WI-8217_43197_CA_CLO_20191202_IAR

WithersRavenel
Our People. Your Success.

115 MacKenan Drive | Cary, NC 27511 
t: 919.469.3340 | f: 919.467.6008 | www.withersravenel.com | License No. C‐0832 
Cary | Greensboro | Pittsboro | Raleigh | Wilmington 
December 2, 2019  State of North Carolina 
Department of Environmental Quality 
Division of Waste Management ‐ Underground Storage Tank Section 
1646 Mail Service Center 
Raleigh, NC 27699‐1646  Attn: Ms. Andria Merritt  RE: UST CLOSURE REPORT 
Midway Kwik Stop 
Three 6,000 Gallon Gasoline USTs & One 6,000 Gallon Diesel UST,  
One 3,000 Gallon Diesel UST & One 8,000 Gallon Diesel UST 
4505 North College Road  
Castle Hayne, New Hanover County, North Carolina 
Facility ID Number: 0‐0‐2529 
NCDEQ‐DWM Incident Number: Unassigned 
WR Project Number: 02180080.10  
Ms. Merritt:  
WithersRavenel (WR) has completed underground storage tank (UST) closures as documented within 
the enclosed UST Closure Report for the above referenced site.  This report documents activities 
conducted at the facility in association with NCDEQ Contract # NTK041318 under task authorizations 
issued by NCDEQ on September 20, 2019 and October 3, 2019.    Based upon the concentration of Total Petroleum Hydrocarbon – Diesel Range Organics in four of the 
closure soil samples, and TPH – Gasoline Range Organics in one of those samples, a release was 
identified in association with the UST system.  Due to the presence of shallow groundwater at the site, 
one monitoring well was installed in the excavation from which two diesel fuel USTs were removed, 
and a second monitoring well was installed in the excavation where three gasoline USTs and one diesel 
fuel UST were removed.     Analytical results for the groundwater samples obtained from these monitoring wells indicated the 
presence of detectable concentrations of several petroleum compounds and total lead.  The 
concentrations of petroleum related constituents and lead did not exceed their respective North 
Carolina Groundwater Standards in the groundwater sample obtained from the well installed in the 
diesel fuel UST excavation.  However, concentrations of three petroleum‐related constituents detected 
in the groundwater sample from the other UST excavation exceeded their respective NC Groundwater 
Standards.  
WR appreciates the opportunity to be of service to NCDEQ.  Should you have any questions regarding 
the attached, please contact Brian Bellis at 919‐469‐3340.  Sincerely, 
WithersRavenel

Kevin Buchanan     Brian Bellis, P.G. 
Staff Environmental Scientist II    Senior Hydrogeologist

Table of Contents
1. Site History and Characterization ........................................................................................... 1 
1.1. UST Owner and Operator Information ..................................................................................... 1 
1.2. Historical & Surrounding UST Information .............................................................................. 1 
1.3. Non‐UST Information .................................................................................................................... 2 
1.4. Description of Release / Offsite UST Releases ....................................................................... 2 
1.5. Site Characteristics and Surrounding Property ....................................................................... 3 
1.6. Initial Abatement Actions and Assessment Activities Performed to Date ....................... 3 
2. UST Closure Activities ............................................................................................................... 4 
2.1. Preparations for ust Closures ...................................................................................................... 4 
2.2. UST Closure Procedures ............................................................................................................... 4 
2.3. Tank Residuals, UST Disposal ..................................................................................................... 6 
2.4. Initial Response Actions ................................................................................................................ 6 
3. Site Investigation ........................................................................................................................ 7 
3.1. Field Screening Techniques ......................................................................................................... 7 
3.2. Soil Sampling Procedures ............................................................................................................. 7 
3.3. Groundwater Sampling Procedures ........................................................................................... 7 
3.4. Quality Control Measures ............................................................................................................ 8 
3.5 Investigative Results ...................................................................................................................... 8 
4. Conclusions and Recommendations..................................................................................... 11 

FIGURES  
Figure 1 General Location Map 
Figure 2 Site Map 
Figure 3 Closure Sample Locations and Analytical Results 
Figure 4 Groundwater Analytical Results 

TABLES  
B‐1 Site History: UST/AST System & Other Release Information 
B‐3 Summary of Soil Analytical Results 
B‐4 Summary of Groundwater Analytical Results 
B‐7 Monitoring & Remediation Well Construction Information 
APPENDICES  
Appendix A Site Photographs 
Appendix B Liquid Waste Disposal Manifest 
Appendix C UST Disposal Manifest 
Appendix D Laboratory Analytical Reports & Chain‐Of‐Custody Records 
Appendix E Well Construction Records 
Appendix F 
 UST 2A Form (Site Investigation for Registered USTs) and  
UST‐61 (24‐Hour Release and UST Leak Reporting Form) 
Appendix G UST‐3 Form (Notice of Intent: UST Permanent Closure or Change‐in‐Service) 

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1. SITE HISTORY AND CHARACTERIZATION

1.1. UST OWNER AND OPERATOR INFORMATION

The abatement action activities described in this report were conducted in association 
with NCDEQ under the guidance of the NCDEQ UST Section.  The UST systems were 
owned and operated by Midway Kwik Stop, LLC and Mohammed & Michelle Khalil.  
The systems were reportedly damaged during Hurricane Florence in September 2018 
and NCDEQ subsequently authorized removal of these systems under the UST 
Section’s Abandoned Tank Program.   
The UST systems removed from the location on October 22 and 23, 2019 included 
three 6,000‐gallon (gal) gasoline tanks, a 6,000‐gal diesel fuel UST, a 3,000‐gal diesel 
fuel UST, and one 8,000‐gal diesel fuel UST.   These USTs were last operated on 
September 12, 2018 after which they were temporarily closed.   
An approximately 500‐gallon aboveground storage tank (AST) that stores off‐road 
diesel fuel and associated fuel dispenser are located adjacent to the northern wall of 
the convenience store.  The AST is equipped with secondary containment and is still in 
use.  Table B‐1 provides additional information regarding the UST and AST systems at 
the site. 
The site is located in a rural and residential area in Castle Hayne, New Hanover County 
NC.  The street address for the site is 4505 North College Road, which is also known 
as Highway 117 (Figure 1).  The site is currently owned by Mohammed and Michelle 
Khalil of Leland NC and operates as a convenience store and U‐Haul trailer rental 
business.   
Site photographs taken during UST closure activities are included in Appendix A.   

1.2. HISTORICAL & SURROUNDING UST INFORMATION

The Midway Kwik Stop previously sold gasoline and diesel fuel stored in six registered 
USTs and nine associated fuel dispensers.  The USTs were last used on the day prior 
to the arrival of Hurricane Florence in September 2018, and were temporarily closed 
on September 12, 2018. The locations of these six USTs and other site features are 
depicted on Figure 2.   
During the site visit on September 20, 2019 WR identified the locations of three 6,000‐
gallon capacity gasoline USTs, a 6,000‐gallon capacity diesel fuel UST, an 8,000‐gallon 
capacity diesel fuel UST, and a 3,000 gallon off‐road diesel fuel UST, all of which are 
situated to the north of the convenience store.  The USTs were connected to nine fuel 
dispensers; five of which were located in front of (to the east of) the convenience store, 
the remaining four were located in the northern portion of the site.   

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Presently, an approximately 550 gallon aboveground diesel fuel storage (AST) and fuel 
dispenser are located adjacent to the north side of the convenience store building.  The 
AST is currently active and in regular use.  The six metal vent pipes for the USTs were 
located together in the northern portion of the site next to one of the stand‐alone 
diesel fuel pumps.   

1.3. NON-UST INFORMATION

As mentioned previously, an active AST is in use on the subject property.  The AST is 
equipped with secondary containment and stores off‐road diesel fuel that is dispensed 
by an attached fuel pump.  The northern portion of the property is used for the storage 
of U‐Haul trailers.   

1.4. DESCRIPTION OF RELEASE / OFFSITE UST RELEASES

Analytical results for soil samples submitted for mobile laboratory analysis of TPH as 
gasoline range organics (GRO) and diesel range organics (DRO) showed GRO and/or 
DRO at concentrations in excess of the laboratory method detection limit (MDL) in the 
majority of soil samples tested (see Table B‐3).  However, concentrations of TPH in 
these samples were below the NCDEQ Action Levels for GRO or DRO in all but one 
case.  The soil sample from beneath one of the northern gasoline fuel pumps (FP‐2) 
exhibited TPH‐DRO and GRO concentrations that exceeded the current NCDEQ 
Action Levels.  These results were confirmed by TPH analyses of a split sample from 
FP‐2 conducted by Pace Analytical Services (Pace).  Analytical results for three other 
spilt soil samples submitted to Pace (FP‐1, FP‐4 and FL‐1) indicated the presence of 
TPH‐DRO at concentrations that exceeded the 100 mg/Kg Action Level.  None of the 
other soil samples from beneath fuel lines, fuel pumps or from the sidewalls of the UST 
excavation exhibited TPH‐DRO or GRO concentrations that exceeded their respective 
action levels (see Table B‐3 and Figure 3).   Laboratory reports for these analyses are 
included in Appendix D. 

Analytical results for the groundwater samples obtained from monitoring wells MW‐1 
and MW‐2 are summarized in Table B‐4 and Figure 4.  Monitoring well construction 
details are summarized in Table B‐7, and on the Well Construction Records contained 
in Appendix E.  Analytical results for the groundwater samples obtained from these 
monitoring wells indicated the presence of detectable concentrations of several 
petroleum compounds and total lead.  The concentrations of petroleum related 
constituents and lead did not exceed their respective North Carolina Groundwater 
Standards in the groundwater sample obtained from the well installed in the diesel fuel 
UST excavation (MW‐1).  However, concentrations of three petroleum‐related 
constituents detected in the groundwater sample from the other UST excavation 
(MW‐2) exceeded their respective NC Groundwater Standards.  

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1.5. SITE CHARACTERISTICS AND SURROUNDING PROPERTY
The site is located in a rural and residential area on the western side of Highway 117 
(North College Road) in the town of Castle Hayne, which is in northern New Hanover 
County.  Adjacent properties are undeveloped although residential properties are 
located to further to the north, east and south.  An unnamed tributary to Prince George 
Creek is located to the west of the site (see Figure 1). Site features, structures and the 
locations of the former UST systems are depicted on Figure 2.   
Properties surrounding the subject site are unoccupied and obvious signs of off‐site 
sources of petroleum or drinking water wells were not noted. 

1.6. INITIAL ABATEMENT ACTIONS AND ASSESSMENT
ACTIVITIES PERFORMED TO DATE
No initial abatement, assessment or corrective action activities have been performed 
at the site, to date, with the exception of those described herein.  The UST closure 
assessment activities conducted during October 2019 are described in Sections 2 and 
3 of this report.  No reports relating to environmental conditions on the property are 
known to have been submitted to NCDEQ or provided to WR by NCDEQ.   

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2. UST CLOSURE ACTIVITIES

2.1. PREPARATIONS FOR UST CLOSURES

 WR submitted the required GW/UST‐3 (Notice of Intent: UST Permanent Closure or 
Change‐in‐Service) form to NCDEQ on October 8, 2019.     Ready Contractors of Wilson, NC (Ready) obtained the requisite permission to remove 
the USTs from Mr. Tom Sosebee, Senior Code Compliance Official (Fire Reviews) of 
the New Hanover County Building Safety unit during closure activities on October 22 
and 23, 2019.  Approval for UST removals was given following testing of the oxygen 
and lower explosive limits of the atmosphere within each tank.    
 Residual fluids contained in the USTs were removed using a vacuum equipped tanker 
truck prior to removal of the USTs.  A combined total of 1,000‐gal of liquids were 
removed from the USTs.  These residuals were disposed of at Eastern Environmental 
Management’s permitted facility located in Rocky Mount, NC.  (see Appendix B for a 
copy of the disposal manifest).     Concrete pavement and soil were excavated from above and around the USTs to 
expose the tops of the tanks and allow for their removals.  Soils excavated to remove 
the USTs were stock piled and samples of these soils were brought to the on‐site 
laboratory operated by RedLab where they were tested for TPH‐DRO and GRO by the 
ultraviolet fluorescence (UVF) method.  Analytical results for 12 samples of these soils 
are summarized in Table B‐3 and the laboratory report is included in Appendix D. None 
of these soil samples exhibited TPH DRO or GRO concentrations that exceeded the 
current NCDEQ action levels, therefore they were used to help backfill the excavations 
following removal of the USTs.     
 Purging of vapors and reduction of oxygen content within the USTs was accomplished 
using compressed carbon dioxide gas.  Under supervision of the New Hanover County 
Building Safety Unit, the O2/LEL levels within each tank were measured prior to their 
removal, and extraction of the tanks was not performed prior to receiving approval 
from that official.   

2.2. UST CLOSURE PROCEDURES

Ready first removed concrete overlying the tanks to expose fill materials covering the 
USTs.  For the purposes of tank removals, only those soils necessary to facilitate the 
removal of the tanks were excavated from the side and end walls of the USTs.  Fill soils 
above the USTs were comprised of sand and did not emit petroleum odors.  The natural 
soils in the vicinity of the USTs were noted to be gray and tan sandy sediments.   

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Ready removed the 8,000‐gallon diesel UST and the 3,000‐gallon diesel UST from the 
northern excavation on October 22, 2019. Groundwater entered the excavation at a 
depth of approximately 6 feet below ground and caused the USTs to rise after the 
overlying concrete and soils were removed.  Due to the presence of groundwater in 
the excavation, WR instructed Ready to collect eight sample of soil at depths of 
approximately five feet from the sidewalls of the excavations (soil samples SW‐1 
through SW‐8) using the bucket of the excavator.  These soil samples were tested on‐
site by RedLab and the analysis results did not identify TPH GRO or DRO 
concentrations that exceeded NCDEQ Action Levels.  Splits of these samples were also 
submitted to Pace for analysis of TPH DRO and GRO and similar results were obtained 
(see Table B‐3 and Appendix D). 

On October 23, 2019 Ready uncovered and removed the three 6,000‐gallon gasoline 
USTs and remaining 6,000‐gallon diesel fuel UST.  Groundwater entered this second 
excavation as well at a depth of approximately six feet below ground.  Therefore, WR 
directed Ready to collect soil samples from the sidewalls of the excavation at depths 
of approximately five feet.  These samples (soil samples SW‐9 through SW‐18) were 
submitted to Pace for analysis TPH DRO and GRO.  The results of these analyses did 
not reveal concentrations that exceeded NCDEQ Action Levels (see Table B‐3 and 
Appendix D).   

On October 23, 2019 and as the UST excavations were being backfilled, one of WR’s 
NC Certified Well Contractors installed groundwater monitoring well MW‐1 within the 
northwestern corner of the northern UST excavation as it was being backfilled with 
clean sand and crushed stone.  Similarly, MW‐2 was installed in the northwestern 
corner of the southern UST excavation.  The approximate location of these monitoring 
wells are shown on Figure 4.  Groundwater samples were obtained from monitoring 
wells MW‐1 and MW‐2 on October 30, 2019 and were submitted to Pace Analytical 
Services for testing of gasoline and diesel fuel constituents specified in the UST Section 
Guidelines.   

Analytical results for the groundwater samples obtained from these monitoring wells 
indicated the presence of detectable concentrations of several petroleum compounds 
and total lead.  The concentrations of petroleum related constituents and lead did not 
exceed their respective North Carolina Groundwater Standards in the groundwater 
sample obtained from the well installed in the diesel fuel UST excavation (MW‐1).  
However, concentrations of three petroleum‐related constituents detected in the 
groundwater sample from the other UST excavation (MW‐2) exceeded their respective 
NC Groundwater Standards. 

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The tanks were extracted using a trackhoe.  The condition of each tank upon removal 
from the subsurface if shown below: 

UST ID Volume (gal) Use Condition
1 6,000 Gasoline Good.  No corrosion,pitting, or obvious leak points
2 6,000 Gasoline Good.  No corrosion,pitting, or obvious leak points
3 6,000 Gasoline Good.  No corrosion,pitting, or obvious leak points
4 6,000 Diesel Fuel Good.  No corrosion,pitting, or obvious leak points
5 3,000 Diesel Fuel Good.  No corrosion,pitting, or obvious leak points
6 8,000 Diesel Fuel Good.  No corrosion,pitting, or obvious leak points

All six USTs were removed from the site on October 23, 2019 were transported to the 
Foss Recycling facility in Wilson, NC for disposal.  Acceptance receipts for the USTs 
are included in Appendix C.   The UST excavation areas are illustrated on Figure 3.   

In association with closure of the USTs WR obtained soil samples FP‐1 through FP‐9 
from beneath each former fuel pump, following their removal by Ready.  Similarly, eight 
samples of natural soils (FL‐1 through FL‐8) were obtained at 10 foot intervals from 
beneath the fuel lines leading from the USTs to the fuel pumps.  All of these samples 
were submitted to Pace for analysis of TPH DRO and GRO.  The locations of the 
samples are shown on Figure 3.  Concentrations of TPH DRO exceeded 100 mg/Kg at 
four of these locations, and a concentration of TPH GRO detected in one of the 
samples exceeded 50 mg/Kg.  Analytical results for these samples are discussed further 
in Section 3.5.1.   

As no heavily impacted soils were identified through the closure of the USTs, no 
additional soils beyond those necessary to facilitate UST closures were excavated from 
the location.     

2.3. TANK RESIDUALS, UST DISPOSAL
Information described in Section 2.1 and 2.2. 

2.4. INITIAL RESPONSE ACTIONS

WR completed and submitted a NCDEQ UST‐61 Form to document the discovery of 
the release on the property.  This form was submitted to NCDEQ on November 6, 
2019.   

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3. SITE INVESTIGATION

3.1. FIELD SCREENING TECHNIQUES

WR physically monitored the excavation of soil by randomly screening the soils as they 
were excavated.  The samples were placed in clean, zip‐lock bags and screened with a 
RAE Systems® MiniRAE 3000™ PID for the presence of volatile vapors typical of 
petroleum hydrocarbons.  The PID is an industry accepted screening device used to 
detect the presence of volatile organic vapors, but is not relied upon to determine 
specific levels of contamination.   

3.2. SOIL SAMPLING PROCEDURES

In accordance with NCDEQ guidance for the closure of commercial UST systems, WR 
obtained the requisite number of soil samples from no more than 2 feet beneath the 
former base of each pump location (FP‐1 through FP‐9), and from approximately less 
than 2 feet beneath the former fuel line locations (FL‐1 through FL‐9).  Soil samples 
collected for closure of the UST systems were obtained from the sidewalls of the 
excavation associated with the removal of the tanks, at locations above the level of 
groundwater within the excavations.  The number of samples obtained beneath each 
pump, fuel line, and along excavation sidewalls, was based on NCDEQ sampling 
guidance for commercial UST systems.   

All soil samples were collected either from the bucket of the tracked excavator or 
through the use of a properly decontaminated hand auger, field screened, and placed 
in laboratory prepared containers including chemical preservatives, if required by 
laboratory methods. WR personnel donned clean nitrile sampling gloves for each 
sample location.  Following collection, the soil samples were placed on ice in a cooler, 
which was subsequently transported via FedEx under chain of custody to Pace where 
they were analyzed for TPH DRO and GRO.    

3.3. GROUNDWATER SAMPLING PROCEDURES

The approximate locations of permanent monitoring wells MW‐1 and MW‐2 are 
shown on Figure 4.  Both wells consist of a five‐foot length of 2‐inch diameter PVC 
well screen with 0.010‐inch slots.  The material used to backfill the bottom portion of 
the excavations was clean medium grained sand, which made installation of a sand 
pack around the screen unnecessary.    The top of each well is equipped with a locking 
cap and is surrounded by a cast iron flush mounted protective cover set in concrete.  
Photographs of the wells are included in Appendix A, and well construction records 
for each well are included in Appendix E. 

MW‐1 and MW‐2 were installed in UST excavations as they were being backfilled.  
Each well was purged and sampled using a new dedicated and disposable polyethylene 

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bailer.  The groundwater samples were decanted into appropriate sample containers 
provided by Pace Analytical Services and were shipped via FedEx under chain of 
custody to their fixed laboratory in Mr. Juliet TN for analysis.     

Both groundwater samples were analyzed for: volatile petroleum hydrocarbons by 
Method MADEP‐VPH, VOCs by Standard Method (SM) 6200B, extractable petroleum 
hydrocarbons by Method MADEP‐EPH, Semi‐VOCs by EPA Method 625.1, and total 
lead by SM 6010C.  A copy of the chain of custody is included with the Pace laboratory 
report in Appendix D.  Analytical results for these samples are discussed in Section 
3.5.2.   

3.4. QUALITY CONTROL MEASURES

Quality control measures were employed during this project and included use of clean 
sampling tools, laboratory prepared sample bottle kits, calibrated field instruments, 
donning of clean sample gloves during each sample collection and preparation effort, 
and a use of third‐party laboratories for analysis of soil and groundwater samples 
obtained in association with completion of this project.   

3.5 INVESTIGATIVE RESULTS

3.5.1 Results of Soil Sampling 

Northern UST Excavation 

Analytical results for soil samples collected from the sidewalls of the diesel fuel UST 
excavation (sample ID’s SW‐1 through SW‐8) were submitted to the on‐site laboratory 
operated by RedLab where they were analyzed for TPH GRO and DRO.  These results 
of these analyses are included in Table B‐3 and are shown by location in Figure 3.  
None of the reported TPH concentrations exceeded the 50 mg/Kg Action Level for 
TPH GRO or the 100 mg/Kg Action Level for TPH DRO.  Analysis of split soil samples 
from these locations by Pace confirmed these initial results. 

Soil samples were also obtained from beneath the four former fuel pump locations 
(sample ID’s FP‐1 through FP‐4) located in the vicinity of the diesel fuel UST 
excavation.  Each of these samples was obtained at depths less than two feet below 
the fuel pump piping.  These samples were also submitted to the on‐site laboratory for 
analysis of TPH DRO and GRO.  The on‐site lab identified concentrations of TPH DRO 
and GRO that exceeded current action levels in sample FP‐2, but not in the remaining 
samples (see Table B‐3 and Figure 3).  The results of analyses performed by Pace also 
indicated the presence of TPH DRO and GRO concentrations in excess of the action 
levels in sample FP‐2, and also identified concentrations of TPH DRO that exceeded 
100 mg/Kg in samples FP‐1, and FP‐4, and in the sample FL‐1, which lead to fuel pump  

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number 1, located near the north western corner of the excavation.  Following receipt 
of the analytical report from Pace, WR prepared and submitted a UST‐61 form to the 
NCDEQ Wilmington Regional office to report the release.  A copy of this form is 
included in Appendix F. 

Southern UST Excavation 

Analytical results for the ten soil samples collected from the sidewalls of the southern 
UST excavation (samples SW‐9 through SW‐18) were submitted to Pace where they 
were analyzed for TPH DRO and GRO.  Detectable concentrations of TPH DRO and 
GRO were identified in all of these two samples, however, the reported concentrations 
the current action levels for TPH DRO and GRO.  Similarly, soil samples obtained 
beneath the five fuel pumps connected to the former USTs in the southern excavation 
(samples FP‐5 through FP‐9) and their associated fuel lines (FP‐5 through FP‐8) 
showed detectable concentrations of TPH DRO and GRO.  However, none of the 
detected concentrations exceeded the current action levels.  These results are shown 
by sample location on Figure 3 and included in Table B‐3.  The laboratory report 
associated with these samples is included in Appendix D.   

3.5.2 Groundwater Results – MW‐1 

Analytical results for sample obtained from monitoring well MW‐1 showed the 
following: 

SM 6200B – A detectable concentration of naphthalene was identified in the sample 
from MW‐1, however the concentration was below the NC Groundwater Standard for 
that compound.    

EPA Method 625 – A detectable concentration of phenol was identified in the sample 
from MW‐1, however the concentration was below the NC Groundwater Standard for 
that compound.   

MADEP‐VPH/EPH – No C5‐C8 or C9‐C18 aliphatic hydrocarbons were reported in the 
sample from MW‐1 at concentrations exceeding the laboratory method detection limit 
(MDL). Detectable concentrations of C19‐C36 Aliphatics and C9‐C22 Aromatics were 
identified in the sample from MW‐1, however the reported concentrations were below 
the respective NC Groundwater Standard for those hydrocarbon chains.     

SM 6010C – A detectable concentration of total lead was identified in the sample from 
MW‐1, however the concentration was below the NC Groundwater Standard for the 
element.  

Analytical results for the sample are shown on Figure 4 and are included in Table B‐4.  
The laboratory report and chain‐of‐custody associated with these samples are included 
in Appendix D.   

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3.5.3 Groundwater Results – MW‐2 

Analytical results for sample obtained from monitoring well MW‐2 showed the 
following: 

SM 6200B – Low concentrations of several volatile organic compounds as reported by 
Standard Method 6200B were identified in the groundwater sample obtained from 
monitoring well MW‐2.  However, only the reported concentration for benzene 
exceeded its NC Groundwater Standard (see Table B‐4). 

EPA Method 625 – Low concentrations of two semi‐volatile organic compounds as 
reported by EPA Method 625 were identified in the groundwater sample obtained 
from monitoring well MW‐2.  However, neither of the reported concentrations 
exceeded the respective North Carolina Groundwater Standards for those compounds 
(see Table B‐4). 

MADEP‐VPH/EPH – Concentrations of C5‐C8, C9‐C18, and C19‐C36 aliphatic 
hydrocarbons  reported for the groundwater sample from MW‐2 did not exceed their 
respective NC Groundwater Standards.  However, the concentration of C9‐C22 
aromatic hydrocarbons in the groundwater sample from this location exceeded its NC 
Groundwater Standard (see Table B‐4). 

SM 6010C – The concentration of total lead in the sample from MW‐2 was found to 
exceed its NC Groundwater Standard.  

Analytical results for the sample are shown on Figure 4 and are included in Table B‐4.  
The laboratory report and chain‐of‐custody associated with these samples are included 
in Appendix D.   

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4. CONCLUSIONS AND RECOMMENDATIONS

WR completed the closure of six registered USTs and associated fuel lines and dispensers 
on October 23, 2019.  Conclusions regarding these UST closures and the results of 
laboratory testing of samples include the following: 

 Six registered USTs were removed from the subsurface of the site on October 22 and 
23, 2019.  Each of these tanks were found to be in good condition with no pitting, 
corrosion or obvious signs of leaks observed on their exterior surfaces.  

 Approximately 1,000 gallons of residual fluid was removed from the tanks prior to their 
closure.  These liquids were transported and disposed of at EEM’s permitted facility in 
Rocky Mount, NC. 

 Three soil samples obtained from beneath former fuel pumps FP‐1, FP‐2 and FP‐4, and 
beneath one of the fuel lines (FL‐1) exhibited a TPH DRO concentrations that 
exceeded the 100 mg/Kg action level.  The concentration of TPH GRO in the soil 
sample from FP‐1 also exceeded the 50 mg/Kg action level.  The remaining samples 
showed TPH GRO and DRO at concentrations above the laboratory MDL, but beneath 
the NC Action Levels for TPH.   

 Laboratory results for the eight samples obtained from the sidewalls of the northern 
UST excavations exhibited TPH DRO and GRO at concentrations above the laboratory 
MDLs, but below the NC Action Levels for TPH.  

 Laboratory results for the ten samples obtained from the sidewalls of the southern UST 
excavations exhibited TPH DRO and GRO at concentrations above the laboratory 
MDLs, but below the NC Action Levels for TPH. 

 Because groundwater was found to be in contact with the USTs, two permanent 
groundwater monitoring wells were installed by one of WR NC Certified Well 
Contractors in each of the two UST excavations. 

 Results of testing of the groundwater sample from the monitoring well installed in the 
northern UST excavation did not indicate the presence of petroleum‐related 
compounds or lead at concentrations that exceeded NC Groundwater Standards. 

 Results of testing of the groundwater sample from the monitoring well installed in the 
southern UST excavation revealed concentrations of two petroleum related 
compounds and lead at concentrations that exceeded NC Groundwater Standards. 

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WR appreciates the opportunity to be of assistance to the NCDEQ‐DWM, UST Section.  
Should you have any questions or comments regarding this report, please contact Brian 
Bellis at your convenience. 

Sincerely, 
WithersRavenel

Kevin Buchanan     Brian Bellis, P.G. 
Staff Environmental Scientist II    Senior Hydrogeologist 

FIGURES

TABLES

UST IDNumberCurrent/LastContentsPreviousContentsCapacity(in gallons)ConstructionDetailsTankDimensions (diameter x length)Description ofAssociatedPiping & PumpsDate of TankInstallationStatus ofUSTWas release associated with UST System? (Y/N)1Gasoline Not Listed 6,000 Single‐Wall Steel 8' X 16'Single‐Wall FRP  European Suction7/15/1990Permanently Closed by Removal       October 2019N2Gasoline Not Listed 6,000 Single‐Wall Steel 8' X 16'Single‐Wall FRP  European Suction7/15/1990Permanently Closed by Removal       October 2019N3Gasoline Not Listed 6,000 Single‐Wall Steel 8' X 16'Single‐Wall FRP  European Suction7/15/1990Permanently Closed by Removal       October 2019N4Diesel Fuel Not Listed6,000Single‐Wall Steel 8' X 16'Single‐Wall FRP  European Suction7/15/1990Permanently Closed by Removal       October 2019N5Diesel Fuel Not Listed 3,000 Single‐Wall Steel 5.3' X 18'Single‐Wall FRP  European Suction8/26/1993Permanently Closed by Removal       October 2019N6Diesel Fuel Not Listed 8,000 Single‐Wall Steel 8' X 22'Single‐Wall FRP  European Suction8/26/1993Permanently Closed by Removal       October 2019NAST IDNumberCurrent/LastContentsPreviousContentsCapacity(in gallons)ConstructionDetailsTankDimensions (diameter x length) (ft)Description ofAssociatedPiping & PumpsDate of TankInstallationStatus ofASTWas release associated with AST System? (Y/N)1Off‐road diesel Unkown ~500Single‐Wall Steel with secondary containment3.75' x 6'Detached pump connected by steel pipeUnknown ActiveNFacility IDMaterialReleasedDateofReleaseFacility ID #0‐0‐2529 Diesel Fuel UnknownNotes:1)Shallow contaminated soils were identified beneath diesel fuel pump locations FP‐1, FP‐2 and FP‐4, and beneath the fuel line associated with diesel fuel pump FP‐1.Tank installation dates from NCDEQ "tblAllTanks 01‐2015" Excel table.  4505 NORTH COLLEGE ROAD (US HIGHWAY 117)CASTLE HAYNE, NEW HANOVER COUNTY, NC Facility ID #0‐0‐2529Description of ReleaseTable B‐1Site History:  UST/AST System & Other Release InformationMIDWAY KWIK STOPPage 1 of 1
Sample
ID
Date
Collected
Gasoline 
Range 
Organics
Diesel Range 
Organics
Gasoline 
Range 
Organics 
(8015D)
Diesel Range 
Organics 
(8015C)
SP‐1 #1 10/22/2019 4 1.4 NA NA
SP‐1 #2 10/22/2019 4.2 0.6 NA NA
SP‐1 #3 10/22/2019 <0.9 0.9 NA NA
SP‐1 #4 10/22/2019 <0.64 1.6 NA NA
SP‐1 #5 10/22/2019 7.4 0.78 NA NAFP‐1 10/22/2019 1.7 2 3.6 168
FP‐2 10/22/2019 2757 21408 140 20500
FP‐3 10/22/2019 <1.4 4.1 1.41 12.6
FP‐4 10/22/2019 18 8.3 2.04 506
SP‐2 #1 10/22/2019 <0.33 1.3 NA NA
SP‐2 #2 10/22/2019 <0.72 3.4 NA NA
SP‐3 #1 10/22/2019 <0.91 5.9 NA NA
SP‐3 #2 10/22/2019 <0.8 1.2 NA NA
SP‐3 #3 10/22/2019 <0.78 1 NA NA
SP‐3 #4 10/22/2019 <0.91 4.8 NA NASP‐3 #5 10/22/2019 <0.95 7.2 NA NA
FL‐1 10/22/2019 5.6 1.2 0.925 164
FL‐2 10/22/2019 2.4 1.8 1.26 4.92
SW‐1 10/22/2019 6.9 2.6 0.841 6.72
SW‐2 10/22/2019 <0.31 0.31 0.936 2.88
SW‐3 10/22/2019 <0.3 0.3 0.597 1.67
SW‐4 10/22/2019 <0.34 <0.34 0.74 4.13
SW‐5 10/22/2019 1.4 0.54 2.64 4.2
SW‐6 10/22/2019 1.1 6 0.741 13.7
SW‐7 10/22/2019 2.4 1.4 0.877 1.5SW‐8 10/22/2019 3.5 0.36 1.73 3
FL‐3 10/22/2019 <0.37 0.45 1.89 8.6
FL‐4 10/22/2019 <0.35 <0.35 2.31 4.15
SW‐9 10/23/2019 NA NA 3.62 1.27
SW‐10 10/23/2019 NA NA 0.887 4.12
SW‐11 10/23/2019 NA NA 3.08 1.14
SW‐12 10/23/2019 NA NA 1.23 2.48
SW‐13 10/23/2019 NA NA 1.02 4.97
SW‐14 10/23/2019 NA NA 2.98 3.73
SW‐15 10/23/2019 NA NA 0.901 3.45SW‐16 10/23/2019 NA NA 1.13 1.35
SW‐17 10/23/2019 NA NA 1.15 5.62
SW‐18 10/23/2019 NA NA 2.65 4.44
FL‐5 10/23/2019 NA NA 4.26 1.1
FL‐6 10/23/2019 NA NA 2.76 1.06
FL‐7 10/23/2019 NA NA 2.93 1.21
FL‐8 10/23/2019 NA NA 1.06 13.4
FP‐5 10/23/2019 NA NA 2.47 4.78
FP‐6 10/23/2019 NA NA 3.75 93.4
FP‐7 10/23/2019 NA NA 2.11 3.53FP‐8 10/23/2019 NA NA 0.991 3.39FP‐9 10/23/2019 NA NA 0.829 3.48
50 100 50 100
Notes:
1)
2)
3)
4)SP = Sample of excavated soil from Stock Pile
5)FP = Soil sample obtained from under Fuel Pump location
6)FL = Soil samplbe obtained from under Fuel Line location
7)SW = Soil sample obtained from Side Wall of excavation
Result
Result
= Result Exceeds Laboratory Detection Limits
=Result Exceeds NCDEQ Action Level for TPH
Analytical Method TPH (QED) ‐ RedLab
NCDEQ Action Level
TPH (8015) ‐ Pace
QED Ultra Violet Fluorescence analyzer utilized for field analysis of RedLab samples.
8015 Analyses performed by Pace Analytical Services in fixed‐base laboratory
All results provided in mg/kg (milligrams per kilogram) or parts per million
TABLE B‐3
SUMMARY OF SOIL ANALYTICAL RESULTS
MIDWAY KWIK STOP
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CASTLE HAYNE, NEW HANOVER COUNTY, NC
WR Project # 02180080.10
SM6010CLEAD (TOTAL)BENZENEN‐BUTYLBENZENEETHYLBENZENEISOPROPYLBENZENENAPHTHALENEN‐PROPYLBENZENETOLUENE1,2,4‐TRIMETHYLBENZENE1,3,5‐TRIMETHYLBENZENETOTAL XYLENESNAPHTHALENEPHENOLC5‐C8 AliphaticsC9‐C18 AliphaticsC19‐C36 AliphaticsC9‐C22 Aromatics7439‐92‐171‐43‐2 104‐51‐8 100‐41‐498‐82‐891‐20‐3 103‐65‐1 108‐88‐395‐63‐6 108‐67‐891‐20‐3 108‐95‐2‐‐‐ ‐‐‐ ‐‐‐ ‐‐‐MW‐1 10/30/20199.45<1.00 <1.00 <1.00 <1.001.03<1.00 <1.00 <1.00 <1.00 <2.00<1.001.76<100 <10083.5 53.9MW‐2 10/30/201937.9 2.42 0.462 0.57 0.674 1.85 1.15 2.21 18.4 6.77 43.30.755 3.75 118 393 568 25415170 600 70 670 600 400400 500 6 30 400 700 10000 20015000 5000 6900 84500 25000 15500 30000 258000 28500 25000 85500 15500 300000‐‐‐ ‐‐‐ ‐‐‐ ‐‐‐Notes:1)2)3)4)NLResultResultResult= Result Exceeds NC 2L Standard for Groundwater= Result Exceeds NC Gross Contaminant Level for GroundwaterTABLE B‐4SUMMARY OF GROUNDWATER ANALYTICAL RESULTSMIDWAY KWIK STOP4505 NORTH COLLEGE ROAD (US HIGHWAY 117)CASTLE HAYNE, NEW HANOVER COUNTY, NCWR Project # 02180080.10All results provided in ug/L (micrograms per liter) or parts per billion.Compounds analyzed for by laboratory but not listed were not detected above laboratory detection limits. See the laboratory report included in the Appendix for a full list of constituents. NC 2L Standard ‐ North Carolina Groundwater Quality Standard as per NC Administrative Code 15A NCAC 02L.GCLs for Groundwater = NCDENR UST Section Gross Contamination Levels for Groundwater.NC 2L Standard GCLs for Groundwater= No Regulatory Level Established= Result Exceeds Laboratory Detection LimitsSample IDDateCollectedSM6200BEPA‐625Analytical MethodMADEP‐VPH/EPH
Easting NorthingMW‐110/23/2019 2 8 3 3‐8 NM 10/23/2019 5.20‐‐‐ ‐‐‐2335150.06 214593.35MW‐210/23/2019 2 7 2 2‐7 NM 10/23/2019 5.50‐‐‐ ‐‐‐2335180.15 214560.01Well Casing Diameter(inches)Total Depth     (feet)Well Casing Depth (feet)Screened Interval     (feet)TABLE B‐7MONITORING & REMEDIATION WELL CONSTRUCTION INFORMATIONMIDWAY KWIK STOP4505 NORTH COLLEGE ROAD (US HIGHWAY 117)CASTLE HAYNE, NEW HANOVER COUNTY, NCWR Project # 02180080.10Top‐of‐Casing Elevation       (feet)Date Water Level MeasuredDepth‐to‐Water from Top‐of‐Casing(feet)Free Product Thickness(feet)GroundwaterElevation        (feet)Well Coordinates(NC State Plane NAD 83 Feet)Well ID Date Installed  

APPENDIX A

SITE PHOTOGRAPHS

UST Closure Photo Documentation  October 2019 
Midway Kwik Stop Facility ID #0‐0‐2529  WR Project No. 02180080.10 

Page 1 of 8 

Photo #1:  Ready Contractors crew disassembling three of five fuel dispensers in front of Midway Kwik Stop store 
at 4505 North College Road, Castle Hayne NC. 

Photo #2:  North looking view of fill ports for four 6,000 gallon USTs and associated vent pipes (foreground), and 
locations of former diesel fuel pumps FP‐1, FP‐2, FP‐3 & FP‐4. 
UST Closure Photo Documentation  October 2019 
Midway Kwik Stop Facility ID #0‐0‐2529  WR Project No. 02180080.10 

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Photo #3:  Removal of rain canopy that was damaged by Hurricane Florence in Sept 2018.  The canopy cover diesel 
fuel pumps FP‐2 and FP‐3.  USTs that were connected to these pumps are beneath concrete rubble on right. 

Photo #4: Uncovering 3,000 gallon diesel UST (foreground) and 8,000 gallon diesel UST (background). 
UST Closure Photo Documentation  October 2019 
Midway Kwik Stop Facility ID #0‐0‐2529  WR Project No. 02180080.10 

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Photo #5:  Uncovering four 6,000 gallon USTs.  The three USTs in foreground stored gasoline and the fourth (near 
rubber tired backhoe in background) stored diesel fuel. 

Photo #6:  Vacuum truck used to remove residual fluids from USTs.  Approximately 1,000 gallons of residual fluids 
were removed and disposed at Eastern Environmental Managements treatment facility in Rocky Mount, NC. 
UST Closure Photo Documentation  October 2019 
Midway Kwik Stop Facility ID #0‐0‐2529  WR Project No. 02180080.10 

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Photo #7:  8,000 gallon diesel fuel UST raised by shallow water table after removal of overlying soils and concrete.  

Photo #8:  8,000 gal diesel fuel UST (UST #6) being loaded onto flatbed trailer.  UST #6 was in good condition with 
no obvious pitting, corrosion or holes. 
UST Closure Photo Documentation  October 2019 
Midway Kwik Stop Facility ID #0‐0‐2529  WR Project No. 02180080.10 

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Photo #9:  Removing 3,000 gal diesel fuel UST (UST #5).  Note groundwater entering excavation. 

Photo #10:  UST #5 following removal was in good condition with no obvious corrosion, pitting or holes. 
UST Closure Photo Documentation  October 2019 
Midway Kwik Stop Facility ID #0‐0‐2529  WR Project No. 02180080.10 

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Photo #11: Purging residual vapors from one of the three 6,000 gasoline USTs using compressed carbon dioxide 
gas as New Hanover County fire marshal observes process (right side of photo). 

Photo #12:  Removing one of the four 6,000 gallon USTs.  All four of these USTs (UST #s 1 through 4) were in good 
condition with no obvious signs of pitting, corrosion or holes. 
UST Closure Photo Documentation October 2019 
Midway Kwik Stop Facility ID #0‐0‐2529 WR Project No. 02180080.10 
Photo #13:  Removing 6,000 gal gasoline UST #2. 
Photo #14:  Loading one of the 6,000 gallon USTs on to flatbed trailer.  All of the 6,000 gallon UST were in good 
condition with no signs of corrosion, pitting or holes and were disposed at the Foss Recycling facility in Wilson NC. 
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UST Closure Photo Documentation October 2019 
Midway Kwik Stop Facility ID #0‐0‐2529 WR Project No. 02180080.10 
Photo #15:  Saw cutting concrete overlying fuel lines to pumps FP‐5 through FP‐9 in front of Midway Kwik Stop. 
Photo #16: Excavation to remove fuel lines and pump apparatus in front of store. 
Page 8
UST Closure Photo Documentation October 2019 
Midway Kwik Stop Facility ID #0‐0‐2529 WR Project No. 02180080.10 
Photo #17:  Backfilling the UST excavations.  Vertical white PVC pipes are monitoring wells MW‐1 (foreground) and 
MW‐2 (background) that were installed by one of WR’s NC Certified Well Contractors as required by UST section. 
Photo #18: Backfilling and compacting excavated areas.  Crushed stone was used for the topmost foot of backfill. 
Page 9
UST Closure Photo Documentation October 2019 
Midway Kwik Stop Facility ID #0‐0‐2529 WR Project No. 02180080.10 
Photo #19:  North looking view of backfilled UST area. 
Photo #20:  South looking view of backfilled and compacted excavation area. 
Page 10
UST Closure Photo Documentation October 2019 
Midway Kwik Stop Facility ID #0‐0‐2529 WR Project No. 02180080.10 
Photo #21:  Completed flush‐mounted well head for MW‐1 in northern UST excavation. 
Photo #22:  Completed flush‐mounted well head for MW‐2 installed in southern UST excavation. 
Page 11

APPENDIX B

LIQUID WASTE DISPOSAL MANIFEST

APPENDIX C

CERTIFICATE OF UST DISPOSAL

APPENDIX D

LABORATORY ANALYTICAL REPORTS

Hydrocarbon Analysis ResultsClient:WITHERSRAVENEL, INC.Samples takenTuesday, October 22, 2019Address:Samples extractedTuesday, October 22, 2019Samples analysedTuesday, October 22, 2019Contact:BRIAN BELLISOperatorCAROLINE STEVENSProject:MIDWAY KWIK STOP11F03640MatrixSample IDDilution usedBTEX (C6 - C9)GRO (C5 - C10)DRO (C10 - C35)TPH (C5 - C35)Total Aromatics (C10-C35)16 EPA PAHsBaP HC Fingerprint Match% light % mid% heavys SP-1 #128.6 <0.71 4 1.4 5.4 1.1 <0.23 <0.029 83.2 10.5 6.3V.Deg.PHC 76%,(FCM)s SP-1 #223.9 <0.6 4.2 0.6 4.8 0.34 <0.19 <0.024 93.5 4.5 2Deg.PHC 76.7%,(FCM)s SP-1 #336.0 <0.9 <0.9 0.9 0.9 0.77 <0.29 <0.036 0 68.2 31.8V.Deg.PHC 77.9%,(FCM)s SP-1 #425.6 <0.64 <0.64 1.6 1.6 0.87 <0.2 <0.026 48.5 36.9 14.6Deg.PHC 76.4%,(FCM)s SP-1 #531.4 <0.78 7.4 0.78 8.18 0.5 <0.25 <0.031 94.5 3.8 1.6Deg.PHC 77.7%,(FCM)s FP#132.3 <0.81 1.7 2 3.7 1.3 <0.26 <0.032 61.5 26.2 12.3V.Deg.PHC 74.1%,(FCM)s FP#218710.0 <467.7 2757 21408 24165 3170 <149.7 <18.7 93.1 6.7 0.2Deg.Diesel 82.1%,(FCM)s FP#357.9 <1.4 <1.4 4.1 4.1 0.92 <0.46 <0.058 0 70.2 29.8V.Deg.PHC 78.5%,(FCM)s FP#461.4 <1.5 18 8.3 26.3 4.8 <0.49 <0.061 82.8 11.3 5.9Deg.PHC 74%,(FCM)s SP-2 #113.2 <0.33 <0.33 1.3 1.3 0.7 <0.11 <0.013 0 70.6 29.4V.Deg.PHC 77.4%,(FCM)Initial Calibrator QC checkOKFinal FCM QC CheckOK101.7 %Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone contentFingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate presentRatios
QED Hydrocarbon Fingerprints
Project: MIDWAY KWIK STOP Tuesday, October 22, 2019
Hydrocarbon Analysis ResultsClient:WITHERSRAVENEL, INC.Samples takenTuesday, October 22, 2019Address:Samples extractedTuesday, October 22, 2019Samples analysedTuesday, October 22, 2019Contact:BRIAN BELLISOperatorCAROLINE STEVENSProject:MIDWAY KWIK STOP21F03640MatrixSample IDDilution usedBTEX (C6 - C9)GRO (C5 - C10)DRO (C10 - C35)TPH (C5 - C35)Total Aromatics (C10-C35)16 EPA PAHsBaP HC Fingerprint Match% light % mid% heavys SP-2 #228.8 <0.72 <0.72 3.4 3.4 1.5 <0.23 <0.029 0 72.2 27.8V.Deg.PHC 93.6%,(FCM)s SP-3 #136.4 <1.8 <0.91 5.9 5.9 1.8 <0.29 <0.036 0 74.1 25.9V.Deg.Diesel 85.7%,(FCM)s SP-3 #232.0 <0.8 <0.8 1.2 1.2 0.65 <0.26 <0.032 0 68.2 31.8V.Deg.PHC 90.7%,(FCM)s SP-3 #331.4 <0.78 <0.78 1 1 0.67 <0.25 <0.031 0 67.3 32.7V.Deg.PHC 76.8%,(FCM)s SP-3 #436.4 <0.91 <0.91 4.8 4.8 1.3 <0.29 <0.036 0 72.2 27.8V.Deg.Diesel 80%,(FCM)s SP-3 #538.1 <0.95 <0.95 7.2 7.2 1.6 <0.3 <0.038 0 74.3 25.7V.Deg.Diesel 85%,(FCM)s FL-123.2 <0.58 5.6 1.2 6.8 0.56 <0.19 <0.023 91.9 6.2 1.9Deg.PHC 74.6%,(FCM)s FL-228.3 <0.71 2.4 1.8 4.2 1 <0.23 <0.028 72.8 18.8 8.5Deg.PHC 80.4%,(FCM)s SW-118.9 <0.47 6.9 2.6 9.5 2.6 <0.15 <0.019 82.4 15 2.6Deg Fuel 77.1%,(FCM)s SW-212.3 <0.31 <0.31 0.31 0.31 0.15 <0.1 <0.012 0 68.4 31.6V.Deg.PHC 77.6%,(FCM)Initial Calibrator QC checkOKFinal FCM QC CheckOK96.4 %Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone contentFingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate presentRatios
QED Hydrocarbon Fingerprints
Project: MIDWAY KWIK STOP Tuesday, October 22, 2019
Hydrocarbon Analysis ResultsClient:WITHERSRAVENEL, INC.Samples takenTuesday, October 22, 2019Address:Samples extractedTuesday, October 22, 2019Samples analysedTuesday, October 22, 2019Contact:BRIAN BELLISOperatorCAROLINE STEVENSProject:MIDWAY KWIK STOP8F03640MatrixSample IDDilution usedBTEX (C6 - C9)GRO (C5 - C10)DRO (C10 - C35)TPH (C5 - C35)Total Aromatics (C10-C35)16 EPA PAHsBaP HC Fingerprint Match% light % mid% heavys SW-312.1 <0.3 <0.3 0.3 0.3 0.18 <0.1 <0.012 0 68 32V.Deg.PHC 77.6%,(FCM)s SW-413.5 <0.34 <0.34 <0.34 <0.34 <0.07 <0.11 <0.013 0 88.9 11.1,(FCM)s SW-511.3 <0.28 1.4 0.54 1.94 0.31 <0.09 <0.011 84.3 10.5 5.1Deg.PHC 87.4%,(FCM)s SW-611.3 <0.28 1.1 6 7.1 1.9 <0.09 <0.011 50.4 35.5 14.1V.Deg.Diesel 83.6%,(FCM)s SW-712.4 <0.31 2.4 1.4 3.8 0.87 <0.1 <0.012 75 19.7 5.3Deg.PHC 73%,(FCM)s SW-814.3 <0.36 3.5 0.36 3.86 0.28 <0.11 <0.014 97 2.1 0.9Deg.PHC 76.2%,(FCM)s FL#314.9 <0.37 <0.37 0.45 0.45 0.29 <0.12 <0.015 38.7 39.6 21.7V.Deg.PHC 76.9%,(FCM)s FL#414.0 <0.35 <0.35 <0.35 <0.35 <0.07 <0.11 <0.014 0 0 100,(FCM)Initial Calibrator QC checkOKFinal FCM QC CheckOK97.1 %Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone contentFingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate presentRatios
QED Hydrocarbon Fingerprints
Project: MIDWAY KWIK STOP Tuesday, October 22, 2019
ANALYTICAL REPORT
November 06, 2019
Withers & Ravenel Eng. - Standard
Sample Delivery Group:L1153653
Samples Received:10/24/2019
Project Number:02180080.10
Description:Midway Kwik Mart
Site:0-0-2529
Report To:Brian Bellis
219 Station Road
Suite 101
Wilmington, NC 28405
Entire Report Reviewed By:
November 06, 2019
[Preliminary Report]
Heather J Wagner
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received.
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 08:51 1 of 63
November 06, 2019
Heather J Wagner
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 10:42 1 of 63
TABLE OF CONTENTS ONE LAB. NATIONWIDE.TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 4
Cn: Case Narrative 10
Sr: Sample Results 11
FP-1 L1153653-01 11
FP-2 L1153653-02 12
FP-3 L1153653-03 13
FP-4 L1153653-04 14
FL-1 L1153653-05 15
FL-2 L1153653-06 16
SW-1 L1153653-07 17
SW-2 L1153653-08 18
SW-3 L1153653-09 19
SW-4 L1153653-10 20
SW-5 L1153653-11 21
SW-6 L1153653-12 22
SW-7 L1153653-13 23
SW-8 L1153653-14 24
FL-3 L1153653-15 25
FL-4 L1153653-16 26
SW-9 L1153653-17 27
SW-10 L1153653-18 28
SW-11 L1153653-19 29
SW-12 L1153653-20 30
SW-13 L1153653-21 31
SW-14 L1153653-22 32
SW-15 L1153653-23 33
SW-16 L1153653-24 34
SW-17 L1153653-25 35
SW-18 L1153653-26 36
FL-5 L1153653-27 37
FL-6 L1153653-28 38
FL-7 L1153653-29 39
FL-8 L1153653-30 40
FP-5 L1153653-31 41
FP-6 L1153653-32 42
FP-7 L1153653-33 43
FP-8 L1153653-34 44
FP-9 L1153653-35 45
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 08:51 2 of 63
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.
Qc: Quality Control Summary 46
Total Solids by Method 2540 G-2011 46
Volatile Organic Compounds (GC) by Method 8015D/GRO 51
Semi-Volatile Organic Compounds (GC) by Method 8015C 55
Gl: Glossary of Terms 58
Al: Accreditations & Locations 59
Sc: Sample Chain of Custody 60
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 08:51 3 of 63
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 10:42 3 of 63
ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
FP-1 L1153653-01 Solid Brian Bellis 10/22/19 09:00 10/24/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1372541 1 10/31/19 11:13 10/31/19 11:23 KDW Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG1373171 25 10/22/19 09:00 11/01/19 10:10 ADM Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015C WG1370012 1 10/26/19 17:13 10/27/19 04:52 KME Mt. Juliet, TN
Collected by Collected date/time Received date/time
FP-2 L1153653-02 Solid Brian Bellis 10/22/19 09:05 10/24/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1372541 1 10/31/19 11:13 10/31/19 11:23 KDW Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG1374243 100 10/22/19 09:05 11/03/19 20:02 JAH Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015C WG1370012 100 10/26/19 17:13 10/28/19 15:28 JDG Mt. Juliet, TN
Collected by Collected date/time Received date/time
FP-3 L1153653-03 Solid Brian Bellis 10/22/19 09:10 10/24/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1372541 1 10/31/19 11:13 10/31/19 11:23 KDW Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG1373179 25 10/22/19 09:10 11/01/19 05:42 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015C WG1370013 1 10/26/19 19:20 10/27/19 09:05 KME Mt. Juliet, TN
Collected by Collected date/time Received date/time
FP-4 L1153653-04 Solid Brian Bellis 10/22/19 09:15 10/24/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1372542 1 10/31/19 12:56 10/31/19 13:07 KDW Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG1373179 25 10/22/19 09:15 11/01/19 06:02 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015C WG1370013 5 10/26/19 19:20 10/27/19 10:10 KME Mt. Juliet, TN
Collected by Collected date/time Received date/time
FL-1 L1153653-05 Solid Brian Bellis 10/22/19 12:15 10/24/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1372542 1 10/31/19 12:56 10/31/19 13:07 KDW Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG1373179 25 10/22/19 12:15 11/01/19 06:23 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015C WG1370013 1 10/26/19 19:20 10/27/19 09:18 KME Mt. Juliet, TN
Collected by Collected date/time Received date/time
FL-2 L1153653-06 Solid Brian Bellis 10/22/19 12:20 10/24/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1372542 1 10/31/19 12:56 10/31/19 13:07 KDW Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG1373179 36.3 10/22/19 12:20 11/01/19 06:44 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015C WG1370013 1 10/26/19 19:20 10/27/19 14:34 KME Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 10:42 4 of 63
ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
SW-1 L1153653-07 Solid Brian Bellis 10/22/19 12:35 10/24/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1372542 1 10/31/19 12:56 10/31/19 13:07 KDW Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG1373179 25 10/22/19 12:35 11/01/19 07:04 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015C WG1370013 1 10/26/19 19:20 10/27/19 14:07 KME Mt. Juliet, TN
Collected by Collected date/time Received date/time
SW-2 L1153653-08 Solid Brian Bellis 10/22/19 12:40 10/24/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1372542 1 10/31/19 12:56 10/31/19 13:07 KDW Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG1373179 25 10/22/19 12:40 11/01/19 07:25 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015C WG1370013 1 10/26/19 19:20 10/27/19 07:52 KME Mt. Juliet, TN
Collected by Collected date/time Received date/time
SW-3 L1153653-09 Solid Brian Bellis 10/22/19 13:10 10/24/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1372542 1 10/31/19 12:56 10/31/19 13:07 KDW Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG1373179 25 10/22/19 13:10 11/01/19 07:46 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015C WG1370013 1 10/26/19 19:20 10/27/19 08:06 KME Mt. Juliet, TN
Collected by Collected date/time Received date/time
SW-4 L1153653-10 Solid Brian Bellis 10/22/19 13:05 10/24/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1372542 1 10/31/19 12:56 10/31/19 13:07 KDW Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG1373179 25 10/22/19 13:05 11/01/19 08:06 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015C WG1370013 1 10/26/19 19:20 10/27/19 06:07 KME Mt. Juliet, TN
Collected by Collected date/time Received date/time
SW-5 L1153653-11 Solid Brian Bellis 10/22/19 13:00 10/24/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1372542 1 10/31/19 12:56 10/31/19 13:07 KDW Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG1373179 25 10/22/19 13:00 11/01/19 08:27 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015C WG1370013 1 10/26/19 19:20 10/27/19 08:19 KME Mt. Juliet, TN
Collected by Collected date/time Received date/time
SW-6 L1153653-12 Solid Brian Bellis 10/22/19 12:55 10/24/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1372542 1 10/31/19 12:56 10/31/19 13:07 KDW Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG1373179 25 10/22/19 12:55 11/01/19 08:48 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015C WG1370013 1 10/26/19 19:20 10/27/19 14:21 KME Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 08:51 5 of 63
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 10:42 5 of 63
ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
SW-7 L1153653-13 Solid Brian Bellis 10/22/19 12:50 10/24/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1372542 1 10/31/19 12:56 10/31/19 13:07 KDW Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG1373179 25 10/22/19 12:50 11/01/19 09:09 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015C WG1370013 1 10/26/19 19:20 10/27/19 06:46 KME Mt. Juliet, TN
Collected by Collected date/time Received date/time
SW-8 L1153653-14 Solid Brian Bellis 10/22/19 12:45 10/24/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1372543 1 10/31/19 12:43 10/31/19 12:54 KDW Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG1373179 25 10/22/19 12:45 11/01/19 09:29 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015C WG1370013 1 10/26/19 19:20 10/27/19 14:47 KME Mt. Juliet, TN
Collected by Collected date/time Received date/time
FL-3 L1153653-15 Solid Brian Bellis 10/22/19 13:20 10/24/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1372543 1 10/31/19 12:43 10/31/19 12:54 KDW Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG1373179 25 10/22/19 13:20 11/01/19 09:50 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015C WG1370013 1 10/26/19 19:20 10/27/19 08:52 KME Mt. Juliet, TN
Collected by Collected date/time Received date/time
FL-4 L1153653-16 Solid Brian Bellis 10/22/19 13:30 10/24/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1372543 1 10/31/19 12:43 10/31/19 12:54 KDW Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG1373179 26.5 10/22/19 13:30 11/01/19 10:11 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015C WG1370013 1 10/26/19 19:20 10/27/19 06:20 KME Mt. Juliet, TN
Collected by Collected date/time Received date/time
SW-9 L1153653-17 Solid Brian Bellis 10/23/19 10:00 10/24/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1372543 1 10/31/19 12:43 10/31/19 12:54 KDW Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG1373179 27.5 10/23/19 10:00 11/01/19 10:31 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015C WG1370013 1 10/26/19 19:20 10/27/19 13:54 KME Mt. Juliet, TN
Collected by Collected date/time Received date/time
SW-10 L1153653-18 Solid Brian Bellis 10/23/19 10:05 10/24/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1372543 1 10/31/19 12:43 10/31/19 12:54 KDW Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG1373179 35.8 10/23/19 10:05 11/01/19 10:52 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015C WG1370013 1 10/26/19 19:20 10/27/19 06:33 KME Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 08:51 6 of 63
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 10:42 6 of 63
ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
SW-11 L1153653-19 Solid Brian Bellis 10/23/19 10:10 10/24/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1372543 1 10/31/19 12:43 10/31/19 12:54 KDW Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG1373752 25.5 10/23/19 10:10 11/01/19 23:25 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015C WG1370013 1 10/26/19 19:20 10/27/19 07:26 KME Mt. Juliet, TN
Collected by Collected date/time Received date/time
SW-12 L1153653-20 Solid Brian Bellis 10/23/19 10:15 10/24/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1372543 1 10/31/19 12:43 10/31/19 12:54 KDW Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG1373752 25 10/23/19 10:15 11/01/19 23:46 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015C WG1370013 1 10/26/19 19:20 10/27/19 08:32 KME Mt. Juliet, TN
Collected by Collected date/time Received date/time
SW-13 L1153653-21 Solid Brian Bellis 10/23/19 11:05 10/24/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1372543 1 10/31/19 12:43 10/31/19 12:54 KDW Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG1373752 25 10/23/19 11:05 11/02/19 00:07 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015C WG1370013 1 10/26/19 19:20 10/27/19 09:44 KME Mt. Juliet, TN
Collected by Collected date/time Received date/time
SW-14 L1153653-22 Solid Brian Bellis 10/23/19 11:10 10/24/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1372543 1 10/31/19 12:43 10/31/19 12:54 KDW Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG1373752 25.5 10/23/19 11:10 11/02/19 00:27 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015C WG1370013 1 10/26/19 19:20 10/27/19 07:39 KME Mt. Juliet, TN
Collected by Collected date/time Received date/time
SW-15 L1153653-23 Solid Brian Bellis 10/23/19 11:15 10/24/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1372543 1 10/31/19 12:43 10/31/19 12:54 KDW Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG1373752 25 10/23/19 11:15 11/02/19 00:48 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015C WG1370558 1 10/27/19 22:48 10/28/19 04:37 KME Mt. Juliet, TN
Collected by Collected date/time Received date/time
SW-16 L1153653-24 Solid Brian Bellis 10/23/19 10:30 10/24/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1372545 1 10/31/19 12:32 10/31/19 12:42 KDW Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG1373752 25 10/23/19 10:30 11/02/19 01:09 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015C WG1370558 1 10/27/19 22:48 10/28/19 04:50 KME Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 08:51 7 of 63
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 10:42 7 of 63
ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
SW-17 L1153653-25 Solid Brian Bellis 10/23/19 10:35 10/24/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1372545 1 10/31/19 12:32 10/31/19 12:42 KDW Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG1373752 25 10/23/19 10:35 11/02/19 01:29 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015C WG1370558 1 10/27/19 22:48 10/28/19 05:03 KME Mt. Juliet, TN
Collected by Collected date/time Received date/time
SW-18 L1153653-26 Solid Brian Bellis 10/23/19 10:40 10/24/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1372545 1 10/31/19 12:32 10/31/19 12:42 KDW Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG1373752 29.3 10/23/19 10:40 11/02/19 01:50 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015C WG1370558 1 10/27/19 22:48 10/28/19 05:15 KME Mt. Juliet, TN
Collected by Collected date/time Received date/time
FL-5 L1153653-27 Solid Brian Bellis 10/23/19 12:55 10/24/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1372545 1 10/31/19 12:32 10/31/19 12:42 KDW Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG1373752 29.8 10/23/19 12:55 11/02/19 02:11 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015C WG1370558 1 10/27/19 22:48 10/28/19 05:28 KME Mt. Juliet, TN
Collected by Collected date/time Received date/time
FL-6 L1153653-28 Solid Brian Bellis 10/23/19 13:00 10/24/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1372545 1 10/31/19 12:32 10/31/19 12:42 KDW Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG1373752 29 10/23/19 13:00 11/02/19 02:31 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015C WG1370558 1 10/27/19 22:48 10/28/19 05:41 KME Mt. Juliet, TN
Collected by Collected date/time Received date/time
FL-7 L1153653-29 Solid Brian Bellis 10/23/19 13:05 10/24/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1372545 1 10/31/19 12:32 10/31/19 12:42 KDW Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG1373752 25.8 10/23/19 13:05 11/02/19 02:52 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015C WG1370558 1 10/27/19 22:48 10/28/19 05:53 KME Mt. Juliet, TN
Collected by Collected date/time Received date/time
FL-8 L1153653-30 Solid Brian Bellis 10/23/19 13:10 10/24/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1372545 1 10/31/19 12:32 10/31/19 12:42 KDW Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG1373752 25 10/23/19 13:10 11/02/19 03:13 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015C WG1370558 5 10/27/19 22:48 10/28/19 11:14 KME Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 08:51 8 of 63
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 10:42 8 of 63
ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
FP-5 L1153653-31 Solid Brian Bellis 10/23/19 13:15 10/24/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1372545 1 10/31/19 12:32 10/31/19 12:42 KDW Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG1373752 25 10/23/19 13:15 11/02/19 03:33 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015C WG1370558 1 10/27/19 22:48 10/28/19 06:19 KME Mt. Juliet, TN
Collected by Collected date/time Received date/time
FP-6 L1153653-32 Solid Brian Bellis 10/23/19 13:20 10/24/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1372545 1 10/31/19 12:32 10/31/19 12:42 KDW Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG1373752 28.7 10/23/19 13:20 11/02/19 03:54 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015C WG1370558 1 10/27/19 22:48 10/28/19 06:31 KME Mt. Juliet, TN
Collected by Collected date/time Received date/time
FP-7 L1153653-33 Solid Brian Bellis 10/23/19 13:25 10/24/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1372545 1 10/31/19 12:32 10/31/19 12:42 KDW Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG1373752 25 10/23/19 13:25 11/02/19 04:14 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015C WG1370558 1 10/27/19 22:48 10/28/19 15:16 JDG Mt. Juliet, TN
Collected by Collected date/time Received date/time
FP-8 L1153653-34 Solid Brian Bellis 10/23/19 13:30 10/24/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1372546 1 10/31/19 13:32 10/31/19 13:42 KDW Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG1373752 25 10/23/19 13:30 11/02/19 04:35 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015C WG1370558 1 10/27/19 22:48 10/28/19 06:57 KME Mt. Juliet, TN
Collected by Collected date/time Received date/time
FP-9 L1153653-35 Solid Brian Bellis 10/23/19 13:35 10/24/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1372546 1 10/31/19 13:32 10/31/19 13:42 KDW Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO WG1373752 25 10/23/19 13:35 11/02/19 04:56 DWR Mt. Juliet, TN
Semi-Volatile Organic Compounds (GC) by Method 8015C WG1370558 1 10/27/19 22:48 10/28/19 07:09 KME Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 10:42 9 of 63
ONE LAB. NATIONWIDE.CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Heather J Wagner
Project Manager
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 08:51 10 of 63
Heather J Wagner
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 10:42 10 of 63
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L1153653
FP-1
Collected date/time: 10/22/19 09:00
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 92.7 1 10/31/2019 11:23 WG1372541
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction 3.60 B 0.586 2.70 25 11/01/2019 10:10 WG1373171
(S) a,a,a-Trifluorotoluene(FID) 104 77.0-120 11/01/2019 10:10 WG1373171
Semi-Volatile Organic Compounds (GC) by Method 8015C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 168 0.830 4.32 1 10/27/2019 04:52 WG1370012
(S) o-Terphenyl 60.0 18.0-148 10/27/2019 04:52 WG1370012
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 08:51 11 of 63
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 10:42 11 of 63
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L1153653
FP-2
Collected date/time: 10/22/19 09:05
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 89.9 1 10/31/2019 11:23 WG1372541
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction 140 2.41 11.1 100 11/03/2019 20:02 WG1374243
(S) a,a,a-Trifluorotoluene(FID) 101 77.0-120 11/03/2019 20:02 WG1374243
Semi-Volatile Organic Compounds (GC) by Method 8015C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 20500 85.6 445 100 10/28/2019 15:28 WG1370012
(S) o-Terphenyl 0.000 J7 18.0-148 10/28/2019 15:28 WG1370012
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 08:51 12 of 63
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 10:42 12 of 63
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L1153653
FP-3
Collected date/time: 10/22/19 09:10
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 88.2 1 10/31/2019 11:23 WG1372541
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction 1.41 B J 0.615 2.83 25 11/01/2019 05:42 WG1373179
(S) a,a,a-Trifluorotoluene(FID) 103 77.0-120 11/01/2019 05:42 WG1373179
Semi-Volatile Organic Compounds (GC) by Method 8015C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 12.6 0.872 4.53 1 10/27/2019 09:05 WG1370013
(S) o-Terphenyl 67.0 18.0-148 10/27/2019 09:05 WG1370013
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 08:51 13 of 63
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 10:42 13 of 63
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04
L1153653
FP-4
Collected date/time: 10/22/19 09:15
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 94.8 1 10/31/2019 13:07 WG1372542
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction 2.04 B J 0.573 2.64 25 11/01/2019 06:02 WG1373179
(S) a,a,a-Trifluorotoluene(FID) 101 77.0-120 11/01/2019 06:02 WG1373179
Semi-Volatile Organic Compounds (GC) by Method 8015C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 506 4.06 21.1 5 10/27/2019 10:10 WG1370013
(S) o-Terphenyl 87.0 18.0-148 10/27/2019 10:10 WG1370013
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 08:51 14 of 63
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 10:42 14 of 63
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 05
L1153653
FL-1
Collected date/time: 10/22/19 12:15
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 95.0 1 10/31/2019 13:07 WG1372542
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction 0.925 B J 0.571 2.63 25 11/01/2019 06:23 WG1373179
(S) a,a,a-Trifluorotoluene(FID) 103 77.0-120 11/01/2019 06:23 WG1373179
Semi-Volatile Organic Compounds (GC) by Method 8015C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 164 0.809 4.21 1 10/27/2019 09:18 WG1370013
(S) o-Terphenyl 75.3 18.0-148 10/27/2019 09:18 WG1370013
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 08:51 15 of 63
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 10:42 15 of 63
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 06
L1153653
FL-2
Collected date/time: 10/22/19 12:20
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 85.6 1 10/31/2019 13:07 WG1372542
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction 1.26 B J 0.921 4.24 36.3 11/01/2019 06:44 WG1373179
(S) a,a,a-Trifluorotoluene(FID) 99.2 77.0-120 11/01/2019 06:44 WG1373179
Semi-Volatile Organic Compounds (GC) by Method 8015C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 4.92 0.899 4.68 1 10/27/2019 14:34 WG1370013
(S) o-Terphenyl 44.6 18.0-148 10/27/2019 14:34 WG1370013
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 08:51 16 of 63
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 10:42 16 of 63
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 07
L1153653
SW-1
Collected date/time: 10/22/19 12:35
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 91.7 1 10/31/2019 13:07 WG1372542
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction 0.841 B J 0.592 2.73 25 11/01/2019 07:04 WG1373179
(S) a,a,a-Trifluorotoluene(FID) 99.7 77.0-120 11/01/2019 07:04 WG1373179
Semi-Volatile Organic Compounds (GC) by Method 8015C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 6.72 0.838 4.36 1 10/27/2019 14:07 WG1370013
(S) o-Terphenyl 57.4 18.0-148 10/27/2019 14:07 WG1370013
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 08:51 17 of 63
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 10:42 17 of 63
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 08
L1153653
SW-2
Collected date/time: 10/22/19 12:40
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 95.6 1 10/31/2019 13:07 WG1372542
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction 0.936 B J 0.568 2.61 25 11/01/2019 07:25 WG1373179
(S) a,a,a-Trifluorotoluene(FID) 103 77.0-120 11/01/2019 07:25 WG1373179
Semi-Volatile Organic Compounds (GC) by Method 8015C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 2.88 J 0.804 4.18 1 10/27/2019 07:52 WG1370013
(S) o-Terphenyl 144 18.0-148 10/27/2019 07:52 WG1370013
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 08:51 18 of 63
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 10:42 18 of 63
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 09
L1153653
SW-3
Collected date/time: 10/22/19 13:10
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 94.1 1 10/31/2019 13:07 WG1372542
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction 0.597 B J 0.577 2.66 25 11/01/2019 07:46 WG1373179
(S) a,a,a-Trifluorotoluene(FID) 103 77.0-120 11/01/2019 07:46 WG1373179
Semi-Volatile Organic Compounds (GC) by Method 8015C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 1.67 J 0.817 4.25 1 10/27/2019 08:06 WG1370013
(S) o-Terphenyl 73.2 18.0-148 10/27/2019 08:06 WG1370013
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 08:51 19 of 63
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 10:42 19 of 63
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 10
L1153653
SW-4
Collected date/time: 10/22/19 13:05
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 96.9 1 10/31/2019 13:07 WG1372542
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction 0.740 B J 0.560 2.58 25 11/01/2019 08:06 WG1373179
(S) a,a,a-Trifluorotoluene(FID) 97.2 77.0-120 11/01/2019 08:06 WG1373179
Semi-Volatile Organic Compounds (GC) by Method 8015C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) High Fraction U 0.794 4.13 1 10/27/2019 06:07 WG1370013
(S) o-Terphenyl 88.1 18.0-148 10/27/2019 06:07 WG1370013
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 08:51 20 of 63
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 10:42 20 of 63
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 11
L1153653
SW-5
Collected date/time: 10/22/19 13:00
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 94.7 1 10/31/2019 13:07 WG1372542
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction U 0.573 2.64 25 11/01/2019 08:27 WG1373179
(S) a,a,a-Trifluorotoluene(FID) 97.9 77.0-120 11/01/2019 08:27 WG1373179
Semi-Volatile Organic Compounds (GC) by Method 8015C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 4.20 J 0.812 4.22 1 10/27/2019 08:19 WG1370013
(S) o-Terphenyl 83.8 18.0-148 10/27/2019 08:19 WG1370013
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 08:51 21 of 63
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 10:42 21 of 63
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 12
L1153653
SW-6
Collected date/time: 10/22/19 12:55
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 91.0 1 10/31/2019 13:07 WG1372542
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction 0.741 B J 0.597 2.75 25 11/01/2019 08:48 WG1373179
(S) a,a,a-Trifluorotoluene(FID) 103 77.0-120 11/01/2019 08:48 WG1373179
Semi-Volatile Organic Compounds (GC) by Method 8015C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 13.7 0.845 4.39 1 10/27/2019 14:21 WG1370013
(S) o-Terphenyl 65.2 18.0-148 10/27/2019 14:21 WG1370013
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 08:51 22 of 63
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 10:42 22 of 63
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 13
L1153653
SW-7
Collected date/time: 10/22/19 12:50
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 95.7 1 10/31/2019 13:07 WG1372542
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction 0.877 B J 0.567 2.61 25 11/01/2019 09:09 WG1373179
(S) a,a,a-Trifluorotoluene(FID) 103 77.0-120 11/01/2019 09:09 WG1373179
Semi-Volatile Organic Compounds (GC) by Method 8015C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 1.50 J 0.803 4.18 1 10/27/2019 06:46 WG1370013
(S) o-Terphenyl 80.5 18.0-148 10/27/2019 06:46 WG1370013
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 08:51 23 of 63
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 10:42 23 of 63
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 14
L1153653
SW-8
Collected date/time: 10/22/19 12:45
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 79.8 1 10/31/2019 12:54 WG1372543
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction 1.73 B J 0.681 3.13 25 11/01/2019 09:29 WG1373179
(S) a,a,a-Trifluorotoluene(FID) 101 77.0-120 11/01/2019 09:29 WG1373179
Semi-Volatile Organic Compounds (GC) by Method 8015C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 3.00 J 0.964 5.01 1 10/27/2019 14:47 WG1370013
(S) o-Terphenyl 61.4 18.0-148 10/27/2019 14:47 WG1370013
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 08:51 24 of 63
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 10:42 24 of 63
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 15
L1153653
FL-3
Collected date/time: 10/22/19 13:20
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 91.8 1 10/31/2019 12:54 WG1372543
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction 1.89 B J 0.592 2.72 25 11/01/2019 09:50 WG1373179
(S) a,a,a-Trifluorotoluene(FID) 97.9 77.0-120 11/01/2019 09:50 WG1373179
Semi-Volatile Organic Compounds (GC) by Method 8015C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 8.60 0.838 4.36 1 10/27/2019 08:52 WG1370013
(S) o-Terphenyl 87.2 18.0-148 10/27/2019 08:52 WG1370013
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 08:51 25 of 63
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 10:42 25 of 63
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 16
L1153653
FL-4
Collected date/time: 10/22/19 13:30
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 96.4 1 10/31/2019 12:54 WG1372543
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction 2.31 B J 0.597 2.75 26.5 11/01/2019 10:11 WG1373179
(S) a,a,a-Trifluorotoluene(FID) 102 77.0-120 11/01/2019 10:11 WG1373179
Semi-Volatile Organic Compounds (GC) by Method 8015C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) High Fraction U 0.798 4.15 1 10/27/2019 06:20 WG1370013
(S) o-Terphenyl 85.7 18.0-148 10/27/2019 06:20 WG1370013
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 08:51 26 of 63
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 10:42 26 of 63
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 17
L1153653
SW-9
Collected date/time: 10/23/19 10:00
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 94.1 1 10/31/2019 12:54 WG1372543
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction 3.62 B 0.634 2.92 27.5 11/01/2019 10:31 WG1373179
(S) a,a,a-Trifluorotoluene(FID) 101 77.0-120 11/01/2019 10:31 WG1373179
Semi-Volatile Organic Compounds (GC) by Method 8015C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 1.27 J 0.817 4.25 1 10/27/2019 13:54 WG1370013
(S) o-Terphenyl 68.1 18.0-148 10/27/2019 13:54 WG1370013
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 08:51 27 of 63
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 10:42 27 of 63
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 18
L1153653
SW-10
Collected date/time: 10/23/19 10:05
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 97.1 1 10/31/2019 12:54 WG1372543
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction 0.887 B J 0.800 3.69 35.8 11/01/2019 10:52 WG1373179
(S) a,a,a-Trifluorotoluene(FID) 98.6 77.0-120 11/01/2019 10:52 WG1373179
Semi-Volatile Organic Compounds (GC) by Method 8015C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) High Fraction U 0.792 4.12 1 10/27/2019 06:33 WG1370013
(S) o-Terphenyl 79.9 18.0-148 10/27/2019 06:33 WG1370013
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 08:51 28 of 63
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 10:42 28 of 63
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 19
L1153653
SW-11
Collected date/time: 10/23/19 10:10
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 91.0 1 10/31/2019 12:54 WG1372543
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction 3.08 B 0.608 2.80 25.5 11/01/2019 23:25 WG1373752
(S) a,a,a-Trifluorotoluene(FID) 106 77.0-120 11/01/2019 23:25 WG1373752
Semi-Volatile Organic Compounds (GC) by Method 8015C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 1.14 J 0.845 4.40 1 10/27/2019 07:26 WG1370013
(S) o-Terphenyl 78.7 18.0-148 10/27/2019 07:26 WG1370013
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 08:51 29 of 63
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 10:42 29 of 63
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 20
L1153653
SW-12
Collected date/time: 10/23/19 10:15
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 95.7 1 10/31/2019 12:54 WG1372543
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction 1.23 B J 0.567 2.61 25 11/01/2019 23:46 WG1373752
(S) a,a,a-Trifluorotoluene(FID) 108 77.0-120 11/01/2019 23:46 WG1373752
Semi-Volatile Organic Compounds (GC) by Method 8015C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 2.48 J 0.804 4.18 1 10/27/2019 08:32 WG1370013
(S) o-Terphenyl 73.9 18.0-148 10/27/2019 08:32 WG1370013
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 08:51 30 of 63
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 10:42 30 of 63
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 21
L1153653
SW-13
Collected date/time: 10/23/19 11:05
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 89.9 1 10/31/2019 12:54 WG1372543
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction 1.02 B J 0.604 2.78 25 11/02/2019 00:07 WG1373752
(S) a,a,a-Trifluorotoluene(FID) 107 77.0-120 11/02/2019 00:07 WG1373752
Semi-Volatile Organic Compounds (GC) by Method 8015C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 4.97 0.855 4.45 1 10/27/2019 09:44 WG1370013
(S) o-Terphenyl 147 18.0-148 10/27/2019 09:44 WG1370013
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 08:51 31 of 63
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 10:42 31 of 63
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 22
L1153653
SW-14
Collected date/time: 10/23/19 11:10
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 79.4 1 10/31/2019 12:54 WG1372543
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction 2.98 B J 0.696 3.21 25.5 11/02/2019 00:27 WG1373752
(S) a,a,a-Trifluorotoluene(FID) 102 77.0-120 11/02/2019 00:27 WG1373752
Semi-Volatile Organic Compounds (GC) by Method 8015C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 3.73 J 0.968 5.04 1 10/27/2019 07:39 WG1370013
(S) o-Terphenyl 64.7 18.0-148 10/27/2019 07:39 WG1370013
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 08:51 32 of 63
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 10:42 32 of 63
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 23
L1153653
SW-15
Collected date/time: 10/23/19 11:15
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 86.8 1 10/31/2019 12:54 WG1372543
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction 0.901 B J 0.626 2.88 25 11/02/2019 00:48 WG1373752
(S) a,a,a-Trifluorotoluene(FID) 107 77.0-120 11/02/2019 00:48 WG1373752
Semi-Volatile Organic Compounds (GC) by Method 8015C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 3.45 J 0.886 4.61 1 10/28/2019 04:37 WG1370558
(S) o-Terphenyl 56.9 18.0-148 10/28/2019 04:37 WG1370558
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 08:51 33 of 63
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 10:42 33 of 63
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 24
L1153653
SW-16
Collected date/time: 10/23/19 10:30
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 94.7 1 10/31/2019 12:42 WG1372545
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction 1.13 B J 0.574 2.64 25 11/02/2019 01:09 WG1373752
(S) a,a,a-Trifluorotoluene(FID) 103 77.0-120 11/02/2019 01:09 WG1373752
Semi-Volatile Organic Compounds (GC) by Method 8015C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 1.35 J 0.812 4.23 1 10/28/2019 04:50 WG1370558
(S) o-Terphenyl 77.6 18.0-148 10/28/2019 04:50 WG1370558
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 08:51 34 of 63
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 10:42 34 of 63
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 25
L1153653
SW-17
Collected date/time: 10/23/19 10:35
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 86.3 1 10/31/2019 12:42 WG1372545
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction 1.15 B J 0.629 2.90 25 11/02/2019 01:29 WG1373752
(S) a,a,a-Trifluorotoluene(FID) 104 77.0-120 11/02/2019 01:29 WG1373752
Semi-Volatile Organic Compounds (GC) by Method 8015C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 5.62 0.891 4.64 1 10/28/2019 05:03 WG1370558
(S) o-Terphenyl 61.8 18.0-148 10/28/2019 05:03 WG1370558
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 08:51 35 of 63
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 10:42 35 of 63
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 26
L1153653
SW-18
Collected date/time: 10/23/19 10:40
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 94.5 1 10/31/2019 12:42 WG1372545
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction 2.65 B J 0.673 3.10 29.3 11/02/2019 01:50 WG1373752
(S) a,a,a-Trifluorotoluene(FID) 103 77.0-120 11/02/2019 01:50 WG1373752
Semi-Volatile Organic Compounds (GC) by Method 8015C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 4.44 0.813 4.23 1 10/28/2019 05:15 WG1370558
(S) o-Terphenyl 75.6 18.0-148 10/28/2019 05:15 WG1370558
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 08:51 36 of 63
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 10:42 36 of 63
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 27
L1153653
FL-5
Collected date/time: 10/23/19 12:55
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 94.8 1 10/31/2019 12:42 WG1372545
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction 4.26 B 0.683 3.14 29.8 11/02/2019 02:11 WG1373752
(S) a,a,a-Trifluorotoluene(FID) 103 77.0-120 11/02/2019 02:11 WG1373752
Semi-Volatile Organic Compounds (GC) by Method 8015C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 1.10 J 0.811 4.22 1 10/28/2019 05:28 WG1370558
(S) o-Terphenyl 75.5 18.0-148 10/28/2019 05:28 WG1370558
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 08:51 37 of 63
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 10:42 37 of 63
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 28
L1153653
FL-6
Collected date/time: 10/23/19 13:00
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 92.6 1 10/31/2019 12:42 WG1372545
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction 2.76 B J 0.679 3.13 29 11/02/2019 02:31 WG1373752
(S) a,a,a-Trifluorotoluene(FID) 103 77.0-120 11/02/2019 02:31 WG1373752
Semi-Volatile Organic Compounds (GC) by Method 8015C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 1.06 J 0.830 4.32 1 10/28/2019 05:41 WG1370558
(S) o-Terphenyl 68.8 18.0-148 10/28/2019 05:41 WG1370558
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 08:51 38 of 63
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 10:42 38 of 63
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 29
L1153653
FL-7
Collected date/time: 10/23/19 13:05
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 86.3 1 10/31/2019 12:42 WG1372545
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction 2.93 B J 0.649 2.99 25.8 11/02/2019 02:52 WG1373752
(S) a,a,a-Trifluorotoluene(FID) 103 77.0-120 11/02/2019 02:52 WG1373752
Semi-Volatile Organic Compounds (GC) by Method 8015C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 1.21 J 0.891 4.64 1 10/28/2019 05:53 WG1370558
(S) o-Terphenyl 63.4 18.0-148 10/28/2019 05:53 WG1370558
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 08:51 39 of 63
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 10:42 39 of 63
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 30
L1153653
FL-8
Collected date/time: 10/23/19 13:10
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 88.2 1 10/31/2019 12:42 WG1372545
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction 1.06 B J 0.616 2.84 25 11/02/2019 03:13 WG1373752
(S) a,a,a-Trifluorotoluene(FID) 106 77.0-120 11/02/2019 03:13 WG1373752
Semi-Volatile Organic Compounds (GC) by Method 8015C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 13.4 J 4.37 22.7 5 10/28/2019 11:14 WG1370558
(S) o-Terphenyl 65.3 18.0-148 10/28/2019 11:14 WG1370558
Sample Narrative:
L1153653-30 WG1370558: Cannot run at lower dilution due to viscosity of extract
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 08:51 40 of 63
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 10:42 40 of 63
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 31
L1153653
FP-5
Collected date/time: 10/23/19 13:15
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 90.8 1 10/31/2019 12:42 WG1372545
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction 2.47 B J 0.598 2.75 25 11/02/2019 03:33 WG1373752
(S) a,a,a-Trifluorotoluene(FID) 103 77.0-120 11/02/2019 03:33 WG1373752
Semi-Volatile Organic Compounds (GC) by Method 8015C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 4.78 0.847 4.41 1 10/28/2019 06:19 WG1370558
(S) o-Terphenyl 67.7 18.0-148 10/28/2019 06:19 WG1370558
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 08:51 41 of 63
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 10:42 41 of 63
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 32
L1153653
FP-6
Collected date/time: 10/23/19 13:20
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 81.8 1 10/31/2019 12:42 WG1372545
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction 3.75 B 0.762 3.51 28.7 11/02/2019 03:54 WG1373752
(S) a,a,a-Trifluorotoluene(FID) 103 77.0-120 11/02/2019 03:54 WG1373752
Semi-Volatile Organic Compounds (GC) by Method 8015C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 93.4 0.940 4.89 1 10/28/2019 06:31 WG1370558
(S) o-Terphenyl 30.9 18.0-148 10/28/2019 06:31 WG1370558
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 08:51 42 of 63
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 10:42 42 of 63
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 33
L1153653
FP-7
Collected date/time: 10/23/19 13:25
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 93.0 1 10/31/2019 12:42 WG1372545
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction 2.11 B J 0.584 2.69 25 11/02/2019 04:14 WG1373752
(S) a,a,a-Trifluorotoluene(FID) 104 77.0-120 11/02/2019 04:14 WG1373752
Semi-Volatile Organic Compounds (GC) by Method 8015C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 3.53 J 0.827 4.30 1 10/28/2019 15:16 WG1370558
(S) o-Terphenyl 74.0 18.0-148 10/28/2019 15:16 WG1370558
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 08:51 43 of 63
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 10:42 43 of 63
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 34
L1153653
FP-8
Collected date/time: 10/23/19 13:30
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 89.1 1 10/31/2019 13:42 WG1372546
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction 0.991 B J 0.609 2.81 25 11/02/2019 04:35 WG1373752
(S) a,a,a-Trifluorotoluene(FID) 107 77.0-120 11/02/2019 04:35 WG1373752
Semi-Volatile Organic Compounds (GC) by Method 8015C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 3.39 J 0.863 4.49 1 10/28/2019 06:57 WG1370558
(S) o-Terphenyl 69.1 18.0-148 10/28/2019 06:57 WG1370558
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 08:51 44 of 63
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 10:42 44 of 63
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 35
L1153653
FP-9
Collected date/time: 10/23/19 13:35
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 89.4 1 10/31/2019 13:42 WG1372546
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) Low Fraction 0.829 B J 0.607 2.80 25 11/02/2019 04:56 WG1373752
(S) a,a,a-Trifluorotoluene(FID) 107 77.0-120 11/02/2019 04:56 WG1373752
Semi-Volatile Organic Compounds (GC) by Method 8015C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date / time
TPH (GC/FID) High Fraction 3.48 J 0.860 4.47 1 10/28/2019 07:09 WG1370558
(S) o-Terphenyl 63.7 18.0-148 10/28/2019 07:09 WG1370558
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 08:51 45 of 63
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 10:42 45 of 63
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1372541
Total Solids by Method 2540 G-2011 L1153653-01,02,03
Method Blank (MB)
(MB) R3467398-1 10/31/19 11:23
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.00100
L1153653-03 Original Sample (OS) • Duplicate (DUP)
(OS) L1153653-03 10/31/19 11:23 • (DUP) R3467398-3 10/31/19 11:23
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 88.2 87.3 1 1.06 10
Laboratory Control Sample (LCS)
(LCS) R3467398-2 10/31/19 11:23
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 08:51 46 of 63
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 10:42 46 of 63
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1372542
Total Solids by Method 2540 G-2011 L1153653-04,05,06,07,08,09,10,11,12,13
Method Blank (MB)
(MB) R3467410-1 10/31/19 13:07
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.000
L1153653-09 Original Sample (OS) • Duplicate (DUP)
(OS) L1153653-09 10/31/19 13:07 • (DUP) R3467410-3 10/31/19 13:07
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 94.1 94.6 1 0.496 10
Laboratory Control Sample (LCS)
(LCS) R3467410-2 10/31/19 13:07
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 08:51 47 of 63
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 10:42 47 of 63
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1372543
Total Solids by Method 2540 G-2011 L1153653-14,15,16,17,18,19,20,21,22,23
Method Blank (MB)
(MB) R3467407-1 10/31/19 12:54
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.000
L1153653-14 Original Sample (OS) • Duplicate (DUP)
(OS) L1153653-14 10/31/19 12:54 • (DUP) R3467407-3 10/31/19 12:54
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 79.8 82.0 1 2.69 10
Laboratory Control Sample (LCS)
(LCS) R3467407-2 10/31/19 12:54
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 08:51 48 of 63
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1153653 11/06/19 10:42 48 of 63
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1372545
Total Solids by Method 2540 G-2011 L1153653-24,25,26,27,28,29,30,31,32,33
Method Blank (MB)
(MB) R3467403-1 10/31/19 12:42
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.000
L1153653-25 Original Sample (OS) • Duplicate (DUP)
(OS) L1153653-25 10/31/19 12:42 • (DUP) R3467403-3 10/31/19 12:42
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 86.3 85.9 1 0.447 10
Laboratory Control Sample (LCS)
(LCS) R3467403-2 10/31/19 12:42
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1372546
Total Solids by Method 2540 G-2011 L1153653-34,35
Method Blank (MB)
(MB) R3467525-1 10/31/19 13:42
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.000
L1153659-03 Original Sample (OS) • Duplicate (DUP)
(OS) L1153659-03 10/31/19 13:42 • (DUP) R3467525-3 10/31/19 13:42
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 90.0 87.4 1 2.89 10
Laboratory Control Sample (LCS)
(LCS) R3467525-2 10/31/19 13:42
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1373171
Volatile Organic Compounds (GC) by Method 8015D/GRO L1153653-01
Method Blank (MB)
(MB) R3467384-3 11/01/19 03:14
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 0.0260 J 0.0217 0.100
(S)
a,a,a-Trifluorotoluene(FID)103 77.0-120
Laboratory Control Sample (LCS)
(LCS) R3467384-2 11/01/19 02:33
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
TPH (GC/FID) Low Fraction 5.50 5.11 92.9 72.0-127
(S)
a,a,a-Trifluorotoluene(FID) 113 77.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1373179
Volatile Organic Compounds (GC) by Method 8015D/GRO L1153653-03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18
Method Blank (MB)
(MB) R3468307-2 11/01/19 03:37
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 0.0289 J 0.0217 0.100
(S)
a,a,a-Trifluorotoluene(FID)100 77.0-120
Laboratory Control Sample (LCS)
(LCS) R3468307-1 11/01/19 02:56
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
TPH (GC/FID) Low Fraction 5.50 5.89 107 72.0-127
(S)
a,a,a-Trifluorotoluene(FID) 114 77.0-120
L1153653-18 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1153653-18 11/01/19 10:52 • (MS) R3468307-3 11/01/19 11:13 • (MSD) R3468307-4 11/01/19 11:33
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
TPH (GC/FID) Low Fraction 203 0.887 261 218 128 107 35.8 10.0-151 17.6 28
(S)
a,a,a-Trifluorotoluene(FID) 118 115 77.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1373752
Volatile Organic Compounds (GC) by Method 8015D/GRO L1153653-19,20,21,22,23,24,25,26,27,28,29,30,31,32,33,34,35
Method Blank (MB)
(MB) R3467922-1 11/01/19 20:34
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction 0.0217 J 0.0217 0.100
(S)
a,a,a-Trifluorotoluene(FID)104 77.0-120
Laboratory Control Sample (LCS)
(LCS) R3467922-2 11/01/19 22:29
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
TPH (GC/FID) Low Fraction 5.50 5.22 94.9 72.0-127
(S)
a,a,a-Trifluorotoluene(FID) 113 77.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1374243
Volatile Organic Compounds (GC) by Method 8015D/GRO L1153653-02
Method Blank (MB)
(MB) R3468102-3 11/03/19 15:38
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
TPH (GC/FID) Low Fraction U 0.0217 0.100
(S)
a,a,a-Trifluorotoluene(FID)101 77.0-120
Laboratory Control Sample (LCS)
(LCS) R3468102-2 11/03/19 14:47
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
TPH (GC/FID) Low Fraction 5.50 5.71 104 72.0-127
(S)
a,a,a-Trifluorotoluene(FID) 114 77.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1370012
Semi-Volatile Organic Compounds (GC) by Method 8015C L1153653-01,02
Method Blank (MB)
(MB) R3465557-1 10/27/19 02:19
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
TPH (GC/FID) High Fraction U 0.769 4.00
(S) o-Terphenyl 72.7 18.0-148
Laboratory Control Sample (LCS)
(LCS) R3465557-2 10/27/19 02:32
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
TPH (GC/FID) High Fraction 50.0 46.5 93.0 50.0-150
(S) o-Terphenyl 108 18.0-148
L1153639-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1153639-01 10/27/19 19:15 • (MS) R3465557-3 10/27/19 19:28 • (MSD) R3465557-4 10/27/19 19:41
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
TPH (GC/FID) High Fraction 55.4 59.5 137 130 141 127 1 50.0-150 5.81 20
(S) o-Terphenyl 88.7 78.5 18.0-148
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1370013
Semi-Volatile Organic Compounds (GC) by Method 8015C L1153653-03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18,19,20,21,22
Method Blank (MB)
(MB) R3465503-1 10/27/19 05:40
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
TPH (GC/FID) High Fraction U 0.769 4.00
(S) o-Terphenyl 75.5 18.0-148
Laboratory Control Sample (LCS)
(LCS) R3465503-2 10/27/19 05:54
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
TPH (GC/FID) High Fraction 50.0 37.0 74.0 50.0-150
(S) o-Terphenyl 96.7 18.0-148
L1153653-13 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1153653-13 10/27/19 06:46 • (MS) R3465503-3 10/27/19 07:00 • (MSD) R3465503-4 10/27/19 07:13
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
TPH (GC/FID) High Fraction 52.2 1.50 41.9 43.2 77.3 79.9 1 50.0-150 3.19 20
(S) o-Terphenyl 104 105 18.0-148
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1370558
Semi-Volatile Organic Compounds (GC) by Method 8015C L1153653-23,24,25,26,27,28,29,30,31,32,33,34,35
Method Blank (MB)
(MB) R3465824-1 10/28/19 04:12
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
TPH (GC/FID) High Fraction U 0.769 4.00
(S) o-Terphenyl 70.3 18.0-148
Laboratory Control Sample (LCS)
(LCS) R3465824-2 10/28/19 04:25
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
TPH (GC/FID) High Fraction 50.0 36.2 72.4 50.0-150
(S) o-Terphenyl 84.4 18.0-148
L1153947-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1153947-02 10/28/19 07:35 • (MS) R3465824-3 10/28/19 07:47 • (MSD) R3465824-4 10/28/19 08:00
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
TPH (GC/FID) High Fraction 55.6 6.06 39.1 33.2 59.4 49.2 1 50.0-150 J6 16.3 20
(S) o-Terphenyl 66.5 57.4 18.0-148
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
(dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils].
MDL Method Detection Limit.
MDL (dry)Method Detection Limit.
RDL Reported Detection Limit.
RDL (dry)Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
B The same analyte is found in the associated blank.
J The identification of the analyte is acceptable; the reported value is an estimate.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low.
J7 Surrogate recovery cannot be used for control limit evaluation due to dilution.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing
turn-around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National.

State Accreditations
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN-03-2002-34
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹n/a
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶90010 South Carolina 84004
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana ¹LA180010 Texas T104704245-18-15
Maine TN0002 Texas ⁵LAB0152
Maryland 324 Utah TN00003
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 460132
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 9980939910
Montana CERT0086 Wyoming A2LA

Third Party Federal Accreditations
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable

Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contactour main office. Pace National performs all testing at our central laboratory.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ANALYTICAL REPORT
November 08, 2019
Withers & Ravenel Eng. - Standard
Sample Delivery Group:L1155985
Samples Received:10/31/2019
Project Number:02180080.10
Description:Midway Kwik Stop
Site:0-0-2529
Report To:Brian Bellis
219 Station Road
Suite 101
Wilmington, NC 28405
Entire Report Reviewed By:
November 08, 2019
[Preliminary Report]
Heather J Wagner
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received.
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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November 08, 2019
Heather J Wagner
Project Manager
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ONE LAB. NATIONWIDE.TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
MW-1 L1155985-01 5
MW-2 L1155985-02 9
Qc: Quality Control Summary 13
Metals (ICP) by Method 6010D 13
Volatile Petroleum Hydrocarbons by Method MADEPV 14
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 15
TPH by Method MADEPE 19
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 20
Gl: Glossary of Terms 25
Al: Accreditations & Locations 26
Sc: Sample Chain of Custody 27
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
MW-1 L1155985-01 GW Brian Bellis 10/30/19 12:00 10/31/19 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Metals (ICP) by Method 6010D WG1374911 1 11/04/19 17:07 11/05/19 13:28 EL Mt. Juliet, TN
Volatile Petroleum Hydrocarbons by Method MADEPV WG1373778 1 11/06/19 23:38 11/06/19 23:38 BMB Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 WG1374034 1 11/02/19 18:43 11/02/19 18:43 HJF Mt. Juliet, TN
TPH by Method MADEPE WG1375597 1 11/04/19 20:30 11/06/19 05:11 SHG Mt. Juliet, TN
TPH by Method MADEPE WG1375597 1 11/04/19 20:30 11/06/19 07:00 SHG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1375392 1 11/06/19 06:39 11/07/19 07:48 AO Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-2 L1155985-02 GW Brian Bellis 10/30/19 13:00 10/31/19 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Metals (ICP) by Method 6010D WG1374911 1 11/04/19 17:07 11/05/19 13:30 EL Mt. Juliet, TN
Volatile Petroleum Hydrocarbons by Method MADEPV WG1373778 1 11/07/19 00:10 11/07/19 00:10 BMB Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 WG1374034 1 11/02/19 19:03 11/02/19 19:03 HJF Mt. Juliet, TN
TPH by Method MADEPE WG1375597 1 11/04/19 20:30 11/06/19 05:33 SHG Mt. Juliet, TN
TPH by Method MADEPE WG1375597 1 11/04/19 20:30 11/06/19 06:38 SHG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1375392 1 11/06/19 06:39 11/07/19 08:08 AO Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Heather J Wagner
Project Manager
Sample Delivery Group (SDG) Narrative
VOC pH outside of method requirement.
Lab Sample ID Project Sample ID Method
L1155985-02 MW-2 MADEPV
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Heather J Wagner
Project Manager
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L1155985
MW-1
Collected date/time: 10/30/19 12:00
Metals (ICP) by Method 6010D
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Lead 9.45 1.90 5.00 1 11/05/2019 13:28 WG1374911
Volatile Petroleum Hydrocarbons by Method MADEPV
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics U 33.3 100 1 11/06/2019 23:38 WG1373778
Unadjusted C9-C12 Aliphatics U 33.3 100 1 11/06/2019 23:38 WG1373778
Unadjusted C9-C10 Aromatics U 33.3 100 1 11/06/2019 23:38 WG1373778
Total VPH U 33.3 100 1 11/06/2019 23:38 WG1373778
(S) 2,5-Dibromotoluene(FID) 104 70.0-130 11/06/2019 23:38 WG1373778
(S) 2,5-Dibromotoluene(PID) 101 70.0-130 11/06/2019 23:38 WG1373778
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acetone U 10.0 50.0 1 11/02/2019 18:43 WG1374034
Acrolein U 8.87 50.0 1 11/02/2019 18:43 WG1374034
Acrylonitrile U 1.87 10.0 1 11/02/2019 18:43 WG1374034
Benzene U 0.331 1.00 1 11/02/2019 18:43 WG1374034
Bromobenzene U 0.352 1.00 1 11/02/2019 18:43 WG1374034
Bromochloromethane U 0.520 1.00 1 11/02/2019 18:43 WG1374034
Bromodichloromethane U 0.380 1.00 1 11/02/2019 18:43 WG1374034
Bromoform U 0.469 1.00 1 11/02/2019 18:43 WG1374034
Bromomethane U 0.866 5.00 1 11/02/2019 18:43 WG1374034
n-Butylbenzene U 0.361 1.00 1 11/02/2019 18:43 WG1374034
sec-Butylbenzene U 0.365 1.00 1 11/02/2019 18:43 WG1374034
tert-Butylbenzene U 0.399 1.00 1 11/02/2019 18:43 WG1374034
Carbon tetrachloride U 0.379 1.00 1 11/02/2019 18:43 WG1374034
Chlorobenzene U 0.348 1.00 1 11/02/2019 18:43 WG1374034
Chlorodibromomethane U 0.327 1.00 1 11/02/2019 18:43 WG1374034
Chloroethane U 0.453 5.00 1 11/02/2019 18:43 WG1374034
Chloroform U 0.324 5.00 1 11/02/2019 18:43 WG1374034
Chloromethane U 0.276 2.50 1 11/02/2019 18:43 WG1374034
2-Chlorotoluene U 0.375 1.00 1 11/02/2019 18:43 WG1374034
4-Chlorotoluene U 0.351 1.00 1 11/02/2019 18:43 WG1374034
1,2-Dibromo-3-Chloropropane U 1.33 5.00 1 11/02/2019 18:43 WG1374034
1,2-Dibromoethane U 0.381 1.00 1 11/02/2019 18:43 WG1374034
Dibromomethane U 0.346 1.00 1 11/02/2019 18:43 WG1374034
1,2-Dichlorobenzene U 0.349 1.00 1 11/02/2019 18:43 WG1374034
1,3-Dichlorobenzene U 0.220 1.00 1 11/02/2019 18:43 WG1374034
1,4-Dichlorobenzene U 0.274 1.00 1 11/02/2019 18:43 WG1374034
Dichlorodifluoromethane U 0.551 5.00 1 11/02/2019 18:43 WG1374034
1,1-Dichloroethane U 0.259 1.00 1 11/02/2019 18:43 WG1374034
1,2-Dichloroethane U 0.361 1.00 1 11/02/2019 18:43 WG1374034
1,1-Dichloroethene U 0.398 1.00 1 11/02/2019 18:43 WG1374034
cis-1,2-Dichloroethene U 0.260 1.00 1 11/02/2019 18:43 WG1374034
trans-1,2-Dichloroethene U 0.396 1.00 1 11/02/2019 18:43 WG1374034
1,2-Dichloropropane U 0.306 1.00 1 11/02/2019 18:43 WG1374034
1,1-Dichloropropene U 0.352 1.00 1 11/02/2019 18:43 WG1374034
1,3-Dichloropropane U 0.366 1.00 1 11/02/2019 18:43 WG1374034
cis-1,3-Dichloropropene U 0.418 1.00 1 11/02/2019 18:43 WG1374034
trans-1,3-Dichloropropene U 0.419 1.00 1 11/02/2019 18:43 WG1374034
2,2-Dichloropropane U 0.321 1.00 1 11/02/2019 18:43 WG1374034
Di-isopropyl ether U 0.320 1.00 1 11/02/2019 18:43 WG1374034
Ethylbenzene U 0.384 1.00 1 11/02/2019 18:43 WG1374034
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L1155985
MW-1
Collected date/time: 10/30/19 12:00
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Hexachloro-1,3-butadiene U 0.256 1.00 1 11/02/2019 18:43 WG1374034
2-Hexanone U 3.82 10.0 1 11/02/2019 18:43 WG1374034
Isopropylbenzene U 0.326 1.00 1 11/02/2019 18:43 WG1374034
p-Isopropyltoluene U 0.350 1.00 1 11/02/2019 18:43 WG1374034
2-Butanone (MEK)U 3.93 10.0 1 11/02/2019 18:43 WG1374034
Methylene Chloride U 1.00 5.00 1 11/02/2019 18:43 WG1374034
4-Methyl-2-pentanone (MIBK) U 2.14 10.0 1 11/02/2019 18:43 WG1374034
Methyl tert-butyl ether U 0.367 1.00 1 11/02/2019 18:43 WG1374034
Naphthalene 1.03 J 1.00 5.00 1 11/02/2019 18:43 WG1374034
n-Propylbenzene U 0.349 1.00 1 11/02/2019 18:43 WG1374034
Styrene U 0.307 1.00 1 11/02/2019 18:43 WG1374034
1,1,1,2-Tetrachloroethane U 0.385 1.00 1 11/02/2019 18:43 WG1374034
1,1,2,2-Tetrachloroethane U 0.130 1.00 1 11/02/2019 18:43 WG1374034
Tetrachloroethene U 0.372 1.00 1 11/02/2019 18:43 WG1374034
Toluene U 0.412 1.00 1 11/02/2019 18:43 WG1374034
1,2,3-Trichlorobenzene U 0.230 1.00 1 11/02/2019 18:43 WG1374034
1,2,4-Trichlorobenzene U 0.355 1.00 1 11/02/2019 18:43 WG1374034
1,1,1-Trichloroethane U 0.319 1.00 1 11/02/2019 18:43 WG1374034
1,1,2-Trichloroethane U 0.383 1.00 1 11/02/2019 18:43 WG1374034
Trichloroethene U 0.398 1.00 1 11/02/2019 18:43 WG1374034
Trichlorofluoromethane U 1.20 5.00 1 11/02/2019 18:43 WG1374034
1,2,3-Trichloropropane U 0.807 2.50 1 11/02/2019 18:43 WG1374034
1,2,4-Trimethylbenzene U 0.373 1.00 1 11/02/2019 18:43 WG1374034
1,3,5-Trimethylbenzene U 0.387 1.00 1 11/02/2019 18:43 WG1374034
Vinyl acetate U 1.63 10.0 1 11/02/2019 18:43 WG1374034
Vinyl chloride U 0.259 1.00 1 11/02/2019 18:43 WG1374034
o-Xylene U 0.341 1.00 1 11/02/2019 18:43 WG1374034
m&p-Xylenes U 0.719 2.00 1 11/02/2019 18:43 WG1374034
(S) Toluene-d8 93.5 80.0-120 11/02/2019 18:43 WG1374034
(S) 4-Bromofluorobenzene 92.8 77.0-126 11/02/2019 18:43 WG1374034
(S) 1,2-Dichloroethane-d4 89.6 70.0-130 11/02/2019 18:43 WG1374034
TPH by Method MADEPE
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics U 33.3 100 1 11/06/2019 05:11 WG1375597
Unadjusted C19-C36 Aliphatics 83.5 B J 33.3 100 1 11/06/2019 05:11 WG1375597
Unadjusted C11-C22 Aromatics 53.9 B J 33.3 100 1 11/06/2019 07:00 WG1375597
Unadjusted Total Petroleum
Hydrocarbons 137 33.3 100 1 11/06/2019 07:00 WG1375597
(S) o-Terphenyl 74.9 40.0-140 11/06/2019 07:00 WG1375597
(S) 1-Chloro-octadecane 47.1 40.0-140 11/06/2019 05:11 WG1375597
(S) 2-Fluorobiphenyl 90.5 40.0-140 11/06/2019 07:00 WG1375597
(S) 2-Bromonaphthalene 84.6 40.0-140 11/06/2019 07:00 WG1375597
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acenaphthene U 0.316 1.00 1 11/07/2019 07:48 WG1375392
Acenaphthylene U 0.309 1.00 1 11/07/2019 07:48 WG1375392
Anthracene U 0.291 1.00 1 11/07/2019 07:48 WG1375392
Benzidine U 4.32 10.0 1 11/07/2019 07:48 WG1375392
Benzo(a)anthracene U 0.0975 1.00 1 11/07/2019 07:48 WG1375392
Benzo(b)fluoranthene U 0.0896 1.00 1 11/07/2019 07:48 WG1375392
Benzo(k)fluoranthene U 0.355 1.00 1 11/07/2019 07:48 WG1375392
Benzo(g,h,i)perylene U 0.161 1.00 1 11/07/2019 07:48 WG1375392
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L1155985
MW-1
Collected date/time: 10/30/19 12:00
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Benzo(a)pyrene U 0.340 1.00 1 11/07/2019 07:48 WG1375392
Bis(2-chlorethoxy)methane U 0.329 10.0 1 11/07/2019 07:48 WG1375392
Bis(2-chloroethyl)ether U 1.62 10.0 1 11/07/2019 07:48 WG1375392
Bis(2-chloroisopropyl)ether U 0.445 10.0 1 11/07/2019 07:48 WG1375392
4-Bromophenyl-phenylether U 0.335 10.0 1 11/07/2019 07:48 WG1375392
2-Chloronaphthalene U 0.330 1.00 1 11/07/2019 07:48 WG1375392
4-Chlorophenyl-phenylether U 0.303 10.0 1 11/07/2019 07:48 WG1375392
Chrysene U 0.332 1.00 1 11/07/2019 07:48 WG1375392
Dibenz(a,h)anthracene U 0.279 1.00 1 11/07/2019 07:48 WG1375392
3,3-Dichlorobenzidine U 2.02 10.0 1 11/07/2019 07:48 WG1375392
2,4-Dinitrotoluene U 1.65 10.0 1 11/07/2019 07:48 WG1375392
2,6-Dinitrotoluene U 0.279 10.0 1 11/07/2019 07:48 WG1375392
Fluoranthene U 0.310 1.00 1 11/07/2019 07:48 WG1375392
Fluorene U 0.323 1.00 1 11/07/2019 07:48 WG1375392
Hexachlorobenzene U 0.341 1.00 1 11/07/2019 07:48 WG1375392
Hexachloro-1,3-butadiene U 0.329 10.0 1 11/07/2019 07:48 WG1375392
Hexachlorocyclopentadiene U 2.33 10.0 1 11/07/2019 07:48 WG1375392
Hexachloroethane U 0.365 10.0 1 11/07/2019 07:48 WG1375392
Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 11/07/2019 07:48 WG1375392
Isophorone U 0.272 10.0 1 11/07/2019 07:48 WG1375392
Naphthalene U 0.372 1.00 1 11/07/2019 07:48 WG1375392
Nitrobenzene U 0.367 10.0 1 11/07/2019 07:48 WG1375392
n-Nitrosodimethylamine U 1.26 10.0 1 11/07/2019 07:48 WG1375392
n-Nitrosodiphenylamine U 1.19 10.0 1 11/07/2019 07:48 WG1375392
n-Nitrosodi-n-propylamine U 0.403 10.0 1 11/07/2019 07:48 WG1375392
Phenanthrene U 0.366 1.00 1 11/07/2019 07:48 WG1375392
Benzylbutyl phthalate U 0.275 3.00 1 11/07/2019 07:48 WG1375392
Bis(2-ethylhexyl)phthalate U 0.709 3.00 1 11/07/2019 07:48 WG1375392
Di-n-butyl phthalate U 0.266 3.00 1 11/07/2019 07:48 WG1375392
Diethyl phthalate U 0.282 3.00 1 11/07/2019 07:48 WG1375392
Dimethyl phthalate U 0.283 3.00 1 11/07/2019 07:48 WG1375392
Di-n-octyl phthalate U 0.278 3.00 1 11/07/2019 07:48 WG1375392
Pyrene U 0.330 1.00 1 11/07/2019 07:48 WG1375392
1,2,4-Trichlorobenzene U 0.355 10.0 1 11/07/2019 07:48 WG1375392
4-Chloro-3-methylphenol U 0.263 10.0 1 11/07/2019 07:48 WG1375392
2-Chlorophenol U 0.283 10.0 1 11/07/2019 07:48 WG1375392
2,4-Dichlorophenol U 0.284 10.0 1 11/07/2019 07:48 WG1375392
2,4-Dimethylphenol U 0.624 10.0 1 11/07/2019 07:48 WG1375392
4,6-Dinitro-2-methylphenol U 2.62 10.0 1 11/07/2019 07:48 WG1375392
2,4-Dinitrophenol U 3.25 10.0 1 11/07/2019 07:48 WG1375392
2-Nitrophenol U 0.320 10.0 1 11/07/2019 07:48 WG1375392
4-Nitrophenol U 2.01 10.0 1 11/07/2019 07:48 WG1375392
Pentachlorophenol U 0.313 10.0 1 11/07/2019 07:48 WG1375392
Phenol 1.76 J 0.334 10.0 1 11/07/2019 07:48 WG1375392
2,4,6-Trichlorophenol U 0.297 10.0 1 11/07/2019 07:48 WG1375392
(S) 2-Fluorophenol 44.9 10.0-120 11/07/2019 07:48 WG1375392
(S) Phenol-d5 29.5 8.00-424 11/07/2019 07:48 WG1375392
(S) Nitrobenzene-d5 57.3 15.0-314 11/07/2019 07:48 WG1375392
(S) 2-Fluorobiphenyl 68.5 22.0-127 11/07/2019 07:48 WG1375392
(S) 2,4,6-Tribromophenol 83.0 10.0-153 11/07/2019 07:48 WG1375392
(S) p-Terphenyl-d14 81.1 29.0-141 11/07/2019 07:48 WG1375392
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L1155985
MW-1
Collected date/time: 10/30/19 12:00
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 - TENTATIVELY IDENTIFIED COMPOUNDS
Result Qualifier MDL RDL Dilution Analysis Batch CAS #
Analyte ug/l ug/l ug/l date / time
Unknown-02 55.7 J N 0.000 0.000 1 11/07/2019 07:48 WG1375392 000000-00-0
[1,2'-Binaphthalene]-5,5',8,8'-T
et 18.3 J N 0.000 0.000 1 11/07/2019 07:48 WG1375392 020175-84-2
Unknown-04 14.6 J N 0.000 0.000 1 11/07/2019 07:48 WG1375392 055517-90-3
Unknown-03 11.5 J N 0.000 0.000 1 11/07/2019 07:48 WG1375392 000112-95-8
Unknown-01 4.58 J N 0.000 0.000 1 11/07/2019 07:48 WG1375392 003404-73-7
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds. Therefore, not all TICs are identified and quantitated using individual standards. TIC
listings are prepared utilizing a computerized library search routine of electron impact mass spectral data and evaluation of the relevant data by a mass spectral data specialist. Quantitation is
accomplished by relative peak area of the TIC compared to that of the nearest internal standard from the total ion chromatogram. TICs are identified and quantitated only if the peak area is
10% or more of that of the nearest internal standard.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L1155985
MW-2
Collected date/time: 10/30/19 13:00
Metals (ICP) by Method 6010D
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Lead 37.9 1.90 5.00 1 11/05/2019 13:30 WG1374911
Volatile Petroleum Hydrocarbons by Method MADEPV
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics 118 33.3 100 1 11/07/2019 00:10 WG1373778
Unadjusted C9-C12 Aliphatics 233 33.3 100 1 11/07/2019 00:10 WG1373778
Unadjusted C9-C10 Aromatics 90.0 J 33.3 100 1 11/07/2019 00:10 WG1373778
Total VPH 441 33.3 100 1 11/07/2019 00:10 WG1373778
(S) 2,5-Dibromotoluene(FID) 102 70.0-130 11/07/2019 00:10 WG1373778
(S) 2,5-Dibromotoluene(PID) 99.9 70.0-130 11/07/2019 00:10 WG1373778
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acetone U 10.0 50.0 1 11/02/2019 19:03 WG1374034
Acrolein U 8.87 50.0 1 11/02/2019 19:03 WG1374034
Acrylonitrile U 1.87 10.0 1 11/02/2019 19:03 WG1374034
Benzene 2.42 0.331 1.00 1 11/02/2019 19:03 WG1374034
Bromobenzene U 0.352 1.00 1 11/02/2019 19:03 WG1374034
Bromochloromethane U 0.520 1.00 1 11/02/2019 19:03 WG1374034
Bromodichloromethane U 0.380 1.00 1 11/02/2019 19:03 WG1374034
Bromoform U 0.469 1.00 1 11/02/2019 19:03 WG1374034
Bromomethane U 0.866 5.00 1 11/02/2019 19:03 WG1374034
n-Butylbenzene 0.462 J 0.361 1.00 1 11/02/2019 19:03 WG1374034
sec-Butylbenzene U 0.365 1.00 1 11/02/2019 19:03 WG1374034
tert-Butylbenzene U 0.399 1.00 1 11/02/2019 19:03 WG1374034
Carbon tetrachloride U 0.379 1.00 1 11/02/2019 19:03 WG1374034
Chlorobenzene U 0.348 1.00 1 11/02/2019 19:03 WG1374034
Chlorodibromomethane U 0.327 1.00 1 11/02/2019 19:03 WG1374034
Chloroethane U 0.453 5.00 1 11/02/2019 19:03 WG1374034
Chloroform U 0.324 5.00 1 11/02/2019 19:03 WG1374034
Chloromethane U 0.276 2.50 1 11/02/2019 19:03 WG1374034
2-Chlorotoluene U 0.375 1.00 1 11/02/2019 19:03 WG1374034
4-Chlorotoluene U 0.351 1.00 1 11/02/2019 19:03 WG1374034
1,2-Dibromo-3-Chloropropane U 1.33 5.00 1 11/02/2019 19:03 WG1374034
1,2-Dibromoethane U 0.381 1.00 1 11/02/2019 19:03 WG1374034
Dibromomethane U 0.346 1.00 1 11/02/2019 19:03 WG1374034
1,2-Dichlorobenzene U 0.349 1.00 1 11/02/2019 19:03 WG1374034
1,3-Dichlorobenzene U 0.220 1.00 1 11/02/2019 19:03 WG1374034
1,4-Dichlorobenzene U 0.274 1.00 1 11/02/2019 19:03 WG1374034
Dichlorodifluoromethane U 0.551 5.00 1 11/02/2019 19:03 WG1374034
1,1-Dichloroethane U 0.259 1.00 1 11/02/2019 19:03 WG1374034
1,2-Dichloroethane U 0.361 1.00 1 11/02/2019 19:03 WG1374034
1,1-Dichloroethene U 0.398 1.00 1 11/02/2019 19:03 WG1374034
cis-1,2-Dichloroethene U 0.260 1.00 1 11/02/2019 19:03 WG1374034
trans-1,2-Dichloroethene U 0.396 1.00 1 11/02/2019 19:03 WG1374034
1,2-Dichloropropane U 0.306 1.00 1 11/02/2019 19:03 WG1374034
1,1-Dichloropropene U 0.352 1.00 1 11/02/2019 19:03 WG1374034
1,3-Dichloropropane U 0.366 1.00 1 11/02/2019 19:03 WG1374034
cis-1,3-Dichloropropene U 0.418 1.00 1 11/02/2019 19:03 WG1374034
trans-1,3-Dichloropropene U 0.419 1.00 1 11/02/2019 19:03 WG1374034
2,2-Dichloropropane U 0.321 1.00 1 11/02/2019 19:03 WG1374034
Di-isopropyl ether U 0.320 1.00 1 11/02/2019 19:03 WG1374034
Ethylbenzene 0.570 J 0.384 1.00 1 11/02/2019 19:03 WG1374034
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L1155985
MW-2
Collected date/time: 10/30/19 13:00
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Hexachloro-1,3-butadiene U 0.256 1.00 1 11/02/2019 19:03 WG1374034
2-Hexanone U 3.82 10.0 1 11/02/2019 19:03 WG1374034
Isopropylbenzene 0.674 J 0.326 1.00 1 11/02/2019 19:03 WG1374034
p-Isopropyltoluene U 0.350 1.00 1 11/02/2019 19:03 WG1374034
2-Butanone (MEK)U 3.93 10.0 1 11/02/2019 19:03 WG1374034
Methylene Chloride U 1.00 5.00 1 11/02/2019 19:03 WG1374034
4-Methyl-2-pentanone (MIBK) U 2.14 10.0 1 11/02/2019 19:03 WG1374034
Methyl tert-butyl ether U 0.367 1.00 1 11/02/2019 19:03 WG1374034
Naphthalene 1.85 J 1.00 5.00 1 11/02/2019 19:03 WG1374034
n-Propylbenzene 1.15 0.349 1.00 1 11/02/2019 19:03 WG1374034
Styrene U 0.307 1.00 1 11/02/2019 19:03 WG1374034
1,1,1,2-Tetrachloroethane U 0.385 1.00 1 11/02/2019 19:03 WG1374034
1,1,2,2-Tetrachloroethane U 0.130 1.00 1 11/02/2019 19:03 WG1374034
Tetrachloroethene U 0.372 1.00 1 11/02/2019 19:03 WG1374034
Toluene 2.21 0.412 1.00 1 11/02/2019 19:03 WG1374034
1,2,3-Trichlorobenzene U 0.230 1.00 1 11/02/2019 19:03 WG1374034
1,2,4-Trichlorobenzene U 0.355 1.00 1 11/02/2019 19:03 WG1374034
1,1,1-Trichloroethane U 0.319 1.00 1 11/02/2019 19:03 WG1374034
1,1,2-Trichloroethane U 0.383 1.00 1 11/02/2019 19:03 WG1374034
Trichloroethene U 0.398 1.00 1 11/02/2019 19:03 WG1374034
Trichlorofluoromethane U 1.20 5.00 1 11/02/2019 19:03 WG1374034
1,2,3-Trichloropropane U 0.807 2.50 1 11/02/2019 19:03 WG1374034
1,2,4-Trimethylbenzene 18.4 0.373 1.00 1 11/02/2019 19:03 WG1374034
1,3,5-Trimethylbenzene 6.77 0.387 1.00 1 11/02/2019 19:03 WG1374034
Vinyl acetate U 1.63 10.0 1 11/02/2019 19:03 WG1374034
Vinyl chloride U 0.259 1.00 1 11/02/2019 19:03 WG1374034
o-Xylene 19.2 0.341 1.00 1 11/02/2019 19:03 WG1374034
m&p-Xylenes 24.1 0.719 2.00 1 11/02/2019 19:03 WG1374034
(S) Toluene-d8 91.6 80.0-120 11/02/2019 19:03 WG1374034
(S) 4-Bromofluorobenzene 89.8 77.0-126 11/02/2019 19:03 WG1374034
(S) 1,2-Dichloroethane-d4 91.1 70.0-130 11/02/2019 19:03 WG1374034
TPH by Method MADEPE
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics 160 B 33.3 100 1 11/06/2019 05:33 WG1375597
Unadjusted C19-C36 Aliphatics 568 B 33.3 100 1 11/06/2019 05:33 WG1375597
Unadjusted C11-C22 Aromatics 164 B 33.3 100 1 11/06/2019 06:38 WG1375597
Unadjusted Total Petroleum
Hydrocarbons 892 33.3 100 1 11/06/2019 06:38 WG1375597
(S) o-Terphenyl 18.4 J2 40.0-140 11/06/2019 06:38 WG1375597
(S) 1-Chloro-octadecane 17.3 J2 40.0-140 11/06/2019 05:33 WG1375597
(S) 2-Fluorobiphenyl 83.6 40.0-140 11/06/2019 06:38 WG1375597
(S) 2-Bromonaphthalene 79.1 40.0-140 11/06/2019 06:38 WG1375597
Sample Narrative:
L1155985-02 WG1375597: Sample produced heavy emulsion during Extraction process, low surr/spike recoveries due to matrix
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Acenaphthene U 0.316 1.00 1 11/07/2019 08:08 WG1375392
Acenaphthylene U 0.309 1.00 1 11/07/2019 08:08 WG1375392
Anthracene U 0.291 1.00 1 11/07/2019 08:08 WG1375392
Benzidine U 4.32 10.0 1 11/07/2019 08:08 WG1375392
Benzo(a)anthracene U 0.0975 1.00 1 11/07/2019 08:08 WG1375392
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1155985 11/08/19 11:37 10 of 27
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L1155985
MW-2
Collected date/time: 10/30/19 13:00
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte ug/l ug/l ug/l date / time
Benzo(b)fluoranthene U 0.0896 1.00 1 11/07/2019 08:08 WG1375392
Benzo(k)fluoranthene U 0.355 1.00 1 11/07/2019 08:08 WG1375392
Benzo(g,h,i)perylene U 0.161 1.00 1 11/07/2019 08:08 WG1375392
Benzo(a)pyrene U 0.340 1.00 1 11/07/2019 08:08 WG1375392
Bis(2-chlorethoxy)methane U 0.329 10.0 1 11/07/2019 08:08 WG1375392
Bis(2-chloroethyl)ether U 1.62 10.0 1 11/07/2019 08:08 WG1375392
Bis(2-chloroisopropyl)ether U 0.445 10.0 1 11/07/2019 08:08 WG1375392
4-Bromophenyl-phenylether U 0.335 10.0 1 11/07/2019 08:08 WG1375392
2-Chloronaphthalene U 0.330 1.00 1 11/07/2019 08:08 WG1375392
4-Chlorophenyl-phenylether U 0.303 10.0 1 11/07/2019 08:08 WG1375392
Chrysene U 0.332 1.00 1 11/07/2019 08:08 WG1375392
Dibenz(a,h)anthracene U 0.279 1.00 1 11/07/2019 08:08 WG1375392
3,3-Dichlorobenzidine U 2.02 10.0 1 11/07/2019 08:08 WG1375392
2,4-Dinitrotoluene U 1.65 10.0 1 11/07/2019 08:08 WG1375392
2,6-Dinitrotoluene U 0.279 10.0 1 11/07/2019 08:08 WG1375392
Fluoranthene U 0.310 1.00 1 11/07/2019 08:08 WG1375392
Fluorene U 0.323 1.00 1 11/07/2019 08:08 WG1375392
Hexachlorobenzene U 0.341 1.00 1 11/07/2019 08:08 WG1375392
Hexachloro-1,3-butadiene U 0.329 10.0 1 11/07/2019 08:08 WG1375392
Hexachlorocyclopentadiene U 2.33 10.0 1 11/07/2019 08:08 WG1375392
Hexachloroethane U 0.365 10.0 1 11/07/2019 08:08 WG1375392
Indeno(1,2,3-cd)pyrene U 0.279 1.00 1 11/07/2019 08:08 WG1375392
Isophorone U 0.272 10.0 1 11/07/2019 08:08 WG1375392
Naphthalene 0.755 J 0.372 1.00 1 11/07/2019 08:08 WG1375392
Nitrobenzene U 0.367 10.0 1 11/07/2019 08:08 WG1375392
n-Nitrosodimethylamine U 1.26 10.0 1 11/07/2019 08:08 WG1375392
n-Nitrosodiphenylamine U 1.19 10.0 1 11/07/2019 08:08 WG1375392
n-Nitrosodi-n-propylamine U 0.403 10.0 1 11/07/2019 08:08 WG1375392
Phenanthrene U 0.366 1.00 1 11/07/2019 08:08 WG1375392
Benzylbutyl phthalate U 0.275 3.00 1 11/07/2019 08:08 WG1375392
Bis(2-ethylhexyl)phthalate U 0.709 3.00 1 11/07/2019 08:08 WG1375392
Di-n-butyl phthalate U 0.266 3.00 1 11/07/2019 08:08 WG1375392
Diethyl phthalate U 0.282 3.00 1 11/07/2019 08:08 WG1375392
Dimethyl phthalate U 0.283 3.00 1 11/07/2019 08:08 WG1375392
Di-n-octyl phthalate U 0.278 3.00 1 11/07/2019 08:08 WG1375392
Pyrene U 0.330 1.00 1 11/07/2019 08:08 WG1375392
1,2,4-Trichlorobenzene U 0.355 10.0 1 11/07/2019 08:08 WG1375392
4-Chloro-3-methylphenol U 0.263 10.0 1 11/07/2019 08:08 WG1375392
2-Chlorophenol U 0.283 10.0 1 11/07/2019 08:08 WG1375392
2,4-Dichlorophenol U 0.284 10.0 1 11/07/2019 08:08 WG1375392
2,4-Dimethylphenol U 0.624 10.0 1 11/07/2019 08:08 WG1375392
4,6-Dinitro-2-methylphenol U 2.62 10.0 1 11/07/2019 08:08 WG1375392
2,4-Dinitrophenol U 3.25 10.0 1 11/07/2019 08:08 WG1375392
2-Nitrophenol U 0.320 10.0 1 11/07/2019 08:08 WG1375392
4-Nitrophenol U 2.01 10.0 1 11/07/2019 08:08 WG1375392
Pentachlorophenol U 0.313 10.0 1 11/07/2019 08:08 WG1375392
Phenol 3.75 J 0.334 10.0 1 11/07/2019 08:08 WG1375392
2,4,6-Trichlorophenol U 0.297 10.0 1 11/07/2019 08:08 WG1375392
(S) 2-Fluorophenol 41.8 10.0-120 11/07/2019 08:08 WG1375392
(S) Phenol-d5 26.4 8.00-424 11/07/2019 08:08 WG1375392
(S) Nitrobenzene-d5 51.4 15.0-314 11/07/2019 08:08 WG1375392
(S) 2-Fluorobiphenyl 63.5 22.0-127 11/07/2019 08:08 WG1375392
(S) 2,4,6-Tribromophenol 72.5 10.0-153 11/07/2019 08:08 WG1375392
(S) p-Terphenyl-d14 64.8 29.0-141 11/07/2019 08:08 WG1375392
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1155985 11/08/19 11:37 11 of 27
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L1155985
MW-2
Collected date/time: 10/30/19 13:00
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 - TENTATIVELY IDENTIFIED COMPOUNDS
Result Qualifier MDL RDL Dilution Analysis Batch CAS #
Analyte ug/l ug/l ug/l date / time
Benzene, 1,3-Dimethyl- 10.1 J N 0.000 0.000 1 11/07/2019 08:08 WG1375392 000108-38-3
Unknown-01 7.50 J N 0.000 0.000 1 11/07/2019 08:08 WG1375392 005076-19-7
Heptadecane 5.02 J N 0.000 0.000 1 11/07/2019 08:08 WG1375392 000629-78-7
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds. Therefore, not all TICs are identified and quantitated using individual standards. TIC
listings are prepared utilizing a computerized library search routine of electron impact mass spectral data and evaluation of the relevant data by a mass spectral data specialist. Quantitation is
accomplished by relative peak area of the TIC compared to that of the nearest internal standard from the total ion chromatogram. TICs are identified and quantitated only if the peak area is
10% or more of that of the nearest internal standard.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1374911
Metals (ICP) by Method 6010D L1155985-01,02
Method Blank (MB)
(MB) R3468800-1 11/05/19 12:37
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Lead U 1.90 5.00
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3468800-2 11/05/19 12:39 • (LCSD) R3468800-3 11/05/19 12:42
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Lead 1000 980 983 98.0 98.3 80.0-120 0.310 20
L1155079-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1155079-05 11/05/19 12:45 • (MS) R3468800-5 11/05/19 12:50 • (MSD) R3468800-6 11/05/19 12:52
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Lead 1000 ND 979 988 97.9 98.8 1 75.0-125 0.918 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1373778
Volatile Petroleum Hydrocarbons by Method MADEPV L1155985-01,02
Method Blank (MB)
(MB) R3469775-3 11/06/19 01:43
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C5-C8 Aliphatics U 33.3 100
Unadjusted C9-C12 Aliphatics U 33.3 100
Unadjusted C9-C10 Aromatics U 33.3 100
Total VPH U 33.3 100
(S) 2,5-Dibromotoluene(FID) 85.1 70.0-130
(S) 2,5-Dibromotoluene(PID) 85.2 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3469775-1 11/05/19 23:35 • (LCSD) R3469775-2 11/06/19 00:07
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C5-C8 Aliphatics 1200 1230 1230 103 103 70.0-130 0.000 25
Unadjusted C9-C12 Aliphatics 1400 1530 1540 109 110 70.0-130 0.651 25
Unadjusted C9-C10 Aromatics 200 207 207 104 104 70.0-130 0.000 25
Total VPH 2800 2970 2980 106 106 70.0-130 0.336 25
(S) 2,5-Dibromotoluene(FID) 101 97.4 70.0-130
(S) 2,5-Dibromotoluene(PID) 99.6 96.6 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1374034
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 L1155985-01,02
Method Blank (MB)
(MB) R3467950-3 11/02/19 11:31
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Acetone U 10.0 50.0
Acrolein U 8.87 50.0
Acrylonitrile U 1.87 10.0
Benzene U 0.331 1.00
Bromobenzene U 0.352 1.00
Bromodichloromethane U 0.380 1.00
Bromochloromethane U 0.520 1.00
Bromoform U 0.469 1.00
Bromomethane U 0.866 5.00
n-Butylbenzene U 0.361 1.00
sec-Butylbenzene U 0.365 1.00
tert-Butylbenzene U 0.399 1.00
Carbon tetrachloride U 0.379 1.00
Chlorobenzene U 0.348 1.00
Chlorodibromomethane U 0.327 1.00
Chloroethane U 0.453 5.00
Chloroform U 0.324 5.00
Chloromethane U 0.276 2.50
2-Chlorotoluene U 0.375 1.00
4-Chlorotoluene U 0.351 1.00
1,2-Dibromo-3-Chloropropane U 1.33 5.00
1,2-Dibromoethane U 0.381 1.00
Dibromomethane U 0.346 1.00
1,2-Dichlorobenzene U 0.349 1.00
1,3-Dichlorobenzene U 0.220 1.00
1,4-Dichlorobenzene U 0.274 1.00
Dichlorodifluoromethane U 0.551 5.00
1,1-Dichloroethane U 0.259 1.00
1,2-Dichloroethane U 0.361 1.00
1,1-Dichloroethene U 0.398 1.00
cis-1,2-Dichloroethene U 0.260 1.00
trans-1,2-Dichloroethene U 0.396 1.00
1,2-Dichloropropane U 0.306 1.00
1,1-Dichloropropene U 0.352 1.00
1,3-Dichloropropane U 0.366 1.00
cis-1,3-Dichloropropene U 0.418 1.00
trans-1,3-Dichloropropene U 0.419 1.00
2,2-Dichloropropane U 0.321 1.00
Di-isopropyl ether U 0.320 1.00
Ethylbenzene U 0.384 1.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Withers & Ravenel Eng. - Standard 02180080.10 L1155985 11/08/19 11:37 15 of 27
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1374034
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 L1155985-01,02
Method Blank (MB)
(MB) R3467950-3 11/02/19 11:31
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Hexachloro-1,3-butadiene U 0.256 1.00
2-Hexanone U 3.82 10.0
Isopropylbenzene U 0.326 1.00
p-Isopropyltoluene U 0.350 1.00
2-Butanone (MEK)U 3.93 10.0
Methylene Chloride U 1.00 5.00
4-Methyl-2-pentanone (MIBK) U 2.14 10.0
Methyl tert-butyl ether U 0.367 1.00
Naphthalene U 1.00 5.00
n-Propylbenzene U 0.349 1.00
Styrene U 0.307 1.00
1,1,1,2-Tetrachloroethane U 0.385 1.00
1,1,2,2-Tetrachloroethane U 0.130 1.00
Tetrachloroethene U 0.372 1.00
Toluene U 0.412 1.00
1,2,3-Trichlorobenzene U 0.230 1.00
1,2,4-Trichlorobenzene U 0.355 1.00
1,1,1-Trichloroethane U 0.319 1.00
1,1,2-Trichloroethane U 0.383 1.00
Trichloroethene U 0.398 1.00
Trichlorofluoromethane U 1.20 5.00
1,2,3-Trichloropropane U 0.807 2.50
1,2,4-Trimethylbenzene U 0.373 1.00
1,3,5-Trimethylbenzene U 0.387 1.00
Vinyl acetate U 1.63 10.0
Vinyl chloride U 0.259 1.00
o-Xylene U 0.341 1.00
m&p-Xylenes U 0.719 2.00
(S) Toluene-d8 95.1 80.0-120
(S) 4-Bromofluorobenzene 91.8 77.0-126
(S) 1,2-Dichloroethane-d4 92.6 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3467950-1 11/02/19 10:32 • (LCSD) R3467950-2 11/02/19 10:52
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Acetone 25.0 32.7 29.2 131 117 19.0-160 11.3 27
Acrolein 25.0 26.3 23.8 105 95.2 10.0-160 9.98 26
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1374034
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 L1155985-01,02
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3467950-1 11/02/19 10:32 • (LCSD) R3467950-2 11/02/19 10:52
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Acrylonitrile 25.0 25.6 23.4 102 93.6 55.0-149 8.98 20
Benzene 5.00 4.45 4.13 89.0 82.6 70.0-123 7.46 20
Bromobenzene 5.00 4.63 4.36 92.6 87.2 73.0-121 6.01 20
Bromodichloromethane 5.00 4.63 4.12 92.6 82.4 75.0-120 11.7 20
Bromochloromethane 5.00 5.52 4.87 110 97.4 76.0-122 12.5 20
Bromoform 5.00 4.61 4.27 92.2 85.4 68.0-132 7.66 20
Bromomethane 5.00 4.88 4.12 97.6 82.4 10.0-160 16.9 25
n-Butylbenzene 5.00 4.58 4.34 91.6 86.8 73.0-125 5.38 20
sec-Butylbenzene 5.00 4.43 4.21 88.6 84.2 75.0-125 5.09 20
tert-Butylbenzene 5.00 4.47 4.16 89.4 83.2 76.0-124 7.18 20
Carbon tetrachloride 5.00 4.17 3.87 83.4 77.4 68.0-126 7.46 20
Chlorobenzene 5.00 4.70 4.41 94.0 88.2 80.0-121 6.37 20
Chlorodibromomethane 5.00 4.67 4.30 93.4 86.0 77.0-125 8.25 20
Chloroethane 5.00 4.36 3.85 87.2 77.0 47.0-150 12.4 20
Chloroform 5.00 4.49 4.20 89.8 84.0 73.0-120 6.67 20
Chloromethane 5.00 4.24 3.74 84.8 74.8 41.0-142 12.5 20
2-Chlorotoluene 5.00 4.62 4.51 92.4 90.2 76.0-123 2.41 20
4-Chlorotoluene 5.00 4.55 4.46 91.0 89.2 75.0-122 2.00 20
1,2-Dibromo-3-Chloropropane 5.00 4.35 4.02 87.0 80.4 58.0-134 7.89 20
1,2-Dibromoethane 5.00 4.71 4.43 94.2 88.6 80.0-122 6.13 20
Dibromomethane 5.00 4.97 4.38 99.4 87.6 80.0-120 12.6 20
1,2-Dichlorobenzene 5.00 4.61 4.41 92.2 88.2 79.0-121 4.43 20
1,3-Dichlorobenzene 5.00 4.62 4.42 92.4 88.4 79.0-120 4.42 20
1,4-Dichlorobenzene 5.00 4.50 4.45 90.0 89.0 79.0-120 1.12 20
Dichlorodifluoromethane 5.00 4.54 4.28 90.8 85.6 51.0-149 5.90 20
1,1-Dichloroethane 5.00 4.75 4.31 95.0 86.2 70.0-126 9.71 20
1,2-Dichloroethane 5.00 4.55 4.41 91.0 88.2 70.0-128 3.13 20
1,1-Dichloroethene 5.00 4.47 4.19 89.4 83.8 71.0-124 6.47 20
cis-1,2-Dichloroethene 5.00 4.88 4.44 97.6 88.8 73.0-120 9.44 20
trans-1,2-Dichloroethene 5.00 4.52 4.27 90.4 85.4 73.0-120 5.69 20
1,2-Dichloropropane 5.00 4.93 4.30 98.6 86.0 77.0-125 13.7 20
1,1-Dichloropropene 5.00 4.33 4.09 86.6 81.8 74.0-126 5.70 20
1,3-Dichloropropane 5.00 4.80 4.46 96.0 89.2 80.0-120 7.34 20
cis-1,3-Dichloropropene 5.00 4.57 4.19 91.4 83.8 80.0-123 8.68 20
trans-1,3-Dichloropropene 5.00 4.66 4.37 93.2 87.4 78.0-124 6.42 20
2,2-Dichloropropane 5.00 4.44 4.22 88.8 84.4 58.0-130 5.08 20
Di-isopropyl ether 5.00 4.89 4.48 97.8 89.6 58.0-138 8.75 20
Ethylbenzene 5.00 4.48 4.32 89.6 86.4 79.0-123 3.64 20
Hexachloro-1,3-butadiene 5.00 4.59 4.76 91.8 95.2 54.0-138 3.64 20
2-Hexanone 25.0 24.9 23.0 99.6 92.0 67.0-149 7.93 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1374034
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 L1155985-01,02
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3467950-1 11/02/19 10:32 • (LCSD) R3467950-2 11/02/19 10:52
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Isopropylbenzene 5.00 4.39 4.15 87.8 83.0 76.0-127 5.62 20
p-Isopropyltoluene 5.00 4.52 4.22 90.4 84.4 76.0-125 6.86 20
2-Butanone (MEK)25.0 28.0 25.3 112 101 44.0-160 10.1 20
Methylene Chloride 5.00 4.92 4.38 98.4 87.6 67.0-120 11.6 20
4-Methyl-2-pentanone (MIBK) 25.0 23.6 21.6 94.4 86.4 68.0-142 8.85 20
Methyl tert-butyl ether 5.00 4.74 4.32 94.8 86.4 68.0-125 9.27 20
Naphthalene 5.00 3.97 4.05 79.4 81.0 54.0-135 2.00 20
n-Propylbenzene 5.00 4.49 4.32 89.8 86.4 77.0-124 3.86 20
Styrene 5.00 4.68 4.46 93.6 89.2 73.0-130 4.81 20
1,1,1,2-Tetrachloroethane 5.00 4.56 4.31 91.2 86.2 75.0-125 5.64 20
1,1,2,2-Tetrachloroethane 5.00 4.60 4.32 92.0 86.4 65.0-130 6.28 20
Tetrachloroethene 5.00 4.38 4.11 87.6 82.2 72.0-132 6.36 20
Toluene 5.00 4.42 4.10 88.4 82.0 79.0-120 7.51 20
1,2,3-Trichlorobenzene 5.00 4.10 4.15 82.0 83.0 50.0-138 1.21 20
1,2,4-Trichlorobenzene 5.00 4.05 4.15 81.0 83.0 57.0-137 2.44 20
1,1,1-Trichloroethane 5.00 4.66 4.39 93.2 87.8 73.0-124 5.97 20
1,1,2-Trichloroethane 5.00 4.64 4.25 92.8 85.0 80.0-120 8.77 20
Trichloroethene 5.00 4.70 4.34 94.0 86.8 78.0-124 7.96 20
Trichlorofluoromethane 5.00 4.32 4.02 86.4 80.4 59.0-147 7.19 20
1,2,3-Trichloropropane 5.00 4.74 4.35 94.8 87.0 73.0-130 8.58 20
1,2,4-Trimethylbenzene 5.00 4.67 4.46 93.4 89.2 76.0-121 4.60 20
1,3,5-Trimethylbenzene 5.00 4.58 4.32 91.6 86.4 76.0-122 5.84 20
Vinyl acetate 25.0 24.6 22.5 98.4 90.0 11.0-160 8.92 20
Vinyl chloride 5.00 4.05 3.77 81.0 75.4 67.0-131 7.16 20
o-Xylene 5.00 4.29 4.10 85.8 82.0 80.0-122 4.53 20
m&p-Xylenes 10.0 8.78 8.47 87.8 84.7 80.0-122 3.59 20
(S) Toluene-d8 90.5 92.9 80.0-120
(S) 4-Bromofluorobenzene 92.8 91.3 77.0-126
(S) 1,2-Dichloroethane-d4 93.3 93.1 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1375597
TPH by Method MADEPE L1155985-01,02
Method Blank (MB)
(MB) R3469044-1 11/06/19 01:12
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C9-C18 Aliphatics 37.5 J 33.3 100
Unadjusted C19-C36 Aliphatics 58.0 J 33.3 100
(S) 1-Chloro-octadecane 81.9 40.0-140
Method Blank (MB)
(MB) R3469044-4 11/06/19 02:18
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C11-C22 Aromatics 86.3 J 33.3 100
(S) o-Terphenyl 79.9 40.0-140
(S) 2-Fluorobiphenyl 90.5 40.0-140
(S) 2-Bromonaphthalene 84.4 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3469044-2 11/06/19 01:34 • (LCSD) R3469044-3 11/06/19 01:56
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C9-C18 Aliphatics 600 386 399 64.3 66.5 40.0-140 3.31 25
Unadjusted C19-C36 Aliphatics 800 640 670 80.0 83.8 40.0-140 4.58 25
(S) 1-Chloro-octadecane 74.4 72.5 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3469044-5 11/06/19 02:39 • (LCSD) R3469044-6 11/06/19 03:01
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C11-C22 Aromatics 1700 1280 1380 75.3 81.2 40.0-140 7.52 25
(S) o-Terphenyl 78.3 83.1 40.0-140
(S) 2-Fluorobiphenyl 88.9 90.0 40.0-140
(S) 2-Bromonaphthalene 85.4 86.3 40.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1375392
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1155985-01,02
Method Blank (MB)
(MB) R3469628-2 11/06/19 14:51
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Acenaphthene U 0.316 1.00
Acenaphthylene U 0.309 1.00
Anthracene U 0.291 1.00
Benzidine U 4.32 10.0
Benzo(a)anthracene U 0.0975 1.00
Benzo(b)fluoranthene U 0.0896 1.00
Benzo(k)fluoranthene U 0.355 1.00
Benzo(g,h,i)perylene U 0.161 1.00
Benzo(a)pyrene U 0.340 1.00
Bis(2-chlorethoxy)methane U 0.329 10.0
Bis(2-chloroethyl)ether U 1.62 10.0
Bis(2-chloroisopropyl)ether U 0.445 10.0
4-Bromophenyl-phenylether U 0.335 10.0
2-Chloronaphthalene U 0.330 1.00
4-Chlorophenyl-phenylether U 0.303 10.0
Chrysene U 0.332 1.00
Dibenz(a,h)anthracene U 0.279 1.00
3,3-Dichlorobenzidine U 2.02 10.0
2,4-Dinitrotoluene U 1.65 10.0
2,6-Dinitrotoluene U 0.279 10.0
Fluoranthene U 0.310 1.00
Fluorene U 0.323 1.00
Hexachlorobenzene U 0.341 1.00
Hexachloro-1,3-butadiene U 0.329 10.0
Hexachlorocyclopentadiene U 2.33 10.0
Hexachloroethane U 0.365 10.0
Indeno(1,2,3-cd)pyrene U 0.279 1.00
Isophorone U 0.272 10.0
Naphthalene U 0.372 1.00
Nitrobenzene U 0.367 10.0
n-Nitrosodimethylamine U 1.26 10.0
n-Nitrosodiphenylamine U 1.19 10.0
n-Nitrosodi-n-propylamine U 0.403 10.0
Phenanthrene U 0.366 1.00
Benzylbutyl phthalate U 0.275 3.00
Bis(2-ethylhexyl)phthalate U 0.709 3.00
Di-n-butyl phthalate U 0.266 3.00
Diethyl phthalate U 0.282 3.00
Dimethyl phthalate U 0.283 3.00
Di-n-octyl phthalate U 0.278 3.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1155985 11/08/19 11:37 20 of 27
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1375392
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1155985-01,02
Method Blank (MB)
(MB) R3469628-2 11/06/19 14:51
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Pyrene U 0.330 1.00
1,2,4-Trichlorobenzene U 0.355 10.0
4-Chloro-3-methylphenol U 0.263 10.0
2-Chlorophenol U 0.283 10.0
2,4-Dichlorophenol U 0.284 10.0
2,4-Dimethylphenol U 0.624 10.0
4,6-Dinitro-2-methylphenol U 2.62 10.0
2,4-Dinitrophenol U 3.25 10.0
2-Nitrophenol U 0.320 10.0
4-Nitrophenol U 2.01 10.0
Pentachlorophenol U 0.313 10.0
Phenol U 0.334 10.0
2,4,6-Trichlorophenol U 0.297 10.0
(S) Nitrobenzene-d5 63.3 15.0-314
(S) 2-Fluorobiphenyl 72.4 22.0-127
(S) p-Terphenyl-d14 75.5 29.0-141
(S) Phenol-d5 30.5 8.00-424
(S) 2-Fluorophenol 47.3 10.0-120
(S) 2,4,6-Tribromophenol 74.0 10.0-153
Laboratory Control Sample (LCS)
(LCS) R3469628-1 11/06/19 14:31
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Acenaphthene 50.0 31.0 62.0 47.0-145
Acenaphthylene 50.0 33.0 66.0 33.0-145
Anthracene 50.0 33.7 67.4 27.0-133
Benzidine 100 30.0 30.0 1.00-120
Benzo(a)anthracene 50.0 34.7 69.4 33.0-143
Benzo(b)fluoranthene 50.0 34.0 68.0 24.0-159
Benzo(k)fluoranthene 50.0 33.8 67.6 11.0-162
Benzo(g,h,i)perylene 50.0 33.2 66.4 1.00-219
Benzo(a)pyrene 50.0 35.2 70.4 17.0-163
Bis(2-chlorethoxy)methane 50.0 28.7 57.4 1.00-219
Bis(2-chloroethyl)ether 50.0 31.8 63.6 33.0-185
Bis(2-chloroisopropyl)ether 50.0 29.8 59.6 36.0-166
4-Bromophenyl-phenylether 50.0 35.3 70.6 53.0-127
2-Chloronaphthalene 50.0 31.4 62.8 60.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Withers & Ravenel Eng. - Standard 02180080.10 L1155985 11/08/19 11:37 21 of 27
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1375392
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1155985-01,02
Laboratory Control Sample (LCS)
(LCS) R3469628-1 11/06/19 14:31
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
4-Chlorophenyl-phenylether 50.0 32.9 65.8 25.0-158
Chrysene 50.0 33.5 67.0 17.0-168
Dibenz(a,h)anthracene 50.0 33.5 67.0 1.00-227
3,3-Dichlorobenzidine 100 70.9 70.9 1.00-262
2,4-Dinitrotoluene 50.0 34.4 68.8 39.0-139
2,6-Dinitrotoluene 50.0 33.0 66.0 50.0-158
Fluoranthene 50.0 33.4 66.8 26.0-137
Fluorene 50.0 33.2 66.4 59.0-121
Hexachlorobenzene 50.0 34.1 68.2 1.00-152
Hexachloro-1,3-butadiene 50.0 29.2 58.4 24.0-120
Hexachlorocyclopentadiene 50.0 27.9 55.8 10.0-120
Hexachloroethane 50.0 28.4 56.8 40.0-120
Indeno(1,2,3-cd)pyrene 50.0 33.5 67.0 1.00-171
Isophorone 50.0 29.3 58.6 21.0-196
Naphthalene 50.0 27.6 55.2 21.0-133
Nitrobenzene 50.0 28.5 57.0 35.0-180
n-Nitrosodimethylamine 50.0 19.8 39.6 10.0-120
n-Nitrosodiphenylamine 50.0 34.5 69.0 44.0-120
n-Nitrosodi-n-propylamine 50.0 30.6 61.2 1.00-230
Phenanthrene 50.0 32.8 65.6 54.0-120
Benzylbutyl phthalate 50.0 36.6 73.2 1.00-152
Bis(2-ethylhexyl)phthalate 50.0 36.7 73.4 8.00-158
Di-n-butyl phthalate 50.0 36.5 73.0 1.00-120
Diethyl phthalate 50.0 33.4 66.8 1.00-120
Dimethyl phthalate 50.0 32.8 65.6 1.00-120
Di-n-octyl phthalate 50.0 36.2 72.4 4.00-146
Pyrene 50.0 34.3 68.6 52.0-120
1,2,4-Trichlorobenzene 50.0 28.5 57.0 44.0-142
4-Chloro-3-methylphenol 50.0 29.8 59.6 22.0-147
2-Chlorophenol 50.0 30.3 60.6 23.0-134
2,4-Dichlorophenol 50.0 30.2 60.4 39.0-135
2,4-Dimethylphenol 50.0 29.1 58.2 32.0-120
4,6-Dinitro-2-methylphenol 50.0 37.0 74.0 1.00-181
2,4-Dinitrophenol 50.0 35.2 70.4 1.00-191
2-Nitrophenol 50.0 31.9 63.8 29.0-182
4-Nitrophenol 50.0 14.5 29.0 1.00-132
Pentachlorophenol 50.0 34.2 68.4 14.0-176
Phenol 50.0 13.8 27.6 5.00-120
2,4,6-Trichlorophenol 50.0 34.1 68.2 37.0-144
(S) Nitrobenzene-d5 47.7 15.0-314
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1375392
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1155985-01,02
Laboratory Control Sample (LCS)
(LCS) R3469628-1 11/06/19 14:31
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
(S) 2-Fluorobiphenyl 64.3 22.0-127
(S) p-Terphenyl-d14 65.7 29.0-141
(S) Phenol-d5 26.0 8.00-424
(S) 2-Fluorophenol 41.5 10.0-120
(S) 2,4,6-Tribromophenol 67.5 10.0-153
L1156304-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1156304-02 11/06/19 19:34 • (MS) R3469628-3 11/06/19 19:54 • (MSD) R3469628-4 11/06/19 20:14
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Acenaphthene 47.2 1.96 31.2 32.7 61.9 64.6 1 47.0-145 4.69 48
Acenaphthylene 47.2 ND 30.7 32.1 65.0 67.4 1 33.0-145 4.46 74
Anthracene 47.2 ND 32.3 28.8 68.4 60.5 1 27.0-133 11.5 66
Benzidine 94.4 ND ND ND 0.000 0.000 1 1.00-120 J6 J6 0.000 40
Benzo(a)anthracene 47.2 ND 34.6 34.9 73.3 73.3 1 33.0-143 0.863 53
Benzo(b)fluoranthene 47.2 ND 34.0 36.5 72.0 76.7 1 24.0-159 7.09 71
Benzo(k)fluoranthene 47.2 ND 33.0 35.7 69.9 75.0 1 11.0-162 7.86 63
Benzo(g,h,i)perylene 47.2 ND 31.2 33.4 66.1 70.2 1 1.00-219 6.81 97
Benzo(a)pyrene 47.2 ND 34.9 29.8 73.9 62.6 1 17.0-163 15.8 72
Bis(2-chlorethoxy)methane 47.2 ND 26.1 27.1 55.3 56.9 1 33.0-184 3.76 54
Bis(2-chloroethyl)ether 47.2 ND 28.0 29.5 59.3 62.0 1 12.0-158 5.22 108
Bis(2-chloroisopropyl)ether 47.2 ND 26.5 28.3 56.1 59.5 1 36.0-166 6.57 76
4-Bromophenyl-phenylether 47.2 ND 33.0 35.2 69.9 73.9 1 53.0-127 6.45 43
2-Chloronaphthalene 47.2 ND 28.4 30.4 60.2 63.9 1 60.0-120 6.80 24
4-Chlorophenyl-phenylether 47.2 ND 32.3 33.7 68.4 70.8 1 25.0-158 4.24 61
Chrysene 47.2 ND 32.6 34.5 69.1 72.5 1 17.0-168 5.66 87
Dibenz(a,h)anthracene 47.2 ND 32.1 34.8 68.0 73.1 1 1.00-227 8.07 126
3,3-Dichlorobenzidine 94.4 ND 30.8 ND 32.6 0.000 1 1.00-262 J3 J6 200 108
2,4-Dinitrotoluene 47.2 ND 35.0 36.9 74.2 77.5 1 39.0-139 5.29 42
2,6-Dinitrotoluene 47.2 ND 32.9 34.9 69.7 73.3 1 50.0-158 5.90 48
Fluoranthene 47.2 ND 33.5 35.0 71.0 73.5 1 26.0-137 4.38 66
Fluorene 47.2 ND 32.3 33.8 67.4 69.9 1 59.0-121 4.54 38
Hexachlorobenzene 47.2 ND 32.1 34.2 68.0 71.8 1 1.00-152 6.33 55
Hexachloro-1,3-butadiene 47.2 ND 25.8 27.7 54.7 58.2 1 24.0-120 7.10 62
Hexachlorocyclopentadiene 47.2 ND 25.9 27.8 54.9 58.4 1 10.0-146 7.08 34
Hexachloroethane 47.2 ND 36.5 36.8 77.3 77.3 1 40.0-120 0.819 52
Indeno(1,2,3-cd)pyrene 47.2 ND 32.5 34.6 68.9 72.7 1 1.00-171 6.26 99
Isophorone 47.2 ND 26.8 27.9 56.8 58.6 1 21.0-196 4.02 93
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1155985 11/08/19 10:53 23 of 27
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Withers & Ravenel Eng. - Standard 02180080.10 L1155985 11/08/19 11:37 23 of 27
ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1375392
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1155985-01,02
L1156304-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1156304-02 11/06/19 19:34 • (MS) R3469628-3 11/06/19 19:54 • (MSD) R3469628-4 11/06/19 20:14
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Naphthalene 47.2 18.5 42.6 39.9 51.1 45.0 1 21.0-133 6.55 65
Nitrobenzene 47.2 ND 26.0 33.3 55.1 70.0 1 35.0-180 24.6 62
n-Nitrosodimethylamine 47.2 ND 15.1 14.8 32.0 31.1 1 10.0-120 2.01 40
n-Nitrosodiphenylamine 47.2 ND 33.0 31.2 69.9 65.5 1 16.0-160 5.61 28
n-Nitrosodi-n-propylamine 47.2 ND 27.2 28.6 57.6 60.1 1 1.00-230 5.02 87
Phenanthrene 47.2 ND 31.9 33.5 67.6 70.4 1 54.0-120 4.89 39
Benzylbutyl phthalate 47.2 ND 38.0 39.9 80.5 83.8 1 1.00-152 4.88 60
Bis(2-ethylhexyl)phthalate 47.2 ND 38.0 39.7 80.5 83.4 1 8.00-158 4.38 82
Di-n-butyl phthalate 47.2 ND 37.3 38.8 79.0 81.5 1 1.00-120 3.94 47
Diethyl phthalate 47.2 ND 34.2 35.4 72.5 74.4 1 1.00-120 3.45 100
Dimethyl phthalate 47.2 ND 32.8 34.1 69.5 71.6 1 1.00-120 3.89 183
Di-n-octyl phthalate 47.2 ND 37.8 39.9 80.1 83.8 1 4.00-146 5.41 69
Pyrene 47.2 ND 33.2 34.9 70.3 73.3 1 52.0-120 4.99 49
1,2,4-Trichlorobenzene 47.2 ND 25.6 27.2 54.2 57.1 1 44.0-142 6.06 50
4-Chloro-3-methylphenol 47.2 ND 29.9 30.5 63.3 64.1 1 22.0-147 1.99 73
2-Chlorophenol 47.2 ND 26.6 28.4 56.4 59.7 1 23.0-134 6.55 61
2,4-Dichlorophenol 47.2 ND 27.5 29.4 58.3 61.8 1 39.0-135 6.68 50
2,4-Dimethylphenol 47.2 ND 25.8 7.21 54.7 15.1 1 32.0-120 J3 J6 113 58
4,6-Dinitro-2-methylphenol 47.2 ND 37.5 40.0 79.4 84.0 1 1.00-181 6.45 203
2,4-Dinitrophenol 47.2 ND 39.8 42.3 84.3 88.9 1 1.00-191 6.09 132
2-Nitrophenol 47.2 ND 28.4 30.2 60.2 63.4 1 29.0-182 6.14 55
4-Nitrophenol 47.2 ND 16.5 18.2 35.0 38.2 1 1.00-132 9.80 131
Pentachlorophenol 47.2 ND 37.5 38.3 79.4 80.5 1 14.0-176 2.11 86
Phenol 47.2 ND 15.3 16.2 15.3 17.1 1 5.00-120 5.71 64
2,4,6-Trichlorophenol 47.2 ND 31.4 33.1 66.5 69.5 1 37.0-144 5.27 58
(S) Nitrobenzene-d5 45.6 47.1 15.0-314
(S) 2-Fluorobiphenyl 61.4 63.9 22.0-127
(S) p-Terphenyl-d14 70.0 74.4 29.0-141
(S) Phenol-d5 25.0 26.8 8.00-424
(S) 2-Fluorophenol 36.9 39.4 10.0-120
(S) 2,4,6-Tribromophenol 70.4 73.2 10.0-153
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
B The same analyte is found in the associated blank.
J The identification of the analyte is acceptable; the reported value is an estimate.
J2 Surrogate recovery limits have been exceeded; values are outside lower control limits.
J3 The associated batch QC was outside the established quality control range for precision.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low.
N The analyte is tentatively identified and the associated numerical value may not be consistent with the actual concentration present in the sample.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing
turn-around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National.

State Accreditations
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN-03-2002-34
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹n/a
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶90010 South Carolina 84004
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana ¹LA180010 Texas T104704245-18-15
Maine TN0002 Texas ⁵LAB0152
Maryland 324 Utah TN00003
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 460132
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 9980939910
Montana CERT0086 Wyoming A2LA

Third Party Federal Accreditations
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable

Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contactour main office. Pace National performs all testing at our central laboratory.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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APPENDIX E

BORING LOGS
WELL CONSTRUCTION RECORD

APPENDIX F

UST-2A FORM
(SITE INVESTIGATION REPORTS)
&
UST-61 FORM
(24-HOUR RELEASE AND UST LEAK
REPORTING FORM)

UST-61 24-Hour Release and UST Leak Reporting Form.
For Releases This form should be completed and submitted to the UST Section’s regional office following a known or suspected release from
an underground storage tank (UST) system. This form is required to be submitted within 24 hours of discovery of a known or in NC suspected release

(DWM USE ONLY) Incident # Risk (H,I,L,U)
Received On Received By
Reported by (circle one): Phone, Fax or Report
Region

Suspected Contamination? (Y/N) Y
Confirmed GW Contamination? (Y/N) N
Confirmed Soil Contamination ?(Y/N) Y
Samples Taken?(Y/N) Y
Free Product? (Y/N) N If Yes, State Greatest
Thickness NA

Facility ID Number 0-0-2529
Date Leak Discovered 11-6-19
Comm/Non-Commercial? Comm
Reg/Non-regulated? Reg
INCIDENT DESCRIPTION
Incident Name: Midway Kwik Stop
Address: 4505 North College Road County: New Hanover
City/Town: Castle Hayne Zip Code: 28429 Regional Office (circle one): Asheville, Mooresville, Fayetteville,
Raleigh, Washington, Wilmington, Winston-Salem
Latitude (decimal degrees): 33.33437 Longitude (decimal degrees) : -77.88974 Obtained by:
・GPS
・Topographic map
・GIS Address matching
X Other (UST-10B form)
・Unknown
Describe location:
Fuel pumps #1, 2 & 4
Fuel line sample FL-1
Briefly describe suspected or confirmed release: (including but not limited to: nature of release, date of release, amount
of release, amount of free product present and recovery efforts, initial responses conducted, impacts to receptors)
 Six petroleum USTs were removed from this site on 10‐22 and 10‐23‐19.  Lab analysis of sidewall 
soil samples did not exhibit TPH DRO or GRO concentrations above action levels and a monitor 
well was installed in each of two UST excavations.  Lab analysis results for three soil samples 
obtained from the former locations of three fuel pumps (FP‐1, FP‐2 and FP‐4) and one sample 
from beneath one of the fuel lines (FL‐1) exhibited TPH DRO concentrations above 100 mg/Kg. 
Sample FP‐2 also exhibited a TPH GRO concentration above 50 mg/Kg 
HOW RELEASE WAS DISCOVERED (Release Code)
(Check one)
・Release Detection Equipment or Methods
X During UST Closure/Removal
・Property Transfer
・Visual/Odor
・Water in Tank
・Water Supply Well Contamination
・Groundwater Contamination
・Surface Water Contamination
・Other (specify)
SOURCE OF CONTAMINATION
Source of Release Cause of Release Type of Release Product Type Released
(Check primary source) (Check primary cause) (Check one) (Check primary product type released)
・ Tank
X Piping
・ Dispenser
・ Submersible Turbine Pump
・ Delivery Problem
・ Spill Bucket
・Other
・ Unknown
Definitions presented on reverse
・ Spill
・ Overfill
・ Corrosion
・ Physical/Mechanical
Damage
・ Install Problem
・ Other
X Unknown
Definitions presented on reverse
X Petroleum
・ Non-Petroleum
・ Both
Location
(Check one)

X Facility
・Residence
・Other

X Gasoline/ Diesel/ ・ Diesel/Veg. Oil
Kerosene Blend
・ Heating Oil ・ Vegetable Oil 100%
・ Other Petroleum ・E10 – E20
Products ・E21 – E84
・ Metals ・E85 – E99
・ Other Inorganics ・Ethanol 100%
・ Other Organics ・E01 – E09
Ownership
1. Municipal 2. Military 3. Unknown 4. Private 5. Federal 6. County 7. State

Operation Type
1. Public Service 2. Agricultural 3. Residential 4. Education/Relig. 5. Industrial 6. Commercial 7. Mining
UST Form 61 (02/19) Page 1 of 2

IMPACT ON DRINKING WATER SUPPLIES
Water Supply Wells Affected? 1. Yes 2. No 3. Unknown
Number of Water Supply Wells Affected Unknown
Water Supply Wells Contaminated: (Include Users Names, Addresses and Phone Numbers. Attach additional sheet if necessary)

1.
2.
3.
UST SYSTEM OWNER
UST Owner/Company
Michelle and Mohammed Khalil
Point of Contact
Mohammed Khalil
Address
9866 Olde Towne Wynd SE
City
Leland
State
NC
Zip Code
28451
Telephone Number
910-383-3600

UST SYSTEM OPERATOR
UST Operator/Company
Midway Kwik Stop, LLC
Address
4505 North College Road
City
Castle Hayne
State
NC
Zip Code
28429
Telephone Number
910-675-3200
LANDOWNER AT LOCATION OF UST INCIDENT
Landowner
Michelle and Mohammed Khalil
Address
9866 Olde Towne Wynd SE
City Leland State NC Zip Code 28451 Telephone Number 910-383-3600
Draw Sketch of Area (showing two major road intersections) or Attach Map

See Attached Map
Person Reporting Incident: Brian Bellis Company: WithersRavenel, Inc. Telephone Number: 910-256-9277
Title: Project Manager Address: 219 Station Road, Unit 101, Wilmington NC 28405 Date: November 6, 2019
UST Form 61 (02/19) Page 2 of 2

Definitions of Sources
Tank: means the tank that stores the product and is part of the underground storage tank system
Piping: means the piping and connectors running from the tank or submersible turbine pump to the dispenser or other end-use equipment (Vent, vapor recovery, or fill
lines are excluded.)
Dispenser: includes the dispenser and the equipment used to connect the dispenser to the piping (e.g., a release from a suction pump or from components located above
the shear valve)
Submersible Turbine Pump (STP) Area includes the submersible turbine pump head (typically located in the tank sump), the line leak detector, and the piping that
connects the submersible turbine pump to the tank
Delivery Problem: identifies releases that occurred during product delivery to the tank. (Typical causes associated with this source are spills and overfills.)
Other: serves as the option to use when the release source is known but does not fit into one of the preceding categories (e.g., for releases from vent lines, vapor
recovery lines, and fill lines)
Unknown: identifies releases for which the source has not been determined

Definitions of Causes
Spill: use this cause when a spill occurs (e.g., when the delivery hose is disconnected from the tank fill pipe or when the nozzle is removed from the dispenser)
Overfill: use when an overfill occurs (e.g., overfills may occur from the fill pipe at the tank or when the nozzle fails to shut off at the dispenser)
Physical or Mechanical Damage: use for all types of physical or mechanical damage, except corrosion (e.g., puncture of tank or piping, loose fittings, broken
components, and components that have changed dimension)
Corrosion: use when a metal tank, piping, or other component has a release due to corrosion (e.g., for steel, corrosion takes the form of rust)
Installation Problem: use when the problem is determined to have occurred specifically because the UST system was not installed properly
Other: use this option when the cause is known but does not fit into one of the preceding categories (e.g., putting regulated substances into monitoring wells)
Unknown: use when the cause has not been determined
FP-9FP-8FP-7FP-6FP-5FP-1*FP-2*FP-3FP-4*FL-1** Indicates location where TPH DROconcentration in soil sampleexceeded 100 mg/Kg action level.4505 North College RoadCastle Hayne, NC (Approximate)N

APPENDIX G

UST-3 FORM
(NOTICE OF INTENT: UST PERMANENT
CLOSURE OR CHANGE-IN-SERVICE)