WI-7595_32692_CA_LTRRPT_20221207

2725 E. Millbrook Road, Suite 121
Raleigh, North Carolina 27604
Telephone [phone]
Fax [phone]
www.oneatlas.com

December 7, 2022

Mr. Mike Haseltine
North Carolina Department of Environmental Quality
Wilmington Regional Office
Division of Waste Management - UST Section
127 Cardinal Drive Extension
Wilmington, North Carolina 28405

Re: Soil Sampling Report
Phoenix #308
13493 N.C. Highway 210
Rocky Point, Pender County, North Carolina
NCDEQ Incident No. 32692
Priority Site Ranking: I172D

Mr. Haseltine:
On behalf of Springer Eubank Co., Inc., ATC Associates of North Carolina, P.C. (ATC) has prepared this letter
report to provide a summary of soil sampling activities, as approved in pre-approval task authorization number
TA-60.

Soil Sampling
On November 1, 2022, soil sampling was performed by ATC to determine if light non-aqueous phase liquid
(LNAPL) is present in proximity to gasoline dispenser 11/12 and to assist in the delineation of petroleum-impacted
soil in proximity to this area at the referenced site. The soil samples were collected for laboratory analyses using
either a field-decontaminated stainless steel hand auger or by using direct push technology. Two soil samples
were collected from each boring location. One soil sample was collected in the unsaturated zone (at a depth of
either 2-3 or 3-5 feet below ground surface (bgs)) and one soil sample was collected in the smear/saturated zone
(at a depth of either 7-9 feet bgs, 9-10 feet bgs, or 9-11 feet bgs).

Upon collection, each soil sample was screened with a PID. The respective PID readings are provided in Table
1. The locations of the soil samples (B-1 through B-7) are depicted on Figure 1. Boring logs are provided in
Attachment I.

All samples were collected into laboratory-supplied containers and shipped on ice to SGS North America, Inc.
(SGS) in Scott, Louisiana. The soil samples collected from the unsaturated zone of each boring was analyzed by
EPA Method 8260 and Massachusetts Department of Environmental Protection (MADEP) method for volatile
petroleum hydrocarbons (VPH). The soil samples collected from the smear/saturated zone of each boring was
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December 7,2022
Page 2 of2
analyzed by Environmental Protection Agency (EPA) Method 8015C for Total Petroleum Hydrocarbons
(TPH)-Gasoline Range Organics (GRO).
Unsaturated Zone
Laboratory analytical results of soil samples B-2 (2-3), B-4 (2-3), B-5 (2-3), and B-7 (3-5) detected target
compound concentrations above Soil-to-Groundwater (STGW) Maximum Contaminant Concentrations (MSCCs)
but below Residential MSCCs.
Based on these analytical results, it appears petroleum-related impacts to soil in the unsaturated zone are not
present above Residential MSCCs.
Smear/Saturated Zone
Laboratory analytical results of soil samples B-2 (7-9), B-5 (7-9), and B-7 (7-9) detected TPH-GRO
concentrations above the State Action Level of 50 micrograms per kilogram (mg/kg).
The soil analytical results are presented in Table 1. Petroleum-related impacts to soil are provided on Figure 3.
A copy of the laboratory report and chain-of-custody documents are provided in Attachment IL
Based on the analytical data,itappears LNAPL is not present near gasoline dispenser 11112 andpetroleum-related
impacts to soilabove Residential MSCCs were not identified.
If you have any questions or require additional information, please contact our office at [phone].
Sincerely,
ATC Associates of North Carolina, P,{\
, )it"**"-adp-r.mr
Maureen Jackson)?.G.
Senior Project Manager
N.C. Licensed Geologist No. 2312
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ffi

TABLE

TABLE 1
SOIL SAMPLE ANALYTICAL RESULTS
PHOENIX #30813493 NC HIGHWAY 210ROCKY POINT, PENDER COUNTY, NORTH CAROLINANCDEQ INCIDENT NO. 32692
EPA METHOD
8015
Sample ID Date Sampled
PID
Reading (ppm)
Sample
Depth (feet)AcetoneBenzenesec-Butylbenzene1,2-DichloropropaneEthylbenzeneIPEIsopropylbenzenep-IsopropyltolueneMethyl Ethyl KetoneMethyl ChlorideNaphthalenen-PropylbenzeneToluene1,1,2-Trichloroethane1,2,3-Trichloropropane1,2,4-Trimehtylbenzene1,3,5-TrimethylbenzeneTotal XylenesTPH-GROC5-C8 AliphaticsC9-C12 AliphaticsC9-C10 AromaticsB-1 (3-5)11/1/22 21.4 3-5 0.0300J 0.0049 0.00083J 0.0015 0.0281 <0.0011 0.0033J 0.00041J <0.014 0.00097J 0.0073 0.0105 0.0194 <0.0011 <0.0054 0.0743 0.0236 0.157 --<7.3 <7.3 <7.3
B-1 (7-9)11/1/22 743.9 7-9 ------------------------------------25.2 ------
B-2 (2-3)11/1/22 2,568 2-3 0.192J <0.037 0.385 <0.074 1.59 <0.074 0.641 0.277J <0.93 <0.37 3.96 3.18 0.212J <0.074 <0.37 22.5E 7.58 9.99 --72.8 135 56.2
B-2 (7-9)11/1/22 699.5 7-9 ------------------------------------242 ------
B-3 (2-3)11/1/22 21.8 2-3 0.0976 0.00054 0.0036J <0.0011 0.161 <0.0011 0.0152 0.0020J 0.0486 <0.0054 0.0273 <0.0054 0.0843 <0.0011 <0.0054 1.33 0.0953 1.49 --<6.4 11.0 4.58J
B-3 (9-11)11/1/22 137.8 9-11 ------------------------------------9.65 ------
B-4 (2-3)11/1/22 20.5 2-3 0.107 0.0391 0.0035J 0.00095J 0.103 <0.0012 0.0118 0.0015J 0.0300 0.0016J 0.0333 0.0455 0.0449 <0.0012 <0.0062 0.604 0.0850 0.497 --<7.5 6.16J <7.5
B-4 (9-10)11/1/22 55.9 9-10 ------------------------------------34.9 ------
B-5 (2-3)11/1/22 20.8 2-3 <3.7 0.0160J 0.0280J 0.0962 0.272 <0.073 0.0472J <0.37 <0.92 <0.37 0.315J 0.238J 0.110J 0.0213J 0.0250J 1.36 0.421 1.54 --7.46 21.1 8.66
B-5 (7-9)11/1/22 5,661 7-9 ------------------------------------452 ------
B-6 (3-5)11/1/22 34.0 3-5 0.0178J 0.0052 <0.0047 0.00065J 0.0200 <0.00094 0.0015J <0.0047 <0.012 0.0011J 0.00093J 0.0042J 0.0224 <0.00094 <0.0047 0.0183 0.0064 0.0854 --<5.4 <5.4 <5.4
B-6 (7-9)11/1/22 109.2 7-9 ------------------------------------8.42 ------
B-7 (3-5)11/1/22 57.0 3-5 0.0359J 0.0110 0.00056J <0.0011 0.0345 0.00020J 0.0029J <0.0055 0.0097J <0.0055 0.0056 0.0087 0.0593 <0.0011 <0.0055 0.0423 0.0146 0.167 --<6.3 <6.3 <6.3
B-7 (7-9)11/1/22 1,849 7-9 ------------------------------------1,440 ------
------------------------------------50 ------
24 0.0072 2.2 0.003 8 0.32 1.3 0.12 16 0.014 0.2 1.4 5.4 0.0032 NE 6.6 6.6 6 --68 540 31
14,000 12 1,560 17.9 60.3 156 1,560 1,560 9,380 51 5.5 1,560 1,250 11.6 NE 156 156 3,120 --939 1,500 469
Notes:
1. Concentrations reported in milligrams per kilogram (mg/kg).
2. Bold type indicates compound concentration was detected above Soil-to-Groundwater MSCC.3. "<" = not detected at or above the laboratory detection limit.
4. E denotes value exceeds calibration range.
5. J denotes compound concentration estimated by project laboratory.6. MSCC denotes maximum soil contaminant concentration.
Residential MSCC (mg/kg)
ANALTYICAL METHOD
State Action Level (mg/kg)
EPA METHOD 8260 MADEP METHOD for VPH
Soil-to-Groundwater MSCC (mg/kg)

FIGURES

NORTH CAROLINA HIGHWAY 210MW-14MW-27MW-8MW-3RMW-15RW-2MW-2RW-3MW-4MW-23MW-9DW-1MW-16MW-12RW-1PHOENIX #308TRAVEL CENTERDIESEL ISLANDCANOPYMW-26MW-7MW-10MW-25UST 3SEPTICTANKSANDLEACHFIELDSUST1&2MW-34MW-6MW-5TRUCKSCALESMW-18MW-17MW-13MW-19MW-21MW-20MW-24SEE FIGURE 2 & 3GASOLINE ISLAND CANOPYMW-1RW-5RW-4AS-26
MW-8MW-3RRW-2MW-2RW-3MW-4MW-9MW-16RW-1MW-7UST1&2MW-6MW-5MW-18MW-17B7B4B2B3*DISPENSERGASOLINE ISLAND CANOPYMW-1RW-5RW-4B5MW-34B1*AS-26B6*
MW-8MW-3RRW-2MW-2RW-3MW-4MW-9RW-1MW-7UST1&2MW-6MW-5MW-18MW-17B7B4B2B3*DISPENSERGASOLINE ISLAND CANOPYMW-1RW-5RW-4B5MW-34B1*AS-26B6**

ATTACHMENT I

11-16-2022 S:\Enviro\Worsley\Phoenix #308\Boring Logs\B-1.borATC Project No. PHX308TA60
Rocky Point, Pender County, North Carolina
13493 NC Highway 210
Phoenix #308
Boring terminated at 12 feet bgs.
PID = Photoionization detector.
PPM = Parts per million.
DPT = Direct push technology.
BORING LOG: B-1
(Page 1 of 1)
Date(s) Drilled : 11/1/2022
Drilling Contractor : Probe Utility
Drilling Method : Hand Auger/DPT
Boring Diameter : 3 Inches
Sampling Method : Soil Cuttings
Sampling Interval : Continuous
Logged By : Chris Hanley
Depth In Feet0
1
2
3
4
5
6
7
8
9
10
11
12 USCSAR
SW
SW
CL GRAPHICDESCRIPTION
Asphalt
Light gray/light brown SAND, fine grained, dry
Light gray/light brown SAND, fine grained, moist, some petroleum odor
Light brown/dark tan sandy CLAY, medium plasticity, sand is fine grained, wet, petroelum
odor.
End of boring
PID (ppm)
Sample ID
3.3
21.4
B-1(3-5)
13.4
743.9
B-1(7-9)
193.2
11-16-2022 S:\Enviro\Worsley\Phoenix #308\Boring Logs\B-2.borATC Project No. PHX308TA60
Rocky Point, Pender County, North Carolina
13493 NC Highway 210
Phoenix #308
Boring terminated at 12 feet bgs.
PID = Photoionization detector.
PPM = Parts per million.
DPT = Direct push technology.
BORING LOG: B-2
(Page 1 of 1)
Date(s) Drilled : 11/1/2022
Drilling Contractor : Probe Utility
Drilling Method : Hand Auger/DPT
Boring Diameter : 3 Inches
Sampling Method : Soil Cuttings
Sampling Interval : Continuous
Logged By : Chris Hanley
Depth In Feet0
1
2
3
4
5
6
7
8
9
10 USCSAR
SW
SW
SW
SW
CL GRAPHICDESCRIPTION
Concrete
Light gray/light brown SAND, fine grained, dry
Black SAND, fine grained, dry, strong petroleum odor
Light gray/light brown SAND, fine grained, dry
Light gray/light brown SAND, fine grained, moist
Light gray/light brown, sandy CLAY, medium plasticity, sand is fine grained, wet
End of boring
PID (ppm)
Sample ID
12.4
2,568
B-2(2-3)
182.1
46.0
699.5
B-2(7-9)
211.6
11-16-2022 S:\Enviro\Worsley\Phoenix #308\Boring Logs\B-3.borATC Project No. PHX308TA60
Rocky Point, Pender County, North Carolina
13493 NC Highway 210
Phoenix #308
Boring terminated at 12 feet bgs.
PID = Photoionization detector.
PPM = Parts per million.
DPT = Direct push technology.
BORING LOG: B-3
(Page 1 of 1)
Date(s) Drilled : 11/1/2022
Drilling Contractor : Probe Utility
Drilling Method : Hand Auger/DPT
Boring Diameter : 3 Inches
Sampling Method : Soil Cuttings
Sampling Interval : Continuous
Logged By : Chris Hanley
Depth In Feet0
1
2
3
4
5
6
7
8
9
10
11
12 USCSAR
SW
SW
SW
CL GRAPHICDESCRIPTION
Concrete
Light gray/light brown SAND, fine grained, dry
Black/dark grey SAND, fine grained, dry, strong petroleum odor
Light gray/light brown SAND, fine grained, dry
No Recovery using Direct Push Technology.
Dark grey to orange CLAY, high plasticity, saturated
End of boring
PID (ppm)
Sample ID
8.0
21.8
B-3(2-3)
1.9
137.8
B-3(9-11)
15.3
11-16-2022 S:\Enviro\Worsley\Phoenix #308\Boring Logs\B-4.borATC Project No. PHX308TA60
Rocky Point, Pender County, North Carolina
13493 NC Highway 210
Phoenix #308
Boring terminated at 12 feet bgs.
PID = Photoionization detector.
PPM = Parts per million.
DPT = Direct push technology.
BORING LOG: B-4
(Page 1 of 1)
Date(s) Drilled : 11/1/2022
Drilling Contractor : Probe Utility
Drilling Method : Hand Auger/DPT
Boring Diameter : 3 Inches
Sampling Method : Soil Cuttings
Sampling Interval : Continuous
Logged By : Chris Hanley
Depth In Feet0
1
2
3
4
5
6
7
8
9
10 USCSAR
SW
SW
SW
SW
CL GRAPHICDESCRIPTION
Concrete
Light gray/light brown SAND, fine grained, dry
Dark grey SAND, fine grained, dry
Light gray/light brown SAND, fine grained, dry
Light gray/light brown SAND, fine grained, moist
Light gray sandy CLAY, low plasticity, wet
End of boring
PID (ppm)
Sample ID
0.8
20.5
B-4(2-3)
17.8
6.4
17.9
55.9
B-4(9-10)
11-16-2022 S:\Enviro\Worsley\Phoenix #308\Boring Logs\B-5.borATC Project No. PHX308TA60
Rocky Point, Pender County, North Carolina
13493 NC Highway 210
Phoenix #308
Boring terminated at 12 feet bgs.
PID = Photoionization detector.
PPM = Parts per million.
DPT = Direct push technology.
BORING LOG: B-5
(Page 1 of 1)
Date(s) Drilled : 11/1/2022
Drilling Contractor : Probe Utility
Drilling Method : Hand Auger/DPT
Boring Diameter : 3 Inches
Sampling Method : Soil Cuttings
Sampling Interval : Continuous
Logged By : Chris Hanley
Depth In Feet0
1
2
3
4
5
6
7
8
9
10 USCSAR
SW
SW
SW
SW
CL GRAPHICDESCRIPTION
Concrete
Light gray/light brown SAND, fine grained, dry
Dark grey SAND, fine grained, dry
Light gray/light brown SAND, fine grained, dry
Light gray/light brown SAND, fine grained, moist, strong petroleum odor
Light gray clayey SAND, wet, strong odor
End of boring
PID (ppm)
Sample ID
1.0
20.8
B-5(2-3)
7.3
38.9
5,661
B-5(7-9)
370.2
11-16-2022 S:\Enviro\Worsley\Phoenix #308\Boring Logs\B-6.borATC Project No. PHX308TA60
Rocky Point, Pender County, North Carolina
13493 NC Highway 210
Phoenix #308
Boring terminated at 12 feet bgs.
PID = Photoionization detector.
PPM = Parts per million.
DPT = Direct push technology.
BORING LOG: B-6
(Page 1 of 1)
Date(s) Drilled : 11/1/2022
Drilling Contractor : Probe Utility
Drilling Method : Hand Auger/DPT
Boring Diameter : 3 Inches
Sampling Method : Soil Cuttings
Sampling Interval : Continuous
Logged By : Chris Hanley
Depth In Feet0
1
2
3
4
5
6
7
8
9
10 USCSAR
SW
SW
SW
SW
CL GRAPHICDESCRIPTION
Concrete
Light gray/light brown SAND, fine grained, dry
Black SAND, fine grained, dry, strong petroleum odor
Light gray/light brown SAND, fine grained, dry
Light gray/light brown SAND, fine grained, moist
Light gray/light brown, sandy CLAY, medium plasticity, sand is fine grained, wet
End of boring
PID (ppm)
Sample ID
0.4
14.9
34.0
B-6(3-5)
19.0
109.2
B-6(7-9)
11.9
11-16-2022 S:\Enviro\Worsley\Phoenix #308\Boring Logs\B-7.borATC Project No. PHX308TA60
Rocky Point, Pender County, North Carolina
13493 NC Highway 210
Phoenix #308
Boring terminated at 12 feet bgs.
PID = Photoionization detector.
PPM = Parts per million.
DPT = Direct push technology.
BORING LOG: B-7
(Page 1 of 1)
Date(s) Drilled : 11/1/2022
Drilling Contractor : Probe Utility
Drilling Method : Hand Auger/DPT
Boring Diameter : 3 Inches
Sampling Method : Soil Cuttings
Sampling Interval : Continuous
Logged By : Chris Hanley
Depth In Feet0
1
2
3
4
5
6
7
8
9
10 USCSAR
SW
SW
SW
SW
CL GRAPHICDESCRIPTION
Concrete
Light gray/light brown SAND, fine grained, dry
Dark grey SAND, fine grained, dry
Light gray/light brown SAND, fine grained, dry
Light gray/light brown SAND, fine grained, moist, strong petroleum odor
Light gray clayey SAND, wet, strong odor
End of boring
PID (ppm)
Sample ID
4.1
12.0
57.0
B-7(3-5)
107.5
1,849
B-7(7-9)
408.7

ATTACHMENT II
11/23/22
Technical Report for
Atlas
Phoenix 308-Rocky PT, NC
SGS Job Number: LA84954
Sampling Date: 11/01/22
Report to:
ATC Group Services LLC.
2725 East Millbrook Road Suite 121
Raleigh, NC 27604
[e-mail]
ATTN: Maureen Jackson
Total number of pages in report:
Certifications: LDEQ(2048), LDHH(LA150012), AR(14-045-04), AZ(AZ0805), FL(E87657), IL(200082), KY(#31),
NC(487), SC(73004001), NJ(LA007), TX(T104704186-18-16), WV(257)
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 500 Ambassador Caffery • Scott, LA 70583 • tel: [phone]
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Rebecca Hebert 337-237-4775
Ron Benjamin
Lab Director
Scott, LA 11/23/22
e-Hardcopy 2.0
Automated Report
90
SGS is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
Review standard terms at: http://www.sgs.com/en/terms-and-conditions
The results set forth herein are provided by SGS North America Inc.
Please share your ideas about
how we can serve you better at:
[e-mail]
1 of 90
LA84954
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................5
Section 3: Sample Results ........................................................................................................9
3.1: LA84954-1: B-1 (3-5) ...................................................................................................10
3.2: LA84954-2: B-1 (7-9) ...................................................................................................14
3.3: LA84954-3: B-2 (2-3) ...................................................................................................15
3.4: LA84954-4: B-2 (7-9) ...................................................................................................19
3.5: LA84954-5: B-3 (2-3) ...................................................................................................20
3.6: LA84954-6: B-3 (9-11) .................................................................................................24
3.7: LA84954-7: B-4 (2-3) ...................................................................................................25
3.8: LA84954-8: B-4 (9-10) .................................................................................................29
3.9: LA84954-9: B-5 (2-3) ...................................................................................................30
3.10: LA84954-10: B-5 (7-9) ...............................................................................................34
3.11: LA84954-11: B-6 (3-5) ...............................................................................................35
3.12: LA84954-12: B-6 (7-9) ...............................................................................................39
3.13: LA84954-13: B-7 (3-5) ...............................................................................................40
3.14: LA84954-14: B-7 (7-9) ...............................................................................................44
Section 4: Misc. Forms ............................................................................................................45
4.1: Chain of Custody ...........................................................................................................46
Section 5: MS Volatiles - QC Data Summaries .....................................................................52
5.1: Method Blank Summary ................................................................................................53
5.2: Blank Spike/Blank Spike Duplicate Summary ..............................................................63
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................73
Section 6: GC Volatiles - QC Data Summaries .....................................................................79
6.1: Method Blank Summary ................................................................................................80
6.2: Blank Spike/Blank Spike Duplicate Summary ..............................................................84
6.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................88
6.4: Duplicate Summary .......................................................................................................90 1234562 of 90
LA84954
SGS North America Inc.
Sample Summary
Atlas
Job No:LA84954
Phoenix 308-Rocky PT, NC
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
This report contains results reported as ND = Not detected. The following applies:
Organics ND = Not detected above the MDL
LA84954-1 11/01/22 12:00 CH 11/03/22 SO Soil B-1 (3-5)
LA84954-2 11/01/22 12:05 CH 11/03/22 SO Soil B-1 (7-9)
LA84954-3 11/01/22 12:30 CH 11/03/22 SO Soil B-2 (2-3)
LA84954-4 11/01/22 12:35 CH 11/03/22 SO Soil B-2 (7-9)
LA84954-5 11/01/22 13:00 CH 11/03/22 SO Soil B-3 (2-3)
LA84954-6 11/01/22 13:05 CH 11/03/22 SO Soil B-3 (9-11)
LA84954-7 11/01/22 13:25 CH 11/03/22 SO Soil B-4 (2-3)
LA84954-8 11/01/22 13:30 CH 11/03/22 SO Soil B-4 (9-10)
LA84954-9 11/01/22 13:45 CH 11/03/22 SO Soil B-5 (2-3)
LA84954-10 11/01/22 13:50 CH 11/03/22 SO Soil B-5 (7-9)
LA84954-11 11/01/22 15:00 CH 11/03/22 SO Soil B-6 (3-5)
LA84954-12 11/01/22 15:05 CH 11/03/22 SO Soil B-6 (7-9)
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
3 of 90
LA849541
SGS North America Inc.
Sample Summary
(continued)
Atlas
Job No:LA84954
Phoenix 308-Rocky PT, NC
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
LA84954-13 11/01/22 15:25 CH 11/03/22 SO Soil B-7 (3-5)
LA84954-14 11/01/22 15:30 CH 11/03/22 SO Soil B-7 (7-9)
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
4 of 90
LA849541
Summary of Hits Page 1 of 4
Job Number:LA84954
Account:Atlas
Project:Phoenix 308-Rocky PT, NC
Collected:11/01/22
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
LA84954-1 B-1 (3-5)
Acetone 0.0300 J 0.054 0.0024 mg/kg SW846 8260D
Benzene 0.0049 0.00054 0.00021 mg/kg SW846 8260D
sec-Butylbenzene 0.00083 J 0.0054 0.00036 mg/kg SW846 8260D
1,2-Dichloropropane 0.0015 0.0011 0.00014 mg/kg SW846 8260D
Ethylbenzene 0.0281 0.0011 0.00028 mg/kg SW846 8260D
Isopropylbenzene 0.0033 J 0.0054 0.00031 mg/kg SW846 8260D
p-Isopropyltoluene 0.00041 J 0.0054 0.00037 mg/kg SW846 8260D
Methyl Chloride 0.00097 J 0.0054 0.00032 mg/kg SW846 8260D
Naphthalene 0.0073 0.0054 0.00062 mg/kg SW846 8260D
n-Propylbenzene 0.0105 0.0054 0.00046 mg/kg SW846 8260D
Toluene 0.0194 0.0054 0.00020 mg/kg SW846 8260D
1,2,4-Trimethylbenzene 0.0743 0.0054 0.00041 mg/kg SW846 8260D
1,3,5-Trimethylbenzene 0.0236 0.0054 0.00027 mg/kg SW846 8260D
m,p-Xylene 0.103 0.0022 0.00049 mg/kg SW846 8260D
o-Xylene 0.0536 0.0011 0.00028 mg/kg SW846 8260D
Xylene (total)0.157 0.0022 0.0013 mg/kg SW846 8260D
LA84954-2 B-1 (7-9)
TPH-GRO (C6-C10)25.2 6.5 3.2 mg/kg SW846 8015C
LA84954-3 B-2 (2-3)
Acetone 0.192 J 3.7 0.16 mg/kg SW846 8260D
sec-Butylbenzene 0.385 0.37 0.024 mg/kg SW846 8260D
Ethylbenzene 1.59 0.074 0.019 mg/kg SW846 8260D
Isopropylbenzene 0.641 0.37 0.021 mg/kg SW846 8260D
p-Isopropyltoluene 0.277 J 0.37 0.025 mg/kg SW846 8260D
Naphthalene 3.96 0.37 0.043 mg/kg SW846 8260D
n-Propylbenzene 3.18 0.37 0.032 mg/kg SW846 8260D
Toluene 0.212 J 0.37 0.013 mg/kg SW846 8260D
1,2,4-Trimethylbenzene a 22.5 E 0.37 0.028 mg/kg SW846 8260D
1,3,5-Trimethylbenzene 7.58 0.37 0.019 mg/kg SW846 8260D
m,p-Xylene 7.04 0.15 0.034 mg/kg SW846 8260D
o-Xylene 2.95 0.074 0.019 mg/kg SW846 8260D
Xylene (total)9.99 0.15 0.086 mg/kg SW846 8260D
C5- C8 Aliphatics (Unadj.)72.8 7.7 3.8 mg/kg MADEP VPH REV 2.1
C9- C12 Aliphatics (Unadj.)135 15 7.3 mg/kg MADEP VPH REV 2.1
C9- C10 Aromatics (Unadj.)56.2 15 7.3 mg/kg MADEP VPH REV 2.1
LA84954-4 B-2 (7-9)
TPH-GRO (C6-C10)242 6.7 3.3 mg/kg SW846 8015C
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Summary of Hits Page 2 of 4
Job Number:LA84954
Account:Atlas
Project:Phoenix 308-Rocky PT, NC
Collected:11/01/22
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
LA84954-5 B-3 (2-3)
Acetone 0.0976 0.054 0.0024 mg/kg SW846 8260D
Benzene 0.0265 0.00054 0.00022 mg/kg SW846 8260D
sec-Butylbenzene 0.0036 J 0.0054 0.00036 mg/kg SW846 8260D
Ethylbenzene 0.161 0.0011 0.00028 mg/kg SW846 8260D
Isopropylbenzene 0.0152 0.0054 0.00031 mg/kg SW846 8260D
p-Isopropyltoluene 0.0020 J 0.0054 0.00037 mg/kg SW846 8260D
Methyl Ethyl Ketone 0.0486 0.014 0.00084 mg/kg SW846 8260D
Naphthalene 0.0273 0.0054 0.00062 mg/kg SW846 8260D
Toluene 0.0843 0.0054 0.00020 mg/kg SW846 8260D
1,2,4-Trimethylbenzene 1.33 0.32 0.024 mg/kg SW846 8260D
1,3,5-Trimethylbenzene 0.0953 0.0054 0.00028 mg/kg SW846 8260D
m,p-Xylene 1.05 0.13 0.029 mg/kg SW846 8260D
o-Xylene 0.437 0.063 0.016 mg/kg SW846 8260D
Xylene (total)1.49 0.13 0.073 mg/kg SW846 8260D
C9- C12 Aliphatics (Unadj.)11.0 6.4 3.2 mg/kg MADEP VPH REV 2.1
C9- C10 Aromatics (Unadj.)4.58 J 6.4 3.2 mg/kg MADEP VPH REV 2.1
LA84954-6 B-3 (9-11)
TPH-GRO (C6-C10)9.65 9.2 4.5 mg/kg SW846 8015C
LA84954-7 B-4 (2-3)
Acetone 0.107 0.062 0.0028 mg/kg SW846 8260D
Benzene 0.0391 0.00062 0.00025 mg/kg SW846 8260D
sec-Butylbenzene 0.0035 J 0.0062 0.00041 mg/kg SW846 8260D
1,2-Dichloropropane 0.00095 J 0.0012 0.00016 mg/kg SW846 8260D
Ethylbenzene 0.103 0.0012 0.00032 mg/kg SW846 8260D
Isopropylbenzene 0.0118 0.0062 0.00035 mg/kg SW846 8260D
p-Isopropyltoluene 0.0015 J 0.0062 0.00042 mg/kg SW846 8260D
Methyl Chloride 0.0016 J 0.0062 0.00037 mg/kg SW846 8260D
Methyl Ethyl Ketone 0.0300 0.016 0.00096 mg/kg SW846 8260D
Naphthalene 0.0333 0.0062 0.00071 mg/kg SW846 8260D
n-Propylbenzene 0.0455 0.0062 0.00053 mg/kg SW846 8260D
Toluene 0.0449 0.0062 0.00023 mg/kg SW846 8260D
1,2,4-Trimethylbenzene 0.604 0.40 0.030 mg/kg SW846 8260D
1,3,5-Trimethylbenzene 0.0850 0.0062 0.00031 mg/kg SW846 8260D
m,p-Xylene 0.359 0.0025 0.00056 mg/kg SW846 8260D
o-Xylene 0.138 0.0012 0.00032 mg/kg SW846 8260D
Xylene (total)0.497 0.0025 0.0014 mg/kg SW846 8260D
C9- C12 Aliphatics (Unadj.)6.16 J 7.5 3.7 mg/kg MADEP VPH REV 2.1
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Summary of Hits Page 3 of 4
Job Number:LA84954
Account:Atlas
Project:Phoenix 308-Rocky PT, NC
Collected:11/01/22
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
LA84954-8 B-4 (9-10)
TPH-GRO (C6-C10)34.9 6.8 3.3 mg/kg SW846 8015C
LA84954-9 B-5 (2-3)
Benzene 0.0160 J 0.037 0.015 mg/kg SW846 8260D
sec-Butylbenzene 0.0280 J 0.37 0.024 mg/kg SW846 8260D
1,2-Dichloropropane 0.0962 0.073 0.0093 mg/kg SW846 8260D
Ethylbenzene 0.272 0.073 0.019 mg/kg SW846 8260D
Isopropylbenzene 0.0472 J 0.37 0.021 mg/kg SW846 8260D
Naphthalene 0.315 J 0.37 0.042 mg/kg SW846 8260D
n-Propylbenzene 0.238 J 0.37 0.031 mg/kg SW846 8260D
Toluene 0.110 J 0.37 0.013 mg/kg SW846 8260D
1,1,2-Trichloroethane 0.0213 J 0.073 0.011 mg/kg SW846 8260D
1,2,3-Trichloropropane 0.0250 J 0.37 0.018 mg/kg SW846 8260D
1,2,4-Trimethylbenzene 1.36 0.37 0.028 mg/kg SW846 8260D
1,3,5-Trimethylbenzene 0.421 0.37 0.019 mg/kg SW846 8260D
m,p-Xylene 1.14 0.15 0.033 mg/kg SW846 8260D
o-Xylene 0.396 0.073 0.019 mg/kg SW846 8260D
Xylene (total)1.54 0.15 0.085 mg/kg SW846 8260D
C5- C8 Aliphatics (Unadj.)7.46 7.3 3.7 mg/kg MADEP VPH REV 2.1
C9- C12 Aliphatics (Unadj.)21.1 7.3 3.7 mg/kg MADEP VPH REV 2.1
C9- C10 Aromatics (Unadj.)8.66 7.3 3.7 mg/kg MADEP VPH REV 2.1
LA84954-10 B-5 (7-9)
TPH-GRO (C6-C10)452 6.5 3.2 mg/kg SW846 8015C
LA84954-11 B-6 (3-5)
Acetone 0.0178 J 0.047 0.0021 mg/kg SW846 8260D
Benzene 0.0052 0.00047 0.00019 mg/kg SW846 8260D
1,2-Dichloropropane 0.00065 J 0.00094 0.00012 mg/kg SW846 8260D
Ethylbenzene 0.0200 0.00094 0.00025 mg/kg SW846 8260D
Isopropylbenzene 0.0015 J 0.0047 0.00027 mg/kg SW846 8260D
Methyl Chloride 0.0011 J 0.0047 0.00028 mg/kg SW846 8260D
Naphthalene 0.00093 J 0.0047 0.00054 mg/kg SW846 8260D
n-Propylbenzene 0.0042 J 0.0047 0.00040 mg/kg SW846 8260D
Toluene 0.0224 0.0047 0.00017 mg/kg SW846 8260D
1,2,4-Trimethylbenzene 0.0183 0.0047 0.00036 mg/kg SW846 8260D
1,3,5-Trimethylbenzene 0.0064 0.0047 0.00024 mg/kg SW846 8260D
m,p-Xylene 0.0591 0.0019 0.00042 mg/kg SW846 8260D
o-Xylene 0.0263 0.00094 0.00024 mg/kg SW846 8260D
Xylene (total)0.0854 0.0019 0.0011 mg/kg SW846 8260D
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LA849542
Summary of Hits Page 4 of 4
Job Number:LA84954
Account:Atlas
Project:Phoenix 308-Rocky PT, NC
Collected:11/01/22
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
LA84954-12 B-6 (7-9)
TPH-GRO (C6-C10)8.42 6.8 3.3 mg/kg SW846 8015C
LA84954-13 B-7 (3-5)
Acetone 0.0359 J 0.055 0.0024 mg/kg SW846 8260D
Benzene 0.0110 0.00055 0.00022 mg/kg SW846 8260D
sec-Butylbenzene 0.00056 J 0.0055 0.00036 mg/kg SW846 8260D
Di-Isopropyl Ether 0.00020 J 0.0011 0.00016 mg/kg SW846 8260D
Ethylbenzene 0.0345 0.0011 0.00029 mg/kg SW846 8260D
Isopropylbenzene 0.0029 J 0.0055 0.00031 mg/kg SW846 8260D
Methyl Ethyl Ketone 0.0097 J 0.014 0.00085 mg/kg SW846 8260D
Naphthalene 0.0056 0.0055 0.00063 mg/kg SW846 8260D
n-Propylbenzene 0.0087 0.0055 0.00047 mg/kg SW846 8260D
Toluene 0.0593 0.0055 0.00020 mg/kg SW846 8260D
1,2,4-Trimethylbenzene 0.0423 0.0055 0.00042 mg/kg SW846 8260D
1,3,5-Trimethylbenzene 0.0146 0.0055 0.00028 mg/kg SW846 8260D
m,p-Xylene 0.111 0.0022 0.00050 mg/kg SW846 8260D
o-Xylene 0.0567 0.0011 0.00028 mg/kg SW846 8260D
Xylene (total)0.167 0.0022 0.0013 mg/kg SW846 8260D
LA84954-14 B-7 (7-9)
TPH-GRO (C6-C10)1440 70 34 mg/kg SW846 8015C
(a) Unable to analyze dilution prior to sample expiration.
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LA849542
SGS North America Inc.
Sample Results
Report of Analysis
Scott, LA
Section 3
9 of 90
LA849543
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:B-1 (3-5)
Lab Sample ID:LA84954-1 Date Sampled:11/01/22
Matrix:SO - Soil Date Received:11/03/22
Method:SW846 8260D SW846 5035 Percent Solids:82.3
Project:Phoenix 308-Rocky PT, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2H0084539.D 1 11/15/22 22:19 MB 11/05/22 10:00 n/a V2H3248
Run #2 a 2H0084617.D 1 11/18/22 15:39 JY 11/05/22 10:00 n/a V2H3251
Initial Weight
Run #1 5.6 g
Run #2 5.6 g
VOA List for NC
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 0.0300 0.054 0.0024 mg/kg J
71-43-2 Benzene 0.0049 0.00054 0.00021 mg/kg
108-86-1 Bromobenzene ND 0.0011 0.00033 mg/kg
74-97-5 Bromochloromethane ND 0.0011 0.00030 mg/kg
75-27-4 Bromodichloromethane ND 0.0011 0.00034 mg/kg
75-25-2 Bromoform ND 0.0011 0.00087 mg/kg
104-51-8 n-Butylbenzene ND 0.0054 0.00035 mg/kg
135-98-8 sec-Butylbenzene 0.00083 0.0054 0.00036 mg/kg J
98-06-6 tert-Butylbenzene ND 0.0011 0.00031 mg/kg
56-23-5 Carbon Tetrachloride ND 0.0011 0.00043 mg/kg
108-90-7 Chlorobenzene ND 0.0011 0.00027 mg/kg
75-00-3 Chloroethane ND b 0.0011 0.00037 mg/kg
67-66-3 Chloroform ND 0.0011 0.00028 mg/kg
95-49-8 o-Chlorotoluene ND 0.0054 0.00053 mg/kg
106-43-4 p-Chlorotoluene ND 0.0054 0.000071mg/kg
124-48-1 Dibromochloromethane ND 0.0011 0.00031 mg/kg
96-12-8 1,2-Dibromo-3-chloropropane ND 0.0054 0.00097 mg/kg
106-93-4 1,2-Dibromoethane ND 0.0011 0.00062 mg/kg
75-71-8 Dichlorodifluoromethane ND 0.0011 0.00071 mg/kg
541-73-1 m-Dichlorobenzene ND 0.0011 0.00034 mg/kg
95-50-1 o-Dichlorobenzene ND 0.0011 0.00021 mg/kg
106-46-7 p-Dichlorobenzene ND 0.0011 0.00028 mg/kg
75-34-3 1,1-Dichloroethane ND 0.0011 0.00025 mg/kg
107-06-2 1,2-Dichloroethane ND 0.0011 0.00024 mg/kg
75-35-4 1,1-Dichloroethylene ND 0.0011 0.00044 mg/kg
156-59-2 cis-1,2-Dichloroethylene ND 0.0011 0.00034 mg/kg
156-60-5 trans-1,2-Dichloroethylene ND 0.0011 0.00022 mg/kg
78-87-5 1,2-Dichloropropane 0.0015 0.0011 0.00014 mg/kg
142-28-9 1,3-Dichloropropane ND 0.0011 0.00026 mg/kg
594-20-7 2,2-Dichloropropane ND 0.0011 0.00037 mg/kg
563-58-6 1,1-Dichloropropene ND 0.0011 0.00036 mg/kg
10061-01-5 cis-1,3-Dichloropropene ND 0.0011 0.00026 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 90
LA8495433.1
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:B-1 (3-5)
Lab Sample ID:LA84954-1 Date Sampled:11/01/22
Matrix:SO - Soil Date Received:11/03/22
Method:SW846 8260D SW846 5035 Percent Solids:82.3
Project:Phoenix 308-Rocky PT, NC
VOA List for NC
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.0011 0.00028 mg/kg
108-20-3 Di-Isopropyl Ether ND 0.0011 0.00016 mg/kg
64-17-5 Ethyl Alcohol ND 0.43 0.027 mg/kg
100-41-4 Ethylbenzene 0.0281 0.0011 0.00028 mg/kg
591-78-6 2-Hexanone ND 0.014 0.00071 mg/kg
87-68-3 Hexachlorobutadiene ND 0.0054 0.00032 mg/kg
98-82-8 Isopropylbenzene 0.0033 0.0054 0.00031 mg/kg J
99-87-6 p-Isopropyltoluene 0.00041 0.0054 0.00037 mg/kg J
74-83-9 Methyl Bromide ND 0.011 0.0017 mg/kg
74-87-3 Methyl Chloride 0.00097 0.0054 0.00032 mg/kg J
74-95-3 Methylene Bromide ND 0.0011 0.00031 mg/kg
75-09-2 Methylene Chloride ND 0.0054 0.00060 mg/kg
78-93-3 Methyl Ethyl Ketone ND 0.014 0.00083 mg/kg
108-10-1 4-Methyl-2-pentanone ND 0.014 0.00056 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.0011 0.00011 mg/kg
91-20-3 Naphthalene 0.0073 0.0054 0.00062 mg/kg
103-65-1 n-Propylbenzene 0.0105 0.0054 0.00046 mg/kg
100-42-5 Styrene ND 0.0011 0.00016 mg/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 0.0011 0.00021 mg/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 0.0011 0.00016 mg/kg
127-18-4 Tetrachloroethylene ND 0.0011 0.00037 mg/kg
108-88-3 Toluene 0.0194 0.0054 0.00020 mg/kg
87-61-6 1,2,3-Trichlorobenzene ND 0.0054 0.00035 mg/kg
120-82-1 1,2,4-Trichlorobenzene ND 0.0054 0.00022 mg/kg
71-55-6 1,1,1-Trichloroethane ND 0.0011 0.00038 mg/kg
79-00-5 1,1,2-Trichloroethane ND 0.0011 0.00016 mg/kg
79-01-6 Trichloroethylene ND 0.0011 0.00054 mg/kg
75-69-4 Trichlorofluoromethane ND b 0.0011 0.00039 mg/kg
96-18-4 1,2,3-Trichloropropane ND 0.0054 0.00027 mg/kg
95-63-6 1,2,4-Trimethylbenzene 0.0743 0.0054 0.00041 mg/kg
108-67-8 1,3,5-Trimethylbenzene 0.0236 0.0054 0.00027 mg/kg
108-05-4 Vinyl Acetate ND 0.0054 0.00038 mg/kg
75-01-4 Vinyl Chloride ND 0.0011 0.00028 mg/kg
m,p-Xylene 0.103 0.0022 0.00049 mg/kg
95-47-6 o-Xylene 0.0536 0.0011 0.00028 mg/kg
1330-20-7 Xylene (total)0.157 0.0022 0.0013 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 107%107%59-143%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 90
LA8495433.1
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:B-1 (3-5)
Lab Sample ID:LA84954-1 Date Sampled:11/01/22
Matrix:SO - Soil Date Received:11/03/22
Method:SW846 8260D SW846 5035 Percent Solids:82.3
Project:Phoenix 308-Rocky PT, NC
VOA List for NC
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 107%101%52-159%
460-00-4 4-Bromofluorobenzene 111%111%38-183%
(a) Sample analyzed beyond hold time.
(b) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 90
LA8495433.1
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:B-1 (3-5)
Lab Sample ID:LA84954-1 Date Sampled:11/01/22
Matrix:SO - Soil Date Received:11/03/22
Method:MADEP VPH REV 2.1 Percent Solids:82.3
Project:Phoenix 308-Rocky PT, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LE039197.D 1 11/07/22 14:57 KM n/a n/a GLE2311
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 4.9 g 5.0 ml 100 ul
Run #2
MA VPH list
CAS No.Compound Result RL MDL Units Q
C5- C8 Aliphatics (Unadj.)ND 7.3 3.6 mg/kg
C9- C12 Aliphatics (Unadj.)ND 7.3 3.6 mg/kg
C9- C10 Aromatics (Unadj.)ND 7.3 3.6 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
615-59-8 2,5-Dibromotoluene 136% a 70-130%
615-59-8 2,5-Dibromotoluene 134% a 70-130%
(a) Outside control limits biased high. Sample is ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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LA8495433.1
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:B-1 (7-9)
Lab Sample ID:LA84954-2 Date Sampled:11/01/22
Matrix:SO - Soil Date Received:11/03/22
Method:SW846 8015C SW846 5035 Percent Solids:78.6
Project:Phoenix 308-Rocky PT, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LA416804.D 1 11/09/22 03:36 KM 11/05/22 10:00 n/a GLA3796
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 6.20 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)25.2 6.5 3.2 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 91%64-128%
540-36-3 1,4-Difluorobenzene 102%80-122%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
14 of 90
LA8495433.2
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:B-2 (2-3)
Lab Sample ID:LA84954-3 Date Sampled:11/01/22
Matrix:SO - Soil Date Received:11/03/22
Method:SW846 8260D SW846 5035 Percent Solids:78.9
Project:Phoenix 308-Rocky PT, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2X01306880.D 1 11/15/22 15:07 JS 11/05/22 10:00 n/a V2X5814
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 5.2 g 5.0 ml 100 ul
Run #2
VOA List for NC
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 0.192 3.7 0.16 mg/kg J
71-43-2 Benzene ND 0.037 0.015 mg/kg
108-86-1 Bromobenzene ND 0.074 0.022 mg/kg
74-97-5 Bromochloromethane ND 0.074 0.020 mg/kg
75-27-4 Bromodichloromethane ND 0.074 0.024 mg/kg
75-25-2 Bromoform ND 0.074 0.060 mg/kg
104-51-8 n-Butylbenzene ND 0.37 0.024 mg/kg
135-98-8 sec-Butylbenzene 0.385 0.37 0.024 mg/kg
98-06-6 tert-Butylbenzene ND 0.074 0.021 mg/kg
56-23-5 Carbon Tetrachloride ND 0.074 0.029 mg/kg
108-90-7 Chlorobenzene ND 0.074 0.018 mg/kg
75-00-3 Chloroethane ND 0.074 0.025 mg/kg
67-66-3 Chloroform ND 0.074 0.020 mg/kg
95-49-8 o-Chlorotoluene ND 0.37 0.036 mg/kg
106-43-4 p-Chlorotoluene ND 0.37 0.0048 mg/kg
124-48-1 Dibromochloromethane ND 0.074 0.021 mg/kg
96-12-8 1,2-Dibromo-3-chloropropane ND 0.37 0.066 mg/kg
106-93-4 1,2-Dibromoethane ND 0.074 0.043 mg/kg
75-71-8 Dichlorodifluoromethane ND 0.074 0.049 mg/kg
541-73-1 m-Dichlorobenzene ND 0.074 0.024 mg/kg
95-50-1 o-Dichlorobenzene ND 0.074 0.014 mg/kg
106-46-7 p-Dichlorobenzene ND 0.074 0.019 mg/kg
75-34-3 1,1-Dichloroethane ND 0.074 0.017 mg/kg
107-06-2 1,2-Dichloroethane ND 0.074 0.016 mg/kg
75-35-4 1,1-Dichloroethylene ND 0.074 0.030 mg/kg
156-59-2 cis-1,2-Dichloroethylene ND 0.074 0.023 mg/kg
156-60-5 trans-1,2-Dichloroethylene ND 0.074 0.015 mg/kg
78-87-5 1,2-Dichloropropane ND 0.074 0.0094 mg/kg
142-28-9 1,3-Dichloropropane ND 0.074 0.018 mg/kg
594-20-7 2,2-Dichloropropane ND 0.074 0.026 mg/kg
563-58-6 1,1-Dichloropropene ND 0.074 0.025 mg/kg
10061-01-5 cis-1,3-Dichloropropene ND 0.074 0.018 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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LA8495433.3
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:B-2 (2-3)
Lab Sample ID:LA84954-3 Date Sampled:11/01/22
Matrix:SO - Soil Date Received:11/03/22
Method:SW846 8260D SW846 5035 Percent Solids:78.9
Project:Phoenix 308-Rocky PT, NC
VOA List for NC
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.074 0.019 mg/kg
108-20-3 Di-Isopropyl Ether ND 0.074 0.011 mg/kg
64-17-5 Ethyl Alcohol ND 30 1.8 mg/kg
100-41-4 Ethylbenzene 1.59 0.074 0.019 mg/kg
591-78-6 2-Hexanone ND 0.93 0.049 mg/kg
87-68-3 Hexachlorobutadiene ND 0.37 0.022 mg/kg
98-82-8 Isopropylbenzene 0.641 0.37 0.021 mg/kg
99-87-6 p-Isopropyltoluene 0.277 0.37 0.025 mg/kg J
74-83-9 Methyl Bromide ND 0.74 0.12 mg/kg
74-87-3 Methyl Chloride ND 0.37 0.022 mg/kg
74-95-3 Methylene Bromide ND 0.074 0.022 mg/kg
75-09-2 Methylene Chloride ND 0.37 0.041 mg/kg
78-93-3 Methyl Ethyl Ketone ND 0.93 0.057 mg/kg
108-10-1 4-Methyl-2-pentanone ND 0.93 0.038 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.074 0.0078 mg/kg
91-20-3 Naphthalene 3.96 0.37 0.043 mg/kg
103-65-1 n-Propylbenzene 3.18 0.37 0.032 mg/kg
100-42-5 Styrene ND 0.074 0.011 mg/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 0.074 0.015 mg/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 0.074 0.011 mg/kg
127-18-4 Tetrachloroethylene ND 0.074 0.025 mg/kg
108-88-3 Toluene 0.212 0.37 0.013 mg/kg J
87-61-6 1,2,3-Trichlorobenzene ND 0.37 0.024 mg/kg
120-82-1 1,2,4-Trichlorobenzene ND 0.37 0.015 mg/kg
71-55-6 1,1,1-Trichloroethane ND 0.074 0.026 mg/kg
79-00-5 1,1,2-Trichloroethane ND 0.074 0.011 mg/kg
79-01-6 Trichloroethylene ND 0.074 0.037 mg/kg
75-69-4 Trichlorofluoromethane ND 0.074 0.027 mg/kg
96-18-4 1,2,3-Trichloropropane ND 0.37 0.018 mg/kg
95-63-6 1,2,4-Trimethylbenzene a 22.5 0.37 0.028 mg/kg E
108-67-8 1,3,5-Trimethylbenzene 7.58 0.37 0.019 mg/kg
108-05-4 Vinyl Acetate ND 0.37 0.026 mg/kg
75-01-4 Vinyl Chloride ND 0.074 0.020 mg/kg
m,p-Xylene 7.04 0.15 0.034 mg/kg
95-47-6 o-Xylene 2.95 0.074 0.019 mg/kg
1330-20-7 Xylene (total)9.99 0.15 0.086 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 86%59-143%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
16 of 90
LA8495433.3
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:B-2 (2-3)
Lab Sample ID:LA84954-3 Date Sampled:11/01/22
Matrix:SO - Soil Date Received:11/03/22
Method:SW846 8260D SW846 5035 Percent Solids:78.9
Project:Phoenix 308-Rocky PT, NC
VOA List for NC
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 95%52-159%
460-00-4 4-Bromofluorobenzene 101%38-183%
(a) Unable to analyze dilution prior to sample expiration.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
17 of 90
LA8495433.3
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:B-2 (2-3)
Lab Sample ID:LA84954-3 Date Sampled:11/01/22
Matrix:SO - Soil Date Received:11/03/22
Method:MADEP VPH REV 2.1 Percent Solids:78.9
Project:Phoenix 308-Rocky PT, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LE039255.D 1 11/10/22 17:47 KM n/a n/a GLE2313
Run #2 LE039198.D 1 11/07/22 15:28 KM n/a n/a GLE2311
Initial Weight Final Volume Methanol Aliquot
Run #1 5.3 g 5.0 ml 50.0 ul
Run #2 5.0 g 5.0 ml 100 ul
MA VPH list
CAS No.Compound Result RL MDL Units Q
C5- C8 Aliphatics (Unadj.)72.8 a 7.7 3.8 mg/kg
C9- C12 Aliphatics (Unadj.)135 15 7.3 mg/kg
C9- C10 Aromatics (Unadj.)56.2 15 7.3 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
615-59-8 2,5-Dibromotoluene 144% b 139% b 70-130%
615-59-8 2,5-Dibromotoluene 143% b 150% b 70-130%
(a) Result is from Run# 2
(b) Outside control limits due to matrix interference. Confirmed by reanalysis.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
18 of 90
LA8495433.3
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:B-2 (7-9)
Lab Sample ID:LA84954-4 Date Sampled:11/01/22
Matrix:SO - Soil Date Received:11/03/22
Method:SW846 8015C Percent Solids:78.1
Project:Phoenix 308-Rocky PT, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LA416806.D 1 11/09/22 03:59 KM n/a n/a GLA3796
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 6.00 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)242 6.7 3.3 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 90%64-128%
540-36-3 1,4-Difluorobenzene 92%80-122%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
19 of 90
LA8495433.4
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:B-3 (2-3)
Lab Sample ID:LA84954-5 Date Sampled:11/01/22
Matrix:SO - Soil Date Received:11/03/22
Method:SW846 8260D SW846 5035 Percent Solids:86.6
Project:Phoenix 308-Rocky PT, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2H0084535.D 1 11/15/22 20:45 MB 11/05/22 10:00 n/a V2H3248
Run #2 2X01306881.D 1 11/15/22 15:30 JS 11/05/22 10:00 n/a V2X5814
Initial Weight Final Volume Methanol Aliquot
Run #1 5.3 g
Run #2 5.2 g 5.0 ml 100 ul
VOA List for NC
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 0.0976 0.054 0.0024 mg/kg
71-43-2 Benzene 0.0265 0.00054 0.00022 mg/kg
108-86-1 Bromobenzene ND 0.0011 0.00033 mg/kg
74-97-5 Bromochloromethane ND 0.0011 0.00030 mg/kg
75-27-4 Bromodichloromethane ND 0.0011 0.00035 mg/kg
75-25-2 Bromoform ND 0.0011 0.00087 mg/kg
104-51-8 n-Butylbenzene ND 0.0054 0.00035 mg/kg
135-98-8 sec-Butylbenzene 0.0036 0.0054 0.00036 mg/kg J
98-06-6 tert-Butylbenzene ND 0.0011 0.00031 mg/kg
56-23-5 Carbon Tetrachloride ND 0.0011 0.00043 mg/kg
108-90-7 Chlorobenzene ND 0.0011 0.00027 mg/kg
75-00-3 Chloroethane ND 0.0011 0.00037 mg/kg
67-66-3 Chloroform ND 0.0011 0.00029 mg/kg
95-49-8 o-Chlorotoluene ND 0.0054 0.00053 mg/kg
106-43-4 p-Chlorotoluene ND 0.0054 0.000071mg/kg
124-48-1 Dibromochloromethane ND 0.0011 0.00031 mg/kg
96-12-8 1,2-Dibromo-3-chloropropane ND 0.0054 0.00097 mg/kg
106-93-4 1,2-Dibromoethane ND 0.0011 0.00062 mg/kg
75-71-8 Dichlorodifluoromethane ND 0.0011 0.00071 mg/kg
541-73-1 m-Dichlorobenzene ND 0.0011 0.00035 mg/kg
95-50-1 o-Dichlorobenzene ND 0.0011 0.00021 mg/kg
106-46-7 p-Dichlorobenzene ND 0.0011 0.00028 mg/kg
75-34-3 1,1-Dichloroethane ND 0.0011 0.00025 mg/kg
107-06-2 1,2-Dichloroethane ND 0.0011 0.00024 mg/kg
75-35-4 1,1-Dichloroethylene ND 0.0011 0.00044 mg/kg
156-59-2 cis-1,2-Dichloroethylene ND 0.0011 0.00034 mg/kg
156-60-5 trans-1,2-Dichloroethylene ND 0.0011 0.00022 mg/kg
78-87-5 1,2-Dichloropropane ND 0.0011 0.00014 mg/kg
142-28-9 1,3-Dichloropropane ND 0.0011 0.00026 mg/kg
594-20-7 2,2-Dichloropropane ND 0.0011 0.00037 mg/kg
563-58-6 1,1-Dichloropropene ND 0.0011 0.00036 mg/kg
10061-01-5 cis-1,3-Dichloropropene ND 0.0011 0.00026 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
20 of 90
LA8495433.5
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:B-3 (2-3)
Lab Sample ID:LA84954-5 Date Sampled:11/01/22
Matrix:SO - Soil Date Received:11/03/22
Method:SW846 8260D SW846 5035 Percent Solids:86.6
Project:Phoenix 308-Rocky PT, NC
VOA List for NC
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.0011 0.00028 mg/kg
108-20-3 Di-Isopropyl Ether ND 0.0011 0.00016 mg/kg
64-17-5 Ethyl Alcohol ND 0.44 0.027 mg/kg
100-41-4 Ethylbenzene 0.161 0.0011 0.00028 mg/kg
591-78-6 2-Hexanone ND 0.014 0.00071 mg/kg
87-68-3 Hexachlorobutadiene ND 0.0054 0.00033 mg/kg
98-82-8 Isopropylbenzene 0.0152 0.0054 0.00031 mg/kg
99-87-6 p-Isopropyltoluene 0.0020 0.0054 0.00037 mg/kg J
74-83-9 Methyl Bromide ND 0.011 0.0017 mg/kg
74-87-3 Methyl Chloride ND 0.0054 0.00033 mg/kg
74-95-3 Methylene Bromide ND 0.0011 0.00032 mg/kg
75-09-2 Methylene Chloride ND 0.0054 0.00060 mg/kg
78-93-3 Methyl Ethyl Ketone 0.0486 0.014 0.00084 mg/kg
108-10-1 4-Methyl-2-pentanone ND 0.014 0.00056 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.0011 0.00011 mg/kg
91-20-3 Naphthalene 0.0273 0.0054 0.00062 mg/kg
103-65-1 n-Propylbenzene ND 0.0054 0.00047 mg/kg
100-42-5 Styrene ND 0.0011 0.00016 mg/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 0.0011 0.00021 mg/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 0.0011 0.00016 mg/kg
127-18-4 Tetrachloroethylene ND 0.0011 0.00037 mg/kg
108-88-3 Toluene 0.0843 0.0054 0.00020 mg/kg
87-61-6 1,2,3-Trichlorobenzene ND 0.0054 0.00035 mg/kg
120-82-1 1,2,4-Trichlorobenzene ND 0.0054 0.00022 mg/kg
71-55-6 1,1,1-Trichloroethane ND 0.0011 0.00038 mg/kg
79-00-5 1,1,2-Trichloroethane ND 0.0011 0.00016 mg/kg
79-01-6 Trichloroethylene ND 0.0011 0.00054 mg/kg
75-69-4 Trichlorofluoromethane ND 0.0011 0.00039 mg/kg
96-18-4 1,2,3-Trichloropropane ND 0.0054 0.00027 mg/kg
95-63-6 1,2,4-Trimethylbenzene 1.33 a 0.32 0.024 mg/kg
108-67-8 1,3,5-Trimethylbenzene 0.0953 0.0054 0.00028 mg/kg
108-05-4 Vinyl Acetate ND 0.0054 0.00038 mg/kg
75-01-4 Vinyl Chloride ND 0.0011 0.00029 mg/kg
m,p-Xylene 1.05 a 0.13 0.029 mg/kg
95-47-6 o-Xylene 0.437 a 0.063 0.016 mg/kg
1330-20-7 Xylene (total)1.49 a 0.13 0.073 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 85%86%59-143%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
21 of 90
LA8495433.5
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:B-3 (2-3)
Lab Sample ID:LA84954-5 Date Sampled:11/01/22
Matrix:SO - Soil Date Received:11/03/22
Method:SW846 8260D SW846 5035 Percent Solids:86.6
Project:Phoenix 308-Rocky PT, NC
VOA List for NC
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 97%99%52-159%
460-00-4 4-Bromofluorobenzene 97%96%38-183%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
22 of 90
LA8495433.5
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:B-3 (2-3)
Lab Sample ID:LA84954-5 Date Sampled:11/01/22
Matrix:SO - Soil Date Received:11/03/22
Method:MADEP VPH REV 2.1 Percent Solids:86.6
Project:Phoenix 308-Rocky PT, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LE039199.D 1 11/07/22 15:58 KM n/a n/a GLE2311
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 5.1 g 5.0 ml 100 ul
Run #2
MA VPH list
CAS No.Compound Result RL MDL Units Q
C5- C8 Aliphatics (Unadj.)ND 6.4 3.2 mg/kg
C9- C12 Aliphatics (Unadj.)11.0 6.4 3.2 mg/kg
C9- C10 Aromatics (Unadj.)4.58 6.4 3.2 mg/kg J
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
615-59-8 2,5-Dibromotoluene 112%70-130%
615-59-8 2,5-Dibromotoluene 116%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
23 of 90
LA8495433.5
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:B-3 (9-11)
Lab Sample ID:LA84954-6 Date Sampled:11/01/22
Matrix:SO - Soil Date Received:11/03/22
Method:SW846 8015C SW846 5035 Percent Solids:69.8
Project:Phoenix 308-Rocky PT, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LA416858.D 1 11/09/22 16:54 KM 11/05/22 10:00 n/a GLA3797
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 5.10 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)9.65 9.2 4.5 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 93%64-128%
540-36-3 1,4-Difluorobenzene 113%80-122%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
24 of 90
LA8495433.6
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:B-4 (2-3)
Lab Sample ID:LA84954-7 Date Sampled:11/01/22
Matrix:SO - Soil Date Received:11/03/22
Method:SW846 8260D SW846 5035 Percent Solids:77.2
Project:Phoenix 308-Rocky PT, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2H0084536.D 1 11/15/22 21:09 MB 11/05/22 10:00 n/a V2H3248
Run #2 2X01306882.D 1 11/15/22 15:53 JS 11/05/22 10:00 n/a V2X5814
Initial Weight Final Volume Methanol Aliquot
Run #1 5.2 g
Run #2 5.0 g 5.0 ml 100 ul
VOA List for NC
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 0.107 0.062 0.0028 mg/kg
71-43-2 Benzene 0.0391 0.00062 0.00025 mg/kg
108-86-1 Bromobenzene ND 0.0012 0.00038 mg/kg
74-97-5 Bromochloromethane ND 0.0012 0.00034 mg/kg
75-27-4 Bromodichloromethane ND 0.0012 0.00040 mg/kg
75-25-2 Bromoform ND 0.0012 0.0010 mg/kg
104-51-8 n-Butylbenzene ND 0.0062 0.00040 mg/kg
135-98-8 sec-Butylbenzene 0.0035 0.0062 0.00041 mg/kg J
98-06-6 tert-Butylbenzene ND 0.0012 0.00036 mg/kg
56-23-5 Carbon Tetrachloride ND 0.0012 0.00049 mg/kg
108-90-7 Chlorobenzene ND 0.0012 0.00031 mg/kg
75-00-3 Chloroethane ND 0.0012 0.00042 mg/kg
67-66-3 Chloroform ND 0.0012 0.00033 mg/kg
95-49-8 o-Chlorotoluene ND 0.0062 0.00061 mg/kg
106-43-4 p-Chlorotoluene ND 0.0062 0.000081mg/kg
124-48-1 Dibromochloromethane ND 0.0012 0.00036 mg/kg
96-12-8 1,2-Dibromo-3-chloropropane ND 0.0062 0.0011 mg/kg
106-93-4 1,2-Dibromoethane ND 0.0012 0.00071 mg/kg
75-71-8 Dichlorodifluoromethane ND 0.0012 0.00081 mg/kg
541-73-1 m-Dichlorobenzene ND 0.0012 0.00040 mg/kg
95-50-1 o-Dichlorobenzene ND 0.0012 0.00024 mg/kg
106-46-7 p-Dichlorobenzene ND 0.0012 0.00032 mg/kg
75-34-3 1,1-Dichloroethane ND 0.0012 0.00028 mg/kg
107-06-2 1,2-Dichloroethane ND 0.0012 0.00027 mg/kg
75-35-4 1,1-Dichloroethylene ND 0.0012 0.00050 mg/kg
156-59-2 cis-1,2-Dichloroethylene ND 0.0012 0.00039 mg/kg
156-60-5 trans-1,2-Dichloroethylene ND 0.0012 0.00025 mg/kg
78-87-5 1,2-Dichloropropane 0.00095 0.0012 0.00016 mg/kg J
142-28-9 1,3-Dichloropropane ND 0.0012 0.00030 mg/kg
594-20-7 2,2-Dichloropropane ND 0.0012 0.00043 mg/kg
563-58-6 1,1-Dichloropropene ND 0.0012 0.00041 mg/kg
10061-01-5 cis-1,3-Dichloropropene ND 0.0012 0.00029 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
25 of 90
LA8495433.7
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:B-4 (2-3)
Lab Sample ID:LA84954-7 Date Sampled:11/01/22
Matrix:SO - Soil Date Received:11/03/22
Method:SW846 8260D SW846 5035 Percent Solids:77.2
Project:Phoenix 308-Rocky PT, NC
VOA List for NC
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.0012 0.00032 mg/kg
108-20-3 Di-Isopropyl Ether ND 0.0012 0.00018 mg/kg
64-17-5 Ethyl Alcohol ND 0.50 0.031 mg/kg
100-41-4 Ethylbenzene 0.103 0.0012 0.00032 mg/kg
591-78-6 2-Hexanone ND 0.016 0.00082 mg/kg
87-68-3 Hexachlorobutadiene ND 0.0062 0.00037 mg/kg
98-82-8 Isopropylbenzene 0.0118 0.0062 0.00035 mg/kg
99-87-6 p-Isopropyltoluene 0.0015 0.0062 0.00042 mg/kg J
74-83-9 Methyl Bromide ND 0.012 0.0019 mg/kg
74-87-3 Methyl Chloride 0.0016 0.0062 0.00037 mg/kg J
74-95-3 Methylene Bromide ND 0.0012 0.00036 mg/kg
75-09-2 Methylene Chloride ND 0.0062 0.00069 mg/kg
78-93-3 Methyl Ethyl Ketone 0.0300 0.016 0.00096 mg/kg
108-10-1 4-Methyl-2-pentanone ND 0.016 0.00064 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.0012 0.00013 mg/kg
91-20-3 Naphthalene 0.0333 0.0062 0.00071 mg/kg
103-65-1 n-Propylbenzene 0.0455 0.0062 0.00053 mg/kg
100-42-5 Styrene ND 0.0012 0.00018 mg/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 0.0012 0.00024 mg/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 0.0012 0.00019 mg/kg
127-18-4 Tetrachloroethylene ND 0.0012 0.00043 mg/kg
108-88-3 Toluene 0.0449 0.0062 0.00023 mg/kg
87-61-6 1,2,3-Trichlorobenzene ND 0.0062 0.00041 mg/kg
120-82-1 1,2,4-Trichlorobenzene ND 0.0062 0.00026 mg/kg
71-55-6 1,1,1-Trichloroethane ND 0.0012 0.00044 mg/kg
79-00-5 1,1,2-Trichloroethane ND 0.0012 0.00019 mg/kg
79-01-6 Trichloroethylene ND 0.0012 0.00062 mg/kg
75-69-4 Trichlorofluoromethane ND 0.0012 0.00045 mg/kg
96-18-4 1,2,3-Trichloropropane ND 0.0062 0.00031 mg/kg
95-63-6 1,2,4-Trimethylbenzene 0.604 a 0.40 0.030 mg/kg
108-67-8 1,3,5-Trimethylbenzene 0.0850 0.0062 0.00031 mg/kg
108-05-4 Vinyl Acetate ND 0.0062 0.00044 mg/kg
75-01-4 Vinyl Chloride ND 0.0012 0.00033 mg/kg
m,p-Xylene 0.359 0.0025 0.00056 mg/kg
95-47-6 o-Xylene 0.138 0.0012 0.00032 mg/kg
1330-20-7 Xylene (total)0.497 0.0025 0.0014 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 89%85%59-143%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
26 of 90
LA8495433.7
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:B-4 (2-3)
Lab Sample ID:LA84954-7 Date Sampled:11/01/22
Matrix:SO - Soil Date Received:11/03/22
Method:SW846 8260D SW846 5035 Percent Solids:77.2
Project:Phoenix 308-Rocky PT, NC
VOA List for NC
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 102%98%52-159%
460-00-4 4-Bromofluorobenzene 101%95%38-183%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
27 of 90
LA8495433.7
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:B-4 (2-3)
Lab Sample ID:LA84954-7 Date Sampled:11/01/22
Matrix:SO - Soil Date Received:11/03/22
Method:MADEP VPH REV 2.1 Percent Solids:77.2
Project:Phoenix 308-Rocky PT, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LE039254.D 1 11/10/22 17:15 KM n/a n/a GLE2313
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 5.4 g 5.0 ml 100 ul
Run #2
MA VPH list
CAS No.Compound Result RL MDL Units Q
C5- C8 Aliphatics (Unadj.)ND 7.5 3.7 mg/kg
C9- C12 Aliphatics (Unadj.)6.16 7.5 3.7 mg/kg J
C9- C10 Aromatics (Unadj.)ND 7.5 3.7 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
615-59-8 2,5-Dibromotoluene 134% a 70-130%
615-59-8 2,5-Dibromotoluene 127%70-130%
(a) Outside control limits biased high. No compounds detected above client requested RLs.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
28 of 90
LA8495433.7
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:B-4 (9-10)
Lab Sample ID:LA84954-8 Date Sampled:11/01/22
Matrix:SO - Soil Date Received:11/03/22
Method:SW846 8015C SW846 5035 Percent Solids:77.5
Project:Phoenix 308-Rocky PT, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LA416810.D 1 11/09/22 04:44 KM 11/05/22 10:00 n/a GLA3796
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 6.00 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)34.9 6.8 3.3 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 93%64-128%
540-36-3 1,4-Difluorobenzene 101%80-122%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
29 of 90
LA8495433.8
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:B-5 (2-3)
Lab Sample ID:LA84954-9 Date Sampled:11/01/22
Matrix:SO - Soil Date Received:11/03/22
Method:SW846 8260D SW846 5035 Percent Solids:80.2
Project:Phoenix 308-Rocky PT, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2J0123370.D 1 11/15/22 21:18 NN 11/05/22 10:00 n/a V2J4441
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 5.1 g 5.0 ml 100 ul
Run #2
VOA List for NC
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 3.7 0.16 mg/kg
71-43-2 Benzene 0.0160 0.037 0.015 mg/kg J
108-86-1 Bromobenzene ND 0.073 0.022 mg/kg
74-97-5 Bromochloromethane ND 0.073 0.020 mg/kg
75-27-4 Bromodichloromethane ND 0.073 0.023 mg/kg
75-25-2 Bromoform ND 0.073 0.059 mg/kg
104-51-8 n-Butylbenzene ND 0.37 0.024 mg/kg
135-98-8 sec-Butylbenzene 0.0280 0.37 0.024 mg/kg J
98-06-6 tert-Butylbenzene ND 0.073 0.021 mg/kg
56-23-5 Carbon Tetrachloride ND 0.073 0.029 mg/kg
108-90-7 Chlorobenzene ND 0.073 0.018 mg/kg
75-00-3 Chloroethane ND 0.073 0.025 mg/kg
67-66-3 Chloroform ND 0.073 0.019 mg/kg
95-49-8 o-Chlorotoluene ND 0.37 0.036 mg/kg
106-43-4 p-Chlorotoluene ND 0.37 0.0048 mg/kg
124-48-1 Dibromochloromethane ND 0.073 0.021 mg/kg
96-12-8 1,2-Dibromo-3-chloropropane ND 0.37 0.066 mg/kg
106-93-4 1,2-Dibromoethane ND 0.073 0.042 mg/kg
75-71-8 Dichlorodifluoromethane ND 0.073 0.048 mg/kg
541-73-1 m-Dichlorobenzene ND 0.073 0.023 mg/kg
95-50-1 o-Dichlorobenzene ND 0.073 0.014 mg/kg
106-46-7 p-Dichlorobenzene ND 0.073 0.019 mg/kg
75-34-3 1,1-Dichloroethane ND 0.073 0.017 mg/kg
107-06-2 1,2-Dichloroethane ND 0.073 0.016 mg/kg
75-35-4 1,1-Dichloroethylene ND 0.073 0.030 mg/kg
156-59-2 cis-1,2-Dichloroethylene ND 0.073 0.023 mg/kg
156-60-5 trans-1,2-Dichloroethylene ND 0.073 0.015 mg/kg
78-87-5 1,2-Dichloropropane 0.0962 0.073 0.0093 mg/kg
142-28-9 1,3-Dichloropropane ND 0.073 0.017 mg/kg
594-20-7 2,2-Dichloropropane ND 0.073 0.025 mg/kg
563-58-6 1,1-Dichloropropene ND 0.073 0.024 mg/kg
10061-01-5 cis-1,3-Dichloropropene ND 0.073 0.017 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
30 of 90
LA8495433.9
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:B-5 (2-3)
Lab Sample ID:LA84954-9 Date Sampled:11/01/22
Matrix:SO - Soil Date Received:11/03/22
Method:SW846 8260D SW846 5035 Percent Solids:80.2
Project:Phoenix 308-Rocky PT, NC
VOA List for NC
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.073 0.019 mg/kg
108-20-3 Di-Isopropyl Ether ND 0.073 0.011 mg/kg
64-17-5 Ethyl Alcohol ND 29 1.8 mg/kg
100-41-4 Ethylbenzene 0.272 0.073 0.019 mg/kg
591-78-6 2-Hexanone ND 0.92 0.048 mg/kg
87-68-3 Hexachlorobutadiene ND 0.37 0.022 mg/kg
98-82-8 Isopropylbenzene 0.0472 0.37 0.021 mg/kg J
99-87-6 p-Isopropyltoluene ND 0.37 0.025 mg/kg
74-83-9 Methyl Bromide ND 0.73 0.11 mg/kg
74-87-3 Methyl Chloride ND 0.37 0.022 mg/kg
74-95-3 Methylene Bromide ND 0.073 0.021 mg/kg
75-09-2 Methylene Chloride ND 0.37 0.041 mg/kg
78-93-3 Methyl Ethyl Ketone ND 0.92 0.056 mg/kg
108-10-1 4-Methyl-2-pentanone ND 0.92 0.038 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.073 0.0077 mg/kg
91-20-3 Naphthalene 0.315 0.37 0.042 mg/kg J
103-65-1 n-Propylbenzene 0.238 0.37 0.031 mg/kg J
100-42-5 Styrene ND 0.073 0.011 mg/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 0.073 0.014 mg/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 0.073 0.011 mg/kg
127-18-4 Tetrachloroethylene ND 0.073 0.025 mg/kg
108-88-3 Toluene 0.110 0.37 0.013 mg/kg J
87-61-6 1,2,3-Trichlorobenzene ND 0.37 0.024 mg/kg
120-82-1 1,2,4-Trichlorobenzene ND 0.37 0.015 mg/kg
71-55-6 1,1,1-Trichloroethane ND 0.073 0.026 mg/kg
79-00-5 1,1,2-Trichloroethane 0.0213 0.073 0.011 mg/kg J
79-01-6 Trichloroethylene ND 0.073 0.037 mg/kg
75-69-4 Trichlorofluoromethane ND 0.073 0.027 mg/kg
96-18-4 1,2,3-Trichloropropane 0.0250 0.37 0.018 mg/kg J
95-63-6 1,2,4-Trimethylbenzene 1.36 0.37 0.028 mg/kg
108-67-8 1,3,5-Trimethylbenzene 0.421 0.37 0.019 mg/kg
108-05-4 Vinyl Acetate ND 0.37 0.026 mg/kg
75-01-4 Vinyl Chloride ND 0.073 0.019 mg/kg
m,p-Xylene 1.14 0.15 0.033 mg/kg
95-47-6 o-Xylene 0.396 0.073 0.019 mg/kg
1330-20-7 Xylene (total)1.54 0.15 0.085 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 95%59-143%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
31 of 90
LA8495433.9
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:B-5 (2-3)
Lab Sample ID:LA84954-9 Date Sampled:11/01/22
Matrix:SO - Soil Date Received:11/03/22
Method:SW846 8260D SW846 5035 Percent Solids:80.2
Project:Phoenix 308-Rocky PT, NC
VOA List for NC
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 97%52-159%
460-00-4 4-Bromofluorobenzene 99%38-183%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
32 of 90
LA8495433.9
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:B-5 (2-3)
Lab Sample ID:LA84954-9 Date Sampled:11/01/22
Matrix:SO - Soil Date Received:11/03/22
Method:MADEP VPH REV 2.1 Percent Solids:80.2
Project:Phoenix 308-Rocky PT, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LE039204.D 1 11/07/22 18:34 KM n/a n/a GLE2311
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 5.1 g 5.0 ml 100 ul
Run #2
MA VPH list
CAS No.Compound Result RL MDL Units Q
C5- C8 Aliphatics (Unadj.)7.46 7.3 3.7 mg/kg
C9- C12 Aliphatics (Unadj.)21.1 7.3 3.7 mg/kg
C9- C10 Aromatics (Unadj.)8.66 7.3 3.7 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
615-59-8 2,5-Dibromotoluene 125%70-130%
615-59-8 2,5-Dibromotoluene 124%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
33 of 90
LA8495433.9
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:B-5 (7-9)
Lab Sample ID:LA84954-10 Date Sampled:11/01/22
Matrix:SO - Soil Date Received:11/03/22
Method:SW846 8015C SW846 5035 Percent Solids:79.1
Project:Phoenix 308-Rocky PT, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LA416816.D 1 11/09/22 05:52 KM 11/05/22 10:00 n/a GLA3796
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 6.10 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)452 6.5 3.2 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 91%64-128%
540-36-3 1,4-Difluorobenzene 91%80-122%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
34 of 90
LA8495433.10
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:B-6 (3-5)
Lab Sample ID:LA84954-11 Date Sampled:11/01/22
Matrix:SO - Soil Date Received:11/03/22
Method:SW846 8260D SW846 5035 Percent Solids:85.6
Project:Phoenix 308-Rocky PT, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2H0084537.D 1 11/15/22 21:32 MB 11/05/22 10:00 n/a V2H3248
Run #2 a 2H0084615.D 1 11/18/22 14:52 JY 11/05/22 10:00 n/a V2H3251
Initial Weight
Run #1 6.2 g
Run #2 6.4 g
VOA List for NC
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 0.0178 0.047 0.0021 mg/kg J
71-43-2 Benzene 0.0052 0.00047 0.00019 mg/kg
108-86-1 Bromobenzene ND 0.00094 0.00028 mg/kg
74-97-5 Bromochloromethane ND 0.00094 0.00026 mg/kg
75-27-4 Bromodichloromethane ND 0.00094 0.00030 mg/kg
75-25-2 Bromoform ND 0.00094 0.00076 mg/kg
104-51-8 n-Butylbenzene ND 0.0047 0.00030 mg/kg
135-98-8 sec-Butylbenzene ND 0.0047 0.00031 mg/kg
98-06-6 tert-Butylbenzene ND 0.00094 0.00027 mg/kg
56-23-5 Carbon Tetrachloride ND 0.00094 0.00037 mg/kg
108-90-7 Chlorobenzene ND 0.00094 0.00023 mg/kg
75-00-3 Chloroethane ND b 0.00091 0.00031 mg/kg
67-66-3 Chloroform ND 0.00094 0.00025 mg/kg
95-49-8 o-Chlorotoluene ND 0.0047 0.00046 mg/kg
106-43-4 p-Chlorotoluene ND 0.0047 0.000061mg/kg
124-48-1 Dibromochloromethane ND 0.00094 0.00027 mg/kg
96-12-8 1,2-Dibromo-3-chloropropane ND 0.0047 0.00084 mg/kg
106-93-4 1,2-Dibromoethane ND 0.00094 0.00054 mg/kg
75-71-8 Dichlorodifluoromethane ND 0.00094 0.00062 mg/kg
541-73-1 m-Dichlorobenzene ND 0.00094 0.00030 mg/kg
95-50-1 o-Dichlorobenzene ND 0.00094 0.00018 mg/kg
106-46-7 p-Dichlorobenzene ND 0.00094 0.00024 mg/kg
75-34-3 1,1-Dichloroethane ND 0.00094 0.00021 mg/kg
107-06-2 1,2-Dichloroethane ND 0.00094 0.00020 mg/kg
75-35-4 1,1-Dichloroethylene ND 0.00094 0.00038 mg/kg
156-59-2 cis-1,2-Dichloroethylene ND 0.00094 0.00030 mg/kg
156-60-5 trans-1,2-Dichloroethylene ND 0.00094 0.00019 mg/kg
78-87-5 1,2-Dichloropropane 0.00065 0.00094 0.00012 mg/kg J
142-28-9 1,3-Dichloropropane ND 0.00094 0.00022 mg/kg
594-20-7 2,2-Dichloropropane ND 0.00094 0.00032 mg/kg
563-58-6 1,1-Dichloropropene ND 0.00094 0.00031 mg/kg
10061-01-5 cis-1,3-Dichloropropene ND 0.00094 0.00022 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
35 of 90
LA8495433.11
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:B-6 (3-5)
Lab Sample ID:LA84954-11 Date Sampled:11/01/22
Matrix:SO - Soil Date Received:11/03/22
Method:SW846 8260D SW846 5035 Percent Solids:85.6
Project:Phoenix 308-Rocky PT, NC
VOA List for NC
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.00094 0.00025 mg/kg
108-20-3 Di-Isopropyl Ether ND 0.00094 0.00014 mg/kg
64-17-5 Ethyl Alcohol ND 0.38 0.023 mg/kg
100-41-4 Ethylbenzene 0.0200 0.00094 0.00025 mg/kg
591-78-6 2-Hexanone ND 0.012 0.00062 mg/kg
87-68-3 Hexachlorobutadiene ND 0.0047 0.00028 mg/kg
98-82-8 Isopropylbenzene 0.0015 0.0047 0.00027 mg/kg J
99-87-6 p-Isopropyltoluene ND 0.0047 0.00032 mg/kg
74-83-9 Methyl Bromide ND 0.0094 0.0015 mg/kg
74-87-3 Methyl Chloride 0.0011 0.0047 0.00028 mg/kg J
74-95-3 Methylene Bromide ND 0.00094 0.00027 mg/kg
75-09-2 Methylene Chloride ND 0.0047 0.00052 mg/kg
78-93-3 Methyl Ethyl Ketone ND 0.012 0.00072 mg/kg
108-10-1 4-Methyl-2-pentanone ND 0.012 0.00049 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.00094 0.000098mg/kg
91-20-3 Naphthalene 0.00093 0.0047 0.00054 mg/kg J
103-65-1 n-Propylbenzene 0.0042 0.0047 0.00040 mg/kg J
100-42-5 Styrene ND 0.00094 0.00014 mg/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 0.00094 0.00018 mg/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 0.00094 0.00014 mg/kg
127-18-4 Tetrachloroethylene ND 0.00094 0.00032 mg/kg
108-88-3 Toluene 0.0224 0.0047 0.00017 mg/kg
87-61-6 1,2,3-Trichlorobenzene ND 0.0047 0.00031 mg/kg
120-82-1 1,2,4-Trichlorobenzene ND 0.0047 0.00019 mg/kg
71-55-6 1,1,1-Trichloroethane ND 0.00094 0.00033 mg/kg
79-00-5 1,1,2-Trichloroethane ND 0.00094 0.00014 mg/kg
79-01-6 Trichloroethylene ND 0.00094 0.00047 mg/kg
75-69-4 Trichlorofluoromethane ND b 0.00091 0.00033 mg/kg
96-18-4 1,2,3-Trichloropropane ND 0.0047 0.00023 mg/kg
95-63-6 1,2,4-Trimethylbenzene 0.0183 0.0047 0.00036 mg/kg
108-67-8 1,3,5-Trimethylbenzene 0.0064 0.0047 0.00024 mg/kg
108-05-4 Vinyl Acetate ND 0.0047 0.00033 mg/kg
75-01-4 Vinyl Chloride ND 0.00094 0.00025 mg/kg
m,p-Xylene 0.0591 0.0019 0.00042 mg/kg
95-47-6 o-Xylene 0.0263 0.00094 0.00024 mg/kg
1330-20-7 Xylene (total)0.0854 0.0019 0.0011 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 96%89%59-143%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
36 of 90
LA8495433.11
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:B-6 (3-5)
Lab Sample ID:LA84954-11 Date Sampled:11/01/22
Matrix:SO - Soil Date Received:11/03/22
Method:SW846 8260D SW846 5035 Percent Solids:85.6
Project:Phoenix 308-Rocky PT, NC
VOA List for NC
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 102%93%52-159%
460-00-4 4-Bromofluorobenzene 107%102%38-183%
(a) Sample analyzed beyond hold time.
(b) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
37 of 90
LA8495433.11
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:B-6 (3-5)
Lab Sample ID:LA84954-11 Date Sampled:11/01/22
Matrix:SO - Soil Date Received:11/03/22
Method:MADEP VPH REV 2.1 Percent Solids:85.6
Project:Phoenix 308-Rocky PT, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LE039205.D 1 11/07/22 19:05 KM n/a n/a GLE2311
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 6.4 g 5.0 ml 100 ul
Run #2
MA VPH list
CAS No.Compound Result RL MDL Units Q
C5- C8 Aliphatics (Unadj.)ND 5.4 2.7 mg/kg
C9- C12 Aliphatics (Unadj.)ND 5.4 2.7 mg/kg
C9- C10 Aromatics (Unadj.)ND 5.4 2.7 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
615-59-8 2,5-Dibromotoluene 131% a 70-130%
615-59-8 2,5-Dibromotoluene 128%70-130%
(a) Outside control limits biased high. Sample is ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
38 of 90
LA8495433.11
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:B-6 (7-9)
Lab Sample ID:LA84954-12 Date Sampled:11/01/22
Matrix:SO - Soil Date Received:11/03/22
Method:SW846 8015C SW846 5035 Percent Solids:76.5
Project:Phoenix 308-Rocky PT, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LA416860.D 1 11/09/22 17:16 KM 11/05/22 10:00 n/a GLA3797
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 6.20 g 5.0 ml 100 ul
Run #2
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)8.42 6.8 3.3 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 88%64-128%
540-36-3 1,4-Difluorobenzene 107%80-122%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
39 of 90
LA8495433.12
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:B-7 (3-5)
Lab Sample ID:LA84954-13 Date Sampled:11/01/22
Matrix:SO - Soil Date Received:11/03/22
Method:SW846 8260D SW846 5035 Percent Solids:82.5
Project:Phoenix 308-Rocky PT, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2H0084538.D 1 11/15/22 21:56 MB 11/05/22 10:00 n/a V2H3248
Run #2 a 2H0084616.D 1 11/18/22 15:16 JY 11/05/22 10:00 n/a V2H3251
Initial Weight
Run #1 5.5 g
Run #2 5.7 g
VOA List for NC
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 0.0359 0.055 0.0024 mg/kg J
71-43-2 Benzene 0.0110 0.00055 0.00022 mg/kg
108-86-1 Bromobenzene ND 0.0011 0.00033 mg/kg
74-97-5 Bromochloromethane ND 0.0011 0.00030 mg/kg
75-27-4 Bromodichloromethane ND 0.0011 0.00035 mg/kg
75-25-2 Bromoform ND 0.0011 0.00088 mg/kg
104-51-8 n-Butylbenzene ND 0.0055 0.00036 mg/kg
135-98-8 sec-Butylbenzene 0.00056 0.0055 0.00036 mg/kg J
98-06-6 tert-Butylbenzene ND 0.0011 0.00032 mg/kg
56-23-5 Carbon Tetrachloride ND 0.0011 0.00043 mg/kg
108-90-7 Chlorobenzene ND 0.0011 0.00027 mg/kg
75-00-3 Chloroethane ND b 0.0011 0.00036 mg/kg
67-66-3 Chloroform ND 0.0011 0.00029 mg/kg
95-49-8 o-Chlorotoluene ND 0.0055 0.00054 mg/kg
106-43-4 p-Chlorotoluene ND 0.0055 0.000072mg/kg
124-48-1 Dibromochloromethane ND 0.0011 0.00032 mg/kg
96-12-8 1,2-Dibromo-3-chloropropane ND 0.0055 0.00098 mg/kg
106-93-4 1,2-Dibromoethane ND 0.0011 0.00063 mg/kg
75-71-8 Dichlorodifluoromethane ND 0.0011 0.00072 mg/kg
541-73-1 m-Dichlorobenzene ND 0.0011 0.00035 mg/kg
95-50-1 o-Dichlorobenzene ND 0.0011 0.00021 mg/kg
106-46-7 p-Dichlorobenzene ND 0.0011 0.00029 mg/kg
75-34-3 1,1-Dichloroethane ND 0.0011 0.00025 mg/kg
107-06-2 1,2-Dichloroethane ND 0.0011 0.00024 mg/kg
75-35-4 1,1-Dichloroethylene ND 0.0011 0.00045 mg/kg
156-59-2 cis-1,2-Dichloroethylene ND 0.0011 0.00035 mg/kg
156-60-5 trans-1,2-Dichloroethylene ND 0.0011 0.00022 mg/kg
78-87-5 1,2-Dichloropropane ND 0.0011 0.00014 mg/kg
142-28-9 1,3-Dichloropropane ND 0.0011 0.00026 mg/kg
594-20-7 2,2-Dichloropropane ND 0.0011 0.00038 mg/kg
563-58-6 1,1-Dichloropropene ND 0.0011 0.00036 mg/kg
10061-01-5 cis-1,3-Dichloropropene ND 0.0011 0.00026 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
40 of 90
LA8495433.13
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:B-7 (3-5)
Lab Sample ID:LA84954-13 Date Sampled:11/01/22
Matrix:SO - Soil Date Received:11/03/22
Method:SW846 8260D SW846 5035 Percent Solids:82.5
Project:Phoenix 308-Rocky PT, NC
VOA List for NC
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.0011 0.00029 mg/kg
108-20-3 Di-Isopropyl Ether 0.00020 0.0011 0.00016 mg/kg J
64-17-5 Ethyl Alcohol ND 0.44 0.027 mg/kg
100-41-4 Ethylbenzene 0.0345 0.0011 0.00029 mg/kg
591-78-6 2-Hexanone ND 0.014 0.00072 mg/kg
87-68-3 Hexachlorobutadiene ND 0.0055 0.00033 mg/kg
98-82-8 Isopropylbenzene 0.0029 0.0055 0.00031 mg/kg J
99-87-6 p-Isopropyltoluene ND 0.0055 0.00038 mg/kg
74-83-9 Methyl Bromide ND 0.011 0.0017 mg/kg
74-87-3 Methyl Chloride ND 0.0055 0.00033 mg/kg
74-95-3 Methylene Bromide ND 0.0011 0.00032 mg/kg
75-09-2 Methylene Chloride ND 0.0055 0.00061 mg/kg
78-93-3 Methyl Ethyl Ketone 0.0097 0.014 0.00085 mg/kg J
108-10-1 4-Methyl-2-pentanone ND 0.014 0.00057 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.0011 0.00011 mg/kg
91-20-3 Naphthalene 0.0056 0.0055 0.00063 mg/kg
103-65-1 n-Propylbenzene 0.0087 0.0055 0.00047 mg/kg
100-42-5 Styrene ND 0.0011 0.00016 mg/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 0.0011 0.00022 mg/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 0.0011 0.00016 mg/kg
127-18-4 Tetrachloroethylene ND 0.0011 0.00038 mg/kg
108-88-3 Toluene 0.0593 0.0055 0.00020 mg/kg
87-61-6 1,2,3-Trichlorobenzene ND 0.0055 0.00036 mg/kg
120-82-1 1,2,4-Trichlorobenzene ND 0.0055 0.00023 mg/kg
71-55-6 1,1,1-Trichloroethane ND 0.0011 0.00039 mg/kg
79-00-5 1,1,2-Trichloroethane ND 0.0011 0.00017 mg/kg
79-01-6 Trichloroethylene ND 0.0011 0.00055 mg/kg
75-69-4 Trichlorofluoromethane ND b 0.0011 0.00038 mg/kg
96-18-4 1,2,3-Trichloropropane ND 0.0055 0.00027 mg/kg
95-63-6 1,2,4-Trimethylbenzene 0.0423 0.0055 0.00042 mg/kg
108-67-8 1,3,5-Trimethylbenzene 0.0146 0.0055 0.00028 mg/kg
108-05-4 Vinyl Acetate ND 0.0055 0.00039 mg/kg
75-01-4 Vinyl Chloride ND 0.0011 0.00029 mg/kg
m,p-Xylene 0.111 0.0022 0.00050 mg/kg
95-47-6 o-Xylene 0.0567 0.0011 0.00028 mg/kg
1330-20-7 Xylene (total)0.167 0.0022 0.0013 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 110%107%59-143%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:B-7 (3-5)
Lab Sample ID:LA84954-13 Date Sampled:11/01/22
Matrix:SO - Soil Date Received:11/03/22
Method:SW846 8260D SW846 5035 Percent Solids:82.5
Project:Phoenix 308-Rocky PT, NC
VOA List for NC
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 107%100%52-159%
460-00-4 4-Bromofluorobenzene 113%111%38-183%
(a) Sample analyzed beyond hold time.
(b) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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LA8495433.13
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:B-7 (3-5)
Lab Sample ID:LA84954-13 Date Sampled:11/01/22
Matrix:SO - Soil Date Received:11/03/22
Method:MADEP VPH REV 2.1 Percent Solids:82.5
Project:Phoenix 308-Rocky PT, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LE039206.D 1 11/07/22 19:36 KM n/a n/a GLE2311
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 5.8 g 5.0 ml 100 ul
Run #2
MA VPH list
CAS No.Compound Result RL MDL Units Q
C5- C8 Aliphatics (Unadj.)ND 6.3 3.1 mg/kg
C9- C12 Aliphatics (Unadj.)ND 6.3 3.1 mg/kg
C9- C10 Aromatics (Unadj.)ND 6.3 3.1 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
615-59-8 2,5-Dibromotoluene 127%70-130%
615-59-8 2,5-Dibromotoluene 123%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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LA8495433.13
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:B-7 (7-9)
Lab Sample ID:LA84954-14 Date Sampled:11/01/22
Matrix:SO - Soil Date Received:11/03/22
Method:SW846 8015C SW846 5035 Percent Solids:76.6
Project:Phoenix 308-Rocky PT, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LA416862.D 1 11/09/22 17:38 KM 11/05/22 10:00 n/a GLA3797
Run #2 a LA416820.D 1 11/09/22 06:37 KM 11/05/22 10:00 n/a GLA3796
Initial Weight Final Volume Methanol Aliquot
Run #1 6.00 g 5.0 ml 10.0 ul
Run #2 6.00 g 5.0 ml 100 ul
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)1440 70 34 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 98%88%64-128%
540-36-3 1,4-Difluorobenzene 96%87%80-122%
(a) Sample used for QC purposes only.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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LA8495433.14
SGS North America Inc.
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Scott, LA
Section 4
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LA849544
LA84954: Chain of Custody
Page 1 of 6
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LA8495444.1
LA84954: Chain of Custody
Page 2 of 6
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LA8495444.1
LA84954: Chain of Custody
Page 3 of 6
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LA8495444.1
LA84954: Chain of Custody
Page 4 of 6
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LA8495444.1
Job Number:LA84954 Client:ATC ASSOCIATES
Date / Time Received:11/3/2022 9:00:00 AM Delivery Method:FED EX
Project:PHOENIX #308
4. No. Coolers:1
Airbill #'s:
Cooler Security
1. Custody Seals Present:
Y or N
2. Custody Seals Intact:
3. COC Present:
4. Smpl Dates/Time OK
2. Thermometer ID:
Cooler Temperature Y or N
1. Temp criteria achieved:
3. Cooler media:
IR002;
Ice (direct contact)
Quality Control Preservation Y or N N/A
1. Trip Blank present / cooler:
2. Trip Blank listed on COC:
3. Samples preserved properly:
4. VOCs headspace free:
Sample Integrity - Documentation Y or N
1. Sample labels present on bottles:
2. Container labeling complete:
3. Sample container label / COC agree:
Sample Integrity - Condition Y or N
1. Sample recvd within HT:
3. Condition of sample:
2. All containers accounted for:
Sample Integrity - Instructions
1. Analysis requested is clear:
2. Bottles received for unspecified tests
3. Sufficient volume recvd for analysis:
4. Compositing instructions clear:
5. Filtering instructions clear:
Intact
Y or N
Comments
Y or N N/A
Cooler Temps (Initial/Adjusted):#1: (3.2/3);
SGS Sample Receipt Summary
LA84954: Chain of Custody
Page 5 of 6
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LA8495444.1
Page 2 of 2
Problem Resolution
CSR:Response Date:
Response:
Job Number:LA84954
LA84954: Chain of Custody
Page 6 of 6
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SGS North America Inc.
MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Scott, LA
Section 5
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LA849545
Method Blank Summary Page 1 of 3
Job Number:LA84954
Account:ATCNCR Atlas
Project:Phoenix 308-Rocky PT, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2X5814-MB1 2X01306872.D 1 11/15/22 JS n/a n/a V2X5814
The QC reported here applies to the following samples:Method: SW846 8260D
LA84954-3, LA84954-5, LA84954-7
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 301 2500 110 ug/kg J
71-43-2 Benzene ND 25 9.9 ug/kg
108-86-1 Bromobenzene ND 50 15 ug/kg
74-97-5 Bromochloromethane ND 50 14 ug/kg
75-27-4 Bromodichloromethane ND 50 16 ug/kg
75-25-2 Bromoform ND 50 40 ug/kg
104-51-8 n-Butylbenzene ND 250 16 ug/kg
135-98-8 sec-Butylbenzene ND 250 16 ug/kg
98-06-6 tert-Butylbenzene ND 50 14 ug/kg
56-23-5 Carbon Tetrachloride ND 50 20 ug/kg
108-90-7 Chlorobenzene ND 50 12 ug/kg
75-00-3 Chloroethane ND 50 17 ug/kg
67-66-3 Chloroform ND 50 13 ug/kg
95-49-8 o-Chlorotoluene ND 250 24 ug/kg
106-43-4 p-Chlorotoluene ND 250 3.3 ug/kg
124-48-1 Dibromochloromethane ND 50 14 ug/kg
96-12-8 1,2-Dibromo-3-chloropropane ND 250 45 ug/kg
106-93-4 1,2-Dibromoethane ND 50 29 ug/kg
75-71-8 Dichlorodifluoromethane ND 50 33 ug/kg
541-73-1 m-Dichlorobenzene ND 50 16 ug/kg
95-50-1 o-Dichlorobenzene ND 50 9.7 ug/kg
106-46-7 p-Dichlorobenzene ND 50 13 ug/kg
75-34-3 1,1-Dichloroethane ND 50 11 ug/kg
107-06-2 1,2-Dichloroethane ND 50 11 ug/kg
75-35-4 1,1-Dichloroethylene ND 50 20 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 50 16 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 50 10 ug/kg
78-87-5 1,2-Dichloropropane ND 50 6.3 ug/kg
142-28-9 1,3-Dichloropropane ND 50 12 ug/kg
594-20-7 2,2-Dichloropropane ND 50 17 ug/kg
563-58-6 1,1-Dichloropropene ND 50 17 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 50 12 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 50 13 ug/kg
108-20-3 Di-Isopropyl Ether ND 50 7.3 ug/kg
64-17-5 Ethyl Alcohol 20400 20000 1200 ug/kg
100-41-4 Ethylbenzene ND 50 13 ug/kg
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LA8495455.1.1
Method Blank Summary Page 2 of 3
Job Number:LA84954
Account:ATCNCR Atlas
Project:Phoenix 308-Rocky PT, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2X5814-MB1 2X01306872.D 1 11/15/22 JS n/a n/a V2X5814
The QC reported here applies to the following samples:Method: SW846 8260D
LA84954-3, LA84954-5, LA84954-7
CAS No.Compound Result RL MDL Units Q
591-78-6 2-Hexanone ND 630 33 ug/kg
87-68-3 Hexachlorobutadiene 46.1 250 15 ug/kg J
98-82-8 Isopropylbenzene ND 250 14 ug/kg
99-87-6 p-Isopropyltoluene ND 250 17 ug/kg
74-83-9 Methyl Bromide ND 500 78 ug/kg
74-87-3 Methyl Chloride ND 250 15 ug/kg
74-95-3 Methylene Bromide ND 50 14 ug/kg
75-09-2 Methylene Chloride ND 250 28 ug/kg
78-93-3 Methyl Ethyl Ketone 164 630 38 ug/kg J
108-10-1 4-Methyl-2-pentanone ND 630 26 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 50 5.2 ug/kg
91-20-3 Naphthalene 71.5 250 29 ug/kg J
103-65-1 n-Propylbenzene ND 250 21 ug/kg
100-42-5 Styrene ND 50 7.3 ug/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 50 9.8 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 50 7.4 ug/kg
127-18-4 Tetrachloroethylene ND 50 17 ug/kg
108-88-3 Toluene ND 250 9.0 ug/kg
87-61-6 1,2,3-Trichlorobenzene 62.9 250 16 ug/kg J
120-82-1 1,2,4-Trichlorobenzene 41.6 250 10 ug/kg J
71-55-6 1,1,1-Trichloroethane ND 50 18 ug/kg
79-00-5 1,1,2-Trichloroethane ND 50 7.5 ug/kg
79-01-6 Trichloroethylene ND 50 25 ug/kg
75-69-4 Trichlorofluoromethane ND 50 18 ug/kg
96-18-4 1,2,3-Trichloropropane ND 250 12 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 250 19 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 250 13 ug/kg
108-05-4 Vinyl Acetate ND 250 18 ug/kg
75-01-4 Vinyl Chloride ND 50 13 ug/kg
m,p-Xylene ND 100 23 ug/kg
95-47-6 o-Xylene ND 50 13 ug/kg
1330-20-7 Xylene (total)ND 100 58 ug/kg
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LA8495455.1.1
Method Blank Summary Page 3 of 3
Job Number:LA84954
Account:ATCNCR Atlas
Project:Phoenix 308-Rocky PT, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2X5814-MB1 2X01306872.D 1 11/15/22 JS n/a n/a V2X5814
The QC reported here applies to the following samples:Method: SW846 8260D
LA84954-3, LA84954-5, LA84954-7
CAS No.Surrogate Recoveries Limits
17060-07-0 1,2-Dichloroethane-D4 86%59-143%
2037-26-5 Toluene-D8 99%52-159%
460-00-4 4-Bromofluorobenzene 97%38-183%
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LA8495455.1.1
Method Blank Summary Page 1 of 3
Job Number:LA84954
Account:ATCNCR Atlas
Project:Phoenix 308-Rocky PT, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2H3248-MB1 2H0084533.D 1 11/15/22 MB n/a n/a V2H3248
The QC reported here applies to the following samples:Method: SW846 8260D
LA84954-1, LA84954-5, LA84954-7, LA84954-11, LA84954-13
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 5.9 50 2.2 ug/kg J
71-43-2 Benzene ND 0.50 0.20 ug/kg
108-86-1 Bromobenzene ND 1.0 0.30 ug/kg
74-97-5 Bromochloromethane ND 1.0 0.27 ug/kg
75-27-4 Bromodichloromethane ND 1.0 0.32 ug/kg
75-25-2 Bromoform ND 1.0 0.80 ug/kg
104-51-8 n-Butylbenzene ND 5.0 0.32 ug/kg
135-98-8 sec-Butylbenzene ND 5.0 0.33 ug/kg
98-06-6 tert-Butylbenzene ND 1.0 0.29 ug/kg
56-23-5 Carbon Tetrachloride ND 1.0 0.39 ug/kg
108-90-7 Chlorobenzene ND 1.0 0.25 ug/kg
75-00-3 Chloroethane ND 1.0 0.34 ug/kg
67-66-3 Chloroform ND 1.0 0.26 ug/kg
95-49-8 o-Chlorotoluene ND 5.0 0.49 ug/kg
106-43-4 p-Chlorotoluene ND 5.0 0.065 ug/kg
124-48-1 Dibromochloromethane ND 1.0 0.29 ug/kg
96-12-8 1,2-Dibromo-3-chloropropane ND 5.0 0.89 ug/kg
106-93-4 1,2-Dibromoethane ND 1.0 0.57 ug/kg
75-71-8 Dichlorodifluoromethane ND 1.0 0.65 ug/kg
541-73-1 m-Dichlorobenzene ND 1.0 0.32 ug/kg
95-50-1 o-Dichlorobenzene ND 1.0 0.19 ug/kg
106-46-7 p-Dichlorobenzene ND 1.0 0.26 ug/kg
75-34-3 1,1-Dichloroethane ND 1.0 0.23 ug/kg
107-06-2 1,2-Dichloroethane ND 1.0 0.22 ug/kg
75-35-4 1,1-Dichloroethylene ND 1.0 0.41 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 1.0 0.31 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 1.0 0.20 ug/kg
78-87-5 1,2-Dichloropropane ND 1.0 0.13 ug/kg
142-28-9 1,3-Dichloropropane ND 1.0 0.24 ug/kg
594-20-7 2,2-Dichloropropane ND 1.0 0.34 ug/kg
563-58-6 1,1-Dichloropropene ND 1.0 0.33 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 1.0 0.24 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 1.0 0.26 ug/kg
108-20-3 Di-Isopropyl Ether ND 1.0 0.15 ug/kg
64-17-5 Ethyl Alcohol ND 400 25 ug/kg
100-41-4 Ethylbenzene ND 1.0 0.26 ug/kg
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LA8495455.1.2
Method Blank Summary Page 2 of 3
Job Number:LA84954
Account:ATCNCR Atlas
Project:Phoenix 308-Rocky PT, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2H3248-MB1 2H0084533.D 1 11/15/22 MB n/a n/a V2H3248
The QC reported here applies to the following samples:Method: SW846 8260D
LA84954-1, LA84954-5, LA84954-7, LA84954-11, LA84954-13
CAS No.Compound Result RL MDL Units Q
591-78-6 2-Hexanone ND 13 0.66 ug/kg
87-68-3 Hexachlorobutadiene ND 5.0 0.30 ug/kg
98-82-8 Isopropylbenzene ND 5.0 0.28 ug/kg
99-87-6 p-Isopropyltoluene ND 5.0 0.34 ug/kg
74-83-9 Methyl Bromide ND 10 1.6 ug/kg
74-87-3 Methyl Chloride ND 5.0 0.30 ug/kg
74-95-3 Methylene Bromide ND 1.0 0.29 ug/kg
75-09-2 Methylene Chloride 0.74 5.0 0.56 ug/kg J
78-93-3 Methyl Ethyl Ketone ND 13 0.77 ug/kg
108-10-1 4-Methyl-2-pentanone ND 13 0.52 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 1.0 0.10 ug/kg
91-20-3 Naphthalene ND 5.0 0.57 ug/kg
103-65-1 n-Propylbenzene ND 5.0 0.43 ug/kg
100-42-5 Styrene ND 1.0 0.15 ug/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 1.0 0.20 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 0.15 ug/kg
127-18-4 Tetrachloroethylene ND 1.0 0.34 ug/kg
108-88-3 Toluene ND 5.0 0.18 ug/kg
87-61-6 1,2,3-Trichlorobenzene 0.34 5.0 0.33 ug/kg J
120-82-1 1,2,4-Trichlorobenzene 0.27 5.0 0.21 ug/kg J
71-55-6 1,1,1-Trichloroethane ND 1.0 0.35 ug/kg
79-00-5 1,1,2-Trichloroethane ND 1.0 0.15 ug/kg
79-01-6 Trichloroethylene ND 1.0 0.50 ug/kg
75-69-4 Trichlorofluoromethane ND 1.0 0.36 ug/kg
96-18-4 1,2,3-Trichloropropane ND 5.0 0.25 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 5.0 0.38 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 5.0 0.25 ug/kg
108-05-4 Vinyl Acetate ND 5.0 0.35 ug/kg
75-01-4 Vinyl Chloride ND 1.0 0.26 ug/kg
m,p-Xylene ND 2.0 0.45 ug/kg
95-47-6 o-Xylene ND 1.0 0.26 ug/kg
1330-20-7 Xylene (total)ND 2.0 1.2 ug/kg
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LA8495455.1.2
Method Blank Summary Page 3 of 3
Job Number:LA84954
Account:ATCNCR Atlas
Project:Phoenix 308-Rocky PT, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2H3248-MB1 2H0084533.D 1 11/15/22 MB n/a n/a V2H3248
The QC reported here applies to the following samples:Method: SW846 8260D
LA84954-1, LA84954-5, LA84954-7, LA84954-11, LA84954-13
CAS No.Surrogate Recoveries Limits
17060-07-0 1,2-Dichloroethane-D4 112%59-143%
2037-26-5 Toluene-D8 108%52-159%
460-00-4 4-Bromofluorobenzene 110%38-183%
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LA8495455.1.2
Method Blank Summary Page 1 of 3
Job Number:LA84954
Account:ATCNCR Atlas
Project:Phoenix 308-Rocky PT, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2J4441-MB1 2J0123366.D 1 11/15/22 NN n/a n/a V2J4441
The QC reported here applies to the following samples:Method: SW846 8260D
LA84954-9
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 2500 110 ug/kg
71-43-2 Benzene ND 25 9.9 ug/kg
108-86-1 Bromobenzene ND 50 15 ug/kg
74-97-5 Bromochloromethane ND 50 14 ug/kg
75-27-4 Bromodichloromethane ND 50 16 ug/kg
75-25-2 Bromoform ND 50 40 ug/kg
104-51-8 n-Butylbenzene ND 250 16 ug/kg
135-98-8 sec-Butylbenzene ND 250 16 ug/kg
98-06-6 tert-Butylbenzene ND 50 14 ug/kg
56-23-5 Carbon Tetrachloride ND 50 20 ug/kg
108-90-7 Chlorobenzene ND 50 12 ug/kg
75-00-3 Chloroethane ND 50 17 ug/kg
67-66-3 Chloroform ND 50 13 ug/kg
95-49-8 o-Chlorotoluene ND 250 24 ug/kg
106-43-4 p-Chlorotoluene ND 250 3.3 ug/kg
124-48-1 Dibromochloromethane ND 50 14 ug/kg
96-12-8 1,2-Dibromo-3-chloropropane ND 250 45 ug/kg
106-93-4 1,2-Dibromoethane ND 50 29 ug/kg
75-71-8 Dichlorodifluoromethane ND 50 33 ug/kg
541-73-1 m-Dichlorobenzene ND 50 16 ug/kg
95-50-1 o-Dichlorobenzene ND 50 9.7 ug/kg
106-46-7 p-Dichlorobenzene ND 50 13 ug/kg
75-34-3 1,1-Dichloroethane ND 50 11 ug/kg
107-06-2 1,2-Dichloroethane ND 50 11 ug/kg
75-35-4 1,1-Dichloroethylene ND 50 20 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 50 16 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 50 10 ug/kg
78-87-5 1,2-Dichloropropane ND 50 6.3 ug/kg
142-28-9 1,3-Dichloropropane ND 50 12 ug/kg
594-20-7 2,2-Dichloropropane ND 50 17 ug/kg
563-58-6 1,1-Dichloropropene ND 50 17 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 50 12 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 50 13 ug/kg
108-20-3 Di-Isopropyl Ether ND 50 7.3 ug/kg
64-17-5 Ethyl Alcohol ND 20000 1200 ug/kg
100-41-4 Ethylbenzene ND 50 13 ug/kg
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LA8495455.1.3
Method Blank Summary Page 2 of 3
Job Number:LA84954
Account:ATCNCR Atlas
Project:Phoenix 308-Rocky PT, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2J4441-MB1 2J0123366.D 1 11/15/22 NN n/a n/a V2J4441
The QC reported here applies to the following samples:Method: SW846 8260D
LA84954-9
CAS No.Compound Result RL MDL Units Q
591-78-6 2-Hexanone ND 630 33 ug/kg
87-68-3 Hexachlorobutadiene 32.5 250 15 ug/kg J
98-82-8 Isopropylbenzene ND 250 14 ug/kg
99-87-6 p-Isopropyltoluene ND 250 17 ug/kg
74-83-9 Methyl Bromide ND 500 78 ug/kg
74-87-3 Methyl Chloride ND 250 15 ug/kg
74-95-3 Methylene Bromide ND 50 14 ug/kg
75-09-2 Methylene Chloride ND 250 28 ug/kg
78-93-3 Methyl Ethyl Ketone ND 630 38 ug/kg
108-10-1 4-Methyl-2-pentanone ND 630 26 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 50 5.2 ug/kg
91-20-3 Naphthalene 36.3 250 29 ug/kg J
103-65-1 n-Propylbenzene ND 250 21 ug/kg
100-42-5 Styrene ND 50 7.3 ug/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 50 9.8 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 50 7.4 ug/kg
127-18-4 Tetrachloroethylene ND 50 17 ug/kg
108-88-3 Toluene ND 250 9.0 ug/kg
87-61-6 1,2,3-Trichlorobenzene 44.9 250 16 ug/kg J
120-82-1 1,2,4-Trichlorobenzene 33.7 250 10 ug/kg J
71-55-6 1,1,1-Trichloroethane ND 50 18 ug/kg
79-00-5 1,1,2-Trichloroethane ND 50 7.5 ug/kg
79-01-6 Trichloroethylene ND 50 25 ug/kg
75-69-4 Trichlorofluoromethane ND 50 18 ug/kg
96-18-4 1,2,3-Trichloropropane ND 250 12 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 250 19 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 250 13 ug/kg
108-05-4 Vinyl Acetate ND 250 18 ug/kg
75-01-4 Vinyl Chloride ND 50 13 ug/kg
m,p-Xylene ND 100 23 ug/kg
95-47-6 o-Xylene ND 50 13 ug/kg
1330-20-7 Xylene (total)ND 100 58 ug/kg
60 of 90
LA8495455.1.3
Method Blank Summary Page 3 of 3
Job Number:LA84954
Account:ATCNCR Atlas
Project:Phoenix 308-Rocky PT, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2J4441-MB1 2J0123366.D 1 11/15/22 NN n/a n/a V2J4441
The QC reported here applies to the following samples:Method: SW846 8260D
LA84954-9
CAS No.Surrogate Recoveries Limits
17060-07-0 1,2-Dichloroethane-D4 99%59-143%
2037-26-5 Toluene-D8 99%52-159%
460-00-4 4-Bromofluorobenzene 98%38-183%
61 of 90
LA8495455.1.3
Method Blank Summary Page 1 of 1
Job Number:LA84954
Account:ATCNCR Atlas
Project:Phoenix 308-Rocky PT, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2H3251-MB1 2H0084607.D 1 11/18/22 JY n/a n/a V2H3251
The QC reported here applies to the following samples:Method: SW846 8260B
LA84954-1, LA84954-11, LA84954-13
CAS No.Compound Result RL MDL Units Q
75-00-3 Chloroethane ND 1.0 0.34 ug/kg
75-69-4 Trichlorofluoromethane ND 1.0 0.36 ug/kg
CAS No.Surrogate Recoveries Limits
17060-07-0 1,2-Dichloroethane-D4 114%59-143%
2037-26-5 Toluene-D8 105%52-159%
460-00-4 4-Bromofluorobenzene 110%38-183%
62 of 90
LA8495455.1.4
Blank Spike/Blank Spike Duplicate Summary Page 1 of 3
Job Number:LA84954
Account:ATCNCR Atlas
Project:Phoenix 308-Rocky PT, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2X5814-BS1 2X01306870.D 1 11/15/22 JS n/a n/a V2X5814
V2X5814-BSD1 2X01306871.D 1 11/15/22 JS n/a n/a V2X5814
The QC reported here applies to the following samples:Method: SW846 8260D
LA84954-3, LA84954-5, LA84954-7
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/kg ug/kg %ug/kg %RPD Rec/RPD
67-64-1 Acetone 2450 1840 75 1990 81 8 40-153/30
71-43-2 Benzene 980 855 87 857 87 0 67-135/30
108-86-1 Bromobenzene 980 965 98 964 98 0 54-144/30
74-97-5 Bromochloromethane 980 741 76 750 77 1 50-147/30
75-27-4 Bromodichloromethane 980 837 85 851 87 2 54-146/30
75-25-2 Bromoform 980 931 95 967 99 4 49-145/30
104-51-8 n-Butylbenzene 980 958 98 950 97 1 47-160/30
135-98-8 sec-Butylbenzene 980 947 97 888 91 6 51-155/30
98-06-6 tert-Butylbenzene 980 913 93 870 89 5 53-152/30
56-23-5 Carbon Tetrachloride 980 823 84 824 84 0 50-152/30
108-90-7 Chlorobenzene 980 908 93 913 93 1 57-144/30
75-00-3 Chloroethane 980 1030 105 1010 103 2 38-176/30
67-66-3 Chloroform 980 816 83 826 84 1 53-147/30
95-49-8 o-Chlorotoluene 980 942 96 936 95 1 52-151/30
106-43-4 p-Chlorotoluene 980 919 94 918 94 0 52-150/30
124-48-1 Dibromochloromethane 980 894 91 901 92 1 54-146/30
96-12-8 1,2-Dibromo-3-chloropropane 980 912 93 1000 102 9 51-145/30
106-93-4 1,2-Dibromoethane 980 900 92 921 94 2 55-145/30
75-71-8 Dichlorodifluoromethane 980 656 67 630 64 4 24-179/30
541-73-1 m-Dichlorobenzene 980 909 93 926 94 2 54-147/30
95-50-1 o-Dichlorobenzene 980 924 94 926 94 0 55-144/30
106-46-7 p-Dichlorobenzene 980 911 93 914 93 0 54-147/30
75-34-3 1,1-Dichloroethane 980 841 86 852 87 1 53-148/30
107-06-2 1,2-Dichloroethane 980 788 80 816 83 3 55-144/30
75-35-4 1,1-Dichloroethylene 980 901 92 877 89 3 49-153/30
156-59-2 cis-1,2-Dichloroethylene 980 860 88 842 86 2 52-147/30
156-60-5 trans-1,2-Dichloroethylene 980 873 89 878 90 1 51-152/30
78-87-5 1,2-Dichloropropane 980 879 90 892 91 1 56-145/30
142-28-9 1,3-Dichloropropane 980 858 88 891 91 4 53-145/30
594-20-7 2,2-Dichloropropane 980 933 95 930 95 0 35-176/30
563-58-6 1,1-Dichloropropene 980 839 86 835 85 0 49-157/30
10061-01-5 cis-1,3-Dichloropropene 980 886 90 912 93 3 54-148/30
10061-02-6 trans-1,3-Dichloropropene 980 893 91 905 92 1 53-151/30
108-20-3 Di-Isopropyl Ether 980 831 85 856 87 3 85-120/30
64-17-5 Ethyl Alcohol 19600 29800 152 30300 155 2 31-164/30
100-41-4 Ethylbenzene 980 861 88 858 88 0 69-136/30
* = Outside of Control Limits.
63 of 90
LA8495455.2.1
Blank Spike/Blank Spike Duplicate Summary Page 2 of 3
Job Number:LA84954
Account:ATCNCR Atlas
Project:Phoenix 308-Rocky PT, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2X5814-BS1 2X01306870.D 1 11/15/22 JS n/a n/a V2X5814
V2X5814-BSD1 2X01306871.D 1 11/15/22 JS n/a n/a V2X5814
The QC reported here applies to the following samples:Method: SW846 8260D
LA84954-3, LA84954-5, LA84954-7
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/kg ug/kg %ug/kg %RPD Rec/RPD
591-78-6 2-Hexanone 2450 2080 85 2270 93 9 45-148/30
87-68-3 Hexachlorobutadiene 980 847 86 809 83 5 48-168/30
98-82-8 Isopropylbenzene 980 921 94 929 95 1 52-151/30
99-87-6 p-Isopropyltoluene 980 953 97 922 94 3 50-155/30
74-83-9 Methyl Bromide 980 753 77 800 82 6 40-170/30
74-87-3 Methyl Chloride 980 867 88 861 88 1 39-152/30
74-95-3 Methylene Bromide 980 857 87 894 91 4 53-147/30
75-09-2 Methylene Chloride 980 793 81 790 81 0 51-142/30
78-93-3 Methyl Ethyl Ketone 2450 2000 82 2290 93 14 48-150/30
108-10-1 4-Methyl-2-pentanone 2450 2160 88 2320 95 7 50-151/30
1634-04-4 Methyl Tert Butyl Ether 980 836 85 881 90 5 61-142/30
91-20-3 Naphthalene 980 972 99 1020 104 5 58-147/30
103-65-1 n-Propylbenzene 980 923 94 916 93 1 50-154/30
100-42-5 Styrene 980 902 92 923 94 2 56-145/30
630-20-6 1,1,1,2-Tetrachloroethane 980 937 96 929 95 1 56-147/30
79-34-5 1,1,2,2-Tetrachloroethane 980 839 86 919 94 9 55-141/30
127-18-4 Tetrachloroethylene 980 975 99 994 101 2 54-156/30
108-88-3 Toluene 980 867 88 868 89 0 71-135/30
87-61-6 1,2,3-Trichlorobenzene 980 874 89 945 96 8 51-157/30
120-82-1 1,2,4-Trichlorobenzene 980 918 94 949 97 3 48-163/30
71-55-6 1,1,1-Trichloroethane 980 846 86 853 87 1 52-153/30
79-00-5 1,1,2-Trichloroethane 980 883 90 903 92 2 55-144/30
79-01-6 Trichloroethylene 980 931 95 930 95 0 56-151/30
75-69-4 Trichlorofluoromethane 980 782 80 779 79 0 36-171/30
96-18-4 1,2,3-Trichloropropane 980 811 83 796 81 2 45-139/30
95-63-6 1,2,4-Trimethylbenzene 980 919 94 903 92 2 50-153/30
108-67-8 1,3,5-Trimethylbenzene 980 904 92 911 93 1 51-153/30
108-05-4 Vinyl Acetate 980 868 89 904 92 4 23-188/30
75-01-4 Vinyl Chloride 980 840 86 834 85 1 42-155/30
m,p-Xylene 1960 1640 84 1700 87 4 70-140/30
95-47-6 o-Xylene 980 845 86 845 86 0 70-132/30
1330-20-7 Xylene (total)2940 2480 84 2550 87 3 69-138/30
* = Outside of Control Limits.
64 of 90
LA8495455.2.1
Blank Spike/Blank Spike Duplicate Summary Page 3 of 3
Job Number:LA84954
Account:ATCNCR Atlas
Project:Phoenix 308-Rocky PT, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2X5814-BS1 2X01306870.D 1 11/15/22 JS n/a n/a V2X5814
V2X5814-BSD1 2X01306871.D 1 11/15/22 JS n/a n/a V2X5814
The QC reported here applies to the following samples:Method: SW846 8260D
LA84954-3, LA84954-5, LA84954-7
CAS No.Surrogate Recoveries BSP BSD Limits
17060-07-0 1,2-Dichloroethane-D4 85%84%59-143%
2037-26-5 Toluene-D8 99%100%52-159%
460-00-4 4-Bromofluorobenzene 97%99%38-183%
* = Outside of Control Limits.
65 of 90
LA8495455.2.1
Blank Spike/Blank Spike Duplicate Summary Page 1 of 3
Job Number:LA84954
Account:ATCNCR Atlas
Project:Phoenix 308-Rocky PT, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2H3248-BS1 2H0084531.D 1 11/15/22 MB n/a n/a V2H3248
V2H3248-BSD1 2H0084532.D 1 11/15/22 MB n/a n/a V2H3248
The QC reported here applies to the following samples:Method: SW846 8260D
LA84954-1, LA84954-5, LA84954-7, LA84954-11, LA84954-13
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/kg ug/kg %ug/kg %RPD Rec/RPD
67-64-1 Acetone 50 63.8 128 71.0 142 11 40-153/30
71-43-2 Benzene 20 20.7 104 20.3 102 2 67-135/30
108-86-1 Bromobenzene 20 19.2 96 18.8 94 2 54-144/30
74-97-5 Bromochloromethane 20 21.8 109 22.4 112 3 50-147/30
75-27-4 Bromodichloromethane 20 20.0 100 20.4 102 2 54-146/30
75-25-2 Bromoform 20 16.0 80 17.3 87 8 49-145/30
104-51-8 n-Butylbenzene 20 18.8 94 17.7 89 6 47-160/30
135-98-8 sec-Butylbenzene 20 19.3 97 18.0 90 7 51-155/30
98-06-6 tert-Butylbenzene 20 19.7 99 18.3 92 7 53-152/30
56-23-5 Carbon Tetrachloride 20 19.3 97 20.0 100 4 50-152/30
108-90-7 Chlorobenzene 20 18.6 93 18.1 91 3 57-144/30
75-00-3 Chloroethane 20 3.6 18*12.0 60 108*38-176/30
67-66-3 Chloroform 20 18.7 94 18.6 93 1 53-147/30
95-49-8 o-Chlorotoluene 20 19.4 97 18.0 90 7 52-151/30
106-43-4 p-Chlorotoluene 20 19.5 98 18.5 93 5 52-150/30
124-48-1 Dibromochloromethane 20 19.8 99 21.1 106 6 54-146/30
96-12-8 1,2-Dibromo-3-chloropropane 20 20.1 101 21.5 108 7 51-145/30
106-93-4 1,2-Dibromoethane 20 20.6 103 21.3 107 3 55-145/30
75-71-8 Dichlorodifluoromethane 20 20.1 101 21.0 105 4 24-179/30
541-73-1 m-Dichlorobenzene 20 19.5 98 18.6 93 5 54-147/30
95-50-1 o-Dichlorobenzene 20 19.0 95 18.3 92 4 55-144/30
106-46-7 p-Dichlorobenzene 20 19.6 98 18.7 94 5 54-147/30
75-34-3 1,1-Dichloroethane 20 20.3 102 20.1 101 1 53-148/30
107-06-2 1,2-Dichloroethane 20 21.1 106 21.7 109 3 55-144/30
75-35-4 1,1-Dichloroethylene 20 22.3 112 18.5 93 19 49-153/30
156-59-2 cis-1,2-Dichloroethylene 20 20.5 103 19.3 97 6 52-147/30
156-60-5 trans-1,2-Dichloroethylene 20 20.1 101 18.8 94 7 51-152/30
78-87-5 1,2-Dichloropropane 20 19.5 98 19.8 99 2 56-145/30
142-28-9 1,3-Dichloropropane 20 22.3 112 22.2 111 0 53-145/30
594-20-7 2,2-Dichloropropane 20 21.4 107 21.2 106 1 35-176/30
563-58-6 1,1-Dichloropropene 20 22.3 112 21.4 107 4 49-157/30
10061-01-5 cis-1,3-Dichloropropene 20 19.5 98 20.3 102 4 54-148/30
10061-02-6 trans-1,3-Dichloropropene 20 20.8 104 21.4 107 3 53-151/30
108-20-3 Di-Isopropyl Ether 20 21.5 108 21.8 109 1 85-120/30
64-17-5 Ethyl Alcohol 400 371 93 376 94 1 31-164/30
100-41-4 Ethylbenzene 20 21.9 110 20.6 103 6 69-136/30
* = Outside of Control Limits.
66 of 90
LA8495455.2.2
Blank Spike/Blank Spike Duplicate Summary Page 2 of 3
Job Number:LA84954
Account:ATCNCR Atlas
Project:Phoenix 308-Rocky PT, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2H3248-BS1 2H0084531.D 1 11/15/22 MB n/a n/a V2H3248
V2H3248-BSD1 2H0084532.D 1 11/15/22 MB n/a n/a V2H3248
The QC reported here applies to the following samples:Method: SW846 8260D
LA84954-1, LA84954-5, LA84954-7, LA84954-11, LA84954-13
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/kg ug/kg %ug/kg %RPD Rec/RPD
591-78-6 2-Hexanone 50 53.7 107 63.7 127 17 45-148/30
87-68-3 Hexachlorobutadiene 20 21.0 105 19.9 100 5 48-168/30
98-82-8 Isopropylbenzene 20 19.5 98 18.1 91 7 52-151/30
99-87-6 p-Isopropyltoluene 20 20.0 100 18.6 93 7 50-155/30
74-83-9 Methyl Bromide 20 17.0 85 18.3 92 7 40-170/30
74-87-3 Methyl Chloride 20 21.8 109 23.0 115 5 39-152/30
74-95-3 Methylene Bromide 20 19.8 99 20.7 104 4 53-147/30
75-09-2 Methylene Chloride 20 22.3 112 21.5 108 4 51-142/30
78-93-3 Methyl Ethyl Ketone 50 56.2 112 64.4 129 14 48-150/30
108-10-1 4-Methyl-2-pentanone 50 45.6 91 53.3 107 16 50-151/30
1634-04-4 Methyl Tert Butyl Ether 20 19.8 99 20.4 102 3 61-142/30
91-20-3 Naphthalene 20 17.7 89 18.3 92 3 58-147/30
103-65-1 n-Propylbenzene 20 19.5 98 18.7 94 4 50-154/30
100-42-5 Styrene 20 20.7 104 19.7 99 5 56-145/30
630-20-6 1,1,1,2-Tetrachloroethane 20 20.6 103 20.4 102 1 56-147/30
79-34-5 1,1,2,2-Tetrachloroethane 20 19.0 95 20.2 101 6 55-141/30
127-18-4 Tetrachloroethylene 20 18.8 94 17.6 88 7 54-156/30
108-88-3 Toluene 20 19.8 99 18.8 94 5 71-135/30
87-61-6 1,2,3-Trichlorobenzene 20 17.6 88 16.6 83 6 51-157/30
120-82-1 1,2,4-Trichlorobenzene 20 17.6 88 16.7 84 5 48-163/30
71-55-6 1,1,1-Trichloroethane 20 19.7 99 19.4 97 2 52-153/30
79-00-5 1,1,2-Trichloroethane 20 19.2 96 19.6 98 2 55-144/30
79-01-6 Trichloroethylene 20 18.9 95 18.3 92 3 56-151/30
75-69-4 Trichlorofluoromethane 20 7.6 38 17.7 89 80*36-171/30
96-18-4 1,2,3-Trichloropropane 20 19.0 95 20.2 101 6 45-139/30
95-63-6 1,2,4-Trimethylbenzene 20 18.6 93 17.6 88 6 50-153/30
108-67-8 1,3,5-Trimethylbenzene 20 19.1 96 17.7 89 8 51-153/30
108-05-4 Vinyl Acetate 20 21.5 108 23.0 115 7 23-188/30
75-01-4 Vinyl Chloride 20 19.6 98 21.6 108 10 42-155/30
m,p-Xylene 40 37.8 95 35.4 89 7 70-140/30
95-47-6 o-Xylene 20 21.6 108 20.2 101 7 70-132/30
1330-20-7 Xylene (total)60 59.5 99 55.6 93 7 69-138/30
* = Outside of Control Limits.
67 of 90
LA8495455.2.2
Blank Spike/Blank Spike Duplicate Summary Page 3 of 3
Job Number:LA84954
Account:ATCNCR Atlas
Project:Phoenix 308-Rocky PT, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2H3248-BS1 2H0084531.D 1 11/15/22 MB n/a n/a V2H3248
V2H3248-BSD1 2H0084532.D 1 11/15/22 MB n/a n/a V2H3248
The QC reported here applies to the following samples:Method: SW846 8260D
LA84954-1, LA84954-5, LA84954-7, LA84954-11, LA84954-13
CAS No.Surrogate Recoveries BSP BSD Limits
17060-07-0 1,2-Dichloroethane-D4 99%100%59-143%
2037-26-5 Toluene-D8 101%104%52-159%
460-00-4 4-Bromofluorobenzene 103%101%38-183%
* = Outside of Control Limits.
68 of 90
LA8495455.2.2
Blank Spike/Blank Spike Duplicate Summary Page 1 of 3
Job Number:LA84954
Account:ATCNCR Atlas
Project:Phoenix 308-Rocky PT, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2J4441-BS1 2J0123362A.D 1 11/15/22 NN n/a n/a V2J4441
V2J4441-BSD1 2J0123364A.D 1 11/15/22 NN n/a n/a V2J4441
The QC reported here applies to the following samples:Method: SW846 8260B
LA84954-9
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/kg ug/kg %ug/kg %RPD Rec/RPD
67-64-1 Acetone 2500 2100 84 2190 88 4 40-153/30
71-43-2 Benzene 1000 983 98 977 98 1 67-135/30
108-86-1 Bromobenzene 1000 963 96 982 98 2 54-144/30
74-97-5 Bromochloromethane 1000 976 98 944 94 3 50-147/30
75-27-4 Bromodichloromethane 1000 1010 101 963 96 5 54-146/30
75-25-2 Bromoform 1000 1030 103 1040 104 1 49-145/30
104-51-8 n-Butylbenzene 1000 1030 103 1040 104 1 47-160/30
135-98-8 sec-Butylbenzene 1000 1050 105 1040 104 1 51-155/30
98-06-6 tert-Butylbenzene 1000 1050 105 1030 103 2 53-152/30
56-23-5 Carbon Tetrachloride 1000 1030 103 998 100 3 50-152/30
108-90-7 Chlorobenzene 1000 995 100 971 97 2 57-144/30
75-00-3 Chloroethane 1000 962 96 947 95 2 38-176/30
67-66-3 Chloroform 1000 1060 106 1050 105 1 53-147/30
95-49-8 o-Chlorotoluene 1000 1040 104 1010 101 3 52-151/30
106-43-4 p-Chlorotoluene 1000 1040 104 1030 103 1 52-150/30
124-48-1 Dibromochloromethane 1000 964 96 953 95 1 54-146/30
96-12-8 1,2-Dibromo-3-chloropropane 1000 970 97 1020 102 5 51-145/30
106-93-4 1,2-Dibromoethane 1000 1050 105 1010 101 4 55-145/30
75-71-8 Dichlorodifluoromethane 1000 855 86 830 83 3 24-179/30
541-73-1 m-Dichlorobenzene 1000 998 100 985 99 1 54-147/30
95-50-1 o-Dichlorobenzene 1000 991 99 976 98 2 55-144/30
106-46-7 p-Dichlorobenzene 1000 984 98 973 97 1 54-147/30
75-34-3 1,1-Dichloroethane 1000 983 98 971 97 1 53-148/30
107-06-2 1,2-Dichloroethane 1000 971 97 970 97 0 55-144/30
75-35-4 1,1-Dichloroethylene 1000 980 98 959 96 2 49-153/30
156-59-2 cis-1,2-Dichloroethylene 1000 1000 100 996 100 0 52-147/30
156-60-5 trans-1,2-Dichloroethylene 1000 988 99 976 98 1 51-152/30
78-87-5 1,2-Dichloropropane 1000 954 95 955 96 0 56-145/30
142-28-9 1,3-Dichloropropane 1000 1000 100 987 99 1 53-145/30
594-20-7 2,2-Dichloropropane 1000 1060 106 1040 104 2 35-176/30
563-58-6 1,1-Dichloropropene 1000 1030 103 1010 101 2 49-157/30
10061-01-5 cis-1,3-Dichloropropene 1000 1050 105 1020 102 3 54-148/30
10061-02-6 trans-1,3-Dichloropropene 1000 1060 106 1050 105 1 53-151/30
108-20-3 Di-Isopropyl Ether 1000 996 100 991 99 1 85-120/30
64-17-5 Ethyl Alcohol 20000 9250 46 12600 63 31* a 31-164/30
100-41-4 Ethylbenzene 1000 1000 100 973 97 3 69-136/30
* = Outside of Control Limits.
69 of 90
LA8495455.2.3
Blank Spike/Blank Spike Duplicate Summary Page 2 of 3
Job Number:LA84954
Account:ATCNCR Atlas
Project:Phoenix 308-Rocky PT, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2J4441-BS1 2J0123362A.D 1 11/15/22 NN n/a n/a V2J4441
V2J4441-BSD1 2J0123364A.D 1 11/15/22 NN n/a n/a V2J4441
The QC reported here applies to the following samples:Method: SW846 8260B
LA84954-9
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/kg ug/kg %ug/kg %RPD Rec/RPD
591-78-6 2-Hexanone 2500 2760 110 2760 110 0 45-148/30
87-68-3 Hexachlorobutadiene 1000 1030 103 986 99 4 48-168/30
98-82-8 Isopropylbenzene 1000 1050 105 1010 101 4 52-151/30
99-87-6 p-Isopropyltoluene 1000 1060 106 1060 106 0 50-155/30
74-83-9 Methyl Bromide 1000 1050 105 955 96 9 40-170/30
74-87-3 Methyl Chloride 1000 935 94 930 93 1 39-152/30
74-95-3 Methylene Bromide 1000 992 99 993 99 0 53-147/30
75-09-2 Methylene Chloride 1000 736 74 726 73 1 51-142/30
78-93-3 Methyl Ethyl Ketone 2500 2530 101 2630 105 4 48-150/30
108-10-1 4-Methyl-2-pentanone 2500 2750 110 2750 110 0 50-151/30
1634-04-4 Methyl Tert Butyl Ether 1000 1050 105 1040 104 1 61-142/30
91-20-3 Naphthalene 1000 1110 111 1120 112 1 58-147/30
103-65-1 n-Propylbenzene 1000 1020 102 1010 101 1 50-154/30
100-42-5 Styrene 1000 1050 105 1030 103 2 56-145/30
630-20-6 1,1,1,2-Tetrachloroethane 1000 1020 102 995 100 2 56-147/30
79-34-5 1,1,2,2-Tetrachloroethane 1000 1030 103 1030 103 0 55-141/30
127-18-4 Tetrachloroethylene 1000 949 95 921 92 3 54-156/30
108-88-3 Toluene 1000 1000 100 983 98 2 71-135/30
87-61-6 1,2,3-Trichlorobenzene 1000 1030 103 1050 105 2 51-157/30
120-82-1 1,2,4-Trichlorobenzene 1000 1020 102 1040 104 2 48-163/30
71-55-6 1,1,1-Trichloroethane 1000 1000 100 998 100 0 52-153/30
79-00-5 1,1,2-Trichloroethane 1000 1000 100 971 97 3 55-144/30
79-01-6 Trichloroethylene 1000 993 99 968 97 3 56-151/30
75-69-4 Trichlorofluoromethane 1000 1010 101 971 97 4 36-171/30
96-18-4 1,2,3-Trichloropropane 1000 995 100 1010 101 1 45-139/30
95-63-6 1,2,4-Trimethylbenzene 1000 1050 105 1040 104 1 50-153/30
108-67-8 1,3,5-Trimethylbenzene 1000 1040 104 1030 103 1 51-153/30
108-05-4 Vinyl Acetate 1000 1070 107 1050 105 2 23-188/30
75-01-4 Vinyl Chloride 1000 938 94 908 91 3 42-155/30
m,p-Xylene 2000 2020 101 1970 99 3 70-140/30
95-47-6 o-Xylene 1000 1030 103 1020 102 1 70-132/30
1330-20-7 Xylene (total)3000 3050 102 2990 100 2 69-138/30
* = Outside of Control Limits.
70 of 90
LA8495455.2.3
Blank Spike/Blank Spike Duplicate Summary Page 3 of 3
Job Number:LA84954
Account:ATCNCR Atlas
Project:Phoenix 308-Rocky PT, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2J4441-BS1 2J0123362A.D 1 11/15/22 NN n/a n/a V2J4441
V2J4441-BSD1 2J0123364A.D 1 11/15/22 NN n/a n/a V2J4441
The QC reported here applies to the following samples:Method: SW846 8260B
LA84954-9
CAS No.Surrogate Recoveries BSP BSD Limits
17060-07-0 1,2-Dichloroethane-D4 97%99%59-143%
2037-26-5 Toluene-D8 101%100%52-159%
460-00-4 4-Bromofluorobenzene 101%101%38-183%
(a) RPD exceeded criteria. However, both recoveries passed criteria and the samples were ND.
* = Outside of Control Limits.
71 of 90
LA8495455.2.3
Blank Spike/Blank Spike Duplicate Summary Page 1 of 1
Job Number:LA84954
Account:ATCNCR Atlas
Project:Phoenix 308-Rocky PT, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2H3251-BS1 2H0084605.D 1 11/18/22 JY n/a n/a V2H3251
V2H3251-BSD1 2H0084606.D 1 11/18/22 JY n/a n/a V2H3251
The QC reported here applies to the following samples:Method: SW846 8260B
LA84954-1, LA84954-11, LA84954-13
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/kg ug/kg %ug/kg %RPD Rec/RPD
75-00-3 Chloroethane 20 23.7 119 21.4 107 10 38-176/30
75-69-4 Trichlorofluoromethane 20 22.0 110 21.6 108 2 36-171/30
CAS No.Surrogate Recoveries BSP BSD Limits
17060-07-0 1,2-Dichloroethane-D4 100%101%59-143%
2037-26-5 Toluene-D8 99%100%52-159%
460-00-4 4-Bromofluorobenzene 103%103%38-183%
* = Outside of Control Limits.
72 of 90
LA8495455.2.4
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3
Job Number:LA84954
Account:ATCNCR Atlas
Project:Phoenix 308-Rocky PT, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
LA84897-1MS 2X01306895.D 1 11/15/22 JS n/a n/a V2X5814
LA84897-1MSD 2X01306896.D 1 11/15/22 JS n/a n/a V2X5814
LA84897-1 2X01306878.D 1 11/15/22 JS n/a n/a V2X5814
The QC reported here applies to the following samples:Method: SW846 8260D
LA84954-3, LA84954-5, LA84954-7
LA84897-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
67-64-1 Acetone 2680 J 7840 5910 41 7840 6260 46 6 19-170/34
71-43-2 Benzene 42 U 3140 2040 65 3140 2040 65 0 15-162/33
108-86-1 Bromobenzene 84 U 3140 2540 81 3140 2540 81 0 28-151/33
74-97-5 Bromochloromethane 84 U 3140 2070 66 3140 2340 75 12 9-176/15
75-27-4 Bromodichloromethane 84 U 3140 2240 71 3140 2150 69 4 48-124/14
75-25-2 Bromoform 84 U 3140 2740 87 3140 2580 82 6 20-128/16
104-51-8 n-Butylbenzene 3720 3140 2070 -53*3140 2020 -54*2 1-199/21
135-98-8 sec-Butylbenzene 63.0 J 3140 2030 63 3140 1920 59 6 16-172/16
98-06-6 tert-Butylbenzene 84 U 3140 1860 59 3140 1780 57 4 27-150/16
56-23-5 Carbon Tetrachloride 84 U 3140 1560 50 3140 1490 48 5 25-136/17
108-90-7 Chlorobenzene 90.7 3140 2280 70 3140 2220 68 3 31-153/12
75-00-3 Chloroethane 84 U 3140 2430 77 3140 1740 55 33 1-171/64
67-66-3 Chloroform 84 U 3140 2070 66 3140 2010 64 3 26-153/42
95-49-8 o-Chlorotoluene 420 U 3140 2270 72 3140 2160 69 5 47-138/16
106-43-4 p-Chlorotoluene 420 U 3140 2320 74 3140 2260 72 3 11-159/14
124-48-1 Dibromochloromethane 84 U 3140 2460 78 3140 2360 75 4 26-131/14
96-12-8 1,2-Dibromo-3-chloropropane 420 U 3140 2710 86 3140 2650 85 2 18-141/68
106-93-4 1,2-Dibromoethane 84 U 3140 2820 90 3140 2680 85 5 39-143/14
75-71-8 Dichlorodifluoromethane 84 U 3140 1040 33 3140 1010 32 3 1-149/18
541-73-1 m-Dichlorobenzene 84 U 3140 2340 75 3140 2330 74 0 22-152/15
95-50-1 o-Dichlorobenzene 84 U 3140 2480 79 3140 2380 76 4 27-150/12
106-46-7 p-Dichlorobenzene 84 U 3140 2330 74 3140 2340 75 0 19-154/12
75-34-3 1,1-Dichloroethane 23.1 J 3140 1990 63 3140 1960 62 2 31-147/13
107-06-2 1,2-Dichloroethane 84 U 3140 2280 73 3140 2210 70 3 31-147/13
75-35-4 1,1-Dichloroethylene 84 U 3140 1860 59 3140 1730 55 7 22-148/19
156-59-2 cis-1,2-Dichloroethylene 84 U 3140 2140 68 3140 2160 69 1 25-145/15
156-60-5 trans-1,2-Dichloroethylene 84 U 3140 2000 64 3140 1910 61 5 24-145/17
78-87-5 1,2-Dichloropropane 84 U 3140 2270 72 3140 2280 73 0 36-141/13
142-28-9 1,3-Dichloropropane 84 U 3140 2590 83 3140 2530 81 2 35-147/12
594-20-7 2,2-Dichloropropane 84 U 3140 1870 60 3140 1830 58 2 45-150/18
563-58-6 1,1-Dichloropropene 84 U 3140 1740 55 3140 1660 53 5 28-146/16
10061-01-5 cis-1,3-Dichloropropene 84 U 3140 2360 75 3140 2270 72 4 27-143/12
10061-02-6 trans-1,3-Dichloropropene 84 U 3140 2420 77 3140 2420 77 0 46-130/14
108-20-3 Di-Isopropyl Ether 227 3140 2250 65 3140 2190 63 3 34-149/13
64-17-5 Ethyl Alcohol 34000 U 62700 37200 59 62700 104000 166*95 1-159/146
100-41-4 Ethylbenzene 80.1 J 3140 2060 63 3140 1990 61 3 14-168/13
* = Outside of Control Limits.
73 of 90
LA8495455.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3
Job Number:LA84954
Account:ATCNCR Atlas
Project:Phoenix 308-Rocky PT, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
LA84897-1MS 2X01306895.D 1 11/15/22 JS n/a n/a V2X5814
LA84897-1MSD 2X01306896.D 1 11/15/22 JS n/a n/a V2X5814
LA84897-1 2X01306878.D 1 11/15/22 JS n/a n/a V2X5814
The QC reported here applies to the following samples:Method: SW846 8260D
LA84954-3, LA84954-5, LA84954-7
LA84897-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
591-78-6 2-Hexanone 1100 U 7840 6860 88 7840 6790 87 1 16-169/26
87-68-3 Hexachlorobutadiene 420 U 3140 1840 59 3140 1990 63 8 8-154/68
98-82-8 Isopropylbenzene 43.2 J 3140 2080 65 3140 2030 63 2 12-186/18
99-87-6 p-Isopropyltoluene 94.6 J 3140 2090 64 3140 2020 61 3 15-171/18
74-83-9 Methyl Bromide 840 U 3140 1790 57 3140 1880 60 5 1-178/40
74-87-3 Methyl Chloride 420 U 3140 1920 61 3140 1820 58 5 1-151/37
74-95-3 Methylene Bromide 84 U 3140 2550 81 3140 2540 81 0 39-143/14
75-09-2 Methylene Chloride 420 U 3140 2110 67 3140 2110 67 0 27-147/18
78-93-3 Methyl Ethyl Ketone 4610 7840 6820 28*7840 7360 35 8 29-156/32
108-10-1 4-Methyl-2-pentanone 1100 U 7840 7090 90 7840 6950 89 2 33-160/23
1634-04-4 Methyl Tert Butyl Ether 84 U 3140 2610 83 3140 2580 82 1 37-145/14
91-20-3 Naphthalene 455 3140 2870 77 3140 2910 78 1 1-192/73
103-65-1 n-Propylbenzene 420 U 3140 2120 68 3140 2030 65 4 8-170/17
100-42-5 Styrene 84 U 3140 2320 74 3140 2280 73 2 24-165/13
630-20-6 1,1,1,2-Tetrachloroethane 84 U 3140 2350 75 3140 2310 74 2 33-140/13
79-34-5 1,1,2,2-Tetrachloroethane 84 U 3140 2690 86 3140 2610 83 3 33-146/48
127-18-4 Tetrachloroethylene 47.3 J 3140 3620 114 3140 3630 114 0 21-149/18
108-88-3 Toluene 220 J 3140 2030 58 3140 2010 57 1 11-173/43
87-61-6 1,2,3-Trichlorobenzene 420 U 3140 2450 78 3140 2540 81 4 17-154/66
120-82-1 1,2,4-Trichlorobenzene 420 U 3140 2430 77 3140 2420 77 0 15-155/65
71-55-6 1,1,1-Trichloroethane 84 U 3140 1730 55 3140 1700 54 2 31-142/16
79-00-5 1,1,2-Trichloroethane 84 U 3140 2620 84 3140 2590 83 1 11-185/16
79-01-6 Trichloroethylene 84 U 3140 2160 69 3140 2110 67 2 21-154/15
75-69-4 Trichlorofluoromethane 84 U 3140 1130 36 3140 1060 34 6 1-163/27
96-18-4 1,2,3-Trichloropropane 223 J 3140 2650 77 3140 2590 75 2 33-157/18
95-63-6 1,2,4-Trimethylbenzene 6750 3140 2270 -143* a 3140 2110 -148* a 7 90-183/15
108-67-8 1,3,5-Trimethylbenzene 1730 3140 2120 12 3140 2060 11 3 10-179/14
108-05-4 Vinyl Acetate 1070 3140 2120 33 3140 2030 31 4 14-146/16
75-01-4 Vinyl Chloride 84 U 3140 1470 47 3140 1390 44 6 32-153/15
m,p-Xylene 1270 6270 4000 44 6270 3910 42 2 14-175/12
95-47-6 o-Xylene 376 3140 2140 56 3140 2100 55 2 19-167/13
1330-20-7 Xylene (total)1640 9410 6140 48 9410 6010 46 2 14-172/12
* = Outside of Control Limits.
74 of 90
LA8495455.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number:LA84954
Account:ATCNCR Atlas
Project:Phoenix 308-Rocky PT, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
LA84897-1MS 2X01306895.D 1 11/15/22 JS n/a n/a V2X5814
LA84897-1MSD 2X01306896.D 1 11/15/22 JS n/a n/a V2X5814
LA84897-1 2X01306878.D 1 11/15/22 JS n/a n/a V2X5814
The QC reported here applies to the following samples:Method: SW846 8260D
LA84954-3, LA84954-5, LA84954-7
CAS No.Surrogate Recoveries MS MSD LA84897-1 Limits
17060-07-0 1,2-Dichloroethane-D4 86%84%85%59-143%
2037-26-5 Toluene-D8 99%98%84%52-159%
460-00-4 4-Bromofluorobenzene 97%97%99%38-183%
(a) Outside control limits due to high level in sample relative to spike amount.
* = Outside of Control Limits.
75 of 90
LA8495455.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3
Job Number:LA84954
Account:ATCNCR Atlas
Project:Phoenix 308-Rocky PT, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
LA84884-6MS 2J0123404.D 1 11/16/22 NN n/a n/a V2J4441
LA84884-6MSD 2J0123406.D 1 11/16/22 NN n/a n/a V2J4441
LA84884-6 2J0123374.D 1 11/15/22 NN n/a n/a V2J4441
The QC reported here applies to the following samples:Method: SW846 8260B
LA84954-9
LA84884-6 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
67-64-1 Acetone 3100 U 12500 9100 73 12500 9350 75 3 19-170/34
71-43-2 Benzene 31 U 5020 4960 99 5020 4860 97 2 15-162/33
108-86-1 Bromobenzene 63 U 5020 4910 98 5020 4940 98 1 28-151/33
74-97-5 Bromochloromethane 63 U 5020 4610 92 5020 4610 92 0 9-176/15
75-27-4 Bromodichloromethane 63 U 5020 4480 89 5020 4340 87 3 48-124/14
75-25-2 Bromoform 63 U 5020 4460 89 5020 4570 91 2 20-128/16
104-51-8 n-Butylbenzene 310 U 5020 5360 107 5020 5220 104 3 1-199/21
135-98-8 sec-Butylbenzene 310 U 5020 5270 105 5020 5260 105 0 16-172/16
98-06-6 tert-Butylbenzene 63 U 5020 5190 103 5020 5120 102 1 27-150/16
56-23-5 Carbon Tetrachloride 63 U 5020 4390 87 5020 4300 86 2 25-136/17
108-90-7 Chlorobenzene 63 U 5020 5010 100 5020 4970 99 1 31-153/12
75-00-3 Chloroethane 63 U 5020 3480 69 5020 3750 75 7 1-171/64
67-66-3 Chloroform 63 U 5020 5130 102 5020 5100 102 1 26-153/42
95-49-8 o-Chlorotoluene 310 U 5020 5290 105 5020 5190 103 2 47-138/16
106-43-4 p-Chlorotoluene 310 U 5020 5260 105 5020 5100 102 3 11-159/14
124-48-1 Dibromochloromethane 63 U 5020 4190 84 5020 4270 85 2 26-131/14
96-12-8 1,2-Dibromo-3-chloropropane 310 U 5020 4880 97 5020 4800 96 2 18-141/68
106-93-4 1,2-Dibromoethane 63 U 5020 5050 101 5020 5150 103 2 39-143/14
75-71-8 Dichlorodifluoromethane 63 U 5020 3960 79 5020 3910 78 1 1-149/18
541-73-1 m-Dichlorobenzene 63 U 5020 5080 101 5020 4990 99 2 22-152/15
95-50-1 o-Dichlorobenzene 63 U 5020 5100 102 5020 5020 100 2 27-150/12
106-46-7 p-Dichlorobenzene 63 U 5020 5010 100 5020 4960 99 1 19-154/12
75-34-3 1,1-Dichloroethane 63 U 5020 4770 95 5020 4820 96 1 31-147/13
107-06-2 1,2-Dichloroethane 63 U 5020 4740 94 5020 4680 93 1 31-147/13
75-35-4 1,1-Dichloroethylene 63 U 5020 4350 87 5020 4370 87 0 22-148/19
156-59-2 cis-1,2-Dichloroethylene 63 U 5020 4810 96 5020 4860 97 1 25-145/15
156-60-5 trans-1,2-Dichloroethylene 63 U 5020 4710 94 5020 4510 90 4 24-145/17
78-87-5 1,2-Dichloropropane 11.3 J 5020 4920 98 5020 4760 95 3 36-141/13
142-28-9 1,3-Dichloropropane 63 U 5020 5080 101 5020 5130 102 1 35-147/12
594-20-7 2,2-Dichloropropane 63 U 5020 4350 87 5020 4380 87 1 45-150/18
563-58-6 1,1-Dichloropropene 63 U 5020 4840 96 5020 4790 95 1 28-146/16
10061-01-5 cis-1,3-Dichloropropene 63 U 5020 4850 97 5020 4770 95 2 27-143/12
10061-02-6 trans-1,3-Dichloropropene 63 U 5020 5120 102 5020 5000 100 2 46-130/14
108-20-3 Di-Isopropyl Ether 63 U 5020 4900 98 5020 4830 96 1 34-149/13
64-17-5 Ethyl Alcohol 25000 U 100000 38500 38 100000 52500 52 31 1-159/146
100-41-4 Ethylbenzene 40.4 J 5020 5040 100 5020 4960 98 2 14-168/13
* = Outside of Control Limits.
76 of 90
LA8495455.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3
Job Number:LA84954
Account:ATCNCR Atlas
Project:Phoenix 308-Rocky PT, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
LA84884-6MS 2J0123404.D 1 11/16/22 NN n/a n/a V2J4441
LA84884-6MSD 2J0123406.D 1 11/16/22 NN n/a n/a V2J4441
LA84884-6 2J0123374.D 1 11/15/22 NN n/a n/a V2J4441
The QC reported here applies to the following samples:Method: SW846 8260B
LA84954-9
LA84884-6 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
591-78-6 2-Hexanone 780 U 12500 14300 114 12500 13900 111 3 16-169/26
87-68-3 Hexachlorobutadiene 310 U 5020 4780 95 5020 4660 93 3 8-154/68
98-82-8 Isopropylbenzene 310 U 5020 5290 105 5020 5210 104 2 12-186/18
99-87-6 p-Isopropyltoluene 310 U 5020 5390 107 5020 5240 104 3 15-171/18
74-83-9 Methyl Bromide 630 U 5020 3740 75 5020 3990 80 6 1-178/40
74-87-3 Methyl Chloride 310 U 5020 5200 104 5020 4860 97 7 1-151/37
74-95-3 Methylene Bromide 63 U 5020 4880 97 5020 4920 98 1 39-143/14
75-09-2 Methylene Chloride 310 U 5020 2990 60 5020 3210 64 7 27-147/18
78-93-3 Methyl Ethyl Ketone 780 U 12500 12900 103 12500 12700 101 2 29-156/32
108-10-1 4-Methyl-2-pentanone 780 U 12500 14300 114 12500 14000 112 2 33-160/23
1634-04-4 Methyl Tert Butyl Ether 63 U 5020 5050 101 5020 5160 103 2 37-145/14
91-20-3 Naphthalene 310 U 5020 5810 116 5020 5760 115 1 1-192/73
103-65-1 n-Propylbenzene 310 U 5020 5200 104 5020 5190 103 0 8-170/17
100-42-5 Styrene 63 U 5020 5210 104 5020 5300 106 2 24-165/13
630-20-6 1,1,1,2-Tetrachloroethane 63 U 5020 4790 95 5020 4680 93 2 33-140/13
79-34-5 1,1,2,2-Tetrachloroethane 63 U 5020 5260 105 5020 5310 106 1 33-146/48
127-18-4 Tetrachloroethylene 63 U 5020 5930 118 5020 5940 118 0 21-149/18
108-88-3 Toluene 310 U 5020 5090 101 5020 5030 100 1 11-173/43
87-61-6 1,2,3-Trichlorobenzene 310 U 5020 5080 101 5020 5220 104 3 17-154/66
120-82-1 1,2,4-Trichlorobenzene 310 U 5020 5150 103 5020 5120 102 1 15-155/65
71-55-6 1,1,1-Trichloroethane 63 U 5020 4770 95 5020 4640 92 3 31-142/16
79-00-5 1,1,2-Trichloroethane 63 U 5020 5190 103 5020 5070 101 2 11-185/16
79-01-6 Trichloroethylene 63 U 5020 4840 96 5020 4770 95 1 21-154/15
75-69-4 Trichlorofluoromethane 63 U 5020 3790 76 5020 3790 76 0 1-163/27
96-18-4 1,2,3-Trichloropropane 310 U 5020 5310 106 5020 5240 104 1 33-157/18
95-63-6 1,2,4-Trimethylbenzene 310 U 5020 5420 108 5020 5320 106 2 90-183/15
108-67-8 1,3,5-Trimethylbenzene 310 U 5020 5390 107 5020 5220 104 3 10-179/14
108-05-4 Vinyl Acetate 310 U 5020 4650 93 5020 4660 93 0 14-146/16
75-01-4 Vinyl Chloride 63 U 5020 4300 86 5020 4310 86 0 32-153/15
m,p-Xylene 130 U 10000 10100 101 10000 9960 99 1 14-175/12
95-47-6 o-Xylene 63 U 5020 5150 103 5020 5160 103 0 19-167/13
1330-20-7 Xylene (total)130 U 15100 15200 101 15100 15100 100 1 14-172/12
* = Outside of Control Limits.
77 of 90
LA8495455.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number:LA84954
Account:ATCNCR Atlas
Project:Phoenix 308-Rocky PT, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
LA84884-6MS 2J0123404.D 1 11/16/22 NN n/a n/a V2J4441
LA84884-6MSD 2J0123406.D 1 11/16/22 NN n/a n/a V2J4441
LA84884-6 2J0123374.D 1 11/15/22 NN n/a n/a V2J4441
The QC reported here applies to the following samples:Method: SW846 8260B
LA84954-9
CAS No.Surrogate Recoveries MS MSD LA84884-6 Limits
17060-07-0 1,2-Dichloroethane-D4 100%99%97%59-143%
2037-26-5 Toluene-D8 99%98%98%52-159%
460-00-4 4-Bromofluorobenzene 99%98%96%38-183%
* = Outside of Control Limits.
78 of 90
LA8495455.3.2
SGS North America Inc.
GC Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Scott, LA
Section 6
79 of 90
LA849546
Method Blank Summary Page 1 of 1
Job Number:LA84954
Account:ATCNCR Atlas
Project:Phoenix 308-Rocky PT, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
GLE2311-MB1 LE039195.D 1 11/07/22 KM n/a n/a GLE2311
The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1
LA84954-1, LA84954-3, LA84954-5, LA84954-9, LA84954-11, LA84954-13
CAS No.Compound Result RL MDL Units Q
C5- C8 Aliphatics (Unadj.)ND 5000 2500 ug/kg
C9- C12 Aliphatics (Unadj.)ND 5000 2500 ug/kg
C9- C10 Aromatics (Unadj.)ND 5000 2500 ug/kg
CAS No.Surrogate Recoveries Limits
615-59-8 2,5-Dibromotoluene 96%70-130%
615-59-8 2,5-Dibromotoluene 94%70-130%
80 of 90
LA8495466.1.1
Method Blank Summary Page 1 of 1
Job Number:LA84954
Account:ATCNCR Atlas
Project:Phoenix 308-Rocky PT, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
GLE2313-MB1 LE039245.D 1 11/10/22 KM n/a n/a GLE2313
The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1
LA84954-3, LA84954-7
CAS No.Compound Result RL MDL Units Q
C5- C8 Aliphatics (Unadj.)ND 5000 2500 ug/kg
C9- C12 Aliphatics (Unadj.)ND 5000 2500 ug/kg
C9- C10 Aromatics (Unadj.)ND 5000 2500 ug/kg
CAS No.Surrogate Recoveries Limits
615-59-8 2,5-Dibromotoluene 104%70-130%
615-59-8 2,5-Dibromotoluene 99%70-130%
81 of 90
LA8495466.1.2
Method Blank Summary Page 1 of 1
Job Number:LA84954
Account:ATCNCR Atlas
Project:Phoenix 308-Rocky PT, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
GLA3796-MB2 LA416800.D 1 11/09/22 KM n/a n/a GLA3796
The QC reported here applies to the following samples:Method: SW846 8015C
LA84954-2, LA84954-4, LA84954-8, LA84954-10
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 5.0 2.4 mg/kg
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 86%64-128%
540-36-3 1,4-Difluorobenzene 102%80-122%
82 of 90
LA8495466.1.3
Method Blank Summary Page 1 of 1
Job Number:LA84954
Account:ATCNCR Atlas
Project:Phoenix 308-Rocky PT, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
GLA3797-MB2 LA416844.D 1 11/09/22 KM n/a n/a GLA3797
The QC reported here applies to the following samples:Method: SW846 8015C
LA84954-6, LA84954-12, LA84954-14
CAS No.Compound Result RL MDL Units Q
TPH-GRO (C6-C10)ND 5.0 2.4 mg/kg
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 88%64-128%
540-36-3 1,4-Difluorobenzene 109%80-122%
83 of 90
LA8495466.1.4
Blank Spike/Blank Spike Duplicate Summary Page 1 of 1
Job Number:LA84954
Account:ATCNCR Atlas
Project:Phoenix 308-Rocky PT, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
GLE2311-BS1 LE039193.D 1 11/07/22 KM n/a n/a GLE2311
GLE2311-BSD1 LE039194.D 1 11/07/22 KM n/a n/a GLE2311
The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1
LA84954-1, LA84954-3, LA84954-5, LA84954-9, LA84954-11, LA84954-13
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/kg ug/kg %ug/kg %RPD Rec/RPD
C5- C8 Aliphatics (Unadj.)6000 5480 91 5400 90 1 70-130/25
C9- C12 Aliphatics (Unadj.)6000 6100 102 5780 96 5 70-130/25
C9- C10 Aromatics (Unadj.)2000 2170 109 2130 107 2 70-130/25
CAS No.Surrogate Recoveries BSP BSD Limits
615-59-8 2,5-Dibromotoluene 101%101%70-130%
615-59-8 2,5-Dibromotoluene 103%100%70-130%
* = Outside of Control Limits.
84 of 90
LA8495466.2.1
Blank Spike/Blank Spike Duplicate Summary Page 1 of 1
Job Number:LA84954
Account:ATCNCR Atlas
Project:Phoenix 308-Rocky PT, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
GLE2313-BS1 LE039243.D 1 11/10/22 KM n/a n/a GLE2313
GLE2313-BSD1 LE039244.D 1 11/10/22 KM n/a n/a GLE2313
The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1
LA84954-3, LA84954-7
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/kg ug/kg %ug/kg %RPD Rec/RPD
C5- C8 Aliphatics (Unadj.)6000 5280 88 5400 90 2 70-130/25
C9- C12 Aliphatics (Unadj.)6000 6260 104 6320 105 1 70-130/25
C9- C10 Aromatics (Unadj.)2000 2180 109 2230 112 2 70-130/25
CAS No.Surrogate Recoveries BSP BSD Limits
615-59-8 2,5-Dibromotoluene 101%105%70-130%
615-59-8 2,5-Dibromotoluene 98%97%70-130%
* = Outside of Control Limits.
85 of 90
LA8495466.2.2
Blank Spike/Blank Spike Duplicate Summary Page 1 of 1
Job Number:LA84954
Account:ATCNCR Atlas
Project:Phoenix 308-Rocky PT, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
GLA3796-BS2 LA416796.D 1 11/09/22 KM n/a n/a GLA3796
GLA3796-BSD2 LA416798.D 1 11/09/22 KM n/a n/a GLA3796
The QC reported here applies to the following samples:Method: SW846 8015C
LA84954-2, LA84954-4, LA84954-8, LA84954-10
Spike BSP BSP BSD BSD Limits
CAS No.Compound mg/kg mg/kg %mg/kg %RPD Rec/RPD
TPH-GRO (C6-C10)50 47.6 95 48.0 96 1 79-112/15
CAS No.Surrogate Recoveries BSP BSD Limits
460-00-4 4-Bromofluorobenzene 90%88%64-128%
540-36-3 1,4-Difluorobenzene 103%102%80-122%
* = Outside of Control Limits.
86 of 90
LA8495466.2.3
Blank Spike/Blank Spike Duplicate Summary Page 1 of 1
Job Number:LA84954
Account:ATCNCR Atlas
Project:Phoenix 308-Rocky PT, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
GLA3797-BS2 LA416840.D 1 11/09/22 KM n/a n/a GLA3797
GLA3797-BSD2 LA416842.D 1 11/09/22 KM n/a n/a GLA3797
The QC reported here applies to the following samples:Method: SW846 8015C
LA84954-6, LA84954-12, LA84954-14
Spike BSP BSP BSD BSD Limits
CAS No.Compound mg/kg mg/kg %mg/kg %RPD Rec/RPD
TPH-GRO (C6-C10)50 52.3 105 52.7 105 1 79-112/15
CAS No.Surrogate Recoveries BSP BSD Limits
460-00-4 4-Bromofluorobenzene 89%88%64-128%
540-36-3 1,4-Difluorobenzene 105%105%80-122%
* = Outside of Control Limits.
87 of 90
LA8495466.2.4
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1
Job Number:LA84954
Account:ATCNCR Atlas
Project:Phoenix 308-Rocky PT, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
LA84954-14MS LA416822.D 1 11/09/22 KM n/a n/a GLA3796
LA84954-14MSD LA416824.D 1 11/09/22 KM n/a n/a GLA3796
LA84954-14 a LA416820.D 1 11/09/22 KM n/a n/a GLA3796
The QC reported here applies to the following samples:Method: SW846 8015C
LA84954-2, LA84954-4, LA84954-8, LA84954-10
LA84954-14 Spike MS MS Spike MSD MSD Limits
CAS No.Compound mg/kg Q mg/kg mg/kg %mg/kg mg/kg %RPD Rec/RPD
TPH-GRO (C6-C10)986 E 139 1320 240* b 139 1280 211* b 3 60-118/16
CAS No.Surrogate Recoveries MS MSD LA84954-14 Limits
460-00-4 4-Bromofluorobenzene 90%91%88%64-128%
540-36-3 1,4-Difluorobenzene 87%86%87%80-122%
(a) Sample used for QC purposes only.
(b) Outside control limits due to high level in sample relative to spike amount.
* = Outside of Control Limits.
88 of 90
LA8495466.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1
Job Number:LA84954
Account:ATCNCR Atlas
Project:Phoenix 308-Rocky PT, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
LA84954-14MS LA416864.D 1 11/09/22 KM n/a n/a GLA3797
LA84954-14MSD LA416866.D 1 11/09/22 KM n/a n/a GLA3797
LA84954-14 LA416862.D 1 11/09/22 KM n/a n/a GLA3797
The QC reported here applies to the following samples:Method: SW846 8015C
LA84954-6, LA84954-12, LA84954-14
LA84954-14 Spike MS MS Spike MSD MSD Limits
CAS No.Compound mg/kg Q mg/kg mg/kg %mg/kg mg/kg %RPD Rec/RPD
TPH-GRO (C6-C10)1440 1390 3030 114 1390 3130 121*3 60-118/16
CAS No.Surrogate Recoveries MS MSD LA84954-14 Limits
460-00-4 4-Bromofluorobenzene 99%98%98%64-128%
540-36-3 1,4-Difluorobenzene 98%97%96%80-122%
* = Outside of Control Limits.
89 of 90
LA8495466.3.2
Duplicate Summary Page 1 of 1
Job Number:LA84954
Account:ATCNCR Atlas
Project:Phoenix 308-Rocky PT, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA99585-4RRDUP LE039247.D 1 11/10/22 KM n/a n/a GLE2313
FA99585-4RR a LE039246.D 1 11/10/22 KM n/a n/a GLE2313
The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1
LA84954-3, LA84954-7
FA99585-4RRDUP
CAS No.Compound ug/kg Q ug/kg Q RPD Limits
C5- C8 Aliphatics (Unadj.)8450 I 7230 J 16 50
C9- C12 Aliphatics (Unadj.)186000 157000 17 50
C9- C10 Aromatics (Unadj.)72700 64600 12 50
CAS No.Surrogate Recoveries DUP FA99585-4RRLimits
615-59-8 2,5-Dibromotoluene 531%* b 617%* b 70-130%
615-59-8 2,5-Dibromotoluene 238%* b 264%* b 70-130%
(a) Sample received outside hold time.
(b) Outside control limits due to matrix interference. Confirmed by duplicate analysis.
* = Outside of Control Limits.
90 of 90
LA8495466.4.1