WI-16971_16971_CA_RMR_20221130_3264

Tetra Tech, Inc.
805 E 20th Street Charlotte, NC 28205
Tel [phone] www.tetratech.com
November 30, 2022

Ms. Liz Price
North Carolina Department of Environmental Quality
Division of Waste Management
127 Cardinal Drive Extension
Wilmington, North Carolina 28405-3845

RE: Remediation Update Report for September 2021 to August 2022
Former Flint Hills Resources North Terminal - Loading Rack Area
3325 River Road, Wilmington, North Carolina
NCDEQ Incident No. 16971

Dear Ms. Price,

Tetra Tech, on behalf of Flint Hills Resources, LP (FHR), is submitting for your review the
Remediation Update Report (RUR) for the period of September 2021 through August 2022 for the
above referenced site. Tetra Tech assumed environmental management of the Loading Rack on behalf
of FHR beginning in January 2021.

In August 2022, Tetra Tech collected groundwater samples from 13 monitoring wells for VOC analysis
in accordance with the 2021 RUR recommendations. One additional well was dry and therefore not
able to be sampled. Laboratory results indicated similar detections of contaminants to previous results,
which continue to demonstrate effective attenuation across the site.

Please notify me at [e-mail] or 734-213-4079 if you have any questions or
comments regarding the information presented in this report.

Sincerely,

Matt Mahony Daniel Sopoci, CHMM
Project Manager Program Manager

cc: Michael Christopher, Flint Hills Resources LP
Stacey Kirk, Chemserve Terminal of Wilmington
Benjamin Francisco, Tetra Tech
2022 Annual Remediation Update Report Former FHR North Terminal – Loading Rack
© 2022. Flint Hills Resources LP. All rights reserved. Page i
Annual Remediation Update Report
September 2021 – August 2022
Flint Hills Resources, LP
North Terminal - Loading Rack Area
NCDEQ Incident No. 16971
Wilmington, North Carolina
November 30, 2022
2022 Annual Remediation Update Report Former FHR North Terminal – Loading Rack
© 2022. Flint Hills Resources LP. All rights reserved. Page ii
Annual Remediation Update Report
September 2021 – August 2022
Flint Hills Resources, LP
North Terminal - Loading Rack Area
NCDEQ Incident No. 16971
Wilmington, North Carolina
Prepared for:
Flint Hills Resources, LP
P.O. Box 2917
Wichita, KS 67201
Prepared by:
Tetra Tech
805 E 20th Street
Charlotte, NC 28205
November 30, 2022
___________________________ __________________________
Daniel Sopoci, CHMM Matt Mahony
Program Manager Project Manager
CERTIFICATIONPAGEREGISTEREDNORTHCAROLINAPROFESSIONALGEOLOGISTCERTIFICATIONI,BenjaminH.Francisco,aLicensedGeologistforTetraTechGeologicalServicesP.C.,docertifythattheinformationcontainedinthisreportiscorrectandaccuratetothebestofmyknowledge.0:°BenjaminH.Francisco,L.G.NorthCarolinaLicenseNo.1987DateTetraTechGeologicalServicesP.C.islicensedtopracticegeologyinNorthCarolina.ThecertificationnumberofthecompanyorcorporationisC-524.2022AnnualRemediationUpdateReport©2022.FlintHillsResourcesLP.Allrightsreserved.FormerFHRNorthTerminal—LoadingRackPageiiiIiiiit‘‘

2022 Annual Remediation Update Report Former FHR North Terminal – Loading Rack
© 2022. Flint Hills Resources LP. All rights reserved. Page iv
TABLE OF CONTENTS
1. INTRODUCTION ................................................................................................................... 1
1.1 Site Description ................................................................................................................... 1
1.2 Facility Status ...................................................................................................................... 2
2. GROUNDWATER MONITORING ......................................................................................... 3
2.1 Groundwater Elevations and Flow Direction ....................................................................... 3
2.2 Groundwater Monitoring Methods ....................................................................................... 4
2.3 Groundwater Monitoring Results ......................................................................................... 4
2.3.1 Loading Rack ................................................................................................................ 5
2.3.2 Apex Property ............................................................................................................... 5
2.3.3 FHR WTP ..................................................................................................................... 6
2.3.4 Mann-Kendall Trend Analysis ....................................................................................... 6
2.4 Groundwater Monitoring Recommendations ....................................................................... 7
3. CONCLUSIONS ....................................................................................................................... 8
TABLES
Table 1 Groundwater Elevations and Water Quality Measurements
Table 2 Groundwater Results, 2013-2022
FIGURES
Figure 1 Site Location
Figure 2 Site Layout
Figure 3 Site Features
Figure 4 Groundwater Elevation Contours
Figure 5 Groundwater Results – Volatile Organic Compounds
APPENDICES
Appendix A Historical Groundwater Elevation Measurements
Appendix B Historical Groundwater Water Quality Measurements
Appendix C Historical Groundwater Results
Appendix D Laboratory Analytical Reports
Appendix E Mann-Kendall Trend Analyses
2022 Annual Remediation Update Report Former FHR North Terminal – Loading Rack
© 2022. Flint Hills Resources LP. All rights reserved. Page 1
1. INTRODUCTION
On behalf of Flint Hills Resources, LP (FHR), Tetra Tech, Inc. (Tetra Tech) has prepared this
Remediation Update Report (RUR) for the former FHR North Terminal Loading Rack area
(Loading Rack) located at 3325 River Road, Wilmington, New Hanover County, North Carolina
(Figure 1). Past groundwater investigations of the former FHR Loading Rack area revealed
concentrations of paraxylene (PX), dissolved gasoline, and fuel oil in exceedance of the 15A North
Carolina Administrative Code (NCAC) 2L.0202 North Carolina Groundwater Quality Standard (2L
GWQS), updated April 1, 2013. RURs for the Loading Rack area have been submitted annually
since 2002 by CATLIN Engineers and Scientists (CATLIN), and Tetra Tech assumed
environmental management of the Loading Rack on behalf of FHR beginning in January 2021.
As detailed in the 2002 Corrective Action Plan (CAP) Addendum, groundwater contamination in
the Loading Rack area is assumed to be from historical operation and maintenance activities of
the former FHR truck and railcar loading racks. These operations are assumed to have resulted
in minor releases. Therefore, current groundwater impacts are not associated with a specific
release event. Historical remedial approaches at the Loading Rack are detailed in previous RURs
and have included ex-situ soil remediation, product removal from recovery wells, aggressive fluid
vapor recovery (AFVR), and most recently in 2017, three Epsom salt and water solution (EAB)
amendment injection events. A technical memorandum summarizing the EAB amendment was
included in Appendix A of the 2017 RUR. Monitored natural attenuation is the current remedial
approach as proposed in the 2021 RUR. Applicable remedial action documents since the initial
2002 CAP Addendum are presented in the 2020 RUR.
This report provides an annual update to remediation activities and results for the monitoring
period between September 2021 through August 2022. The annual groundwater sampling event
occurred in August 2022 with no other significant activities during the reporting period.
1.1 Site Description
The Loading Rack area is a subdivision of the larger North Terminal site, a facility comprising
approximately 37 acres for bulk chemical storage and transfer previously owned and operated by
FHR (Figure 2). Approximately 33 acres of the former North Terminal are located on the east
side of River Road and are divided into three project areas: the Loading Rack in the southwestern
corner of the site, the Paraxylene (PX) Facility in the north, and the Gasoline Fuel Oil (GFO)
Facility in the southeast. Remediation activities related to the PX Facility revealed additional
2022 Annual Remediation Update Report Former FHR North Terminal – Loading Rack
© 2022. Flint Hills Resources LP. All rights reserved. Page 2
environmental concerns and in 2002 the North Carolina Department of Environmental Quality
(NCDEQ) accepted a CAP Addendum by FHR which addressed the Loading Rack area. These
properties are currently owned and operated by Chemserve Terminal of Wilmington, LLC
(Chemserve) for bulk chemical storage and transfer operations.
FHR retains ownership of an additional four acres on the west side of River Road comprising the
FHR water treatment plant (FHR WTP) area which was initially designed to treat groundwater
from recovery wells on the PX Facility. FHR regularly updates NCDEQ on the status of the PX
Facility in separate reports filed under separate covers. The GFO Facility immediately east of the
Loading Rack area received No Further Action (NFA) status from NCDEQ on December 2, 2019.
1.2 Facility Status
The former FHR truck loading rack was disassembled in 2003 and the lot remained largely
undeveloped until 2014 when Chemserve built a new bulk chemical truck loading rack in the same
general footprint of the former FHR rack.
Since 2013, Loading Rack sampling activities have also included monitoring non-FHR petroleum
hydrocarbon source areas on the Apex Oil Company, Inc. (Apex) petroleum fuel property on the
west side of River Road, as well as several monitoring wells on the FHR WTP property adjacent
to the north (Figure 2). Based on review of NCDEQ files, it is understood that Apex has
implemented various technologies to address the presence of free-phase product and are
monitoring the dissolved groundwater contaminant plume on their property on an annual basis.
Regulatory responsibilities for managing contamination at the Loading Rack were transferred from
NCDEQ’s Division of Water Quality (DWQ) – Aquifer Protection Section (APS), to the Division of
Waste Management (DWM) - Underground Storage Tank (UST) Section in 2007. FHR
understands that the DWM-UST Section will manage the site in accordance with the July 1, 2012
Guidelines for Initial Response and Abatement, Assessment, and Corrective Action for Non-UST
Releases of Petroleum. The corrective actions implemented and documented within this report
are in general accordance with this guidance document.
2022 Annual Remediation Update Report
© 2022. Flint Hills Resources LP. All rights reserved.
Former FHR North Terminal – Loading Rack
Page 3
2. GROUNDWATER MONITORING
Contaminants of concern in groundwater with concentration detections greater than 2L GWQS
criteria at the Loading Rack site since 2001 include benzene, n-butylbenzene, sec-butylbenzene,
ethylbenzene, isopropylbenzene, naphthalene, methyl tert butyl ether (MTBE), n-propylbenzene,
toluene, 1,2,4-trimethylbenzene, 1,3,5-trimethylbenzene and xylenes. Through active remediation
and attenuation, concentrations of these contaminants have decreased over time. In the last three
years since 2018, the only contaminants of concern with detections greater than 2L GWQS are:
Benzene
Ethylbenzene
Isopropylbenzene (Cumene)
Naphthalene
1,2,4-trimethylbenzene
Total meta/para-xylenes
Based on the recommendations in the 2021 RUR, Tetra Tech gauged and sampled 13
groundwater wells in August 2022 to continue to monitor attenuation. One additional well was
planned to be gauged and sampled but was dry. Well locations included four monitoring wells on
the Loading Rack site, seven on the Apex property, and three on the FHR WTP property (Figure
3). Sample locations included mostly shallow Type II wells with total depths ranging from 7.11 to
16.00 feet below ground surface (bgs), as measured by Tetra Tech personnel in August 2021.
Field personnel completed groundwater sampling in accordance with the June 7, 2005 Revised
Remedial Action Plan (RAP); the December 21, 2015 CAP Addendum; and minor modifications
in subsequent RURs. The following sections describe field activities completed in 2022.
2.1 Groundwater Elevations and Flow Direction
Tetra Tech field personnel measured static groundwater levels of 13 groundwater monitoring
wells on August 1, 2022. One additional well, KMW-12, was dry and therefore was not able to be
measured. All wells were gauged with an oil/water interface probe accurate to 0.01 foot which
was thoroughly rinsed with Liquinox and distilled water following each use to minimize the
potential for cross contamination between wells. Depth-to-water measurements were subtracted
from top-of-casing elevations for each well to obtain groundwater surface elevations.
Depth-to-water measurements are presented in Table 1 and a summary of historical depth-to-
water measurements are presented in Appendix A. Water elevations at the Loading Rack site
2022 Annual Remediation Update Report
© 2022. Flint Hills Resources LP. All rights reserved.
Former FHR North Terminal – Loading Rack
Page 4
ranged from 5.41 to 23.08 feet amsl, and static elevations in August 2022 were on average 2.58
feet lower than those measured in August 2021. Groundwater elevation contours are provided in
Figure 4, indicating groundwater flow in the vicinity of the Loading Rack is towards the west-
northwest, consistent with previous findings.
2.2 Groundwater Monitoring Methods
Groundwater sampling included low flow methods consistent with the Low Stress (Low Flow)
Purging and Sampling Procedure for the Collection of Groundwater Samples from Monitoring
Wells (2017), published by the United States Environmental Protection Agency (EPA). At each
monitoring well, groundwater was purged using a peristaltic pump with disposable tubing while
measuring field groundwater quality parameters including temperature, specific conductivity,
dissolved oxygen, pH, oxidation reduction potential, and turbidity multi-parameter meter with a
flow-through cell. Groundwater samples were transferred to laboratory-supplied containers,
placed into ice-packed coolers, and handled under the proper chain-of-custody procedures for
laboratory analysis of volatile organic compounds (VOCs) per EPA Method 8260 by Pace
Analytical of Huntersville, North Carolina (NC Certification #12).
2.3 Groundwater Monitoring Results
A summary of field measurements is presented as Table 1 and a summary of historical water
quality results are presented in Appendix B. A summary of laboratory analytical results for 2013
through 2022 is presented as Table 2 and a summary of historical laboratory analytical results is
presented in Appendix C. Laboratory analytical reports are included as Appendix D.
Groundwater sample detections of benzene, toluene, ethylbenzene, MTBE, naphthalene, and
total xylenes are presented in Figure 5. Free product has not been detected in Loading Rack
monitoring wells since August 2008. VOCs were detected in ten of 13 monitoring wells sampled.
In eight wells, detections of at least one constituent exceeded 2L GWQS.
The following sections describe groundwater monitoring results in each of three areas: the
Loading Rack east of River Road, the Apex property west of River Road, and the FHR WTP area
west of River Road.
2022 Annual Remediation Update Report Former FHR North Terminal – Loading Rack
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2.3.1 Loading Rack
Two monitoring wells were sampled in the Loading Rack area east of River Road. KMW-7 and
KMW-9R are in the truck loading rack area and exhibit VOC detections generally consistent with
detections in the previous few years. Detections of naphthalene in KMW-9R exceed 2L GWQS
but continue to exhibit a generally decreasing trend. KMW-7 continues to have low-level
detections less than 2L GWQS and has not had an exceedance since 2015.
Monitoring wells KMW-6 and KMW-8 are also east of River Road and are located in the railcar
loading area. Although detections of meta/para-xylenes continue to exceed 2L GWQS in KMW-
6, detections decreased more than 80% compared to 2021 results, and have decreased over
90% since 2020. Similarly in KMW-8, detections of naphthalene have sharply decreased and are
below 2L GWQS for the first time at this location. Although benzene continues to exceed 2L
GWQS in KMW-8, detections also decreased more than 70% compared to 2021 results.
Results in 2022 demonstrate continued attenuation in recent years following active remediation
efforts implemented by FHR.
2.3.2 Apex Property
Six monitoring wells were sampled west of River Road located on the Apex property. One
additional well, KMW-12, was dry and therefore not sampled. Of the sampled wells, three are
located directly across from the Loading Rack along the west side of River Road. KMW-13 is
located immediately west of the Loading Rack and exhibit concentrations naphthalene and
meta/para-xylenes exceeding 2L GWQS, consistent with previous detections. Although
concentrations continue to exceed 2L GWQS, concentrations at KMW-13 continue to
demonstrate sustained decreases from previous high values. Also, just 75 feet north along River
Road, KMW-14 did not exhibit any contaminant concentrations greater than 2L GWQS, consistent
with recent monitoring results.
Wells AMW-2 through AMW-5 monitor groundwater quality throughout the Apex property. All
three monitoring locations exceeded 2L GWQS. In recent years, concentrations have remained
elevated in AMW-4 for numerous constitutes, while monitoring results from the rest of the wells
across the site demonstrate sustained decreasing trends. This observation suggests a potential
alternate source of elevated VOCs in AMW-4 unrelated to the previous operation and
maintenance activities of the former FHR truck and railcar loading racks.
2022 Annual Remediation Update Report Former FHR North Terminal – Loading Rack
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2.3.3 FHR WTP
Monitoring wells located on the FHR WTP include three locations: KMW-1, KMW-3, and KMW-
18. For the second year in a row, only one detection exceeded 2L GWQS at these locations.
Benzene at KMW-3 exceeded 2L GWQS but remained 40% less than 2019 detections.
Meta/para-xylenes continue a general decreasing trend at KMW-1 and KMW-3, including non-
detect results in 2022. Monitoring results from locations at the FHR WTP continue to
demonstrate attenuation of groundwater contaminants.
2.3.4 Mann-Kendall Trend Analysis
A graphical representation of VOC concentrations versus time for monitoring wells are included
in Appendix E. Mann-Kendall trend analyses were performed using the EPA’s ProUCL for the
historical Loading Rack data sets from 2001 to present, which are summarized in the table below.
The 13 Type II shallow wells sampled in 2022 were included in the dataset.
Monitoring 
Well 
Trends 
Benzene Naphthalene Total 
Xylenes 
KMW‐1 Decreasing Decreasing No Trend 
KMW‐3 No Trend No Trend No Trend 
KMW‐6 Decreasing Decreasing No Trend 
KMW‐7 Decreasing Decreasing Decreasing 
KMW‐8 Decreasing Decreasing Decreasing 
KMW‐9R Decreasing Decreasing Decreasing 
KMW‐13 Decreasing Decreasing Decreasing 
KMW‐14 Decreasing Decreasing Decreasing 
KMW‐18 No Trend No Trend No Trend 
AMW‐2 Decreasing Decreasing Decreasing 
AMW‐3 Decreasing Decreasing Decreasing 
AMW‐4 Decreasing Increasing Increasing 
AMW‐5 Decreasing No Trend No Trend 
2022 Annual Remediation Update Report Former FHR North Terminal – Loading Rack
© 2022. Flint Hills Resources LP. All rights reserved. Page 7
Statistical analysis indicates decreasing contaminant concentration trends are prevalent for the
wells sampled in 2022 which have either decreasing trends or no trend, with the exception of
increasing naphthalene and total xylene trends in AMW-4 on the Apex property. As discussed in
previous RURs, review of historical groundwater data indicates an alternative source of
groundwater contaminants at AMW-4 that are unrelated to the previous operation and
maintenance activities of the former FHR truck and railcar loading racks. This potential source
area in the vicinity of AMW-4 is likely the cause of elevated levels of various analytes detected in
monitoring wells located on the downgradient portion of Apex property as well as the western
portion of the FHR WTP area. FHR’s understanding is that Apex has implemented and continues
to monitor remedial activities on their property.
2.4 Groundwater Monitoring Recommendations
Select groundwater monitoring wells will continue to be sampled annually for laboratory analysis
of VOCs per EPA Method 8260, and an RUR summarizing the August 2023 sampling event will
be submitted to NCDEQ by November 30, 2023.

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3. CONCLUSIONS
This annual report summarizes the annual groundwater monitoring completed in August 2022.

Water depths were gauged with an interface probe from 13 monitoring wells on the Loading Rack,
Apex property, and FHR WTP. One additional well was dry and therefore not sampled.
Groundwater elevations were consistent with previous monitoring events, indicating a west-
northwest flow in the direction of the Cape Fear River.

Groundwater samples collected from 13 monitoring wells for VOC analysis indicated similar
detections of contaminants to previous results, which continue to demonstrate effective
attenuation across the site. Free product has not been observed in Loading Rack monitoring wells
since 2008. Although concentrations of several contaminants exceeded 2L GWQS in eight
locations in 2022, results indicate a sustained decreasing or stable trend in all instances except
at AMW-4. As discussed in Section 2.3.4 and in previous RURs, elevated contaminant
concentrations at AMW-4 are likely from another source unrelated to previous operation and
maintenance activities of the former FHR truck and railcar loading racks.

Groundwater sampling will continue in 2023 to monitor natural attenuation of contaminants. The
next sampling event will be completed in August 2023 to include monitoring wells KMW-1, KMW-
3, KMW-6, KMW-7, KMW-8, KMW-9R, KMW-12, KMW-13, KMW-14, KMW-18, AMW-2, AMW-3,
AMW-4, and AMW-5 for laboratory analysis of VOCs using EPA Method 8260. A RUR
summarizing August 2023 sampling results will be submitted to NCDEQ by November 30, 2023.

TABLES

Table 1
Depth to Groundwater and Water Quality Measurements
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
AMW-2 Apex Property 8/3/2022 11.73 16.00 24.25 0.635 NR 6.67 -165 0.0
AMW-3 Apex Property 8/3/2022 7.49 14.94 24.77 0.381 NR 6.76 -98 0.0
AMW-4 Apex Property 8/3/2022 7.09 15.49 26.63 0.255 NR 6.47 -138 3.9
AMW-5 Apex Property 8/3/2022 2.02 7.11 31.37 0.306 NR 6.77 -126 56.9
KMW-1 FHR WTP 8/3/2022 3.52 11.79 28.81 0.128 NR 6.85 -98 0.4
KMW-3 FHR WTP 8/3/2022 2.48 11.22 26.59 0.140 NR 6.32 -95 7.0
KMW-6 Loading Rack 8/4/2022 2.92 12.21 28.73 0.473 NR 7.04 -315 28.1
KMW-7 Loading Rack 8/4/2022 2.56 12.81 29.87 0.219 NR 6.89 -233 0.0
KMW-8 Loading Rack 8/4/2022 2.33 9.45 25.76 0.617 NR 6.76 -187 11.6
KMW-9R Loading Rack 8/4/2022 4.31 11.47 27.17 1.00 NR 7.13 -188 13.4
KMW-12 Apex Property 8/1/2022 DRY 11.86 ---------- --
KMW-13 Apex Property 8/5/2022 10.26 15.36 27.60 0.837 NR 6.43 -127 94.9
KMW-14 Apex Property 8/4/2022 10.76 14.83 28.62 0.296 NR 6.20 -32 0.0
KMW-18 FHR WTP 8/3/2022 3.40 12.65 24.99 0.439 NR 6.80 -165 0.0
Notes:
Historical groundwater elevations and water quality readings are provided in Appendix A and Appendix B, respectively.
Water quality parameter results presented in this table represent the final measurements prior to sampling.
Groundwater elevations were measured by Tetra Tech on August 1, 2022. Total depths were measured by Tetra Tech in August 2021.
KMW-12 was dry in August 2022 and therefore not sampled.
KMW-13 had excessive drawdown and the last reading after approximately 10 minutes of low flow purging is presented, after which the well was pumped dry.
FHR WTP = Flint Hills Resources Water Treatment Plant
bgs = below ground surface
Temp = Temperature
°C = degrees Celsius
mS/cm = millisiemens per centimeter
mg/L = milligrams per liter
mV = millivolts
ORP = Oxidation Reduction Potential
NTU = Nephelometric Turbidity Unit
NR = Not recorded.
Well ID ORP
(mV)
Turbidity
(NTU)Location Date pH
Specific
Conductance
(mS/cm)
Dissolved
Oxygen
(mg/L)
Depth to
Groundwater
(bgs)
Temp (°C) Total Depth
(bgs)
Table 2
Groundwater Results, 2013-2022
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
Contaminant of Concern
Sample ID Date Collected
1 70 70 600 70 20 6 70 600 400 400 Varies
8/13/2013 <0.25 <0.41 <0.38 0.35 J <0.40 <0.21 <0.24 <0.42 <0.26 0.31 J <0.36 113 <0.23 ND
8/21/2014 <0.25 <0.41 <0.38 0.48 J <0.40 <0.21 0.27 J <0.42 <0.26 <0.31 <0.36 39.9 <0.23 11.95 J
3/11/2015 <0.25 <0.41 <0.38 0.94 J <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36 713 <0.23 0.35 J
8/5/2015 <0.50 2.2 <0.76 12.0 <0.80 <0.42 0.86 J <0.84 <0.52 3.0 <0.72 14,700 1.8 J 0.73 J
8/1/2016 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36 5.6 <0.23 ND
8/7/2017 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36 10.0 <0.23 ND
8/7/2019 <0.15 <0.23 <0.20 <0.26 <0.20 <0.28 <0.35 <0.18 <0.24 <0.17 <0.20 33.3 <0.22 ND
8/6/2020 <0.30 <0.47 <0.40 0.69 J <0.40 <0.55 <0.70 <0.37 0.57 J <0.34 <0.39 416 <0.44 ND
8/21/2021 <0.34 <0.49 <0.40 <0.30 <0.33 <0.42 <0.64 <0.34 <0.48 <0.50 <0.33 <0.71 <0.34 ND
8/3/2022 <0.34 <0.49 <0.40 <0.30 <0.33 <0.42 <0.64 <0.34 <0.48 <0.50 <0.33 <0.71 <0.34 ND
8/13/2013 27.8 <0.41 2.2 1.4 24.5 0.45 J 2.0 16.7 3.4 11.1 6.5 7.1 0.93 J ND
8/21/2014 18.9 <0.41 <0.38 342 88.9 0.50 J 78.1 42.3 92.5 362 91.4 396 0.59 J 30.0
3/11/2015 7.5 <0.82 <0.76 42.4 54.8 <0.42 46.3 29.3 1.6 J 242 86.7 237 0.57 J 8.7 J
8/5/2015 10.7 <0.41 <0.38 0.95 J 33.0 <0.21 11.7 16.4 1.5 38.6 31.6 33.5 <0.23 5.2 J
8/1/2016 12.1 <1.0 8.1 8.5 62.3 <0.52 40.9 32.7 3.4 298 133 311 <0.58 58.2 J
8/8/2017 14.0 <0.41 <0.38 1.2 27.9 <0.21 2.2 14.7 2.6 8.8 9.4 3.4 0.76 J ND
8/7/2019 35.9 <0.23 12.2 3.3 89.9 1.2 0.96 J 47.9 3.5 68.0 <0.20 4.2 0.43 J 7.6
8/6/2020 8.0 <0.23 2.0 <0.26 16.3 <0.28 0.41 J 12.0 1.4 0.52 J <0.20 4.6 0.25 J ND
8/21/2021 8.0 <0.49 1.1 <0.30 11.6 <0.42 <0.64 7.5 1.6 <0.50 <0.33 <0.71 <0.34 ND
8/3/2022 20.3 <0.49 3.8 <0.30 39.5 <0.42 <0.64 23.9 3.6 <0.50 <0.33 3.7 <0.34 ND
Notes are provided on the final page of this table. All Other 8260B AnalytesNaphthalenen-PropylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-Trimethylbenzenem/p-Xylenessec-ButylbenzeneEthylbenzeneIsopropylbenzene (Cumene)Benzenen-ButylbenzeneMethyl Tert Butyl Ether (MTBE)o-XyleneGroundwater Clean-up Goal (ug/L)500
TYPE II MONITORING WELLS
KMW-1
KMW-3
Page 1 of 6
Table 2
Groundwater Results, 2013-2022
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
Contaminant of Concern
Sample ID Date Collected
1 70 70 600 70 20 6 70 600 400 400 VariesAll Other 8260B AnalytesNaphthalenen-PropylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-Trimethylbenzenem/p-Xylenessec-ButylbenzeneEthylbenzeneIsopropylbenzene (Cumene)Benzenen-ButylbenzeneMethyl Tert Butyl Ether (MTBE)o-XyleneGroundwater Clean-up Goal (ug/L)500
8/14/2013 <50.0 <82.0 <76.0 69.0 J <80.0 <42.0 <48.0 <84.0 <52.0 <62.0 <72.0 40,600 56.8 J 360 J
8/14/2014 <50.0 <82.0 <76.0 99.7 J <80.0 <42.0 <48.0 <84.0 <52.0 <62.0 <72.0 61,300 78.6 J ND
3/11/2015 <50.0 <82.0 <76.0 125 J <80.0 <42.0 <48.0 <84.0 <52.0 <62.0 <72.0 76,800 95.6 J ND
8/5/2015 <62.5 <102 <95.0 102 J <100 <52.5 <60.0 <105 <65.0 <77.5 <90.0 69,500 102 J ND
8/1/2016 <50.0 <82.0 <76.0 78.8 J <80.0 <42.0 <48.0 <84.0 <52.0 <62.0 <72.0 45,600 66.6 J ND
10/6/2016 <50.0 NA NA <60.0 NA NA NA NA <52.0 NA NA 27,400 <46.0 NA
11/23/2016 <50.0 NA NA 90.9 J NA NA NA NA <52.0 NA NA 57,800 79.2 J NA
3/2/2017 <62.5 <102 <95.0 93.8 J <100 <52.5 256 <105 <65.0 <77.5 <90.0 48,400 66.2 J ND
4/26/2017 <62.5 NA NA 81.2 J NA NA NA NA 86.8 J NA NA 45,000 72.8 J NA
8/9/2017 <50.0 <82.0 <76.0 60.6 J <80.0 <42.0 <48.0 <84.0 79.0 J 148 J <72.0 43,500 93.7 J ND
3/7/2018 <50.0 NA NA 106 J NA NA NA NA <52.0 NA NA 73,700 96.6 J NA
5/23/2018 <62.5 NA NA 125 J NA NA NA NA <65.0 NA NA 67,700 115 J NA
8/8/2018 <50.0 <82.0 <76.0 62.9 J <80.0 <42.0 <48.0 <84.0 <52.0 <62.0 <72.0 40,900 66.4 J ND
2/5/2019 <30.0 NA NA 72.6 J NA NA NA NA <48.8 NA NA 40,200 <44.0 NA
8/7/2019 <30.0 <46.8 <40.2 60.8 J <40.2 <55.0 <70.4 <37.0 <48.8 <34.0 <39.4 28,900 55.6 J ND
8/6/2020 <15.0 <23.4 <20.1 34.6 J <20.1 <27.5 <35.2 <18.5 <24.4 <17.0 <19.7 19,700 26.0 J ND
8/22/2021 <8.6 <12.2 <10.0 <7.6 <8.3 <10.6 <16.1 <8.5 <12.1 <12.4 <8.3 7,120 <8.4 ND
8/4/2022 <1.7 <2.4 <2.0 5.3 <1.7 <2.1 <3.2 <1.7 <2.4 <2.5 <1.7 1,420 <1.7 26.0
8/14/2013 <0.25 <0.41 1.1 10.7 7.3 <0.21 78.5 10.6 <0.26 2.3 2.4 26.7 1.1 ND
8/14/2013 DUP <0.25 <0.41 <0.38 12.4 7.9 <0.21 88.6 11.4 <0.26 2.8 2.6 28.8 1.2 ND
8/14/2014 <0.25 <0.41 5.5 7.8 13.1 0.22 J 7.0 26.5 <0.26 <0.31 3.2 9.5 0.26 J 1.5
3/11/2015 <0.25 <0.41 <0.38 6.5 10.4 <0.21 9.9 19.3 <0.26 <0.31 2.3 7.0 0.40 J ND
8/5/2015 <0.25 2.2 2.3 7.1 12.5 <0.21 12.5 24.7 <0.26 2.4 2.0 4.5 0.32 J ND
8/1/2016 <0.25 0.89 J 0.79 J 2.5 4.0 <0.21 4.5 8.4 <0.26 1.2 0.77 J 1.4 J <0.23 ND
10/6/2016 <0.25 NA NA 2.3 NA NA NA NA <0.26 NA NA 1.1 J <0.23 NA
3/2/2017 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 0.56 J
8/7/2017 <0.25 <0.41 0.61 J 1.1 2.9 <0.21 <0.24 5.3 <0.26 0.37 J <0.36 0.82 J <0.23 ND
3/7/2018 <0.25 NA NA 1.7 NA NA NA NA <0.26 NA NA 1.7 J <0.23 NA
5/23/2018 <0.25 NA NA 0.65 J NA NA NA NA <0.26 NA NA 0.85 J <0.23 NA
8/7/2018 <0.25 <0.41 <0.38 <0.30 <0.40 0.28 J <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 ND
8/7/2019 <0.15 <0.23 1.3 0.87 J 4.4 1.4 <0.35 6.5 <0.24 <0.17 <0.20 1.2 J <0.22 ND
8/6/2020 <0.15 <0.23 0.76 J <0.26 2.8 <0.28 0.56 J 3.4 <0.24 <0.17 0.31 J 5.0 <0.22 ND
8/23/2021 <0.34 <0.49 <0.40 <0.30 1.9 <0.42 <0.64 2.3 <0.48 <0.50 <0.33 <0.71 <0.34 ND
8/4/2022 <0.34 <0.49 <0.40 <0.30 3.5 <0.42 1.4 4.1 <0.48 <0.50 <0.33 <0.71 <0.34 ND
Notes are provided on the final page of this table.
TYPE II MONITORING WELLS (Continued)
KMW-6
KMW-7
Page 2 of 6
Table 2
Groundwater Results, 2013-2022
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
Contaminant of Concern
Sample ID Date Collected
1 70 70 600 70 20 6 70 600 400 400 VariesAll Other 8260B AnalytesNaphthalenen-PropylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-Trimethylbenzenem/p-Xylenessec-ButylbenzeneEthylbenzeneIsopropylbenzene (Cumene)Benzenen-ButylbenzeneMethyl Tert Butyl Ether (MTBE)o-XyleneGroundwater Clean-up Goal (ug/L)500
8/14/2013 271 42.5 463 204 30.4 <4.2 244 61.0 20.9 513 120 1,630 54.9 54.7 J
8/14/2014 169 <2.0 1.9 279 33.5 <1.0 173 47.0 15.9 385 94.8 1,060 35.8 ND
3/11/2015 89.1 <0.41 <0.38 195 30.3 0.45 J 151 51.3 7.5 154 <0.36 371 25.9 60.94 J
8/5/2015 15.6 <0.82 <0.76 51.9 23.3 <0.42 112 32.7 2.2 245 53.1 202 6.7 1,042
8/1/2016 76.9 <0.82 2.6 44.0 24.3 0.68 J 61.9 28.4 2.4 161 16.6 190 8.9 10.3 J
10/6/2016 55.2 NA NA 14.1 NA NA NA NA 1.2 NA NA 32.2 3.3 NA
11/23/2016 83.7 NA NA 31.4 NA NA NA NA 0.88 J NA NA 59.8 6.2 NA
3/2/2017 14.7 <0.41 <0.38 7.8 1.8 <0.21 15.9 2.4 0.37 J 70.5 9.6 18.5 2.8 27.86 J
4/26/2017 4.7 NA NA 1.4 NA NA NA NA <0.26 NA NA 56.3 0.67 J NA
8/9/2017 13.9 <0.41 <0.38 6.6 3.7 <0.21 30.4 2.9 0.35 J 101 <0.36 15.3 3.3 ND
3/7/2018 52.6 NA NA 17.4 NA NA NA NA 0.80 J NA NA 31.9 4.2 NA
5/23/2018 20.8 NA NA 1.4 NA NA NA NA <0.26 NA NA 6.2 3.8 NA
8/8/2018 44.1 <0.41 <0.38 21.4 10.2 0.76 J 59.4 <0.42 0.55 J 178 <0.36 16.7 4.5 3.69 J
2/5/2019 56.2 NA NA 12.3 NA NA NA NA 0.44 J NA NA 37.1 2.3 NA
8/7/2019 35.5 <0.23 <0.20 16.1 7.2 <0.28 12.7 6.0 0.95 J 32.1 <0.20 8.8 2.6 26.2
8/6/2020 42.6 <0.23 <0.20 11.1 6.4 <0.28 11.7 4.5 0.94 J 40.4 4.9 20.3 2.3 14.3 J
8/22/2021 44.9 1.7 4.8 9.1 22.9 <0.42 6.4 22.5 <0.48 9.0 1.9 5.7 <0.34 ND
8/4/2022 12.7 <0.49 1.5 3.5 9.9 <0.42 <0.64 2.7 <0.48 1.8 <0.33 <0.71 <0.34 ND
2/2/2015 <6.2 <10.2 <9.5 774 48.2 <5.2 396 107 40.6 297 96.3 541 8.5 J 47.9 J
3/11/2015 1.4 J 24.0 <1.9 535 59.8 <1.0 385 102 34.3 154 39.1 364 4.9 J ND
8/5/2015 0.91 J 13.5 <0.76 <0.60 54.4 <0.42 146 78.1 24.9 76.9 14.8 45.5 1.7 J 43.9 J
8/1/2016 <0.62 7.0 7.6 288 61.6 <0.52 229 67.4 23.3 97.4 20.3 105 2.7 44.3 J
10/6/2016 <0.25 NA NA 46.0 NA NA NA NA 5.5 NA NA 17.7 0.64 J NA
8/9/2017 <0.25 7.0 <0.38 37.9 18.3 <0.21 48.1 31.8 0.86 J 53.9 12.9 5.0 0.52 J ND
8/8/2018 <0.25 <0.41 <0.38 2.5 2.4 <0.21 5.2 1.7 0.39 J 5.9 1.2 3.3 <0.23 ND
8/7/2019 <0.15 9.1 <0.20 20.1 64.1 <0.28 110 34.2 5.1 115 31.4 33.7 4.4 33.5
8/6/2020 <0.15 1.0 <0.20 0.68 J 3.2 <0.28 21.0 <0.18 0.49 J 13.7 4.4 8.9 0.56 J 0.39 J
8/23/2021 <0.34 <0.49 <0.40 <0.30 <0.33 <0.42 3.6 <0.34 <0.48 <0.50 <0.33 <0.71 <0.34 ND
8/4/2022 <0.34 2.3 3.6 <0.30 15.2 <0.42 80.8 1.4 <0.48 3.9 4.5 2.1 1.0 2.3
8/14/2013 68.6 <0.41 <0.38 51.8 24.2 <0.21 119 46.3 3.1 40.7 19.0 10.4 0.67 J 1.3 J
3/11/2014 308 <0.41 9.6 149 90.7 0.79 J 549 136 15.4 29.4 29.3 21.8 2.6 17.6
8/14/2014 182 <0.41 <0.38 124 52.8 0.74 J 479 80.8 10.0 112 86.7 31.2 1.9 11.0
8/5/2015
8/1/2016 124 6.8 12.9 989 126 <1.0 991 208 59.9 32.8 16.5 138 3.4 J 9.2 J
10/6/2016 176 NA NA 405 NA NA NA NA 36.9 NA NA 36.2 1.4 J NA
11/23/2016 233 NA NA 878 NA NA NA NA 41.3 NA NA 134 4.4 J NA
3/2/2017 120 <4.1 <3.8 951 108 8.4 J 918 167 38.1 45.0 13.9 204 5.0 J 18.8 J
4/26/2017 118 NA NA 464 NA NA NA NA 17.7 NA NA 59.5 2.6 J NA
8/9/2017 107 <2.0 <1.9 322 37.1 <1.0 829 43.4 13.1 <1.6 36.3 43.1 2.4 J ND
3/7/2018 121 NA NA 647 NA NA NA NA 9.8 NA NA 45.7 6.3 NA
5/23/2018 36.4 NA NA 331 NA NA NA NA 1.5 J NA NA 21.6 4.1 J NA
8/8/2018 76.2 <0.82 <0.76 111 16.7 <0.42 222 26.5 2.9 <0.62 10.3 8.4 2.1 75.5
2/5/2019 77.0 NA NA 556 NA NA NA NA 22.9 NA NA 747 17.8 NA
8/6/2020 29.8 <0.47 <0.40 64.2 11.9 <0.55 273 25.6 2.0 32.8 9.0 21.9 3.0 ND
8/22/2021 13.1 <0.49 <0.40 6.3 <0.33 <0.42 50.9 <0.34 <0.48 2.4 7.7 11.7 <0.34 ND
8/1/2022
Notes are provided on the final page of this table.
COULD NOT SAMPLE - WELL WAS DRY
TYPE II MONITORING WELLS (Continued)
KMW-8
KMW-9R
KMW-12
COULD NOT SAMPLE - WELL WAS DRY
Page 3 of 6
Table 2
Groundwater Results, 2013-2022
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
Contaminant of Concern
Sample ID Date Collected
1 70 70 600 70 20 6 70 600 400 400 VariesAll Other 8260B AnalytesNaphthalenen-PropylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-Trimethylbenzenem/p-Xylenessec-ButylbenzeneEthylbenzeneIsopropylbenzene (Cumene)Benzenen-ButylbenzeneMethyl Tert Butyl Ether (MTBE)o-XyleneGroundwater Clean-up Goal (ug/L)500
8/14/2013 <50.0 <82.0 <76.0 256 <80.0 <42.0 549 <84.0 <52.0 195 J <72.0 73,700 86.5 J 510
3/11/2014 137 J <102 <95.0 336 <100 <52.5 2,270 180 J 309 217 J <90.0 63,600 178 J 48.2 J
8/14/2014 54.5 J <41.0 <38.0 99.6 J <40.0 <21.0 58.1 J <42.0 71.6 J 134 <36.0 25,700 25.9 J 33.2 J
3/11/2015 38.5 J <51.2 <47.5 328 <50.0 <26.2 163 <52.5 <32.5 222 <45.0 90,900 49.9 J ND
8/5/2015 <62.5 <102 <95.0 271 <100 <52.5 326 <105 <65.0 229 J <90.0 66,400 <57.5 ND
8/2/2016 <25.0 <41.0 <38.0 132 <40.0 <21.0 193 <42.0 <26.0 202 38.4J 21,300 <23.0 ND
10/6/2016 <12.5 NA NA 107 NA NA NA NA 16.4 J NA NA 13,800 <11.5 NA
11/23/2016 25.7 J NA NA 244 NA NA NA NA 34.5 J NA NA 20,400 <23.0 NA
3/2/2017 <12.5 <20.5 <19.0 57.5 65.9 <10.5 242 81.8 20.8 J 997 210 4,370 <11.5 ND
4/26/2017 <12.5 NA NA 82.2 NA NA NA NA 18.9 J NA NA 11,400 <11.5 NA
8/29/2017 0.38 J <0.41 <0.38 0.46 J 0.73 J <0.21 1.7 0.69 J 0.32 J 1.6 <0.36 92.7 0.35 J 18.25 J
3/12/2018 <25.0 NA NA 83.2 J NA NA NA NA <26.0 NA NA 11,200 <23.0 NA
5/23/2018 <10.0 NA NA 63.8 NA NA NA NA <10.4 NA NA 9,330 <9.2 NA
8/8/2018 1.7 <0.41 <0.38 3.6 4.2 <0.21 6.3 4.8 0.67 J 8.9 <0.36 379 0.88 J 9.0 J
2/5/2019 3.6 J NA NA 40.1 NA NA NA NA <1.2 NA NA 1,340 2.3 J NA
8/7/2019 1.5 J 0.58 0.50 19.7 11.1 <0.69 47.0 16.4 <0.61 81.7 11.5 905 1.0 J 45.5 J
8/6/2020 3.4 2.2 J <0.50 17.6 27.4 <0.69 63.5 41.9 <0.61 61.3 14.6 602 1.6 J ND
8/23/2021 <0.86 <1.2 2.6 6.4 15.6 <1.1 22.1 22.8 <1.2 5.4 <0.83 704 <0.84 20.9
8/5/2022 <1.7 <2.4 <2.0 <1.5 9.9 <2.1 20.3 14.1 <2.4 7.8 <1.7 1,040 <1.7 ND
8/14/2013 <2.5 <4.1 <3.8 8.9 J <4.0 <2.1 9.7 J <4.2 <2.6 8.0 J <3.6 6,430 <2.3 26.9
3/11/2014 <0.25 <0.41 <0.38 <0.30 <0.40 0.21 J 0.43 J <0.42 <0.26 <0.31 <0.36 2.4 <0.23 1.26 J
8/14/2014 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 0.43 J <0.42 <0.26 <0.31 <0.36 114 <0.23 ND
3/11/2015 <0.25 <0.41 <0.38 0.67 J <0.40 <0.21 0.73 J <0.42 <0.26 0.52 J <0.36 296 0.46 J 3.0
8/5/2015 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36 4.0 <0.23 ND
8/1/2016 <0.25 <0.41 <0.38 0.94 J <0.40 <0.21 0.84 J <0.42 <0.26 2.6 0.76 J 15.7 0.78 J ND
8/9/2017 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 ND
8/7/2018 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36 12.1 <0.23 ND
8/7/2019 <0.15 <0.23 <0.20 <0.26 <0.20 <0.28 <0.35 <0.18 <0.24 <0.17 <0.20 0.89 J <0.22 ND
8/6/2020 <0.15 <0.23 <0.20 <0.26 <0.20 <0.28 <0.35 <0.18 <0.24 <0.17 <0.20 167 <0.22 ND
8/22/2021 <0.34 <0.49 <0.40 <0.30 <0.33 <0.42 <0.64 <0.34 <0.48 <0.50 <0.33 <0.71 <0.34 ND
8/4/2022 <0.34 <0.49 <0.40 <0.30 <0.33 <0.42 <0.64 <0.34 <0.48 <0.50 <0.33 <0.71 <0.34 ND
8/13/2013 1.8 <0.41 <0.38 0.31 J 0.79 J 0.87 J <0.24 <0.42 <0.26 <0.31 <0.36 0.88 J <0.23 10.6 J
8/21/2014 2.7 <0.41 <0.38 <0.30 1.1 0.93 J 0.25 J 0.49 J 0.28 J 2.2 0.73 J 6.4 0.26 J 2.4 J
3/11/2015 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 0.35 J <0.42 <0.26 0.31 J <0.36 <0.66 <0.23 0.71 J
8/5/2015 <0.25 <0.41 <0.38 <0.30 <0.40 0.44 J <0.24 <0.42 <0.26 <0.31 <0.36 0.70 J <0.23 0.73 J
8/1/2016 5.3 <0.41 <0.38 0.87 J 2.9 0.89 J 2.1 2.7 0.71 J 3.3 0.82 J 5.4 0.43 J 1.73 J
8/7/2017 6.7 <0.41 <0.38 0.77 J 6.5 0.69 J 4.0 6.6 0.87 J <0.31 <0.36 3.7 <0.23 0.16 J
8/8/2018 2.8 <0.41 <0.38 8.0 4.9 0.70 J 4.0 4.6 0.79 J 16.9 <0.36 24.7 0.46 J ND
8/7/2019 <0.15 <0.23 0.65 J <0.26 5.5 1.2 0.73 J <0.18 <0.24 <0.17 5.1 2.3 <0.22 2.7
8/6/2020 <0.15 <0.23 <0.20 <0.26 <0.20 0.32 J <0.35 <0.18 <0.24 <0.17 <0.20 8.9 <0.22 ND
8/21/2021 <0.34 <0.49 <0.40 <0.30 <0.33 <0.42 <0.64 <0.34 <0.48 <0.50 <0.33 <0.71 <0.34 ND
8/3/2022 <0.34 <0.49 <0.40 <0.30 <0.33 <0.42 <0.64 <0.34 <0.48 <0.50 <0.33 <0.71 <0.34 ND
Notes are provided on the final page of this table.
TYPE II MONITORING WELLS (Continued)
KMW-13
KMW-18
KMW-14
Page 4 of 6
Table 2
Groundwater Results, 2013-2022
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
Contaminant of Concern
Sample ID Date Collected
1 70 70 600 70 20 6 70 600 400 400 VariesAll Other 8260B AnalytesNaphthalenen-PropylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-Trimethylbenzenem/p-Xylenessec-ButylbenzeneEthylbenzeneIsopropylbenzene (Cumene)Benzenen-ButylbenzeneMethyl Tert Butyl Ether (MTBE)o-XyleneGroundwater Clean-up Goal (ug/L)500
8/14/2013 225 <41.0 <38.0 740 106 <21.0 421 223 33.3 J 1,110 317 15,500 37.2 J 323
3/11/2014 71.7 <10.2 <9.5 204 19.9 J 32.1 74.2 35.2 25.8 193 54.4 9,500 28.4 ND
8/14/2014 166 <20.5 <19.0 323 81.3 <10.5 168 165 16.5 J 351 96.4 12,900 <11.5 ND
3/11/2015 245 <20.5 <19.0 513 106 <10.5 311 205 25.0 J 596 177 13,300 12.7 J ND
8/5/2015 155 <20.5 <19.0 787 99.4 <10.5 370 203 41.7 J 1,020 302 15,100 40.8 J ND
8/1/2016 <10.0 <16.4 <15.2 446 71.3 <8.4 217 154 57.4 1,290 363 8,250 308 11.7 J
10/6/2016 <10.0 NA NA 405 NA NA NA NA 94.2 NA NA 11,000 251 NA
8/9/2017 <6.2 26.6 <9.5 354 63.2 <5.2 172 129 33.6 823 170 6,170 182 ND
8/8/2018 <2.5 <4.1 <3.8 202 25.9 <2.1 92.0 68.6 <2.6 438 92.7 2,610 58.5 16.9 J
8/7/2019 22.4 <4.7 <4.0 442 57.3 <5.5 178 <3.7 20.0 717 183 7,710 351 ND
8/6/2020 26.0 <5.8 <5.0 777 91.2 <6.9 463 <4.6 23.4 J 1,440 371 8,180 174 ND
8/21/2021 <4.3 <6.1 <5.0 296 27.8 <5.3 150 <4.2 <6.1 404 101 3,750 57.2 ND
8/3/2022 <4.3 <6.1 <5.0 282 27.3 <5.3 117 47.8 15.0 372 97.9 3,800 122 ND
8/14/2013 93.6 <0.41 5.6 35.4 36.2 1.1 85.6 74.0 3.4 <0.31 43.0 276 <0.23 22.0 J
8/14/2014 47.8 <0.41 2.5 6.3 16.1 0.27 J 36.0 29.0 2.8 5.1 2.1 40.6 0.41 J ND
3/11/2015 55.2 <0.41 <0.38 52.9 41.0 0.59 J 92.4 76.0 6.8 14.3 5.7 1,360 6.5 ND
8/5/2015 25.1 6.2 3.7 23.1 19.6 <0.42 34.4 36.4 4.5 11.2 <0.72 473 0.90 J 144.8
8/1/2016 1.8 <0.41 0.92 J 6.8 1.9 <0.21 7.0 3.8 2.0 15.4 10.7 80.3 5.6 0.67 J
10/6/2016 2.3 NA NA 8.1 NA NA NA NA 1.5 NA NA 57.1 7.1 NA
8/9/2017 0.76 J <0.41 <0.38 2.2 0.84 J <0.21 3.1 2.2 <0.26 <0.31 4.1 2.5 <0.23 ND
8/8/2018 2.0 <0.41 <0.38 17.3 18.3 <0.21 42.0 43.0 2.0 17.8 26.7 399 1.2 1.58 J
8/7/2019 <0.30 3.5 3.7 17.5 15.1 <0.55 34.7 26.1 1.2 J 10.3 11.4 398 <0.44 ND
8/6/2020 1.5 J <0.47 3.7 26.2 13.2 0.74 J 14.0 22.1 4.5 16.9 9.1 309 3.1 ND
8/22/2021 <0.69 <0.98 <0.80 7.9 18.1 <0.84 38.6 28.1 2.1 37.1 14.5 353 2.6 15.3
8/3/2022 4.5 <0.49 2.8 47.6 30.3 3.7 18.1 38.6 2.0 7.7 21.0 75.9 <0.34 ND
Notes are provided on the final page of this table.
FHR TYPE II MONITORING WELLS WITHIN APEX TERMINAL
AMW-2
AMW-3
Page 5 of 6
Table 2
Groundwater Results, 2013-2022
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
Contaminant of Concern
Sample ID Date Collected
1 70 70 600 70 20 6 70 600 400 400 VariesAll Other 8260B AnalytesNaphthalenen-PropylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-Trimethylbenzenem/p-Xylenessec-ButylbenzeneEthylbenzeneIsopropylbenzene (Cumene)Benzenen-ButylbenzeneMethyl Tert Butyl Ether (MTBE)o-XyleneGroundwater Clean-up Goal (ug/L)500
8/13/2013 927 <82.0 <76.0 2,990 197 J <42.0 337 242 12,500 1,590 436 11,200 5,170 675
8/21/2014 796 <20.5 <19.0 3,110 215 <10.5 451 271 6,050 1,970 508 12,300 6,020 179.3
3/11/2015 1,120 <20.5 <19.0 3,410 <20.0 <10.5 483 293 7,290 1,890 <18.0 13,400 5,960 32.1 J
8/5/2015 780 <20.5 <19.0 2,030 180 <10.5 352 184 5,070 1,090 <18.0 8,660 3,620 84.7 J
8/1/2016 663 <41.0 <38.0 4,660 253 <21.0 505 247 12,100 1,770 480 16,300 8,350 128.1 J
8/9/2017 41.9 J <20.5 <19.0 3,240 171 <10.5 327 164 9,750 1,110 <18.0 12,600 5,940 ND
8/8/2018 <6.2 <10.2 <9.5 1,260 134 <5.2 410 226 3,560 1,700 426 5,410 3,040 54.9 J
8/7/2019 11.9 J <0.94 <8.0 2,710 121 <11.0 341 <7.4 2,640 1,040 <7.9 9,920 5,380 41.3
8/6/2020 <6.0 <9.4 <8.0 2,590 144 <11.0 550 <7.4 241 1,230 <7.9 10,600 5,410 16.9 J
8/21/2021 <17.2 <24.5 <20.0 2,730 250 <21.1 686 <17.0 247 2,260 <16.6 11,900 5,600 ND
8/3/2022 <17.2 <24.5 <20.0 2,770 253 <21.1 697 268 521 2,110 510 12,300 5,640 ND
8/14/2013 <0.25 <0.41 <0.38 <0.30 4.4 2.1 0.93 J 3.6 <0.26 <0.31 <0.36 1.2 J <0.23 27.8
8/14/2014 0.29 J <0.41 <0.38 <0.30 8.7 31.2 0.97 J 3.9 <0.26 <0.31 <0.36 1.0 J 0.36 J 154.5
3/11/2015 6.6 <0.41 <0.38 52.7 <0.40 29.3 2.3 2.9 14.9 1.4 <0.36 142 91.2 10.3
8/5/2015 <0.25 <0.41 <0.38 <0.30 <0.40 0.22 J <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 ND
8/1/2016 0.26 J <0.41 0.71 J <0.30 24.1 12.0 0.68 J 26.0 0.63 J 0.33 J <0.36 2.8 0.62 J 9.4
8/9/2017 <0.25 <0.41 1.3 1.3 12.7 4.7 10.8 16.2 0.62 J 7.2 3.9 22.4 1.0 25.9
8/8/2018 <0.25 <0.41 1.1 <0.30 16.4 4.5 0.33 J 11.9 <0.26 <0.31 <0.36 1.4 J 0.34 J 2.4
8/7/2019 <0.15 <0.23 0.84 J <0.26 17.0 6.4 26.4 7.0 <0.24 2.1 4.5 5.1 0.39 J 4.1
8/6/2020 <0.15 <0.23 0.46 J <0.26 5.5 0.95 J <0.35 1.8 <0.24 <0.17 <0.20 <0.41 <0.22 5.63 J
8/21/2021 <0.34 <0.49 <0.40 <0.30 18.4 6.2 <0.64 2.3 <0.48 <0.50 <0.33 <0.71 <0.34 5.9
8/3/2022 <0.34 <0.49 <0.40 <0.30 7.8 1.0 <0.64 1.5 <0.48 <0.50 <0.33 <0.71 <0.34 1.5
Notes:
1. All results in micrograms per liter (ug/L).
2. Groundwater results from wells sampled in 2022 are included with the past 10 years of measurements, when applicable. Historical wells and results are presented in Appendix C.
3. Shaded concentrations exceed the 15A North Carolina Administrative Code (NCAC) 2L.0202 North Carolina Groundwater Quality Standard (2L GWQS), updated April 1, 2013.
4. Refer to laboratory reports for other 8260 analytes detected.
6. October/November 2016, April 2017 and February 2019 data is from post EAB sampling events and select samples from these events were analyzed via EPA Method 8260B for BTEX constituents only.
7. March 2017 data is from a post EAB sampling event and samples were analyzed for the full 8260 list.
FHR TYPE II MONITORING WELLS WITHIN APEX TERMINAL (Continued)
5. NA = Not Analyzed; ND = Not Detected.
AMW-4
AMW-5
Page 6 of 6

FIGURES

www.tetratech.com Checked By:
Project No.:
Drawn By:11/11/2021 10:15:35 AM - P:\PROJECTS\GEORGIA-PACIFIC\SITE MANAGEMENT PROGRAM\SITE FILES\WILMINGTON, NC\CAD\FIGURE 1 - SITE LOCATION.DWG - MAHONY, MATTBar Measures 1 inch Copyright: Tetra Tech710 AVIS DRIVE, SUITE 100ANN ARBOR, MICHIGAN734.213.2204
FORMER NORTH TERMINAL - LOADING RACK
WILMINGTON, NORTH CAROLINA
N 0
SCALE:
1250' 2500'
1" = 1250'
= APPROXIMATE SITE BOUNDARIES
DRS
MEM
117-4124SMP4310
FIGURE1
NEW HANOVER COUNTY,NORTH CAROLINA
SITE
RIVER
ROAD
SHIPYARD BLVD
CAPE FEAR RIVERFLINT HILLS RESOURCES, LP
SITE LOCATION MAP
SOURCE: GOOGLE EARTH, NOVEMBER 2019
NOTES:1) FHR = FLINT HILLS RESOURCES.2) GASOLINE FUEL OIL FACILITY (GFO) REFERS TO BOTH FORMER GASOLINE AND #2 FUEL OIL FACILITIES.
3) THE GFO FACILITY RECEIVED NO FURTHER ACTION STATUS FROM NCDEQ ON DECEMBER 2, 2019.4) SITE FEATURES AND PROPERTY BOUNDARIES ARE APPROXIMATE.www.tetratech.comProject No.:MARK DATE DESCRIPTIONBY11/11/2021 1:37:50 PM - P:\PROJECTS\GEORGIA-PACIFIC\SITE MANAGEMENT PROGRAM\SITE FILES\WILMINGTON, NC\CAD\FIGURE 1 - SITE LOCATION.DWG - MAHONY, MATTChecked By:
Drawn By:
Designed By:
Bar Measures 1 inch Copyright: Tetra Tech117-4124SMP43103325 RIVER ROADWILMINGTON, NORTH CAROLINA 28412FLINT HILLS RESOURCES, LP710 AVIS DR, SUITE 100ANN ARBOR, MICHIGAN734.2132204FIGURE2 NORTH TERMINAL - LOADING RACKSITE LAYOUTM. MAHONY
M. MAHONY
D. SOPOCI
0
SCALE:
100' 200'400'
1" = 200'N
APEX OIL TERMINAL
FHR WATER
TREATMENT PLANT
FORMER FHR
LOADING RACK
FORMER FHR GASOLINE
FUEL OIL FACILITY
ASTs
AMW-2 RIVER ROADRIVER ROADAST
AST
AST
AST
AST
AST
AST
ASTAST
ASTAST
AST
SYSTEM
POND
POND
POND
TANK
STORAGE
STORAGESTORAGE
OFFICEOFFICEOFFICE
STORMWATERPOND
NC STATE AUTHORITY PROPERTY
CHEMSERVE
APEX OIL PROPERTY
APEX OIL PROPERTY
APEX OIL PROPERTY
PROPERTY
OFFICE
AMW-3
KMW-3 KMW-1
KMW-7
KMW-12
KMW-15
KMW-18
KMW-9R
AMW-4
CHEMSERVELOADINGRACKS
KMW-6
KMW-13
KMW-14
AMW-5
KMW-8
KMW-5
AMW-1
ADW-1
KDW-1
KMW-4
KMW-2
KMW-10
KMW-11
(DESTROYED)
KMW-17
KMW-16
AMW-6
(ABANDONED)
PW-1
LEGEND
MONITORING WELL
MONITORING WELL (NOT SAMPLED)
ABOVEGROUND STORAGE TANK
BUILDING NOTES: 1) MONITORING WELLS WERE INSTALLED AND SURVEYED BY PREVIOUS CONSULTANTS.2) SITE FEATURES AND PROPERTY BOUNDARIES ARE APPROXIMATE.
PROPERTY BOUNDARIES
RAILROAD TRACKS
ROAD / PARKING LOTAST www.tetratech.comProject No.:MARK DATE DESCRIPTIONBY11/14/2022 3:03:59 PM - P:\PROJECTS\GEORGIA-PACIFIC\SITE MANAGEMENT PROGRAM\SITE FILES\WILMINGTON, NC\CAD\MASTER LOADING RACK V2.1.DWG - MAHONY, MATTChecked By:
Drawn By:
Designed By:
Bar Measures 1 inch Copyright: Tetra Tech117-4124SMP43103325 RIVER ROADWILMINGTON, NORTH CAROLINA 28412FLINT HILLS RESOURCES, LP710 AVIS DR, SUITE 100ANN ARBOR, MICHIGAN734.2132204FIGURE3 NORTH TERMINAL - LOADING RACKSITE FEATURESM. MAHONY
M. MAHONY
D. SOPOCI
0
SCALE:
45' 90'180'
1" = 90'N
ASTsRIVER ROADRIVER ROADAST
AST
AST
AST
AST
AST
ASTAST
ASTAST
AST
SYSTEM
POND
POND
POND
TANK
STORAGE
STORAGESTORAGE
OFFICEOFFICEOFFICE
STORMWATER
POND
NC STATE AUTHORITY PROPERTY
CHEMSERVE
APEX OIL PROPERTY
APEX OIL PROPERTY
APEX OIL PROPERTY
PROPERTY
OFFICE
AMW-3
KMW-3 KMW-1
KMW-7
KMW-9R
AMW-4
AMW-2
KMW-1212.011.010.09.08.07.0CHEMSERVE
LOADING
RACKS
(11.05 ft)
(DRY)(22.94 ft)
(23.08 ft)
(22.75 ft)
(12.98 ft)
KMW-14
(14.03 ft)
(8.51 ft)
(7.46 ft)
(7.98 ft)(5.41 ft)
AMW-5 (11.81 ft)
(12.43 ft)6.0(22.36 ft)13.015.017.019.021.023.0KMW-8
KMW-18
KMW-6
KMW-13
LEGEND
NOTES:1) ELEVATIONS ARE BASED ON NORTH AMERICAN VERTICAL DATUM (NAVD '88) BASEPOINT.
2) STATIC GROUNDWATER MEASUREMENTS WERE RECORDED AUGUST 1, 2022.
3) POTENTIOMETRIC SURFACE CONTOURS ARE CONSISTENT WITH THOSE PRESENTED IN PREVIOUS REPORTS.
4) CONTOURS CREATED USING SURFER 16.0 WITH DEFAULT KRIGING SETTINGS.
5) MONITORING WELLS WERE INSTALLED AND SURVEYED BY PREVIOUS CONSULTANTS.
6) SITE FEATURES AND PROPERTY BOUNDARIES ARE APPROXIMATE.
MONITORING WELL
ABOVEGROUND STORAGE TANK
BUILDING
PROPERTY BOUNDARIES
RAILROAD TRACKS
ROAD / PARKING LOT
ELEVATION CONTOUR
(1 FOOT INTERVAL)
AST
15.0 www.tetratech.comProject No.:MARKDATEDESCRIPTIONBY11/30/2022 5:31:11 AM - P:\PROJECTS\GEORGIA-PACIFIC\SITE MANAGEMENT PROGRAM\SITE FILES\WILMINGTON, NC\CAD\MASTER LOADING RACK V2.1.DWG - MAHONY, MATTChecked By:
Drawn By:
Designed By:
Bar Measures 1 inch Copyright: Tetra Tech117-4124SMP43103325 RIVER ROADWILMINGTON, NORTH CAROLINA 28412FLINT HILLS RESOURCES, LP710 AVIS DR, SUITE 100ANN ARBOR, MICHIGAN734.2132204FIGURE4NORTH TERMINAL - LOADING RACKGROUNDWATER ELEVATIONCONTOURS, AUGUST 2022M. MAHONY
M. MAHONY
D. SOPOCI
0
SCALE:
45'90'180'
1" = 90'
N
ASTsRIVER ROADRIVER ROADAST
AST
AST
AST
AST
AST
ASTAST
ASTAST
AST
SYSTEM
POND
POND
POND
TANK
STORAGE
STORAGESTORAGE
OFFICEOFFICEOFFICE
STORMWATERPOND
NC STATE AUTHORITY PROPERTY
CHEMSERVE
APEX OIL PROPERTY
APEX OIL PROPERTY
APEX OIL PROPERTY
PROPERTY
OFFICE
CHEMSERVELOADINGRACKS
AMW-2
Benzene <4.3*
Ethylbenzene 282
MTBE <5.3
Naphthalene 117
Toluene 15.0
Total xylenes 3,920
AMW-3
Benzene 4.5
Ethylbenzene 47.6
MTBE 3.7
Naphthalene 18.1
Toluene 2.0
Total xylenes 75.9
AMW-4
Benzene <17.2*
Ethylbenzene 2,770
MTBE <21.1*
Naphthalene 697
Toluene 521
Total xylenes 18,000
AMW-5
Benzene <0.34
Ethylbenzene <0.30
MTBE 1.0
Naphthalene <0.64
Toluene <0.48
Total xylenes <0.71
KMW-1
Benzene <0.34
Ethylbenzene <0.30
MTBE <0.42
Naphthalene <0.64
Toluene <0.48
Total xylenes <0.71
KMW-3
Benzene 20.3
Ethylbenzene <0.30
MTBE <0.42
Naphthalene <0.64
Toluene 3.6
Total xylenes 3.7 KMW-6
Benzene <1.7*
Ethylbenzene 5.3
MTBE <2.1
Naphthalene <3.2
Toluene <2.4
Total xylenes 1,420
KMW-7
Benzene <0.34
Ethylbenzene <0.30
MTBE <0.42
Naphthalene 1.4
Toluene <0.48
Total xylenes <0.71
KMW-8
Benzene 12.7
Ethylbenzene 3.5
MTBE <0.42
Naphthalene <0.64
Toluene <0.48
Total xylenes <0.71
KMW-9R
Benzene <0.34
Ethylbenzene <0.30
MTBE <0.42
Naphthalene 80.8
Toluene <0.48
Total xylenes 3.1
KMW-13
Benzene <1.7*
Ethylbenzene <1.5
MTBE <2.1
Naphthalene 20.3
Toluene <2.4
Total xylenes 1,040
KMW-14
Benzene <0.34
Ethylbenzene <0.30
MTBE <0.42
Naphthalene <0.64
Toluene <0.48
Total xylenes <0.71
KMW-18
Benzene <0.34
Ethylbenzene <0.30
MTBE <0.42
Naphthalene <0.64
Toluene <0.48
Total xylenes <0.71
FLINT HILLS RESOURCES PROPERTY
APEXLOADINGRACKS KMW-12
LEGEND
NOTES: 1) DATA ARE PRESENTED IN MICROGRAMS PER LITER (UG/L). METHOD DETECTION LIMITS INCLUDED FOR NON-DETECT ANALYSES..
2) * = REPORTING LIMIT EXCEEDS APPLICABLE GROUNDWATER STANDARD.2) MTBE = METHYL-TERT-BUTYL ETHER.3) GROUNDWATER RESULTS COMPARED TO NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL
QUALITY 15A NCAC 02L .0202 GROUNDWATER STANDARD (2L GWQS), APRIL 1, 2013.4) MONITORING WELLS SAMPLED BY TETRA TECH BETWEEN AUGUST 3-5, 2022.5) MONITORING WELLS WERE INSTALLED AND SURVEYED BY PREVIOUS CONSULTANTS.
6) SITE FEATURES AND PROPERTY BOUNDARIES ARE APPROXIMATE.
MONITORING WELL RESULTSBELOW STANDARDS
MONITORING WELL RESULTSEXCEEDING STANDARDS
MONITORING WELL DRY
ABOVEGROUND STORAGE TANKAST
BUILDING
PROPERTY BOUNDARIES
RAILROAD TRACKS
ROAD / PARKING LOT www.tetratech.comProject No.:MARK DATE DESCRIPTIONBY8/17/2022 1:45:49 PM - P:\PROJECTS\GEORGIA-PACIFIC\SITE MANAGEMENT PROGRAM\SITE FILES\WILMINGTON, NC\CAD\MASTER LOADING RACK V2.1.DWG - MAHONY, MATTChecked By:
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Bar Measures 1 inch Copyright: Tetra Tech117-4124SMP43103325 RIVER ROADWILMINGTON, NORTH CAROLINA 28412FLINT HILLS RESOURCES, LP710 AVIS DR, SUITE 100ANN ARBOR, MICHIGAN734.2132204FIGURE5NORTH TERMINAL - LOADING RACKGROUNDWATER RESULTSVOC DETECTIONSM. MAHONY
M. MAHONY
D. SOPOCI
0
SCALE:
45'90'180'
1" = 90'
N
2L GWQS
Benzene 1
Ethylbenzene 600
MTBE 20
Naphthalene 6
Toluene 600
Total xylenes 500

APPENDICES

Appendix A
Historical Groundwater Elevations
Appendix A
Historical Groundwater Elevation Measurements
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
DATA POINT DATE DATA
COLLECTED
TOP OF
CASING
ELEVATION
(in feet)
DEPTH TO
WATER
BELOW TOC
(in feet)
FREE PHASE
PRODUCT
THICKNESS
(in feet)
SPECIFIC
GRAVITY
ADJUSTMENT
WATER
TABLE
ELEVATION
(in feet)
2/27/2002 8.03 NMT NA 11.59
2/28/2003 7.58 NMT NA 12.04
9/16/2003 7.26 NMT NA 12.36
2/19/2004 6.28 NMT NA 13.34
8/3/2004 6.28 NMT NA 13.34
2/16/2005 7.54 NMT NA 12.08
8/17/2005 5.60 NMT NA 14.02
9/21/2005 3.70 NMT NA 15.92
9/22/2005 3.79 NMT NA 15.83
2/8/2006 5.54 NMT NA 14.08
8/2/2006 6.54 NMT NA 13.08
2/5/2007 5.37 NMT NA 14.25
3/30/2007 6.60 NMT NA 13.02
8/8/2007 6.76 NMT NA 12.86
8/17/2007 7.06 NMT NA 12.56
2/20/2008 6.86 NMT NA 12.76
8/14/2008 7.04 NMT NA 12.58
2/12/2009 7.43 NMT NA 12.19
5/13/2009 7.74 NMT NA 11.88
8/17/2009 7.20 NMT NA 12.42
11/18/2009 6.75 NMT NA 12.87
5/13/2010 6.82 NMT NA 12.80
8/10/2010 7.00 NMT NA 12.62
10/14/2010 3.88 NMT NA 15.74
11/17/2010 5.22 NMT NA 14.40
2/16/2011 5.91 NMT NA 13.71
2/23/2011 6.05 NMT NA 13.57
5/26/2011 7.14 NMT NA 12.48
8/15/2011 7.43 NMT NA 12.19
11/29/2011 6.54 NMT NA 13.08
3/1/2012 7.18 NMT NA 12.44
5/22/2012 7.77 NMT NA 11.85
8/13/2012 6.08 NMT NA 13.54
10/3/2012 6.83 NMT NA 12.79
1/10/2013 6.54 NMT NA 13.08
4/18/2013 6.11 NMT NA 13.51
7/23/2013 5.17 NMT NA 14.45
8/7/2013 5.45 NMT NA 14.17
10/31/2013 6.58 NMT NA 13.04
2/13/2014 7.06 NMT NA 12.56
5/15/2014 6.15 NMT NA 13.47
8/14/2014 2.80 NMT NA 16.82
3/11/2015 5.53 NMT NA 14.09
8/5/2015 5.61 NMT NA 12.94
8/1/2016 5.59 NMT NA 12.96
8/7/2017 5.35 NMT NA 13.20
8/9/2017 4.00 NMT NA 14.55
2/7/2018 5.61 NMT NA 12.94
8/7/2019 6.85 NMT NA 11.70
8/6/2020 4.64 NMT NA 13.91
8/21/2021 4.55 NMT NA 14.00
8/1/2022 6.74 NMT NA 11.81
19.62
TYPE II MONITORING WELLS
KMW-1
18.55
Notes are provided on the final page of this table.
Page 1 of 18
Appendix A
Historical Groundwater Elevation Measurements
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
DATA POINT DATE DATA
COLLECTED
TOP OF
CASING
ELEVATION
(in feet)
DEPTH TO
WATER
BELOW TOC
(in feet)
FREE PHASE
PRODUCT
THICKNESS
(in feet)
SPECIFIC
GRAVITY
ADJUSTMENT
WATER
TABLE
ELEVATION
(in feet)
2/16/2005 7.48 NMT NA 9.80
8/17/2005 5.95 NMT NA 11.33
9/21/2005 3.63 NMT NA 13.65
9/22/2005 3.88 NMT NA 13.40
10/11/2005 2.41 NMT NA 14.87
10/14/2005 2.84 NMT NA 14.44
2/8/2006 5.71 NMT NA 11.57
8/2/2006 6.67 NMT NA 10.61
2/5/2007 5.78 NMT NA 11.50
3/30/2007 6.72 NMT NA 10.56
8/8/2007 6.90 NMT NA 10.38
8/17/2007 7.21 NMT NA 10.07
2/20/2008 6.97 NMT NA 10.31
8/14/2008 6.89 NMT NA 10.39
2/12/2009 7.38 NMT NA 9.90
5/13/2009 7.69 NMT NA 9.59
8/17/2009 7.18 NMT NA 10.10
11/18/2009 6.75 NMT NA 10.53
5/13/2010 7.01 NMT NA 10.27
8/10/2010 6.98 NMT NA 10.30
10/14/2010 4.01 NMT NA 13.27
2/16/2011 6.04 NMT NA 11.24
5/26/2011 7.28 NMT NA 10.00
8/15/2011 7.19 NMT NA 10.09
8/13/2012 5.80 NMT NA 11.48
10/3/2012 6.68 NMT NA 10.60
1/10/2013 6.57 NMT NA 10.71
4/18/2013 6.04 NMT NA 11.24
7/23/2013 5.19 NMT NA 12.09
8/7/2013 5.38 NMT NA 11.90
10/31/2013 6.53 NMT NA 10.75
2/13/2014 6.87 NMT NA 10.41
5/15/2014 6.23 NMT NA 11.05
8/14/2014 2.13 NMT NA 15.15
8/5/2015
2/7/2018 5.67 NMT NA 10.66
TYPE II MONITORING WELLS (Continued)
Notes are provided on the final page of this table.
17.28
NM
KMW-2
16.33
Page 2 of 18
Appendix A
Historical Groundwater Elevation Measurements
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
DATA POINT DATE DATA
COLLECTED
TOP OF
CASING
ELEVATION
(in feet)
DEPTH TO
WATER
BELOW TOC
(in feet)
FREE PHASE
PRODUCT
THICKNESS
(in feet)
SPECIFIC
GRAVITY
ADJUSTMENT
WATER
TABLE
ELEVATION
(in feet)
2/27/2002 6.33 NMT NA 8.30
2/28/2003 5.68 NMT NA 8.95
9/16/2003 5.59 NMT NA 9.04
2/19/2004 5.00 NMT NA 9.63
8/3/2004 4.67 NMT NA 9.96
2/16/2005 6.08 NMT NA 8.55
8/17/2005 5.42 NMT NA 9.21
9/21/2005 5.10 2.02 0.77 11.09
9/22/2005 5.04 1.36 0.77 10.64
10/11/2005 1.39 1.43 0.77 14.34
10/14/2005 4.37 0.96 0.77 11.00
11/21/2005 4.12 0.26 0.77 10.71
11/28/2005 4.75 0.10 0.77 9.96
12/8/2005 4.78 0.28 0.77 10.07
12/28/2005 4.65 0.38 0.77 10.27
2/8/2006 4.88 0.16 0.77 9.87
8/2/2006 5.42 NMT NA 9.21
2/5/2007 4.95 NMT NA 9.68
3/30/2007 6.03 NMT NA 8.60
8/8/2007 5.86 NMT NA 8.77
8/17/2007 6.20 NMT NA 8.43
2/20/2008 5.33 NMT NA 9.30
8/14/2008 5.48 NMT NA 9.15
2/12/2009 4.92 NMT NA 9.71
5/13/2009 5.92 NMT NA 8.71
8/17/2009 5.57 NMT NA 9.06
11/18/2009 5.03 NMT NA 9.60
5/13/2010 5.85 NMT NA 8.78
8/10/2010 5.67 NMT NA 8.96
10/14/2010 3.76 NMT NA 10.87
2/16/2011 5.00 NMT NA 9.63
5/26/2011 6.10 NMT NA 8.53
8/15/2011 5.70 NMT NA 8.93
8/13/2012 4.13 NMT NA 10.50
10/3/2012 5.40 NMT NA 9.23
1/10/2013 5.32 NMT NA 9.31
4/18/2013 4.85 NMT NA 9.78
7/23/2013 4.47 NMT NA 10.16
8/7/2013 4.49 NMT NA 10.14
10/31/2013 5.14 NMT NA 9.49
2/13/2014 4.95 NMT NA 9.68
5/15/2014 5.39 NMT NA 9.24
8/14/2014 2.99 NMT NA 11.64
3/11/2015 4.70 NMT NA 9.93
8/5/2015 4.28 NMT NA 9.39
8/1/2016 4.86 NMT NA 8.81
8/8/2017 4.85 NMT NA 8.82
8/9/2017 3.15 NMT NA 10.52
2/7/2018 4.50 NMT NA 9.17
8/7/2018 2.60 NMT NA 11.07
8/7/2019 5.75 NMT NA 7.92
8/6/2020 3.37 NMT NA 10.30
8/21/2021 3.75 NMT NA 9.92
8/1/2022 5.69 NMT NA 7.98
Notes are provided on the final page of this table.
TYPE II MONITORING WELLS (Continued)
14.63
KMW-3
13.67
Page 3 of 18
Appendix A
Historical Groundwater Elevation Measurements
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
DATA POINT DATE DATA
COLLECTED
TOP OF
CASING
ELEVATION
(in feet)
DEPTH TO
WATER
BELOW TOC
(in feet)
FREE PHASE
PRODUCT
THICKNESS
(in feet)
SPECIFIC
GRAVITY
ADJUSTMENT
WATER
TABLE
ELEVATION
(in feet)
2/27/2002 11.42 NMT NA 8.73
2/28/2003 11.16 NMT NA 8.99
9/16/2003 10.85 NMT NA 9.30
2/19/2004 10.32 NMT NA 9.83
8/3/2004 10.12 NMT NA 10.03
2/16/2005 11.01 NMT NA 9.14
8/17/2005 10.24 NMT NA 9.91
9/21/2005 8.80 NMT NA 11.35
9/22/2005 8.92 NMT NA 11.23
10/11/2005 7.45 NMT NA 12.70
10/14/2005 8.31 NMT NA 11.84
2/8/2006 9.87 NMT NA 10.28
8/2/2006 10.39 NMT NA 9.76
2/5/2007 9.92 NMT NA 10.23
3/30/2007 10.61 NMT NA 9.54
8/8/2007 10.57 NMT NA 9.58
8/17/2007 10.80 NMT NA 9.35
2/20/2008 10.45 NMT NA 9.70
8/14/2008 10.54 NMT NA 9.61
2/12/2009 10.75 NMT NA 9.40
5/13/2009 10.97 NMT NA 9.18
8/17/2009 10.67 NMT NA 9.48
11/18/2009 10.37 NMT NA 9.78
4/21/2010 10.30 NMT NA 9.85
5/13/2010 10.53 NMT NA 9.62
8/10/2010 10.62 NMT NA 9.53
10/14/2010 8.92 NMT NA 11.23
11/17/2010 9.71 NMT NA 10.44
2/16/2011 9.97 NMT NA 10.18
2/23/2011 10.05 NMT NA 10.10
5/26/2011 10.73 NMT NA 9.42
8/15/2011 10.80 NMT NA 9.35
11/29/2011 6.36 NMT NA 13.79
3/1/2012 10.57 NMT NA 9.58
5/22/2012 10.94 NMT NA 9.21
8/13/2012 9.70 NMT NA 10.45
10/3/2012 9.77 NMT NA 10.38
1/10/2013 10.14 NMT NA 10.01
4/18/2013 9.80 NMT NA 10.35
7/23/2013 7.28 NMT NA 12.87
8/7/2013 9.48 NMT NA 10.67
10/31/2013 10.32 NMT NA 9.83
2/13/2014 10.46 NMT NA 9.69
5/15/2014 9.90 NMT NA 10.25
8/14/2014 7.88 NMT NA 12.27
8/5/2015
2/7/2018 9.60 NMT NA 9.50
Notes are provided on the final page of this table.
TYPE II MONITORING WELLS (Continued)
20.15
NM
KMW-4
19.10
Page 4 of 18
Appendix A
Historical Groundwater Elevation Measurements
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
DATA POINT DATE DATA
COLLECTED
TOP OF
CASING
ELEVATION
(in feet)
DEPTH TO
WATER
BELOW TOC
(in feet)
FREE PHASE
PRODUCT
THICKNESS
(in feet)
SPECIFIC
GRAVITY
ADJUSTMENT
WATER
TABLE
ELEVATION
(in feet)
2/27/2002 3.74 NMT NA 12.55
2/28/2003 3.34 NMT NA 12.95
9/16/2003 2.90 NMT NA 13.39
2/19/2004 1.74 NMT NA 14.55
8/3/2004 1.85 NMT NA 14.44
2/16/2005 3.20 NMT NA 13.09
8/17/2005 0.90 NMT NA 15.39
2/8/2006 0.88 NMT NA 15.41
2/5/2007 0.23 NMT NA 16.06
3/30/2007 6.10 NMT NA 10.19
8/8/2007 6.73 NMT NA 13.72
8/17/2007 6.98 NMT NA 13.47
2/20/2008 7.00 NMT NA 13.45
8/14/2008 7.04 NMT NA 13.41
2/12/2009 7.30 NMT NA 13.15
5/13/2009 7.68 NMT NA 12.77
8/17/2009 7.03 NMT NA 13.42
11/18/2009 6.49 NMT NA 13.96
4/21/2010 6.08 NMT NA 14.37
5/13/2010 6.55 NMT NA 13.90
8/10/2010 6.73 NMT NA 13.72
10/14/2010 2.86 NMT NA 17.59
11/17/2010 5.48 NMT NA 14.97
2/16/2011 5.39 NMT NA 15.06
2/23/2011 5.61 NMT NA 14.84
5/26/2011 6.90 NMT NA 13.55
8/15/2011 7.32 NMT NA 13.13
11/29/2012 6.24 NMT NA 14.21
3/1/2012 7.29 NMT NA 13.16
5/22/2012 7.71 NMT NA 12.74
8/13/2012 5.78 NMT NA 14.67
10/3/2012 6.61 NMT NA 13.84
1/10/2013 6.23 NMT NA 14.22
4/18/2013 5.80 NMT NA 14.65
7/23/2013 4.60 NMT NA 15.85
8/7/2013 4.98 NMT NA 15.47
10/31/2013 6.32 NMT NA 14.13
2/13/2014 6.95 NMT NA 13.50
5/15/2014 5.30 NMT NA 15.15
8/14/2014 2.38 NMT NA 18.07
3/11/2015 5.11 NMT NA 15.34
8/5/2015 5.28 NMT NA 14.14
8/1/2016 5.14 NMT NA 14.28
8/9/2017 3.25 NMT NA 16.17
8/16/2017 3.35 NMT NA 16.07
2/7/2018 5.03 NMT NA 14.39
8/7/2018 1.55 NMT NA 17.87
8/7/2019 6.52 NMT NA 12.90
8/6/2020 4.05 NMT NA 15.37
8/21/2021 3.86 NMT NA 15.56
Notes are provided on the final page of this table.
TYPE II MONITORING WELLS (Continued)
20.45
16.29
19.42
KMW-5*
Page 5 of 18
Appendix A
Historical Groundwater Elevation Measurements
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
DATA POINT DATE DATA
COLLECTED
TOP OF
CASING
ELEVATION
(in feet)
DEPTH TO
WATER
BELOW TOC
(in feet)
FREE PHASE
PRODUCT
THICKNESS
(in feet)
SPECIFIC
GRAVITY
ADJUSTMENT
WATER
TABLE
ELEVATION
(in feet)
2/27/2002 4.82 NMT NA 20.08
2/28/2003 2.19 NMT NA 22.71
9/16/2003 2.21 NMT NA 22.69
2/19/2004 0.56 NMT NA 24.34
8/3/2004 1.38 NMT NA 23.52
2/16/2005 3.14 NMT NA 21.76
8/17/2005 1.53 NMT NA 23.37
2/8/2006 1.84 NMT NA 23.06
8/2/2006 2.56 NMT NA 22.34
2/5/2007 1.55 NMT NA 23.35
8/6/2007 2.72 NMT NA 22.18
2/20/2008 2.69 NMT NA 22.21
8/14/2008 2.85 NMT NA 22.05
8/17/2009 2.85 NMT NA 22.05
8/10/2010 2.61 NMT NA 22.29
8/18/2011 3.06 NMT NA 21.84
8/13/2012 1.37 NMT NA 23.53
8/7/2013 1.76 NMT NA 23.14
8/14/2014 1.07 NMT NA 23.83
3/11/2015 1.79 NMT NA 23.11
8/5/2015 0.98 NMT NA 23.98
8/1/2016 2.23 NMT NA 22.73
10/6/2016 1.72 NMT NA 23.24
11/23/2016 2.50 NMT NA 22.46
3/2/2017 2.32 NMT NA 22.64
4/26/2017 1.25 NMT NA 23.71
8/9/2017 0.97 NMT NA 23.99
2/7/2018 1.81 NMT NA 23.15
3/7/2018 1.91 NMT NA 23.05
5/23/2018 1.56 NMT NA 23.40
8/7/2018 0.25 NMT NA 24.71
2/5/2019 2.26 NMT NA 22.70
8/7/2019 2.85 NMT NA 22.11
8/6/2020 1.55 NMT NA 23.41
8/22/2021 1.48 NMT NA 23.48
8/1/2022 2.60 NMT NA 22.36
2/27/2002 4.63 NMT NA 20.48
2/28/2003 2.03 NMT NA 23.08
9/16/2003 1.92 NMT NA 23.19
2/19/2004 0.21 NMT NA 24.90
8/3/2004 0.77 NMT NA 24.34
2/16/2005 2.69 NMT NA 22.42
8/17/2005 1.20 NMT NA 23.91
2/8/2006 1.63 NMT NA 23.48
8/2/2006 2.61 NMT NA 22.50
2/5/2007 0.81 NMT NA 24.30
8/6/2007 2.15 NMT NA 22.96
2/20/2008 2.33 NMT NA 22.78
8/14/2008 2.26 NMT NA 22.85
8/17/2009 2.39 NMT NA 22.72
8/10/2010 2.10 NMT NA 23.01
8/18/2011 2.52 NMT NA 22.59
8/13/2012 1.01 NMT NA 24.10
8/7/2013 1.20 NMT NA 23.91
8/14/2014 0.93 NMT NA 24.18
3/11/2015 1.37 NMT NA 23.74
Notes are provided on the final page of this table.
TYPE II MONITORING WELLS (Continued)
24.90
25.11
KMW-6
24.96
KMW-7
Page 6 of 18
Appendix A
Historical Groundwater Elevation Measurements
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
DATA POINT DATE DATA
COLLECTED
TOP OF
CASING
ELEVATION
(in feet)
DEPTH TO
WATER
BELOW TOC
(in feet)
FREE PHASE
PRODUCT
THICKNESS
(in feet)
SPECIFIC
GRAVITY
ADJUSTMENT
WATER
TABLE
ELEVATION
(in feet)
8/5/2015 0.96 NMT NA 24.26
8/1/2016 1.79 NMT NA 23.43
10/6/2016 1.26 NMT NA 23.96
3/2/2017 2.51 NMT NA 22.71
8/7/2017 1.61 NMT NA 23.61
8/9/2017 0.50 NMT NA 24.72
2/7/2018 1.33 NMT NA 23.89
3/7/2018 1.43 NMT NA 23.79
5/23/2018 1.10 NMT NA 24.12
8/7/2018 0.00 NMT NA 25.22
8/7/2019 2.40 NMT NA 22.82
8/6/2020 1.18 NMT NA 24.04
8/22/2021 1.02 NMT NA 24.20
8/1/2022 2.14 NMT NA 23.08
2/27/2002 5.56 0.20 0.86 20.47
2/28/2003 2.41 NMT NA 23.45
9/16/2003 2.40 NMT NA 23.46
2/19/2004 0.73 NMT NA 25.13
8/3/2004 1.22 NMT NA 24.64
2/16/2005 3.18 NMT NA 22.68
8/17/2005 1.75 0.12 0.77 24.20
2/8/2006 2.15 NMT NA 23.71
8/2/2006 2.92 NMT NA 22.94
2/5/2007 1.37 0.10 0.77 24.57
8/6/2007 2.77 0.02 0.77 23.11
2/20/2008 2.82 0.07 0.77 23.09
8/14/2008 2.90 0.04 0.77 22.99
8/17/2009 2.96 NMT NA 22.90
8/10/2010 2.72 NMT NA 23.14
8/18/2011 3.17 NMT NA 22.69
8/13/2012 1.55 NMT NA 24.31
8/7/2013 1.82 NMT NA 24.04
8/14/2014 1.32 NMT NA 24.54
3/11/2015 1.86 NMT NA 24.00
8/5/2015 1.15 NMT NA 24.04
8/1/2016 2.00 NMT NA 23.19
10/6/2016 1.83 NMT NA 23.36
11/23/2016 2.40 NMT NA 22.79
3/2/2017 2.30 NMT NA 22.89
4/26/2017 1.46 NMT NA 23.73
8/9/2017 0.58 NMT NA 24.61
2/7/2018 1.51 NMT NA 23.68
3/7/2018 1.66 NMT NA 23.53
5/23/2018 1.27 NMT NA 23.92
8/7/2018 0.17 NMT NA 25.02
2/5/2019 2.36 NMT NA 22.83
8/7/2019 2.71 NMT NA 22.48
8/6/2020 1.29 NMT NA 23.90
8/22/2021 1.21 NMT NA 23.98
8/1/2022 2.44 NMT NA 22.75
2/27/2002 5.08 0.15 0.86 20.78
9/16/2003 2.69 NMT NA 23.04
2/19/2004 0.95 NMT NA 24.78
8/3/2004 1.28 NMT NA 24.45
Notes are provided on the final page of this table.
TYPE II MONITORING WELLS (Continued)
KMW-9 was abandoned on August 11, 2004.
25.73KMW-9
KMW-8
25.19
25.22KMW-7
(cont'd)
25.86
Page 7 of 18
Appendix A
Historical Groundwater Elevation Measurements
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
DATA POINT DATE DATA
COLLECTED
TOP OF
CASING
ELEVATION
(in feet)
DEPTH TO
WATER
BELOW TOC
(in feet)
FREE PHASE
PRODUCT
THICKNESS
(in feet)
SPECIFIC
GRAVITY
ADJUSTMENT
WATER
TABLE
ELEVATION
(in feet)
2/2/2015 2.86 NMT NA 24.47
3/11/2015 3.35 NMT NA 23.98
8/5/2015 3.02 NMT NA 24.23
8/1/2016 3.81 NMT NA 23.44
10/6/2016 3.21 NMT NA 24.04
8/9/2017 2.26 NMT NA 24.99
2/7/2018 3.26 NMT NA 23.99
8/7/2018 1.80 NMT NA 25.45
8/7/2019 4.56 NMT NA 22.69
8/6/2020 3.22 NMT NA 24.03
8/23/2021 3.08 NMT NA 24.17
8/1/2022 4.31 NMT NA 22.94
2/27/2002 4.87 NMT NA 20.05
2/28/2003 2.36 NMT NA 22.56
9/16/2003 2.23 NMT NA 22.69
2/19/2004 0.82 NMT NA 24.10
8/3/2004 1.06 NMT NA 23.86
2/16/2005 3.05 NMT NA 21.87
8/17/2005 1.58 NMT NA 23.34
2/8/2006 1.94 NMT NA 22.98
8/2/2006 2.49 NMT NA 22.43
2/5/2007 1.25 NMT NA 23.67
8/6/2007 2.68 NMT NA 22.24
2/20/2008 2.64 NMT NA 22.28
8/14/2008 2.85 NMT NA 22.07
8/10/2010 2.60 NMT NA 22.32
8/13/2012 1.47 NMT NA 23.45
8/14/2014 1.11 NMT NA 23.81
8/5/2015
2/7/2018 1.66 NMT NA 23.33
2/27/2002 5.70 NMT NA 21.64
2/28/2003 2.68 NMT NA 24.66
9/16/2003 2.66 NMT NA 24.68
2/19/2004 1.22 NMT NA 26.12
8/3/2004 1.6 NMT NA 25.74
2/16/2005 3.51 NMT NA 23.83
8/17/2005 1.98 NMT NA 25.36
2/8/2006 1.92 NMT NA 25.42
8/2/2006 3.26 NMT NA 24.08
2/5/2007 1.33 NMT NA 26.01
8/6/2007 3.38 NMT NA 23.96
8/14/2008 3.78 NMT NA 23.56
8/10/2010 3.32 NMT NA 24.02
8/13/2012 1.82 NMT NA 25.52
3/11/2014 2.61 NMT NA 24.73
TYPE II MONITORING WELLS (Continued)
Notes are provided on the final page of this table.
KMW-11
24.92
27.34
NM
Could not locate during August 2014 event - presumed destroyed
KMW-10
24.99
27.33
KMW-9R
27.25
Page 8 of 18
Appendix A
Historical Groundwater Elevation Measurements
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
DATA POINT DATE DATA
COLLECTED
TOP OF
CASING
ELEVATION
(in feet)
DEPTH TO
WATER
BELOW TOC
(in feet)
FREE PHASE
PRODUCT
THICKNESS
(in feet)
SPECIFIC
GRAVITY
ADJUSTMENT
WATER
TABLE
ELEVATION
(in feet)
2/27/2002 13.38 NMT NA 10.81
2/28/2003 12.27 NMT NA 11.92
9/16/2003 11.69 NMT NA 12.50
2/19/2004 10.53 NMT NA 13.66
8/3/2004 10.83 NMT NA 13.36
2/16/2005 12.18 NMT NA 12.01
8/17/2005 9.76 NMT NA 14.43
2/8/2006 9.88 NMT NA 14.31
8/2/2006 11.47 NMT NA 12.72
2/5/2007 9.45 NMT NA 14.74
8/6/2007 11.83 NMT NA 12.36
2/20/2008 12.36 NMT NA 11.83
8/14/2008 12.11 NMT NA 12.08
2/12/2009 12.56 NMT NA 11.63
5/13/2009 12.95 NMT NA 11.24
8/17/2009 12.10 NMT NA 12.09
8/10/2010 11.57 NMT NA 12.62
10/14/2010 6.27 NMT NA 17.92
2/16/2011 10.28 NMT NA 13.91
5/26/2011 12.08 NMT NA 12.11
8/18/2011 12.39 NMT NA 11.80
8/13/2012 10.71 NMT NA 13.48
10/3/2012 11.50 NMT NA 12.69
1/10/2013 11.16 NMT NA 13.03
4/18/2013 10.73 NMT NA 13.46
7/23/2013 9.02 NMT NA 15.17
8/7/2013 9.41 NMT NA 14.78
10/31/2013 11.06 NMT NA 13.13
2/13/2014 11.98 NMT NA 12.21
3/11/2014 11.36 NMT NA 12.83
5/15/2014 10.55 NMT NA 13.64
8/14/2014 6.70 NMT NA 17.49
8/5/2015 DRY NMT NA NA
8/1/2016 9.74 NMT NA 14.56
10/6/2016 7.79 NMT NA 16.51
11/23/2016 2.29 NMT NA 22.01
3/2/2017 10.90 NMT NA 13.40
4/26/2017 9.75 NMT NA 14.55
8/9/2017 8.79 NMT NA 15.51
2/7/2018 9.91 NMT NA 14.39
3/7/2018 10.15 NMT NA 14.15
5/23/2018 9.66 NMT NA 14.64
8/7/2018 4.95 NMT NA 19.35
2/5/2019 8.50 NMT NA 15.80
8/7/2019 DRY NMT NA NA
8/6/2020 9.32 NMT NA 14.98
8/22/2021 8.80 NMT NA 15.50
8/1/2022 DRY NMT NA NA
TYPE II MONITORING WELLS (Continued)
Notes are provided on the final page of this table.
24.30
24.19
KMW-12
Page 9 of 18
Appendix A
Historical Groundwater Elevation Measurements
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
DATA POINT DATE DATA
COLLECTED
TOP OF
CASING
ELEVATION
(in feet)
DEPTH TO
WATER
BELOW TOC
(in feet)
FREE PHASE
PRODUCT
THICKNESS
(in feet)
SPECIFIC
GRAVITY
ADJUSTMENT
WATER
TABLE
ELEVATION
(in feet)
2/27/2002 12.80 NMT NA 11.04
2/28/2003 11.82 NMT NA 12.02
9/16/2003 11.29 NMT NA 12.55
2/19/2004 10.07 NMT NA 13.77
8/3/2004 10.32 NMT NA 13.52
2/16/2005 11.74 NMT NA 12.10
8/17/2005 9.30 NMT NA 14.54
2/8/2006 5.38 NMT NA 18.46
8/2/2006 10.87 NMT NA 12.97
2/5/2007 8.41 NMT NA 15.43
8/6/2007 11.26 NMT NA 12.58
2/20/2008 11.72 NMT NA 12.12
8/14/2008 11.31 NMT NA 12.53
2/12/2009 11.93 NMT NA 11.91
5/13/2009 11.65 NMT NA 12.19
8/17/2009 11.53 NMT NA 12.31
8/10/2010 11.05 NMT NA 12.79
10/14/2010 5.81 NMT NA 18.03
2/16/2011 9.66 NMT NA 14.18
5/26/2011 11.46 NMT NA 12.38
8/18/2011 11.35 NMT NA 12.49
8/13/2012 10.02 NMT NA 13.82
10/3/2012 11.02 NMT NA 12.82
1/10/2013 10.68 NMT NA 13.16
4/18/2013 10.21 NMT NA 13.63
7/23/2013 8.63 NMT NA 15.21
8/7/2013 9.03 NMT NA 14.81
10/31/2013 10.56 NMT NA 13.28
2/13/2014 11.13 NMT NA 12.71
3/11/2014 10.83 NMT NA 13.01
5/15/2014 10.10 NMT NA 13.74
8/14/2014 6.11 NMT NA 17.73
3/11/2015 9.42 NMT NA 14.42
8/5/2015 9.85 NMT NA 14.08
8/1/2016 9.26 NMT NA 14.67
10/6/2016 6.91 NMT NA 17.02
11/23/2016 9.15 NMT NA 14.78
3/2/2017 9.51 NMT NA 14.42
4/26/2017 9.58 NMT NA 14.35
8/9/2017 6.40 NMT NA 17.53
8/29/2017 6.25 NMT NA 17.68
2/7/2018 4.50 NMT NA 19.43
3/12/2018 9.61 NMT NA 14.32
5/23/2018 8.81 NMT NA 15.12
8/7/2018 4.50 NMT NA 19.43
2/5/2019 7.42 NMT NA 16.51
8/7/2019 8.75 NMT NA 15.18
8/6/2020 8.84 NMT NA 15.09
8/22/2021 7.88 NMT NA 16.05
8/1/2022 9.90 NMT NA 14.03
TYPE II MONITORING WELLS (Continued)
Notes are provided on the final page of this table.
23.84
KMW-13
23.93
Page 10 of 18
Appendix A
Historical Groundwater Elevation Measurements
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
DATA POINT DATE DATA
COLLECTED
TOP OF
CASING
ELEVATION
(in feet)
DEPTH TO
WATER
BELOW TOC
(in feet)
FREE PHASE
PRODUCT
THICKNESS
(in feet)
SPECIFIC
GRAVITY
ADJUSTMENT
WATER
TABLE
ELEVATION
(in feet)
2/27/2002 11.99 NMT NA 11.32
2/28/2003 11.13 NMT NA 12.18
9/16/2003 10.66 NMT NA 12.65
2/19/2004 9.28 NMT NA 14.03
8/3/2004 9.50 NMT NA 13.81
2/16/2005 11.07 NMT NA 12.24
8/17/2005 8.56 NMT NA 14.75
2/8/2006 8.59 NMT NA 14.72
8/2/2006 10.03 NMT NA 13.28
2/5/2007 8.09 NMT NA 15.22
8/6/2007 10.45 NMT NA 12.86
2/20/2008 10.88 NMT NA 12.43
8/14/2008 10.71 NMT NA 12.60
2/12/2009 11.14 NMT NA 12.17
5/13/2009 11.54 NMT NA 11.77
8/17/2009 10.75 NMT NA 12.56
8/10/2010 10.35 NMT NA 12.96
10/14/2010 5.44 NMT NA 17.87
2/16/2011 8.90 NMT NA 14.41
5/26/2011 10.68 NMT NA 12.63
8/18/2011 11.05 NMT NA 12.26
8/13/2012 9.24 NMT NA 14.07
10/3/2012 10.33 NMT NA 12.98
1/10/2013 9.98 NMT NA 13.33
4/18/2013 9.45 NMT NA 13.86
7/23/2013 7.94 NMT NA 15.37
8/7/2013 8.37 NMT NA 14.94
10/31/2013 9.99 NMT NA 13.32
2/13/2014 10.80 NMT NA 12.51
3/11/2014 10.13 NMT NA 13.18
5/15/2014 9.39 NMT NA 13.92
8/14/2014 5.59 NMT NA 17.72
3/11/2015 8.72 NMT NA 14.59
8/5/2015 9.02 NMT NA 14.30
8/1/2016 8.70 NMT NA 14.62
8/9/2017 7.60 NMT NA 15.72
2/7/2018 8.64 NMT NA 14.68
8/7/2018 3.98 NMT NA 19.34
8/7/2019 10.18 NMT NA 13.14
8/6/2020 7.73 NMT NA 15.59
8/22/2021 7.36 NMT NA 15.96
8/1/2022 10.34 NMT NA 12.98
TYPE II MONITORING WELLS (Continued)
Notes are provided on the final page of this table.
23.31
KMW-14
23.32
Page 11 of 18
Appendix A
Historical Groundwater Elevation Measurements
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
DATA POINT DATE DATA
COLLECTED
TOP OF
CASING
ELEVATION
(in feet)
DEPTH TO
WATER
BELOW TOC
(in feet)
FREE PHASE
PRODUCT
THICKNESS
(in feet)
SPECIFIC
GRAVITY
ADJUSTMENT
WATER
TABLE
ELEVATION
(in feet)
8/17/2005 9.90 NMT NA 16.32
2/8/2006 9.56 NMT NA -9.56
8/2/2006 10.98 NMT NA -10.98
2/5/2007 9.13 NMT NA 17.09
3/30/2007 10.70 NMT NA 15.52
8/8/2007 11.42 NMT NA 14.80
8/17/2007 11.80 NMT NA 14.42
2/20/2008 12.08 NMT NA 14.14
8/14/2008 11.91 NMT NA 14.31
2/12/2009 12.16 NMT NA 14.06
5/13/2009 12.68 NMT NA 13.54
8/17/2009 11.82 NMT NA 14.40
11/18/2009 11.27 NMT NA 14.95
5/13/2010 11.25 NMT NA 14.97
8/10/2010 11.54 NMT NA 14.68
2/16/2011 10.02 NMT NA 16.20
5/26/2011 11.60 NMT NA 14.62
8/15/2011 12.17 NMT NA 14.05
8/13/2012 10.55 NMT NA 15.67
10/3/2012 11.39 NMT NA 14.83
1/10/2013 10.99 NMT NA 15.23
4/18/2013 10.58 NMT NA 15.64
7/23/2013 9.22 NMT NA 17.00
8/7/2013 9.63 NMT NA 16.59
10/31/2013 11.10 NMT NA 15.12
2/13/2014 11.87 NMT NA 14.35
3/11/2014 11.21 NMT NA 15.01
5/15/2014 10.50 NMT NA 15.72
8/14/2014 6.97 NMT NA 19.25
8/5/2015
2/7/2018 9.51 NMT NA 15.72
8/17/2005 7.21 NMT NA 22.94
2/8/2006 7.07 NMT NA 23.08
8/2/2006 8.28 NMT NA 21.87
2/5/2007 6.72 NMT NA 23.43
8/6/2007 8.57 NMT NA 21.58
2/20/2008 8.42 NMT NA 21.73
8/14/2008 9.01 NMT NA 21.14
8/17/2009 7.93 NMT NA 22.22
8/10/2010 8.60 NMT NA 21.55
8/13/2012 7.55 NMT NA 22.60
8/14/2014 5.59 NMT NA 24.56
8/5/2015
2/7/2018 6.87 NMT NA 23.38
TYPE II MONITORING WELLS (Continued)
26.22
Notes are provided on the final page of this table.
30.15
NM
NM
KMW-16
30.25
KMW-15
25.23
Page 12 of 18
Appendix A
Historical Groundwater Elevation Measurements
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
DATA POINT DATE DATA
COLLECTED
TOP OF
CASING
ELEVATION
(in feet)
DEPTH TO
WATER
BELOW TOC
(in feet)
FREE PHASE
PRODUCT
THICKNESS
(in feet)
SPECIFIC
GRAVITY
ADJUSTMENT
WATER
TABLE
ELEVATION
(in feet)
8/17/2005 7.08 NMT NA 23.48
2/8/2006 7.41 NMT NA 23.15
8/2/2006 7.88 NMT NA 22.68
2/5/2007 6.72 NMT NA 23.84
8/6/2007 8.15 NMT NA 22.41
2/20/2008 8.09 NMT NA 22.47
8/14/2008 8.28 NMT NA 22.28
8/17/2009 8.53 NMT NA 22.03
8/10/2010 8.23 NMT NA 22.33
8/13/2012 7.23 NMT NA 23.33
8/14/2014 6.06 NMT NA 24.50
8/15/2015
2/7/2018 7.24 NMT NA 23.42
8/15/2011 3.69 NMT NA 7.77
8/13/2012 2.70 NMT NA 8.76
8/7/2013 2.90 NMT NA 8.56
8/14/2014 1.39 NMT NA 10.07
3/11/2015 2.76 NMT NA 8.70
8/5/2015 2.67 NMT NA 7.95
8/1/2016 2.59 NMT NA 8.03
8/7/2017 2.75 NMT NA 7.87
8/9/2017 1.95 NMT NA 8.67
2/7/2018 3.03 NMT NA 7.59
8/7/2018 0.40 NMT NA 10.22
8/7/2019 3.33 NMT NA 7.29
8/6/2020 1.93 NMT NA 8.69
8/21/2021 1.80 NMT NA 8.82
8/1/2022 3.16 NMT NA 7.46
2/19/2004 10.03 NMT NA 13.39
8/3/2004 10.55 NMT NA 12.87
2/16/2005 11.65 NMT NA 11.77
8/17/2005 9.53 NMT NA 13.89
2/8/2006 9.70 NMT NA 13.72
8/2/2006 11.94 NMT NA 11.48
8/6/2007 11.79 NMT NA 11.50
2/20/2008 12.27 NMT NA 11.02
8/14/2008 12.27 NMT NA 11.02
8/17/2009 12.36 NMT NA 10.93
8/10/2010 11.90 NMT NA 11.39
10/14/2010 5.28 NMT NA 18.01
8/18/2011 12.50 NMT NA 10.79
8/13/2012 10.82 NMT NA 12.47
8/7/2013 8.89 NMT NA 14.40
8/14/2014 5.84 NMT NA 17.45
3/11/2015 9.52 NMT NA 13.77
8/5/2015 9.41 NMT NA 13.90
8/1/2016 8.72 NMT NA 14.59
8/8/2017 8.24 NMT NA 15.07
8/9/2017 6.90 NMT NA 16.41
2/7/2018 9.12 NMT NA 14.19
8/7/2018 3.10 NMT NA 20.21
8/7/2019 10.83 NMT NA 12.48
8/6/2020 8.62 NMT NA 14.69
8/21/2021 8.32 NMT NA 14.99
TYPE II MONITORING WELLS (Continued)
Notes are provided on the final page of this table.
NM
KMW-18
30.56
23.29
FHR TYPE II MONITORING WELLS WITHIN APEX TERMINAL
10.62
30.66
23.42
KMW-17
AMW-1*
23.31
11.46
Page 13 of 18
Appendix A
Historical Groundwater Elevation Measurements
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
DATA POINT DATE DATA
COLLECTED
TOP OF
CASING
ELEVATION
(in feet)
DEPTH TO
WATER
BELOW TOC
(in feet)
FREE PHASE
PRODUCT
THICKNESS
(in feet)
SPECIFIC
GRAVITY
ADJUSTMENT
WATER
TABLE
ELEVATION
(in feet)
2/19/2004 9.99 NMT NA 13.36
8/3/2004 10.32 NMT NA 13.03
2/16/2005 11.54 NMT NA 11.81
8/17/2005 9.25 NMT NA 14.10
9/21/2005 6.80 NMT NA 16.55
9/22/2005 6.88 NMT NA 16.47
2/8/2006 9.35 NMT NA 14.00
8/2/2006 11.00 NMT NA 12.35
2/5/2007 8.97 NMT NA 14.38
8/6/2007 11.29 NMT NA 12.06
2/20/2008 11.79 NMT NA 11.56
8/14/2008 11.58 NMT NA 11.77
8/17/2009 11.62 NMT NA 11.73
8/10/2010 11.05 NMT NA 12.30
10/14/2010 5.69 NMT NA 17.66
8/18/2011 11.88 NMT NA 11.47
8/13/2012 10.28 NMT NA 13.07
8/7/2013 8.92 NMT NA 14.43
3/11/2014 10.90 NMT NA 12.45
3/11/2015 9.37 NMT NA 13.98
8/5/2015 9.73 NMT NA 13.72
8/1/2016 9.05 NMT NA 14.40
10/6/2016 7.08 NMT NA 16.37
8/9/2017 8.20 NMT NA 15.25
2/7/2018 9.23 NMT NA 14.22
8/7/2018 4.39 NMT NA 19.06
8/7/2019 10.84 NMT NA 12.61
8/6/2020 8.71 NMT NA 14.74
8/21/2021 8.22 NMT NA 15.23
8/1/2022 11.02 NMT NA 12.43
2/19/2004 9.85 NMT NA 11.87
8/3/2004 9.97 NMT NA 11.75
2/16/2005 11.37 NMT NA 10.35
8/17/2005 9.31 NMT NA 12.41
9/21/2005 7.18 NMT NA 14.54
9/22/2005 7.24 NMT NA 14.48
2/8/2006 9.43 NMT NA 12.29
8/2/2006 10.94 NMT NA 10.78
2/5/2007 9.04 NMT NA 12.68
8/6/2007 10.83 NMT NA 10.89
2/20/2008 11.17 NMT NA 10.55
8/14/2008 11.02 NMT NA 10.70
8/17/2009 11.38 NMT NA 10.34
8/10/2010 11.07 NMT NA 10.65
10/14/2010 6.83 NMT NA 14.89
8/18/2011 11.41 NMT NA 10.31
8/7/2013 8.93 NMT NA 12.79
8/14/2014 6.53 NMT NA 15.19
3/11/2015 9.39 NMT NA 12.33
8/5/2015 9.00 NMT NA 12.82
8/1/2016 8.95 NMT NA 12.87
10/6/2016 7.48 NMT NA 14.34
8/9/2017 6.95 NMT NA 14.87
2/7/2018 9.19 NMT NA 12.63
8/7/2018 5.53 NMT NA 16.29
8/7/2019 10.75 NMT NA 11.07
8/6/2020 8.46 NMT NA 13.36
8/22/2021 8.21 NMT NA 13.61
8/1/2022 10.77 NMT NA 11.05
Notes are provided on the final page of this table.
FHR TYPE II MONITORING WELLS WITHIN APEX TERMINAL (Continued)
21.82
23.35
21.72
AMW-2
AMW-3
23.45
Page 14 of 18
Appendix A
Historical Groundwater Elevation Measurements
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
DATA POINT DATE DATA
COLLECTED
TOP OF
CASING
ELEVATION
(in feet)
DEPTH TO
WATER
BELOW TOC
(in feet)
FREE PHASE
PRODUCT
THICKNESS
(in feet)
SPECIFIC
GRAVITY
ADJUSTMENT
WATER
TABLE
ELEVATION
(in feet)
2/19/2004 6.54 NMT NA 8.62
8/3/2004 6.90 0.8 0.86 8.95
2/16/2005 9.40 2.10 0.77 7.38
8/17/2005 7.25 1.45 0.77 9.03
9/21/2005 4.16 0.04 0.77 11.03
9/22/2005 4.32 0.04 0.77 10.87
2/8/2006 6.14 0.15 0.77 9.14
8/2/2006 7.33 0.21 0.77 7.99
2/5/2007 5.93 NMT NA 9.23
3/30/2007 7.00 NMT NA 8.16
8/8/2007 7.19 NMT NA 7.97
8/17/2007 7.55 NMT NA 7.61
2/20/2008 7.31 NMT NA 7.85
8/14/2008 7.10 NMT NA 8.06
2/12/2009 7.69 NMT NA 7.47
5/13/2009 8.00 NMT NA 7.16
8/17/2009 7.54 NMT NA 7.62
11/18/2009 6.92 NMT NA 8.24
8/10/2010 7.25 NMT NA 7.91
2/16/2011 6.39 NMT NA 8.77
5/26/2011 7.63 NMT NA 7.53
8/15/2011 7.32 NMT NA 7.84
8/13/2012 5.85 NMT NA 9.31
1/10/2013 6.75 NMT NA 8.41
4/17/2013 6.12 NMT NA 9.04
7/23/2013 5.35 NMT NA 9.81
8/7/2013 5.57 NMT NA 9.59
10/31/2013 6.67 NMT NA 8.49
2/13/2014 7.04 NMT NA 8.12
5/15/2014 6.43 NMT NA 8.73
8/14/2014 3.30 NMT NA 11.86
3/11/2015 5.99 NMT NA 9.17
8/5/2015 5.37 NMT NA 9.80
8/1/2016 5.53 NMT NA 9.64
8/9/2017 3.30 NMT NA 11.87
2/7/2018 5.74 NMT NA 9.43
8/7/2018 2.33 NMT NA 12.84
8/7/2019 6.85 NMT NA 8.32
8/6/2020 4.57 NMT NA 10.60
8/21/2021 4.58 NMT NA 10.59
8/1/2022 6.66 NMT NA 8.51
Notes are provided on the final page of this table.
FHR TYPE II MONITORING WELLS WITHIN APEX TERMINAL (Continued)
15.16
15.17
AMW-4
Page 15 of 18
Appendix A
Historical Groundwater Elevation Measurements
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
DATA POINT DATE DATA
COLLECTED
TOP OF
CASING
ELEVATION
(in feet)
DEPTH TO
WATER
BELOW TOC
(in feet)
FREE PHASE
PRODUCT
THICKNESS
(in feet)
SPECIFIC
GRAVITY
ADJUSTMENT
WATER
TABLE
ELEVATION
(in feet)
2/19/2004 4.42 NMT NA 5.96
8/3/2004 4.52 NMT NA 5.86
2/16/2005 5.40 NMT NA 4.98
8/17/2005 4.58 NMT NA 5.80
9/21/2005 4.09 NMT NA 6.29
9/22/2005 4.40 NMT NA 5.98
2/8/2006 4.56 NMT NA 5.82
8/2/2006 6.00 NMT NA 4.38
2/5/2007 4.61 NMT NA 5.77
8/6/2007 5.43 NMT NA 4.95
2/20/2008 4.55 NMT NA 5.83
8/14/2008 4.76 NMT NA 5.62
8/17/2009 5.14 NMT NA 5.24
8/10/2010 5.66 NMT NA 4.72
10/14/2010 4.67 NMT NA 5.71
2/16/2011 4.81 NMT NA 5.57
5/26/2011 5.88 NMT NA 4.50
8/18/2011 4.83 NMT NA 5.55
8/13/2012 4.18 NMT NA 6.20
8/7/2013 4.98 NMT NA 5.40
8/14/2014 3.34 NMT NA 7.04
3/11/2015 4.90 NMT NA 5.48
8/5/2015 3.71 NMT NA 6.89
8/1/2016 4.98 NMT NA 5.62
8/9/2017 3.70 NMT NA 6.90
2/7/2018 4.77 NMT NA 5.83
8/7/2018 3.92 NMT NA 6.68
8/7/2019 5.23 NMT NA 5.37
8/6/2020 4.20 NMT NA 6.40
8/21/2021 4.39 NMT NA 6.21
8/1/2022 5.19 NMT NA 5.41
2/19/2004 6.80 NMT NA 5.17
8/3/2004 6.76 NMT NA 5.21
2/16/2005 7.69 NMT NA 4.28
8/17/2005 6.92 NMT NA 5.05
9/21/2005 6.09 NMT NA 5.88
9/22/2005 6.17 NMT NA 5.80
2/8/2006 7.03 NMT NA 4.94
8/2/2006 8.68 NMT NA 3.29
2/5/2007 6.64 NMT NA 5.33
8/6/2007 7.25 NMT NA 4.72
2/20/2008 7.13 NMT NA 4.84
8/14/2008 7.30 NMT NA 4.67
8/17/2009 7.48 NMT NA 4.49
8/10/2010 7.43 NMT NA 4.54
10/14/2010 6.16 NMT NA 5.81
2/16/2011 6.88 NMT NA 5.09
5/26/2011 6.66 NMT NA 5.31
8/13/2012 6.62 NMT NA 5.35
8/7/2013 6.74 NMT NA 5.23
8/14/2014 4.19 NMT NA 7.78
3/11/2015 6.33 NMT NA 5.64
8/5/2015 5.99 NMT NA 5.89
8/1/2016 6.28 NMT NA 5.60
8/9/2017 4.45 NMT NA 7.43
2/7/2018 6.19 NMT NA 5.69
8/7/2018
Notes are provided on the final page of this table.
FHR TYPE II MONITORING WELLS WITHIN APEX TERMINAL (Continued)
10.60
11.97
AMW-5
AMW-6
10.38
11.88
Abandoned
Page 16 of 18
Appendix A
Historical Groundwater Elevation Measurements
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
DATA POINT DATE DATA
COLLECTED
TOP OF
CASING
ELEVATION
(in feet)
DEPTH TO
WATER
BELOW TOC
(in feet)
FREE PHASE
PRODUCT
THICKNESS
(in feet)
SPECIFIC
GRAVITY
ADJUSTMENT
WATER
TABLE
ELEVATION
(in feet)
3/11/2015 8.46 NMT NA 18.58
3/12/2015 10.27 NMT NA 16.77
8/5/2015 8.67 NMT NA 18.37
8/1/2016 8.33 NMT NA 18.71
8/8/2017 8.45 NMT NA 18.59
8/9/2017 6.74 NMT NA 20.30
2/7/2018 8.11 NMT NA 18.93
8/7/2018 4.18 NMT NA 22.86
8/7/2019 9.77 NMT NA 17.27
8/6/2020 7.71 NMT NA 19.33
8/23/2021 7.49 NMT NA 19.55
3/11/2014 8.95 NMT NA 14.61
4/9/2014 8.40 NMT NA 15.16
5/20/2014 8.18 NMT NA 15.38
8/14/2014 4.86 NMT NA 18.70
10/23/2014 7.35 NMT NA 16.21
3/11/20115 7.50 NMT NA 16.06
8/5/2015 7.59 NMT NA 15.94
8/1/2016 7.22 NMT NA 16.31
8/9/2017 5.65 NMT NA 17.88
2/7/2018 6.24 NMT NA 17.29
8/7/2018 2.75 NMT NA 20.78
8/7/2019 8.75 NMT NA 14.78
8/6/2020 7.04 NMT NA 16.49
8/22/2021 6.22 NMT NA 17.31
ATW-1 10/23/2014 --9.70 NMT NA NA
ATW-2 10/23/2014 --9.59 NMT NA NA
GW-10 7/22/2005 --7.00 1.50 0.77 NA
GW-11 7/22/2005 --3.50 NMT NA NA
9/21/2005 19.14 5.60 NMT NA 13.54
9/22/2005 19.14 5.78 NMT NA 13.36
9/21/2005 18.76 5.59 0.09 0.77 13.24
9/22/2005 18.76 5.81 0.08 0.77 13.01
9/21/2005 18.55 5.59 NMT NA 12.96
9/22/2005 18.55 5.80 NMT NA 12.75
9/21/2005 18.21 5.44 NMT NA 12.77
9/22/2005 18.21 5.70 NMT NA 12.51
9/21/2005 18.11 6.09 0.51 0.77 12.41
9/22/2005 18.11 6.14 0.30 0.77 12.20
9/21/2005 17.72 6.13 0.68 0.77 12.11
9/22/2005 17.72 6.22 0.50 0.77 11.89
9/21/2005 13.96 3.81 1.84 0.77 11.57
9/22/2005 13.96 4.22 2.11 0.77 11.36
9/21/2005 13.49 2.98 1.03 0.77 11.30
9/22/2005 13.49 3.17 1.05 0.77 11.13
9/21/2005 13.98 3.35 NMT NA 10.63
9/22/2005 13.98 3.56 NMT NA 10.42
9/21/2005 13.61 2.96 NMT NA 10.65
9/22/2005 13.61 3.12 NMT NA 10.49
9/21/2005 13.58 3.05 NMT NA 10.53
9/22/2005 13.58 3.10 NMT NA 10.48
Notes are provided on the final page of this table.
KDW-1 27.04
TW-02
TW-01
ADW-1
TW-11
TW-09
TW-08
23.56
TW-07
TW-04
TW-03
TW-06
TEMPORARY WELLS ABONDONED AFTER SAMPLING
TW-05
23.53
TW-10
TYPE III MONITORING WELLS
FHR TYPE III MONITORING WELLS WITHIN APEX TERMINAL
Page 17 of 18
Appendix A
Historical Groundwater Elevation Measurements
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
DATA POINT DATE DATA
COLLECTED
TOP OF
CASING
ELEVATION
(in feet)
DEPTH TO
WATER
BELOW TOC
(in feet)
FREE PHASE
PRODUCT
THICKNESS
(in feet)
SPECIFIC
GRAVITY
ADJUSTMENT
WATER
TABLE
ELEVATION
(in feet)
9/21/2005 12.98 2.55 NMT NA 10.43
9/22/2005 12.98 2.56 NMT NA 10.42
9/21/2005 12.24 1.96 NMT NA 10.28
9/22/2005 12.24 1.93 NMT NA 10.31
9/21/2005 12.61 2.17 NMT NA 10.44
9/22/2005 12.61 2.13 NMT NA 10.48
9/21/2005 12.74 2.66 NMT NA 10.08
9/22/2005 12.74 2.65 NMT NA 10.09
9/21/2005 11.67 1.84 NMT NA 9.83
9/22/2005 11.67 1.82 NMT NA 9.85
9/21/2005 11.09 3.13 NMT NA 7.96
9/22/2005 11.09 3.18 NMT NA 7.91
TW-18 10/11/2005 NA 1.12 1.54 NA NA
TW-19 10/11/2005 NA 2.55 NMT NA NA
Specific gravity adjustment for gasoline is 0.77.
NMT = No Measurable Thickness
NA = Not Applicable
TOC = Top of Casing
* = TOC elevation changed during the August 2007 reporting period.
Top of Casing Elevations surveyed by Paramounte Engineering, Inc. in June 2015
Per Apex personnel on 8/7/18, AMW-6 has been abandoned.
TEMPORARY WELLS ABONDONED AFTER SAMPLING (Continued)
Specific gravity adjustment for para-xylene is 0.86.
TW-13
TW-14
TW-15
TW-16
TW-17
TW-12
October/November 2016 and March/April 2017 data was obtained during post EAB sampling on 10/6/16, 11/23/16, 3/2/17 and 4/26/17,
respectively.
The referenced gauging data at monitoring wells KMW-8, KMW-12 and KMW-13 between September 2006 and August 2009 is for only
February and August events. Gauging data collected other months during this time period was previously reported.
EAB = Enhanced Anaerobic Bioremediation
Page 18 of 18

Appendix B

Historical Groundwater Field Measurements

Appendix B
Historical Groundwater Water Quality Measurements
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
Well ID Date
Measured
Time of
Measurement
Dissolved
Oxygen
(mg/L)
pH
(Standard
Units)
Specific
Conductivity
(mS/cm)
Temperature
(°C)
Redox-
Potential
(mV)
Turbidity
(NTU)
8/1/2016 18:00 0.35 7.14 0.149 28.26 -84.7 26.8
8/7/2017 14:30 0.74 6.97 0.262 27.32 -20.6 14.2
8/7/2019 9:40 0.68 6.12 0.278 28.15 -170.0 22.4
8/6/2020 10:55 0.96 6.73 0.172 28.40 -20.9 18.6
8/21/2021 8:30 2.65 6.79 0.089 27.94 79.0 58.6
8/3/2022 14:10 NR 6.85 0.128 28.81 -98.0 0.4
8/1/2016 18:45 0.96 6.65 0.201 26.38 -93.4 7.21
8/8/2017 8:05 0.66 6.08 0.140 24.62 -29.4 15.5
8/7/2019 10:10 1.67 5.65 0.222 25.84 -153.5 20.9
8/6/2020 13:00 0.03 6.18 0.255 27.45 -100.6 1.19
8/21/2021 10:50 0.00 6.46 0.254 28.89 -169 11.2
8/3/2022 13:45 NR 6.32 0.140 26.59 -95 7.0
8/1/2016 17:10 0.31 7.11 0.371 24.78 -243.8 1.56
8/16/2017 12:40 0.74 6.55 0.408 25.63 -110.5 1.54
8/8/2018 9:35 1.30 7.06 0.343 25.73 -11.7 0.35
8/7/2019 9:10 1.83 6.29 0.241 24.26 -115.2 1.46
8/6/2020 11:50 0.93 6.71 0.388 26.37 6.6 0.35
8/21/2021 9:20 0.11 6.83 0.257 25.09 -19 4.7
8/1/2016 12:02 0.23 6.94 1.023 29.25 -171.1 3.89
10/6/2016 14:50 0.35 6.60 0.437 24.86 -223.3 5.2
11/23/2016 10:45 0.73 6.61 0.390 20.64 -155.6 2.4
3/2/2017 11:04 0.11 6.42 2.213 16.61 -141.5 4.38
4/26/2017 9:50 0.61 6.11 1.704 20.34 -132.1 7.47
8/9/2017 15:45 0.47 6.48 0.344 26.30 -209.9 8.52
3/7/2018 13:55 1.18 6.78 0.871 16.31 -218.9 4.94
5/23/2018 12:25 0.09 6.81 1.066 25.90 -209.5 6.23
8/8/2018 11:25 4.27 6.95 2.073 26.75 -294.8 3.62
2/5/2019 12:55 0.70 7.12 0.865 18.31 -297.1 41.9
8/7/2019 15:40 0.16 6.89 0.809 30.70 -306.3 6.31
8/6/2020 13:50 0.11 6.51 0.422 26.30 -289.2 18.4
8/22/2021 12:17 0.00 6.98 0.783 27.93 -333 6.8
8/4/2022 9:10 NR 7.04 0.473 28.73 -315 28.1
8/1/2016 13:05 0.05 6.76 0.231 31.84 -202.8 1.63
10/6/2016 9:15 2.22 6.28 0.214 24.62 -137.8 1.3
3/2/2017 9:29 0.24 6.24 0.191 17.68 -50.0 8.97
8/7/2017 10:55 0.30 6.67 0.258 29.59 -106.9 2.87
3/7/2018 13:10 1.08 6.95 0.304 17.55 -223.5 2.05
5/23/2018 9:05 0.15 7.17 0.330 24.17 -136.1 0.47
8/7/2018 15:30 0.28 6.41 0.236 28.69 -218.5 1.96
8/7/2019 11:35 0.19 6.55 0.245 30.75 -139.3 2.37
8/6/2020 9:55 0.33 6.98 0.321 27.32 -80.8 2.75
8/23/2021 9:20 0.00 6.72 0.178 29.15 -246 28.0
8/4/2022 9:54 NR 6.89 0.219 29.87 -233 0.0
8/1/2016 14:10 0.05 6.99 0.959 29.99 -288.0 55.8
10/6/2016 13:25 0.57 6.60 0.732 25.44 -168.5 9.75
11/23/2016 11:35 0.63 6.65 1.012 20.26 -186.4 14
3/2/2017 10:35 0.68 6.12 0.644 16.45 -37.4 12.8
4/26/2017 10:35 0.68 6.10 0.237 21.92 -7.3 3.46
8/9/2017 13:20 0.68 6.20 0.980 26.48 -7.8 10.35
3/7/2018 9:50 2.09 6.86 0.646 16.51 -127.5 15.3
5/23/2018 9:40 0.39 6.59 0.657 26.27 45.0 12.4
8/8/2018 10:20 4.47 6.87 0.965 28.52 -237.6 40
2/5/2019 12:30 0.62 7.11 0.716 16.11 -198.0 44.5
8/7/2019 13:15 0.10 7.08 0.810 31.63 -201.6 51.4
8/6/2020 14:10 0.25 6.75 0.464 28.62 -86.6 25.2
8/22/2021 12:53 0.00 6.96 0.474 26.01 -257 18.8
8/4/2022 8:42 NR 6.76 0.617 25.76 -187 11.6
KMW-1
KMW-5
KMW-6
KMW-8
KMW-7
Notes are provided on the final page of this table.
TYPE II MONITORING WELLS
KMW-3
1 of 4
Appendix B
Historical Groundwater Water Quality Measurements
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
Well ID Date
Measured
Time of
Measurement
Dissolved
Oxygen
(mg/L)
pH
(Standard
Units)
Specific
Conductivity
(mS/cm)
Temperature
(°C)
Redox-
Potential
(mV)
Turbidity
(NTU)
8/1/2016 10:30 0.92 6.38*0.785 26.33 -292.7 57.6
10/6/2016 10:20 1.07 6.63 0.301 24.11 -113.9 25
8/9/2017 15:10 1.89 6.68 0.268 25.86 -48.6 13.7
8/8/2018 8:50 0.67 7.13 0.242 26.63 -2.6 7.65
8/7/2019 10:30 0.15 7.51 0.802 28.12 -173.5 15.4
8/6/2020 12:10 0.78 6.59 0.458 24.20 -10.9 12.5
8/23/2021 15:05 0.04 6.39 0.408 27.80 95 17.9
8/4/2022 10:48 NR 7.13 1.000 27.17 -188 13.4
8/1/2016 16:25 0.11 7.13 6.506 27.20 -342.6 3.17
10/6/2016 13:15 0.31 6.56 2.587 26.86 -269.3 4.5
11/23/2016 12:35 0.41 6.79 2.767 22.80 -291.9 65**
3/2/2017 11:40 0.42 6.81 3.431 17.62 -239.9 5.04
4/26/2017 12:30 0.57 5.67 0.304 22.32 -156.8 1.85
8/9/2017 10:55 0.29 6.39 1.511 25.30 -198.2 3.6
3/7/2018 11:40 4.82 6.72 2.252 17.12 -186.5 1.77
5/23/2018 16:00 0.27 6.16 0.261 23.79 -92.1 16.6
8/8/2018 11:30 0.09 6.78 8.336 30.22 -308.2 6.0
2/5/2019 9:25 0.30 7.13 1.819 17.05 -285.9 6.10
8/6/2020 12:50 0.44 6.18 0.530 30.1 -236.9 13.5
8/22/2021 14:08 0.00 6.41 0.435 28.74 -243 62.7
8/1/2022
8/1/2016 15:10 0.25 6.86 1.084 32.94 -319.8 110
10/6/2016 12:00 0.34 6.62 1.000 25.53 -287.6 15
11/23/2016 14:05 1.18 6.59 1.102 21.75 -269.8 119**
3/2/2017 9:45 0.65 6.69 0.498 15.32 -221.5 10.1
4/26/2017 13:35 0.41 6.84 0.961 28.89 -289.3 22.4
8/29/2017 15:25 1.32 7.15 0.315 26.26 -97.0 9.10
3/12/2018 9:20 1.96 6.89 0.796 13.56 -257.6 40.7
5/23/2018 11:05 0.67 6.71 1.342 28.74 -49.2 18.7
8/8/2018 9:20 1.17 7.00 0.819 28.30 -40.9 22
2/5/2019 11:15 0.34 7.12 1.001 19.35 -77.3 17.0
8/7/2019 12:40 2.99 5.80 1.274 30.09 -173.2 13.9
8/6/2020 12:20 0.53 6.74 1.054 28.7 -127.2 8.18
8/22/2021 14:52 0.00 6.71 0.844 29.13 -125 24.4
8/5/2022 11:30 NR 6.43 0.837 27.6 -127 94.9
8/1/2016 14:15 0.50 6.23 0.618 31.64 -55.6 2.9
8/9/2017 9:30 2.07 6.41 0.986 26.72 68.0 6.6
8/7/2018 15:50 1.30 6.88 0.333 29.76 64.6 0.00
8/7/2019 8:55 0.40 6.24 0.627 28.61 20.4 2.52
8/6/2020 13:20 0.33 6.52 0.340 29.10 -154.5 7.27
8/22/2021 13:33 2.04 6.68 0.315 28.93 -63 12.4
8/4/2022 12:30 NR 6.2 0.296 28.62 -32 0.0
8/1/2016 19:40 0.07 7.34 0.681 23.89 -97.4 5.41
8/7/2017 15:40 0.18 6.87 0.569 24.29 -142.3 9.5
8/8/2018 8:50 7.23 6.80 0.506 25.22 -92.0 7.6
8/7/2019 10:40 2.72 5.93 0.493 26.32 -147.9 16.1
8/6/2020 9:55 0.15 6.77 0.560 27.28 -123.4 10.7
8/21/2021 11:45 0.00 6.97 0.525 26.52 -190 7.6
8/3/2022 13:14 NR 6.8 0.439 24.99 -165 0.0
Notes are provided on the final page of this table.
KMW-9R
TYPE II MONITORING WELLS (Continued)
KMW-18
KMW-13
KMW-14
KMW-12
WELL DRY
2 of 4
Appendix B
Historical Groundwater Water Quality Measurements
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
Well ID Date
Measured
Time of
Measurement
Dissolved
Oxygen
(mg/L)
pH
(Standard
Units)
Specific
Conductivity
(mS/cm)
Temperature
(°C)
Redox-
Potential
(mV)
Turbidity
(NTU)
8/1/2016 15:30 1.16 6.46 0.275 28.39 -25.6 1.62
8/8/2017 8:55 1.61 6.40 0.328 25.52 31.8 4.20
8/8/2018 9:05 2.01 6.08 0.318 27.79 226.5 0.61
8/7/2019 14:15 0.25 6.74 0.291 27.27 -130.1 1.48
8/6/2020 9:55 0.16 6.71 0.358 26.1 -141.1 1.10
8/21/2021 15:48 0.00 6.77 0.324 27.32 -135 11.6
8/1/2016 11:15 0.54 6.33 0.260 24.49 -49.5 0.93
10/6/2016 9:35 1.19 6.37 0.267 22.45 -77.0 1.04
8/9/2017 13:45 0.32 6.52 0.591 24.25 -275.2 0.90
8/8/2018 13:10 1.73 6.58 0.394 23.47 -76.1 0.66
8/7/2019 10:01 0.50 7.17 1.261 23.07 -264.9 3.33
8/6/2020 10:50 0.23 6.65 0.552 23.2 -293.5 5.34
8/21/2021 12:55 0.00 6.73 0.677 24.61 -235 7.0
8/3/2022 12:25 NR 6.67 0.635 24.25 -165 0.0
8/1/2016 13:00 0.44 6.44 0.239 31.72 -99.7 55
10/6/2016 11:10 0.54 6.39 0.195 23.31 -90.3 2.69
8/9/2017 11:35 1.32 6.35 0.122 25.55 71.3 7.69
8/8/2018 10:20 0.38 6.67 0.335 25.60 -77.7 0.29
8/7/2019 9:21 0.19 6.74 0.245 26.95 -170.2 1.77
8/6/2020 10:25 0.49 6.68 0.650 25.80 -258.8 4.62
8/22/2021 9:03 0.00 6.62 0.296 24.31 -237 14.9
8/3/2022 9:59 NR 6.76 0.381 24.77 -98 0
8/1/2016 13:45 0.21 6.27 0.180 27.92 -98.0 5.52
8/9/2017 15:15 0.40 6.58 0.267 23.98 -129.3 3.08
8/8/2018 13:50 0.20 6.33 0.183 32.40 20.3 1.92
8/7/2019 12:35 0.23 6.41 0.335 28.18 -186.0 3.97
8/6/2020 11:45 0.45 6.21 0.300 27.70 -236.3 4.20
8/21/2021 14:55 0.00 6.46 0.241 27.42 -197 11.0
8/3/2022 12:00 NR 6.47 0.255 26.63 -138 3.9
8/1/2016 10:25 0.29 6.62 0.423 29.43 -80.6 0.63
8/9/2017 14:30 0.96 6.79 0.448 26.44 -73.8 22.0
8/8/2018 12:30 0.22 6.67 0.509 28.85 -52.3 2.17
8/7/2019 11:00 0.35 6.76 0.415 29.26 -105.1 1.76
8/6/2020 11:20 0.38 6.81 0.484 29.90 -130.2 7.16
8/21/2021 13:35 0.00 6.83 0.540 29.30 -124 16.0
8/3/2022 11:17 NR 6.77 0.306 31.37 -126 56.9
8/1/2016 11:40 0.09 6.14 0.224 33.00 -109.6 1.25
8/9/2017 9:55 7.62 6.80 0.112 28.02 5.3 7.12
AMW-3
AMW-2
AMW-4
AMW-1
FHR TYPE II MONITOING WELLS WITHIN APEX TERMINAL
AMW-5
AMW-6
Notes are provided on the final page of this table.
3 of 4
Appendix B
Historical Groundwater Water Quality Measurements
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
Well ID Date
Measured
Time of
Measurement
Dissolved
Oxygen
(mg/L)
pH
(Standard
Units)
Specific
Conductivity
(mS/cm)
Temperature
(°C)
Redox-
Potential
(mV)
Turbidity
(NTU)
8/1/2016 10:30 0.14 11.12 0.220 24.69 -112.9 0.90
8/8/2017 11:10 0.93 11.31 0.631 23.39 -71.7 1.74
8/8/2018 8:00 5.37 10.17 0.211 23.83 -70.9 5.16
8/7/2019 14:50 1.29 11.31 1.084 25.45 -88.7 3.38
8/6/2020 10:45 1.85 11.72 1.150 21.04 -70.4 1.77
8/23/2021 12:08 1.24 11.76 1.70 26.70 -171 3.4
8/1/2016 15:00 0.65 10.34 0.268 25.50 -69.7 6.01
8/9/2017 11:20 2.78 12.01 2.015 24.37 -100.5 8.17
8/7/2018 15:30 2.82 11.62 1.938 28.09 1.9 12.9
8/7/2019 13:20 3.51 11.47 2.662 26.93 -121.2 7.53
8/6/2020 9:25 3.86 12.30 5.571 26.60 -86.4 0.70
8/22/2021 11:00 0.09 11.69 0.925 25.78 -155 35.60
°C = Degrees Celsius
mS/cm = Millisiemens per Centimeter
mg/L = Milligrams per Liter
mV = Millivolt
NTU = Nephelometric Turbidity Units
Data presented is the final field measurement recorded immediately prior to collection of laboratory sample.
* prior to sampling on 8/1/16, pH reading was questionable due to suspected equipment malfunction. pH was remeasured on 8/3/16.
** prior to sampling on 11/23/16, turbidity reading was questionable due to suspected equipment malfunction. Turbidity was remeasured on 11/29/16.
October/November 2016, March/April 2017 and February 2019 data was obtained during post EAB sampling on 10/6/16, 11/23/16, 3/2/17, 4/26/17 and 2/5/19 respectively.
Per Apex personnel on 8/7/18, AMW-6 has been abandoned.
NR = Not recorded.
KDW-1
FHR TYPE III MONITORING WELLS WITHIN APEX TERMINAL
ADW-1
TYPE III MONITORING WELLS
4 of 4

Appendix C

Historical Groundwater Results

Appendix C
Historical Groundwater Results
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
Sample ID Date Collected
1 70 70 600 70 20 6 70 600 400 400 Varies
ATW-1 10/23/2014 12.6 <0.41 <0.38 96.8 2.6 0.29 J 20.0 <0.42 24.4 43.4 13.8 67,600 111 14.63 J
ATW-2 10/23/2014 <0.25 <0.41 <0.38 <0.30 <0.40 8.4 <0.24 <0.42 <0.26 0.43 J <0.36 268 0.39 J 16.0 J
T-1**8/1/2001 -----------1,100 --
T-2**8/1/2001 -----------4.9*--
T-3**8/24/2001 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 210 <5.0 ND
T-4**8/24/2001 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 44 <5.0 ND
T-5**8/24/2001 <500 <500 <500 <500 <500 <500 <500 <500 <500 <500 <500 34,000 <500 ND
T-6**8/24/2001 8,300 <500 <500 <500 <500 48,000 830 <500 4,100 1,700 <500 11,000 860 ND
T-8**8/24/2001 20 <5.0 <5.0 <5.0 <5.0 21 <5.0 <5.0 18 <5.0 <5.0 22 <5.0 ND
4/1/94 -----------7,900*--
2/10/99 -----------780*--
2/24/00 -----------66.9*--
9/21/00 -----------128*--
2/14/01 -----------16,000*--
7/10/01 -----------7,600*<500 -
8/1/01 -----------4,900*--
8/24/01 <500 <500 <500 3,400 <500 <500 <500 <500 <500 <500 <500 4,500 <500 ND
9/18/01 <50 <50 81 <50 <50 <50 <50 <50 <50 340 170 3,000 <50 BQL
1/3/02 <5.0 <5.0 37 <5.0 <5.0 <5.0 5.5 9 <5.0 39 <5.0 <10 <5.0 ND
2/27/02 <5.0 5.7 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 51 43 <10 <5.0 ND
2/28/03 <50 <50 <50 <50 <50 <50 <50 <50 <50 <50 <50 540 <50 ND
9/16/03 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 53 40 22 <5.0 ND
2/19/04 <1.0 <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 26 27 2.6 <1.0 ND
8/5/04 <0.36 7.7 0.81J <0.34 0.27J <0.31 1.9J 0.85J <0.54 52 60 <0.40 <0.35 ND
2/17/05 <0.54 <0.38 3.2 <0.62 <0.66 <0.45 <0.12 <0.45 <0.62 69 100 1.3
8/23/05 <0.54 7.6 0.84J <0.62 <0.66 <0.45 <0.12 <0.45 <0.62 14 24 ND
Notes are provided on the final page of this table.
TYPE II MONITORING WELLS
KMW-1
<1.6 (Total Xylenes)
6.3 (Total Xylenes)m/p-Xyleneso-XyleneAll Other 8260B AnalytesGroundwater Clean-up Goal (ug/L)500
TEMPORARY MONITORING WELLSMethyl Tert Butyl Ether (MTBE)Naphthalenen-PropylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneContaminant of Concern
Benzenen-Butylbenzenesec-ButylbenzeneEthylbenzeneIsopropylbenzene (Cumene)Page 1 of 20
Appendix C
Historical Groundwater Results
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
Sample ID Date Collected
1 70 70 600 70 20 6 70 600 400 400 Variesm/p-Xyleneso-XyleneAll Other 8260B AnalytesGroundwater Clean-up Goal (ug/L)500Methyl Tert Butyl Ether (MTBE)Naphthalenen-PropylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneContaminant of Concern
Benzenen-Butylbenzenesec-ButylbenzeneEthylbenzeneIsopropylbenzene (Cumene)10/14/05 NM NM NM NM NM NM NM NM NM NM NM NM NM NM
2/9/06 <0.54 <0.38 <0.60J <0.62 <0.66 1.0 J <0.12 <0.45 <0.62 21 42 ND
3/27/2006 <1.0 <1.0 <1.0 <1.0 <1.0 <10.0 <5.0 <1.0 <1.0 6.2 10 ND
8/8/2006 <0.54 <0.38 <0.60 1.0 <0.66 0.69 J <0.12 <0.45 <0.62 27 56 ND
2/7/2007 <0.54 <0.38 <0.60 <0.62 <0.66 <0.45 <0.12 <0.45 <0.62 4.1 8.6 ND
3/30/2007 <0.54 <0.38 <0.60 <0.62 <0.66 <0.45 <0.12 <0.45 <0.62 4.2 9.1 8.4 J*
8/17/2007 <1.6 <1.7 <1.5 <1.5 <1.4 3.1 J <1.4 <1.7 2.2 J 5.7 14 12 B
2/25/2008 1.2 <1.0 <1.0 <1.0 <1.0 13 <5.0 <1.0 <1.0 1.3 2.1 ND
8/19/2008 1.4 <1.0 1.4 <1.0 <1.0 <10 <5.0 <1.0 <1.0 2.4 8.9 14
2/12/2009 <1.0 <1.0 2.0 <1.0 <1.0 <10 <5.0 3.0 <1.0 2.4 11 ND
5/13/2009 <1.0 <1.0 2.2 <1.0 1.7 <10 <5.0 3.9 <1.0 22 12 ND
8/18/2009 <1.0 <1.0 1.8 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 3.8 <2.0 <1.0 ND11/18/2009 <1.0 <1.0 1.5 0.36 J <1.0 2.8 <1.0 1.2 <1.0 0.89 J 6.2 303 0.61 J 6.1
5/13/2010 <1.0 <1.0 0.93 J 22.7 0.49 J <1.0 <1.0 0.69 J 0.33 J 1.9 2.7 19,700 22.1 ND
8/12/2010 <1.0 <1.0 1.3 14.4 0.63 J 0.95 J 1.7 0.68 J <1.0 4.5 1 9,670 1.5 3.42J
11/17/2010 <0.25 <0.41 <0.38 <0.3 <0.4 <0.21 <0.24 1.5 <0.26 6.5 3.1 1.2 J <0.23 4.7 J
2/23/2011 <0.25 <0.41 0.41 J <0.3 <0.4 <0.21 <0.24 <0.42 <0.26 <0.31 2.4 <0.66 <0.23 3.0 J
8/19/2011 <0.25 <0.41 2.0 <0.3 1.1 <0.21 <0.24 3.6 <0.26 1.9 2.1 8.5 J
11/29/2011 <0.25 6.1 0.41 J 3.0 <0.40 0.25 J <0.24 <0.42 <0.26 0.69 J 0.95 J 2,210 0.70 J 1.69 J
3/1/2012 <0.25 <0.41 <0.38 <0.30 <0.40 1.2 <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 ND
5/22/2012 <0.25 6.0 2.0 <0.30 1.3 <0.21 1.8 3.5 <0.26 2.3 0.71 J <0.66 <0.23 55.9
8/17/2012 <0.25 <0.41 1.1 <0.30 <0.40 0.73 J <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 ND
8/13/2013 <0.25 <0.41 <0.38 0.35 J <0.40 <0.21 <0.24 <0.42 <0.26 0.31 J <0.36 113 <0.23 ND
8/21/2014 <0.25 <0.41 <0.38 0.48 J <0.40 <0.21 0.27 J <0.42 <0.26 <0.31 <0.36 39.9 <0.23 11.95 J
3/11/2015 <0.25 <0.41 <0.38 0.94 J <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36 713 <0.23 0.35 J
8/5/2015 <0.50 2.2 <0.76 12.0 <0.80 <0.42 0.86 J <0.84 <0.52 3.0 <0.72 14,700 1.8 J 0.73 J
8/1/2016 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36 5.6 <0.23 ND
8/7/2017 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36 10.0 <0.23 ND
8/7/2019 <0.15 <0.23 <0.20 <0.26 <0.20 <0.28 <0.35 <0.18 <0.24 <0.17 <0.20 33.3 <0.22 ND
8/6/2020 <0.30 <0.47 <0.40 0.69 J <0.40 <0.55 <0.70 <0.37 0.57 J <0.34 <0.39 416 <0.44 ND
8/21/2021 <0.34 <0.49 <0.40 <0.30 <0.33 <0.42 <0.64 <0.34 <0.48 <0.50 <0.33 <0.71 <0.34 ND
8/3/2022 <0.34 <0.49 <0.40 <0.30 <0.33 <0.42 <0.64 <0.34 <0.48 <0.50 <0.33 <0.71 <0.34 ND
Notes are provided on the final page of this table.
<2.0 (Total Xylenes)
0.81 J (Total Xylenes)
KMW-1 (cont'd)
<1.3 (Total Xylenes)
<2.0 (Total Xylenes)
1,000 (Total Xylenes)<1.3 (Total Xylenes)
3.3 (Total Xylenes)
1,100 (Total Xylenes)
<2.0 (Total Xylenes)
<2.0 (Total Xylenes)
<2.0 (Total Xylenes)
TYPE II MONITORING WELLS (Continued)
Page 2 of 20
Appendix C
Historical Groundwater Results
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
Sample ID Date Collected
1 70 70 600 70 20 6 70 600 400 400 Variesm/p-Xyleneso-XyleneAll Other 8260B AnalytesGroundwater Clean-up Goal (ug/L)500Methyl Tert Butyl Ether (MTBE)Naphthalenen-PropylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneContaminant of Concern
Benzenen-Butylbenzenesec-ButylbenzeneEthylbenzeneIsopropylbenzene (Cumene)4/1/94 -----------19,000*--
2/10/99 -----------5*--
2/17/05 <1.1 1.1J <1.2 <1.2 <1.3 <0.90 6.7J 1.4J <1.2 3.6 1.8J ND
7/22/05 <0.54 <0.38 <0.60 <0.62 <0.66 <0.45 <0.12 <0.45 <0.62 <0.44 <0.49 BQL
8/23/05 <0.54 <0.38 <0.60 <0.62 <0.66 <0.45 0.63J <0.45 <0.62 <0.44 <0.49 ND
10/11/05 <0.54 <0.38 <0.60 <0.62 <0.66 <0.72 J <0.12 <0.45 <0.62 <0.44 <0.49 <1.3 <0.49 BQL
10/14/05 <0.54 NM NM <0.62 NM NM NM NM <0.62 NM NM BQL
2/9/06 <1.1 <0.76 <1.2 <1.2 <1.3 1.5J <0.24 <0.90 <1.2 1.1 J <0.98 ND
3/27/2006 <1.0 <1.0 <1.0 <1.0 1.4 <10.0 6.2 <1.0 <1.0 3.9 <1.0 ND
8/8/2006 <0.54 <0.38 <0.60 <0.62 <0.66 <0.45 <0.12 <0.45 <0.62 <0.44 <0.49 ND
2/7/2007 <2.7 <1.9 <3.0 <3.1 <3.3 2.9 J <0.60 <2.3 <3.1 <2.2 <2.3 ND
3/30/2007 <1.1 <0.76 <1.2 <1.2 <1.3 1.7 J <0.24 <0.90 <1.2 3.1 <0.98 ND8/17/2007 <1 <0.33 0.36 J <0.30 <0.27 <0.58 <0.27 <0.34 <0.31 <0.27 <0.28 ND
2/25/2008 <1.0 <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0 ND
8/19/2008 <1.0 <1.0 <1.0 <1.0 1.2 <10 <5.0 1.6 <1.0 13 <1.0 ND
2/12/2009 <1.0 <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0 ND
5/13/2009 <1.0 <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0 ND
8/18/2009 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 ND
11/18/2009 <1.0 <1.0 0.53 J <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 ND
5/13/2010 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 ND
8/12/2010 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 1.6 J <1.0 0.47 J
Notes are provided on the final page of this table.
<2.0 (Total Xylenes)
<2.0 (Total Xylenes)
<2.0 (Total Xylenes)
<2.0 (Total Xylenes)
250 (Total Xylenes)
<2.0 (Total Xylenes)
2.5 (Total Xylenes)
1,200 (Total Xylenes)
790 (Total Xylenes)
<0.87 (Total Xylenes)
TYPE II MONITORING WELLS (Continued)
KMW-2
580 (Total Xylenes)
<1.3 (Total Xylenes)6.3 (Total Xylenes)
19 (Total Xylenes)
Page 3 of 20
Appendix C
Historical Groundwater Results
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
Sample ID Date Collected
1 70 70 600 70 20 6 70 600 400 400 Variesm/p-Xyleneso-XyleneAll Other 8260B AnalytesGroundwater Clean-up Goal (ug/L)500Methyl Tert Butyl Ether (MTBE)Naphthalenen-PropylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneContaminant of Concern
Benzenen-Butylbenzenesec-ButylbenzeneEthylbenzeneIsopropylbenzene (Cumene)4/1/94 -----------6.5*--
2/10/99 -----------96*--
2/14/01 -----------62*--
8/24/01 <5.0 <5.0 <5.0 33 <5.0 13 6.7 5.7 <5.0 17 <5.0 59 <5.0 ND
9/18/01 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 <1 BQL
1/3/02 <5.0 <5.0 99 17 13 <5.0 16 48 <5.0 110 38 32 <5.0 ND
2/27/02 <5.0 8.4 <5.0 12 <5.0 <5.0 5.3 44 <5.0 48 29 23 <5.0 ND
2/28/03 <5.0 <5.0 <5.0 12 <5.0 <5.0 <5.0 <5.0 <5.0 37 11 38 <5.0 ND2
9/16/03 <5.0 <5.0 <5.0 120 <5.0 <5.0 8.1 9.4 <5.0 74 32 250 <5.0 ND
2/19/04 <1.0 <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ND
8/5/04 <0.36 <0.31 <0.24 <0.34 <0.25 <0.31 <0.44 <0.32 <0.54 0.23J <0.21 <0.40 <0.35 ND
2/17/05 3.8 <0.38 <0.60 82 39 <0.45 61 95 1.3 640 93 8.9J8/23/05 11,000 <380 <600 6,700 <660 340,000 340J 700J 53,000 3,800 1,100 ND
10/14/05
2/9/06
8/8/2006 540 <0.38 <0.60 4,600 360 2,700 270 J 220 17,000 2,100 580 ND
2/7/2007 32 <1.9 11 130 18 130 24 J 13 180 110 43 48.6 J
3/30/2007 730 <19 <30 2,900 210 2,300 140 J 120 8,300 1,100 310 ND
8/17/2007 730 <3.3 8.0 J 540 62 3,400 29 J 37 2,100 300 80 3.6 JB
2/25/2008 62 <1.0 <1.0 53 2.6 360 <5.0 2.2 10 19 1.5 ND
8/19/2008 180 <0.66 <0.58 820 13 400 110 1.9 1,700 120 31 100
2/12/2009 490 <16 23 2,100 380 <29 390 160 14,000 2,900 1,100 ND
5/13/2009 34 <6.6 7.0 660 130 <12 130 61 240 1,200 320 ND
8/18/2009 <100 <100 <100 1,210 115 <100 572 <100 749 1,260 405 3,600 2,560 625
11/18/2009 19.9 <1.0 <1.0 104 113 2.1 65.7 74.5 2.4 581 256 303 14.2 39.13 J
5/13/2010 79.3 <5.0 <5.0 166 67.9 2.6 J 63.0 57.5 218 557 84.1 305 103 54
8/12/2010 <1.0 <1.0 <1.0 <1.0 <1.0 0.41 J <1.0 <1.0 <1.0 <1.0 <1.0 7.7 1.4 0.63 J
8/19/2011 48.9 <0.82 <0.76 185 62.1 1.0 J 38.5 35.0 9.5 345 52.7 103 4.2 15.4
8/17/2012 12.8 <0.41 <0.38 3.0 33.0 0.25 J 1.1 21.2 0.68 J 51.6 <0.36 <0.66 0.24 J ND
8/13/2013 27.8 <0.41 2.2 1.4 24.5 0.45 J 2.0 16.7 3.4 11.1 6.5 7.1 0.93 J ND
8/21/2014 18.9 <0.41 <0.38 342 88.9 0.50 J 78.1 42.3 92.5 362 91.4 396 0.59 J 30.0
3/11/2015 7.5 <0.82 <0.76 42.4 54.8 <0.42 46.3 29.3 1.6 J 242 86.7 237 0.57 J 8.7 J
8/5/2015 10.7 <0.41 <0.38 0.95 J 33.0 <0.21 11.7 16.4 1.5 38.6 31.6 33.5 <0.23 5.2 J
8/1/2016 12.1 <1.0 8.1 8.5 62.3 <0.52 40.9 32.7 3.4 298 133 311 <0.58 58.2J
8/8/2017 14.0 <0.41 <0.38 1.2 27.9 <0.21 2.2 14.7 2.6 8.8 9.4 3.4 0.76 J ND
8/7/2019 35.9 <0.23 12.2 3.3 89.9 1.2 0.96 J 47.9 3.5 68.0 <0.20 4.2 0.43 J 7.6
8/6/2020 8.0 <0.23 2.0 <0.26 16.3 <0.28 0.41 J 12.0 1.4 0.52 J <0.20 4.6 0.25 J ND8/21/2021 8.0 <0.49 1.1 <0.30 11.6 <0.42 <0.64 7.5 1.6 <0.50 <0.33 <0.71 <0.34 ND
8/3/2022 20.3 <0.49 3.8 <0.30 39.5 <0.42 <0.64 23.9 3.6 <0.50 <0.33 3.7 <0.34 ND
Notes are provided on the final page of this table.
20,000 (Total Xylenes)
2,900 (Total Xylenes)
26,000 (Total Xylenes)
530 (Total Xylenes)
16,000 (Total Xylenes)
1,800 (Total Xylenes)
58 (Total Xylenes)
11,000 (Total Xylenes)
TYPE II MONITORING WELLS (Continued)
KMW-3
110 (Total Xylenes)
29,000 (Total Xylenes)
0.49' FREE-PHASE PRODUCT PRESENT IN KMW-3
FREE-PHASE PRODUCT PRESENT IN KMW-3
Page 4 of 20
Appendix C
Historical Groundwater Results
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
Sample ID Date Collected
1 70 70 600 70 20 6 70 600 400 400 Variesm/p-Xyleneso-XyleneAll Other 8260B AnalytesGroundwater Clean-up Goal (ug/L)500Methyl Tert Butyl Ether (MTBE)Naphthalenen-PropylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneContaminant of Concern
Benzenen-Butylbenzenesec-ButylbenzeneEthylbenzeneIsopropylbenzene (Cumene)4/1/94 -----------28,000*--
2/24/00 -----------9.4*--
9/21/00 -----------198*--
2/14/01 -----------110*--
8/24/01 <5.0 <5.0 <5.0 <5.0 <5.0 210 7.1 <5.0 <5.0 7.7 <5.0 <10 <5.0 ND
9/17/01 1 1 1 <1 8 17 8 12 <1 12 10 28 <1 BQL
1/3/02 <5.0 <5.0 <5.0 41 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 52 <5.0 ND
2/27/02 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <10 <5.0 ND
2/28/03 <5.0 <5.0 <5.0 <5.0 <5.0 9 <5.0 <5.0 <5.0 15 11 <5.0 <5.0 ND
9/16/03 <5.0 <5.0 <5.0 <5.0 <5.0 12 <5.0 <5.0 <5.0 <5.0 <5.0 <10 <5.0 ND
2/19/04 <1.0 <1.0 <1.0 <1.0 <1.0 17 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ND
8/5/04 <0.36 <0.31 <0.24 <0.34 <0.25 1.1J 0.50J <0.32 <0.54 0.38J 0.24J <0.40 <0.35 ND2/17/05 <0.54 <0.38 <0.60 <0.62 1.2 6.0J 1.2J 1.2 <0.62 10 1.2 ND
8/23/05 <0.54 <0.38 <0.60 <0.62 1.2 <0.45 0.45J 1.5 <0.62 <0.44 <0.49 ND
10/11/05 <0.54 <0.38 5.1 <0.62 1.2 0.47J 1.3J 2.5 <0.62 6.9 3.5 51 51 BQL
10/14/05 <0.54 --<0.62 ----<0.62 --BQL
2/9/06 <0.54 <0.38 <0.60 1.9 <0.66 63 <0.12 <0.45 1.5 <0.44 <0.49 0.58J
3/27/2006 <1.0 <1.0 <1.0 <1.0 <1.0 38 <5.0 <1.0 <1.0 <1.0 <1.0 ND
8/8/2006 <0.54 <0.38 <0.60 <0.62 <0.66 0.53 J <0.12 <0.45 <0.62 <0.44 <0.49 ND
2/7/2007 <0.54 <0.38 <0.60 <0.62 <0.66 0.63 J <0.12 <0.45 <0.62 1.7 2.4 ND
3/30/2007 <0.54 <0.38 <0.60 <0.62 <0.66 0.64 J <0.12 <0.45 <0.62 <0.44 <0.49 ND
8/17/2007 <0.32 <0.33 <0.29 <0.30 <0.27 <0.58 <0.27 <0.34 <0.31 <0.27 <0.28 3.9 B
2/25/2008 <1.0 <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0 ND
8/19/2008 <1.0 <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0 ND
2/12/2009 <1.0 <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0 ND
5/13/2009 <1.0 <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0 ND
8/18/2009 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 ND
11/18/2009 0.57 J <1.0 <1.0 <1.0 <1.0 2.1 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 ND
4/21/2010 <1.0 <1.0 0.88 J 6.2 0.40 J 0.40 J 1.3 <1.0 <1.0 1.2 <1.0 3,170 0.58 J 0.63 J
5/13/2010 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 7.5 <1.0 ND
8/12/2010 54.2 <1.0 <1.0 149 115 2.6 77.2 59.7 18.6 712 <1.0 147 84.3 0.40 J
11/17/2010 <0.25 <0.41 <0.38 0.35 J <0.4 0.36 J <0.24 <0.42 <0.26 <0.31 <0.36 79.9 <0.23 4.2 J
2/23/2011 <0.25 <0.41 <0.38 <0.30 <0.4 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 3.5 J
8/19/2011 <0.25 <0.41 <0.38 0.67 J <0.4 1.8 0.88 J <0.42 <0.26 0.99 J <0.36 13.4 <0.23 5.67 J
11/29/2011 <0.25 <0.41 <0.38 0.48 J <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 2.44 J
3/1/2012 <0.25 <0.41 <0.38 0.82 J <0.40 0.21 J <0.24 <0.42 <0.26 <0.31 <0.36 504 0.66 J ND
5/22/2012 <0.25 <0.41 <0.38 <0.30 <0.40 0.58 J <0.24 <0.42 <0.26 <0.31 <0.36 ND8/17/2012 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 ND
Notes are provided on the final page of this table.
<2.0 (Total Xylenes)
<0.66 (Total Xylenes)
<1.3 (Total Xylenes)
<1.3 (Total Xylenes)
9.4 (Total Xylenes)
<2.0 (Total Xylenes)
<2.0 (Total Xylenes)
<2.0 (Total Xylenes)
TYPE II MONITORING WELLS (Continued)
KMW-4
71 (Total Xylenes)
<1.3 (Total Xylenes)
19 (Total Xylenes)
10 (Total Xylenes)
<2.0 (Total Xylenes)
2.7 (Total Xylenes)
Page 5 of 20
Appendix C
Historical Groundwater Results
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
Sample ID Date Collected
1 70 70 600 70 20 6 70 600 400 400 Variesm/p-Xyleneso-XyleneAll Other 8260B AnalytesGroundwater Clean-up Goal (ug/L)500Methyl Tert Butyl Ether (MTBE)Naphthalenen-PropylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneContaminant of Concern
Benzenen-Butylbenzenesec-ButylbenzeneEthylbenzeneIsopropylbenzene (Cumene)9/17/01 <20 <20 <20 <20 <20 <20 33 26 <20 210 56 800 <20 BQL
1/3/02 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <10 <5.0 ND
2/27/02 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <10 <5.0 ND1
2/28/03 <500 <500 <500 <500 <500 <500 <500 <500 <500 <500 <500 78,000 <500 ND
9/16/03 <120 <120 <120 <120 <120 <120 <120 <120 <120 <120 <120 13,000 <120 ND
2/19/04 <500 <500 <500 <500 <500 <5,000 <2,500 <500 <500 <500 <500 15,000 <500 ND
8/5/04 <36 <31 <24 <34 <25 <31 <44 <32 <54 <19 <21 25,000 <35 ND
2/17/05 <54 <38 <60 <62 <66 <45 <12 <45 <62 <44 <49 ND
8/23/05 <54 <38 <60 <62 <66 <45 <12 <45 <62 <44 <49 ND
10/14/05 NM NM NM NM NM NM NM NM NM NM NM NM NM NM
2/9/06 <54 <38 <60 <62 <66 <45 <12 <45 <62 <44 <49 ND
8/14/2006 <2.7 <1.9 <3.0 <3.1 <3.3 7.4 J 1.6 J <2.3 <3.1 <2.2 <2.5 ND2/7/2007 <0.54 <0.38 <0.60 <0.62 <0.66 1.6 J <0.12 <0.45 <0.62 <0.44 <0.49 ND
3/30/2007 <27 <19 <30 <31 <33 <23 <6.0 <23 <31 <22 <25 ND
8/17/2007 <0.32 <0.33 <0.29 <0.30 <0.27 12 <0.27 <0.34 <0.31 <0.27 <0.28 8.0 B
2/25/2008 <1.0 <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0 ND
8/19/2008 3.1 <1.0 <1.0 <1.0 2.2 <10 <5.0 <1.0 <1.0 7.3 1.3 7.5
2/12/2009 <1.0 <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0 ND
5/13/2009 <1.0 <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0 ND
8/18/2009 <1.0 <1.0 <1.0 <1.0 <1.0 5.1 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 ND
11/18/2009 <1.0 <1.0 0.48 J <1.0 0.57 J 1.8 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 ND
4/21/2010 <1.0 <1.0 <1.0 16.6 1.1 1.7 2.3 0.72 J 0.75 J 5.6 0.94 J 15,200 10.9 1.67 J
5/13/2010 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 922 <5.0 14.6
8/12/2010 <1.0 <1.0 <1.0 <1.0 <1.0 8.2 <1.0 <1.0 <1.0 <1.0 <1.0 139 <1.0 0.40 J
11/17/2010 <1.2 <2.0 <1.9 <1.5 <2.0 <1.0 <1.2 <2.1 <1.3 <1.6 <1.8 26 <1.2 ND
2/23/2011 <0.25 <0.41 8.3 12.1 0.83 J 4.3 2.1 1.2 0.28 J 10.4 1.9 9,490 5.5 3.95 J
8/19/2011 <0.25 <0.41 <0.38 <0.3 <0.4 0.82 J <0.24 <0.42 <0.26 <0.31 <0.36 2.6 <0.23 5.9 J
11/29/2011 <12.5 <20.5 <19.0 <15.0 <20.0 <10.5 <12.0 <21.0 <13.0 <15.5 <18.0 5,470 <11.5 14.9 J
3/1/2012 <0.25 <0.41 1.0 <0.30 0.64 J 0.80 J <0.24 1.9 <0.26 0.48 J 0.41 J <0.66 <0.23 ND
5/22/2012 <0.25 <0.41 <0.38 <0.30 <0.40 3.2 <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 4.1 J
8/17/2012 <0.25 <0.41 <0.38 <0.30 <0.40 2.1 <0.24 <0.42 <0.26 <0.31 <0.36 58.7 <0.23 ND
8/13/2013 <0.25 <0.41 <0.38 <0.30 <0.40 1.0 0.45 J <0.42 <0.26 1.3 <0.36 5,710 0.83 J 4.87 J
8/13/2013 DUP <50.0 <82.0 <76.0 <60.0 <80.0 <42.0 <48.0 <84.0 <52.0 <62.0 <72.0 6,450 <46.0 731
8/21/2014 <0.25 <0.41 <0.38 0.45 J <0.40 0.49 J 0.44 J <0.42 <0.26 <0.31 <0.36 164 <0.23 0.30 J
3/11/2015 <0.25 <0.41 <0.38 <0.30 <0.40 0.88 J <0.24 <0.42 <0.26 <0.31 <0.36 5.1 <0.23 ND
8/5/2015 <0.25 <0.41 <0.38 <0.30 <0.40 0.52 J <0.24 <0.42 <0.26 <0.31 <0.36 0.78 J <0.23 ND
8/1/2016 <0.25 <0.41 <0.38 3.6 <0.40 0.78 J <0.24 <0.42 <0.26 0.32 J <0.36 99.1 1.3 0.62 J8/16/2017 <1.2 <2.0 <1.9 2.2 J <2.0 <1.0 <1.2 <2.1 5.1 <1.6 <1.8 1,840 <1.2 ND
8/8/2018 <0.25 <0.41 <0.38 0.30 J <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36 99.6 0.23 J ND
8/7/2019 <0.15 <0.23 <0.20 <0.26 <0.20 3.0 <0.35 <0.18 <0.24 <0.17 <0.20 <0.41 <0.22 ND
8/6/2020 <0.15 <0.23 <0.20 <0.26 <0.20 <0.28 <0.35 <0.18 <0.24 <0.17 <0.20 <0.41 <0.22 ND
8/21/2021 <0.34 <0.49 <0.40 <0.30 <0.33 <0.42 <0.64 <0.34 <0.48 <0.50 <0.33 <0.71 <0.34 ND
Notes are provided on the final page of this table.
12,000 (Total Xylenes)
11 (Total Xylenes)
<2.0 (Total Xylenes)
150 (Total Xylenes)
<2.0 (Total Xylenes)
<2.0 (Total Xylenes)
TYPE II MONITORING WELLS (Continued)
KMW-5
46,000 (Total Xylenes)
19,000 (Total Xylenes)
76,000 (Total Xylenes)
980 (Total Xylenes)
<1.3 (Total Xylenes)
Page 6 of 20
Appendix C
Historical Groundwater Results
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
Sample ID Date Collected
1 70 70 600 70 20 6 70 600 400 400 Variesm/p-Xyleneso-XyleneAll Other 8260B AnalytesGroundwater Clean-up Goal (ug/L)500Methyl Tert Butyl Ether (MTBE)Naphthalenen-PropylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneContaminant of Concern
Benzenen-Butylbenzenesec-ButylbenzeneEthylbenzeneIsopropylbenzene (Cumene)9/17/01 <4.4 <8.4 <6.2 410 <7.4 <9.3 <14 <7.1 66 <9.7 <7.4 160,000 270 50
1/3/02 <250 <250 <250 <250 <250 <250 <250 <250 <250 <250 <250 19,000 <250 ND
2/27/02 <500 <500 <500 <500 <500 <500 <500 <500 <500 <500 <500 37,000 <500 ND
2/28/03 67 <50 <50 <50 <50 <50 <50 <50 <50 <50 <50 6,300 <50 ND
9/16/03 <120 <120 <120 <120 <120 <120 <120 <120 <120 <120 <120 14,000 <120 ND
2/19/04 <1,000 <1,000 <1,000 <1,000 <1,000 <10,000 <5,000 <1,000 <1,000 <1,000 <1,000 31,000 <1,000 ND
8/5/2004 <36 <31 <24 <34 <25 <31 73J <32 <54 36J <21 51,000 75 ND
2/17/05 <54 <38 <60 <62 <66 54J 110J <45 <62 77J <49 ND
8/23/05 <54 <38 <60 <62 <66 <45 <12 <45 <62 <44 <49 ND
2/10/06 <54 <38 <60 <62 <66 <45 79J <45 <62 140 <49 ND
8/7/2006 1.3 <0.38 0.90 J 27 1.6 1.0 J 5.1 1.7 4.5 6.4 1.9 ND
2/7/2007 <0.54 <0.38 <0.60 44 <0.66 <0.45 9.4 2.2 6.7 12 <0.49 7.7 J8/9/2007 <64 <66 <58 <60 <54 <120 <54 <68 <62 <54 <56 ND
2/26/2008 <640 <660 <580 <600 <540 <1200 <540 <680 <620 <540 <560 ND
8/19/2008 <64 <66 <58 <60 <54 <120 <54 <68 <62 <54 <56 ND
8/18/2009 <100 <100 <100 <100 <100 <100 <100 <100 <100 <100 <100 35,400 <100 948
5/13/2010 34.6 J <100 <100 49.6 J <100 <100 <100 <100 77.7 J <100 <100 24,700 47.0 J 1,100
8/12/2010 <100 <100 <100 57.8 J <100 <100 <100 <100 <100 <100 <100 33,100 48.9 J 1,122
8/18/2011 <25.0 <41 <38 38.2 J <40 <21 24.2 J <42 42.4 J 38.1 J 60.3 J 21,900 69.7 J ND
8/20/2012 <12.5 <20.5 <19.0 18.4 J <20.0 <10.5 <12.0 <21.0 <13.0 <15.5 <18.0 11,600 16.4 J ND
8/14/2013 <50.0 <82.0 <76.0 69.0 J <80.0 <42.0 <48.0 <84.0 <52.0 <62.0 <72.0 40,600 56.8 J 360 J
8/14/2014 <50.0 <82.0 <76.0 99.7 J <80.0 <42.0 <48.0 <84.0 <52.0 <62.0 <72.0 61,300 78.6 J ND
3/11/2015 <50.0 <82.0 <76.0 125 J <80.0 <42.0 <48.0 <84.0 <52.0 <62.0 <72.0 76,800 95.6 J ND
8/5/2015 <62.5 <102 <95.0 102 J <100 <52.5 <60.0 <105 <65.0 <77.5 <90.0 69,500 102 J ND
8/1/2016 <50.0 <82.0 <76.0 78.8 J <80.0 <42.0 <48.0 <84.0 <52.0 <62.0 <72.0 45,600 66.6 J ND
10/6/2016 <50.0 NA NA <60.0 NA NA NA NA <52.0 NA NA 27,400 <46.0 NA
11/23/2016 <50.0 NA NA 90.9 J NA NA NA NA <52.0 NA NA 57,800 79.2 J NA
3/2/2017 <62.5 <102 <95.0 93.8 J <100 <52.5 256 <105 <65.0 <77.5 <90.0 48,400 66.2 J ND
4/26/2017 <62.5 NA NA 81.2 J NA NA NA NA 86.8 J NA NA 45,000 72.8 J NA
8/9/2017 <50.0 <82.0 <76.0 60.6 J <80.0 <42.0 <48.0 <84.0 79.0 J 148 J <72.0 43,500 93.7 J ND
3/7/2018 <50.0 NA NA 106 J NA NA NA NA <52.0 NA NA 73,700 96.6 J NA
5/23/2018 <62.5 NA NA 125 J NA NA NA NA <65.0 NA NA 67,700 115 J NA
8/8/2018 <50.0 <82.0 <76.0 62.9 J <80.0 <42.0 <48.0 <84.0 <52.0 <62.0 <72.0 40,900 66.4 J ND
2/5/2019 <30.0 NA NA 72.6 J NA NA NA NA <48.8 NA NA 40,200 <44.0 NA
8/7/2019 <30.0 <46.8 <40.2 60.8 J <40.2 <55.0 <70.4 <37.0 <48.8 <34.0 <39.4 28,900 55.6 J ND
8/6/2020 <15.0 <23.4 <20.1 34.6 J <20.1 <27.5 <35.2 <18.5 <24.4 <17.0 <19.7 19,700 26.0 J ND
8/22/2021 <8.6 <12.2 <10.0 <7.6 <8.3 <10.6 <16.1 <8.5 <12.1 <12.4 <8.3 7,120 <8.4 ND8/4/2022 <1.7 <2.4 <2.0 5.3 <1.7 <2.1 <3.2 <1.7 <2.4 <2.5 <1.7 1,420 <1.7 26.0
Notes are provided on the final page of this table.
41,000 (Total Xylenes)
62,000 (Total Xylenes)
TYPE II MONITORING WELLS (Continued)
KMW-6
8,100 (Total Xylenes)
19,000 (Total Xylenes)
13,000 (Total Xylenes)
12,000 (Total Xylenes)
16,000 (Total Xylenes)
25,000 (Total Xylenes)
Page 7 of 20
Appendix C
Historical Groundwater Results
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
Sample ID Date Collected
1 70 70 600 70 20 6 70 600 400 400 Variesm/p-Xyleneso-XyleneAll Other 8260B AnalytesGroundwater Clean-up Goal (ug/L)500Methyl Tert Butyl Ether (MTBE)Naphthalenen-PropylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneContaminant of Concern
Benzenen-Butylbenzenesec-ButylbenzeneEthylbenzeneIsopropylbenzene (Cumene)9/17/01 370 <10 <10 88 <10 330 48 12 450 120 36 570 330 BQL
1/3/02 160 5.4 <5.0 24 <5.0 94 19 <5.0 44 20 7.1 100 16 ND
2/27/02 270 <5.0 32 41 <5.0 110 41 5.5 210 33 31 180 140 ND
2/28/03 120 <5.0 <5.0 74 <5.0 5.4 32 7.8 31 40 33 180 20 ND
9/16/03 300 <5.0 <5.0 180 12 <5.0 150 22 14 170 62 560 8.2 ND
2/19/04 110 <10 <10 120 12 <100 190 26 <10 410 110 600 12 ND
8/5/2004 140 <1.6 <1.2 140 10 <1.6 200 19 5.8 150 34 330 28 ND
2/17/05 96 6.5 2.4 180 16 <0.45 200 30 6.8 170 24 ND
8/23/05 30 7.3 3.3 130 16 1.1J 180 28 5.7 110 13 ND
2/8/06 34 20 5.8 250 23 5.2J 430 50 11 290 85 49.6
8/7/2006 7 <0.38 1.7 100 11 0.73 J 170 B 20 5.2 51 12 ND
2/7/2007 0.94 J <0.38 3.1 170 22 <0.45 200 42 3.9 55 21 ND8/9/2007 0.35 J 4.3 2.3 59 15 <0.58 130 27 4.4 4.6 4.9 9.4 J
2/26/2008 <0.32 <0.33 2.7 36 15 <0.58 79 28 2.8 7.4 3.5 ND
8/19/2008 <0.32 6.1 2.7 35 15 <0.58 69 28 4.2 2.1 3.2 5.1 J
8/18/2009 <1.0 <1.0 <1.0 52.4 10.1 <1.0 113 15.4 3.2 3.0 <1.0 15.8 1.8 ND
8/12/2010 <1.0 <1.0 <1.0 66 13.9 <1.0 134 21.7 <1.0 7.5 4.6 53.3 2.9 44.5
8/18/2011 <0.25 <0.41 <0.38 116 34.4 <0.21 253 55.6 1.6 44.7 <0.36 121 4.9 ND
8/20/2012 <0.25 <0.41 <0.38 10.0 4.4 <0.21 49.2 6.5 <0.26 1.6 1.3 13.8 0.76 J ND
8/14/2013 <0.25 <0.41 1.1 10.7 7.3 <0.21 78.5 10.6 <0.26 2.3 2.4 26.7 1.1 ND
8/14/2013 DUP <0.25 <0.41 <0.38 12.4 7.9 <0.21 88.6 11.4 <0.26 2.8 2.6 28.8 1.2 ND
8/14/2014 <0.25 <0.41 5.5 7.8 13.1 0.22 J 7.0 26.5 <0.26 <0.31 3.2 9.5 0.26 J 1.5
3/11/2015 <0.25 <0.41 <0.38 6.5 10.4 <0.21 9.9 19.3 <0.26 <0.31 2.3 7.0 0.40 J ND
8/5/2015 <0.25 2.2 2.3 7.1 12.5 <0.21 12.5 24.7 <0.26 2.4 2.0 4.5 0.32 J ND
8/1/2016 <0.25 0.89 J 0.79 J 2.5 4.0 <0.21 4.5 8.4 <0.26 1.2 0.77 J 1.4 J <0.23 ND
10/6/2016 <0.25 NA NA 2.3 NA NA NA NA <0.26 NA NA 1.1 J <0.23 NA
3/2/2017 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 0.56 J
8/7/2017 <0.25 <0.41 0.61 J 1.1 2.9 <0.21 <0.24 5.3 <0.26 0.37 J <0.36 0.82 J <0.23 ND
3/7/2018 <0.25 NA NA 1.7 NA NA NA NA <0.26 NA NA 1.7 J <0.23 NA
5/23/2018 <0.25 NA NA 0.65 J NA NA NA NA <0.26 NA NA 0.85 J <0.23 NA
8/7/2018 <0.25 <0.41 <0.38 <0.30 <0.40 0.28 J <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 ND
8/7/2019 <0.15 <0.23 1.3 0.87 J 4.4 1.4 <0.35 6.5 <0.24 <0.17 <0.20 1.2 J <0.22 ND
8/6/2020 <0.15 <0.23 0.76 J <0.26 2.8 <0.28 0.56 J 3.4 <0.24 <0.17 0.31 J 5.0 <0.22 ND
8/23/2021 <0.34 <0.49 <0.40 <0.30 1.9 <0.42 <0.64 2.3 <0.48 <0.50 <0.33 <0.71 <0.34 ND
8/4/2022 <0.34 <0.49 <0.40 <0.30 3.5 <0.42 1.4 4.1 <0.48 <0.50 <0.33 <0.71 <0.34 ND
Notes are provided on the final page of this table.
21 (Total Xylenes)
17 (Total Xylenes)
TYPE II MONITORING WELLS (Continued)
KMW-7
350 (Total Xylenes)
220 (Total Xylenes)
590 (Total Xylenes)
130 (Total Xylenes)
220 (Total Xylenes)
36 (Total Xylenes)
Page 8 of 20
Appendix C
Historical Groundwater Results
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
Sample ID Date Collected
1 70 70 600 70 20 6 70 600 400 400 Variesm/p-Xyleneso-XyleneAll Other 8260B AnalytesGroundwater Clean-up Goal (ug/L)500Methyl Tert Butyl Ether (MTBE)Naphthalenen-PropylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneContaminant of Concern
Benzenen-Butylbenzenesec-ButylbenzeneEthylbenzeneIsopropylbenzene (Cumene)9/17/01 3,400 <200 450 840 <200 6,300 530 <200 600 2,300 580 12,000 650 BQL
1/3/02 1,300 <100 <100 190 <100 3,700 180 130 <100 390 130 930 <100 ND
2/27/02
2/28/03 1,400 <250 <250 550 <250 1,400 320 <250 <250 1,700 630 8,000 340 ND
9/16/03 1,900 <250 <250 670 <250 1,600 480 <250 680 1,200 390 5,900 450 ND
2/19/04 2,600 <100 <100 990 <100 <1,000 680 110 820 1,400 380 8,800 670 ND
8/5/2004 560 <31 <24 430 40J 200J 560 60J 200 1,200 310 5,500 580 ND
2/17/05 620 <7.6 14J 480 68 330 690 130 82 860 240 ND
8/17/05
2/9/06 900 <19 <30 780 47J 360J 680 92 160 1,300 320 ND
8/7/2006 340 <7.6 <12 640 67 130 J 520 B 150 81 1,100 300 ND
2/7/20078/9/2007 520 42 12 390 68 140 480 B 130 51 1,100 310 ND
2/26/2008 630 <0.33 9.8 460 68 79 470 120 48 1,600 430 69.84 J
8/19/2008
8/18/2009 265 <1.0 <1.0 303 77.8 17.8 591 146 20.7 900 284 1,770 56.0 327.9
8/12/2010 <1.0 0.74 J 0.73 J <1.0 0.47 J <1.0 <1.0 1.1 <1.0 0.49 J 0.48 J <2.0 <1.0 ND
8/18/2011 196 23 <1.9 93.2 38.8 1.1 J 133 77.4 12.1 332 159 642 20.8 3.4 J
8/20/2012 91.8 <1.0 <0.95 27.8 16.1 0.57 J 41.5 37.1 3.8 83.5 28.3 145 4.5 64.4
8/14/2013 271 42.5 463 204 30.4 <4.2 244 61.0 20.9 513 120 1,630 54.9 54.7 J
8/14/2014 169 <2.0 1.9 279 33.5 <1.0 173 47.0 15.9 385 94.8 1,060 35.8 ND
3/11/2015 89.1 <0.41 <0.38 195 30.3 0.45 J 151 51.3 7.5 154 <0.36 371 25.9 60.94 J
8/5/2015 15.6 <0.82 <0.76 51.9 23.3 <0.42 112 32.7 2.2 245 53.1 202 6.7 1,042
8/1/2016 76.9 <0.82 2.6 44.0 24.3 0.68 J 61.9 28.4 2.4 161 16.6 190 8.9 10.3 J
10/6/2016 55.2 NA NA 14.1 NA NA NA NA 1.2 NA NA 32.2 3.3 NA
11/23/2016 83.7 NA NA 31.4 NA NA NA NA 0.88 J NA NA 59.8 6.2 NA
3/2/2017 14.7 <0.41 <0.38 7.8 1.8 <0.21 15.9 2.4 0.37 J 70.5 9.6 18.5 2.8 27.86 J
4/26/2017 4.7 NA NA 1.4 NA NA NA NA <0.26 NA NA 56.3 0.67 J NA
8/9/2017 13.9 <0.41 <0.38 6.6 3.7 <0.21 30.4 2.9 0.35 J 101 <0.36 15.3 3.3 ND
3/7/2018 52.6 NA NA 17.4 NA NA NA NA 0.80 J NA NA 31.9 4.2 NA
5/23/2018 20.8 NA NA 1.4 NA NA NA NA <0.26 NA NA 6.2 3.8 NA
8/8/2018 44.1 <0.41 <0.38 21.4 10.2 0.76 J 59.4 <0.42 0.55 J 178 <0.36 16.7 4.5 3.69 J
2/5/2019 56.2 NA NA 12.3 NA NA NA NA 0.44 J NA NA 37.1 2.3 NA
8/7/2019 35.5 <0.23 <0.20 16.1 7.2 <0.28 12.7 6.0 0.95 J 32.1 <0.20 8.8 2.6 26.2
8/6/2020 42.6 <0.23 <0.20 11.1 6.4 <0.28 11.7 4.5 0.94 J 40.4 4.9 20.3 2.3 14.3 J
8/22/2021 44.9 1.7 4.8 9.1 22.9 <0.42 6.4 22.5 <0.48 9.0 1.9 5.7 <0.34 ND
8/4/2022 12.7 <0.49 1.5 3.5 9.9 <0.42 <0.64 2.7 <0.48 1.8 <0.33 <0.71 <0.34 ND
9/17/01 6,200 <200 260 2,800 <200 3,900 540 360 1,100 1,000 <200 3,700 440 BQL
1/3/02
2/27/02
2/28/03
9/16/03 1,200 <250 <250 2,000 <250 540 660 340 1,200 2,700 830 10,000 1,200 ND
2/19/04 560 <200 <200 830 <200 <2,000 <1,000 <200 310 1,400 330 6,900 640 ND
8/5/04 600 45J <24 930 89J 100J 550 170 280 1,500 350 5,900 510 ND
2/17/05
Notes are provided on the final page of this table.
3,600 (Total Xylenes)
2,800 (Total Xylenes)
0.04' FREE-PHASE PRODUCT
KMW-9
0.21' FREE-PHASE PRODUCT
0.12' FREE-PHASE PRODUCT
NOT MEASURED, WELL DAMAGED/WELL WAS REPLACED ON 7/2/03
WELL PERMENANTLY ABANDONED
TYPE II MONITORING WELLS (Continued)
KMW-8
0.17' FREE-PHASE PRODUCT
2,100 (Total Xylenes)
0.12' FREE-PHASE PRODUCT
6,500 (Total Xylenes)
4,100 (Total Xylenes)
0.10' FREE-PHASE PRODUCT
Page 9 of 20
Appendix C
Historical Groundwater Results
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
Sample ID Date Collected
1 70 70 600 70 20 6 70 600 400 400 Variesm/p-Xyleneso-XyleneAll Other 8260B AnalytesGroundwater Clean-up Goal (ug/L)500Methyl Tert Butyl Ether (MTBE)Naphthalenen-PropylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneContaminant of Concern
Benzenen-Butylbenzenesec-ButylbenzeneEthylbenzeneIsopropylbenzene (Cumene)2/2/2015 <6.2 <10.2 <9.5 774 48.2 <5.2 396 107 40.6 297 96.3 541 8.5 J 47.9 J
3/11/2015 1.4 J 24.0 <1.9 535 59.8 <1.0 385 102 34.3 154 39.1 364 4.9 J ND
8/5/2015 0.91 J 13.5 <0.76 <0.60 54.4 <0.42 146 78.1 24.9 76.9 14.8 45.5 1.7 J 43.9 J
8/1/2016 <0.62 7.0 7.6 288 61.6 <0.52 229 67.4 23.3 97.4 20.3 105 2.7 44.3 J
10/6/2016 <0.25 NA NA 46.0 NA NA NA NA 5.5 NA NA 17.7 0.64 J NA
8/9/2017 <0.25 7.0 <0.38 37.9 18.3 <0.21 48.1 31.8 0.86 J 53.9 12.9 5.0 0.52 J ND
8/8/2018 <0.25 <0.41 <0.38 2.5 2.4 <0.21 5.2 1.7 0.39 J 5.9 1.2 3.3 <0.23 ND
8/7/2019 <0.15 9.1 <0.20 20.1 64.1 <0.28 110 34.2 5.1 115 31.4 33.7 4.4 33.5
8/6/2020 <0.15 1.0 <0.20 0.68 J 3.2 <0.28 21.0 <0.18 0.49 J 13.7 4.4 8.9 0.56 J 0.39 J
8/23/2021 <0.34 <0.49 <0.40 <0.30 <0.33 <0.42 3.6 <0.34 <0.48 <0.50 <0.33 <0.71 <0.34 ND
8/4/2022 <0.34 2.3 3.6 <0.30 15.2 <0.42 80.8 1.4 <0.48 3.9 4.5 2.1 1.0 2.3
9/17/01 88 <20 <20 <20 <20 750 <20 <20 <20 <20 <20 <40 <20 BQL
1/3/02 37 <10 <10 12 <10 120 15 <10 18 12 <10 37 18 ND
2/27/02 32 <10 <10 <10 <10 69 10 <10 <10 <10 <10 <20 <10 ND
2/28/03 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 ND
9/16/03 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <10 <5.0 ND
2/19/04 440 <10 <10 190 19 <100 140 30 28 190 38 260 <10 ND
8/5/04 36 5.3 2.2 29 9.3 2.4J 94 20 3.2 77 9.6 17 0.69 J 6.29 J
2/17/05 <0.54 1 0.62J <0.62 1.6 <0.45 6.5 1.4 <0.62 0.45J <0.49 ND
8/23/05 6 <0.38 0.79J <0.62 2.3 <0.45 1.7J 0.46J <0.62 <0.44 <0.49 ND
2/9/06 <0.54 <0.38 <0.60 <0.62 0.91J <0.45 <0.12 <0.45 <0.62 <0.44 <0.49 ND
8/7/2006 <0.54 <0.38 2.4 4.3 16 <0.45 39 B 20 <0.62 110 14 ND
2/7/2007 <0.54 <0.38 1.3 <0.62 5.3 <0.45 13 9.7 <0.62 27 5.2 ND
8/9/2007 <5.0 2.3 1.8 <0.30 1.2 <0.58 2.5 J 5.5 <0.31 0.45 J 0.76 J ND
2/26/2008 <0.32 <0.33 0.84 J <0.30 1.2 <0.58 <0.27 2.2 <0.31 <0.27 <0.28 ND
8/19/2008 0.70 J <0.33 2.6 <0.30 5.1 <0.58 1.7 J 5.3 <0.31 <0.27 <0.28 ND
9/17/01 110 <80 <80 610 <80 <80 89 <80 2,000 650 130 2,500 1,200 BQL1/3/02 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 19 11 ND
2/27/02 6 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 32 5.2 <5.0 81 <5.0 ND
2/28/03 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 ND
9/16/03 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <10 <5.0 ND
2/19/04 <1.0 <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ND
8/5/04 <0.36 <0.31 <0.24 <0.34 <0.25 <0.31 <0.44 <0.32 <0.54 <0.19 <0.21 <0.4 <0.3 ND
2/17/05 <0.54 <0.38 <0.60 <0.62 <0.66 <0.45 <0.12 <0.45 <0.62 <0.44 <0.49 ND
8/23/05 <0.54 <0.38 <0.60 <0.62 <0.66 <0.45 0.29J <0.45 <0.62 <0.44 <0.49 ND
2/8/06 <0.54 <0.38 <0.60 <0.62 <0.66 <0.45 <0.12 <0.45 <0.62 <0.44 <0.49 ND
8/7/2006 <0.54 <0.38 <0.60 <0.62 <0.66 <0.45 0.64 JB <0.45 <0.62 <0.44 <0.49 ND
2/7/2007 <0.54 <0.38 <0.60 <0.62 <0.66 <0.45 0.44 J <0.45 <0.62 <0.44 <0.49 ND
3/11/2014 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 ND
Notes are provided on the final page of this table.
<0.87 (Total Xylenes)
<0.87 (Total Xylenes)
KMW-11 <1.6 (Total Xylenes)
<1.3 (Total Xylenes)
<1.3 (Total Xylenes)
<1.3 (Total Xylenes)
<1.3 (Total Xylenes)
COULD NOT LOCATE DURING AUGUST 2014 EVENT - PRESUMED DESTROYED
TYPE II MONITORING WELLS (Continued)
KMW-9R
KMW-10 <1.6 (Total Xylenes)
<1.3 (Total Xylenes)<1.3 (Total Xylenes)
13 (Total Xylenes)
2.4 (Total Xylenes)
<0.87 (Total Xylenes)
Page 10 of 20
Appendix C
Historical Groundwater Results
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
Sample ID Date Collected
1 70 70 600 70 20 6 70 600 400 400 Variesm/p-Xyleneso-XyleneAll Other 8260B AnalytesGroundwater Clean-up Goal (ug/L)500Methyl Tert Butyl Ether (MTBE)Naphthalenen-PropylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneContaminant of Concern
Benzenen-Butylbenzenesec-ButylbenzeneEthylbenzeneIsopropylbenzene (Cumene)1/3/02
2/27/02 1,400 <5.0 14 190 77 670 200 160 39 760 130 1,800 47 Varies
2/28/03 3,500 <250 <250 730 <250 990 340 <250 <250 1,100 360 5,800 <250 ND
9/16/03 2,000 <250 <250 680 <250 <250 370 <250 <250 950 290 4,400 <250 ND
2/19/04 2,400 <500 <500 1,600 <500 <5,000 <2,500 <500 <500 2,700 670 13,000 <500 ND
8/5/04 1,800 <77 <60 1,500 170J 160J 1,300 340 220J 3,400 860 12,000 120 J ND
2/17/05 1,600 <76 52 810 180 150J 940 380 64 2,100 510 ND
8/22/05 1,700 <7.6 30 770 130 140J 1,100 230 73 2,700 680 ND
2/8/06 2,000 <1.9 12 1,100 100 28J 920 160 68 2,200 470 56.4
8/7/2006 1,200 <7.6 <12 1,100 140 27 J 910 260 48 2,100 420 ND
2/7/2007 1,000 <0.38 <0.60 920 140 11 1,200 180 49 2,600 600 ND
8/9/2007 630 52 18 420 150 10 740 310 41 1,200 190 21 J2/26/2008 480 <3.3 17 180 120 8.1 J 370 B 240 25 830 130 ND
8/19/2008 440 47 17 170 110 6.8 J 380 210 25 660 93 28.5 J
2/12/2009 450 38 15 88 100 <2.9 180 210 18 310 49 ND
5/13/2009 260 41 15 96 94 <10 230 210 11 500 100 41
8/18/2009 331 <20.0 <20.0 102 95.1 <20.0 315 204 <20.0 451 59.9 154 <20.0 ND
8/12/2010 959 28.7 <2.0 115 142 2.7 163 259 69.4 218 30.3 58.5 4.7 239.98 J
8/18/2011 211 23.7 12.6 70.4 114 0.99 J 92.5 203 23.1 81.6 <0.72 34.5 3 220
8/20/2012 463 20.7 <0.76 158 106 1.6 J 387 183 15.7 392 79.2 92.3 3.6 ND
8/14/2013 68.6 <0.41 <0.38 51.8 24.2 <0.21 119 46.3 3.1 40.7 19.0 10.4 0.67 J 1.3 J
3/11/2014 308 <0.41 9.6 149 90.7 0.79 J 549 136 15.4 29.4 29.3 21.8 2.6 17.6
8/14/2014 182 <0.41 <0.38 124 52.8 0.74 J 479 80.8 10.0 112 86.7 31.2 1.9 11.0
8/5/2015
8/1/2016 124 6.8 12.9 989 126 <1.0 991 208 59.9 32.8 16.5 138 3.4 J 9.2 J
10/6/2016 176 NA NA 405 NA NA NA NA 36.9 NA NA 36.2 1.4 J NA
11/23/2016 233 NA NA 878 NA NA NA NA 41.3 NA NA 134 4.4 J NA
3/2/2017 120 <4.1 <3.8 951 108 8.4 J 918 167 38.1 45.0 13.9 204 5.0 J 18.8 J
4/26/2017 118 NA NA 464 NA NA NA NA 17.7 NA NA 59.5 2.6 J NA
8/9/2017 107 <2.0 <1.9 322 37.1 <1.0 829 43.4 13.1 <1.6 36.3 43.1 2.4 J ND
3/7/2018 121 NA NA 647 NA NA NA NA 9.8 NA NA 45.7 6.3 NA
5/23/2018 36.4 NA NA 331 NA NA NA NA 1.5 J NA NA 21.6 4.1 J NA
8/8/2018 76.2 <0.82 <0.76 111 16.7 <0.42 222 26.5 2.9 <0.62 10.3 8.4 2.1 75.5
2/5/2019 77.0 NA NA 556 NA NA NA NA 22.9 NA NA 747 17.8 NA
8/6/2020 29.8 <0.47 <0.40 64.2 11.9 <0.55 273 25.6 2.0 32.8 9.0 21.9 3.0 ND
8/22/2021 13.1 <0.49 <0.40 6.3 <0.33 <0.42 50.9 <0.34 <0.48 2.4 7.7 11.7 <0.34 ND
8/1/2022
Notes are provided on the final page of this table.
COULD NOT SAMPLE - WELL WAS DRY
290 (Total Xylenes)
140 (Total Xylenes)
310 (Total Xylenes)
COULD NOT SAMPLE - WELL WAS DRY
TYPE II MONITORING WELLS (Continued)
KMW-12
0.30' FREE PHASE PRODUCT
2,000 (Total Xylenes)
4,800 (Total Xylenes)
4,100 (Total Xylenes)
310 (Total Xylenes)
<1.3 (Total Xylenes)
440 (Total Xylenes)
540 (Total Xylenes)
Page 11 of 20
Appendix C
Historical Groundwater Results
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
Sample ID Date Collected
1 70 70 600 70 20 6 70 600 400 400 Variesm/p-Xyleneso-XyleneAll Other 8260B AnalytesGroundwater Clean-up Goal (ug/L)500Methyl Tert Butyl Ether (MTBE)Naphthalenen-PropylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneContaminant of Concern
Benzenen-Butylbenzenesec-ButylbenzeneEthylbenzeneIsopropylbenzene (Cumene)1/3/02
2/27/02 690 <5.0 <5.0 140 24 1,800 160 46 34 100 38 35,000 74 ND
2/28/03 690 <1,200 <1,200 <1,200 <1,200 1,100J <1,200 <1,200 <1,200 210J <1,200 19,000 <1,200 ND
9/16/03 <1,000 <1,000 <1,000 <1,000 <1,000 <1,000 <1,000 <1,000 <1,000 <1,000 <1,000 20,000 <1,000 ND
2/19/04 <1,000 <1,000 <1,000 <1,000 <1,000 <10,000 <5,000 <1,000 <1,000 <1,000 <1,000 71,000 <1,000 ND
8/5/04 <180 <160 <120 <170 <120 <160 <220 <160 <270 <95 <100 68,000 <180 ND
2/17/05 920 <76 <120 <120 <130 120J 240J <90 <120 270 <98 ND
8/22/05 340 <38 <60 150 <66 58J 610 <45 <62 140 <49 ND
2/8/06 450 <38 <60 <62 <66 <45 160J <45 <62 130 <49 ND
8/7/2006 740 <190 <300 <310 <330 <230 160 JB <230 <310 <220 <250 ND
2/7/2007 230 <0.38 <0.60 69 1.4 41 68 2 16 28 8.4 20.7
8/9/2007 680 <83 <73 280 <68 <150 120 J <85 160 J 150 J <70 ND2/26/2008 620 <83 <73 <75 <68 <150 190 J <85 110 J 170 J <70 ND
8/19/2008 370 J <160 <140 280 J <140 <290 <140 <170 <160 190 J <140 ND
2/12/2009 310 J <160 <140 290 J <140 <290 210 J <170 <160 310 J <140 ND
5/13/2009 <64 <66 <58 74 <54 <120 <54 <68 <62 80 <56 ND
8/18/2009 162 <1.0 <1.0 134 12.0 1.2 98.6 14.2 25.3 175 43.1 57,400 72.8 ND
8/12/2010 77.5 J <200 <200 <200 <200 <200 <200 <200 <200 67.7 J <200 22,900 100 1,550
8/18/2011 63.8 J <82 <76 188 J <80 <42 476 120 J <52 150 J <72 65,400 108 J ND
8/20/2012 <50.0 <82.0 <76.0 <60.0 <80.0 <42.0 <48.0 <84.0 <52.0 134 J <72.0 60,500 119 J ND
8/14/2013 <50.0 <82.0 <76.0 256 <80.0 <42.0 549 <84.0 <52.0 195 J <72.0 73,700 86.5 J 510
3/11/2014 137 J <102 <95.0 336 <100 <52.5 2,270 180 J 309 217 J <90.0 63,600 178 J 48.2 J
8/14/2014 54.5 J <41.0 <38.0 99.6 J <40.0 <21.0 58.1 J <42.0 71.6 J 134 <36.0 25,700 25.9 J 33.2 J
3/11/2015 38.5 J <51.2 <47.5 328 <50.0 <26.2 163 <52.5 <32.5 222 <45.0 90,900 49.9 J ND
8/5/2015 <62.5 <102 <95.0 271 <100 <52.5 326 <105 <65.0 229 J <90.0 66,400 <57.5 ND
8/2/2016 <25.0 <41.0 <38.0 132 <40.0 <21.0 193 <42.0 <26.0 202 38.4J 21,300 <23.0 ND
10/6/2016 <12.5 NA NA 107 NA NA NA NA 16.4 J NA NA 13,800 <11.5 NA
11/23/2016 25.7 J NA NA 244 NA NA NA NA 34.5 J NA NA 20,400 <23.0 NA
3/2/2017 <12.5 <20.5 <19.0 57.5 65.9 <10.5 242 81.8 20.8 J 997 210 4,370 <11.5 ND
4/26/2017 <12.5 NA NA 82.2 NA NA NA NA 18.9 J NA NA 11,400 <11.5 NA
8/29/2017 0.38 J <0.41 <0.38 0.46 J 0.73 J <0.21 1.7 0.69 J 0.32 J 1.6 <0.36 92.7 0.35 J 18.25 J
3/12/2018 <25.0 NA NA 83.2 J NA NA NA NA <26.0 NA NA 11,200 <23.0 NA
5/23/2018 <10.0 NA NA 63.8 NA NA NA NA <10.4 NA NA 9,330 <9.2 NA
8/8/2018 1.7 <0.41 <0.38 3.6 4.2 <0.21 6.3 4.8 0.67 J 8.9 <0.36 379 0.88 J 9.0 J
2/5/2019 3.6 J NA NA 40.1 NA NA NA NA <1.2 NA NA 1,340 2.3 J NA
8/7/2019 1.5 J 0.58 0.50 19.7 11.1 <0.69 47.0 16.4 <0.61 81.7 11.5 905 1.0 J 45.5 J
8/6/2020 3.4 2.2 J <0.50 17.6 27.4 <0.69 63.5 41.9 <0.61 61.3 14.6 602 1.6 J ND8/23/2021 <0.86 <1.2 2.6 6.4 15.6 <1.1 22.1 22.8 <1.2 5.4 <0.83 704 <0.84 20.9
8/5/2022 <1.7 <2.4 <2.0 <1.5 9.9 <2.1 20.3 14.1 <2.4 7.8 <1.7 1,040 <1.7 ND
Notes are provided on the final page of this table.
27,000 (Total Xylenes)
100,000 (Total Xylenes)
19,000 (Total Xylenes)
83,000 (Total Xylenes)
78,000 (Total Xylenes)
88,000 (Total Xylenes)
96,000 (Total Xylenes)
TYPE II MONITORING WELLS (Continued)
KMW-13
2.51' FREE PHASE PRODUCT
57,000 (Total Xylenes)
71,000D (Total Xylenes)
72,000 (Total Xylenes)
Page 12 of 20
Appendix C
Historical Groundwater Results
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
Sample ID Date Collected
1 70 70 600 70 20 6 70 600 400 400 Variesm/p-Xyleneso-XyleneAll Other 8260B AnalytesGroundwater Clean-up Goal (ug/L)500Methyl Tert Butyl Ether (MTBE)Naphthalenen-PropylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneContaminant of Concern
Benzenen-Butylbenzenesec-ButylbenzeneEthylbenzeneIsopropylbenzene (Cumene)1/3/02 8.5 <5.0 <5.0 <5.0 <5.0 38 <5.0 <5.0 <5.0 <5.0 <5.0 2,900 <5.0 ND
2/27/02 6.9 <5.0 <5.0 66 5 27 13 <5.0 <5.0 25 11 30,000 59 ND
2/28/03 <120 <120 <120 <120 <120 <120 <120 <120 <120 <120 23,000 <120 ND
9/16/03 <500 <500 <500 45,000 <500 <500 <500 <500 <500 <500 <500 38,000 <500 ND
2/19/04 <1,000 <1,000 <1,000 <1,000 <1,000 <10,000 <5,000 <1,000 <1,000 <1,000 <1,000 62,000 <1,000 ND
8/5/04 <180 <160 <120 <170 <120 <160 400J <160 <270 140J <100 50,000 <180 ND
2/17/05 <54 <38 <60 <62 <66 <45 42J <45 <62 <44 <49 ND
8/22/05 <54 <38 <60 74J <66 <45 <12 <45 <62 <44 <49 ND
2/8/06 <54 <38 <60 <62 <66 <45 <12 <45 <62 <44 <49 ND
8/7/2006 <110 <76 <120 <120 <130 <90 72 JB <90 <120 <88 <98 ND
2/7/2007 0.74 J <0.38 <0.60 8.3 0.86 J <0.45 12 1.8 <0.62 18 4.9 0.65 J
8/9/2007 <32 <33 <29 <30 <27 <58 72 J <34 <31 45 J <28 ND2/26/2008 <6.4 <6.6 <5.8 <6.0 <5.4 <12 11 JB <6.8 6.9 J 16 J <5.6 ND
8/19/2008 <6.4 <6.6 <5.8 15 J <5.4 <12 12 J <6.8 <6.2 16 J 6.8 J ND
2/12/2009 <32 <33 <29 <30 <27 <58 100 J <34 <31 33 J <28 ND
5/13/2009 <16 <16 <14 22 <14 <29 <14 <17 <16 22 <14 350
8/18/2009 1.1 <1.0 <1.0 13.4 2.0 <1.0 11.8 2.7 <1.0 27.3 8.7 8,040 3.7 ND
5/13/2010 <20.0 <20.0 18.6 J <20.0 <20.0 <20.0 6.8 J <20.0 <20.0 21.7 7.4 J 3,440 <20.0 ND
8/12/2010 <25.0 <25.0 <25.0 9.0 J <25.0 <25.0 <25.0 <25.0 <25.0 <25.0 <25.0 3,830 <25.0 192
8/18/2011 <1.2 <2 <1.9 1.8 J <2 1.5 J 4.6 J <2.1 <1.3 <1.6 <1.8 1,720 <1.2 ND
8/20/2012 <1.2 <2.0 <1.9 <1.5 <2.0 <1.0 2.7 J <2.1 <1.3 <1.6 <1.8 2,990 1.6 J ND
8/14/2013 <2.5 <4.1 <3.8 8.9 J <4.0 <2.1 9.7 J <4.2 <2.6 8.0 J <3.6 6,430 <2.3 26.9
3/11/2014 <0.25 <0.41 <0.38 <0.30 <0.40 0.21 J 0.43 J <0.42 <0.26 <0.31 <0.36 2.4 <0.23 1.26 J
8/14/2014 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 0.43 J <0.42 <0.26 <0.31 <0.36 114 <0.23 ND
3/11/2015 <0.25 <0.41 <0.38 0.67 J <0.40 <0.21 0.73 J <0.42 <0.26 0.52 J <0.36 296 0.46 J 3.0
8/5/2015 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36 4.0 <0.23 ND
8/1/2016 <0.25 <0.41 <0.38 0.94 J <0.40 <0.21 0.84 J <0.42 <0.26 2.6 0.76 J 15.7 0.78 J ND
8/9/2017 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 ND
8/7/2018 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36 12.1 <0.23 ND
8/7/2019 <0.15 <0.23 <0.20 <0.26 <0.20 <0.28 <0.35 <0.18 <0.24 <0.17 <0.20 0.89 J <0.22 ND
8/6/2020 <0.15 <0.23 <0.20 <0.26 <0.20 <0.28 <0.35 <0.18 <0.24 <0.17 <0.20 167 <0.22 ND
8/22/2021 <0.34 <0.49 <0.40 <0.30 <0.33 <0.42 <0.64 <0.34 <0.48 <0.50 <0.33 <0.71 <0.34 ND
8/4/2022 <0.34 <0.49 <0.40 <0.30 <0.33 <0.42 <0.64 <0.34 <0.48 <0.50 <0.33 <0.71 <0.34 ND
Notes are provided on the final page of this table.
6,300 (Total Xylenes)
20,000 (Total Xylenes)
14,000 (Total Xylenes)
TYPE II MONITORING WELLS (Continued)
KMW-14
21,000 (Total Xylenes)
47,000D (Total Xylenes)
14,000 (Total Xylenes)
37,000 (Total Xylenes)
6,200 (Total Xylenes)
15,000 (Total Xylenes)
4,800 (Total Xylenes)
Page 13 of 20
Appendix C
Historical Groundwater Results
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
Sample ID Date Collected
1 70 70 600 70 20 6 70 600 400 400 Variesm/p-Xyleneso-XyleneAll Other 8260B AnalytesGroundwater Clean-up Goal (ug/L)500Methyl Tert Butyl Ether (MTBE)Naphthalenen-PropylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneContaminant of Concern
Benzenen-Butylbenzenesec-ButylbenzeneEthylbenzeneIsopropylbenzene (Cumene)8/23/05 <1.1 <0.76 <1.2 <1.2 <1.3 30 <0.24 <0.90 <1.2 <0.88 <0.98 ND
10/14/05 <0.54 <0.38 <0.6 <0.62 <0.66 <0.45 <0.12 <0.45 <0.62 <0.44 <0.49 <1.3 <0.49 BQL
2/9/06 <0.54 <0.38 <0.60 <0.62 <0.66 380 <0.12 <0.45 <0.62 <0.44 <0.49 1.1
8/8/2006 <0.54 <0.38 <0.60 <0.62 0.79 J 63 4.9 J 0.54 J 11 5.2 1.4 ND
,0.35 4.7 <0.38 <0.60 1.2 <0.66 200 0.80 J 0.46 J <0.62 <0.44 <0.49 ND
3/30/2007 <0.54 <0.38 <0.60 0.84 J <0.66 99 <0.12 <0.45 <0.62 <0.44 <0.49 ND
8/17/2007 9.8 <1.7 <1.5 <1.5 <1.4 47 J <1.4 <1.7 <1.6 <1.4 <1.4 ND
2/25/2008 2.4 <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0 ND
8/19/2008 <1.0 <1.0 <1.0 2.5 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0 ND
2/12/2009 <1.0 <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0 ND
5/13/2009 <1.0 <1.0 <1.0 1.7 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0 ND
8/18/2009 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 288 <1.0 ND11/18/2009 <1.0 <1.0 <1.0 0.35 J <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 226 0.24 J ND
5/13/2010 <1.0 <1.0 <1.0 <1.0 <1.0 7.3 <1.0 <1.0 <1.0 <1.0 <1.0 152 <1.0 ND
8/12/2010 <1.0 <1.0 <1.0 <1.0 <1.0 0.33 J <1.0 <1.0 <1.0 <1.0 <1.0 5.6 <1.0 ND
8/19/2011 <0.25 <0.41 <0.38 <0.3 <0.4 19.1 <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 6.4 J
8/17/2012 <0.25 <0.41 <0.38 <0.30 <0.31 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 ND
3/11/2014 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 ND
8/23/05 0.80J <0.38 <0.60 <0.62 0.66J 24 <0.12 <0.45 <0.62 <0.44 <0.49 ND
2/8/06 190 <1.9 <3.0 <3.1 3.8 J 600 13J 8.6 3.2J 88 22 ND
8/7/2006 20 <0.38 <0.60 <0.62 4.1 190 5 3.5 <0.62 15 4.3 ND
2/7/2007 31 <0.38 0.61 J <0.62 3.4 43 7.8 6.7 1.6 49 17 ND
8/9/2007 5.0 <0.33 0.73 J <0.30 3.4 37 1.0 JB 1.3 <0.31 6.4 1.4 ND
2/26/2008 0.38 J <0.33 <0.29 <0.30 0.89 J 9.7 J 0.89 J 0.55 J <0.31 2.7 0.97 J 0.39 JB
8/19/2008 <0.32 <0.33 <0.29 <0.30 <0.27 4.6 J <0.27 <0.34 <0.31 <0.27 <0.28 ND
8/18/2009 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 ND
5/13/2010 <1.0 <1.0 0.40 J <1.0 <1.0 4.6 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 ND
8/12/2010 <1.0 <1.0 <1.0 <1.0 <1.0 0.70 J <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 ND
8/23/05 <0.54 <0.38 0.70J <0.62 3.2 8.8J 0.32J <0.45 <0.62 <0.44 <0.49 ND
2/8/06 110 <0.38 <0.60 55 2.9 20 2.8J 3.6 3.7 32 5.0 ND
8/7/2006 2.4 0.40 J 0.60 J <0.62 <0.66 1.4 J 0.81 J <0.45 <0.62 2.6 0.88 J ND
2/7/2007 3 <0.38 1.4 <0.62 4.8 4.7 J 6.8 2.3 <0.62 36 12 ND
8/9/2007 3.5 1.6 1.8 <0.30 4.1 6.3 J 5.2 B 1.6 0.55 J 38 14 ND
2/26/2008 <0.32 <0.33 <0.29 <0.30 1.1 4.1 J 2.7 J <0.34 <0.31 <0.27 <0.28 ND
8/19/2008 <0.32 <0.33 <0.29 <0.30 <0.27 1.2 J <0.27 <0.34 <0.31 <0.27 <0.28 13 J8/18/2009 <1.0 <1.0 <1.0 <1.0 <1.0 2.9 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 ND
5/13/2010 <1.0 <1.0 <1.0 <1.0 <1.0 1.1 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 ND
8/12/2010 <1.0 <1.0 <1.0 <1.0 <1.0 1.7 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 ND
Notes are provided on the final page of this table.
KMW-17
<1.3 (Total Xylenes)
170 (Total Xylenes)
4.8 (Total Xylenes)
11 (Total Xylenes)
16 (Total Xylenes)
<0.87 (Total Xylenes)
<0.87 (Total Xylenes)
KMW-16
<1.3 (Total Xylenes)
7.0J (Total Xylenes)
<1.3 (Total Xylenes)
5.1 (Total Xylenes)
1.4 J (Total Xylenes)
<0.87 (Total Xylenes)
<0.87 (Total Xylenes)
1,800 (Total Xylenes)
51 (Total Xylenes)
5,600 (Total Xylenes)
40 (Total Xylenes)
1,400 E (Total Xylenes)
TYPE II MONITORING WELLS (Continued)
KMW-15
530 (Total Xylenes)
<1.3 (Total Xylenes)
1,300 (Total Xylenes)<1.3 (Total Xylenes)
<1.3 (Total Xylenes)
Page 14 of 20
Appendix C
Historical Groundwater Results
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
Sample ID Date Collected
1 70 70 600 70 20 6 70 600 400 400 Variesm/p-Xyleneso-XyleneAll Other 8260B AnalytesGroundwater Clean-up Goal (ug/L)500Methyl Tert Butyl Ether (MTBE)Naphthalenen-PropylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneContaminant of Concern
Benzenen-Butylbenzenesec-ButylbenzeneEthylbenzeneIsopropylbenzene (Cumene)5/13/2010 10.8 <1.0 <1.0 14.1 10 1.0 0.42 J 1.1 12.8 2.8 1.1 34.9 9.2 1.4
8/12/2010 1.9 <1.0 <1.0 <1.0 7.3 1.9 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 11.4 J
8/19/2011 <0.25 <0.41 <0.38 <0.3 2.3 1.4 <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 9.8 J
8/17/2012 <0.25 <0.41 <0.38 <0.30 <0.40 0.54 J <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 0.20 J
8/13/2013 1.8 <0.41 <0.38 0.31 J 0.79 J 0.87 J <0.24 <0.42 <0.26 <0.31 <0.36 0.88 J <0.23 10.6 J
8/21/2014 2.7 <0.41 <0.38 <0.30 1.1 0.93 J 0.25 J 0.49 J 0.28 J 2.2 0.73 J 6.4 0.26 J 2.4 J
3/11/2015 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 0.35 J <0.42 <0.26 0.31 J <0.36 <0.66 <0.23 0.71 J
8/5/2015 <0.25 <0.41 <0.38 <0.30 <0.40 0.44 J <0.24 <0.42 <0.26 <0.31 <0.36 0.70 J <0.23 0.73 J
8/1/2016 5.3 <0.41 <0.38 0.87 J 2.9 0.89 J 2.1 2.7 0.71 J 3.3 0.82 J 5.4 0.43 J 1.73 J
8/7/2017 6.7 <0.41 <0.38 0.77 J 6.5 0.69 J 4.0 6.6 0.87 J <0.31 <0.36 3.7 <0.23 0.16 J
8/8/2018 2.8 <0.41 <0.38 8.0 4.9 0.70 J 4.0 4.6 0.79 J 16.9 <0.36 24.7 0.46 J ND
8/7/2019 <0.15 <0.23 0.65 J <0.26 5.5 1.2 0.73 J <0.18 <0.24 <0.17 5.1 2.3 <0.22 2.78/6/2020 <0.15 <0.23 <0.20 <0.26 <0.20 0.32 J <0.35 <0.18 <0.24 <0.17 <0.20 8.9 <0.22 ND
8/21/2021 <0.34 <0.49 <0.40 <0.30 <0.33 <0.42 <0.64 <0.34 <0.48 <0.50 <0.33 <0.71 <0.34 ND
8/3/2022 <0.34 <0.49 <0.40 <0.30 <0.33 <0.42 <0.64 <0.34 <0.48 <0.50 <0.33 <0.71 <0.34 ND
12/22/03 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 3.6 2.7 <2.0 <1.0 2.2
2/19/04 <1.0 <1.0 <1.0 <1.0 <1.0 <10.0 <5.0 <1.0 <1.0 <1.0 4.3 <1.0 <1.0 35
8/5/04 <0.36 <0.3 <0.24 <0.34 <0.25 <0.31 <0.44 <0.32 <0.54 <0.19 1.2 <0.40 <0.35 ND
2/16/05 <0.54 2.5 <0.60 1.0 <0.66 3.0J <0.12 <0.45 <0.62 3.3 4.7 14.07
8/22/05 <0.54 0.89J <0.60 <0.62 <0.66 <0.45 <0.12 <0.45 <0.62 <0.44 1.2 ND
2/8/06 <0.54 0.38 <0.60 <0.62 <0.66 <0.45 <0.12 <0.45 <0.62 <0.44 <0.49 ND
8/7/2006 <0.54 <0.38 <0.60 <0.62 <0.66 83 <0.12 <0.45 <0.62 <0.44 2.5 4.2 J
2/7/2007 <0.54 <0.38 <0.60 <0.62 <0.66 <0.45 <0.12 <0.45 <0.62 <0.44 0.55 J 57
8/9/2007 530 <1.3 <1.2 <1.2 <1.1 56 <1.1 <1.4 200 <1.1 2.2 J ND
2/26/2008 270 <1.3 <1.2 5.3 <1.1 25 J 2.7 J <1.4 50 <1.1 <1.1 ND
8/19/2008 170 <1.6 <1.4 3.8 J 1.8 J 7.7 J 9.4 J <1.7 500 17 12 3.9 J
8/18/2009 22.6 5.9 <1.0 39.5 8.3 <1.0 15.0 16.9 13.1 59.4 17.5 164 65.0 ND
8/12/2010 12.9 0.85 J <1.0 3.6 <1.0 9.2 <1.0 <1.0 <1.0 <1.0 1 <2.0 3.5 ND
8/18/2011 5.7 <0.41 <0.38 58.7 1.4 <0.21 2.2 1 10.4 4.8 1.2 10.2 35.0 6.9 J
8/20/2012 1.5 <0.41 <0.38 10.6 1.0 <0.21 <0.24 <0.42 0.60 J 0.99 J 1.0 2.2 15.2 1.2 J
8/14/2013 <0.25 <0.41 <0.38 4.0 <0.40 <0.21 0.46 J <0.42 <0.26 <0.31 <0.36 1.6 J <0.23 ND
8/14/2014 <0.25 <0.41 <0.38 2.7 <0.40 <0.21 0.80 J <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 ND
3/11/2015 <0.25 <0.41 <0.38 2.8 <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 ND
8/5/2015 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 0.26 J <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 ND
8/1/2016 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 0.82 J8/8/2017 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 ND
8/8/2018 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 0.28 J
8/7/2019 <0.15 <0.23 <0.20 0.82 J <0.20 <0.28 0.37 J <0.18 0.45 J 0.65 J <0.20 4.8 1.3 ND
8/6/2020 <0.15 <0.23 <0.20 <0.26 <0.20 <0.28 <0.35 <0.18 <0.24 <0.17 <0.20 <0.41 <0.22 ND
8/21/2021 <0.34 <0.49 <0.40 <0.30 <0.33 <0.42 <0.64 <0.34 <0.48 <0.50 <0.33 <0.71 <0.34 ND
Notes are provided on the final page of this table.
<3.5 (Total Xylenes)
21 (Total Xylenes)
80 (Total Xylenes)
TYPE II MONITORING WELLS (Continued)
KMW-18
FHR TYPE II MONITORING WELLS WITHIN APEX TERMINAL
AMW-1
<1.6 (Total Xylenes)
<1.3 (Total Xylenes)
<1.3 (Total Xylenes)
<1.3 (Total Xylenes)
<1.3 (Total Xylenes)
Page 15 of 20
Appendix C
Historical Groundwater Results
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
Sample ID Date Collected
1 70 70 600 70 20 6 70 600 400 400 Variesm/p-Xyleneso-XyleneAll Other 8260B AnalytesGroundwater Clean-up Goal (ug/L)500Methyl Tert Butyl Ether (MTBE)Naphthalenen-PropylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneContaminant of Concern
Benzenen-Butylbenzenesec-ButylbenzeneEthylbenzeneIsopropylbenzene (Cumene)12/22/03 1,700 <1.0 <1.0 1,400 130 300 660 390 1,100 2,500 710 27,000 680 5.2
2/19/04 2,200 <200 <200 1,700 <200 <2,000 <1,000 300 2,000 2,200 600 39,000 940 ND
8/5/04 2,300 <62 <48 2,000 140J 440J 750J 260 1,900 2,100 560 40,000 970 ND
2/16/05 1,200 <38 <60 1,300 130 130J 840 260 1,700 2,100 490 ND
8/22/05 1,700 48J <60 1,300 120 190J 900 230 1,000 1,300 340 ND
2/8/06 1,700 <76 <120 1,300 <130 <90 370J 140J 2,100 1,100 290 ND
8/7/2006 1,300 110 J <120 1,400 <130 200 J 540 JB <90 2,000 1,200 330 ND
2/7/2007 790 <0.38 <0.60 760 80 86 310 180 420 1,000 180 ND
8/9/2007 580 <66 <58 570 70 J 120 J 250 J 130 J 120 J 680 180 J ND
2/26/2008 720 <66 <58 960 79 J 260 J 530 J 170 J 210 1,300 340 ND
8/19/2008 320 <66 <58 410 <54 140 J 250 J 100 J 82 J 540 140 J ND
8/18/2009 305 <20.0 <20.0 505 50.3 88.5 254 92.2 59.2 711 170 50,900 175 ND8/12/2010 645 <200 <200 956 93.0 J <200 400 216 <200 799 244 28,900 107 J 783
8/18/2011 169 <41 <38 493 48.2 J <21 221 99.5 J 275 473 142 31,800 349 ND
8/21/2012 209 <41.0 <38.0 529 72.3 J <21.0 299 134 40.0 J 756 199 22,000 90.3 J ND
8/14/2013 225 <41.0 <38.0 740 106 <21.0 421 223 33.3 J 1,110 317 15,500 37.2 J 323
3/11/2014 71.7 <10.2 <9.5 204 19.9 J 32.1 74.2 35.2 25.8 193 54.4 9,500 28.4 ND
8/14/2014 166 <20.5 <19.0 323 81.3 <10.5 168 165 16.5 J 351 96.4 12,900 <11.5 ND
3/11/2015 245 <20.5 <19.0 513 106 <10.5 311 205 25.0 J 596 177 13,300 12.7 J ND
8/5/2015 155 <20.5 <19.0 787 99.4 <10.5 370 203 41.7 J 1,020 302 15,100 40.8 J ND
8/1/2016 <10.0 <16.4 <15.2 446 71.3 <8.4 217 154 57.4 1,290 363 8,250 308 11.7 J
10/6/2016 <10.0 NA NA 405 NA NA NA NA 94.2 NA NA 11,000 251 NA
8/9/2017 <6.2 26.6 <9.5 354 63.2 <5.2 172 129 33.6 823 170 6,170 182 ND
8/8/2018 <2.5 <4.1 <3.8 202 25.9 <2.1 92.0 68.6 <2.6 438 92.7 2,610 58.5 16.9 J
8/7/2019 22.4 <4.7 <4.0 442 57.3 <5.5 178 <3.7 20.0 717 183 7,710 351 ND
8/6/2020 26.0 <5.8 <5.0 777 91.2 <6.9 463 <4.6 23.4 J 1,440 371 8,180 174 ND
8/21/2021 <4.3 <6.1 <5.0 296 27.8 <5.3 150 <4.2 <6.1 404 101 3,750 57.2 ND
8/3/2022 <4.3 <6.1 <5.0 282 27.3 <5.3 117 47.8 15.0 372 97.9 3,800 122 ND
Notes are provided on the final page of this table.
26,000 (Total Xylenes)
48,000 (Total Xylenes)
38,000 (Total Xylenes)
FHR TYPE II MONITORING WELLS WITHIN APEX TERMINAL (Continued)
AMW-2
35,000 (Total Xylenes)25,000 (Total Xylenes)
38,000 (Total Xylenes)
50,000 (Total Xylenes)
20,000 (Total Xylenes)
Page 16 of 20
Appendix C
Historical Groundwater Results
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
Sample ID Date Collected
1 70 70 600 70 20 6 70 600 400 400 Variesm/p-Xyleneso-XyleneAll Other 8260B AnalytesGroundwater Clean-up Goal (ug/L)500Methyl Tert Butyl Ether (MTBE)Naphthalenen-PropylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneContaminant of Concern
Benzenen-Butylbenzenesec-ButylbenzeneEthylbenzeneIsopropylbenzene (Cumene)12/22/03 220 <1.0 <1.0 30 25 10 56 39 12 89 23 1,600 8.5 7.2
2/19/04 170 <50 <50 50 <50 <500 <250 <50 <50 100 <50 2,800 <50 ND
8/5/04 230 10 4.8J 70 43 4.6J 170 69 13 94 29 670 5.8 ND
2/16/05 360 <19 <30 130 42J <23 160J 59 34J 250 58 ND
8/22/05 200 11 4.2 60 42 28 96 72 9.8 71 29 3.8J
2/8/06 380 <19 <30 73 <33 <23 78J 49J 41J 63 <25 ND
8/7/2006 560 <9.5 <15 73 39 5,900 120 JB 65 490 93 32 ND
2/7/2007 410 <0.38 <0.60 550 52 32 260 100 60 270 130 ND
8/9/2007 380 8.0 4.2 160 37 86 100 B 61 49 39 19 ND
2/26/2008 33 <0.66 2.4 28 9.5 24 18 18 86 8.5 8.3 ND
8/19/2008 47 2.9 1.8 J 13 5.9 200 9.2 J 9.3 3.7 7.7 1.8 J 18
8/18/2009 45.5 <1.0 <1.0 24.9 5.3 8.7 37.9 5.9 3.9 28.6 16.7 134 80.2 6.3
8/12/2010 51.2 <1.0 <1.0 28.3 4.9 37.0 10.4 4.2 1.9 10.7 8.3 1,320 35.1 6.29 J
8/18/2011 112 <1.0 <0.95 91.9 25.3 1.9 J 80.7 35 255 146 47.9 841 8.5 ND
8/22/2012 28.2 <1.6 <1.5 <1.2 7.5 8.3 20.1 6.9 3.3 J 14.7 4.6 5,150 1.6 J 21.0
8/14/2013 93.6 <0.41 5.6 35.4 36.2 1.1 85.6 74.0 3.4 <0.31 43.0 276 <0.23 22.0 J
8/14/2014 47.8 <0.41 2.5 6.3 16.1 0.27 J 36.0 29.0 2.8 5.1 2.1 40.6 0.41 J ND
3/11/2015 55.2 <0.41 <0.38 52.9 41.0 0.59 J 92.4 76.0 6.8 14.3 5.7 1,360 6.5 ND
8/5/2015 25.1 6.2 3.7 23.1 19.6 <0.42 34.4 36.4 4.5 11.2 <0.72 473 0.90 J 144.8
8/1/2016 1.8 <0.41 0.92 J 6.8 1.9 <0.21 7.0 3.8 2.0 15.4 10.7 80.3 5.6 0.67 J
10/6/2016 2.3 NA NA 8.1 NA NA NA NA 1.5 NA NA 57.1 7.1 NA
8/9/2017 0.76 J <0.41 <0.38 2.2 0.84 J <0.21 3.1 2.2 <0.26 <0.31 4.1 2.5 <0.23 ND
8/8/2018 2.0 <0.41 <0.38 17.3 18.3 <0.21 42.0 43.0 2.0 17.8 26.7 399 1.2 1.58 J
8/7/2019 <0.30 3.5 3.7 17.5 15.1 <0.55 34.7 26.1 1.2 J 10.3 11.4 398 <0.44 ND
8/6/2020 1.5 J <0.47 3.7 26.2 13.2 0.74 J 14.0 22.1 4.5 16.9 9.1 309 3.1 ND
8/22/2021 <0.69 <0.98 <0.80 7.9 18.1 <0.84 38.6 28.1 2.1 37.1 14.5 353 2.6 15.3
8/3/2022 4.5 <0.49 2.8 47.6 30.3 3.7 18.1 38.6 2.0 7.7 21.0 75.9 <0.34 ND
Notes are provided on the final page of this table.
500 (Total Xylenes)
1,200 (Total Xylenes)
2,000 (Total Xylenes)
FHR TYPE II MONITORING WELLS WITHIN APEX TERMINAL (Continued)
AMW-3
9,200 (Total Xylenes)530 (Total Xylenes)
11,000 (Total Xylenes)
4,100 (Total Xylenes)
10,000 (Total Xylenes)
Page 17 of 20
Appendix C
Historical Groundwater Results
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
Sample ID Date Collected
1 70 70 600 70 20 6 70 600 400 400 Variesm/p-Xyleneso-XyleneAll Other 8260B AnalytesGroundwater Clean-up Goal (ug/L)500Methyl Tert Butyl Ether (MTBE)Naphthalenen-PropylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneContaminant of Concern
Benzenen-Butylbenzenesec-ButylbenzeneEthylbenzeneIsopropylbenzene (Cumene)12/22/03 200 15 18 11 14 240 26 26 2.8 140 110 68 <1.0 36
2/19/04 420 <10 13 21 28 110 <50 34 17 200 93 98 <10 ND
8/5/04
2/16/05
8/17/05
10/14/05 --------------
2/8/06
8/8/2006
2/7/2007 16,000 <1,900 <3,000 <3,100 <3,300 570,000 <600 <2,300 34,000 <2,200 <2,500 ND
3/30/2007 20,000 <190 <300 2,400 <330 140,000 <60 <230 43,000 860 310 J ND
8/17/2007 15,000 <33 40 J 2,200 220 31,000 120 J 260 33,000 1600 480 33 JB
2/25/2008 13,000 <66 <58 2,000 130 34,000 150 160 24,000 1,300 390 ND8/19/2008 9,800 <66 <58 3,200 280 31,000 80 320 32,000 2,000 580 ND
2/12/2009 7,000 <66 <58 2,100 160 1,300 150 180 36,000 1,100 330 ND
8/18/2009 6,510 <250 <250 2,770 267 3,800 1,270 292 22,000 1,820 561 9,490 3,990 1,720
11/18/2009 6,810 <200 <200 3,570 289 3,700 1,260 342 30,600 2,270 601 12,500 5,630 38.1 J
8/12/2010 3,310 <100 <100 846 67.5 J 1,100 <100 85.6 J 8,170 414 160 2,920 1,390 ND
8/19/2011 5,730 <20.5 <19.0 4,570 326 66.9 509 425 27,500 2,800 865 16,000 7,420 66.4 J
8/17/2012 1,730 <82.0 <76.0 3,600 215 <42.0 364 326 25,600 2,030 613 12,600 5,700 ND
8/13/2013 927 <82.0 <76.0 2,990 197 J <42.0 337 242 12,500 1,590 436 11,200 5,170 675
8/21/2014 796 <20.5 <19.0 3,110 215 <10.5 451 271 6,050 1,970 508 12,300 6,020 179.3
3/11/2015 1,120 <20.5 <19.0 3,410 <20.0 <10.5 483 293 7,290 1,890 <18.0 13,400 5,960 32.1 J
8/5/2015 780 <20.5 <19.0 2,030 180 <10.5 352 184 5,070 1,090 <18.0 8,660 3,620 84.7 J
8/1/2016 663 <41.0 <38.0 4,660 253 <21.0 505 247 12,100 1,770 480 16,300 8,350 128.1 J
8/9/2017 41.9 J <20.5 <19.0 3,240 171 <10.5 327 164 9,750 1,110 <18.0 12,600 5,940 ND
8/8/2018 <6.2 <10.2 <9.5 1,260 134 <5.2 410 226 3,560 1,700 426 5,410 3,040 54.9 J
8/7/2019 11.9 J <0.94 <8.0 2,710 121 <11.0 341 <7.4 2,640 1,040 <7.9 9,920 5,380 41.3
8/6/2020 <6.0 <9.4 <8.0 2,590 144 <11.0 550 <7.4 241 1,230 <7.9 10,600 5,410 16.9 J
8/21/2021 <17.2 <24.5 <20.0 2,730 250 <21.1 686 <17.0 247 2,260 <16.6 11,900 5,600 ND
8/3/2022 <17.2 <24.5 <20.0 2,770 253 <21.1 697 268 521 2,110 510 12,300 5,640 ND
Notes are provided on the final page of this table.
16,000 (Total Xylenes)
11,000 (Total Xylenes)
11,000 (Total Xylenes)
9,800 (Total Xylenes)
16,000 (Total Xylenes)
10,000 (Total Xylenes)
FHR TYPE II MONITORING WELLS WITHIN APEX TERMINAL (Continued)
AMW-4
0.8' FREE- PHASE PRODUCT PRESENT
2.10' FREE- PHASE PRODUCT PRESENT1.45' FREE- PHASE PRODUCT PRESENT
0.15' FREE-PHASE PRODUCT PRESENT
0.21' FREE-PHASE PRODUCT PRESENT
Page 18 of 20
Appendix C
Historical Groundwater Results
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
Sample ID Date Collected
1 70 70 600 70 20 6 70 600 400 400 Variesm/p-Xyleneso-XyleneAll Other 8260B AnalytesGroundwater Clean-up Goal (ug/L)500Methyl Tert Butyl Ether (MTBE)Naphthalenen-PropylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneContaminant of Concern
Benzenen-Butylbenzenesec-ButylbenzeneEthylbenzeneIsopropylbenzene (Cumene)12/22/2003 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 ND
2/19/04 <1.0 <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 1.3
8/5/04 <0.36 <0.31 <0.24 <0.34 <0.25 <0.31 <0.44 <0.32 <0.54 <0.19 <0.21 0.90J <0.35 ND
2/16/05 <0.54 <0.38 <0.60 <0.62 <0.66 <0.45 0.44J <0.45 <0.62 <0.44 <0.49 ND
8/22/05 <0.54 <0.38 <0.60 <0.62 <0.66 1.5J <0.12 <0.45 <0.62 <0.44 <0.49 ND
2/8/06 <0.54 <0.38 <0.60 <0.62 <0.66 2.8J <0.12 <0.45 <0.62 <0.44 <0.49 ND
8/7/2006 <0.54 <0.38 <0.60 <0.62 <0.66 2,400 <0.12 <0.45 <0.62 <0.44 <0.49 ND
2/7/2007 35 <3.8 <6.0 <6.2 <6.6 16,000 <1.2 <4.5 <6.2 <4.4 <4.9 ND
8/9/2007 430 <3.3 <2.9 3.8 J <2.7 8,400 <2.7 <3.4 4.9 J <2.7 <2.8 ND
2/26/2008 300 <3.3 <2.9 <3.0 <2.7 210 4.9 J <3.4 4.0 J <2.7 <2.8 ND
8/19/2008 110 <0.33 <0.29 <0.30 <0.27 87 1.6 J <0.34 0.60 J <0.27 <0.28 3.2
8/18/2009 15.6 <1.0 <1.0 <1.0 <1.0 54.5 4.7 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 23.58/12/2010 1.1 <1.0 <1.0 <1.0 0.60 J 60.3 <1.0 <1.0 <1.0 1.4 <1.0 3.9 0.77 J 382.9
8/18/2011 4.3 <0.41 <0.38 0.32 J 8.6 74.3 18.2 6.7 1.0 J 1.7 1.4 3.1 0.36 J 317.8
8/20/2012 <0.25 <0.41 <0.38 <0.30 5.1 15.8 11.8 3.2 0.27 J <0.31 <0.36 0.78 J <0.23 270.8
8/14/2013 <0.25 <0.41 <0.38 <0.30 4.4 2.1 0.93 J 3.6 <0.26 <0.31 <0.36 1.2 J <0.23 27.8
8/14/2014 0.29 J <0.41 <0.38 <0.30 8.7 31.2 0.97 J 3.9 <0.26 <0.31 <0.36 1.0 J 0.36 J 154.5
3/11/2015 6.6 <0.41 <0.38 52.7 <0.40 29.3 2.3 2.9 14.9 1.4 <0.36 142 91.2 10.3
8/5/2015 <0.25 <0.41 <0.38 <0.30 <0.40 0.22 J <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 ND
8/1/2016 0.26 J <0.41 0.71 J <0.30 24.1 12.0 0.68 J 26.0 0.63 J 0.33 J <0.36 2.8 0.62 J 9.4
8/9/2017 <0.25 <0.41 1.3 1.3 12.7 4.7 10.8 16.2 0.62 J 7.2 3.9 22.4 1.0 25.9
8/8/2018 <0.25 <0.41 1.1 <0.30 16.4 4.5 0.33 J 11.9 <0.26 <0.31 <0.36 1.4 J 0.34 J 2.4
8/7/2019 <0.15 <0.23 0.84 J <0.26 17.0 6.4 26.4 7.0 <0.24 2.1 4.5 5.1 0.39 J 4.1
8/6/2020 <0.15 <0.23 0.46 J <0.26 5.5 0.95 J <0.35 1.8 <0.24 <0.17 <0.20 <0.41 <0.22 5.63 J
8/21/2021 <0.34 <0.49 <0.40 <0.30 18.4 6.2 <0.64 2.3 <0.48 <0.50 <0.33 <0.71 <0.34 5.9
8/3/2022 <0.34 <0.49 <0.40 <0.30 7.8 1.0 <0.64 1.5 <0.48 <0.50 <0.33 <0.71 <0.34 1.5
12/22/03 76 <1.0 2.7 5.3 4.1 24 <1.0 1.1 1.1 3.4 <1.0 11 <1.0 ND
2/19/04 66 2.6 4.2 3.5 5.5 24 5.7 1.8 2.2 17 <5.0 23 2.2 ND
8/5/04 210E 3.2 5.5 1.9 6 59 1.1 J 2.4 3.5 23 8.5 20 2.6 ND
2/16/05 82 3.2 3.4 2.8 12 70 11 3.8 2.2 35 6.9 1.7J
8/22/05 5.9 2.2 2.8 <0.62 6.2 28 6.7 0.95 J 1.3 9.5 2.9 ND
2/8/06 20 1.8J <1.2 <1.2 9.4 21 4.8 J 1.8 J <1.2 20 2.8 ND
8/7/2006 170 <0.76 2.9 5.2 5.3 1,900 1.3 J 1.8 J 7.2 45 10 ND
2/7/2007 41 <0.38 3.3 <0.62 8 18 1.4 J 2.5 0.98 J 36 8.4 2.5 J
8/9/2007 220 3.2 4.9 5.1 11 65 9.4 JB 7.2 3.4 59 19 ND
2/26/2008 200 <0.66 5.5 1.2 J 8.3 26 7.5 J 6.3 3.6 43 12 ND8/19/2008 200 1.9 J 2.4 0.80 J 6.2 40 0.80 J 1.2 J 3.9 15 3.6 ND
8/18/2009 60.1 <1.0 2.4 <1.0 8.7 8.1 <1.0 <1.0 1.7 8.2 2.2 3.7 1.2 2.2
8/21/2012 1.5 <0.41 0.75 J <0.30 3.0 1.4 0.34 J <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 ND
8/14/2013 34.0 <0.41 2.5 5.0 13.7 2.6 0.69 J 1.7 28.0 8.0 1.8 25.1 1.4 16.6 J
8/14/2014 0.82 J <0.41 <0.38 <0.30 <0.40 <0.21 <0.24 <0.42 0.54 J <0.31 <0.36 <0.66 <0.23 ND
3/11/2015 309 <0.41 <0.38 48.8 7.3 6.6 8.6 3.0 207 25.4 6.5 231 34.2 57.14 J
8/5/2015 294 <1.0 <0.95 30.6 5.2 6.4 13.1 3.3 43.1 29.7 8.7 134 18.4 ND
8/1/2016 168 0.78 J <0.38 8.8 5.3 22.0 3.6 1.8 2.2 18.1 3.8 95.3 2.3 0.22 J
8/9/2017 30.2 <0.41 <0.38 0.69 J 1.9 <0.21 <0.24 <0.42 <0.26 1.8 0.48 J 6.4 0.29 J ND
Notes are provided on the final page of this table.
AMW-6
240 (Total Xylenes)
3.2 (Total Xylenes)
370 (Total Xylenes)
38 (Total Xylenes)
6.9 (Total Xylenes)
28 (Total Xylenes)
19 (Total Xylenes)
15 (Total Xylenes)
FHR TYPE II MONITORING WELLS WITHIN APEX TERMINAL (Continued)
AMW-5
<1.6 (Total Xylenes)<1.3 (Total Xylenes)
<1.3 (Total Xylenes)
<1.3 (Total Xylenes)
<13 (Total Xylenes)
24 (Total Xylenes)
23 (Total Xylenes)
0.88 J (Total Xylenes)
Page 19 of 20
Appendix C
Historical Groundwater Results
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
Sample ID Date Collected
1 70 70 600 70 20 6 70 600 400 400 Variesm/p-Xyleneso-XyleneAll Other 8260B AnalytesGroundwater Clean-up Goal (ug/L)500Methyl Tert Butyl Ether (MTBE)Naphthalenen-PropylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneContaminant of Concern
Benzenen-Butylbenzenesec-ButylbenzeneEthylbenzeneIsopropylbenzene (Cumene)3/12/2015 <0.62 <1.0 <0.95 1.2 J <1.0 86.6 6.2 <1.0 <0.65 1.2 J <0.90 <1.6 <0.58 3.3 J
8/5/2015 <0.25 <0.41 <0.38 0.99 J <0.40 82.5 0.77 J <0.42 0.33 J 0.60 J <0.36 4.3 <0.23 32.8 J
8/1/2016 <0.25 <0.41 <0.38 0.53 J <0.40 72.7 0.33 J <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 14.0
8/8/2017 <0.25 <0.41 <0.38 0.50 J <0.40 34.8 0.29 J <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 6.3
8/8/2018 <0.25 <0.41 <0.38 <0.30 <0.40 1.7 <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 0.35 J
8/7/2019 <0.15 <0.23 <0.20 <0.26 <0.20 12.1 <0.35 <0.18 <0.24 <0.17 <0.20 <0.41 <0.22 ND
8/6/2020 <0.15 <0.23 <0.20 <0.26 <0.20 13.7 0.59 J <0.18 <0.24 <0.17 <0.20 3.0 <0.22 ND
8/23/2021 <0.34 <0.49 <0.40 <0.30 <0.33 7.6 <0.64 <0.34 <0.48 <0.50 <0.33 <0.71 <0.34 ND
3/11/2014 <0.25 <0.41 <0.38 <0.30 <0.40 37.0 <0.24 <0.42 <0.26 <0.31 <0.36 12.8 <0.23 ND
4/9/2014 <0.25 <0.41 <0.38 <0.30 <0.40 28.3 <0.24 <0.42 <0.26 <0.31 <0.36 2.2 <0.23 ND5/20/2014 <0.25 <0.41 <0.38 <0.30 <0.40 23.8 <0.24 <0.42 <0.26 <0.31 <0.36 1.3 J <0.23 ND
8/14/2014 <0.25 <0.41 <0.38 <0.30 <0.40 21.2 <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 ND
10/23/2014 <0.25 <0.41 <0.38 <0.30 <0.40 37.8 <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 ND
3/12/2015 <0.25 <0.41 <0.38 <0.30 <0.40 42.0 <0.24 <0.42 <0.26 <0.31 <0.36 0.87 J <0.23 ND
8/5/2015 <0.25 <0.41 <0.38 <0.30 <0.40 22.6 <0.24 <0.42 <0.26 <0.31 <0.36 0.73 J <0.23 3.9 J
8/1/2016 <0.25 <0.41 <0.38 <0.30 <0.40 27.9 <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 ND
8/9/2017 <0.25 <0.41 <0.38 <0.30 <0.40 9.9 0.61 J <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 ND
8/7/2018 <0.25 <0.41 <0.38 <0.30 <0.40 19.7 <0.24 <0.42 <0.26 <0.31 <0.36 0.82 J <0.23 ND
8/7/2019 <0.15 <0.23 <0.20 2.0 <0.20 12.5 1.4 <0.18 0.95 J 1.5 0.48 J 10.1 3.8 ND
8/6/2020 <0.15 <0.23 <0.20 <0.26 <0.20 6.2 <0.35 <0.18 <0.24 <0.17 <0.20 <0.41 <0.22 ND
8/22/2021 <0.34 <0.49 <0.40 <0.30 <0.33 12.5 <0.64 <0.34 <0.48 <0.50 <0.33 <0.71 <0.34 ND
10/2/2013***<0.25 <0.25 <0.25 <0.25 <0.25 0.53 <1.0 <0.25 <0.25 <0.25 <0.25 <0.50 <0.25 0.74 J
3/11/2015 0.49 J <0.41 <0.38 <0.30 <0.40 0.43 J 0.36 J <0.42 0.48 J <0.31 <0.36 1.1 J <0.23 ND
Notes:
All results in micrograms per liter (ug/L).
- = No data
Shaded concentrations exceed the 15A North Carolina Administrative Code (NCAC) 2L.0202 North Carolina Groundwater Quality Standard (2L GWQS), updated April 1, 2013.
Refer to laboratory reports for other 8260 analytes detected.
ND = Not detected
ND1 = Chloroform was also detected in KMW-5 with a result of 7.5 ug/l.
ND2 = Tert-butylbenzene was detected in KMW-3 with a result of 5.2 ug/l.
BQL = Below Quantitation Limits
* = Determined with EPA Method 602 analysis
** = Temporary wells have been permanently abandoned and location of temporary wells were last documented in the Corrective Action Plan Addendum dated August 9, 2002.
*** = Groundwater sampled was analyzed per EPA Method 6200B
J = Value is estimated concentration that is less than RL, but greater than or equal to the MDL.
E = The reported result exceeded the calibration range of the instrument.
D = The reported result is from a secondary dilution.
B = Compound was found in blank and sample.
October/November 2016, April 2017 and February 2019 data is from post EAB sampling events and select samples from these events were analyzed via EPA Method 8260B for BTEX constituents only.
March 2017 data is from a post EAB sampling event and samples were analyzed for the full 8260 list.
PW-1
< = Less than method detection limit or reporting limit
NA = Not Analyzed
TYPE III MONITORING WELLS
KDW-1
FHR TYPE III MONITORING WELLS WITHIN APEX TERMINAL
ADW-1
WATER SUPPLY WELLS
Page 20 of 20

Appendix D

Laboratory Analytical Reports

#=CL#
August 09, 2022
LIMS USE: FR - MATT MAHONY
LIMS OBJECT ID: 92618510
92618510
Project:
Pace Project No.:
RE:
Matt Mahony
Tetra Tech
805 E 20th St
Charlotte, NC 28205
LOADING RACK SITE WIILMINGTON
Dear Matt Mahony:
Enclosed are the analytical results for sample(s) received by the laboratory on August 04, 2022. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Nikita Kuruganty
[e-mail]
Project Manager
[phone]
Enclosures
cc: Michael Christopher
Rod Kremer
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 32
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92618510
LOADING RACK SITE WIILMINGTON
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 32
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92618510
LOADING RACK SITE WIILMINGTON
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92618510001 AMW-2 EPA 8260D 69 PASI-CCL
92618510002 AMW-3 EPA 8260D 69 PASI-CCL
92618510003 AMW-4 EPA 8260D 69 PASI-CCL
92618510004 AMW-5 EPA 8260D 69 PASI-CCL
92618510005 KMW-1 EPA 8260D 69 PASI-CCL
92618510006 KMW-3 EPA 8260D 69 PASI-CCL
92618510007 KMW-18 EPA 8260D 69 PASI-CCL
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92618510
LOADING RACK SITE WIILMINGTON
Sample: AMW-2 Lab ID: 92618510001 Collected: 08/03/22 12:26 Received: 08/04/22 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 08/05/22 09:18 67-64-1312 12.5
Benzene ND ug/L 08/05/22 09:18 71-43-212.5 12.5
Bromobenzene ND ug/L 08/05/22 09:18 108-86-112.5 12.5
Bromochloromethane ND ug/L 08/05/22 09:18 74-97-512.5 12.5
Bromodichloromethane ND ug/L 08/05/22 09:18 75-27-412.5 12.5
Bromoform ND ug/L 08/05/22 09:18 75-25-212.5 12.5
Bromomethane ND ug/L 08/05/22 09:18 74-83-9 v225.0 12.5
2-Butanone (MEK)ND ug/L 08/05/22 09:18 78-93-362.5 12.5
n-Butylbenzene ND ug/L 08/05/22 09:18 104-51-812.5 12.5
sec-Butylbenzene ND ug/L 08/05/22 09:18 135-98-812.5 12.5
Carbon tetrachloride ND ug/L 08/05/22 09:18 56-23-512.5 12.5
Chlorobenzene ND ug/L 08/05/22 09:18 108-90-712.5 12.5
Chloroethane ND ug/L 08/05/22 09:18 75-00-312.5 12.5
Chloroform ND ug/L 08/05/22 09:18 67-66-312.5 12.5
Chloromethane ND ug/L 08/05/22 09:18 74-87-312.5 12.5
2-Chlorotoluene ND ug/L 08/05/22 09:18 95-49-812.5 12.5
4-Chlorotoluene ND ug/L 08/05/22 09:18 106-43-412.5 12.5
1,2-Dibromo-3-chloropropane ND ug/L 08/05/22 09:18 96-12-825.0 12.5
Dibromochloromethane ND ug/L 08/05/22 09:18 124-48-112.5 12.5
1,2-Dibromoethane (EDB)ND ug/L 08/05/22 09:18 106-93-412.5 12.5
Dibromomethane ND ug/L 08/05/22 09:18 74-95-312.5 12.5
1,2-Dichlorobenzene ND ug/L 08/05/22 09:18 95-50-112.5 12.5
1,3-Dichlorobenzene ND ug/L 08/05/22 09:18 541-73-112.5 12.5
1,4-Dichlorobenzene ND ug/L 08/05/22 09:18 106-46-712.5 12.5
Dichlorodifluoromethane ND ug/L 08/05/22 09:18 75-71-812.5 12.5
1,1-Dichloroethane ND ug/L 08/05/22 09:18 75-34-312.5 12.5
1,2-Dichloroethane ND ug/L 08/05/22 09:18 107-06-212.5 12.5
1,1-Dichloroethene ND ug/L 08/05/22 09:18 75-35-412.5 12.5
cis-1,2-Dichloroethene ND ug/L 08/05/22 09:18 156-59-212.5 12.5
trans-1,2-Dichloroethene ND ug/L 08/05/22 09:18 156-60-512.5 12.5
1,2-Dichloropropane ND ug/L 08/05/22 09:18 78-87-512.5 12.5
1,3-Dichloropropane ND ug/L 08/05/22 09:18 142-28-912.5 12.5
2,2-Dichloropropane ND ug/L 08/05/22 09:18 594-20-712.5 12.5
1,1-Dichloropropene ND ug/L 08/05/22 09:18 563-58-612.5 12.5
cis-1,3-Dichloropropene ND ug/L 08/05/22 09:18 10061-01-512.5 12.5
trans-1,3-Dichloropropene ND ug/L 08/05/22 09:18 10061-02-612.5 12.5
Diisopropyl ether ND ug/L 08/05/22 09:18 108-20-312.5 12.5
Ethylbenzene 282 ug/L 08/05/22 09:18 100-41-412.5 12.5
Hexachloro-1,3-butadiene ND ug/L 08/05/22 09:18 87-68-325.0 12.5
2-Hexanone ND ug/L 08/05/22 09:18 591-78-662.5 12.5
Isopropylbenzene (Cumene)27.3 ug/L 08/05/22 09:18 98-82-812.5 12.5
p-Isopropyltoluene ND ug/L 08/05/22 09:18 99-87-612.5 12.5
Methylene Chloride ND ug/L 08/05/22 09:18 75-09-262.5 12.5
4-Methyl-2-pentanone (MIBK)ND ug/L 08/05/22 09:18 108-10-162.5 12.5
Methyl-tert-butyl ether ND ug/L 08/05/22 09:18 1634-04-412.5 12.5
Naphthalene 117 ug/L 08/05/22 09:18 91-20-312.5 12.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/09/2022 09:52 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92618510
LOADING RACK SITE WIILMINGTON
Sample: AMW-2 Lab ID: 92618510001 Collected: 08/03/22 12:26 Received: 08/04/22 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
n-Propylbenzene 47.8 ug/L 08/05/22 09:18 103-65-112.5 12.5
Styrene ND ug/L 08/05/22 09:18 100-42-512.5 12.5
1,1,1,2-Tetrachloroethane ND ug/L 08/05/22 09:18 630-20-612.5 12.5
1,1,2,2-Tetrachloroethane ND ug/L 08/05/22 09:18 79-34-512.5 12.5
Tetrachloroethene ND ug/L 08/05/22 09:18 127-18-412.5 12.5
Toluene 15.0 ug/L 08/05/22 09:18 108-88-312.5 12.5
1,2,3-Trichlorobenzene ND ug/L 08/05/22 09:18 87-61-612.5 12.5
1,2,4-Trichlorobenzene ND ug/L 08/05/22 09:18 120-82-112.5 12.5
1,1,1-Trichloroethane ND ug/L 08/05/22 09:18 71-55-612.5 12.5
1,1,2-Trichloroethane ND ug/L 08/05/22 09:18 79-00-512.5 12.5
Trichloroethene ND ug/L 08/05/22 09:18 79-01-612.5 12.5
Trichlorofluoromethane ND ug/L 08/05/22 09:18 75-69-412.5 12.5
1,2,3-Trichloropropane ND ug/L 08/05/22 09:18 96-18-412.5 12.5
1,2,4-Trimethylbenzene 372 ug/L 08/05/22 09:18 95-63-612.5 12.5
1,3,5-Trimethylbenzene 97.9 ug/L 08/05/22 09:18 108-67-812.5 12.5
Vinyl acetate ND ug/L 08/05/22 09:18 108-05-425.0 12.5
Vinyl chloride ND ug/L 08/05/22 09:18 75-01-412.5 12.5
Xylene (Total)3920 ug/L 08/05/22 09:18 1330-20-712.5 12.5
m&p-Xylene 3800 ug/L 08/05/22 09:18 179601-23-125.0 12.5
o-Xylene 122 ug/L 08/05/22 09:18 95-47-612.5 12.5
Surrogates
4-Bromofluorobenzene (S)99 %08/05/22 09:18 460-00-470-130 12.5
1,2-Dichloroethane-d4 (S)104 %08/05/22 09:18 17060-07-070-130 12.5
Toluene-d8 (S)99 %08/05/22 09:18 2037-26-570-130 12.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/09/2022 09:52 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92618510
LOADING RACK SITE WIILMINGTON
Sample: AMW-3 Lab ID: 92618510002 Collected: 08/03/22 10:00 Received: 08/04/22 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 08/05/22 22:13 67-64-125.0 1
Benzene 4.5 ug/L 08/05/22 22:13 71-43-21.0 1
Bromobenzene ND ug/L 08/05/22 22:13 108-86-11.0 1
Bromochloromethane ND ug/L 08/05/22 22:13 74-97-51.0 1
Bromodichloromethane ND ug/L 08/05/22 22:13 75-27-41.0 1
Bromoform ND ug/L 08/05/22 22:13 75-25-21.0 1
Bromomethane ND ug/L 08/05/22 22:13 74-83-9 IH,IK,v12.0 1
2-Butanone (MEK)ND ug/L 08/05/22 22:13 78-93-35.0 1
n-Butylbenzene ND ug/L 08/05/22 22:13 104-51-81.0 1
sec-Butylbenzene 2.8 ug/L 08/05/22 22:13 135-98-81.0 1
Carbon tetrachloride ND ug/L 08/05/22 22:13 56-23-51.0 1
Chlorobenzene ND ug/L 08/05/22 22:13 108-90-71.0 1
Chloroethane ND ug/L 08/05/22 22:13 75-00-31.0 1
Chloroform ND ug/L 08/05/22 22:13 67-66-31.0 1
Chloromethane ND ug/L 08/05/22 22:13 74-87-31.0 1
2-Chlorotoluene ND ug/L 08/05/22 22:13 95-49-81.0 1
4-Chlorotoluene ND ug/L 08/05/22 22:13 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 08/05/22 22:13 96-12-82.0 1
Dibromochloromethane ND ug/L 08/05/22 22:13 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 08/05/22 22:13 106-93-41.0 1
Dibromomethane ND ug/L 08/05/22 22:13 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 08/05/22 22:13 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 08/05/22 22:13 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 08/05/22 22:13 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 08/05/22 22:13 75-71-81.0 1
1,1-Dichloroethane ND ug/L 08/05/22 22:13 75-34-31.0 1
1,2-Dichloroethane ND ug/L 08/05/22 22:13 107-06-21.0 1
1,1-Dichloroethene ND ug/L 08/05/22 22:13 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 08/05/22 22:13 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 08/05/22 22:13 156-60-51.0 1
1,2-Dichloropropane ND ug/L 08/05/22 22:13 78-87-51.0 1
1,3-Dichloropropane ND ug/L 08/05/22 22:13 142-28-91.0 1
2,2-Dichloropropane ND ug/L 08/05/22 22:13 594-20-71.0 1
1,1-Dichloropropene ND ug/L 08/05/22 22:13 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 08/05/22 22:13 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 08/05/22 22:13 10061-02-61.0 1
Diisopropyl ether ND ug/L 08/05/22 22:13 108-20-31.0 1
Ethylbenzene 47.6 ug/L 08/05/22 22:13 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 08/05/22 22:13 87-68-32.0 1
2-Hexanone ND ug/L 08/05/22 22:13 591-78-65.0 1
Isopropylbenzene (Cumene)30.3 ug/L 08/05/22 22:13 98-82-81.0 1
p-Isopropyltoluene ND ug/L 08/05/22 22:13 99-87-61.0 1
Methylene Chloride ND ug/L 08/05/22 22:13 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/05/22 22:13 108-10-15.0 1
Methyl-tert-butyl ether 3.7 ug/L 08/05/22 22:13 1634-04-41.0 1
Naphthalene 18.1 ug/L 08/05/22 22:13 91-20-31.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/09/2022 09:52 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92618510
LOADING RACK SITE WIILMINGTON
Sample: AMW-3 Lab ID: 92618510002 Collected: 08/03/22 10:00 Received: 08/04/22 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
n-Propylbenzene 38.6 ug/L 08/05/22 22:13 103-65-11.0 1
Styrene ND ug/L 08/05/22 22:13 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 08/05/22 22:13 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 08/05/22 22:13 79-34-51.0 1
Tetrachloroethene ND ug/L 08/05/22 22:13 127-18-41.0 1
Toluene 2.0 ug/L 08/05/22 22:13 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 08/05/22 22:13 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 08/05/22 22:13 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 08/05/22 22:13 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 08/05/22 22:13 79-00-51.0 1
Trichloroethene ND ug/L 08/05/22 22:13 79-01-61.0 1
Trichlorofluoromethane ND ug/L 08/05/22 22:13 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 08/05/22 22:13 96-18-41.0 1
1,2,4-Trimethylbenzene 7.7 ug/L 08/05/22 22:13 95-63-61.0 1
1,3,5-Trimethylbenzene 21.0 ug/L 08/05/22 22:13 108-67-81.0 1
Vinyl acetate ND ug/L 08/05/22 22:13 108-05-42.0 1
Vinyl chloride ND ug/L 08/05/22 22:13 75-01-41.0 1
Xylene (Total)75.9 ug/L 08/05/22 22:13 1330-20-71.0 1
m&p-Xylene 75.9 ug/L 08/05/22 22:13 179601-23-12.0 1
o-Xylene ND ug/L 08/05/22 22:13 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)99 %08/05/22 22:13 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %08/05/22 22:13 17060-07-070-130 1
Toluene-d8 (S)98 %08/05/22 22:13 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/09/2022 09:52 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92618510
LOADING RACK SITE WIILMINGTON
Sample: AMW-4 Lab ID: 92618510003 Collected: 08/03/22 12:00 Received: 08/04/22 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 08/05/22 10:12 67-64-11250 50
Benzene ND ug/L 08/05/22 10:12 71-43-250.0 50
Bromobenzene ND ug/L 08/05/22 10:12 108-86-150.0 50
Bromochloromethane ND ug/L 08/05/22 10:12 74-97-550.0 50
Bromodichloromethane ND ug/L 08/05/22 10:12 75-27-450.0 50
Bromoform ND ug/L 08/05/22 10:12 75-25-250.0 50
Bromomethane ND ug/L 08/05/22 10:12 74-83-9 v2100 50
2-Butanone (MEK)ND ug/L 08/05/22 10:12 78-93-3250 50
n-Butylbenzene ND ug/L 08/05/22 10:12 104-51-850.0 50
sec-Butylbenzene ND ug/L 08/05/22 10:12 135-98-850.0 50
Carbon tetrachloride ND ug/L 08/05/22 10:12 56-23-550.0 50
Chlorobenzene ND ug/L 08/05/22 10:12 108-90-750.0 50
Chloroethane ND ug/L 08/05/22 10:12 75-00-350.0 50
Chloroform ND ug/L 08/05/22 10:12 67-66-350.0 50
Chloromethane ND ug/L 08/05/22 10:12 74-87-350.0 50
2-Chlorotoluene ND ug/L 08/05/22 10:12 95-49-850.0 50
4-Chlorotoluene ND ug/L 08/05/22 10:12 106-43-450.0 50
1,2-Dibromo-3-chloropropane ND ug/L 08/05/22 10:12 96-12-8100 50
Dibromochloromethane ND ug/L 08/05/22 10:12 124-48-150.0 50
1,2-Dibromoethane (EDB)ND ug/L 08/05/22 10:12 106-93-450.0 50
Dibromomethane ND ug/L 08/05/22 10:12 74-95-350.0 50
1,2-Dichlorobenzene ND ug/L 08/05/22 10:12 95-50-150.0 50
1,3-Dichlorobenzene ND ug/L 08/05/22 10:12 541-73-150.0 50
1,4-Dichlorobenzene ND ug/L 08/05/22 10:12 106-46-750.0 50
Dichlorodifluoromethane ND ug/L 08/05/22 10:12 75-71-850.0 50
1,1-Dichloroethane ND ug/L 08/05/22 10:12 75-34-350.0 50
1,2-Dichloroethane ND ug/L 08/05/22 10:12 107-06-250.0 50
1,1-Dichloroethene ND ug/L 08/05/22 10:12 75-35-450.0 50
cis-1,2-Dichloroethene ND ug/L 08/05/22 10:12 156-59-250.0 50
trans-1,2-Dichloroethene ND ug/L 08/05/22 10:12 156-60-550.0 50
1,2-Dichloropropane ND ug/L 08/05/22 10:12 78-87-550.0 50
1,3-Dichloropropane ND ug/L 08/05/22 10:12 142-28-950.0 50
2,2-Dichloropropane ND ug/L 08/05/22 10:12 594-20-750.0 50
1,1-Dichloropropene ND ug/L 08/05/22 10:12 563-58-650.0 50
cis-1,3-Dichloropropene ND ug/L 08/05/22 10:12 10061-01-550.0 50
trans-1,3-Dichloropropene ND ug/L 08/05/22 10:12 10061-02-650.0 50
Diisopropyl ether ND ug/L 08/05/22 10:12 108-20-350.0 50
Ethylbenzene 2770 ug/L 08/05/22 10:12 100-41-450.0 50
Hexachloro-1,3-butadiene ND ug/L 08/05/22 10:12 87-68-3100 50
2-Hexanone ND ug/L 08/05/22 10:12 591-78-6250 50
Isopropylbenzene (Cumene)253 ug/L 08/05/22 10:12 98-82-850.0 50
p-Isopropyltoluene ND ug/L 08/05/22 10:12 99-87-650.0 50
Methylene Chloride ND ug/L 08/05/22 10:12 75-09-2250 50
4-Methyl-2-pentanone (MIBK)ND ug/L 08/05/22 10:12 108-10-1250 50
Methyl-tert-butyl ether ND ug/L 08/05/22 10:12 1634-04-450.0 50
Naphthalene 697 ug/L 08/05/22 10:12 91-20-350.0 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/09/2022 09:52 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92618510
LOADING RACK SITE WIILMINGTON
Sample: AMW-4 Lab ID: 92618510003 Collected: 08/03/22 12:00 Received: 08/04/22 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
n-Propylbenzene 268 ug/L 08/05/22 10:12 103-65-150.0 50
Styrene ND ug/L 08/05/22 10:12 100-42-550.0 50
1,1,1,2-Tetrachloroethane ND ug/L 08/05/22 10:12 630-20-650.0 50
1,1,2,2-Tetrachloroethane ND ug/L 08/05/22 10:12 79-34-550.0 50
Tetrachloroethene ND ug/L 08/05/22 10:12 127-18-450.0 50
Toluene 521 ug/L 08/05/22 10:12 108-88-350.0 50
1,2,3-Trichlorobenzene ND ug/L 08/05/22 10:12 87-61-650.0 50
1,2,4-Trichlorobenzene ND ug/L 08/05/22 10:12 120-82-150.0 50
1,1,1-Trichloroethane ND ug/L 08/05/22 10:12 71-55-650.0 50
1,1,2-Trichloroethane ND ug/L 08/05/22 10:12 79-00-550.0 50
Trichloroethene ND ug/L 08/05/22 10:12 79-01-650.0 50
Trichlorofluoromethane ND ug/L 08/05/22 10:12 75-69-450.0 50
1,2,3-Trichloropropane ND ug/L 08/05/22 10:12 96-18-450.0 50
1,2,4-Trimethylbenzene 2110 ug/L 08/05/22 10:12 95-63-650.0 50
1,3,5-Trimethylbenzene 510 ug/L 08/05/22 10:12 108-67-850.0 50
Vinyl acetate ND ug/L 08/05/22 10:12 108-05-4100 50
Vinyl chloride ND ug/L 08/05/22 10:12 75-01-450.0 50
Xylene (Total)18000 ug/L 08/05/22 10:12 1330-20-750.0 50
m&p-Xylene 12300 ug/L 08/05/22 10:12 179601-23-1100 50
o-Xylene 5640 ug/L 08/05/22 10:12 95-47-650.0 50
Surrogates
4-Bromofluorobenzene (S)97 %08/05/22 10:12 460-00-470-130 50
1,2-Dichloroethane-d4 (S)104 %08/05/22 10:12 17060-07-070-130 50
Toluene-d8 (S)99 %08/05/22 10:12 2037-26-570-130 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/09/2022 09:52 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92618510
LOADING RACK SITE WIILMINGTON
Sample: AMW-5 Lab ID: 92618510004 Collected: 08/03/22 11:20 Received: 08/04/22 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 08/05/22 06:35 67-64-125.0 1
Benzene ND ug/L 08/05/22 06:35 71-43-21.0 1
Bromobenzene ND ug/L 08/05/22 06:35 108-86-11.0 1
Bromochloromethane ND ug/L 08/05/22 06:35 74-97-51.0 1
Bromodichloromethane ND ug/L 08/05/22 06:35 75-27-41.0 1
Bromoform ND ug/L 08/05/22 06:35 75-25-21.0 1
Bromomethane ND ug/L 08/05/22 06:35 74-83-9 v22.0 1
2-Butanone (MEK)ND ug/L 08/05/22 06:35 78-93-35.0 1
n-Butylbenzene ND ug/L 08/05/22 06:35 104-51-81.0 1
sec-Butylbenzene ND ug/L 08/05/22 06:35 135-98-81.0 1
Carbon tetrachloride ND ug/L 08/05/22 06:35 56-23-51.0 1
Chlorobenzene ND ug/L 08/05/22 06:35 108-90-71.0 1
Chloroethane ND ug/L 08/05/22 06:35 75-00-31.0 1
Chloroform ND ug/L 08/05/22 06:35 67-66-31.0 1
Chloromethane ND ug/L 08/05/22 06:35 74-87-31.0 1
2-Chlorotoluene ND ug/L 08/05/22 06:35 95-49-81.0 1
4-Chlorotoluene ND ug/L 08/05/22 06:35 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 08/05/22 06:35 96-12-82.0 1
Dibromochloromethane ND ug/L 08/05/22 06:35 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 08/05/22 06:35 106-93-41.0 1
Dibromomethane ND ug/L 08/05/22 06:35 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 08/05/22 06:35 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 08/05/22 06:35 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 08/05/22 06:35 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 08/05/22 06:35 75-71-81.0 1
1,1-Dichloroethane ND ug/L 08/05/22 06:35 75-34-31.0 1
1,2-Dichloroethane ND ug/L 08/05/22 06:35 107-06-21.0 1
1,1-Dichloroethene ND ug/L 08/05/22 06:35 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 08/05/22 06:35 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 08/05/22 06:35 156-60-51.0 1
1,2-Dichloropropane ND ug/L 08/05/22 06:35 78-87-51.0 1
1,3-Dichloropropane ND ug/L 08/05/22 06:35 142-28-91.0 1
2,2-Dichloropropane ND ug/L 08/05/22 06:35 594-20-71.0 1
1,1-Dichloropropene ND ug/L 08/05/22 06:35 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 08/05/22 06:35 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 08/05/22 06:35 10061-02-61.0 1
Diisopropyl ether 1.5 ug/L 08/05/22 06:35 108-20-31.0 1
Ethylbenzene ND ug/L 08/05/22 06:35 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 08/05/22 06:35 87-68-32.0 1
2-Hexanone ND ug/L 08/05/22 06:35 591-78-65.0 1
Isopropylbenzene (Cumene)7.8 ug/L 08/05/22 06:35 98-82-81.0 1
p-Isopropyltoluene ND ug/L 08/05/22 06:35 99-87-61.0 1
Methylene Chloride ND ug/L 08/05/22 06:35 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/05/22 06:35 108-10-15.0 1
Methyl-tert-butyl ether 1.0 ug/L 08/05/22 06:35 1634-04-41.0 1
Naphthalene ND ug/L 08/05/22 06:35 91-20-31.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/09/2022 09:52 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92618510
LOADING RACK SITE WIILMINGTON
Sample: AMW-5 Lab ID: 92618510004 Collected: 08/03/22 11:20 Received: 08/04/22 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
n-Propylbenzene 1.5 ug/L 08/05/22 06:35 103-65-11.0 1
Styrene ND ug/L 08/05/22 06:35 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 08/05/22 06:35 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 08/05/22 06:35 79-34-51.0 1
Tetrachloroethene ND ug/L 08/05/22 06:35 127-18-41.0 1
Toluene ND ug/L 08/05/22 06:35 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 08/05/22 06:35 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 08/05/22 06:35 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 08/05/22 06:35 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 08/05/22 06:35 79-00-51.0 1
Trichloroethene ND ug/L 08/05/22 06:35 79-01-61.0 1
Trichlorofluoromethane ND ug/L 08/05/22 06:35 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 08/05/22 06:35 96-18-41.0 1
1,2,4-Trimethylbenzene ND ug/L 08/05/22 06:35 95-63-61.0 1
1,3,5-Trimethylbenzene ND ug/L 08/05/22 06:35 108-67-81.0 1
Vinyl acetate ND ug/L 08/05/22 06:35 108-05-42.0 1
Vinyl chloride ND ug/L 08/05/22 06:35 75-01-41.0 1
Xylene (Total)ND ug/L 08/05/22 06:35 1330-20-71.0 1
m&p-Xylene ND ug/L 08/05/22 06:35 179601-23-12.0 1
o-Xylene ND ug/L 08/05/22 06:35 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)95 %08/05/22 06:35 460-00-470-130 1
1,2-Dichloroethane-d4 (S)103 %08/05/22 06:35 17060-07-070-130 1
Toluene-d8 (S)99 %08/05/22 06:35 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/09/2022 09:52 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92618510
LOADING RACK SITE WIILMINGTON
Sample: KMW-1 Lab ID: 92618510005 Collected: 08/03/22 14:12 Received: 08/04/22 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 08/05/22 05:59 67-64-125.0 1
Benzene ND ug/L 08/05/22 05:59 71-43-21.0 1
Bromobenzene ND ug/L 08/05/22 05:59 108-86-11.0 1
Bromochloromethane ND ug/L 08/05/22 05:59 74-97-51.0 1
Bromodichloromethane ND ug/L 08/05/22 05:59 75-27-41.0 1
Bromoform ND ug/L 08/05/22 05:59 75-25-21.0 1
Bromomethane ND ug/L 08/05/22 05:59 74-83-9 v22.0 1
2-Butanone (MEK)ND ug/L 08/05/22 05:59 78-93-35.0 1
n-Butylbenzene ND ug/L 08/05/22 05:59 104-51-81.0 1
sec-Butylbenzene ND ug/L 08/05/22 05:59 135-98-81.0 1
Carbon tetrachloride ND ug/L 08/05/22 05:59 56-23-51.0 1
Chlorobenzene ND ug/L 08/05/22 05:59 108-90-71.0 1
Chloroethane ND ug/L 08/05/22 05:59 75-00-31.0 1
Chloroform ND ug/L 08/05/22 05:59 67-66-31.0 1
Chloromethane ND ug/L 08/05/22 05:59 74-87-31.0 1
2-Chlorotoluene ND ug/L 08/05/22 05:59 95-49-81.0 1
4-Chlorotoluene ND ug/L 08/05/22 05:59 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 08/05/22 05:59 96-12-82.0 1
Dibromochloromethane ND ug/L 08/05/22 05:59 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 08/05/22 05:59 106-93-41.0 1
Dibromomethane ND ug/L 08/05/22 05:59 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 08/05/22 05:59 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 08/05/22 05:59 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 08/05/22 05:59 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 08/05/22 05:59 75-71-81.0 1
1,1-Dichloroethane ND ug/L 08/05/22 05:59 75-34-31.0 1
1,2-Dichloroethane ND ug/L 08/05/22 05:59 107-06-21.0 1
1,1-Dichloroethene ND ug/L 08/05/22 05:59 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 08/05/22 05:59 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 08/05/22 05:59 156-60-51.0 1
1,2-Dichloropropane ND ug/L 08/05/22 05:59 78-87-51.0 1
1,3-Dichloropropane ND ug/L 08/05/22 05:59 142-28-91.0 1
2,2-Dichloropropane ND ug/L 08/05/22 05:59 594-20-71.0 1
1,1-Dichloropropene ND ug/L 08/05/22 05:59 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 08/05/22 05:59 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 08/05/22 05:59 10061-02-61.0 1
Diisopropyl ether ND ug/L 08/05/22 05:59 108-20-31.0 1
Ethylbenzene ND ug/L 08/05/22 05:59 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 08/05/22 05:59 87-68-32.0 1
2-Hexanone ND ug/L 08/05/22 05:59 591-78-65.0 1
Isopropylbenzene (Cumene)ND ug/L 08/05/22 05:59 98-82-81.0 1
p-Isopropyltoluene ND ug/L 08/05/22 05:59 99-87-61.0 1
Methylene Chloride ND ug/L 08/05/22 05:59 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/05/22 05:59 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 08/05/22 05:59 1634-04-41.0 1
Naphthalene ND ug/L 08/05/22 05:59 91-20-31.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/09/2022 09:52 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92618510
LOADING RACK SITE WIILMINGTON
Sample: KMW-1 Lab ID: 92618510005 Collected: 08/03/22 14:12 Received: 08/04/22 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
n-Propylbenzene ND ug/L 08/05/22 05:59 103-65-11.0 1
Styrene ND ug/L 08/05/22 05:59 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 08/05/22 05:59 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 08/05/22 05:59 79-34-51.0 1
Tetrachloroethene ND ug/L 08/05/22 05:59 127-18-41.0 1
Toluene ND ug/L 08/05/22 05:59 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 08/05/22 05:59 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 08/05/22 05:59 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 08/05/22 05:59 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 08/05/22 05:59 79-00-51.0 1
Trichloroethene ND ug/L 08/05/22 05:59 79-01-61.0 1
Trichlorofluoromethane ND ug/L 08/05/22 05:59 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 08/05/22 05:59 96-18-41.0 1
1,2,4-Trimethylbenzene ND ug/L 08/05/22 05:59 95-63-61.0 1
1,3,5-Trimethylbenzene ND ug/L 08/05/22 05:59 108-67-81.0 1
Vinyl acetate ND ug/L 08/05/22 05:59 108-05-42.0 1
Vinyl chloride ND ug/L 08/05/22 05:59 75-01-41.0 1
Xylene (Total)ND ug/L 08/05/22 05:59 1330-20-71.0 1
m&p-Xylene ND ug/L 08/05/22 05:59 179601-23-12.0 1
o-Xylene ND ug/L 08/05/22 05:59 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)96 %08/05/22 05:59 460-00-470-130 1
1,2-Dichloroethane-d4 (S)103 %08/05/22 05:59 17060-07-070-130 1
Toluene-d8 (S)100 %08/05/22 05:59 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/09/2022 09:52 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92618510
LOADING RACK SITE WIILMINGTON
Sample: KMW-3 Lab ID: 92618510006 Collected: 08/03/22 13:45 Received: 08/04/22 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 08/05/22 06:17 67-64-125.0 1
Benzene 20.3 ug/L 08/05/22 06:17 71-43-21.0 1
Bromobenzene ND ug/L 08/05/22 06:17 108-86-11.0 1
Bromochloromethane ND ug/L 08/05/22 06:17 74-97-51.0 1
Bromodichloromethane ND ug/L 08/05/22 06:17 75-27-41.0 1
Bromoform ND ug/L 08/05/22 06:17 75-25-21.0 1
Bromomethane ND ug/L 08/05/22 06:17 74-83-9 v22.0 1
2-Butanone (MEK)ND ug/L 08/05/22 06:17 78-93-35.0 1
n-Butylbenzene ND ug/L 08/05/22 06:17 104-51-81.0 1
sec-Butylbenzene 3.8 ug/L 08/05/22 06:17 135-98-81.0 1
Carbon tetrachloride ND ug/L 08/05/22 06:17 56-23-51.0 1
Chlorobenzene ND ug/L 08/05/22 06:17 108-90-71.0 1
Chloroethane ND ug/L 08/05/22 06:17 75-00-31.0 1
Chloroform ND ug/L 08/05/22 06:17 67-66-31.0 1
Chloromethane ND ug/L 08/05/22 06:17 74-87-31.0 1
2-Chlorotoluene ND ug/L 08/05/22 06:17 95-49-81.0 1
4-Chlorotoluene ND ug/L 08/05/22 06:17 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 08/05/22 06:17 96-12-82.0 1
Dibromochloromethane ND ug/L 08/05/22 06:17 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 08/05/22 06:17 106-93-41.0 1
Dibromomethane ND ug/L 08/05/22 06:17 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 08/05/22 06:17 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 08/05/22 06:17 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 08/05/22 06:17 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 08/05/22 06:17 75-71-81.0 1
1,1-Dichloroethane ND ug/L 08/05/22 06:17 75-34-31.0 1
1,2-Dichloroethane ND ug/L 08/05/22 06:17 107-06-21.0 1
1,1-Dichloroethene ND ug/L 08/05/22 06:17 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 08/05/22 06:17 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 08/05/22 06:17 156-60-51.0 1
1,2-Dichloropropane ND ug/L 08/05/22 06:17 78-87-51.0 1
1,3-Dichloropropane ND ug/L 08/05/22 06:17 142-28-91.0 1
2,2-Dichloropropane ND ug/L 08/05/22 06:17 594-20-71.0 1
1,1-Dichloropropene ND ug/L 08/05/22 06:17 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 08/05/22 06:17 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 08/05/22 06:17 10061-02-61.0 1
Diisopropyl ether ND ug/L 08/05/22 06:17 108-20-31.0 1
Ethylbenzene ND ug/L 08/05/22 06:17 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 08/05/22 06:17 87-68-32.0 1
2-Hexanone ND ug/L 08/05/22 06:17 591-78-65.0 1
Isopropylbenzene (Cumene)39.5 ug/L 08/05/22 06:17 98-82-81.0 1
p-Isopropyltoluene ND ug/L 08/05/22 06:17 99-87-61.0 1
Methylene Chloride ND ug/L 08/05/22 06:17 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/05/22 06:17 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 08/05/22 06:17 1634-04-41.0 1
Naphthalene ND ug/L 08/05/22 06:17 91-20-31.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/09/2022 09:52 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92618510
LOADING RACK SITE WIILMINGTON
Sample: KMW-3 Lab ID: 92618510006 Collected: 08/03/22 13:45 Received: 08/04/22 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
n-Propylbenzene 23.9 ug/L 08/05/22 06:17 103-65-11.0 1
Styrene ND ug/L 08/05/22 06:17 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 08/05/22 06:17 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 08/05/22 06:17 79-34-51.0 1
Tetrachloroethene ND ug/L 08/05/22 06:17 127-18-41.0 1
Toluene 3.6 ug/L 08/05/22 06:17 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 08/05/22 06:17 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 08/05/22 06:17 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 08/05/22 06:17 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 08/05/22 06:17 79-00-51.0 1
Trichloroethene ND ug/L 08/05/22 06:17 79-01-61.0 1
Trichlorofluoromethane ND ug/L 08/05/22 06:17 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 08/05/22 06:17 96-18-41.0 1
1,2,4-Trimethylbenzene ND ug/L 08/05/22 06:17 95-63-61.0 1
1,3,5-Trimethylbenzene ND ug/L 08/05/22 06:17 108-67-81.0 1
Vinyl acetate ND ug/L 08/05/22 06:17 108-05-42.0 1
Vinyl chloride ND ug/L 08/05/22 06:17 75-01-41.0 1
Xylene (Total)3.7 ug/L 08/05/22 06:17 1330-20-71.0 1
m&p-Xylene 3.7 ug/L 08/05/22 06:17 179601-23-12.0 1
o-Xylene ND ug/L 08/05/22 06:17 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)98 %08/05/22 06:17 460-00-470-130 1
1,2-Dichloroethane-d4 (S)104 %08/05/22 06:17 17060-07-070-130 1
Toluene-d8 (S)99 %08/05/22 06:17 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/09/2022 09:52 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92618510
LOADING RACK SITE WIILMINGTON
Sample: KMW-18 Lab ID: 92618510007 Collected: 08/03/22 13:15 Received: 08/04/22 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 08/05/22 06:53 67-64-125.0 1
Benzene ND ug/L 08/05/22 06:53 71-43-21.0 1
Bromobenzene ND ug/L 08/05/22 06:53 108-86-11.0 1
Bromochloromethane ND ug/L 08/05/22 06:53 74-97-51.0 1
Bromodichloromethane ND ug/L 08/05/22 06:53 75-27-41.0 1
Bromoform ND ug/L 08/05/22 06:53 75-25-21.0 1
Bromomethane ND ug/L 08/05/22 06:53 74-83-9 v22.0 1
2-Butanone (MEK)ND ug/L 08/05/22 06:53 78-93-35.0 1
n-Butylbenzene ND ug/L 08/05/22 06:53 104-51-81.0 1
sec-Butylbenzene ND ug/L 08/05/22 06:53 135-98-81.0 1
Carbon tetrachloride ND ug/L 08/05/22 06:53 56-23-51.0 1
Chlorobenzene ND ug/L 08/05/22 06:53 108-90-71.0 1
Chloroethane ND ug/L 08/05/22 06:53 75-00-31.0 1
Chloroform ND ug/L 08/05/22 06:53 67-66-31.0 1
Chloromethane ND ug/L 08/05/22 06:53 74-87-31.0 1
2-Chlorotoluene ND ug/L 08/05/22 06:53 95-49-81.0 1
4-Chlorotoluene ND ug/L 08/05/22 06:53 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 08/05/22 06:53 96-12-82.0 1
Dibromochloromethane ND ug/L 08/05/22 06:53 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 08/05/22 06:53 106-93-41.0 1
Dibromomethane ND ug/L 08/05/22 06:53 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 08/05/22 06:53 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 08/05/22 06:53 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 08/05/22 06:53 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 08/05/22 06:53 75-71-81.0 1
1,1-Dichloroethane ND ug/L 08/05/22 06:53 75-34-31.0 1
1,2-Dichloroethane ND ug/L 08/05/22 06:53 107-06-21.0 1
1,1-Dichloroethene ND ug/L 08/05/22 06:53 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 08/05/22 06:53 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 08/05/22 06:53 156-60-51.0 1
1,2-Dichloropropane ND ug/L 08/05/22 06:53 78-87-51.0 1
1,3-Dichloropropane ND ug/L 08/05/22 06:53 142-28-91.0 1
2,2-Dichloropropane ND ug/L 08/05/22 06:53 594-20-71.0 1
1,1-Dichloropropene ND ug/L 08/05/22 06:53 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 08/05/22 06:53 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 08/05/22 06:53 10061-02-61.0 1
Diisopropyl ether ND ug/L 08/05/22 06:53 108-20-31.0 1
Ethylbenzene ND ug/L 08/05/22 06:53 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 08/05/22 06:53 87-68-32.0 1
2-Hexanone ND ug/L 08/05/22 06:53 591-78-65.0 1
Isopropylbenzene (Cumene)ND ug/L 08/05/22 06:53 98-82-81.0 1
p-Isopropyltoluene ND ug/L 08/05/22 06:53 99-87-61.0 1
Methylene Chloride ND ug/L 08/05/22 06:53 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/05/22 06:53 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 08/05/22 06:53 1634-04-41.0 1
Naphthalene ND ug/L 08/05/22 06:53 91-20-31.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/09/2022 09:52 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92618510
LOADING RACK SITE WIILMINGTON
Sample: KMW-18 Lab ID: 92618510007 Collected: 08/03/22 13:15 Received: 08/04/22 08:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
n-Propylbenzene ND ug/L 08/05/22 06:53 103-65-11.0 1
Styrene ND ug/L 08/05/22 06:53 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 08/05/22 06:53 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 08/05/22 06:53 79-34-51.0 1
Tetrachloroethene ND ug/L 08/05/22 06:53 127-18-41.0 1
Toluene ND ug/L 08/05/22 06:53 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 08/05/22 06:53 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 08/05/22 06:53 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 08/05/22 06:53 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 08/05/22 06:53 79-00-51.0 1
Trichloroethene ND ug/L 08/05/22 06:53 79-01-61.0 1
Trichlorofluoromethane ND ug/L 08/05/22 06:53 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 08/05/22 06:53 96-18-41.0 1
1,2,4-Trimethylbenzene ND ug/L 08/05/22 06:53 95-63-61.0 1
1,3,5-Trimethylbenzene ND ug/L 08/05/22 06:53 108-67-81.0 1
Vinyl acetate ND ug/L 08/05/22 06:53 108-05-42.0 1
Vinyl chloride ND ug/L 08/05/22 06:53 75-01-41.0 1
Xylene (Total)ND ug/L 08/05/22 06:53 1330-20-71.0 1
m&p-Xylene ND ug/L 08/05/22 06:53 179601-23-12.0 1
o-Xylene ND ug/L 08/05/22 06:53 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)95 %08/05/22 06:53 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %08/05/22 06:53 17060-07-070-130 1
Toluene-d8 (S)99 %08/05/22 06:53 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/09/2022 09:52 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92618510
LOADING RACK SITE WIILMINGTON
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
715043
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92618510001, 92618510003, 92618510004, 92618510005, 92618510006, 92618510007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3727718
Associated Lab Samples:92618510001, 92618510003, 92618510004, 92618510005, 92618510006, 92618510007
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 08/05/22 05:22
1,1,1-Trichloroethane ug/L ND 1.0 08/05/22 05:22
1,1,2,2-Tetrachloroethane ug/L ND 1.0 08/05/22 05:22
1,1,2-Trichloroethane ug/L ND 1.0 08/05/22 05:22
1,1-Dichloroethane ug/L ND 1.0 08/05/22 05:22
1,1-Dichloroethene ug/L ND 1.0 08/05/22 05:22
1,1-Dichloropropene ug/L ND 1.0 08/05/22 05:22
1,2,3-Trichlorobenzene ug/L ND 1.0 08/05/22 05:22
1,2,3-Trichloropropane ug/L ND 1.0 08/05/22 05:22
1,2,4-Trichlorobenzene ug/L ND 1.0 08/05/22 05:22
1,2,4-Trimethylbenzene ug/L ND 1.0 08/05/22 05:22
1,2-Dibromo-3-chloropropane ug/L ND 2.0 08/05/22 05:22
1,2-Dibromoethane (EDB)ug/L ND 1.0 08/05/22 05:22
1,2-Dichlorobenzene ug/L ND 1.0 08/05/22 05:22
1,2-Dichloroethane ug/L ND 1.0 08/05/22 05:22
1,2-Dichloropropane ug/L ND 1.0 08/05/22 05:22
1,3,5-Trimethylbenzene ug/L ND 1.0 08/05/22 05:22
1,3-Dichlorobenzene ug/L ND 1.0 08/05/22 05:22
1,3-Dichloropropane ug/L ND 1.0 08/05/22 05:22
1,4-Dichlorobenzene ug/L ND 1.0 08/05/22 05:22
2,2-Dichloropropane ug/L ND 1.0 08/05/22 05:22
2-Butanone (MEK)ug/L ND 5.0 08/05/22 05:22
2-Chlorotoluene ug/L ND 1.0 08/05/22 05:22
2-Hexanone ug/L ND 5.0 08/05/22 05:22
4-Chlorotoluene ug/L ND 1.0 08/05/22 05:22
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 08/05/22 05:22
Acetone ug/L ND 25.0 08/05/22 05:22
Benzene ug/L ND 1.0 08/05/22 05:22
Bromobenzene ug/L ND 1.0 08/05/22 05:22
Bromochloromethane ug/L ND 1.0 08/05/22 05:22
Bromodichloromethane ug/L ND 1.0 08/05/22 05:22
Bromoform ug/L ND 1.0 08/05/22 05:22
Bromomethane ug/L ND 2.0 v208/05/22 05:22
Carbon tetrachloride ug/L ND 1.0 08/05/22 05:22
Chlorobenzene ug/L ND 1.0 08/05/22 05:22
Chloroethane ug/L ND 1.0 08/05/22 05:22
Chloroform ug/L ND 1.0 08/05/22 05:22
Chloromethane ug/L ND 1.0 08/05/22 05:22
cis-1,2-Dichloroethene ug/L ND 1.0 08/05/22 05:22
cis-1,3-Dichloropropene ug/L ND 1.0 08/05/22 05:22
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/09/2022 09:52 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92618510
LOADING RACK SITE WIILMINGTON
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3727718
Associated Lab Samples:92618510001, 92618510003, 92618510004, 92618510005, 92618510006, 92618510007
Matrix: Water
Analyzed
Dibromochloromethane ug/L ND 1.0 08/05/22 05:22
Dibromomethane ug/L ND 1.0 08/05/22 05:22
Dichlorodifluoromethane ug/L ND 1.0 08/05/22 05:22
Diisopropyl ether ug/L ND 1.0 08/05/22 05:22
Ethylbenzene ug/L ND 1.0 08/05/22 05:22
Hexachloro-1,3-butadiene ug/L ND 2.0 08/05/22 05:22
Isopropylbenzene (Cumene)ug/L ND 1.0 08/05/22 05:22
m&p-Xylene ug/L ND 2.0 08/05/22 05:22
Methyl-tert-butyl ether ug/L ND 1.0 08/05/22 05:22
Methylene Chloride ug/L ND 5.0 08/05/22 05:22
n-Butylbenzene ug/L ND 1.0 08/05/22 05:22
n-Propylbenzene ug/L ND 1.0 08/05/22 05:22
Naphthalene ug/L ND 1.0 08/05/22 05:22
o-Xylene ug/L ND 1.0 08/05/22 05:22
p-Isopropyltoluene ug/L ND 1.0 08/05/22 05:22
sec-Butylbenzene ug/L ND 1.0 08/05/22 05:22
Styrene ug/L ND 1.0 08/05/22 05:22
Tetrachloroethene ug/L ND 1.0 08/05/22 05:22
Toluene ug/L ND 1.0 08/05/22 05:22
trans-1,2-Dichloroethene ug/L ND 1.0 08/05/22 05:22
trans-1,3-Dichloropropene ug/L ND 1.0 08/05/22 05:22
Trichloroethene ug/L ND 1.0 08/05/22 05:22
Trichlorofluoromethane ug/L ND 1.0 08/05/22 05:22
Vinyl acetate ug/L ND 2.0 08/05/22 05:22
Vinyl chloride ug/L ND 1.0 08/05/22 05:22
Xylene (Total)ug/L ND 1.0 08/05/22 05:22
1,2-Dichloroethane-d4 (S)%102 70-130 08/05/22 05:22
4-Bromofluorobenzene (S)%95 70-130 08/05/22 05:22
Toluene-d8 (S)%99 70-130 08/05/22 05:22
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3727719LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.850 102 70-130
1,1,1-Trichloroethane ug/L 47.850 96 70-130
1,1,2,2-Tetrachloroethane ug/L 49.150 98 70-130
1,1,2-Trichloroethane ug/L 47.450 95 70-130
1,1-Dichloroethane ug/L 45.850 92 70-130
1,1-Dichloroethene ug/L 48.850 98 70-132
1,1-Dichloropropene ug/L 47.550 95 70-131
1,2,3-Trichlorobenzene ug/L 47.450 95 70-134
1,2,3-Trichloropropane ug/L 51.350 103 70-130
1,2,4-Trichlorobenzene ug/L 48.050 96 70-130
1,2,4-Trimethylbenzene ug/L 47.050 94 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/09/2022 09:52 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92618510
LOADING RACK SITE WIILMINGTON
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3727719LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/L 49.250 98 70-132
1,2-Dibromoethane (EDB)ug/L 49.350 99 70-130
1,2-Dichlorobenzene ug/L 48.750 97 70-130
1,2-Dichloroethane ug/L 46.850 94 70-130
1,2-Dichloropropane ug/L 49.250 98 70-130
1,3,5-Trimethylbenzene ug/L 48.850 98 70-130
1,3-Dichlorobenzene ug/L 47.950 96 70-130
1,3-Dichloropropane ug/L 48.450 97 70-130
1,4-Dichlorobenzene ug/L 48.150 96 70-130
2,2-Dichloropropane ug/L 45.550 91 70-130
2-Butanone (MEK)ug/L 96.0100 96 70-133
2-Chlorotoluene ug/L 48.150 96 70-130
2-Hexanone ug/L 123100 123 70-130
4-Chlorotoluene ug/L 48.150 96 70-130
4-Methyl-2-pentanone (MIBK)ug/L 109100 109 70-130
Acetone ug/L 104100 104 70-144
Benzene ug/L 40.350 81 70-130
Bromobenzene ug/L 49.050 98 70-130
Bromochloromethane ug/L 46.150 92 70-130
Bromodichloromethane ug/L 48.450 97 70-130
Bromoform ug/L 53.350 107 70-131
Bromomethane ug/L 37.6 v35075 30-177
Carbon tetrachloride ug/L 47.850 96 70-130
Chlorobenzene ug/L 47.650 95 70-130
Chloroethane ug/L 43.850 88 46-131
Chloroform ug/L 47.650 95 70-130
Chloromethane ug/L 43.650 87 49-130
cis-1,2-Dichloroethene ug/L 46.350 93 70-130
cis-1,3-Dichloropropene ug/L 49.450 99 70-130
Dibromochloromethane ug/L 51.450 103 70-130
Dibromomethane ug/L 45.950 92 70-130
Dichlorodifluoromethane ug/L 41.850 84 52-134
Diisopropyl ether ug/L 50.050 100 70-131
Ethylbenzene ug/L 47.650 95 70-130
Hexachloro-1,3-butadiene ug/L 47.750 95 70-131
Isopropylbenzene (Cumene)ug/L 48.650 97 70-130
m&p-Xylene ug/L 96.1100 96 70-130
Methyl-tert-butyl ether ug/L 48.150 96 70-130
Methylene Chloride ug/L 48.550 97 68-130
n-Butylbenzene ug/L 49.450 99 70-130
n-Propylbenzene ug/L 47.750 95 70-130
Naphthalene ug/L 49.050 98 70-133
o-Xylene ug/L 48.450 97 70-130
p-Isopropyltoluene ug/L 49.450 99 70-130
sec-Butylbenzene ug/L 48.050 96 70-130
Styrene ug/L 49.050 98 70-130
Tetrachloroethene ug/L 45.650 91 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/09/2022 09:52 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92618510
LOADING RACK SITE WIILMINGTON
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3727719LABORATORY CONTROL SAMPLE:
LCSSpike
Toluene ug/L 42.950 86 70-130
trans-1,2-Dichloroethene ug/L 47.350 95 70-130
trans-1,3-Dichloropropene ug/L 51.050 102 70-130
Trichloroethene ug/L 46.050 92 70-130
Trichlorofluoromethane ug/L 45.450 91 61-130
Vinyl acetate ug/L 104100 104 70-140
Vinyl chloride ug/L 47.550 95 59-142
Xylene (Total)ug/L 144150 96 70-130
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3727720MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92617858001
3727721
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 109 70-135113 420ND21.8 22.7
1,1,1-Trichloroethane ug/L 20 108 70-148115 620ND21.7 23.0
1,1,2,2-Tetrachloroethane ug/L 20 104 70-131108 420ND20.8 21.6
1,1,2-Trichloroethane ug/L 20 103 70-136109 520ND20.6 21.7
1,1-Dichloroethane ug/L 20 104 70-147111 720ND20.8 22.2
1,1-Dichloroethene ug/L 20 118 70-158123 420ND23.5 24.6
1,1-Dichloropropene ug/L 20 109 70-149116 720ND21.8 23.3
1,2,3-Trichlorobenzene ug/L 20 97 68-140104 720ND19.4 20.8
1,2,3-Trichloropropane ug/L 20 107 67-137113 520ND21.5 22.5
1,2,4-Trichlorobenzene ug/L 20 101 70-139107 620ND20.1 21.4
1,2,4-Trimethylbenzene ug/L 20 104 70-134110 620ND20.8 22.0
1,2-Dibromo-3-chloropropane ug/L 20 109 69-136113 420ND21.8 22.5
1,2-Dibromoethane (EDB)ug/L 20 103 70-137106 320ND20.6 21.3
1,2-Dichlorobenzene ug/L 20 107 70-133112 420ND21.4 22.3
1,2-Dichloroethane ug/L 20 103 67-138108 520ND20.6 21.6
1,2-Dichloropropane ug/L 20 106 70-138112 620ND21.1 22.4
1,3,5-Trimethylbenzene ug/L 20 109 70-138113 420ND21.7 22.6
1,3-Dichlorobenzene ug/L 20 107 70-133113 620ND21.3 22.5
1,3-Dichloropropane ug/L 20 103 70-136108 520ND20.6 21.6
1,4-Dichlorobenzene ug/L 20 105 70-133109 320ND21.1 21.7
2,2-Dichloropropane ug/L 20 115 52-155120 520ND22.9 24.1
2-Butanone (MEK)ug/L 40 111 61-147116 440ND46.6 48.6
2-Chlorotoluene ug/L 20 106 70-141113 620ND21.2 22.6
2-Hexanone ug/L v14013267-139139 540ND52.9 55.6
4-Chlorotoluene ug/L 20 106 70-135111 520ND21.2 22.2
4-Methyl-2-pentanone (MIBK) ug/L 40 116 67-136123 540ND46.5 49.1
Acetone ug/L 40 123 55-159130 640ND49.0 51.8
Benzene ug/L 20 93 67-15096 420ND18.5 19.3
Bromobenzene ug/L 20 108 70-134113 520ND21.6 22.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/09/2022 09:52 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92618510
LOADING RACK SITE WIILMINGTON
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3727720MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92617858001
3727721
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Bromochloromethane ug/L 20 102 70-146106 320ND20.4 21.1
Bromodichloromethane ug/L 20 106 70-138113 720ND21.1 22.7
Bromoform ug/L 20 109 57-138111 220ND21.7 22.2
Bromomethane ug/L v3209110-20097 620ND18.2 19.4
Carbon tetrachloride ug/L 20 110 70-147119 820ND22.1 23.9
Chlorobenzene ug/L 20 104 70-137110 620ND20.8 22.0
Chloroethane ug/L 20 115 51-166120 520ND23.0 24.1
Chloroform ug/L 20 104 70-144106 220ND20.8 21.2
Chloromethane ug/L 20 105 24-161110 520ND20.9 22.0
cis-1,2-Dichloroethene ug/L 20 105 67-148111 520ND21.1 22.1
cis-1,3-Dichloropropene ug/L 20 103 70-142110 620ND20.7 22.1
Dibromochloromethane ug/L 20 107 68-138110 220ND21.5 21.9
Dibromomethane ug/L 20 101 70-134111 1020ND20.1 22.2
Dichlorodifluoromethane ug/L 20 105 43-155111 620ND20.9 22.2
Diisopropyl ether ug/L 20 112 65-146119 620ND22.5 23.8
Ethylbenzene ug/L 20 105 68-143109 420ND20.9 21.8
Hexachloro-1,3-butadiene ug/L 20 103 62-151109 620ND20.5 21.9
Isopropylbenzene (Cumene) ug/L 20 105 70-136109 420ND20.9 21.7
m&p-Xylene ug/L 40 105 53-157110 540ND42.1 44.1
Methyl-tert-butyl ether ug/L 20 108 59-156113 520ND21.5 22.6
Methylene Chloride ug/L 20 95 64-148102 720ND19.1 20.4
n-Butylbenzene ug/L 20 109 70-139116 620ND21.8 23.2
n-Propylbenzene ug/L 20 107 70-138113 520ND21.4 22.5
Naphthalene ug/L 20 100 57-150107 720ND20.0 21.4
o-Xylene ug/L 20 105 68-143107 220ND20.9 21.4
p-Isopropyltoluene ug/L 20 109 70-141116 620ND21.8 23.1
sec-Butylbenzene ug/L 20 107 70-137115 720ND21.4 22.9
Styrene ug/L 20 106 70-136109 320ND21.1 21.7
Tetrachloroethene ug/L 20 103 70-139107 420ND20.6 21.4
Toluene ug/L 20 96 47-157101 520ND19.2 20.1
trans-1,2-Dichloroethene ug/L 20 108 70-149116 720ND21.5 23.1
trans-1,3-Dichloropropene ug/L 20 109 70-138114 520ND21.7 22.7
Trichloroethene ug/L 20 106 70-149110 320ND21.3 22.0
Trichlorofluoromethane ug/L 20 109 61-154115 520ND21.8 23.0
Vinyl acetate ug/L 40 110 48-156116 540ND44.1 46.2
Vinyl chloride ug/L 20 115 55-172119 420ND23.0 23.8
Xylene (Total)ug/L 60 105 66-145109 460ND63.0 65.5
1,2-Dichloroethane-d4 (S)%101 70-13099
4-Bromofluorobenzene (S)%99 70-13098
Toluene-d8 (S)%99 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/09/2022 09:52 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92618510
LOADING RACK SITE WIILMINGTON
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
715434
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92618510002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3730118
Associated Lab Samples:92618510002
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 08/05/22 20:23
1,1,1-Trichloroethane ug/L ND 1.0 08/05/22 20:23
1,1,2,2-Tetrachloroethane ug/L ND 1.0 08/05/22 20:23
1,1,2-Trichloroethane ug/L ND 1.0 08/05/22 20:23
1,1-Dichloroethane ug/L ND 1.0 08/05/22 20:23
1,1-Dichloroethene ug/L ND 1.0 08/05/22 20:23
1,1-Dichloropropene ug/L ND 1.0 08/05/22 20:23
1,2,3-Trichlorobenzene ug/L ND 1.0 08/05/22 20:23
1,2,3-Trichloropropane ug/L ND 1.0 08/05/22 20:23
1,2,4-Trichlorobenzene ug/L ND 1.0 08/05/22 20:23
1,2,4-Trimethylbenzene ug/L ND 1.0 08/05/22 20:23
1,2-Dibromo-3-chloropropane ug/L ND 2.0 08/05/22 20:23
1,2-Dibromoethane (EDB)ug/L ND 1.0 08/05/22 20:23
1,2-Dichlorobenzene ug/L ND 1.0 08/05/22 20:23
1,2-Dichloroethane ug/L ND 1.0 08/05/22 20:23
1,2-Dichloropropane ug/L ND 1.0 08/05/22 20:23
1,3,5-Trimethylbenzene ug/L ND 1.0 08/05/22 20:23
1,3-Dichlorobenzene ug/L ND 1.0 08/05/22 20:23
1,3-Dichloropropane ug/L ND 1.0 08/05/22 20:23
1,4-Dichlorobenzene ug/L ND 1.0 08/05/22 20:23
2,2-Dichloropropane ug/L ND 1.0 08/05/22 20:23
2-Butanone (MEK)ug/L ND 5.0 08/05/22 20:23
2-Chlorotoluene ug/L ND 1.0 08/05/22 20:23
2-Hexanone ug/L ND 5.0 08/05/22 20:23
4-Chlorotoluene ug/L ND 1.0 08/05/22 20:23
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 08/05/22 20:23
Acetone ug/L ND 25.0 08/05/22 20:23
Benzene ug/L ND 1.0 08/05/22 20:23
Bromobenzene ug/L ND 1.0 08/05/22 20:23
Bromochloromethane ug/L ND 1.0 08/05/22 20:23
Bromodichloromethane ug/L ND 1.0 08/05/22 20:23
Bromoform ug/L ND 1.0 08/05/22 20:23
Bromomethane ug/L ND 2.0 IH,IK,v108/05/22 20:23
Carbon tetrachloride ug/L ND 1.0 08/05/22 20:23
Chlorobenzene ug/L ND 1.0 08/05/22 20:23
Chloroethane ug/L ND 1.0 08/05/22 20:23
Chloroform ug/L ND 1.0 08/05/22 20:23
Chloromethane ug/L ND 1.0 08/05/22 20:23
cis-1,2-Dichloroethene ug/L ND 1.0 08/05/22 20:23
cis-1,3-Dichloropropene ug/L ND 1.0 08/05/22 20:23
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/09/2022 09:52 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92618510
LOADING RACK SITE WIILMINGTON
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3730118
Associated Lab Samples:92618510002
Matrix: Water
Analyzed
Dibromochloromethane ug/L ND 1.0 08/05/22 20:23
Dibromomethane ug/L ND 1.0 08/05/22 20:23
Dichlorodifluoromethane ug/L ND 1.0 08/05/22 20:23
Diisopropyl ether ug/L ND 1.0 08/05/22 20:23
Ethylbenzene ug/L ND 1.0 08/05/22 20:23
Hexachloro-1,3-butadiene ug/L ND 2.0 08/05/22 20:23
Isopropylbenzene (Cumene)ug/L ND 1.0 08/05/22 20:23
m&p-Xylene ug/L ND 2.0 08/05/22 20:23
Methyl-tert-butyl ether ug/L ND 1.0 08/05/22 20:23
Methylene Chloride ug/L ND 5.0 08/05/22 20:23
n-Butylbenzene ug/L ND 1.0 08/05/22 20:23
n-Propylbenzene ug/L ND 1.0 08/05/22 20:23
Naphthalene ug/L ND 1.0 08/05/22 20:23
o-Xylene ug/L ND 1.0 08/05/22 20:23
p-Isopropyltoluene ug/L ND 1.0 08/05/22 20:23
sec-Butylbenzene ug/L ND 1.0 08/05/22 20:23
Styrene ug/L ND 1.0 08/05/22 20:23
Tetrachloroethene ug/L ND 1.0 08/05/22 20:23
Toluene ug/L ND 1.0 08/05/22 20:23
trans-1,2-Dichloroethene ug/L ND 1.0 08/05/22 20:23
trans-1,3-Dichloropropene ug/L ND 1.0 08/05/22 20:23
Trichloroethene ug/L ND 1.0 08/05/22 20:23
Trichlorofluoromethane ug/L ND 1.0 08/05/22 20:23
Vinyl acetate ug/L ND 2.0 08/05/22 20:23
Vinyl chloride ug/L ND 1.0 08/05/22 20:23
Xylene (Total)ug/L ND 1.0 08/05/22 20:23
1,2-Dichloroethane-d4 (S)%98 70-130 08/05/22 20:23
4-Bromofluorobenzene (S)%101 70-130 08/05/22 20:23
Toluene-d8 (S)%99 70-130 08/05/22 20:23
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3730119LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 52.150 104 70-130
1,1,1-Trichloroethane ug/L 49.250 98 70-130
1,1,2,2-Tetrachloroethane ug/L 51.250 102 70-130
1,1,2-Trichloroethane ug/L 50.350 101 70-130
1,1-Dichloroethane ug/L 49.250 98 70-130
1,1-Dichloroethene ug/L 49.850 100 70-132
1,1-Dichloropropene ug/L 52.950 106 70-131
1,2,3-Trichlorobenzene ug/L 52.050 104 70-134
1,2,3-Trichloropropane ug/L 50.650 101 70-130
1,2,4-Trichlorobenzene ug/L 51.250 102 70-130
1,2,4-Trimethylbenzene ug/L 49.950 100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/09/2022 09:52 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92618510
LOADING RACK SITE WIILMINGTON
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3730119LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/L 50.850 102 70-132
1,2-Dibromoethane (EDB)ug/L 51.250 102 70-130
1,2-Dichlorobenzene ug/L 52.650 105 70-130
1,2-Dichloroethane ug/L 50.050 100 70-130
1,2-Dichloropropane ug/L 51.750 103 70-130
1,3,5-Trimethylbenzene ug/L 51.350 103 70-130
1,3-Dichlorobenzene ug/L 52.250 104 70-130
1,3-Dichloropropane ug/L 49.650 99 70-130
1,4-Dichlorobenzene ug/L 51.550 103 70-130
2,2-Dichloropropane ug/L 47.150 94 70-130
2-Butanone (MEK)ug/L 97.4100 97 70-133
2-Chlorotoluene ug/L 51.850 104 70-130
2-Hexanone ug/L 106100 106 70-130
4-Chlorotoluene ug/L 51.050 102 70-130
4-Methyl-2-pentanone (MIBK)ug/L 108100 108 70-130
Acetone ug/L 96.2100 96 70-144
Benzene ug/L 48.550 97 70-130
Bromobenzene ug/L 50.550 101 70-130
Bromochloromethane ug/L 45.950 92 70-130
Bromodichloromethane ug/L 52.350 105 70-130
Bromoform ug/L 50.450 101 70-131
Bromomethane ug/L 60.9 IH,IK,v150122 30-177
Carbon tetrachloride ug/L 51.850 104 70-130
Chlorobenzene ug/L 51.550 103 70-130
Chloroethane ug/L 42.050 84 46-131
Chloroform ug/L 47.950 96 70-130
Chloromethane ug/L 45.550 91 49-130
cis-1,2-Dichloroethene ug/L 51.550 103 70-130
cis-1,3-Dichloropropene ug/L 51.450 103 70-130
Dibromochloromethane ug/L 50.550 101 70-130
Dibromomethane ug/L 50.350 101 70-130
Dichlorodifluoromethane ug/L 45.650 91 52-134
Diisopropyl ether ug/L 52.650 105 70-131
Ethylbenzene ug/L 51.450 103 70-130
Hexachloro-1,3-butadiene ug/L 47.750 95 70-131
Isopropylbenzene (Cumene)ug/L 50.750 101 70-130
m&p-Xylene ug/L 104100 104 70-130
Methyl-tert-butyl ether ug/L 50.050 100 70-130
Methylene Chloride ug/L 40.950 82 68-130
n-Butylbenzene ug/L 50.950 102 70-130
n-Propylbenzene ug/L 50.550 101 70-130
Naphthalene ug/L 54.450 109 70-133
o-Xylene ug/L 50.950 102 70-130
p-Isopropyltoluene ug/L 52.450 105 70-130
sec-Butylbenzene ug/L 50.350 101 70-130
Styrene ug/L 53.050 106 70-130
Tetrachloroethene ug/L 47.850 96 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/09/2022 09:52 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92618510
LOADING RACK SITE WIILMINGTON
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3730119LABORATORY CONTROL SAMPLE:
LCSSpike
Toluene ug/L 49.950 100 70-130
trans-1,2-Dichloroethene ug/L 51.350 103 70-130
trans-1,3-Dichloropropene ug/L 51.750 103 70-130
Trichloroethene ug/L 50.950 102 70-130
Trichlorofluoromethane ug/L 42.750 85 61-130
Vinyl acetate ug/L 108100 108 70-140
Vinyl chloride ug/L 50.750 101 59-142
Xylene (Total)ug/L 155150 103 70-130
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3730120MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92618506004
3730121
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 2500 107 70-135114 62500ND2680 2860
1,1,1-Trichloroethane ug/L 2500 107 70-148113 62500ND2670 2830
1,1,2,2-Tetrachloroethane ug/L 2500 100 70-131104 42500ND2510 2600
1,1,2-Trichloroethane ug/L 2500 102 70-136110 82500ND2550 2750
1,1-Dichloroethane ug/L 2500 107 70-147112 52500ND2670 2800
1,1-Dichloroethene ug/L 2500 106 70-158116 92500ND2640 2900
1,1-Dichloropropene ug/L 2500 114 70-149122 82500ND2840 3060
1,2,3-Trichlorobenzene ug/L 2500 96 68-140105 82500ND2410 2620
1,2,3-Trichloropropane ug/L 2500 98 67-137103 52500ND2450 2570
1,2,4-Trichlorobenzene ug/L 2500 96 70-139102 62500ND2390 2550
1,2,4-Trimethylbenzene ug/L 2500 101 70-134106 52500ND2510 2640
1,2-Dibromo-3-chloropropane ug/L 2500 90 69-13697 82500ND2250 2440
1,2-Dibromoethane (EDB)ug/L 2500 105 70-137109 32500ND2620 2710
1,2-Dichlorobenzene ug/L 2500 105 70-133111 62500ND2640 2790
1,2-Dichloroethane ug/L 2500 104 67-138112 72500ND2610 2800
1,2-Dichloropropane ug/L 2500 106 70-138114 82500ND2640 2860
1,3,5-Trimethylbenzene ug/L 2500 105 70-138112 62500ND2630 2800
1,3-Dichlorobenzene ug/L 2500 107 70-133114 62500ND2690 2840
1,3-Dichloropropane ug/L 2500 104 70-136108 42500ND2600 2710
1,4-Dichlorobenzene ug/L 2500 107 70-133111 32500ND2680 2770
2,2-Dichloropropane ug/L 2500 100 52-155106 62500ND2490 2650
2-Butanone (MEK)ug/L 5000 93 61-14798 55000ND4630 4880
2-Chlorotoluene ug/L 2500 106 70-141112 52500ND2660 2800
2-Hexanone ug/L 5000 100 67-139105 55000ND4990 5260
4-Chlorotoluene ug/L 2500 106 70-135109 32500ND2660 2730
4-Methyl-2-pentanone (MIBK) ug/L 5000 102 67-136106 45000ND5090 5310
Acetone ug/L 5000 99 55-159110 105000ND4970 5520
Benzene ug/L 2500 104 67-150110 52500ND2610 2750
Bromobenzene ug/L 2500 104 70-134112 72500ND2600 2790
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/09/2022 09:52 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92618510
LOADING RACK SITE WIILMINGTON
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3730120MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92618506004
3730121
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Bromochloromethane ug/L 2500 105 70-146112 72500ND2630 2810
Bromodichloromethane ug/L 2500 103 70-138113 92500ND2570 2810
Bromoform ug/L 2500 96 57-13899 32500ND2400 2470
Bromomethane ug/L IH,IK,v1250011610-200136 162500ND2910 3400
Carbon tetrachloride ug/L 2500 112 70-147119 62500ND2800 2980
Chlorobenzene ug/L 2500 107 70-137113 52500ND2680 2820
Chloroethane ug/L 2500 105 51-166111 62500ND2630 2780
Chloroform ug/L 2500 97 70-144107 102500ND2410 2680
Chloromethane ug/L 2500 97 24-161103 52500ND2430 2560
cis-1,2-Dichloroethene ug/L 2500 110 67-148115 52500ND2740 2880
cis-1,3-Dichloropropene ug/L 2500 103 70-142111 82500ND2580 2790
Dibromochloromethane ug/L 2500 101 68-138107 62500ND2520 2670
Dibromomethane ug/L 2500 103 70-134107 42500ND2580 2680
Dichlorodifluoromethane ug/L 2500 100 43-155102 22500ND2510 2550
Diisopropyl ether ug/L 2500 110 65-146116 52500ND2750 2900
Ethylbenzene ug/L 2500 110 68-143113 32500ND2780 2860
Hexachloro-1,3-butadiene ug/L 2500 101 62-151104 42500ND2510 2610
Isopropylbenzene (Cumene) ug/L 2500 108 70-136111 32500ND2700 2790
m&p-Xylene ug/L 5000 97 53-157106 150003460039400 39900
Methyl-tert-butyl ether ug/L 2500 105 59-156111 62500ND2630 2790
Methylene Chloride ug/L 2500 82 64-14890 92500ND2060 2250
n-Butylbenzene ug/L 2500 103 70-139109 52500ND2590 2720
n-Propylbenzene ug/L 2500 106 70-138112 62500ND2640 2810
Naphthalene ug/L 2500 94 57-150104 102500ND2350 2590
o-Xylene ug/L 2500 109 68-143112 22500ND2730 2800
p-Isopropyltoluene ug/L 2500 109 70-141116 62500ND2720 2890
sec-Butylbenzene ug/L 2500 106 70-137112 52500ND2640 2790
Styrene ug/L 2500 109 70-136115 52500ND2740 2890
Tetrachloroethene ug/L 2500 101 70-139107 52500ND2520 2660
Toluene ug/L 2500 104 47-157111 62500ND2610 2770
trans-1,2-Dichloroethene ug/L 2500 112 70-149118 62500ND2790 2960
trans-1,3-Dichloropropene ug/L 2500 101 70-138106 42500ND2540 2640
Trichloroethene ug/L 2500 108 70-149114 62500ND2690 2860
Trichlorofluoromethane ug/L 2500 97 61-154106 92500ND2430 2660
Vinyl acetate ug/L 5000 107 48-156114 65000ND5370 5680
Vinyl chloride ug/L 2500 108 55-172114 52500ND2700 2850
Xylene (Total)ug/L 7500 101 66-145108 175003460042200 42700
1,2-Dichloroethane-d4 (S)%97 70-13095
4-Bromofluorobenzene (S)%103 70-130103
Toluene-d8 (S)%98 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/09/2022 09:52 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 32
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92618510
LOADING RACK SITE WIILMINGTON
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.IH
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.IK
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/09/2022 09:52 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 32
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92618510
LOADING RACK SITE WIILMINGTON
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92618510001 715043AMW-2 EPA 8260D
92618510002 715434AMW-3 EPA 8260D
92618510003 715043AMW-4 EPA 8260D
92618510004 715043AMW-5 EPA 8260D
92618510005 715043KMW-1 EPA 8260D
92618510006 715043KMW-3 EPA 8260D
92618510007 715043KMW-18 EPA 8260D
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/09/2022 09:52 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 32
Page 30 of 32
Page 31 of 32
Page 32 of 32
#=CL#
August 11, 2022
LIMS USE: FR - MATT MAHONY
LIMS OBJECT ID: 92619080
92619080
Project:
Pace Project No.:
RE:
Matt Mahony
Tetra Tech
805 E 20th St
Charlotte, NC 28205
LOADING RACK ( WILMINGTON)
Dear Matt Mahony:
Enclosed are the analytical results for sample(s) received by the laboratory on August 05, 2022. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Nikita Kuruganty
[e-mail]
Project Manager
[phone]
Enclosures
cc: Michael Christopher
Rod Kremer
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 32
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92619080
LOADING RACK ( WILMINGTON)
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 32
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92619080
LOADING RACK ( WILMINGTON)
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92619080001 KMW-6 EPA 8260D 69 PASI-CCL
92619080002 KMW-7 EPA 8260D 69 PASI-CCL
92619080003 KMW-8 EPA 8260D 69 PASI-CCL
92619080004 KMW-9R EPA 8260D 69 PASI-CCL
92619080005 KMW-13 EPA 8260D 69 PASI-CCL
92619080006 KMW-14 EPA 8260D 69 PASI-CCL
92619080007 TRIP BLANK EPA 8260D 69 PASI-CCL
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92619080
LOADING RACK ( WILMINGTON)
Sample: KMW-6 Lab ID: 92619080001 Collected: 08/04/22 09:10 Received: 08/05/22 11:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 08/09/22 20:57 67-64-1125 5
Benzene ND ug/L 08/09/22 20:57 71-43-25.0 5
Bromobenzene ND ug/L 08/09/22 20:57 108-86-15.0 5
Bromochloromethane ND ug/L 08/09/22 20:57 74-97-55.0 5
Bromodichloromethane ND ug/L 08/09/22 20:57 75-27-45.0 5
Bromoform ND ug/L 08/09/22 20:57 75-25-25.0 5
Bromomethane ND ug/L 08/09/22 20:57 74-83-910.0 5
2-Butanone (MEK)ND ug/L 08/09/22 20:57 78-93-325.0 5
n-Butylbenzene ND ug/L 08/09/22 20:57 104-51-85.0 5
sec-Butylbenzene ND ug/L 08/09/22 20:57 135-98-85.0 5
Carbon tetrachloride ND ug/L 08/09/22 20:57 56-23-55.0 5
Chlorobenzene ND ug/L 08/09/22 20:57 108-90-75.0 5
Chloroethane ND ug/L 08/09/22 20:57 75-00-35.0 5
Chloroform ND ug/L 08/09/22 20:57 67-66-35.0 5
Chloromethane ND ug/L 08/09/22 20:57 74-87-35.0 5
2-Chlorotoluene ND ug/L 08/09/22 20:57 95-49-85.0 5
4-Chlorotoluene ND ug/L 08/09/22 20:57 106-43-45.0 5
1,2-Dibromo-3-chloropropane ND ug/L 08/09/22 20:57 96-12-810.0 5
Dibromochloromethane ND ug/L 08/09/22 20:57 124-48-15.0 5
1,2-Dibromoethane (EDB)ND ug/L 08/09/22 20:57 106-93-45.0 5
Dibromomethane ND ug/L 08/09/22 20:57 74-95-35.0 5
1,2-Dichlorobenzene ND ug/L 08/09/22 20:57 95-50-15.0 5
1,3-Dichlorobenzene ND ug/L 08/09/22 20:57 541-73-15.0 5
1,4-Dichlorobenzene ND ug/L 08/09/22 20:57 106-46-75.0 5
Dichlorodifluoromethane ND ug/L 08/09/22 20:57 75-71-85.0 5
1,1-Dichloroethane ND ug/L 08/09/22 20:57 75-34-35.0 5
1,2-Dichloroethane ND ug/L 08/09/22 20:57 107-06-25.0 5
1,1-Dichloroethene ND ug/L 08/09/22 20:57 75-35-45.0 5
cis-1,2-Dichloroethene ND ug/L 08/09/22 20:57 156-59-25.0 5
trans-1,2-Dichloroethene ND ug/L 08/09/22 20:57 156-60-55.0 5
1,2-Dichloropropane ND ug/L 08/09/22 20:57 78-87-55.0 5
1,3-Dichloropropane ND ug/L 08/09/22 20:57 142-28-95.0 5
2,2-Dichloropropane ND ug/L 08/09/22 20:57 594-20-75.0 5
1,1-Dichloropropene ND ug/L 08/09/22 20:57 563-58-65.0 5
cis-1,3-Dichloropropene ND ug/L 08/09/22 20:57 10061-01-55.0 5
trans-1,3-Dichloropropene ND ug/L 08/09/22 20:57 10061-02-65.0 5
Diisopropyl ether ND ug/L 08/09/22 20:57 108-20-35.0 5
Ethylbenzene 5.3 ug/L 08/09/22 20:57 100-41-45.0 5
Hexachloro-1,3-butadiene ND ug/L 08/09/22 20:57 87-68-310.0 5
2-Hexanone ND ug/L 08/09/22 20:57 591-78-625.0 5
Isopropylbenzene (Cumene)ND ug/L 08/09/22 20:57 98-82-85.0 5
p-Isopropyltoluene ND ug/L 08/09/22 20:57 99-87-65.0 5
Methylene Chloride 26.0 ug/L 08/09/22 20:57 75-09-225.0 5
4-Methyl-2-pentanone (MIBK)ND ug/L 08/09/22 20:57 108-10-125.0 5
Methyl-tert-butyl ether ND ug/L 08/09/22 20:57 1634-04-45.0 5
Naphthalene ND ug/L 08/09/22 20:57 91-20-35.0 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/11/2022 01:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92619080
LOADING RACK ( WILMINGTON)
Sample: KMW-6 Lab ID: 92619080001 Collected: 08/04/22 09:10 Received: 08/05/22 11:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
n-Propylbenzene ND ug/L 08/09/22 20:57 103-65-15.0 5
Styrene ND ug/L 08/09/22 20:57 100-42-55.0 5
1,1,1,2-Tetrachloroethane ND ug/L 08/09/22 20:57 630-20-65.0 5
1,1,2,2-Tetrachloroethane ND ug/L 08/09/22 20:57 79-34-55.0 5
Tetrachloroethene ND ug/L 08/09/22 20:57 127-18-45.0 5
Toluene ND ug/L 08/09/22 20:57 108-88-35.0 5
1,2,3-Trichlorobenzene ND ug/L 08/09/22 20:57 87-61-65.0 5
1,2,4-Trichlorobenzene ND ug/L 08/09/22 20:57 120-82-15.0 5
1,1,1-Trichloroethane ND ug/L 08/09/22 20:57 71-55-65.0 5
1,1,2-Trichloroethane ND ug/L 08/09/22 20:57 79-00-55.0 5
Trichloroethene ND ug/L 08/09/22 20:57 79-01-65.0 5
Trichlorofluoromethane ND ug/L 08/09/22 20:57 75-69-45.0 5
1,2,3-Trichloropropane ND ug/L 08/09/22 20:57 96-18-45.0 5
1,2,4-Trimethylbenzene ND ug/L 08/09/22 20:57 95-63-65.0 5
1,3,5-Trimethylbenzene ND ug/L 08/09/22 20:57 108-67-85.0 5
Vinyl acetate ND ug/L 08/09/22 20:57 108-05-410.0 5
Vinyl chloride ND ug/L 08/09/22 20:57 75-01-45.0 5
Xylene (Total)1420 ug/L 08/09/22 20:57 1330-20-75.0 5
m&p-Xylene 1420 ug/L 08/09/22 20:57 179601-23-110.0 5
o-Xylene ND ug/L 08/09/22 20:57 95-47-65.0 5
Surrogates
4-Bromofluorobenzene (S)100 %08/09/22 20:57 460-00-470-130 5
1,2-Dichloroethane-d4 (S)100 %08/09/22 20:57 17060-07-070-130 5
Toluene-d8 (S)105 %08/09/22 20:57 2037-26-570-130 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/11/2022 01:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92619080
LOADING RACK ( WILMINGTON)
Sample: KMW-7 Lab ID: 92619080002 Collected: 08/04/22 09:55 Received: 08/05/22 11:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 08/09/22 18:00 67-64-125.0 1
Benzene ND ug/L 08/09/22 18:00 71-43-21.0 1
Bromobenzene ND ug/L 08/09/22 18:00 108-86-11.0 1
Bromochloromethane ND ug/L 08/09/22 18:00 74-97-51.0 1
Bromodichloromethane ND ug/L 08/09/22 18:00 75-27-41.0 1
Bromoform ND ug/L 08/09/22 18:00 75-25-21.0 1
Bromomethane ND ug/L 08/09/22 18:00 74-83-92.0 1
2-Butanone (MEK)ND ug/L 08/09/22 18:00 78-93-35.0 1
n-Butylbenzene ND ug/L 08/09/22 18:00 104-51-81.0 1
sec-Butylbenzene ND ug/L 08/09/22 18:00 135-98-81.0 1
Carbon tetrachloride ND ug/L 08/09/22 18:00 56-23-51.0 1
Chlorobenzene ND ug/L 08/09/22 18:00 108-90-71.0 1
Chloroethane ND ug/L 08/09/22 18:00 75-00-31.0 1
Chloroform ND ug/L 08/09/22 18:00 67-66-31.0 1
Chloromethane ND ug/L 08/09/22 18:00 74-87-31.0 1
2-Chlorotoluene ND ug/L 08/09/22 18:00 95-49-81.0 1
4-Chlorotoluene ND ug/L 08/09/22 18:00 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 08/09/22 18:00 96-12-82.0 1
Dibromochloromethane ND ug/L 08/09/22 18:00 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 08/09/22 18:00 106-93-41.0 1
Dibromomethane ND ug/L 08/09/22 18:00 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 08/09/22 18:00 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 08/09/22 18:00 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 08/09/22 18:00 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 08/09/22 18:00 75-71-81.0 1
1,1-Dichloroethane ND ug/L 08/09/22 18:00 75-34-31.0 1
1,2-Dichloroethane ND ug/L 08/09/22 18:00 107-06-21.0 1
1,1-Dichloroethene ND ug/L 08/09/22 18:00 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 08/09/22 18:00 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 08/09/22 18:00 156-60-51.0 1
1,2-Dichloropropane ND ug/L 08/09/22 18:00 78-87-51.0 1
1,3-Dichloropropane ND ug/L 08/09/22 18:00 142-28-91.0 1
2,2-Dichloropropane ND ug/L 08/09/22 18:00 594-20-71.0 1
1,1-Dichloropropene ND ug/L 08/09/22 18:00 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 08/09/22 18:00 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 08/09/22 18:00 10061-02-61.0 1
Diisopropyl ether ND ug/L 08/09/22 18:00 108-20-31.0 1
Ethylbenzene ND ug/L 08/09/22 18:00 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 08/09/22 18:00 87-68-32.0 1
2-Hexanone ND ug/L 08/09/22 18:00 591-78-65.0 1
Isopropylbenzene (Cumene)3.5 ug/L 08/09/22 18:00 98-82-81.0 1
p-Isopropyltoluene ND ug/L 08/09/22 18:00 99-87-61.0 1
Methylene Chloride ND ug/L 08/09/22 18:00 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/09/22 18:00 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 08/09/22 18:00 1634-04-41.0 1
Naphthalene 1.4 ug/L 08/09/22 18:00 91-20-31.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/11/2022 01:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92619080
LOADING RACK ( WILMINGTON)
Sample: KMW-7 Lab ID: 92619080002 Collected: 08/04/22 09:55 Received: 08/05/22 11:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
n-Propylbenzene 4.1 ug/L 08/09/22 18:00 103-65-11.0 1
Styrene ND ug/L 08/09/22 18:00 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 08/09/22 18:00 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 08/09/22 18:00 79-34-51.0 1
Tetrachloroethene ND ug/L 08/09/22 18:00 127-18-41.0 1
Toluene ND ug/L 08/09/22 18:00 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 08/09/22 18:00 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 08/09/22 18:00 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 08/09/22 18:00 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 08/09/22 18:00 79-00-51.0 1
Trichloroethene ND ug/L 08/09/22 18:00 79-01-61.0 1
Trichlorofluoromethane ND ug/L 08/09/22 18:00 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 08/09/22 18:00 96-18-41.0 1
1,2,4-Trimethylbenzene ND ug/L 08/09/22 18:00 95-63-61.0 1
1,3,5-Trimethylbenzene ND ug/L 08/09/22 18:00 108-67-81.0 1
Vinyl acetate ND ug/L 08/09/22 18:00 108-05-42.0 1
Vinyl chloride ND ug/L 08/09/22 18:00 75-01-41.0 1
Xylene (Total)ND ug/L 08/09/22 18:00 1330-20-71.0 1
m&p-Xylene ND ug/L 08/09/22 18:00 179601-23-12.0 1
o-Xylene ND ug/L 08/09/22 18:00 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)100 %08/09/22 18:00 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %08/09/22 18:00 17060-07-070-130 1
Toluene-d8 (S)103 %08/09/22 18:00 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/11/2022 01:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92619080
LOADING RACK ( WILMINGTON)
Sample: KMW-8 Lab ID: 92619080003 Collected: 08/04/22 08:42 Received: 08/05/22 11:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 08/09/22 18:18 67-64-125.0 1
Benzene 12.7 ug/L 08/09/22 18:18 71-43-21.0 1
Bromobenzene ND ug/L 08/09/22 18:18 108-86-11.0 1
Bromochloromethane ND ug/L 08/09/22 18:18 74-97-51.0 1
Bromodichloromethane ND ug/L 08/09/22 18:18 75-27-41.0 1
Bromoform ND ug/L 08/09/22 18:18 75-25-21.0 1
Bromomethane ND ug/L 08/09/22 18:18 74-83-92.0 1
2-Butanone (MEK)ND ug/L 08/09/22 18:18 78-93-35.0 1
n-Butylbenzene ND ug/L 08/09/22 18:18 104-51-81.0 1
sec-Butylbenzene 1.5 ug/L 08/09/22 18:18 135-98-81.0 1
Carbon tetrachloride ND ug/L 08/09/22 18:18 56-23-51.0 1
Chlorobenzene ND ug/L 08/09/22 18:18 108-90-71.0 1
Chloroethane ND ug/L 08/09/22 18:18 75-00-31.0 1
Chloroform ND ug/L 08/09/22 18:18 67-66-31.0 1
Chloromethane ND ug/L 08/09/22 18:18 74-87-31.0 1
2-Chlorotoluene ND ug/L 08/09/22 18:18 95-49-81.0 1
4-Chlorotoluene ND ug/L 08/09/22 18:18 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 08/09/22 18:18 96-12-82.0 1
Dibromochloromethane ND ug/L 08/09/22 18:18 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 08/09/22 18:18 106-93-41.0 1
Dibromomethane ND ug/L 08/09/22 18:18 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 08/09/22 18:18 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 08/09/22 18:18 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 08/09/22 18:18 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 08/09/22 18:18 75-71-81.0 1
1,1-Dichloroethane ND ug/L 08/09/22 18:18 75-34-31.0 1
1,2-Dichloroethane ND ug/L 08/09/22 18:18 107-06-21.0 1
1,1-Dichloroethene ND ug/L 08/09/22 18:18 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 08/09/22 18:18 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 08/09/22 18:18 156-60-51.0 1
1,2-Dichloropropane ND ug/L 08/09/22 18:18 78-87-51.0 1
1,3-Dichloropropane ND ug/L 08/09/22 18:18 142-28-91.0 1
2,2-Dichloropropane ND ug/L 08/09/22 18:18 594-20-71.0 1
1,1-Dichloropropene ND ug/L 08/09/22 18:18 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 08/09/22 18:18 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 08/09/22 18:18 10061-02-61.0 1
Diisopropyl ether ND ug/L 08/09/22 18:18 108-20-31.0 1
Ethylbenzene 3.5 ug/L 08/09/22 18:18 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 08/09/22 18:18 87-68-32.0 1
2-Hexanone ND ug/L 08/09/22 18:18 591-78-65.0 1
Isopropylbenzene (Cumene)9.9 ug/L 08/09/22 18:18 98-82-81.0 1
p-Isopropyltoluene ND ug/L 08/09/22 18:18 99-87-61.0 1
Methylene Chloride ND ug/L 08/09/22 18:18 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/09/22 18:18 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 08/09/22 18:18 1634-04-41.0 1
Naphthalene ND ug/L 08/09/22 18:18 91-20-31.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/11/2022 01:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92619080
LOADING RACK ( WILMINGTON)
Sample: KMW-8 Lab ID: 92619080003 Collected: 08/04/22 08:42 Received: 08/05/22 11:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
n-Propylbenzene 2.7 ug/L 08/09/22 18:18 103-65-11.0 1
Styrene ND ug/L 08/09/22 18:18 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 08/09/22 18:18 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 08/09/22 18:18 79-34-51.0 1
Tetrachloroethene ND ug/L 08/09/22 18:18 127-18-41.0 1
Toluene ND ug/L 08/09/22 18:18 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 08/09/22 18:18 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 08/09/22 18:18 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 08/09/22 18:18 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 08/09/22 18:18 79-00-51.0 1
Trichloroethene ND ug/L 08/09/22 18:18 79-01-61.0 1
Trichlorofluoromethane ND ug/L 08/09/22 18:18 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 08/09/22 18:18 96-18-41.0 1
1,2,4-Trimethylbenzene 1.8 ug/L 08/09/22 18:18 95-63-61.0 1
1,3,5-Trimethylbenzene ND ug/L 08/09/22 18:18 108-67-81.0 1
Vinyl acetate ND ug/L 08/09/22 18:18 108-05-42.0 1
Vinyl chloride ND ug/L 08/09/22 18:18 75-01-41.0 1
Xylene (Total)ND ug/L 08/09/22 18:18 1330-20-71.0 1
m&p-Xylene ND ug/L 08/09/22 18:18 179601-23-12.0 1
o-Xylene ND ug/L 08/09/22 18:18 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)101 %08/09/22 18:18 460-00-470-130 1
1,2-Dichloroethane-d4 (S)103 %08/09/22 18:18 17060-07-070-130 1
Toluene-d8 (S)104 %08/09/22 18:18 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/11/2022 01:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92619080
LOADING RACK ( WILMINGTON)
Sample: KMW-9R Lab ID: 92619080004 Collected: 08/04/22 10:50 Received: 08/05/22 11:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 08/09/22 19:46 67-64-125.0 1
Benzene ND ug/L 08/09/22 19:46 71-43-21.0 1
Bromobenzene ND ug/L 08/09/22 19:46 108-86-11.0 1
Bromochloromethane ND ug/L 08/09/22 19:46 74-97-51.0 1
Bromodichloromethane ND ug/L 08/09/22 19:46 75-27-41.0 1
Bromoform ND ug/L 08/09/22 19:46 75-25-21.0 1
Bromomethane ND ug/L 08/09/22 19:46 74-83-92.0 1
2-Butanone (MEK)ND ug/L 08/09/22 19:46 78-93-35.0 1
n-Butylbenzene 2.3 ug/L 08/09/22 19:46 104-51-81.0 1
sec-Butylbenzene 3.6 ug/L 08/09/22 19:46 135-98-81.0 1
Carbon tetrachloride ND ug/L 08/09/22 19:46 56-23-51.0 1
Chlorobenzene ND ug/L 08/09/22 19:46 108-90-71.0 1
Chloroethane ND ug/L 08/09/22 19:46 75-00-31.0 1
Chloroform ND ug/L 08/09/22 19:46 67-66-31.0 1
Chloromethane ND ug/L 08/09/22 19:46 74-87-31.0 1
2-Chlorotoluene ND ug/L 08/09/22 19:46 95-49-81.0 1
4-Chlorotoluene ND ug/L 08/09/22 19:46 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 08/09/22 19:46 96-12-82.0 1
Dibromochloromethane ND ug/L 08/09/22 19:46 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 08/09/22 19:46 106-93-41.0 1
Dibromomethane ND ug/L 08/09/22 19:46 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 08/09/22 19:46 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 08/09/22 19:46 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 08/09/22 19:46 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 08/09/22 19:46 75-71-81.0 1
1,1-Dichloroethane ND ug/L 08/09/22 19:46 75-34-31.0 1
1,2-Dichloroethane ND ug/L 08/09/22 19:46 107-06-21.0 1
1,1-Dichloroethene ND ug/L 08/09/22 19:46 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 08/09/22 19:46 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 08/09/22 19:46 156-60-51.0 1
1,2-Dichloropropane ND ug/L 08/09/22 19:46 78-87-51.0 1
1,3-Dichloropropane ND ug/L 08/09/22 19:46 142-28-91.0 1
2,2-Dichloropropane ND ug/L 08/09/22 19:46 594-20-71.0 1
1,1-Dichloropropene ND ug/L 08/09/22 19:46 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 08/09/22 19:46 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 08/09/22 19:46 10061-02-61.0 1
Diisopropyl ether ND ug/L 08/09/22 19:46 108-20-31.0 1
Ethylbenzene ND ug/L 08/09/22 19:46 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 08/09/22 19:46 87-68-32.0 1
2-Hexanone ND ug/L 08/09/22 19:46 591-78-65.0 1
Isopropylbenzene (Cumene)15.2 ug/L 08/09/22 19:46 98-82-81.0 1
p-Isopropyltoluene ND ug/L 08/09/22 19:46 99-87-61.0 1
Methylene Chloride ND ug/L 08/09/22 19:46 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/09/22 19:46 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 08/09/22 19:46 1634-04-41.0 1
Naphthalene 80.8 ug/L 08/09/22 19:46 91-20-31.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/11/2022 01:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92619080
LOADING RACK ( WILMINGTON)
Sample: KMW-9R Lab ID: 92619080004 Collected: 08/04/22 10:50 Received: 08/05/22 11:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
n-Propylbenzene 1.4 ug/L 08/09/22 19:46 103-65-11.0 1
Styrene ND ug/L 08/09/22 19:46 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 08/09/22 19:46 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 08/09/22 19:46 79-34-51.0 1
Tetrachloroethene ND ug/L 08/09/22 19:46 127-18-41.0 1
Toluene ND ug/L 08/09/22 19:46 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 08/09/22 19:46 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 08/09/22 19:46 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 08/09/22 19:46 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 08/09/22 19:46 79-00-51.0 1
Trichloroethene ND ug/L 08/09/22 19:46 79-01-61.0 1
Trichlorofluoromethane ND ug/L 08/09/22 19:46 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 08/09/22 19:46 96-18-41.0 1
1,2,4-Trimethylbenzene 3.9 ug/L 08/09/22 19:46 95-63-61.0 1
1,3,5-Trimethylbenzene 4.5 ug/L 08/09/22 19:46 108-67-81.0 1
Vinyl acetate ND ug/L 08/09/22 19:46 108-05-42.0 1
Vinyl chloride ND ug/L 08/09/22 19:46 75-01-41.0 1
Xylene (Total)3.1 ug/L 08/09/22 19:46 1330-20-71.0 1
m&p-Xylene 2.1 ug/L 08/09/22 19:46 179601-23-12.0 1
o-Xylene 1.0 ug/L 08/09/22 19:46 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)100 %08/09/22 19:46 460-00-470-130 1
1,2-Dichloroethane-d4 (S)104 %08/09/22 19:46 17060-07-070-130 1
Toluene-d8 (S)104 %08/09/22 19:46 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/11/2022 01:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92619080
LOADING RACK ( WILMINGTON)
Sample: KMW-13 Lab ID: 92619080005 Collected: 08/05/22 10:00 Received: 08/05/22 11:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 08/09/22 20:39 67-64-1125 5
Benzene ND ug/L 08/09/22 20:39 71-43-25.0 5
Bromobenzene ND ug/L 08/09/22 20:39 108-86-15.0 5
Bromochloromethane ND ug/L 08/09/22 20:39 74-97-55.0 5
Bromodichloromethane ND ug/L 08/09/22 20:39 75-27-45.0 5
Bromoform ND ug/L 08/09/22 20:39 75-25-25.0 5
Bromomethane ND ug/L 08/09/22 20:39 74-83-910.0 5
2-Butanone (MEK)ND ug/L 08/09/22 20:39 78-93-325.0 5
n-Butylbenzene ND ug/L 08/09/22 20:39 104-51-85.0 5
sec-Butylbenzene ND ug/L 08/09/22 20:39 135-98-85.0 5
Carbon tetrachloride ND ug/L 08/09/22 20:39 56-23-55.0 5
Chlorobenzene ND ug/L 08/09/22 20:39 108-90-75.0 5
Chloroethane ND ug/L 08/09/22 20:39 75-00-35.0 5
Chloroform ND ug/L 08/09/22 20:39 67-66-35.0 5
Chloromethane ND ug/L 08/09/22 20:39 74-87-35.0 5
2-Chlorotoluene ND ug/L 08/09/22 20:39 95-49-85.0 5
4-Chlorotoluene ND ug/L 08/09/22 20:39 106-43-45.0 5
1,2-Dibromo-3-chloropropane ND ug/L 08/09/22 20:39 96-12-810.0 5
Dibromochloromethane ND ug/L 08/09/22 20:39 124-48-15.0 5
1,2-Dibromoethane (EDB)ND ug/L 08/09/22 20:39 106-93-45.0 5
Dibromomethane ND ug/L 08/09/22 20:39 74-95-35.0 5
1,2-Dichlorobenzene ND ug/L 08/09/22 20:39 95-50-15.0 5
1,3-Dichlorobenzene ND ug/L 08/09/22 20:39 541-73-15.0 5
1,4-Dichlorobenzene ND ug/L 08/09/22 20:39 106-46-75.0 5
Dichlorodifluoromethane ND ug/L 08/09/22 20:39 75-71-85.0 5
1,1-Dichloroethane ND ug/L 08/09/22 20:39 75-34-35.0 5
1,2-Dichloroethane ND ug/L 08/09/22 20:39 107-06-25.0 5
1,1-Dichloroethene ND ug/L 08/09/22 20:39 75-35-45.0 5
cis-1,2-Dichloroethene ND ug/L 08/09/22 20:39 156-59-25.0 5
trans-1,2-Dichloroethene ND ug/L 08/09/22 20:39 156-60-55.0 5
1,2-Dichloropropane ND ug/L 08/09/22 20:39 78-87-55.0 5
1,3-Dichloropropane ND ug/L 08/09/22 20:39 142-28-95.0 5
2,2-Dichloropropane ND ug/L 08/09/22 20:39 594-20-75.0 5
1,1-Dichloropropene ND ug/L 08/09/22 20:39 563-58-65.0 5
cis-1,3-Dichloropropene ND ug/L 08/09/22 20:39 10061-01-55.0 5
trans-1,3-Dichloropropene ND ug/L 08/09/22 20:39 10061-02-65.0 5
Diisopropyl ether ND ug/L 08/09/22 20:39 108-20-35.0 5
Ethylbenzene ND ug/L 08/09/22 20:39 100-41-45.0 5
Hexachloro-1,3-butadiene ND ug/L 08/09/22 20:39 87-68-310.0 5
2-Hexanone ND ug/L 08/09/22 20:39 591-78-625.0 5
Isopropylbenzene (Cumene)9.9 ug/L 08/09/22 20:39 98-82-85.0 5
p-Isopropyltoluene ND ug/L 08/09/22 20:39 99-87-65.0 5
Methylene Chloride ND ug/L 08/09/22 20:39 75-09-225.0 5
4-Methyl-2-pentanone (MIBK)ND ug/L 08/09/22 20:39 108-10-125.0 5
Methyl-tert-butyl ether ND ug/L 08/09/22 20:39 1634-04-45.0 5
Naphthalene 20.3 ug/L 08/09/22 20:39 91-20-35.0 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/11/2022 01:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92619080
LOADING RACK ( WILMINGTON)
Sample: KMW-13 Lab ID: 92619080005 Collected: 08/05/22 10:00 Received: 08/05/22 11:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
n-Propylbenzene 14.1 ug/L 08/09/22 20:39 103-65-15.0 5
Styrene ND ug/L 08/09/22 20:39 100-42-55.0 5
1,1,1,2-Tetrachloroethane ND ug/L 08/09/22 20:39 630-20-65.0 5
1,1,2,2-Tetrachloroethane ND ug/L 08/09/22 20:39 79-34-55.0 5
Tetrachloroethene ND ug/L 08/09/22 20:39 127-18-45.0 5
Toluene ND ug/L 08/09/22 20:39 108-88-35.0 5
1,2,3-Trichlorobenzene ND ug/L 08/09/22 20:39 87-61-65.0 5
1,2,4-Trichlorobenzene ND ug/L 08/09/22 20:39 120-82-15.0 5
1,1,1-Trichloroethane ND ug/L 08/09/22 20:39 71-55-65.0 5
1,1,2-Trichloroethane ND ug/L 08/09/22 20:39 79-00-55.0 5
Trichloroethene ND ug/L 08/09/22 20:39 79-01-65.0 5
Trichlorofluoromethane ND ug/L 08/09/22 20:39 75-69-45.0 5
1,2,3-Trichloropropane ND ug/L 08/09/22 20:39 96-18-45.0 5
1,2,4-Trimethylbenzene 7.8 ug/L 08/09/22 20:39 95-63-65.0 5
1,3,5-Trimethylbenzene ND ug/L 08/09/22 20:39 108-67-85.0 5
Vinyl acetate ND ug/L 08/09/22 20:39 108-05-410.0 5
Vinyl chloride ND ug/L 08/09/22 20:39 75-01-45.0 5
Xylene (Total)1040 ug/L 08/09/22 20:39 1330-20-75.0 5
m&p-Xylene 1040 ug/L 08/09/22 20:39 179601-23-110.0 5
o-Xylene ND ug/L 08/09/22 20:39 95-47-65.0 5
Surrogates
4-Bromofluorobenzene (S)101 %08/09/22 20:39 460-00-470-130 5
1,2-Dichloroethane-d4 (S)103 %08/09/22 20:39 17060-07-070-130 5
Toluene-d8 (S)105 %08/09/22 20:39 2037-26-570-130 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/11/2022 01:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92619080
LOADING RACK ( WILMINGTON)
Sample: KMW-14 Lab ID: 92619080006 Collected: 08/04/22 12:32 Received: 08/05/22 11:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 08/09/22 18:36 67-64-125.0 1
Benzene ND ug/L 08/09/22 18:36 71-43-21.0 1
Bromobenzene ND ug/L 08/09/22 18:36 108-86-11.0 1
Bromochloromethane ND ug/L 08/09/22 18:36 74-97-51.0 1
Bromodichloromethane ND ug/L 08/09/22 18:36 75-27-41.0 1
Bromoform ND ug/L 08/09/22 18:36 75-25-21.0 1
Bromomethane ND ug/L 08/09/22 18:36 74-83-92.0 1
2-Butanone (MEK)ND ug/L 08/09/22 18:36 78-93-35.0 1
n-Butylbenzene ND ug/L 08/09/22 18:36 104-51-81.0 1
sec-Butylbenzene ND ug/L 08/09/22 18:36 135-98-81.0 1
Carbon tetrachloride ND ug/L 08/09/22 18:36 56-23-51.0 1
Chlorobenzene ND ug/L 08/09/22 18:36 108-90-71.0 1
Chloroethane ND ug/L 08/09/22 18:36 75-00-31.0 1
Chloroform ND ug/L 08/09/22 18:36 67-66-31.0 1
Chloromethane ND ug/L 08/09/22 18:36 74-87-31.0 1
2-Chlorotoluene ND ug/L 08/09/22 18:36 95-49-81.0 1
4-Chlorotoluene ND ug/L 08/09/22 18:36 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 08/09/22 18:36 96-12-82.0 1
Dibromochloromethane ND ug/L 08/09/22 18:36 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 08/09/22 18:36 106-93-41.0 1
Dibromomethane ND ug/L 08/09/22 18:36 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 08/09/22 18:36 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 08/09/22 18:36 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 08/09/22 18:36 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 08/09/22 18:36 75-71-81.0 1
1,1-Dichloroethane ND ug/L 08/09/22 18:36 75-34-31.0 1
1,2-Dichloroethane ND ug/L 08/09/22 18:36 107-06-21.0 1
1,1-Dichloroethene ND ug/L 08/09/22 18:36 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 08/09/22 18:36 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 08/09/22 18:36 156-60-51.0 1
1,2-Dichloropropane ND ug/L 08/09/22 18:36 78-87-51.0 1
1,3-Dichloropropane ND ug/L 08/09/22 18:36 142-28-91.0 1
2,2-Dichloropropane ND ug/L 08/09/22 18:36 594-20-71.0 1
1,1-Dichloropropene ND ug/L 08/09/22 18:36 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 08/09/22 18:36 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 08/09/22 18:36 10061-02-61.0 1
Diisopropyl ether ND ug/L 08/09/22 18:36 108-20-31.0 1
Ethylbenzene ND ug/L 08/09/22 18:36 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 08/09/22 18:36 87-68-32.0 1
2-Hexanone ND ug/L 08/09/22 18:36 591-78-65.0 1
Isopropylbenzene (Cumene)ND ug/L 08/09/22 18:36 98-82-81.0 1
p-Isopropyltoluene ND ug/L 08/09/22 18:36 99-87-61.0 1
Methylene Chloride ND ug/L 08/09/22 18:36 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/09/22 18:36 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 08/09/22 18:36 1634-04-41.0 1
Naphthalene ND ug/L 08/09/22 18:36 91-20-31.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/11/2022 01:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92619080
LOADING RACK ( WILMINGTON)
Sample: KMW-14 Lab ID: 92619080006 Collected: 08/04/22 12:32 Received: 08/05/22 11:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
n-Propylbenzene ND ug/L 08/09/22 18:36 103-65-11.0 1
Styrene ND ug/L 08/09/22 18:36 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 08/09/22 18:36 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 08/09/22 18:36 79-34-51.0 1
Tetrachloroethene ND ug/L 08/09/22 18:36 127-18-41.0 1
Toluene ND ug/L 08/09/22 18:36 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 08/09/22 18:36 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 08/09/22 18:36 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 08/09/22 18:36 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 08/09/22 18:36 79-00-51.0 1
Trichloroethene ND ug/L 08/09/22 18:36 79-01-61.0 1
Trichlorofluoromethane ND ug/L 08/09/22 18:36 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 08/09/22 18:36 96-18-41.0 1
1,2,4-Trimethylbenzene ND ug/L 08/09/22 18:36 95-63-61.0 1
1,3,5-Trimethylbenzene ND ug/L 08/09/22 18:36 108-67-81.0 1
Vinyl acetate ND ug/L 08/09/22 18:36 108-05-42.0 1
Vinyl chloride ND ug/L 08/09/22 18:36 75-01-41.0 1
Xylene (Total)ND ug/L 08/09/22 18:36 1330-20-71.0 1
m&p-Xylene ND ug/L 08/09/22 18:36 179601-23-12.0 1
o-Xylene ND ug/L 08/09/22 18:36 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)99 %08/09/22 18:36 460-00-470-130 1
1,2-Dichloroethane-d4 (S)106 %08/09/22 18:36 17060-07-070-130 1
Toluene-d8 (S)102 %08/09/22 18:36 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/11/2022 01:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92619080
LOADING RACK ( WILMINGTON)
Sample: TRIP BLANK Lab ID: 92619080007 Collected: 08/04/22 00:00 Received: 08/05/22 11:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 08/08/22 19:01 67-64-125.0 1
Benzene ND ug/L 08/08/22 19:01 71-43-21.0 1
Bromobenzene ND ug/L 08/08/22 19:01 108-86-11.0 1
Bromochloromethane ND ug/L 08/08/22 19:01 74-97-51.0 1
Bromodichloromethane ND ug/L 08/08/22 19:01 75-27-41.0 1
Bromoform ND ug/L 08/08/22 19:01 75-25-21.0 1
Bromomethane ND ug/L 08/08/22 19:01 74-83-92.0 1
2-Butanone (MEK)ND ug/L 08/08/22 19:01 78-93-35.0 1
n-Butylbenzene ND ug/L 08/08/22 19:01 104-51-81.0 1
sec-Butylbenzene ND ug/L 08/08/22 19:01 135-98-81.0 1
Carbon tetrachloride ND ug/L 08/08/22 19:01 56-23-51.0 1
Chlorobenzene ND ug/L 08/08/22 19:01 108-90-71.0 1
Chloroethane ND ug/L 08/08/22 19:01 75-00-31.0 1
Chloroform ND ug/L 08/08/22 19:01 67-66-31.0 1
Chloromethane ND ug/L 08/08/22 19:01 74-87-31.0 1
2-Chlorotoluene ND ug/L 08/08/22 19:01 95-49-81.0 1
4-Chlorotoluene ND ug/L 08/08/22 19:01 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 08/08/22 19:01 96-12-82.0 1
Dibromochloromethane ND ug/L 08/08/22 19:01 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 08/08/22 19:01 106-93-41.0 1
Dibromomethane ND ug/L 08/08/22 19:01 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 08/08/22 19:01 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 08/08/22 19:01 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 08/08/22 19:01 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 08/08/22 19:01 75-71-81.0 1
1,1-Dichloroethane ND ug/L 08/08/22 19:01 75-34-31.0 1
1,2-Dichloroethane ND ug/L 08/08/22 19:01 107-06-21.0 1
1,1-Dichloroethene ND ug/L 08/08/22 19:01 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 08/08/22 19:01 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 08/08/22 19:01 156-60-51.0 1
1,2-Dichloropropane ND ug/L 08/08/22 19:01 78-87-51.0 1
1,3-Dichloropropane ND ug/L 08/08/22 19:01 142-28-91.0 1
2,2-Dichloropropane ND ug/L 08/08/22 19:01 594-20-71.0 1
1,1-Dichloropropene ND ug/L 08/08/22 19:01 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 08/08/22 19:01 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 08/08/22 19:01 10061-02-61.0 1
Diisopropyl ether ND ug/L 08/08/22 19:01 108-20-31.0 1
Ethylbenzene ND ug/L 08/08/22 19:01 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 08/08/22 19:01 87-68-32.0 1
2-Hexanone ND ug/L 08/08/22 19:01 591-78-65.0 1
Isopropylbenzene (Cumene)ND ug/L 08/08/22 19:01 98-82-81.0 1
p-Isopropyltoluene ND ug/L 08/08/22 19:01 99-87-61.0 1
Methylene Chloride ND ug/L 08/08/22 19:01 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/08/22 19:01 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 08/08/22 19:01 1634-04-41.0 1
Naphthalene ND ug/L 08/08/22 19:01 91-20-31.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/11/2022 01:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92619080
LOADING RACK ( WILMINGTON)
Sample: TRIP BLANK Lab ID: 92619080007 Collected: 08/04/22 00:00 Received: 08/05/22 11:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
n-Propylbenzene ND ug/L 08/08/22 19:01 103-65-11.0 1
Styrene ND ug/L 08/08/22 19:01 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 08/08/22 19:01 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 08/08/22 19:01 79-34-51.0 1
Tetrachloroethene ND ug/L 08/08/22 19:01 127-18-41.0 1
Toluene ND ug/L 08/08/22 19:01 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 08/08/22 19:01 87-61-6 v21.0 1
1,2,4-Trichlorobenzene ND ug/L 08/08/22 19:01 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 08/08/22 19:01 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 08/08/22 19:01 79-00-51.0 1
Trichloroethene ND ug/L 08/08/22 19:01 79-01-61.0 1
Trichlorofluoromethane ND ug/L 08/08/22 19:01 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 08/08/22 19:01 96-18-41.0 1
1,2,4-Trimethylbenzene ND ug/L 08/08/22 19:01 95-63-61.0 1
1,3,5-Trimethylbenzene ND ug/L 08/08/22 19:01 108-67-81.0 1
Vinyl acetate ND ug/L 08/08/22 19:01 108-05-42.0 1
Vinyl chloride ND ug/L 08/08/22 19:01 75-01-41.0 1
Xylene (Total)ND ug/L 08/08/22 19:01 1330-20-71.0 1
m&p-Xylene ND ug/L 08/08/22 19:01 179601-23-12.0 1
o-Xylene ND ug/L 08/08/22 19:01 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)102 %08/08/22 19:01 460-00-470-130 1
1,2-Dichloroethane-d4 (S)124 %08/08/22 19:01 17060-07-070-130 1
Toluene-d8 (S)102 %08/08/22 19:01 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/11/2022 01:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92619080
LOADING RACK ( WILMINGTON)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
715792
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92619080007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3731626
Associated Lab Samples:92619080007
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 08/08/22 13:53
1,1,1-Trichloroethane ug/L ND 1.0 08/08/22 13:53
1,1,2,2-Tetrachloroethane ug/L ND 1.0 08/08/22 13:53
1,1,2-Trichloroethane ug/L ND 1.0 08/08/22 13:53
1,1-Dichloroethane ug/L ND 1.0 08/08/22 13:53
1,1-Dichloroethene ug/L ND 1.0 08/08/22 13:53
1,1-Dichloropropene ug/L ND 1.0 08/08/22 13:53
1,2,3-Trichlorobenzene ug/L ND 1.0 v208/08/22 13:53
1,2,3-Trichloropropane ug/L ND 1.0 08/08/22 13:53
1,2,4-Trichlorobenzene ug/L ND 1.0 08/08/22 13:53
1,2,4-Trimethylbenzene ug/L ND 1.0 08/08/22 13:53
1,2-Dibromo-3-chloropropane ug/L ND 2.0 08/08/22 13:53
1,2-Dibromoethane (EDB)ug/L ND 1.0 08/08/22 13:53
1,2-Dichlorobenzene ug/L ND 1.0 08/08/22 13:53
1,2-Dichloroethane ug/L ND 1.0 08/08/22 13:53
1,2-Dichloropropane ug/L ND 1.0 08/08/22 13:53
1,3,5-Trimethylbenzene ug/L ND 1.0 08/08/22 13:53
1,3-Dichlorobenzene ug/L ND 1.0 08/08/22 13:53
1,3-Dichloropropane ug/L ND 1.0 08/08/22 13:53
1,4-Dichlorobenzene ug/L ND 1.0 08/08/22 13:53
2,2-Dichloropropane ug/L ND 1.0 08/08/22 13:53
2-Butanone (MEK)ug/L ND 5.0 08/08/22 13:53
2-Chlorotoluene ug/L ND 1.0 08/08/22 13:53
2-Hexanone ug/L ND 5.0 08/08/22 13:53
4-Chlorotoluene ug/L ND 1.0 08/08/22 13:53
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 08/08/22 13:53
Acetone ug/L ND 25.0 08/08/22 13:53
Benzene ug/L ND 1.0 08/08/22 13:53
Bromobenzene ug/L ND 1.0 08/08/22 13:53
Bromochloromethane ug/L ND 1.0 08/08/22 13:53
Bromodichloromethane ug/L ND 1.0 08/08/22 13:53
Bromoform ug/L ND 1.0 08/08/22 13:53
Bromomethane ug/L ND 2.0 08/08/22 13:53
Carbon tetrachloride ug/L ND 1.0 08/08/22 13:53
Chlorobenzene ug/L ND 1.0 08/08/22 13:53
Chloroethane ug/L ND 1.0 08/08/22 13:53
Chloroform ug/L ND 1.0 08/08/22 13:53
Chloromethane ug/L ND 1.0 08/08/22 13:53
cis-1,2-Dichloroethene ug/L ND 1.0 08/08/22 13:53
cis-1,3-Dichloropropene ug/L ND 1.0 08/08/22 13:53
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/11/2022 01:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92619080
LOADING RACK ( WILMINGTON)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3731626
Associated Lab Samples:92619080007
Matrix: Water
Analyzed
Dibromochloromethane ug/L ND 1.0 08/08/22 13:53
Dibromomethane ug/L ND 1.0 08/08/22 13:53
Dichlorodifluoromethane ug/L ND 1.0 08/08/22 13:53
Diisopropyl ether ug/L ND 1.0 08/08/22 13:53
Ethylbenzene ug/L ND 1.0 08/08/22 13:53
Hexachloro-1,3-butadiene ug/L ND 2.0 08/08/22 13:53
Isopropylbenzene (Cumene)ug/L ND 1.0 08/08/22 13:53
m&p-Xylene ug/L ND 2.0 08/08/22 13:53
Methyl-tert-butyl ether ug/L ND 1.0 08/08/22 13:53
Methylene Chloride ug/L ND 5.0 08/08/22 13:53
n-Butylbenzene ug/L ND 1.0 08/08/22 13:53
n-Propylbenzene ug/L ND 1.0 08/08/22 13:53
Naphthalene ug/L ND 1.0 08/08/22 13:53
o-Xylene ug/L ND 1.0 08/08/22 13:53
p-Isopropyltoluene ug/L ND 1.0 08/08/22 13:53
sec-Butylbenzene ug/L ND 1.0 08/08/22 13:53
Styrene ug/L ND 1.0 08/08/22 13:53
Tetrachloroethene ug/L ND 1.0 08/08/22 13:53
Toluene ug/L ND 1.0 08/08/22 13:53
trans-1,2-Dichloroethene ug/L ND 1.0 08/08/22 13:53
trans-1,3-Dichloropropene ug/L ND 1.0 08/08/22 13:53
Trichloroethene ug/L ND 1.0 08/08/22 13:53
Trichlorofluoromethane ug/L ND 1.0 08/08/22 13:53
Vinyl acetate ug/L ND 2.0 08/08/22 13:53
Vinyl chloride ug/L ND 1.0 08/08/22 13:53
Xylene (Total)ug/L ND 1.0 08/08/22 13:53
1,2-Dichloroethane-d4 (S)%112 70-130 08/08/22 13:53
4-Bromofluorobenzene (S)%101 70-130 08/08/22 13:53
Toluene-d8 (S)%103 70-130 08/08/22 13:53
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3731627LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 47.750 95 70-130
1,1,1-Trichloroethane ug/L 48.350 97 70-130
1,1,2,2-Tetrachloroethane ug/L 46.750 93 70-130
1,1,2-Trichloroethane ug/L 46.250 92 70-130
1,1-Dichloroethane ug/L 48.050 96 70-130
1,1-Dichloroethene ug/L 46.750 93 70-132
1,1-Dichloropropene ug/L 51.950 104 70-131
1,2,3-Trichlorobenzene ug/L 41.1 v35082 70-134
1,2,3-Trichloropropane ug/L 46.250 92 70-130
1,2,4-Trichlorobenzene ug/L 43.350 87 70-130
1,2,4-Trimethylbenzene ug/L 47.350 95 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/11/2022 01:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92619080
LOADING RACK ( WILMINGTON)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3731627LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/L 45.550 91 70-132
1,2-Dibromoethane (EDB)ug/L 46.250 92 70-130
1,2-Dichlorobenzene ug/L 46.350 93 70-130
1,2-Dichloroethane ug/L 50.150 100 70-130
1,2-Dichloropropane ug/L 45.650 91 70-130
1,3,5-Trimethylbenzene ug/L 47.350 95 70-130
1,3-Dichlorobenzene ug/L 46.050 92 70-130
1,3-Dichloropropane ug/L 47.150 94 70-130
1,4-Dichlorobenzene ug/L 45.450 91 70-130
2,2-Dichloropropane ug/L 50.550 101 70-130
2-Butanone (MEK)ug/L 116100 116 70-133
2-Chlorotoluene ug/L 47.250 94 70-130
2-Hexanone ug/L 108100 108 70-130
4-Chlorotoluene ug/L 47.050 94 70-130
4-Methyl-2-pentanone (MIBK)ug/L 103100 103 70-130
Acetone ug/L 114100 114 70-144
Benzene ug/L 43.550 87 70-130
Bromobenzene ug/L 43.950 88 70-130
Bromochloromethane ug/L 48.750 97 70-130
Bromodichloromethane ug/L 46.350 93 70-130
Bromoform ug/L 48.650 97 70-131
Bromomethane ug/L 47.050 94 30-177
Carbon tetrachloride ug/L 45.850 92 70-130
Chlorobenzene ug/L 44.350 89 70-130
Chloroethane ug/L 55.750 111 46-131
Chloroform ug/L 44.650 89 70-130
Chloromethane ug/L 51.450 103 49-130
cis-1,2-Dichloroethene ug/L 47.250 94 70-130
cis-1,3-Dichloropropene ug/L 48.950 98 70-130
Dibromochloromethane ug/L 45.850 92 70-130
Dibromomethane ug/L 41.750 83 70-130
Dichlorodifluoromethane ug/L 53.550 107 52-134
Diisopropyl ether ug/L 53.250 106 70-131
Ethylbenzene ug/L 45.850 92 70-130
Hexachloro-1,3-butadiene ug/L 43.650 87 70-131
Isopropylbenzene (Cumene)ug/L 46.050 92 70-130
m&p-Xylene ug/L 92.7100 93 70-130
Methyl-tert-butyl ether ug/L 52.750 105 70-130
Methylene Chloride ug/L 47.150 94 68-130
n-Butylbenzene ug/L 49.950 100 70-130
n-Propylbenzene ug/L 46.550 93 70-130
Naphthalene ug/L 45.650 91 70-133
o-Xylene ug/L 46.450 93 70-130
p-Isopropyltoluene ug/L 49.350 99 70-130
sec-Butylbenzene ug/L 47.650 95 70-130
Styrene ug/L 47.150 94 70-130
Tetrachloroethene ug/L 41.450 83 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/11/2022 01:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92619080
LOADING RACK ( WILMINGTON)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3731627LABORATORY CONTROL SAMPLE:
LCSSpike
Toluene ug/L 42.950 86 70-130
trans-1,2-Dichloroethene ug/L 49.950 100 70-130
trans-1,3-Dichloropropene ug/L 49.050 98 70-130
Trichloroethene ug/L 44.750 89 70-130
Trichlorofluoromethane ug/L 47.350 95 61-130
Vinyl acetate ug/L 111100 111 70-140
Vinyl chloride ug/L 53.950 108 59-142
Xylene (Total)ug/L 139150 93 70-130
1,2-Dichloroethane-d4 (S)%114 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3731628MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92619168001
3731629
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 132 70-135124 620ND26.3 24.8
1,1,1-Trichloroethane ug/L 20 136 70-148128 620ND27.1 25.6
1,1,2,2-Tetrachloroethane ug/L 20 126 70-131120 520ND25.2 23.9
1,1,2-Trichloroethane ug/L 20 130 70-136123 520ND25.9 24.6
1,1-Dichloroethane ug/L 20 133 70-147126 520ND26.6 25.2
1,1-Dichloroethene ug/L 20 144 70-158137 520ND28.7 27.4
1,1-Dichloropropene ug/L 20 148 70-149139 620ND29.5 27.9
1,2,3-Trichlorobenzene ug/L M12014168-140128 1020ND28.3 25.5
1,2,3-Trichloropropane ug/L 20 126 67-137119 520ND25.1 23.8
1,2,4-Trichlorobenzene ug/L 20 139 70-139128 920ND27.8 25.5
1,2,4-Trimethylbenzene ug/L M12013570-134126 720ND26.9 25.1
1,2-Dibromo-3-chloropropane ug/L 20 126 69-136119 520ND25.2 23.9
1,2-Dibromoethane (EDB)ug/L 20 127 70-137121 520ND25.4 24.1
1,2-Dichlorobenzene ug/L 20 131 70-133122 720ND26.1 24.4
1,2-Dichloroethane ug/L 20 127 67-138121 520ND25.3 24.2
1,2-Dichloropropane ug/L 20 136 70-138126 720ND27.2 25.3
1,3,5-Trimethylbenzene ug/L M12013970-138129 720ND27.8 25.9
1,3-Dichlorobenzene ug/L 20 133 70-133122 820ND26.5 24.5
1,3-Dichloropropane ug/L 20 127 70-136121 520ND25.4 24.1
1,4-Dichlorobenzene ug/L 20 127 70-133119 720ND25.5 23.7
2,2-Dichloropropane ug/L 20 141 52-155132 620ND28.2 26.5
2-Butanone (MEK)ug/L 40 114 61-147110 340ND45.5 43.9
2-Chlorotoluene ug/L 20 132 70-141125 620ND26.5 24.9
2-Hexanone ug/L 40 121 67-139116 540ND48.6 46.4
4-Chlorotoluene ug/L 20 132 70-135125 620ND26.4 25.0
4-Methyl-2-pentanone (MIBK) ug/L 40 120 67-136114 440ND47.9 45.8
Acetone ug/L 40 97 55-15993 440ND38.9 37.3
Benzene ug/L 20 126 67-150119 620ND25.3 23.8
Bromobenzene ug/L 20 128 70-134121 620ND25.7 24.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/11/2022 01:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92619080
LOADING RACK ( WILMINGTON)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3731628MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92619168001
3731629
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Bromochloromethane ug/L 20 133 70-146126 520ND26.6 25.2
Bromodichloromethane ug/L 20 128 70-138121 620ND25.7 24.2
Bromoform ug/L 20 130 57-138122 720ND26.1 24.3
Bromomethane ug/L 20 132 10-200125 620ND26.4 24.9
Carbon tetrachloride ug/L 20 134 70-147126 620ND26.8 25.3
Chlorobenzene ug/L 20 130 70-137121 720ND26.0 24.2
Chloroethane ug/L IL2012951-166126 320ND25.9 25.2
Chloroform ug/L 20 125 70-144115 820ND25.0 23.0
Chloromethane ug/L M12017124-161158 720ND34.1 31.7
cis-1,2-Dichloroethene ug/L 20 134 67-148127 520ND27.5 26.1
cis-1,3-Dichloropropene ug/L 20 135 70-142128 620ND27.1 25.5
Dibromochloromethane ug/L 20 130 68-138122 620ND25.9 24.3
Dibromomethane ug/L 20 124 70-134118 520ND24.9 23.7
Dichlorodifluoromethane ug/L 20 149 43-155141 520ND29.8 28.2
Diisopropyl ether ug/L 20 128 65-146122 520ND25.6 24.4
Ethylbenzene ug/L 20 132 68-143124 620ND26.4 24.8
Hexachloro-1,3-butadiene ug/L M12015762-151140 1120ND31.4 28.0
Isopropylbenzene (Cumene) ug/L 20 131 70-136124 620ND26.3 24.7
m&p-Xylene ug/L 40 133 53-157126 640ND53.3 50.3
Methyl-tert-butyl ether ug/L 20 121 59-156114 620ND24.3 22.8
Methylene Chloride ug/L 20 111 64-148105 520ND22.2 21.1
n-Butylbenzene ug/L M12014570-139134 820ND29.1 26.7
n-Propylbenzene ug/L 20 136 70-138127 720ND27.2 25.4
Naphthalene ug/L 20 141 57-150128 1020ND28.3 25.6
o-Xylene ug/L 20 131 68-143125 520ND26.2 24.9
p-Isopropyltoluene ug/L M12014570-141132 920ND29.0 26.5
sec-Butylbenzene ug/L 20 137 70-137128 720ND27.4 25.6
Styrene ug/L 20 132 70-136125 520ND26.3 25.1
Tetrachloroethene ug/L 20 126 70-139121 420ND25.7 24.7
Toluene ug/L 20 130 47-157123 620ND26.1 24.6
trans-1,2-Dichloroethene ug/L 20 140 70-149132 620ND28.1 26.4
trans-1,3-Dichloropropene ug/L 20 135 70-138126 620ND26.9 25.3
Trichloroethene ug/L 20 140 70-149130 6207.1 35.2 33.1
Trichlorofluoromethane ug/L 20 137 61-154130 620ND27.5 25.9
Vinyl acetate ug/L 40 136 48-156129 540ND54.6 51.8
Vinyl chloride ug/L 20 161 55-172154 420ND32.3 30.8
Xylene (Total)ug/L 60 133 66-145125 660ND79.5 75.2
1,2-Dichloroethane-d4 (S)%102 70-130102
4-Bromofluorobenzene (S)%102 70-130102
Toluene-d8 (S)%101 70-130101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/11/2022 01:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92619080
LOADING RACK ( WILMINGTON)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
716050
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92619080001, 92619080002, 92619080003, 92619080004, 92619080005, 92619080006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3732938
Associated Lab Samples:92619080001, 92619080002, 92619080003, 92619080004, 92619080005, 92619080006
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 08/09/22 13:35
1,1,1-Trichloroethane ug/L ND 1.0 08/09/22 13:35
1,1,2,2-Tetrachloroethane ug/L ND 1.0 08/09/22 13:35
1,1,2-Trichloroethane ug/L ND 1.0 08/09/22 13:35
1,1-Dichloroethane ug/L ND 1.0 08/09/22 13:35
1,1-Dichloroethene ug/L ND 1.0 08/09/22 13:35
1,1-Dichloropropene ug/L ND 1.0 08/09/22 13:35
1,2,3-Trichlorobenzene ug/L ND 1.0 08/09/22 13:35
1,2,3-Trichloropropane ug/L ND 1.0 08/09/22 13:35
1,2,4-Trichlorobenzene ug/L ND 1.0 08/09/22 13:35
1,2,4-Trimethylbenzene ug/L ND 1.0 08/09/22 13:35
1,2-Dibromo-3-chloropropane ug/L ND 2.0 08/09/22 13:35
1,2-Dibromoethane (EDB)ug/L ND 1.0 08/09/22 13:35
1,2-Dichlorobenzene ug/L ND 1.0 08/09/22 13:35
1,2-Dichloroethane ug/L ND 1.0 08/09/22 13:35
1,2-Dichloropropane ug/L ND 1.0 08/09/22 13:35
1,3,5-Trimethylbenzene ug/L ND 1.0 08/09/22 13:35
1,3-Dichlorobenzene ug/L ND 1.0 08/09/22 13:35
1,3-Dichloropropane ug/L ND 1.0 08/09/22 13:35
1,4-Dichlorobenzene ug/L ND 1.0 08/09/22 13:35
2,2-Dichloropropane ug/L ND 1.0 08/09/22 13:35
2-Butanone (MEK)ug/L ND 5.0 08/09/22 13:35
2-Chlorotoluene ug/L ND 1.0 08/09/22 13:35
2-Hexanone ug/L ND 5.0 08/09/22 13:35
4-Chlorotoluene ug/L ND 1.0 08/09/22 13:35
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 08/09/22 13:35
Acetone ug/L ND 25.0 08/09/22 13:35
Benzene ug/L ND 1.0 08/09/22 13:35
Bromobenzene ug/L ND 1.0 08/09/22 13:35
Bromochloromethane ug/L ND 1.0 08/09/22 13:35
Bromodichloromethane ug/L ND 1.0 08/09/22 13:35
Bromoform ug/L ND 1.0 08/09/22 13:35
Bromomethane ug/L ND 2.0 08/09/22 13:35
Carbon tetrachloride ug/L ND 1.0 08/09/22 13:35
Chlorobenzene ug/L ND 1.0 08/09/22 13:35
Chloroethane ug/L ND 1.0 08/09/22 13:35
Chloroform ug/L ND 1.0 08/09/22 13:35
Chloromethane ug/L ND 1.0 08/09/22 13:35
cis-1,2-Dichloroethene ug/L ND 1.0 08/09/22 13:35
cis-1,3-Dichloropropene ug/L ND 1.0 08/09/22 13:35
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/11/2022 01:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92619080
LOADING RACK ( WILMINGTON)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3732938
Associated Lab Samples:92619080001, 92619080002, 92619080003, 92619080004, 92619080005, 92619080006
Matrix: Water
Analyzed
Dibromochloromethane ug/L ND 1.0 08/09/22 13:35
Dibromomethane ug/L ND 1.0 08/09/22 13:35
Dichlorodifluoromethane ug/L ND 1.0 08/09/22 13:35
Diisopropyl ether ug/L ND 1.0 08/09/22 13:35
Ethylbenzene ug/L ND 1.0 08/09/22 13:35
Hexachloro-1,3-butadiene ug/L ND 2.0 08/09/22 13:35
Isopropylbenzene (Cumene)ug/L ND 1.0 08/09/22 13:35
m&p-Xylene ug/L ND 2.0 08/09/22 13:35
Methyl-tert-butyl ether ug/L ND 1.0 08/09/22 13:35
Methylene Chloride ug/L ND 5.0 08/09/22 13:35
n-Butylbenzene ug/L ND 1.0 08/09/22 13:35
n-Propylbenzene ug/L ND 1.0 08/09/22 13:35
Naphthalene ug/L ND 1.0 08/09/22 13:35
o-Xylene ug/L ND 1.0 08/09/22 13:35
p-Isopropyltoluene ug/L ND 1.0 08/09/22 13:35
sec-Butylbenzene ug/L ND 1.0 08/09/22 13:35
Styrene ug/L ND 1.0 08/09/22 13:35
Tetrachloroethene ug/L ND 1.0 08/09/22 13:35
Toluene ug/L ND 1.0 08/09/22 13:35
trans-1,2-Dichloroethene ug/L ND 1.0 08/09/22 13:35
trans-1,3-Dichloropropene ug/L ND 1.0 08/09/22 13:35
Trichloroethene ug/L ND 1.0 08/09/22 13:35
Trichlorofluoromethane ug/L ND 1.0 08/09/22 13:35
Vinyl acetate ug/L ND 2.0 08/09/22 13:35
Vinyl chloride ug/L ND 1.0 08/09/22 13:35
Xylene (Total)ug/L ND 1.0 08/09/22 13:35
1,2-Dichloroethane-d4 (S)%102 70-130 08/09/22 13:35
4-Bromofluorobenzene (S)%102 70-130 08/09/22 13:35
Toluene-d8 (S)%102 70-130 08/09/22 13:35
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3732939LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 51.350 103 70-130
1,1,1-Trichloroethane ug/L 53.350 107 70-130
1,1,2,2-Tetrachloroethane ug/L 47.350 95 70-130
1,1,2-Trichloroethane ug/L 50.950 102 70-130
1,1-Dichloroethane ug/L 52.050 104 70-130
1,1-Dichloroethene ug/L 55.650 111 70-132
1,1-Dichloropropene ug/L 57.350 115 70-131
1,2,3-Trichlorobenzene ug/L 52.750 105 70-134
1,2,3-Trichloropropane ug/L 46.650 93 70-130
1,2,4-Trichlorobenzene ug/L 52.550 105 70-130
1,2,4-Trimethylbenzene ug/L 50.750 101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/11/2022 01:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92619080
LOADING RACK ( WILMINGTON)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3732939LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/L 46.750 93 70-132
1,2-Dibromoethane (EDB)ug/L 50.650 101 70-130
1,2-Dichlorobenzene ug/L 51.050 102 70-130
1,2-Dichloroethane ug/L 54.050 108 70-130
1,2-Dichloropropane ug/L 51.050 102 70-130
1,3,5-Trimethylbenzene ug/L 51.850 104 70-130
1,3-Dichlorobenzene ug/L 51.550 103 70-130
1,3-Dichloropropane ug/L 51.150 102 70-130
1,4-Dichlorobenzene ug/L 50.250 100 70-130
2,2-Dichloropropane ug/L 55.250 110 70-130
2-Butanone (MEK)ug/L 90.7100 91 70-133
2-Chlorotoluene ug/L 50.050 100 70-130
2-Hexanone ug/L 86.3100 86 70-130
4-Chlorotoluene ug/L 50.450 101 70-130
4-Methyl-2-pentanone (MIBK)ug/L 88.1100 88 70-130
Acetone ug/L 91.9100 92 70-144
Benzene ug/L 48.050 96 70-130
Bromobenzene ug/L 50.050 100 70-130
Bromochloromethane ug/L 56.550 113 70-130
Bromodichloromethane ug/L 52.450 105 70-130
Bromoform ug/L 51.850 104 70-131
Bromomethane ug/L 52.650 105 30-177
Carbon tetrachloride ug/L 49.350 99 70-130
Chlorobenzene ug/L 50.150 100 70-130
Chloroethane ug/L 57.850 116 46-131
Chloroform ug/L 53.050 106 70-130
Chloromethane ug/L 50.950 102 49-130
cis-1,2-Dichloroethene ug/L 52.850 106 70-130
cis-1,3-Dichloropropene ug/L 53.650 107 70-130
Dibromochloromethane ug/L 51.650 103 70-130
Dibromomethane ug/L 50.650 101 70-130
Dichlorodifluoromethane ug/L 51.750 103 52-134
Diisopropyl ether ug/L 50.650 101 70-131
Ethylbenzene ug/L 49.750 99 70-130
Hexachloro-1,3-butadiene ug/L 54.150 108 70-131
Isopropylbenzene (Cumene)ug/L 50.750 101 70-130
m&p-Xylene ug/L 100100 100 70-130
Methyl-tert-butyl ether ug/L 53.150 106 70-130
Methylene Chloride ug/L 50.150 100 68-130
n-Butylbenzene ug/L 53.350 107 70-130
n-Propylbenzene ug/L 50.350 101 70-130
Naphthalene ug/L 50.950 102 70-133
o-Xylene ug/L 49.850 100 70-130
p-Isopropyltoluene ug/L 53.550 107 70-130
sec-Butylbenzene ug/L 51.050 102 70-130
Styrene ug/L 51.150 102 70-130
Tetrachloroethene ug/L 48.650 97 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/11/2022 01:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92619080
LOADING RACK ( WILMINGTON)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3732939LABORATORY CONTROL SAMPLE:
LCSSpike
Toluene ug/L 47.250 94 70-130
trans-1,2-Dichloroethene ug/L 55.550 111 70-130
trans-1,3-Dichloropropene ug/L 53.950 108 70-130
Trichloroethene ug/L 52.250 104 70-130
Trichlorofluoromethane ug/L 49.250 98 61-130
Vinyl acetate ug/L 112100 112 70-140
Vinyl chloride ug/L 54.450 109 59-142
Xylene (Total)ug/L 150150 100 70-130
1,2-Dichloroethane-d4 (S)%104 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3732940MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92619069004
3732941
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 4000 100 70-135104 44000ND4020 4170
1,1,1-Trichloroethane ug/L 4000 118 70-148120 24000ND4720 4800
1,1,2,2-Tetrachloroethane ug/L 4000 101 70-131125 214000ND4030 5000
1,1,2-Trichloroethane ug/L 4000 105 70-136112 64000ND4210 4460
1,1-Dichloroethane ug/L 4000 119 70-147124 44000ND4750 4950
1,1-Dichloroethene ug/L 4000 119 70-158129 84000ND4770 5160
1,1-Dichloropropene ug/L 4000 128 70-149131 24000ND5110 5230
1,2,3-Trichlorobenzene ug/L M140008768-14065 294000ND3480 2600
1,2,3-Trichloropropane ug/L v340009567-137118 214000ND3790 4700
1,2,4-Trichlorobenzene ug/L R1400010170-13973 324000ND4030 2930
1,2,4-Trimethylbenzene ug/L 4000 101 70-134106 54000ND4120 4320
1,2-Dibromo-3-chloropropane ug/L 4000 80 69-13678 34000ND3200 3110
1,2-Dibromoethane (EDB)ug/L 4000 97 70-137108 104000ND3890 4310
1,2-Dichlorobenzene ug/L 4000 103 70-133107 34000ND4140 4270
1,2-Dichloroethane ug/L 4000 117 67-138124 64000ND4690 4960
1,2-Dichloropropane ug/L 4000 104 70-138113 84000ND4160 4520
1,3,5-Trimethylbenzene ug/L 4000 109 70-138110 14000ND4370 4410
1,3-Dichlorobenzene ug/L 4000 98 70-133110 114000ND3920 4390
1,3-Dichloropropane ug/L 4000 85 70-136111 264000ND3400 4430
1,4-Dichlorobenzene ug/L 4000 99 70-133109 94000ND3970 4360
2,2-Dichloropropane ug/L 4000 102 52-155112 104000ND4060 4470
2-Butanone (MEK)ug/L 8000 104 61-147104 08000ND8340 8350
2-Chlorotoluene ug/L 4000 107 70-141109 14000ND4290 4340
2-Hexanone ug/L 8000 86 67-139100 158000ND6880 7980
4-Chlorotoluene ug/L 4000 103 70-135107 44000ND4110 4260
4-Methyl-2-pentanone (MIBK) ug/L 8000 96 67-13699 38000ND7640 7900
Acetone ug/L 8000 113 55-159122 88000ND9030 9770
Benzene ug/L 4000 103 67-150110 74000ND4130 4410
Bromobenzene ug/L 4000 103 70-134105 24000ND4100 4190
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/11/2022 01:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92619080
LOADING RACK ( WILMINGTON)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3732940MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92619069004
3732941
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Bromochloromethane ug/L 4000 109 70-146120 94000ND4370 4780
Bromodichloromethane ug/L 4000 101 70-138108 74000ND4040 4330
Bromoform ug/L 4000 63 57-13886 304000ND2530 3430
Bromomethane ug/L 4000 117 10-200121 34000ND4660 4820
Carbon tetrachloride ug/L 4000 116 70-147120 34000ND4650 4800
Chlorobenzene ug/L 4000 103 70-137109 64000ND4130 4370
Chloroethane ug/L 4000 137 51-166146 64000ND5500 5830
Chloroform ug/L 4000 114 70-144111 24000ND4540 4440
Chloromethane ug/L 4000 126 24-161136 74000ND5050 5430
cis-1,2-Dichloroethene ug/L 4000 113 67-148120 54000ND4540 4790
cis-1,3-Dichloropropene ug/L 4000 100 70-142106 64000ND4010 4250
Dibromochloromethane ug/L 4000 70 68-13889 244000ND2780 3550
Dibromomethane ug/L 4000 89 70-13495 64000ND3570 3790
Dichlorodifluoromethane ug/L 4000 145 43-155151 54000ND5790 6060
Diisopropyl ether ug/L 4000 104 65-146111 64000ND4170 4430
Ethylbenzene ug/L 4000 102 68-143114 104000ND4160 4610
Hexachloro-1,3-butadiene ug/L 4000 107 62-15179 304000ND4300 3170
Isopropylbenzene (Cumene) ug/L M1400010770-136143 284000ND4290 5700
m&p-Xylene ug/L M1800015853-157199 480006210074800 78100
Methyl-tert-butyl ether ug/L 4000 102 59-156115 124000ND4080 4580
Methylene Chloride ug/L 4000 102 64-148114 94000ND4980 5460
n-Butylbenzene ug/L 4000 108 70-139113 54000ND4310 4530
n-Propylbenzene ug/L 4000 108 70-138110 14000ND4330 4390
Naphthalene ug/L 4000 88 57-15071 224000ND3530 2840
o-Xylene ug/L 4000 109 68-143135 214000ND4430 5450
p-Isopropyltoluene ug/L 4000 108 70-141118 94000ND4330 4720
sec-Butylbenzene ug/L 4000 110 70-137114 44000ND4390 4580
Styrene ug/L 4000 106 70-136133 234000ND4240 5330
Tetrachloroethene ug/L 4000 78 70-139100 254000ND3100 3980
Toluene ug/L 4000 105 47-157112 74000ND4190 4490
trans-1,2-Dichloroethene ug/L 4000 120 70-149129 74000ND4820 5170
trans-1,3-Dichloropropene ug/L 4000 96 70-138103 74000ND3850 4120
Trichloroethene ug/L 4000 106 70-149113 74000ND4230 4520
Trichlorofluoromethane ug/L 4000 114 61-154119 54000ND4560 4770
Vinyl acetate ug/L 8000 117 48-156118 18000ND9330 9450
Vinyl chloride ug/L 4000 137 55-172148 84000ND5480 5940
Xylene (Total)ug/L MS1200014266-145178 5120006210079200 83500
1,2-Dichloroethane-d4 (S)%111 70-130114
4-Bromofluorobenzene (S)%109 70-130128
Toluene-d8 (S)%103 70-130102
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/11/2022 01:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 32
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92619080
LOADING RACK ( WILMINGTON)
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be
considered an estimated value.IL
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Analyte recovery in the matrix spike was outside QC limits for one or more of the constituent analytes used in the
calculated result.MS
RPD value was outside control limits.R1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/11/2022 01:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 32
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92619080
LOADING RACK ( WILMINGTON)
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92619080001 716050KMW-6 EPA 8260D
92619080002 716050KMW-7 EPA 8260D
92619080003 716050KMW-8 EPA 8260D
92619080004 716050KMW-9R EPA 8260D
92619080005 716050KMW-13 EPA 8260D
92619080006 716050KMW-14 EPA 8260D
92619080007 715792TRIP BLANK EPA 8260D
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/11/2022 01:26 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 32
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Appendix E

Mann-Kendall Trend Analyses

BENZENE

NAPHTHALENE

TOTAL XYLENES