WI-17324_17324_CA_MRP_20150325

GROUND WATER MONITORING REPORT
MARCH 2015
HAN-DEE HUGO #1
87 JOHN L. RIEGEL ROAD
RIEGELWOOD, COLUMBUS COUNTY
NORTH CAROLINA
APS INCIDENT NO. 17324
UST INCIDENT NO. 16383 and 21823
GRI PROJECT NO.: 2652

Prepared For:

Sampson-Bladen Oil Company, Inc.
Post Office 160
Elizabethtown, North Carolina 28337

Prepared by:

Geological Resources, Inc.
3502 Hayes Road
Monroe, North Carolina 28110
[phone]

March 25, 2015

Angela Roach
Staff Scientist

EXECUTIVE SUMMARY

Han-Dee Hugo #1 is located at 87 John L. Riegel Road, in Riegelwood, Columbus County, North
Carolina. The adjoining properties are residential and commercial. Public water is available to the site
and surrounding properties. A co-mingled UST/AST ground water plume continues to exist at the site.
The site has had an active AST investigation since 1997. The UST section has reviewed the site data and
determined that a No Further Action status can be granted to the AST incident under risk based rules after
free product has been removed and consecutive sampling events demonstrate contaminant concentrations
are less than Gross Contaminant Levels (GCLs)

On March 3, 2015, seven monitoring wells were gauged, purged and sampled. Concentrations of one or
more BTEX constituents, naphthalene, isopropylbenzene, p-isopropylbenzene, n-propylbenzene, methyl
chloride, 1,2,4-trimethylbenzene, and/or 1,3,5-trimethylbenzene that exceeded the Maximum Allowable
Concentrations were reported in the ground water samples collected from MW-5R, MW-7R, MW-8R,
MW-9, MW-17R, MW-18R and MW-21R. No contaminant concentrations exceeded the GCLs.

No GCL violations have been reported at the site since 2010. Therefore, the site risk should be re-
classified to low risk; the incident should be closed; and, no further action should be required.

TABLE OF CONTENTS

1.0 SITE HISTORY AND CHARACTERIZATION ....................................................................... 1 
2.0 CURRENT SITE ASSESSMENT ................................................................................................ 1 
3.0 GROUND WATER SAMPLING ACTIVITIES ......................................................................... 1 
4.0 CONCLUSIONS AND RECOMMENDATIONS ....................................................................... 2 
5.0 LIMITATIONS .............................................................................................................................. 2 

FIGURES
Figure 1: Site Location Map
Figure 2: Site Map
Figure 3: Water Table Surface Map
Figure 4: Ground Water Quality Map

TABLES

Table 1: Well Construction and Gauging Information
Table 2: Summary of Soil Sample Analytical Results

APPENDIX
Appendix A: Laboratory Analytical Report – Ground Water Samples

1

1.0 SITE HISTORY AND CHARACTERIZATION
The Han-Dee Hugo #1 is located at 87 John L. Riegel Road, in Riegelwood, Columbus County, North
Carolina (Figure 1). The site has been in operation as a retail petroleum facility since 1969. Previously,
the on-site bulk petroleum facility had four ASTs: one 14,000-gallon diesel, one 14,000-gallon kerosene,
one 15,500-gallon fuel oil, and one 500-gallon kerosene.

Please note that prior to January 2008, previous investigation activities at the site were conducted by
Environmental Hydrogeological Consultants, Inc. (EHC) and CBM Environmental Services, Inc. (CBM).
Previous investigation activities included a Comprehensive Site Assessment (CSA) by EHC in 1997 and
subsequent LSA activities by CBM pertaining to a UST release at the site. The UST incident was
classified as low risk and the incident was closed following a deed recordation of a Notice of Residual
Petroleum. At that time the AST incident was managed by the North Carolina Department of
Environment and Natural Resources (NCDENR) Ground Water Section. The Ground Water Section
acknowledged that the UST and AST plumes had comingled and therefore applied risk-based clean-up
rules to the incident.

Please note that some of the information contained in this report was obtained under the supervision of
EHC and CBM, the previous consultants on the project, until GRI conducted assessment activities in
January 2008. Although Geological Resources, Inc. (GRI) cannot verify the accuracy of the information
obtained by previous consultants, for the purpose of this report it is assumed to be correct, and any
inferences or interpretations made by GRI based on data that may be incorrect are not the responsibility of
GRI. Please refer to earlier submittals for additional information regarding assessment activities.

2.0 CURRENT SITE ASSESSMENT
The purpose of this report presents the results of the monitoring well installation and ground water
sampling activities conducted at the Han-Dee Hugo #1 in Riegelwood, Columbus County, North Carolina
(Figure 1). The activities were conducted in accordance with GRI Proposal Number 15-004 which was
submitted to NCDENR on January 21, 2015 and approved as Task Authorization Number 21823-06 on
February 26, 2015. The purpose of these activities was to obtain current ground water quality data.

3.0 GROUND WATER SAMPLING ACTIVITIES
On March 3, 2015, seven Type II monitoring wells (MW-5R, MW-7R, MW-8R, MW-9, MW-17R, MW-
18R, and MW-21R) were gauged, purged, and sampled. The depths to ground water in the Type II
monitoring wells during the March 2015 sampling event ranged from 7.76 to 12.28 feet below the tops of

2

well casings. Ground water elevations in the Type II monitoring wells relative to a temporary benchmark
assumed by the previous consultant ranged from 91.22 to 91.54 feet. Based on these data, the ground
water flow direction at the site is primarily towards the south with an average horizontal hydraulic
gradient of less than 0.01 feet per foot. A Site Map showing the structures on-site and the locations of the
monitoring wells is included as Figure 2. A Water Table Surface Map for the March 3, 2015 sampling
event has been included as Figure 3. A summary of well construction information including ground
water elevation data is presented in Table 1.

Laboratory analyses were performed on the ground water samples collected from the monitoring wells
during the March 2015 sampling event for volatile organic compounds by EPA Method 6200B.
Concentrations of one or more BTEX constituents, naphthalene, isopropylbenzene, p-isopropylbenzene,
n-propylbenzene, methyl chloride, 1,2,4-trimethylbenzene, and/or 1,3,5-trimethylbenzene that exceeded
the maximum allowable concentrations (MACs) specified in T15A NCAC 2L.0202 were reported in the
ground water samples collected from MW-5R, MW-7R, MW-8R, MW-9, MW-17R, MW-18R, and MW-
21R. However, no contaminant concentrations exceeded the gross contaminant levels (GCLs). A Ground
Water Quality Map based on data from the March 3, 2015 sampling event has been included as Figure 4.
A summary of ground water sample analytical results is presented in Table 2. A complete laboratory
report has been included as Appendix A.

4.0 CONCLUSIONS AND RECOMMENDATIONS
 The average depth to ground water in the Type II monitoring wells during the March 2015
sampling event was 9.22 feet. Ground water flow was generally toward the south.
 Concentrations of one or more BTEX constituents, naphthalene, isopropylbenzene, p-
isopropylbenzene, n-propylbenzene, methyl chloride, 1,2,4-trimethylbenzene, and/or 1,3,5-
trimethylbenzene that exceeded the MACs were reported in the ground water samples collected
from MW-5R, MW-7R, MW-8R, MW-9, MW-17R, MW-18R and MW-21R. No contaminant
concentrations exceeded the GCLs.
 No GCL violations have been reported at the site since 2010. Therefore, the site risk should be
reduced to low; and, no further action should be required.

5.0 LIMITATIONS
This report has been prepared for the exclusive use of Sampson-Bladen Oil Company, Inc. for specific
application to the referenced site in Columbus County, North Carolina. The assessment was conducted
based on the scope of work and level of effort specified by the NCDENR and with resources adequate

3

only for that scope of work. Our findings have been developed in accordance with generally accepted
standards of geology and hydrogeology practices in the State of North Carolina, available information,
and our professional judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would be
interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data.

FIGURES

TABLES
Date: 3/23/15
07/10/06 7.81 0.00 90.28
10/30/06 7.19 0.00 90.90
02/21/07 6.47 0.00 91.62
05/24/07 7.55 0.00 90.54
01/30/08 10.40 0.00 87.69
08/11/08 9.98 0.00 88.11
02/09/09 9.06 0.00 89.03
08/03/09 7.59 0.00 90.50
05/13/10 NM NM NM
07/25/12 9.90 0.00 88.19
06/25/14 7.94 0.00 90.15
07/10/06 10.87 0.00 89.84
10/30/06 10.34 0.00 90.37
02/21/07 9.60 0.00 91.11
05/24/07 10.64 0.00 90.07
01/30/08 14.17 1.03 87.42
02/07/08 14.30 1.20 87.44
02/14/08 13.38 0.11 87.42
08/11/08 12.84 0.03 87.90
02/09/09 12.12 0.00 88.59
08/03/09 10.65 0.00 90.06
05/13/10 11.20 0.00 89.51
07/25/12 12.87 0.00 87.84
03/11/13 11.64 0.00 89.07
03/15/13 11.88 0.00 88.83
04/11/13 11.51 0.00 89.20
09/24/13
05/15/14 10.31 0.00 90.47
06/25/14 11.02 0.00 89.76
11/05/14 10.91 0.00 89.87
03/03/15 9.39 0.00 91.39
07/10/06 8.58 0.00 90.11
10/30/06 7.97 0.00 90.72
02/21/07 7.27 0.00 91.42
05/24/07 8.31 0.00 90.38
01/30/08 11.12 0.00 87.57
02/07/08 11.05 0.00 87.64
02/14/08 11.06 0.00 87.63
08/11/08 10.65 0.00 88.04
02/09/09 9.84 0.00 88.85
08/03/09
07/10/06 9.83 0.00 89.82
10/30/06 9.28 0.00 90.37
02/21/07 8.50 0.00 91.15
05/24/07 9.59 0.00 90.06
01/30/08 12.23 0.00 87.42
08/11/08 11.83 0.00 87.82
02/09/09 11.03 0.00 88.62
08/03/09 9.42 0.00 90.23
05/13/10 10.07 0.00 89.58
07/25/12 11.78 0.00 87.87
05/15/14 9.26 0.00 90.39
06/25/14 9.90 0.00 89.75
11/05/14 9.78 0.00 89.87
03/03/15 8.31 0.00 91.34
07/10/06 13.83 0.00 89.99
10/30/06 13.23 0.00 90.59
02/21/07 12.42 0.00 91.40
05/24/07 13.54 0.00 90.28
01/30/08 16.41 0.11 87.50
02/07/08 12.34 0.06 91.53
02/14/08 16.35 0.08 87.54
08/11/08 15.68 0.00 88.14
02/09/09 15.08 0.00 88.74
08/03/09 13.59 0.00 90.23
05/13/10 14.08 0.00 89.74
07/25/12 15.84 0.00 87.98
06/25/14 13.99 0.00 89.83
11/05/14 13.75 0.00 90.07
03/03/15 12.28 0.00 91.54
Abandoned
MW-6R 07/06/06 0 - 8 8 - 18 18 98.69
Destroyed
MW-5R 07/06/06 0 - 8 8 - 18 18 100.71
TABLE 1
WELL CONSTRUCTION & GAUGING INFORMATION
HAN-DEE HUGO #1
Well ID
Date
Installed
(m/dd/yy)
Date Water
Level
Measured
(m/dd/yy)
Well Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom of
Well
(ft. BGS)
Top of Casing
Elevation*
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
Groundwater
Elevation* (ft.)
(APS INCIDENT NO. 17324; UST INCIDENT NOS. 16383 and 21823)
Facility ID#: 0-002328
MW-4R 07/06/06 0 - 8 8 - 18 18 98.09
MW-5R 05/07/14 0 - 5 5 - 20 20 100.78
MW-7R 07/06/06 0 - 8 8 - 18 18 99.65
MW-8R 07/06/06 0 - 8 8 - 18 18 103.82
Page 1 of 4
Date: 3/23/15
TABLE 1
WELL CONSTRUCTION & GAUGING INFORMATION
HAN-DEE HUGO #1
Well ID
Date
Installed
(m/dd/yy)
Date Water
Level
Measured
(m/dd/yy)
Well Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom of
Well
(ft. BGS)
Top of Casing
Elevation*
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
Groundwater
Elevation* (ft.)
(APS INCIDENT NO. 17324; UST INCIDENT NOS. 16383 and 21823)
Facility ID#: 0-002328
07/10/06 9.97 0.00 90.03
10/30/06 9.29 0.00 90.71
02/21/07 8.65 0.00 91.35
05/24/07 9.79 0.00 90.21
01/30/08 12.57 0.03 87.46
02/07/08 12.47 0.02 87.55
02/14/08 12.48 0.03 87.55
08/11/08 12.06 0.00 87.94
02/09/09 11.26 0.00 88.74
08/03/09 9.88 0.00 90.12
05/13/10 10.38 0.00 89.62
07/25/12 12.13 0.00 87.87
06/25/14 10.21 0.00 89.79
11/05/14 10.02 0.00 89.98
03/03/15 8.51 0.00 91.49
10/30/06 8.73 0.00 88.95
02/21/07 7.99 0.00 89.69
05/24/07 8.99 0.00 88.69
01/30/08 11.36 0.00 86.32
08/11/08 11.12 0.00 86.56
02/09/09 10.43 0.00 87.25
08/03/09 8.76 0.00 88.92
05/13/10 9.51 0.00 88.17
07/25/12 11.10 0.00 86.58
06/25/14 9.32 0.00 88.36
10/30/06 8.67 0.00 85.58
02/21/07 8.00 0.00 86.25
05/24/07 8.98 0.00 85.27
01/30/08 11.46 0.00 82.79
08/11/08 11.12 0.00 83.13
02/09/09 10.43 0.00 83.82
08/03/09 8.70 0.00 85.55
05/13/10 NM NM NM
07/25/12 11.11 0.00 83.14
06/25/14 9.32 0.00 84.93
10/30/06 9.62 0.00 83.23
02/21/07 11.52 0.00 81.33
05/24/07 12.89 0.00 79.96
01/30/08 DRY DRY DRY
08/11/08 DRY DRY DRY
02/09/09 14.57 0.00 78.28
08/03/09 13.02 0.00 79.83
05/13/10 NM NM NM
07/25/12 DRY DRY DRY
10/30/06 8.56 0.00 84.12
02/21/07 8.20 0.00 84.48
05/24/07 9.13 0.00 83.55
01/30/08 11.63 0.00 81.05
08/11/08 11.45 0.00 81.23
02/09/09 10.71 0.00 81.97
08/03/09 9.11 0.00 83.57
05/13/10 9.65 0.00 83.03
07/25/12 11.47 0.00 81.21
06/25/14 11.73 0.00 80.95
10/30/06 8.56 0.00 87.50
02/21/07 7.90 0.00 88.16
05/24/07 8.59 0.00 87.47
01/30/08 11.12 0.00 84.94
08/11/08 10.76 0.00 85.30
02/09/09 10.14 0.00 85.92
08/03/09 8.54 0.00 87.52
05/13/10 9.27 0.00 86.79
07/25/12 10.83 0.00 85.23
06/25/14 9.21 0.00 86.85
5 - 15
MW-11R 10/26/06 0 - 8 8 - 18 18 97.68
MW-12R 10/26/06 0 - 8 8 - 18 18
10/26/06 0 - 5 15 92.85
MW-14R 10/26/06 0 - 8 8 - 18 18 92.68
MW-15 07/02/97 0 - 8 8 - 18 18 96.06
MW-9 05/29/97 0 - 3 3 - 13 13 100.00
94.25
MW-13R
Page 2 of 4
Date: 3/23/15
TABLE 1
WELL CONSTRUCTION & GAUGING INFORMATION
HAN-DEE HUGO #1
Well ID
Date
Installed
(m/dd/yy)
Date Water
Level
Measured
(m/dd/yy)
Well Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom of
Well
(ft. BGS)
Top of Casing
Elevation*
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
Groundwater
Elevation* (ft.)
(APS INCIDENT NO. 17324; UST INCIDENT NOS. 16383 and 21823)
Facility ID#: 0-002328
07/10/06 10.68 0.00 89.72
10/30/06 10.11 0.00 90.29
02/21/07 9.40 0.00 91.00
05/24/07 10.43 0.00 89.97
01/30/08 13.84 1.03 87.44
02/07/08 14.11 1.38 87.47
02/14/08 13.02 0.02 87.40
08/11/08 12.55 0.03 87.88
02/09/09 11.84 0.00 88.56
08/03/09 10.49 0.00 89.91
05/13/10 10.91 0.00 89.49
07/25/12 12.54 0.00 87.86
05/15/14 10.07 0.00 90.33
06/25/14 10.78 0.00 89.62
11/05/14 10.61 0.00 89.79
03/03/15 9.18 0.00 91.22
07/10/06 10.65 0.00 89.73
10/30/06 10.00 0.00 90.38
02/21/07 9.34 0.00 91.04
05/24/07 10.27 0.00 90.11
01/30/08 12.97 0.00 87.41
08/11/08 12.59 0.00 87.79
02/09/09 11.79 0.00 88.59
08/03/09 10.34 0.00 90.04
05/13/10 10.87 0.00 89.51
07/25/12 12.55 0.00 87.83
05/15/14 10.03 0.00 90.35
06/25/14 10.73 0.00 89.65
11/05/14 10.56 0.00 89.82
03/03/15 9.12 0.00 91.26
07/10/06 7.81 0.00 90.28
10/30/06 7.25 0.00 90.84
02/21/07 6.47 0.00 91.62
05/24/07 7.59 0.00 90.50
01/30/08 10.38 0.00 87.71
08/11/08 10.00 0.00 88.09
02/09/09 9.18 0.00 88.91
08/03/09 7.65 0.00 90.44
05/13/10 8.11 0.00 89.98
07/25/12 9.95 0.00 88.14
06/25/14 8.00 0.00 90.09
07/10/06 9.25 0.00 90.02
10/30/06 8.65 0.00 90.62
02/21/07 7.90 0.00 91.37
05/24/07 8.96 0.00 90.31
01/30/08 11.80 0.09 87.55
02/07/08 11.68 0.02 87.61
02/14/08 11.80 0.12 87.57
08/11/08 11.30 0.00 87.97
02/09/09 10.47 0.00 88.80
08/03/09 9.03 0.00 90.24
05/13/10 9.49 0.00 89.78
07/25/12 13.15 1.20 87.15
03/11/13 10.01 0.00 89.26
03/15/13 10.23 0.00 89.04
04/11/13 9.66 0.00 89.61
09/24/13
05/15/14 8.73 0.00 90.51
06/25/14 9.45 0.00 89.79
11/05/14 9.23 0.00 90.01
03/03/15 7.76 0.00 91.48
08/11/08 10.56 0.00 88.04
02/09/09 9.73 0.00 88.87
08/03/09 8.27 0.00 90.33
05/13/10 8.58 0.00 90.02
07/25/12 10.51 0.00 88.09
06/25/14 8.61 0.00 89.99
MW-21R 07/06/06 0 - 8 8 - 18 18 99.27
Abandoned
MW-22 08/07/08 0 - 4 4 - 14 14 98.60
MW-20R 07/06/06 0 - 8 8 - 18 18 98.09
MW-17R 07/06/06 0 - 8 8 - 18 18 100.40
MW-18R 07/06/06 0 - 8 8 - 18 18 100.38
MW-21R 05/07/14 0 - 5 5 - 20 20 99.24
Page 3 of 4
Date: 3/23/15
TABLE 1
WELL CONSTRUCTION & GAUGING INFORMATION
HAN-DEE HUGO #1
Well ID
Date
Installed
(m/dd/yy)
Date Water
Level
Measured
(m/dd/yy)
Well Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom of
Well
(ft. BGS)
Top of Casing
Elevation*
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
Groundwater
Elevation* (ft.)
(APS INCIDENT NO. 17324; UST INCIDENT NOS. 16383 and 21823)
Facility ID#: 0-002328
08/11/08 14.10 0.00 88.01
02/09/09 13.24 0.00 88.87
08/03/09 11.77 0.00 90.34
05/13/10 NM NM NM
07/25/12 14.02 0.00 88.09
06/25/14 12.11 0.00 90.00
02/09/09 7.94 0.00 92.63
08/03/09 11.71 0.00 88.86
05/13/10 NM NM NM
07/25/12 11.76 0.00 88.81
06/25/14 11.13 0.00 89.44
03/11/13 10.05 0.00 NM
03/15/13 10.51 0.00 NM
04/11/13 9.86 0.00 NM
09/24/13
03/11/13 11.68 0.00 NM
03/15/13 12.06 0.00 NM
04/11/13 11.52 0.00 NM
9/24/2013
Notes:
• If free product is present, groundwater elevation is calculated by: [Top of Casing Elevation - Depth to Water] + [free product thickness x 0.8581].
• Please note, monitoring wells MW-5R and MW-21R were reinstalled on May 7, 2014.
• *: Top-of-casing elevation and well construction data is reproduced from the GWSR Report dated June 22, 2007 prepared
by CBM Environmental Services, Inc.
• **: Elevations relative to arbitrary datum with assumed elevation of 100.00 feet; data reported in feet.
• ft BGS: feet below ground surface.
Abandoned
20 NM0-5 5-20
RW-2 03/04/13 0-5 5-20 20 NM
Abandoned
MW-23 08/07/08 0 - 6.5 6.5 - 16.5 16.5 102.11
TW-2 02/06/09 0 - 55 55 - 60 60 100.57
RW-1 03/04/13
Page 4 of 4
Date: 03/23/15Well IDDateCollected(mm/dd/yy)1 600 600 500 20 6 3 70 25 70 400 4005,000 260,000 84,500 85,500 20,000 6,000 3,000 25,000 11,700 30,000 28,500 25,00007/25/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 ******06/25/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 0.16 J <0.10 <0.10 <0.10 <0.10 <0.10 07/25/124,05066.93,170 2,19015.9 J901******06/25/143,62061.42,990 72611.3 J779<5.0 19214.6 J472 2,80019011/05/144,68073.23,230498 <10 930<10 17912.2 J433 2,63015403/03/152,18036.82,200310 4.2653 8.6 19617430 2,29011907/25/1235.7 2,050 1,900 11,000<6.5 698******06/25/1411.7 J 909 1,180 10,900<10 676<10 95.8<10 198 2,070 56311/05/1410.2 J 645 987 9,680<10 687<10 78.2<10 169 1,950 55903/03/15 <0.86 22.4 92.41,140<0.82 98.9<0.79 14.8 2.7 34.4 396 16207/25/12 <6.5 2,070 1,100 5,520<6.5 374******06/25/1427.9 2,070 1,170 11,800<5.0 741<5.0 10615.8 J207 3,860 85111/05/1417.3 J 1,650 666 6,890<10 537<10 48.3 J <10 86.2 1,420 46803/03/15 <1.7 92.9 98876<1.6 84.4<1.6 11.8 3.5 J 23.6 345 13307/25/12 <1.3 13.3 1881000<1.3 136******06/25/14 0.62 J 11.5 66 430 <0.50 66.31.7 J 7.5 3.6 18.1 171 52.911/05/142.911 49.6 434 <0.50 69.5<0.50 3.4 0.77 J 6.7 89.8 47.803/03/15 0.82 6.4 30.9 233 <0.16 36.70.56 2.6 0.76 5.1 56.4 33.807/25/12 0.93 <0.13 <0.15 <0.30 0.35 J 0.17 J******06/25/14 <0.10 <0.10 <0.10 <0.20 0.13 J 0.21 J 0.17 J <0.10 <0.10 <0.10 <0.10 <0.10 07/25/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 ******06/25/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 MW-14 07/25/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 ******MW-14R 06/25/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 07/25/12 0.92 <0.13 <0.15 <0.30 0.74 <0.10 ******06/25/14 <0.10 <0.10 <0.10 <0.20 0.46 J <0.10 0.26 J <0.10 <0.10 <0.10 <0.10 <0.10 MW-17 07/25/121,480 2,710 3,100 17,200<26 840******TABLE 2SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTSHAN-DEE HUGO #1(APS INCIDENT NO. 17324; UST INCIDENT NOS. 16383 and 21823) Facility ID#: 0-002328Analytical Method Contaminant of Concern BenzeneTolueneEthylbenzeneTotal XylenesMethyl-tert-butyl ether(MTBE)NaphthaleneMethyl chloride(Chloromethane)Isopropylbenzenep-Isopropyltoluene(4-Isopropyltoluene)1,3,5-Trimethylbenzene2L Standard (µg/l)GCL (µg/l)MW-4RMW-5REPA Method 6200B or EPA Method 602MW-7RMW-8RMW-9MW-11RMW-12RMW-151,2,4-Trimethylbenzenen-PropylbenzenePage 1 of 2
Date: 03/23/15Well IDDateCollected(mm/dd/yy)1 600 600 500 20 6 3 70 25 70 400 4005,000 260,000 84,500 85,500 20,000 6,000 3,000 25,000 11,700 30,000 28,500 25,000TABLE 2SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTSHAN-DEE HUGO #1(APS INCIDENT NO. 17324; UST INCIDENT NOS. 16383 and 21823) Facility ID#: 0-002328Analytical Method Contaminant of Concern BenzeneTolueneEthylbenzeneTotal XylenesMethyl-tert-butyl ether(MTBE)NaphthaleneMethyl chloride(Chloromethane)Isopropylbenzenep-Isopropyltoluene(4-Isopropyltoluene)1,3,5-Trimethylbenzene2L Standard (µg/l)GCL (µg/l)EPA Method 6200B or EPA Method 6021,2,4-Trimethylbenzenen-Propylbenzene06/25/14756 1,660 2,390 12,900<5.0 762<5.0 262 32.1 639 4,830 1,24011/05/141,520 4,930 3,180 20,000<10 1,020<10 21923.2 J533 4,610 1,27003/03/15654 1,540 1,660 9,880<16 729<16 196 43.5 J 512 4,110 1,410MW-18 07/25/12139031.2 201 40.7 J 8.2 J63.5******06/25/141856.5 43.9 15.7 1.317.8<0.10 49.1 0.785.831.8 4.211/05/142708.3 118 32.2 2.543.70.7281.20.7318651.4 9.503/03/151444.5 13.1 2.5 J 1.2 J7.02.4 J 31.1 <0.61 68.6 3 0.70 JMW-20 07/25/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 ******MW-20R 06/25/14 <0.10 <0.10 <0.10 <0.20 <0.10 0.18 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 06/25/145.10.33 J 58.4 38.3 0.15 J46.40.34 J 18 6.9 34.3 222 14.611/05/14130.44 J 49 14.7 0.46 J130.38 J 8.5 3.1 12.2 47.6 3.103/03/153.60.19 J 27.8 7.7 <0.16 8.8<0.16 6.7 3.6 12.3 28.5 0.8307/25/12 0.44 J 0.65 128 53.4 <0.13 51.7******06/25/14 0.54 1 457 288 <0.10 3160.18 J 61.7 8.9147 80117507/25/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 ******06/25/14 <0.10 <0.10 <0.10 <0.20 <0.10 0.18 J 0.11 J <0.10 <0.10 <0.10 <0.10 <0.10 07/25/125.80.7 0.89 9.1 0.25 J 0.24 J******06/25/14 0.18 J <0.10 <0.10 0.26 J <0.10 <0.10 0.15 J <0.10 <0.10 <0.10 <0.10 <0.10 Notes:• Results reported in micrograms per liter (µg/l).• < : Less than the method detection limit specified in the laboratory report.• 2L Standard specified in T15A NCAC 2L.0202.• GCL: Gross contamination level.• NE: Not Established• Concentrations in bold face type exceeded the 2L standards.• Concentrations in italics exceeded the gross contamination levels.• * Refer to laboratory report for detected constituents that did not exceed the GCLs, or for which no standard has been established.MW-17RMW-18RMW-21RMW-22MW-23TW-2Page 2 of 2

APPENDIX

APPENDIX A
Laboratory Analytical Report-Ground Water Samples

03/20/15
Technical Report for
GRI (Geological Resources Inc.)
Handee Hugo 1; US Hwy 87, Reigelwood, NC
17324
Accutest Job Number: FA22722
Sampling Date: 03/03/15
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28207
[e-mail]; [e-mail];
[e-mail]; [e-mail]
ATTN: Rae Brown
Total number of pages in report:
Certifications: FL (E83510), LA (03051), KS (E-10327), IA (366), IL (200063), NC (573), NJ (FL002), SC (96038001)
DoD ELAP (L-A-B L2229), CA (2937), TX (T104704404), PA (68-03573), VA (460177),
AK, AR, GA, KY, MA, NV, OK, UT, WA
This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone] • http://www.accutest.com
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Norm Farmer
Technical Director
Southeast
03/20/15
e-Hardcopy 2.0
Automated Report
44
Accutest Laboratories is the sole authority for authorizing edits or modifications to this
document. Unauthorized modification of this report is strictly prohibited.
1 of 44
FA22722
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................7
3.1: FA22722-1: MW-21R ...................................................................................................8
3.2: FA22722-2: MW-9 ........................................................................................................10
3.3: FA22722-3: MW-8R .....................................................................................................12
3.4: FA22722-4: MW-7R .....................................................................................................14
3.5: FA22722-5: MW-5R .....................................................................................................16
3.6: FA22722-6: MW-18R ...................................................................................................18
3.7: FA22722-7: MW-17R ...................................................................................................20
Section 4: Misc. Forms ............................................................................................................22
4.1: Chain of Custody ...........................................................................................................23
Section 5: GC/MS Volatiles - QC Data Summaries ..............................................................26
5.1: Method Blank Summary ................................................................................................27
5.2: Blank Spike Summary ...................................................................................................33
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................39 123452 of 44
FA22722
Accutest Laboratories
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA22722
Handee Hugo 1; US Hwy 87, Reigelwood, NC
Project No: 17324
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA22722-1 03/03/15 14:09 DB 03/11/15 AQ Ground Water MW-21R
FA22722-2 03/03/15 14:19 DB 03/11/15 AQ Ground Water MW-9
FA22722-3 03/03/15 14:27 DB 03/11/15 AQ Ground Water MW-8R
FA22722-4 03/03/15 14:43 DB 03/11/15 AQ Ground Water MW-7R
FA22722-5 03/03/15 14:58 DB 03/11/15 AQ Ground Water MW-5R
FA22722-6 03/03/15 15:15 DB 03/11/15 AQ Ground Water MW-18R
FA22722-7 03/03/15 15:29 DB 03/11/15 AQ Ground Water MW-17R
3 of 44
FA22722 1
Summary of Hits Page 1 of 3
Job Number:FA22722
Account:GRI (Geological Resources Inc.)
Project:Handee Hugo 1; US Hwy 87, Reigelwood, NC
Collected:03/03/15
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA22722-1 MW-21R
Benzene 3.6 0.50 0.17 ug/l SM 6200B
n-Butylbenzene 2.6 0.50 0.14 ug/l SM 6200B
sec-Butylbenzene 4.6 0.50 0.14 ug/l SM 6200B
tert-Butylbenzene 0.82 0.50 0.15 ug/l SM 6200B
Ethylbenzene 27.8 0.50 0.15 ug/l SM 6200B
Isopropylbenzene 6.7 0.50 0.12 ug/l SM 6200B
p-Isopropyltoluene 3.6 0.50 0.12 ug/l SM 6200B
Naphthalene 8.8 0.50 0.12 ug/l SM 6200B
n-Propylbenzene 12.3 0.50 0.16 ug/l SM 6200B
Toluene 0.19 J 0.50 0.17 ug/l SM 6200B
1,2,4-Trimethylbenzene 28.5 0.50 0.14 ug/l SM 6200B
1,3,5-Trimethylbenzene 0.83 0.50 0.14 ug/l SM 6200B
m,p-Xylene 7.5 1.0 0.30 ug/l SM 6200B
o-Xylene 0.18 J 0.50 0.13 ug/l SM 6200B
Xylene (total)7.7 1.5 0.43 ug/l SM 6200B
FA22722-2 MW-9
Benzene 0.82 0.50 0.17 ug/l SM 6200B
n-Butylbenzene 0.60 0.50 0.14 ug/l SM 6200B
sec-Butylbenzene 0.51 0.50 0.14 ug/l SM 6200B
Chloroethane 0.52 0.50 0.21 ug/l SM 6200B
Ethylbenzene 30.9 0.50 0.15 ug/l SM 6200B
Isopropylbenzene 2.6 0.50 0.12 ug/l SM 6200B
p-Isopropyltoluene 0.76 0.50 0.12 ug/l SM 6200B
Methyl Chloride 0.56 0.50 0.16 ug/l SM 6200B
Naphthalene 36.7 0.50 0.12 ug/l SM 6200B
n-Propylbenzene 5.1 0.50 0.16 ug/l SM 6200B
Toluene 6.4 0.50 0.17 ug/l SM 6200B
1,2,4-Trimethylbenzene 56.4 2.5 0.68 ug/l SM 6200B
1,3,5-Trimethylbenzene 33.8 0.50 0.14 ug/l SM 6200B
m,p-Xylene 171 5.0 1.5 ug/l SM 6200B
o-Xylene 62.5 2.5 0.67 ug/l SM 6200B
Xylene (total)233 7.5 2.2 ug/l SM 6200B
FA22722-3 MW-8R
n-Butylbenzene 4.3 J 5.0 1.4 ug/l SM 6200B
sec-Butylbenzene 3.5 J 5.0 1.4 ug/l SM 6200B
tert-Butylbenzene 1.6 J 5.0 1.5 ug/l SM 6200B
Ethylbenzene 98.0 5.0 1.5 ug/l SM 6200B
Isopropylbenzene 11.8 5.0 1.2 ug/l SM 6200B
p-Isopropyltoluene 3.5 J 5.0 1.2 ug/l SM 6200B
4 of 44
FA22722 2
Summary of Hits Page 2 of 3
Job Number:FA22722
Account:GRI (Geological Resources Inc.)
Project:Handee Hugo 1; US Hwy 87, Reigelwood, NC
Collected:03/03/15
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
Naphthalene 84.4 5.0 1.2 ug/l SM 6200B
n-Propylbenzene 23.6 5.0 1.6 ug/l SM 6200B
Toluene 92.9 5.0 1.7 ug/l SM 6200B
1,2,4-Trimethylbenzene 345 5.0 1.4 ug/l SM 6200B
1,3,5-Trimethylbenzene 133 5.0 1.4 ug/l SM 6200B
m,p-Xylene 595 10 3.0 ug/l SM 6200B
o-Xylene 281 5.0 1.3 ug/l SM 6200B
Xylene (total)876 15 4.3 ug/l SM 6200B
FA22722-4 MW-7R
n-Butylbenzene 3.9 2.5 0.72 ug/l SM 6200B
sec-Butylbenzene 3.1 2.5 0.69 ug/l SM 6200B
tert-Butylbenzene 0.75 J 2.5 0.73 ug/l SM 6200B
Ethylbenzene 92.4 2.5 0.76 ug/l SM 6200B
Isopropylbenzene 14.8 2.5 0.59 ug/l SM 6200B
p-Isopropyltoluene 2.7 2.5 0.61 ug/l SM 6200B
Naphthalene 98.9 2.5 0.61 ug/l SM 6200B
n-Propylbenzene 34.4 2.5 0.78 ug/l SM 6200B
Toluene 22.4 2.5 0.83 ug/l SM 6200B
1,2,4-Trimethylbenzene 396 10 2.7 ug/l SM 6200B
1,3,5-Trimethylbenzene 162 2.5 0.68 ug/l SM 6200B
m,p-Xylene 724 20 5.9 ug/l SM 6200B
o-Xylene 411 10 2.7 ug/l SM 6200B
Xylene (total)1140 30 8.6 ug/l SM 6200B
FA22722-5 MW-5R
Benzene 2180 25 8.6 ug/l SM 6200B
n-Butylbenzene 38.7 2.5 0.72 ug/l SM 6200B
sec-Butylbenzene 29.2 2.5 0.69 ug/l SM 6200B
tert-Butylbenzene 4.0 2.5 0.73 ug/l SM 6200B
Chloroethane 14.0 2.5 1.0 ug/l SM 6200B
Ethylbenzene 2200 25 7.6 ug/l SM 6200B
Isopropylbenzene 196 2.5 0.59 ug/l SM 6200B
p-Isopropyltoluene 17.0 2.5 0.61 ug/l SM 6200B
Methyl Chloride 8.6 2.5 0.79 ug/l SM 6200B
Methyl Tert Butyl Ether 4.2 2.5 0.82 ug/l SM 6200B
Naphthalene 653 25 6.1 ug/l SM 6200B
n-Propylbenzene 430 25 7.8 ug/l SM 6200B
Toluene 36.8 2.5 0.83 ug/l SM 6200B
1,2,4-Trimethylbenzene 2290 25 6.8 ug/l SM 6200B
1,3,5-Trimethylbenzene 119 2.5 0.68 ug/l SM 6200B
m,p-Xylene 305 5.0 1.5 ug/l SM 6200B
o-Xylene 4.0 2.5 0.67 ug/l SM 6200B
5 of 44
FA22722 2
Summary of Hits Page 3 of 3
Job Number:FA22722
Account:GRI (Geological Resources Inc.)
Project:Handee Hugo 1; US Hwy 87, Reigelwood, NC
Collected:03/03/15
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
Xylene (total)310 7.5 2.2 ug/l SM 6200B
FA22722-6 MW-18R
Benzene 144 2.5 0.86 ug/l SM 6200B
n-Butylbenzene 5.2 2.5 0.72 ug/l SM 6200B
sec-Butylbenzene 5.4 2.5 0.69 ug/l SM 6200B
Chloroethane 3.2 2.5 1.0 ug/l SM 6200B
Ethylbenzene 13.1 2.5 0.76 ug/l SM 6200B
Isopropylbenzene 31.1 2.5 0.59 ug/l SM 6200B
Methyl Chloride 2.4 J 2.5 0.79 ug/l SM 6200B
Methyl Tert Butyl Ether 1.2 J 2.5 0.82 ug/l SM 6200B
Naphthalene 7.0 2.5 0.61 ug/l SM 6200B
n-Propylbenzene 68.6 2.5 0.78 ug/l SM 6200B
Toluene 4.5 2.5 0.83 ug/l SM 6200B
1,2,4-Trimethylbenzene 3.0 2.5 0.68 ug/l SM 6200B
1,3,5-Trimethylbenzene 0.70 J 2.5 0.68 ug/l SM 6200B
m,p-Xylene 2.5 J 5.0 1.5 ug/l SM 6200B
Xylene (total)2.5 J 7.5 2.2 ug/l SM 6200B
FA22722-7 MW-17R
Benzene 654 50 17 ug/l SM 6200B
n-Butylbenzene 59.4 50 14 ug/l SM 6200B
sec-Butylbenzene 50.2 50 14 ug/l SM 6200B
Ethylbenzene 1660 50 15 ug/l SM 6200B
Isopropylbenzene 196 50 12 ug/l SM 6200B
p-Isopropyltoluene 43.5 J 50 12 ug/l SM 6200B
Naphthalene 729 50 12 ug/l SM 6200B
n-Propylbenzene 512 50 16 ug/l SM 6200B
Toluene 1540 50 17 ug/l SM 6200B
1,2,4-Trimethylbenzene 4110 50 14 ug/l SM 6200B
1,3,5-Trimethylbenzene 1410 50 14 ug/l SM 6200B
m,p-Xylene 7110 100 30 ug/l SM 6200B
o-Xylene 2770 50 13 ug/l SM 6200B
Xylene (total)9880 150 43 ug/l SM 6200B
6 of 44
FA22722 2
Accutest Laboratories
Sample Results
Report of Analysis
Southeast
Section 3
7 of 44
FA22722 3
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-21R
Lab Sample ID:FA22722-1 Date Sampled:03/03/15
Matrix:AQ - Ground Water Date Received:03/11/15
Method:SM 6200B Percent Solids:n/a
Project:Handee Hugo 1; US Hwy 87, Reigelwood, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0192950.D 1 03/17/15 TD n/a n/a VA1658
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 3.6 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene 2.6 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene 4.6 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene 0.82 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
8 of 44
FA22722 33.1
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-21R
Lab Sample ID:FA22722-1 Date Sampled:03/03/15
Matrix:AQ - Ground Water Date Received:03/11/15
Method:SM 6200B Percent Solids:n/a
Project:Handee Hugo 1; US Hwy 87, Reigelwood, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene 27.8 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene 6.7 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene 3.6 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene 8.8 0.50 0.12 ug/l
103-65-1 n-Propylbenzene 12.3 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene 0.19 0.50 0.17 ug/l J
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 28.5 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene 0.83 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 7.5 1.0 0.30 ug/l
95-47-6 o-Xylene 0.18 0.50 0.13 ug/l J
1330-20-7 Xylene (total)7.7 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
9 of 44
FA22722 33.1
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-9
Lab Sample ID:FA22722-2 Date Sampled:03/03/15
Matrix:AQ - Ground Water Date Received:03/11/15
Method:SM 6200B Percent Solids:n/a
Project:Handee Hugo 1; US Hwy 87, Reigelwood, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0192971.D 1 03/17/15 TD n/a n/a VA1659
Run #2 A0192934.D 5 03/16/15 TD n/a n/a VA1657
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 0.82 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene 0.60 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene 0.51 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane 0.52 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 44
FA22722 33.2
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-9
Lab Sample ID:FA22722-2 Date Sampled:03/03/15
Matrix:AQ - Ground Water Date Received:03/11/15
Method:SM 6200B Percent Solids:n/a
Project:Handee Hugo 1; US Hwy 87, Reigelwood, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene 30.9 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene 2.6 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene 0.76 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride 0.56 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene 36.7 0.50 0.12 ug/l
103-65-1 n-Propylbenzene 5.1 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene 6.4 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 56.4 a 2.5 0.68 ug/l
108-67-8 1,3,5-Trimethylbenzene 33.8 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 171 a 5.0 1.5 ug/l
95-47-6 o-Xylene 62.5 a 2.5 0.67 ug/l
1330-20-7 Xylene (total)233 a 7.5 2.2 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 105%103%70-130%
17060-07-0 1,2-Dichloroethane-D4 110%105%70-130%
2037-26-5 Toluene-D8 94%96%70-130%
460-00-4 4-Bromofluorobenzene 105%100%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 44
FA22722 33.2
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-8R
Lab Sample ID:FA22722-3 Date Sampled:03/03/15
Matrix:AQ - Ground Water Date Received:03/11/15
Method:SM 6200B Percent Solids:n/a
Project:Handee Hugo 1; US Hwy 87, Reigelwood, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0192935.D 10 03/16/15 TD n/a n/a VA1657
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 5.0 1.7 ug/l
108-86-1 Bromobenzene ND 5.0 1.6 ug/l
74-97-5 Bromochloromethane ND 5.0 1.6 ug/l
75-27-4 Bromodichloromethane ND 5.0 1.5 ug/l
75-25-2 Bromoform ND 5.0 1.1 ug/l
104-51-8 n-Butylbenzene 4.3 5.0 1.4 ug/l J
135-98-8 sec-Butylbenzene 3.5 5.0 1.4 ug/l J
98-06-6 tert-Butylbenzene 1.6 5.0 1.5 ug/l J
56-23-5 Carbon Tetrachloride ND 5.0 1.5 ug/l
108-90-7 Chlorobenzene ND 5.0 1.6 ug/l
75-00-3 Chloroethane ND 5.0 2.1 ug/l
67-66-3 Chloroform ND 5.0 1.7 ug/l
95-49-8 o-Chlorotoluene ND 5.0 1.5 ug/l
106-43-4 p-Chlorotoluene ND 5.0 1.4 ug/l
124-48-1 Dibromochloromethane ND 5.0 1.2 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 5.0 2.0 ug/l
106-93-4 1,2-Dibromoethane ND 5.0 1.4 ug/l
75-71-8 Dichlorodifluoromethane ND 5.0 1.3 ug/l
95-50-1 1,2-Dichlorobenzene ND 5.0 1.3 ug/l
541-73-1 1,3-Dichlorobenzene ND 5.0 1.4 ug/l
106-46-7 1,4-Dichlorobenzene ND 5.0 1.5 ug/l
75-34-3 1,1-Dichloroethane ND 5.0 1.8 ug/l
107-06-2 1,2-Dichloroethane ND 5.0 1.6 ug/l
75-35-4 1,1-Dichloroethylene ND 5.0 1.7 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.8 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.7 ug/l
78-87-5 1,2-Dichloropropane ND 5.0 1.7 ug/l
142-28-9 1,3-Dichloropropane ND 5.0 1.5 ug/l
594-20-7 2,2-Dichloropropane ND 5.0 1.2 ug/l
563-58-6 1,1-Dichloropropene ND 5.0 1.6 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.3 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.3 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 44
FA22722 33.3
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-8R
Lab Sample ID:FA22722-3 Date Sampled:03/03/15
Matrix:AQ - Ground Water Date Received:03/11/15
Method:SM 6200B Percent Solids:n/a
Project:Handee Hugo 1; US Hwy 87, Reigelwood, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 5.0 1.6 ug/l
100-41-4 Ethylbenzene 98.0 5.0 1.5 ug/l
87-68-3 Hexachlorobutadiene ND 5.0 1.2 ug/l
98-82-8 Isopropylbenzene 11.8 5.0 1.2 ug/l
99-87-6 p-Isopropyltoluene 3.5 5.0 1.2 ug/l J
74-83-9 Methyl Bromide ND 5.0 1.8 ug/l
74-87-3 Methyl Chloride ND 5.0 1.6 ug/l
74-95-3 Methylene Bromide ND 5.0 1.7 ug/l
75-09-2 Methylene Chloride ND 20 10 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 5.0 1.6 ug/l
91-20-3 Naphthalene 84.4 5.0 1.2 ug/l
103-65-1 n-Propylbenzene 23.6 5.0 1.6 ug/l
100-42-5 Styrene ND 5.0 1.2 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 5.0 1.3 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 1.4 ug/l
127-18-4 Tetrachloroethylene ND 5.0 1.5 ug/l
108-88-3 Toluene 92.9 5.0 1.7 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 5.0 1.4 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.3 ug/l
71-55-6 1,1,1-Trichloroethane ND 5.0 1.6 ug/l
79-00-5 1,1,2-Trichloroethane ND 5.0 1.4 ug/l
79-01-6 Trichloroethylene ND 5.0 1.5 ug/l
75-69-4 Trichlorofluoromethane ND 5.0 1.6 ug/l
96-18-4 1,2,3-Trichloropropane ND 5.0 1.3 ug/l
95-63-6 1,2,4-Trimethylbenzene 345 5.0 1.4 ug/l
108-67-8 1,3,5-Trimethylbenzene 133 5.0 1.4 ug/l
75-01-4 Vinyl Chloride ND 5.0 1.3 ug/l
m,p-Xylene 595 10 3.0 ug/l
95-47-6 o-Xylene 281 5.0 1.3 ug/l
1330-20-7 Xylene (total)876 15 4.3 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
13 of 44
FA22722 33.3
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-7R
Lab Sample ID:FA22722-4 Date Sampled:03/03/15
Matrix:AQ - Ground Water Date Received:03/11/15
Method:SM 6200B Percent Solids:n/a
Project:Handee Hugo 1; US Hwy 87, Reigelwood, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0192936.D 5 03/16/15 TD n/a n/a VA1657
Run #2 A0192972.D 20 03/17/15 TD n/a n/a VA1659
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 2.5 0.86 ug/l
108-86-1 Bromobenzene ND 2.5 0.80 ug/l
74-97-5 Bromochloromethane ND 2.5 0.80 ug/l
75-27-4 Bromodichloromethane ND 2.5 0.74 ug/l
75-25-2 Bromoform ND 2.5 0.55 ug/l
104-51-8 n-Butylbenzene 3.9 2.5 0.72 ug/l
135-98-8 sec-Butylbenzene 3.1 2.5 0.69 ug/l
98-06-6 tert-Butylbenzene 0.75 2.5 0.73 ug/l J
56-23-5 Carbon Tetrachloride ND 2.5 0.77 ug/l
108-90-7 Chlorobenzene ND 2.5 0.79 ug/l
75-00-3 Chloroethane ND 2.5 1.0 ug/l
67-66-3 Chloroform ND 2.5 0.86 ug/l
95-49-8 o-Chlorotoluene ND 2.5 0.76 ug/l
106-43-4 p-Chlorotoluene ND 2.5 0.69 ug/l
124-48-1 Dibromochloromethane ND 2.5 0.62 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 2.5 0.99 ug/l
106-93-4 1,2-Dibromoethane ND 2.5 0.71 ug/l
75-71-8 Dichlorodifluoromethane ND 2.5 0.65 ug/l
95-50-1 1,2-Dichlorobenzene ND 2.5 0.65 ug/l
541-73-1 1,3-Dichlorobenzene ND 2.5 0.70 ug/l
106-46-7 1,4-Dichlorobenzene ND 2.5 0.76 ug/l
75-34-3 1,1-Dichloroethane ND 2.5 0.91 ug/l
107-06-2 1,2-Dichloroethane ND 2.5 0.82 ug/l
75-35-4 1,1-Dichloroethylene ND 2.5 0.85 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 2.5 0.90 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 2.5 0.85 ug/l
78-87-5 1,2-Dichloropropane ND 2.5 0.87 ug/l
142-28-9 1,3-Dichloropropane ND 2.5 0.73 ug/l
594-20-7 2,2-Dichloropropane ND 2.5 0.61 ug/l
563-58-6 1,1-Dichloropropene ND 2.5 0.79 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 2.5 0.66 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 2.5 0.63 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
14 of 44
FA22722 33.4
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-7R
Lab Sample ID:FA22722-4 Date Sampled:03/03/15
Matrix:AQ - Ground Water Date Received:03/11/15
Method:SM 6200B Percent Solids:n/a
Project:Handee Hugo 1; US Hwy 87, Reigelwood, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 2.5 0.80 ug/l
100-41-4 Ethylbenzene 92.4 2.5 0.76 ug/l
87-68-3 Hexachlorobutadiene ND 2.5 0.61 ug/l
98-82-8 Isopropylbenzene 14.8 2.5 0.59 ug/l
99-87-6 p-Isopropyltoluene 2.7 2.5 0.61 ug/l
74-83-9 Methyl Bromide ND 2.5 0.91 ug/l
74-87-3 Methyl Chloride ND 2.5 0.79 ug/l
74-95-3 Methylene Bromide ND 2.5 0.85 ug/l
75-09-2 Methylene Chloride ND 10 5.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 2.5 0.82 ug/l
91-20-3 Naphthalene 98.9 2.5 0.61 ug/l
103-65-1 n-Propylbenzene 34.4 2.5 0.78 ug/l
100-42-5 Styrene ND 2.5 0.60 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 2.5 0.63 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 2.5 0.71 ug/l
127-18-4 Tetrachloroethylene ND 2.5 0.74 ug/l
108-88-3 Toluene 22.4 2.5 0.83 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 2.5 0.68 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 2.5 0.65 ug/l
71-55-6 1,1,1-Trichloroethane ND 2.5 0.81 ug/l
79-00-5 1,1,2-Trichloroethane ND 2.5 0.70 ug/l
79-01-6 Trichloroethylene ND 2.5 0.73 ug/l
75-69-4 Trichlorofluoromethane ND 2.5 0.81 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.5 0.64 ug/l
95-63-6 1,2,4-Trimethylbenzene 396 a 10 2.7 ug/l
108-67-8 1,3,5-Trimethylbenzene 162 2.5 0.68 ug/l
75-01-4 Vinyl Chloride ND 2.5 0.65 ug/l
m,p-Xylene 724 a 20 5.9 ug/l
95-47-6 o-Xylene 411 a 10 2.7 ug/l
1330-20-7 Xylene (total)1140 a 30 8.6 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 99%101%70-130%
17060-07-0 1,2-Dichloroethane-D4 101%104%70-130%
2037-26-5 Toluene-D8 100%98%70-130%
460-00-4 4-Bromofluorobenzene 102%99%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
15 of 44
FA22722 33.4
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-5R
Lab Sample ID:FA22722-5 Date Sampled:03/03/15
Matrix:AQ - Ground Water Date Received:03/11/15
Method:SM 6200B Percent Solids:n/a
Project:Handee Hugo 1; US Hwy 87, Reigelwood, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0192937.D 5 03/16/15 TD n/a n/a VA1657
Run #2 A0192976.D 50 03/17/15 TD n/a n/a VA1659
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 2180 a 25 8.6 ug/l
108-86-1 Bromobenzene ND 2.5 0.80 ug/l
74-97-5 Bromochloromethane ND 2.5 0.80 ug/l
75-27-4 Bromodichloromethane ND 2.5 0.74 ug/l
75-25-2 Bromoform ND 2.5 0.55 ug/l
104-51-8 n-Butylbenzene 38.7 2.5 0.72 ug/l
135-98-8 sec-Butylbenzene 29.2 2.5 0.69 ug/l
98-06-6 tert-Butylbenzene 4.0 2.5 0.73 ug/l
56-23-5 Carbon Tetrachloride ND 2.5 0.77 ug/l
108-90-7 Chlorobenzene ND 2.5 0.79 ug/l
75-00-3 Chloroethane 14.0 2.5 1.0 ug/l
67-66-3 Chloroform ND 2.5 0.86 ug/l
95-49-8 o-Chlorotoluene ND 2.5 0.76 ug/l
106-43-4 p-Chlorotoluene ND 2.5 0.69 ug/l
124-48-1 Dibromochloromethane ND 2.5 0.62 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 2.5 0.99 ug/l
106-93-4 1,2-Dibromoethane ND 2.5 0.71 ug/l
75-71-8 Dichlorodifluoromethane ND 2.5 0.65 ug/l
95-50-1 1,2-Dichlorobenzene ND 2.5 0.65 ug/l
541-73-1 1,3-Dichlorobenzene ND 2.5 0.70 ug/l
106-46-7 1,4-Dichlorobenzene ND 2.5 0.76 ug/l
75-34-3 1,1-Dichloroethane ND 2.5 0.91 ug/l
107-06-2 1,2-Dichloroethane ND 2.5 0.82 ug/l
75-35-4 1,1-Dichloroethylene ND 2.5 0.85 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 2.5 0.90 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 2.5 0.85 ug/l
78-87-5 1,2-Dichloropropane ND 2.5 0.87 ug/l
142-28-9 1,3-Dichloropropane ND 2.5 0.73 ug/l
594-20-7 2,2-Dichloropropane ND 2.5 0.61 ug/l
563-58-6 1,1-Dichloropropene ND 2.5 0.79 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 2.5 0.66 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 2.5 0.63 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
16 of 44
FA22722 33.5
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-5R
Lab Sample ID:FA22722-5 Date Sampled:03/03/15
Matrix:AQ - Ground Water Date Received:03/11/15
Method:SM 6200B Percent Solids:n/a
Project:Handee Hugo 1; US Hwy 87, Reigelwood, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 2.5 0.80 ug/l
100-41-4 Ethylbenzene 2200 a 25 7.6 ug/l
87-68-3 Hexachlorobutadiene ND 2.5 0.61 ug/l
98-82-8 Isopropylbenzene 196 2.5 0.59 ug/l
99-87-6 p-Isopropyltoluene 17.0 2.5 0.61 ug/l
74-83-9 Methyl Bromide ND 2.5 0.91 ug/l
74-87-3 Methyl Chloride 8.6 2.5 0.79 ug/l
74-95-3 Methylene Bromide ND 2.5 0.85 ug/l
75-09-2 Methylene Chloride ND 10 5.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 4.2 2.5 0.82 ug/l
91-20-3 Naphthalene 653 a 25 6.1 ug/l
103-65-1 n-Propylbenzene 430 a 25 7.8 ug/l
100-42-5 Styrene ND 2.5 0.60 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 2.5 0.63 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 2.5 0.71 ug/l
127-18-4 Tetrachloroethylene ND 2.5 0.74 ug/l
108-88-3 Toluene 36.8 2.5 0.83 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 2.5 0.68 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 2.5 0.65 ug/l
71-55-6 1,1,1-Trichloroethane ND 2.5 0.81 ug/l
79-00-5 1,1,2-Trichloroethane ND 2.5 0.70 ug/l
79-01-6 Trichloroethylene ND 2.5 0.73 ug/l
75-69-4 Trichlorofluoromethane ND 2.5 0.81 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.5 0.64 ug/l
95-63-6 1,2,4-Trimethylbenzene 2290 a 25 6.8 ug/l
108-67-8 1,3,5-Trimethylbenzene 119 2.5 0.68 ug/l
75-01-4 Vinyl Chloride ND 2.5 0.65 ug/l
m,p-Xylene 305 5.0 1.5 ug/l
95-47-6 o-Xylene 4.0 2.5 0.67 ug/l
1330-20-7 Xylene (total)310 7.5 2.2 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 115%99%70-130%
17060-07-0 1,2-Dichloroethane-D4 122%104%70-130%
2037-26-5 Toluene-D8 101%99%70-130%
460-00-4 4-Bromofluorobenzene 102%99%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
17 of 44
FA22722 33.5
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-18R
Lab Sample ID:FA22722-6 Date Sampled:03/03/15
Matrix:AQ - Ground Water Date Received:03/11/15
Method:SM 6200B Percent Solids:n/a
Project:Handee Hugo 1; US Hwy 87, Reigelwood, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0192938.D 5 03/16/15 TD n/a n/a VA1657
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 144 2.5 0.86 ug/l
108-86-1 Bromobenzene ND 2.5 0.80 ug/l
74-97-5 Bromochloromethane ND 2.5 0.80 ug/l
75-27-4 Bromodichloromethane ND 2.5 0.74 ug/l
75-25-2 Bromoform ND 2.5 0.55 ug/l
104-51-8 n-Butylbenzene 5.2 2.5 0.72 ug/l
135-98-8 sec-Butylbenzene 5.4 2.5 0.69 ug/l
98-06-6 tert-Butylbenzene ND 2.5 0.73 ug/l
56-23-5 Carbon Tetrachloride ND 2.5 0.77 ug/l
108-90-7 Chlorobenzene ND 2.5 0.79 ug/l
75-00-3 Chloroethane 3.2 2.5 1.0 ug/l
67-66-3 Chloroform ND 2.5 0.86 ug/l
95-49-8 o-Chlorotoluene ND 2.5 0.76 ug/l
106-43-4 p-Chlorotoluene ND 2.5 0.69 ug/l
124-48-1 Dibromochloromethane ND 2.5 0.62 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 2.5 0.99 ug/l
106-93-4 1,2-Dibromoethane ND 2.5 0.71 ug/l
75-71-8 Dichlorodifluoromethane ND 2.5 0.65 ug/l
95-50-1 1,2-Dichlorobenzene ND 2.5 0.65 ug/l
541-73-1 1,3-Dichlorobenzene ND 2.5 0.70 ug/l
106-46-7 1,4-Dichlorobenzene ND 2.5 0.76 ug/l
75-34-3 1,1-Dichloroethane ND 2.5 0.91 ug/l
107-06-2 1,2-Dichloroethane ND 2.5 0.82 ug/l
75-35-4 1,1-Dichloroethylene ND 2.5 0.85 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 2.5 0.90 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 2.5 0.85 ug/l
78-87-5 1,2-Dichloropropane ND 2.5 0.87 ug/l
142-28-9 1,3-Dichloropropane ND 2.5 0.73 ug/l
594-20-7 2,2-Dichloropropane ND 2.5 0.61 ug/l
563-58-6 1,1-Dichloropropene ND 2.5 0.79 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 2.5 0.66 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 2.5 0.63 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
18 of 44
FA22722 33.6
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-18R
Lab Sample ID:FA22722-6 Date Sampled:03/03/15
Matrix:AQ - Ground Water Date Received:03/11/15
Method:SM 6200B Percent Solids:n/a
Project:Handee Hugo 1; US Hwy 87, Reigelwood, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 2.5 0.80 ug/l
100-41-4 Ethylbenzene 13.1 2.5 0.76 ug/l
87-68-3 Hexachlorobutadiene ND 2.5 0.61 ug/l
98-82-8 Isopropylbenzene 31.1 2.5 0.59 ug/l
99-87-6 p-Isopropyltoluene ND 2.5 0.61 ug/l
74-83-9 Methyl Bromide ND 2.5 0.91 ug/l
74-87-3 Methyl Chloride 2.4 2.5 0.79 ug/l J
74-95-3 Methylene Bromide ND 2.5 0.85 ug/l
75-09-2 Methylene Chloride ND 10 5.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 1.2 2.5 0.82 ug/l J
91-20-3 Naphthalene 7.0 2.5 0.61 ug/l
103-65-1 n-Propylbenzene 68.6 2.5 0.78 ug/l
100-42-5 Styrene ND 2.5 0.60 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 2.5 0.63 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 2.5 0.71 ug/l
127-18-4 Tetrachloroethylene ND 2.5 0.74 ug/l
108-88-3 Toluene 4.5 2.5 0.83 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 2.5 0.68 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 2.5 0.65 ug/l
71-55-6 1,1,1-Trichloroethane ND 2.5 0.81 ug/l
79-00-5 1,1,2-Trichloroethane ND 2.5 0.70 ug/l
79-01-6 Trichloroethylene ND 2.5 0.73 ug/l
75-69-4 Trichlorofluoromethane ND 2.5 0.81 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.5 0.64 ug/l
95-63-6 1,2,4-Trimethylbenzene 3.0 2.5 0.68 ug/l
108-67-8 1,3,5-Trimethylbenzene 0.70 2.5 0.68 ug/l J
75-01-4 Vinyl Chloride ND 2.5 0.65 ug/l
m,p-Xylene 2.5 5.0 1.5 ug/l J
95-47-6 o-Xylene ND 2.5 0.67 ug/l
1330-20-7 Xylene (total)2.5 7.5 2.2 ug/l J
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 121%70-130%
17060-07-0 1,2-Dichloroethane-D4 122%70-130%
2037-26-5 Toluene-D8 95%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
19 of 44
FA22722 33.6
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-17R
Lab Sample ID:FA22722-7 Date Sampled:03/03/15
Matrix:AQ - Ground Water Date Received:03/11/15
Method:SM 6200B Percent Solids:n/a
Project:Handee Hugo 1; US Hwy 87, Reigelwood, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0192973.D 100 03/17/15 TD n/a n/a VA1659
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 654 50 17 ug/l
108-86-1 Bromobenzene ND 50 16 ug/l
74-97-5 Bromochloromethane ND 50 16 ug/l
75-27-4 Bromodichloromethane ND 50 15 ug/l
75-25-2 Bromoform ND 50 11 ug/l
104-51-8 n-Butylbenzene 59.4 50 14 ug/l
135-98-8 sec-Butylbenzene 50.2 50 14 ug/l
98-06-6 tert-Butylbenzene ND 50 15 ug/l
56-23-5 Carbon Tetrachloride ND 50 15 ug/l
108-90-7 Chlorobenzene ND 50 16 ug/l
75-00-3 Chloroethane ND 50 21 ug/l
67-66-3 Chloroform ND 50 17 ug/l
95-49-8 o-Chlorotoluene ND 50 15 ug/l
106-43-4 p-Chlorotoluene ND 50 14 ug/l
124-48-1 Dibromochloromethane ND 50 12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 50 20 ug/l
106-93-4 1,2-Dibromoethane ND 50 14 ug/l
75-71-8 Dichlorodifluoromethane ND 50 13 ug/l
95-50-1 1,2-Dichlorobenzene ND 50 13 ug/l
541-73-1 1,3-Dichlorobenzene ND 50 14 ug/l
106-46-7 1,4-Dichlorobenzene ND 50 15 ug/l
75-34-3 1,1-Dichloroethane ND 50 18 ug/l
107-06-2 1,2-Dichloroethane ND 50 16 ug/l
75-35-4 1,1-Dichloroethylene ND 50 17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 50 18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 50 17 ug/l
78-87-5 1,2-Dichloropropane ND 50 17 ug/l
142-28-9 1,3-Dichloropropane ND 50 15 ug/l
594-20-7 2,2-Dichloropropane ND 50 12 ug/l
563-58-6 1,1-Dichloropropene ND 50 16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 50 13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 50 13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
20 of 44
FA22722 33.7
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-17R
Lab Sample ID:FA22722-7 Date Sampled:03/03/15
Matrix:AQ - Ground Water Date Received:03/11/15
Method:SM 6200B Percent Solids:n/a
Project:Handee Hugo 1; US Hwy 87, Reigelwood, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 50 16 ug/l
100-41-4 Ethylbenzene 1660 50 15 ug/l
87-68-3 Hexachlorobutadiene ND 50 12 ug/l
98-82-8 Isopropylbenzene 196 50 12 ug/l
99-87-6 p-Isopropyltoluene 43.5 50 12 ug/l J
74-83-9 Methyl Bromide ND 50 18 ug/l
74-87-3 Methyl Chloride ND 50 16 ug/l
74-95-3 Methylene Bromide ND 50 17 ug/l
75-09-2 Methylene Chloride ND 200 100 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 50 16 ug/l
91-20-3 Naphthalene 729 50 12 ug/l
103-65-1 n-Propylbenzene 512 50 16 ug/l
100-42-5 Styrene ND 50 12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 50 13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 50 14 ug/l
127-18-4 Tetrachloroethylene ND 50 15 ug/l
108-88-3 Toluene 1540 50 17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 50 14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 50 13 ug/l
71-55-6 1,1,1-Trichloroethane ND 50 16 ug/l
79-00-5 1,1,2-Trichloroethane ND 50 14 ug/l
79-01-6 Trichloroethylene ND 50 15 ug/l
75-69-4 Trichlorofluoromethane ND 50 16 ug/l
96-18-4 1,2,3-Trichloropropane ND 50 13 ug/l
95-63-6 1,2,4-Trimethylbenzene 4110 50 14 ug/l
108-67-8 1,3,5-Trimethylbenzene 1410 50 14 ug/l
75-01-4 Vinyl Chloride ND 50 13 ug/l
m,p-Xylene 7110 100 30 ug/l
95-47-6 o-Xylene 2770 50 13 ug/l
1330-20-7 Xylene (total)9880 150 43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
21 of 44
FA22722 33.7
Accutest Laboratories
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Southeast
Section 4
22 of 44
FA22722 4
FA22722: Chain of Custody
Page 1 of 3
23 of 44
FA22722 44.1
FA22722: Chain of Custody
Page 2 of 3
24 of 44
FA22722 44.1
FA22722: Chain of Custody
Page 3 of 3
25 of 44
FA22722 44.1
Accutest Laboratories
GC/MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Southeast
Section 5
26 of 44
FA22722 5
Method Blank Summary Page 1 of 2
Job Number:FA22722
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 1; US Hwy 87, Reigelwood, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1657-MB A0192916.D 1 03/16/15 TD n/a n/a VA1657
The QC reported here applies to the following samples:Method: SM 6200B
FA22722-2, FA22722-3, FA22722-4, FA22722-5, FA22722-6
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
27 of 44
FA22722 55.1.1
Method Blank Summary Page 2 of 2
Job Number:FA22722
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 1; US Hwy 87, Reigelwood, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1657-MB A0192916.D 1 03/16/15 TD n/a n/a VA1657
The QC reported here applies to the following samples:Method: SM 6200B
FA22722-2, FA22722-3, FA22722-4, FA22722-5, FA22722-6
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
28 of 44
FA22722 55.1.1
Method Blank Summary Page 1 of 2
Job Number:FA22722
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 1; US Hwy 87, Reigelwood, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1658-MB A0192946.D 1 03/17/15 TD n/a n/a VA1658
The QC reported here applies to the following samples:Method: SM 6200B
FA22722-1
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
29 of 44
FA22722 55.1.2
Method Blank Summary Page 2 of 2
Job Number:FA22722
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 1; US Hwy 87, Reigelwood, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1658-MB A0192946.D 1 03/17/15 TD n/a n/a VA1658
The QC reported here applies to the following samples:Method: SM 6200B
FA22722-1
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 101%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
30 of 44
FA22722 55.1.2
Method Blank Summary Page 1 of 2
Job Number:FA22722
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 1; US Hwy 87, Reigelwood, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1659-MB A0192964.D 1 03/17/15 TD n/a n/a VA1659
The QC reported here applies to the following samples:Method: SM 6200B
FA22722-2, FA22722-4, FA22722-5, FA22722-7
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
31 of 44
FA22722 55.1.3
Method Blank Summary Page 2 of 2
Job Number:FA22722
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 1; US Hwy 87, Reigelwood, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1659-MB A0192964.D 1 03/17/15 TD n/a n/a VA1659
The QC reported here applies to the following samples:Method: SM 6200B
FA22722-2, FA22722-4, FA22722-5, FA22722-7
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 107%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
32 of 44
FA22722 55.1.3
Blank Spike Summary Page 1 of 2
Job Number:FA22722
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 1; US Hwy 87, Reigelwood, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1657-BS A0192917.D 1 03/16/15 TD n/a n/a VA1657
The QC reported here applies to the following samples:Method: SM 6200B
FA22722-2, FA22722-3, FA22722-4, FA22722-5, FA22722-6
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 10.3 103 70-130
108-86-1 Bromobenzene 10 10.2 102 70-130
74-97-5 Bromochloromethane 10 9.7 97 70-130
75-27-4 Bromodichloromethane 10 10.6 106 70-130
75-25-2 Bromoform 10 10.3 103 70-130
104-51-8 n-Butylbenzene 10 10.3 103 70-130
135-98-8 sec-Butylbenzene 10 11.4 114 70-130
98-06-6 tert-Butylbenzene 10 11.2 112 70-130
56-23-5 Carbon Tetrachloride 10 10.8 108 70-130
108-90-7 Chlorobenzene 10 10.9 109 70-130
75-00-3 Chloroethane 10 11.2 112 60-140
67-66-3 Chloroform 10 10.4 104 70-130
95-49-8 o-Chlorotoluene 10 10.9 109 70-130
106-43-4 p-Chlorotoluene 10 11.2 112 70-130
124-48-1 Dibromochloromethane 10 10.7 107 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 9.0 90 70-130
106-93-4 1,2-Dibromoethane 10 10.1 101 70-130
75-71-8 Dichlorodifluoromethane 10 9.0 90 60-140
95-50-1 1,2-Dichlorobenzene 10 10.8 108 70-130
541-73-1 1,3-Dichlorobenzene 10 11.2 112 70-130
106-46-7 1,4-Dichlorobenzene 10 10.1 101 70-130
75-34-3 1,1-Dichloroethane 10 10.3 103 70-130
107-06-2 1,2-Dichloroethane 10 10.3 103 70-130
75-35-4 1,1-Dichloroethylene 10 11.0 110 70-130
156-59-2 cis-1,2-Dichloroethylene 10 10.5 105 70-130
156-60-5 trans-1,2-Dichloroethylene 10 10.4 104 70-130
78-87-5 1,2-Dichloropropane 10 10.3 103 70-130
142-28-9 1,3-Dichloropropane 10 10.0 100 70-130
594-20-7 2,2-Dichloropropane 10 10.3 103 70-130
563-58-6 1,1-Dichloropropene 10 11.1 111 70-130
10061-01-5 cis-1,3-Dichloropropene 10 10.0 100 70-130
10061-02-6 trans-1,3-Dichloropropene 10 10.6 106 70-130
108-20-3 Di-Isopropyl Ether 10 9.4 94 70-130
100-41-4 Ethylbenzene 10 10.3 103 70-130
87-68-3 Hexachlorobutadiene 10 10.6 106 70-130
98-82-8 Isopropylbenzene 10 11.1 111 70-130
* = Outside of Control Limits.
33 of 44
FA22722 55.2.1
Blank Spike Summary Page 2 of 2
Job Number:FA22722
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 1; US Hwy 87, Reigelwood, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1657-BS A0192917.D 1 03/16/15 TD n/a n/a VA1657
The QC reported here applies to the following samples:Method: SM 6200B
FA22722-2, FA22722-3, FA22722-4, FA22722-5, FA22722-6
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 11.1 111 70-130
74-83-9 Methyl Bromide 10 10.7 107 60-140
74-87-3 Methyl Chloride 10 10.3 103 60-140
74-95-3 Methylene Bromide 10 10.5 105 70-130
75-09-2 Methylene Chloride 10 9.2 92 70-130
1634-04-4 Methyl Tert Butyl Ether 10 9.5 95 70-130
91-20-3 Naphthalene 10 9.2 92 70-130
103-65-1 n-Propylbenzene 10 11.5 115 70-130
100-42-5 Styrene 10 10.1 101 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 10.4 104 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 9.6 96 70-130
127-18-4 Tetrachloroethylene 10 11.2 112 70-130
108-88-3 Toluene 10 10.2 102 70-130
87-61-6 1,2,3-Trichlorobenzene 10 9.6 96 70-130
120-82-1 1,2,4-Trichlorobenzene 10 9.8 98 70-130
71-55-6 1,1,1-Trichloroethane 10 10.4 104 70-130
79-00-5 1,1,2-Trichloroethane 10 10.2 102 70-130
79-01-6 Trichloroethylene 10 10.9 109 70-130
75-69-4 Trichlorofluoromethane 10 9.8 98 60-140
96-18-4 1,2,3-Trichloropropane 10 9.8 98 70-130
95-63-6 1,2,4-Trimethylbenzene 10 10 100 70-130
108-67-8 1,3,5-Trimethylbenzene 10 10.2 102 70-130
75-01-4 Vinyl Chloride 10 9.8 98 60-140
m,p-Xylene 20 21.2 106 70-130
95-47-6 o-Xylene 10 11.0 110 70-130
1330-20-7 Xylene (total)30 32.2 107 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 101%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
* = Outside of Control Limits.
34 of 44
FA22722 55.2.1
Blank Spike Summary Page 1 of 2
Job Number:FA22722
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 1; US Hwy 87, Reigelwood, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1658-BS A0192947.D 1 03/17/15 TD n/a n/a VA1658
The QC reported here applies to the following samples:Method: SM 6200B
FA22722-1
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 10.2 102 70-130
108-86-1 Bromobenzene 10 10.2 102 70-130
74-97-5 Bromochloromethane 10 9.6 96 70-130
75-27-4 Bromodichloromethane 10 10.4 104 70-130
75-25-2 Bromoform 10 10.3 103 70-130
104-51-8 n-Butylbenzene 10 10.3 103 70-130
135-98-8 sec-Butylbenzene 10 11.4 114 70-130
98-06-6 tert-Butylbenzene 10 11.3 113 70-130
56-23-5 Carbon Tetrachloride 10 10.7 107 70-130
108-90-7 Chlorobenzene 10 10.9 109 70-130
75-00-3 Chloroethane 10 13.2 132 60-140
67-66-3 Chloroform 10 10.6 106 70-130
95-49-8 o-Chlorotoluene 10 10.9 109 70-130
106-43-4 p-Chlorotoluene 10 11.2 112 70-130
124-48-1 Dibromochloromethane 10 10.5 105 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 9.7 97 70-130
106-93-4 1,2-Dibromoethane 10 10.1 101 70-130
75-71-8 Dichlorodifluoromethane 10 12.8 128 60-140
95-50-1 1,2-Dichlorobenzene 10 10.8 108 70-130
541-73-1 1,3-Dichlorobenzene 10 11.2 112 70-130
106-46-7 1,4-Dichlorobenzene 10 10.2 102 70-130
75-34-3 1,1-Dichloroethane 10 10.2 102 70-130
107-06-2 1,2-Dichloroethane 10 10.1 101 70-130
75-35-4 1,1-Dichloroethylene 10 10.7 107 70-130
156-59-2 cis-1,2-Dichloroethylene 10 10.4 104 70-130
156-60-5 trans-1,2-Dichloroethylene 10 10.3 103 70-130
78-87-5 1,2-Dichloropropane 10 10.2 102 70-130
142-28-9 1,3-Dichloropropane 10 9.9 99 70-130
594-20-7 2,2-Dichloropropane 10 10.4 104 70-130
563-58-6 1,1-Dichloropropene 10 11.1 111 70-130
10061-01-5 cis-1,3-Dichloropropene 10 10.0 100 70-130
10061-02-6 trans-1,3-Dichloropropene 10 10.5 105 70-130
108-20-3 Di-Isopropyl Ether 10 9.2 92 70-130
100-41-4 Ethylbenzene 10 10.2 102 70-130
87-68-3 Hexachlorobutadiene 10 10.6 106 70-130
98-82-8 Isopropylbenzene 10 11.0 110 70-130
* = Outside of Control Limits.
35 of 44
FA22722 55.2.2
Blank Spike Summary Page 2 of 2
Job Number:FA22722
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 1; US Hwy 87, Reigelwood, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1658-BS A0192947.D 1 03/17/15 TD n/a n/a VA1658
The QC reported here applies to the following samples:Method: SM 6200B
FA22722-1
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 11.2 112 70-130
74-83-9 Methyl Bromide 10 12.8 128 60-140
74-87-3 Methyl Chloride 10 12.7 127 60-140
74-95-3 Methylene Bromide 10 10.3 103 70-130
75-09-2 Methylene Chloride 10 9.4 94 70-130
1634-04-4 Methyl Tert Butyl Ether 10 9.2 92 70-130
91-20-3 Naphthalene 10 9.3 93 70-130
103-65-1 n-Propylbenzene 10 11.4 114 70-130
100-42-5 Styrene 10 9.9 99 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 10.4 104 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 9.7 97 70-130
127-18-4 Tetrachloroethylene 10 11.1 111 70-130
108-88-3 Toluene 10 10.1 101 70-130
87-61-6 1,2,3-Trichlorobenzene 10 9.8 98 70-130
120-82-1 1,2,4-Trichlorobenzene 10 9.9 99 70-130
71-55-6 1,1,1-Trichloroethane 10 10.3 103 70-130
79-00-5 1,1,2-Trichloroethane 10 9.9 99 70-130
79-01-6 Trichloroethylene 10 10.7 107 70-130
75-69-4 Trichlorofluoromethane 10 11.7 117 60-140
96-18-4 1,2,3-Trichloropropane 10 9.8 98 70-130
95-63-6 1,2,4-Trimethylbenzene 10 10.1 101 70-130
108-67-8 1,3,5-Trimethylbenzene 10 10.2 102 70-130
75-01-4 Vinyl Chloride 10 12.2 122 60-140
m,p-Xylene 20 21.0 105 70-130
95-47-6 o-Xylene 10 10.8 108 70-130
1330-20-7 Xylene (total)30 31.7 106 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
* = Outside of Control Limits.
36 of 44
FA22722 55.2.2
Blank Spike Summary Page 1 of 2
Job Number:FA22722
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 1; US Hwy 87, Reigelwood, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1659-BS A0192965.D 1 03/17/15 TD n/a n/a VA1659
The QC reported here applies to the following samples:Method: SM 6200B
FA22722-2, FA22722-4, FA22722-5, FA22722-7
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 9.0 90 70-130
108-86-1 Bromobenzene 10 8.9 89 70-130
74-97-5 Bromochloromethane 10 8.4 84 70-130
75-27-4 Bromodichloromethane 10 9.5 95 70-130
75-25-2 Bromoform 10 9.0 90 70-130
104-51-8 n-Butylbenzene 10 8.9 89 70-130
135-98-8 sec-Butylbenzene 10 9.9 99 70-130
98-06-6 tert-Butylbenzene 10 9.7 97 70-130
56-23-5 Carbon Tetrachloride 10 9.8 98 70-130
108-90-7 Chlorobenzene 10 9.6 96 70-130
75-00-3 Chloroethane 10 10.4 104 60-140
67-66-3 Chloroform 10 9.4 94 70-130
95-49-8 o-Chlorotoluene 10 9.5 95 70-130
106-43-4 p-Chlorotoluene 10 9.7 97 70-130
124-48-1 Dibromochloromethane 10 9.3 93 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 8.1 81 70-130
106-93-4 1,2-Dibromoethane 10 8.7 87 70-130
75-71-8 Dichlorodifluoromethane 10 10.7 107 60-140
95-50-1 1,2-Dichlorobenzene 10 9.5 95 70-130
541-73-1 1,3-Dichlorobenzene 10 9.8 98 70-130
106-46-7 1,4-Dichlorobenzene 10 8.8 88 70-130
75-34-3 1,1-Dichloroethane 10 9.0 90 70-130
107-06-2 1,2-Dichloroethane 10 9.5 95 70-130
75-35-4 1,1-Dichloroethylene 10 9.6 96 70-130
156-59-2 cis-1,2-Dichloroethylene 10 9.2 92 70-130
156-60-5 trans-1,2-Dichloroethylene 10 9.1 91 70-130
78-87-5 1,2-Dichloropropane 10 9.0 90 70-130
142-28-9 1,3-Dichloropropane 10 8.8 88 70-130
594-20-7 2,2-Dichloropropane 10 9.2 92 70-130
563-58-6 1,1-Dichloropropene 10 9.8 98 70-130
10061-01-5 cis-1,3-Dichloropropene 10 8.7 87 70-130
10061-02-6 trans-1,3-Dichloropropene 10 9.2 92 70-130
108-20-3 Di-Isopropyl Ether 10 8.4 84 70-130
100-41-4 Ethylbenzene 10 8.9 89 70-130
87-68-3 Hexachlorobutadiene 10 9.2 92 70-130
98-82-8 Isopropylbenzene 10 9.6 96 70-130
* = Outside of Control Limits.
37 of 44
FA22722 55.2.3
Blank Spike Summary Page 2 of 2
Job Number:FA22722
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 1; US Hwy 87, Reigelwood, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1659-BS A0192965.D 1 03/17/15 TD n/a n/a VA1659
The QC reported here applies to the following samples:Method: SM 6200B
FA22722-2, FA22722-4, FA22722-5, FA22722-7
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 9.6 96 70-130
74-83-9 Methyl Bromide 10 10.4 104 60-140
74-87-3 Methyl Chloride 10 10.9 109 60-140
74-95-3 Methylene Bromide 10 9.3 93 70-130
75-09-2 Methylene Chloride 10 8.7 87 70-130
1634-04-4 Methyl Tert Butyl Ether 10 8.4 84 70-130
91-20-3 Naphthalene 10 8.0 80 70-130
103-65-1 n-Propylbenzene 10 9.9 99 70-130
100-42-5 Styrene 10 8.5 85 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 9.3 93 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 8.5 85 70-130
127-18-4 Tetrachloroethylene 10 9.7 97 70-130
108-88-3 Toluene 10 8.8 88 70-130
87-61-6 1,2,3-Trichlorobenzene 10 8.7 87 70-130
120-82-1 1,2,4-Trichlorobenzene 10 8.6 86 70-130
71-55-6 1,1,1-Trichloroethane 10 9.4 94 70-130
79-00-5 1,1,2-Trichloroethane 10 8.8 88 70-130
79-01-6 Trichloroethylene 10 9.7 97 70-130
75-69-4 Trichlorofluoromethane 10 9.7 97 60-140
96-18-4 1,2,3-Trichloropropane 10 8.5 85 70-130
95-63-6 1,2,4-Trimethylbenzene 10 8.6 86 70-130
108-67-8 1,3,5-Trimethylbenzene 10 8.8 88 70-130
75-01-4 Vinyl Chloride 10 9.8 98 60-140
m,p-Xylene 20 18.4 92 70-130
95-47-6 o-Xylene 10 9.4 94 70-130
1330-20-7 Xylene (total)30 27.9 93 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 105%70-130%
17060-07-0 1,2-Dichloroethane-D4 108%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
* = Outside of Control Limits.
38 of 44
FA22722 55.2.3
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA22722
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 1; US Hwy 87, Reigelwood, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA22594-12MS A0192925.D 1 03/16/15 TD n/a n/a VA1657
FA22594-12MSD A0192926.D 1 03/16/15 TD n/a n/a VA1657
FA22594-12 A0192918.D 1 03/16/15 TD n/a n/a VA1657
The QC reported here applies to the following samples:Method: SM 6200B
FA22722-2, FA22722-3, FA22722-4, FA22722-5, FA22722-6
FA22594-12 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene ND 10 9.4 94 10 8.2 82 14 70-130/20
108-86-1 Bromobenzene ND 10 10.3 103 10 9.2 92 11 70-130/20
74-97-5 Bromochloromethane ND 10 9.2 92 10 8.0 80 14 70-130/20
75-27-4 Bromodichloromethane ND 10 10.0 100 10 9.0 90 11 70-130/20
75-25-2 Bromoform ND 10 9.6 96 10 8.9 89 8 70-130/20
104-51-8 n-Butylbenzene ND 10 10.5 105 10 9.3 93 12 70-130/20
135-98-8 sec-Butylbenzene ND 10 11.5 115 10 10.3 103 11 70-130/20
98-06-6 tert-Butylbenzene ND 10 11.3 113 10 10.0 100 12 70-130/20
56-23-5 Carbon Tetrachloride ND 10 9.5 95 10 8.4 84 12 70-130/20
108-90-7 Chlorobenzene ND 10 10.7 107 10 9.6 96 11 70-130/20
75-00-3 Chloroethane ND 10 10.7 107 10 8.9 89 18 60-140/20
67-66-3 Chloroform ND 10 9.7 97 10 8.5 85 13 70-130/20
95-49-8 o-Chlorotoluene ND 10 11.0 110 10 9.7 97 13 70-130/20
106-43-4 p-Chlorotoluene ND 10 11.4 114 10 10.1 101 12 70-130/20
124-48-1 Dibromochloromethane ND 10 10.1 101 10 9.1 91 10 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 10 9.6 96 10 8.9 89 8 70-130/20
106-93-4 1,2-Dibromoethane ND 10 9.8 98 10 9.0 90 9 70-130/20
75-71-8 Dichlorodifluoromethane ND 10 9.7 97 10 8.6 86 12 60-140/20
95-50-1 1,2-Dichlorobenzene ND 10 11.1 111 10 10.1 101 9 70-130/20
541-73-1 1,3-Dichlorobenzene ND 10 11.3 113 10 10.1 101 11 70-130/20
106-46-7 1,4-Dichlorobenzene ND 10 10.3 103 10 9.2 92 11 70-130/20
75-34-3 1,1-Dichloroethane ND 10 9.1 91 10 7.9 79 14 70-130/20
107-06-2 1,2-Dichloroethane ND 10 9.5 95 10 8.5 85 11 70-130/20
75-35-4 1,1-Dichloroethylene ND 10 8.8 88 10 7.7 77 13 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 10 9.6 96 10 8.4 84 13 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 10 9.0 90 10 7.8 78 14 70-130/20
78-87-5 1,2-Dichloropropane ND 10 9.8 98 10 8.8 88 11 70-130/20
142-28-9 1,3-Dichloropropane ND 10 9.8 98 10 8.9 89 10 70-130/20
594-20-7 2,2-Dichloropropane ND 10 9.5 95 10 8.4 84 12 70-130/20
563-58-6 1,1-Dichloropropene ND 10 10 100 10 8.7 87 14 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 10 9.5 95 10 8.4 84 12 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 10 10.3 103 10 9.2 92 11 70-130/20
108-20-3 Di-Isopropyl Ether ND 10 8.8 88 10 7.9 79 11 70-130/20
100-41-4 Ethylbenzene ND 10 10.0 100 10 8.9 89 12 70-130/20
87-68-3 Hexachlorobutadiene ND 10 10.6 106 10 9.3 93 13 70-130/20
98-82-8 Isopropylbenzene ND 10 11.2 112 10 9.9 99 12 70-130/20
* = Outside of Control Limits.
39 of 44
FA22722 55.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA22722
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 1; US Hwy 87, Reigelwood, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA22594-12MS A0192925.D 1 03/16/15 TD n/a n/a VA1657
FA22594-12MSD A0192926.D 1 03/16/15 TD n/a n/a VA1657
FA22594-12 A0192918.D 1 03/16/15 TD n/a n/a VA1657
The QC reported here applies to the following samples:Method: SM 6200B
FA22722-2, FA22722-3, FA22722-4, FA22722-5, FA22722-6
FA22594-12 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 10 11.3 113 10 10.0 100 12 70-130/20
74-83-9 Methyl Bromide ND 10 10.2 102 10 9.0 90 13 60-140/20
74-87-3 Methyl Chloride ND 10 9.9 99 10 8.6 86 14 60-140/20
74-95-3 Methylene Bromide ND 10 9.8 98 10 8.8 88 11 70-130/20
75-09-2 Methylene Chloride ND 10 8.2 82 10 7.3 73 12 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 10 8.7 87 10 8.0 80 8 70-130/20
91-20-3 Naphthalene ND 10 9.5 95 10 9.1 91 4 70-130/20
103-65-1 n-Propylbenzene ND 10 11.5 115 10 10.2 102 12 70-130/20
100-42-5 Styrene ND 10 9.8 98 10 8.7 87 12 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 10 10.5 105 10 9.4 94 11 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 10 10.2 102 10 9.6 96 6 70-130/20
127-18-4 Tetrachloroethylene ND 10 10.3 103 10 9.1 91 12 70-130/20
108-88-3 Toluene ND 10 9.5 95 10 8.5 85 11 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 10 10 100 10 9.3 93 7 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 10 10.1 101 10 9.2 92 9 70-130/20
71-55-6 1,1,1-Trichloroethane ND 10 9.3 93 10 8.2 82 13 70-130/20
79-00-5 1,1,2-Trichloroethane ND 10 10.0 100 10 9.3 93 7 70-130/20
79-01-6 Trichloroethylene ND 10 9.7 97 10 8.6 86 12 70-130/20
75-69-4 Trichlorofluoromethane ND 10 8.8 88 10 7.6 76 15 60-140/20
96-18-4 1,2,3-Trichloropropane ND 10 10.1 101 10 9.4 94 7 70-130/20
95-63-6 1,2,4-Trimethylbenzene ND 10 10.0 100 10 8.9 89 12 70-130/20
108-67-8 1,3,5-Trimethylbenzene ND 10 10.2 102 10 9.0 90 13 70-130/20
75-01-4 Vinyl Chloride ND 10 9.3 93 10 8.3 83 11 60-140/20
m,p-Xylene ND 20 20.7 104 20 18.2 91 13 70-130/20
95-47-6 o-Xylene ND 10 10.8 108 10 9.6 96 12 70-130/20
1330-20-7 Xylene (total)ND 30 31.5 105 30 27.8 93 12 70-130/20
CAS No.Surrogate Recoveries MS MSD FA22594-12 Limits
1868-53-7 Dibromofluoromethane 101%100%98%70-130%
17060-07-0 1,2-Dichloroethane-D4 99%100%101%70-130%
2037-26-5 Toluene-D8 99%99%98%70-130%
460-00-4 4-Bromofluorobenzene 100%99%98%70-130%
* = Outside of Control Limits.
40 of 44
FA22722 55.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA22722
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 1; US Hwy 87, Reigelwood, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA22647-2MS A0192958.D 500 03/17/15 TD n/a n/a VA1658
FA22647-2MSD A0192959.D 500 03/17/15 TD n/a n/a VA1658
FA22647-2 A0192948.D 500 03/17/15 TD n/a n/a VA1658
The QC reported here applies to the following samples:Method: SM 6200B
FA22722-1
FA22647-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 1030 5000 5150 82 5000 5310 86 3 70-130/20
108-86-1 Bromobenzene ND 5000 4120 82 5000 4230 85 3 70-130/20
74-97-5 Bromochloromethane ND 5000 3870 77 5000 4060 81 5 70-130/20
75-27-4 Bromodichloromethane ND 5000 4270 85 5000 4440 89 4 70-130/20
75-25-2 Bromoform ND 5000 3970 79 5000 4230 85 6 70-130/20
104-51-8 n-Butylbenzene ND 5000 4150 83 5000 4290 86 3 70-130/20
135-98-8 sec-Butylbenzene ND 5000 4570 91 5000 4710 94 3 70-130/20
98-06-6 tert-Butylbenzene ND 5000 4470 89 5000 4680 94 5 70-130/20
56-23-5 Carbon Tetrachloride ND 5000 4350 87 5000 4550 91 4 70-130/20
108-90-7 Chlorobenzene ND 5000 4360 87 5000 4580 92 5 70-130/20
75-00-3 Chloroethane ND 5000 4760 95 5000 4860 97 2 60-140/20
67-66-3 Chloroform ND 5000 4260 85 5000 4460 89 5 70-130/20
95-49-8 o-Chlorotoluene ND 5000 4480 90 5000 4650 93 4 70-130/20
106-43-4 p-Chlorotoluene ND 5000 4510 90 5000 4640 93 3 70-130/20
124-48-1 Dibromochloromethane ND 5000 4140 83 5000 4410 88 6 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 5000 3760 75 5000 4110 82 9 70-130/20
106-93-4 1,2-Dibromoethane ND 5000 3990 80 5000 4250 85 6 70-130/20
75-71-8 Dichlorodifluoromethane ND 5000 4910 98 5000 5020 100 2 60-140/20
95-50-1 1,2-Dichlorobenzene ND 5000 4390 88 5000 4560 91 4 70-130/20
541-73-1 1,3-Dichlorobenzene ND 5000 4490 90 5000 4640 93 3 70-130/20
106-46-7 1,4-Dichlorobenzene ND 5000 4050 81 5000 4240 85 5 70-130/20
75-34-3 1,1-Dichloroethane ND 5000 4090 82 5000 4250 85 4 70-130/20
107-06-2 1,2-Dichloroethane ND 5000 4160 83 5000 4480 90 7 70-130/20
75-35-4 1,1-Dichloroethylene ND 5000 4330 87 5000 4550 91 5 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 5000 4170 83 5000 4310 86 3 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 5000 4070 81 5000 4230 85 4 70-130/20
78-87-5 1,2-Dichloropropane ND 5000 4120 82 5000 4340 87 5 70-130/20
142-28-9 1,3-Dichloropropane ND 5000 3960 79 5000 4220 84 6 70-130/20
594-20-7 2,2-Dichloropropane ND 5000 4150 83 5000 4180 84 1 70-130/20
563-58-6 1,1-Dichloropropene ND 5000 4480 90 5000 4610 92 3 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 5000 3960 79 5000 4080 82 3 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 5000 4150 83 5000 4410 88 6 70-130/20
108-20-3 Di-Isopropyl Ether 293 5000 4030 75 5000 4270 80 6 70-130/20
100-41-4 Ethylbenzene 2200 5000 6350 83 5000 6580 88 4 70-130/20
87-68-3 Hexachlorobutadiene ND 5000 4220 84 5000 4380 88 4 70-130/20
98-82-8 Isopropylbenzene 136 J 5000 4570 89 5000 4760 92 4 70-130/20
* = Outside of Control Limits.
41 of 44
FA22722 55.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA22722
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 1; US Hwy 87, Reigelwood, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA22647-2MS A0192958.D 500 03/17/15 TD n/a n/a VA1658
FA22647-2MSD A0192959.D 500 03/17/15 TD n/a n/a VA1658
FA22647-2 A0192948.D 500 03/17/15 TD n/a n/a VA1658
The QC reported here applies to the following samples:Method: SM 6200B
FA22722-1
FA22647-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 5000 4510 90 5000 4600 92 2 70-130/20
74-83-9 Methyl Bromide ND 5000 4740 95 5000 5000 100 5 60-140/20
74-87-3 Methyl Chloride ND 5000 4950 99 5000 5100 102 3 60-140/20
74-95-3 Methylene Bromide ND 5000 4100 82 5000 4370 87 6 70-130/20
75-09-2 Methylene Chloride ND 5000 4070 81 5000 4220 84 4 70-130/20
1634-04-4 Methyl Tert Butyl Ether 484 5000 4200 74 5000 4530 81 8 70-130/20
91-20-3 Naphthalene 741 5000 4360 72 5000 4720 80 8 70-130/20
103-65-1 n-Propylbenzene 401 5000 4970 91 5000 5140 95 3 70-130/20
100-42-5 Styrene 78.3 J 5000 4040 79 5000 4200 82 4 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 5000 4160 83 5000 4400 88 6 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 5000 3890 78 5000 4150 83 6 70-130/20
127-18-4 Tetrachloroethylene ND 5000 4400 88 5000 4560 91 4 70-130/20
108-88-3 Toluene 12900 5000 17000 82 5000 17600 94 3 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 5000 3870 77 5000 4220 84 9 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 5000 3900 78 5000 4120 82 5 70-130/20
71-55-6 1,1,1-Trichloroethane ND 5000 4200 84 5000 4330 87 3 70-130/20
79-00-5 1,1,2-Trichloroethane ND 5000 4070 81 5000 4340 87 6 70-130/20
79-01-6 Trichloroethylene ND 5000 4360 87 5000 4460 89 2 70-130/20
75-69-4 Trichlorofluoromethane ND 5000 4370 87 5000 4520 90 3 60-140/20
96-18-4 1,2,3-Trichloropropane ND 5000 3900 78 5000 4200 84 7 70-130/20
95-63-6 1,2,4-Trimethylbenzene 3400 5000 7400 80 5000 7700 86 4 70-130/20
108-67-8 1,3,5-Trimethylbenzene 912 5000 5000 82 5000 5130 84 3 70-130/20
75-01-4 Vinyl Chloride ND 5000 4440 89 5000 4630 93 4 60-140/20
m,p-Xylene 9980 10000 18600 86 10000 19300 93 4 70-130/20
95-47-6 o-Xylene 5300 5000 9740 89 5000 10200 98 5 70-130/20
1330-20-7 Xylene (total)15300 15000 28400 87 15000 29400 94 3 70-130/20
CAS No.Surrogate Recoveries MS MSD FA22647-2 Limits
1868-53-7 Dibromofluoromethane 103%103%99%70-130%
17060-07-0 1,2-Dichloroethane-D4 105%105%102%70-130%
2037-26-5 Toluene-D8 99%100%99%70-130%
460-00-4 4-Bromofluorobenzene 100%99%101%70-130%
* = Outside of Control Limits.
42 of 44
FA22722 55.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA22722
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 1; US Hwy 87, Reigelwood, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA22714-4MS A0192974.D 1 03/17/15 TD n/a n/a VA1659
FA22714-4MSD A0192975.D 1 03/17/15 TD n/a n/a VA1659
FA22714-4 A0192969.D 1 03/17/15 TD n/a n/a VA1659
The QC reported here applies to the following samples:Method: SM 6200B
FA22722-2, FA22722-4, FA22722-5, FA22722-7
FA22714-4 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene ND 10 9.8 98 10 10.4 104 6 70-130/20
108-86-1 Bromobenzene ND 10 9.6 96 10 10.5 105 9 70-130/20
74-97-5 Bromochloromethane ND 10 9.1 91 10 9.8 98 7 70-130/20
75-27-4 Bromodichloromethane ND 10 9.9 99 10 10.2 102 3 70-130/20
75-25-2 Bromoform ND 10 9.3 93 10 9.1 91 2 70-130/20
104-51-8 n-Butylbenzene ND 10 9.5 95 10 10.2 102 7 70-130/20
135-98-8 sec-Butylbenzene ND 10 10.6 106 10 11.5 115 8 70-130/20
98-06-6 tert-Butylbenzene ND 10 10.4 104 10 11.3 113 8 70-130/20
56-23-5 Carbon Tetrachloride ND 10 10.2 102 10 10.1 101 1 70-130/20
108-90-7 Chlorobenzene ND 10 10.3 103 10 11.1 111 7 70-130/20
75-00-3 Chloroethane ND 10 9.9 99 10 10.2 102 3 60-140/20
67-66-3 Chloroform ND 10 10.1 101 10 10.8 108 7 70-130/20
95-49-8 o-Chlorotoluene ND 10 10.2 102 10 11.2 112 9 70-130/20
106-43-4 p-Chlorotoluene ND 10 10.6 106 10 11.5 115 8 70-130/20
124-48-1 Dibromochloromethane ND 10 9.7 97 10 9.9 99 2 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 10 8.9 89 10 9.6 96 8 70-130/20
106-93-4 1,2-Dibromoethane ND 10 9.4 94 10 10.3 103 9 70-130/20
75-71-8 Dichlorodifluoromethane ND 10 9.9 99 10 10.6 106 7 60-140/20
95-50-1 1,2-Dichlorobenzene ND 10 10.3 103 10 11.1 111 7 70-130/20
541-73-1 1,3-Dichlorobenzene ND 10 10.5 105 10 11.4 114 8 70-130/20
106-46-7 1,4-Dichlorobenzene ND 10 9.5 95 10 10.3 103 8 70-130/20
75-34-3 1,1-Dichloroethane ND 10 9.8 98 10 10.5 105 7 70-130/20
107-06-2 1,2-Dichloroethane ND 10 9.7 97 10 10.6 106 9 70-130/20
75-35-4 1,1-Dichloroethylene ND 10 10.5 105 10 11.1 111 6 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 10 10.1 101 10 10.7 107 6 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 10 9.8 98 10 10.3 103 5 70-130/20
78-87-5 1,2-Dichloropropane ND 10 9.9 99 10 10.6 106 7 70-130/20
142-28-9 1,3-Dichloropropane ND 10 9.4 94 10 10.4 104 10 70-130/20
594-20-7 2,2-Dichloropropane ND 10 8.9 89 10 9.5 95 7 70-130/20
563-58-6 1,1-Dichloropropene ND 10 10.7 107 10 11.2 112 5 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 10 9.0 90 10 8.9 89 1 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 10 9.5 95 10 9.5 95 0 70-130/20
108-20-3 Di-Isopropyl Ether ND 10 9.0 90 10 9.8 98 9 70-130/20
100-41-4 Ethylbenzene ND 10 9.7 97 10 10.5 105 8 70-130/20
87-68-3 Hexachlorobutadiene ND 10 9.6 96 10 10.3 103 7 70-130/20
98-82-8 Isopropylbenzene ND 10 10.5 105 10 11.2 112 6 70-130/20
* = Outside of Control Limits.
43 of 44
FA22722 55.3.3
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA22722
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 1; US Hwy 87, Reigelwood, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA22714-4MS A0192974.D 1 03/17/15 TD n/a n/a VA1659
FA22714-4MSD A0192975.D 1 03/17/15 TD n/a n/a VA1659
FA22714-4 A0192969.D 1 03/17/15 TD n/a n/a VA1659
The QC reported here applies to the following samples:Method: SM 6200B
FA22722-2, FA22722-4, FA22722-5, FA22722-7
FA22714-4 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 10 10.3 103 10 11.2 112 8 70-130/20
74-83-9 Methyl Bromide ND 10 9.9 99 10 10.3 103 4 60-140/20
74-87-3 Methyl Chloride ND 10 10.2 102 10 10.7 107 5 60-140/20
74-95-3 Methylene Bromide ND 10 9.7 97 10 10.6 106 9 70-130/20
75-09-2 Methylene Chloride ND 10 8.9 89 10 9.7 97 9 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 10 9.1 91 10 9.9 99 8 70-130/20
91-20-3 Naphthalene ND 10 8.7 87 10 9.7 97 11 70-130/20
103-65-1 n-Propylbenzene ND 10 10.7 107 10 11.7 117 9 70-130/20
100-42-5 Styrene ND 10 8.6 86 10 9.1 91 6 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 10 9.8 98 10 10.5 105 7 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 10 9.2 92 10 10.3 103 11 70-130/20
127-18-4 Tetrachloroethylene ND 10 10.3 103 10 11.0 110 7 70-130/20
108-88-3 Toluene ND 10 9.4 94 10 10.2 102 8 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 10 9.1 91 10 10.1 101 10 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 10 9.2 92 10 10.1 101 9 70-130/20
71-55-6 1,1,1-Trichloroethane ND 10 10 100 10 10.5 105 5 70-130/20
79-00-5 1,1,2-Trichloroethane ND 10 9.6 96 10 10.7 107 11 70-130/20
79-01-6 Trichloroethylene ND 10 10.1 101 10 10.8 108 7 70-130/20
75-69-4 Trichlorofluoromethane ND 10 9.0 90 10 9.3 93 3 60-140/20
96-18-4 1,2,3-Trichloropropane ND 10 9.1 91 10 10.2 102 11 70-130/20
95-63-6 1,2,4-Trimethylbenzene ND 10 9.3 93 10 10.2 102 9 70-130/20
108-67-8 1,3,5-Trimethylbenzene ND 10 9.6 96 10 10.3 103 7 70-130/20
75-01-4 Vinyl Chloride ND 10 9.3 93 10 10 100 7 60-140/20
m,p-Xylene ND 20 20.0 100 20 21.4 107 7 70-130/20
95-47-6 o-Xylene ND 10 10.3 103 10 11.2 112 8 70-130/20
1330-20-7 Xylene (total)ND 30 30.3 101 30 32.6 109 7 70-130/20
CAS No.Surrogate Recoveries MS MSD FA22714-4 Limits
1868-53-7 Dibromofluoromethane 104%104%103%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%102%108%70-130%
2037-26-5 Toluene-D8 98%99%97%70-130%
460-00-4 4-Bromofluorobenzene 99%100%100%70-130%
* = Outside of Control Limits.
44 of 44
FA22722 55.3.3