WI-16971_16971_CA_RMR_20211124_3264

Tetra Tech, Inc.
805 E 20th Street Charlotte, NC 28205
Tel [phone] www.tetratech.com
November 24, 2021
Ms. Liz Price
North Carolina Department of Environmental Quality
Division of Waste Management
127 Cardinal Drive Extension
Wilmington, North Carolina 28405-3845
RE: Remediation Update Report for September 2020 to August 2021
Former Flint Hills Resources North Terminal - Loading Rack Area
3325 River Road, Wilmington, North Carolina
NCDEQ Incident No. 16971
Dear Ms. Price,
Tetra Tech, on behalf of Flint Hills Resources, LP (FHR), is submitting for your review the
Remediation Update Report (RUR) for the period of September 2020 through August 2021 for the
above referenced site. Tetra Tech assumed environmental management of the Loading Rack on behalf
of FHR beginning in January 2021.
In August 2021, Tetra Tech collected groundwater samples from 18 monitoring wells for VOC analysis
in accordance with the 2020 RUR recommendations. Laboratory results indicated similar detections of
contaminants to previous results, which continue to demonstrate effective attenuation across the site.
We recommended removing monitoring wells ADW-1, AMW-1, KDW-1, and KMW-5 from the
monitoring network in 2022, as concentrations at these locations have been decreasing and have been
less than 2L GWQS for multiple years, and other wells in the network adequately monitor the extent
of groundwater impacts.
Please notify me at [e-mail] or 734-213-4079 if you have any questions or
comments regarding the information presented in this report.
Sincerely,
Matt Mahony Daniel Sopoci, CHMM
Project Manager Program Manager
cc: Michael Christopher, Flint Hills Resources LP
Stacey Kirk, Chemserve Terminal of Wilmington
Benjamin Francisco, Tetra Tech
© 2021. Flint Hills Resources LP. All rights reserved.
Annual Remediation Update Report
September 2020 – August 2021
Flint Hills Resources, LP
North Terminal - Loading Rack Area
NCDEQ Incident No. 16971
Wilmington, North Carolina
November 24, 2021
© 2021. Flint Hills Resources LP. All rights reserved.
Annual Remediation Update Report
September 2020 – August 2021
Flint Hills Resources, LP
North Terminal - Loading Rack Area
NCDEQ Incident No. 16971
Wilmington, North Carolina
Prepared for:
Flint Hills Resources, LP
P.O. Box 2917
Wichita, KS 67201
Prepared by:
Tetra Tech
805 E 20th Street
Charlotte, NC 28205
November 24, 2021
___________________________ __________________________
Daniel Sopoci, CHMM Matt Mahony
Program Manager Project Manager
CERTIFICATIONPAGENORTHCAROLINALICENSEDGEOLOGISTCERTIFICATIONI,BenjaminH.Francisco,aLicensedGeologistforTetraTechGeologicalServicesP.C.,docertifythattheinformationcontainedinthisreportiscorrectandaccuratetothebestofmyknowledge.DatTetraTechGeologicalServicesP.C.islicensedtopracticegeologyinNorthCarolina.ThecertificationnumberofthecompanyorcorporationisC-524.BenjaminH.Francisco,L.G.NorthCarolinaLicenseNo.1987

2021 Annual Remediation Update Report Former FHR North Terminal – Loading Rack
© 2021. Flint Hills Resources LP. All rights reserved. Page i
TABLE OF CONTENTS

1. INTRODUCTION ................................................................................................................ 1
1.1 Site Description ................................................................................................................ 1
1.2 Facility Status ................................................................................................................... 2
2. GROUNDWATER MONITORING ....................................................................................... 3
2.1 Groundwater Elevations and Flow Direction ..................................................................... 3
2.2 Groundwater Monitoring Methods ..................................................................................... 2
2.3 Groundwater Monitoring Results ...................................................................................... 2
2.3.1 Loading Rack ............................................................................................................. 3
2.3.2 Apex Property ............................................................................................................ 3
2.3.3 FHR WTP................................................................................................................... 4
2.3.4 Mann-Kendall Trend Analysis..................................................................................... 4
2.4 Groundwater Monitoring Recommendations ..................................................................... 5
2.4.1 Loading Rack ............................................................................................................. 5
2.4.2 Apex Property ............................................................................................................ 6
2.4.3 FHR WTP................................................................................................................... 6
3. CONCLUSIONS .................................................................................................................... 7

TABLES
Table 1 2021 Groundwater Elevations and Field Measurements
Table 2 Groundwater Results – Volatile Organic Compounds
FIGURES
Figure 1 Site Location
Figure 2 Site Layout
Figure 3 Site Features
Figure 4 Groundwater Elevation Contours
Figure 5 Groundwater Results – Volatile Organic Compounds
APPENDICES
Appendix A Historical Groundwater Elevations
Appendix B Historical Groundwater Field Measurements
Appendix C Historical Groundwater Results
Appendix D Laboratory Analytical Reports
Appendix E Mann-Kendall Trend Analyses

2021 Annual Remediation Update Report Former FHR North Terminal – Loading Rack
© 2021. Flint Hills Resources LP. All rights reserved. Page 1
1. INTRODUCTION
On behalf of Flint Hills Resources, LP (FHR), Tetra Tech, Inc. (Tetra Tech) has prepared this
Remediation Update Report (RUR) for the former FHR North Terminal Loading Rack area
(Loading Rack) located at 3325 River Road, Wilmington, New Hanover County, North Carolina
(Figure 1). Past groundwater investigations of the former FHR Loading Rack area revealed
concentrations of paraxylene (PX), dissolved gasoline, and fuel oil in exceedance of the 15A North
Carolina Administrative Code (NCAC) 2L.0202 North Carolina Groundwater Quality Standard (2L
GWQS), updated April 1, 2013. RURs for the Loading Rack area have been submitted annually
since 2002 by CATLIN Engineers and Scientists (CATLIN), and Tetra Tech has assumed
environmental management of the Loading Rack on behalf of FHR beginning in January 2021.

As detailed in the 2002 Corrective Action Plan (CAP) Addendum, groundwater contamination in
the Loading Rack area is assumed to be from historical operation and maintenance activities of
the former FHR truck and railcar loading racks. These operations are assumed to have resulted
in minor releases. Therefore, current groundwater impacts are not associated with a specific
release event. Historical remedial approaches at the Loading Rack are detailed in previous RURs
and have included ex-situ soil remediation, product removal from recovery wells, aggressive fluid
vapor recovery (AFVR), and most recently in 2017, three Epsom salt and water solution (EAB)
amendment injection events. A technical memorandum summarizing the EAB amendment was
included in Appendix A of the 2017 RUR. Monitored natural attenuation is the current remedial
approach as proposed in the 2020 RUR. Applicable remedial action documents since the initial
2002 CAP Addendum are presented in the 2020 RUR.

This report provides an annual update to remediation activities and results for the monitoring
period between September 2020 through August 2021. The annual groundwater sampling event
occurred in August 2021 with no other significant activities during the reporting period.
1.1 Site Description
The Loading Rack area is a subdivision of the larger North Terminal site, a facility comprising
approximately 37 acres for bulk chemical storage and transfer previously owned and operated by
FHR (Figure 2). Approximately 33 acres of the former North Terminal are located on the east
side of River Road and are divided into three project areas: the Loading Rack in the southwestern
corner of the site, the Paraxylene (PX) Facility in the north, and the Gasoline Fuel Oil (GFO)
Facility in the southeast. Remediation activities related to the PX Facility revealed additional

2021 Annual Remediation Update Report Former FHR North Terminal – Loading Rack
© 2021. Flint Hills Resources LP. All rights reserved. Page 2
environmental concerns and in 2002 the North Carolina Department of Environmental Quality
(NCDEQ) accepted a CAP Addendum by FHR which addressed the Loading Rack area. These
properties are currently owned and operated by Chemserve Terminal of Wilmington, LLC
(Chemserve) for bulk chemical storage and transfer operations.
FHR retains ownership of an additional four acres on the west side of River Road comprising the
FHR water treatment plant (FHR WTP) area which was initially designed to treat groundwater
from recovery wells on the PX Facility. FHR regularly updates NCDEQ on the status of the PX
Facility in separate reports filed under separate covers. The GFO Facility immediately east of the
Loading Rack area received No Further Action (NFA) status from NCDEQ on December 2, 2019.
1.2 Facility Status
The former FHR truck loading rack was disassembled in 2003 and the lot remained largely
undeveloped until 2014 when Chemserve built a new bulk chemical truck loading rack in the same
general footprint of the former FHR rack.

Since 2013, Loading Rack sampling activities have also included monitoring non-FHR petroleum
hydrocarbon source areas on the Apex Oil Company, Inc. (Apex) petroleum fuel property on the
west side of River Road, as well as several monitoring wells on the FHR WTP property adjacent
to the north (Figure 2). Based on review of NCDEQ files, it is understood that Apex has
implemented various technologies to address the presence of free-phase product and are
monitoring the dissolved groundwater contaminant plume on their property on an annual basis.

Regulatory responsibilities for managing contamination at the Loading Rack were transferred from
NCDEQ’s Division of Water Quality (DWQ) – Aquifer Protection Section (APS), to the Division of
Waste Management (DWM) - Underground Storage Tank (UST) Section in 2007. FHR
understands that the DWM-UST Section will manage the site in accordance with the July 1, 2012
Guidelines for Initial Response and Abatement, Assessment, and Corrective Action for Non-UST
Releases of Petroleum. The corrective actions implemented and documented within this report
are in general accordance with this guidance document.

2021 Annual Remediation Update Report Former FHR North Terminal – Loading Rack
© 2021. Flint Hills Resources LP. All rights reserved. Page 3
2. GROUNDWATER MONITORING
Contaminants of concern in groundwater with concentration detections greater than 2L GWQS
criteria at the Loading Rack site since 2001 include benzene, n-butylbenzene, sec-butylbenzene,
ethylbenzene, isopropylbenzene, naphthalene, methyl tert butyl ether (MTBE), n-propylbenzene,
toluene, 1,2,4-trimethylbenzene, 1,3,5-trimethylbenzene and xylenes. Through active remediation
and attenuation, concentrations of these contaminants have decreased over time. In the last three
years since 2017, the only contaminants of concern with detections greater than 2L GWQS are:

 Benzene
 Ethylbenzene
 Isopropylbenzene (Cumene)
 Naphthalene
 1,2,4-trimethylbenzene
 Total meta/para-xylenes

Based on the recommendations in the 2020 RUR, Tetra Tech gauged and sampled 18
groundwater wells in August 2021 to continue to monitor attenuation. Sample locations included
five monitoring wells on the Loading Rack site, eight on the Apex property, and four on the FHR
WTP property (Figure 3). Sample locations included mostly shallow Type II wells with total depths
ranging from 7.11 to 17.51 feet below ground surface (bgs). Two locations were deep Type III
wells, with total depths of 41.63 and 50.28 feet bgs on the Loading Rack and Apex property,
respectively.

Field personnel completed groundwater sampling in accordance with the June 7, 2005 Revised
Remedial Action Plan (RAP); the December 21, 2015 CAP Addendum; and minor modifications
in subsequent RURs. The following sections describe field activities completed in 2021.

2.1 Groundwater Elevations and Flow Direction
Tetra Tech field personnel measured static groundwater levels of 18 groundwater monitoring
wells on August 20, 2021. All wells were gauged with an oil/water interface probe accurate to 0.01
foot which was thoroughly rinsed with Liquinox and distilled water following each use to minimize
the potential for cross contamination between wells. Depth-to-water measurements were
subtracted from top-of-casing elevations for each well to obtain groundwater surface elevations.

Groundwater elevations are presented in Table 1 and a summary of historical groundwater
elevations is presented in Appendix A. Water elevations at the Loading Rack site ranged from

2021 Annual Remediation Update Report Former FHR North Terminal – Loading Rack
© 2021. Flint Hills Resources LP. All rights reserved. Page 2
6.21 to 24.20 feet amsl, and static elevations in August 2021 were on average 0.24 feet higher
than those measured in August 2020. Groundwater elevation contours are provided in Figure 4,
indicating groundwater flow in the vicinity of the Loading Rack is towards the west-northwest,
consistent with previous findings.

2.2 Groundwater Monitoring Methods
Groundwater sampling included low flow methods consistent with the Low Stress (Low Flow)
Purging and Sampling Procedure for the Collection of Groundwater Samples from Monitoring
Wells (2017), published by the United States Environmental Protection Agency (EPA). At each
monitoring well, groundwater was purged using a peristaltic pump with disposable tubing while
measuring field groundwater quality parameters including temperature, specific conductivity,
dissolved oxygen, pH, oxidation reduction potential, and turbidity multi-parameter meter with a
flow-through cell. Groundwater samples were transferred to laboratory-supplied containers,
placed into ice-packed coolers, and handled under the proper chain-of-custody procedures for
laboratory analysis of volatile organic compounds (VOCs) per EPA Method 8260 by Pace
Analytical of Huntersville, North Carolina (NC Certification #12).

2.3 Groundwater Monitoring Results
A summary of field measurements is presented as Table 1 and a summary of historical water
quality results are presented in Appendix B. A summary of laboratory analytical results for 2012
through 2021 is presented as Table 2 and a summary of historical laboratory analytical results is
presented in Appendix C. Laboratory analytical reports are included as Appendix D.
Groundwater sample detections of benzene, toluene, ethylbenzene, MTBE, naphthalene, and
total xylenes are presented in Figure 5. Free product has not been detected in Loading Rack
monitoring wells since August 2008. VOC were detected in 13 of 18 monitoring wells sampled. In
eight wells, detections of at least one constituent exceeded 2L GWQS.

The following sections describe groundwater monitoring results in each of three areas: the
Loading Rack east of River Road, the Apex property west of River Road, and the FHR WTP area
west of River Road.

2021 Annual Remediation Update Report Former FHR North Terminal – Loading Rack
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2.3.1 Loading Rack
There are five monitoring wells east of River Road in the Loading Rack area. Of these, KMW-1,
KMW-7, and KMW-9R are in the truck loading rack area and exhibit detections less than 2L
GWQS and generally continue to decrease. Detections of VOCs in KMW-1, KMW-7, and KMW-
9R were generally consistent with detections in the previous few years, with a few notable
exceptions. For the first time since 2012, meta/para-xylenes were not detected in KMW-1. In
addition, several constituents were not detected in KMW-9R for the first time, including non-detect
results for n-propylene, toluene, trimethylbenzene isomers, and xylenes.

Monitoring wells KMW-6 and KMW-8 are also east of River Road and are located in the railcar
loading area. Although detections of meta/para-xylenes continue to exceed 2L GWQS in KMW-
6, detections decreased more than 60% compared to 2020 results, and have decreased over
90% since 2018. Similarly, detections of naphthalene continue to exceed 2L GWQS in KMW-8,
however; concentrations decreased 45% compared to 2020 results, and the 2021 detection is the
lowest recorded at this location. Benzene also exceeded 2L GWQS at KMW-8.

Results in 2021 demonstrate continued attenuation in recent years following active remediation
efforts implemented by FHR.

2.3.2 Apex Property
There are nine monitoring wells west of River Road located on the Apex property. Of these, four
wells are located directly across from the Loading Rack along the west side of River Road. KMW-
12 and KMW-13 are located immediately west of the Loading Rack and exhibit concentrations of
benzene, naphthalene, and meta/para-xylenes exceeding 2L GWQS, consistent with previous
detections. Although concentrations continue to exceed 2L GWQS, attenuation is occurring.
Detections of several constituents in KMW-12 are the lowest recorded, including for benzene and
naphthalene. Concentrations at KMW-13 continue to demonstrate sustained decreases from
previous high values as well. Also, directly across from the Loading Rack, wells KMW-14 and
ADW-1 did not exhibit any contaminant concentrations greater than 2L GWQS, consistent with
recent monitoring results.

Wells AMW-1 through AMW-5 monitor groundwater quality throughout the remainder of Apex
property. AMW-1 is the southernmost monitoring location and AMW-5 is the westernmost

2021 Annual Remediation Update Report Former FHR North Terminal – Loading Rack
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monitoring location. Results from both locations are less than 2L GWQS, similar to 2020.
Monitoring locations AMW-2, AMW-3 and AMW-4 exceeded 2L GWQS. In recent years,
concentrations have remained elevated in AMW-4, while monitoring results from the rest of the
wells across the site demonstrate sustained decreasing trends. This observation suggests a
potential alternate source of elevated VOCs in AMW-4 unrelated to the previous operation and
maintenance activities of the former FHR truck and railcar loading racks.

2.3.3 FHR WTP
Monitoring wells located on the FHR WTP include four locations: KMW-1, KMW-3, KMW-5, and
KMW-18. For the second year in a row, only one detection exceeded 2L GWQS at these locations.
Benzene at KMW-3 exceeded 2L GWQS but remained 75% less than 2019 detections.
Meta/para-xylenes continue to decrease at KMW-1 and KMW-3, including non-detect results in
2021. Monitoring results from locations at the FHR WTP continue to demonstrate attenuation of
groundwater contaminants.

2.3.4 Mann-Kendall Trend Analysis
A graphical representation of VOC concentrations versus time for monitoring wells are included
in Appendix E. Mann-Kendall trend analyses were performed using the EPA’s ProUCL for the
historical Loading Rack data sets from 2001 to present, which are summarized in the table below.
The 16 Type II shallow wells sampled in 2021 were included in the dataset.

Monitoring
Well
Trends
Benzene Naphthalene Total Xylenes
KMW-1 Decreasing Decreasing No Trend
KMW-3 No Trend No Trend No Trend
KMW-5 Decreasing Decreasing Decreasing
KMW-6 Decreasing Decreasing No Trend
KMW-7 Decreasing Decreasing Decreasing
KMW-8 Decreasing Decreasing Decreasing
KMW-9R Decreasing Decreasing Decreasing
KMW-12 Decreasing Decreasing Decreasing

2021 Annual Remediation Update Report Former FHR North Terminal – Loading Rack
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Monitoring
Well
Trends (Continued)
Benzene Naphthalene Total Xylenes
KMW-13 Decreasing Decreasing Decreasing
KMW-14 Decreasing Decreasing Decreasing
KMW-18 No Trend No Trend No Trend
AMW-1 Decreasing No Trend Decreasing
AMW-2 Decreasing Decreasing Decreasing
AMW-3 Decreasing Decreasing Decreasing
AMW-4 Decreasing Increasing Increasing
AMW-5 Decreasing No Trend No Trend

Statistical analysis indicates decreasing contaminant concentration trends are prevalent for the
wells sampled in 2021 which have either decreasing trends or no trend, with the exception of
increasing naphthalene and total xylene trends in AMW-4 on the Apex property. As discussed in
previous RURs, review of historical groundwater data indicates an alternative source of
groundwater contaminants at AMW-4 that are unrelated to the previous operation and
maintenance activities of the former FHR truck and railcar loading racks. This potential source
area in the vicinity of AMW-4 is likely the cause of elevated levels of various analytes detected in
monitoring wells located on the downgradient portion of Apex property as well as the western
portion of the FHR WTP area. FHR’s understanding is that Apex has implemented and continues
to monitor remedial activities on their property.

2.4 Groundwater Monitoring Recommendations
Select groundwater monitoring wells will continue to be sampled annually for laboratory analysis
of VOCs per EPA Method 8260, and an RUR summarizing the August 2022 sampling event will
be submitted to NCDEQ by November 30, 2022. The following sections discuss the justification
for eliminating KDW-1, ADW-1, AMW-1, and KMW-5 from the current monitoring network.

2.4.1 Loading Rack
Monitoring well KDW-1 is a Type III deep monitoring well located within the source area of the
Loading Rack and was first sampled in 2015 for vertical delineation of contaminants. Analytical
results demonstrate a sustained decrease in VOC concentrations that have remained less than

2021 Annual Remediation Update Report Former FHR North Terminal – Loading Rack
© 2021. Flint Hills Resources LP. All rights reserved. Page 6
2L GWQS for all constituents since 2017. Shallow Type II well KMW-9R, adjacent to KDW-1, will
continue to be monitored. Results from KMW-9R will provide data to sufficiently monitor
groundwater quality in the immediate vicinity of KDW-1.

2.4.2 Apex Property
Monitoring well ADW-1 is a Type III deep monitoring well located along River Road across from
the Loading Rack and was first sampled in 2014 for vertical delineation of contaminants. Analytical
results demonstrate a sustained decrease in VOC concentrations that have remained less than
2L GWQS for all constituents since 2017. Shallow Type II wells KMW-13 and KMW-14, near
ADW-1, will continue to be monitored. Results from KMW-13 and KMW-14 will provide data to
sufficiently monitor groundwater quality in the immediate vicinity of ADW-1.

Monitoring well AMW-1 is located approximately 350 feet south-southwest of the Loading Rack
site and is hydraulically cross-gradient. AMW-1 had no detections of VOCs in 2021 or 2020, and
the most recent detection greater than 2L GWQS was a benzene result of 1.5 micrograms per
liter (ug/L) in 2012.

2.4.3 FHR WTP
Monitoring well KMW-5 is located approximately 350 feet north-northwest and hydraulically cross-
gradient from the Loading Rack site. KMW-5 has had no detections of VOCs over the laboratory
reporting limits in the last three years, except for a detection of MTBE at 3.0 ug/L in 2019, well
below the 2L GWQS of 20 ug/L. There have been no exceedances of 2L GWQS in KMW-5 since
2017. Furthermore, KMW-1 is located in the general vicinity of KMW-5 and will continue to provide
cross-gradient delineation of the extent of groundwater impacts.

2021 Annual Remediation Update Report Former FHR North Terminal – Loading Rack
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3. CONCLUSIONS
This annual report summarizes the annual groundwater monitoring completed in August 2021.

Water depths were gauged with an interface probe from 18 monitoring wells on the Loading Rack,
Apex property, and FHR WTP. Groundwater elevations were consistent with previous monitoring
events, indicating a west-northwest flow in the direction of the Cape Fear River.

Groundwater samples collected from 18 monitoring wells for VOC analysis indicated similar
detections of contaminants to previous results, which continue to demonstrate effective
attenuation across the site. Free product has not been observed in Loading Rack monitoring wells
since 2008. Although concentrations of several contaminants exceeded 2L GWQS in eight
locations in 2021, result indicate a sustained decreasing or stable trend in all instances except at
AMW-4. As discussed in Section 2.3.4 and in previous RURs, elevated contaminant
concentrations at AMW-4 are likely from another source unrelated to previous operation and
maintenance activities of the former FHR truck and railcar loading racks.

Groundwater sampling will continue in 2022 to monitor natural attenuation of contaminants. As
discussed in Section 2.4, it is recommended to remove monitoring wells ADW-1, AMW-1, KDW-
1, and KMW-5 from the monitoring network in 2022. Concentrations at these locations have been
decreasing and have been less than 2L GWQS for multiple years. Other monitoring wells in the
network adequately monitor the extent of groundwater impacts.

The next sampling event will be completed in August 2022 to include monitoring wells KMW-1,
KMW-3, KMW-6, KMW-7, KMW-8, KMW-9R, KMW-12, KMW-13, KMW-14, KMW-18, AMW-2,
AMW-3, AMW-4, and AMW-5 for laboratory analysis of VOCs using EPA Method 8260. A RUR
summarizing August 2022 sampling results will be submitted to NCDEQ by November 30, 2022.

TABLES

Table 1
Groundwater Elevations and Water Quality Measurements
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
FHR WTP KMW-1 8/21/2021 1.33 11.79 27.94 0.089 2.65 6.79 79 58.6
FHR WTP KMW-3 8/21/2021 0.54 11.22 28.89 0.254 0.00 6.46 -169 11.2
FHR WTP KMW-5 8/21/2021 2.76 15.24 25.09 0.257 0.11 6.83 -19 4.7
Loading Rack KMW-6 8/22/2021 1.80 12.21 27.93 0.783 0.00 6.98 -333 6.8
Loading Rack KMW-7 8/23/2021 1.44 12.81 29.15 0.178 0.00 6.72 -246 28.0
Loading Rack KMW-8 8/22/2021 1.10 9.45 26.01 0.474 0.00 6.96 -257 18.8
Loading Rack KMW-9R 8/23/2021 3.08 11.47 27.80 0.408 0.04 6.39 95 17.9
Apex Property KMW-12 8/22/2021 9.18 11.86 28.74 0.435 0.00 6.41 -243 62.7
Apex Property KMW-13 8/23/2021 8.24 15.36 29.13 0.844 0.00 6.71 -125 24.4
Apex Property KMW-14 8/22/2021 7.78 14.83 28.93 0.315 2.04 6.68 -63 12.4
FHR WTP KMW-18 8/21/2021 2.04 12.65 26.52 0.525 0.00 6.97 -190 7.6
Apex Property AMW-1 8/21/2021 8.40 17.51 27.32 0.324 0.00 6.77 -135 11.6
Apex Property AMW-2 8/21/2021 8.93 16.00 24.61 0.677 0.00 6.73 -235 7.0
Apex Property AMW-3 8/22/2021 4.93 14.94 24.31 0.296 0.00 6.62 -237 14.9
Apex Property AMW-4 8/21/2021 5.01 15.49 27.42 0.241 0.00 6.46 -197 11.0
Apex Property AMW-5 8/21/2021 1.22 7.11 29.30 0.540 0.00 6.83 -124 16.0
Apex Property ADW-1 8/22/2021 6.63 41.63 25.78 0.925 0.09 11.69 -155 35.6
Loading Rack KDW-1 8/23/2021 7.68 50.28 26.70 1.70 1.24 11.76 -171 3.4
Notes:
Historical groundwater elevations and water quality readings are provided in Appendix A and Appendix B, respectively.
Water quality parameter results presented in this table represent the final measurements prior to sampling.
Total depths measured in the field by Tetra Tech August 20, 2021.
KMW-13 had excessive drawdown and the last reading after approximately 20 minutes of low flow purging is presented, after which the pump was turned up and the well pumped dry.
FHR WTP = Flint Hills Resources Water Treatment Plant
bgs = below ground surface
Temp = Temperature
°C = degrees Celsius
mS/cm = millisiemens per centimeter
mg/L = milligrams per liter
mV = millivolts
ORP = Oxidation Reduction Potential
NTU = Nephelometric Turbidity Unit
Location ORP
(mV)
Turbidity
(NTU)Well ID Date pH
Specific
Conductance
(mS/cm)
Dissolved
Oxygen
(mg/L)
Depth to
Groundwater
(bgs)
Temp (°C) Total Depth
(bgs)
Table 2Groundwater Results, 2012-2021Loading Rack AreaFormer FHR North TerminalWilmington, North CarolinaSample ID Date Collected170 70 600 70 20670 600 400 400Varies3/1/2012 <0.25 <0.41 <0.38 <0.30 <0.40 1.2 <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 ND5/22/2012 <0.25 6.0 2.0 <0.30 1.3 <0.21 1.8 3.5 <0.26 2.3 0.71 J <0.66 <0.23 55.98/17/2012 <0.25 <0.41 1.1 <0.30 <0.40 0.73 J <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 ND8/13/2013 <0.25 <0.41 <0.38 0.35 J <0.40 <0.21 <0.24 <0.42 <0.26 0.31 J <0.36 113 <0.23 ND8/21/2014 <0.25 <0.41 <0.38 0.48 J <0.40 <0.21 0.27 J <0.42 <0.26 <0.31 <0.36 39.9 <0.23 11.95 J3/11/2015 <0.25 <0.41 <0.38 0.94 J <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36 713 <0.23 0.35 J8/5/2015 <0.50 2.2 <0.76 12.0 <0.80 <0.42 0.86 J <0.84 <0.52 3.0 <0.72 14,700 1.8 J 0.73 J8/1/2016 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36 5.6 <0.23 ND8/7/2017 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36 10.0 <0.23 ND8/7/2019 <0.15 <0.23 <0.20 <0.26 <0.20 <0.28 <0.35 <0.18 <0.24 <0.17 <0.20 33.3 <0.22 ND8/6/2020 <0.30 <0.47 <0.40 0.69 J <0.40 <0.55 <0.70 <0.37 0.57 J <0.34 <0.39 416 <0.44 ND8/21/2021 <0.34 <0.49 <0.40 <0.30 <0.33 <0.42 <0.64 <0.34 <0.48 <0.50 <0.33 <0.71 <0.34 ND8/17/2012 12.8 <0.41 <0.38 3.0 33.0 0.25 J 1.1 21.2 0.68 J 51.6 <0.36 <0.66 0.24 J ND8/13/2013 27.8 <0.41 2.2 1.4 24.5 0.45 J 2.0 16.7 3.4 11.1 6.5 7.1 0.93 J ND8/21/2014 18.9 <0.41 <0.38 342 88.9 0.50 J 78.1 42.3 92.5 362 91.4 396 0.59 J 30.03/11/2015 7.5 <0.82 <0.76 42.4 54.8 <0.42 46.3 29.3 1.6 J 242 86.7 237 0.57 J 8.7 J8/5/2015 10.7 <0.41 <0.38 0.95 J 33.0 <0.21 11.7 16.4 1.5 38.6 31.6 33.5 <0.23 5.2 J8/1/2016 12.1 <1.0 8.1 8.5 62.3 <0.52 40.9 32.7 3.4 298 133 311 <0.58 58.2J8/8/2017 14.0 <0.41 <0.38 1.2 27.9 <0.21 2.2 14.7 2.6 8.8 9.4 3.4 0.76 J ND8/7/2019 35.9 <0.23 12.2 3.3 89.9 1.2 0.96 J 47.9 3.5 68.0 <0.20 4.2 0.43 J 7.68/6/2020 8.0 <0.23 2.0 <0.26 16.3 <0.28 0.41 J 12.0 1.4 0.52 J <0.20 4.6 0.25 J ND8/21/2021 8.0 <0.49 1.1 <0.30 11.6 <0.42 <0.64 7.5 1.6 <0.50 <0.33 <0.71 <0.34 ND3/1/2012 <0.25 <0.41 1.0 <0.30 0.64 J 0.80 J <0.24 1.9 <0.26 0.48 J 0.41 J <0.66 <0.23 ND5/22/2012 <0.25 <0.41 <0.38 <0.30 <0.40 3.2 <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 4.1 J8/17/2012 <0.25 <0.41 <0.38 <0.30 <0.40 2.1 <0.24 <0.42 <0.26 <0.31 <0.36 58.7 <0.23 ND8/13/2013 <0.25 <0.41 <0.38 <0.30 <0.40 1.0 0.45 J <0.42 <0.26 1.3 <0.36 5,710 0.83 J 4.87 J8/13/2013 DUP <50.0 <82.0 <76.0 <60.0 <80.0 <42.0 <48.0 <84.0 <52.0 <62.0 <72.0 6,450 <46.0 7318/21/2014 <0.25 <0.41 <0.38 0.45 J <0.40 0.49 J 0.44 J <0.42 <0.26 <0.31 <0.36 164 <0.23 0.30 J3/11/2015 <0.25 <0.41 <0.38 <0.30 <0.40 0.88 J <0.24 <0.42 <0.26 <0.31 <0.36 5.1 <0.23 ND8/5/2015 <0.25 <0.41 <0.38 <0.30 <0.40 0.52 J <0.24 <0.42 <0.26 <0.31 <0.36 0.78 J <0.23 ND8/1/2016 <0.25 <0.41 <0.38 3.6 <0.40 0.78 J <0.24 <0.42 <0.26 0.32 J <0.36 99.1 1.3 0.62 J8/16/2017 <1.2 <2.0 <1.9 2.2 J <2.0 <1.0 <1.2 <2.1 5.1 <1.6 <1.8 1,840 <1.2 ND8/8/2018 <0.25 <0.41 <0.38 0.30 J <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36 99.6 0.23 J ND8/7/2019 <0.15 <0.23 <0.20 <0.26 <0.20 3.0 <0.35 <0.18 <0.24 <0.17 <0.20 <0.41 <0.22 ND8/6/2020 <0.15 <0.23 <0.20 <0.26 <0.20 <0.28 <0.35 <0.18 <0.24 <0.17 <0.20 <0.41 <0.22 ND8/21/2021 <0.34 <0.49 <0.40 <0.30 <0.33 <0.42 <0.64 <0.34 <0.48 <0.50 <0.33 <0.71 <0.34 NDNotes are provided on the final page of this table. KMW-5KMW-3TYPE II MONITORING WELLSKMW-1m/p-Xyleneso-XyleneAll Other 8260B AnalytesGroundwater Clean-up Goal (ug/L)500Methyl Tert Butyl Ether (MTBE)Naphthalenen-PropylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneContaminant of ConcernBenzenen-Butylbenzenesec-ButylbenzeneEthylbenzeneIsopropylbenzene (Cumene)Page 1 of 7
Table 2Groundwater Results, 2012-2021Loading Rack AreaFormer FHR North TerminalWilmington, North CarolinaSample ID Date Collected170 70 600 70 20670 600 400 400Variesm/p-Xyleneso-XyleneAll Other 8260B AnalytesGroundwater Clean-up Goal (ug/L)500Methyl Tert Butyl Ether (MTBE)Naphthalenen-PropylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneContaminant of ConcernBenzenen-Butylbenzenesec-ButylbenzeneEthylbenzeneIsopropylbenzene (Cumene)8/20/2012 <12.5 <20.5 <19.0 18.4 J <20.0 <10.5 <12.0 <21.0 <13.0 <15.5 <18.011,60016.4 J ND8/14/2013 <50.0 <82.0 <76.0 69.0 J <80.0 <42.0 <48.0 <84.0 <52.0 <62.0 <72.040,60056.8 J 360 J8/14/2014 <50.0 <82.0 <76.0 99.7 J <80.0 <42.0 <48.0 <84.0 <52.0 <62.0 <72.061,30078.6 J ND3/11/2015 <50.0 <82.0 <76.0 125 J <80.0 <42.0 <48.0 <84.0 <52.0 <62.0 <72.076,80095.6 J ND8/5/2015 <62.5 <102 <95.0 102 J <100 <52.5 <60.0 <105 <65.0 <77.5 <90.069,500102 J ND8/1/2016 <50.0 <82.0 <76.0 78.8 J <80.0 <42.0 <48.0 <84.0 <52.0 <62.0 <72.045,60066.6 J ND10/6/2016<50.0NA NA<60.0NA NA NA NA<52.0NA NA27,400 <46.0NA11/23/2016<50.0NA NA90.9 JNA NA NA NA<52.0NA NA57,800 79.2 JNA3/2/2017<62.5<102 <95.093.8 J<100 <52.5 256 <105<65.0<77.5 <90.048,400 66.2 JND4/26/2017<62.5 NA NA 81.2 J NA NA NA NA 86.8 J NA NA 45,000 72.8 JNA8/9/2017<50.0<82.0 <76.060.6 J <80.0<42.0 <48.0 <84.079.0 J 148 J <72.0 43,500 93.7 JND3/7/2018 <50.0 NA NA 106 J NA NA NA NA <52.0 NA NA 73,700 96.6 J NA5/23/2018 <62.5 NA NA 125 J NA NA NA NA <65.0 NA NA 67,700 115 J NA8/8/2018 <50.0<82.0 <76.062.9 J <80.0<42.0 <48.0 <84.0<52.0<62.0 <72.040,900 66.4 J ND2/5/2019 <30.0 NA NA 72.6 J NA NA NA NA <48.8 NA NA 40,200 <44.0 NA8/7/2019 <30.0 <46.8 <40.2 60.8 J <40.2 <55.0 <70.4 <37.0 <48.8 <34.0 <39.4 28,900 55.6 J ND8/6/2020 <15.0 <23.4 <20.1 34.6 J <20.1 <27.5 <35.2 <18.5 <24.4 <17.0 <19.7 19,700 26.0 J ND8/22/2021 <8.6 <12.2 <10.0 <7.6 <8.3 <10.6 <16.1 <8.5 <12.1 <12.4 <8.3 7,120 <8.4 ND8/20/2012 <0.25 <0.41 <0.38 10.0 4.4 <0.21 49.2 6.5 <0.26 1.6 1.3 13.8 0.76 J ND8/14/2013 <0.25 <0.41 1.1 10.7 7.3 <0.21 78.5 10.6 <0.26 2.3 2.4 26.7 1.1 ND8/14/2013 DUP <0.25 <0.41 <0.38 12.4 7.9 <0.21 88.6 11.4 <0.26 2.8 2.6 28.8 1.2 ND8/14/2014 <0.25 <0.41 5.5 7.8 13.1 0.22 J 7.0 26.5 <0.26 <0.31 3.2 9.5 0.26 J 1.53/11/2015 <0.25 <0.41 <0.38 6.5 10.4 <0.21 9.9 19.3 <0.26 <0.31 2.3 7.0 0.40 J ND8/5/2015 <0.25 2.2 2.3 7.1 12.5 <0.21 12.5 24.7 <0.26 2.4 2.0 4.5 0.32 J ND8/1/2016 <0.25 0.89 J 0.79 J 2.5 4.0 <0.21 4.5 8.4 <0.26 1.2 0.77 J 1.4 J <0.23 ND10/6/2016 <0.25 NA NA 2.3 NA NA NA NA <0.26 NA NA 1.1 J <0.23 NA3/2/2017 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 0.56 J8/7/2017 <0.25 <0.41 0.61 J 1.1 2.9 <0.21 <0.24 5.3 <0.26 0.37 J <0.36 0.82 J <0.23 ND3/7/2018 <0.25 NA NA 1.7 NA NA NA NA <0.26 NA NA 1.7 J <0.23 NA5/23/2018 <0.25 NA NA 0.65 J NA NA NA NA <0.26 NA NA 0.85 J <0.23 NA8/7/2018 <0.25 <0.41 <0.38<0.30 <0.400.28 J<0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23ND8/7/2019 <0.15 <0.23 1.30.87 J 4.41.4<0.35 6.5 <0.24 <0.17 <0.20 1.2 J <0.22ND8/6/2020 <0.15 <0.23 0.76 J<0.26 2.8<0.280.56 J 3.4 <0.24 <0.17 0.31 J 5.0 <0.22ND8/23/2021 <0.34 <0.49 <0.40<0.30 1.9<0.42<0.64 2.3 <0.48 <0.50 <0.33 <0.71 <0.34NDNotes are provided on the final page of this table. KMW-6KMW-7TYPE II MONITORING WELLS (Continued)Page 2 of 7
Table 2Groundwater Results, 2012-2021Loading Rack AreaFormer FHR North TerminalWilmington, North CarolinaSample ID Date Collected170 70 600 70 20670 600 400 400Variesm/p-Xyleneso-XyleneAll Other 8260B AnalytesGroundwater Clean-up Goal (ug/L)500Methyl Tert Butyl Ether (MTBE)Naphthalenen-PropylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneContaminant of ConcernBenzenen-Butylbenzenesec-ButylbenzeneEthylbenzeneIsopropylbenzene (Cumene)8/20/2012 91.8 <1.0 <0.95 27.8 16.1 0.57 J 41.5 37.1 3.8 83.5 28.3145 4.564.48/14/2013 271 42.5 463 204 30.4 <4.2 244 61.0 20.9 513 1201,630 54.954.7 J8/14/2014 169 <2.0 1.9 279 33.5 <1.0 173 47.0 15.9 385 94.81,060 35.8ND3/11/2015 89.1 <0.41 <0.38 195 30.3 0.45 J 151 51.3 7.5 154 <0.36371 25.960.94 J8/5/2015 15.6 <0.82 <0.76 51.9 23.3 <0.42 112 32.7 2.2 245 53.1202 6.71,0428/1/2016 76.9 <0.82 2.6 44.0 24.3 0.68 J 61.9 28.4 2.4 161 16.6190 8.910.3 J10/6/2016 55.2 NA NA 14.1 NA NA NA NA 1.2 NA NA 32.2 3.3 NA11/23/2016 83.7 NA NA 31.4 NA NA NA NA 0.88 J NA NA 59.8 6.2 NA3/2/2017 14.7 <0.41 <0.38 7.8 1.8 <0.21 15.9 2.4 0.37 J 70.5 9.6 18.5 2.8 27.86 J4/26/2017 4.7 NA NA 1.4 NA NA NA NA <0.26 NA NA 56.3 0.67 J NA8/9/2017 13.9 <0.41 <0.38 6.6 3.7 <0.21 30.4 2.9 0.35 J 101 <0.36 15.3 3.3 ND3/7/2018 52.6 NA NA 17.4 NA NA NA NA 0.80 J NA NA 31.9 4.2 NA5/23/2018 20.8 NA NA 1.4 NA NA NA NA <0.26 NA NA 6.2 3.8 NA8/8/2018 44.1<0.41 <0.3821.4 10.2 0.76 J 59.4 <0.42 0.55 J 178 <0.36 16.7 4.5 3.69 J2/5/2019 56.2 NA NA 12.3 NA NA NA NA 0.44 J NA NA 37.1 2.3 NA8/7/2019 35.5 <0.23 <0.20 16.1 7.2 <0.28 12.7 6.0 0.95 J 32.1 <0.20 8.8 2.6 26.28/6/2020 42.6 <0.23 <0.20 11.1 6.4 <0.28 11.7 4.5 0.94 J 40.4 4.9 20.3 2.3 14.3 J8/22/2021 44.9 1.7 4.8 9.1 22.9 <0.42 6.4 22.5 <0.48 9.0 1.9 5.7 <0.34 ND2/2/2015 <6.2 <10.2 <9.5 774 48.2 <5.2 396 107 40.6 297 96.3 541 8.5 J 47.9 J3/11/2015 1.4 J 24.0 <1.9 535 59.8 <1.0 385 102 34.3 154 39.1 364 4.9 J ND8/5/2015 0.91 J 13.5 <0.76 <0.60 54.4 <0.42 146 78.1 24.9 76.9 14.8 45.5 1.7 J 43.9 J8/1/2016 <0.62 7.0 7.6 288 61.6 <0.52 229 67.4 23.3 97.4 20.3 105 2.7 44.3 J10/6/2016 <0.25 NA NA 46.0 NA NA NA NA 5.5 NA NA 17.7 0.64 J NA8/9/2017 <0.25 7.0 <0.38 37.9 18.3 <0.21 48.1 31.8 0.86 J 53.9 12.9 5.0 0.52 J ND8/8/2018 <0.25 <0.41 <0.38 2.5 2.4 <0.21 5.2 1.7 0.39 J 5.9 1.2 3.3 <0.23 ND8/7/2019 <0.15 9.1 <0.20 20.1 64.1 <0.28 110 34.2 5.1 115 31.4 33.7 4.4 33.58/6/2020 <0.15 1.0 <0.20 0.68 J 3.2 <0.28 21.0 <0.18 0.49 J 13.7 4.4 8.9 0.56 J 0.39 J8/23/2021 <0.34 <0.49 <0.40 <0.30 <0.33 <0.42 3.6 <0.34 <0.48 <0.50 <0.33 <0.71 <0.34 ND8/20/2012 463 20.7 <0.76 158 106 1.6 J 387 183 15.7 392 79.2 92.3 3.6 ND8/14/2013 68.6 <0.41 <0.38 51.8 24.2 <0.21 119 46.3 3.1 40.7 19.0 10.4 0.67 J 1.3 J3/11/2014 308 <0.41 9.6 149 90.7 0.79 J 549 136 15.4 29.4 29.3 21.8 2.6 17.68/14/2014 182 <0.41 <0.38 124 52.8 0.74 J 479 80.8 10.0 112 86.7 31.2 1.9 11.08/5/20158/1/2016 124 6.8 12.9 989 126 <1.0 991 208 59.9 32.8 16.5 138 3.4 J 9.2 J10/6/2016 176 NA NA 405 NA NA NA NA 36.9 NA NA 36.2 1.4 J NA11/23/2016 233 NA NA 878 NA NA NA NA 41.3 NA NA 134 4.4 J NA3/2/2017 120 <4.1 <3.8 951 108 8.4 J 918 167 38.1 45.0 13.9 204 5.0 J 18.8 J4/26/2017 118 NA NA 464 NA NA NA NA 17.7 NA NA 59.5 2.6 J NA8/9/2017 107 <2.0 <1.9 322 37.1 <1.0 829 43.4 13.1 <1.6 36.3 43.1 2.4 J ND3/7/2018 121 NA NA 647 NA NA NA NA 9.8 NA NA 45.7 6.3 NA5/23/2018 36.4 NA NA 331 NA NA NA NA 1.5 J NA NA 21.6 4.1 J NA8/8/2018 76.2 <0.82 <0.76 111 16.7 <0.42 222 26.5 2.9 <0.62 10.3 8.4 2.1 75.52/5/2019 77.0 NA NA 556 NA NA NA NA 22.9 NA NA74717.8 NA8/6/2020 29.8 <0.47 <0.40 64.2 11.9 <0.55 273 25.6 2.0 32.8 9.021.93.0 ND8/22/2021 13.1 <0.49 <0.40 6.3<0.33<0.42 50.9 <0.34 <0.48 2.4 7.711.7<0.34 NDNotes are provided on the final page of this table. KMW-8TYPE II MONITORING WELLS (Continued)COULD NOT SAMPLE - WELL WAS DRYKMW-12KMW-9RPage 3 of 7
Table 2Groundwater Results, 2012-2021Loading Rack AreaFormer FHR North TerminalWilmington, North CarolinaSample ID Date Collected170 70 600 70 20670 600 400 400Variesm/p-Xyleneso-XyleneAll Other 8260B AnalytesGroundwater Clean-up Goal (ug/L)500Methyl Tert Butyl Ether (MTBE)Naphthalenen-PropylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneContaminant of ConcernBenzenen-Butylbenzenesec-ButylbenzeneEthylbenzeneIsopropylbenzene (Cumene)8/20/2012 <50.0 <82.0 <76.0 <60.0 <80.0 <42.0 <48.0 <84.0 <52.0 134 J <72.060,500119 J ND8/14/2013 <50.0 <82.0 <76.0 256 <80.0 <42.0 549 <84.0 <52.0 195 J <72.073,70086.5 J 5103/11/2014 137 J <102 <95.0 336 <100 <52.5 2,270 180 J 309 217 J <90.063,600178 J 48.2 J8/14/2014 54.5 J <41.0 <38.0 99.6 J <40.0 <21.0 58.1 J <42.0 71.6 J 134 <36.025,70025.9 J 33.2 J3/11/2015 38.5 J <51.2 <47.5 328 <50.0 <26.2 163 <52.5 <32.5 222 <45.090,90049.9 J ND8/5/2015 <62.5 <102 <95.0 271 <100 <52.5 326 <105 <65.0 229 J <90.066,400<57.5 ND8/2/2016 <25.0 <41.0 <38.0 132 <40.0 <21.0 193 <42.0 <26.0 202 38.4J21,300<23.0 ND10/6/2016 <12.5 NA NA 107 NA NA NA NA 16.4 J NA NA 13,800 <11.5 NA11/23/2016 25.7 J NA NA 244 NA NA NA NA 34.5 J NA NA 20,400 <23.0 NA3/2/2017 <12.5 <20.5 <19.0 57.5 65.9 <10.5 242 81.8 20.8 J 997 210 4,370 <11.5 ND4/26/2017 <12.5 NA NA 82.2 NA NA NA NA 18.9 J NA NA 11,400 <11.5 NA8/29/2017 0.38 J <0.41 <0.38 0.46 J 0.73 J <0.21 1.7 0.69 J 0.32 J 1.6 <0.36 92.7 0.35 J 18.25 J3/12/2018 <25.0 NA NA 83.2 J NA NA NA NA <26.0 NA NA 11,200 <23.0 NA5/23/2018 <10.0 NA NA 63.8 NA NA NA NA <10.4 NA NA 9,330 <9.2 NA8/8/2018 1.7<0.41 <0.383.6 4.2<0.216.3 4.8 0.67 J 8.9 <0.36 379 0.88 J 9.0 J2/5/2019 3.6 JNANA40.1NANANANA<1.2NANA1,3402.3 J NA8/7/2019 1.5 J0.58 0.50 19.7 11.1 <0.69 47.0 16.4 <0.61 81.7 11.59051.0 J 45.5 J8/6/2020 3.42.2 J <0.50 17.6 27.4 <0.69 63.5 41.9 <0.61 61.3 14.66021.6 J ND8/23/2021 <0.86<1.2 2.6 6.4 15.6 <1.1 22.1 22.8 <1.2 5.4 <0.83704<0.84 20.98/20/2012 <1.2 <2.0 <1.9 <1.5 <2.0 <1.0 2.7 J <2.1 <1.3 <1.6 <1.82,9901.6 J ND8/14/2013 <2.5 <4.1 <3.8 8.9 J <4.0 <2.1 9.7 J <4.2 <2.6 8.0 J <3.66,430<2.3 26.93/11/2014 <0.25 <0.41 <0.38 <0.30 <0.40 0.21 J 0.43 J <0.42 <0.26 <0.31 <0.362.4<0.23 1.26 J8/14/2014 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 0.43 J <0.42 <0.26 <0.31 <0.36114<0.23 ND3/11/2015 <0.25 <0.41 <0.38 0.67 J <0.40 <0.21 0.73 J <0.42 <0.26 0.52 J <0.362960.46 J 3.08/5/2015 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.364.0<0.23 ND8/1/2016 <0.25 <0.41 <0.38 0.94 J <0.40 <0.21 0.84 J <0.42 <0.26 2.6 0.76 J15.70.78 J ND8/9/2017 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36<0.66<0.23 ND8/7/2018 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.3612.1<0.23 ND8/7/2019 <0.15 <0.23 <0.20 <0.26 <0.20 <0.28 <0.35 <0.18 <0.24 <0.17 <0.200.89 J<0.22 ND8/6/2020 <0.15 <0.23 <0.20 <0.26 <0.20 <0.28 <0.35 <0.18 <0.24 <0.17 <0.20167<0.22 ND8/22/2021 <0.34 <0.49 <0.40 <0.30 <0.33 <0.42 <0.64 <0.34 <0.48 <0.50 <0.33<0.71<0.34 ND8/17/2012 <0.25 <0.41 <0.38 <0.30 <0.40 0.54 J <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 0.20 J8/13/2013 1.8 <0.41 <0.38 0.31 J 0.79 J 0.87 J <0.24 <0.42 <0.26 <0.31 <0.36 0.88 J <0.23 10.6 J8/21/2014 2.7 <0.41 <0.38 <0.30 1.1 0.93 J 0.25 J 0.49 J 0.28 J 2.2 0.73 J 6.4 0.26 J 2.4 J3/11/2015 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 0.35 J <0.42 <0.26 0.31 J <0.36 <0.66 <0.23 0.71 J8/5/2015 <0.25 <0.41 <0.38 <0.30 <0.40 0.44 J <0.24 <0.42 <0.26 <0.31 <0.36 0.70 J <0.23 0.73 J8/1/2016 5.3 <0.41 <0.38 0.87 J 2.9 0.89 J 2.1 2.7 0.71 J 3.3 0.82 J 5.4 0.43 J 1.73 J8/7/2017 6.7 <0.41 <0.38 0.77 J 6.5 0.69 J 4.0 6.6 0.87 J <0.31 <0.36 3.7 <0.23 0.16 J8/8/2018 2.8 <0.41 <0.38 8.0 4.9 0.70 J 4.0 4.6 0.79 J 16.9 <0.36 24.7 0.46 J ND8/7/2019 <0.15 <0.23 0.65 J <0.26 5.5 1.2 0.73 J <0.18 <0.24 <0.17 5.1 2.3 <0.22 2.78/6/2020 <0.15 <0.23 <0.20 <0.26 <0.20 0.32 J <0.35 <0.18 <0.24 <0.17 <0.20 8.9 <0.22 ND8/21/2021 <0.34 <0.49 <0.40 <0.30 <0.33 <0.42 <0.64 <0.34 <0.48 <0.50 <0.33 <0.71 <0.34 NDNotes are provided on the final page of this table. KMW-13TYPE II MONITORING WELLS (Continued)KMW-18KMW-14Page 4 of 7
Table 2Groundwater Results, 2012-2021Loading Rack AreaFormer FHR North TerminalWilmington, North CarolinaSample ID Date Collected170 70 600 70 20670 600 400 400Variesm/p-Xyleneso-XyleneAll Other 8260B AnalytesGroundwater Clean-up Goal (ug/L)500Methyl Tert Butyl Ether (MTBE)Naphthalenen-PropylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneContaminant of ConcernBenzenen-Butylbenzenesec-ButylbenzeneEthylbenzeneIsopropylbenzene (Cumene)8/20/2012 1.5 <0.41 <0.38 10.6 1.0 <0.21 <0.24 <0.42 0.60 J 0.99 J 1.02.215.2 1.2 J8/14/2013 <0.25 <0.41 <0.38 4.0 <0.40 <0.21 0.46 J <0.42 <0.26 <0.31 <0.361.6 J<0.23 ND8/14/2014 <0.25 <0.41 <0.38 2.7 <0.40 <0.21 0.80 J <0.42 <0.26 <0.31 <0.36<0.66<0.23 ND3/11/2015 <0.25 <0.41 <0.38 2.8 <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36<0.66<0.23 ND8/5/2015 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 0.26 J <0.42 <0.26 <0.31 <0.36<0.66<0.23 ND8/1/2016 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36<0.66<0.23 0.82 J8/8/2017 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36<0.66<0.23 ND8/8/2018 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36<0.66<0.23 0.28 J8/7/2019 <0.15 <0.23 <0.20 0.82 J <0.20 <0.28 0.37 J <0.18 0.45 J 0.65 J <0.204.81.3 ND8/6/2020 <0.15 <0.23 <0.20 <0.26 <0.20 <0.28 <0.35 <0.18 <0.24 <0.17 <0.20<0.41<0.22 ND8/21/2021 <0.34 <0.49 <0.40 <0.30 <0.33 <0.42 <0.64 <0.34 <0.48 <0.50 <0.33<0.71<0.34 ND8/21/2012 209 <41.0 <38.0 529 72.3 J <21.0 299 134 40.0 J 756 19922,000 90.3 JND8/14/2013 225 <41.0 <38.0 740 106 <21.0 421 223 33.3 J 1,110 31715,500 37.2 J3233/11/2014 71.7 <10.2 <9.5 204 19.9 J 32.1 74.2 35.2 25.8 193 54.49,500 28.4ND8/14/2014 166 <20.5 <19.0 323 81.3 <10.5 168 165 16.5 J 351 96.412,900 <11.5ND3/11/2015 245 <20.5 <19.0 513 106 <10.5 311 205 25.0 J 596 17713,300 12.7 JND8/5/2015 155 <20.5 <19.0 787 99.4 <10.5 370 203 41.7 J 1,020 30215,100 40.8 JND8/1/2016 <10.0 <16.4 <15.2 446 71.3 <8.4 217 154 57.4 1,290 3638,250 30811.7 J10/6/2016 <10.0 NA NA 405 NA NA NA NA 94.2 NA NA 11,000 251 NA8/9/2017 <6.2 26.6 <9.5 354 63.2 <5.2 172 129 33.6 823 170 6,170 182 ND8/8/2018 <2.5 <4.1 <3.8 202 25.9 <2.1 92.0 68.6 <2.6 438 92.7 2,610 58.5 16.9 J8/7/2019 22.4 <4.7 <4.0 442 57.3 <5.5 178 <3.7 20.0 717 183 7,710 351 ND8/6/2020 26.0 <5.8 <5.0 777 91.2 <6.9 463 <4.6 23.4 J 1,440 371 8,180 174 ND8/21/2021 <4.3 <6.1 <5.0 296 27.8 <5.3 150 <4.2 <6.1 404 101 3,750 57.2 ND8/22/2012 28.2 <1.6 <1.5 <1.2 7.5 8.3 20.1 6.9 3.3 J 14.7 4.6 5,150 1.6 J 21.08/14/2013 93.6 <0.41 5.6 35.4 36.2 1.1 85.6 74.0 3.4 <0.31 43.0 276 <0.23 22.0 J8/14/2014 47.8 <0.41 2.5 6.3 16.1 0.27 J 36.0 29.0 2.8 5.1 2.1 40.6 0.41 J ND3/11/2015 55.2 <0.41 <0.38 52.9 41.0 0.59 J 92.4 76.0 6.8 14.3 5.7 1,360 6.5 ND8/5/2015 25.1 6.2 3.7 23.1 19.6 <0.42 34.4 36.4 4.5 11.2 <0.72 473 0.90 J 144.88/1/2016 1.8 <0.41 0.92 J 6.8 1.9 <0.21 7.0 3.8 2.0 15.4 10.7 80.3 5.6 0.67 J10/6/2016 2.3 NA NA 8.1 NA NA NA NA 1.5 NA NA 57.1 7.1 NA8/9/2017 0.76 J <0.41 <0.38 2.2 0.84 J <0.21 3.1 2.2 <0.26 <0.31 4.1 2.5 <0.23 ND8/8/2018 2.0 <0.41 <0.38 17.3 18.3 <0.21 42.0 43.0 2.0 17.8 26.7 399 1.2 1.58 J8/7/2019 <0.30 3.5 3.7 17.5 15.1 <0.55 34.7 26.1 1.2 J 10.3 11.4 398 <0.44 ND8/6/2020 1.5 J <0.47 3.7 26.2 13.2 0.74 J 14.0 22.1 4.5 16.9 9.1 309 3.1 ND8/22/2021 <0.69 <0.98 <0.80 7.9 18.1 <0.84 38.6 28.1 2.1 37.1 14.5 353 2.6 15.3Notes are provided on the final page of this table. AMW-3AMW-2FHR TYPE II MONITORING WELLS WITHIN APEX TERMINALAMW-1Page 5 of 7
Table 2Groundwater Results, 2012-2021Loading Rack AreaFormer FHR North TerminalWilmington, North CarolinaSample ID Date Collected170 70 600 70 20670 600 400 400Variesm/p-Xyleneso-XyleneAll Other 8260B AnalytesGroundwater Clean-up Goal (ug/L)500Methyl Tert Butyl Ether (MTBE)Naphthalenen-PropylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneContaminant of ConcernBenzenen-Butylbenzenesec-ButylbenzeneEthylbenzeneIsopropylbenzene (Cumene)8/17/2012 1,730 <82.0 <76.0 3,600 215 <42.0 364 326 25,600 2,030 613 12,600 5,700 ND8/13/2013 927 <82.0 <76.0 2,990 197 J <42.0 337 242 12,500 1,590 436 11,200 5,170 6758/21/2014 796 <20.5 <19.0 3,110 215 <10.5 451 271 6,050 1,970 508 12,300 6,020 179.33/11/2015 1,120 <20.5 <19.0 3,410 <20.0 <10.5483 293 7,290 1,890 <18.0 13,400 5,960 32.1 J8/5/2015 780 <20.5 <19.0 2,030 180 <10.5 352184 5,070 1,090 <18.0 8,660 3,620 84.7 J8/1/2016 663 <41.0 <38.0 4,660 253 <21.0 505 247 12,100 1,770 480 16,300 8,350 128.1 J8/9/2017 41.9 J <20.5 <19.0 3,240 171 <10.5 327 164 9,750 1,110 <18.0 12,600 5,940 ND8/8/2018 <6.2 <10.2 <9.5 1,260 134 <5.2 410 226 3,560 1,700 426 5,410 3,040 54.9 J8/7/2019 11.9 J <0.94 <8.0 2,710 121 <11.0 341 <7.4 2,640 1,040 <7.9 9,920 5,380 41.38/6/2020 <6.0 <9.4 <8.0 2,590 144 <11.0 550 <7.4 241 1,230 <7.9 10,600 5,410 16.9 J8/21/2021 <17.2 <24.5 <20.0 2,730 250 <21.1686 <17.0 247 2,260 <16.6 11,900 5,600 ND8/20/2012 <0.25 <0.41 <0.38 <0.30 5.1 15.8 11.8 3.2 0.27 J <0.31 <0.36 0.78 J <0.23 270.88/14/2013 <0.25 <0.41 <0.38 <0.30 4.4 2.1 0.93 J 3.6 <0.26 <0.31 <0.36 1.2 J <0.23 27.88/14/2014 0.29 J <0.41 <0.38 <0.30 8.7 31.2 0.97 J 3.9 <0.26 <0.31 <0.36 1.0 J 0.36 J 154.53/11/2015 6.6 <0.41 <0.38 52.7 <0.40 29.3 2.3 2.9 14.9 1.4 <0.36 142 91.2 10.38/5/2015 <0.25 <0.41 <0.38 <0.30 <0.40 0.22 J <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 ND8/1/2016 0.26 J <0.41 0.71 J <0.30 24.1 12.0 0.68 J 26.0 0.63 J 0.33 J <0.36 2.8 0.62 J 9.48/9/2017 <0.25 <0.41 1.3 1.3 12.7 4.7 10.8 16.2 0.62 J 7.2 3.9 22.4 1.0 25.98/8/2018 <0.25 <0.41 1.1 <0.30 16.4 4.5 0.33 J 11.9 <0.26 <0.31 <0.36 1.4 J 0.34 J 2.48/7/2019 <0.15 <0.23 0.84 J <0.26 17.0 6.4 26.4 7.0 <0.24 2.1 4.5 5.1 0.39 J 4.18/6/2020 <0.15 <0.23 0.46 J <0.26 5.5 0.95 J <0.35 1.8 <0.24 <0.17 <0.20 <0.41 <0.22 5.63 J8/21/2021 <0.34 <0.49 <0.40 <0.30 18.4 6.2 <0.64 2.3 <0.48 <0.50 <0.33 <0.71 <0.34 5.93/12/2015 <0.62 <1.0 <0.95 1.2 J <1.0 86.6 6.2 <1.0 <0.65 1.2 J <0.90 <1.6 <0.58 3.3 J8/5/2015 <0.25 <0.41 <0.38 0.99 J <0.40 82.5 0.77 J <0.42 0.33 J 0.60 J <0.36 4.3 <0.23 32.8 J8/1/2016 <0.25 <0.41 <0.38 0.53 J <0.40 72.7 0.33 J <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 14.08/8/2017 <0.25 <0.41 <0.38 0.50 J <0.40 34.8 0.29 J <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 6.38/8/2018 <0.25 <0.41 <0.38 <0.30 <0.40 1.7 <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 0.35 J8/7/2019 <0.15 <0.23 <0.20 <0.26 <0.20 12.1 <0.35 <0.18 <0.24 <0.17 <0.20 <0.41 <0.22 ND8/6/2020 <0.15 <0.23 <0.20 <0.26 <0.20 13.7 0.59 J <0.18 <0.24 <0.17 <0.20 3.0 <0.22 ND8/23/2021 <0.34 <0.49 <0.40 <0.30 <0.33 7.6 <0.64 <0.34 <0.48 <0.50 <0.33 <0.71 <0.34 NDNotes are provided on the final page of this table. AMW-4FHR TYPE II MONITORING WELLS WITHIN APEX TERMINAL (Continued)TYPE III MONITORING WELLSKDW-1AMW-5Page 6 of 7
Table 2Groundwater Results, 2012-2021Loading Rack AreaFormer FHR North TerminalWilmington, North CarolinaSample ID Date Collected170 70 600 70 20670 600 400 400Variesm/p-Xyleneso-XyleneAll Other 8260B AnalytesGroundwater Clean-up Goal (ug/L)500Methyl Tert Butyl Ether (MTBE)Naphthalenen-PropylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneContaminant of ConcernBenzenen-Butylbenzenesec-ButylbenzeneEthylbenzeneIsopropylbenzene (Cumene)3/11/2014 <0.25 <0.41 <0.38 <0.30 <0.40 37.0 <0.24 <0.42 <0.26 <0.31 <0.3612.8<0.23 ND4/9/2014 <0.25 <0.41 <0.38 <0.30 <0.40 28.3 <0.24 <0.42 <0.26 <0.31 <0.362.2<0.23 ND5/20/2014 <0.25 <0.41 <0.38 <0.30 <0.40 23.8 <0.24 <0.42 <0.26 <0.31 <0.361.3 J<0.23 ND8/14/2014 <0.25 <0.41 <0.38 <0.30 <0.40 21.2 <0.24 <0.42 <0.26 <0.31 <0.36<0.66<0.23 ND10/23/2014 <0.25 <0.41 <0.38 <0.30 <0.40 37.8 <0.24 <0.42 <0.26 <0.31 <0.36<0.66<0.23 ND3/12/2015 <0.25 <0.41 <0.38 <0.30 <0.40 42.0 <0.24 <0.42 <0.26 <0.31 <0.360.87 J<0.23 ND8/5/2015 <0.25 <0.41 <0.38 <0.30 <0.40 22.6 <0.24 <0.42 <0.26 <0.31 <0.360.73 J<0.23 3.9 J8/1/2016 <0.25 <0.41 <0.38 <0.30 <0.40 27.9 <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 ND8/9/2017 <0.25 <0.41 <0.38 <0.30 <0.40 9.9 0.61 J <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 ND8/7/2018 <0.25 <0.41 <0.38 <0.30 <0.40 19.7 <0.24 <0.42 <0.26 <0.31 <0.36 0.82 J <0.23 ND8/7/2019 <0.15 <0.23 <0.20 2.0 <0.20 12.5 1.4 <0.18 0.95 J 1.5 0.48 J 10.1 3.8 ND8/6/2020 <0.15 <0.23 <0.20 <0.26 <0.20 6.2 <0.35 <0.18 <0.24 <0.17 <0.20 <0.41 <0.22 ND8/22/2021 <0.34 <0.49 <0.40 <0.30 <0.33 12.5 <0.64 <0.34 <0.48 <0.50 <0.33 <0.71 <0.34 NDNotes:1. All results in micrograms per liter (ug/L).2. Groundwater results from wells sampled in 2021 are included with the past 10 years of measurements, when applicable. Historical wells and results are presented in Appendix C. 3. Shaded concentrations exceed the 15A North Carolina Administrative Code (NCAC) 2L.0202 North Carolina Groundwater Quality Standard (2L GWQS), updated April 1, 2013. 4. Refer to laboratory reports for other 8260 analytes detected.5. J = Value is estimated concentration that is less than RL, but greater than or equal to the MDL.7. October/November 2016, April 2017 and February 2019 data is from post EAB sampling events and select samples from these events were analyzed via EPA Method 8260B for BTEX constituents only.8. March 2017 data is from a post EAB sampling event and samples were analyzed for the full 8260 list.6. NA = Not Analyzed; ND = Not Detected.FHR TYPE III MONITORING WELLS WITHIN APEX TERMINALADW-1Page 7 of 7

FIGURES

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Project No.:
Drawn By:11/11/2021 10:15:35 AM - P:\PROJECTS\GEORGIA-PACIFIC\SITE MANAGEMENT PROGRAM\SITE FILES\WILMINGTON, NC\CAD\FIGURE 1 - SITE LOCATION.DWG - MAHONY, MATTBar Measures 1 inch Copyright: Tetra Tech805 E 20TH STREETCHARLOTTE, NC 734.213.4079
FORMER NORTH TERMINAL - LOADING RACK
WILMINGTON, NORTH CAROLINA
N 0
SCALE:
1250' 2500'
1" = 1250'
= APPROXIMATE SITE BOUNDARIES
DRS
MEM
117-4124SMP4310
FIGURE1
NEW HANOVER COUNTY,NORTH CAROLINA
SITE
RIVER
ROAD
SHIPYARD BLVD
CAPE FEAR RIVERFLINT HILLS RESOURCES, LP
SITE LOCATION MAP
SOURCE: GOOGLE EARTH, NOVEMBER 2019
NOTES:1) FHR = FLINT HILLS RESOURCES.2) GASOLINE FUEL OIL FACILITY (GFO) REFERS TO BOTH FORMER GASOLINE AND #2 FUEL OIL FACILITIES.
3) THE GFO FACILITY RECEIVED NO FURTHER ACTION STATUS FROM NCDEQ ON DECEMBER 2, 2019.4) SITE FEATURES AND PROPERTY BOUNDARIES ARE APPROXIMATE.www.tetratech.comProject No.:MARK DATE DESCRIPTIONBY11/11/2021 1:37:50 PM - P:\PROJECTS\GEORGIA-PACIFIC\SITE MANAGEMENT PROGRAM\SITE FILES\WILMINGTON, NC\CAD\FIGURE 1 - SITE LOCATION.DWG - MAHONY, MATTChecked By:
Drawn By:
Designed By:
Bar Measures 1 inch Copyright: Tetra Tech117-4124SMP43103325 RIVER ROADWILMINGTON, NORTH CAROLINA 28412FLINT HILLS RESOURCES, LP805 E 20TH STCHARLOTTE, NC 734.213.4079FIGURE2 NORTH TERMINAL - LOADING RACKSITE LAYOUTM. MAHONY
M. MAHONY
D. SOPOCI
0
SCALE:
100' 200'400'
1" = 200'N
APEX OIL TERMINAL
FHR WATER
TREATMENT PLANT
FORMER FHR
LOADING RACK
FORMER FHR GASOLINE
FUEL OIL FACILITY
ASTs
AMW-2 RIVER ROADRIVER ROADAST
AST
AST
AST
AST
AST
AST AST
ASTAST
ASTAST
AST
SYSTEM
POND
POND
POND
TANK
STORAGE
STORAGESTORAGE
OFFICEOFFICEOFFICE
APEXLOADINGRACKS
STORMWATERPOND
NC STATE AUTHORITY PROPERTY
CHEMSERVE
APEX OIL PROPERTY
APEX OIL PROPERTY
FLINT HILLS RESOURCES PROPERTYAPEX OIL PROPERTY
PROPERTYFLINT HILLS RESOURCES
WATER TREATMENT SYSTEM
OFFICE
AMW-3
KMW-3 KMW-1
KMW-5
KMW-7
AMW-1
KMW-12
KMW-6 KMW-15
AMW-6
KMW-18
ADW-1
KDW-1
KMW-9R
AMW-4
CHEMSERVELOADINGRACKS
KMW-6
KMW-13
KMW-14
AMW-5
KMW-8
LEGEND
MONITORING WELL
MONITORING WELL (NOT SAMPLED)
ABOVEGROUND STORAGE TANK
BUILDING NOTES:1) MONITORING WELLS WERE INSTALLED AND SURVEYED BY PREVIOUS CONSULTANTS.2) ADDITIONAL MONITORING WELLS WHICH WERE NOT SAMPLED IN 2021 WERE INCLUDEDIN THE MAP AREA IF THEY HAD BEEN SAMPLED IN THE PAST 10 YEARS.
3) SITE FEATURES AND PROPERTY BOUNDARIES ARE APPROXIMATE.
PROPERTY BOUNDARIES
RAILROAD TRACKS
ROAD / PARKING LOTAST www.tetratech.comProject No.:MARK DATE DESCRIPTIONBY11/23/2021 2:35:06 PM - P:\PROJECTS\GEORGIA-PACIFIC\SITE MANAGEMENT PROGRAM\SITE FILES\WILMINGTON, NC\CAD\MASTER LOADING RACK V1.1.DWG - MAHONY, MATTChecked By:
Drawn By:
Designed By:
Bar Measures 1 inch Copyright: Tetra Tech117-4124SMP43103325 RIVER ROADWILMINGTON, NORTH CAROLINA 28412FLINT HILLS RESOURCES, LPFIGURE3 NORTH TERMINAL - LOADING RACKSITE FEATURESM. MAHONY
M. MAHONY
D. SOPOCI
0
SCALE:
45' 90'180'
1" = 90'N 805 E 20TH STCHARLOTTE, NC 734.213.4079
ASTs
AMW-2 RIVER ROADRIVER ROADAST
AST
AST
AST
AST
AST
AST AST
ASTAST
ASTAST
AST
SYSTEM
POND
POND
POND
TANK
STORAGE
STORAGESTORAGE
OFFICEOFFICEOFFICE
APEXLOADINGRACKS
STORMWATERPOND
NC STATE AUTHORITY PROPERTY
CHEMSERVE
APEX OIL PROPERTY
APEX OIL PROPERTY
FLINT HILLS RESOURCES PROPERTYAPEX OIL PROPERTY
PROPERTY
OFFICE
AMW-3
KMW-3 KMW-1
KMW-5
KMW-7
AMW-1
KMW-12
AMW-6
KMW-18
ADW-1
KDW-1
KMW-9R
AMW-4
*
*13.014.015.012.011.010.09.08.07.016.018.020.022.024.0CHEMSERVELOADINGRACKS
KMW-6
KMW-13
(13.61 ft)(15.23 ft)15.50 ft)(24.17 ft)
(24.20 ft)
(23.48 ft)
(24.17 ft)KMW-8
(15.96 ft)KMW-14
(16.05 ft)
(14.99 ft)
(10.59 ft)
(8.82 ft)
(9.92 ft)(6.21 ft)AMW-5 (14.00 ft)
(15.56 ft)
LEGEND
NOTES:1) ELEVATIONS ARE BASED ON NORTH AMERICAN VERTICAL DATUM (NAVD '88) BASEPOINT.2) STATIC GROUNDWATER MEASUREMENTS WERE RECORDED AUGUST 20, 2021.
3) *STATIC WATER LEVELS IN TYPE III WELLS WERE NOT USED TO CREATE POTENTIOMETRIC SURFACE CONTOURS.3) POTENTIOMETRIC SURFACE CONTOURS ARE CONSISTENT WITH THOSE PRESENTED IN PREVIOUS REPORTS.4) CONTOURS CREATED USING SURFER 16.0 WITH DEFAULT KRIGING SETTINGS.
5) MONITORING WELLS WERE INSTALLED AND SURVEYED BY PREVIOUS CONSULTANTS.6) SITE FEATURES AND PROPERTY BOUNDARIES ARE APPROXIMATE.
MONITORING WELL
ABOVEGROUND STORAGE TANK
BUILDING
PROPERTY BOUNDARIES
RAILROAD TRACKS
ROAD / PARKING LOT
ELEVATION CONTOUR(1 FOOT INTERVAL)
AST
15.0 www.tetratech.comProject No.:MARK DATE DESCRIPTIONBY11/23/2021 1:51:45 PM - P:\PROJECTS\GEORGIA-PACIFIC\SITE MANAGEMENT PROGRAM\SITE FILES\WILMINGTON, NC\CAD\MASTER LOADING RACK V1.1.DWG - MAHONY, MATTChecked By:
Drawn By:
Designed By:
Bar Measures 1 inch Copyright: Tetra Tech117-4124SMP43103325 RIVER ROADWILMINGTON, NORTH CAROLINA 28412FLINT HILLS RESOURCES, LPFIGURE4NORTH TERMINAL - LOADING RACKGROUNDWATER ELEVATIONCONTOURS, AUGUST 2021M. MAHONY
M. MAHONY
D. SOPOCI
0
SCALE:
45'90'180'
1" = 90'
N 805 E 20TH STCHARLOTTE, NC 734.213.4079
ASTsRIVER ROADRIVER ROADAST
AST
AST
AST
AST
AST
AST AST
ASTAST
ASTAST
AST
SYSTEM
POND
POND
POND
TANK
STORAGE
STORAGESTORAGE
OFFICEOFFICEOFFICE
STORMWATERPOND
NC STATE AUTHORITY PROPERTY
CHEMSERVE
APEX OIL PROPERTY
APEX OIL PROPERTY
APEX OIL PROPERTY
PROPERTY
OFFICE
CHEMSERVELOADINGRACKS
AMW-1
Benzene <0.34
Ethylbenzene <0.30
MTBE <0.42
Naphthalene <0.64
Toluene <0.48
Total xylenes <0.71
ADW-1
Benzene <0.34
Ethylbenzene <0.30
MTBE 12.5
Naphthalene <0.64
Toluene <0.48
Total xylenes <0.71
AMW-2
Benzene <4.3*
Ethylbenzene 296
MTBE <5.3
Naphthalene 150
Toluene <6.1
Total xylenes 3,807
AMW-3
Benzene <0.69
Ethylbenzene 7.9
MTBE <0.84
Naphthalene 38.6
Toluene 2.1
Total xylenes 355
AMW-4
Benzene <17.2*
Ethylbenzene 2,730
MTBE <21.1*
Naphthalene 686
Toluene 247
Total xylenes 17,500
AMW-5
Benzene <0.34
Ethylbenzene <0.30
MTBE 6.2
Naphthalene <0.64
Toluene <0.48
Total xylenes <0.71
KDW-1
Benzene <0.34
Ethylbenzene <0.30
MTBE 7.6
Naphthalene <0.64
Toluene <0.48
Total xylenes <0.71
KMW-1
Benzene <0.34
Ethylbenzene <0.30
MTBE <0.42
Naphthalene <0.64
Toluene <0.48
Total xylenes <0.71
KMW-3
Benzene 8.0
Ethylbenzene <0.30
MTBE <0.42
Naphthalene <0.64
Toluene 1.6
Total xylenes <0.71
KMW-5
Benzene <0.34
Ethylbenzene <0.30
MTBE <0.42
Naphthalene <0.64
Toluene <0.48
Total xylenes <0.71
KMW-6
Benzene <8.6*
Ethylbenzene <7.6
MTBE <10.6
Naphthalene <16.1*
Toluene <12.1
Total xylenes 7,120
KMW-7
Benzene <0.34
Ethylbenzene <0.30
MTBE <0.42
Naphthalene <0.64
Toluene <0.48
Total xylenes <0.71
KMW-8
Benzene 44.9
Ethylbenzene 9.1
MTBE <0.42
Naphthalene 6.4
Toluene <0.48
Total xylenes 5.7
KMW-9R
Benzene <0.34
Ethylbenzene <0.30
MTBE <0.42
Naphthalene 3.6
Toluene <0.48
Total xylenes <0.71
KMW-12
Benzene 13.1
Ethylbenzene 6.3
MTBE <0.42
Naphthalene 50.9
Toluene <0.48
Total xylenes 11.7
KMW-13
Benzene <0.86
Ethylbenzene 6.4
MTBE <1.1
Naphthalene 22.1
Toluene <1.2
Total xylenes 704
KMW-14
Benzene <0.34
Ethylbenzene <0.30
MTBE <0.42
Naphthalene <0.64
Toluene <0.48
Total xylenes <0.71
KMW-18
Benzene <0.34
Ethylbenzene <0.30
MTBE <0.42
Naphthalene <0.64
Toluene <0.48
Total xylenes <0.71
FLINT HILLS RESOURCES PROPERTY
APEXLOADINGRACKS
LEGEND
NOTES:1) DATA ARE PRESENTED IN MICROGRAMS PER LITER (UG/L). METHOD DETECTION LIMITS INCLUDED FOR NON-DETECT ANALYSES..2) * = REPORTING LIMIT EXCEEDS APPLICABLE GROUNDWATER STANDARD.
2) MTBE = METHYL-TERT-BUTYL ETHER.3) GROUNDWATER RESULTS COMPARED TO NORTH CAROLINA DEPARTMENT OF ENVIRONMENTALQUALITY 15A NCAC 02L .0202 GROUNDWATER STANDARD (2L GWQS), APRIL 1, 2013.
4) MONITORING WELLS SAMPLED BY TETRA TECH BETWEEN AUGUST 21-23, 2021.5) MONITORING WELLS WERE INSTALLED AND SURVEYED BY PREVIOUS CONSULTANTS.6) SITE FEATURES AND PROPERTY BOUNDARIES ARE APPROXIMATE.
MONITORING WELL RESULTS
BELOW STANDARDS
MONITORING WELL RESULTSEXCEEDING STANDARDS
ABOVEGROUND STORAGE TANK
BUILDING
PROPERTY BOUNDARIES
RAILROAD TRACKS
ROAD / PARKING LOTAST www.tetratech.comProject No.:MARK DATE DESCRIPTIONBY11/23/2021 1:34:46 PM - P:\PROJECTS\GEORGIA-PACIFIC\SITE MANAGEMENT PROGRAM\SITE FILES\WILMINGTON, NC\CAD\MASTER LOADING RACK V1.1.DWG - MAHONY, MATTChecked By:
Drawn By:
Designed By:
Bar Measures 1 inch Copyright: Tetra Tech117-4124SMP43103325 RIVER ROADWILMINGTON, NORTH CAROLINA 28412FLINT HILLS RESOURCES, LPFIGURE5NORTH TERMINAL - LOADING RACKGROUNDWATER RESULTSVOC DETECTIONSM. MAHONY
M. MAHONY
D. SOPOCI
0
SCALE:
45' 90'180'
1" = 90'
N
2L GWQS
Benzene 1
Ethylbenzene 600
MTBE 20
Naphthalene 6
Toluene 600
Total xylenes 500 805 E 20TH STCHARLOTTE, NC 734.213.4079
APPENDICES

Appendix A

Historical Groundwater Elevations

Appendix A
Historical Groundwater Elevation Measurements
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
DATA POINT DATE DATA
COLLECTED
TOP OF
CASING
ELEVATION
(in feet)
DEPTH TO
WATER
BELOW TOC
(in feet)
FREE PHASE
PRODUCT
THICKNESS
(in feet)
SPECIFIC
GRAVITY
ADJUSTMENT
WATER
TABLE
ELEVATION
(in feet)
2/27/2002 8.03 NMT NA 11.59
2/28/2003 7.58 NMT NA 12.04
9/16/2003 7.26 NMT NA 12.36
2/19/2004 6.28 NMT NA 13.34
8/3/2004 6.28 NMT NA 13.34
2/16/2005 7.54 NMT NA 12.08
8/17/2005 5.60 NMT NA 14.02
9/21/2005 3.70 NMT NA 15.92
9/22/2005 3.79 NMT NA 15.83
2/8/2006 5.54 NMT NA 14.08
8/2/2006 6.54 NMT NA 13.08
2/5/2007 5.37 NMT NA 14.25
3/30/2007 6.60 NMT NA 13.02
8/8/2007 6.76 NMT NA 12.86
8/17/2007 7.06 NMT NA 12.56
2/20/2008 6.86 NMT NA 12.76
8/14/2008 7.04 NMT NA 12.58
2/12/2009 7.43 NMT NA 12.19
5/13/2009 7.74 NMT NA 11.88
8/17/2009 7.20 NMT NA 12.42
11/18/2009 6.75 NMT NA 12.87
5/13/2010 6.82 NMT NA 12.80
8/10/2010 7.00 NMT NA 12.62
10/14/2010 3.88 NMT NA 15.74
11/17/2010 5.22 NMT NA 14.40
2/16/2011 5.91 NMT NA 13.71
2/23/2011 6.05 NMT NA 13.57
5/26/2011 7.14 NMT NA 12.48
8/15/2011 7.43 NMT NA 12.19
11/29/2011 6.54 NMT NA 13.08
3/1/2012 7.18 NMT NA 12.44
5/22/2012 7.77 NMT NA 11.85
8/13/2012 6.08 NMT NA 13.54
10/3/2012 6.83 NMT NA 12.79
1/10/2013 6.54 NMT NA 13.08
4/18/2013 6.11 NMT NA 13.51
7/23/2013 5.17 NMT NA 14.45
8/7/2013 5.45 NMT NA 14.17
10/31/2013 6.58 NMT NA 13.04
2/13/2014 7.06 NMT NA 12.56
5/15/2014 6.15 NMT NA 13.47
8/14/2014 2.80 NMT NA 16.82
3/11/2015 5.53 NMT NA 14.09
8/5/2015 5.61 NMT NA 12.94
8/1/2016 5.59 NMT NA 12.96
8/7/2017 5.35 NMT NA 13.20
8/9/2017 4.00 NMT NA 14.55
2/7/2018 5.61 NMT NA 12.94
8/7/2019 6.85 NMT NA 11.70
8/6/2020 4.64 NMT NA 13.91
8/21/2021 4.55 NMT NA 14.00
18.55
Notes are provided on the final page of this table.
TYPE II MONITORING WELLS
KMW-1
19.62
Page 1 of 18
Appendix A
Historical Groundwater Elevation Measurements
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
DATA POINT DATE DATA
COLLECTED
TOP OF
CASING
ELEVATION
(in feet)
DEPTH TO
WATER
BELOW TOC
(in feet)
FREE PHASE
PRODUCT
THICKNESS
(in feet)
SPECIFIC
GRAVITY
ADJUSTMENT
WATER
TABLE
ELEVATION
(in feet)
2/16/2005 7.48 NMT NA 9.80
8/17/2005 5.95 NMT NA 11.33
9/21/2005 3.63 NMT NA 13.65
9/22/2005 3.88 NMT NA 13.40
10/11/2005 2.41 NMT NA 14.87
10/14/2005 2.84 NMT NA 14.44
2/8/2006 5.71 NMT NA 11.57
8/2/2006 6.67 NMT NA 10.61
2/5/2007 5.78 NMT NA 11.50
3/30/2007 6.72 NMT NA 10.56
8/8/2007 6.90 NMT NA 10.38
8/17/2007 7.21 NMT NA 10.07
2/20/2008 6.97 NMT NA 10.31
8/14/2008 6.89 NMT NA 10.39
2/12/2009 7.38 NMT NA 9.90
5/13/2009 7.69 NMT NA 9.59
8/17/2009 7.18 NMT NA 10.10
11/18/2009 6.75 NMT NA 10.53
5/13/2010 7.01 NMT NA 10.27
8/10/2010 6.98 NMT NA 10.30
10/14/2010 4.01 NMT NA 13.27
2/16/2011 6.04 NMT NA 11.24
5/26/2011 7.28 NMT NA 10.00
8/15/2011 7.19 NMT NA 10.09
8/13/2012 5.80 NMT NA 11.48
10/3/2012 6.68 NMT NA 10.60
1/10/2013 6.57 NMT NA 10.71
4/18/2013 6.04 NMT NA 11.24
7/23/2013 5.19 NMT NA 12.09
8/7/2013 5.38 NMT NA 11.90
10/31/2013 6.53 NMT NA 10.75
2/13/2014 6.87 NMT NA 10.41
5/15/2014 6.23 NMT NA 11.05
8/14/2014 2.13 NMT NA 15.15
8/5/2015
2/7/2018 5.67 NMT NA 10.66
KMW-2
16.33 NM
17.28
Notes are provided on the final page of this table.
TYPE II MONITORING WELLS (Continued)
Page 2 of 18
Appendix A
Historical Groundwater Elevation Measurements
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
DATA POINT DATE DATA
COLLECTED
TOP OF
CASING
ELEVATION
(in feet)
DEPTH TO
WATER
BELOW TOC
(in feet)
FREE PHASE
PRODUCT
THICKNESS
(in feet)
SPECIFIC
GRAVITY
ADJUSTMENT
WATER
TABLE
ELEVATION
(in feet)
2/27/2002 6.33 NMT NA 8.30
2/28/2003 5.68 NMT NA 8.95
9/16/2003 5.59 NMT NA 9.04
2/19/2004 5.00 NMT NA 9.63
8/3/2004 4.67 NMT NA 9.96
2/16/2005 6.08 NMT NA 8.55
8/17/2005 5.42 NMT NA 9.21
9/21/2005 5.10 2.02 0.77 11.09
9/22/2005 5.04 1.36 0.77 10.64
10/11/2005 1.39 1.43 0.77 14.34
10/14/2005 4.37 0.96 0.77 11.00
11/21/2005 4.12 0.26 0.77 10.71
11/28/2005 4.75 0.10 0.77 9.96
12/8/2005 4.78 0.28 0.77 10.07
12/28/2005 4.65 0.38 0.77 10.27
2/8/2006 4.88 0.16 0.77 9.87
8/2/2006 5.42 NMT NA 9.21
2/5/2007 4.95 NMT NA 9.68
3/30/2007 6.03 NMT NA 8.60
8/8/2007 5.86 NMT NA 8.77
8/17/2007 6.20 NMT NA 8.43
2/20/2008 5.33 NMT NA 9.30
8/14/2008 5.48 NMT NA 9.15
2/12/2009 4.92 NMT NA 9.71
5/13/2009 5.92 NMT NA 8.71
8/17/2009 5.57 NMT NA 9.06
11/18/2009 5.03 NMT NA 9.60
5/13/2010 5.85 NMT NA 8.78
8/10/2010 5.67 NMT NA 8.96
10/14/2010 3.76 NMT NA 10.87
2/16/2011 5.00 NMT NA 9.63
5/26/2011 6.10 NMT NA 8.53
8/15/2011 5.70 NMT NA 8.93
8/13/2012 4.13 NMT NA 10.50
10/3/2012 5.40 NMT NA 9.23
1/10/2013 5.32 NMT NA 9.31
4/18/2013 4.85 NMT NA 9.78
7/23/2013 4.47 NMT NA 10.16
8/7/2013 4.49 NMT NA 10.14
10/31/2013 5.14 NMT NA 9.49
2/13/2014 4.95 NMT NA 9.68
5/15/2014 5.39 NMT NA 9.24
8/14/2014 2.99 NMT NA 11.64
3/11/2015 4.70 NMT NA 9.93
8/5/2015 4.28 NMT NA 9.39
8/1/2016 4.86 NMT NA 8.81
8/8/2017 4.85 NMT NA 8.82
8/9/2017 3.15 NMT NA 10.52
2/7/2018 4.50 NMT NA 9.17
8/7/2018 2.60 NMT NA 11.07
8/7/2019 5.75 NMT NA 7.92
8/6/2020 3.37 NMT NA 10.30
8/21/2021 3.75 NMT NA 9.92
KMW-3
13.67
14.63
TYPE II MONITORING WELLS (Continued)
Notes are provided on the final page of this table.
Page 3 of 18
Appendix A
Historical Groundwater Elevation Measurements
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
DATA POINT DATE DATA
COLLECTED
TOP OF
CASING
ELEVATION
(in feet)
DEPTH TO
WATER
BELOW TOC
(in feet)
FREE PHASE
PRODUCT
THICKNESS
(in feet)
SPECIFIC
GRAVITY
ADJUSTMENT
WATER
TABLE
ELEVATION
(in feet)
2/27/2002 11.42 NMT NA 8.73
2/28/2003 11.16 NMT NA 8.99
9/16/2003 10.85 NMT NA 9.30
2/19/2004 10.32 NMT NA 9.83
8/3/2004 10.12 NMT NA 10.03
2/16/2005 11.01 NMT NA 9.14
8/17/2005 10.24 NMT NA 9.91
9/21/2005 8.80 NMT NA 11.35
9/22/2005 8.92 NMT NA 11.23
10/11/2005 7.45 NMT NA 12.70
10/14/2005 8.31 NMT NA 11.84
2/8/2006 9.87 NMT NA 10.28
8/2/2006 10.39 NMT NA 9.76
2/5/2007 9.92 NMT NA 10.23
3/30/2007 10.61 NMT NA 9.54
8/8/2007 10.57 NMT NA 9.58
8/17/2007 10.80 NMT NA 9.35
2/20/2008 10.45 NMT NA 9.70
8/14/2008 10.54 NMT NA 9.61
2/12/2009 10.75 NMT NA 9.40
5/13/2009 10.97 NMT NA 9.18
8/17/2009 10.67 NMT NA 9.48
11/18/2009 10.37 NMT NA 9.78
4/21/2010 10.30 NMT NA 9.85
5/13/2010 10.53 NMT NA 9.62
8/10/2010 10.62 NMT NA 9.53
10/14/2010 8.92 NMT NA 11.23
11/17/2010 9.71 NMT NA 10.44
2/16/2011 9.97 NMT NA 10.18
2/23/2011 10.05 NMT NA 10.10
5/26/2011 10.73 NMT NA 9.42
8/15/2011 10.80 NMT NA 9.35
11/29/2011 6.36 NMT NA 13.79
3/1/2012 10.57 NMT NA 9.58
5/22/2012 10.94 NMT NA 9.21
8/13/2012 9.70 NMT NA 10.45
10/3/2012 9.77 NMT NA 10.38
1/10/2013 10.14 NMT NA 10.01
4/18/2013 9.80 NMT NA 10.35
7/23/2013 7.28 NMT NA 12.87
8/7/2013 9.48 NMT NA 10.67
10/31/2013 10.32 NMT NA 9.83
2/13/2014 10.46 NMT NA 9.69
5/15/2014 9.90 NMT NA 10.25
8/14/2014 7.88 NMT NA 12.27
8/5/2015
2/7/2018 9.60 NMT NA 9.5019.10 NM
KMW-4
20.15
TYPE II MONITORING WELLS (Continued)
Notes are provided on the final page of this table.
Page 4 of 18
Appendix A
Historical Groundwater Elevation Measurements
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
DATA POINT DATE DATA
COLLECTED
TOP OF
CASING
ELEVATION
(in feet)
DEPTH TO
WATER
BELOW TOC
(in feet)
FREE PHASE
PRODUCT
THICKNESS
(in feet)
SPECIFIC
GRAVITY
ADJUSTMENT
WATER
TABLE
ELEVATION
(in feet)
2/27/2002 3.74 NMT NA 12.55
2/28/2003 3.34 NMT NA 12.95
9/16/2003 2.90 NMT NA 13.39
2/19/2004 1.74 NMT NA 14.55
8/3/2004 1.85 NMT NA 14.44
2/16/2005 3.20 NMT NA 13.09
8/17/2005 0.90 NMT NA 15.39
2/8/2006 0.88 NMT NA 15.41
2/5/2007 0.23 NMT NA 16.06
3/30/2007 6.10 NMT NA 10.19
8/8/2007 6.73 NMT NA 13.72
8/17/2007 6.98 NMT NA 13.47
2/20/2008 7.00 NMT NA 13.45
8/14/2008 7.04 NMT NA 13.41
2/12/2009 7.30 NMT NA 13.15
5/13/2009 7.68 NMT NA 12.77
8/17/2009 7.03 NMT NA 13.42
11/18/2009 6.49 NMT NA 13.96
4/21/2010 6.08 NMT NA 14.37
5/13/2010 6.55 NMT NA 13.90
8/10/2010 6.73 NMT NA 13.72
10/14/2010 2.86 NMT NA 17.59
11/17/2010 5.48 NMT NA 14.97
2/16/2011 5.39 NMT NA 15.06
2/23/2011 5.61 NMT NA 14.84
5/26/2011 6.90 NMT NA 13.55
8/15/2011 7.32 NMT NA 13.13
11/29/2012 6.24 NMT NA 14.21
3/1/2012 7.29 NMT NA 13.16
5/22/2012 7.71 NMT NA 12.74
8/13/2012 5.78 NMT NA 14.67
10/3/2012 6.61 NMT NA 13.84
1/10/2013 6.23 NMT NA 14.22
4/18/2013 5.80 NMT NA 14.65
7/23/2013 4.60 NMT NA 15.85
8/7/2013 4.98 NMT NA 15.47
10/31/2013 6.32 NMT NA 14.13
2/13/2014 6.95 NMT NA 13.50
5/15/2014 5.30 NMT NA 15.15
8/14/2014 2.38 NMT NA 18.07
3/11/2015 5.11 NMT NA 15.34
8/5/2015 5.28 NMT NA 14.14
8/1/2016 5.14 NMT NA 14.28
8/9/2017 3.25 NMT NA 16.17
8/16/2017 3.35 NMT NA 16.07
2/7/2018 5.03 NMT NA 14.39
8/7/2018 1.55 NMT NA 17.87
8/7/2019 6.52 NMT NA 12.90
8/6/2020 4.05 NMT NA 15.37
8/21/2021 3.86 NMT NA 15.56
KMW-5*
19.42
16.29
20.45
TYPE II MONITORING WELLS (Continued)
Notes are provided on the final page of this table.
Page 5 of 18
Appendix A
Historical Groundwater Elevation Measurements
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
DATA POINT DATE DATA
COLLECTED
TOP OF
CASING
ELEVATION
(in feet)
DEPTH TO
WATER
BELOW TOC
(in feet)
FREE PHASE
PRODUCT
THICKNESS
(in feet)
SPECIFIC
GRAVITY
ADJUSTMENT
WATER
TABLE
ELEVATION
(in feet)
2/27/2002 4.82 NMT NA 20.08
2/28/2003 2.19 NMT NA 22.71
9/16/2003 2.21 NMT NA 22.69
2/19/2004 0.56 NMT NA 24.34
8/3/2004 1.38 NMT NA 23.52
2/16/2005 3.14 NMT NA 21.76
8/17/2005 1.53 NMT NA 23.37
2/8/2006 1.84 NMT NA 23.06
8/2/2006 2.56 NMT NA 22.34
2/5/2007 1.55 NMT NA 23.35
8/6/2007 2.72 NMT NA 22.18
2/20/2008 2.69 NMT NA 22.21
8/14/2008 2.85 NMT NA 22.05
8/17/2009 2.85 NMT NA 22.05
8/10/2010 2.61 NMT NA 22.29
8/18/2011 3.06 NMT NA 21.84
8/13/2012 1.37 NMT NA 23.53
8/7/2013 1.76 NMT NA 23.14
8/14/2014 1.07 NMT NA 23.83
3/11/2015 1.79 NMT NA 23.11
8/5/2015 0.98 NMT NA 23.98
8/1/2016 2.23 NMT NA 22.73
10/6/2016 1.72 NMT NA 23.24
11/23/2016 2.50 NMT NA 22.46
3/2/2017 2.32 NMT NA 22.64
4/26/2017 1.25 NMT NA 23.71
8/9/2017 0.97 NMT NA 23.99
2/7/2018 1.81 NMT NA 23.15
3/7/2018 1.91 NMT NA 23.05
5/23/2018 1.56 NMT NA 23.40
8/7/2018 0.25 NMT NA 24.71
2/5/2019 2.26 NMT NA 22.70
8/7/2019 2.85 NMT NA 22.11
8/6/2020 1.55 NMT NA 23.41
8/22/2021 1.48 NMT NA 23.48
2/27/2002 4.63 NMT NA 20.48
2/28/2003 2.03 NMT NA 23.08
9/16/2003 1.92 NMT NA 23.19
2/19/2004 0.21 NMT NA 24.90
8/3/2004 0.77 NMT NA 24.34
2/16/2005 2.69 NMT NA 22.42
8/17/2005 1.20 NMT NA 23.91
2/8/2006 1.63 NMT NA 23.48
8/2/2006 2.61 NMT NA 22.50
2/5/2007 0.81 NMT NA 24.30
8/6/2007 2.15 NMT NA 22.96
2/20/2008 2.33 NMT NA 22.78
8/14/2008 2.26 NMT NA 22.85
8/17/2009 2.39 NMT NA 22.72
8/10/2010 2.10 NMT NA 23.01
8/18/2011 2.52 NMT NA 22.59
8/13/2012 1.01 NMT NA 24.10
8/7/2013 1.20 NMT NA 23.91
8/14/2014 0.93 NMT NA 24.18
3/11/2015 1.37 NMT NA 23.74
KMW-6
24.96
KMW-7 25.11
24.90
TYPE II MONITORING WELLS (Continued)
Notes are provided on the final page of this table.
Page 6 of 18
Appendix A
Historical Groundwater Elevation Measurements
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
DATA POINT DATE DATA
COLLECTED
TOP OF
CASING
ELEVATION
(in feet)
DEPTH TO
WATER
BELOW TOC
(in feet)
FREE PHASE
PRODUCT
THICKNESS
(in feet)
SPECIFIC
GRAVITY
ADJUSTMENT
WATER
TABLE
ELEVATION
(in feet)
8/5/2015 0.96 NMT NA 24.26
8/1/2016 1.79 NMT NA 23.43
10/6/2016 1.26 NMT NA 23.96
3/2/2017 2.51 NMT NA 22.71
8/7/2017 1.61 NMT NA 23.61
8/9/2017 0.50 NMT NA 24.72
2/7/2018 1.33 NMT NA 23.89
3/7/2018 1.43 NMT NA 23.79
5/23/2018 1.10 NMT NA 24.12
8/7/2018 0.00 NMT NA 25.22
8/7/2019 2.40 NMT NA 22.82
8/6/2020 1.18 NMT NA 24.04
8/6/2020 1.02 NMT NA 24.2
2/27/2002 5.56 0.20 0.86 20.47
2/28/2003 2.41 NMT NA 23.45
9/16/2003 2.40 NMT NA 23.46
2/19/2004 0.73 NMT NA 25.13
8/3/2004 1.22 NMT NA 24.64
2/16/2005 3.18 NMT NA 22.68
8/17/2005 1.75 0.12 0.77 24.20
2/8/2006 2.15 NMT NA 23.71
8/2/2006 2.92 NMT NA 22.94
2/5/2007 1.37 0.10 0.77 24.57
8/6/2007 2.77 0.02 0.77 23.11
2/20/2008 2.82 0.07 0.77 23.09
8/14/2008 2.90 0.04 0.77 22.99
8/17/2009 2.96 NMT NA 22.90
8/10/2010 2.72 NMT NA 23.14
8/18/2011 3.17 NMT NA 22.69
8/13/2012 1.55 NMT NA 24.31
8/7/2013 1.82 NMT NA 24.04
8/14/2014 1.32 NMT NA 24.54
3/11/2015 1.86 NMT NA 24.00
8/5/2015 1.15 NMT NA 24.04
8/1/2016 2.00 NMT NA 23.19
10/6/2016 1.83 NMT NA 23.36
11/23/2016 2.40 NMT NA 22.79
3/2/2017 2.30 NMT NA 22.89
4/26/2017 1.46 NMT NA 23.73
8/9/2017 0.58 NMT NA 24.61
2/7/2018 1.51 NMT NA 23.68
3/7/2018 1.66 NMT NA 23.53
5/23/2018 1.27 NMT NA 23.92
8/7/2018 0.17 NMT NA 25.02
2/5/2019 2.36 NMT NA 22.83
8/7/2019 2.71 NMT NA 22.48
8/6/2020 1.29 NMT NA 23.90
8/22/2021 1.21 NMT NA 23.98
2/27/2002 5.08 0.15 0.86 20.78
9/16/2003 2.69 NMT NA 23.04
2/19/2004 0.95 NMT NA 24.78
8/3/2004 1.28 NMT NA 24.45
KMW-7
(cont'd)
25.86
25.22
KMW-8
25.19
KMW-9 25.73
KMW-9 was abandoned on August 11, 2004.
TYPE II MONITORING WELLS (Continued)
Notes are provided on the final page of this table.
Page 7 of 18
Appendix A
Historical Groundwater Elevation Measurements
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
DATA POINT DATE DATA
COLLECTED
TOP OF
CASING
ELEVATION
(in feet)
DEPTH TO
WATER
BELOW TOC
(in feet)
FREE PHASE
PRODUCT
THICKNESS
(in feet)
SPECIFIC
GRAVITY
ADJUSTMENT
WATER
TABLE
ELEVATION
(in feet)
2/2/2015 2.86 NMT NA 24.47
3/11/2015 3.35 NMT NA 23.98
8/5/2015 3.02 NMT NA 24.23
8/1/2016 3.81 NMT NA 23.44
10/6/2016 3.21 NMT NA 24.04
8/9/2017 2.26 NMT NA 24.99
2/7/2018 3.26 NMT NA 23.99
8/7/2018 1.80 NMT NA 25.45
8/7/2019 4.56 NMT NA 22.69
8/6/2020 3.22 NMT NA 24.03
8/23/2021 3.08 NMT NA 24.17
2/27/2002 4.87 NMT NA 20.05
2/28/2003 2.36 NMT NA 22.56
9/16/2003 2.23 NMT NA 22.69
2/19/2004 0.82 NMT NA 24.10
8/3/2004 1.06 NMT NA 23.86
2/16/2005 3.05 NMT NA 21.87
8/17/2005 1.58 NMT NA 23.34
2/8/2006 1.94 NMT NA 22.98
8/2/2006 2.49 NMT NA 22.43
2/5/2007 1.25 NMT NA 23.67
8/6/2007 2.68 NMT NA 22.24
2/20/2008 2.64 NMT NA 22.28
8/14/2008 2.85 NMT NA 22.07
8/10/2010 2.60 NMT NA 22.32
8/13/2012 1.47 NMT NA 23.45
8/14/2014 1.11 NMT NA 23.81
8/5/2015
2/7/2018 1.66 NMT NA 23.33
2/27/2002 5.70 NMT NA 21.64
2/28/2003 2.68 NMT NA 24.66
9/16/2003 2.66 NMT NA 24.68
2/19/2004 1.22 NMT NA 26.12
8/3/2004 1.6 NMT NA 25.74
2/16/2005 3.51 NMT NA 23.83
8/17/2005 1.98 NMT NA 25.36
2/8/2006 1.92 NMT NA 25.42
8/2/2006 3.26 NMT NA 24.08
2/5/2007 1.33 NMT NA 26.01
8/6/2007 3.38 NMT NA 23.96
8/14/2008 3.78 NMT NA 23.56
8/10/2010 3.32 NMT NA 24.02
8/13/2012 1.82 NMT NA 25.52
3/11/2014 2.61 NMT NA 24.73
24.99
27.33
KMW-9R
27.25
KMW-10
Could not locate during August 2014 event - presumed destroyed
NM
27.34
24.92
KMW-11
Notes are provided on the final page of this table.
TYPE II MONITORING WELLS (Continued)
Page 8 of 18
Appendix A
Historical Groundwater Elevation Measurements
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
DATA POINT DATE DATA
COLLECTED
TOP OF
CASING
ELEVATION
(in feet)
DEPTH TO
WATER
BELOW TOC
(in feet)
FREE PHASE
PRODUCT
THICKNESS
(in feet)
SPECIFIC
GRAVITY
ADJUSTMENT
WATER
TABLE
ELEVATION
(in feet)
2/27/2002 13.38 NMT NA 10.81
2/28/2003 12.27 NMT NA 11.92
9/16/2003 11.69 NMT NA 12.50
2/19/2004 10.53 NMT NA 13.66
8/3/2004 10.83 NMT NA 13.36
2/16/2005 12.18 NMT NA 12.01
8/17/2005 9.76 NMT NA 14.43
2/8/2006 9.88 NMT NA 14.31
8/2/2006 11.47 NMT NA 12.72
2/5/2007 9.45 NMT NA 14.74
8/6/2007 11.83 NMT NA 12.36
2/20/2008 12.36 NMT NA 11.83
8/14/2008 12.11 NMT NA 12.08
2/12/2009 12.56 NMT NA 11.63
5/13/2009 12.95 NMT NA 11.24
8/17/2009 12.10 NMT NA 12.09
8/10/2010 11.57 NMT NA 12.62
10/14/2010 6.27 NMT NA 17.92
2/16/2011 10.28 NMT NA 13.91
5/26/2011 12.08 NMT NA 12.11
8/18/2011 12.39 NMT NA 11.80
8/13/2012 10.71 NMT NA 13.48
10/3/2012 11.50 NMT NA 12.69
1/10/2013 11.16 NMT NA 13.03
4/18/2013 10.73 NMT NA 13.46
7/23/2013 9.02 NMT NA 15.17
8/7/2013 9.41 NMT NA 14.78
10/31/2013 11.06 NMT NA 13.13
2/13/2014 11.98 NMT NA 12.21
3/11/2014 11.36 NMT NA 12.83
5/15/2014 10.55 NMT NA 13.64
8/14/2014 6.70 NMT NA 17.49
8/5/2015 DRY NMT NA NA
8/1/2016 9.74 NMT NA 14.56
10/6/2016 7.79 NMT NA 16.51
11/23/2016 2.29 NMT NA 22.01
3/2/2017 10.90 NMT NA 13.40
4/26/2017 9.75 NMT NA 14.55
8/9/2017 8.79 NMT NA 15.51
2/7/2018 9.91 NMT NA 14.39
3/7/2018 10.15 NMT NA 14.15
5/23/2018 9.66 NMT NA 14.64
8/7/2018 4.95 NMT NA 19.35
2/5/2019 8.50 NMT NA 15.80
8/7/2019 DRY NMT NA NA
8/6/2020 9.32 NMT NA -9.32
8/22/2021 8.80 NMT NA 15.50
KMW-12
24.30
24.19
Notes are provided on the final page of this table.
TYPE II MONITORING WELLS (Continued)
Page 9 of 18
Appendix A
Historical Groundwater Elevation Measurements
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
DATA POINT DATE DATA
COLLECTED
TOP OF
CASING
ELEVATION
(in feet)
DEPTH TO
WATER
BELOW TOC
(in feet)
FREE PHASE
PRODUCT
THICKNESS
(in feet)
SPECIFIC
GRAVITY
ADJUSTMENT
WATER
TABLE
ELEVATION
(in feet)
2/27/2002 12.80 NMT NA 11.04
2/28/2003 11.82 NMT NA 12.02
9/16/2003 11.29 NMT NA 12.55
2/19/2004 10.07 NMT NA 13.77
8/3/2004 10.32 NMT NA 13.52
2/16/2005 11.74 NMT NA 12.10
8/17/2005 9.30 NMT NA 14.54
2/8/2006 5.38 NMT NA 18.46
8/2/2006 10.87 NMT NA 12.97
2/5/2007 8.41 NMT NA 15.43
8/6/2007 11.26 NMT NA 12.58
2/20/2008 11.72 NMT NA 12.12
8/14/2008 11.31 NMT NA 12.53
2/12/2009 11.93 NMT NA 11.91
5/13/2009 11.65 NMT NA 12.19
8/17/2009 11.53 NMT NA 12.31
8/10/2010 11.05 NMT NA 12.79
10/14/2010 5.81 NMT NA 18.03
2/16/2011 9.66 NMT NA 14.18
5/26/2011 11.46 NMT NA 12.38
8/18/2011 11.35 NMT NA 12.49
8/13/2012 10.02 NMT NA 13.82
10/3/2012 11.02 NMT NA 12.82
1/10/2013 10.68 NMT NA 13.16
4/18/2013 10.21 NMT NA 13.63
7/23/2013 8.63 NMT NA 15.21
8/7/2013 9.03 NMT NA 14.81
10/31/2013 10.56 NMT NA 13.28
2/13/2014 11.13 NMT NA 12.71
3/11/2014 10.83 NMT NA 13.01
5/15/2014 10.10 NMT NA 13.74
8/14/2014 6.11 NMT NA 17.73
3/11/2015 9.42 NMT NA 14.42
8/5/2015 9.85 NMT NA 14.08
8/1/2016 9.26 NMT NA 14.67
10/6/2016 6.91 NMT NA 17.02
11/23/2016 9.15 NMT NA 14.78
3/2/2017 9.51 NMT NA 14.42
4/26/2017 9.58 NMT NA 14.35
8/9/2017 6.40 NMT NA 17.53
8/29/2017 6.25 NMT NA 17.68
2/7/2018 4.50 NMT NA 19.43
3/12/2018 9.61 NMT NA 14.32
5/23/2018 8.81 NMT NA 15.12
8/7/2018 4.50 NMT NA 19.43
2/5/2019 7.42 NMT NA 16.51
8/7/2019 8.75 NMT NA 15.18
8/6/2020 8.84 NMT NA 15.09
8/22/2021 7.88 NMT NA 16.05
23.84
KMW-13
23.93
Notes are provided on the final page of this table.
TYPE II MONITORING WELLS (Continued)
Page 10 of 18
Appendix A
Historical Groundwater Elevation Measurements
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
DATA POINT DATE DATA
COLLECTED
TOP OF
CASING
ELEVATION
(in feet)
DEPTH TO
WATER
BELOW TOC
(in feet)
FREE PHASE
PRODUCT
THICKNESS
(in feet)
SPECIFIC
GRAVITY
ADJUSTMENT
WATER
TABLE
ELEVATION
(in feet)
2/27/2002 11.99 NMT NA 11.32
2/28/2003 11.13 NMT NA 12.18
9/16/2003 10.66 NMT NA 12.65
2/19/2004 9.28 NMT NA 14.03
8/3/2004 9.50 NMT NA 13.81
2/16/2005 11.07 NMT NA 12.24
8/17/2005 8.56 NMT NA 14.75
2/8/2006 8.59 NMT NA 14.72
8/2/2006 10.03 NMT NA 13.28
2/5/2007 8.09 NMT NA 15.22
8/6/2007 10.45 NMT NA 12.86
2/20/2008 10.88 NMT NA 12.43
8/14/2008 10.71 NMT NA 12.60
2/12/2009 11.14 NMT NA 12.17
5/13/2009 11.54 NMT NA 11.77
8/17/2009 10.75 NMT NA 12.56
8/10/2010 10.35 NMT NA 12.96
10/14/2010 5.44 NMT NA 17.87
2/16/2011 8.90 NMT NA 14.41
5/26/2011 10.68 NMT NA 12.63
8/18/2011 11.05 NMT NA 12.26
8/13/2012 9.24 NMT NA 14.07
10/3/2012 10.33 NMT NA 12.98
1/10/2013 9.98 NMT NA 13.33
4/18/2013 9.45 NMT NA 13.86
7/23/2013 7.94 NMT NA 15.37
8/7/2013 8.37 NMT NA 14.94
10/31/2013 9.99 NMT NA 13.32
2/13/2014 10.80 NMT NA 12.51
3/11/2014 10.13 NMT NA 13.18
5/15/2014 9.39 NMT NA 13.92
8/14/2014 5.59 NMT NA 17.72
3/11/2015 8.72 NMT NA 14.59
8/5/2015 9.02 NMT NA 14.30
8/1/2016 8.70 NMT NA 14.62
8/9/2017 7.60 NMT NA 15.72
2/7/2018 8.64 NMT NA 14.68
8/7/2018 3.98 NMT NA 19.34
8/7/2019 10.18 NMT NA 13.14
8/6/2020 7.73 NMT NA 15.59
8/22/2021 7.36 NMT NA 15.96
23.31
KMW-14
23.32
Notes are provided on the final page of this table.
TYPE II MONITORING WELLS (Continued)
Page 11 of 18
Appendix A
Historical Groundwater Elevation Measurements
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
DATA POINT DATE DATA
COLLECTED
TOP OF
CASING
ELEVATION
(in feet)
DEPTH TO
WATER
BELOW TOC
(in feet)
FREE PHASE
PRODUCT
THICKNESS
(in feet)
SPECIFIC
GRAVITY
ADJUSTMENT
WATER
TABLE
ELEVATION
(in feet)
8/17/2005 9.90 NMT NA 16.32
2/8/2006 9.56 NMT NA -9.56
8/2/2006 10.98 NMT NA -10.98
2/5/2007 9.13 NMT NA 17.09
3/30/2007 10.70 NMT NA 15.52
8/8/2007 11.42 NMT NA 14.80
8/17/2007 11.80 NMT NA 14.42
2/20/2008 12.08 NMT NA 14.14
8/14/2008 11.91 NMT NA 14.31
2/12/2009 12.16 NMT NA 14.06
5/13/2009 12.68 NMT NA 13.54
8/17/2009 11.82 NMT NA 14.40
11/18/2009 11.27 NMT NA 14.95
5/13/2010 11.25 NMT NA 14.97
8/10/2010 11.54 NMT NA 14.68
2/16/2011 10.02 NMT NA 16.20
5/26/2011 11.60 NMT NA 14.62
8/15/2011 12.17 NMT NA 14.05
8/13/2012 10.55 NMT NA 15.67
10/3/2012 11.39 NMT NA 14.83
1/10/2013 10.99 NMT NA 15.23
4/18/2013 10.58 NMT NA 15.64
7/23/2013 9.22 NMT NA 17.00
8/7/2013 9.63 NMT NA 16.59
10/31/2013 11.10 NMT NA 15.12
2/13/2014 11.87 NMT NA 14.35
3/11/2014 11.21 NMT NA 15.01
5/15/2014 10.50 NMT NA 15.72
8/14/2014 6.97 NMT NA 19.25
8/5/2015
2/7/2018 9.51 NMT NA 15.72
8/17/2005 7.21 NMT NA 22.94
2/8/2006 7.07 NMT NA 23.08
8/2/2006 8.28 NMT NA 21.87
2/5/2007 6.72 NMT NA 23.43
8/6/2007 8.57 NMT NA 21.58
2/20/2008 8.42 NMT NA 21.73
8/14/2008 9.01 NMT NA 21.14
8/17/2009 7.93 NMT NA 22.22
8/10/2010 8.60 NMT NA 21.55
8/13/2012 7.55 NMT NA 22.60
8/14/2014 5.59 NMT NA 24.56
8/5/2015
2/7/2018 6.87 NMT NA 23.38
KMW-15
25.23 NM
KMW-16
30.25 NM
30.15
26.22
Notes are provided on the final page of this table.
TYPE II MONITORING WELLS (Continued)
Page 12 of 18
Appendix A
Historical Groundwater Elevation Measurements
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
DATA POINT DATE DATA
COLLECTED
TOP OF
CASING
ELEVATION
(in feet)
DEPTH TO
WATER
BELOW TOC
(in feet)
FREE PHASE
PRODUCT
THICKNESS
(in feet)
SPECIFIC
GRAVITY
ADJUSTMENT
WATER
TABLE
ELEVATION
(in feet)
8/17/2005 7.08 NMT NA 23.48
2/8/2006 7.41 NMT NA 23.15
8/2/2006 7.88 NMT NA 22.68
2/5/2007 6.72 NMT NA 23.84
8/6/2007 8.15 NMT NA 22.41
2/20/2008 8.09 NMT NA 22.47
8/14/2008 8.28 NMT NA 22.28
8/17/2009 8.53 NMT NA 22.03
8/10/2010 8.23 NMT NA 22.33
8/13/2012 7.23 NMT NA 23.33
8/14/2014 6.06 NMT NA 24.50
8/15/2015
2/7/2018 7.24 NMT NA 23.42
8/15/2011 3.69 NMT NA 7.77
8/13/2012 2.70 NMT NA 8.76
8/7/2013 2.90 NMT NA 8.56
8/14/2014 1.39 NMT NA 10.07
3/11/2015 2.76 NMT NA 8.70
8/5/2015 2.67 NMT NA 7.95
8/1/2016 2.59 NMT NA 8.03
8/7/2017 2.75 NMT NA 7.87
8/9/2017 1.95 NMT NA 8.67
2/7/2018 3.03 NMT NA 7.59
8/7/2018 0.40 NMT NA 10.22
8/7/2019 3.33 NMT NA 7.29
8/6/2020 1.93 NMT NA 8.69
8/21/2021 1.80 NMT NA 8.82
2/19/2004 10.03 NMT NA 13.39
8/3/2004 10.55 NMT NA 12.87
2/16/2005 11.65 NMT NA 11.77
8/17/2005 9.53 NMT NA 13.89
2/8/2006 9.70 NMT NA 13.72
8/2/2006 11.94 NMT NA 11.48
8/6/2007 11.79 NMT NA 11.50
2/20/2008 12.27 NMT NA 11.02
8/14/2008 12.27 NMT NA 11.02
8/17/2009 12.36 NMT NA 10.93
8/10/2010 11.90 NMT NA 11.39
10/14/2010 5.28 NMT NA 18.01
8/18/2011 12.50 NMT NA 10.79
8/13/2012 10.82 NMT NA 12.47
8/7/2013 8.89 NMT NA 14.40
8/14/2014 5.84 NMT NA 17.45
3/11/2015 9.52 NMT NA 13.77
8/5/2015 9.41 NMT NA 13.90
8/1/2016 8.72 NMT NA 14.59
8/8/2017 8.24 NMT NA 15.07
8/9/2017 6.90 NMT NA 16.41
2/7/2018 9.12 NMT NA 14.19
8/7/2018 3.10 NMT NA 20.21
8/7/2019 10.83 NMT NA 12.48
8/6/2020 8.62 NMT NA 14.69
8/21/2021 8.32 NMT NA 14.99
AMW-1*
23.31
11.46
KMW-17
23.42
30.66
FHR TYPE II MONITORING WELLS WITHIN APEX TERMINAL
10.62
KMW-18
30.56
23.29
NM
TYPE II MONITORING WELLS (Continued)
Notes are provided on the final page of this table.
Page 13 of 18
Appendix A
Historical Groundwater Elevation Measurements
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
DATA POINT DATE DATA
COLLECTED
TOP OF
CASING
ELEVATION
(in feet)
DEPTH TO
WATER
BELOW TOC
(in feet)
FREE PHASE
PRODUCT
THICKNESS
(in feet)
SPECIFIC
GRAVITY
ADJUSTMENT
WATER
TABLE
ELEVATION
(in feet)
2/19/2004 9.99 NMT NA 13.36
8/3/2004 10.32 NMT NA 13.03
2/16/2005 11.54 NMT NA 11.81
8/17/2005 9.25 NMT NA 14.10
9/21/2005 6.80 NMT NA 16.55
9/22/2005 6.88 NMT NA 16.47
2/8/2006 9.35 NMT NA 14.00
8/2/2006 11.00 NMT NA 12.35
2/5/2007 8.97 NMT NA 14.38
8/6/2007 11.29 NMT NA 12.06
2/20/2008 11.79 NMT NA 11.56
8/14/2008 11.58 NMT NA 11.77
8/17/2009 11.62 NMT NA 11.73
8/10/2010 11.05 NMT NA 12.30
10/14/2010 5.69 NMT NA 17.66
8/18/2011 11.88 NMT NA 11.47
8/13/2012 10.28 NMT NA 13.07
8/7/2013 8.92 NMT NA 14.43
3/11/2014 10.90 NMT NA 12.45
3/11/2015 9.37 NMT NA 13.98
8/5/2015 9.73 NMT NA 13.72
8/1/2016 9.05 NMT NA 14.40
10/6/2016 7.08 NMT NA 16.37
8/9/2017 8.20 NMT NA 15.25
2/7/2018 9.23 NMT NA 14.22
8/7/2018 4.39 NMT NA 19.06
8/7/2019 10.84 NMT NA 12.61
8/6/2020 8.71 NMT NA 14.74
8/21/2021 8.22 NMT NA 15.23
2/19/2004 9.85 NMT NA 11.87
8/3/2004 9.97 NMT NA 11.75
2/16/2005 11.37 NMT NA 10.35
8/17/2005 9.31 NMT NA 12.41
9/21/2005 7.18 NMT NA 14.54
9/22/2005 7.24 NMT NA 14.48
2/8/2006 9.43 NMT NA 12.29
8/2/2006 10.94 NMT NA 10.78
2/5/2007 9.04 NMT NA 12.68
8/6/2007 10.83 NMT NA 10.89
2/20/2008 11.17 NMT NA 10.55
8/14/2008 11.02 NMT NA 10.70
8/17/2009 11.38 NMT NA 10.34
8/10/2010 11.07 NMT NA 10.65
10/14/2010 6.83 NMT NA 14.89
8/18/2011 11.41 NMT NA 10.31
8/7/2013 8.93 NMT NA 12.79
8/14/2014 6.53 NMT NA 15.19
3/11/2015 9.39 NMT NA 12.33
8/5/2015 9.00 NMT NA 12.82
8/1/2016 8.95 NMT NA 12.87
10/6/2016 7.48 NMT NA 14.34
8/9/2017 6.95 NMT NA 14.87
2/7/2018 9.19 NMT NA 12.63
8/7/2018 5.53 NMT NA 16.29
8/7/2019 10.75 NMT NA 11.07
8/6/2020 8.46 NMT NA 13.36
8/22/2021 8.21 NMT NA 13.61
23.45
AMW-2
AMW-3
21.72
23.35
21.82
FHR TYPE II MONITORING WELLS WITHIN APEX TERMINAL (Continued)
Notes are provided on the final page of this table.
Page 14 of 18
Appendix A
Historical Groundwater Elevation Measurements
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
DATA POINT DATE DATA
COLLECTED
TOP OF
CASING
ELEVATION
(in feet)
DEPTH TO
WATER
BELOW TOC
(in feet)
FREE PHASE
PRODUCT
THICKNESS
(in feet)
SPECIFIC
GRAVITY
ADJUSTMENT
WATER
TABLE
ELEVATION
(in feet)
2/19/2004 6.54 NMT NA 8.62
8/3/2004 6.90 0.8 0.86 8.95
2/16/2005 9.40 2.10 0.77 7.38
8/17/2005 7.25 1.45 0.77 9.03
9/21/2005 4.16 0.04 0.77 11.03
9/22/2005 4.32 0.04 0.77 10.87
2/8/2006 6.14 0.15 0.77 9.14
8/2/2006 7.33 0.21 0.77 7.99
2/5/2007 5.93 NMT NA 9.23
3/30/2007 7.00 NMT NA 8.16
8/8/2007 7.19 NMT NA 7.97
8/17/2007 7.55 NMT NA 7.61
2/20/2008 7.31 NMT NA 7.85
8/14/2008 7.10 NMT NA 8.06
2/12/2009 7.69 NMT NA 7.47
5/13/2009 8.00 NMT NA 7.16
8/17/2009 7.54 NMT NA 7.62
11/18/2009 6.92 NMT NA 8.24
8/10/2010 7.25 NMT NA 7.91
2/16/2011 6.39 NMT NA 8.77
5/26/2011 7.63 NMT NA 7.53
8/15/2011 7.32 NMT NA 7.84
8/13/2012 5.85 NMT NA 9.31
1/10/2013 6.75 NMT NA 8.41
4/17/2013 6.12 NMT NA 9.04
7/23/2013 5.35 NMT NA 9.81
8/7/2013 5.57 NMT NA 9.59
10/31/2013 6.67 NMT NA 8.49
2/13/2014 7.04 NMT NA 8.12
5/15/2014 6.43 NMT NA 8.73
8/14/2014 3.30 NMT NA 11.86
3/11/2015 5.99 NMT NA 9.17
8/5/2015 5.37 NMT NA 9.80
8/1/2016 5.53 NMT NA 9.64
8/9/2017 3.30 NMT NA 11.87
2/7/2018 5.74 NMT NA 9.43
8/7/2018 2.33 NMT NA 12.84
8/7/2019 6.85 NMT NA 8.32
8/6/2020 4.57 NMT NA 10.60
8/21/2021 4.58 NMT NA 10.59
AMW-4
15.17
15.16
FHR TYPE II MONITORING WELLS WITHIN APEX TERMINAL (Continued)
Notes are provided on the final page of this table.
Page 15 of 18
Appendix A
Historical Groundwater Elevation Measurements
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
DATA POINT DATE DATA
COLLECTED
TOP OF
CASING
ELEVATION
(in feet)
DEPTH TO
WATER
BELOW TOC
(in feet)
FREE PHASE
PRODUCT
THICKNESS
(in feet)
SPECIFIC
GRAVITY
ADJUSTMENT
WATER
TABLE
ELEVATION
(in feet)
2/19/2004 4.42 NMT NA 5.96
8/3/2004 4.52 NMT NA 5.86
2/16/2005 5.40 NMT NA 4.98
8/17/2005 4.58 NMT NA 5.80
9/21/2005 4.09 NMT NA 6.29
9/22/2005 4.40 NMT NA 5.98
2/8/2006 4.56 NMT NA 5.82
8/2/2006 6.00 NMT NA 4.38
2/5/2007 4.61 NMT NA 5.77
8/6/2007 5.43 NMT NA 4.95
2/20/2008 4.55 NMT NA 5.83
8/14/2008 4.76 NMT NA 5.62
8/17/2009 5.14 NMT NA 5.24
8/10/2010 5.66 NMT NA 4.72
10/14/2010 4.67 NMT NA 5.71
2/16/2011 4.81 NMT NA 5.57
5/26/2011 5.88 NMT NA 4.50
8/18/2011 4.83 NMT NA 5.55
8/13/2012 4.18 NMT NA 6.20
8/7/2013 4.98 NMT NA 5.40
8/14/2014 3.34 NMT NA 7.04
3/11/2015 4.90 NMT NA 5.48
8/5/2015 3.71 NMT NA 6.89
8/1/2016 4.98 NMT NA 5.62
8/9/2017 3.70 NMT NA 6.90
2/7/2018 4.77 NMT NA 5.83
8/7/2018 3.92 NMT NA 6.68
8/7/2019 5.23 NMT NA 5.37
8/6/2020 4.20 NMT NA 6.40
8/21/2021 4.39 NMT NA 6.21
2/19/2004 6.80 NMT NA 5.17
8/3/2004 6.76 NMT NA 5.21
2/16/2005 7.69 NMT NA 4.28
8/17/2005 6.92 NMT NA 5.05
9/21/2005 6.09 NMT NA 5.88
9/22/2005 6.17 NMT NA 5.80
2/8/2006 7.03 NMT NA 4.94
8/2/2006 8.68 NMT NA 3.29
2/5/2007 6.64 NMT NA 5.33
8/6/2007 7.25 NMT NA 4.72
2/20/2008 7.13 NMT NA 4.84
8/14/2008 7.30 NMT NA 4.67
8/17/2009 7.48 NMT NA 4.49
8/10/2010 7.43 NMT NA 4.54
10/14/2010 6.16 NMT NA 5.81
2/16/2011 6.88 NMT NA 5.09
5/26/2011 6.66 NMT NA 5.31
8/13/2012 6.62 NMT NA 5.35
8/7/2013 6.74 NMT NA 5.23
8/14/2014 4.19 NMT NA 7.78
3/11/2015 6.33 NMT NA 5.64
8/5/2015 5.99 NMT NA 5.89
8/1/2016 6.28 NMT NA 5.60
8/9/2017 4.45 NMT NA 7.43
2/7/2018 6.19 NMT NA 5.69
8/7/2018 Abandoned
11.88
AMW-6
10.38
11.97
AMW-5
10.60
FHR TYPE II MONITORING WELLS WITHIN APEX TERMINAL (Continued)
Notes are provided on the final page of this table.
Page 16 of 18
Appendix A
Historical Groundwater Elevation Measurements
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
DATA POINT DATE DATA
COLLECTED
TOP OF
CASING
ELEVATION
(in feet)
DEPTH TO
WATER
BELOW TOC
(in feet)
FREE PHASE
PRODUCT
THICKNESS
(in feet)
SPECIFIC
GRAVITY
ADJUSTMENT
WATER
TABLE
ELEVATION
(in feet)
3/11/2015 8.46 NMT NA 18.58
3/12/2015 10.27 NMT NA 16.77
8/5/2015 8.67 NMT NA 18.37
8/1/2016 8.33 NMT NA 18.71
8/8/2017 8.45 NMT NA 18.59
8/9/2017 6.74 NMT NA 20.30
2/7/2018 8.11 NMT NA 18.93
8/7/2018 4.18 NMT NA 22.86
8/7/2019 9.77 NMT NA 17.27
8/6/2020 7.71 NMT NA 19.33
8/23/2021 7.49 NMT NA 19.55
3/11/2014 8.95 NMT NA 14.61
4/9/2014 8.40 NMT NA 15.16
5/20/2014 8.18 NMT NA 15.38
8/14/2014 4.86 NMT NA 18.70
10/23/2014 7.35 NMT NA 16.21
3/11/20115 7.50 NMT NA 16.06
8/5/2015 7.59 NMT NA 15.94
8/1/2016 7.22 NMT NA 16.31
8/9/2017 5.65 NMT NA 17.88
2/7/2018 6.24 NMT NA 17.29
8/7/2018 2.75 NMT NA 20.78
8/7/2019 8.75 NMT NA 14.78
8/6/2020 7.04 NMT NA 16.49
8/22/2021 6.22 NMT NA 17.31
ATW-1 10/23/2014 --9.70 NMT NA NA
ATW-2 10/23/2014 --9.59 NMT NA NA
GW-10 7/22/2005 --7.00 1.50 0.77 NA
GW-11 7/22/2005 --3.50 NMT NA NA
9/21/2005 19.14 5.60 NMT NA 13.54
9/22/2005 19.14 5.78 NMT NA 13.36
9/21/2005 18.76 5.59 0.09 0.77 13.24
9/22/2005 18.76 5.81 0.08 0.77 13.01
9/21/2005 18.55 5.59 NMT NA 12.96
9/22/2005 18.55 5.80 NMT NA 12.75
9/21/2005 18.21 5.44 NMT NA 12.77
9/22/2005 18.21 5.70 NMT NA 12.51
9/21/2005 18.11 6.09 0.51 0.77 12.41
9/22/2005 18.11 6.14 0.30 0.77 12.20
9/21/2005 17.72 6.13 0.68 0.77 12.11
9/22/2005 17.72 6.22 0.50 0.77 11.89
9/21/2005 13.96 3.81 1.84 0.77 11.57
9/22/2005 13.96 4.22 2.11 0.77 11.36
9/21/2005 13.49 2.98 1.03 0.77 11.30
9/22/2005 13.49 3.17 1.05 0.77 11.13
9/21/2005 13.98 3.35 NMT NA 10.63
9/22/2005 13.98 3.56 NMT NA 10.42
9/21/2005 13.61 2.96 NMT NA 10.65
9/22/2005 13.61 3.12 NMT NA 10.49
9/21/2005 13.58 3.05 NMT NA 10.53
9/22/2005 13.58 3.10 NMT NA 10.48
FHR TYPE III MONITORING WELLS WITHIN APEX TERMINAL
TW-10
TYPE III MONITORING WELLS
TW-07
TW-04
TW-03
TW-06
TEMPORARY WELLS ABONDONED AFTER SAMPLING
TW-08
23.56
TW-09
TW-11
TW-05
TW-02
TW-01
ADW-1
23.53
KDW-1 27.04
Notes are provided on the final page of this table.
Page 17 of 18
Appendix A
Historical Groundwater Elevation Measurements
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
DATA POINT DATE DATA
COLLECTED
TOP OF
CASING
ELEVATION
(in feet)
DEPTH TO
WATER
BELOW TOC
(in feet)
FREE PHASE
PRODUCT
THICKNESS
(in feet)
SPECIFIC
GRAVITY
ADJUSTMENT
WATER
TABLE
ELEVATION
(in feet)
9/21/2005 12.98 2.55 NMT NA 10.43
9/22/2005 12.98 2.56 NMT NA 10.42
9/21/2005 12.24 1.96 NMT NA 10.28
9/22/2005 12.24 1.93 NMT NA 10.31
9/21/2005 12.61 2.17 NMT NA 10.44
9/22/2005 12.61 2.13 NMT NA 10.48
9/21/2005 12.74 2.66 NMT NA 10.08
9/22/2005 12.74 2.65 NMT NA 10.09
9/21/2005 11.67 1.84 NMT NA 9.83
9/22/2005 11.67 1.82 NMT NA 9.85
9/21/2005 11.09 3.13 NMT NA 7.96
9/22/2005 11.09 3.18 NMT NA 7.91
TW-18 10/11/2005 NA 1.12 1.54 NA NA
TW-19 10/11/2005 NA 2.55 NMT NA NA
Specific gravity adjustment for gasoline is 0.77.
NMT = No Measurable Thickness
NA = Not Applicable
TOC = Top of Casing
* = TOC elevation changed during the August 2007 reporting period.
Top of Casing Elevations surveyed by Paramounte Engineering, Inc. in June 2015
Per Apex personnel on 8/7/18, AMW-6 has been abandoned.
EAB = Enhanced Anaerobic Bioremediation
October/November 2016 and March/April 2017 data was obtained during post EAB sampling on 10/6/16, 11/23/16, 3/2/17 and 4/26/17,
respectively.
The referenced gauging data at monitoring wells KMW-8, KMW-12 and KMW-13 between September 2006 and August 2009 is for only
February and August events. Gauging data collected other months during this time period was previously reported.
Specific gravity adjustment for para-xylene is 0.86.
TW-13
TW-14
TW-15
TW-16
TW-17
TW-12
TEMPORARY WELLS ABONDONED AFTER SAMPLING (Continued)
Page 18 of 18

Appendix B

Historical Groundwater Field Measurements

Appendix B
Historical Groundwater Water Quality Measurements
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
Well ID Date
Measured
Time of
Measurement
Dissolved
Oxygen
(mg/L)
pH
(Standard
Units)
Specific
Conductivity
(mS/cm)
Temperature
(°C)
Redox-
Potential
(mV)
Turbidity
(NTU)
8/1/2016 18:00 0.35 7.14 0.149 28.26 -84.7 26.8
8/7/2017 14:30 0.74 6.97 0.262 27.32 -20.6 14.2
8/7/2019 9:40 0.68 6.12 0.278 28.15 -170.0 22.4
8/6/2020 10:55 0.96 6.73 0.172 28.40 -20.9 18.6
8/21/2021 8:30 2.65 6.79 0.089 27.94 79.0 58.6
8/1/2016 18:45 0.96 6.65 0.201 26.38 -93.4 7.21
8/8/2017 8:05 0.66 6.08 0.140 24.62 -29.4 15.5
8/7/2019 10:10 1.67 5.65 0.222 25.84 -153.5 20.9
8/6/2020 13:00 0.03 6.18 0.255 27.45 -100.6 1.19
8/21/2021 10:50 0.00 6.46 0.254 28.89 -169 11.2
8/1/2016 17:10 0.31 7.11 0.371 24.78 -243.8 1.56
8/16/2017 12:40 0.74 6.55 0.408 25.63 -110.5 1.54
8/8/2018 9:35 1.30 7.06 0.343 25.73 -11.7 0.35
8/7/2019 9:10 1.83 6.29 0.241 24.26 -115.2 1.46
8/6/2020 11:50 0.93 6.71 0.388 26.37 6.6 0.35
8/21/2021 9:20 0.11 6.83 0.257 25.09 -19 4.7
8/1/2016 12:02 0.23 6.94 1.023 29.25 -171.1 3.89
10/6/2016 14:50 0.35 6.60 0.437 24.86 -223.3 5.2
11/23/2016 10:45 0.73 6.61 0.390 20.64 -155.6 2.4
3/2/2017 11:04 0.11 6.42 2.213 16.61 -141.5 4.38
4/26/2017 9:50 0.61 6.11 1.704 20.34 -132.1 7.47
8/9/2017 15:45 0.47 6.48 0.344 26.30 -209.9 8.52
3/7/2018 13:55 1.18 6.78 0.871 16.31 -218.9 4.94
5/23/2018 12:25 0.09 6.81 1.066 25.90 -209.5 6.23
8/8/2018 11:25 4.27 6.95 2.073 26.75 -294.8 3.62
2/5/2019 12:55 0.70 7.12 0.865 18.31 -297.1 41.9
8/7/2019 15:40 0.16 6.89 0.809 30.70 -306.3 6.31
8/6/2020 13:50 0.11 6.51 0.422 26.30 -289.2 18.4
8/22/2021 12:17 0.00 6.98 0.783 27.93 -333 6.8
8/1/2016 13:05 0.05 6.76 0.231 31.84 -202.8 1.63
10/6/2016 9:15 2.22 6.28 0.214 24.62 -137.8 1.3
3/2/2017 9:29 0.24 6.24 0.191 17.68 -50.0 8.97
8/7/2017 10:55 0.30 6.67 0.258 29.59 -106.9 2.87
3/7/2018 13:10 1.08 6.95 0.304 17.55 -223.5 2.05
5/23/2018 9:05 0.15 7.17 0.330 24.17 -136.1 0.47
8/7/2018 15:30 0.28 6.41 0.236 28.69 -218.5 1.96
8/7/2019 11:35 0.19 6.55 0.245 30.75 -139.3 2.37
8/6/2020 9:55 0.33 6.98 0.321 27.32 -80.8 2.75
8/23/2021 9:20 0.00 6.72 0.178 29.15 -246 28.0
8/1/2016 14:10 0.05 6.99 0.959 29.99 -288.0 55.8
10/6/2016 13:25 0.57 6.60 0.732 25.44 -168.5 9.75
11/23/2016 11:35 0.63 6.65 1.012 20.26 -186.4 14
3/2/2017 10:35 0.68 6.12 0.644 16.45 -37.4 12.8
4/26/2017 10:35 0.68 6.10 0.237 21.92 -7.3 3.46
8/9/2017 13:20 0.68 6.20 0.980 26.48 -7.8 10.35
3/7/2018 9:50 2.09 6.86 0.646 16.51 -127.5 15.3
5/23/2018 9:40 0.39 6.59 0.657 26.27 45.0 12.4
8/8/2018 10:20 4.47 6.87 0.965 28.52 -237.6 40
2/5/2019 12:30 0.62 7.11 0.716 16.11 -198.0 44.5
8/7/2019 13:15 0.10 7.08 0.810 31.63 -201.6 51.4
8/6/2020 14:10 0.25 6.75 0.464 28.62 -86.6 25.2
8/22/2021 12:53 0.00 6.96 0.474 26.01 -257 18.8
KMW-1
KMW-5
KMW-6
KMW-8
KMW-7
KMW-3
TYPE II MONITORING WELLS
Notes are provided on the final page of this table.
1 of 4
Appendix B
Historical Groundwater Water Quality Measurements
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
Well ID Date
Measured
Time of
Measurement
Dissolved
Oxygen
(mg/L)
pH
(Standard
Units)
Specific
Conductivity
(mS/cm)
Temperature
(°C)
Redox-
Potential
(mV)
Turbidity
(NTU)
8/1/2016 10:30 0.92 6.38*0.785 26.33 -292.7 57.6
10/6/2016 10:20 1.07 6.63 0.301 24.11 -113.9 25
8/9/2017 15:10 1.89 6.68 0.268 25.86 -48.6 13.7
8/8/2018 8:50 0.67 7.13 0.242 26.63 -2.6 7.65
8/7/2019 10:30 0.15 7.51 0.802 28.12 -173.5 15.4
8/6/2020 12:10 0.78 6.59 0.458 24.20 -10.9 12.5
8/23/2021 15:05 0.04 6.39 0.408 27.80 95 17.9
8/1/2016 16:25 0.11 7.13 6.506 27.20 -342.6 3.17
10/6/2016 13:15 0.31 6.56 2.587 26.86 -269.3 4.5
11/23/2016 12:35 0.41 6.79 2.767 22.80 -291.9 65**
3/2/2017 11:40 0.42 6.81 3.431 17.62 -239.9 5.04
4/26/2017 12:30 0.57 5.67 0.304 22.32 -156.8 1.85
8/9/2017 10:55 0.29 6.39 1.511 25.30 -198.2 3.6
3/7/2018 11:40 4.82 6.72 2.252 17.12 -186.5 1.77
5/23/2018 16:00 0.27 6.16 0.261 23.79 -92.1 16.6
8/8/2018 11:30 0.09 6.78 8.336 30.22 -308.2 6.0
2/5/2019 9:25 0.30 7.13 1.819 17.05 -285.9 6.10
8/6/2020 12:50 0.44 6.18 0.530 30.1 -236.9 13.5
8/22/2021 14:08 0.00 6.41 0.435 28.74 -243 62.7
8/1/2016 15:10 0.25 6.86 1.084 32.94 -319.8 110
10/6/2016 12:00 0.34 6.62 1.000 25.53 -287.6 15
11/23/2016 14:05 1.18 6.59 1.102 21.75 -269.8 119**
3/2/2017 9:45 0.65 6.69 0.498 15.32 -221.5 10.1
4/26/2017 13:35 0.41 6.84 0.961 28.89 -289.3 22.4
8/29/2017 15:25 1.32 7.15 0.315 26.26 -97.0 9.10
3/12/2018 9:20 1.96 6.89 0.796 13.56 -257.6 40.7
5/23/2018 11:05 0.67 6.71 1.342 28.74 -49.2 18.7
8/8/2018 9:20 1.17 7.00 0.819 28.30 -40.9 22
2/5/2019 11:15 0.34 7.12 1.001 19.35 -77.3 17.0
8/7/2019 12:40 2.99 5.80 1.274 30.09 -173.2 13.9
8/6/2020 12:20 0.53 6.74 1.054 28.7 -127.2 8.18
8/22/2021 14:52 0.00 6.71 0.844 29.13 -125 24.4
8/1/2016 14:15 0.50 6.23 0.618 31.64 -55.6 2.9
8/9/2017 9:30 2.07 6.41 0.986 26.72 68.0 6.6
8/7/2018 15:50 1.30 6.88 0.333 29.76 64.6 0.00
8/7/2019 8:55 0.40 6.24 0.627 28.61 20.4 2.52
8/6/2020 13:20 0.33 6.52 0.340 29.10 -154.5 7.27
8/22/2021 13:33 2.04 6.68 0.315 28.93 -63 12.4
8/1/2016 19:40 0.07 7.34 0.681 23.89 -97.4 5.41
8/7/2017 15:40 0.18 6.87 0.569 24.29 -142.3 9.5
8/8/2018 8:50 7.23 6.80 0.506 25.22 -92.0 7.6
8/7/2019 10:40 2.72 5.93 0.493 26.32 -147.9 16.1
8/6/2020 9:55 0.15 6.77 0.560 27.28 -123.4 10.7
8/21/2021 11:45 0.00 6.97 0.525 26.52 -190 7.6
KMW-18
KMW-13
KMW-9R
KMW-12
KMW-14
TYPE II MONITORING WELLS (Continued)
Notes are provided on the final page of this table.
2 of 4
Appendix B
Historical Groundwater Water Quality Measurements
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
Well ID Date
Measured
Time of
Measurement
Dissolved
Oxygen
(mg/L)
pH
(Standard
Units)
Specific
Conductivity
(mS/cm)
Temperature
(°C)
Redox-
Potential
(mV)
Turbidity
(NTU)
8/1/2016 15:30 1.16 6.46 0.275 28.39 -25.6 1.62
8/8/2017 8:55 1.61 6.40 0.328 25.52 31.8 4.20
8/8/2018 9:05 2.01 6.08 0.318 27.79 226.5 0.61
8/7/2019 14:15 0.25 6.74 0.291 27.27 -130.1 1.48
8/6/2020 9:55 0.16 6.71 0.358 26.1 -141.1 1.10
8/21/2021 15:48 0.00 6.77 0.324 27.32 -135 11.6
8/1/2016 11:15 0.54 6.33 0.260 24.49 -49.5 0.93
10/6/2016 9:35 1.19 6.37 0.267 22.45 -77.0 1.04
8/9/2017 13:45 0.32 6.52 0.591 24.25 -275.2 0.90
8/8/2018 13:10 1.73 6.58 0.394 23.47 -76.1 0.66
8/7/2019 10:01 0.50 7.17 1.261 23.07 -264.9 3.33
8/6/2020 10:50 0.23 6.65 0.552 23.2 -293.5 5.34
8/21/2021 12:55 0.00 6.73 0.677 24.61 -235 7.0
8/1/2016 13:00 0.44 6.44 0.239 31.72 -99.7 55
10/6/2016 11:10 0.54 6.39 0.195 23.31 -90.3 2.69
8/9/2017 11:35 1.32 6.35 0.122 25.55 71.3 7.69
8/8/2018 10:20 0.38 6.67 0.335 25.60 -77.7 0.29
8/7/2019 9:21 0.19 6.74 0.245 26.95 -170.2 1.77
8/6/2020 10:25 0.49 6.68 0.650 25.80 -258.8 4.62
8/22/2021 9:03 0.00 6.62 0.296 24.31 -237 14.9
8/1/2016 13:45 0.21 6.27 0.180 27.92 -98.0 5.52
8/9/2017 15:15 0.40 6.58 0.267 23.98 -129.3 3.08
8/8/2018 13:50 0.20 6.33 0.183 32.40 20.3 1.92
8/7/2019 12:35 0.23 6.41 0.335 28.18 -186.0 3.97
8/6/2020 11:45 0.45 6.21 0.300 27.70 -236.3 4.20
8/21/2021 14:55 0.00 6.46 0.241 27.42 -197 11.0
8/1/2016 10:25 0.29 6.62 0.423 29.43 -80.6 0.63
8/9/2017 14:30 0.96 6.79 0.448 26.44 -73.8 22.0
8/8/2018 12:30 0.22 6.67 0.509 28.85 -52.3 2.17
8/7/2019 11:00 0.35 6.76 0.415 29.26 -105.1 1.76
8/6/2020 11:20 0.38 6.81 0.484 29.90 -130.2 7.16
8/21/2021 13:35 0.00 6.83 0.540 29.30 -124 16.0
8/1/2016 11:40 0.09 6.14 0.224 33.00 -109.6 1.25
8/9/2017 9:55 7.62 6.80 0.112 28.02 5.3 7.12
AMW-3
AMW-2
AMW-5
AMW-6
AMW-4
AMW-1
FHR TYPE II MONITOING WELLS WITHIN APEX TERMINAL
Notes are provided on the final page of this table.
3 of 4
Appendix B
Historical Groundwater Water Quality Measurements
Loading Rack Area
Former FHR North Terminal
Wilmington, North Carolina
Well ID Date
Measured
Time of
Measurement
Dissolved
Oxygen
(mg/L)
pH
(Standard
Units)
Specific
Conductivity
(mS/cm)
Temperature
(°C)
Redox-
Potential
(mV)
Turbidity
(NTU)
8/1/2016 10:30 0.14 11.12 0.220 24.69 -112.9 0.90
8/8/2017 11:10 0.93 11.31 0.631 23.39 -71.7 1.74
8/8/2018 8:00 5.37 10.17 0.211 23.83 -70.9 5.16
8/7/2019 14:50 1.29 11.31 1.084 25.45 -88.7 3.38
8/6/2020 10:45 1.85 11.72 1.150 21.04 -70.4 1.77
8/23/2021 12:08 1.24 11.76 1.70 26.70 -171 3.4
8/1/2016 15:00 0.65 10.34 0.268 25.50 -69.7 6.01
8/9/2017 11:20 2.78 12.01 2.015 24.37 -100.5 8.17
8/7/2018 15:30 2.82 11.62 1.938 28.09 1.9 12.9
8/7/2019 13:20 3.51 11.47 2.662 26.93 -121.2 7.53
8/6/2020 9:25 3.86 12.30 5.571 26.60 -86.4 0.70
8/22/2021 11:00 0.09 11.69 0.925 25.78 -155 35.60
°C = Degrees Celsius
mS/cm = Millisiemens per Centimeter
mg/L = Milligrams per Liter
mV = Millivolt
NTU = Nephelometric Turbidity Units
Data presented is the final field measurement recorded immediately prior to collection of laboratory sample.
* prior to sampling on 8/1/16, pH reading was questionable due to suspected equipment malfunction. pH was remeasured on 8/3/16.
** prior to sampling on 11/23/16, turbidity reading was questionable due to suspected equipment malfunction. Turbidity was remeasured on 11/29/16.
October/November 2016, March/April 2017 and February 2019 data was obtained during post EAB sampling on 10/6/16, 11/23/16, 3/2/17, 4/26/17 and 2/5/19 respectively.
Per Apex personnel on 8/7/18, AMW-6 has been abandoned.
KDW-1
FHR TYPE III MONITORING WELLS WITHIN APEX TERMINAL
ADW-1
TYPE III MONITORING WELLS
4 of 4

Appendix C

Historical Groundwater Results

Appendix CHistorical Groundwater ResultsLoading Rack AreaFormer FHR North TerminalWilmington, North CarolinaSample ID Date Collected1 70 70 600 70 20 6 70 600 400 400 VariesATW-1 10/23/2014 12.6 <0.41 <0.38 96.82.6 0.29 J 20.0 <0.42 24.4 43.4 13.8 67,600 111 14.63 JATW-2 10/23/2014 <0.25 <0.41 <0.38 <0.30 <0.40 8.4 <0.24 <0.42 <0.26 0.43 J <0.36 268 0.39 J 16.0 JT-1** 8/1/2001-----------1,100--T-2** 8/1/2001-----------4.9*--T-3** 8/24/2001 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 210 <5.0 NDT-4** 8/24/2001 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 44 <5.0 NDT-5** 8/24/2001 <500 <500 <500 <500 <500 <500 <500 <500 <500 <500 <500 34,000 <500 NDT-6** 8/24/2001 8,300 <500 <500 <500 <500 48,000 830 <500 4,100 1,700 <500 11,000 860 NDT-8** 8/24/2001 20 <5.0 <5.0 <5.0 <5.0 21 <5.0 <5.0 18 <5.0 <5.0 22 <5.0 ND4/1/94-----------7,900* - -2/10/99-----------780* - -2/24/00-----------66.9*--9/21/00-----------128* - -2/14/01-----------16,000* - -7/10/01-----------7,600* <500 -8/1/01-----------4,900* - -8/24/01 <500 <500 <500 3,400 <500 <500 <500 <500 <500 <500 <500 4,500 <500 ND9/18/01 <50 <50 81 <50 <50 <50 <50 <50 <50 340 170 3,000 <50 BQL1/3/02 <5.0 <5.0 37 <5.0 <5.0 <5.0 5.5 9 <5.0 39 <5.0 <10 <5.0 ND2/27/02 <5.0 5.7 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 51 43 <10 <5.0 ND2/28/03 <50 <50 <50 <50 <50 <50 <50 <50 <50 <50 <50 540 <50 ND9/16/03 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 53 40 22 <5.0 ND2/19/04 <1.0 <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 26 27 2.6 <1.0 ND8/5/04 <0.36 7.7 0.81J <0.34 0.27J <0.31 1.9J 0.85J <0.54 52 60 <0.40 <0.35 ND2/17/05 <0.54 <0.38 3.2 <0.62 <0.66 <0.45 <0.12 <0.45 <0.62 69 100 1.38/23/05 <0.54 7.6 0.84J <0.62 <0.66 <0.45 <0.12 <0.45 <0.62 14 24 NDNotes are provided on the final page of this table.Toluene1,2,4-TrimethylbenzeneContaminant of ConcernBenzenen-Butylbenzenesec-ButylbenzeneEthylbenzene1,3,5-Trimethylbenzenem/p-Xyleneso-XyleneAll Other 8260B AnalytesGroundwater Clean-up Goal (ug/L)500Isopropylbenzene (Cumene)Methyl Tert Butyl Ether (MTBE)Naphthalenen-PropylbenzeneTEMPORARY MONITORING WELLSTYPE II MONITORING WELLSKMW-1<1.6 (Total Xylenes)6.3 (Total Xylenes)Page 1 of 20
Appendix CHistorical Groundwater ResultsLoading Rack AreaFormer FHR North TerminalWilmington, North CarolinaSample ID Date Collected1 70 70 600 70 20 6 70 600 400 400 VariesToluene1,2,4-TrimethylbenzeneContaminant of ConcernBenzenen-Butylbenzenesec-ButylbenzeneEthylbenzene1,3,5-Trimethylbenzenem/p-Xyleneso-XyleneAll Other 8260B AnalytesGroundwater Clean-up Goal (ug/L)500Isopropylbenzene (Cumene)Methyl Tert Butyl Ether (MTBE)Naphthalenen-Propylbenzene10/14/05NMNMNMNMNMNMNMNMNMNMNMNMNMNM2/9/06<0.54 <0.38 <0.60J <0.62 <0.66 1.0 J <0.12 <0.45 <0.62 2142ND3/27/2006 <1.0 <1.0 <1.0 <1.0 <1.0 <10.0 <5.0 <1.0 <1.06.210ND8/8/2006 <0.54 <0.38 <0.60 1.0 <0.66 0.69 J <0.12 <0.45 <0.62 2756ND2/7/2007 <0.54 <0.38 <0.60 <0.62 <0.66 <0.45 <0.12 <0.45 <0.62 4.18.6ND3/30/2007 <0.54 <0.38 <0.60 <0.62 <0.66 <0.45 <0.12 <0.45 <0.62 4.29.18.4 J*8/17/2007 <1.6 <1.7 <1.5 <1.5 <1.4 3.1 J <1.4 <1.7 2.2 J5.71412 B2/25/20081.2<1.0 <1.0 <1.0 <1.013<5.0 <1.0 <1.01.32.1ND8/19/20081.4<1.01.4<1.0 <1.0 <10 <5.0 <1.0 <1.02.48.9142/12/2009 <1.0 <1.02.0<1.0 <1.0 <10 <5.03.0<1.02.411ND5/13/2009 <1.0 <1.02.2<1.01.7<10 <5.03.9<1.02212ND8/18/2009 <1.0 <1.01.8<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.03.8<2.0 <1.0ND11/18/2009 <1.0 <1.01.5 0.36 J <1.02.8<1.01.2<1.0 0.89 J 6.2303 0.61 J 6.15/13/2010 <1.0 <1.0 0.93 J 22.7 0.49 J <1.0 <1.0 0.69 J 0.33 J 1.92.7 19,700 22.1ND8/12/2010 <1.0 <1.01.314.4 0.63 J 0.95 J 1.7 0.68 J <1.04.519,670 1.5 3.42J11/17/2010 <0.25 <0.41 <0.38 <0.3 <0.4 <0.21 <0.24 1.5 <0.26 6.53.11.2 J <0.23 4.7 J2/23/2011 <0.25 <0.41 0.41 J <0.3 <0.4 <0.21 <0.24 <0.42 <0.26 <0.31 2.4 <0.66 <0.23 3.0 J8/19/2011 <0.25 <0.41 2.0<0.31.1 <0.21 <0.24 3.6 <0.26 1.92.18.5 J11/29/2011 <0.25 6.1 0.41 J 3.0 <0.40 0.25 J <0.24 <0.42 <0.26 0.69 J 0.95 J 2,210 0.70 J 1.69 J3/1/2012 <0.25 <0.41 <0.38 <0.30 <0.40 1.2 <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 ND5/22/2012 <0.25 6.02.0 <0.30 1.3 <0.21 1.83.5 <0.26 2.3 0.71 J <0.66 <0.23 55.98/17/2012 <0.25 <0.41 1.1 <0.30 <0.40 0.73 J <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 ND8/13/2013 <0.25 <0.41 <0.38 0.35 J <0.40 <0.21 <0.24 <0.42 <0.26 0.31 J <0.36 113 <0.23 ND8/21/2014 <0.25 <0.41 <0.38 0.48 J <0.40 <0.21 0.27 J <0.42 <0.26 <0.31 <0.36 39.9 <0.23 11.95 J3/11/2015 <0.25 <0.41 <0.38 0.94 J <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36 713 <0.23 0.35 J8/5/2015 <0.50 2.2 <0.76 12.0 <0.80 <0.42 0.86 J <0.84 <0.52 3.0 <0.72 14,700 1.8 J 0.73 J8/1/2016 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36 5.6 <0.23 ND8/7/2017 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36 10.0 <0.23 ND8/7/2019 <0.15 <0.23 <0.20 <0.26 <0.20 <0.28 <0.35 <0.18 <0.24 <0.17 <0.20 33.3 <0.22 ND8/6/2020 <0.30 <0.47 <0.40 0.69 J <0.40 <0.55 <0.70 <0.37 0.57 J <0.34 <0.39 416 <0.44 ND8/21/2021 <0.34 <0.49 <0.40 <0.30 <0.33 <0.42 <0.64 <0.34 <0.48 <0.50 <0.33 <0.71 <0.34 NDNotes are provided on the final page of this table.TYPE II MONITORING WELLS (Continued)KMW-1 (cont'd)<1.3 (Total Xylenes)<2.0 (Total Xylenes)1,000 (Total Xylenes)<1.3 (Total Xylenes)3.3 (Total Xylenes)1,100 (Total Xylenes)<2.0 (Total Xylenes)<2.0 (Total Xylenes)<2.0 (Total Xylenes)<2.0 (Total Xylenes)0.81 J (Total Xylenes)Page 2 of 20
Appendix CHistorical Groundwater ResultsLoading Rack AreaFormer FHR North TerminalWilmington, North CarolinaSample ID Date Collected1 70 70 600 70 20 6 70 600 400 400 VariesToluene1,2,4-TrimethylbenzeneContaminant of ConcernBenzenen-Butylbenzenesec-ButylbenzeneEthylbenzene1,3,5-Trimethylbenzenem/p-Xyleneso-XyleneAll Other 8260B AnalytesGroundwater Clean-up Goal (ug/L)500Isopropylbenzene (Cumene)Methyl Tert Butyl Ether (MTBE)Naphthalenen-Propylbenzene4/1/94-----------19,000* --2/10/99-----------5*--2/17/05<1.1 1.1J <1.2 <1.2 <1.3 <0.90 6.7J 1.4J <1.23.61.8JND7/22/05<0.54 <0.38 <0.60 <0.62 <0.66 <0.45 <0.12 <0.45 <0.62 <0.44 <0.49BQL8/23/05<0.54 <0.38 <0.60 <0.62 <0.66 <0.45 0.63J <0.45 <0.62 <0.44 <0.49ND10/11/05 <0.54 <0.38 <0.60 <0.62 <0.66 <0.72 J <0.12 <0.45 <0.62 <0.44 <0.49 <1.3 <0.49 BQL10/14/05 <0.54 NMNM <0.62 NMNMNMNM <0.62 NMNMBQL2/9/06<1.1 <0.76 <1.2 <1.2 <1.3 1.5J <0.24 <0.90 <1.2 1.1 J <0.98ND3/27/2006 <1.0 <1.0 <1.0 <1.01.4 <10.0 6.2<1.0 <1.03.9<1.0ND8/8/2006 <0.54 <0.38 <0.60 <0.62 <0.66 <0.45 <0.12 <0.45 <0.62 <0.44 <0.49ND2/7/2007<2.7 <1.9 <3.0 <3.1 <3.3 2.9 J <0.60 <2.3 <3.1 <2.2 <2.3ND3/30/2007 <1.1 <0.76 <1.2 <1.2 <1.3 1.7 J <0.24 <0.90 <1.23.1 <0.98ND8/17/2007<1 <0.33 0.36 J <0.30 <0.27 <0.58 <0.27 <0.34 <0.31 <0.27 <0.28ND2/25/2008 <1.0 <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0ND8/19/2008 <1.0 <1.0 <1.0 <1.01.2<10 <5.01.6<1.013<1.0ND2/12/2009 <1.0 <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0ND5/13/2009 <1.0 <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0ND8/18/2009 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0ND11/18/2009 <1.0 <1.0 0.53 J <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0ND5/13/2010 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0ND8/12/2010 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 1.6 J <1.0 0.47 JNotes are provided on the final page of this table.TYPE II MONITORING WELLS (Continued)KMW-2580 (Total Xylenes)<1.3 (Total Xylenes)6.3 (Total Xylenes)19 (Total Xylenes)250 (Total Xylenes)<2.0 (Total Xylenes)2.5 (Total Xylenes)1,200 (Total Xylenes)790 (Total Xylenes)<0.87 (Total Xylenes)<2.0 (Total Xylenes)<2.0 (Total Xylenes)<2.0 (Total Xylenes)<2.0 (Total Xylenes)Page 3 of 20
Appendix CHistorical Groundwater ResultsLoading Rack AreaFormer FHR North TerminalWilmington, North CarolinaSample ID Date Collected1 70 70 600 70 20 6 70 600 400 400 VariesToluene1,2,4-TrimethylbenzeneContaminant of ConcernBenzenen-Butylbenzenesec-ButylbenzeneEthylbenzene1,3,5-Trimethylbenzenem/p-Xyleneso-XyleneAll Other 8260B AnalytesGroundwater Clean-up Goal (ug/L)500Isopropylbenzene (Cumene)Methyl Tert Butyl Ether (MTBE)Naphthalenen-Propylbenzene4/1/94-----------6.5*--2/10/99-----------96*--2/14/01-----------62*--8/24/01<5.0 <5.0 <5.033<5.0136.75.7<5.017<5.059<5.0ND9/18/01<1<1<1<1<1<1<1<1<1<1<1<2<1BQL1/3/02<5.0 <5.0991713<5.01648<5.0 1103832<5.0ND2/27/02<5.08.4<5.012<5.0 <5.05.344<5.0482923<5.0ND2/28/03<5.0 <5.0 <5.012<5.0 <5.0 <5.0 <5.0 <5.0371138<5.0ND29/16/03<5.0 <5.0 <5.0 120 <5.0 <5.08.19.4<5.07432250 <5.0ND2/19/04<1.0 <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND8/5/04<0.36 <0.31 <0.24 <0.34 <0.25 <0.31 <0.44 <0.32 <0.54 0.23J <0.21 <0.40 <0.35 ND2/17/053.8 <0.38 <0.60 8239 <0.45 61951.3640938.9J8/23/05 11,000 <380 <600 6,700 <660 340,000 340J 700J 53,000 3,800 1,100ND10/14/052/9/068/8/2006540 <0.38 <0.60 4,600 360 2,700 270 J 220 17,000 2,100 580ND2/7/200732<1.9111301813024 J131801104348.6 J3/30/2007 730<19<30 2,900 210 2,300 140 J 120 8,300 1,100 310ND8/17/2007 730 <3.3 8.0 J 540623,400 29 J372,100 300803.6 JB2/25/200862<1.0 <1.0532.6360 <5.02.210191.5ND8/19/2008 180 <0.66 <0.58 820134001101.9 1,700 120311002/12/2009 490<16232,100 380<29390160 14,000 2,900 1,100ND5/13/200934<6.67.0660130<1213061240 1,200 320ND8/18/2009 <100 <100 <100 1,210 115 <100 572 <100 749 1,260 405 3,600 2,560 62511/18/2009 19.9 <1.0 <1.0 1041132.165.7 74.52.458125630314.2 39.13 J5/13/2010 79.3 <5.0 <5.0 16667.9 2.6 J 63.0 57.521855784.1305103548/12/2010 <1.0 <1.0 <1.0 <1.0 <1.0 0.41 J <1.0 <1.0 <1.0 <1.0 <1.07.71.4 0.63 J8/19/2011 48.9 <0.82 <0.76 18562.1 1.0 J 38.5 35.09.534552.71034.215.48/17/2012 12.8 <0.41 <0.38 3.033.0 0.25 J 1.121.2 0.68 J 51.6 <0.36 <0.66 0.24 J ND8/13/2013 27.8 <0.41 2.21.424.5 0.45 J 2.016.73.411.16.57.1 0.93 J ND8/21/2014 18.9 <0.41 <0.38 34288.9 0.50 J 78.1 42.3 92.536291.4396 0.59 J 30.03/11/20157.5 <0.82 <0.76 42.4 54.8 <0.42 46.3 29.3 1.6 J 24286.7237 0.57 J 8.7 J8/5/201510.7 <0.41 <0.38 0.95 J 33.0 <0.21 11.7 16.41.538.6 31.6 33.5 <0.23 5.2 J8/1/201612.1 <1.08.18.562.3 <0.52 40.9 32.73.4298133311 <0.58 58.2J8/8/201714.0 <0.41 <0.38 1.227.9 <0.21 2.214.72.68.89.43.4 0.76 J ND8/7/201935.9 <0.23 12.23.389.91.2 0.96 J 47.93.568.0 <0.20 4.2 0.43 J 7.68/6/20208.0 <0.23 2.0 <0.26 16.3 <0.28 0.41 J 12.01.4 0.52 J <0.20 4.6 0.25 J ND8/21/20218.0 <0.49 1.1 <0.30 11.6 <0.42 <0.64 7.51.6 <0.50 <0.33 <0.71 <0.34 NDNotes are provided on the final page of this table.TYPE II MONITORING WELLS (Continued)KMW-3110 (Total Xylenes)29,000 (Total Xylenes)0.49' FREE-PHASE PRODUCT PRESENT IN KMW-3FREE-PHASE PRODUCT PRESENT IN KMW-326,000 (Total Xylenes)530 (Total Xylenes)16,000 (Total Xylenes)1,800 (Total Xylenes)58 (Total Xylenes)11,000 (Total Xylenes)20,000 (Total Xylenes)2,900 (Total Xylenes)Page 4 of 20
Appendix CHistorical Groundwater ResultsLoading Rack AreaFormer FHR North TerminalWilmington, North CarolinaSample ID Date Collected1 70 70 600 70 20 6 70 600 400 400 VariesToluene1,2,4-TrimethylbenzeneContaminant of ConcernBenzenen-Butylbenzenesec-ButylbenzeneEthylbenzene1,3,5-Trimethylbenzenem/p-Xyleneso-XyleneAll Other 8260B AnalytesGroundwater Clean-up Goal (ug/L)500Isopropylbenzene (Cumene)Methyl Tert Butyl Ether (MTBE)Naphthalenen-Propylbenzene4/1/94-----------28,000* --2/24/00-----------9.4*--9/21/00-----------198*--2/14/01-----------110*--8/24/01<5.0 <5.0 <5.0 <5.0 <5.0 2107.1<5.0 <5.07.7<5.0 <10 <5.0ND9/17/01111<1817812<1121028<1BQL1/3/02<5.0 <5.0 <5.041<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.052<5.0ND2/27/02<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <10 <5.0ND2/28/03<5.0 <5.0 <5.0 <5.0 <5.09<5.0 <5.0 <5.01511<5.0 <5.0ND9/16/03<5.0 <5.0 <5.0 <5.0 <5.012<5.0 <5.0 <5.0 <5.0 <5.0 <10 <5.0ND2/19/04<1.0 <1.0 <1.0 <1.0 <1.017<5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND8/5/04<0.36 <0.31 <0.24 <0.34 <0.25 1.1J 0.50J <0.32 <0.54 0.38J 0.24J <0.40 <0.35 ND2/17/05<0.54 <0.38 <0.60 <0.62 1.26.0J 1.2J1.2 <0.62 101.2ND8/23/05<0.54 <0.38 <0.60 <0.62 1.2 <0.45 0.45J 1.5 <0.62 <0.44 <0.49ND10/11/05 <0.54 <0.38 5.1 <0.62 1.2 0.47J 1.3J2.5 <0.62 6.93.55151BQL10/14/05<0.54--<0.62----<0.62--BQL 2/9/06<0.54 <0.38 <0.60 1.9 <0.66 63 <0.12 <0.45 1.5 <0.44 <0.490.58J3/27/2006 <1.0 <1.0 <1.0 <1.0 <1.038<5.0 <1.0 <1.0 <1.0 <1.0ND8/8/2006 <0.54 <0.38 <0.60 <0.62 <0.66 0.53 J <0.12 <0.45 <0.62 <0.44 <0.49ND2/7/2007 <0.54 <0.38 <0.60 <0.62 <0.66 0.63 J <0.12 <0.45 <0.62 1.72.4ND3/30/2007 <0.54 <0.38 <0.60 <0.62 <0.66 0.64 J <0.12 <0.45 <0.62 <0.44 <0.49ND8/17/2007 <0.32 <0.33 <0.29 <0.30 <0.27 <0.58 <0.27 <0.34 <0.31 <0.27 <0.283.9 B2/25/2008 <1.0 <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0ND8/19/2008 <1.0 <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0ND2/12/2009 <1.0 <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0ND5/13/2009 <1.0 <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0ND8/18/2009 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0ND11/18/2009 0.57 J <1.0 <1.0 <1.0 <1.02.1<1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0ND4/21/2010 <1.0 <1.0 0.88 J 6.2 0.40 J 0.40 J 1.3<1.0 <1.01.2<1.0 3,170 0.58 J 0.63 J5/13/2010 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.07.5<1.0ND8/12/2010 54.2 <1.0 <1.0 1491152.677.2 59.7 18.6712 <1.0 14784.3 0.40 J11/17/2010 <0.25 <0.41 <0.38 0.35 J <0.4 0.36 J <0.24 <0.42 <0.26 <0.31 <0.36 79.9 <0.23 4.2 J2/23/2011 <0.25 <0.41 <0.38 <0.30 <0.4 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 3.5 J8/19/2011 <0.25 <0.41 <0.38 0.67 J <0.41.8 0.88 J <0.42 <0.26 0.99 J <0.36 13.4 <0.23 5.67 J11/29/2011 <0.25 <0.41 <0.38 0.48 J <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 2.44 J3/1/2012 <0.25 <0.41 <0.38 0.82 J <0.40 0.21 J <0.24 <0.42 <0.26 <0.31 <0.36 504 0.66 J ND5/22/2012 <0.25 <0.41 <0.38 <0.30 <0.40 0.58 J <0.24 <0.42 <0.26 <0.31 <0.36ND8/17/2012 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 NDNotes are provided on the final page of this table.TYPE II MONITORING WELLS (Continued)KMW-471 (Total Xylenes)<1.3 (Total Xylenes)19 (Total Xylenes)10 (Total Xylenes)<2.0 (Total Xylenes)2.7 (Total Xylenes)<1.3 (Total Xylenes)<1.3 (Total Xylenes)9.4 (Total Xylenes)<2.0 (Total Xylenes)<2.0 (Total Xylenes)<2.0 (Total Xylenes)<2.0 (Total Xylenes)<0.66 (Total Xylenes)Page 5 of 20
Appendix CHistorical Groundwater ResultsLoading Rack AreaFormer FHR North TerminalWilmington, North CarolinaSample ID Date Collected1 70 70 600 70 20 6 70 600 400 400 VariesToluene1,2,4-TrimethylbenzeneContaminant of ConcernBenzenen-Butylbenzenesec-ButylbenzeneEthylbenzene1,3,5-Trimethylbenzenem/p-Xyleneso-XyleneAll Other 8260B AnalytesGroundwater Clean-up Goal (ug/L)500Isopropylbenzene (Cumene)Methyl Tert Butyl Ether (MTBE)Naphthalenen-Propylbenzene9/17/01<20<20<20<20<20<203326<2021056800<20 BQL1/3/02<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <10 <5.0ND2/27/02<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <10 <5.0ND12/28/03<500 <500 <500 <500 <500 <500 <500 <500 <500 <500 <500 78,000 <500 ND9/16/03<120 <120 <120 <120 <120 <120 <120 <120 <120 <120 <120 13,000 <120 ND2/19/04<500 <500 <500 <500 <500 <5,000 <2,500 <500 <500 <500 <500 15,000 <500 ND8/5/04<36<31<24<34<25<31<44<32<54<19<21 25,000 <35ND2/17/05<54<38<60<62<66<45<12<45<62<44<49ND8/23/05<54<38<60<62<66<45<12<45<62<44<49ND10/14/05NMNMNMNMNMNMNMNMNMNMNMNMNMNM2/9/06<54<38<60<62<66<45<12<45<62<44<49ND8/14/2006 <2.7 <1.9 <3.0 <3.1 <3.3 7.4 J 1.6 J <2.3 <3.1 <2.2 <2.5ND2/7/2007 <0.54 <0.38 <0.60 <0.62 <0.66 1.6 J <0.12 <0.45 <0.62 <0.44 <0.49ND3/30/2007 <27<19<30<31<33<23 <6.0 <23<31<22<25ND8/17/2007 <0.32 <0.33 <0.29 <0.30 <0.27 12 <0.27 <0.34 <0.31 <0.27 <0.288.0 B2/25/2008 <1.0 <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0ND8/19/20083.1<1.0 <1.0 <1.02.2<10 <5.0 <1.0 <1.07.31.37.52/12/2009 <1.0 <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0ND5/13/2009 <1.0 <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0ND8/18/2009 <1.0 <1.0 <1.0 <1.0 <1.05.1<1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0ND11/18/2009 <1.0 <1.0 0.48 J <1.0 0.57 J 1.8<1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0ND4/21/2010 <1.0 <1.0 <1.0 16.61.11.72.3 0.72 J 0.75 J 5.6 0.94 J 15,200 10.9 1.67 J5/13/2010 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 922 <5.0 14.68/12/2010 <1.0 <1.0 <1.0 <1.0 <1.08.2<1.0 <1.0 <1.0 <1.0 <1.0 139 <1.0 0.40 J11/17/2010 <1.2 <2.0 <1.9 <1.5 <2.0 <1.0 <1.2 <2.1 <1.3 <1.6 <1.826<1.2ND2/23/2011 <0.25 <0.41 8.312.1 0.83 J 4.32.11.2 0.28 J 10.41.9 9,490 5.5 3.95 J8/19/2011 <0.25 <0.41 <0.38 <0.3 <0.4 0.82 J <0.24 <0.42 <0.26 <0.31 <0.36 2.6 <0.23 5.9 J11/29/2011 <12.5 <20.5 <19.0 <15.0 <20.0 <10.5 <12.0 <21.0 <13.0 <15.5 <18.0 5,470 <11.5 14.9 J3/1/2012 <0.25 <0.41 1.0 <0.30 0.64 J 0.80 J <0.24 1.9 <0.26 0.48 J 0.41 J <0.66 <0.23 ND5/22/2012 <0.25 <0.41 <0.38 <0.30 <0.40 3.2 <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 4.1 J8/17/2012 <0.25 <0.41 <0.38 <0.30 <0.40 2.1 <0.24 <0.42 <0.26 <0.31 <0.36 58.7 <0.23 ND8/13/2013 <0.25 <0.41 <0.38 <0.30 <0.40 1.0 0.45 J <0.42 <0.26 1.3 <0.36 5,710 0.83 J 4.87 J8/13/2013 DUP <50.0 <82.0 <76.0 <60.0 <80.0 <42.0 <48.0 <84.0 <52.0 <62.0 <72.0 6,450 <46.0 7318/21/2014 <0.25 <0.41 <0.38 0.45 J <0.40 0.49 J 0.44 J <0.42 <0.26 <0.31 <0.36 164 <0.23 0.30 J3/11/2015 <0.25 <0.41 <0.38 <0.30 <0.40 0.88 J <0.24 <0.42 <0.26 <0.31 <0.36 5.1 <0.23 ND8/5/2015 <0.25 <0.41 <0.38 <0.30 <0.40 0.52 J <0.24 <0.42 <0.26 <0.31 <0.36 0.78 J <0.23 ND8/1/2016 <0.25 <0.41 <0.38 3.6 <0.40 0.78 J <0.24 <0.42 <0.26 0.32 J <0.36 99.11.3 0.62 J8/16/2017 <1.2 <2.0 <1.9 2.2 J <2.0 <1.0 <1.2 <2.15.1<1.6 <1.8 1,840 <1.2ND8/8/2018 <0.25 <0.41 <0.38 0.30 J <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36 99.6 0.23 J ND8/7/2019 <0.15 <0.23 <0.20 <0.26 <0.20 3.0 <0.35 <0.18 <0.24 <0.17 <0.20 <0.41 <0.22 ND8/6/2020 <0.15 <0.23 <0.20 <0.26 <0.20 <0.28 <0.35 <0.18 <0.24 <0.17 <0.20 <0.41 <0.22 ND8/21/2021 <0.34 <0.49 <0.40 <0.30 <0.33 <0.42 <0.64 <0.34 <0.48 <0.50 <0.33 <0.71 <0.34 NDNotes are provided on the final page of this table.TYPE II MONITORING WELLS (Continued)KMW-546,000 (Total Xylenes)19,000 (Total Xylenes)76,000 (Total Xylenes)980 (Total Xylenes)<1.3 (Total Xylenes)12,000 (Total Xylenes)11 (Total Xylenes)<2.0 (Total Xylenes)150 (Total Xylenes)<2.0 (Total Xylenes)<2.0 (Total Xylenes)Page 6 of 20
Appendix CHistorical Groundwater ResultsLoading Rack AreaFormer FHR North TerminalWilmington, North CarolinaSample ID Date Collected1 70 70 600 70 20 6 70 600 400 400 VariesToluene1,2,4-TrimethylbenzeneContaminant of ConcernBenzenen-Butylbenzenesec-ButylbenzeneEthylbenzene1,3,5-Trimethylbenzenem/p-Xyleneso-XyleneAll Other 8260B AnalytesGroundwater Clean-up Goal (ug/L)500Isopropylbenzene (Cumene)Methyl Tert Butyl Ether (MTBE)Naphthalenen-Propylbenzene9/17/01<4.4 <8.4 <6.2 410 <7.4 <9.3 <14 <7.166<9.7 <7.4 160,000 270501/3/02<250 <250 <250 <250 <250 <250 <250 <250 <250 <250 <250 19,000 <250 ND2/27/02<500 <500 <500 <500 <500 <500 <500 <500 <500 <500 <500 37,000 <500 ND2/28/0367<50<50<50<50<50<50<50<50<50<50 6,300 <50ND9/16/03<120 <120 <120 <120 <120 <120 <120 <120 <120 <120 <120 14,000 <120 ND2/19/04 <1,000 <1,000 <1,000 <1,000 <1,000 <10,000 <5,000 <1,000 <1,000 <1,000 <1,000 31,000 <1,000 ND8/5/2004<36<31<24<34<25<3173J<32<5436J<21 51,000 75ND2/17/05<54<38<60<62<6654J 110J <45<6277J<49ND8/23/05<54<38<60<62<66<45<12<45<62<44<49ND2/10/06<54<38<60<62<66<4579J<45<62140<49ND8/7/20061.3 <0.38 0.90 J 271.61.0 J5.11.74.56.41.9ND2/7/2007 <0.54 <0.38 <0.60 44 <0.66 <0.45 9.42.26.712 <0.497.7 J8/9/2007<64<66<58<60<54 <120 <54<68<62<54<56ND2/26/2008 <640 <660 <580 <600 <540 <1200 <540 <680 <620 <540 <560ND8/19/2008 <64<66<58<60<54 <120 <54<68<62<54<56ND8/18/2009 <100 <100 <100 <100 <100 <100 <100 <100 <100 <100 <10035,400<100 9485/13/2010 34.6 J <100 <100 49.6 J <100 <100 <100 <100 77.7 J <100 <10024,70047.0 J 1,1008/12/2010 <100 <100 <100 57.8 J <100 <100 <100 <100 <100 <100 <10033,10048.9 J 1,1228/18/2011 <25.0 <41<38 38.2 J <40<21 24.2 J <42 42.4 J 38.1 J 60.3 J21,90069.7 J ND8/20/2012 <12.5 <20.5 <19.0 18.4 J <20.0 <10.5 <12.0 <21.0 <13.0 <15.5 <18.011,60016.4 J ND8/14/2013 <50.0 <82.0 <76.0 69.0 J <80.0 <42.0 <48.0 <84.0 <52.0 <62.0 <72.040,60056.8 J 360 J8/14/2014 <50.0 <82.0 <76.0 99.7 J <80.0 <42.0 <48.0 <84.0 <52.0 <62.0 <72.061,30078.6 J ND3/11/2015 <50.0 <82.0 <76.0 125 J <80.0 <42.0 <48.0 <84.0 <52.0 <62.0 <72.076,80095.6 J ND8/5/2015 <62.5 <102 <95.0 102 J <100 <52.5 <60.0 <105 <65.0 <77.5 <90.069,500102 J ND8/1/2016 <50.0 <82.0 <76.0 78.8 J <80.0 <42.0 <48.0 <84.0 <52.0 <62.0 <72.045,60066.6 J ND10/6/2016<50.0NANA<60.0NANANANA<52.0NANA27,400 <46.0NA11/23/2016<50.0NANA90.9 JNANANANA<52.0NANA57,800 79.2 JNA3/2/2017<62.5<102 <95.093.8 J<100 <52.5 256 <105<65.0<77.5 <90.048,400 66.2 JND4/26/2017<62.5 NANA 81.2 J NANANANA 86.8 J NANA 45,000 72.8 JNA8/9/2017<50.0<82.0 <76.060.6 J <80.0<42.0 <48.0 <84.079.0 J 148 J <72.0 43,500 93.7 JND3/7/2018 <50.0 NANA 106 J NANANANA <52.0 NANA 73,700 96.6 J NA5/23/2018 <62.5 NANA 125 J NANANANA <65.0 NANA 67,700 115 J NA8/8/2018 <50.0<82.0 <76.062.9 J <80.0<42.0 <48.0 <84.0<52.0<62.0 <72.040,900 66.4 J ND2/5/2019 <30.0 NANA 72.6 J NANANANA <48.8 NANA 40,200 <44.0 NA8/7/2019 <30.0 <46.8 <40.2 60.8 J <40.2 <55.0 <70.4 <37.0 <48.8 <34.0 <39.4 28,900 55.6 J ND8/6/2020 <15.0 <23.4 <20.1 34.6 J <20.1 <27.5 <35.2 <18.5 <24.4 <17.0 <19.7 19,700 26.0 J ND8/22/2021 <8.6 <12.2 <10.0 <7.6 <8.3 <10.6 <16.1 <8.5 <12.1 <12.4 <8.3 7,120 <8.4NDNotes are provided on the final page of this table.TYPE II MONITORING WELLS (Continued)KMW-68,100 (Total Xylenes)19,000 (Total Xylenes)13,000 (Total Xylenes)12,000 (Total Xylenes)16,000 (Total Xylenes)25,000 (Total Xylenes)41,000 (Total Xylenes) 62,000 (Total Xylenes) Page 7 of 20
Appendix CHistorical Groundwater ResultsLoading Rack AreaFormer FHR North TerminalWilmington, North CarolinaSample ID Date Collected1 70 70 600 70 20 6 70 600 400 400 VariesToluene1,2,4-TrimethylbenzeneContaminant of ConcernBenzenen-Butylbenzenesec-ButylbenzeneEthylbenzene1,3,5-Trimethylbenzenem/p-Xyleneso-XyleneAll Other 8260B AnalytesGroundwater Clean-up Goal (ug/L)500Isopropylbenzene (Cumene)Methyl Tert Butyl Ether (MTBE)Naphthalenen-Propylbenzene9/17/01370<10<1088<10330481245012036570330 BQL1/3/021605.4<5.024<5.09419<5.044207.110016ND2/27/02270 <5.03241<5.0 110415.52103331180140ND2/28/03120 <5.0 <5.074<5.05.4327.831403318020ND9/16/03300 <5.0 <5.0 18012<5.0 1502214170625608.2ND2/19/04110<10<1012012<100 19026<1041011060012ND8/5/2004140 <1.6 <1.2 14010<1.6 200195.81503433028ND2/17/05966.52.418016 <0.45 200306.817024ND8/23/05307.33.3130161.1J180285.711013ND2/8/0634205.8250235.2J43050112908549.68/7/20067<0.38 1.710011 0.73 J 170 B 205.25112ND2/7/2007 0.94 J <0.38 3.117022 <0.45 200423.95521ND8/9/2007 0.35 J 4.32.35915 <0.58 130274.44.64.99.4 J2/26/2008 <0.32 <0.33 2.73615 <0.58 79282.87.43.5ND8/19/2008 <0.32 6.12.73515 <0.58 69284.22.13.25.1 J8/18/2009 <1.0 <1.0 <1.0 52.4 10.1 <1.0 11315.43.23.0<1.015.81.8ND8/12/2010 <1.0 <1.0 <1.06613.9 <1.0 13421.7 <1.07.54.653.32.944.58/18/2011 <0.25 <0.41 <0.38 11634.4 <0.21 25355.61.644.7 <0.36 1214.9ND8/20/2012 <0.25 <0.41 <0.38 10.04.4 <0.21 49.26.5 <0.26 1.61.313.8 0.76 J ND8/14/2013 <0.25 <0.41 1.110.77.3 <0.21 78.5 10.6 <0.26 2.32.426.71.1ND8/14/2013 DUP <0.25 <0.41 <0.38 12.47.9 <0.21 88.6 11.4 <0.26 2.82.628.81.2ND8/14/2014 <0.25 <0.41 5.57.813.1 0.22 J 7.026.5 <0.26 <0.31 3.29.5 0.26 J 1.53/11/2015 <0.25 <0.41 <0.38 6.510.4 <0.21 9.919.3 <0.26 <0.31 2.37.0 0.40 J ND8/5/2015 <0.25 2.22.37.112.5 <0.21 12.5 24.7 <0.26 2.42.04.5 0.32 J ND8/1/2016 <0.25 0.89 J 0.79 J 2.54.0 <0.21 4.58.4 <0.26 1.2 0.77 J 1.4 J <0.23 ND10/6/2016 <0.25 NANA2.3NANANANA <0.26 NANA1.1 J <0.23 NA3/2/2017 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 0.56 J8/7/2017 <0.25 <0.41 0.61 J 1.12.9 <0.21 <0.24 5.3 <0.26 0.37 J <0.36 0.82 J <0.23 ND3/7/2018 <0.25 NANA1.7NANANANA <0.26 NANA1.7 J <0.23 NA5/23/2018 <0.25 NANA 0.65 J NANANANA <0.26 NANA 0.85 J <0.23 NA8/7/2018 <0.25 <0.41 <0.38<0.30 <0.400.28 J<0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23ND8/7/2019 <0.15 <0.23 1.30.87 J 4.41.4<0.35 6.5 <0.24 <0.17 <0.20 1.2 J <0.22ND8/6/2020 <0.15 <0.23 0.76 J<0.26 2.8<0.280.56 J 3.4 <0.24 <0.17 0.31 J 5.0 <0.22ND8/23/2021 <0.34 <0.49 <0.40<0.30 1.9<0.42<0.64 2.3 <0.48 <0.50 <0.33 <0.71 <0.34NDNotes are provided on the final page of this table.TYPE II MONITORING WELLS (Continued)KMW-7350 (Total Xylenes)220 (Total Xylenes)590 (Total Xylenes)130 (Total Xylenes)220 (Total Xylenes)36 (Total Xylenes)21 (Total Xylenes)17 (Total Xylenes)Page 8 of 20
Appendix CHistorical Groundwater ResultsLoading Rack AreaFormer FHR North TerminalWilmington, North CarolinaSample ID Date Collected1 70 70 600 70 20 6 70 600 400 400 VariesToluene1,2,4-TrimethylbenzeneContaminant of ConcernBenzenen-Butylbenzenesec-ButylbenzeneEthylbenzene1,3,5-Trimethylbenzenem/p-Xyleneso-XyleneAll Other 8260B AnalytesGroundwater Clean-up Goal (ug/L)500Isopropylbenzene (Cumene)Methyl Tert Butyl Ether (MTBE)Naphthalenen-Propylbenzene9/17/013,400 <200 450840 <200 6,300 530 <200 600 2,300 580 12,000 650 BQL1/3/021,300 <100 <100 190 <100 3,700 180130 <100 390130930 <100 ND2/27/022/28/031,400 <250 <250 550 <250 1,400 320 <250 <250 1,700 630 8,000 340ND9/16/031,900 <250 <250 670 <250 1,600 480 <250 680 1,200 390 5,900 450ND2/19/042,600 <100 <100 990 <100 <1,000 680110820 1,400 380 8,800 670ND8/5/2004560<31<2443040J 200J 56060J200 1,200 310 5,500 580ND2/17/05620 <7.614J4806833069013082860240ND8/17/052/9/06900<19<3078047J 360J 68092160 1,300 320ND8/7/2006340 <7.6 <1264067130 J 520 B 150811,100 300ND2/7/20078/9/2007520421239068140 480 B 130511,100 310ND2/26/2008 630 <0.33 9.84606879470120481,600 43069.84 J8/19/20088/18/2009 265 <1.0 <1.0 30377.8 17.859114620.79002841,770 56.0327.98/12/2010 <1.0 0.74 J 0.73 J <1.0 0.47 J <1.0 <1.01.1<1.0 0.49 J 0.48 J<2.0 <1.0ND8/18/2011 19623<1.9 93.2 38.8 1.1 J 13377.4 12.133215964220.83.4 J8/20/2012 91.8 <1.0 <0.95 27.8 16.1 0.57 J 41.5 37.13.883.5 28.31454.564.48/14/2013 27142.546320430.4 <4.2 24461.0 20.95131201,630 54.954.7 J8/14/2014 169 <2.01.927933.5 <1.0 17347.0 15.938594.81,060 35.8ND3/11/2015 89.1 <0.41 <0.38 19530.3 0.45 J 15151.37.5154 <0.3637125.960.94 J8/5/201515.6 <0.82 <0.76 51.9 23.3 <0.42 11232.72.224553.12026.71,0428/1/201676.9 <0.82 2.644.0 24.3 0.68 J 61.9 28.42.416116.61908.910.3 J10/6/2016 55.2NANA14.1NANANANA1.2NANA32.23.3NA11/23/2016 83.7NANA31.4NANANANA 0.88 J NANA59.86.2NA3/2/201714.7 <0.41 <0.38 7.81.8 <0.21 15.92.4 0.37 J 70.59.618.52.8 27.86 J4/26/20174.7NANA1.4NANANANA <0.26 NANA56.3 0.67 J NA8/9/201713.9 <0.41 <0.38 6.63.7 <0.21 30.42.9 0.35 J 101 <0.36 15.33.3ND3/7/201852.6NANA17.4NANANANA 0.80 J NANA31.94.2NA5/23/2018 20.8NANA1.4NANANANA <0.26 NANA6.23.8NA8/8/201844.1<0.41 <0.3821.4 10.2 0.76 J 59.4 <0.42 0.55 J 178 <0.36 16.74.5 3.69 J2/5/201956.2NANA12.3NANANANA 0.44 J NANA37.12.3NA8/7/201935.5 <0.23 <0.20 16.17.2 <0.28 12.76.0 0.95 J 32.1 <0.20 8.82.626.28/6/202042.6 <0.23 <0.20 11.16.4 <0.28 11.74.5 0.94 J 40.44.920.32.3 14.3 J8/22/2021 44.91.74.89.122.9 <0.42 6.422.5 <0.48 9.01.95.7 <0.34 ND9/17/016,200 <200 260 2,800 <200 3,900 540360 1,100 1,000 <200 3,700 440 BQL1/3/022/27/022/28/039/16/031,200 <250 <250 2,000 <250 540660340 1,200 2,700 830 10,000 1,200 ND2/19/04560 <200 <200 830 <200 <2,000 <1,000 <200 310 1,400 330 6,900 640ND8/5/0460045J<2493089J 100J 550170280 1,500 350 5,900 510ND2/17/05Notes are provided on the final page of this table.TYPE II MONITORING WELLS (Continued)KMW-80.17' FREE-PHASE PRODUCT2,100 (Total Xylenes)0.12' FREE-PHASE PRODUCT6,500 (Total Xylenes)4,100 (Total Xylenes)0.10' FREE-PHASE PRODUCT3,600 (Total Xylenes)2,800 (Total Xylenes)0.04' FREE-PHASE PRODUCTKMW-90.21' FREE-PHASE PRODUCT0.12' FREE-PHASE PRODUCTNOT MEASURED, WELL DAMAGED/WELL WAS REPLACED ON 7/2/03WELL PERMENANTLY ABANDONEDPage 9 of 20
Appendix CHistorical Groundwater ResultsLoading Rack AreaFormer FHR North TerminalWilmington, North CarolinaSample ID Date Collected1 70 70 600 70 20 6 70 600 400 400 VariesToluene1,2,4-TrimethylbenzeneContaminant of ConcernBenzenen-Butylbenzenesec-ButylbenzeneEthylbenzene1,3,5-Trimethylbenzenem/p-Xyleneso-XyleneAll Other 8260B AnalytesGroundwater Clean-up Goal (ug/L)500Isopropylbenzene (Cumene)Methyl Tert Butyl Ether (MTBE)Naphthalenen-Propylbenzene2/2/2015<6.2 <10.2 <9.5 77448.2 <5.2 39610740.629796.3541 8.5 J 47.9 J3/11/2015 1.4 J 24.0 <1.9 53559.8 <1.0 38510234.315439.1364 4.9 J ND8/5/2015 0.91 J 13.5 <0.76 <0.60 54.4 <0.42 14678.1 24.9 76.9 14.8 45.5 1.7 J 43.9 J8/1/2016 <0.62 7.07.628861.6 <0.52 22967.4 23.3 97.4 20.31052.7 44.3 J10/6/2016 <0.25 NANA46.0NANANANA5.5NANA17.7 0.64 J NA8/9/2017 <0.25 7.0 <0.38 37.9 18.3 <0.21 48.1 31.8 0.86 J 53.9 12.95.0 0.52 J ND8/8/2018 <0.25 <0.41 <0.38 2.52.4 <0.21 5.21.7 0.39 J 5.91.23.3 <0.23 ND8/7/2019 <0.15 9.1 <0.20 20.1 64.1 <0.28 11034.25.111531.4 33.74.433.58/6/2020 <0.15 1.0 <0.20 0.68 J 3.2 <0.28 21.0 <0.18 0.49 J 13.74.48.9 0.56 J 0.39 J8/23/2021 <0.34 <0.49 <0.40 <0.30 <0.33 <0.42 3.6 <0.34 <0.48 <0.50 <0.33 <0.71 <0.34 ND9/17/0188<20<20<20<20750<20<20<20<20<20<40<20 BQL1/3/0237<10<1012<1012015<101812<103718ND2/27/0232<10<10<10<106910<10<10<10<10<20<10ND2/28/03<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0ND9/16/03<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <10 <5.0ND2/19/04440<10<1019019<100 140302819038260<10ND8/5/04365.32.2299.32.4J94203.2779.617 0.69 J 6.29 J2/17/05<0.5410.62J <0.62 1.6 <0.45 6.51.4 <0.62 0.45J <0.49ND8/23/056<0.38 0.79J <0.62 2.3 <0.45 1.7J 0.46J <0.62 <0.44 <0.49ND2/9/06<0.54 <0.38 <0.60 <0.62 0.91J <0.45 <0.12 <0.45 <0.62 <0.44 <0.49ND8/7/2006 <0.54 <0.38 2.44.316 <0.45 39 B20 <0.62 11014ND2/7/2007 <0.54 <0.38 1.3 <0.62 5.3 <0.45 139.7 <0.62 275.2ND8/9/2007<5.02.31.8 <0.30 1.2 <0.58 2.5 J5.5 <0.31 0.45 J 0.76 JND2/26/2008 <0.32 <0.33 0.84 J <0.30 1.2 <0.58 <0.27 2.2 <0.31 <0.27 <0.28ND8/19/2008 0.70 J <0.33 2.6 <0.30 5.1 <0.58 1.7 J5.3 <0.31 <0.27 <0.28ND9/17/01110<80<80610<80<8089<80 2,000 650130 2,500 1,200 BQL1/3/02<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.01911ND2/27/026<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0325.2<5.081<5.0ND2/28/03<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0ND9/16/03<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <10 <5.0ND2/19/04<1.0 <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND8/5/04<0.36 <0.31 <0.24 <0.34 <0.25 <0.31 <0.44 <0.32 <0.54 <0.19 <0.21 <0.4 <0.3ND2/17/05<0.54 <0.38 <0.60 <0.62 <0.66 <0.45 <0.12 <0.45 <0.62 <0.44 <0.49ND8/23/05<0.54 <0.38 <0.60 <0.62 <0.66 <0.45 0.29J <0.45 <0.62 <0.44 <0.49ND2/8/06<0.54 <0.38 <0.60 <0.62 <0.66 <0.45 <0.12 <0.45 <0.62 <0.44 <0.49ND8/7/2006 <0.54 <0.38 <0.60 <0.62 <0.66 <0.45 0.64 JB <0.45 <0.62 <0.44 <0.49ND2/7/2007 <0.54 <0.38 <0.60 <0.62 <0.66 <0.45 0.44 J <0.45 <0.62 <0.44 <0.49ND3/11/2014 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 NDNotes are provided on the final page of this table.TYPE II MONITORING WELLS (Continued)KMW-9RKMW-10<1.6 (Total Xylenes)<1.3 (Total Xylenes)<1.3 (Total Xylenes)13 (Total Xylenes)2.4 (Total Xylenes)<0.87 (Total Xylenes)<0.87 (Total Xylenes)<0.87 (Total Xylenes)KMW-11<1.6 (Total Xylenes)<1.3 (Total Xylenes)<1.3 (Total Xylenes)<1.3 (Total Xylenes)<1.3 (Total Xylenes)COULD NOT LOCATE DURING AUGUST 2014 EVENT - PRESUMED DESTROYEDPage 10 of 20
Appendix CHistorical Groundwater ResultsLoading Rack AreaFormer FHR North TerminalWilmington, North CarolinaSample ID Date Collected1 70 70 600 70 20 6 70 600 400 400 VariesToluene1,2,4-TrimethylbenzeneContaminant of ConcernBenzenen-Butylbenzenesec-ButylbenzeneEthylbenzene1,3,5-Trimethylbenzenem/p-Xyleneso-XyleneAll Other 8260B AnalytesGroundwater Clean-up Goal (ug/L)500Isopropylbenzene (Cumene)Methyl Tert Butyl Ether (MTBE)Naphthalenen-Propylbenzene1/3/022/27/02 1,400 <5.0 14 190 77 670 200 160 39 760 130 1,800 47 Varies2/28/03 3,500 <250 <250 730 <250 990 340 <250 <250 1,100 360 5,800 <250 ND9/16/03 2,000 <250 <250 680 <250 <250 370 <250 <250 950 290 4,400 <250 ND2/19/04 2,400 <500 <500 1,600 <500 <5,000 <2,500 <500 <500 2,700 670 13,000 <500 ND8/5/04 1,800 <77 <60 1,500 170J 160J 1,300 340 220J 3,400 860 12,000 120 J ND2/17/05 1,600 <76 52 810 180 150J 940 380 64 2,100 510 ND8/22/05 1,700 <7.6 30 770 130 140J 1,100 230 73 2,700 680 ND2/8/06 2,000 <1.9 12 1,100 100 28J 920 160 68 2,200 470 56.48/7/2006 1,200 <7.6 <12 1,100 140 27 J910260482,100 420ND2/7/2007 1,000 <0.38 <0.60 920140111,200 180492,600 600ND8/9/2007630521842015010740310411,200 19021 J2/26/2008 480 <3.317180120 8.1 J 370 B 24025830130ND8/19/2008 4404717170110 6.8 J 380210256609328.5 J2/12/2009 450381588100 <2.9 1802101831049ND5/13/2009 26041159694<1023021011500100418/18/2009 331 <20.0 <20.0 10295.1 <20.0 315204 <20.0 45159.9154 <20.0 ND8/12/2010 95928.7 <2.0 1151422.716325969.421830.3 58.54.7 239.98 J8/18/2011 21123.7 12.6 70.4114 0.99 J 92.520323.1 81.6 <0.72 34.532208/20/2012 46320.7 <0.76 158106 1.6 J 38718315.739279.2 92.33.6ND8/14/2013 68.6 <0.41 <0.38 51.8 24.2 <0.21 11946.33.140.7 19.0 10.4 0.67 J 1.3 J3/11/2014 308 <0.41 9.614990.7 0.79 J 54913615.4 29.4 29.3 21.82.617.68/14/2014 182 <0.41 <0.38 12452.8 0.74 J 47980.8 10.011286.7 31.21.911.08/5/20158/1/20161246.812.9989126 <1.0 99120859.9 32.8 16.5138 3.4 J 9.2 J10/6/2016 176NANA405NANANANA36.9NANA36.2 1.4 JNA11/23/2016 233NANA878NANANANA41.3NANA134 4.4 JNA3/2/2017120 <4.1 <3.8 951108 8.4 J 91816738.1 45.0 13.9204 5.0 J 18.8 J4/26/2017 118NANA464NANANANA17.7NANA59.5 2.6 JNA8/9/2017107 <2.0 <1.9 32237.1 <1.0 82943.4 13.1 <1.6 36.3 43.1 2.4 J ND3/7/2018121NANA647NANANANA9.8NANA45.76.3NA5/23/2018 36.4NANA331NANANANA1.5 JNANA21.6 4.1 JNA8/8/201876.2 <0.82 <0.76 11116.7 <0.42 22226.52.9 <0.62 10.38.42.175.52/5/201977.0NANA556NANANANA22.9NANA74717.8NA8/6/202029.8 <0.47 <0.40 64.2 11.9 <0.55 27325.62.032.89.021.93.0ND8/22/2021 13.1 <0.49 <0.40 6.3<0.33<0.42 50.9 <0.34 <0.48 2.47.711.7<0.34 NDNotes are provided on the final page of this table.TYPE II MONITORING WELLS (Continued)KMW-120.30' FREE PHASE PRODUCT2,000 (Total Xylenes)4,800 (Total Xylenes)4,100 (Total Xylenes)310 (Total Xylenes)<1.3 (Total Xylenes)440 (Total Xylenes)540 (Total Xylenes)290 (Total Xylenes)140 (Total Xylenes)310 (Total Xylenes)COULD NOT SAMPLE - WELL WAS DRYPage 11 of 20
Appendix CHistorical Groundwater ResultsLoading Rack AreaFormer FHR North TerminalWilmington, North CarolinaSample ID Date Collected1 70 70 600 70 20 6 70 600 400 400 VariesToluene1,2,4-TrimethylbenzeneContaminant of ConcernBenzenen-Butylbenzenesec-ButylbenzeneEthylbenzene1,3,5-Trimethylbenzenem/p-Xyleneso-XyleneAll Other 8260B AnalytesGroundwater Clean-up Goal (ug/L)500Isopropylbenzene (Cumene)Methyl Tert Butyl Ether (MTBE)Naphthalenen-Propylbenzene1/3/022/27/02 690 <5.0 <5.0 140 24 1,800 160 46 34 100 38 35,000 74 ND2/28/03 690 <1,200 <1,200 <1,200 <1,200 1,100J <1,200 <1,200 <1,200 210J <1,200 19,000 <1,200 ND9/16/03 <1,000 <1,000 <1,000 <1,000 <1,000 <1,000 <1,000 <1,000 <1,000 <1,000 <1,000 20,000 <1,000 ND2/19/04 <1,000 <1,000 <1,000 <1,000 <1,000 <10,000 <5,000 <1,000 <1,000 <1,000 <1,000 71,000 <1,000 ND8/5/04 <180 <160 <120 <170 <120 <160 <220 <160 <270 <95 <100 68,000 <180 ND2/17/05 920 <76 <120 <120 <130 120J 240J <90 <120 270 <98 ND8/22/05 340 <38 <60 150 <66 58J 610 <45 <62 140 <49 ND2/8/06 450 <38 <60 <62 <66 <45 160J <45 <62 130 <49 ND8/7/2006 740 <190 <300 <310 <330 <230 160 JB <230 <310 <220 <250ND2/7/2007230 <0.38 <0.60 691.44168216288.420.78/9/2007680<83<73280<68 <150 120 J <85 160 J 150 J <70ND2/26/2008 620<83<73<75<68 <150 190 J <85 110 J 170 J <70ND8/19/2008 370 J <160 <140 280 J <140 <290 <140 <170 <160 190 J <140ND2/12/2009 310 J <160 <140 290 J <140 <290 210 J <170 <160 310 J <140ND5/13/2009 <64<66<5874<54 <120 <54<68<6280<56ND8/18/2009 162 <1.0 <1.0 13412.01.298.6 14.2 25.317543.157,40072.8ND8/12/2010 77.5 J <200 <200 <200 <200 <200 <200 <200 <200 67.7 J <20022,900100 1,5508/18/2011 63.8 J <82<76 188 J <80<42476 120 J <52 150 J <7265,400108 J ND8/20/2012 <50.0 <82.0 <76.0 <60.0 <80.0 <42.0 <48.0 <84.0 <52.0 134 J <72.060,500119 J ND8/14/2013 <50.0 <82.0 <76.0 256 <80.0 <42.0 549 <84.0 <52.0 195 J <72.073,70086.5 J 5103/11/2014 137 J <102 <95.0 336 <100 <52.5 2,270 180 J 309 217 J <90.063,600178 J 48.2 J8/14/2014 54.5 J <41.0 <38.0 99.6 J <40.0 <21.0 58.1 J <42.0 71.6 J 134 <36.025,70025.9 J 33.2 J3/11/2015 38.5 J <51.2 <47.5 328 <50.0 <26.2 163 <52.5 <32.5 222 <45.090,90049.9 J ND8/5/2015 <62.5 <102 <95.0 271 <100 <52.5 326 <105 <65.0 229 J <90.066,400<57.5 ND8/2/2016 <25.0 <41.0 <38.0 132 <40.0 <21.0 193 <42.0 <26.0 202 38.4J21,300<23.0 ND10/6/2016 <12.5 NANA107NANANANA 16.4 J NANA 13,800 <11.5 NA11/23/2016 25.7 J NANA244NANANANA 34.5 J NANA 20,400 <23.0 NA3/2/2017 <12.5 <20.5 <19.0 57.5 65.9 <10.5 24281.8 20.8 J 997210 4,370 <11.5 ND4/26/2017 <12.5 NANA82.2NANANANA 18.9 J NANA 11,400 <11.5 NA8/29/2017 0.38 J <0.41 <0.38 0.46 J 0.73 J <0.21 1.7 0.69 J 0.32 J 1.6 <0.36 92.7 0.35 J 18.25 J3/12/2018 <25.0 NANA 83.2 J NANANANA <26.0 NANA 11,200 <23.0 NA5/23/2018 <10.0 NANA63.8NANANANA <10.4 NANA 9,330 <9.2NA8/8/20181.7<0.41 <0.383.64.2<0.216.34.8 0.67 J 8.9 <0.36 379 0.88 J 9.0 J2/5/2019 3.6 JNANA40.1NANANANA<1.2NANA1,3402.3 JNA8/7/2019 1.5 J0.58 0.50 19.7 11.1 <0.69 47.0 16.4 <0.61 81.7 11.59051.0 J 45.5 J8/6/20203.42.2 J <0.50 17.6 27.4 <0.69 63.5 41.9 <0.61 61.3 14.66021.6 J ND8/23/2021 <0.86<1.22.66.415.6 <1.1 22.1 22.8 <1.25.4 <0.83704<0.84 20.9Notes are provided on the final page of this table.TYPE II MONITORING WELLS (Continued)KMW-132.51' FREE PHASE PRODUCT57,000 (Total Xylenes)71,000D (Total Xylenes)72,000 (Total Xylenes)100,000 (Total Xylenes)19,000 (Total Xylenes)83,000 (Total Xylenes)78,000 (Total Xylenes)88,000 (Total Xylenes)96,000 (Total Xylenes)27,000 (Total Xylenes)Page 12 of 20
Appendix CHistorical Groundwater ResultsLoading Rack AreaFormer FHR North TerminalWilmington, North CarolinaSample ID Date Collected1 70 70 600 70 20 6 70 600 400 400 VariesToluene1,2,4-TrimethylbenzeneContaminant of ConcernBenzenen-Butylbenzenesec-ButylbenzeneEthylbenzene1,3,5-Trimethylbenzenem/p-Xyleneso-XyleneAll Other 8260B AnalytesGroundwater Clean-up Goal (ug/L)500Isopropylbenzene (Cumene)Methyl Tert Butyl Ether (MTBE)Naphthalenen-Propylbenzene1/3/028.5<5.0 <5.0 <5.0 <5.038<5.0 <5.0 <5.0 <5.0 <5.0 2,900 <5.0ND2/27/026.9<5.0 <5.06652713<5.0 <5.02511 30,000 59ND2/28/03<120 <120 <120 <120 <120 <120 <120 <120 <120 <120 23,000 <120 ND9/16/03<500 <500 <500 45,000 <500 <500 <500 <500 <500 <500 <500 38,000 <500 ND2/19/04 <1,000 <1,000 <1,000 <1,000 <1,000 <10,000 <5,000 <1,000 <1,000 <1,000 <1,000 62,000 <1,000 ND8/5/04<180 <160 <120 <170 <120 <160 400J <160 <270 140J <100 50,000 <180 ND2/17/05<54<38<60<62<66<4542J<45<62<44<49ND8/22/05<54<38<6074J<66<45<12<45<62<44<49ND2/8/06<54<38<60<62<66<45<12<45<62<44<49ND8/7/2006 <110 <76 <120 <120 <130 <90 72 JB <90 <120 <88<98ND2/7/2007 0.74 J <0.38 <0.60 8.3 0.86 J <0.45 121.8 <0.62 184.90.65 J8/9/2007<32<33<29<30<27<5872 J<34<3145 J<28ND2/26/2008 <6.4 <6.6 <5.8 <6.0 <5.4 <12 11 JB <6.8 6.9 J 16 J <5.6ND8/19/2008 <6.4 <6.6 <5.8 15 J <5.4 <1212 J <6.8 <6.2 16 J 6.8 JND2/12/2009 <32<33<29<30<27<58 100 J <34<3133 J<28ND5/13/2009 <16<16<1422<14<29<14<17<1622<143508/18/20091.1<1.0 <1.0 13.42.0<1.0 11.82.7<1.0 27.38.78,0403.7ND5/13/2010 <20.0 <20.0 18.6 J <20.0 <20.0 <20.0 6.8 J <20.0 <20.0 21.7 7.4 J3,440<20.0 ND8/12/2010 <25.0 <25.0 <25.0 9.0 J <25.0 <25.0 <25.0 <25.0 <25.0 <25.0 <25.03,830<25.0 1928/18/2011 <1.2<2<1.9 1.8 J<21.5 J 4.6 J <2.1 <1.3 <1.6 <1.81,720<1.2ND8/20/2012 <1.2 <2.0 <1.9 <1.5 <2.0 <1.0 2.7 J <2.1 <1.3 <1.6 <1.82,9901.6 J ND8/14/2013 <2.5 <4.1 <3.8 8.9 J <4.0 <2.1 9.7 J <4.2 <2.6 8.0 J <3.66,430<2.3 26.93/11/2014 <0.25 <0.41 <0.38 <0.30 <0.40 0.21 J 0.43 J <0.42 <0.26 <0.31 <0.362.4<0.23 1.26 J8/14/2014 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 0.43 J <0.42 <0.26 <0.31 <0.36114<0.23 ND3/11/2015 <0.25 <0.41 <0.38 0.67 J <0.40 <0.21 0.73 J <0.42 <0.26 0.52 J <0.362960.46 J 3.08/5/2015 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.364.0<0.23 ND8/1/2016 <0.25 <0.41 <0.38 0.94 J <0.40 <0.21 0.84 J <0.42 <0.26 2.6 0.76 J15.70.78 J ND8/9/2017 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36<0.66<0.23 ND8/7/2018 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.3612.1<0.23 ND8/7/2019 <0.15 <0.23 <0.20 <0.26 <0.20 <0.28 <0.35 <0.18 <0.24 <0.17 <0.200.89 J<0.22 ND8/6/2020 <0.15 <0.23 <0.20 <0.26 <0.20 <0.28 <0.35 <0.18 <0.24 <0.17 <0.20167<0.22 ND8/22/2021 <0.34 <0.49 <0.40 <0.30 <0.33 <0.42 <0.64 <0.34 <0.48 <0.50 <0.33<0.71<0.34 NDNotes are provided on the final page of this table.TYPE II MONITORING WELLS (Continued)KMW-1421,000 (Total Xylenes)47,000D (Total Xylenes)14,000 (Total Xylenes)37,000 (Total Xylenes)6,200 (Total Xylenes)15,000 (Total Xylenes)4,800 (Total Xylenes)6,300 (Total Xylenes)20,000 (Total Xylenes)14,000 (Total Xylenes)Page 13 of 20
Appendix CHistorical Groundwater ResultsLoading Rack AreaFormer FHR North TerminalWilmington, North CarolinaSample ID Date Collected1 70 70 600 70 20 6 70 600 400 400 VariesToluene1,2,4-TrimethylbenzeneContaminant of ConcernBenzenen-Butylbenzenesec-ButylbenzeneEthylbenzene1,3,5-Trimethylbenzenem/p-Xyleneso-XyleneAll Other 8260B AnalytesGroundwater Clean-up Goal (ug/L)500Isopropylbenzene (Cumene)Methyl Tert Butyl Ether (MTBE)Naphthalenen-Propylbenzene8/23/05<1.1 <0.76 <1.2 <1.2 <1.330 <0.24 <0.90 <1.2 <0.88 <0.98ND10/14/05 <0.54 <0.38 <0.6 <0.62 <0.66 <0.45 <0.12 <0.45 <0.62 <0.44 <0.49 <1.3 <0.49 BQL2/9/06<0.54 <0.38 <0.60 <0.62 <0.66 380 <0.12 <0.45 <0.62 <0.44 <0.491.18/8/2006 <0.54 <0.38 <0.60 <0.62 0.79 J 634.9 J 0.54 J 115.21.4ND,0.354.7 <0.38 <0.60 1.2 <0.66 200 0.80 J 0.46 J <0.62 <0.44 <0.49ND3/30/2007 <0.54 <0.38 <0.60 0.84 J <0.66 99 <0.12 <0.45 <0.62 <0.44 <0.49ND8/17/20079.8<1.7 <1.5 <1.5 <1.4 47 J <1.4 <1.7 <1.6 <1.4 <1.4ND2/25/20082.4<1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0ND8/19/2008 <1.0 <1.0 <1.02.5<1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0ND2/12/2009 <1.0 <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0ND5/13/2009 <1.0 <1.0 <1.01.7<1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0ND8/18/2009 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 288 <1.0ND11/18/2009 <1.0 <1.0 <1.0 0.35 J <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 226 0.24 J ND5/13/2010 <1.0 <1.0 <1.0 <1.0 <1.07.3<1.0 <1.0 <1.0 <1.0 <1.0 152 <1.0ND8/12/2010 <1.0 <1.0 <1.0 <1.0 <1.0 0.33 J <1.0 <1.0 <1.0 <1.0 <1.05.6<1.0ND8/19/2011 <0.25 <0.41 <0.38 <0.3 <0.4 19.1 <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 6.4 J8/17/2012 <0.25 <0.41 <0.38 <0.30 <0.31 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 ND3/11/2014 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 ND8/23/050.80J <0.38 <0.60 <0.62 0.66J24 <0.12 <0.45 <0.62 <0.44 <0.49ND2/8/06190 <1.9 <3.0 <3.1 3.8 J 60013J8.63.2J8822ND8/7/200620 <0.38 <0.60 <0.62 4.119053.5 <0.62 154.3ND2/7/200731 <0.38 0.61 J <0.62 3.4437.86.71.64917ND8/9/20075.0 <0.33 0.73 J <0.30 3.437 1.0 JB 1.3 <0.31 6.41.4ND2/26/2008 0.38 J <0.33 <0.29 <0.30 0.89 J 9.7 J 0.89 J 0.55 J <0.31 2.7 0.97 J0.39 JB8/19/2008 <0.32 <0.33 <0.29 <0.30 <0.27 4.6 J <0.27 <0.34 <0.31 <0.27 <0.28ND8/18/2009 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0ND5/13/2010 <1.0 <1.0 0.40 J <1.0 <1.04.6<1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0ND8/12/2010 <1.0 <1.0 <1.0 <1.0 <1.0 0.70 J <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0ND8/23/05<0.54 <0.38 0.70J <0.62 3.28.8J 0.32J <0.45 <0.62 <0.44 <0.49ND2/8/06110 <0.38 <0.60 552.9202.8J3.63.7325.0ND8/7/20062.4 0.40 J 0.60 J <0.62 <0.66 1.4 J 0.81 J <0.45 <0.62 2.6 0.88 JND2/7/20073<0.38 1.4 <0.62 4.84.7 J6.82.3 <0.62 3612ND8/9/20073.51.61.8 <0.30 4.16.3 J 5.2 B 1.6 0.55 J 3814ND2/26/2008 <0.32 <0.33 <0.29 <0.30 1.14.1 J 2.7 J <0.34 <0.31 <0.27 <0.28ND8/19/2008 <0.32 <0.33 <0.29 <0.30 <0.27 1.2 J <0.27 <0.34 <0.31 <0.27 <0.2813 J8/18/2009 <1.0 <1.0 <1.0 <1.0 <1.02.9<1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0ND5/13/2010 <1.0 <1.0 <1.0 <1.0 <1.01.1<1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0ND8/12/2010 <1.0 <1.0 <1.0 <1.0 <1.01.7<1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0NDNotes are provided on the final page of this table.TYPE II MONITORING WELLS (Continued)KMW-15530 (Total Xylenes)<1.3 (Total Xylenes)1,300 (Total Xylenes)<1.3 (Total Xylenes)<1.3 (Total Xylenes)1,800 (Total Xylenes)51 (Total Xylenes)5,600 (Total Xylenes)40 (Total Xylenes)1,400 E (Total Xylenes)KMW-16<1.3 (Total Xylenes)7.0J (Total Xylenes)<1.3 (Total Xylenes)5.1 (Total Xylenes)1.4 J (Total Xylenes)<0.87 (Total Xylenes)<0.87 (Total Xylenes)KMW-17<1.3 (Total Xylenes)170 (Total Xylenes)4.8 (Total Xylenes)11 (Total Xylenes)16 (Total Xylenes)<0.87 (Total Xylenes)<0.87 (Total Xylenes)Page 14 of 20
Appendix CHistorical Groundwater ResultsLoading Rack AreaFormer FHR North TerminalWilmington, North CarolinaSample ID Date Collected1 70 70 600 70 20 6 70 600 400 400 VariesToluene1,2,4-TrimethylbenzeneContaminant of ConcernBenzenen-Butylbenzenesec-ButylbenzeneEthylbenzene1,3,5-Trimethylbenzenem/p-Xyleneso-XyleneAll Other 8260B AnalytesGroundwater Clean-up Goal (ug/L)500Isopropylbenzene (Cumene)Methyl Tert Butyl Ether (MTBE)Naphthalenen-Propylbenzene5/13/2010 10.8 <1.0 <1.0 14.1101.0 0.42 J 1.112.82.81.134.99.21.48/12/20101.9<1.0 <1.0 <1.07.31.9<1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 11.4 J8/19/2011 <0.25 <0.41 <0.38 <0.32.31.4 <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 9.8 J8/17/2012 <0.25 <0.41 <0.38 <0.30 <0.40 0.54 J <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 0.20 J8/13/20131.8 <0.41 <0.38 0.31 J 0.79 J 0.87 J <0.24 <0.42 <0.26 <0.31 <0.36 0.88 J <0.23 10.6 J8/21/20142.7 <0.41 <0.38 <0.30 1.1 0.93 J 0.25 J 0.49 J 0.28 J 2.2 0.73 J 6.4 0.26 J 2.4 J3/11/2015 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 0.35 J <0.42 <0.26 0.31 J <0.36 <0.66 <0.23 0.71 J8/5/2015 <0.25 <0.41 <0.38 <0.30 <0.40 0.44 J <0.24 <0.42 <0.26 <0.31 <0.36 0.70 J <0.23 0.73 J8/1/20165.3 <0.41 <0.38 0.87 J 2.9 0.89 J 2.12.7 0.71 J 3.3 0.82 J 5.4 0.43 J 1.73 J8/7/20176.7 <0.41 <0.38 0.77 J 6.5 0.69 J 4.06.6 0.87 J <0.31 <0.36 3.7 <0.23 0.16 J8/8/20182.8 <0.41 <0.38 8.04.9 0.70 J 4.04.6 0.79 J 16.9 <0.36 24.7 0.46 J ND8/7/2019 <0.15 <0.23 0.65 J <0.26 5.51.2 0.73 J <0.18 <0.24 <0.17 5.12.3 <0.22 2.78/6/2020 <0.15 <0.23 <0.20 <0.26 <0.20 0.32 J <0.35 <0.18 <0.24 <0.17 <0.20 8.9 <0.22 ND8/21/2021 <0.34 <0.49 <0.40 <0.30 <0.33 <0.42 <0.64 <0.34 <0.48 <0.50 <0.33 <0.71 <0.34 ND12/22/03<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.03.62.7<2.0 <1.02.22/19/04<1.0 <1.0 <1.0 <1.0 <1.0 <10.0 <5.0 <1.0 <1.0 <1.04.3<1.0 <1.0358/5/04<0.36 <0.3 <0.24 <0.34 <0.25 <0.31 <0.44 <0.32 <0.54 <0.19 1.2 <0.40 <0.35 ND2/16/05<0.54 2.5 <0.60 1.0 <0.66 3.0J <0.12 <0.45 <0.62 3.34.714.078/22/05<0.54 0.89J <0.60 <0.62 <0.66 <0.45 <0.12 <0.45 <0.62 <0.44 1.2ND2/8/06<0.54 0.38 <0.60 <0.62 <0.66 <0.45 <0.12 <0.45 <0.62 <0.44 <0.49ND8/7/2006 <0.54 <0.38 <0.60 <0.62 <0.66 83 <0.12 <0.45 <0.62 <0.44 2.54.2 J2/7/2007 <0.54 <0.38 <0.60 <0.62 <0.66 <0.45 <0.12 <0.45 <0.62 <0.44 0.55 J578/9/2007530 <1.3 <1.2 <1.2 <1.156<1.1 <1.4 200 <1.1 2.2 JND2/26/2008 270 <1.3 <1.25.3<1.1 25 J 2.7 J <1.450<1.1 <1.1ND8/19/2008 170 <1.6 <1.4 3.8 J 1.8 J 7.7 J 9.4 J <1.7 50017123.9 J8/18/2009 22.65.9<1.0 39.58.3<1.0 15.0 16.9 13.1 59.4 17.516465.0ND8/12/2010 12.9 0.85 J <1.03.6<1.09.2<1.0 <1.0 <1.0 <1.01<2.03.5ND8/18/20115.7 <0.41 <0.38 58.71.4 <0.21 2.2110.44.81.210.235.0 6.9 J8/20/20121.5 <0.41 <0.38 10.61.0 <0.21 <0.24 <0.42 0.60 J 0.99 J 1.02.215.2 1.2 J8/14/2013 <0.25 <0.41 <0.38 4.0 <0.40 <0.21 0.46 J <0.42 <0.26 <0.31 <0.361.6 J<0.23 ND8/14/2014 <0.25 <0.41 <0.38 2.7 <0.40 <0.21 0.80 J <0.42 <0.26 <0.31 <0.36<0.66<0.23 ND3/11/2015 <0.25 <0.41 <0.38 2.8 <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36<0.66<0.23 ND8/5/2015 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 0.26 J <0.42 <0.26 <0.31 <0.36<0.66<0.23 ND8/1/2016 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36<0.66<0.23 0.82 J8/8/2017 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36<0.66<0.23 ND8/8/2018 <0.25 <0.41 <0.38 <0.30 <0.40 <0.21 <0.24 <0.42 <0.26 <0.31 <0.36<0.66<0.23 0.28 J8/7/2019 <0.15 <0.23 <0.20 0.82 J <0.20 <0.28 0.37 J <0.18 0.45 J 0.65 J <0.204.81.3ND8/6/2020 <0.15 <0.23 <0.20 <0.26 <0.20 <0.28 <0.35 <0.18 <0.24 <0.17 <0.20<0.41<0.22 ND8/21/2021 <0.34 <0.49 <0.40 <0.30 <0.33 <0.42 <0.64 <0.34 <0.48 <0.50 <0.33<0.71<0.34 NDNotes are provided on the final page of this table.TYPE II MONITORING WELLS (Continued)KMW-18FHR TYPE II MONITORING WELLS WITHIN APEX TERMINALAMW-1<1.6 (Total Xylenes)<1.3 (Total Xylenes)<1.3 (Total Xylenes)<1.3 (Total Xylenes)<1.3 (Total Xylenes)<3.5 (Total Xylenes)21 (Total Xylenes)80 (Total Xylenes)Page 15 of 20
Appendix CHistorical Groundwater ResultsLoading Rack AreaFormer FHR North TerminalWilmington, North CarolinaSample ID Date Collected1 70 70 600 70 20 6 70 600 400 400 VariesToluene1,2,4-TrimethylbenzeneContaminant of ConcernBenzenen-Butylbenzenesec-ButylbenzeneEthylbenzene1,3,5-Trimethylbenzenem/p-Xyleneso-XyleneAll Other 8260B AnalytesGroundwater Clean-up Goal (ug/L)500Isopropylbenzene (Cumene)Methyl Tert Butyl Ether (MTBE)Naphthalenen-Propylbenzene12/22/03 1,700 <1.0 <1.0 1,400 130300660390 1,100 2,500 710 27,000 6805.22/19/042,200 <200 <200 1,700 <200 <2,000 <1,000 300 2,000 2,200 600 39,000 940ND8/5/042,300 <62<48 2,000 140J 440J 750J 260 1,900 2,100 560 40,000 970ND2/16/051,200 <38<60 1,300 130 130J 840260 1,700 2,100 490ND8/22/051,700 48J<60 1,300 120 190J 900230 1,000 1,300 340ND2/8/061,700 <76 <120 1,300 <130 <90 370J 140J 2,100 1,100 290ND8/7/2006 1,300 110 J <120 1,400 <130 200 J 540 JB <90 2,000 1,200 330ND2/7/2007790 <0.38 <0.60 7608086310180420 1,000 180ND8/9/2007580<66<5857070 J 120 J 250 J 130 J 120 J 680 180 JND2/26/2008 720<66<5896079 J 260 J 530 J 170 J 210 1,300 340ND8/19/2008 320<66<58410<54 140 J 250 J 100 J 82 J540 140 JND8/18/2009 305 <20.0 <20.0 50550.3 88.525492.2 59.271117050,900 175ND8/12/2010 645 <200 <200 956 93.0 J <200 400216 <200 79924428,900 107 J7838/18/2011 169<41<38493 48.2 J <21221 99.5 J 27547314231,800 349ND8/21/2012 209 <41.0 <38.0 529 72.3 J <21.0 299134 40.0 J 75619922,000 90.3 JND8/14/2013 225 <41.0 <38.0 740106 <21.0 421223 33.3 J 1,110 31715,500 37.2 J3233/11/2014 71.7 <10.2 <9.5 204 19.9 J 32.1 74.2 35.2 25.819354.49,500 28.4ND8/14/2014 166 <20.5 <19.0 32381.3 <10.5 168165 16.5 J 35196.412,900 <11.5ND3/11/2015 245 <20.5 <19.0 513106 <10.5 311205 25.0 J 59617713,300 12.7 JND8/5/2015155 <20.5 <19.0 78799.4 <10.5 370203 41.7 J 1,020 30215,100 40.8 JND8/1/2016 <10.0 <16.4 <15.2 44671.3 <8.4 21715457.4 1,290 3638,250 30811.7 J10/6/2016 <10.0 NANA405NANANANA94.2NANA 11,000 251NA8/9/2017<6.2 26.6 <9.5 35463.2 <5.2 17212933.6823170 6,170 182ND8/8/2018<2.5 <4.1 <3.8 20225.9 <2.1 92.0 68.6 <2.6 43892.7 2,610 58.5 16.9 J8/7/201922.4 <4.7 <4.0 44257.3 <5.5 178 <3.7 20.0717183 7,710 351ND8/6/202026.0 <5.8 <5.0 77791.2 <6.9 463 <4.6 23.4 J 1,440 371 8,180 174ND8/21/2021 <4.3 <6.1 <5.0 29627.8 <5.3 150 <4.2 <6.1 404101 3,750 57.2NDNotes are provided on the final page of this table.FHR TYPE II MONITORING WELLS WITHIN APEX TERMINAL (Continued)AMW-235,000 (Total Xylenes)25,000 (Total Xylenes)38,000 (Total Xylenes)50,000 (Total Xylenes)20,000 (Total Xylenes)26,000 (Total Xylenes)48,000 (Total Xylenes)38,000 (Total Xylenes)Page 16 of 20
Appendix CHistorical Groundwater ResultsLoading Rack AreaFormer FHR North TerminalWilmington, North CarolinaSample ID Date Collected1 70 70 600 70 20 6 70 600 400 400 VariesToluene1,2,4-TrimethylbenzeneContaminant of ConcernBenzenen-Butylbenzenesec-ButylbenzeneEthylbenzene1,3,5-Trimethylbenzenem/p-Xyleneso-XyleneAll Other 8260B AnalytesGroundwater Clean-up Goal (ug/L)500Isopropylbenzene (Cumene)Methyl Tert Butyl Ether (MTBE)Naphthalenen-Propylbenzene12/22/03220 <1.0 <1.030251056391289231,600 8.57.22/19/04170<50<5050<50 <500 <250 <50<50100<50 2,800 <50ND8/5/04230104.8J70434.6J170691394296705.8ND2/16/05360<19<3013042J<23 160J5934J25058ND8/22/05200114.260422896729.871293.8J2/8/06380<19<3073<33<2378J49J41J63<25ND8/7/2006560 <9.5 <1573395,900 120 JB 654909332ND2/7/2007410 <0.38 <0.60 550523226010060270130ND8/9/20073808.04.21603786 100 B 61493919ND2/26/200833 <0.66 2.4289.5241818868.58.3ND8/19/2008472.91.8 J135.9200 9.2 J9.33.77.71.8 J188/18/2009 45.5 <1.0 <1.0 24.95.38.737.95.93.928.6 16.713480.26.38/12/2010 51.2 <1.0 <1.0 28.34.937.0 10.44.21.910.78.3 1,320 35.1 6.29 J8/18/2011 112 <1.0 <0.95 91.9 25.3 1.9 J 80.73525514647.98418.5ND8/22/2012 28.2 <1.6 <1.5 <1.27.58.320.16.93.3 J 14.74.6 5,150 1.6 J 21.08/14/2013 93.6 <0.41 5.635.4 36.21.185.6 74.03.4 <0.31 43.0276 <0.23 22.0 J8/14/2014 47.8 <0.41 2.56.316.1 0.27 J 36.0 29.02.85.12.140.6 0.41 J ND3/11/2015 55.2 <0.41 <0.38 52.9 41.0 0.59 J 92.4 76.06.814.35.7 1,360 6.5ND8/5/201525.16.23.723.1 19.6 <0.42 34.4 36.44.511.2 <0.72 473 0.90 J 144.88/1/20161.8 <0.41 0.92 J 6.81.9 <0.21 7.03.82.015.4 10.7 80.35.6 0.67 J10/6/20162.3NANA8.1NANANANA1.5NANA57.17.1NA8/9/2017 0.76 J <0.41 <0.38 2.2 0.84 J <0.21 3.12.2 <0.26 <0.31 4.12.5 <0.23 ND8/8/20182.0 <0.41 <0.38 17.3 18.3 <0.21 42.0 43.02.017.8 26.73991.2 1.58 J8/7/2019 <0.30 3.53.717.5 15.1 <0.55 34.7 26.1 1.2 J 10.3 11.4398 <0.44 ND8/6/2020 1.5 J <0.47 3.726.2 13.2 0.74 J 14.0 22.14.516.99.13093.1ND8/22/2021 <0.69 <0.98 <0.80 7.918.1 <0.84 38.6 28.12.137.1 14.53532.615.3Notes are provided on the final page of this table.FHR TYPE II MONITORING WELLS WITHIN APEX TERMINAL (Continued)AMW-39,200 (Total Xylenes)530 (Total Xylenes)11,000 (Total Xylenes)4,100 (Total Xylenes)10,000 (Total Xylenes)500 (Total Xylenes)1,200 (Total Xylenes)2,000 (Total Xylenes)Page 17 of 20
Appendix CHistorical Groundwater ResultsLoading Rack AreaFormer FHR North TerminalWilmington, North CarolinaSample ID Date Collected1 70 70 600 70 20 6 70 600 400 400 VariesToluene1,2,4-TrimethylbenzeneContaminant of ConcernBenzenen-Butylbenzenesec-ButylbenzeneEthylbenzene1,3,5-Trimethylbenzenem/p-Xyleneso-XyleneAll Other 8260B AnalytesGroundwater Clean-up Goal (ug/L)500Isopropylbenzene (Cumene)Methyl Tert Butyl Ether (MTBE)Naphthalenen-Propylbenzene12/22/032001518111424026262.814011068<1.0362/19/04420<10132128110<5034172009398<10ND8/5/042/16/058/17/0510/14/05--------------2/8/068/8/20062/7/2007 16,000 <1,900 <3,000 <3,100 <3,300 570,000 <600 <2,300 34,000 <2,200 <2,500ND3/30/2007 20,000 <190 <300 2,400 <330 140,000 <60 <230 43,000 860 310 JND8/17/2007 15,000 <3340 J 2,200 220 31,000 120 J 260 33,000 1600 48033 JB2/25/2008 13,000 <66<58 2,000 130 34,000 150160 24,000 1,300 390ND8/19/2008 9,800 <66<58 3,200 280 31,000 80320 32,000 2,000 580ND2/12/2009 7,000 <66<58 2,100 160 1,300 150180 36,000 1,100 330ND8/18/2009 6,510 <250 <250 2,770 267 3,800 1,270 292 22,000 1,820 561 9,490 3,990 1,72011/18/2009 6,810 <200 <200 3,570 289 3,700 1,260 342 30,600 2,270 601 12,500 5,630 38.1 J8/12/2010 3,310 <100 <100 846 67.5 J 1,100 <100 85.6 J 8,170 414160 2,920 1,390 ND8/19/2011 5,730 <20.5 <19.0 4,570 32666.9509425 27,500 2,800 865 16,000 7,420 66.4 J8/17/2012 1,730 <82.0 <76.0 3,600 215 <42.0 364326 25,600 2,030 613 12,600 5,700 ND8/13/2013 927 <82.0 <76.0 2,990 197 J <42.0 337242 12,500 1,590 436 11,200 5,170 6758/21/2014 796 <20.5 <19.0 3,110 215 <10.5 451271 6,050 1,970 508 12,300 6,020 179.33/11/2015 1,120 <20.5 <19.0 3,410 <20.0 <10.5 483293 7,290 1,890 <18.0 13,400 5,960 32.1 J8/5/2015780 <20.5 <19.0 2,030 180 <10.5 352184 5,070 1,090 <18.0 8,660 3,620 84.7 J8/1/2016663 <41.0 <38.0 4,660 253 <21.0 505247 12,100 1,770 480 16,300 8,350 128.1 J8/9/2017 41.9 J <20.5 <19.0 3,240 171 <10.5 327164 9,750 1,110 <18.0 12,600 5,940 ND8/8/2018<6.2 <10.2 <9.5 1,260 134 <5.2 410226 3,560 1,700 426 5,410 3,040 54.9 J8/7/2019 11.9 J <0.94 <8.0 2,710 121 <11.0 341 <7.4 2,640 1,040 <7.9 9,920 5,380 41.38/6/2020<6.0 <9.4 <8.0 2,590 144 <11.0 550 <7.4 241 1,230 <7.9 10,600 5,410 16.9 J8/21/2021 <17.2 <24.5 <20.0 2,730 250 <21.1 686 <17.0 247 2,260 <16.6 11,900 5,600 NDNotes are provided on the final page of this table.FHR TYPE II MONITORING WELLS WITHIN APEX TERMINAL (Continued)AMW-40.8' FREE- PHASE PRODUCT PRESENT 2.10' FREE- PHASE PRODUCT PRESENT1.45' FREE- PHASE PRODUCT PRESENT0.15' FREE-PHASE PRODUCT PRESENT 0.21' FREE-PHASE PRODUCT PRESENT16,000 (Total Xylenes)11,000 (Total Xylenes)11,000 (Total Xylenes)9,800 (Total Xylenes)16,000 (Total Xylenes)10,000 (Total Xylenes)Page 18 of 20
Appendix CHistorical Groundwater ResultsLoading Rack AreaFormer FHR North TerminalWilmington, North CarolinaSample ID Date Collected1 70 70 600 70 20 6 70 600 400 400 VariesToluene1,2,4-TrimethylbenzeneContaminant of ConcernBenzenen-Butylbenzenesec-ButylbenzeneEthylbenzene1,3,5-Trimethylbenzenem/p-Xyleneso-XyleneAll Other 8260B AnalytesGroundwater Clean-up Goal (ug/L)500Isopropylbenzene (Cumene)Methyl Tert Butyl Ether (MTBE)Naphthalenen-Propylbenzene12/22/2003 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0ND2/19/04<1.0 <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.01.38/5/04<0.36 <0.31 <0.24 <0.34 <0.25 <0.31 <0.44 <0.32 <0.54 <0.19 <0.21 0.90J <0.35 ND2/16/05<0.54 <0.38 <0.60 <0.62 <0.66 <0.45 0.44J <0.45 <0.62 <0.44 <0.49ND8/22/05<0.54 <0.38 <0.60 <0.62 <0.66 1.5J <0.12 <0.45 <0.62 <0.44 <0.49ND2/8/06<0.54 <0.38 <0.60 <0.62 <0.66 2.8J <0.12 <0.45 <0.62 <0.44 <0.49ND8/7/2006 <0.54 <0.38 <0.60 <0.62 <0.66 2,400 <0.12 <0.45 <0.62 <0.44 <0.49ND2/7/200735<3.8 <6.0 <6.2 <6.6 16,000 <1.2 <4.5 <6.2 <4.4 <4.9ND8/9/2007430 <3.3 <2.9 3.8 J <2.7 8,400 <2.7 <3.4 4.9 J <2.7 <2.8ND2/26/2008 300 <3.3 <2.9 <3.0 <2.7 210 4.9 J <3.4 4.0 J <2.7 <2.8ND8/19/2008 110 <0.33 <0.29 <0.30 <0.27 871.6 J <0.34 0.60 J <0.27 <0.283.28/18/2009 15.6 <1.0 <1.0 <1.0 <1.0 54.54.7<1.0 <1.0 <1.0 <1.0 <2.0 <1.0 23.58/12/20101.1<1.0 <1.0 <1.0 0.60 J 60.3 <1.0 <1.0 <1.01.4<1.03.9 0.77 J 382.98/18/20114.3 <0.41 <0.38 0.32 J 8.674.3 18.26.71.0 J1.71.43.1 0.36 J 317.88/20/2012 <0.25 <0.41 <0.38 <0.30 5.115.8 11.83.2 0.27 J <0.31 <0.36 0.78 J <0.23 270.88/14/2013 <0.25 <0.41 <0.38 <0.30 4.42.1 0.93 J 3.6 <0.26 <0.31 <0.36 1.2 J <0.23 27.88/14/2014 0.29 J <0.41 <0.38 <0.30 8.731.2 0.97 J 3.9 <0.26 <0.31 <0.36 1.0 J 0.36 J 154.53/11/20156.6 <0.41 <0.38 52.7 <0.40 29.32.32.914.91.4 <0.36 14291.2 10.38/5/2015 <0.25 <0.41 <0.38 <0.30 <0.40 0.22 J <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 ND8/1/2016 0.26 J <0.41 0.71 J <0.30 24.1 12.0 0.68 J 26.0 0.63 J 0.33 J <0.36 2.8 0.62 J 9.48/9/2017 <0.25 <0.41 1.31.312.74.710.8 16.2 0.62 J 7.23.922.41.025.98/8/2018 <0.25 <0.41 1.1 <0.30 16.44.5 0.33 J 11.9 <0.26 <0.31 <0.36 1.4 J 0.34 J 2.48/7/2019 <0.15 <0.23 0.84 J <0.26 17.06.426.47.0 <0.24 2.14.55.1 0.39 J 4.18/6/2020 <0.15 <0.23 0.46 J <0.26 5.5 0.95 J <0.35 1.8 <0.24 <0.17 <0.20 <0.41 <0.22 5.63 J8/21/2021 <0.34 <0.49 <0.40 <0.30 18.46.2 <0.64 2.3 <0.48 <0.50 <0.33 <0.71 <0.34 5.912/22/0376<1.02.75.34.124<1.01.11.13.4<1.011<1.0ND2/19/04662.64.23.55.5245.71.82.217<5.0232.2ND8/5/04210E 3.25.51.96591.1 J2.43.5238.5202.6ND2/16/05823.23.42.81270113.82.2356.91.7J8/22/055.92.22.8 <0.62 6.2286.7 0.95 J 1.39.52.9ND2/8/06201.8J <1.2 <1.29.4214.8 J 1.8 J <1.2202.8ND8/7/2006170 <0.76 2.95.25.3 1,900 1.3 J 1.8 J7.24510ND2/7/200741 <0.38 3.3 <0.628181.4 J2.5 0.98 J 368.42.5 J8/9/20072203.24.95.11165 9.4 JB 7.23.45919ND2/26/2008 200 <0.66 5.51.2 J8.3267.5 J6.33.64312ND8/19/2008 200 1.9 J2.4 0.80 J 6.240 0.80 J 1.2 J3.9153.6ND8/18/2009 60.1 <1.02.4<1.08.78.1<1.0 <1.01.78.22.23.71.22.28/21/20121.5 <0.41 0.75 J <0.30 3.01.4 0.34 J <0.42 <0.26 <0.31 <0.36<0.66<0.23 ND8/14/2013 34.0 <0.41 2.55.013.72.6 0.69 J 1.728.08.01.825.11.4 16.6 J8/14/2014 0.82 J <0.41 <0.38 <0.30 <0.40 <0.21 <0.24 <0.42 0.54 J <0.31 <0.36<0.66<0.23 ND3/11/2015 309 <0.41 <0.38 48.87.36.68.63.020725.46.523134.2 57.14 J8/5/2015294 <1.0 <0.95 30.65.26.413.13.343.1 29.78.713418.4ND8/1/2016168 0.78 J <0.38 8.85.322.03.61.82.218.13.895.32.3 0.22 J8/9/201730.2 <0.41 <0.38 0.69 J 1.9 <0.21 <0.24 <0.42 <0.26 1.8 0.48 J6.40.29 J NDNotes are provided on the final page of this table.FHR TYPE II MONITORING WELLS WITHIN APEX TERMINAL (Continued)AMW-5<1.6 (Total Xylenes)<1.3 (Total Xylenes)<1.3 (Total Xylenes)<1.3 (Total Xylenes)<13 (Total Xylenes)24 (Total Xylenes)23 (Total Xylenes)0.88 J (Total Xylenes)AMW-6240 (Total Xylenes)3.2 (Total Xylenes)370 (Total Xylenes)38 (Total Xylenes)6.9 (Total Xylenes)28 (Total Xylenes)19 (Total Xylenes)15 (Total Xylenes)Page 19 of 20
Appendix CHistorical Groundwater ResultsLoading Rack AreaFormer FHR North TerminalWilmington, North CarolinaSample ID Date Collected1 70 70 600 70 20 6 70 600 400 400 VariesToluene1,2,4-TrimethylbenzeneContaminant of ConcernBenzenen-Butylbenzenesec-ButylbenzeneEthylbenzene1,3,5-Trimethylbenzenem/p-Xyleneso-XyleneAll Other 8260B AnalytesGroundwater Clean-up Goal (ug/L)500Isopropylbenzene (Cumene)Methyl Tert Butyl Ether (MTBE)Naphthalenen-Propylbenzene3/12/2015 <0.62 <1.0 <0.95 1.2 J <1.0 86.66.2<1.0 <0.65 1.2 J <0.90 <1.6 <0.58 3.3 J8/5/2015 <0.25 <0.41 <0.38 0.99 J <0.40 82.5 0.77 J <0.42 0.33 J 0.60 J <0.36 4.3 <0.23 32.8 J8/1/2016 <0.25 <0.41 <0.38 0.53 J <0.40 72.7 0.33 J <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 14.08/8/2017 <0.25 <0.41 <0.38 0.50 J <0.40 34.8 0.29 J <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 6.38/8/2018 <0.25 <0.41 <0.38 <0.30 <0.40 1.7 <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 0.35 J8/7/2019 <0.15 <0.23 <0.20 <0.26 <0.20 12.1 <0.35 <0.18 <0.24 <0.17 <0.20 <0.41 <0.22 ND8/6/2020 <0.15 <0.23 <0.20 <0.26 <0.20 13.7 0.59 J <0.18 <0.24 <0.17 <0.20 3.0 <0.22 ND8/23/2021 <0.34 <0.49 <0.40 <0.30 <0.33 7.6 <0.64 <0.34 <0.48 <0.50 <0.33 <0.71 <0.34 ND3/11/2014 <0.25 <0.41 <0.38 <0.30 <0.40 37.0 <0.24 <0.42 <0.26 <0.31 <0.3612.8<0.23 ND4/9/2014 <0.25 <0.41 <0.38 <0.30 <0.40 28.3 <0.24 <0.42 <0.26 <0.31 <0.362.2<0.23 ND5/20/2014 <0.25 <0.41 <0.38 <0.30 <0.40 23.8 <0.24 <0.42 <0.26 <0.31 <0.361.3 J<0.23 ND8/14/2014 <0.25 <0.41 <0.38 <0.30 <0.40 21.2 <0.24 <0.42 <0.26 <0.31 <0.36<0.66<0.23 ND10/23/2014 <0.25 <0.41 <0.38 <0.30 <0.40 37.8 <0.24 <0.42 <0.26 <0.31 <0.36<0.66<0.23 ND3/12/2015 <0.25 <0.41 <0.38 <0.30 <0.40 42.0 <0.24 <0.42 <0.26 <0.31 <0.360.87 J<0.23 ND8/5/2015 <0.25 <0.41 <0.38 <0.30 <0.40 22.6 <0.24 <0.42 <0.26 <0.31 <0.360.73 J<0.23 3.9 J8/1/2016 <0.25 <0.41 <0.38 <0.30 <0.40 27.9 <0.24 <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 ND8/9/2017 <0.25 <0.41 <0.38 <0.30 <0.40 9.9 0.61 J <0.42 <0.26 <0.31 <0.36 <0.66 <0.23 ND8/7/2018 <0.25 <0.41 <0.38 <0.30 <0.40 19.7 <0.24 <0.42 <0.26 <0.31 <0.36 0.82 J <0.23 ND8/7/2019 <0.15 <0.23 <0.20 2.0 <0.20 12.51.4 <0.18 0.95 J 1.5 0.48 J 10.13.8ND8/6/2020 <0.15 <0.23 <0.20 <0.26 <0.20 6.2 <0.35 <0.18 <0.24 <0.17 <0.20 <0.41 <0.22 ND8/22/2021 <0.34 <0.49 <0.40 <0.30 <0.33 12.5 <0.64 <0.34 <0.48 <0.50 <0.33 <0.71 <0.34 ND10/2/2013*** <0.25 <0.25 <0.25 <0.25 <0.25 0.53 <1.0 <0.25 <0.25 <0.25 <0.25 <0.50 <0.25 0.74 J3/11/2015 0.49 J <0.41 <0.38 <0.30 <0.40 0.43 J 0.36 J <0.42 0.48 J <0.31 <0.36 1.1 J <0.23 NDNotes:All results in micrograms per liter (ug/L).- = No dataShaded concentrations exceed the 15A North Carolina Administrative Code (NCAC) 2L.0202 North Carolina Groundwater Quality Standard (2L GWQS), updated April 1, 2013. Refer to laboratory reports for other 8260 analytes detected.ND = Not detectedND1 = Chloroform was also detected in KMW-5 with a result of 7.5 ug/l.ND2 = Tert-butylbenzene was detected in KMW-3 with a result of 5.2 ug/l.BQL = Below Quantitation Limits* = Determined with EPA Method 602 analysis** = Temporary wells have been permanently abandoned and location of temporary wells were last documented in the Corrective Action Plan Addendum dated August 9, 2002.*** = Groundwater sampled was analyzed per EPA Method 6200BJ = Value is estimated concentration that is less than RL, but greater than or equal to the MDL.E = The reported result exceeded the calibration range of the instrument.D = The reported result is from a secondary dilution.B = Compound was found in blank and sample.October/November 2016, April 2017 and February 2019 data is from post EAB sampling events and select samples from these events were analyzed via EPA Method 8260B for BTEX constituents only.March 2017 data is from a post EAB sampling event and samples were analyzed for the full 8260 list.WATER SUPPLY WELLSPW-1< = Less than method detection limit or reporting limitNA = Not AnalyzedTYPE III MONITORING WELLSKDW-1FHR TYPE III MONITORING WELLS WITHIN APEX TERMINALADW-1Page 20 of 20

Appendix D

Laboratory Analytical Reports

#=CL#
September 14, 2021
LIMS USE: FR - MATT MAHONY
LIMS OBJECT ID: 92557149
92557149
Project:
Pace Project No.:
RE:
Matt Mahony
Tetra Tech
805 E 20th St
Charlotte, NC 28205
LOADING RACK
Dear Matt Mahony:
Enclosed are the analytical results for sample(s) received by the laboratory on August 24, 2021. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
This revised report replaces the report issued on August 27, 2021. Per client request, this report has been revised to add
Isopropylbenzene (Cumene) to all submitted samples. No other changes have been made to this report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Nikita Kuruganty
[e-mail]
Project Manager
[phone]
Enclosures
cc: Michael Christopher
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 69
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92557149
LOADING RACK
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 69
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92557149
LOADING RACK
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92557149001 ADW-1 EPA 8260D 69 PASI-CSAS
92557149002 AMW-1 EPA 8260D 69 PASI-CSAS
92557149003 AMW-2 EPA 8260D 69 PASI-CPM1
92557149004 AMW-3 EPA 8260D 69 PASI-CSAS
92557149005 AMW-4 EPA 8260D 69 PASI-CPM1
92557149006 AMW-5 EPA 8260D 69 PASI-CPM1
92557149007 KDW-1 EPA 8260D 69 PASI-CNSCQ
92557149008 KMW-1 EPA 8260D 69 PASI-CNSCQ
92557149009 KMW-3 EPA 8260D 69 PASI-CPM1
92557149010 KMW-5 EPA 8260D 69 PASI-CNSCQ
92557149011 KMW-6 EPA 8260D 69 PASI-CPM1
92557149012 KMW-7 EPA 8260D 69 PASI-CPM1
92557149013 KMW-8 EPA 8260D 69 PASI-CCL
92557149014 KMW-9R EPA 8260D 69 PASI-CNSCQ
92557149015 KMW-12 EPA 8260D 69 PASI-CCL
92557149016 KMW-13 EPA 8260D 69 PASI-CCL
92557149017 KMW-14 EPA 8260D 69 PASI-CCL
92557149018 KMW-18 EPA 8260D 69 PASI-CCL
92557149019 TRIP BLANK EPA 8260D 69 PASI-CNSCQ
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92557149
LOADING RACK
Sample: ADW-1 Lab ID: 92557149001 Collected: 08/22/21 11:02 Received: 08/24/21 10:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 08/24/21 16:39 67-64-125.0 1
Benzene ND ug/L 08/24/21 16:39 71-43-2 R11.0 1
Bromobenzene ND ug/L 08/24/21 16:39 108-86-1 R11.0 1
Bromochloromethane ND ug/L 08/24/21 16:39 74-97-5 R11.0 1
Bromodichloromethane ND ug/L 08/24/21 16:39 75-27-4 R11.0 1
Bromoform ND ug/L 08/24/21 16:39 75-25-2 R11.0 1
Bromomethane ND ug/L 08/24/21 16:39 74-83-9 R1,v12.0 1
2-Butanone (MEK)ND ug/L 08/24/21 16:39 78-93-3 R15.0 1
n-Butylbenzene ND ug/L 08/24/21 16:39 104-51-8 R11.0 1
sec-Butylbenzene ND ug/L 08/24/21 16:39 135-98-8 R11.0 1
Carbon tetrachloride ND ug/L 08/24/21 16:39 56-23-5 R11.0 1
Chlorobenzene ND ug/L 08/24/21 16:39 108-90-7 R11.0 1
Chloroethane ND ug/L 08/24/21 16:39 75-00-3 R11.0 1
Chloroform ND ug/L 08/24/21 16:39 67-66-3 R11.0 1
Chloromethane ND ug/L 08/24/21 16:39 74-87-3 R11.0 1
2-Chlorotoluene ND ug/L 08/24/21 16:39 95-49-8 R11.0 1
4-Chlorotoluene ND ug/L 08/24/21 16:39 106-43-4 R11.0 1
1,2-Dibromo-3-chloropropane ND ug/L 08/24/21 16:39 96-12-8 R12.0 1
Dibromochloromethane ND ug/L 08/24/21 16:39 124-48-1 R11.0 1
1,2-Dibromoethane (EDB)ND ug/L 08/24/21 16:39 106-93-4 R11.0 1
Dibromomethane ND ug/L 08/24/21 16:39 74-95-3 R11.0 1
1,2-Dichlorobenzene ND ug/L 08/24/21 16:39 95-50-1 R11.0 1
1,3-Dichlorobenzene ND ug/L 08/24/21 16:39 541-73-1 R11.0 1
1,4-Dichlorobenzene ND ug/L 08/24/21 16:39 106-46-7 R11.0 1
Dichlorodifluoromethane ND ug/L 08/24/21 16:39 75-71-8 R11.0 1
1,1-Dichloroethane ND ug/L 08/24/21 16:39 75-34-3 R11.0 1
1,2-Dichloroethane ND ug/L 08/24/21 16:39 107-06-2 R11.0 1
1,1-Dichloroethene ND ug/L 08/24/21 16:39 75-35-4 R11.0 1
cis-1,2-Dichloroethene ND ug/L 08/24/21 16:39 156-59-2 R11.0 1
trans-1,2-Dichloroethene ND ug/L 08/24/21 16:39 156-60-5 R11.0 1
1,2-Dichloropropane ND ug/L 08/24/21 16:39 78-87-5 R11.0 1
1,3-Dichloropropane ND ug/L 08/24/21 16:39 142-28-9 R11.0 1
2,2-Dichloropropane ND ug/L 08/24/21 16:39 594-20-7 R11.0 1
1,1-Dichloropropene ND ug/L 08/24/21 16:39 563-58-6 R11.0 1
cis-1,3-Dichloropropene ND ug/L 08/24/21 16:39 10061-01-5 R11.0 1
trans-1,3-Dichloropropene ND ug/L 08/24/21 16:39 10061-02-6 R11.0 1
Diisopropyl ether ND ug/L 08/24/21 16:39 108-20-3 R11.0 1
Ethylbenzene ND ug/L 08/24/21 16:39 100-41-4 R11.0 1
Hexachloro-1,3-butadiene ND ug/L 08/24/21 16:39 87-68-3 R12.0 1
2-Hexanone ND ug/L 08/24/21 16:39 591-78-6 R15.0 1
Isopropylbenzene (Cumene)ND ug/L 08/24/21 16:39 98-82-81.0 1
p-Isopropyltoluene ND ug/L 08/24/21 16:39 99-87-6 R11.0 1
Methylene Chloride ND ug/L 08/24/21 16:39 75-09-2 R15.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/24/21 16:39 108-10-1 R15.0 1
Methyl-tert-butyl ether 12.5 ug/L 08/24/21 16:39 1634-04-41.0 1
Naphthalene ND ug/L 08/24/21 16:39 91-20-3 R11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92557149
LOADING RACK
Sample: ADW-1 Lab ID: 92557149001 Collected: 08/22/21 11:02 Received: 08/24/21 10:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
n-Propylbenzene ND ug/L 08/24/21 16:39 103-65-1 R11.0 1
Styrene ND ug/L 08/24/21 16:39 100-42-5 R11.0 1
1,1,1,2-Tetrachloroethane ND ug/L 08/24/21 16:39 630-20-6 R11.0 1
1,1,2,2-Tetrachloroethane ND ug/L 08/24/21 16:39 79-34-5 R11.0 1
Tetrachloroethene ND ug/L 08/24/21 16:39 127-18-4 R11.0 1
Toluene ND ug/L 08/24/21 16:39 108-88-3 R11.0 1
1,2,3-Trichlorobenzene ND ug/L 08/24/21 16:39 87-61-6 R11.0 1
1,2,4-Trichlorobenzene ND ug/L 08/24/21 16:39 120-82-1 R11.0 1
1,1,1-Trichloroethane ND ug/L 08/24/21 16:39 71-55-6 R11.0 1
1,1,2-Trichloroethane ND ug/L 08/24/21 16:39 79-00-5 R11.0 1
Trichloroethene ND ug/L 08/24/21 16:39 79-01-6 R11.0 1
Trichlorofluoromethane ND ug/L 08/24/21 16:39 75-69-4 R11.0 1
1,2,3-Trichloropropane ND ug/L 08/24/21 16:39 96-18-4 R11.0 1
1,2,4-Trimethylbenzene ND ug/L 08/24/21 16:39 95-63-6 R11.0 1
1,3,5-Trimethylbenzene ND ug/L 08/24/21 16:39 108-67-8 R11.0 1
Vinyl acetate ND ug/L 08/24/21 16:39 108-05-4 R12.0 1
Vinyl chloride ND ug/L 08/24/21 16:39 75-01-4 R11.0 1
Xylene (Total)ND ug/L 08/24/21 16:39 1330-20-7 RS1.0 1
m&p-Xylene ND ug/L 08/24/21 16:39 179601-23-1 R12.0 1
o-Xylene ND ug/L 08/24/21 16:39 95-47-6 R11.0 1
Surrogates
4-Bromofluorobenzene (S)97 %08/24/21 16:39 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %08/24/21 16:39 17060-07-070-130 1
Toluene-d8 (S)100 %08/24/21 16:39 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92557149
LOADING RACK
Sample: AMW-1 Lab ID: 92557149002 Collected: 08/21/21 15:50 Received: 08/24/21 10:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 08/24/21 16:57 67-64-125.0 1
Benzene ND ug/L 08/24/21 16:57 71-43-21.0 1
Bromobenzene ND ug/L 08/24/21 16:57 108-86-11.0 1
Bromochloromethane ND ug/L 08/24/21 16:57 74-97-51.0 1
Bromodichloromethane ND ug/L 08/24/21 16:57 75-27-41.0 1
Bromoform ND ug/L 08/24/21 16:57 75-25-21.0 1
Bromomethane ND ug/L 08/24/21 16:57 74-83-92.0 1
2-Butanone (MEK)ND ug/L 08/24/21 16:57 78-93-35.0 1
n-Butylbenzene ND ug/L 08/24/21 16:57 104-51-81.0 1
sec-Butylbenzene ND ug/L 08/24/21 16:57 135-98-81.0 1
Carbon tetrachloride ND ug/L 08/24/21 16:57 56-23-51.0 1
Chlorobenzene ND ug/L 08/24/21 16:57 108-90-71.0 1
Chloroethane ND ug/L 08/24/21 16:57 75-00-31.0 1
Chloroform ND ug/L 08/24/21 16:57 67-66-31.0 1
Chloromethane ND ug/L 08/24/21 16:57 74-87-31.0 1
2-Chlorotoluene ND ug/L 08/24/21 16:57 95-49-81.0 1
4-Chlorotoluene ND ug/L 08/24/21 16:57 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 08/24/21 16:57 96-12-82.0 1
Dibromochloromethane ND ug/L 08/24/21 16:57 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 08/24/21 16:57 106-93-41.0 1
Dibromomethane ND ug/L 08/24/21 16:57 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 08/24/21 16:57 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 08/24/21 16:57 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 08/24/21 16:57 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 08/24/21 16:57 75-71-81.0 1
1,1-Dichloroethane ND ug/L 08/24/21 16:57 75-34-31.0 1
1,2-Dichloroethane ND ug/L 08/24/21 16:57 107-06-21.0 1
1,1-Dichloroethene ND ug/L 08/24/21 16:57 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 08/24/21 16:57 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 08/24/21 16:57 156-60-51.0 1
1,2-Dichloropropane ND ug/L 08/24/21 16:57 78-87-51.0 1
1,3-Dichloropropane ND ug/L 08/24/21 16:57 142-28-91.0 1
2,2-Dichloropropane ND ug/L 08/24/21 16:57 594-20-71.0 1
1,1-Dichloropropene ND ug/L 08/24/21 16:57 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 08/24/21 16:57 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 08/24/21 16:57 10061-02-61.0 1
Diisopropyl ether ND ug/L 08/24/21 16:57 108-20-31.0 1
Ethylbenzene ND ug/L 08/24/21 16:57 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 08/24/21 16:57 87-68-32.0 1
2-Hexanone ND ug/L 08/24/21 16:57 591-78-65.0 1
Isopropylbenzene (Cumene)ND ug/L 08/24/21 16:57 98-82-81.0 1
p-Isopropyltoluene ND ug/L 08/24/21 16:57 99-87-61.0 1
Methylene Chloride ND ug/L 08/24/21 16:57 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/24/21 16:57 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 08/24/21 16:57 1634-04-41.0 1
Naphthalene ND ug/L 08/24/21 16:57 91-20-31.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92557149
LOADING RACK
Sample: AMW-1 Lab ID: 92557149002 Collected: 08/21/21 15:50 Received: 08/24/21 10:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
n-Propylbenzene ND ug/L 08/24/21 16:57 103-65-11.0 1
Styrene ND ug/L 08/24/21 16:57 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 08/24/21 16:57 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 08/24/21 16:57 79-34-51.0 1
Tetrachloroethene ND ug/L 08/24/21 16:57 127-18-41.0 1
Toluene ND ug/L 08/24/21 16:57 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 08/24/21 16:57 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 08/24/21 16:57 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 08/24/21 16:57 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 08/24/21 16:57 79-00-51.0 1
Trichloroethene ND ug/L 08/24/21 16:57 79-01-61.0 1
Trichlorofluoromethane ND ug/L 08/24/21 16:57 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 08/24/21 16:57 96-18-41.0 1
1,2,4-Trimethylbenzene ND ug/L 08/24/21 16:57 95-63-61.0 1
1,3,5-Trimethylbenzene ND ug/L 08/24/21 16:57 108-67-81.0 1
Vinyl acetate ND ug/L 08/24/21 16:57 108-05-42.0 1
Vinyl chloride ND ug/L 08/24/21 16:57 75-01-41.0 1
Xylene (Total)ND ug/L 08/24/21 16:57 1330-20-71.0 1
m&p-Xylene ND ug/L 08/24/21 16:57 179601-23-12.0 1
o-Xylene ND ug/L 08/24/21 16:57 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)97 %08/24/21 16:57 460-00-470-130 1
1,2-Dichloroethane-d4 (S)104 %08/24/21 16:57 17060-07-070-130 1
Toluene-d8 (S)99 %08/24/21 16:57 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92557149
LOADING RACK
Sample: AMW-2 Lab ID: 92557149003 Collected: 08/21/21 12:56 Received: 08/24/21 10:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 08/25/21 13:59 67-64-1312 12.5
Benzene ND ug/L 08/25/21 13:59 71-43-212.5 12.5
Bromobenzene ND ug/L 08/25/21 13:59 108-86-112.5 12.5
Bromochloromethane ND ug/L 08/25/21 13:59 74-97-512.5 12.5
Bromodichloromethane ND ug/L 08/25/21 13:59 75-27-412.5 12.5
Bromoform ND ug/L 08/25/21 13:59 75-25-212.5 12.5
Bromomethane ND ug/L 08/25/21 13:59 74-83-925.0 12.5
2-Butanone (MEK)ND ug/L 08/25/21 13:59 78-93-362.5 12.5
n-Butylbenzene ND ug/L 08/25/21 13:59 104-51-812.5 12.5
sec-Butylbenzene ND ug/L 08/25/21 13:59 135-98-812.5 12.5
Carbon tetrachloride ND ug/L 08/25/21 13:59 56-23-512.5 12.5
Chlorobenzene ND ug/L 08/25/21 13:59 108-90-712.5 12.5
Chloroethane ND ug/L 08/25/21 13:59 75-00-3 IL12.5 12.5
Chloroform ND ug/L 08/25/21 13:59 67-66-312.5 12.5
Chloromethane ND ug/L 08/25/21 13:59 74-87-312.5 12.5
2-Chlorotoluene ND ug/L 08/25/21 13:59 95-49-812.5 12.5
4-Chlorotoluene ND ug/L 08/25/21 13:59 106-43-412.5 12.5
1,2-Dibromo-3-chloropropane ND ug/L 08/25/21 13:59 96-12-825.0 12.5
Dibromochloromethane ND ug/L 08/25/21 13:59 124-48-112.5 12.5
1,2-Dibromoethane (EDB)ND ug/L 08/25/21 13:59 106-93-412.5 12.5
Dibromomethane ND ug/L 08/25/21 13:59 74-95-312.5 12.5
1,2-Dichlorobenzene ND ug/L 08/25/21 13:59 95-50-112.5 12.5
1,3-Dichlorobenzene ND ug/L 08/25/21 13:59 541-73-112.5 12.5
1,4-Dichlorobenzene ND ug/L 08/25/21 13:59 106-46-712.5 12.5
Dichlorodifluoromethane ND ug/L 08/25/21 13:59 75-71-812.5 12.5
1,1-Dichloroethane ND ug/L 08/25/21 13:59 75-34-312.5 12.5
1,2-Dichloroethane ND ug/L 08/25/21 13:59 107-06-212.5 12.5
1,1-Dichloroethene ND ug/L 08/25/21 13:59 75-35-412.5 12.5
cis-1,2-Dichloroethene ND ug/L 08/25/21 13:59 156-59-212.5 12.5
trans-1,2-Dichloroethene ND ug/L 08/25/21 13:59 156-60-512.5 12.5
1,2-Dichloropropane ND ug/L 08/25/21 13:59 78-87-512.5 12.5
1,3-Dichloropropane ND ug/L 08/25/21 13:59 142-28-912.5 12.5
2,2-Dichloropropane ND ug/L 08/25/21 13:59 594-20-712.5 12.5
1,1-Dichloropropene ND ug/L 08/25/21 13:59 563-58-612.5 12.5
cis-1,3-Dichloropropene ND ug/L 08/25/21 13:59 10061-01-512.5 12.5
trans-1,3-Dichloropropene ND ug/L 08/25/21 13:59 10061-02-612.5 12.5
Diisopropyl ether ND ug/L 08/25/21 13:59 108-20-312.5 12.5
Ethylbenzene 296 ug/L 08/25/21 13:59 100-41-412.5 12.5
Hexachloro-1,3-butadiene ND ug/L 08/25/21 13:59 87-68-325.0 12.5
2-Hexanone ND ug/L 08/25/21 13:59 591-78-662.5 12.5
Isopropylbenzene (Cumene)27.8 ug/L 08/25/21 13:59 98-82-812.5 12.5
p-Isopropyltoluene ND ug/L 08/25/21 13:59 99-87-612.5 12.5
Methylene Chloride ND ug/L 08/25/21 13:59 75-09-262.5 12.5
4-Methyl-2-pentanone (MIBK)ND ug/L 08/25/21 13:59 108-10-162.5 12.5
Methyl-tert-butyl ether ND ug/L 08/25/21 13:59 1634-04-412.5 12.5
Naphthalene 150 ug/L 08/25/21 13:59 91-20-312.5 12.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92557149
LOADING RACK
Sample: AMW-2 Lab ID: 92557149003 Collected: 08/21/21 12:56 Received: 08/24/21 10:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
n-Propylbenzene ND ug/L 08/25/21 13:59 103-65-112.5 12.5
Styrene ND ug/L 08/25/21 13:59 100-42-512.5 12.5
1,1,1,2-Tetrachloroethane ND ug/L 08/25/21 13:59 630-20-612.5 12.5
1,1,2,2-Tetrachloroethane ND ug/L 08/25/21 13:59 79-34-512.5 12.5
Tetrachloroethene ND ug/L 08/25/21 13:59 127-18-412.5 12.5
Toluene ND ug/L 08/25/21 13:59 108-88-312.5 12.5
1,2,3-Trichlorobenzene ND ug/L 08/25/21 13:59 87-61-612.5 12.5
1,2,4-Trichlorobenzene ND ug/L 08/25/21 13:59 120-82-112.5 12.5
1,1,1-Trichloroethane ND ug/L 08/25/21 13:59 71-55-612.5 12.5
1,1,2-Trichloroethane ND ug/L 08/25/21 13:59 79-00-512.5 12.5
Trichloroethene ND ug/L 08/25/21 13:59 79-01-612.5 12.5
Trichlorofluoromethane ND ug/L 08/25/21 13:59 75-69-412.5 12.5
1,2,3-Trichloropropane ND ug/L 08/25/21 13:59 96-18-412.5 12.5
1,2,4-Trimethylbenzene 404 ug/L 08/25/21 13:59 95-63-612.5 12.5
1,3,5-Trimethylbenzene 101 ug/L 08/25/21 13:59 108-67-812.5 12.5
Vinyl acetate ND ug/L 08/25/21 13:59 108-05-4 v125.0 12.5
Vinyl chloride ND ug/L 08/25/21 13:59 75-01-412.5 12.5
Xylene (Total)3810 ug/L 08/25/21 13:59 1330-20-712.5 12.5
m&p-Xylene 3750 ug/L 08/25/21 13:59 179601-23-125.0 12.5
o-Xylene 57.2 ug/L 08/25/21 13:59 95-47-612.5 12.5
Surrogates
4-Bromofluorobenzene (S)98 %08/25/21 13:59 460-00-470-130 12.5
1,2-Dichloroethane-d4 (S)99 %08/25/21 13:59 17060-07-070-130 12.5
Toluene-d8 (S)107 %08/25/21 13:59 2037-26-570-130 12.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92557149
LOADING RACK
Sample: AMW-3 Lab ID: 92557149004 Collected: 08/22/21 09:06 Received: 08/24/21 10:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 08/24/21 17:15 67-64-150.0 2
Benzene ND ug/L 08/24/21 17:15 71-43-22.0 2
Bromobenzene ND ug/L 08/24/21 17:15 108-86-12.0 2
Bromochloromethane ND ug/L 08/24/21 17:15 74-97-52.0 2
Bromodichloromethane ND ug/L 08/24/21 17:15 75-27-42.0 2
Bromoform ND ug/L 08/24/21 17:15 75-25-22.0 2
Bromomethane ND ug/L 08/24/21 17:15 74-83-94.0 2
2-Butanone (MEK)ND ug/L 08/24/21 17:15 78-93-310.0 2
n-Butylbenzene ND ug/L 08/24/21 17:15 104-51-82.0 2
sec-Butylbenzene ND ug/L 08/24/21 17:15 135-98-82.0 2
Carbon tetrachloride ND ug/L 08/24/21 17:15 56-23-52.0 2
Chlorobenzene ND ug/L 08/24/21 17:15 108-90-72.0 2
Chloroethane ND ug/L 08/24/21 17:15 75-00-32.0 2
Chloroform ND ug/L 08/24/21 17:15 67-66-32.0 2
Chloromethane ND ug/L 08/24/21 17:15 74-87-32.0 2
2-Chlorotoluene ND ug/L 08/24/21 17:15 95-49-82.0 2
4-Chlorotoluene ND ug/L 08/24/21 17:15 106-43-42.0 2
1,2-Dibromo-3-chloropropane ND ug/L 08/24/21 17:15 96-12-84.0 2
Dibromochloromethane ND ug/L 08/24/21 17:15 124-48-12.0 2
1,2-Dibromoethane (EDB)ND ug/L 08/24/21 17:15 106-93-42.0 2
Dibromomethane ND ug/L 08/24/21 17:15 74-95-32.0 2
1,2-Dichlorobenzene ND ug/L 08/24/21 17:15 95-50-12.0 2
1,3-Dichlorobenzene ND ug/L 08/24/21 17:15 541-73-12.0 2
1,4-Dichlorobenzene ND ug/L 08/24/21 17:15 106-46-72.0 2
Dichlorodifluoromethane ND ug/L 08/24/21 17:15 75-71-82.0 2
1,1-Dichloroethane ND ug/L 08/24/21 17:15 75-34-32.0 2
1,2-Dichloroethane ND ug/L 08/24/21 17:15 107-06-22.0 2
1,1-Dichloroethene ND ug/L 08/24/21 17:15 75-35-42.0 2
cis-1,2-Dichloroethene ND ug/L 08/24/21 17:15 156-59-22.0 2
trans-1,2-Dichloroethene ND ug/L 08/24/21 17:15 156-60-52.0 2
1,2-Dichloropropane ND ug/L 08/24/21 17:15 78-87-52.0 2
1,3-Dichloropropane ND ug/L 08/24/21 17:15 142-28-92.0 2
2,2-Dichloropropane ND ug/L 08/24/21 17:15 594-20-72.0 2
1,1-Dichloropropene ND ug/L 08/24/21 17:15 563-58-62.0 2
cis-1,3-Dichloropropene ND ug/L 08/24/21 17:15 10061-01-52.0 2
trans-1,3-Dichloropropene ND ug/L 08/24/21 17:15 10061-02-62.0 2
Diisopropyl ether ND ug/L 08/24/21 17:15 108-20-32.0 2
Ethylbenzene 7.9 ug/L 08/24/21 17:15 100-41-42.0 2
Hexachloro-1,3-butadiene ND ug/L 08/24/21 17:15 87-68-34.0 2
2-Hexanone ND ug/L 08/24/21 17:15 591-78-610.0 2
Isopropylbenzene (Cumene)18.1 ug/L 08/24/21 17:15 98-82-82.0 2
p-Isopropyltoluene ND ug/L 08/24/21 17:15 99-87-62.0 2
Methylene Chloride 15.3 ug/L 08/24/21 17:15 75-09-210.0 2
4-Methyl-2-pentanone (MIBK)ND ug/L 08/24/21 17:15 108-10-110.0 2
Methyl-tert-butyl ether ND ug/L 08/24/21 17:15 1634-04-42.0 2
Naphthalene 38.6 ug/L 08/24/21 17:15 91-20-32.0 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92557149
LOADING RACK
Sample: AMW-3 Lab ID: 92557149004 Collected: 08/22/21 09:06 Received: 08/24/21 10:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
n-Propylbenzene 28.1 ug/L 08/24/21 17:15 103-65-12.0 2
Styrene ND ug/L 08/24/21 17:15 100-42-52.0 2
1,1,1,2-Tetrachloroethane ND ug/L 08/24/21 17:15 630-20-62.0 2
1,1,2,2-Tetrachloroethane ND ug/L 08/24/21 17:15 79-34-52.0 2
Tetrachloroethene ND ug/L 08/24/21 17:15 127-18-42.0 2
Toluene 2.1 ug/L 08/24/21 17:15 108-88-32.0 2
1,2,3-Trichlorobenzene ND ug/L 08/24/21 17:15 87-61-62.0 2
1,2,4-Trichlorobenzene ND ug/L 08/24/21 17:15 120-82-12.0 2
1,1,1-Trichloroethane ND ug/L 08/24/21 17:15 71-55-62.0 2
1,1,2-Trichloroethane ND ug/L 08/24/21 17:15 79-00-52.0 2
Trichloroethene ND ug/L 08/24/21 17:15 79-01-62.0 2
Trichlorofluoromethane ND ug/L 08/24/21 17:15 75-69-42.0 2
1,2,3-Trichloropropane ND ug/L 08/24/21 17:15 96-18-42.0 2
1,2,4-Trimethylbenzene 37.1 ug/L 08/24/21 17:15 95-63-62.0 2
1,3,5-Trimethylbenzene 14.5 ug/L 08/24/21 17:15 108-67-82.0 2
Vinyl acetate ND ug/L 08/24/21 17:15 108-05-44.0 2
Vinyl chloride ND ug/L 08/24/21 17:15 75-01-42.0 2
Xylene (Total)355 ug/L 08/24/21 17:15 1330-20-72.0 2
m&p-Xylene 353 ug/L 08/24/21 17:15 179601-23-14.0 2
o-Xylene 2.6 ug/L 08/24/21 17:15 95-47-62.0 2
Surrogates
4-Bromofluorobenzene (S)98 %08/24/21 17:15 460-00-470-130 2
1,2-Dichloroethane-d4 (S)104 %08/24/21 17:15 17060-07-070-130 2
Toluene-d8 (S)101 %08/24/21 17:15 2037-26-570-130 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92557149
LOADING RACK
Sample: AMW-4 Lab ID: 92557149005 Collected: 08/21/21 14:56 Received: 08/24/21 10:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 08/25/21 14:34 67-64-11250 50
Benzene ND ug/L 08/25/21 14:34 71-43-250.0 50
Bromobenzene ND ug/L 08/25/21 14:34 108-86-150.0 50
Bromochloromethane ND ug/L 08/25/21 14:34 74-97-550.0 50
Bromodichloromethane ND ug/L 08/25/21 14:34 75-27-450.0 50
Bromoform ND ug/L 08/25/21 14:34 75-25-250.0 50
Bromomethane ND ug/L 08/25/21 14:34 74-83-9100 50
2-Butanone (MEK)ND ug/L 08/25/21 14:34 78-93-3250 50
n-Butylbenzene ND ug/L 08/25/21 14:34 104-51-850.0 50
sec-Butylbenzene ND ug/L 08/25/21 14:34 135-98-850.0 50
Carbon tetrachloride ND ug/L 08/25/21 14:34 56-23-550.0 50
Chlorobenzene ND ug/L 08/25/21 14:34 108-90-750.0 50
Chloroethane ND ug/L 08/25/21 14:34 75-00-3 IL50.0 50
Chloroform ND ug/L 08/25/21 14:34 67-66-350.0 50
Chloromethane ND ug/L 08/25/21 14:34 74-87-350.0 50
2-Chlorotoluene ND ug/L 08/25/21 14:34 95-49-850.0 50
4-Chlorotoluene ND ug/L 08/25/21 14:34 106-43-450.0 50
1,2-Dibromo-3-chloropropane ND ug/L 08/25/21 14:34 96-12-8100 50
Dibromochloromethane ND ug/L 08/25/21 14:34 124-48-150.0 50
1,2-Dibromoethane (EDB)ND ug/L 08/25/21 14:34 106-93-450.0 50
Dibromomethane ND ug/L 08/25/21 14:34 74-95-350.0 50
1,2-Dichlorobenzene ND ug/L 08/25/21 14:34 95-50-150.0 50
1,3-Dichlorobenzene ND ug/L 08/25/21 14:34 541-73-150.0 50
1,4-Dichlorobenzene ND ug/L 08/25/21 14:34 106-46-750.0 50
Dichlorodifluoromethane ND ug/L 08/25/21 14:34 75-71-850.0 50
1,1-Dichloroethane ND ug/L 08/25/21 14:34 75-34-350.0 50
1,2-Dichloroethane ND ug/L 08/25/21 14:34 107-06-250.0 50
1,1-Dichloroethene ND ug/L 08/25/21 14:34 75-35-450.0 50
cis-1,2-Dichloroethene ND ug/L 08/25/21 14:34 156-59-250.0 50
trans-1,2-Dichloroethene ND ug/L 08/25/21 14:34 156-60-550.0 50
1,2-Dichloropropane ND ug/L 08/25/21 14:34 78-87-550.0 50
1,3-Dichloropropane ND ug/L 08/25/21 14:34 142-28-950.0 50
2,2-Dichloropropane ND ug/L 08/25/21 14:34 594-20-750.0 50
1,1-Dichloropropene ND ug/L 08/25/21 14:34 563-58-650.0 50
cis-1,3-Dichloropropene ND ug/L 08/25/21 14:34 10061-01-550.0 50
trans-1,3-Dichloropropene ND ug/L 08/25/21 14:34 10061-02-650.0 50
Diisopropyl ether ND ug/L 08/25/21 14:34 108-20-350.0 50
Ethylbenzene 2730 ug/L 08/25/21 14:34 100-41-450.0 50
Hexachloro-1,3-butadiene ND ug/L 08/25/21 14:34 87-68-3100 50
2-Hexanone ND ug/L 08/25/21 14:34 591-78-6250 50
Isopropylbenzene (Cumene)250 ug/L 08/25/21 14:34 98-82-850.0 50
p-Isopropyltoluene ND ug/L 08/25/21 14:34 99-87-650.0 50
Methylene Chloride ND ug/L 08/25/21 14:34 75-09-2250 50
4-Methyl-2-pentanone (MIBK)ND ug/L 08/25/21 14:34 108-10-1250 50
Methyl-tert-butyl ether ND ug/L 08/25/21 14:34 1634-04-450.0 50
Naphthalene 686 ug/L 08/25/21 14:34 91-20-350.0 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92557149
LOADING RACK
Sample: AMW-4 Lab ID: 92557149005 Collected: 08/21/21 14:56 Received: 08/24/21 10:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
n-Propylbenzene ND ug/L 08/25/21 14:34 103-65-150.0 50
Styrene ND ug/L 08/25/21 14:34 100-42-550.0 50
1,1,1,2-Tetrachloroethane ND ug/L 08/25/21 14:34 630-20-650.0 50
1,1,2,2-Tetrachloroethane ND ug/L 08/25/21 14:34 79-34-550.0 50
Tetrachloroethene ND ug/L 08/25/21 14:34 127-18-450.0 50
Toluene 247 ug/L 08/25/21 14:34 108-88-350.0 50
1,2,3-Trichlorobenzene ND ug/L 08/25/21 14:34 87-61-650.0 50
1,2,4-Trichlorobenzene ND ug/L 08/25/21 14:34 120-82-150.0 50
1,1,1-Trichloroethane ND ug/L 08/25/21 14:34 71-55-650.0 50
1,1,2-Trichloroethane ND ug/L 08/25/21 14:34 79-00-550.0 50
Trichloroethene ND ug/L 08/25/21 14:34 79-01-650.0 50
Trichlorofluoromethane ND ug/L 08/25/21 14:34 75-69-450.0 50
1,2,3-Trichloropropane ND ug/L 08/25/21 14:34 96-18-450.0 50
1,2,4-Trimethylbenzene 2260 ug/L 08/25/21 14:34 95-63-650.0 50
1,3,5-Trimethylbenzene ND ug/L 08/25/21 14:34 108-67-850.0 50
Vinyl acetate ND ug/L 08/25/21 14:34 108-05-4 v1100 50
Vinyl chloride ND ug/L 08/25/21 14:34 75-01-450.0 50
Xylene (Total)17500 ug/L 08/25/21 14:34 1330-20-750.0 50
m&p-Xylene 11900 ug/L 08/25/21 14:34 179601-23-1100 50
o-Xylene 5600 ug/L 08/25/21 14:34 95-47-650.0 50
Surrogates
4-Bromofluorobenzene (S)99 %08/25/21 14:34 460-00-470-130 50
1,2-Dichloroethane-d4 (S)100 %08/25/21 14:34 17060-07-070-130 50
Toluene-d8 (S)105 %08/25/21 14:34 2037-26-570-130 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92557149
LOADING RACK
Sample: AMW-5 Lab ID: 92557149006 Collected: 08/21/21 13:38 Received: 08/24/21 10:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 08/25/21 12:48 67-64-125.0 1
Benzene ND ug/L 08/25/21 12:48 71-43-21.0 1
Bromobenzene ND ug/L 08/25/21 12:48 108-86-11.0 1
Bromochloromethane ND ug/L 08/25/21 12:48 74-97-51.0 1
Bromodichloromethane ND ug/L 08/25/21 12:48 75-27-41.0 1
Bromoform ND ug/L 08/25/21 12:48 75-25-21.0 1
Bromomethane ND ug/L 08/25/21 12:48 74-83-92.0 1
2-Butanone (MEK)ND ug/L 08/25/21 12:48 78-93-35.0 1
n-Butylbenzene ND ug/L 08/25/21 12:48 104-51-81.0 1
sec-Butylbenzene ND ug/L 08/25/21 12:48 135-98-81.0 1
Carbon tetrachloride ND ug/L 08/25/21 12:48 56-23-51.0 1
Chlorobenzene ND ug/L 08/25/21 12:48 108-90-71.0 1
Chloroethane ND ug/L 08/25/21 12:48 75-00-3 IL1.0 1
Chloroform ND ug/L 08/25/21 12:48 67-66-31.0 1
Chloromethane ND ug/L 08/25/21 12:48 74-87-31.0 1
2-Chlorotoluene ND ug/L 08/25/21 12:48 95-49-81.0 1
4-Chlorotoluene ND ug/L 08/25/21 12:48 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 08/25/21 12:48 96-12-82.0 1
Dibromochloromethane ND ug/L 08/25/21 12:48 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 08/25/21 12:48 106-93-41.0 1
Dibromomethane ND ug/L 08/25/21 12:48 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 08/25/21 12:48 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 08/25/21 12:48 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 08/25/21 12:48 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 08/25/21 12:48 75-71-81.0 1
1,1-Dichloroethane ND ug/L 08/25/21 12:48 75-34-31.0 1
1,2-Dichloroethane ND ug/L 08/25/21 12:48 107-06-21.0 1
1,1-Dichloroethene ND ug/L 08/25/21 12:48 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 08/25/21 12:48 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 08/25/21 12:48 156-60-51.0 1
1,2-Dichloropropane ND ug/L 08/25/21 12:48 78-87-51.0 1
1,3-Dichloropropane ND ug/L 08/25/21 12:48 142-28-91.0 1
2,2-Dichloropropane ND ug/L 08/25/21 12:48 594-20-71.0 1
1,1-Dichloropropene ND ug/L 08/25/21 12:48 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 08/25/21 12:48 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 08/25/21 12:48 10061-02-61.0 1
Diisopropyl ether 5.9 ug/L 08/25/21 12:48 108-20-31.0 1
Ethylbenzene ND ug/L 08/25/21 12:48 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 08/25/21 12:48 87-68-32.0 1
2-Hexanone ND ug/L 08/25/21 12:48 591-78-65.0 1
Isopropylbenzene (Cumene)18.4 ug/L 08/25/21 12:48 98-82-81.0 1
p-Isopropyltoluene ND ug/L 08/25/21 12:48 99-87-61.0 1
Methylene Chloride ND ug/L 08/25/21 12:48 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/25/21 12:48 108-10-15.0 1
Methyl-tert-butyl ether 6.2 ug/L 08/25/21 12:48 1634-04-41.0 1
Naphthalene ND ug/L 08/25/21 12:48 91-20-31.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92557149
LOADING RACK
Sample: AMW-5 Lab ID: 92557149006 Collected: 08/21/21 13:38 Received: 08/24/21 10:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
n-Propylbenzene 2.3 ug/L 08/25/21 12:48 103-65-11.0 1
Styrene ND ug/L 08/25/21 12:48 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 08/25/21 12:48 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 08/25/21 12:48 79-34-51.0 1
Tetrachloroethene ND ug/L 08/25/21 12:48 127-18-41.0 1
Toluene ND ug/L 08/25/21 12:48 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 08/25/21 12:48 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 08/25/21 12:48 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 08/25/21 12:48 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 08/25/21 12:48 79-00-51.0 1
Trichloroethene ND ug/L 08/25/21 12:48 79-01-61.0 1
Trichlorofluoromethane ND ug/L 08/25/21 12:48 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 08/25/21 12:48 96-18-41.0 1
1,2,4-Trimethylbenzene ND ug/L 08/25/21 12:48 95-63-61.0 1
1,3,5-Trimethylbenzene ND ug/L 08/25/21 12:48 108-67-81.0 1
Vinyl acetate ND ug/L 08/25/21 12:48 108-05-4 v12.0 1
Vinyl chloride ND ug/L 08/25/21 12:48 75-01-41.0 1
Xylene (Total)ND ug/L 08/25/21 12:48 1330-20-71.0 1
m&p-Xylene ND ug/L 08/25/21 12:48 179601-23-12.0 1
o-Xylene ND ug/L 08/25/21 12:48 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)99 %08/25/21 12:48 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %08/25/21 12:48 17060-07-070-130 1
Toluene-d8 (S)99 %08/25/21 12:48 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92557149
LOADING RACK
Sample: KDW-1 Lab ID: 92557149007 Collected: 08/23/21 15:10 Received: 08/24/21 10:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 08/24/21 20:05 67-64-125.0 1
Benzene ND ug/L 08/24/21 20:05 71-43-21.0 1
Bromobenzene ND ug/L 08/24/21 20:05 108-86-11.0 1
Bromochloromethane ND ug/L 08/24/21 20:05 74-97-51.0 1
Bromodichloromethane ND ug/L 08/24/21 20:05 75-27-41.0 1
Bromoform ND ug/L 08/24/21 20:05 75-25-21.0 1
Bromomethane ND ug/L 08/24/21 20:05 74-83-92.0 1
2-Butanone (MEK)ND ug/L 08/24/21 20:05 78-93-35.0 1
n-Butylbenzene ND ug/L 08/24/21 20:05 104-51-81.0 1
sec-Butylbenzene ND ug/L 08/24/21 20:05 135-98-81.0 1
Carbon tetrachloride ND ug/L 08/24/21 20:05 56-23-51.0 1
Chlorobenzene ND ug/L 08/24/21 20:05 108-90-71.0 1
Chloroethane ND ug/L 08/24/21 20:05 75-00-31.0 1
Chloroform ND ug/L 08/24/21 20:05 67-66-31.0 1
Chloromethane ND ug/L 08/24/21 20:05 74-87-31.0 1
2-Chlorotoluene ND ug/L 08/24/21 20:05 95-49-81.0 1
4-Chlorotoluene ND ug/L 08/24/21 20:05 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 08/24/21 20:05 96-12-82.0 1
Dibromochloromethane ND ug/L 08/24/21 20:05 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 08/24/21 20:05 106-93-41.0 1
Dibromomethane ND ug/L 08/24/21 20:05 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 08/24/21 20:05 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 08/24/21 20:05 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 08/24/21 20:05 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 08/24/21 20:05 75-71-81.0 1
1,1-Dichloroethane ND ug/L 08/24/21 20:05 75-34-31.0 1
1,2-Dichloroethane ND ug/L 08/24/21 20:05 107-06-21.0 1
1,1-Dichloroethene ND ug/L 08/24/21 20:05 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 08/24/21 20:05 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 08/24/21 20:05 156-60-51.0 1
1,2-Dichloropropane ND ug/L 08/24/21 20:05 78-87-51.0 1
1,3-Dichloropropane ND ug/L 08/24/21 20:05 142-28-91.0 1
2,2-Dichloropropane ND ug/L 08/24/21 20:05 594-20-71.0 1
1,1-Dichloropropene ND ug/L 08/24/21 20:05 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 08/24/21 20:05 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 08/24/21 20:05 10061-02-61.0 1
Diisopropyl ether ND ug/L 08/24/21 20:05 108-20-31.0 1
Ethylbenzene ND ug/L 08/24/21 20:05 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 08/24/21 20:05 87-68-32.0 1
2-Hexanone ND ug/L 08/24/21 20:05 591-78-65.0 1
Isopropylbenzene (Cumene)ND ug/L 08/24/21 20:05 98-82-81.0 1
p-Isopropyltoluene ND ug/L 08/24/21 20:05 99-87-61.0 1
Methylene Chloride ND ug/L 08/24/21 20:05 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/24/21 20:05 108-10-15.0 1
Methyl-tert-butyl ether 7.6 ug/L 08/24/21 20:05 1634-04-41.0 1
Naphthalene ND ug/L 08/24/21 20:05 91-20-31.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92557149
LOADING RACK
Sample: KDW-1 Lab ID: 92557149007 Collected: 08/23/21 15:10 Received: 08/24/21 10:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
n-Propylbenzene ND ug/L 08/24/21 20:05 103-65-11.0 1
Styrene ND ug/L 08/24/21 20:05 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 08/24/21 20:05 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 08/24/21 20:05 79-34-51.0 1
Tetrachloroethene ND ug/L 08/24/21 20:05 127-18-41.0 1
Toluene ND ug/L 08/24/21 20:05 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 08/24/21 20:05 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 08/24/21 20:05 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 08/24/21 20:05 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 08/24/21 20:05 79-00-51.0 1
Trichloroethene ND ug/L 08/24/21 20:05 79-01-61.0 1
Trichlorofluoromethane ND ug/L 08/24/21 20:05 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 08/24/21 20:05 96-18-41.0 1
1,2,4-Trimethylbenzene ND ug/L 08/24/21 20:05 95-63-61.0 1
1,3,5-Trimethylbenzene ND ug/L 08/24/21 20:05 108-67-81.0 1
Vinyl acetate ND ug/L 08/24/21 20:05 108-05-42.0 1
Vinyl chloride ND ug/L 08/24/21 20:05 75-01-41.0 1
Xylene (Total)ND ug/L 08/24/21 20:05 1330-20-71.0 1
m&p-Xylene ND ug/L 08/24/21 20:05 179601-23-12.0 1
o-Xylene ND ug/L 08/24/21 20:05 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)96 %08/24/21 20:05 460-00-470-130 1
1,2-Dichloroethane-d4 (S)96 %08/24/21 20:05 17060-07-070-130 1
Toluene-d8 (S)98 %08/24/21 20:05 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92557149
LOADING RACK
Sample: KMW-1 Lab ID: 92557149008 Collected: 08/21/21 08:33 Received: 08/24/21 10:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 08/24/21 20:23 67-64-125.0 1
Benzene ND ug/L 08/24/21 20:23 71-43-21.0 1
Bromobenzene ND ug/L 08/24/21 20:23 108-86-11.0 1
Bromochloromethane ND ug/L 08/24/21 20:23 74-97-51.0 1
Bromodichloromethane ND ug/L 08/24/21 20:23 75-27-41.0 1
Bromoform ND ug/L 08/24/21 20:23 75-25-21.0 1
Bromomethane ND ug/L 08/24/21 20:23 74-83-9 v22.0 1
2-Butanone (MEK)ND ug/L 08/24/21 20:23 78-93-35.0 1
n-Butylbenzene ND ug/L 08/24/21 20:23 104-51-81.0 1
sec-Butylbenzene ND ug/L 08/24/21 20:23 135-98-81.0 1
Carbon tetrachloride ND ug/L 08/24/21 20:23 56-23-51.0 1
Chlorobenzene ND ug/L 08/24/21 20:23 108-90-71.0 1
Chloroethane ND ug/L 08/24/21 20:23 75-00-31.0 1
Chloroform ND ug/L 08/24/21 20:23 67-66-31.0 1
Chloromethane ND ug/L 08/24/21 20:23 74-87-31.0 1
2-Chlorotoluene ND ug/L 08/24/21 20:23 95-49-81.0 1
4-Chlorotoluene ND ug/L 08/24/21 20:23 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 08/24/21 20:23 96-12-82.0 1
Dibromochloromethane ND ug/L 08/24/21 20:23 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 08/24/21 20:23 106-93-41.0 1
Dibromomethane ND ug/L 08/24/21 20:23 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 08/24/21 20:23 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 08/24/21 20:23 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 08/24/21 20:23 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 08/24/21 20:23 75-71-81.0 1
1,1-Dichloroethane ND ug/L 08/24/21 20:23 75-34-31.0 1
1,2-Dichloroethane ND ug/L 08/24/21 20:23 107-06-21.0 1
1,1-Dichloroethene ND ug/L 08/24/21 20:23 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 08/24/21 20:23 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 08/24/21 20:23 156-60-51.0 1
1,2-Dichloropropane ND ug/L 08/24/21 20:23 78-87-51.0 1
1,3-Dichloropropane ND ug/L 08/24/21 20:23 142-28-91.0 1
2,2-Dichloropropane ND ug/L 08/24/21 20:23 594-20-71.0 1
1,1-Dichloropropene ND ug/L 08/24/21 20:23 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 08/24/21 20:23 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 08/24/21 20:23 10061-02-61.0 1
Diisopropyl ether ND ug/L 08/24/21 20:23 108-20-31.0 1
Ethylbenzene ND ug/L 08/24/21 20:23 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 08/24/21 20:23 87-68-32.0 1
2-Hexanone ND ug/L 08/24/21 20:23 591-78-65.0 1
Isopropylbenzene (Cumene)ND ug/L 08/24/21 20:23 98-82-81.0 1
p-Isopropyltoluene ND ug/L 08/24/21 20:23 99-87-61.0 1
Methylene Chloride ND ug/L 08/24/21 20:23 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/24/21 20:23 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 08/24/21 20:23 1634-04-41.0 1
Naphthalene ND ug/L 08/24/21 20:23 91-20-31.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92557149
LOADING RACK
Sample: KMW-1 Lab ID: 92557149008 Collected: 08/21/21 08:33 Received: 08/24/21 10:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
n-Propylbenzene ND ug/L 08/24/21 20:23 103-65-11.0 1
Styrene ND ug/L 08/24/21 20:23 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 08/24/21 20:23 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 08/24/21 20:23 79-34-51.0 1
Tetrachloroethene ND ug/L 08/24/21 20:23 127-18-41.0 1
Toluene ND ug/L 08/24/21 20:23 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 08/24/21 20:23 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 08/24/21 20:23 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 08/24/21 20:23 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 08/24/21 20:23 79-00-51.0 1
Trichloroethene ND ug/L 08/24/21 20:23 79-01-61.0 1
Trichlorofluoromethane ND ug/L 08/24/21 20:23 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 08/24/21 20:23 96-18-41.0 1
1,2,4-Trimethylbenzene ND ug/L 08/24/21 20:23 95-63-61.0 1
1,3,5-Trimethylbenzene ND ug/L 08/24/21 20:23 108-67-81.0 1
Vinyl acetate ND ug/L 08/24/21 20:23 108-05-42.0 1
Vinyl chloride ND ug/L 08/24/21 20:23 75-01-41.0 1
Xylene (Total)ND ug/L 08/24/21 20:23 1330-20-71.0 1
m&p-Xylene ND ug/L 08/24/21 20:23 179601-23-12.0 1
o-Xylene ND ug/L 08/24/21 20:23 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)96 %08/24/21 20:23 460-00-470-130 1
1,2-Dichloroethane-d4 (S)96 %08/24/21 20:23 17060-07-070-130 1
Toluene-d8 (S)97 %08/24/21 20:23 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92557149
LOADING RACK
Sample: KMW-3 Lab ID: 92557149009 Collected: 08/21/21 10:51 Received: 08/24/21 10:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 08/25/21 11:19 67-64-125.0 1
Benzene 8.0 ug/L 08/25/21 11:19 71-43-21.0 1
Bromobenzene ND ug/L 08/25/21 11:19 108-86-11.0 1
Bromochloromethane ND ug/L 08/25/21 11:19 74-97-51.0 1
Bromodichloromethane ND ug/L 08/25/21 11:19 75-27-41.0 1
Bromoform ND ug/L 08/25/21 11:19 75-25-21.0 1
Bromomethane ND ug/L 08/25/21 11:19 74-83-92.0 1
2-Butanone (MEK)ND ug/L 08/25/21 11:19 78-93-35.0 1
n-Butylbenzene ND ug/L 08/25/21 11:19 104-51-81.0 1
sec-Butylbenzene 1.1 ug/L 08/25/21 11:19 135-98-81.0 1
Carbon tetrachloride ND ug/L 08/25/21 11:19 56-23-51.0 1
Chlorobenzene ND ug/L 08/25/21 11:19 108-90-71.0 1
Chloroethane ND ug/L 08/25/21 11:19 75-00-3 IL1.0 1
Chloroform ND ug/L 08/25/21 11:19 67-66-31.0 1
Chloromethane ND ug/L 08/25/21 11:19 74-87-31.0 1
2-Chlorotoluene ND ug/L 08/25/21 11:19 95-49-81.0 1
4-Chlorotoluene ND ug/L 08/25/21 11:19 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 08/25/21 11:19 96-12-82.0 1
Dibromochloromethane ND ug/L 08/25/21 11:19 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 08/25/21 11:19 106-93-41.0 1
Dibromomethane ND ug/L 08/25/21 11:19 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 08/25/21 11:19 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 08/25/21 11:19 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 08/25/21 11:19 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 08/25/21 11:19 75-71-81.0 1
1,1-Dichloroethane ND ug/L 08/25/21 11:19 75-34-31.0 1
1,2-Dichloroethane ND ug/L 08/25/21 11:19 107-06-21.0 1
1,1-Dichloroethene ND ug/L 08/25/21 11:19 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 08/25/21 11:19 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 08/25/21 11:19 156-60-51.0 1
1,2-Dichloropropane ND ug/L 08/25/21 11:19 78-87-51.0 1
1,3-Dichloropropane ND ug/L 08/25/21 11:19 142-28-91.0 1
2,2-Dichloropropane ND ug/L 08/25/21 11:19 594-20-71.0 1
1,1-Dichloropropene ND ug/L 08/25/21 11:19 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 08/25/21 11:19 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 08/25/21 11:19 10061-02-61.0 1
Diisopropyl ether ND ug/L 08/25/21 11:19 108-20-31.0 1
Ethylbenzene ND ug/L 08/25/21 11:19 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 08/25/21 11:19 87-68-32.0 1
2-Hexanone ND ug/L 08/25/21 11:19 591-78-65.0 1
Isopropylbenzene (Cumene)11.6 ug/L 08/25/21 11:19 98-82-81.0 1
p-Isopropyltoluene ND ug/L 08/25/21 11:19 99-87-61.0 1
Methylene Chloride ND ug/L 08/25/21 11:19 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/25/21 11:19 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 08/25/21 11:19 1634-04-41.0 1
Naphthalene ND ug/L 08/25/21 11:19 91-20-31.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92557149
LOADING RACK
Sample: KMW-3 Lab ID: 92557149009 Collected: 08/21/21 10:51 Received: 08/24/21 10:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
n-Propylbenzene 7.5 ug/L 08/25/21 11:19 103-65-11.0 1
Styrene ND ug/L 08/25/21 11:19 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 08/25/21 11:19 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 08/25/21 11:19 79-34-51.0 1
Tetrachloroethene ND ug/L 08/25/21 11:19 127-18-41.0 1
Toluene 1.6 ug/L 08/25/21 11:19 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 08/25/21 11:19 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 08/25/21 11:19 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 08/25/21 11:19 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 08/25/21 11:19 79-00-51.0 1
Trichloroethene ND ug/L 08/25/21 11:19 79-01-61.0 1
Trichlorofluoromethane ND ug/L 08/25/21 11:19 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 08/25/21 11:19 96-18-41.0 1
1,2,4-Trimethylbenzene ND ug/L 08/25/21 11:19 95-63-61.0 1
1,3,5-Trimethylbenzene ND ug/L 08/25/21 11:19 108-67-81.0 1
Vinyl acetate ND ug/L 08/25/21 11:19 108-05-4 v12.0 1
Vinyl chloride ND ug/L 08/25/21 11:19 75-01-41.0 1
Xylene (Total)ND ug/L 08/25/21 11:19 1330-20-71.0 1
m&p-Xylene ND ug/L 08/25/21 11:19 179601-23-12.0 1
o-Xylene ND ug/L 08/25/21 11:19 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)101 %08/25/21 11:19 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %08/25/21 11:19 17060-07-070-130 1
Toluene-d8 (S)103 %08/25/21 11:19 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92557149
LOADING RACK
Sample: KMW-5 Lab ID: 92557149010 Collected: 08/21/21 09:23 Received: 08/24/21 10:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 08/24/21 19:29 67-64-125.0 1
Benzene ND ug/L 08/24/21 19:29 71-43-21.0 1
Bromobenzene ND ug/L 08/24/21 19:29 108-86-11.0 1
Bromochloromethane ND ug/L 08/24/21 19:29 74-97-51.0 1
Bromodichloromethane ND ug/L 08/24/21 19:29 75-27-41.0 1
Bromoform ND ug/L 08/24/21 19:29 75-25-21.0 1
Bromomethane ND ug/L 08/24/21 19:29 74-83-92.0 1
2-Butanone (MEK)ND ug/L 08/24/21 19:29 78-93-35.0 1
n-Butylbenzene ND ug/L 08/24/21 19:29 104-51-81.0 1
sec-Butylbenzene ND ug/L 08/24/21 19:29 135-98-81.0 1
Carbon tetrachloride ND ug/L 08/24/21 19:29 56-23-51.0 1
Chlorobenzene ND ug/L 08/24/21 19:29 108-90-71.0 1
Chloroethane ND ug/L 08/24/21 19:29 75-00-31.0 1
Chloroform ND ug/L 08/24/21 19:29 67-66-31.0 1
Chloromethane ND ug/L 08/24/21 19:29 74-87-31.0 1
2-Chlorotoluene ND ug/L 08/24/21 19:29 95-49-81.0 1
4-Chlorotoluene ND ug/L 08/24/21 19:29 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 08/24/21 19:29 96-12-82.0 1
Dibromochloromethane ND ug/L 08/24/21 19:29 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 08/24/21 19:29 106-93-41.0 1
Dibromomethane ND ug/L 08/24/21 19:29 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 08/24/21 19:29 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 08/24/21 19:29 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 08/24/21 19:29 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 08/24/21 19:29 75-71-81.0 1
1,1-Dichloroethane ND ug/L 08/24/21 19:29 75-34-31.0 1
1,2-Dichloroethane ND ug/L 08/24/21 19:29 107-06-21.0 1
1,1-Dichloroethene ND ug/L 08/24/21 19:29 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 08/24/21 19:29 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 08/24/21 19:29 156-60-51.0 1
1,2-Dichloropropane ND ug/L 08/24/21 19:29 78-87-51.0 1
1,3-Dichloropropane ND ug/L 08/24/21 19:29 142-28-91.0 1
2,2-Dichloropropane ND ug/L 08/24/21 19:29 594-20-71.0 1
1,1-Dichloropropene ND ug/L 08/24/21 19:29 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 08/24/21 19:29 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 08/24/21 19:29 10061-02-61.0 1
Diisopropyl ether ND ug/L 08/24/21 19:29 108-20-31.0 1
Ethylbenzene ND ug/L 08/24/21 19:29 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 08/24/21 19:29 87-68-32.0 1
2-Hexanone ND ug/L 08/24/21 19:29 591-78-65.0 1
Isopropylbenzene (Cumene)ND ug/L 08/24/21 19:29 98-82-81.0 1
p-Isopropyltoluene ND ug/L 08/24/21 19:29 99-87-61.0 1
Methylene Chloride ND ug/L 08/24/21 19:29 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/24/21 19:29 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 08/24/21 19:29 1634-04-41.0 1
Naphthalene ND ug/L 08/24/21 19:29 91-20-31.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92557149
LOADING RACK
Sample: KMW-5 Lab ID: 92557149010 Collected: 08/21/21 09:23 Received: 08/24/21 10:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
n-Propylbenzene ND ug/L 08/24/21 19:29 103-65-11.0 1
Styrene ND ug/L 08/24/21 19:29 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 08/24/21 19:29 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 08/24/21 19:29 79-34-51.0 1
Tetrachloroethene ND ug/L 08/24/21 19:29 127-18-41.0 1
Toluene ND ug/L 08/24/21 19:29 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 08/24/21 19:29 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 08/24/21 19:29 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 08/24/21 19:29 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 08/24/21 19:29 79-00-51.0 1
Trichloroethene ND ug/L 08/24/21 19:29 79-01-61.0 1
Trichlorofluoromethane ND ug/L 08/24/21 19:29 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 08/24/21 19:29 96-18-41.0 1
1,2,4-Trimethylbenzene ND ug/L 08/24/21 19:29 95-63-61.0 1
1,3,5-Trimethylbenzene ND ug/L 08/24/21 19:29 108-67-81.0 1
Vinyl acetate ND ug/L 08/24/21 19:29 108-05-42.0 1
Vinyl chloride ND ug/L 08/24/21 19:29 75-01-41.0 1
Xylene (Total)ND ug/L 08/24/21 19:29 1330-20-71.0 1
m&p-Xylene ND ug/L 08/24/21 19:29 179601-23-12.0 1
o-Xylene ND ug/L 08/24/21 19:29 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)97 %08/24/21 19:29 460-00-470-130 1
1,2-Dichloroethane-d4 (S)96 %08/24/21 19:29 17060-07-070-130 1
Toluene-d8 (S)98 %08/24/21 19:29 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92557149
LOADING RACK
Sample: KMW-6 Lab ID: 92557149011 Collected: 08/22/21 12:20 Received: 08/24/21 10:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 08/25/21 14:17 67-64-1625 25
Benzene ND ug/L 08/25/21 14:17 71-43-225.0 25
Bromobenzene ND ug/L 08/25/21 14:17 108-86-125.0 25
Bromochloromethane ND ug/L 08/25/21 14:17 74-97-525.0 25
Bromodichloromethane ND ug/L 08/25/21 14:17 75-27-425.0 25
Bromoform ND ug/L 08/25/21 14:17 75-25-225.0 25
Bromomethane ND ug/L 08/25/21 14:17 74-83-950.0 25
2-Butanone (MEK)ND ug/L 08/25/21 14:17 78-93-3125 25
n-Butylbenzene ND ug/L 08/25/21 14:17 104-51-825.0 25
sec-Butylbenzene ND ug/L 08/25/21 14:17 135-98-825.0 25
Carbon tetrachloride ND ug/L 08/25/21 14:17 56-23-525.0 25
Chlorobenzene ND ug/L 08/25/21 14:17 108-90-725.0 25
Chloroethane ND ug/L 08/25/21 14:17 75-00-3 IL25.0 25
Chloroform ND ug/L 08/25/21 14:17 67-66-325.0 25
Chloromethane ND ug/L 08/25/21 14:17 74-87-325.0 25
2-Chlorotoluene ND ug/L 08/25/21 14:17 95-49-825.0 25
4-Chlorotoluene ND ug/L 08/25/21 14:17 106-43-425.0 25
1,2-Dibromo-3-chloropropane ND ug/L 08/25/21 14:17 96-12-850.0 25
Dibromochloromethane ND ug/L 08/25/21 14:17 124-48-125.0 25
1,2-Dibromoethane (EDB)ND ug/L 08/25/21 14:17 106-93-425.0 25
Dibromomethane ND ug/L 08/25/21 14:17 74-95-325.0 25
1,2-Dichlorobenzene ND ug/L 08/25/21 14:17 95-50-125.0 25
1,3-Dichlorobenzene ND ug/L 08/25/21 14:17 541-73-125.0 25
1,4-Dichlorobenzene ND ug/L 08/25/21 14:17 106-46-725.0 25
Dichlorodifluoromethane ND ug/L 08/25/21 14:17 75-71-825.0 25
1,1-Dichloroethane ND ug/L 08/25/21 14:17 75-34-325.0 25
1,2-Dichloroethane ND ug/L 08/25/21 14:17 107-06-225.0 25
1,1-Dichloroethene ND ug/L 08/25/21 14:17 75-35-425.0 25
cis-1,2-Dichloroethene ND ug/L 08/25/21 14:17 156-59-225.0 25
trans-1,2-Dichloroethene ND ug/L 08/25/21 14:17 156-60-525.0 25
1,2-Dichloropropane ND ug/L 08/25/21 14:17 78-87-525.0 25
1,3-Dichloropropane ND ug/L 08/25/21 14:17 142-28-925.0 25
2,2-Dichloropropane ND ug/L 08/25/21 14:17 594-20-725.0 25
1,1-Dichloropropene ND ug/L 08/25/21 14:17 563-58-625.0 25
cis-1,3-Dichloropropene ND ug/L 08/25/21 14:17 10061-01-525.0 25
trans-1,3-Dichloropropene ND ug/L 08/25/21 14:17 10061-02-625.0 25
Diisopropyl ether ND ug/L 08/25/21 14:17 108-20-325.0 25
Ethylbenzene ND ug/L 08/25/21 14:17 100-41-425.0 25
Hexachloro-1,3-butadiene ND ug/L 08/25/21 14:17 87-68-350.0 25
2-Hexanone ND ug/L 08/25/21 14:17 591-78-6125 25
Isopropylbenzene (Cumene)ND ug/L 08/25/21 14:17 98-82-825.0 25
p-Isopropyltoluene ND ug/L 08/25/21 14:17 99-87-625.0 25
Methylene Chloride ND ug/L 08/25/21 14:17 75-09-2125 25
4-Methyl-2-pentanone (MIBK)ND ug/L 08/25/21 14:17 108-10-1125 25
Methyl-tert-butyl ether ND ug/L 08/25/21 14:17 1634-04-425.0 25
Naphthalene ND ug/L 08/25/21 14:17 91-20-325.0 25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92557149
LOADING RACK
Sample: KMW-6 Lab ID: 92557149011 Collected: 08/22/21 12:20 Received: 08/24/21 10:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
n-Propylbenzene ND ug/L 08/25/21 14:17 103-65-125.0 25
Styrene ND ug/L 08/25/21 14:17 100-42-525.0 25
1,1,1,2-Tetrachloroethane ND ug/L 08/25/21 14:17 630-20-625.0 25
1,1,2,2-Tetrachloroethane ND ug/L 08/25/21 14:17 79-34-525.0 25
Tetrachloroethene ND ug/L 08/25/21 14:17 127-18-425.0 25
Toluene ND ug/L 08/25/21 14:17 108-88-325.0 25
1,2,3-Trichlorobenzene ND ug/L 08/25/21 14:17 87-61-625.0 25
1,2,4-Trichlorobenzene ND ug/L 08/25/21 14:17 120-82-125.0 25
1,1,1-Trichloroethane ND ug/L 08/25/21 14:17 71-55-625.0 25
1,1,2-Trichloroethane ND ug/L 08/25/21 14:17 79-00-525.0 25
Trichloroethene ND ug/L 08/25/21 14:17 79-01-625.0 25
Trichlorofluoromethane ND ug/L 08/25/21 14:17 75-69-425.0 25
1,2,3-Trichloropropane ND ug/L 08/25/21 14:17 96-18-425.0 25
1,2,4-Trimethylbenzene ND ug/L 08/25/21 14:17 95-63-625.0 25
1,3,5-Trimethylbenzene ND ug/L 08/25/21 14:17 108-67-825.0 25
Vinyl acetate ND ug/L 08/25/21 14:17 108-05-4 v150.0 25
Vinyl chloride ND ug/L 08/25/21 14:17 75-01-425.0 25
Xylene (Total)7120 ug/L 08/25/21 14:17 1330-20-725.0 25
m&p-Xylene 7120 ug/L 08/25/21 14:17 179601-23-150.0 25
o-Xylene ND ug/L 08/25/21 14:17 95-47-625.0 25
Surrogates
4-Bromofluorobenzene (S)98 %08/25/21 14:17 460-00-470-130 25
1,2-Dichloroethane-d4 (S)99 %08/25/21 14:17 17060-07-070-130 25
Toluene-d8 (S)105 %08/25/21 14:17 2037-26-570-130 25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92557149
LOADING RACK
Sample: KMW-7 Lab ID: 92557149012 Collected: 08/23/21 09:21 Received: 08/24/21 10:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 08/25/21 11:01 67-64-125.0 1
Benzene ND ug/L 08/25/21 11:01 71-43-21.0 1
Bromobenzene ND ug/L 08/25/21 11:01 108-86-11.0 1
Bromochloromethane ND ug/L 08/25/21 11:01 74-97-51.0 1
Bromodichloromethane ND ug/L 08/25/21 11:01 75-27-41.0 1
Bromoform ND ug/L 08/25/21 11:01 75-25-21.0 1
Bromomethane ND ug/L 08/25/21 11:01 74-83-92.0 1
2-Butanone (MEK)ND ug/L 08/25/21 11:01 78-93-35.0 1
n-Butylbenzene ND ug/L 08/25/21 11:01 104-51-81.0 1
sec-Butylbenzene ND ug/L 08/25/21 11:01 135-98-81.0 1
Carbon tetrachloride ND ug/L 08/25/21 11:01 56-23-51.0 1
Chlorobenzene ND ug/L 08/25/21 11:01 108-90-71.0 1
Chloroethane ND ug/L 08/25/21 11:01 75-00-3 IL1.0 1
Chloroform ND ug/L 08/25/21 11:01 67-66-31.0 1
Chloromethane ND ug/L 08/25/21 11:01 74-87-31.0 1
2-Chlorotoluene ND ug/L 08/25/21 11:01 95-49-81.0 1
4-Chlorotoluene ND ug/L 08/25/21 11:01 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 08/25/21 11:01 96-12-82.0 1
Dibromochloromethane ND ug/L 08/25/21 11:01 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 08/25/21 11:01 106-93-41.0 1
Dibromomethane ND ug/L 08/25/21 11:01 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 08/25/21 11:01 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 08/25/21 11:01 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 08/25/21 11:01 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 08/25/21 11:01 75-71-81.0 1
1,1-Dichloroethane ND ug/L 08/25/21 11:01 75-34-31.0 1
1,2-Dichloroethane ND ug/L 08/25/21 11:01 107-06-21.0 1
1,1-Dichloroethene ND ug/L 08/25/21 11:01 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 08/25/21 11:01 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 08/25/21 11:01 156-60-51.0 1
1,2-Dichloropropane ND ug/L 08/25/21 11:01 78-87-51.0 1
1,3-Dichloropropane ND ug/L 08/25/21 11:01 142-28-91.0 1
2,2-Dichloropropane ND ug/L 08/25/21 11:01 594-20-71.0 1
1,1-Dichloropropene ND ug/L 08/25/21 11:01 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 08/25/21 11:01 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 08/25/21 11:01 10061-02-61.0 1
Diisopropyl ether ND ug/L 08/25/21 11:01 108-20-31.0 1
Ethylbenzene ND ug/L 08/25/21 11:01 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 08/25/21 11:01 87-68-32.0 1
2-Hexanone ND ug/L 08/25/21 11:01 591-78-65.0 1
Isopropylbenzene (Cumene)1.9 ug/L 08/25/21 11:01 98-82-81.0 1
p-Isopropyltoluene ND ug/L 08/25/21 11:01 99-87-61.0 1
Methylene Chloride ND ug/L 08/25/21 11:01 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/25/21 11:01 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 08/25/21 11:01 1634-04-41.0 1
Naphthalene ND ug/L 08/25/21 11:01 91-20-31.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92557149
LOADING RACK
Sample: KMW-7 Lab ID: 92557149012 Collected: 08/23/21 09:21 Received: 08/24/21 10:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
n-Propylbenzene 2.3 ug/L 08/25/21 11:01 103-65-11.0 1
Styrene ND ug/L 08/25/21 11:01 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 08/25/21 11:01 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 08/25/21 11:01 79-34-51.0 1
Tetrachloroethene ND ug/L 08/25/21 11:01 127-18-41.0 1
Toluene ND ug/L 08/25/21 11:01 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 08/25/21 11:01 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 08/25/21 11:01 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 08/25/21 11:01 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 08/25/21 11:01 79-00-51.0 1
Trichloroethene ND ug/L 08/25/21 11:01 79-01-61.0 1
Trichlorofluoromethane ND ug/L 08/25/21 11:01 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 08/25/21 11:01 96-18-41.0 1
1,2,4-Trimethylbenzene ND ug/L 08/25/21 11:01 95-63-61.0 1
1,3,5-Trimethylbenzene ND ug/L 08/25/21 11:01 108-67-81.0 1
Vinyl acetate ND ug/L 08/25/21 11:01 108-05-4 v12.0 1
Vinyl chloride ND ug/L 08/25/21 11:01 75-01-41.0 1
Xylene (Total)ND ug/L 08/25/21 11:01 1330-20-71.0 1
m&p-Xylene ND ug/L 08/25/21 11:01 179601-23-12.0 1
o-Xylene ND ug/L 08/25/21 11:01 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)100 %08/25/21 11:01 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %08/25/21 11:01 17060-07-070-130 1
Toluene-d8 (S)104 %08/25/21 11:01 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92557149
LOADING RACK
Sample: KMW-8 Lab ID: 92557149013 Collected: 08/22/21 12:55 Received: 08/24/21 10:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 08/25/21 18:21 67-64-125.0 1
Benzene 44.9 ug/L 08/25/21 18:21 71-43-21.0 1
Bromobenzene ND ug/L 08/25/21 18:21 108-86-11.0 1
Bromochloromethane ND ug/L 08/25/21 18:21 74-97-51.0 1
Bromodichloromethane ND ug/L 08/25/21 18:21 75-27-41.0 1
Bromoform ND ug/L 08/25/21 18:21 75-25-21.0 1
Bromomethane ND ug/L 08/25/21 18:21 74-83-92.0 1
2-Butanone (MEK)ND ug/L 08/25/21 18:21 78-93-35.0 1
n-Butylbenzene 1.7 ug/L 08/25/21 18:21 104-51-81.0 1
sec-Butylbenzene 4.8 ug/L 08/25/21 18:21 135-98-81.0 1
Carbon tetrachloride ND ug/L 08/25/21 18:21 56-23-51.0 1
Chlorobenzene ND ug/L 08/25/21 18:21 108-90-71.0 1
Chloroethane ND ug/L 08/25/21 18:21 75-00-31.0 1
Chloroform ND ug/L 08/25/21 18:21 67-66-31.0 1
Chloromethane ND ug/L 08/25/21 18:21 74-87-31.0 1
2-Chlorotoluene ND ug/L 08/25/21 18:21 95-49-81.0 1
4-Chlorotoluene ND ug/L 08/25/21 18:21 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 08/25/21 18:21 96-12-82.0 1
Dibromochloromethane ND ug/L 08/25/21 18:21 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 08/25/21 18:21 106-93-41.0 1
Dibromomethane ND ug/L 08/25/21 18:21 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 08/25/21 18:21 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 08/25/21 18:21 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 08/25/21 18:21 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 08/25/21 18:21 75-71-81.0 1
1,1-Dichloroethane ND ug/L 08/25/21 18:21 75-34-31.0 1
1,2-Dichloroethane ND ug/L 08/25/21 18:21 107-06-21.0 1
1,1-Dichloroethene ND ug/L 08/25/21 18:21 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 08/25/21 18:21 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 08/25/21 18:21 156-60-51.0 1
1,2-Dichloropropane ND ug/L 08/25/21 18:21 78-87-51.0 1
1,3-Dichloropropane ND ug/L 08/25/21 18:21 142-28-91.0 1
2,2-Dichloropropane ND ug/L 08/25/21 18:21 594-20-71.0 1
1,1-Dichloropropene ND ug/L 08/25/21 18:21 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 08/25/21 18:21 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 08/25/21 18:21 10061-02-61.0 1
Diisopropyl ether ND ug/L 08/25/21 18:21 108-20-31.0 1
Ethylbenzene 9.1 ug/L 08/25/21 18:21 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 08/25/21 18:21 87-68-32.0 1
2-Hexanone ND ug/L 08/25/21 18:21 591-78-65.0 1
Isopropylbenzene (Cumene)22.9 ug/L 08/25/21 18:21 98-82-81.0 1
p-Isopropyltoluene ND ug/L 08/25/21 18:21 99-87-61.0 1
Methylene Chloride ND ug/L 08/25/21 18:21 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/25/21 18:21 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 08/25/21 18:21 1634-04-41.0 1
Naphthalene 6.4 ug/L 08/25/21 18:21 91-20-31.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92557149
LOADING RACK
Sample: KMW-8 Lab ID: 92557149013 Collected: 08/22/21 12:55 Received: 08/24/21 10:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
n-Propylbenzene 22.5 ug/L 08/25/21 18:21 103-65-11.0 1
Styrene ND ug/L 08/25/21 18:21 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 08/25/21 18:21 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 08/25/21 18:21 79-34-51.0 1
Tetrachloroethene ND ug/L 08/25/21 18:21 127-18-41.0 1
Toluene ND ug/L 08/25/21 18:21 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 08/25/21 18:21 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 08/25/21 18:21 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 08/25/21 18:21 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 08/25/21 18:21 79-00-51.0 1
Trichloroethene ND ug/L 08/25/21 18:21 79-01-61.0 1
Trichlorofluoromethane ND ug/L 08/25/21 18:21 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 08/25/21 18:21 96-18-41.0 1
1,2,4-Trimethylbenzene 9.0 ug/L 08/25/21 18:21 95-63-61.0 1
1,3,5-Trimethylbenzene 1.9 ug/L 08/25/21 18:21 108-67-81.0 1
Vinyl acetate ND ug/L 08/25/21 18:21 108-05-42.0 1
Vinyl chloride ND ug/L 08/25/21 18:21 75-01-41.0 1
Xylene (Total)5.7 ug/L 08/25/21 18:21 1330-20-71.0 1
m&p-Xylene 5.7 ug/L 08/25/21 18:21 179601-23-12.0 1
o-Xylene ND ug/L 08/25/21 18:21 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)101 %08/25/21 18:21 460-00-470-130 1
1,2-Dichloroethane-d4 (S)107 %08/25/21 18:21 17060-07-070-130 1
Toluene-d8 (S)103 %08/25/21 18:21 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92557149
LOADING RACK
Sample: KMW-9R Lab ID: 92557149014 Collected: 08/23/21 15:06 Received: 08/24/21 10:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 08/24/21 19:47 67-64-125.0 1
Benzene ND ug/L 08/24/21 19:47 71-43-21.0 1
Bromobenzene ND ug/L 08/24/21 19:47 108-86-11.0 1
Bromochloromethane ND ug/L 08/24/21 19:47 74-97-51.0 1
Bromodichloromethane ND ug/L 08/24/21 19:47 75-27-41.0 1
Bromoform ND ug/L 08/24/21 19:47 75-25-21.0 1
Bromomethane ND ug/L 08/24/21 19:47 74-83-92.0 1
2-Butanone (MEK)ND ug/L 08/24/21 19:47 78-93-35.0 1
n-Butylbenzene ND ug/L 08/24/21 19:47 104-51-81.0 1
sec-Butylbenzene ND ug/L 08/24/21 19:47 135-98-81.0 1
Carbon tetrachloride ND ug/L 08/24/21 19:47 56-23-51.0 1
Chlorobenzene ND ug/L 08/24/21 19:47 108-90-71.0 1
Chloroethane ND ug/L 08/24/21 19:47 75-00-31.0 1
Chloroform ND ug/L 08/24/21 19:47 67-66-31.0 1
Chloromethane ND ug/L 08/24/21 19:47 74-87-31.0 1
2-Chlorotoluene ND ug/L 08/24/21 19:47 95-49-81.0 1
4-Chlorotoluene ND ug/L 08/24/21 19:47 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 08/24/21 19:47 96-12-82.0 1
Dibromochloromethane ND ug/L 08/24/21 19:47 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 08/24/21 19:47 106-93-41.0 1
Dibromomethane ND ug/L 08/24/21 19:47 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 08/24/21 19:47 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 08/24/21 19:47 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 08/24/21 19:47 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 08/24/21 19:47 75-71-81.0 1
1,1-Dichloroethane ND ug/L 08/24/21 19:47 75-34-31.0 1
1,2-Dichloroethane ND ug/L 08/24/21 19:47 107-06-21.0 1
1,1-Dichloroethene ND ug/L 08/24/21 19:47 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 08/24/21 19:47 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 08/24/21 19:47 156-60-51.0 1
1,2-Dichloropropane ND ug/L 08/24/21 19:47 78-87-51.0 1
1,3-Dichloropropane ND ug/L 08/24/21 19:47 142-28-91.0 1
2,2-Dichloropropane ND ug/L 08/24/21 19:47 594-20-71.0 1
1,1-Dichloropropene ND ug/L 08/24/21 19:47 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 08/24/21 19:47 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 08/24/21 19:47 10061-02-61.0 1
Diisopropyl ether ND ug/L 08/24/21 19:47 108-20-31.0 1
Ethylbenzene ND ug/L 08/24/21 19:47 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 08/24/21 19:47 87-68-32.0 1
2-Hexanone ND ug/L 08/24/21 19:47 591-78-65.0 1
Isopropylbenzene (Cumene)ND ug/L 08/24/21 19:47 98-82-81.0 1
p-Isopropyltoluene ND ug/L 08/24/21 19:47 99-87-61.0 1
Methylene Chloride ND ug/L 08/24/21 19:47 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/24/21 19:47 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 08/24/21 19:47 1634-04-41.0 1
Naphthalene 3.6 ug/L 08/24/21 19:47 91-20-31.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92557149
LOADING RACK
Sample: KMW-9R Lab ID: 92557149014 Collected: 08/23/21 15:06 Received: 08/24/21 10:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
n-Propylbenzene ND ug/L 08/24/21 19:47 103-65-11.0 1
Styrene ND ug/L 08/24/21 19:47 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 08/24/21 19:47 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 08/24/21 19:47 79-34-51.0 1
Tetrachloroethene ND ug/L 08/24/21 19:47 127-18-41.0 1
Toluene ND ug/L 08/24/21 19:47 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 08/24/21 19:47 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 08/24/21 19:47 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 08/24/21 19:47 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 08/24/21 19:47 79-00-51.0 1
Trichloroethene ND ug/L 08/24/21 19:47 79-01-61.0 1
Trichlorofluoromethane ND ug/L 08/24/21 19:47 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 08/24/21 19:47 96-18-41.0 1
1,2,4-Trimethylbenzene ND ug/L 08/24/21 19:47 95-63-61.0 1
1,3,5-Trimethylbenzene ND ug/L 08/24/21 19:47 108-67-81.0 1
Vinyl acetate ND ug/L 08/24/21 19:47 108-05-42.0 1
Vinyl chloride ND ug/L 08/24/21 19:47 75-01-41.0 1
Xylene (Total)ND ug/L 08/24/21 19:47 1330-20-71.0 1
m&p-Xylene ND ug/L 08/24/21 19:47 179601-23-12.0 1
o-Xylene ND ug/L 08/24/21 19:47 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)96 %08/24/21 19:47 460-00-470-130 1
1,2-Dichloroethane-d4 (S)96 %08/24/21 19:47 17060-07-070-130 1
Toluene-d8 (S)98 %08/24/21 19:47 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92557149
LOADING RACK
Sample: KMW-12 Lab ID: 92557149015 Collected: 08/22/21 14:09 Received: 08/24/21 10:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 08/25/21 18:39 67-64-125.0 1
Benzene 13.1 ug/L 08/25/21 18:39 71-43-21.0 1
Bromobenzene ND ug/L 08/25/21 18:39 108-86-11.0 1
Bromochloromethane ND ug/L 08/25/21 18:39 74-97-51.0 1
Bromodichloromethane ND ug/L 08/25/21 18:39 75-27-41.0 1
Bromoform ND ug/L 08/25/21 18:39 75-25-21.0 1
Bromomethane ND ug/L 08/25/21 18:39 74-83-92.0 1
2-Butanone (MEK)ND ug/L 08/25/21 18:39 78-93-35.0 1
n-Butylbenzene ND ug/L 08/25/21 18:39 104-51-81.0 1
sec-Butylbenzene ND ug/L 08/25/21 18:39 135-98-81.0 1
Carbon tetrachloride ND ug/L 08/25/21 18:39 56-23-51.0 1
Chlorobenzene ND ug/L 08/25/21 18:39 108-90-71.0 1
Chloroethane ND ug/L 08/25/21 18:39 75-00-31.0 1
Chloroform ND ug/L 08/25/21 18:39 67-66-31.0 1
Chloromethane ND ug/L 08/25/21 18:39 74-87-31.0 1
2-Chlorotoluene ND ug/L 08/25/21 18:39 95-49-81.0 1
4-Chlorotoluene ND ug/L 08/25/21 18:39 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 08/25/21 18:39 96-12-82.0 1
Dibromochloromethane ND ug/L 08/25/21 18:39 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 08/25/21 18:39 106-93-41.0 1
Dibromomethane ND ug/L 08/25/21 18:39 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 08/25/21 18:39 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 08/25/21 18:39 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 08/25/21 18:39 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 08/25/21 18:39 75-71-81.0 1
1,1-Dichloroethane ND ug/L 08/25/21 18:39 75-34-31.0 1
1,2-Dichloroethane ND ug/L 08/25/21 18:39 107-06-21.0 1
1,1-Dichloroethene ND ug/L 08/25/21 18:39 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 08/25/21 18:39 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 08/25/21 18:39 156-60-51.0 1
1,2-Dichloropropane ND ug/L 08/25/21 18:39 78-87-51.0 1
1,3-Dichloropropane ND ug/L 08/25/21 18:39 142-28-91.0 1
2,2-Dichloropropane ND ug/L 08/25/21 18:39 594-20-71.0 1
1,1-Dichloropropene ND ug/L 08/25/21 18:39 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 08/25/21 18:39 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 08/25/21 18:39 10061-02-61.0 1
Diisopropyl ether ND ug/L 08/25/21 18:39 108-20-31.0 1
Ethylbenzene 6.3 ug/L 08/25/21 18:39 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 08/25/21 18:39 87-68-32.0 1
2-Hexanone ND ug/L 08/25/21 18:39 591-78-65.0 1
Isopropylbenzene (Cumene)ND ug/L 08/25/21 18:39 98-82-81.0 1
p-Isopropyltoluene ND ug/L 08/25/21 18:39 99-87-61.0 1
Methylene Chloride ND ug/L 08/25/21 18:39 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/25/21 18:39 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 08/25/21 18:39 1634-04-41.0 1
Naphthalene 50.9 ug/L 08/25/21 18:39 91-20-31.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92557149
LOADING RACK
Sample: KMW-12 Lab ID: 92557149015 Collected: 08/22/21 14:09 Received: 08/24/21 10:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
n-Propylbenzene ND ug/L 08/25/21 18:39 103-65-11.0 1
Styrene ND ug/L 08/25/21 18:39 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 08/25/21 18:39 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 08/25/21 18:39 79-34-51.0 1
Tetrachloroethene ND ug/L 08/25/21 18:39 127-18-41.0 1
Toluene ND ug/L 08/25/21 18:39 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 08/25/21 18:39 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 08/25/21 18:39 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 08/25/21 18:39 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 08/25/21 18:39 79-00-51.0 1
Trichloroethene ND ug/L 08/25/21 18:39 79-01-61.0 1
Trichlorofluoromethane ND ug/L 08/25/21 18:39 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 08/25/21 18:39 96-18-41.0 1
1,2,4-Trimethylbenzene 2.4 ug/L 08/25/21 18:39 95-63-61.0 1
1,3,5-Trimethylbenzene 7.7 ug/L 08/25/21 18:39 108-67-81.0 1
Vinyl acetate ND ug/L 08/25/21 18:39 108-05-42.0 1
Vinyl chloride ND ug/L 08/25/21 18:39 75-01-41.0 1
Xylene (Total)11.7 ug/L 08/25/21 18:39 1330-20-71.0 1
m&p-Xylene 11.7 ug/L 08/25/21 18:39 179601-23-12.0 1
o-Xylene ND ug/L 08/25/21 18:39 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)98 %08/25/21 18:39 460-00-470-130 1
1,2-Dichloroethane-d4 (S)104 %08/25/21 18:39 17060-07-070-130 1
Toluene-d8 (S)102 %08/25/21 18:39 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92557149
LOADING RACK
Sample: KMW-13 Lab ID: 92557149016 Collected: 08/23/21 07:28 Received: 08/24/21 10:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 08/25/21 21:59 67-64-162.5 2.5
Benzene ND ug/L 08/25/21 21:59 71-43-22.5 2.5
Bromobenzene ND ug/L 08/25/21 21:59 108-86-12.5 2.5
Bromochloromethane ND ug/L 08/25/21 21:59 74-97-52.5 2.5
Bromodichloromethane ND ug/L 08/25/21 21:59 75-27-42.5 2.5
Bromoform ND ug/L 08/25/21 21:59 75-25-22.5 2.5
Bromomethane ND ug/L 08/25/21 21:59 74-83-95.0 2.5
2-Butanone (MEK)ND ug/L 08/25/21 21:59 78-93-312.5 2.5
n-Butylbenzene ND ug/L 08/25/21 21:59 104-51-82.5 2.5
sec-Butylbenzene 2.6 ug/L 08/25/21 21:59 135-98-82.5 2.5
Carbon tetrachloride ND ug/L 08/25/21 21:59 56-23-52.5 2.5
Chlorobenzene ND ug/L 08/25/21 21:59 108-90-72.5 2.5
Chloroethane ND ug/L 08/25/21 21:59 75-00-32.5 2.5
Chloroform ND ug/L 08/25/21 21:59 67-66-32.5 2.5
Chloromethane ND ug/L 08/25/21 21:59 74-87-32.5 2.5
2-Chlorotoluene ND ug/L 08/25/21 21:59 95-49-82.5 2.5
4-Chlorotoluene ND ug/L 08/25/21 21:59 106-43-42.5 2.5
1,2-Dibromo-3-chloropropane ND ug/L 08/25/21 21:59 96-12-85.0 2.5
Dibromochloromethane ND ug/L 08/25/21 21:59 124-48-12.5 2.5
1,2-Dibromoethane (EDB)ND ug/L 08/25/21 21:59 106-93-42.5 2.5
Dibromomethane ND ug/L 08/25/21 21:59 74-95-32.5 2.5
1,2-Dichlorobenzene ND ug/L 08/25/21 21:59 95-50-12.5 2.5
1,3-Dichlorobenzene ND ug/L 08/25/21 21:59 541-73-12.5 2.5
1,4-Dichlorobenzene ND ug/L 08/25/21 21:59 106-46-72.5 2.5
Dichlorodifluoromethane ND ug/L 08/25/21 21:59 75-71-82.5 2.5
1,1-Dichloroethane ND ug/L 08/25/21 21:59 75-34-32.5 2.5
1,2-Dichloroethane ND ug/L 08/25/21 21:59 107-06-22.5 2.5
1,1-Dichloroethene ND ug/L 08/25/21 21:59 75-35-42.5 2.5
cis-1,2-Dichloroethene ND ug/L 08/25/21 21:59 156-59-22.5 2.5
trans-1,2-Dichloroethene ND ug/L 08/25/21 21:59 156-60-52.5 2.5
1,2-Dichloropropane ND ug/L 08/25/21 21:59 78-87-52.5 2.5
1,3-Dichloropropane ND ug/L 08/25/21 21:59 142-28-92.5 2.5
2,2-Dichloropropane ND ug/L 08/25/21 21:59 594-20-72.5 2.5
1,1-Dichloropropene ND ug/L 08/25/21 21:59 563-58-62.5 2.5
cis-1,3-Dichloropropene ND ug/L 08/25/21 21:59 10061-01-52.5 2.5
trans-1,3-Dichloropropene ND ug/L 08/25/21 21:59 10061-02-62.5 2.5
Diisopropyl ether ND ug/L 08/25/21 21:59 108-20-32.5 2.5
Ethylbenzene 6.4 ug/L 08/25/21 21:59 100-41-42.5 2.5
Hexachloro-1,3-butadiene ND ug/L 08/25/21 21:59 87-68-35.0 2.5
2-Hexanone ND ug/L 08/25/21 21:59 591-78-612.5 2.5
Isopropylbenzene (Cumene)15.6 ug/L 08/25/21 21:59 98-82-82.5 2.5
p-Isopropyltoluene ND ug/L 08/25/21 21:59 99-87-62.5 2.5
Methylene Chloride 20.9 ug/L 08/25/21 21:59 75-09-2 C912.5 2.5
4-Methyl-2-pentanone (MIBK)ND ug/L 08/25/21 21:59 108-10-112.5 2.5
Methyl-tert-butyl ether ND ug/L 08/25/21 21:59 1634-04-42.5 2.5
Naphthalene 22.1 ug/L 08/25/21 21:59 91-20-32.5 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92557149
LOADING RACK
Sample: KMW-13 Lab ID: 92557149016 Collected: 08/23/21 07:28 Received: 08/24/21 10:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
n-Propylbenzene 22.8 ug/L 08/25/21 21:59 103-65-12.5 2.5
Styrene ND ug/L 08/25/21 21:59 100-42-52.5 2.5
1,1,1,2-Tetrachloroethane ND ug/L 08/25/21 21:59 630-20-62.5 2.5
1,1,2,2-Tetrachloroethane ND ug/L 08/25/21 21:59 79-34-52.5 2.5
Tetrachloroethene ND ug/L 08/25/21 21:59 127-18-42.5 2.5
Toluene ND ug/L 08/25/21 21:59 108-88-32.5 2.5
1,2,3-Trichlorobenzene ND ug/L 08/25/21 21:59 87-61-62.5 2.5
1,2,4-Trichlorobenzene ND ug/L 08/25/21 21:59 120-82-12.5 2.5
1,1,1-Trichloroethane ND ug/L 08/25/21 21:59 71-55-62.5 2.5
1,1,2-Trichloroethane ND ug/L 08/25/21 21:59 79-00-52.5 2.5
Trichloroethene ND ug/L 08/25/21 21:59 79-01-62.5 2.5
Trichlorofluoromethane ND ug/L 08/25/21 21:59 75-69-42.5 2.5
1,2,3-Trichloropropane ND ug/L 08/25/21 21:59 96-18-42.5 2.5
1,2,4-Trimethylbenzene 5.4 ug/L 08/25/21 21:59 95-63-62.5 2.5
1,3,5-Trimethylbenzene ND ug/L 08/25/21 21:59 108-67-82.5 2.5
Vinyl acetate ND ug/L 08/25/21 21:59 108-05-45.0 2.5
Vinyl chloride ND ug/L 08/25/21 21:59 75-01-42.5 2.5
Xylene (Total)704 ug/L 08/25/21 21:59 1330-20-72.5 2.5
m&p-Xylene 704 ug/L 08/25/21 21:59 179601-23-15.0 2.5
o-Xylene ND ug/L 08/25/21 21:59 95-47-62.5 2.5
Surrogates
4-Bromofluorobenzene (S)100 %08/25/21 21:59 460-00-470-130 2.5
1,2-Dichloroethane-d4 (S)109 %08/25/21 21:59 17060-07-070-130 2.5
Toluene-d8 (S)108 %08/25/21 21:59 2037-26-570-130 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92557149
LOADING RACK
Sample: KMW-14 Lab ID: 92557149017 Collected: 08/22/21 13:35 Received: 08/24/21 10:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 08/25/21 18:57 67-64-125.0 1
Benzene ND ug/L 08/25/21 18:57 71-43-21.0 1
Bromobenzene ND ug/L 08/25/21 18:57 108-86-11.0 1
Bromochloromethane ND ug/L 08/25/21 18:57 74-97-51.0 1
Bromodichloromethane ND ug/L 08/25/21 18:57 75-27-41.0 1
Bromoform ND ug/L 08/25/21 18:57 75-25-21.0 1
Bromomethane ND ug/L 08/25/21 18:57 74-83-92.0 1
2-Butanone (MEK)ND ug/L 08/25/21 18:57 78-93-35.0 1
n-Butylbenzene ND ug/L 08/25/21 18:57 104-51-81.0 1
sec-Butylbenzene ND ug/L 08/25/21 18:57 135-98-81.0 1
Carbon tetrachloride ND ug/L 08/25/21 18:57 56-23-51.0 1
Chlorobenzene ND ug/L 08/25/21 18:57 108-90-71.0 1
Chloroethane ND ug/L 08/25/21 18:57 75-00-31.0 1
Chloroform ND ug/L 08/25/21 18:57 67-66-31.0 1
Chloromethane ND ug/L 08/25/21 18:57 74-87-31.0 1
2-Chlorotoluene ND ug/L 08/25/21 18:57 95-49-81.0 1
4-Chlorotoluene ND ug/L 08/25/21 18:57 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 08/25/21 18:57 96-12-82.0 1
Dibromochloromethane ND ug/L 08/25/21 18:57 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 08/25/21 18:57 106-93-41.0 1
Dibromomethane ND ug/L 08/25/21 18:57 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 08/25/21 18:57 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 08/25/21 18:57 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 08/25/21 18:57 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 08/25/21 18:57 75-71-81.0 1
1,1-Dichloroethane ND ug/L 08/25/21 18:57 75-34-31.0 1
1,2-Dichloroethane ND ug/L 08/25/21 18:57 107-06-21.0 1
1,1-Dichloroethene ND ug/L 08/25/21 18:57 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 08/25/21 18:57 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 08/25/21 18:57 156-60-51.0 1
1,2-Dichloropropane ND ug/L 08/25/21 18:57 78-87-51.0 1
1,3-Dichloropropane ND ug/L 08/25/21 18:57 142-28-91.0 1
2,2-Dichloropropane ND ug/L 08/25/21 18:57 594-20-71.0 1
1,1-Dichloropropene ND ug/L 08/25/21 18:57 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 08/25/21 18:57 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 08/25/21 18:57 10061-02-61.0 1
Diisopropyl ether ND ug/L 08/25/21 18:57 108-20-31.0 1
Ethylbenzene ND ug/L 08/25/21 18:57 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 08/25/21 18:57 87-68-32.0 1
2-Hexanone ND ug/L 08/25/21 18:57 591-78-65.0 1
Isopropylbenzene (Cumene)ND ug/L 08/25/21 18:57 98-82-81.0 1
p-Isopropyltoluene ND ug/L 08/25/21 18:57 99-87-61.0 1
Methylene Chloride ND ug/L 08/25/21 18:57 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/25/21 18:57 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 08/25/21 18:57 1634-04-41.0 1
Naphthalene ND ug/L 08/25/21 18:57 91-20-31.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92557149
LOADING RACK
Sample: KMW-14 Lab ID: 92557149017 Collected: 08/22/21 13:35 Received: 08/24/21 10:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
n-Propylbenzene ND ug/L 08/25/21 18:57 103-65-11.0 1
Styrene ND ug/L 08/25/21 18:57 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 08/25/21 18:57 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 08/25/21 18:57 79-34-51.0 1
Tetrachloroethene ND ug/L 08/25/21 18:57 127-18-41.0 1
Toluene ND ug/L 08/25/21 18:57 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 08/25/21 18:57 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 08/25/21 18:57 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 08/25/21 18:57 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 08/25/21 18:57 79-00-51.0 1
Trichloroethene ND ug/L 08/25/21 18:57 79-01-61.0 1
Trichlorofluoromethane ND ug/L 08/25/21 18:57 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 08/25/21 18:57 96-18-41.0 1
1,2,4-Trimethylbenzene ND ug/L 08/25/21 18:57 95-63-61.0 1
1,3,5-Trimethylbenzene ND ug/L 08/25/21 18:57 108-67-81.0 1
Vinyl acetate ND ug/L 08/25/21 18:57 108-05-42.0 1
Vinyl chloride ND ug/L 08/25/21 18:57 75-01-41.0 1
Xylene (Total)ND ug/L 08/25/21 18:57 1330-20-71.0 1
m&p-Xylene ND ug/L 08/25/21 18:57 179601-23-12.0 1
o-Xylene ND ug/L 08/25/21 18:57 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)98 %08/25/21 18:57 460-00-470-130 1
1,2-Dichloroethane-d4 (S)107 %08/25/21 18:57 17060-07-070-130 1
Toluene-d8 (S)101 %08/25/21 18:57 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92557149
LOADING RACK
Sample: KMW-18 Lab ID: 92557149018 Collected: 08/21/21 11:49 Received: 08/24/21 10:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 08/25/21 19:15 67-64-125.0 1
Benzene ND ug/L 08/25/21 19:15 71-43-21.0 1
Bromobenzene ND ug/L 08/25/21 19:15 108-86-11.0 1
Bromochloromethane ND ug/L 08/25/21 19:15 74-97-51.0 1
Bromodichloromethane ND ug/L 08/25/21 19:15 75-27-41.0 1
Bromoform ND ug/L 08/25/21 19:15 75-25-21.0 1
Bromomethane ND ug/L 08/25/21 19:15 74-83-92.0 1
2-Butanone (MEK)ND ug/L 08/25/21 19:15 78-93-35.0 1
n-Butylbenzene ND ug/L 08/25/21 19:15 104-51-81.0 1
sec-Butylbenzene ND ug/L 08/25/21 19:15 135-98-81.0 1
Carbon tetrachloride ND ug/L 08/25/21 19:15 56-23-51.0 1
Chlorobenzene ND ug/L 08/25/21 19:15 108-90-71.0 1
Chloroethane ND ug/L 08/25/21 19:15 75-00-31.0 1
Chloroform ND ug/L 08/25/21 19:15 67-66-31.0 1
Chloromethane ND ug/L 08/25/21 19:15 74-87-31.0 1
2-Chlorotoluene ND ug/L 08/25/21 19:15 95-49-81.0 1
4-Chlorotoluene ND ug/L 08/25/21 19:15 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 08/25/21 19:15 96-12-82.0 1
Dibromochloromethane ND ug/L 08/25/21 19:15 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 08/25/21 19:15 106-93-41.0 1
Dibromomethane ND ug/L 08/25/21 19:15 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 08/25/21 19:15 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 08/25/21 19:15 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 08/25/21 19:15 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 08/25/21 19:15 75-71-81.0 1
1,1-Dichloroethane ND ug/L 08/25/21 19:15 75-34-31.0 1
1,2-Dichloroethane ND ug/L 08/25/21 19:15 107-06-21.0 1
1,1-Dichloroethene ND ug/L 08/25/21 19:15 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 08/25/21 19:15 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 08/25/21 19:15 156-60-51.0 1
1,2-Dichloropropane ND ug/L 08/25/21 19:15 78-87-51.0 1
1,3-Dichloropropane ND ug/L 08/25/21 19:15 142-28-91.0 1
2,2-Dichloropropane ND ug/L 08/25/21 19:15 594-20-71.0 1
1,1-Dichloropropene ND ug/L 08/25/21 19:15 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 08/25/21 19:15 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 08/25/21 19:15 10061-02-61.0 1
Diisopropyl ether ND ug/L 08/25/21 19:15 108-20-31.0 1
Ethylbenzene ND ug/L 08/25/21 19:15 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 08/25/21 19:15 87-68-32.0 1
2-Hexanone ND ug/L 08/25/21 19:15 591-78-65.0 1
Isopropylbenzene (Cumene)ND ug/L 08/25/21 19:15 98-82-81.0 1
p-Isopropyltoluene ND ug/L 08/25/21 19:15 99-87-61.0 1
Methylene Chloride ND ug/L 08/25/21 19:15 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/25/21 19:15 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 08/25/21 19:15 1634-04-41.0 1
Naphthalene ND ug/L 08/25/21 19:15 91-20-31.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92557149
LOADING RACK
Sample: KMW-18 Lab ID: 92557149018 Collected: 08/21/21 11:49 Received: 08/24/21 10:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
n-Propylbenzene ND ug/L 08/25/21 19:15 103-65-11.0 1
Styrene ND ug/L 08/25/21 19:15 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 08/25/21 19:15 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 08/25/21 19:15 79-34-51.0 1
Tetrachloroethene ND ug/L 08/25/21 19:15 127-18-41.0 1
Toluene ND ug/L 08/25/21 19:15 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 08/25/21 19:15 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 08/25/21 19:15 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 08/25/21 19:15 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 08/25/21 19:15 79-00-51.0 1
Trichloroethene ND ug/L 08/25/21 19:15 79-01-61.0 1
Trichlorofluoromethane ND ug/L 08/25/21 19:15 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 08/25/21 19:15 96-18-41.0 1
1,2,4-Trimethylbenzene ND ug/L 08/25/21 19:15 95-63-61.0 1
1,3,5-Trimethylbenzene ND ug/L 08/25/21 19:15 108-67-81.0 1
Vinyl acetate ND ug/L 08/25/21 19:15 108-05-42.0 1
Vinyl chloride ND ug/L 08/25/21 19:15 75-01-41.0 1
Xylene (Total)ND ug/L 08/25/21 19:15 1330-20-71.0 1
m&p-Xylene ND ug/L 08/25/21 19:15 179601-23-12.0 1
o-Xylene ND ug/L 08/25/21 19:15 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)98 %08/25/21 19:15 460-00-470-130 1
1,2-Dichloroethane-d4 (S)106 %08/25/21 19:15 17060-07-070-130 1
Toluene-d8 (S)101 %08/25/21 19:15 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92557149
LOADING RACK
Sample: TRIP BLANK Lab ID: 92557149019 Collected: 08/21/21 00:00 Received: 08/24/21 10:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 08/24/21 16:27 67-64-125.0 1
Benzene ND ug/L 08/24/21 16:27 71-43-21.0 1
Bromobenzene ND ug/L 08/24/21 16:27 108-86-11.0 1
Bromochloromethane ND ug/L 08/24/21 16:27 74-97-51.0 1
Bromodichloromethane ND ug/L 08/24/21 16:27 75-27-41.0 1
Bromoform ND ug/L 08/24/21 16:27 75-25-21.0 1
Bromomethane ND ug/L 08/24/21 16:27 74-83-92.0 1
2-Butanone (MEK)ND ug/L 08/24/21 16:27 78-93-35.0 1
n-Butylbenzene ND ug/L 08/24/21 16:27 104-51-81.0 1
sec-Butylbenzene ND ug/L 08/24/21 16:27 135-98-81.0 1
Carbon tetrachloride ND ug/L 08/24/21 16:27 56-23-51.0 1
Chlorobenzene ND ug/L 08/24/21 16:27 108-90-71.0 1
Chloroethane ND ug/L 08/24/21 16:27 75-00-31.0 1
Chloroform ND ug/L 08/24/21 16:27 67-66-31.0 1
Chloromethane ND ug/L 08/24/21 16:27 74-87-31.0 1
2-Chlorotoluene ND ug/L 08/24/21 16:27 95-49-81.0 1
4-Chlorotoluene ND ug/L 08/24/21 16:27 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 08/24/21 16:27 96-12-82.0 1
Dibromochloromethane ND ug/L 08/24/21 16:27 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 08/24/21 16:27 106-93-41.0 1
Dibromomethane ND ug/L 08/24/21 16:27 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 08/24/21 16:27 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 08/24/21 16:27 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 08/24/21 16:27 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 08/24/21 16:27 75-71-81.0 1
1,1-Dichloroethane ND ug/L 08/24/21 16:27 75-34-31.0 1
1,2-Dichloroethane ND ug/L 08/24/21 16:27 107-06-21.0 1
1,1-Dichloroethene ND ug/L 08/24/21 16:27 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 08/24/21 16:27 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 08/24/21 16:27 156-60-51.0 1
1,2-Dichloropropane ND ug/L 08/24/21 16:27 78-87-51.0 1
1,3-Dichloropropane ND ug/L 08/24/21 16:27 142-28-91.0 1
2,2-Dichloropropane ND ug/L 08/24/21 16:27 594-20-71.0 1
1,1-Dichloropropene ND ug/L 08/24/21 16:27 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 08/24/21 16:27 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 08/24/21 16:27 10061-02-61.0 1
Diisopropyl ether ND ug/L 08/24/21 16:27 108-20-31.0 1
Ethylbenzene ND ug/L 08/24/21 16:27 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 08/24/21 16:27 87-68-32.0 1
2-Hexanone ND ug/L 08/24/21 16:27 591-78-65.0 1
Isopropylbenzene (Cumene)ND ug/L 08/24/21 16:27 98-82-81.0 1
p-Isopropyltoluene ND ug/L 08/24/21 16:27 99-87-61.0 1
Methylene Chloride ND ug/L 08/24/21 16:27 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/24/21 16:27 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 08/24/21 16:27 1634-04-41.0 1
Naphthalene ND ug/L 08/24/21 16:27 91-20-31.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92557149
LOADING RACK
Sample: TRIP BLANK Lab ID: 92557149019 Collected: 08/21/21 00:00 Received: 08/24/21 10:05 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
n-Propylbenzene ND ug/L 08/24/21 16:27 103-65-11.0 1
Styrene ND ug/L 08/24/21 16:27 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 08/24/21 16:27 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 08/24/21 16:27 79-34-51.0 1
Tetrachloroethene ND ug/L 08/24/21 16:27 127-18-41.0 1
Toluene ND ug/L 08/24/21 16:27 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 08/24/21 16:27 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 08/24/21 16:27 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 08/24/21 16:27 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 08/24/21 16:27 79-00-51.0 1
Trichloroethene ND ug/L 08/24/21 16:27 79-01-61.0 1
Trichlorofluoromethane ND ug/L 08/24/21 16:27 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 08/24/21 16:27 96-18-41.0 1
1,2,4-Trimethylbenzene ND ug/L 08/24/21 16:27 95-63-61.0 1
1,3,5-Trimethylbenzene ND ug/L 08/24/21 16:27 108-67-81.0 1
Vinyl acetate ND ug/L 08/24/21 16:27 108-05-42.0 1
Vinyl chloride ND ug/L 08/24/21 16:27 75-01-41.0 1
Xylene (Total)ND ug/L 08/24/21 16:27 1330-20-71.0 1
m&p-Xylene ND ug/L 08/24/21 16:27 179601-23-12.0 1
o-Xylene ND ug/L 08/24/21 16:27 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)97 %08/24/21 16:27 460-00-470-130 1
1,2-Dichloroethane-d4 (S)95 %08/24/21 16:27 17060-07-070-130 1
Toluene-d8 (S)98 %08/24/21 16:27 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92557149
LOADING RACK
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
642586
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92557149007, 92557149008, 92557149010, 92557149014, 92557149019
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3372320
Associated Lab Samples:92557149007, 92557149008, 92557149010, 92557149014, 92557149019
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 08/24/21 15:51
1,1,1-Trichloroethane ug/L ND 1.0 08/24/21 15:51
1,1,2,2-Tetrachloroethane ug/L ND 1.0 08/24/21 15:51
1,1,2-Trichloroethane ug/L ND 1.0 08/24/21 15:51
1,1-Dichloroethane ug/L ND 1.0 08/24/21 15:51
1,1-Dichloroethene ug/L ND 1.0 08/24/21 15:51
1,1-Dichloropropene ug/L ND 1.0 08/24/21 15:51
1,2,3-Trichlorobenzene ug/L ND 1.0 08/24/21 15:51
1,2,3-Trichloropropane ug/L ND 1.0 08/24/21 15:51
1,2,4-Trichlorobenzene ug/L ND 1.0 08/24/21 15:51
1,2,4-Trimethylbenzene ug/L ND 1.0 08/24/21 15:51
1,2-Dibromo-3-chloropropane ug/L ND 2.0 08/24/21 15:51
1,2-Dibromoethane (EDB)ug/L ND 1.0 08/24/21 15:51
1,2-Dichlorobenzene ug/L ND 1.0 08/24/21 15:51
1,2-Dichloroethane ug/L ND 1.0 08/24/21 15:51
1,2-Dichloropropane ug/L ND 1.0 08/24/21 15:51
1,3,5-Trimethylbenzene ug/L ND 1.0 08/24/21 15:51
1,3-Dichlorobenzene ug/L ND 1.0 08/24/21 15:51
1,3-Dichloropropane ug/L ND 1.0 08/24/21 15:51
1,4-Dichlorobenzene ug/L ND 1.0 08/24/21 15:51
2,2-Dichloropropane ug/L ND 1.0 08/24/21 15:51
2-Butanone (MEK)ug/L ND 5.0 08/24/21 15:51
2-Chlorotoluene ug/L ND 1.0 08/24/21 15:51
2-Hexanone ug/L ND 5.0 08/24/21 15:51
4-Chlorotoluene ug/L ND 1.0 08/24/21 15:51
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 08/24/21 15:51
Acetone ug/L ND 25.0 08/24/21 15:51
Benzene ug/L ND 1.0 08/24/21 15:51
Bromobenzene ug/L ND 1.0 08/24/21 15:51
Bromochloromethane ug/L ND 1.0 08/24/21 15:51
Bromodichloromethane ug/L ND 1.0 08/24/21 15:51
Bromoform ug/L ND 1.0 08/24/21 15:51
Bromomethane ug/L ND 2.0 08/24/21 15:51
Carbon tetrachloride ug/L ND 1.0 08/24/21 15:51
Chlorobenzene ug/L ND 1.0 08/24/21 15:51
Chloroethane ug/L ND 1.0 08/24/21 15:51
Chloroform ug/L ND 1.0 08/24/21 15:51
Chloromethane ug/L ND 1.0 08/24/21 15:51
cis-1,2-Dichloroethene ug/L ND 1.0 08/24/21 15:51
cis-1,3-Dichloropropene ug/L ND 1.0 08/24/21 15:51
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92557149
LOADING RACK
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3372320
Associated Lab Samples:92557149007, 92557149008, 92557149010, 92557149014, 92557149019
Matrix: Water
Analyzed
Dibromochloromethane ug/L ND 1.0 08/24/21 15:51
Dibromomethane ug/L ND 1.0 08/24/21 15:51
Dichlorodifluoromethane ug/L ND 1.0 08/24/21 15:51
Diisopropyl ether ug/L ND 1.0 08/24/21 15:51
Ethylbenzene ug/L ND 1.0 08/24/21 15:51
Hexachloro-1,3-butadiene ug/L ND 2.0 08/24/21 15:51
Isopropylbenzene (Cumene)ug/L ND 1.0 08/24/21 15:51
m&p-Xylene ug/L ND 2.0 08/24/21 15:51
Methyl-tert-butyl ether ug/L ND 1.0 08/24/21 15:51
Methylene Chloride ug/L ND 5.0 08/24/21 15:51
n-Butylbenzene ug/L ND 1.0 08/24/21 15:51
n-Propylbenzene ug/L ND 1.0 08/24/21 15:51
Naphthalene ug/L ND 1.0 08/24/21 15:51
o-Xylene ug/L ND 1.0 08/24/21 15:51
p-Isopropyltoluene ug/L ND 1.0 08/24/21 15:51
sec-Butylbenzene ug/L ND 1.0 08/24/21 15:51
Styrene ug/L ND 1.0 08/24/21 15:51
Tetrachloroethene ug/L ND 1.0 08/24/21 15:51
Toluene ug/L ND 1.0 08/24/21 15:51
trans-1,2-Dichloroethene ug/L ND 1.0 08/24/21 15:51
trans-1,3-Dichloropropene ug/L ND 1.0 08/24/21 15:51
Trichloroethene ug/L ND 1.0 08/24/21 15:51
Trichlorofluoromethane ug/L ND 1.0 08/24/21 15:51
Vinyl acetate ug/L ND 2.0 08/24/21 15:51
Vinyl chloride ug/L ND 1.0 08/24/21 15:51
Xylene (Total)ug/L ND 1.0 08/24/21 15:51
1,2-Dichloroethane-d4 (S)%96 70-130 08/24/21 15:51
4-Bromofluorobenzene (S)%97 70-130 08/24/21 15:51
Toluene-d8 (S)%99 70-130 08/24/21 15:51
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3372321LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 53.550 107 70-130
1,1,1-Trichloroethane ug/L 50.350 101 70-130
1,1,2,2-Tetrachloroethane ug/L 54.350 109 70-130
1,1,2-Trichloroethane ug/L 52.850 106 70-130
1,1-Dichloroethane ug/L 55.550 111 70-130
1,1-Dichloroethene ug/L 54.950 110 70-132
1,1-Dichloropropene ug/L 52.050 104 70-131
1,2,3-Trichlorobenzene ug/L 57.050 114 70-134
1,2,3-Trichloropropane ug/L 53.050 106 70-130
1,2,4-Trichlorobenzene ug/L 56.350 113 70-130
1,2,4-Trimethylbenzene ug/L 55.350 111 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92557149
LOADING RACK
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3372321LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/L 60.750 121 70-132
1,2-Dibromoethane (EDB)ug/L 54.850 110 70-130
1,2-Dichlorobenzene ug/L 54.550 109 70-130
1,2-Dichloroethane ug/L 49.350 99 70-130
1,2-Dichloropropane ug/L 56.850 114 70-130
1,3,5-Trimethylbenzene ug/L 55.050 110 70-130
1,3-Dichlorobenzene ug/L 54.950 110 70-130
1,3-Dichloropropane ug/L 52.050 104 70-130
1,4-Dichlorobenzene ug/L 55.350 111 70-130
2,2-Dichloropropane ug/L 53.450 107 70-130
2-Butanone (MEK)ug/L 108100 108 70-133
2-Chlorotoluene ug/L 55.750 111 70-130
2-Hexanone ug/L 121100 121 70-130
4-Chlorotoluene ug/L 52.450 105 70-130
4-Methyl-2-pentanone (MIBK)ug/L 115100 115 70-130
Acetone ug/L 112100 112 70-144
Benzene ug/L 53.650 107 70-130
Bromobenzene ug/L 56.150 112 70-130
Bromochloromethane ug/L 52.850 106 70-130
Bromodichloromethane ug/L 52.350 105 70-130
Bromoform ug/L 54.850 110 70-131
Bromomethane ug/L 47.550 95 30-177
Carbon tetrachloride ug/L 51.450 103 70-130
Chlorobenzene ug/L 53.350 107 70-130
Chloroethane ug/L 44.750 89 46-131
Chloroform ug/L 50.250 100 70-130
Chloromethane ug/L 54.150 108 49-130
cis-1,2-Dichloroethene ug/L 54.250 108 70-130
cis-1,3-Dichloropropene ug/L 54.950 110 70-130
Dibromochloromethane ug/L 55.650 111 70-130
Dibromomethane ug/L 54.250 108 70-130
Dichlorodifluoromethane ug/L 46.950 94 52-134
Diisopropyl ether ug/L 55.050 110 70-131
Ethylbenzene ug/L 53.150 106 70-130
Hexachloro-1,3-butadiene ug/L 55.750 111 70-131
Isopropylbenzene (Cumene)ug/L 55.650 111 70-130
m&p-Xylene ug/L 105100 105 70-130
Methyl-tert-butyl ether ug/L 50.950 102 70-130
Methylene Chloride ug/L 54.550 109 68-130
n-Butylbenzene ug/L 56.050 112 70-130
n-Propylbenzene ug/L 54.650 109 70-130
Naphthalene ug/L 57.150 114 70-133
o-Xylene ug/L 54.050 108 70-130
p-Isopropyltoluene ug/L 55.850 112 70-130
sec-Butylbenzene ug/L 53.750 107 70-130
Styrene ug/L 56.250 112 70-130
Tetrachloroethene ug/L 53.350 107 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92557149
LOADING RACK
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3372321LABORATORY CONTROL SAMPLE:
LCSSpike
Toluene ug/L 53.050 106 70-130
trans-1,2-Dichloroethene ug/L 55.450 111 70-130
trans-1,3-Dichloropropene ug/L 53.050 106 70-130
Trichloroethene ug/L 52.450 105 70-130
Trichlorofluoromethane ug/L 44.550 89 61-130
Vinyl acetate ug/L 115100 115 70-140
Vinyl chloride ug/L 56.650 113 59-142
Xylene (Total)ug/L 159150 106 70-130
1,2-Dichloroethane-d4 (S)%88 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3372322MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92557149008
3372323
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 104 70-135105 120ND20.8 21.0
1,1,1-Trichloroethane ug/L 20 102 70-148100 220ND20.5 20.0
1,1,2,2-Tetrachloroethane ug/L 20 105 70-131104 020ND20.9 20.9
1,1,2-Trichloroethane ug/L 20 102 70-136100 220ND20.5 20.1
1,1-Dichloroethane ug/L 20 112 70-147111 020ND22.3 22.3
1,1-Dichloroethene ug/L 20 109 70-158110 120ND21.8 22.0
1,1-Dichloropropene ug/L 20 105 70-149103 220ND20.9 20.6
1,2,3-Trichlorobenzene ug/L 20 109 68-140108 120ND21.9 21.6
1,2,3-Trichloropropane ug/L 20 100 67-13798 220ND19.9 19.6
1,2,4-Trichlorobenzene ug/L 20 107 70-139106 120ND21.3 21.2
1,2,4-Trimethylbenzene ug/L 20 108 70-134106 220ND21.6 21.2
1,2-Dibromo-3-chloropropane ug/L 20 115 69-136113 220ND23.0 22.6
1,2-Dibromoethane (EDB)ug/L 20 105 70-137106 120ND20.9 21.2
1,2-Dichlorobenzene ug/L 20 106 70-133104 320ND21.3 20.8
1,2-Dichloroethane ug/L 20 97 67-13894 220ND19.3 18.9
1,2-Dichloropropane ug/L 20 110 70-138108 220ND22.1 21.7
1,3,5-Trimethylbenzene ug/L 20 110 70-138106 420ND22.0 21.3
1,3-Dichlorobenzene ug/L 20 107 70-133104 320ND21.4 20.8
1,3-Dichloropropane ug/L 20 103 70-136103 020ND20.7 20.6
1,4-Dichlorobenzene ug/L 20 107 70-133105 220ND21.4 21.0
2,2-Dichloropropane ug/L 20 87 52-15585 220ND17.3 17.0
2-Butanone (MEK)ug/L 40 108 61-147104 440ND43.0 41.5
2-Chlorotoluene ug/L 20 109 70-141106 220ND21.7 21.3
2-Hexanone ug/L 40 111 67-139107 440ND44.6 42.8
4-Chlorotoluene ug/L 20 104 70-135100 420ND20.8 20.1
4-Methyl-2-pentanone (MIBK) ug/L 40 103 67-136101 240ND41.2 40.5
Acetone ug/L 40 112 55-159110 240ND44.9 43.9
Benzene ug/L 20 106 67-150105 120ND21.2 21.0
Bromobenzene ug/L 20 111 70-134107 320ND22.1 21.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92557149
LOADING RACK
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3372322MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92557149008
3372323
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Bromochloromethane ug/L 20 112 70-146113 120ND22.5 22.7
Bromodichloromethane ug/L 20 101 70-13897 420ND20.2 19.5
Bromoform ug/L 20 102 57-138105 220ND20.5 20.9
Bromomethane ug/L v22010010-200103 320ND20.0 20.6
Carbon tetrachloride ug/L 20 104 70-147103 120ND20.7 20.5
Chlorobenzene ug/L 20 108 70-137106 220ND21.6 21.1
Chloroethane ug/L 20 107 51-166107 120ND21.5 21.3
Chloroform ug/L 20 101 70-14499 220ND20.2 19.7
Chloromethane ug/L 20 101 24-161109 820ND20.1 21.7
cis-1,2-Dichloroethene ug/L 20 107 67-148106 120ND21.4 21.2
cis-1,3-Dichloropropene ug/L 20 98 70-14297 120ND19.6 19.4
Dibromochloromethane ug/L 20 108 68-138106 120ND21.6 21.3
Dibromomethane ug/L 20 104 70-134102 220ND20.9 20.4
Dichlorodifluoromethane ug/L 20 95 43-15595 020ND19.0 18.9
Diisopropyl ether ug/L 20 106 65-146105 020ND21.2 21.1
Ethylbenzene ug/L 20 106 68-143106 020ND21.2 21.2
Hexachloro-1,3-butadiene ug/L 20 103 62-151104 020ND20.6 20.7
m&p-Xylene ug/L 40 106 53-157106 140ND42.5 42.2
Methyl-tert-butyl ether ug/L 20 99 59-15697 220ND19.9 19.4
Methylene Chloride ug/L 20 104 64-148102 220ND20.9 20.5
n-Butylbenzene ug/L 20 103 70-139103 020ND20.6 20.7
n-Propylbenzene ug/L 20 105 70-138103 220ND21.1 20.6
Naphthalene ug/L 20 125 57-150126 120ND25.1 25.3
o-Xylene ug/L 20 110 68-143108 220ND21.9 21.6
p-Isopropyltoluene ug/L 20 106 70-141105 120ND21.2 21.0
sec-Butylbenzene ug/L 20 107 70-137104 320ND21.4 20.8
Styrene ug/L 20 109 70-136108 120ND21.8 21.6
Tetrachloroethene ug/L 20 107 70-139106 120ND21.4 21.2
Toluene ug/L 20 104 47-157103 120ND20.9 20.6
trans-1,2-Dichloroethene ug/L 20 110 70-149110 020ND22.1 22.0
trans-1,3-Dichloropropene ug/L 20 95 70-13895 020ND19.0 19.0
Trichloroethene ug/L 20 104 70-149103 120ND20.8 20.6
Trichlorofluoromethane ug/L 20 94 61-15492 120ND18.8 18.5
Vinyl acetate ug/L 40 91 48-15687 540ND36.3 34.7
Vinyl chloride ug/L 20 113 55-172115 120ND22.7 22.9
Xylene (Total)ug/L 60 107 66-145106 160ND64.5 63.8
1,2-Dichloroethane-d4 (S)%92 70-13093
4-Bromofluorobenzene (S)%97 70-13099
Toluene-d8 (S)%98 70-13097
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92557149
LOADING RACK
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
642588
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92557149003, 92557149005, 92557149006, 92557149009, 92557149011, 92557149012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3372331
Associated Lab Samples:92557149003, 92557149005, 92557149006, 92557149009, 92557149011, 92557149012
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 08/25/21 10:44
1,1,1-Trichloroethane ug/L ND 1.0 08/25/21 10:44
1,1,2,2-Tetrachloroethane ug/L ND 1.0 08/25/21 10:44
1,1,2-Trichloroethane ug/L ND 1.0 08/25/21 10:44
1,1-Dichloroethane ug/L ND 1.0 08/25/21 10:44
1,1-Dichloroethene ug/L ND 1.0 08/25/21 10:44
1,1-Dichloropropene ug/L ND 1.0 08/25/21 10:44
1,2,3-Trichlorobenzene ug/L ND 1.0 08/25/21 10:44
1,2,3-Trichloropropane ug/L ND 1.0 08/25/21 10:44
1,2,4-Trichlorobenzene ug/L ND 1.0 08/25/21 10:44
1,2,4-Trimethylbenzene ug/L ND 1.0 08/25/21 10:44
1,2-Dibromo-3-chloropropane ug/L ND 2.0 08/25/21 10:44
1,2-Dibromoethane (EDB)ug/L ND 1.0 08/25/21 10:44
1,2-Dichlorobenzene ug/L ND 1.0 08/25/21 10:44
1,2-Dichloroethane ug/L ND 1.0 08/25/21 10:44
1,2-Dichloropropane ug/L ND 1.0 08/25/21 10:44
1,3,5-Trimethylbenzene ug/L ND 1.0 08/25/21 10:44
1,3-Dichlorobenzene ug/L ND 1.0 08/25/21 10:44
1,3-Dichloropropane ug/L ND 1.0 08/25/21 10:44
1,4-Dichlorobenzene ug/L ND 1.0 08/25/21 10:44
2,2-Dichloropropane ug/L ND 1.0 08/25/21 10:44
2-Butanone (MEK)ug/L ND 5.0 08/25/21 10:44
2-Chlorotoluene ug/L ND 1.0 08/25/21 10:44
2-Hexanone ug/L ND 5.0 08/25/21 10:44
4-Chlorotoluene ug/L ND 1.0 08/25/21 10:44
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 08/25/21 10:44
Acetone ug/L ND 25.0 08/25/21 10:44
Benzene ug/L ND 1.0 08/25/21 10:44
Bromobenzene ug/L ND 1.0 08/25/21 10:44
Bromochloromethane ug/L ND 1.0 08/25/21 10:44
Bromodichloromethane ug/L ND 1.0 08/25/21 10:44
Bromoform ug/L ND 1.0 08/25/21 10:44
Bromomethane ug/L ND 2.0 08/25/21 10:44
Carbon tetrachloride ug/L ND 1.0 08/25/21 10:44
Chlorobenzene ug/L ND 1.0 08/25/21 10:44
Chloroethane ug/L ND 1.0 IL08/25/21 10:44
Chloroform ug/L ND 1.0 08/25/21 10:44
Chloromethane ug/L ND 1.0 08/25/21 10:44
cis-1,2-Dichloroethene ug/L ND 1.0 08/25/21 10:44
cis-1,3-Dichloropropene ug/L ND 1.0 08/25/21 10:44
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92557149
LOADING RACK
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3372331
Associated Lab Samples:92557149003, 92557149005, 92557149006, 92557149009, 92557149011, 92557149012
Matrix: Water
Analyzed
Dibromochloromethane ug/L ND 1.0 08/25/21 10:44
Dibromomethane ug/L ND 1.0 08/25/21 10:44
Dichlorodifluoromethane ug/L ND 1.0 08/25/21 10:44
Diisopropyl ether ug/L ND 1.0 08/25/21 10:44
Ethylbenzene ug/L ND 1.0 08/25/21 10:44
Hexachloro-1,3-butadiene ug/L ND 2.0 08/25/21 10:44
Isopropylbenzene (Cumene)ug/L ND 1.0 08/25/21 10:44
m&p-Xylene ug/L ND 2.0 08/25/21 10:44
Methyl-tert-butyl ether ug/L ND 1.0 08/25/21 10:44
Methylene Chloride ug/L ND 5.0 08/25/21 10:44
n-Butylbenzene ug/L ND 1.0 08/25/21 10:44
n-Propylbenzene ug/L ND 1.0 08/25/21 10:44
Naphthalene ug/L ND 1.0 08/25/21 10:44
o-Xylene ug/L ND 1.0 08/25/21 10:44
p-Isopropyltoluene ug/L ND 1.0 08/25/21 10:44
sec-Butylbenzene ug/L ND 1.0 08/25/21 10:44
Styrene ug/L ND 1.0 08/25/21 10:44
Tetrachloroethene ug/L ND 1.0 08/25/21 10:44
Toluene ug/L ND 1.0 08/25/21 10:44
trans-1,2-Dichloroethene ug/L ND 1.0 08/25/21 10:44
trans-1,3-Dichloropropene ug/L ND 1.0 08/25/21 10:44
Trichloroethene ug/L ND 1.0 08/25/21 10:44
Trichlorofluoromethane ug/L ND 1.0 08/25/21 10:44
Vinyl acetate ug/L ND 2.0 v108/25/21 10:44
Vinyl chloride ug/L ND 1.0 08/25/21 10:44
Xylene (Total)ug/L ND 1.0 08/25/21 10:44
1,2-Dichloroethane-d4 (S)%100 70-130 08/25/21 10:44
4-Bromofluorobenzene (S)%102 70-130 08/25/21 10:44
Toluene-d8 (S)%104 70-130 08/25/21 10:44
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3372332LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 46.450 93 70-130
1,1,1-Trichloroethane ug/L 52.750 105 70-130
1,1,2,2-Tetrachloroethane ug/L 45.750 91 70-130
1,1,2-Trichloroethane ug/L 50.850 102 70-130
1,1-Dichloroethane ug/L 54.650 109 70-130
1,1-Dichloroethene ug/L 54.050 108 70-132
1,1-Dichloropropene ug/L 49.850 100 70-131
1,2,3-Trichlorobenzene ug/L 48.150 96 70-134
1,2,3-Trichloropropane ug/L 44.950 90 70-130
1,2,4-Trichlorobenzene ug/L 49.050 98 70-130
1,2,4-Trimethylbenzene ug/L 45.050 90 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92557149
LOADING RACK
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3372332LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/L 44.450 89 70-132
1,2-Dibromoethane (EDB)ug/L 47.250 94 70-130
1,2-Dichlorobenzene ug/L 45.250 90 70-130
1,2-Dichloroethane ug/L 50.350 101 70-130
1,2-Dichloropropane ug/L 50.550 101 70-130
1,3,5-Trimethylbenzene ug/L 46.050 92 70-130
1,3-Dichlorobenzene ug/L 44.250 88 70-130
1,3-Dichloropropane ug/L 47.250 94 70-130
1,4-Dichlorobenzene ug/L 45.550 91 70-130
2,2-Dichloropropane ug/L 55.250 110 70-130
2-Butanone (MEK)ug/L 114100 114 70-133
2-Chlorotoluene ug/L 44.250 88 70-130
2-Hexanone ug/L 90.1100 90 70-130
4-Chlorotoluene ug/L 42.450 85 70-130
4-Methyl-2-pentanone (MIBK)ug/L 99.7100 100 70-130
Acetone ug/L 105100 105 70-144
Benzene ug/L 49.450 99 70-130
Bromobenzene ug/L 44.450 89 70-130
Bromochloromethane ug/L 54.050 108 70-130
Bromodichloromethane ug/L 49.150 98 70-130
Bromoform ug/L 42.750 85 70-131
Bromomethane ug/L 57.250 114 30-177
Carbon tetrachloride ug/L 50.850 102 70-130
Chlorobenzene ug/L 45.350 91 70-130
Chloroethane ug/L 45.5 IL5091 46-131
Chloroform ug/L 50.950 102 70-130
Chloromethane ug/L 45.450 91 49-130
cis-1,2-Dichloroethene ug/L 53.550 107 70-130
cis-1,3-Dichloropropene ug/L 50.650 101 70-130
Dibromochloromethane ug/L 43.750 87 70-130
Dibromomethane ug/L 49.350 99 70-130
Dichlorodifluoromethane ug/L 51.750 103 52-134
Diisopropyl ether ug/L 48.650 97 70-131
Ethylbenzene ug/L 45.750 91 70-130
Hexachloro-1,3-butadiene ug/L 47.250 94 70-131
m&p-Xylene ug/L 92.9100 93 70-130
Methyl-tert-butyl ether ug/L 53.750 107 70-130
Methylene Chloride ug/L 53.450 107 68-130
n-Butylbenzene ug/L 47.550 95 70-130
n-Propylbenzene ug/L 44.950 90 70-130
Naphthalene ug/L 45.450 91 70-133
o-Xylene ug/L 46.150 92 70-130
p-Isopropyltoluene ug/L 47.450 95 70-130
sec-Butylbenzene ug/L 45.950 92 70-130
Styrene ug/L 46.950 94 70-130
Tetrachloroethene ug/L 45.150 90 70-130
Toluene ug/L 48.150 96 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92557149
LOADING RACK
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3372332LABORATORY CONTROL SAMPLE:
LCSSpike
trans-1,2-Dichloroethene ug/L 56.550 113 70-130
trans-1,3-Dichloropropene ug/L 49.550 99 70-130
Trichloroethene ug/L 50.750 101 70-130
Trichlorofluoromethane ug/L 50.750 101 61-130
Vinyl acetate ug/L 122 v1100122 70-140
Vinyl chloride ug/L 52.150 104 59-142
Xylene (Total)ug/L 139150 93 70-130
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3372333MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92556599019
3372334
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 8000 110 70-135108 28000ND8790 8600
1,1,1-Trichloroethane ug/L 8000 127 70-148134 180004840058600 59200
1,1,2,2-Tetrachloroethane ug/L 8000 107 70-131106 18000ND8550 8460
1,1,2-Trichloroethane ug/L 8000 122 70-136115 78000ND9790 9160
1,1-Dichloroethane ug/L 8000 128 70-147122 58000390J10600 10200
1,1-Dichloroethene ug/L 8000 128 70-158123 280001050020700 20300
1,1-Dichloropropene ug/L 8000 118 70-149115 38000ND9470 9190
1,2,3-Trichlorobenzene ug/L 8000 104 68-140107 38000ND8300 8550
1,2,3-Trichloropropane ug/L 8000 106 67-137104 28000ND8490 8290
1,2,4-Trichlorobenzene ug/L 8000 99 70-139104 48000ND7930 8290
1,2,4-Trimethylbenzene ug/L 8000 103 70-134100 38000281J8500 8250
1,2-Dibromo-3-chloropropane ug/L 8000 97 69-136101 48000ND7800 8090
1,2-Dibromoethane (EDB)ug/L 8000 110 70-137108 28000ND8770 8630
1,2-Dichlorobenzene ug/L 8000 103 70-133102 18000ND8270 8160
1,2-Dichloroethane ug/L 8000 120 67-138116 48000ND9630 9270
1,2-Dichloropropane ug/L 8000 122 70-138115 68000ND9780 9190
1,3,5-Trimethylbenzene ug/L 8000 107 70-138106 18000ND8570 8510
1,3-Dichlorobenzene ug/L 8000 104 70-133102 28000ND8290 8150
1,3-Dichloropropane ug/L 8000 110 70-136108 28000ND8770 8630
1,4-Dichlorobenzene ug/L 8000 105 70-133103 18000ND8370 8280
2,2-Dichloropropane ug/L 8000 119 52-155113 68000ND9530 9010
2-Butanone (MEK)ug/L 16000 128 61-147127 116000ND20500 20300
2-Chlorotoluene ug/L 8000 106 70-141104 18000ND8450 8320
2-Hexanone ug/L 16000 112 67-139109 316000ND17900 17400
4-Chlorotoluene ug/L 8000 102 70-135100 28000ND8160 7970
4-Methyl-2-pentanone (MIBK) ug/L 16000 123 67-136119 316000ND19700 19000
Acetone ug/L 16000 119 55-159114 416000ND19100 18300
Benzene ug/L 8000 121 67-150115 58000186J9890 9400
Bromobenzene ug/L 8000 107 70-134105 28000ND8540 8400
Bromochloromethane ug/L 8000 124 70-146123 18000ND9950 9810
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92557149
LOADING RACK
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3372333MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92556599019
3372334
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Bromodichloromethane ug/L 8000 116 70-138112 48000ND9300 8960
Bromoform ug/L 8000 94 57-13891 38000ND7520 7270
Bromomethane ug/L 8000 40 10-20049 218000ND3180 3940
Carbon tetrachloride ug/L 8000 121 70-147116 48000ND9640 9250
Chlorobenzene ug/L 8000 111 70-137107 58000ND8920 8520
Chloroethane ug/L IL800010751-166101 58000ND8530 8110
Chloroform ug/L 8000 117 70-144113 38000277J9640 9340
Chloromethane ug/L 8000 56 24-16161 88000ND4510 4860
cis-1,2-Dichloroethene ug/L 8000 123 67-148119 38000ND9850 9560
cis-1,3-Dichloropropene ug/L 8000 115 70-142111 48000ND9200 8860
Dibromochloromethane ug/L 8000 98 68-13897 18000ND7840 7720
Dibromomethane ug/L 8000 117 70-134115 28000ND9390 9170
Dichlorodifluoromethane ug/L 8000 114 43-155109 48000ND9110 8740
Diisopropyl ether ug/L 8000 116 65-146113 28000ND9250 9040
Ethylbenzene ug/L 8000 110 68-143107 28000ND8790 8580
Hexachloro-1,3-butadiene ug/L 8000 99 62-151103 48000ND7920 8240
Isopropylbenzene (Cumene) ug/L 28810 8650
m&p-Xylene ug/L 16000 109 53-157107 116000ND17700 17400
Methyl-tert-butyl ether ug/L 8000 125 59-156123 18000ND9960 9840
Methylene Chloride ug/L 8000 120 64-148117 38000ND10200 9880
n-Butylbenzene ug/L 8000 102 70-139105 28000ND8190 8370
n-Propylbenzene ug/L 8000 105 70-138104 18000ND8410 8320
Naphthalene ug/L 8000 96 57-15097 18000290J7960 8080
o-Xylene ug/L 8000 109 68-143106 28000ND8820 8620
p-Isopropyltoluene ug/L 8000 106 70-141106 08000ND8510 8500
sec-Butylbenzene ug/L 8000 105 70-137106 18000ND8380 8460
Styrene ug/L 8000 110 70-136108 28000ND8810 8600
Tetrachloroethene ug/L 8000 104 70-139102 28000ND8360 8190
Toluene ug/L 8000 120 47-157114 48000351J9910 9490
trans-1,2-Dichloroethene ug/L 8000 130 70-149125 48000ND10400 9980
trans-1,3-Dichloropropene ug/L 8000 109 70-138107 28000ND8700 8520
Trichloroethene ug/L 8000 124 70-149118 58000ND9920 9470
Trichlorofluoromethane ug/L 8000 121 61-154115 58000ND9660 9240
Vinyl acetate ug/L v11600014048-156137 216000ND22400 21900
Vinyl chloride ug/L 8000 120 55-172112 78000ND9580 8950
Xylene (Total)ug/L 24000 110 66-145109 224000ND26500 26000
1,2-Dichloroethane-d4 (S)%96 70-13096
4-Bromofluorobenzene (S)%99 70-130100
Toluene-d8 (S)%101 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92557149
LOADING RACK
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
642624
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92557149001, 92557149002, 92557149004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3372506
Associated Lab Samples:92557149001, 92557149002, 92557149004
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 08/24/21 12:07
1,1,1-Trichloroethane ug/L ND 1.0 08/24/21 12:07
1,1,2,2-Tetrachloroethane ug/L ND 1.0 08/24/21 12:07
1,1,2-Trichloroethane ug/L ND 1.0 08/24/21 12:07
1,1-Dichloroethane ug/L ND 1.0 08/24/21 12:07
1,1-Dichloroethene ug/L ND 1.0 08/24/21 12:07
1,1-Dichloropropene ug/L ND 1.0 08/24/21 12:07
1,2,3-Trichlorobenzene ug/L ND 1.0 08/24/21 12:07
1,2,3-Trichloropropane ug/L ND 1.0 08/24/21 12:07
1,2,4-Trichlorobenzene ug/L ND 1.0 08/24/21 12:07
1,2,4-Trimethylbenzene ug/L ND 1.0 08/24/21 12:07
1,2-Dibromo-3-chloropropane ug/L ND 2.0 08/24/21 12:07
1,2-Dibromoethane (EDB)ug/L ND 1.0 08/24/21 12:07
1,2-Dichlorobenzene ug/L ND 1.0 08/24/21 12:07
1,2-Dichloroethane ug/L ND 1.0 08/24/21 12:07
1,2-Dichloropropane ug/L ND 1.0 08/24/21 12:07
1,3,5-Trimethylbenzene ug/L ND 1.0 08/24/21 12:07
1,3-Dichlorobenzene ug/L ND 1.0 08/24/21 12:07
1,3-Dichloropropane ug/L ND 1.0 08/24/21 12:07
1,4-Dichlorobenzene ug/L ND 1.0 08/24/21 12:07
2,2-Dichloropropane ug/L ND 1.0 08/24/21 12:07
2-Butanone (MEK)ug/L ND 5.0 08/24/21 12:07
2-Chlorotoluene ug/L ND 1.0 08/24/21 12:07
2-Hexanone ug/L ND 5.0 08/24/21 12:07
4-Chlorotoluene ug/L ND 1.0 08/24/21 12:07
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 08/24/21 12:07
Acetone ug/L ND 25.0 08/24/21 12:07
Benzene ug/L ND 1.0 08/24/21 12:07
Bromobenzene ug/L ND 1.0 08/24/21 12:07
Bromochloromethane ug/L ND 1.0 08/24/21 12:07
Bromodichloromethane ug/L ND 1.0 08/24/21 12:07
Bromoform ug/L ND 1.0 08/24/21 12:07
Bromomethane ug/L ND 2.0 08/24/21 12:07
Carbon tetrachloride ug/L ND 1.0 08/24/21 12:07
Chlorobenzene ug/L ND 1.0 08/24/21 12:07
Chloroethane ug/L ND 1.0 08/24/21 12:07
Chloroform ug/L ND 1.0 08/24/21 12:07
Chloromethane ug/L ND 1.0 08/24/21 12:07
cis-1,2-Dichloroethene ug/L ND 1.0 08/24/21 12:07
cis-1,3-Dichloropropene ug/L ND 1.0 08/24/21 12:07
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92557149
LOADING RACK
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3372506
Associated Lab Samples:92557149001, 92557149002, 92557149004
Matrix: Water
Analyzed
Dibromochloromethane ug/L ND 1.0 08/24/21 12:07
Dibromomethane ug/L ND 1.0 08/24/21 12:07
Dichlorodifluoromethane ug/L ND 1.0 08/24/21 12:07
Diisopropyl ether ug/L ND 1.0 08/24/21 12:07
Ethylbenzene ug/L ND 1.0 08/24/21 12:07
Hexachloro-1,3-butadiene ug/L ND 2.0 08/24/21 12:07
Isopropylbenzene (Cumene)ug/L ND 1.0 08/24/21 12:07
m&p-Xylene ug/L ND 2.0 08/24/21 12:07
Methyl-tert-butyl ether ug/L ND 1.0 08/24/21 12:07
Methylene Chloride ug/L ND 5.0 08/24/21 12:07
n-Butylbenzene ug/L ND 1.0 08/24/21 12:07
n-Propylbenzene ug/L ND 1.0 08/24/21 12:07
Naphthalene ug/L ND 1.0 08/24/21 12:07
o-Xylene ug/L ND 1.0 08/24/21 12:07
p-Isopropyltoluene ug/L ND 1.0 08/24/21 12:07
sec-Butylbenzene ug/L ND 1.0 08/24/21 12:07
Styrene ug/L ND 1.0 08/24/21 12:07
Tetrachloroethene ug/L ND 1.0 08/24/21 12:07
Toluene ug/L ND 1.0 08/24/21 12:07
trans-1,2-Dichloroethene ug/L ND 1.0 08/24/21 12:07
trans-1,3-Dichloropropene ug/L ND 1.0 08/24/21 12:07
Trichloroethene ug/L ND 1.0 08/24/21 12:07
Trichlorofluoromethane ug/L ND 1.0 08/24/21 12:07
Vinyl acetate ug/L ND 2.0 08/24/21 12:07
Vinyl chloride ug/L ND 1.0 08/24/21 12:07
Xylene (Total)ug/L ND 1.0 08/24/21 12:07
1,2-Dichloroethane-d4 (S)%102 70-130 08/24/21 12:07
4-Bromofluorobenzene (S)%97 70-130 08/24/21 12:07
Toluene-d8 (S)%99 70-130 08/24/21 12:07
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3372507LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.550 101 70-130
1,1,1-Trichloroethane ug/L 50.450 101 70-130
1,1,2,2-Tetrachloroethane ug/L 48.850 98 70-130
1,1,2-Trichloroethane ug/L 47.850 96 70-130
1,1-Dichloroethane ug/L 49.250 98 70-130
1,1-Dichloroethene ug/L 52.550 105 70-132
1,1-Dichloropropene ug/L 48.850 98 70-131
1,2,3-Trichlorobenzene ug/L 50.450 101 70-134
1,2,3-Trichloropropane ug/L 46.950 94 70-130
1,2,4-Trichlorobenzene ug/L 51.850 104 70-130
1,2,4-Trimethylbenzene ug/L 52.050 104 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92557149
LOADING RACK
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3372507LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/L 49.350 99 70-132
1,2-Dibromoethane (EDB)ug/L 49.650 99 70-130
1,2-Dichlorobenzene ug/L 52.050 104 70-130
1,2-Dichloroethane ug/L 47.450 95 70-130
1,2-Dichloropropane ug/L 48.350 97 70-130
1,3,5-Trimethylbenzene ug/L 52.350 105 70-130
1,3-Dichlorobenzene ug/L 52.650 105 70-130
1,3-Dichloropropane ug/L 48.050 96 70-130
1,4-Dichlorobenzene ug/L 53.050 106 70-130
2,2-Dichloropropane ug/L 51.250 102 70-130
2-Butanone (MEK)ug/L 86.5100 86 70-133
2-Chlorotoluene ug/L 51.650 103 70-130
2-Hexanone ug/L 89.4100 89 70-130
4-Chlorotoluene ug/L 50.050 100 70-130
4-Methyl-2-pentanone (MIBK)ug/L 87.8100 88 70-130
Acetone ug/L 91.3100 91 70-144
Benzene ug/L 48.750 97 70-130
Bromobenzene ug/L 51.550 103 70-130
Bromochloromethane ug/L 50.550 101 70-130
Bromodichloromethane ug/L 50.050 100 70-130
Bromoform ug/L 50.850 102 70-131
Bromomethane ug/L 65.550 131 30-177
Carbon tetrachloride ug/L 51.150 102 70-130
Chlorobenzene ug/L 51.050 102 70-130
Chloroethane ug/L 50.350 101 46-131
Chloroform ug/L 47.350 95 70-130
Chloromethane ug/L 45.950 92 49-130
cis-1,2-Dichloroethene ug/L 48.550 97 70-130
cis-1,3-Dichloropropene ug/L 49.450 99 70-130
Dibromochloromethane ug/L 51.650 103 70-130
Dibromomethane ug/L 49.050 98 70-130
Dichlorodifluoromethane ug/L 48.850 98 52-134
Diisopropyl ether ug/L 45.550 91 70-131
Ethylbenzene ug/L 51.250 102 70-130
Hexachloro-1,3-butadiene ug/L 53.850 108 70-131
Isopropylbenzene (Cumene)ug/L 53.450 107 70-130
m&p-Xylene ug/L 102100 102 70-130
Methyl-tert-butyl ether ug/L 46.950 94 70-130
Methylene Chloride ug/L 45.650 91 68-130
n-Butylbenzene ug/L 54.250 108 70-130
n-Propylbenzene ug/L 51.750 103 70-130
Naphthalene ug/L 48.650 97 70-133
o-Xylene ug/L 49.850 100 70-130
p-Isopropyltoluene ug/L 53.050 106 70-130
sec-Butylbenzene ug/L 51.850 104 70-130
Styrene ug/L 51.350 103 70-130
Tetrachloroethene ug/L 51.150 102 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92557149
LOADING RACK
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3372507LABORATORY CONTROL SAMPLE:
LCSSpike
Toluene ug/L 48.850 98 70-130
trans-1,2-Dichloroethene ug/L 49.850 100 70-130
trans-1,3-Dichloropropene ug/L 49.550 99 70-130
Trichloroethene ug/L 50.250 100 70-130
Trichlorofluoromethane ug/L 50.550 101 61-130
Vinyl acetate ug/L 94.5100 94 70-140
Vinyl chloride ug/L 51.250 102 59-142
Xylene (Total)ug/L 152150 101 70-130
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3372508MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92557149001
3372509
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L R11011370-13595 5120ND11.3 19.1
1,1,1-Trichloroethane ug/L R11011870-148100 5220ND11.8 20.0
1,1,2,2-Tetrachloroethane ug/L R11011070-13191 4920ND11.0 18.2
1,1,2-Trichloroethane ug/L R11010570-13691 5420ND10.5 18.3
1,1-Dichloroethane ug/L R11011570-14798 5220ND11.5 19.7
1,1-Dichloroethene ug/L R11013070-158108 5020ND13.0 21.5
1,1-Dichloropropene ug/L R11012070-149101 5120ND12.0 20.2
1,2,3-Trichlorobenzene ug/L R11013268-14096 3720ND13.2 19.1
1,2,3-Trichloropropane ug/L R11010867-13787 4720ND10.8 17.5
1,2,4-Trichlorobenzene ug/L R11012970-13994 3820ND12.9 18.9
1,2,4-Trimethylbenzene ug/L R11011870-13494 4620ND11.8 18.9
1,2-Dibromo-3-chloropropane ug/L R11011569-13691 4520ND11.5 18.1
1,2-Dibromoethane (EDB)ug/L R11011470-13794 4820ND11.4 18.7
1,2-Dichlorobenzene ug/L R11011570-13392 4620ND11.5 18.4
1,2-Dichloroethane ug/L R11010767-13890 5120ND10.7 18.0
1,2-Dichloropropane ug/L R11011270-13897 5420ND11.2 19.4
1,3,5-Trimethylbenzene ug/L R11012070-138100 4920ND12.0 19.9
1,3-Dichlorobenzene ug/L R11011970-13397 4820ND11.9 19.4
1,3-Dichloropropane ug/L R11010970-13693 5220ND10.9 18.5
1,4-Dichlorobenzene ug/L R11012070-13396 4720ND12.0 19.2
2,2-Dichloropropane ug/L R11012152-155103 5220ND12.1 20.7
2-Butanone (MEK)ug/L R1209561-14781 5240ND19.0 32.4
2-Chlorotoluene ug/L R11011670-14196 4920ND11.6 19.2
2-Hexanone ug/L R12010167-13984 5040ND20.2 33.6
4-Chlorotoluene ug/L R11011370-13594 4920ND11.3 18.7
4-Methyl-2-pentanone (MIBK) ug/L R1209867-13683 5140ND19.7 33.2
Acetone ug/L 20 110 55-1598740ND22J 34.7
Benzene ug/L R11011467-15097 5220ND11.4 19.4
Bromobenzene ug/L R11011770-13497 5020ND11.7 19.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92557149
LOADING RACK
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3372508MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92557149001
3372509
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Bromochloromethane ug/L R11011270-146100 5720ND11.2 20.0
Bromodichloromethane ug/L R11010870-13898 5820ND10.8 19.6
Bromoform ug/L R11010757-13894 5520ND10.7 18.8
Bromomethane ug/L R1,v11016010-200134 5120ND16.0 26.9
Carbon tetrachloride ug/L R11012270-147104 5220ND12.2 20.8
Chlorobenzene ug/L R11011870-13797 4920ND11.8 19.4
Chloroethane ug/L R11014451-166108 4020ND14.4 21.6
Chloroform ug/L R11010670-14490 5120ND10.6 18.0
Chloromethane ug/L R11011724-16195 4820ND11.7 18.9
cis-1,2-Dichloroethene ug/L R11011167-14899 5620ND11.1 19.7
cis-1,3-Dichloropropene ug/L R11010970-14294 5320ND10.9 18.8
Dibromochloromethane ug/L R11011168-13897 5420ND11.1 19.4
Dibromomethane ug/L R11011570-13493 4820ND11.5 18.7
Dichlorodifluoromethane ug/L R11011243-15597 5420ND11.2 19.3
Diisopropyl ether ug/L R11010165-14689 5520ND10.1 17.7
Ethylbenzene ug/L R11011868-143100 5120ND11.8 19.9
Hexachloro-1,3-butadiene ug/L R11015062-151109 3720ND15.0 21.9
Isopropylbenzene (Cumene) ug/L 10 124 70-136103 5020ND12.4 20.5
m&p-Xylene ug/L R12012053-15799 4940ND24.0 39.5
Methyl-tert-butyl ether ug/L 10 102 59-15690 292012.5 22.6 30.4
Methylene Chloride ug/L R11010864-14891 5020ND10.8 18.1
n-Butylbenzene ug/L R11013370-139104 4420ND13.3 20.8
n-Propylbenzene ug/L R11012270-138100 4820ND12.2 20.0
Naphthalene ug/L R11011857-15085 3620ND11.8 17.0
o-Xylene ug/L R11011468-14394 4920ND11.4 18.9
p-Isopropyltoluene ug/L R11012870-141102 4620ND12.8 20.4
sec-Butylbenzene ug/L R11012370-137101 4920ND12.3 20.2
Styrene ug/L R11011370-13693 4920ND11.3 18.7
Tetrachloroethene ug/L R11012870-139102 4620ND12.8 20.4
Toluene ug/L R11011647-15798 5220ND11.6 19.7
trans-1,2-Dichloroethene ug/L R11011970-149101 5220ND11.9 20.3
trans-1,3-Dichloropropene ug/L R11010670-13894 5520ND10.6 18.7
Trichloroethene ug/L R11012070-14998 4820ND12.0 19.6
Trichlorofluoromethane ug/L R11012661-154105 5020ND12.6 21.1
Vinyl acetate ug/L R12010448-15690 5340ND20.8 35.8
Vinyl chloride ug/L R11012555-172104 5020ND12.5 20.8
Xylene (Total)ug/L RS3011866-14597 4960ND35.4 58.4
1,2-Dichloroethane-d4 (S)%96 70-13094
4-Bromofluorobenzene (S)%98 70-13099
Toluene-d8 (S)%99 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92557149
LOADING RACK
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
642882
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92557149013, 92557149015, 92557149016, 92557149017, 92557149018
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3373519
Associated Lab Samples:92557149013, 92557149015, 92557149016, 92557149017, 92557149018
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 08/25/21 14:58
1,1,1-Trichloroethane ug/L ND 1.0 08/25/21 14:58
1,1,2,2-Tetrachloroethane ug/L ND 1.0 08/25/21 14:58
1,1,2-Trichloroethane ug/L ND 1.0 08/25/21 14:58
1,1-Dichloroethane ug/L ND 1.0 08/25/21 14:58
1,1-Dichloroethene ug/L ND 1.0 08/25/21 14:58
1,1-Dichloropropene ug/L ND 1.0 08/25/21 14:58
1,2,3-Trichlorobenzene ug/L ND 1.0 08/25/21 14:58
1,2,3-Trichloropropane ug/L ND 1.0 08/25/21 14:58
1,2,4-Trichlorobenzene ug/L ND 1.0 08/25/21 14:58
1,2,4-Trimethylbenzene ug/L ND 1.0 08/25/21 14:58
1,2-Dibromo-3-chloropropane ug/L ND 2.0 08/25/21 14:58
1,2-Dibromoethane (EDB)ug/L ND 1.0 08/25/21 14:58
1,2-Dichlorobenzene ug/L ND 1.0 08/25/21 14:58
1,2-Dichloroethane ug/L ND 1.0 08/25/21 14:58
1,2-Dichloropropane ug/L ND 1.0 08/25/21 14:58
1,3,5-Trimethylbenzene ug/L ND 1.0 08/25/21 14:58
1,3-Dichlorobenzene ug/L ND 1.0 08/25/21 14:58
1,3-Dichloropropane ug/L ND 1.0 08/25/21 14:58
1,4-Dichlorobenzene ug/L ND 1.0 08/25/21 14:58
2,2-Dichloropropane ug/L ND 1.0 08/25/21 14:58
2-Butanone (MEK)ug/L ND 5.0 08/25/21 14:58
2-Chlorotoluene ug/L ND 1.0 08/25/21 14:58
2-Hexanone ug/L ND 5.0 08/25/21 14:58
4-Chlorotoluene ug/L ND 1.0 08/25/21 14:58
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 08/25/21 14:58
Acetone ug/L ND 25.0 08/25/21 14:58
Benzene ug/L ND 1.0 08/25/21 14:58
Bromobenzene ug/L ND 1.0 08/25/21 14:58
Bromochloromethane ug/L ND 1.0 08/25/21 14:58
Bromodichloromethane ug/L ND 1.0 08/25/21 14:58
Bromoform ug/L ND 1.0 08/25/21 14:58
Bromomethane ug/L ND 2.0 08/25/21 14:58
Carbon tetrachloride ug/L ND 1.0 08/25/21 14:58
Chlorobenzene ug/L ND 1.0 08/25/21 14:58
Chloroethane ug/L ND 1.0 08/25/21 14:58
Chloroform ug/L ND 1.0 08/25/21 14:58
Chloromethane ug/L ND 1.0 08/25/21 14:58
cis-1,2-Dichloroethene ug/L ND 1.0 08/25/21 14:58
cis-1,3-Dichloropropene ug/L ND 1.0 08/25/21 14:58
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92557149
LOADING RACK
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3373519
Associated Lab Samples:92557149013, 92557149015, 92557149016, 92557149017, 92557149018
Matrix: Water
Analyzed
Dibromochloromethane ug/L ND 1.0 08/25/21 14:58
Dibromomethane ug/L ND 1.0 08/25/21 14:58
Dichlorodifluoromethane ug/L ND 1.0 08/25/21 14:58
Diisopropyl ether ug/L ND 1.0 08/25/21 14:58
Ethylbenzene ug/L ND 1.0 08/25/21 14:58
Hexachloro-1,3-butadiene ug/L ND 2.0 08/25/21 14:58
Isopropylbenzene (Cumene)ug/L ND 1.0 08/25/21 14:58
m&p-Xylene ug/L ND 2.0 08/25/21 14:58
Methyl-tert-butyl ether ug/L ND 1.0 08/25/21 14:58
Methylene Chloride ug/L ND 5.0 08/25/21 14:58
n-Butylbenzene ug/L ND 1.0 08/25/21 14:58
n-Propylbenzene ug/L ND 1.0 08/25/21 14:58
Naphthalene ug/L ND 1.0 08/25/21 14:58
o-Xylene ug/L ND 1.0 08/25/21 14:58
p-Isopropyltoluene ug/L ND 1.0 08/25/21 14:58
sec-Butylbenzene ug/L ND 1.0 08/25/21 14:58
Styrene ug/L ND 1.0 08/25/21 14:58
Tetrachloroethene ug/L ND 1.0 08/25/21 14:58
Toluene ug/L ND 1.0 08/25/21 14:58
trans-1,2-Dichloroethene ug/L ND 1.0 08/25/21 14:58
trans-1,3-Dichloropropene ug/L ND 1.0 08/25/21 14:58
Trichloroethene ug/L ND 1.0 08/25/21 14:58
Trichlorofluoromethane ug/L ND 1.0 08/25/21 14:58
Vinyl acetate ug/L ND 2.0 08/25/21 14:58
Vinyl chloride ug/L ND 1.0 08/25/21 14:58
Xylene (Total)ug/L ND 1.0 08/25/21 14:58
1,2-Dichloroethane-d4 (S)%105 70-130 08/25/21 14:58
4-Bromofluorobenzene (S)%101 70-130 08/25/21 14:58
Toluene-d8 (S)%101 70-130 08/25/21 14:58
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3373520LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.950 102 70-130
1,1,1-Trichloroethane ug/L 44.950 90 70-130
1,1,2,2-Tetrachloroethane ug/L 52.550 105 70-130
1,1,2-Trichloroethane ug/L 48.250 96 70-130
1,1-Dichloroethane ug/L 47.250 94 70-130
1,1-Dichloroethene ug/L 45.850 92 70-132
1,1-Dichloropropene ug/L 47.050 94 70-131
1,2,3-Trichlorobenzene ug/L 49.750 99 70-134
1,2,3-Trichloropropane ug/L 51.650 103 70-130
1,2,4-Trichlorobenzene ug/L 50.050 100 70-130
1,2,4-Trimethylbenzene ug/L 52.050 104 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92557149
LOADING RACK
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3373520LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/L 56.450 113 70-132
1,2-Dibromoethane (EDB)ug/L 52.250 104 70-130
1,2-Dichlorobenzene ug/L 49.550 99 70-130
1,2-Dichloroethane ug/L 46.650 93 70-130
1,2-Dichloropropane ug/L 49.150 98 70-130
1,3,5-Trimethylbenzene ug/L 51.250 102 70-130
1,3-Dichlorobenzene ug/L 50.050 100 70-130
1,3-Dichloropropane ug/L 50.650 101 70-130
1,4-Dichlorobenzene ug/L 50.150 100 70-130
2,2-Dichloropropane ug/L 47.250 94 70-130
2-Butanone (MEK)ug/L 108100 108 70-133
2-Chlorotoluene ug/L 52.650 105 70-130
2-Hexanone ug/L 117100 117 70-130
4-Chlorotoluene ug/L 51.350 103 70-130
4-Methyl-2-pentanone (MIBK)ug/L 108100 108 70-130
Acetone ug/L 98.8100 99 70-144
Benzene ug/L 47.650 95 70-130
Bromobenzene ug/L 51.350 103 70-130
Bromochloromethane ug/L 44.650 89 70-130
Bromodichloromethane ug/L 48.150 96 70-130
Bromoform ug/L 51.250 102 70-131
Bromomethane ug/L 38.850 78 30-177
Carbon tetrachloride ug/L 45.550 91 70-130
Chlorobenzene ug/L 49.150 98 70-130
Chloroethane ug/L 48.550 97 46-131
Chloroform ug/L 45.650 91 70-130
Chloromethane ug/L 48.450 97 49-130
cis-1,2-Dichloroethene ug/L 46.350 93 70-130
cis-1,3-Dichloropropene ug/L 49.850 100 70-130
Dibromochloromethane ug/L 52.550 105 70-130
Dibromomethane ug/L 44.850 90 70-130
Dichlorodifluoromethane ug/L 49.250 98 52-134
Diisopropyl ether ug/L 48.550 97 70-131
Ethylbenzene ug/L 49.650 99 70-130
Hexachloro-1,3-butadiene ug/L 47.450 95 70-131
Isopropylbenzene (Cumene)ug/L 50.250 100 70-130
m&p-Xylene ug/L 99.3100 99 70-130
Methyl-tert-butyl ether ug/L 48.050 96 70-130
Methylene Chloride ug/L 50.350 101 68-130
n-Butylbenzene ug/L 52.150 104 70-130
n-Propylbenzene ug/L 52.050 104 70-130
Naphthalene ug/L 51.850 104 70-133
o-Xylene ug/L 48.850 98 70-130
p-Isopropyltoluene ug/L 49.550 99 70-130
sec-Butylbenzene ug/L 49.450 99 70-130
Styrene ug/L 50.450 101 70-130
Tetrachloroethene ug/L 47.350 95 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92557149
LOADING RACK
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3373520LABORATORY CONTROL SAMPLE:
LCSSpike
Toluene ug/L 46.450 93 70-130
trans-1,2-Dichloroethene ug/L 47.150 94 70-130
trans-1,3-Dichloropropene ug/L 48.550 97 70-130
Trichloroethene ug/L 45.750 91 70-130
Trichlorofluoromethane ug/L 43.150 86 61-130
Vinyl acetate ug/L 116100 116 70-140
Vinyl chloride ug/L 49.150 98 59-142
Xylene (Total)ug/L 148150 99 70-130
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3373522MATRIX SPIKE SAMPLE:
MSSpike
Result
92557043003
1,1,1,2-Tetrachloroethane ug/L 22.520 112 70-135ND
1,1,1-Trichloroethane ug/L 25.220 126 70-148ND
1,1,2,2-Tetrachloroethane ug/L 22.320 111 70-131ND
1,1,2-Trichloroethane ug/L 22.320 112 70-136ND
1,1-Dichloroethane ug/L 24.920 124 70-147ND
1,1-Dichloroethene ug/L 24.820 124 70-158ND
1,1-Dichloropropene ug/L 24.520 123 70-149ND
1,2,3-Trichlorobenzene ug/L 22.820 114 68-140ND
1,2,3-Trichloropropane ug/L 21.620 108 67-137ND
1,2,4-Trichlorobenzene ug/L 23.220 116 70-139ND
1,2,4-Trimethylbenzene ug/L 23.320 111 70-134ND
1,2-Dibromo-3-chloropropane ug/L 22.420 112 69-136ND
1,2-Dibromoethane (EDB)ug/L 22.120 110 70-137ND
1,2-Dichlorobenzene ug/L 22.920 114 70-133ND
1,2-Dichloroethane ug/L 23.520 118 67-138ND
1,2-Dichloropropane ug/L 23.320 117 70-138ND
1,3,5-Trimethylbenzene ug/L 23.720 118 70-138ND
1,3-Dichlorobenzene ug/L 23.520 118 70-133ND
1,3-Dichloropropane ug/L 22.120 111 70-136ND
1,4-Dichlorobenzene ug/L 23.520 118 70-133ND
2,2-Dichloropropane ug/L 31.3 M120156 52-155ND
2-Butanone (MEK)ug/L 46.740 117 61-147ND
2-Chlorotoluene ug/L 23.620 118 70-141ND
2-Hexanone ug/L 44.240 110 67-139ND
4-Chlorotoluene ug/L 22.520 113 70-135ND
4-Methyl-2-pentanone (MIBK)ug/L 43.640 109 67-136ND
Acetone ug/L 48.440 121 55-159ND
Benzene ug/L 23.320 116 67-150ND
Bromobenzene ug/L 23.420 117 70-134ND
Bromochloromethane ug/L 24.820 124 70-146ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92557149
LOADING RACK
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3373522MATRIX SPIKE SAMPLE:
MSSpike
Result
92557043003
Bromodichloromethane ug/L 22.420 112 70-138ND
Bromoform ug/L 21.320 107 57-138ND
Bromomethane ug/L 31.1 v120155 10-200ND
Carbon tetrachloride ug/L 23.920 120 70-147ND
Chlorobenzene ug/L 23.420 117 70-137ND
Chloroethane ug/L 24.020 120 51-166ND
Chloroform ug/L 24.920 125 70-144ND
Chloromethane ug/L 21.720 108 24-161ND
cis-1,2-Dichloroethene ug/L 24.520 122 67-148ND
cis-1,3-Dichloropropene ug/L 23.220 116 70-142ND
Dibromochloromethane ug/L 21.920 110 68-138ND
Dibromomethane ug/L 23.320 117 70-134ND
Dichlorodifluoromethane ug/L 22.720 113 43-155ND
Diisopropyl ether ug/L 22.920 115 65-146ND
Ethylbenzene ug/L 24.120 118 68-143ND
Hexachloro-1,3-butadiene ug/L 22.820 114 62-151ND
Isopropylbenzene (Cumene)ug/L 24.5
m&p-Xylene ug/L 29840 75 53-157269
Methyl-tert-butyl ether ug/L 22.520 112 59-156ND
Methylene Chloride ug/L 22.420 112 64-148ND
n-Butylbenzene ug/L 23.220 116 70-139ND
n-Propylbenzene ug/L 24.020 120 70-138ND
Naphthalene ug/L 23.220 110 57-1501.2
o-Xylene ug/L 23.320 115 68-143ND
p-Isopropyltoluene ug/L 23.820 119 70-141ND
sec-Butylbenzene ug/L 23.320 116 70-137ND
Styrene ug/L 23.420 117 70-136ND
Tetrachloroethene ug/L 22.520 112 70-139ND
Toluene ug/L 23.720 119 47-157ND
trans-1,2-Dichloroethene ug/L 25.520 128 70-149ND
trans-1,3-Dichloropropene ug/L 22.420 112 70-138ND
Trichloroethene ug/L 23.920 120 70-149ND
Trichlorofluoromethane ug/L 22.620 113 61-154ND
Vinyl acetate ug/L 50.540 126 48-156ND
Vinyl chloride ug/L 25.020 125 55-172ND
Xylene (Total)ug/L 32260 89 66-145269
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%HS99 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92557043001
3373521SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L NDND
1,1,1-Trichloroethane ug/L NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 61 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92557149
LOADING RACK
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92557043001
3373521SAMPLE DUPLICATE:
1,1,2,2-Tetrachloroethane ug/L NDND
1,1,2-Trichloroethane ug/L NDND
1,1-Dichloroethane ug/L NDND
1,1-Dichloroethene ug/L NDND
1,1-Dichloropropene ug/L NDND
1,2,3-Trichlorobenzene ug/L NDND
1,2,3-Trichloropropane ug/L .78JND
1,2,4-Trichlorobenzene ug/L NDND
1,2,4-Trimethylbenzene ug/L 143 4138
1,2-Dibromo-3-chloropropane ug/L NDND
1,2-Dibromoethane (EDB)ug/L NDND
1,2-Dichlorobenzene ug/L NDND
1,2-Dichloroethane ug/L NDND
1,2-Dichloropropane ug/L NDND
1,3,5-Trimethylbenzene ug/L 22.2 620.8
1,3-Dichlorobenzene ug/L NDND
1,3-Dichloropropane ug/L NDND
1,4-Dichlorobenzene ug/L NDND
2,2-Dichloropropane ug/L NDND
2-Butanone (MEK)ug/L NDND
2-Chlorotoluene ug/L NDND
2-Hexanone ug/L NDND
4-Chlorotoluene ug/L NDND
4-Methyl-2-pentanone (MIBK)ug/L NDND
Acetone ug/L NDND
Benzene ug/L .43JND
Bromobenzene ug/L NDND
Bromochloromethane ug/L NDND
Bromodichloromethane ug/L NDND
Bromoform ug/L NDND
Bromomethane ug/L ND v1ND
Carbon tetrachloride ug/L NDND
Chlorobenzene ug/L NDND
Chloroethane ug/L NDND
Chloroform ug/L NDND
Chloromethane ug/L NDND
cis-1,2-Dichloroethene ug/L NDND
cis-1,3-Dichloropropene ug/L NDND
Dibromochloromethane ug/L NDND
Dibromomethane ug/L NDND
Dichlorodifluoromethane ug/L NDND
Diisopropyl ether ug/L NDND
Ethylbenzene ug/L .61JND
Hexachloro-1,3-butadiene ug/L NDND
Isopropylbenzene (Cumene)ug/L 7.6
m&p-Xylene ug/L 46.2 1539.8
Methyl-tert-butyl ether ug/L 1.1ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 62 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92557149
LOADING RACK
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92557043001
3373521SAMPLE DUPLICATE:
Methylene Chloride ug/L NDND
n-Butylbenzene ug/L 2.7 D6411.8
n-Propylbenzene ug/L 10.8 810
Naphthalene ug/L 42.1 141.7
o-Xylene ug/L 3.6 133.1
p-Isopropyltoluene ug/L .91JND
sec-Butylbenzene ug/L NDND
Styrene ug/L NDND
Tetrachloroethene ug/L NDND
Toluene ug/L .62JND
trans-1,2-Dichloroethene ug/L NDND
trans-1,3-Dichloropropene ug/L NDND
Trichloroethene ug/L NDND
Trichlorofluoromethane ug/L NDND
Vinyl acetate ug/L NDND
Vinyl chloride ug/L NDND
Xylene (Total)ug/L 49.8 1543.0
1,2-Dichloroethane-d4 (S)%106103
4-Bromofluorobenzene (S)%10199
Toluene-d8 (S)%101104
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
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[phone]
Page 63 of 69
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92557149
LOADING RACK
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Common Laboratory Contaminant.C9
The precision between the sample and sample duplicate exceeded laboratory control limits.D6
Results are from sample aliquot taken from VOA vial with headspace (air bubble greater than 6 mm diameter).HS
This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be
considered an estimated value.IL
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
The RPD value in one of the constituent analytes was outside the control limits.RS
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in theassociated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 64 of 69
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92557149
LOADING RACK
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92557149001 642624ADW-1 EPA 8260D
92557149002 642624AMW-1 EPA 8260D
92557149003 642588AMW-2 EPA 8260D
92557149004 642624AMW-3 EPA 8260D
92557149005 642588AMW-4 EPA 8260D
92557149006 642588AMW-5 EPA 8260D
92557149007 642586KDW-1 EPA 8260D
92557149008 642586KMW-1 EPA 8260D
92557149009 642588KMW-3 EPA 8260D
92557149010 642586KMW-5 EPA 8260D
92557149011 642588KMW-6 EPA 8260D
92557149012 642588KMW-7 EPA 8260D
92557149013 642882KMW-8 EPA 8260D
92557149014 642586KMW-9R EPA 8260D
92557149015 642882KMW-12 EPA 8260D
92557149016 642882KMW-13 EPA 8260D
92557149017 642882KMW-14 EPA 8260D
92557149018 642882KMW-18 EPA 8260D
92557149019 642586TRIP BLANK EPA 8260D
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/14/2021 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 65 of 69
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Appendix E

Mann-Kendall Trend Analyses

BENZENE

NAPHTHALENE

TOTAL XYLENES