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Home My WebLink AboutWI-7488_32595_CA_MRP_20220615 3502 Hayes Road • Monroe, North Carolina 28110 113 West Firetower Road, Suite G • Winterville, North Carolina 28590 Phone (704) 845-4010 • (888) 870-4133 • Fax (704) 845-4012 June 15, 2022 Mr. Stephen Kay NCDEQ-UST Section Wilmington Regional Office 127 Cardinal Drive Extension Wilmington, NC 28405 Re: Ground Water Monitoring Report March 2022 Sam’s Pit Stop #64 4236 Sam Potts Highway Hallsboro, Columbus County North Carolina Incident Number: 32595 GRI Project Number: 2895 Dear Mr. Kay, Please find enclosed the referenced report for the above mentioned site. If you have any questions, please contact Rae Brown at 704-845-4010. Sincerely, Geological Resources, Inc. Leslie Maxtone-Graham Administrative Assistant Enclosure Cc: Mr. William S. Black; Sam’s Pit Stop, Inc., file 3502 Hayes Road • Monroe, North Carolina 28110 113 West Firetower Road, Suite G • Winterville, North Carolina 28590 Phone (704) 845-4010 • (888) 870-4133 • Fax (704) 845-4012 Ground Water Monitoring Report March 2022 Sam’s Pit Stop #64 4236 Sam Potts Highway Hallsboro, North Carolina Columbus County Facility ID Number. 00-0-0000035658 Incident Number. 32595 GRI Project Number.: 2895 Prepared for: Mr. William S. Black Sam’s Pit Stop, Inc. Post Office Box 689 Whiteville, North Carolina 28472 June 15, 2022 Rae Troiano Brown, P.G. Project Manager Sharon Lowther Report Writer ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: June 15, 2022 Sam’s Pit Stop Project Manager: Rae Troiano Brown, P.G. GRI Project No. 3077 i SITE INFORMATION 1. Site Identification  Sam’s Pit Stop (Facility ID 0-00-0000035658)  Incident Number 32595 – High 550 D (H550D)  Location of Source Area: 4236 Sam Potts Highway Hallsboro, North Carolina Columbus County 34.3219583°N, 78.5986083°W (Topographical Map) 2. Information about Contacts Associated with the Leaking UST System UST Owner Sam’s Pit Stop PO Box 689 Whiteville, NC 28472 wsblack12@yahoo.com 910-642-3188 UST Operator Sam’s Pit Stop PO Box 689 Whiteville, NC 28472 wsblack12@yahoo.com 910-642-3188 Property Owner Sams Pit Stop Properties LLC PO Box 689 Whiteville, NC 28472 wsblack12@yahoo.com 910-642-3188 Property Occupant Sam’s Pit Stop PO Box 689 Whiteville, NC 28472 wsblack12@yahoo.com 910-642-3188 Consultant/Contractor Geological Resources, Inc. 3502 Hayes Road Monroe, NC 28110 rtb@geologicalresourcesinc.com 704-845-4010 Analytical Laboratory SGS North America, Inc. 4405 Vineland Road, Suite C15 Orlando, Fl 32811 State Certification No. 573 407-425-6700 3. Information about Release  Release was discovered on October 23, 2009.  An unknown amount of product was released from the leaking UST System.  One 12,000-gallon gasoline, one 10,000-gallon gasoline USTs and associated pumps and product piping are active at the site. ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: June 15, 2022 Sam’s Pit Stop Project Manager: Rae Troiano Brown, P.G. GRI Project No. 3077 EXECUTIVE SUMMARY Sam’s Pit Stop is located at 4236 Sam Potts Highway in Hallsboro, Columbus County, North Carolina. One 10,000-gallon gasoline UST, one 12,000-gallon gasoline UST, associated pumps, and product piping are active at the site. Cracked spill buckets were observed during a compliance inspection and a release was confirmed during Site Check activities conducted in September 2009. A total of fourteen Type II monitoring wells (MW-1 through MW-14) and one Type III monitoring well (TW-1) have been installed at the site during previous ground water assessment activities. A Corrective Action Plan has not been requested by the North Carolina Department of Environmental Quality. According to the Limited Site Assessment Report (2010), 48 water supply wells were identified with 1,000 feet of the source area. In March and April 2022, an updated receptor survey was conducted. Municipal water is available to the site and surrounding areas. The water supply well at the subject site, WSW-1, has been abandoned and the site uses municipal water. Two water supply wells (WSW-2 and WSW-3) were identified within 250 feet of the source area. The owner confirmed WSW-2 is still in use; however, the well is located southeast of the site which is not in the down-gradient direction of ground water. No well survey response was obtained for WSW-3; however, the well is located north site in the upgradient direction of ground water flow. On March 29, 2022, six Type II monitoring wells (MW-1, MW-4, MW-7, MW-8, MW-9, and MW-13) were gauged, purged, and sampled. Concentrations of benzene that exceeded the Maximum Allowable Concentrations (MACs) were reported in the ground water samples collected from MW-1 and MW-9. None of the reported concentrations exceeded the gross contamination levels (GCLs). A fate and transport simulation was developed using ground water data collected in March 2019 to evaluate whether any receptors would be at risk if the plume were to migrate from the source area. Based on ground water flow direction and distances of MW-1 and MW-9 to the down-gradient property boundary, the fate and transport simulation indicated that the benzene plume will naturally attenuate to below the MAC before migrating off-site. Therefore, the site risk should be reduced to low because the benzene plume will not impact receptors. No additional assessment should be required after a Notice of Petroleum and public notice are completed. ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: June 15, 2022 Sam’s Pit Stop Project Manager: Rae Troiano Brown, P.G. GRI Project No. 3077 TABLE OF CONTENTS SITE INFORMATION ............................................................................................................................ i EXECUTIVE SUMMARY ....................................................................................................................... ii 1.0 SITE HISTORY AND CHARACTERIZATION ...................................................................................1 2.0 CURRENT ACTIVITIES ...............................................................................................................2 3.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION................................................2 4.0 FATE AND TRANSPORT MODEL ................................................................................................3 5.0 CONCLUSIONS .........................................................................................................................3 6.0 LIMITATIONS ...........................................................................................................................4 7.0 STATEMENTS AND CERTIFICATION ...........................................................................................5 FIGURES Figure 1: Site Location Map Figure 2: Site Vicinity Map Figure 3: Site Map Figure 4: Water Table Surface Map Figure 5: Ground Water Quality Map TABLES Table 1: Water Supply Well Information Table 2: Well Construction and Gauging Information Table 3: Ground Water Sample Analytical Results APPENDICES Appendix A: Well Surveys Appendix B: State Correspondence Appendix B: Laboratory Analytical Report – Ground Water Samples ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: June 15, 2022 Sam’s Pit Stop Project Manager: Rae Troiano Brown, P.G. GRI Project No. 3077 1.0 SITE HISTORY AND CHARACTERIZATION Sam’s Pit Stop #64 is an active convenience store and petroleum retail facility located at 4236 Sam Potts Highway in Hallsboro, Columbus County, North Carolina (Figures 1 and 2). One 10,000-gallon gasoline and one 12,000-gallon gasoline underground storage tanks (USTs) and associated pumps and product piping are active at the site. Cracked spill buckets were observed during a compliance inspection and a release was confirmed during Site Check activities conducted in September 2009. A Site Check, Phase II Limited Site Assessment, and Comprehensive Site Assessment were submitted by Geological Resources, Inc. (GRI). A Corrective Action Plan (CAP) has not been requested by the North Carolina Department of Environmental Quality (NCDEQ). The Registered Tank Report is shown below: The site and surrounding area is a mixture of single family residential and commercial properties. The site has one building and is primarily capped with concrete and asphalt. The overall topography at the site is relatively flat. No surface water bodies were identified within a 500-foot radius of the site. According to the Limited Site Assessment Report (2010), 78 water supply wells were identified with 1,500 feet of the source area. Of the 78 water supply wells identified, 48 potable water supply wells were identified within 1,000 feet of the source area. In March and April 2022, an updated receptor survey was conducted. Municipal water is available to the site and surrounding areas. According to John Hooks of the NCDEQ, the water tower located up-gradient of the site at 4136 Sam Potts Highway is a holding tank and does not pump ground water at this location. Well surveys were mailed to the owners of water supply wells (WSW-1 through WSW-19) located nearest to the site. The water supply well at the subject site, WSW-1, has been abandoned and the site uses municipal water. Two water supply wells (WSW-2 and WSW-3) were identified within 250 feet of the ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: June 15, 2022 Sam’s Pit Stop Project Manager: Rae Troiano Brown, P.G. GRI Project No. 3077 source area. The owner of WSW-2 confirmed it is still in use; however, the well is located southeast of the site which is not in the down-gradient direction of ground water. No well survey response was obtained for WSW-3; however, the well is located north of the site in the upgradient direction of ground water flow. Supply wells WSW-2, WSW-4, WSW-10, WSW-13, and WSW-15 were confirmed by survey responses to be potable. At the submission of this report, no other responses have been received. A summary of supply well information is included in Table 1. A Site Vicinity Map is included as Figure 2. Copies of survey responses and current property owner cards are included in Appendix A. A total of fourteen Type II monitoring wells (MW-1 through MW-14) and one Type III monitoring well (TW- 1) have been installed at the site during previous ground water assessment activities. Well construction information is included in Table 2. A Site Map showing the locations of the monitoring wells and the structures on-site has been included as Figure 3. A fate and transport simulation was developed using ground water data collected in March 2019 to evaluate whether any receptors would be at risk if the plume were to migrate from the source area. The results of the fate and transport simulation indicated that the contaminant plume will naturally attenuate to below the Maximum Allowable Concentration (MAC) for benzene and will not reach the distance of the downgradient property line. 2.0 CURRENT ACTIVITIES The purpose of this report is to obtain updated receptor survey information and present the results of the ground water sampling activities conducted in March 2022 at the Sam’s Pit Stop #64 site. The activities were conducted in accordance with GRI Proposal No. 22-099, which was approved as Task Authorization No. 32595-18 on March 7, 2022. The purpose of these activities was to obtain current ground water quality data for the site to confirm the fate and transport model. A copy of NCDEQ correspondence has been included in Appendix B. 3.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION On March 29, 2022, six monitoring wells (MW-1, MW-4, MW-7, MW-8, MW-10, and MW-13) were gauged, purged, and sampled. During the March 2021 sampling event, depths to ground water in the Type II monitoring wells ranged from 2.33 to 5.88 feet below the tops of well casings. The average depth to water was 4.89 feet. Ground water elevations in the Type II monitoring wells relative to a temporary benchmark with an assumed datum of 100.00 feet ranged from 94.19 to 96.62 feet. During the March 2022 sampling event, ground water flow on-site was toward the east, which is consistent with historical data. A Site Map showing the locations of the monitoring wells and the structures on-site and on surrounding properties has been included as Figure 3. A Water Table Surface Map for the March 29, 2022 sampling event has been included as Figure 4. A summary of well construction information including ground water elevation data is presented in Table 2. Concentrations of benzene that exceeded the MACs specified in T15A NCAC 2L.0202 were reported in the ground water samples collected from MW-1 and MW-9. None of the reported concentrations exceeded the gross contamination levels (GCLs). A Ground Water Quality Map based on data from the March 2022 ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: June 15, 2022 Sam’s Pit Stop Project Manager: Rae Troiano Brown, P.G. GRI Project No. 3077 sampling event has been included as Figure 5. A summary of ground water sample analytical results is presented in Table 3. A complete laboratory analytical report has been included in Appendix C. 4.0 FATE AND TRANSPORT MODEL A fate and transport simulation based on ground water data collected in 2019 was performed to determine the feasibility of site remediation by natural attenuation. In 2019, benzene exceeded the MAC in the source area monitoring well. Therefore, after the model was calibrated for site conditions, simulations were run to determine the fate and transport of benzene. The results of the fate and transport simulation indicated that the benzene plume will naturally attenuate to below the MAC and will not reach the distance of the downgradient property line. Please refer to the Ground Water Monitoring and Fate and Transport Model Report (March 2019) for additional information. The benzene concentrations reported in MW-1 in 2019, 2021, and 2022 were 276 g/L, <0.13 g/L, and 54.7 g/L, respectively. The overall reduction trend seems to confirm natural attenuation simulation. Please note, MW-9 is located cross-gradient of the dispensers and product piping, along the northern property boundary adjacent to Sam Potts Highway. The concentration of benzene in MW-9 (104 g/L) in 2022 exceeds the MAC. Compare this to monitoring well MW-2 which is down-gradient of the dispensers and has no detectable contaminant concentrations. This suggests that concentrations reported in MW-9 may be reflective of surface water run-off from Sam Potts Highway. Ground water flow has been consistently documented toward the east; and the property boundary is approximately 275’ down- gradient of MW-9 which according to the fate and transport simulation will allow benzene to attenuate below the MAC before migrating off-site. 5.0 CONCLUSIONS  In March and April 2022, an updated receptor survey was conducted. Municipal water is available to the surrounding area. The on-site supply well has been abandoned and the site uses municipal water.  Ground water flow during the March 2022 sampling event was generally toward the east which is consistent with historical data. The average depth to ground water in the Type II monitoring wells was 4.89 feet.  The benzene concentrations reported in MW-1 in 2019, 2021, and 2022 were 276 g/L, <0.13 g/L, and 54.7 g/L, respectively. The overall reduction trend seems to confirm natural attenuation projected by the 2019 fate and transport simulation.  Concentrations of benzene that exceeded the MACs in MW-9 appear to be reflective of impact from Sam Potts Highway rather than the UST system. No ground water violations have been reported since 2016 in wells MW-4, MW-8, or MW-13 which are down-gradient of the MW-9 and the UST system. Based on ground water flow direction and distance of MW-9 to the down- gradient property boundary, the fate and transport simulation indicated that the benzene plume will naturally attenuate to below the MAC before migrating off-site. ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: June 15, 2022 Sam’s Pit Stop Project Manager: Rae Troiano Brown, P.G. GRI Project No. 3077  The March 2022 sampling event was conducted to confirm the results of the model which has been done. Therefore, the site risk should be reduced to low because the benzene plume will not impact receptors. No additional assessment should be required after a Notice of Petroleum and public notice are completed. 6.0 LIMITATIONS This report has been prepared for the exclusive use of Sam’s Pit Stop, Inc for specific application to the referenced site in Columbus County, North Carolina. The assessment was conducted based on the scope of work and level of effort desired by the NCDEQ and with resources adequate only for that scope of work. Our findings have been developed in accordance with generally accepted standards of environmental practices in the State of North Carolina, available information, and our professional judgment. No other warranty is expressed or implied. The data that are presented in this report are indicative of conditions that existed at the precise locations sampled and at the time the samples were collected. In addition, the data obtained from samples would be interpreted as being meaningful with respect to parameters indicated in the laboratory report. No additional information can logically be inferred from these data. ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: June 15, 2022 Sam’s Pit Stop Project Manager: Rae Troiano Brown, P.G. GRI Project No. 3077 7.0 STATEMENTS AND CERTIFICATION 1 Enter the date the monitoring report was due. n/a Will this report be submitted after the established due date? YES NO 2 Was any required information from the above template missing from this report? YES NO IF the answer to question #1 or# 2 is “YES”, please provide additional information in this cell to explain what was missing and why. 3 If applicable, will any of the proposed attenuation milestones under the schedule approved in the Corrective Action Plan not be met? (within a reasonable margin of error) YES NO IF the answer to question #3 is “NO”, skip to the certification under #8 below. IF the answer to question #3 is “YES”, please generally describe in this cell the possible reason(s) and outline proposed remedies. (This should be described in more detail in the report text above.) N/A 4 Does any known or suspected source zone soil contamination or free product remain outside of the assessed area that could be inhibiting natural attenuation? YES NO 5 Has there been an unexpected increase in contaminant mass sufficient to suggest a potential new release from a separate onsite or offsite source? YES NO IF the answer to either question #4 or #5 is “YES”, generally describe in this cell any actions recommended to further assess or clean up this known or suspected source. (This should be described in more detail in the report text above.) 6 Certification: I, Rae Troiano Brown, a Licensed Geologist for Geological Resources, Inc., do certify that the information contained in this report is correct and accurate to the best of my knowledge. Geological Resources, Inc. is licensed to practice engineering and geology in North Carolina. The certification number of the company or corporation is C-2727/C-127. FIGURES "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J"J"J "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J"J "J "J "J"J "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J SITE SAM POTTS HWYFOX DRHALLSBORO RDBUSSY RD WYCHE RD GILES BYRD RD SCHOOL RDRED BUG RDCEDAR STBARDY HIGH RDOAK STWYCHE WYCHE MEWS MACIE KING RDCOWPEN BRANCHWSW-2 WSW-9 WSW-8 WSW-7 WSW-6WSW-5WSW-4 WSW-3 WSW-1 WSW-78 WSW-77 WSW-76 WSW-75 WSW-74 WSW-73WSW-72 WSW-71 WSW-70 WSW-69 WSW-68WSW-67WSW-66WSW-65 WSW-63 WSW-62 WSW-61 WSW-60 WSW-59 WSW-58 WSW-57 WSW-56 WSW-55 WSW-54 WSW-53 WSW-52 WSW-51 WSW-50 WSW-49 WSW-48 WSW-47 WSW-46 WSW-45 WSW-44 WSW-43 WSW-42 WSW-41 WSW-40 WSW-39 WSW-38 WSW-37 WSW-36 WSW-35 WSW-33 WSW-32 WSW-31 WSW-30 WSW-29WSW-28 WSW-27 WSW-26 WSW-25 WSW-24 WSW-23 WSW-22 WSW-21 WSW-20 WSW-19 WSW-18 WSW-17 WSW-16 WSW-14 WSW-13 WSW-12 WSW-11 WSW-10 20512 85448 75855 19517 9334920520 18571 20528 19809 18909 19380 88934 87318 19581 19867 19597 18642 86207 86685 19793 19018 2039887728 20409 19579 62077 19263 20269 18694 90428 19774 19481 19267 19363 20231 19306 19580 19810 62082 18532 18535 19680 1936820060620831925319752 20513 2014220282 20232203952004719281 19762 90408184771889820387 19355 18888 19176 20110 18907 18725 19608 92043 88935 19367 20397 2037818900 19590 18497 18890 18904 18899 18695 18987 19692 19536 19913 18902 18903 19175WSW-64 WSW-34 WSW-15 18510 FIGURE 2: SITE VICINITY MAPSAM'S PIT STOP #644236 SAM POTTS HIGHWAYHALLSBORO, COLUMBUS COUNTYNORTH CAROLINAINCIDENT NO. 32595 , INC. ³ 0 300150Feet 1 inch = 300 feet 1,500-FOOT RADIUS 1,000-FOOT RADIUS 250-FOOT RADIUS LEGEND Water Supply Well parcels Wet Weather Creek 88934 Property ID Number PREPARED BY:GEOLOGICAL RESOURCES APRIL 28, 2022 ncrivers centerlines "J Well Destroyed Water Supply Well Water Tower x 8 n l l TABLES Well # and/or Tax Number Well Owner Address Phone Number Well Use Municipal Water? Well Depth (ft BGS) Type of Well (Drilled/ Bored) Well Casing Depth (ft. BGS) Well Screen Interval (x to y ft. BGS) Approximate Distance from Source Area of Release (ft.) 88934 (WSW-1) Sam's Pit Stop Properties, LLC Post Office Box 689 Whiteville, NC 28472 910-642-3188 Abandoned Connected --- --- --- --- ~80' SE 20395 (WSW-2)Lugene T. Ward 153 Rockway Dr. Lexington, NC 27295 336-695-4847 Potable Available Unknown Unknown Unknown Unknown ~200' S 19793 (WSW-3) Pierce & Co. General Store LLC Post Office Box 246 Hallsboro, NC 28442 910-646-4158 Potable Available 216' Unknown 100' Unknown ~175' N 18903 (WSW-4)Kenneth R Todd 185 Lakeland Cir. Hallsboro, NC 28442 910-642-7280 Potable Available Unknown Unknown Unknown Unknown ~260' NE 19692 (WSW-5)Patricia Mitchell 744 Bella Coola Road Lake Waccamaw, NC 28450 910-646-4389 Unknown Available Unknown Unknown Unknown Unknown ~450' NE 19608 (WSW-6)Rodney Wilson 4339 Sam Potts Hwy Hallsboro, NC 28442 910-646-9915 Unknown Available Unknown Unknown Unknown Unknown ~550' NE 19809 (WSW-7)Bernard Gregory 4330 Sam Potts Hwy Hallsboro, NC 28442 Unknown Unknown Available Unknown Unknown Unknown Unknown ~400' ESE 20142 (WSW-8)Micheal & Betty Duncan 103-A Paradise Cir. Havelock, NC 28532 910-646-3259 Unknown Available Unknown Unknown Unknown Unknown ~350' SE 20387 (WSW-9) Marilyn Boring & Kenneth E. Ward 153 Rockway Drive Lexington, NC 27295 Unknown Unknown Available Unknown Unknown Unknown Unknown ~275' S 19281 (WSW-10)Peggy Blanchard 1833 Waccamaw Shores Rd. Lake Waccamaw, NC 28450 910-840-3374 Potable No Unknown Unknown Unknown Unknown ~300' S 62077 (WSW-11) Hallsoboro Volunteer Fire Department Post Office Box 8 Hallsboro, NC 28442 910-646-3104 Unknown Available Unknown Unknown Unknown Unknown ~300' W 18907 (WSW-12)Reinaldo V. Argueta 1104 Kingswood Rd. Conway, SC 29526 Unknown Unknown Available Unknown Unknown Unknown Unknown ~450' NW 18900 (WSW-13)Cam-Brent Inc.1941 Giles Byrd Road Hallsboro, NC 28442 910-840-6693 Potable Available Unknown Unknown Unknown Unknown ~400' NW 18535 (WSW-14)Mrs. Clarkie Barnhardt 1715 Old Stage Road Delco, NC 28436 Unknown Unknown Available Unknown Unknown Unknown Unknown ~450' N 18904 (WSW-15)Kenneth R Todd 185 Lakeland Cir. Hallsboro, NC 28442 910-642-7280 Potable Available Unknown Unknown Unknown Unknown ~300' N 18497 (WSW-16)Nellie T. Imm 37 Oak St. Hallsboro, NC 28442 Unknown Unknown Available Unknown Unknown Unknown Unknown ~350' N 19536 (WSW-17)Evon Ward Boren 81 Parker Road Whiteville, NC 28472 910-642-4156 Irrigation Connected Unknown Unknown Unknown Unknown ~475' SE TABLE 1 WATER SUPPLY WELL INFORMATION SAM'S PIT STOP #64 (INCIDENT NO. 32595) Date: 04/08/22 Facility ID # : 00-0-0000035658 Well # and/or Tax Number Well Owner Address Phone Number Well Use Municipal Water? Well Depth (ft BGS) Type of Well (Drilled/ Bored) Well Casing Depth (ft. BGS) Well Screen Interval (x to y ft. BGS) Approximate Distance from Source Area of Release (ft.) TABLE 1 WATER SUPPLY WELL INFORMATION SAM'S PIT STOP #64 (INCIDENT NO. 32595) Date: 04/08/22 Facility ID # : 00-0-0000035658 19913 (WSW-18)Micheal & Betty Duncan 103-A Paradise Cir. Havelock, NC 28532 910-646-3259 Unknown Available Unknown Unknown Unknown Unknown ~475' S 18510 (WSW-19) Ceasar & Isadora Lambright Trust 12 Lambright Circle Columbia, SC 29203 Unknown Unknown Available Unknown Unknown Unknown Unknown ~500' S 18695 (WSW-20)Fredrikia Britt Post Office Box 154 Hallsboro, NC 28442 Unknown Potable Available Unknown Unknown Unknown Unknown ~775' N 18694 (WSW-21)Fredrikia Britt Post Office Box 154 Hallsboro, NC 28442 Unknown Potable Available Unknown Unknown Unknown Unknown ~600' N 19762 (WSW-22)Eddie & Betty Morgan 131 Bardy High Road Hallsboro, NC 28442 Unknown Potable Available Unknown Unknown Unknown Unknown ~900' NE 19306 (WSW-23)Rodney Wilson 105 Bardy High Road Hallsboro, NC 28442 910-646-9915 Potable Available Unknown Unknown Unknown Unknown ~825' NE 19774 (WSW-24)Christopher Canady 83 Bardy High Road Hallsboro, NC 28442 Unknown Potable Available Unknown Unknown Unknown Unknown ~725' NE 20110 (WSW-25)Allen Shipman 326 Schley St. #1-R Newark, NJ 07112 Unknown Potable Available Unknown Unknown Unknown Unknown ~600' NE 19590 (WSW-26)Ray Long 5371 Red Hill Road Whiteville, NC 28472 Unknown Potable Available Unknown Unknown Unknown Unknown ~950' NE 19363 (WSW-27)Kenneth Lindahl 72 Bardy High Road Hallsboro, NC 28442 Unknown Potable Available Unknown Unknown Unknown Unknown ~800' NE 19597 (WSW-28)William Long 251 E Floral Avenue Arcadia, CA 91006 Unknown Potable Available Unknown Unknown Unknown Unknown ~625' NE 20378 (WSW-29)Jesee Long 251 E Floral Avenue Arcadia, CA 91006 Unknown Potable Available Unknown Unknown Unknown Unknown ~750' NE 19176 (WSW-30)Billy & Mary Gilliland 3510 Chalmers Drive Wilmington, NC 28409 Unknown Potable Available Unknown Unknown Unknown Unknown ~800' NE 18888 (WSW-31)Rebecca Boswell 195 Wyche Road Hallsboro, NC 28442 Unknown Potable Available Unknown Unknown Unknown Unknown ~950' NE 20398 (WSW-32)Lila Ruth Ward 102 Furnie Hinson Road Whiteville, NC 28472 910-642-3114 Potable Available Unknown Unknown Unknown Unknown ~650' ESE 20397 (WSW-33)Lila Ruth Ward 102 Furnie Hinson Road Whiteville, NC 28472 910-642-3114 Potable Available Unknown Unknown Unknown Unknown ~750' SE 18987 (WSW-34)Charles Wakild 10-A West Columbia St. Wrightsville Beach, NC 28480 910-509-2826 Potable Available Unknown Unknown Unknown Unknown ~800' ESE 90408 (WSW-35)Charles Wakild 10-A West Columbia St. Wrightsville Beach, NC 28480 910-509-2826 Potable Available Unknown Unknown Unknown Unknown ~900' ESE Well # and/or Tax Number Well Owner Address Phone Number Well Use Municipal Water? Well Depth (ft BGS) Type of Well (Drilled/ Bored) Well Casing Depth (ft. BGS) Well Screen Interval (x to y ft. BGS) Approximate Distance from Source Area of Release (ft.) TABLE 1 WATER SUPPLY WELL INFORMATION SAM'S PIT STOP #64 (INCIDENT NO. 32595) Date: 04/08/22 Facility ID # : 00-0-0000035658 90428 (WSW-36)Jerry Holland 7129 Dennis Road Walnut Cove, NC 27052 Unknown Potable Available Unknown Unknown Unknown Unknown ~950' NE 87728 (WSW-37)Frances Batten Heirs 144 Bussey Road Hallsboro, NC 28442 Unknown Potable Available Unknown Unknown Unknown Unknown ~975' SE 19752 (WSW-38)Charles Norris 144 Bussey Road Hallsboro, NC 28442 Unknown Potable Available Unknown Unknown Unknown Unknown ~800' SE 85448 (WSW-39)Charles Norris 144 Bussey Road Hallsboro, NC 28442 Unknown Potable Available Unknown Unknown Unknown Unknown ~700' SE 18725 (WSW-40)Marie Buchanan 76 Bussey Road Hallsboro, NC 28442 910-646-3952 Potable Available Unknown Unknown Unknown Unknown ~500' SE 19018 (WSW-41)Michael and Betty Duncan 103 A Paradise Circle Havelock, NC 28532 Unknown Potable Available Unknown Unknown Unknown Unknown ~700' SE 86207 (WSW-42)Frank Sotomayer 87 Giles Road Hallsboro, NC 28442 Unknown Potable Available Unknown Unknown Unknown Unknown ~900' S 20282 (WSW-43)Francella Thurman (etal)Post Office Box 352 Hallsboro, NC 28442 Unknown Potable Available Unknown Unknown Unknown Unknown ~800' S 19680 (WSW-44) Artesia Alumni Association Inc. 221 McKoy Road Hallsboro, NC 28442 Unknown Potable Available Unknown Unknown Unknown Unknown ~800' S 20513 (WSW-45)Jennie Thompson 810 Hallsboro Road Hallsboro, NC 28442 Unknown Potable Available Unknown Unknown Unknown Unknown ~750' SE 19867 (WSW-46)Trudy Pope 875 Dismal Road Hallsboro, NC 27442 Unknown Potable Available Unknown Unknown Unknown Unknown ~950' S 18477 (WSW-47)Van and Betty Ward Post Office Box 241 Whiteville, NC 28472 Unknown Potable Available Unknown Unknown Unknown Unknown ~900' S 20528 (WSW-48)Ray & Melba Wyche Post Office Box 183 Hallsboro, NC 28442 910-646-3704 Potable Available Unknown Unknown Unknown Unknown ~800' N 62083 (WSW-49) Hallsboro Baptist Pastorum 514 Hallsboro Road South Hallsboro, NC 28442 910-646-3283 Potable Available Unknown Unknown Unknown Unknown ~1,100' N 20409 (WSW-50)Jane Ward Post Office Box 42 Hallsboro, NC 28442 Unknown Potable Available Unknown Unknown Unknown Unknown ~1,250' N 19517 (WSW-51)Darrell Thompson 464 Hallsboro Road S Hallsboro, NC 28442 910-646-4766 Potable Available Unknown Unknown Unknown Unknown ~1,400' N 20269 (WSW-52)William Thompson Post Office Box 39 Hallsboro, NC 28442 Unknown Potable Available Unknown Unknown Unknown Unknown ~1,100' N 19263 (WSW-53) Secretary of Housing & Urban Development 40 Marietta Street Atlanta, GA 30303 Unknown Potable Available Unknown Unknown Unknown Unknown ~1,250' N Well # and/or Tax Number Well Owner Address Phone Number Well Use Municipal Water? Well Depth (ft BGS) Type of Well (Drilled/ Bored) Well Casing Depth (ft. BGS) Well Screen Interval (x to y ft. BGS) Approximate Distance from Source Area of Release (ft.) TABLE 1 WATER SUPPLY WELL INFORMATION SAM'S PIT STOP #64 (INCIDENT NO. 32595) Date: 04/08/22 Facility ID # : 00-0-0000035658 18642 (WSW-54)William Blackman Heirs Post Office Box 126 Hallsboro, NC 28442 Unknown Potable Available Unknown Unknown Unknown Unknown ~1,400' N 75855 (WSW-55)Joseph McGuire 1511 Hemphill Drive Raleigh, NC 27609 919-790-9365 Potable Available Unknown Unknown Unknown Unknown ~1,150' NE 19380 (WSW-56)Karen Reagan 24 Cedar Street Hallsboro, NC 27442 910-646-1335 Potable Available Unknown Unknown Unknown Unknown ~1,100' NE 20520 (WSW-57)Paul Wyche Post Office Box 246 Hallsboro, NC 28442 Unknown Potable Available Unknown Unknown Unknown Unknown ~1,300' NE 93349 (WSW-58)Pauline Council Post Office Box 156 Hallsboro, NC 28442 Unknown Potable Available Unknown Unknown Unknown Unknown ~1,400' NE 19355 (WSW-59)Ethelene Hewett 130 Bardy High Road Hallsboro, NC 27442 Unknown Potable Available Unknown Unknown Unknown Unknown ~1,100' NE 18890 (WSW-60)Melody Bordeaux 193 Wyche Street Hallsboro, NC 28442 Unknown Potable Available Unknown Unknown Unknown Unknown ~1,100' NE 19481 (WSW-61)Joe Dale Jackson 3532 Old Wilmington Road Hallsboro, NC 28442 910-646-4145 Potable Available Unknown Unknown Unknown Unknown ~1,250' NE 20060 (WSW-62)Allison Greene 124 Wyche Street Hallsboro, NC 28442 910-646-6458 Potable Available Unknown Unknown Unknown Unknown ~1,450' NE 62082 (WSW-63) Hallsboro Methodist Church Parsonage 553 Honey Hill Road Hallsboro, NC 28442 910-646-4105 Potable Available Unknown Unknown Unknown Unknown ~1,400' NE 19175 (WSW-64)Billy & Mary Gilliland 3510 Chalmers Drive Wilmington, NC 28409 Unknown Potable Available Unknown Unknown Unknown Unknown ~1,000' E 19253 (WSW-65)William McNair 4451 Sam Potts Highway Hallsboro, NC 27442 Unknown Potable Available Unknown Unknown Unknown Unknown ~1,100' E 19580 (WSW-66)Charles Long 114 Marshfield Drive Wilmington, NC 28411 Unknown Potable Available Unknown Unknown Unknown Unknown ~1,200' E 19579 (WSW-67) Kimberly Small and Randall James 4491 Sam Potts Highway Hallsboro, NC 28442 Unknown Potable Available Unknown Unknown Unknown Unknown ~1,300' E 19581 (WSW-68)Charles & Vendall Long 4469 Sam Potts Highway Hallsboro, NC 28442 910-646-3030 Potable Available Unknown Unknown Unknown Unknown ~1,400' E 18571 (WSW-69)Jesse & John Fisher 107 Powell Building Whiteville, NC 27472 910-642-4958 Potable Available Unknown Unknown Unknown Unknown ~1,450' E 20231 (WSW-70)Barbara Young Post Office Box 214 Lake Waccamaw, NC 28450 Unknown Potable Available Unknown Unknown Unknown Unknown ~1,450' E Well # and/or Tax Number Well Owner Address Phone Number Well Use Municipal Water? Well Depth (ft BGS) Type of Well (Drilled/ Bored) Well Casing Depth (ft. BGS) Well Screen Interval (x to y ft. BGS) Approximate Distance from Source Area of Release (ft.) TABLE 1 WATER SUPPLY WELL INFORMATION SAM'S PIT STOP #64 (INCIDENT NO. 32595) Date: 04/08/22 Facility ID # : 00-0-0000035658 20047 (WSW-71)Joseph Clemmons 1468 Dupree Landing Road Hallsboro, NC 28442 910-646-3269 Potable Available Unknown Unknown Unknown Unknown ~1,100' SE 20095 (WSW-72)Joseph Clemmons 1468 Dupree Landing Road Hallsboro, NC 28442 910-646-3269 Potable Available Unknown Unknown Unknown Unknown ~1,200' SE 20232 (WSW-73)James and Nancy Miller 264 Lewis Burchette Road Whiteville, NC 27472 910-642-0612 Potable Available Unknown Unknown Unknown Unknown ~1,250' SE 19368 (WSW-74)Jefferson Davis Hill Post Office Box 158 Hallsboro, NC 28442 910-646-4723 Potable Available Unknown Unknown Unknown Unknown ~1,450' SE 19367 (WSW-75)Jefferson Davis Hill Post Office Box 158 Hallsboro, NC 28442 910-646-4723 Potable Available Unknown Unknown Unknown Unknown ~1,450' SE 86685 (WSW-76)Barry Lee Andrews 184 School Road Hallsboro, NC 28442 Unknown Potable Available Unknown Unknown Unknown Unknown ~1,200' SE 87318 (WSW-77)Joe Tyler 221 Giles Byrd Road Hallsboro, NC 28442 910-646-3891 Potable Available Unknown Unknown Unknown Unknown ~1,350' SE 20512 (WSW-78)Jamie and Jaimee Welch 55 Wyche Mew S Hallsboro, NC 28442 Unknown Potable Available Unknown Unknown Unknown Unknown ~1,300' NW Notes: • Water supply wells are keyed to Figure 2. • Ft. BGS : Feet below ground surface • Information for entries in bold was obtained from well survey responses recevied in 2022. 01/26/10 4.68 --- 95.57 02/11/10 NM --- NM 11/10/10 9.21 --- 91.04 01/17/11 7.34 --- 92.91 07/14/11 9.93 --- 90.32 01/10/12 7.46 --- 92.79 05/31/12 7.20 --- 93.05 11/07/12 8.17 --- 92.08 06/05/13 6.79 --- 93.46 04/22/14 4.39 --- 95.86 08/25/14 6.10 --- 94.15 Before MMPE 08/29/14 10.00 --- 90.25 After MMPE 09/29/14 5.13 --- 95.12 03/16/15 4.43 --- 95.82 01/19/16 4.67 --- 95.58 06/07/16 4.67 --- 95.58 11/10/16 7.30 --- 92.95 05/09/17 6.14 --- 94.11 11/13/17 6.68 --- 93.57 05/10/18 5.95 --- 94.30 03/18/19 5.09 --- 95.16 03/09/21 4.77 --- 95.48 03/29/22 5.88 --- 94.37 02/11/10 2.40 --- 98.37 11/10/10 3.22 --- 97.55 01/17/11 2.78 --- 97.99 07/14/11 3.15 --- 97.62 01/10/12 3.21 --- 97.56 05/31/12 2.28 --- 98.49 11/07/12 2.94 --- 97.83 04/22/14 2.12 --- 98.65 09/29/14 1.91 --- 98.86 03/16/15 2.11 --- 98.66 01/19/16 2.35 --- 98.42 06/07/16 1.67 --- 99.10 11/10/16 3.00 --- 97.77 05/09/17 2.42 --- 98.35 11/13/17 2.64 --- 98.13 05/10/18 2.29 --- 98.48 03/18/19 2.15 --- 98.62 03/09/21 2.28 --- 98.49 02/11/10 5.87 --- 94.20 11/10/10 9.00 --- 91.07 01/17/11 7.61 --- 92.46 07/14/11 9.83 --- 90.24 01/10/12 7.39 --- 92.68 05/31/12 6.97 --- 93.10 11/07/12 7.83 --- 92.24 06/05/13 6.60 --- 93.47 04/22/14 4.32 --- 95.75 09/29/14 5.13 --- 94.94 01/19/16 4.58 --- 95.49 06/07/16 4.48 --- 95.59 11/10/16 7.35 --- 92.72 05/09/17 5.93 --- 94.14 11/13/17 5.91 --- 94.16 05/10/18 6.02 --- 94.05 03/18/19 5.17 --- 94.90 03/09/21 5.02 --- 95.05 100.25122 - 12201/26/10MW-1 100.77122 - 12202/11/10MW-2 100.07122 - 12202/11/10MW-3 Comments TABLE 2 WELL CONSTRUCTION AND GAUGING INFORMATION Date: 04/08/22 Facility ID #: 00-0-0000035658 Well ID Date Installed (mm/dd/yy) Date Water Level Measured (mm/dd/yy) Well Casing Depth (ft. BGS) Screened Interval (x to y ft. BGS) Bottom of Well (ft. BGS) Top of Casing Elevation* (ft.) Depth to Water from Top of Casing (ft.) Free Product Thickness (ft.) Ground Water Elevation* (ft.) SAM'S PIT STOP Page 1 of 5 Comments TABLE 2 WELL CONSTRUCTION AND GAUGING INFORMATION Date: 04/08/22 Facility ID #: 00-0-0000035658 Well ID Date Installed (mm/dd/yy) Date Water Level Measured (mm/dd/yy) Well Casing Depth (ft. BGS) Screened Interval (x to y ft. BGS) Bottom of Well (ft. BGS) Top of Casing Elevation* (ft.) Depth to Water from Top of Casing (ft.) Free Product Thickness (ft.) Ground Water Elevation* (ft.) SAM'S PIT STOP 02/11/10 4.68 --- 95.50 11/10/10 9.15 --- 91.03 01/17/11 7.33 --- 92.85 07/14/11 9.87 --- 90.31 01/10/12 7.43 --- 92.75 05/31/12 7.00 --- 93.18 11/07/12 7.92 --- 92.26 06/05/13 6.71 --- 93.47 04/22/14 4.39 --- 95.79 09/29/14 5.18 --- 95.00 03/16/15 4.42 --- 95.76 01/19/16 4.63 --- 95.55 06/07/16 4.48 --- 95.70 11/10/16 7.65 --- 92.53 05/09/17 6.07 --- 94.11 11/13/17 6.62 --- 93.56 05/10/18 5.95 --- 94.23 03/18/19 5.12 --- 95.06 03/09/21 5.00 --- 95.18 03/29/22 5.85 --- 94.33 11/10/10 3.08 --- 97.34 01/17/11 1.82 --- 98.60 07/14/11 3.32 --- 97.10 01/10/12 2.67 --- 97.75 05/31/12 2.02 --- 98.40 11/07/12 3.20 --- 97.22 06/05/13 2.00 --- 98.42 04/22/14 1.21 --- 99.21 09/29/14 1.61 --- 98.81 01/19/16 1.99 --- 98.43 06/07/16 0.90 --- 99.52 11/10/16 3.31 --- 97.11 05/09/17 1.97 --- 98.45 11/13/17 1.91 --- 98.51 Destroyed 11/10/10 8.86 --- 91.01 01/17/11 6.74 --- 93.13 07/14/11 9.66 --- 90.21 01/10/12 7.28 --- 92.59 05/31/12 6.80 --- 93.07 11/07/12 7.74 --- 92.13 06/05/13 6.50 --- 93.37 04/22/14 4.21 --- 95.66 09/29/14 4.99 --- 94.88 03/16/15 4.24 --- 95.63 01/19/16 4.20 --- 95.67 06/07/16 5.61 --- 94.26 11/10/16 6.97 --- 92.90 05/09/17 5.61 --- 94.26 100.18122 - 12202/11/10MW-4 99.87122 - 12211/05/10MW-6 100.42122 - 12211/05/10MW-5 Page 2 of 5 Comments TABLE 2 WELL CONSTRUCTION AND GAUGING INFORMATION Date: 04/08/22 Facility ID #: 00-0-0000035658 Well ID Date Installed (mm/dd/yy) Date Water Level Measured (mm/dd/yy) Well Casing Depth (ft. BGS) Screened Interval (x to y ft. BGS) Bottom of Well (ft. BGS) Top of Casing Elevation* (ft.) Depth to Water from Top of Casing (ft.) Free Product Thickness (ft.) Ground Water Elevation* (ft.) SAM'S PIT STOP 11/10/10 7.02 --- 91.93 01/17/11 3.53 --- 95.42 07/14/11 8.64 --- 90.31 01/10/12 5.97 --- 92.98 05/31/12 2.06 --- 96.89 11/07/12 6.54 --- 92.41 06/05/13 2.59 --- 96.36 04/22/14 1.69 --- 97.26 09/29/14 3.08 --- 95.87 06/07/16 1.23 --- 97.72 11/10/16 5.88 --- 93.07 05/09/17 4.34 --- 94.61 11/13/17 2.62 --- 96.33 05/10/18 4.41 --- 94.54 03/18/19 2.15 --- 96.80 03/09/21 2.02 --- 96.93 03/29/22 2.33 --- 96.62 11/10/10 8.53 --- 91.02 01/17/11 6.70 --- 92.85 07/14/11 9.27 --- 90.28 01/10/12 6.82 --- 92.73 05/31/12 6.34 --- 93.21 11/07/12 7.34 --- 92.21 04/22/14 3.73 --- 95.82 09/29/14 4.60 --- 94.95 06/07/16 3.87 --- 95.68 11/10/16 6.70 --- 92.85 05/09/17 5.27 --- 94.28 11/13/17 5.24 --- 94.31 05/10/18 5.30 --- 94.25 03/18/19 4.53 --- 95.02 03/09/21 4.40 --- 95.15 03/29/22 5.26 --- 94.29 11/10/10 6.06 --- 94.33 01/17/11 5.48 --- 94.91 07/14/11 8.40 --- 91.99 01/10/12 6.95 --- 93.44 05/31/12 6.28 --- 94.11 11/07/12 7.31 --- 93.08 04/22/14 4.41 --- 95.98 09/29/14 5.04 --- 95.35 03/16/15 4.44 --- 95.95 01/19/16 4.68 --- 95.71 06/07/16 4.53 --- 95.86 11/10/16 7.30 --- 93.09 05/09/17 5.84 --- 94.55 11/13/17 6.17 --- 94.22 05/10/18 6.96 --- 93.43 03/18/19 5.09 --- 95.30 03/09/21 4.95 --- 95.44 03/29/22 5.69 --- 94.70 211/05/10MW-9 98.95122 - 12211/05/10MW-7 99.55122 - 12211/05/10MW-8 100.39122 - 12 Page 3 of 5 Comments TABLE 2 WELL CONSTRUCTION AND GAUGING INFORMATION Date: 04/08/22 Facility ID #: 00-0-0000035658 Well ID Date Installed (mm/dd/yy) Date Water Level Measured (mm/dd/yy) Well Casing Depth (ft. BGS) Screened Interval (x to y ft. BGS) Bottom of Well (ft. BGS) Top of Casing Elevation* (ft.) Depth to Water from Top of Casing (ft.) Free Product Thickness (ft.) Ground Water Elevation* (ft.) SAM'S PIT STOP 11/10/10 2.97 --- 97.66 01/17/11 2.11 --- 98.52 07/14/11 2.90 --- 97.73 01/10/12 2.86 --- 97.77 05/31/12 2.10 --- 98.53 11/07/12 2.86 --- 97.77 04/22/14 1.96 --- 98.67 09/29/14 1.93 --- 98.70 06/07/16 1.82 --- 98.81 11/10/16 2.95 --- 97.68 05/09/17 2.17 --- 98.46 11/13/17 2.03 --- 98.60 05/10/18 1.97 --- 98.66 03/18/19 1.76 --- 98.87 03/09/21 2.18 --- 98.45 11/10/10 7.38 --- 90.92 01/17/11 NM --- NM 07/14/11 8.17 --- 90.13 01/10/12 5.53 --- 92.77 05/31/12 4.38 --- 93.92 11/07/12 6.15 --- 92.15 04/22/14 1.79 --- 96.51 09/29/14 3.07 --- 95.23 11/10/10 6.91 --- 90.99 01/17/11 NM --- NM 07/14/11 7.75 --- 90.15 01/10/12 5.23 --- 92.67 05/31/12 5.75 --- 92.15 11/07/12 5.80 --- 92.10 04/22/14 2.31 --- 95.59 09/29/14 3.16 --- 94.74 05/10/18 3.91 --- 93.99 11/10/10 7.51 --- 90.99 01/17/11 5.57 --- 92.93 07/14/11 8.29 --- 90.21 01/10/12 5.80 --- 92.70 05/31/12 5.39 --- 93.11 11/07/12 6.34 --- 92.16 06/05/13 5.01 --- 93.49 04/22/14 2.56 --- 95.94 09/29/14 3.64 --- 94.86 06/07/16 2.82 --- 95.68 11/10/16 5.75 --- 92.75 05/09/17 4.32 --- 94.18 05/10/18 4.39 --- 94.11 03/18/19 5.57 --- 92.93 03/09/21 3.46 --- 95.04 03/29/22 4.31 --- 94.19 01/17/11 1.31 --- 98.31 07/14/11 NM --- NM Not found 01/27/12 1.28 --- 98.34 05/31/12 1.30 --- 98.32 11/07/12 2.54 --- 97.08 04/22/14 1.05 --- 98.57 09/29/14 1.46 --- 98.16 Destroyed 98.50122 - 12211/05/10MW-13 100.63122 - 12211/05/10MW-10 97.90122 - 12211/05/10MW-12 MW-11 11/05/10 2 2 - 12 12 98.30 MW-14 01/12/11 2 2 - 12 12 99.62 Page 4 of 5 Comments TABLE 2 WELL CONSTRUCTION AND GAUGING INFORMATION Date: 04/08/22 Facility ID #: 00-0-0000035658 Well ID Date Installed (mm/dd/yy) Date Water Level Measured (mm/dd/yy) Well Casing Depth (ft. BGS) Screened Interval (x to y ft. BGS) Bottom of Well (ft. BGS) Top of Casing Elevation* (ft.) Depth to Water from Top of Casing (ft.) Free Product Thickness (ft.) Ground Water Elevation* (ft.) SAM'S PIT STOP 11/10/10 9.67 --- 91.01 01/17/11 NM --- NM 07/14/11 10.35 --- 90.33 01/10/12 7.92 --- 92.76 05/31/12 7.50 --- 93.18 11/07/12 8.57 --- 92.11 04/22/14 4.91 ---95.77 09/29/14 5.72 ---94.96 03/09/21 5.52 ---95.16 Notes: TW-1 100.684540-454011/04/10 • NM: Not measured. • Top of casing elevations were measured by Anderson Surveying in January 2011. • ft BGS : feet below ground surface Page 5 of 5 Date: 05/15/22 Facility ID No.: 00-0-0000035658 Well ID Date Collected (mm/dd/yy) 1 600 600 500 20 6 5,000 260,000 84,500 85,500 20,000 6,000 01/26/10 9,450 42.7 J 132 234 3,240 748 11/10/10 389 4.65 J 10.4 19.9 276 12.8 07/14/11 331 4.6 J 11.2 14.4 J 122 4.4 J 01/09/12 974 4.2 J 11.9 16.1 165 40.1 05/31/12 1,300 39.7 32.8 52.9 143 67.4 11/07/12 822 3.8 J 18.1 21.7 J 70.8 40.7 06/05/13 124 2.1 4.8 16.5 39 6.1 04/22/14 489 38.4 17.9 39 47.4 93.8 09/29/14 869 430 251 1,370 30.8 108 03/16/15 737 2.6 54.4 120 20 47.9 01/19/16 323 3.0 J 11.8 15.1 14.2 4.5 J 06/07/16 223 5.5 9.7 48.7 14.6 3.2 11/13/17 101 2.4 6.2 20.8 5.9 1.3 03/18/19 276 18.1 19.3 32.0 6.3 1.5 J 03/09/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 03/29/22 54.7 2.1 3.6 11 3.8 0.8 02/11/10 <0.140 <0.190 <0.150 <0.220 19.4 <0.500 11/10/10 <0.140 <0.190 <0.150 <0.220 9.11 <0.500 07/14/11 <0.13 <0.13 0.15 <0.30 7.9 <0.10 01/09/12 <0.13 <0.13 0.15 <0.30 1.8 0.15 J 05/31/12 <0.13 <0.13 0.15 <0.30 2.3 <0.10 11/07/12 <0.10 <0.10 <0.10 <0.22 4 <0.15 04/22/14 <0.10 <0.10 <0.10 <0.20 6.7 0.22 J 09/29/14 <0.10 <0.10 <0.10 <0.20 2.5 <0.10 03/16/15 <0.17 <0.17 <0.15 <0.43 2.8 <0.12 01/19/16 <0.13 <0.13 <0.13 <0.31 4.8 <0.13 06/07/16 <0.13 <0.13 <0.13 <0.31 1.3 <0.13 11/13/17 <0.13 <0.13 <0.13 <0.25 1.2 <0.13 03/18/19 <0.13 <0.13 <0.13 <0.25 5.3 <0.13 03/09/21 <0.13 <0.13 <0.13 <0.25 1.3 <0.13 02/11/10 11.2 <0.190 <0.150 1.05 156 <0.500 11/10/10 <0.140 <0.190 <0.150 <0.220 0.666 J <0.500 07/14/11 <0.13 <0.13 0.15 <0.30 3.6 <0.10 01/09/12 <0.13 <0.13 0.15 <0.30 1.4 <0.10 05/31/12 <0.13 <0.13 0.15 <0.30 1.7 <0.10 11/07/12 <0.10 <0.10 <0.10 <0.22 1.2 <0.15 06/05/13 <0.10 <0.10 <0.10 <0.22 1.2 <0.15 04/22/14 <0.10 <0.10 <0.10 <0.20 4.4 <0.10 09/29/14 <0.10 <0.10 <0.10 <0.20 2.6 <0.10 03/16/15 NR NR NR NR NR NR 01/19/16 <0.13 <0.13 <0.13 <0.31 0.99 <0.13 03/18/19 <0.13 <0.13 <0.13 <0.25 0.37 J <0.13 03/09/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 Methyl-tert-butyl ether(MTBE)NaphthaleneTABLE 3 SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS SAM'S PIT STOP #64 (INCIDENT NO. 32595) Analytical Method SM 6200B Contaminant of Concern BenzeneTolueneEthylbenzeneTotal XylenesMW-1 MAC (µg/l) GCL (µg/l) MW-2 MW-3 Page 1 of 5 Date: 05/15/22 Facility ID No.: 00-0-0000035658 Well ID Date Collected (mm/dd/yy) 1 600 600 500 20 6 5,000 260,000 84,500 85,500 20,000 6,000Methyl-tert-butyl ether(MTBE)NaphthaleneTABLE 3 SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS SAM'S PIT STOP #64 (INCIDENT NO. 32595) Analytical Method SM 6200B Contaminant of Concern BenzeneTolueneEthylbenzeneTotal XylenesMAC (µg/l) GCL (µg/l) 02/11/10 <0.140 <0.190 <0.150 <0.220 5.67 <0.500 11/10/10 <0.140 <0.190 <0.150 <0.220 3.34 <0.500 07/14/11 <0.13 <0.13 0.15 <0.30 0.64 <0.10 01/09/12 <0.13 <0.13 0.15 <0.30 0.26 J <0.10 05/31/12 <0.13 <0.13 0.15 <0.30 <0.13 <0.10 11/07/12 <0.10 <0.10 <0.10 <0.22 0.39 J <0.15 06/05/13 <0.10 <0.10 <0.10 <0.22 1.9 <0.15 04/22/14 <0.10 <0.10 <0.10 <0.20 11.5 <0.10 09/29/14 <0.10 <0.10 <0.10 <0.20 15.7 <0.10 03/16/15 <0.17 <0.17 <0.15 <0.43 25.5 <0.12 01/19/16 <0.13 <0.13 <0.13 <0.31 37.7 <0.13 06/07/16 <0.13 0.14 J <0.13 <0.31 27.6 <0.13 11/13/17 <0.13 50.5 <0.13 <0.25 3.2 <0.13 03/18/19 <0.13 <0.13 <0.13 <0.25 3.2 <0.13 03/09/21 <0.13 <0.13 <0.13 <0.25 1.6 <0.13 03/29/22 <0.13 <0.13 <0.13 <0.25 0.77 <0.13 11/10/10 <0.140 <0.190 <0.150 <0.220 21.5 <0.500 07/14/11 <0.13 <0.13 0.15 0.33 J 25.0 0.13 J 01/09/12 <0.13 <0.13 0.15 <0.30 21.8 <0.10 05/31/12 <0.13 0.33 J 0.15 0.30 J 19.6 <0.10 11/07/12 <0.10 <0.10 <0.10 <0.22 17 <0.15 06/05/13 <0.10 <0.10 <0.10 <0.22 15.5 <0.15 04/22/14 <0.10 <0.10 <0.10 <0.20 15.1 <0.10 09/29/14 <0.10 <0.10 <0.10 <0.20 17.9 <0.10 03/16/15 NR NR NR NR NR NR 01/19/16 <0.13 <0.13 <0.13 <0.31 17.4 <0.13 11/10/10 <0.140 <0.190 <0.150 <0.220 23.4 <0.500 07/14/11 <0.13 <0.13 0.15 <0.30 8.9 <0.10 01/09/12 <0.13 <0.13 0.15 <0.30 20.0 <0.10 05/31/12 <0.13 <0.13 0.15 <0.30 10.7 <0.10 11/07/12 <0.10 <0.10 <0.10 <0.22 20.6 <0.15 06/05/13 <0.10 <0.10 <0.10 <0.22 6.9 <0.15 04/22/14 <0.10 <0.10 <0.10 <0.20 6.1 <0.10 09/29/14 <0.10 <0.10 <0.10 <0.20 9.5 <0.10 03/16/15 <0.17 <0.17 <0.15 <0.43 12.3 <0.12 01/19/16 <0.13 <0.13 <0.13 <0.31 14.4 <0.13 11/10/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 07/14/11 <0.13 <0.13 0.15 <0.30 <0.13 <0.10 01/09/12 <0.13 <0.13 0.15 <0.30 0.20 J <0.10 05/31/12 <0.13 <0.13 0.15 <0.30 <0.13 <0.10 11/07/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 06/05/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 04/22/14 <0.10 <0.10 <0.10 <0.20 0.67 <0.10 09/29/14 <0.10 <0.10 <0.10 <0.20 0.17 J <0.10 03/16/15 NR NR NR NR NR NR 01/19/16 NR NR NR NR NR NR 03/18/19 <0.13 <0.13 <0.13 <0.25 0.56 <0.13 03/09/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 03/29/22 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 MW-6 MW-4 MW-7 MW-5 Page 2 of 5 Date: 05/15/22 Facility ID No.: 00-0-0000035658 Well ID Date Collected (mm/dd/yy) 1 600 600 500 20 6 5,000 260,000 84,500 85,500 20,000 6,000Methyl-tert-butyl ether(MTBE)NaphthaleneTABLE 3 SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS SAM'S PIT STOP #64 (INCIDENT NO. 32595) Analytical Method SM 6200B Contaminant of Concern BenzeneTolueneEthylbenzeneTotal XylenesMAC (µg/l) GCL (µg/l) 11/10/10 <0.140 <0.190 <0.150 <0.220 0.388 J <0.500 07/14/11 <0.13 <0.13 0.15 <0.30 0.34 J <0.10 01/09/12 <0.13 <0.13 0.15 <0.30 0.32 J <0.10 05/31/12 <0.13 0.17 J 0.15 <0.30 <0.13 <0.10 11/07/12 <0.10 <0.10 <0.10 <0.22 0.21 J <0.15 04/22/14 <0.10 <0.10 <0.10 <0.20 0.12 J <0.10 09/29/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 03/16/15 NR NR NR NR NR NR 01/19/16 NR NR NR NR NR NR 06/07/16 <0.13 <0.13 <0.13 <0.31 0.25 J <0.13 11/13/17 <0.13 <0.13 <0.13 <0.25 0.24 J <0.13 03/18/19 <0.13 <0.13 <0.13 <0.25 0.19 J <0.13 03/09/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 03/29/22 <0.13 <0.13 <0.13 <0.25 0.18 J <0.13 11/10/10 <0.700 <0.950 <0.750 <1.10 <1.25 6.34 07/14/11 <0.13 <0.13 <0.15 <0.30 0.79 <0.10 01/09/12 <0.13 <0.13 <0.15 <0.30 0.79 <0.10 05/31/12 <0.13 <0.13 <0.15 <0.30 0.83 <0.10 11/07/12 <0.10 <0.10 <0.10 <0.22 0.68 <0.15 04/22/14 7.5 1.2 1.2 3.1 <0.10 <0.10 09/29/14 25.7 3.1 3.9 10.1 <0.10 <0.10 03/16/15 27.2 4.1 3.5 11.2 <0.16 <0.12 01/19/16 70.5 11.3 16.5 36.6 <0.13 <0.13 06/07/16 17.7 2.7 2.1 6.1 0.22 J <0.13 11/13/17 78.9 9 6.6 25.1 <0.13 0.45 J 03/18/19 13.1 0.86 0.80 3.8 <0.13 <0.13 03/09/21 13.6 3.5 0.73 6.6 <0.13 <0.13 03/29/22 104 10.2 5.9 33.3 <0.13 <0.13 11/10/10 <0.140 <0.190 <0.150 <0.220 2.36 <0.500 07/14/11 <0.13 <0.13 <0.15 <0.30 3.8 <0.10 01/09/12 <0.13 <0.13 <0.15 <0.30 2.6 <0.10 05/31/12 <0.13 <0.13 <0.15 <0.30 2.6 <0.10 11/07/12 <0.10 <0.10 <0.10 <0.22 1.4 <0.15 04/22/14 <0.10 <0.10 <0.10 <0.20 2.5 <0.10 09/29/14 <0.10 <0.10 <0.10 <0.20 1.2 <0.10 03/16/15 NR NR NR NR NR NR 01/19/16 NR NR NR NR NR NR 03/18/19 <0.13 <0.13 <0.13 <0.25 0.82 <0.13 03/09/21 <0.13 <0.13 <0.13 <0.25 1.7 <0.13 11/10/10 <0.140 <0.190 <0.150 <0.220 0.269 J <0.500 07/14/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 01/09/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 05/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 11/07/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 04/22/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 09/29/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 03/16/15 NR NR NR NR NR NR 01/19/16 NR NR NR NR NR NR MW-9 MW-8 MW-10 MW-11 Page 3 of 5 Date: 05/15/22 Facility ID No.: 00-0-0000035658 Well ID Date Collected (mm/dd/yy) 1 600 600 500 20 6 5,000 260,000 84,500 85,500 20,000 6,000Methyl-tert-butyl ether(MTBE)NaphthaleneTABLE 3 SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS SAM'S PIT STOP #64 (INCIDENT NO. 32595) Analytical Method SM 6200B Contaminant of Concern BenzeneTolueneEthylbenzeneTotal XylenesMAC (µg/l) GCL (µg/l) 11/10/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 07/14/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 01/09/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 05/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 11/07/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 04/22/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 09/29/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 03/16/15 NR NR NR NR NR NR 01/19/16 NR NR NR NR NR NR 11/10/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 07/14/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 01/09/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 05/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 11/07/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 06/05/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 04/22/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 09/29/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 03/16/15 NR NR NR NR NR NR 01/19/16 NR NR NR NR NR NR 03/18/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 03/09/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 03/29/22 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 01/17/11 <0.140 0.248 J <0.150 <0.220 0.786 J <0.500 01/27/12 <0.13 <0.13 <0.15 <0.30 0.97 <0.10 05/31/12 <0.13 0.37 J 0.15 <0.30 0.51 <0.10 11/07/12 <0.10 <0.10 <0.10 <0.22 2.5 <0.15 04/22/14 <0.10 <0.10 <0.10 <0.20 1.3 <0.10 09/29/14 <0.10 <0.10 <0.10 <0.20 1.3 <0.10 03/16/15 NR NR NR NR NR NR 01/19/16 NR NR NR NR NR NR 11/10/10 0.826 J 0.404 J 0.693 J 4.00 0.789 J <0.500 07/14/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 01/09/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 05/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 11/07/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 04/22/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 09/29/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 03/16/15 NR NR NR NR NR NR 01/19/16 NR NR NR NR NR NR 03/09/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 11/10/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 03/16/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 11/10/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 09/29/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 WSW-6 03/16/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 WSW-7 09/29/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 WSW-9 03/16/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 WSW-1 WSW-2 MW-12 MW-14 TW-1 MW-13 Page 4 of 5 Date: 05/15/22 Facility ID No.: 00-0-0000035658 Well ID Date Collected (mm/dd/yy) 1 600 600 500 20 6 5,000 260,000 84,500 85,500 20,000 6,000Methyl-tert-butyl ether(MTBE)NaphthaleneTABLE 3 SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS SAM'S PIT STOP #64 (INCIDENT NO. 32595) Analytical Method SM 6200B Contaminant of Concern BenzeneTolueneEthylbenzeneTotal XylenesMAC (µg/l) GCL (µg/l) Notes: • Results reported in micrograms per liter (µg/l). • < : Less than the method detection limit specified in the laboratory report. • MAC: Maximum Allowable Concentration as pecified in 2L Standard specified in T15A NCAC 2L.0202. • GCL: Gross contamination level. • NE: Not Established • Concentrations in bold face type exceeded the 2L standards. • Concentrations in italics exceeded the gross contamination levels. • ND: No Data provided. • NR: Analysis not requested. • Refer to laboratory report for detected constituents that did not exceed the MACs, or for which no standard has been established. Page 5 of 5 APPENDICES APPENDIX A Well Surveys COLUMBUS COUNTY LAND RECORDS - PROPERTY RECORD CARDPROPERTY#TWSHP PIN LAST REVAL PRIOR VALUE CARD#LEGAL DESCRIPTION PROPERTY FACTORS MAP ACCESS TOPO LND IMP SHAPE RECORD OF OWNERSHIP BOOK PAGE YEAR STAMPS PROPERTY LOCATION CLASS OCCUP LISTED DATE BUILDING APPR DATE ZONED % COMPLETE ACT YR BLT COND EFF. YR BLT.BUILDING ELEMENTS AND CALCULATIONS VALUE DESCRIPTION VALUE FOUNDATION ATTIC FLOORING SYSTEM BASE OF AREA STRUCTURAL FRM BASE S/F EXTERIOR WALLS STORY C/D ROOF FRAMING WALL HEIGHT ROOF COVER ATTACHMENTS ROOF DESIGN FLOOR COVER INTERIOR FINISH CAB/MILL WORK ELECTRICAL PLUMBING FIXTURES PERIMETER MULT SPRINKLER SYSTEM GRADE HEAT/COOL DEPR P/F/E FIREPLACE TOTAL VALUE BASEMENT NEIGHBORHOOD INFLUENCE SUMMARY OF OTHER IMPROVEMENTS LINE #CODE DESCRIPTION #CONST SIZE AREA RATE YR DEP VALUE SALES INFORMATION AMOUNT: DATE: QUAL SALE: TOTAL VALUE SUMMARY OF OTHER IMPROVEMENTS TOTAL VALUE LAND TOTAL VALUE BUILDINGS TOTAL VALUE LAND DESCRIPTION CALCULATIONS FRTG DEPTH UT PR DEP FAC FF PRICE SUB TOTAL SH TOPO R/W OTHER ADJ LAND VALUE SQUARE FOOTAGE SF PRICE SUB TOTAL SH TOPO R/W OTHER ADJ LAND VALUE CLASS ACRES SIZE FAC NET %RATE LAND VALUE TOTAL ACRES TOTAL LAND VALUE LAND USE VALUATIONS AND TOTALS CLASS # ACRES RATE LAND VALUE BUILDING SITE TOTAL ACRES TOTAL USE VALUE LAND TOTAL USE VALUE BUILDINGS TOTAL USE VALUE 1220.01-18-2462.000 00680O 000002 155758 88934 11 HB 3 129 162400 174700 1 HALLSBORO STORE#64//WHITEVILLE OIL CO 00680O 000003 155759 11-05843 00680O 000004 155760 SAMS PIT STOP PROPERTIES LLC 04 41 04 01 00 01 00680O 000005 155761 PO BOX 689 765 5892003 4236 SAM POTTS HWY 00680O 000006 155762 28472 PPD 01-1590 00680O 000007 155763 WHITEVILLE NC HF -- CR -- 00680O 000008 155764 SEE765/589-PAECEL#6 TRCT#2'03 00680O 000009 155765 STORE & IMPR FR #20447 HERE FOR'18 00680O 000010 155766 IH-ADJ'21 00680O 000011 155767 1990 A 1995 00680O 000014 155768 03 SLAB 00680O 000016 155769 02 SLAB BASE 1728 65.92 00680O 000018 155770 01 WD.FR. BASE 1728 65.92 113909 00680O 000020 155771 01-1STY 00680O 000021 155772 01 BRICK BASE 00680O 000022 155773 01 WD.FR. BASE 1 00680O 000024 155774 01 COMP. 00680O 000026 155775 03 GABEL 00680O 000027 155776 BASE +-------------54-----------+ 00680O 000028 155777 08 H.TILE : : 00680O 000029 155778 06 CONC. BASE : : 00680O 000030 155779 : : 00680O 000031 155780 03 AVG. BASE : : 00680O 000032 155781 : : 00680O 000033 155782 03 AVG BASE 3 3 00680O 000034 155783 2 2 00680O 000035 155784 03 AVG. BASE : : 00680O 000036 155785 : : 00680O 000037 155786 4 2500 : : 00680O 000038 155787 130785 : 50 : 00680O 000039 155788 C+05 105 137324 +------------54------------+ 00680O 000040 155789 07 P.H/AC 14376 30/ / 5 46004 00680O 000042 155790 01 NONE XF UD FACT 00680O 000043 155791 91320 .00 91300 448 130 165 94 155.1 69484.21 .21- 54892 00680O 000044 155792 6 PAV-CO 1 CONC 80X50 4000 295 90 20 9440 00680O 000049 155793 6 PAV-CO 1 CONC 80X25 2000 295 90 20 4720 00680O 000050 155794 4 CNP-SER 1 STG 22X40 8802037 90 20 14340 DIRT FACT 00680O 000051 155795 28500 00680O 000059 155796 54900 00680O 000061 155797 10/01/2003 00680O 000062 155798 NO - 119800 00680O 000063 155799 174700 4/20/22 00680O 000066 155800 COLUMBUS COUNTY LAND RECORDS - PROPERTY RECORD CARDPROPERTY#TWSHP PIN LAST REVAL PRIOR VALUE CARD#LEGAL DESCRIPTION PROPERTY FACTORS MAP ACCESS TOPO LND IMP SHAPE RECORD OF OWNERSHIP BOOK PAGE YEAR STAMPS PROPERTY LOCATION CLASS OCCUP LISTED DATE BUILDING APPR DATE ZONED % COMPLETE ACT YR BLT COND EFF. YR BLT.BUILDING ELEMENTS AND CALCULATIONS VALUE DESCRIPTION VALUE FOUNDATION ATTIC FLOORING SYSTEM BASE OF AREA STRUCTURAL FRM BASE S/F EXTERIOR WALLS STORY C/D ROOF FRAMING WALL HEIGHT ROOF COVER ATTACHMENTS ROOF DESIGN FLOOR COVER INTERIOR FINISH CAB/MILL WORK ELECTRICAL PLUMBING FIXTURES PERIMETER MULT SPRINKLER SYSTEM GRADE HEAT/COOL DEPR P/F/E FIREPLACE TOTAL VALUE BASEMENT NEIGHBORHOOD INFLUENCE SUMMARY OF OTHER IMPROVEMENTS LINE #CODE DESCRIPTION #CONST SIZE AREA RATE YR DEP VALUE SALES INFORMATION AMOUNT: DATE: QUAL SALE: TOTAL VALUE SUMMARY OF OTHER IMPROVEMENTS TOTAL VALUE LAND TOTAL VALUE BUILDINGS TOTAL VALUE LAND DESCRIPTION CALCULATIONS FRTG DEPTH UT PR DEP FAC FF PRICE SUB TOTAL SH TOPO R/W OTHER ADJ LAND VALUE SQUARE FOOTAGE SF PRICE SUB TOTAL SH TOPO R/W OTHER ADJ LAND VALUE CLASS ACRES SIZE FAC NET %RATE LAND VALUE TOTAL ACRES TOTAL LAND VALUE LAND USE VALUATIONS AND TOTALS CLASS # ACRES RATE LAND VALUE BUILDING SITE TOTAL ACRES TOTAL USE VALUE LAND TOTAL USE VALUE BUILDINGS TOTAL USE VALUE 1220.01-18-1375.000 00680N 000002 155801 88935 11 HB 3 124 10800 11300 1 HALLSBORO STORE #64/WHITEVILLE OIL CO 00680N 000003 155802 11-05843 00680N 000004 155803 SAMS PIT STOP PROPERTIES LLC 13 00 04 01 00 01 00680N 000005 155804 PO BOX 689 765 5892003 NEAR 4236 SAM POTTS HWY 00680N 000006 155805 28472 00-0000 00680N 000007 155806 WHITEVILLE NC HF -- CR -- 00680N 000008 155807 SEE 765/589-PARCEL#6 TRCT#6'03 00680N 000009 155808 / / 00680N 000042 155809 XF UD FACT 00680N 000043 155810 .00 50 165 120106 127.2 6360 6360 00680N 000044 155811 80 50 110 56 61.6 4928 4928 00680N 000045 155812 DIRT FACT 00680N 000051 155813 11300 00680N 000061 155814 10/01/2003 00680N 000062 155815 NO - 00680N 000063 155816 11300 4/20/22 00680N 000066 155817 COLUMBUS COUNTY LAND RECORDS - PROPERTY RECORD CARDPROPERTY#TWSHP PIN LAST REVAL PRIOR VALUE CARD#LEGAL DESCRIPTION PROPERTY FACTORS MAP ACCESS TOPO LND IMP SHAPE RECORD OF OWNERSHIP BOOK PAGE YEAR STAMPS PROPERTY LOCATION CLASS OCCUP LISTED DATE BUILDING APPR DATE ZONED % COMPLETE ACT YR BLT COND EFF. YR BLT.BUILDING ELEMENTS AND CALCULATIONS VALUE DESCRIPTION VALUE FOUNDATION ATTIC FLOORING SYSTEM BASE OF AREA STRUCTURAL FRM BASE S/F EXTERIOR WALLS STORY C/D ROOF FRAMING WALL HEIGHT ROOF COVER ATTACHMENTS ROOF DESIGN FLOOR COVER INTERIOR FINISH CAB/MILL WORK ELECTRICAL PLUMBING FIXTURES PERIMETER MULT SPRINKLER SYSTEM GRADE HEAT/COOL DEPR P/F/E FIREPLACE TOTAL VALUE BASEMENT NEIGHBORHOOD INFLUENCE SUMMARY OF OTHER IMPROVEMENTS LINE #CODE DESCRIPTION #CONST SIZE AREA RATE YR DEP VALUE SALES INFORMATION AMOUNT: DATE: QUAL SALE: TOTAL VALUE SUMMARY OF OTHER IMPROVEMENTS TOTAL VALUE LAND TOTAL VALUE BUILDINGS TOTAL VALUE LAND DESCRIPTION CALCULATIONS FRTG DEPTH UT PR DEP FAC FF PRICE SUB TOTAL SH TOPO R/W OTHER ADJ LAND VALUE SQUARE FOOTAGE SF PRICE SUB TOTAL SH TOPO R/W OTHER ADJ LAND VALUE CLASS ACRES SIZE FAC NET %RATE LAND VALUE TOTAL ACRES TOTAL LAND VALUE LAND USE VALUATIONS AND TOTALS CLASS # ACRES RATE LAND VALUE BUILDING SITE TOTAL ACRES TOTAL USE VALUE LAND TOTAL USE VALUE BUILDINGS TOTAL USE VALUE 1220.01-18-1219.000 00680M 000002 155818 88936 11 HB 3 124 8400 9200 1 HALLSBORO STORE #64//LOT#2-3 00680M 000003 155819 11-05843 00680M 000004 155820 SAMS PIT STOP PROPERTIES LLC 14 00 04 01 00 01 00680M 000005 155821 PO BOX 689 765 5892003 NEAR 4236 SAM POTTS HWY 00680M 000006 155822 28472 00-0000 00680M 000007 155823 WHITEVILLE NC HF -- CR -- 00680M 000008 155824 PAR#6,TRCT#5-SEE 765/589'03 00680M 000009 155825 / / 00680M 000042 155826 XF UD FACT 00680M 000043 155827 .00 85 115 120 90 108.0 9180 9180 00680M 000044 155828 DIRT FACT 00680M 000051 155829 9200 00680M 000061 155830 10/01/2003 00680M 000062 155831 NO - 00680M 000063 155832 9200 4/20/22 00680M 000066 155833 COLUMBUS COUNTY LAND RECORDS - PROPERTY RECORD CARDPROPERTY#TWSHP PIN LAST REVAL PRIOR VALUE CARD#LEGAL DESCRIPTION PROPERTY FACTORS MAP ACCESS TOPO LND IMP SHAPE RECORD OF OWNERSHIP BOOK PAGE YEAR STAMPS PROPERTY LOCATION CLASS OCCUP LISTED DATE BUILDING APPR DATE ZONED % COMPLETE ACT YR BLT COND EFF. 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BASE : 2 007695 000036 230388 1 5 007695 000037 230389 5 3125 5 : 007695 000038 230390 66692 : : 007695 000039 230391 E+- 65 43350 +-------33------+ 007695 000040 230392 01 NONE 70/ / 30345 007695 000042 230393 01 NONE XF UD FACT 007695 000043 230394 13005 .00 13000 50 116 100 90 90.0 4500 4500 007695 000044 230395 DIRT FACT 007695 000051 230396 4500 007695 000061 230397 3/25/2005 007695 000062 230398 NO - 13000 007695 000063 230399 17500 4/22/22 007695 000066 230400 APPENDIX B State Correspondence Site Name City / County /Columbus Incident #32595 Resp Pty Name / Contact Incident Mgr Region WIL RP Type (Owner/Operator / Landowner / Attny-in-fact)Change Order?Prev. TA #17 Consultant / Project Mgr /Rae Troiano Brown Telephone / Fax Number /Task Authorization Number:18 ChangeOrd: Project Mgr Email Site Risk / Rank / Abatement:H550D RRA Date:3/29/2010 Proposal# / Scope Dates /% Commercial (C=100%, NC=0%, Both=1%-99%) Has STF Eligibility Been Determined? (Y/N)Site Status (Active or NFA Date) With Claim: [ ] All Main Consultant/Contractor invoices attached?[ ] Proof of payment attached directly to the front of each invoice? w Important: The date of reimbursement is dependent on the Trust Fund balance. There may be a delay in the reimbursement of claims for work under this ePATA.3rd Pty Ded?Task #Lab / SubCode RO IM AuthProposed Rate/Price (Consultant)RO Supv. AuthProposed Task Subtotal (Consultant) Preapproved Subtotal (UST Section) Claimed Amount3 (Consultant) 1.025 1 /site y $740.00 Y $740.00 $740.00 / 4.031 8 /wells 6 $110.00 Y $880.00 $660.00 / 4.090 #220 9 /samples n $37.00 N $333.00 $0.00 / 4.091 1 /shipment y $60.00 Y $60.00 $60.00 / 6.091 1 /report y $900.00 Y $900.00 $900.00 / 12.050 1 /trip y $250.00 Y $250.00 $250.00 / // // 4.090 #240 6 /wells y $88.00 Y $528.00 $528.00 / // // // // // // // // // // // // // // // // // // Requested Preapproved Claimed3 TOTAL:$3,691.00 $3,138.00 TOTAL: Total Standard Costs (Not Third Party)$3,691.00 $3,138.00 Total Standard Costs Total applied as Third Party Deductible/Damage Costs $0.00 $0.00 Total Third Pty Costs Process Tracking (Date) TA Submittal:2/2/22 by:(PM)(Reserved for RO) RO Review:3/3/22 by:(IM)Joint UST Preapproval Confirmed By:Date1 3/7/2022 RO Supv. Review:3/3/22 by:(STF)RP or Designee Receipt Confirmation By:Date 4 1 - This ePATA expires one year from the Joint UST Preapproval date. This does not extend, alter, or supersede any regulatory deadlines (e.g., NORR's, NOV's, Enforcements, etc.) 2 - THE ONE YEAR STATUTE OF LIMITATIONS APPLIES TO EACH INDIVIDUAL TASK. Costs must be claimed within one year of completion of that task to be reimbursable. 3 - Only Tasks included on this ePATA may be claimed. Do not include other Tasks or claimed costs (i.e., Claim preparation) that were not preapproved or the claim will be returned. 4 - Preapproval is not valid (i.e., claimable) until receipt is signed as 'Confirmed' by the RP or their designee within a week of approval. The signed pre-approval must be submitted in the submitted claim. Signature indicates acknowledgement of the tasks and amounts approved. Any objections/appeals must be submitted via Change Order prior to work proceeding. Scope/cost negotiations do not supersede other regulatory deadlines as described in #1 above. Also, any ePATA that has been signed as 'Confirmed' by both the UST Section and RP is not to be modified without written consent by all signatories. 5 - Tasks approved on Directed - CAB Only ePATAs must be performed in accordance with all applicable rules, statutes, and RRD Task Scopes of Work to be reimbursed in full. DWM/UST ePATA 8/1/2020 DIRECTED - CAB ONLY Hallsboro (Must Complete with Claim Submittal)(See Instructions / RRD for Tasks requiring Preapproval / Task Authorization) Owner/Operator 704-845-4010 (Reserved for Incident Manager) PREAPPROVAL / TASK AUTHORIZATION Sam's Pit Stop Note: This Electronic Preapproval Task Authorization (ePATA) shall be used to receive preapproval from the UST Section. A proposal,including maps and figures,must be attached to elaborate on the costs for the tasks listed below that describes the scope of work and the rationale for theproposed activities.If, following completion ofthis ePATA, you discover that unexpected tasks must be performed, incurring costs for tasks not originally included with this form, you must complete and submit a separate ePATA request designated as a "Change Order"in the provided space above prior to conducting those tasks. Include a copy of the prior ePATA form for confirmation. Please attach this form to the cover of the corresponding claim when requesting reimbursement. IMPORTANT:Only one claim may be submitted per ePATA and all work on the ePATA must have been completed within 12 months of the completion date of the FIRST completed task to remain within the Statute of Limitations. All ePATAs submitted within a claim are closed with that claim, and may not be re-used ina separate submittal,evenfor costs or tasks that were not originally claimed. Final reimbursement of costs associated with the Total Claimed amount below may be affected by the eligibility status of the site (i.e., deductibles, apportionment, etc.), and the documentary validation of incurred costs as reasonable and necessary expenses per 15A NCAC 2P .0402 and .0404. SAK MHH (Initials) RTB Proposed Units / Type (Consultant) Steve kay activeTRUE 22-099 Mar.-Apr. 2022 704-845-4012 Dates of Work (Consultant) Started1 / Completed2 FINAL REIMBURSEMENT 100.00% rtb@geologicalresourcesinc.com Sam's Pit Stop inc. Geological Resources, Inc. ELECTRONIC PREAPPROVAL TASK AUTHORIZATION FORM Dept of Environmental Quality -Division of Waste Management Sample monitoring wells MW-1, MW-4, MW-7, MW-8, MW-9 & MW-13 APPENDIX C Laboratory Report – Ground Water Samples 04/14/22 Technical Report for GRI (Geological Resources Inc.) Sam's Pit Stop; 4236 Sam Potts Hwy, Hallsboro, NC 32595/2895 SGS Job Number: FA94413 Sampling Date: 03/29/22 Report to: GRI 3502 Hayes Rd Monroe, NC 28110 rtb@geologicalresourcesinc.com; carriekennedy@geologicalresourcesinc.com; jjr@geologicalresourcesinc.com; nml@geologicalresourcesinc.com ATTN: Rae Brown Total number of pages in report: Certifications: FL(E83510), LA(03051), KS(E-10327), NC(573), NJ(FL002), NY(12022), SC(96038001) DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177), AL, AK, AR, CT, IA, KY, MA, MI. MS, ND, NH, NV, OK, OR, IL, UT, VT, WA, WI, WV This report shall not be reproduced, except in its entirety, without the written approval of SGS. Test results relate only to samples analyzed. SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: 407-425-6700 • fax: 407-425-0707 Test results contained within this data package meet the requirements of the National Environmental Laboratory Accreditation Program and/or state specific certification programs as applicable. Client Service contact: Muna Mohammed 407-425-6700 Norm Farmer Technical Director Orlando, FL 04/14/22 e-Hardcopy 2.0 Automated Report 40 SGS is the sole authority for authorizing edits or modifications to this document. Unauthorized modification of this report is strictly prohibited. Review standard terms at: http://www.sgs.com/en/terms-and-conditions The results set forth herein are provided by SGS North America Inc. Please share your ideas about how we can serve you better at: EHS.US.CustomerCare@sgs.com 1 of 40 FA94413 Table of Contents -1- Sections: Section 1: Sample Summary ...................................................................................................3 Section 2: Summary of Hits ....................................................................................................4 Section 3: Sample Results ........................................................................................................6 3.1: FA94413-1: MW-1 ........................................................................................................7 3.2: FA94413-2: MW-4 ........................................................................................................10 3.3: FA94413-3: MW-7 ........................................................................................................13 3.4: FA94413-4: MW-8 ........................................................................................................16 3.5: FA94413-5: MW-9 ........................................................................................................19 3.6: FA94413-6: MW-13 ......................................................................................................22 Section 4: Misc. Forms ............................................................................................................25 4.1: Chain of Custody ...........................................................................................................26 Section 5: MS Volatiles - QC Data Summaries .....................................................................28 5.1: Method Blank Summary ................................................................................................29 5.2: Blank Spike Summary ...................................................................................................33 5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................37 123452 of 40 FA94413 SGS North America Inc. Sample Summary GRI (Geological Resources Inc.) Job No:FA94413 Sam's Pit Stop; 4236 Sam Potts Hwy, Hallsboro, NC Project No: 32595/2895 Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID This report contains results reported as ND = Not detected. The following applies: Organics ND = Not detected above the MDL FA94413-1 03/29/22 09:15 ER 03/30/22 AQ Ground Water MW-1 FA94413-2 03/29/22 10:00 ER 03/30/22 AQ Ground Water MW-4 FA94413-3 03/29/22 09:33 ER 03/30/22 AQ Ground Water MW-7 FA94413-4 03/29/22 09:51 ER 03/30/22 AQ Ground Water MW-8 FA94413-5 03/29/22 09:23 ER 03/30/22 AQ Ground Water MW-9 FA94413-6 03/29/22 09:41 ER 03/30/22 AQ Ground Water MW-13 3 of 40 FA944131 Summary of Hits Page 1 of 2 Job Number:FA94413 Account:GRI (Geological Resources Inc.) Project:Sam's Pit Stop; 4236 Sam Potts Hwy, Hallsboro, NC Collected:03/29/22 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method FA94413-1 MW-1 Benzene 54.7 1.0 0.25 ug/l SM 6200B n-Butylbenzene 1.7 0.50 0.13 ug/l SM 6200B sec-Butylbenzene 1.9 0.50 0.13 ug/l SM 6200B Chloroethane a 0.52 J 1.0 0.40 ug/l SM 6200B Di-Isopropyl Ether 0.15 J 0.50 0.13 ug/l SM 6200B Ethylbenzene 3.6 0.50 0.13 ug/l SM 6200B Ethyl Tert Butyl Ether 3.7 0.50 0.13 ug/l SM 6200B Isopropylbenzene 23.2 0.50 0.13 ug/l SM 6200B Methyl Chloride 1.5 1.0 0.40 ug/l SM 6200B Methyl Tert Butyl Ether 3.8 0.50 0.13 ug/l SM 6200B Naphthalene 0.80 0.50 0.13 ug/l SM 6200B n-Propylbenzene 45.5 1.0 0.25 ug/l SM 6200B Tert-Amyl Alcohol 75.2 10 2.0 ug/l SM 6200B Tert-Butyl Alcohol 59.4 10 2.0 ug/l SM 6200B Toluene 2.1 0.50 0.13 ug/l SM 6200B 1,2,4-Trimethylbenzene 0.39 J 0.50 0.13 ug/l SM 6200B 1,3,5-Trimethylbenzene 0.22 J 0.50 0.13 ug/l SM 6200B m,p-Xylene 9.6 1.0 0.13 ug/l SM 6200B o-Xylene 1.4 0.50 0.13 ug/l SM 6200B Xylene (total)11.0 1.5 0.25 ug/l SM 6200B FA94413-2 MW-4 Methyl Bromide 0.30 J 0.50 0.20 ug/l SM 6200B Methyl Chloride 0.55 0.50 0.20 ug/l SM 6200B Methyl Tert Butyl Ether 0.77 0.50 0.13 ug/l SM 6200B Tert-Butyl Alcohol 2.8 J 10 2.0 ug/l SM 6200B FA94413-3 MW-7 Methyl Bromide 0.46 J 0.50 0.20 ug/l SM 6200B Methyl Chloride 1.1 0.50 0.20 ug/l SM 6200B FA94413-4 MW-8 Methyl Bromide 0.34 J 0.50 0.20 ug/l SM 6200B Methyl Chloride 0.46 J 0.50 0.20 ug/l SM 6200B Methyl Tert Butyl Ether 0.18 J 0.50 0.13 ug/l SM 6200B FA94413-5 MW-9 Benzene 104 2.5 0.63 ug/l SM 6200B n-Butylbenzene 0.37 J 0.50 0.13 ug/l SM 6200B 4 of 40 FA944132 Summary of Hits Page 2 of 2 Job Number:FA94413 Account:GRI (Geological Resources Inc.) Project:Sam's Pit Stop; 4236 Sam Potts Hwy, Hallsboro, NC Collected:03/29/22 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method sec-Butylbenzene 0.87 0.50 0.13 ug/l SM 6200B tert-Butylbenzene 0.39 J 0.50 0.13 ug/l SM 6200B Ethylbenzene 5.9 0.50 0.13 ug/l SM 6200B Isopropylbenzene 3.1 0.50 0.13 ug/l SM 6200B p-Isopropyltoluene 0.85 0.50 0.13 ug/l SM 6200B n-Propylbenzene 1.9 0.50 0.13 ug/l SM 6200B Tert-Amyl Alcohol 246 10 2.0 ug/l SM 6200B Toluene 10.2 0.50 0.13 ug/l SM 6200B 1,2,4-Trimethylbenzene 0.65 0.50 0.13 ug/l SM 6200B 1,3,5-Trimethylbenzene 1.3 0.50 0.13 ug/l SM 6200B m,p-Xylene 31.4 1.0 0.13 ug/l SM 6200B o-Xylene 1.9 0.50 0.13 ug/l SM 6200B Xylene (total)33.3 1.5 0.25 ug/l SM 6200B FA94413-6 MW-13 Methyl Bromide 0.35 J 0.50 0.20 ug/l SM 6200B Methyl Chloride 0.55 0.50 0.20 ug/l SM 6200B (a) Associated Initial Calibration outside control limits (%RSD > 15%). 5 of 40 FA944132 SGS North America Inc. Sample Results Report of Analysis Orlando, FL Section 3 6 of 40 FA944133 SGS North America Inc. Report of Analysis Page 1 of 3 Client Sample ID:MW-1 Lab Sample ID:FA94413-1 Date Sampled:03/29/22 Matrix:AQ - Ground Water Date Received:03/30/22 Method:SM 6200B Percent Solids:n/a Project:Sam's Pit Stop; 4236 Sam Potts Hwy, Hallsboro, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 A0231524.D 1 04/08/22 18:21 SS n/a n/a VA3109 Run #2 A0231603.D 2 04/12/22 17:18 SS n/a n/a VA3112 Purge Volume Run #1 10.0 ml Run #2 10.0 ml VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene 54.7 a 1.0 0.25 ug/l 108-86-1 Bromobenzene ND 0.50 0.13 ug/l 74-97-5 Bromochloromethane ND 0.50 0.13 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l 75-25-2 Bromoform ND 0.50 0.13 ug/l 104-51-8 n-Butylbenzene 1.7 0.50 0.13 ug/l 135-98-8 sec-Butylbenzene 1.9 0.50 0.13 ug/l 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane b 0.52 a 1.0 0.40 ug/l J 67-66-3 Chloroform ND 0.50 0.13 ug/l 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l 75-71-8 Dichlorodifluoromethane ND a 1.0 0.40 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l 75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l 563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 7 of 40 FA9441333.1 SGS North America Inc. Report of Analysis Page 2 of 3 Client Sample ID:MW-1 Lab Sample ID:FA94413-1 Date Sampled:03/29/22 Matrix:AQ - Ground Water Date Received:03/30/22 Method:SM 6200B Percent Solids:n/a Project:Sam's Pit Stop; 4236 Sam Potts Hwy, Hallsboro, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether 0.15 0.50 0.13 ug/l J 100-41-4 Ethylbenzene 3.6 0.50 0.13 ug/l 637-92-3 Ethyl Tert Butyl Ether 3.7 0.50 0.13 ug/l 87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l 98-82-8 Isopropylbenzene 23.2 0.50 0.13 ug/l 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l 74-83-9 Methyl Bromide ND 0.50 0.20 ug/l 74-87-3 Methyl Chloride 1.5 a 1.0 0.40 ug/l 74-95-3 Methylene Bromide ND 0.50 0.13 ug/l 75-09-2 Methylene Chloride ND 2.0 1.0 ug/l 1634-04-4 Methyl Tert Butyl Ether 3.8 0.50 0.13 ug/l 91-20-3 Naphthalene 0.80 0.50 0.13 ug/l 103-65-1 n-Propylbenzene 45.5 a 1.0 0.25 ug/l 100-42-5 Styrene ND 0.50 0.13 ug/l 75-85-4 Tert-Amyl Alcohol 75.2 10 2.0 ug/l 994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l 75-65-0 Tert-Butyl Alcohol 59.4 10 2.0 ug/l 762-75-4 Tert-Butyl Formate ND 10 2.0 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l 108-88-3 Toluene 2.1 0.50 0.13 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l 71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l 79-01-6 Trichloroethylene ND 0.50 0.13 ug/l 75-69-4 Trichlorofluoromethane c ND 0.50 0.20 ug/l 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l 95-63-6 1,2,4-Trimethylbenzene 0.39 0.50 0.13 ug/l J 108-67-8 1,3,5-Trimethylbenzene 0.22 0.50 0.13 ug/l J 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l m,p-Xylene 9.6 1.0 0.13 ug/l 95-47-6 o-Xylene 1.4 0.50 0.13 ug/l 1330-20-7 Xylene (total)11.0 1.5 0.25 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 99%107%70-130% 17060-07-0 1,2-Dichloroethane-D4 105%110%70-130% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 8 of 40 FA9441333.1 SGS North America Inc. Report of Analysis Page 3 of 3 Client Sample ID:MW-1 Lab Sample ID:FA94413-1 Date Sampled:03/29/22 Matrix:AQ - Ground Water Date Received:03/30/22 Method:SM 6200B Percent Solids:n/a Project:Sam's Pit Stop; 4236 Sam Potts Hwy, Hallsboro, NC VOA 6200B List CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 2037-26-5 Toluene-D8 99%97%70-130% 460-00-4 4-Bromofluorobenzene 101%100%70-130% (a) Result is from Run# 2 (b) Associated Initial Calibration outside control limits (%RSD > 15%). (c) Associated CCV outside control limits low. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 9 of 40 FA9441333.1 SGS North America Inc. Report of Analysis Page 1 of 3 Client Sample ID:MW-4 Lab Sample ID:FA94413-2 Date Sampled:03/29/22 Matrix:AQ - Ground Water Date Received:03/30/22 Method:SM 6200B Percent Solids:n/a Project:Sam's Pit Stop; 4236 Sam Potts Hwy, Hallsboro, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 A0231525.D 1 04/08/22 18:43 SS n/a n/a VA3109 Run #2 A0231598.D 1 04/12/22 15:21 SS n/a n/a VA3112 Purge Volume Run #1 10.0 ml Run #2 10.0 ml VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.13 ug/l 108-86-1 Bromobenzene ND 0.50 0.13 ug/l 74-97-5 Bromochloromethane ND 0.50 0.13 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l 75-25-2 Bromoform ND 0.50 0.13 ug/l 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane a ND 0.50 0.20 ug/l 67-66-3 Chloroform ND 0.50 0.13 ug/l 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l 75-71-8 Dichlorodifluoromethane ND b 0.50 0.20 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l 75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l 563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 10 of 40 FA9441333.2 SGS North America Inc. Report of Analysis Page 2 of 3 Client Sample ID:MW-4 Lab Sample ID:FA94413-2 Date Sampled:03/29/22 Matrix:AQ - Ground Water Date Received:03/30/22 Method:SM 6200B Percent Solids:n/a Project:Sam's Pit Stop; 4236 Sam Potts Hwy, Hallsboro, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l 100-41-4 Ethylbenzene ND 0.50 0.13 ug/l 637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l 87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l 74-83-9 Methyl Bromide 0.30 0.50 0.20 ug/l J 74-87-3 Methyl Chloride 0.55 0.50 0.20 ug/l 74-95-3 Methylene Bromide ND 0.50 0.13 ug/l 75-09-2 Methylene Chloride ND 2.0 1.0 ug/l 1634-04-4 Methyl Tert Butyl Ether 0.77 0.50 0.13 ug/l 91-20-3 Naphthalene ND 0.50 0.13 ug/l 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l 100-42-5 Styrene ND 0.50 0.13 ug/l 75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l 994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l 75-65-0 Tert-Butyl Alcohol 2.8 10 2.0 ug/l J 762-75-4 Tert-Butyl Formate ND 10 2.0 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l 108-88-3 Toluene ND 0.50 0.13 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l 71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l 79-01-6 Trichloroethylene ND 0.50 0.13 ug/l 75-69-4 Trichlorofluoromethane c ND 0.50 0.20 ug/l 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l m,p-Xylene ND 1.0 0.13 ug/l 95-47-6 o-Xylene ND 0.50 0.13 ug/l 1330-20-7 Xylene (total)ND 1.5 0.25 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 103%108%70-130% 17060-07-0 1,2-Dichloroethane-D4 104%107%70-130% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 11 of 40 FA9441333.2 SGS North America Inc. Report of Analysis Page 3 of 3 Client Sample ID:MW-4 Lab Sample ID:FA94413-2 Date Sampled:03/29/22 Matrix:AQ - Ground Water Date Received:03/30/22 Method:SM 6200B Percent Solids:n/a Project:Sam's Pit Stop; 4236 Sam Potts Hwy, Hallsboro, NC VOA 6200B List CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 2037-26-5 Toluene-D8 98%97%70-130% 460-00-4 4-Bromofluorobenzene 98%97%70-130% (a) Associated Initial Calibration outside control limits (%RSD > 15%); sample is ND. (b) Result is from Run# 2 (c) Associated CCV outside control limits low. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 12 of 40 FA9441333.2 SGS North America Inc. Report of Analysis Page 1 of 3 Client Sample ID:MW-7 Lab Sample ID:FA94413-3 Date Sampled:03/29/22 Matrix:AQ - Ground Water Date Received:03/30/22 Method:SM 6200B Percent Solids:n/a Project:Sam's Pit Stop; 4236 Sam Potts Hwy, Hallsboro, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 A0231526.D 1 04/08/22 19:06 SS n/a n/a VA3109 Run #2 A0231599.D 1 04/12/22 15:44 SS n/a n/a VA3112 Purge Volume Run #1 10.0 ml Run #2 10.0 ml VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.13 ug/l 108-86-1 Bromobenzene ND 0.50 0.13 ug/l 74-97-5 Bromochloromethane ND 0.50 0.13 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l 75-25-2 Bromoform ND 0.50 0.13 ug/l 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane a ND 0.50 0.20 ug/l 67-66-3 Chloroform ND 0.50 0.13 ug/l 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l 75-71-8 Dichlorodifluoromethane ND b 0.50 0.20 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l 75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l 563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 13 of 40 FA9441333.3 SGS North America Inc. Report of Analysis Page 2 of 3 Client Sample ID:MW-7 Lab Sample ID:FA94413-3 Date Sampled:03/29/22 Matrix:AQ - Ground Water Date Received:03/30/22 Method:SM 6200B Percent Solids:n/a Project:Sam's Pit Stop; 4236 Sam Potts Hwy, Hallsboro, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l 100-41-4 Ethylbenzene ND 0.50 0.13 ug/l 637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l 87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l 74-83-9 Methyl Bromide 0.46 0.50 0.20 ug/l J 74-87-3 Methyl Chloride 1.1 0.50 0.20 ug/l 74-95-3 Methylene Bromide ND 0.50 0.13 ug/l 75-09-2 Methylene Chloride ND 2.0 1.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l 91-20-3 Naphthalene ND 0.50 0.13 ug/l 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l 100-42-5 Styrene ND 0.50 0.13 ug/l 75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l 994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l 75-65-0 Tert-Butyl Alcohol ND 10 2.0 ug/l 762-75-4 Tert-Butyl Formate ND 10 2.0 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l 108-88-3 Toluene ND 0.50 0.13 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l 71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l 79-01-6 Trichloroethylene ND 0.50 0.13 ug/l 75-69-4 Trichlorofluoromethane c ND 0.50 0.20 ug/l 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l m,p-Xylene ND 1.0 0.13 ug/l 95-47-6 o-Xylene ND 0.50 0.13 ug/l 1330-20-7 Xylene (total)ND 1.5 0.25 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 105%108%70-130% 17060-07-0 1,2-Dichloroethane-D4 106%108%70-130% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 14 of 40 FA9441333.3 SGS North America Inc. Report of Analysis Page 3 of 3 Client Sample ID:MW-7 Lab Sample ID:FA94413-3 Date Sampled:03/29/22 Matrix:AQ - Ground Water Date Received:03/30/22 Method:SM 6200B Percent Solids:n/a Project:Sam's Pit Stop; 4236 Sam Potts Hwy, Hallsboro, NC VOA 6200B List CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 2037-26-5 Toluene-D8 94%93%70-130% 460-00-4 4-Bromofluorobenzene 98%95%70-130% (a) Associated Initial Calibration outside control limits (%RSD > 15%); sample is ND. (b) Result is from Run# 2 (c) Associated CCV outside control limits low. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 15 of 40 FA9441333.3 SGS North America Inc. Report of Analysis Page 1 of 3 Client Sample ID:MW-8 Lab Sample ID:FA94413-4 Date Sampled:03/29/22 Matrix:AQ - Ground Water Date Received:03/30/22 Method:SM 6200B Percent Solids:n/a Project:Sam's Pit Stop; 4236 Sam Potts Hwy, Hallsboro, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 A0231527.D 1 04/08/22 19:29 SS n/a n/a VA3109 Run #2 A0231600.D 1 04/12/22 16:07 SS n/a n/a VA3112 Purge Volume Run #1 10.0 ml Run #2 10.0 ml VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.13 ug/l 108-86-1 Bromobenzene ND 0.50 0.13 ug/l 74-97-5 Bromochloromethane ND 0.50 0.13 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l 75-25-2 Bromoform ND 0.50 0.13 ug/l 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane a ND 0.50 0.20 ug/l 67-66-3 Chloroform ND 0.50 0.13 ug/l 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l 75-71-8 Dichlorodifluoromethane ND b 0.50 0.20 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l 75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l 563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 16 of 40 FA9441333.4 SGS North America Inc. Report of Analysis Page 2 of 3 Client Sample ID:MW-8 Lab Sample ID:FA94413-4 Date Sampled:03/29/22 Matrix:AQ - Ground Water Date Received:03/30/22 Method:SM 6200B Percent Solids:n/a Project:Sam's Pit Stop; 4236 Sam Potts Hwy, Hallsboro, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l 100-41-4 Ethylbenzene ND 0.50 0.13 ug/l 637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l 87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l 74-83-9 Methyl Bromide 0.34 0.50 0.20 ug/l J 74-87-3 Methyl Chloride 0.46 0.50 0.20 ug/l J 74-95-3 Methylene Bromide ND 0.50 0.13 ug/l 75-09-2 Methylene Chloride ND 2.0 1.0 ug/l 1634-04-4 Methyl Tert Butyl Ether 0.18 0.50 0.13 ug/l J 91-20-3 Naphthalene ND 0.50 0.13 ug/l 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l 100-42-5 Styrene ND 0.50 0.13 ug/l 75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l 994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l 75-65-0 Tert-Butyl Alcohol ND 10 2.0 ug/l 762-75-4 Tert-Butyl Formate ND 10 2.0 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l 108-88-3 Toluene ND 0.50 0.13 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l 71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l 79-01-6 Trichloroethylene ND 0.50 0.13 ug/l 75-69-4 Trichlorofluoromethane c ND 0.50 0.20 ug/l 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l m,p-Xylene ND 1.0 0.13 ug/l 95-47-6 o-Xylene ND 0.50 0.13 ug/l 1330-20-7 Xylene (total)ND 1.5 0.25 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 104%109%70-130% 17060-07-0 1,2-Dichloroethane-D4 106%110%70-130% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 17 of 40 FA9441333.4 SGS North America Inc. Report of Analysis Page 3 of 3 Client Sample ID:MW-8 Lab Sample ID:FA94413-4 Date Sampled:03/29/22 Matrix:AQ - Ground Water Date Received:03/30/22 Method:SM 6200B Percent Solids:n/a Project:Sam's Pit Stop; 4236 Sam Potts Hwy, Hallsboro, NC VOA 6200B List CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 2037-26-5 Toluene-D8 99%99%70-130% 460-00-4 4-Bromofluorobenzene 98%97%70-130% (a) Associated Initial Calibration outside control limits (%RSD > 15%); sample is ND. (b) Result is from Run# 2 (c) Associated CCV outside control limits low. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 18 of 40 FA9441333.4 SGS North America Inc. Report of Analysis Page 1 of 3 Client Sample ID:MW-9 Lab Sample ID:FA94413-5 Date Sampled:03/29/22 Matrix:AQ - Ground Water Date Received:03/30/22 Method:SM 6200B Percent Solids:n/a Project:Sam's Pit Stop; 4236 Sam Potts Hwy, Hallsboro, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 A0231528.D 1 04/08/22 19:52 SS n/a n/a VA3109 Run #2 A0231604.D 5 04/12/22 17:41 SS n/a n/a VA3112 Purge Volume Run #1 10.0 ml Run #2 10.0 ml VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene 104 a 2.5 0.63 ug/l 108-86-1 Bromobenzene ND 0.50 0.13 ug/l 74-97-5 Bromochloromethane ND 0.50 0.13 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l 75-25-2 Bromoform ND 0.50 0.13 ug/l 104-51-8 n-Butylbenzene 0.37 0.50 0.13 ug/l J 135-98-8 sec-Butylbenzene 0.87 0.50 0.13 ug/l 98-06-6 tert-Butylbenzene 0.39 0.50 0.13 ug/l J 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane b ND 0.50 0.20 ug/l 67-66-3 Chloroform ND 0.50 0.13 ug/l 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l 75-71-8 Dichlorodifluoromethane ND a 2.5 1.0 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l 75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l 563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 19 of 40 FA9441333.5 SGS North America Inc. Report of Analysis Page 2 of 3 Client Sample ID:MW-9 Lab Sample ID:FA94413-5 Date Sampled:03/29/22 Matrix:AQ - Ground Water Date Received:03/30/22 Method:SM 6200B Percent Solids:n/a Project:Sam's Pit Stop; 4236 Sam Potts Hwy, Hallsboro, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l 100-41-4 Ethylbenzene 5.9 0.50 0.13 ug/l 637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l 87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l 98-82-8 Isopropylbenzene 3.1 0.50 0.13 ug/l 99-87-6 p-Isopropyltoluene 0.85 0.50 0.13 ug/l 74-83-9 Methyl Bromide ND 0.50 0.20 ug/l 74-87-3 Methyl Chloride ND 0.50 0.20 ug/l 74-95-3 Methylene Bromide ND 0.50 0.13 ug/l 75-09-2 Methylene Chloride ND 2.0 1.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l 91-20-3 Naphthalene ND 0.50 0.13 ug/l 103-65-1 n-Propylbenzene 1.9 0.50 0.13 ug/l 100-42-5 Styrene ND 0.50 0.13 ug/l 75-85-4 Tert-Amyl Alcohol 246 10 2.0 ug/l 994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l 75-65-0 Tert-Butyl Alcohol ND 10 2.0 ug/l 762-75-4 Tert-Butyl Formate ND 10 2.0 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l 108-88-3 Toluene 10.2 0.50 0.13 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l 71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l 79-01-6 Trichloroethylene ND 0.50 0.13 ug/l 75-69-4 Trichlorofluoromethane c ND 0.50 0.20 ug/l 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l 95-63-6 1,2,4-Trimethylbenzene 0.65 0.50 0.13 ug/l 108-67-8 1,3,5-Trimethylbenzene 1.3 0.50 0.13 ug/l 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l m,p-Xylene 31.4 1.0 0.13 ug/l 95-47-6 o-Xylene 1.9 0.50 0.13 ug/l 1330-20-7 Xylene (total)33.3 1.5 0.25 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 99%105%70-130% 17060-07-0 1,2-Dichloroethane-D4 105%108%70-130% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 20 of 40 FA9441333.5 SGS North America Inc. Report of Analysis Page 3 of 3 Client Sample ID:MW-9 Lab Sample ID:FA94413-5 Date Sampled:03/29/22 Matrix:AQ - Ground Water Date Received:03/30/22 Method:SM 6200B Percent Solids:n/a Project:Sam's Pit Stop; 4236 Sam Potts Hwy, Hallsboro, NC VOA 6200B List CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 2037-26-5 Toluene-D8 103%99%70-130% 460-00-4 4-Bromofluorobenzene 108%102%70-130% (a) Result is from Run# 2 (b) Associated Initial Calibration outside control limits (%RSD > 15%); sample is ND. (c) Associated CCV outside control limits low. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 21 of 40 FA9441333.5 SGS North America Inc. Report of Analysis Page 1 of 3 Client Sample ID:MW-13 Lab Sample ID:FA94413-6 Date Sampled:03/29/22 Matrix:AQ - Ground Water Date Received:03/30/22 Method:SM 6200B Percent Solids:n/a Project:Sam's Pit Stop; 4236 Sam Potts Hwy, Hallsboro, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 A0231531.D 1 04/08/22 21:00 SS n/a n/a VA3109 Run #2 A0231601.D 1 04/12/22 16:31 SS n/a n/a VA3112 Purge Volume Run #1 10.0 ml Run #2 10.0 ml VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.13 ug/l 108-86-1 Bromobenzene ND 0.50 0.13 ug/l 74-97-5 Bromochloromethane ND 0.50 0.13 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l 75-25-2 Bromoform ND 0.50 0.13 ug/l 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane a ND 0.50 0.20 ug/l 67-66-3 Chloroform ND 0.50 0.13 ug/l 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l 75-71-8 Dichlorodifluoromethane ND b 0.50 0.20 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l 75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l 563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 22 of 40 FA9441333.6 SGS North America Inc. Report of Analysis Page 2 of 3 Client Sample ID:MW-13 Lab Sample ID:FA94413-6 Date Sampled:03/29/22 Matrix:AQ - Ground Water Date Received:03/30/22 Method:SM 6200B Percent Solids:n/a Project:Sam's Pit Stop; 4236 Sam Potts Hwy, Hallsboro, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l 100-41-4 Ethylbenzene ND 0.50 0.13 ug/l 637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l 87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l 74-83-9 Methyl Bromide 0.35 0.50 0.20 ug/l J 74-87-3 Methyl Chloride 0.55 0.50 0.20 ug/l 74-95-3 Methylene Bromide ND 0.50 0.13 ug/l 75-09-2 Methylene Chloride ND 2.0 1.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l 91-20-3 Naphthalene ND 0.50 0.13 ug/l 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l 100-42-5 Styrene ND 0.50 0.13 ug/l 75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l 994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l 75-65-0 Tert-Butyl Alcohol ND 10 2.0 ug/l 762-75-4 Tert-Butyl Formate ND 10 2.0 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l 108-88-3 Toluene ND 0.50 0.13 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l 71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l 79-01-6 Trichloroethylene ND 0.50 0.13 ug/l 75-69-4 Trichlorofluoromethane c ND 0.50 0.20 ug/l 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l m,p-Xylene ND 1.0 0.13 ug/l 95-47-6 o-Xylene ND 0.50 0.13 ug/l 1330-20-7 Xylene (total)ND 1.5 0.25 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 104%110%70-130% 17060-07-0 1,2-Dichloroethane-D4 105%109%70-130% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 23 of 40 FA9441333.6 SGS North America Inc. Report of Analysis Page 3 of 3 Client Sample ID:MW-13 Lab Sample ID:FA94413-6 Date Sampled:03/29/22 Matrix:AQ - Ground Water Date Received:03/30/22 Method:SM 6200B Percent Solids:n/a Project:Sam's Pit Stop; 4236 Sam Potts Hwy, Hallsboro, NC VOA 6200B List CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 2037-26-5 Toluene-D8 95%94%70-130% 460-00-4 4-Bromofluorobenzene 97%95%70-130% (a) Associated Initial Calibration outside control limits (%RSD > 15%); sample is ND. (b) Result is from Run# 2 (c) Associated CCV outside control limits low. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 24 of 40 FA9441333.6 SGS North America Inc. Misc. Forms Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody Orlando, FL Section 4 25 of 40 FA944134 FA94413: Chain of Custody Page 1 of 2 26 of 40 FA9441344.1 Job Number:FA94413 Client:GEOLOGICAL RESOURCES, INC Date / Time Received:3/30/2022 9:30:00 AM Delivery Method:FEDEX Project:SAM'S PIT STOP Airbill #'s:1009 6379 5983 Cooler Information 1. Custody Seals Present 2. Custody Seals Intact 4. Cooler temp verification 3. Temp criteria achieved 5. Cooler media IR Gun Ice (Bag) Trip Blank Information 1. Trip Blank present / cooler 2. Trip Blank listed on COC 2. Samples preserved properly Sample Information 1. Sample labels present on bottles 5. Sample recvd within HT 4. Condition of sample 3. Sufficient volume/containers recvd for analysis: Intact Comments SM001Rev. Date 05/24/17 SGS Sample Receipt Summary Cooler Temps (Raw Measured) °C: Cooler Temps (Corrected) °C: Cooler 1: (2.8); Cooler 1: (3.2); 3. Type Of TB Received W or S N/A 6. Dates/Times/IDs on COC match Sample Label 7. VOCs have headspace 8. Bottles received for unspecified tests 9. Compositing instructions clear 10. Voa Soil Kits/Jars received past 48hrs? 11. % Solids Jar received? Misc. Information 25-Gram 5-GramNumber of Encores:Number of 5035 Field Kits:Number of Lab Filtered Metals: Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify) Y or N N/A Y or N Therm ID:IR 1; Therm CF:0.4; # of Coolers:1 Y or N N/A 12. Residual Chlorine Present? Residual Chlorine Test Strip Lot #: Technician:Reviewer:SAMUELM Date:Date:3/30/2022 9:30:00 AM FA94413: Chain of Custody Page 2 of 2 27 of 40 FA9441344.1 SGS North America Inc. MS Volatiles QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries Orlando, FL Section 5 28 of 40 FA944135 Method Blank Summary Page 1 of 3 Job Number:FA94413 Account:GRINCC GRI (Geological Resources Inc.) Project:Sam's Pit Stop; 4236 Sam Potts Hwy, Hallsboro, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VA3109-MB A0231518.D 1 04/08/22 SS n/a n/a VA3109 The QC reported here applies to the following samples:Method: SM 6200B FA94413-1, FA94413-2, FA94413-3, FA94413-4, FA94413-5, FA94413-6 CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.13 ug/l 108-86-1 Bromobenzene ND 0.50 0.13 ug/l 74-97-5 Bromochloromethane ND 0.50 0.13 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l 75-25-2 Bromoform ND 0.50 0.13 ug/l 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane ND 0.50 0.20 ug/l 67-66-3 Chloroform ND 0.50 0.13 ug/l 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l 75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l 563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l 108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l 100-41-4 Ethylbenzene ND 0.50 0.13 ug/l 637-92-3 Ethyl Tert Butyl Ether ND 0.50 0.13 ug/l 87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l 29 of 40 FA9441355.1.1 Method Blank Summary Page 2 of 3 Job Number:FA94413 Account:GRINCC GRI (Geological Resources Inc.) Project:Sam's Pit Stop; 4236 Sam Potts Hwy, Hallsboro, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VA3109-MB A0231518.D 1 04/08/22 SS n/a n/a VA3109 The QC reported here applies to the following samples:Method: SM 6200B FA94413-1, FA94413-2, FA94413-3, FA94413-4, FA94413-5, FA94413-6 CAS No.Compound Result RL MDL Units Q 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l 74-83-9 Methyl Bromide ND 0.50 0.20 ug/l 74-87-3 Methyl Chloride ND 0.50 0.20 ug/l 74-95-3 Methylene Bromide ND 0.50 0.13 ug/l 75-09-2 Methylene Chloride ND 2.0 1.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l 91-20-3 Naphthalene ND 0.50 0.13 ug/l 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l 100-42-5 Styrene ND 0.50 0.13 ug/l 75-85-4 Tert-Amyl Alcohol ND 10 2.0 ug/l 994-05-8 Tert-Amyl Methyl Ether ND 1.0 0.20 ug/l 75-65-0 Tert-Butyl Alcohol ND 10 2.0 ug/l 762-75-4 Tert-Butyl Formate ND 10 2.0 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l 108-88-3 Toluene ND 0.50 0.13 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l 71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l 79-01-6 Trichloroethylene ND 0.50 0.13 ug/l 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l m,p-Xylene ND 1.0 0.13 ug/l 95-47-6 o-Xylene ND 0.50 0.13 ug/l 1330-20-7 Xylene (total)ND 1.5 0.25 ug/l CAS No.Surrogate Recoveries Limits 1868-53-7 Dibromofluoromethane 104%70-130% 17060-07-0 1,2-Dichloroethane-D4 104%70-130% 30 of 40 FA9441355.1.1 Method Blank Summary Page 3 of 3 Job Number:FA94413 Account:GRINCC GRI (Geological Resources Inc.) Project:Sam's Pit Stop; 4236 Sam Potts Hwy, Hallsboro, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VA3109-MB A0231518.D 1 04/08/22 SS n/a n/a VA3109 The QC reported here applies to the following samples:Method: SM 6200B FA94413-1, FA94413-2, FA94413-3, FA94413-4, FA94413-5, FA94413-6 CAS No.Surrogate Recoveries Limits 2037-26-5 Toluene-D8 101%70-130% 460-00-4 4-Bromofluorobenzene 98%70-130% 31 of 40 FA9441355.1.1 Method Blank Summary Page 1 of 1 Job Number:FA94413 Account:GRINCC GRI (Geological Resources Inc.) Project:Sam's Pit Stop; 4236 Sam Potts Hwy, Hallsboro, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VA3112-MB A0231596.D 1 04/12/22 SS n/a n/a VA3112 The QC reported here applies to the following samples:Method: SM 6200B FA94413-1, FA94413-2, FA94413-3, FA94413-4, FA94413-5, FA94413-6 CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane ND 0.50 0.20 ug/l 75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l 74-87-3 Methyl Chloride ND 0.50 0.20 ug/l 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l CAS No.Surrogate Recoveries Limits 1868-53-7 Dibromofluoromethane 106%70-130% 17060-07-0 1,2-Dichloroethane-D4 107%70-130% 2037-26-5 Toluene-D8 99%70-130% 460-00-4 4-Bromofluorobenzene 95%70-130% 32 of 40 FA9441355.1.2 Blank Spike Summary Page 1 of 3 Job Number:FA94413 Account:GRINCC GRI (Geological Resources Inc.) Project:Sam's Pit Stop; 4236 Sam Potts Hwy, Hallsboro, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VA3109-BS A0231516.D 1 04/08/22 SS n/a n/a VA3109 The QC reported here applies to the following samples:Method: SM 6200B FA94413-1, FA94413-2, FA94413-3, FA94413-4, FA94413-5, FA94413-6 Spike BSP BSP CAS No.Compound ug/l ug/l %Limits 71-43-2 Benzene 10 10.1 101 70-130 108-86-1 Bromobenzene 10 9.1 91 70-130 74-97-5 Bromochloromethane 10 8.6 86 70-130 75-27-4 Bromodichloromethane 10 9.3 93 70-130 75-25-2 Bromoform 10 7.7 77 70-130 104-51-8 n-Butylbenzene 10 9.8 98 70-130 135-98-8 sec-Butylbenzene 10 10.4 104 70-130 98-06-6 tert-Butylbenzene 10 9.9 99 70-130 56-23-5 Carbon Tetrachloride 10 10.1 101 70-130 108-90-7 Chlorobenzene 10 9.3 93 70-130 75-00-3 Chloroethane 10 9.6 96 60-140 67-66-3 Chloroform 10 9.3 93 70-130 95-49-8 o-Chlorotoluene 10 9.5 95 70-130 106-43-4 p-Chlorotoluene 10 9.5 95 70-130 124-48-1 Dibromochloromethane 10 8.6 86 70-130 96-12-8 1,2-Dibromo-3-chloropropane 10 8.6 86 70-130 106-93-4 1,2-Dibromoethane 10 9.1 91 70-130 95-50-1 1,2-Dichlorobenzene 10 9.1 91 70-130 541-73-1 1,3-Dichlorobenzene 10 9.4 94 70-130 106-46-7 1,4-Dichlorobenzene 10 9.3 93 70-130 75-34-3 1,1-Dichloroethane 10 10.1 101 70-130 107-06-2 1,2-Dichloroethane 10 9.5 95 70-130 75-35-4 1,1-Dichloroethylene 10 10.6 106 70-130 156-59-2 cis-1,2-Dichloroethylene 10 9.8 98 70-130 156-60-5 trans-1,2-Dichloroethylene 10 10.3 103 70-130 78-87-5 1,2-Dichloropropane 10 9.6 96 70-130 142-28-9 1,3-Dichloropropane 10 9.0 90 70-130 594-20-7 2,2-Dichloropropane 10 10.9 109 70-130 563-58-6 1,1-Dichloropropene 10 10.3 103 70-130 10061-01-5 cis-1,3-Dichloropropene 10 9.7 97 70-130 10061-02-6 trans-1,3-Dichloropropene 10 9.6 96 70-130 108-20-3 Di-Isopropyl Ether 10 9.6 96 70-130 100-41-4 Ethylbenzene 10 9.8 98 70-130 637-92-3 Ethyl Tert Butyl Ether 10 8.3 83 70-130 87-68-3 Hexachlorobutadiene 10 10.1 101 70-130 98-82-8 Isopropylbenzene 10 10.1 101 70-130 * = Outside of Control Limits. 33 of 40 FA9441355.2.1 Blank Spike Summary Page 2 of 3 Job Number:FA94413 Account:GRINCC GRI (Geological Resources Inc.) Project:Sam's Pit Stop; 4236 Sam Potts Hwy, Hallsboro, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VA3109-BS A0231516.D 1 04/08/22 SS n/a n/a VA3109 The QC reported here applies to the following samples:Method: SM 6200B FA94413-1, FA94413-2, FA94413-3, FA94413-4, FA94413-5, FA94413-6 Spike BSP BSP CAS No.Compound ug/l ug/l %Limits 99-87-6 p-Isopropyltoluene 10 10.2 102 70-130 74-83-9 Methyl Bromide 10 10.7 107 60-140 74-87-3 Methyl Chloride 10 9.9 99 60-140 74-95-3 Methylene Bromide 10 8.7 87 70-130 75-09-2 Methylene Chloride 10 9.6 96 70-130 1634-04-4 Methyl Tert Butyl Ether 10 9.3 93 70-130 91-20-3 Naphthalene 10 8.5 85 70-130 103-65-1 n-Propylbenzene 10 9.8 98 70-130 100-42-5 Styrene 10 8.9 89 70-130 75-85-4 Tert-Amyl Alcohol 100 87.2 87 70-130 994-05-8 Tert-Amyl Methyl Ether 10 8.4 84 70-130 75-65-0 Tert-Butyl Alcohol 100 100 100 70-130 762-75-4 Tert-Butyl Formate 100 88.3 88 70-130 630-20-6 1,1,1,2-Tetrachloroethane 10 9.4 94 70-130 79-34-5 1,1,2,2-Tetrachloroethane 10 9.1 91 70-130 127-18-4 Tetrachloroethylene 10 9.6 96 70-130 108-88-3 Toluene 10 9.7 97 70-130 87-61-6 1,2,3-Trichlorobenzene 10 9.4 94 70-130 120-82-1 1,2,4-Trichlorobenzene 10 9.4 94 70-130 71-55-6 1,1,1-Trichloroethane 10 9.8 98 70-130 79-00-5 1,1,2-Trichloroethane 10 9.2 92 70-130 79-01-6 Trichloroethylene 10 9.8 98 70-130 75-69-4 Trichlorofluoromethane 10 9.2 92 60-140 96-18-4 1,2,3-Trichloropropane 10 8.7 87 70-130 95-63-6 1,2,4-Trimethylbenzene 10 9.8 98 70-130 108-67-8 1,3,5-Trimethylbenzene 10 9.9 99 70-130 75-01-4 Vinyl Chloride 10 8.7 87 60-140 m,p-Xylene 20 19.8 99 70-130 95-47-6 o-Xylene 10 9.8 98 70-130 1330-20-7 Xylene (total)30 29.6 99 70-130 CAS No.Surrogate Recoveries BSP Limits 1868-53-7 Dibromofluoromethane 101%70-130% 17060-07-0 1,2-Dichloroethane-D4 101%70-130% * = Outside of Control Limits. 34 of 40 FA9441355.2.1 Blank Spike Summary Page 3 of 3 Job Number:FA94413 Account:GRINCC GRI (Geological Resources Inc.) Project:Sam's Pit Stop; 4236 Sam Potts Hwy, Hallsboro, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VA3109-BS A0231516.D 1 04/08/22 SS n/a n/a VA3109 The QC reported here applies to the following samples:Method: SM 6200B FA94413-1, FA94413-2, FA94413-3, FA94413-4, FA94413-5, FA94413-6 CAS No.Surrogate Recoveries BSP Limits 2037-26-5 Toluene-D8 100%70-130% 460-00-4 4-Bromofluorobenzene 98%70-130% * = Outside of Control Limits. 35 of 40 FA9441355.2.1 Blank Spike Summary Page 1 of 1 Job Number:FA94413 Account:GRINCC GRI (Geological Resources Inc.) Project:Sam's Pit Stop; 4236 Sam Potts Hwy, Hallsboro, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VA3112-BS A0231594.D 1 04/12/22 SS n/a n/a VA3112 The QC reported here applies to the following samples:Method: SM 6200B FA94413-1, FA94413-2, FA94413-3, FA94413-4, FA94413-5, FA94413-6 Spike BSP BSP CAS No.Compound ug/l ug/l %Limits 71-43-2 Benzene 10 10.4 104 70-130 75-00-3 Chloroethane 10 14.1 141*60-140 75-71-8 Dichlorodifluoromethane 10 6.7 67 60-140 74-87-3 Methyl Chloride 10 9.7 97 60-140 103-65-1 n-Propylbenzene 10 10.1 101 70-130 CAS No.Surrogate Recoveries BSP Limits 1868-53-7 Dibromofluoromethane 106%70-130% 17060-07-0 1,2-Dichloroethane-D4 102%70-130% 2037-26-5 Toluene-D8 99%70-130% 460-00-4 4-Bromofluorobenzene 97%70-130% * = Outside of Control Limits. 36 of 40 FA9441355.2.2 Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3 Job Number:FA94413 Account:GRINCC GRI (Geological Resources Inc.) Project:Sam's Pit Stop; 4236 Sam Potts Hwy, Hallsboro, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA94581-1MS A0231541.D 500 04/09/22 SS n/a n/a VA3109 FA94581-1MSD A0231542.D 500 04/09/22 SS n/a n/a VA3109 FA94581-1 A0231538.D 500 04/08/22 SS n/a n/a VA3109 The QC reported here applies to the following samples:Method: SM 6200B FA94413-1, FA94413-2, FA94413-3, FA94413-4, FA94413-5, FA94413-6 FA94581-1 Spike MS MS Spike MSD MSD Limits CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD 71-43-2 Benzene 123 J 5000 5640 110 5000 5430 106 4 70-130/20 108-86-1 Bromobenzene ND 5000 4900 98 5000 4740 95 3 70-130/20 74-97-5 Bromochloromethane ND 5000 4680 94 5000 4510 90 4 70-130/20 75-27-4 Bromodichloromethane ND 5000 5250 105 5000 5010 100 5 70-130/20 75-25-2 Bromoform ND 5000 4240 85 5000 4020 80 5 70-130/20 104-51-8 n-Butylbenzene ND 5000 4800 96 5000 4570 91 5 70-130/20 135-98-8 sec-Butylbenzene ND 5000 5250 105 5000 5040 101 4 70-130/20 98-06-6 tert-Butylbenzene ND 5000 5150 103 5000 4910 98 5 70-130/20 56-23-5 Carbon Tetrachloride ND 5000 4890 98 5000 4740 95 3 70-130/20 108-90-7 Chlorobenzene ND 5000 5050 101 5000 4810 96 5 70-130/20 75-00-3 Chloroethane ND 5000 9900 198*5000 9360 187*6 60-140/20 67-66-3 Chloroform ND 5000 5070 101 5000 4910 98 3 70-130/20 95-49-8 o-Chlorotoluene ND 5000 5150 103 5000 4920 98 5 70-130/20 106-43-4 p-Chlorotoluene ND 5000 5080 102 5000 4890 98 4 70-130/20 124-48-1 Dibromochloromethane ND 5000 4780 96 5000 4560 91 5 70-130/20 96-12-8 1,2-Dibromo-3-chloropropane ND 5000 4800 96 5000 4570 91 5 70-130/20 106-93-4 1,2-Dibromoethane ND 5000 4880 98 5000 4770 95 2 70-130/20 95-50-1 1,2-Dichlorobenzene ND 5000 4910 98 5000 4680 94 5 70-130/20 541-73-1 1,3-Dichlorobenzene ND 5000 4990 100 5000 4800 96 4 70-130/20 106-46-7 1,4-Dichlorobenzene ND 5000 5020 100 5000 4790 96 5 70-130/20 75-34-3 1,1-Dichloroethane ND 5000 5530 111 5000 5320 106 4 70-130/20 107-06-2 1,2-Dichloroethane ND 5000 5390 108 5000 5160 103 4 70-130/20 75-35-4 1,1-Dichloroethylene ND 5000 5310 106 5000 5150 103 3 70-130/20 156-59-2 cis-1,2-Dichloroethylene ND 5000 5230 105 5000 5070 101 3 70-130/20 156-60-5 trans-1,2-Dichloroethylene ND 5000 5550 111 5000 5310 106 4 70-130/20 78-87-5 1,2-Dichloropropane ND 5000 5270 105 5000 5080 102 4 70-130/20 142-28-9 1,3-Dichloropropane ND 5000 4920 98 5000 4730 95 4 70-130/20 594-20-7 2,2-Dichloropropane ND 5000 4700 94 5000 4640 93 1 70-130/20 563-58-6 1,1-Dichloropropene ND 5000 5180 104 5000 5020 100 3 70-130/20 10061-01-5 cis-1,3-Dichloropropene ND 5000 5120 102 5000 5000 100 2 70-130/20 10061-02-6 trans-1,3-Dichloropropene ND 5000 5130 103 5000 4990 100 3 70-130/20 108-20-3 Di-Isopropyl Ether 156 J 5000 5440 106 5000 5320 103 2 70-130/20 100-41-4 Ethylbenzene 177 J 5000 5380 104 5000 5150 99 4 70-130/20 637-92-3 Ethyl Tert Butyl Ether ND 5000 4310 86 5000 4310 86 0 70-130/20 87-68-3 Hexachlorobutadiene ND 5000 4720 94 5000 4430 89 6 70-130/20 98-82-8 Isopropylbenzene ND 5000 5210 104 5000 5000 100 4 70-130/20 * = Outside of Control Limits. 37 of 40 FA9441355.3.1 Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3 Job Number:FA94413 Account:GRINCC GRI (Geological Resources Inc.) Project:Sam's Pit Stop; 4236 Sam Potts Hwy, Hallsboro, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA94581-1MS A0231541.D 500 04/09/22 SS n/a n/a VA3109 FA94581-1MSD A0231542.D 500 04/09/22 SS n/a n/a VA3109 FA94581-1 A0231538.D 500 04/08/22 SS n/a n/a VA3109 The QC reported here applies to the following samples:Method: SM 6200B FA94413-1, FA94413-2, FA94413-3, FA94413-4, FA94413-5, FA94413-6 FA94581-1 Spike MS MS Spike MSD MSD Limits CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD 99-87-6 p-Isopropyltoluene ND 5000 5170 103 5000 4960 99 4 70-130/20 74-83-9 Methyl Bromide ND 5000 7930 159*5000 7950 159*0 60-140/20 74-87-3 Methyl Chloride ND 5000 5990 120 5000 5450 109 9 60-140/20 74-95-3 Methylene Bromide ND 5000 4730 95 5000 4610 92 3 70-130/20 75-09-2 Methylene Chloride ND 5000 5440 109 5000 5180 104 5 70-130/20 1634-04-4 Methyl Tert Butyl Ether 645 5000 5720 102 5000 5660 100 1 70-130/20 91-20-3 Naphthalene 79.4 J 5000 4460 88 5000 4290 84 4 70-130/20 103-65-1 n-Propylbenzene ND 5000 5050 101 5000 4840 97 4 70-130/20 100-42-5 Styrene ND 5000 4740 95 5000 4550 91 4 70-130/20 75-85-4 Tert-Amyl Alcohol ND 50000 41500 83 50000 37300 75 11 70-130/20 994-05-8 Tert-Amyl Methyl Ether ND 5000 4270 85 5000 4300 86 1 70-130/20 75-65-0 Tert-Butyl Alcohol ND 50000 41500 83 50000 34400 69*19 70-130/20 762-75-4 Tert-Butyl Formate ND 50000 35200 70 50000 41900 84 17 70-130/20 630-20-6 1,1,1,2-Tetrachloroethane ND 5000 5140 103 5000 4870 97 5 70-130/20 79-34-5 1,1,2,2-Tetrachloroethane ND 5000 5520 110 5000 5310 106 4 70-130/20 127-18-4 Tetrachloroethylene ND 5000 4850 97 5000 4620 92 5 70-130/20 108-88-3 Toluene 1870 5000 6930 101 5000 6780 98 2 70-130/20 87-61-6 1,2,3-Trichlorobenzene ND 5000 4700 94 5000 4450 89 5 70-130/20 120-82-1 1,2,4-Trichlorobenzene ND 5000 4720 94 5000 4490 90 5 70-130/20 71-55-6 1,1,1-Trichloroethane ND 5000 5030 101 5000 4880 98 3 70-130/20 79-00-5 1,1,2-Trichloroethane ND 5000 5080 102 5000 4900 98 4 70-130/20 79-01-6 Trichloroethylene ND 5000 5100 102 5000 4810 96 6 70-130/20 75-69-4 Trichlorofluoromethane ND 5000 4640 93 5000 4160 83 11 60-140/20 96-18-4 1,2,3-Trichloropropane ND 5000 4820 96 5000 4660 93 3 70-130/20 95-63-6 1,2,4-Trimethylbenzene 269 5000 5620 107 5000 5430 103 3 70-130/20 108-67-8 1,3,5-Trimethylbenzene 107 J 5000 5390 106 5000 5200 102 4 70-130/20 75-01-4 Vinyl Chloride ND 5000 4400 88 5000 4160 83 6 60-140/20 m,p-Xylene 968 10000 11600 106 10000 11200 102 4 70-130/20 95-47-6 o-Xylene 770 5000 6110 107 5000 5940 103 3 70-130/20 1330-20-7 Xylene (total)1740 15000 17700 106 15000 17200 103 3 70-130/20 CAS No.Surrogate Recoveries MS MSD FA94581-1 Limits 1868-53-7 Dibromofluoromethane 106%105%105%70-130% 17060-07-0 1,2-Dichloroethane-D4 104%104%108%70-130% * = Outside of Control Limits. 38 of 40 FA9441355.3.1 Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3 Job Number:FA94413 Account:GRINCC GRI (Geological Resources Inc.) Project:Sam's Pit Stop; 4236 Sam Potts Hwy, Hallsboro, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA94581-1MS A0231541.D 500 04/09/22 SS n/a n/a VA3109 FA94581-1MSD A0231542.D 500 04/09/22 SS n/a n/a VA3109 FA94581-1 A0231538.D 500 04/08/22 SS n/a n/a VA3109 The QC reported here applies to the following samples:Method: SM 6200B FA94413-1, FA94413-2, FA94413-3, FA94413-4, FA94413-5, FA94413-6 CAS No.Surrogate Recoveries MS MSD FA94581-1 Limits 2037-26-5 Toluene-D8 100%100%101%70-130% 460-00-4 4-Bromofluorobenzene 97%98%98%70-130% * = Outside of Control Limits. 39 of 40 FA9441355.3.1 Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1 Job Number:FA94413 Account:GRINCC GRI (Geological Resources Inc.) Project:Sam's Pit Stop; 4236 Sam Potts Hwy, Hallsboro, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA94541-1MS A0231617.D 100 04/12/22 SS n/a n/a VA3112 FA94541-1MSD A0231618.D 100 04/12/22 SS n/a n/a VA3112 FA94541-1 A0231612.D 100 04/12/22 SS n/a n/a VA3112 The QC reported here applies to the following samples:Method: SM 6200B FA94413-1, FA94413-2, FA94413-3, FA94413-4, FA94413-5, FA94413-6 FA94541-1 Spike MS MS Spike MSD MSD Limits CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD 71-43-2 Benzene 4340 1000 5340 100 1000 5090 75 5 70-130/20 75-00-3 Chloroethane <50 1000 1620 162*1000 1810 181*11 60-140/20 75-71-8 Dichlorodifluoromethane <50 1000 647 65 1000 731 73 12 60-140/20 74-87-3 Methyl Chloride <50 1000 1070 107 1000 1130 113 5 60-140/20 103-65-1 n-Propylbenzene <50 1000 1060 106 1000 875 88 19 70-130/20 CAS No.Surrogate Recoveries MS MSD FA94541-1 Limits 1868-53-7 Dibromofluoromethane 106%106%103%70-130% 17060-07-0 1,2-Dichloroethane-D4 103%102%109%70-130% 2037-26-5 Toluene-D8 99%100%101%70-130% 460-00-4 4-Bromofluorobenzene 96%97%95%70-130% * = Outside of Control Limits. 40 of 40 FA9441355.3.2