WI-7755_32840_CA_MRP_20210508

GROUNDWATER MONITORING REPORT

HANDY HOUSE 3
6742 HWY 70, NEWPORT, NC 28570
GROUNDWATER INCIDENT #: 32840; FACILITY ID #: 0-011113

LATITUDE: N 34.77793o; LONGITUDE: W 76.871506o (From GPS)

MAY 8, 2021

UST OWNER:
J.M. Davis Industries, Inc. 201 Arendell Street, Morehead City, NC 28557 [phone]

PROPERTY OWNER & OCCUPANT:
Property Owner & Occupant:Dominick Spadaro, 301 Roberts Road, Newport, NC 28570 [phone]

CONSULTANT:
Henry Nemargut Engineering Services, 2211 Chestnut Street, Wilmington, NC 28405
Phone Number: [phone]
RELEASE INFORMATION: Date Discovered: 3/7/13 Estimated Quantity of Release: Unknown Cause of Release: Gasoline USTs; Source of Release: Gasoline UST System Size and Contents: (2) 6,000 Gallon Gasoline USTs; (1) 4,000 Gallon Gasoline UST

The Monitoring Report for this site has been prepared by Henry Nemargut Engineering
Services. All engineering work performed on this project was conducted under my direct
supervision:

Henry Nemargut, P.E.
Henry Nemargut Engineering Services
North Carolina License #17669

May 8, 2021

Jim Davis
J.M. Davis Industries, Inc.
812 Arendell Street
Morehead City, NC 28557

Reference: Groundwater Monitoring Report
Handy House 3
6724 Hwy 70
Newport, Carteret County, North Carolina 28570
Incident #32840; Facility ID #0-011113

Dear Mr. Davis:

In accordance with an approved Task Authorization Form (TAF) from the North Carolina
Department of Environmental Quality (NCDEQ), contained herein is a Groundwater Monitoring
Report for the release which occurred at the above referenced facility. The field activities for
this project consisted of the sampling of existing monitor wells with the laboratory analyses of
the collected groundwater samples. All activities were conducted in accordance with the
NCDEQ guidelines and the requirements of 15A NCAC 2L .0115.

Mr. Davis, if you have any questions concerning this report, please contact our office.

Sincerely,

Henry Nemargut, P.E.
Henry Nemargut Engineering Services

B. EXECUTIVE SUMMARY
1. Free Product: Free product has not been observed at the site.
2. Contaminant Mass: Based on the soil & groundwater data from the original CSA with subsequent placement of final wells at the site in August 2014, the estimated baseline total contaminant mass at this site during initial investigations is 194 lbs of total petroleum mass, which includes an estimated 32.5 lbs of petroleum dissolved into the aqueous phase at this site. The latest groundwater monitoring event conducted on January 29, 2021 indicates that an estimated 1.15 lbs of petroleum contaminant mass remains dissolved in groundwater at the site based on analytical data. Current data indicates a 96.5% contaminant decrease in dissolved aqueous phase petroleum mass has occurred at the site compared to the original CSA total dissolved mass, due to natural processes and nutrient sock installation.

3. Maximum Concentrations of Dissolved Groundwater Contaminants:

Current Groundwater Maximums:
Contaminant Result Well ID 2L Standard Toluene 2.7 ug/L (MW-3) 600 ug/L Ethyl Benzene 163 ug/L (MW-3) 600 ug/L Xylenes 319 ug/L (MW-3) 500 ug/L 1,2,4-Trimethylbenzene 630 ug/L (MW-3) 400 ug/L 1,3,5-Trimethylbenzene 252 ug/L (MW-3) 400 ug/L Naphthalene 251 ug/L (MW-3) 6 ug/L Isopropylbenzene 38 ug/L (MW-3) 70 ug/L Total 6200B 1,666 ug/L (MW-3) NSE No other compounds exceeded 2L Standards for 6200B compounds during the latest groundwater monitoring event for this site. 4. Extent of Dissolved Groundwater Contamination: The plume of dissolved groundwater contamination appears to be reducing significantly in downgradient areas of this site with the addition of nutrient socks, and as a result of abatement soil excavation activities, based on the historical data for the site. Historically, the plume appears to be originating from the gasoline UST basin. Data from the 2014 baseline sampling event indicated that the dissolved plume above 2L Standards had migrated 220’ from the UST source area. Currently, 2L Violations are present at relatively low levels compared to the 2L & GCL Standards, with a plume reduced to 50’ from the source in the downgradient direction. 5. Maximum Soil Contaminant Concentrations (From 2013-2014 Soil Assessments): Contaminant Result Sample ID Lowest MSCC MTBE 0.631 mg/kg (SE) 0.091 mg/kg Xylenes (total) 34.1 mg/kg (DPE) 4.6 mg/kg Naphthalene 50.1 mg/kg (DPE) 0.16 mg/kg Isopropylbenzene 15.1 mg/kg (DPE) 2.0 mg/kg 1,2,4-Trimethylbenzene 172 mg/kg (DPE) 8.5 mg/kg 1,3,5-Trimethylbenzene 71 mg/kg (DPE) 8.4 mg/kg
C5-C8 Aliphatics 112 mg/kg (DPE) 68 mg/kg C9-C18 Aliphatics 2,420 mg/kg (DPE) 540 mg/kg C9-C22 Aromatics 1,030 mg/kg (DPE) 31 mg/kg Soil assessment at this site indicates that an estimated 20 tons of contaminated soil above the seasonal water table and in the smear zone remain in the area of the dispenser island, at the base of the canopy footer. Based on the local public water supply well, Lowest MSCC standards may apply for this site. Approximately 1806 tons of petroleum contaminated soils were excavated and disposed of from around the USTs and dispenser islands during IAA excavation activities. 6. Remedial Action Plan:
No CAP has been developed for this site. The NCDEQ Wilmington Regional Office has approved the experimental use of nutrient and absorbent socks at this site to evaluate their effectiveness on contaminant reduction at this site. Nutrient socks have been installed at this site on the following dates: March 18, 2017 (nutrient socks/MW-2,3,8,9,10) October 16, 2017 (nutrient/oxygenating socks/ MW-2,3,8,9,10) May 16, 2018 (nutrient/oxygenating socks/ MW-2,3,8,9,10) March 28, 2019 (nutrient socks/MW-2,3,8,9,10) January 29, 2021 (nutrient socks/MW-2,3,8,9,10) The available data suggests that these nutrient socks have been effective in reducing 6200B concentrations at this site, particularly in downgradient wells. The plume appears to be significantly reduced in size and concentrations since the socks have been introduced into the impacted wells at this site. Current plans for remedial action at this site include evaluation continued use of nutrient socks via semi-annual sampling to collect data for continued evaluation of the effectiveness of the use of nutrient socks on the reduction of petroleum constituents at this site.

7. Impacted Receptors:
3 private potable wells serve as a water supply well for residents located on Roberts Road. A public water supply well located downgradient of the release source at 6760 Hwy 70 has routinely failed to contain petroleum related compounds. Since this is an active water supply well, the site will retain its High Risk classification as long as this well is used to provide water supply to the tenants of this small strip shopping center. A drainage ditch on the east side of the NCDOT right-of-way may now or formerly intercepted the dissolved plume during high water table periods. This ditch has never been tested for impact from the UST release originating at the Handy House 3 site.
TABLE OF CONTENTS

Section Page 1.0 Site History and Characterization 1.1 Introduction .................................................................... 1 1.2 Scope of Services ........................................................... 2 1.3 Receptor Survey Update ................................................ 2 2.0 Presentation of Current Site Assessment Information / Comparison to Historical Assessment Information 2.1 Historical Soil Assessment Information ........................ 2 2.2 Groundwater Flow Direction and Gradient ................... 3 2.3 Monitor Well Sampling and Analyses ........................... 3 2.4 Supply Well Sampling and Analyses ............................. 3 2.5 Regional / Site Geology and Hydrogeology .................. 4 2.6 Plume Development ....................................................... 5 3.0 Monitored Natural Attenuation 3.1 Natural Source Zone Depletion Status ........................... 5 4.0 Conclusions 4.1 General Summary .......................................................... 6 4.2 Recommendations .......................................................... 6 4.3 Limitations ..................................................................... 6 5.0 Statements and Certification 5.1 Statements ...................................................................... 7 5.2 Certification ................................................................... 7

LIST OF FIGURES Figure 1: Project Location Figure 2: Receptor Map Figure 3: Soil Concentrations Map Figure 4: Site Layout & UST Locations Figure 5: Monitor Well Locations Map Figure 6: Shallow Well Potentiometric Surface Map (3/18/20) Figure 7: Naphthalene Isoconcentration Map Figure 8: 1,2,4-Trimethylbenzene Isoconcentration Map Figure 9: Total 6200B Compounds Concentration Map – 3/18/20 Figure 10: Total 6200B Compounds Concentration Map – Baseline-3/11/15

LIST OF TABLES

Table 1: Site History
Table 2: Summary of Soil Analytical Data
Table 3: Monitoring Well Information and Groundwater Elevations
Table 4: Summary of Groundwater Analytical Results-3/18/2020 Table 5: Water Supply Well Information Table 6: Mass Calculation Table
Table 7: Cumulative Groundwater Summary
Table 8: Baseline Groundwater Analytical Data – 8/28/2014

APPENDICES Appendix A: Laboratory Analytical Results
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GROUNDWATER MONITORING REPORT Handy House 3 6724 Hwy 70, Newport, North Carolina 28570

1.0 Site History and Characterization
1.1 Introduction

J.M. Davis Industries, Inc. owned USTs which were operated at the Handy House 3
facility located at 6724 Hwy 70 in Newport, North Carolina. Figure 1 illustrates the
location of this facility on the Newport Quadrangle U.S.G.S. Topo Map. This facility
contains one permanent structure which was used as a convenience store. The site
formerly contained (2) 6,000 gallon gasoline and (1) 4,000 gallon gasoline UST which
were last used at this facility in June, 2012. The locations of the USTs and the site layout
are illustrated on Figure 4. A release from the UST system was suspected on 3/6/13 and
reported to NCDENR personnel based on elevated PID readings observed in soil samples
collected from soils removed from around the USTs. This release was confirmed upon
receipt of analytical results from soil samples collected during the tank closure activities
conducted on 3/6-13/2013. In response to this release, J.M. Davis Industries, Inc. took
immediate abatement measures at the site including excavation and proper disposal of
accessible contaminated soils in the UST and dispenser island areas resulting in
remediation of 1,806 tons of petroleum contaminated soils. Groundwater monitoring
activities are ongoing at the site on a semi-annual basis. Table 1 contains the UST
history for this site.
The site and adjacent properties are used for commercial and residential purposes.
Municipal water supply from the Town of Newport serves the site and is available to all
properties within 1,500’; however, (4) active water supply wells are in use within 1,000’
of the release source originating at this facility. The NCDEQ Wilmington Regional
should evaluate the information contained in this report to determine whether
development of a CAP is warranted.
1.2 Scope of Services

This Groundwater Monitoring Report contains documentation concerning the following
activities which have been conducted at this facility:

o Sampling of five monitor wells conducted by Henry Nemargut Engineering on January 29, 2021.

o Removal of nutrient socks.

o Laboratory analyses of groundwater samples conducted by Pace Analytical, Inc. of Huntersville, NC.
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2.0 Presentation of Current Site Assessment Information / Comparison to Historical Assessment Information 2.1 Historical Soil Assessment Information
Soil samples were collected from the sidewalls of the remedial excavation during 2013
IAA activities. (4) soil borings (B1 through B4) advanced at the site during CSA soil
assessment activities to depths of 4’ below grade in the approximate locations depicted
on Figure 3 to assess the extent of non-excavatable soils beneath the canopy structure at
this site. An estimated 60 square foot area was estimated during assessment to contain
contaminated soil in the area of the UST basin. With an assumed thickness of 6’, that
would represent approximately 20 tons of contaminated soils remain in place at the
project site beneath the canopy structure. Based on the existence of local potable wells
within 1,000’, Lowest MSCC standards should apply for soil cleanup standards for this
site.
Figure 3 illustrates the locations of the risk-based soil samples collected at the subject site
and the estimated extent of soil contamination above lowest MSCCs, and Table 2
summarizes the laboratory results for the “Risk-Based” soil samples from 6724 Hwy 70
in Newport, NC. Laboratory analytical reports and the chain of custody records for the
soil samples collected at the project site are contained in the IAA and CSA reports
submitted for this site.

Based on the limited time between the original soil sampling and the most recent
groundwater sampling event, it is estimated that natural processes have not significantly
reduced soil contaminant levels beyond the original estimate. Additional soil assessment
activities would be required to formulate new soil mass contaminant calculation for the
site. 2.2 Ground Water Flow Direction and Gradient

In order to estimate the groundwater flow direction in the vicinity of the petroleum
release, elevations of the monitor well casings were measured using surveying
equipment. During the January 29, 2021 sampling event, static water levels were
obtained from the monitor wells (see Table 3) and the data was used to compute a
potentiometric surface map. Figure 6 illustrates the current potentiometric surface map
as calculated based on the measurements obtained on January 29, 2021.
Groundwater data and monitoring well information were also used to estimate the
hydraulic gradient at the project site. Using the horizontal distance between the monitor
wells and the static water levels, the groundwater was calculated to flow toward the
north/northwest with a hydraulic gradient of approximately 0.0209 ft/ft.

2.3 Monitor Well Sampling and Analyses

On January 29, 2021, (5) monitor wells were sampled for analyses utilizing Standard
Method 6200B + oxygenates. Before collecting the samples, the monitor wells were
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purged by removing a minimum of three well volumes to ensure that the samples were
representative of the actual groundwater conditions. The wells were developed using
disposable plastic bailers suspended with unused nylon string.

All samples were placed in laboratory supplied glassware, labeled with sample location,
analysis to be performed, time, date and sampler's name. The sample jars were then
immediately placed in a cooler, chilled with ice to approximately 4oC in preparation of
transportation to an analytical laboratory utilizing EPA approved chain-of-custody
procedures.

Laboratory analytical results indicate the presence of (2) 6200B compounds groups above
the current listed 2L Standards in monitor wells MW-3 only. 1,2,4-Trimethylbenzene
was detected at a maximum concentration of 630 ug/l in MW-3, above its 2L standard of
400 ug/l but below its GCL of 28,500 ug/l. No GCL violations were noted at the site.
Naphthalene was detected at a maximum concentration of 251 ug/l in monitoring well
MW-3. Total 6200B compounds were noted in MW-3 at a maximum concentration of
1,666 ug/l. No oxygenates were detected at the site. Table 4 summarizes the laboratory
analytical results, and Appendix A contains a copy of the laboratory analytical report and
chain of custody records. Figure 7 contains a naphthalene iso-concentration map and
Figure 8 contains a 1,2,4-Trimethylbenzene iso-concentration map. Figures 9 and Figure
10 contain current and baseline total 6200B isoconcentration maps which were prepared
for total dissolved constituent groundwater contaminant mass calculations.

2.4 Supply Well Sampling and Analyses

On January 29, 2021, the supply well at the Elaine Honeycutt property (SW-3) was
sampled for analyses utilizing Standard Method 6200B. Before sampling, the supply
well was purged by pumping from the wells for approximately 5 minutes to ensure that
the samples were representative of the actual groundwater conditions. After pumping,
the flowrate was reduced for collection of samples. The sample from SW-3 was obtained
from the spigot closest to the supply well.

All samples were placed in laboratory supplied glassware, labeled with sample location,
analysis to be performed, time, date and sampler's name. The sample jars were then
immediately placed in a cooler, chilled with ice to approximately 4oC in preparation of
transportation to an analytical laboratory utilizing EPA approved chain-of-custody
procedures.

Laboratory analytical results failed to indicate the presence of any 6200B compounds
above laboratory detection limits in the Honeycutt supply well sample. Appendix A
contains a copy of the laboratory analytical report and chain of custody records. 2.5 Regional / Site Geology and Hydrogeology
The site is situated in the Coastal Plain Physiographic Province. According to the
Geological Map of North Carolina local geology of the region consists of surficial
deposits, undivided, including sand, clay, gravel and peat deposited in marine, fluvial,
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eolian, and lacustrine environments. Bedrock was not encountered to a depth of 68 feet
below surface which was the maximum depth explored during the subsurface
investigation.

Three single well rising head tests or "slug tests" were performed on MW-3, MW-7 and
MW-9 to determine the saturated hydraulic conductivity of the water table aquifer. The
method of Bouwer and Rice (Bouwer and Rice, 1989, 1976) was chosen to reduce the
slug test data. A computer program developed by the Geraghty & Miller Modeling
Group named AQTESOLV was used to estimate the aquifer parameters. Results of the
slug tests indicated a hydraulic conductivity of 6.501 x10-3 feet/minute for MW-3, 2.221
x 10-3 feet/minute for MW-7, and 4.08 x 10-3 feet/minute for MW-9. The results from
MW-3, MW-7 and MW-9 are consistent with published values for silty sand and fine
clean sand (Freeze & Cherry, 1979). 2.6 Plume Development

The monitoring well network at this release site was installed between June, 2013 and
August, 2014. In prior sampling events conducted at the site, contaminants have been
reported above 2L Standards in on-site and off-site monitoring wells. The contaminant
concentrations in source area wells MW-1 and MW-2, where soils were excavated, have
continually decreased throughout the monitoring history for this site. Down-gradient
wells at the site generally showed a decrease to a historically low concentrations during
the October 16, 2017 sampling event. This decrease may have in part been related to pit
dewatering conducted by the Town of Newport in the DOT right-of-way during
installation of underground sewer lines during 1st quarter 2017. Several wells were lost
or destroyed on adjacent properties and in the NC-DOT right-of-way by the Town of
Newport in 2017. Additional wells have been lost due to construction activities on off-
site properties. The current reduced monitoring well network is illustrated on Figure 5.

The latest groundwater monitoring event conducted on January 29, 2021 indicates that an
estimated 1.15 lbs of petroleum contaminant mass remains dissolved in groundwater at
the site based on analytical data. Current data indicates a 96.5% contaminant decrease in
dissolved aqueous phase petroleum mass has occurred at the site compared to the August
2014 baseline total dissolved mass, due to natural processes and nutrient sock installation.
Both the size and concentration of the dissolved constituent plume at this site has
decreased significantly over the history of this site. Historical groundwater data are
summarized on Table 7, which includes groundwater elevation data. Table 6 contains
contaminant mass calculations.

3.0 Monitored Natural Attenuation 3.1 Natural Source Zone Depletion Status
Historically, 2L violations for 10 compounds/compound groups have been observed in
groundwater monitoring activities conducted since March 11, 2015. The groundwater
contaminant plume in August, 2014 appeared to have migrated to the north/northwest to a
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distance of 220’ from the UST source area; however, based on the results of the January
29, 2021 groundwater sampling event, it appears that the groundwater contaminant plume
has been reduced to a down-gradient distance of 50’. Targeted petroleum concentrations
detected in the groundwater samples collected from within the plume over that time
period appear to be significantly reduced based on available data.
Based on current analytical data, it appears that natural processes are remediating the
dissolved contaminant plume at this site originating from the UST source area. Estimates
based on the analytical data available for this site indicate that dissolved contaminant
mass has decreased by 96.5% over the monitoring history of this site.

4.0 Conclusions
4.1 General Summary
A Groundwater Monitoring event at Handy House 3 located at 6724 Hwy 70 in Wilmington, NC has been completed. From a review of all information gathered during this monitoring project, Henry Nemargut Engineering makes the following conclusions:

o Laboratory analytical results indicate the presence of (2) 6200B compounds groups above the current listed 2L Standards in monitor wells MW-3 only. 1,2,4-Trimethylbenzene was detected at a maximum concentration of 630 ug/l in MW-3, above its 2L standard of 400 ug/l but below its GCL of 28,500 ug/l. No GCL violations were noted at the site. Naphthalene was detected at a maximum concentration of 251 ug/l in monitoring well MW-3. Total 6200B compounds were noted in MW-3 at a maximum concentration of 1,666 ug/l. No oxygenates were detected at the site.

o Nutrient socks were removed during this sampling event and not replaced.

o One nearby in-use water supply well (Honeycutt property - SW-3) was sampled on January 29, 2021. Laboratory analytical results failed to indicate the presence of any 6200B compounds above laboratory detection limits in the Honeycutt supply well sample.

o Based on current analytical data, it appears that natural processes are remediating the dissolved contaminant plume at this site originating from the UST source area. The latest groundwater monitoring event conducted on January 29, 2021 indicates that an estimated 1.15 lbs of petroleum contaminant mass remains dissolved in groundwater at the site based on current analytical data. Current data indicates a 96.5% contaminant decrease in dissolved aqueous phase petroleum mass has occurred at the site compared to the August, 2014 baseline total dissolved mass, due to natural processes and nutrient sock installation.

Page - 6

4.2 Recommendations

Based on information obtained during this sampling event, Henry Nemargut Engineering
Services makes the following recommendations for this site:

o Semi-annual sampling should be continued with results used to evaluate the
effectiveness of past nutrient sock addition on groundwater contaminant level
reduction compared to natural processes alone with no nutrient sock additions.
Oxygenates should not be analyzed during future sampling events to reduce
project costs since none were detected at this site.

o The NCDEQ should determine whether any replacement monitoring wells are
warranted since all leading edge monitoring wells were destroyed by others from
site development and construction on downgradient properties. A copy of this monitoring report has been forwarded to the following address:

Liz Price
NCDEQ-WiRO UST Section
127 Cardinal Drive Extension
Wilmington, NC 28405 4.3 Limitations

This report has been prepared for the exclusive use of J.M. Davis Industries, Inc. for the specific application to the referenced site located in Carteret County, North Carolina. The assessment was conducted based on the scope of work and level of effort desired by the client. Our findings have been developed in accordance with generally accepted standards in the practice of Groundwater Monitoring Reports in the State of North Carolina, available information, and our professional judgment. No other warranty is expressed or implied.

The data presented in this report are indicative of conditions that existed at the precise
locations sampled and at the time the samples were collected. Additionally, the data
obtained from the samples would be interpreted as meaningful with respect to the
parameters indicated in the laboratory reports. No additional information can be logically
inferred from this data.

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5.0 Statements and Certification 5.1 Statements The monitoring report was due on May 1, 2021. Will this report be submitted after the established due date? No – Late submittal approved by Liz Price Was any required information from the template missing from this report? No If applicable, will any of the proposed attenuation milestones under the schedule approved in the Corrective Action Plan not be met? Not Applicable, no CAP has been prepared for this site. Does any known or suspected source zone soil contamination or free product remain outside of the assessed area that could be inhibiting natural attenuation? No Has there been an unexpected increase in contaminant mass sufficient to suggest a potential new release from a separate onsite or offsite source? No 5.2 Certification I, Henry Nemargut, a Professional Engineer, do certify that the information contained in this report is correct and accurate to the best of my knowledge.
Henry Nemargut, P.E.
Henry Nemargut Engineering Services
North Carolina License #17669

FIGURES
Send To Printer Back To MSR Maps Change to 11x17 Print Size Show Grid Lines Change to Landscape
Newport, North Carolina, United States01 Jul 1983
Im a g e co u rte sy o f th e U.S. Geological Survey
© 2010 Microsoft Corporatio n . Terms of Use Privacy Statement
Page 1 of 1MSRMaps: Print
12/18/2012http://msrmaps.com/PrintImage.aspx?T=2&S=12&Z=18&X=410&Y=4812&W=3&qs=...
FIGURE 1: PROJECT LOCATION - USGS TOPO
Project Location
feet
meters
1000
300

TABLES
TABLE 1: SITE HISTORY
Handy House 3
6724 Hwy 70, Newport, NC 28570

Property Ownership:

Dominick Spadaro
303 Roberts Road
Newport, NC 28570
12/20/2012 to Present

Previous Owners:

J.M. Davis Industries, Inc.
201 Arendell Street
Morehead City, NC 28557
NCDENR Facility ID #0-035849
5/3/78 to 12/20/2012

UST Information:

Tank Inst. Size Closure UST Tank
No Date (Gal) Date Status Contents
T1 5/3/78 6,000 3/7/13 Closed Gasoline
T2 5/3/78 6,000 3/7/13 Closed Gasoline
T3 5/3/78 4,000 3/7/13 Closed Gasoline

Tank owner:

J.M. Davis Industries, Inc.
201 Arendell Street
Morehead City, NC 28557
NCDENR Facility ID #0-035849
5/3/78 to present

Sample Location E1 E2 SE S2 SW EF Lowest MSCC Ind/Comm MSCC Residential MSCCDate3/13/2013 3/13/2013 3/13/2013 3/13/2013 3/13/2013 5/23/2013 (note units) (note units) (note units)Sample depth4'-5' 4'-5' 4'-5' 4'-5' 4'-5' 4'-5' Method 8260 (ug/kg)Benzene BDL BDL BDL BDL BDL BDL 5.6 164,000.0 18,000Methyl Ethyl Ketone BDL BDL BDL BDL BDL BDL 16,000 245,280,000 7,821,000Methyl Isobutyl Ketone BDL BDL BDL BDL BDL BDL NSE NSE NSEMethyl Butyl Ketone BDL BDL BDL BDL BDL BDL NSE NSE NSEn-Butylbenzene BDL BDL BDL BDL BDL BDL 4,300 16,350,000 626,000sec-Butylbenzene BDL BDL BDL BDL BDL BDL 3,300 16,350,000 626,000Ethylbenzene BDL BDL 22.1 BDL BDL BDL 4,900 40,000,000 1,560,000Isopropylbenzene BDL BDL BDL BDL BDL BDL 2,000 40,880,000 1,564,000p-Isopropyltoluene BDL BDL BDL BDL BDL BDL NSE NSE NSENaphthalene BDL BDL BDL 9.1 BDL BDL 160 8176000 313,000Acetone BDL 21.5 21.1 BDL BDL BDL 24,000 360,000,000 14,000,000n-Propylbenzene BDL BDL BDL BDL BDL BDL 2,000 16,350,000 626,000Toluene BDL BDL 81.1 BDL BDL BDL 4,300 32,000,000 1,200,0001,2,4-Trimethylbenzene BDL BDL 24.3 15.1 BDL BDL 8,500 20,440,000 782,0001,3,5-Trimethylbenzene BDL BDL 8.7 5.8 BDL BDL 8,300 20,440,000 782,000MTBE BDL BDL631BDL BDL BDL 91 3,100,000 350,000Methylene Chloride6.3BDLBDLBDLBDLBDL20763,00085,000StyreneBDLBDLBDLBDLBDLBDL1,50081,760,0003,128,000Xylenes (total)BDLBDL2166.1BDLBDL4,60081,760,0003,129,000Method 8270 (ug/kg)ChryseneNRNRNRNRNRNR39,000780,00088,000Benzoic AcidNRNRNRNRNRNR120,000163,520,00062,571,000Phenanthrene NR NR NR NR NR NR 56,000 12,264,000 469,000Pyrene NR NR NR NR NR NR 270,000 12,264,000 469,0002-Methylnapthalene NR NR NR NR NR NR 3,600 1,635,000 63,000Naphthalene NR NR NR NR NR NR 160 8176000 313,000Aliphatic Fraction Classes (mg/kg) C5 - C8 Volatile Aliphatics BDL BDL BDL BDL BDL BDL 68 24,528 939C9 - C12 Volatile Aliphatics BDL BDL BDL BDL BDL BDL NSE NSE NSEC9-C18 Extractable Aliphatics NR NR NR NR NR NR NSE NSE NSEC9-C18 Aliphatics (total) BDL BDL BDL BDL BDL BDL 540 40,000 1,500C19-C36 Extractable Aliphatics NR NR NR NR NR NR NSE 810,000 31,000Aromatic Fraction Classes (mg/kg) C9 - C10 Volatile AromaticsBDLBDLBDLBDLBDLBDLNSENSENSEC11 - C22 Extractable AromaticsNRNRNRNRNRNRNSENSENSEC9 - C22 Aromatics (total)BDLBDLBDLBDLBDLBDL3112264469BDL = below detection limits NR = analyses not requested NSE = no standard establishedTABLE 2Laboratory Analytical Results - Risk Based Soil SamplesHandy House 3, 6724 Hwy 70, Newport, NC 28570
Sample Location SEF DPN DPW DPS1 DPS2 DPE Lowest MSCC Ind/Comm MSCC Residential MSCCDate5/23/2013 5/28/2013 5/28/2013 5/28/2013 5/28/2013 5/28/2013 (note units) (note units) (note units)Sample depth4'-5' 4'-5' 4'-5' 4'-5' 4'-5' 4'-5' Method 8260 (ug/kg)Benzene BDL BDL BDL BDL BDL BDL 5.6 164,000.0 18,000Methyl Ethyl Ketone BDL BDL BDL BDL BDL BDL 16,000 245,280,000 7,821,000Methyl Isobutyl Ketone BDL BDL BDL BDL BDL BDL NSE NSE NSEMethyl Butyl Ketone BDL BDL BDL BDL BDL BDL NSE NSE NSEn-Butylbenzene BDL BDL BDL BDL BDL BDL 4,300 16,350,000 626,000sec-Butylbenzene BDL BDL BDL BDL BDL 288 3,300 16,350,000 626,000Ethylbenzene BDL BDL BDL BDL BDL 961 4,900 40,000,000 1,560,000Isopropylbenzene BDL BDL BDL BDL BDL 808 2,000 40,880,000 1,564,000p-Isopropyltoluene BDL BDL BDL BDL BDL 11,300 NSE NSE NSENaphthalene BDL BDL BDL BDL BDL10,400160 8176000 313,000Acetone 122 BDL BDL BDL BDL BDL 24,000 360,000,000 14,000,000n-Propylbenzene BDL BDL BDL BDL BDL 1540 2,000 16,350,000 626,000Toluene BDL BDL BDL BDL BDL BDL 4,300 32,000,000 1,200,0001,2,4-Trimethylbenzene BDL BDL BDL BDL BDL172,0008,500 20,440,000 782,0001,3,5-Trimethylbenzene BDL BDL BDL BDL BDL70,5008,300 20,440,000 782,000MTBE BDL BDL BDL BDL BDL BDL 91 3,100,000 350,000trans-1,2-DichloroetheneBDL20.816.910.9BDLBDL5408,200,000310,000StyreneBDLBDLBDLBDLBDLBDL1,50081,760,0003,128,000Xylenes (total)BDLBDLBDLBDLBDL34,1004,60081,760,0003,129,000Method 8270 (ug/kg)ChryseneNRNRNRNRNRNR39,000780,00088,000Benzoic AcidNRNRNRNRNRNR120,000163,520,00062,571,000Phenanthrene NR NR NR NR NR NR 56,000 12,264,000 469,000Pyrene NR NR NR NR NR NR 270,000 12,264,000 469,0002-Methylnapthalene NR NR NR NR NR NR 3,600 1,635,000 63,000Naphthalene NR NR NR NR NR NR 160 8176000 313,000Aliphatic Fraction Classes (mg/kg) C5 - C8 Volatile Aliphatics BDL BDL BDL BDL BDL11268 24,528 939C9 - C12 Volatile Aliphatics BDL BDL BDL BDL 5.1 2420 NSE NSE NSEC9-C18 Extractable Aliphatics NR NR NR NR NR NR NSE NSE NSEC9-C18 Aliphatics (total) BDL BDL BDL BDL 5.12420540 40,000 1,500C19-C36 Extractable Aliphatics NR NR NR NR NR NR NSE 810,000 31,000Aromatic Fraction Classes (mg/kg) C9 - C10 Volatile AromaticsBDLBDLBDLBDLBDL1030NSENSENSEC11 - C22 Extractable AromaticsNRNRNRNRNRNRNSENSENSEC9 - C22 Aromatics (total)BDLBDLBDLBDLBDL10303112264469BDL = below detection limits NR = analyses not requested NSE = no standard establishedTABLE 2 (continued)Laboratory Analytical Results - Risk Based Soil SamplesHandy House 3, 6724 Hwy 70, Newport, NC 28570
Sample Location B1 B2 B3 B4 Lowest MSCC Ind/Comm MSCC Residential MSCCDate5/6/2014 5/6/2014 5/6/2014 5/6/2014 (note units) (note units) (note units)Sample depth4' 4' 4' 4' Method 8260 (ug/kg)Benzene BDL BDL BDL BDL 5.6 164,000.0 18,000Methyl Ethyl Ketone BDL BDL BDL BDL 16,000 245,280,000 7,821,000Methyl Isobutyl Ketone BDL BDL BDL BDL NSE NSE NSEMethyl Butyl Ketone BDL BDL BDL BDL NSE NSE NSEn-Butylbenzene BDL BDL BDL BDL 4,300 16,350,000 626,000sec-Butylbenzene BDL BDL BDL BDL 3,300 16,350,000 626,000Ethylbenzene BDL BDL BDL BDL 4,900 40,000,000 1,560,000Isopropylbenzene BDL BDL BDL BDL 2,000 40,880,000 1,564,000p-Isopropyltoluene BDL BDL BDL BDL NSE NSE NSENaphthalene BDL BDL BDL BDL 160 8176000 313,000Acetone BDL BDL BDL BDL 24,000 360,000,000 14,000,000n-Propylbenzene BDL BDL BDL BDL 2,000 16,350,000 626,000Toluene BDL BDL BDL BDL 4,300 32,000,000 1,200,0001,2,4-Trimethylbenzene BDL BDL BDL BDL 8,500 20,440,000 782,0001,3,5-Trimethylbenzene BDL BDL BDL BDL 8,300 20,440,000 782,000MTBE BDL BDL BDL BDL 91 3,100,000 350,000trans-1,2-DichloroetheneBDLBDLBDLBDL5408,200,000310,000StyreneBDLBDLBDLBDL1,50081,760,0003,128,000Xylenes (total)BDLBDLBDLBDL4,60081,760,0003,129,000Method 8270 (ug/kg)ChryseneNRNRNRNR39,000780,00088,000Benzoic AcidNRNRNRNR120,000163,520,00062,571,000Phenanthrene NR NR NR NR 56,000 12,264,000 469,000Pyrene NR NR NR NR 270,000 12,264,000 469,0002-Methylnapthalene NR NR NR NR 3,600 1,635,000 63,000Naphthalene NR NR NR NR 160 8176000 313,000Aliphatic Fraction Classes (mg/kg) C5 - C8 Volatile Aliphatics BDL BDL BDL BDL 68 24,528 939C9 - C12 Volatile Aliphatics BDL BDL BDL BDL NSE NSE NSEC9-C18 Extractable Aliphatics NR NR NR NR NSE NSE NSEC9-C18 Aliphatics (total) BDL BDL BDL BDL 540 40,000 1,500C19-C36 Extractable Aliphatics NR NR NR NR NSE 810,000 31,000Aromatic Fraction Classes (mg/kg) C9 - C10 Volatile AromaticsBDLBDLBDLBDLNSENSENSEC11 - C22 Extractable AromaticsNRNRNRNRNSENSENSEC9 - C22 Aromatics (total)BDLBDLBDLBDL3112264469BDL = below detection limits NR = analyses not requested NSE = no standard establishedTABLE 2 (continued)Laboratory Analytical Results - Risk Based Soil SamplesHandy House 3, 6724 Hwy 70, Newport, NC 28570
TABLE 3Monitoring Well Information and Groundwater ElevationsHandy House #3, 6724 Hwy 70, Newport, NC 28570Well Number Top of Casing Elevation Top of Screen Elevation Bottom of Screen Elevation Depth to Water Groundwater ElevationMW-1 99.31 96.31 81.31 4.44 94.87MW-2 99.32 96.32 81.32 5.31 94.01MW-3 100.00 97.00 82.00 6.83 93.17MW-4 100.00 96.00 81.00 n/a #VALUE!MW-5 98.20 93.20 83.20 n/a #VALUE!MW-6 99.18 94.18 84.18 n/a #VALUE!MW-7 98.43 94.43 80.43 n/a #VALUE!MW-8 100.15 95.15 80.15 7.63 92.52MW-9 100.17 95.17 80.17 n/a #VALUE!MW-10 99.43 97.43 82.43 5.25 94.18MW-11 98.78 93.78 83.78 n/a #VALUE!MW-12 99.21 94.21 79.21 n/a #VALUE!MW-13 98.45 93.45 78.45 n/a #VALUE!MW-14 100.60 95.60 80.60 n/a #VALUE!MW-15 97.06 92.06 77.06 n/a #VALUE!MW-16 97.18 92.18 77.18 n/a #VALUE!MW-17 94.62 89.62 74.62 n/a #VALUE!VEW-1 99.96 32.96 22.96 n/a #VALUE!All measurements taken in feet and based on an arbitrary benchmark of 100 ft. established at MW-3Groundwater levels measured on 1/29/2021HH3
TABLE 4SUMMARY OF GROUNDWATER ANALYTICAL RESULTSHANDY HOUSE 36724 HWY 70, NEWPORT, NC 28570Constituent MW-1 MW-2 MW-3 MW-8 MW-10 GCL 2L Standard Date1/29/2021 1/29/2021 1/29/2021 1/29/2021 1/29/2021 Method 6200B (ug/L)Benzene BDL BDL BDL BDL BDL 5,000 1Toluene BDL BDL 2.7 BDL BDL 260,000 600Ethylbenzene BDL 0.7 163 BDL BDL 84,500 600Xylenes (total) BDL BDL 319 BDL BDL 85,500 500BTEX (total) 0 0.7 484.7 0 0 NSE NSEp-Isopropyltoluene BDL BDL BDL BDL BDL NSE NSEIsopropylbenzene BDL 0.51 38 BDL BDL 25,000 70Diisopropyl Ether (DIPE) BDL BDL BDL BDL BDL 70,000 70Naphthalene BDL 2.5251BDL 5.1 6,000 6n-propylbenzene BDL BDL BDL BDL BDL 30,000 70n-butylbenzene BDL BDL BDL BDL BDL 6,900 70sec-butylbenzene 4.7 2 BDL BDL BDL 8,500 70tert-butylbenzene BDL BDL BDL BDL BDL 7,000 70Methyl-tert-butyl-ether (MTBE) BDL BDL BDL BDL BDL 20,000 20Acetone BDL BDL BDL BDL BDL 6,000,000 6,0001,2,3-Trichloropropane BDL BDL BDL BDL BDL NSE NSEMethyl Isobutyl Ketone BDL BDL BDL BDL BDL 100,000 1001,2,4-Trimethylbenzene 7 BDL630BDL 201 28,500 4001,3,5-Trimethylbenzene 12 BDL 252 BDL BDL 25,000 400TOTAL 6200B 23.7 5.71 1655.7 0 206.1 15,000 15Aliphatic Fraction Classes (ug/L)C5-C8 Volatile Aliphatics N/A N/A N/A N/A N/A NSE 400C9-C12 Volatile Aliphatics N/A N/A N/A N/A N/A NSE NSEC9-C18 Extractable Aliphatics N/A N/A N/A N/A N/A NSE 700C9-C18 Aliphatics (total) N/A N/A N/A N/A N/A NSE 700C19-C36 Extractable Aliphatics N/A N/A N/A N/A N/A NSE 10,000Aromatic Fraction Classes (ug/L)C9-C10 Volatile Aromatics N/A N/A N/A N/A N/A NSE NSEC11-C22 Extractable Aromatics N/A N/A N/A N/A N/A NSE NSEC9-C22 Aromatics (total)N/AN/AN/AN/AN/ANSE 200N/A = Not Analyzed BDL = Below Detection Limits NSE = No Standard Established
TABLE 4 (Continued)SUMMARY OF GROUNDWATER ANALYTICAL RESULTSHANDY HOUSE 36724 HWY 70, NEWPORT, NC 28570Constituent SW-3 GCL 2L Standard Date1/29/2021 Method 6200B (ug/L)Benzene BDL 5,000 1Toluene BDL 260,000 600Ethylbenzene BDL 84,500 600Xylenes (total) BDL 85,500 500BTEX (total) 0 NSE NSEp-Isopropyltoluene BDL NSE NSEIsopropylbenzene BDL 25,000 70Diisopropyl Ether (DIPE) BDL 70,000 70Naphthalene BDL 6,000 6n-propylbenzene BDL 30,000 70n-butylbenzene BDL 6,900 70sec-butylbenzene BDL 8,500 70tert-butylbenzene BDL 7,000 70Methyl-tert-butyl-ether (MTBE) BDL 20,000 201,2,4-Trimethylbenzene BDL 28,500 4001,3,5-Trimethylbenzene BDL 25,000 400Acetone BDL 6,000,000 6000TOTAL 6200B 0 15,000 15Aliphatic Fraction Classes (ug/L)C5-C8 Volatile Aliphatics N/A NSE 400C9-C12 Volatile Aliphatics N/A NSE NSEC9-C18 Extractable Aliphatics N/A NSE 700C9-C18 Aliphatics (total) N/A NSE 700C19-C36 Extractable Aliphatics N/A NSE 10,000Aromatic Fraction Classes (ug/L)C9-C10 Volatile Aromatics N/A NSE NSEC11-C22 Extractable Aromatics N/A NSE NSEC9-C22 Aromatics (total)N/ANSE 200N/A = Not AnalyzedBDL = Below Detection LimitsNSE = No Standard Established
WellIdentification IW-2 SW-3 SW-4 SW-5 SW-6Owner Name Atlantic Coast Properties Elaine Honeycutt Dominick Spadaro Christine Arnette Daniel ClapsadlOwner Address 112 Queen Creek Rd #1 313 Brook Lane 303 Roberts Road 297 Roberts Road 332 Roberts RoadSwansboro, NC 28584 Newport, NC 28570 Newport, NC 28570 Newport, NC 28570 Newport, NC 28570Well Address 6650 Highway 70 6760 Hwy 70 303 Roberts Road 297 Roberts Road 332 Roberts RoadNewport, NC 28570 Newport, NC 28570 Newport, NC 28570 Newport, NC 28570 Newport, NC 28570Occupant Unoccupied Second Go-Round Co Dominick Spadaro Larry & Ashley Arnette Daniel ClapsadlTelephone # none [phone] [phone] [phone] [phone]UseOut of Service -no structureDrinking - Potable Drinking - Potable Drinking - Potable Drinking - PotableDistance 300' 485' 765' 855' 890'City Water? NO NO NO NO NODepth of Well Unknown Unknown Unknown Unknown UnknownWell Diameter Unknown Unknown Unknown Unknown UnknownWell Yield Unknown Unknown Unknown Unknown UnknownDepth to Pump Unknown Unknown Unknown Unknown UnknownDepth of Casing Unknown Unknown Unknown Unknown UnknownStatic Water Unknown Unknown Unknown Unknown UnknownTABLE 5SUPPLY WELL INFORMATION1,000' RADIUSHANDY HOUSE #36724 HWY 70, NEWPORT, NC 28570
Estimated Area  (Ft2) Est. Thickness  (ft) Avg Cont. Level (ppm) Est. Cont. Mass (lbs) EstimatedDate Zone  Soil in  Soil in Soil in  Soil in Soil in  Soil in Soil in  Soil in Total Massof  Isonconcen. Source  Smear  Source  Smear  Source  Smear  Source  Smear Measurement Designation Area Zone GH2O Area Zone GH2O Area Zone GH2O Area Zone GH2O in LbsAug‐14 UST Pit 50 200 6720 2 6 6 200 1200 50 2.2222 160 31.441 193.66336Aug‐14 Downgradient 0 0 13510 0 0 10 0 0 0.5 0 0 1.0535 1.0534963Date Totals 2.2222 160 32.495 194.716851/29/2021 UST Pit 50 200 900 2 6 6 200 1200 10 2.2222 160 0.8422 163.06441/29/2021 Downgradient 0 0 3940 0 0 10 0 0 0.5 0 0 0.3072 0.3072373Date Totals 2.2222 160 1.1494 163.37163% Mass Reduction 0 0.9646 0.1609785Estimated Soil Porosity = 0.25Estimated Soil Density = 1.5 tons/cubic yardSoil CalculationsArea x Thickness x Density/27 x 2000lbs/ton x contaminated fraction (ppm) Groundwater Calculations 6200B compounds assumed to represent 10% of total dissolved organic compoundsArea x Thickness x porosity x 7.48 gallons/cu.ft. x 8.34 lbs/gallon x contaminated fraction (ppm)TABLE 6 - MASS CALCULATION TABLEHandy House 3, 6724 Hwy 70, Newport, NC  28570
NC 2L Standard 600 600 500 70 6 20 70 400 400 N/A
NC GCL Standard 260000 84500 85500 25000 6000 20000 30000 28500 25000 N/A
Toluene Ethyl- Xylenes Isopro- Napht MTBE n-propyl 1,2,4-tri- 1,3,5-tri- Total GH2O
Well Date Benzene benzene halene benzene methylbenz methylbenz 6200B Elev
# Sampled (ug/l) (ug/l) (ug/l) (ug/l) (ug/l) (ug/l) (ug/l) (ug/l) (ug/l) (ug/l) (ft)
MW-1 7/11/2013 BDL 4.3 206.4 34.3 17.1 BDL 70.7 1120 321 1528.8 89.76
5/7/2014 17.4 16.2 274.5 34.3 65.9 BDL 81.2 1950 684 2781.1 94.94
8/28/2014 BDL 7 226 122 67.3 BDL 111 4920 1760 6858.3 95.41
3/10/2015 BDL BDL 80.5 70.5 BDL BDL 72.6 2700 1190 3962.6 95.59
11/29/2015 BDL BDL 61.2 34.8 BDL BDL 17.5 3140 1460 4617.5 95.77
8/28/2016 BDL BDL BDL 25.3 BDL BDL 9.1 975 346 1330.1 93.91
3/18/2017 BDL BDL 7.7 6.3 BDL BDL 7.4 191 34.7 233.1 92.92
10/16/2017 BDL BDL 11.2 15.1 BDL BDL BDL 624 419 1043 93.05
5/16/2018 BDL 0.55 15 15.55 1.8 BDL 8.4 450 300 760.2 94.23
2/14/2019 BDL BDL BDL BDL BDL BDL BDL 166 306 472 95.1
3/18/2020 BDL BDL BDL 1.1 BDL BDL BDL 82.6 86.2 168.8 94.5
3/18/2020 BDL BDL BDL BDL BDL BDL BDL 7 12 23.7 94.87
MW-2 7/11/2013 8.6 127 1274.3 55.8 372 BDL 155 2030 722 4744.7 93.31
5/7/2014 134 646 824 58 322 BDL 126 672 90.2 2872.2 94.37
8/28/2014 BDL 283 9.4 36.5 276 BDL 91.2 152 BDL 848.1 94.87
3/10/2015 BDL 93.7 18.9 16.9 166 BDL 32.6 BDL BDL 328.1 95.02
11/29/2015 BDL 37 7.5 8.9 91.9 BDL 16.3 14.1 16.5 192.2 95.26
8/28/2016 BDL 90.8 0.68 16.8 135 BDL 38.3 1.5 0.93 284.01 93.53
3/18/2017 BDL 9.9 1.9 11.8 3.9 BDL 8.6 8.2 1.3 45.6 92.05
10/16/2017 BDL 7.7 1.3 9 26.7 BDL 4.8 2.2 BDL 51.7 92.2
5/16/2018 BDL 1.1 BDL BDL 9 BDL 0.68 BDL BDL 10.78 93.32
2/14/2019 BDL BDL BDL BDL 3.4 BDL BDL BDL BDL 3.4 94.05
3/18/2020 BDL 0.66 BDL 0.56 2.7 BDL BDL 0.51 BDL 4.43 93.59
3/18/2020 BDL 0.7 BDL 0.51 2.5 BDL BDL BDL BDL 3.71 94.01
MW-3 7/11/2013 2390 1800 19590 183 1170 41.7 410 4690 1410 31684.7 92.88
5/7/2014 414 392 2900 34.9 328 BDL 73.3 1010 233 5385.2 89.28
8/28/2014 469 474 3850 45.7 457 BDL 101 1310 320 7026.7 91.72
3/10/2015 570 596 3060 53.2 370 BDL 125 925 290 5989.2 94.15
11/29/2015 108 260 2353 38.7 371 BDL 93.6 972 271 4467.3 93.96
8/28/2016 162 298 2044 33.7 352 BDL 82.7 899 244 4115.4 92.26
3/18/2017 BDL 63.9 133.5 14.9 133 BDL 34.4 230 88.5 698.2 91.25
10/16/2017 0.74 13.7 32.4 3.1 38.4 BDL BDL 66.1 46.4 200.84 91.45
5/16/2018 3.1 180 1200 37 290 BDL 90 930 460 3190.1 92.57
2/14/2019 BDL 72.9 481 32.7 333 BDL 84.5 1380 618 3002.1 93.39
3/18/2020 7.9 338 734 55.7 332 BDL BDL 972 BDL 2439.6 92.99
3/18/2020 2.7 163 319 38 251 BDL BDL 630 252 1655.7 93.17
MW-4 7/11/2013 BDL BDL BDL BDL BDL 0.64 BDL BDL BDL 0.64 92.97
5/7/2014 BDL BDL BDL BDL BDL 0.64 BDL BDL BDL 0.64 93.91
8/28/2014 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 94.7
3/10/2015 1.5 0.55 2.69 BDL BDL BDL BDL 1.1 BDL 5.84 94.83
11/29/2015 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 95.44
8/28/2016 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 93.14
MW-5 7/11/2013 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 93.57
5/7/2014 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 95.28
8/28/2014 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 95.7
3/10/2015 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 95.88
11/29/2015 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 95.92
8/28/2016 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 94.01
MW-6 5/7/2014 BDL 1.5 7.1 BDL BDL BDL 0.65 4.4 0.93 14.58 94.72
8/28/2014 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 95.06
3/10/2015 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 95.23
11/29/2015 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 95.33
8/28/2016 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 93.73
MW-7 5/7/2014 BDL 0.59 BDL BDL BDL 0.64 BDL BDL BDL 1.23 93.45
8/28/2014 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 93.91
3/10/2015 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 93.99
11/29/2015 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 94.23
8/28/2016 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 92.8
TABLE 7: SUMMARY OF 6200B GROUNDWATER ANALYTICAL RESULTS
Handy House #3, 6724 Hwy 70, Newport, NC 28570
MW-8 5/7/2014 18.3 610 546 65.5 392 BDL 148 937 222 2938.8 90.01
8/28/2014 3.9 343 87.5 35.6 234 BDL 86 267 20 1077 93.02
3/10/2015 BDL 303 11 39.3 189 BDL 91.4 44 10.2 687.9 93.63
11/29/2015 BDL 306 BDL 41.7 231 BDL 101 5.9 BDL 685.6 94.14
8/28/2016 BDL 91.4 BDL 13 81.3 BDL 30.2 1.4 BDL 217.3 92.32
3/18/2017 1.2 BDL BDL BDL BDL BDL BDL BDL BDL 1.2 91.02
10/16/2017 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 91.25
5/16/2018 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 92.24
2/14/2019 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 92.86
3/18/2020 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 92.46
1/29/2021 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 92.52
MW-9 5/7/2014 10.8 608 2990 70 255 BDL 157 1150 254 5494.8 90.32
8/28/2014 BDL 36.2 25.2 5 28.8 BDL 14.6 88.4 19.8 218 93.94
3/11/2015 1.8 16.5 18.9 39.3 189 BDL 9.6 41.1 4.8 321 93.84
11/28/2015 BDL 26.8 6.1 4.8 27.8 BDL 14 52.1 10.4 142 94.94
8/28/2016 27.5 556 2370 57.9 279 BDL 150 1380 338 5158.4 92.65
3/18/2017 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 91.94
10/16/2017 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 91.6
5/16/2018 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 92.88
2/14/2019 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 93.76
3/18/2020 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 93.21
MW-10 5/7/2014 3.2 848 5350 94.6 304 0.81 206 1560 357 8723.61 93.06
8/28/2014 12.8 419 2704 54 253 BDL 142 1100 284 4968.8 93.63
3/11/2015 9.7 238 1558 30.9 105 BDL 83.9 655 161 2841.5 93.77
11/28/2015 BDL 285 1893 37.7 268 BDL 93.5 948 391 3916.2 95.36
8/28/2016 5 391 2596 56.8 293 BDL 150 1380 338 5209.8 93.24
3/18/2017 BDL 3.9 30.8 5 10 BDL 17.1 180 53.9 300.7 92.37
10/16/2017 BDL 4.6 39.2 2.5 10.7 BDL BDL 141 46.4 244.4 92.61
5/16/2018 BDL 5.9 180 5.9 74 BDL 15 850 270 1400.8 93.78
2/14/2019 BDL 2.4 37.2 3.4 23.7 BDL 8.4 465 156 696.1 94.55
3/18/2020 BDL BDL 7.5 BDL 34.9 BDL BDL 289 BDL 331.4 93.95
1/29/2021 BDL BDL BDL BDL 5.1 BDL BDL 201 BDL 206.1 94.18
MW-11 5/7/2014 BDL 4.4 23.7 0.56 6.2 BDL 1.8 13.4 2.8 52.86 95.11
8/28/2014 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 95.54
3/11/2015 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 95.75
11/28/2015 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 95.9
8/21/2016 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 93.91
2/14/2019 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 95.34
3/18/2020 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 94.73
MW-12 5/7/2014 BDL 2.2 5.2 BDL 2.4 3.6 0.65 4.8 0.83 19.68 92.61
8/28/2014 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 93.09
3/11/2015 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 93.29
11/28/2015 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 93.86
8/28/2016 BDL BDL BDL BDL BDL 0.56 BDL BDL BDL 0.56 91.13
3/18/2017 BDL BDL BDL BDL BDL 0.57 BDL BDL BDL 0.57 90.34
MW-13 6/7/2014 14.5 441 1023 38.2 232 5.5 85.7 717 143 2699.9 92.06
8/28/2014 BDL 16.2 5.8 1.9 8.6 BDL 4.9 23.6 5.5 66.5 92.46
3/10/2015 BDL 218 1.3 25.8 122 BDL 61.6 20.9 BDL 449.6 92.54
11/29/2015 BDL 16.3 BDL 4 BDL BDL 11.3 1.5 BDL 33.1 92.72
MW-14 5/7/2014 BDL 3 9.1 BDL BDL BDL 0.67 3.9 BDL 16.67 93.74
8/28/2014 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 93.96
3/11/2015 2.2 0.93 4.1 25.8 BDL 0.52 BDL 0.52 1.7 35.77 94.13
11/28/2015 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 94.8
8/28/2016 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 92.56
5/16/2018 BDL BDL BDL BDL 0.84 BDL BDL BDL BDL 0.84 92.3
2/14/2019 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 93.43
3/18/2020 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 93.46
MW-15 8/28/2014 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 90.34
3/10/2015 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 91.21
11/29/2015 BDL 3.4 BDL 2 BDL BDL 1.4 BDL BDL 6.8 91.58
8/28/2016 BDL 0.82 BDL 2.7 BDL BDL BDL BDL BDL 3.52 87.41
3/18/2017 BDL BDL BDL BDL BDL 7.9 BDL BDL BDL 7.9 86.92
10/16/2017 BDL BDL BDL BDL BDL 15.4 BDL BDL BDL 15.4 85.83
5/16/2018 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 88.25
2/14/2019 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 88.39
3/18/2020 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 88.39
MW-16 8/28/2014 BDL 15.6 BDL 4.8 4.3 BDL 9.9 0.74 BDL 35.34 91.78
3/10/2015 BDL 8.9 BDL 0.78 2.9 1.7 1.7 1.1 BDL 17.08 91.86
11/29/2015 BDL 68.9 BDL 14 21.4 BDL 22.4 77 BDL 203.7 92.49
8/28/2016 BDL 2 BDL 4.6 BDL BDL BDL BDL BDL 6.6 89.54
3/18/2017 BDL BDL BDL 1.1 BDL BDL BDL BDL BDL 1.1 88.82
MW-17 8/28/2014 BDL BDL BDL BDL BDL 1.1 BDL BDL BDL 1.1 90.32
3/10/2015 BDL BDL BDL BDL BDL BDL 0.61 BDL BDL 0.61 84.75
11/29/2015 BDL 4.7 BDL 1.1 BDL 3 1.6 BDL BDL 10.4 88.95
8/28/2016 BDL 0.56 BDL BDL BDL 3.9 BDL BDL BDL 4.46 86.34
10/16/2017 BDL BDL BDL BDL BDL 0.55 BDL BDL BDL 0.55 88.37
5/16/2018 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 89.01
2/14/2019 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 89.66
3/18/2020 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 90.28
VEW-1 5/7/2014 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 78.82
8/28/2014 4.8 1.5 9.4 BDL BDL BDL BDL 1.1 BDL 16.8 78.12
3/11/2015 4.3 1.6 7.7 BDL BDL BDL BDL 2.3 0.68 16.58 78.71
11/28/2015 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 78.84
8/28/2016 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 76.56
2/14/2019 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 78.97
3/18/2020 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 78.55
SW-1 5/7/2014 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
8/28/2014 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
3/10/2015 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
11/29/2015 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
8/28/2016 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
3/18/2017 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
SW-3 8/28/2014 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
3/10/2015 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
11/29/2015 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
8/28/2016 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
3/18/2017 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
10/16/2017 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
5/16/2018 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
2/14/2019 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
3/18/2020 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
1/29/2021 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
BDL = Below Detection Limits
NSE = No Standard Established
N/A = Not Applicable
TABLE 8SUMMARY OF GROUNDWATER ANALYTICAL RESULTSHANDY HOUSE 36724 HWY 70, NEWPORT, NC 28570Constituent MW-1 MW-2 MW-3 MW-4 MW-5 GCL 2L Standard Date8/28/2014 8/28/2014 8/28/2014 8/28/2014 8/28/2014 Method 6200B (ug/L)Benzene BDL BDL BDL BDL BDL 5,000 1Toluene BDL BDL 469 BDL BDL 260,000 600Ethylbenzene 7 283 474 BDL BDL 84,500 600Xylenes (total) 226.1 9.43850BDL BDL 85,500 500BTEX (total) 233.1 292.4 4793 0 0 NSE NSEp-Isopropyltoluene BDL BDL BDL BDL BDL NSE NSEIsopropylbenzene12236.5 45.7 BDL BDL 25,000 70Diisopropyl Ether (DIPE) BDL BDL BDL BDL BDL 70,000 70Naphthalene67.3 276 457BDL BDL 6,000 6n-propylbenzene111 91.2 101BDL BDL 30,000 70n-butylbenzene BDL 17.9 BDL BDL BDL 6,900 70sec-butylbenzene BDL 9.3 BDL BDL BDL 8,500 70Methyl-tert-butyl-ether (MTBE) BDL BDL BDL BDL BDL 20,000 201,2,4-Trimethylbenzene49201521310BDL BDL 28,500 4001,3,5-Trimethylbenzene1760BDL 320 BDL BDL 25,000 400Tetrachloroethene BDL BDL BDL BDL BDL 700 0.7Acetone BDL BDL BDL BDL BDL 6,000,000 6000Total 6200B 7213.4 875.3 7026.7 0 0 15,000 15Aliphatic Fraction Classes (ug/L) 4/12/2014 4/12/2014 4/12/2014 4/12/2014 4/12/2014C5-C8 Volatile Aliphatics BDL BDL876BDL BDL NSE 400C9-C12 Volatile Aliphatics 7,840 6,600 11,900 BDL BDL NSE NSEC9-C18 Extractable Aliphatics N/A N/A N/A N/A N/A NSE 700C9-C18 Aliphatics (total)7,840 6,600 11,900BDL BDL NSE 700C19-C36 Extractable Aliphatics N/A N/A N/A N/A N/A NSE 10,000Aromatic Fraction Classes (ug/L)C9-C10 Volatile Aromatics 3,840 1,540 2,160 BDL BDL NSE NSEC11-C22 Extractable Aromatics N/A N/A N/A N/A N/A NSE NSEC9-C22 Aromatics (total)3,840 1,540 2,160BDL BDLNSE 200N/A = Not AnalyzedBDL = Below Detection LimitsNSE = No Standard Established
TABLE 8 (Continued)SUMMARY OF GROUNDWATER ANALYTICAL RESULTSHANDY HOUSE 36724 HWY 70, NEWPORT, NC 28570Constituent MW-6 MW-7 MW-8 MW-9 MW-10 GCL 2L Standard Date8/28/2014 8/28/2014 8/28/2014 8/28/2014 8/28/2014 Method 6200B (ug/L)Benzene BDL BDL BDL BDL BDL 5,000 1Toluene BDL BDL 3.9 BDL 12.8 260,000 600Ethylbenzene BDL BDL 343 36.2 419 84,500 600Xylenes (total) BDL BDL 87.5 25.2270485,500 500BTEX (total) 0 0 434.4 61.4 3135.8 NSE NSEp-Isopropyltoluene BDL BDL BDL BDL BDL NSE NSEIsopropylbenzene BDL BDL 35.6 5 54 25,000 70Diisopropyl Ether (DIPE) BDL BDL BDL BDL BDL 70,000 70Naphthalene BDL BDL234 28.8 2536,000 6n-propylbenzene BDL BDL8614.614230,000 70n-butylbenzene BDL BDL BDL BDL BDL 6,900 70sec-butylbenzene BDL BDL BDL BDL BDL 8,500 70Methyl-tert-butyl-ether (MTBE) BDL BDL BDL BDL BDL 20,000 201,2,4-Trimethylbenzene BDL BDL 267 88.4110028,500 4001,3,5-Trimethylbenzene BDL BDL 20 19.8 284 25,000 400Tetrachloroethene BDL BDL BDL BDL BDL 700 0.7Styrene BDL BDL BDL BDL BDL 70,000 70Total 6200B 0 0 1077 218 4968.8 15,000 15Aliphatic Fraction Classes (ug/L) 4/12/2014 4/12/2014 4/12/2014 4/12/2014 4/12/2014C5-C8 Volatile Aliphatics BDL BDL BDL BDL BDL NSE 400C9-C12 Volatile Aliphatics BDL BDL 6,950 12,500 21,400 NSE NSEC9-C18 Extractable Aliphatics N/A N/A N/A N/A N/A NSE 700C9-C18 Aliphatics (total) BDL BDL6,950 12,500 21,400NSE 700C19-C36 Extractable Aliphatics N/A N/A N/A N/A N/A NSE 10,000Aromatic Fraction Classes (ug/L)C9-C10 Volatile Aromatics BDL BDL 2,020 2,180 3,310 NSE NSEC11-C22 Extractable Aromatics N/A N/A N/A N/A N/A NSE NSEC9-C22 Aromatics (total) BDL BDL2,020 2,180 3,310NSE 200N/A = Not AnalyzedBDL = Below Detection LimitsNSE = No Standard Established
TABLE 8 (Continued)SUMMARY OF GROUNDWATER ANALYTICAL RESULTSHANDY HOUSE 36724 HWY 70, NEWPORT, NC 28570Constituent MW-11 MW-12 MW-13 MW-14 VEW-1 GCL 2L Standard Date8/28/2014 8/28/2014 8/28/2014 8/28/2014 8/28/2014 Method 6200B (ug/L)Benzene BDL BDL BDL BDL BDL 5,000 1Toluene BDL BDL BDL BDL 4.8 260,000 600Ethylbenzene BDL BDL 16.2 BDL 1.5 84,500 600Xylenes (total) BDL BDL 5.8 BDL 9.4 85,500 500BTEX (total) 0 0 22 0 15.7 NSE NSEp-Isopropyltoluene BDL BDL BDL BDL BDL NSE NSEIsopropylbenzene BDL BDL 1.9 BDL BDL 25,000 70Diisopropyl Ether (DIPE) BDL BDL BDL BDL BDL 70,000 70Naphthalene BDL BDL8.6BDL BDL 6,000 6n-propylbenzene BDL BDL 4.9 BDL BDL 30,000 70n-butylbenzene BDL BDL BDL BDL BDL 6,900 70sec-butylbenzene BDL BDL BDL BDL BDL 8,500 70Methyl-tert-butyl-ether (MTBE) BDL BDL BDL BDL BDL 20,000 201,2,4-Trimethylbenzene BDL BDL 23.6 BDL 1.1 28,500 4001,3,5-Trimethylbenzene BDL BDL 5.5 BDL BDL 25,000 400Methylene Chloride BDL BDL BDL BDL BDL 5,000 5Styrene BDL BDL BDL BDL BDL 70,000 70TOTAL 0 0 66.5 0 16.8 15,000 15Aliphatic Fraction Classes (ug/L) 4/12/2014 5/7/2014 5/7/2014 5/7/2014 5/7/2014C5-C8 Volatile Aliphatics BDL BDL BDL BDL BDL NSE 400C9-C12 Volatile Aliphatics 68.6 BDL 5720 BDL BDL NSE NSEC9-C18 Extractable Aliphatics N/A N/A N/A N/A N/A NSE 700C9-C18 Aliphatics (total) 68.6 BDL5720BDL BDL NSE 700C19-C36 Extractable Aliphatics N/A N/A N/A N/A N/A NSE 10,000Aromatic Fraction Classes (ug/L)C9-C10 Volatile Aromatics BDL BDL 1380 BDL BDL NSE NSEC11-C22 Extractable Aromatics N/A N/A N/A N/A N/A NSE NSEC9-C22 Aromatics (total) BDL BDL1,380BDL BDLNSE 200N/A = Not AnalyzedBDL = Below Detection LimitsNSE = No Standard Established
TABLE 8 (Continued)SUMMARY OF GROUNDWATER ANALYTICAL RESULTSHANDY HOUSE 36724 HWY 70, NEWPORT, NC 28570Constituent MW-15 MW-16 MW-17 SW-1 SW-3 GCL 2L Standard Date8/28/2014 8/28/2014 8/28/2014 8/28/2014 8/28/2014 Method 6200B (ug/L)Benzene BDL BDL BDL BDL BDL 5,000 1Toluene BDL BDL BDL BDL BDL 260,000 600Ethylbenzene BDL 15.6 BDL BDL BDL 84,500 600Xylenes (total) BDL BDL BDL BDL BDL 85,500 500BTEX (total) 0 15.6 0 0 0 NSE NSEp-Isopropyltoluene BDL BDL BDL BDL BDL NSE NSEIsopropylbenzene BDL 4.8 BDL BDL BDL 25,000 70Diisopropyl Ether (DIPE) BDL BDL BDL BDL BDL 70,000 70Naphthalene BDL 4.3 BDL BDL BDL 6,000 6n-propylbenzene BDL 9.9 BDL BDL BDL 30,000 70n-butylbenzene BDL 1.1 BDL BDL BDL 6,900 70sec-butylbenzene BDL 0.93 BDL BDL BDL 8,500 70Methyl-tert-butyl-ether (MTBE) BDL BDL 1.1 BDL BDL 20,000 201,2,4-Trimethylbenzene BDL 0.74 BDL BDL BDL 28,500 4001,3,5-Trimethylbenzene BDL BDL BDL BDL BDL 25,000 400Methylene Chloride BDL BDL BDL BDL BDL 5,000 5Styrene BDL BDL BDL BDL BDL 70,000 70TOTAL 0 37.37 1.1 0 0 15,000 15Aliphatic Fraction Classes (ug/L) 8/28/2014 8/28/2014 8/28/2014 8/28/2014 8/28/2014C5-C8 Volatile Aliphatics BDL BDL BDL BDL BDL NSE 400C9-C12 Volatile Aliphatics 951 122 BDL BDL BDL NSE NSEC9-C18 Extractable Aliphatics N/A N/A N/A N/A N/A NSE 700C9-C18 Aliphatics (total)951122 BDL BDL BDL NSE 700C19-C36 Extractable Aliphatics N/A N/A N/A N/A N/A NSE 10,000Aromatic Fraction Classes (ug/L)C9-C10 Volatile Aromatics BDL BDL BDL BDL BDL NSE NSEC11-C22 Extractable Aromatics N/A N/A N/A N/A N/A NSE NSEC9-C22 Aromatics (total) BDL BDL BDL BDL BDLNSE 200N/A = Not AnalyzedBDL = Below Detection LimitsNSE = No Standard Established

APPENDIX A

LABORATORY ANALYTICAL RESULTS
#=CL#
February 05, 2021
LIMS USE: FR - HENRY NEMARGUT
LIMS OBJECT ID: 92519465
92519465
Project:
Pace Project No.:
RE:
Henry Nemargut
Henry Nemargut Engineering
2211 Chestnut Street
Wilmington, NC 28405
Handy House 3 (HH3)
Dear Henry Nemargut:
Enclosed are the analytical results for sample(s) received by the laboratory on January 29, 2021. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Bonnie Vang
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 35
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92519465
Handy House 3 (HH3)
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 35
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92519465
Handy House 3 (HH3)
Lab ID Sample ID Matrix Date Collected Date Received
92519465001 MW1 Water 01/29/21 12:15 01/29/21 17:30
92519465002 MW2 Water 01/29/21 12:40 01/29/21 17:30
92519465003 MW3 Water 01/29/21 13:05 01/29/21 17:30
92519465004 MW8 Water 01/29/21 13:40 01/29/21 17:30
92519465005 MW10 Water 01/29/21 14:00 01/29/21 17:30
92519465006 SW3 Water 01/29/21 14:15 01/29/21 17:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 35
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92519465
Handy House 3 (HH3)
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92519465001 MW1 SM 6200B 69 PASI-CSAS
92519465002 MW2 SM 6200B 69 PASI-CSAS
92519465003 MW3 SM 6200B 69 PASI-CSAS
92519465004 MW8 SM 6200B 69 PASI-CSAS
92519465005 MW10 SM 6200B 69 PASI-CSAS
92519465006 SW3 SM 6200B 69 PASI-CPM1
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 35
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92519465
Handy House 3 (HH3)
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92519465001 MW1
sec-Butylbenzene 4.7 ug/L 02/04/21 14:480.50SM 6200B
1,2,4-Trimethylbenzene 7.0 ug/L 02/04/21 14:480.50SM 6200B
1,3,5-Trimethylbenzene 12.0 ug/L 02/04/21 14:480.50SM 6200B
92519465002 MW2
sec-Butylbenzene 2.0 ug/L 02/04/21 13:350.50SM 6200B
Ethylbenzene 0.70 ug/L 02/04/21 13:350.50SM 6200B
Isopropylbenzene (Cumene)0.51 ug/L 02/04/21 13:350.50SM 6200B
Naphthalene 2.5 ug/L 02/04/21 13:352.0SM 6200B
92519465003 MW3
Ethylbenzene 163 ug/L 02/05/21 14:172.5SM 6200B
Isopropylbenzene (Cumene)38.0 ug/L 02/05/21 14:172.5SM 6200B
Naphthalene 251 ug/L 02/05/21 14:1710.0SM 6200B
Toluene 2.7 ug/L 02/05/21 14:172.5SM 6200B
1,2,4-Trimethylbenzene 630 ug/L 02/05/21 14:172.5SM 6200B
1,3,5-Trimethylbenzene 252 ug/L 02/05/21 14:172.5SM 6200B
m&p-Xylene 113 ug/L 02/05/21 14:175.0SM 6200B
o-Xylene 206 ug/L 02/05/21 14:172.5SM 6200B
92519465005 MW10
Naphthalene 5.1 ug/L 02/05/21 14:534.0SM 6200B
1,2,4-Trimethylbenzene 201 ug/L 02/05/21 14:531.0SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92519465
Handy House 3 (HH3)
Sample:MW1 Lab ID:92519465001 Collected:01/29/21 12:15 Received:01/29/21 17:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 02/04/21 14:48 75-85-41001
tert-Amylmethyl ether ND ug/L 02/04/21 14:48 994-05-810.0 1
Benzene ND ug/L 02/04/21 14:48 71-43-20.50 1
Bromobenzene ND ug/L 02/04/21 14:48 108-86-10.50 1
Bromochloromethane ND ug/L 02/04/21 14:48 74-97-50.50 1
Bromodichloromethane ND ug/L 02/04/21 14:48 75-27-40.50 1
Bromoform ND ug/L 02/04/21 14:48 75-25-20.50 1
Bromomethane ND ug/L 02/04/21 14:48 74-83-95.0 1
tert-Butyl Alcohol ND ug/L 02/04/21 14:48 75-65-020.0 1
n-Butylbenzene ND ug/L 02/04/21 14:48 104-51-80.50 1
sec-Butylbenzene 4.7 ug/L 02/04/21 14:48 135-98-80.50 1
tert-Butylbenzene ND ug/L 02/04/21 14:48 98-06-60.50 1
tert-Butyl Formate ND ug/L 02/04/21 14:48 762-75-420.0 1
Carbon tetrachloride ND ug/L 02/04/21 14:48 56-23-50.50 1
Chlorobenzene ND ug/L 02/04/21 14:48 108-90-70.50 1
Chloroethane ND ug/L 02/04/21 14:48 75-00-31.0 1
Chloroform ND ug/L 02/04/21 14:48 67-66-30.50 1
Chloromethane ND ug/L 02/04/21 14:48 74-87-31.0 1
2-Chlorotoluene ND ug/L 02/04/21 14:48 95-49-80.50 1
4-Chlorotoluene ND ug/L 02/04/21 14:48 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 02/04/21 14:48 96-12-81.0 1
Dibromochloromethane ND ug/L 02/04/21 14:48 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 02/04/21 14:48 106-93-40.50 1
Dibromomethane ND ug/L 02/04/21 14:48 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 02/04/21 14:48 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 02/04/21 14:48 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 02/04/21 14:48 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 02/04/21 14:48 75-71-80.50 1
1,1-Dichloroethane ND ug/L 02/04/21 14:48 75-34-30.50 1
1,2-Dichloroethane ND ug/L 02/04/21 14:48 107-06-20.50 1
1,1-Dichloroethene ND ug/L 02/04/21 14:48 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 02/04/21 14:48 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 02/04/21 14:48 156-60-50.50 1
1,2-Dichloropropane ND ug/L 02/04/21 14:48 78-87-50.50 1
1,3-Dichloropropane ND ug/L 02/04/21 14:48 142-28-90.50 1
2,2-Dichloropropane ND ug/L 02/04/21 14:48 594-20-70.50 1
1,1-Dichloropropene ND ug/L 02/04/21 14:48 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 02/04/21 14:48 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 02/04/21 14:48 10061-02-60.50 1
Diisopropyl ether ND ug/L 02/04/21 14:48 108-20-30.50 1
Ethanol ND ug/L 02/04/21 14:48 64-17-52001
Ethylbenzene ND ug/L 02/04/21 14:48 100-41-40.50 1
Ethyl-tert-butyl ether ND ug/L 02/04/21 14:48 637-92-310.0 1
Hexachloro-1,3-butadiene ND ug/L 02/04/21 14:48 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 02/04/21 14:48 98-82-80.50 1
Methylene Chloride ND ug/L 02/04/21 14:48 75-09-22.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/05/2021 03:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92519465
Handy House 3 (HH3)
Sample:MW1 Lab ID:92519465001 Collected:01/29/21 12:15 Received:01/29/21 17:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methyl-tert-butyl ether ND ug/L 02/04/21 14:48 1634-04-40.50 1
Naphthalene ND ug/L 02/04/21 14:48 91-20-32.0 1
n-Propylbenzene ND ug/L 02/04/21 14:48 103-65-10.50 1
Styrene ND ug/L 02/04/21 14:48 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 02/04/21 14:48 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 02/04/21 14:48 79-34-50.50 1
Tetrachloroethene ND ug/L 02/04/21 14:48 127-18-40.50 1
Toluene ND ug/L 02/04/21 14:48 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 02/04/21 14:48 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 02/04/21 14:48 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 02/04/21 14:48 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 02/04/21 14:48 79-00-50.50 1
Trichloroethene ND ug/L 02/04/21 14:48 79-01-60.50 1
Trichlorofluoromethane ND ug/L 02/04/21 14:48 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 02/04/21 14:48 96-18-40.50 1
1,2,4-Trimethylbenzene 7.0 ug/L 02/04/21 14:48 95-63-60.50 1
1,3,5-Trimethylbenzene 12.0 ug/L 02/04/21 14:48 108-67-80.50 1
Vinyl chloride ND ug/L 02/04/21 14:48 75-01-41.0 1
m&p-Xylene ND ug/L 02/04/21 14:48 179601-23-11.0 1
o-Xylene ND ug/L 02/04/21 14:48 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)79 %02/04/21 14:48 17060-07-070-130 1
4-Bromofluorobenzene (S)92 %02/04/21 14:48 460-00-470-130 1
Toluene-d8 (S)100 %02/04/21 14:48 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/05/2021 03:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92519465
Handy House 3 (HH3)
Sample:MW2 Lab ID:92519465002 Collected:01/29/21 12:40 Received:01/29/21 17:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 02/04/21 13:35 75-85-41001
tert-Amylmethyl ether ND ug/L 02/04/21 13:35 994-05-810.0 1
Benzene ND ug/L 02/04/21 13:35 71-43-20.50 1
Bromobenzene ND ug/L 02/04/21 13:35 108-86-10.50 1
Bromochloromethane ND ug/L 02/04/21 13:35 74-97-50.50 1
Bromodichloromethane ND ug/L 02/04/21 13:35 75-27-40.50 1
Bromoform ND ug/L 02/04/21 13:35 75-25-20.50 1
Bromomethane ND ug/L 02/04/21 13:35 74-83-95.0 1
tert-Butyl Alcohol ND ug/L 02/04/21 13:35 75-65-020.0 1
n-Butylbenzene ND ug/L 02/04/21 13:35 104-51-80.50 1
sec-Butylbenzene 2.0 ug/L 02/04/21 13:35 135-98-80.50 1
tert-Butylbenzene ND ug/L 02/04/21 13:35 98-06-60.50 1
tert-Butyl Formate ND ug/L 02/04/21 13:35 762-75-420.0 1
Carbon tetrachloride ND ug/L 02/04/21 13:35 56-23-50.50 1
Chlorobenzene ND ug/L 02/04/21 13:35 108-90-70.50 1
Chloroethane ND ug/L 02/04/21 13:35 75-00-31.0 1
Chloroform ND ug/L 02/04/21 13:35 67-66-30.50 1
Chloromethane ND ug/L 02/04/21 13:35 74-87-31.0 1
2-Chlorotoluene ND ug/L 02/04/21 13:35 95-49-80.50 1
4-Chlorotoluene ND ug/L 02/04/21 13:35 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 02/04/21 13:35 96-12-81.0 1
Dibromochloromethane ND ug/L 02/04/21 13:35 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 02/04/21 13:35 106-93-40.50 1
Dibromomethane ND ug/L 02/04/21 13:35 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 02/04/21 13:35 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 02/04/21 13:35 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 02/04/21 13:35 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 02/04/21 13:35 75-71-80.50 1
1,1-Dichloroethane ND ug/L 02/04/21 13:35 75-34-30.50 1
1,2-Dichloroethane ND ug/L 02/04/21 13:35 107-06-20.50 1
1,1-Dichloroethene ND ug/L 02/04/21 13:35 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 02/04/21 13:35 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 02/04/21 13:35 156-60-50.50 1
1,2-Dichloropropane ND ug/L 02/04/21 13:35 78-87-50.50 1
1,3-Dichloropropane ND ug/L 02/04/21 13:35 142-28-90.50 1
2,2-Dichloropropane ND ug/L 02/04/21 13:35 594-20-70.50 1
1,1-Dichloropropene ND ug/L 02/04/21 13:35 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 02/04/21 13:35 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 02/04/21 13:35 10061-02-60.50 1
Diisopropyl ether ND ug/L 02/04/21 13:35 108-20-30.50 1
Ethanol ND ug/L 02/04/21 13:35 64-17-52001
Ethylbenzene 0.70 ug/L 02/04/21 13:35 100-41-40.50 1
Ethyl-tert-butyl ether ND ug/L 02/04/21 13:35 637-92-310.0 1
Hexachloro-1,3-butadiene ND ug/L 02/04/21 13:35 87-68-32.0 1
Isopropylbenzene (Cumene)0.51 ug/L 02/04/21 13:35 98-82-80.50 1
Methylene Chloride ND ug/L 02/04/21 13:35 75-09-22.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/05/2021 03:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92519465
Handy House 3 (HH3)
Sample:MW2 Lab ID:92519465002 Collected:01/29/21 12:40 Received:01/29/21 17:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methyl-tert-butyl ether ND ug/L 02/04/21 13:35 1634-04-40.50 1
Naphthalene 2.5 ug/L 02/04/21 13:35 91-20-32.0 1
n-Propylbenzene ND ug/L 02/04/21 13:35 103-65-10.50 1
Styrene ND ug/L 02/04/21 13:35 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 02/04/21 13:35 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 02/04/21 13:35 79-34-50.50 1
Tetrachloroethene ND ug/L 02/04/21 13:35 127-18-40.50 1
Toluene ND ug/L 02/04/21 13:35 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 02/04/21 13:35 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 02/04/21 13:35 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 02/04/21 13:35 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 02/04/21 13:35 79-00-50.50 1
Trichloroethene ND ug/L 02/04/21 13:35 79-01-60.50 1
Trichlorofluoromethane ND ug/L 02/04/21 13:35 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 02/04/21 13:35 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 02/04/21 13:35 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 02/04/21 13:35 108-67-80.50 1
Vinyl chloride ND ug/L 02/04/21 13:35 75-01-41.0 1
m&p-Xylene ND ug/L 02/04/21 13:35 179601-23-11.0 1
o-Xylene ND ug/L 02/04/21 13:35 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)81 %02/04/21 13:35 17060-07-070-130 1
4-Bromofluorobenzene (S)93 %02/04/21 13:35 460-00-470-130 1
Toluene-d8 (S)100 %02/04/21 13:35 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/05/2021 03:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92519465
Handy House 3 (HH3)
Sample:MW3 Lab ID:92519465003 Collected:01/29/21 13:05 Received:01/29/21 17:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 02/05/21 14:17 75-85-45005
tert-Amylmethyl ether ND ug/L 02/05/21 14:17 994-05-850.0 5
Benzene ND ug/L 02/05/21 14:17 71-43-22.5 5
Bromobenzene ND ug/L 02/05/21 14:17 108-86-12.5 5
Bromochloromethane ND ug/L 02/05/21 14:17 74-97-52.5 5
Bromodichloromethane ND ug/L 02/05/21 14:17 75-27-42.5 5
Bromoform ND ug/L 02/05/21 14:17 75-25-22.5 5
Bromomethane ND ug/L 02/05/21 14:17 74-83-925.0 5
tert-Butyl Alcohol ND ug/L 02/05/21 14:17 75-65-01005
n-Butylbenzene ND ug/L 02/05/21 14:17 104-51-82.5 5
sec-Butylbenzene ND ug/L 02/05/21 14:17 135-98-82.5 5
tert-Butylbenzene ND ug/L 02/05/21 14:17 98-06-62.5 5
tert-Butyl Formate ND ug/L 02/05/21 14:17 762-75-41005
Carbon tetrachloride ND ug/L 02/05/21 14:17 56-23-52.5 5
Chlorobenzene ND ug/L 02/05/21 14:17 108-90-72.5 5
Chloroethane ND ug/L 02/05/21 14:17 75-00-35.0 5
Chloroform ND ug/L 02/05/21 14:17 67-66-32.5 5
Chloromethane ND ug/L 02/05/21 14:17 74-87-35.0 5
2-Chlorotoluene ND ug/L 02/05/21 14:17 95-49-82.5 5
4-Chlorotoluene ND ug/L 02/05/21 14:17 106-43-42.5 5
1,2-Dibromo-3-chloropropane ND ug/L 02/05/21 14:17 96-12-85.0 5
Dibromochloromethane ND ug/L 02/05/21 14:17 124-48-12.5 5
1,2-Dibromoethane (EDB)ND ug/L 02/05/21 14:17 106-93-42.5 5
Dibromomethane ND ug/L 02/05/21 14:17 74-95-32.5 5
1,2-Dichlorobenzene ND ug/L 02/05/21 14:17 95-50-12.5 5
1,3-Dichlorobenzene ND ug/L 02/05/21 14:17 541-73-12.5 5
1,4-Dichlorobenzene ND ug/L 02/05/21 14:17 106-46-72.5 5
Dichlorodifluoromethane ND ug/L 02/05/21 14:17 75-71-82.5 5
1,1-Dichloroethane ND ug/L 02/05/21 14:17 75-34-32.5 5
1,2-Dichloroethane ND ug/L 02/05/21 14:17 107-06-22.5 5
1,1-Dichloroethene ND ug/L 02/05/21 14:17 75-35-42.5 5
cis-1,2-Dichloroethene ND ug/L 02/05/21 14:17 156-59-22.5 5
trans-1,2-Dichloroethene ND ug/L 02/05/21 14:17 156-60-52.5 5
1,2-Dichloropropane ND ug/L 02/05/21 14:17 78-87-52.5 5
1,3-Dichloropropane ND ug/L 02/05/21 14:17 142-28-92.5 5
2,2-Dichloropropane ND ug/L 02/05/21 14:17 594-20-72.5 5
1,1-Dichloropropene ND ug/L 02/05/21 14:17 563-58-62.5 5
cis-1,3-Dichloropropene ND ug/L 02/05/21 14:17 10061-01-52.5 5
trans-1,3-Dichloropropene ND ug/L 02/05/21 14:17 10061-02-62.5 5
Diisopropyl ether ND ug/L 02/05/21 14:17 108-20-32.5 5
Ethanol ND ug/L 02/05/21 14:17 64-17-510005
Ethylbenzene 163 ug/L 02/05/21 14:17 100-41-42.5 5
Ethyl-tert-butyl ether ND ug/L 02/05/21 14:17 637-92-350.0 5
Hexachloro-1,3-butadiene ND ug/L 02/05/21 14:17 87-68-310.0 5
Isopropylbenzene (Cumene)38.0 ug/L 02/05/21 14:17 98-82-82.5 5
Methylene Chloride ND ug/L 02/05/21 14:17 75-09-210.0 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/05/2021 03:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92519465
Handy House 3 (HH3)
Sample:MW3 Lab ID:92519465003 Collected:01/29/21 13:05 Received:01/29/21 17:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methyl-tert-butyl ether ND ug/L 02/05/21 14:17 1634-04-42.5 5
Naphthalene 251 ug/L 02/05/21 14:17 91-20-310.0 5
n-Propylbenzene ND ug/L 02/05/21 14:17 103-65-12.5 5
Styrene ND ug/L 02/05/21 14:17 100-42-52.5 5
1,1,1,2-Tetrachloroethane ND ug/L 02/05/21 14:17 630-20-62.5 5
1,1,2,2-Tetrachloroethane ND ug/L 02/05/21 14:17 79-34-52.5 5
Tetrachloroethene ND ug/L 02/05/21 14:17 127-18-42.5 5
Toluene 2.7 ug/L 02/05/21 14:17 108-88-32.5 5
1,2,3-Trichlorobenzene ND ug/L 02/05/21 14:17 87-61-610.0 5
1,2,4-Trichlorobenzene ND ug/L 02/05/21 14:17 120-82-110.0 5
1,1,1-Trichloroethane ND ug/L 02/05/21 14:17 71-55-62.5 5
1,1,2-Trichloroethane ND ug/L 02/05/21 14:17 79-00-52.5 5
Trichloroethene ND ug/L 02/05/21 14:17 79-01-62.5 5
Trichlorofluoromethane ND ug/L 02/05/21 14:17 75-69-45.0 5
1,2,3-Trichloropropane ND ug/L 02/05/21 14:17 96-18-42.5 5
1,2,4-Trimethylbenzene 630 ug/L 02/05/21 14:17 95-63-62.5 5
1,3,5-Trimethylbenzene 252 ug/L 02/05/21 14:17 108-67-82.5 5
Vinyl chloride ND ug/L 02/05/21 14:17 75-01-45.0 5
m&p-Xylene 113 ug/L 02/05/21 14:17 179601-23-15.0 5
o-Xylene 206 ug/L 02/05/21 14:17 95-47-62.5 5
Surrogates
1,2-Dichloroethane-d4 (S)77 %02/05/21 14:17 17060-07-070-130 5
4-Bromofluorobenzene (S)92 %02/05/21 14:17 460-00-470-130 5
Toluene-d8 (S)96 %02/05/21 14:17 2037-26-570-130 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/05/2021 03:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92519465
Handy House 3 (HH3)
Sample:MW8 Lab ID:92519465004 Collected:01/29/21 13:40 Received:01/29/21 17:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 02/04/21 13:53 75-85-41001
tert-Amylmethyl ether ND ug/L 02/04/21 13:53 994-05-810.0 1
Benzene ND ug/L 02/04/21 13:53 71-43-20.50 1
Bromobenzene ND ug/L 02/04/21 13:53 108-86-10.50 1
Bromochloromethane ND ug/L 02/04/21 13:53 74-97-50.50 1
Bromodichloromethane ND ug/L 02/04/21 13:53 75-27-40.50 1
Bromoform ND ug/L 02/04/21 13:53 75-25-20.50 1
Bromomethane ND ug/L 02/04/21 13:53 74-83-95.0 1
tert-Butyl Alcohol ND ug/L 02/04/21 13:53 75-65-020.0 1
n-Butylbenzene ND ug/L 02/04/21 13:53 104-51-80.50 1
sec-Butylbenzene ND ug/L 02/04/21 13:53 135-98-80.50 1
tert-Butylbenzene ND ug/L 02/04/21 13:53 98-06-60.50 1
tert-Butyl Formate ND ug/L 02/04/21 13:53 762-75-420.0 1
Carbon tetrachloride ND ug/L 02/04/21 13:53 56-23-50.50 1
Chlorobenzene ND ug/L 02/04/21 13:53 108-90-70.50 1
Chloroethane ND ug/L 02/04/21 13:53 75-00-31.0 1
Chloroform ND ug/L 02/04/21 13:53 67-66-30.50 1
Chloromethane ND ug/L 02/04/21 13:53 74-87-31.0 1
2-Chlorotoluene ND ug/L 02/04/21 13:53 95-49-80.50 1
4-Chlorotoluene ND ug/L 02/04/21 13:53 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 02/04/21 13:53 96-12-81.0 1
Dibromochloromethane ND ug/L 02/04/21 13:53 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 02/04/21 13:53 106-93-40.50 1
Dibromomethane ND ug/L 02/04/21 13:53 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 02/04/21 13:53 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 02/04/21 13:53 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 02/04/21 13:53 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 02/04/21 13:53 75-71-80.50 1
1,1-Dichloroethane ND ug/L 02/04/21 13:53 75-34-30.50 1
1,2-Dichloroethane ND ug/L 02/04/21 13:53 107-06-20.50 1
1,1-Dichloroethene ND ug/L 02/04/21 13:53 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 02/04/21 13:53 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 02/04/21 13:53 156-60-50.50 1
1,2-Dichloropropane ND ug/L 02/04/21 13:53 78-87-50.50 1
1,3-Dichloropropane ND ug/L 02/04/21 13:53 142-28-90.50 1
2,2-Dichloropropane ND ug/L 02/04/21 13:53 594-20-70.50 1
1,1-Dichloropropene ND ug/L 02/04/21 13:53 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 02/04/21 13:53 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 02/04/21 13:53 10061-02-60.50 1
Diisopropyl ether ND ug/L 02/04/21 13:53 108-20-30.50 1
Ethanol ND ug/L 02/04/21 13:53 64-17-52001
Ethylbenzene ND ug/L 02/04/21 13:53 100-41-40.50 1
Ethyl-tert-butyl ether ND ug/L 02/04/21 13:53 637-92-310.0 1
Hexachloro-1,3-butadiene ND ug/L 02/04/21 13:53 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 02/04/21 13:53 98-82-80.50 1
Methylene Chloride ND ug/L 02/04/21 13:53 75-09-22.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/05/2021 03:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92519465
Handy House 3 (HH3)
Sample:MW8 Lab ID:92519465004 Collected:01/29/21 13:40 Received:01/29/21 17:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methyl-tert-butyl ether ND ug/L 02/04/21 13:53 1634-04-40.50 1
Naphthalene ND ug/L 02/04/21 13:53 91-20-32.0 1
n-Propylbenzene ND ug/L 02/04/21 13:53 103-65-10.50 1
Styrene ND ug/L 02/04/21 13:53 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 02/04/21 13:53 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 02/04/21 13:53 79-34-50.50 1
Tetrachloroethene ND ug/L 02/04/21 13:53 127-18-40.50 1
Toluene ND ug/L 02/04/21 13:53 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 02/04/21 13:53 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 02/04/21 13:53 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 02/04/21 13:53 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 02/04/21 13:53 79-00-50.50 1
Trichloroethene ND ug/L 02/04/21 13:53 79-01-60.50 1
Trichlorofluoromethane ND ug/L 02/04/21 13:53 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 02/04/21 13:53 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 02/04/21 13:53 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 02/04/21 13:53 108-67-80.50 1
Vinyl chloride ND ug/L 02/04/21 13:53 75-01-41.0 1
m&p-Xylene ND ug/L 02/04/21 13:53 179601-23-11.0 1
o-Xylene ND ug/L 02/04/21 13:53 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)80 %02/04/21 13:53 17060-07-070-130 1
4-Bromofluorobenzene (S)90 %02/04/21 13:53 460-00-470-130 1
Toluene-d8 (S)99 %02/04/21 13:53 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/05/2021 03:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92519465
Handy House 3 (HH3)
Sample:MW10 Lab ID:92519465005 Collected:01/29/21 14:00 Received:01/29/21 17:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 02/05/21 14:53 75-85-42002
tert-Amylmethyl ether ND ug/L 02/05/21 14:53 994-05-820.0 2
Benzene ND ug/L 02/05/21 14:53 71-43-21.0 2
Bromobenzene ND ug/L 02/05/21 14:53 108-86-11.0 2
Bromochloromethane ND ug/L 02/05/21 14:53 74-97-51.0 2
Bromodichloromethane ND ug/L 02/05/21 14:53 75-27-41.0 2
Bromoform ND ug/L 02/05/21 14:53 75-25-21.0 2
Bromomethane ND ug/L 02/05/21 14:53 74-83-910.0 2
tert-Butyl Alcohol ND ug/L 02/05/21 14:53 75-65-040.0 2
n-Butylbenzene ND ug/L 02/05/21 14:53 104-51-81.0 2
sec-Butylbenzene ND ug/L 02/05/21 14:53 135-98-81.0 2
tert-Butylbenzene ND ug/L 02/05/21 14:53 98-06-61.0 2
tert-Butyl Formate ND ug/L 02/05/21 14:53 762-75-440.0 2
Carbon tetrachloride ND ug/L 02/05/21 14:53 56-23-51.0 2
Chlorobenzene ND ug/L 02/05/21 14:53 108-90-71.0 2
Chloroethane ND ug/L 02/05/21 14:53 75-00-32.0 2
Chloroform ND ug/L 02/05/21 14:53 67-66-31.0 2
Chloromethane ND ug/L 02/05/21 14:53 74-87-32.0 2
2-Chlorotoluene ND ug/L 02/05/21 14:53 95-49-81.0 2
4-Chlorotoluene ND ug/L 02/05/21 14:53 106-43-41.0 2
1,2-Dibromo-3-chloropropane ND ug/L 02/05/21 14:53 96-12-82.0 2
Dibromochloromethane ND ug/L 02/05/21 14:53 124-48-11.0 2
1,2-Dibromoethane (EDB)ND ug/L 02/05/21 14:53 106-93-41.0 2
Dibromomethane ND ug/L 02/05/21 14:53 74-95-31.0 2
1,2-Dichlorobenzene ND ug/L 02/05/21 14:53 95-50-11.0 2
1,3-Dichlorobenzene ND ug/L 02/05/21 14:53 541-73-11.0 2
1,4-Dichlorobenzene ND ug/L 02/05/21 14:53 106-46-71.0 2
Dichlorodifluoromethane ND ug/L 02/05/21 14:53 75-71-81.0 2
1,1-Dichloroethane ND ug/L 02/05/21 14:53 75-34-31.0 2
1,2-Dichloroethane ND ug/L 02/05/21 14:53 107-06-21.0 2
1,1-Dichloroethene ND ug/L 02/05/21 14:53 75-35-41.0 2
cis-1,2-Dichloroethene ND ug/L 02/05/21 14:53 156-59-21.0 2
trans-1,2-Dichloroethene ND ug/L 02/05/21 14:53 156-60-51.0 2
1,2-Dichloropropane ND ug/L 02/05/21 14:53 78-87-51.0 2
1,3-Dichloropropane ND ug/L 02/05/21 14:53 142-28-91.0 2
2,2-Dichloropropane ND ug/L 02/05/21 14:53 594-20-71.0 2
1,1-Dichloropropene ND ug/L 02/05/21 14:53 563-58-61.0 2
cis-1,3-Dichloropropene ND ug/L 02/05/21 14:53 10061-01-51.0 2
trans-1,3-Dichloropropene ND ug/L 02/05/21 14:53 10061-02-61.0 2
Diisopropyl ether ND ug/L 02/05/21 14:53 108-20-31.0 2
Ethanol ND ug/L 02/05/21 14:53 64-17-54002
Ethylbenzene ND ug/L 02/05/21 14:53 100-41-41.0 2
Ethyl-tert-butyl ether ND ug/L 02/05/21 14:53 637-92-320.0 2
Hexachloro-1,3-butadiene ND ug/L 02/05/21 14:53 87-68-34.0 2
Isopropylbenzene (Cumene)ND ug/L 02/05/21 14:53 98-82-81.0 2
Methylene Chloride ND ug/L 02/05/21 14:53 75-09-24.0 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/05/2021 03:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92519465
Handy House 3 (HH3)
Sample:MW10 Lab ID:92519465005 Collected:01/29/21 14:00 Received:01/29/21 17:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methyl-tert-butyl ether ND ug/L 02/05/21 14:53 1634-04-41.0 2
Naphthalene 5.1 ug/L 02/05/21 14:53 91-20-34.0 2
n-Propylbenzene ND ug/L 02/05/21 14:53 103-65-11.0 2
Styrene ND ug/L 02/05/21 14:53 100-42-51.0 2
1,1,1,2-Tetrachloroethane ND ug/L 02/05/21 14:53 630-20-61.0 2
1,1,2,2-Tetrachloroethane ND ug/L 02/05/21 14:53 79-34-51.0 2
Tetrachloroethene ND ug/L 02/05/21 14:53 127-18-41.0 2
Toluene ND ug/L 02/05/21 14:53 108-88-31.0 2
1,2,3-Trichlorobenzene ND ug/L 02/05/21 14:53 87-61-64.0 2
1,2,4-Trichlorobenzene ND ug/L 02/05/21 14:53 120-82-14.0 2
1,1,1-Trichloroethane ND ug/L 02/05/21 14:53 71-55-61.0 2
1,1,2-Trichloroethane ND ug/L 02/05/21 14:53 79-00-51.0 2
Trichloroethene ND ug/L 02/05/21 14:53 79-01-61.0 2
Trichlorofluoromethane ND ug/L 02/05/21 14:53 75-69-42.0 2
1,2,3-Trichloropropane ND ug/L 02/05/21 14:53 96-18-41.0 2
1,2,4-Trimethylbenzene 201 ug/L 02/05/21 14:53 95-63-61.0 2
1,3,5-Trimethylbenzene ND ug/L 02/05/21 14:53 108-67-81.0 2
Vinyl chloride ND ug/L 02/05/21 14:53 75-01-42.0 2
m&p-Xylene ND ug/L 02/05/21 14:53 179601-23-12.0 2
o-Xylene ND ug/L 02/05/21 14:53 95-47-61.0 2
Surrogates
1,2-Dichloroethane-d4 (S)78 %02/05/21 14:53 17060-07-070-130 2
4-Bromofluorobenzene (S)91 %02/05/21 14:53 460-00-470-130 2
Toluene-d8 (S)99 %02/05/21 14:53 2037-26-570-130 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/05/2021 03:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92519465
Handy House 3 (HH3)
Sample:SW3 Lab ID:92519465006 Collected:01/29/21 14:15 Received:01/29/21 17:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 02/04/21 05:39 75-85-41001
tert-Amylmethyl ether ND ug/L 02/04/21 05:39 994-05-810.0 1
Benzene ND ug/L 02/04/21 05:39 71-43-2 L10.50 1
Bromobenzene ND ug/L 02/04/21 05:39 108-86-10.50 1
Bromochloromethane ND ug/L 02/04/21 05:39 74-97-5 L10.50 1
Bromodichloromethane ND ug/L 02/04/21 05:39 75-27-40.50 1
Bromoform ND ug/L 02/04/21 05:39 75-25-20.50 1
Bromomethane ND ug/L 02/04/21 05:39 74-83-9 L15.0 1
tert-Butyl Alcohol ND ug/L 02/04/21 05:39 75-65-020.0 1
n-Butylbenzene ND ug/L 02/04/21 05:39 104-51-80.50 1
sec-Butylbenzene ND ug/L 02/04/21 05:39 135-98-80.50 1
tert-Butylbenzene ND ug/L 02/04/21 05:39 98-06-60.50 1
tert-Butyl Formate ND ug/L 02/04/21 05:39 762-75-420.0 1
Carbon tetrachloride ND ug/L 02/04/21 05:39 56-23-5 L10.50 1
Chlorobenzene ND ug/L 02/04/21 05:39 108-90-70.50 1
Chloroethane ND ug/L 02/04/21 05:39 75-00-31.0 1
Chloroform ND ug/L 02/04/21 05:39 67-66-30.50 1
Chloromethane ND ug/L 02/04/21 05:39 74-87-31.0 1
2-Chlorotoluene ND ug/L 02/04/21 05:39 95-49-80.50 1
4-Chlorotoluene ND ug/L 02/04/21 05:39 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 02/04/21 05:39 96-12-81.0 1
Dibromochloromethane ND ug/L 02/04/21 05:39 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 02/04/21 05:39 106-93-40.50 1
Dibromomethane ND ug/L 02/04/21 05:39 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 02/04/21 05:39 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 02/04/21 05:39 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 02/04/21 05:39 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 02/04/21 05:39 75-71-80.50 1
1,1-Dichloroethane ND ug/L 02/04/21 05:39 75-34-30.50 1
1,2-Dichloroethane ND ug/L 02/04/21 05:39 107-06-20.50 1
1,1-Dichloroethene ND ug/L 02/04/21 05:39 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 02/04/21 05:39 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 02/04/21 05:39 156-60-50.50 1
1,2-Dichloropropane ND ug/L 02/04/21 05:39 78-87-50.50 1
1,3-Dichloropropane ND ug/L 02/04/21 05:39 142-28-90.50 1
2,2-Dichloropropane ND ug/L 02/04/21 05:39 594-20-70.50 1
1,1-Dichloropropene ND ug/L 02/04/21 05:39 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 02/04/21 05:39 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 02/04/21 05:39 10061-02-60.50 1
Diisopropyl ether ND ug/L 02/04/21 05:39 108-20-30.50 1
Ethanol ND ug/L 02/04/21 05:39 64-17-52001
Ethylbenzene ND ug/L 02/04/21 05:39 100-41-40.50 1
Ethyl-tert-butyl ether ND ug/L 02/04/21 05:39 637-92-310.0 1
Hexachloro-1,3-butadiene ND ug/L 02/04/21 05:39 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 02/04/21 05:39 98-82-80.50 1
Methylene Chloride ND ug/L 02/04/21 05:39 75-09-22.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/05/2021 03:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92519465
Handy House 3 (HH3)
Sample:SW3 Lab ID:92519465006 Collected:01/29/21 14:15 Received:01/29/21 17:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methyl-tert-butyl ether ND ug/L 02/04/21 05:39 1634-04-40.50 1
Naphthalene ND ug/L 02/04/21 05:39 91-20-32.0 1
n-Propylbenzene ND ug/L 02/04/21 05:39 103-65-10.50 1
Styrene ND ug/L 02/04/21 05:39 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 02/04/21 05:39 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 02/04/21 05:39 79-34-50.50 1
Tetrachloroethene ND ug/L 02/04/21 05:39 127-18-40.50 1
Toluene ND ug/L 02/04/21 05:39 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 02/04/21 05:39 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 02/04/21 05:39 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 02/04/21 05:39 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 02/04/21 05:39 79-00-50.50 1
Trichloroethene ND ug/L 02/04/21 05:39 79-01-60.50 1
Trichlorofluoromethane ND ug/L 02/04/21 05:39 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 02/04/21 05:39 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 02/04/21 05:39 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 02/04/21 05:39 108-67-80.50 1
Vinyl chloride ND ug/L 02/04/21 05:39 75-01-41.0 1
m&p-Xylene ND ug/L 02/04/21 05:39 179601-23-11.0 1
o-Xylene ND ug/L 02/04/21 05:39 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)95 %02/04/21 05:39 17060-07-070-130 1
4-Bromofluorobenzene (S)116 %02/04/21 05:39 460-00-470-130 1
Toluene-d8 (S)110 %02/04/21 05:39 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/05/2021 03:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519465
Handy House 3 (HH3)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
597068
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92519465006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3148761
Associated Lab Samples:92519465006
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 02/04/21 00:00
1,1,1-Trichloroethane ug/L ND 0.50 02/04/21 00:00
1,1,2,2-Tetrachloroethane ug/L ND 0.50 02/04/21 00:00
1,1,2-Trichloroethane ug/L ND 0.50 02/04/21 00:00
1,1-Dichloroethane ug/L ND 0.50 02/04/21 00:00
1,1-Dichloroethene ug/L ND 0.50 02/04/21 00:00
1,1-Dichloropropene ug/L ND 0.50 02/04/21 00:00
1,2,3-Trichlorobenzene ug/L ND 2.0 02/04/21 00:00
1,2,3-Trichloropropane ug/L ND 0.50 02/04/21 00:00
1,2,4-Trichlorobenzene ug/L ND 2.0 02/04/21 00:00
1,2,4-Trimethylbenzene ug/L ND 0.50 02/04/21 00:00
1,2-Dibromo-3-chloropropane ug/L ND 1.0 02/04/21 00:00
1,2-Dibromoethane (EDB)ug/L ND 0.50 02/04/21 00:00
1,2-Dichlorobenzene ug/L ND 0.50 02/04/21 00:00
1,2-Dichloroethane ug/L ND 0.50 02/04/21 00:00
1,2-Dichloropropane ug/L ND 0.50 02/04/21 00:00
1,3,5-Trimethylbenzene ug/L ND 0.50 02/04/21 00:00
1,3-Dichlorobenzene ug/L ND 0.50 02/04/21 00:00
1,3-Dichloropropane ug/L ND 0.50 02/04/21 00:00
1,4-Dichlorobenzene ug/L ND 0.50 02/04/21 00:00
2,2-Dichloropropane ug/L ND 0.50 02/04/21 00:00
2-Chlorotoluene ug/L ND 0.50 02/04/21 00:00
4-Chlorotoluene ug/L ND 0.50 02/04/21 00:00
Benzene ug/L ND 0.50 02/04/21 00:00
Bromobenzene ug/L ND 0.50 02/04/21 00:00
Bromochloromethane ug/L ND 0.50 02/04/21 00:00
Bromodichloromethane ug/L ND 0.50 02/04/21 00:00
Bromoform ug/L ND 0.50 02/04/21 00:00
Bromomethane ug/L ND 5.0 02/04/21 00:00
Carbon tetrachloride ug/L ND 0.50 02/04/21 00:00
Chlorobenzene ug/L ND 0.50 02/04/21 00:00
Chloroethane ug/L ND 1.0 02/04/21 00:00
Chloroform ug/L ND 0.50 02/04/21 00:00
Chloromethane ug/L ND 1.0 02/04/21 00:00
cis-1,2-Dichloroethene ug/L ND 0.50 02/04/21 00:00
cis-1,3-Dichloropropene ug/L ND 0.50 02/04/21 00:00
Dibromochloromethane ug/L ND 0.50 02/04/21 00:00
Dibromomethane ug/L ND 0.50 02/04/21 00:00
Dichlorodifluoromethane ug/L ND 0.50 02/04/21 00:00
Diisopropyl ether ug/L ND 0.50 02/04/21 00:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/05/2021 03:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519465
Handy House 3 (HH3)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3148761
Associated Lab Samples:92519465006
Matrix:Water
Analyzed
Ethanol ug/L ND 200 02/04/21 00:00
Ethyl-tert-butyl ether ug/L ND 10.0 02/04/21 00:00
Ethylbenzene ug/L ND 0.50 02/04/21 00:00
Hexachloro-1,3-butadiene ug/L 2.1 2.0 02/04/21 00:00
Isopropylbenzene (Cumene)ug/L ND 0.50 02/04/21 00:00
m&p-Xylene ug/L ND 1.0 02/04/21 00:00
Methyl-tert-butyl ether ug/L ND 0.50 02/04/21 00:00
Methylene Chloride ug/L ND 2.0 02/04/21 00:00
n-Butylbenzene ug/L ND 0.50 02/04/21 00:00
n-Propylbenzene ug/L ND 0.50 02/04/21 00:00
Naphthalene ug/L ND 2.0 02/04/21 00:00
o-Xylene ug/L ND 0.50 02/04/21 00:00
sec-Butylbenzene ug/L ND 0.50 02/04/21 00:00
Styrene ug/L ND 0.50 02/04/21 00:00
tert-Amyl Alcohol ug/L ND 100 02/04/21 00:00
tert-Amylmethyl ether ug/L ND 10.0 02/04/21 00:00
tert-Butyl Alcohol ug/L ND 20.0 02/04/21 00:00
tert-Butyl Formate ug/L ND 20.0 02/04/21 00:00
tert-Butylbenzene ug/L ND 0.50 02/04/21 00:00
Tetrachloroethene ug/L ND 0.50 02/04/21 00:00
Toluene ug/L ND 0.50 02/04/21 00:00
trans-1,2-Dichloroethene ug/L ND 0.50 02/04/21 00:00
trans-1,3-Dichloropropene ug/L ND 0.50 02/04/21 00:00
Trichloroethene ug/L ND 0.50 02/04/21 00:00
Trichlorofluoromethane ug/L ND 1.0 02/04/21 00:00
Vinyl chloride ug/L ND 1.0 02/04/21 00:00
1,2-Dichloroethane-d4 (S)%94 70-130 02/04/21 00:00
4-Bromofluorobenzene (S)%98 70-130 02/04/21 00:00
Toluene-d8 (S)%117 70-130 02/04/21 00:00
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3148762LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 54.250 108 60-140
1,1,1-Trichloroethane ug/L 57.250 114 60-140
1,1,2,2-Tetrachloroethane ug/L 53.650 107 60-140
1,1,2-Trichloroethane ug/L 65.150 130 60-140
1,1-Dichloroethane ug/L 62.350 125 60-140
1,1-Dichloroethene ug/L 57.250 114 60-140
1,1-Dichloropropene ug/L 61.950 124 60-140
1,2,3-Trichlorobenzene ug/L 52.250 104 60-140
1,2,3-Trichloropropane ug/L 53.250 106 60-140
1,2,4-Trichlorobenzene ug/L 52.050 104 60-140
1,2,4-Trimethylbenzene ug/L 52.250 104 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/05/2021 03:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519465
Handy House 3 (HH3)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3148762LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/L 52.950 106 60-140
1,2-Dibromoethane (EDB)ug/L 56.350 113 60-140
1,2-Dichlorobenzene ug/L 50.750 101 60-140
1,2-Dichloroethane ug/L 49.350 99 60-140
1,2-Dichloropropane ug/L 58.150 116 60-140
1,3,5-Trimethylbenzene ug/L 49.450 99 60-140
1,3-Dichlorobenzene ug/L 49.450 99 60-140
1,3-Dichloropropane ug/L 56.350 113 60-140
1,4-Dichlorobenzene ug/L 51.650 103 60-140
2,2-Dichloropropane ug/L 67.850 136 60-140
2-Chlorotoluene ug/L 51.350 103 60-140
4-Chlorotoluene ug/L 50.850 102 60-140
Benzene ug/L 70.7 L15014160-140
Bromobenzene ug/L 53.550 107 60-140
Bromochloromethane ug/L 72.1 L15014460-140
Bromodichloromethane ug/L 56.550 113 60-140
Bromoform ug/L 59.450 119 60-140
Bromomethane ug/L 77.4 L15015560-140
Carbon tetrachloride ug/L 71.1 L15014260-140
Chlorobenzene ug/L 51.750 103 60-140
Chloroethane ug/L 60.050 120 60-140
Chloroform ug/L 62.750 125 60-140
Chloromethane ug/L 48.950 98 60-140
cis-1,2-Dichloroethene ug/L 61.550 123 60-140
cis-1,3-Dichloropropene ug/L 65.550 131 60-140
Dibromochloromethane ug/L 60.050 120 60-140
Dibromomethane ug/L 63.650 127 60-140
Dichlorodifluoromethane ug/L 58.550 117 60-140
Diisopropyl ether ug/L 62.650 125 60-140
Ethanol ug/L 20302000 101 60-140
Ethyl-tert-butyl ether ug/L 133100 133 60-140
Ethylbenzene ug/L 50.750 101 60-140
Hexachloro-1,3-butadiene ug/L 56.950 114 60-140
Isopropylbenzene (Cumene)ug/L 54.850 110 60-140
m&p-Xylene ug/L 96.2100 96 60-140
Methyl-tert-butyl ether ug/L 56.350 113 60-140
Methylene Chloride ug/L 53.150 106 60-140
n-Butylbenzene ug/L 53.350 107 60-140
n-Propylbenzene ug/L 50.750 101 60-140
Naphthalene ug/L 51.850 104 60-140
o-Xylene ug/L 55.150 110 60-140
sec-Butylbenzene ug/L 49.850 100 60-140
Styrene ug/L 53.850 108 60-140
tert-Amyl Alcohol ug/L 11801000 118 60-140
tert-Amylmethyl ether ug/L 128100 128 60-140
tert-Butyl Alcohol ug/L 588500 118 60-140
tert-Butyl Formate ug/L 542400 136 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/05/2021 03:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519465
Handy House 3 (HH3)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3148762LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/L 42.550 85 60-140
Tetrachloroethene ug/L 48.950 98 60-140
Toluene ug/L 54.250 108 60-140
trans-1,2-Dichloroethene ug/L 56.050 112 60-140
trans-1,3-Dichloropropene ug/L 62.050 124 60-140
Trichloroethene ug/L 52.050 104 60-140
Trichlorofluoromethane ug/L 52.950 106 60-140
Vinyl chloride ug/L 46.750 93 60-140
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%108 70-130
Toluene-d8 (S)%107 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3148763MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92519122001
3148764
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 100 60-140110 10 3020ND20.0 22.1
1,1,1-Trichloroethane ug/L 20 107 60-140140 27 3020ND21.4 27.9
1,1,2,2-Tetrachloroethane ug/L 20 97 60-14099 2 3020ND19.5 19.9
1,1,2-Trichloroethane ug/L 20 117 60-140118 1 3020ND23.5 23.6
1,1-Dichloroethane ug/L 20 102 60-140131 24 3020ND20.5 26.1
1,1-Dichloroethene ug/L 20 104 60-140134 25 3020ND20.7 26.7
1,1-Dichloropropene ug/L 20 111 60-140140 23 3020ND22.2 28.0
1,2,3-Trichlorobenzene ug/L 20 109 60-140107 2 3020ND21.9 21.3
1,2,3-Trichloropropane ug/L 20 103 60-140105 2 3020ND20.7 21.0
1,2,4-Trichlorobenzene ug/L 20 108 60-140111 3 3020ND21.6 22.2
1,2,4-Trimethylbenzene ug/L 20 112 60-140110 2 3020ND22.4 22.1
1,2-Dibromo-3-
chloropropane ug/L 20 96 60-140112 15 3020ND19.2 22.4
1,2-Dibromoethane (EDB)ug/L 20 107 60-140107 0 3020ND21.4 21.3
1,2-Dichlorobenzene ug/L 20 89 60-14098 10 3020ND17.8 19.6
1,2-Dichloroethane ug/L 20 92 60-140116 23 3020ND18.4 23.2
1,2-Dichloropropane ug/L 20 120 60-140124 3 3020ND24.0 24.8
1,3,5-Trimethylbenzene ug/L 20 101 60-140103 2 3020ND20.2 20.6
1,3-Dichlorobenzene ug/L 20 97 60-140104 7 3020ND19.4 20.8
1,3-Dichloropropane ug/L 20 109 60-140109 0 3020ND21.9 21.9
1,4-Dichlorobenzene ug/L 20 93 60-140102 9 3020ND18.6 20.3
2,2-Dichloropropane ug/L M12012360-140152 21 3020ND24.6 30.5
2-Chlorotoluene ug/L 20 105 60-140107 2 3020ND20.9 21.3
4-Chlorotoluene ug/L 20 102 60-140113 10 3020ND20.4 22.7
Benzene ug/L M02014760-140119 21 3020ND29.4 23.8
Bromobenzene ug/L 20 108 60-140104 3 3020ND21.5 20.8
Bromochloromethane ug/L M02011760-140150 25 3020ND23.3 30.1
Bromodichloromethane ug/L 20 112 60-140117 4 3020ND22.5 23.3
Bromoform ug/L 20 100 60-140103 3 3020ND20.1 20.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/05/2021 03:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519465
Handy House 3 (HH3)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3148763MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92519122001
3148764
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Bromomethane ug/L M02013260-140167 24 3020ND26.4 33.5
Carbon tetrachloride ug/L M02014860-140146 1 3020ND29.5 29.2
Chlorobenzene ug/L 20 102 60-140106 4 3020ND20.3 21.2
Chloroethane ug/L 20 101 60-140128 23 3020ND20.2 25.5
Chloroform ug/L 20 105 60-140135 25 3020ND20.9 27.0
Chloromethane ug/L 20 89 60-140108 19 3020ND17.9 21.6
cis-1,2-Dichloroethene ug/L 20 102 60-140125 21 3020ND20.3 25.1
cis-1,3-Dichloropropene ug/L 20 118 60-140126 6 3020ND23.7 25.1
Dibromochloromethane ug/L 20 108 60-140108 0 3020ND21.5 21.5
Dibromomethane ug/L 20 129 60-140137 6 3020ND25.7 27.3
Dichlorodifluoromethane ug/L 20 120 60-140137 13 3020ND24.0 27.3
Diisopropyl ether ug/L 20 94 60-140115 20 3020ND18.9 23.1
Ethanol ug/L R18007260-140104 36 30800ND577832
Ethyl-tert-butyl ether ug/L 40 97 60-140126 26 3040ND39.0 50.4
Ethylbenzene ug/L 20 100 60-140105 5 3020ND20.0 21.0
Hexachloro-1,3-butadiene ug/L M12014260-140123 14 3020ND29.1 25.3
Isopropylbenzene
(Cumene)ug/L 20 108 60-140104 3 3020ND21.5 20.8
m&p-Xylene ug/L 40 100 60-140100 0 3040ND40.0 40.0
Methyl-tert-butyl ether ug/L 20 103 60-140132 25 3020ND20.6 26.5
Methylene Chloride ug/L 20 105 60-140139 28 3020ND21.0 27.7
n-Butylbenzene ug/L 20 121 60-140114 6 3020ND24.2 22.8
n-Propylbenzene ug/L 20 108 60-140102 6 3020ND21.5 20.4
Naphthalene ug/L 20 98 60-140103 5 3020ND19.7 20.6
o-Xylene ug/L 20 99 60-140109 10 3020ND19.7 21.8
sec-Butylbenzene ug/L 20 122 60-140109 12 3020ND24.4 21.7
Styrene ug/L 20 97 60-140105 7 3020ND19.5 20.9
tert-Amyl Alcohol ug/L 400 95 60-140111 16 30400ND379443
tert-Amylmethyl ether ug/L 40 135 60-140116 15 3040ND54.0 46.4
tert-Butyl Alcohol ug/L R12009160-140138 42 30200ND181276
tert-Butyl Formate ug/L 160 87 60-14080 8 30160ND139128
tert-Butylbenzene ug/L 20 94 60-14095 1 3020ND18.8 19.0
Tetrachloroethene ug/L 20 99 60-140106 7 3020ND19.7 21.2
Toluene ug/L 20 105 60-140113 8 3020ND20.9 22.6
trans-1,2-Dichloroethene ug/L M12011360-140141 22 3020ND22.6 28.1
trans-1,3-Dichloropropene ug/L 20 107 60-140118 9 3020ND21.4 23.5
Trichloroethene ug/L 20 113 60-140121 7 3020ND22.6 24.2
Trichlorofluoromethane ug/L 20 101 60-140130 24 30201.6 21.7 27.6
Vinyl chloride ug/L 20 87 60-140112 25 3020ND17.5 22.4
1,2-Dichloroethane-d4 (S)%96 70-130104
4-Bromofluorobenzene (S)%107 70-130100
Toluene-d8 (S)%100 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/05/2021 03:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519465
Handy House 3 (HH3)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
597637
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92519465001, 92519465002, 92519465004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3151279
Associated Lab Samples:92519465001, 92519465002, 92519465004
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 02/04/21 11:30
1,1,1-Trichloroethane ug/L ND 0.50 02/04/21 11:30
1,1,2,2-Tetrachloroethane ug/L ND 0.50 02/04/21 11:30
1,1,2-Trichloroethane ug/L ND 0.50 02/04/21 11:30
1,1-Dichloroethane ug/L ND 0.50 02/04/21 11:30
1,1-Dichloroethene ug/L ND 0.50 02/04/21 11:30
1,1-Dichloropropene ug/L ND 0.50 02/04/21 11:30
1,2,3-Trichlorobenzene ug/L ND 2.0 02/04/21 11:30
1,2,3-Trichloropropane ug/L ND 0.50 02/04/21 11:30
1,2,4-Trichlorobenzene ug/L ND 2.0 02/04/21 11:30
1,2,4-Trimethylbenzene ug/L ND 0.50 02/04/21 11:30
1,2-Dibromo-3-chloropropane ug/L ND 1.0 02/04/21 11:30
1,2-Dibromoethane (EDB)ug/L ND 0.50 02/04/21 11:30
1,2-Dichlorobenzene ug/L ND 0.50 02/04/21 11:30
1,2-Dichloroethane ug/L ND 0.50 02/04/21 11:30
1,2-Dichloropropane ug/L ND 0.50 02/04/21 11:30
1,3,5-Trimethylbenzene ug/L ND 0.50 02/04/21 11:30
1,3-Dichlorobenzene ug/L ND 0.50 02/04/21 11:30
1,3-Dichloropropane ug/L ND 0.50 02/04/21 11:30
1,4-Dichlorobenzene ug/L ND 0.50 02/04/21 11:30
2,2-Dichloropropane ug/L ND 0.50 02/04/21 11:30
2-Chlorotoluene ug/L ND 0.50 02/04/21 11:30
4-Chlorotoluene ug/L ND 0.50 02/04/21 11:30
Benzene ug/L ND 0.50 02/04/21 11:30
Bromobenzene ug/L ND 0.50 02/04/21 11:30
Bromochloromethane ug/L ND 0.50 02/04/21 11:30
Bromodichloromethane ug/L ND 0.50 02/04/21 11:30
Bromoform ug/L ND 0.50 02/04/21 11:30
Bromomethane ug/L ND 5.0 02/04/21 11:30
Carbon tetrachloride ug/L ND 0.50 02/04/21 11:30
Chlorobenzene ug/L ND 0.50 02/04/21 11:30
Chloroethane ug/L ND 1.0 02/04/21 11:30
Chloroform ug/L ND 0.50 02/04/21 11:30
Chloromethane ug/L ND 1.0 02/04/21 11:30
cis-1,2-Dichloroethene ug/L ND 0.50 02/04/21 11:30
cis-1,3-Dichloropropene ug/L ND 0.50 02/04/21 11:30
Dibromochloromethane ug/L ND 0.50 02/04/21 11:30
Dibromomethane ug/L ND 0.50 02/04/21 11:30
Dichlorodifluoromethane ug/L ND 0.50 02/04/21 11:30
Diisopropyl ether ug/L ND 0.50 02/04/21 11:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/05/2021 03:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519465
Handy House 3 (HH3)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3151279
Associated Lab Samples:92519465001, 92519465002, 92519465004
Matrix:Water
Analyzed
Ethanol ug/L ND 200 02/04/21 11:30
Ethyl-tert-butyl ether ug/L ND 10.0 02/04/21 11:30
Ethylbenzene ug/L ND 0.50 02/04/21 11:30
Hexachloro-1,3-butadiene ug/L ND 2.0 02/04/21 11:30
Isopropylbenzene (Cumene)ug/L ND 0.50 02/04/21 11:30
m&p-Xylene ug/L ND 1.0 02/04/21 11:30
Methyl-tert-butyl ether ug/L ND 0.50 02/04/21 11:30
Methylene Chloride ug/L ND 2.0 02/04/21 11:30
n-Butylbenzene ug/L ND 0.50 02/04/21 11:30
n-Propylbenzene ug/L ND 0.50 02/04/21 11:30
Naphthalene ug/L ND 2.0 02/04/21 11:30
o-Xylene ug/L ND 0.50 02/04/21 11:30
sec-Butylbenzene ug/L ND 0.50 02/04/21 11:30
Styrene ug/L ND 0.50 02/04/21 11:30
tert-Amyl Alcohol ug/L ND 100 02/04/21 11:30
tert-Amylmethyl ether ug/L ND 10.0 02/04/21 11:30
tert-Butyl Alcohol ug/L ND 20.0 02/04/21 11:30
tert-Butyl Formate ug/L ND 20.0 02/04/21 11:30
tert-Butylbenzene ug/L ND 0.50 02/04/21 11:30
Tetrachloroethene ug/L ND 0.50 02/04/21 11:30
Toluene ug/L ND 0.50 02/04/21 11:30
trans-1,2-Dichloroethene ug/L ND 0.50 02/04/21 11:30
trans-1,3-Dichloropropene ug/L ND 0.50 02/04/21 11:30
Trichloroethene ug/L ND 0.50 02/04/21 11:30
Trichlorofluoromethane ug/L ND 1.0 02/04/21 11:30
Vinyl chloride ug/L ND 1.0 02/04/21 11:30
1,2-Dichloroethane-d4 (S)%79 70-130 02/04/21 11:30
4-Bromofluorobenzene (S)%92 70-130 02/04/21 11:30
Toluene-d8 (S)%98 70-130 02/04/21 11:30
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3151280LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 55.750 111 60-140
1,1,1-Trichloroethane ug/L 46.050 92 60-140
1,1,2,2-Tetrachloroethane ug/L 52.250 104 60-140
1,1,2-Trichloroethane ug/L 52.950 106 60-140
1,1-Dichloroethane ug/L 46.550 93 60-140
1,1-Dichloroethene ug/L 47.450 95 60-140
1,1-Dichloropropene ug/L 47.550 95 60-140
1,2,3-Trichlorobenzene ug/L 52.250 104 60-140
1,2,3-Trichloropropane ug/L 48.550 97 60-140
1,2,4-Trichlorobenzene ug/L 53.150 106 60-140
1,2,4-Trimethylbenzene ug/L 46.750 93 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/05/2021 03:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519465
Handy House 3 (HH3)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3151280LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/L 54.450 109 60-140
1,2-Dibromoethane (EDB)ug/L 54.950 110 60-140
1,2-Dichlorobenzene ug/L 52.150 104 60-140
1,2-Dichloroethane ug/L 42.550 85 60-140
1,2-Dichloropropane ug/L 48.450 97 60-140
1,3,5-Trimethylbenzene ug/L 48.250 96 60-140
1,3-Dichlorobenzene ug/L 53.350 107 60-140
1,3-Dichloropropane ug/L 51.350 103 60-140
1,4-Dichlorobenzene ug/L 52.250 104 60-140
2,2-Dichloropropane ug/L 49.550 99 60-140
2-Chlorotoluene ug/L 48.650 97 60-140
4-Chlorotoluene ug/L 47.850 96 60-140
Benzene ug/L 50.450 101 60-140
Bromobenzene ug/L 49.650 99 60-140
Bromochloromethane ug/L 54.150 108 60-140
Bromodichloromethane ug/L 48.650 97 60-140
Bromoform ug/L 58.250 116 60-140
Bromomethane ug/L 36.150 72 60-140
Carbon tetrachloride ug/L 52.750 105 60-140
Chlorobenzene ug/L 55.650 111 60-140
Chloroethane ug/L 34.950 70 60-140
Chloroform ug/L 45.450 91 60-140
Chloromethane ug/L 39.350 79 60-140
cis-1,2-Dichloroethene ug/L 44.250 88 60-140
cis-1,3-Dichloropropene ug/L 53.550 107 60-140
Dibromochloromethane ug/L 56.750 113 60-140
Dibromomethane ug/L 55.650 111 60-140
Dichlorodifluoromethane ug/L 46.150 92 60-140
Diisopropyl ether ug/L 41.650 83 60-140
Ethanol ug/L 16502000 83 60-140
Ethyl-tert-butyl ether ug/L 88.5100 89 60-140
Ethylbenzene ug/L 51.250 102 60-140
Hexachloro-1,3-butadiene ug/L 54.450 109 60-140
Isopropylbenzene (Cumene)ug/L 53.450 107 60-140
m&p-Xylene ug/L 101100 101 60-140
Methyl-tert-butyl ether ug/L 44.350 89 60-140
Methylene Chloride ug/L 40.150 80 60-140
n-Butylbenzene ug/L 50.350 101 60-140
n-Propylbenzene ug/L 47.750 95 60-140
Naphthalene ug/L 51.450 103 60-140
o-Xylene ug/L 53.150 106 60-140
sec-Butylbenzene ug/L 50.450 101 60-140
Styrene ug/L 56.050 112 60-140
tert-Amyl Alcohol ug/L 8831000 88 60-140
tert-Amylmethyl ether ug/L 95.4100 95 60-140
tert-Butyl Alcohol ug/L 389500 78 60-140
tert-Butyl Formate ug/L 371400 93 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/05/2021 03:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519465
Handy House 3 (HH3)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3151280LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/L 42.150 84 60-140
Tetrachloroethene ug/L 52.250 104 60-140
Toluene ug/L 49.650 99 60-140
trans-1,2-Dichloroethene ug/L 46.950 94 60-140
trans-1,3-Dichloropropene ug/L 51.850 104 60-140
Trichloroethene ug/L 54.950 110 60-140
Trichlorofluoromethane ug/L 39.550 79 60-140
Vinyl chloride ug/L 41.550 83 60-140
1,2-Dichloroethane-d4 (S)%76 70-130
4-Bromofluorobenzene (S)%95 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3151281MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92519453004
3151282
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 250 113 60-140110 3 30250ND284275
1,1,1-Trichloroethane ug/L 250 97 60-14093 4 30250ND243233
1,1,2,2-Tetrachloroethane ug/L 250 104 60-140100 3 30250ND259251
1,1,2-Trichloroethane ug/L 250 104 60-140104 0 30250ND260260
1,1-Dichloroethane ug/L 250 99 60-14094 5 30250ND248236
1,1-Dichloroethene ug/L 250 105 60-140101 3 30250ND262253
1,1-Dichloropropene ug/L 250 101 60-14099 2 30250ND253247
1,2,3-Trichlorobenzene ug/L 250 91 60-14098 8 30250ND228246
1,2,3-Trichloropropane ug/L 250 103 60-140101 2 30250ND258254
1,2,4-Trichlorobenzene ug/L 250 93 60-14097 4 30250ND233242
1,2,4-Trimethylbenzene ug/L 250 75 60-14071 1 30250147016601650
1,2-Dibromo-3-
chloropropane ug/L 250 100 60-140104 4 30250ND249260
1,2-Dibromoethane (EDB)ug/L 250 112 60-140110 1 30250ND280276
1,2-Dichlorobenzene ug/L 250 101 60-14099 1 30250ND251249
1,2-Dichloroethane ug/L 250 86 60-14083 4 30250ND216208
1,2-Dichloropropane ug/L 250 100 60-14099 1 30250ND250248
1,3,5-Trimethylbenzene ug/L 250 95 60-14089 2 30250447684671
1,3-Dichlorobenzene ug/L 250 104 60-140101 3 30250ND259252
1,3-Dichloropropane ug/L 250 104 60-140102 1 30250ND260256
1,4-Dichlorobenzene ug/L 250 101 60-140100 1 30250ND253251
2,2-Dichloropropane ug/L 250 94 60-14091 4 30250ND236227
2-Chlorotoluene ug/L 250 114 60-140104 9 30250ND285260
4-Chlorotoluene ug/L 250 93 60-14092 1 30250ND232231
Benzene ug/L 250 100 60-140103 1 3025084310901100
Bromobenzene ug/L 250 100 60-14097 3 30250ND249242
Bromochloromethane ug/L 250 108 60-140108 1 30250ND271269
Bromodichloromethane ug/L 250 94 60-14097 3 30250ND236242
Bromoform ug/L 250 110 60-140109 1 30250ND274272
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/05/2021 03:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519465
Handy House 3 (HH3)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3151281MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92519453004
3151282
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Bromomethane ug/L M12504760-14055 15 30250ND117136
Carbon tetrachloride ug/L 250 105 60-140107 2 30250ND262267
Chlorobenzene ug/L 250 116 60-140111 4 30250ND289278
Chloroethane ug/L 250 86 60-14084 2 30250ND215211
Chloroform ug/L 250 92 60-14087 5 30250ND230219
Chloromethane ug/L 250 76 60-14077 1 30250ND190191
cis-1,2-Dichloroethene ug/L 250 94 60-14090 5 30250ND239228
cis-1,3-Dichloropropene ug/L 250 101 60-140103 2 30250ND252257
Dibromochloromethane ug/L 250 109 60-140106 3 30250ND273265
Dibromomethane ug/L 250 109 60-140115 5 30250ND273288
Dichlorodifluoromethane ug/L 250 93 60-14089 5 30250ND233222
Diisopropyl ether ug/L 250 87 60-14086 1 30250ND217214
Ethanol ug/L 10000 86 60-14085 1 3010000ND86308520
Ethyl-tert-butyl ether ug/L 500 92 60-14091 1 30500ND458453
Ethylbenzene ug/L 250 106 60-140103 1 30250324589582
Hexachloro-1,3-butadiene ug/L 250 97 60-140102 5 30250ND243254
Isopropylbenzene
(Cumene)ug/L 250 109 60-140108 0 3025032.9 304 304
m&p-Xylene ug/L 500 94 60-14096 0 30500290033703380
Methyl-tert-butyl ether ug/L 250 93 60-14093 0 30250175408408
Methylene Chloride ug/L 250 86 60-14083 4 30250ND216207
n-Butylbenzene ug/L 250 123 60-140121 2 30250ND307302
n-Propylbenzene ug/L 250 125 60-140120 4 30250ND312299
Naphthalene ug/L 250 89 60-14093 2 30250295517529
o-Xylene ug/L 250 114 60-140114 0 30250146017401740
sec-Butylbenzene ug/L 250 100 60-14098 1 30250ND249246
Styrene ug/L 250 114 60-140111 2 30250ND284278
tert-Amyl Alcohol ug/L 5000 93 60-14095 2 305000ND46404730
tert-Amylmethyl ether ug/L 500 95 60-14098 3 30500ND485502
tert-Butyl Alcohol ug/L 2500 92 60-14095 2 302500ND24902540
tert-Butyl Formate ug/L P520006060-14059 2 302000ND12101180
tert-Butylbenzene ug/L 250 88 60-14085 4 30250ND221212
Tetrachloroethene ug/L 250 112 60-140109 3 30250ND281272
Toluene ug/L 250 94 60-140106 1 30250199022302260
trans-1,2-Dichloroethene ug/L 250 100 60-14096 5 30250ND251239
trans-1,3-Dichloropropene ug/L 250 97 60-14097 0 30250ND243243
Trichloroethene ug/L 250 114 60-140115 1 30250ND284287
Trichlorofluoromethane ug/L 250 93 60-14092 2 30250ND233229
Vinyl chloride ug/L 250 88 60-14087 2 30250ND220217
1,2-Dichloroethane-d4 (S)%82 70-13079
4-Bromofluorobenzene (S)%94 70-13094
Toluene-d8 (S)%97 70-13096
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/05/2021 03:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519465
Handy House 3 (HH3)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
597994
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92519465003, 92519465005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3153258
Associated Lab Samples:92519465003, 92519465005
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 02/05/21 12:11
1,1,1-Trichloroethane ug/L ND 0.50 02/05/21 12:11
1,1,2,2-Tetrachloroethane ug/L ND 0.50 02/05/21 12:11
1,1,2-Trichloroethane ug/L ND 0.50 02/05/21 12:11
1,1-Dichloroethane ug/L ND 0.50 02/05/21 12:11
1,1-Dichloroethene ug/L ND 0.50 02/05/21 12:11
1,1-Dichloropropene ug/L ND 0.50 02/05/21 12:11
1,2,3-Trichlorobenzene ug/L ND 2.0 02/05/21 12:11
1,2,3-Trichloropropane ug/L ND 0.50 02/05/21 12:11
1,2,4-Trichlorobenzene ug/L ND 2.0 02/05/21 12:11
1,2,4-Trimethylbenzene ug/L ND 0.50 02/05/21 12:11
1,2-Dibromo-3-chloropropane ug/L ND 1.0 02/05/21 12:11
1,2-Dibromoethane (EDB)ug/L ND 0.50 02/05/21 12:11
1,2-Dichlorobenzene ug/L ND 0.50 02/05/21 12:11
1,2-Dichloroethane ug/L ND 0.50 02/05/21 12:11
1,2-Dichloropropane ug/L ND 0.50 02/05/21 12:11
1,3,5-Trimethylbenzene ug/L ND 0.50 02/05/21 12:11
1,3-Dichlorobenzene ug/L ND 0.50 02/05/21 12:11
1,3-Dichloropropane ug/L ND 0.50 02/05/21 12:11
1,4-Dichlorobenzene ug/L ND 0.50 02/05/21 12:11
2,2-Dichloropropane ug/L ND 0.50 02/05/21 12:11
2-Chlorotoluene ug/L ND 0.50 02/05/21 12:11
4-Chlorotoluene ug/L ND 0.50 02/05/21 12:11
Benzene ug/L ND 0.50 02/05/21 12:11
Bromobenzene ug/L ND 0.50 02/05/21 12:11
Bromochloromethane ug/L ND 0.50 02/05/21 12:11
Bromodichloromethane ug/L ND 0.50 02/05/21 12:11
Bromoform ug/L ND 0.50 02/05/21 12:11
Bromomethane ug/L ND 5.0 02/05/21 12:11
Carbon tetrachloride ug/L ND 0.50 02/05/21 12:11
Chlorobenzene ug/L ND 0.50 02/05/21 12:11
Chloroethane ug/L ND 1.0 02/05/21 12:11
Chloroform ug/L ND 0.50 02/05/21 12:11
Chloromethane ug/L ND 1.0 02/05/21 12:11
cis-1,2-Dichloroethene ug/L ND 0.50 02/05/21 12:11
cis-1,3-Dichloropropene ug/L ND 0.50 02/05/21 12:11
Dibromochloromethane ug/L ND 0.50 02/05/21 12:11
Dibromomethane ug/L ND 0.50 02/05/21 12:11
Dichlorodifluoromethane ug/L ND 0.50 02/05/21 12:11
Diisopropyl ether ug/L ND 0.50 02/05/21 12:11
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/05/2021 03:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519465
Handy House 3 (HH3)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3153258
Associated Lab Samples:92519465003, 92519465005
Matrix:Water
Analyzed
Ethanol ug/L ND 200 02/05/21 12:11
Ethyl-tert-butyl ether ug/L ND 10.0 02/05/21 12:11
Ethylbenzene ug/L ND 0.50 02/05/21 12:11
Hexachloro-1,3-butadiene ug/L ND 2.0 02/05/21 12:11
Isopropylbenzene (Cumene)ug/L ND 0.50 02/05/21 12:11
m&p-Xylene ug/L ND 1.0 02/05/21 12:11
Methyl-tert-butyl ether ug/L ND 0.50 02/05/21 12:11
Methylene Chloride ug/L ND 2.0 02/05/21 12:11
n-Butylbenzene ug/L ND 0.50 02/05/21 12:11
n-Propylbenzene ug/L ND 0.50 02/05/21 12:11
Naphthalene ug/L ND 2.0 02/05/21 12:11
o-Xylene ug/L ND 0.50 02/05/21 12:11
sec-Butylbenzene ug/L ND 0.50 02/05/21 12:11
Styrene ug/L ND 0.50 02/05/21 12:11
tert-Amyl Alcohol ug/L ND 100 02/05/21 12:11
tert-Amylmethyl ether ug/L ND 10.0 02/05/21 12:11
tert-Butyl Alcohol ug/L ND 20.0 02/05/21 12:11
tert-Butyl Formate ug/L ND 20.0 02/05/21 12:11
tert-Butylbenzene ug/L ND 0.50 02/05/21 12:11
Tetrachloroethene ug/L ND 0.50 02/05/21 12:11
Toluene ug/L ND 0.50 02/05/21 12:11
trans-1,2-Dichloroethene ug/L ND 0.50 02/05/21 12:11
trans-1,3-Dichloropropene ug/L ND 0.50 02/05/21 12:11
Trichloroethene ug/L ND 0.50 02/05/21 12:11
Trichlorofluoromethane ug/L ND 1.0 02/05/21 12:11
Vinyl chloride ug/L ND 1.0 02/05/21 12:11
1,2-Dichloroethane-d4 (S)%78 70-130 02/05/21 12:11
4-Bromofluorobenzene (S)%90 70-130 02/05/21 12:11
Toluene-d8 (S)%97 70-130 02/05/21 12:11
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3153259LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 51.950 104 60-140
1,1,1-Trichloroethane ug/L 41.750 83 60-140
1,1,2,2-Tetrachloroethane ug/L 49.450 99 60-140
1,1,2-Trichloroethane ug/L 48.750 97 60-140
1,1-Dichloroethane ug/L 41.650 83 60-140
1,1-Dichloroethene ug/L 43.650 87 60-140
1,1-Dichloropropene ug/L 44.650 89 60-140
1,2,3-Trichlorobenzene ug/L 49.550 99 60-140
1,2,3-Trichloropropane ug/L 44.750 89 60-140
1,2,4-Trichlorobenzene ug/L 50.650 101 60-140
1,2,4-Trimethylbenzene ug/L 42.650 85 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/05/2021 03:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519465
Handy House 3 (HH3)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3153259LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/L 52.050 104 60-140
1,2-Dibromoethane (EDB)ug/L 51.550 103 60-140
1,2-Dichlorobenzene ug/L 48.850 98 60-140
1,2-Dichloroethane ug/L 38.950 78 60-140
1,2-Dichloropropane ug/L 44.750 89 60-140
1,3,5-Trimethylbenzene ug/L 44.850 90 60-140
1,3-Dichlorobenzene ug/L 49.650 99 60-140
1,3-Dichloropropane ug/L 47.550 95 60-140
1,4-Dichlorobenzene ug/L 49.050 98 60-140
2,2-Dichloropropane ug/L 45.850 92 60-140
2-Chlorotoluene ug/L 44.050 88 60-140
4-Chlorotoluene ug/L 44.250 88 60-140
Benzene ug/L 46.050 92 60-140
Bromobenzene ug/L 46.750 93 60-140
Bromochloromethane ug/L 49.150 98 60-140
Bromodichloromethane ug/L 43.850 88 60-140
Bromoform ug/L 55.250 110 60-140
Bromomethane ug/L 33.350 67 60-140
Carbon tetrachloride ug/L 47.850 96 60-140
Chlorobenzene ug/L 52.550 105 60-140
Chloroethane ug/L 30.550 61 60-140
Chloroform ug/L 40.450 81 60-140
Chloromethane ug/L 34.850 70 60-140
cis-1,2-Dichloroethene ug/L 40.750 81 60-140
cis-1,3-Dichloropropene ug/L 48.750 97 60-140
Dibromochloromethane ug/L 51.650 103 60-140
Dibromomethane ug/L 52.150 104 60-140
Dichlorodifluoromethane ug/L 42.750 85 60-140
Diisopropyl ether ug/L 39.150 78 60-140
Ethanol ug/L 16402000 82 60-140
Ethyl-tert-butyl ether ug/L 83.1100 83 60-140
Ethylbenzene ug/L 47.550 95 60-140
Hexachloro-1,3-butadiene ug/L 50.350 101 60-140
Isopropylbenzene (Cumene)ug/L 49.850 100 60-140
m&p-Xylene ug/L 91.9100 92 60-140
Methyl-tert-butyl ether ug/L 42.350 85 60-140
Methylene Chloride ug/L 37.250 74 60-140
n-Butylbenzene ug/L 46.350 93 60-140
n-Propylbenzene ug/L 43.450 87 60-140
Naphthalene ug/L 49.850 100 60-140
o-Xylene ug/L 50.050 100 60-140
sec-Butylbenzene ug/L 46.050 92 60-140
Styrene ug/L 51.950 104 60-140
tert-Amyl Alcohol ug/L 8721000 87 60-140
tert-Amylmethyl ether ug/L 90.3100 90 60-140
tert-Butyl Alcohol ug/L 396500 79 60-140
tert-Butyl Formate ug/L 355400 89 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/05/2021 03:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519465
Handy House 3 (HH3)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3153259LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/L 39.250 78 60-140
Tetrachloroethene ug/L 49.450 99 60-140
Toluene ug/L 46.750 93 60-140
trans-1,2-Dichloroethene ug/L 43.050 86 60-140
trans-1,3-Dichloropropene ug/L 47.250 94 60-140
Trichloroethene ug/L 51.950 104 60-140
Trichlorofluoromethane ug/L 36.450 73 60-140
Vinyl chloride ug/L 37.650 75 60-140
1,2-Dichloroethane-d4 (S)%75 70-130
4-Bromofluorobenzene (S)%95 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3153260MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92520197001
3153261
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 10000 116 60-140111 4 3010000ND1160011100
1,1,1-Trichloroethane ug/L 10000 99 60-14092 8 3010000ND98809160
1,1,2,2-Tetrachloroethane ug/L 10000 104 60-140101 3 3010000ND1040010100
1,1,2-Trichloroethane ug/L 10000 107 60-140104 3 3010000ND1070010400
1,1-Dichloroethane ug/L 10000 93 60-14088 5 3010000ND92908830
1,1-Dichloroethene ug/L 10000 101 60-14099 2 3010000ND101009940
1,1-Dichloropropene ug/L 10000 101 60-14096 5 3010000ND101009620
1,2,3-Trichlorobenzene ug/L 10000 100 60-140107 6 3010000ND1000010700
1,2,3-Trichloropropane ug/L 10000 96 60-14097 1 3010000ND96109750
1,2,4-Trichlorobenzene ug/L 10000 105 60-140106 1 3010000ND1050010600
1,2,4-Trimethylbenzene ug/L 10000 99 60-14091 6 301000041301400013200
1,2-Dibromo-3-
chloropropane ug/L 10000 105 60-140104 1 3010000ND1050010400
1,2-Dibromoethane (EDB)ug/L 10000 112 60-140104 7 3010000ND1120010400
1,2-Dichlorobenzene ug/L 10000 108 60-140103 4 3010000ND1080010300
1,2-Dichloroethane ug/L 10000 85 60-14083 3 3010000ND84908280
1,2-Dichloropropane ug/L 10000 102 60-14096 7 3010000ND102009560
1,3,5-Trimethylbenzene ug/L 10000 117 60-140107 9 3010000ND1170010700
1,3-Dichlorobenzene ug/L 10000 111 60-140107 4 3010000ND1110010700
1,3-Dichloropropane ug/L 10000 105 60-14099 6 3010000ND105009880
1,4-Dichlorobenzene ug/L 10000 109 60-140103 6 3010000ND1090010300
2,2-Dichloropropane ug/L 10000 98 60-14092 6 3010000ND98409250
2-Chlorotoluene ug/L 10000 102 60-14099 3 3010000ND102009920
4-Chlorotoluene ug/L 10000 101 60-14094 7 3010000ND101009440
Benzene ug/L 10000 109 60-140100 8 3010000ND1110010300
Bromobenzene ug/L 10000 106 60-140101 5 3010000ND1060010100
Bromochloromethane ug/L 10000 108 60-140102 6 3010000ND1080010200
Bromodichloromethane ug/L 10000 98 60-14092 7 3010000ND98109160
Bromoform ug/L 10000 112 60-140111 1 3010000ND1120011100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/05/2021 03:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519465
Handy House 3 (HH3)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3153260MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92520197001
3153261
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Bromomethane ug/L M1100004960-14062 22 3010000ND49306170
Carbon tetrachloride ug/L 10000 114 60-140104 9 3010000ND1140010400
Chlorobenzene ug/L 10000 118 60-140112 5 3010000ND1180011200
Chloroethane ug/L 10000 93 60-14082 14 3010000ND93408160
Chloroform ug/L 10000 91 60-14090 1 3010000ND91509020
Chloromethane ug/L 10000 69 60-14070 0 3010000ND69306960
cis-1,2-Dichloroethene ug/L 10000 90 60-14086 5 3010000ND90108560
cis-1,3-Dichloropropene ug/L 10000 107 60-140103 3 3010000ND1070010300
Dibromochloromethane ug/L 10000 111 60-140104 7 3010000ND1110010400
Dibromomethane ug/L 10000 114 60-140111 3 3010000ND1140011100
Dichlorodifluoromethane ug/L 10000 88 60-14083 6 3010000ND88008300
Diisopropyl ether ug/L 10000 84 60-14081 3 3010000ND83808120
Ethanol ug/L 400000 86 60-14083 4 30400000ND345000332000
Ethyl-tert-butyl ether ug/L 20000 89 60-14086 4 3020000ND1780017100
Ethylbenzene ug/L 10000 111 60-140104 5 301000039801510014400
Hexachloro-1,3-butadiene ug/L 10000 115 60-140109 6 3010000ND1150010900
Isopropylbenzene
(Cumene)ug/L 10000 114 60-140109 4 3010000ND1140010900
m&p-Xylene ug/L 20000 109 60-140100 6 3020000119003380032000
Methyl-tert-butyl ether ug/L 10000 89 60-14087 2 3010000ND88508680
Methylene Chloride ug/L 10000 81 60-14077 5 3010000ND81007750
n-Butylbenzene ug/L 10000 104 60-140101 2 3010000ND1040010100
n-Propylbenzene ug/L 10000 105 60-14099 7 3010000ND105009880
Naphthalene ug/L 10000 84 60-14089 5 301000027301110011700
o-Xylene ug/L 10000 112 60-140106 4 301000057101690016400
sec-Butylbenzene ug/L 10000 106 60-140101 5 3010000ND1060010100
Styrene ug/L 10000 114 60-140110 3 3010000ND1140011000
tert-Amyl Alcohol ug/L 200000 88 60-14087 1 30200000ND175000174000
tert-Amylmethyl ether ug/L 20000 97 60-14094 4 3020000ND1950018800
tert-Butyl Alcohol ug/L 100000 75 60-14078 4 30100000ND7520078100
tert-Butyl Formate ug/L 80000 93 60-14089 5 3080000ND7440071100
tert-Butylbenzene ug/L 10000 92 60-14086 7 3010000ND91808570
Tetrachloroethene ug/L 10000 114 60-140109 5 3010000ND1140010900
Toluene ug/L E,M11000015360-140112 4 301000093800109000105000
trans-1,2-Dichloroethene ug/L 10000 97 60-14090 7 3010000ND96609050
trans-1,3-Dichloropropene ug/L 10000 102 60-14097 5 3010000ND102009680
Trichloroethene ug/L 10000 122 60-140113 7 3010000ND1220011300
Trichlorofluoromethane ug/L 10000 96 60-14090 7 3010000ND96509030
Vinyl chloride ug/L 10000 85 60-14080 6 3010000ND85108000
1,2-Dichloroethane-d4 (S)%76 70-13078
4-Bromofluorobenzene (S)%93 70-13094
Toluene-d8 (S)%100 70-13097
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/05/2021 03:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 35
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92519465
Handy House 3 (HH3)
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Analyte concentration exceeded the calibration range. The reported result is estimated.E
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The EPA or method required sample preservation degrades this compound, therefore acceptable recoveries may not be
achieved in sample matrix spikes.P5
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/05/2021 03:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 35
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92519465
Handy House 3 (HH3)
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92519465001 597637MW1SM 6200B
92519465002 597637MW2SM 6200B
92519465003 597994MW3SM 6200B
92519465004 597637MW8SM 6200B
92519465005 597994MW10SM 6200B
92519465006 597068SW3SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/05/2021 03:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 35
Page 35 of 35