC28078-7929
McGuire Nuclear Complex - MG03A 2
Ce-rtlflcata 4of ^n zatlysis
New York State Department of Health Certification # 11717
Oklahoma Department of Environmental Quality Cernificabion # 9930
Kansas Department of Health and Environment Certificate 9 E .103111
North Carolina Department of Health &Human Services Certification #378D4
South Carolina (DHEC)Laboratory ID # 99DO5 North Carolina (DENR) Certification #248
station Name :BURLINGTON Job Number:03-JUL-0338
Sample ID #: 23024527 Desktop #Customer ID:RALPH ROBERTS
Sample Description : PMWL-BR (SHAL FRACT BR WELLS )
Collection Date : 24-Jul-03 10 :45 :00 Date Received in Laboratory : 14-Ju"3 TypeofSample :MGPSITE
Reference Method : Data Posted 8126/2003 15 :29:25
VARIOUS SAMPLE TYPES SUBMITTED TO PACE PACE TEST COMPLETED
i/~__ -
DataJenfiedandAppmmday,oate
0
Nom
812-12003 09 362 ;http ://d,~w%v/ese~ivl/liib-srv/1", IW 5
Duke Duke Energy Analytical Laborator y
Phone :704,875-5245 Fax:[phone]anerg.13339 Hagers Ferry Road Huntersville,NC28078-7929
McGuire Nuclear Complex - MG03A 2
Cortificaltei of Analysi s
Now York State Department of Health Certification # 11717
Olklahoma Department of Environmental Quality Certification # 9930
Kansas Department of Heath and Environment Certificate 9 E-1031 1
North Carolina Department of Health &Human Sermces Cent icabon # 37804
South Carolina (DHEC)Laboratory ID # 99305 North Carolina (DENR) Certification 9 248
SamplelD#: 23024521 job#:03-JUL-033 8
Sample Description:DMW-1 (SHAL FRACT BR WELLS )
Collection Date : 25-Jul-03 06 :45 :00 Site :BURLINGTON Sample Type: MGP SITE Desktop #
01313 PARAMETERS IN WATER BY GCIMS - 8260
Test Code : MS8260MGPW Test Method : SW-846 5030B18260B Date Posted :07128103
Result Reporting Limit -frla9-
Bemene < 0 .50 pg/L 0.50 pg/L 0
Toluene < 1 .0 pg/L 1 .0 pg/L 0
Ethylberizene < 1 .0 Vgtl .1 .0 pgll. 0
rn-p-Xylene <2 .0 pglL 2 .0 pg/L 0
o .Xylene < 1 .0 Vg/L 1 .0 pgf. 0
Sample ID #:23024522 Job#:03-JUL-0338
Sample Description :DMW-2 (SHAL FRACT BR WELLS )
ellection Date : 24-Jul-03 16 :50 :00 Site :BURLINGTON Sample Type: MGP SITE Desktop #
OGP PARAMETERS IN WATER BY GC/MS - 826 0
Test Code : MS8260MGPW Test Method : SW-846 6030818260B Date Posted :07/28103
Result Re Limit Flag
Benzene 85 pg/L 0.50 pg/L 0
Toluene 9.7 pg/L 1 .0 pg/L 0
Ethylbenzene 130 pg/L 1 .0 pg/L. 0
m-p-Xylene 43 pg/L.2.0 pg/L 0
o-Xylene 47 pg/L 1 .0 pg/L 0
T Iny 77, ~;~7:TE777 74-77
SamplelD#: 23024623 Job#:03-JUL-033 8
Sample Description :PMWC-BR (SHAL FRACT BR WELLS )
Collection Date 22-Jul-03 16 :50 :00 Site :BURLINGTON Sample Type: MGP SITE Desktop #
RF ~-=77--W ~z '
*GP PARAMETERS IN WATER BY GC/MS - 826 0
Test Code : MS8260MGPW Test Method : SW-846 503013/826013 Date Posted :07/28/03
Result Reporting Limit Fla g
Bemene 5.3 Vg/L.2 .6 pg/L 0
Toluene < 5.0 pglL 5 .0 pg/L 0
Ethylbenzene 11 pg/L 5 .0 pglL 0
m-p-Xylene < 10 Vg/L 10 pg/L 0
Vilt,", ~,,, 111~Int,aNdal
.12-11,1113,19 41,12 litip :Hdc~yww/es~env/lab-.srv/
Duke Duke Energy Analytical Laborator y
Phone :[phone] Fax :[phone]lbergy.13339 Hagers Ferry Road Huritersville .NC 28078-7929
McGuire Nuclear Complex - MG03A 2
Cartificate of Analysis
Now York State Department of Health Certification 9 11717Oklahoma Department of Environmental Quality Certification # 9930
Kansas Department of Health and Environment Certificate 4 E-1031 1
North Carolina Department of Health &Human Services Certification #37804
South Carolina (DHEC)Laboratory ID # 99005 North Carolina (DENR) Certification 9 248
~M
Sample ID #:23024523 Job#: 03,JUL-033 8
Sample Description :PMWC-BR (SHAL FRACT EIR WELLS )
Collection Date : 224ul-03 16 :50:00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
~GP PARAMETERS IN WATER BY GCtMS -82B o
Test Code : MS8260MGPW Test Method : SW-846 5030B18260B Date Posted :07128/03
Result Reporting Limit Flag_
o-Xylene 10 pg/L 5 .0 0911-0
Sample ID #:23024524 Job#: 03-JUL-0338
Sample Descdption :PMWH-BR (SHAL FRACT EIR WELLS )
Collection Date: 22-Jul-03 09 :30:00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
rP PARAMETERS IN WATER BY GC/MS - 8260
1W Test Code : MS8260MGPW Test Method : SW-846 6030B18260B Date Posted :07/28103
Result ReiD-od~mlt Flag
Benzene 4.5 pg/L 2 .6 pg/L 0
Toluene 6A jiglL 5.0 Pg/L 0
Ethylbenzene 38 pg/L 5.0 p9lL 0
m-p-Xylene 23 ug/L 10 P911-0
o.Xylene 22 pg/L 5.0 P911-0
SamplelD#: 23024525 Job#: 03,JUL-033 8
Sample Description :PMWI-BR (SHAL FRACT BR WELLS )
Collection Date : 21-Jul-0317 :20:00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
"Mll , '1111 1 M I 111 11111111111111111 1 ~ MgVTUM7~
~FGP ARAMETERS IN WATER BY GC/MS - 8260
Test Code : MS8260MGPW Test Method : SW-846 503OB/8260B Date Posted :07128103
Result Reporting Limit Fla g
Benzene 150 Vg/L 2.5 V911-0
Toluene 5.2 pq/L 5.0 pgtL 0
Ethylbenzene 180 pg/L 5.0 pglL 0
m .p.Xylene 30 pg/L 10 pgr- 0
o.Xylene 97 ug/L 5.0 pglL 0
Visa . .. ...hwaNoat
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Duke Duke Energy Analytical Laboratory
Phone [phone] Fax :[phone]
13339 Hagers Ferry Road Huntersville .NC 28078-7929
McGuire Nuclear Complex - MG03A2
Cartificate of Analysis
New York State Department of Health Certification # 11717Oklahoma Department of Environmental Quality Certification # 9930
Kansas Department of Health and Environment Certificate # E-1031 1
North Carolina Department of Health &Human Sermces Certification 4 37804
South Carolina (DHEC)Laboratory ID # 99(X15 North Carolina (DENR) Certification #248
Sample]D#: 23024526 Job#: 03~JUL-0338
Sample Description :PMWM-BR (SHAL FRACT EIR WELLS )
Collection Date: 21-Jul-03 13:00:00 Site :BURLINGTON Sample Type : MGF,SITE Desktop #
01312 PARAMETERS IN WATER BY GCIMS - 8260
Test Code : MS8260MGPW Test Method : SW-846 5030B18260B Date Posted :07128103
Result ___f!eeq"in Limit RaL
Benzene 0.50 pg/L 0 .60 pqtL 0
Toluene < 1 .0 pg/L 1 .0 pg[L 0
Ethylbenzene 2 .3 ptill. 1 .0 pg/L 0
m-p-Xylene 8 .0 pg/L 2 .0 pqtL 0
~Xylene 4.0 pgVL 1 .0 Pg/L 0
Sample ID #: 23024527 Job#:0311jUL-033 8
ample Description :PMWL-BR (SHAL FRACT EIR WELLS )
illection Date: 24,Jul-03 10 :45 :00 Site :BURLINGTON Sample Type : MGP SITE Deskto p
OGP PARAMETERS IN WATER BY GCIMS - 8260 _71
Test Code : MS8260MGPW Test Method : SW-846 5030B/8260B Date Posted :0712810 3
Result _Reparting Limit Rag
Benzene < 0 .50 pg/L 0.50 pgtL 0
Toluene < 1 .0 pg/L 1 .0 pq11-0
Ethylbenzene < 1 .0 pg/L 1 .0 pq1L 0
nn-p-Xylene <2 .0 p9/1-2.0 pgtL 0
o-Xylene < 1 .0 pg/L 11 .0 pg/L 0
------------------------------------
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Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100aneAnalXicalHuntersville,NC 28078
Phone :[phone]
Fax :[phone]
August 21,200 3
Mr . Paul J .Fitzgerald
Duke Power
Mail Code :MG03A2
13339 Hagers Ferry Road
Huntersville,NC 28078-792 9
RE : Client Project ID :03-JLJL-039/Mll 356
Pace Project ID : 924779 6
Dear Mr . Fitzgerald :
I am writing in regards to your concerns about the recovery of the acid surrogates in several of the
samples associated with the above referenced project .
I have reviewed the extraction log and the raw data for these samples and believe that this is an
extraction problem with these samples . Four of the samples (23024532/PMWC-S ;
23024516/PMWC-D ; 23024523/PMWC-BR ; 23024524/PMWH-BR) emulsified during the
extraction process . As stated in the laboratory report, there was insufficient sample volume available
for reextraction and reanalysis of these samples .
LCS 923180525,which was extracted alongside the samples, shows acceptable recoveries for
phenol-d5 and 2-fluorophenol . Other samples analyzed on the same day but not extracted on the
same day show recoveries for these two surrogates in the range of 50-70%recovery . Therefore,I do
not believe that the low recoveries are caused by a problem with the instrumentation .
Our acceptance limits for phenol-d5 and 2-fluorophenol are 10-125%,which are consistent with
EPA data for these surrogates .
If you have any additional questions or need additional information, please contact me at
704-875-9092 Ext .229 .
Sincerely yours,
Mavis Jones
Quality Manager
Ross AnillytiC81 Serview IRV
98LV ftity Amm $vlle 100
Motaryw1k AC 28078715c'emalyticalsis Phorw 70f 875 9092
wwt,ii.pacelabs.com Far 704.875.9091
auquat 28,200 3
Kr . Jay Perkins
Duke Power
13339 Nagers Ferry Road
U030A2
Hunterouille,KC 2607 6
RE :Lab Project Numbers 924979 4
Client Project IDs 03-TUL-0336/01356
Do"Kr . Perkines s
Enclosed are the ...lytLcal ressulte for sample(a)received by the laboratory on July 23, 2003 .Results reported
herein conforia to the met current NzUC scandarde, here applicable, unless othereile lawarrated in the body of
the report .
if you have my questione concerning this report Planar,feel free to contact nw .
ginceraly ,
Kristi Tart
Kriati .Tartepacelsibe .con,
Project Massager
Enclonurais
2Itrinjarom Certification ID REPORT OF LABORATORY ANALYSIS KY Druilung Water 9DD90NCWastewater 1 2
NC Drinking Water 37106 Thin report shelf not be reproduced,irsirept in full,VA thinking Water 213
SC 9M without the witten conisint of Pam Asiallucal Services.1M .FL NELAP E87627
Pago Anifivilefil $81film, Inc.
98X Kiww AywA Sub 100
HalWSW11A AC 28078ZuciumalyticalPhorw 704 875 9LI92
winninfiepsoelabs .com Far 704.875.9091
Lab Project Number ; 924979 4
Client Project ID :03-JUL-0338/NI135 6
Lab Sample No :923172050 Project Sample Number : 9249794-001 Date Collected :07/22/03 16 :50
Client Sample ID ;23024523/PKKC-BR Matrix : Water Date Received :07/23/03 11 :50
Parameters Unitz Rewrt Limit Analyzed BY CA.S No .Oual RwLm t
GCIKS Sentivolatiles
Sainivolatile Organics Prep/Method : EPA 827 0
Acenaplatheme 210 ug/1 50 . 07/29/03 12 :31 BUT 83-32-9
Aceoulphthyliale, 24 .ug/l 10 . 07/29/03 12 :31 BET 208-96-8
Aniline KID ug/l 10 . 07/29/03 12s3l BET 62-53-3
Anthracene 20 .ug/l 10 . 07/29/03 12 :31 BET 120-12-7
Benno (a) anthraceppe ND ug/l 10 . 07/29/03 12 :31 BET 56-SS-3
Bmzo(&)pyrme ND ug/l 10 . 07/29/03 12 :31 BET 50-32-8
Bwzo (b) f luoranthene ED ug/l 10 . 07/29/03 12 ;31 BET 205-99-2
Bmzo(g,h,i)perylme ED ug/l 10 . 07/29/03 12 :31 BET 191-24-2
Banco (k) f lucranthene,ND ug/l 10 . 07/29/03 1201 BET 207-08-9
Benzoic acid ND ug/l 50 . 07/29/03 12 :31 BET 65-85-0
Sfanzyl alcohol ND ug/l 20 .07/29/03 12 :31 BET 100-51-6
4-Bramophertylpheetyl ether ND ug/l 10 . 07/29/03 12 :31 BET 101-55-3
Butylbefoxylphithislate ND ug/l 10 . 07/29/03 12 ;31 BET 85-68-7
4-Chloro-3-methylphenol ND ug/l 20 .07/29/03 12 :31 BET 59-50-7
4-Chloroagailine ED ug/l 20 .07/29/03 1201 BET 106-47-8
bin (2-Chloroathox0mathearm ND ug/l 10 . 07/29/03 12 :31 BET 111-91-1
bio(2-Chloroothyl) ether ND ug/l 10 . 07/29/03 1201 BET 111-44-4
bia(2-Chloroisopropyl) ether ND ug/l 10 . 07/29/03 12 :31 BET 39638-32-9
2-Chloronaphthalene ED ug/l 10 . 07/29/03 12 ;31 BET 91-58-7
2-Chlorophemol ED ug/l 10 . 07/29/03 12 :31 BET 95-57-8
4-Chlarophenylphanyl ether ND ug/l 10 . 07/29/03 12 :31 BET 7005-72-3
Chrysene ND ug/l 10 . 07129/03 12 :31 BET 218-01-9
Dibraaz (a,h)anthracene ED ug/l 10 . 07/29/03 12 :31 BET 53-70-3
Dibenzofuraza 23 . ug/l 10 . 07/29/03 12 :31 BET 132-64-9
1,2-Dichlorobertzene ND ug/l 10 . 07/29/03 12 :31 BET 95-50-1
1,21-Dichlorobeatzene ND ug/l 10 . 07/29/03 12 :31 BET 541-73-1
1,4-Dichloroberizene ND ug/l 10 . 07/29/03 12 :31 BET 106-46-7
3,3--DichlorobenzidinG ND ug/l 20 .07/29/03 12 :31 BET 91-94-1
2,4-Dichlorophenal ND ug/l 10 . 07/29/03 12 :31 BET 120-63-2
Diethylphthalate ND ug/l 10 . 07/29/03 12 :31 BET 04-66-2
2,4-Dimethylphanol ND ug/l 10 . 07/29/03 12 :31 BET 105-67-9
Dimathylphthalate ND ug/l 10 . 07/29/03 12 :31 BET 131-11-3
Di-n-butylphthalate ND ug/l 10 . 07/29/03 12 :31 BET 64-74-2
41,6-Diraitro-2-mathylphenol MD ug/l 50 . 07/29/03 12 :31 BET 534-52-1
2,4-Dinitrophanol ND ug/l 50 . 07/29/03 12 :31 BET 51-28-5
2,41-Dinitrotaluene ED ug/l 10 . 07/29/03 12 :31 BET 121-14-2
2,6-Dinitrotoluene ND ug/l 10 . 07/29/03 12 ;31 BET 606-20-2
Date,08/28/03 plig.; I of 20
lifferal,tv Unification U2a REPORT OF LABORATORY ANALYSIS Ky Drir,Wng Water 90090NCWasts"Illf 1 2
NC Drinking Water 37706 This report shall not be produced, exupt in full . VA Drinking Water 213
SC 9M without the mitten consent of pace AnalYfical Serlices . Im ft NELAP E87627
Pace AR8101981 SerWess,Inc.
M rincey Ayww,Whi 100
HMVW11e,NC 280782cema0cal"'Phone [phone]M
PPvPivPace1abs .coM Far 704.875.9091
Lab Project Number : 9249794
Client Project ID : 03-JUL-0338/MI135 6
Lab Sample No ;923172050 Project Sample Number : 9249794-001 Date Collected :07/22/03 16 :50
Clisat Sample ID : 23024S23/PKWC-Bk Xatrix : Water Date Received :07/23/03 11 ;50
Parameters Reault!) Units RMrt Limi ..ARE1yLcd --ft-ChS No . Cruel gegzza t
Di-n-ocitylpitthalate ED ug/l 10 . 07/29/03 1201 BET 117-84-0
1,2-Dipbmylhydrazine up uq/I 20 .07/29/03 12 :31 BET 122-66-7
bia(2-Ithylhaxyl)phthalate No USA 10 . 07/29/03 12 :31 BET 117-81-7
Pluoranthene No USA 10 . 07129/03 1201 BET 206-44-0
Fluorecia 48 .ug/l 10 . 07/29/03 12 :31 BET 86-73-7
Sexachloro-1,3-butadiame ND USA 10 . 07/29/03 12&31 BET 87-68-3
Sexachlorobenzece No USA 10 . 07/29/03 12 :31 BET 118-74-1
sexachlorocyclopewitadiece No ug/I 10 . 07/29/03 12 :31 BET 77-47-4
R-e-chloroathaus ND ug/l Ia . 07/29/03 1201 BET 67-72-1
Indaw (1,2,31-eftyrane ED ug/l 10 . 07/29/03 12 :31 BIT 193-39-5
Isophorone,ED uq/I 10 . 07/29/03 12 :31 BET 78-59-1
2-Methy1naphthalene 30 . USA 10 . 07/29/03 12 :31 BET 91-57-6
2-Kethylphemol (o-Cresol)No ug/I 10 . 07/29/03 12 :31 BET 95-48-7
364-Methylphemol ED uq/1 10 . 07/29103 12 :31 BET
Naphthalene 160 uq/l 50 . 07/29/03 1201 BET 91-20-3
2-Nitromiline No ug/l 50 . 07/29/03 12 :31 BET 88-74-4
3-Nitroaniline ED uq/I 50 . 07/29/03 12 :31 BET 99-09-2
4-Hitromiline No uar/I 50 . 07/29/03 12 .31 BET 100-01-6
Mitrobenzwe ED USA 10 . 07/29/03 12 :31 BET 98-95-3
2-Nitrophimaol No USA 10 . 07/29/03 12 :31 BET 88-75-5
4-Nitropheriol ED ug/l 50 . 07/29/03 12 :31 BET 100-02-7
N-Nitrosodimthylazine ED ug/l 10 . 07/29/03 12 :31 BET 62-75-9
N-Nitroso-di-n-propylaagine ED ug/1 10 . 07/29/03 1201 BET 621-64-7
N-Nitrosodiphenylemine No ug/I 10 . 07/29/03 12 :31 BET 06-30-6
Pentachlorophignol ED uq/l 50 . 07/29/03 1201 BET 07-86-5
Pheinauthrens,89 . ug/l 10 . 07/29/03 12 :31 BET 85-01-8
Phenol ED ug/1 10 . 07/29/03 12 :31 BET 108-95-2
Pyrerie No Ug/I 10 . 07/29/03 12 :31 BET 129-00-0
1,2,4-Trichlorobsoczene No USA 10 . 07/29/03 12 :31 BET 120-82-1
2,41 .5-Trichloropheaud.No ug/l 50 . 07/29/03 12 :31 BET 95-95-4
2,4,6-Trichlorophawol ED ug/I 10 . 07/29/03 12 :31 BET 88-06-2
Nitrobecutene-dS (S) 73 % 07/29/03 12 :31 BET 4165-60-0
2-Fluortibiphanyl (S) 70 % 07/29/03 12 :31 BUT 321-60-8
Terpheiryl-,114 (S) 76 It 07/29/03 12 :31 BET 1718-51-0
Phecol-d5 (S)2 11, 07/29/03 12 :31 BET 4165-62-2 1,2
2-Fluorophanol (S) 3 07/29/03 12 :31 BET 367-12-4 1,2
2,41,6-Tribromophenol (S) 39 07/29/03 12 :31 BET
Date Extracted 07/25/03 07/25/0 3
Data :00/28/03
Page : 2 of 2 0
I aboratory Certification IDS REPORT OF LABORATORY ANALYSIS KY Drinking Water 900110NCWastweater 12
KorinkingiWater 37106 This report "it wit be r4P,0,k1QXJ,excOPI in full. VA Drindra Water 213
SC 9M without the witten torment ol Pace AnaVical Ser*as . Im FL NELAP E87627
Pat Anelyticst Services toe
9MGnMAww.Svd9100
HulftWik NC 28078ZemaiXicarMove704.8759092
mw.pacelabs .com Far M.875.9091
Lab Project Number : 924979 4
Client Project ID ;03-JUL-0338/MI135 6
Lab Sample No :923172060 Project Sample Number : 9249794-002 Date collected :07/22/03 09 :30
Client Sample ID :23024524/PMWH-BR Katris~ Water Date Received ;07/23/03 11 :50
Parameters Result@ Units Report Limi Analyzed BY CAB NO .Oual Sealant
GC/KS sentivolatiles
Seenivolatile Organics Prep/method : Spit 827 0
Acenaphthene 300 ug/l 200 07/29/03 08 :00 BET 63-32-9
Acenaphthyleme 13 . ug/1 10 . 07/29/03 08 :00 BET 208-96-8
Aniline ND ug/1 10 . 07/29/03 08 :00 BET 62-53-3
Anthr&c=e 16 . ug/l 10 . 07/29/03 MOO BET 120-12-7
Beaten (a) anthracene NO ug/l 10 . 07/29/03 MOO BET 56-55-3
Santo (a) pyrme 14) USA 10 . 07/29/03 08 :00 BET 50-32-8
Swan (b) f luartuatheam NO ug/1 10 . 07/29/03 08 :00 BET 205-99-2
Bezuso(g'h,i)PGrylaae NO ug/1 10 . 07/29/03 06 :00 BET 191-24-2
Benno (k) fluoranthene,ND Ug/l 10 . 07/29/03 08 :00 BET 207-08-9
BenZOiC acid NO ug/l 50 . 07/29/03 08 :00 BET 65-85-0
Bawaxyl alcohol NO ug/l 20 .07/29/03 08 :00 BET 100-51-6
4-Bromophonarylphanyl other NO USA 10 . 07/29/03 08 :00 BET 101-55-3
Butylbenzylphthalate NO ug/l 10 . 07/29/03 MOO BET 85-68-7
4 -Chloro-3 -mathylphonol ND USA 20 .07/29/03 08 :00 BET 59-50-7
4-Chloroaniline NO ug/l 20 .07/29/03 06 :00 BET 106-47-8
bin (2 -ChloMetboXY) Mth-6 NO ug/1 10 . 07/29/03 08 :00 BET 111-91-1
bis(2-Chloroothyl) Other NO USA 10 . 07/29/03 MOO BET 111-44-4
bio(2-Chloroisopropyl) other NO USA 10 . 07/29/03 08 :00 BET 39638-32-9
2-Chlorowaphthalone ND ug/l 10 . 07/29/03 08 :00 BUT 91-58-7
2-Chlorophemol NO ug/l 10 . 07/29/03 08 :00 BET 95-57-B
41-Chlorophonylphertyl other NO ug/l 10 . 07/29/03 08 :00 BET 7005-72-3
Chrysene NO ug/1 10 . 07/29/03 08 :00 BET 218-01-9
Dibezz (a, h) anthracene NO ug/l 10 . 07/29/03 08 :00 BET 53-70-3
Dib=zofur= 28 .ug/1 10 . 07/29/03 06 :00 BET 132-64-9
1,2-Dichlorobenzene ND ug/l 10 . 07/29/03 08 :00 BET 95-50-1
1,31-DichlorobafflZme NO ug/l 10 . 07/29/03 08 :00 BET 541-73-1
1,4-Dichloroboxasene,NO ug/l 10 . 07/29/03 08 :00 BET 106-46-7
3,31-Dichlorobenzidine NO ug/l 20 .07/29/03 08 :00 BET 91-94-1
2,4-Dichlorophmol ND USA 10 . 07/29/03 08 :00 BET 120-83-2
Diethylphthalate NO ug/l 10 . 07/29/03 08 :00 BET 84-66-2
2,4-Dimthylphmol ND ug/l 10 . 07/29/03 08 :00 BET 105-67-9
Dimethylphthalate NO ug/l 10 . 07/29/03 08 :00 BET 131-11-3
Di-a-butylphthalate NO ug/1 10 . 07/29/03 08 :00 BET 04-74-2
4,6 -Dinitro-2 -Mthylphon0l ND uq/1 50 . 07/29/03 00 :00 BET 534-S2-1
2,4-Dinitrophazol NO ug/l 50 . 07/29/03 08 :00 BET 51-28-5
2,4-Dinitrotolume NO ug/l 10 . 07/29/03 08 :00 BET 121-14-2
2,6-Dinitrotolume NO ug/l 10 . 07/29/03 06 :00 BET 606-20-2
Pa,e :3 of 20Data:00/38/03
lmorwouREPORT OF LABORATORY ANALYSIS Ky Drinking Water 9MNCWastermter 1 2
NC Drinking Water 37706 This report shall not be reproduced . exupt in full, VA Drinking Water 213
SC 99OD6 unths the witten consent of Pate AMOW SerMIM.111C Fl.NELAP E87627
Pace Angl4liest Serriew,11w.
9800 KIway Amai Sude 100
fliell HunhisW11A AC 28078
a L
.Mnalyfical"a Phigno 704.875.9W
VVIVIvloacelabsoom Far 704.875.9091
Lab Project Number : 924979 4
Client; Proj act ID :03-JUL-0338/MI135 6
Lab Sample No :923172060 Project Sample Number : 9249794-002 Date Collected :07/22/03 09 :30
Climatic Sample ID : 23024524/P)M-BR Matrix : Water Date Received ;07/23/03 11 :50
Results Units Retort Limit Analysed By Chs No .Qual RwLmt
Di-n-octylphthalate ND USA 10 . 07/29/03 08 :00 BFT 117-64-0
1,2-Diplarsay1hydraziner ND ug/l 20 .07129/03 08 :00 BET 122-66-7
bia(2-Ztbylhexyl)phthalate BID ug/l 10 . 07/29/03 41800 BET 117-01-7
Fluarmth=O ND ug/l 10 . 07/29/03 08 :00 BET 206-44-0
Pliscirease 57 . ug/l 10 . 07/29/03 08 ;00 BET 86-73-7
Rexamblorts-1 1 3 -butadieue KID ug/l 10 . 07/29/03 0800 BET 87-66-3
Haxachloroberuseess BID ug/l 10 . 07/29/03 08 :00 Bffr 110-74-1
Hessichlorocyclopeastadireme BID ug/l 10 . 07/29/03 00 :00 SET 77-47-4
Hims-obloroetbane SID ug/l 10 . 07/29/03 00 :00 EST 67-72-1
Indears(1,2,31-cftyreass ED ug/l 10 . 07/29/03 0800 BRT 193-39-5
leophormate ND ug/l 10 . 07/29/03 0800 NET 70-59-1
2-Hathyltiaphthrelease 290 ug/l 200 07/29/03 08 :00 BRT 91-57-6
2-Methylpheacil (o-Crefol)ND ug/l 10 . 07/29/03 00100 BET 95-48-7
U4-Mathylphraccol ND ug/l 10 . 07/29/03 08 :00 BET
Naphthalene 980 Ug/l 200 07/29/03 08 :00 BET 91-20-3
2-Mitrowiline BID ug/l 50 . 07/29/03 08 ;00 BET 00-74-4
3-Mitroamiline ND ug/l 50 . 07/29/03 08 :00 BET 99-09-2
4-Nitmaniline ED ug/l 50 . 07/29/03 08 :00 BZT 100-01-6
Mitroberizease ND uq/l 10 . 07/29/03 08,00 BET 98-95-3
2-Kitropherfol ND ug/l 10 . 07/29/03 08 ;00 BET 68-75-5
4-Nitrophesool ND ug/l 50 . 07/29/03 08 :00 BET 100-02-7
N-Nitrosodimethylamine ND ug/l 10 . 07/29/03 08 ;00 BET 62-75-9
M-Nitroso-di-n-propylamine ND ug/l 10 . 07/29/03 08 :00 BIT 621-64-7
M-Nitrooodiphmylamine ND ug/l 10 . 07/29/03 08 ;00 BET 86-30-6
Peritachlorophreacil ND USA 50 . 07/29/03 08 :00 BET 97-86-5
Phenticathrexte 09 . ug/l 10 . 07/29/03 08 :00 BET 65-01-8
Phessol ND ug/l 10 . 07/29/03 08 :00 BET 108-95-2
Pyrwa ND Ug/l 10 . 07/29/03 08 :00 BET 129-00-0
1,2,4-Trichlorisbanzene BID ug/l 10 . 07/29/03 08 :00 BET 120-82-1
2,4,5-Trichlorcpbeecil ND ug/l 50 . 07/29/03 08 :00 BET 95-95-4
2,4,6-Trichlorophemol ND uq1l 10 . 07/29/03 08 :00 BET 08-06-2
Nitroberizene-0 (S) so Is 07/29/03 09 :00 BET 4165-60-0
2-Fluorobiph"yl (S) 68 % 07/29/03 08 :00 BET 321-60-0
Torphmyl-dl4 (S) 72 07/29/03 08 :00 BET 1718-51-0
Phattool-,15 (S)2 07/29/03 08 :00 BET 4165-62-2 1,2
2-Fluorophezi (S)4 07/29/03 08 :00 BET 367-12-4 1,2
2,4,6-Tribramopherriol (S)49 07/29/03 08 :00 BET
Date Rictracted 07/25/03 07/25/0 3
Data :08/28/03 Page : 4 of 20
liturgralnN can fication I
I aborstory COrtilkalkIn IU REPORT OF LABORATORY ANALYSIS KY Drinking Water 9MNCWastrarater 1 2
NC Drinking Water 37706 This report shall hot be reproduced . except in full, VA Drinking Water 213
SC 99DO6 urithout the wifien Consent of Pam "hi ServiCn.Inc Fl.NELAP E87627
Pace Atislyticiff Soriffices,Inc.
9W Kinney Aww, Svib 100
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Lab Project Number ; 924979 4
Client Project ID : 03-JUL-0338/NI135 6
Lab Sample No :923172076 Project Sample Number : 9249794-003 Date Collecteds 07/21/03 17 :20
Client Sample ID :23024525/PNWX-BR matrix : water Date Received :07/23/03 11 :50
Parameters Results Units Revort Limit _AnalX&Rd-~CAS No, Oust RwLm
GCIMS Seunivolatilo o
Seraivolatile organics Prep/Method ; SPA 827 0
keenaphthans 65 . ug/l 10 . 07/29/03 0609 BET 83-32-9
Acenatiplathylene 21 .ug/l 10 . 07/29/03 08 :39 Brr 208-96-8
Aniline ND ug/l 10 . 07/29/03 0809 NET 62-53-3
Anthracene,KID ug/l 10 . 07/29/03 00 :39 BET 120-12-7
Bauman (a)anthracene ND ug/l 10 . 07/29/03 08 :39 BET 56-55-3
Benso (a) pyrons ND USA 10 . 07/29/03 08 :39 BET SO-32-8
Benzo (b) f luorawthene ND ug/l 10 . 07/29/03 08 :39 RNT 205-99-2
Benwo(g,h'Operylene ND ug/l 10 . 07/29/03 08 :39 Brr 191-24-2
Swan (k) f luormthene ND USA in . 07/29/03 0809 BET 207-08-9
Beruzoic acid ND uy/l 50 . 07/29/03 08 :39 Birr 65-85-0
Benzyl alcohol ND ug/l 20 .07/29/03 00 :39 BET 100-51-6
4-Bromophanylphenyl other ND ug/l 10 . 07/29/03 08 :39 BET 101-55-3
Butylbenzylphthalate ND ug/l 10 . 07/29/03 08,39 BET 85-68-7
4-Chloro-3-mothylphenol BID ug/l 20 .07/29/03 08 :39 SIT 59-50-7
4-Chloromiline ND ug/l 20 .07/29/03 08 :39 BET 106-47-6
bia(2-Chloroothozy)mthane HD ug/l 10 . 07/29/03 O8z39 BET 111-91-1
bis(2-Chloroothyl) other BID ug/l 10 . 07/29/03 0009 BET 111-44-4
bis(2-Chloroisopropyl) other ND ug/l 10 . 07/29/03 08 :39 BET 39638-32-9
2-Chloronaphthalene ND ug/l 10 . 07/29/03 O8z39 BET 91-58-7
2-Chlorophectol KID ug/l 10 . 07/29/03 08 :39 BET 95-57-0
4-Chlorophmylphenyl etber ND ug/l 10 . 07/29/03 08i39 BET 7005-72-3
Chryden ND ug/l 10 . 07/29/03 011109 BET 216-01-9
Dibertz (:,h) anthracene ND ug/l 10 . 07/29/03 08 :39 BET 53-70-3
Dibenzofuran ND ug/l 10 . 07/29/03 08 :39 BET 132-64-9
1,2-Dichlorobenzeas ND ug/l 10 . 07/29/03 08 :39 BET 95-50-1
1,31-Dichlorobenzene ND ug/l 10 . 07/29/03 08 :39 BET 541-73-1
1,4-Dichlorobauxers ND ug/l 10 . 07/29/03 08 :39 BET 106-46-7
3,31-Dichlorobecizidine ND ug/l 20 .07/29/03 08 :39 BET 91-94-1
2 .4-Dichlorophanol ND ug/l 10 . 07/29/03 08 ;39 BET 120-83-2
Diethylphthalate ND ug/l 10, 07/29/03 08 :39 BET 04-66-2
2,41-Dimothylphoool ND ug/l 10 . 07/29/03 08 :39 BET 105-67-9
Dirsethylphthalate ND ug/l 10 . 07/29/03 08 :39 BET 131-11-3
Di-n-bUtylphthalatO ND ug/l 10 . 07/29/03 O8t39 BET 84-74-2
4,6-Dinitro-2-methylphenol HD ug/l 50 . 07/29/03 06 ;39 BET 534-52-1
2,4-Dinitroph"ol ND ug/l 50 . 07/29/03 08 :39 BET 51-28-5
2,4-Dinitrotoluene ND ug/l 10 . 07/29/03 08 :39 BET 121-14-2
2,6-Dinitrotoluens ND ug/l 10 . 07/29/03 08 :39 BET 606-20-2
Data ;08/28/03 page :5 Of 20
1 -b,,,-,r-difical no IIAnfal,ru Unification IDS REPORT OF LABORATORY ANALYSIS KY Drinking Water 9=1NCWastraner 1 2
4C Drunbrig Water 37706 This report shall mt be reproduced, except in full . VA DrMng Water 213
SC 9M without the wetten consent of Pace wlyfical SOrvic". Inc FL NELAP E87627
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aceAnalyfical"'HmWsvflk.AC 28078
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Lab Project Number : 924979 4
Cliwt Project 1Dr 03-JUL-0338INI135 6
Lab Sample No :923172076 Project Sample Number : 9249794-003 Data Collected :07/21/03 17 :20
Cliciat Sample ID ; 23024525/PMIFI-BR matrix : water Date Receivedt 07/23/03 11 ;50
Parmeters Results Units Revort Limit AAalyzed By CAB go,Ougl RecrLm t
Di-n-OCtylphthillate ND ug/l 10 . 07/29/03 06 :39 BET 117-84-0
1,2-Diphazzy1hydrazine ND USA 20 .07/29/03 08 :39 BET 122-66-7
bio(2-gthylhexyl)phthalate ND USA 10 . 07/29/03 08 ;39 BET 117-81-7
Flucrazathese No ug/l 10 . 07/29/03 0809 BZT 206-44-0
Pluorimas ND ug/l lo . 07/29/03 08 ;39 BET 86-73-7
Rexachloro-1,3-butadimis ND ug/l 10 . 07/29/03 08 :39 BET 87-68-3
Hasoachlorobeateasne ND USA 10 . 07129/03 08 ;39 BET 118-74-1
Sexachlorocyclopentadiene HD ug/l 10 . 07/29/03 Mee BET 77-47-4
Reatiachloroeth"a ND ug/l 10 . 07/29/03 08%39 BET 67-72-1
Indeffor (1,2,3-ed)pyr"e ND ug/l 10 . 07/29/03 08 :39 BBT 193-39-5
Isophorome No ug/l 10 . 07/29/03 00 :39 BET 78-59-1
2-Methylitaphthalme 28 .USA 10 . 07/29/03 08 :39 BET 91-57-6
2-Kethylphanool. (o-Cresol)ND ug/l 10 . 07/29/03 0809 BET 95-48-7
3a,11-Methylphanol ND USA 10 . 07/29/03 08 :39 BET
Naphthalme 1100 ug/l 200 07/29/03 0809 BET 91-20-3
2-Mitromiline ND ug/l 50 . 07/29/03 08 ;39 BET 80-74-4
3-Nitroartiline No ug/l 50 . 07/29/03 08 :39 BET 99-09-2
4-Witroaniline ND ug/l 50 . 07/29/03 08 ;39 BIrr 100-01-6
Nitrobeargazte ND USA 10 . 07/29/03 00 :39 BET 98-95-3
2-Nitropherv,l ND USA 10 . 07/29/03 00 :39 BET 88-75-5
4-Nitrophawail ND ug/l 50 . 07/29/03 08 :39 MIT 100-02-7
U-Nitrosodimthylanine ND ug/l 10 . 07/29/03 08 ;39 BET 62-75-9
N-Nitroso-di-n-propylazine ND ug/l 10 . 07/29/03 08 :39 BET 621-64-7
N-Nitrosodiphenylazine No ug/l 10 . 07/29/03 08 :39 BET 06-30-6
Pentachlorophenol ND ug/l 50 . 07/29/03 08 :39 BET 87-86-5
Phimaitanthrene 19 . ug/l 10 . 07/29/03 08 :39 BET 85-01-8
Phenol ND USA 10 . 07/29/03 08 :39 BET 108-95-2
Pyrese No ug/l 10 . 07/29/03 08 ;39 BET 129-00-0
1 .2 .4-Tricb,lorabanazene ND USA 10 . 07/29/03 08 :39 BET 120-82-1
2,4,5-Trichlorophewol HD USA 50 . 07/29/03 08 :39 BET 95-95-4
2,4,6-Trichlomphowl ND USA 10 . 07/29/03 00 :39 BET 88-06-2
Nitrobansene-dS (S) 75 % 07/29/03 00 :39 BET 4165-60 .0
2-Fluorobiphezayl (S) 67 111 07/29/03 08 :39 BET 321-60-8
Torpbmyl .dl4 (S) 00 % 07/29/03 08 :39 BErr 1718-51-0
Phezaol-,15 (S) 3 15 07/29/03 011 :39 BET 4165-62-2 1,2
2-Fluorophaeful (8)4 111 07/29/03 06 :39 BET 367-12-4 1,2
2,4,6-Tribromophenol .(S) 52 07/29/03 08 :39 BET
Date Rxtracted 07/25/03 07/25/0 3
vats~08/20/03 Page~6 of 20
I aboutory Cartnication Ips laboratory Cand mfion I
RC vvam"tu 12 REPORT OF LABORATORY ANALYSIS Ky Drinking Water 90090
NC Driniang Water 37706 This rimort sball no] be reproduced. emuipt in fuh .VA Drinking Water 213
sc 99DO6 vAthout the wfflw consant 01 Pao Analytiot Ser*ft,Inc .FL NELAP E87627
ftas,AWIFUC81 sorric",h7c.
M Kinzy Aym, Suits 100
HufaMvills AC 2W78CIL.F.Analyficaln'Phoov 704 875 9092
mm.pacelabs .com Far 704.875.9091
"C'
Lab Project Number : 9249794
Client Project ID : 03-JUL-0338/KI135 6
Lab Sample No :923172004 Project Sample Number : 9249794-004 Date Collected :07/21/03 13 :00
Client Sample ID :23024526/PMM-BR Matrix : Water Date ReCeiVed :07/23/03 11 :50
Parameters Results Units Reffort Limi --_Aq9Jy-zei CAB NO -Goal R§gL=
GCIKS Sisaivolatiles
Sainivolatiles Organics Prep/Method :EPA 827 0
Aceagasphthens is . ug/l 10 . 07/29/03 09 :17 BET 83-32-9
Acensphthylents 31 . ug/l 10 . 07/29/03 09 ;17 BET 208-96-8
Aniline ED ug/i 10 . 07/29/03 09 :17 BET 62-53-3
Anthracrame ED ug/1 10 . 07/29/03 09 ;17 BET 120-12-7
Benito (a) asithracene NO ug/l 10 . 07/29/03 09 :17 BET 56-SS-3
Benzo (a)pyrane ED ug/l 10 . 07/29/03 09 :17 BET 50-32-0
Beauto (b) f luorawthisse ED ug/l 10 . 07/29/03 09 :17 BET 205-99-2
Beraso(g,h .Uperylaige ED ug/l 10 . 07/29/03 09 ;17 BET 191-24-2
Benzo (k) fluoranthene MD ug/1 10 . 07/29/03 09 :17 BET 207-08-9
Beeszoic acid ED ug/i 50 . 07/29/03 09 :17 BET 65-85-0
Bensyl alcohol ED ug/l 20 .07/29/03 09 :17 BET 100-51-6
4-Brossopbranylphanyl ether ED ug/l 10 . 07/29/03 09 ;17 BET 101-55-3
Butylbenzylphthalate NO ug/I 10 . 07/29/03 09 :17 BET 85-68-7
4-Chloro-3-methylpherfol NO ug/I 20 .07/29/03 09 :17 BET 59-50-7
4-Chloroaniline ND USA 20 .07/29/03 09 :17 BET 106-47-8
bis(2-Chloroethozy),eathfuse ED ug/l 10 . 07/29/03 09 ;17 BET 111-91-1
bis(2-Chlomethyl) other ND ug/l 10 . 07/29/03 09 :17 B13T 111-44-4
bis(2-Chloroisopropyl) other ND ug/l 10 . 07/29/03 09 :17 BET 39638-32 .9
2-Chloronalphthal"s NO ug/l 10 . 07/29/03 09 :17 BET 91-58-7
2-Chlorophmol ND ug/l 10, 07/29/03 09 ;17 BET 95-57-8
4-Chlorophanylphenryl ether ED ug/l 10 . 07/29/03 09 :17 BET 7005-72-3
Chryselike ED ug/l 10 . 07/29/03 09l17 BET 210-01-9
Dibeass(a,h)anthracene ND ug/I 10 . 07/29/03 09 :17 BET 53-70-3
Dibiagurofuran No ug/1 10 . 07/29/03 09 :17 BET 132-64-9
1,2-Dichlorobenzene ED Ug/l 10 . 07/29/03 09 :17 BIT 95-50-1
1,3-Dichlorobaluseas ND ug/l 10 . 07/29/03 09 :17 BET 541-73-1
1,41-Dichlortfbanzene ED ug/l 10 . 07/29/03 09l17 BET 106-46-7
3,38-Dichlorobazilaidinee NO ug/1 20 .07/29/03 09 ;17 BET 91-94-1
2,41-Dichlorophancil No ug/l 10 . 07/29/03 09 :17 BET 120-83-2
Diethylphthalate ED ug/l 10 . 07/29/03 09 :17 BET 84-66-2
2,4-Dimthylphmol RD USA 10 . 07/29/03 09 :17 BET 105-67-9
Dimethylphthalate RD ug/l 10 . 07/29/03 09 :17 BET 131-11-3
Di-n-butylPhthalatO M) ug/1 Ia . 07/29/03 09 :17 BET 84-74-2
4,6-Dinitro-2-metbLylphenol NO uq/1 50 . 07/29/03 09 :17 BET 534-52-1
2,4-Dinitrophen0l ED Ug/l 50 . 07/29/03 09 :17 BET 51-28-5
2,4-Dinitrotoluene ND USA 10 . 07/29/03 09 :17 BET 121-14-2
2,6-Dinitrotoluens ND ug/l 10 . 07/29/03 09 :17 BET 606-20-2
Data$08/28/03 Ia,.:7 f 2D
t AMMON Certdimtiffl 105 REPORT OF LABORATORY ANALYSIS KY Drinking Water QMNCWastewater 1 2
NC Drinking Wate,37706 This reW shall not be reprodumed. Main in full,VA Drinking Water 213
SC 99006 without the wiam onsere of Pace, Analytical SerAC".Im FL NELAP E87627
ftee Anelyffical Sitifirlm,Inc.
98M KsiowAwK Stide 100
Hw&M110.AC 28078acieAnalytical"Phm 704 875 9092
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Lab Project Number : 9249794
Cliedst Project ID :03-JUL-0338/MI135 6
Lab Sample NO : 923172084 Project Sample Number : 9249794-004 Date Collected :07/21/03 13 :00
Cliesit Sample ID : 23024526/PNKH-BR Matrix : Water Date Received :07/23/03 11 :50
Parameters Ressults Units Reliort Limit __Iaa lEyaB CAS No . Oual Regileatt
Di-n-octylphthalate ND ug/l 10 . 07/29/03 09 ;17 BET 117-84-0
1,2-Diphwylbydrazine ND ug/l 20 .07/29/03 09 :17 BET 122-66-7
bia(2-2thylluercyUplathalate KID ug/l 10 . 07/29/03 09 :17 BET 117-81-7
Plucrazitheiviss ND ug/l 10 . 07/29103 09 :17 BET 206-44-0
Pluoresse 19 . ug/l 10 . 07/29/03 09 :17 BET 86-73-7
Hastacb1oro-1,3-butsidiedue SID ug/l 10 . 07/29/03 09%17 BET 87-68-3
Saxachlorobardsworse BID ug/l 10 . 07/29/03 09 :17 BET 118-74-1
Racachlorocyclopeatadifuse RD ug/l 10 . 07/29103 09 ;17 BET 77-47-4
Hestsuchloroethavie ND ug/l 10 . 07/29/03 09j17 BET 67-72-1
Waldo, (1,2,3-cd)pyrme ND ug/l 10 . 07/29/03 09t17 BET 193-39-5
loophorme ND USA 10 . 07/29/03 09 :17 BET 78-59-1
2-Methy1naplathaleag, 140 ug/l 50 . 07/29/03 09 ;17 BET 91-57-6
2-Kethylphmol (cf-Cresol)ND ug/l 10 . 07/29/03 09 :17 BET 95-48-7
U41-Hathylphersol ND ug/l 10 . 07/29/03 09 :17 BET
Naphthalene 170 ug/l 50 . 07/29/03 09 :17 BET 91-20-3
2-Nitromiline ND ug/l 50 . 07/29/03 09 :17 BET 88-74-4
3,Nitromiline BID ug/l 50 . 07/29/03 09 ;17 BET 99-09-2
4-Nitroaailiaa ND ug/l 50 . 07/29/03 09 :17 BET 100-01-6
Mitrobeirozeirse ND ug/l 10 . 07/29/03 09 :17 BET 98-95-3
2-Nitropherool RD ug/l 10 . 07/29/03 09 :17 BET 88-75-5
4-Mitrophadsol ND ug/l 50 . 07/29/03 09 :17 BET 100-02-7
N-Nitrolsodimethyladdine MID Ug/l 10 . 07/29/03 09 :17 BET 62-75-9
N-Nitroso-di-n-propylagoine KID ug/l 10 . 07/29/03 09 :17 BET 621-64-7
M-Nitroacidiphessylamine KID ug/l 10 . 07/29/03 09 :17 BET 06-30-6
Peditachlorophedsol ND ug/l 50 . 07/29/03 09 ;17 BET 87-06-5
Ph"ardthredide 31 . ug/l 10 . 07/29/03 09 :17 BET 85-01-8
Phenol ND ug/l 10 . 07/29/03 09 :17 BET 108-95-2
pyraide ND uq/l 10 . 07/29/03 09 :17 BET 129-00-0
1,2,4-Trichlorobenzesse ND uff/l 10 . 07/29/03 09z17 BET 120-02-1
2,4,5-Trichloropheacol MID ug/l 50 . 07/29/03 09 :17 BET 95-95-4
2,4,6-Trichlorophenol ND ug/l 10 . 07/29/03 09i17 BET 88-06-2
Nitrobesizene-d5 (S) 73 07/29/03 09 :17 BET 4165-60-0
2-Fluorobiplieforyl (S) 69 07/29/03 09 :17 BET 321-60-8
Terphassyl-d14 (S) so Is 07/29/03 09 :17 BET 1718-51-0
Phenol-d5 (S)12 07/29/03 09 :17 BET 4165-62-2
2-Pluoropheddol (S) 13 07/29/03 09 :17 BET 367-12-4
2,4,6-Tribromeopherfol.(S)54 07/29/03 09 :17 BET
Date Extracted 07/25/03 07/25/03
Date :06/28/03 page : 0 Of 20
JD
I abruratory Certification IDS REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090NCWasteenater 1 2
NC Drinking Water 37706 This report shall not be reproduced, e.cep! in full,VA Drinking Water 213
SC 99006 without the within consent or Pace Analytical Seneves,Inc.Fl.NELAP E87627
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PARAMETER FOOTNOTE S
Inorganic Not Chemistry Analyses were performed at our Pace Asheville laboratory and Organic and Metals
testing was performed at our Pace Charlotte laboratory unless otherwise footnoted .
NO Not detected at or above adjusted reporting limit
KC Not Calculabl e
J Estimated concentration above the adjusted method detection limit and balm the adjusted reporting limit
VDL Adjusted Method Detection Limi t
(a)Surrogat e
[1)The surrogate aad/or spike recovery van outside acceptance limits .
[2) The sample could Dot be re-entracted due to limited sample volume .
Data :DO/29/03 Page : 9 of 20
1 eheramn, Cerllficafion IDS REPORT OF LABORATORY ANALYSIS UwalmardulifiG11111102
NO Weariness, 12 KY Drinking Water 9M
NC Drinking Water 37706 This report shall not be reproduced, except in full . VA Drinking Water 213
SC 99006 without the written consent of Pam Anaocal SerViCK . li FL NELAP E87627
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QUALITY CONTROL DATA
Lab Project Number ; 924979 4
client Project ID : 03-JtYL-0338/KI1356
QC Batch :78376 Analysis Method :EPA 827 0
QC Batch Method : Analysis Description : Seevivolatile OrganiCG
Associated Lab Samples :923172050 923172068 923172076 92317208 4
METHOD BLAME :92318051 7
Associated Lab Samples :923172050 923172068 923172076 923172084
Blank Reporting
Parameter units Result limit Footnotes
kcanaybthens ug/l ND 10 .
Acepasphthylene ug/l ND 10 .
Aniline ugi/l ND 10 .
Anthracens ug/l RD 10 .
Benzo(a)anthracene ug/l ND 10 .
Benzo(a~pyreipe ug/l BID 10 .
Bandeto (b)fluorapithens,ug/l ND 10 .
Bezuzo(g']%J~Perylens ug/l ND 10 .
Boxiso M fluoranthene ug/l ND 10 .
Banzoic acid ug/l HD 50 .
Banzyl alcohol ug/l ND 20 .
4-Bromophearylphanyl other ug/l ND 10 .
Butylbanzylphthalate ug/l HD 10 .
4-Chloro-3-methylphesol ug/l ND 20 .
4-Chloroaniline ug/l ND 20 .
bis(2-Chloroothoury)methane ug/l MID 10 .
bis(2-Chloroothyl) other ug/l ND 10 .
bis(2-Chlaroisopropyl) other ug/l ND 10 .
2-Chloronaphthalene ug/l ND 10 .
2-Chlorophepol ug/l ND 10 .
4-Chloropheirylphertyl ether ug/l RD 10 .
Chrysene ug/l ND 10 .
Dibenz(a,h) anthracene ug/l ND 10 .
Dibenzofurlsp ug/l ND 10 .
1,2-Dichlorobeinvene ug/l HD 10 .
1,31-Dichloroberizene ug/l ND 10 .
1,4-Dichlorobenzene ug/l ND 10 .
3 .3--Dichlorobeausidine ug/l ND 20 .
2,4-Dichlorophanol ug/l ND 10 .
Diethylphthalate ug/l RD 10 .
2,4-Dimethylphowl ug/l ND 10 .
Date :00/28/03 Page :10 *f 20
I gpiatow Gertifleaffierh IDS REPORT OF LABORATORY ANALYSIS KY Drinking Water 9MNCWastewater 1 2
NC Drinking Water 37706 This report shall not be reproduced, except 10 full,VA Drinking Water 213
SC 9M without the wman co,,,,t of paw Ajuelyi" Serviars .Im.FL NELAP E87627
'fv* Ine
.
P8=4n'c'v"yAv5v8m S"~~q 100
0^0 Hunbl*118,AV 28078caltavAnalyfical"'Aw M8759092
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QUALITY CONTROL DATA
Lab Project Number ; 924979 4
Client Project ID : 03-JUL-0338/MI1356
VSMD BLANK :92318051 7
Associated Lab Samples ;923172050 923172068 923172076 923172084
Blank Reporting
P"amseter units Result Limit Footnotes
Diamethylphthalate ug/l ND 10 .
Di-n-butylphthalate ug/l ND 10 .
41,6-Dinitro-2-methylphenol ug/l RD 50 .
2,4-Dinitmph=Ol ug/l ND SO .
2,4-Dinitrotoluene ug/l ND 10 .
2,45-Dinitrotolums ug/l RD 10 .
Di-n-octylphthalate ug/l NID 10 .
1,2-Diphany lhydr&zinG ug/l HD 20 .
bis(2-Htbylhexyl)Phthalat6 ug/l MD 10 .
Pluarruathene ug/l NID 10 .
Fluorwe ug/l RD 10 .
Haveachloro-1,21-butadiene ug/l ND 10 .
11...chl orobenzene ug/l IM 10 .
Resalchlorocyclopentadiene ug/l NID 10 .
sexachlorosthasee ug/l ND 10 .
indeato (1,2,3-cd)pyr"o ug/l BID 10 .
isophorons,ug/l ND 10 .
2-KetIryluaphthalanG USA No 10 .
2-Metbylpherol (o-Cresol)ug/l ND 10 .
344-Kethylphemol ug/l ND 10 .
Naplatbalexte USA ND 10 .
2-Nitromiline ug/l ND 50 .
3-Nitroastilize ug/l ND 50 .
4-Nitroaniline ug/l ND 50 .
Nitrobenzene ug/l ND 10 .
2-Nitroph emn I ug/l ND le .
41-Nitrophanol ug/l ND 50 .
N-Nitrosodimthylazine ug/l ND 10 .
N-Nitroso-di-a-propylamine ug/l ND 10 .
N-Nitrosodipheanylamine ug/l ND 10 .
P"tachlorophenol.ug/l ND 50,
Phealwalthrene ug/l ND 10 .
Phenol ug/l ND 10,
Pyrome ug/l ND 10 .
1,2,4-Trichloroberrene ug/l ND 10 .
2,4,5-Trichloroph=ol ug/l ND 50 .
Date :08/28/03 ?.,a : t 20
i,hnnamly Certification ws REPORT OF LABORATORY ANALYSIS KY Drinking Water 9DD90MCwagrinaafter 1 2
NC Drinking Water 37706 This report shall wt be reproduced, anept in full, VA Drinking Water 213
Sc 99006 without the wiften consent of Pau AawOul Servkn, Im FL NELAP E87627
Pace AnRlyftal Selndm, Inc.
M1Gnc&yAvwA Sv* 100
Hw&w11A AfC 28078aceAnalyfical"Phom 704 875 90S2
MM.Pacelabs .corts Far 704.875.9091
QUALITY CONTROL DATA
Lab Project Number : 924979 4
Client Project ID ; 03-JUL-0338/KI1356
MEMD BLANK :9231BOS1 7
Associated Lab Samples ;923172050 92317206B 923172076 923172084
Blank Reporting
R&Egattar'-units Result --kiMLt-Footnotes
2,4,6-Trichlorophanol ug/l No 10 .
Nitrobansene-dS (9) %64
2-Pluortabiphanyl (8) %64
Torphenyl-dili (8)B4
Phmonl-dS (S) 16
2-Fluorophollsol (S)21
2,4,6-Tribrompbmol (S) 77
LABORATORY CONTROL SAMPLE LCSD : 923171169 92317117 7
Spike LCS LCSD LCS LCS D
units Conc, Result Result %Rec Rao RPD Footnotes
kanaphthene ug/l 50 .00 37 .74 37 .20 76 74 1
Acenaphthylene ug/l 50 .00 37 .28 37 .32 75 75 0
Aniline ug/l 50 .00 22 .16 29 .07 44 60 30
Anthracene,ug/l 50 .00 41 .27 40 .10 82 80 3
Benzo (a) awthracane,ug/l 50 .00 41 .87 40 .90 84 82 2
Bentso (a)pyrene ug/l 50 .00 43 .88 42 .79 88 86 3
Bonso (b) f luorassthene USA 50 .00 44 .46 42 .86 89 86 4
Beazo(g,h,i)perYlsDa ug/l 50 .00 43 .01 42 .37 86 85 2
B*oZ0 (k) f luoranthene ug/l 50 .00 41 .41 41 .39 83 83 0
Bensoic acid ug/l 50 .00 15 .28 22 .35 31 45 38 1
B"Zyl alcohol ug/l 50 .00 29 .24 40 .86 58 B2 33 1
41-Bromophanylpheasyl other ug/l 50 .00 39 .11 39 .48 78 77 2
Butylbenzylphthalate ug/l 50 .00 92 .59 109 .4 185 219 17 2,3,2 .3
4-Chloro-3-seethylphesuol ug/l 50 .00 24 .72 42 .34 49 85 53 1
4-Chloroanilina ug/l 50 .00 20 .20 30 .09 40 60 39 1
bia(2-Chloroethoxy)gwgthane ug/l 50 .00 38 .60 37 .08 77 74 4
bio(2-chloroothyl) ether ug/l 50 .00 34 .34 34 .57 69 69 1
bis(2-Chloroisopropyl) ether ug/l 50 .00 37 .22 36 .56 74 73 2
2-Chloronaphthelene ug/l 50 .00 35 .46 35 .09 71 70 1
2-Chloropbenol ug/l 50 .00 21 .33 34 .B3 43 70 48 1
41-Chloroplumylphanyl ether ug/l 50 .00 38 .66 30 .52 77 77 0
Chrysene ug/l 50 .00 41 .19 40 .40 82 81 2
Dibenz (a, h) anthracene ug/l 50 .00 44 .11 44 .37 Be 69 1
Date :00/28/03 Page ; 12 of 20
(Aborignm rArtifiEstlOn IDS REPORT OF UBORATORY AKALYSIS KY Onrulking Water gmNCWasts-ate, 1 2
NG Drinking Water 37706 This report shall not be reproduMd, exupt in full . VA Drinlang Water 213
Sc 99006 Without the wiften consent of Pau linalytical Send0s.10C Fl .NELAP E67627
Pfco AnslyVerl Smitiess Ing
W Kincey Amu,Sutto 100
HWOM114 NC 28078weAnalyfical"'Phom 70487590
wtnvwPaoel8bs .com F.U.'704.875.9091
QUALITY CONTROL DATA
Lab Project November : 924979 4
Client Project IV : 03-JUL-0338/KI1356
LABORA?ORY CONTROL SAMPLE LCSD : 923171169 92317117 7
Spike LCS LCSD LCS TCSD
Partummiter Units Conc, Result Result gec %Rec RPD Footnotes;
Dibenteofuram ug/1 50 .00 37 .64 37 .19 75 74 1
1,2-Dichlorobtanumene Ug/1 50 .00 30 .47 28 .89 61 58 5
1, 3 -Dichlorobenteme Ug/1 50 .00 29 .22 20 .19 513 56 4
1,4-Dichlorobenzens,Ug/1 50 .00 29 .83 28 .19 60 56 6
3,3--Dichlorobenzidine,Ug/1 100 .00 41 .14 41 .62 41 42 1
2,4-Dichloropheriol ug/1 50 .00 24 .76 37 .97 50 76 42 1
Diethylphthalate Ug/1 50 .00 35 .86 35 .09 72 70 2
2,4-Dimethylphell Ug/1 50 .00 24 .20 38 .19 40 76 45 1
Dimethylphthalats Ug/1 50 .00 23 .33 23 .94 47 48 3
Di-n-butylphthalate ug/1 50 .00 41 .09 39 .66 82 79 4
41,6-Dinitro-2-imethylphemol Usr/1 50 .00 41 .65 45 .36 83 91 9
2,41-Dinitrophenol tug/1 50 .00 34 .81 49 .86 70 100 36 1
2,4-Dinitrotoluenut ug/1 50 .00 44 .35 43 .69 89 87 1
2,6-Dinitmtolume Ug/1 50 .00 43 .41 43 .03 87 86 1
Di,n-octylphtllalate uq/1 11*11 47*81 47,46 91 91 1
1,2-Diphany1hydrazine,ug/1 50 .00 35 .15 34 .56 70 69 2
bis(2-11thy1haroyUphthallete Ug/1 50 .00 47 .10 46 .53 94 93 1
Pluorantherm ug/1 50 .00 39 .83 38 .90 so 78 2
Fluorene ug/1 50 .00 39 .63 38 .90 79 78 2
Hazatchloro-1 .3-butaidiene ug/1 50 .00 28 .82 28 .07 58 56 3
Heakatchlorobenteemat Ug/1 50 .00 38 .29 37 .68 77 75 2
K"achlorocyclopwtadiene ug/1 50 .00 23 .39 24 .67 47 49 5
Statialchloroethane Ug/1 50 .00 29 .98 28 .59 60 57 5
Indwo(1,2,3-cd)pyrene ug/1 SO .00 43 .69 43 .77 87 88 0
Isophorone ug/1 50 .00 42 .38 41 .51 85 83 2
2-1116thylasiphthalstle ug/1 50 .00 34 .91 34 .05 70 66 2
2-Methylphencil (o-Cresol)ug/1 50 .00 20 .11 33.42 40 67 50 1
3&4-Methylphenol ugl/1 50 .00 19 .26 32 .72 38 65 52 1
Naphthalene ug/1 SO .00 33 .71 32 .30 67 65 4
2-Hitroautiline ug/1 50 .00 37 .50 37 .96 75 76 1
3-Nitroaniline ug/1 50 .00 31 .60 34 .57 63 69 9
41-Nitromeniline,ug/1 50 .00 28 .96 35 .15 58 70 19
Nitrobenzeme ug/1 50 .00 36 .30 35 .20 73 70 3
2-Nitrophenol ug/1 50 .00 32 .10 39 .97 64 80 22
4-Hitrophenol ug/1 50 .00 13 .70 20 .22 27 40 38 1
N-Nitrooodimethylanine ug/1 50 .00 14 .88 18 .76 30 38 23
N-Nitroso-di-a-propylmine ug/1 50 .00 41 .01 40 .27 82 80 2
Date :06/26/03 ftg .~ 13 of 20
40
NG Wastawn-e" 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 9DO90
NC Drinlang Water 37706 Time roport Vail not be reproduOld.0=131 in full . VA Drinking Wain 213
sc 99OD6 Without UA wiften content of Pool Analirfical Services .Inc Fl-NELAP E87627
Paw AnislWal Servim, Inc.
9800 lancey Amu,Sves 100HunblW11AAC 28078ceAnalWcal'Mom 7048739092
~Pacelabs.oom Far 704.875.9091
ac,
QUALITY CONTROL DATA
Lab Project Number : 924979 4
Client Project ID :03-JUL-0338/MI1356
LABORATORY CONTROL SAMPLE 6, LCSD : 923171169 92317117 7
Spike LCS LCSID LCS LCSID
rAJAMqtqlL-Units Couc,Result Result %Roo %Roo M Footnotes
11-Mitroneodiphearylamine,ug/l 50 .00 38 .29 37.12 77 74 3
Pentachlorophenol ug/l SO .00 39 .07 40 .47 78 81 4
Ph ....threffe,ug/l 50 .00 39 .10 38 .34 76 77 2
phenal ug/l 50 .00 12 .24 16 .90 24 34 32 1
Pyrene ug/l 50 .00 40 .63 39 .69 el 79 2
1,2 .4-Trichlorobenzena,ug/l 50 .00 30 .01 29 .60 62 59 4
2,4,5-Triclaorophwol ug/l 50 .00 31 .04 42 .19 62 84 30
2,4,6-Trichlorophaffol uq/l 50 .00 33 .25 41 .66 66 83 22
Hitrobanstene-d5 (S) 76 75
2-Pluorobiphenyl (8)74 74
Terphenyl-d14 (S)84 63
Phaffol-dS (9)24 34
2-Pluorophenol (8)28 44
2,4,6-Tribromeophenol (S) 89 93
LABORATORY CONTROL SAMPLE :923180525
spike LCs r1cs
E11:911111=-units Conc, Result Rao Footnotes
Acenaphtliene ug/l 50 .00 35 .86 72
Acenaphthylefle,ug/l 50 .00 35 .53 71
Aniline ug/l 50 .00 32 .43 65
Anthracene ug/l 50 .00 39 .89 s o
Return (a) anthracene uq/l 50 .00 39 .12 78
Ronan (a) pyrene ug/l 50 .00 42 .54 85
Benzo (b) f luorstatherle ug/l 50 .00 45 .25 90
RsufZo(g,b,i)Perylene ug/l 50 .00 34 .35 69
Ewan (k) f luorafathene uq/l 50 .00 39 .35 79
somatic acid ug/l 50 .00 10 .31 21
Bentryl alcohol ug/l 50 .00 32 .60 65
4-Bromfophartylpherlyl ether ug/l 50 .00 41 .60 83
Butylbearylphthalate,ug/l 50 .00 74 .08 148 2
4-Chloro-3-mthylphanol ug/l 50 .00 33 .09 66
4-Chloroaniline uq/l 50 .00 34 .44 69
bia(2-ChloroethoacOmethane ug/l 50 .00 33 .67 67
bis(2-Chloroothyl) other ug/l 50 .00 32 .75 6 6
Date ;08/29/03 Page : 14 Of 20
1 aharshortr Cartnic,stlon IDS I -borm-N rarld of an 11)
Nc Wastenter 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 9DO90
NC Drinking Water 37106 This (spon stul mt be mproduced, exceps in full. VA Drolking Water 213
Sc TIM without the written consent of Pace Amlylicill SeNicss,Inc .FL NELAP E87627
Pace Anso),11vell Sorilm,Inc.
98M IllincelyAwnue, Suite 100
Hunbern,ille,NO 28078ceAnalyfical"'Phone [phone]~.Pacelsbs .wm Far 704.875.9091
ac,
QUALITY CONTROL DATA
Lab Project Number : 924979 4
Clieet Project ID :03-JUL-0338/MI1356
LAWRATORY CONTROL SAMPLEt 923180525
Spike LCS MIS
Partiggeeter units Conc, Result % Bag Footnotes
bis(2-Chloroisopropyl) ether Ug/1 50 .00 32 .56 65
2-Chl.orctiaphthaleffe ug/1 50 .00 33 .04 66
2-Chlorophavool ug/1 50 .00 27 .82 56
4-Chlorophaamylpherryl other ug/1 50 .00 40 .14 s o
Chrysme Ug/1 50 .00 40 .62 81
Dibimaz ta,h) authracene ug/1 50 .00 35 .57 71
Diloalaxofuratit,Uq/1 so .00 36 .40 73
1,2-Dichlorobeolesoa,Ug/1 50 .00 31 .11 62
1,11-Dichlorobenzatte Ug/1 50 .00 29 .98 60
1,4-Dich1orobenzwe Ug/1 50 .00 29 .76 60
3,21--Dichlorobnazzidine ug/1 100 .00 50 .02 so
2,4-Dichlorophenol ug/1 50 .00 32 .09 64
Diethylghthalate ug/1 50 .00 37 .34 75
2,4-Dimethylphe][101 Ug/1 50 .00 29 .95 60
Dimethylphthalate Ug/1 50 .00 26 .58 53
Di-n-butylphthalate Ug/1 SO .00 39 .56 79
4,6-Dinitro-2-meethylphenol Ug/1 50 .00 48 .22 96
2,4-Dinitraphearol ug/1 50 .00 38 .05 76
2,4-Dinitrotoluene,Ug/1 50 .00 43 .01 86
2,6-Dinitmtolume Ug/1 50 .00 39 .07 78
Di-n-octylphthalate ug/1 50 .00 41 .74 84
1,2-Dipbanylhydrazine Ug/1 50 .00 27 .84 56
bis(2-Sthylbaxyl)phthalate ug/1 50 .00 41 .15 B2
Pluoratathwar uq/1 50 .00 41 .74 84
Pluorwe Ug/1 50 .00 39 .36 79
Razatchloro-1,3-butadiene,Ug/1 50 .00 31 .21 62
gertachlorobeasemer ug/1 50 .00 40 .34 81
Heatachlorocyclopeotadiene,ug/1 50 .00 22 .33 45
Seetachloroethane ug/1 50 .00 29 .08 58
Indeco(1,2,3-ctipyrene ug/1 50 .00 34 .99 70
Isophorone Ug/1 SO .00 36 .05 72
2-Methylvaphthalerie Ug/1 50 .00 31 .89 64
2-Methylphevol (o-Cresol)ug/1 50 .00 26 .20 52
344-Methylphsool Ug/1 50 .00 23 .90 48
Naplathalsoa,Ug/1 50 .00 33 .16 66
2-Nitroaniline Ug/1 50 .00 34 .39 69
3-Nitroafmiline Ug/1 50 .00 36 .09 7 2
Date :09/28/03 PageI 15 of 2 0
I abongnm Ceddication IIahoramn, Carutcation lps REPORT OF LABORATORY ANALYSIS KY Ddnldng Water 9MNCWaMnIater 1 2
NC Drinking Water 37706 This report shall not be rePrOduCed, OxcePt In futi . VA Drinking Water 213
sc 9M Mthout the witten torment of Pace Ana"at Sermes,Inc.FL NELAP E87627
Proff Anfilillearl Selftleff, hw.
9=KinceyAwav, Sude 100
' 12 HurriftmWils.AfC 28078aOf%oauu Phone [phone]mm.pacelabs .com Far M4.875.9091
QUALITY CONTROL DATA
Lab Project Number : 924979 4
Client Project ID : 03-JUL-0338/MI1356
LABORATORY CONTROL SAMPLE : 923190525
Spike LCs LCS
Parawarater Units Conc .Result Rec Footnotea
4-Nitroaluailine ug/l 50 .00 40 .21 Be
Ritrobazzaturs ug/l 50 .00 34 .92 70
2-Mitropbenol USA 50 .00 32 .67 6s
4-Nitrophenol ug/l 50 .00 20 .07 40
N-Nitrosodivelthylaraine ug/l 50 .00 23 .41 47
N-Nitrooo-di-n-propylanine ug/I 50 .00 35 .26 70
H-Mitrosodiphextylazinas ug/l 50 .00 38 .43 77
Peratachlorophamol ug/l 50 .00 39 .14 78
Phenjunthrene ug/I 50 .00 40 .15 so
Phenol ug/l 50 .00 13 .82 26
Pyrrme ug/l 50 .00 41 .55 63
1,21,4-Trichlorobenzene,USA 50 .00 30 .97 62
2,4,5-Trichlorophanol ug/l 50 .00 38 .47 77
2,4,6-Trichlorophenol ug/l 50 .00 37 .02 74
Hitrobenzame-dS (S) 70
2-Fluorobiphemyl (8) 68
Terphezayl-d14 (S) 87
Phenol-d5 (S) 29
2-Fluorophenol (S)311
2,4,6-Tribromaphenol (S) 89
MATRIX SPIKE &MATRIX SPIKE DUPLICATE :923171185 92317119 3
923152805 Spike ME Men ME Men
zarneffitar-- 221tfi--Penult Conc,Reault Result %-EB.Q %-RQ.C RPD Footnotes
Acenaplathawne ug/l 0 100 .00 73 .40 79 .82 73 so 8
4-Chloro-3-methylpherial ug/l 0 100 .00 70 .76 75 .74 71 76 7
2-Chlorophencl ug/l 0 100 .00 64 .12 63 .35 64 63 1
1,41-Dichlorobenzene ug/l 1 .001 100 .00 60 .36 60 .58 59 60 0
2,41-Dinitrotoluene,ug/l 0 100 .00 66 .10 96 .37 66 96 11
4-Nitrophemol ug/l 0 100 .00 41 .91 42 .25 42 42 1
N-Nitroso-di-n-propylamine USA 0 100 .00 79 .00 83 .19 79 83 5
Pentachlorophenol ug/l 0 100 .00 62 .73 71 .68 63 72 1 3
Phenol ug/l 0 100 .00 29 .85 28 .87 30 29 3
Pyrene ug/l 0 100 .00 79 .09 87 .81 79 88 10
1,2,4-Trichlorobenzene ug/l 0 100 .00 59 .09 61 .22 59 61 4
Date :08/28/03 Page :16 of 20
I ahnMmW Cartillrallon 11) 1 -bonwign, Can f ution I
11CWastanter 12 REPORT OF LABORATORY ANALYSIS KY Drurking Water 90090
NC Drinking Water 37706 This report shall not be rephduced, ex"pt in full, VA Drinluinif Water 213
SC 9M v4MOD, the migan conont of Pm Anahrucal Sermces . Inc . Fl.NELAP E87627
Pace flosovest Setwen,far.9MKInMAMM Suds 100
HwWwWA NC 28078aceAnalyfical'e Phone [phone]
ianvwpooelabs.cono Far 704.875.9091
QUALITY CONTROL DATA
Lab Project Number : 924979 4
Client Project ID : 03-JUL-0338/KI1356
EiRTRIX SPIKE &MATRIX SPIKE DUPLICATE : 923171185 92317119 3
923152805 Spike MS NSD NS XS D
Parimmurtax 2qJtE__Result Conc . Regult Result Rec li-Riff;RED Footnotes
Mitrobourceffe-415 (S)74 79
2-Pluorobipherryl 48) 71 7 6
Terphel (S) 70 73
Ph~l-d5 (8) 32 31
2-Fluctrophenol (S)42 38
2,4,15-Tribromphancil (8) 78 90
SAME DUPLICATE : 923173916
923152839 DUP
Parameter -units Result Result M Footnotes
Acelcumphtheate ug/l No Not NC
Aceicaphthylene ug/1 No ND KC
Amiline ug/l No No NC
Arithraciame ug/l ND ND Hic
Bectizo(a) atathraceire ug/l No No HE
ffecizo(a)pyreccua ug/1 No ND KC
Bectso(b)fluctranthene ug/l No ND NC
Baoao(q,h,i)porylwe ug/l No No NC
BecumoMfluorarithouge,ug/1 No So Ne
Ballistic acid ug/l ND ND NC
Bmzyl alcohol ug/l No No Kc
4-Br~phmylphwyl other ug/l No No NC
Butylb=zylpbthalate ug/l No ND NC
4-Chloro-3-mthylphowl ug/l No ND VC
4-ChloroanilinG ug/l No No NC
bis(2-Chloroothoxy)mth=O ug/l No ND NC
bis(2-chloroothyl) other ug/l No ND NC
bio(2-Chloroisopropyl) other ug/1 No ND KC
2-Chlor"aphthalene ugll No ND SIC
2-Chlorciphonal ug/l No ND NC
4-Chlorophmylphenyl ether ug/l No No NC
Chrysalis ug/l No No NC
Diberaz (a,h)anthracGEM ug/l No ND NC
Dib=zofur=ug/l No ND NC
1,2-Dichlorobanzene ug/1 ND No HC
Page :17 of 20Date:08/20/03
IDs REPORT OF LABORATORY AMALYSIS KY Drmldng Water 9DD90MCwashineater 1 2
NC Drinking Water 37706 This report shall not be reprodumd, except in full, VA Ddrumpt Wale'213
SC 99006 without the written consent Of PRO Amirtioll SeNlOs.Inc F .NELAP E87627
Pave Anslociel SetWevs,Inc.
M KMM Awnue, Svite 100
W610114 AC28078calcueAnalyticaln'Phone [phone]mm.pacelabs.oom Far 704.875.9091
QUALITY CONTROL DATA
Lab Project N=ber : 924979 4
client Project ID :03-itrL-0338/MI1356
SMwLl DtrPLlClTls 923173918
923152839 DUP
Egualtar-utaits Result Result RPD Footnotes
1,3-Dicb,l0r0bGcz6JM6 ug/l ND No KC
1,4-Dichlorcb~eaaa,ug/l RD ND KC
3,3--Dichlorob~idina ug/l No HD IN:
2,4-Dichlor0Phec0l ug/l HD HD BIC
DiethylPhthalStil ug/l HD ND KC
2,4-DillifilthylPhill10101 ug/l ND ND KC
DimulthylPhthalatO ug/l ND No NC
Di-n-butylPhthalate ug/l MD ND NC
4,6-DiV.itrD-2-=thYlPhec0l ug/l In HD HC
2,4-Dinitroph-1 ug/l ND No KC
2,41-DinitrOtOlumb ug/l ND ND KC
2,6-DinitmtOIUMG ug/l ND No NC
Di-n-wtylphthalate ug/l HD ND HC
1,2-Dipbmylbydrazine ug/l RD ND NC
bie,2-gthylhimmyll platleallito ug/l 11D ND NC
Fluormthens ug/l HD No NC
Fluoreme,ug/l HD No HC
Hea~gchlom-1,3-butmidiene ug/l ND ND NC
Hea,i%clalorobeutizece ug/l ND ND NC
Heatechlorocyclopentailierxe ug/l an ED HC
H,exiachloroatkume ug/l ND No KC
lnd=o(1,2,3-cd)pyreme ug/l No HD HC
loophorons ug/l ND ND NC
2-Methylnaphthalwo ug/l HD ND NC
2 .Xethylph=ol (o-Cresol)ug/l HD No KC
364-Methylphfulol ug/l No ND NC
Naplithalleall ug/l ND ND HC
2-Nitroaniline ug/l ND ND NC
3-Nitromiline ug/l HD ND NC
4-Nitroanilinf,ug/l No No KC
Hitrobenzene ug/l HD No NC
2-Hitrophemol ug/l ND ND NC
4-Nitrophmol ug/l HD No NC
N-Kitrosodimthylamina,ug/l ND HD Nc
N-Nitroso-di-in-propylamine ug/l ND HD NC
N-Nitrosodiphenylaiminf,ug/l ND No NC
Pauntachlorophemol ug/l KD ND NC
Date :08/28/0 3
1,herattino Cartifitation IDA REPORT OF LABORATORY ANALYSIS KY DrinWito Water 9DD90NCWdmter 1 2
NC Drioldno Water 37706 This report shall ml be repmduced . e-Pt in hit .VA Donking Water 213
sc 9m withmA the win,,Consent of Pace wivilcal servic",Im.FL NELAP E87627
Pace Analytical Services,Inc.
16=7 Aww,Sufte 100
Hurthilmlis,AIC 28078ceAnalytical"'Phone [phone]M.M.Paoslabs.com Fax.,704.875.9091
ac,
QUALITY CONTROL DATA
Lab Project firmber : 924979 4
Client Project ID ;03-JUL-0336/X11356
SAMPLE ]DUPLICKT11t 923173918
923152839 UU1 ?
Partammiter ullits Result Result m Footnotes
Pheausumthrecus Ug/1 RD No MC
Phenol Ugf/1 ED NID KC
Pyrme ug/1 NO RD KC
1,2,4-Trichloroberausens Ugr/1 ED HD NC
2,4,S-Trichloraph"ol og/1 RD ND SIC
2,4,6-Trichloropheno, 1 Ug/1 So ]KID NC
Nitrobmzme-dS (8) % 62 5 8
2~rlfaorolgighenyl (9) 55 53
Terphentyl-d141 (S) 81 75
Phezi (8) 11 19
2-Fluxtralphenol (8) 13 26
2,4,6-Tribromophmol (0) %40 78
Pogo : 19 of 21)
I 2110010M Cend Cation IDSREPORT OF LABORATORY ANALYSIS KY Drinking Water 9DD90KCWastewater 1 2
NC Drinking Water 37706 Thus report $11all Put be reproduced, except irl full. VA Drinking Water 213
sc 99006 VA#W the wiw cownt Of Pace Armillical Servkn,Inc.FL NELAP E87627
Pace Aamlyflat Savic",Inc.
W Kmelly Awfuel, SuIll 100
HoWmIle,AC 28070aL.UAnalyfical"'Phare.-704.875SW
mvivoacelabs cam FaK.'704.875.091
ac,
Lab Project Number ; 924979 4
Client Project ID :03-JUL-0338/MI1356
QUALITY CONTROL DATA PARAMETER FOOTNOTES
Consistent with EPA guidelines, unrounded concentrations are displayed and have beea used to calculate %Rac and RPD values .
LOW Laboratory Control sample (Duplicate )
XS(D)Matrix Spike (Duplicate)
DUP Sample Duplicat e
MID Not detected at or above adjusted reporting limit
KC Not calculable
J Hatimated concentration above the adjusted method detection . limit and below the adjusted reporting limit
KDL Adjusted Method Detection Limi t
RPD Relative Percent Difference
(S)Surrogate
Ill RPD value was outside control limits, however both percent recoveries were acceptable . Sample results for the
QC batch were accepted based on percent recoveries and completeness of QC data .
[21 Recovery falls outside of QC limits, however, this compound is not found in the associated samples .
[3)Analyte is f ound in the associated blank ag well as in the sample (CLP B-Flag).
Data :06/20/03 page :20 Of 20
I amongry Can dIaheratary Cartillation iDs REPORT OF LABORATORY ANALYSIS KY Drerldng Water 90090NC Wastewater 1 2
NC orinking Water 37106 This feWrf their not be reprodutced, except in full, VA Onniang Water 213
Sc 99006 without the Wittier CORS81111 01 Pace klalytcal Services, IK. FL NELAP E87627
0 0
CHAIN OF CUSTODY RECORD AND ANALYSIS REQUEST FORM
Ana cal Laboratory Services iDuke---- ---F~c--- ------- * -------------------
Mail Code MG03A2 (Building 7405)N-IMS s*'Is 'a 9Page I Of
DISTF1113UTION1w4wEnergy..13339 Hagers Ferry Rd ORIGINAL to LAB ,
For Detailed Instructions, see
: HuntersvIlle,N . C. 28078 COPY to CLIENT
h1tpJ1de~/assenv/coc/ [phone]
-------------Fax :.(704)SLS-A.M~............
1)Project Name 2)Phone No :875-5257
BURLINGrON MGP (OVERBURDEN WELLS)If
E 3)Cli*nt C .Campbell I R . Roberts 4)Fa . No :875 .5032 15Pr eerv .:11= C
2 .
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Z-3 - st 22 Requested Turnaround
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CHAIN OF CUSTODY RECORD AND ANALYSIS REQUEST FORM 7q~
..................................Duke oratory Service sM I 'Page.i~YC'Id := (Building 7405)--L of
DISTRIBUTIONIWOEneY. 13339 Hagers Ferry R d
For Detailed Instructicrnfee! Huntersville,N . 0 . 28078 ORIGINAL to LAB,
51 [phone] COPY to CLIENThUpJlde~/essenvllocl Fax:[phone]............. ..........................
1)Project Name
BURLINGTON MGP (SAPROLITE WELLS)
2)Plh .~. No:875~525 7
E 3)Client C.Campbell /R. Roberts 4)Fax No ;875-50320
V 120VS)BusinessUnit : 20010 6)Process : 7)Resp .To :0193
0B)Nolect to :MGPBURL 9)ActiAly to : ALLACTV 10)Mall Code :MG03A3
Customer to compl le all 0- 0
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---------------- 0
LASUSEONLY 12 4 .0Chem Collection Information E013SaM <0
i "Labil)i Desktop No . pie Description or ID Date Time Signature V z 2 .0~23(3 PMWB-D x 1 1 6
.21 PMWC-O litz,q -7 2-z 0 1-05-X I 1 3 1
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0 01 )Ilk
CHAIN OF CUSTODY RECORD AND ANALYSIS REQUEST FORM- - --- ----------- -- - - --mEhL Duke I ly
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Mail Code MG03A2 (Building 7405)M It 'Page--X-of -A-
DISTRIBUTION13339Hagers Ferry R dPO'Energy.Huntersville,N . C. 28078 ORIGINAL to LAB,
For Detailed Instructions,see :[phone] COPY to CLIENT
h tip Wde~lessenv/cocJ Fax:-------------.(7041 §L5-.~q:L
I)Prol ..t Na ..2)Phone No :875-5257
BURLINGTON MGP (SHAL FRACT BR WELLS)
0 le I El1=01
3)C1i.nt C .Campbell R . Roberts 4)Fax No :875-5032
C2=H 3=H E24=11 w
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custs2mpr to Complete all 16
approli)rlate NON-- - - - - - - - - -d
A
14 C12LABUSEONLY:Chem ollectlon Information E
13 6 0 < <
"Lab 10 1 Sample Description or ID Q. (LueSKTOp NO Date Time Signature t:z M w w
DMW-1 x 1 1 1 3 1 1 1 6
DMW-2 x 1 1 3 1 6
0 6PMWC-BR 7 IA2-1-3 0 e,,LA X 1 1 3 1
3 0!110 X 1 1 3 1PMWH-BR -7 (A2~.5 6
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21)R .1i.0l!h.d By L3 DolanIlme
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14 Days0 0
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A DaysDatc/'Fime :Ve, E
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Date/T' -48 H,Lm e::U,---7
Pace AnIOIC81 $erthfirm, Inc.
9800 Kiray Aym,&tM 100
Huntersvilie,AIC 28078aceAnaljiffticaf-Phone [phone]
wiAvpacelabs.Cohn Fax.[phone]
kugust 26, 200 3
Its . Jay Perkins
Duke Powe r
13339 Hagers Perry Road
XG30A2
Runter,ville,NC 2807 8
RE :Lab Project Number :924896 3
Client Project ID : 03-JUL-0338/KI1356
Do&. lifur .Perkins ;
Enclosed are the analytical results for sautple(s) received by the laboratory on kugust 13, 2003 .Result .
reported herein conform to the met current NELhC standards, where applicable, unleas othervise narrated in the
body of the report .
if you have my questions concerning this report please feel free to contactize .
sincerely ,
I/. A .
r4WA /7
Xxieti Tart
Kristi .Tartillpacelake .c .
Project Naasager
Enclosures
1 horabon, Cerblagan IDS aboffalory Cerld-lball I
NC Wastirmater 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
NC Drinking Water 37706 This tenon shall not be reproduced, except in full, VA Drinking Water 213
SC 99006 without the either, consent of Paco AM~Aiul Services IM. FL NELAP E87627
Pam A
hh"
98M
100!'nolAwn"iHunWialle,NO 280 MceAnalXicaf"Phone [phone]M
vvvAv.pace1abS.conh Faw 704.875.9091
Lab Project Number :924896 3
Client Project ID : 03-JUL-0338/MI135 6
Lab Sample NO :923239040 Project Sample Number :9248963-001 Date Collected :07/25/03 06 :45
Client Sample ID : 23024521/DMW.l Matrix : Water Date Received :08/13/03 12 :05
pa,m,tor, Fesulto Units Report Limit CAB NO .Dual ReqLan
GCIKS Slaunivolatile S
Sebeivolatile Organics Prep/Method ;EPA 827 0
Acenaphthene ND ug/l 10 . 08/20/03 17 :23 BET 83-32-9
AcerubphthYlo,110 ND USA 10 . 08/20/03 17 :23 BET 208-96-0
Aniline ED ug/l 10 . 08/20/03 17 :23 BET 62-53-3
Anthracene ND ug/l 10 . 08/20/03 17 :23 BET 120-12-7
Beessio (a) anthracerne ND ug/l 10 . 08120/03 17 :23 BET 56-SS-3
Bmazo(a)pyrene ND ug/l 10 . 08/20/03 17 :23 BET 50-32-8
Benzo(b)fluoranthene ED ug/l 10 . 08/20/03 17 :23 BET 205-99-2
Bmzo(g,h,i)POrYlms No ug/l 10 . 08/20/03 17 :23 BET 191-24-2
Beetzo(k)fluoranthedges KID ug/l 10 . 08/20/03 17 :23 BET 207-08-9
Benzoic acid ED u9/1 50 . 08/20/03 17 :23 BET 65-85-0
Beci alcohol No ug/l 20 .08/20/03 17 :23 BHT 100-51-6
4-BrosolophoorYlPheeYl other No ug/l 10 . 08120/03 17i23 BET 101-55-3
Butylbrauzylphthalate ED ug/l 10 . 08/20/03 17 :23 BET 85-66-7
4-Chloro-3-methylphmol ND ug/l 20 .08/20/03 17 :23 BET 59-50-7
41-Chlorcesuctilins ND ug/l 20 .08/20/03 17 :23 BET 106-47-8
bis(2-Chloroethoxy)methme ND ug/l 10 . 08/20/03 17 :23 BET 111-91-1
bia(2-Chloroethyl) ether No ug/l 10 . 08/20/03 17 :23 BET 111-44-4
bio(2-Chloroisopropyl) ether ND ug/l 10 . 08/20/03 17 :23 BET 39638-32-9
2-Chlorcmaphthalepak ND ug/l 10 . 08/20/03 17 :23 BET 91-58-7
2-Chlorophen0l KID ug/l 10 . 08/20/03 17 :23 BET 95-57-8
4-ChlorophenylpheasYl ether ND ug/l 10 . DS/20/03 17 :23 BET 7005-72-3
Chryoeade ND ug/l 10 . 08/20/03 17 :23 BET 218-01-9
Diberts (a, h) anthracene No ug/l 10 . 08/20/03 17 :23 BET 53-70-3
Dibenzofuran ND ug/l 10 . 08/20/03 17 :23 BET 132-64-9
1,2-Dichlorobwzene ND ug/l 10 .OB/20/03 17 :23 BET 95-50-1
1,3-Dichlorobenzerabi ND ug/l 10 . 08/20/03 17 :23 BET 541-73-1
1,4-Dichlorobenzene No ug/l 10 . 08/20/03 17 :23 BET 106-46-7
3,3--loichloroberatidine ND ug/l 20 .09/20/03 17 :23 BET 91-94-1
2,4-DicbLlorophwol ND ug/l 10 . 08/20/03 l?z23 BET 120-83-2
Diethylphthalate ND Ug/l 10 . 08/20/03 17 :23 BET 84-66-2
2,4-Dimethylph=Ol ED ug/l 10 . 08/20/03 17 :23 BET 105-67-9
Dimethylplathalate No ug/l 10 . 08/20/03 17 :23 BET 131-11-3
Di-n-butylphthalate KID ug/l 10 . 08/20/03 17 :23 BET 84-74-2
4,6-Dinitro-2-methylph=Ol No ugf/l 50 . 08/20/03 17 :23 BET 534-52-1
2,41-Dirlitrophenol No ug/l 50 . 08/20/03 17 :23 BET 51-28-5
2,4-Dinitrotoluene ND ug/l 10 . 08/20/03 17 :23 BET 121-14-2
2,6-Dinitrotoluene ND ug/l 10 . 08/20/03 17 :23 BET 606-20-2
Date :08/26103 Page : of is
0
aboratort Cernbcalion II lboah.ri,Celldsall)(1.11hi REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090NCWaSteVofteF 1 2
NG Drinking Water 377D6 This report shall not be reproduced, except in foil, VA Drinking Water 213
Sc 99006 without the written consent of Pace Arelytical Services,ric .Fl.NELAP E87627
Pace Analytical Sertirices, Inc.
M Kincity Avertine, Suite 100
Huntaiswile A(028078aceAnaIjilitical"Phone [phone]
M-Ay Pincelabs.coun Far 704.875.9091
Lab Project Number :924896 3
Client Project ID! 03-JUL _0338/NI135 6
Lab Sample No : 923239040 Project Sample Number :9248963-001 Date Collected :07/25/03 06 :45
Client Sample ID :23024521/DMW-1 Katrix : Water Date Received :08/13/03 12 :05
Parameters Results Units Report Limit Analyzed By CAB NO .Gual Raglan
vi-n-octylphthalate ND ug/l 10 . 08/20/03 17 :23 BET 117-84-0
1,2-Diphanylhydrazims ND Ug/l 20 .08/20/03 17 :23 BET 122-66-7
bis(2-Etbylhexyl)pb,thalate ND ug/l 10 . 08/20/03 17 :23 BET 117-81-7
Fluoranthene ND ug/l 10 . 08/20/03 17 :23 BET 20644-0
Fluorinate ND ug/l 10 . 08/20/03 17 :23 BET 86-73-7
sexachloro-1,31-buttediene ND ug/l 10 . 08/20/03 17 :23 BET 87-68-3
Sexachlorobenzens ND ug/l 10 . 08/20/03 17 :23 BET 118-74-1
Himeachlorocyclopentadinne ND ug/l 10 . 08/20/03 17 :23 BET 77-47-4
Rexachloroethane ND ug/l 10 . 08/20/03 17 ;23 BET 67-72-1
Indebact(1,2,31-cid)pyrene ND ug/l 10 . 08/20/03 17 :23 BET 193-39-5
Isophorone ND ug/l 10 . 08/20/03 17 :23 BET 78-59-1
2-Methyloaplathalene ND ug/l 10 . 08/20/03 17 ;23 BET 91-57-6
2-Methylphenol (0-Crell0l)ND ug/l 10 . 08/20/03 17 :23 BET 95-48-7
3&4-Metbylph=ol ND ug/l 10 . 08/20/03 17 :23 BET
Naphthalene ED ug/l 10 . 08120/03 17 :23 BET 91-20-3
2-Nitromiline ND ug/l 50 . 00/20/03 17 ;23 BET OB-74-4
3-Nitroarbiline ND ug/l 50 . 09/20/03 17 :23 BET 99-09-2
4-Nitrowiline ND ug/l 50 . 08/20/03 17 :23 BET 100-01-6
Nitrobenzwe ND ug/l 10 . 08/20/03 17 :23 BET 98-95-3
2-Nitrophenol ND ug/l 10 . 08/20/03 17 :23 BET 88-75-5
4-Nitrophencl ND ug/l So . 08/20/03 17 :23 BET 100-02-7
N-Nitrooodimethylamine ND ug/l 10 . 08/20/03 17 :23 BET 62-75-9
N-Nitroso-di-n-propylanine ND uq/l 10 . 08/20/03 17 :23 BET 621-64-7
N-Nitrosodiphenylamine ND ug/l 10 .OB/20/03 17 :23 BET 86-30-6
Pentachlorophenol ND ug/l 50 . 08/20/03 17 :23 BET 87-86-5
Phenanthrene ND ug/l 10 . 08/20/03 17 :23 BET 85-01-8
Phenol ND ug/l 10 . 08/20/03 17 :23 BET 108-95-2
Pyrexaa ND ug/l 10 . 08/20/03 17 :23 BET 129-00-0
1,2,4-Trichlorobenzene ND ug/l 10 . 08/20/03 17 :23 BET 120-62-1
2,4,5-Trichlorophewl ND ug/l 50 . 08/20/03 17 :23 BET 95-95-4
2,4,6-Trichlorophenol ND ug/l 10, 08/20/03 17 :23 BET 88-06-2
Nitrobenzene-,15 (9) 51 % 08/20/03 17 :23 BET 4165-60-0
2-Fluorobiphenyl (S)52 It 08/2D/03 M23 BET 321-60-8
Terphenyl-,114 (9) 87 % 08/20/03 17 :23 BET 1718-51-0
Phenol-0 (S) 16 % 08/20/03 17 :23 BET 4165-62-2
2-Pluourophenol (S)24 % 08/20/03 17 :23 BET 367-12-4
2,4,6-Tribromophenol (S) 71 % 08/20/03 17 :23 BET
Date Extracted 08/19/03 08/19/03
C crabia ants :Sample received outside of EPA recommended holding time .
Date :06/26/03 Page : 2 Of 15
1 Aortfl,rv Cerblication M 1,horatark Unification I
11CWasterainer W REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
NC Drinking Water 37706 This report shah not be reproduced . exoi in lull, VA Drinking Water 213
&C 99DD6 enhaut the wiffen consent Of Pace Analki Services, Im . FL NELAP E87627
Pace AMIXICS1 SerWees,Inc.
KincayAwne, Suite 100
Hunterswifle;AC 28078aceAnaljiitical"Phone [phone]wi"Vpacelabs.cont Fax 704,875.M
Lab Project Number :924896 3
Client Project ID :03-JUL-0338/MI135 6
Lab Sample No :923239057 Project Sample Number : 9248963-002 Date Collected : 07124/03 16 :50
Client Sample ID : 23024522/DMW-2 Matrix : Water Date Received :08/13/03 12 ;05
Parameters Results Units Report Limi Analyzed By CAS No .Oual RegrIab
GCINS Sesuivolatile s
Sainivolatile Organics Prep/Method :EPA 827 0
Acemaphthene 220 uq/l 100 08/25/03 17 :19 BET 83-32-9
AcmaphtbylM*ND ug/l 10 . 08/25/03 17 :19 BET 208-96-B
Aniline RD ug/l 10 . 08/25/03 17 :19 BET 62-53-3
Anthracerue ND ug/l 10 . 08/25/03 17 :19 BET 120-12-7
Beezo (a) anthracene ND ug/l 10 . 06/25/03 17 :19 BET 56-55-3
Befuzo(a)pyrene ND ug/l 10 . 00/25/03 17 :19 BET SO-32-8
BerixoWfluoranthene No ug/l 10 . 08/25/03 17 :19 BET 205-99 .2
Bmzo(g,h,i)perylene No ug/l 10 . 09/25/03 17 :19 BET 191-24-2
BenzoMfluorafathene No ug/l 10 . 08/25/03 17 :19 BET 207-08-9
Benzoic acid RD ug/l 50 . 08/25/03 17 :19 BET 65-85-0
Beenryl alcohol No ug/l 20 .08/25/03 17 :19 BET 100-51-6
4-Brolociphearylphecryl ether ND ug/l 10 . 08/25/03 17 :19 BET 101-55-3
Butylbenzylphthalate No ug/l 10 . 08/25/03 17 :19 BET 85-68-7
4-Cbloro-3-methylphmol No ug/l 20 .08/25/03 17 :19 BET 59-50-7
41-Chloroafailine ND ug/l 20 .08/25/03 17 :19 BET 106-47-8
bio(2-Chloroothoxy)meth"e No ug/l 10 . 08/25/03 17 :19 BET 111-91 .1
bis(2-Chloroethyl) ether MID ug/l 10 . 08/25/03 17 :19 BET 111-44-4
bia(2-Chloroisopropyl) ether ND ug/l 10 . 08/25/03 17 :19 BET 39638-32-9
2-Chlormaphthalene ND ug/l 10 . 08/25/03 17 :19 BET 91-58-7
2-Chlorcipheriol ND ug/l 10 . 08/25/03 17 :19 BET 95-57-8
4-Chlorophwylphanyl ether RD uq/l 10 . 08/25/03 17il9 BET 7005-72-3
Chrysene ND ug/l 10 . 08/25/03 17 :19 BET 218-01-9
Dibenz (a . h) anthracene ND ug/l 10 . 08/25/03 17 :19 BET 53-70-3
Dibenzofuraz 21 .ug/l 10 . 08/25/03 17 :19 BET 132-64-9
1,2-Dicblorobenzene ND ug/l 10 . 08/25/03 17 :19 BET 95-50-1
1,3-Dichlorobenzera No ug/l 10 . 08/25/03 17 :19 BET 541-73-1
1,4-Dichloroberizene ND ug/l 10 . 08/25/03 17 :19 BET 106-46-7
3 . 3 --Dichlorobenzidine No ug/l 20 .08/25/03 17 :19 BET 91-94-1
2,41-Dichlorophenol No ug/l 10 . 08/25/03 17 :19 BET 120-83-2
Diathylphthalate ND ug/l 10 . 08/25/03 17 :19 BET 84-66-2
2,4-Dimethylpbenol ND ug/l 10 . 08/25/03 17 :19 BET 105-67-9
Dimethylphthalate No ug/l 10 . 08/25/03 17 :19 BET 131-11 .3
Di-n-butylphthalate ND ug/l 10 . 08/25/03 17 :19 BET 84-74-2
4,6-Dinitro-2-methylpbenol No raq/1 50 . 08/25/03 17 :19 BET 534-52-1
2,41-Dinitrophenol No ug/l 50 . 08/25/03 17 :19 BET 51-28-5
2,4-Dinitrotoluene No ug/l 10 . 08/25/03 17 :19 BET 121-14-2
2,6-Dinitrotoluene No ug/l 10 . 08/25/03 17 :19 BET 606-20-2
Date~00/26/03 Page : 3 of 15
1 ahoralon, Cert ficaluan 105 REPORT OF LABORATORY ANALYSIS I ahoMfor, Cert ficalion I
NC Wastwater 12 KY Drinking Water 9M
NC Drinking Water 37706 This report shall not be reproduced . except in lull, VA Ddriking Water 213
Sc 99DO6 without the written consent of Pace AnciVical Serinces .Inc.Ft.NELAP E87627
Pace Awfolowl Semew, Inc.
WKWWAvenue, Suits 100
Hunlerhelft AIC 28078aceAnalXical:'Phone.,M.875.9092
WilAY.pacelabs .con) Fat.704.875.9091
Lab Project Number :924896 3
Client Project ID : 03-JUL_ 0338/KI13S 6
Lab Sample No :923239057 Project Sample Number :9248963-002 Date Collected : 07/24/03 16 :50
Client Sample ID :23024522/DKW-2 Matrix : water Date Received :08/13/03 12 :05
Parametern
-
Results units Reoort LW Anal"ed BY CAS No .0=1 ReoLlet
Di-n-OCtYlPhth&l&te KID ug/l 10 . 08/25/03 17 :19 BET 117-84-0
1,2-Diphmylhydrazine ND ug/l 20 .08/25/03 17 :19 BET 122-66-7
bis(2-Ethylhexyl)phthalate ND ug/l 10 . 08/25/03 17il9 BET 117-81-7
Fluoranthence ND ug/l 10 . 08/25103 17 ;19 BET 206-44-0
Fluoresce,58 . ug/l 10 . 08/25/03 17 :19 BET 86-73-7
Hexachloro-1,21-butadiene ND ug/l 10 . 08/25/03 17 :19 BET 87-68-3
Rexachlorobenzene No ug/l 10 . 08/25/03 17 :19 BET 118-74-1
R,,,chlorocyclopentadiene No ug/l 10 . 08/25/03 17 :19 BET 77-47-4
Hexachlorciethasse ND ug/l 10 . 08/25/03 17 :19 BET 67-72-1
Jndaoux(l,2,3-cd)pyrene ND ug/l 10 . 08/25/03 17 :19 BET 193-39-5
Isophorcrue BID ug/l 10 . 08/25/03 17 :19 BET 78-59-1
2-Hathylinaiplathaletas 230 ug/l 100 08/25/03 17 :19 BET 91-57-6
2-Methylphimpol (0-Cres0l)No ug/l 10 . 08/25/03 17 :19 BET 95-48-7
3&4-Mathylphmol ND ug/l 10 . 08/25/03 17 :19 BET
Naphthalene 900 ug/l 100 08/25/03 17 :19 BET 91-20-3
2-Nitromiline ND ug/l 50 . 08/25103 17 :19 BET 88-74-4
3-Nitromiline No ug/l 50 . 08/25/03 17 :19 BET 99-09-2
41-Nitroaniliffe,His ug/l 50 . 08/25/03 17 :19 BET 100-01-6
Nitroberazeacte ND ug/l 10 . 08/25/03 17 :19 BUT 98-95-3
2-Kitrophenol No ug/l 10 . 08/25/03 17 :19 BET 88-75-5
4-Nitrophenol ND ug/l 50 . 08/25/03 17 :19 BET 100-02-7
N-Nitrosodimethylamine ND ug/l 10 . 08/25/03 17 :19 BET 62-75-9
N-Nitroso-di-n-propylmine ND ug/l 10 . 08/25/03 17 :19 BET 621-64-7
N-Nitrosocliplansaylassaine ND ug/l 10 . 08/25/03 17 :19 BET 86-30-6
Pentachlorophenol No ug/l 50 . 08/25/03 17 :19 BET 87-86-5
Phicaparithrene 46 .ug/l 10 . 08/25/03 17 :19 BET 85-01-8
Phenol ND ug/l 10 . 08/25/03 17 :19 BET 108-95-2
Pyramus,ND ug/l 10 . 08/25/03 17 :19 BET 129-00-0
1,2,4-Trichlorobenzene ND ug/l 10 . 08/25/03 17 :19 BET 120-82-1
2,4,5 .Trichlorophenol ND ug/l 50 . 08/2S/03 17 :19 BET 95-95-4
2,4,6-Tricblorophenol ND ug/l 10 . 08/2S/03 17 ;19 BET 88-06-2
Nitrobecrucene-dS (S) 71 % 08/25/03 17 :19 BET 4165-60-0
2-Fluctrobipharayl (S)64 le 08/25/03 17 :19 BET 321-60-8
Terphenyl-dl4 (S) 67 % 08/25/03 17~19 BET 1718-51-0
Ph=ol-d5 (S)14 % 08/25/03 17 :19 BET 4165-62-2
2-Pluorophenol (S) 19 % 08/25/03 17 :19 BET 367-12-4
2,4,6-Tribromophenol (S) 33 % 08/25/03 17 :19 BET
Date Extracted 08/19/03 08/19/03
comments :Sample received outside of EPA recommended holding time .
Date~08/26/D3 Page ; 4 of 15
I aboralory Urtificallm I REPORT OF LABORATORY ANALYSIS I abonlon, Carfification I
NC WaShMalef 12 KY Drinking Water 9DO90
NC Drinking Water 37706 This report shall not be reproduced, except in full . VA Drinking Water 213
Sc 99DO6 arthourt the written consent of Pace Amytical Services,Inc.Fl.NELAP E87627
Pace Awlyflesi Sortl1cm, Inc.
M &M Amenue, $Wta 100
Hunlasiolle,AC 28078aceAnalXicalPhone 704 875 9092
w"AV.Pacelab&com Far 704.875.9091
Lab Project Humber :924896 3
Client Project ID :03-JUL_ 0338/MI135 6
Lab Sample NO : 923239065 Project Sample Number : 924B963-003 Date Collected : 07/24/03 10 ;45
Client Sample ID :23024527/PMWL-BR Matrix : Water Date Received : OB/13/03 12 :05
ka Results Unite Report Limit Analyzed By CAB No .Qual Reglizz
GC/KS Seglivolatile S
Senivolatile Organics Prep/Metbod ; EPA 827 0
Acenaphthente,ND ug/1 10 . 08/20/03 19 :48 BET 83-32-9
Acenaphthylene No ug/1 10 . 08/20/03 19 ;48 BET 208-96-8
Aniline No ug/1 10 . 08/20/03 19 :48 BET 62-53-3
Anthracene ND USA 10 . 08/20/03 19 :48 BET 120-12-7
Benzo (a) anthracene ND ug/l 10 . 08/20/03 19 :46 BET 56-55-3
Below (a)pyrene ND ug/l 10 . 08/20/03 19 :48 BET 50-32-8
Benzo (b) f luouranthene No ug/l 10 . 08/20/03 19 :48 BET 205-99-2
Bmzo(g,h,i)ParYl"e No ug/1 10 . 08/20/03 19 :48 BET 191-24-2
Benzo (k) f luoranthene ED ug/1 10 . 08/20/03 19 :48 BET 207-08-9
Benzoic acid ND USA 50 . 08/20/03 19 :40 BET 65-65-0
Bmzyl alcohol KID ug/1 20 .08/20/03 19 :48 BET 100-51-6
41-Bromophacylphentyl ether ND ug/1 10 . 08/20/03 19 :48 BET 101-55-3
Butylbenrylphthalate KID ug/1 10 . 08/20/03 19 :48 BET 85-68-7
4-Chloro-3-methylphenol ND ug/1 20 .08/20/03 19 :48 BET 59-50-7
4-Chloroautiline ND ug/1 20 .08/20/03 19 :48 BET 106-47-8
bis(2-Chloroetboxy)methane ND ug/1 10 . 08/20/03 19 :48 BET 111-91-1
bis(2-Chloroethyl) ether No ug/1 10 . 08/20/03 19 :48 BET 111-44-4
bis(2-Chloroisoprolyyl) other ND ug/1 10 . 08/20/03 19 :48 BET 39630-32-9
2-Chloronaphthalene ND ug/1 10 . 08/20/03 19 :48 BET 91-58-7
2-Chlorophwol ND ug/1 10 . 08/20/03 19 :48 BET 95-57-8
4-Chlorophanylphanyl other ND ug/l 10 . 00/20/03 19 :48 BET 7005-72-3
Chrysene No ug/l 10 . 08/20/03 19 :48 BET 218-01-9
Dibenz (a, h) anthracene ND ug/1 10 . 08/20/03 19 :48 BET 53-70-3
Dibeamofuran ND ug/1 10 . 08/20/03 19 :48 BET 132-64-9
1,2-Dicblorobenzeze ND ug/1 10 . 08/20/03 19:48 BET 95-50-1
1,21-Dichlorobenzwe ND ug/1 10 . 08/20/03 19 :48 BET 541-73-1
1,4-Dichlorobenzene ND ug/1 10 . 08/20/03 19 :48 BET 106-46-7
3,3--Dichlorobanzidine ND uq/1 20 .08/20/03 19 :48 BET 91-94-1
2,4-Dichlorophenol ND USA 10 . 08/20/03 19:48 BET 120-83-2
Diethylphthalate ND ug/l 10 . 08/20/03 19 :48 BET 84-66-2
2,4-Dimethylphenol No ug/1 10 . 08/20/03 19:48 BET 105-67-9
Dimethylphthalate ND ug/l 10 . 08/20/03 19;48 BET 131-11-3
Di-n-butylphthalate No ug/1 10 . 08/20/03 19 :48 BET 84-74-2
4,6-Dinitro-2-methylpbenol No ug/1 50 . 08/20/03 19 :48 BET 534-52-1
2,4-Dinitrophwol NJ)ug/1 50 . 08/20/03 19 :48 BET 51-28-5
2,4-Dinitrotoluene ND ug/1 10 . 08/20/03 19 :48 BET 121-14-2
2,6-Dinitrotoluene ND ug/l 10 . 08/20/03 19 :48 BET 606-20-2
Date!08/26/03 page ; 5 f 15
1,1b,nuart, Cell,futetro I albagunrt, Certifitation J Q
4C Wastmter 12 00 REPORT OF LABORATORY ANALYSIS KY Dratung Water 9OD90
NG Drinking Water 37706 This report sftall not be reproduced . excePt in lull . VA Drinking Water 213
sc 99DD6 wrthout the written content ol Pam Malytical Sences,Inc.FL NELAP E87627
Pace Analkficst Serlifen, five.
M Kincey Averal Suite 100
Huruminfle,NC 28078aceAnalXicaf-Phone-704.875.9092
M-Airpacelabs-com Fat 704 .675.9091
Lab Project Number :924896 3
Client Project ID :03-JUL _ 0338/M1135 6
Lab Sample NO : 923239065 Project Sample Number :9248963-003 Date Collected ; 07/24/03 10 :45
Client Sample ID :23024527/PNKL-BR Matrix : Water Date Received :08/13/03 12 :05
Parameters Results Units Report Limit Analyged By CAB No .Dual ReqLmt
Di-n-octylphtbalate No ug/l 10 . 08/20/03 19 :48 BET 117-84-0
1,2-Diphanyllaydrazine ND ug/l 20 .08/20/03 19 :48 BET 122-66-7
bis(2-Etbylhexyl)phtbalate 96 . ug/l 10 . 08/20/03 19 :48 BET 117-81-7
Pluoramtheme No ug/l 10 . 08/20/03 19 :48 BET 206-44-0
Pluorene ND ug/l 10 . 08/20/03 19 :48 BET 86-73-7
Hexachloro-1,31-butadleme ND ug/l 10 . 08/20/03 19 :48 BET 87-68-3
Smachlorobenzene No ug/l 10 . 08/20/03 19 :48 BET 118-74-1
Nateachlorocyclopentadiame No ug/l 10 . 00/20/03 19 :46 EST 77-47-4
Sexachloroethame No ug/l 10 . 08/20/03 19i4B BET 67-72-1
Jndeawo(l,2,3-cd)pyreoe KID ug/l 10 . 08/20/03 19:48 BET 193-39-5
Isopborous ND ug/l 10 . 08/20/03 19:48 BET 78-59-1
2-Methylaulphtlialene No ug/l 10 . 08/20/03 19:48 BET 91-57-6
2-Methylphemol (0-Cres0l)No ug/l 10 . 00/20/03 19 :48 BET 95-48-7
3&4-Metbylphemol ND uq/l 10 . 08120/03 19 :48 BET
Haphthaleme 13 . DO 10 . 08/20/03 19 :48 BET 91-20-3
2-Nitromiline ND ug/l 50 . 08/20/03 19 :48 BET 88-74-4
3-Nitroaniline No ug/l 50 . 08/20/03 19 :48 BET 99-09-2
4-Nitroamiliae No Ug/l 50 . 08/20/03 19 :48 BET 100-01-6
Nitrobenzene No ug/l 10 . 08/20/03 19 :48 BET 98-95-3
2-Nitrophenol ND USA 10 . 08/20/03 19 :48 BET 88-75-5
4-Nitrophenol No ug/l 50 . 08/20/03 19 :48 BET 100-02-7
N-Nitrosodimethylamine No ug/l 10 . 08/20/03 19 :48 BET 62-75-9
N-Nitroso-di-n-propylamine No ugri'l 10 . 08/20/03 19 :48 BET 621-64-7
N-Nitrosodiphemylamine No ug/l 10 . 00/20/03 19 :48 BET 86-30-6
Pentachlorophecol No ug/l 50 . 08/20/03 19 :411 BET 87-86-5
Phanianthrene No ug/l 10 . 08/20/03 19:48 BUT 85-01-6
Phenol No ug/l 10 . 08/20/03 19:48 BET 108-95-2
Pyrene No ug/l 10 . 08/20/03 19:48 BET 129-00-0
1,2,4-Trichlorobeftzene No ug/l 10 . 00/20/03 19 :48 EST 120-02-1
2,4,5-Trichlorophenol ND DO 50 . 08/20/03 19 :48 BET 95-95-4
2,4,6-Trichlorophmol No ug/l 10 . 08/20/03 19:48 BET 88-06-2
Nitrobecizell (S) 72 % 08/20103 19 :48 BET 4165-60-0
2-Fluorobiphenyl (S) 107 % 08/20/03 19 :48 BHT 321-60-8
Terphemyl-d14 (S) 178 % 08/20/03 19 :48 BET 1718-51-0 1
Phwol-d5 (S)14 % 08/20/03 19 :48 BET 4165-62-2
2-Fluorophenol (S) 26 % 08/20/03 19 :48 BET 367-12-4
2,4,6-Tribroneophernol (S) 85 % 08/20/03 19 :48 BET
Date Extracted 08/19/03 08/19/03
Comments :Sample received outside of EPA reccbmaeuded holdinii time .
Date :06/26/03 page ; 6 Of is
t abomeow Cartifical u1195 reffilicalexi I
NC WaStexal 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090
NC Drinking Water 37706 This reporl shall not be reproduceD . except in full, VA Drinking Water 213
Sc 99DD6 without the written consent of Pace Ana"! Strobes,I%.FL NELAP E87627
Pace Analyflest Senleff,Inc.MKinoWAvenue, Suite 100
Hunhusilifle,NC 28078aceAnal3iiitical-Phone:[phone]
wwpaCelabS .COM Fax.[phone]
Lab Project Number ;924896 3
Client Project ID : 03-JUL_ 0338/1411356
PARAMETER FOOTNOTE S
inorganic Net Chemistry Analyses were performed at our Pace Asheville laboratory and Organic and Metals
testing was performed at our Pace Charlotte laboratory unless otherwrise footnoted .
ME,Not detected at or above adjusted reporting limit
NC Not Calculabl e
J Estimated concentration above the adjusted method detection limit and balm the adjusted reporting limit
MDL Adjusted Method Detection Limi t
(S)Surrogat e
Ill Bass/neutral surrogate recovery outside of control limits . The data "a accepted based on valid recovery of
remaining tiec, base/neutral surrogates .
Date :08/26/03 Page :7 of 15
on ID I rerlificidio nCenfleal,REPORT OF LABORATORY ANALYSIS KY Drinking Water 9wNCWastineater12
NC Drinking Water 37706 This repom chair not be reproduced, e.cept in lull . VA Drinking Water 213
SC 99006 without the imen consent of Pace Analyficaul Semites, Inc. I'L NELAP E87627
Pace Analyfical Serfrices,Inc.
MKinMAY&W Suits 100
HoWswile,AV 26078aceAnalXical:-Phone [phone]
wmv.pace1abs .corn Fa.704.675,9091
QUALITY CONTROL DATA
Lab Project Number :924896 3
Client Project 111): 03-JUL_ 0338/11111356
QC Batch :79954 Analysis Method :EPA 827 0
QC Batch Method : Analysis Description :Sencivolatile organics
Associated Lab Samples : 923239040 923239057 92323906 5
MMOD BLANK :92325969 1
Associated Lab Samples : 923239040 923239057 923239065
Blank Reporting
Parameter units Result Limit Footnotes
Aceasphthene ug/l ND 10,
Acenaphthylene ug/l No 10 .
Aniline ug/l ND 10 .
Anthracene ug/l ND 10 .
Santo (a) anthracene ug/l ND 10 .
Basso (a) pyreas ug/l No 10 .
Becczo (b)fluorecathene ug/l NID 10 .
Bmzo(g,l,,i)perylene -9/1 No I"
Basso (k)fluoranthene ug/l NID 10 .
Benzoic acid ug/l ND 50 .
BMZYI alcohol ug/l No 20 .
4-Broacphabsylphenyl ether ug/l No 10 .
Butylbenzylphtbalate ug/l MID 10 .
4-Chloro-3-methylphenol ug/l ND 20 .
41-Chloroaziline ug/l No 20 .
bis(2-Chloroetboxy)metheltle ug/l No 10 .
bis(2-Chloroethyl) other ug/l ND 10 .
bis(2-Chloroisopropyl) ether ug/l ND 10 .
2-Chloronaphthalene ug/l ND 10 .
2-Chlorophenol ug/l No 10 .
4 .Cbloropbenylphenyl ether ug/l ND 10 .
Chrysene ug/l No 10 .
Dibgar(a,h) anthracene uq/l NID 10 .
Dibenzofuraxf ug/l No 10,
1,2-Dichlorobenzene ug/l NID 10 .
1,3-Dichlorobenzene ug/l ND 10 .
1,4-Dichlorobenzene ug/l ND 10 .
3,31-Dichlorobenzidine ug/l KID 20 .
2,4-Dichlorophanol ug/l MID 10 .
Diethylphthalate ug/l NID 10 .
2,4-Dimethylphenol ug/l ND 10 .
Data ;08/26/03 Page :a of 15
40
1 nagmung Cerlithutcut IDsI ablualoN Certif"110111D5 REPORT OF LABORATORY ANALYSIS KY Drinking Water SOD90NCWalifirwiter 1 2
NC Drinkint) Water 37706 This report shall not be rePfldKed, exceptl ut full, VA Drinking Water 213
SC 99DO6 wilhout the written consent Of Pace AmYtical SeNices . Im fl- NELAP E87627
ftee A"101cal Serwen,Inc.
9M KinM Atimue, Suite 100
HunWwfle,AV 28078aceAnaljliticalPhom7048759092
m-Ay.pacelabus.wrn Far 704.875.9091
QUALITY CONTROL DATA
Lab Project Number :9248963
Client Project ID : 03-JUL-0338/MI1356
MEMD BLANK : 92325969 1
Associated Lab Samples : 923239040 923239057 923239065
Blank Reporting
ParametlK -Units Result Limit Footnotes
Dimethylpbthalate ug/l ND 10 .
Di-n-butylphthalate ug/l ND 10 .
4,6-Dinitro-2-mthylphenol ug/1 ND 50 .
2,4-Dinitrophenol.uq/l ND 50 .
2,4-Di.nitrotolume ug/l ND 10 .
2,6-Dinitrotolume ug/l ND 10 .
Di-n-mtylphthalate uq/l BID 11).
1,2-Diphany1hydrazine ug/l ND 20 .
bia(2-ztbylhexyl)phthalate USA ND 10 .
Plunrianthene ug/l ND 10 .
Fluorews ug/l ND 10 .
Rapsactiloro-1,21-butadierue ug/l BID 10 .
Beapschlorobee2e.. ug/l ND 11,
Reficachlorocyclopentactiene ug/l ND 10 .
Hermactilorcethans,ug/l ND 10 .
Indwo(1,2,3-cd)pyr=e ug/l ND 10 .
loophorone ug/l ND 10 .
2-Methy1naptithalene ug/l ND 10 .
2-Hathylphenol (o-Cresol)ug/l ND 10 .
3&4-Methylphenol ug/l ND 10 .
Naphthalene ug/l ND 10 .
2-Nitroaniline ug/l . ND 50 .
3-Nitroaxpiline ug/l ND 50 .
4-Nitrowiline ug/l ND 50 .
Nitrobenzwe ug/l ND 10 .
2-Nitropherpol ug/l ND 10 .
4-Nitrophmol ug/l ND 50 .
N-Hitrosodimethylamine ug/l BID 10 .
N-Nitroso-di-n-propylmine ug/l ND 10 .
N-Nitroacidiphenylastive ug/l ND 10 .
Pwtacblorophenol ug/l ND 50 .
Phenanthrene ug/l ND 10 .
Phenol ug/l MD 10 .
Pyribne ug/l ND 10 .
1,2,4-Trichlorobenzene ug/l ND 10 .
2,4,5-Trichlorophenol ug/l ND 50 .
Date :00/26/03 Page :9 of 15
0
l,hgMtpN Certifitabon JDI~hpratorv Ceftifuligo IN REPORT OF LABORATORY ANALYSIS KY Drinking Water 9DD90NCWastwater 1 2
NC Drinking Water 37706 This report shall not be produced, except in lull. VA Drinking Water 213
Sc 99006 without the written consent ol Pam Analytical SerAces . Inc. FL NELAP E87627
pace Maiyucal Serwiffs,life.
M Kinoey Avebefe, Suite 100
HunterSinfile,AIC 28078aceAnaljiftical"Phone.,704.8759M
WiMparoelabs.p0n)Fac 704.875.9091
QUALITY CONTROL DATA
Lab Project Number ;924896 3
Client Project ID : 03-JUL_ 0338/H11356
HMoD BLANK ;92325969 1
Associated Lab Samples : 923239040 923239057 923239065
Blank Reporting
Unity Result Limit Footnote s
2,4,6-Trichlorophmol ug/l No 10 .
Nitrobensenti (S) % 53
2-Fluorobiphenyl (S) % 5 3
Teriphezi (S) 79
Phenol-0 (S)24
2-Fluorophwol (S)34
2,41,45-Tribromophernol (S) %64
LABORATORY CONTROL SAMPLE LCSD ; 923259709 923259717
Spike LCS LCS]D LCS LCSD
p4r..t .r Units Conc, Result Result %Rac 1,Rec RPID Footnotes
Aconaplitherte ug/l 50 .00 28 .65 32 .81 57 66 14
Acenaphthyleftes ug/l 50 .00 28 .33 32 .90 57 66 1 5
Aniline ug/l 50 .00 46 .60 65 .42 93 131 34 1,2
Anthracene ug/l 50 .00 30 .60 35 .09 61 70 14
Benzo(a) anthraceme ug/l 50 .00 31 .54 34 .98 63 70 10
Bonso(a)pyrene ug/l 50 .00 34 .90 39 .40 70 79 12
Benzo(b)fluoranthene ug/l 50 .00 33 .45 34 .93 67 70 4
Benzo(g,h,i)perylei ug/l 50 .00 37 .64 41 .79 75 84 10
Benzo(k)fluoramthene ug/l 50 .00 40 .56 53 .07 81 106 27
Benzoic acid ug/l 50 .00 8 .259 10 .30 16 21 22
BanZyl alcohol ug/l 50 .00 24 .40 31 .61 49 63 26
4-Bromeophertylploetcyl other ug/l 50 .00 26 .59 32 .89 57 66 14
Butylbenzylphthalate ug/l 50 .00 24 .54 30 .85 49 62 23
4-Chloro-3-mthylphenol USA 50 .00 24 .97 32 .72 50 65 27
4-Chloroafailine ug/l 50 .00 29 .26 36 .23 58 72 21
bis(2-Chloroethotcy)methazie ug/l 50 .00 23 .63 26 .81 47 54 13
bia(2-Chloroethyl) ether ug/l 50 .00 21 .53 24 .83 43 50 14
bis(2-Chloroisopropyl) ether ug/l 50 .00 22 .06 25 .51 44 51 14
2-Chloronaphthalme ug/l 50 .00 29 .46 34 .63 59 69 16
2-Chloropherol ug/l 50 .00 19 .58 26.75 39 54 31 3
4-Chlorophenylphanyl ether ug/l 50 .00 28 .18 32 .41 56 65 14
Chrysene ug/l 50 .00 32 .13 35 .38 64 71 10
Dibenz(a,h) authracene ug/l 50 .00 31 .43 35 .65 63 71 1 3
Date :09/26/03 Page :10 of 15
is
L AhnGIDN Certiftation JDsIaboratcay Certificalton-11i REPORT Of LABORATORY ANALYSIS Ky Drinking Water 9OD90NCWasterean, 1 2
K Drinking Water 37706 This retain stall not be (wroducei except in full . VA Drinking Water 213
Sc 99DD6 Without the whin consent of Pace AmMiul Services, Inc. FL NELAP E87627
Pace ma"Cal Servic",Inc.
M KinMAwnue, Suite 100
HoWsPilk,NO 28078aceAnalXical!'Am-704.875.9092
Far 704 .875.9091
QUALITY CONTROL DATA
Lab Project Number :924896 3
Clieut Project ID : 03-JUL_0338/1411356
LA,BORATORY CONTROL SAMPLE & LCSD : 923259709 92325971 7
Spike LCS LCSJD LCS LCSD
Units Conc,Result Result Rec %Rec, RPD Footnotes
Dibertz0furac ug/1 50 .00 32 .78 37.10 66 74 12
1,2-Dichlorolgenzene ug/1 50 .00 26 .15 29 .96 52 60 14
1,21-Dichloroberazene ug/1 50 .00 24 .76 28 .91 so 58 15
1,4-Dichloroberiazette ug/1 50 .00 24 .58 28 .74 49 58 16
3,3--Dictilorobiazasidine ug/1 100 .00 18 .59 19 .58 19 20 5 4
2,4-Dichlorophmol ug/1 50 .00 24 .74 30 .09 50 60 19
Diethylphthalate ug/1 50 .00 18 .70 22 .20 37 44 17
2,4-Dimest1pylpheatol Ug/1 50 .00 21 .82 25 .89 44 52 17
Distathylphthalate ug/1 50 .00 6 .526 7 .756 13 16 17
Di-n-butylphthalate uq/1 50 .00 23 .77 27 .28 46 55 14
4,6-Dinitro-2-methylpherool ug/1 50 .00 32 .44 35 .92 65 72 10
2,4-Dinitrophmol uq/1 50 .00 28 .22 31 .82 56 64 12
2,4-Dinitrotoluene ug/1 50 .00 34 .66 39 .56 69 79 13
2,6-DinitrotolU-a g/1 11,10 34,10 39*10 61 11 1 10
Di-n-octylphthalate ug/1 50 .00 27 .65 31 .27 55 62 12
1,2-Dipherry1hydrazine ug/1 50 .00 27 .62 31 .06 55 62 12
bi8(2-Ethy1bexy1)phth&1ate ug/1 50 .00 30 .89 34 .76 62 70 12
Pluorantheme ug/1 50 .00 28 .48 32 .34 57 65 13
Fluorerne ug/1 50 .00 30 .51 34 .93 61 70 14
Hestachloro-1,21-butradiene ug/1 50 .00 26 .05 29 .00 52 58 11
Heouschlorobenzene ug/1 50 .00 35 .05 39 .73 70 80 13
Reauschlorocyclopentadiene ug/i 50 .00 14 .44 19 .69 29 40 32 3
Hialcachloroethappe ug/1 50 .00 24 .18 28 .31 48 57 16
Indeno(1,2.3-cftyreate ug/1 50 .00 33 .54 38 .16 67 76 13
Iaophorone ug/1 50 .00 32 .83 36 .53 66 73 11
2-Methyllpaphthaletae,ug/1 50 .00 28 .79 31.92 so 64 10
2-Methylphetwol (o-Cresol)ug/1 50 .00 17 .84 24 .04 36 48 30
3&4-Methylphmol ug/1 50 .00 15 .57 22 .73 31 46 37 3
blacphtbalepus ug/1 50 .00 25 .31 27 .99 51 56 10
2-Nitromiline ug/1 50 .00 28 .36 32 .65 57 65 14
3-Nitromiline ug/1 50 .00 28 .32 35 .49 57 71 22
4-Nitroacailine ug/1 50 .00 23 .69 30 .19 47 60 24
Nitrabenzene ug/1 50 .00 29 .55 32 .46 59 65 9
2-Nitropheavol ug,11 50 .00 26 .29 28 .92 53 58 10
4-Nitrophenol ug/1 50 .00 10 .56 15 .40 21 31 37 3
N-Nitrooodimethylamine ug/1 50 .00 13 .52 16.85 27 34 22
N-Nitroso-di-n-propylmine ug/1 50 .00 22 .77 26 .52 46 53 1 5
Date ;011/26/03 Page :11 of 15
I aboralorv Certification 10s REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090NCwastember 1 2
NC Drinking Water 37706 This report "it not be reproducep, except in full. VA Drinking Water 213
Sc 99OD6 without the witten consent of Pace Amlytical Services . Im FL NELAP E87627
Pace Analliffell ServIves,Ific.
98W Kincey Avenue, Suite 100
Huntelswiti NC 28078aceAnalyficalPhone 704 875 9092
Falf.7104.875.901
QUALITY CONTROL DATA
Lab Project Number :924896 3
Client Project ID :03-JUL-0338/KI1356
LABORATORY CONTROL SAMPLE & LCSD : 923259709 923259717
Spike LCS LCSD LCS xFCSD
kA~Mato Conc . Reffult Result %Rec %Rec RPD Footnotes
N-Nitrozodiphenylausine ug/I 50 .00 28 .15 32 .73 56 66 15
Fecotalchlorophervol ug/i 50 .00 31 .57 35 .69 63 71 12
Pheolicathrene ug/1 50 .00 30 .01 34 .50 60 69 1 4
Pherfol ug/1 50 .00 9 .068 12 .44 is 25 31 3
Pyrexua ug/i 50,00 38 .62 45 .31 77 91 16
1,2,4-Trichlorobeciazerive ug/1 50 .00 25 .67 29 .26 51 58 13
2,4,5-Trichlorophertol ug/1 50 .00 32 .81 38 .55 66 77 16
2,4,6-Trichlorophenol ug/1 50 .00 29 .83 36 .07 60 72 19
Nitrobenzeci IS)49 55
2-Fluorobiphernyl IS) 50 58
Terphenryl-cI14 IS)74 85
Phisourci IS) is 24
2-Fluorciphillool IS)22 33
2,4,6,Tribrph.01 IS) 67 72
MATRIX SPIKE a MATRIX SPIKE DUPLICATE :923259733 92325974 1
923239040 Spike ME MsD ME KSD
Parameter -Units Result Conc .Result Result Rec Is Rec Up Footnotes
Acereplatheme ug/1 0 50 .00 32 .48 30 .67 65 61 6
4-Chloro-3-mathylphenol ug/1 0 50 .00 35 .69 27 .58 71 55 26
2-Chlorophmol ug/1 0 50 .00 27 .70 23 .55 55 47 16
1,41-Dichlorobenzene uq/1 0 50 .00 26 .16 28 .02 52 56 7
2,4-Dinitrotolume ug/1 0 50 .00 40 .17 38 .43 so 77 4
4-Nitrophimccol ug/1 0 50 .00 17 .76 14 .14 36 28 23
N-Nitroso-di-a-propylamine ug/1 0 50 .00 25 .71 26 .27 51 52 2
Pentachlorophencol ug/1 0 50 .00 36 .03 32 .23 72 64 11
Phenol ug/1 0 50 .00 12 .99 10 .78 26 22 19
Pyreme ug/1 0 50 .00 46 .11 42 .73 92 86 8
1,2,4-Trichlorobenzene ug/1 0 50 .00 28 .05 28 .74 56 58 2
Nitrobetbaceri IS)54 55
2-Fluorobiphenyl IS) 57 55
Terphenyl-dl4 IS) 88 83
Phenol-d5 IS) 25 21
2-Fluorophenol IS) 35 28
2,4,6-Tribromopherrol IS) 75 7 0
Date~08/26/03
Page : 12 of 1 5
I ahnraloN Cenilabon 105 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090NGWasteenater 1 2
NC Drinking Water 37706 This report stual not be ferroduced, OxcePt in full,VA Drinking Water 213
SC 99DD6 without the witten convint of Pace kia"I Serinces,Inc . ft NELAP E87627
Pace AnsVlal Serlefen .Inc.98M KeTMAveffale, Suiti;100
Huribsk1fle,AC 28078cleAnalyfical"AM 704 875 9092
wvAy.pacelabscorn Fax 704.875.M
QUALITY CONTROL DATA
Lab Project Number :924896 3
Client Project ID :03-JUL-0338/KI1356
SAMPLE DUPLICATE :923259725
923239248 DUP
Raralleter-Unite Result Result gPD Footnotes
AcernaPhth=e ug/l ND ND KC
Ac,roapht1tylecte ug/l MID ND NC
Aniline ug/l ND NID NC
Anthracene,ug/l ND NID KC
Benzo (a) anthracene ug/l ND NID KC
Benuco (a) pyrene ug/l MID ND NC
Bmzo (b) f luoranthiffne ug/l ED NID NC
Bel (g, h,i) perylene ug/l ND NID NC
Senzo (k) f luciranthene ug/l ND ND KC
Sal acid ug/l ND ND NC
Senryl alcohol ug/l ED ND NC
4-B,,,,pha,ylph=yl ether ug/l ND NID KC
Butylbetucylphthalate ug/l NID ND KC
41-Chloro-3-alethylili"AH301 119/1 ND ND NC
4-Chloroaniline ug/l ND ND NC
bis(2-Chloroatboxy)methane ug/l ND ED NC
bio(2-Chloroothyl) ether uq/l ND MID KC
bis(2-Chloroisopropyl) ether ug/l ND ND KC
2-Chlormaphthalme ug/l MID ND NC
2-Chlorophwol ug/l ND ND NC
4-Chlorophenylpbenyl ether ug/l MID ND NC
Chryseene ug/l ND MID NC
Dibelaz(a,h)anthracene ug/l MID ND NC
Dib=zofur=ugr/l ND ND NC
1,2-Dichlorobenzene ug/l MID ND NC
1,3-Dichlorobenzene ug/l ND ED KC
1,41-Dichlorobecluceate ug/l ND ND KC
3,3 --Dichlorobenzidine ug/l KID ND NC
2,4-Dichlorophenol ug/l ND ND NC
Diethylphthalate ug/l MID ND NC
2,4-Dimethylphenol ug/l ND ND NC
Dimethylphthalate ug/l ND ED NC
Di-n-butylphthalate ug/l ND MID NC
4,6-Dinitro-2-methylphenol ug/l ND ND NC
2,4-Dinitropbenol ug/l MID ND NC
2,4-Dinitrotolume ug/l ND ND NC
2,6-DinitrotOlume ug/l ND ND KC
Date :DS/26/03 Fix,: 13 of 15
1 Aborlift'll,Unification Iabratorll certirlatom-1125 REPORT OF LABORATORY ANALYSIS Ky Drinking Water 90090NGWastewater 1 2
K Drinking Water 37706 This report shall not be reproduced, except in foil,VA Drinking Water 213
SC 99DO6 without the written consent of Pau ilotaPylical Set*"Im FL NELAP E87627
pacti,Ano4ill Serliflins,Inc.
M Kinm Aviblue, Suits 100
Hunwitillt MC 2WM
Phow 704.875.9092aceAnalytical'Fax.[phone]inn"f,paoelabs wm
QUALITY CONTROL DATA
Lab Project Number :924896 3
Client Project ID : 03-M-0338/01356
SANPLE DUPLXCATE : 923259725
923239248 DUP
EtlamqLqL~
Unite Result Result 9PD Pucrtnoteag
Di-n~octylphthalrrrtra ug/1 ND ND NC
1,2-Diphenylhydrazine ug/l ND ND NC
bis(2-Ithylhexyl)phthalate ug/1 ND ND NC
Pluortanthene ug/l ND ND NC
Fluorebus ug/l N11,ND NC
9,,g,claloro-1,31-butardirappre,ug/1 ND ND NC
Er,orsupblorobenzene ug/l N11, ND VC
liefiechlortacyclopentlediene ug/l IND ND NC
Haticachlorcethane ug/1 ND ND PIC
1zpdeno(l,2,3-cd)y,yreuae ug/l ND ND NC
loophorcise ug/1 ND ND KC
2-M,tbylbruelphthislene ug/l ND ND NC
2-MethYlph=Ol (o-Cresol~ug/l ND ND VIC
3&4-Methylpherpol uq/1 ND ND NC
Naphthalene ug/l ND ND NC
2-Nitroarailizues ug/l ND ND KC
3-Nitroappiline ug/l ND ND NC
4-Nitroaniline ug/l ND ND NC
Nitrobenzerre ug/1 ND ND NC
2-Nitraphercual ug/1 ND ND PIC
4-Nitropheni ug/l ND ND NC
N-NitrooodimethYlazine ug/1 ND ND NC
N-Nitroso-di-a-propylanine ug/l ND ND NC
N-NitrosodiPhmYlminO uq/1 ND ND KC
Pentachlorophenual ug/l ND ND NC
Ph---tb,rme ug/l ND ND NC
Phenol ug/l ND ND NC
Pyrene ug/l ND ND NC
1,2,41-Trichlorobenzenf,ug/l ND ND NC
2,4,5-Trichloropb,=Ol ug/l ND ND NC
2,4,6-Trichlorophertural ug/1 ND ND NC
Nitroberpicepri (S) % 58 6 2
2-Fluorobipheppyl (S) % 58 61
Terpheri (S) % 99 9 6
Plarcal (S) % 0 0 5
2-Fluorophanol (S) 1 0 5
2,4,6-Tribroaripopherpol (S) 13 11 5
Page : 14 of 15
Data :DO/26/03
1,horathN rendicalhan Ds
REPORT OF LABORATORY ANALYSIS KY DrinkirV Water 9OD90
NC Drinking Water 377G6 This report shall not be reprocticed, except in full . VA Drinking Water 213
SC 99f without me nnen consent of Pace AMM~l Services .Inc FL NELAP E87627
Pace Alaslyffeal S01*611,10C .
M KinMAym, Suite 100
Hunwitfle,NC 2W78aceAnalXical!-Pitim:M4.875.9M
M"Y"Mostabs.com Fac 704.875.091
Lab Project Number :924896 3
Client Project ID ;03-JUL-0338/MI135 6
Consistent with EPA guidelines, unrounded concentrations are displayed and have been used to calculate %Rec and RPD values .
LCS(D)Laboratory Control Sample (Duplicate )
MS(D)matrix Spike (Duplicate)
DUP Sample Duplicate
ND Not detected at or above adjusted reporting limit
NC Not Calculabl e
J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
HDL Adjusted Method Detection Limi t
RPD Relative Percent Difference
(S)Surrogat e
III Recovery falls outside of OC limits, however, this compound is not found in the associated samples .
(21 The calculated RPD "a outside QC acceptance limits .
[3)RPD value "a outside control limits, however both percent recoveries were acceptable . Sample results for the
QC batch were accepted based on percent recoveries and completeness of QC data .
[4) The surrogate and/or spike recovery was outside acceptance limits .
[5)The surrogate recovery was outside QC acceptance limits due to matrix interference .
Datei 08/26/03 Page :15 f is
aborainN Cerldicabeen iLaboraboN Certification 195 REPORT OF LABORATORY ANALYSIS KY Drinking Water 9OD90NCWastewater 1 2
NC Drinking Water 37706 This report "it not be reproduced . except in lull,VA Drinking Water 213
Sc 9M wilhout the wittlen consent of Pace Analytical Services, Inc. FL NELAP E87627
Burlington MGP
October 2003 Groundwater
Field Analytical Data
Field Calibration Forms
Groundwater Monitoring Data Sheets
Chain Of Custody Records
Laboratory Analytical Data
Burlington MNA Proposal /Appendix B
BURLINGTON OPERATIONS CENTER -MGP SITE
GROUNDWATER MONITORING FIELD DATA
SAPROLITE WELLS
AVGWELL DEPTH TO PROD PUMP WELL EVAC WELL EVAC SPECIFICWELD(E III WATER LEVEL RATE -VOL VOL VOL VOL EVAC TEMP pH CONDUCTANCE DO ORP TO"DATE NO.f:O (f_,)
(feet) ODOR (ad/niin)
O=dgC (units) bu cca g" (.V) (NTU)10121/2003 PPWB-D
8,8 801 6-2
-8 R2- il,66)L2 5)NO 20450TTL20,7 67-6-49A 3r97±388-38)1.07 (F07,0.d.147,147 .14T-5 .14 .6,4,610121/2003 PMWC-D 25.20 13 .47 NONE NONE T60 ';L -8NONE NONE 87 .5 7.24 10AI 1 .91 2 .75 NO 20.0,20.0,19 .9 6.6.6,6.6 .6 538,542 .543 0,22'0 13, 0.13 156,150,149 4 .1,4 .5 .4,5l0f2l12003PMWFD 16.32 7 .51 NONE NONE 300 5." 5 .69 L" 1 .50 YES 20,0,20.0 6.7 .6.7 967 .952 0.31 0,06 97,79 11 .2,9 .110/20~003 PMWG-D 19,07 9,12 NONE NONE 260 6,14 13 .25 1,62 3 .50 NO 19.1,19.1,19 .1 6.1,6 .1,6 .1 513 .517,518 O~07, 0108, 0.06 199,194 .191 3,2,3 .5,3 010120/2003 PMWI 16 .12 10,71 NONE NONE 50 3.34 5 .68 0 .98 1,50 NO 216, 22 .7, 22 .8 6,8,6 .8,6 .8 410.411 .411 0 .47,0 37, 0.33 94,93 .92 5,0,4,4,4 .2lOn2/2003 PMWL-D 9 .70 3 .89 NONE NONE 40 3.59 5 .68 0 .95 1,50 NO 21 2 .21 .2,21 .3 6.0. 6 .0, 6 .0 307,3W. 302 1 .1,0 .87 .0,78 264,266 .268 15 .3 .13 .8 .13 .9
OVERBURDEN WELLS
AVGWELL DEPTH TO PROD PUMP WELL EVAC WELL EVAC SPECIFI CWELL DEPTH WATER LEVEL RATE -VOL VOL VOL VOL EVAC TEMP pH CONDUCTANCE DO ORP TURBDATE NO .(feeo ODOR (adifirti .) (I I I 'Llerj)11!~-)(deg Q (units)(ustah./c.)fing/1)INTO)4 61 27 N
a`V )I er1012Y2003 MW-3 7-24 r2_39L NONE NONE -250 0-81 0 19,2,19 .2 .ig 1 58,58 5l;.11 ".10.U.13,0A6 3"44-7318 21 .28.2910/20/2003 MW-5 13 .54 6,36 NONE NONE 115 4 .43 7 .57 1 .17 2,00 NO 21 .5 .21 .5 .21 .4 6 .8,6S, 6.8 950,950,948 0.19,0.12,0 .09 102,98,93 6 .3 .6.2,5 .910/22/2003 MW-9 9.50 6 .96 NONE NONE 109 1 .57 3 .79 0.41 1 .00 NO 21 .8,21 .7,21 .7 6 .2.6 .2,6.2 616,626 .643 0,36. 0 26,0.22 275 .259,264 38,61,3310=003 PMWB-S 13 .58 7 .97 NONE NONE 70 3 .46 5 .68 0.91 1 .50 NO 23 .1 .22 .9,22,8 6 .8.6.8,6.8 825 .825 .826 O~06.0.06 . 0.05 77,75,74 9 .4,9D. 8A10/2112003 PMWC-S 21 .09 12 .37 NONE NONE 160 5 .38 8 .52 1 .42 2 .25 NO 19,3.19 .3,19 .2 6A6 .6,6 .6 477 .486,481 0.09.0 .08 . 0.08 105 .102,101 7 .1,74,6 .110=003 PMWL S 7 .60 191 NONE NONE 72.5 2 .28 4 .73 0.60 1 .25 NO 20 .7.20S, 21 .0 6 .1 . 6 .1 .6 .1 556,553 .554 1 .0,0 60.0 .40 160,160,159 H .12,12l0f20r2003PMWM S 12 .68 11 .28 NONE NONE 115 0,86 5 .68 0.23 1 .50 NO 19 .3,19A,19 .4 5 .5.5 .5,5 .5 140,141,142 0,60, 0 .65 . 0,70 423 .428,430 8 .0.12, t51012112003 P-IS 1171 7 .35 NONE NONE 202 2.69 6 .62 0.71 1 .75 NO 24 .7, 24 7,24 .7 6.5,6,5 .6 .5 1018 .1019,1017 0.()6.0 .05,0,04 182 .181 .180 19,14 .12
SRALLOW FRACTURED BEDROCK WELLS
AVGWELL DEPTH TO PROD PUMP WELL EVAC WELL EVACWELL DEPTH WATER LEVEL RATE VOL SPECIFI C
DATE NO .VOL VOL VOL EVAC TEMP pH CONDUCTANCE DO ORP TURD10/2312003 OMW-("'a"
(feet) (feet)ODOR leal/ndril Llftegl jjrea)L,.72)
Van'(dcg C!(units) "P ca (si (.V) (NTU)14 2_ 2L 4
415-07 6 .24 NONE 70NE 450
0 2 3 5
-10121f2003 DMW-2 32 .08 7 .29 NONE NONE 365 15 .30 50 NO 20.r2O.r2O.l 6 .r6 .0L-;,0 ID 120-312'3 0.11,0.08,0 .13 237.239,242 11,14.1110/2112003 PMWC-BR 36.00 24 .60 4 .04 6.50 NO 20.4, 20.4, 20 .4 6A,6 .4,6A 473 .474,475 0.04,0 .04 .0,04 170,169 .169 14 .8,1,8,112,43 NONE MINOR 935 14 .55 35 .96 3 .84 9.50 NO 18 .8 .18,8,18 .8 6 .5.6S .6.5 485 .483,481 0.05 . 0 .07,0.07 117.115,114 4g .4.3,4 .01012212003PMWHRR20.72 8 .10 NONE NONE 290 7.79 13 .25 2,06 3 .50 NO 18 .9 .18.9,18 .9 6 .3, 6 .3, 6.3 465,463 .461 0,06, OD5 . 0.05 113,112,110 11,11,11IW2012003 PMWI-BR 38 .07 10.19 NONE NONE 437 17 .21 24 .60 4 .55 6,50 NO 19 .5 .19.5 .19 .5 6 .6.6 .6 .6 .6 557,558,555 0.04, OD4,0 .03 86,86,86 2 .3.2 .6,2 .410122f2OD3PMWL-BR 24,46 5.81 NONE NONE 153 11 .51 15 .14 3 .04 4,00 NO 19 .6,19.8 .19 .9 6 .3.6 .3 .6 .3 326,329,326 0.27 .0 .27.0.25 229,231 .231 11,11,121012012003PMWM-BR 19,16 11 .29 NONE NONE 87 4 .86 7 .57 1 .28 2 .00 NO 19 .5. 1&5,18 .5 6.0, 6,13, 6 .0 244.243,241 0 .46,0,25.0,11 211 .210~210 2 .7 .23,23
COMMENTS
Water levels and well depths an, referenced in top of PVC casin g* =Avg pumping rate used to minimize or stabilize drawilman while removing one well volume and stabilizing indicator parameters,
FIELD SAMPLING CALIBRATION DATA FORM
STUoy :
DATE : 40 zo 103 WEATHER CONDITIONS: ('k-E0,A-
COLLECTORS :%-0 C~ (1-%, kKA SURFACE UNIT READER:%-W
HYDROLAB SERIAL Lk -) V G COMPUTER:3
OTHEREQUIPMENT:1AAClIt SURVEYOR SERIAL #:
Procedure Number 3210 .1
Calibration Time Time 0 53 ~J L~ Time Orl 15 Time
Barometric 1,01XI 10 3
Pressure 75Li, 5mmHg mmHg mmHg
Instrument Standard Instrument Standard Instrument Standard
Value Value Value Value Value Value
Thermomete r
No .(i hA rj A
TEMP > > >
(deg C) > > >
W
DO W
(Mgt')W
AW > > >
pH B > 7 .00 > 7 .00 > 7 .00
(units) B q-3o
> -
4 .00 3,VL >4 .00 >4 .0 0
B > 10 .00 > 10 .00 > 10.00
SPCOND SS 0 -L)> 0 .00 0~0 > 0 .00 >0 .00
(US/CM) SS >-7 ~L C)-204 .>-2 XO >
SS > > >
ORP SS 310 >;V),:~> >
(MV) SS > > >
/,I rJ J A
TURBIDITY SS > 0 .00 > 0 .00 > 0.00
(ntu)SS >>
KEY :B ~Buffer W =Winkler NA Not Applicabl e
SS =Standard Solution AW =Average Winkle r
-- -- > =Adjusted To -- / -- > =Not Adjusted To
FIELD SAMPLING CALIBRATION DATA FORM
STUDY :on C-P
DATE : 0 -z WEATHER CONDITIONS : -7
COLLECTORS:~-b C ft-SURFACE UNIT READER :Cz- k-J
HYDROLAS SERIAL -7 COMPUTER :L-Dc 3
OTHER EOUIPMENT'.11,604 1 Q^429 z A,cKu-'SURVEYOR SERIAL #:
Procedure Number 3210 .1
Calibration Time Time 0-2 J Time W)t5 Time
Barometric I O(xJ-1 a 3
Pressure r)mmHg '-I mmHg mmHg
Instrument Standard Instrument Standard Instrument Standard
Value Value Value Value Value Value
Thermomete r
No .V1 J 1A
TEMP > > >
(deg C) > > >
ed 0W
DO W
(mgA)W
AW -T 3 'd - 0 >
pH B >7 .00 > 7 .00 > 7 .00
(units) B
> -
4 .00 4,03 >4 .00 >4 .00
B > 10 .00 > 10 .00 >10 .00
SPCOND SS 0 .0 > 0 .00 0,0 > 0 .00 > 0 .00
- --- ~ff(US/Cm) SS > > -7 -;1-0 >
SS > > >
ORP SS b >3L->l 302->;t-9 >
(MV) SS > > >
TURBIDITY SS 44> 0 .00 0 .00 > 0 .00
(ntu)SS
KEY : B =Buffer W =Winkler NA Not Applicable
SS =Standard Solution AW =Average Winkle r
> =Adjusted To -- / -- > =Not Adjusted To
FIELD SAMPLING CALIBRATION DATA FORM
STUDY :C--J1\A (-?
DATE : t.Q I k ;2- ( o WEATHER CONOMONS: (7 LL-A4\.,P 4~,CIF Z
COLLECTORS :~_f) c i il SURFACE UNFT READER:rL ~-W'
HYDROLAB SERIAL #:3-f ? Y 6 COMPUTER :3
OTHER EQUIPMENT :(AAC tA I \J Z,n &-TIZ r~-SURVEYOR SERML 0 :
Procedure Number 3210 .1
Calibration Time Time Time a -1 % 5 Time
Barometric 1 0 M-310 3
Pressure 'NO mmHg ~7 4 'A , 0 mmHg mmHg
Parameter Calib . Instrument Standard Instrument Standard Instrument Standard
I Value Value Value Value Value Value
Thermometer
No .vi
A
TEMP > >
(deg C)
W
DO W
(mg/l)W
AW L)~s >
pH B > 7 .00 4 -') 4 -- -- > 7 .00 > 7 .00
(units) B 0 >4 .00 3 -CJ 0 >4 .00 >4 .00
B > 10 .00 > 10 .00 > 10 .0 0
SPCOND SS 0 -0 >0 .00 > 0 .00 > 0 .00
(US/cm) SS ->7,;t-0 > -72-0 >
SS > > >
3L >ORP SS ?o >*% ol,>
(MV) SS >
(A V'JJ A
TURBIDITY SS >0 .00 > > 0 .00
(ntu)SS > >
KEY : B =Buffer W =Winkler NA Not Applicabl e
SS =Standard Solution AW =Average Winkle r
> =Adjusted To -- / -- > =Not Adjusted To
FIELD SAMPLING CALIBRATION DATA FORM
SrUDY:
DATE :7-3 /1 3,WEATHER CONDITIONS:C~eAO-
COLLECTORS :0)(L SURFACE UNIT READER :~-o
HYDROLAB SERIAL 8:COMPUTER :C-
OTHER EOUIPMENT : J'INAC 0 J NZ 1J)rM E lrt~1"-SURVEYOR SERIAL C
Procedure Number 3210 .1
Calibration Time Time C,),l Time ~01 C)Time
Barometric
Li 0Pressure mmHg Li 57 mmHg mmHg
Parameter Calib . Instrument Standard Instrument Standard Instrument Standard
I Value Value Value Value Value Value
Thermometer V ~No .V- VA-
TEM P
(deg C)
W
DO W
(mgA)W
AW g,q
pH B 74 7 .00 (6,20 > 7.00 >7 .00
(units) B '3 , cl 4 .00 >4.00 >4 .00
B > 10 .00 > 10 .00 > 10 .00
SPCOND SS 0,0 >0 .00 n 'n --/> 0 .00 > 0.00
(US/CM) SS 2, 1 ->
SS > >
ORP SS 3 o 9 >3 ic~- 31o >
(MV) SS - >
0 .00TURBIDITYSS >0.00 >0 .00
(ntu)SS > - >>
KEY:11 ~Buffer W =Winkler NA Not Applicable
SS =Standard Solution AW =Average Winkle r
-- -- > =Adjusted To -- / -- > =Not Adjusted To
UUMIC rVVVCr1 %,%JIV[rAI'4 T
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
LOCATION :I BURLINGTON, NC PROC NO : 1 3500
PROJECT NAME: IBURLINGTON MGP (SAPROLITE WELLS)FIELDCREWd LDC,RLW
ISAMPLING DATE :-Z0-0cT-TJ,T-j 21-Oct-03 I 22-Oct-03 20-%0 2
MONITORING WELL NO .PMW13-771
WATER LEVEL METER S/N
: '
A
PID READING npm PRODUCT LEVEL METER S/N : Ejj-~j I
METHOD (Pump /Sail)1PERISTALTIC PUMP I TIME / INITIALS OF COLLECTED SAMPLE:xs-
WELL VOLUME CALCULATION :
WELL W IWELL DE=jiTH TfO WAT CONVERSIONN W1E LILtj VolL 'IVolLNJ
DIAM DEPTH (ft)WATER. it X 7FACTOR L alI)
2-18 .18 X 0 .1631
X
N/A gallons X 1 3 .785 1 N/A I 7tes7
SCREENINTERVA L
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
18 16 .68 Ift TYPE, DEPTH TO WATER :ISTRONG~DEPTH TO PRODUCT,j~104e- (ft)
MINOR PRODUCT THICKNESS :_(ft)
Pump INT!~IKEJ NONE : IDON'T SAMPLE IF THICKNESS >OR =TO 0.1 FT I
1 .7 'o ftATSTARTAT
E
:N5D
17.50 It it
INITIAL READINGS MEASURED AT GROUNDWATER /AIR INTERFACE INDICATED BELO W
W
A FLOWRATE TEMP SPEC TURBIDITY JoH ORP DISSOLVED
TIME LEVEL COND OXYGEN-HTE
US/cm)(mu) (unit)(mv )(hh :mm~s (ml/mi I I (M A)
N/A N/A N/A N/A NIA N/A N/A N/A N/A'Y
WATER FLOWRATE TEMP --MM TURBIDITY]PH)ORP DISSOLVED
TIME LEVEL COND OXYGEN
(hh :mm :ss)(ft)(mi/min)(deg C) (US/cm)(ntu) (unit (mv) (mg/1 )
13 :xg '02 ~i' V ()k L 0 STABILIZED DRAWDOWN AND REMOVED j,'75 - BEGAN LOGGING DATA
I ~t *.1 0 .;L,7, 10'k o i 11-o ao-"?c 399,1? S,lq 4 -1 1 y'? 0-)
(4'.ts :5-21 1 Z~' %'; 1 (~ o 20 .14 3218,11 ~' I 1-i 1 -2 z:1
I Lf 3 10 (Lo -2 0 -7387 .8 i ~f 0 o-Y
ELECTRONIC FILENAME -mw (3,b
iCOM TS C--o
cl MYC~z r. -~t--0 11-~k 4~ '-t ~4e ^
k %~ to 15 ~11 - , ~J~'vp-~11 " - ~ %,,P, I,:, f'. A k 4~-
TOTAL VOLUP E REMOVED =41 sv~~- C .~ '1-~'-~p A-sj~
NOTE :WATER LEVEL, PRODUCT LEVEL .AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
UUr%t FL)VVtH t;L)MIJAN Y
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
LOCATION :BURLINGTON .NC PROC NO :
PROJECT NAME : BURLINGTON MGP (2~~ELLS)FIELDCREWd LDC,RLW
ISAMPLING DATE :~n-Ort-0.';I 21-Oct-03
MONITORING WELL NO .PMWC-D
WATER LEVEL METER SIN :N/A
PID READING MA,-S-.-L-,Lo1j
i~m
PRODUCT LEVEL METER SIN :kc~'vl - i
METHOD (I p /Ball)P TIME / INITIALS OF COLLECTED SAMPLE :H30
WELL VOLUME CALCULATION :
C CoILUMN ft0WELL WELL DEPTH TO WATER CONVERSIO WELLWATER [605iNiVVER~S~UO N
DIAM DEPTH (ft)EWATER (ft)ILUMN (ft) X FACTOR OL (gal)j
2'25 .20 X
X
N/A gallons X 3.785 N/A ht"s
SCREENINTERVA L
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
25 .20 23.70 ft .TYPE DEPTH TO WATER:I
STRONG :DEPTH TO PRODUCT :---ti tZ (ft)
MINOR~PRODUCT THICKNESS :=(ft)
PUMP INTAKEI NONE : IDON'T SAMPLE IF THICKNESS >OR =TO 0 .1 FT !
AT START I AT END
2 ;Is -r.N
INITIAL READINGS MEASURED AT GROUNDWATER AIR INTERFACE INDICATED BELO W
WATER FLOWRATE TEMP SPEC TURBIDITY PH)ORP D1995=
TIME LEVEL COND OXYGEN
(hh -,I's (ml/mi (us/cm)(ntu) unit (mv)(mg/l )
N/A NIA N/A N/A N/A N/A N/A N/A N/A
WATER FLOWRATF TEMP --prC TURBIDITY PH ORP DISSOLVED
TIME LEVEL COND OXYGE N
(hh :mm :ss)(ft)(mllmin)(deg C) (us/cm)(ntu)(mv)(MgA)
STABILIZED DRAWDOWN AND REMOVED ;7_,C)BEGAN LOGGING DATA
i o :5 3 -3 5'115,(9 cl 53 7, q Ll ~1,5- (' ~svj k 4 (0~ -ts
I I " o ~-"-5 ;1--& Q ;2,C),L-538,1 q, 10 4 (-5 L 0,
11-ko ILIC't I-), ? ct 90 (cl C75 '54 1-? If'5--f 6 /~'-o o'I
i r .1(. ~cl n'V5 o(o vi .ClLe Sly-Z-9 1~~ 50 C-5 -2 3
ELECTRONIC FILENAM E- pcy\~'Jcb c'A p
COMMENTS :(-,3 w
TOTAL VOLUME REMOVE D
NOTE :WATER LEVEL, PRODUCT LEVEL,AND WELL DEPTH ARE REFERENCED TO THE TOPj0FWELLEGASING .
LJUNC ruvvcm L'UIVIII-All4 v
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
LOCATION :IBURLINGTON, NG PROC NO : 3500.1
PROJECT NAME : IBURLINGTON MGP (SAPROUTE WELLS)FIELD CREW :LDC,RL
SAMPLING DATE :20-Oct-03 I X_-Da~~~~K-AC,
MONITORING WELL NO .PMWF-D`___~~
3
WATER LEVEL METER S/N :N/A
PID READING _~ A ~7_ ppm PRODUCT LEVEL METER SIN :
METHOD (Pump /Ball)1PERISTALTIC PUMP TIME I INrTIALS OF COLLECTED SAMPLE :
WELL VOLUME CALCULATION :
WELL WELL IYEPTH TO WATER CONVERSION WEL LCoF~~DIAM DEPTH (ft)WATER (ft)
)LUMN ft X
FACTOR VOL (gal)
2'16 .32 X
X
N/A gallons X 3 .785 N/A lit,717s :~]
SCREENINTERVA L
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
16 .32 ft. 14 .32 TYPE : DEPTH TO WATER :I
STRONG :DEPTH TO PRODUCT :---No 00
MINOR 04 PRODUCTTI =(ft)
Pump INTAKE NONE: BON'T SAMPLE IF THICKNESS >OR TO 0 .1 FT !
AT START AT iND
16 .32 4 ~~J.Ift
INITIAL READINGS MEASURED AT GROUNDWATER AIR INTERFACE INDICATED BELO W
WATER FLOWRATE TEMP SPEC TURBIDITY PH DRIP Dls§a=
TIME LEVEL COND OXYGEN
(hh mm*ss) (ft)(ml/min)(US/cm)(nt (unit)(Mv) (mg/1 )
NIA N/A N/A N/A N/A N/A N/A N/A N/A
--MF6WATER FLOWHATE TEMP T TURBIDITY PH)ORP DISSOLVED
TIME LEVEL COND OXYGEN
(hh :mm :ss)(ft)(mftin~(deg C) lus/cm)(nfu) (unit (mv)(m9A)
ri(0i /,-('I STABILIZED DRAWDOWN AND REMOVED ~(4 -BEGAN LOGGING DATA
IV 3 J-4 01 tol,.-"01",r)a--1~t_31
i Li ~j 9 CD 0 &Z 01,
-n-Ao ~,IkIZI
g .'i A C~,ATd I A A c-,J N r5s A C- ft-c~-(I.-, (3, 1 .
qwt;A If 4 C 4 4 1 3 3 1~z ci
163
It. b 01 /.A_1 In 3 o
ELECTRONIC FILENAME -4y\
uurl.r rvvvr_ri t1UIVIrAI%j T
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
LOCATION :BURLINGTON, NC PROC NO :
PROJECT NAME, BURLINGTON MGP ISAPROLITE WEI FIELDCREWd LDC,RLW
SAMPLING DATE :20-Oct-03 1 24 F;.t
MONITORING WELL NO .PMWG-D
WATER LEVEL METER S/N : N/A
PID READING M PRODUCT LEVEL METER S/N :-7
METHOD (Pump /Bail)PERISTALTIC PUMP TIME / INITIALS OF COLLECTED SAMPLE :
WELL VOLUME CALCULATION :
WELL WELL FDEPTH TO WATER C0NVERSI10qN WEL LR F IVolL [a[
DIAM DEPTH (11)L WATER (ft)COLUMN ft X FACTOR L 'a
2-19 .07 '9 X
j X
N/A gall,ns X 3 .785 N/A litIls
SCREENINTERVA L
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
19 .07 16 .57 Ift TYPE : IDEPTH TO WATER :
STRONG :DEPTH TO PRODUCT :---
IVIINOR~PRODUCT THICKNESS : = (ft)
PUMP INTAKE NONE: I V IDON7 SAMPLE IF THICKNESS >OR =TO 0 .1 FT I
AT START I AT END
fl
1 Ib .0
INITIAL READINGS MEASURED AT GROUNDWATER I AIR INTERFACE INDICATED BELOW
WATER FLOWHATE TEMP SPEC TURBIDITY PH ORP DISSOLVED
TIME LEVEL COND OXYGEN(hh :mMs (MI/Mi (us/cm)(ntu) unit)(Mv)(mgA )
N/A N/A N/A N/A N/A N/A N/A N/A N/A
WATER FLOWMAIL I tzMv --70 TUR131DITY (PH ORP DISSOLVEDTIME LEVEL COND OXYGE N(hh :mm :ss)(milmin)(deg C) (US/cm)(ntu) unit)(mv) (mg/1)
(5 ;2T .,OY 7-(.0 STABILIZED DRAWDOWN AND REMOVED 1 75'BEGAN LOGGING DATA
16 ',-2-y'- 3 8 L 0 - '.I-L 0 k cl - 3 q93 5-36 1 t 2-15 olig
15'. 3 LV-3 9 i 0 1 x It ;L-&0 1 cl . tot ~50A-t.Li .~l .11 a OY 0,1(2
is : Y ;Z,. I q (a k ;g '140 ict .I :)-51 A,8 3 A (.,to (q 81 0'7
1'~q0t " It cl i 0 k ci 2 L 0 k 01. 1, 0 514-1 3 4-10 CA
Is q 1, 0 - A 0 ;LL It ell -0 5 5(9-.l 6 .1 0
~'p "--10
ELECTRONIC FILENAME -VMWG 1) C A
COMMENTS :<-ov 6 vo :'04N if L-3k~"/
4001 = ~1
TOTAL VOLUME F C-A L-
NOTE :WATER LEVEL, PRODUCT LEVEL,AND WELL DEPTH ARE REFERENCED TO THELTOP OF WELLMCASINGI.--
UUKt IJUVVtK %~UJIVIrA14 Y
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
LOCATION :PROC NO : 1 3600 .1
PROJECT NAME : BURLINGTON MGP (SAPROLITE WELLS)FIELDCREW :j LOG, RLW
ISAMPLING DATE:20-Oct-03 I -UQet-~-
MONITORING WELL NO.PMWI
WATER LEVEL METER SIN :N/A
PID READING o Q rz, M PRODUCT LEVEL METER S/N :so - I
METHOD (Pump/ Bail)1PERISTALTIC PUMP TIME / INITIALS OF COLLECTED SAMPLE :t'k o o
WELL VOLUME CALCULATION :
CoWELL WELL DEPTH TO WATER CONVERSION W1kEL LILUMN ft Vol ;IL 'al
DIAM DEPTH (ft)WATER (ft) X FACTOR al)I
2'16.12 X
- I X
1 9
0 .,6g gallons X 3.785 .3, -3 lite,s
SCREENINTERVAL 3 33~1
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMEN T
16 14 .12 Ift TYPE : IDEPTHTOWATER :I
STRONG DEPTH TO PRODUCT :---I otJE (ft)
MINOI PRODUCT THICKNESS : = I (ft)
Pump INTAKEI NONE: ]DON'T SAMPLE IFTHICKNESS >OR =TO 0 .1 FT I
ATSTART ATEN D
15 ls .~
INITIAL READINGS MEASURED AT GROUNDWATER /AIR INTERFACE INDICATED BELO W
WATER FLOWHATE TEMP SPEC TURBIDITY pH)oRP DISSOLVED
TIME LEVEL COND OXYGEN
(hh mnss)(11)(MI/Mi lus/cm)(ntu) unit (Mv)(mgA )
N/A N/A N/A N/A N/A N/A N/A N/A N/A
WATER FLOWRATE TEMP --M51-T TURBIDITY PH ORP DISSOLVED
TIME LEVEL COND OXYGE N
(hh :mm :ss)(it) (ml/min)(deg C)(us/cm)(ntu) (unit)(Mv) (Mg/0
k 3 :3 -)-I.k 'j ~-7 60 STABILIZED DRAWDOWN AND REMOVED I I Q CIA EGAN LOGGING DATA
ur 3-):.53 1 Li .-?7 -So ~~,sx A-10 I ~g ( , - xig i 4x 014
Z3 I ~~ -7 4 '50 L101-3 S-00 6 . ~6 1
a.1 N,w-? '50 22 .-?o ly 1 1 .Lf .to.6
53 -t 14,-C~ 1 ;1.2 .-?q .A ci
~o ~Loloj oc k too
ELECTRONIC FILENAME -PMVAT-CA P
COMMENTS :
TOTAL VOLUME REM VIED C-A L
NOTE,WATER LEVEL, PRODUCT LEVEL,AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
~~F%~ rWVy"n I
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
LOCATION :I BURLINGTON, NC PROC NO : 1 3500.1
1PROJECT NAME: 1BURLINGTON MGP (SAPROLITE
W~~LL"
FIELDCREWd LDC,RLW
ISAMPLING DATE : I 22wO~1-03 1 -12~~~o C
MONITORING WELL NO .PMWL-D
WATER LEVEL METER StN :N/A
PID READING G, 61 M PRODUCT LEVEL METER S/N :
METHOD (Pump/ Bail)1PERISTALTIC PUMP TIME / INITIALS OF COLLECTED SAMPLE :
WELL VOLUME CALCULATION :
CoILUM OLWELL WELL DEPTH TO WATER FCONVERSIO~WELL
DIAM DEPTH (ft)WATER (ft)N It X FACTOR
V
L I
al
2'9 .70 3 ~V cl X
X
N/A gallons X 3 .785 N/A 1Hibe~11
SCREENINTERVA L
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
9 .70 8 .70 Ift TYPE I DEPTH TO WATER : T____STRON&IDEPTH TO PRODUCT :--- I r-j (ft)
MINOR~I PRODUCT THICKNESS : = I (it)
PUMP INTAKE NONE : IDONT SAMPLE IF THICKNESS>OR =TO 0.1 F71
ATi~ART..I AT ;n
9 .7 cil
ft
INITIAL READINGS MEASURED AT GROUNDWATER AIR INTERFACE INDICATED BELOW
WATER FLOWRATE TEMP SPEC TURBIDITY PH ORP DISSOLVED
TIME LEVEL COND OXYGEN
(hh :mm :ss)(ft)(mumi (us/cm)(ntu) (unit)(mv) (mg/0
NIA N/A N/A N/A NIA N/A N/A N/A N/A
WATER FLOWHATE TEMP -9m I TURBIDITY DISSOLVED
TIME LEVEL COND OXYGEN
(hh :mm :ss)(ft)(ml/min)(deg C) (us/cm)
(nt (unit)
(mv) (mg/0
~F L(STABILIZED DRAWDOWN A D REMOVED 1%0 cjAj -BEGAN LOGGING DATA
ip .ILI'3 .1- Ase,1 30~-t, 4,03 _-2 4
I o 'A,, I ~=j 0 2\,ke 30C .4 15,3 4,00 2114 1 , 0,v
'0 -to ;z ~,k 3o3_~7 0, 3 s .cj 6 0 8-7
k 3 6-VI 1 1-y 1);L 3oa..a 1 3,01 51 C15-0 :~ 8
I L 0 1'x 0 3
ELECTRONIC FILENAME -ff) LAJ L_A jP
,~AJJ)VNCOMMENTS:ocjW
TOTAL VOLUME REMOVED
NOTE :WATER LEVEL. PRODUCT LE EL, AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
Liumv- r%jvwL;n v
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
LOCATION : N, NC PROC NO : I 3SO0 .1
IBURLINGTON MGP (g~~~~ELLS)FIELDCREW :j LDC,RLW
ISAMPLING DATE:20-ect-e9 4-2t-qAt nq 1 Qal-L~ 23-Oct-0 3
MONITORING WELL NO.MW-3 I
WATER LEVEL METER SfN :N/A
PID READING ~4 Li PPM PRODUCT LEVEL METER S/N :-i c;
METHOD (Pump I Ball)PERISTALTIC PUMP TIME / INITIALS OF COLLECTED SAMPLE :')c
WELL VOLUME CALCULATION
: 'ON WELLWELL WELL DEPTH TO WATER CONVERSICo)LUMN ftCo)L R Vol[L Ja i
DIAM DEPTH (ft)WATER III)UMN (ft) X FACTO
L al
2-22 .24 1 - 3~X
=q X
N/A 911101s X 3 .785 N/A lite,s
SCREENINTERVA L
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
2 12 .0 ift TYPE : I DEPTH TO WATER-ISTRONG~IDEPTH TO PRODUCT :---I "j'vj c- (h)
MINOR,IPRODUCT THI = I (ft)
Pump INTAKE NONE :kZ DON'T SAMPLE IF THICKNESS >OR =TO 0 . 1 FT !
AT START AT END i t
INITIALREA INGS MEASURED AT GROUNDWATER /AIR INTERFACE INDICATED BELOW
WATER FLOWRATE TEMP SPLC TURBIDITY PH ORP DISSOLVED
TIME LEVEL COND OXYGEN
(hh :mm,ss)(ft)(MI/mil (us/cm)(ntu) (unit)(mv) (mg/1 )
N/A N/A N/A N/A N/A N/A N/A N/A N/A
WATER FLOWRATE TFMP --91IM TURBIDITY PH)ORP OISSOLVFIJTIME LEVEL COND OXYGE N
(hh :mm :ss) (it) (ml/min)(deg C) (US/cm)(ntu) (unit (mv)(mgA)
;L- STABILIZED DRAWDOWN A DREMOVEDJ .?~;dAl- EGANLOGGINGDATAI
o-) 2 ;2-50 1q, k L~ka?. 3 ;~Li .5-i~,-7 31 1 005
09 1 ~s 19 '2-'50 IIA-k 9 1 X 7 .1 A 'i , -)"5'. -?3 0,1 C
0 01 11"dcj ;L50 k ", I \ k 2-L .~A 27-~.57,-?3 Ok3
act 12,~'6~t 01,L)-7 7
5A .-vucN~oc)55- 0 3
ELECTRONIC FILENAME N vi 3, CM'
Comm S 'q P -1 b -A
iTOTAL VOLUME REMOVED )A L
I I NOTE :WATER LEVEL, FRODUL;I LEVEL,ANCFWELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
uur%r- r%jvvr-n %1%JIvIrMIM T
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
ILOCATION :IBLIRLINGTON, NC PROC NO :
PROJECT NAME : I BURLINGTON jMG1 !OVERBURDEN WELLS)FIELDCREW :j LDC,RLW
ISAMPLING DATE: I 20-Oct-03 2!eem 85 '.o c
MONITORING WELL NO .F-MW-5 __1
WATER LEVEL METER StN:N/A
PID READING I '_~M PRODUCT LEVEL METER S/N :
METHOD (Pump /Bail)1PERISTALTIC PUMP TIME / INITIALS OF COLLECTED SAMPLE :
WELL VOLUME CALCULATION :
CoWATER 1CONVERSIONCo)LUMN ft VOLWELL WELL WATER CONVERSION WELL
)LUMN (ft)FACTORDIAM DEPTH (ft)X FACTOR
I jai
I
2'13.54 XX En:d
N/A gallons X 3 .785 1 N/A liters
SCREENINTERVAL
DFROM TO DETECTE ODORS FREE PRODUCT MEASUREMENT
3 .54 Ift TYPE : DEPTH TO WATE R
STRONG :DEPTH TO PRODUCT :C (ft)
MINOR' PRODUCT THICKNESS : (ft)
PUMP INTAKE NONE : IDON'T SAMPLE IF THIC~NESS >OR =TO 0 .1 FT I
AT START AT END
1 jo'j
INITIAL READINGS MEASURED AT GROUNDWATER /AIR INTERFACE INDICATED BELOW
WATER FLOWRATE TEMP SPEC I =_PH ORP DIS9OLVED
TIME LEVEL COND OXYGEN
(hh 'mm'ss) (ft)(ml/min) (deg C) (us/cm)(unit)(mv) (mg/1 )
N/A N/A N/A N/A N/A N/A N/A N/A N/A
WATER FLOWRATE TEMP __9M TURBIDITY PH ORP DISSOLVED
TIME LEVEL COND OXYGE N
(hh :mm :ss)(ft)(mi/min)(deg C)(US/cm)(ntu) (unit)(mv)(mqA)
I .',Li 9 , ~' sr7 40 STABILIZED DRAWDOWN AND REMOVED 5 -BEGAN LOGGING DATA
1, 0-1 -L-_319 10 3_7 .IL cfqo,t;,s-'?I11, t3'4 .2-1 -t;,q q 4 q,5 4,;1 6 , -7 V 0 ~2,
116 ., kok' I 3!T a 1-4 16 ciso - 1 '79 CL & 01 ia
9 A 35-2 L \t 0 214 C~3 0'. cpt
Ii L 3 o
ELECTRONIC FILENAME -
COMMENTS C, 00 t,T -A h T ACl =
16 .
TOTAL VOLUh E F
PNOTE :WATERLEVEL, PRODUCT LEVEL,AND WELL DEPTH ARE REFERENCED TO TWE TOP OF WELL CASING
LIUF%L; rwvv"n ~wlvlrmll I
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
ILOCATION :IBURLINGTON, NC PROC NO : 3500.
1PROJECT NAME:BURLINGTON MGP (OVERBURDEN WELLS)FIELD CREW :LDC,R
ISAMPLING DATE : 1 22-01t-03
MONITORING WELL NO .MW-9
WATER LEVEL METER S/N :N/A
PID READING tj PPM PRODUCT LEVEL METER SfN : 'I ci 4
METHOD (Pump /Ball)PERISTALTIC PUMP TIME / INITIALS OF COLLECTED SAMPLE :~b c
WELL VOLUME CALCULATION :
CONVERSIONWELL WELL DEPTH TO WATER lco~DIAM DEPTH (ft)WATER (ft)COLUMN (ft)X FACTO R
2-9 .50 o C-;z - 5 X
~ -~ 4 X
N/A 911111,X 3 .785 N/A liters
SCREENINTERVA L
FROM TO DETECTED 0 ORS FREE PRODUCT MEASUREMENT
-0 ift TYPE DEPTH TO WATER :I_-STRONG :DEPTH TO PRODUCT ---pJ3!JC It
MINOR PRODUCT THICKNESS :_=It
Pump INTAKE NONE : IDON'T SAMPLE IF THICKNESS >OR =TO 0 .1 FT
AT START I AT END
ft.
INITIAL READINGS MEASURED AT GROUNDWATER AIR INTERFACE INDICATED BELO W
WATER FLOWHATF TEMP SPEC TURBIDITY (PH)DISSOLVEDTIME LEVEL COND OXYGEN
(hh :mm :ss)(ft)(ml/min) (deg C) (us/cm)(ntu) unit (mv) Img/0
N/A N/A N/A N/A N/A N/A N/A N/A N/A
WATER FLOWRATE TEMP --VIM TURBIDITY pH ORP DISSOLVED
TIME LEVEL COND OXYGE N
(hh :mm :ss)(ft)(ml/min)(deg C) (US/cm)(nt (mv)(mgA)
k~~Ltl '.5 1 ?,yo 10~-STABILIZED DRAWDOWN AND REMOVED BEGAN LOGGING DATA
3'.'A k'~ ~1 -7 .50 (05- 9,~L .-k--) ~? 9 -7
i V 5 1'. D,kc);;Z :Z,k 4 z0j ;;I~o
3 ~-~V'. 9 :1-k 0 -~ \ -8 ~-41,43 35, \A (.,\g ;z 0, 3
N-D .A .32 to I Z k --2 q 0S,61 .4 ci o .:)-/.
~t'. t 1 2-k o ci 3 ;z,.5 't :z
I L LA (z;-
ELECTRONIC FILENAME -C
COMMEN4 S :7 EYE 7 lAi)
.'CI = rp I
TOTAL VOLUME REMOVED
0
CA I-0
ffNOTE:WAjTEjRLEV!EML,EPROD=L~CTgLEVE L,AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
LJUF%" rwvv LLn %'wevirmill I
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
LOCATION : N . NC PROC NO : 3500.1
PROJECT N ME :BURLINGTON MGP (OVERBURDEN WELLS)FIELDCREW :L~LOC RLW
SAMPLING DATE :j .-ZLQ",Q3-I 21-Oct-03 I
MONITORING WELL NO .PMW
S
WATER LEVEL METER S/N :N/A
PID READING 3~-t m PRODUCT LEVEL METER SIN :
METHOD (Pump/Bail)1PERISTALTIC PUMP TIME / INITIALS OF COLLEC PLE:0
WELL VOLUME CALCULATION :
WELL WELL DEPTH TO WATER CONVERiION WELCoILUMNit
DIAM DEPTH (ft)WATER (ft)COLUMN (ft)X FACTOR IkS1
2'13.58 X
X
N/A gallons X 3 .785 N/A liters
SCREENINTERVA L
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
1 3 .58
ft .
TYPE :DEPTH TO WATER :
STRONG :DEPTH TO PRODUCT:--- or, kc (ft)
MINOR, PRODUCT THICKNESS :(ft)
Pump INTAKE N( IICKNESS >OR =TO 0 . 1 FT !
AT START ATEND
1
INITIAL READINGS MEASURED AT GROUNDWATER /AIR INTERFACE INDICATED BELOW
WATER FLOWHATF TEMP SPEC TURBIDITY PH ORP 15=5=TIME LEVEL COND OXYGEN
(hh :mmss) (ft)(deg C) us/cm)(nt (mv) (mg/0
N N/A N/A N/A N/A N/A N/A N/A N/A
WATER FLOWFIATE TEMP -3F0--7T=DITY PH ORP DISSOLVEDTIME LEVEL COND I OXYGE N(hh :mm :ss)(ft) (ml/min)(cleg C1 (us/cm)(ntu)(unit)(mv) (mg/1)
36'00 O~STABILIZED DRAWDOWN AND REMOVED ~0 QA1- EGAN LOGGING DATA
3?: 3 Q%,~a 'L 3 -c ~L 9 3 J~-,.1 o 5-6 "f,-!;
~t Lt -, -5 1 n,'61 Z .3 Lo-j 1~Ll Q,(j
50, 50 1 o -.~-Li 3 .~L-)95-7~ 0 o3 S~ s 6 0~)0
k L(SG I 1D io-3 V -7o 1 2-3 .:?-3 S3 ;>.o 1 0,0-2
IS " k)o I (0~51z-1,R 2- 3,LL 2; ZL(-5-,Y-~-0,oi6
is : Oct'. 4 t o .-?LL o X :Z .9 ~.k5 . 0 CA -oA 3iobj c)ex~-Ll 9 - 1 1 6 3
1 .~Afy\P ~ZzD I c ;;1-0
ELECTRONIC FILENAME -
r,O~MMENT~~~!~- PIJA
Z r-C- -~~ C, --~J A c-JA -Q-f aJ -P fn W S -t)Fr-,~<-7H~--T-
EMOVED=L -5 DITOTALVOLUMER
RODUCT LEVEL,A DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .INOTE :WATER LEVEL, P N D mL L,
L)UKr- rUVVCri tUIVI1'AI4 Y
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
ILOCATION :[BURLINGTON, NC PROC NO :3500 .1
PROJECT NAME : IBURLINGTON~~P V RBIRDENWELLS)FIELD CREW :LDC,RLW21~~
SAMPLING DATE :20 ect 09
1 03
29,n,f-Q3
-W, --71MONITORINGWELLNO.PMWC-S
WATER LEVEL METER S/N :N/A
PID READING Al ptj VJ~.:rr-c m PRODUCT LEVEL METER S/N :11 -(-1 - ~
METHOD (Pump/ Bail)1PERISTALTIC PUMP TIME / INITIALS OF COLLECTED SAMPLE:
WELL VOLUME CALCULATION :
CoWELL WELL DEPTH TO WATER CONVERSION WELLWELLVERSION
DIAM DEPTH (ft)WATER (it)
ILUMN ft X
FACTORACTOR0 163 1COLUMN (ft)VOL alI
2-21~09 3,X
X
N/A gallons X 3.785 N/A liters]
SCREENINTERVAL I
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
21 .09
ft
6 .09
f,
TYPE IDEPTH TO WATER :I
STRONG :DEPTH TO PRODUCT :(ft)MINOI 00PumpfNTAKEj NONE IDON'T SAMPLE IF THICKNESS >OR TO 0 .1 FT I
AT START AT EN D
1 1 -)- 0 ft
.
INITIAL READINGS MEASURED AT GROUNDWATER I AIR INTERFACE INDICATED BELO W
WATER FLOWRATE TEMP SPEC TURBIDITY PH ORP DISSOLVEDTIME LEVEL COND OXYGEN(hh :mm :ss)(ft)(MI/Mi (us/cm)~ntu) unit)(mv) (mg/1 )
N/A N/A N/A N/A N/A N/A N/A N/A N/A
WATER FLOWRATE TEMP SPEC TURBIDITY PH ORP DISSOLVEDTIME LEVEL COND OXYGE N(hh :mm :ss)(ft)(mUmin)(deg C)(us/cm)(ntu) unit)(mv) (mg/1)
t 1 . ~~(.i I, a STABILIZED DRAWDOWN AND REMOVED 5' q, I - BEGAN LOGGING DATA
OCJ~0-) 7 570 kL 0 1q .X-t LtL3-%i CA ~1 1 4-s-(.-10--)0.03
ocv.13 o c Li??,;L -)'10 e -:i 105-t'01
Oct -~ %%,-2-0 4y/-- I ~')' rj C S-1 ku :2-0,0a
001-1 3.3 52 L 4 i5o I Icl ~xo ciel .3 lo t
ct 2-5-
ELECTRONIC FILENAME -
COMMENTS :-%-%rc-'P")C:L L,
IC I
TOTAL VOLUME REMOVED JL -7-5 k
NOTE :WATER LEVEL, PRODUCT LEVEL, AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
UUM"V%.'VVLmn ~WIVIVMI'4 I
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
LOCATION, BURLINGTON, NC PROC NO : 3500
PROJECT NAME, BURLINGTON MGP (OVERBURDEN WELLS)FIELD CREW :LDC,RLW
JSAMPLINr.DATE :5)n-O,t 02 22-Oct-03 1 2&~
MONITORING WELL NO .PMWL-S
WATER LEVEL METER SfN :N/A
PID READING PRODUCT LEVEL METER S/N :
METHOD (Pump /Ball)1PERISTALTIC PUMP gm TIME / INITIALS OF COLLECTED SAMPLE:
WELL VOLUME CALCULATION :
WELL WELL DEPTH TO WAATER [CONVERSION WELLR Vol
DIAM DEPTH (ft)WATER Cft)COLUMN III X FACTOR L 'al
2'7 .60 3 .4 XX P~
gallons X 3 .785 IIt,rs
SCREENINTERVA L
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
7.60 4 .10 ift .TYPE : DEPTH TO WATER :
STRONG :DEPTH TO PRODUCT:---L:r (ft)
MINOR : PRODUCT THICKNESS :=(11)
PUMP INTAKE NONE IlCKNESS >OR TO 0 .1 FT !
AT START Al ;EN_JD
7 .50
INITIAL READINGS M ASURED AT GROUNDWATER AIR INTERFACE INDICATED BELO W
WATER FLOWHATE TEMP SSPJE TURBIDITY PH)ORP DISSOLVED
TIME LEVEL (CONCD) I OXYGEN(hh :MMS (deg C)(ntu) (unit (Mv) (mg/0
N/A N/A N/A N/A N/A N/A N/A N/A
WATER FLOWRATE TEMP -9PCU--7TuREIIUITY pH)ORP DISSOLVEDTIME LEVEL COND I OXYGE N(hh ~mm :ss)(ft)(ml/min)(deg C) (US/cm)(ntu) unit (mv)(Mg/1)
Oct-~j 1 -.45 5 .4S -7 5;STABILIZED DRAWDOWN A DREMOVED J . ~~k- EGAN LOGGING DATA
In,x5 T-tt 5"-2 1.4 SS5~ 4 ~k .3 (' i Ll 40 t , a -(
0 cl 3'~ ?6 553 If t I - C G 1 21 140 O,Co
0 11 ;-3 :2L 1 -0 0 55q q I ;k -;L cl
-5 tv r\ e 13 bg 0- If c.
ELECTRONIC FILENAME W L S CA P
COMMENTS :Go~~.D ?vl 0 14 WELL-14 4-0 1^
E REMOVED I A %
PRODUCT LEVEL,AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
UUM"F-Wvv"n I
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
ILOCATION : BURLINGTON, NC PROC NO : 1 3500 .1
1 PROJECT NAME : BURLINGTON MGP (OVERBURDEN WELLS)FIELDCREW :j LDC,RL
ISAMPLING DATE :20-Olt-0 3
MONITORING WELL NO . PMWM-S
WATER LEVEL METER SIN :N/A
PID READING L 2)ppm PRODUCT LEVEL METER S//N :ct-i -?-I
METHOD (Pump/ Bail)1PERISTALTIC PUMP TIME / INITIALS OF COLLECT LE :It 0'~0
WELL VOLUME CALCULATION :
WELL WELL DEPTH TO WATER 1CONVERSION]WELLCo
DIAM DEPTH (ft)WATER (ft)
)LUMN ft X
FACTOR
2-12 .68 X
X
gallons X 3 .785
SCREENINTERVA L
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
1 6 .18 Ift TYPE : DEPTH TO WATER :
STRONG :DEPTH TO PRODUCT :---(10
MINOR : PRODUCT THICKNESS : (ft)
ft .PUMP INTAKE NONE KNESS >OR =TO 0 .1 FT!
1 :1 . ~'
INITIAL READINGS MEASURED AT GROUNDWATER AIR INTERFACE INDICATED BELOW
WATER FLOWRATE TEMP SSPJEC SIDITY P Hit)ORP DlSgn-VffTIME LEVEL (COND I OXYGEN(hh :mm :ss)(it) (mVm1n) (de C)
u / )
(nt (mv) lmg/0
N N/A N/A N/A N/A N/A N/A N/A N/A
WATER FLOWHATE TEMP TURBIDITY PH DISSOLVEDTIME LEVEL COND OXYGE N(hh :mm :ss) (ft) (ml/min)(deg C) (US/CM)(nt (unit)(mg/0
to-'Co'.75 1 k I I (. x 1 1%0 STABILIZED DRAWDOWN A DREMOVED 'k-)!5 A_- EGANLOGGINGDAT A
! 0*-Oti - 3 k ki . 4r) (.ko k 'i -2.5 13cl .-i -5-YG q06 0.1
io,it 3j 11 . 01 IX0 I It .;Lt.A 3cl'-) q,)
1 .1 X f 2,0 19-31 1 3q,g;ita 0 -5 q
X 3,L(2-k t o lcl-33 t L4 0 .1 i-o4 5"Q 12-3 0, c q
t 1 --)8 1 k 0 1,;L iA-3 S-4')~Y-z s 0 .(.,7
0 3,5"4 A Lt .-)OL k1o %C1 .41 vA I - q ot - q 5-lit If 3o o
5Ajv, P Le-b c LO ;ZO103 0~j'0
'Aj e ~ 0 ~J UvO ~i"IVE V~-
5 -T c 4-1~- A Lc~e-!) -it
fv"-1~4
ELECTRONIC FILENAME-P(AvJJY\S,CA P
OMMENTS :tic,-%AC-C,&O'b e^h FTLLab PA,)ZtC-,~Vk~ LAi
I V-LjLJey~Eo fyA%r T-MrAk~j~To
!TOTAL VOLUME REMOVED =i ,L--iA I--
INOTE WATER LEVEL, PRODUCT LEVEL,AND WELL DEPTH ARE REFERENCED TOT TOP OF WELL CASING .
wwsx~ ff-www "I I ~wgvlv~ll I
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
LOCATION :-~~~BURL INGTON, NC PROC NO:3500 .1
PROJECT NAME : BURLINGTON RDEN ZWWELLS).,FIELD CREW :LDC,RLW
SAMPLING DATE :L-2
41MONITORING WELL NO .P-1S
c
WATER LEVEL METER S/N :N/A
PID READING
m
PRODUCT LEVEL METER S/N:11-7 -k
METHOD (Pump I Bail)PERISTAL IC PUMP TIME / INITIALS OF COLLECTI LE: ILA-01
WELL VOLUME CALCULATION :
WELL WELL DEPTH TO 0ILUMN ft X Vo lH WATER CONVERSION WELLNVERSION
PT To [EDDIAM DEPTH (ft)E[W!ATER fftt I FACTOR L 'al
2-11 .71 X c)
X
gallons X 3.785 ters
SCREENINTERVA L
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
11 .71 1 .71 ft .TYPE :DEPTH TO WATER :
STRONG :DEPTH TO PRODUCT:---#IV L).^4 %E
MINOR : PRODUCT THICKNESS :
INTAKE NONE,PUMP DON'T SAMPLE IF THICKNESS >OR =TO 0 1 FT
ATSTART .1 ATEN D
11 .21 ft
il,2_1
It .
INITIAL READINGS MEASURED AT GROUNDWATER AIR INTERFACE INDICATED BELOW
WATER FLOWRATE TEMP SPEC TURBIDITY pH ORP DI996=TIME LEVEL COND OXYGEN(hh :mff (ml/r (deg C) US/cm)(ntu) (unit)(mv) (mg/1 )
N/A N/A N/A N/A N/A N/A N/A N/A N/A
WATER FLOWHATE TE TUHBIDITY PH ORP DISSOLVEDTIME LEVEL COND OXYGE N(hh :mm :ss)(ft)(ml/min)(deg C) (us/cm)intu) (unit)(mv) (Mg/0
-SNI 0 2-1~2- STABILIZED DRAWDOWN AND REMOVED BEGAN LOGGING DAT A
16 k ?-oo pLt 1 q3 loxo -5 4 -!~L ;,
w 7 L,),-:-2 0 2 q,07 tokv Vk~~L
4 1~ -7 .L t';-,;)-oo ;Z4 . 4 5 k t c)t t;C>5-iL os~ ~~9 o I
0
ELECTRONIC FILENAME -C A
OMMENTS 1-A(-
T
TOTAL VOLUME REMOVE D
NOTE :WATER LEVEL, PRODUCT LEVEL, A~~DEPTH ARE REFERENCED TO THE TOP OF W aLL UA61NU .
~wlx" rwvv "I I ~~Ivlr~ll I
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
LOCATION : BURLINGTON, NC
i
PROC NO : I 350D
PROJECT NAME : BURLINGTON MGP (SHAL FRACT E FIELDCREWd LDC,
ISAMPLING DATE:90 04 9A I PI A-1705 ei? em E)a 23-Oct-03
MONITORING WELL NO.DMW-1
WATER LEVEL METER SfN: N/A
PID READING 0,M PRODUCT LEVEL METER S/N :
METHOD (Pump/ Bail)1PERISTALTIC PUMP TIME / INITIALS OF COLLECTED SAMPLE:~6 L)
WELL VOLUME CALCULATION :
tj Co~LUMN VOLWELL WELL TfO WATER .]CONVERSION WIELI-I a lVo~I ~
DIAM DEPTH (ft) COLUMN (ft)X FACTOR 'al
2-29 .02 X 0 .163 1
X I
N/A gallons X 3 .785 N/A 71,t:e7,Ts7]
SCREENINTERVA L
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
29 16 .72
ft .
TYPE :I DEPTH TO WATE R
STRONG~IDEPTH TO PRODUCT:---
-I PRODUCT THICKNESS :(ft)E DPumpINT8K:Ej NONE :Z IDON'T SAMPLE IF THICKNESS >OR =TO 0 .1 FT!
A
. 0 ft
AT START AT d
2 -%A ft
INITIAL READINGS M ASURED AT GROUNDWATER AIR INTERFACE INDICATED BELOW
WATE FLOWHATE TEMP SP TURBIDITY PH)ORP DIS§U=
TIME LEVEL COND OXYGENjell(hh (ft)(MI/Min) (deg C) (US/cm)(ntu) (unit (mv) (mg/1 )
N/A N/A N/A N/A N/A N/A N/A N/A
WAILK I-LUWRATF TEMP -MP1T7-7TUHBIUITY P H
TIME LEVEL COND I OXYGEN
(US/cm)(nt (unit)
V)DISSOLVED
(hh :mm :ss) (it) (mi/min)(deg C) (Mg/0
-?,. 3 3 3 8 & 1k 14 L(150 STABILIZED DRAWDOWN AND REMOVED (i EGAN LOGGING DATA
14,1 14 t~% G -,A I Ll -so ;2-0 .0 5 ~ )1-3'01 k I -~i -0 ~t,23-2 \k
o V'~ -vt x v 6 Li 3 -1-0 - o ->-C'S3
n K ..+i A ci
ELECTRONIC FILENAME - ~'j t
AdKCOMMENTS :
IIIIIIIIIIIIIIICI = U,
TOTAL VOLUME REMOVED 2,5
INOTE :WATER LEVEL, PRODUCT LEVEL,AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING,
uufxr- rwvvr-n %o%jovir#ki4 T
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
LOCATION, BURLINGTON, NC PROC NO :3500 .1
PROJECT NAME : BURLINGTON MGP (SHAL FRACT BR WELLS)FIELD CREW :LDC,RLW
ISAMPLING DATE : 3 21-Oct-03 I 9P.n,f .rlq 1 2-
MONITORING WELL NO . D=
WATER LEVEL METER SIN :N/A
PID READING ppml PRODUCT LEVEL METER SIN :
METHOD (Pump /Ball)Pump TIME / INITIALS OF COLLECTED SAMPLE :
WELL VOLUME CALCULATION :
L CoR It ILUMN ftWELL WELL kDEPTH TO r WATER-]CONVERSION WELL
DIAM DEPTH (ft)WATER ft COLUM (ft)X FACTOR VOL alI
2-32.08 X 0.1631
X
N/A gallons X 1 3 .785 1 N/A I 17tes
SCREENINTERVA L
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
32 .08 22 .08 Ift TYPE : DEPTH TO WATER :i
STRONG :DEPTH TO PRODUCT:--- ri C .v LE ft
MINOR : PRODUCT THICKNESS : ft
PUMP INTAKE NONE DON'T SAMPLE IF THICTNESS OR =TO 0 .1 FT l4t
AT START I AT EN D
2 X7,0
INITIAL READINGS MEASURED AT GROUNDWATER AIR INTERFACE INDICATED BELO W
WATER FLOWHATE TEMP SPEC TUR131DITY PH)OR PTIMELEVELCOND OXYGEN(hh :mm,ss)(ft)(ml/mi (uslcm)(ntu) unit (mv)(MgA)
N1 N/A N/A N/A N/A N/A N/A N/A N/A
WATER FLOWRATE TEMP -7§M I TURBIDITY (pH)ORP DISSOLVEDTIME LEVEL COND OXYGEN(hh :mm :ss)(ft)(mUmin)(deg C) (us/cm)(ntu) unit (mv)(mgA )
i S"!~3%00 ck,t o L-tOO STABILIZED DRAWDOWN AND REMOVED 1-4,0 EGAN LOGGING DATA
3~~ ~ 00 ct --3 ~-C-))-0,(.-2,447(.-?(~--P,1-7 6 ,?3
4Li *.1 0 1--)L34 0 ;2 0,-f LOS,1 1 3, 5? 4 .?o
9 -, 5 ~~1 . -? o 31-0 ;L o,3 Lt -7,y, o 8 .06 6 t 1(3 -o-oi
L 3'. -3 (1 e) Lf ?zf y
L (o
EELECTRONIC FILENAME -
d OMMENTS:C- 0 ID Ili vr,~6K-I=0--
ITOTAL VOLUME REMOVE D
INOTE :WATER LEVFL,HHUDUC; I LLVE-qL AN&WL-ECIL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
wulxr_rwvvQ n
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
ILOCATION :IBURLINGTON, NC PROC NO :3500 .1
L__PROJECT NAME~JBURLINGTONrGP SCH'~LFIACTBR WELLS)FIELDCREWd LDC,RLW
SAMPLING DATE : *0-~2s-oc-r-m-~_f)C
MONITORING WELL NO.PMWC-13R
WATER LEVEL METER SIN : N/A
PID READING (AA ~. J~J~l CTI-4 rj
m
PRODUCT LEVEL METER S/N :lclti-)-1
METHOD (Pump /Bail)I LIRS SUB PUMP~fl TIME I INITIALS OF COLLECTED SAMPLE :
WELL VOLUME CALCULATION :
WELL WELL DE TO WATER CONVERSIO WELLCo
DIAM DEPTH (ft)WATER (ft)
)LUMN ft X
FACTOR -VOL (gal)
2'36.00 3 X 3 . 3 1
- - A -X I
NIA clallons X 3 .785 /A liters-i
SCREENINTERVAL ]
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
3 27 .0 TYPE :UA t-TA&DEPTH TO WATER :I
STRONG,DEPTH TO PRODUCT :---I "jz'^41E (ft)
MINOR :PRODUCT THICKNESS :
PUMP INTAKE NONE IDON'T SAMPLE IF THICKNESS >OR =TO 0 .1 FT!
AT START AT
3 1 ~
INITIAL READINGS MEASURED AT GROUNDWATER AIR INTERFACE INDICATED BELO W
I W R TLMP SPEC TURBIDITY PH ORP DISSOLVEWTIME
L I FLOWHATE I
COND OXYGEN(hh :mm'ss)(ft)(ml/mi (us/cm)(ntu) (unit)(mv) (mg/1 )
N N/A NIA N/A N/A N/A N/A N/A
WATER FLOWHATE TEMP SPEC TURBIDITY PH ORP DISSOLVEDTIME LEVEL COND OXYGEN(hh :mm :ss)(ft) (ml/min)(dog C) (us/cm)(ntu) (unit)(mv) (mg/1)w.k a_'3 71,1 (1 . %~)'a .2-0 STABILIZED DRAWDOWN AND REMOVED L4 .0 BEGAN LOGGING DATA
0 " I %~ " 1 3 ~ ~. 0 ;_~_ jc~~O 18 ~ 8EJ ff A - -)'-I .VO (.V -) I I ;?, 1 1 0,03
O~. lcl'~53 i 51 q k %00 1 V"6 9 qVg~L -5,19 L . LC?119 0-01
10 _Is . 2. %k CA oo %,A - G ~qf t q
10,3o'. LJLJ (L 9 -xv 8 3 . c ~1 - J-~,o 3 A".3
3 cA
ELECTRONIC FILENAME -f4v\wc'Blz
OMMENTS : C-0 0 J~t'A4)P,
c
TOTAL VOLUME REMOVED 01 -C-4~v L~
INOTE :WATER LEVEL, PRODUCT LEVEL,AND WELL DEPTH ARE REFERENCED TO) THE TOPj0F WELL CASING .
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
P Oj ~L2CLI~TCION- 'BURLINGTON, NC PROC NO : 3500 .1
R I NAME : IBURLINGTON MGP (SHAL FjAgT BR WELLS~FIELDCREW :j LDC,AL
SAMPLING DATE : IQ-QU-03 24 44,142 22-Oct-03
MONITORING WELL NO .PMWH-BR
WATER LEVEL METER SIN:NIA
PID READING PRODUCT LEVEL METER S/N :
METHOD (Pump I Ball)~Pml TIME /INITIALS OF COLLECTED SAMPLE:
IWELL VOLUME CALCULATION:
COWELL WELL DEPTH TO WATER CONVERSION WELL
DIAM DEPTH (ft)WATER (ft))LUMN ft X FACTOR
VOL "I
2-20.72 X 0 .1631 021
X
N/A gallons X 3 .785 N/A lites
SCREENINTERVA L
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
20 19 .72 Ift TYPE :IDEPTH TO WATER :i
STRONG :EPTH TO PRODUCT:... ~j L,~~
MINOR :Z---EPRODUCT THICKNESS :
Pump INTAKE NONE IDON'T SAMPLE IF THICKNESS >OR =TO 0 .1 FT I
AT START AT EN D
2 2,0,0 j
INITIAL READINGS MEASURED AT GROUNDWATER AIR INTERFACE INDICATED BELO W
WATER FLOWHATE TEMP SPEC TURBIDITY p DISSOLVEDTIMELEVELCOND OXYGEN(hh :mr (ml/mi (US/cm)(ntu)(u (mg/1 )
N N/A N/A N/A N/A N/A N/A N/A N/A
WATER FLOWHATE TEMP TURBIDITY PH)DISSOLVE D-777 =TIME LEVEL C NO OXYGEN(hh :mm :ss)(ft)(ml/min)(deg C)(USICM)(,tu) unit (mgA)
ks .. I ok . ~-j V ~b-~?-cl 0 STABILIZED DRAWDOWN A D REMOVED 2-6 al I 'EGAN LOGGING DAT A
13 0 wci 300 ('6 -cl 6 416 7 .10 Ji k - 73 ("2-(,0,03
51',,3 ~rct -300 (ig, q,4 1?6s, 14 to-0 .0 6
5- S " ->, \,~6-8~A -12- ~ D k~.CA 0 q L 0 .0 5ow,3 S .le~L )L 6 0 k V,9 3 44 1,3 o cl 5
A 0(7;,Ac L 1 0
ELECTRONIC FILENAME -IP [3 P
,go
I
h~OMMENTS:'S 7 t Z~177~c~
OT
E
OTAL
VOLUME
RE OVED v-,A 1,
N _ E~WATER LEVEML, PRODUCT LEVEL .AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
LOCATION : BURLINGTON, NC PROC NO : 3500.1
I kL FRACT BR WELLS)FIELD CREW:LDC,RLW
SAMPLING DATE :.20-Oct-03 I _24-90t-g&--~
MONITORING WELL NO .PMWI-13R
WATER LEVEL METER SfN : N/A
PID READING PRODUCT LEVEL METER S/N :kc~ so - I
METHOD (Pump I Ball)~Pml TIME / INITIALS OF COLLECTED SAMPLE :
WELL VOLUME CALCULATION :
WELL WELL DEPTH TO WATER CONVERSI WELLCo
DIAM DEPTH (ft)WATER (ft)
ILUMN It
X VOL al
2-38 .07 X
X
NIA gallo,s X 3 .785 N/A lite ~rs
SCREENINTERVA L
FROM TO DETECTED ODORS -FREE PRODUCT MEASUREMENT
38.07 28.07 ift TYPE : DEPTH TO WATER :
STRONG :DEPTH TO PRODUCT:
PUMP INTAKE
MINOR, PRODUCT THICKNESS : (ft)
AT START I AT END
ftj NONE ICKNESS >OR =TO 0 .1 FT
33 .0 ft .1 33 .0
INITIAL READINGS MEASURED AT GROUNDWATER AIR INTERFACE INDICATED BELO W
WATER FLOWRATF TEMP SPEC TURBIDITY pH)ORP DIS96=TIME COND OXYGEN(hh IMMISS) I M)(mumi (us/cm)(ntu) (unit (mv) (mg/1 )
N/A N/A N/A N/A N/A NIA N/A N/A N/A
WATER FLOWHATE TEMP SPEC TURBIDITY PH)DC) (uSjCOND DISSOLVETIME LEVEL OXYGEN(hh :mm :ss) 00 (ml/min)(cl / I (ntu) (unit
(mv)
(mg/1 )
L'3 -L,;L',t3 k k 13 Li Ll L~STABILIZED DRAWDOWN AND REMOVED 4f,EGAN LOGGING DATA
0 ~k '. 9-5? \ N k S -A 4 0 k c~ --i /. -~7,5-c . f-2 .;).5 t:ki 9(~
3'.to,.-5 9 j%.xl 430 ket-4w a-55-( ,i R (.
13', 0-2-3 Iq 4 1 C\ -\-L 3t sssio ;Z .-3L /.-c 0
e-A^P(Ch 3 a-0 c-
ELECTRONIC FILENAME - kAIS-940-- r- A
lo=m TS
:
TOTAL VOLUME REMOVED =
NOTE,WATER LEVEL, PRODUCT LEVE ,D WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
Liu r%r-f-%j vv v_n %1%Jlv1rMI4 T
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
LOCATION : IBURLINGTON . NC PROC NO :3500.1
PROJECT NA IE : BURLINGTON MGP (SHAL FRACT EIR WELLS)FIELDCREWd LDC,RLW
SAMPLING Dj 2QnctQ;I -240,IQ-3 22-Oct-0 3
MONITORING WELL NO .PMWL-BR
WATER LEVEL METER SfN :N/A
PID READING PRODUCT LEVEL METER S/N :~k -1 - k
METHOD (Pump /Bail)[PERISTALTIC Pump TIME / INITIALS OF COLLECT,LE:o t~
WELL VOLUME CALCULATION :
WELL CONVERSMWELL DEPTH TO WATER WELLCo)LUMN ft X VOL
DIAM DEPTH (ft)WATER (ft)LCOLUMN (ft)I I "IFACTOR VOL (gal)
2- 24 .46 X 0.163 1FalqX
N/A gallons X 3 .785 N/A liters
SCREENINTERVA L
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
24 .0 14 .0 ft .TYPE :DEPTH TO WATER :
STRONG :DEPTH TO PRODUCT :--- NJG NIF (ft)MINOR : PRODUCT THICKNESS : = (ft)Pump INTAKE NONE : DON'T SAMPLE IFTHICKNESS >OR =TO 0 .1 FT!
ATSTART ATEN D
2
Xo~
0
c- k~.a c-L)
INITIAL READINGS MEASURED AT GROUNDWATER AIR INTERFACE INDICATED BELO W
T =LR FLOWRATE TEMP SPEC TURBIDITY pH oRP DISSOLVEU[ME COND OXYGEN(hh :mm~ss) (ft) (mvmi (US/cm)(ntu) (unit)(mv)(mgA )
N/A N/A N/A N/A N/A NIA N/A N/A N/A
WATER FLOWRIATE TEMP SPE C TURBIDITY pH ORP DISSOLVEDTIME LEVEL COND OXYGE N(hh :mm :ss)(ft)(milmin)(dec
C) I, / I
(ntu) (unit)(mv) (mg/1)
tocr- 34,;LO 03441~~ STABILIZED DRAWDOWN A D REMOVED EGANLOGGINGDATA
3 V cl -~(ct 3J-3--t 2-1 61 0 .50L
L)CI 4 5'. 5 o 1-5-0 to(. s 3 .;L5~4 ki .~j
OCI 0 o .9 0 15-4 tc~R 6-7 6 x ck 0 .
oct "54 :;,-1 -7-cl q /54 tcl .~9 31-9-0 10-9 4 A5-x .?
to 4-o I '.51 v- ISL k4t cl 3 .7-s-,.2 t-?-0 a-!;-
N~~ k 60 LD L ko Ix .;t-
ELECTRONIC FILENAME - 9 in w Lpa -cA P
d OMMENTS:c- o a 0 P .10 jf=~!~-MC-ir 0- '~c -
cy C,A^i P L ti C %D~r d'D 0
VIED .0 c 4^f~RODUCT LEVEL,AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
I www"11 I
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLIN G
LOCATION :IBURLINGTON, NC PROC NO :
Fli~~PROJECT NAME : BURLINGTON,MGP (SHAL FRACT BA WELLS) FIELDCREW:j LDC .RLW
SAMPLING DATE :20~0,t-03
MONITORING WELL NO .r-~MWM-B-A
WATER LEVEL METER SIN :N/A
PID READING PRODUCT LEVEL METER S/N :'(rl
- IMETHOD (Pump /Bail)1PERISTALTIC PUMP TIME / INITIALS OF COLLECTED SAMPLE :t o
WELL VOLUME CALCULATION :
WELL WELL DEPTH TO CONVERSION WELLVolDIAM DEPTH (ft)WATER (ft)X FACTOR
L "I
2-19 .16 X 0.1631 1 .1 8
X
N/A qallons X 3 .785 N/A liters
SCREENINTERVA L
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
19 15 .66 tit TYPE : DEPTH TO WATER :
STRONG :DEPTH TO PRODUCT :
MINOR : PRODUCT THICKNESS :
PUMP INTAKE NONE : DON'T SAMPLE IF THIC~NESS OR =TO 0. 1 Fr iATSTART,ATEN D
1
l'i ,
tit
INITIAL READINGS MEASURED AT GROUNDWATER /AIR INTERFACE INDICATED BELO W
WATER FLOWRATE TEMP SPEC TURBIDITY pH-- DISSOLVEDTIME LEVEL OXYGEN(hh :mr (ft)(mVmin)(d (ntu) (unit)(mv)(m9A )
N/A N/A N/A N/A N/A N/A N/A _j N/A N/A
WATER FLOWHATE TEMP SPEC TURBIDITY PH)URP DISSOLVEDTIME LEVEL COND OXYGE N(hh ~mmss)(ft)(Mvmin)(d .g C) (us/cm)(ntu) (unit
(mv)
(mqA)
0 cl q I . Ii -) I ') (,ISTABILIZED DRAWDOWN AND REMOVED BEGAN LOGGING DATA
56'12 .1,1 1 ct o ( & ~ S .2,x 4 '1 -.2,1 1-1.(- 1 111 1 0--ic I
03 : 5L VI-14 ci 0 $?- %I cl 2-(X-g a ..x 4 % o 1 0 .
ook",34 015 115 to 0-1 1
'~AAO L %~O I kQ ;LO 0 %1
ELECTRONIC FILENAME - P (hyj Jv-j A (Z.
-OMME.NTS .,No 'ktAc'1)tArA
I
TOTALVOLUM REMOVED =
NOTE : WATER 'EVEL,PRODUCT LEVEL,AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
jb,~e 3 -0 c7-,,)6 ~~zCHAINOFCUSTODY REOU D AND ANALYSIS REQUEST FORM--------- , 1111 P 11 1,1,1,1 fl~ 711 :boratory ervices I MWAM11111,11111115 1 :11106N ~:I,Pk Duke i a VAR,OW
I Mail Code G03A2 (Building 7405) "'Page-L of -A-Energy'..,1333M9 Hagers .Ferry Rd ! , DISTRIBUTION
For Detailed Instructions, see : Huntersville,N C. 28078 ORIGINAL to LAB,I
http :/Ydewww/essenv/coc/ (704) 875~5245 COPY to CLIENT............-------------Fqx :.(704)§L!~q:L
1)Project Name 2)Phone No :675-5257 1 d
BURLINGTON MGP (OVERBURDEN WELLS)
E 3)CIlent C .Campbell R . Roberts i~F..N . 875-5-032 lp",
2=H 3=H
4=1 a 'a M5)BusinessUnit: 20018 6)Process : F)R ..p T.0-193 M
E C0 om c~18)Projectll): MGPBURL 10)Mail Code :MG03A3 09)ActMtylD :ALLACTV
complete all 75y 2 0 0w2proorlate Now <.... ... ... .......I I 14CO,0 0LASUSEONLY 12Chem lection Information a M 0E <
< <- - -FT p 0 w Q- 0-"Lab to Desktop No . "Sample Description or ID Data ,e7 Signature z 2 W-1 w I
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- - - - - I 1
1 3MINx 1 1 3 1foh~oq 5 5
!,I :; x 1 1 3 1PMWB-S 1 0 15--2-0 6
P-1S t o a il ;1D x 1 1 3 1 6t- - - - - - -PMWC-S 10 x 1 1 3 1 6
MW-50.lo olo-1,1430 6x 1 1 3 1WAfti20 Mw-9 10 x 1 1 3 1 6
H ;tLt-3 vAt!;
PMWM-S x 1 1 3 1/z4a-t %O'Ao J-4 6
PMWL-S x 1 1 -u-103 Og J!~3 1 6104,0 ,0
FIELD BLAN K0 10 A3103 (O ;L x 1 1 3 1 n/a 6
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-Cu-stometo sion &date below2 ip .inquished B Daterri .e Aift
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*7 Days23)SeaULOcKea by DaterTi .e seal
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' Add .Cost Will Apply
aPhOub MiKeFowerAnaiyucat LaDoratory,power.Phone 70$-875-5245 Fox. 704-875-5038
A A.6 ~V G~1333.9HOgefsFetrl Road HunterevilllaNC28078-792a
MCGufte NuMar ComplaX - MG03A2
cortificat4.- ciir Amnalysi s
Now York Stoic Dopormoint ofHoofth Conficolion ff f f7f7
Oklahoma Department of Environmental Oua Cartificalmon # 9930
Kansas Department of Heath and EnvininmenvIcarlificale # E-fO3f f
North Carolina Department of Health &Human Services Certification # 37804
South Carolina (DHEQ Laboratory ID # 99005 North Carolina QBVI~ Certification #248
Station Name:BURLINGTON Job Number 03-OCT-0052
I
Sample ID #: 23038616 Desktop S Customer ID :R .ROBERTS
Sample Description: MW-3 (OVERBURDEN WELLS )
Collection Date: 23-Oct-03 09 :55 :00 Date Receivied in Laboratory. 02-Oct-03 TypeolSample :MGPSITE
Refereru ;e Method EPA310 .11SM232013 Data Posted :10/28/2003 15 :20:46
-ALKALINITY (TOTAL INFLECTION POINTI ALKALINITY 0 .74 meg/L
Reference Method :EPA 200 .716010B Data Posted :11/5/200308 :20:4 5
IRON BY ICP (DIGESTED)IRON 0 .542 mgll
Reference Method :EPA 200 .71601011 Data Posted 111512003 08 20A6
MANGANESE BY ICP (DIGESTED)MANGANESE 0 .031 mg/L.
Referenm Method :EPA 300~O Data Posted : 10/2412003 16:17 :53
MG-NIL 6Y CALCULATION NITRA TE 0.63 mg-NIL.
Reference Method :EPA 300 .0 Data Posted : 10124/2003 14 :40 :03
NITRATE JIC)NrTRA TE 2.81 mg/L.
Reference Method :EPA 300 .0 Data Posted 1012412003 14 :40 03
SULFATE (IC)SULFATE 12 .07 mgfL
Sample ID #: 23038617 Desktop #Customer 10:R .ROBERTS
Sample Description: PMWB-S (OVERBURDEN WELLS )
Collection Date : 21-Oct-03 15:20 :00 Date Received in Laboratory'. 02-Oct-03 Type of Sample :MGP SITE
Reference Method :EPA310 .1/SM23208 Data Posted 10128/2003 15 :20 :46
ALKALINITY (TOTAL INFLECTION POINT)ALK4L1NfTY 7.00 mog/L
Reference Method :EPA 200 .7160108 Data Posted : 11/5/200308 :20 :48
IRON BY lCP (DIGESTED)IRON 29 .513 mo
Reference Method :EPA 200.7/6010B OataPosted : 111612003DB :20 :46
MANGANESE BY ICP (DIGESTED)MANGANESE 0.196 mg[L
Reference Method :EPA 300~O Data Posted: 1012412D03 16:24 :0 2
MG-11111 . BY CALCULATION NITRA TE <0.02 mg-WL
Reference Method :EPA 300 .0 Data Posted : 1012AU2003 13:03 :1 1
MTRATE JIC)NITRATE < 0.10 mg/L
Reference Method:EPA 300 .0 Data Posted : 10/2412003 13 :03 :1 1
SULFATE SULFATE 1 .66 mglL
Visit us on the ln~Net to
Report Genewtud 111512003 14:13:17 http :1/de~/essemAab-srv/Ag, -.1
0pbDk*e ime Fower Anaiyuicai LaDormory
Y POW.Phone :[phone] Fax.[phone]
13339Ha9erSFefIYR0ad HunfetsvilleNC28078-7929
AfcGufre NUC(ear Complex - MG03A 2
caartlrlc~ata- cill J%nalysle-
Now York statc Doporfmant of Hoolth Corfificalion ft ff7f7Oklahoma DepartmentofErwronmentelQuall Cerhfcahon#9930
Kansas Deparlment of Heagh and EnvirunmenMart&a1a # E- f031 1
NoHh carolkia Department of fileafth &Human Seivices Ceffification P 37804
South Carolina (DI-EQ Laboratory ID # 99005 Nodh Carolina Q8VR Ceffificalion #248
Station Name :BURLINGTON Job Number 03-OCT-0052
Sample ID #: 23038618 Desktop #Customer ID :R .ROBERTS
Sample Description :P-IS (OVERBURDEN WELLS )
CollectionDate: 21-Oct-0316:20 :00 Date Received in Laboratory. 02-Oct-03 TypeofSample :IMGPSITE
ReferenoeMethod :EPA310 .11SM23208 Data Posted: IW=003 15 :20:46
ALKALINITY (TOTAL INFLECTION POINT)ALKAUVITY 7 .94 ineqn.
ReferenceMethod EPA2DO .716010B OstaPosted :11/5/200308 :20:4 7
IRON BY ICP (DIGESTED)IRON 2.792 mgR
Reference Method :EPA 200.7t60108 Data Posted :1115/200308:20 :47
MANGANESE BY ICP (DIGESTED)MANGANESE 2 .277 mall-
Reference Method :EPA 3DO .0 Data Posted : 10/2412003 16 24 03
MG-N/L BY CALCULATION NfTRATE <0 .02 mg-NIL
Reference Method :EPA 300 .0 Data Posted: 10/24/2D03 13 05 3 7
NITRATE (IC)NrTRATE 0 .10 m9fl-
Reference Method :EPA 3000 Data Posted : 1012412W3 13 05 3 7
SULFATE (IC)SULFATE 35 .35 ma/L
-----------
Sample ID C 23038619 Desktop #CuslornerID : R .ROBERTS
Sample Description: PMWC-S (OVERBURDEN WELLS )
ColleLftionDalte: 21-Oct-0309 :25:00 Date Received in Laboratory. 02-Oct-03 TypeofSample :IMGPSITE
Reference Method :EPA310 .11SM232013 Date Posted : 10/2ar2W3 15 :20 :46
ALKAL[NrrY (TOTAL INFLECTION POINT)ALKALHVfry 3 .92 m&qA.
Reference Method : EPA 200.71601013 Data Posted: 1115/2003Da :20 :47
IRON BY ICIP (DIGESTED)IRON 24.fiS6 ing/l
Reference Method:EPA 2001/6010B Data Posted,1115/2003 08:20 :4 8
MANGANESE BY ICP (DIGESTED)MANGANESE 2 .698 inall-
Reference Method :EPA 300.0 Dale Posted : 10124/2OD3 16 :24 :04
MG-ML BY CALCULATION NfTRATE <0 .02 ma-N/L
Reference Method :EPA 300.0 Data Posted : 10124/2003 13 :06:1 0
NITRATE [IC NfTRA TE <0.10 muIL
Reference Method :EPA 3DO .0 Data Posted 10124/2DO3 13 06 :1 0
SULFATE (IC)SULFATE 0 .85 mail.
R,p,nGenen,md 11151200314 :13:37 http:I/dcwww/cssenvIlab-~/
PhOuke DuKeFowerAnaiyucai LaDoraiof y
arpower.Phone: [phone] Fax,704-875-5038
13339 HagersFerty Road Hunteraville,NC28078-7929
McGuire Nucfear Complex -MG03A 2
Cortificat4e cot Antnaly!sI s
Now York Sloto Doportmont of HoolfhCortification #ff7f7
Oklahoma D9partment nfErwironmental Qua# Certification #9930
Kansas Department of Heath and EnvironmenMailificale # E-fO3f I
North Carolina Department of Health &Hunitir? Services Certification # 378 N
South Carolina (DHEQ Laboratory ID If 99005 North Cgtolina (DENR Certification #248
Station Name :BURLINGTON Job Number:03-OCT-0052
Sample ID # 23038620 Desktop #Customer ID:R .ROBERTS
Sample Description :MW-5 (OVERBURDEN WELLS )
Coltedon Date : 20-Get-03 16 :30:00 Date Recehed in Laboratory : 02-Oct-03 TypeofSample :MGPSITE
Reference Method :EPA310 .11SM2320B Data Posted : 1012812003 15 :20 :47
ALKALINITY (TOTAL INFLECTION POtNTj ALKALINITY 9.27 meg/L
Reference Method :EPA 200 .7/60108 Date Posted :111512003 08 :20 :48
IRON BY 1CP (DIGESTED)IRON 4 .619 mg/1
Reference Method :EPA 200 .716010B DataPosted 1115/200308 :20 :48
MANGANESE BY ICP (DIGESTED)MANGANESE 0.698 mall.
Reference Method:EPA 3DO .0 Data Posted 1012412003 08 :59:58
MG-NIL BY CALCULATION NITRA TE <0 .02 mg-NIL
Reference Method:EPA 300o Data Posted,10123/2003 11 :46 :08
NITRATE (IC)NITRATE < 0.10 mg/L.
Reference Method :EPA 3DO.0 Data Posted :10/23/2003 11 :46 :DS
SULFATE (IC)SULFA TE 24.81 mg/L.
-------- -----
Sample ID #: 23038621 Desktop S Customer ID:R .ROBERTS
Sample Description : MW-9 (OVERBURDEN WELLS)
CollectionDalle: 22-Oct-0314 :15 :00 Date Received in Laboratory : 02-Oct-03 Type of Sample : MGP SITE
---------- -
Reference Method :EPA310-1/SM2320B Data Posted :10/28/2003 15 :20 :47
ALKALINITY (TOTAL INFLECTION POINT)ALKALINITY 5.69 mgqlL
Reference Method :EPA 200.7160108 Data Posted:111512003 08 :20 :49
IRON 13Y ICP (DIGESTED)IRON 0 .335 mg/l
ReferenceMethod :EPA 200.7/6010B Date Posted :1115/2003 08 :20:49
MANGANESE BY ICP (DIGESTED)MANGANESE 0.079 mgIl.
Reference Method:EPA 300.0 Data Posted : 10124r2M 16:17 :54
MG-NIL BY CALCULATION NITRATE 0.67 mg .N/L
Reference Method :EPA 300 .0 Data Posted : 10/2412003 14 :40 :37
NITRATE 11C)NITRATE 2.99 mgfL
Reference Method :EPA 300 .0 Data Posted : 1012412003 14 :40 :37
SULFATE (I SULFATE 49 .71 mgfL
Visit us on dw,1 .U.Nd 9
ReporlGenewled 111512003 14 .13:37 htp://dc~/csscuvAab-srv/P(~qe 43 o.1 5
*Duke Duke Power Analytical Laboratory
POW.Phone:70$-875-5245 Fax.7&$-875,5038
AD,&~uC~13339 HagersFeriy Road HunlefevilkNC28078-7929
AfcGulle Numar Complex - MG03A 2
Cartificatom- of^maiysus
Now York Slato Do"rimni of Hoalth Gortification If f f7f7
OklahornaDaparlrnentofErvitonrmntalQuah Cartficabon#9930
Kansas Department of Health and EnvironmenMailificale # E-103f f
North Carolina Department of f-bafth &Human Services Gellification # 378N
South Carolina QfIEQ Laboratory ID It 99005 North Carolina (DOOO Certification #248
Station Name :BURLINGTON Job Number 03-OCT-0052
Sample ID 23038622 Desktop #Customer ID :R .RCEIERTS
Sample Description : PMWM-S (OVERBURDEN WELLS )
Collection Date: 20-Oct-03 10:40 :00 Date Recehied in Laboratory 02-Oct-03 Type of Sample :MGP SITE
Reference Method :EPA310.11SM23208 Data Posted 10/2812003 15:20 :4 7
-ALKALINITY JTGTAL INFLECTION POINTI ALKALINrFY 0.39 meqlL.
Reference Method :EPA 200 .7/6010B Data Posted:111512OD3 08 :20 :49
-[RON BY ICP IDIGESTEDI IRON 0 .536 mgn
Reference Method :EPA 200.7/6010B Data Posted:11/5/2003 08:20 :50
-MANGANESE BY ICP (DIGESTED)MANGANESE 0 .097 mg/L
Reference Method :EPA 300o Data Posted: 10r24/2D03 08 :59 :59
MG-NIL BY CALCULATION NITRA TE 0.98 mg-NfL.
Reference Method :EPA 300 .0 Data Posted :1012312003 11 :47 :22
NITRATE 11C)NITRA TE 4.36 mg/L
Reference Method :EPA 300 .0 Data Posted : 101231200 11 :47:22
SULFATE (IC)SULFATE 15.93 ma
Sample ID 8 : 23038623 Desktop #Customer ID:R .ROBERTS
Sample Description : PMWL-S (OVERBURDEN WELLS)
Collection Date : 22-Oct-03 09:25 :00 Date ReceNed in Laboratory: 02-Oct-03 TypeolSample : MGPSrTE
-------------
Reference Method :EPA310.1/SM2320B Data Posted : ID/2811200315 :20:4 7
ALKALINITY (TOTAL INFLECTION POINT)ALKALINITY 4 .39 mag/L
Reference Method :EPA 2DO .716010B Data Posted :11/512DO3 08 :20:50
IRON BY ICP (DIGESTED)IRON 35.837 mg/I
Reference Method :EPA 200 .7/SD10B Data Posted 11/512003 08 :20:50
MANGANESE BY ICIP (DIGESTED)MANGANESE 1 .993 mg/L.
Reference Method :EPA 300 .0 Data Posted : 1012412003 16 :17 :5 5
MG-NIL BY CALCULATION NITRATE <0.02 mg-HIL.
Reference Method :EPA 300 .0 Data Posted ; 1012412003 14 :41 :DB
NITRATE (IC)NITRA TE <0.10 mglL.
Reference Method :EPA 300 .0 Data Posted 1012412003 14:41 :08
SULFATE (IC)SULFATE 24.37 mg/L
Vi.t " on th~btraNet V
ReportGeneraied 111512003 14 :13:37 http ://dcw~IessenvAab stv/P,~44"15
*Duke Duke Power Analytical Lawrator y
Power. Phone:70$-875-5245 Fax [phone]
13339Ha9erGFerfyR0sd Hunteraville,NC28078-7929
mcGuffe Nuclear Complex - MG03A 2
c4-=rtmcato-- cot Amnaiysius
Now York Sloto 0cloortmntof Hoolth Corf&ohon # ff7f7
OkOhoymoapartnvntofErwitonrmnlalOuab Cartfication#9930
Kansas Department OfHeafh and EnvironmenMerfArate #E-1031 1
North Carolina D9parfroent of t-k-afth &Human Services Certification # 378N
South CaroMa (DHEQ Laboratory ID # M5 North Qrolkta QOVF~Certification #248
Station Name :BURLINGTON Job Number :03-OCT-0052
Sample 10 S : 23038624 Desktop #Customer ID :R .ROBERTS
Sample Description :FIELD BLANK JOVERBURDEN WELLS )
Collection Date : 23-Oct-03 10 :25:00 Date Recaried in Laboratory : 02-Oct-03 TypeolSample :MGPSITE
ReferwwMalhod :EPA310.1/SM123200 Data Posted:10/28/2D03 15 :20.4 7
ALKALINITY (TOTAL INFLECTION POINT)ALKALHVtTY < 0.01 meq/L
Reference Method :EPA 200 .7/601 OB Data Posted:11151200308 :20:5 1
IRON 13Y ICP (DIGESTED)IRON 0.019 mg/1
Referenm Method :EPA 200 .716010B Data Posted:11151200308 :20:51
MANGANESE BY ICP (DIGESTED)MANGANESE < 0.005 mg/L
Referen" Method :EPA 3DO .0 Data Posted : 10124=03 16 :17:56
MG-NIL BY CALCULATION NfTRA TE <0 .02 mg-NfL
Referen" Method EPA 300 .0 Data Posted 10/2412003 14:41 :27
NITRATE (IC)NrFRATE 0.10 mg/L__
Referwm Method :EPA 300 .0 Data Posted : 10124/2003 14 :41 :27
SULFATE (IC)SULFATE < 0.10 mg/L
D-h0fied
and Appmved By,Date
0
Visit as oe the fritzisNet 9
ReportGenerated 111512003 14 :13:37 http :flde~/~vfilab-srv/
November 4,2003 1 :57:52 PM Page #1 of I
Duke 8270/625 Analysis
Energy.Case Narrativ e
(This domment must a=mpany releatse ofAnalytical Data)
- - - - ----------- - -- - -----------------
LIMS Job #03-OCT-0052
WorkUst #03-OCT-064 2
The percent recovery for the surrogates were outside of the laboratory control limit in
samples 23038619 and 23038622.The results for all analytes should be considered
estimates for these samples .
--------------
ignature
Shannon Rollins
--------------------------------------------------------------------------------------
Duke Energy .Analytical Laboratory Service s
Environment, Health &Safety Services Environmental Center - MG03A2
Phone :[phone] Hagers Ferry Road
FAX :[phone] HuntersvilleNC 28078-7929
SACase Nwativ~\Organic\SVOA\oct-0052 .doc
P&Duke DUKeFowerAnaiytical Lai3orator ytvftwerPhone. 704-875~5245 Fax : [phone]
A~&Vce"7 13339HagefsFefly Road HunterSyl/119,NC28076-7929
MCGUife Nuclear CoMpleX - MG03A 2cartiricace af Anaiysis
New York State Department of Health Certification # f 1717Oklahoma Deparrnent of Enwronmeintal Quality Certification #9930Kansas Department of Health and Environment Certificate # E-f03f j
North Cortifine Department of Health &Human Services Ceifificabon #37804
South Carolina (DHEK)Laboratory ID #99W5 North Carolina (DENF~ Certification #248
SamplelD#:23038615 Job #: 03-OCT-0052
Sample Description :TRIP BLANK (OVERBURDEN WELLS )
Collection Date: 18-Oct-03 16:35:00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
OGIP PARAMETERS IN WATER BY GC/MS - 826 0
Test Code : MS8260MGPW Test Method : SW-846 503013/82608 Date Posted :11/03/03
Result Ra~ Limit Rag
Benzene e 0 .50 pg/L 0.50 pg(L 0
Toluene < 1 .0 Pg/1- 1 .0 pg/L 0
Ethylbomene < 1 .0 pg/L 1 .0 pgfL 0
rn~p-Xylone <2.0 pgVL 2 .0 pelt,0
o-Xylene e 1 .0 pg1L 1.0 Pg/L 0
Naphthalene 2 .0 pgfL 2 .0 plill . 0
SamplelD#:23038616 Job#:03-OCT-0052
Sample Description:MW-3 (OVERBURDEN WELLS )
ollection Date : 23-Oct-03 09 :65:00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
IMGP PARAMETERS IN WATER BY GC/MS - 826 0
Test Code: MS8260MGPW Test method : SW-846 5030B/8260B Date Posted :11/03/03
Result Reporting Lknit Flag
Benzene < 0 .60 pg1L 0.50 pg(L 0
Toluene < 1 .0 pg/L 1 .0 Pg/L 0
Ethylbenzene e 1 .0 lig/L 1 .0 PGVL 0
~p-xylene <2.0 pgfL 2 .0 pg(L 0
o-XyIene < 1 .0 pgVL 1 .0 Pg/L 0
Naphthalene <2 .0 pgtL 2.0 pg/L 0
PVOC MGP IN WATER BY GC/MS - 827 0
Test Code: MS8270MGPW Test Method : SW-846 8270C Date Posted :11/04/03
Result Reporting Lknit Flaq
Naphthalene < 10 Vg(L 10 PgVL 0
2-Mothyinaphlhalene 10 plill. 13 pg/L 0
Acenaphthylene < 10 pgfL 10 Pg/L 0
Acenaphthene < 10 pgfL 10 Pg/L 0
Dibemofuren < 10 pg/L 10 pg&0
Fluorene < 10 Vg/L 10 Pg/L 0
Phenanthrene 10 pg/L 10 pg/L 0
Anthracene < 10 pg/L 10 pgIL 0
0 Fluoranthene < 10 pg/L 10 Vg/L 0
Visit us on the IntraNet a tR,,n G,,~,rutd It 1512"14:01 .'42 http ://dew~/essenvAab-srw/P-g~ # I of 10
PkDuke VuKe Flower Analytical LaDoratoyyaPower.Phone [phone] Fox.764-875-5038
A Ah &~ C~ 13339 Hag ers Ferry Road Huntersville,NC28078-7929
McGuire Nuclear Comptax - MG03A 2C4ertific:at4e arAnaiysis
New York State Department of Health Certification # 11717
Oklahorm0aparin)entofEnvironrnenlalQuebtyCertfficalon #9930Kansas Department of Health and Environment 09dificale # E-f03ffNorth Carolina Department of Health &Human Services Certification # 37804
South Carolina (DHEC)Laboratory ID # 99005 North Carolina (DENF~Certification #248
SamplelD#:23038616 Job#:03-OCT-005 2
Sample Description :MW-3 (OVERBURDEN WELLS )
Collection Date : 23-Oct-M 09 :55:00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
~VOC MGP IN WATER BY GC/MS - 8270
Test Code : MS8270MGPW Test Method : SW-846 8270C Date Posted : 11/04/03
Result Reporting Limit Fyagpyrene< 10 PWI 10 vg/L 0
Benzo(a)anthracene < 10 pg/L 10 pq/L 0
Chrysene < 10 pg/L 10 pl;V1.0
Bomo(b)fluoranlhene < 10 pg1L 10 pg/L 0
Bemo(k)fluoranthene < 10 pgfL 10 pgfL 0
Bemo(a)pyrene < 10 Vq/L 10 pgVL 0
lndeno(1,2,3~,d)pyrene < 10 pg/L 10 Vg(L 0
Dibenzo(a,h)anthracene < 10 pg1 10 pg1L 0
Beruto(g,hJ)perylene < 10 pg/L 10 pg/L 0
mple ID #: 23038617 Job#: 03-OCT-0052
Sample Descliption :PMWB-S (OVERBURDEN WELLS )
Collection Date : 21-00-03 15 :20:00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
!MGP PARAMETERS IN WATER BY GC/MS - 826 0
Test Code : MS8260MGPW Test Method : SW-846 50308/8260B Date Posted :11/03/03
Result Reportmg Limit Flag
Bomene 140 VqVL 2 .5 pGVL 0
Toluene 93 pg/L 5 .0 pgVL 0
Ethylbemene 290 pg1L 5 .0 pg/L 0
~;,-Xylene 120 lig/L 10 pgfL 0
o-Xylene 86 pgfL 5 .0 pWL 0
Naphthalene 2500 pl/L 100 pg/L 0
SVOC MGP IN WATER BY GCIMS - 8270
Test Code :MS8270MGPW Test Method : SW-846 8270C Date Posted : 11/04/03
Result Reporting Limit Flag
Naphthalene 3200 pg/L 1000 pgvl-0
2-Mothylnaphthalone 730 pgfL 100 pg/L 0
Acenaphthylene 10 pgr- 10 pgtL 0
Acenaphthene 230 plill . 100 VgA- 0
Dibenzofuran 19 pgfL 10 plifl- 0
Fluorene 69 pgVL 10 pg/L 0
Visit us on the IntraNet a tR,~r, ~n,.,,d 111512W3 14.01:42 http :/rde~/essen~Aabsrw/Page 2 of 10
1,0,vulle VUKe Fower Anaiyucal LaDoratoryPower.Phone .704-875,5245 Fax:[phone]
13339HagersFeriyPoed HontersvilleNC28076 .7929
McGuire Nuclear Complex - MG03A 2
Cartificato at Amnaiysis
New York Stale Department of Health C4'9116calior?# f 1717Oklahoma 0epartment of Environmental Quality Certification # 9930Kansas Department of Health and 5nifiromnent Oert&aje # E- 1031 t
North Carolina Department of Health &Human Services Cerfificatron # 37804
South Carolina (DHEQ Laboratory ID # 99005 North Carolina QENjr~ Certification #248
SamplelD#:23038617 Job #: 03-OCT-0052
Sample Description :PMWB-S (OVERBURDEN WELLS )
Collection Date : 211-00-03 15 :20:00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
IN WATER BY GC/MS - 827 0
Test Code : MS8270MGPW TestMethod :SW-8468270C Date Posted : 11/04/03
Result Reporting Limit Flag
Phenanthrene 36 pg(L 10 PGVL 0
Anthracene < 10 pg/L 10 Pg/L 0
Fluoranthene < 10 lig/L 10 pg1L 0
Pyrene < 10 pgVL 10 Pg/L 0
Benzo(a)anthracene < 10 P91L 10 P91 0
Chrysene < 10 Pg/L 10 Pg/L 0
Semo(b)fluoranthene < 10 pg/L 10 pgfL 0
Bemo(k)fluorafflhene < 10 pgtL 10 PgL 0
Bewo(a)pyrene < 10 pgVL 10 PGVL 0
lndeno(1,2,3~4pyrene < 10 pgVL 10 Pg/L 0
Dibemo(a,h)anthracene < 10 pgtI- 10 PgIL 0
Bemo(g,h,i)peryiene < 10 VgIL 10 pg/L 0
SamplelD#:23038618 Job #: 03-OCT-005 2
Sample Description :P-1S (OVERBURDEN WELLS )
Collection Date : 21-Oct-03 16 :20:00 Site :BURLINGTON Sample Type: IMGP SITE Desktop At
IMGIP PARAMETERS IN WATER BY GCIMS - 826 0
Test Code : MS8260MGPW Test Method : SW-846 603OB/8260B Date Posted:11/03/03
Result Reporting Limit Flag
Benzene 2.1 pgtL 0.50 pg/L 0
Toluene < 1 .0 pg/L 1 .0 pg/L 0
Ethylbenzene 2 .8 pgtL 1 .0 Pg/1- 0
~p-Xylene <2 .0 pg/L 2 .0 pgVL 0
o-Xylene 5 .2 pg/L 1 .0 pg/L 0
Naphthalene 17 pg/L 2 .0 pg/L 0
SVOC MGIP IN WATER BY GC/MS - 827 0
Test Code :MS8270MGPW Test Method : SW-846 8270C Date Posted : 11/04/03
Result Reporting Limit Flag
Naphthalene 17 pgVL 10 poll. 0
2-Methyinaphthalent 71 pg/L 10 PA 0
is Acenaphthylene 14 pgtL 10 pg/L 0
Vait as ..the IntraNet a tRe,~H Genemied 111512W314 01,42 http ://de~/essenv/lab-s"/P.&3 .r 10
I.Wvuite VUKe rower Anaiyucal LaDorator yPower.Phone :[phone] Fax [phone]
13339 Hag ers Perry Road HUntersville,NC26078-7929
McGuire Nuclear Compiox - MG03A 2
Cartificalhe afAmnaiysis
New York Stale Department of Health Certifrabon If 117f7Oklahoma Department of ErivironmentalQuably Certification #9930Kansas Deparlmrit of Health and Environment Certificate # E-103f f
North Carolina Department of ii-balth &Human Services Certification # 3780 4South Carolina QHEQ Laboratory 10 # 99005 North Carolina QIENF~ Certification #248
Sample ID #: 23038618 Job #: 03-OCT-005 2
Sample Description :P-IS (OVERBURDEN WELLS )
Collection Date : 21-Oct-0316 :20 :00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
OVOC 1MGP IN WATER BY GC/MS - 827 0
Test Code : MS8270MGPW Te ;t Method : SW-846 8270C Date Posted: 11/04/03
Result Reporting Limit Flag
Acenaphthene 34 pg(L 10 pg/L 0
Dibenzoluran < 10 pg/L 10 pq/L 0
Fluorene < 10 poll- 10 pg/L 0
Phenanthrene I I pg(L 10 pg/L a
Anthracene < 10 pg/L 10 pg/L 0
Fluoranthene < 10 pgfL 10 Pg/L 0
Pyrene < 10 pg1L 10 pg/L a
Bemo(a)anthracene 10 ug/L 10 pg/L 0
Chrysene 10 pg(L 10 pgfL 0
Bomo(b)fluoranthene < 10 pg/L 10 lig/L 0
Benzo(k)fluoranthene < 10 pg/L 10 pg/L 0
Benzo(a)pyrene < 10 pg(L 10 pg/L 0
lndenei(1,2.3~,d)pyrene < 10 PgA. 10 pgVL 0
Dibenzo(a,h)anthracene < 10 pg/L 10 pg/L a
Benzo(g.h.1)perylene 10 plill-10 VgA-0
Sample ID#:23038619 Job 03-OCT-005 2
Sample Description ;PMWC-S (OVERBURDEN WELLS )
Collection Date : 21 -Oct-03 09 :25 :00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
IMGP PARAMETERS IN WATER BY GC/MS - 826 0
Test Code : MS8260MGPW Test Method : SW-846 5030B/8260B Date Posted :11/03/03
Result Reppaing Limit F7a9
Benzene 3.4 pgVL 0 .50 pg/L 0
Toluene 1 .0 pg/L 1 .0 pg1l. 0
Ethylbenzene 2 .1 pg/L 1 .0 pgVL 0
m-p-Xylene <2 .0 p91L 2.0 "911 .0
~Xylene 4 .4 pq/L 1 .0 pgi.0
Naphthalene 90 pg/L 2 .0 pg/L 0
0
Vi.it s o. the lntt~et a tRepoH Genemfed 111512003 14 01 :42 http ://de~1essenvAab-srw/P.,#4 ~f 10
~%Uuke VUKe vowerAnaiyucal LarloratoryPower.Phone [phone] Pax,704-875-5038
D& E.T C~ 13339 Hag ers Feny Road Hunteraville,NC26078~7929
McGuire Nuclear Complex - MG03A 2
111~-4ertificate of Aftnaiysis
New YoniSlate Depatirrent of Health CerlifCalion #fl7t7Oklahoma Department of Environmental Quat Certification # 9930
Kansas Department of Heagh and Epvjronrwn (Cartificate # E-103f f
North Carolina Department of 1-kallh &Human Services Certification # 378N
South Carolina QHEQ Laboratory 0 # 99005 North Carolina (Dcpi~~Certification #248
SamplelD#:23038619 Job #: 03-OCT-0052
Sample Description :PMWC-S (OVERBURDEN WELLS )
Co4lection Date : 21-Oct-0309 :25:00 Site :BURLINGTON Sample Type: MGP SITE Desktop #
~SVOC MGP IN WATER BY GC/MS - 8270
Test Code :MS8270MGPW Test Method : SW-846 8270C Date Posted: 11104/03
Result Reporvng Limit Flag
Naphthalene 47 pg1L 10 p911-I
2-Methyinaphthalone 20 pg/L 10 pall, I
Acenaphthylene < 10 pg/L 10 PgIL 1
Acenaphthene 100 pg1l- 10 P911 .1
Dibenzofuran < 10 pg(L 10 Pg/L 1
Fluorene 22 pg/L 10 pg/L I
Phenanthrene I I pg/L 10 pg/L 1
Anthracene < 10 pg/L 10 pg/L I
Fluorarnhene < 10 pg(L 10 pg1L I
Pyrene < 10 pg/L 10 pgtL 1
Bamo(a)anthracene 10 ug/l . 10 pg/L I
Chrysene < 10 pall, 10 Pg/L I
emo(b)fluoranthene < 10 pg/L 10 Vg/L 1
emo(k)fluoranthene < 10 pg/L 10 pgtL 1
Benzo(a)pyrene < 10 pg/L 10 PgA.1
Indeno(l .2,3~,d)pyrene < 10 pg/L 10 Pg/L 1
Dibenzo(a,h)anthracene < 10 pg/L 10 pg1L I
Denzo(g,hJ)perylene < 10 pg/L 10 Pg/L 1
Sample ID #: 23038620 Job #: 03-OCT-0052
Sample Description ;MW-5 (OVERBURDEN WELLS )
Collection Date : 20-Oct-03 16 :30:00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
~MGP PARAMETERS IN WATER BY GC/MS - 8260
Test Code : MS8260MGPW Test Method : SW-846 5030B/8260B Date Posted :11/03/G3
Result Reporting Limit Rag
Bemene < 0 .50 pgA. 0.50 pg/L a
Toluene < 1 .0 pg/L 1 .0 pg/L 0
Ethylbenzene 1 .0 pg/l. 1 .0 Pgr- 0
M-p-Xylene <2.0 pgVL 2 .0 pgVL 0
o-Xylene < 1 .0 Vg/I. 1 .0 pgfL 0
Naphthalene 6.0 pg/L 2.0 pgtL 0
0
Vi.it w o. th~ Intr .Net a tR,.HG,~t~d 111512W3 14.0142 http ://dewww/essenvfIab-s"/P-g' # 5 ~f 10
r UUKe L)LtKeyower Anaiyucal LaDomory#Power.Phone [phone] Fax:[phone]
AD~[-VG~13339H8gersFetrl Road HuntersvilleNC28078-7929
McGuire Nuclear Complex - MG03A 2
Cartificata af A%nalysis
Now York State Department of Health Certifeation # ll7f7
Oklahormi)?paffnvnfofEnvironrwntolQuebtyCeilffication#9930
Kansas Departrmnl of Heath and Environment Certificate # 154031 1
North Carolina Department of Health &Human Services Certification # 3780 4
South Carolina (DHEQ Laboratory ID # 99005 North Carolina (D&0~ Certification #246
Sample ID It : 23038620 Job It : 03-OCT-0052
Sample Description :MW-5 (OVERBURDEN WELLS )
Collection Date : 20-Oct-03 16 :30:00 Site :BURLINGTON Sample Type : MGP SITE Desktop At
~SVOC MGP IN WATER BY GUMS - 827 0
Test Code : MS8270MGPW Test Method : SW-846 8270C Date Posted : 11/04103
Result RepoHM Limit Rag
Naphthalene < 10 pgrL 10 pg/L 0
2-Mothyinaphthalene < 10 pg/L 10 pg/L 0
Acenaphthylene < 10 pg/L 10 pg/L 0
Acenaphthene 14 PgA .10 PgVL 0
Ditsemofuran < 10 PgIL 10 Pgr-0
Fluorene < 10 pq1L 10 VgIL 0
Phenanthrene < 10 pg/L 10 Pq/L 0
Anthracene < 10 pg/L 10 pg1L 0
Fluoranthene < 10 pg1L 10 P91L 0
Pytene < 10 pgAL 10 Vg/L 0
Benzo(s)snthracene < 10 V911.10 pq/l. 0
Chrysene < 10 pqA. 10 pglL 0
Bemo(b)fluoranthene < 10 pg1L 10 PgrL 0
Beruto(k)fluoranthene < 10 pglL 10 Pgr- 0
BenWa)pyrone < 10 pgr. 10 VW1 0
Indeno(11,2,3~,d)pyrene < 10 pg/L 10 par . 0
Ditionzo(a,h)anthracene < 10 pg/L 10 pgVL 0
Benza(g,h,lhaerylene < 10 pglL 10 Pgr- 0
SampleID#:23038621 Job#: 03-OCT-0052
Sample Description : MW-9 (OVERBURDEN WELLS )
Collection Date : 22-Oct-03 14:15 :00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
;MGP PARAMETERS IN WATER BY GC/MS - 8260
Test Code : MS8260MGPW Test Method : SW-846 5030BIS260B Date Posted : 11/03/o3
Result- Reponing Limit Flag
Benzene <P.50 pgA . 0.50 VgA . 0
Toluene < 1 .0 pg1L 1 .0 pg/L 0
Ethylbomene < 1 .0 pgr- 1 .0 pg/L 0
~p-Xylene <2 .0 pg/L 2 .0 VGVL 0
c-Xylene 1 .0 pgA . 1 .0 V911-0
Naphthalene <2 .0 pgA .2 .0 pg/L 0
0
Visit a on tho lnt~.Net a t
R,,od G ..ramd 11151200314:0142 http ://de~/essenvAab-srw/P.&4 6 .f]O
P MUKe DIUKerower Anaiyucal LaDoraoryNower.Phone 704-875,5245 Fax :[phone]
A Er C~13339 Hagefs Ferry Road Huntersville,NC28078-7929
McGuire Nuclear Complex - MG03A 2
Cartificato of nnalysis
New York Slate Deparlment of Health Certification #t f7f 7Oklahoma D9partmentofEnvirtinmentalQualt Cgrificallon#9930
Kansas Deparlment of Heath an ~cerllfjcale If E-1031 1
North Carolina Department of t-befth &Human Services Certification # 378W
South Carolina (DHEQ Laboratory ID # 99005 North Carolina (DENR Cerlificatton,#248
SamplelD#:23038621 Job#:03-OCT-005 2
Sample Description :MW-9 (OVERBURDEN WELLS )
Collection Date : 22-Oct-M 14:15 :00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
~SVOC MGP IN WATER BY GC/MS - 827 0
Test Code : MS8270MGPW Test Method : SW-846 8270C Date Posted : 11/04103
Result Reporting Limit Rag
Naphthalene < 10 VgVL 10 WgIL 0
2-Methyinaphthalene < 10 ugl 10 pgA. 0
Acenaphthylene < 10 lig/L 10 pgr. 0
Acenaphthene < 10 pg1L 10 PgfI- 0
01benzofuran < 10 pgtL 10 Pg/L 0
Fluorene < 10 pqVL 10 PgA .0
Phenanthrene < 10 pgA. 10 PGVL 0
Anthracene < 10 pgfL 10 PgAL 0
Fluoranthene 10 pgtL 10 PGVL a
Pyrane < 10 pgVL 10 Pg/L 0
Bonzo(alanthrcene < 10 pg/L 10 P911 .0
Chrysene < 10 V91L 10 pg/L 0
Bonzo(b)fluoranthene < 10 pg/L 10 Vg/L 0
Bamo(k)Huorenthene < 10 pg/L 10 pg/L 0
Benzo(a)pyrene < 10 pgVL 10 pg/L 0
lndeno(1,2,3~,d)pyrene < 10 pg/L 10 pg/L 0
Dibenzo(a,h)anthracene < 10 pgtL 10 pg/L a
Domo(g .1t,itaorylene < 10 VgIL 10 Vg/L a
Sample ID #: 23038622 Job #: 03-OCT-005 2
Sample Description :PMWM-S (OVERBURDEN WELLS )
Collection Date : 2D-Oct-03 10:40 :00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
,MGP PARAMETERS IN WATER BY GICIMS - 826 0
Test Code : MS8260MGPW Test Method : SW-846 6030B/8260B Date Posted :11/03/03
Result Reporting Limit Rag
Benuteno < 0.50 pgr. 0 .50 pgr. 0
Toluene < 1 .0 plyl. 1 .0 PgV1- 0
Ethylbenzene < 1 .0 pgr- 1 .0 Pg/L 0
na-p-Xylene 2.0 Vg/L 2.0 p9r, 0
o-Xylene < 1 .0 pg/L 1 .0 PgVL 0
Naphthalene <2 .0 pgtL 2 .0 pg/L 0
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UUMe VUKe Fower Anaiyucal LaDoratior ypower.Phone [phone] Fax,704-875-5038
l3339H&gefsFeriyRo&d HuntersviIA9,NC28078-7929
McGuire Nuclear Complex - MG03A 2
Cartificat4e at fflinalysis
Now York Slate Department of Health Certification #t 17 f 7Oklahoma Department of Environmental Quality Cartifilcation # 9930Kansas Department of Health and Environment Cerlifrale # E-fO3f fNorth Carolina Department of I feafth &Human Services Certification # 3780 4
South Carolina IDHEQ Laboratory ID # 99005 North Carolina (DBVR Certification #248
1111 sill
Sample ID#:23038622 Job #: 03-OCT-005 2
Sample Description :PMWM-S (OVERBURDEN WELLS )
Collection Date: 20-Oct-03 10:40 :00 Site :BURLINGTON Sample Type: MGP SITE Desktop At
~VOC MGP IN WATER BY GC/MS - 827 0
Test Code : MS8270MGPW Test Method : SW-846 8270C Date Posted : 11/04/03
Result Reportng Limit Flag
Naphthalene < 10 pg(L 10 pgf .1
2-Methyinaphthalene < 10 pgIL 10 pg1L 1
Acenaphthylene < 10 pg(L 10 pg/L I
Acenaphthene < 10 pgfL 10 pg/L 1
Dibenvoluran < 10 pg/L 10 pgr-1
Fluorene < 10 pg/L 10 pg(L 1
Phenanthrene < 10 pg/L 10 pgA- I
Anthracene < 10 pgr- 10 pgtL 1
Fluoranthene < 10 pgtL 10 pg/L I
Pyrene < 10 pg(L 10 pg/L I
Benvo(a)anthracene < 10 pg1L 10 pgr- 1
Chrysene < 10 pg/L 10 pg1L 1
8enzo(b)fluoranthene < 10 pg/L 10 pg/L I
Beruto(k)fluoranthene < 10 pgtL 10 pg/L 1
Benzo(a)pyrene < 10 pgVL 10 pg(L 1
lndeno(1,2,3~,d)pyrene < 10 pg/L 10 pgVL I
Dibenzo(a,h)anthracene < 10 pg/L 10 pg1l. I
Bento(g,h,I)perylene < 10 pgn.10 jg/L 1
SamplelD#:23038623 Job #: 03-OCT-005 2
Sample Description :PMWL-S (OVERBURDEN WELLS )
Collection Date : 22-00-03 09 :25 :00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
~MGP PARAMETERS IN WATER BY GC/MS - 8260
Test Code : MS8260MGPW Test Method : SW-846 5030BIS260B Date Posted :11/03/03
Result Reporting Limit F-7ag
Benzene < 0.50 pg/L 0 .50 pg/L 0
Toluene < 1 .0 poll. 1 .0 pgVL 0
Ethylbenzene < 1 .0 pg/L 1 .0 pg1L 0
m-p-Xylene <2 .0 pg/L 2 .0 pgVL 0
~Xylene < 1 .0 pg/L 1 .0 pg/L 0
Naphthalene 2 .0 pg/L 2.0 pA 0
0
Visit us an the IntraNet a tRe~n Gnerated 111512003 14:01 :42 http ://dew~/essenv/lab-srv/Pas,8 af 10
?UUKe VUKe -rowerAnaiyuieal LaDoratoryP"Power.Phone : 704-67-r-5245 Fax:[phone]
13339HagetsFertyPoad lfuntersvilAq,NC28076-7929
McGuire Nuclear Complax - MG03A 2
Cartificata ofAnaly -,%i~s
New York State Department of Health Carlification # ll7f7
Oklahoma Department of Environmental Quality Ceriffication # 9930Kansas Department of Heath and Environment Certificate If E-103 f I
North Carolina Department of Health &Human Services Certification # 37804
South Carchna QHEQ Laboratory ID # 99005 North Carolina Q80~ Certification 248
Sample ID #: 23038623 Job #: 03-OCT-0052
Sample Description :PMWL-S (OVERBURDEN WELLS )
Collection Date: 22-Oct-03 09 :25 :00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
I
OVOC MGP IN WATER BY GCIMS - 8270
Test Code : MS8270MGPW Test Method : SW-846 8270C Date Posted : I l/D4/03
Result Reporting Limit Rag
Naphthalene < 10 pgtL 10 pg1L 0
2-Mothylmphthalene < 10 pgVL 10 Pg/L 0
Acanaphthylene < 10 pgtL 10 pgA-0
Acenaphthene < 10 VgVL 10 Pg/L 0
ItIliemohmm < 10 pgVL 10 Pg/1.0
Ruorens < 10 pg1L 10 pg1l. 0
Phenanthrene < 10 Vg/L 10 pg/L 0
Anthmcene < 10 pGVL 10 pg/L 0
Fluoranthene < 10 pg/L 10 Pg/L 0
Pytene < 10 pg/L 10 pgIL 0
Benzo(a)anthracene < 10 pg/l. 10 pgVL 0
chrysene < 10 pg1L to P91L 0
Bomo(b)fluoranthene < 10 PWL 10 poll. 0
Borutolk)fluoranthene < 10 poll. 10 pg/L 0
Sento(a)ptinme < 10 pg/L 10 PgVL 0
lndeno(1 .2,3~,d)pyrene < 10 pg/L to pg/L 0
Ditienzo(a,h)anthracene 10 Vg(L 10 PgA-0
Sento(g,h,I)perylene < 10 pgA.10 PgVL 0
Sample ID #:23038624 Job#: 03-OCT-0052
Sample Description :FIELD BLANK (OVERBURDEN WELLS )
Collection Date: 23-Oct-03 10 :25:00 Site :BURLINGTON Sample Type : MGP SITE Desktop At
!,MGP PARAMETERS IN WATER BY GCIMS - 8260 _7
Test Code : MS8260MGPW Test Method : SW-846 5030B/8260B Date Posted:11/03/03
Result Reporting Limit Rag
Bomene < 0 .50 pg(L O .SO pq1L 0
Toluene < 1 .0 Pg/L 1 .0 Pg/L 0
Ethylbenzene < 1 .0 pgtL 1 .0 pg/L 0
m-p-Xylene <2 .0 Vg(L 2.0 pgVL 0
o-Xylone < 1 .0 pg/L 1 .0 pg1L 0
Naphthalene <2.0 Vg/L 2 .0 fig/L 0
Visit us on the Int~aNet a tR,,~,,ot,d 11151200314.01 :42 http ://de~/essenvAab s~l pae 9 of 10
p.pume VUKe Fower Anaiyricai LaDoreatoryPower.Phone [phone] Fax.7C4-675-503 8
13339 Hagers Ferry Road HuntefsvilleNC28078-7929
McGuire Nuclear Compkax - MG03A 2
C4ert!Mciiata af Aknaiy --sis
New York State Dwartment of Health Certification # lf7f7
Oklahoma Department of Environmental Quality Ogr1ification # 9930Kansas Depanirnent of Health and Environment Certificate # E-fO3f I
North Cerohna D9partment of l'bafth &Human Services Certification # 37804
South Carolina (DHEQ Laboratory ID # 99CO5 North Carolina Q&Vf~Certification #248
Sample]D#:23038624 Job #: 03-OCT-0052
Sample Descilption :FIELD BLANK (OVERBURDEN WELLS )
Collection Date : 23-Oct-03 10 :25 :00 Site :BURLINGTON Sample Type: MGP SITE Desktop #
~SVOC MGP IN WATER BY GVIMS - 8270
Test Code: MS8270MGPW Test Method: SW-846 8270C Date Posted: 11/04/03
Result Reporting Limit Flag
Naphthalene < 10 pg1l. 10 pg/L 0
2-Mettlyinaphthalene < 10 pgtL 10 p9tL 0
Acenaphthylene < 10 pgtL 10 pg(L 0
Acenaphthene < 10 Vg/L 10 pg/L 0
Dibenzofuran < 10 Vg/L 10 pg/L 0
Fluorene < 10 p(YL 10 VgVL 0
Phenanthrene < 10 pg& 10 pg/L 0
Anthracene < 10 Vg/L 10 lig1l. 0
Fluorinthene < 10 pg/L 10 VgVL a
Pyrene < 10 pg/L 10 pgfL 0
Bemo(a)anthracene s: 10 pg/L 10 pg/L 0
Chrysene < 10 PA 10 POIL 0
Benzo(b)fluoranthene < 10 pgtL 10 pg/L 0
Bemo(k)fluoranthene < 10 piyl 10 pg1l. 0
Ba=o(a)pyrene < 10 VgIL 10 VgVL 0
Indeno(1,2,~c,d)pyrent < 10 pg(L 10 pg/L 0
Dibenzo(a,h)anthracene < 10 pg/L 10 pg1l . 0
Bemo(g,h,I)perylene < 10 PPI 10 pg/L 0
------------------------------------
r)escriTptic>n c3f Flacrs :
0 - All Analytical Procedure Requirements Were Met
I St . C...Nastruse.
2 -Estimated Concemenestion .site Cans,~nashss
3 -Ra,,mt Users Motivated ohn,. frimmetere...,I .
4 -Re,ort ~fm,Marooned don, a required somi &lot ..
5-SamploRcealtsSihould at Be Used For Reulasory Porprea s
6 -Antolini defamed b .i- 1 .1mrst.eir remain, 1,.,,....ad
...tarmsm-h,
7 -Reported caticentratiest is rise constanstron of more thin one sroclor.
- - - - - - - - - - - - - - - - -L - - - (Repored Aroinor 19-the Aroolin of highest concentration in the surepa)_
PtaRePodedBy. Date
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RiWH (il,thhated 111512003 14 :01 :42 http ://de,,vww/essenv/Iab-srv/Page 10 of 10
0 1 QUEST FORMCHAINOFCUSTODYREC RD AND ANALYSIS R E
boratory ervices i aTa,PW Duke ----------~`----------- Sa IeC 'Page k ofOW
Mail Code MG03A2 (Building 7405)Energy..13339 Hagers Ferry Rd DISTRIBUTION
For Detailed Instructions, see : Huntersville,N . C. 28078 ORIGINAL to LAB,
http ://dewww/essenv/cocl Fa
[phone] COPY to CLIENT
..........................i:.(7L4)~?5-Aqj
I)Project Name 2)Phone No :875-5257
BURLINGTON MGP(SAPROLITE WELLS)
r 3)Client C .Campbell R . Roberts 4)Fax No:875-5032
>
5)BusinessUnit: 20018 6)Process : T)R..p To 0-193 E
E
08)Proje .t ID .MGPBURL 9)Activity to: ALLACTV 10)NIall Code :MG03-A3U Customer W comolete all 0&2orojariate NoN-sHADED areas,0 7E---------------14C 0 0 0LABUSEONLY12Chem ollection Information .0 20
E < =1-<13 0 W"Lab to i Desktop No . Sample Description or ID D .tTTimT SlanatUre z 2 W I W I of
PMWB-D x 1 1 3 111031It ~.5-
04 -DPMWC
1:16 ,
.1 C --LiA x 1 1 3 1 6- I : 0 f f~-l PMWF-D x 1 1 3 1 6i'M
~1 r PMWG-D IQ /,3 X I I t3l
-9
PMWI x 1 1 3 1tobolol let 00 "1
PMWL-D x I 1 3
Ar
cL0U
Customer to sign &date below
21)Rell nqui shed By Daternme A c
D/z o /a z ~;-o ~Requested Turnaround
915 tedBpT9(T A ed B
ti,
14 DaysDAM -vn~* 0 W 0~11 .61111M..2 M'F1 1-11 _n V,
FK..S -I Uays
23)SeaVLockea uy Dater'nme E om ~w
'48Hr-
I
24)Comments "PLEASE HAR
November 4,2003 1 :58 :27 PM Page #1 of l
Duke 8270/625 Analysis
OvEnergy.Case Narrativ e
r1his domment must aownymny release of Analqtical Data)
LIMS Job #03-OCT-0053
Wor"St #03-.wOCT-;06-42
4 The percent recovery for the surrogates were outside of the laboratory control lirnit in
sample 23038625.Me results for all analytes should be considered estimates for
these samples .
- --------------
Shannon Rollin s
-------------------------------------------------------------------------------------
Duke Energy Analytical Laboratory Service s
Envirorurnent, Heah &Safety Semices Environmental Center - MG03A2
Phone:[phone] Hagers Ferry Road
FAX:[phone] Huntersville NC 28078-7929
SACasc Nwativ~\Orgmic\SVOA\oc(-0053 .doe
PhDuke Duke Power Analytical Laboratory
OrPower.Phone :[phone] Fax:701-875,5038
AD~E-,G",13339 HagerSFerly Road Huntefsville,NC28078-7929
McGuire Nuclear Complex - MG03A 2
Cc--rt1114=mtt--Clot AIX n m I yLs i
Now York Slate Department of Health Certification # f 1717
OklahorneDi?partrnentofEnvironmenialOuab Carlification#9930
Kansas Department of Heath and Environment Certificate # E-fO3f j
North Carolina f)Rpadment of Health &Human Services Certification # 378M
South Carolina (OHEQ Laboratory ID # 9"5 North Carolina (DEIVR Certification #248
Station Name :BURLINGTON Job Number 03-OCT-0053
Sample ID #: 23038625 Desktop #Customer ID :R.ROBERTS
Sample Description : PMWB-D (SAPROLITE WELLS)
Collection Date : 21-Oct-03 14 :25 :00 Date Received in Laboratory : 02-Oct-03 Type of Sample : MGP SITE
ReferenceMethod :EPA310.1/SM2320B Data Posted :10/2812003 15:20:4 7
ALKALINITY (TOTAL INFLECTION POINT'ALKOV-11VITY 3.56 meg/L
Reference Method :EPA200.7/601013 Data Posted : I VW200308:20:5 1
[RON BY 1CP (DIGESTED)IRON 18.668 MgA
Reference Method :EPA 200-7/6010B Data Posted :11/5/2003 08:20:5 1
MANGANESE BY 1CP (DIGESTED)MANGANESE 3 .781 mg/L
Reference Method :EPA 300.0 Data Posted : 1012412003 16:24 :0 5
MG-N/L BY CALCULATION TE <0.02 mg-N/L
Reference Method :EPA 300.0 Data Posted : 10/24/2003 13:18 :38
NITRATE (IC)TE < 0.10 mcf/L
Reference Method :EPA 300.0 Data Posted : 10/2412OD3 13:18 :38
SULFATE (IC)SULFA TE 0 .11 mgfL
Sample ID #: 23038626 Desktop If CustomerID: R .ROBERTS
Sample Description : PMWC-D (SAPROUTE WELLS )
Collection Dale : 21-Oct-03 11 :30:00 Date Received in Laboratory: 02-Oct-03 Type of Sample :MGP SITE
Reference Method: EPA31O.i/SM23208 Data Posted: 10/28120M 15 :20.47
ALKALINITY (TOTAL INFLECTION POINT ALK4UAYTY 5.09 mea/L
Reference Method :EPA 200 .7/601013 Data Posted:11/5/2003 08 :20:52
IRON BY ICIP (DIGESTED)IRON 9.791 mqA
Reference Method:EPA 200 .7/60108 Data Posted:11/5/2DD3 0820:52
MANGANESE BY ICIP (DIGESTED)AMGANESE 8 .529 mg/L
Reference Method:EPA 300.0 Data Posted: 10/2412003 16 :24 ;06
MG-N/L BY CALCULATION NITRATE <0,02 mg-N/L
Reference Method:EPA 300.0 Data Posted : 10/2412003 13 :09 :56
NITRATE (IC)NfTRATE < 0 .10 mg[L
Reference Method :EPA 300.0 Data Posted : 101241=13 :09 :56
SULFATE (ICI SULFATE 0.10 m_q/L
Vi.it ~,.n~ t.h. Int.,.Nt.t.
Report Ge"mied 111512003 14:00 http ://de~/essenvAab.sm/Ng, 0 1 4 4
PhDuke Duke Power Analytical Laborator y
,wPower.Phone : 7os-875-5245 Fox 704-875-5038
AD,k&VC.V,13339 Hagers Ferry Road Huntelsvitle,NC 28078-7929
McGuire Nuclear COMPlax - MG03A 2cof ALnaiy-sir~
New York State Dwarlmont otHealth Certification # If 7t7
OklahoniaDepedrnentofEnvironrwnlalQuab Certification #9930
Kansas Department of Heagh and EmnironmenMedificate # E-103f f
North Carolina Department of 1-bafth &Human Services Codification #37604
South Carolina (DI-EQ Laboratory 10 #99005 North Cambria (Di3VR Certification #248
Station Name :BURLINGTON Job Number 03-OCT-0053
Sample ID 23038627 Desktop #Customer ID :R .ROBERTS
Sample Description : PMWF-D (SAPROUTE WELLS)
Collection Date : 21!-Oct~03 08:45 :00 Date Received in Laboratory ; 02-Oct-03 Type of Sample :MGPSfTE
Reference Method :EPA310.1/SM23208 Data Posted : 10/211~2003 15:20 :47
ALKALINITY (TOTAL INFLECTION POINT ALKALINITY 10.09 mecilL
Reference Method:EPA200.7/6010B Data Posted :11/5/2003 08 :20 :52
IRON BY ICIP (DIGESTED)IRON 12.844 mqA
Reference Method:EPA20D.7/6010B Data Posted :11/512003 08 :20:53
MANGANESE BY ICIP (DIGESTED)MANGANESE 4.793 mglL
Reference Method :EPA 300.0 Data Posted : 10/24/2003 16:24 :07
MG-WL BY CALCULATION NfTR4TE <0.02 mg-N/L
Reference Method :EPA 300.0 Data Posted : 10/2412003 13:16 :3 9
NITRATE (IC)NITRATE < 0.10 mg/L
Reference Method :EPA 300 .0 Data Posted : 10/24/2003 13 :16 :3 9
SULFATE (IC)SULFATE 0.43 mg/l.
Sample ID #: 23038628 Desktop It Customer ID :R.ROBERTS
Sample Description : PMWG-D (SAPIROLITE WELLS )
Collection Date : 20-Oct-03 15:65:00 Date Received in Laboratory: 02-Oct-03 Type of Sample :MGP SITE
Reference Method:EPA310.1/SM2320B Data Posted: 1042812003 15:20:47
ALKALINITY (TOTAL INFLECTION POINT ALKALINITY 4.08 mag/L.
Reference Method:EPA 200.7/6DIOB Data Posted: 11/512003 08:20:53
IRON BY ICP (DIGESTED)IRON 0 .426 m-qfl
Reference Method :EPA 200 .7/6010B Data Posted :11/512OD3 08:20 :53
MANGANESE BY ICP (DIGESTED)A44NGANESE 2.465 m_q/L
Reference Method :EPA 300 .0 Data Posted : 1012412003 09 :00 :00
MG-NIL BY CALCULATION NITRATE 0.77 mg-N/L
Reference Method :EPA 300.0 Data Posted:10/23/2003 11 :47:56
NITRATE (IC)NITRATE 3.42 mg/L
Reference Method:EPA 300.0 Data Posted:1(V=OD3 11 :47:56
SULFATE (IC)SULFATE 20.60 m_q/L
vi-it th
. T .t,.N~t 0Repart,Gen,mted 11151200314:00 http://d,~/essenv/Iab-arv/Pg,02,,t 4
PhDuke Duke Power Anal ical LaboratoryorYtPower.Phone : [phone] Fax:[phone]
A D~&V 13339 HagersFerry Road HuntetSWIS,NC28078-7929
McGuire Nuclear Complex - MG03A 2
t-- r I c : -%t %--cip r A na i ys. i
New York State Department of Health CoHilication # f f717
OklahormDapaifnvntofErwitonmentolQuab CgrIdicabon#9930Kansas Deparlment of Heath end EnvirotimimMerifficate #E-tot iNorth Carolina DRP811mont of Health &Human Services Certification # 37804SouthCarohnefDHEQLaboratoryID It 99005 North Carolmina,(DENR Codification #248
Station Name :BURLINGTON Job Number.,03-OCT-0053
Sample ID 23038629 Desktop If Customer ID :R .ROBERTS
Sample Description : PMWI (SAPROLFTE WELLS )
Collection Date : 20-Oct-03 14 :00 :00 Date Received in Laboratory : 02-Oct-03 TypeofSample :MGPSITE
Reference Method:EPA310.1/SM2320B Data Posted: 10/21112003 15:20:47
ALKALINITY (TOTAL INFLECTION POINT ALKALINITY 3.09 meg/L
Reference Method:EPA200 .7/6010B Data Posted :ll/SI200308 :20 :54
IRON BY ICP (DIGESTED)IRON 9 .916 mgA
Reference Method :EPA200.7/6010B Data Posted : 11/5/200308 :20 :54
MANGANESE BY ICP (DIGESTEDI MANGANESE 1 .148 mg/L
Reference Method :EPA 300.0 Data Posted:I Qt24/2003 09:00 0 1
MG-N/L BY CALCULATION NITRATE <0.02 mg-N&
Reference Method :EPA 300~O Data Posted :10/23/2003 11 :48:49
NITRATE (IC)NURATE < 0.10 ma/L.
Reference Method :EPA 300 .0 Data Posted: 10123V2003 11 :48 :4 9
SULFATE (IC)SULFATE 9 .02 mg/L
Sample ID #: 23038630 Desktop Of CustomerID : R .ROBERTS
Sample Description : PMWL-D (SAPROLITE WELLS )
Collection Date: 22-Oct-03 11 :05 :00 Date Received in Laboratory : 02-Oct-03 TypeofSample :MGPSfTE
Reference Method:EPA310.11SM2320B Data Posted:1012812003 15:20:47
ALKALINITY (TOTAL INFLECTION POINT ALKALINITY 2.06 meg/L.
Reference Method :EPA 200.7/60108 Data Posted: 11/5/2DD308 :20:54
IRON BY ICP (DIGESTED)IRON 26.742 mcO
Reference Method:EPA 200 .7/6010B Data Posted :1115/2003 08 :20 :5 5
MANGANESE BY ICIP IDIGESTEDI MANGANESE 0 .668 mg/L.
Reference Method:EPA 300.0 Data Posted: 10/24/2003 16:17:57
IVIG-WIL BY CALCULATION NITRATE <0.02 mg-N/L
Reference Method :EPA 300.0 Data Posted: 1012412OD3 14 :42 :0 2
NITRATE flC)NiTFL4TE < 0.10 m_q/L
&p.rt Gew~ted 111512003 14:00 httpWitle~/essenr/lab aml Pg, #3,,l 4Vi. it "...t T .t'.N .t -t
Pkvuke Duke Power Analytical Laborator y,wPower.Phone :[phone] Fox.70$-875,%36
13339 HagOrSFGrIY Road HuntersvilleNC28078-7929
McGuire Nucfear Complex - MG03A 2C4ert1f14=at*-- 64A n a i ys i n,
Now York Slate Department of Health Certification 9 117f7
OklahornaDgpadn~entofEnvitonrnentolQuab CarlAcation#9930
Kansas Department of Heath and EnvironmenMerfificale # E-fO3f f
North Carolina Departrient of Hatifth &Human Services Cedification # 37804
South Carolina (DhEQ Laboratory ID# 99005 North Carolina (DeqR Certification 0 248
Station Name :BURLINGTON Job Number 03-OCT-0053
Sample ID # 23038630 Desktop #Customer ID :R.ROBERTS
Sample Description : PMWL-D (SAPROLITE WELLS)
CollectionDate : 22-Oct-0311 :05 :00 Date Received in Laboratory : 02-Oct-03 Type of Sample :MGP SITE
Reference Method :EPA 300.0 Data Posted : 10124/2003 14 :42.02
SULFATE (IC)SULFATE 30.62 mg/L
D#Veffmd~Approvadfly,Date
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Repo~ Ge~rated 111512003 14:00 http ://dew~w/essenv11ab-Sm/Pg,04,4 4
phpuke Duke Power Analytical Laborator y#Power.Phone:[phone] Fax.[phone]
ADAE-VG~13339HagersFerlYPOad HuntersviliaNC28078-7929
McGuire Nuclear Compex - MG03A 2
cortificata of nnalysis
New York Slate Deloartment of Health Cerlifralion # f f717Okfahoma Depaillnent of Environmental QvaM/Certification # 9930
Kansas Department of Heath and 15Dvironrlent Certificate # E. f 03 f f
North Carolina Department of Heafth &Hurnan Services Certification #37804
South Carolina (DHEQ Laboratory ID # 99005 North Carolina (DENq Certification #248
1 -
SamplelD#:23038625 Jobilt :03-OCT-0053
Sample Description :PMWB-D (SAPROLITE WELLS )
Collection Date: 21-Oct-03 14:25 :00 Site :BURLINGTON Sample Type : MGP SITE Desktop It
OGP PARAMETERS IN WATER BY GCIMS .8260
Test Code: MS8260MGPW Test Method : SW-846 503OB/8260B Date Posted :11/03/03
Result Repoffing Lknit Flag
Benzene 20 VgIL 5 .0 P91.0
Toluene < 10 pg/L 10 PGVL 0
Ethylbonmne < 10 pg/L 10 PgVL 0
m-p-Xylene <20 pgA-20 Vg/L 0
~Xylene < 10 V91L 10 11gri .0 .
Naphthalene 230 pgtL 20 pgVL 0
R BY GCIMS - 827 0
Test Code : MS8270MGPW Test Method : SW-846 8270C Date Posted : 11/04/03
Result Reporyngyrnit Flag
Naphthalene 660 pgA. 100 PWL
2-Mathyinaphthalene 170 pA 100 P911 .
Acenaphthylene 10 Pg(L 10 PgtI .I
Acenaphthene 370 Vg/L 100 PA I
Dibemofuran 32 ;jg/L 10 PglL I
Fluorene,79 pgVL 10 pg(L I
Phenanthrene 93 pA 10 PgA . I
Anthnacene 19 Poll.10 VA
Fluoranthene < 10 pgA- 10 WIL
Pyrene < 10 pglL 10 PA 1
Bemo(a)anthracene < 10 pgt 10 PGVL I
Chrysene < to P(YL 10 M1 1
Bento(b)lluaranthene < 10 pg/L 10 PWI
Banzo(k)fluoranthene < 10 Pgit.10 PgVL
Bertto(a)pynsne < to Pgri. 10 PGVL
Indew(l .2,3~4)pyrene < 10 pg/L 10 Pg/I.
DIben ;eo(a,h)anthra"ne < 10 PA 10 Vg/L
8en ;to(q,h,I)peryIene < 10 Vg(L 10 VglL I
Visit us an the IntraNet a tJU,,~Ge~nued 11151200314:W.34 httpJ/de~/essenv/Iab-szv/P.,,8 1 .r7
P.&DUke VUKe Fower Analytical Laborator yPower.Phone [phone] Fax .704-875-W38
13339HagersFeriy Road HuntersvillsNC28078-7929
McGuire Nuclear Comoilax - MG03A 2cartificata of Aknalysis
New York State Department of Health Certification # f f717Oklahoma Department of Environmental Quah~ Certification # 9930Kansas Department of Health and Environmen cerfificale#15403f tNorth Carolina Deparlment of Fkalth &Human Services Cerlificabon # 37804South Carolina (DHEQ Laboratory ID #99W5 North Carolina (DENF~Certification #248
Sample ID#:23038626 Job #: 03-OCT-0053
SamPleDescription :PMWC-D (SAPROLITE WELLS )
Collection Date : 21 -Oct-03 11 :30:00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
OGP PARAMETERS IN WATER BYGCIMS-826 0
Test Code : MS8260MGPW Test Method : SW-846 50301318260B Date Posted :11/03103
Resuft Reponng Limit Flag
Bemene < 5.0 pg/L 5.0 ygll- 0
Toluene < 10 WA 10 pg(L 0
Ethylbemene 37 pg/L 10 VgVL 0
m-p-Xylene <20 pg/L 20 V91L 0
o-Xylene 13 pipt 10 PA 0
Naphthalene 630 pgI 20 pA 0
OVOC MGP IN WATER BY GC4MS - 8270
Test Code : MS8270MGPW Test method: SW-846 6270C Date Posted : jifoii/o3
Restsit Reporting Limit Reg
Naphthalene 19M pg/L 1000 pgtL 0
2-Methyinaphthalene 640 p91L 100 Pg/L 0
Acenaphthylene 23 VA 10 pgtL 0
Acenaphthene 230 pg& 100 pgVL 0
Ditiemoturan 23 pgVL 10 pg/L 0
Fluorene 57 pgVL 10 pg& 0
Phenanthrene 47 pg/L 10 pgVL 0
Anthracene < 10 p91L 10 Pgr- 0
Fluoranthene < 10 IjGVL 10 WA 0
loyrene < 10 pgVL 10 pg(L 0
Bema(a)anthracene < 10 pg/L 10 Pg/L 0
Chrysene < 10 pWL 10 pgIL 0
lle~(b)fluoranthene < 10 pg/L 10 pg/L 0
Be=(k)fluoranthene < 10 p91L 10 pgVL 0
Bemo(a)pyrene < 10 pg(L 10 pgVL 0
Indeno(1,2.3~.d)pyrene < 10 pg/1- 10 PgVL 0
Dibemo(a,h)anthracene < 10 pg(L 10 VgVL 0
Bemo(q,h,I)perylene < 10 pg(L 10 PgA.0
0
Visit us on the IntraNet atFa,,oHC~~mud 111512W314:W.34 littliJ/de~/essenvAtibisiw/Poll #2 f 7
phpuke Duke Power Analytical Laborator ytrPower.Phone :[phone] Fax :[phone]
A Dsk 5s,0 Cs"13339HagefsFerrf Road Huntemv1119,NC28078-7929
McGuile Nuclear Compiax - MG03/1 2cartificato of Analysis
New York Slate OVailment of Health Cerfifration # I f7f 7Oklahoma Department of Environmental Quah~ Cadlication # 9930Kansas Department of Heath and Environmen Cerlkate # E-103i ft
North Carolina Department of Health &Hurnan Services Cerlificalion # 37804
South Carolina (DHEQ Laboratory ID # 99005 North Carolina (DBVR Certification #248
SamplelD#:23038627 Job #: 03-OCT-0053
Sample Description :PMWF-D (SAPROLITE WELLS )
Collection Date: 21-Oct-03 08:45 :00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
OGP PARAMETERS IN WATER BY GCIMS - 8260
Test Code: MS8260MGPW Test Method : SIN-846 50305/8260B Dale Posted: 11/04103
Result Reporting Limit gag
Bemene 0 .55 V91 0 .50 Vg/L 0
Toluene 4 .6 VgL 1 .0 Vq/t,0
Ethylbemem 26 pg/L 1 .0 pg1l. 0
rn-p-Xylene I I pg/l.2 .0 pA 0
~Xylene 13 pg&1 .0 pg/L 0
Naphthalene 320 pg4-20 pg/L 0
~SVOC IMGP IN WATER BY GCfMS - 8270
Test Code : MS$270MGPW Test Method :SW.8468270C Date Posted: 11/04103
Result RopoVng Unit Flag
Naphthalene 2100 jig& 1000 PA 0
2-Methyinaphthatene 570 pgtL 100 PA 0
Acenaphthylene < 10 pgVL 10 POIL 0
Acenaphthene 270 pA 100 Pq& 0
Dibemofuran is PgIL 10 IjgVI.0
Fluomne 63 PGVL 10 PgI 0
Phenanthnene 44 pg1l. 10 Pg/L 0
Anthracene < 10 pg/L 10 PgIL 0
Fluoranthene < 10 pg/L 10 P91L 0
pyrene < 10 pg1L 10 Pg/l. 0
Bomo(a)anthracene < 10 Pg1.10 WA 0
Chrysene < 10 pg/L 10 pg4,0
Benzo(b)fluoranthene < 10 pg/L 10 PGVL 0
Bemoik)fluoranthene < 10 pgtL 10 PA a
Bemo(a)pyrene < 10 pgtL 10 p9t 0
lndeno(11,2,3~,d)pyrene < 10 pg/L 10 P91L 0
Dibemo(a.h)anthracene < 10 Pg4- 10 PgVL 0
13emo(g,h,Qperylene < 10 pg/L 10 ligIL 0
Visit us on the IntraNet a tRepon C~wroied 111512003 14.,0034 http :llde~/essenvflab-s~/Pn,,13 .f 7
pkDuke Duke Power Analytical Laborator yOftwer.Phone:[phone] Fax : [phone]
AD*b-,C-"13339 HagefsFerly Road Huntefsville,NC28078-7929
mcGutfe Nuclear Complex - MG03,4 2Cartificate of fflinalysis
New York Slate DWarlment of Heafth ClerIfficalion # f 1717OklahormOspedn)entofEnvironrr,entolQuab Cedification#9930
Kansas Department of Heath and EnvirowneriNCerlificale It E-fO3f INorth Carolina D~pafimnf of Heafth &Human Services Certification # 378 NSouth Carolina QHM Laboratory ID # 99005 North Carolina (DBVF~ Certification #248
SampIeID#:23038628 Job #: 03-OCT-005 3
Sample Description :PMWG-D (SAPROLITE WELLS )
Collection Date : 20-Oct-03 15 :55 :00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
OGIP PARAMETERS IN WATER BY GCIMS - 8260
Test Code : MS8260MGPW Test Method : SW-846 503OB/8260B Date Posted:11/04/03
Result Reporting Lirnft Rao
Elemene O.S2 pgtL 0.50 PWL 0
Toluene < 1 .0 pg/L 1 .0 pgVL 0
Ethylbenzene 1 .0 pg1L 1 .0 pg/L 0
m-p-Xylene < 70 pgVL 2.0 pWL 0
o-Xylene 1 .8 pg1l. 1 .0 PWL 0
Naphthalene 0 .9 pg/L 2.0 pWL 0
~VOC MGP IN WATER BY GC/MS - 8270
Test Code : MS8270MGPW Test Method : SW-846 8270C Date Posted: 11/04/03
Resuft Repa" Lena Flag
Naphthalene < 10 pg/L 10 Po(L 0
2-Methyinaphthalene < 10 Pg& 10 pgtL 0
Acenaplithylene < 10 pg/L 10 Pg&0
Acensphthens 51 pg/L 10 pg/L 0
Diberurofuran < 10 pg1L 10 Pg1L 0
Fluorene 12 VgVL 10 PWL 0
Phonanthrene 20 pg/L 10 P91. 0
Anthracene < 10 pg1L 10 pq1t. 0
Fluoranthens < 10 pg(L 10 pg&0
Pyrene < 10 pgVL 10 PGVL 0
Bemo(a)anthnscene < 10 pg/L 10 PgVL 0
Chrysene < 10 VA 10 PA 0
Bemo(b)fluonenthene < 10 pgtL 10 PgA. 0
Benzo(k)fluoranthene < 10 PA 10 PA 0
Benzo(a)pyrene < 10 pg/L 10 PgIL 0
Indeno(1,2-1-C,d)pyrene < 10 Vg/L 10 Pg/L 0
Dibemo(a,h)anthnacene < 10 pgL 10 PA 0
Bemo(g .h .operylene < 10 1,911- 10 pqfl. 0
C
Visit us on the IntraNet a tP,,,on G,.ro,,d 11151200 14,00 34 httpJ/de~/essenv/lab~s~/Pog~8 4 f7
P,kDuke Duke Power Analytical Laborator yPower.Phone :[phone] Fax:[phone]
ADAE-VC-fM 13339 HagersFeriy Road Huntelsville,NC26078-7929
McGuire Nuclear Complex - MG03A 2Cartificato af janalysis
New York State Depadwit! ofHeafth Certification # 11717
OklahorwDepailnvntofErwimnnvnlalQuaktyCen&alion#9930
Kansas Department of Heath and EnvironmentGarlifrole #E-fO3f f
North Carolina Department of 1-bagh &Human Services Certification #37804
South Carolina (DHEQ Laboratory ID # 99005 NoHh Carolina (D04)~~ Certification #248
Sample ID #: 23038629 Job #: 03-OCT-0053
Sample Description : PMWI (SAPROLITE WELLS)
Collection Date : 2G-Oct-03 14 :00 :00 Site :BURLINGTON Sample Type: MGP SITE Desktop #
OGIP PARAMETERS IN WATER BY GCIMS - 826 0
Test Code : MS8260MGPW Test Method : SW-846 503013/826013 Date Posted :11/03103
Resuft Repoffing Urnk F7ag
Benzene < 0.50 pg1l. 0 .50 PWL 0
Toluene 1 .0 pgtL 1 .0 PA 0
Etbylbenzene < 1 .0 *t 1 .0 PA 0
M-p-Xylene <2.0 pg1L 2.0 pyl- 0
o-Xylene 4 1 .0 VgVL 1 .0 PgA,0
Naphthalene 4 .7 pg/L 2.0 p9k 0
OVOC MGP IN WATER BY GCIMS - 827 0
Test Code :MS8270MGPW Test Method: SW-846 8270C Date Posted : 11/04/03
Resuft gepomng Lknit Flag
Naphthalene < 10 VgIL 10 pqrL 0
2-Methyinaphthelene < 10 pg1L 10 Pg/L 0
Amnaphthylem < 10 pgVL 10 Mt 0
Acenaphthene < 10 pgVL 10 PgVL 0
Dibenzofuran < 10 IKA 10 PWL 0
Fluorene < 10 VCVL 10 WA 0
Phenanthmne < 10 pgVL 10 V71. 0
Anthracene < 10 jig& 10 PA 0
Fluoranthene < 10 pg1L 10 Pg/L 0
Pirrone < 10 pgVL 10 M& 0
Bonzo(a)anthracene < 10 PA 10 PgVL 0
Chrysene < 10 pg(L 10 Pqk a
Benzo(b)fluoranthene < 10 pgtL 10 pg/L 0
Senza(k)fluoranthene < 10 pgVL 10 $XVL 0
Berao(a)pyrene < 10 VA 10 Pgri .0
lndeno(1,2,3~,d)pyrene < 10 pg/L 10 pgL 0
Dibenzo(a,h)anthnscene < 10 pgVL 10 Pg& 0
Benzo(g,h,I)perylone < 10 pgtL 10 *t 0
Visit us on the Int~.Net a tR,,~G,neruud 1115120031400:34 httpJ/de~/essenvfiab~srw/IVe 0 5 q(7
PhDuke Dtike Power Analytical Laborator yOftwer.Phone :704-675,5245 Fax :[phone]
13339HagersFer'Y Road HuntersvilleNC28078-7929
A&Gune Nuclear CompAqx - MG03A 2
Ciertificate of Analysis
New York StaloDeloartmentofHeafth Cartificalkin#ff7f7
Okfahorna 09pailmant of Environmental Quality Certification # 9930
Kansas Department of Health and Environment Certificate # E-fO3f l
North Carolina Depailment of i-bafth &Human Services Cerlificabon It 37804
South Carolina (DHEQ Laboratory ID # 99005 North Carolina (DEIVR Certification #248
SamplelD#:23038630 Job#: 03-OCT-005 3
Sample Description :PMWL-D (SAPROLITE WELLS )
Collection Date : 22-Oct-03 11 :05 :00 Site :BURLINGTON Sample Type: MGP SITE Desktop #
OGP PARAMETERS IN WATER BY GUMS - 8260
Test Code : MS8260MGPW Test Method: SW-846 5030B/8260B Date Posted :11/03/03
Resuft -Reporhng Limit Flag
Benzene < 0 .50 pgt-0.50 VW1 0
Toluene < 1 .0 pg1L 1 .0 pg/L 0
Ethylbenzene < 1 .0 pgtL 1 .0 pgVL 0
~P-Xylene <2.0 tjgVL 2.0 tig/L 0
o-Xylene < 1 .0 PA 1 .0 WA 0
Naphthalene <2.0 jQ1L 2.0 pg/L 0
OVOC MGP IN WATER BY GC/MS - 827 0
Test Code :MS8270MGPW Test Method : SW-846 8270C Date Posted: 11/04/03
nesuft Reponmg Limit Flag
Naphthalene < 10 vWL 10 Pg/L 0
2-Methyinaphthelene < 10 pg1L 10 lig/L 0
Acenaphthylent < 10 pgtL 10 pg& 0
Acenaphthene < 10 pgL 10 pg/L 0
Dibenzolluran < 10 PgI 10 pg1L 0
Fluorene < 10 pgVL 10 Pq(L 0
Phonanthrene < 10 pg1t. 10 Pg(L 0
Anthracene < 10 pg1.10 Pg/L 0
Fluoranthene < 10 tjg&10 pg/L 0
Pyrene < 10 pg'L 10 PgIL 0
Benzo(a)anthracene < 10 pg(L 10 PgL 0
Chrysene < 10 pgtL 10 PA 0
Benzo(b)fluoranthene < 10 pg/L 10 mt 0
Benzo(k)fluoranthene < 10 pgv.10 PA 0
Benzo(a)pymne < 10 pgVL 10 PgVL 0
Indeno(1 .2.3~,d)pyrene < 10 pg/L 10 pgL 0
DIbenzo(a,h)anthracene < 10 pglL 10 P91L 0
Vi.it us on the IntraNet at~,o~G,~rug~11151200314M.34 http://de~/essenv/Iab-s"/Pa,,0 6 .f 7
PkDuke Duke Power Analytical LaboratorydyPower.Phone:[phone] Fax.70$-875,5038
AD-kii.,C",13339 HagersFerly Road Huntetsvilb,NC28078-7929
McGuire Nuclear Compbx - MG03A 2C4ertifiaait4e al PLnaly!sir,
Now York Slate Dsp8HmenIOfHea#hC1art&ab&n #ff7f7Oklahoma Department of Environmental Quali Carlificition#9930Kansas Department ofHealh and Environmen Certificate # E-f03f jNorth Ceroli7a C9partment Of I-b8fth &Human Services Ceilification # 37W4
South Carofiria (DhEQ LaboreloryID # 99005 North Carolina (DBVR Certification #248
Sample ID 0 : 23038630 Job#: 03-OCT-0053
Sample Description:PMWL-D (SAPROLITE WELLS)
Collection Date: 22-Oct-0311 :05 :00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
OVOC MGP IN WATER BY GVMS - 827 0
Test Code :MS8270MGPW Test Method: SW-846 8270C Date Posted: 11/04/03
Resuft _Reporting Limit Flag
Benzo(g,h,I)perylene <10 RA 10 pg1L 0
------------------------------------
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0 isCHAINOF CUSTODY RECURD AND ANALYSIS REQUEST FORM
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"Page ofMail Code MG03A2 (Building 7405) -t- _LlawriEnergy.13339 Hagers Ferry Rd DISTRIBUTION
Huntersville,N. C . 28078 ORIGINAL to LAB,For Detailed Instructions, see :I -V t COPY to C IENThttp:Hdewww/essenv/coc/ (704) 875-524 5.............Faw..(704)~L5-,~q:L .............II)Project Name 2)Phone No :875-5257 nBURLINGTONMGP(SHAL FRACTBR WELLS)
E 3)Client C.Campbell R . Roberts 4)Fax No :875-50320
2=H 3=HI E24=1111 a `t MS)Business Unit : 20018 G)Process : 7)Resp .To :0193 1 !R
0B)Proo tlD : MGPBURL 9)ActlAty M ALLACTV MG03A3TO)M.,l Code-2Customer to Coml2lete all Q_ 0171 _j aporgi2roate No -SHADE12 areas <16 c. -ja----------- 1 8 .5 -614COLABUSEONLY12 Chem Ilection Information 0
E Z"Lab 10 Desktop No .13 Sample Description or ID Data eT z 2 w w 0---FT Signatt P W :E
DMW-1 10 x 1 1 3 1 6
DIVIW-2 It x 1 1 3 1 0 6"1". 0
PMWC-BR to '2-1 103 1035-d14-a x 1 1 3 1 6E3PMWH-BR L 0 Ix--li,103 k4to z- - _.1V x 1 1 3 1 6l__,~~21>1 ;1' OU PMWI-BR to X-1-3 k _3 ;L0 x 1 1 3 1 6
PMWM_BR oil jK j,eIM -X I 1 3 1 pr 6
PMWL-BR X0 I2.a 0 k 005 A &tZ 1
aC- 541r-ll_i~Pm V1 L_ -(L 10 (1705 x Ii.'4 ArkAIV it E1 0
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~Requested TurnaroundRellpq lish B 0,4 i4 Dat rr me vMlciii a 14 Day sar""MmRelincli.E
-7 Days
23)Sea Locked by Daterrime E in w -48Hr"~j~.E,LECTRONICALLY TRANSER THE AN L ,1 .;Commri 3r -,PLEASE HARD COPYA CALI 'Otherk'Add,Cost Will Apply
November 4,2003 1 :59:10 PM Page #1 of I
Duke 8270/625 Analysis
OvEnergy-a-Case Narrativ e
(This document must acoompany rele~se of Analytiml Data)
----------------- - - - - - - --------------- -
ILIMS Job #03-OCT-0054
Workfist #03-OCT-064 2
The percent recovery for the surrogates were outside of the laboratory control limit in
sample 23038636.The results for all analyntes should be considered estimates for
these samples.
------------
Shannon Rollins
-------------------------------------------------------------------------------------
Duke Energy Analytical Laboratory Service s
Environment. Health &Safety Servioes Environmental Center - MG03A2Phone:[phone] Hagers Ferry RoadFAX:704-875-5038 Huntersville NC 28078-7929
SACase N~tiv~\Organic~SVOA\oct-0054 .doc
phoub Duke Power Analytical LaboratoryOpower.Phone: [phone] Fax'704-875-5038
1333,9HagersForly Road HvIlleravifleNC28078-7929
McGuire Nuclear Como/,9x - AfGOJA 2
Coartlflcata of Jkmalysli s
Now York Sloto Goadmant of Hoolth Codification #f f 7 f 7
OWborwDgpartnRntotErwironimniolQuak Carlification#9930
Kansas Department of Heath and Environr=(Carffficala # E-fO3f I
North Carolina Department of ftelth &Human Services Certification # 376N
South Carolina (OfEQ Laboratory ID # 99005 North Carolina (DENR Certification IF 246
Station Name:BURLINGTON Job Number: 03-OCT-0054
Sample ID V 23038631 Desktop #Customer ID :R .ROBERTS
Sample Description: DMW-1 (SRAL FRACT EIR WELLS)
Collection Date: 23-Oct-03 08 :60:00 Date Received in Laboratory: 02-Oct-03 Type of Sample :MGP SITE
Reference Method :EPA310.11SM23208 Data Posted : 1012812003 15:20 :4 7
ALKALINITY (TOTAL INFLECTION POINT)ALKALINITY 0 .87 meg/L
Reference Method : EPA 200 .71601011 Data Posted 1 1/512003 08:20 :5 5
IRON BY ICP (DIGESTED)IRON 2 .584 mg/l
Reference Method :EPA 200 .7/60108 Data Posted :111512003 08:20 :55
MANGANESE BY ICP (DIGESTED)MANGANESE 0.290 mg[L
Reference Method :EPA 300 .0 Data Posted 10124/2003 16 :17 :58
MG-NIL BY CALCULATION N[TRA TE 0 .06 mg-NIL
Reference Method :EPA 300 .0 Date Posted 1012412003 14:42 :59
NITRATE (IC)NITRATE 0.25 mgIL.
Reference Method :EPA 300 .0 Data Posted- 10124/2003 14:42 :5 9
SULFATE (IC)SULFATE 9.97 mg/l.
Sample ID #: 23038632 Desktop S Customer ID :R .ROBERTS
Sample Description : DMW-2 (SHAL FRACT EIR WELLS )
CollectonDate : 21-Oct-0316 :55 :00 Date Received in Laboratory : 02-Oct-03 TypeofSample :MGPSfTE
Reference Method :EPA310.11SM23208 Data Posted 10/2812003 15 :20:47
ALKALINITY (TOTAL INFLECTION POINT)ALKALINITY 4.64 mestfl.
Reference Method:EPA 200.710010B Data Posted :1115/2003 08 :20 :56
IRON BY ICP IDIGESTED)IRON 7 .257 mgn
Reference Method:EPA 20,031601011 Data Posted:11/51200308:20 :56
MANGANESE BY ICP IDIGESTED)MANGANESE 6 .923 mqll.
Reference Method :EPA 300 .0 Data Posted : 10124rM3 16:24 :0 8
MG-WL BY CALCULATION NfrRA TE <0 .02 ma-1111.
Reference Method :EPA 300 .0 Data Posted : 1012412DO3 13 :29 :48
NITRATE 11C)NITRATE <0.10 mg1l.
Reference Method :EPA 300 .0 Data Posted : 1012,V2003 13 :29:4 8
SULFATE (IC)SULFATE < 0.10 mgfL
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phpuke Duke Power Analytical Laboratory
aPower.Phone:[phone] Fax.70$-875-5038
13339 Hagers Ferry Road Huntemid0a,NC 28078-7929
McGuire Nuclear Complex - MG03A 2
Cart1ficata 4or Ainaiysir,
Now York Stoic Doporiment of Hoofth Cortification If f f 7f 7OklahoflwDepartimnlofEnvironrwntelOuak Cafficalion#9930
Kansas Department ofHeath and EnvininnnimiNCarlificale #E-f03f f
North Carolina Department of lbafth &Human Services Certification # 378M
South Carolina (DhFQ Laboratory ID # 99005 North Cgrolina (DBVI :o Certification #248
Station Name :BURLINGTON Job Number. 03-OCT-0054
Sample ID V 23038633 Desktop 0 Customer ID :R .ROBERTS
Sample Description : PMWC-BR (SHAL FIRACT BR WELLS)
CollectionDate: 21-Oct-0310:35:00 Date Received in LaboraW. 02-Oct-03 TypeofSarnple :MGPSrTE
Reference Method :EPA310 .11SM2320B Data Posted :1012812003 15 :20 47
ALKALINITY (TOTAL INFLECTION POINT) 0 ALKALINITY 4 .27 meqLL
Reference Method :EPA 200 .71601013 Data Posted :111512003 08 :20 56
IRON BY ICP (DIGESTED)IRON 14 .543 mall
Reference Method:EPA 200 .7/60108 Data Posted :11/5/2003 08 20 57
MANGANESE BY ICIP (DIGESTED)MANGANESE 3.733 malL.
Reference Method :EPA 3DO .0 Data Posted : 10124/2DO3 16 :24 :08
MG-MIL BY CALCULATION NITRATE <0.02 mg-NIL
Reference Method :EPA 300 .0 Data P05ted, 10124/2003 13 30,35
NITRATE (IC)NrrRATE < 0.10 irmilL
Reference Method EPA 3DO.0 Data Posted : 1012412OD3 13:30 :35
SULFATE (IC)SULFA TE 1 .28 ma/L
Sample ID 9 : 23038634 Desktop 0 Customer ID :R .ROBEIRTS
Sample Description : PMWH-BR (SHAL FRACT BIR WELLS )
Collection Date : 22-00-03 16 :10:00 Date Received in Laboratory: 02-Oct-03 Type at Sample :IAGP SITE
Reference Method :EPA310 .11SM2320B Date Posted :10/2W003 15:20:4 7
ALKALINITY (TOTAL INFLECTION POINT)ALKALINrrY 4 .09 meg/L
Reference Method : EPA 2DO.71601013 Data Posted :11151200 08 :20 :5 7
IRON BY ICIP (DIGESTED)IRON 4.722 man
Reference Method :EPA 200.715010B Data Posted :11151200308 :20 :57
MANGANESE 13Y ICP (DIGESTED)MANGANESE 4 .023 mg/L
Reference Method :EPA 300 .0 Data Posted : 10124/2003 16:17:5 9
MG-NIL BY CALCULATION NfTRATE <0 .02 mg-NIL
Reference Method:EPA 300 .0 Data Posted- 1012V2003 14 43 :38
NITRATE (IC)NITRATE < 0 .10 mg/l .
Reference Method :EPA 300.0 Date Posted: 1012412003 14 :43 :38
SULFATE (IC SULFATE 114A ..n
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*Duke Mike Power Analytical Lal)orator yPower.Phone:[phone] Fax 704-675M38
AD.k&,VG~13339 HagerS Ferry Road Huntelaville,NC 28078-7929
McGuire IVucteaf COMPOX - MG03A 2
coaritiricat4e 4or Annaiysus
Now York Stoic Doparlmont of Hoolth Coriftation it ff7f7Oklahoma Department of Environmental Qua# Carlification#9930
Kansas Department ofHealh and EnvironmeNerificale #E-fO3f f
North Carolina Deloarinient of l1balth &Hurmn Services Certification # 378N
South Carolina (01-~Laboratory ID # 99005 North Carolina (1)60~ Codification #240
Station Name :BURLINGTON Job Number : 03-OCT-0054
Sample ID U 23038635 Dasktop #Customer ID :R .ROBERTS
Sample Description : PMWI-BR (SHAL FRACT EIR WELLS)
Collection Date: 20-Oct-03 13 :20 :00 Date Recehed in Laboratory. 02-Oct-03 TypeofSample :MGPSITE
Reference Method:EPA310 .11SM2320B Data Posted:10/28/2003 15 :20:47
ALKALINITY (TOTAL INFLECTION POINT)ALKALPVrrY 5.33 meg/L.
Reference Method :EPA 200 .7160108 Data Posted :11151200308 :20:58
IRON BY ICP JOIGESTED)IRON 2 .682 mail
Reference Method :EPA 200.7180108 Data Posted :111512DO308 :20:58
MANGANESE BY ICP (DIGESTED)MANGANESE 3.977 mail.
Reference Method EPA 300.0 Data Posted : 10/2412003 09 :00:03
MG-NIL BY CALCULATION NrIRATE <0.02 mg-NIL
Reference Method EPA 300 .0 Data Posted :10/23/2003 11 :49 :38
NITRATE (IC)NfTRATE < 0 .10 mg/L
Reference Method :EPA 300 .0 Data Posted:10/23/2003 11 :49 :38
SULFATE (IC)SULFATE 10 .63 mall.
Sample ID V 23038636 Desktop #Customer ID :R .ROBERTS
Sample oescripitkin : PMVAIN-BR (SHAL FRACT BR WELLS )
CollectionDate : 20-Oct-0311 :10 :00 Date Recahimed m Laboratory,02-Od-03 Typ8ofSample :MGPSITE
Reference Method:EPA310.1/SM2320B Data Posted:1 D/28r2003 15:20 :47
ALKALINrrY (TOTAL INFLECTION POINT)ALKALWrrY 1 .15 meg/l.
Reference Method :EPA 200 .715010B Date Posted :1115/200308 :20 :58
IRON BY ICP (INGESTED)IRON 1 .432 mg/I
Reference Method :EPA 200.71001013 Data Posted :1115/2003 08 :20:58
MANGANESE BY ICIP (DIGESTED)MANGANESE 1 .043 mg/L
Reference Method :EPA 300.0 Data Posted : 1012412003 09:DD :04
MG-NIL BY CALCULATION NTTRA TE 0.41 mg-NIL.
Reference Method:EPA 300 .0 Data Posted :10/2312003 11 :50:38
NITRATE (IC)NITRATE 1 .82 mg/l.
Reference Method:EPA 300 .0 Data Posted : 10/23rl00311 :50:38
SULFATE (IC)SULFATE 25 .92 mglL
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PhDub Duke Power Analytical Laboratory
arpowff.Phone:[phone] Fax:70$-875-5036
A D.& 15~Q.P-1 1333QHagefsForly Road HunlarevilleNC28078-7929
McGufte Nuclear Comptex - MG03A2
cartimi-ata col J%malysi s
Now York Stoic Doportmord of Hoofth Cortficotion V f f 717Oklahoma Daparlmentof EnvitonnigntalQuak Gartification#9930
Kansas DoWment of Heath and EnvironmenMarlificale #E-f03f l
North Carolina Department of Health &Human SeNices Ceffification N 378N
South Camlina (DFEq Laboratory ID # 99005 North Carolina (DBVR Certification #248
Station Name :BURLINGTON Job Number. 03-OCT-0054
Sample ID IF : 23038637 Desktop #Customer ID:R .ROBERTS
Sample Description : PMWL-BR (SHAL FRACT BR VVELLS)
Collection Date: 22-00.03 10 :05:00 Date Recented in Laboratory: 02-Oct-03 TypeofSample :MGPSITE
Refer"m Method:EPA310.11SM2320B Data Posted :1012812003 15:20 :47
ALKALINITY (TOTAL INFLECTION POINT)ALKALWFFY 2.59 meqlL
Refentrim Method:EPA 200.7160108 Data Posted :111512003 08:20 :59
IRON BY ICP (DIGESTED)IRON 0 .334 mg/I
Refererim Method: EPA 2DO .71601013 DataPosted : 11/5t200308 :20 :59
MANGANESE BY ICP fDIGESTED)MANGANESE 0.339 malL.
Referenm Method :EPA 300 .0 Data Posted: 10/2412003 16 :18 :DO
MG-N/L BY CALCULATION NITRATE <0.02 mg-kiL
Referenm Method :EPA 300 .0 Data Posted : 10124/2003 14:44 :09
NITRATE (C)NITRA TE < 0.10 mg/L.
Referenm Method :EPA 300.0 Data Posted : IOJ2412DO314:44 :09
SULFATE (IC)SULFATE 16 .59 man.
11014,610 OWAPPID~BY,D~
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ReportGenemied IIIJ1200314:11:24 http ://dc~/essertv/lab-srv/M~ge ~-4 ~j 4
P guile VUKe Fower Anaiyucal LaDorator yoftwer.Phone .[phone] Fax :[phone]
A D~ 1~G~M 13339 HagersFerty Road HUntersvilleNC26078-7929
McGuire Nuclear Complex - MG03A 2
Cartlfl4aata af Anaiysis
New York State Department of Health Certification #I f 717Oklahoma Department of Environmental Quefity Certification # 9930Kansas Department of Health and Environment Certificate # E- 103f INorth Carolina Department of fbalth &Human Services Certification # 37804
South Carolina (DHEQ Laboratory ID # 99W5 North Carolina (DEIVF~ Certification #248
SamplelD#:23038631 Job *:03-OCT-005 4
Sample Description :DMW-1 (SHALFRACTBR WELLS )
Collection Date : 23-Oct-03 08 :50 :00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
IMGP PARAMETERS IN WATER BY GC/MS - 8260
Test Code : MS8260MGPW Test Method : SW-846 50308/8260B Date Posted :11/03/03
Result Reporting Limit Flag
Benzene < 0.50 pg/L 0.50 pgr- 0
Toluene < 1 .0 uglL 1 .0 Pg/L 0
Ethylbenzene < 1 .0 VglL 1 .0 PqlL 0
rn-p-Xylene <2 .0 pg(L 2 .0 pg/L 0
o-Xylene < 1 .0 pg/L 1 .0 Pg/L a
Naphthalene <2 .0 pg/L 2 .0 pgfL 0
'SVOC MGP IN WATER BY GC/MS - 827 0
Test Code: MS8270MGPW Test Method : SW-846 8270C Date Posted: 11/04/03
Result Reporting Limit F7ag
Naphthalene < 10 pVL 10 Pg/L 0
2-Methyinaphthelene < 10 pg/L 10 PglL 0
Acenaphthylene < 10 pglL 10 Vg/L 0
Acenaphthene < 10 pg(L 10 PgVL 0
Dibenzofuran < 10 pelt. 10 Pg(L 0
Fluoreno < 10 pg1L 10 Pg/L 0
Phenanthrene < 10 pgfL 10 Pg/L 0
Anthracene < 10 Vg/L 10 pgfL 0
Fluoranthene < 10 pgr- 10 pgtL 0
Pyrene < 10 pg/L 10 Pg1L 0
Benzo(a)anthracene < 10 Vg/L 10 Pg/L 0
Chrysene < 10 pq1L 10 Pg/L 0
Bamo(b)fluoranthene < 10 pg/L 10 P91 0
Benzo(k)tluoranthene < 10 pg/L 10 pg/L 0
Bertzo(a)pyrene < 10 pg/L 10 Pg/L 0
Indeno(1,2,3-c,d)pyrene < to pgfL 10 Pg/L 0
Dibenzo(a,h)anthracene < 10 pg/L 10 Pg(L 0
Benzo(g,hJ)parylene < 10 Vg/L 10 Pg/L 0
Visit us on the IntraNet atR~oHG~nemted 1115120313:59:M Ittip1lde~w/essenvilab-srv/P-g, N I (S
MUKe VUKe rowerAnaiyucal LaDora-uor yPower.Phone [phone] Fax [phone]
A~E~Tc~y 13339 Hag e(S Ferry Road HuntersviliaNC28078-7929
McGuire Nuclear CompLex - MG03A 2
Cartiri4cata= al Analysis*
New York State Department of Health Certification #I f 717Oklahoma Department of Environmental Quality Certification # 9930
Kansas Department of Hea#h and Environment Certificate # E-103 I tisNorth Carolina Department of H991th &Human Sennces Cerfificalion # 37804
South Carolina (DHEQ Laboratory ID # 99005 North Carolina (DBNF~Certification #248
Sample ID#:23038632 Job #:03-OCT-0054
Sample Description :DMW-2 (SHAL FRACT BR WELLS)
Collection Date : 21-Oct-03 16 :55 :00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
~MGP PARAMETERS IN WATER BY GC/MS - 826 0
Test Code : MS8260MGPW Test Method: SW-846 5030B/8260B Date Posted :11103/03
Result Reporting Limit Rag
Benzene 43 pg/L S .0 pg/L 0
Toluene < 10 pg(L 10 Vg/L 0
Ethylbenzene 61 pg/L 10 Pgr. 0
rn-p-Xylene 20 pg/L 20 pg/L 0
~Xylene 19 pgr- 10 pgfL 0
Naphthalene 580 Vg1l.20 pgfL 0
SVCC MGP IN WATER BY GC/MS - 827 0
Test Code :MS8270MGPW Test Method : SW-846 8270C Date Posted : 11/04/03
Result Reporting Limit Flag
Naphthalene 2000 VWL 1000 pg(L 0
2-Mothyinaphthalene 680 pg/L 100 ug/L 0
Acenaphthylene < 10 pg(L 10 Vq/L 0
Acenaphthene 400 pgfL 100 pgtL 0
Dibenzofuran 35 pg1L 10 pgVL 0
Fluorene 93 Vg(L 10 VgIL 0
Phenanthrene 83 Vg/L 10 pg(L a
Anthracene 16 pg/L 10 pg/L 0
Fluoranthene < 10 pgfL 10 Vg(L 0
Pyrene < 10 pg(L 10 pgr- 0
Benzo(s)anthracene < 10 pgVL 10 pg/L 0
Chrysene < 10 pg/L 10 pg/L 0
Bemo(b)fluoranthene < 10 pg(L 10 pg/L 0
Benzo(k)fluoranthene < 10 pg/L 10 pg/L 0
Semo(a)pyrene < 10 pg(L 10 pg/L 0
lndeno(1,2,3.c,d)pyrene < 10 pgtL 10 pq/L 0
Dibemo(a,h)anthracene < 10 pg/L 10 pg/L 0
Benzo(g,h,i)peryiene < 10 pg1L 10 Pg/L 0
Visit us on the IntraNot a tR~oH~nemted 11151YW313:59:0 http :flde~w/essenv/labs~/Pqg,#2~f8
p VUKe V U Ke rower Anaiyucal LaDoraioryarPower.Phone [phone] Fax, 704-a75-5038
A A.4 E~g G-i-T 13339 Hag ers Ferry Road HuntelsvilleNC28078-7929
McGuire Nuclear Compkax - MG03A 2Coertific:ato af Aftnalysi s
Now York State Department of Health Certification #I f 7 f 7Oklahon)aDepantmntofErmironrmntafQuali Carlificabor?#9930
Kansas Department of Health and Enviro Certificate # E-1031 iNorth Carolina Dgliartment of H4afth &Human Services Certification # 37804
South Carolina (DHEQ Laboratory ID # 99X5 North Carolina (DENR Certification #248
Samplell)#:23038633 Job#: 03-OCT-005 4
Sample Description:PMWC-BR (SHAL FRACT BR WELLS )
Collection Date: 211-Oct-03 10 :36:00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
OGP PARAMETERS IN WATER BY GC/MS - 826 0
Test Code : MS8260MGPW Test Method : SW-846 503013/826019 Date Posted :11/03103
Result -Reporting Limit Fla g
Benzene 6.1 pg/L 1 .0 pg/L 0
Toluene 3.2 pg/L 2 .0 pg/L 0
Ethylbenzene 13 Pen.2 .0 pgfL 0
nt-p~Xyleno 8 .4 pgVL 4 .0 pgfL 0
o-Xylene 11 P9/L 2.0 pg/L 0
Naphthalene 380 pg/L 4.0 p(YL 0
'~VOC MGP IN WATER BY GC/MS - 8270
Test Code :MS8270MGPW Test Method :SW-8468270C Date Posted: 11/04103
Result Reportog Limit Flag
Naphthalene 320 pglL 100 PgA-0
2-Mothylnaphthalene 120 pg(L 10 PGVL 0
Acenaphthylene 27 PWL 10 PgVL 0
Acenaphthene 290 PgfL 100 PgIL a
Dibenzofuran 29 P91L 10 PgVL 0
Fluorene 85 pg/L 10 WgIL 0
Phenanthrene 84 pgVL 10 Pell-0
Anthnscene 17 pg/L 10 Pg/L 0
Fluoranthene < 10 PgIL 10 PglL 0
Pytene < 10 PsVL 10 PgVL 0
Bemo(a)anthracene < 10 p9l. 10 Pg/L 0
Chrysene 10 PGVL 10 Vg/L 0
Benzo(b)fluoranthene < 10 PgIL 10 PgAIL 0
Benzo(k)fluomnthene < 10 pelt. 10 pg/L 0
Benzo(a)pyrene < 10 Pg/L 10 Well-0
lndeno(11,2,3~,d)pyrene < 10 pg/L 10 Pg/L 0
Dibenzo(a,h)anthracene < 10 pg/L 10 PglL 0
Benro(g,h,QperyIene < 10 Ijg/L 10 Pg/L 0
Visit us o. th . lnt~Net atR,~H C,,~Ud 111512003 13 59 08 http ://de~/essenvAab-srv/P-g, 03 .fB
P guile VUKe rowerAnaiyueal LaDoratoryaPower.Phone [phone] Fax:[phone]
A D~61V G~13339HegersFerlyPoed HuntersvillePVC26078-7929
McGuire Nuclear Complex - MG03A 2
Cartif icat4e at Aftnaiysi-s
New York Slate Department of Health Ceriffration # I Y 717Oklahoma Depailment of Environmental Quality Certification # 9930Kansas Department of Health and Environment Certificate #E.103f f
North Carolina Department of Health &Human Services Cerlification # 37804South Carolina (DHEQ Laboratory ID # 99005 North Carolina (Dav;~Cerfificabon #248
SamplelD#:23038634 Job #:03-OCT-0054
Sample Description:PMWH-BR (SHALFRACT EIR WELLS )
Collection Date : 22-Oct-03 16 :10 :00 Site :BURLINGTON Sample Type : MGP SITE Desktop if
MGP PARAMETERS IN WATER BY GC/MS - 826 0
Test Code: MS8260MGPW Test Method: SW-846 503OB/8260B DatePosted : 11/o4lo3
Resuft -Repornng Limit Flag
Benzene 4 .0 VgIL 2 .5 gg/L 0
Toluene < 5 .0 pg/L 5 .0 Vg/L 0
Ethylbenzene 26 pg1l. 5 .0 pg/L 0
m.p.Xylano 16 pg1L 10 PWL 0
o.Xylene 13 pg/L S.0 POIL 0
Naphthalene 730 pg/L 10 PgVL 0
SVOC MGP IN WATER BY GCIMS - 8270
Test Code: MS8270MGPW Test Method : SW-846 8270C Date Posted : 11/04/03
Result Repoffing Limit Flag
Naphthalene 1100 pg/L 100 Pell-0
2-Mathylnaphthalene 410 pg/l. 100 ptitt.0
Acenaphthylene < 10 pg/L 10 Pg/L 0
Acenaphthene 340 pg(L 100 PgVL 0
Dibenzoluran 34 pg/L 10 pg/L 0
Fluorene 79 pg(L 10 Plitt, 0
Phenanthreno 94 pg/L lo Pelt 0
Anthnicene 18 pg/l. 10 Pg1L 0
Fluoranthene < 10 pg/L 10 Pg1l,0
Pynane < 10 pg/L 10 VA 0
Bomo(a)anthracene < 10 PA 10 P91L 0
Chrysens < 10 pg/L 10 VgIL 0
13emo(b)fluoranthene < 10 pg/L 10 Pg/L 0
Benzo(k)fluonanthene < 10 pg(L 10 P91L 0
Bemo(a)pyrene < 10 pg/L 10 Pg/L 0
Indeno(1,2,3-c,d)pyrene < 10 pgfL 10 PgIL 0
Dibenzo(a,h)anthracene < 10 pg/L 10 PGVL 0
Benzo(g .hJ)perylone < 10 pgtL 10 jig/L 0
0
Visit us on the l.t,aNet a tR,~H G ..olld 11151200313 .59,08 http://de~/essenv/1ab-s"/P-R,N 4 (8
P Duke JUUKeFowerAnaiyucal LaDoratoy yNower.Phone:[phone] Fox 704-875-5038
A ~ 6-0 G~ 13339 Hagers Perry Road Huntersville,NC26078-7929
McGuire Nuclear Complax - MG03A 2
Cartificat4e cif Aknaiysis,
New York State Dwartment of Health Certification # 11717Okfahome Department of Environmental Quality Cerifkabon # 9930Kansas DepartrTeril of Heagh and Environment Certificale # E-fO3f INorth Carolina Department of i Agalth &Human Services Certification # 3780 4
South Carolina (DHEC)Laboratory ID # 99005 North Carolina (DENR Certification #248
SamplelD#:23038635 jot)#:03-OCT-0054
Sample Description:PMWI-BR (SHAL FRACTBR WELLS )
Collection Date : 20-00-03 13 :20:00 Site :BURLINGTON Sample Type : MGP SITE Desktop If
IMGP PARAMETERS IN WATER BY GUMS - 8260
Test Code : MS8260MGPW Test Method : SW-846 5030B/8260B Date Posted :11/03103
Result RgpqqvU Limit Flag
Bemene 89 Vg/l. 5 .0 pvt 0
Toluene < 10 PA 10 Pg/L 0
Ethylbenzene 95 pg/L 10 PgA. 0
m-p-Xylene 20 pgr-20 pgVL 0
~Xyiene 38 pg/L 10 P91L 0
Naphthalene 390 Pg/L 20 pg/L 0
SVOC IMGP IN WATER BY GUMS - 8270
Test Code :MS8270MGPW Test Method ; SW-846 8270C DatePosted : iitto4fQ3
Result Reportng Limit F7ag
Naphthalene 1500 Pail-1000 pg/L 0
2-Methylnaphthatene 44 pgr. 10 lig/L 0
Acenaphthylene 25 pg/L 10 pg/L 0
Acenaphthene 79 pg/L 10 pg/L 0
Dibenzofuran 13 p9r. 10 pgVL 0
Fluorene < 10 PgA . 10 pg/i.0
Phananthrene 24 pg/L 10 WgIL 0
Anthracene < 10 pgr- 10 PgA, 0
Fluotanthene < 10 pgll- 10 vg/L 0
Pimme < 10 pg/L 10 pg/l. 0
Bemo(a)anthracene < IQ P911.10 pgA. 0
Chrysene < 10 pg/L 10 pg/L 0
Bemo(b)fluoranthene < 10 pgVL 10 PgVL 0
Benzo(k)fluoranthene < 10 PgA . 10 PgVL 0
Bewo(a)pyrene < 10 p9A . 10 pg(L 0
lndeno(1,2,3~,d)pyrene < 10 Poll-10 Pgli. 0
Dibenzo(a,h)anthracene < 10 pg/L 10 pgVL 0
Berueo(g .hJ)perylene 10 PgA. 10 PgA, 0
0
Visit us on the IntraNet a tR,,vH G~1~1,alld 111512003 13 59 08 hap1lde~/essenv/lab-s~/pag, # 5 r8
PhDuke Duke Fower Analytical LaboratoryOftwer.Phone :[phone] Fax. 704-875-r,03 6
13339 HagersFerrl Road Huntersville,NC28078-7929
McGuire Nuclear Compfiqx - MG03A 2
Cartificato at fflinalysis
Now York State Deparltnent of Health Certification # 11717
Oklahoma Department of Enwronmental Qua# Ceifificalion#9930
Kansas Deparfmaml of Health and EnvironmenMerlificale # E403f f
North Carolina Department of ttalth &Human Services Certification # 378N
South Carolina (DHEQ Laboratory ID # 99005 Ncv1h Carolina (DaR Certification If 248
Sample ID #: 23038636 Job V 03-OCT-0054
Sample Description :PMWM-BR(SHALFRACT BR WELLS )
Collection Date: 20-Oct-D3 11 :10:00 Site :BURLINGTON Sample Type: MGP SITE Desktop #
IMGP PARAMETERS IN WATER BY GC/MS - 826 0
Test Code: MS8260MGPW Test Method : SW-846 50308/8260B Date Posted :11/03/03
Result Reporting Limit Flaq
Benzene < 0 .50 pgr . 0.50 pgVL 0
Toluene 1 .0 pg/L- 1.0 PgIL 0
Ethylbenzene 2 .3 pg/L 1 .0 pg(L 0
~p-Xylone 7 .2 pg/L 2.0 pg/L 0
~Xyleno 3 .6 pgtL 1 .0 Pq(I.0
Naphthalene 200 pg1L 10 PGA.0
SVOC MGP IN WATER BY GCIMS - 827 0
Test Code :MS8270MGPW Test Method : SW-846 8270C Date Posted : 11/04103
Res.1t Reporting Urnif Flag
0 Naphthalene 120 pg(L 10 PGVL 1
2-Methyinaphthalone 99 pgr . 10 vg/L I
Acenaphthylone 28 pg/L 10 Pg/L 1
Acenaphthene 17 p9A. 10 PgAIL I
Dibenzofuran < 10 Von. 10 PgA,I
Fluorene 26 pg/L 10 VgIL I
Phananthrene 33 p9t 10 Pg1l. I
Anthracene < 10 pgA- 10 pq(I.
Fluoranthene < 10 Vgr- 10 PgA.
Pyrene 10 pg/L 10 pg/L I
Bemo(a)anthracene < 10 pqll .10 pqA .
Chrysene < 10 pgr, 10 pg/L
Benzo(b)fluoranthene < 10 pg/L 10 pg1L I
Benzo(k)ftuoranthene < 10 pgA. 10 PGVL
Bemo(a)pyrene < 10 VgIL 10 VA
lndeno(1,2,3~,d)pyrene < 10 pgVL 10 pgtL
Dibemo(a,h)anthracene < 10 pg/L 10 PGVL
Benzo(g,hJ)perylene < 10 VgIL 10 PWL 1
0
Vi .it ~s an the I.tr&Net a tR,~n Gneeakd 111512003 13 59,98 httlaWde~/essenvAab s"I pa,16,(8
P,kDuke VuKe Flower Analytical LaDorator yPower.Phone .[phone] Fax 704-875,5038
13339 Hag ers Fer/y Road HUntetSville,NC28078-7929
McGune Nuclear Complex - MG03A2
Cartifl4cat4e of Ammaiysi s
Now York Slate Department of Health Certilration # f 1717
Oklahoma Department of Environmental Quality, Certification # 9930Kansas Department of Heath and Environment Certificate # E-f031 f
North Carolina Department of ftalth &Hurnan Services Certification #37W4
South Carolina (DHEQ Laboratory ID # 99005 North Carolina (D6NR Certification #248
Sample]D#:23038637 Job #:03-OCT-005 4
Sample Description:PMWL-BR (SHAL FRACT BR WELLS )
Collection Date: 22-W-03 10 :05:00 Site ;BURLINGTON Sample Type : MGP SITE Desktop #
IMGP PARAMETERS IN WATER BY GCIMS - 826 0
Test Code: MS8260MGPW Test Method: SW-846 503013/8260B Date Posted :11/03/03
Result -ReportIng Limit Rag
Benzene < 0 .60 VglL 0.50 pgfL 0
Toluene < 1 .0 pg(L 1 .0 Ijg/L 0
Ethylbemene < 1 .0 pgVL 1 .0 PgrL 0
m-p-Xyleno <2.0 pgVL 2 .0 pglL 0
~Xylene < 1 .0 pgA. 1 .0 Pg/L 0
Naphthalene <2.0 pg/L 2 .0 pg/L 0
SVOC MGP IN WATER BY GCIMS - 8270
Test Code : MS8270MGPW Test method : SW-846 8270C DatePosted : 11/o4ja3
Resuft Reporting Limit Flag
Naphthalene < 10 pglL 10 PglL 0
2-Mothytnaphthalem < 10 Vg/L 10 pg/L 0
Acenaphthylene < 10 pg(L 10 Vg/L 0
Acenaphthene 10 pgVL 10 pg/L 0
Ditsenofuran < 10 pg/L 10 VqfL 0
Fluorene < 10 VgVL 10 PgVL 0
Phenanthrene < 10 pg1L 10 Pg/L 0
Anthracene < 10 pgVL 10 pg/L 0
Fluoranthene < 10 pg/L 10 ;jgtL 0
Pmene < 10 pg/L 10 pgA- 0
Bemo(a)anthracene < 10 pglL 10 pg/L 0
Chrysene 10 Vg/L 10 jigIL 0
Bemo(lsffluoranthene < 10 pg/L 10 pg/L 0
Benzo(k)fluoranthene < 10 VgIL 10 PVL 0
Beruto(a)pyrene < 10 VgIL 10 pglL 0
lndeno(1,2,3~,d)pyrona < 10 pg/L 10 P911-0
Dibenzo(a,h)anthracene < 10 poll. 10 Pg1L 0
Visit us on the IntraNet a tRe,on Generated 111512003 1339:08 httpJ/de~/essenvRab srv/Psg~N 7 .f 8
PhDake VUKeFowerAnaiytical LaDoratoy y
Oftwer.Phone 70$-875-5245 Fax [phone]
1333,9HagersFeny Road HuntersvilleNC28078-7929
McGuire Nuclear COMPlex - MG03A 2
Cartificat4e cof Axnalysis
New York State Department of Health 05riffication # ff7f7
Oklahoma Deperlment of Environmental QuaMy Certification # 9930
Kansas Department of Health and Environment Certificate # E-103f f
North Carolina Department of l-bafth &Human Services Certification #37804
South Carolina (DHEQ Laboratory ID # 99005 North Carolina (060~ Certification #248
SampleID#:23038637 Job #:03-OCT-005 4
Sample Description :PMWL-BR (SHALFRACTBR WELLS )
Collection Date : 22-Oct-0310:05 :00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
,SVOC MGP IN WATER BY GC/MS - 827 0
Test Code :MS8270MGPW Test Method : SW-846 8270C DatePosled : 111(W03
Resuft Reporting Urnit Rag
Sama(g,h,I)perylene < 10 pg1L 10 PgIL 0
------------------------------------
Descrijpti4= cA Flacts :
0 - ~U ~W~ocml Procc~re Ree~nreeoetn . Wete Met
I - See C...
2 -E .irnea.d
3 R,.vt M-ettd ~. I- lal-fficieot --,I-
4 Ret,on Um,t Meented ~c W r*W,red anidyttcal &1utso n
5 S-pl .Rerun .Sit-ld Net Be U ..d F- P-p....(See C ...
A .W". det ....4 bl .- teb...u '.P*r4e~luni,ed-at.d
R .,
."
.d -.-traoi .... fl~.c-bi ...E enete 1h.eee ee .dee .
C)r
Rspoftd By. Date
Vi.it to,on the ItraNet a t
R,,on G~.,.Ied 11151200 13.59 M http ://de~/essenvAab srv/Page N 8 ofs
Burlington MGP
January 2004 Groundwate r
Field Analytical Data
Field Calibration Forms
Groundwater Monitoring Data Sheet s
Chain Of Custody Records
Laboratory Analytical Data
Burlington MNA Proposal Appendix B
BURLINGTON OPERATIONS CENTER -MGP SITE
GROUNDWATER MONITORING FIELD DATA
SAPROLITE WELLS
AVGWELL DEPTH TO PROD PUMP WELL EVAC WELL EVAC SPECIFI CWELL DEPTH WATER LEVEL RATE -VOL VOL VOL VOL EVAC TEMP PH CONDUCTANCE DO ORP TUBBDATE NO.(f,,t)(fann)(r"t) ODOR (nni/min)B Bj~Lll)9~)(unita)L LL9!)Dad..)(dag C) (.V) (NTU)?MWB-D 18 8 .34 NONE NONE 51 R=
75 60 0,6
12 .5,12 .8.12 .8 6 .7 .6 .7,6 .7 (u "ag")112112004 70,
No
3733~3~68CF'l 0.23 .437.0.21 165,158 .156 3 .6,3 .7.3 .8U2012004PMWC-D LF 25 .20 15.55 NONE MINOR 62 5~96 3 .10 1 .57 082 NO 15, 1 ~15.2.14 .7 6 .9. 6,9. 6 .9 512,514,514 0,18,0,17 .0.15 103,98 .95 1 .9,2 .1 .1 .91/2012OD4 PMWC-D 25 .20 15.55 NONE MINOR 62 5~% 6 .90 1 .57 1 .82 NO 13 .7,13,8.13 .7 6 .8 .6 .8.6 .8 53 1 ~534 .534 0.26,0.17,0.17 74 .73,69 1 .6,1 .9,1 .61f2WOD4 PMWF-D 16 .32 8 .59 NONE NONE 94 4,77 4 .40 1 .26 1 16 YES 15 .5 . 15 4.15 .3 6 .9, 6 .9, 6 .9 933.928,928 0.21L 0 .26 . 0.30 NOTE 1 3 .3.19,551119/2OD4 PMWG-D 1907 9 .58 NONE NONE 100 5~86 4 .75 1 .55 1 .25 NO 14 .3, 14 .1 .13 .8 6 .2,6 .2. 6 .2 433,459,457 0.32,0,34,0.33 NOTE 1 2 .6. 1 9,2 .2111912004PMWI 16 .12 11 .39 NONE NONE 27 .5 2 .92 1 .00 0.77 0 .26 NO 12 .4,11,6.11 .3 7 .0,7A 7 .0 364,365,366 2A .2,0,1 .9 237 .245,240 7 .0.3 .6,3 .21121f2004 PMWL-D 9,70 4 .47 NONE NONE 36 3 .23 1 50 0.85 0 .40 NO 9 .8,9.4,11 .3 6 .5 . 6,6,6 .5 354,354,352 4 .2 .41A 3 .7 NOTE 1 7 .5.5 .7,5 .3
NOTE I -ORP Probe malfunction (no, c.,aned )
OVERBURDEN WELLS
AVG
WELL DEPTH TO PROD PUMP WELL EVAC WELL EVAC SPECIFICWELLDEPTHWATER LEVEL RATE -VOL VOL VOL VOL EVAC TEMP pH CONDUCTANCE DO ORP TURBDATE NO.Tect) (reet) (Ifeet) ODOR Dral/mi.)(.V) (NTU)112laOD4 MW 11 .67 -M NE-N o1ca-!227 .)00(LIF 16) LiONE 97 if r) 4'U!no)dcg u'3
22 .24 5 .29 2 .40 IALO)LORV) N~O I S4, 1-6 . C116.0 5 .r(,5377 1 ;!97±120-1 1)' 0.29,40 17 NOTE 1 18,13,t4Ia(v2004 MW-5 13 .54 678 NONE NONE 30 4 .17 1 .50 1 .10 0,40 NO 103, 11 . 1 .1 1 .3 7 .1, 7A, 7 .1 839,837.837 0,31 . 0 .30 0.29 NOTE 1 20,20,191f2l/2004 MW-9 9 .50 642 NONE NONE 40 1 .90 240 0,50 0,63 NO 6 .6. 63, 63 6 .6.6A,6 .6 ~5, 661 . 662 1 ~4 .1 4 .1 .3 288 .281 .276 2,9.3 .0.2 .81/21/2004 PMWB 5 13 .58 8,37 NONE NONE 50 3 .22 1 10 0,85 0,32 NO 10,6,10 8.11 .4 7A, 7.1, 7 .1 834,828,830 0,31 . 0 22,0.19 78,78,77 4 .1,3 .9.2 .9112WO04 PMWC-S-LF 21,09 1 3,08 NONE NONE 53 4 .94 3 .65 1 . 3 t O~96 NO 9 .4,93,9.8 7 .0,7.0,7 .0 486,490.494 0 .21,0.19 . 0.16 36,35.31 5 .6.4 .4,3 .8lf20/2004 PMWC-S 21 .09 13 .08 NONE NONE 168 4 .94 10,45 1 .31 2 .76 NO 13 .&13 .8,14 .2 6 .9,7.0,7~O 472,485.484 0 .14,0 .15 .0,13 22,18,16 5 .2.3 .8,3 .6U20/2004 PMWC-S-CONV 21,09 13 .08 NONE NONE 1045 4 .94 3813 L31 10,26 NO 18 .0.19 .0.17 .7 7 .0. 7.0,7 .0 497.517.521 0,10,0,07 . 0.07 6,6,5 ;6,9.14V2012004 PMWL-S 7 .60 3 .23 NONE NONE 30 2 .70 1 .80 0.71 0 .48 NO 9 .6.8 .7, 8.5 6 .6, 6.6. 6 .6 535,541,539 0,22. 0.21, 0 .21 NOTE 1 1 .7 .1 .7,L51119a~PMWM-S 12 .68 11 .38 NONE NONE 54 0 .80 2 .20 0,21 0 .58 NO 13 .6,12.8.12 .6 5 .5 .5 .5 .5 .5 150,146.148 2A .1 .3.1 .2 401,411 .4M 4 .9.4.1,13V2112004P-IS 1 L71 8 .08 NONE NONE 153 224 5 .15 039 1 .36 NO 16,7 . 16 .5.16,7 7,0,T0. 7 .0 762,766 .770 0,09,0,08, 0.07 101,99,96 6 .6, 9A 6 .8
NOTE I -ORP Probe malfunction (not nottatured )
SHALLOW FRACTURED BEDROCK WELLS
AVG
WELL DEPTH TO PROD PUMP WELL EVAC WELL EVAC SPECIFI CWELLDEPTHWATER LEVEL RATE -VOL VOL VOL VOL EVAC TEMP pH CONDUCTANCE DO ORP TO"DATE NO .(fect) (feet) (r~t) ODOR (ted/man) ILI 1. r,) (Dl~rsl 96~) 95 IYLV trial, C)(unita)(.V) (NTU)-- NONE 2M'7 85 L L213)
l6g,16 6.16 8 6 .2 6!~U uro '1/21/2004 DMW-1 29,02 6JI NONE 3 1 N~o)
IFL1007caIO)-'0 56.(0 54,0 53 NOTEI 16,11 .11U21/2004 DMW-2 32 .08 7~95 NONE NONE 80 14 .90 100 3 .94 0 .79 NO 108 . 10.6,10A 6A,'6 4,6 4 413,411 .412 0 13 .0 .14,0 14 NOTEI 0.3 .03.031/2012004 PMWC-BR-LF 36,00 13 .17 NONE NONE 40D 14 .09 6 .09 3 72 1 ~61 NO 17.7, 17.5 . 17 .9 6o . 6.9, &9 488 .488.487 0 28.0.23,0.19 20 .19 .ig 5A~4 .4,3n1120n004PMWC-BR 36 .00 13 .17 NONE NONE 400 14 .09 23 .65 3 .72 625 NO 18.1, 18 .0. 18 .0 6.9 . 7 .0 . 7 .0 476,473 .473 0,14 .0 15,0.21 13.12,12 2 .5 .2 2.2,2I120t2004 PMWH-BR 20 .72 8 .45 NONE NONE 150 7.57 1 ~60 2 .00 0 .42 NO 16.1, 15~9 . 15 .6 6.7 . 6 .7 .6.7 433,429 .427 0,25,0 20,0.23 NOTE 1 2 .2,0 .4,0.21119,2004 PMWI-BR 38 .07 10 .32 NONE NONE 143 17 .13 4 .50 4 .53 1,19 NO 17,0,17 .0,17 .1 7.7 . 7 .7 . 7 .7 678 .677 .681 0.71 . 0,68, 0,67 -16-18-18 3 .3 . 15,2 1InOI2004PMWL-BR 24.46 5 .61 NONE NONE 62S 11 .64 2,40 3 .07 0,63 NO 12.8 .12,8,116 6.2,6 .2 .6 .3 233 .234,234 0 .26, 0,27 .0.24 NOTE 1 1,5,15,1 5~/IW2004 PMWM-BR 19 .16 11 .52 NONE NONE 86.5 4~72 4 .80 1 .25 1 .27 NO 12,0.12 .3 .124 5 .9.5 .9 .5 .9 230,226,226 1 .4,1 .3 .1 .0 NOTE 1 3 .4.3 .6.3 4
NOTE I -ORP Probe malf-n16.n (an,orea,ured)
COMMENTS
Water le,el, and oil depth .are reftnoread to to, of PVC c.n .g.- = A,g p..pi.g,.,a ... d I taioimi~ c,tabilioc d,a,d,,n while removing one well volume and stabilizing indicator parameters,
FIELD SAMPLING CALIBRATION DATA FORM
STUDY :C,-k-u'd M (-~P
DATE::::=ki C n -J WEATHER CONDITIONS :
COLLECTORS :c- X SURFACE UNIT READER :A,L-4,J
HYDROLAB SERIAL 43 COMPUTER :
OTHER EQUIPMENT : ~j rvAz N~D SURVEYOR SERIAL X :
Procedure Number 3210 .1
Calibration Time ~ime (000 Time 00--~Q Time
Barometric t C1Pressure'7 mHq -7 ~J 1,mmHg mmHg
lnstru~ent ndard Instrument Standard Instrument Standard
Valu orvalue Value Value Value Value
Thermomete r
No .r-,VATEMP
(deg C)
W
DO W
(mg/1)W
AW >a-T >
pH B 7 .00 13 > 7 .00 >7 .00
(units) B
>
4 .00 ~41 >4 .00 >4 .00
B > 10 .00 > 10 .00 >10 .00
SPCOND SS 0 .00 > 0 .00 >0 .00
(US/Cm) SS JAO >-2X V >
SS
>
ORP SS > >
(MV) SS >
SS > 00 0 .00 > 0 .00
SS >
KEY : B =Buffer W =Winkler NA Not Applicable
SS =Standard Solution AW =Average Winkle r
> =Adjusted To -- / -- > =Not Adjusted To
FIELD SAMPLING CALIBRATION DATA FORM
STUDY : 1,J
DATE : a -A WEATHER CONDMONS,C.LeAN 0 F g A
COLLECTORS :Q C (L-W)SURFACE UNFT READER :V P-u w
HYDROLAB SERIAL 1 ? 0 .1-COMPUTER :
OTHER EQUIPMENT :Vt A -J?~n Z4%) L~Vl L-7 CC if~~SURVEYOR SERIAL 0 :.9L-
Procedure Number 3210.1
Calibration Time Time J Time Time
Barometric tell O .-A
Pressure -3 mmHg mmHg mmHg
Parameter Calib . Instrument Standard Instrument Standard Instrument Standard
I Value Value Value Value Value Value
Thermomete r
No .ta
TEM P
(deg C)
W
DO W
(mg/1)W
AW c'I >S%3
pH B > 7 .00 > 7 .00 > 7 .00
(units) B >4 .00 >4 .00 >4 .00
B > 10 .00 > 10 .00 >10 .00
SPCOND SS 0 0 > 0 .00 > 0 .00 > 0 .00
(US/Cm) SS 75--S-,>-'7,X 0 >>
SS > > >
ORP SS 4430 ----> ---->(MV) SS >>
TURBIDITY SS 0 .00 > 0 .00 > 0 .00
(ntu)SS > >
KEY : B =Buffer W =Winkler NA Not Applicabl e
SS =Standard Solution AW =Average Winkle r
> =Adjusted To -- / -- > =Not Adjusted To
FIELD SAMPLING CALIBRATION DATA FORM
STUDY: ~-~A ,J
DATE :51"04 WEATHER CONDMON 3
COLLECTORS : SURFACE UNI-T READER :zoc-"L'~w
HYDROLAB SERIAL L) COMPUTER :
OTHER EQUIPMENT : C kA ly~^T-p t: T 6r~,-SURVEYOR SERIAL #:
Procedure Number 3210 .1
Calibration Time Time ()-730 Time Time
Barometric Q2-0 104
-Pressure JC4 mmHg mmHg mmHg
Parameter Calib . Instrument Standard Instrument Standard Instrument Standard
I Value Value Value Value Value Value
Thermometer
No .
TEMP
(deg C)
W
DO W
(mgA)W
AW 3
pH B 7 r2 > 7 .00 > 7 .00 >7 .00
(units) B -3,61 >4 .00 >4 .00 >4.00
B - > 10 .00 >10 .00 >10 .0 0
SPCOND Ss 0~0 > 0 .00 > 0 .00 >0 .00
(US/cm) SS >1);LO >>
SS > > >
ORP SS 5~X5 > >
(MV) SS >
TURBIDITY Ss 0 .00 > 0 .00 > 0 .00
(ntu)I SS F->
>>
KEY : B =Buffer W Winkler NA Not Applicable
SS =Standard Solution AW =Average Winkle r
> =Adjusted To -- / -- >z Not Adjusted To
FIELD SAMPLING CALIBRATION DATA FORM
STUDY :L.)N Lx~C- -% 0 -J (V%, (~-P
DATE: 0 1 c.-WEATHER CONDMONS :4\3
COLLECTORS:t. 0 c -x %-SURFACE UNrr READER,:LA-~J
HYDROLAB SERIAL #:316,,1 3 COMPUTER :
OTHER EQUIPMENT:J4,ALtt SURVEYOR SERIAL #:
Procedure Number 3210 .1
Calibration Time Time 0 7,3 c,Time n Time
Barometric k/t c
Pressure Hg I '? 5 3 , 3 mmHg mmHg
Parameter Calb . Instrument SVr Instrument Standard Instrument Standard
Walue lValue Value Value Value Value
Thermomete r
No .
TEMP
(deg C)
W 9 .3
DO W
(mgA)W
AW
pH B > 7 .00 __~_~C( >7 .00 > 7 .0 0
(units) B 4 .00 11 .0 >4 .00 >4 .0 0
B -A > 10 .00 10 .00 10 .00
SPCOND SS f.,0 .00 0,10 >0 .00 > 0 .00(US/cm) SS 7 -2-0 TAL >72 0 >
SS > > >
DRIP SS >
(MV) SS >
TURBIDITY SS 0 .00 > 0 .00
(ntu)SS >~.oo
KEY :6 =Buffer W =Winkler NA Not Applicable
SS =Standard Solution AW =Average Winkle r
> =Adjusted To -- / -- > =Not Adjusted To
FIELD SAMPLING CALIBRATION DATA FORM
STUDY : 5 Q NA-T~L~-Vo'.J M ~'P
DATE : Xk WEATHER CONDMONS :CC~D CLA.~e6,I
COLLECTORS :~'o C SURFACE UNrr READER :Ljl (L~k.,J
HYDROLAS SERIAL #:-3 COMPUTER:
OTHEREQUIPMENT:k-Aikr %A 7ti ~jp T,,O r~e I-tf f~~SURVEYOR SERIAL N:4
Procedure Number 3210 .1
Calibration Time Time Time 5--5 0 Time
Barometric Ix, I t;
Pressure mmHg 75,z,4 mmHg mmHg
Parameter Calib . Instrument Standard Instrument Standard Instrument Standard
I Value Value Value Value Value Value
Thermomete r
No,'J
TEMP --/-->
(deg C) > > >
W
DO W
(mg/1)W
AW >CJ C1 .t >10 1 >
pH B 7,0/> 7 .00 >7 .00 > 7.00
(units) B >4 .00 4 .00 >4 .00
> 10.00 > 10 .00 > 10 .00
SPCOND SS >0 .00 L9,0 /> 0 .00 > 0 .00
(US/cm) SS >-)d-0 ---->
SS
ORP SS k4-k~tft ~f'>
(MV) SS > >>
10 0 .00 0,00 0 .00TURBIDITYSS - > >>
(ntu)SS
KEY : B =Buffer W =Winkler NA Not Applicable
SS =Standard Solution AW =Average Winkle r
> =Adjusted To -- / -- > =Not Adjusted To
FIELD SAMPLING CALIBRATION DATA FORM
STUDY :
DATE :WEATHER CONDITIONS: ('(:)-0,
I
COLLECTORS:\-b C V3 SURFACE UNIT READER :Q fL ~ \~J
HYDROLAB SERIAL 0 :3?;?0 ;L_ COMPUTER :
OTHER EQUIPMENT : 14,4 1 -V\D ~_J>Z SURVEYOR .SERIAL #:
Procedure Number 3210 .1
Calibration Time Time 3 0 Time Time
Barometric )r-t 5L,6-4
Pressure 6 mmHg 4CI .t mmHg mmHg
Parameter Calib . Instrument Standard Instrument Standard Instrument Standard
I Value Value Value Value Value Value
Thermomete r
No .VA
TEM P
(deg C)
W _C1 (ad
DO W
(mg/0 W
AW tc .l,>
pH B > 7 .00 0 >7 .00 > 7 .00
(units) B L3 >4 .00 --rl>4 .00 >4 .0 0
B > 10 .00 > 10 .00 > 10 .00
SPCOND SS 6,0 >0 .00 C .0 > 0 .00 > 0 .00
(US/cm) SS 7 Q!J,> _2~.L(.-/> 7 .7-1)>
SS >
ORP SS 3L Z >
(MV) SS > >
,-J i,4TURBIDITYSS -- > 0 .00 0 .00 > 0 .00
(ntu)SS >
KEY : B =Buffer W =Winkler NA Not Applicable
SS =Standard Solution AW =Average Winkle r
> =Adjusted To -- / -- > =Not Adjusted To
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
LOCATION :DN, NC PROC NO : 1 3500mi
PROJECT NA DN IVIGP (SAPROLITE WELLS)FIELDCREW :j LDC,RLW
SAMPLING DATE : -I~21-Jan-04
MONITORING WELL NO .PMWB-D
WATER LEVEL METER SIN :N/A
PID READING 0 0 ppm PRODUCT LEVEL METER S/N :C7 4 ~; - I
METHOD (Pump /Ball)1PERISTALTIC PUMP TIME I INITIALS OF COLLECTED SAMPLE :L-0
WELL VOLUME CALCULATION :
WELL WELL DEPTH TO WATER CONVERSION WELLCo)LUMN ft VOL 'a l
DIAM DEPTH (ft)WATER (ft)COLUMN (ft)X FACTOR VOL (gal)
2-18 .18 X 0 .163 1
X
NIA gallons X N/A ~Jiters
SCREENINTERVAL
FREE PRODUCT MEASUREMEN TFROM TO DETECTED ODOR S
16 .68 18 .18 Ift .TYPE : DEPTH TO WATER :
STRONG :DEPTH TO PRODUCT~---00MINOR: PRODUCTTFI I
50 ftftjPumpINT~KE_ NONE DON'T SAMPLE IF THICKNESS >OR TO 0.1 FT
AT START I AT
NO
17 17 .
INITIAL READINGS MEASURED AT GROUNDWATER /AIR INTERFACE INDICATED BELO W
WATER FLOWRATE TEMP SPEC TURBIDITY PH ORP DISSOLVEDTIME LEVEL COND OXYGEN(hh -MMS (ft)~mllmtn) (deg C) (us/cm)(ntu) (unit)(mv)(MgA )
~/A N/A N/A N/A NIA N/A N/A N/A N/A
WATER FLOWRATE TEMP SFFC TURBIDITY PH ORP DISSOLVEDTIME LEVEL COND OXYGEN(hh :mm :ss)(ft)(ml/min)(deg C)(us/cm)(unil (MgA)
STABILIZED DRAWDOWN AND REMOVED BEGAN LOGGING DATA
17?0 I~L~ocl I L 6 .5 z -4-3 174 0 .5
131 350 3?b,~'4 .1 -7 -a,0 . -;
1 3 N 3ic)5-(9 a
15 0-3-)
v ~'q Ll 370 L 3 .y
5,Ao^~~V LO i33q-. i/z o v
ELECTRONIC FILENAME - rIj
COMMENTS :
OTN OTA VOLUME REMOVE D
PWATER LEVEL, PRODUCT LEVEL,AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
BJ%JM" rwvv ""~~Ivlr~lv I
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
ILOCATION :I BURLINGTON, NC PROC NO :3500 .1
1PROJECT NAME : IBURLINGTON P TE WELLS)FIELD CREW :LDC,RLW
ISAMPLING DATE,404WIM r220~~91-1~p .04
MONITORING WELL NO . PMWC-D
twc - 1) -WATER LEVEL METER SIN :N/A
PID READING PRODUCT LEVEL METER S/N :LZ
METHOD (Pump I Bail)IPERISTALTIC PUMP TIME / INITIALS OF COLLECTED SAMPLE :f3s
WELL VOLUME CALCULATION
: ISIO NWELL WELL DEPTH TO FWATER CONVERSIONon
DIAM DEPTH (ft)WATER [ft)COLUMN (tt)X 7FACTOR
2-25 .20 0
1
X 0 .1631]OR
X
N/A gallons X 3 .785 N/A
SCREENINTERVA L
FROM ft .1 TO DETECTED ODORS FREE PRODUCT MEASUREMENT
23 .70 2520 Ift TYPE : r DEPTH TO WATER :
STRONG :12EPTH TO PRODUCT~---I c-i"I
MINOR :-j P~E5UCT THICKNESS : (ft)
Pump INTAKEI NONE: IDON'T SAMPLE IF THICKNESS >OR =TO 0 .1 FT !
AT START I AT END
25~O
tt
2 .& 0 , ~ , ~
INITIAL READINGS MEASURED AT GROUNDWATER AIR INTERFACE INDICATED BELO W
WATER FLOWHATE TEMP SPFC TURBIDITY PH)ORP DIS§b=
TIME LEVEL COND OXYGEN
all (hh :Mmlss) (ft)(ml/mi (us/cm)(ntu)unit (mv)(mgA )
N/A N/A N/A N/A N/A N/A N/A N/A NIA
WATER FLOWHATL TEMP TURBIDITY pH OMP DISSOLVED
TIME LEVEL COND OXYGE N
(hh :mm :ss)(it) (mumin)(deg C) (us/cm)(nt (mv)(mgA)
MOVED & jQ. - EGAN LOGGING DATA
15-17 1 . )L-7 to cl 0 - A-X
1 550 i L,(5 15,0 '5 1 ;,. LA t - ol ;)- (03 0 ,
G f,"Lf 1 15,4 . '1 3 6 .V4~C,
o 0 11 .51 2--4i J'A .I
-)P ov,1356 XL)f
fv C-Mr.wi:L,Vo L-IN'o 1v*iyT-v-b 1-1 A S: E &Q\~ej~E7
i 'b c -s 5 6 0 1 3 .~-3i .3 -i,s 0 -1-k
i 566 q 2-0 it -cl 0 to 1 3 .-7 1 lilq w ;
15113 q20 L .(13 13 . G ~ ~'3'I, L -)-0~
o'l 14 15 1~- k 66 /c-f
ELECTRONIC FILENAME -
kCOMMENTS :
Cl=9 F~L-J ~' - 'Q L r LP L
0 ON Lvi"-i)
TOTAL VOLUME REMOVED =
KO-TE-WATER LEVEL, PRODUCT LEVEL,AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
Wwff%Lm r%jvvv-n S~%Jlvjrmim I
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
LOCATION :BURLINGTON . NC PROC NO:3500.1
PROJECT NAME :BURLINGTON MGP (SAPROLITE WELLS)FIELD CREW :
SAMPLING DATE : I 19-Jan-04 L R ;j a
MONITORING WELL NO .PMWF-D
WATER LEVEL METER SIN :N/A
PID READING PPM PRODUCT LEVEL METER SIN :
METHOD (Pump /Bail)1PERISTALTIC PUMP TIME I INITIALS OF COLLECTED SAMPLE :
WELL VOLUME CALCULATION :
CoWELL WELL DEPTH TO WATER CONVERSION WELLILUMN ft Vo l
DIAM DEPTH (ft)WATER (ft)X FACTOR L jai"0
2-16 .32 0 X I , z Q,
X
SCREEN INTERVAL
NIA gallons X 3 .785 N/A ~Ilters
FROM TO DETECTE ODORS FREE PRODUCT MEASUREMEN T
1 16 .32 TYPE : EPTH TO WATER :ISTRONG:EPTH TO PRODUCT :---(it)
MINOR~RODUCTTHICKNESS = (ft)
Pump INTAKEI NONE : IDON'TSAMPLEIFTHICKNESS>OR=TOO .lFTI
AT START AT EN D
16 16 .32
INITIAL READINGS MEASURED AT GROUNDWATER I AIR INTERFACE INDICATED BELO W
W
A -R FLOWHATE TEMP SPEC TURBIDITY pH)ORP DISSOLVEDTIMELEVELCOND OXYGENTE
(hh :mm,ss) (ft)(MI/mi US/cm)(ntu) unit (mv)(mgA)
N/A N/A N/A N/A N/A NIA N/A N/A N/A
WATER FLOWRATE TEMP --PTC TURBIDITY pH ORP DISSOLVE DTIME LEVEL COND OXYGEN(hh :mm :ss)(ft) (ml/min)(dog C) (US/cm)(ntu) (unit)(mv)(mgA)
~ANX)STABILIZED DRAWDOWN AND REMOVED BEGAN LOGGING DATA
I'Au,tico 3 . cl (Y Ot 5'3 . ct 3,-5-2- 6 .,3 ~-o"O
1421 i-160 i 0 CI 151 ~i ~ LA'(~ - L5-~1, -5 7
1 Li-1-v (I .'? I 111 (5". 5 01 (i ~( cl . 1 3, )--;1,0 LZ
11~ 3 o' ~--t 3 cl 15 . 5-k `13 2 .0 Z . 0-1~f
ILi 3ck 90 C (3, -1'? 1'5 ,'Irl C1 7~ 3,~j-0_2_4
o 3 ti - ~- 3 Cl Lt 6 CI 3 3-,~A '4
C1 Ll 3 3 ~k 0-24
1~~b 15 5 0 15-30 cIi L7 -5'sl 3
1 ~ 0 -26 o
ic-As /-tr~c'IV3-L cl I I It --3 S rz
13 --7 -L I cjS I I E;%t4,-%g kil
ELECTRONIC FILENAME -
awvOMMENTS :
TOTAL-VOLUME REMOVE D
NOTE :WATER LEVEL, PRODUCT LEVEL,AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
Ljvg%u- rwvvLzn %'%JsvWM11 I
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
ILOCATION :1BURLINGTON, NC PROC NO :1 3500 .1
PROJECT NAME : BURLINGTON MGP (SAPROLITE WELLS)FIELD CREW :LDC,RLW
SAMPLING DATE :19-Jan-04 90 -m-Q4 =1~~~-04 DC_
MONITORING WELL NO.
WATER LEVEL METER SIN : N/A
PID READING M PRODUCT LEVEL METER S/N :
METHOD (Pump /Sail)1PERISTALTIC PUMP TIME / INITIALS OF COLLECTED SAMPLE :
WELL VOLUME CALCULATION :
WELL WELL DEPTH TO WATER CONVERSIO WELLCoILUMN ft VolL 'al
DIAM DEPTH (11)WATER (11)X VOL a l
2'19 .07 9 .IS Is X S's
X
NIA galloll X 3 .785 N/A IIt,,7s7]
SCREENINTFFIVA L
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
16 .57 19 .07 Ift TYPE: DEPTH TO WATER :ISTRONGIDEPTH TO PRODUCT :---I og-tt:-~-(ft)
MINOR~I PRODUCT THICKNESS : = I (ft)
PUMP INTAKE NONE : IDON'T SAMPLE IF THICKNESS >OR =TO 0 .1 FT !
AT START AT END
1 18 .0
INITIAL READINGS MEASURED AT GROUNDWATER AIR INTERFACE INDICATED BELOW
WATER FLOWHAT TEMP SPEC TURBIDITY pH CHIP DIS0[7M
TIME LEVEL COND OXYGEN(hh :mm :ss)(it) (ml/min) (deg C) (US/cm)(ntu) (unit)(mv)(mgA )
NIA N/A N/A N/A N/A N/A N/A N/A N/A
WATER FLOWRATF TFMP --MTE TURBIDITY pH ORP DISSOLVED
TIME LEVEL COND OXYGE N(hh :mm :ss)(ft)(ml/min)(deg C) (US/cm)(nt (mv) (mg/1)
~-~%L)STABILIZED DRAWDOWN AND REMOVED BEGAN LOGGING DAT A
i 5)L.~tn I O,ko~ (D 1 -3 .5'7 2 L(3 .9,51 515~419
i5lx-?
L'Co ttiD~'-'r'0 1 Ll -.5 5
;??,L k t I ~9 )14~ lr,,c 7 ~oz t5,oL a -o ct .3 1 3,1 '7
3 . ~1-
1~L4 tl!i C)Un 319 . '5-It A5' a
quc I U C 14-3~
C, -33 '132 . t a L
I L C ~E r~; U0 1 0 uo I Lf, 05- -1~- I . D I
10 1 b--!5 c;
ELECTRONIC FILENAME -
OMMENTS :Pvx7t \7';~Mn
I= I
-
T
TOTAL VOLUME REMOVED
NOTE :WATER LEVEL, PRODUCT LEVEL,AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
Ljur%c ruvvr_n Llulvirpkili T
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
ILOCATION :I BURLINGTON . NC PROC NO :
PROJECT NAME, BURLINGTON MGP (SAPROLITE WELLS)FIELDCREW :1 LDC,RLW
SAMPLING DATE :19-J,n-04 20~tamt4,L21-,111-04 I 22-J,n-01--~
MONITORING WELL NO.PMWI
WATER LEVEL METER SIN :N/A
PID READING ~I:' PPM PRODUCT LEVEL METER S/N :
METHOD (Pump /Ball)1PERISTALTIC PUMP TIME / INITIALS OF COLLECTED SAMPLE :P1
WELL VOLUME CALCULATION :
WELL WELL T TO WATER CONVERSI WELLColLUMN ft Vo lF7L JalL~Lja
DIAM DEPTH (ft)WATER (11)
X __I.,
2-16 .12 %N~39t XX
gallons X 3 .785
SCREENINTERVA L
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
14 16 .12 TYPE : EPTH TO WATER :i
STRONG :DEPTH TO PRODUCT, (ft)
MINOR : IPRODUCT THICKNESS : (ft)
PUMP INTAKE NONI DON'T SAMPLE IF THICTNESS OR =TO 0 .1 FT I
AT START AT END
1 15 .5
INITIAL READINGS MEASURED AT GROUNDWATER /AIR INTERFACE INDICATED BELOW
W
A -H FLOWHATE TEMP SPEC TUR131DITY PH)ORP DISSOLVEDTIME LEVEL COND OXYGENTE
(hh mm :s (MI/Mi us/cm)(ntu) unit (mv) (m A)
N/A N/A NIA N/A N/A N/A N/A N/A NIACY
WATER FLOWHATE TEMP TUR131DITY PH ORP DISSOLVEDTIMEZ%4 LEVEL CONC, OXYGENI
(ntu) unit)(Mv)(hh :mm :(ft) (mi/min)(deg C) ('S/cm) I I (mg/10
STABILIZED DRAWDOWN AND REMOVED BEGAN LOGGING DATA
2 f ;t 'k -76%3% tj 7Z-2. Q 'L t-3,j
S io ZS-~ 2-,3 -L .:3c~3's I,c,%r"t
S-5
5 3,k 3 1 30 si'o 3't-T tts 2-Z -t'D
ELECTRONIC FILENAME -
LCOM64ENTS :
Ax-nv
TOTAL VOLUME REMOVED
NOTE :WATER LEVEL, PRODUCT LEVEL .AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
Llurxr- r%jvvr-n %~%JlvlrAIIA T
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
PROC NO : 3500 .1
21 .!nAPROLITE.W FIELD CREW :LDC,RLW
MONITORING WELL NO .PMWL-D 71
WATER LEVEL METER S/N : N/A
PR OPIDREADINGpm DUCT LEVEL METER S/N :
METHOD (Pump I Bail)
PUMP
TIME I INITIALS OF COLLECTED SAMPLE : 0 CA
WELL VOLUME CALCULATION :
WELL WELL DEPTH TO WATER CONVERSI WELLCo~LUMN ft0~LUMN Ift Vo lEy~n-]L la l
DIAM DEPTH (ft)WATER (ft)X VOL al
2'9 .70 X Q, I %S"
X
N/A gallons X 3 .785 N/A Ilt11s
SCREENINTERVAL
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
8 .70 ft . 9 .70 ft.TYPE :DEPTH TO WATE R
STRONG :DEPTH TO PRODUCT:...~rj lz~
MINOR : PRODUCT THICKNESS :-(ft)
Pump INTAKEI NONE : j IDON'T SAMPLE IF THICKNESS >OR =TO 0 .1 FT !
AT START AT END
9 9 .7
INITIAL READINGS MEASURED AT GROUNDWATER AIR INTERFACE INDICATED BELO W
WATER FLOWRATE TLMP SPEC TURBIOI :~EpH)ORP DISSOLVED
TIME LEVEL COND OXYGEN-mm :ss)(ft) (ml/min)(dpg C) (us/cm)(ntu) (unit (mv) (Mgt')
N/A N/A N/A N/A N/A N/A N/A N/A
WATER FLOWRATE TEM SPE TURBIDITY PH ORP DISSOLVED
TIME~4; LEVEL COND OXYGE N
(hh :mm :(ft)(ml/min)(deg C)(us/cm)(unit)(mv) (mg/0
STABILIZED DRAWDOWN AND REMOVED BEGAN LOGGING DATA77f-S,9k,7 !3~, t; +.3 C-S 7, 1 V !3- 1,
+
S -7 t -A LA ,-2L
c rt ~-i /-3 Z'-~S't 41 K .-7
CA 3c!/Scz Lj .~j k'Ir.J52*4 SA 3,6-7
ELECTRONIC FILENAME - r)
COMk4_ENTS :c 'z'
TOTAL VOLUME REMOVED
NOTE :WATER LEVEL, PRODUCT LEVEL,AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
Ljur%.r_ r%jvvr-n %~%ilwirmill T
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
LOCATION : BU RLINGTON, NC PROC NO : 1 3500 .1
PROJECT NAME : BURLINGTON MGP (OVERBURDEN WELL~- FIELDCREWd LDC,RLW
SAMPLING DATE :21-Jan-04 -W_Jan-0 4
MONITORING WELL NO.MW-3 "b
WATER LEVEL METER SIN :
PID READING k*7-P~m PRODUCT LEVEL METER SIN :
METHOD (Pump /Ball)
Ump
TIME / INITIALS OF COLLECTED SAMPLE :
WELL VOLUME CALCULATION :
W=Tf~WATER,ft CONVEROSRIONICoCTIWELL WELL --DEPTH T O
DIAM DEPTH (ft)WATER ft
)LUMN X F
A
2- 22 .24 X 0 .1631
X
N/A gallons X 3 .785 N/A liters
SCREENINTERVA L
FROM TO DETECTE ODORS FREE PRODUCT MEASUREMENT
1 22 .0 ft .TYPE:DEPTH TO WATER :I
STRONG~DEPTH TO PRODUCT :---1 DAAE (ft)
MINOR, PRODUCT THICKNESS : = I (ft)
PUMP INTAKE NONE : 1~ IDON'T SAMPLE IF THICKNESS>OR =TO 0 .1 FT!
ATSTART .1 ATEN D
17 .0 ft 17 .0 ft .
INITIAL READINGS MEASURED AT GROUNDWATER /AIR INTERFACE INDICATED BELOW
ATE FLOWRATE TEMP SPF(;TURBIDITY PH ORP DISSOLVED
TIME LEVEL COND OXYGEN
(hh nnss) (ft)(ml/min) (deg C) (Us/cm)(ntu) (unit)(mv)(m A )
N/A N/A N/A N/A N/A N/A N/A N/A N/A
WATER FLOWRATE TEMP --MTE TURBIDITY PH)ORP DISSOLVED
TIME At, LEVEL COND OXYGEN
(US/cm)(n1u) unit (Mv )(hh :mm :s (ft) (ml/min)(deg C)(mg/1)
7 7d--
-
STABILIZED DRAWDOWN AND REMOVED BEGAN LOGGING 7DATAtV,t As -3 t
1~ I ~, !3
S
-1 '3 .%:~13 c-I L-1 -2-'3 L -r..',S*s
I% 0Y -~fj U cl,csq 9,-J-I s,cd-l I\ kq il k
IN-9 /42~c~,,&C3 le.13,1
I tz ~/'t-~-ciz (L- oz,S%-l
I,(3i (Lf itzs ri ~A.1 7--l
ELECTRONIC FILENAME -
COM
NTS :o\~
C ,
TOTAL VOLUME REMOVED =
NOTE :WATER LEVEL, PRODUCT LEVEL,AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
~wlx" r ~vw "I I ~wlvjl ~...
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
ILOCATION : BURLINGTON, NC PROC NO :3500.1
P I OVERBURDEN WELLS)FIELDCREW :j LDC,RLW
SAMPLING DATE :_16.laa,04 I 20-Jan-04 21 le 04 1 2P In 1 84,
MONITORING WELL NO .MW-5
WATER LEVEL METER SIN : N/A
PID READING PRODUCT LEVEL METER SIN :
METHOD (Pump /Ball)[PERISTALTIC Pump TIME / INITIALS OF COLLECTED SAMPLE:
WELL VOLUME CALCULATION
: ~O~~)LU MWELL WELL EPTH TO WATER CONVERSION0CoEynir.lDIAM DEPTH (ft)WATER (ft)
)LUMN
Itt X FACTORRI
2'13 .54 X
X
N/A 9,11,n, X 3.785 N/A :1i t~e r~s
SCREENINTERVA L
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
3 .54 13 .54 TYPE~ TO WATER :
STRON&DEPTH TO PRODUCT : 00
MINOR, PRODUCT THICKNES 00
Pump INTAKE NONE: DON'T SAMPLE IF THICKNESS >OR =TO 0 .1 FT I
AT START AT END
10 .5 ft . 10 .5
INITIAL READINGS MEASURED AT GROUNDWATER /AIR INTERFACE INDICATED BELOW
WATER FLOWHATE TEMP SPEC TURBIDITY pH URP DISSOLVED
TIME LEVEL COND OXYGEN
(hh :mm,~) (ft) (ml/mi (us/cm)(nt (mv) (mg1l )
N/A N/A N/A N/A N/A N/A N/A N/A N/A
WATER FLOWRATE TEMP) -MM TURBIDITY pH ORP DISSOLVED I
T1 LEVEL COND OXYGEN
(h h :rMM5,/,)(ft)(ml/min)(deg C (us/cm)(ntu) (unit)(mv)(mg/1)
STABILIZED DRAWDOWN AND REMOVED BEGAN LOGGING DATA
rF _70-2- 3 r-1 7_,-J~& ~15 %Ix
-2. 1z,A&CA 34% Ji 11A
I z_t 3 ;~j % Q) I Lit%%ci, to '7,
-3 t -L k XIQ%~~-l irl, S -1 .
7-'T
ELECTRONIC FILENAME -
COMMENTS :--z 0 c)~fN
cl
ITOTAL VOLUME REMOVED
INOTE~WATER LEVEL,k'KUUUL; I LtVML,AND WELL DEPTH RE REFERENCED TO THE TOP OF WELL CASING .
~wqx" v w WT "I I ~~lvll ~11 I
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
LOCATION : IBURLINGTON . NC PROC NO : 1 3500 .1
1PROJECT NAME :1BURLINGTON MGP OVERBURDEN WELLS)FIELDCREW :j LDC,RL
ISAMPLING DATE : I 21-Jan-04 1 -22~1
MONITORING WELL NO.MW-9
~D c
WATER LEVEL METER S/N : NIA
PID READING PPMI PRODUCT LEVEL METER S/N :I Ll ;
METHOD (Pump /Ball)1PERISTALTIC PUMP TIME / INITIALS OF COLLECTED SAMPLE :
WELL VOLUME CALCULATION :
Co)LUMN ftWELL WELL F-WATEER CONVERSION
IDIAM DEPTH (ft)COLU!M~N [ft)X FACTOR
2-9 .50 X 0.1631
X
gallons X 3 .785 liters
SCREENINTERVA L
FROM DETECTED ODORS FREE PRODUCT MEASUREMENT
2.0 ft .1 TYPE* DEPTH TO WATER :i
STRONG :DEPTH TO PRODUCT:--- ~j OfJ Z 00
MINOR :__.,;,.PRODUCT THICKNESS : = I (ft)
PUMP INTAKE NONE : DON7 SAMPLE IF THICKNESS >OR =TO 0 .1 FT !
AT START I AT END
9 .50 9 .50
INITIAL READINGS MEASURED AT GROUNDWATER AIR INTERFACE INDICATED BELO W
WATER FLOWHATF TEMP SPEC TURBIDITY pH ORP DT995=
TIME LEVEL COND OXYGEN
~hh :mm*.S)(tt) (milmin)(US/cm)(nt (mv) (mg/0
N/A N/A N/A N/A N/A NIA NIA N/A N/A
WATER FLOWHATE TEMP --MTM TUR131DITY PH ORP DISSOLVED
TIME LEVEL COND OXYGE N
(hh :mm :ss) Vj I, (ft) (mllmin)(deg C) (US/cm)(nt (mv)(mgA)
=- J STABILIZED DRAWDOWN AND REMOVED BEGAN LOGGING DATA
13 t"'39 -7 0
14 -7 1%, 0 -?'a-?~' I.,L 3-3 1
L;-I I 'f - ~-~;'"t (~.L L~-1 1 .
'ci I I Li 0 ~:j 11 .3 0, ot
2-'3 7,c, i -f L 3'2 q 3 .5 6 -L 2-~zl'l C
~f,2-1briL-37, D ?~tq 7 .-40 1 4 ti -2 i 73 S-
C,71 VID -~U-D '),15 il p L
C~l q Foo 'I'l xq 0 C 2--7 L I .)L-:,i
ELECTRONIC FILENAME -
COMMENTS-
CI =
711
'TOTAL VOLUME REMOVE D
'OTE :WATER LEVEL, PRODUCT LEVEL,AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
UUF%C r'UVVr-n %,%JIVIrAI4 T
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
LOCA71ON : BURLINGTON, NC PROC NO : 1 3500
IPROJECT NAME : BURLINGTON MGP (OVERB ROEN FIELD CREW :[LDCF
ISAMPLING DATE:A-Jtan-04~- 21-Jan-04 C
MONITORING WELL NO.
PMWB-S WATER LEVEL METER SIN:N/A
PID READING DPml PRODUCT LEVEL METER S/N :'i
METHOD (Pump /Ball)"PERISTAL C PUMP TIME / INITIALS OF COLLECTED SAMPLE :ci
WELL VOLUME CALCULATION :
Co)LUMN ft0)LUMN ftWELL WELL DEPTH ro WATER CONVERSIO F-W-E-LL -1DIAMDEPTH(ft)WATER (ft)X FACTOR VOL(gal )
2-13 .58 g' v7 Tq XPX
N/A gallons X 3 .785 N/A liters
SCREENINTERVA L
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
3 13 .58 Ift TYPE : DEPTH TO WATER:I
STRONG~DEPTH TO PRODUCT:
MINOR,PRODUCT THICKNESS:(ft)
PUMP
INTAKE NONE: IDON'T SAMPLE IF THICKNESS >OR =TO 0 .1 FT!
Afi~ART AT EN D11.5 ft
.1 11 .5 ift .
INITIAL READINGS MEASURED AT GROUNDWATER AIR INTERFACE INDICATED BELO W
WATER FLOWHATE TEMP SSPJEC TURBIDITY PH ORP DIS95=
TIME
LEVEL
(COND OXYGEN
(hh :mm~ss)(ft)(mVmln)(de C)
i
(ntu) (unit)(mv)(M%A )
N/A NIA N/A N/A N/A N/A N/A N/A N/A
WATER FLOWHATF TEMP ---myo TURBIDITY pH ORP DISSOLVEDC) S
)TIME LEVEL COND OXYGEN
(hh :mm :ss)(tt) (ml/min)(dei (nt (mv )
STABILIZED DRAWDOWN AND REMOVED BEGAN LOGGING DATA
1 300 T -7p, 50 tl .%L S ;L5~ 7,ol go' ().7f.
0 3oo 9, (- I 5o io-L 3 '6 3q "i Li . 12..?, 0(. -? A a
I ;Lo 300 lillio -50 10 . ~50 s ;L t~-'L 3, Y7 -).(ri 7 v
I OL V UO 3,clO '50 1 (1 .3e lir3o--i 2" ~~r lo~
ELECTRONIC FILENAME - %-J
OMME TS :
I= ff
TOTALVOLU EREMOVED =
N'OTE :WATER LEVEL, PRODUCT LEVEL,AND W -LL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
UUr%t FUWtK L;L)MPAN Y
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
LOCATION : I BURLINGTON . NC PROC NO :1 3500 .1
PROJECT NAME : IBURLINGTON MGP (OVERBURDEN WELLS)FIELDCREW :l LDC .RLW
SAMPLING DATE : lg-j"-
MONITORING WELL NO .PMWM-S
WATER LEVEL METER S/N :NIA
PID READING PPM PRODUCT LEVEL METER S/N :
METHOD (Pump /Ball)1PERISTALTIC PUMP TIME t INITIALS OF COLLECTED SAMPLE :
WELL VOLUME CALCULATION :
WELL WELL DEPTH TO WATER CONVERSION WELLCoILUMN ftCoILUMIft X VOL ILUM F7 al.!~_J a
DIAM DEPTH (ft)WATER (ft)N FACTOR
_l'
2-12 .68 X
X
gallons X 3 .785 liters
SCREENINTERVA L
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
6 12 .68 ft TYPE : DEPTH TO WATER :
STRONG~DEPTH TO PRODUCT :---fj 0 'j 1,7 yo
PRODUCT THICKNESS :(ft)
Pump INTAKE NONE : IDONTSAMPLE IFTHICKNESS >OR=TOO .l FT!
ATSTART ATEND
t t
1 12 .5
INITIAL READINGS MEASURED AT GROUNDWATER AIR INTERFACE INDICATED BELO W
WATER FLOWHATF TLMP SPEC 7UMMIrv PH ORP DISSOLVED
TIME LEVEL I COND I OXYGEN
(hh :MM's (deg C) US/CM)(ntu) unit)(Mv)(Mgt')
N/A N/A N/A N/A N/A N/A N/A NIA N/A
_79nWATER FLOWHATE TFMP T I TURBIDITY PH)OHP DISSOLVE D
TIME LEVEL COND OXYGEN
(hh :mm .,".((ft) (ml/min)(deg C) (Us/cm)(ntu) _(unit (Mv)(mgA)
STABILIZED DRAWDOWN AND REMOVED BEGAN LOGGING DATA
it 3 c-2--[Fj vt I tjj .3 7-,L~ _r~-,S-,j -,~. %-1 'A'-Ls
1 3 i S (013 3q '+ 3 i'%l;z1
'iS 2-1-S %%.s5 5-5 A c;,S 31s 2-~cl S
I I -1y 3 275 \ - -';L,S5 ILi,%O i 4 &-rA Ill I -E~,13 3-1-1 2-to
17-c"- /z-1 S ik's 1 5 S'L~I j-j'r-'j %'. kl:~ 5,~s* A ri t -z k't
1 2-lick 2:1 1~3 .ut I -A '1 5 A
-t5 -L-1 5 1 k S 1~.' 1,AL->. - ~-J . r,-4 -t I % 1 1.--2 -2
7-15 k -7--L~It LAS N'cj -Z-S~S ;4 -7 "k C kc
AIN W~F
ELECTRONIC FILENAME -
7
ICOMMENTS :
CI =16L
T
L V
W LOTALVOLUME REMOVE D
TNo0=T:E :WALTER LEVEL . PRODUCT LEVEL,AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .T OLUM
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
LOCATION : BURLINGTON, NC PROC NO :3500 .1
IPROJECTN ME :BURLINGTON MGP FIELD CREW :LDC,RLW
ISAMPLING DATE :/A t;joll I
MONITORING WELL NO .P M 0~c- voc
WATER LEVEL METER StN :N/A
PID READING PPM PRODUCT LEVEL METER SIN :
METHOD (Pump /Ball)IPERISTALTIC PUMP TIME / INITIALS OF COLLECTED SAMPLE :tic
WELL VOLUME CALCULATION :
IONWELL WELL FDEPTH TO WATER CONVERSI WELL
DIAM DEPTH (ft)COLUMN (ftj X FACTOR VOL (gal )I
2-X 0 .1631
X
gallons X 3 .785 liters
SCREENINTERVA L
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
TYPE : I DEPTH TO WATER :
STRONG IDEPTH TO PRODUCT :---MINOR~I PRODUCT THICKNESS :=
PUMP INTAKE NONE : IDON'T SAMPLE IF THICKNESS>OR =TO 0 .1 FT!
ATHART AT n
I ~. C,~ ft-1 f
t
INITIAL READINGS MEASURED AT GROUNDWATER I AIR INTERFACE INDICATED BELO W
WATER FLOWRATE1 TEMP SPEC TURBIDITY PH)ORP DISSOLVED
TIME LEVEL COND OXYGEN
(hh :mm :ss)(ft)01/min) (deg C) (us/cm)(ntu) (unit (Mv) (Mg/1)
NIA N/A N/A N/A N/A N/A N/A N/A
WATER FLOWHATE TFMP -9150 TURBIDITY PH ORP DISSOLVED
TIME LEVEL COND OXYGEN
(hh :mm :ss)(ft) (mlftin)(deg C) (uslcm)(ntu) (unit) (mv)(m A )
J,ocuAi S SAr4Lt L STAB!IZED DRAWDOWN AND REMOVED BEGAN LOGGING DATA
nx,u,1 4
ko 39 3,1Q 'k ~4 -96 -7
4 ~'(Ca i ~3 1 Sl il .3 -~, is (, 'I'l Iq
ig-li IL .A yl L4 Y ;~a-I V 3 6 ci cl
q Yl .14 105~t 1 -4 .4 rlr.1 n 1 :3
~V~XPL-~I k 00 oc-er-i
ELECTRONIC FILENAME - V~
COMMENTS :
CI
NED
PRODUCT LEVEL,AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
uurtc rvvvr_ri tvIvIrAI4 T
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
ILOCATION :IBURLINGTON, NC I PROC NO :
PROJECT NAME: IBURLINGTON MGP (OVERBURDEN WELLS)FIELD CREW:
I 49--Ja-,-()4 20-Jan-04 an-04 22 . an .
MONITORING WELL NO.PMWC-S Ll
WATER LEVEL METER SIN : N/A
PID READING PPm1 PRODUCT LEVEL METER SIN :I cl
METHOD (pump /Bail)PERISTALTIC PUMP TIME / INITIALS OF COLLECTED SAMPLE :C ;
WELL VOLUME CALCULATION
: CONVERSITCoWELL
WELL
DEPTH TO WATER F--WELL
DIAM DEP H(ft) WATER (ft)
ILUMN ft X
FACTO VOL (Sal)j
2"21 .09 X
X
N/A gallons X 3 .785 N/A 711tem
SCREENINTERVAL I
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
6 .09 ft
.1
21 .09
ft .
TYPE : DEPTH TO WATER :i
STRONG~DEPTH TO PRODUCT:---f-oo(~(ft)
MINOR~IPRODUCT THICKNESS : - (ft)
PUMP INTAKE NONE : IDON'T SAMPLE IF THICFNESS >OR =TO 0.1 FT !
AT START I AT END
1 17 .0
INITIAL READINGS MEASURED AT GROUNDWATER AIR INTERFACE INDICATED BELO W
W
A -H FLOWHATF.1 TLMP SPEC TURBIDITY PH)ORP DISSOLVFD
TIME LEVEL COND OXYGENTV
(hh :mm:ss)(ft)(Mvmi lus/cm)(ntu) unit (mv)(M9A)
N N/A N/A N/A N/A N/A N/A N/A N/A
WATER FLOWHATE TEMP --PrC TURBIDITY pH ORP DISSOLVE D
TIME LEVEL COND OXYGEN
(hh :mm :ss)(ft) (ml/min)(deg C) (US/cm)(ntu) unit)(mv)(m9A)
STABILIZED DRAWDOWN AND REMOVED BEGAN LOGGING DATA
0 6 yo 13-11 C dl r.I ;L .L 1 &'VY -7 . C5 4~0 0 3C
13 ~ioo Z .cq -:z L4
vq 3'~-1 .3-19 4 x q ql~ticYl .9-,2-5 1,,ci 2 33 CL Lz-'>-
ON ~f Lt 1 3 .49 15 1z 19 -V66
0 q 1 q '4 C1 ~Allo -.2-q,39. &,cl L 0 w I rf
fz 0 0 13115 v-LO-I'l 31 01
ELECTRONIC FILENAME -
COMMENTS :L
G q
TOTAL VOLUME REMOVE D
NOTE :WATER LEVEL,PRODUCT LEVEL,AND WELL DEPTH ARE REFERENCED TO HE TOP OF WELL CASING .
~ ~. 1~. ~.. `. ~~..'. ~...
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
ILOCATION : N, NC PROC NO :3500.1
1PROJECT NAME :BURLINGTON MGP FIELDCREWd LDC,RLW
ISAMPLING DATE :
MONITORING WELL NO.
WATER LEVEL METER S/N :N/A
PID READING PRODUCT LEVEL METER S/N :PU :
METHOD (Pump /Bail)PERISTALTIC Mp~m TIME I INITIALS OF COLLECTED SAMPLE :
WELL VOLUME CALCULATION :
F-WATEWELL WELL FDEPTH TO R I FCONVERSIO ~N F WELL I
DIAM DEPTH (11)WATER (ft)COLUMN (ft~X FACTOR I VOL (gal)j
2'XX
gallons X 3 .785 liters
SCREENINTERVAL
FROM it TO DETECTED ODORS FREE PRODUCT MEASUREMENT
fit TYPE~ DEPTH TO WATER :T~-STRONG DEPTH TO PRODUCT :---I
MINOR,PRODUCT THICKNESS : = I (tt)
PUMP INTAKE NONE : DON'T SAMPLE IF THICKNESS >OR =TO 0 .1 FT 1
ATHARTft AT nit
INITIAL READINGS MEASURED AT GROUNDWATER AIR INTERFACE INDICATED BELOW
T WATER FLOWRATE TEMP SPEC TURBIDITY PH)ORP DISSOLVED
IME LEVEL COND OXYGEN
(mumi (us/cm)(ntu) unit (mv)(mg/1)(it)I
N N/A N/A NIA N/A N/A N/A N/A N/A
WATER FLOWRATE TEMP SPEC TURBIDITY PH)ORP DISSOLVED
TIME LEVEL COND OXYGE N
(hh :mm :ss) (ft)(mumi (de C) (us/cm)(ntu) (unit (mv)(MgA)
STABILIZED DRAWDOWN AND REMOVED - BEGAN LOGGING DATA
A,Lf 1 2 7 A 4 4 A 1 0 ~'(I-)t7~cj)~v
-'z oc -L.r- C.)
V ;L ix,1'3
j ;k-t 0 1
i I ~,o k ;z
i tin 0 j%,oq V1 7 .1L .1 7. 0 1 1)
i 1 1000 16,00,5,1 7-c o2
I -),Cl C,
I ci 70 5~z 7,.2,q 7, C31~ct 10
m9x-.,e rD -4 c I k (4 ~c 4-rloj
ELE(TRONIC FILENAME -
tj 6M-MENTS
6c~i TUM
I< 17C 1b~5-L,-Q,~ zjo~l
VOLUME REMOVED
VATER LEVEL, PRODUCT LEVEL,AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
DUKE POWER COMPAN Y
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLIN G
N, NC PROC NO : 1 3500.1
PROJECT NAME : BURLINGTON MGP ~OVERBURDEN FIELDCREW :1 LL)C,RLW
TE :-6-ArT*4 I 2o-jan-04 1-24--
MONITORING WELL NO.PMWL-S 1
WATER LEVEL METER SIN: N/A
PID READING tt ppm PRODUCT LEVEL METER S/N :
METHOD (Pump /Ball)1PERISTALTIC PUMP TIME / INITIALS OF COLLECTED SAMPLE :
WELL VOLUME CALCULATION :
WELL WELL DEPTH TO WATER FCONVERSIONCo)LUMN tt
ISIDIAMDEPTH(ft)WATER (ft)COLUMN It X FACTOR
2-7 .60 4t -3 -7 XTX R5~
gallons X 3.785 liters
SCREENtNTERVA L
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
4 7 .60 ft TYPE, DEPTH TO WATER :
STRONG~DEPTH TO PRODUCT :---NQ I-v-(ft)
F 1PRODUCT THICKNESS : = (ft)
PUMP INTAKE NONE : IDON-TSAMPLE IFTHICKNESS>OR =TOO .l Fl
AT START ATEND
7.50 7 .50 ft .
INITIAL READINGS MEASURED AT GROUNDWATER AIR INTERFACE INDICATED BELO W
WATER FLOWRATE TEMP SPEC TURBIDITY PH)ORP DISSOLVED
TIME LEVEL COND OXYGEN
(hh :mm :ss)(tt) (ml/mi (us/cm)(ntu) (unit (mv) (mg(l )
N/A N/A N/A N/A N/A N/A N/A N/A N/A
WATER FLOWRATE TEMP --myn TURBIDITY 4 RP DISSOLVED
TIME V<;,~ LEVEL COND
(unit)70
OXYGEN
(hh nm~so (ft)(ml/min)(deg C) (us/cm)(ntu) (unit)(mv)(mgA)
STABILIZED DRAWDOWN AND REMOVED - BEGAN LOGGING DATA
j 2_5 -4,3 -L-7
I Lt S 5
30 5 't-L ri -7 1
1 3,L 3 rf 5 ci -15 .3 1,1 0
5,3 5, f T~ k ~ l--ko
2-b -t
ELECTRONIC FILENAME - vi
7
OMWNTS :L~i cc o,% I
Cl
T
W
TOTAL VOLUME REMOVED01
NOTE :WATER LFVEL,FHUUUU I Lt:VEL,AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
DUKE POWER COMPAN Y
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
ILOCATION : BURLINGTON, NC PROC NO : 3500 .1:)M
1PROJECT NAME : I BURLINGTON MGP (OVERBURDEN WELLS FIELD CR EW :LDC,RLW
ISAMPLING DATE:A~-~1 zu-jan-M I 21-Jan-04
Ile MONITORING WELL NO . P-IS
WATER LEVEL METER S/N :N/A
PID READING U ppml PRODUCT LEVEL METER SIN!15-1
METHOD (Pump /Bail)1PERISTALTIC PUMP TIME / INITIALS OF COLLECTED SAMPLE :
WELL VOLUME CALCULATION :
WELL WELL D TfO WAT CONVERSIONWIFf!~j~~Ttjft F~~DIAM DEPTH (11)
111
X FACTOR
2-11 .71 XFClqX
gallons X 3.785 liters7]
SCREENINTERVA L
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
1 .71 ft . 11 .71 ft.TYPE :DEPTH TO WATER :
STRONG :DEPTH TO PRODUCT :---o 0 01 c-
MINOR : PRODUCT TI =I
PUMP INTAKE NONE : IDON'T SAMPLE IF THICKNESS >OR =TO 0 .1 FT!
ATSTART AT EN D
11 .21 ft .11 .21 ft .
INITIAL READINGS MEASURED AT GROUNDWATER /AIR INTERFACE INDICATED BELOW
WATER FLOWRATE TEMP SPEC TURBIDITY PH)ORP DISSOLVED
TIME LEVEL COND OXYGEN
(hh :mm~ss)(ft) (mvmi (us/cm)(ntu) unit (mv)(mgA )
N/A N/A N/A N/A N/A N/A N/A N/A N/A
WATER FLOWRATF TEMP --3M TURBIDITY PH ORP DISSOLVED
TIME LEVEL COND OXYGEN
(hh :mm :ss)(ft)(ml/min)(deg C) (US/cm)(ntu) (unit)(mv)(mg/l)
STABILIZED DRAWDOWN AND REMOVED - BEGAN LOGGING DATA
!2 -7 17,o ;1-)413 .2 10 1 t,IV_ 150 ()~ 5 .)-
1 Ll 'i t ~,x(~7 ~,5-:2 45 .5 4-~tl -3 R o-3~2-
I't J';45 0 lv'-ilk Li 14 -"2-~2-)L-G 1'), 2-o --Lo
li't 5 Q ~ 0 0 5 Q ((,. -~-7~~.i~15, ~I'D(t q
7r, o 8% 3 ~-D 1 '75-4 .3 (a,Ct ---7,o i fo~
?co 3, 3 IL~L 6-5L I '?, 0 3
I 50L (100 4~-3 /s-o -).0 3
1511 C L10 (S13-1 S-CL 7,03 9L (1,0)
-DC IA .ToiLi
ELECTRONIC FILENAME -
MCOMME~NTS :
C!=
IOTA~,VOLUME REMOVE DNOTE
ATER LEVEL,PHUUUU I LEVEL,AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
L)Umr- rvvvr_ri kUIVIrAI14 T
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
[LOCATCION :N, NC PROC NO :3500 .1PROjeT
PROJeCT N;ME:BURLINGTON MGP (SHAL FRACT BR WELLS)FIELDCREW :j LDC,RLW
SAMPLING DATE :j9,J,,-04j- 20,Aj-P4 1 21-Jan-0 4
MONITORING WELL NO .DMW-I
WATER LEVEL METER S/N :
PID READING 0, z PRODUCT LEVEL METER S/N :
METHOD (Pump /Ball)1PERISTALTIC PUMP TIME / INITIALS OF COLLECTED SAMPLE :
WELL VOLUME CALCULATION :
WELL WELL DEPTH TO WATER CONVERSION WEL LCo)LUMN ftCo)LUMN ttt IE7~DIAM DEPTH (ft)WATER ft
0 _LUMN It
X L FACTOR I OL a [ISI
2-29 .02 7-
L,
X
X
N/A gallons X 3.785 N/A litem
SCREENINTERVA L
FROM ft TO DETECTED ODORS FREE PRODUCT MEASUREMENT
16 .72 29.02 ft .1 TYPE' DEPTH TO WATER :
STRONG :DEPTH TO PRODUCT :---L-- ft
MINOR, PRODUCT THICKNESS : =(Ift)
Pump INTAKE NONE : IDON'T SAMPLE IF THICKNESS >OR =TO 0 .1 FT !
AT START
I
ATEND
24 .0 ft .24 .0 ft.
INITIAL READINGS MEASURED AT GROUNDWATER I AIR INTERFACE INDICATED BELOW
WATER FLOWHATE TEMP (SPEC TURBIDITY pH ORP DISSOLVED
TIME LEVEL COND OXYGEN
(hh :mm~ss)(ft)mllmi us/cm)(ntu) 0 (mv) (mg/1 )
N/A N/A N/A N/A N/A N/A N/A N/A N/A
--TFEC TURBIDITY pH ORP DISSOLVEDWATERI-LUWHAI TEM P
TIME LEVEL COND OXYGENmS[-EA
(ml/min)(deg C) (US/cm )(hh (ft)(nt (mv) (mg/0
STABILIZED DRAWDOWN AND REMOVED BEGAN LOGGING DATA
-3 z-~lrk't.-7 -g . U -t %~t
T sn~' i ir 1-11; q'o'A(L A3%
(r-0 -1 Lt ,--1 -1 cl
-1 3 .3 5 3 2-,-l L S ',S ~--L
k 3 ~k C3 ~2--T 3 z-
7- 'A
3 L'-1-1 -7-u z4 S \c- 'I, 'A 'L!~'~k -L\
2~~J~~\ ~-) I -I 2~~z-
I -Lcaz, I I ri'l \%,c 1-~Q- -L
1 3 5 S /*Sz.C-,Ll L. tc,6
1 3 5 -~,' /t-~~<, -1~1 (.-- ~ -3 (~-
I ucz'c' -7- Q c,(3 -0 ro~ k4 (z ko
vI\trali /
ELECTRONIC FILENAME -
COMMENTS :
Cl =
TOTAL VOLUME REMOVE D
NOTE :WATER LEVEL, PRODUCT LEVEL,AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
DUKE POWER COMPAN Y
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
ILOCATION : 113URLINGTON, NC PROC NO :3500.1
1PROJECT NAME, BURLINGTON MGP (SHAL FRACT BR WELLS) FIELDCREWJ LDC,RLW
ISAMPLING DATE : 21-J11-04
MONITORING WELL NO .DMW-2
WATER LEVEL METER SIN :N/A
PID READING ppml PRODUCT LEVEL METERS/N
."~Z~-fMETHOD (Pump /Ball)1PERISTALTIC Pump TIME / INITIALS OF COLLECTED SAMPLE :c;-3-
WELL VOLUME CALCULATION :
CONVERSIONWELL WELL DEPTH TO WATER CONVERSICoILUMM ft R
DIAM DEPTH (ft)WATER (ft)COLUMN (ft)X FACTORX
2-32 .08 -T~9 S X 0.163 1
N/A gallons X 3.785 N/A liters
SCREENINTERVAL I
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
22 .08 ftl 32 .08
ft
. TYPE : DEPTH TO WATER :I
STRONG~DEPTH TO PRODUCT :---lij I-rq (ft)
MINOR~ PRODUCT THICKNESS :_ =(ft)
PUMP INTAKE NONE : I J IDON'T SAMPLE IF THICKNESS >OR =TO 0 .1 FT !
AT START I AT END
2 27 .0
INITIAL READINGS MEASURED AT GROUNDWATER AIR INTERFACE INDICATED BELOW
WATER FLOWHATE TEMP I SPEC I TURBIDITY PH ORP Dil
TIME LEVEL COND OXYGEN
(hh MMS (ml/mi (us/cm)unit (mv) (m
N/A NIA NIA N/A N/A N/A NIA N/A3XY
WATFR FLOWRATE TFMP --70 TURBIDITY PH)ORP DISSOLVED
TIME LEVEL COND OXYGEN
(hh :mm :ss)(ft)(ml/min)(deg C) (us/cm)(ntu) (unit (mv)(MgA)IRW STABILIZED DRAWDOWN AND REMOVED BEGAN LOGGING DATA
S k3 U -t1470 %rj (c %3 1 Lt 5-4,5 1%,-3ci
Lt k S t'3 o -7 t
15'~ft .4 3 .4 t %Q 0~04S Lt ((- --7 (~ - 3 t3 o ('
Isk \ / 5-~sc~ I Z~~i Lk k -3,:1 0 % ?.~'-3 1 0113
ts'kct/3 je kok 's:C~3 -3 (,c C .
jo ,
ELECTRONIC FILENAME - d-j ~o
7
OM NTS *
Cl
TOTALLVOLUME EREMOVED
NOTE :WATER LEVEL, PROD !UCTELEVEL, AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
UUKt IJUVVtH kUIVIrAINI Y
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
LOCATION, BURLINGTON, NC PROC NO :3500.1
PROJECT NAME : 113URLINGTON MGP (SHAL FRACT BR WELLS)FIELD CREW :LDC,RLW
ISAMPLING DATE : I "-n-04 I 20-jan-(-,+MY-94-
MONITORING WELL NO.PMWC-BR
C, -C~o- - k~c-WATER LEVEL METER S/N :N/A
PID READING PRODUCT LEVEL METER S/N :
METHOD (Pump /Ball)URSSUB TIME / INITIALS OF COLLECTED SAMPLE :L,10 f "D
WELL VOLUME CALCULATION :
L tatI
ELL
WELL WATER [&CO NVERSSMN]VWELLWIT~EnL jDAMDEPTH(ft
I
COLUMN ft X FACTOR V
2-36 .00 X
X End
N/A gallons X 3 .1185 NIA liters
SCREENINTERVA L
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
27 .0 ft . 36 .0 ft.TYPE :DEPTH TO WATER :i
STRONG :DEPTH TO PRODUCT :--- !w o tj ~E
MINOR~ PRODUCTTHI (ft)
Pump INTAKE j NONE :DONr SAMPLE IF THICKNESS >OR =TO 0 .1 FT!
ATSTART .1 ATEN D
34 .5 ft 34 .5 f
INITIAL READINGS MEASURED AT GROUNDWATER AIR INTERFACE INDICATED BELO W
WATER I FLOWRATE TFMP)SPEC URBIDITY PH ORP DISSO ED
TIM E I LE VEL COND OXYGEN
(hh :mMss)
ft)
(ml/min)(deg C (uslcm)(ntu) (unit)(mv)(mgA )
N/A I N/A L N/A N/A N/A N/A N/A N/A N/A
WATER FLOWRATE TEMP SSP/EC TURBIDITY PH ORP DISSOLVFD
TIME LEVEL (COND OXYGE N
(hh :mm :ss) v4~(ft)(ml/min) (dec
u I I
(ntu)(unit)(mv) (m.
(~W#~8~~STABILIZED DRAWDOWN AND REMOVED J,I
i!~6-0 700 60 C. 0 11 . 3!5 jcj~ 0 ~ 1 .4 ~2 -1 1 .04
i 55 LA 700 1 -1 "A q Ig 0, 0 i -).L k9i .8 I'.L .;?,
-
a 1 0,61
w co ~j C 0 1. 1 ~-l ys~ -~A I G,i C ~cl 2-'2,C)0 .~4
I C 0 9 Lt sa ~ 1 5,09 -cu .2-cl 0 .;),
'A - Its ~t ;1-2 q -is-). 5-4 .37 -cl 3 kci ollz-A
(PC 70 L'15-02-Li C ~ 1 .1 &1; - (-3 .40 4A 1
"A ~N L j'n- F&D-1Ot ov A ^J6 a t~iv I >
I L .2 U 15 .1 1 rl 3 ~3
if,J4 r-.30 c,U6,02 ;Z,5 1 -cl 4 1 3 Ig
f5 4~Et"o ~, 1 ;L1 ,~-. --v -) cl 05
L
ELECTRONIC FILENAME -
C-0-MMENTS :e
cl L t 0
3 A-
TOTAL VOLUME REMOVE D
INOTE :WATER LEVEL,PHUDUU I LEVEL .AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
uumv_rwvvfm~%1wevir~1v I
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLIN G
ILOCAnON :I BURLINGTON, NC PROC NO : 1 3500 .11
::::::~1 PROJECT NAME, IBURLINGTON MGP (SHAL~FRACTI BR WELL FIELDCREW :j LDC,RL W
ISAMPLING DATE : I AR4aA-04 I 20-Jan-04 -'aR Q 4
MONITORING WELL NO .PMWH-13R
WATER LEVEL METER StN :N/A
PID READING M PRODUCT LEVEL METER SIN :
METHOD (Pump /Bail)1PERISTALTIC PUMP TIME I INITIALS OF COLLECTED SAMPLE :
WELL VOLUME CALCULATION :
WELL WELL DEPTH TO WATER CONVERS1 WELLCoILUMN ft VOL 'a lWELVOLI
DIAM DEPTH (ft)WATER (ft)x
2-20.72 xX FEiq
N/A gallons X 3 .785 N/A literS
SCREENINTERVAL
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
19.72 ft .1 20.72 111
.
TYPE : DEPTH TO WATER :
STRONG DEPTH TO PRODUCT :---d3y'a~(ft)
MINOR: PRODUCT THICKNESS : (ft)
PUMP INTAKE NONE : DON'T SAMPLE IF THICKNESS ~OR =TO 0 .1 FT !
AT START I AT EN D
2 20 .0 ft .
INITIAL READINGS MEASURED AT GROUNDWATER AIR INTERFACE INDICATED BELOW
WATER FLOWRATE TEMP SPEC TURUIDITY PH :EORP DISS
TIME LEVEL COND OXYGEN4
(hh :mm :ss)(ft)(ml/min) (deg C) USICM)(ntu) (unit)(Mv) (m
N/A N/A N/A N/A N/A N/A N/A N/A N/A
WATER FLOWRATE TEMP SPEC TURBIDITY PH)ORP DISSOLVED
TIME LEVEL COND OXYGEN
(hh ~mm,ss (ft)(ml/min)(deg C) (US/cm)(ntu) (unit (mv) (M
STABILIZED DRAWDOWN AND REMOVED BEGAN LOGGING DATA
o ck -I Lt k 'r-c
11.43 -rs z 5
40~ Z,cj-j k ';';Z~q-2.95 2-
7-3
ELECTRONIC FILENAME -
COMMI~NTS :LAr, Z
CI -
1
LTA
LUM
REMOVED =
11NOTtVVA2TER EVEL,PRODUCT LEVEL,AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
ILOCATION : BURLINGTON, NG PROC NO,:3500 .1
',TON MGP SHAL~FRACT BR ~WELLS)FIELD CREW :1PROJECT NAME : IBURLING I Et~
[SAMPLING DATE:19-Jan_~
;
41MONITORING WELL NO .PMWI-BR-----]
WATER LEVEL METER SIN : N/A
PID READING m PRODUCT LEVEL METER S/N :
METHOD (Pump /Bail)IPERISTALTIC PUMP TIME / INITIALS OF COLLECTED SAMPLE :
WELL VOLUME CALCULATION :
WELL WELL DEPTH TO WATER CONVERSION WELLCo)LUMN ft RCo)LUMNOLUMN ft F7_[aX
DIAM DEPTH (ft)WATER (ft)X FACTO
2-38 .07 A L X 0 .163 1
N/A gallons X 3 .785 N/A liters
SCREENINTERVA L
FROM To DETECTED ODORS FREE PRODUCT MEASUREMENT
28 .07 38.07 ft.TYPE :DEPTH TO WATER :
STRONG :iDEPTH TO PRODUCT :---rj a tic (ft)
MINOR PRODUCT THICKNESS :(ft)
Pump INTAKE NONE: i IDONr SAMPLE IF THICKNESS >OR =TO 0.1 Fr !
AT START AT END
330 ft 33 .0 ft.
INITIAL READINGS MEASURED AT GROUNDWATER /AIR INTERFACE INDICATED BELOW
WATFH FLOWRATE TEMP SPEC I TURBIDITY PH)ORP DI S
TIME LEVEL COND I OXYGEN
Ali (hh :MMSS) (ft)(MI/mi (us/cm)(ntu) unit (mv) (mg/1)
NIA N/A N/A N/A N/A N/A N/A N/A N/A
--'MykWATER FLOWHATE TEMP T I TURBIDITY pH ORP DISSOLVED
TIME LEVEL COND OXYGEN
(hh :mm :ss)(ft)(mi/min)(deg C) (US/cm)(ntu) (unit)(mv)(mgA )
STABILIZED AWDOWN AVI:[BEMOVED BEGAN LOGGING DATA
ic" 55 ttl~1-71-1-1 743A Ad-1 ft
7 5k)t!j br%Q -7,-1 9
scle Z~ ~Lo- L I 9-c -1 ok -7 M\ Lt(, L -7%'1-1 A
7-4v"t 1 -3
%I.,( -5-Gcb --L I k -'A I k-P 0~-j 3
7~/-TQio 3J~ 3 (P r"--I I
j -t 7-It /~foc).zi~ks -7"-Iu is I C.,Vi~
-t 7-k C)
tj ui,,,
ELECTRONIC FLENAM E
Ago~~COMkJHENTS :
I
TOTAL
VOLUME
REMOVE D
NOTE WATER LEVEL, PRODUCT LEVEL,AND WFLL DEPTH ARE REFERENCED TO~THE TOP OF WELL CASING
P - Ck
LJUF%V-rWVVr-n %,%JlVlr-pklj T
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
LOCATION : BURLINGTON, NC PROC NO :3500.1
PROJECT NAME: IBURLINGTON MGP (SHAL FRACT BR WELLS) FIELDCREWd -DC,RLVV
SAMPLING DATE :W,'M~j 20-Jal-04 21~~OmOi 9 a
MONITORING WELL NO .PMWL-SR
WATER LEVEL METER StN :N/A
PID READING PRODUCT LEVEL METER S/N ;tck 5 <i -
METHOD (Pump /Bail)1PERISTALTIC PUMP TIME / INITIALS OF COLLECTED SAMPLE :-x]
WELL VOLUME CALCULATION :
WELL WELL DEPTHHT0 WATER CONVERSION WELLCTR]
0 1DIAM DEPTH (ft)WFATTER fftot COLUMN (ft)X !FACTOR
2- 24.46 1 yc~X 0.163 10
X
N/A gallons X 3 .785 N/A liters
SCREENINTERVA L
FROM ft.1 TO DETECTED ODORS FREE PRODUCT MEASUREMENT
14.0 24 .0 Ift TYPE : IDEPTH TO WATER:
STRONG :DEPTH TO PRODUCT :---A"ONtE-n
MINOR, PRODUCT THICKNES &
Pump INTAKEJ NONE**I (ft)]DON'T SAMPLE IF THICKNESS >OR =TO 0 .1 FT 1
AT START AT
EN D
2 213
.0 ft .
NITIAL READINGS MEASURED AT GROUNDWATER AIR INTERFACE INDICATED BELOW
FLOWRATE TEMP SPEC TURBIDITY PH ORP DIS9OLVEDTIME/tj-.k LEVEL COND OXYGENAsk(hh :mm :ss) (ft)(ml/mi us/cm)(ntu) (unit)(mv) (mg/1)~w'I
N/A N/A N/A N/A N/A N/A N/A N/A N/A
W -R FLOWHATE TEM PATEC,(SPEC TURBID117 P"ORP DISSOLVED
TIME LEVEL COND OXYGEN(hh :mm :ss) (ft)(ml/min)(de,US/cm)(ntul (unit)(mv)(m A )
STABILIZED DRAWDOWN AND REMOVED BEGAN LOGGING DATA
13'L-t /'kzz;' I E,7-3 Z:N2-,-l 3%7-.5 o,
(3 S, rj Q 1 :3 .7-1 k,-2-L -ZZ C)
L345 5%9-1 \Z.k Vi 2.-SLj,3 ~%-1-1 2-0
1357-~,Lkz<~Q t%I -Lkv~ 1 1 2,-~.:l 0+L \7-
I v:y!'L / -k Z.~ C"'.3 %Lt'~&'4 -L-3-~ ~k (z ,-Lt ,
I Lkr-,q I L a I L(Q1 -L-j ID Q %7-S c.~zi III
I It
ELECTRONIC FILENAME -
OMMENTS :
N
OT W T L V L'
P 0
L~L-cc-'r -0
TOTAL VOLUME REMOVE D
OTE :WATER LEVEL, PRODUCT LEVEL,AND WELL DEPTH ARE REFERENCED TO ffiE Top FWELLZ~ASING .
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
LOCATION :-1 PROC NO :3500 .1
PROJECT NAME : BURLINGTON MGP (SHAL FRACT BR WELLS)FIELDCREW :j LDC,RLW
ISAMPLING DATE :19~Jan-04 I -MJan-04--+-Zr-Ua-n-ZZ-t-71-Uan-04 O C
MONITORING WELL NO .PNIWM-BR
WATER LEVEL METER SIN :
PID READING PRODUCT LEVEL METER SIN :
METHOD (Pump I Bail)1PERISTALTIC PUM :P~TIME / INITIALS OF COLLECTED SAMPLE :'t;2 ~f
WELL VOLUME CALCULATION :
CoWELL WELL DEPTH TO WATER CONVERSIO WELL)LUMN It Vol
DIAM DEPTH (ft)WATER (11)X
L Jai
2-19j6 X
X
N/A gallons X 3 .785 N/A Ilws
SCREENINTERVA L
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
is 19.16 Ift TYPE: DEPTH TO WATER :i
STRONG :EPTH TO PRODUCT~---(ft
MINOR :ODUCT THICKNE S
PUMP INTAKE IDON'T SAMPLE IF THICKNESS >OR TO 0 . 1 FT
,~,,ATSTART~ATEN D
INITIAL READING$ MEASURED AT GROUNDWATER AIR INTERFACE INDICATED BELO W
WATER FLOWHATF TEMP SPEC TURBIDITY PH ORP DISSOITIMELEVELICOND('tu)OXYGEN(hh :mm :ss) (it)(Mvmj (uS/cm)unit)(mv) (mg/1 )
N/A NIA N/A N/A N/A N/A N/A N/A NIA
WATER FLOWHATE TIzMP TURBIDITY PH ORP DISSOLVEDTIME LEVEL COND OXYGE N(hh :mm:ss) (it) (ml/min)(deg C) (us/cm)(nt (mv)(mgA)
STABILIZED DRAWDOWN AND REMOVED - BEGAN LOGGING DATA
(147 ;Z' 0 ;Z 57 4~,'q 5"12 3, ?2,31151 5-1 ;1-0-7 k 7LJ?.
U Uk 4 1 q 6, 0 ;x'3 a
HSL)I I D I 1~ I 1,31 12, 1 ?I'x
'q5 0 . 10- V 3 ;t 3t.,1 3-9 ?9
-5 L)1 ;~- I s ss 3,83 5 .C2 4
5 (I .?v --3 cA 5-')L4
>-L) jx-oo '4 3 o' (')5 .ci ~y
1'~'4 0 Li ~; 0 s 5- 1 3,59 7,1 -3 1 .31
i .)-,l 5-'-i3'0 ;~'-l 1 3,~LD 5~1 2
1 12--f 7 LJ t
ELECTRONIC FILENAME -A
AlIkC-OMME~NT-5
iTOTAL VOLUME REMOVE D
INOTE,WATER LEVEL .PRODUCT LEVEL,AND WELL DEPTH ARE REFERENCED TO THE TOP OF WEIL-CASIN G
I - I
0CHAINOFCUSTODYRECC.ID AND ANALYSIS REQUEST FORM--------------------
nalyfical Laboratory Service sDukeMail Code MG03A2 (Building 7405)1 "Page -A-oi
DISTRIBUTION*vEnergy..13339 Hagers Ferry Rd ORIGINAL to LAB ,
For Detailed Instructions, see : Kunteraville,N . C . 28078 COPY to CLIENT
http :1/de~1essenv/coc/ (704)875-524 5
Fa 4 )..............i:.C7~L . k ............
I)Prolect Name 2)F"ne No : uf~bzbl`
2 BURLINGTON MGP (OVERBURDEN WELLS)
2
E 3)Cllont C .Campbell R .Roberts 4)Fax No :875-6032
C17 C.1amPr a s1: 0,~3==H >EaIM
5)BusinessUnit : 20016 6)Process : 7)Rasp .To :0193 C
OE0 0
MGPBURL )Activity to: ALLACTV I O)Mall Code :MG03A 3-8)P,olect to Customer to comolete al l
anoropriate Nows <73
------------- 0 0 0
LAB USE ONLY 12 14COChem llection Information E <X
13 0 < W 00 LU tL 1-
"Lab to Desktop NO .Sample Description or ID Date Time q'q,-t -r-19 z 21 1 UJ 03
TRIP BLANK I-x 3 n/a 3
MW-3 x 1 3 '%,1 51
0 PMWB-S 004 11,301 kj,x i I i 1 3 5 1
E 4,P-is X I I 1 33L,I OIL 1515-1 4 0, 5 1
0 PMWC-S x ~L ~oc i c L:) X 1 1 3 54
MW-5 x 1 1 3 '~11 5
MIN-9 Y ocils o x I 1 3
PMWM-S I Z-3 . x 1 1 3
x 1 1 3.2 PIAWL-S 5
r
0 FIELD BLANK X I 1 3 5U50
Customer to sign &date belo w
21)Relin By DTIme
C
'2Requested Turnaround
'D 14 Days I/0
E :5
*7 Days
23)S*aVLocked By Datamme E we vo0 0 t:-48 Hr
A 'Other
Add .Cost Will Apply
Duke Duke Power Analytical Laborator yPower.Phone [phone] Fax 704-LI75-5038
~E~ C~ 13339 Hag~ers Ferry Road Huntersville,NC 28078-7929
McGuire Nuclear Compbx - MG03A 2
Ciertifiiicat4e of Anaiysis
Now York State Department of Health C-erldication #t 17f7
Oklahoma Department of Environmental Quality Certification # 9930
Kansas Department of Heath and Environment Certificate # E- f03 i I
North Carolina Department of 1-k-alth &Human Sewices Certification # 37804
South Carolina (DHE-Q Laboratory ID # 99005 North Carolina (()Bvi~ Certification #248
Sample ID #:24000578 Job#:04-JAN-0127
Sample Description :TRIP BLANK (OVERBURDEN WELLS )
Collection Date : 17-Jan-04 11 :00 :00 Site :BURLINGTON Sample Type: MGP SITE Desktop #
MGP PARAMETERS IN WATER BY GC/MS - 8260
Test Code : MS8260MGPW Test Method : SW-846 5030B18260B Date Posted : 02/02/04
Result ?222 9 L-t Flag
Benzene < 0 .60 pg/L 0.50 pg/L 0
Toluene < 1 .0 pg/L 1 .0 pg/L 0
Ethylbenzene < 1 .0 pg/L 1 .0 pg/L a
m-p-Xylene <2.0 Vg/L 2.0 pg/L 0
o-Xylene < 1 .0 pg/L 1 .0 pg/L 0
Naphthalene <2.0 pg/L 2 .0 pg/L I
RA-9
Sample[D#:24000679 Job#:04-JAN-012 7
Sample Description:MW-3 (OVERBURDEN WELLS )
ection Date : 21-Jan-04 11 :40 :00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
MGP PARAMETERS IN WATER BY GCIMS - 826 0
Test Code : MS8260MGPW Test Method : SW-846 5030131826013 Date Posted : 02102104
Resuft Repartingurritt Flag
Benzene < 0 .50 lig/L 0.50 Pg/L 0
Toluene < 1-0 pg/L 1 .0 p91L 0
Ethylbenzene <11-0 pg/L 1 .0 pg/L 0
m-p .Xylene <2 .0 pg/L 2.0 pg/L 0
o-Xylene < 1 .0 Vg/L 1 .0 Vg/L 0
Naphthalene <2 .0 pelt.2.0 pg/L 1
Sample]D#: 24000580 Job#: 04-JAN-012 7
Sample Description :PMWB-S (OVERBURDEN WELLS )
Collection Date : 2Wan-04 11 :30 :00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
MGP PARAMETERS IN WATER BY GCIMS - 826 0
Test Code : MS8260MGPW Test Method : SW-846 5030B18260B Date Posted : 02/02104
Result -.ReportingLan#Fla g
Benzene 120 pg/L 0.50 pg/L 0
Toluene 83 pg/L 11-0 pgtL 0
Ethylbenzene 250 pg/L 100 pg1L 0
m-p.Xylene 100 Vg/L 2 .0 vg/l.0
o-Xylene 77 P91L 1 .0 vg/L 0
Vkit o~on the Inu-nNo on
215120010-.42 1~Min Ild ....... I ....n,/Iih "15
~,hDuke Duke Power Analytical Laborator yFPower.Phone .[phone] Fax :704-875~5038
13339 HagersFefiry Road Hunteisville,NC28078-7929
McGuire Nuclear Complex - MG03A 2
C4ertifiq--at4e of &ftnaiysi s
New York Slate Department of Health Cerlithcatoon # f 1717
Oklahoma Department of Environmental Quality Certification # 9930
Kansas Department of Heath and Environment Carliticalle # E- fO3 f f
North Carolina Department of Health &Human Services Certification # 37BN
South Carolina (DHEQ Laboratory ID # 99005 North Carolina QBVF~ Certification #24B
Sample]D#: 24000680 Job#:04-JAN-012 7
Sample Description :PMWB-S (OVERBURDEN WELLS )
Collection Date: 21-Jan-0411 :30 :00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
MGP PARAMETERS IN WATER BY GC/MS -826 0
Test Code : MS8260MGPW Test Method : SW-846 5030B18260B Date Posted : 02102104
Result ffixiaing Limit Flag-
Naphthalene 1700 pg/L 200 pgtL
Sample[D#: 24000581 Job#: 04-JAN-0127
Sample Description :PAS (OVERBURDEN WELLS )
CollectionDate 21-Jan-0416 :15 :00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
MGP PARAMETERS IN WATER BY GC/MS - 826 0
0 Test Code: MS8260MGPW Test Method : SW-946 5030B18260B Date Posted : 02/02/04
Result Rel?artmq Limit Flag~
Benzene Is Pgf- 0.50 Pg[L 0
Toluene 2.3 VgIL 1 .0 pgfL 0
Ethylbenzene 41 pg/L 1 .0 pg/L 0
m-p-Xylene I I Vg1L 2 .0 pg1L 0
o-Xylene 44 pgVL 1 .0 pg/L 0
Naphthalene 70 pg/L 20 PgJL I
Sample ID #:24000582 Job#: 04-JAN-012 7
Sample Description :PMWC-S (OVERBURDEN WELLS )
Collection Date : 204an-04 11 :00:00 Site :BURLINGTON Sample Type: MGP SITE Desktop #
MGP PARAMETERS IN WATER BY GCIMS - 8260
Test Code : MS8260MGPW Test Method : SW-846 5030B18260B Date Posted : 02102/D4
Result Reporting Limit Flag~
Benzene 3.3 pq/L 0 .50 pg/L 0
Toluene < 1 .0 pg/L 1 .0 ug/L 0
Ethylbenzene 2.0 pg/L 10 Pg/L 0
rn-p-Xylene <2.0 pg/L 2 .0 pg/L 0
o.Xylene 4.2 pg/L 1 .0 ug/L 0
Naphthalene 110 pg/L 2 .0 pgtL I
vi,it at,th~lmraNcl at
Ph Duke Duke Power Analytical LaboratoryOFPower.Phone [phone] Fax:[phone]
A E-WC~13339 Hag ers Ferry Road HuntersvilleNC28078-7929
McGuire Nuclear Compbx - MG03A 2
Cliertifiti--at4e at jmnaiysi s
New York State Department of Health Cartification tl fl7f7
OklahorwDgpaHmentofEnvironrnentalOuehyCeHifeation#9930
Kansas Department of Health and Environment Certificate # E-f03l f
North Carolina Department of I-Laith &Human Services Certification #3780 4
South Carolina (DHEQ Laboratory 10 It 99M5 North Carolina QENF~Certification #246
~q
Sample ID #:24000583 Job#: 04-JAN-012 7
Sample Description :MW-5 (OVERBURDEN WELLS )
Collection Date : 20-Jan-04 09 :40 :00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
MGP PARAMETERS IN WATER BY GC/MS - 826 0
Test Code : MS8260MGPW Test Method : SW-846 5030BIS260B Date Posted : 02102104
Result --rtinqLmit a QAe~___ Aq
Benzene < G-SO pg/L 0 .50 pg/L 0
Toluene < 1 .0 VglL 1 .0 pg/L 0
Ethylbenzene < 1 .0 pg/L 1 .0 pg/L 0
m-p-Xylene <2.0 P91L 2.0 glL 0
o-Xylene < 1 .0 pg1L 1 .0 pg/L 0
Naphthalene <2.0 V911 . 2.0 pg& I
SamplelD#: 24000584 Job#:04-JAN-0127
Sample Description :MW-9 (OVERBURDEN WELLS )
Ilection Date: 211~Jan-04 09 :50 :00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
MGP PARAMETERS IN WATER BY GCIMS - 826 0
Test Code: MS8260MGPW Test Method : SW-846 5030B18260B Date Posted : 02102104
Result _Repqyin Limit Fla g
Benzene < 0.50 Vg/L 0 .50 Vgr- 0
Toluene 1 .0 pg/L 1 .0 pgfL 0
Ethylbenzene < 1 .0 lign. 1 .0 Pg/L 0
m-p-XyIene <2 .0 pg/L 2 .0 Vg/L 0
o-Xylene < 1 .0 pg/L 1 .0 Pg(L 0
Naphthalene <2-0 pg/L 2.0 Vg/L I
L
SamplelD#: 24000585 Job#:04-JAN-012 7
Sample Description :PMWM-S (OVERBURDEN WELLS )
Collection Date : 19-Jan-04 12:30:00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
7 77-
MGP PARAMETERS IN WATER BY GC/MS - 826 0
Test Code : MS8260MGPW Test Method : SW-846 5030B/8260B Date Posted : 02102/04
Result ---Flag_
Benzene 0.50 VglL 0 .50 Pq/L 0
Toluene < 1 .0 p9r .1 .0 pg/L 0
Ethylbenzene 1 .0 lign. 10 pg)L 0
m-p-Xylene <2 .0 pg/L 2 .0 pg/L 0
o-Xylene 1 .0 pg/L 1 .0 ug/L 0
Vuel .~n lh~ lnml,lo w
d -'151.'f)04 4?10 ~11- 11,1-.... .. . .
pkDuke Duke Power Analytical LaboratoryOPower.Phone [phone] Fox 704-875-503 6
13339 HagersFerry Road Huntetsvills,NC 28078-7929
McGuire Nuclear Complex - MG03A 2
Ctamrtifiq--at4e of Aftnalysi s
New York Slate 0epailment of Health Certification #tf7f7
Oklahoma Department of Environmental Quality Certification # 9930
Kansas Department of Health and Environment Cernifeale # E-fO3l f
North Carolina Department of Health &Human Services Certification # 37804
South Carolina (0HEQ Laboratory ID # 99X5 North Carolina (DEJO~ Certification #248
Samplell)#: 24000585 Job#:04-JAN-012 7
Sample Description :PMWM-S (OVERBURDEN WELLS )
Collection Date : 19~jan-04 12 :30 :00 Site BURLINGTON Sample Type : MGP SITE Desktop #
M~P -P A--RA-M-ETERS IN WATER BY GCiMS - 8260
Test Code : MS8260MGPW Test Method : SW-846 5030B/8260B Date Posted : 02102104
Resuft -feloorinig ur Flae~_
Naphthalene <2 .0 P91L 2 .0 pg/L I
SamplelD#: 24000586 Job#:04~JAN-012 7
Sample Description :PMWL-S (OVERBURDEN WELLS )
Collection Date : 20-Jan .04 16 :00 :00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
~:qrv-n'
MGP PARAMETERS IN WATER BY GC/MS -826 0
Test Code MS826DMGPW Test Method : SW-846 503013/8260B Date Posted : 02t,02104
Result Reporting Limit Flag-
Benzene < 0.50 pg/L 0.50 Veil- 0
Toluene < 1 .0 pg/L 1 .0 pg/L 0
Ethylberazene < 1 .0 pg/L 1 .0 pg/L 0
m-p-Xylene <2.0 pgh .2 .0 ug/L 0
o .Xylene < 1 .0 pgA- 1 .0 ug/L 0
Naphthalene <2.0 lig[L 2 .0 VgiL I
Ml;--aLA- L'fi
Sample ID #: 24000687 Job#: 04-JAN-0127
Sample Description :FIELD BLANK (OVERBURDEN WELLS )
Collection Date : 20-Jan-04 16 :06:00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
MGP PARAMETERS IN WATER BY GC/MS - 826 0
Test Code : MS8260MGPW Test Method : SW-846 5030B18260B Date Posted: 02JO2104
Result -..Reporting Lim-it Fla g
Benzene 0 .60 pg/L Me Vg/i. 0
Toluene < 1 .0 pg/L 1-0 P911-0
Ethylbenzene < 1 .0 pg/l . 10 Pg/L 0
m .p.Xylene 4 2 .0 pg/L 2 .0 pgiL 0
o.Xytene < 1 .0 Pg/L 1 .0 jug/L 0
Vma ts ..th~ IrtraNcl at
h1tp//dcN~w%v/esscnv/Iib srv/hill 1 4 IIJ5
phpuke Duke Power Analytical Laborator y#Power.Phone .[phone] Fax [phone]
A lMrFa,,Ga,d,13339 Hagers Ferry Road Huntersville,NC 28078-7929
McGuire Nuclear Comiobx - MG03A 2
Ciertifilii--att-- of Anaiysi s
Now York State Department of Health Cerlificabon N t 1717
Oklahoma Departhrient of Environmental Quality Cerhficalion # 9930
Kansas Department of Health and Environment Certificate # E- t03 f f
North Carolina Department of Health &Human Services Certification #37W4
South Carolina (DHEQ Laboratory ID # 99005 North Carolina (DENR Certification #246
-11 I'll,
SamplelD#:24000687 Job#: 04-JAN-012 7
Sample Description :FIELD BLANK (OVERBURDEN WELLS )
Collection Date : 20-Jan-04 16 :05 :00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
MGP PARAMETERS IN WATER BY GCIMS - 8260
Test Code : MS8260MGPW Test Method : SW-846 6030818260B Date Posted : 02102/04
--.-Resuft !Zepaorting Limit Flag_
Naphthalene <2 .0 pg/L 2 .0 pgVL i
------------------------------------
Description af Flacfs :
0 -All Anal"caJ Procedlittre Req-rements Were Met
I . See C .- N-1. o .
2 - C ..... trat ....Sea Co-
3 Repent 1,r-, M eo .,.d did 1..-pl . -m
a Report 1-n-1 El-aled d.. 1. r.1.-d anatti-ral
5 .Sample R ... 11 . Sh..ld No,Be U ad F- Rcr..lai .r,1P,t ......(Sea C ...
6 . Adel,
. d
.la .led be[.-r .,dm .e ],.it .1 - alannea ..
-conerim ..
7 - Reported concentration * me comt,maloon of more that one aroolor .
felepo - led Araciar- IS -the AroC10, - of h,gh**l concentration - the amp*)_-- ---- ---- ---------------- at--O~z
By.Date
0
Visit its or, th,, IntraNcl at
. ...... ....11-4:19 hupJ/dewww/esscit srv/"J5
phpuke Duke Power Analytical Laborator y
0'Power.Phone.[phone] Fax:[phone]
13339 Hag ers Feriy Road Hunteisville,NC 28078-7929
McGuire Nuclear Comp)ex - MG03A 2
4r, te r it i r j 4r- a t 4-- 46 1 An n -a I y s. i
Now York State Department otHealth Certification # I f717Oklaborm0apartrwntofEwiron"ntelOuebtyCoHificalion #9930Kansas Department of Heath and Ervironment Certificate #E-103f fNorth Carolina Department of PRallh &Human Services Cerifficalion It 378N
South Carolina QhEiq Laboratory ID # 99005 North Carolina (DBVR Certification #248
!~~atjon Nam~:BURLINGTON Job Number:04-JAN-0127
Sample ID #:24000579 Desktop #Customer ID :R . ROBERTS
Sample Description : MW-3 (OVERBURDEN WELLS )
Collection Date : 21-Jan-04 11 :40 :00 Date Received in Laboratory : 07~Jan-04 TypeofSample :MGPSITE
7--
ReferenceMethod EPA310,1/SM2320B Date Posted : 21312004 11 :58 :58
ALKALINITY (TOTAL INFLECTION POINT)ALKALINITY 0 .76 meg/L.
ReferenceMetinDd EPA200.71601013 Data Posted : 1/30/2004 11 :03 :3 5
IRON BY ICP (DIGESTg.D)____IRON 0.742 mg/I
ReferenceMethod EPA200 .7160108 Data Posted: 1/30/2004 11 :03 :3 6
MANGANESE BY ICP (DIGESTED)MANGANESE 0 .055 mg/!___
Referen" Method EPA 300 .0 Data Posted: V28/2004 13 20 4 5
NITRATE (IC)_NITRATE 2 .8S.,mg!L-
Referent;e Method EPA 300 .0 Data Posted : V28/2004 16 :54 :0 9
NITRATE By CALCULATION (WG-N/L)___NITRATE 0 .64 mg-N/L
ReferenwMethod EPA300.0 Data Posted : 1/2812004 13:20 :4 5
SULFATE (IC)SULFATE 11 .90 M91L-
Sampie ID #:24000580 Desktop #Customer ID :R . ROBERTS
Sample Description : PIdWB-S (OVERBURDEN WELLS )
CollectionDate : 21-Jan-0411 :30 :00 Date Received in Laboratory : 07~Jan-04 TypeofSample :MGPSITE
ReferenceMethod EPA310 .11SM2320B Data Posted : 213/2004 11 :58 :5 8
ALKALINITY (TOTAL INFLECTION POINT)ALKALINITY 6 .63 meql!,__
ReferenceMethod EPA200Y/6010S Data Posted V3012004 11-03 :36
Al11-GESTED)-IRO NIRON BYICIP 28 .498 m9l
ReferenwMethod EPA200,71601013 Data Posted : 113012004 11 :03:36
MANGANESE BY ICP DIGESTED)MANGANESE 0.181 rn /L
Referent;e Method EPA 300 .0 Data Posted : It2M004 13 :21 :0 8
JI-1TTR&T-E[lC-)-NITRATE 0 .82 mg/L_
Reference Method EPA 300.0 Data Posted: 1/2817004 16 :54 :1 1
NITRATE BY CALCULATION (MCL-NlL)__--NITRA TE 0.19 mg-WIL
Referen,;eMetho,d!EPA300 .0 Data Posted : 1/28/2004 13:21 :08
SULFATE (11C)SULFATE 22.94 mg/L
Visit us on the IntraNei at
Rer,urf Generuied 2 j,2004 09.31 23 hup ://de~iv/essenW1ab-srv/
PkDuke Duke Power Analytical Laborator y,rPower.Phone [phone] Fox.701-875..5036
A ~ Ep C", 13339 Hagers Ferfy Road Huntersvillit,NC 280 78-7929
McGuire Nuclear Complex - MG03A 2
4-. rt i I i c--a t o-- cm,r Atxnaiysis,
New York Slate Department ofHealth Certification # f ff17Oklahoma Department of Environmental Quahly Canificabon # 9930Kansas Department of Heath and Environment CerfifAcale # E. 103 f I
North Carolina Department of i ~eallh &Human Services Certification # 376N
South Carolina (DiiEQ Laboratory 10 # 99005 North Carolina (DENO-Cerblicabon #248
Station Name :BURLINGTON Job Number:04~JAN-01127
Sample ID 24000581 Desktop #Customer ID,R . ROBERTS
Sample Description:P-1S (OVERBURDEN WELLS)
CollectionDate: 2Wan-0415 :15 :00 Date Received in Laboratory : 07~Jan-04 TypeofSample :MGPSITE
ReferenceMethod :EPA310.1/SM2320B Dam Posted : 213/20014 11 :58 5 8
ALKALINITY (TOTAL INFLECTION POINT)ALKALINITY 6 .61 meq/L
Reference Method :EPA 200 .7/6010B Data Posted : 113012004 11 :03 :37
[RON BY ICP (OnESTED IRON 13 .210 nq 11j-- -9-
Reference Method :EPA 200 .71601013 Data Posted : MO/2004 11 :03 :37
MANGANESE BY ICIP (DIGESTED)_MANGANESE 2 .721 nng/L____
Reference Method:EPA 3DO.0 Data Posted: 1/28/2004 13 :22:1 2
NITRATE (IC)0 .10
Reference Method EPA 300.0 Data Pos,ted: 112812004 16 :54 1 2
NITRATE BY CALCULATION (MG-NIL)__NITRATE <0.02 mg-NIL
Reference Method :EPA 300 .0 Data Posted : 1128/2004 13 :22 1 2
SULFATE (KC)SULFATE 20 .19 nnG/L
Sample ID #:24000582 Desktop It Customer 10 :R- ROBERTS
Sample Description : PMWC-S (OVERBURDEN WELLS )
CollectionDate : 204an-0411 :00 :00 Date Received in Laboratory : 07-Jan-04 Typeol'Sample :MGPSITE
ReferenceMethod EPA310 .11SM2320B Data Posted : 2/312004 11 58 58 'pl-
ALKALINITY (TOTAL INFLECTION POINT)_ALKALINITY I ag ---IL X-50 -%qj .!5
ReferenceMethod :EPA200 .71601013 Data Posted: 1130/2004 11 :03 :3 7
IRON BY ICP (DIGESTED)___IRON 23 .223
ReferenceMethod:EPA200 .7/6010B Data Posted : 1/30/2004 11 :03:38
-- -MANGANESE BY ICP(DIGESTE )__ ___MANGANESE 2.521 mg/L
Reference Method : EPA 300.0 Data Posted : 1/2812OD4 11 :10 :4 6
NITRATE (LC)___NITRATE < 0 .10 mg/L
Reference Method EPA 300.0 Data Posted : 112aI2004 16-48 24
NITRATE BY CALCULATION (qG-NAL)-_.NITRATE <0 .02 mg-WIL
Reference Method EPA 300 .0 Data Posted : 1/28/2004 11 :10:4 6
- - ---SULFATE (IC)_SULFATE 0.16 mgLL,
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PkDuke DukePowerAnalytical Laboratory0,Power.Phone 704-B75-5245 Fax [phone]
A ~E~ C~ 13339 Hagers Ferry Road Huntersville,NC 28078-7929
McGuire Nuclear Complex - MG03A 2
4611 Ainmiysi --%
New York Slate Department of Heaflh Certification # I f 7 V
Oklahoma Department of Environmental Quality Certification # 9930
Kansas Deparlintint of Heagh and Environment Certificate # E- f03 f I
North Carolina Deparinient of 1-kelth &Human Services Cerliticalion #37804
South Cgroturia (DHEQ Letioratory ID # 99005 North Carolina (DENR Certification #24 6
Station Name :BURLINGTON Job Number :04-JAN-0127
L
Sample ID #: 24000583 Desktop If Customer ID :R . ROBERTS
Sample Description : MW-5 (OVERBURDEN WELLS )
Collection Date : 20-Jan-04 09 :40 :00 Date Received in Laboratory : 07-Jan-04 TypeofSample :MGPSITE
Reference Method :EPA31 0 .I/SM2320B Data Posted 2/3/2004 11 :58 5 8
ALKALINITY (TOTAL INFLECTION POINT)ALKALINITY 9 .25 meq/L
ReferenceMethod .EPA200 .7/6010B Data Posted : 1130/2004 11 :03 :3 8
-------IRON Y~ICP DIGESTED IRON 5 .076
Referenm Method :EPA 2GO.71601 08 Data Posted : 113012OG4 11 :03:38
MANGANESE BY ICP (QnES~TED MANGANESE 0 .531
Referen~ Method:EPA 300.0 Data Posted: 112812004 1 VI 1-0 7
NITRATE (IC)___--NITRATE 0 .10 mg/L
Referert Method EPA 300.0 Data Posted : 1128/20D4 16 :48 :26
NITRATE BY CALCULATION (MG-NIL)- -----NITRATE --- <0 .02,_mg-N/L
Reference Method :EPA 300 .0 DataPosted 1/2812004111107
SULFATE VC)SULFATE 31 .88 mg[L
Sample ID #:24000584 Desktop #Customer ID:R . ROBERTS
Sample Description : MW-9 (OVERBURDEN WELLS )
Collection Date : 214an-04 09 :60:00 Date Received in Laboratory: 07~Jan-04 TypeofSample :MGPSITE
ReferenwMethod EPA310.11SM23208 Data Posted 213/2004 11'58 58
ALKALINITY (TOTAL INFLECTION POINT)---ALKALINITY 5 .49 T _L.9V
Refersi Method :EPA 200 .71601 OB Data Posted : 1/30120G4 11 :03:39
IRON BY ICP (DIGESTED)IRON 0 .087 mg_/L__,
Refereni;e Method :EPA 2003160108 Data Posted 113012004 11 033 9
MANGANESE BY ICP (QKGESTED)_MANGANESE --0 .011 mg/!-_
Referenm Method :EPA 300.0 Data Posted 1/28/2004 13223 7
NITRATE (Lq)_NITRATE 7 .05_mg/L
Reterenots Method EPA 300o Data Posted 1128/2004 16 54*1 3
---NITRATE BYCALCUUTI0NLMG-_N/L)____ _ __ _M/TRATE ._,__1.59 njg-N/L
Reference Method :EPA 300 .0 Data Posted 1128120134 13223 7
SULFATE (IC)SULFATE 53 .26 mg/L
Visit its ort th~ Int,"t
Rep(,, Generaled 2 S 2004 0:31 23 Ishii //dc~Ies,,,nAaIh-srv/
pkvuke Duke Power Analytical Laboratory
0,Powera,Phone [phone] Fax:[phone]
13339 Hagers Ferry Road HuntelsvdAD,NC 28078-7929
McGuire Nuclear Compilex - MG03A 2
4-- r t i r i 4--a t 4--4o r A n a i y s.
New York Slate Department of Health Certification # f 1717
Oklahoma Department of Environmental Quality Certification N 9930
Kansas Department of Heath and Environment Certificate # E. f031 fNorth Carolina Department of Health &Human Services Certification N 37804
South Carolina (DHEC)Laboratory 10 #99W5 North Carolina (DENF~Certification It 248
-Station Name :BURLINGTON Job Number :04-JAN-0127
Sample ID #:24000585 Desktop #Customer ID :R . ROBERTS
Sample Description : PMWM-S (OVERBURDEN WELLS )
Collection Date: 19-Jan-04 12 :30 :00 Date Received in Laboratory : 07-Jan-04 Typeol'Sample :NIGPSITE
ReferenceMethod :EPA310.11SM2320B Data Posted : 213/2004 11 58 5 8
ALKALINITY (TOTAL INFLECTION POINT ALKALINITY ......11,39 rri
Referenceltilethod :EPA200 .716010B Data Posted : 113012004 11 :03 :39
IRON BY ICP (DIGESTED IRON 0 .086 rngfl
Referen,:e Method:EPA 200 .716010B Data Posted 1/3012004 11 :03 :40
MANGANESE BY ICP (DIGESTED)-MANGANESE 0 .036 mg-IL-
Referenm Method:EPA 300 .0 Data Posted 1/23/2004 14 35 5 0
NITRATE,VC)_____.__NITRATE 4 .27 _mgfL
Reference Method EPA 300.0 Data Posted: 1/2312004 16 :11 :04
NITRATE BY CALCULATION (IkLG-NIL)_____NITRATE 0.96 mg .N/L
Referenm Method EPA 300.0 Data Posted : 1/2312004 14 :35:50
SULFATE (IC)__SULFATE ______18.14 mg/L
Sample ID #:24000586 Desktop #Customer ID :R . ROBERTS
Sample Description : PMWL-S (OVERBURDEN WELLS)
Collection Date : 20~Jan-04 16 :00:00 Date Received in Laboratory : 07-Jan-04 Type of Sample : MGP SITE
Reference Method :EPA310.1/SM2320B Data Posted 2IM004 11 :58 :58
ALKALINITY (TOTAL INFLECTION POINT)ALKALINITY .......A53 meq/L
ReferenoeMethod EPA2DO.7/60108 Data Posted : 113012OD4 11 :03:40
- - -lRONBY ICP (DIGESTED .IRON 53.311 mg/I
ReferenceMethod EPA200.7160108 Data Posted 1/30/2004 11 :03 :4 0
MANGANESE BY ICP (DIGESTED)-MANGANESE 2 .074 mgIL
Reference Method EPA 300 .0 Data Posted 1/28/2004 11 :11 :3 5
NITRA E (IC)NITRATE
Reference Method.EPA 300 .0 Data Posted 1128/2004 16 :48 :27
NITRATE BY CALCULATION (MG--NfL)--NITRATE 0 .02 mq-NIL
Reference Method :EPA 300 .0 Dam Posted 1/28/20G4 11 :11 :3 5
SULFATE (IC)-SULFATE .-14 .49 mg/L
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*Duke Duke Power Analytical Laborator y
Power.Phone [phone] Fax.[phone]
13339 HagerS Per/yRoad Hunteisvilb,NC 28078-7929
McGuire Nuclear Comipt~x - MG03A 2c 4-- rt i r i 4--.a t #I--a I AL in za i i
Now York Stale Department of Health Cerhhcalion #I f 717
Oklahoma Department ofErwironrnentsiQuai)tyCertifA~ation #9930
Kansas Department ofHeagh and Environment Certificate #E-1031 1
North Carolina ELpariment ofi0alth &Human Services Certification #37804
South Carolina QHEQ Laboratory ID # 99W5 North Carolina (DENR Certification #248
Station Name :BURLINGTON Job Number :04,JAN-0127
Sample ID #: 24000587 Desktop #Customer ID :R . ROBERTS
Sample Description:FIELD BLANK (OVERBURDEN WELLS )
Collection Date: 20-Jan-04 16 :06 :00 Date Received in Laboratory : 07~jan-04 TypeofSample :MGPSIT E
Reference Method :EPA310.11SM2320B Data Posted : 2WO04 11 58 5 8
ALKALINITY (TOTAL INFLECTION POINT _ALKALINITY 0.01 meqLL
Referer~ltffiethod :EPA200 .7/601013 Data Posted:I/30f2004 11 :03 4 1
IRON BY ICIP (DIGESTED)IRON <
Referen~ Method :EPA 200 .716010B Data Posted : 1130/2004 11 034 1
MANGANESE BY ICIP (DIGESTED)____MANGANESE < 0.006
Referenos Method EPA 300.0 Data Posted : 1/2812004 13234 7
NITRATE (IC NITR4TE < 0.10
Referenm Method EPA 300.0 Data Posted : 1/2WOD4 1654 1 4
NITRATE BY CALCULATION (MG-NIL)_NI-TP.4TE-------0 .02 mq-N/L
Referent;e Method :EPA 300 .0 Data Posted: 112a12004 13 23 47
~ULFATE (IC)SULFATE < 0 .10 mg/L___
a-1,VefdbdawtPtaw~ By.Date
0
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CHAIN OF CUSTODY READ AND ANALYSIS REQUEST FORM
Analytical Laboratory Services iDuke----- -- *-'-* ------- * ---------1 9
Mail Code MG03A2 (Building 7405)
Page -L of
DISTRIBUTION?DwEnergya.13339 Hagers Ferry Rd
For Detailed Instructions, see
: Huntereville,N . C . 28078 ORIGINAL to LAB,
hUpI/cle~/essenv/coc/ Fa (704)
$75-5245 COPY to CLIENT
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I)Pfolect Name Z)Pnone No : urS-5257
BURLINGTON MGP (SAPROLITE WELLS)
E 3)CIIent C .Campbell R . Roberts 4)Fax No :875-5032 16p,sem .:I=C
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LABUSEONLY ollection Information 0 'K"Chem E ,i <x
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PM WB-D f tj -Cwtx x 1 1 3 5
PMWC-D J1 e~~X 1 1 1 1 1 3 5
PMWF-D jQr-, i~~;VA-.1 x 1 1 1 3 5
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CHAIN OF CUSTODY RECORD ANDANALYSIS REQUEST-FORM
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: MG03A2 (Building 7405)MDEnergya .1 13339 Hagers Ferry Rd DISTRIBUTIO N
Hunteraville,N . C. 28078 ORIGINAL to LAB,
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BURLINGTON MGP (SAPROLITE WELLS)
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XLjO0 PMWB-D x 1 1 3
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CHAIN OF CUSTODY RE04D AND ANALYSIS REQUEST FORM--------------- -----------------n ...--- - ---------
Duke Analytical Laboratory Services i i .110-11105
Mail Code MG03A2 (Building 7405) "Page --L of
DISTRIBUTION*wEnergy.13339 Hagers, Ferry Rd ORIGINAL to LAB,
For Detailed Instructions, see
: Huntersville,N . C . 2807 0
hltp*J/c1e~1essenv/coc/ [phone] COPY to CLIENT
F a..............~:.ULN T-5:~Q:Lk .............
1)Project Name 2)Phone NO : 87~5257
BURLINGTON MGP (SAPROLITE WELLS)
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;Lqm PMWB-D x I 1 3 5
PMWC-D x 1 1 3 5
PMWF-D x 1 1 3 5
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PMWI x 1 1 3 5
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February 6,2004 11 :50 :42 AM Page #1 of I
Duke 8260 Analysis
drEnergy.. Case Narrativ e
rrhis document must acmmpany release of Analytical Data)
ILIMS Job #04-JAN-0130
Workfist #04-FEB-002 6
*The percent drift and/or recovery for the continuing calibration standard for naphthalene
exceeded the laboratory quality control limits . The results for this compound should be
considered estimates .
*The percent recovery for the laboratory control sample for naphthalene exceeded the
laboratory quality control limits . The results for this compound should be considered
estimates .
------------- ----------------Iher ihames
--------------------------------------------------------------------------------------
Duke Energy Analytical Laboratory Service s
Environment Heath &Safety Services Environmental Center - MG03A2
Phone :7D4-875-5245 13339 Hagers Ferry Road
FAX:[phone] Huntersville NC 28078-7929
EACasc NarraIivm\Org2nic\VOA\04-JAN-0l 30 .doc
P MiCe IJUKe rower Anaiyucal LaDoratoryoftwer.Phone 701-67S5245 Fox 704-675.503 8
A ~15~ C~ 13339 Hagers Ferry Road HuntefsvilbNC28078-7929
McGuire Nuclear Complex - MG03A 2
ctertill4catte cor A%n a i
Now York Slate DEpartmentofHealth Cartification # ff7f7OklahornaE)apartrmnlofEwironn)entafQuablyCerfoicalionngg3o
Kansas Department of Heath and Environment Certificate # E-jo3f f
North Carolina Department of Health &Human Services Ceriffication If 37804
South Carolina (DHEQ Laboratory ID N 99005 North Carolina (DBVF~ Certification #248
Station Name :BURLINGTON Job Number:04-JAN-0130
i
Sample ID #24000595 Desktop #Customer ID*R. ROBERTS
Sample Description : PMWB-1D (SAPROLITE WELLS )
Collection Date : 21-Jan-04 13 :35 :00 Date Received in Laboratory : 07-Jan-04 Type of Sample :MGP SITE
ReferenceMethod : EPA310 .l/SM2320B Data Posted 2/3/2004 11 58 58
ALKALINITY (TOTAL INFLECTION POINT)ALKALINITY 3 .26 meq/L
Refere~ Method :EPA 200 .7/6010B Data Posted . 1/30/2004 11 :03 4 1
IRON BY ICIP (PtIESTED)IRON 13 .970 mgII
Referenm Method :EPA 200 .71601 OB Data Posted: 113012004 11 :03 4 2
MANGANESE BY ICP (DIGESTED)MANGANESE 3 .603 mg/L
Referenm Method:EPA 300.0 Data Posted I t2B/2OD4 13 :24 1 5
NITRATE IC)NITRATE < 0.10 mg/L
Reference Method :EPA 300 .0 Data Posted . 1/2812004 16 :54 :1 5
NITRATE BY CALCULATION (MG-NIL)NITRATE <0 .02 mg-N/L
Referen~ method :EPA 300 .0 Data Posted : 1/28/2004 13:24 1 5
SULFATIEflC),SULFATE < 0.10 mg/L
Sample ID #:24000596 Desktop #Customer ID :R .ROBERTS
Sample Description : PMWC-D (SAPROLITE WELLS )
Collection Date : 204an-04 15 :15:00 Date Received in Laboratory : 074an-04 Type of Sample MGP SITE
ReferenceMeth0d :EPA310 .11SM23208 Data Posted : 21312004 11 :58 :58
ALKALINITY (TOTAL INFLECTION POINT)ALKALINITY 5 .13 meqlL )ISO
Reference Method :EPA 2GO .7/6010B Data Posted : 113012DO4 11 :03 :4 2
[RON BY ICIP (DIGESTED)IRON 9 .678 mg/I
Reference Method :EPA 200 .7/601 OB Data Posted : 1/3012004 11 0342
MANGANESE BY ICIP (DIGESTED)MANGANESE 8.448 mg/L
Referenm Method :EPA 300.0 Data Posted 112812004 11 122 7
NITRATE IC)NITRATE < 0.10 mg/L
Reference method EPA 300 .0 Data Posted 1/28/2004 1648 28
NITRATE BY CALCULATION (MG-N/L)NITRATE <0 .02 nng-N/L
Referent;e Method .EPA 3000 Data Posted : 1128/2004 11 122 7
SULFATE IC)SULFATE < 0.10 rngIL
le .....G~,,,,aM 2,%/2(X'4 /1 15 29 hill,I/dww ./csscnv/lab-srv/
Duke UtlKeFowerAnaiyucal LaDoratory
Power.Phone [phone] Fax [phone]
I3339Ha9orSFerIYR00d Huntersinitle,NC28078-7929
McGuire Nuclear COMPiex - MG03A 2
a,1 Axmaiy--~us
Now York State GLeloadment of Health Certification # f f7f7Oklahoma Department of Ervironmental Quality Certification #9930Kansas Department of Heath and Environment Certificate # E-103f INorth Carolina 09pall of Heafth &Human Services Certification N 378 NSouth Carolina I'l Laboratory ID # 99005 North Carolina (DENF0 Certification #248
Station Name :BURLINGTON Job Number :04-JAN-0130
Sample ID #: 24000597 Desktop #Customer 10 R . ROBERTS
Sample Description : PMWF-D (SAPROLITE WELLS )
Collection Date : 20-Jan-04 10 :50:00 Date Received in Laboratory : 07-jan-04 TypeofSample :MGPSITE
ReferenciiiMethod :EPA310 .11SM232013 Data Posted : 2/3/2OD4 11 :58 58
ALKALINITY (TOTAL INFLECTION POINT)ALKALINITY 10 .01 meq/L
ReferenceMethod EPA200 .715010B Data Posted : 1130/2004 11 :03 :42
IRON BY ICP (DIGESTED IRON 12.380 mgfl
ReferenceMethod : EPA200 .716010B Data Posted : 113012004 11 :03 :4 3
MANGANESE BY ICP (DIGESTED)MANGANESE 4 .659 mg/L
Referenceflethod EPA300 .0 Data Posted : 1/28/2004 11 12 4 7
NITRATE (IC)NITRATE < 0.10 mg/L
Reference Method:EPA 300b Data Posted: V2812004 16 48 29
.NITRATE BY CALCULATION (MG-NIL)NITRATE <0 .02 mg-NIL
Reference Method :EPA 300o Data Posted : 1/2812004 11 12 :4 7
SULFATE IC)SULFATE 0 .66 mg/L
Sample ID li 24000598 Desktop #Customer ID R . ROBERTS
Sample Description : PMWG-D (SAPROLITE WELLS)
Collection Date : 19-Jan-04 16 :15:00 Date Received in Laboratory : 07-Jan-04 TypeofSample :MGPSITE
ReferenceMethod EPA310 .11SM2320B Data Posted: 2rJI2004 11 58 5 8
ALKALINITY (TOTAL INFLECTION POINT)ALKALINITY 3.50 meq/L
ReferenceMethod EPA2DO.716010B Data Posted:V30/2004 11 :03 :4 3
IRON BY ICP (DIGESTED)[RON 0 .134 mg/I
Reference Method :EPA 200.7/601 OB Data Posted : 1/3012004 11 03,4 3
MANGANESE BY ICP (DIGESTED)MANGANESE 1 .585 mg/L
Reference Method EPA 300 .0 Data Posted : 1/29/2004 10 :51 :6 9
NITRATE IC) NJ TRA TE 3 .43 mg/L
Reference Method .EPA 300 .0 Data Posted : 2/6/20G4 10 47 58
NITRATE BY CALCULATION (MG-NIL)NITRATE 0 .77 mg-l
Reference Method :EPA 300o Dam Posted: 112912004 10~51 :59
SULFATE (IC)SULFATE 19.10 mg/L
Vim,. ..... ih~ I. . .. ~,,V MY6120114 /1 15 29 h1lp ://dcwww/csscnv/lah-srv/
P Duke Duke Power Analytical Laborator yNower.Phone 704-87-'L5245 Fax 704 .875,5038
A Ak~,G~13339HagerSFer(YROad Hvntersv#ADNC28076-7929
McGuire Nuclear CompAax - MG03A 2
C4--rtific~att-- cior Am na i y --%i s
New York State Department of Health Certification # I l7f7OklahomDeparirnentofEwironrwntaiQuahtyCLrtjftcationN9930
Kansas Department of HeaRh and Environment Cerifficate N E-fO3f fNorthCarolina Department of Health &Human Services Certification #37804
South Carolina (0HEQ Laboratory ID #99005 North Carolina QENF~ Certification #24 6
Station Name :BURLINGTON Job Number :04-JAN-0130
Sample to #:24000599 Desktop #Customer ID :R . ROBERTS
Sample Description : PMWI (SAPROLITE WELLS )
Collection Date : 119~Jan-04 15 :45 :00 Date Received in Laboratory : 07-Jan-04 Type of Sample MGP SITE
ReferenceMethod :EPA310 .11SM2320B Data Posted. 2/312004 11-58 58
ALKALINITY (TOTAL INFLECTION POINT)ALKALINITY 3 .32 meqIL
ReferenceMethod :EPA200 .7160108 Data Posted : V3012004 11 :03 :4 4
IRON BY ICP (DIPESTED)IRON 0.676 mg/I
ReferenceMethod :EPA200.7/6010B Data Posted 113012004 11 .03 44
MANGANESE BY ICP (DIGESTED)MANGANESE 0 .230 mg/L
Reference Method :EPA 300 .0 Data Posted . 1/29/2004 10 .55 :54
NITRATE (IC)NITRATE 0.15 mg/L
Reference Method :EPA 3GO .0 Data Posted 21612004 10 48 02
NITRATE BY CALCULATION (MG-N/L)NITRATE 0 .03 mg-NIL
Reference Method :EPA 300 .0 Data Posted : V2912004 10 :55 54
SULFATE ICJ SULFATE 7 .68 mg/L
Sample ID #24000600 Desktop #Customer 10 :R . ROBERTS
Sample Description : PMWL-D (SAPROLITE WELLS )
Collection Date : 2Wan-04 09 :50 :00 Date Received in Laboratory : 07~,Ian-04 TypeofSample :MGPSITE
ReferenceMethod:EPA31O .ItSM2320B Data Posted: V312004 11 :58 :58
ALKALINITY (TOTAL INFLECTION POINT).ALKALINITY 2.79 meq/L
ReferenceMethod :EPA200.716010B Data Posted . 113012004 11 :03 :4 4
IRON BY ICP (DIGESTED)IRON 0 .447 mg/I
Reference Method :EPA 200.7/60108 Data Posted : 1/3012OG4 11 :03 4 5
MANGANESE BY ICIP (DIGESTED)MANGANESE 0.228 mg/L
Reference Method :EPA 300o Data Posted:112812G04 13 24,4 1
NITRATE IC)NITRATE < 0 .10 mg/L
Reference Method :EPA 300 .0 Data Posted 112812004 16 54 1 6
NITRATE BY CALCULATION (MG-N/L)NITRATE <0 .02 mg-NIL
Vkil fh~ 1,,.,.No IH 21612004 /1 /j 29 IiItp://dcwww/esicnv/Iab-srv1
P Duke Duke Fower AnalyLicat LaDoratof yNower.Phone .[phone] Fax.[phone]
13339 HagersFerly Road Huntersvibig,NC28078-7929
McGuire Nuclear Complex - MG03A 2
C 4e rtiti 4r-atc-- cof Am n a iyt--.i -s
New York Slate Department of Health Certification #f f 717
Oklahoma Department of Environmental Ouably Caildration # 9930
Kansas Department of Heath and Environment Certificate # E- 103f f
North Carolina Department of Health &Human Services Certification # 378N
South Carolina (DHEC)Laboratory ID N 99005 North Carolina (DENR CerIfficabon If 248
Station Name :BURLINGTON Job Number :04-JAN-0130
Sample ID #:24000600 Desktop #Customer ID :R . ROBERTS
Sample Description : PMWL-D (SAPROLITE WELLS )
CollectionDate : 21-Jan-0409 :50 :00 Date Received in Laboratory : 07-Jan-04 Type of Sample : MGP SITE
Reference Method :EPA 300.0 Data Posted 1/2812004 13*24 4 1
SULFATE (IC)SULFATE 25 .66 mg/L
--L("0-t-04-k1a VenhW and Aponived Syr Date
Vj,i,, n tl,~I. . .r~No a l
R~M,ri 216120114 11 15 29 http :Hdc%Yww/csscnv/Iab-srv/I
PW UU11e 1)U KeFowerAnaiyucal LaDorator yOFPdwer.Phone [phone] Fax [phone]
13339 HegersFeny Road HunterstrilleNC28078-7929
McGuire Nudear CompAqx - MG03A 2
Ctertificatie of Analysi s
Now York State Department of Health Codification # 117f 7
Okfahoma Department of Enwronmentai Quably Codification # 9930Kansas Department of Heagh and Enwronment Certificate # E. f03f l
North Carolina Department of Haallh &Human Services Cedification # 37804
South Carolina (DHEQ Laboratory ID # 99GO5 North Carolina QENF~Codification ft 248
samplelD#: 24000596 Job#: 04,JAN-013 0
Sample Description :PMWB-D (SAPROLITE WELLS )
Collection Date : 2Wan-04 13 :35:00 Site :BURLINGTON Sample Type: MGP SITE Desktop #
MGP PARAMETERS IN WATER BY GCIMS - 826 0
Test Code : MS8260MGPW Test Method : SW-846 5030B18260B Date Posted : 02/02104
Result Reporting Lumut Flag
Benzene 35 pg/L 0 .50 Pq/L 0
Toluene 1 .4 pgAL 1 .0 P91L 0Ethylbenzene9.0 Poll- 1 .0 Pq/L 0
m-p-Xylene 6 .7 pg/L 2 .0 Pg/L 0
o.Xylene to Pg/L 1 .0 Pg/L 0
Naphthalene 300 jig/L 20 pgiL I
KMSMEM Y7--
Sample ID #:24000596 Job#: 04-JAN-013 0
Sample Description :PMWC-D (SAPROLITE WELLS )
n .t. 20,Jan-04 15 :16:00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
'Row
MGP PARAMETERS IN WATER BY GC/MS -826 0
Test Code, MS8260MGPW Test Method : SW-846 503OB18260B Date Posted : 02102104
Result Repoilting Limit Flag
Benzene 110 Vg/L 0 .50 PA 0Toluene9.8 Pg/L 1 .0 PgtL 0
Ethylbenzene 86 pg/L. 1 .0 PgIL 0
m-p-Xylene 33 VWL 2 .0 P91L 0
o-Xylene 37 Vg1L 1 .0 pg/L 0
Naphthalene 1500 pg/L 200 pgtL I
SamplelD#:24000597 Job#: 04-JAN-0130
Sample Description :PMWF-D(SAPROLITE WELLS )
CollectionDate 20-Jan-0410 :50 :00 Site :BURLINGTON Sample Type: MGP SITE Desktop #
MGP PARAMETERS IN WATER BY GC/MS - 826 0
Test Code MS8260MGPW Test Method : SW-846 503OB18260B Date Posted: 02102/04
Resuit Reporting Limit Fla g
Benzene 0 .71 pg[L 0 .50 Vg/L 0Toluene5.7 pg/L. 1 .0 Pg/L 0
Elhylbenzene 27 pg/L 1 .0 Pg/L 0
m~p-Xylene 17 pg/L 2 .0 grL 0o.Xylene 21 Pg/L 1 0 P91L a
vi,il lk lwnaNo ,Ihup:/Ide, ww/csscn0Iab-srv/
P%uke MlKeFowerAnaiytical LaDoratioryPower.Phone 7G4-875-5245 Fox 701-875-5038
13339 HagersFerly Road Huntefsville,NC28078-7929
McGuire Nuclear Complex - MG03A 2
Cortificato of Anaiysis .
New York State Department of Health Cerlificaltion # If717
Oklahoma DepadimnlofEnvironrwntafQuafilyCeripfcalion #9930
Kansas Department ofHeakh and Environment Certificate It E-fO3l f
North Carolina Department of Health &Human Services Certification # 378N
South Carolina (DHEQ Laboratory ID # 99005 North Carolina (OENF~Certification If 248
SamplelDO :24000597 Job#:04-JAN-013 0
Sample Description :PMWF-D (SAPROLITE WELLS )
Collection Date : 20-Jan-04 10 :50 :00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
WMr ~,~
IMGP PARAMETERS IN WATER BY GCIMS - 8260
Test Code : MS8260MGPW Test Method : SW-846 5030BIS260B Date Posted: 02102/04
-Result ..Reporting Limit Flag
Naphthalene 1100 VgtL 200 Plitt. I
SamplelD#:24000598 Job#:04-JAN-0130
Sample Description :PMWG-D (SAPROLITE WELLS )
Collection Date : 19-Jan-04 16 :15:00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
7
MGP PARAMETERS IN WATER BY GC/MS - 8260
Test Code : MS8260MGPW Test Method : SW-846 5030B18260B Date Posted : 02/02104
-Resuft Reporting Limit Flag
Benzene < 0 .50 pg/L 0 .50 Plitt.0
Toluene < 1 .0 Pg1L 1 .0 P911.0
Ethylbenzene < 1 .0 PgtL 1 .0 P91L 0
m-p-Xylene <2 .0 pg/L 2 .0 pq/L 0
o .Xylene 1 .4 pgtL 1 .0 pg/L 0
Naphthalene 2 .9 pgfL 2.0 pg[L I
SamplelD#: 24000599 Job#:04-JAN-013 0
Sample Description :PMW1 (SAPROLITE WELLS )
Collection Date : 19-Jan-04 16 :45 :00 Site :BURLINGTON Sample Type: MGP SITE Desktop #
0GP PARAMETERS IN WATER BY GC/MS - 826 0
Test Code : MS8260MGPW Test Method : SW-846 503OB18260B Date Posted : 02/02104
Result Reporting Limit Fla g
Benzene < 0-50 pg/L 0.50 P91L 0
Toluene 1 0 Pg/L 1 .0 pg/L 0
Ethylbenzene < 1 .0 pgfL 1 .0 Vg/L 0
m-p .Xylene <2 .0 Pgr-2 .0 vg/L 0
o .Xylene < 1 .0 Pg/l . 1 .0 pg/L 0
Naphthalene <2.0 Pg/L 2 .0 pg/L I
1 ;. ...",,/X12 .1 i 1 13 IJ litip :ttdc ..w/es .%cn~/lab-srv/.:"/j
P.Duke VUKeFowerAnaiytical LaDorator yPower.Phone:7N-675-5245 Fax [phone]
A D4, &~ C~ 13339 HagersFeriy Road Hunteisville,NC28078-7929
McGuire Nuclear Complex - MG03A 2
Ctartificatiie of Anaiy :sis;
New York State Department of Health Certification # f f7f7
Oklahoma Department of Environmental Quably Ced&ahon # 9930
Kansas Department of Heath and Environment Certificate N E. 1031 1
North Carolina Department of Health &Human Services Certification # 378N
South Carolina (DFC-Q Laboratory ID # 99W5 North Carolina (DBVR Certification #248
SamplelD#: 24000600 Job#:04-JAN-0130
Sample Description :PMWL-D (SAPROLITE WELLS )
Collection Date : 21 -Jan-04 09 :50 :00 Site :BURLINGTON Sample Type: MGP SITE Desktop #
~RkMWTIERSIN -WATER BY,GC/MS .8260
Test Code : MS8260MGPW Test Method : SW-846 503OB/8260B Date Posted : 02102/04
Result Reporting Limit Flag
Benzene < 0.50 pg/L 0.50 Pg/L 0
Toluene 1 .0 pg/L 1 .0 pg/L 0
Ethylbenzene < 1 .0 VgrL 1 .0 pg/L 0
m.p .Xylene <2 .0 pgrL 2 .0 pgr. 0
o.Xylene 1 .0 pg/L 1 .0 pg1L 0
Naphthalene 2 .0 pg/L 2 .0 VVI.I
------------------------------------
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pk Duke 8260 Analysis
OvEnergy,Case Narrativ e
(This document must awompany release of Analytical Data)
- -- - -------- - -------------
LIMS Job #04-A&AIWO11-3 9
Worklist #04-FEB-0052
•The percent drift and/or recovery for the continuing calibration standard for naphthalene
exceeded the laboratory quality control limits . The results for this compound should be
considered estimates .
•The percent recovery for the laboratory control sample for naphthalene exceeded the
laboratory quality control limits . The results for this compound should be considered
estimates .
----------------------------------------
Analyst Si lure
itTher)onmes
----------------------------------------------------------------------------
Duke Energy Analytical Laboratory Service s
Enwonment. Health &Safety Servioes Environrmntal Center - MG03A2
Phone :[phone] Hagers Ferry Road
FAX :[phone] Huntersville NC 28078-7929
E :\Casc Naffativ"\Organic\VOA~04-Jan-0139.dm
phDuke Duke Power Analytical LaboratoryOftwer.Phone .[phone] Fax,704-875-5038
13339 Hagersiceny Road Huntelsville,NC26078-7929
McGuire Nuclear ComPA9x - MG03A 2
t-- rt i 11 4a ~a t t--- cp r A%n a I Y!s i :s
New York State Department of Health Certification #1 17 f 7Oklahoma Department of Erwironmental Quably,CL III dicalion # 9930Kansas Department of Heath and Environment Ce illfical a # E- 103 f I
North Carolina Department oflballh &Human Sentices Cerlibcation #37804South Carolina (OHEQ Laboratory ID # 99005 North Carohna QENF~Corlihoallon #248
Station Name :BURLINGTON JobNumber:04-JAN-0139
Sample 10 #:240006SI Desktop #Customer ID R . ROBERTS
Sample Description : DMW-1 (SHALLOW WELLS)
Collection Date: 2Wan-04 14 :15 :00 Date Received in Laboratory : 08-Jan-04 TypeofSample :MGPSITE
ReferenceMethDd EPA310A/SM23208 Data Posted 213r2004 11 58 5 8
ALKALINITY (TOTAL INFLECTIONPOINT)-ALKALINITY 0 .82 meqlL
ReferenwMethod EPA200.716010B Data Posted : V30/2004 11 034 5
]RON BY ICP (DIGESTED)_IRON 3 .118 mg/I
Reference Method :EPA 200 .716010B Data Posted: 113012004 11 034 5
MANGANESE BY ICP (DIGESTED)MANGANESE 0 .191 mg/L
Referertce Method EPA 300 .0 Data Posted : 112812004 1325 .1 8
NITRATE (IC)NITRATE 0 .12 mg/L
Reference Method .EPA 300 .0 Data Posted 1/2812004 1654 1 8
NITRATE BY CALCULATION (MG-NIL)NITRATE 0.03 mg-NIL
Reference Method EPA 300.0 Data Posted : 1/2812004 1325 1 8
SULFATE (IC)SULFATE 9 .12 mg/L
Sample ID 24000653 Desktop #Customer ID R . ROBERTS
Sample Description : DMW-2 (SHALLOW WELLS )
Collection Date : 21-Jan-04 15 :30 :00 Date Received in Laboratory : 08,Jan-04 TypeofSample :MGPSITE
ReferenoeMethod :EPA310 .11SM2320B Data Posted : 213/2004 1 1 :58 :5 8
ALKALINITY (TOTAL INFLECTION POINT)ALKALINITY 4 .16 meq/L
ReferenceMethod :EPA200.7/6010B Data Posted : 1130/2004 11 :03 46
IRON BY ICP (DIGESTED)IRON 6 .103 rng/I
ReferenwMethod EPA200 .7/6010B Data Posted : 1130t2004 11 034 6
MANGANESE BY 1CP (DIGESTED)MANGANESE 6 .464 mg/L
Reterenm Method .EPA 300,0 Data Posted: 1/28/2004 13:25 3 9
NITRATE (IC)NITRATE < 0 .10 mg/L
Reference Method .EPA 300o Data Posted : 112a/2004 16 .54 1 9
NITRATE BY CALCULATION (MG-NIL)NITRATE <0 .02 mg-NIL
Reference Method EPA 300,0 Data Posted . V28120G4 13 :25 3 9
SULFATE (IC)SULFATE 0.20 mg/L
V'w ..'
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puke Duke Flower Analytical Laborator y
Power.Phone [phone] Fax :[phone]
A C~ 13339 Hagefs Ferry Road HuntersvilAe,NC 28078-7929
McGuire Nuclear Complex - MG03A 2
C 4~ rt ! r 1 4-- za t 4e 4o 1 *4% n a I y --s I
New York State Deparlment of Health Certification 9 11717
Oklahoma Department of Environmental Quahly Certification N 9930
Kansas Department of Heath and Environment Certificate N E-1031 1
North Carolina Department of Health &Human Services Certification 9 378N
South Carolina (OHEQ Laboratory ID # 99005 Noah Carolina (OENR Certification If 248
Station Name :BURLINGTON Job Number :04-JAN-0139
i
Sample ID #i 24000654 Desktop #Customer ID R . ROBERTS
Sample Description : PMWC-BR (SHALLOW WELLS )
Collection Date : 20-Jan-04 16 :40 :00 Date Received in Laboratory : 08-Jan-04 TypeofSample :MGPSITE
Reference Method :EPA310 .11SM2320B Data Posted 2/3/2004 11 58 58 C-
ALKALINITY (TOTAL INFLECTION POINT)ALKALINITY 4-15 mecI/L y 5 0
Reference Method :EPA 200 .7/60108 Data Posted . 1/3012004 11 03 46 V"
IRON BY ICP (DIGESTED)IRON 13.290 mg/I
Reference Method :EPA 200.7/601013 Data Posted . 113012004 11 :014 7
MANGANESE BY ICP (DIGESTED)MANGANESE 3 .544 mg/L
Reference Method EPA 3DO .0 Data Posted, 1128t2004 11 :08 :4 3
NITRATE (IC)NITRATE 0 .12 mg/L
Reference Method EPA 300~O Data Posted V28/20G41648 :3 1
NITRATE BY CALCULATION (MG-N/L)NITRATE 0.03 mg-N/L
Reference Method :EPA 300o Data Posted 1/28120114 11 :08 :4 3
SULFATE (IC)SULFATE 1 .13 mg/L
Sample ID #: 24000655 Desktop #Customer ID :R . ROBERTS
Sample Description : PMWH-BR (SHALLOW WELLS )
Collection Date : 20-Jan-04 10 :15:00 Date Received in Laboratory: 08-Jan-04 TypeofSample :MGPSITE
ReferenceMethod EPA310 .11SM2320B Data Posted: 2/3f2004 11 :58 :5 8
ALKALINITY (TOTAL INFLECTION POINT)ALKALINITY 4 .05 meqIL
ReferenceMethod EPA200 .71601013 Data Posted 113012004 11 :03 :4 7
IRON BY ICP (DIGESTED)IRON 4.577 mg/I
Refererice Method EPA 200 .7/6010B Data Posted : 113012004 11 :03 :4 7
MANGANESE BY ICP (DIGESTED)MANGANESE 4 .141 mg/L
Reference Method EPA 300 0 Data Posted 1/2812004 1 1 .09 :06
NITRATE (IC)NITRATE 0 .10 mg/L
Reference Method EPA 300o Data Posted It28/20G4 16 :4&3 2
NITRATE BY CALCULATION (MG-NIL)NITRATE 0 .02 mg-NIL
Reference Method EPA 300 .0 Data Posted 112812004 11 :09:D6
SULFATE (IC)SULFA TE 0 .48 mg/L
V .,tl lh~ Int,.No .1G.. .......I 2AW2004 /I It, ~J I1uP :Hdwww1csscnv1Ia1b-sr0 I
Duke -L)uxe Fower Anaiyucal LaDorator yPower.Phone .[phone] Fax [phone]
AD~~,G~13339 HagersFerly Road Huntelsvitle,NC28076-7929
McGuire Nuclear Comok-x - MG03A 2
4=4--rtlfl4r-~atie 4or Aknaiy!si-ss
Now York Slate Department of Health Certification N f 1717
Okleho~DBparlrmnlofEwironrnenialOuahtyCLrtdcation #9930Kansas Department of Heath and Environment Certificate NE4031 fNorth Carolina Department of Health &Human Services Certification # 37804
South CaroAna (DHEQ Laboratory ID # 99005 North Carolina (DENR Certification 111 24 6
Station Name :BURLINGTON Job Number:04~JAN-01139
Sample ID #: 24000656 Desktop #Customer ID R . ROBERTS
Sample Description : PMWI-BR (SHALLOW WELLS )
Collection Date : 19-Jan-04 14 :40 :00 Date Received in Laboratory: 08-Jan-04 Type of Sample MGP SITE
ReferenceMethod EPA310 .11SM2320B Data Posted: 2/3/2004 11 :58 :58
ALKALINITY (TOTAL INFLECTION POINT)ALKALINITY 5.91 meq/L
ReferenceMethod EPA200.7/6010B Data Posted : 1/30/2004 11 :03:4 8
IRON BY ICP (DIGESTED)IRON 1 .970 mgII
ReferenceMethod :EPA200.7/6010B Data Posted . 1130/2004 11 :03 :4 8
MANGANESE BY ICP (DIGESTED)MANGANESE 2.577 mg/L
Reference Method EPA 300,0 Data Posted 1/2912004 10 40 25
NITRATE (IC)NITRATE < 0 .10 mg/L
RefetenceMethod EPA300 .0 Data Posted 2/6/2004 10 48 05
NITRATE BY CALCULATION (MG-NIL)NJ TRA TE <0.02 mg-N/L
Reference Method EPA 300 0 Data Posted 1129/2004 10 :40:25
SULFATE (IC)SULFATE 35 .26 mg/L
Sample ID #: 24000657 Desktop #Customer ID R . ROBERTS
Sample Description : F`MWM-BR (SHALLOW WELLS)
Collection Date : 19~,Ian-04 12 :47 :00 Date Received in Laboratory : 084an-04 Type of Sample MGP SITE
RelerenceMethod EPA310.1/SM2320B Data Posted : 213/2004 11 58 58
ALKALINITY (TOTAL INFLECTION POINT)ALKALINITY 1 .07 meq/L
ReferenceMethod.EPA200,7160108 Data Posted 1130/2004 11 :03 4 8
IRON BY ICP (DIGESTED)IRON 0 .623 mg/I
Referenceivethod EPA200 .7160108 Data Posted : 113012004 11 :03 49
MANGANESE BY [CP (DIGESTED)MANGANESE 1 .064 mg/L
ReterenceMethod EPA300 .0 Data Posted : 112912004 10 .41 38
NITRATE (IC~NITRATE 1 .78 mg/L
Reference Method EPA 300 .0 Data Posted . 216/2004 10 48 08
NITRATE BY CALCULATION (MG-NIL)NITRATE 0 .40 mg-N/L
Reference Method .EPA 3000 Data Posted 1/2912004 10 :41 38
SULFATE (IC)SULFATE 24 .72 mg/L
V,,i,,,,,~n N eReImPH Genenaed ~16/2004 11 16 24 hup I/d w .,,/es c iv/lab-srv/i
P iDuke Duke Power Analytical Laborator yNower.Phone [phone] Fax 704-675~5038
13339 Hagers Ferry Road Huntelsville,NC26078-7929
McGurraNucleatCompilex-MG03A 2
ct--ruI14--ate- cpr Amnaiy-si s
Now York State Department of Heallh Certification # f 1717
Oklahoma Department of Environmental Quality Certification # 9930
Kansas Department of Health and Environment Certificate # E- 1`031 f
North Carolina Department of Flaafilt &Human Services Certification # 378N
South Carolina (DHEC)Laboratory ID # 99005 North Carolina (DENF~Certification #246
Station Name :BURLINGTON Job Number :04-JAN-0139
Sample ID # 24000658 Desktop #Customer ID :R . ROBERTS
Sample Description : PlMWL-BR (SHALLOW WELLS )
Collection Date 20-Jan-04 14 :20 :00 Date Received in Laboratory : 08-Jan-04 TypeofSample :MGPSITE
ReterenwMethod :EPA310.11SM2320B Data Posted : 213/2004 11 :58 :58
ALKALINITY (TOTAL INFLECTION POINT)ALKALINITY 2 .03 meq/L
ReferenceMethod EPA200.7/6010B Data Posted : 113012004 11 :03 :49
IRON BY ICP (DIGESTED)IRON 0 .186 mgII
Reference Method :EPA200.716010B Data Posted 1/30/2004 11034 9
MANGANESE BY ICP (DIGESTED)MANGANESE 0 .230 mg/L
Referenoe Method :EPA 300.0 Data Posted :1128/20G4 11 :10:05
NITRATE (IC)NITRATE < 0 .10 mg/L
Reference Method EPA 300b Data Posted. 1/28/2004 1648 33
NITRATE BY CALCULATION (MG-NIL)NITRATE <0 .02 mg-N/L
Reference Method :EPA 300p Data Posted 1/2812004 11 10 .0 5
SULFATE IC)SULFATE 20 .78 mg/L
Data a aw Apiio~ By.ciale
finft .,Wt MG. ......,,/2102004 /116 24 hup I/dc~ww/csscnv/Iah-sW 1%,
PhDuke Duke Fower Analytical LaDoratoryOrPower.Phone 7C4 .875-5245 Fax 704-875~5038
A 0~F-1 1333.9 Hag ers Ferry Road Huntersville,NC28078-7929
McGuire Nuclear CompA9x - MG03A 2
c4--ruticato c14 Amnalysi s
New York Slate Department of Health Certification # 117f7
OWhoma Department of Environmental Quality Certification # 9930
Kansas Department of Heath and Environment Cenificale # E- 1031 1
North Carolina Deparlinerif of I-Laith &Hurnan Services Certification # 378N
South Carolina (DHE~Laboratory ID # 99005 North Carolina QBVI~ Certification #248
"jar !T-
SamplelD#: 24000651 Job#: 04-JAN-013 9
Sample Description :DMW-1 (SHALLOW WELLS )
Collection Date : 21-Jan-0414 :15 :00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
MGP PARAMETERS IN WATER BY GCIMS - 826 0
Test Code : MS8260MGPW Test Method : SW-846 5030B18260B Date Posted : 02103104
Result Reporting Limit Flag
Benzene 0.50 pg/L 0 .50 Vg/L 0
Toluene < 1 .0 pg/L 11-0 Vg/L 0
Ethylbenzene < 1 .0 pgfL 1 .0 Vq/L.0
m .p.Xylene <2.0 pgri.2.0 pg/L 0
o.Xylene < 1 .0 pg/L 1 .0 Vg/L 0
Naphthalene <2.0 pg/L 2.0 pg/L I
SampletD#:24000653 Job#: 04-JAN-013 9
Sample Description :DMW-2 (SHALLOW WELLS )
ollection Date : 21-Jan-04 16 :30:00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
MGP PARAMETERS IN WATER BY GC/MS - 826 0
Test Code : MS8260MGPW Test Method : SW-846 5030B18260B Date Posted : 02/03/04
Result Reporting Limit Flag
Benzene 79 pg/L 5 .0 Pgr_0
Toluene < 10 pg/L 10 PgrL 0
Ethylbenzene 93 pg/L 10 pg/L 0
m.p .Xylene 34 pgfL 20 lig/L.0
o-Xylene 35 pg/L io Pgr- 0
Naphthalene 1100 pg/L 20 pg/L I
F -,my, 9 M -,, 77-7 77 77 -7TV97 "MW I r
SamplelD#: 24000654 Job#: 04-JAN-013 9
Sample Description :PMWC-BR (SHALLOW WELLS )
Collection Date : 20~Jan-04 16 :40 :00 Site :BURLINGTON Sample Type: MGP SITE Desktop #
...............
MGP PARAMETERS IN WATER BY GCIMS - 826 0
Test Code : MS8260MGPW Test Method : SW-846 5030B/82608 Date Posted : 02/03104
Resuft Reporting Limit Flag
Benzene 8 .2 pglL 5.0 pgL 0
Toluene < 10 pg1L to P91L 0
Ethylbenzene,16 pgfl- 10 pgiL 0
m.p .Xylene 20 pg/L 20 pg/L 0
o .Xylene 12 pg/L 10 V911 .0
Vimil ',,on lh~lau.No .1
lit(p :Bdcw.w/esscnv/lah-srv/
*Duke Duke Power Analytical Laborator yPower.Phone [phone] Fax.?N~875-5036
A D~E-, C~13339 Hagers Ferry Road Huntersville,NC 28078-7929
McGuire Nuclear Complex - MG03A2
ct--rtim--ate a1`Ana1y!si!s
New York Slate Depatirwrill of Health Cerlification # I f7f7
OklahomDepgdrmntofEnvironrTentelOualilyCerldcalion#9930
Kansas Deparlment ofHeallh and Environment Certificate # E-103f f
North Carolina Department of Health &Human Services Certification #37804
South Carolina (DHCQ Laboratory ID # 9"5 North Carolina (DENR Certification #248
Sample ID #:24000654 Job#: 04-JAN-013 9
Sample Description :PMWC-BR (SHALLOW WELLS )
Collection Date: 20-Jan-04 16 :40 :00 Site :BURLINGTON Sample Type: MGP SITE Desktop #
MGP PARAMETERS IN WATER BY GCIMS - 826 0
Test Code MS8260MGPW Test Method : SW-846 5030B18260B Date Posted : 02/03/04
Result Report~ng LiTit Flag
Naphthalene 220 Vg/L 20 pqAL I
Sample 10 #: 24000655 Job#:04-JAN-013 9
Sample Description :PMWH-BR (SHALLOW WELLS )
Collection Date 20-Jan-04 10 :15:00 Site :BURLINGTON Sample Type: MGP SITE Desktop #
MGP PARAMETERS IN WATER BY GCIMS - 826 0
Test Code : MS8260MGPW Test Method : SW-846 5030BIS260B Date Posted : 02103/04
Result Reporting Limit Flag
Benzene < 5 .0 pg/L 5.0 pg/L 0
Toluene < 10 pg/L 10 pg/L 0
Ethylbenzene 19 P91L 10 PgrL 0
m-p-Xylene 14 pg/L 20 pg/L 0
o-Xylene 14 VgA, 10 P91L 0
Naphthalene 730 pq/L 20 pgtL I
IFIN-1111111 IS AIM :In
Sample ID #: 24000656 Job#:04-JAN-013 9
Sample Description :PMWI-BR (SHALLOW WELLS )
Collection Date : 19~Jan-0414 :40:00 Site :BURLINGTON Sample Type: MGP SITE Desktop #
MGP PARAMETERS IN WATER BY GCIMS - 826 0
Test Code : MS8260MGPW Test Method : SW-846 5030B/82608 Date Posted : 02103/04
Result Reporting Limit Flag
Benzene 120 pg/L 5 .0 pgtL 0
Toluene 10 P91L 10 VgAL 0
Ethylbenzene 110 pg/L 10 pg/L 0
m-p-Xylene 26 pq/L 20 VgIL 0
o-Xylene S5 pg/L 10 Vg/L 0
Naphthalene 510 pq/L 20 pg/L I
Is
lw,.Noat.... . ....[)tip ://deww.w/essetiv/];ib-srv/
uuKe DUKerrower Anaiyucal LaDoreatoryNower.Phone,704-675-5245 Fax [phone]
A 13339HagersFerly Road Hunteisvil,19,111C28078-7929
McGuilre Nuclear Complex - MG03A 2
Ctartificatle clof Analysi n
Now York Slate Department ofHeallh Certification # lf717
Oklahoma Department of Environmentol Quahty Certification # 9930
Kansas Department of Health and Environment Ceilificate # E- t031 1
North Carolina Department of i-talth &Human Services Certification N 378N
South Carolina (Of E-Q Laboratory ID # 99005 North Carolina (DEN9 Certification #248
mmlelz q 1--l--I.,:2-m :~~-'
SamplelD#:24000657 Job#:04-JAN-013 9
Sample Description :PMWM-BR (SHALLOW WELLS )
Collection Date : 19-Jan-0412 :47 :00 Site :BURLINGTON Sample Type: MGP SITE Desktop #
"",Llsa~'al
IMGP PARAMETERS IN WATER BY GC/IMS - 826 0
Test Code: MS8260MGPW Test Method : SW-846 50308/8260B Date Posted : 02103104
-.--Result Reporting Limit Flag
Benzene ~ 0 .50 PgrL 0 .50 PgA- 0
Toluene < 1 .0 Pq/L to pg/L 0
Ethyibenzene 1 .7 WA 1 0 9g/L. 0
m-p-xylene 5.1 0911. 2 .0 Pg1l . 0
o .Xylene 2.7 pg/L 1 .0 WgIL 0
Naphthalene 130 pA 20 pg/L I
SamplelD#:24000658 Job#:04-JAN-013 9
Sample Description :PMWL-BR (SHALLOW WELLS )
,mOllection Date 20-Jan-04 14 :20 :00 Site :BURLINGTON Sample Type : MGP SITE Desktop #
MGP PARAMETERS IN WATER BY GC/MIS - 826 0
Test Code : MS8260MGPW Test Method : SW-846 5030B/826013 Date Posted : 02/031D4
Result .-Reporting Limit Flag
Benzene < 0 .60 PglL 0 .50 pglL 0
Toluene < 1 .0 Pgn-1 .0 pg/L 0
Ethylberauene < 1 .0 PgrL 1 .0 pg/L 0
m .p .Xylene <2.0 pgtt-2.0 Pelt-0
o-Xylene < 1 .0 Pgfl-1 .0 P911-0
Naphthalene <2.0 pgtL 2.0 Pg/L 1
7 -----------------------------------Dt-ascrilption cd Flacfs :
0 All Ar,el"ce,l Procedure Requ-nnent, Were Met
See C...N.".e
E .,,-.,rd C ....ner .1,...taht C- At---
3 R .'.rt U-1 ahr ...'
.,rt L,-., F.e-r . due 1.re,..r .d -ai ... ma
S-,Ie Re,..,.Sh-ld IST ., Be U ..d F- R ...1.1 .1 P .,-,see C . ..
6 Ah4,,. bete-.p.... I ... I a, ah
Rer,.rt .d .17 -.,.tha t(n,pore,, A,ccee,s the A-101 or hIgh-tcanceffl-4- n the *-Ple )- - - - - - - - - - - - - - - - - - - - - -
qo"a
Repmed By. Date
V"ilus ..t fle, IntraNel at6"te .... . .1 210.1.1 // 16 11 IlIIp ://dcwww/csscn0ab-srv/".13
Burlington MGP
April 2004 Groundwate r
Field Analytical Data
Field Calibration Fonns
Groundwater Monitoring Data Sheet s
Chain Of Custody Records
Laboratory Analytical Data
Burlington MNA Pioposid /Appendix B
BURLINGTON OPERATIONS CENTER -MGP SITE
GROUNDWATER MONITORING FIELD DATA
SAPROLITE WELLS
AVG
WELL DEPTH TO PROD PUMP WELL EVAC WELL EVAC SPECIFI CWELL DEPTH WATER LEVEL RATE -VOL VOL VOL VOL EVAC TEMP PH CONDUCTANCI DO OPP TURBDATE NO .11m) (feet)HIM)ODOR (nd/nalo)Iftem) (lite.)(921) (gal)OeVno) (deg Q (units)(UmInsfem) Inn) (mv) NTIJ)4128/2fKM PMWB-D 18 .18 8 .07 NONE NONE IW 6 .24 8 .52 1 .65 2 .25 NO 6 .3,6.3 .6 .3 377 .376 .376 0 .26.0.22, 0 .20 ~7-67 .47 21 .8 .3.7 .4412612004 PMWC-D 25 .20 15 .27 NONE NONE 84 6 .13 7.57 1 .62 2 .00 NO 21 .2,21 .1,21 .3 6 .5,6.5,6 .3 533 .536,537 0 .47 .0 .33,0 .28 44,46.47 73,55 .574/21112004 PMWF-D 16 .32 9 .% NONE MINOR 75 4,49 4 .73 1 .19 1 .25 YES 15.8.16 .0.15 .9 6 .9.6 .9 .6 .9 734 .737 .741 2 .5 .2.7.2 .9 -50.49-52 %,45 .22412712004 PMWG-D 19.07 9 .88 NONE NONE 34(1 5 .67 19 .93 1 .50 sm NO I&S. 16.6.16.6 6 .4. 6 .4 . 6 .4 516.529 .530 0 .77 .0 .77,0.94 21,17,15 4.2 .4 .0 .3 .7412712004PMWI 16 .12 11 .29 NONE NONE 100 2 .98 3 .79 0.79 1 .00 YES 16.5.16.4.16A 6.8,6 .9 .6 .9 323,349,254 3.5.1 .8 .2 .4 -1 .42-67 36,30 .124/29/2004 PMWL-D 9.70 3 .4,4 NONE NONE 50 3 .86 4 .73 1 .02 1 .25 NO 15.8, 151, 15 .8 6.4. 6 .4, 6 .4 346.3". 342 1 14 .114 .114 2.2,2 .1,2 .0
OVERBURDEN WELLS
AVG
WELL DEPTH TO PROD PUMP WELL EVAC WELL EVAC SPECIFI CWELL DEPTH WATER LEVEL RATE -VOL VOL VOL VOL EVAC TEMP PH CONDUCTANCI DO ORP TURRDATENO. (Im)(feet) (leet) ODOR (ndluda)(liters) Hitera)(gal) (gal)Dwno)(deg Q (units)(unkholcird (crag/1) (MV) INTIJ)4/27/2004 MW-3 22.24 13 .75 NONE NONE 85 5 .24 6 .62 1 .38 1 .75 NO 19.4 . 19 .6,19 .5 5 .7 .5 .7.5.7 117,117.117 0.63 .0.39.0.39 138,137,138 6.6,5 .5 .5 .34127/2f04 MW-5 13.54 6.84 NONE NONE 35 4A4 4 .73 1 .09 1 .25 NO 19.0.17 .8,18 .3 7 .1,7 .1, 7.1 920.918.921 0.29 .0.21 . 0.22 -94-93-93 19,10,7 .74128/2f*4 MW-9 9 .30 6.47 NONE NONE 133 1 .97 5 .68 0 .49 1 .50 NO 15 .7 .15 .7,15 .7 6 .5 .6.5.6.5 647.659,659 0.47~ 0.39.0.41 133.136.137 6.1,6 .3 .7 .1412712~ PMWB-S 13.59 8 .% NONE NONE so 3 .41 4 .73 0 .% 1 .25 NO 19.9. 19 .8 . 19 .9 6 .6.6.6.6.6 696. 7W. 7% 0.28,0.25,0 .23 -78-81-85 40,34.34412W(a1l PMWC-S 2 1 .09 12.84 NONE NONE 133 5,~ 11 .36 1 .35 3 .W NO 19.5 . 19 .2 . 19 .2 6 .6 . 6.6. 6.6 508,513,512 0.28. 0 .25 .0 .29 -75-75-75 6.0,4 .8, 4 .2412912()(M PMWL-S 7 .60 3 .17 NONE NONE so 2 .73 4 .73 0 .72 1 .25 NO 17 .9, 17 .8 . 17 .7 6 .5,6.5.6.5 541,527,520 0.30.0 .23,0 .21 -58,56-56 3 .6, 3 .8 . 3 .74/2&2004 PMWM-S 12 .68 10.97 NONE NONE 55 1 .06 2 .84 0 .28 0 .75 NO 17 .6. 17 .6 . 17 .6 5 .3 .5.3 .5 .3 127 .127 .126 4 .1,4 .0,4.0 192,193.193 3 .4 .2 .8 .2 .84128/2004 NIS 11 .71 8 .04 NONE NONE 194 2 .27 8 .52 0 .60 2 .25 NO 18 .4 . 18 .4, 18 .4 6 .6 . 6.6. 6 .6 678,686,692 0,16.0 .15 .0 .15 .93-93-93 4 .4 .4.0.4,0
SHALLOW FRACTURED BEDROCK WELLS
AVG
WELL DEPTHTO PROD PUMP WELL EVAC WELL EVAC SPECIFI CWELL DEPTH WATER LEVEL RATE -VOL VOL VOL VOL EVAC TEMP PH CONDUCTANCI DO ORP TURRDATE
N2. (feel -(feet) ODOR (nd/.dn)(lite")Hitus)(gal) (gal)(yWno) (deg Q (units)(..Wcm)(mg/1)(MV) (NTIJ)4128/2004 D7~-I r9 0-2)L6540"NONE NONE 220 13.96 22 .71 3 .69 6 .00 NO 17 .9 .18.0,18.1 6.2 .6 .2 .6 .2 107,107 .106 0 .42 . 0.46. 0.45 70.71 .72 9.3,6 .3 .6.64/2812004 DMW-2 32.08 7.85 NONE NONE 3W 14.96 18.93 3 .95 5.m NO 18 .6. 18.6,18.5 6.4 . 6 .4 . 6 .4 450,451,452 0.29.0.18.0.17 ~ 1, ~62-62 6.9.5 .0 .5 .4412612004 PMWC-RR 36.00 13 .01 NONE NONE 675 14.0 25 .55 3 .75 6.73 NO 19 .6. 18.6.18.6 6.4 .6 .5 .6 .5 528,522,520 0.62 .0.59,0.57 .59, ~2-62 3.3,2 .8 .2.5412712004 PMWH-BR 20.72 8.68 NONE MINOR 377 7.43 17 .03 1 .%4~50 NO 15 .6,tS .7,15 .7 6.7 .6~7 .6.7 4t,6. 461 . 456 0.28, 0 .24,0.23 -74,45,77 2 .7 .3 .0 .2 .74/27/2004 PMWI-BR 38 .07 10 .35 NONE NONE 170 17.11 20.82 4 .52 5.50 NO 17.4. 17 .4 .17 .4 6 .8 . 6 .8, 6 .8 579.575.576 0.15,0 .20 .0 .20 -77-78,48 1 .4 .1.2.1 .24/28/2f(M PMWL-BR 24 .46 5 .35 NONE NONE 50 11 .80 14 .19 3 .12 3.75 NO 19~9,20.1, 20.1 6 .2 .6 .2,6 .2 236,234.234 0.17.0 .19,0 .21 116,118,119 2 .6,1.7.1 .5412612~ PMWM-BR 19 .16 11 .19 NONE NONE 75 4 .92 7.57 1 .30 2 .00 NO 17.8.17 .8,17 .8 5 .8,5,8,5 .8 142,146.142 1 .7,1 .7~ 1 .7 31 .35.37 0.8 . 0.9 . 0.9
COMMENTS:
Water levels and well depths arc referenced to top of PVC cuing .* -Avg ponsing rate used to minanize or stabilize drawdown while rearoving one well volonx,and stabilizing indicator Warnaers .
FIELD SAMPLING CALIBRATION DATA FORM
STUDY: rl
DATE :.WEATHER CONDITIONS : SNEe7-Y . CU~DY A .qZ4 1, 0
COLLECTORS :I'D C &~o SURFACE UNrr READER :~-A C-r
HYDROLAH SERIAL #:42'
-
~isq3 COMPUTER:
OTHER EOUIPMENT:SURVEYOR SERIAL 0:
Procedure Number 3210 .1
Calibration Time Time C330 Time o ~Joo Time
Barometric 0-c 1,; 4 6k 1 -,,, -) 10 -1
Pressure ~51 ~_3 mmHg q ~t 9 mmHg mmHg
Parameter Calib . Instrument Standard Instrument Standard Instrument Standard
I Value Value Value Value Value Value
Thermomete r
No .JA
TEM P
(deg C)
W
DO W
(mgA)W
AW 8 .)L t JILS >~6,;)->
pH B >7 .00 -7 .01 > 7.00 > 7 .00
(units) B a >4 .00 11 .0 >4 .00 >4 .00
B > 10 .00 > 10 .00 > 10 .00
SPCOND SS -J > 0.00 >0 .00 > 0 .00
(US/Cm) SS >-7XO > ? -7-0 >
SS > >>
ORP SS Li >-i n >c13 >(MV) SS > > >
V-kTURBIDITYSS--Lj pr, 000 > 0 .00 > 0 .00
(ntu)SS - ----> -- ---->>
KEY : B =Buffer W =Winkler NA Not Applicable
SS =Standard Solution AW =Average Winkle r
-- -- > =Adjusted To -- / -- > =Not Adjusted To
FIELD SAMPLING CALIBRATION DATA FORM
STUDY : C-
DATE:WEATHER CONDITIONS : 6D
COLLECTORS :C 0 t,--Vi SURFACE UNIT READER :U~b
HYDROLAB SERIAL COMPUTER:
OTHER EQUIPMENT :\W-kA SURVEYOR SERIAL 9:oob
Procedure Number 3210 .1
Calibration Time Time n-loo Time Time
Barometric T;-L---7/-o-i
Pressure J Ok .7.-mmHg :J,,S -7 -3 mmHg mmHg
Parameter Calib . Instrument Standard Instrument Standard Instrument Standard
I Value Value Value Value Value Value
Thermometer
No .
TEMP
(deg C)
W
DO W
(mg,l)W
AW
pH B -7, 0 ~A 7 .00 03 > 7 .00 > 7 .00
(units)a LA .O .A,4.00 O)L_>4 .00 >4 .0 0
B > 10-00 1 10 .00 >10 .00
SPCOND SS Jo->0 .00 > 0 .00 >0 .0 0
(US/CM) SS 3-- b C >-7 XO >
SS '72-5 > > >
ORP SS >OL >r7
(MV) SS > >>
TURBIDITY SS y1i 0.00 >0 .00 > 0.00
(ntu)SS > -->
KEY : B =Buffer W =Winkler NA Not Applicable
SS =Standard Solution AW =Average Winkle r
> =Adjusted To -- / -- > =Not Adjusted To
FIELD SAMPLING CALIBRATION DATA FORM
STUDY : ftA
DATE :WEATHER CONDMONS : 0 Q
COLLECTORS:0 SURFACE UNrr READER :
HYDROLAB SERIAL COMPUTER :
OTHER EQUIPMENT:SURVEYOR SERIAL #:
Procedure Number 3210 .1
Calibration Time Time ()L ~4 Time Time
Barometric Li t -3--6
Pressure -2 57, 3 mmHg --? -,-> ?.),mmHg mmHg
Parameter Calib . Instrument Standard Instrument Standard Instrument Standard
I Value Value Value Value Value Value
Thermomete r
No . 4/4
TEMP --/--> -- --/-->
(deg C) > > >
W
DO W
(mg/1) W
AW
pH B U3 > 7 .00 7.00 > 7.00
(units)B 0 :1,>4 .00 Lq 4 .00 >4 .00
B > 10 .00 > 10 .00 > 10 .00
oc-
SPCOND SS -40-0 FL > 0 .00 > 0.00
(US/Cm) SS 7 ~t->7ZO >>
SS > >
ORP SS ct > >
(MV) SS >
TURBIDITY SS 0 .00 >0.00
(ntu)SS >
KEY : B =Buffer W =Winkler NA Not Applicabl e
SS =Standard Solution AW =Average Winkle r
> =Adjusted To -- I -- > =Not Adjusted To
FIELD SAMPLING CALIBRATION DATA FORM
STUDY :3Urt"-ZrJ C--110 ;J
DATE:-t la-(-10-~WEATHER CONDMONS:(3 "r -,b -y AAj,-j 4
C
COLLECTORS:k-0 C fL %.-W SURFACE UNrT READER :
HYDROLAB SERIAL #:3 V1 C-3 COMPUTER :
OTHER EQUIPMENT :kiAc ki -VU,KA T 6 ZAA i,1!L SURVEYOR SERIAL C
Procedure Number 3210 .1
Calibration Time Time 0C%00 Time n L ~k 0 Time
Barometric It P- 6 /OT- OL-)ON(
Pressure -7,51 .3 mmHg mmHg mmHg
Parameter Calib . Instrument Standard Instrument Standard Instrument Standard
I Value Value Value Value Value Value
Thermomete r
No .V1 1A ri
TEM P
(deg C)
W
DO W
(mg/1)W
AW <67,>
pH B Q3 > 7 .00 > 7 .00 >7 .00
(units) B Aj .0 0 >4 .00 CN >4 .00 >4 .0 0
B >10 .00 > 10 .00 > 10 .00
SPCOND SS > 0 .00 > 0 .00 > 0 .00
(US/Cm) SS 7 O-A >'7-7, 0 '1 X?,->
SS ----> - >
ORP SS >(1 0 >"(3 >
(MV) SS > -- > - >
tj 149 -1J lf~~
TURBIDITY SS 0 .00 > 0 .00 > 0 .00
(ntu)SS -- >
KEY : B =Buffer W =Winkler NA =Not Applicable
SS =Standard Solution AW =Average Winkle r
> =Adjusted To -- / -- > =Not Adjusted To
FIELD SAMPLING CALIBRATION DATA FORM
STUDY :
WEATHER CONDMONS, B&
COLLECTORS : LD SURFACE UNIT READER:
HYDROLAB SERIAL C 3N,4 L-3 COMPUTER:
OTHER EQUIPMENT: k-kA i 0 Q f~D "_VV'k: Xr~SURVEYOR SERIAL #: 5 k!o 3
Procedure Number 3210 .1
Calibration Time Time 0 0 Time OL 10 Time
Barometric 13--) / Oct 4 1 ~,-x 10-t
Pressure ;t, mmHg -7~!~ -),3 mmHg mmHg
Parameter Calib . Instrument Standard Instrument Standard Instrument Standard
I Value Value Value Value Value Value
Thermometer
No .d e-:~
TEMP > >
(deg C)>
W
DO W
(mg/10 W
AW '6 k >!~,:2,> -
pH B >7 .00 cL > 7 .00 > 7 .00
(units) B (N R >4 .00 0 :)->4 .00 >4 .0 0
B >10 .00 >10 .00 >10 .00
SPCOND SS o-O >0 .00 0 .00 >0 .00
(US/CM) SS >-7-2-0 77 >-2,~-()>
SS > > >
ORP SS leci > 01 -1, >
(mV)SS > >
V-J/0.00TURBIDITYSS - >0 .00 > 0 .00
(ntu)SS ----> -->
KEY : B =Buffer W =Winkler NA Not Applicable
SS =Standard Solution AW =Average Winkle r
> =Adjusted To -- / -- > =Not Adjusted To
FIELD SAMPLING CALIBRATION DATA FORM
-STUDY :19 U N ~_Id (--.-\ (-P
DATE: -(I ), q I WEATHER CONDMONS:-t 0 13
COLLECTORS:Lp C SURFACE UNIT READER :
i
HYDROLAB SERIAL #:fs L40 COMPUTER:
OTHER EQUIPMENT :k-M C k 1~~g W SURVEYOR SERIAL #: 'S
Procedure Number 3210 .1
Calibration Time Time 06 ~50 Time I L30 Time
Barometric I I -J-19 ( 0 3 q I ;'-,e I C),--k
Pressure _75-),J mmHg -7,51 .a- mmHg mmHg
Parameter Calib . Instrument Standard Instrument Standard Instrument Standard
I Value Value Value Value Value Value
Thermomete r
No .J 1,A
TEMP > > >
(deg C) > >>
W 16 7L5
DO W
(mg/1)W
AW r6 >~6 -/>
pH B >7 .00 OrA 7 .00 >7.00
(units) B >4 .00 0 y>4 .00 >4 .00
B >10 .00 > 10 .00 > 10 .0 0
SPCOND SS --/>0400 0 .0 > 0 .00 >0.00
(USICM) SS > -7 0 -> 0
>
SS > > >
ORP SS >Ct I K-7 >
(MV) SS > -
TURBIDITY SS 0 .00 0 .00 > 0.00
(ntu)SS >
KEY : B =Buffer W =Winkler NA Not Applicable
SS =Standard Solution AW =Average Winkle r
> =Adjusted To -- / -- > =Not Adjusted To
uur%r- r%jvvr-n %~%Jlvlrmlld I
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
ILOCATION :~N . NG PROC NO :3500.1
JPROJFCT NAf I POLITE W FIELD CREW :LDC,RLW
ISAMPLING DATE :_2~~r 0 4
ONITORING WELL NO .PMWB-D
WATER LEVEL METER SIN :N/A
PID READING loo-i ftt~N~*-Q ppm PRODUCT LEVEL METER S/N :
METHOD (Pump /Bail)1PERISTALTIC PUMP TIME / INITIALS OF COLLECTED SAMPLE :
WELL VOLUME CALCULATION :
OR VolEP~~THTO WATER CoNvERsioNjWELL WELL DEPTH TO WAT CONVERSION WELL
DIAM DEPTH (ft)X FACT
L jai
WATER (ft) COLUMN ft FACTOR
V c
0.16312'18 .18 X
X
Ions X 3 .785 1 N/A liters
SCREENINTERVA L
FROM T DETECTED ODORS FREE PRODUCT MEASUREMENT
16 .68 ft . 18 TYPE: DEPTH TO WATER :i
STRONG :DEPTH TO PRODUCT~---(ft)
MINOR : PRODUCTTHI ft
INTAKE NONE, DON'T SAMPLE IF THICKNESS >OR =TO 0 .1 FT !
F
START AT END
~T_17.50 17 .50 Ift
INITIAL READINGS MEASURED AT GROUNDWATER /AIR INTERFACE INDICATED
BELOW OLVEDFLOWRATE TfMP SPEC TURBIDITY PH ORP DIS N
COND OXYGEM ss)TIME (deg C) (Us/cm) (mv)(M9A)(hh :m :ss (ntu) unit )
N/A N/A N/A N/A N/A N/A N/A N/A N/A
f___
-WATER FLOWHATF TFMP -"M%F--UP DISSOLVEDTTURBIDITYPIT
TIME LEVEL
(unit) (MV)
COND OXYGEN
(hh :mm :ss) 00 (ml/min)(deg C (us/cm)(ntu)(mg/1 )
1 2:;~t 010 STABILIZED DRAWDOWN A 0 REMOVED 1,7.57 Aj- EGANLOGGINGDATA
--(.Z n cl31L I 76-C x s
t~f OL
q 2, 3 5 2, C -7
"'-Ill Lo C 4 1 V-
ELECTRONIC FILENAME - N/A
OMMENTS :
Cl=
TOTAL VOLUME REMOVED .2-
NOTE :WATER LEVEL, PRODUCT LEVEL,AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
tiumr_ r-vvvr_n I
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
LOCATION :BURLINGTON,NC PROC NO :3500.1
_PROJECT NAME : BURLINGTON MGP ~SAPROLITE W
ISAMPLING DATE:26-API-04 I ZF-Apf-~
IMONITORING WELL NO .PMWC-D
WATER LEVEL METER S/N : N/A
PID READING ppml PRODUCT LEVEL METER S/N :
METHOD (Pump /Ball)1PERISTALTIC PUMP TIME / INITIALS OF COLLECTED SAMPLE :30c,
WELL VOLUME CALCULATION :
FDEPTH T OWELL WELL DEPTH TO WAT CONVERSION
IWATEROLUMN (IftWATER(ft )DIAM DEPTH (ft) X FACTOR
2'25 .20 X 0.1631I15-A7
XIL~~j
N/A gallo,s X 3 .785 N/A _~ljtlrs
SCREEN INTERVAL
I DETECTE ODORS I FREE PRODUCT MEASUREMEN Tft
TYPE : DEPTH TO WATER :I
ti
PUMP IN ~AKE NONE : I/ 1DON'TSAMPLE IFTHICRNESS >OR=TOO .l FT I
ATSTART I ATEND
25 .0 ft 25 .0 tt .1
INITIAL READINGS MEASURED AT GROUNDWATER AIR INTERFACE INDICATED BELOW
WATER PEC TURBIDITY PH OPP DISSOLVED
TIME LEVEL OND OXYGEN
(hh :mm :ss) 00 3=c)(Cl
S,/
(ntu) (unit)(mv)(MgA )
N/A N/A -1 N/A I N/A N/A___L N/A N/A N/A N/A
FLOWRATF TEMP _776T TURBIDITY PH UKF DISSOLVED
TIME LEVEL COND OXYGE N
(hh :mm :ss)(ft)(mVmin)(d q C)(US/cm)(nt (mv)(mgA)
k I 'Ao LM STABILIZED AWDOWN AND REMOVED EGAN LOGGING DATA
k ;L3L li~o z 1 .6-) 53'1 4 .2 .0 4 .-(g _1_0 0 .1.9
IX43 Ko 2 1 .;t,1 -5 3 :3 72 .(,-44 o-q
ix~0 gn )L%- k 3 53(-55 .4 t.-51 -44 0 .~
5'2 .f t..5 1
fv,Po_-r*)--4c-j 30o
ELECTRONIC FILENAME - N/A
; COMMEN S,_13~Z:7
Cl=
TOTAL VOL ERE OVED =
NOTE :WATER LEVEL, 'PRODUr.T LEW-L .ANDO WVVELLL DUEPT M-AR E ~REFERE~NCED TO THE TOP OF WELL CASING .TS
UUM: lUWtK L;UMPAN Y
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
ILOCATION :BURLINGTON, NG PROC NO:3500.1
PROJECT NAME : BURLINGTON MGP (SAPROLITE WELLS) FIELDCREWd LDC,RLW
SAMPLING DATE :-Z&ADL-04 I 27-Apr-04 I ~! ~o (-
MONITORING WELL NO .PMWF-D~~~
WATER LEVEL METER S/N :N/A
PID READING -7i ppm PRODUCT LEVEL METER StN :9 -I
METHOD (Pump /Ball)1PERISTALTIC PUMP TIME/INITIALS OF COLI-EqTED SAMPLE:
WELL VOLUME CALCULATION :
WELL WELL TO WATER CONVERSION WELL
DEP
R ftl I VOL
DIAM DEPTH (ft)WAT7E COLUMN (ft)X FACTDR
I jai
2-16 .32 1"10 X 0 .1631 , 1 1?
X -9
------
SCREE
N/A gallons X 3.785 1 1 N/A riters
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
14 .32 ft . 16 .32 ft .TYPE
.-
lcl ;~ DEPTH TO WATER:I
STRONG :DEPTH TO PRODUCT, (ft)
MINI PRODUCT THICKNESS :(ft)
PUMP INTAKEJ NONE : IDON'T SAMPLE IF THICKNESS >OR =TO 0 .1 FT 1
AT START I AT END
16 .32 ft. 16 .3 2
INITIAL READINGS MEASURED AT GROUNDWATER AIR INTERFACE INDICATED BELOW
WATER FLOWRATE TEMP SPEC TURUIDITY PH ORP DISSOL7ff
TIME LEVEL COND OXYGEN
(hh :mm:ss)(ft)(ml/min)(us/cm)(m unit (mv)(mgA )
N/A N/A N/A N/A N/A NIA N/A N/A N/A
WATER FLOWHATE TEMP -9M TURUIDITY PHI)ORP DISSOLVED
TIME LEVEL COND OXYGEN
(hh :mMss)(ft)(mVmin)(deg C) (US/cm)(ntu)(mv)(mgA)
174---7714 STABILIZED DRAWDOWN AND REMOVED BEGAN LOGGING DATA
(c 50 is .Lt :3 -),I, x 5 ~i cl - 6 L 6
()'6( So i 3,Ov 5o IiS-t-A 7 3 ~;-3,D--)~V-) -511 L42,
o ~X-3 13,Lo 55 k5-t,-~-7 3 -t 94 .4 L .,6 t -50 A-5 i
W15Xq N-0-31 L 0 t5 9 t;'7 3 ~)14~ct It ..,d -2 -49 a .,)I
0 D 35-1 4 .50 ~ClLi 7111 4 1
9-7 3c) 1 0 /oLf ~t
-,3 It LI k C - 6 L,
41 0~R I OL I
CA k -k V k-~o -(e Ct Li 71 -7 .,A!j
-L Vil Q~(50 -02-71OLf tj 0-1
r
ELECTRONIC FILENAME -N/A
NTS :c- o o FA-)t,-L,
c "Av so AA V_A J
TOTAL VOLUME REMOVED =
NOTE~WATER LEVEL, PRODUCT LEVEL,~AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
LJLPF%V-Vwvv~"%,%.flVlr^lv I
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
ILOCATION :I BURLINGTON, NC PROC NO : 1 3600
PROJECT NAME : IBURLINGTON -P TE WELLS)FIELDCREW :j LDC,
SAMPLING DATE:-2&-~r227=1 MAPP44~~L'o (-
MONITORING WELL NO .
PMWG-D WATER LEVEL METER SfN :N/A
PID READING PRODUCT LEVEL METER S/N :
METHOD (Pump /Ball)PERISTALTIC PUt TIME / INITIALS OF COLLECTED SAMPLE :k 0 1 <-
WELL VOLUME CALCULATION :
WELL WELL DEPTH TO F-WATER CONVERSION F WELL
DIAM DEPTH (ft)WATER (ft)COLUMN (ft)X FACTOR VOL (gal)
2-19 .07 X 0.163 1
X
N/A gallons X 3 .785 NIA ~lltors
SCREENINTERVA L
FROM tj TO DETECTED ODORS FREE PRODUCT MEASUREMENT
16 .57 19 .07 ft .TYPE : DEPTH TO WATER,
STRONG :DEPTH TO PRODUCT,tJ 0 C4 IZ (ft)
MINOR: PRODUCT THICKNESS :
Pump INTAKE NONE :-Eo-wr SAMPLE IF THICKNESS >OR =TO 0.1 FT!
AT START AT EN D
18 .0 ft . 18 .0 "-
INITIAL READINGS MEASURED AT GROUNDWATER /AIR INTERFACE INDICATED BELOW
WATER FLOWRATE TEMP SPEC I TURBIDITY PH OHP UI55OLV
TIME LEVEL COND (mu) (unit)
OXYGEN
(hh :mm*ss) (tt) (mVmin) (deg C) (us/cm) I (mv)(MgA)
NIA NIA N/A N/A N/A ..-A NIA N/A N/A WA
---WATER FLOWRATE TEMP -ITIM TURBIDITY P ORP DISSOLVED
TIME LEVEL COND I OXYGEN
(hh :m:ss)(tt)(mUmin)(deg C) (us/cm)(nt (unit)(rmf)(MgA)
ki .3 )~ 0 STABILIZED DRAWDOWN AND REMOVED A-0 j A - EGAN LOGGING DAT A
OCN 3 E)t I .3,;P, 0 -L~-5 )--; U k J ;L -c (~2, 7 -Z3 1 0,L).
o ci 4 ~7 (,I ~7 3 5"o 14,15 5os-6 - ~~,~i "?-?
0 ok,5 ( j 1 . ~L!5' -3 S0 j4 .L5 5t (. t- - 3 5-
3 ;~,360 1 14-54 5 11-Lt (3
3 (, -3~ 0 5 cl 51cl '-t ~ 0 -L 6 -3 2 1`7
t,-13 1 530 3~-)4 6-3S
ELECTRONIC FILENAME - N/A
COMMENTS*P A 4)7'125 C,Cl =
TOTAL
REMOVED=
P10 2A k
NOTE :WArER LEVEL . PRODUCT LEVEL .AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .VOEUME
DUKE POWER COMPAN Y
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
OJECT
J
OCA ONE IBURLINGTON, NC PROC NO :
PRE NAM~lj~;APROLITE WELLS)FIELD CREW :
ISAMPLING DATE:I 26-Apr. 27-~r-04 28-Aor-04 29-Anr-04
MONITORING WELL NO .PMWl
WATER LEVEL METER SIN :N/A
PID READING PUMP PRODUCT LEVEL METER SIN :Ql -k (~ - \
METHOD (Pump/Ball)]PERISTALTIC TIME / INITIALS OF COLLECTED SAMPLE :k -z, / Vv
WELL VOLUME CALCULATION
: CONVERSION VOL[4alWELL WELL FDEPTH TO WATER CONVERSI WELI.IE7~V
DIAM DEPTH (ft)WATER ift) COLUMN ft X FACTOR OL al
2-16 .12 2)X
I-t X
gallons X 3 .785
SCREENINTERVAL
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
1 16,19 ft.TYPE :DEPTH TO WATER ::~I~
STRONG
: gE.PTH 10 PRODUCT:---I (ft)
MIN~R--P~ DUCT THICKNES& = I (ft)
Pump INTAKE I DON'T SAMPLE IF THICKNESS >OR =TO 0 .1 FT!
ATSTA R
15 .5
T
ft
AT E
INITIAL READINGS MEASURED AT GROUNDWATER AIR INTERFACE INDICATED BELOW
W
AV Lk FLOWRATE TEMP--SPEC TURBIDITY PH ORP DISSOLVED
TIME LE EL COND OXYGENI
(hh :i-(dng C) (USICM)~ntu) (unit)(mv)(mgA)
N/A N/A N/A _WA N/A N/A NIA N/A N/A
-'N
TUF RP DISSOLVE D----WATER FLOWRATE
TEMP
IBIDITY ptl
fj~0114 OXYGENLEVEL.07TIME(ft)I -7mv)(hh :mm:ss) (ml/mm) Idea C)(un (mgA)
STABILIZED D AWDOWN AND REMOVED BEGAN LOGGING DATA
1-4 3C3 Z-, 1 C3 (OQ 3 i 0 t!5 0', ~~ 1 %-j Ltt 3 1
2.5 1(017-16 .915 -74 -1 k -LS
'40 2-Dt 1 (0,95 -51 -'3 t9
Z2 J2- kj~ kt~b It. kl~S ~k 1
I fA 0%3 ~3 .L%(oct 3 3,
Eli #-31q,sci (O-qz) [(..So .32 (-,%3 3,1
14To,-r-,T.-.3 3 41in '4
(to t+3 Z53-6
~A w
57-1 0 . %:q
ELECTRONIC FILENAME - N/A
Col NTS~
ci
=%E
M~l :A?X
TOTAL VOE-UME RE-MOVED ~jckx\~J,,
-~-OTEWATEA LEVEL, PRODUL ;I LMEL,AND WELL Ut:F'l ARE HtF t:Kt D TO THE TOP OF WELL CASING .
IJUKE P0WI=H GUMPAN Y
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
ILOCATION :1BURLINGTON,NO PROC NO :3500 .1
1PROJECT NAME :BURLINGTON MGP!~PIIIT~21EL FIELDCREW :l LDC,Rl-W
[SAMPLING DATE :26-Apr-04 1 27
A,
29-Apr-04
MONITORING WELL NO .PMWL-D
WATER LEVEL METER SfN:N/A
PID READING m PRODUCT LEVEL METER SIN :
METHOD (Pump/ Ball)IPERISTALTIC PUMP TIME / INITIALS OF COLLECTED SAMPLE :
WELL VOLUME CALCULATION:
Co NVERSIONCo UMN ftWELL WELL DEPTH TO WATER CONVERSION WELLATER[Eo-~DIAM DEPTH (ft)WATER
III )LUMN ft X
FACTOR VOL 'alEPT"ToATERIII F-~n-FACTOR
E3 0.16312-9 .70 3 i-k X-Z
X
NIA gallons X 3 .78S N/A lit~ers
SCREENINTERVA L
FROM TO DETECTE ODORS FREE PRODUCT MEASUREMENT
8.70 9 .70 ft.TYPE : IDEPTHTOWATER,i
STRONG :DEPTH TO PRODUCT :---(tt)
MINOR :IEBODUCT THICKNE S
Pump INTAKE NONE
: DON
'T SAMPLE IF THICKNESS >OR =TO 0 .1 FT!
ATSTART ATEN5 C-ck
9 .7 1 w, ~--0\t~x~-
INITIAL READINGS MEASURED AT GROUNDWATER AIR INTERFACE INDICATED BELO W
LE FLOWRATE TEMP SPEC TURBIDITY pH ORP DISSOLVEDWAVTER
rimE L OXYGEN
(hh ~.mm :ss)(ft) (mVmin) (nt (mv)(mgA)
N/A N/A NIA N/A WAA N/A N/A N/A N/A
(u it)~~WATER FLOWRATE TFMP)7M I TU141310ITY --Png--DISSOLVED
TIME LEVEL COND OXYGEN
(hh :mm :ss) (ft)(mVmin)(dog C (USICM)(ntu) Mv (MgA )
STABILIZED DRAWDOWN AND REMOVED - BEGAN LOGGING DATA
15,Lc)3ct I, q C3 I ( cl,7-,(as
Lk(cl (Sjl~'%7;~,U -1 %4,3 5 k k -I 2-k Z-ks
5,t (5,(S 3 91
1 :3 2 t-ca-,-L3 q -3 3
1 [;,34 t53 -1 1 ,
1 -Ik,ci :3,-13 (,,Sl lis i
o%-3 Sk-1 -I- JQ -1 7-, ct Ij (.,4-1 1
,%-t c)C) 5'~ I Q 3 (r,2-k r6 -L (b,q -1 (k
o%--k 5 ~3 2-~9 C,G7--k -T--
1 . Q 'Li J .kj rA-q~k SA11444 C~!*,u,\N
0%r~5~ cl 3 4(.e (
-Z~ sc,'3 Lt
(P z 3 ct cA 4k (4,Lt i
ELECTRONIC FILENAME - NIA
COMMENTS :
TOTAL VOLUME REMOVED -I
NOTE:WATER LEVEL .PRQDUU I-LETEtEZ&WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
LIUKh PUWEH COMPAN Y
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
ILOCATION : I BURLINGTON, NC PROC NO:3500.1
I PROJECT NAME : ISURLINGTON MGP (OVERBURDEN WELLS)FIELDCREWd LDC,RLW
ISAMPLING DATE: I 26-Apr-04 27-Apr-04
MONITORING WELL NO .MW-3 71
WATER LEVEL METER SIN : N/A
PID READING ppm PRODUCT LEVEL METER SIN :
METHOD (Pump /Ball)JPERISTALTIC PUMP TIME / INITIALS OF COLLECTED SAMPLE :
WELL VOLUME CALCULATION :
WATZ TWELL WELL DEPTH T F WATER CONVERSI10]N WELL.
1DIAM DEPTH (ft)
ER ft~
COLUM X FACTOR VOL
Jai
01
r
S'
2-22.24 x 0.1631 1%3 B
x
WA gallons X 3 .785 N/A
SCREEN INTERVA L
FROM To DETECTED ODORS FREE PRODUCT MEASUREMENT
12 .0 22.0 ft .TYPE : DEPTH TO WATER::~-_STRONG :DEPTH TO PRODUCT :---(ft)
MINOR: PRODUCT THICKNESS : = (ft)
PUMP INTAKE NONE :DONT SAMPLE IF THICKNESS >OR =TO 0 .1 FT !
AT START I AT END
17 17.0 ft .
INITIAL READINGS MEASURED AT GROUNDWATER AIR INTERFACE INDICATED BELOW
w A
-ti rLUWRATE TEMP SPEC TURBIDITY pH ORP DISSOLVED
TIME LEVEL COND OXYGENIr
(hh :mm,ss)(ft)(ml/min) (deg C) (us/=)(nt (mv)(mqA)
N/A N/A N/A N/A N/A WA N/A NIA N/A
TURB TY PH URP DISSOLVED--WATER FLOWRATL TEM P
TIME LEVEL COND OXYGEN
(hh :mm :ss)(ft)(ml/mln)(deg C) -(-Ugsp/Mcm)(ntlu[)) (unit)(mv) (m
13 %ck 5 STABILIZED DRAWDOWN AND REMOVED 1-5 BEGAN LOGGING DATA
ct (,A k sk (.Cl
S 3 5 13 't,5 I&S 1, ct k 1k L tok 13'a
ks C-Irlu kl'Cks 176's Ict, CQ I ~ -1\ 3 5"A -1 slr.;~I -~ -I I'l
ks Lt 5 3 1% S4 ~~-Ak 1 5 3-2-S'(il i 3'9 3'1 1
ELECTRONIC FILENAME - N/A
CC 10=% NTS
:
TOTAL VOLUME REMOVED
NOTE :WATER LEVEL,PRODU(; I L PEL,EAN~ WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
UUKL PUWt:K t;UMI'AN Y
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
LOCATION : BURLINGTON, NC PROC NO ;
1PROJECT NAME :BURLINGTON MGP (OVERBURDEN WELL FIELDCREWd LDC,RL W
[SAIWPLING DATE:26-Apr-04 I 27-APT-04 28-Apr-04!Ei~~;d
MONITORING WELL NO.
MW-5 WATER LEVEL METER S/N :N/A
PID READING G PRODUCT LEVEL METER S/N :
METHOD (Pump I Ball)PERISTALTIC PUMP TIME /INITIALS OF COLLECTED SAMPLE :
WELL VOLUME CALCULATION :
C )LUMN ft X VolWELL WELL DEPTH TO WATER CONVERS14ON WELL
DIAM DEPTH (ft)WATER [ft)[YET.]FACTOR L Jai
2'13 .54 (10 1 X 0 .163 1
F_X
mtA gallons X 3.785 l=rs
SCREENINTERVA L
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
3 .54 itl 1 3r4 fil TYPE : DEPTH TO WATER :E~,
STRONG :DEPTH TO PRODUCT:--- I -yourof- (ft)
MINOR~PFODUCTfIHICKNESS : = I ift)
PUMP INTAKE NONE :DON'r SAMPLE IF THICKNESS >OR =TO 0 .1 FATPUMPRTft,INTAK ESTA105
AT AR AT EN DSTT
10 .5 ft. 10 .5 ft .
INITIAL READINGS MEASURED AT GROUNDWATER t AIR INTERFACE INDICATED BELO W
C
OKI'DISWATFR FLOWRATE TIZMP SOPE TURBIDITY PH SOLVED
TIME LEVEL ND) I OXYGE N
(hh :mm :ss) I (ft) - I (ml/min)(dp~(nt (mv)(mgA)
N/A I N/A NiA N/A N/A N/A NIA NIA NIA
---WATER FLOWRATL TEMP brt:L;IURB OK PIDITPH
LVLOCOND 0 ENTIME LEVEL (mv)(mgA)(hh :mm :ss) (ft) (ml/min)(deg C) (US/cm)(niu) unit)
-3 S STABILIZED DRAWDOWN AND REMOVED Ill-%kk -BEGAN LOGGING DATA
-ct s c"5,~~
_?k -9,4-
(31-0 7 . 23 35 k-It'iQ 1X%14 ook-t -i_~C)~93 0 2 1
3 -L-5 712-5 135 R%3o Z-_i,-7,
33o
ELECTRONIC FILENAME - NI A
COMiI&ENTS :
a = CS1
TOTAL VOLUME_REMOVED 77 Fj n j
NOTE :WATER
LEVEL
, PHUUUL, I LLVLL .Mu WELL DEPTH ARE REF ERENCED TD~THE TOP OF WELL CASING .
WUr%r rUVVr-rl I~VIIVIII-AIM T
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
ILOCATION:IBURLINGTON, NC PROC NO: 1 3500 .1
PROJECT NAME, IBURLINGTON MGP (OVERBURDEN WELLS)FIELDCREWd LDC,RL
ISAMPLING DATE:-e"pro* 28-Ap,-04 QQAWQ&-j',A (
4 kONITORING WELL NO .MW-9
WATER LEVEL METER SIN :N/A
PID READING jkJZrt All eW o Ne 1) ppm PRODUCT LEVEL METER S/N :
METHOD (Pump /Ball)1PERISTALTIC PUMP TIME / INITIALS OF COLLECTED SAMPLE:0~ 53- 6 c
WELL VOLUME CALCULATION :
VERSIONWELL WELL D PTH TO WATER CONVER WELLCo)LUMN tt Vol160DIAMDEPTH(ft)WATER (11)x FACTOR L Jai
2-9 .50 &X
X
gallons X 3.785
SCREENINTERVA L
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
2 .0 ft .1 7 .0 f1t TYPE : DEPTH TO WATER ::I:_STRONG~DEPTH TO PRODUCT:---I (ft)
MINOR~1PRODUCT THICKNESS : = I (ft)
PUMP INTAKE NONE : IDON'T SAMPLE IF THICKNESS >OR TO 0.1 FT !
AT START I ATEND
9.50 It 9
.50
Ift
INITIAL READINGS MEASURED AT GROUNDWATER AIR INTERFACE INDICATED BELO W
If A -H FLOWRAT'E I EMP)SPEC TURESIDITY ph GRP D159OLVFL)
TIME LEVEL COND OXYGENW T F
(hh :mm,s (mVmin)eg C us/cm)(ntu) (unit)(mv) (m I
N/A N/A N/A N/A NIA N/A N/A NIA N/A
WATER FLOWRATE TEMP TURBIDITY PH ORP DISSOLVED
TIME LEVEL COND OXYGEN
(hh :mm :ss)(ft)(mvmin)(deg C) (Us/cm)(nt (mv)(m9n)
STABILIZED DRAWDOWN AND REMOVED 0 BEGAN LOGGING DATA
og -7-50 (13 (5 .L 1 L0-7 1 10 - 3 4 4 5,f .7,~ci?c
0`13 -) - ~3 k o /a ID . L3
1,151 kli oOck'3 (o I "
:A IR fxo 15 .(.4
7 9 6 . -t c 3
firl 14 6.47 4,10 6 .,1(,13,3
"4 f,6, ICA 11 0 5~ 7 1 C S-cf 6 -'L%3 136 L),-~4
0151 3 175' 1 ~L-7 J %4 1 13-)C., 'b
ELECTRONIC FILENAME - N/A
OMMENTS :J-,-,04 4)%~j Lz
I=
W 'T LEVE ANTOTALVOLUMEREMOVED=
NO=TE WATER LEVEL,PRQUUU I LtVtL,AND WE DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
Liur\r- r%jvvr-n %,%jivirmvA v
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
LOCATION :BURLINGTON, NC PROC NO : 3500
=-,2 7PROJECT NAME :JBURLINGTONMLPj~V RBIRDEN WELLS)FIELDCREWd LDC,~~L-w-~
SAMPLING DATE:e-z~
ONITORING WELL NO .PMWB-S
WATER LEVEL METER SIN :N/A
p, D READING m PRODUCT LEVEL METER S/N :iCA50 - \
METHOD (Pump /Bail)PERISTALTIC PUMP TIME / INITIALS OF COLLECTED SAMPLE :k-t3o t
WELL VOLUME CALCULATION :
CoWELL WELL DEPTH TO WATER CONVERSION WELL
DIAM DEPTH (ft)WATER (ft)
)LUMN ft X
FACT04 VOL( al)
2-13 .58 o I!,X
X
N/A gallons X 3.785 N/A ltes
SCREENINTERVA L
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
3 .58 ft .1 13 .58 TYPE : I DEPTH TO WATER :
-STRONG~IDEPTH TO PRODUCT :---
MINOR~ IPRODUCT THICKNESS :-(ft)
Pump INTAKE NONE : [DONT SAMPLE IF THICKNESS >OR =TO 0.1 FT 1
AT START .1 AT END
11 .5 ft 11 .5 J
INITIAL READINGS MEASURED AT GROUNDWATER AIR INTERFACE INDICATED BELOW
WATER FLOWHATE TEMP SPEC TURBIDITY PH ORP DISSOLVED
TIME LEVEL COND OXYGENdb(hh :mm,ss)(it) (MI/Mi (us/cm)(ntu) (unit)(mv)(mgA )
N N/A N/A N/A N/A N/A N/A N/A N/A
WATER FLOWHATE TEMP -9150 TURBIDITY PH)OHP DISSOLVED
LEVEL COND OXYGENTIME
(hh :mm :ss) (it)(ml/min)(deg C) (us/cm)(ntu) unit (mv)(ML/1)I STABILIZED DRAWDOWN AND REMOVED k 0 .1- EGAN LOGGING DATA
I 35ct a C ict .4 3 ~0 46,0 -52---20 C53 9
c Y, ok o i q , V, 1"9 t,31 .9 (a -5-< -18 0 ),F
.'4 k 75 toi,-7,5- ?00 33 .4,59 _F1 0-2-5-
1 .9 5~-2 1-1 (ok .15--2 0 e,31 -C-SR JA5- 6--)-l
ELECTRONIC FILENAME - N/A
_OMMENTS:Pim 71
0 M Ro~ CTTOTALVOLUMEREMOVED
NOTE :WATER LEVEL . PRODUCT LIEVEL,AN WMI-L DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
UUMr- rUVVMM %,UIVIrAINI T
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
LOCATION :IBURLINGTON, NC PROC NO : 3500 .1
1PROJECTNAME :BURLINGTON MGP (OVERBU RDEN WELLS)El FIELD CREW :LDC,RL
SAMPLING DATE :26-Apr-04 I ei-A, 0-0 28-Am-o~~I
MONITORING WELL NO.PMWC-S
WATER LEVEL METER S/N : N/A
PID READING ppm PRODUCT LEVEL METER SIN :(CLJS~
METHOD (Pump /Bail)1PERISTALTIC PLIM TIME / INITIALS OF COLLECTED SAMPLE :
WELL VOLUME CALCULATION :
W I[--6EPTHTO CONVERRSI]OGN WELLCTWELL WELL D=Tf~WATER CONVERSION WELL
IDIAMDEPTH(ft) COLUMN (ft)X FACTOR al)S 'WATER (ft)7FACTOR VOL (gal)
0
0 1 1
2-21 .09 X 0LUA 4 1 .163 1
XF----
-T--
H~~
I N/A gallons X 3 .786 N/A ~Iitels
SCREENINTERVA L
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
6 .09 21 .09 ft .TYPE :DEPTH TO WATER :
STRONG :DEPTH TO PRODUCT : (ft)
MINOR : PRODUCT THICKNESS : (ft)
Pump INT KE NONE : DON'T SAMPLE IF THICKNESS >OR =TO 0.1 FT !
AT START I AT END
17.0 ft . 17 .0 ft.
INITIAL READINGS MEASURED AT GROUNDWATER /AIR INTERFACE INDICATED BELO W
WATER FLOWHATF TFMP 5PEC TURBIDITY (PH ORP DISSOLVED
TIME LEVEL COND OXYGEN
(hh nnss)(ft)(MI/mi (US/cm)(ntu) unit (mgA)
N/A N/A N/A N/A N/A N/A N/A N/A N/A
WATER FLOWRATE TEMP -3m TURBIDITY F--ZW DI5SOLVFD
TIME LEVEL COND
(u it)('v)
OXYGE N
(hh :mm:ss)(ft)(ml/min)(deg C) (US/cm)(nt (mg/1)
100& 3 . 1.4 i0o STABILIZED DRAWDOWN AND REMOVED BEGAN LOGGING DATA
to la Icjt ;,q f 01 C 13 .t -'70 0-4r)
1,035-%3 .,4-)t-to ICA, 3 50 1,JL 6~33
4 .574 0,a-810 -t kcI .~tl 50S G .o t
j3 .ac-- t4o Ict -;1,3 513 '1-791 4-5(75'0,2sL
)too i 3 -C4 w Il C, kcwL 51 ;1'-2-s-0 a-C,
A rn P L-'z 0
ELECTRONIC FILENAME - N/A
COMMENTS-C-00 J) f orb TAC- "4 in-L L-
cl
TOTAL VOLUME REMOVE D
'OTE :WATER LEVEL, PRODUCT LEVEL,AND WELL DEPTH A
uul%r- r%jvvr-n %,%Jlwlrmi*a I
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
ILOCATION :]BURLINGTON . NC I PROC NO :1 3500 .1
Ap't ]___.04 2:8PROJECTNAMEiIBURLINGTONMGP (OVERBURDEN WELLS)I FIELD CREW :L122~ELW
SAMPLING DATE :26-Apr-04 I 27-Apr-04
...
28-Apr.04 29±p,-04
MONITORING WELL NO .PMWL-S
WATER LEVEL METER SfN :N/A
rPIDREADINGPRODUCT LEVEL METER S/N :
TIME / INITIALS OF COLLECTED SAMPMETHOD(Pi p/Ball)1C PUMP LE :
WELL VOLUME CALCULATION :
CONVERSION)LU MWELL WATE'CONVERSION WELLF-yn-~!U0
R FACTDR VOL (qal)FACTORDEPTH(ft) N Ift X
0 .16312-7 .60 X
X
gallons X 3 .785
SCREENINTERVA L
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
4.10 7 .60 TYPE : DEPTH TO WATER:
: UCT I CSTRONG:E H TO PRO
I
kf as-ftz (ft)
PT 25 9MINOR:JP!RODK~ES (ft)
PUMP INTAKE NONE : IDONT SAMPLE IF THICKNESS >OR =TO 0A FT !
AT END \a~AT START A,
7 .50 ft .7 .50 ft .
INITIAL READINGS MEASURED AT GROUNDWATER AIR INTERFACE INDICATED BELOW
WATER F=-7EMP SPEC TURBIDITY PH ORP DISSOLVED
TIME LEVEL COND OXYGEN
(hh :mm,ss)(tt)
mVmin)
(deg C)
(uS/cFn) (nt (mv) (mgA )
N/A MA NtA N/A M/A N/A N/A NIA N/A
--WATER FLOWHATE TEMPI -SPEC TURBIDITY PH ORP Dil SOLVED
TIME LEVEL (deq C I
COND
(nt
OXYGEN
(hh mm :ss) (ft)(mVmin)us/cm) U)unit)(mv)(mgA)
STABILIZED DRAWDOWN AND REMOVED BEGAN LOGGING DATA
I it S19 57 5 5-, ~c- I -1 -.4 S - (,p Z.0~ sz_
ci~5
(Q -2-5 -3 ~c( ~)-Z)
5~z)i2ko 1 5- 5- (~,Q 3
ct,
.3 CA cl
olk Lt,7,Aj -Z- _,,3 -L-
S tk 7- I-lkscA 5 LO&-3%S-7- to S'l ot -3
~,L~-7 %~A -L F)4`z- ~"i,2z& Lo t Li cl c k 3 rz
~4 -3 5-0 1 .ri '3 k'l 13 .7 3
ri ,C15 t -7 Cl -!5 2~'3 1(--5 (c %A
ELECTRONIC FILENAME - NI A
COMMENTS :
cl
TOTAL VOLUME REMOVED ED TO THE TOP OF WELL CASING .ILNOTE :WATER Lt:VtL.VHUU)UU IT LE~VVELAND WELL DEPTH ARE REFERENC
LPUr%r_ rUVVr-M kUIVIrAr4 Y
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLIN G
ILOCATION :IBURLINGTON, NC
_EN
PROC NO: 1 3500.1
:::~~PROJECT NAME :BURLINGTON MGP OVERBURDI
WELLS)
FIELDCREW :j LDC,RL w
SAMPLING DATE:26-Apr-04 I 27~Apr-04 28-Apr_04 29-Apr-04
MONITORING WELL NO.PMWM-S
WATER LEVEL METER SfN: N/A
PID READING ppm PRODUCT LEVEL METER S/N:
METHOD (Pump f Ball)PERISTALTIC PUMP TIME i INITIALS OF COLLECTED SAMPLE:
WELL VOLUME CALCULATION :
WELL WELL DEPTH TO WATER CONVERSION WELLFii~DIAM DEPTH (ft)WATER (ft) COLUMN ft X FACTOR VOL at
2'12 .68 X 0 .163 1
X
gallon,X 3.785 liters
SCREENINTERVAL
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
6 .18 12 .68 ft .TYPE : DEPTH TO WATER~
-
i
STRONG :DEPTH TO PRODUCT :---(ft)
MINOR :PRODUCT THICKNESS ,
PUMP INTAKE NONE: 14 DON'T SAMPLE IF THICKNESS >OR TO 0 .1 FT?
AT START I AT END
1 12 .5 ft.
INITIAL READINGS MEASURED AT GROUNDWATER I AIR INTERFACE INDICATED BELO W
WATER FLOWRATE TEMP SPEC TURBIDITY pH OHP Oil SOLVED
nME LEVEL COND OXYGEN
(hh mm:ss) (it) (Mvmin) (cleg C)uS/cm) (nt (mv)(mgA )
N/A N/A N/A N/A N/A N/A N/A N/A N/A
TURBIDITY PH ORP DISSOLVED IWATER FLOWRATE TEM P
TIME LEVEL COND OXYGEN
(hh :mm:ss) (mftin)) I (US/cm) (mv)(mg/l)(ft) (egC (ntu) (unft )
lb go It . to T 5 STABILIZED DRAWDOWN AND REMOVED 011cS"kk -BEGAN LOGGING DATA
lo : 13 lot to 55 1 -(, -0-oio CA i3k a .543 1 1 -1 &4kt 5
jo~ %%_(0 to 3-5,c?k-?T~(12 (0 . cl (_ Sk 3 -L I r6 4
-L 3 It# to ty 5 t _(q (P4 IS C, 1 -3 4k3 5 5,3 -1 ( 1~ -I
Z-'t tk%%o 5 'Ll,0 3,40 S', 3 Z. I I -L 4,0-1
to 3s i.",k T,5 (7-1~ - 5 Z-(%-2 -3 :1 Ici'l 1 .1t
55 1 -L(p,k ~Yi -3 Z_
ELECTRONIC FILENAME - N/A
COMWNTS :
Cl =-T--~,. rt-k,k
TOTAL VOCU-MEREMOVED .
0 N 5 Wt,
~
NOTE :WATER LEVEL, PRODUCT LL~iLU WELL UbTH ARE REFERENCED TO THE TOP OF WELL CASING .
L)Ur%r VUVVr-t1l tVlVlt-ArJ T
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
LOCATION :BURLINGTON, NC PROC NO :3500
.1PROJECT NAME : 1BURLINGTON MGP(OVERBURDEN WELLS)FIELDCREW :j LDC,~iL-w--~:::~
SAMPLING DATE,1,2~~-~28-Apr-04 I -22-Ap~~"C
41MONITORING WELL NO .P-IS
WATER LEVEL METER SIN :N/A
PID READING titn rv"-w Ill ppm PRODUCT LEVEL METER S/N :C, 50
kbcMETHOD (Pump /Sail)1PERISTALTIC PUMP I TIME / INITIALS OF COLLECTED SAMPLE :A
WELL VOLUME CALCULATION :
CoWELL WELL DEPTH TO WATER CONVERSI WEEL)LUMN ft)LU X VOLCo
DIAM DEPTH (ft)WATER (ft)
2-X
n X PE~
gallons X 3 .785 liters
SCREENINTERVA L
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
1 .71 11 .71 Ift TYPE : DEPTH TO WATER :I
STRONG~DEPTH TO PRODUCT :---c
MINOR, JPRODUCTTHI =
Pump INTAKE NONE :DONr SAMPLE IF THICKNESS >OR TO 0 . 1 FT!
AT START AT EN D
11 .21 ft 11 .21
ft .
INITIAL READINGS MEASURED AT GROUNDWATER AIR INTERFACE INDICATED BELOW
WATER FLOWRATE T SPEC TURBIDITY PH ORP DIS OLVFv
TIME LEVEL I COND
unit)(mv)
OXYGEN
(hh mm's (ml/min) (deg C)(uS/cm) (ntu)I (mg/0
N/A N/A N/A N/A NIA N/A NIA NIA N/A
WATER FLOWRATE TEMP SPEC TURBIDITY (pH)ORP DISSOLVED
TIME LEVEL COND OXYGE N
(hh :mm :ss)(ft)(ml/min)(deg C) (Us/cm)(ntu) unil (mv) (m
I -STABILIZED DRAWDOWN AND REMOVED k C3 "A BEGAN LOGGING DAT A
613 k I -?o k 9 -19 4 4,A L-2-9 &.~g -8~cn,t~
6,34 -102 ~ V, ) 'k L .5-k ~ 8 -90 c-, (I
~5,3 -)a-0 q,3 R (~ I 'A q~j 0 --93 0~11 ~
i GILL Y,31~~-oo k5s .19 6t,-~.qX, 4 .Lo .-.g 3 01 1 C;
w"i k n
uz Z;kloe
ELECTRONIC FILENAME - N/A
W
COMMENTSNO;TEATER LEVEL, PRODUCT LEVEL,AN WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASIN GCl
uur%= rvvvr_n %~VlvlrM14 T
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLIN G
LOQ~TION :BURLINGTON, NC _T PROC NO :35D0
.1===1PROJECT NAME : BURLINGTON MGP (SHAL FjAg2,BRWELLS FIELD CREW :LDC,RL~~-
[SAMPLING DATE :26-Apr-04 I 27-Apr-04
_A _0 4
MONITORING WELL NO.DMW-l
WATER LEVEL METER S/N:N/A
PID READING m PRODUCT LEVEL METER SIN :
METHOD (pump /Ball)IPERISTALTIC PUMP TIME t INITIALS OF COLLECTED SAMPLE :
WELL VOLUME CALCULATION :
WELL WELL r DEPTH TO WATER CONVERSION WELI-
DIAM DEPTH (ft)
,~,R
It COLUMN (ft)X FACTOR
VOL al
2-29 .02 2Z2-, (~4-X 0.163 1
X
N/A gallons X 3 .785 N/A
SCREENINTER V
FROM DETECTED ODORS FREE PRODUCT MEASUREMENT
16 .72 ft-1 TYPE :DEPTH TO WATER :i
STRONG :DEPTH TO PRODUCT :---N'ov-%c (ft)
MINOR :PRODUCT THICKNESS :(ft)
I Pump INTAKE ~LONE :DON'T SAMPLE IF THICKNESS >OR =TO 0 .1 FTI
ATSTART AT EN D
24 .0 ft 24.0
:4.
(A, A ,
INITIAL READINGS MEASURED AT GROUNDWATER /AIR INTERFACE INDICATED BELO W
WATER ITLOWRATE TFMP SPEC PK U11 SOLVED
TIME LEVEL I COND I I mv)
XYGEN
(hh IMMISS (ft)[ml/mln) (deg C) (u~unit)U(H"imgm-
N/A N/A N/A N/A NIA NIA N/A N/A N/A
WATER FLOWRATF T -'9M TURBIDITY DISSOLVED
TIME LEVEL COND OXYGE N
(Lh (tt) (mVmin)(deg C) (US/cm)
(nt unit) Mv)
(mgA)
STABILIZED DRAWDOWN AND REMOVED 3 k-7 BEGAN LOGGING DATA
I
I ~~-Z- c (~p Cp 6-1 (,,,S L)t
5~SQ j-c-l G (-1 0,-2-
-A (~ &A ('0
I IS ~k --72- c, ~+s
ELECTRONIC FILENAME - N/A
COM~KNT§
Cl
TOTALVOLUM E REMOVEDg-
NOTE :WATER LEVEL,FHUL)ULC;IT LEVEL,AND WEREWH ARE REFERENCED TO THE TOP OF WELL CASING .
wur%r- rvvvcm tvivirAi,4 T
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
LOC~ATJON :IBURLINGTON, NC I PROC NO : 1 3500 .1
PROJECT NAME : IBURLINGTON MGP (SHAL FRACT EIR WELLS)FIELDCREW :j LDC,RLW
SAMPLING DATE:I ~ I 28-Apr-04 U c
ONITORING WELL NO .DMW-2
WATER LEVEL METER S/N :N/A
PID READING NUT ~jJ6,cf*jppm PRODUCT LEVEL METER S/N :~q 50 -1
1(.0 -,, /METHOD (Pump /Ball)1PERISTALTIC PUMP TIME I INITIALS OF COLLECTED SAMPLE :jut
WELL VOLUME CALCULATION :
CoFDEPTH TO [CCENIVERSION LL'aWELL WELL EPTH TO WATER CONVE
'RS"ON WEWATER (ft)FACTOR
_.1,]
DIAM DEPTH
(ft) )LUMN ft X
FACTOR -
2'32 .08 ;Lq, 13 X IF 3j-_5__j
X
N/A gallons -F-x T-3 .7-as--T-N/A
SCREENINTERVA L
FROM TO DETECTE ODORS FREE PRODUCT MEASUREMENT
22 .08 32 .08 ft .TYPE :DEPTH TO WATER :i
STRONG :DEPTH TO PRODUCT :---"AejlE (ft)
MINOR~ iPRODUCT THICKNESS:
Pump INTA E NONE : IDON'T SAMPLE IF THICKNESS >OR =TO 0 .1 FT!
I
ATSTART .1 ATEN D
27 .0 ft 27 .0 ft.
NITIAL READINGS MEASURED AT GROUNDWATER /AIR INTERFACE INDICATED BELOW
WATER FLOWRATE TEMP (SPEC TURBIDITY PH ORP DIS
TIME LEVEL COND OXYGEN
(hh 'MM7SS)(ft) (ml/min) (deg C) US/CM)(nt (Mv)(mqA )
N/A N/A N/A N/A N/A N/A N/A N/A N/A
(r-WATER FLOWHATE TEMP -PYc TURBIDITY PH _7RP DISSOLVE D
TIME LEVEL OXYGEN
(hh ~mm~ss) 00 (ml/min) (deg C)(ntu) (unit)(Mv)(mgA)
STABILIZED DRAWDOWN AND REMOVED 4,0 EGANLOGGINGDATA
3 0 0 ty,sV LC5-o c -
"1 9 30z O&IS 5-Lts 1 9 A o,
kO,O -~oo N&V~!:j5 :2_T-40 -3 o ~C7
ELECTRONIC FILENAME - N/A
IDOMMENTS :Cl
TOTAL VOLUME REMOVED L
NOTE:WAT R LEVEL,FHUL)UUl L~W,ANU VVtLL UtVi "ARE REFERENCED TO THE TOP OF WELL CAS11Z ."M
DUKE POWER COMPAN Y
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
ILOCATION : BURLINGTON, NC PROC NO :3500.1
1 PROJECT N ME :SHAL FRACT BR WEL L
J SAMPLING DATE:Ap,~I -28-AZ
MONITORING WELL NO .71
WATER LEVEL METER SfN :N/A
PID READING Ll
m
PRODUCT LEVEL METER S/l 5-0-
METHOD (Pump /Ball)A~P~TIME / INITIALS OF COLLECTED SAMPLE :
WELL VOLUME CALCULATION :
UMN Ift
WELL
WELL DEPTH TO WATE CONVERSION
E ATE RYTT--]O LDIAMDEPTH(ft)WATER [ft)X FACTOR
2-36.00 X 0 .1631r
X
N/A gallons X F 3 .785 NIA ~Iiters
SCREENINTERVA L
FROM TO DETECTE ODORS FREE PRODUCT MEASUREMENT
27 .0 36 0 Ift .TYPE : IDEPTH TO WATER:
STRONG :InEPTH TO PRODUCT~---I Ill ill (ftj
MINOR :RODUCTTHICKNES&=I (ft)
F--PU`M-P--7iNT:A:K=E NONE :7'-4DON7 SAMPLE IF THICKNESS >OR =TO 0 1 FT I
AT START AT END
34.5 It 34 .5 ft .
INITIAL READINGS MEASURED AT GROUNDWATER I AIR INTERFACE INDICATED BELOW
ER FLOWRATE TEMP SPEC TUR"'O'=Pnit) ORP DISSOLVED
TIME CO OXYGEN
:mm :ss)(ml/min) (deg C) (uS/c-m)Int
(U
[mv)(MgA)
N/A N/A N/A N/A N/A N/A N/A N/A
I ORP Dili SOL--WMTN- -FLOWRATE TEMi UPbU VED
TIME LEVEL COND
I
OXYGE N
(hh :mm :ss)(ft)(ml/min) (deg C)(uS/cm) unii (mgA)
11AX3 15okil j, 00 STABILIZED DRAWDOWN A D REMOVED 4 0 BEGAN LOGGING DAT A
oill-till,200 > 8 3 .2-,7 f .4 2 --15 q C~ L J~
100 5,;L >-;z .53 6,pstt o .Ski
100 5't`7
11ELECTRON C FILENAME - N/A
ICOMMENTS:
VOLUME REMOVED
IVATER LEVEL.PRODUCT LEVi AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
LJUMr- tUVVrtl t~UIVIrAIM T
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
ILOCATION :~TBIURLINGTON, NC PROC NO : 3500.1
1 _26 ~PROJECT NAME : IBURLINGTON P FRACT BR WELLS)FIELDCREW :j LDC,ALVV El
SAMPLING DATE :r227=
MONITORING WELL NO.PMWH-BR
WATER LEVEL METER SIN :N/A
PID READING m PRODUCT LEVEL METER S/N :N~- ~
METHOD (Pump /Ball) TIME / INITIALS OF COLLECTED SAMPLE : k k k5-L-D C
WELL VOLUME CALCULATION :
CONVERSIONUACo0)LUWELL WELL DEPTH TO WATE'CONVERSION WELLWAIER166~EEH -5 M ft
ATER E nn-lDIAM DEPTH (ft)WATER ft
)LUMN
tt X FACT VOL (gal)N FACTO RRPTTo
0 .16312'20.72 X
X
NIA gallons X 3 .785 N/A
SCRFENINTERVA L
.1 TO DETECTED ODORS FREE PRODUCT MEASUREMENTFROM
19 .72 ft 20 .72 TYPE : DEPTHTOWATER :1
STRONG : DEPTH TO PRODUCT :Pj &~Ar-
MINOR~ PRODUCT THICKNESS:
PUMP INTAK NONE : DON7 SAMPLE IF THICKNESS >OR =TO 0.1 FT!
AT START I AT EN
20 20 .0
INITIAL READINGS MEASURED AT GROUNDWATER AIR INTERFACE INDICATED BELOW
ATER FLowRATE TEMP SS`iEr-))TUR131UITY pH ORP DISSOLVED
CONE OXYGENTIME WLEVEL
(u (,tu)I
(hh :mm~ss)(ft)(ml/min) (deg unit)(mv) (m
m
/
YN/A N/A NIA N/A N/A N/A N/A N/A NN/AA
-1 EWATER FLOWRATE TEMP TO TURBIDITY --PnR---DISSOLV v
TIME LEVEL COND OXYGEN
(hh :mm :ss)(ft)(mllmin) (deg C) (US/cm)(ntu)
(U it)(mv)
(mgA)
W3 46 c~, -t 0 JEC)STABILIZED DRAWDOWN A D REMOVED 0 % " I - EGAN LOGGING DATA
10 -j c~ ci,5 2--~; c 0 t 5,S9 V?319 I~ 6 ; --)1
In55 'i 1 5 t~36 0 /5"(-,~1?.2-?R (~,4y - -7~-
k koo ci,55,3(Ko V6 6 2 -2 0 (o 9 -7 q
it 0 9 .5'5' 390 IS,~e.(- ~f4 1 3 o3 t,5 - 7 ~;-0 .
cw~ 5-t L ~ff 6 -Z -L 4 L 8 0 -)L.-21
ELECTRONIC FILENAME - N/A
C,~O M-ME N T S :
Cl =
VTR
TA VOLUME
REMOVED
NOTE,WATER LEVEL, PRODUCT L VELA ARE REFFHtNL;tU i u FHE TOP OF WELL CASING .0 L D&EPTH
DUKE PQWhH UUMPAN Y
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
LOCATION :BURLINGTON, NC PROC NO :3500.1
1PROJECT NAME : IBURLINGTON MGP (SHAL FRACT EIR WELLS)--FIELD CREW:LDC,RLW
ISAMPLING DATE :26-Apr-04 I 27-Apr-04 1 2 -Apr-04 I 29-Apr-04
MONITORING WELL NO .PMWI-BR
WATER LEVEL METER SfN :N/A
PID READING m PRODUCT LEVEL METER S/N :
METHOD (Pump/ Ball)1PERISTALTIC PUMP TIME /INITIALS OF COLLECTED SAMPLE :
WELL VOLUME CALCULATION:
U=C oWELL WELL H Tf~WATER CONVERS14ON WELL
DIAM D Fl!=Tl )LUMN ft
R I icG=
ft I
VOL(a[)EPTH (ft) E. X FACTO R
2-38 .07 X 0 .1631
X
N/A gallons X 3.785 N/A ll ~ters
SCREENINTERVA L
FROM TO DETECTED ODORS FREE PRODUCT MEASUREMENT
28 .07 38 .n7 ft .TYPE : DEPTH TO WATEk i
STRONG :DEPTHTOPRODUCT~--ftj iti "v (ft)
MINOR : PRODUC (ft)
PUMP INTAKE NONE DON'T SAMPLE IF THICKNESS > 08 =TO 0 .1 FT I
AT START AT END
33 33.0 ft.
INITIAL READINGS MEASURED AT GROUNDWATER AIR INTERFACE INDICATED BELOW -
AV
k:K
FLOWRATE1 TEMP SPEC TURBIDITY PH ORP DISSOLVED
nmE LE EL COND OXYGENWI
(hh I (nVrrgn)(deg C) (us/cm)(nt (mv) (mgA)
N/A N/A N/A N/A NIA N/A N/A WA N/A
--WATER FLOWRATF T -MFEU-TURBIDITY PH GRP DISSOLVE D
TIME LEVEL COND OXYGEN
(hh ~:ss) (ft)(mlimin)dog C) (us/cm)unit (mv)(mgA)
10"OF ko0&-L-i7o STABILIZED DRAWDOWN AND REMOVED 'tk 5 - BEGAN LOGGING DATA
(D 1 -7 'K
fo(193 klo I7iL(0 5-7"1
70
Lk
ELECTRONIC FILENAME - N/A
CONJ&ENTS :
c l
TOTAL VOLUME REMOVED 5'~"J k
NOTE~WATER LEVEL,PRODUU I LEVEL,AND WELL DEPTH ARE REFERENCED TO THE TOP OF WELL CASING .
DUKE POWER COMPAN Y
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
LOCATION :PROC NO: 3500.1
I ~29~:PROJECT NAME : BURLINGTON MGP (SHAL FRACT 13R WELLS FIELD CREW :LDC,RLVV
]SAMPLING DATE :26-Apr-04 I 27-Apr-04 1 28, ~r-04
_A
MONITORING WELL NO . PMWL-B
WATER LEVEL METER S/N :N/A
PID READING Ppm PRODUCT LEVEL METER S/N : -I
I METHOD (Pump I Ball)1PERISTALTIC PUMP TIME / INITIALS OF COLLECTED SAMPLE: 13'3 ~
WELL VOLUME CALCULATION :
okV&Slok --WELLVOL atWELL WELL FOEPTH TO WATER CONVERSION WELIL
DIAM DEPTH (tt)I WATER (ft) I COLUMN ft X FACTOR VOL (gal)
2-24 .46 1 SN 35-J I,r . k,X 0.163 1
X
N/A gallons X 3 .785 NIA liters
SCREENINTERVAL
FROM TO DETECTE ODORS L FREE PRODUCT MEASUREMENT
14 .0
ft .1
24 .0
ft.
TYPE*JDEPTHTOWATER ~
RO:N G DEPTH TO PRODUCT :---f
MINOR (ft)TK
F-`PU`M-P IN KE NONE~DON'T SAMPLE I F THICKN ESS >OR TO 0. 1 FT I
AT START
~:T~A
tj AT END
20 .0 20 .0 ft .
INITIALRE DINGS MEASURED AT GROUNDWATER IAIR INTERFACE INDICATED BELO W
WATER FLOWRAT EMP I -SPEC TURBIDITY pK oRP--DISSOLVED
TIME LEVEL COND u)OXYGEN
(hh :mm :ss)M-(mVmin) (deg C) (us/cm)(nt (unit)(mv)(mg/1)
N/A N/A N/A N/A N/A N/A NIA N/A N/A
---WATER FLOWHATE TEMP -3PEC TURBIDITY PH ORP ISSOLVED
LEVEL COND OXYGENTIMEeqC)(ntu)(unit)(mv) mg1l)(hh :mm :ss)(tt) ml/rnin)(us/cm )
/155 G 1 33,c-,=j STABILIZED DRAWDOWN A D REMOVED 3,-J-,kk BEGAN LOGGING DATA
("Oo 5,0 Z~-3 z-ot(0'3
U ~Q 5-c t9k<~5 (a Io I ON3
c Cl ciz~ ((p ~,2,t i t-j z-; -y i (,,(? 18 0 .:1 kP
I o t --xx I
-3k1l rl -2--2 CA I
3 1 ct Ikl Q,
5A3 Z-0 k-2- -2-3 3 Lt-1 I (Ot kl V1 C)
ELECTRONIC FILENAME - N/A
CO!IeAE~NTS:
clW-~~
"I
OC SAMPLE COLLECTED FOR 8270
TOTAL VOLUME REMOVED =:~ , 1 -5 -THE TOP OF WELL CASING .11 INOTE :WATER LEVEL, PRODUL;I LEVEL,AND WELL DFV i H ARE REF
UUKL FUWth kUlVlrAINl T
GROUNDWATER MONITORING DATA SHEET FOR LOW FLOW SAMPLING
LOCATION :13URLINGTON NC PROC NCO :35M.1
PRcOjEcT N ME:BURLINGTON MGP (SHAL FRACT 13R WELLS)
ISAMPLING ATE:26-Apr-04 27-Ap,-04 I 28-ADr-04 I 29-ADr-04
MONITORING WELL NO .PMWM-BR 71
WATER LEVEL METER S/N : N/A
PID READING I ~b ppml PRODUCT LEVEL METER SIN :kckLt S - k
METHOD (Pump/Ball)JPERISTALTIC PUMP I TIME/INITIALS OF COLLECTED SAMPLE
WELL V E CALCULATION :
WELL WELL WATER FCONVERSICI~N WELL0)LUMN ft X
DIAM DEPTH (ft)I FACTOR I VOL al
2'19 .16 X
X
NtA gallons X 3 .785 NIA literT~]
R SCREENINTERVAL
FROM TO ODORS FREE PRODUCT MEASUREMENT
15 .66 ft . 19 .16 ft .TYPE : DEPTH TO WATER :
STRONG :DEPTH TO PRODUCT :
MINOR : PRODUCT THICKNESS :
fFPUMP INTA=KE NONE~EENT SAMPLE IF THICKNESS >OR =TO 0 .1 FT I
F_~VT START AT END
1 1 17 .5 f II I
INITIAL READINGS MEASURED AT GROUNDWATER AIR INTERFACE INDICATED BELO W
- 'WATE
SPEC TURBIDITY pK CORP DISSOLVED
TIME LEVEL COND (ntu) (unit
OXYGEN
(hh :mm :rs (mVmin) (deg C)(uSlcm)(mgA )
1 (0) 7FO~~~_
W,:VA~~~N/A ~N/A N/A N/A N/A N/A N/A N/A
WATER- FLOWRATE IDITY ph UHe SOLVED
TIME LEVEL CON XYGE N
(hh :mm:ss)00 (mVrnin)do C) u /(ntu)(unit)(mv)7o 1)
(0 -1 5 STABILIZED D AWDOWN A D REMOVED -BEGAN LOGGIII G DATA
s'3 5-~'R-j 44 2t 1kci
-7 S It(41 V,%(p 31 2.1
3
_31t k, Qz) S 3 5
5 A
5 A'&1-14
I V 3 3
-2-,'-5 i'L I~-L Ttl~.3 3 -1 (1 Cos
ELECTRONIC FILENAME - N/A
GOINTS :
cl =:::~,
TOTAL VOLUME REMOVED=7,: A~,\PN S
NOTE :WATER LEVEL,FKUL)UU I LtVtL~AND WELL DEVI H ARE REFERENCED TU I HE I UV Ul-WELL t~ASING .
CHAIN OF CUSTODY READ AND ANALYSIS REQUEST FORM
Duke PowerAnalytical Laboratory Services i i Analytical Laboratory Use Onl yPhDuke- ------------------------------------ ----------------------------------------------------------------------a i !Lbas a Sample Cie.. Sample NCMail Code MG03A2 (Building 7405)a
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MW-5 X 1 1 3 5
MW-9 X 1 1 1 1 32.9/01 07 .-~5- 5
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PMWL-S X I I 1 3 5
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23)S*811L=k9d By %-Dtarr.m
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24)Co.ments - PLEASE HARD COPY AND ELECTRONICALLY TRANSER THE ANALYTICAL RESULTS 'Other
I ' Add .Cost Will Apply
CHAIN OF CUSTODY RECORD AND ANALYSIS REQUEST FORM 0
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Duke PowerAnalytical Laboratory Services i i Anal Ical Laboratory Use Onl yDuke- --------"'Page t otMail Code MG03A2 (Building 7406)!UMS Sample Class sample *Originating sc-!!~DISTRIBUTION13339Hagers Ferry Rd '011-,4P)?- oool /V7 C7 )0 Fro mAftwEnergya.i I --ORIGINAL to LAB ,
For Detailed Instructions, see : Huntereville,N . C . 28078 !Logged By Date &Time SAMPLE PROG COPY to CLIENT
hap :11de~rIessenv/coc/ Fa [phone] 1 Ground Water
-.V..9L i NPDES.............. (7 4jjLS-.qq:Lk
I)Project Name 2)Phone No:875-5257 iVendor Drinking Water
BURLINGTON MGP (OVERBURDEN WELLS)dill UST -
Cooler Tento (C RCRA Waste
E 3)ClIent C.Campbell If R . Roberts /T. Hunsucker 4)Fsx No:875.5032 :pO
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0-------------41 012 14Collection I nLABUSEONLY Chem formation Em < x .90 <w13 Q. i-.9 .9 C,i "Lab to i Desktop No .Sample Description or ID Date Time Signature z
TRIP BLANK x 3 n1a 3
A-1 MW-3 X 1 1 1 1 3 5
PMWB-S x 1 1 3 5
'91 E P-IS x 1 1 3 5
0 PMwC-S L /0',x 1 1 3 5
N1w-5 x 1 1 3 51
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-E -7 Days
23)SeaVLmk*d By Datemme SealedtLock Opened By Datemme E0 0 -48Hr
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CHAIN OF CUSTODY RE ARD AND ANALYSIS REQUEST FORM
Duke erAnalytical Laboratory Services i i ADuke---------------------------------r- -------------------n -a 1-y-t-1-c-a-1. -L-a-b- -o-r-a-t-o-r-y--U--s e----n--1y ------------------ I
"'P aMail Code MG03A2 (Building 7405)!Umbw Sample Class Sampi I ge -L OlOrlgln:tslng INC DISTRIBUTION13339Hagers Ferry Rd &P C--Energy..From ORIGINAL to LAB,For Detailed Instructions, see : Huntersville,N . C. 28078 1 IL09900 By Date &TImo SAMPLE PROG Rhttp:/1de~/essenvIcoc/ [phone] i i Ground Water COPY to CLIENT-------------E~~:.TLN ~ T§-A.Rk .............i i I&dc /-,0/-0 41 7 - '1-5-- NPDES,)Project Name 2)Phone No : 875-5257 IVOndor 0 C~Drinking WaterS)BURLINGTON MGP (OVERBURDEN WELL UST
Cooler Tenno (C RCRAWasteE3)Client C.Campbell R . Roberts /T . Hunsucker 4)Fax No :875-5032 :PO 0 "Pr sem .:I=C2=H 0 . 3=H
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MW-5 x 1 1 3L-7
MW-9 x 1 1 3 1 1 5
PMwM-S x 1 1 3 5I Z, (,A
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FIELD BLAN K0t,3 n/a 5
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Daterri eC~-o I c a BY:2"Requested Turnaroundc740sZVA J-- 'P .-Relinquished By Datarnme opted By: M C124ol-oll"A),4p "i -, 2 5 14 Days I'/-0 M 0J=:aRelinquishedByDatsrnme~ Accepted By:638 -tarrime -5" 0 a -1 Lays
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pkDuke Duke Fower Analytical Laboratof yOftwer.Phone .[phone] Fax 704-875.,5038
13339 Hogefs Ferry Road Huntersville NC 28078-7929
McGuire Nuclear Complex - MG03A2
4C;4ert11i4-_at,a co f
New York Slate Department of Health Certification # f 17f7
Oklahoma Department of Environmental Quality Certification # 9930
Kansas Department of Health and Environtrienil Certificate # E. 1031 1
North Carolina Department of Health &Human Services Certification #37804
South Carolina (DHEQ)Laboratory 10 # 99005 North Carolina (DENR Certification 4 24 B
Station Name :BURLINGTON Job Number : 04-APR-0001
i
Sample ID #:24010615 Desktop #Customer ID L .D CAMPBELL
Sample Description : MW-3
CollectionDate : 27-Apr-0415 :50 :00 Date Received in Laboratory: 01-Apr-04 TypeofSample : OBWELLS
ReferenceMethod :EPA310.1/SM2320B Data Posted: 511712004 16 :53 :57
ALKALINITY (TOTAL INFLECTION POINT)ALKALINITY 0 .74 mtq/L
Referent;eMethod :EPA310.1/SM232013 Data Posted : 512012004 14 :59 :1 0
ALKALINITY BY CALCULATION -_ _-ALKALINITY 37 .00 mg/L
ReferenceMethod :EPA200 .7/6010B Data Posted :5f7/2004 13 :21 :1 6
RON BYACP (DIGESTED)IRON 0 .188 rng/I
Reference Method :EPA 200 .716010B Data Posted 517/20134 13 211 6
MANGANESE BY ICP (DIGESTED)MANGANESE 0 .037 mgLL
Reference Method EPA 300o Data Posted 5/3/2OD4 11 57 :1 3
NITRATE JIC).---NITRATE 2 .97 mg/L
ReferenceMethod EPA300 .0 Data Posted 514/2004 08 :40 :05
NITRATE BY CALCULATION (MG-NIL)NITRATE 0 .67 mg-NIL
Reference Method .EPA 3WO Data Posted 51312004 11 :57 1 3
SULFATE [IC)SULFATE 13 .10 mg/L
Sample ID #:24010616 Desktop #Customer ID :L.D . CAMPBELL
Sample Description : PMW`B-S
Collection Date : 27-Apr-04 14 :30 :00 Date Received in Laboratory : 01-Apr-04 Type of Sample : OB WELLS
ReferenceMethod EPA310.11SM2320B Data Posted :5/17/20D4 16 :53 :5 7
-ALKALINITY.(TOTAL INFLECTION POINT)ALKALINITY 5.69 meq/L
ReferenceMethod EPA310.1/SM2320B Data Posted 512012004 14 :591 4
ALKALINITY BY CALCULATION ALKALINITY 285.00 mg/L
Referen~lvlethod :EPA200 .7/6010B Data Posted .5f7/2OD4 13 :21 :1 7
IRON BY ICP (DIGESTED)IRON 20.772 mg/I
ReterenceMethod EPA200.7/60108 Data Posted 5r712004 13 21A 7
MANGANESE BY ICP (DIGESTED)MANGANESE 0.169 mg/L
Reteren"Method :EPA300 .0 Data Posted 5/312004 11,57 :42
NITRATE (IC)NITRATE 1 .70 mg/L
Reference Method :EPA 3000 Data Posted 51412004 08:40 :06
NITRATE BY CALCULATION JMG-NIL)NITRATE 0 .38 mg-NIL
Vko . ..... 111~hnlr~Noa l
G1111,ord 512112004 11 05 411 httpJ/dewww/csscnv/lab srv/i%,: .
P
BUke 1) U Ke -rower Anaiyucal LaDora-Lor yOrPower.Phone:[phone] Fax [phone]
A D&&V C~ 13339 Hagers Ferry Poad Huntersville,NC 28076-7929
McGuire Nuclear Compilgir - MG03A 2
C 4e rt i 1 1 4--~a t 4-- 4o f AMnmlyrsis
Now York Slate Department of Health Certification #f f 71`7
Oklahoma, Department of Ervironmental Quality Certification # 9930
Kansas Departmitint of Heagh and Erivironmeril Corlificale # E-1031 1
North Carolina Deparlment of 1-talth &Human Services Ceilificalion # 3780 4
South Carolina (DFlEQ Laboratory ID 9 99005 North Carolina (DeVR Cedificabon #246
Station Name :BURLINGTON Job Number : 04-APR-0001
Sample ID #:24010616 Desktop #Customer ID :L .D .CAMPBELL
Sample Description : PMWB-S
Collection Date : 27-Apr-04 14 :30 :00 Date Received in Laboratory : 01-Apr-04 Type of Sample : OB WELLS
Reference Method :EPA 300 .0 Data Posted: 5/3/2004 11 :57:4 2
SULFATE (Lq)_SULFATE 11 .09 mg/L
Sample ID 24010617 Desktop #Customer ID,L .D . CAMPBELL
Sample Description :P-II S
Collection Date: 28-Apr-04 11 :35:00 Date Received in Laboratory : 01-Apr-04 TypeofSample : OBWELLS
ReteienceMethod EPA310 .11SM2320B Data Posted : 5/1712004 16 :53 :57
ALKALINITY_(ICLTALINFLECT!Q?tF!Olt~T)ALKALINITY 6 .31 meg/L
ReferenceMethod EPA310 .11SM2320B Data Posted : 512012004 14 59 1 7
ALKALINITY BY CALCULATION ALKALIN17-Y 316.00 mg1j..
Reference Method :EPA 2001/60108 Data Posted: 5nI2004 13 :21 :1 7
URQN[BY ICP (DIGESTED)IRON 17 .962 mWI
RefefenceMethod :EPA200 .7/6010B Data Posted :517/20DAI 13 :21 :1 8
MANGANESE BY ICP (DIG STED)_MANGANESE 2.952 mgtL
Reference Method :EPA 300 .0 Data Posted 5/5f2OG4 11 :15 :08
.NIT-F;LA-T E.(IC)_NITRATE < 0 .10 g!g/L
Referen~ Method :EPA 300 .0 Data Posted : 5/612004 12 12 :3 1
NITRATE BY CALCULATION (!4q-N/L)_ NITRATE <0.02 rn -Nll~
Reference Method :EPA 300 .0 Data Posted : 5151'2004 11 :15 :0 8
SULFATE (!P)._SULFATE 16 .08 mg1L
Sample ID #:24010618 Desktop #Customer ID L .D . CAMPBELL
Sample Description : IPMWC-S
Collection Date : 26-Apr-04 111 :05 :00 Date Received in Laboratory: 01-Apr-04 TypeofSample : OBWELLS
Referen~Method :EPA310.1/SM2320B Data Posted . 5117/2004 16 53 5 7
ALKALINITY (TOTAL INFLECTION POINT)ALKALINITY 4 .07 meq/L
ReferenceMethod :EPA310.11SM23208 Data Posted : 5/2012004 14:59 :2 1
ALKALINITY BY CALCULATION ALKALINITY 204 .00 mgIL
ReterenceMethoa:EPA 200 .7/6010B Data Posted : 51712004 13:21 :1 8
IRON BY ICP (DIGESTED)IRON 25.119 mg/I
V21121HU 11 05 41)h1tp :I/dcw~wIcssenv/]ah-srv/1"', 2"',
Duke MiKeFlowerAnatyucal LaDorator yPower.Phone 704 .87-'L5245 Fax [phone]
13339 Hagefs Ferry Road Huntersville,NC 28078-7929
McGurfe Nuclear Complex - MG03A 2
c3if Anniysi-s
New York State Department of Health Certification #f f 717
OWhoms Department of Environmental Quably, Ceribcalion If 9930Kansas Department of Heagh and Environment Certificate # E- 103 ff
North Carolina Department of ftelth &Human Services CeffAcalion # 378N
South Carolina (DHEQ Laboratory 10 # 99005 North Carolina (DEWR Certification #24 8
Station Name :BURLINGTON Job Number: 04-APR-0001
Sample 10 24010618 Desktop if Customer ID :L .D . CAMPBELL
Sample Description : PMWC-S
Collection Date : 26-Apr-04 11 :05 :00 Date Received in Laboratory : 01-Apr-04 TypeofSample : OBWELLS
ReferenceMethod :EPA200 .716010B Data Posted:51`7/2004 13 :21 :1 8
MANGANESE BY ICP DIGESTEDI MANGANESE 2 .714 mg/L
Reference Method :EPA 300 .0 Data Posted 5r3f2004 15 :40 20
NITRATE IC)NITRATE 0 .3 0- - - -mg/L
ReferenceMethod EPA300 .0 Data Posted 5/6/2004 12 :05 :53
NITRATE BY CALCULATION [MG-WL)NITRATE 0 .07 mg-NIL
Reference Method :EPA 300 .0 Data Posted 51312004 1 5 40 2 0
SULFATEtIC)SULFATE 0 .25,mg!L
Sample ID #:24010619 Desktop N Customer ID :L .D . CAMPBELL
Sample Description : MW,S
Collection Date : 27-Apr-04 13 :30:00 Date Remived in Laboratory: 01-Apr-04 TypeofSample : OBWELLS
Reference Method :EPA310.1/SM2320B Data Posted :5/1712OD4 16:53 :57
ALKALINITY (TOTAL INFLECTION POINT)ALKALINITY 9.38 arm cill-
Referenc*Method :EPA310.1/SM2320B Data Posted 512012GD4 14 :59 24
ALKALINITY BYPALCULATION ALKALINITY 469 .00 mg/~
Reference Method :EPA 200.716010B Data Posted 5nt2004 13:21 :1 9
IRON BY ICP_(DnESTED)_IRON 4 .138 mg/I
Reference Method :EPA 200.7/6010B Data Posted:5f7/2004 13:21 :1 9
MANGANESE BY ICP (DIGESTED)MANGANESE 0.502 mg/L
Reference Method :EPA 300,0 DataPosted 513/200411 :58 :1 0
NITRATE (IC)NITRATE 0.19 mgfL
Reference Method EPA 300 .0 Data Posted . 51412OD4 08 :40:0 7
NITRATE BY CALCULATION (MG-N/L)NITRA TE 0.04 mg-NIL
Reference Method EPA 300 .0 Data Posted 513/2004 11 :58 : 1 0
SULFATE (IC)SULFATE 39 .47 mg/L
hn,,,Nv .1511112004/1 05 41)litip ://d~%~,v~Icsscn~/lah-srvI Pi,, i .,j I
P vuke vuRe FowerAnaiytical LaDoratory
oftwer.Phone [phone] Fax:7G4-675-5038
A ~6.,C~13339HagersFerly Road HuntersvilleNC28078-7929
McGirrie Nuclear Complex - MG03A 2
Ctertllic--~atii-- 4of Atimalys--i s
New York State Department of Health Certification #f f 717
Oklahoma Department of Environmental Quahty Certification N 9930
Kansas Department of Heath and Environment Certificate # E- fO3 I f
North Carolina Department of Health &Human Services Certification # 37804
South Carolina (DHE~Laboratory ID # 99005 North Carolina (DENF0 Certification #248
Station Name :BURLINGTON Job Number : 04-APR-0001
Sample ID #:24010620 Desktop #Customer ID :L .D . CAMPBELL
Sample Description : MW-9
Collection Date : 28-Apr-04 09 :55:00 Date Received in Laboratory : 01-Apr-04 TypeofSample : OBWELLS
Referenci~Methodj EPA310 .1/SM2320B Data Posted 5117f2004 16 53 57
_A_~KALINITY (TOTAL INFLECTIONPOINT)_ALKALINITY 5.58 _meq/L
ReferenceMethod EPA310 .1/SM2320B Data Posted 5/20/2004 14 :59:28
ALKALINITY BY CALCULATION ALKALINITY 279.00 Ing/L.
ReferenceMethod :EPA200,71601013 Data Posted : 51712004 13 :21 :1 9
M RON BY ICP (DIGESTED)IRON 0 .397 nn 11_
Referenoelvethod :EPA200 .716010B Data Posted : 51712004 13 :21 :2 0
MANGANESE BY ICP (DIGESTED)...MANGANESE 0 .021 mg/L
ReferenceMethod EPA300 .0 Data Posted : 515/2004 11 :15 :4 1
NITRATE (IC)_NITRATE 9.87 nn-----gLL-
Reference Method EPA 300 .0 Data Posted 5/6/2004 12 :12 :3 2
NITRATE BY CALCULATION (MG-N/L)NITRA TE 2.23 mg-KI
Reference Method EPA 300o Data Posted : 515/2004 11 :15 :4 1
SULFATE QC)SULFATE 62 .42 mg/L
Sample ID 24010621 Desktop III Customer ID L .D . CAMPBELL
Sample Description : PMWM-S
Collection Date : 26-Apr-04 10 :45:00 Date Received in Laboratory : 01-Apr-04 Type of Sample : OB WELLS
ReferenceMelhod EPA310.11SM2320B Data Posted .5/1 7/2004 16 :53 :57
ALKALINITY (TOTAL INFLECTION P0-1-NT)ALKAYNITY 0.37 meq/L
ReferenmMethod :EPA310 .1/SM2320B Data Posted : 5/20/20G4 14 :59:3 1
ALKALINITY BY CALCULATION ALKALINITY 18.50 mg/L
ReferenceMethod :EPA 200 .7/6010B Data Posted W12004 13 :21 :2 0
IRON BY ICP (DIGESTED)IRON 0 .066 mg/I
Reference Method:EPA 200 .7/6010B Data Posted. 5n12004 13 :21 :2 0
MANGANESE BY ICP (DIGESTED)MANGANESE 0.007 nng/L
Reference Method :EPA 300 .0 Data Posted : 5t3/2004 15:43 :30
.NITRATE (IC)NITRATE 8 .65 mg/L
Reference Method EPA 300o Data Posted 516/2004 12:05 :54
0
NITRATE BY CALCULATION (MG-N/L)NITRATE 1 .95 mg-NIL
V11 .1 ,, ~n lh~ ln .,.N~, ~.ir".'rr 512112004 1/ (15 40 1... P
fld,.w%y/csscnv/IaI,-srvI "44
P BUke IAIKe -rower Anaiyucal LaDW-ator y01'Power.Phone [phone] Fox 704-875-5038
A~b-vc~I3339HaqefSFefIY Road Huntersville,NC28078-7929
McGuire Nuclear CompAiix - MG03A 2Cterufl,ii--att-- of ^na1ys-.i!s
New York Slate Department of Health Certification It f f 7 f 7
Oklahoma Department of EmironnIenial Quality Certification It 9930
Kansas Department of Health and Finvironment Certificate P E-103 f f
North Carolina Department of I Aeallh &Human Services Certification # 378N
South Carolina (OHEq Laboratory ID # 99005 North Carohna (DENR Certification If 24 8
Station Name :BURLINGTON Job Number, 04-APR-0001
Sample ID #:24010621 Desktop #Customer ID L .D . CAMPBELL
Sample Description: PMWM-S
Collection Date : 26-Apr-04 10 :45 :00 Date Received in Laboratory : 01-Apr-04 Typeol'Sample : OBWELLS
Reference Method:EPA 300~O Data Posted 5/412OD4 08 45 3 1
SULFATE [IC) ---SULFA TE 17 .96 mg/L
Sample ID #:24010622 Desktop III CustomeriD : L .D .CAMPBELL
Sample Description : PMWL-S
CollectionDate : 28-Apr.0411 :15 :00 Date Received in Laboratory : 01-Apr.04 TypeofSample : OBWELLS
ReferenoeMethod :EPA310 .11SM2320B Data Posted : 5/1712004 16 :53 :57
ALKALINITY (TOTAL INFLECTION POINT ALKALINITY 3 .98 meq/L
Reference Method :EPA310 .11SM23208 Data Posted : 5/20/2004 14 :59 :34
ALKALINITY BY CALCULATION ALKALINITY 1199 .00 mg/L
ReferenoeMethod :EPA200.716010B Data Posted : 517t2004 13 21 :20
IRON BY ICP (DIGESTED)IRON 39.419 mgII
ReferenwMethod :EPA200.7/60108 Data Posted : 5RI20D4 13:21 :2 1
- -MA .NG .ANE .SEBY-IC~_(QIPESTEDL------- __MANGANESE 2.039 mg/L
Reference Method :EPA 300.0 Data Posted : 5/5t2004 11 :16 :0 1
NITRATE .(IC)N/TR47E 0 .17 mg/L
Reference Method :EPA 300.0 Data Posted 5/6t2OO4 12:12 :34
NITRATE BY CALCULATION MG-N/L)NITRATE 0.04 mg-NIL
Reference Method .EPA 300o Data Posted : 51512004 11 16 :0 1
SULFATE (IC)SULFATE 21 .95 mg/L
Sample ID #:24010623 Desktop #Customer ID L .D . CAMPBELL
Sample Description :FIELD BLAN K
Collection Date : 28-Apr-04 16 :15 :00 Date Received in Laboratory : 01-Apr-04 TypeofSample : OBWELLS
ReferenmMethod :EPA310 .11SM232013 Data Posted 5/1712OD4 16 53 :5 7
ALKALINITY (TOTAL INFLECTION POINT)ALKALINITY < 0 .01 meq/L
RelerenoeMethod :EPA3101ISM2320B Data Posted 5120/2004 14 :59 :3 8
ALKALINITY BY CALCULATION ALKALINITY < 0 .50 mg/L
ReferenceMethod EPA200 .716010B Dam Posted .51`712004 13 21 :2 1
IRON BY ICP (DIGESTED)IRON < 0.010 mg/I
VM1 . ... .. .llk~. .....wd 512112V04 11 .05 .40 litip ://dcwiv%v/essetiv/lab-srv/
P
UUKe IJL[Kt r0We1'A11d1yL1Cd1 1~dUUI'dLUFYaPower.Phone [phone] Fax [phone]
A 13339 HagefsFeriy Road HUnteisville,NC28078-7929
McGuire Nuclear Complex - MG03A 2
Ct-_rt1f14-_a1tt-_43f Aftnalysi!%
New York Slate Department of Health Certification #f f 717
OklahorwDepa4~nlofEmironn)entalOuahlyCerliti~alion#9930
Kansas Departinent ofHeagh and Environment Certificate # E4031 1
North Carolina Department of Haallh &Human Services Certification #37W4
South Carolina QHEQ Laboratory 10 # 99005 North Carolina QENF~ Codification #24 8
Station Name :BURLINGTON Job Number : 04-APR-0001
i
Sample ID #:24010623 Desktop #Customer 10 L .D . CAMPBELL
Sample Description :FIELD BLAN K
Collection Date : 28-Apr-04 16 :15 :00 Date Received in Laboratory : 01-Apr-04 TypeofSample : OBWELLS
Reference Method :EPA 200.7/6010B Data Posted : 5(7/2004 13 :21 :2 1
MANGANESE BY ICP (DIGESTED)MANGANESE < 0 .005 mg/L.
ReferenmMethod EPA300.0 Data Posted 5/512OD4 11 16 :2 1
NITRATE (IC).NITRATE < 0 .10 mg/l .
Reference Method EPA 300.0 Data Posted 51612004 12 12 :3 5
NITRATE BY CALCULATION (MG-NIL)NITRATE <0 .02 mg-NIL
Reference Method-EPA 300o Data Posted SWO04 1116 :2 1
SULFATE(IC)__.SULFATE < 0.10 mg/L.
Data VenfiW 8~ Apo~ By,Da~
Vi,il lh~ I . ...:,No ~,l
6~1111,11 1 512112004 11 IIJ 411 1111P
?UuKe 1A[bX 1rUWV,1'A11d1yL1Cd1 1-jaDUFaLlUl ydorPower.Phone .[phone] Fax [phone]
A NAliIi,01G~13339 Hagers Ferly Road Huntersvittle,NC 28078-7929
McGuire Nuclear Complex - MG03A 2
Cortificato cof Analysi s
New York Slate Depadinent of Health Certification # f 17 f 7
Oklahoma Deparifflent of Environrnenlaf Quality Carlificallon # 9930
Kansas Department of Heath and Environment Certificate # E4031 1
North Carolina Depadnient of l'balth &Hurnen Services Codification # 37804
South Carolina (DHEC)Laboratory ID # 99005 North Carolina (Dr*R Certification If 248
7P
SamplelD#: 24010614 Job#: 04-APR-000 1
Sample Description :TRIP BLANK -BURLINGTON OB WEL L
Collection Date : 25-Apr-04 14 :40 :00 Site :BURLINGTON Sample Type: OB WELLS Desktop #
MGP PARAMETERS IN WATER BY GCIMS - 826 0
Test Code : MS8260MGPW Test Method : SW-846 503013/8260B Date Posted : 05107/04
Result _ -R~~,n Limit Flag
Benzene < 0 .50 Vg1L 0.50 PgA. 0
Toluene < 1 .0 pg/L 1 .0 pg/L 0
Ethylbenzene < 1 .0 pg/L 1 .0 P911 .a
m .p .Xylene <2 .0 pg/L 2 .0 ligit .0
o-Xylene < 1 .0 pg/L 1 .0 P91L 0
Naphthalene 2 .0 pg/L 2 .0 ug/L 0
SampjeID#: 24010615 Job#:04-APR-000 1
Sample Description :MW-3
s
ollection Date : 27-Apr .04 15 :50 :00 Site :BURLINGTON Sample Type : OB WELLS Desktop #
ic
MGP PARAMETERS IN WATER BY GC/MS - 826 0
Test Code : MS8260MGPW Test Method : SW-846 5030B18260B Date Posted : 05/07104
-Result .-Reporting Limit Fla g
Benzene < 0.50 pgIL 0 .50 Vg/L 0
Toluene 2 .2 pillt. 1 .0 pg/L 0
Ethylbenzene < 1 .0 pg/L 1 .0 PgIL 0
rn-p-Xylene 2 .0 pg/L 2.0 pgrL 0
o-Xyleme 1 .0 Vg/L 1 .0 Pert, 0
Naphthalene <2 .0 pgfL 2.0 Vg/L 0
SamplelD#: 24010616 Job#: 04-APR-000 1
Sample Description :PMWB-S
Collection Date : 27-Apr-04 14 :30 :00 Site :BURLINGTON Sample Type : OB WELLS Desktop #
MGP PARAMETERS IN WATER BY GCIMS - 826 0
Test Code : MS8260MGPW Test Method : SW.846 5030B18260B Date Posted : 05/07/04
Resuft Reporting Limit Fla g
Benzene 140 pg/L 0.50 pg/L 0
Toluene 98 pg/L 1 .0 pg/L 0
0 Ethylbenzene 250 pgIL 100 pg/L 0
m.p .Xylene 82 pg/L 2 .0 lig/L 0
o-Xylene 79 Pg/L 1 .0 Pg& 0
V,,,t I, ,,,thc horaNci a tI",............ 1 11 I'll Ili hllp ://dc%v%~,,v/es,~cn~/lab-sr~/A, ~ I " I
P uuKe IL)L[Kt JroWel' AlldlyLlUdl 1-jdUU1dLU1Yoftwer.Phone:[phone] Fax 7C4-675-5038
A LWE~ C~13339HagerSFeffY Road Hunteirsvillia,NC28078-7929
mcGuile Nuclear Complex - MG03A 2
C4-artificatle of AllalySiS
New York Slate Department of Health Certification # 11717
OklabomDepailn7entofEr?vironrmnlatQuahlyCeHffcalAon#9930
Kansas Department of Heath and Environment Certificate # E-f03f f
North Carolina Department of Health &Human Services Certification # 378N
South Carolina (0HEQ Laboratory ID # 99005 North Carolina (DENR Certification It 248
SamplelD#: 24010616 Job#: 04-APR-000 1
Sample Description :PMWB-S
Collection Date : 27-Apr.04 14 :30 :00 Site BURLINGTON Sample Type : OB WELLS Desktop If
OGP PARAMETERS IN WATER BY GC/MS - 826 0
Test Code : MS8260MGPW Test Method : SW-846 5030B/826013 Date Posted : 05107104
--Res-uft -Rep~rlinq Limit Fla g
Naphthalene 2700 pgfL 200 pgtL 0
Sample]D#: 24010617 Job#: 04-APR-000 1
Sample Description :PA S
Collection Date : 28-Apr-04 11 :35:00 Site :BURLINGTON Sample Type : OB WELLS Desktop At
MGP PARAMETERS IN WATER BY GC/MS .826 0
Test Code: MS8260MGPW Test Method : SW-846 5030B/826013 Date Posted : 05107104
Result ReportingLinut Flag
Benzene 30 Vg1l. 0.50 pg/L.0
Toluene 8 .8 lig/L 1 .0 pg/L 0
Ethylbenzene 110 pg/L 1.0 pgJL 0
m.p .Xylene 33 pg/L 2.0 pg/L 0
o.Xylene 76 pgdL 1 .0 pg/L 0
Naphthalene 820 pgfL 200 pgfL 0
SamplelD# 24010618 Job#: 04-APR-000 1
Sample Description :PMWC-S
Collection Date : 26-Apr .0411 :05 :00 Site :BURLINGTON Sample Type : OB WELLS Desktop #
OGP PARAMETERS IN WATER BY 6CIMS - 8260
Test Code: MS8260MGPW Test Method : SW-846 S030B18260B Date Posted : 05107104
Result Reporting Limit Flag
Benzene 4 .8 VglL 050 pg/L 0
Toluene < 1 .0 lig/L 1 0 lign-0
Ethylbenzene 2 .6 pgtL 1 .0 Pg/L 0
m .p.Xylene 2 .5 Pg1l .2 .0 pg/L 0
o.Xylene 5 .7 pgtL 1 0 pg/L 0
Naphthalene 120 pg(L 10 pg/L 0
th,, fiu,aNo ~1
i"'.";.... ..... ~.... .hup //dc .ww/esscnv/Iab_sr,/
p,,vuke vuKe Fower Anaiyuical LaDOratoryPower.Phone [phone] Fax:[phone]
13339 Hagers Ferry Road HuntersvilAq,NC 28078-7929
McGuire Nuclear Complex - MG03A 2
C4--rtificatt-- of Analysis
New York Slate Department ofHealth Certification #II?f7
OklahornaDepadmntofErAtironrmnialQuahtyC--ridicalion#9930
Kansas Department of Heath end Environment Certificate #E-fO3t f
North Cgrolina Department of Health &Hurnen Services Certification # 378N
South Carolina (D!-~Laboratory ID It 99005 North Cgrolina (DENF~ Certification #248
SampIeID#: 24010619 Job#: 04-APR-000 1
Sample Description :MW-5
Collection Date : 27-Apr-04 13 :30:00 Site :BURLINGTON Sample Type : OB WELLS Desktop #
I GIR PARAMETERS IN WATER BY GCIMS - 826 0M
Test Code MS8260MGPW Test Method : SW-846 5030B18260B Date Posted : 05107/04
Result Reponin6LUmit Flag
Benzene < 0 .60 Pg/L 0 .50 pg/L 0
Toluene 2 .7 pg/L 1 .0 vg/L 0
Ethylbenzene 1 .0 Pg1L 1 .0 pgtL 0
m .p .Xylene <2 .0 WgIL 2 .0 pgr- 0
o .Xylene 1 .0 PgAL 1 .0 VgAL 0
Naphthalene <2 .0 pgr-2 .0 pg/L 0
SamplelD#: 24010620 Job#: 04-APR-000 1
Sample Description :MW-9
ollection Date: 28-Apr .04 09 :65:00 Site :BURLINGTON Sample Type : OB WELLS Desktop At
OGP PARAMETERS IN WATER BY GC/MS - 8260
Test Code : MS8260MGPW Test Method : SW-846 5030B18260B Date Posted : 05/07104
-Misuvlt RegoIM2 Limit Flag
Benzene < 0 .50 Pg/L 0 .50 Vg/L 0
Toluene 1 .0 ligil, 1 .0 pen. 0
Ethylbenzene 1 .0 PqlL 1 .0 pg/L 0
m-p-Xylene <2 .0 Pg/L 2.0 pg/L 0
o .Xylene < 1 .0 PglL 1 .0 pg/L 0
Naphthalene <2 .0 Pg/L 2.0 pgh,0
Ron Eg~~-
SamplelD#: 24010621 Job#: 04-APR-000 1
Sample Description :PMWM-S
Collection Date : 26-Apr-04 10 :45 :00 Site :BURLINGTON Sample Type : OB WELLS Desktop At
MGP PARAMETERS IN WATER BY GCIMS - 826 0
Test Code : MS8260MGPW Test Method : SW-846 503OB18260B Date Posted : 05/07104
Re5ult Reporting Limit Flag
Benzene < 0 .50 Vg/L 050 pg/L 0
Toluene 2 .0 pgfL 1 .0 pgr- 0
Ethyllbenzene . 1 .0 PgIL 10 pg/L 0
m .p .Xylene -2.0 pglL 2 .0 pglL 0
0 o-Xylene 1 .0 Pg/L 1 .0 pgA . 0
V,s,l u,.,,11"~ 1,*~NO M312112111111"1 "1 Imp //dCWw,V/.env/lah ,rv/
P,&,Uuke VUKe Fower Anaiylical LaDomor yPower.Phone [phone] Fox 704-675-5038
A ~E-,r G~13339 Hagers Ferry Poad Huntelsville,NC 26078-7929
McGuire Nuclear CompAax - MG03A 2
Cortificato cof Alxnaiysis.
New York State Department of Health Gerifficetion # I f717
Oklahorm Department of Environmental Quality Certification 9 9930
Kansas Department of Heath and Environment Certificate # & 1031 f
North Carolina Department of Health &Human Services Certification # 378N
South Carolina (DhEQ Laboratory ID #99005 North Carolina (DBVR Cedification #246
Sample ID#:24010621 Job#:04-APR-000 1
Sample Description :PMWM-S
Collection Date: 26-Apr-04 10 :45 :00 Site :BURLINGTON Sample Type : OB WELLS Desktop #
Liv G-P-PA--R-A -ME- TE-RS--IN-WA TE R B Y G C /M S - 8 2 60
Test Code : MS8260MGPW Test Method : SW-846 50308/8260B Date Posted : 05107/04
-Result
-
Reiooffinq Limit Flag
Naphthalene <2 .0 V911- 2 .0 vg/L
Sample ID #:24010622 Job#: 04-APR-000 1
Sample Description :PMWL-S
Collection Date : 28-Apr-04 11 :16:00 Site :BURLINGTON Sample Type :08 WELLS Desktop #
MGP PARAMETERS IN WATER BY GCIMS .826 0
Test Code : MS8260MGPW Test Method : SW-846 503OB18260B Date Posted : 05/07104
Resuft Reporting Lima Flag
Benzene < 0.60 pg/L 0.50 Pgr, 0
Toluene < 1 0 pg/L 1 .0 Pg/L 0
Ethylbenzene < 1 .0 PgIL 1 .0 Pg/L 0
m.p.Xylene <2.0 Pg/l. 2 .0 ugll. 0
o-Xylene < 1 .0 Pg/L 1 .0 vgIL 0
Naphthalene <2.0 Vg/L 2 .0 pg/L a
Sample ID #:24010623 Job#: 04-APR-000 1
Sample Description :FIELD BLAN K
CollectionDate 28-Apr-0416 :16 :00 Site :BURLINGTON Sample Type : OB WELLS Desktop #
OGP PARAMETERS IN WATER BY GC/IMS - 8260 --
Test Code : MS8260MGPW Test Method : SW-846 503013/826013 Date Posted : 05/07104
Result Reporting Limit Flag
Benzene < 050 Pg/L 0 .50 pg1L 0
Toluene 1 .0 Pg/L 10 P911.0
Ethylbenzene 1 .0 Vg/L 1 .0 PgrL 0
m.p.Xylene <2 .0 VgiL 2.0 Pg/L 0
o.Xylene < 1 .0 pg/L 10 OgIL 0
0
V .0 lik 1"I'.No .1d Y21 .. ..... 11 .....hill, //deww~/cs%cnv/1ah-srv/P.,1 4,11
p,k guke uuKe FowerAnaiytical LaDoratoryPower.Phone [phone] Fox.704-875,5038
13339 Hagers Ferry Road Huntefsvilila,NC 26076-7929
McGuire Nuclear ComPbx - MG03,1 2
Cortificat4e Of Analysi s
Now York State Department of Health Certification # f f7f7
Oklahoma Department of Environmental Quality Certification # 9930
Kansas Department of Heath and Environment Certificate # E-f031 I
North Carolina Department of Health &Human Services Certification #3780 4
South Carolina (DHEQ Laboratory ID # 99005 North Carolina (DEAIF~Certification #248
SamplelD#: 24010623 Job#: 04-APR-000 1
Sample Description :FIELDBLAN K
Collection Date : 28-Apr-04 16 :15:00 Site :BURLINGTON Sample Type : OB WELLS Desktop #
MGP PARAMETERS IN WATER BY GCIMS - 8260
Test Code : MS8260MGPW Test Method : SW-846 5030B/8260B Date Posted : 05107/04
Result . Reporting Limit Flag
Naphthalene <2.0 pgtL 20 pgA, 0
------------------------------------Di4ascri-ptic)-n c)f Flactrs :
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2 C . .... er .... ..Se, Co.
3 . 1-1-, due .-,I .
4 Rel..U-t El .o .,ed 4- so -,u .,.d anal~..a l
5 S-,I .R-4 . Should No,Be U,.d Fo, P,.-
(So . C ...Narr .t-)
6 Ana] tile dat,ct,d below labotatot, reporting limit at ao emmaxe d
7 -Re,.rt .d ...... b.,.. I . the -biziaso .. of -ir .hal,I-o taroel .,
falte,al,t,,i By. Date
Visil 'is oil the ltliraNci it
..... . .. ... . 11 .1 liltp ://de~.,~/csscliv/lab-srv/
CHAIN OF CUSTODY READ AND ANALYSIS REQUEST FOR Mr-------------------------------------------------------------------Duke PowerAnalytical Laboratory Services i i Analytical Laboratory Use Only
1 9Duke-- -- -------------i !LIMS*-TS---P1-cl---Sa .pl 5 Page atMail Code MG03A2 (Building 7405)-1-
13339 Hagers Ferry Rd !011-yqP1q-OOOZ OfiglZing Nc ztw4wEnergy.I From sc-DISTRLTIO N
Huntersville,N.C . 28078 ORIGINAL to LAB,For Detailed Instructions, see :!Logged By Date &Time SAMPLE PROGRA
hItp :/1de~1essenv/coc1 Fa [phone] Ground Water COPY to CLIENT
.L79L4-----------X:............ .NPDES
iVendor Drinking Waterj<2)Phone No:875-5257 2.toRLINGTONMGP(SAPR h *7 LIST
O~~S)Cooler Temp (C RCRA Waste
~E 3)Ciient C.Campbell /R . Roberts /T. Hunsucker 4)Fax No :875-5032 :P0 I Prtserv.:11~C
2=H~SO, 3=Hq
4=1ke S-No aS)BuslnessUnit :20018 6)Process : 7)Resp. To :0193 IMR x
E
02.18)P10ject to:MGPSURL 9)Activity ID : ALLACTV 10)Mail Cod .:MG03A3 C 0Customer to complete all (D
-SHADED areas .te cc <
12 14CO Ci <LABUSEONLY Chem llection Information TE--01 u`CM x<n ,13 0 w :E"Lab to Desktop No . Sample Description or ID Date Time Signature z 2 w t o
2Y-
PMWB-D 1,ti5-X 1 1 3 5
PIVIVVC-D.0 0 J/ x 1 1 3 5
x 1 1 3PIVIWF-D ti lmdc)-(075()5
PMWG-D 122~0~1 jok5 x 1 1 3 5
PIVIw1 x 1 1 3 5
PMWL-D al~ Its x 1 1 3 '631 5
E
0
.... ... ..........
21)RalinquisheciS Dat m e627 eq) 'cc Dalwpme
oo : ,-11;2,~10 5//6 00 uRequested Turnaround
all,julshad e ;'!2 -1 C 10,9 ,0 t ime me7a Accepted By:terri S 14 Day s,!~V -71Y-0 ~z J,,,oe-~~0 M 0
D tam /bateprime
2I-,E
0y3,q - -Z 0
a *7 Days
23)SeaVL"ked By watamme -40ML 7-5~~-healedfLOCk Opened By IDeterTima t:-48 Hr
1 ..,~ommems 1PLEASE HARD COPY AND q~~Oqlck~Y Tli~l~
L) 'Othe r
* Add .Cost Wil(Apply
PhDuke Duke Power Analytical Laborator y
OrPower.Phone :[phone] Fax.[phone]
13339 HagetsFefly Road Huntereville,NC28076-7929
McGuire NucAearCompAqx-MG03,4 2
C 4-- rt III c--a t4e cor ALn a iysis
Now York Slate Department of Health Certification #f f 7 f 7
OklahoimDgpedrmnlofErwironrrentalOuak Carlificalion#9930
Kansas Department of Heath and EhVironfrenMallfficale #E-fO3f f
North Carolina Department of Health &Human Services Certification It 37W4
South Carolina (Dt-Eq Laboratory 10 #99005 North Carolina IDENR Certification #248
Station Name :BURLINGTON Job Number : 04-APR-0002
-------------
Sample ID #:24010624 Desktop #Customer ID:L .D. CAMPBELL
Sample Description : PMWB-D
Collection Date : 28-Apr-04 14 :16 :00 Date Received in Laboratory : 011-Apr-04 TypeofSample : SAPRWELLS
--------------
ReferenoeMethod :EPA310 .1/SM23208 Data Posted : 5/17r2OO4 16:53:57
ALKALINITY (TOTAL INFLECTION POINT)ALKALINITY 3 .51 meg/L
RelerenceMethod :EPA310.1/SM2320B Data Posted : 5/2012004 14 :59:4 1
ALKALINITY BY CALCULATION ALKALINITY 176 .00 mg1L
Reference Method :EPA 200 .716010B Data Posted :5/7f2OO4 13 :21 :22
IRON BY ICP (DIGESTED)IRON 18 .250 mgn
Reference Method :EPA 200 .7160108 Data Posted : 517/2004 13 :21 :22
MANGANESE BY ICP (DIGESTED)MANGANESE 3 .670 mg1L
Reference Method :EPA 300.0 Data Posted : 51512004 11:24 :36
NITRATE (IC)NITRATE 0.17 mglL.
Refereme Method:EPA 300.0 Data Posted : 51612004 12 :12 :36
NITRATE BY CALCULATION (MG-NIL)NITRATE 0 .04 mg-WL
Reference Method:EPA 300.0 Data Posted : 515r2004 11 :24 :36
SULFATE OC)SULFATE 0.23 mgfL
Sample ID V 24010626 Desktop #Customer ID :L .D.CAMPBELL
Sample Description: PMWC-D
CollectionDate : 26-Apr-04113 :00 :00 Date Reoeived in Laboratory: 01-Apr-04 TypeofSample : SAPRWELLS
ReferenceMethod :EPA310 .1/SM2320B Data Posted: 5/17/2004 16:53 :57
ALKALINITY (TOTAL INFLECTION POINT)ALKALINfrY 6.04 megIL
Fteferencelyletl~od EPA310,11SM2320B Data Posted: 5/20/2004 14 :59 :44
ALKALINITY BY CALCULATION ALKALINITY 252 .00 mg/L
Reference Method :EPA 200 .716010B Data Posted:W7/2004 13:21 :22
IRON BY ICP (DIGESTEDL_IRON 8 .520 mg/I
ReferenceMethod:EPA 200 .7/6010B Data Posted 5r7r2OD4 13:21 :2 3
MANGANESE BY ICP (DIGESTED)MANGANESE 8.478 mgtL
Reference Method:EPA 300.0 Data Posted: 513/2004 15:44 :4 1
NITRATE (!g__NITRATE 0.31 m L
Reference Method EPA 300.0 Data Posted : 516/200,4 12:05 :5 5
NITRATE BY CALCULATIONJIVIG-NI'l .) -NITRATE 0 .07 m All-g-
Vj~jt 11%on ohe IrnmNei at
PkDuke Duke Power Analytical Laborator y
,oPower.Phone :70$-875-5245 Fax :[phone]
13339HagersFerly Road Huntersville,NC26078-7929
McGuire NuclearComplax - MG03A 2
C 4-- rtif 1 4-- a te~ all Ammaiyr~i--%
New York Slate Department of Health Certification #f f 7f7
Oklahoma Department of Environmental Quably Certification N 9930
Kansas Depanniant of Heagh and Environment Certificate # E-f03 f I
North Carolina Department of Heath &Human Services Certification # 37801
South Carolina (DI-EQ Laboratory ID #99005 North Carolina (D8VR Ceilsfication #246
Station Name :BURLINGTON Job Number: 04-APR-0002
Sample ID 24010626 Desktop 0 Customer ID:L .0- CAMPBELL
Sample Description : PMWC-D
Collection Date : 26-Apr-04 13 :00 :00 Date Received in Laboratory : 01-Apr-04 TypeofSample : SAPRWELLS
Refeninoe Method :EPA 300 .0 Data Posted : 5/312OD4 1 5 :"A l
SULFATE (IC)SULFATE 0 .25 m /L
Sample ID #:24010627 Desktop Customer ID:L .D. CAMPBELL
Sample Description : PMWF-D
Collection Date : 28-Apr-04 07 :60:00 Date Received in Laboratory: 01-Apr-04 TypeofSample : SAPRWELLS
ReferenoeMethod:EPA310 .11SM2320B Data Posted : 5117/2004 16 :53 :57
ALKALINITY (TOTAL INFLECTION POINT)ALKALINITY 9 .54 meqLL
ReferenoeMethod:EPA310 .11SM2320B Data Posted: 5r2MDD4 14 ;59 :48
ALKALINITY BY CALCULATION ALKALINITY 477 .00 mgfL.
Referencelylethod:EPA200 .7/6010B Data Posted:5f7/2DO4 13 :21 :23
IRON BY ICP (DIGESTED)IRON 11 .335 mg/I
ReferenoeMethod :EPA 200 .7160108 Data Posted:51712004 13 :21 :23
MANGANESE BY ICP (DIGESTED)MANGANESE 4 .523 mg/L.
Reference Method : EPA 300 .0 Data Posted: 5/5/2OD4 11 :24 :59
NITRATE (IC)NnRATE 0 .17 mg/L
Reference Method :EPA 300 .0 Data Posted: 5/21/2004 13 :38 :55
NITRATE BY CALCULATION (MG-NIL)NITRATE 0 .04 mg-NIL
Refere~Method :EPA 300 .0 Data Posted: SIM004 11 :24 :59
SULFATE 11C)SULFATE 0.73 mg/L.
Sample 10 24010628 Desktop #Customer ID:L.D . CAMPBELL
Sample Description : PMWG-D
Collection Date : 29-Apr-04 10 :15 :00 Date Received in Laboratory : 01-Apr-04 TypeofSample : SAPRWELLS
ReferenmMethod: EPA31O.i/SM2320B Data Posted : 5117/2004 16 :53 :57
-ALKALINITY (TOTAL INFLECTION ?Q"NT _ALKALINITY 4 .07 nneqt~_
ReferenceMethod: EPA31O.i/SM2320B Data Posted : 512CM20D4 14 :59 :5 1
ALKALIN[W BY CALCULATION -ALKALINITY 204 .00 mgIL
Reference Method:EPA 2DO,7/6010B Data Posted :5r7/2DD4 13 :21 :24
1RQN BY ICJP (DIGESTED)IRON .0 .526 mgIl_
Vj~jt, th~ I .I .Ne .1
PhDuke Duke Power Analytical Laborator y
drPower.Phone :70$-875-5245 Fax.704-875,%38
13339HegersForly Road Hunteisvil,19,NC26078-7929
McGuire Nuclear Complex - MG03A 2
Coertill'14--.%te~ cof ALnaiyEi--~
Now York Slate Department of Health Certification If f f717
OklehormDepartrnentafEnvironrwnlaiQuaA Carldication#9930
Kansas Department of Heath and EnvitunmenNCerldricale # E-YO3f f
North Carolina Deportment of Health &Human Services Certification # 378 N
South Carolina (DHEC)Laboratory ID # 99005 North Carolina QENF~Certification #248
Station Name:BURLINGTON Job Number: 04-APR-0002_
Sample ID #:24010628 Desktop #Customer ID:L.D . CAMPBELL
Sample Description : PMWG-D
CollectionDate : 29-Apr-0410:15 :DO Date Received in Laboratory : 01-Apr.04 TypeofSample : SAPRWELLS
F--
Refere~Method: EPA 200 .71601011 Data Posted : 5f7r2DD4 13 :21 :2 4
MANGANESE BY ICP (DIGESTED)MANGANESE 2 .687 mgfL
Reference Method :EPA 300 .0 Data Posted : 5/5r-W4 11 :31 :07
NITRATE (IC)NITRATE 3.44 mglL.
Referehoe Method :EPA 300 .0 Data Posted : 511=004 10 :26 :1 5
NITRATE BY CALCULATION (MG-NIL)NITRATE 0.78 mg-NIL
Reference Method :EPA 300 .0 Data Posted: 5/512004 11 :31 :07
SULFATE (C)SULFATE 20.06 mgfl.
Sample 11) Of 24010629 Desktop #Customer ID:L .D . CAMPBELL
Sample Description : PMW I
CollectionDate : 27-Apr-0408 :10:00 Date Reoeivedin Laboratory: 01-Apr.04 Type of Sample : SAPR WELLS
ReferenoitMethod :EPA310.11SM2320B Data Posted: 511712004 16 :53 :57
ALKALINITY (TOTAL INFLECTION POINT)ALKAUNITY 3.01 meg/L
ReferertceMethod :EPA310.11SM2320B Data Posted: 5r2Qf2OO4 14 :59 :54
ALKALINITY BY CALCULATION ALKALIN17Y 151 .00 mg/L
ReferenoeMethod:EPA 200.7/6010B Data Posted:5f7r2OG4 13 :21 :24
IRON BY ICP (DIGESTED)IRON 3 .349 mgA
RefererceMethod:EPA200.7ffiOIOB Data Posted:UM2004 13 :21 :24
MANGANESE BY ICP (DIGESTED)MANGANESE 0 .745 mg/L
Refererce Method:EPA 300o DataPmted:5r3200411 :59 :1 8
NITRATE QC)__NITRATE 0 .27 mg1L
Retere~ Method:EPA 300~O Data Posted: 514r2OG4 08 :40 :08
NITRATE BY CALCULATION (AMGLN/LL_NITRATE mg-NIL
Reference Method :EPA 300 .0 Data Posted: 5r3l"04 11 :59 : 1 8
SULFATE (IC)SULFATE 8 .63 mg/L.
Vi,i, In .,Ne
pkvuke Duke Power Analytical Laboratory
Oftwer.Phone:70$-875-5245 Fax:704-875-W36
A Dv~ &I C~13339HOgersFerly Road HuntersvilAq,NC28078-7929
McGuire Nudear Complex - MG03A 2
Ct--rt1114--at4e cor ALnaiysi s
Now York Slate DEparlment of Health Certification #f f 7 f 7
OklahornaDoperfrmntofEnvironrnentalOuafi Cerlticabon#9930
Kansas DoWmani of Heath and EnvironmenMerlificale # E403f f
North Carolina Department of I balth &Human Services Certification # 378N
South Carolina (DHEQ Laboratory ID # 99005 North 0grohna (DENF~Certification Of 248
Station Name :BURLINGTON Job Number : 04-APR-0002
Sample to #:24010631 Desktop #Customer ID:L .D . CAMPBELL
Sample Description : PMWL-D
Collection Date : 28-Apr-04 09 :15 :00 Date Received in Laboratory : 01-Apr-04 TypeofSample : SAPRWELLS
RefererceMetnod:EPA310.11SM23208 Data Posted : 5/17/2004 16 :53 :57
-ALKALINITY (TOTAL INFLECTION POINT)ALKALINITY 2.65 meqfL
RefererceMethod :EPA310.1/SM23208 Data Posted : SnO/2004 14 :59 :58
ALKALINITY BY CALCULATION ALKALINITY 133 .00 mg/L
Refereme Mellmd :EPA 200 .7/601 OB Data Posted :W/2004 13:21 :2 5
IRON BY ICP (DIGESTED)IRON 0.161 mg/I
Refemricelyletrod :EPA 2DO .7/6010B Data Posted :V712004 13:21 :2 5
MANGANESE BY ICP (DIGESTED)MANG41VESE 0.210 mg1L
Refereme Meftxxi:EPA 300.0 Data Posted : 5/512004 11 :33:20
NITRATE (IC)NITR4TE < 0 .10 mull .
Refereme lvled~od:EPA 300.0 Data Posted: 5WOD4 12 :12:38
NITRATE BY CALCULATION (MG-NIL)1VrTRATE <0 .02 mg4tfl-
ltefere~ MeVxxl :EPA 300.0 Data Posted: 515/2004 11 :33:20
SULFAIEJIC)SULFA TE 26 .67 mgfL.
Data ve Aopro"d By. D"
~4D~
0
Vmt th~1~.~Nv .1
phpuke Duke Power Analytical Laborator y
OPower.Phone:[phone] Fax :[phone]
1333gHagetsFerty Road Huntensvil,19,1011C28078-7929
MCGUile Nuclear Complex - MG03A 2
Ciiertiflc:ate of Ainalysis
New York Slate DeparfintentofHatith Certification It if717
OklehorwDapadrrentofErwironrwnlalQuahtyCarttication#9930
Kansas Department of Heath and Environment Cedficala #E-f03l f
North Carolina Depailtrient of Health &Human Services Certification # 378 N
South Carolina (DHEQ Laboratory ID # 99005 North Carolina (DENI~Certification #248
SamplelDN : 24010624 Job#: 04-APR-0002
Sample Description : PMWB-D
Collection Date: 28-Apr-04 14 :16 :00 Site :BURLINGTON Sample Type: SAPR WELLS Desktop #
Test Code : MS8260MGPW Test Method : SW-846 5030B18260B Date Posted : 05107104
Result Reporting Limit Flag
Benzene so V91L 13 vg'L 0
Toluene < 25 Vg&26 pgtL 0
Ethylbenzene <25 P91L 25 119/1-a
m-p-Xylens < so Pg/L so P9/L 0
o-Xylene <25 P91L 25 pgtL 0
Naphthalene 720 pgrL so lign. 0
SamplelD#: 24010626 Job#: 04-APR-000 2
Sample Description :PMWC-D
ilection Date : 26-Apr-0413 :00 :00 Site :BURLINGTON Sample Type : SAPR WELLS Desktop
Glo PARAMETERS IN WATER BY
Test Code : MS8260MGPW Test Method : SW-846 6030BIB260B Date Posted : 05107104
Rewit Reporting Limit Flag
Benzene < 13 ljgrL 13 Wt.0
Toluene <26 VgIL 25 pqrL 0
Ethylbenzene 54 pgVL 26 WL 0
m-p-Xylene < so WL 60 Pg/L 0
o-Xylene <25 pA 26 pgtL 0
Naphthalene 1800 119/1-50 Pg/L 0
SamplelD#: 24010627 Job #:04-APR-000 2
Sample Description :PMWF-D
Collection Date : 28-Apr-04 07 :50 :00 Site :BURLINGTON Sample Type : SAPR WELLS Desktop #
MGF` PARAMETERS IN WATER BY GCIMS - 826 0
Test Code : MS8260MGPW Test Method : SW-846 5030B/8260B Date Posted : 05107/04
Result _Reindmit Limit Fla9-
Benzene < 13 pg/L 13 pgr- 0
Toluene <25 pg/L 25 WL 0
Ethylbenzene 27 pgrL 25 P9A-0
m-p-Xylene 50 PgAL 50 P911-0
o .Xylene 26 pg/L 25 pg/L 0
Visit us on 1hc IntraNcl a,
p,guke Duke Power Analytical Laboratory
Power.Phone:[phone] Fax :[phone]
13339 HegersFefly Road Huntersvills,NC28078-7929
McGuue Nuclear Complex - MG03A 2
Certific-,at4e li Analysis
New York Slate Department of Health Certification #I f717
Oklahoma D9pailmentofEnvironmentalQuak carlificallon#9930
Kansas Department of Health and EnvironmeNtifficate # E-f03 H
North rArolina Department of lbalth &Human Services Certification #37W4
South Carolva (DhEp Laboratory ID # 99005 North Carolina (DENFO Certification #248
SampIeID#: 24010627 Job#: 04-APR-000 2
Sample Desc4iption : PMWF-D
Collection Date : 28-Apr-04 07 :50:00 Site :BURLINGTON Sample Type : SAPR WELLS Desktop #
GIP PARAMETERS IN WATER BY GCIMS - 826 0
Test Code : MS8260MGPW Test Method : SW-846 5030B/826013 Date Posted : 05/07104
Result Relx~ding Limit Flag
Naphthalene 1200 pgtL so Pg/L a
SamplelD#: 24010628 Job#: 04-APIR-000 2
Sample Description :PMWG-D
Collection Date : 29-Apr-04 10 :15:00 Site :BURLINGTON Sample Type: SAPR WELLS Desktop #
MGIP PARAMETERS IN WATER IMS - 8260
is Test Code : MS8260MGPW Test Method : SW-846 503013/8260B Date Posted : 05107104
Result Reponing Limit Flag
Benzene 0 .63 pgiL 0.50 PA 0
Toluene < 1 .0 pg/l.1 .0 IQA. a
Ethyllienzerie 11 .4 MR .1 .0 IQ& 0
m-p-Xylene <2.0 Plitt.2.0 IV& 0
o-Xylene 2.2 pg/L 1 .0 PWL 0
Naphthalene 9.2 pg/L 2.0 PWL 0
Sampliti 24010629 Job#:04-APR-000 2
Sample Description:PMWI
Collection Date: 27-Apr-04 08 :10 :00 Site :BURLINGTON Sample Type : SAPR WELLS Desktop #
MGP PARAMETERS IN WATER BY GCIMS - 8260
Test Code : MS8260MGPW Test Method: SW446 5030818260B Date Posted : 05107/04
Resuit 9 Limit Ra L
Benzene < 0 .60 p9A . 0 .50 Pg/l, 0
Toluene < 1 .0 Pg/L 1 .0 pg/L 0
Ethylbenzene <11 .0 pg/L io PA 0
m-p-Xylene <2 .0 pg/L 2 .0 Vg/L 0
o .Xylene < 1 .0 PgA- 1 .0 PgIL 0
Naphthalene 4 .9 pg/L 2 .0 VA 0
visit os on iiii, Int .1,1v t
PkDuke Duke Power Analytical Laborator yOPower.Phone:7G4-875-5245 Fox.704-875-5038
A Dti, Eet, (seoo 13339HagersFerly Road Huntelsville,NC28078-7929
McGuire Nuclear ComoA3x - MG03A2
c4ertificatili-m of A%nalysi s
New York State Department ofHGagh Certification If If7f7
Oklahorm Deparfrilant of Envirunrnentel Quality Codification # 9930
Kansas Deparbnent ofHeagh and Environment Certificate #E-fO3f f
North Carolina Deparrnont of ftalth &Hurnan Services Codification # 378N
South Carolina (DfC-Q Laboratory ID # 9005 North Carolina (DENF~Certification #248
SamplelD#: 24010631 Job #:04-APR-000 2
Sample Description : PMWL-D
Collection Date : 28-Apr-04 09 :16:00 Site :BURLINGTON Sample Type: SAPR WELLS Desktop #
Test Code : MS8260MGPW Test Method : SW-846 503OB/8260B Date Posted : 05107104
Restift Reppaigg Lend Flag
Benzene < 0 .50 pg/L 0.50 pg/L a
Toluene 1 .3 pqn. 1 .0 pgfL a
Ethylbenzene < 1 .0 ygA. 1 .0 Pg/L a
rn-p-Xylene <2 .0 W&2 .0 V9/L a
o-Xylene < 1 .0 1.19/1 .1 .0 Pg/L 0
Naphthalene <2 .0 PgVL 2 .0 1.19/1-0
------------------------------------
Descriptic>n Of Flacrs :
0 -All Ans!"cal P-cesixes, Requirements Were Met
I - So. C .m Nes-ne.
2 -E.ureated Concemensisess .~Cow Ashensmst
3 -Rc,n. ]L&m,.0 .e .d cits...s .-M-cel .-,1 .--.1
A -Rennes, ~mst Elcesned eftse to reemmmet se-l"cal efilubon
5 . S-,].Remit .sbonsid ~-,Be U .ml For R .,.l .w,3P,s1p ..c.
(S .. C ...
6 Analtrec detected below labomme,r repornina limit at see cmimmed
cters .-teesion ,
7 -R on n c d concente son i r use c ombs nam on of mom that one wocl cer
n .d A-ms 1 1 . 1 ....-w .1 Is 1h ..can ...r l...n m."'s
0.4.4~,W.d By.Date
0
Vkil the 1nh-.Nc,.1
CHAIN OF CUSTODY REAORD AND ANALYSIS REQUEST FOR M--------------- --------------------------------------------------------------------
& o;er al ;tical Laboratory Se"Icesi i Analytical Laboratory Use Onl y';eDukeI
Mail Code MG03A2 (Building 7405) i ILIMS a Sample Class Samples NC-Z "Page -L 01
13339 Hagers Ferry Rd i i,01/- )9,PR-00,04 P Originallng SC DISTRIBUTIO N?DwEnergya-i i I -From ORIGINAL to LAB ,
For Detailed Instructions, see : Huntersville,N . C . 28078 ~~~e &Time SAMPLE PROGRAM COPY to CLIENT(704)875-524 5httpJ/de~/essenvIcoGI Fax :cfde-1 2 .-//Ground Water
-----------------C7U4 .............i I NPDES
I)Project Name 2)Phone No :875~5257 iVendor 2 .4 b 7 Drinling Water
BURLINGTON MGP ISHAL FRACTBR WELLS)UST -
Cooler Ternp (C RCRA Waste
E 3)Client C .Campbell I R . Roberts I T . Hunsucker 4)Fax No :875-5032 :PO#'Pr serv .:1=C
2-0. 3=H
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StSusiness Unit :20018 6)Process : 7)Resp.To:0193 IMR #
0 0C1B)Project to:MGPBURL 9)Activlty to : ALLACTV 10)Mail Code .MG03A3 M - 'a w U
Customer to comnlete all 1-1- E,z Eanorcior ate NON-~-cc
0 w
LAB USE ONLY 12 14CO,lection Inf CL M NChemormationE0clir- <13 0 0 w"Lab to uesKlOp NO .Sample Description or ID ate Time Signature t:V z 2 to 01 01
Omw-1 X 1 1 1 3 5EIA4
DMW-2 x 1 1 3 5
1 44 PMWC-BR q 1;(- D'I /SOS ir X 1 1 3 (75 5
~5!E PMWH-BR k 1 1 3 5=-i =~x0PMWI-BR 144 1 1 3 5
PMWM-BR X 1 1 3 5
PMWL-BR 7z
10.
Customer to sign &date belo w
21)Rellnquished oat 0 Accepted By:951afTlip e
By e11;&00 Requested TurnaroundAW,ell?(0 /0 y 7/t arm -Relinquished 8 C/4ej Daterr rn
A6r ~a -
;'A DatafrIme w C
14 Days -kpy?/ -0
W ,,(,/A q/.2 7/0 7F ?aw P v vjv,5 '0Relinquished BY a, Acce Ezzs *7 Days
23)SeaVLocked By Delarnme Sealedn-ock Opened By E om vo
0 0 .2 -48 Hr
- PLEASE HARD COPY AND ELECTRONICALLY TRANSER THE ANALY11CAL RESULTS L)'Other
*Add .Cost Will Apply I
0 CHAIN OF CUSTODY REVAD AND ANALYSIS REQUEST FORM 0
Pk Duke I &;e-~-o;;e r-Zin al ;t ic-a'-1 L'-a'b-o* r-a*t-o*ry*-S*e-Wlc as* i r ----------- - ------------------------------------------------:a ! I ~~al tical Laboratory Use nly
"'Page OtMailCad 3A2 (Building 7405 )Energy.3363M9CHOgers Ferry Rd DISTRIBUTION
ORIGINAL to LAB,For D(Huntereville,N . C . 28078 !Logged By Date &Time SAMPLE PROGRA Mhttp:[phone] Ground Water -,t- COPY to CLIENT
-.x:............. i I-------------Fa (79L4)2L!~qq:L NPDESI)ProjectNams 2)Phone No:875-5257 !Vendor DrInIdn WaterI/,;7 11C,9BURLINGTON MGP(SHAL FRACTEIR WELLS)LIST
Cooler Temo (C)RCRAWasteT)Fa . No 875 5-032 :PO #E 3)Cll,,, C .Campbell I R . Roberts /T Hunsucker Pr serv .:11=C2 2=H 0. 3=H
4=1111S)BusinessUnIt : 20018 6)Process : 7)Resp .To:0193 [MR 0E0 C$)Project to :MGPBURL E L)9)Actlvlty to : ALLACTV 10)Mall Code:MG03A3 AdCuStomer to comolete all
approorlateNoN-s-g-
14CO ILABUSEONLY12 Chem lectlon Information r 0 x130"Lab to ueSKTOP NO .Sample Description or ID Date Time Signal,P 0z L)
i246/P,6 DMW-1 x 1 1 3 5
DMW-2 x 1 1 3 5
PlAWC-BR x 1 1 3 56 Ov /SOS z A /'1--1 -1/
r PMWH-BR X 1 1 3UPIVIWI-BR rA -x i 1 3 5:2.M PMWM-BR i"s x 1 1 3
PMWL-B R
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&date belo wzi,melmqu Datzrrlme,A,,*plW By:Daterri e~L-1 - 0 - 0 a &/-nRequested TurnaroundRelinquishedByDate/Time ACCPW By: C vDaternmeM ,C/1y t 3 yso0 0 14 Da, , g X,1 ".2 r,Rellnquisnea By Ime Accepted By:Dat Ime E c
*7 Days23)SOSVLO~Iked y DataMme S led/Lock Opened By DataMme 0 0 -t:-48 Hr24)Com .enu PLEASE HARD COPY AND ELECTRONICALLY TRANSER THE ANALT nGAL RESULTS w
herdd :FT,Will A,,I,
CHAIN OF CUSTODY REARD AND ANALYSIS REQUEST FORM
0
---------------------------------------------------------------------
ical Laboratory Servicesi i nalytical Laboratory Use Only IDuke[&;e -o;er-La-iil~t ------ - * ------- *A !
'P aMail Code MG03A2 (Building 7405)!UMS#nPle' ge -L of
13339 Hagers Ferry Rd gin On NC_Z
A 9 SC- DISTRIBUTIONEnleargy.1 Huntersville,N. C . 28078 1 ORIGINAL to LAB,For Detailed Instructions, see :1 [phone] !Logged By Date E,Time SAMPLE PROGRAM I COPY to CLIENThttp://de~/essenv/coc/f'(S"r--'o #9-.11 Ground Water .1~...........7U4 PL5-.~.Q:L !I < 1 '/.'0 /k ............. NPDES-7)p-,.j .'.t-N.-e 2 lVendor Drinking Water - I)Phone No :875-5257 0''7SURLINGTONMGP (SHAL FRACTBR WELLS)UST
Cooler Terno (C)RCRA Waste -
E.3)Cllent C.Campbell R . Roberts T . Hunsucker 4)Fax No :875.5032 :PO #~Se c
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2-N*"l C
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CS)Project ID :MGPBURL 9)ActMty to : ALLACTV 10)Mall Code :MG03A3 C0'Customer to comolete all -072approor ate NoN-SHADEi2 areas .
0LAB USE ONLY "Chem "Collection Information E <UeSKtOp No "Sample Description or ID Q. 1-:E"Lab to Date Time Signature 1~ v z M w M 1 0DIVIW-1 x 1 1 3 5
DIVIW-2 x 1 1 3 5
PMWC-BR x 1 1 3 5
eo/"-15 PMWH-BR X 1 1 3 5Z
u PMWI-BR x 1 1 3 5
PMWL-BR
M13
555
PMWM-BR x 1 1 30
E
Customer to sign &date belo .21)Relinqu s d By a Accepted By :
22Requested TurnaroundHaunquishedByAccepiem uy: DateMme t 2 S 14 Days0 co 0M .2 alRelinquishedByUaternme Accepted By:Dit-eFim-e E v 2
n *7 Days23)SeBVLocked y Daternme beweWILOCK opened By D .-te/Tim .E M0 002~i;a '41 H,24)Comments PLEASE HARD COPY AND ELECTRONICALLY TRANSER THE ANA1100 11 CAL RE: i 1111111111 1111 ~ "A . z . ..~ , - , 1-'Other
P
UUKe 1AMIC Jr-VW`U1 1A.IldlyLlUdl I-ddUUIdL(-)IyoPower.Phone [phone] Fax [phone]
A 13339flagersFerryRoacr Huntefsvilb,NC26078-7929
McGuire Nuclear Complex - MG03A 2
CtertI114--attia. 43of Aknaly~.is.
New York State Department of Health Certification #I t 7 f 7
Oklahoma Department of Emironmentai Quality Certification # 9930
Kansas Department ofHeagh and Environment Certificate # E403f f
North Carolina Department of Health &Human Services Certification # 378 N
South Carolina (DHEQ Laboratory ID 9,99005 North Carolina (DBVR Certification 9 248
Station Name :BURLINGTON Job Number : 04-APR-0004
Sample ID #24010642 Desktop #Customer ID :L .D . CAMPBELL
Sample Description : DMW-1
CollectionDate : 28-Apr-0416 :50 :00 Date Received in Laboratory : 01-Apr-04 TypeofSample : SFBRWELLS
ReferenceMethod:EPA310 .11SM2320B Data Posted : 511712004 16 53 5 7
ALKALINITY (TOTAL INFLECTION POINT ALKALINITY 0 .84 mpqIL
Reference Method :EPA310 .1/SM2320B Data Posted : 512012004 15 :00 :0 1
ALKALINITY 13Y CALCULATION ALKALINITY 42 .00 mgLL
Reference Method :EPA 200 .716010B Data Posted:V712004 13 :21 25
IRON BY ICPtDIGESTED)IRON 1 .752 mgll
ReferenceMethod :EPA200 .7/6010B Data Posted :51"712004 13 :21 :26
MANGANESE BY ICIP (DIGESTED)_MANGANESE 0.258 mg/L
Reference Method :EPA 300.0 Data Posted : 5/5/2004 11 34 :0 0
NITRATE (IC)NITRATE 0 .45 mg/L
Reference Method :EPA 300.0 Data Posted : 5/612004 12 :12 :3 9
NITRATE BY CALCULATION(MG-NIL)NITRATE 0.10 mg-N/L
Reference Method :EPA 300b Data Posted : 5/5/2004 11 :34 :00
SULFATE .(IC)SULFATE 12.10 mg/L
Sample ID 111 :24010643 Desktop Customer 10 :L .D . CAMPBELL
Sample Description : DMW-2
Collection Date : 28-Apr-04 16:00 :00 Date Received in Laboratory : 01-Apr-04 TypeofSample : SFBRWELLS
ReferenceMethod:EPA310 .11SM23208 Data Posted : 5/1712004 16 :53 :5 7
ALKALINITY (TOTAL INFLECTION POINT)ALKALINITY,4 .56 meq/L
ReferenceMethod :EPA310 .11SM2320B Data Posted : 5/20/2004 15 :00 :D4
ALKALINITY BY CALCULATION ALKALINITY 228 .00 mg/L
Reference Method :EPA 200,7/6010B Data Posted .V712004 13 :21 :26
IRON BY ICP (DIGESTED)IRON 7 .006 mg/I
ReferenceMethod EPA200 .716010B Data Posted 51"712004 13 :21 :26
MANGANESE BY ICP (DIGESTED)MANGANESE 6 .585 mg/L
RelerenceMethod EPA300 .0 Data Posted 51512004 11 :34 35
NITRATE (IC~NITRATE < 0 .10 mg/L
Reference Method :EPA 300b Data Posted 5/612004 12 :12 :4 0
NITRATE BY CALCULATION (MG-NIL)NITRATE <0 .02 mg-NIL
... ... I G .. ..... . .1 5,~111111114 11 $16 2-
?UUKe I-AI&C rUWt1 1-kIldlyLlUdi LddL)U1dLU1y
Nower.Phone 704~15175,5245 Fax :[phone]
A W,&, C~,13339HagersFerry Road HunteisviliteNC28078-7929
McGuire Nuclear Comp,~x - MG03A 2
Cc-rtM4r-.at4-- coit AlXnalysir~
New York State Department of Health Certification #f f 717
Oklahoma Department of Environmental Quahty Certification # 9930
Kansas Department otHeagh and Environment Certificate #E-1031 1
North Carolina Department of Health &Human Services Cerlibcabon It 37804
South Carolina (DHEQ)Laboratory ID # 99005 North Carolina (DBVFO Certification #248
Station Name :BURLINGTON Job Number 04-APR-0004
Sample ID #:24010643 Desktop #Customer ID :L .D . CAMPBELL
Sample Description : DMW-2
Collection Date : 28-Apr-04 16 :00 :00 Date Received in Laboratory : 01-Apr-04 TypeofSample : SFBRWELLS
Reference Method :EPA 300 .0 Data Posted 51512004 11 34 3 5
SLILFATE(IC)SULFATE 0 .20 mgIlL
Sample ID #:24010644 Desktop #Customer ID :L .D . CAMPBELL
Sample Description : PMWC-BR
Collection Date : 26-Apr-04 15 :05 :00 Date Received in Laboratory : 01-Apr-04 TypeofSample : SFBRWELLS
ReferenceMethod :EPA310.1/SM2320B Data Posted : 5/1712DO4 16 :53:5 7
ALKALINITY. (TOTAL INFLECTION POINT)ALKALINITY 4 .26 me /L
ReferenuMethod EPA310.11SM2320B Data Posted : 5120120G4 15 .00 :0 8
ALKALINITY BY CALCULATION ALKALINITY 213 .00 mg/L
Referericeltilethiiii :EPA 200316010B Data Posted 58/2004 13212 7
IRON BY ICP(DIGESTED)IRON 13 .885 mg/I
Reference Method :EPA 2001/6010S Data Posted :V712004 13 :21 :2 7
MANGANESE BY ICP DIGESTED)_MANGANESE 3.758 mg/L
Reterenoe Method :EPA 300 .0 Data Posted 5/3/2004 15 47 00
NITRATE(IC).NITRATE 0 .22 mg1L
Relerenm Method :EPA 300o Data Posted 5/612004 12o5 5 7
NITRATE BY CALCULATION (MG-NIL)NITRATE 0.07 mg-NIL
Reference Method :EPA 300 .0 Data Posted : 5t3/2004 15 47 00
SULFATE [IC)SULFA rE 0.80 mg/l.
Sample ID if :24010645 Desktop #Customer ID :L .D . CAMPBELL
Sample Description : PMWH-B R
Collection Date: 27-Apr.04 11 :15 :00 Date Received in Laboratory: 01-Apr-04 Typeol'Sample : SFBRWELLS
Referen"Method :EPA310 .11SM23206 Data Posted 511712004 16 53.5 7
ALKALINITY (TOTAL INFLECTION POINT)ALKALINITY 3 .91 meq/L
RefiefenmMethod EPA310 .11SM2320B Data Posted 5/2WOU 15 00 1 1
ALKALINITY BY CALCULATION ALKALINITY 196 .00 mg/L
RefiefenceMethod :EPA200,7160108 Data Posted:5R120G4 13 21,2 7
IRON BY ICP (DIGESTED)IRON 4 .446 mg/l
V-11 . "I hu,~W, ~1WI-W 512112004 /1 04 2-hill,
:/Idc,v../csscn~/lab-sr,/
uuke IL)L[Kt JrUWtl'Al Idly LlUdl 1-,dL)UldLUIY
60yPower.Phone [phone] Fax [phone]
13339 Hagers Ferry Road HuntefsvIlAq,NC 28078-7929
McGulm Nuclear Complex - MG03A 2
t-- rt I 11 4= a t 4-- 43 f AOX n a I y -4s I s
New York Slate Department of Health Certification # f f717
Oklahoma Department of Environmental Quably Carlificallon #9930
Kansas Department of Heagh and Environment Certificate 9 E-103f f
North Carolina Department of t-ballh &Human Services Corlibcalion N 3780 4
South Cefohna QHEQ Laboratory ID If 9"5 North Corolina (DENR Certification N 246
Station Name :BURLINGTON Job Number: 04-APR-0004
Sample to #:24010645 Desktop #Customer ID L .D . CAMPBELL
Sample Description: PMWH-B R
Collection Date : 27-Apr-04 11 :15:00 Date Received in Laboratory : 01-Apr-04 TypeofSample : SFBRWELLS
ReferenwMethod EPA200,71501013 Data Posted :V772004 13:21 :2 8
MANGANESE BY IQP_DIGESTED)______MANGANESE 3 .854 mg/L
Reference Method.EPA 300 .0 Data Posted 5/3t2GO4 12 00 1 1
NITRAT.E .(IC)NITRATE - 0 .10 mg1L
Reference Method:EPA 300 .0 Data Posted : 5/4/2004 08 40 09
NITRATE BY CALCULATIONJMG-NILL--NITRATE <0.02 mg-NIL
Referenoe Method :EPA 300 .0 Data Posted 51312004 12 00 1 1
SULFATE (IC)_SULFATE 0 .36 mg/L
Sample to #:24010646 Desktop #Customer ID L .D .CAMPBELL
Sample Description : PMWI-B R
Collection Date : 27-Apr-04 10 :30:00 Date Received in Laboratory : 01-Apr-04 TypeofSample : SFBRWELLS
ReferenceMethod :EPA310 .11SM2320B Data Posted : 511712004 16 :53:57
ALKALINITY (TOTAL INFLECTION POIkTj,ALKALINITY 5.37 meq/L
Reference Method :EPA310 .1/SM2320B Data Posted : 5/2012004 15 :00:1 5
. ...ALKALINITY BY CALCULATION ALKALINITY 269.00 mg/L
Reference Method :EPA 200YI60108 Data Posted :5R/2004 13 :21 :2 8
IRON BY ICP,(DIGESTED)_IRON 1 .928 mg/I
ReferenwMethod EPA200 .716010B Data Posted :WINN 13 :21 :2 8
MANGANESE BY ICP JDIGESTED)MANGANESE 2.822 mg/L
Reference Method EPA 300 .0 Data Posted: 5/5/2004 11 :35 :00
NITRATE (IC)NITRATE 0 .18 mg.1-L
Reference Method .EPA 300 0 Data Posted 516/2004 12 :12 :4 1
NITRATE BY CALCULATION (MG-NIL)NITRATE 0 .04 mg-N/L
Reference Method EPA 300 .0 Data Posted 5/5/2004 11 :35 :00
SULFATE (IC)SULFATE 23.30 mg/L
0
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P UUKe VLL&t rUWtt A11d1yL1f_;d1 1-idL)U1dLU1yaPower.Phone .[phone] Fox,704-875-503 8
A~&,C~13339HOgefsFeffy Road HuntefevilleNC28078-7929
McGune Nuclear Complex - MG03A2
4~,*_-rtM4=att-_ all 9knalyEA s
New Yet* State DWartment of Health Certification # f 17 f 7
Oklahoma Department of Environmenlat Quably Certification # 9930
Kansas Department of Heagh and Environment CarlifIcale # E-103f t
North Carolina Department of Health &Human Services Certification # 37804
South Carolina (DHEQ Laboratory 10 # 99005 North Carohna (DENF~ Certification #248
Station Name :BURLINGTON Job Number 04-APR-0004
i
Sample I D #24010647 Desktop #Customer ID :L .D . CAMPBELL
Sample Description : PMWM-B R
Collection Date : 26-Apr-04 12 :45 :00 Date Received in Laboratory : 01-Apr-04 TypeofSample : SFBRWELLS
Reference Method: EPA310A/SM2320B Data Posted : 5117/2004 16 :53:57
ALKALINITY .TOTAL INFLECTION POINT)ALKALINITY 1 .07 Teg/L
Reference Method:EPA310 .11SM2320B Data Posted 512012004 15 00 1 8
ALKALINITY BY CALCULATION ALKALINITY 53.50 mg/L
ReferenceMethod EPA200 .7/6010B Data Posted W/2004 13 :21 2 9
IRON .BY ICP (DIGESTED)IRON 0 .305 ing/I
Reference Method EPA 200.716010B Data Posted :5f7/2004 13 :21 :2 9
MANGANESE BY ICP DIGESTED)MANGANESE 0.968 rng/L
Reference Method!EPA 300.0 Data Posted 51512004 11 365 5
NITRATE .(IC)NITRATE 18.75 mg/L
Reference Method :EPA 300,0 Data Posted 5/612004 12124 3
NITRATE BY CALCULATION _(MG-NIL)NITRATE.4 .23 mg-NIL
Reference Method :EPA 300.0 Data Posted 515/2OD4 113655
_SULFATE.[IC)SULFATE ... . .. 25.96 _rng/L
Sample ID #:24010648 Desktop #Customer ID :L .D . CAMPBELL
Sample Description : PMWL-B R
Collection Date : 28-Apr-04 13 :30:00 Date Received in Laboratory : 01-Apr-04 TypeofSample : SFBRWELLS
ReferenceMethod : EPA310A/SM232013 Data Posted 5117/2004 16 53 57
ALKALINITY (TOTAL INFLECTION POINT)ALKALINITY 1 .95 meq/L
RefefenmMethod :EPA310 .1/SM2320B Data Posted 5/20/2004 15 00.2 2
ALKALINITY BY CALCULATION ALKALINITY 97.50 mg/L
ReferenceMethod EPA200 .7/60i013 Data Posted : 51"712004 1121 29
IRON BY ICP (DIGESTED)IRON 0 .185 mg/I
Reference Method .EPA 200 716010B Data Posted 517/2004 13 21 30
MANGANESE BY ICP (DIGESTED)MANGANESE 0.230 mg/L
ReferenceMethod EPA300 .0 Data Posted 5/5/2004 11 39 5 1
NITRATE (IC)NITRATE < 0 .10 mg/L
Reference Method EPA 300o Data Posted : 5112/2004 07 :59 .33
NITRATE BY CALCULATION (MG-N/L)NI TRA TE <0 .02 mg-NIL
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oftwer.Phone [phone] Fax.[phone]
13339 Hagers Ferry Road Huntetsville,NC 28078-7929
McGuire Nuclear Complex - MG03A 2
4of AnalyEis
New York State Department of Health Certification #I f 717
Oklahoma Department of Environmental Quality Carlsbcalion # 9930
Kansas Department of Health and Environment Cedificate # E-1031 1
North Carolina Department of Health &Human Services Codification fit 378N
South Carolina (DHEQ Laboratory ID # 99005 North Carolina (DENR Cediftabon #24 6
Station Name :BURLINGTON Job Number : 04-APR-0004
Sample ID #:24010648 Desktop #Customer ID :L .D . CAMPBELL
Sample Description : PMWL-B R
Collection Date : 28-Apr-04 13 :30:00 Date Received in Laboratory : 01-Apr-04 TypeofSample : SFBRWELLS
Referenm Method :EPA 300 .0 Data Posted : 5/5/2004 11 :39 :5 1
SULFATE SULFATE 23.00 mg/L
Data Venfied and APPMvect 0,Date
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r UUKe DUKerrower Anaiyucal LaWraior y#Power.Phone [phone] Fox 704 .875-5036
A~E%V&~ 13339 HagersFeriy Road Huntersville,N028078-7929
McGuire Nuclear Complex - MG03A 2
Cortificate of Analysi s
New York Slate Dapadment of Health Certification #I f 7f 7
Oklahoma Department of Environmental Quality Certification #9930
Kansas Department of Heath and Environment Certificate # E. f031 f10North Carolina Department of 1-balth &Human Services Codification #37804
South Carolina (DHE-Q Laboratory ID # 99005 North Carolina (DENT~Certification #248
Sampie[D#: 24010642 Job#: 04-APR-0004
Sample Description :DMW-1
Collection Date : 28-Apr~04 15 :50 :00 Site :BURLINGTON Sample Type :S F BR WELLS Desktop #
~GPPARAWETIERSIN WATER 13Y GC/MS - 8260-
Test Code : MS8260MGPW Test Method : SW-846 50301211826013 Date Posted: 05107/04
Result Repo,_~Ljmd Flag
Benzene < 0.50 Pg/L 0 .50 Pgh- 0
Toluene < 1 .0 Pg/L 1 .0 pg/L 0
Ethylbenzene < 1 .0 PgtL 1 .0 Pgn, 0
m-p.Xylene <2.0 Per.2 .0 pWL 0
o-Xylene < 1 .0 pg/L 1 .0 pg/L 0
Naphthalene <2.0 pg/L 2 .0 vg/L 0
Sample ID#:24010643 Job#: 04-APR-0004
Sample Description :DMW-2
28-Apr-04 16 :00 :00 Site :BURLINGTON Sample Type :S F BIR WELLS Desktop #
iviG-P P-A-R-AMET-E-R-S--IN--WA-T-ER-I3-Y G-C-/-M S-- 8-26-0-
Test Code : MS8260MGPW Test Method : SW-846 5030B18260B Date Posted : 05/()7/04
Result ReporlingLumt Flag
Benzene 580 Pg/L 13 VgIL 0
Toluene 59 pg/L 25 P911 .0
Ethylbenzene 710 Pg/L 25 Par- 0
m-p-Xylene 250 Vq/L so PgrL 0
o-Xylene 250 p9h . 25 P91L 0
Naphthalene 2600 Pg/L SOD Pg/L 0
SamplelD#: 24010644 Job#: 04-APR-0004
Sample Description :PMWC-B R
Collection Date : 26-Apr-04 15 :05 :00 Site :BURLINGTON Sample Type :S F BR WELLS Desktop #
MGP PARAMETERS IN WATER BY GC/MS - 826 0
Test Code* MS8260MGPW Test Method : SW-846 503013/826013 Date Posted : 05107/04
Result Reporting Limit Fla g
Benzene 8.0 pg/L 2.5 V911 .0
Toluene < 5.0 plit, 5 .0 PglL 0
0 Ethylbenzone 14 P91L 5 .0 pg/L 0
m-p .Xylene 10 PQIL 10 P911-0
o-Xylene 13 Pg/L 5 .0 P91L 0
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"UUKe IJL[Kt IrOWel'AllalyLICal LADUFMOF YNower.Phone.[phone] Fax 704.675-,503a
&V C~13339HegersFerlyPoed Huntelsville,NC28078-7929
McGuire Nudear Comphx - MG03A 2Ct--rtmcato cof A%naly~x,-j s
New York Stale Deloartment of Health Certification # 1 f717
Oklahoma Department ofEnvironrmntalQuahtyCeififtation #9930
Kansas Department of Heath and Environment Certificate # E-1031 1
North Carolina Department of f-balth &Human Services Certification # 376N
South Carolina (DHEQ Laboratory ID #99W5 North Carolina (DENP)Certification if 248
SamplelD#: 24010644 Job#:04-APR-0004
Sample Description :PMWC-B R
Collection Date : 26-Apr-04 15 :05 :00 Site :BURLINGTON Sample Type :S F BR WELLS Desktop #
OGP PARAMETERS-I-N WATER BY-GC/-MS - 826 0
Test Code: MS8260MGPW Test Method : SW-846 5030B/8260B Date Posted : 05/07104
Result Reporyinqui-it Flag
Naphthalene 330 pg/L 10 PgtL 0
Sample ID *:24010645 Job#: 04-APR-0004
Sample Description : PMWH-B R
Collection Date : 27-Apr-04 11 :16 :00 Site :BURLINGTON Sample Type :S F BR WELLS Desktop #
imams I MMEIP111111IN
11VIG-P PARAMETERS IN WATER BY GC/MlS - 826 0
Test Code : MS8260MGPW Test Method : SW-846 5030B18260B Date Posted : 05107/04
Resufl Regorting Limit Flag
Benzene S4 pgtL 13 vg1L 0
Toluene 29 pgtL 25 pgfL 0
Ethylbenzene 220 pg/L 25 Pg/L 0
m .p.Xylene 120 p9r, 50 PgrL 0
o-Xylene 110 p9r.25 P91L 0
Naphthalene 1400 pA 200 Pgr-0
SamplelD#: 24010646 Job#:04-APR-0004
Sample Description :PMWI-B R
Collection Date : 27-Apr-04 10 :30 :00 Site :BURLINGTON Sample Type :S F BR WELLS Desktop #
IIAGP PARAMETERS IN WATER BY GCIMS - 8260
Test Code : MS8260MGPW Test Method : SW-846 5030818260B Date Posted : 05107/04
Result Repoding Limit Flag
Benzene 760 vg/L 13 Per-0
Toluene 25 pg/L 25 Pell-0
Ethylbenzene 830 pg/L 25 Pg/L 0
m-p-Xylene 110 pg/L 60 Pg/L 0
o-Xylene 350 pg/L 25 Part- 0
Naphthalene 1400 pg/L 200 pq/L 0
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NUUKe UILIKerower Anaiyrical LaDoratoryower.Phone 7C4-675-5245 Fax .[phone]
A All, &n, C~13339 Hagers Ferry Road HuntelsviIA9,NC28078-7929
McGuire Nuclear Complex - MG03A2
Cliertificatta Of Analy!sl s
New York State Department of Health Certification # I f7f7Oklahoma Depallment of Enwronmenlal Qua Wt Carlification N 9930Kansas Department of Heath end Environment Certificate # E-f03f INorth Carolina Department of f-ilealth &human Services Certification # 376NSouth Carolina (DHI5q Laboratory ID # 99005 North Carolina (DENR Certification 246
SamplelD#: 24010647 Job#: 04-APR-000 4
Sample Description : PMWM-B R
Collection Date : 26-Apr-04 12 :45 :00 Site :BURLINGTON Sample Type :S F BR WELLS Desktop #
0_GP PARAMETERS IN WATER BY GC/MS - 8260
Test Code : MS8260MGPW Test Method' SW-8"603OB/8260B Date Posted : 05/07104
Result Repo" ijinit Fla g
Benzene <2 .5 1.191 2 .5 ligh. 0
Toluene < 5 .0 Pg/L 5 .0 PgA. 0Ethylbenzene< 5 .0 PgIL 5 .0 pg/L 0
m-p .Xylene < 10 pg& 10 Pelt. 0o-Xylene < 5 .0 PgA . 5 .0 vg/L 0Naphthalene180 PglL 10 pg/L 0
SamplelD#: 24010648 Job#: 04-APR-000 4
Sample Description :PMWL-B R
,,,,,Collection Date : 28-Apr-04 13 :30 :00 Site :BURLINGTON Sample Type :S F BR WELLS Desktop #
P PARAMETERS IN WATER BY GC/IMS - 826 0
Test Code : MS8260MGPW Test Method : SW-846 5030B18260B Date Posted : W07/04
Result Rejewring Limit Fla g
Benzene < 0 .50 P91L 0 .50 Pg/L 0Toluene 2.1 Vgll . 1 .0 uglL 0
Ethylbenzene < 1 .0 Pg/L 1 .0 pg/L 0
m-p-Xylene <2.0 pgfL 2 .0 pg/L 0
o-Xylene e: 1 .0 VgtL 1 .0 pg/L 0
Naphthalene e:2 .0 pg&2.0 P91L 0
------------------------------------
Dt-_scrii:)tian c3f Flacirs :
0 -All ArriiLyticstl Proccelure Requirement, Were Met
I - St .C...
2 E .I.-.I.d Co.,ortir .l .,~ C.- ~ror-
3 Re,.rt U-1 ~.,,.loel do ..-,In owfor,n,
R .,-Urn ., 0--ler olta~ to r.q.,,..rtnalytt .rtl
(S .. C ...5 S,le R-ults Should Not Be Ucd For Rej&ul-,,r Purpose,
6 An,tlll .d.l ..'e . be'.- l .b .f .t .,r ...... 1-1concenetat,on
7 -Reported con-trat-,s, tJte cornl,,nabo, or more th,t one moclor(el,red Aettfo, of eo...nl,.~-..,n .---- ------------------------------
0
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