WI-7755_32840_CA_MRP_20200430

GROUNDWATER MONITORING REPORT

HANDY HOUSE 3
6742 HWY 70, NEWPORT, NC 28570
GROUNDWATER INCIDENT #: 32840; FACILITY ID #: 0-011113

LATITUDE: N 34.77793o; LONGITUDE: W 76.871506o (From GPS)

APRIL 30, 2020

UST OWNER:
J.M. Davis Industries, Inc. 201 Arendell Street, Morehead City, NC 28557 [phone]

PROPERTY OWNER & OCCUPANT:
Property Owner & Occupant:Dominick Spadaro, 301 Roberts Road, Newport, NC 28570 [phone]

CONSULTANT:
Henry Nemargut Engineering Services, 2211 Chestnut Street, Wilmington, NC 28405
Phone Number: [phone]
RELEASE INFORMATION: Date Discovered: 3/7/13 Estimated Quantity of Release: Unknown Cause of Release: Gasoline USTs; Source of Release: Gasoline UST System Size and Contents: (2) 6,000 Gallon Gasoline USTs; (1) 4,000 Gallon Gasoline UST

The Monitoring Report for this site has been prepared by Henry Nemargut Engineering
Services. All engineering work performed on this project was conducted under my direct
supervision:

Henry Nemargut, P.E.
Henry Nemargut Engineering Services
North Carolina License #17669

April 30, 2020

Jim Davis
J.M. Davis Industries, Inc.
812 Arendell Street
Morehead City, NC 28557

Reference: Groundwater Monitoring Report
Handy House 3
6724 Hwy 70
Newport, Carteret County, North Carolina 28570
Incident #32840; Facility ID #0-011113

Dear Mr. Davis:

In accordance with an approved Task Authorization Form (TAF) from the North Carolina
Department of Environmental Quality (NCDEQ), contained herein is a Groundwater Monitoring
Report for the release which occurred at the above referenced facility. The field activities for
this project consisted of the sampling of existing monitor wells with the laboratory analyses of
the collected groundwater samples. All activities were conducted in accordance with the
NCDEQ guidelines and the requirements of 15A NCAC 2L .0115.

Mr. Davis, if you have any questions concerning this report, please contact our office.

Sincerely,

Henry Nemargut, P.E.
Henry Nemargut Engineering Services

B. EXECUTIVE SUMMARY
1. Free Product: Free product has not been observed at the site.
2. Contaminant Mass: Based on the soil & groundwater data from the original CSA with subsequent placement of final wells at the site in August 2014, the estimated baseline total contaminant mass at this site during initial investigations is 194 lbs of total petroleum mass, which includes an estimated 32.5 lbs of petroleum dissolved into the aqueous phase at this site. The latest groundwater monitoring event conducted on March 18, 2020 indicates that an estimated 2.05 lbs of petroleum contaminant mass remains dissolved in groundwater at the site based on analytical data. Current data indicates a 93.7% contaminant decrease in dissolved aqueous phase petroleum mass has occurred at the site compared to the original CSA total dissolved mass, due to natural processes and nutrient sock installation.

3. Maximum Concentrations of Dissolved Groundwater Contaminants:

Current Groundwater Maximums:
Contaminant Result Well ID 2L Standard Toluene 7.9 ug/L (MW-3) 600 ug/L Ethyl Benzene 338 ug/L (MW-3) 600 ug/L Xylenes 734 ug/L (MW-3) 500 ug/L 1,2,4-Trimethylbenzene 972 ug/L (MW-3) 400 ug/L 1,3,5-Trimethylbenzene 86 ug/L (MW-1) 400 ug/L Naphthalene 332 ug/L (MW-3) 6 ug/L Isopropylbenzene 55.7 ug/L (MW-3) 70 ug/L Total 6200B 2,440 ug/L (MW-3) NSE No other compounds exceeded 2L Standards for 6200B compounds during the latest groundwater monitoring event for this site. 4. Extent of Dissolved Groundwater Contamination: The plume of dissolved groundwater contamination appears to be reducing significantly in downgradient areas of this site with the addition of nutrient socks, and as a result of abatement soil excavation activities, based on the historical data for the site. Historically, the plume appears to be originating from the gasoline UST basin. Data from the 2014 baseline sampling event indicated that the dissolved plume above 2L Standards had migrated 220’ from the UST source area. Currently, 2L Violations are present at relatively low levels compared to the 2L & GCL Standards, with a plume reduced to 50’ from the source in the downgradient direction. 5. Maximum Soil Contaminant Concentrations (From 2013-2014 Soil Assessments): Contaminant Result Sample ID Lowest MSCC MTBE 0.631 mg/kg (SE) 0.091 mg/kg Xylenes (total) 34.1 mg/kg (DPE) 4.6 mg/kg Naphthalene 50.1 mg/kg (DPE) 0.16 mg/kg Isopropylbenzene 15.1 mg/kg (DPE) 2.0 mg/kg 1,2,4-Trimethylbenzene 172 mg/kg (DPE) 8.5 mg/kg 1,3,5-Trimethylbenzene 71 mg/kg (DPE) 8.4 mg/kg
C5-C8 Aliphatics 112 mg/kg (DPE) 68 mg/kg C9-C18 Aliphatics 2,420 mg/kg (DPE) 540 mg/kg C9-C22 Aromatics 1,030 mg/kg (DPE) 31 mg/kg Soil assessment at this site indicates that an estimated 20 tons of contaminated soil above the seasonal water table and in the smear zone remain in the area of the dispenser island, at the base of the canopy footer. Based on the local public water supply well, Lowest MSCC standards may apply for this site. Approximately 1806 tons of petroleum contaminated soils were excavated and disposed of from around the USTs and dispenser islands during IAA excavation activities. 6. Remedial Action Plan:
No CAP has been developed for this site. The NCDEQ Wilmington Regional Office has approved the experimental use of nutrient and absorbent socks at this site to evaluate their effectiveness on contaminant reduction at this site. Nutrient socks have been installed at this site on the following dates: March 18, 2017 (nutrient socks/MW-2,3,8,9,10) October 16, 2017 (nutrient/oxygenating socks/ MW-2,3,8,9,10) May 16, 2018 (nutrient/oxygenating socks/ MW-2,3,8,9,10) March 28, 2019 (nutrient socks/MW-2,3,8,9,10) March 18, 2020 (nutrient socks/MW-2,3,8,9,10) The available data suggests that these nutrient socks have been effective in reducing 6200B concentrations at this site, particularly in downgradient wells. The plume appears to be significantly reduced in size and concentrations since the socks have been introduced into the impacted wells at this site. Current plans for remedial action at this site include replacement of nutrient socks on a semi-annual basis to collect data for continued evaluation of the effectiveness of the use of nutrient socks on the reduction of petroleum constituents at this site.

7. Impacted Receptors:
3 private potable wells serve as a water supply well for residents located on Roberts Road. A public water supply well located downgradient of the release source at 6760 Hwy 70 has routinely failed to contain petroleum related compounds. Since this is an active water supply well, the site will retain its High Risk classification as long as this well is used to provide water supply to the tenants of this small strip shopping center. A drainage ditch on the east side of the NCDOT right-of-way may now or formerly intercepted the dissolved plume during high water table periods. This ditch has never been tested for impact from the UST release originating at the Handy House 3 site.
TABLE OF CONTENTS

Section Page 1.0 Site History and Characterization 1.1 Introduction .................................................................... 1 1.2 Scope of Services ........................................................... 2 1.3 Receptor Survey Update ................................................ 2 2.0 Presentation of Current Site Assessment Information / Comparison to Historical Assessment Information 2.1 Historical Soil Assessment Information ........................ 2 2.2 Groundwater Flow Direction and Gradient ................... 3 2.3 Monitor Well Sampling and Analyses ........................... 3 2.4 Supply Well Sampling and Analyses ............................. 3 2.5 Regional / Site Geology and Hydrogeology .................. 4 2.6 Plume Development ....................................................... 5 3.0 Monitored Natural Attenuation 3.1 Natural Source Zone Depletion Status ........................... 5 4.0 Conclusions 4.1 General Summary .......................................................... 6 4.2 Recommendations .......................................................... 6 4.3 Limitations ..................................................................... 6 5.0 Statements and Certification 5.1 Statements ...................................................................... 7 5.2 Certification ................................................................... 7

LIST OF FIGURES Figure 1: Project Location Figure 2: Receptor Map Figure 3: Soil Concentrations Map Figure 4: Site Layout & UST Locations Figure 5: Monitor Well Locations Map Figure 6: Shallow Well Potentiometric Surface Map (3/18/20) Figure 7: Naphthalene Isoconcentration Map Figure 8: 1,2,4-Trimethylbenzene Isoconcentration Map Figure 9: Total 6200B Compounds Concentration Map – 3/18/20 Figure 10: Total 6200B Compounds Concentration Map – Baseline-3/11/15

LIST OF TABLES Table 1: Site History Table 2: Summary of Soil Analytical Data
Table 3: Monitoring Well Information and Groundwater Elevations
Table 4: Summary of Groundwater Analytical Results-3/18/2020
Table 5: Water Supply Well Information
Table 6: Mass Calculation Table
Table 7: Cumulative Groundwater Summary
Table 8: Baseline Groundwater Analytical Data – 8/28/2014

APPENDICES Appendix A: Laboratory Analytical Results
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GROUNDWATER MONITORING REPORT Handy House 3 6724 Hwy 70, Newport, North Carolina 28570

1.0 Site History and Characterization
1.1 Introduction

J.M. Davis Industries, Inc. owned USTs which were operated at the Handy House 3
facility located at 6724 Hwy 70 in Newport, North Carolina. Figure 1 illustrates the
location of this facility on the Newport Quadrangle U.S.G.S. Topo Map. This facility
contains one permanent structure which was used as a convenience store. The site
formerly contained (2) 6,000 gallon gasoline and (1) 4,000 gallon gasoline UST which
were last used at this facility in June, 2012. The locations of the USTs and the site layout
are illustrated on Figure 4. A release from the UST system was suspected on 3/6/13 and
reported to NCDENR personnel based on elevated PID readings observed in soil samples
collected from soils removed from around the USTs. This release was confirmed upon
receipt of analytical results from soil samples collected during the tank closure activities
conducted on 3/6-13/2013. In response to this release, J.M. Davis Industries, Inc. took
immediate abatement measures at the site including excavation and proper disposal of
accessible contaminated soils in the UST and dispenser island areas resulting in
remediation of 1,806 tons of petroleum contaminated soils. Groundwater monitoring
activities are ongoing at the site on a semi-annual basis. Table 1 contains the UST
history for this site.
The site and adjacent properties are used for commercial and residential purposes.
Municipal water supply from the Town of Newport serves the site and is available to all
properties within 1,500’; however, (4) active water supply wells are in use within 1,000’
of the release source originating at this facility. The NCDEQ Wilmington Regional
should evaluate the information contained in this report to determine whether
development of a CAP is warranted.
1.2 Scope of Services

This Groundwater Monitoring Report contains documentation concerning the following
activities which have been conducted at this facility:

o Sampling of twelve monitor wells conducted by Henry Nemargut Engineering on March 18, 2020.

o Installation of nutrient socks.

o Laboratory analyses of groundwater samples conducted by Pace Analytical, Inc. of Huntersville, NC.
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2.0 Presentation of Current Site Assessment Information / Comparison to Historical Assessment Information 2.1 Historical Soil Assessment Information
Soil samples were collected from the sidewalls of the remedial excavation during 2013
IAA activities. (4) soil borings (B1 through B4) advanced at the site during CSA soil
assessment activities to depths of 4’ below grade in the approximate locations depicted
on Figure 3 to assess the extent of non-excavatable soils beneath the canopy structure at
this site. An estimated 60 square foot area was estimated during assessment to contain
contaminated soil in the area of the UST basin. With an assumed thickness of 6’, that
would represent approximately 20 tons of contaminated soils remain in place at the
project site beneath the canopy structure. Based on the existence of local potable wells
within 1,000’, Lowest MSCC standards should apply for soil cleanup standards for this
site.
Figure 3 illustrates the locations of the risk-based soil samples collected at the subject site
and the estimated extent of soil contamination above lowest MSCCs, and Table 2
summarizes the laboratory results for the “Risk-Based” soil samples from 6724 Hwy 70
in Newport, NC. Laboratory analytical reports and the chain of custody records for the
soil samples collected at the project site are contained in the IAA and CSA reports
submitted for this site.

Based on the limited time between the original soil sampling and the most recent
groundwater sampling event, it is estimated that natural processes have not significantly
reduced soil contaminant levels beyond the original estimate. Additional soil assessment
activities would be required to formulate new soil mass contaminant calculation for the
site. 2.2 Ground Water Flow Direction and Gradient

In order to estimate the groundwater flow direction in the vicinity of the petroleum
release, elevations of the monitor well casings were measured using surveying
equipment. During the March 18, 2020 sampling event, static water levels were obtained
from the monitor wells (see Table 3) and the data was used to compute a potentiometric
surface map. Figure 6 illustrates the current potentiometric surface map as calculated
based on the measurements obtained on March 18, 2020.
Groundwater data and monitoring well information were also used to estimate the
hydraulic gradient at the project site. Using the horizontal distance between the monitor
wells and the static water levels, the groundwater was calculated to flow toward the
north/northwest with a hydraulic gradient of approximately 0.0215 ft/ft.

2.3 Monitor Well Sampling and Analyses

On March 18, 2020, (12) monitor wells were sampled for analyses utilizing Standard
Method 6200B + VPH. Before collecting the samples, the monitor wells were purged by
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removing a minimum of three well volumes to ensure that the samples were
representative of the actual groundwater conditions. The wells were developed using
disposable plastic bailers suspended with unused nylon string.

All samples were placed in laboratory supplied glassware, labeled with sample location,
analysis to be performed, time, date and sampler's name. The sample jars were then
immediately placed in a cooler, chilled with ice to approximately 4oC in preparation of
transportation to an analytical laboratory utilizing EPA approved chain-of-custody
procedures.

Laboratory analytical results indicate the presence of (3) 6200B compounds groups above
the current listed 2L Standards in monitor wells MW-3 and MW-10 only. 1,2,4-
Trimethylbenzene was detected at a maximum concentration of 972 ug/l in MW-3, above
its 2L standard of 400 ug/l but below its GCL of 28,500 ug/l. No GCL violations were
noted at the site. Naphthalene was detected at a maximum concentration of 332 ug/l in
monitoring well MW-3. Total 6200B compounds were noted in MW-3 at a maximum
concentration of 2,440 ug/l.

Laboratory analytical results indicate the presence of VPH compounds groups above the
current listed 2L Standards in monitor wells MW-1, MW-2, MW-3 and MW-10. Total
VPH compounds were noted in MW-3 at a concentration of 8,050 ug/l. The fractions of
6200B/VPH compounds noted at: MW-10 (10.5%); MW-3 (30.3%); MW-2 (0.8%);
MW-1 (11.8%). Noting these ratios, mass calculations for the site are based on 6200B
values representing 10% of actual contaminant mass at this site. Table 4 summarizes the
laboratory analytical results, and Appendix A contains a copy of the laboratory analytical
report and chain of custody records. Figure 7 contains a naphthalene iso-concentration
map and Figure 8 contains a 1,2,4-Trimethylbenzene iso-concentration map. Figures 9
and Figure 10 contain current and baseline total 6200B isoconcentration maps which
were prepared for total dissolved constituent groundwater contaminant mass calculations.

2.4 Supply Well Sampling and Analyses

On March 18, 2020, the supply well at the Elaine Honeycutt property (SW-3) was
sampled for analyses utilizing Standard Method 6200B. Before sampling, the supply
well was purged by pumping from the wells for approximately 5 minutes to ensure that
the samples were representative of the actual groundwater conditions. After pumping,
the flowrate was reduced for collection of samples. The sample from SW-3 was obtained
from the spigot closest to the supply well.

All samples were placed in laboratory supplied glassware, labeled with sample location,
analysis to be performed, time, date and sampler's name. The sample jars were then
immediately placed in a cooler, chilled with ice to approximately 4oC in preparation of
transportation to an analytical laboratory utilizing EPA approved chain-of-custody
procedures.

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Laboratory analytical results failed to indicate the presence of any 6200B compounds
above laboratory detection limits in the Honeycutt supply well sample. Appendix A
contains a copy of the laboratory analytical report and chain of custody records.

2.5 Regional / Site Geology and Hydrogeology

The site is situated in the Coastal Plain Physiographic Province. According to the
Geological Map of North Carolina local geology of the region consists of surficial
deposits, undivided, including sand, clay, gravel and peat deposited in marine, fluvial,
eolian, and lacustrine environments. Bedrock was not encountered to a depth of 68 feet
below surface which was the maximum depth explored during the subsurface
investigation.
Three single well rising head tests or "slug tests" were performed on MW-3, MW-7 and
MW-9 to determine the saturated hydraulic conductivity of the water table aquifer. The
method of Bouwer and Rice (Bouwer and Rice, 1989, 1976) was chosen to reduce the
slug test data. A computer program developed by the Geraghty & Miller Modeling
Group named AQTESOLV was used to estimate the aquifer parameters. Results of the
slug tests indicated a hydraulic conductivity of 6.501 x10-3 feet/minute for MW-3, 2.221
x 10-3 feet/minute for MW-7, and 4.08 x 10-3 feet/minute for MW-9. The results from
MW-3, MW-7 and MW-9 are consistent with published values for silty sand and fine
clean sand (Freeze & Cherry, 1979).

2.6 Plume Development

The monitoring well network at this release site was installed between June, 2013 and
August, 2014. In prior sampling events conducted at the site, contaminants have been
reported above 2L Standards in on-site and off-site monitoring wells. The contaminant
concentrations in source area wells MW-1 and MW-2, where soils were excavated, have
continually decreased throughout the monitoring history for this site. Down-gradient
wells at the site generally showed a decrease to a historically low concentrations during
the October 16, 2017 sampling event. This decrease may have in part been related to pit
dewatering conducted by the Town of Newport in the DOT right-of-way during
installation of underground sewer lines during 1st quarter 2017. Several wells were lost
or destroyed on adjacent properties and in the NC-DOT right-of-way by the Town of
Newport in 2017. The addition of nutrient socks at the site appears to be reducing
contaminant concentrations based on historical analytical trends.

The latest groundwater monitoring event conducted on March 18, 2020 indicates that an
estimated 2.04 lbs of petroleum contaminant mass remains dissolved in groundwater at
the site based on analytical data. Current data indicates a 93.7% contaminant decrease in
dissolved aqueous phase petroleum mass has occurred at the site compared to the August
2014 baseline total dissolved mass, due to natural processes and nutrient sock installation.
Both the size and concentration of the dissolved constituent plume at this site has
decreased significantly over the history of this site. Historical groundwater data are
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summarized on Table 7, which includes groundwater elevation data. Table 6 contains
contaminant mass calculations.

3.0 Monitored Natural Attenuation 3.1 Natural Source Zone Depletion Status
Historically, 2L violations for 10 compounds/compound groups have been observed in
groundwater monitoring activities conducted since March 11, 2015. The groundwater
contaminant plume in August, 2014 appeared to have migrated to the north/northwest to a
distance of 220’ from the UST source area; however, based on the results of the March
18, 2020 groundwater sampling event, it appears that the groundwater contaminant plume
has been reduced to a down-gradient distance of 50’. Targeted petroleum concentrations
detected in the groundwater samples collected from within the plume over that time
period appear to be significantly reduced based on available data.

Based on current analytical data, it appears that natural processes are remediating the
dissolved contaminant plume at this site originating from the UST source area. Estimates
based on the analytical data available for this site indicate that dissolved contaminant
mass has decreased by 93.7% over the monitoring history of this site.
4.0 Conclusions

4.1 General Summary
A Groundwater Monitoring event at Handy House 3 located at 6724 Hwy 70 in Wilmington, NC has been completed. From a review of all information gathered during this monitoring project, Henry Nemargut Engineering makes the following conclusions:

o (3) 6200B compounds were detected above the current listed 2L Standards in the monitor wells MW-3 and MW-10 at this site during sampling on March 18, 2020. 1,2,4-Trimethylbenzene was detected at a maximum concentration of 972 ug/l in MW-3, above its 2L standard of 400 ug/l but below its GCL of 28,500 ug/l. No GCL violations were noted at the site. Naphthalene was detected at a maximum concentration of 332 ug/l in monitoring well MW-3. Total 6200B compounds were noted in MW-3 at a maximum concentration of 2,440 ug/l.

o One nearby in-use water supply well (Honeycutt property - SW-3) was sampled on March 18, 2020. Laboratory analytical results failed to indicate the presence of any 6200B compounds above laboratory detection limits in the Honeycutt supply well sample.

o Based on current analytical data, it appears that natural processes are remediating the dissolved contaminant plume at this site originating from the UST source area. The latest groundwater monitoring event conducted on March 18, 2020 indicates that an estimated 2.05 lbs of petroleum contaminant mass remains dissolved in groundwater at the site based on current analytical data. Current data indicates a 93.7% contaminant decrease in dissolved aqueous phase petroleum mass has occurred at the site compared to the August, 2014 baseline total dissolved mass, due to natural processes and nutrient sock installation.
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4.2 Recommendations

Based on information obtained during this sampling event, Henry Nemargut Engineering Services makes the following recommendations for this site:
o Experimental use of nutrient socks should be continued at this site to reduce
groundwater contaminant levels.

o The NCDEQ should determine whether additional soil assessment activities
should be conducted at the site to provide a more accurate measurement of current
contaminant mass in the vadose and smear zones. A copy of this monitoring report has been forwarded to the following address:

Liz Price
NCDEQ-WiRO UST Section
127 Cardinal Drive Extension
Wilmington, NC 28405 4.3 Limitations

This report has been prepared for the exclusive use of J.M. Davis Industries, Inc. for the
specific application to the referenced site located in Carteret County, North Carolina.
The assessment was conducted based on the scope of work and level of effort desired by
the client. Our findings have been developed in accordance with generally accepted
standards in the practice of Groundwater Monitoring Reports in the State of North
Carolina, available information, and our professional judgment. No other warranty is
expressed or implied.
The data presented in this report are indicative of conditions that existed at the precise locations sampled and at the time the samples were collected. Additionally, the data obtained from the samples would be interpreted as meaningful with respect to the parameters indicated in the laboratory reports. No additional information can be logically inferred from this data.
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5.0 Statements and Certification 5.1 Statements The monitoring report was due on April 30, 2020. Will this report be submitted after the established due date? No Was any required information from the template missing from this report? No If applicable, will any of the proposed attenuation milestones under the schedule approved in the Corrective Action Plan not be met? Not Applicable, no CAP has been prepared for this site. Does any known or suspected source zone soil contamination or free product remain outside of the assessed area that could be inhibiting natural attenuation? No Has there been an unexpected increase in contaminant mass sufficient to suggest a potential new release from a separate onsite or offsite source? No 5.2 Certification I, Henry Nemargut, a Professional Engineer, do certify that the information contained in this report is correct and accurate to the best of my knowledge.
Henry Nemargut, P.E.
Henry Nemargut Engineering Services
North Carolina License #17669

FIGURES
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Newport, North Carolina, United States01 Jul 1983
Im a g e co u rte sy o f th e U.S. Geological Survey
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12/18/2012http://msrmaps.com/PrintImage.aspx?T=2&S=12&Z=18&X=410&Y=4812&W=3&qs=...
FIGURE 1: PROJECT LOCATION - USGS TOPO
Project Location
feet
meters
1000
300

TABLES
TABLE 1: SITE HISTORY
Handy House 3
6724 Hwy 70, Newport, NC 28570

Property Ownership:

Dominick Spadaro
303 Roberts Road
Newport, NC 28570
12/20/2012 to Present

Previous Owners:

J.M. Davis Industries, Inc.
201 Arendell Street
Morehead City, NC 28557
NCDENR Facility ID #0-035849
5/3/78 to 12/20/2012

UST Information:

Tank Inst. Size Closure UST Tank
No Date (Gal) Date Status Contents
T1 5/3/78 6,000 3/7/13 Closed Gasoline
T2 5/3/78 6,000 3/7/13 Closed Gasoline
T3 5/3/78 4,000 3/7/13 Closed Gasoline

Tank owner:

J.M. Davis Industries, Inc.
201 Arendell Street
Morehead City, NC 28557
NCDENR Facility ID #0-035849
5/3/78 to present

Sample Location E1 E2 SE S2 SW EF Lowest MSCC Ind/Comm MSCC Residential MSCCDate3/13/2013 3/13/2013 3/13/2013 3/13/2013 3/13/2013 5/23/2013 (note units) (note units) (note units)Sample depth4'-5' 4'-5' 4'-5' 4'-5' 4'-5' 4'-5' Method 8260 (ug/kg)Benzene BDL BDL BDL BDL BDL BDL 5.6 164,000.0 18,000Methyl Ethyl Ketone BDL BDL BDL BDL BDL BDL 16,000 245,280,000 7,821,000Methyl Isobutyl Ketone BDL BDL BDL BDL BDL BDL NSE NSE NSEMethyl Butyl Ketone BDL BDL BDL BDL BDL BDL NSE NSE NSEn-Butylbenzene BDL BDL BDL BDL BDL BDL 4,300 16,350,000 626,000sec-Butylbenzene BDL BDL BDL BDL BDL BDL 3,300 16,350,000 626,000Ethylbenzene BDL BDL 22.1 BDL BDL BDL 4,900 40,000,000 1,560,000Isopropylbenzene BDL BDL BDL BDL BDL BDL 2,000 40,880,000 1,564,000p-Isopropyltoluene BDL BDL BDL BDL BDL BDL NSE NSE NSENaphthalene BDL BDL BDL 9.1 BDL BDL 160 8176000 313,000Acetone BDL 21.5 21.1 BDL BDL BDL 24,000 360,000,000 14,000,000n-Propylbenzene BDL BDL BDL BDL BDL BDL 2,000 16,350,000 626,000Toluene BDL BDL 81.1 BDL BDL BDL 4,300 32,000,000 1,200,0001,2,4-Trimethylbenzene BDL BDL 24.3 15.1 BDL BDL 8,500 20,440,000 782,0001,3,5-Trimethylbenzene BDL BDL 8.7 5.8 BDL BDL 8,300 20,440,000 782,000MTBE BDL BDL631BDL BDL BDL 91 3,100,000 350,000Methylene Chloride6.3BDLBDLBDLBDLBDL20763,00085,000StyreneBDLBDLBDLBDLBDLBDL1,50081,760,0003,128,000Xylenes (total)BDLBDL2166.1BDLBDL4,60081,760,0003,129,000Method 8270 (ug/kg)ChryseneNRNRNRNRNRNR39,000780,00088,000Benzoic AcidNRNRNRNRNRNR120,000163,520,00062,571,000Phenanthrene NR NR NR NR NR NR 56,000 12,264,000 469,000Pyrene NR NR NR NR NR NR 270,000 12,264,000 469,0002-Methylnapthalene NR NR NR NR NR NR 3,600 1,635,000 63,000Naphthalene NR NR NR NR NR NR 160 8176000 313,000Aliphatic Fraction Classes (mg/kg) C5 - C8 Volatile Aliphatics BDL BDL BDL BDL BDL BDL 68 24,528 939C9 - C12 Volatile Aliphatics BDL BDL BDL BDL BDL BDL NSE NSE NSEC9-C18 Extractable Aliphatics NR NR NR NR NR NR NSE NSE NSEC9-C18 Aliphatics (total) BDL BDL BDL BDL BDL BDL 540 40,000 1,500C19-C36 Extractable Aliphatics NR NR NR NR NR NR NSE 810,000 31,000Aromatic Fraction Classes (mg/kg) C9 - C10 Volatile AromaticsBDLBDLBDLBDLBDLBDLNSENSENSEC11 - C22 Extractable AromaticsNRNRNRNRNRNRNSENSENSEC9 - C22 Aromatics (total)BDLBDLBDLBDLBDLBDL3112264469BDL = below detection limits NR = analyses not requested NSE = no standard establishedTABLE 2Laboratory Analytical Results - Risk Based Soil SamplesHandy House 3, 6724 Hwy 70, Newport, NC 28570
Sample Location SEF DPN DPW DPS1 DPS2 DPE Lowest MSCC Ind/Comm MSCC Residential MSCCDate5/23/2013 5/28/2013 5/28/2013 5/28/2013 5/28/2013 5/28/2013 (note units) (note units) (note units)Sample depth4'-5' 4'-5' 4'-5' 4'-5' 4'-5' 4'-5' Method 8260 (ug/kg)Benzene BDL BDL BDL BDL BDL BDL 5.6 164,000.0 18,000Methyl Ethyl Ketone BDL BDL BDL BDL BDL BDL 16,000 245,280,000 7,821,000Methyl Isobutyl Ketone BDL BDL BDL BDL BDL BDL NSE NSE NSEMethyl Butyl Ketone BDL BDL BDL BDL BDL BDL NSE NSE NSEn-Butylbenzene BDL BDL BDL BDL BDL BDL 4,300 16,350,000 626,000sec-Butylbenzene BDL BDL BDL BDL BDL 288 3,300 16,350,000 626,000Ethylbenzene BDL BDL BDL BDL BDL 961 4,900 40,000,000 1,560,000Isopropylbenzene BDL BDL BDL BDL BDL 808 2,000 40,880,000 1,564,000p-Isopropyltoluene BDL BDL BDL BDL BDL 11,300 NSE NSE NSENaphthalene BDL BDL BDL BDL BDL10,400160 8176000 313,000Acetone 122 BDL BDL BDL BDL BDL 24,000 360,000,000 14,000,000n-Propylbenzene BDL BDL BDL BDL BDL 1540 2,000 16,350,000 626,000Toluene BDL BDL BDL BDL BDL BDL 4,300 32,000,000 1,200,0001,2,4-Trimethylbenzene BDL BDL BDL BDL BDL172,0008,500 20,440,000 782,0001,3,5-Trimethylbenzene BDL BDL BDL BDL BDL70,5008,300 20,440,000 782,000MTBE BDL BDL BDL BDL BDL BDL 91 3,100,000 350,000trans-1,2-DichloroetheneBDL20.816.910.9BDLBDL5408,200,000310,000StyreneBDLBDLBDLBDLBDLBDL1,50081,760,0003,128,000Xylenes (total)BDLBDLBDLBDLBDL34,1004,60081,760,0003,129,000Method 8270 (ug/kg)ChryseneNRNRNRNRNRNR39,000780,00088,000Benzoic AcidNRNRNRNRNRNR120,000163,520,00062,571,000Phenanthrene NR NR NR NR NR NR 56,000 12,264,000 469,000Pyrene NR NR NR NR NR NR 270,000 12,264,000 469,0002-Methylnapthalene NR NR NR NR NR NR 3,600 1,635,000 63,000Naphthalene NR NR NR NR NR NR 160 8176000 313,000Aliphatic Fraction Classes (mg/kg) C5 - C8 Volatile Aliphatics BDL BDL BDL BDL BDL11268 24,528 939C9 - C12 Volatile Aliphatics BDL BDL BDL BDL 5.1 2420 NSE NSE NSEC9-C18 Extractable Aliphatics NR NR NR NR NR NR NSE NSE NSEC9-C18 Aliphatics (total) BDL BDL BDL BDL 5.12420540 40,000 1,500C19-C36 Extractable Aliphatics NR NR NR NR NR NR NSE 810,000 31,000Aromatic Fraction Classes (mg/kg) C9 - C10 Volatile AromaticsBDLBDLBDLBDLBDL1030NSENSENSEC11 - C22 Extractable AromaticsNRNRNRNRNRNRNSENSENSEC9 - C22 Aromatics (total)BDLBDLBDLBDLBDL10303112264469BDL = below detection limits NR = analyses not requested NSE = no standard establishedTABLE 2 (continued)Laboratory Analytical Results - Risk Based Soil SamplesHandy House 3, 6724 Hwy 70, Newport, NC 28570
Sample Location B1 B2 B3 B4 Lowest MSCC Ind/Comm MSCC Residential MSCCDate5/6/2014 5/6/2014 5/6/2014 5/6/2014 (note units) (note units) (note units)Sample depth4' 4' 4' 4' Method 8260 (ug/kg)Benzene BDL BDL BDL BDL 5.6 164,000.0 18,000Methyl Ethyl Ketone BDL BDL BDL BDL 16,000 245,280,000 7,821,000Methyl Isobutyl Ketone BDL BDL BDL BDL NSE NSE NSEMethyl Butyl Ketone BDL BDL BDL BDL NSE NSE NSEn-Butylbenzene BDL BDL BDL BDL 4,300 16,350,000 626,000sec-Butylbenzene BDL BDL BDL BDL 3,300 16,350,000 626,000Ethylbenzene BDL BDL BDL BDL 4,900 40,000,000 1,560,000Isopropylbenzene BDL BDL BDL BDL 2,000 40,880,000 1,564,000p-Isopropyltoluene BDL BDL BDL BDL NSE NSE NSENaphthalene BDL BDL BDL BDL 160 8176000 313,000Acetone BDL BDL BDL BDL 24,000 360,000,000 14,000,000n-Propylbenzene BDL BDL BDL BDL 2,000 16,350,000 626,000Toluene BDL BDL BDL BDL 4,300 32,000,000 1,200,0001,2,4-Trimethylbenzene BDL BDL BDL BDL 8,500 20,440,000 782,0001,3,5-Trimethylbenzene BDL BDL BDL BDL 8,300 20,440,000 782,000MTBE BDL BDL BDL BDL 91 3,100,000 350,000trans-1,2-DichloroetheneBDLBDLBDLBDL5408,200,000310,000StyreneBDLBDLBDLBDL1,50081,760,0003,128,000Xylenes (total)BDLBDLBDLBDL4,60081,760,0003,129,000Method 8270 (ug/kg)ChryseneNRNRNRNR39,000780,00088,000Benzoic AcidNRNRNRNR120,000163,520,00062,571,000Phenanthrene NR NR NR NR 56,000 12,264,000 469,000Pyrene NR NR NR NR 270,000 12,264,000 469,0002-Methylnapthalene NR NR NR NR 3,600 1,635,000 63,000Naphthalene NR NR NR NR 160 8176000 313,000Aliphatic Fraction Classes (mg/kg) C5 - C8 Volatile Aliphatics BDL BDL BDL BDL 68 24,528 939C9 - C12 Volatile Aliphatics BDL BDL BDL BDL NSE NSE NSEC9-C18 Extractable Aliphatics NR NR NR NR NSE NSE NSEC9-C18 Aliphatics (total) BDL BDL BDL BDL 540 40,000 1,500C19-C36 Extractable Aliphatics NR NR NR NR NSE 810,000 31,000Aromatic Fraction Classes (mg/kg) C9 - C10 Volatile AromaticsBDLBDLBDLBDLNSENSENSEC11 - C22 Extractable AromaticsNRNRNRNRNSENSENSEC9 - C22 Aromatics (total)BDLBDLBDLBDL3112264469BDL = below detection limits NR = analyses not requested NSE = no standard establishedTABLE 2 (continued)Laboratory Analytical Results - Risk Based Soil SamplesHandy House 3, 6724 Hwy 70, Newport, NC 28570
TABLE 3Monitoring Well Information and Groundwater ElevationsHandy House #3, 6724 Hwy 70, Newport, NC 28570Well Number Top of Casing Elevation Top of Screen Elevation Bottom of Screen Elevation Depth to Water Groundwater ElevationMW-1 99.31 96.31 81.31 4.81 94.50MW-2 99.32 96.32 81.32 5.73 93.59MW-3 100.00 97.00 82.00 7.01 92.99MW-4 100.00 96.00 81.00 n/a #VALUE!MW-5 98.20 93.20 83.20 n/a #VALUE!MW-6 99.18 94.18 84.18 n/a #VALUE!MW-7 98.43 94.43 80.43 n/a #VALUE!MW-8 100.15 95.15 80.15 7.69 92.46MW-9 100.17 95.17 80.17 6.96 93.21MW-10 99.43 97.43 82.43 5.48 93.95MW-11 98.78 93.78 83.78 4.05 94.73MW-12 99.21 94.21 79.21 n/a #VALUE!MW-13 98.45 93.45 78.45 n/a #VALUE!MW-14 100.60 95.60 80.60 7.14 93.46MW-15 97.06 92.06 77.06 8.67 88.39MW-16 97.18 92.18 77.18 n/a #VALUE!MW-17 94.62 89.62 74.62 4.34 90.28VEW-1 99.96 32.96 22.96 21.41 78.55All measurements taken in feet and based on an arbitrary benchmark of 100 ft. established at MW-3Groundwater levels measured on 3/18/2020HH3
TABLE 4SUMMARY OF GROUNDWATER ANALYTICAL RESULTSHANDY HOUSE 36724 HWY 70, NEWPORT, NC 28570Constituent MW-1 MW-2 MW-3 MW-8 MW-9 GCL 2L Standard Date3/18/2020 3/18/2020 3/18/2020 3/18/2020 3/18/2020 Method 6200B (ug/L)Benzene BDL BDL BDL BDL BDL 5,000 1Toluene BDL BDL 7.9 BDL BDL 260,000 600Ethylbenzene BDL 0.66 338 BDL BDL 84,500 600Xylenes (total) BDL BDL734BDL BDL 85,500 500BTEX (total) 0 0.66 1079.9 0 0 NSE NSEp-Isopropyltoluene BDL BDL BDL BDL BDL NSE NSEIsopropylbenzene 1.1 0.56 55.7 BDL BDL 25,000 70Diisopropyl Ether (DIPE) BDL BDL BDL BDL BDL 70,000 70Naphthalene BDL 2.7332BDL BDL 6,000 6n-propylbenzene BDL BDL BDL BDL BDL 30,000 70n-butylbenzene BDL BDL BDL BDL BDL 6,900 70sec-butylbenzene BDL 1.4 BDL BDL BDL 8,500 70tert-butylbenzene BDL BDL BDL BDL BDL 7,000 70Methyl-tert-butyl-ether (MTBE) BDL BDL BDL BDL BDL 20,000 20Acetone BDL BDL BDL BDL BDL 6,000,000 6,0001,2,3-Trichloropropane 2.5 BDL BDL BDL BDL NSE NSEMethyl Isobutyl Ketone BDL BDL BDL BDL BDL 100,000 1001,2,4-Trimethylbenzene 82.6 0.51972BDL BDL 28,500 4001,3,5-Trimethylbenzene 86.2 BDL BDL BDL BDL 25,000 400TOTAL 6200B 172.4 5.83 2439.6 0 0 15,000 15Aliphatic Fraction Classes (ug/L)C5-C8 Volatile Aliphatics BDL 343 BDL BDL BDL NSE 400C9-C12 Volatile Aliphatics 410 135 3690 BDL BDL NSE NSEC9-C18 Extractable Aliphatics N/A N/A N/A N/A N/A NSE 700C9-C18 Aliphatics (total) 410 4783690BDL BDL NSE 700C19-C36 Extractable Aliphatics N/A N/A N/A N/A N/A NSE 10,000Aromatic Fraction Classes (ug/L)C9-C10 Volatile Aromatics 1040 258 4360 BDL BDL NSE NSEC11-C22 Extractable Aromatics N/A N/A N/A N/A N/A NSE NSEC9-C22 Aromatics (total)1,040 258 4,360BDL BDLNSE 200N/A = Not Analyzed BDL = Below Detection Limits NSE = No Standard Established
TABLE 4 (Continued)SUMMARY OF GROUNDWATER ANALYTICAL RESULTSHANDY HOUSE 36724 HWY 70, NEWPORT, NC 28570Constituent MW-10 MW-11 MW-14 MW-15 MW-17 GCL 2L Standard Date3/18/2020 3/18/2020 3/18/2020 3/18/2020 3/18/2020 Method 6200B (ug/L)Benzene BDL BDL BDL BDL BDL 5,000 1Toluene BDL BDL BDL BDL BDL 260,000 600Ethylbenzene BDL BDL BDL BDL BDL 84,500 600Xylenes (total) 7.5 BDL BDL BDL BDL 85,500 500BTEX (total) 7.5 0 0 0 0 NSE NSEp-Isopropyltoluene BDL BDL BDL BDL BDL NSE NSEIsopropylbenzene BDL BDL BDL BDL BDL 25,000 70Diisopropyl Ether (DIPE) BDL BDL BDL BDL BDL 70,000 70Naphthalene34.9BDL BDL BDL BDL 6,000 6n-propylbenzene BDL BDL BDL BDL BDL 30,000 70n-butylbenzene BDL BDL BDL BDL BDL 6,900 70sec-butylbenzene BDL BDL BDL BDL BDL 8,500 70tert-butylbenzene BDL BDL BDL BDL BDL 7,000 70Methyl-tert-butyl-ether (MTBE) BDL BDL BDL BDL BDL 20,000 201,2,4-Trimethylbenzene 289 BDL BDL BDL BDL 28,500 4001,3,5-Trimethylbenzene BDL BDL BDL BDL BDL 25,000 400Acetone BDL BDL BDL BDL BDL 6,000,000 6000TOTAL 6200B 331.4 0 0 0 0 15,000 15Aliphatic Fraction Classes (ug/L)C5-C8 Volatile Aliphatics 140 BDL BDL BDL BDL NSE 400C9-C12 Volatile Aliphatics 1050 BDL BDL BDL BDL NSE NSEC9-C18 Extractable Aliphatics N/A N/A N/A N/A N/A NSE 700C9-C18 Aliphatics (total)1190BDL BDL BDL BDL NSE 700C19-C36 Extractable Aliphatics N/A N/A N/A N/A N/A NSE 10,000Aromatic Fraction Classes (ug/L)C9-C10 Volatile Aromatics 1970 BDL BDL BDL BDL NSE NSEC11-C22 Extractable Aromatics N/A N/A N/A N/A N/A NSE NSEC9-C22 Aromatics (total)1,970BDL BDL BDL BDLNSE 200N/A = Not AnalyzedBDL = Below Detection LimitsNSE = No Standard Established
TABLE 4 (Continued)SUMMARY OF GROUNDWATER ANALYTICAL RESULTSHANDY HOUSE 36724 HWY 70, NEWPORT, NC 28570Constituent VEW-1 SW-3 GCL 2L Standard Date3/18/2020 3/18/2020 Method 6200B (ug/L)Benzene BDL BDL 5,000 1Toluene BDL BDL 260,000 600Ethylbenzene BDL BDL 84,500 600Xylenes (total) BDL BDL 85,500 500BTEX (total) 0 0 NSE NSEp-Isopropyltoluene BDL BDL NSE NSEIsopropylbenzene BDL BDL 25,000 70Diisopropyl Ether (DIPE) BDL BDL 70,000 70Naphthalene BDL BDL 6,000 6n-propylbenzene BDL BDL 30,000 70n-butylbenzene BDL BDL 6,900 70sec-butylbenzene BDL BDL 8,500 70tert-butylbenzene BDL BDL 7,000 70Methyl-tert-butyl-ether (MTBE) BDL BDL 20,000 201,2,4-Trimethylbenzene BDL BDL 28,500 4001,3,5-Trimethylbenzene BDL BDL 25,000 400Acetone BDL BDL 6,000,000 6000TOTAL 6200B 0 0 15,000 15Aliphatic Fraction Classes (ug/L)C5-C8 Volatile Aliphatics BDL BDL NSE 400C9-C12 Volatile Aliphatics BDL BDL NSE NSEC9-C18 Extractable Aliphatics N/A N/A NSE 700C9-C18 Aliphatics (total) BDL BDL NSE 700C19-C36 Extractable Aliphatics N/A N/A NSE 10,000Aromatic Fraction Classes (ug/L)C9-C10 Volatile Aromatics BDL BDL NSE NSEC11-C22 Extractable Aromatics N/A N/A NSE NSEC9-C22 Aromatics (total) BDL BDLNSE 200N/A = Not AnalyzedBDL = Below Detection LimitsNSE = No Standard Established
WellIdentification IW-2 SW-3 SW-4 SW-5 SW-6Owner Name Atlantic Coast Properties Elaine Honeycutt Dominick Spadaro Christine Arnette Daniel ClapsadlOwner Address 112 Queen Creek Rd #1 313 Brook Lane 303 Roberts Road 297 Roberts Road 332 Roberts RoadSwansboro, NC 28584 Newport, NC 28570 Newport, NC 28570 Newport, NC 28570 Newport, NC 28570Well Address 6650 Highway 70 6760 Hwy 70 303 Roberts Road 297 Roberts Road 332 Roberts RoadNewport, NC 28570 Newport, NC 28570 Newport, NC 28570 Newport, NC 28570 Newport, NC 28570Occupant Unoccupied Second Go-Round Co Dominick Spadaro Larry & Ashley Arnette Daniel ClapsadlTelephone # none [phone] [phone] [phone] [phone]UseOut of Service -no structureDrinking - Potable Drinking - Potable Drinking - Potable Drinking - PotableDistance 300' 485' 765' 855' 890'City Water? NO NO NO NO NODepth of Well Unknown Unknown Unknown Unknown UnknownWell Diameter Unknown Unknown Unknown Unknown UnknownWell Yield Unknown Unknown Unknown Unknown UnknownDepth to Pump Unknown Unknown Unknown Unknown UnknownDepth of Casing Unknown Unknown Unknown Unknown UnknownStatic Water Unknown Unknown Unknown Unknown UnknownTABLE 5SUPPLY WELL INFORMATION1,000' RADIUSHANDY HOUSE #36724 HWY 70, NEWPORT, NC 28570
Estimated Area  (Ft2) Est. Thickness  (ft) Avg Cont. Level (ppm) Est. Cont. Mass (lbs) EstimatedDate Zone Soil in Soil in Soil in Soil in Soil in Soil in Soil in Soil in Total Massof Isonconcen. Source Smear Source Smear Source Smear Source Smear Measurement Designation Area Zone GH2O Area Zone GH2O Area Zone GH2O Area Zone GH2O in LbsAug‐14 UST Pit 50 200 6720 2 6 6 200 1200 50 2.2222 160 31.441 193.66336Aug‐14 Downgradient 0 0 13510 0 0 10 0 0 0.5 0 0 1.0535 1.0534963Date Totals 2.2222 160 32.495 194.716853/18/2020 UST Pit 50 200 900 2 6 6 200 1200 20 2.2222 160 1.6843 163.906573/18/2020 Downgradient 0 0 4570 0 0 10 0 0 0.5 0 0 0.3564 0.356364Date Totals 2.2222 160 2.0407 164.26293% Mass Reduction 0 0.9372 0.156401Estimated Soil Porosity = 0.25Estimated Soil Density = 1.5 tons/cubic yardSoil CalculationsArea x Thickness x Density/27 x 2000lbs/ton x contaminated fraction (ppm) Groundwater Calculations 6200B compounds assumed to represent 10% of total dissolved organic compoundsArea x Thickness x porosity x 7.48 gallons/cu.ft. x 8.34 lbs/gallon x contaminated fraction (ppm)TABLE 6 - MASS CALCULATION TABLEHandy House 3, 6724 Hwy 70, Newport, NC  28570
NC 2L Standard 600 600 500 70 6 20 70 400 400 N/A
NC GCL Standard 260000 84500 85500 25000 6000 20000 30000 28500 25000 N/A
Toluene Ethyl- Xylenes Isopro- Napht MTBE n-propyl 1,2,4-tri- 1,3,5-tri- Total GH2O
Well Date Benzene benzene halene benzene methylbenz methylbenz 6200B Elev
# Sampled (ug/l) (ug/l) (ug/l) (ug/l) (ug/l) (ug/l) (ug/l) (ug/l) (ug/l) (ug/l) (ft)
MW-1 7/11/2013 BDL 4.3 206.4 34.3 17.1 BDL 70.7 1120 321 1528.8 89.76
5/7/2014 17.4 16.2 274.5 34.3 65.9 BDL 81.2 1950 684 2781.1 94.94
8/28/2014 BDL 7 226 122 67.3 BDL 111 4920 1760 6858.3 95.41
3/10/2015 BDL BDL 80.5 70.5 BDL BDL 72.6 2700 1190 3962.6 95.59
11/29/2015 BDL BDL 61.2 34.8 BDL BDL 17.5 3140 1460 4617.5 95.77
8/28/2016 BDL BDL BDL 25.3 BDL BDL 9.1 975 346 1330.1 93.91
3/18/2017 BDL BDL 7.7 6.3 BDL BDL 7.4 191 34.7 233.1 92.92
10/16/2017 BDL BDL 11.2 15.1 BDL BDL BDL 624 419 1043 93.05
5/16/2018 BDL 0.55 15 15.55 1.8 BDL 8.4 450 300 760.2 94.23
2/14/2019 BDL BDL BDL BDL BDL BDL BDL 166 306 472 95.1
3/18/2020 BDL BDL BDL 1.1 BDL BDL BDL 82.6 86.2 168.8 94.5
MW-2 7/11/2013 8.6 127 1274.3 55.8 372 BDL 155 2030 722 3279 93.31
5/7/2014 134 646 824 58 322 BDL 126 672 90.2 1210.2 94.37
8/28/2014 BDL 283 9.4 36.5 276 BDL 91.2 152 BDL 519.2 94.87
3/10/2015 BDL 93.7 18.9 16.9 166 BDL 32.6 BDL BDL 198.6 95.02
11/29/2015 BDL 37 7.5 8.9 91.9 BDL 16.3 14.1 16.5 138.8 95.26
8/28/2016 BDL 90.8 0.68 16.8 135 BDL 38.3 1.5 0.93 175.73 93.53
3/18/2017 BDL 9.9 1.9 11.8 3.9 BDL 8.6 8.2 1.3 22 92.05
10/16/2017 BDL 7.7 1.3 9 26.7 BDL 4.8 2.2 BDL 33.7 92.2
5/16/2018 BDL 1.1 BDL BDL 9 BDL 0.68 BDL BDL 9.68 93.32
2/14/2019 BDL BDL BDL BDL 3.4 BDL BDL BDL BDL 3.4 94.05
3/18/2020 BDL 0.66 BDL 0.56 2.7 BDL BDL 0.51 BDL 3.21 93.59
MW-3 7/11/2013 2390 1800 19590 183 1170 41.7 410 4690 1410 7721.7 92.88
5/7/2014 414 392 2900 34.9 328 BDL 73.3 1010 233 1644.3 89.28
8/28/2014 469 474 3850 45.7 457 BDL 101 1310 320 2188 91.72
3/10/2015 570 596 3060 53.2 370 BDL 125 925 290 1710 94.15
11/29/2015 108 260 2353 38.7 371 BDL 93.6 972 271 1707.6 93.96
8/28/2016 162 298 2044 33.7 352 BDL 82.7 899 244 1577.7 92.26
3/18/2017 BDL 63.9 133.5 14.9 133 BDL 34.4 230 88.5 485.9 91.25
10/16/2017 0.74 13.7 32.4 3.1 38.4 BDL BDL 66.1 46.4 150.9 91.45
5/16/2018 3.1 180 1200 37 290 BDL 90 930 460 1770 92.57
2/14/2019 BDL 72.9 481 32.7 333 BDL 84.5 1380 618 2415.5 93.39
3/18/2020 7.9 338 734 55.7 332 BDL BDL 972 BDL 1304 92.99
MW-4 7/11/2013 BDL BDL BDL BDL BDL 0.64 BDL BDL BDL 0.64 92.97
5/7/2014 BDL BDL BDL BDL BDL 0.64 BDL BDL BDL 0.64 93.91
8/28/2014 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 94.7
3/10/2015 1.5 0.55 2.69 BDL BDL BDL BDL 1.1 BDL 1.1 94.83
11/29/2015 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 95.44
8/28/2016 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 93.14
MW-5 7/11/2013 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 93.57
5/7/2014 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 95.28
8/28/2014 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 95.7
3/10/2015 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 95.88
11/29/2015 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 95.92
8/28/2016 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 94.01
MW-6 5/7/2014 BDL 1.5 7.1 BDL BDL BDL 0.65 4.4 0.93 5.98 94.72
8/28/2014 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 95.06
3/10/2015 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 95.23
11/29/2015 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 95.33
8/28/2016 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 93.73
MW-7 5/7/2014 BDL 0.59 BDL BDL BDL 0.64 BDL BDL BDL 0.64 93.45
8/28/2014 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 93.91
3/10/2015 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 93.99
11/29/2015 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 94.23
8/28/2016 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 92.8
MW-8 5/7/2014 18.3 610 546 65.5 392 BDL 148 937 222 1699 90.01
8/28/2014 3.9 343 87.5 35.6 234 BDL 86 267 20 607 93.02
TABLE 7: SUMMARY OF 6200B GROUNDWATER ANALYTICAL RESULTS
Handy House #3, 6724 Hwy 70, Newport, NC 28570
3/10/2015 BDL 303 11 39.3 189 BDL 91.4 44 10.2 334.6 93.63
11/29/2015 BDL 306 BDL 41.7 231 BDL 101 5.9 BDL 337.9 94.14
8/28/2016 BDL 91.4 BDL 13 81.3 BDL 30.2 1.4 BDL 112.9 92.32
3/18/2017 1.2 BDL BDL BDL BDL BDL BDL BDL BDL 0 91.02
10/16/2017 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 91.25
5/16/2018 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 92.24
2/14/2019 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 92.86
3/18/2020 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 92.46
MW-9 5/7/2014 10.8 608 2990 70 255 BDL 157 1150 254 1816 90.32
8/28/2014 BDL 36.2 25.2 5 28.8 BDL 14.6 88.4 19.8 151.6 93.94
3/11/2015 1.8 16.5 18.9 39.3 189 BDL 9.6 41.1 4.8 244.5 93.84
11/28/2015 BDL 26.8 6.1 4.8 27.8 BDL 14 52.1 10.4 104.3 94.94
8/28/2016 27.5 556 2370 57.9 279 BDL 150 1380 338 2147 92.65
3/18/2017 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 91.94
10/16/2017 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 91.6
5/16/2018 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 92.88
2/14/2019 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 93.76
3/18/2020 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 93.21
MW-10 5/7/2014 3.2 848 5350 94.6 304 0.81 206 1560 357 2427.81 93.06
8/28/2014 12.8 419 2704 54 253 BDL 142 1100 284 1779 93.63
3/11/2015 9.7 238 1558 30.9 105 BDL 83.9 655 161 1004.9 93.77
11/28/2015 BDL 285 1893 37.7 268 BDL 93.5 948 391 1700.5 95.36
8/28/2016 5 391 2596 56.8 293 BDL 150 1380 338 2161 93.24
3/18/2017 BDL 3.9 30.8 5 10 BDL 17.1 180 53.9 261 92.37
10/16/2017 BDL 4.6 39.2 2.5 10.7 BDL BDL 141 46.4 198.1 92.61
5/16/2018 BDL 5.9 180 5.9 74 BDL 15 850 270 1209 93.78
2/14/2019 BDL 2.4 37.2 3.4 23.7 BDL 8.4 465 156 653.1 94.55
3/18/2020 BDL BDL 7.5 BDL 34.9 BDL BDL 289 BDL 323.9 93.95
MW-11 5/7/2014 BDL 4.4 23.7 0.56 6.2 BDL 1.8 13.4 2.8 24.2 95.11
8/28/2014 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 95.54
3/11/2015 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 95.75
11/28/2015 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 95.9
8/21/2016 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 93.91
2/14/2019 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 95.34
3/18/2020 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 94.73
MW-12 5/7/2014 BDL 2.2 5.2 BDL 2.4 3.6 0.65 4.8 0.83 12.28 92.61
8/28/2014 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 93.09
3/11/2015 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 93.29
11/28/2015 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 93.86
8/28/2016 BDL BDL BDL BDL BDL 0.56 BDL BDL BDL 0.56 91.13
3/18/2017 BDL BDL BDL BDL BDL 0.57 BDL BDL BDL 0.57 90.34
MW-13 6/7/2014 14.5 441 1023 38.2 232 5.5 85.7 717 143 1183.2 92.06
8/28/2014 BDL 16.2 5.8 1.9 8.6 BDL 4.9 23.6 5.5 42.6 92.46
3/10/2015 BDL 218 1.3 25.8 122 BDL 61.6 20.9 BDL 204.5 92.54
11/29/2015 BDL 16.3 BDL 4 BDL BDL 11.3 1.5 BDL 12.8 92.72
MW-14 5/7/2014 BDL 3 9.1 BDL BDL BDL 0.67 3.9 BDL 4.57 93.74
8/28/2014 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 93.96
3/11/2015 2.2 0.93 4.1 25.8 BDL 0.52 BDL 0.52 1.7 2.74 94.13
11/28/2015 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 94.8
8/28/2016 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 92.56
5/16/2018 BDL BDL BDL BDL 0.84 BDL BDL BDL BDL 0.84 92.3
2/14/2019 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 93.43
3/18/2020 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 93.46
MW-15 8/28/2014 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 90.34
3/10/2015 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 91.21
11/29/2015 BDL 3.4 BDL 2 BDL BDL 1.4 BDL BDL 1.4 91.58
8/28/2016 BDL 0.82 BDL 2.7 BDL BDL BDL BDL BDL 0 87.41
3/18/2017 BDL BDL BDL BDL BDL 7.9 BDL BDL BDL 7.9 86.92
10/16/2017 BDL BDL BDL BDL BDL 15.4 BDL BDL BDL 15.4 85.83
5/16/2018 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 88.25
2/14/2019 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 88.39
3/18/2020 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 88.39
MW-16 8/28/2014 BDL 15.6 BDL 4.8 4.3 BDL 9.9 0.74 BDL 14.94 91.78
3/10/2015 BDL 8.9 BDL 0.78 2.9 1.7 1.7 1.1 BDL 7.4 91.86
11/29/2015 BDL 68.9 BDL 14 21.4 BDL 22.4 77 BDL 120.8 92.49
8/28/2016 BDL 2 BDL 4.6 BDL BDL BDL BDL BDL 0 89.54
3/18/2017 BDL BDL BDL 1.1 BDL BDL BDL BDL BDL 0 88.82
MW-17 8/28/2014 BDL BDL BDL BDL BDL 1.1 BDL BDL BDL 1.1 90.32
3/10/2015 BDL BDL BDL BDL BDL BDL 0.61 BDL BDL 0.61 84.75
11/29/2015 BDL 4.7 BDL 1.1 BDL 3 1.6 BDL BDL 4.6 88.95
8/28/2016 BDL 0.56 BDL BDL BDL 3.9 BDL BDL BDL 3.9 86.34
10/16/2017 BDL BDL BDL BDL BDL 0.55 BDL BDL BDL 0.55 88.37
5/16/2018 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 89.01
2/14/2019 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 89.66
3/18/2020 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 90.28
VEW-1 5/7/2014 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 78.82
8/28/2014 4.8 1.5 9.4 BDL BDL BDL BDL 1.1 BDL 1.1 78.12
3/11/2015 4.3 1.6 7.7 BDL BDL BDL BDL 2.3 0.68 2.98 78.71
11/28/2015 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 78.84
8/28/2016 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 76.56
2/14/2019 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 78.97
3/18/2020 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0 78.55
SW-1 5/7/2014 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
8/28/2014 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
3/10/2015 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
11/29/2015 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
8/28/2016 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
3/18/2017 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
SW-3 8/28/2014 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
3/10/2015 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
11/29/2015 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
8/28/2016 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
3/18/2017 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
10/16/2017 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
5/16/2018 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
2/14/2019 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
3/18/2020 BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
BDL = Below Detection Limits
NSE = No Standard Established
N/A = Not Applicable
TABLE 8SUMMARY OF GROUNDWATER ANALYTICAL RESULTSHANDY HOUSE 36724 HWY 70, NEWPORT, NC 28570Constituent MW-1 MW-2 MW-3 MW-4 MW-5 GCL 2L Standard Date8/28/2014 8/28/2014 8/28/2014 8/28/2014 8/28/2014 Method 6200B (ug/L)Benzene BDL BDL BDL BDL BDL 5,000 1Toluene BDL BDL 469 BDL BDL 260,000 600Ethylbenzene 7 283 474 BDL BDL 84,500 600Xylenes (total) 226.1 9.43850BDL BDL 85,500 500BTEX (total) 233.1 292.4 4793 0 0 NSE NSEp-Isopropyltoluene BDL BDL BDL BDL BDL NSE NSEIsopropylbenzene12236.5 45.7 BDL BDL 25,000 70Diisopropyl Ether (DIPE) BDL BDL BDL BDL BDL 70,000 70Naphthalene67.3 276 457BDL BDL 6,000 6n-propylbenzene111 91.2 101BDL BDL 30,000 70n-butylbenzene BDL 17.9 BDL BDL BDL 6,900 70sec-butylbenzene BDL 9.3 BDL BDL BDL 8,500 70Methyl-tert-butyl-ether (MTBE) BDL BDL BDL BDL BDL 20,000 201,2,4-Trimethylbenzene49201521310BDL BDL 28,500 4001,3,5-Trimethylbenzene1760BDL 320 BDL BDL 25,000 400Tetrachloroethene BDL BDL BDL BDL BDL 700 0.7Acetone BDL BDL BDL BDL BDL 6,000,000 6000Total 6200B 7213.4 875.3 7026.7 0 0 15,000 15Aliphatic Fraction Classes (ug/L) 4/12/2014 4/12/2014 4/12/2014 4/12/2014 4/12/2014C5-C8 Volatile Aliphatics BDL BDL876BDL BDL NSE 400C9-C12 Volatile Aliphatics 7,840 6,600 11,900 BDL BDL NSE NSEC9-C18 Extractable Aliphatics N/A N/A N/A N/A N/A NSE 700C9-C18 Aliphatics (total)7,840 6,600 11,900BDL BDL NSE 700C19-C36 Extractable Aliphatics N/A N/A N/A N/A N/A NSE 10,000Aromatic Fraction Classes (ug/L)C9-C10 Volatile Aromatics 3,840 1,540 2,160 BDL BDL NSE NSEC11-C22 Extractable Aromatics N/A N/A N/A N/A N/A NSE NSEC9-C22 Aromatics (total)3,840 1,540 2,160BDL BDLNSE 200N/A = Not AnalyzedBDL = Below Detection LimitsNSE = No Standard Established
TABLE 8 (Continued)SUMMARY OF GROUNDWATER ANALYTICAL RESULTSHANDY HOUSE 36724 HWY 70, NEWPORT, NC 28570Constituent MW-6 MW-7 MW-8 MW-9 MW-10 GCL 2L Standard Date8/28/2014 8/28/2014 8/28/2014 8/28/2014 8/28/2014 Method 6200B (ug/L)Benzene BDL BDL BDL BDL BDL 5,000 1Toluene BDL BDL 3.9 BDL 12.8 260,000 600Ethylbenzene BDL BDL 343 36.2 419 84,500 600Xylenes (total) BDL BDL 87.5 25.2270485,500 500BTEX (total) 0 0 434.4 61.4 3135.8 NSE NSEp-Isopropyltoluene BDL BDL BDL BDL BDL NSE NSEIsopropylbenzene BDL BDL 35.6 5 54 25,000 70Diisopropyl Ether (DIPE) BDL BDL BDL BDL BDL 70,000 70Naphthalene BDL BDL234 28.8 2536,000 6n-propylbenzene BDL BDL8614.614230,000 70n-butylbenzene BDL BDL BDL BDL BDL 6,900 70sec-butylbenzene BDL BDL BDL BDL BDL 8,500 70Methyl-tert-butyl-ether (MTBE) BDL BDL BDL BDL BDL 20,000 201,2,4-Trimethylbenzene BDL BDL 267 88.4110028,500 4001,3,5-Trimethylbenzene BDL BDL 20 19.8 284 25,000 400Tetrachloroethene BDL BDL BDL BDL BDL 700 0.7Styrene BDL BDL BDL BDL BDL 70,000 70Total 6200B 0 0 1077 218 4968.8 15,000 15Aliphatic Fraction Classes (ug/L) 4/12/2014 4/12/2014 4/12/2014 4/12/2014 4/12/2014C5-C8 Volatile Aliphatics BDL BDL BDL BDL BDL NSE 400C9-C12 Volatile Aliphatics BDL BDL 6,950 12,500 21,400 NSE NSEC9-C18 Extractable Aliphatics N/A N/A N/A N/A N/A NSE 700C9-C18 Aliphatics (total) BDL BDL6,950 12,500 21,400NSE 700C19-C36 Extractable Aliphatics N/A N/A N/A N/A N/A NSE 10,000Aromatic Fraction Classes (ug/L)C9-C10 Volatile Aromatics BDL BDL 2,020 2,180 3,310 NSE NSEC11-C22 Extractable Aromatics N/A N/A N/A N/A N/A NSE NSEC9-C22 Aromatics (total) BDL BDL2,020 2,180 3,310NSE 200N/A = Not AnalyzedBDL = Below Detection LimitsNSE = No Standard Established
TABLE 8 (Continued)SUMMARY OF GROUNDWATER ANALYTICAL RESULTSHANDY HOUSE 36724 HWY 70, NEWPORT, NC 28570Constituent MW-11 MW-12 MW-13 MW-14 VEW-1 GCL 2L Standard Date8/28/2014 8/28/2014 8/28/2014 8/28/2014 8/28/2014 Method 6200B (ug/L)Benzene BDL BDL BDL BDL BDL 5,000 1Toluene BDL BDL BDL BDL 4.8 260,000 600Ethylbenzene BDL BDL 16.2 BDL 1.5 84,500 600Xylenes (total) BDL BDL 5.8 BDL 9.4 85,500 500BTEX (total) 0 0 22 0 15.7 NSE NSEp-Isopropyltoluene BDL BDL BDL BDL BDL NSE NSEIsopropylbenzene BDL BDL 1.9 BDL BDL 25,000 70Diisopropyl Ether (DIPE) BDL BDL BDL BDL BDL 70,000 70Naphthalene BDL BDL8.6BDL BDL 6,000 6n-propylbenzene BDL BDL 4.9 BDL BDL 30,000 70n-butylbenzene BDL BDL BDL BDL BDL 6,900 70sec-butylbenzene BDL BDL BDL BDL BDL 8,500 70Methyl-tert-butyl-ether (MTBE) BDL BDL BDL BDL BDL 20,000 201,2,4-Trimethylbenzene BDL BDL 23.6 BDL 1.1 28,500 4001,3,5-Trimethylbenzene BDL BDL 5.5 BDL BDL 25,000 400Methylene Chloride BDL BDL BDL BDL BDL 5,000 5Styrene BDL BDL BDL BDL BDL 70,000 70TOTAL 0 0 66.5 0 16.8 15,000 15Aliphatic Fraction Classes (ug/L) 4/12/2014 5/7/2014 5/7/2014 5/7/2014 5/7/2014C5-C8 Volatile Aliphatics BDL BDL BDL BDL BDL NSE 400C9-C12 Volatile Aliphatics 68.6 BDL 5720 BDL BDL NSE NSEC9-C18 Extractable Aliphatics N/A N/A N/A N/A N/A NSE 700C9-C18 Aliphatics (total) 68.6 BDL5720BDL BDL NSE 700C19-C36 Extractable Aliphatics N/A N/A N/A N/A N/A NSE 10,000Aromatic Fraction Classes (ug/L)C9-C10 Volatile Aromatics BDL BDL 1380 BDL BDL NSE NSEC11-C22 Extractable Aromatics N/A N/A N/A N/A N/A NSE NSEC9-C22 Aromatics (total) BDL BDL1,380BDL BDLNSE 200N/A = Not AnalyzedBDL = Below Detection LimitsNSE = No Standard Established
TABLE 8 (Continued)SUMMARY OF GROUNDWATER ANALYTICAL RESULTSHANDY HOUSE 36724 HWY 70, NEWPORT, NC 28570Constituent MW-15 MW-16 MW-17 SW-1 SW-3 GCL 2L Standard Date8/28/2014 8/28/2014 8/28/2014 8/28/2014 8/28/2014 Method 6200B (ug/L)Benzene BDL BDL BDL BDL BDL 5,000 1Toluene BDL BDL BDL BDL BDL 260,000 600Ethylbenzene BDL 15.6 BDL BDL BDL 84,500 600Xylenes (total) BDL BDL BDL BDL BDL 85,500 500BTEX (total) 0 15.6 0 0 0 NSE NSEp-Isopropyltoluene BDL BDL BDL BDL BDL NSE NSEIsopropylbenzene BDL 4.8 BDL BDL BDL 25,000 70Diisopropyl Ether (DIPE) BDL BDL BDL BDL BDL 70,000 70Naphthalene BDL 4.3 BDL BDL BDL 6,000 6n-propylbenzene BDL 9.9 BDL BDL BDL 30,000 70n-butylbenzene BDL 1.1 BDL BDL BDL 6,900 70sec-butylbenzene BDL 0.93 BDL BDL BDL 8,500 70Methyl-tert-butyl-ether (MTBE) BDL BDL 1.1 BDL BDL 20,000 201,2,4-Trimethylbenzene BDL 0.74 BDL BDL BDL 28,500 4001,3,5-Trimethylbenzene BDL BDL BDL BDL BDL 25,000 400Methylene Chloride BDL BDL BDL BDL BDL 5,000 5Styrene BDL BDL BDL BDL BDL 70,000 70TOTAL 0 37.37 1.1 0 0 15,000 15Aliphatic Fraction Classes (ug/L) 8/28/2014 8/28/2014 8/28/2014 8/28/2014 8/28/2014C5-C8 Volatile Aliphatics BDL BDL BDL BDL BDL NSE 400C9-C12 Volatile Aliphatics 951 122 BDL BDL BDL NSE NSEC9-C18 Extractable Aliphatics N/A N/A N/A N/A N/A NSE 700C9-C18 Aliphatics (total)951122 BDL BDL BDL NSE 700C19-C36 Extractable Aliphatics N/A N/A N/A N/A N/A NSE 10,000Aromatic Fraction Classes (ug/L)C9-C10 Volatile Aromatics BDL BDL BDL BDL BDL NSE NSEC11-C22 Extractable Aromatics N/A N/A N/A N/A N/A NSE NSEC9-C22 Aromatics (total) BDL BDL BDL BDL BDLNSE 200N/A = Not AnalyzedBDL = Below Detection LimitsNSE = No Standard Established

APPENDIX A

LABORATORY ANALYTICAL RESULTS
#=CL#
March 30, 2020
LIMS USE: FR - HENRY NEMARGUT
LIMS OBJECT ID: 92470400
92470400
Project:
Pace Project No.:
RE:
Henry Nemargut
Henry Nemargut Engineering
2211 Chestnut Street
Wilmington, NC 28405
HANDY HOUSE 3
Dear Henry Nemargut:
Enclosed are the analytical results for sample(s) received by the laboratory on March 20, 2020. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
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[phone]
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REPORT OF LABORATORY ANALYSIS
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#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92470400
HANDY HOUSE 3
Lab ID Sample ID Matrix Date Collected Date Received
92470400001 MW-1 Water 03/18/20 08:20 03/20/20 09:57
92470400002 MW-2 Water 03/18/20 08:40 03/20/20 09:57
92470400003 MW-3 Water 03/18/20 09:05 03/20/20 09:57
92470400004 MW-8 Water 03/18/20 09:30 03/20/20 09:57
92470400005 MW-9 Water 03/18/20 09:55 03/20/20 09:57
92470400006 MW-10 Water 03/18/20 10:20 03/20/20 09:57
92470400007 MW-11 Water 03/18/20 10:45 03/20/20 09:57
92470400008 MW-14 Water 03/18/20 11:10 03/20/20 09:57
92470400009 MW-15 Water 03/18/20 11:30 03/20/20 09:57
92470400010 MW-17 Water 03/18/20 11:55 03/20/20 09:57
92470400011 VEW1 Water 03/18/20 12:30 03/20/20 09:57
92470400012 SW-3 Water 03/18/20 12:50 03/20/20 09:57
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 3 of 52
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92470400
HANDY HOUSE 3
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92470400001 MW-1 MADEP VPH 6 PANBMB
SM 6200B 63 PASI-CSAS
92470400002 MW-2 MADEP VPH 6 PANBMB
SM 6200B 63 PASI-CCL
92470400003 MW-3 MADEP VPH 6 PANBMB
SM 6200B 63 PASI-CSAS
92470400004 MW-8 MADEP VPH 6 PANBMB
SM 6200B 63 PASI-CCL
92470400005 MW-9 MADEP VPH 6 PANBMB
SM 6200B 63 PASI-CCL
92470400006 MW-10 MADEP VPH 6 PANJAH
SM 6200B 63 PASI-CSAS
92470400007 MW-11 MADEP VPH 6 PANJAH
SM 6200B 63 PASI-CCL
92470400008 MW-14 MADEP VPH 6 PANJAH
SM 6200B 63 PASI-CCL
92470400009 MW-15 MADEP VPH 6 PANJAH
SM 6200B 63 PASI-CCL
92470400010 MW-17 MADEP VPH 6 PANACG
SM 6200B 63 PASI-CCL
92470400011 VEW1 MADEP VPH 6 PANJAH
SM 6200B 63 PASI-CCL
92470400012 SW-3 MADEP VPH 6 PANJAH
SM 6200B 63 PASI-CCL
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 4 of 52
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92470400
HANDY HOUSE 3
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92470400001 MW-1
Aliphatic (C09-C12) 410 ug/L 03/25/20 19:08100MADEP VPH
Aromatic (C09-C10),Unadjusted 1040 ug/L 03/25/20 19:08100MADEP VPH
Total VPH 1450 ug/L 03/25/20 19:08100MADEP VPH
Isopropylbenzene (Cumene) 1.1 ug/L 03/26/20 09:310.50SM 6200B
1,2,3-Trichloropropane 2.5 ug/L 03/26/20 09:310.50SM 6200B
1,2,4-Trimethylbenzene 82.6 ug/L 03/26/20 09:310.50SM 6200B
1,3,5-Trimethylbenzene 86.2 ug/L 03/26/20 09:310.50SM 6200B
92470400002 MW-2
Aliphatic (C05-C08) 343 ug/L 03/25/20 19:40100MADEP VPH
Aliphatic (C09-C12) 135 ug/L 03/25/20 19:40100MADEP VPH
Aromatic (C09-C10),Unadjusted 258 ug/L 03/25/20 19:40100MADEP VPH
Total VPH 736 ug/L 03/25/20 19:40100MADEP VPH
sec-Butylbenzene 1.4 ug/L 03/25/20 21:140.50SM 6200B
Ethylbenzene 0.66 ug/L 03/25/20 21:140.50SM 6200B
Isopropylbenzene (Cumene) 0.56 ug/L 03/25/20 21:140.50SM 6200B
Naphthalene 2.7 ug/L 03/25/20 21:142.0SM 6200B
1,2,4-Trimethylbenzene 0.51 ug/L 03/25/20 21:140.50SM 6200B
92470400003 MW-3
Aliphatic (C09-C12) 3690 ug/L 03/25/20 20:121000MADEP VPH
Aromatic (C09-C10),Unadjusted 4360 ug/L 03/25/20 20:121000MADEP VPH
Total VPH 8500 ug/L 03/25/20 20:121000MADEP VPH
Ethylbenzene 338 ug/L 03/26/20 08:375.0SM 6200B
Isopropylbenzene (Cumene) 55.7 ug/L 03/26/20 08:375.0SM 6200B
Naphthalene 332 ug/L 03/26/20 08:3720.0SM 6200B
Toluene 7.9 ug/L 03/26/20 08:375.0SM 6200B
1,2,4-Trimethylbenzene 972 ug/L 03/26/20 08:375.0SM 6200B
m&p-Xylene 348 ug/L 03/26/20 08:3710.0SM 6200B
o-Xylene 386 ug/L 03/26/20 08:375.0SM 6200B
92470400006 MW-10
Aliphatic (C05-C08) 140 ug/L 03/26/20 15:25100MADEP VPH
Aliphatic (C09-C12) 1050 ug/L 03/26/20 15:25100MADEP VPH
Aromatic (C09-C10),Unadjusted 1970 ug/L 03/26/20 15:25100MADEP VPH
Total VPH 3160 ug/L 03/26/20 15:25100MADEP VPH
Naphthalene 34.9 ug/L 03/26/20 14:365.0SM 6200B
1,2,4-Trimethylbenzene 289 ug/L 03/26/20 14:361.2SM 6200B
m&p-Xylene 3.2 ug/L 03/26/20 14:362.5SM 6200B
o-Xylene 4.3 ug/L 03/26/20 14:361.2SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92470400
HANDY HOUSE 3
Sample: MW-1 Lab ID: 92470400001 Collected: 03/18/20 08:20 Received: 03/20/20 09:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: MADEP VPH Preparation Method: MADEPVMADEPV
Aliphatic (C05-C08) ND ug/L 03/25/20 19:0803/25/20 19:08100 1
Aliphatic (C09-C12)410 ug/L 03/25/20 19:0803/25/20 19:08100 1
Aromatic (C09-C10),Unadjusted 1040 ug/L 03/25/20 19:08 TPHC9C10A03/25/20 19:08100 1
Total VPH 1450 ug/L 03/25/20 19:08 VPH03/25/20 19:08100 1
Surrogates
2,5-Dibromotoluene (FID) 104 % 03/25/20 19:08 615-59-8FID03/25/20 19:0870.0-130 1
2,5-Dibromotoluene (PID) 102 % 03/25/20 19:08 615-59-8PID03/25/20 19:0870.0-130 1
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 03/26/20 09:31 71-43-20.50 1
Bromobenzene ND ug/L 03/26/20 09:31 108-86-10.50 1
Bromochloromethane ND ug/L 03/26/20 09:31 74-97-50.50 1
Bromodichloromethane ND ug/L 03/26/20 09:31 75-27-40.50 1
Bromoform ND ug/L 03/26/20 09:31 75-25-20.50 1
Bromomethane ND ug/L 03/26/20 09:31 74-83-95.0 1
n-Butylbenzene ND ug/L 03/26/20 09:31 104-51-80.50 1
sec-Butylbenzene ND ug/L 03/26/20 09:31 135-98-80.50 1
tert-Butylbenzene ND ug/L 03/26/20 09:31 98-06-60.50 1
Carbon tetrachloride ND ug/L 03/26/20 09:31 56-23-50.50 1
Chlorobenzene ND ug/L 03/26/20 09:31 108-90-70.50 1
Chloroethane ND ug/L 03/26/20 09:31 75-00-31.0 1
Chloroform ND ug/L 03/26/20 09:31 67-66-30.50 1
Chloromethane ND ug/L 03/26/20 09:31 74-87-31.0 1
2-Chlorotoluene ND ug/L 03/26/20 09:31 95-49-80.50 1
4-Chlorotoluene ND ug/L 03/26/20 09:31 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 03/26/20 09:31 96-12-81.0 1
Dibromochloromethane ND ug/L 03/26/20 09:31 124-48-10.50 1
1,2-Dibromoethane (EDB) ND ug/L 03/26/20 09:31 106-93-40.50 1
Dibromomethane ND ug/L 03/26/20 09:31 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 03/26/20 09:31 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 03/26/20 09:31 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 03/26/20 09:31 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 03/26/20 09:31 75-71-80.50 1
1,1-Dichloroethane ND ug/L 03/26/20 09:31 75-34-30.50 1
1,2-Dichloroethane ND ug/L 03/26/20 09:31 107-06-20.50 1
1,1-Dichloroethene ND ug/L 03/26/20 09:31 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 03/26/20 09:31 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 03/26/20 09:31 156-60-50.50 1
1,2-Dichloropropane ND ug/L 03/26/20 09:31 78-87-50.50 1
1,3-Dichloropropane ND ug/L 03/26/20 09:31 142-28-90.50 1
2,2-Dichloropropane ND ug/L 03/26/20 09:31 594-20-70.50 1
1,1-Dichloropropene ND ug/L 03/26/20 09:31 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 03/26/20 09:31 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 03/26/20 09:31 10061-02-60.50 1
Diisopropyl ether ND ug/L 03/26/20 09:31 108-20-30.50 1
Ethylbenzene ND ug/L 03/26/20 09:31 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 03/26/20 09:31 87-68-32.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/30/2020 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 6 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92470400
HANDY HOUSE 3
Sample: MW-1 Lab ID: 92470400001 Collected: 03/18/20 08:20 Received: 03/20/20 09:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B6200B MSV
Isopropylbenzene (Cumene)1.1 ug/L 03/26/20 09:31 98-82-80.50 1
Methylene Chloride ND ug/L 03/26/20 09:31 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 03/26/20 09:31 1634-04-40.50 1
Naphthalene ND ug/L 03/26/20 09:31 91-20-32.0 1
n-Propylbenzene ND ug/L 03/26/20 09:31 103-65-10.50 1
Styrene ND ug/L 03/26/20 09:31 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 03/26/20 09:31 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 03/26/20 09:31 79-34-50.50 1
Tetrachloroethene ND ug/L 03/26/20 09:31 127-18-40.50 1
Toluene ND ug/L 03/26/20 09:31 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 03/26/20 09:31 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 03/26/20 09:31 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 03/26/20 09:31 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 03/26/20 09:31 79-00-50.50 1
Trichloroethene ND ug/L 03/26/20 09:31 79-01-60.50 1
Trichlorofluoromethane ND ug/L 03/26/20 09:31 75-69-41.0 1
1,2,3-Trichloropropane 2.5 ug/L 03/26/20 09:31 96-18-40.50 1
1,2,4-Trimethylbenzene 82.6 ug/L 03/26/20 09:31 95-63-60.50 1
1,3,5-Trimethylbenzene 86.2 ug/L 03/26/20 09:31 108-67-80.50 1
Vinyl chloride ND ug/L 03/26/20 09:31 75-01-41.0 1
m&p-Xylene ND ug/L 03/26/20 09:31 179601-23-11.0 1
o-Xylene ND ug/L 03/26/20 09:31 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S) 99 % 03/26/20 09:31 17060-07-070-130 1
4-Bromofluorobenzene (S) 102 % 03/26/20 09:31 460-00-470-130 1
Toluene-d8 (S) 103 % 03/26/20 09:31 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/30/2020 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92470400
HANDY HOUSE 3
Sample: MW-2 Lab ID: 92470400002 Collected: 03/18/20 08:40 Received: 03/20/20 09:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: MADEP VPH Preparation Method: MADEPVMADEPV
Aliphatic (C05-C08)343 ug/L 03/25/20 19:4003/25/20 19:40100 1
Aliphatic (C09-C12)135 ug/L 03/25/20 19:4003/25/20 19:40100 1
Aromatic (C09-C10),Unadjusted 258 ug/L 03/25/20 19:40 TPHC9C10A03/25/20 19:40100 1
Total VPH 736 ug/L 03/25/20 19:40 VPH03/25/20 19:40100 1
Surrogates
2,5-Dibromotoluene (FID) 105 % 03/25/20 19:40 615-59-8FID03/25/20 19:4070.0-130 1
2,5-Dibromotoluene (PID) 101 % 03/25/20 19:40 615-59-8PID03/25/20 19:4070.0-130 1
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 03/25/20 21:14 71-43-20.50 1
Bromobenzene ND ug/L 03/25/20 21:14 108-86-10.50 1
Bromochloromethane ND ug/L 03/25/20 21:14 74-97-50.50 1
Bromodichloromethane ND ug/L 03/25/20 21:14 75-27-40.50 1
Bromoform ND ug/L 03/25/20 21:14 75-25-20.50 1
Bromomethane ND ug/L 03/25/20 21:14 74-83-95.0 1
n-Butylbenzene ND ug/L 03/25/20 21:14 104-51-80.50 1
sec-Butylbenzene 1.4 ug/L 03/25/20 21:14 135-98-80.50 1
tert-Butylbenzene ND ug/L 03/25/20 21:14 98-06-60.50 1
Carbon tetrachloride ND ug/L 03/25/20 21:14 56-23-50.50 1
Chlorobenzene ND ug/L 03/25/20 21:14 108-90-70.50 1
Chloroethane ND ug/L 03/25/20 21:14 75-00-31.0 1
Chloroform ND ug/L 03/25/20 21:14 67-66-30.50 1
Chloromethane ND ug/L 03/25/20 21:14 74-87-31.0 1
2-Chlorotoluene ND ug/L 03/25/20 21:14 95-49-80.50 1
4-Chlorotoluene ND ug/L 03/25/20 21:14 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 03/25/20 21:14 96-12-81.0 1
Dibromochloromethane ND ug/L 03/25/20 21:14 124-48-10.50 1
1,2-Dibromoethane (EDB) ND ug/L 03/25/20 21:14 106-93-40.50 1
Dibromomethane ND ug/L 03/25/20 21:14 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 03/25/20 21:14 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 03/25/20 21:14 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 03/25/20 21:14 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 03/25/20 21:14 75-71-80.50 1
1,1-Dichloroethane ND ug/L 03/25/20 21:14 75-34-30.50 1
1,2-Dichloroethane ND ug/L 03/25/20 21:14 107-06-20.50 1
1,1-Dichloroethene ND ug/L 03/25/20 21:14 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 03/25/20 21:14 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 03/25/20 21:14 156-60-50.50 1
1,2-Dichloropropane ND ug/L 03/25/20 21:14 78-87-50.50 1
1,3-Dichloropropane ND ug/L 03/25/20 21:14 142-28-90.50 1
2,2-Dichloropropane ND ug/L 03/25/20 21:14 594-20-70.50 1
1,1-Dichloropropene ND ug/L 03/25/20 21:14 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 03/25/20 21:14 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 03/25/20 21:14 10061-02-60.50 1
Diisopropyl ether ND ug/L 03/25/20 21:14 108-20-30.50 1
Ethylbenzene 0.66 ug/L 03/25/20 21:14 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 03/25/20 21:14 87-68-32.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/30/2020 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92470400
HANDY HOUSE 3
Sample: MW-2 Lab ID: 92470400002 Collected: 03/18/20 08:40 Received: 03/20/20 09:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B6200B MSV
Isopropylbenzene (Cumene)0.56 ug/L 03/25/20 21:14 98-82-80.50 1
Methylene Chloride ND ug/L 03/25/20 21:14 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 03/25/20 21:14 1634-04-40.50 1
Naphthalene 2.7 ug/L 03/25/20 21:14 91-20-32.0 1
n-Propylbenzene ND ug/L 03/25/20 21:14 103-65-10.50 1
Styrene ND ug/L 03/25/20 21:14 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 03/25/20 21:14 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 03/25/20 21:14 79-34-50.50 1
Tetrachloroethene ND ug/L 03/25/20 21:14 127-18-40.50 1
Toluene ND ug/L 03/25/20 21:14 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 03/25/20 21:14 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 03/25/20 21:14 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 03/25/20 21:14 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 03/25/20 21:14 79-00-50.50 1
Trichloroethene ND ug/L 03/25/20 21:14 79-01-60.50 1
Trichlorofluoromethane ND ug/L 03/25/20 21:14 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 03/25/20 21:14 96-18-40.50 1
1,2,4-Trimethylbenzene 0.51 ug/L 03/25/20 21:14 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 03/25/20 21:14 108-67-80.50 1
Vinyl chloride ND ug/L 03/25/20 21:14 75-01-41.0 1
m&p-Xylene ND ug/L 03/25/20 21:14 179601-23-11.0 1
o-Xylene ND ug/L 03/25/20 21:14 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S) 99 % 03/25/20 21:14 17060-07-070-130 1
4-Bromofluorobenzene (S) 99 % 03/25/20 21:14 460-00-470-130 1
Toluene-d8 (S) 100 % 03/25/20 21:14 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/30/2020 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92470400
HANDY HOUSE 3
Sample: MW-3 Lab ID: 92470400003 Collected: 03/18/20 09:05 Received: 03/20/20 09:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: MADEP VPH Preparation Method: MADEPVMADEPV
Aliphatic (C05-C08) ND ug/L 03/25/20 20:1203/25/20 20:121000 10
Aliphatic (C09-C12)3690 ug/L 03/25/20 20:1203/25/20 20:121000 10
Aromatic (C09-C10),Unadjusted 4360 ug/L 03/25/20 20:12 TPHC9C10A03/25/20 20:121000 10
Total VPH 8500 ug/L 03/25/20 20:12 VPH03/25/20 20:121000 10
Surrogates
2,5-Dibromotoluene (FID) 100 % 03/25/20 20:12 615-59-8FID03/25/20 20:1270.0-130 10
2,5-Dibromotoluene (PID) 99.0 % 03/25/20 20:12 615-59-8PID03/25/20 20:1270.0-130 10
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 03/26/20 08:37 71-43-25.0 10
Bromobenzene ND ug/L 03/26/20 08:37 108-86-15.0 10
Bromochloromethane ND ug/L 03/26/20 08:37 74-97-55.0 10
Bromodichloromethane ND ug/L 03/26/20 08:37 75-27-45.0 10
Bromoform ND ug/L 03/26/20 08:37 75-25-25.0 10
Bromomethane ND ug/L 03/26/20 08:37 74-83-950.0 10
n-Butylbenzene ND ug/L 03/26/20 08:37 104-51-85.0 10
sec-Butylbenzene ND ug/L 03/26/20 08:37 135-98-85.0 10
tert-Butylbenzene ND ug/L 03/26/20 08:37 98-06-65.0 10
Carbon tetrachloride ND ug/L 03/26/20 08:37 56-23-55.0 10
Chlorobenzene ND ug/L 03/26/20 08:37 108-90-75.0 10
Chloroethane ND ug/L 03/26/20 08:37 75-00-310.0 10
Chloroform ND ug/L 03/26/20 08:37 67-66-35.0 10
Chloromethane ND ug/L 03/26/20 08:37 74-87-310.0 10
2-Chlorotoluene ND ug/L 03/26/20 08:37 95-49-8 M15.0 10
4-Chlorotoluene ND ug/L 03/26/20 08:37 106-43-45.0 10
1,2-Dibromo-3-chloropropane ND ug/L 03/26/20 08:37 96-12-810.0 10
Dibromochloromethane ND ug/L 03/26/20 08:37 124-48-15.0 10
1,2-Dibromoethane (EDB) ND ug/L 03/26/20 08:37 106-93-45.0 10
Dibromomethane ND ug/L 03/26/20 08:37 74-95-35.0 10
1,2-Dichlorobenzene ND ug/L 03/26/20 08:37 95-50-15.0 10
1,3-Dichlorobenzene ND ug/L 03/26/20 08:37 541-73-15.0 10
1,4-Dichlorobenzene ND ug/L 03/26/20 08:37 106-46-75.0 10
Dichlorodifluoromethane ND ug/L 03/26/20 08:37 75-71-85.0 10
1,1-Dichloroethane ND ug/L 03/26/20 08:37 75-34-35.0 10
1,2-Dichloroethane ND ug/L 03/26/20 08:37 107-06-25.0 10
1,1-Dichloroethene ND ug/L 03/26/20 08:37 75-35-45.0 10
cis-1,2-Dichloroethene ND ug/L 03/26/20 08:37 156-59-25.0 10
trans-1,2-Dichloroethene ND ug/L 03/26/20 08:37 156-60-55.0 10
1,2-Dichloropropane ND ug/L 03/26/20 08:37 78-87-55.0 10
1,3-Dichloropropane ND ug/L 03/26/20 08:37 142-28-95.0 10
2,2-Dichloropropane ND ug/L 03/26/20 08:37 594-20-75.0 10
1,1-Dichloropropene ND ug/L 03/26/20 08:37 563-58-65.0 10
cis-1,3-Dichloropropene ND ug/L 03/26/20 08:37 10061-01-55.0 10
trans-1,3-Dichloropropene ND ug/L 03/26/20 08:37 10061-02-65.0 10
Diisopropyl ether ND ug/L 03/26/20 08:37 108-20-35.0 10
Ethylbenzene 338 ug/L 03/26/20 08:37 100-41-45.0 10
Hexachloro-1,3-butadiene ND ug/L 03/26/20 08:37 87-68-320.0 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/30/2020 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92470400
HANDY HOUSE 3
Sample: MW-3 Lab ID: 92470400003 Collected: 03/18/20 09:05 Received: 03/20/20 09:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B6200B MSV
Isopropylbenzene (Cumene)55.7 ug/L 03/26/20 08:37 98-82-85.0 10
Methylene Chloride ND ug/L 03/26/20 08:37 75-09-220.0 10
Methyl-tert-butyl ether ND ug/L 03/26/20 08:37 1634-04-45.0 10
Naphthalene 332 ug/L 03/26/20 08:37 91-20-320.0 10
n-Propylbenzene ND ug/L 03/26/20 08:37 103-65-1 M15.0 10
Styrene ND ug/L 03/26/20 08:37 100-42-55.0 10
1,1,1,2-Tetrachloroethane ND ug/L 03/26/20 08:37 630-20-65.0 10
1,1,2,2-Tetrachloroethane ND ug/L 03/26/20 08:37 79-34-55.0 10
Tetrachloroethene ND ug/L 03/26/20 08:37 127-18-45.0 10
Toluene 7.9 ug/L 03/26/20 08:37 108-88-35.0 10
1,2,3-Trichlorobenzene ND ug/L 03/26/20 08:37 87-61-620.0 10
1,2,4-Trichlorobenzene ND ug/L 03/26/20 08:37 120-82-120.0 10
1,1,1-Trichloroethane ND ug/L 03/26/20 08:37 71-55-65.0 10
1,1,2-Trichloroethane ND ug/L 03/26/20 08:37 79-00-55.0 10
Trichloroethene ND ug/L 03/26/20 08:37 79-01-65.0 10
Trichlorofluoromethane ND ug/L 03/26/20 08:37 75-69-410.0 10
1,2,3-Trichloropropane ND ug/L 03/26/20 08:37 96-18-45.0 10
1,2,4-Trimethylbenzene 972 ug/L 03/26/20 08:37 95-63-65.0 10
1,3,5-Trimethylbenzene ND ug/L 03/26/20 08:37 108-67-8 M15.0 10
Vinyl chloride ND ug/L 03/26/20 08:37 75-01-410.0 10
m&p-Xylene 348 ug/L 03/26/20 08:37 179601-23-110.0 10
o-Xylene 386 ug/L 03/26/20 08:37 95-47-65.0 10
Surrogates
1,2-Dichloroethane-d4 (S) 99 % 03/26/20 08:37 17060-07-070-130 10
4-Bromofluorobenzene (S) 103 % 03/26/20 08:37 460-00-470-130 10
Toluene-d8 (S) 102 % 03/26/20 08:37 2037-26-570-130 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/30/2020 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92470400
HANDY HOUSE 3
Sample: MW-8 Lab ID: 92470400004 Collected: 03/18/20 09:30 Received: 03/20/20 09:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: MADEP VPH Preparation Method: MADEPVMADEPV
Aliphatic (C05-C08) ND ug/L 03/25/20 21:1603/25/20 21:16100 1
Aliphatic (C09-C12) ND ug/L 03/25/20 21:1603/25/20 21:16100 1
Aromatic (C09-C10),Unadjusted ND ug/L 03/25/20 21:16 TPHC9C10A03/25/20 21:16100 1
Total VPH ND ug/L 03/25/20 21:16 VPH03/25/20 21:16100 1
Surrogates
2,5-Dibromotoluene (FID) 98.0 % 03/25/20 21:16 615-59-8FID03/25/20 21:1670.0-130 1
2,5-Dibromotoluene (PID) 96.6 % 03/25/20 21:16 615-59-8PID03/25/20 21:1670.0-130 1
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 03/25/20 21:33 71-43-20.50 1
Bromobenzene ND ug/L 03/25/20 21:33 108-86-10.50 1
Bromochloromethane ND ug/L 03/25/20 21:33 74-97-50.50 1
Bromodichloromethane ND ug/L 03/25/20 21:33 75-27-40.50 1
Bromoform ND ug/L 03/25/20 21:33 75-25-20.50 1
Bromomethane ND ug/L 03/25/20 21:33 74-83-95.0 1
n-Butylbenzene ND ug/L 03/25/20 21:33 104-51-80.50 1
sec-Butylbenzene ND ug/L 03/25/20 21:33 135-98-80.50 1
tert-Butylbenzene ND ug/L 03/25/20 21:33 98-06-60.50 1
Carbon tetrachloride ND ug/L 03/25/20 21:33 56-23-50.50 1
Chlorobenzene ND ug/L 03/25/20 21:33 108-90-70.50 1
Chloroethane ND ug/L 03/25/20 21:33 75-00-31.0 1
Chloroform ND ug/L 03/25/20 21:33 67-66-30.50 1
Chloromethane ND ug/L 03/25/20 21:33 74-87-31.0 1
2-Chlorotoluene ND ug/L 03/25/20 21:33 95-49-80.50 1
4-Chlorotoluene ND ug/L 03/25/20 21:33 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 03/25/20 21:33 96-12-81.0 1
Dibromochloromethane ND ug/L 03/25/20 21:33 124-48-10.50 1
1,2-Dibromoethane (EDB) ND ug/L 03/25/20 21:33 106-93-40.50 1
Dibromomethane ND ug/L 03/25/20 21:33 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 03/25/20 21:33 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 03/25/20 21:33 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 03/25/20 21:33 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 03/25/20 21:33 75-71-80.50 1
1,1-Dichloroethane ND ug/L 03/25/20 21:33 75-34-30.50 1
1,2-Dichloroethane ND ug/L 03/25/20 21:33 107-06-20.50 1
1,1-Dichloroethene ND ug/L 03/25/20 21:33 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 03/25/20 21:33 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 03/25/20 21:33 156-60-50.50 1
1,2-Dichloropropane ND ug/L 03/25/20 21:33 78-87-50.50 1
1,3-Dichloropropane ND ug/L 03/25/20 21:33 142-28-90.50 1
2,2-Dichloropropane ND ug/L 03/25/20 21:33 594-20-70.50 1
1,1-Dichloropropene ND ug/L 03/25/20 21:33 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 03/25/20 21:33 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 03/25/20 21:33 10061-02-60.50 1
Diisopropyl ether ND ug/L 03/25/20 21:33 108-20-30.50 1
Ethylbenzene ND ug/L 03/25/20 21:33 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 03/25/20 21:33 87-68-32.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/30/2020 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92470400
HANDY HOUSE 3
Sample: MW-8 Lab ID: 92470400004 Collected: 03/18/20 09:30 Received: 03/20/20 09:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B6200B MSV
Isopropylbenzene (Cumene) ND ug/L 03/25/20 21:33 98-82-80.50 1
Methylene Chloride ND ug/L 03/25/20 21:33 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 03/25/20 21:33 1634-04-40.50 1
Naphthalene ND ug/L 03/25/20 21:33 91-20-32.0 1
n-Propylbenzene ND ug/L 03/25/20 21:33 103-65-10.50 1
Styrene ND ug/L 03/25/20 21:33 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 03/25/20 21:33 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 03/25/20 21:33 79-34-50.50 1
Tetrachloroethene ND ug/L 03/25/20 21:33 127-18-40.50 1
Toluene ND ug/L 03/25/20 21:33 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 03/25/20 21:33 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 03/25/20 21:33 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 03/25/20 21:33 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 03/25/20 21:33 79-00-50.50 1
Trichloroethene ND ug/L 03/25/20 21:33 79-01-60.50 1
Trichlorofluoromethane ND ug/L 03/25/20 21:33 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 03/25/20 21:33 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 03/25/20 21:33 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 03/25/20 21:33 108-67-80.50 1
Vinyl chloride ND ug/L 03/25/20 21:33 75-01-41.0 1
m&p-Xylene ND ug/L 03/25/20 21:33 179601-23-11.0 1
o-Xylene ND ug/L 03/25/20 21:33 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S) 99 % 03/25/20 21:33 17060-07-070-130 1
4-Bromofluorobenzene (S) 103 % 03/25/20 21:33 460-00-470-130 1
Toluene-d8 (S) 104 % 03/25/20 21:33 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/30/2020 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92470400
HANDY HOUSE 3
Sample: MW-9 Lab ID: 92470400005 Collected: 03/18/20 09:55 Received: 03/20/20 09:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: MADEP VPH Preparation Method: MADEPVMADEPV
Aliphatic (C05-C08) ND ug/L 03/25/20 21:4803/25/20 21:48100 1
Aliphatic (C09-C12) ND ug/L 03/25/20 21:4803/25/20 21:48100 1
Aromatic (C09-C10),Unadjusted ND ug/L 03/25/20 21:48 TPHC9C10A03/25/20 21:48100 1
Total VPH ND ug/L 03/25/20 21:48 VPH03/25/20 21:48100 1
Surrogates
2,5-Dibromotoluene (FID) 95.8 % 03/25/20 21:48 615-59-8FID03/25/20 21:4870.0-130 1
2,5-Dibromotoluene (PID) 97.5 % 03/25/20 21:48 615-59-8PID03/25/20 21:4870.0-130 1
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 03/25/20 21:51 71-43-20.50 1
Bromobenzene ND ug/L 03/25/20 21:51 108-86-10.50 1
Bromochloromethane ND ug/L 03/25/20 21:51 74-97-50.50 1
Bromodichloromethane ND ug/L 03/25/20 21:51 75-27-40.50 1
Bromoform ND ug/L 03/25/20 21:51 75-25-20.50 1
Bromomethane ND ug/L 03/25/20 21:51 74-83-95.0 1
n-Butylbenzene ND ug/L 03/25/20 21:51 104-51-80.50 1
sec-Butylbenzene ND ug/L 03/25/20 21:51 135-98-80.50 1
tert-Butylbenzene ND ug/L 03/25/20 21:51 98-06-60.50 1
Carbon tetrachloride ND ug/L 03/25/20 21:51 56-23-50.50 1
Chlorobenzene ND ug/L 03/25/20 21:51 108-90-70.50 1
Chloroethane ND ug/L 03/25/20 21:51 75-00-31.0 1
Chloroform ND ug/L 03/25/20 21:51 67-66-30.50 1
Chloromethane ND ug/L 03/25/20 21:51 74-87-31.0 1
2-Chlorotoluene ND ug/L 03/25/20 21:51 95-49-80.50 1
4-Chlorotoluene ND ug/L 03/25/20 21:51 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 03/25/20 21:51 96-12-81.0 1
Dibromochloromethane ND ug/L 03/25/20 21:51 124-48-10.50 1
1,2-Dibromoethane (EDB) ND ug/L 03/25/20 21:51 106-93-40.50 1
Dibromomethane ND ug/L 03/25/20 21:51 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 03/25/20 21:51 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 03/25/20 21:51 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 03/25/20 21:51 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 03/25/20 21:51 75-71-80.50 1
1,1-Dichloroethane ND ug/L 03/25/20 21:51 75-34-30.50 1
1,2-Dichloroethane ND ug/L 03/25/20 21:51 107-06-20.50 1
1,1-Dichloroethene ND ug/L 03/25/20 21:51 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 03/25/20 21:51 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 03/25/20 21:51 156-60-50.50 1
1,2-Dichloropropane ND ug/L 03/25/20 21:51 78-87-50.50 1
1,3-Dichloropropane ND ug/L 03/25/20 21:51 142-28-90.50 1
2,2-Dichloropropane ND ug/L 03/25/20 21:51 594-20-70.50 1
1,1-Dichloropropene ND ug/L 03/25/20 21:51 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 03/25/20 21:51 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 03/25/20 21:51 10061-02-60.50 1
Diisopropyl ether ND ug/L 03/25/20 21:51 108-20-30.50 1
Ethylbenzene ND ug/L 03/25/20 21:51 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 03/25/20 21:51 87-68-32.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/30/2020 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92470400
HANDY HOUSE 3
Sample: MW-9 Lab ID: 92470400005 Collected: 03/18/20 09:55 Received: 03/20/20 09:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B6200B MSV
Isopropylbenzene (Cumene) ND ug/L 03/25/20 21:51 98-82-80.50 1
Methylene Chloride ND ug/L 03/25/20 21:51 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 03/25/20 21:51 1634-04-40.50 1
Naphthalene ND ug/L 03/25/20 21:51 91-20-32.0 1
n-Propylbenzene ND ug/L 03/25/20 21:51 103-65-10.50 1
Styrene ND ug/L 03/25/20 21:51 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 03/25/20 21:51 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 03/25/20 21:51 79-34-50.50 1
Tetrachloroethene ND ug/L 03/25/20 21:51 127-18-40.50 1
Toluene ND ug/L 03/25/20 21:51 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 03/25/20 21:51 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 03/25/20 21:51 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 03/25/20 21:51 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 03/25/20 21:51 79-00-50.50 1
Trichloroethene ND ug/L 03/25/20 21:51 79-01-60.50 1
Trichlorofluoromethane ND ug/L 03/25/20 21:51 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 03/25/20 21:51 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 03/25/20 21:51 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 03/25/20 21:51 108-67-80.50 1
Vinyl chloride ND ug/L 03/25/20 21:51 75-01-41.0 1
m&p-Xylene ND ug/L 03/25/20 21:51 179601-23-11.0 1
o-Xylene ND ug/L 03/25/20 21:51 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S) 98 % 03/25/20 21:51 17060-07-070-130 1
4-Bromofluorobenzene (S) 101 % 03/25/20 21:51 460-00-470-130 1
Toluene-d8 (S) 102 % 03/25/20 21:51 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/30/2020 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92470400
HANDY HOUSE 3
Sample: MW-10 Lab ID: 92470400006 Collected: 03/18/20 10:20 Received: 03/20/20 09:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: MADEP VPH Preparation Method: MADEPVMADEPV
Aliphatic (C05-C08)140 ug/L 03/26/20 15:2503/26/20 15:25100 1
Aliphatic (C09-C12)1050 ug/L 03/26/20 15:2503/26/20 15:25100 1
Aromatic (C09-C10),Unadjusted 1970 ug/L 03/26/20 15:25 TPHC9C10A03/26/20 15:25100 1
Total VPH 3160 ug/L 03/26/20 15:25 VPH03/26/20 15:25100 1
Surrogates
2,5-Dibromotoluene (FID) 103 % 03/26/20 15:25 615-59-8FID03/26/20 15:2570.0-130 1
2,5-Dibromotoluene (PID) 99.9 % 03/26/20 15:25 615-59-8PID03/26/20 15:2570.0-130 1
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 03/26/20 14:36 71-43-21.2 2.5
Bromobenzene ND ug/L 03/26/20 14:36 108-86-11.2 2.5
Bromochloromethane ND ug/L 03/26/20 14:36 74-97-51.2 2.5
Bromodichloromethane ND ug/L 03/26/20 14:36 75-27-41.2 2.5
Bromoform ND ug/L 03/26/20 14:36 75-25-21.2 2.5
Bromomethane ND ug/L 03/26/20 14:36 74-83-912.5 2.5
n-Butylbenzene ND ug/L 03/26/20 14:36 104-51-81.2 2.5
sec-Butylbenzene ND ug/L 03/26/20 14:36 135-98-81.2 2.5
tert-Butylbenzene ND ug/L 03/26/20 14:36 98-06-61.2 2.5
Carbon tetrachloride ND ug/L 03/26/20 14:36 56-23-51.2 2.5
Chlorobenzene ND ug/L 03/26/20 14:36 108-90-71.2 2.5
Chloroethane ND ug/L 03/26/20 14:36 75-00-32.5 2.5
Chloroform ND ug/L 03/26/20 14:36 67-66-31.2 2.5
Chloromethane ND ug/L 03/26/20 14:36 74-87-32.5 2.5
2-Chlorotoluene ND ug/L 03/26/20 14:36 95-49-81.2 2.5
4-Chlorotoluene ND ug/L 03/26/20 14:36 106-43-41.2 2.5
1,2-Dibromo-3-chloropropane ND ug/L 03/26/20 14:36 96-12-82.5 2.5
Dibromochloromethane ND ug/L 03/26/20 14:36 124-48-11.2 2.5
1,2-Dibromoethane (EDB) ND ug/L 03/26/20 14:36 106-93-41.2 2.5
Dibromomethane ND ug/L 03/26/20 14:36 74-95-31.2 2.5
1,2-Dichlorobenzene ND ug/L 03/26/20 14:36 95-50-11.2 2.5
1,3-Dichlorobenzene ND ug/L 03/26/20 14:36 541-73-11.2 2.5
1,4-Dichlorobenzene ND ug/L 03/26/20 14:36 106-46-71.2 2.5
Dichlorodifluoromethane ND ug/L 03/26/20 14:36 75-71-81.2 2.5
1,1-Dichloroethane ND ug/L 03/26/20 14:36 75-34-31.2 2.5
1,2-Dichloroethane ND ug/L 03/26/20 14:36 107-06-21.2 2.5
1,1-Dichloroethene ND ug/L 03/26/20 14:36 75-35-41.2 2.5
cis-1,2-Dichloroethene ND ug/L 03/26/20 14:36 156-59-21.2 2.5
trans-1,2-Dichloroethene ND ug/L 03/26/20 14:36 156-60-51.2 2.5
1,2-Dichloropropane ND ug/L 03/26/20 14:36 78-87-51.2 2.5
1,3-Dichloropropane ND ug/L 03/26/20 14:36 142-28-91.2 2.5
2,2-Dichloropropane ND ug/L 03/26/20 14:36 594-20-71.2 2.5
1,1-Dichloropropene ND ug/L 03/26/20 14:36 563-58-61.2 2.5
cis-1,3-Dichloropropene ND ug/L 03/26/20 14:36 10061-01-51.2 2.5
trans-1,3-Dichloropropene ND ug/L 03/26/20 14:36 10061-02-61.2 2.5
Diisopropyl ether ND ug/L 03/26/20 14:36 108-20-31.2 2.5
Ethylbenzene ND ug/L 03/26/20 14:36 100-41-41.2 2.5
Hexachloro-1,3-butadiene ND ug/L 03/26/20 14:36 87-68-35.0 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/30/2020 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92470400
HANDY HOUSE 3
Sample: MW-10 Lab ID: 92470400006 Collected: 03/18/20 10:20 Received: 03/20/20 09:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B6200B MSV
Isopropylbenzene (Cumene) ND ug/L 03/26/20 14:36 98-82-81.2 2.5
Methylene Chloride ND ug/L 03/26/20 14:36 75-09-25.0 2.5
Methyl-tert-butyl ether ND ug/L 03/26/20 14:36 1634-04-41.2 2.5
Naphthalene 34.9 ug/L 03/26/20 14:36 91-20-35.0 2.5
n-Propylbenzene ND ug/L 03/26/20 14:36 103-65-11.2 2.5
Styrene ND ug/L 03/26/20 14:36 100-42-51.2 2.5
1,1,1,2-Tetrachloroethane ND ug/L 03/26/20 14:36 630-20-61.2 2.5
1,1,2,2-Tetrachloroethane ND ug/L 03/26/20 14:36 79-34-51.2 2.5
Tetrachloroethene ND ug/L 03/26/20 14:36 127-18-41.2 2.5
Toluene ND ug/L 03/26/20 14:36 108-88-31.2 2.5
1,2,3-Trichlorobenzene ND ug/L 03/26/20 14:36 87-61-65.0 2.5
1,2,4-Trichlorobenzene ND ug/L 03/26/20 14:36 120-82-15.0 2.5
1,1,1-Trichloroethane ND ug/L 03/26/20 14:36 71-55-61.2 2.5
1,1,2-Trichloroethane ND ug/L 03/26/20 14:36 79-00-51.2 2.5
Trichloroethene ND ug/L 03/26/20 14:36 79-01-61.2 2.5
Trichlorofluoromethane ND ug/L 03/26/20 14:36 75-69-42.5 2.5
1,2,3-Trichloropropane ND ug/L 03/26/20 14:36 96-18-41.2 2.5
1,2,4-Trimethylbenzene 289 ug/L 03/26/20 14:36 95-63-61.2 2.5
1,3,5-Trimethylbenzene ND ug/L 03/26/20 14:36 108-67-81.2 2.5
Vinyl chloride ND ug/L 03/26/20 14:36 75-01-42.5 2.5
m&p-Xylene 3.2 ug/L 03/26/20 14:36 179601-23-12.5 2.5
o-Xylene 4.3 ug/L 03/26/20 14:36 95-47-61.2 2.5
Surrogates
1,2-Dichloroethane-d4 (S) 98 % 03/26/20 14:36 17060-07-070-130 2.5
4-Bromofluorobenzene (S) 101 % 03/26/20 14:36 460-00-470-130 2.5
Toluene-d8 (S) 105 % 03/26/20 14:36 2037-26-570-130 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/30/2020 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92470400
HANDY HOUSE 3
Sample: MW-11 Lab ID: 92470400007 Collected: 03/18/20 10:45 Received: 03/20/20 09:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: MADEP VPH Preparation Method: MADEPVMADEPV
Aliphatic (C05-C08) ND ug/L 03/26/20 16:0303/26/20 16:03100 1
Aliphatic (C09-C12) ND ug/L 03/26/20 16:0303/26/20 16:03100 1
Aromatic (C09-C10),Unadjusted ND ug/L 03/26/20 16:03 TPHC9C10A03/26/20 16:03100 1
Total VPH ND ug/L 03/26/20 16:03 VPH03/26/20 16:03100 1
Surrogates
2,5-Dibromotoluene (FID) 93.7 % 03/26/20 16:03 615-59-8FID03/26/20 16:0370.0-130 1
2,5-Dibromotoluene (PID) 92.4 % 03/26/20 16:03 615-59-8PID03/26/20 16:0370.0-130 1
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 03/25/20 22:08 71-43-20.50 1
Bromobenzene ND ug/L 03/25/20 22:08 108-86-10.50 1
Bromochloromethane ND ug/L 03/25/20 22:08 74-97-50.50 1
Bromodichloromethane ND ug/L 03/25/20 22:08 75-27-40.50 1
Bromoform ND ug/L 03/25/20 22:08 75-25-20.50 1
Bromomethane ND ug/L 03/25/20 22:08 74-83-95.0 1
n-Butylbenzene ND ug/L 03/25/20 22:08 104-51-80.50 1
sec-Butylbenzene ND ug/L 03/25/20 22:08 135-98-80.50 1
tert-Butylbenzene ND ug/L 03/25/20 22:08 98-06-60.50 1
Carbon tetrachloride ND ug/L 03/25/20 22:08 56-23-50.50 1
Chlorobenzene ND ug/L 03/25/20 22:08 108-90-70.50 1
Chloroethane ND ug/L 03/25/20 22:08 75-00-31.0 1
Chloroform ND ug/L 03/25/20 22:08 67-66-30.50 1
Chloromethane ND ug/L 03/25/20 22:08 74-87-31.0 1
2-Chlorotoluene ND ug/L 03/25/20 22:08 95-49-80.50 1
4-Chlorotoluene ND ug/L 03/25/20 22:08 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 03/25/20 22:08 96-12-81.0 1
Dibromochloromethane ND ug/L 03/25/20 22:08 124-48-10.50 1
1,2-Dibromoethane (EDB) ND ug/L 03/25/20 22:08 106-93-40.50 1
Dibromomethane ND ug/L 03/25/20 22:08 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 03/25/20 22:08 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 03/25/20 22:08 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 03/25/20 22:08 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 03/25/20 22:08 75-71-80.50 1
1,1-Dichloroethane ND ug/L 03/25/20 22:08 75-34-30.50 1
1,2-Dichloroethane ND ug/L 03/25/20 22:08 107-06-20.50 1
1,1-Dichloroethene ND ug/L 03/25/20 22:08 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 03/25/20 22:08 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 03/25/20 22:08 156-60-50.50 1
1,2-Dichloropropane ND ug/L 03/25/20 22:08 78-87-50.50 1
1,3-Dichloropropane ND ug/L 03/25/20 22:08 142-28-90.50 1
2,2-Dichloropropane ND ug/L 03/25/20 22:08 594-20-70.50 1
1,1-Dichloropropene ND ug/L 03/25/20 22:08 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 03/25/20 22:08 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 03/25/20 22:08 10061-02-60.50 1
Diisopropyl ether ND ug/L 03/25/20 22:08 108-20-30.50 1
Ethylbenzene ND ug/L 03/25/20 22:08 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 03/25/20 22:08 87-68-32.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/30/2020 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92470400
HANDY HOUSE 3
Sample: MW-11 Lab ID: 92470400007 Collected: 03/18/20 10:45 Received: 03/20/20 09:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B6200B MSV
Isopropylbenzene (Cumene) ND ug/L 03/25/20 22:08 98-82-80.50 1
Methylene Chloride ND ug/L 03/25/20 22:08 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 03/25/20 22:08 1634-04-40.50 1
Naphthalene ND ug/L 03/25/20 22:08 91-20-32.0 1
n-Propylbenzene ND ug/L 03/25/20 22:08 103-65-10.50 1
Styrene ND ug/L 03/25/20 22:08 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 03/25/20 22:08 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 03/25/20 22:08 79-34-50.50 1
Tetrachloroethene ND ug/L 03/25/20 22:08 127-18-40.50 1
Toluene ND ug/L 03/25/20 22:08 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 03/25/20 22:08 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 03/25/20 22:08 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 03/25/20 22:08 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 03/25/20 22:08 79-00-50.50 1
Trichloroethene ND ug/L 03/25/20 22:08 79-01-60.50 1
Trichlorofluoromethane ND ug/L 03/25/20 22:08 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 03/25/20 22:08 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 03/25/20 22:08 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 03/25/20 22:08 108-67-80.50 1
Vinyl chloride ND ug/L 03/25/20 22:08 75-01-41.0 1
m&p-Xylene ND ug/L 03/25/20 22:08 179601-23-11.0 1
o-Xylene ND ug/L 03/25/20 22:08 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S) 102 % 03/25/20 22:08 17060-07-070-130 1
4-Bromofluorobenzene (S) 99 % 03/25/20 22:08 460-00-470-130 1
Toluene-d8 (S) 103 % 03/25/20 22:08 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/30/2020 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92470400
HANDY HOUSE 3
Sample: MW-14 Lab ID: 92470400008 Collected: 03/18/20 11:10 Received: 03/20/20 09:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: MADEP VPH Preparation Method: MADEPVMADEPV
Aliphatic (C05-C08) ND ug/L 03/26/20 16:3603/26/20 16:36100 1
Aliphatic (C09-C12) ND ug/L 03/26/20 16:3603/26/20 16:36100 1
Aromatic (C09-C10),Unadjusted ND ug/L 03/26/20 16:36 TPHC9C10A03/26/20 16:36100 1
Total VPH ND ug/L 03/26/20 16:36 VPH03/26/20 16:36100 1
Surrogates
2,5-Dibromotoluene (FID) 93.6 % 03/26/20 16:36 615-59-8FID03/26/20 16:3670.0-130 1
2,5-Dibromotoluene (PID) 92.8 % 03/26/20 16:36 615-59-8PID03/26/20 16:3670.0-130 1
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 03/25/20 22:26 71-43-20.50 1
Bromobenzene ND ug/L 03/25/20 22:26 108-86-10.50 1
Bromochloromethane ND ug/L 03/25/20 22:26 74-97-50.50 1
Bromodichloromethane ND ug/L 03/25/20 22:26 75-27-40.50 1
Bromoform ND ug/L 03/25/20 22:26 75-25-20.50 1
Bromomethane ND ug/L 03/25/20 22:26 74-83-95.0 1
n-Butylbenzene ND ug/L 03/25/20 22:26 104-51-80.50 1
sec-Butylbenzene ND ug/L 03/25/20 22:26 135-98-80.50 1
tert-Butylbenzene ND ug/L 03/25/20 22:26 98-06-60.50 1
Carbon tetrachloride ND ug/L 03/25/20 22:26 56-23-50.50 1
Chlorobenzene ND ug/L 03/25/20 22:26 108-90-70.50 1
Chloroethane ND ug/L 03/25/20 22:26 75-00-31.0 1
Chloroform ND ug/L 03/25/20 22:26 67-66-30.50 1
Chloromethane ND ug/L 03/25/20 22:26 74-87-31.0 1
2-Chlorotoluene ND ug/L 03/25/20 22:26 95-49-80.50 1
4-Chlorotoluene ND ug/L 03/25/20 22:26 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 03/25/20 22:26 96-12-81.0 1
Dibromochloromethane ND ug/L 03/25/20 22:26 124-48-10.50 1
1,2-Dibromoethane (EDB) ND ug/L 03/25/20 22:26 106-93-40.50 1
Dibromomethane ND ug/L 03/25/20 22:26 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 03/25/20 22:26 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 03/25/20 22:26 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 03/25/20 22:26 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 03/25/20 22:26 75-71-80.50 1
1,1-Dichloroethane ND ug/L 03/25/20 22:26 75-34-30.50 1
1,2-Dichloroethane ND ug/L 03/25/20 22:26 107-06-20.50 1
1,1-Dichloroethene ND ug/L 03/25/20 22:26 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 03/25/20 22:26 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 03/25/20 22:26 156-60-50.50 1
1,2-Dichloropropane ND ug/L 03/25/20 22:26 78-87-50.50 1
1,3-Dichloropropane ND ug/L 03/25/20 22:26 142-28-90.50 1
2,2-Dichloropropane ND ug/L 03/25/20 22:26 594-20-70.50 1
1,1-Dichloropropene ND ug/L 03/25/20 22:26 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 03/25/20 22:26 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 03/25/20 22:26 10061-02-60.50 1
Diisopropyl ether ND ug/L 03/25/20 22:26 108-20-30.50 1
Ethylbenzene ND ug/L 03/25/20 22:26 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 03/25/20 22:26 87-68-32.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/30/2020 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92470400
HANDY HOUSE 3
Sample: MW-14 Lab ID: 92470400008 Collected: 03/18/20 11:10 Received: 03/20/20 09:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B6200B MSV
Isopropylbenzene (Cumene) ND ug/L 03/25/20 22:26 98-82-80.50 1
Methylene Chloride ND ug/L 03/25/20 22:26 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 03/25/20 22:26 1634-04-40.50 1
Naphthalene ND ug/L 03/25/20 22:26 91-20-32.0 1
n-Propylbenzene ND ug/L 03/25/20 22:26 103-65-10.50 1
Styrene ND ug/L 03/25/20 22:26 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 03/25/20 22:26 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 03/25/20 22:26 79-34-50.50 1
Tetrachloroethene ND ug/L 03/25/20 22:26 127-18-40.50 1
Toluene ND ug/L 03/25/20 22:26 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 03/25/20 22:26 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 03/25/20 22:26 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 03/25/20 22:26 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 03/25/20 22:26 79-00-50.50 1
Trichloroethene ND ug/L 03/25/20 22:26 79-01-60.50 1
Trichlorofluoromethane ND ug/L 03/25/20 22:26 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 03/25/20 22:26 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 03/25/20 22:26 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 03/25/20 22:26 108-67-80.50 1
Vinyl chloride ND ug/L 03/25/20 22:26 75-01-41.0 1
m&p-Xylene ND ug/L 03/25/20 22:26 179601-23-11.0 1
o-Xylene ND ug/L 03/25/20 22:26 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S) 98 % 03/25/20 22:26 17060-07-070-130 1
4-Bromofluorobenzene (S) 101 % 03/25/20 22:26 460-00-470-130 1
Toluene-d8 (S) 103 % 03/25/20 22:26 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/30/2020 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92470400
HANDY HOUSE 3
Sample: MW-15 Lab ID: 92470400009 Collected: 03/18/20 11:30 Received: 03/20/20 09:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: MADEP VPH Preparation Method: MADEPVMADEPV
Aliphatic (C05-C08) ND ug/L 03/26/20 17:0803/26/20 17:08100 1
Aliphatic (C09-C12) ND ug/L 03/26/20 17:0803/26/20 17:08100 1
Aromatic (C09-C10),Unadjusted ND ug/L 03/26/20 17:08 TPHC9C10A03/26/20 17:08100 1
Total VPH ND ug/L 03/26/20 17:08 VPH03/26/20 17:08100 1
Surrogates
2,5-Dibromotoluene (FID) 95.1 % 03/26/20 17:08 615-59-8FID03/26/20 17:0870.0-130 1
2,5-Dibromotoluene (PID) 96.6 % 03/26/20 17:08 615-59-8PID03/26/20 17:0870.0-130 1
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 03/25/20 22:44 71-43-20.50 1
Bromobenzene ND ug/L 03/25/20 22:44 108-86-10.50 1
Bromochloromethane ND ug/L 03/25/20 22:44 74-97-50.50 1
Bromodichloromethane ND ug/L 03/25/20 22:44 75-27-40.50 1
Bromoform ND ug/L 03/25/20 22:44 75-25-20.50 1
Bromomethane ND ug/L 03/25/20 22:44 74-83-95.0 1
n-Butylbenzene ND ug/L 03/25/20 22:44 104-51-80.50 1
sec-Butylbenzene ND ug/L 03/25/20 22:44 135-98-80.50 1
tert-Butylbenzene ND ug/L 03/25/20 22:44 98-06-60.50 1
Carbon tetrachloride ND ug/L 03/25/20 22:44 56-23-50.50 1
Chlorobenzene ND ug/L 03/25/20 22:44 108-90-70.50 1
Chloroethane ND ug/L 03/25/20 22:44 75-00-31.0 1
Chloroform ND ug/L 03/25/20 22:44 67-66-30.50 1
Chloromethane ND ug/L 03/25/20 22:44 74-87-31.0 1
2-Chlorotoluene ND ug/L 03/25/20 22:44 95-49-80.50 1
4-Chlorotoluene ND ug/L 03/25/20 22:44 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 03/25/20 22:44 96-12-81.0 1
Dibromochloromethane ND ug/L 03/25/20 22:44 124-48-10.50 1
1,2-Dibromoethane (EDB) ND ug/L 03/25/20 22:44 106-93-40.50 1
Dibromomethane ND ug/L 03/25/20 22:44 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 03/25/20 22:44 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 03/25/20 22:44 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 03/25/20 22:44 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 03/25/20 22:44 75-71-80.50 1
1,1-Dichloroethane ND ug/L 03/25/20 22:44 75-34-30.50 1
1,2-Dichloroethane ND ug/L 03/25/20 22:44 107-06-20.50 1
1,1-Dichloroethene ND ug/L 03/25/20 22:44 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 03/25/20 22:44 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 03/25/20 22:44 156-60-50.50 1
1,2-Dichloropropane ND ug/L 03/25/20 22:44 78-87-50.50 1
1,3-Dichloropropane ND ug/L 03/25/20 22:44 142-28-90.50 1
2,2-Dichloropropane ND ug/L 03/25/20 22:44 594-20-70.50 1
1,1-Dichloropropene ND ug/L 03/25/20 22:44 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 03/25/20 22:44 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 03/25/20 22:44 10061-02-60.50 1
Diisopropyl ether ND ug/L 03/25/20 22:44 108-20-30.50 1
Ethylbenzene ND ug/L 03/25/20 22:44 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 03/25/20 22:44 87-68-32.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/30/2020 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92470400
HANDY HOUSE 3
Sample: MW-15 Lab ID: 92470400009 Collected: 03/18/20 11:30 Received: 03/20/20 09:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B6200B MSV
Isopropylbenzene (Cumene) ND ug/L 03/25/20 22:44 98-82-80.50 1
Methylene Chloride ND ug/L 03/25/20 22:44 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 03/25/20 22:44 1634-04-40.50 1
Naphthalene ND ug/L 03/25/20 22:44 91-20-32.0 1
n-Propylbenzene ND ug/L 03/25/20 22:44 103-65-10.50 1
Styrene ND ug/L 03/25/20 22:44 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 03/25/20 22:44 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 03/25/20 22:44 79-34-50.50 1
Tetrachloroethene ND ug/L 03/25/20 22:44 127-18-40.50 1
Toluene ND ug/L 03/25/20 22:44 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 03/25/20 22:44 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 03/25/20 22:44 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 03/25/20 22:44 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 03/25/20 22:44 79-00-50.50 1
Trichloroethene ND ug/L 03/25/20 22:44 79-01-60.50 1
Trichlorofluoromethane ND ug/L 03/25/20 22:44 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 03/25/20 22:44 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 03/25/20 22:44 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 03/25/20 22:44 108-67-80.50 1
Vinyl chloride ND ug/L 03/25/20 22:44 75-01-41.0 1
m&p-Xylene ND ug/L 03/25/20 22:44 179601-23-11.0 1
o-Xylene ND ug/L 03/25/20 22:44 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S) 98 % 03/25/20 22:44 17060-07-070-130 1
4-Bromofluorobenzene (S) 99 % 03/25/20 22:44 460-00-470-130 1
Toluene-d8 (S) 104 % 03/25/20 22:44 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/30/2020 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92470400
HANDY HOUSE 3
Sample: MW-17 Lab ID: 92470400010 Collected: 03/18/20 11:55 Received: 03/20/20 09:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: MADEP VPH Preparation Method: MADEPVMADEPV
Aliphatic (C05-C08) ND ug/L 03/27/20 15:4603/27/20 15:46100 1
Aliphatic (C09-C12) ND ug/L 03/27/20 15:4603/27/20 15:46100 1
Aromatic (C09-C10),Unadjusted ND ug/L 03/27/20 15:46 TPHC9C10A03/27/20 15:46100 1
Total VPH ND ug/L 03/27/20 15:46 VPH03/27/20 15:46100 1
Surrogates
2,5-Dibromotoluene (FID) 94.7 % 03/27/20 15:46 615-59-8FID03/27/20 15:4670.0-130 1
2,5-Dibromotoluene (PID) 93.5 % 03/27/20 15:46 615-59-8PID03/27/20 15:4670.0-130 1
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 03/25/20 23:02 71-43-20.50 1
Bromobenzene ND ug/L 03/25/20 23:02 108-86-10.50 1
Bromochloromethane ND ug/L 03/25/20 23:02 74-97-50.50 1
Bromodichloromethane ND ug/L 03/25/20 23:02 75-27-40.50 1
Bromoform ND ug/L 03/25/20 23:02 75-25-20.50 1
Bromomethane ND ug/L 03/25/20 23:02 74-83-95.0 1
n-Butylbenzene ND ug/L 03/25/20 23:02 104-51-80.50 1
sec-Butylbenzene ND ug/L 03/25/20 23:02 135-98-80.50 1
tert-Butylbenzene ND ug/L 03/25/20 23:02 98-06-60.50 1
Carbon tetrachloride ND ug/L 03/25/20 23:02 56-23-50.50 1
Chlorobenzene ND ug/L 03/25/20 23:02 108-90-70.50 1
Chloroethane ND ug/L 03/25/20 23:02 75-00-31.0 1
Chloroform ND ug/L 03/25/20 23:02 67-66-30.50 1
Chloromethane ND ug/L 03/25/20 23:02 74-87-31.0 1
2-Chlorotoluene ND ug/L 03/25/20 23:02 95-49-80.50 1
4-Chlorotoluene ND ug/L 03/25/20 23:02 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 03/25/20 23:02 96-12-81.0 1
Dibromochloromethane ND ug/L 03/25/20 23:02 124-48-10.50 1
1,2-Dibromoethane (EDB) ND ug/L 03/25/20 23:02 106-93-40.50 1
Dibromomethane ND ug/L 03/25/20 23:02 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 03/25/20 23:02 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 03/25/20 23:02 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 03/25/20 23:02 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 03/25/20 23:02 75-71-80.50 1
1,1-Dichloroethane ND ug/L 03/25/20 23:02 75-34-30.50 1
1,2-Dichloroethane ND ug/L 03/25/20 23:02 107-06-20.50 1
1,1-Dichloroethene ND ug/L 03/25/20 23:02 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 03/25/20 23:02 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 03/25/20 23:02 156-60-50.50 1
1,2-Dichloropropane ND ug/L 03/25/20 23:02 78-87-50.50 1
1,3-Dichloropropane ND ug/L 03/25/20 23:02 142-28-90.50 1
2,2-Dichloropropane ND ug/L 03/25/20 23:02 594-20-70.50 1
1,1-Dichloropropene ND ug/L 03/25/20 23:02 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 03/25/20 23:02 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 03/25/20 23:02 10061-02-60.50 1
Diisopropyl ether ND ug/L 03/25/20 23:02 108-20-30.50 1
Ethylbenzene ND ug/L 03/25/20 23:02 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 03/25/20 23:02 87-68-32.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/30/2020 08:33 AM
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9800 Kincey Ave. Suite 100
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Page 24 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92470400
HANDY HOUSE 3
Sample: MW-17 Lab ID: 92470400010 Collected: 03/18/20 11:55 Received: 03/20/20 09:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B6200B MSV
Isopropylbenzene (Cumene) ND ug/L 03/25/20 23:02 98-82-80.50 1
Methylene Chloride ND ug/L 03/25/20 23:02 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 03/25/20 23:02 1634-04-40.50 1
Naphthalene ND ug/L 03/25/20 23:02 91-20-32.0 1
n-Propylbenzene ND ug/L 03/25/20 23:02 103-65-10.50 1
Styrene ND ug/L 03/25/20 23:02 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 03/25/20 23:02 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 03/25/20 23:02 79-34-50.50 1
Tetrachloroethene ND ug/L 03/25/20 23:02 127-18-40.50 1
Toluene ND ug/L 03/25/20 23:02 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 03/25/20 23:02 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 03/25/20 23:02 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 03/25/20 23:02 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 03/25/20 23:02 79-00-50.50 1
Trichloroethene ND ug/L 03/25/20 23:02 79-01-60.50 1
Trichlorofluoromethane ND ug/L 03/25/20 23:02 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 03/25/20 23:02 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 03/25/20 23:02 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 03/25/20 23:02 108-67-80.50 1
Vinyl chloride ND ug/L 03/25/20 23:02 75-01-41.0 1
m&p-Xylene ND ug/L 03/25/20 23:02 179601-23-11.0 1
o-Xylene ND ug/L 03/25/20 23:02 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S) 100 % 03/25/20 23:02 17060-07-070-130 1
4-Bromofluorobenzene (S) 100 % 03/25/20 23:02 460-00-470-130 1
Toluene-d8 (S) 100 % 03/25/20 23:02 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/30/2020 08:33 AM
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Huntersville, NC 28078
[phone]
Page 25 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92470400
HANDY HOUSE 3
Sample: VEW1 Lab ID: 92470400011 Collected: 03/18/20 12:30 Received: 03/20/20 09:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: MADEP VPH Preparation Method: MADEPVMADEPV
Aliphatic (C05-C08) ND ug/L 03/26/20 18:4503/26/20 18:45100 1
Aliphatic (C09-C12) ND ug/L 03/26/20 18:4503/26/20 18:45100 1
Aromatic (C09-C10),Unadjusted ND ug/L 03/26/20 18:45 TPHC9C10A03/26/20 18:45100 1
Total VPH ND ug/L 03/26/20 18:45 VPH03/26/20 18:45100 1
Surrogates
2,5-Dibromotoluene (FID) 96.6 % 03/26/20 18:45 615-59-8FID03/26/20 18:4570.0-130 1
2,5-Dibromotoluene (PID) 94.5 % 03/26/20 18:45 615-59-8PID03/26/20 18:4570.0-130 1
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 03/25/20 23:20 71-43-20.50 1
Bromobenzene ND ug/L 03/25/20 23:20 108-86-10.50 1
Bromochloromethane ND ug/L 03/25/20 23:20 74-97-50.50 1
Bromodichloromethane ND ug/L 03/25/20 23:20 75-27-40.50 1
Bromoform ND ug/L 03/25/20 23:20 75-25-20.50 1
Bromomethane ND ug/L 03/25/20 23:20 74-83-95.0 1
n-Butylbenzene ND ug/L 03/25/20 23:20 104-51-80.50 1
sec-Butylbenzene ND ug/L 03/25/20 23:20 135-98-80.50 1
tert-Butylbenzene ND ug/L 03/25/20 23:20 98-06-60.50 1
Carbon tetrachloride ND ug/L 03/25/20 23:20 56-23-50.50 1
Chlorobenzene ND ug/L 03/25/20 23:20 108-90-70.50 1
Chloroethane ND ug/L 03/25/20 23:20 75-00-31.0 1
Chloroform ND ug/L 03/25/20 23:20 67-66-30.50 1
Chloromethane ND ug/L 03/25/20 23:20 74-87-31.0 1
2-Chlorotoluene ND ug/L 03/25/20 23:20 95-49-80.50 1
4-Chlorotoluene ND ug/L 03/25/20 23:20 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 03/25/20 23:20 96-12-81.0 1
Dibromochloromethane ND ug/L 03/25/20 23:20 124-48-10.50 1
1,2-Dibromoethane (EDB) ND ug/L 03/25/20 23:20 106-93-40.50 1
Dibromomethane ND ug/L 03/25/20 23:20 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 03/25/20 23:20 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 03/25/20 23:20 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 03/25/20 23:20 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 03/25/20 23:20 75-71-80.50 1
1,1-Dichloroethane ND ug/L 03/25/20 23:20 75-34-30.50 1
1,2-Dichloroethane ND ug/L 03/25/20 23:20 107-06-20.50 1
1,1-Dichloroethene ND ug/L 03/25/20 23:20 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 03/25/20 23:20 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 03/25/20 23:20 156-60-50.50 1
1,2-Dichloropropane ND ug/L 03/25/20 23:20 78-87-50.50 1
1,3-Dichloropropane ND ug/L 03/25/20 23:20 142-28-90.50 1
2,2-Dichloropropane ND ug/L 03/25/20 23:20 594-20-70.50 1
1,1-Dichloropropene ND ug/L 03/25/20 23:20 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 03/25/20 23:20 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 03/25/20 23:20 10061-02-60.50 1
Diisopropyl ether ND ug/L 03/25/20 23:20 108-20-30.50 1
Ethylbenzene ND ug/L 03/25/20 23:20 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 03/25/20 23:20 87-68-32.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/30/2020 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92470400
HANDY HOUSE 3
Sample: VEW1 Lab ID: 92470400011 Collected: 03/18/20 12:30 Received: 03/20/20 09:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B6200B MSV
Isopropylbenzene (Cumene) ND ug/L 03/25/20 23:20 98-82-80.50 1
Methylene Chloride ND ug/L 03/25/20 23:20 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 03/25/20 23:20 1634-04-40.50 1
Naphthalene ND ug/L 03/25/20 23:20 91-20-32.0 1
n-Propylbenzene ND ug/L 03/25/20 23:20 103-65-10.50 1
Styrene ND ug/L 03/25/20 23:20 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 03/25/20 23:20 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 03/25/20 23:20 79-34-50.50 1
Tetrachloroethene ND ug/L 03/25/20 23:20 127-18-40.50 1
Toluene ND ug/L 03/25/20 23:20 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 03/25/20 23:20 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 03/25/20 23:20 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 03/25/20 23:20 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 03/25/20 23:20 79-00-50.50 1
Trichloroethene ND ug/L 03/25/20 23:20 79-01-60.50 1
Trichlorofluoromethane ND ug/L 03/25/20 23:20 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 03/25/20 23:20 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 03/25/20 23:20 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 03/25/20 23:20 108-67-80.50 1
Vinyl chloride ND ug/L 03/25/20 23:20 75-01-41.0 1
m&p-Xylene ND ug/L 03/25/20 23:20 179601-23-11.0 1
o-Xylene ND ug/L 03/25/20 23:20 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S) 99 % 03/25/20 23:20 17060-07-070-130 1
4-Bromofluorobenzene (S) 98 % 03/25/20 23:20 460-00-470-130 1
Toluene-d8 (S) 101 % 03/25/20 23:20 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/30/2020 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92470400
HANDY HOUSE 3
Sample: SW-3 Lab ID: 92470400012 Collected: 03/18/20 12:50 Received: 03/20/20 09:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: MADEP VPH Preparation Method: MADEPVMADEPV
Aliphatic (C05-C08) ND ug/L 03/26/20 19:1703/26/20 19:17100 1
Aliphatic (C09-C12) ND ug/L 03/26/20 19:1703/26/20 19:17100 1
Aromatic (C09-C10),Unadjusted ND ug/L 03/26/20 19:17 TPHC9C10A03/26/20 19:17100 1
Total VPH ND ug/L 03/26/20 19:17 VPH03/26/20 19:17100 1
Surrogates
2,5-Dibromotoluene (FID) 93.9 % 03/26/20 19:17 615-59-8FID03/26/20 19:1770.0-130 1
2,5-Dibromotoluene (PID) 95.3 % 03/26/20 19:17 615-59-8PID03/26/20 19:1770.0-130 1
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 03/26/20 02:56 71-43-20.50 1
Bromobenzene ND ug/L 03/26/20 02:56 108-86-10.50 1
Bromochloromethane ND ug/L 03/26/20 02:56 74-97-50.50 1
Bromodichloromethane ND ug/L 03/26/20 02:56 75-27-40.50 1
Bromoform ND ug/L 03/26/20 02:56 75-25-20.50 1
Bromomethane ND ug/L 03/26/20 02:56 74-83-95.0 1
n-Butylbenzene ND ug/L 03/26/20 02:56 104-51-80.50 1
sec-Butylbenzene ND ug/L 03/26/20 02:56 135-98-80.50 1
tert-Butylbenzene ND ug/L 03/26/20 02:56 98-06-60.50 1
Carbon tetrachloride ND ug/L 03/26/20 02:56 56-23-50.50 1
Chlorobenzene ND ug/L 03/26/20 02:56 108-90-70.50 1
Chloroethane ND ug/L 03/26/20 02:56 75-00-31.0 1
Chloroform ND ug/L 03/26/20 02:56 67-66-30.50 1
Chloromethane ND ug/L 03/26/20 02:56 74-87-31.0 1
2-Chlorotoluene ND ug/L 03/26/20 02:56 95-49-80.50 1
4-Chlorotoluene ND ug/L 03/26/20 02:56 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 03/26/20 02:56 96-12-81.0 1
Dibromochloromethane ND ug/L 03/26/20 02:56 124-48-10.50 1
1,2-Dibromoethane (EDB) ND ug/L 03/26/20 02:56 106-93-40.50 1
Dibromomethane ND ug/L 03/26/20 02:56 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 03/26/20 02:56 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 03/26/20 02:56 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 03/26/20 02:56 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 03/26/20 02:56 75-71-80.50 1
1,1-Dichloroethane ND ug/L 03/26/20 02:56 75-34-30.50 1
1,2-Dichloroethane ND ug/L 03/26/20 02:56 107-06-20.50 1
1,1-Dichloroethene ND ug/L 03/26/20 02:56 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 03/26/20 02:56 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 03/26/20 02:56 156-60-50.50 1
1,2-Dichloropropane ND ug/L 03/26/20 02:56 78-87-50.50 1
1,3-Dichloropropane ND ug/L 03/26/20 02:56 142-28-90.50 1
2,2-Dichloropropane ND ug/L 03/26/20 02:56 594-20-70.50 1
1,1-Dichloropropene ND ug/L 03/26/20 02:56 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 03/26/20 02:56 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 03/26/20 02:56 10061-02-60.50 1
Diisopropyl ether ND ug/L 03/26/20 02:56 108-20-30.50 1
Ethylbenzene ND ug/L 03/26/20 02:56 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 03/26/20 02:56 87-68-32.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/30/2020 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92470400
HANDY HOUSE 3
Sample: SW-3 Lab ID: 92470400012 Collected: 03/18/20 12:50 Received: 03/20/20 09:57 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B6200B MSV
Isopropylbenzene (Cumene) ND ug/L 03/26/20 02:56 98-82-80.50 1
Methylene Chloride ND ug/L 03/26/20 02:56 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 03/26/20 02:56 1634-04-40.50 1
Naphthalene ND ug/L 03/26/20 02:56 91-20-32.0 1
n-Propylbenzene ND ug/L 03/26/20 02:56 103-65-10.50 1
Styrene ND ug/L 03/26/20 02:56 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 03/26/20 02:56 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 03/26/20 02:56 79-34-50.50 1
Tetrachloroethene ND ug/L 03/26/20 02:56 127-18-40.50 1
Toluene ND ug/L 03/26/20 02:56 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 03/26/20 02:56 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 03/26/20 02:56 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 03/26/20 02:56 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 03/26/20 02:56 79-00-50.50 1
Trichloroethene ND ug/L 03/26/20 02:56 79-01-60.50 1
Trichlorofluoromethane ND ug/L 03/26/20 02:56 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 03/26/20 02:56 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 03/26/20 02:56 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 03/26/20 02:56 108-67-80.50 1
Vinyl chloride ND ug/L 03/26/20 02:56 75-01-41.0 1
m&p-Xylene ND ug/L 03/26/20 02:56 179601-23-11.0 1
o-Xylene ND ug/L 03/26/20 02:56 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S) 101 % 03/26/20 02:56 17060-07-070-130 1
4-Bromofluorobenzene (S) 98 % 03/26/20 02:56 460-00-470-130 1
Toluene-d8 (S) 106 % 03/26/20 02:56 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/30/2020 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92470400
HANDY HOUSE 3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1449867
MADEPV
MADEP VPH
MADEPV
Associated Lab Samples: 92470400001, 92470400002, 92470400003, 92470400004, 92470400005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: R3512992-3
Associated Lab Samples:92470400001, 92470400002, 92470400003, 92470400004, 92470400005
Matrix: Water
Analyzed
Aliphatic (C05-C08) ug/L ND 100 03/25/20 09:27
Aliphatic (C09-C12) ug/L ND 100 03/25/20 09:27
Aromatic (C09-C10),Unadjusted ug/L ND 100 03/25/20 09:27
Total VPH ug/L ND 100 03/25/20 09:27
2,5-Dibromotoluene (FID) % 91.9 70.0-130 03/25/20 09:27
2,5-Dibromotoluene (PID) % 90.8 70.0-130 03/25/20 09:27
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3512992-1LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3512992-2
Aliphatic (C05-C08) ug/L 13501200 113 70.0-1301131350 0.00 25
Aliphatic (C09-C12) ug/L 16401400 117 70.0-1301171640 0.00 25
Aromatic (C09-C10),Unadjusted ug/L 247200 123 70.0-130124249 0.806 25
Total VPH ug/L 32402800 116 70.0-1301163240 0.00 25
2,5-Dibromotoluene (FID) % 101 70.0-130100
2,5-Dibromotoluene (PID) % 99.9 70.0-13098.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/30/2020 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92470400
HANDY HOUSE 3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1450627
MADEPV
MADEP VPH
MADEPV
Associated Lab Samples: 92470400006, 92470400007, 92470400008, 92470400009, 92470400011, 92470400012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: R3513107-3
Associated Lab Samples:92470400006, 92470400007, 92470400008, 92470400009, 92470400011, 92470400012
Matrix: Water
Analyzed
Aliphatic (C05-C08) ug/L ND 100 03/26/20 14:07
Aliphatic (C09-C12) ug/L ND 100 03/26/20 14:07
Aromatic (C09-C10),Unadjusted ug/L ND 100 03/26/20 14:07
Total VPH ug/L ND 100 03/26/20 14:07
2,5-Dibromotoluene (FID) % 93.6 70.0-130 03/26/20 14:07
2,5-Dibromotoluene (PID) % 92.5 70.0-130 03/26/20 14:07
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3513107-1LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3513107-2
Aliphatic (C05-C08) ug/L 12701200 106 70.0-1301071280 0.784 25
Aliphatic (C09-C12) ug/L 15701400 112 70.0-1301131580 0.635 25
Aromatic (C09-C10),Unadjusted ug/L 242200 121 70.0-130123245 1.23 25
Total VPH ug/L 30802800 110 70.0-1301113110 0.969 25
2,5-Dibromotoluene (FID) % 102 70.0-13099.9
2,5-Dibromotoluene (PID) % 102 70.0-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/30/2020 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92470400
HANDY HOUSE 3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1451334
MADEPV
MADEP VPH
MADEPV
Associated Lab Samples: 92470400010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: R3513341-3
Associated Lab Samples:92470400010
Matrix: Water
Analyzed
Aliphatic (C05-C08) ug/L ND 100 03/27/20 14:10
Aliphatic (C09-C12) ug/L ND 100 03/27/20 14:10
Aromatic (C09-C10),Unadjusted ug/L ND 100 03/27/20 14:10
Total VPH ug/L ND 100 03/27/20 14:10
2,5-Dibromotoluene (FID) % 88.1 70.0-130 03/27/20 14:10
2,5-Dibromotoluene (PID) % 87.3 70.0-130 03/27/20 14:10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3513341-1LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3513341-2
Aliphatic (C05-C08) ug/L 11801200 98.3 70.0-1301021220 3.33 25
Aliphatic (C09-C12) ug/L 15201400 109 70.0-1301111550 1.95 25
Aromatic (C09-C10),Unadjusted ug/L 232200 116 70.0-130119239 2.97 25
Total VPH ug/L 29302800 105 70.0-1301083010 2.69 25
2,5-Dibromotoluene (FID) % 96.8 70.0-13097.2
2,5-Dibromotoluene (PID) % 96.0 70.0-13096.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/30/2020 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92470400
HANDY HOUSE 3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
532453
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92470400002, 92470400004, 92470400005, 92470400007, 92470400008, 92470400009, 92470400010,
92470400011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2842329
Associated Lab Samples: 92470400002, 92470400004, 92470400005, 92470400007, 92470400008, 92470400009, 92470400010,
92470400011
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 03/25/20 17:39
1,1,1-Trichloroethane ug/L ND 0.50 03/25/20 17:39
1,1,2,2-Tetrachloroethane ug/L ND 0.50 03/25/20 17:39
1,1,2-Trichloroethane ug/L ND 0.50 03/25/20 17:39
1,1-Dichloroethane ug/L ND 0.50 03/25/20 17:39
1,1-Dichloroethene ug/L ND 0.50 03/25/20 17:39
1,1-Dichloropropene ug/L ND 0.50 03/25/20 17:39
1,2,3-Trichlorobenzene ug/L ND 2.0 03/25/20 17:39
1,2,3-Trichloropropane ug/L ND 0.50 03/25/20 17:39
1,2,4-Trichlorobenzene ug/L ND 2.0 03/25/20 17:39
1,2,4-Trimethylbenzene ug/L ND 0.50 03/25/20 17:39
1,2-Dibromo-3-chloropropane ug/L ND 1.0 03/25/20 17:39
1,2-Dibromoethane (EDB) ug/L ND 0.50 03/25/20 17:39
1,2-Dichlorobenzene ug/L ND 0.50 03/25/20 17:39
1,2-Dichloroethane ug/L ND 0.50 03/25/20 17:39
1,2-Dichloropropane ug/L ND 0.50 03/25/20 17:39
1,3,5-Trimethylbenzene ug/L ND 0.50 03/25/20 17:39
1,3-Dichlorobenzene ug/L ND 0.50 03/25/20 17:39
1,3-Dichloropropane ug/L ND 0.50 03/25/20 17:39
1,4-Dichlorobenzene ug/L ND 0.50 03/25/20 17:39
2,2-Dichloropropane ug/L ND 0.50 03/25/20 17:39
2-Chlorotoluene ug/L ND 0.50 03/25/20 17:39
4-Chlorotoluene ug/L ND 0.50 03/25/20 17:39
Benzene ug/L ND 0.50 03/25/20 17:39
Bromobenzene ug/L ND 0.50 03/25/20 17:39
Bromochloromethane ug/L ND 0.50 03/25/20 17:39
Bromodichloromethane ug/L ND 0.50 03/25/20 17:39
Bromoform ug/L ND 0.50 03/25/20 17:39
Bromomethane ug/L ND 5.0 03/25/20 17:39
Carbon tetrachloride ug/L ND 0.50 03/25/20 17:39
Chlorobenzene ug/L ND 0.50 03/25/20 17:39
Chloroethane ug/L ND 1.0 03/25/20 17:39
Chloroform ug/L ND 0.50 03/25/20 17:39
Chloromethane ug/L ND 1.0 03/25/20 17:39
cis-1,2-Dichloroethene ug/L ND 0.50 03/25/20 17:39
cis-1,3-Dichloropropene ug/L ND 0.50 03/25/20 17:39
Dibromochloromethane ug/L ND 0.50 03/25/20 17:39
Dibromomethane ug/L ND 0.50 03/25/20 17:39
Dichlorodifluoromethane ug/L ND 0.50 03/25/20 17:39
Diisopropyl ether ug/L ND 0.50 03/25/20 17:39
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/30/2020 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92470400
HANDY HOUSE 3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2842329
Associated Lab Samples: 92470400002, 92470400004, 92470400005, 92470400007, 92470400008, 92470400009, 92470400010,
92470400011
Matrix: Water
Analyzed
Ethylbenzene ug/L ND 0.50 03/25/20 17:39
Hexachloro-1,3-butadiene ug/L ND 2.0 03/25/20 17:39
Isopropylbenzene (Cumene) ug/L ND 0.50 03/25/20 17:39
m&p-Xylene ug/L ND 1.0 03/25/20 17:39
Methyl-tert-butyl ether ug/L ND 0.50 03/25/20 17:39
Methylene Chloride ug/L ND 2.0 03/25/20 17:39
n-Butylbenzene ug/L ND 0.50 03/25/20 17:39
n-Propylbenzene ug/L ND 0.50 03/25/20 17:39
Naphthalene ug/L ND 2.0 03/25/20 17:39
o-Xylene ug/L ND 0.50 03/25/20 17:39
sec-Butylbenzene ug/L ND 0.50 03/25/20 17:39
Styrene ug/L ND 0.50 03/25/20 17:39
tert-Butylbenzene ug/L ND 0.50 03/25/20 17:39
Tetrachloroethene ug/L ND 0.50 03/25/20 17:39
Toluene ug/L ND 0.50 03/25/20 17:39
trans-1,2-Dichloroethene ug/L ND 0.50 03/25/20 17:39
trans-1,3-Dichloropropene ug/L ND 0.50 03/25/20 17:39
Trichloroethene ug/L ND 0.50 03/25/20 17:39
Trichlorofluoromethane ug/L ND 1.0 03/25/20 17:39
Vinyl chloride ug/L ND 1.0 03/25/20 17:39
1,2-Dichloroethane-d4 (S) % 94 70-130 03/25/20 17:39
4-Bromofluorobenzene (S) % 103 70-130 03/25/20 17:39
Toluene-d8 (S) % 104 70-130 03/25/20 17:39
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2842330LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 55.950 112 60-140
1,1,1-Trichloroethane ug/L 51.750 103 60-140
1,1,2,2-Tetrachloroethane ug/L 53.150 106 60-140
1,1,2-Trichloroethane ug/L 57.850 116 60-140
1,1-Dichloroethane ug/L 50.250 100 60-140
1,1-Dichloroethene ug/L 49.750 99 60-140
1,1-Dichloropropene ug/L 54.550 109 60-140
1,2,3-Trichlorobenzene ug/L 58.350 117 60-140
1,2,3-Trichloropropane ug/L 52.450 105 60-140
1,2,4-Trichlorobenzene ug/L 59.250 118 60-140
1,2,4-Trimethylbenzene ug/L 52.850 106 60-140
1,2-Dibromo-3-chloropropane ug/L 61.950 124 60-140
1,2-Dibromoethane (EDB) ug/L 56.550 113 60-140
1,2-Dichlorobenzene ug/L 55.450 111 60-140
1,2-Dichloroethane ug/L 47.650 95 60-140
1,2-Dichloropropane ug/L 52.550 105 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/30/2020 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92470400
HANDY HOUSE 3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2842330LABORATORY CONTROL SAMPLE:
LCSSpike
1,3,5-Trimethylbenzene ug/L 52.450 105 60-140
1,3-Dichlorobenzene ug/L 54.850 110 60-140
1,3-Dichloropropane ug/L 53.450 107 60-140
1,4-Dichlorobenzene ug/L 53.850 108 60-140
2,2-Dichloropropane ug/L 51.450 103 60-140
2-Chlorotoluene ug/L 53.450 107 60-140
4-Chlorotoluene ug/L 54.750 109 60-140
Benzene ug/L 53.750 107 60-140
Bromobenzene ug/L 55.150 110 60-140
Bromochloromethane ug/L 55.550 111 60-140
Bromodichloromethane ug/L 51.150 102 60-140
Bromoform ug/L 54.350 109 60-140
Bromomethane ug/L 57.950 116 60-140
Carbon tetrachloride ug/L 54.450 109 60-140
Chlorobenzene ug/L 52.850 106 60-140
Chloroethane ug/L 43.650 87 60-140
Chloroform ug/L 53.750 107 60-140
Chloromethane ug/L 43.250 86 60-140
cis-1,2-Dichloroethene ug/L 51.850 104 60-140
cis-1,3-Dichloropropene ug/L 53.750 107 60-140
Dibromochloromethane ug/L 56.950 114 60-140
Dibromomethane ug/L 56.350 113 60-140
Dichlorodifluoromethane ug/L 45.450 91 60-140
Diisopropyl ether ug/L 51.450 103 60-140
Ethylbenzene ug/L 51.250 102 60-140
Hexachloro-1,3-butadiene ug/L 53.750 107 60-140
Isopropylbenzene (Cumene) ug/L 54.150 108 60-140
m&p-Xylene ug/L 103100 103 60-140
Methyl-tert-butyl ether ug/L 54.350 109 60-140
Methylene Chloride ug/L 48.250 96 60-140
n-Butylbenzene ug/L 51.550 103 60-140
n-Propylbenzene ug/L 52.250 104 60-140
Naphthalene ug/L 57.950 116 60-140
o-Xylene ug/L 51.950 104 60-140
sec-Butylbenzene ug/L 52.650 105 60-140
Styrene ug/L 52.750 105 60-140
tert-Butylbenzene ug/L 45.250 90 60-140
Tetrachloroethene ug/L 52.150 104 60-140
Toluene ug/L 50.950 102 60-140
trans-1,2-Dichloroethene ug/L 49.950 100 60-140
trans-1,3-Dichloropropene ug/L 54.750 109 60-140
Trichloroethene ug/L 55.850 112 60-140
Trichlorofluoromethane ug/L 44.450 89 60-140
Vinyl chloride ug/L 52.050 104 60-140
1,2-Dichloroethane-d4 (S) % 95 70-130
4-Bromofluorobenzene (S) % 101 70-130
Toluene-d8 (S) % 101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/30/2020 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92470400
HANDY HOUSE 3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2842331MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92470362001
2842332
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 200 117 60-140113 3 30200ND 233 226
1,1,1-Trichloroethane ug/L 200 119 60-140118 0 30200ND 237 236
1,1,2,2-Tetrachloroethane ug/L 200 111 60-140109 2 30200ND 222 218
1,1,2-Trichloroethane ug/L 200 119 60-140121 1 30200ND 238 241
1,1-Dichloroethane ug/L 200 116 60-140110 6 30200ND 233 219
1,1-Dichloroethene ug/L 200 116 60-140111 5 30200ND 232 221
1,1-Dichloropropene ug/L 200 123 60-140121 2 30200ND 246 242
1,2,3-Trichlorobenzene ug/L 200 117 60-140122 4 30200ND 234 244
1,2,3-Trichloropropane ug/L 200 111 60-140102 9 30200ND 222 204
1,2,4-Trichlorobenzene ug/L 200 117 60-140117 0 30200ND 234 233
1,2,4-Trimethylbenzene ug/L 200 96 60-140113 3 30200959 1150 1190
1,2-Dibromo-3-
chloropropane ug/L 200 109 60-140114 4 30200ND 218 228
1,2-Dibromoethane (EDB) ug/L 200 114 60-140110 4 30200ND 228 220
1,2-Dichlorobenzene ug/L 200 114 60-140112 2 30200ND 227 223
1,2-Dichloroethane ug/L 200 106 60-140100 6 30200ND 212 200
1,2-Dichloropropane ug/L 200 117 60-140113 3 30200ND 234 227
1,3,5-Trimethylbenzene ug/L 200 113 60-140112 1 30200154 381 378
1,3-Dichlorobenzene ug/L 200 115 60-140114 1 30200ND 229 228
1,3-Dichloropropane ug/L 200 112 60-140108 4 30200ND 224 216
1,4-Dichlorobenzene ug/L 200 112 60-140110 2 30200ND 223 219
2,2-Dichloropropane ug/L 200 101 60-14099 2 30200ND 202 198
2-Chlorotoluene ug/L 200 140 60-140139 1 30200ND 280 277
4-Chlorotoluene ug/L 200 117 60-140113 4 30200ND 235 226
Benzene ug/L 200 124 60-140120 3 3020015.0 264 256
Bromobenzene ug/L 200 114 60-140109 4 30200ND 228 219
Bromochloromethane ug/L 200 119 60-140118 1 30200ND 238 235
Bromodichloromethane ug/L 200 108 60-140104 3 30200ND 215 208
Bromoform ug/L 200 107 60-14099 8 30200ND 214 198
Bromomethane ug/L 200 101 60-140119 17 30200ND 202 238
Carbon tetrachloride ug/L 200 121 60-140114 6 30200ND 242 228
Chlorobenzene ug/L 200 115 60-140112 2 30200ND 230 224
Chloroethane ug/L 200 115 60-140107 7 30200ND 231 214
Chloroform ug/L 200 117 60-140112 5 30200ND 235 224
Chloromethane ug/L 200 96 60-14097 2 30200ND 192 195
cis-1,2-Dichloroethene ug/L 200 113 60-140111 2 30200ND 227 223
cis-1,3-Dichloropropene ug/L 200 115 60-140106 9 30200ND 231 212
Dibromochloromethane ug/L 200 119 60-140108 9 30200ND 237 217
Dibromomethane ug/L 200 120 60-140110 8 30200ND 239 220
Dichlorodifluoromethane ug/L 200 117 60-140108 8 30200ND 233 216
Diisopropyl ether ug/L 200 116 60-140111 5 30200ND 232 221
Ethylbenzene ug/L 200 123 60-140114 2 30200718 964 945
Hexachloro-1,3-butadiene ug/L 200 114 60-140119 5 30200ND 227 239
Isopropylbenzene
(Cumene)
ug/L 200 120 60-140114 4 3020049.6 289 278
m&p-Xylene ug/L 400 117 60-140114 1 304001570 2040 2030
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/30/2020 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92470400
HANDY HOUSE 3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2842331MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92470362001
2842332
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Methyl-tert-butyl ether ug/L 200 116 60-140114 1 30200ND 231 228
Methylene Chloride ug/L 200 112 60-140108 4 30200ND 224 215
n-Butylbenzene ug/L 200 123 60-140123 0 30200ND 245 246
n-Propylbenzene ug/L 200 109 60-140108 1 30200168 387 384
Naphthalene ug/L M1200 127 60-140146 7 30200273 526 566
o-Xylene ug/L 200 117 60-140113 2 30200210 444 436
sec-Butylbenzene ug/L 200 114 60-140115 1 30200ND 228 229
Styrene ug/L 200 116 60-140109 6 30200ND 232 219
tert-Butylbenzene ug/L 200 95 60-14095 1 30200ND 191 189
Tetrachloroethene ug/L 200 115 60-140109 6 30200ND 231 217
Toluene ug/L 200 115 60-140114 0 30200117 347 346
trans-1,2-Dichloroethene ug/L 200 114 60-140112 1 30200ND 227 224
trans-1,3-Dichloropropene ug/L 200 110 60-140109 0 30200ND 220 219
Trichloroethene ug/L 200 120 60-140118 2 30200ND 241 235
Trichlorofluoromethane ug/L 200 110 60-140106 4 30200ND 219 211
Vinyl chloride ug/L 200 127 60-140119 6 30200ND 254 238
1,2-Dichloroethane-d4 (S) % 97 70-130102
4-Bromofluorobenzene (S) % 102 70-130101
Toluene-d8 (S) % 101 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/30/2020 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92470400
HANDY HOUSE 3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
532455
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples: 92470400001, 92470400003, 92470400012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2842334
Associated Lab Samples:92470400001, 92470400003, 92470400012
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 03/26/20 02:38
1,1,1-Trichloroethane ug/L ND 0.50 03/26/20 02:38
1,1,2,2-Tetrachloroethane ug/L ND 0.50 03/26/20 02:38
1,1,2-Trichloroethane ug/L ND 0.50 03/26/20 02:38
1,1-Dichloroethane ug/L ND 0.50 03/26/20 02:38
1,1-Dichloroethene ug/L ND 0.50 03/26/20 02:38
1,1-Dichloropropene ug/L ND 0.50 03/26/20 02:38
1,2,3-Trichlorobenzene ug/L ND 2.0 03/26/20 02:38
1,2,3-Trichloropropane ug/L ND 0.50 03/26/20 02:38
1,2,4-Trichlorobenzene ug/L ND 2.0 03/26/20 02:38
1,2,4-Trimethylbenzene ug/L ND 0.50 03/26/20 02:38
1,2-Dibromo-3-chloropropane ug/L ND 1.0 03/26/20 02:38
1,2-Dibromoethane (EDB) ug/L ND 0.50 03/26/20 02:38
1,2-Dichlorobenzene ug/L ND 0.50 03/26/20 02:38
1,2-Dichloroethane ug/L ND 0.50 03/26/20 02:38
1,2-Dichloropropane ug/L ND 0.50 03/26/20 02:38
1,3,5-Trimethylbenzene ug/L ND 0.50 03/26/20 02:38
1,3-Dichlorobenzene ug/L ND 0.50 03/26/20 02:38
1,3-Dichloropropane ug/L ND 0.50 03/26/20 02:38
1,4-Dichlorobenzene ug/L ND 0.50 03/26/20 02:38
2,2-Dichloropropane ug/L ND 0.50 03/26/20 02:38
2-Chlorotoluene ug/L ND 0.50 03/26/20 02:38
4-Chlorotoluene ug/L ND 0.50 03/26/20 02:38
Benzene ug/L ND 0.50 03/26/20 02:38
Bromobenzene ug/L ND 0.50 03/26/20 02:38
Bromochloromethane ug/L ND 0.50 03/26/20 02:38
Bromodichloromethane ug/L ND 0.50 03/26/20 02:38
Bromoform ug/L ND 0.50 03/26/20 02:38
Bromomethane ug/L ND 5.0 03/26/20 02:38
Carbon tetrachloride ug/L ND 0.50 03/26/20 02:38
Chlorobenzene ug/L ND 0.50 03/26/20 02:38
Chloroethane ug/L ND 1.0 03/26/20 02:38
Chloroform ug/L ND 0.50 03/26/20 02:38
Chloromethane ug/L ND 1.0 03/26/20 02:38
cis-1,2-Dichloroethene ug/L ND 0.50 03/26/20 02:38
cis-1,3-Dichloropropene ug/L ND 0.50 03/26/20 02:38
Dibromochloromethane ug/L ND 0.50 03/26/20 02:38
Dibromomethane ug/L ND 0.50 03/26/20 02:38
Dichlorodifluoromethane ug/L ND 0.50 03/26/20 02:38
Diisopropyl ether ug/L ND 0.50 03/26/20 02:38
Ethylbenzene ug/L ND 0.50 03/26/20 02:38
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/30/2020 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92470400
HANDY HOUSE 3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2842334
Associated Lab Samples:92470400001, 92470400003, 92470400012
Matrix: Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 2.0 03/26/20 02:38
Isopropylbenzene (Cumene) ug/L ND 0.50 03/26/20 02:38
m&p-Xylene ug/L ND 1.0 03/26/20 02:38
Methyl-tert-butyl ether ug/L ND 0.50 03/26/20 02:38
Methylene Chloride ug/L ND 2.0 03/26/20 02:38
n-Butylbenzene ug/L ND 0.50 03/26/20 02:38
n-Propylbenzene ug/L ND 0.50 03/26/20 02:38
Naphthalene ug/L ND 2.0 03/26/20 02:38
o-Xylene ug/L ND 0.50 03/26/20 02:38
sec-Butylbenzene ug/L ND 0.50 03/26/20 02:38
Styrene ug/L ND 0.50 03/26/20 02:38
tert-Butylbenzene ug/L ND 0.50 03/26/20 02:38
Tetrachloroethene ug/L ND 0.50 03/26/20 02:38
Toluene ug/L ND 0.50 03/26/20 02:38
trans-1,2-Dichloroethene ug/L ND 0.50 03/26/20 02:38
trans-1,3-Dichloropropene ug/L ND 0.50 03/26/20 02:38
Trichloroethene ug/L ND 0.50 03/26/20 02:38
Trichlorofluoromethane ug/L ND 1.0 03/26/20 02:38
Vinyl chloride ug/L ND 1.0 03/26/20 02:38
1,2-Dichloroethane-d4 (S) % 99 70-130 03/26/20 02:38
4-Bromofluorobenzene (S) % 99 70-130 03/26/20 02:38
Toluene-d8 (S) % 105 70-130 03/26/20 02:38
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2842335LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 53.850 108 60-140
1,1,1-Trichloroethane ug/L 52.050 104 60-140
1,1,2,2-Tetrachloroethane ug/L 52.050 104 60-140
1,1,2-Trichloroethane ug/L 55.250 110 60-140
1,1-Dichloroethane ug/L 49.650 99 60-140
1,1-Dichloroethene ug/L 48.650 97 60-140
1,1-Dichloropropene ug/L 53.050 106 60-140
1,2,3-Trichlorobenzene ug/L 56.450 113 60-140
1,2,3-Trichloropropane ug/L 50.450 101 60-140
1,2,4-Trichlorobenzene ug/L 54.250 108 60-140
1,2,4-Trimethylbenzene ug/L 49.450 99 60-140
1,2-Dibromo-3-chloropropane ug/L 54.050 108 60-140
1,2-Dibromoethane (EDB) ug/L 53.650 107 60-140
1,2-Dichlorobenzene ug/L 51.550 103 60-140
1,2-Dichloroethane ug/L 47.950 96 60-140
1,2-Dichloropropane ug/L 51.750 103 60-140
1,3,5-Trimethylbenzene ug/L 49.650 99 60-140
1,3-Dichlorobenzene ug/L 51.450 103 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/30/2020 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92470400
HANDY HOUSE 3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2842335LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 51.950 104 60-140
1,4-Dichlorobenzene ug/L 51.150 102 60-140
2,2-Dichloropropane ug/L 45.450 91 60-140
2-Chlorotoluene ug/L 49.650 99 60-140
4-Chlorotoluene ug/L 51.750 103 60-140
Benzene ug/L 51.050 102 60-140
Bromobenzene ug/L 51.950 104 60-140
Bromochloromethane ug/L 54.550 109 60-140
Bromodichloromethane ug/L 49.550 99 60-140
Bromoform ug/L 51.550 103 60-140
Bromomethane ug/L 55.050 110 60-140
Carbon tetrachloride ug/L 50.850 102 60-140
Chlorobenzene ug/L 51.350 103 60-140
Chloroethane ug/L 44.250 88 60-140
Chloroform ug/L 50.150 100 60-140
Chloromethane ug/L 41.450 83 60-140
cis-1,2-Dichloroethene ug/L 50.850 102 60-140
cis-1,3-Dichloropropene ug/L 51.850 104 60-140
Dibromochloromethane ug/L 56.250 112 60-140
Dibromomethane ug/L 54.650 109 60-140
Dichlorodifluoromethane ug/L 42.950 86 60-140
Diisopropyl ether ug/L 51.750 103 60-140
Ethylbenzene ug/L 49.250 98 60-140
Hexachloro-1,3-butadiene ug/L 50.050 100 60-140
Isopropylbenzene (Cumene) ug/L 51.250 102 60-140
m&p-Xylene ug/L 100100 100 60-140
Methyl-tert-butyl ether ug/L 52.150 104 60-140
Methylene Chloride ug/L 47.650 95 60-140
n-Butylbenzene ug/L 46.450 93 60-140
n-Propylbenzene ug/L 48.450 97 60-140
Naphthalene ug/L 53.850 108 60-140
o-Xylene ug/L 51.050 102 60-140
sec-Butylbenzene ug/L 47.750 95 60-140
Styrene ug/L 51.350 103 60-140
tert-Butylbenzene ug/L 42.150 84 60-140
Tetrachloroethene ug/L 48.250 96 60-140
Toluene ug/L 48.650 97 60-140
trans-1,2-Dichloroethene ug/L 49.050 98 60-140
trans-1,3-Dichloropropene ug/L 50.950 102 60-140
Trichloroethene ug/L 53.050 106 60-140
Trichlorofluoromethane ug/L 43.250 86 60-140
Vinyl chloride ug/L 49.450 99 60-140
1,2-Dichloroethane-d4 (S) % 96 70-130
4-Bromofluorobenzene (S) % 103 70-130
Toluene-d8 (S) % 99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/30/2020 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92470400
HANDY HOUSE 3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2842336MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92470400003
2842337
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 200 112 60-140111 1 30200ND 224 222
1,1,1-Trichloroethane ug/L 200 115 60-140116 1 30200ND 230 231
1,1,2,2-Tetrachloroethane ug/L 200 109 60-140107 2 30200ND 217 213
1,1,2-Trichloroethane ug/L 200 118 60-140119 1 30200ND 236 239
1,1-Dichloroethane ug/L 200 109 60-140112 2 30200ND 218 224
1,1-Dichloroethene ug/L 200 113 60-140115 2 30200ND 225 230
1,1-Dichloropropene ug/L 200 116 60-140119 2 30200ND 232 238
1,2,3-Trichlorobenzene ug/L 200 105 60-140117 10 30200ND 210 233
1,2,3-Trichloropropane ug/L 200 109 60-140109 0 30200ND 218 219
1,2,4-Trichlorobenzene ug/L 200 106 60-140111 4 30200ND 213 222
1,2,4-Trimethylbenzene ug/L 200 81 60-14095 3 30200972 1130 1160
1,2-Dibromo-3-
chloropropane ug/L 200 106 60-140113 6 30200ND 212 226
1,2-Dibromoethane (EDB) ug/L 200 112 60-140110 2 30200ND 224 221
1,2-Dichlorobenzene ug/L 200 102 60-140110 7 30200ND 204 219
1,2-Dichloroethane ug/L 200 102 60-140104 2 30200ND 204 207
1,2-Dichloropropane ug/L 200 110 60-140111 1 30200ND 220 223
1,3,5-Trimethylbenzene ug/L M1200 292 60-140302 3 30200ND 585 604
1,3-Dichlorobenzene ug/L 200 104 60-140108 4 30200ND 208 217
1,3-Dichloropropane ug/L 200 108 60-140108 0 30200ND 215 216
1,4-Dichlorobenzene ug/L 200 100 60-140105 4 30200ND 201 210
2,2-Dichloropropane ug/L 200 84 60-14082 3 30200ND 167 163
2-Chlorotoluene ug/L M1200 113 60-140141 22 30200ND 226 282
4-Chlorotoluene ug/L 200 107 60-140111 4 30200ND 213 223
Benzene ug/L 200 114 60-140113 1 30200ND 228 226
Bromobenzene ug/L 200 108 60-140108 0 30200ND 215 215
Bromochloromethane ug/L 200 117 60-140115 2 30200ND 234 230
Bromodichloromethane ug/L 200 104 60-140106 2 30200ND 208 212
Bromoform ug/L 200 103 60-140100 3 30200ND 206 200
Bromomethane ug/L 200 76 60-14096 23 30200ND 152 192
Carbon tetrachloride ug/L 200 111 60-140116 4 30200ND 222 232
Chlorobenzene ug/L 200 110 60-140110 1 30200ND 219 221
Chloroethane ug/L 200 109 60-140110 1 30200ND 218 220
Chloroform ug/L 200 118 60-140119 1 30200ND 236 238
Chloromethane ug/L 200 90 60-14089 1 30200ND 180 179
cis-1,2-Dichloroethene ug/L 200 111 60-140114 2 30200ND 223 227
cis-1,3-Dichloropropene ug/L 200 105 60-140104 0 30200ND 209 209
Dibromochloromethane ug/L 200 110 60-140115 4 30200ND 219 229
Dibromomethane ug/L 200 111 60-140119 7 30200ND 222 239
Dichlorodifluoromethane ug/L 200 109 60-140111 1 30200ND 219 222
Diisopropyl ether ug/L 200 112 60-140111 1 30200ND 223 222
Ethylbenzene ug/L 200 104 60-140100 1 30200338 547 539
Hexachloro-1,3-butadiene ug/L 200 100 60-140109 9 30200ND 199 219
Isopropylbenzene
(Cumene)
ug/L 200 112 60-140110 1 3020055.7 280 276
m&p-Xylene ug/L 400 105 60-140105 0 30400348 767 767
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/30/2020 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92470400
HANDY HOUSE 3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2842336MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92470400003
2842337
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Methyl-tert-butyl ether ug/L 200 112 60-140112 0 30200ND 224 224
Methylene Chloride ug/L 200 110 60-140110 0 30200ND 219 220
n-Butylbenzene ug/L 200 123 60-140127 3 30200ND 246 253
n-Propylbenzene ug/L M1200 167 60-140173 4 30200ND 334 347
Naphthalene ug/L 200 94 60-140121 10 30200332 521 574
o-Xylene ug/L 200 114 60-140106 2 30200386 613 598
sec-Butylbenzene ug/L 200 104 60-140107 3 30200ND 208 214
Styrene ug/L 200 107 60-140108 1 30200ND 214 215
tert-Butylbenzene ug/L 200 90 60-14093 3 30200ND 180 185
Tetrachloroethene ug/L 200 109 60-140110 1 30200ND 218 219
Toluene ug/L 200 109 60-140109 1 302007.9 225 227
trans-1,2-Dichloroethene ug/L 200 111 60-140113 1 30200ND 223 226
trans-1,3-Dichloropropene ug/L 200 105 60-140105 0 30200ND 210 209
Trichloroethene ug/L 200 117 60-140119 2 30200ND 234 238
Trichlorofluoromethane ug/L 200 107 60-140106 1 30200ND 215 213
Vinyl chloride ug/L 200 124 60-140127 2 30200ND 249 255
1,2-Dichloroethane-d4 (S) % 104 70-130102
4-Bromofluorobenzene (S) % 101 70-130101
Toluene-d8 (S) % 102 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/30/2020 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92470400
HANDY HOUSE 3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
532457
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples: 92470400006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2842344
Associated Lab Samples:92470400006
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 03/26/20 12:48
1,1,1-Trichloroethane ug/L ND 0.50 03/26/20 12:48
1,1,2,2-Tetrachloroethane ug/L ND 0.50 03/26/20 12:48
1,1,2-Trichloroethane ug/L ND 0.50 03/26/20 12:48
1,1-Dichloroethane ug/L ND 0.50 03/26/20 12:48
1,1-Dichloroethene ug/L ND 0.50 03/26/20 12:48
1,1-Dichloropropene ug/L ND 0.50 03/26/20 12:48
1,2,3-Trichlorobenzene ug/L ND 2.0 03/26/20 12:48
1,2,3-Trichloropropane ug/L ND 0.50 03/26/20 12:48
1,2,4-Trichlorobenzene ug/L ND 2.0 03/26/20 12:48
1,2,4-Trimethylbenzene ug/L ND 0.50 03/26/20 12:48
1,2-Dibromo-3-chloropropane ug/L ND 1.0 03/26/20 12:48
1,2-Dibromoethane (EDB) ug/L ND 0.50 03/26/20 12:48
1,2-Dichlorobenzene ug/L ND 0.50 03/26/20 12:48
1,2-Dichloroethane ug/L ND 0.50 03/26/20 12:48
1,2-Dichloropropane ug/L ND 0.50 03/26/20 12:48
1,3,5-Trimethylbenzene ug/L ND 0.50 03/26/20 12:48
1,3-Dichlorobenzene ug/L ND 0.50 03/26/20 12:48
1,3-Dichloropropane ug/L ND 0.50 03/26/20 12:48
1,4-Dichlorobenzene ug/L ND 0.50 03/26/20 12:48
2,2-Dichloropropane ug/L ND 0.50 03/26/20 12:48
2-Chlorotoluene ug/L ND 0.50 03/26/20 12:48
4-Chlorotoluene ug/L ND 0.50 03/26/20 12:48
Benzene ug/L ND 0.50 03/26/20 12:48
Bromobenzene ug/L ND 0.50 03/26/20 12:48
Bromochloromethane ug/L ND 0.50 03/26/20 12:48
Bromodichloromethane ug/L ND 0.50 03/26/20 12:48
Bromoform ug/L ND 0.50 03/26/20 12:48
Bromomethane ug/L ND 5.0 03/26/20 12:48
Carbon tetrachloride ug/L ND 0.50 03/26/20 12:48
Chlorobenzene ug/L ND 0.50 03/26/20 12:48
Chloroethane ug/L ND 1.0 03/26/20 12:48
Chloroform ug/L ND 0.50 03/26/20 12:48
Chloromethane ug/L ND 1.0 03/26/20 12:48
cis-1,2-Dichloroethene ug/L ND 0.50 03/26/20 12:48
cis-1,3-Dichloropropene ug/L ND 0.50 03/26/20 12:48
Dibromochloromethane ug/L ND 0.50 03/26/20 12:48
Dibromomethane ug/L ND 0.50 03/26/20 12:48
Dichlorodifluoromethane ug/L ND 0.50 03/26/20 12:48
Diisopropyl ether ug/L ND 0.50 03/26/20 12:48
Ethylbenzene ug/L ND 0.50 03/26/20 12:48
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/30/2020 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92470400
HANDY HOUSE 3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2842344
Associated Lab Samples:92470400006
Matrix: Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 2.0 03/26/20 12:48
Isopropylbenzene (Cumene) ug/L ND 0.50 03/26/20 12:48
m&p-Xylene ug/L ND 1.0 03/26/20 12:48
Methyl-tert-butyl ether ug/L ND 0.50 03/26/20 12:48
Methylene Chloride ug/L ND 2.0 03/26/20 12:48
n-Butylbenzene ug/L ND 0.50 03/26/20 12:48
n-Propylbenzene ug/L ND 0.50 03/26/20 12:48
Naphthalene ug/L ND 2.0 03/26/20 12:48
o-Xylene ug/L ND 0.50 03/26/20 12:48
sec-Butylbenzene ug/L ND 0.50 03/26/20 12:48
Styrene ug/L ND 0.50 03/26/20 12:48
tert-Butylbenzene ug/L ND 0.50 03/26/20 12:48
Tetrachloroethene ug/L ND 0.50 03/26/20 12:48
Toluene ug/L ND 0.50 03/26/20 12:48
trans-1,2-Dichloroethene ug/L ND 0.50 03/26/20 12:48
trans-1,3-Dichloropropene ug/L ND 0.50 03/26/20 12:48
Trichloroethene ug/L ND 0.50 03/26/20 12:48
Trichlorofluoromethane ug/L ND 1.0 03/26/20 12:48
Vinyl chloride ug/L ND 1.0 03/26/20 12:48
1,2-Dichloroethane-d4 (S) % 98 70-130 03/26/20 12:48
4-Bromofluorobenzene (S) % 100 70-130 03/26/20 12:48
Toluene-d8 (S) % 100 70-130 03/26/20 12:48
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2842345LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 56.450 113 60-140
1,1,1-Trichloroethane ug/L 55.050 110 60-140
1,1,2,2-Tetrachloroethane ug/L 53.850 108 60-140
1,1,2-Trichloroethane ug/L 57.250 114 60-140
1,1-Dichloroethane ug/L 52.750 105 60-140
1,1-Dichloroethene ug/L 52.550 105 60-140
1,1-Dichloropropene ug/L 57.850 116 60-140
1,2,3-Trichlorobenzene ug/L 62.650 125 60-140
1,2,3-Trichloropropane ug/L 51.150 102 60-140
1,2,4-Trichlorobenzene ug/L 59.850 120 60-140
1,2,4-Trimethylbenzene ug/L 53.350 107 60-140
1,2-Dibromo-3-chloropropane ug/L 57.150 114 60-140
1,2-Dibromoethane (EDB) ug/L 56.550 113 60-140
1,2-Dichlorobenzene ug/L 56.850 114 60-140
1,2-Dichloroethane ug/L 49.650 99 60-140
1,2-Dichloropropane ug/L 54.050 108 60-140
1,3,5-Trimethylbenzene ug/L 53.850 108 60-140
1,3-Dichlorobenzene ug/L 55.950 112 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/30/2020 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92470400
HANDY HOUSE 3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2842345LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 53.650 107 60-140
1,4-Dichlorobenzene ug/L 54.750 109 60-140
2,2-Dichloropropane ug/L 55.050 110 60-140
2-Chlorotoluene ug/L 54.450 109 60-140
4-Chlorotoluene ug/L 55.850 112 60-140
Benzene ug/L 55.950 112 60-140
Bromobenzene ug/L 55.050 110 60-140
Bromochloromethane ug/L 56.550 113 60-140
Bromodichloromethane ug/L 52.250 104 60-140
Bromoform ug/L 55.050 110 60-140
Bromomethane ug/L 59.650 119 60-140
Carbon tetrachloride ug/L 55.650 111 60-140
Chlorobenzene ug/L 54.350 109 60-140
Chloroethane ug/L 45.150 90 60-140
Chloroform ug/L 54.750 109 60-140
Chloromethane ug/L 44.550 89 60-140
cis-1,2-Dichloroethene ug/L 53.750 107 60-140
cis-1,3-Dichloropropene ug/L 55.950 112 60-140
Dibromochloromethane ug/L 57.750 115 60-140
Dibromomethane ug/L 55.750 111 60-140
Dichlorodifluoromethane ug/L 47.450 95 60-140
Diisopropyl ether ug/L 54.350 109 60-140
Ethylbenzene ug/L 52.850 106 60-140
Hexachloro-1,3-butadiene ug/L 58.050 116 60-140
Isopropylbenzene (Cumene) ug/L 54.850 110 60-140
m&p-Xylene ug/L 108100 108 60-140
Methyl-tert-butyl ether ug/L 54.950 110 60-140
Methylene Chloride ug/L 49.450 99 60-140
n-Butylbenzene ug/L 54.150 108 60-140
n-Propylbenzene ug/L 53.150 106 60-140
Naphthalene ug/L 58.650 117 60-140
o-Xylene ug/L 54.150 108 60-140
sec-Butylbenzene ug/L 52.950 106 60-140
Styrene ug/L 53.850 108 60-140
tert-Butylbenzene ug/L 45.350 91 60-140
Tetrachloroethene ug/L 53.350 107 60-140
Toluene ug/L 53.950 108 60-140
trans-1,2-Dichloroethene ug/L 53.150 106 60-140
trans-1,3-Dichloropropene ug/L 55.050 110 60-140
Trichloroethene ug/L 56.650 113 60-140
Trichlorofluoromethane ug/L 46.650 93 60-140
Vinyl chloride ug/L 55.450 111 60-140
1,2-Dichloroethane-d4 (S) % 98 70-130
4-Bromofluorobenzene (S) % 101 70-130
Toluene-d8 (S) % 99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/30/2020 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92470400
HANDY HOUSE 3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2843777MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92470366001
2843778
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 114 60-140112 2 3020ND 22.8 22.5
1,1,1-Trichloroethane ug/L 20 118 60-140116 2 3020ND 23.7 23.2
1,1,2,2-Tetrachloroethane ug/L 20 110 60-140107 2 3020ND 22.0 21.5
1,1,2-Trichloroethane ug/L 20 120 60-140118 1 3020ND 23.9 23.6
1,1-Dichloroethane ug/L 20 115 60-140114 1 3020ND 23.0 22.8
1,1-Dichloroethene ug/L 20 114 60-140113 1 3020ND 22.9 22.6
1,1-Dichloropropene ug/L 20 122 60-140119 2 3020ND 24.3 23.8
1,2,3-Trichlorobenzene ug/L 20 108 60-140110 2 3020ND 21.5 22.0
1,2,3-Trichloropropane ug/L 20 107 60-140104 3 3020ND 21.5 20.8
1,2,4-Trichlorobenzene ug/L 20 109 60-140107 2 3020ND 21.8 21.4
1,2,4-Trimethylbenzene ug/L 20 103 60-140117 2 3020150 171 174
1,2-Dibromo-3-
chloropropane ug/L 20 108 60-140108 0 3020ND 21.7 21.6
1,2-Dibromoethane (EDB) ug/L 20 113 60-140117 3 3020ND 22.6 23.3
1,2-Dichlorobenzene ug/L 20 106 60-140106 1 3020ND 21.3 21.1
1,2-Dichloroethane ug/L 20 108 60-140104 3 3020ND 21.6 20.9
1,2-Dichloropropane ug/L 20 112 60-140111 1 3020ND 22.4 22.2
1,3,5-Trimethylbenzene ug/L M120 290 60-140293 1 3020ND 57.9 58.6
1,3-Dichlorobenzene ug/L 20 105 60-140105 0 3020ND 21.0 21.0
1,3-Dichloropropane ug/L 20 111 60-140107 4 3020ND 22.2 21.5
1,4-Dichlorobenzene ug/L 20 106 60-140104 2 3020ND 21.2 20.9
2,2-Dichloropropane ug/L 20 105 60-140104 1 3020ND 21.1 20.8
2-Chlorotoluene ug/L 20 121 60-140122 0 3020ND 24.2 24.3
4-Chlorotoluene ug/L 20 107 60-140106 1 3020ND 21.4 21.1
Benzene ug/L 20 131 60-140130 0 302046.2 72.4 72.2
Bromobenzene ug/L 20 108 60-140105 2 3020ND 21.5 21.0
Bromochloromethane ug/L 20 117 60-140116 0 3020ND 23.3 23.2
Bromodichloromethane ug/L 20 110 60-140106 4 3020ND 22.0 21.2
Bromoform ug/L 20 103 60-140101 3 3020ND 20.6 20.1
Bromomethane ug/L 20 97 60-140104 7 3020ND 19.4 20.9
Carbon tetrachloride ug/L 20 117 60-140114 3 3020ND 23.5 22.9
Chlorobenzene ug/L 20 111 60-140110 1 3020ND 22.3 22.1
Chloroethane ug/L 20 107 60-140107 0 3020ND 21.4 21.4
Chloroform ug/L 20 108 60-140111 3 3020ND 21.5 22.3
Chloromethane ug/L 20 92 60-14093 0 3020ND 18.5 18.5
cis-1,2-Dichloroethene ug/L 20 114 60-140113 1 3020ND 22.9 22.6
cis-1,3-Dichloropropene ug/L 20 112 60-140108 3 3020ND 22.4 21.7
Dibromochloromethane ug/L 20 115 60-140109 5 3020ND 22.9 21.8
Dibromomethane ug/L 20 123 60-140118 4 3020ND 24.6 23.6
Dichlorodifluoromethane ug/L 20 116 60-140117 0 3020ND 23.3 23.4
Diisopropyl ether ug/L 20 131 60-140127 3 3020ND 26.1 25.4
Ethylbenzene ug/L 20 111 60-140112 0 3020147 169 169
Hexachloro-1,3-butadiene ug/L 20 104 60-140104 1 3020ND 20.8 20.9
Isopropylbenzene
(Cumene)
ug/L 20 112 60-140109 1 302010.2 32.5 32.1
m&p-Xylene ug/L E40 112 60-140109 0 3040392 437 436
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/30/2020 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92470400
HANDY HOUSE 3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2843777MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92470366001
2843778
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Methyl-tert-butyl ether ug/L 20 117 60-140112 4 30200.51 24.0 23.0
Methylene Chloride ug/L 20 111 60-140110 1 3020ND 22.2 21.9
n-Butylbenzene ug/L 20 111 60-140113 2 3020ND 22.2 22.6
n-Propylbenzene ug/L M120 205 60-140206 0 3020ND 41.0 41.2
Naphthalene ug/L 20 99 60-140121 8 302034.1 53.8 58.3
o-Xylene ug/L 20 116 60-140115 0 3020167 191 190
sec-Butylbenzene ug/L 20 104 60-140102 2 3020ND 20.7 20.3
Styrene ug/L 20 105 60-140104 1 3020ND 21.0 20.8
tert-Butylbenzene ug/L 20 90 60-14090 0 3020ND 18.1 18.1
Tetrachloroethene ug/L 20 112 60-140109 2 30201.1 23.5 22.9
Toluene ug/L 20 135 60-140131 0 3020142 169 168
trans-1,2-Dichloroethene ug/L 20 114 60-140114 0 3020ND 22.8 22.8
trans-1,3-Dichloropropene ug/L 20 108 60-140109 0 3020ND 21.7 21.8
Trichloroethene ug/L 20 121 60-140116 5 3020ND 24.3 23.1
Trichlorofluoromethane ug/L 20 112 60-140107 4 3020ND 22.3 21.4
Vinyl chloride ug/L 20 127 60-140123 3 3020ND 25.4 24.7
1,2-Dichloroethane-d4 (S) % 103 70-130105
4-Bromofluorobenzene (S) % 102 70-130103
Toluene-d8 (S) % 101 70-13098
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/30/2020 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 52
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92470400
HANDY HOUSE 3
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical NationalPAN
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte concentration exceeded the calibration range. The reported result is estimated.E
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/30/2020 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 52
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92470400
HANDY HOUSE 3
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92470400001 1449867 1449867MW-1 MADEPV MADEP VPH
92470400002 1449867 1449867MW-2 MADEPV MADEP VPH
92470400003 1449867 1449867MW-3 MADEPV MADEP VPH
92470400004 1449867 1449867MW-8 MADEPV MADEP VPH
92470400005 1449867 1449867MW-9 MADEPV MADEP VPH
92470400006 1450627 1450627MW-10 MADEPV MADEP VPH
92470400007 1450627 1450627MW-11 MADEPV MADEP VPH
92470400008 1450627 1450627MW-14 MADEPV MADEP VPH
92470400009 1450627 1450627MW-15 MADEPV MADEP VPH
92470400010 1451334 1451334MW-17 MADEPV MADEP VPH
92470400011 1450627 1450627VEW1MADEPV MADEP VPH
92470400012 1450627 1450627SW-3 MADEPV MADEP VPH
92470400001 532455MW-1 SM 6200B
92470400002 532453MW-2 SM 6200B
92470400003 532455MW-3 SM 6200B
92470400004 532453MW-8 SM 6200B
92470400005 532453MW-9 SM 6200B
92470400006 532457MW-10 SM 6200B
92470400007 532453MW-11 SM 6200B
92470400008 532453MW-14 SM 6200B
92470400009 532453MW-15 SM 6200B
92470400010 532453MW-17 SM 6200B
92470400011 532453VEW1SM 6200B
92470400012 532455SW-3 SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/30/2020 08:33 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 52
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