WI-7389_32505_CA_RMR_20221109

FINAL
2022 ANNUAL MONITORING REPORT
AUGUST 2021 – JULY 2022
TC-341 PIPELINE RELEASE SITE
NCDEQ INCIDENT #32505
MARINE CORPS BASE CAMP LEJEUNE, NORTH CAROLINA
Prepared for:
NAVFAC MIDLANT
Bldg. N-26 Rm. 3300
1510 Gilbert St.
Norfolk, VA 23511-3095
Prepared by:
Cherokee Nation 3S and Rhea Engineers and Consultants, Inc.
2 W. 2nd St., Ste. 1500
Tulsa, OK 74103
CONTRACT NO. N40085-21-D-1208
CTO: N4008521F5438
October 12, 2022
Benjamin Grosser, PG
NC Licensed Geologist No. 2233
2022 Annual Monitoring Report – TC-341
MCAS New River, NC
TABLE OF CONTENTS

EXECUTIVE SUMMARY ................................................................................................. i
SUMMARY OF RECOMMENDATIONS ........................................................................ iii
SITE INFORMATION ..................................................................................................... iv
1.0 Introduction .......................................................................................................... 1
1.1 Camp Geiger/MCB Camp Lejeune Location and Description .............. 1
1.2 TC-341 Site Description ........................................................................... 1
2.0 CONTAMINATION INVESTIGATION HISTORY ................................................... 4
2.1 1990 Site Assessments ........................................................................... 4
2.2 2010 Vapor Intrusion Investigation ........................................................ 4
2.3 2010 Revised Corrective Action Plan – Site Assessment .................... 4
2.4 2011/2012 Pipeline Excavation ............................................................... 5
2.5 2013 Free-Phase Product Recovery System Installation ..................... 5
2.6 Free-Phase Product Recovery System Modifications .......................... 6
2.7 2019-2020 Surfactant Injections ............................................................. 6
3.0 SYSTEM OPERATION AND RESULTS ............................................................... 7
3.1 Free-Phase Product Recovery Summary ............................................... 7
4.0 Groundwater analysis summary......................................................................... 8
4.1 Groundwater Gauging Summary ............................................................ 8
4.2 July 2022 Groundwater Flow Direction .................................................. 8
4.3 July 2022 Groundwater Sampling and Analytical Results ................... 8
4.4 2022 Groundwater Vapor Intrusion Screening .................................... 10
5.0 Conclusions ....................................................................................................... 11
5.1 FPR System Operations ........................................................................ 11
5.2 Groundwater Elevation Measurements ................................................ 11
5.3 Groundwater Analytical Conclusions .................................................. 11
5.4 Vapor Intrusion Monitoring ................................................................... 13
6.0 RECOMMENDATIONS ....................................................................................... 14
6.1 FPR System ............................................................................................ 14
6.2 Groundwater Monitoring ....................................................................... 14
7.0 References ......................................................................................................... 16

2022 Annual Monitoring Report – TC-341
MCAS New River, NC
TABLES

Table 1 FPR System Performance Data
Table 2 Cumulative Mass of Volatilized Hydrocarbons
Table 3 Monthly Monitoring Well Gauging Data
Table 4 Weekly Monitoring Well Gauging Data
Table 5 Groundwater Elevation Data July 2022
Table 6 Site Rehabilitation Goals for Chemicals of Concern
Table 7 Groundwater Analytical Results
Table 8 Proposed Monitoring Plan August 2022 to July 2023

FIGURES

Figure 1 Site Vicinity and Receptors
Figure 2 Site Map with Well Locations
Figure 3 System Layout
Figure 4A Site Map with Shallow Groundwater Elevation Contours July 2022
Figure 4B Site Map with Intermediate Groundwater Elevation Contours July
2022
Figure 5 Site Map with Free-Phase Product Detections
Figure 6 Site Map with Dissolved Phase Plume as of July 2022
Figure 7 Site Map with Proposed Sampling Plan – July 2023

APPENDICES

Appendix A Historical Gauging and Free-Phase Product Recovery Data
Appendix B Free-Phase Product Thickness vs. Time Charts
Appendix C 2022 Groundwater Laboratory Analytical Reports
Appendix D Contaminants of Concern vs. Time Charts
Appendix E Mann-Kendall Trend Analysis

2022 Annual Monitoring Report – TC-341
MCAS New River, NC
ACRONYMS AND ABBREVIATIONS

AFVR Aggressive Fluid Vapor Recovery
AMR Annual Monitoring Report
AST Aboveground Storage Tank

CATLIN Catlin Engineers and Scientists
CGFF Camp Geiger Fuel Farm
CN3S Cherokee Nation Support, Service, and Solutions, LLC.
COC Contaminants of Concern
CSA Comprehensive Site Assessment

DAVENPORT John Davenport Engineering, Inc.
DAVENPORT/Rhea Davenport-Rhea JV, LLC
DWQ Division of Water Quality

EMD Environmental Management Division
EPA Environmental Protection Agency
EPH Extractable Petroleum Hydrocarbons
EQB Environmental Quality Branch

FPR Free-phase Product Recovery
ft feet

G-480 Building G-480
GCL Gross Contaminant Level
GWSL Groundwater Screening Level
GWQS Groundwater Quality Standard

JV Joint Venture

MADEP Massachusetts Department of Environmental Protection
MCB Marine Corps Base
MSCC Maximum Soil Contaminant Concentration

NAVD North American Vertical Datum
NAVFAC Naval Facilities Engineering Command
NCAC North Carolina Administrative Code
NCDEQ North Carolina Department of Environmental Quality
NFA No Further Action
NPDES National Pollutant Discharge Elimination System
NSW Nutrient Sensitive Water

2022 Annual Monitoring Report – TC-341
MCAS New River, NC
Osage Osage of Virginia
OWS Oil/Water Separator

Pace Pace National Analytical
PAH Polycyclic Aromatic Hydrocarbons
PVI Petroleum Vapor Intrusion

RAC Remedial Action Construction
RBCA Risk Based Corrective Actions
RCAP-SA Revised Corrective Action Plan and Site Assessment
Rhea Rhea Engineers & Consultants, Inc.
RheaCon Consultech-Rhea JV, LLC

Site TC-341 Pipeline Release Site
STGW Soil to Groundwater

UST Underground Storage Tank

VI Vapor Intrusion
VOC Volatile Organic Compound
VPH Volatile Petroleum Hydrocarbons

WWTP Wastewater Treatment Plant

2022 Annual Monitoring Report – TC-341
MCAS New River, NC
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EXECUTIVE SUMMARY

Cherokee Nation Support, Service & Solutions, LLC. (CN3S) has been tasked by the
Department of the Navy, Naval Facilities Engineering Command (NAVFAC) Mid-Atlantic,
under Contract Number N40085-21-D-1208, Task Order N4008521F5438 to prepare this
Annual Monitoring Report (AMR) for the TC-341 Pipeline Release Site (Site), North
Carolina Department of Environmental Protection (NCDEQ) Incident Number 32505. The
Site is located within Camp Geiger on Marine Corps Base (MCB) Camp Lejeune, Onslow
County, North Carolina. The purpose of this report is to present the findings and
recommendations associated with the groundwater monitoring activities and groundwater
analytical results reported by John Davenport Engineering, Inc. (DAVENPORT)-Rhea
Engineers & Consultants, Inc. (Rhea) JV, LLC (DAVENPORT/Rhea) and CN3S-Rhea for
the monitoring period August 1, 2021 through July 31, 2022.

During August 2021 to July 2022, the system effectively operated for 305 of 365 days for
an operational efficiency of 84 percent. Downtime during the monitoring period was
mainly attributed to routine system maintenance, and electrical issues. During this
monitoring period, the Free-Phase Product Recovery (FPR) system recovered 880,988
gallons of groundwater; 106 gallons of free-phase product were recovered from the
oil/water separator (OWS) and monthly monitoring well product recovery events (passive
skimmers, peristaltic pump, bailing). Passive free-phase product skimmers are deployed
in monitoring wells USTG480-MW07, MW13, and MW20. During the August 2021 to July
2022 monitoring period, approximately 8.5 lbs. of hydrocarbons were emitted from the air
diffuser towers.

A site-wide gauging event of 71 wells was conducted and groundwater samples were
collected from 30 Site monitoring wells in July 2022. The groundwater samples were
analyzed for Volatile Organic Compounds (VOCs) via Standard Method (SM) 6200B,
Polycyclic Aromatic Hydrocarbons (PAH) via EPA Method 625, and Massachusetts
Department of Environmental Protection (MADEP) Volatile Petroleum Hydrocarbons
(VPH) and Extractable Petroleum Hydrocarbons (EPH).

Analytical results from the July 2022 sampling events determined that of the 30 shallow
and intermediate monitoring wells sampled, 19 exhibited Contaminant of Concern (COC)
concentrations above North Carolina Administrative Code (NCAC) 2L Groundwater
Quality Standards (GWQS). One monitoring well located within 30 feet (ft) of Building G-
480 (G-480) yielded naphthalene and MADEP exceedances of Non-Residential Vapor
Intrusion (VI) Groundwater Screening Levels (GWSLs).

CN3S-Rhea recommends continued FPR system operation, weekly gauging of the
recovery wells and sump to monitor drawdown of the shallow groundwater, monthly
gauging/product removal at 15 monitoring wells, and performing an annual site-wide
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gauging event in July 2023. CN3S-Rhea also recommends continued annual
groundwater sample collection at 28 monitoring wells in July 2023. The samples are to
be analyzed for VOCs via SM 6200B, PAHs via EPA Method 625, and MADEP VPH/EPH.

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MCAS New River, NC
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SUMMARY OF RECOMMENDATIONS

Based on the system operational status and the groundwater analytical results, CN3S-
Rhea recommends the following:

 Based on the presence of free-phase product at the Site, continued operation of
the FPR system.

 Weekly gauging of the 7 recovery wells and the recovery sump to document
drawdown of the shallow groundwater.

 The continued deployment of passive free-phase product passive skimmers and
monthly gauging/product removal at 15 monitoring wells.

 Conducting an annual site-wide gauging and groundwater sampling event of 28
monitoring wells in July 2023. The samples will be analyzed for VOCs via SM
6200B, EPA Method 625, and MADEP VPH/EPH.

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SITE INFORMATION

NCDEQ Incident No.: 32505
Facility ID No.: Building TC-341
Risk Classification: Intermediate
Land Use Classification: Industrial/Commercial

UST Owner/Operator:

Commanding General, MCB Camp Lejeune
G-F/EMD/EQB
PSC Box 20004
Onslow County,
Camp Lejeune, NC 28542
[phone]

Primary Responsible Party Contact:

Hagan Ratliff
Environmental Engineer
G-F/EMD/EQB
12 Post Lane
Onslow County,
Camp Lejeune, NC 28547
[phone]

Date of Release: Unknown
Quantity of Release: Unknown
Source of Release: Six-inch diameter transfer pipeline (No. 6 Fuel Oil and Kerosene)
Latitude/Longitude: 34.73891/-77.45195 [Former No. 6 Fuel Oil/Kerosene
Underground Storage Tank (UST) Location]

Tank
Number
Installation Date Tank
Capacity
Tank
Dimensions
Last
Contents
Previous
Contents
UST-TC-
341 Unknown 1,300
gallons Unknown No. 6 Fuel
Oil/Kerosene Unknown
2022 Annual Monitoring Report – TC-341
MCAS New River, NC
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1.0 INTRODUCTION

CN3S has been tasked by the Department of the Navy, NAVFAC Mid-Atlantic, under
Contract Number N40085-20-D-0022, Task Order N4008520F6234 to prepare this AMR
for the Site. The Site is located within Camp Geiger on MCB Camp Lejeune, Onslow
County, North Carolina. The objectives of this AMR are to document the current FPR
system performance and groundwater gauging events and to evaluate the extent of
dissolved-phase contamination at the Site based on the results of the annual sampling
event conducted in July 2022. The report also provides a brief environmental history of
the Site, summarizes the 2010 Revised Corrective Action Plan and Site Assessment
(RCAP-SA), and describes the installation and operation of the recommended remedial
alternative.

1.1 Camp Geiger/MCB Camp Lejeune Location and
Description

Camp Geiger/MCB Camp Lejeune is located in Onslow County, North Carolina and
serves as a training base for the United States Marine Corps. The Base covers
approximately 236 square miles (153,000 acres) and includes 14 miles of coastline. The
Base is bounded to the southeast by the Atlantic Ocean and to the northeast by NC State
Highway 24. The town of Jacksonville, North Carolina, is located north of the Base.

1.2 TC-341 Site Description

1.2.1 Site Characterization

The TC-341 Pipeline Release FPR system is located along F Street, within Camp Geiger,
which is part of MCB Camp Lejeune, in Onslow County, North Carolina (Figure 1).
Currently, the Site consists of Building G-480, a classroom facility for the Advanced
Infantry Training Battalion, the G-480 parking lot, and a grassed/wooded area. The Site
previously contained a mess hall heating plant (TC-341), the Camp Geiger Fuel Farm
(CGFF), and the infrastructure such as pumping stations, loading/unloading pads, and
underground distribution lines, necessary to receive and deliver petroleum products.

The former CGFF contained five 10,000 to 15,000-gallon aboveground storage tanks
(ASTs) used to store No. 6 fuel oil. The ASTs were later converted to store unleaded
gasoline, diesel fuel, No. 6 fuel oil, and kerosene. G-480 formerly contained a 500-gallon
diesel UST (UST G-480-1). The TC-341 heating plant formerly contained a 1,300-gallon
No. 6 fuel oil and kerosene UST (UST TC-341). The source of petroleum impact at the
Site is believed to be the six-inch diameter pipeline that was previously used to transfer
No. 6 fuel oil and kerosene from the CGFF to UST TC-341. The CGFF was abandoned
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and demolished between 1995 and 1997 to facilitate construction of the US Highway 17
Bypass. The tanks at each site were either removed or abandoned in place.

The groundwater monitoring network at the Site consists of 64 shallow-screened
monitoring wells, six intermediate-screened Type III monitoring wells and one deeper-
screened Type III monitoring well.

1.2.2 Site Geology

The Site is underlain by interbedded sand, silty sand, and clayey sand to a depth of
approximately 20 feet. The surficial material is underlain by limestone with varying
degrees of weathering (CATLIN Engineers and Scientists [CATLIN], 2008).

1.2.3 Site Hydrogeology

CATLIN reported groundwater elevation data in the 2008 Comprehensive Site
Assessment (CSA) and concluded that the generalized groundwater flow trend in the
shallow aquifer was towards the east to northeast across the Site at an approximate
horizontal hydraulic gradient of 0.011 feet per foot.

Vertical hydraulic gradients were calculated on Type II/Type III well pairs USTG480-
MW03/USTG480-MW15 and USTTC341-MW14/USTTC341-MW15 with resultant
vertical hydraulic gradients of -0.0039 and +0.0077. A shallow hydraulic conductivity
value of 0.00001221 feet per second, or 1.06 feet per day, was calculated, via a falling
head slug test performed at shallow monitoring well USTG480-MW09. A hydraulic
conductivity value of 0.00004433 feet per second, or 3.83 feet per day, was calculated
for the deep monitoring well USTG480-MW15 (CATLIN, 2008).

1.2.4 Site Receptors

The Site is not within a wellhead protection area and public water is provided to buildings
within 1,500 feet of the subject Site by water mains. The nearest named surface water
body is Brinson Creek approximately 600 feet northeast of the Site. According to the
NCDEQ Division of Water Quality (DWQ) Surface Water Classification, Brinson Creek is
classified as tidal saltwater (SC) with a supplemental classification of Nutrient Sensitive
Water (NSW). A manmade drainage ditch is located approximately 100 feet east of
Building G-480. Water in the drainage ditch flows northeast through a 48-inch diameter
drainage pipe under the US Highway 17 Bypass and discharges into wetlands located to
the northeast of the Bypass. Site conditions were not changed or altered during the
monitoring period of August 2021 to July 2022.

Several stormwater pipes transect the area of the contaminant plume and discharge into
Brinson Creek. CATLIN conducted a comprehensive monitoring well and stormwater
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sampling event to determine if any contamination was reaching Brinson Creek via the
stormwater system. This sampling event determined that petroleum hydrocarbons were
impacting the stormwater piping (CATLIN, 2009). To mitigate the impact, Rhea lined a
total of 519 feet of the existing stormwater piping downgradient from the contaminant
plume in July 2010. This was documented in the TC-341 Pipe Lining Project Construction
Closeout Report (Rhea, 2010).

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MCAS New River, NC
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2.0 CONTAMINATION INVESTIGATION HISTORY

2.1 1990 Site Assessments

Several investigations have been conducted at the Site since the early 1990s. These
investigations identified soil contamination, along with dissolved and free-phase
petroleum contamination in the groundwater. In August 2008, CATLIN conducted a site
assessment that documented the extent of the free-phase product contamination in the
surficial aquifer (CATLIN, 2008).

2.2 2010 Vapor Intrusion Investigation

Building G-480 is a classroom facility for the Advanced Infantry Training Battalion. In
2010, CH2M Hill performed a VI evaluation of the Site and reported recommendations in
the Final Vapor Intrusion Evaluation Report (CH2M Hill, 2010). Sub-slab, soil gas, and
indoor and outdoor air samples were collected at Building G-480. No Further Action (NFA)
for VI Assessment was recommended based on multiple lines of evidence; however,
CH2M Hill recommended that air quality monitoring be conducted if future construction
activities involve slab penetrations.

2.3 2010 Revised Corrective Action Plan – Site Assessment

In the RCAP-SA, CATLIN installed additional groundwater monitoring wells and
delineated the horizontal and vertical extent of dissolved and free-phase contaminant
plumes. The RCAP-SA recommended that Aggressive Fluid Vapor Recovery (AFVR)
events be periodically conducted on monitoring well USTTC341-MW01, based on the
presence of free-phase product in that well. The RCAP-SA also recommended installing
an FPR system with a recovery trench and recovery well network, including a series of
injection wells, to remediate the dissolved and free-phase product contamination.
Injection wells, placed within the contaminant plume, were recommended as a means to
mobilize residual free-phase product using surfactant injections (CATLIN, 2010).

The recommendations for remedial requirements from the RCAP-SA were based on the
Risk Based Corrective Actions (RBCA) for Petroleum USTs per 15A NCAC 2L .0106.
Additionally, the requirements in the NCDENR UST Section, 2008 Guidelines for
Assessment and Corrective Action for UST Releases are also applicable. The applicable
remedial goals for the Site are:

 Removal and recovery of the free-phase product. The goal of the remediation is to
reduce free-phase product levels to less than 0.01 feet. The Site may then be re-
evaluated and may be reclassified as “Low Risk.” If reclassified as a “Low Risk”
site, Gross Contaminant Levels (GCLs) will become the appropriate groundwater
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cleanup standard and Industrial/Commercial Maximum Soil Contaminant
Concentrations (MSCCs) will become the appropriate soil cleanup standard.

 Protect surface waters from free-phase product and dissolved phase
contamination associated with the release.

2.4 2011/2012 Pipeline Excavation

Soil, fuel pipeline, and asbestos-wrapped steam line removal actions were conducted
from October 2011 to September 2012 in two phases by Osage of Virginia (Osage). A
total of 375 feet of 3- and 6-inch fuel pipeline, 180 feet of 10-inch asbestos-wrapped steam
line, and 15,629 tons of petroleum impacted soil was removed from the Site and properly
disposed; however, soil contamination above Soil to Groundwater (STGW) and
Residential MSCCs are still present at the Site. Additional details of these activities can
be found in the TC-341 Pipeline Removal and Soil Excavation Completion Report (Osage,
2014).

2.5 2013 Free-Phase Product Recovery System Installation

Rhea installed the FPR system and began operation on October 7, 2013. The FPR
system uses both a horizontal trench system and a series of vertical recovery wells,
connected to an FPR system to recover and treat impacted groundwater (Figure 2).

The FPR system includes the following major components:

 Seven vertical FPR wells with submersible pumps (USTTC341-RW01 through -
RW07)
 Six injection wells (USTTC341-IW01 through -IW06)
 Two observation wells (USTTC341-OW01 and -OW02)
 310 feet of FPR trench with recovery sump and double-diaphragm pump
 OWS
 Four air diffuser boxes
 Water holding tank
 Air compressor

The Site has been included in the UST Management Program Annual Monitoring Program
since the installation of the FPR system in 2013. Historical soil and groundwater analytical
results are available in Appendix A.

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MCAS New River, NC
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2.6 Free-Phase Product Recovery System Modifications

On April 23, 2014, the FPR system was taken offline due to low-level PAH exceedances
in the National Pollutant Discharge Elimination System (NPDES) permitted outfall. To
remove free-phase product while the system was offline, Rhea began weekly AFVR
events on May 30, 2014. Based on the PAH exceedances, it was decided to alter the
system discharge to empty into the sanitary sewer system for transport to and final
treatment at the MCB Camp Lejeune Wastewater Treatment Plant (WWTP). After an
NPDES permit rescission request was approved by NCDEQ, the discharge was re-routed
to a nearby WWTP sewer manhole, and the system was restarted on October 27, 2014.

In February 2015, Rhea-Consultech JV, LLC (RheaCon) modified the FPR system to
include treatment with a proprietary iron sequestering agent to reduce iron fouling of
components and reduce system downtime due to iron fouling. The iron sequestering
treatment appeared to significantly reduce iron fouling of system components. After the
iron sequestering implementation, weekly cleanouts of the air stripper reduced to monthly
cleanout events.

An additional modification was made to the system in September 2019, when bag filters
and associated pretreatment equipment, no longer needed after discharge was re-routed
to the sewer, were disconnected from the treatment train. A 200-gallon poly tank was
installed to store water coming from the air diffuser boxes and a sump pump in the poly
tank provided sufficient pressure to discharge system effluent to the sanitary sewer. With
this modification, system water is more directly discharged to the sanitary sewer following
treatment by the air-diffuser boxes.

Passive free-phase product skimmers were added to the following four monitoring wells
in 2020-2021 to aid in the recovery of free-phase product: USTG480-MW07, USTG480-
MW13 and USTG480-MW20.

2.7 2019-2020 Surfactant Injections

To accelerate free product removal, surfactant injection events were conducted in
October 2019 and April 2020 at six permitted injection points. A total of 630 gallons of a
5% PetroSolv/water mixture was injected during each injection event, and each event
was followed by approximately 150 gallons of chase water to help move the injectate into
the subsurface. Both injection events resulted in increased free-phase product recovery.
However, the potential exists for enhanced mobilization of dissolved phase contaminants
beyond the capture zone of the FPR system. As such, no further surfactant injections are
recommended at the Site.

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MCAS New River, NC
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3.0 SYSTEM OPERATION AND RESULTS

3.1 Free-Phase Product Recovery Summary

During August 2021 to July 2022, the system effectively operated for 305 of 365 days for
an operational efficiency of 84 percent. Downtime during the August 2021 to July 2022
monitoring period was mainly attributed to routine system maintenance, and electrical
issues. A general layout of the TC-341 Pipeline Release FPR System is provided in Figure
3. Charts illustrating free-phase product presence over time at select monitoring wells are
presented in Appendix B.

During this monitoring period, the FPR system recovered 880,988 gallons of groundwater,
and 106 gallons of free-phase product were recovered from the OWS and monthly
monitoring well product recovery events (passive skimmers, peristaltic pump, bailer)
(Table 1). During the August 2021 to July 2022 monitoring period, approximately 8.5 lbs.
of hydrocarbons were emitted from the air diffuser towers (Table 2).

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MCAS New River, NC
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4.0 GROUNDWATER ANALYSIS SUMMARY

4.1 Groundwater Gauging Summary

During the August 2021 through July 2022 monitoring period, CN3S-Rhea conducted
weekly gauging of the 7 recovery wells and the recovery sump, monthly gauging of 24
monitoring wells, and an annual site-wide gauging event in July 2022. A free-phase
product thickness of 0.01 feet or greater in any monitoring well was removed with a
peristaltic pump or a bailer. A passive free-phase product skimmer is installed in
monitoring wells USTG480-MW07, MW13, and MW20.

During the 2021 to 2022 monitoring period, free-phase product was detected in
monitoring wells USTTC341-IW06, USTG480-MW06, MW07, MW08, MW13, and MW20,
as shown in Figure 5, as well as in recovery wells USTTC341-RW04, RW05, and RW07,
and the Recovery Sump. During the monitoring period, the skimmers recovered a total of
0.7 gallons of free-phase product and 0.3 gallons of free-phase product was removed
from the other monitoring wells. The free-phase product recovered from the monitoring
wells is included in the recovery totals presented in Table 1.

The monthly gauging data is detailed in Table 3, weekly gauging data is detailed in Table
4, and the annual gauging event in July 2022 is detailed in Table 5.

4.2 July 2022 Groundwater Flow Direction

In July 2022, the general groundwater flow direction in the shallow zone based on the
groundwater contour elevations shown in Figure 4A was towards the east, consistent with
previous findings.

The general groundwater flow direction in the intermediate zone based on the
groundwater contour elevations shown in Figure 4B was towards the northeast,
consistent with previous findings.

4.3 July 2022 Groundwater Sampling and Analytical Results

Groundwater samples were collected from 30 Site monitoring wells in July 2022. Samples
were collected via low flow techniques in accordance with NCDEQ guidelines. In shallow,
non-submerged well screens, one well volume as purged prior to stabilizing groundwater
drawdown and the collection of water quality parameters. Samples were then collected
once water quality parameters (conductivity, pH, temperature, dissolved oxygen, and
turbidity [if applicable]) stabilized. For deeper, submerged well screens, one tubing and
flow-through cell volume were purged prior to stabilizing groundwater drawdown and the
collection of water quality parameters. Samples were delivered under chain of custody to
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MCAS New River, NC
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Pace National Analytical (Pace) in Mt. Juliet, Tennessee (NC Certification Number 375)
and analyzed for VOCs using SM 6200B, PAHs by EPA Method 625 list, and MADEP
VPH/EPH.

A total of 28 shallow monitoring wells were sampled:

 USTG480-MW02  USTG480-MW26
 USTG480-MW06  USTG480-MW27
 USTG480-MW07  USTG480-MW28
 USTG480-MW08  USTG480-MW29
 USTG480-MW11  USTG480-MW30
 USTG480-MW12  USTG480-MW33R
 USTG480-MW13  USTTC341-MW01
 USTG480-MW14  USTTC341-MW05
 USTG480-MW16  USTTC341-MW08
 USTG480-MW17  USTTC341-MW13
 USTG480-MW18  USTTC341-MW14R
 USTG480-MW19  USTTC341-MW17
 USTG480-MW20  USTTC341-MW18
 USTG480-MW23  IR35-MW67AR

A total of 2 intermediate monitoring wells were sampled in July 2022:

 USTG480-MW25
 USTTC341-MW15R

Notes: Bolded monitoring wells indicate that a groundwater sample collected from the
well was reported with COC concentrations above 2L GWQS. No GCL exceedances were
reported in any sample collected in July 2022.

Petroleum hydrocarbon constituents were detected above their respective NCAC 2L
GWQS in 15 of the 28 shallow monitoring wells and one of the two intermediate
monitoring wells sampled. The groundwater sample from USTG480-MW16 exhibited a
NCAC 2L GWQS exceedance of vinyl chloride only, which is a COC associated with IR
Site 35 located to the south of this Site. Therefore, it was not included in shallow zone
contamination plume on Figure 6. Shallow monitoring well USTG480-MW30 and
Intermediate monitoring well USTG480-MW25 also exhibited a NCAC 2L GWQS
exceedance of vinyl chloride; along with a benzene NCAC 2L GWQS exceedance.
Accordingly, it is reasonable to assume those wells are also impacted by IR Site 35.

Benzene, naphthalene, 1-methylnaphthalene, 2-methylnaphthalene, and MADEP
aliphatic and aromatic fractions were the most commonly detected COCs at the Site in
excess of their respective NCAC 2L GWQS. Site rehabilitation goals for detected COCs
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are presented in Table 6. It should be noted that the significant increase in concentrations
of COCs observed in USTG480-MW26 in the July 2021 sampling event, and affecting the
2021 conditions in Table 6, was not repeated in the July 2022 event.

Groundwater analytical data are presented in Table 7. The shallow zone contamination
plume is depicted on Figure 6, along with indicators of intermediate zone groundwater
quality. Laboratory analytical data and chain of custody documentation are available in
Appendix C and charts showing changes in COC concentrations over time are available
in Appendix D.

4.4 2022 Groundwater Vapor Intrusion Screening

Laboratory analysis of wells within 30 feet of Building G-480 (USTG480-MW23,
USTTC341-MW17, and USTG480-MW14) revealed Non-Residential VI GWSL
exceedances for naphthalene and MADEP VPH/EPH during the July 2022 monitoring
event in monitoring well USTG480-MW23. January 2022 updates in the VI GWSLs are
used in Table 7; most notably, the new, more conservative screening level for
naphthalene resulted in this exceedance at USTG480-MW23. The total concentration of
petroleum constituents at USTG480-MW23 was well below the EPA petroleum vapor
intrusion (PVI) criterion of 30 mg/L.

In March 2021, CH2M collected two (2) subslab air samples, one (1) indoor air sample,
and one (1) outdoor air sample at Building G-480 and analyzed for Naphthalene. Although
the report that includes these samples taken at Building G-480 is still in draft, the results
were all non-detect, and NFA for the VI pathway is still recommended. Additionally, it
should be noted that Building G-480 is used as a classroom training building and is not
always occupied.

2022 Annual Monitoring Report – TC-341
MCAS New River, NC
11
5.0 CONCLUSIONS

5.1 FPR System Operations

During the August 2021 through July 2022 monitoring period, the treatment system
processed approximately 880,988 gallons of groundwater, and 106 gallons of free-phase
product were recovered from the OWS and monthly monitoring well product recovery
events. Since initial system startup in October 2013, the treatment system has recovered
a total of 20,675,309 gallons of water, and 2,518 gallons of free-phase product were
recovered from the OWS, monthly product recovery events, and AFVR events.

5.2 Groundwater Elevation Measurements

Groundwater elevations and free-phase product thicknesses at select monitoring wells
were measured monthly from August 2021 to July 2022. Free-phase product was
detected throughout this monitoring period at thicknesses ranging from 0.04 feet to 1.33
feet at various wells across the Site. Based on a review of the gauging data throughout
the August 2021 to July 2022 monitoring period, the number of wells containing free-
phase product decreased compared to the previous monitoring period.

5.3 Groundwater Analytical Conclusions

Analytical results from the July 2022 sampling events indicated COC concentrations
above NCAC 2L GWQS in 18 of the 28 shallow monitoring wells and one of the two
intermediate monitoring wells sampled. No GCL exceedances were observed in any
sample collected in July 2022.

Based on the results of the groundwater sampling event, the shallow groundwater
dissolved-phase plume has decreased in aerial extent. It should be noted that the furthest
downgradient monitoring well with an NCAC 2L GWQS exceedance (USTG480-MW16)
exhibited an exceedance of a single analyte, vinyl chloride. Vinyl chloride is not a COC
for this Site, but for adjoining IR Site 35 located to the south. Therefore, that well is not
included in the shallow dissolved-phase plume for the current Site AMR.

To quantitatively monitor trends in the dissolved phase plume, a review of monitoring well
data from 2013 to present was conducted for wells that have been routinely monitored
through that period. The review involved an analysis of benzene and naphthalene
concentration trends using the Mann-Kendall statistical method. Wells with free-phase
product detections in the last four years were eliminated from the analysis (to provide a
statistically sufficient number of data points after the most recent product presence), as
were wells with a history of consistently low constituent levels, near or below detection
2022 Annual Monitoring Report – TC-341
MCAS New River, NC
12
limits The Mann-Kendall analysis is presented in Appendix E. The analysis produced the
following results for the monitoring wells reviewed:

Trend Benzene Naphthalene
Increasing 0 0
Probably Increasing 0 0
Stable 3:
USTG480-MW02
USTG480-MW09R
USTG480-MW25
4:
USTG480-MW02
USTG480-MW04R
USTG480-MW11
USTG480-MW29
Probably Decreasing 1:
USTG480-MW31
1:
USTTC341-MW14/R
Decreasing 5:
USTG480-MW01
USTG480-MW17
USTG480-MW27
USTG480-MW30
USTTC341-MW14/R
5:
IR35-MW67AR
USTG480-MW01
USTG480-MW17
USTG480-MW27
USTTC341-MW18
No Trend 5:
IR35-MW67AR
USTG480-MW04R
USTG480-MW10
USTG480-MW29
USTTC341-MW18
3:
USTG480-MW09R
USTG480-MW10
USTG480-MW31

No increasing concentration trends were identified for benzene or naphthalene. Results
are somewhat different for the two compounds, in terms of the list of wells in each trend
category. The following general observations are noted:
 For benzene, decreasing or probably decreasing trends are indicated at six wells,
while stable trends or no trend are indicated at eight wells.
 For naphthalene, decreasing or probably decreasing trends are indicated at six
wells, while stable trends or no trend are indicated at seven wells.

Overall, the Mann-Kendall results indicate that, for the analyzed wells, while concentration
trends are not statistically increasing, less than half of the wells have decreasing trends.
The “stable” or “no trend” categories in some cases apply to wells with higher
concentrations than wells with decreasing trends, as can be seen in the summary tables
in Appendix E.

2022 Annual Monitoring Report – TC-341
MCAS New River, NC
13
5.4 Vapor Intrusion Monitoring

Laboratory analysis of wells within 30 feet of Building G-480 (USTG480-MW23,
USTTC341-MW17, and USTG480-MW14) yielded Non-Residential VI GWSL
exceedances for naphthalene and MADEP VPH/EPH during the July 2022 monitoring
event in monitoring well USTG480-MW23. The total concentration of petroleum
constituents at USTG480-MW23 was well below the EPA PVI criterion of 30 mg/L.

In 2010, CH2M Hill performed a VI evaluation of the Site and reported recommendations
in the Final Vapor Intrusion Evaluation Report (CH2M Hill, 2010). Sub-slab soil gas, and
indoor and outdoor samples were collected at Building G-480. NFA for VI Assessment
was recommended based on multiple lines of evidence; however, CH2M Hill
recommended that air quality monitoring be conducted if future construction activities
involve slab penetrations. Site conditions, including free-phase product presence and
groundwater analytical results, have not significantly adversely changed in the area near
Building G-480 since CH2M Hill’s 2010 VI evaluation at the Site.

In March 2021 CH2M collected two (2) subslab air samples, one (1) indoor air sample
and one (1) outdoor air sample at Building G-480 and analyzed for Naphthalene. Although
the report that includes these samples taken at Building G-480 is still in draft, the results
were all non-detect, and NFA for the VI pathway is still recommended.

As the levels of free-phase and dissolved phase impacts at the Site have been reduced
from historical levels at the time of CH2M Hill’s 2010 VI evaluation, coupled with the March
2021 air sample results and Building G-480 only being used intermittently as a classroom,
CN3S-Rhea supports CH2M Hill’s recommendation that no further VI assessment is
warranted, unless site conditions worsen or building activities involve slab penetration.

2022 Annual Monitoring Report – TC-341
MCAS New River, NC
14
6.0 RECOMMENDATIONS

Based on the RCAP-SA prepared by CATLIN in 2010, the Site meets the criteria for
classification as an Intermediate Risk and Industrial/Commercial Land Use Site. The goal
for the Site is to reduce free-phase produce thickness to less than 0.01 feet. Following
removal of free-phase product, the Site may be reclassified as Low Risk. If reclassified
as a Low-Risk Site, the appropriate groundwater cleanup standard will be GCLs and
Industrial/Commercial MSCCs will become the appropriate soil cleanup standard.

6.1 FPR System

Based on the presence of free-phase product at the Site, continued operation and
optimization of the FPR system is recommended.

6.2 Groundwater Monitoring

CN3S-Rhea recommends weekly gauging of the 7 recovery wells and recovery sump to
track groundwater drawdown:

 USTTC341-RW01  USTTC341-RW05
 USTTC341-RW02  USTTC341-RW06
 USTTC341-RW03  USTTC341-RW07
 USTTC341-RW04  Recovery Sump

CN3S-Rhea recommends monthly gauging of 15 monitoring wells (Table 8):

 USTG480-MW03  USTG480-MW08
 USTG480-MW06  USTG480-MW13
 USTG480-MW07  USTG480-MW20
 USTG480-MW26  USTTC341-IW01
 USTG480-MW28  USTTC341-IW06
 USTG480-MW29  USTTC341-MW01
 USTG480-MW31  USTTC341-MW18
 USTG480-MW32

The passive free-phase product skimmers will continue to be deployed in monitoring wells
USTG480-MW07, MW13, and MW20. If free-phase product greater than 0.01 feet in
thickness is detected in any of the monthly gauged monitoring wells, the product will be
removed by peristaltic pump or bailing.

CN3S-Rhea recommends a comprehensive gauging event including all 71 available Site
wells be performed annually in July 2023.
2022 Annual Monitoring Report – TC-341
MCAS New River, NC
15

Continued annual groundwater sample collection and analysis are recommended for July
2023 at the following 28 monitoring wells (Table 8):

 USTG480-MW02  USTG480-MW26
 USTG480-MW06  USTG480-MW27
 USTG480-MW07  USTG480-MW28
 USTG480-MW08  USTG480-MW29
 USTG480-MW11  USTG480-MW30
 USTG480-MW12  USTG480-MW33R
 USTG480-MW13  USTTC341-MW01
 USTG480-MW14  USTTC341-MW08
 USTG480-MW16  USTTC341-MW13
 USTG480-MW17  USTTC341-MW14
 USTG480-MW18  USTTC341-MW15
 USTG480-MW20  USTTC341-MW17
 USTG480-MW23  USTTC341-MW18
 USTG480-MW25  IR35-MW67AR

The list of proposed monitoring wells to be sampled in July 2023 has been optimized to
include plume perimeter monitoring wells, sentinel monitoring wells, and only a select
group of plume interior monitoring wells for statistical tracking purposes. It should also be
noted that if a monitoring well presents a free-phase product detection, a groundwater
sample will still be collected to assess the level of dissolved phase contaminants present
in that location.

Samples will be collected using low flow techniques and will be analyzed for VOCs via
SM 6200B, EPA Method 625, and MADEP VPH/EPH.

Free-phase product and COC levels will be re-evaluated in the next AMR to determine if
modifications to the recovery system are warranted. Based on a review of the August
2021 through July 2022 data, modifications to the FPR system are not currently
recommended at the Site.

2022 Annual Monitoring Report – TC-341
MCAS New River, NC
16
7.0 REFERENCES

CATLIN 2008. Leaking Underground Storage Tank Comprehensive Site Assessment
Report for TC-341 Pipeline, Marine Corps Base, Camp Lejeune, NC. August 19.

CATLIN 2009. Additional Assessment and Corrective Action Plan for TC-341 Pipeline,
Marine Corps Base, Camp Lejeune, NC. April 3.

CATLIN 2009. Revised Additional Assessment and Corrective Action Plan for TC-341
Pipeline, Marine Corps Base, Camp Lejeune, NC. October 9.

CATLIN 2010. Revised Corrective Action Plan and Site Assessment for TC-341
Pipeline, Marine Corps Base, Camp Lejeune, NC. August 25.

CATLIN 2011. RAC Design Package Final Submittal, Free-Phase Product Recovery
System TC-341 Pipeline Marine Corps Base Camp Lejeune, North Carolina. September
20.

CH2M Hill, 2010. Final Phase III Vapor Intrusion Evaluation Report.

DAVENPORT/Rhea, 2020. Final 2019 Annual Monitoring Report for TC-341 Free-Phase
Product Recovery System Marine Corps Air Station New River, North Carolina. February.

NCDENR, Division of Water Quality, 2002. Title 15A Subchapter 2L-Classifications and
Water Quality Standards Applicable to the Groundwaters of North Carolina. Effective
December 2002.

NCDENR, Division of Waste Management, UST Section, 2008. Guidelines for
Assessment and Corrective Action for UST Releases, July 15, 2008, Change 1 effective
December 1.

Rhea 2010. Final Construction Closeout Report, TC-341 Pipe Lining Project, Marine
Corps Air Station New River, Jacksonville, NC. October 25.

Rhea, 2013. Final Work Plan for TC-341 Free-Phase Product Recovery System
Installation Marine Corps Air Station New River, North Carolina. May.

Rhea, 2014. After Action Report TC-341 Free-Phase Product Recovery System
Installation and Groundwater Sampling, Marine Corps Air Station New River, North
Carolina. May.

2022 Annual Monitoring Report – TC-341
MCAS New River, NC
17
Rhea, 2015. Final 2015/2016 Annual Monitoring Report for TC-341 Free-Phase Product
Recovery System Marine Corps Air Station New River, North Carolina. December.

Rhea, 2018. Final 2017/2018 Annual Monitoring Report for TC-341 Free-Phase Product
Recovery System Marine Corps Air Station New River, North Carolina. December.

2022 Annual Monitoring Report – TC-341
MCAS New River, NC

TABLES
(.'\ (HEROKEENATION™ ~ 3 S-Support, Service & Solutions
Table 1
FPR System Performance Data
2022 Annual Monitoring Report - TC-341
August 2021 - July 2022
(gpm) (gpd)
Product Tank
& Bailing Cumulative
10/7/2013 0 0 0.00 0.00 0 0
10/14/2013 168 2190 0.22 312.86 10 10
10/21/2013 168 88772 8.81 12681.71 10 20
10/28/2013 168 17677 1.75 2525.29 38 58
11/5/2013 192 194691 16.90 24336.38 215 273
11/11/2013 48 838 0.29 419.00 3 276
12/5/2013 120 35834 4.98 7166.80 5 281
12/16/2013 264 149489 9.44 13589.91 17 298
1/21/2014 240 130510 9.06 13051.00 6 304
2/18/2014 48 13468 4.68 6734.00 16 320
3/5/2014 360 248465 11.50 16564.33 15 335
4/7/2014 720 405423 9.38 13514.10 8 343
4/23/2014 384 217892 9.46 13618.25 45 388
5/30/2014 0 0 0.00 0.00 7 395
6/24/2014 0 0 0.00 0.00 53 448
7/31/2014 0 0 0.00 0.00 70 518
11/3/2014 168 132361 13.13 18908.71 148* 613
12/5/2014 624 221761 5.92 8529.27 31 644
1/22/2015 840 281426 5.58 8040.74 23.5 668
2/25/2015 768 334901 7.27 10465.66 11 679
3/24/2015 624 301952 8.06 11613.54 47.5 726
4/29/2015 744 260153 5.83 8392.03 65 791
5/19/2015 384 97563 4.23 6097.69 60 851
5/26/2015 144 47216 5.46 7869.33 10 861
6/15/2015 384 70425 3.06 4401.56 15 876
7/28/2015 1032 274668 4.44 6387.63 25 901
8/17/2015 480 179717 6.24 8985.85 5 906
9/14/2015 672 163124 4.05 5825.86 0 906
10/13/2015 576 153346 4.44 6389.42 44.5 951
11/16/2015 720 94468 2.19 3148.93 0 951
12/14/2015 576 747 0.02 31.13 0 951
1/4/2016 504 127810 4.23 6086.19 0 951
2/1/2016 480 48321 1.68 2416.05 110.4 1061
2/22/2016 360 5565 0.26 371.00 2.94 1064
3/14/2016 408 11734 0.48 690.24 0 1064
3/22/2016 192 8488 0.74 1061.00 3.25 1067
5/6/2016 840 45663 0.91 1304.66 64.0175 1131
5/24/2016 432 175500 6.77 9750.00 15.896 1147
6/14/2016 504 144561 4.78 6883.86 29.8116 1177
6/28/2016 336 94458 4.69 6747.00 0 1177
7/28/2016 552 408408 12.33 17756.87 51 1228
8/9/2016 288 41675 2.41 3472.92 20.5 1248
8/16/2016 168 31035 3.08 4433.57 25 1273
8/25/2016 216 49258 3.80 5473.11 15 1288
9/8/2016 336 82949 4.11 5924.93 15 1303
9/13/2016 120 31225 4.34 6245.00 0 1303
10/18/2016 840 119571 2.37 3416.31 40 1343
10/26/2016 192 26862 2.33 3357.75 5 1348
11/1/2016 144 1289 0.15 214.83 20 1368
12/27/2016 1344 21538 0.27 384.61 10 1378
1/6/2017 240 11899 0.83 1189.90 0.2 1379
2/10/2017 840 17369 0.34 496.26 20 1399
2/13/2017 72 9622 2.23 3207.33 0 1399
2/20/2017 168 14874 1.48 2124.86 25.6 1424
3/1/2017 216 25231 1.95 2803.44 200 1624
3/6/2017 144 46159 5.34 7693.17 10 1634
3/13/2017 168 72777 7.22 10396.71 0 1634
3/22/2017 216 82368 6.36 9152.00 0 1634
3/29/2017 168 45096 4.47 6442.29 0.1 1634
Flow meter failed
Flow meter replaced
System run hours is the amount
between readings
Date
Approximate
System Run
Hours
Total
Discharge
(gallons)
Approximate Well
Yield Product Recovery (gallons)
Comments
System Startup
RheaCon assumed O&M
Switched to hour meter reading
1 of 4
Table 1
FPR System Performance Data
2022 Annual Monitoring Report - TC-341
August 2021 - July 2022
(gpm) (gpd)
Product Tank
& Bailing Cumulative
Date
Approximate
System Run
Hours
Total
Discharge
(gallons)
Approximate Well
Yield Product Recovery (gallons)
Comments
System Startup4/3/2017 96 13228 2.30 3307.00 0 1634
4/10/2017 168 49005 4.86 7000.71 0 1634
4/21/2017 264 71805 4.53 6527.73 0 1634
4/26/2017 120 16246 2.26 3249.20 0.5 1635
5/3/2017 168 52680 5.23 7525.71 10 1645
5/12/2017 216 53344 4.12 5927.11 13.25 1658
7/21/2017 840 65091 1.29 1859.74 0 1658
7/26/2017 120 36500 5.07 7300.00 0 1658
8/9/2017 336 10623 0.53 758.79 0 1658
8/11/2017 46 21382 7.75 11155.83 0 1658
8/18/2017 173 64827 6.25 8993.34 5 1663
8/25/2017 162 60238 6.20 8924.15 10 1673
9/1/2017 168 374175 37.12 53453.57 20 1693
9/8/2017 164 240265 24.42 35160.73 5 1698
9/15/2017 97 76065 13.07 18820.21 5 1703
9/22/2017 146 45652 5.21 7504.44 5 1708
10/6/2017 341 75083 3.67 5284.43 5 1713
10/13/2017 160 22030 2.29 3304.50 0 1713
10/27/2017 254 59560 3.91 5627.72 10 1723
11/3/2017 122 46010 6.29 9051.15 10 1733
11/10/2017 126 58818 7.78 11203.43 10 1743
11/16/2017 108 49008 7.56 10890.67 10 1753
11/21/2017 117 33070 4.71 6783.59 5 1758
12/1/2017 211 62929 4.97 7157.80 10 1768
12/7/2017 115 36247 5.25 7564.59 15 1783
12/13/2017 105 32218 5.11 7364.11 0 1783
12/21/2017 147 43170 4.89 7048.16 30 1813
12/29/2017 198 58690 4.94 7113.94 15 1828
1/31/2018 326 91659 4.69 6747.90 10 1838
02/15/18 353 106950 5.05 7271.39 50 1888
02/21/18 144 32437 3.75 5406.17 5 1893
02/28/18 163 34338 3.51 5055.90 0 1893
03/09/18 217 562445 43.20 62205.90 10 1903
03/14/18 111 36438 5.47 7878.49 5 1908
03/21/18 168 420119 41.68 60017.00 5 1913
03/28/18 168 219538 21.78 31362.57 5 1918
04/04/18 117 8305 1.18 1703.59 0 1918
04/11/18 167 233816 23.33 33602.30 10 1928
04/19/18 193 54084 4.67 6725.47 0 1928
04/26/18 169 25180 2.48 3575.86 0 1928
05/02/18 141 21814 2.58 3713.02 10 1938
05/11/18 214 62239 4.85 6980.07 5 1943
05/14/18 67 18577 4.62 6654.45 0 1943
05/23/18 215 57635 4.47 6433.67 5 1948
06/01/18 214 57113 4.45 6405.20 5 1953
06/06/18 125 41037 5.47 7879.10 0 1953
06/15/18 190 58535 5.13 7393.89 10 1963
07/05/18 203 25361 2.08 2998.34 5 1968
07/11/18 26 12939 8.29 11943.69 0 1968
07/20/18 210 63915 5.07 7304.57 10 1978
07/25/18 114 20860 3.05 4391.58 5 1983
08/20/18 352 258895 12.26 17651.93 15 1998
09/26/18 517 400280 12.90 18581.66 40.27 2038
10/23/18 463 234488 8.44 12154.89 10 2048
11/26/18 809 139939 2.88 4151.47 1 2049
01/09/19 657 454486 11.53 16602.23 25 2074
01/17/19 165 121207 12.24 17630.11 0.25 2074
02/12/19 615 1051500 28.50 41034.15 3 2077
03/13/19 696 565266 13.54 19491.93 3 2080
DAVENPORT-Rhea assumed O&M
2 of 4
Table 1
FPR System Performance Data
2022 Annual Monitoring Report - TC-341
August 2021 - July 2022
(gpm) (gpd)
Product Tank
& Bailing Cumulative
Date
Approximate
System Run
Hours
Total
Discharge
(gallons)
Approximate Well
Yield Product Recovery (gallons)
Comments
System Startup03/27/19 298 42006 2.35 3383.03 0.25 2081
04/01/19 120 63723 8.85 12744.60 1 2082
04/15/19 334 182280 9.10 13097.96 1 2083
05/01/19 333 195143 9.77 14064.36 3.25 2086
05/06/19 167 60242 6.01 8657.53 0.75 2087
05/28/19 523 251424 8.01 11537.62 5 2092
06/17/19 477 179097 6.26 9011.17 4 2096
06/27/19 236 232202 16.40 23613.76 2.75 2098
07/12/19 264 NA NA NA 1.56 2100
07/31/19 274 NA NA NA 1.86 2102
08/26/19 611 141305 3.85 5550.44 7.2 2109
09/30/19 497 255678 8.57 12346.62 6.0 2115
10/23/19 387 105177 4.53 6522.60 4.0 2119
11/20/19 642 236935 6.15 8857.38 5.2 2124
12/26/19 853 353591 6.91 9948.63 18.7 2143
01/06/20 263 101968 6.46 9305.06 2.2 2145
01/13/20 166 62068 6.23 8973.69 6.2 2151
01/30/20 307 110978 6.02 8675.80 4.9 2156
02/05/20 141 44440 5.25 7564.26 1.3 2157
02/10/20 109 10952 1.67 2411.45 1.2 2159
02/24/20 187 24253 2.16 3112.68 1.3 2160
03/04/20 210 88787 7.05 10147.09 1.8 2162
03/09/20 117 52150 7.43 10697.44 0.9 2163
03/20/20 234 109870 7.83 11268.72 1.6 2164
03/23/20 73 33110 7.56 10885.48 1.5 2166
04/03/20 256 84835 5.52 7953.28 2.9 2169
04/06/20 72 31655 7.33 10551.67 0.8 2169
04/14/20 142 44425 5.21 7508.45 1.8 2171
04/22/20 188 76395 6.77 9752.55 10.0 2181
04/27/20 108 43870 6.77 9748.89 2.2 2183
05/04/20 166 67395 6.77 9743.86 4.7 2188
05/11/20 89 36015 6.74 9711.91 1.2 2189
05/19/20 190 87152 7.64 11008.67 1.8 2191
05/26/20 160 58868 6.13 8830.20 1.6 2193
06/05/20 182 52486 4.81 6921.23 1.8 2195
06/12/20 113 55698 8.22 11829.66 1.3 2196
06/18/20 119 54356 7.61 10962.55 2.3 2198
07/31/20 700 376409 8.96 12905.45 8.1 2206
08/07/20 132 52572 6.64 9558.55 0.6 2207
08/13/20 81 33432 6.88 9905.78 0.5 2207
08/20/20 164 83072 8.44 12156.88 3.1 2210
08/31/20 261 119360 7.62 10975.63 7.4 2218
09/04/20 92 43553 7.89 11361.65 0.5 2218
09/11/20 164 79882 8.12 11690.05 1.1 2219
09/17/20 144 70540 8.16 11756.67 1.9 2221
09/30/20 289 146385 8.44 12156.54 7.4 2229
10/08/20 169 67577 6.66 9596.73 6.0 2235
10/15/20 169 55078 5.43 7821.73 8.2 2243
10/22/20 95 27733 4.87 7006.23 4.6 2247
10/30/20 191 44587 3.89 5602.55 9.0 2256
11/05/20 144 37486 4.34 6247.67 6.3 2263
11/12/20 164 54202 5.51 7932.00 6.4 2269
11/19/20 171 73243 7.14 10279.72 2.4 2272
11/30/20 261 85654 5.47 7876.23 16.4 2288
12/03/20 70 22949 5.46 7868.23 6.5 2294
12/10/20 110 40505 6.14 8837.45 5.8 2300
12/17/20 166 53028 5.32 7666.70 2.1 2302
12/30/20 311 101159 5.42 7806.48 6.9 2309
01/07/21 89 30745 5.76 8290.79 2.0 2311
Flowmeter inoperable
Flowmeter inoperable
3 of 4
Table 1
FPR System Performance Data
2022 Annual Monitoring Report - TC-341
August 2021 - July 2022
(gpm) (gpd)
Product Tank
& Bailing Cumulative
Date
Approximate
System Run
Hours
Total
Discharge
(gallons)
Approximate Well
Yield Product Recovery (gallons)
Comments
System Startup01/15/21 171 98192 9.57 13781.33 0.2 2312
01/22/21 164 87336 8.88 12780.88 1.8 2313
01/28/21 144 69616 8.06 11602.67 3.7 2317
02/04/21 131 59049 7.51 10818.14 3.2 2320
02/11/21 167 70581 7.04 10143.38 3.7 2324
02/19/21 192 70918 6.16 8864.75 6.3 2330
02/25/21 143 57215 6.67 9602.52 3.9 2334
03/04/21 167 68993 6.89 9915.16 2.6 2337
03/11/21 169 66086 6.52 9384.99 3.4 2340
03/19/21 197 83824 7.09 10212.06 0.7 2341
03/31/21 276 102170 6.17 8884.35 8.3 2349
04/08/21 192 48168 4.18 6021.00 4.1 2353
04/15/21 172 40045 3.88 5587.67 4.5 2358
04/22/21 164 30911 3.14 4523.56 3.2 2361
04/29/21 164 26746 2.72 3914.05 2.3 2363
05/06/21 171 19224 1.87 2698.11 2.6 2366
05/14/21 185 24866 2.24 3225.86 4.9 2371
05/20/21 144 14361 1.66 2393.50 8.0 2379
05/27/21 120 21421 2.98 4284.20 2.5 2381
06/04/21 192 38036 3.30 4754.50 1.2 2382
06/10/21 137 25014 3.04 4382.01 3.5 2386
06/17/21 167 43559 4.35 6259.98 3.8 2390
06/24/21 166 23429 2.35 3387.33 5.3 2395
07/09/21 313 24657 1.31 1890.63 8.3 2403 system off 7/8-7/9 for Elsa
07/15/21 148 4032 0.45 653.84 2.8 2406 Malfunctioning Flowmeter
07/22/21 168 5326 0.53 760.86 2.5 2409 Malfunctioning Flowmeter
07/29/21 168 1130 0.11 161.43 3.8 2412 Malfunctioning Flowmeter
08/12/21 327 18271 0.93 1340.99 9.4 2422
08/26/21 333 74548 3.73 5372.83 12.7 2434
09/13/21 415 85997 3.45 4973.32 14.1 2449
10/05/21 405 81620 3.36 4836.74 8.2 2457
10/20/21 328 20680 1.05 1513.17 4.0 2461
11/03/21 335 26276 1.31 1882.46 3.3 2464
11/23/21 405 50156 2.06 2972.21 5.1 2469
12/14/21 405 53288 2.19 3157.81 3.4 2473
12/22/21 245 40967 2.79 4013.09 0.8 2473
01/20/22 293 50016 2.85 4096.87 0.7 2474
02/07/22 424 45196 1.78 2558.26 1.6 2476 Flow meter failure, replaced 2/16/22
02/22/22 359 23370 1.08 1562.34 3.2 2479
03/14/22 476 41147 1.44 2074.64 4.1 2483
04/08/22 299 40152 2.24 3222.90 4.3 2487
05/09/22 693 100856 2.43 3492.85 5.9 2493
06/14/22 601 40600 1.13 1621.30 10.7 2504
06/30/22 314 21475 1.14 1641.40 4.8 2509
07/29/22 673 66373 1.64 2366.94 8.9 2518
Total Discharge 20,675,309 Total LPH 2,518
4 of 4
Table 2
Cumulative Mass of Volatilized Hydrocarbons
2022 Annual Monitoring Report - TC-341
August 2021 - July 2022
10/7/2013 0 NA NA NA NA NA NA 0.0 System startup
10/14/2013 168 2675 6.1 75.5 921 0.032 2.674 18.7
10/21/2013 168 2363 307.8 69.2 823 1.637 120.597 862.9
10/28/2013 168 3163 9.3 69.6 1101 0.049 4.874 897.0
12/5/2013 360 2455 3.0 73.8 848 0.016 1.211 915.2
12/16/2013 264 1920 1.2 60.5 680 0.006 0.388 919.4
2/18/2014 288 2788 0.1 70.4 969 0.001 0.046 920.0
3/5/2014 360 3676 1.0 70.8 1277 0.005 0.608 929.1
4/21/2014 1056 2566 0.9 70.5 892 0.005 0.382 945.9
11/03/14 168 2096 0.0 68.8 731 0.000 0.000 945.9
12/05/14 624 1480 0.0 66.7 518 0.000 0.000 945.9
01/22/15 840 2103 0.0 61.4 744 0.000 0.000 945.9
02/25/15 768 1870 0.0 60.0 663 0.000 0.000 945.9
03/24/15 624 1875 1.6 63.0 661 0.009 0.503 959.0
04/29/15 744 1939 7.4 64.4 682 0.039 2.401 1033.4
05/19/15 384 2690 3.9 74.9 927 0.021 1.721 1061.0
05/26/15 144 1639 14.3 74.9 565 0.076 3.845 1084.0
06/15/15 384 4300 0.1 71.3 1492 0.001 0.071 1085.2
07/06/15 504 948 0.0 105.2 309 0.000 0.000 1085.2
07/28/15 528 435 2.0 101.1 143 0.011 0.136 1088.2
08/17/15 480 856 0.0 96.2 284 0.000 0.000 1088.2
09/14/15 672 1154 0.0 91.3 386 0.000 0.000 1088.2
10/13/15 576 4132 0.0 89.2 1387 0.000 0.000 1088.2
11/16/15 720 650 0.8 70.1 226 0.004 0.086 1090.7
12/14/15 576 1500 0.0 87.4 505 0.000 0.000 1090.7
01/04/16 504 5029 2.5 64.4 1768 0.013 2.104 1134.9
02/01/16 480 1442 0.1 70.8 501 0.001 0.024 1135.4
02/22/16 360 4744 0.0 79.6 1621 0.000 0.000 1135.4
03/14/16 408 4018 0.7 90.5 1346 0.004 0.448 1143.0
03/22/16 192 1368 0.0 62.0 483 0.000 0.000 1143.0
05/06/16 840 1292 0.3 60.5 458 0.002 0.065 1145.3
05/24/16 432 1262 4.1 69.1 440 0.022 0.858 1160.8
06/14/16 504 1597 0.6 77.8 547 0.003 0.156 1164.0
06/28/16 336 1232 0.0 71.2 428 0.000 0.000 1164.0
7/28/2016 552 1222 0.0 83.2 415 0.000 0.000 1164.0
8/9/2016 245 1282 0.0 91.0 429 0.000 0.000 1164.0
8/16/2016 140 1164 0.0 82.5 396 0.000 0.000 1164.0
8/25/2016 209 1411 0.3 78.9 483 0.002 0.069 1164.6
9/8/2016 316 1227 0.0 85.6 415 0.000 0.000 1164.6
9/13/2016 117 1048 1.2 78.9 359 0.006 0.205 1165.6
10/18/2016 318 1301 0.0 78.4 445 0.000 0.000 1165.6
10/26/2016 68 1448 0.0 63.0 510 0.000 0.000 1165.6
11/1/2016 86 1418 0.0 61.7 501 0.000 0.000 1165.6
12/27/2016 1060 1231 0.0 68.6 429 0.000 0.000 1165.6
1/6/2017 136 456 0.0 49.6 165 0.000 0.000 1165.6
2/10/2017 91 484 0.4 66.1 170 0.002 0.032 1165.8
2/13/2017 59 609 0.0 62.9 215 0.000 0.000 1165.8
02/20/17 83 1202 0.2 66.7 421 0.001 0.040 1165.9
03/01/17 148 1197 0.0 74.7 413 0.000 0.000 1165.9
03/06/17 103 1053 0.1 64.9 370 0.001 0.018 1166.0
03/13/17 166 1238 0.0 62.0 437 0.000 0.000 1166.0
03/22/17 211 1408 0.0 67.6 492 0.000 0.000 1166.0
03/29/17 127 2806 0.0 73.5 970 0.000 0.000 1166.0
04/03/17 43 1431 0.0 76.8 491 0.000 0.000 1166.0
04/10/17 139 1687 0.3 73.5 583 0.002 0.083 1166.5
04/21/17 256 1987 0.0 73.5 687 0.000 0.000 1166.5
04/26/17 44 1195 0.1 65.4 419 0.001 0.020 1166.5
05/03/17 174 1327 0.0 76.5 456 0.000 0.000 1166.5
05/12/17 212 1488 0.0 67.6 520 0.000 0.000 1166.5
07/21/17 194 1720 0.0 84.3 583 0.000 0.000 1166.5
07/26/17 117 1531 0.0 73.5 529 0.000 0.000 1166.5
08/11/17 382 1257 0.8 70.5 437 0.004 0.166 1169.1
08/18/17 173 789 0.2 82.8 268 0.001 0.026 1169.3
08/25/17 162 1139 1.4 73.7 393 0.007 0.262 1171.1
09/01/17 168 997 0.9 74.6 344 0.005 0.147 1172.1
09/08/17 164 1247 0.1 74.1 430 0.001 0.020 1172.3
09/15/17 97 721 0.1 79.8 246 0.001 0.012 1172.3
09/22/17 146 845 0.4 85.5 286 0.002 0.054 1172.6
10/06/17 341 1115 1.2 82.6 379 0.006 0.216 1175.7
10/13/17 160 1215 1.2 71.3 422 0.006 0.241 1177.3
TH Conc
(C) (mg/l)
TH Recovery
Rate (M)
(lb/day)
Cumulative Mass
of Hydrocarbons
Recovered (lbs)
CommentsDate
Air Diffuser
Blower
Hours of
Operation
(Hrs)
Vapor
Velocity
(ft/min)
Vapor
Concentration
(PPM)
Temperature (°F)
Calculated
Vapor
Flowrate (Q)
(SCFM)
1 of 4
Table 2
Cumulative Mass of Volatilized Hydrocarbons
2022 Annual Monitoring Report - TC-341
August 2021 - July 2022
TH Conc
(C) (mg/l)
TH Recovery
Rate (M)
(lb/day)
Cumulative Mass
of Hydrocarbons
Recovered (lbs)
CommentsDate
Air Diffuser
Blower
Hours of
Operation
(Hrs)
Vapor
Velocity
(ft/min)
Vapor
Concentration
(PPM)
Temperature (°F)
Calculated
Vapor
Flowrate (Q)
(SCFM)
10/27/17 254 1201 0.4 71.2 417 0.002 0.079 1178.2
11/03/17 122 1505 0.3 77.5 516 0.002 0.074 1178.5
11/10/17 126 601 0.9 66.8 210 0.005 0.090 1179.0
11/16/17 108 741 0.3 69.8 258 0.002 0.037 1179.2
11/21/17 117 823 0.4 68.3 287 0.002 0.055 1179.4
12/01/17 211 772 0.3 74.0 267 0.002 0.038 1179.8
12/07/17 115 605 5.6 61.3 214 0.030 0.570 1182.5
12/13/17 105 589 1.8 68.4 206 0.010 0.176 1183.3
12/21/17 147 897 0.2 63.5 316 0.001 0.030 1183.5
12/29/17 198 1106 0.3 57.9 394 0.002 0.056 1183.9
01/31/18 326 956 0.1 57.3 341 0.001 0.016 1184.1
02/15/18 353 1177 0.1 74.4 406 0.001 0.019 1184.4
02/21/18 144 1011 0.1 76.4 347 0.001 0.017 1184.5
02/28/18 163 1114 0.0 55.0 399 0.000 0.000 1184.5
03/09/18 217 1116 0.1 55.4 399 0.001 0.019 1184.7
03/14/18 111 1071 0.4 56.8 382 0.002 0.073 1185.0
03/21/18 168 1038 0.1 55.6 371 0.001 0.018 1185.2
03/28/18 168 920 0.2 63.9 324 0.001 0.031 1185.4
04/04/18 117 966 0.0 72.8 334 0.000 0.000 1185.4
04/11/18 167 951 0.6 60.3 337 0.003 0.096 1186.1
04/19/18 193 971 0.2 82.5 330 0.001 0.031 1186.3
04/26/18 169 847 0.0 75.3 292 0.000 0.000 1186.3
05/02/18 141 650 0.3 65.2 228 0.002 0.033 1186.5
05/11/18 214 842 0.0 98.9 278 0.000 0.000 1186.5
05/14/18 67 883 0.0 92.9 294 0.000 0.000 1186.5
05/23/18 215 831 0.1 74.0 287 0.001 0.014 1186.6
06/01/18 214 484 0.0 81.3 165 0.000 0.000 1186.6
06/06/18 125 753 0.0 83.8 255 0.000 0.000 1186.6
06/15/18 190 746 0.1 85.8 252 0.001 0.012 1186.7
07/05/18 203 845 0.3 83.1 287 0.002 0.041 1187.1
07/11/18 26 798 0.1 95.1 265 0.001 0.013 1187.1
07/20/18 210 923 0.1 75.6 318 0.001 0.015 1187.2
07/25/18 114 856 0.3 82.2 291 0.002 0.042 1187.4
08/20/18 352 738 0.6 85.2 250 0.003 0.071 1188.4
09/26/18 517 936 0.3 76.3 322 0.002 0.046 1189.4
10/23/18 463 742 0.2 66.8 260 0.001 0.025 1189.9
11/26/18 809 948 0.7 68.5 331 0.004 0.110 1193.6
01/09/19 119 1048 0.0 58.3 373 0.000 0.000 1193.6 DAVENPORT/Rhea assumed O&M
01/17/19 165 1052 0.1 59.6 373 0.000 0.009 1193.7
01/24/19 165 1022 0.0 63.0 360 0.000 0.004 1193.7
02/06/19 306 882 0.0 58.9 313 0.000 0.000 1193.7
02/12/19 144 1063 0.1 60.9 376 0.000 0.009 1193.8
02/19/19 165 1028 0.1 53.3 369 0.000 0.009 1193.7
02/26/19 166 1030 0.0 57.2 367 0.000 0.004 1193.7
03/13/19 365 1115 0.0 63.3 393 0.000 0.005 1193.7
03/20/19 161 1133 0.0 57.8 403 0.000 0.000 1193.7
03/27/19 137 998 0.7 60.0 354 0.004 0.122 1194.4
04/01/19 120 982 2.7 56.9 350 0.014 0.450 1196.7
04/08/19 169 1081 2.4 75.3 372 0.013 0.425 1199.7
04/15/19 165 997 7.4 66.9 349 0.039 1.221 1208.1
04/22/19 171 996 10.8 71.6 346 0.057 1.776 1220.7
04/29/19 162 809 1.5 72.0 280 0.008 0.204 1222.1
05/06/19 167 617 3.6 73.0 213 0.019 0.365 1224.6
05/13/19 165 943 4.2 70.6 328 0.022 0.651 1229.1
05/21/19 193 918 0.6 75.4 316 0.003 0.094 1229.9
05/28/19 165 1019 1.1 78.1 349 0.006 0.174 1231.1
06/03/19 143 933 3.1 72.9 323 0.016 0.468 1233.9
06/12/19 215 1200 0.0 70.0 418 0.000 0.005 1233.9
06/17/19 119 1188 3.6 79.1 406 0.019 0.696 1237.3
06/24/19 165 1139 0.0 75.8 392 0.000 0.005 1237.4
07/01/19 172 1190 0.6 84.0 403 0.003 0.115 1238.2
07/08/19 73 1264 1.2 79.9 431 0.007 0.252 1239.0
07/15/19 167 1177 1.6 82.8 400 0.008 0.300 1241.1
07/26/19 76 1183 0.1 77.5 406 0.001 0.019 1241.1
07/29/19 70 1124 0.5 75.4 387 0.002 0.083 1241.4
08/26/19 611 607 3.3 80.8 207 0.018 0.325 1249.6
09/30/19 497 1018 0.3 74.9 351 0.002 0.050 1250.7
10/23/19 387 1060 0.0 67.5 370 0.000 0.000 1250.7
11/20/19 642 1188 3.4 63.0 419 0.018 0.678 1268.8
12/26/19 853 1012 0.3 63.8 356 0.002 0.051 1270.6
2 of 4
Table 2
Cumulative Mass of Volatilized Hydrocarbons
2022 Annual Monitoring Report - TC-341
August 2021 - July 2022
TH Conc
(C) (mg/l)
TH Recovery
Rate (M)
(lb/day)
Cumulative Mass
of Hydrocarbons
Recovered (lbs)
CommentsDate
Air Diffuser
Blower
Hours of
Operation
(Hrs)
Vapor
Velocity
(ft/min)
Vapor
Concentration
(PPM)
Temperature (°F)
Calculated
Vapor
Flowrate (Q)
(SCFM)
01/06/20 263 864 8.9 66.1 303 0.047 1.283 1284.7
01/13/20 166 811 7.4 64.6 285 0.039 1.004 1291.6
01/30/20 307 1220 2.5 60.6 432 0.013 0.514 1298.2
02/05/20 141 1638 0.3 69.2 571 0.002 0.081 1298.7
02/10/20 109 720 0.3 67.9 251 0.002 0.036 1298.8
02/24/20 187 1035 5.6 59.4 367 0.030 0.979 1306.5
03/04/20 210 840 0.1 61.3 297 0.001 0.014 1306.6
03/09/20 117 1175 0.8 64.1 413 0.004 0.157 1307.3
03/20/20 234 1425 0.6 72.4 493 0.003 0.141 1308.7
03/23/20 73 1185 0.1 64.4 417 0.001 0.020 1308.8
04/03/20 256 1025 0.4 65.1 360 0.002 0.069 1309.5
04/06/20 72 1130 0.1 72.9 391 0.001 0.019 1309.6
04/14/20 142 1185 0.1 73.5 409 0.001 0.019 1309.7
04/22/20 188 955 0.2 66.4 334 0.001 0.032 1309.9
04/27/20 108 1172 0.2 68.2 409 0.001 0.039 1310.1
05/04/20 166 1015 1.3 72.2 352 0.007 0.218 1311.6
05/11/20 89 1085 1.7 71.5 376 0.009 0.305 1312.7
05/19/20 190 998 0.2 67.8 349 0.001 0.033 1313.0
05/26/20 160 805 0.3 71.2 279 0.002 0.040 1313.3
06/05/20 182 1115 0.5 75.1 384 0.003 0.091 1314.0
06/12/20 113 1090 0.3 76.3 375 0.002 0.054 1314.2
06/18/20 119 1286 0.3 70.7 447 0.002 0.064 1314.5
07/31/20 700 939 0.4 75.8 323 0.002 0.062 1316.3
08/07/20 132 1109 0.5 77.1 381 0.003 0.091 1316.8
08/13/20 81 999 0.1 85.3 338 0.000 0.008 1316.8
08/20/20 164 0 0.0 0.0 0 0.000 0.000 1316.8 NO DATA
08/31/20 261 938 0.9 81.5 319 0.005 0.141 1318.4
09/04/20 92 1021 2.2 76.3 351 0.012 0.368 1319.8
09/11/20 164 996 1.7 77.0 342 0.009 0.277 1321.7
09/17/20 144 874 0.2 76.4 300 0.001 0.021 1321.8
09/30/20 289 1053 1.0 74.6 363 0.005 0.169 1323.8
10/08/20 169 1172 0.6 75.5 404 0.003 0.115 1324.6
10/15/20 169 1050 4.3 74.2 362 0.023 0.746 1329.9
10/22/20 95 0 0.0 0.0 0 0.000 0.000 1329.9 NO DATA
10/30/20 191 1096 0.0 68.8 382 0.000 0.005 1329.9
11/05/20 144 750 0.0 68.4 262 0.000 0.000 1329.9
11/12/20 164 536 2.6 69.5 187 0.014 0.233 1331.5
11/19/20 171 1145 0.1 66.9 400 0.001 0.024 1331.7
11/30/20 261 1142 0.6 69.7 398 0.003 0.104 1332.8
12/03/20 70 1159 0.5 59.5 411 0.003 0.103 1333.1
12/10/20 110 1090 0.1 61.1 386 0.001 0.023 1333.2
12/17/20 166 1013 0.3 58.3 360 0.001 0.047 1333.6
12/30/20 311 751 1.0 55.8 268 0.005 0.131 1335.3
01/07/21 89 631 0.7 62.5 223 0.003 0.069 1335.5
01/15/21 171 598 1.2 61.7 211 0.006 0.116 1336.3
01/22/21 164 1013 0.6 60.8 359 0.003 0.094 1337.0
01/28/21 144 967 1.3 65.8 339 0.007 0.214 1338.3
02/04/21 131 1035 0.1 47.1 376 0.000 0.013 1338.3
02/11/21 167 888 0.1 59.2 315 0.001 0.019 1338.5
02/19/21 192 666 0.1 57.6 237 0.001 0.014 1338.6
02/25/21 143 597 4.1 59.9 212 0.022 0.408 1341.0
03/04/21 167 986 0.3 66.8 345 0.002 0.049 1341.4
03/11/21 169 1133 0.5 55.7 405 0.003 0.096 1342.0
03/19/21 197 1126 0.5 57.5 401 0.002 0.086 1342.7
03/31/21 276 638 0.3 58.2 227 0.001 0.030 1343.1
04/08/21 192 517 7.9 56.0 185 0.042 0.697 1348.6
04/15/21 172 306 1.9 67.8 107 0.010 0.094 1349.3
04/22/21 164 263 4.7 64.4 92 0.025 0.205 1350.7
04/29/21 164 908 1.2 60.3 322 0.006 0.176 1351.9
05/06/21 171 829 1.2 74.5 286 0.006 0.156 1353.0
05/14/21 185 829 1.0 58.2 295 0.005 0.137 1354.1
05/20/21 144 809 0.3 65.5 284 0.001 0.034 1354.3
05/27/21 120 660 10.2 75.7 227 0.054 1.099 1359.8
06/04/21 192 604 4.2 74.6 208 0.022 0.414 1363.1
06/10/21 137 473 5.5 75.0 163 0.029 0.423 1365.5
06/17/21 167 358 4.0 75.7 123 0.021 0.233 1367.1
06/24/21 166 203 4.6 73.3 70 0.025 0.154 1368.2
07/09/21 313 902 0.3 82.3 307 0.001 0.040 1368.7
07/15/21 148 882 0.3 80.0 301 0.002 0.043 1369.0
07/22/21 168 733 0.3 74.9 253 0.001 0.033 1369.2
3 of 4
Table 2
Cumulative Mass of Volatilized Hydrocarbons
2022 Annual Monitoring Report - TC-341
August 2021 - July 2022
TH Conc
(C) (mg/l)
TH Recovery
Rate (M)
(lb/day)
Cumulative Mass
of Hydrocarbons
Recovered (lbs)
CommentsDate
Air Diffuser
Blower
Hours of
Operation
(Hrs)
Vapor
Velocity
(ft/min)
Vapor
Concentration
(PPM)
Temperature (°F)
Calculated
Vapor
Flowrate (Q)
(SCFM)
07/29/21 168 635 2.5 84.7 215 0.013 0.258 1371.0
08/12/21 327 543 1.4 76.3 187 0.007 0.124 1372.7
08/26/21 333 543 0.4 79.8 185 0.002 0.035 1373.2
09/13/21 415 811 0.3 74.0 280 0.002 0.040 1373.9
10/05/21 405 809 0.1 79.1 277 0.001 0.013 1374.1
10/20/21 328 809 0.0 79.2 277 0.000 0.000 1374.1
11/03/21 335 906 0.0 62.1 320 0.000 0.000 1374.1
11/23/21 405 780 0.0 61.7 276 0.000 0.000 1374.1
12/14/21 405 789 0.0 63.3 278 0.000 0.000 1374.1
12/22/21 245 795 0.0 65.2 279 0.000 0.000 1374.1
01/20/22 293 869 0.2 54.0 312 0.001 0.030 1374.5
02/07/22 424 982 0.2 52.0 354 0.001 0.034 1375.1
02/22/22 359 986 0.3 54.7 353 0.002 0.050 1375.8
03/14/22 476 1022 0.3 57.5 364 0.001 0.043 1376.7
04/08/22 299 973 0.3 59.5 345 0.001 0.041 1377.2
05/09/22 693 969 0.2 59.6 344 0.001 0.028 1378.0
06/14/22 601 1016 0.3 58.5 361 0.002 0.052 1379.3
06/30/22 314 983 0.1 59.0 349 0.001 0.017 1379.5
Average 1156 2.5 69.9 401.6 0.013 0.745
Notes:
SVE blower Hours of operation = value calculated between readings K = number of carbon atoms in calibration gas (1 in methane)
Vapor Velocity = flow measured at blower influent P = absolute pressure of flowstream (" Hg)
Q = vapor flowrate = (1-B) x V x A x (Tstd/T)Kg = 24.07 dsm^3/10^6 gm -mole
0.00
200.00
400.00
600.00
800.00
1000.00
1200.00
1400.00
1600.00
Lbs.Date
TC-341 Air Diffuser Blower - Cumulative Mass of Volatilized Hydrocarbons
4 of 4
,--,--
~
~
Table 3
Monthly Monitoring Well Gauging Data
2022 Annual Monitoring Report - TC-341
August 2021 - July 2022
USTTC341-MW01 15.99 8/16/2021 ND 4.25 NA 11.74 9/1/2021 ND 4.31 NA 11.68 10/5/2021 ND 4.41 NA 11.58
USTTC341-IW01 13.55 8/16/2021 ND 7.60 NA 5.95 9/1/2021 ND 4.94 NA 8.61 10/5/2021 ND 7.70 NA 5.85
USTTC341-IW04 14.60 8/16/2021 ND 6.80 NA 7.80 9/1/2021 ND 7.35 NA 7.25 10/5/2021 ND 7.42 NA 7.18
USTTC341-IW05 14.73 8/16/2021 ND 6.87 NA 7.86 9/1/2021 ND 7.63 NA 7.10 10/5/2021 ND 7.66 NA 7.07
USTTC341-IW06 14.76 8/16/2021 7.00 7.43 0.43 7.67 9/1/2021 7.43 7.69 0.26 7.28 10/5/2021 7.76 8.00 0.24 6.95
USTG480-MW03 13.89 8/16/2021 ND 7.95 NA 5.94 9/1/2021 ND 7.49 NA 6.40 10/5/2021 ND 7.58 NA 6.31
USTG480-MW04R 15.21 8/16/2021 ND 7.10 NA 8.11 9/1/2021 ND 7.44 NA 7.77 10/5/2021 ND 7.97 NA 7.24
USTG480-MW06 13.34 8/16/2021 ND 7.2 NA 6.14 9/1/2021 ND 7.31 NA 6.03 10/5/2021 ND 7.38 NA 5.96
USTG480-MW07 11.12 8/16/2021 ND* 5.83 NA 5.29 9/1/2021 ND* 6.19 NA 4.93 10/5/2021 ND* 5.45 NA 5.67
USTG480-MW08 12.94 8/16/2021 ND 7.43 NA 5.51 9/1/2021 ND 7.91 NA 5.03 10/5/2021 ND 7.23 NA 5.71
USTG480-MW13 13.03 8/16/2021 ND* 7.28 NA 5.75 9/1/2021 ND 7.78 NA 5.25 10/5/2021 7.57 7.62 0.05 5.45
USTG480-MW16 10.16 8/16/2021 ND 5.71 NA 4.45 9/1/2021 ND 6.20 NA 3.96 10/5/2021 ND 6.19 NA 3.97
USTG480-MW17 10.00 8/16/2021 ND 4.85 NA 5.15 9/1/2021 ND 5.21 NA 4.79 10/5/2021 ND 6.42 NA 3.58
USTG480-MW18 12.65 8/16/2021 ND 6.79 NA 5.86 9/1/2021 ND 7.27 NA 5.38 10/5/2021 ND 7.76 NA 4.89
USTG480-MW20 15.03 8/16/2021 ND 6.80 NA 8.23 9/1/2021 ND 7.12 NA 7.91 10/5/2021 ND* 7.82 NA 7.21
USTG480-MW23 14.83 8/16/2021 ND 5.37 NA 9.46 9/1/2021 ND 5.91 NA 8.92 10/5/2021 ND 6.44 NA 8.39
USTG480-MW26 9.09 8/16/2021 ND 3.90 NA 5.19 9/1/2021 ND 4.15 NA 4.94 10/5/2021 ND 4.10 NA 4.99
USTG480-MW28 10.31 8/16/2021 ND 5.58 NA 4.73 9/1/2021 ND 5.98 NA 4.33 10/5/2021 ND 4.83 NA 5.48
USTG480-MW29 9.01 8/16/2021 ND 4.05 NA 4.96 9/1/2021 ND 4.38 NA 4.63 10/5/2021 ND 3.75 NA 5.26
USTG480-MW30 8.86 8/16/2021 ND 3.64 NA 5.22 9/1/2021 ND 3.98 NA 4.88 10/5/2021 ND 3.94 NA 4.92
USTG480-MW31 13.99 8/16/2021 ND 7.15 NA 6.84 9/1/2021 ND 7.62 NA 6.37 10/5/2021 ND 7.74 NA 6.25
USTG480-MW32 13.92 8/16/2021 ND 7.9 NA 6.02 9/1/2021 ND 7.44 NA 6.48 10/5/2021 ND 7.48 NA 6.44
USTTC341-MW18 11.35 8/16/2021 ND 6.35 NA 5.00 9/1/2021 ND 6.55 NA 4.80 10/5/2021 ND 6.00 NA 5.35
IR35-MW67AR 14.51 8/16/2021 ND 7.29 NA 7.22 9/1/2021 ND 7.78 NA 6.73 10/5/2021 ND 8.02 NA 6.49
NOTES:
Monitoring wells USTG480-MW07, USTG480-MW13, and USTG480-MW20 are outfitted with free-phase product passive skimmers
*: No free-phase product was detected but was recovered in the passive skimmer
TOC: Top of well casing
MSL: Mean Sea Level
btoc: Below Top of Casing
1 Groundwater elevations adjusted to account for the presence of free product (Specific Gravity = 0.8).
ND: Not detected
NA: Not Applicable
Groundwater elevation datum is North American Vertical Datum.
Depth to
Product
(ft btoc)
Depth to
Water (ft
btoc)
Product
Thickness
(ft)
Groundwater
Elevation1
(ft MSL)
Depth to
Product
(ft btoc)
Depth to
Water
(ft btoc)
Product
Thickness
(ft)
Groundwater
Elevation1
(ft MSL)
Depth to
Water
(ft btoc)
Date
Measured
Product
Thickness
(ft)
Date
Measured
Groundwater
Elevation1
(ft MSL)
Well ID Date
Measured
Depth to
Product
(ft btoc)
TOC
Elevation
(ft MSL)
1 of 4
Table 3
Monthly Monitoring Well Gauging Data
2022 Annual Monitoring Report - TC-341
August 2021 - July 2022
USTTC341-MW01 15.99 11/2/2021 ND 5.86 NA 10.13 12/3/2021 ND 6.24 NA 9.75 1/12/2022 ND 6.31 NA 9.68
USTTC341-IW01 13.55 11/2/2021 ND 7.84 NA 5.71 12/3/2021 ND 7.98 NA 5.57 1/12/2022 ND 8.12 NA 5.43
USTTC341-IW04 14.60 11/2/2021 ND 7.61 NA 6.99 12/3/2021 ND 8.12 NA 6.48 1/12/2022 ND 8.21 NA 6.39
USTTC341-IW05 14.73 11/2/2021 ND 7.87 NA 6.86 12/3/2021 ND 7.35 NA 7.38 1/12/2022 ND 7.46 NA 7.27
USTTC341-IW06 14.76 11/2/2021 ND 7.46 NA 7.30 12/3/2021 ND 7.19 NA 7.57 1/12/2022 ND 7.28 NA 7.48
USTG480-MW03 13.89 11/2/2021 ND 7.74 NA 6.15 12/3/2021 ND 7.98 NA 5.91 1/12/2022 ND 8.07 NA 5.82
USTG480-MW04R 15.21 11/2/2021 ND 8.20 NA 7.01 12/3/2021 ND 9.76 NA 5.45 1/12/2022 ND 9.81 NA 5.40
USTG480-MW06 13.34 11/2/2021 8.00 8.21 0.21 5.30 12/3/2021 8.00 9.33 1.33 5.07 1/12/2022 ND 9.38 NA 3.96
USTG480-MW07 11.12 11/2/2021 ND 5.82 NA 5.30 12/3/2021 ND 4.89 NA 6.23 1/12/2022 ND* 5.02 NA 6.10
USTG480-MW08 12.94 11/2/2021 7.34 7.39 0.05 5.59 12/3/2021 7.13 7.34 0.21 5.60 1/12/2022 ND 7.34 NA 5.60
USTG480-MW13 13.03 11/2/2021 ND* 7.83 NA 5.20 12/3/2021 ND* 8.44 NA 4.59 1/12/2022 ND* 8.52 NA 4.51
USTG480-MW16 10.16 11/2/2021 ND 6.30 NA 3.86 12/3/2021 ND 7.44 NA 2.72 1/12/2022 ND 7.53 NA 2.63
USTG480-MW17 10.00 11/2/2021 ND 8.36 NA 1.64 12/3/2021 ND 8.33 NA 1.67 1/12/2022 ND 8.44 NA 1.56
USTG480-MW18 12.65 11/2/2021 ND 5.62 NA 7.03 12/3/2021 ND 7.66 NA 4.99 1/12/2022 ND 7.71 NA 4.94
USTG480-MW20 15.03 11/2/2021 ND* 10.45 NA 4.58 12/3/2021 ND 11.05 NA 3.98 1/12/2022 ND* 11.21 NA 3.82
USTG480-MW23 14.83 11/2/2021 ND 6.82 NA 8.01 12/3/2021 ND 6.98 NA 7.85 1/12/2022 ND 7.08 NA 7.75
USTG480-MW26 9.09 11/2/2021 ND 4.27 NA 4.82 12/3/2021 ND 5.23 NA 3.86 1/12/2022 ND 5.29 NA 3.80
USTG480-MW28 10.31 11/2/2021 ND 5.05 NA 5.26 12/3/2021 ND 5.59 NA 4.72 1/12/2022 ND 5.71 NA 4.60
USTG480-MW29 9.01 11/2/2021 ND 3.97 NA 5.04 12/3/2021 ND 4.19 NA 4.82 1/12/2022 ND 4.28 NA 4.73
USTG480-MW30 8.86 11/2/2021 ND 4.11 NA 4.75 12/3/2021 ND 5.32 NA 3.54 1/12/2022 ND 5.44 NA 3.42
USTG480-MW31 13.99 11/2/2021 ND 7.87 NA 6.12 12/3/2021 ND 8.46 NA 5.53 1/12/2022 ND 8.51 NA 5.48
USTG480-MW32 13.92 11/2/2021 ND 7.65 NA 6.27 12/3/2021 ND 7.26 NA 6.66 1/12/2022 ND 7.32 NA 6.60
USTTC341-MW18 11.35 11/2/2021 ND 6.12 NA 5.23 12/3/2021 ND 6.81 NA 4.54 1/12/2022 ND 6.89 NA 4.46
IR35-MW67AR 14.51 11/2/2021 ND 8.17 NA 6.34 12/3/2021 ND 8.49 NA 6.02 1/12/2022 ND 8.57 NA 5.94
NOTES:
Monitoring wells USTG480-MW07, USTG480-MW13, and USTG480-MW20 are outfitted with free-phase product passive skimmers
*: No free-phase product was detected but was recovered in the passive skimmer
TOC: Top of well casing
MSL: Mean Sea Level
btoc: Below Top of Casing
1 Groundwater elevations adjusted to account for the presence of free product (Specific Gravity = 0.8).
ND: Not detected
NA: Not Applicable
Groundwater elevation datum is North American Vertical Datum.
Product
Thickness
(ft)
Groundwater
Elevation1
(ft MSL)
Depth to
Water (ft
btoc)
Product
Thickness
(ft)
Groundwater
Elevation1
(ft MSL)
Depth to
Product
(ft btoc)
Depth to
Water
(ft btoc)
TOC
Elevation
(ft MSL)
Depth to
Product
(ft btoc)
Depth to
Water
(ft btoc)
Product
Thickness
(ft)
Groundwater
Elevation1
(ft MSL)
Depth to
Product
(ft btoc)
Date
MeasuredWell ID Date
Measured
Date
Measured
2 of 4
Table 3
Monthly Monitoring Well Gauging Data
2022 Annual Monitoring Report - TC-341
August 2021 - July 2022
USTTC341-MW01 15.99 2/3/2022 ND 7.67 NA 8.32 3/1/2022 ND 7.81 NA 8.18 4/4/2022 ND 7.60 NA 8.39
USTTC341-IW01 13.89 2/3/2022 ND 8.15 NA 5.74 3/1/2022 ND 8.78 NA 5.11 4/4/2022 ND 8.17 NA 5.72
USTTC341-IW04 15.21 2/3/2022 ND 7.49 NA 7.72 3/1/2022 ND 7.67 NA 7.54 4/4/2022 ND 6.95 NA 8.26
USTTC341-IW05 13.34 2/3/2022 ND 7.53 NA 5.81 3/1/2022 ND 8.95 NA 4.39 4/4/2022 ND 7.64 NA 5.70
USTTC341-IW06 11.12 2/3/2022 ND 7.42 NA 3.70 3/1/2022 ND 8.55 NA 2.57 4/4/2022 ND 7.35 NA 3.77
USTG480-MW03 12.94 2/3/2022 ND 7.66 NA 5.28 3/1/2022 ND 8.7 NA 4.24 4/4/2022 ND 7.48 NA 5.46
USTG480-MW04R 13.03 2/3/2022 ND 7.04 NA 5.99 3/1/2022 ND 8.19 NA 4.84 4/4/2022 ND 7.21 NA 5.82
USTG480-MW06 10.16 2/3/2022 ND 7.31 NA 2.85 3/1/2022 ND 7.4 NA 2.76 4/4/2022 ND 7.22 NA 2.94
USTG480-MW07 10.00 2/3/2022 ND* 5.98 NA 4.02 3/1/2022 ND* 7.15 NA 2.85 4/4/2022 ND 6.88 NA 3.12
USTG480-MW08 12.65 2/3/2022 7.64 7.74 0.10 4.99 3/1/2022 8.55 8.77 0.22 4.06 4/4/2022 8.42 8.55 0.13 4.20
USTG480-MW13 15.03 2/3/2022 ND 7.90 NA 7.13 3/1/2022 ND* 8.68 NA 6.35 4/4/2022 ND 8.53 NA 6.50
USTG480-MW16 10.16 2/3/2022 ND 5.75 NA 4.41 3/1/2022 ND 5.78 NA 4.38 4/4/2022 ND 5.98 NA 4.18
USTG480-MW17 10.00 2/3/2022 ND 5.45 NA 4.55 3/1/2022 ND 5.51 NA 4.49 4/4/2022 ND 5.71 NA 4.29
USTG480-MW18 12.65 2/3/2022 ND 7.76 NA 4.89 3/1/2022 ND 7.81 NA 4.84 4/4/2022 ND 7.75 NA 4.90
USTG480-MW20 14.83 2/3/2022 ND* 8.13 NA 6.70 3/1/2022 ND* 7.95 NA 6.88 4/4/2022 7.68 7.80 0.12 7.13
USTG480-MW23 14.83 2/3/2022 ND 7.65 NA 7.18 3/1/2022 ND 6.51 NA 8.32 4/4/2022 ND 6.49 NA 8.34
USTG480-MW26 10.31 2/3/2022 ND 4.55 NA 5.76 3/1/2022 ND 4.18 NA 6.13 4/4/2022 ND 3.88 NA 6.43
USTG480-MW28 9.01 2/3/2022 ND 4.02 NA 4.99 3/1/2022 ND 6.25 NA 2.76 4/4/2022 ND 6.44 NA 2.57
USTG480-MW29 8.86 2/3/2022 ND 3.78 NA 5.08 3/1/2022 ND 4.01 NA 4.85 4/4/2022 ND 4.03 NA 4.83
USTG480-MW30 8.86 2/3/2022 ND 3.75 NA 5.11 3/1/2022 ND 4.22 NA 4.64 4/4/2022 ND 4.31 NA 4.55
USTG480-MW31 13.99 2/3/2022 ND 7.85 NA 6.14 3/1/2022 ND 8.32 NA 5.67 4/4/2022 ND 8.01 NA 5.98
USTG480-MW32 13.92 2/3/2022 ND 7.47 NA 6.45 3/1/2022 ND 8.09 NA 5.83 4/4/2022 ND 7.69 NA 6.23
USTTC341-MW18 11.35 2/3/2022 ND 7.76 NA 3.59 3/1/2022 ND 7.95 NA 3.40 4/4/2022 ND 8.09 NA 3.26
IR35-MW67AR 14.51 2/3/2022 ND 8.00 NA 6.51 3/1/2022 ND 8.41 NA 6.10 4/4/2022 ND 7.95 NA 6.56
NOTES:
Monitoring wells USTG480-MW07, USTG480-MW13, and USTG480-MW20 are outfitted with free-phase product passive skimmers
*: No free-phase product was detected but was recovered in the passive skimmer
TOC: Top of well casing
MSL: Mean Sea Level
btoc: Below Top of Casing
1 Groundwater elevations adjusted to account for the presence of free product (Specific Gravity = 0.8).
ND: Not detected
NA: Not Applicable
Groundwater elevation datum is North American Vertical Datum.
Depth to
Product
(ft btoc)
Depth to
Water
(ft btoc)
Product
Thickness
(ft)
Groundwater
Elevation1
(ft MSL)
Depth to
Product
(ft btoc)
Depth to
Water (ft
btoc)
Product
Thickness
(ft)
Groundwater
Elevation1
(ft MSL)
Depth to
Product
(ft btoc)
Depth to
Water
(ft btoc)
Product
Thickness
(ft)
Groundwater
Elevation1
(ft MSL)
TOC
Elevation
(ft MSL)
Date
MeasuredWell ID Date
Measured
Date
Measured
3 of 4
Table 3
Monthly Monitoring Well Gauging Data
2022 Annual Monitoring Report - TC-341
August 2021 - July 2022
USTTC341-MW01 15.99 5/9/2022 ND 8.07 NA 7.92 6/15/2022 ND 6.37 NA 9.62
USTTC341-IW01 12.94 5/9/2022 ND 8.95 NA 3.99 6/15/2022 ND 8.19 NA 4.75
USTTC341-IW04 13.03 5/9/2022 ND 7.47 NA 5.56 6/15/2022 ND 8.25 NA 4.78
USTTC341-IW05 10.16 5/9/2022 ND 7.29 NA 2.87 6/15/2022 ND 7.51 NA 2.65
USTTC341-IW06 10.00 5/9/2022 ND 7.55 NA 2.45 6/15/2022 ND 7.32 NA 2.68
USTG480-MW03 12.65 5/9/2022 ND 7.76 NA 4.89 6/15/2022 ND 8.01 NA 4.64
USTG480-MW04R 15.03 5/9/2022 ND 7.85 NA 7.18 6/15/2022 ND 9.74 NA 5.29
USTG480-MW06 10.16 5/9/2022 ND 7.43 NA 2.73 6/15/2022 ND 9.41 NA 0.75
USTG480-MW07 10.00 5/9/2022 ND 6.49 NA 3.51 6/15/2022 ND* 5.09 NA 4.91
USTG480-MW08 12.65 5/9/2022 ND 8.83 NA 3.82 6/15/2022 ND 7.38 NA 5.27
USTG480-MW13 14.83 5/9/2022 ND 8.74 NA 6.09 6/15/2022 ND* 8.59 NA 6.24
USTG480-MW16 10.16 5/9/2022 ND 5.86 NA 4.30 6/15/2022 ND 7.61 NA 2.55
USTG480-MW17 10.00 5/9/2022 ND 5.60 NA 4.40 6/15/2022 ND 8.48 NA 1.52
USTG480-MW18 12.65 5/9/2022 ND 7.84 NA 4.81 6/15/2022 ND 7.80 NA 4.85
USTG480-MW20 14.83 5/9/2022 7.51 7.64 0.13 7.29 6/15/2022 ND* 11.27 NA 3.56
USTG480-MW23 14.83 5/9/2022 ND 6.61 NA 8.22 6/15/2022 ND 7.14 NA 7.69
USTG480-MW26 9.01 5/9/2022 ND 3.71 NA 5.30 6/15/2022 ND 5.23 NA 3.78
USTG480-MW28 8.86 5/9/2022 ND 6.32 NA 2.54 6/15/2022 ND 5.74 NA 3.12
USTG480-MW29 8.86 5/9/2022 ND 4.11 NA 4.75 6/15/2022 ND 4.31 NA 4.55
USTG480-MW30 8.86 5/9/2022 ND 4.29 NA 4.57 6/15/2022 ND 5.41 NA 3.45
USTG480-MW31 13.99 5/9/2022 ND 8.09 NA 5.90 6/15/2022 ND 8.54 NA 5.45
USTG480-MW32 13.92 5/9/2022 ND 7.79 NA 6.13 6/15/2022 ND 7.29 NA 6.63
USTTC341-MW18 11.35 5/9/2022 ND 8.03 NA 3.32 6/15/2022 ND 6.81 NA 4.54
IR35-MW67AR 14.51 5/9/2022 ND 7.91 NA 6.60 6/15/2022 ND 8.53 NA 5.98
NOTES:
Monitoring wells USTG480-MW07, USTG480-MW13, and USTG480-MW20 are outfitted with free-phase product passive skimmers
*: No free-phase product was detected but was recovered in the passive skimmer
TOC: Top of well casing
MSL: Mean Sea Level
btoc: Below Top of Casing
1 Groundwater elevations adjusted to account for the presence of free product (Specific Gravity = 0.8).
ND: Not detected
NA: Not Applicable
Groundwater elevation datum is North American Vertical Datum.
TOC
Elevation
(ft MSL)
Groundwater
Elevation1
(ft MSL)
Depth to
Water
(ft btoc)
Depth to
Product
(ft btoc)
Depth to
Water (ft
btoc)
Product
Thickness
(ft)
Well ID
Groundwater
Elevation1
(ft MSL)
Depth to
Product
(ft btoc)
Date
Measured
Product
Thickness
(ft)
Date
Measured
4 of 4
Table 4
Weekly Recovery Well Gauging Data
2022 Annual Monitoring Report - TC-341
August 2021 - July 2022
USTTC341-RW01 12.02 shallow 8/2/2021 ND 6.32 NA 5.70 8/10/2021 ND 5.93 NA 6.09 8/18/2021 ND 5.84 NA 6.18 8/24/2021 ND 6.95 NA 5.07
USTTC341-RW02 11.70 shallow 8/2/2021 ND 6.13 NA 5.57 8/10/2021 ND 5.44 NA 6.26 8/18/2021 ND 5.74 NA 5.96 8/24/2021 ND 6.27 NA 5.43
USTTC341-RW03 12.07 shallow 8/2/2021 ND 6.97 NA 5.10 8/10/2021 ND 5.96 NA 6.11 8/18/2021 ND 7.49 NA 4.58 8/24/2021 ND 7.08 NA 4.99
USTTC341-RW04 12.20 shallow 8/2/2021 ND 7.69 NA 4.51 8/10/2021 ND 6.19 NA 6.01 8/18/2021 ND 8.77 NA 3.43 8/24/2021 ND 9.35 NA 2.85
USTTC341-RW05 10.36 shallow 8/2/2021 ND 7.73 NA 2.63 8/10/2021 ND 5.45 NA 4.91 8/18/2021 6.17 7.35 1.18 3.95 8/24/2021 ND 11.76 NA -1.40
USTTC341-RW06 10.96 shallow 8/2/2021 ND 9.50 NA 1.46 8/10/2021 ND 8.64 NA 2.32 8/18/2021 ND 9.85 NA 1.11 8/24/2021 ND 9.35 NA 1.61
USTTC341-RW07 9.77 shallow 8/2/2021 ND 9.02 NA 0.75 8/10/2021 ND 5.95 NA 3.82 8/18/2021 12.34 12.70 0.36 -2.64 8/24/2021 ND 11.66 NA -1.89
RECOVERY SUMP NA NA 8/2/2021 ND 5.62 NA NA 8/10/2021 ND 5.23 NA NA 8/18/2021 5.24 5.51 0.27 NA 8/24/2021 ND 5.58 NA NA
USTTC341-RW01 12.02 shallow 9/2/2021 ND 6.17 NA 5.85 9/7/2021 ND 7.00 NA 5.02 9/13/2021 ND 7.26 NA 4.76 9/22/2021 ND 6.60 NA 5.42
USTTC341-RW02 11.70 shallow 9/2/2021 ND 5.96 NA 5.74 9/7/2021 ND 6.49 NA 5.21 9/13/2021 ND 6.51 NA 5.19 9/22/2021 ND 6.72 NA 4.98
USTTC341-RW03 12.07 shallow 9/2/2021 ND 7.35 NA 4.72 9/7/2021 ND 7.18 NA 4.89 9/13/2021 ND 7.14 NA 4.93 9/22/2021 ND 7.09 NA 4.98
USTTC341-RW04 12.20 shallow 9/2/2021 8.02 8.14 0.12 4.16 9/7/2021 7.83 7.87 0.04 4.36 9/13/2021 7.96 8.06 0.10 4.22 9/22/2021 ND 7.74 NA 4.46
USTTC341-RW05 10.36 shallow 9/2/2021 ND 9.35 NA 1.01 9/7/2021 9.11 9.60 0.49 1.15 9/13/2021 10.60 11.01 0.41 -0.32 9/22/2021 ND 9.81 NA 0.55
USTTC341-RW06 10.96 shallow 9/2/2021 ND 9.82 NA 1.14 9/7/2021 ND 9.86 NA 1.10 9/13/2021 ND 7.19 NA 3.77 9/22/2021 ND 7.04 NA 3.92
USTTC341-RW07 9.77 shallow 9/2/2021 ND 7.95 NA 1.82 9/7/2021 ND 10.65 NA -0.88 9/13/2021 ND 11.19 NA -1.42 9/22/2021 ND 8.12 NA 1.65
RECOVERY SUMP NA NA 9/2/2021 6.47 6.66 0.19 NA 9/7/2021 ND 10.54 NA NA 9/13/2021 ND 10.60 NA NA 9/22/2021 ND 10.58 NA NA
USTTC341-RW01 12.02 shallow 9/27/2021 ND 6.60 NA 5.42 10/6/2021 ND 6.63 NA 5.39 10/13/2021 ND 6.26 NA 5.76 10/18/2021 ND 6.38 NA 5.64
USTTC341-RW02 11.70 shallow 9/27/2021 ND 6.72 NA 4.98 10/6/2021 ND 6.35 NA 5.35 10/13/2021 ND 5.98 NA 5.72 10/18/2021 ND 6.06 NA 5.64
USTTC341-RW03 12.07 shallow 9/27/2021 ND 7.09 NA 4.98 10/6/2021 ND 6.95 NA 5.12 10/13/2021 ND 6.53 NA 5.54 10/18/2021 ND 7.30 NA 4.77
USTTC341-RW04 12.20 shallow 9/27/2021 ND 7.74 NA 4.46 10/6/2021 7.27 7.45 0.18 4.89 10/13/2021 6.12 6.32 0.20 6.04 10/18/2021 6.39 6.82 0.43 5.72
USTTC341-RW05 10.36 shallow 9/27/2021 ND 9.81 NA 0.55 10/6/2021 ND 8.67 NA 1.69 10/13/2021 ND 5.68 NA 4.68 10/18/2021 ND 5.75 NA 4.61
USTTC341-RW06 10.96 shallow 9/27/2021 ND 7.04 NA 3.92 10/6/2021 ND 7.28 NA 3.68 10/13/2021 ND 5.05 NA 5.91 10/18/2021 ND 4.89 NA 6.07
USTTC341-RW07 9.77 shallow 9/27/2021 ND 8.12 NA 1.65 10/6/2021 ND 13.04 NA -3.27 10/13/2021 ND 4.23 NA 5.54 10/18/2021 ND 4.20 NA 5.57
RECOVERY SUMP NA NA 9/27/2021 ND 10.58 NA NA 10/6/2021 ND 10.99 NA NA 10/13/2021 ND 7.98 NA NA 10/18/2021 ND 7.82 NA NA
USTTC341-RW01 12.02 shallow 10/25/2021 ND 6.74 NA 5.28 11/8/2021 ND 6.37 NA 5.65 11/15/2021 ND 6.26 NA 5.76 11/24/2021 ND 6.74 NA 5.28
USTTC341-RW02 11.70 shallow 10/25/2021 ND 6.62 NA 5.08 11/8/2021 ND 7.23 NA 4.47 11/15/2021 ND 6.97 NA 4.73 11/24/2021 ND 7.65 NA 4.05
USTTC341-RW03 12.07 shallow 10/25/2021 ND 6.93 NA 5.14 11/8/2021 ND 6.45 NA 5.62 11/15/2021 ND 6.33 NA 5.74 11/24/2021 ND 7.22 NA 4.85
USTTC341-RW04 12.20 shallow 10/25/2021 7.12 7.24 0.12 5.06 11/8/2021 6.12 6.36 0.24 6.03 11/15/2021 ND 6.87 NA 5.33 11/24/2021 5.77 5.89 0.12 6.41
USTTC341-RW05 10.36 shallow 10/25/2021 ND 6.49 NA 3.87 11/8/2021 ND 9.87 NA 0.49 11/15/2021 ND 9.23 NA 1.13 11/24/2021 ND 9.06 NA 1.30
USTTC341-RW06 10.96 shallow 10/25/2021 ND 6.29 NA 4.67 11/8/2021 ND 6.21 NA 4.75 11/15/2021 ND 6.81 NA 4.15 11/24/2021 ND 6.92 NA 4.04
USTTC341-RW07 9.77 shallow 10/25/2021 ND 11.82 NA -2.05 11/8/2021 ND 4.88 NA 4.89 11/15/2021 ND 5.18 NA 4.59 11/24/2021 ND 5.67 NA 4.10
RECOVERY SUMP NA NA 10/25/2021 ND 10.72 NA NA 11/8/2021 ND 7.82 NA NA 11/15/2021 ND 7.92 NA NA 11/24/2021 ND 8.33 NA NA
NOTES:
TOC: Top of well casing
MSL: Mean Sea Level
btoc: Below Top of Casing
1 Groundwater elevations adjusted to account for the presence of free product (Specific Gravity = 0.8).
ND: Not detected
NA: Not Available/Not Applicable
Groundwater elevation datum is North American Vertical Datum.
Product
Thickness
(ft)
Groundwater
Elevation1
(ft MSL)
Depth to
Product
(ft btoc)
Depth to
Water
(ft btoc)
Product
Thickness
(ft)
Groundwater
Elevation1
(ft MSL)
Depth to
Water
(ft btoc)
Product
Thickness
(ft)
Groundwater
Elevation1
(ft MSL)
Depth to
Product
(ft btoc)
Depth to
Water
(ft btoc)
Product
Thickness
(ft)
Groundwater
Elevation1
(ft MSL)
Depth to
Product
(ft btoc)
Depth to
Water
(ft btoc)
Product
Thickness
(ft)
Groundwater
Elevation1
(ft MSL)
Depth to
Water
(ft btoc)
Product
Thickness
(ft)
Groundwater
Elevation1
(ft MSL)
Date
Measured
Depth to
Product
(ft btoc)
Depth to
Water
(ft btoc)
Date
Measured
Depth to
Product
(ft btoc)
Depth to
Water
(ft btoc)
Product
Thickness
(ft)
Groundwater
Elevation1
(ft MSL)
Date
MeasuredWell ID
TOC
Elevation
(ft MSL)
Well
Type
(Depth)
Date
Measured
Depth to
Product
(ft btoc)
Depth to
Water
(ft btoc)
Product
Thickness
(ft)
Groundwater
Elevation1
(ft MSL)
Well ID
TOC
Elevation
(ft MSL)
Well
Type
(Depth)
Well ID
TOC
Elevation
(ft MSL)
Date
Measured
Well
Type
(Depth)
Date
Measured
Date
Measured
Date
MeasuredWell ID
TOC
Elevation
(ft MSL)
Well
Type
(Depth)
Date
Measured
Depth to
Product
(ft btoc)
Date
Measured
Depth to
Product
(ft btoc)
Depth to
Water
(ft btoc)
Product
Thickness
(ft)
Groundwater
Elevation1
(ft MSL)
Depth to
Product
(ft btoc)
Date
Measured
Depth to
Product
(ft btoc)
Depth to
Water
(ft btoc)
Product
Thickness
(ft)
Groundwater
Elevation1
(ft MSL)
Depth to
Water
(ft btoc)
Product
Thickness
(ft)
Groundwater
Elevation1
(ft MSL)
Date
Measured
Depth to
Product
(ft btoc)
Depth to
Water
(ft btoc)
Depth to
Product
(ft btoc)
Depth to
Product
(ft btoc)
Depth to
Water
(ft btoc)
Depth to
Water
(ft btoc)
Product
Thickness
(ft)
Groundwater
Elevation1
(ft MSL)
Groundwater
Elevation1
(ft MSL)
Date
Measured
Depth to
Product
(ft btoc)
Product
Thickness
(ft)
Groundwater
Elevation1
(ft MSL)
Product
Thickness
(ft)
Groundwater
Elevation1
(ft MSL)
Date
Measured
Depth to
Product
(ft btoc)
Depth to
Water
(ft btoc)
Product
Thickness
(ft)
Groundwater
Elevation1
(ft MSL)
Date
Measured
Depth to
Water
(ft btoc)
Product
Thickness
(ft)
Depth to
Product
(ft btoc)
Date
Measured
1 of 3
Table 4
Weekly Recovery Well Gauging Data
2022 Annual Monitoring Report - TC-341
August 2021 - July 2022
USTTC341-RW01 12.02 shallow 12/2/2021 ND 6.86 NA 5.16 12/6/2021 ND 6.86 NA 5.16 12/14/2021 ND 7.84 NA 4.18 12/22/2021 ND 7.92 NA 4.10
USTTC341-RW02 11.70 shallow 12/2/2021 ND 6.17 NA 5.53 12/6/2021 ND 6.17 NA 5.53 12/14/2021 ND 8.37 NA 3.33 12/22/2021 ND 9.23 NA 2.47
USTTC341-RW03 12.07 shallow 12/2/2021 ND 7.18 NA 4.89 12/6/2021 ND 7.18 NA 4.89 12/14/2021 ND 9.01 NA 3.06 12/22/2021 ND 9.87 NA 2.20
USTTC341-RW04 12.20 shallow 12/2/2021 ND 8.21 NA 3.99 12/6/2021 ND 8.21 NA 3.99 12/14/2021 ND 6.32 NA 5.88 12/22/2021 ND 6.11 NA 6.09
USTTC341-RW05 10.36 shallow 12/2/2021 ND 9.98 NA 0.38 12/6/2021 ND 9.98 NA 0.38 12/14/2021 ND 9.16 NA 1.20 12/22/2021 ND 10.74 NA -0.38
USTTC341-RW06 10.96 shallow 12/2/2021 ND 4.87 NA 6.09 12/6/2021 ND 4.87 NA 6.09 12/14/2021 ND 8.33 NA 2.63 12/22/2021 ND 9.33 NA 1.63
USTTC341-RW07 9.77 shallow 12/2/2021 ND 7.86 NA 1.91 12/6/2021 ND 7.86 NA 1.91 12/14/2021 ND 5.97 NA 3.80 12/22/2021 ND 6.64 NA 3.13
RECOVERY SUMP NA NA 12/2/2021 ND 7.23 NA NA 12/6/2021 ND 7.23 NA NA 12/14/2021 ND 8.59 NA NA 12/22/2021 ND 8.38 NA NA
USTTC341-RW01 12.02 shallow 1/20/2022 ND 6.45 NA 5.57 1/24/2022 ND 6.44 NA 5.58 1/31/2022 ND 7.42 NA 4.60 2/7/2022 ND 7.44 NA 4.58
USTTC341-RW02 11.70 shallow 1/20/2022 ND 12.65 NA -0.95 1/24/2022 ND 12.65 NA -0.95 1/31/2022 ND 12.77 NA -1.07 2/7/2022 ND 12.78 NA -1.08
USTTC341-RW03 12.07 shallow 1/20/2022 ND 6.83 NA 5.24 1/24/2022 ND 6.85 NA 5.22 1/31/2022 ND 10.55 NA 1.52 2/7/2022 ND 10.56 NA 1.51
USTTC341-RW04 12.20 shallow 1/20/2022 ND 8.10 NA 4.10 1/24/2022 ND 8.10 NA 4.10 1/31/2022 ND 8.84 NA 3.36 2/7/2022 ND 8.84 NA 3.36
USTTC341-RW05 10.36 shallow 1/20/2022 ND 10.10 NA 0.26 1/24/2022 ND 10.08 NA 0.28 1/31/2022 ND 9.94 NA 0.42 2/7/2022 ND 9.97 NA 0.39
USTTC341-RW06 10.96 shallow 1/20/2022 ND 5.83 NA 5.13 1/24/2022 ND 5.85 NA 5.11 1/31/2022 ND 16.91 NA -5.95 2/7/2022 ND 16.93 NA -5.97
USTTC341-RW07 9.77 shallow 1/20/2022 ND 6.75 NA 3.02 1/24/2022 ND 6.74 NA 3.03 1/31/2022 ND 7.33 NA 2.44 2/7/2022 ND 7.34 NA 2.43
RECOVERY SUMP NA NA 1/20/2022 ND 6.12 NA NA 1/24/2022 ND 6.10 NA NA 1/31/2022 ND 10.55 NA NA 2/7/2022 ND 10.56 NA NA
USTTC341-RW01 12.02 shallow 2/14/2022 ND 7.48 NA 4.54 2/22/2022 ND 7.39 NA 4.63 2/28/2022 ND 7.42 NA 4.60 3/14/2022 ND 7.39 NA 4.63
USTTC341-RW02 11.70 shallow 2/14/2022 ND 12.80 NA -1.10 2/22/2022 ND 12.79 NA -1.09 2/28/2022 ND 12.87 NA -1.17 3/14/2022 ND 12.71 NA -1.01
USTTC341-RW03 12.07 shallow 2/14/2022 ND 10.53 NA 1.54 2/22/2022 ND 10.51 NA 1.56 2/28/2022 ND 10.51 NA 1.56 3/14/2022 ND 10.48 NA 1.59
USTTC341-RW04 12.20 shallow 2/14/2022 ND 8.81 NA 3.39 2/22/2022 ND 8.81 NA 3.39 2/28/2022 ND 8.79 NA 3.41 3/14/2022 ND 8.81 NA 3.39
USTTC341-RW05 10.36 shallow 2/14/2022 ND 9.91 NA 0.45 2/22/2022 ND 9.94 NA 0.42 2/28/2022 ND 9.91 NA 0.45 3/14/2022 ND 9.87 NA 0.49
USTTC341-RW06 10.96 shallow 2/14/2022 ND 16.97 NA -6.01 2/22/2022 ND 16.93 NA -5.97 2/28/2022 ND 16.87 NA -5.91 3/14/2022 ND 16.91 NA -5.95
USTTC341-RW07 9.77 shallow 2/14/2022 ND 7.33 NA 2.44 2/22/2022 ND 7.34 NA 2.43 2/28/2022 ND 7.41 NA 2.36 3/14/2022 ND 7.29 NA 2.48
RECOVERY SUMP NA NA 2/14/2022 ND 10.55 NA NA 2/22/2022 ND 10.51 NA NA 2/28/2022 ND 10.50 NA NA 3/14/2022 ND 10.47 NA NA
USTTC341-RW01 12.02 shallow 3/30/2022 ND 7.39 NA 4.63 4/8/2022 ND 7.38 NA 4.64 4/11/2022 ND 7.31 NA 4.71 5/4/2022 ND 7.45 NA 4.57
USTTC341-RW02 11.70 shallow 3/30/2022 ND 12.41 NA -0.71 4/8/2022 ND 12.61 NA -0.91 4/11/2022 ND 12.59 NA -0.89 5/4/2022 ND 12.91 NA -1.21
USTTC341-RW03 12.07 shallow 3/30/2022 ND 10.37 NA 1.70 4/8/2022 ND 10.22 NA 1.85 4/11/2022 ND 10.21 NA 1.86 5/4/2022 ND 10.24 NA 1.83
USTTC341-RW04 12.20 shallow 3/30/2022 ND 8.79 NA 3.41 4/8/2022 ND 8.69 NA 3.51 4/11/2022 ND 8.68 NA 3.52 5/4/2022 ND 8.71 NA 3.49
USTTC341-RW05 10.36 shallow 3/30/2022 ND 9.91 NA 0.45 4/8/2022 ND 9.71 NA 0.65 4/11/2022 ND 9.69 NA 0.67 5/4/2022 ND 9.73 NA 0.63
USTTC341-RW06 10.96 shallow 3/30/2022 ND 16.94 NA -5.98 4/8/2022 ND 16.52 NA -5.56 4/11/2022 ND 16.51 NA -5.55 5/4/2022 ND 16.51 NA -5.55
USTTC341-RW07 9.77 shallow 3/30/2022 ND 7.34 NA 2.43 4/8/2022 ND 7.31 NA 2.46 4/11/2022 ND 7.32 NA 2.45 5/4/2022 ND 7.50 NA 2.27
RECOVERY SUMP NA NA 3/30/2022 ND 10.44 NA NA 4/8/2022 ND 10.42 NA NA 4/11/2022 ND 10.40 NA NA 5/4/2022 ND 10.41 NA NA
NOTES:
TOC: Top of well casing
MSL: Mean Sea Level
btoc: Below Top of Casing
1 Groundwater elevations adjusted to account for the presence of free product (Specific Gravity = 0.8).
ND: Not detected
NA: Not Available/Not Applicable
Groundwater elevation datum is North American Vertical Datum.
Depth to
Product
(ft btoc)
Date
Measured
Depth to
Product
(ft btoc)
Depth to
Water
(ft btoc)
Product
Thickness
(ft)
Well ID
TOC
Elevation
(ft MSL)
Well
Type
(Depth)
Well ID
TOC
Elevation
(ft MSL)
Date
Measured
Depth to
Product
(ft btoc)
Depth to
Water
(ft btoc)
Well
Type
(Depth)
Depth to
Water
(ft btoc)
Product
Thickness
(ft)
Date
Measured
Depth to
Product
(ft btoc)
Depth to
Water
(ft btoc)
Product
Thickness
(ft)
Well ID
TOC
Elevation
(ft MSL)
Well
Type
(Depth)
Depth to
Product
(ft btoc)
Depth to
Water
(ft btoc)
Date
Measured
Depth to
Product
(ft btoc)
Depth to
Water
(ft btoc)
Well ID
TOC
Elevation
(ft MSL)
Well
Type
(Depth)
Groundwater
Elevation1
(ft MSL)
Date
Measured
Depth to
Product
(ft btoc)
Depth to
Water
(ft btoc)
Product
Thickness
(ft)
Groundwater
Elevation1
(ft MSL)
Groundwater
Elevation1
(ft MSL)
Groundwater
Elevation1
(ft MSL)
Product
Thickness
(ft)
Groundwater
Elevation1
(ft MSL)
Date
Measured
Date
Measured
Product
Thickness
(ft)
Groundwater
Elevation1
(ft MSL)
Product
Thickness
(ft)
Groundwater
Elevation1
(ft MSL)
Date
Measured
Product
Thickness
(ft)
Groundwater
Elevation1
(ft MSL)
Date
Measured
Depth to
Product
(ft btoc)
Date
Measured
Depth to
Product
(ft btoc)
Product
Thickness
(ft)
Date
Measured
Depth to
Product
(ft btoc)
Depth to
Product
(ft btoc)
Depth to
Water
(ft btoc)
Depth to
Water
(ft btoc)
Depth to
Water
(ft btoc)
Product
Thickness
(ft)
Groundwater
Elevation1
(ft MSL)
Date
Measured
Depth to
Product
(ft btoc)
Depth to
Water
(ft btoc)
Groundwater
Elevation1
(ft MSL)
Product
Thickness
(ft)
Groundwater
Elevation1
(ft MSL)
Product
Thickness
(ft)
Groundwater
Elevation1
(ft MSL)
Product
Thickness
(ft)
Groundwater
Elevation1
(ft MSL)
Date
Measured
Depth to
Product
(ft btoc)
Depth to
Water
(ft btoc)
Product
Thickness
(ft)
Product
Thickness
(ft)
Groundwater
Elevation1
(ft MSL)
Groundwater
Elevation1
(ft MSL)
Date
Measured
Depth to
Product
(ft btoc)
Depth to
Water
(ft btoc)
Date
Measured
Depth to
Product
(ft btoc)
Depth to
Water
(ft btoc)
Date
Measured
Depth to
Product
(ft btoc)
Depth to
Water
(ft btoc)
Product
Thickness
(ft)
Groundwater
Elevation1
(ft MSL)
Depth to
Water
(ft btoc)
2 of 3
Table 4
Weekly Recovery Well Gauging Data
2022 Annual Monitoring Report - TC-341
August 2021 - July 2022
USTTC341-RW01 12.02 shallow 5/9/2022 ND 7.47 NA 4.55 5/16/2022 ND 7.42 NA 4.60 5/26/2022 ND 7.40 NA 4.62 6/6/2022 ND 7.38 NA 4.64
USTTC341-RW02 11.70 shallow 5/9/2022 ND 12.70 NA -1.00 5/16/2022 ND 12.67 NA -0.97 5/26/2022 ND 12.64 NA -0.94 6/6/2022 ND 12.61 NA -0.91
USTTC341-RW03 12.07 shallow 5/9/2022 ND 10.26 NA 1.81 5/16/2022 ND 10.24 NA 1.83 5/26/2022 ND 10.20 NA 1.87 6/6/2022 ND 10.17 NA 1.90
USTTC341-RW04 12.20 shallow 5/9/2022 ND 8.73 NA 3.47 5/16/2022 ND 8.70 NA 3.50 5/26/2022 ND 8.64 NA 3.56 6/6/2022 ND 8.65 NA 3.55
USTTC341-RW05 10.36 shallow 5/9/2022 ND 9.75 NA 0.61 5/16/2022 ND 9.71 NA 0.65 5/26/2022 ND 9.69 NA 0.67 6/6/2022 ND 9.67 NA 0.69
USTTC341-RW06 10.96 shallow 5/9/2022 ND 16.53 NA -5.57 5/16/2022 ND 16.49 NA -5.53 5/26/2022 ND 16.47 NA -5.51 6/6/2022 ND 16.45 NA -5.49
USTTC341-RW07 9.77 shallow 5/9/2022 ND 7.51 NA 2.26 5/16/2022 ND 7.49 NA 2.28 5/26/2022 ND 7.48 NA 2.29 6/6/2022 ND 7.41 NA 2.36
RECOVERY SUMP NA NA 5/9/2022 ND 10.44 NA NA 5/16/2022 ND 10.41 NA NA 5/26/2022 ND 10.40 NA NA 6/6/2022 ND 10.35 NA NA
USTTC341-RW01 12.02 shallow 6/14/2022 ND 7.35 NA 4.67 6/20/2022 ND 7.41 NA 4.61 6/29/2022 ND 7.40 NA 4.62 7/6/2022 ND 7.41 NA 4.61
USTTC341-RW02 11.70 shallow 6/14/2022 ND 12.63 NA -0.93 6/20/2022 ND 12.69 NA -0.99 6/29/2022 ND 12.63 NA -0.93 7/6/2022 ND 12.64 NA -0.94
USTTC341-RW03 12.07 shallow 6/14/2022 ND 10.19 NA 1.88 6/20/2022 ND 10.24 NA 1.83 6/29/2022 ND 10.15 NA 1.92 7/6/2022 ND 10.22 NA 1.85
USTTC341-RW04 12.20 shallow 6/14/2022 ND 8.67 NA 3.53 6/20/2022 ND 8.71 NA 3.49 6/29/2022 ND 8.66 NA 3.54 7/6/2022 ND 8.75 NA 3.45
USTTC341-RW05 10.36 shallow 6/14/2022 ND 9.68 NA 0.68 6/20/2022 ND 9.73 NA 0.63 6/29/2022 ND 9.69 NA 0.67 7/6/2022 ND 9.74 NA 0.62
USTTC341-RW06 10.96 shallow 6/14/2022 ND 16.48 NA -5.52 6/20/2022 ND 16.51 NA -5.55 6/29/2022 ND 16.48 NA -5.52 7/6/2022 ND 16.56 NA -5.60
USTTC341-RW07 9.77 shallow 6/14/2022 ND 7.43 NA 2.34 6/20/2022 ND 7.47 NA 2.30 6/29/2022 ND 7.44 NA 2.33 7/6/2022 ND 7.35 NA 2.42
RECOVERY SUMP NA NA 6/14/2022 ND 10.33 NA NA 6/20/2022 ND 10.36 NA NA 6/29/2022 ND 10.38 NA NA 7/6/2022 ND 10.32 NA NA
USTTC341-RW01 12.02 shallow 7/11/2022 ND 7.45 NA 4.57 7/19/2022 ND 7.46 NA 4.56 7/25/2022 ND 7.35 NA 4.67
USTTC341-RW02 11.70 shallow 7/11/2022 ND 12.61 NA -0.91 7/19/2022 ND 12.67 NA -0.97 7/25/2022 ND 12.59 NA -0.89
USTTC341-RW03 12.07 shallow 7/11/2022 ND 10.18 NA 1.89 7/19/2022 ND 10.24 NA 1.83 7/25/2022 ND 10.17 NA 1.90
USTTC341-RW04 12.20 shallow 7/11/2022 ND 8.74 NA 3.46 7/19/2022 ND 8.77 NA 3.43 7/25/2022 ND 8.69 NA 3.51
USTTC341-RW05 10.36 shallow 7/11/2022 ND 9.71 NA 0.65 7/19/2022 ND 9.71 NA 0.65 7/25/2022 ND 9.61 NA 0.75
USTTC341-RW06 10.96 shallow 7/11/2022 ND 16.53 NA -5.57 7/19/2022 ND 16.56 NA -5.60 7/25/2022 ND 16.49 NA -5.53
USTTC341-RW07 9.77 shallow 7/11/2022 ND 7.31 NA 2.46 7/19/2022 ND 7.36 NA 2.41 7/25/2022 ND 7.28 NA 2.49
RECOVERY SUMP NA NA 7/11/2022 ND 10.30 NA NA 7/19/2022 ND 10.29 NA NA 7/25/2022 ND 10.27 NA NA
NOTES:
TOC: Top of well casing
MSL: Mean Sea Level
btoc: Below Top of Casing
1 Groundwater elevations adjusted to account for the presence of free product (Specific Gravity = 0.8).
ND: Not detected
NA: Not Available/Not Applicable
Groundwater elevation datum is North American Vertical Datum.
Date
Measured
Depth to
Product
(ft btoc)
Depth to
Water
(ft btoc)
Product
Thickness
(ft)
Product
Thickness
(ft)
Groundwater
Elevation1
(ft MSL)
Depth to
Water
(ft btoc)
Product
Thickness
(ft)
Groundwater
Elevation1
(ft MSL)
Date
Measured
Depth to
Product
(ft btoc)
Depth to
Water
(ft btoc)
Depth to
Product
(ft btoc)
Depth to
Water
(ft btoc)
Product
Thickness
(ft)
Groundwater
Elevation1
(ft MSL)
Date
Measured
Depth to
Product
(ft btoc)
Groundwater
Elevation1
(ft MSL)
Date
MeasuredWell ID
TOC
Elevation
(ft MSL)
Well
Type
(Depth)
Well ID
TOC
Elevation
(ft MSL)
Well
Type
(Depth)
Date
Measured
Depth to
Product
(ft btoc)
Depth to
Water
(ft btoc)
Product
Thickness
(ft)
Groundwater
Elevation1
(ft MSL)
Date
Measured
Depth to
Product
(ft btoc)
Depth to
Water
(ft btoc)
Product
Thickness
(ft)
Groundwater
Elevation1
(ft MSL)
Date
Measured
Depth to
Product
(ft btoc)
Depth to
Water
(ft btoc)
Product
Thickness
(ft)
Groundwater
Elevation1
(ft MSL)
Well ID
TOC
Elevation
(ft MSL)
Well
Type
(Depth)
Date
Measured
Depth to
Product
(ft btoc)
Depth to
Water
(ft btoc)
Product
Thickness
(ft)
Groundwater
Elevation1
(ft MSL)
Date
Measured
Date
Measured
Depth to
Product
(ft btoc)
Depth to
Water
(ft btoc)
Product
Thickness
(ft)
Groundwater
Elevation1
(ft MSL)
Depth to
Product
(ft btoc)
Depth to
Water
(ft btoc)
Product
Thickness
(ft)
Groundwater
Elevation1
(ft MSL)
Date
Measured
Depth to
Product
(ft btoc)
Depth to
Water
(ft btoc)
Product
Thickness
(ft)
Groundwater
Elevation1
(ft MSL)
3 of 3
Table 5
Groundwater Elevation Data July 2022
2022 Annual Monitoring Report - TC-341
August 2021 - July 2022
Well ID Well Type
(Depth)
TOC
Elevation
(ft MSL)
Date
Measured
Depth to
Product
(ft btoc)
Depth to
Water
(ft btoc)
Product
Thickness
(ft)
Groundwater
Elevation1
(ft MSL)
USTTC341-RW01 shallow 12.02 7/5/2022 ND 12.87 NA -0.85
USTTC341-RW02 shallow 11.70 7/5/2022 ND 12.87 NA -1.17
USTTC341-RW03 shallow 12.07 7/5/2022 ND 10.48 NA 1.59
USTTC341-RW04 shallow 12.20 7/5/2022 ND 8.71 NA 3.49
USTTC341-RW05 shallow 10.36 7/5/2022 ND 9.81 NA 0.55
USTTC341-RW06 shallow 10.96 7/5/2022 ND 16.54 NA -5.58
USTTC341-RW07 shallow 9.77 7/5/2022 ND 7.49 NA 2.28
USTTC341-IW01 shallow 13.55 7/5/2022 ND 8.15 NA 5.40
USTTC341-IW02 shallow 13.90 7/5/2022 ND 8.26 NA 5.64
USTTC341-IW03 shallow 14.06 7/5/2022 ND 6.88 NA 7.18
USTTC341-IW04 shallow 14.60 7/5/2022 ND 5.96 NA 8.64
USTTC341-IW05 shallow 14.73 7/5/2022 ND 7.48 NA 7.25
USTTC341-IW06 shallow 14.76 7/5/2022 ND 7.71 NA 7.05
USTTC341-MW01 shallow 15.99 7/5/2022 ND 5.15 NA 10.84
USTTC341-MW02 shallow 16.07 7/5/2022 ND 9.75 NA 6.32
USTTC341-MW03 shallow 20.67 7/5/2022 ND 8.91 NA 11.76
USTTC341-MW05 shallow 19.95 7/5/2022 ND 9.04 NA 10.91
USTTC341-MW06 shallow 19.26 7/5/2022 ND 8.32 NA 10.94
USTTC341-MW08R shallow 16.73 7/5/2022 ND 7.71 NA 9.02
USTTC341-MW10 shallow 19.46 7/5/2022 ND 8.20 NA 11.26
USTTC341-MW11 shallow 19.36 7/5/2022 ND 8.61 NA 10.75
USTTC341-MW12 shallow 19.88 7/5/2022 ND 7.21 NA 12.67
USTTC341-MW13 shallow 16.66 7/5/2022 ND 6.75 NA 9.91
USTTC341-MW14R shallow 16.47 7/5/2022 ND 3.57 NA 12.90
USTTC341-MW17 shallow 16.34 7/5/2022 ND 8.11 NA 8.23
USTTC341-MW18 shallow 11.35 7/5/2022 ND 8.90 NA 2.45
USTG480-MW01 shallow 13.70 7/5/2022 ND 7.34 NA 6.36
USTG480-MW02 shallow 14.10 7/5/2022 ND 6.65 NA 7.45
USTG480-MW03 shallow 13.89 7/5/2022 ND 7.04 NA 6.85
USTG480-MW04R shallow 15.21 7/5/2022 ND 6.31 NA 8.90
USTG480-MW06 shallow 13.34 7/5/2022 ND 6.76 NA 6.58
USTG480-MW07 shallow 11.12 7/5/2022 ND 7.95 NA 3.17
USTG480-MW08 shallow 12.94 7/5/2022 7.80 8.45 0.65 5.01
USTG480-MW09R shallow 15.50 7/5/2022 ND 7.67 NA 7.83
USTG480-MW10 shallow 14.44 7/5/2022 ND 7.45 NA 6.99
USTG480-MW11 shallow 14.31 7/5/2022 ND 8.20 NA 6.11
USTG480-MW12 shallow 13.51 7/5/2022 ND 8.61 NA 4.90
USTG480-MW13 shallow 13.03 7/5/2022 ND 8.05 NA 4.98
USTG480-MW14 shallow 14.76 7/5/2022 ND 7.45 NA 7.31
USTG480-MW16 shallow 10.16 7/5/2022 ND 6.20 NA 3.96
USTG480-MW17 shallow 10.00 7/5/2022 ND 5.61 NA 4.39
USTG480-MW18 shallow 12.65 7/5/2022 ND 7.75 NA 4.90
USTG480-MW19 shallow 14.95 7/5/2022 ND 8.32 NA 6.63
USTG480-MW20 shallow 15.03 7/5/2022 ND 6.82 NA 8.21
USTG480-MW23 shallow 14.83 7/5/2022 ND 6.31 NA 8.52
USTG480-MW24 shallow 12.00 7/5/2022 ND 5.95 NA 6.05
USTG480-MW26 shallow 9.09 7/5/2022 ND 4.05 NA 5.04
USTG480-MW27 shallow 13.37 7/5/2022 ND 7.36 NA 6.01
USTG480-MW28 shallow 10.31 7/5/2022 ND 5.25 NA 5.06
USTG480-MW29 shallow 9.01 7/5/2022 ND 4.08 NA 4.93
USTG480-MW30 shallow 8.86 7/5/2022 ND 7.91 NA 0.95
USTG480-MW31 shallow 13.99 7/5/2022 ND 6.75 NA 7.24
USTG480-MW32 shallow 13.92 7/5/2022 ND 6.32 NA 7.60
USTG480-MW33R shallow 14.57 7/5/2022 ND 8.30 NA 6.27
IR35-MW09S shallow 18.92 7/5/2022 ND 8.15 NA 10.77
IR35-MW14S shallow 16.55 7/5/2022 ND 10.78 NA 5.77
IR35-MW31A shallow 17.10 7/5/2022 ND 10.45 NA 6.65
IR35-MW67AR shallow 14.51 7/5/2022 ND 7.61 NA 6.90
Recovery Sump shallow NA 7/5/2022 ND 10.61 NA NA
USTTC341-OW01 shallow NA 7/5/2022 ND 7.91 NA NA
USTTC341-OW02 shallow NA 7/5/2022 ND 8.23 NA NA
USTTC341-IS01 shallow NA 7/5/2022 ND 6.78 NA NA
USTTC341-IS03 shallow NA 7/5/2022 ND 7.18 NA NA
USTCGFF-EMW01 shallow NA 7/5/2022 ND 9.76 NA NA
USTTC341-MW09 intermediate 19.55 7/5/2022 ND 8.75 NA 10.80
USTTC341-MW15R intermediate 16.44 7/5/2022 ND 5.95 NA 10.49
USTG480-MW25 intermediate 13.26 7/5/2022 ND 6.19 NA 7.07
IR35-MW09IW intermediate 18.92 7/5/2022 ND 7.97 NA 10.95
IR35-MW14D intermediate 16.51 7/5/2022 ND 10.15 NA 6.36
IR35-MW31B intermediate 17.25 7/5/2022 ND 7.95 NA 9.30
USTG480-MW15 deep 13.80 7/5/2022 ND 6.35 NA 7.45
NOTES:
TOC: Top of well casing
MSL: Mean Sea Level
btoc: Below Top of Casing
1 Groundwater elevations adjusted to account for the presence of free product (Specific Gravity = 0.8).
ND: Not detected
NA: Not Available/Not Applicable
Groundwater elevation datum is North American Vertical Datum.
Table 6
Site Rehabilitation Goals for Chemicals of Concern
2022 Annual Monitoring Report - TC-341
August 2021 - July 2022
Benzene 190 300 300 257 197 167 1 ug/L
Ethlybenzene 270 450 420 335 307 333 600 ug/L
Isopropyl Ether 24 32 47 33.9 38.3 48.0 70 ug/L
Methyl tert-butyl ether 0.55 J BLOD BLOD BLOD BLOD BLOD 20 ug/L
Naphthalene 520 1,900 1,300 816 E 1,180 459 6 ug/L
Toluene 8.1 5.2 9.0 21.6 20.2 58.2 600 ug/L
m, -p Xylene 280 500 460 244 BLOD BLOD 500 ug/L
o-Xylene 19 95 54 107 BLOD BLOD 500 ug/L
Acenaphthene 5.0 J 180 J 20 7.32 J 22.6 J 10.7 J 80 ug/L
Benzo(a)anthracene BLOD BLOD BLOD BLOD BLOD BLOD 0.05 ug/L
Fluorene 9.0 J 410 42 29.7 J 29.1 20.7 J 300 ug/L
1-Methylnaphthalene 230 3,600 1,200 413 445 278 1 ug/L
2-Methylnaphthalene 330 7,100 1,800 653 950 336 30 ug/L
Phenanthrene 8.6 J 900 88 68 61.7 35.4 J 200 ug/L
C5-C8 Aliphatics 420 650 1,100 J 831 2,450 716 400 ug/L
C9-C18 Aliphatics 1,520 262,300 238,800 66,150 60,000 41,500 700 ug/L
C19-C36 Aliphatics 150 37,000 19,000 4,190 7,240 5,490 10,000 ug/L
C9-C22 Aromatics 3,100 155,100 115,300 31,640 42,600 28,230 200 ug/L
NOTES:
Maximum analyte concentrations presented each monitoring year.
NA: Not Applicable
BLOD: Below Limit Of Detection
##Exceedances of Target Cleanup goals highlighted yellow.
J: Indicates an estimated value
Maximum
Groundwater
(µg/L)
Component
Exceedances
Free-phase product
observed in USTG480-
MW05, USTG480-
MW07, USTG480-
MW20, USTG480-
MW28, USTTC341-IW4,
USTTC341-IW5
Free-phase product
observed in USTG480-
MW03, MW04R, MW06 to
MW08, MW13, MW20,
MW26, MW28, MW32,
USTTC341-RW05 to
RW07, OW01, IS01, IW01,
IW05, recovery sump
Free-phase product observed
in USTG480-MW03, MW04R,
MW06 to MW08, MW13,
MW20, MW28, MW29, MW31,
MW32, IR35-MW67AR,
USTTC341-RW01, RW03 to
RW07, OW01, OW02, IS01,
IW01, IW04 to IW06, recovery
sump
SM6200B (602 VOCs),
625/610, MADEP
EPH/VPH
NA
Analytical Method
Free-Phase
Product NA
Medium
Free-phase product
observed in
USTG480- MW08,
MW20, MW26,
MW28, OW02
2013 Conditions 2015 Conditions
Free-phase product
observed in USTG480-
MW03, MW04R, MW06 to
MW08, MW13, MW20,
MW26, MW28, MW32,
USTTC341-RW05 to
RW07, OW01, IS01, IW01,
IW05,
recovery sump
2014 Conditions 2017 Conditions2016 Conditions Target Cleanup
No free product
observed in any well
2018 Conditions
Free-phase product
observed in USTG480-
MW03, MW06 to MW08,
MW13, MW20, MW28,
MW32, USTTC341-RW01,
RW03, RW05 to RW07,
OW01, OW02, IS01,
recovery sump
1 of 2
Table 6
Site Rehabilitation Goals for Chemicals of Concern
2022 Annual Monitoring Report - TC-341
August 2021 - July 2022
Benzene 178 245 192 540 Q 1 ug/L
Ethlybenzene 363 289 272 312 Q 600 ug/L
Isopropyl Ether 47.0 38.6 4.93 5.69 70 ug/L
Methyl tert-butyl ether BLOD 0.128 J BLOD BLOD 20 ug/L
Naphthalene 968 265 291 923 Q 6 ug/L
Toluene 4.7 J 33.8 5.22 5.22 600 ug/L
m, -p Xylene 454* 375 346 398 500 ug/L
o-Xylene 454* 64 57.1 60.1 500 ug/L
Acenaphthene 7.9 6.37 90.9 17.7 80 ug/L
Benzo(a)anthracene BLOD BLOD 1.16 J BLOD 0.05 ug/L
Fluorene 15.1 8.48 127 22.3 300 ug/L
1-Methylnaphthalene 285 184 1,060 93.5 1 ug/L
2-Methylnaphthalene 404 266 1,600 118 30 ug/L
Phenanthrene 26.2 9.42 320 47.5 200 ug/L
C5-C8 Aliphatics 1,410 647 1,010 16,100 400 ug/L
C9-C18 Aliphatics 16,400 6,992 52,070 19,650 J 700 ug/L
C19-C36 Aliphatics 2,600 1,600 9,650 3,250 10,000 ug/L
C9-C22 Aromatics 16,130 E 5,050 37,750 16,820 J 200 ug/L
NOTES:
Maximum analyte concentrations presented each monitoring year.
NA: Not Applicable
BLOD: Below Limit Of Detection
##Exceedances of Target Cleanup goals highlighted yellow.
J: Indicates an estimated value
Q: Sample was prepared and/or analyzed past holding time, concentrations are considered minimum values.
*Total Xylenes value used.
No free product
observed in any
well
Free-phase product observed
in RW04, RW05, RW07, IW06,
USTG480-MW06, MW07,
MW08, MW13, MW20,
recovery sump
Free-phase product
observed in USTG480-
MW03, MW06,
MW07, MW08,
MW13, MW20,
MW26, OW01,
USTTC341-MW01,
IW05, IW06
Free-phase product observed
in USTTC341-MW01, RW03,
RW05, RW06, IW06,
USTG480-MW08, MW13,
MW20, MW26, recovery sump
Free-phase product observed
in USTG480-MW03, MW07,
MW08, MW13, MW20, MW23,
MW26, MW28, USTTC341-
RW03, RW05 to RW07, IW01,
IW05, IW06, MW01, recovery
sump
Free-Phase
Product NA NA
Maximum
Groundwater
(µg/L)
SM6200B (602 VOCs),
625/610, MADEP
EPH/VPH
2020 Conditions 2022 Conditions2019 Conditions Target CleanupMedium Analytical Method
Component
Exceedances 2021 Conditions
2 of 2
Table 7
Groundwater Analytical Results
2022 Annual Monitoring Report - TC-341
August 2021 - July 2022
Sample ID/Well ID Date
Collected
Well Type
(Depth)
USTG480-MW02 7/18/2022 shallow BLOD 169 BLOD 11 J BLOD BLOD BLOD BLOD BLOD 270 40 22.5 J BLOD BLOD 550 50.5 BLOD 286 80 BLOD 398 BLOD
USTG480-MW06 7/18/2022 shallow BLOD 148 BLOD BLOD BLOD 4.66 J BLOD BLOD BLOD 192 21.2 J 12.5 J BLOD BLOD 319 27.2 BLOD 147 41.6 BLOD 267 BLOD
USTG480-MW07 7/20/2022 shallow BLOD 63.5 Q 10.8 15.2 BLOD BLOD 0.317 J BLOD 0.645 J 47 Q 65.5 11.7 BLOD BLOD 286 Q 88.7 0.734 J 136 Q 15 BLOD 145.32 BLOD
USTG480-MW08 7/20/2022 shallow BLOD 119 10.1 J 10.9 J 2.8 J BLOD BLOD BLOD BLOD 203 43.9 9.42 J BLOD BLOD 606 65.8 BLOD 214 43.8 BLOD 125.9 J BLOD
USTG480-MW11 7/18/2022 shallow 11.6 J 0.423 J BLOD 0.448 J 0.505 J BLOD BLOD BLOD BLOD 15.3 14 0.381 J 1.7 J BLOD 72.7 15.5 0.641 J BLOD BLOD BLOD 1.964 J BLOD
USTG480-MW12 7/18/2022 shallow BLOD BLOD BLOD 0.287 J BLOD BLOD BLOD BLOD BLOD BLOD 0.288 J BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD
USTG480-MW13 7/20/2022 shallow 132 J 7.38 J 4.05 J 4.21 J 1.7 J BLOD BLOD BLOD BLOD 20.1 7.17 J 4.7 J BLOD BLOD 227 11.1 BLOD 69 31.1 BLOD 31.64 J BLOD
USTG480-MW14 7/21/2022 shallow BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD
USTG480-MW16 7/20/2022 shallow 13.2 J 0.119 J BLOD BLOD BLOD BLOD 3.07 BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD 3.95 BLOD BLOD
USTG480-MW17 7/20/2022 shallow 15.1 J BLOD BLOD 0.141 J BLOD BLOD BLOD BLOD BLOD BLOD 0.165 J BLOD BLOD BLOD 2.87 J 0.146 J BLOD BLOD BLOD BLOD BLOD BLOD
USTG480-MW18 7/20/2022 shallow BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD
USTG480-MW19 7/20/2022 shallow BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD
USTG480-MW20 7/20/2022 shallow 542 Q 61.1 5.99 J 7.59 J 1.64 J BLOD BLOD BLOD BLOD 156 25.8 7.43 J 23.7 J BLOD 479 39.8 5.01 J 194 66.6 BLOD 213.1 BLOD
USTG480-MW23 7/18/2022 shallow BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD 5.38 J 6.61 J BLOD BLOD BLOD 136 9.89 J BLOD 10.6 J 6.06 J BLOD 5.98 J BLOD
USTG480-MW26 7/20/2022 shallow BLOD 0.287 J 4.6 4.24 0.828 J BLOD BLOD BLOD BLOD 0.216 J 12.3 3.85 BLOD BLOD BLOD 19.6 0.394 J BLOD BLOD BLOD 0.711 J BLOD
USTG480-MW27 7/18/2022 shallow 30.5 J 0.372 J BLOD 1.17 0.309 J BLOD BLOD BLOD BLOD 1.91 1.82 5.41 2.29 J BLOD 33.7 2.25 1.01 J BLOD 0.155 J BLOD BLOD BLOD
USTG480-MW28 7/21/2022 shallow BLOD 80.4 7.09 J 8.01 J 1.51 J BLOD BLOD BLOD BLOD 42.7 31 7.42 J BLOD BLOD 446 46 BLOD 216 26.8 BLOD 114.28 J BLOD
USTG480-MW29 7/20/2022 shallow BLOD 540 Q 17.8 18.8 1.51 BLOD 5.69 BLOD 3.74 173 Q 81.6 4.68 BLOD BLOD 923 Q 157 Q 3.33 9.31 0.67 J 9.53 J Q 18.09 BLOD
USTG480-MW30 7/20/2022 shallow BLOD 2 BLOD 0.261 J 0.224 J BLOD 0.267 J BLOD 0.711 J BLOD 0.582 J 0.172 J BLOD 0.524 J BLOD 0.456 J BLOD BLOD BLOD 14.5 BLOD BLOD
USTG480-MW33R 7/20/2022 shallow BLOD BLOD 0.22 J 0.453 J BLOD BLOD BLOD BLOD BLOD BLOD 0.372 J BLOD BLOD BLOD BLOD 0.38 J BLOD BLOD BLOD BLOD BLOD BLOD
USTTC341-MW01 7/18/2022 shallow 12.1 J 0.28 J BLOD 0.297 J 0.158 J BLOD BLOD BLOD BLOD 1.1 1.23 0.128 J 2.11 J BLOD 3.36 J 1.48 BLOD BLOD BLOD BLOD BLOD BLOD
USTTC341-MW05 7/18/2022 shallow BLOD BLOD BLOD 0.858 J 0.567 J BLOD BLOD BLOD BLOD BLOD 0.242 J BLOD BLOD BLOD 2.76 J BLOD BLOD BLOD BLOD BLOD BLOD BLOD
USTTC341-MW08 7/18/2022 shallow BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD 1.27 J BLOD BLOD BLOD BLOD BLOD BLOD BLOD
USTTC341-MW13 7/18/2022 shallow BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD
USTTC341-MW14R 7/18/2022 shallow 1,590 8.07 J BLOD 3.07 J BLOD BLOD BLOD BLOD BLOD 20.5 15.2 3.21 J 30.2 J BLOD 145 18 BLOD 18 J BLOD BLOD 16 J BLOD
USTTC341-MW17 7/18/2022 shallow BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD
USTTC341-MW18 7/20/2022 shallow 22.6 J 19.7 1.08 1.61 0.257 J BLOD 0.332 J BLOD 2.31 2.85 7.39 BLOD BLOD BLOD 52.7 9.85 3.52 3.43 0.542 J BLOD 4.97 BLOD
IR35-MW67AR 7/20/2022 shallow BLOD 203 Q 12.3 16.6 1.25 BLOD BLOD BLOD BLOD 312 Q 59.4 13.9 1.3 J BLOD 523 Q 80.7 5.22 261 Q 3.25 BLOD 161.775 J BLOD
USTG480-MW25 7/18/2022 intermediate BLOD 1.1 BLOD BLOD BLOD BLOD 1.68 1.7 5.69 0.578 J BLOD BLOD BLOD BLOD 1.33 J 0.408 J BLOD 0.374 J 0.116 J 16.2 0.679 J BLOD
USTTC341-MW15R 7/20/2022 intermediate BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD 0.292 J BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD
19,000,000 6.9 NE NE NE NE NE NE 5,900 15 NE NE 1,900,000 4,000 20 200 16,000 210 150 25 320 Varies
6,000 1 70 70 70 NE 70 100 70 600 70 25 4,000 400 6 70 600 400 400 0.03 500 Varies
6,000,000 5,000 5,900 8,800 14,750 NE 70,000 100,000 70,000 80,000 30,500 11,700 4,000,000 400,000 6,000 26,100 260,000 24,100 24,100 30 50,000 Varies
NOTES:
Results and standards reported in µg/L
Detections in bold
VI GWSL: Vapor Intrusion Groundwater Screeing Level
NCAC 2L GWQS: North Carolina Administrative Code T15A:02L Groundwater Quality Standards
GCL: Gross Contaminant Levels
##Exceedances of the NCAC 2L GWQS highlighted in yellow.
##VI GWSL exceedances for monitoring wells within 30 ft of a building.
BLOD: Below Limit Of Detection
J: Indicates an estimated value
Q: Sample was prepared and/or analyzed past holding time, concentrations are considered minimum values.
NE: None Established All other VOCsSM 6200B - VOCsAnalytical Method
Contaminant of Concern
AcetoneBenzenen-Butylbenzenesec-Butylbenzene2-Chlorotoluenecis-1,2-DichloroetheneNC Non-Residential VI GWSL 1,3,5-TrimethylbenzeneVinyl chlorideTotal Xylenes2-Butanone (MEK)Methylene ChlorideNaphthalenen-Propylbenzenetrans-1,2-DichloroetheneDi-isopropyl ether (DIPE)EthylbenzeneIsopropylbenzenep-Isopropyltoluenetert-ButylbenzeneToluene1,2,4-TrimethylbenzeneGCL
NCAC 2L GWQS
1 of 3
Table 7
Groundwater Analytical Results
2022 Annual Monitoring Report - TC-341
August 2021 - July 2022
Sample ID/Well ID Date
Collected
Well Type
(Depth)
USTG480-MW02 7/18/2022 shallow 1.82 J BLOD BLOD BLOD BLOD BLOD 2.52 J 113 1.54 J BLOD BLOD BLOD BLOD 75.8 111 BLOD
USTG480-MW06 7/18/2022 shallow 0.972 J BLOD BLOD BLOD BLOD BLOD 0.711 J 59.1 0.407 J BLOD BLOD 0.509 J BLOD 26.4 36.2 BLOD
USTG480-MW07 7/20/2022 shallow 4.18 BLOD BLOD BLOD BLOD BLOD 4.81 195 4.16 BLOD BLOD BLOD BLOD BLOD BLOD BLOD
USTG480-MW08 7/20/2022 shallow 17.7 BLOD BLOD BLOD BLOD 0.994 J 22.3 289 47.5 BLOD 1.72 J BLOD BLOD BLOD BLOD BLOD
USTG480-MW11 7/18/2022 shallow 2.35 0.249 J BLOD BLOD BLOD BLOD 3.22 32.1 2.92 BLOD BLOD BLOD BLOD 74.8 5.68 BLOD
USTG480-MW12 7/18/2022 shallow 0.276 J BLOD BLOD BLOD BLOD BLOD 0.272 J 0.43 J BLOD BLOD BLOD BLOD BLOD 0.816 J 0.128 J BLOD
USTG480-MW13 7/20/2022 shallow 1.67 0.519 J BLOD BLOD BLOD BLOD 3.3 34.4 4.83 BLOD 0.187 J BLOD 5.37 J 51.8 55.2 BLOD
USTG480-MW14 7/21/2022 shallow BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD
USTG480-MW16 7/20/2022 shallow BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD
USTG480-MW17 7/20/2022 shallow BLOD BLOD BLOD BLOD BLOD BLOD BLOD 0.262 J BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD
USTG480-MW18 7/20/2022 shallow BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD
USTG480-MW19 7/20/2022 shallow BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD
USTG480-MW20 7/20/2022 shallow 2.58 J 0.594 J BLOD BLOD BLOD BLOD 4.08 J 99.5 4.35 J BLOD BLOD BLOD BLOD 82.7 94.5 BLOD
USTG480-MW23 7/18/2022 shallow 1.06 BLOD BLOD BLOD BLOD BLOD 1.77 23.7 1.54 BLOD BLOD BLOD BLOD 28.6 20.3 BLOD
USTG480-MW26 7/20/2022 shallow 2.44 0.323 J BLOD BLOD BLOD BLOD 3.89 BLOD 2.5 BLOD BLOD BLOD BLOD 46.6 41.2 BLOD
USTG480-MW27 7/18/2022 shallow 1.6 J4 BLOD BLOD BLOD BLOD 0.167 J 2.48 4.77 3.53 22.9 0.337 J BLOD BLOD 16.4 13.4 BLOD
USTG480-MW28 7/21/2022 shallow 3.25 0.665 J BLOD BLOD BLOD 0.106 J 5.26 111 6.55 BLOD 0.215 J BLOD BLOD 93.5 118 BLOD
USTG480-MW29 7/20/2022 shallow 3.69 0.395 J BLOD BLOD BLOD BLOD 4.84 185 5.42 BLOD BLOD BLOD BLOD BLOD BLOD BLOD
USTG480-MW30 7/20/2022 shallow BLOD BLOD BLOD BLOD BLOD BLOD BLOD 0.355 J BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD
USTG480-MW33R 7/20/2022 shallow BLOD BLOD BLOD BLOD BLOD BLOD 0.113 J 0.212 J BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD
USTTC341-MW01 7/18/2022 shallow 0.423 J BLOD BLOD BLOD BLOD BLOD 0.532 J 0.572 J BLOD BLOD BLOD BLOD BLOD 3.7 0.616 J BLOD
USTTC341-MW05 7/18/2022 shallow BLOD BLOD BLOD BLOD BLOD BLOD BLOD 0.469 J BLOD BLOD BLOD BLOD BLOD 0.286 J BLOD BLOD
USTTC341-MW08 7/18/2022 shallow BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD
USTTC341-MW13 7/18/2022 shallow BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD
USTTC341-MW14R 7/18/2022 shallow 2.49 J BLOD BLOD BLOD BLOD BLOD 2.45 J 26.3 1.72 J BLOD BLOD BLOD BLOD 25.8 20.5 BLOD
USTTC341-MW17 7/18/2022 shallow BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD
USTTC341-MW18 7/20/2022 shallow 0.571 J BLOD BLOD BLOD BLOD 0.18 J 1.06 BLOD BLOD BLOD 0.295 J BLOD BLOD BLOD BLOD BLOD
IR35-MW67AR 7/20/2022 shallow 3.15 BLOD 0.292 J 0.16 J 0.178 J 0.148 J 4.32 174 5.13 0.94 J 0.21 J BLOD BLOD BLOD BLOD BLOD
USTG480-MW25 7/18/2022 intermediate BLOD BLOD BLOD BLOD BLOD BLOD BLOD 0.478 J BLOD BLOD BLOD BLOD BLOD 0.279 J 0.309 J BLOD
USTTC341-MW15R 7/20/2022 intermediate BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD BLOD
NE NE NE NE NE NE NE 20 NE NE NE NE NE NE NE VARIES
80 2,000 0.05 200 0.005 300 300 6 200 3 200 NE 30 1 30 VARIES
2,120 2,000 0.75 200 0.8 300 845 6,000 550 135 200 NE 30,000 1,000 12,000 VARIES
NOTES:
Results and standards reported in µg/L
Detections in bold
VI GWSL: Vapor Intrusion Groundwater Screeing Level
NCAC 2L GWQS: North Carolina Administrative Code T15A:02L Groundwater Quality Standards
GCL: Gross Contaminant Levels
##Exceedances of the NCAC 2L GWQS highlighted in yellow.
##VI GWSL exceedances for monitoring wells within 30 ft of a building.
BLOD: Below Limit Of Detection
J: Indicates an estimated value
NE: None Established
EPA 625 - PAHs
AcenaphtheneAnthracene2,4-DimethylphenolPhenolNaphthalene2-MethylnaphthaleneAll other PAHsPhenanthrene1-MethylnaphthaleneBenzo(b)fluorantheneBenzo(g,h,i)peryleneBenzo(a)pyreneFluorantheneFluorenePyreneBis(2-ethylhexyl)phthalateAnalytical Method
Contaminant of Concern
NC Non-Residential VI GWSL
NCAC 2L GWQS
GCL
2 of 3
Table 7
Groundwater Analytical Results
2022 Annual Monitoring Report - TC-341
August 2021 - July 2022
Sample ID/Well ID Date
Collected
Well Type
(Depth)
USTG480-MW02 7/18/2022 shallow 518 J 1,690 1,550 2,360 106 J BLOD 1,796 J 3,910
USTG480-MW06 7/18/2022 shallow 387 1,130 815 1,030 63.8 J BLOD 1,193.8 J 1,845
USTG480-MW07 7/20/2022 shallow 336 1,230 1,000 1,730 335 87.6 J 1,565 2,730
USTG480-MW08 7/20/2022 shallow 16,100 2,150 J 1,920 J 14,900 17,500 3,250 19,650 J 16,820 J
USTG480-MW11 7/18/2022 shallow 42 J 254 344 650 123 J 56.2 J 377 J 994
USTG480-MW12 7/18/2022 shallow BLOD 62.2 J BLOD 79.8 J BLOD 37.1 J 62.2 J 79.8 J
USTG480-MW13 7/20/2022 shallow BLOD 755 J 835 J 2,050 1,910 397 2,665 J 2,885 J
USTG480-MW14 7/21/2022 shallow BLOD 54.7 J BLOD BLOD BLOD BLOD 54.7 J BLOD
USTG480-MW16 7/20/2022 shallow BLOD 40.3 J BLOD 47.3 J BLOD 33.3 J 40.3 J 47.3 J
USTG480-MW17 7/20/2022 shallow BLOD 73.9 J BLOD 142 145 54.6 J 218.9 J 142
USTG480-MW18 7/20/2022 shallow BLOD 47.8 J BLOD 46.2 J BLOD BLOD 47.8 J 46.2 J
USTG480-MW19 7/20/2022 shallow BLOD 37.5 J BLOD 67.1 J BLOD 35 J 37.5 J 67.1 J
USTG480-MW20 7/20/2022 shallow 439 J 1,420 1,160 1,600 1,200 198 2,620 2,760
USTG480-MW23 7/18/2022 shallow BLOD 708 J BLOD 5,290 10,600 1,810 11,308 J 5,290
USTG480-MW26 7/20/2022 shallow 107 J 303 353 1,610 1,330 333 1,633 1,963
USTG480-MW27 7/18/2022 shallow 60.4 J 179 217 1,100 2,000 652 2,179 1,327
USTG480-MW28 7/21/2022 shallow 185 B 599 701 2,110 2,120 420 2,719 2,811
USTG480-MW29 7/20/2022 shallow 554 692 778 1,610 72.1 J 38.1 J 764.1 J 2,388
USTG480-MW30 7/20/2022 shallow 35.4 J 138 59.1 J 47.6 J BLOD BLOD 138 106.7 J
USTG480-MW33R 7/20/2022 shallow BLOD 90.2 J BLOD 71.1 J BLOD 35.4 J 90.2 J 71.1 J
USTTC341-MW01 7/18/2022 shallow BLOD 67.8 J 78.2 J 252 160 98 J 227.8 J 330.2 J
USTTC341-MW05 7/18/2022 shallow BLOD 128 J 60.7 J 77.6 J 60.1 J 639 188.1 J 138.3 J
USTTC341-MW08 7/18/2022 shallow BLOD 111 J BLOD 62.2 J BLOD 115 J 111 J 62.2 J
USTTC341-MW13 7/18/2022 shallow BLOD BLOD BLOD 41.7 J BLOD 34.9 J BLOD 41.7 J
USTTC341-MW14R 7/18/2022 shallow BLOD 522 J 508 J 1,010 585 186 1,107 J 1,518 J
USTTC341-MW17 7/18/2022 shallow BLOD 37.7 J BLOD 47.2 J BLOD 36.6 J 37.7 J 47.2 J
USTTC341-MW18 7/20/2022 shallow 69.2 J 128 B J 122 727 1,040 244 1,168 J 849
IR35-MW67AR 7/20/2022 shallow 491 1,450 914 1,790 397 89.2 J 1,847 2,704
USTG480-MW25 7/18/2022 intermediate BLOD 58.3 J BLOD 55.2 J BLOD 51.9 J 58.3 J 55.2 J
USTTC341-MW15R 7/20/2022 intermediate BLOD BLOD BLOD 53.6 J BLOD 34.8 J BLOD 53.6 J
7.1 0.63 120 130 0.63 NE 0.63 120¹
400 NE NE NE 700 10,000 700 200
NE NE NE NE NE NE NE NE
NOTES:
Results and standards reported in µg/L
Detections in bold
VI GWSL: Vapor Intrusion Groundwater Screeing Level
NCAC 2L GWQS: North Carolina Administrative Code T15A:02L Groundwater Quality Standards
GCL: Gross Contaminant Levels
##Exceedances of the NCAC 2L GWQS highlighted in yellow.
##VI GWSL exceedances for monitoring wells within 30 ft of a building.
BLOD: Below Limit Of Detection
J: Indicates an estimated value
NE: None Established
1: The lower of the aromatic fractions was used as the VI GWSL.
MADEP VPH MADEP EPH MADEP VPH/EPHAnalytical Method
Unadjusted C9-C18 AliphaticsUnadjusted C19-C36 AliphaticsC9-C18 AliphaticsContaminant of Concern
Unadjusted C5-C8 AliphaticsC9-C22 AromaticsUnadjusted C9-C12 AliphaticsUnadjusted C9-C10 AromaticsUnadjusted C11-C22 AromaticsNC Non-Residential VI GWSL
NCAC 2L GWQS
GCL
3 of 3
Table 8
Proposed Monitoring Plan August 2022 to July 2023
2022 Annual Monitoring Report - TC-341
August 2021 - July 2022
Monitoring Wells to be
Gauged Monthly
Monitoring Wells to be
Sampled Annually
USTG480-MW03 USTG480-MW02
USTG480-MW06 USTG480-MW06
USTG480-MW07 USTG480-MW07
USTG480-MW08 USTG480-MW08
USTG480-MW13 USTG480-MW11
USTG480-MW20 USTG480-MW12
USTG480-MW26 USTG480-MW13
USTG480-MW28 USTG480-MW14
USTG480-MW29 USTG480-MW16
USTG480-MW31 USTG480-MW17
USTG480-MW32 USTG480-MW18
USTTC341-IW01 USTG480-MW20
USTTC341-IW06 USTG480-MW23
USTTC341-MW01 USTG480-MW25
USTTC341-MW18 USTG480-MW26
USTG480-MW27
USTG480-MW28
USTG480-MW29
USTG480-MW30
USTG480-MW33R
USTTC341-MW01
USTTC341-MW08
USTTC341-MW13
USTTC341-MW14
USTTC341-MW15
USTTC341-MW17
USTTC341-MW18
IR35-MW67AR
2022 Annual Monitoring Report – TC-341
MCAS New River, NC

FIGURES
(.'\ (HEROKEENATION™ ~ 3 S-Support, Service & Solutions
1,500-F
O
O
T
RADI
USUS

1
7NC 2
4
ANBAR STSIXTH ST
EIGHTH ST FALLUJAH STFOURTH ST
FIFTH ST
SEVENTH ST GARMSIR STEDSON RIDGE STUNN
A
M
E
DCHAPULTEPEC STSECO
N
D
S
T
DERNA STTHIRD ST
BETIO STUS 17 BUSN WHITE STUS
1
7
UNNAM
E
D
UNN
A
M
E
D
UNNA
M
E
DDERNA STNC 2
4
U
N
N
A
M
E
D
FIGUREPROJECT:TITLE:
1
TC-341
2022 ANNUAL MONITORING
REPORT
MARINE CORPS AIR STATION
NEW RIVER, NORTH CAROLINA
SITE VICINITY
AND RECEPTORS
Data Sources: GIS data layers provided by the MCB Camp Lejeune GIS Department, ESRI, and Cherokee Nation 3S.
500 0 500250 Feet
SCALE
PROJECT NO.:DATE:
221102 SEP 2022
LEGEND
Existing Building
Demolished Building
TC-341
D
D ~ D 5?□
IZZZA I D
ul
:.-,··
',,, ·----~~ ...
. ---... , . .-
1 Cherokee Nation 1s
USTTC341-RW07
USTTC341-RW06
USTTC341-RW05
USTTC341-RW03
USTTC341-RW02
USTTC341-RW04
USTTC341-RW01
IR35-MW31A
IR35-MW14S
IR35-MW09S
IR35-MW67AR
USTG480-MW18
USTG480-MW32
USTG480-MW31
USTG480-MW30
USTG480-MW29
USTG480-MW28
USTG480-MW27
USTG480-MW26
USTG480-MW24
USTG480-MW23
USTG480-MW20
USTG480-MW19
USTG480-MW17
USTG480-MW16
USTG480-MW14
USTG480-MW13
USTG480-MW12
USTG480-MW11
USTG480-MW10 USTG480-MW08
USTG480-MW07
USTG480-MW06
USTG480-MW03
USTG480-MW02
USTG480-MW01
USTTC341-IW06
USTTC341-IW03
USTTC341-IW05
USTTC341-IW04
USTTC341-MW18
USTCGFF-EMW05
USTTC341-IS03
USTTC341-IS02
USTTC341-IS01
USTTC341-MW12
USTTC341-MW01
USTTC341-MW02
USTTC341-MW03
USTTC341-MW05
USTGCFF-EMW01
USTTC341-MW17
USTTC341-MW13
USTTC341-MW11
USTTC341-MW10 USTTC341-MW08
USTTC341-MW06
USTG480-MW33R
USTG480-MW09R
USTG480-MW04R
USTTC341-MW14R USTTC341-IW02
USTTC341-IW01
USTTC341-OW01
USTTC341-OW02
IR35-MW31B
IR35-MW09IW
USTTC341-MW09
USTTC341-MW15R
USTG480-MW25
IR35-MW14D
USTG480-MW15
D STUS 17F STE STTHIRD ST NC 2
4
FOURTH ST
G ST
US

1
7
G480
TC341
TC342
TC460
TC362
G482
TC364
UNK382
FIGUREPROJECTTITLE
2
TC-341
2022 ANNUAL MONITORING
REPORT
MARINE CORPS AIR STATION
NEW RIVER, NORTH CAROLINA
SITE MAP WITH
WELL LOCATIONS
Data Sources: GIS data layers provided by the MCB Camp Lejeune GIS Department, ESRI, and/or Cherokee Nation 3S.
100 0 10050 Feet
SCALE
PROJECT NO.:DATE:
221102 SEP 2022
LEGEND
Injection Well
Inspection Sump
Observation Well
Monitoring Well
Intermediate Groundwater Monitoring Well
Deep Groundwater Monitoring Well
Recovery Well
Junction Vault
FreeProduct Recovery Line
Free-Product Recovery Trench
Former Fuel Lines
30-Foot VISL Boundary
Recovery Sump
Treatment System
FormerUSTs
Existing Building
Demolished Building
' Cherokee Nation JS
CJ
Cl
Cl
CJ -CJ
FIGUREPROJECTTITLE
3
TC-341
2022 ANNUAL MONITORING
REPORT
MARINE CORPS AIR STATION
NEW RIVER, NORTH CAROLINA
SYSTEM LAYOUT
Data Sources: GIS data layers provided by the MCB Camp Lejeune GIS Department, ESRI, and/or Cherokee Nation 3S.
NOT TO SCALE
PROJECT NO.:DATE:
221102 SEP 2022
3: rr w 8 w Q:'.
FENCED-IN TREATMENT SYSTEM COMPOUND
AlR SUPPLIED TO FPR SYSTEM
AIR
COMPRESSOR
30' x 45' CONCRETE CONTAINMENT PAD WITH 12" CONTAINMENT WALt
I
OILIW;,jrER
SEPARATOR
X -----~PRODUCT f I L TA K
~X~X~X*X
' Cherokee Nation JS
AIR DIFFUSER
BOX 1
AIR DIFFUSER
BOX2
TREATED WATER
HOL I GTANK
AIR DIFFUSER
BOX3
AIR DIFFUSER
BOX4
L:-_-_---~-------------_._.----~1
CONCRETE
SUMP
x~ x~x~x x~x*x~ ~
WI/VTP
:r.
I X
I X
I
i X
f X
I
IR35-MW09S
USTG480-MW30
USTTC341-MW18
USTCGFF-EMW05
USTTC341-IS03
USTTC341-IS01
USTGCFF-EMW01
USTG480-MW07
USTTC341-IS02
USTTC341-OW01
USTTC341-OW02
USTTC341-RW07
USTTC341-RW06
USTTC341-RW05
USTTC341-RW03
USTTC341-RW02
USTTC341-RW04
USTTC341-RW01
IR35-MW67AR
6.90
IR35-MW31A
6.65
IR35-MW14S
5.77
USTG480-MW18
4.9
USTG480-MW32
7.6
USTG480-MW12
4.90
IR35-MW09S
10.77
USTTC341-IW01
5.40
USTG480-MW31
7.24
USTG480-MW29
4.93
USTG480-MW28
5.06
USTG480-MW27
6.01
USTG480-MW26
5.04
USTG480-MW24
6.05
USTG480-MW23
8.52
USTG480-MW20
8.21
USTG480-MW19
6.63
USTG480-MW17
4.39
USTG480-MW14
7.31
USTG480-MW13
4.98
USTG480-MW11
6.11
USTG480-MW10
6.99
USTG480-MW08
5.01
USTG480-MW06
6.58
USTG480-MW04R
8.9
USTG480-MW03
6.85
USTG480-MW02
7.45
USTG480-MW01
6.36
USTTC341-IW06
7.05
USTTC341-IW03
7.18
USTTC341-IW02
5.64
USTTC341-IW05
7.25
USTTC341-IW04
8.64
USTTC341-MW02
6.32
USTTC341-MW17
8.23
USTTC341-MW13
9.91
USTTC341-MW08
9.02
USTG480-MW33R
6.27
USTG480-MW09R
7.83
USTTC341-MW12
12.67
USTTC341-MW01
10.84
USTTC341-MW03
11.76
USTTC341-MW05
10.91 USTTC341-MW14R
12.90
USTTC341-MW11
10.75
USTTC341-MW10
11.26
USTTC341-MW06
10.94
7
6
8
9
11
1
0
45
D STUS 17F STE STNC 2
4
THIRD ST
FOURTH ST
G ST
US

1
7
G480
TC341
TC342
TC460
TC362
G482
TC364
UNK382
FIGUREPROJECTTITLE
4A
TC-341
2022 ANNUAL MONITORING
REPORT
MARINE CORPS AIR STATION
NEW RIVER, NORTH CAROLINA
SITE MAP WITH
SHALLOW GROUNDWATER
ELEVATION CONTOURS
JULY 2022
Data Sources: GIS data layers provided by the MCB Camp Lejeune GIS Department, ESRI, and/or Cherokee Nation 3S.
Note: All wells were gauged on 7/5/2022.
100 0 10050 Feet
SCALE
PROJECT NO.:DATE:
221102 SEP 2022
LEGEND
Groundwater Flow Direction
Injection Well
Inspection Sump
Observation Well
Shallow Groundwater Monitoring Well
Recovery Well
Junction Vault
Shallow Groundwater Elevation Contour (ft. NGVD)
FreeProduct Recovery Line
Free-Product Recovery Trench
Former Fuel Lines
Recovery Sump
Treatment System
Former USTs
Existing Building
Demolished Building
' Cherokee Nation JS
D
D
D -D
USTTC341-RW07
USTTC341-RW06
USTTC341-RW05
USTTC341-RW03
USTTC341-RW02
USTTC341-RW04
USTTC341-RW01
IR35-MW31B
9.30
IR35-MW14D
6.36
IR35-MW09IW
10.95
USTG480-MW25
7.07
USTTC341-MW09
10.80
USTTC341-MW15R
10.49
9 810
G480
TC460
TC341
TC342
G482
TC362
TC364
UNK382F STE STUS 17THIRD ST
G ST
FOURTH ST NC

2
4 US

1
7
FIGUREPROJECTTITLE
4B
TC-341
2022 ANNUAL MONITORING
REPORT
MARINE CORPS AIR STATION
NEW RIVER, NORTH CAROLINA
SITE MAP WITH
INTERMEDIATE GROUNDWATER
ELEVATION CONTOURS
JULY 2022
Data Sources: GIS data layers provided by the MCB Camp Lejeune GIS Department, ESRI, and/or Cherokee Nation 3S.
Note: All wells were gauged on 7/5/2022.
90 0 9045 Feet
SCALE
PROJECT NO.:DATE:
221102 SEP 2022
LEGEND
Groundwater Flow Direction
Intermediate Groundwater Monitoring Well
Recovery Well
Junction Vault
Intermediate Groundwater Elevation Contour (ft. NGVD)
FreeProduct Recovery Line
Free-Product Recovery Trench
Former Fuel Lines
Recovery Sump
Treatment System
Former USTs
Existing Building
Demolished Building
' Cherokee Nation JS
-D
D
D -D
USTTC341-RW07
USTTC341-RW06
USTTC341-RW05
USTTC341-RW03
USTTC341-RW02
USTTC341-RW04
USTTC341-RW01
IR35-MW31B
IR35-MW09IW
USTTC341-MW09
USTTC341-MW15R
USTG480-MW25
IR35-MW14D
USTG480-MW15
IR35-MW31A
IR35-MW14S
IR35-MW09S
IR35-MW67AR
USTG480-MW18
USTG480-MW32
USTG480-MW31
USTG480-MW30
USTG480-MW29
USTG480-MW27
USTG480-MW26
USTG480-MW24
USTG480-MW23
USTG480-MW20
USTG480-MW19
USTG480-MW17
USTG480-MW16
USTG480-MW14
USTG480-MW13
USTG480-MW12
USTG480-MW11
USTG480-MW10
USTG480-MW07
USTG480-MW06
USTG480-MW03
USTG480-MW02
USTG480-MW01
USTTC341-IW06
USTTC341-IW03
USTTC341-IW05
USTTC341-IW04
USTCGFF-EMW05
USTTC341-IS03
USTTC341-IS02
USTTC341-IS01
USTTC341-MW12
USTTC341-MW01
USTTC341-MW02
USTTC341-MW03
USTTC341-MW05
USTGCFF-EMW01
USTTC341-MW17
USTTC341-MW13
USTTC341-MW11
USTTC341-MW10
USTTC341-MW08
USTTC341-MW06
USTG480-MW33R
USTG480-MW09R
USTG480-MW04R
USTTC341-MW14R
USTG480-MW28
USTG480-MW08
USTTC341-IW02
USTTC341-IW01
USTTC341-MW18
USTTC341-OW01
USTTC341-OW02
D STUS 17F STE STTHIRD ST NC 2
4
FOURTH ST
G ST
US

1
7
G480
TC341
TC342
TC460
TC362
G482
TC364
UNK382
FIGUREPROJECTTITLE
5
TC-341
2022 ANNUAL MONITORING
REPORT
MARINE CORPS AIR STATION
NEW RIVER, NORTH CAROLINA
SITE MAP WITH
FREE-PHASE PRODUCT
DETECTIONS
Data Sources: GIS data layers provided by the MCB Camp Lejeune GIS Department, ESRI, and/or Cherokee Nation 3S.
Note: Refer to Table 3 for more information on free-phase product detections.
Note: Free-phase product passive skimmers are installed in monitoring wells USTG480-MW-07, USTG480-MW-13,
and USTG480-MW-20.
100 0 10050 Feet
SCALE
PROJECT NO.:DATE:
221102 SEP 2022
LEGEND
Injection Well, Measurable Free-Phase Product
Shallow Groundwater Monitoring Well, Measurable Free-Phase Product
Injection Well, No Measurable Free-Phase ProductInspection Sump, No Measurable Free-Phase Product
Observation Well, No Measurable Free-Phase Product
Shallow Groundwater Monitoring Well, No Measurable Free-Phase ProductIntermediate Groundwater Monitoring Well, No Measurable Free-Phase Product
Deep Groundwater Monitoring Well, No Measurable Free-Phase Product
Recovery Well, No Measurable Free-Phase Product
Junction Vault
FreeProduct Recovery Line
Recovery SumpFree-Product Recovery Trench
Former Fuel Lines
Treatment System
Former USTsExisting Building
Demolished Building
USTTC341-RW07
USTTC341-RW06
USTTC341-RW05
USTTC341-RW03
USTTC341-RW02
USTTC341-RW04
USTTC341-RW01
IR35-MW31B
IR35-MW09IW
USTTC341-MW09
USTTC341-MW15R
USTG480-MW25
IR35-MW14D
USTG480-MW15
IR35-MW31A
IR35-MW14S
IR35-MW09S
IR35-MW67AR
USTG480-MW18
USTG480-MW32
USTG480-MW31
USTG480-MW30
USTG480-MW29
USTG480-MW27
USTG480-MW26
USTG480-MW24
USTG480-MW23
USTG480-MW20
USTG480-MW19
USTG480-MW17
USTG480-MW16
USTG480-MW14
USTG480-MW13
USTG480-MW12
USTG480-MW11
USTG480-MW10
USTG480-MW07
USTG480-MW06
USTG480-MW03
USTG480-MW02
USTG480-MW01
USTTC341-IW06
USTTC341-IW03
USTTC341-IW05
USTTC341-IW04
USTCGFF-EMW05
USTTC341-IS03
USTTC341-IS02
USTTC341-IS01
USTTC341-MW12
USTTC341-MW01
USTTC341-MW02
USTTC341-MW03
USTTC341-MW05
USTGCFF-EMW01
USTTC341-MW17
USTTC341-MW13
USTTC341-MW11
USTTC341-MW10
USTTC341-MW08
USTTC341-MW06
USTG480-MW33R
USTG480-MW09R
USTG480-MW04R
USTTC341-MW14R
USTG480-MW28
USTG480-MW08
USTTC341-IW02
USTTC341-IW01
USTTC341-MW18
USTTC341-OW01
USTTC341-OW02
D STUS 17F STE STTHIRD ST NC 2
4
FOURTH ST
G ST
US

1
7
G480
TC341
TC342
TC460
TC362
G482
TC364
UNK382
FIGUREPROJECTTITLE
6
TC-341
2022 ANNUAL MONITORING
REPORT
MARINE CORPS AIR STATION
NEW RIVER, NORTH CAROLINA
SITE MAP WITH
DISSOLVED-PHASE
PLUME AS OF JULY 2022
Data Sources: GIS data layers provided by the MCB Camp
Lejeune GIS Department, ESRI, and/or Cherokee Nation 3S.
100 0 10050 Feet
SCALE
PROJECT NO.:DATE:
221102 SEP 2022
LEGEND
Injection Well Not Sampled
Inspection Sump Not Sampled
Observation Well Not Sampled
Shallow Groundwater Monitoring Well Above NCAC 2L GWQS
Shallow Groundwater Monitoring Well Below NCAC 2L GWQ
Shallow Groundwater Monitoring Well Not Sampled
Intermediate Groundwater Monitoring Well Above NCAC 2L GWQS
Intermediate Groundwater Monitoring Well Below NCAC 2L GWQS
Intermediate Groundwater Monitoring Well Not Sampled
Deep Groundwater Monitoring Well Not Sampled
Recovery Well
Junction Vault
FreeProduct Recovery Line
Free-Product Recovery Trench
Former Fuel Lines
30-Foot VISL Boundary
Recovery Sump
Shallow Groundwater Contamination Plume Above NCAC 2L GWQS (July 2022)
Shallow Groundwater Contamination Plume Above NCAC 2L GWQS (July 2021)
Treatment System
Former USTs
Existing Building
Demolished Building
® s ·-++ CJ
0 s c:::::J -@ s c:::::J c:::::J EB ~ CJ EB 0 -EB ■ c:::::J
' Cherokee Nation JS
USTTC341-RW07
USTTC341-RW06
USTTC341-RW05
USTTC341-RW03
USTTC341-RW02
USTTC341-RW04
USTTC341-RW01
IR35-MW31B
IR35-MW09IW
USTTC341-MW09
USTTC341-MW15R
USTG480-MW25
IR35-MW14D
USTG480-MW15
IR35-MW31A
IR35-MW14S
IR35-MW09S
IR35-MW67AR
USTG480-MW18
USTG480-MW32
USTG480-MW31
USTG480-MW30
USTG480-MW29
USTG480-MW27
USTG480-MW26
USTG480-MW24
USTG480-MW23
USTG480-MW20
USTG480-MW19
USTG480-MW17
USTG480-MW16
USTG480-MW14
USTG480-MW13
USTG480-MW12
USTG480-MW11
USTG480-MW10
USTG480-MW07
USTG480-MW06
USTG480-MW03
USTG480-MW02
USTG480-MW01
USTTC341-IW06
USTTC341-IW03
USTTC341-IW05
USTTC341-IW04
USTCGFF-EMW05
USTTC341-IS03
USTTC341-IS02
USTTC341-IS01
USTTC341-MW12
USTTC341-MW01
USTTC341-MW02
USTTC341-MW03
USTTC341-MW05
USTGCFF-EMW01
USTTC341-MW17
USTTC341-MW13
USTTC341-MW11
USTTC341-MW10
USTTC341-MW08
USTTC341-MW06
USTG480-MW33R
USTG480-MW09R
USTG480-MW04R
USTTC341-MW14R
USTG480-MW28
USTG480-MW08
USTTC341-IW02
USTTC341-IW01
USTTC341-MW18
USTTC341-OW01
USTTC341-OW02
D STUS 17F STE STTHIRD ST NC 2
4
FOURTH ST
G ST
US

1
7
G480
TC341
TC342
TC460
TC362
G482
TC364
UNK382
FIGUREPROJECTTITLE
7
TC-341
2022 ANNUAL MONITORING
REPORT
MARINE CORPS AIR STATION
NEW RIVER, NORTH CAROLINA
SITE MAP WITH
PROPOSED SAMPLING
PLAN - JULY 2023
Data Sources: GIS data layers provided by the MCB Camp Lejeune GIS Department, ESRI, and/or Cherokee Nation 3S.
100 0 10050 Feet
SCALE
PROJECT NO.:DATE:
221102 SEP 2022
LEGEND
Injection Well
Inspection Sump
Observation Well
Shallow Groundwater Monitoring Well
Shallow Groundwater Monitoring Well to be Sampled
Intermediate Groundwater Monitoring Well
Intermediate Groundwater Monitoring Well to be Sampled
Deep Groundwater Monitoring Well
Recovery Well
Junction Vault
FreeProduct Recovery Line
Free-Product Recovery Trench
Former Fuel Lines
30-Foot VISL Boundary
Recovery Sump
Treatment System
FormerUSTs
Existing Building
Demolished Building
' Cherokee Nation JS
·-++-
CJ
CJ
CJ
c::::J -c::::J
2022 Annual Monitoring Report – TC-341
MCAS New River, NC

APPENDICES
(.'\ (HEROKEENATION™ ~ 3 S-Support, Service & Solutions
2022 Annual Monitoring Report – TC-341
MCAS New River, NC

APPENDIX A

Historical Gauging and Free-Phase Product Recovery Data
(.'\ (HEROKEENATION™ ~ 3 S-Support, Service & Solutions
DTP DTW Product
Thickness DTP DTW Product
Thickness
USTTC341-RW01 ND 13.85 NA ND 5.95 NA
USTTC341-RW02 ND 8.40 NA ND 5.60 NA
USTTC341-RW03 ND 9.90 NA ND 6.01 NA
USTTC341-RW04 ND 10.65 NA ND 5.94 NA
USTTC341-RW05 ND 6.20 NA 5.20 5.25 0.05
USTTC341-RW06 ND 11.70 NA 4.60 4.95 0.35
USTTC341-RW07 ND 12.40 NA ND <1.0 NA
USTTC341-IW01 ND 7.09 NA
USTTC341-IW02 ND 7.21 NA
USTTC341-IW03
USTTC341-IW04 sheen 7.50 sheen ND 6.58 NA
USTTC341-IW05 sheen 7.40 sheen ND 7.13 NA
USTTC341-IW06 ND 7.95 NA ND 7.31 NA
USTTC341-OW01 ND 3.60 NA ND 6.50 NA
USTTC341-OW02 ND 8.80 NA
USTTC341-MW01 ND 5.40 NA ND 5.46 NA
USTTC341-MW08
USTTC341-MW13 ND 7.61 NA ND 7.90 NA
USTTC341-MW14
USTTC341-MW15
USTG480-MW01 ND 6.91 NA ND 5.46 NA
USTG480-MW02 sheen 8.37 sheen ND 7.15 NA
USTG480-MW03
USTG480-MW04R ND 7.74 NA
USTG480-MW06 ND 8.10 NA
USTG480-MW07 ND 6.40 NA ND 4.43 NA
USTG480-MW08 8.40 9.45 1.05 6.64 6.69 0.05
USTG480-MW09R ND 7.05 NA ND 7.09 NA
USTG480-MW10 ND 7.20 NA ND 5.50 NA
USTG480-MW13 8.20 8.40 0.20 6.60 7.57 0.97
USTG480-MW20 6.90 6.96 0.06 ND 7.05 NA
USTG480-MW23 ND 6.35 NA ND 4.47 NA
USTG480-MW26 ND 4.75 NA ND 3.53 NA
USTG480-MW27 ND 8.63 NA ND 7.05 NA
USTG480-MW28 ND 7.10 NA ND 3.82 NA
USTG480-MW29 ND 5.06 NA ND 3.35 NA
USTG480-MW31
USTG480-MW32 ND 7.95 NA
USTG480-MW33R ND 6.02 NA
IR35-MW67AR ND 8.06 NA ND 7.39 NA
Recovery Sump NM NM NM ND 5.45 NA
IR35-MW14 NM NM NM ND 10.41 NA
IR35-MW14D NM NM NM ND 10.40 NA
5 3
5 5
DTP DTW Product Thickness DTP DTW Product Thickness
USTTC341-RW01 ND 13.09 NA ND 5.74 NA
USTTC341-RW02 ND 8.60 NA ND 5.40 NA
USTTC341-RW03 ND 6.00 NA ND 5.53 NA
USTTC341-RW04 ND 10.65 NA ND 5.90 NA
USTTC341-RW05 ND 9.15 NA ND 5.10 NA
USTTC341-RW06 ND 11.65 NA ND 5.69 NA
USTTC341-RW07 ND 11.35 NA ND 3.60 NA
USTTC341-IW01 9.65 9.66 0.01 ND 7.15 NA
USTTC341-IW02 ND 9.10 NA ND 7.13 NA
USTTC341-IW03
USTTC341-IW04 7.57 8.28 0.71 ND 6.55 NA
USTTC341-IW05 7.55 10.06 2.51 7.03 7.05 0.02
USTTC341-IW06 ND 7.95 NA ND 7.05 NA
USTTC341-OW01 8.15 8.17 0.02 ND 6.70 NA
USTTC341-OW02 8.89 8.94 0.05 ND 7.40 NA
USTTC341-MW01 ND 5.27 NA ND 4.83 NA
USTTC341-MW08
USTTC341-MW13 ND 7.77 NA ND 7.25 NA
USTTC341-MW14
USTTC341-MW15
USTG480-MW01 ND 7.76 NA ND 6.50 NA
USTG480-MW02 ND 8.56 NA ND 6.94 NA
USTG480-MW03 ND 7.61 NA
USTG480-MW04R ND 8.05 NA ND 7.62 NA
USTG480-MW06 ND 6.55 NA
USTG480-MW07 6.35 6.49 0.14 ND 4.04 NA
USTG480-MW08 ND 9.26 NA ND 6.51 NA
USTG480-MW09R ND 7.80 NA ND 7.39 NA
USTG480-MW10 ND 7.53 NA ND 6.65 NA
USTG480-MW13 8.70 9.55 0.85 ND 6.15 NA
USTG480-MW20 7.26 7.36 0.10 ND 6.75 NA
USTG480-MW23 ND 6.30 NA ND 5.75 NA
USTG480-MW26 ND 4.03 NA ND 3.20 NA
USTG480-MW27 ND 8.87 NA ND 6.80 NA
USTG480-MW28 7.20 8.35 1.15 ND 4.41 NA
USTG480-MW29 ND 5.02 NA ND 3.35 NA
USTG480-MW31
USTG480-MW32 8.25 8.71 0.46 ND 6.71 NA
USTG480-MW33R ND 5.90 NA
IR35-MW67AR ND 8.43 NA ND 7.19 NA
Recovery Sump ND 10.95 NA ND 5.70 NA
IR35-MW14 ND 10.79 NA ND 10.16 NA
IR35-MW14D ND 10.84 NA ND 10.17 NA
5 1
5 5
Well 10/22/2013 11/27/2013
GAUGING, BAILING, AND AFVR DATA
MCAS New River, North Carolina
Contract No. N40085-15-D-0007, CTO: 0004
TC-341
2018 Annual Monitoring Report
APPENDIX A
Inaccesible due to construction
Inaccesible due to construction
Inaccesible due to construction
Inaccesible due to construction
Inaccesible due to construction
Inaccesible due to construction
Inaccesible due to construction
Inaccesible due to construction
Well currently abandonded/destroyed.
Well currently abandonded/destroyed.
Well currently abandonded/destroyed.
Water Recovered (gal):Water Recovered (gal):
Product Recovered (gal): Product Recovered (gal):
Inaccessible, monitoring well underwater
Inaccesible due to construction
Inaccesible due to construction
Well currently abandonded/destroyed.
Well currently abandonded/destroyed.
Well currently abandonded/destroyed.
Inaccesible due to construction
Inaccesible due to construction
Inaccesible due to construction
Inaccesible due to construction
Inaccessible, monitoring well underwater
Well currently abandonded/destroyed.
Well currently abandonded/destroyed.
Well currently abandonded/destroyed.
Well currently abandonded/destroyed.
Inaccesible due to construction
Inaccesible due to construction
Inaccesible due to construction
Inaccesible due to construction
Well currently abandonded/destroyed.
Well currently abandonded/destroyed.
Water Recovered (gal):
Product Recovered (gal):
Water Recovered (gal):
Well 12/11/2013 1/8/2014
Product Recovered (gal):
Page 1 of 10
'
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CONSULTECH JV
T
I
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l I I
T
I
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GAUGING, BAILING, AND AFVR DATA
MCAS New River, North Carolina
Contract No. N40085-15-D-0007, CTO: 0004
TC-341
2018 Annual Monitoring Report
APPENDIX A
DTP DTW Product
Thickness DTP DTW Product
Thickness
USTTC341-RW01 ND 13.30 NA ND 6.95 NA
USTTC341-RW02 ND 8.70 NA ND 7.13 NA
USTTC341-RW03 NM NM NM ND 7.68 NA
USTTC341-RW04 ND 10.65 NA ND 7.72 NA
USTTC341-RW05 ND 9.20 NA ND 7.10 NA
USTTC341-RW06 ND 11.50 NA ND 6.52 NA
USTTC341-RW07 NM NM NM ND 5.05 NA
USTTC341-IW01 ND 8.78 NA ND 8.71 NA
USTTC341-IW02 ND 8.19 NA ND 8.56 NA
USTTC341-IW03 ND 7.81 NA ND 8.42 NA
USTTC341-IW04 ND 6.78 NA ND 7.57 NA
USTTC341-IW05 ND 6.80 NA 7.55 7.99 0.44
USTTC341-IW06 ND 6.94 NA ND 7.65 NA
USTTC341-OW01 ND 8.10 NA ND 8.12 NA
USTTC341-OW02 ND 7.85 NA ND 8.82 NA
USTTC341-MW01 ND 4.03 NA ND 4.77 NA
USTTC341-MW08
USTTC341-MW13 ND 6.45 NA ND 8.07 NA
USTTC341-MW14
USTTC341-MW15
USTG480-MW01 ND 5.25 NA ND 6.46 NA
USTG480-MW02 ND 7.47 NA ND 8.06 NA
USTG480-MW03 ND 8.50 NA NM NM NM
USTG480-MW04R ND 6.95 NA ND 7.62 NA
USTG480-MW06 ND 6.31 NA ND 7.79 NA
USTG480-MW07 ND 4.36 NA 5.87 7.65 1.78
USTG480-MW08 ND 8.45 NA ND 8.10 NA
USTG480-MW09R ND 6.56 NA ND 7.00 NA
USTG480-MW10 ND 7.35 NA ND 7.03 NA
USTG480-MW13 8.19 8.24 0.05 ND 7.15 NA
USTG480-MW20 ND 6.04 NA 6.65 6.95 0.30
USTG480-MW23 ND 4.90 NA ND 5.81 NA
USTG480-MW26 ND 3.05 NA ND 4.25 NA
USTG480-MW27 ND 7.09 NA ND 8.01 NA
USTG480-MW28 ND 6.16 NA 5.75 7.25 1.50
USTG480-MW29 ND 4.30 NA ND 4.52 NA
USTG480-MW31
USTG480-MW32 ND 7.26 NA ND 7.74 NA
USTG480-MW33R ND 5.34 NA ND 6.10 NA
IR35-MW67AR ND 7.17 NA ND 8.18 NA
Recovery Sump ND 6.83 NA ND 8.30 NA
IR35-MW14 ND 10.01 NA ND 10.51 NA
IR35-MW14D ND 9.90 NA ND 10.51 NA
1 5
1 5
DTP DTW Product
Thickness DTP DTW Product
Thickness
USTTC341-RW01 ND 5.15 NA ND 5.60 NA
USTTC341-RW02 ND 4.83 NA ND 5.25 NA
USTTC341-RW03 4.62 5.30 0.68 ND 5.70 NA
USTTC341-RW04 4.21 4.65 0.44 ND 5.80 NA
USTTC341-RW05 4.21 4.32 0.11 ND 5.21 NA
USTTC341-RW06 ND 4.41 NA 4.63 5.03 0.40
USTTC341-RW07 ND 3.11 NA 3.52 3.93 0.41
USTTC341-IW01 ND 7.37 NA ND 7.12 NA
USTTC341-IW02 ND 6.69 NA ND 7.10 NA
USTTC341-IW03 ND 7.07 NA ND 7.51 NA
USTTC341-IW04 ND 6.21 NA ND 6.70 NA
USTTC341-IW05 ND 6.99 NA ND 7.10 NA
USTTC341-IW06 ND 6.66 NA ND 7.22 NA
USTTC341-OW01 ND 6.26 NA ND 6.15 NA
USTTC341-OW02 ND 6.81 NA ND 6.80 NA
USTTC341-MW01 ND 4.32 NA ND 5.20 NA
USTTC341-MW08
USTTC341-MW13 ND 6.63 NA ND 7.35 NA
USTTC341-MW14
USTTC341-MW15
USTG480-MW01 ND 5.61 NA ND 6.40 NA
USTG480-MW02 ND 6.71 NA ND 6.90 NA
USTG480-MW03 ND 6.25 NA 7.65 7.85 0.20
USTG480-MW04R ND 7.05 NA ND 7.30 NA
USTG480-MW06 ND 6.30 NA ND 6.70 NA
USTG480-MW07 ND 4.30 NA ND 4.70 NA
USTG480-MW08 ND 5.35 NA 6.45 6.67 0.22
USTG480-MW09R ND 6.73 NA ND 7.00 NA
USTG480-MW10 ND 6.01 NA ND 4.50 NA
USTG480-MW13 ND 6.71 NA 6.45 6.82 0.37
USTG480-MW20 6.18 7.18 1.00 ND 6.70 NA
USTG480-MW23 ND 5.21 NA ND 5.90 NA
USTG480-MW26 NM NM NM ND 3.59 NA
USTG480-MW27 ND 6.79 NA ND 6.60 NA
USTG480-MW28 ND 3.83 NA 3.74 3.95 0.21
USTG480-MW29 2.80 2.86 0.06 ND 3.54 NA
USTG480-MW31 ND 6.79 NA ND 6.90 NA
USTG480-MW32 ND 6.56 NA ND 6.71 NA
USTG480-MW33R ND 4.85 NA ND 6.80 NA
IR35-MW67AR ND 6.09 NA ND 7.30 NA
Recovery Sump 5.16 5.20 0.04 NM NM NM
IR35-MW14 NM NM NM ND 10.40 NA
IR35-MW14D NM NM NM ND 10.40 NA
5 7
5 200
AFVRs began May 30, 2014
Well currently abandonded/destroyed.Well currently abandonded/destroyed.
Water Recovered (gal):Water Recovered (gal):
Well 4/30/2014 5/30/2014
Product Recovered (gal): Product Recovered (gal):
Product Recovered (gal): Product Recovered (gal):
Water Recovered (gal):Water Recovered (gal):
Well currently abandonded/destroyed.
Well currently abandonded/destroyed.
Well currently abandonded/destroyed.
Well currently abandonded/destroyed.
Well currently abandonded/destroyed.
Well currently abandonded/destroyed.
Inaccesible due to construction
Well currently abandonded/destroyed.
Well currently abandonded/destroyed.
Inaccesible due to construction
Well 2/18/2014 3/5/2014
Well currently abandonded/destroyed.Well currently abandonded/destroyed.
Page 2 of 10
RHE~
• CONSULTECH JV
I I I I
GAUGING, BAILING, AND AFVR DATA
MCAS New River, North Carolina
Contract No. N40085-15-D-0007, CTO: 0004
TC-341
2018 Annual Monitoring Report
APPENDIX A
DTP DTW Product
Thickness DTP DTW Product
Thickness
USTTC341-RW01 ND 5.62 NA ND 5.70 NA
USTTC341-RW02 ND 5.30 NA ND 5.40 NA
USTTC341-RW03 ND 5.62 NA ND 5.79 NA
USTTC341-RW04 ND 5.82 NA ND 5.91 NA
USTTC341-RW05 5.10 5.30 0.20 ND 5.72 NA
USTTC341-RW06 4.60 4.85 0.25 4.80 5.20 0.40
USTTC341-RW07 3.60 3.80 0.20 3.70 4.15 0.45
USTTC341-IW01 ND 7.13 NA ND 7.27 NA
USTTC341-IW02 ND 7.12 NA ND 7.25 NA
USTTC341-IW03 ND 7.54 NA ND 5.68 NA
USTTC341-IW04 ND 6.72 NA ND 6.82 NA
USTTC341-IW05 ND 7.15 NA ND 7.27 NA
USTTC341-IW06 ND 7.27 NA ND 7.38 NA
USTTC341-OW01 ND 6.20 NA 6.32 6.39 0.07
USTTC341-OW02 ND 7.11 NA ND 6.99 NA
USTTC341-MW01 ND 5.32 NA ND 5.40 NA
USTTC341-MW08
USTTC341-MW13 ND 7.49 NA ND 7.64 NA
USTTC341-MW14
USTTC341-MW15
USTG480-MW01 ND 6.45 NA ND 6.54 NA
USTG480-MW02 ND 6.96 NA ND 7.06 NA
USTG480-MW03 6.62 6.95 0.33 6.71 7.40 0.69
USTG480-MW04R ND 7.30 NA ND 7.45 NA
USTG480-MW06 ND 6.77 NA ND 6.86 NA
USTG480-MW07 4.65 5.65 1.00 4.70 5.80 1.10
USTG480-MW08 6.45 7.00 0.55 6.52 7.65 1.13
USTG480-MW09R ND 7.70 NA ND 7.22 NA
USTG480-MW10 ND 6.55 NA ND 6.71 NA
USTG480-MW13 6.50 7.00 0.50 6.60 7.09 0.49
USTG480-MW20 6.79 7.42 0.63 6.89 7.55 0.66
USTG480-MW23 ND 6.01 NA ND 6.09 NA
USTG480-MW26 ND 3.67 NA ND 3.78 NA
USTG480-MW27 ND 6.64 NA ND 6.78 NA
USTG480-MW28 4.01 5.80 1.79 4.15 5.77 1.62
USTG480-MW29 ND 3.30 NA ND 3.40 NA
USTG480-MW31 ND 6.96 NA ND 7.06 NA
USTG480-MW32 6.75 6.95 0.20 6.82 7.12 0.30
USTG480-MW33R ND 6.82 NA ND 6.78 NA
IR35-MW67AR ND 7.26 NA ND 7.39 NA
Recovery Sump NM NM NM NM NM NM
IR35-MW14 ND 10.40 NA ND 10.51 NA
IR35-MW14D ND 10.40 NA ND 10.49 NA
10 15
300 400
DTP DTW Product
Thickness DTP DTW Product
Thickness
USTTC341-RW01 5.78 5.90 0.12 ND 5.85 NA
USTTC341-RW02 ND 5.46 NA ND 5.55 NA
USTTC341-RW03 ND 5.89 NA ND 5.95 NA
USTTC341-RW04 ND 5.98 NA ND 6.05 NA
USTTC341-RW05 5.28 5.57 0.29 5.35 5.70 0.35
USTTC341-RW06 4.88 5.10 0.22 4.90 5.05 0.15
USTTC341-RW07 3.80 4.18 0.38 3.80 4.20 0.40
USTTC341-IW01 ND 7.37 NA ND 7.35 NA
USTTC341-IW02 ND 7.31 NA ND 7.35 NA
USTTC341-IW03 ND 7.73 NA ND 7.75 NA
USTTC341-IW04 ND 6.89 NA ND 6.93 NA
USTTC341-IW05 ND 7.32 NA ND 7.37 NA
USTTC341-IW06 7.42 7.50 0.08 ND 7.45 NA
USTTC341-OW01 NM NM NM ND 6.45 NA
USTTC341-OW02 7.05 7.15 0.10 ND 7.10 NA
USTTC341-MW01 ND 6.57 NA ND 5.45 NA
USTTC341-MW08
USTTC341-MW13 ND 7.71 NA ND 7.75 NA
USTTC341-MW14
USTTC341-MW15
USTG480-MW01 ND 6.51 NA ND 6.64 NA
USTG480-MW02 ND 7.17 NA ND 7.20 NA
USTG480-MW03 6.80 7.35 0.55 ND 6.02 NA
USTG480-MW04R 7.49 7.51 0.02 ND 7.55 NA
USTG480-MW06 ND 6.92 NA ND 6.95 NA
USTG480-MW07 ND 5.85 NA ND 4.80 NA
USTG480-MW08 ND 7.48 NA 6.60 7.90 1.30
USTG480-MW09R ND 7.27 NA ND 7.30 NA
USTG480-MW10 ND 6.77 NA ND 6.68 NA
USTG480-MW13 ND 7.98 NA 6.75 7.20 0.45
USTG480-MW20 ND 7.38 NA ND 7.00 NA
USTG480-MW23 ND 6.18 NA ND 6.15 NA
USTG480-MW26 ND 3.81 NA ND 3.75 NA
USTG480-MW27 ND 6.86 NA ND 6.90 NA
USTG480-MW28 ND 5.88 NA 3.40 4.05 0.65
USTG480-MW29 ND 3.46 NA ND 3.45 NA
USTG480-MW31 ND 7.16 NA ND 7.17 NA
USTG480-MW32 ND 7.20 NA ND 6.95 NA
USTG480-MW33R ND 6.82 NA ND 6.75 NA
IR35-MW67AR ND 7.50 NA ND 7.50 NA
Recovery Sump NM NM NA ND 5.35 NA
IR35-MW14 ND 10.56 NA ND 10.59 NA
IR35-MW14D ND 10.56 NA ND 10.58 NA
20 8
500 200
Well currently abandonded/destroyed.
Well currently abandonded/destroyed.
Well currently abandonded/destroyed.
Well currently abandonded/destroyed.
Well currently abandonded/destroyed.
Well currently abandonded/destroyed.
Product Recovered (gal): Product Recovered (gal):
Water Recovered (gal):Water Recovered (gal):
Well 6/19/2014 6/24/2014
Well currently abandonded/destroyed.
Well currently abandonded/destroyed.
Well currently abandonded/destroyed.
Well 6/2/2014 6/13/2014
Product Recovered (gal): Product Recovered (gal):
Water Recovered (gal):Water Recovered (gal):
Well currently abandonded/destroyed.
Well currently abandonded/destroyed.
Well currently abandonded/destroyed.
Page 3 of 10
RHE~
• CONSULTECH JV
I
I
I ' T
I I I
GAUGING, BAILING, AND AFVR DATA
MCAS New River, North Carolina
Contract No. N40085-15-D-0007, CTO: 0004
TC-341
2018 Annual Monitoring Report
APPENDIX A
DTP DTW Product
Thickness DTP DTW Product
Thickness
USTTC341-RW01 ND 5.92 NA ND 5.85 NA
USTTC341-RW02 ND 5.63 NA ND 5.50 NA
USTTC341-RW03 ND 6.01 NA ND 5.88 NA
USTTC341-RW04 ND 6.07 NA ND 6.00 NA
USTTC341-RW05 5.40 5.70 0.30 5.20 5.52 0.32
USTTC341-RW06 4.90 5.03 0.13 4.81 5.01 0.20
USTTC341-RW07 ND 5.08 NA 3.76 3.90 0.14
USTTC341-IW01 ND 7.52 NA ND 7.35 NA
USTTC341-IW02 ND 7.60 NA ND 7.30 NA
USTTC341-IW03 ND 7.81 NA ND 7.73 NA
USTTC341-IW04 ND 6.95 NA ND 6.63 NA
USTTC341-IW05 ND 7.43 NA ND 7.30 NA
USTTC341-IW06 ND 7.48 NA ND 7.39 NA
USTTC341-OW01 ND 6.53 NA 6.42 6.43 0.01
USTTC341-OW02 ND 7.10 NA ND 7.09 NA
USTTC341-MW01 ND 5.49 NA ND 5.41 NA
USTTC341-MW08R ND 5.90 NA ND 5.81 NA
USTTC341-MW13 ND 7.80 NA ND 7.75 NA
USTTC341-MW14R ND 5.96 NA ND 5.86 NA
USTTC341-MW15R ND 5.78 NA ND 6.10 NA
USTG480-MW01 ND 6.79 NA ND 6.51 NA
USTG480-MW02 ND 7.24 NA ND 7.16 NA
USTG480-MW03 ND 6.09 NA 6.65 7.30 0.65
USTG480-MW04R ND 7.58 NA ND 7.50 NA
USTG480-MW06 ND 7.00 NA ND 6.90 NA
USTG480-MW07 ND 4.89 NA 4.75 4.89 0.14
USTG480-MW08 6.78 7.00 0.22 6.55 7.55 1.00
USTG480-MW09R ND 7.34 NA ND 7.30 NA
USTG480-MW10 ND 6.75 NA ND 6.80 NA
USTG480-MW13 6.75 7.02 0.27 6.70 6.97 0.27
USTG480-MW20 ND 7.10 NA ND 6.65 NA
USTG480-MW23 ND 6.23 NA ND 6.10 NA
USTG480-MW26 ND 3.81 NA ND 3.41 NA
USTG480-MW27 ND 6.96 NA ND 6.82 NA
USTG480-MW28 ND 4.11 NA 3.81 5.96 2.15
USTG480-MW29 ND 3.40 NA ND 3.41 NA
USTG480-MW31 ND 7.21 NA ND 7.15 NA
USTG480-MW32 ND 7.03 NA 6.86 7.41 0.55
USTG480-MW33R ND 6.84 NA ND 6.62 NA
IR35-MW67AR ND 7.60 NA 7.42 7.48 0.06
Recovery Sump ND 5.40 NA 5.31 6.01 0.70
IR35-MW14 ND 10.40 NA ND 10.52 NA
IR35-MW14D ND 10.41 NA ND 10.52 NA
15 25
250 400
DTP DTW Product Thickness DTP DTW Product Thickness
USTTC341-RW01 ND 10.98 NA ND 5.38 NA
USTTC341-RW02 ND 9.37 NA ND 4.91 NA
USTTC341-RW03 ND 10.72 NA ND 5.42 NA
USTTC341-RW04 ND 10.57 NA ND 5.48 NA
USTTC341-RW05 ND 9.14 NA 4.62 4.82 0.20
USTTC341-RW06 ND 11.52 NA 4.23 4.64 0.41
USTTC341-RW07 ND 11.40 NA ND 2.58 NA
USTTC341-IW01 ND 7.12 NA ND 6.81 NA
USTTC341-IW02 ND 7.12 NA ND 6.82 NA
USTTC341-IW03 ND 7.53 NA ND 7.22 NA
USTTC341-IW04 ND 6.98 NA ND 5.06 NA
USTTC341-IW05 ND 7.15 NA ND 6.82 NA
USTTC341-IW06 ND 7.07 NA ND 6.68 NA
USTTC341-OW01 NM NM NM NM NM NM
USTTC341-OW02 ND 6.99 NA ND 6.82 NA
USTTC341-MW01 ND 5.06 NA ND 4.22 NA
USTTC341-MW08 ND 5.42 NA ND 4.91 NA
USTTC341-MW13 ND 7.53 NA ND 7.12 NA
USTTC341-MW14 ND 5.45 NA ND 4.31 NA
USTTC341-MW15 ND 5.59 NA ND 4.37 NA
USTG480-MW01 ND 6.37 NA ND 5.94 NA
USTG480-MW02 ND 6.96 NA ND 6.67 NA
USTG480-MW03 6.62 6.93 0.31 NM NM NM
USTG480-MW04R ND 7.38 NA ND 6.89 NA
USTG480-MW06 ND 6.71 NA ND 6.42 NA
USTG480-MW07 4.48 5.22 0.74 4.36 4.52 0.16
USTG480-MW08 6.37 7.03 0.66 6.08 6.39 0.31
USTG480-MW09R ND 7.20 NA ND 7.06 NA
USTG480-MW10 ND 6.61 NA ND 4.96 NA
USTG480-MW13 6.42 6.67 0.25 6.18 6.33 0.15
USTG480-MW20 6.75 7.23 0.48 6.45 6.65 0.20
USTG480-MW23 ND 5.94 NA ND 5.46 NA
USTG480-MW26 ND 3.12 NA ND 2.96 NA
USTG480-MW27 ND 6.64 NA ND 6.37 NA
USTG480-MW28 3.44 5.44 2.00 3.78 5.43 1.65
USTG480-MW29 ND 3.17 NA ND 2.87 NA
USTG480-MW31 ND 6.96 NA ND 6.67 NA
USTG480-MW32 6.83 6.96 0.13 ND 6.42 NA
USTG480-MW33R ND 6.38 NA ND 5.48 NA
IR35-MW67AR ND 7.26 NA ND 6.97 NA
Recovery Sump NM NM NM NM NM NM
IR35-MW14 ND 10.32 NA ND 9.94 NA
IR35-MW14D ND 10.31 NA ND 9.94 NA
10 10
200 200
Product Recovered (gal): Product Recovered (gal):
Water Recovered (gal):
Product Recovered (gal): Product Recovered (gal):
Water Recovered (gal):Water Recovered (gal):
Water Recovered (gal):
Well 7/16/2014 7/22/2014
Well 7/3/2014 7/9/2014
Page 4 of 10
RHE~
• CONSULTECH JV
GAUGING, BAILING, AND AFVR DATA
MCAS New River, North Carolina
Contract No. N40085-15-D-0007, CTO: 0004
TC-341
2018 Annual Monitoring Report
APPENDIX A
DTP DTW Product
Thickness DTP DTW Product
Thickness
USTTC341-RW01 ND 5.18 NA ND 4.68 NA
USTTC341-RW02 ND 4.82 NA ND 4.42 NA
USTTC341-RW03 ND 5.27 NA ND 4.82 NA
USTTC341-RW04 ND 5.33 NA ND 4.90 NA
USTTC341-RW05 4.48 4.57 0.09 ND 3.42 NA
USTTC341-RW06 4.15 4.62 0.47 3.68 3.92 0.24
USTTC341-RW07 ND 3.15 NA
USTTC341-IW01 ND 6.66 NA ND 6.24 NA
USTTC341-IW02 ND 6.62 NA ND 6.22 NA
USTTC341-IW03 ND 7.04 NA ND 6.62 NA
USTTC341-IW04 ND 6.19 NA ND 5.74 NA
USTTC341-IW05 ND 6.67 NA ND 6.18 NA
USTTC341-IW06 ND 6.65 NA ND 6.12 NA
USTTC341-OW01 NM NM NM ND 5.66 NA
USTTC341-OW02 ND 6.42 NA ND 6.28 NA
USTTC341-MW01 ND 4.28 NA ND 3.02 NA
USTTC341-MW08 ND 4.47 NA ND 3.32 NA
USTTC341-MW13 ND 6.81 NA ND 5.96 NA
USTTC341-MW14 ND 5.02 NA ND 4.46 NA
USTTC341-MW15 ND 5.16 NA ND 4.42 NA
USTG480-MW01 ND 5.57 NA ND 4.73 NA
USTG480-MW02 ND 6.46 NA ND 6.02 NA
USTG480-MW03 ND 6.21 NA
USTG480-MW04R ND 6.94 NA ND 6.73 NA
USTG480-MW06 ND 6.24 NA
USTG480-MW07 4.23 4.33 0.10 ND 3.71 NA
USTG480-MW08 6.04 6.26 0.22 5.52 5.62 0.10
USTG480-MW09R ND 6.09 NA ND 4.59 NA
USTG480-MW10 ND 4.61 NA ND 5.44 NA
USTG480-MW13 5.97 6.12 0.15 5.42 5.67 0.25
USTG480-MW20 6.25 6.59 0.34 5.82 5.85 0.03
USTG480-MW23 ND 5.35 NA ND 4.53 NA
USTG480-MW26 ND 2.96 NA ND 2.27 NA
USTG480-MW27 ND 5.94 NA ND 5.27 NA
USTG480-MW28 3.35 6.02 2.67 2.99 4.51 1.52
USTG480-MW29 ND 2.82 NA ND 2.37 NA
USTG480-MW31 ND 6.42 NA ND 6.00 NA
USTG480-MW32 ND 6.27 NA ND 5.81 NA
USTG480-MW33R ND 5.45 NA
IR35-MW67AR ND 6.77 NA ND 6.37 NA
Recovery Sump NM NM NM NM NM NM
IR35-MW14 ND 10.78 NA ND 9.26 NA
IR35-MW14D ND 10.77 NA ND 9.29 NA
10 7
200 0
Ceased AFVRs and began gauging/bailing
DTP DTW Product
Thickness DTP DTW Product
Thickness
USTTC341-RW01 ND 4.68 NA ND 5.02 NA
USTTC341-RW02 ND 4.32 NA ND 4.66 NA
USTTC341-RW03 ND 4.46 NA ND 5.03 NA
USTTC341-RW04 ND 4.81 NA ND 5.12 NA
USTTC341-RW05 ND 4.36 NA ND 4.42 NA
USTTC341-RW06 3.38 3.68 0.30 4.06 4.30 0.24
USTTC341-RW07 ND 3.35 NA ND 2.92 NA
USTTC341-IW01 ND 6.22 NA ND 6.41 NA
USTTC341-IW02 ND 6.19 NA ND 6.38 NA
USTTC341-IW03 ND 6.64 NA ND 6.82 NA
USTTC341-IW04 ND 5.78 NA ND 5.93 NA
USTTC341-IW05 ND 6.22 NA ND 6.39 NA
USTTC341-IW06 ND 6.26 NA ND 6.47 NA
USTTC341-OW01 ND 5.37 NA ND 5.36 NA
USTTC341-OW02 ND 6.00 NA ND 5.97 NA
USTTC341-MW01 ND 4.71 NA ND 4.09 NA
USTTC341-MW08 ND 4.06 NA ND 4.12 NA
USTTC341-MW13 ND 6.26 NA ND 6.52 NA
USTTC341-MW14 ND 4.51 NA ND 4.68 NA
USTTC341-MW15 ND 4.71 NA ND 4.96 NA
USTG480-MW01 ND 4.77 NA ND 6.23 NA
USTG480-MW02 ND 6.01 NA ND 6.17 NA
USTG480-MW03 ND 5.76 NA ND 5.81 NA
USTG480-MW04R ND 6.54 NA ND 6.58 NA
USTG480-MW06 ND 5.83 NA ND 5.99 NA
USTG480-MW07 3.30 3.84 0.54 3.82 4.94 1.12
USTG480-MW08 5.61 5.65 0.04 5.74 6.06 0.32
USTG480-MW09R ND 6.04 NA ND 6.37 NA
USTG480-MW10 ND 5.56 NA ND 5.64 NA
USTG480-MW13 6.60 6.75 0.15 5.77 5.98 0.21
USTG480-MW20 5.84 5.94 0.10 6.02 6.18 0.16
USTG480-MW23 ND 4.78 NA ND 5.11 NA
USTG480-MW26 ND 2.38 NA ND 2.89 NA
USTG480-MW27 ND 5.68 NA ND 5.86 NA
USTG480-MW28 2.98 5.76 2.78 3.62 4.89 1.27
USTG480-MW29 ND 2.43 NA ND 2.68 NA
USTG480-MW31 ND 6.02 NA ND 6.06 NA
USTG480-MW32 ND 5.81 NA 5.96 6.06 0.10
USTG480-MW33R ND 5.16 NA ND 4.93 NA
IR35-MW67AR ND 6.36 NA ND 6.48 NA
IR35-MW14 ND 9.42 NA ND 9.87 NA
IR35-MW14D ND 9.42 NA ND 10.67 NA
8 5
Water Recovered (gal):
Well 7/31/2014 8/4/2014
Product Recovered (gal): Product Recovered (gal):
vault flooded/submerged
Product Recovered (gal): Product Recovered (gal):
Well 8/12/2014 8/19/2014
Water Recovered (gal):
vault flooded/submerged
vault flooded/submerged
vault flooded/submerged
Page 5 of 10
RHE~
• CONSULTECH JV
I I
GAUGING, BAILING, AND AFVR DATA
MCAS New River, North Carolina
Contract No. N40085-15-D-0007, CTO: 0004
TC-341
2018 Annual Monitoring Report
APPENDIX A
DTP DTW Product
Thickness DTP DTW Product
Thickness
USTTC341-RW01 ND 6.21 NA NM NM NM
USTTC341-RW02 ND 6.09 NA NM NM NM
USTTC341-RW03 ND 7.01 NA NM NM NM
USTTC341-RW04 ND 6.84 NA NM NM NM
USTTC341-RW05 ND 6.10 NA 4.80 4.87 0.07
USTTC341-RW06 ND 6.02 NA 4.41 4.56 0.15
USTTC341-RW07 ND 4.98 NA ND 3.39 NA
USTTC341-IW01 ND 7.77 NA NM NM NM
USTTC341-IW02 ND 7.56 NA NM NM NM
USTTC341-IW03 ND 7.10 NA NM NM NM
USTTC341-IW04 ND 6.51 NA NM NM NM
USTTC341-IW05 ND 6.62 NA ND 6.86 NA
USTTC341-IW06 ND 6.34 NA NM NM NM
USTTC341-OW01 ND 7.67 NA NM NM NM
USTTC341-OW02 ND 8.01 NA NM NM NM
USTTC341-MW01 ND 4.84 NA NM NM NM
USTTC341-MW08 ND 7.62 NA NM NM NM
USTTC341-MW13 ND 7.07 NA NM NM NM
USTTC341-MW14 ND 5.03 NA NM NM NM
USTTC341-MW15 ND 5.25 NA NM NM NM
USTG480-MW01 ND 5.99 NA NM NM NM
USTG480-MW02 ND 7.12 NA NM NM NM
USTG480-MW03 6.15 6.22 0.07 NM NM NM
USTG480-MW04R ND 6.65 NA NM NM NM
USTG480-MW06 ND 6.25 NA ND 6.50 NA
USTG480-MW07 4.10 4.95 0.85 4.26 4.98 0.72
USTG480-MW09R ND 6.01 NA NM NM NM
USTG480-MW10 ND 6.23 NA NM NM NM
USTG480-MW13 ND 6.15 NA NM NM NM
USTG480-MW20 6.08 6.48 0.40 6.93 6.98 0.05
USTG480-MW23 ND 5.90 NA NM NM NM
USTG480-MW26 ND 5.06 NA NM NM NM
USTG480-MW27 ND 6.86 NA NM NM NM
USTG480-MW28 5.91 6.85 0.94 3.75 5.84 2.09
USTG480-MW29 ND 5.51 NA NM NM NM
USTG480-MW31 ND 6.42 NA NM NM NM
USTG480-MW32 ND 6.74 NA NM NM NM
USTG480-MW33R ND 5.30 NA NM NM NM
IR35-MW67AR ND 6.74 NA ND 6.96 NA
Recovery Sump ND 8.02 NA NM NM NM
IR35-MW14 ND 7.04 NA NM NM NM
IR35-MW14D ND 9.91 NA NM NM NM
5 8
DTP DTW Product
Thickness DTP DTW Product
Thickness
USTTC341-RW01 ND 5.01 NA 4.95 4.96 0.01
USTTC341-RW02 ND 4.69 NA ND 4.60 NA
USTTC341-RW03 5.01 5.06 0.05 ND 5.05 NA
USTTC341-RW04 ND 5.28 NA ND 5.10 NA
USTTC341-RW05 4.48 4.61 0.13 4.35 4.45 0.10
USTTC341-RW06 3.97 4.00 0.03 3.95 4.16 0.21
USTTC341-RW07 ND 2.40 NA ND 0.00 NA
USTTC341-IW01 ND 6.37 NA ND 6.48 NA
USTTC341-IW02 ND 6.36 NA ND 6.47 NA
USTTC341-IW03 ND 6.78 NA ND 6.9 NA
USTTC341-IW04 ND 5.91 NA ND 6.05 NA
USTTC341-IW05 ND 6.39 NA ND 6.49 NA
USTTC341-IW06 ND 6.40 NA ND 6.58 NA
USTTC341-OW01 ND 5.61 NA 5.56 5.60 0.04
USTTC341-OW02 ND 6.22 NA ND 6.12 NA
USTTC341-MW01 ND 3.90 NA ND 4.01 NA
USTTC341-MW08 ND 4.77 NA ND 4.91 NA
USTTC341-MW13 ND 6.51 NA ND 6.54 NA
USTTC341-MW14 ND 4.70 NA ND 4.85 NA
USTTC341-MW15 ND 4.95 NA ND 5.12 NA
USTG480-MW01 ND 5.06 NA ND 5.09 NA
USTG480-MW02 ND 6.15 NA ND 6.26 NA
USTG480-MW03 ND 5.90 NA ND 5.97 NA
USTG480-MW04R ND 6.69 NA ND 6.74 NA
USTG480-MW06 ND 5.98 NA ND 5.71 NA
USTG480-MW07 3.91 4.46 0.55 3.92 4.65 0.73
USTG480-MW08 6.07 6.99 0.92 6.24 7.02 0.78
USTG480-MW09R ND 6.50 NA ND 6.61 NA
USTG480-MW10 ND 5.35 NA ND 5.40 NA
USTG480-MW13 5.87 6.00 0.13 5.8 6.01 0.21
USTG480-MW20 6.00 6.25 0.25 6.04 6.24 0.20
USTG480-MW23 ND 5.88 NA ND 5.91 NA
USTG480-MW26 ND 2.49 NA ND 2.38 NA
USTG480-MW27 ND 5.83 NA ND 6.00 NA
USTG480-MW28 3.50 5.06 1.56 3.49 5.00 1.51
USTG480-MW29 ND 2.77 NA ND 2.60 NA
USTG480-MW31 ND 6.15 NA ND 6.26 NA
USTG480-MW32 5.91 5.93 0.02 6.04 6.08 0.04
USTG480-MW33R ND 5.17 NA ND 5.25 NA
IR35-MW67AR ND 6.50 NA ND 6.60 NA
Recovery Sump 4.70 4.93 0.23 4.68 4.97 0.29
IR35-MW14 ND 9.55 NA ND 9.58 NA
IR35-MW14D ND 9.57 NA ND 9.62 NA
5 10
Well 8/27/2014 9/5/2014
Product Recovered (gal): Product Recovered (gal):
Well 9/17/2014 9/24/2014
Product Recovered (gal): Product Recovered (gal):
Page 6 of 10
RHE~
• CONSULTECH JV
GAUGING, BAILING, AND AFVR DATA
MCAS New River, North Carolina
Contract No. N40085-15-D-0007, CTO: 0004
TC-341
2018 Annual Monitoring Report
APPENDIX A
DTP DTW Product
Thickness DTP DTW Product
Thickness
USTTC341-RW01 ND 5.21 NA ND 5.20 NA
USTTC341-RW02 ND 4.77 NA ND 4.90 NA
USTTC341-RW03 4.87 5.00 0.13 5.29 5.59 0.30
USTTC341-RW04 ND 5.20 NA ND 5.40 NA
USTTC341-RW05 ND 4.55 NA 4.63 4.94 0.31
USTTC341-RW06 3.86 4.01 0.15 4.3 4.45 0.15
USTTC341-RW07 ND 1.87 NA 3.25 3.29 0.04
USTTC341-IW01 ND 6.36 NA ND 6.74 NA
USTTC341-IW02 ND 6.38 NA ND 6.76 NA
USTTC341-IW03 ND 6.58 NA ND 6.88 NA
USTTC341-IW04 ND 6.02 NA ND 6.01 NA
USTTC341-IW05 ND 6.41 NA ND 6.87 NA
USTTC341-IW06 ND 6.33 NA ND 6.99 NA
USTTC341-OW01 ND 5.60 NA ND 5.90 NA
USTTC341-OW02 ND 6.21 NA ND 6.56 NA
USTTC341-MW01 ND 4.00 NA ND 8.33 NA
USTTC341-MW08 ND 4.36 NA ND 5.02 NA
USTTC341-MW13 ND 6.50 NA ND 6.72 NA
USTTC341-MW14 ND 4.68 NA ND 4.99 NA
USTTC341-MW15 ND 4.89 NA ND 5.19 NA
USTG480-MW01 ND 5.02 NA ND 5.91 NA
USTG480-MW02 ND 6.60 NA ND 6.02 NA
USTG480-MW03 ND 5.97 NA 6.25 6.81 0.56
USTG480-MW04R ND 6.42 NA ND 7.02 NA
USTG480-MW06 ND 6.01 NA ND 6.40 NA
USTG480-MW07 6.84 7.77 0.93 4.15 5.67 1.52
USTG480-MW08 6.00 6.97 0.97 6.01 7.21 1.20
USTG480-MW09R ND 6.42 NA ND 6.88 NA
USTG480-MW10 ND 5.35 NA ND 5.60 NA
USTG480-MW13 ND 6.14 NA 6.19 6.32 0.13
USTG480-MW20 5.95 6.34 0.39 6.38 6.98 0.60
USTG480-MW23 ND 4.90 NA ND 5.46 NA
USTG480-MW26 ND 2.82 NA ND 3.15 NA
USTG480-MW27 ND 6.00 NA ND 6.24 NA
USTG480-MW28 3.38 5.00 1.62 3.65 5.64 1.99
USTG480-MW29 ND 3.01 NA ND 2.91 NA
USTG480-MW31 ND 6.43 NA ND 6.5 NA
USTG480-MW32 6.14 6.21 0.07 6.34 6.50 0.16
USTG480-MW33R ND 5.25 NA ND 6.71 NA
IR35-MW67AR ND 6.80 NA ND 6.84 NA
Recovery Sump 4.77 4.90 0.13 4.55 4.85 0.30
IR35-MW14 ND 9.65 NA ND 9.87 NA
IR35-MW14D ND 9.63 NA ND 9.86 NA
10 20
DTP DTW Product
Thickness DTP DTW Product
Thickness
USTG480-MW01 ND 5.92 NA NM NM NM
USTG480-MW02 ND 7.12 NA ND 6.91 NA
USTG480-MW03 6.81 6.83 0.02 6.61 6.71 0.10
USTG480-MW04R ND 7.57 NA ND 7.24 NA
USTG480-MW06 ND 7.01 NA ND 6.80 NA
USTG480-MW07 ND 5.93 NA ND 5.51 NA
USTG480-MW08 ND 7.62 NA ND 4.97 NA
USTG480-MW09R ND 7.39 NA NM NM NM
USTG480-MW10 ND 6.44 NA NM NM NM
USTG480-MW11 ND 5.95 NA NM NM NM
USTG480-MW12 ND 6.05 NA NM NM NM
USTG480-MW13 7.34 7.94 0.60 ND 6.64 NA
USTG480-MW14 ND 6.81 NA NM NM NM
USTG480-MW15 ND 6.10 NA NM NM NM
USTG480-MW16 ND 6.02 NA NM NM NM
USTG480-MW17 ND 5.86 NA NM NM NM
USTG480-MW18 ND 7.16 NA NM NM NM
USTG480-MW20 6.65 7.03 0.38 6.41 6.81 0.40
USTG480-MW23 ND 5.41 NA NM NM NM
USTG480-MW24 ND 5.05 NA NM NM NM
USTG480-MW25 ND 6.05 NA NM NM NM
USTG480-MW26 ND 3.67 NA NM NM NM
USTG480-MW27 ND 7.05 NA NM NM NM
USTG480-MW28 6.18 6.25 0.07 6.71 6.86 0.15
USTG480-MW29 ND 3.82 NA ND 3.60 NA
USTG480-MW30 ND 3.30 NA NM NM NM
USTG480-MW31 ND 7.16 NA ND 6.94 NA
USTG480-MW32 6.90 7.16 0.26 ND 6.53 NA
USTG480-MW33R ND 6.03 NA NM NM NM
IR35-MW09S ND 7.00 NA NM NM NM
IR35-MW09IW ND 7.35 NA NM NM NM
IR35-MW14S ND 10.00 NA NM NM NM
IR35-MW14D ND 10.02 NA NM NM NM
IR35-MW31A ND 9.71 NA NM NM NM
IR35-MW31B ND 9.69 NA NM NM NM
IR35-MW67AR ND 7.30 NA ND 7.16 NA
USTTC341-MW01 ND 4.40 NA NM NM NM
USTTC341-MW02 ND 4.79 NA NM NM NM
USTTC341-MW03 ND 7.91 NA NM NM NM
USTTC341-MW05 ND 6.80 NA NM NM NM
USTTC341-MW06 ND 7.43 NA NM NM NM
USTTC341-MW08 ND 4.76 NA NM NM NM
USTTC341-MW09 ND 7.43 NA NM NM NM
USTTC341-MW10 ND 6.98 NA NM NM NM
USTTC341-MW11 ND 6.60 NA NM NM NM
USTTC341-MW12 ND 6.71 NA NM NM NM
USTTC341-MW13 ND 7.05 NA NM NM NM
USTTC341-MW14 ND 5.32 NA NM NM NM
USTTC341-MW15 ND 5.41 NA NM NM NM
USTTC341-MW17 ND 4.88 NA NM NM NM
USTTC341-IW01 ND 7.91 NA ND 7.68 NA
USTTC341-IW02 ND 7.60 NA NM NM NM
USTTC341-IW03 ND 7.64 NA NM NM NM
USTTC341-IW04 ND 6.84 NA ND 6.51 NA
USTTC341-IW05 ND 7.10 NA ND 6.91 NA
USTTC341-IW06 ND 6.98 NA ND 6.88 NA
USTTC341-RW01 ND 9.35 NA ND 11.50 NA
USTTC341-RW02 ND 8.85 NA ND 8.70 NA
USTTC341-RW03 ND 6.60 NA ND 9.75 NA
USTTC341-RW04 ND 6.90 NA ND 10.58 NA
USTTC341-RW05 ND 9.20 NA ND 7.18 NA
USTTC341-RW06 ND 11.55 NA ND 11.60 NA
USTTC341-RW07 ND 11.45 NA ND 11.42 NA
USTCGFF-EMW01 ND 8.31 NA NM NM NM
USTTC341-SUMP 6.10 6.25 0.15 5.88 6.10 0.22
USTTC341-OW01 NM NM NM NM NM NM
USTTC341-OW02 7.84 7.86 0.02 NM NM NM
USTTC341-IS01 ND 7.04 NA NM NM NM
USTTC341-IS03 ND 7.60 NA NM NM NM
Well 9/29/2014 10/9/2014
Product Recovered (gal): Product Recovered (gal):
Well 1/6/2015 2/10/2015
Page 7 of 10
RHE~
• CONSULTECH JV
GAUGING, BAILING, AND AFVR DATA
MCAS New River, North Carolina
Contract No. N40085-15-D-0007, CTO: 0004
TC-341
2018 Annual Monitoring Report
APPENDIX A
DTP DTW Product
Thickness DTP DTW Product
Thickness
USTTC341-RW01 ND 4.20 NA ND 4.10 NA
USTTC341-RW02 ND 8.70 NA ND 8.68 NA
USTTC341-RW03 ND 7.18 NA ND 6.85 NA
USTTC341-RW04 ND 7.31 NA ND 7.11 NA
USTTC341-RW05 ND 9.16 NA ND 9.12 NA
USTTC341-RW06 ND 11.58 NA ND 11.60 NA
USTTC341-RW07 ND 11.43 NA 4.66 4.74 0.08
USTTC341-IW01 ND 8.00 NA ND 7.96 NA
USTTC341-IW04 ND 7.11 NA ND 7.28 NA
USTTC341-IW05 ND 7.09 NA ND 7.22 NA
USTTC341-IW06 ND 7.05 NA ND 7.32 NA
USTG480-MW03 ND 7.02 NA 7.4 7.42 0.02
USTG480-MW04R ND 7.22 NA ND 7.31 NA
USTG480-MW06 ND 7.53 NA ND 7.45 NA
USTG480-MW07 6.49 6.52 0.03 6.01 6.12 0.11
USTG480-MW08 ND 8.22 NA ND 7.87 NA
USTG480-MW13 7.79 8.50 0.71 ND 7.29 NA
USTG480-MW20 6.36 6.89 0.53 6.58 7.26 0.68
USTG480-MW28 6.47 7.45 0.98 6.01 6.72 0.71
USTG480-MW29 ND 4.23 NA ND 3.98 NA
USTG480-MW31 ND 7.59 NA
USTG480-MW32 ND 6.61 NA ND 7.40 NA
IR35-MW67AR ND 7.63 NA ND 7.76 NA
Recovery Sump 10.94 10.95 0.01 ND 10.92 NA
DTP DTW Product
Thickness DTP DTW Product
Thickness
USTTC341-RW01 ND 10.50 NA ND 9.35 NA
USTTC341-RW02 ND 5.90 NA ND 4.81 NA
USTTC341-RW03 ND 6.31 NA ND 9.95 NA
USTTC341-RW04 ND 6.57 NA ND 5.46 NA
USTTC341-RW05 ND 9.18 NA ND 9.14 NA
USTTC341-RW06 ND 11.65 NA 5.6 5.78 0.18
USTTC341-RW07 4.19 4.25 0.06 ND 11.41 NA
USTTC341-IW01 ND 7.67 NA ND 6.65 NA
USTTC341-IW04 ND 7.20 NA ND 6.05 NA
USTTC341-IW05 ND 7.42 NA ND 6.48 NA
USTTC341-IW06 ND 7.48 NA ND 6.50 NA
USTG480-MW03 7.28 7.64 0.36 ND 6.45 NA
USTG480-MW04R ND 7.59 NA ND 6.77 NA
USTG480-MW06 ND 7.19 NA ND 6.10 NA
USTG480-MW07 ND 5.48 NA ND 4.33 NA
USTG480-MW08 ND 7.18 NA ND 7.56 NA
USTG480-MW13 7.09 7.17 0.08 8.5 8.75 0.25
USTG480-MW20 6.87 7.44 0.57 6.01 6.41 0.40
USTG480-MW28 ND 5.47 NA 4.75 8.50 3.75
USTG480-MW29 ND 3.69 NA ND 3.65 NA
USTG480-MW31 ND 7.56 NA ND 6.42 NA
USTG480-MW32 ND 7.32 NA ND 6.18 NA
IR35-MW67AR ND 7.73 NA ND 6.61 NA
Recovery Sump ND 10.93 NA 4.8 5.18 0.38
4
DTP DTW Product Thickness DTP DTW Product Thickness
USTTC341-RW01 ND 11.85 NA ND 9.62 NA
USTTC341-RW02 ND 10.75 NA ND 9.44 NA
USTTC341-RW03 ND 9.91 NA ND 8.58 NA
USTTC341-RW04 ND 10.10 NA ND 9.12 NA
USTTC341-RW05 ND 10.80 NA ND 9.52 NA
USTTC341-RW06 ND 9.10 NA ND 8.74 NA
USTTC341-RW07 ND 6.50 NA ND 6.28 NA
USTTC341-IW01 ND 7.39 NA ND 7.39 NA
USTTC341-IW04 ND 7.51 NA ND 7.56 NA
USTTC341-IW05 ND 7.78 NA ND 7.18 NA
USTTC341-IW06 ND 7.61 NA ND 7.19 NA
USTG480-MW03 7.95 8.15 0.20 7.51 8.44 0.93
USTG480-MW04R ND 8.04 NA ND 8.22 NA
USTG480-MW06 ND 7.61 NA ND 7.92 NA
USTG480-MW07 5.95 7.51 1.56 6.45 8.01 1.56
USTG480-MW08 8.50 9.60 1.10 8.52 9.70 1.18
USTG480-MW13 7.90 8.40 0.50 8.01 8.90 0.89
USTG480-MW20 7.10 7.79 0.69 7.42 8.20 0.78
USTG480-MW28 4.93 8.01 3.08 5.45 6.93 1.48
USTG480-MW29 ND 4.50 NA ND 5.90 NA
USTG480-MW31 ND 8.35 NA ND 7.22 NA
USTG480-MW32 7.98 8.30 0.32 8.11 8.55 0.44
IR35-MW67AR ND 7.93 NA ND 7.51 NA
Recovery Sump 7.93 8.81 0.88 ND 9.62 NA
DTP DTW Product
Thickness DTP DTW Product
Thickness
USTTC341-RW01 ND 9.88 NA ND 11.45 NA
USTTC341-RW02 ND 10.01 NA ND 10.65 NA
USTTC341-RW03 ND 9.63 NA ND 9.95 NA
USTTC341-RW04 ND 8.76 NA ND 10.15 NA
USTTC341-RW05 ND 9.41 NA ND 9.65 NA
USTTC341-RW06 ND 9.87 NA ND 7.35 NA
USTTC341-RW07 ND 8.88 NA ND 5.75 NA
USTTC341-IW01 6.95 6.96 0.01 ND 7.20 NA
USTTC341-IW04 ND 5.71 NA ND 7.35 NA
USTTC341-IW05 ND 8.95 NA ND 7.75 NA
USTTC341-IW06 ND 6.10 NA ND 7.55 NA
USTG480-MW03 ND 6.51 NA 8.15 8.25 0.10
USTG480-MW04R ND 6.83 NA ND 8.05 NA
USTG480-MW06 ND 5.80 NA ND 7.65 NA
USTG480-MW07 ND 4.28 NA 6.20 7.30 1.10
USTG480-MW08 8.98 9.21 0.23 8.20 9.50 1.30
USTG480-MW13 8.53 8.55 0.02 7.95 8.65 0.70
USTG480-MW20 ND 9.70 NA 7.10 9.25 2.15
USTG480-MW28 6.79 7.01 0.22 4.95 7.45 2.50
USTG480-MW29 ND 6.23 NA ND 3.65 NA
USTG480-MW31 ND 6.44 NA N/A N/A NA
USTG480-MW32 ND 7.53 NA ND 7.30 NA
IR35-MW67AR ND 9.62 NA ND 7.45 NA
Recovery Sump ND 9.88 NA 7.75 8.25 0.50
Well 8/11/2015 9/23/2015
Well 10/7/2015 11/11/2015
4/1/2015
NA-injection in progress
Well 5/5/2015 6/29/2015
Product Recovered (gal):
Well 3/10/2015
Page 8 of 10
RHE~
• CONSULTECH JV
GAUGING, BAILING, AND AFVR DATA
MCAS New River, North Carolina
Contract No. N40085-15-D-0007, CTO: 0004
TC-341
2018 Annual Monitoring Report
APPENDIX A
DTP DTW Product
Thickness DTP DTW Product
Thickness
USTTC341-RW01 ND 7.55 NA ND 10.85 NA
USTTC341-RW02 ND 5.80 NA ND 9.75 NA
USTTC341-RW03 ND 6.20 NA ND 9.10 NA
USTTC341-RW04 ND 10.70 NA ND 9.50 NA
USTTC341-RW05 ND 9.55 NA ND 9.65 NA
USTTC341-RW06 ND 4.67 NA ND 5.70 NA
USTTC341-RW07 ND 3.45 NA ND 3.70 NA
USTTC341-IW01 ND 7.46 NA ND 6.01 NA
USTTC341-IW04 ND 6.08 NA ND 5.50 NA
USTTC341-IW05 ND 6.36 NA ND 6.12 NA
USTTC341-IW06 ND 6.74 NA ND 6.32 NA
USTG480-MW03 7.70 7.80 0.10 ND 5.91 NA
USTG480-MW04R ND 6.74 NA ND 6.49 NA
USTG480-MW06 ND 6.25 NA ND 5.92 NA
USTG480-MW07 3.76 7.30 3.54 3.74 5.05 1.31
USTG480-MW08 7.25 7.36 0.11 ND 6.51 NA
USTG480-MW13 6.85 7.85 1.00 5.62 5.71 0.09
USTG480-MW20 5.55 6.10 0.55 5.82 5.91 0.09
USTG480-MW28 3.90 6.55 2.65 3.40 4.51 1.11
USTG480-MW29 ND 3.18 NA ND 3.59 NA
USTG480-MW31 ND 6.93 NA ND 6.01 NA
USTG480-MW32 ND 6.61 NA ND 5.82 NA
IR35-MW67AR ND 6.98 NA ND 6.41 NA
Recovery Sump 6.00 7.50 1.50 4.95 5.01 0.06
0.4
DTP DTW Product
Thickness DTP DTW Product
Thickness
USTTC341-RW01 ND 4.50 NA ND 5.05 NA
USTTC341-RW02 ND 4.30 NA ND 8.34 NA
USTTC341-RW03 ND 4.65 NA ND 8.00 NA
USTTC341-RW04 ND 4.81 NA ND 4.45 NA
USTTC341-RW05 ND 2.70 NA 4.45 6.00 1.55
USTTC341-RW06 ND 4.58 NA 4.25 4.60 0.35
USTTC341-RW07 ND 4.30 NA ND 3.13 NA
USTTC341-IW01 ND 6.00 NA ND 6.65 NA
USTTC341-IW04 ND 6.32 NA ND 5.12 NA
USTTC341-IW05 ND 7.00 NA ND 6.14 NA
USTTC341-IW06 ND 7.15 NA ND 6.47 NA
USTG480-MW03 5.90 7.70 1.80 ND 6.05 NA
USTG480-MW04R 6.20 7.53 1.33 ND 6.65 NA
USTG480-MW06 5.65 7.00 1.35 ND 5.80 NA
USTG480-MW07 3.60 6.10 2.50 3.50 4.95 1.45
USTG480-MW08 ND 5.53 NA 6.06 6.80 0.74
USTG480-MW13 5.45 5.49 0.04 5.83 5.85 0.02
USTG480-MW20 5.65 6.96 1.31 6.00 6.10 0.10
USTG480-MW28 2.48 5.80 3.32 2.73 4.90 2.17
USTG480-MW29 ND 2.51 NA ND 2.91 NA
USTG480-MW31 ND 6.00 NA ND 6.33 NA
USTG480-MW32 ND 5.66 NA ND 6.00 NA
IR35-MW67AR ND 7.43 NA ND 6.57 NA
Recovery Sump 6.00 7.00 1.00 ND 4.90 NA
2.94 3.25
DTP DTW Product
Thickness DTP DTW Product
Thickness
USTTC341-RW01 ND 5.70 NA ND 6.40 NA
USTTC341-RW02 ND 5.45 NA ND 8.90 NA
USTTC341-RW03 ND 5.90 NA ND 10.25 NA
USTTC341-RW04 ND 5.95 NA ND 7.50 NA
USTTC341-RW05 3.50 3.82 0.32 ND 9.20 NA
USTTC341-RW06 4.80 5.23 0.43 ND 11.50 NA
USTTC341-RW07 5.15 5.45 0.30 ND 11.50 NA
USTTC341-IW01 ND 7.10 NA ND 8.31 NA
USTTC341-IW04 ND 6.65 NA ND 7.06 NA
USTTC341-IW05 6.80 7.20 0.40 ND 7.05 NA
USTTC341-IW06 ND 7.21 NA ND 7.05 NA
USTG480-MW03 ND 6.95 NA ND 7.58 NA
USTG480-MW04R ND 6.47 NA ND 7.58 NA
USTG480-MW06 ND 6.58 NA ND 7.45 NA
USTG480-MW07 4.21 7.54 3.33 6.15 9.27 3.12
USTG480-MW08 6.50 7.50 1.00 8.03 9.85 1.82
USTG480-MW13 6.63 7.30 0.67 ND 7.45 NA
USTG480-MW20 6.63 9.82 3.19 6.85 7.16 0.31
USTG480-MW28 3.65 6.14 2.49 6.10 7.50 1.40
USTG480-MW29 ND 3.37 NA ND 4.45 NA
USTG480-MW31 ND 7.16 NA ND 7.73 NA
USTG480-MW32 ND 6.74 NA ND 7.40 NA
IR35-MW67AR ND 7.30 NA ND 7.85 NA
Recovery Sump ND 11.00 NA ND 11.00 NA
3.0175 0.896
DTP DTW Product
Thickness
USTTC341-RW01 ND 6.55 NA
USTTC341-RW02 ND 8.78 NA
USTTC341-RW03 ND 10.40 NA
USTTC341-RW04 ND 10.75 NA
USTTC341-RW05 ND 9.30 NA
USTTC341-RW06 ND 11.60 NA
USTTC341-RW07 ND 11.50 NA
USTTC341-IW01 ND 8.53 NA
USTTC341-IW04 ND 7.61 NA
USTTC341-IW05 ND 7.35 NA
USTTC341-IW06 ND 7.81 NA
USTG480-MW03 ND 7.70 NA
USTG480-MW04R ND 7.67 NA
USTG480-MW06 ND 7.65 NA
USTG480-MW07 6.20 8.87 2.67
USTG480-MW08 8.40 9.27 0.87
USTG480-MW13 7.58 7.66 0.08
USTG480-MW20 6.95 7.45 0.50
USTG480-MW28 6.20 8.85 2.65
USTG480-MW29 ND 4.42 NA
USTG480-MW31 ND 7.89 NA
USTG480-MW32 ND 7.70 NA
IR35-MW67AR ND 8.05 NA
Recovery Sump ND 11.00 NA
1.8116
Product Recovered (gal):
Product Recovered (gal):
Product Recovered (gal):
Well
4/29/2016 5/31/2016
Product Recovered (gal):
Well 6/13/2016
Product Recovered (gal):
Well 12/22/2015 1/14/2016
Product Recovered (gal):
Well 2/29/2016 3/31/2016
Page 9 of 10
RHE~
• CONSULTECH JV
GAUGING, BAILING, AND AFVR DATA
MCAS New River, North Carolina
Contract No. N40085-15-D-0007, CTO: 0004
TC-341
2018 Annual Monitoring Report
APPENDIX A
Date Water Recovered
10/22/2013 5
11/27/2013 5
12/11/2013 5
1/8/2014 5
2/18/2014 1
3/5/2014 5
4/30/2014 5
5/30/2014 200
6/2/2014 300
6/13/2014 400
6/19/2014 500
6/24/2014 200
7/3/2014 250
7/9/2014 400
7/16/2014 200
7/22/2014 200
7/31/2014 200
8/4/2014 0
8/12/2014 0
8/19/2014 0
8/27/2014 0
9/5/2014 0
9/10/2014 0
9/17/2014 0
9/24/2014 0
9/29/2014 0
10/9/2014 0
6/29/2015 0
1/14/2016 0
2/29/2016 0
3/31/2016 0
4/29/2016 0
5/31/2016 0
6/13/2016 0
7/11/2016 0
8/24/2016 0
9/12/2016 0
10/31/2016 0
11/28/2016 0
12/14/2016 0
1/30/2017 0
2/23/2017 0
3/30/2017 0
4/28/2017 0
5/31/2017 0
6/30/2017 0
7/21/2017 0
8/21/2017 0
9/4/2017 0
10/26/2017 0
11/30/2017 0
12/29/2017 0
1/31/2018 0
2/28/2018 0
3/29/2018 0
4/30/2018 0
5/31/2018 0
6/25/2018 0
7/18/2018 0
Totals 2,881
Notes:
DTP - Depth to product, measured from top of casing, in feet.
DTW - Depth to water, measured from top of casing, in feet.
ND: Not detected
NA: Not applicable
NM: Not Measured (monitoring well under pressure, not accessible)
Volume is measured in gallons
Gallons recovered is estimated based on the volume of the tank following gauging of the tank water level.
1.8116
0.896
3.0175
3.25
2.94
Recovery Totals (gallons)
Free-Phase Product Recovered
5
Rhea performed monthly gauging and bailing of monitoring wells with free-phase product from September 2013 through May 2014. In late May 2014, Rhea began
performing weekly AFVR events while the pump and treat system was offline.
3
5
1
1
5
5
7
10
15
20
8
15
25
10
10
10
7
8
5
5
8
269
8
5
10
10
20
4
0.4
0.5
0
2.5
0
0.5
0.37
0
0
0.2
0.6
0.1
0.5
3.25
0.3
0.25
0.35
0.06
0.1
0.87
0.15
0.01
0.47
0.35
0.09
0.1
Page 10 of 10
RHE~
• CONSULTECH JV
Monitoring Well Gauging SheetProject Name: TC341
Date of Gauging Event: 8/21/2017
Gauging Conducted by: AU
USTTC341-RW01 6.90 ND NA
USTTC341-RW02 8.80 ND NA
USTTC341-RW03 10.30 ND NA
USTTC341-RW04 11.00 ND NA
USTTC341-RW05 9.20 ND NA
USTTC341-RW06 11.50 ND NA
USTTC341-RW07 11.50 ND NA
USTTC341-IW01 7.80 ND NA
USTTC341-IW04 6.70 ND NA
USTTC341-IW05 6.53 ND NA
USTTC341-IW06 6.60 ND NA
USTG480-MW03 6.84 ND NA
USTG480-MW04R 6.90 ND NA
USTG480-MW06 6.95 ND NA
USTG480-MW07 5.96 5.77 0.19
USTG480-MW08 9.18 7.6 1.58
USTG480-MW13 6.70 ND NA
USTG480-MW20 6.52 5.9 0.62
USTG480-MW28 6.71 5.72 0.99
USTG480-MW29 3.55 ND NA
USTG480-MW31 7.09 ND NA
USTG480-MW32 6.85 ND NA
IR35-MW67AR 7.18 ND NA
Recovery Sump 10.91 ND NA
USTTC341-MW18 6.30 ND NA
Total Product Recovered 0.35 gallons
Notes: 1) ND: Not Detected
2) NA: Not Applicable
3) btoc: Below Top of Casing
Monitoring Well
Identification
Depth to Water (feet
btoc)
Depth to Product (feet
btoc)
Total Product
Thickness (feet)
RH E;~ /~"'~ >"--, ... ;
CONSULT ECH JV
Monitoring Well Gauging SheetProject Name: TC341
Date of Gauging Event: 9/14/2017
Gauging Conducted by: AU
USTTC341-RW01 6.20 ND NA
USTTC341-RW02 7.90 ND NA
USTTC341-RW03 8.80 ND NA
USTTC341-RW04 10.70 ND NA
USTTC341-RW05 9.00 ND NA
USTTC341-RW06 11.50 ND NA
USTTC341-RW07 11.50 ND NA
USTTC341-IW01 7.42 ND NA
USTTC341-IW04 6.40 ND NA
USTTC341-IW05 6.35 ND NA
USTTC341-IW06 6.45 ND NA
USTG480-MW03 6.52 ND NA
USTG480-MW04R 6.68 ND NA
USTG480-MW06 6.78 ND NA
USTG480-MW07 5.64 ND NA
USTG480-MW08 7.60 7.54 0.06
USTG480-MW13 6.35 ND NA
USTG480-MW20 6.50 5.76 0.74
USTG480-MW28 5.60 5.51 0.09
USTG480-MW29 3.50 ND NA
USTG480-MW31 6.70 ND NA
USTG480-MW32 6.52 ND NA
IR35-MW67AR 6.89 ND NA
Recovery Sump 6.00 ND NA
USTTC341-MW18 6.06 ND NA
Total Product Recovered 0.06 gallons
Notes: 1) ND: Not Detected
2) NA: Not Applicable
3) btoc: Below Top of Casing
Monitoring Well
Identification
Depth to Water (feet
btoc)
Depth to Product (feet
btoc)
Total Product
Thickness (feet)
CONSULTECHJV
Monitoring Well Gauging Sheet
Project Name: TC341
Date of Gauging Event: 10/26/2017Gauging Conducted by: AU
USTTC341-RW01 8.05 ND NA
USTTC341-RW02 7.37 ND NA
USTTC341-RW03 8.15 ND NA
USTTC341-RW04 10.80 ND NA
USTTC341-RW05 13.10 ND NA
USTTC341-RW06 11.70 ND NA
USTTC341-RW07 10.66 ND NA
USTTC341-IW01 10.89 ND NA
USTTC341-IW04 10.19 ND NA
USTTC341-IW05 7.17 ND NA
USTTC341-IW06 7.35 ND NA
USTG480-MW03 7.30 ND NA
USTG480-MW04R 7.32 ND NA
USTG480-MW06 7.37 ND NA
USTG480-MW07 5.80 ND NA
USTG480-MW08 8.95 8.00 0.95
USTG480-MW13 6.99 ND NA
USTG480-MW20 7.40 6.67 0.73
USTG480-MW28 6.05 5.32 0.73
USTG480-MW29 3.88 ND NA
USTG480-MW31 7.44 ND NA
USTG480-MW32 7.26 ND NA
IR35-MW67AR 7.63 ND NA
Recovery Sump 7.10 6.95 0.15
USTTC341-MW18 6.31 ND NA
Total Product Recovered 0.1 gallons
Notes: 1) ND: Not Detected
2) NA: Not Applicable
3) btoc: Below Top of Casing
Monitoring Well
Identification
Depth to Water (feet
btoc)
Depth to Product (feet
btoc)
Total Product
Thickness (feet)
CONSULTECH JV
Monitoring Well Gauging SheetProject Name: TC341
Date of Gauging Event: 11/30/2017
Gauging Conducted by: AU
USTTC341-RW01 8.82 ND NA
USTTC341-RW02 8.97 ND NA
USTTC341-RW03 10.35 ND NA
USTTC341-RW04 10.80 ND NA
USTTC341-RW05 13.80 ND NA
USTTC341-RW06 11.80 ND NA
USTTC341-RW07 10.70 ND NA
USTTC341-IW01 8.85 ND NA
USTTC341-IW04 7.60 ND NA
USTTC341-IW05 7.59 ND NA
USTTC341-IW06 7.74 ND NA
USTG480-MW03 7.79 ND NA
USTG480-MW04R 7.83 ND NA
USTG480-MW06 7.88 ND NA
USTG480-MW07 5.64 5.6 0.04
USTG480-MW08 12.28 8.27 4.01
USTG480-MW13 7.65 ND NA
USTG480-MW20 7.85 7.05 0.80
USTG480-MW28 7.72 6.41 1.31
USTG480-MW29 4.43 ND NA
USTG480-MW31 7.93 ND NA
USTG480-MW32 7.71 ND NA
IR35-MW67AR 8.02 ND NA
Recovery Sump 6.48 6.35 0.13
USTTC341-MW18 7.36 ND NA
Total Product Recovered 0.87 gallons
Notes: 1) ND: Not Detected
2) NA: Not Applicable
3) btoc: Below Top of Casing
Monitoring Well
Identification
Depth to Water (feet
btoc)
Depth to Product (feet
btoc)
Total Product
Thickness (feet)
CONSUi.TECH JV
Monitoring Well Gauging SheetProject Name: TC341
Date of Gauging Event: 12/29/2017
Gauging Conducted by: AU
USTTC341-RW01 6.25 ND NA
USTTC341-RW02 9.00 ND NA
USTTC341-RW03 10.40 ND NA
USTTC341-RW04 10.90 ND NA
USTTC341-RW05 13.30 ND NA
USTTC341-RW06 11.70 ND NA
USTTC341-RW07 10.70 ND NA
USTTC341-IW01 8.32 ND NA
USTTC341-IW04 7.32 ND NA
USTTC341-IW05 7.23 ND NA
USTTC341-IW06 7.30 ND NA
USTG480-MW03 7.47 ND NA
USTG480-MW04R 7.62 ND NA
USTG480-MW06 7.55 ND NA
USTG480-MW07 6.15 ND NA
USTG480-MW08 9.25 8.98 0.27
USTG480-MW13 7.41 ND NA
USTG480-MW20 7.23 6.71 0.52
USTG480-MW28 6.33 6.01 0.32
USTG480-MW29 4.05 ND NA
USTG480-MW31 7.46 ND NA
USTG480-MW32 7.67 ND NA
IR35-MW67AR 7.76 ND NA
Recovery Sump 10.80 ND NA
USTTC341-MW18 6.96 ND NA
Total Product Recovered 0.1 gallons
Notes: 1) ND: Not Detected
2) NA: Not Applicable
3) btoc: Below Top of Casing
Monitoring Well
Identification
Depth to Water (feet
btoc)
Depth to Product (feet
btoc)
Total Product
Thickness (feet)
RH E;~ /~"'~ >"--, ... ;
CONSULT ECH JV
Monitoring Well Gauging Sheet
Project Name: TC341
Date of Gauging Event: 1/31/2018Gauging Conducted by: AU
USTTC341-RW01 7.20 ND NA
USTTC341-RW02 9.01 ND NA
USTTC341-RW03 10.40 ND NA
USTTC341-RW04 10.80 ND NA
USTTC341-RW05 12.80 12.64 0.16
USTTC341-RW06 11.80 ND NA
USTTC341-RW07 10.80 ND NA
USTTC341-IW01 7.70 ND NA
USTTC341-IW04 6.58 ND NA
USTTC341-IW05 6.60 ND NA
USTTC341-IW06 6.72 ND NA
USTG480-MW03 6.74 ND NA
USTG480-MW04R 7.07 ND NA
USTG480-MW06 6.80 ND NA
USTG480-MW07 5.30 ND NA
USTG480-MW08 7.75 7.70 0.05
USTG480-MW13 6.69 ND NA
USTG480-MW20 6.46 6.11 0.35
USTG480-MW28 5.08 5.00 0.08
USTG480-MW29 3.34 ND NA
USTG480-MW31 6.50 ND NA
USTG480-MW32 6.72 ND NA
IR35-MW67AR 7.09 ND NA
Recovery Sump 5.90 ND NA
USTTC341-MW18 5.40 ND NA
Total Product Recovered 0.09 gallons
Notes: 1) ND: Not Detected
2) NA: Not Applicable
3) btoc: Below Top of Casing
Monitoring Well
Identification
Depth to Water (feet
btoc)
Depth to Product (feet
btoc)
Total Product
Thickness (feet)
' RHEA
CONSULTECH JV
Monitoring Well Gauging SheetProject Name: TC341
Date of Gauging Event: 2/28/2018
Gauging Conducted by: AU
USTTC341-RW01 8.80 ND NA
USTTC341-RW02 8.95 ND NA
USTTC341-RW03 10.35 ND NA
USTTC341-RW04 10.85 ND NA
USTTC341-RW05 12.80 12.65 0.15
USTTC341-RW06 11.85 ND NA
USTTC341-RW07 10.90 ND NA
USTTC341-IW01 8.29 ND NA
USTTC341-IW04 7.22 ND NA
USTTC341-IW05 7.15 ND NA
USTTC341-IW06 7.29 ND NA
USTG480-MW03 7.38 ND NA
USTG480-MW04R 7.31 ND NA
USTG480-MW06 7.46 ND NA
USTG480-MW07 6.23 ND NA
USTG480-MW08 9.20 8.30 0.90
USTG480-MW13 7.21 ND NA
USTG480-MW20 7.81 6.51 1.30
USTG480-MW28 7.90 6.03 1.87
USTG480-MW29 4.10 ND NA
USTG480-MW31 7.57 ND NA
USTG480-MW32 7.36 ND NA
IR35-MW67AR 7.67 ND NA
Recovery Sump 10.90 ND NA
USTTC341-MW18 6.92 ND NA
Total Product Recovered 0.35 gallons
Notes: 1) ND: Not Detected
2) NA: Not Applicable
3) btoc: Below Top of Casing
Monitoring Well
Identification
Depth to Water (feet
btoc)
Depth to Product (feet
btoc)
Total Product
Thickness (feet)
RHE;~f
/~.Jl///f ·~ , ..... /
CONSUL T ECH JV
Monitoring Well Gauging SheetProject Name: TC341
Date of Gauging Event: 3/29/2018
Gauging Conducted by: AU
USTTC341-RW01 8.40 ND NA
USTTC341-RW02 9.90 ND NA
USTTC341-RW03 10.35 ND NA
USTTC341-RW04 11.00 ND NA
USTTC341-RW05 13.80 13.20 0.60
USTTC341-RW06 11.80 ND NA
USTTC341-RW07 11.80 ND NA
USTTC341-IW01 8.36 ND NA
USTTC341-IW04 7.29 ND NA
USTTC341-IW05 7.15 ND NA
USTTC341-IW06 7.27 ND NA
USTG480-MW03 7.44 ND NA
USTG480-MW04R 7.43 ND NA
USTG480-MW06 7.54 ND NA
USTG480-MW07 6.42 6.35 0.07
USTG480-MW08 10.10 8.28 1.82
USTG480-MW13 7.30 ND NA
USTG480-MW20 7.40 6.52 0.88
USTG480-MW28 7.38 6.21 1.17
USTG480-MW29 4.12 ND NA
USTG480-MW31 7.62 ND NA
USTG480-MW32 7.41 ND NA
IR35-MW67AR 7.75 ND NA
Recovery Sump 10.92 ND NA
USTTC341-MW18 6.95 ND NA
Total Product Recovered 0.47 gallons
Notes: 1) ND: Not Detected
2) NA: Not Applicable
3) btoc: Below Top of Casing
Monitoring Well
Identification
Depth to Water (feet
btoc)
Depth to Product (feet
btoc)
Total Product
Thickness (feet)
CONSUi.TECH JV
Monitoring Well Gauging Sheet
Project Name: TC341
Date of Gauging Event: 4/30/2018Gauging Conducted by: AU
USTTC341-RW01 7.70 ND NA
USTTC341-RW02 9.00 ND NA
USTTC341-RW03 10.40 ND NA
USTTC341-RW04 10.85 ND NA
USTTC341-RW05 12.90 11.2 1.70
USTTC341-RW06 5.20 ND NA
USTTC341-RW07 4.00 3.90 0.10
USTTC341-IW01 7.44 ND NA
USTTC341-IW04 6.45 ND NA
USTTC341-IW05 6.59 ND NA
USTTC341-IW06 6.76 ND NA
USTG480-MW03 6.57 ND NA
USTG480-MW04R 6.91 ND NA
USTG480-MW06 6.60 ND NA
USTG480-MW07 4.81 ND NA
USTG480-MW08 7.92 7.32 0.60
USTG480-MW13 7.53 ND NA
USTG480-MW20 6.32 6.25 0.07
USTG480-MW28 2.89 2.85 0.04
USTG480-MW29 3.11 ND NA
USTG480-MW31 6.66 ND NA
USTG480-MW32 6.51 ND NA
IR35-MW67AR 6.99 ND NA
Recovery Sump 6.00 5.25 0.75
USTTC341-MW18 5.60 ND NA
Total Product Recovered 0.01 gallons
Notes: 1) ND: Not Detected
2) NA: Not Applicable
3) btoc: Below Top of Casing
Monitoring Well
Identification
Depth to Water (feet
btoc)
Depth to Product (feet
btoc)
Total Product
Thickness (feet)
CONSULTECH JV
Monitoring Well Gauging SheetProject Name: TC341
Date of Gauging Event: 5/31/2018
Gauging Conducted by: AU
USTTC341-RW01 8.75 ND NA
USTTC341-RW02 9.00 ND NA
USTTC341-RW03 10.35 ND NA
USTTC341-RW04 10.90 ND NA
USTTC341-RW05 11.50 ND NA
USTTC341-RW06 11.70 ND NA
USTTC341-RW07 11.50 ND NA
USTTC341-IW01 7.55 ND NA
USTTC341-IW04 6.48 ND NA
USTTC341-IW05 6.45 ND NA
USTTC341-IW06 6.49 ND NA
USTG480-MW03 6.63 ND NA
USTG480-MW04R 7.01 ND NA
USTG480-MW06 6.83 ND NA
USTG480-MW07 5.61 ND NA
USTG480-MW08 9.12 7.24 1.88
USTG480-MW13 6.56 ND NA
USTG480-MW20 6.12 5.93 0.19
USTG480-MW28 6.00 5.71 0.29
USTG480-MW29 3.45 ND NA
USTG480-MW31 6.79 ND NA
USTG480-MW32 6.60 ND NA
IR35-MW67AR 6.97 ND NA
Recovery Sump 9.80 ND NA
USTTC341-MW18 5.13 ND NA
Total Product Recovered 0.25 gallons
Notes: 1) ND: Not Detected
2) NA: Not Applicable
3) btoc: Below Top of Casing
Monitoring Well
Identification
Depth to Water (feet
btoc)
Depth to Product (feet
btoc)
Total Product
Thickness (feet)
CONSUi.TECH JV
Monitoring Well Gauging SheetProject Name: TC341
Date of Gauging Event: 6/25/2018
Gauging Conducted by: AU
USTTC341-RW01 5.00 ND NA
USTTC341-RW02 6.20 ND NA
USTTC341-RW03 5.20 ND NA
USTTC341-RW04 5.30 5.20 0.10
USTTC341-RW05 4.42 ND NA
USTTC341-RW06 3.95 ND NA
USTTC341-RW07 0.00 ND NA
USTTC341-IW01 6.43 ND NA
USTTC341-IW04 6.08 ND NA
USTTC341-IW05 6.40 ND NA
USTTC341-IW06 6.60 ND NA
USTG480-MW03 6.19 ND NA
USTG480-MW04R 6.85 ND NA
USTG480-MW06 6.11 ND NA
USTG480-MW07 3.97 ND NA
USTG480-MW08 5.95 ND NA
USTG480-MW13 5.48 ND NA
USTG480-MW20 6.90 5.95 0.95
USTG480-MW28 3.92 3.81 0.11
USTG480-MW29 2.60 ND NA
USTG480-MW31 6.34 ND NA
USTG480-MW32 6.10 ND NA
IR35-MW67AR 6.40 ND NA
Recovery Sump 5.00 4.90 0.10
USTTC341-MW18 4.30 ND NA
Total Product Recovered 0.15 gallons
Notes: 1) ND: Not Detected
2) NA: Not Applicable
3) btoc: Below Top of Casing
Monitoring Well
Identification
Depth to Water (feet
btoc)
Depth to Product (feet
btoc)
Total Product
Thickness (feet)
RH E;~ /~"'~ >"--, ... ;
CONSULT ECH JV
Monitoring Well Gauging Sheet
Project Name: TC341
Date of Gauging Event: 7/18/2018Gauging Conducted by: AW/LM
USTTC341-RW01 7.50 ND NA
USTTC341-RW02 9.20 ND NA
USTTC341-RW03 10.35 ND NA
USTTC341-RW04 10.60 ND NA
USTTC341-RW05 11.70 ND NA
USTTC341-RW06 11.30 ND NA
USTTC341-RW07 11.60 ND NA
USTTC341-IW01 8.30 ND NA
USTTC341-IW04 7.35 ND NA
USTTC341-IW05 7.25 ND NA
USTTC341-IW06 7.45 ND NA
USTG480-MW03 7.50 ND NA
USTG480-MW04R 7.29 ND NA
USTG480-MW06 7.65 ND NA
USTG480-MW07 6.47 ND NA
USTG480-MW08 8.53 8.39 0.14
USTG480-MW13 7.28 ND NA
USTG480-MW20 7.95 6.50 1.45
USTG480-MW28 6.68 6.47 0.21
USTG480-MW29 4.30 ND NA
USTG480-MW31 7.65 ND NA
USTG480-MW32 7.44 ND NA
IR35-MW67AR 7.80 ND NA
Recovery Sump 10.95 ND NA
USTTC341-MW18 5.60 ND NA
Total Product Recovered 0.37 gallons
Notes: 1) ND: Not Detected
2) NA: Not Applicable
3) btoc: Below Top of Casing
Monitoring Well
Identification
Depth to Water (feet
btoc)
Depth to Product (feet
btoc)
Total Product
Thickness (feet)
CONSULTECH JV
Monitoring Well Gauging Sheet
Project Name: TC341
Date of Gauging Event: 8/30/2018
Gauging Conducted by: AW
USTTC341-RW01 5.50 ND NA
USTTC341-RW02 9.01 ND NA
USTTC341-RW03 9.51 ND NA
USTTC341-RW04 8.75 ND NA
USTTC341-RW05 6.40 ND NA
USTTC341-RW06 11.70 ND NA
USTTC341-RW07 11.60 ND NA
USTTC341-IW01 7.53 ND NA
USTTC341-IW04 6.73 ND NA
USTTC341-IW05 6.61 ND NA
USTTC341-IW06 6.80 ND NA
USTG480-MW03 6.88 ND NA
USTG480-MW04R 6.63 ND NA
USTG480-MW06 7.00 ND NA
USTG480-MW07 5.78 ND NA
USTG480-MW08 7.77 7.35 0.42
USTG480-MW13 6.52 ND NA
USTG480-MW20 6.19 5.93 0.26
USTG480-MW26 3.71 3.44 0.27
USTG480-MW28 5.83 5.82 0.01
USTG480-MW29 3.70 ND NA
USTG480-MW31 6.99 ND NA
USTG480-MW32 6.81 ND NA
IR35-MW67AR 7.22 ND NA
Recovery Sump 10.97 ND NA
USTTC341-MW18 6.31 ND NA
Total Product Recovered 0.12 gallons
Notes: 1) ND: Not Detected
Monitoring Well
Identification
Depth to Water (feet
btoc)
Depth to Product (feet
btoc)
Total Product
Thickness (feet)
CONSULTECH JV
Monitoring Well Gauging Sheet
Project Name: TC341
Date of Gauging Event: 9/21/2018
Gauging Conducted by: AW/LM
USTTC341-RW01 3.80 ND NA
USTTC341-RW02 5.90 ND NA
USTTC341-RW03 5.90 ND NA
USTTC341-RW04 4.90 ND NA
USTTC341-RW05 3.40 ND NA
USTTC341-RW06 4.00 ND NA
USTTC341-RW07 11.60 ND NA
USTTC341-IW01 5.48 ND NA
USTTC341-IW04 5.03 ND NA
USTTC341-IW05 5.20 ND NA
USTTC341-IW06 5.75 5.30 0.45
USTG480-MW03 5.04 ND NA
USTG480-MW04R 5.73 ND NA
USTG480-MW06 5.21 ND NA
USTG480-MW07 3.60 ND NA
USTG480-MW08 5.12 ND NA
USTG480-MW13 4.79 ND NA
USTG480-MW20 5.02 4.83 0.19
USTG480-MW26 2.07 1.96 0.11
USTG480-MW28 7.13 ND NA
USTG480-MW29 2.00 ND NA
USTG480-MW31 5.13 ND NA
USTG480-MW32 4.96 ND NA
IR35-MW67AR 5.55 ND NA
Recovery Sump 8.00 ND NA
USTTC341-MW18 3.83 ND NA
Total Product Recovered 0.15 gallons
Notes: 1) ND: Not Detected
2) NA: Not Applicable
Monitoring Well
Identification
Depth to Water (feet
btoc)
Depth to Product (feet
btoc)
Total Product
Thickness (feet)
~ RHEA
~ ~
CONSULTECH JV
Monitoring Well Gauging Sheet
Project Name: TC341
Date of Gauging Event: 10/29/2018Gauging Conducted by: AW/LM
USTTC341-RW01 6.00 ND NA
USTTC341-RW02 9.00 ND NA
USTTC341-RW03 10.30 ND NA
USTTC341-RW04 10.80 ND NA
USTTC341-RW05 13.20 ND NA
USTTC341-RW06 11.80 ND NA
USTTC341-RW07 11.70 ND NA
USTTC341-IW01 8.02 ND NA
USTTC341-IW04 7.10 ND NA
USTTC341-IW05 7.10 ND NA
USTTC341-IW06 7.28 ND NA
USTG480-MW03 7.24 ND NA
USTG480-MW04R 7.13 ND NA
USTG480-MW06 6.80 ND NA
USTG480-MW07 5.42 ND NA
USTG480-MW08 8.42 ND NA
USTG480-MW13 7.15 ND NA
USTG480-MW20 6.60 ND NA
USTG480-MW26 4.60 4.00 0.60
USTG480-MW28 6.58 6.20 0.38
USTG480-MW29 4.25 ND NA
USTG480-MW31 7.46 ND NA
USTG480-MW32 7.23 ND NA
IR35-MW67AR 7.67 ND NA
Recovery Sump 11.00 ND NA
USTTC341-MW18 7.84 ND NA
Total Product Recovered <0.5 gallons
Notes: 1) ND: Not Detected
2) NA: Not Applicable
3) btoc: Below Top of Casing
Monitoring Well
Identification
Depth to Water (feet
btoc)
Depth to Product (feet
btoc)
Total Product
Thickness (feet)
CONSIJLTECH JV
Monitoring Well Gauging Sheet
Project Name: TC341Date of Gauging Event: 11/26/2018Gauging Conducted by: AU/LM
USTTC341-RW01 5.65 ND NA
USTTC341-RW02 9.00 ND NA
USTTC341-RW03 10.35 ND NA
USTTC341-RW04 10.80 ND NA
USTTC341-RW05 12.20 ND NA
USTTC341-RW06 11.80 ND NA
USTTC341-RW07 11.65 ND NA
USTTC341-IW01 7.72 ND NA
USTTC341-IW04 6.80 ND NA
USTTC341-IW05 6.70 ND NA
USTTC341-IW06 6.91 ND NA
USTG480-MW03 6.95 ND NA
USTG480-MW04R 6.98 ND NA
USTG480-MW06 7.01 ND NA
USTG480-MW07 5.60 ND NA
USTG480-MW08 7.87 7.65 0.22
USTG480-MW13 6.71 ND NA
USTG480-MW20 6.51 6.12 0.39
USTG480-MW26 3.65 3.39 0.26
USTG480-MW28 5.00 ND NA
USTG480-MW29 3.60 ND NA
USTG480-MW31 7.09 ND NA
USTG480-MW32 6.91 ND NA
IR35-MW67AR 7.58 ND NA
Recovery Sump 8.68 ND NA
USTTC341-MW18 6.34 ND NA
Total Product Recovered <0.5 gallons
Notes: 1) ND: Not Detected
2) NA: Not Applicable
3) btoc: Below Top of Casing
Monitoring Well
Identification
Depth to Water (feet
btoc)
Depth to Product (feet
btoc)
Total Product
Thickness (feet)
RH~ ~ ~
CONSULTECH JV
Monitoring Well Gauging Sheet
Project Name: TC341Date of Gauging Event: 12/17/2018Gauging Conducted by: LM
USTTC341-RW01 6.01 ND NA
USTTC341-RW02 9.98 ND NA
USTTC341-RW03 10.35 ND NA
USTTC341-RW04 10.20 ND NA
USTTC341-RW05 11.81 ND NA
USTTC341-RW06 11.31 ND NA
USTTC341-RW07 11.48 ND NA
USTTC341-IW01 7.69 ND NA
USTTC341-IW04 NM NM NM
USTTC341-IW05 6.75 ND NA
USTTC341-IW06 6.98 6.90 0.08
USTG480-MW03 NM NM NM
USTG480-MW04R 6.64 ND NA
USTG480-MW06 7.11 ND NA
USTG480-MW07 5.41 ND NA
USTG480-MW08 7.33 ND NA
USTG480-MW13 7.01 ND NA
USTG480-MW20 6.51 6.22 0.29
USTG480-MW26 3.58 3.34 0.24
USTG480-MW28 5.16 ND NA
USTG480-MW29 3.65 ND NA
USTG480-MW31 7.21 ND NA
USTG480-MW32 6.84 ND NA
IR35-MW67AR 7.51 7.42 NA
Recovery Sump NM NM NM
USTTC341-MW18 6.21 ND NA
Total Product Recovered 0
Notes: 1) ND: Not Detected
2) NA: Not Applicable
3) btoc: Below Top of Casing
Monitoring Well
Identification
Depth to Water (feet
btoc)
Depth to Product (feet
btoc)
Total Product
Thickness (feet)
Monitoring Well Gauging SheetProject Name: TC-341Project Number: 180815
Date of Gauging Event: 1/28/2019
Gauging Conducted by: Robert Thornton
USTTC341-RW01 5.37 ND NA
USTTC341-RW02 8.42 ND NA
USTTC341-RW03 7.54 ND NA
USTTC341-RW04 10.78 ND NA
USTTC341-RW05 5.22 ND NA
USTTC341-RW06 4.67 ND NA
USTTC341-RW07 3.34 ND NA
USTTC341-IW01 7.21 ND NA
USTTC341-IW04 6.61 ND NA
USTTC341-IW05 6.65 ND NA
USTTC341-IW06 6.80 ND NA
USTG480-MW03 8.76 ND NA
USTG480-MW04R 6.86 ND NA
USTG480-MW06 6.54 ND NA
USTG480-MW07 4.58 ND NA
USTG480-MW08 6.95 ND NA
USTG480-MW13 6.40 ND NA
USTG480-MW20 6.28 ND NA
USTG480-MW26 Not Measured Not Measured NA
USTG480-MW28 3.05 ND NA
USTG480-MW29 3.01 ND NA
USTG480-MW31 6.95 ND NA
USTG480-MW32 6.77 ND NA
USTTC341-MW18 Not Measured Not Measured NA
IR35-MW67AR 7.18 ND NA
Recovery Sump Not Measured Not Measured NA
Total Product Recovered 0 gallons
Notes: 1) ND: Not Detected
2) NA: Not Applicable
3) btoc: Below Top of Casing
Monitoring Well
Identification
Depth to Water (feet
btoc)
Depth to Product (feet
btoc)
Total Product
Thickness (feet)
DAVE~ORT
RHE ..
Monitoring Well Gauging Sheet
Project Name: TC-341
Project Number: 180815
Date of Gauging Event: 2/27/2019
Gauging Conducted by: Kevin DeFosset
USTTC341-RW01 5.68 ND NA
USTTC341-RW02 7.46 7.45 0.01
USTTC341-RW03 6.54 ND NA
USTTC341-RW04 10.75 10.74 0.01
USTTC341-RW05 12.90 12.38 0.52
USTTC341-RW06 8.04 8.03 0.01
USTTC341-RW07 11.65 ND NA
USTTC341-IW01 7.70 7.69 0.01
USTTC341-IW04 7.00 ND NA
USTTC341-IW05 6.94 ND NA
USTTC341-IW06 7.20 7.12 0.08
USTG480-MW03 8.76 8.75 0.01
USTG480-MW04R 7.17 ND NA
USTG480-MW06 7.17 ND NA
USTG480-MW07 5.84 5.61 0.23
USTG480-MW08 8.43 7.71 0.72
USTG480-MW13 6.79 ND NA
USTG480-MW20 6.73 6.33 0.40
USTG480-MW26 4.13 3.56 0.57
USTG480-MW28 6.00 5.32 0.68
USTG480-MW29 3.77 ND NA
USTG480-MW31 7.27 ND NA
USTG480-MW32 7.11 ND NA
USTTC341-MW18 6.28 ND NA
IR35-MW67AR 8.49 ND NA
Recovery Sump 11.01 ND NA
Total Product Recovered 0.4 gallons
Notes: 1) ND: Not Detected
2) NA: Not Applicable
3) btoc: Below Top of Casing
Monitoring Well Identification Depth to Water (feet btoc)Depth to Product (feet btoc)Total Product Thickness (feet)
DAVE~ORT
RHE
Monitoring Well Gauging Sheet
Project Name: TC-341Project Number: 180815
Date of Gauging Event: 3/27/2019Gauging Conducted by:Kevin DeFosset
USTTC341-RW01 12.26 ND NA
USTTC341-RW02 8.52 ND NA
USTTC341-RW03 10.28 ND NA
USTTC341-RW04 10.75 ND NA
USTTC341-RW05 13.61 ND NA
USTTC341-RW06 9.95 ND NA
USTTC341-RW07 11.66 ND NA
USTTC341-IW01 9.25 ND NA
USTTC341-IW04 7.74 ND NA
USTTC341-IW05 7.51 ND NA
USTTC341-IW06 7.62 7.92 0.30
USTG480-MW03 8.80 8.76 0.04
USTG480-MW04R 7.44 ND NA
USTG480-MW06 7.95 ND NA
USTG480-MW07 6.91 6.69 0.22
USTG480-MW08 9.67 9.16 0.51
USTG480-MW13 8.71 ND NA
USTG480-MW20 7.16 6.73 0.43
USTG480-MW26 3.92 3.70 0.22
USTG480-MW28 6.73 6.72 0.01
USTG480-MW29 4.54 ND NA
USTG480-MW31 8.36 ND NA
USTG480-MW32 8.00 ND NA
USTTC341-MW18 6.98 ND NA
IR35-MW67AR 8.06 ND NA
Recovery Sump 11.02 ND NA
Total Product Recovered 0.20 gallons
Notes: 1) ND: Not Detected
2) NA: Not Applicable
3) btoc: Below Top of Casing
Monitoring Well
Identification
Depth to Water (feet
btoc)
Depth to Product (feet
btoc)
Total Product
Thickness (feet)
D ~ N=>ORT
RHE
Monitoring Well Gauging Sheet
Project Name: TC-341Project Number: 180815
Date of Gauging Event: 4/24/2019
Gauging Conducted by:Kevin DeFosset
USTTC341-RW01 12.40 ND NA
USTTC341-RW02 8.45 ND NA
USTTC341-RW03 10.29 ND NA
USTTC341-RW04 10.69 ND NA
USTTC341-RW05 13.54 ND NA
USTTC341-RW06 9.99 ND NA
USTTC341-RW07 12.41 ND NA
USTTC341-IW01 9.49 ND NA
USTTC341-IW04 7.90 ND NA
USTTC341-IW05 7.66 ND NA
USTTC341-IW06 7.79 7.73 0.06
USTG480-MW03 8.81 8.79 0.02
USTG480-MW04R 7.76 ND NA
USTG480-MW06 8.12 ND NA
USTG480-MW07 7.09 6.90 0.19
USTG480-MW08 12.30 8.98 3.32
USTG480-MW13 9.32 ND NA
USTG480-MW20 7.07 6.91 0.16
USTG480-MW26 4.42 4.19 0.23
USTG480-MW28 6.87 6.82 0.05
USTG480-MW29 4.70 ND NA
USTG480-MW31 8.59 ND NA
USTG480-MW32 8.20 ND NA
USTTC341-MW18 7.67 ND NA
IR35-MW67AR 8.27 ND NA
Recovery Sump 8.48 8.47 0.01
Total Product Recovered 1.0 gallons
Notes: 1) ND: Not Detected
2) NA: Not Applicable
3) btoc: Below Top of Casing
Monitoring Well
Identification
Depth to Water
(feet btoc)
Depth to Product
(feet btoc)
Total Product Thickness
(feet)
DAYE~ORT
~~E~
Monitoring Well Gauging Sheet
Project Name:TC-341Project Number: 180815
Date of Gauging Event: 5/28/2019
Gauging Conducted by:Kevin DeFosset
USTTC341-RW01 13.42 ND NA
USTTC341-RW02 10.73 ND NA
USTTC341-RW03 10.17 ND NA
USTTC341-RW04 10.13 ND NA
USTTC341-RW05 13.60 ND NA
USTTC341-RW06 10.02 ND NA
USTTC341-RW07 12.42 ND NA
USTTC341-IW01 10.10 ND NA
USTTC341-IW04 8.54 ND NA
USTTC341-IW05 8.41 8.31 0.10
USTTC341-IW06 8.66 8.35 0.31
USTG480-MW03 8.78 ND NA
USTG480-MW04R 8.38 ND NA
USTG480-MW06 8.71 ND NA
USTG480-MW07 7.84 7.31 0.53
USTG480-MW08 12.30 9.45 2.85
USTG480-MW13 10.12 ND NA
USTG480-MW20 8.22 7.79 0.43
USTG480-MW26 5.41 5.30 0.11
USTG480-MW28 8.31 8.15 0.16
USTG480-MW29 5.14 ND NA
USTG480-MW31 9.28 ND NA
USTG480-MW32 8.86 ND NA
USTTC341-MW18 8.20 ND NA
IR35-MW67AR 8.89 ND NA
Recovery Sump 8.70 8.69 0.01
Total Product Recovered 0.9 gallons
Notes: 1) ND: Not Detected
2) NA: Not Applicable
3) btoc: Below Top of Casing
Monitoring Well
Identification
Depth to Water
(feet btoc)
Depth to Product
(feet btoc)
Total Product Thickness
(feet)
DAYE~ORT
~~E~
Monitoring Well Gauging Sheet
Project Name: TC-341Project Number: 180815
Date of Gauging Event: 6/13/2019
Gauging Conducted by:Jamie Burney
USTTC341-RW01 14.74 ND NA
USTTC341-RW02 10.88 ND NA
USTTC341-RW03 10.24 ND NA
USTTC341-RW04 10.79 ND NA
USTTC341-RW05 13.57 13.55 0.02
USTTC341-RW06 10.01 ND NA
USTTC341-RW07 12.18 ND NA
USTTC341-IW01 9.98 ND NA
USTTC341-IW04 8.39 ND NA
USTTC341-IW05 8.54 8.49 0.05
USTTC341-IW06 8.70 8.53 0.17
USTG480-MW03 8.80 ND NA
USTG480-MW04R 8.66 ND NA
USTG480-MW06 8.48 ND NA
USTG480-MW07 7.13 6.89 0.24
USTG480-MW08 10.78 9.16 1.62
USTG480-MW13 10.24 ND NA
USTG480-MW20 8.41 7.91 0.5
USTG480-MW26 5.20 5.18 0.02
USTG480-MW28 7.54 6.41 1.13
USTG480-MW29 4.91 ND NA
USTG480-MW31 9.37 ND NA
USTG480-MW32 8.81 ND NA
USTTC341-MW18 7.67 ND NA
IR35-MW67AR 8.96 ND NA
Recovery Sump 9.03 ND NA
Total Product Recovered 0.8 gallons
Notes: 1) ND: Not Detected
2) NA: Not Applicable
3) btoc: Below Top of Casing
Monitoring Well
Identification
Depth to Water
(feet btoc)
Depth to Product
(feet btoc)
Total Product Thickness
(feet)
DAYE~ORT
~~E~
Monitoring Well Gauging Sheet
Project Name: TC341
Project Number: 180815
Date of Gauging Event: 7/16/2019
Gauging Conducted by:Jamie Burney
USTTC341-RW01 16.07 ND NA 0
USTTC341-RW02 11.00 ND NA 0
USTTC341-RW03 10.27 ND NA 0
USTTC341-RW04 10.45 ND NA 0
USTTC341-RW05 14.75 ND NA 0
USTTC341-RW06 7.98 ND NA 0
USTTC341-RW07 12.52 ND NA 0
USTTC341-IW01 10.44 ND NA 0
USTTC341-IW04 8.89 ND NA 0
USTTC341-IW05 8.79 8.77 0.02 < 1
USTTC341-IW06 9.15 9 0.15 3
USTG480-MW03 9.86 9.83 0.03 0
USTG480-MW04R 8.98 ND NA 0
USTG480-MW06 8.62 ND NA 0
USTG480-MW07 7.86 7.45 0.41 4
USTG480-MW08 12.31 9.65 2.66 56
USTG480-MW13 9.26 9.25 0.01 2
USTG480-MW20 5.62 5.14 0.48 6
USTG480-MW26 5.45 ND NA 0
USTG480-MW28 7.83 7.26 0.57 6
USTG480-MW29 4.80 ND NA 0
USTG480-MW31 9.25 ND NA 0
USTG480-MW32 8.6 ND NA 0
USTTC341-MW18 7.73 ND NA 0
IR35-MW67AR 9.01 ND NA 0
Recovery Sump 9.08 ND NA 0
Total Product Recovered 78 ounces
Notes: 1) ND: Not Detected Total Product Recovered 0.61 gallons
2) NA: Not Applicable
3) btoc: Below Top of Casing
Monitoring Well
Identification
Depth to Water
(feet btoc)
Depth to Product
(feet btoc)
Total Product Thickness
(feet)
Total Product Removed
(ounces)
DAVE~ORT
RHE
Monitoring Well Gauging Sheet
Project Name: TC341
Project Number: 180815
Date of Gauging Event: 8/21/2019
Gauging Conducted by:Kevin DeFosset
USTTC341-RW01 16.75 ND NA
USTTC341-RW02 10.97 ND NA
USTTC341-RW03 10.26 ND NA
USTTC341-RW04 10.82 ND NA
USTTC341-RW05 10.95 ND NA
USTTC341-RW06 10.07 ND NA
USTTC341-RW07 12.76 ND NA
USTTC341-MW01 5.88 5.87 0.01
USTTC341-IW01 10.17 ND NA
USTTC341-IW04 8.85 ND NA
USTTC341-IW05 8.71 8.70 0.01
USTTC341-IW06 8.98 8.47 0.51
USTG480-MW03 9.17 9.14 0.03
USTG480-MW04R 8.90 ND NA
USTG480-MW06 8.76 ND NA
USTG480-MW07 7.75 7.33 0.42
USTG480-MW08 10.43 9.75 0.68
USTG480-MW13 10.90 10.43 0.47
USTG480-MW20 8.22 8.00 0.22
USTG480-MW23 6.09 ND NA
USTG480-MW26 4.90 4.89 0.01
USTG480-MW28 8.46 7.20 1.26
USTG480-MW29 5.12 ND NA
USTG480-MW31 9.42 ND NA
USTG480-MW32 8.97 ND NA
USTTC341-MW18 8.17 ND NA
IR35-MW67AR 9.01 ND NA
Recovery Sump 9.75 ND NA
Total Product Recovered 0.27 gallons
Notes: 1) ND: Not Detected
2) NA: Not Applicable
3) btoc: Below Top of Casing
4) Total Product Recovered does not include product removed by AFVR.
Monitoring Well
Identification
Depth to Water
(feet btoc)
Depth to Product
(feet btoc)
Total Product Thickness
(feet)
DAVEN='ORT
1:{~E .(\
Monitoring Well Gauging Sheet
Project Name: TC-341
Project Number: 180815
Date of Gauging Event: 9/16/2019
Gauging Conducted by:Jamie Burney
USTTC341-RW01 11.93 ND NA
USTTC341-RW02 10.88 ND NA
USTTC341-RW03 9.96 ND NA
USTTC341-RW04 10.82 ND NA
USTTC341-RW05 10.94 ND NA
USTTC341-RW06 10.04 ND NA
USTTC341-RW07 12.77 ND NA
USTTC341-MW01 4.91 ND NA
USTTC341-IW01 8.36 ND NA
USTTC341-IW04 7.12 ND NA
USTTC341-IW05 7.23 sheen NA
USTTC341-IW06 7.48 7.27 0.21
USTG480-MW03 7.32 ND NA
USTG480-MW04R 7.9 ND NA
USTG480-MW06 7.22 ND NA
USTG480-MW07 5.93 sheen NA
USTG480-MW08 8.11 ND NA
USTG480-MW13 7.84 sheen NA
USTG480-MW20 6.95 6.96 0.01
USTG480-MW23 5.93 ND NA
USTG480-MW26 3.55 ND NA
USTG480-MW28 6.06 6.04 0.02
USTG480-MW29 3.93 ND NA
USTG480-MW31 7.71 ND NA
USTG480-MW32 7.35 ND NA
USTTC341-MW18 5.71 ND NA
IR35-MW67AR 7.56 ND NA
Recovery Sump 8.16 ND NA
Total Product Recovered 0.02 gallons
Notes: 1) ND: Not Detected
2) NA: Not Applicable
3) btoc: Below Top of Casing
Monitoring Well
Identification
Depth to Water (feet
btoc)Depth to Product (feet btoc)Total Product Thickness
(feet)
DAVEN>ORT
~~EA\
Monitoring Well Gauging Sheet
Project Name: TC-341
Date of Gauging Event: 10/10/2019
Gauging Conducted by:Jamie Burney
USTTC341-RW01 12.61 ND NA
USTTC341-RW02 11.04 ND NA
USTTC341-RW03 10.29 ND NA
USTTC341-RW04 10.84 ND NA
USTTC341-RW05 10.72 ND NA
USTTC341-RW06 9.85 9.83 0.02
USTTC341-RW07 10.51 ND NA
USTTC341-MW01 5.90 5.89 0.01
USTTC341-IW01 8.36 ND NA
USTTC341-IW04 7.12 ND NA
USTTC341-IW05 7.23 ND NA
USTTC341-IW06 7.48 ND NA
USTG480-MW03 7.32 ND NA
USTG480-MW04R 7.90 ND NA
USTG480-MW06 7.22 ND NA
USTG480-MW07 5.93 ND NA
USTG480-MW08 8.11 ND NA
USTG480-MW13 7.84 ND NA
USTG480-MW16 6.27 ND NA
USTG480-MW17 5.88 ND NA
USTG480-MW18 7.94 ND NA
USTG480-MW20 6.95 ND NA
USTG480-MW23 5.93 ND NA
USTG480-MW26 3.55 ND NA
USTG480-MW28 NM NM NA
USTG480-MW29 NM NM NA
USTG480-MW30 NM NM NA
USTG480-MW31 7.71 ND NA
USTG480-MW32 7.35 ND NA
USTTC341-MW18 NM NM NA
IR35-MW67AR 7.56 ND NA
Recovery Sump 7.09 ND NA
Total Product Recovered
(gallons)0
Notes: 1) ND: Not Detected
2) NA: Not Applicable
3) btoc: Below Top of Casing
Monitoring Well
Identification
Depth to Water
(feet btoc)
Depth to Product
(feet btoc)
Total Product Thickness
(feet)
DAVE~ORT
~~E~
Monitoring Well Gauging Sheet
Project Name: TC-341
Date of Gauging Event: 11/14/2019
Gauging Conducted by:Airell Swanson
USTTC341-RW01 13.45 ND NA
USTTC341-RW02 10.90 ND NA
USTTC341-RW03 8.39 ND NA
USTTC341-RW04 10.76 ND NA
USTTC341-RW05 10.93 ND NA
USTTC341-RW06 9.95 ND NA
USTTC341-RW07 11.45 ND Sheen
USTTC341-MW01 6.35 6.15 0.20
USTTC341-IW01 9.59 ND NA
USTTC341-IW04 8.40 ND NA
USTTC341-IW05 8.42 ND NA
USTTC341-IW06 8.50 ND NA
USTG480-MW03 8.61 ND NA
USTG480-MW04R 8.78 ND NA
USTG480-MW06 8.50 ND NA
USTG480-MW07 7.25 ND NA
USTG480-MW08 10.90 9.15 1.75
USTG480-MW13 10.65 10.60 0.05
USTG480-MW16 6.40 ND NA
USTG480-MW17 5.87 ND NA
USTG480-MW18 7.75 ND NA
USTG480-MW20 8.00 ND NA
USTG480-MW23 7.15 7.09 0.06
USTG480-MW26 5.14 ND NA
USTG480-MW28 6.70 6.60 0.10
USTG480-MW29 5.02 ND NA
USTG480-MW30 4.37 ND NA
USTG480-MW31 8.99 ND NA
USTG480-MW32 8.64 ND NA
USTTC341-MW18 7.75 ND NA
IR35-MW67AR 8.85 ND NA
Recovery Sump 10.05 ND Sheen
Total Product Recovered
(gallons)0.4
Notes: 1) ND: Not Detected
2) NA: Not Applicable
3) btoc: Below Top of Casing
Monitoring Well
Identification
Depth to Water
(feet btoc)
Depth to Product
(feet btoc)
Total Product Thickness
(feet)
DAVEN='ORT
~~E ~
Monitoring Well Gauging Sheet
Project Name: TC-341
Date of Gauging Event: 12/4/2019
Gauging Conducted by:Airell Swanson
USTTC341-RW01 14.25 ND NA
USTTC341-RW02 10.97 ND NA
USTTC341-RW03 10.18 ND NA
USTTC341-RW04 10.75 ND NA
USTTC341-RW05 10.90 ND Sheen
USTTC341-RW06 10.57 ND NA
USTTC341-RW07 11.90 ND Sheen
USTTC341-MW01 5.27 5.25 0.02
USTTC341-IW01 9.05 ND NA
USTTC341-IW04 8.10 ND NA
USTTC341-IW05 8.05 ND NA
USTTC341-IW06 8.07 ND NA
USTG480-MW03 8.29 ND NA
USTG480-MW04R 8.43 ND NA
USTG480-MW06 8.27 ND NA
USTG480-MW07 6.60 ND Sheen
USTG480-MW08 9.40 8.70 0.70
USTG480-MW13 9.12 8.82 0.30
USTG480-MW16 6.09 ND NA
USTG480-MW17 5.69 ND NA
USTG480-MW18 7.57 ND NA
USTG480-MW20 7.61 7.52 0.09
USTG480-MW23 6.50 6.45 0.05
USTG480-MW26 4.32 4.30 0.02
USTG480-MW28 7.30 6.28 1.02
USTG480-MW29 4.60 ND NA
USTG480-MW30 3.99 ND NA
USTG480-MW31 8.50 ND NA
USTG480-MW32 8.30 ND NA
USTTC341-MW18 7.70 ND NA
IR35-MW67AR 8.50 ND NA
Recovery Sump 10.05 ND Sheen
Total Product Recovered
(gallons)0.6
Notes: 1) ND: Not Detected
2) NA: Not Applicable
3) btoc: Below Top of Casing
Monitoring Well
Identification
Depth to Water
(feet btoc)
Depth to Product
(feet btoc)
Total Product Thickness
(feet)
DAVEN='ORT
~~E ~
Monitoring Well Gauging Sheet
Project Name: TC-341
Project Number: 180820
Date of Gauging Event: 01/13-16/2020
Gauging Conducted by: KD
USTTC341-RW01 7.52 ND NA
USTTC341-RW02 11.01 ND NA
USTTC341-RW03 10.23 ND NA
USTTC341-RW04 10.42 ND NA
USTTC341-RW05 10.89 ND NA
USTTC341-RW06 10.05 ND NA
USTTC341-RW07 11.30 ND NA
USTTC341-MW01 5.46 5.45 0.01
USTTC341-IW01 8.92 ND NA
USTTC341-IW04 7.90 ND NA
USTTC341-IW05 7.90 ND NA
USTTC341-IW06 7.98 7.97 0.01
USTG480-MW03 8.04 ND NA
USTG480-MW04R 8.20 ND NA
USTG480-MW06 8.13 ND NA
USTG480-MW07 6.97 6.80 0.17
USTG480-MW08 10.12 8.75 1.37
USTG480-MW13 8.46 8.00 0.46
USTG480-MW16 6.19 ND NA
USTG480-MW17 5.63 ND NA
USTG480-MW18 7.60 ND NA
USTG480-MW20 7.47 7.42 0.05
USTG480-MW23 6.49 ND NA
USTG480-MW26 4.32 ND NA
USTG480-MW28 8.31 6.55 1.76
USTG480-MW29 4.69 ND NA
USTG480-MW30 4.04 ND NA
USTG480-MW31 8.28 ND NA
USTG480-MW32 8.02 ND NA
USTTC341-MW18 7.42 ND NA
IR35-MW67AR 8.34 ND NA
Recovery Sump 10.15 ND NA
Total Product Recovered
(gallons)1.1
Notes: 1) ND: Not Detected
2) NA: Not Applicable
3) btoc: Below Top of Casing
Monitoring Well
Identification
Depth to Water
(feet btoc)
Depth to Product
(feet btoc)
Total Product Thickness
(feet)
Monitoring Well Gauging Sheet
Project Name: TC-341
Project Number: 180820
Date of Gauging Event: 02/12-13/2020
Gauging Conducted by: JBW
USTTC341-RW01 14.75 ND NA
USTTC341-RW02 7.64 ND NA
USTTC341-RW03 9.98 ND NA
USTTC341-RW04 7.96 ND NA
USTTC341-RW05 11.01 ND NA
USTTC341-RW06 9.83 ND NA
USTTC341-RW07 13.01 ND NA
USTTC341-MW01 5.90 4.78 1.12
USTTC341-IW01 9.00 ND NA
USTTC341-IW04 7.79 ND NA
USTTC341-IW05 7.64 ND NA
USTTC341-IW06 7.72 ND NA
USTG480-MW03 8.01 ND NA
USTG480-MW04R 7.89 ND NA
USTG480-MW06 7.97 ND NA
USTG480-MW07 6.83 6.61 0.22
USTG480-MW08 9.13 8.87 0.26
USTG480-MW13 9.11 8.87 0.24
USTG480-MW16 5.80 ND NA
USTG480-MW17 5.37 ND NA
USTG480-MW18 7.24 ND NA
USTG480-MW20 7.20 7.13 0.07
USTG480-MW23 6.07 ND NA
USTG480-MW26 4.07 ND NA
USTG480-MW28 8.73 6.68 2.05
USTG480-MW29 4.51 ND NA
USTG480-MW30 3.77 ND NA
USTG480-MW31 8.38 ND NA
USTG480-MW32 8.03 ND NA
USTTC341-MW18 7.53 ND NA
IR35-MW67AR 8.20 ND NA
Recovery Sump 10.5 7.80 2.70
Total Product Recovered
(gallons)0.1
Notes: 1) ND: Not Detected
2) NA: Not Applicable
3) btoc: Below Top of Casing
Monitoring Well
Identification
Depth to Water
(feet btoc)
Depth to Product
(feet btoc)
Total Product Thickness
(feet)
Monitoring Well Gauging Sheet
Project Name: TC-341
Project Number: 180820
Date of Gauging Event: 3/4/2020
Gauging Conducted by: BR, SM
USTTC341-RW01 7.23 ND NA
USTTC341-RW02 7.49 ND NA
USTTC341-RW03 7.91 ND NA
USTTC341-RW04 8.06 ND NA
USTTC341-RW05 7.68 ND NA
USTTC341-RW06 6.84 ND NA
USTTC341-RW07 4.87 ND NA
USTTC341-MW01 4.21 ND NA
USTTC341-IW01 8.75 ND NA
USTTC341-IW04 7.49 ND NA
USTTC341-IW05 7.40 ND NA
USTTC341-IW06 7.41 ND NA
USTG480-MW03 7.65 ND NA
USTG480-MW04R 7.70 ND NA
USTG480-MW06 7.49 ND NA
USTG480-MW07 6.37 6.32 0.05
USTG480-MW08 9.08 8.96 0.12
USTG480-MW13 8.68 8.59 0.09
USTG480-MW16 5.60 ND NA
USTG480-MW17 5.09 ND NA
USTG480-MW18 6.79 ND NA
USTG480-MW20 6.76 6.75 0.01
USTG480-MW23 5.60 ND NA
USTG480-MW26 3.63 ND NA
USTG480-MW28 6.42 6.28 0.14
USTG480-MW29 3.93 ND NA
USTG480-MW30 3.44 ND NA
USTG480-MW31
USTG480-MW32 7.68 ND NA
USTTC341-MW18
IR35-MW67AR
Recovery Sump 8.21 ND NA
Total Product Recovered
(gallons)0.06
Notes: 1) ND: Not Detected
2) NA: Not Applicable
3) btoc: Below Top of Casing
NM
NM
Monitoring Well
Identification
Depth to Water
(feet btoc)
Depth to Product
(feet btoc)
Total Product Thickness
(feet)
NM - Obstruction
Monitoring Well Gauging Sheet
Project Name: TC-341
Project Number: 180820
Date of Gauging Event: 4/14/2020
Gauging Conducted by: BR
USTTC341-MW01 4.81 ND NA
USTTC341-IW01 9.13 ND NA
USTTC341-IW04 7.68 ND NA
USTTC341-IW05 7.54 ND NA
USTTC341-IW06 7.65 ND NA
USTG480-MW03 7.89 ND NA
USTG480-MW04R 7.65 ND NA
USTG480-MW06 7.92 ND NA
USTG480-MW07 6.89 ND NA
USTG480-MW08 9.05 9.04 0.01
USTG480-MW13 8.75 ND NA
USTG480-MW16 5.92 ND NA
USTG480-MW17 5.27 ND NA
USTG480-MW18 6.96 ND NA
USTG480-MW20 6.87 ND NA
USTG480-MW23 5.86 ND NA
USTG480-MW26 3.46 ND NA
USTG480-MW28 7.36 7.24 0.12
USTG480-MW29 4.49 ND NA
USTG480-MW30 3.78 ND NA
USTG480-MW31 5.21 ND NA
USTG480-MW32 8.89 ND NA
USTTC341-MW18 7.12 ND NA
IR35-MW67AR 8.06 ND NA
Total Product Recovered
(gallons)0.06
Notes: 1) ND: Not Detected
2) NA: Not Applicable
3) btoc: Below Top of Casing
Monitoring Well
Identification
Depth to Water
(feet btoc)
Depth to Product
(feet btoc)
Total Product Thickness
(feet)
DAVEN>ORT
~~E~
Monitoring Well Gauging Sheet
Project Name: TC-341
Project Number: 180820
Date of Gauging Event: 5/5/2020
Gauging Conducted by: BR / AA
USTTC341-MW01 5.16 ND NA
USTTC341-IW01 9.12 ND NA
USTTC341-IW04 8.07 ND NA
USTTC341-IW05 7.92 ND NA
USTTC341-IW06 8.01 ND NA
USTG480-MW03 8.28 ND NA
USTG480-MW04R 8.02 ND NA
USTG480-MW06 8.31 ND NA
USTG480-MW07 7.24 ND NA
USTG480-MW08 10.88 9.17 1.17
USTG480-MW13 9.43 9.17 0.26
USTG480-MW16 6.18 ND NA
USTG480-MW17 5.64 ND NA
USTG480-MW18 7.57 ND NA
USTG480-MW20 8.8 ND NA
USTG480-MW23 6.29 ND NA
USTG480-MW26 4.42 ND NA
USTG480-MW28 7.06 6.98 0.06
USTG480-MW29 4.83 ND NA
USTG480-MW30 4.1 ND NA
USTG480-MW31 8.64 ND NA
USTG480-MW32 8.3 ND NA
USTTC341-MW18 7.73 ND NA
IR35-MW67AR 8.46 ND NA
Total Product Recovered
(gallons)0.56
Notes: 1) ND: Not Detected
2) NA: Not Applicable
3) btoc: Below Top of Casing
Monitoring Well
Identification
Depth to Water
(feet btoc)
Depth to Product
(feet btoc)
Total Product Thickness
(feet)
DAVEN>ORT
~~E~
Monitoring Well Gauging Sheet
Project Name: TC-341
Project Number: 180820
Date of Gauging Event: 6/30/2020
Gauging Conducted by: BR/MO
USTTC341-MW01 5.64 4.5 1.14
USTTC341-IW01 8.35 8.3 0.05
USTTC341-IW04 6.93 ND NA
USTTC341-IW05 6.70 ND NA
USTTC341-IW06 6.85 ND NA
USTG480-MW03 7.28 ND NA
USTG480-MW04R 6.73 ND NA
USTG480-MW06 6.45 ND NA
USTG480-MW07 6.42 ND NA
USTG480-MW08 8.39 8.35 0.04
USTG480-MW13 8.03 7.99 0.04
USTG480-MW16 5.15 ND NA
USTG480-MW17 4.64 ND NA
USTG480-MW18 6.81 ND NA
USTG480-MW20 8.78 8.75 0.03
USTG480-MW23 4.70 ND NA
USTG480-MW26 6.32 ND NA
USTG480-MW28 6.45 6.36 0.09
USTG480-MW29 4.00 ND NA
USTG480-MW30 3.15 ND NA
USTG480-MW31 7.42 ND NA
USTG480-MW32 7.17 ND NA
USTTC341-MW18 5.91 ND NA
IR35-MW67AR 7.32 ND NA
Total Product Recovered
(gallons)0.05
Notes: 1) ND: Not Detected
2) NA: Not Applicable
3) btoc: Below Top of Casing
Monitoring Well
Identification
Depth to Water
(feet btoc)
Depth to Product
(feet btoc)
Total Product Thickness
(feet)
DAVEN>ORT
~~E~
Monitoring Well Gauging Sheet
Project Name: TC-341
Date of Gauging Event: 7/1/2020
Gauging Conducted by: BR/MO
USTTC341-MW01 5.64 4.5 1.14
USTTC341-IW01 8.35 8.3 0.05
USTTC341-IW04 6.93 ND NA
USTTC341-IW05 6.70 ND NA
USTTC341-IW06 6.85 ND NA
USTG480-MW03 7.28 ND NA
USTG480-MW04R 6.73 ND NA
USTG480-MW06 6.45 ND NA
USTG480-MW07 6.42 ND NA
USTG480-MW08 8.39 8.35 0.04
USTG480-MW13 8.03 7.99 0.04
USTG480-MW16 5.15 ND NA
USTG480-MW17 4.64 ND NA
USTG480-MW18 6.81 ND NA
USTG480-MW20 8.78 8.75 0.03
USTG480-MW23 4.70 ND NA
USTG480-MW26 6.32 ND NA
USTG480-MW28 6.45 6.36 0.09
USTG480-MW29 4.00 ND NA
USTG480-MW30 3.15 ND NA
USTG480-MW31 7.42 ND NA
USTG480-MW32 7.17 ND NA
USTTC341-MW18 5.91 ND NA
IR35-MW67AR 7.32 ND NA
Total Product Recovered
(gallons)0.05
Notes: 1) ND: Not Detected
2) NA: Not Applicable
3) btoc: Below Top of Casing
4) A passive skimmer was installed in USTG480-MW07 during March 2020
Monitoring Well
Identification
Depth to Water
(feet btoc)
Depth to Product
(feet btoc)
Total Product Thickness
(feet)
DAVEN>ORT
~~E~
Monitoring Well Gauging Sheet
Project Name: TC-341
Date of Gauging Event: 8/3/2020
Gauging Conducted by: BR/MO
USTTC341-MW01 4.83 ND NA
USTTC341-IW01 8.42 ND NA
USTTC341-IW04 7.44 ND NA
USTTC341-IW05 7.38 ND NA
USTTC341-IW06 7.52 ND NA
USTG480-MW03 7.64 ND NA
USTG480-MW04R 7.40 ND NA
USTG480-MW06 7.83 ND NA
USTG480-MW07 6.19 ND NA
USTG480-MW08 8.29 ND NA
USTG480-MW13 8.13 ND NA
USTG480-MW16 5.90 ND NA
USTG480-MW17 5.19 ND NA
USTG480-MW18 6.92 ND NA
USTG480-MW20 8.77 8.7 0.07
USTG480-MW23 5.91 ND NA
USTG480-MW26 4.31 3.96 0.35
USTG480-MW28 5.89 ND NA
USTG480-MW29 4.21 ND NA
USTG480-MW30 3.69 ND NA
USTG480-MW31 7.93 ND NA
USTG480-MW32 7.64 ND NA
USTTC341-MW18 7.01 ND NA
IR35-MW67AR 7.93 ND NA
Total Product Recovered
(gallons)0.04
Notes: 1) ND: Not Detected
2) NA: Not Applicable
3) btoc: Below Top of Casing
4) A passive skimmer was installed in USTG480-MW07 during March 2020
Monitoring Well
Identification
Depth to Water
(feet btoc)
Depth to Product
(feet btoc)
Total Product Thickness
(feet)
DAVEN>ORT
~~E~
Monitoring Well Gauging Sheet
Project Name: TC-341
Date of Gauging Event: 9/9/2020
Gauging Conducted by: BR/MO
USTTC341-MW01 4.54 ND NA
USTTC341-IW01 8.78 ND NA
USTTC341-IW04 7.52 ND NA
USTTC341-IW05 7.34 ND NA
USTTC341-IW06 7.46 ND NA
USTG480-MW03 7.71 ND NA
USTG480-MW04R 7.43 ND NA
USTG480-MW06 7.67 ND NA
USTG480-MW07 6.52 ND NA
USTG480-MW08 9.47 8.63 0.84
USTG480-MW13 9.05 8.85 0.20
USTG480-MW16 5.57 ND NA
USTG480-MW17 4.52 ND NA
USTG480-MW18 6.64 ND NA
USTG480-MW20 6.82 ND NA
USTG480-MW23 5.52 ND NA
USTG480-MW26 3.88 3.74 0.14
USTG480-MW28 5.44 ND NA
USTG480-MW29 4.08 ND NA
USTG480-MW30 3.56 ND NA
USTG480-MW31 8.07 ND NA
USTG480-MW32 7.7 ND NA
USTTC341-MW18 7.05 ND NA
IR35-MW67AR 7.93 ND NA
Total Product Recovered
(gallons)0.86
Notes: 1) ND: Not Detected
2) NA: Not Applicable
3) btoc: Below Top of Casing
4) A passive skimmer was installed in USTG480-MW07 in March 2020
5) A passive skimmer was installed in USTG480-MW13 and USTG480-MW20 in August 2020
Monitoring Well
Identification
Depth to Water
(feet btoc)
Depth to Product
(feet btoc)
Total Product Thickness
(feet)
DAVEN>ORT
~~E~
Monitoring Well Gauging SheetProject Name: TC-341Date of Gauging Event: 10/8/2020Gauging Conducted by:BR/MO
USTTC341-MW01 3.84 ND NA
USTTC341-IW01 8.41 ND NA
USTTC341-IW04 7.14 ND NA
USTTC341-IW05 6.94 ND NA
USTTC341-IW06 7.06 ND NA
USTG480-MW03 7.31 ND NA
USTG480-MW04R 7.06 ND NA
USTG480-MW06 8.33 ND NA
USTG480-MW07 6.34 ND NA
USTG480-MW08 8.77 8.38 0.39
USTG480-MW13 8.40 ND NA*
USTG480-MW16 5.43 ND NA
USTG480-MW17 4.21 ND NA
USTG480-MW18 6.48 ND NA
USTG480-MW20 7.03 ND NA*
USTG480-MW23 5.07 ND NA
USTG480-MW26 3.57 3.53 0.04
USTG480-MW28 5.90 ND NA
USTG480-MW29 3.83 ND NA
USTG480-MW30 3.32 ND NA
USTG480-MW31 7.61 ND NA
USTG480-MW32 7.33 ND NA
USTTC341-MW18 6.78 ND NA
IR35-MW67AR 7.53 ND NA
Total Product Recovered(gallons)0.40
Notes: 1) ND: Not Detected
2) NA: Not Applicable
3) btoc: Below Top of Casing
4) A passive skimmer was installed in USTG480-MW07 in March 2020
5) A passive skimmer was installed in USTG480-MW13 and USTG480-MW20 in August 2020
6) * Product not detected during gauging, but recovered with skimmer
Monitoring Well
Identification
Depth to Water
(feet btoc)
Depth to Product
(feet btoc)
Total Product Thickness
(feet)
DAVE~ORT
~~E~
Monitoring Well Gauging SheetProject Name: TC-341Date of Gauging Event: 11/2/2020Gauging Conducted by:BR/MO
USTTC341-MW01 3.43 ND NA
USTTC341-IW01 7.93 ND NA
USTTC341-IW04 7.19 ND NA
USTTC341-IW05 7.13 ND NA
USTTC341-IW06 7.31 ND NA
USTG480-MW03 7.31 ND NA
USTG480-MW04R 7.27 ND NA
USTG480-MW06 7.41 ND NA
USTG480-MW07 6.27 ND NA
USTG480-MW08 8.40 8.11 0.29
USTG480-MW13 7.36 ND NA*
USTG480-MW16 5.62 ND NA
USTG480-MW17 4.28 ND NA
USTG480-MW18 6.38 ND NA
USTG480-MW20 7.23 ND NA
USTG480-MW23 5.46 ND NA
USTG480-MW26 3.74 ND NA
USTG480-MW28 5.84 ND NA
USTG480-MW29 3.88 ND NA
USTG480-MW30 3.44 ND NA
USTG480-MW31 7.42 ND NA
USTG480-MW32 7.26 ND NA
USTTC341-MW18 6.59 ND NA
IR35-MW67AR 7.69 ND NA
Total Product Recovered(gallons)0.17
Notes: 1) ND: Not Detected
2) NA: Not Applicable
3) btoc: Below Top of Casing
4) A passive skimmer was installed in USTG480-MW07 in March 2020
5) A passive skimmer was installed in USTG480-MW13 and USTG480-MW20 in August 2020
6) * Product not detected during gauging, but recovered with skimmer
Monitoring Well
Identification
Depth to Water
(feet btoc)
Depth to Product
(feet btoc)
Total Product Thickness
(feet)
DAVEN>ORT
;l;{~E~
Monitoring Well Gauging SheetProject Name: TC-341Date of Gauging Event: 12/1/2020Gauging Conducted by:MO/BR
USTTC341-MW01 3.87 ND NA
USTTC341-IW01 8.32 ND NA
USTTC341-IW04 7.16 ND NA
USTTC341-IW05 7.04 ND NA
USTTC341-IW06 7.25 ND NA
USTG480-MW03 7.32 ND NA
USTG480-MW04R 7.26 ND NA
USTG480-MW06 3.85 ND NA
USTG480-MW07 6.26 ND NA
USTG480-MW08 8.88 8.24 0.64
USTG480-MW13 8.21 8.18 0.03
USTG480-MW16 5.54 ND NA
USTG480-MW17 4.81 ND NA
USTG480-MW18 5.59 ND NA
USTG480-MW20 8.23 ND NA
USTG480-MW23 5.14 ND NA
USTG480-MW26 3.37 ND NA
USTG480-MW28 5.81 ND NA
USTG480-MW29 3.34 ND NA
USTG480-MW30 3.28 ND NA
USTG480-MW31 7.55 ND NA
USTG480-MW32 7.3 ND NA
USTTC341-MW18 5.83 ND NA
IR35-MW67AR 7.64 ND NA
Total Product Recovered
(gallons)0.34
Notes: 1) ND: Not Detected
2) NA: Not Applicable
3) btoc: Below Top of Casing
4) A passive skimmer was installed in USTG480-MW07 in March 2020
5) A passive skimmer was installed in USTG480-MW13 and USTG480-MW20 in August 2020
Monitoring Well
Identification
Depth to Water
(feet btoc)
Depth to Product
(feet btoc)
Total Product Thickness
(feet)
DAVEN>ORT
~~E~
Monitoring Well Gauging SheetProject Name: TC-341Date of Gauging Event: 1/4/2021Gauging Conducted by:MO/BR
USTTC341-MW01 3.15 3.13 0.02
USTTC341-IW01 78.96 ND NA
USTTC341-IW04 7.12 ND NA
USTTC341-IW05 6.81 ND NA
USTTC341-IW06 6.92 ND NA
USTG480-MW03 7.33 ND NA
USTG480-MW04R 6.97 ND NA
USTG480-MW06 7.47 ND NA
USTG480-MW07 6.74 ND NA*
USTG480-MW08 8.83 8.80 0.03
USTG480-MW13 8.62 ND NA*
USTG480-MW16 5.44 ND NA
USTG480-MW17 4.22 ND NA
USTG480-MW18 4.18 ND NA
USTG480-MW20 6.79 ND NA*
USTG480-MW23 4.67 ND NA
USTG480-MW26 3.28 ND NA
USTG480-MW28 6.44 ND NA
USTG480-MW29 4.18 ND NA
USTG480-MW30 3.27 ND NA
USTG480-MW31 7.77 ND NA
USTG480-MW32 7.41 ND NA
USTTC341-MW18 6.58 ND NA
IR35-MW67AR 7.46 ND NA
Total Product Recovered(gallons)0.37
Notes: 1) ND: Not Detected
2) NA: Not Applicable
3) btoc: Below Top of Casing
4) A passive skimmer was installed in USTG480-MW07 in March 2020
5) A passive skimmer was installed in USTG480-MW13 and USTG480-MW20 in August 2020
6)* Product not detected during gauging, but recovered with skimmer
Monitoring Well
Identification
Depth to Water
(feet btoc)
Depth to Product
(feet btoc)
Total Product Thickness
(feet)
DAVE~ORT
~~E~
Monitoring Well Gauging SheetProject Name: TC-341Date of Gauging Event: 2/8/2021Gauging Conducted by:MO
USTTC341-MW01 3.49 ND NA
USTTC341-IW01 8.68 ND NA
USTTC341-IW04 7.13 ND NA
USTTC341-IW05 6.97 ND NA
USTTC341-IW06 7.05 ND NA
USTG480-MW03 7.31 ND NA
USTG480-MW04R 7.16 ND NA
USTG480-MW06 7.36 ND NA
USTG480-MW07 6.24 ND NA
USTG480-MW08 8.68 8.57 0.11
USTG480-MW13 8.63 ND NA*
USTG480-MW16 5.53 ND NA
USTG480-MW17 Measured not reported ND NA
USTG480-MW18 6.36 ND NA
USTG480-MW20 6.88 6.87 0.01
USTG480-MW23 4.91 ND NA
USTG480-MW26 3.07 ND NA
USTG480-MW28 5.93 ND NA
USTG480-MW29 4.00 ND NA
USTG480-MW30 3.31 ND NA
USTG480-MW31 7.76 ND NA
USTG480-MW32 7.38 ND NA
USTTC341-MW18 6.28 ND NA
IR35-MW67AR 7.53 ND NA
Total Product Recovered(gallons)0.24
Notes: 1) ND: Not Detected
2) NA: Not Applicable
3) btoc: Below Top of Casing
4) A passive skimmer was installed in USTG480-MW07 in March 2020
5) A passive skimmer was installed in USTG480-MW13 and USTG480-MW20 in August 2020
6) * Product not detected during gauging, but recovered with skimmer
Monitoring Well
Identification
Depth to Water
(feet btoc)
Depth to Product
(feet btoc)
Total Product Thickness
(feet)
DAVEN>ORT
~~E~
Monitoring Well Gauging SheetProject Name: TC-341Date of Gauging Event: 3/2/2021Gauging Conducted by:MO
USTTC341-MW01 3.15 ND NA
USTTC341-IW01 8.28 ND NA
USTTC341-IW04 6.42 ND NA
USTTC341-IW05 6.38 ND NA
USTTC341-IW06 7.70 7.57 0.13
USTG480-MW03 6.53 ND NA
USTG480-MW04R 6.55 ND NA
USTG480-MW06 7.02 ND NA
USTG480-MW07 6.34 ND NA
USTG480-MW08 8.65 8.29 0.36
USTG480-MW13 8.20 ND NA
USTG480-MW16 6.14 ND NA
USTG480-MW17 1.17 ND NA
USTG480-MW18 6.26 ND NA
USTG480-MW20 6.22 ND NA
USTG480-MW23 4.65 ND NA
USTG480-MW26 3.09 ND NA
USTG480-MW28 6.16 ND NA
USTG480-MW29 4.01 ND NA
USTG480-MW30 3.10 ND NA
USTG480-MW31 6.91 ND NA
USTG480-MW32 6.56 ND NA
USTTC341-MW18 6.51 ND NA
IR35-MW67AR 6.76 ND NA
Total Product Recovered
(gallons)0.17
Notes: 1) ND: Not Detected
2) NA: Not Applicable
3) btoc: Below Top of Casing
4) A passive skimmer was installed in USTG480-MW07 in March 2020
5) A passive skimmer was installed in USTG480-MW13 and USTG480-MW20 in August 2020
Monitoring Well
Identification
Depth to Water
(feet btoc)
Depth to Product
(feet btoc)
Total Product Thickness
(feet)
DAVE~ORT
~~E~
Monitoring Well Gauging SheetProject Name: TC-341Date of Gauging Event: 4/5/2021Gauging Conducted by:MO
USTTC341-MW01 4.18 ND NA
USTTC341-IW01 7.81 ND NA
USTTC341-IW04 6.91 ND NA
USTTC341-IW05 6.87 ND NA
USTTC341-IW06 7.65 7.00 0.65
USTG480-MW03 7.03 ND NA
USTG480-MW04R 7.07 ND NA
USTG480-MW06 7.36 ND NA
USTG480-MW07 6.24 ND NA
USTG480-MW08 9.07 7.87 1.20
USTG480-MW13 7.29 7.28 0.01
USTG480-MW16 5.77 ND NA
USTG480-MW17 4.70 ND NA
USTG480-MW18 6.37 ND NA
USTG480-MW20 6.97 6.91 0.06
USTG480-MW23 5.25 ND NA
USTG480-MW26 4.81 4.62 0.19
USTG480-MW28 6.24 ND NA
USTG480-MW29 4.29 ND NA
USTG480-MW30 3.78 ND NA
USTG480-MW31 7.2 ND NA
USTG480-MW32 6.97 ND NA
USTTC341-MW18 6.71 ND NA
IR35-MW67AR 7.35 ND NA
Total Product Recovered
(gallons)0.86
Notes: 1) ND: Not Detected
2) NA: Not Applicable
3) btoc: Below Top of Casing
4) A passive skimmer was installed in USTG480-MW07 in March 2020
5) A passive skimmer was installed in USTG480-MW13 and USTG480-MW20 in August 2020
Monitoring Well
Identification
Depth to Water
(feet btoc)
Depth to Product
(feet btoc)
Total Product Thickness
(feet)
Monitoring Well Gauging SheetProject Name: TC-341Date of Gauging Event: 5/3/2021Gauging Conducted by:MO
USTTC341-MW01 5.13 ND NA
USTTC341-IW01 8.28 ND NA
USTTC341-IW04 7.42 ND NA
USTTC341-IW05 7.43 ND NA
USTTC341-IW06 7.93 7.53 0.40
USTG480-MW03 7.55 ND NA
USTG480-MW04R 7.56 ND NA
USTG480-MW06 7.76 ND NA
USTG480-MW07 6.84 ND NA*
USTG480-MW08 9.96 8.21 1.75
USTG480-MW13 8.10 ND NA*
USTG480-MW16 6.14 ND NA
USTG480-MW17 5.26 ND NA
USTG480-MW18 7.17 ND NA
USTG480-MW20 7.53 7.48 0.05
USTG480-MW23 6.06 ND NA
USTG480-MW26 4.55 4.54 0.01
USTG480-MW28 6.52 ND NA
USTG480-MW29 4.58 ND NA
USTG480-MW30 4.02 ND NA
USTG480-MW31 7.74 ND NA
USTG480-MW32 7.48 ND NA
USTTC341-MW18 7.12 ND NA
IR35-MW67AR 7.84 ND NA
Total Product Recovered
(gallons)0.33
Notes: 1) ND: Not Detected
2) NA: Not Applicable
3) btoc: Below Top of Casing
4) A passive skimmer was installed in USTG480-MW07 in March 2020
5) A passive skimmer was installed in USTG480-MW13 and USTG480-MW20 in August 2020
6) * Product not detected during gauging, but recovered with skimmer
Monitoring Well
Identification
Depth to Water
(feet btoc)
Depth to Product
(feet btoc)
Total Product Thickness
(feet)
DAVE~ORT
~~E~
Monitoring Well Gauging SheetProject Name: TC-341Date of Gauging Event: 6/1/2021Gauging Conducted by:MO
USTTC341-MW01 5.55 ND NA
USTTC341-IW01 8.83 ND NA
USTTC341-IW04 7.77 ND NA
USTTC341-IW05 7.78 ND NA
USTTC341-IW06 8.41 7.91 0.50
USTG480-MW03 7.91 ND NA
USTG480-MW04R 7.92 ND NA
USTG480-MW06 8.11 ND NA
USTG480-MW07 6.88 ND NA*
USTG480-MW08 9.71 8.71 1.00
USTG480-MW13 8.41 8.36 0.05
USTG480-MW16 6.38 ND NA
USTG480-MW17 5.51 ND NA
USTG480-MW18 7.67 ND NA
USTG480-MW20 7.72 7.65 0.07
USTG480-MW23 6.40 ND NA
USTG480-MW26 4.88 4.77 0.11
USTG480-MW28 6.75 ND NA
USTG480-MW29 4.76 ND NA
USTG480-MW30 4.25 ND NA
USTG480-MW31 8.11 ND NA
USTG480-MW32 7.88 ND NA
USTTC341-MW18 7.45 ND NA
IR35-MW67AR 8.20 ND NA
Total Product Recovered
(gallons)0.78
Notes: 1) ND: Not Detected
2) NA: Not Applicable
3) btoc: Below Top of Casing
4) A passive skimmer was installed in USTG480-MW07 in March 2020
5) A passive skimmer was installed in USTG480-MW13 and USTG480-MW20 in August 2020
6) * Product not detected during gauging, but recovered with skimmer
Monitoring Well
Identification
Depth to Water
(feet btoc)
Depth to Product
(feet btoc)
Total Product Thickness
(feet)
DAVE~ORT
~~E~
Monitoring Well Gauging SheetProject Name: TC-341Date of Gauging Event: 7/7/2021Gauging Conducted by:MO
USTTC341-MW01 5.94 ND NA
USTTC341-IW01 7.91 ND NA
USTTC341-IW04 7.23 ND NA
USTTC341-IW05 7.28 ND NA
USTTC341-IW06 7.70 7.42 0.28
USTG480-MW03 7.37 ND NA
USTG480-MW04R 7.49 ND NA
USTG480-MW06 7.63 ND NA
USTG480-MW07 6.51 ND NA
USTG480-MW08 8.91 7.91 1.00
USTG480-MW13 7.54 ND NA
USTG480-MW16 6.08 ND NA
USTG480-MW17 5.28 ND NA
USTG480-MW18 7.26 ND NA
USTG480-MW20 6.87 6.85 0.02
USTG480-MW23 5.84 ND NA
USTG480-MW26 4.28 ND NA
USTG480-MW28 6.41 ND NA
USTG480-MW29 4.43 ND NA
USTG480-MW30 3.92 ND NA
USTG480-MW31 7.53 ND NA
USTG480-MW32 7.31 ND NA
USTTC341-MW18 6.92 ND NA
IR35-MW67AR 7.69 ND NA
Total Product Recovered (Gal)0.35
Notes: 1) ND: Not Detected
2) NA: Not Applicable
3) btoc: Below Top of Casing
4) A passive skimmer was installed in USTG480-MW07 in March 2020 5) A passive skimmer was installed in USTG480-MW13 and USTG480-MW20 in August 2020 6) * Product not detected during gauging, but recovered with skimmer
Monitoring Well
Identification
Depth to Water (feet
btoc)Depth to Product (feet btoc)Total Product Thickness (feet)
DAVEN>ORT
~~E~
Monitoring Well Gauging SheetProject Name: TC-341Project Number: Date of Gauging Event: 8/16/2021Gauging Conducted by:Mo
USTTC341-MW01 4.25 ND NA 0.00
USTTC341-IW01 7.60 ND NA 0.00
USTTC341-IW04 6.80 ND NA 0.00
USTTC341-IW05 6.87 ND NA 0.00
USTTC341-IW06 7.43 7 0.43 6.00
USTG480-MW03 7.95 ND NA 0.00
USTG480-MW04R 7.10 ND NA 0.00
USTG480-MW06 7.2 ND NA 0.00
USTG480-MW07 5.83 ND NA 0.25
USTG480-MW08 7.43 ND NA 0.00
USTG480-MW13 7.28 ND NA 0.25
USTG480-MW16 5.71 ND NA 0.00
USTG480-MW17 4.85 ND NA 0.00
USTG480-MW18 6.79 ND NA 0.00
USTG480-MW20 6.80 ND NA 0.00
USTG480-MW23 5.37 ND NA 0.00
USTG480-MW26 3.90 ND NA 0.00
USTG480-MW28 5.58 ND NA 0.00
USTG480-MW29 4.05 ND NA 0.00
USTG480-MW30 3.64 ND NA 0.00
USTG480-MW31 7.15 ND NA 0.00
USTG480-MW32 7.9 ND NA 0.00
USTTC341-MW18 6.35 ND NA 0.00
IR35-MW67AR 7.29 ND NA 0.00
Total Product Recovered (oz)6.5
Notes: 1) ND: Not Detected Total Product Recovered (gal)0.05
2) NA: Not Applicable
3) btoc: Below Top of Casing
=Passive Skimmer Installed
Monitoring Well
Identification
Depth to Water (feet
btoc)
Depth to Product
(feet btoc)Total Product Thickness (feet)Total Product
Removed (ounces)
DAVEN>ORT
;t;{~E~
Monitoring Well Gauging SheetProject Name: TC-341Project Number: Date of Gauging Event: 9/1/2021Gauging Conducted by:Lh
USTTC341-MW01 4.31 ND NA 0.00
USTTC341-IW01 4.94 ND NA 0.00
USTTC341-IW04 7.35 ND NA 0.00
USTTC341-IW05 7.63 ND NA 0.00
USTTC341-IW06 7.69 7.43 0.26 7.00
USTG480-MW03 7.49 ND NA 0.00
USTG480-MW04R 7.44 ND NA 0.00
USTG480-MW06 7.31 ND NA 0.00
USTG480-MW07 6.19 ND NA 0.50
USTG480-MW08 7.91 ND NA 0.00
USTG480-MW13 7.78 ND NA 0.00
USTG480-MW16 6.20 ND NA 0.00
USTG480-MW17 5.21 ND NA 0.00
USTG480-MW18 7.27 ND NA 0.00
USTG480-MW20 7.12 ND NA 0.00
USTG480-MW23 5.91 ND NA 0.00
USTG480-MW26 4.15 ND NA 0.00
USTG480-MW28 5.98 ND NA 0.00
USTG480-MW29 4.38 ND NA 0.00
USTG480-MW30 3.98 ND NA 0.00
USTG480-MW31 7.62 ND NA 0.00
USTG480-MW32 7.44 ND NA 0.00
USTTC341-MW18 6.55 ND NA 0.00
IR35-MW67AR 7.78 ND NA 0.00
Total Product Recovered (oz)7.5
Notes: 1) ND: Not Detected Total Product Recovered (gal)0.06
2) NA: Not Applicable
3) btoc: Below Top of Casing
=Passive Skimmer Installed
Monitoring Well
Identification
Depth to Water (feet
btoc)
Depth to Product
(feet btoc)Total Product Thickness (feet)Total Product
Removed (ounces)
DAVEN>ORT
;t;{~E~
Monitoring Well Gauging SheetProject Name: TC-341Project Number: Date of Gauging Event: 10/5/2021Gauging Conducted by:Mo
USTTC341-MW01 4.41 ND NA 0
USTTC341-IW01 7.70 ND NA 0
USTTC341-IW04 7.42 ND NA 0
USTTC341-IW05 7.66 ND NA 0
USTTC341-IW06 8.00 7.76 0.24 8
USTG480-MW03 7.58 ND NA 0
USTG480-MW04R 7.97 ND NA 0
USTG480-MW06 7.38 ND NA 0
USTG480-MW07 5.45 ND NA 0.5
USTG480-MW08 7.23 ND NA 0
USTG480-MW13 7.62 7.57 0.05 16
USTG480-MW16 6.19 ND NA 0
USTG480-MW17 6.42 ND NA 0
USTG480-MW18 7.76 ND NA 0
USTG480-MW20 7.82 ND NA 13.00
USTG480-MW23 6.44 ND NA 0
USTG480-MW26 4.10 ND NA 0
USTG480-MW28 4.83 ND NA 0
USTG480-MW29 3.75 ND NA 0
USTG480-MW30 3.94 ND NA 0
USTG480-MW31 7.74 ND NA 0
USTG480-MW32 7.48 ND NA 0
USTTC341-MW18 6.00 ND NA 0
IR35-MW67AR 8.02 ND NA 0
Total Product Recovered (oz)37.5
Notes: 1) ND: Not Detected Total Product Recovered (gal)0.29
2) NA: Not Applicable
3) btoc: Below Top of Casing
=Passive Skimmer Installed
Monitoring Well
Identification
Depth to Water (feet
btoc)
Depth to Product
(feet btoc)Total Product Thickness (feet)Total Product
Removed (ounces)
DAVEN>ORT
;t;{~E~
Monitoring Well Gauging SheetProject Name: TC-341Project Number: Date of Gauging Event: 11/2/2021Gauging Conducted by:LH
USTTC341-MW01 5.86 ND NA 0.00
USTTC341-IW01 7.84 ND NA 0.00
USTTC341-IW04 7.61 ND NA 0.00
USTTC341-IW05 7.87 ND NA 0.00
USTTC341-IW06 7.46 ND NA 0.00
USTG480-MW03 7.74 ND NA 0.00
USTG480-MW04R 8.20 ND NA 0.00
USTG480-MW06 8.21 8.00 0.21 0.00
USTG480-MW07 5.82 ND NA 0.00
USTG480-MW08 7.39 7.34 0.05 5.00
USTG480-MW13 7.83 ND NA 6.00
USTG480-MW16 6.30 ND NA 0.00
USTG480-MW17 8.36 ND NA 0.00
USTG480-MW18 5.62 ND NA 0.00
USTG480-MW20 10.45 ND NA 2.00
USTG480-MW23 6.82 ND NA 0.00
USTG480-MW26 4.27 ND NA 0.00
USTG480-MW28 5.05 ND NA 0.00
USTG480-MW29 3.97 ND NA 0.00
USTG480-MW30 4.11 ND NA 0.00
USTG480-MW31 7.87 ND NA 0.00
USTG480-MW32 7.65 ND NA 0.00
USTTC341-MW18 6.12 ND NA 0.00
IR35-MW67AR 8.17 ND NA 0.00
Total Product Recovered (oz)13.00
Notes: 1) ND: Not Detected Total Product Recovered (gal)0.10
2) NA: Not Applicable
3) btoc: Below Top of Casing
=Passive Skimmer Installed
Monitoring Well
Identification
Depth to Water (feet
btoc)
Depth to Product
(feet btoc)Total Product Thickness (feet)Total Product
Removed (ounces)
DAVEN>ORT
;t;{~E~
Monitoring Well Gauging SheetProject Name: TC-341Project Number: Date of Gauging Event: 12/3/2021Gauging Conducted by:LH
USTTC341-MW01 6.24 ND NA 0.00
USTTC341-IW01 7.98 ND NA 0.00
USTTC341-IW04 8.12 ND NA 0.00
USTTC341-IW05 7.35 ND NA 0.00
USTTC341-IW06 7.19 ND NA 0.00
USTG480-MW03 7.98 ND NA 0.00
USTG480-MW04R 9.76 ND NA 0.00
USTG480-MW06 9.33 8.00 1.33 2.00
USTG480-MW07 4.89 ND NA 0.00
USTG480-MW08 7.34 7.13 0.21 5.00
USTG480-MW13 8.44 ND NA 12.00
USTG480-MW16 7.44 ND NA 0.00
USTG480-MW17 8.33 ND NA 0.00
USTG480-MW18 7.66 ND NA 0.00
USTG480-MW20 11.05 ND NA 0.00
USTG480-MW23 6.98 ND NA 0.00
USTG480-MW26 5.23 ND NA 0.00
USTG480-MW28 5.59 ND NA 0.00
USTG480-MW29 4.19 ND NA 0.00
USTG480-MW30 5.32 ND NA 0.00
USTG480-MW31 8.46 ND NA 0.00
USTG480-MW32 7.26 ND NA 0.00
USTTC341-MW18 6.81 ND NA 0.00
IR35-MW67AR 8.49 ND NA 0.00
Total Product Recovered (oz)19.00
Notes: 1) ND: Not Detected Total Product Recovered (gal)0.15
2) NA: Not Applicable
3) btoc: Below Top of Casing
=Passive Skimmer Installed
Monitoring Well
Identification
Depth to Water (feet
btoc)
Depth to Product
(feet btoc)Total Product Thickness (feet)Total Product
Removed (ounces)
DAVEN>ORT
;t;{~E~
Monitoring Well Gauging Sheet
Project Name: TC-341
Project Number: 221102
Date of Gauging Event: 1/12/2022
Gauging Conducted by:SY
USTTC341-MW01 6.31 ND NA
USTTC341-IW01 8.12 ND NA
USTTC341-IW04 8.21 ND NA
USTTC341-IW05 7.46 ND NA
USTTC341-IW06 7.28 ND NA
USTG480-MW03 8.07 ND NA
USTG480-MW04R 9.81 ND NA
USTG480-MW06 9.38 ND NA
USTG480-MW07 5.02 ND NA 3
USTG480-MW08 7.34 ND NA 3
USTG480-MW13 8.52 ND NA 2
USTG480-MW16 7.53 ND NA
USTG480-MW17 8.44 ND NA
USTG480-MW18 7.71 ND NA
USTG480-MW20 11.21 ND NA 2
USTG480-MW23 7.08 ND NA
USTG480-MW26 5.29 ND NA
USTG480-MW28 5.71 ND NA
USTG480-MW29 4.28 ND NA
USTG480-MW30 5.44 ND NA
USTG480-MW31 8.51 ND NA
USTG480-MW32 7.32 ND NA
USTTC341-MW18 6.89 ND NA
IR35-MW67AR 8.57 ND NA
Total Product Recovered
(oz)10
Notes: 1) ND: Not Detected
Total Product Recovered
(gal)0.08
2) NA: Not Applicable
3) btoc: Below Top of Casing
=Passive Skimmer Installed
Monitoring Well
Identification
Depth to Water (feet
btoc)
Depth to Product (feet
btoc)
Total Product Thickness
(feet)
Total Product Removed
(ounces)
Cherokee Nation 1s
Monitoring Well Gauging SheetProject Name: TC-341Project Number: 221102Date of Gauging Event: 2/3/2022Gauging Conducted by:SY
USTTC341-MW01 7.67 ND NA
USTTC341-IW01 8.15 ND NA
USTTC341-IW04 7.49 ND NA
USTTC341-IW05 7.53 ND NA
USTTC341-IW06 7.42 ND NA
USTG480-MW03 7.66 ND NA
USTG480-MW04R 7.04 ND NA
USTG480-MW06 7.31 ND NA
USTG480-MW07 5.98 ND NA 1
USTG480-MW08 7.74 7.64 0.10 2
USTG480-MW13 7.90 ND NA
USTG480-MW16 5.75 ND NA
USTG480-MW17 5.45 ND NA
USTG480-MW18 7.76 ND NA
USTG480-MW20 8.13 ND NA 4
USTG480-MW23 7.65 ND NA
USTG480-MW26 4.55 ND NA
USTG480-MW28 4.02 ND NA
USTG480-MW29 3.78 ND NA
USTG480-MW30 3.75 ND NA
USTG480-MW31 7.85 ND NA
USTG480-MW32 7.47 ND NA
USTTC341-MW18 7.76 ND NA
IR35-MW67AR 8.00 ND NA
Total Product
Recovered 7
Notes: 1) ND: Not Detected Total Product
Recovered 0.05
2) NA: Not Applicable
3) btoc: Below Top of Casing
=Passive Skimmer Installed
Monitoring Well
Identification
Depth to Water (feet
btoc)
Depth to Product (feet
btoc)
Total Product
Thickness (feet)
Total Product
Removed (ounces)
Cherokee Nation 1s
Monitoring Well Gauging SheetProject Name: TC-341Project Number: 221102Date of Gauging Event: 3/1/2022Gauging Conducted by:SY
USTTC341-MW01 7.81 ND NA
USTTC341-IW01 8.78 ND NA
USTTC341-IW04 7.67 ND NA
USTTC341-IW05 8.95 ND NA
USTTC341-IW06 8.55 ND NA
USTG480-MW03 8.7 ND NA
USTG480-MW04R 8.19 ND NA
USTG480-MW06 7.4 ND NA
USTG480-MW07 7.15 ND NA 6
USTG480-MW08 8.77 8.55 0.22 3
USTG480-MW13 8.68 ND NA 4
USTG480-MW16 5.78 ND NA
USTG480-MW17 5.51 ND NA
USTG480-MW18 7.81 ND NA
USTG480-MW20 7.95 ND NA 6
USTG480-MW23 6.51 ND NA
USTG480-MW26 4.18 ND NA
USTG480-MW28 6.25 ND NA
USTG480-MW29 4.01 ND NA
USTG480-MW30 4.22 ND NA
USTG480-MW31 8.32 ND NA
USTG480-MW32 8.09 ND NA
USTTC341-MW18 7.95 ND NA
IR35-MW67AR 8.41 ND NA
Total Product
Recovered (oz)19
Notes: 1) ND: Not Detected Total Product
Recovered (gal)0.15
2) NA: Not Applicable
3) btoc: Below Top of Casing
=Passive Skimmer Installed
Monitoring Well
Identification
Depth to Water (feet
btoc)
Depth to Product (feet
btoc)
Total Product
Thickness (feet)
Total Product
Removed (ounces)
Cherokee Nation 1s
Monitoring Well Gauging SheetProject Name: TC-341Project Number: 221102Date of Gauging Event: 4/4/2022Gauging Conducted by:SY
USTTC341-MW01 7.60 ND NA
USTTC341-IW01 8.17 ND NA
USTTC341-IW04 6.95 ND NA
USTTC341-IW05 7.64 ND NA
USTTC341-IW06 7.35 ND NA
USTG480-MW03 7.48 ND NA
USTG480-MW04R 7.21 ND NA
USTG480-MW06 7.22 ND NA
USTG480-MW07 6.88 ND NA
USTG480-MW08 8.55 8.42 0.13 1
USTG480-MW13 8.53 ND NA
USTG480-MW16 5.98 ND NA
USTG480-MW17 5.71 ND NA
USTG480-MW18 7.75 ND NA
USTG480-MW20 7.80 7.68 0.12 1
USTG480-MW23 6.49 ND NA
USTG480-MW26 3.88 ND NA
USTG480-MW28 6.44 ND NA
USTG480-MW29 4.03 ND NA
USTG480-MW30 4.31 ND NA
USTG480-MW31 8.01 ND NA
USTG480-MW32 7.69 ND NA
USTTC341-MW18 8.09 ND NA
IR35-MW67AR 7.95 ND NA
Total Product
Recovered (oz)2
Notes: 1) ND: Not Detected Total Product
Recovered (gal)0.02
2) NA: Not Applicable
3) btoc: Below Top of Casing
=Passive Skimmer Installed
Monitoring Well
Identification
Depth to Water (feet
btoc)
Depth to Product (feet
btoc)
Total Product
Thickness (feet)
Total Product
Removed (ounces)
Cherokee Nation 1s
Monitoring Well Gauging SheetProject Name: TC-341Project Number: 221102Date of Gauging Event: 5/9/2022Gauging Conducted by:SY
USTTC341-MW01 8.07 ND NA
USTTC341-IW01 8.95 ND NA
USTTC341-IW04 7.47 ND NA
USTTC341-IW05 7.29 ND NA
USTTC341-IW06 7.55 ND NA
USTG480-MW03 7.76 ND NA
USTG480-MW04R 7.85 ND NA
USTG480-MW06 7.43 ND NA
USTG480-MW07 6.49 ND NA
USTG480-MW08 8.83 ND NA 1
USTG480-MW13 8.74 ND NA
USTG480-MW16 5.86 ND NA
USTG480-MW17 5.60 ND NA
USTG480-MW18 7.84 ND NA
USTG480-MW20 7.64 7.51 0.13 2
USTG480-MW23 6.61 ND NA
USTG480-MW26 3.71 ND NA
USTG480-MW28 6.32 ND NA
USTG480-MW29 4.11 ND NA
USTG480-MW30 4.29 ND NA
USTG480-MW31 8.09 ND NA
USTG480-MW32 7.79 ND NA
USTTC341-MW18 8.03 ND NA
IR35-MW67AR 7.91 ND NA
Total Product
Recovered (oz)3
Notes: 1) ND: Not Detected Total Product
Recovered (gal)0.02
2) NA: Not Applicable
3) btoc: Below Top of Casing
=Passive Skimmer Installed
Monitoring Well
Identification
Depth to Water (feet
btoc)
Depth to Product (feet
btoc)
Total Product
Thickness (feet)
Total Product
Removed (ounces)
Cherokee Nation 1s
Monitoring Well Gauging Sheet
Project Name: TC-341
Project Number: 221102
Date of Gauging Event: 6/15/2022
Gauging Conducted by:SY
USTTC341-MW01 6.37 ND NA
USTTC341-IW01 8.19 ND NA
USTTC341-IW04 8.25 ND NA
USTTC341-IW05 7.51 ND NA
USTTC341-IW06 7.32 ND NA
USTG480-MW03 8.01 ND NA
USTG480-MW04R 9.74 ND NA
USTG480-MW06 9.41 ND NA
USTG480-MW07 5.09 ND NA 2
USTG480-MW08 7.38 ND NA 3
USTG480-MW13 8.59 ND NA 2
USTG480-MW16 7.61 ND NA
USTG480-MW17 8.48 ND NA
USTG480-MW18 7.80 ND NA
USTG480-MW20 11.27 ND NA 2
USTG480-MW23 7.14 ND NA
USTG480-MW26 5.23 ND NA
USTG480-MW28 5.74 ND NA
USTG480-MW29 4.31 ND NA
USTG480-MW30 5.41 ND NA
USTG480-MW31 8.54 ND NA
USTG480-MW32 7.29 ND NA
USTTC341-MW18 6.81 ND NA
IR35-MW67AR 8.53 ND NA
Total Product Recovered
(oz)9
Notes: 1) ND: Not Detected
Total Product Recovered
(gal)0.07
2) NA: Not Applicable
3) btoc: Below Top of Casing
=Passive Skimmer Installed
Monitoring Well
Identification
Depth to Water (feet
btoc)
Depth to Product (feet
btoc)
Total Product Thickness
(feet)
Total Product Removed
(ounces)
Cherokee Nation 1s
2022 Annual Monitoring Report – TC-341
MCAS New River, NC

APPENDIX B

Free-Phase Product Thickness vs. Time Charts
(.'\ (HEROKEENATION™ ~ 3 S-Support, Service & Solutions
* Note: charts have been revised to show recent/relevant data.
0
0.1
0.2
0.3
0.4
0.5
0.6
0.7
Free-phase Product Thickness (ft)Gauging Date
USTTC341-IW06
Product
Thickness
0.00
0.20
0.40
0.60
0.80
1.00
1.20
1.40
Free-phase Product Thickness (ft)Gauging Date
USTG480-MW06
Product
Thickness
0
0.1
0.2
0.3
0.4
0.5
0.6
Free-phase Product Thickness (ft)Gauging Date
USTG480-MW07
Product
Thickness
◄ ►
..
◄ ► ~ ►
u
'◄-.
-► ◄ ►
.~ 1J ◄► .... ~ ~J ~
~ ~ ~ --·------
◄ ►
1111 ►
◄ 111111 I◄ • ◄ ► • ◄,
◄► ~A l...J ·L ----........ --
* Note: charts have been revised to show recent/relevant data.
0
0.5
1
1.5
2
2.5
3
3.5
Free-phase Product Thickness (ft)Gauging Date
USTG480-MW08
Product
Thickness
0
0.05
0.1
0.15
0.2
0.25
0.3
0.35
0.4
0.45
0.5
Free-phase Product Thickness (ft)Gauging Date
USTG480-MW13
Product
Thickness
0
0.2
0.4
0.6
0.8
1
1.2
1.4
1.6
Free-phase Product Thickness (ft)Gauging Date
USTG480-MW20
Product
Thickness
◄ ►
J
'
~
\ -,
{ \ ..... .....
41 .J ' "\j .A ~~,..J\. J\. ~ ---........ -~ ,..., .... ,...,.. ............... ...,....., ... .........................
* Note: charts have been revised to show recent/relevant data.
0
0.1
0.2
0.3
0.4
0.5
0.6
0.7
Free-phase Product Thickness (ft)Gauging Date
USTG480-MW26
Product…
0
0.5
1
1.5
2
2.5
Free-phase Product Thickness (ft)Gauging Date
USTG480-MW28
Product…
0.00
0.20
0.40
0.60
0.80
1.00
1.20
Free-phase Product Thickness (ft)Gauging Date
USTTC341-MW01
Product
Thickness
◄ ► ◄ ►
.....
~A ~ ..........................................................................
~ ~ ............ --~ ~ --~ .............. -
2022 Annual Monitoring Report – TC-341
MCAS New River, NC

APPENDIX C

2022 Groundwater Laboratory Analytical Reports
(.'\ (HEROKEENATION™ ~ 3 S-Support, Service & Solutions
ANALYTICAL REPORT
August 08, 2022
Revised Report
Cherokee Nation 3S
Sample Delivery Group:L1516722
Samples Received:07/20/2022
Project Number:221102
Description:TC-341
Site:TC-341
Report To:Kevin DeFosset
10838 E. Marshall St.
Suite 240
Tulsa, OK 74116
Entire Report Reviewed By:
August 08, 2022
[Preliminary Report]
Heather J Wagner
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 15:39 1 of 65
August 08, 2022
Heather J Wagner
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 16:01 1 of 65
p eAnalytical "
I _J
□ □ □ □ □ □ □ □
TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 6
Sr: Sample Results 7
USTG480-MW12 L1516722-01 7
USTTC341-MW01 L1516722-02 10
USTG480-MW11 L1516722-03 13
USTTC341-MW05 L1516722-04 16
USTG480-MW27 L1516722-05 19
USTTC341-MW14R L1516722-06 22
USTG480-MW02 L1516722-07 25
USTTC341-MW08 L1516722-08 28
USTG480-MW25 L1516722-09 31
USTTC341-MW17 L1516722-10 34
USTTC341-MW13 L1516722-11 37
USTG480-MW06 L1516722-12 40
USTG480-MW23 L1516722-13 43
Qc: Quality Control Summary 46
Volatile Petroleum Hydrocarbons by Method MADEPV 46
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 50
TPH by Method MADEPE 55
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 57
Gl: Glossary of Terms 61
Al: Accreditations & Locations 62
Sc: Sample Chain of Custody 63
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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□
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
USTG480-MW12 L1516722-01 GW Richardson 07/18/22 09:30 07/20/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Petroleum Hydrocarbons by Method MADEPV WG1899531 1 07/23/22 19:34 07/23/22 19:34 ADM Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1899800 1 07/23/22 12:48 07/23/22 12:48 TJJ Mt. Juliet, TN
TPH by Method MADEPE WG1902170 1 07/27/22 18:04 07/29/22 18:13 DMG Mt. Juliet, TN
TPH by Method MADEPE WG1902170 1 07/27/22 18:04 07/29/22 20:55 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1899773 1 07/22/22 16:28 07/23/22 14:06 ADF Mt. Juliet, TN
Collected by Collected date/time Received date/time
USTTC341-MW01 L1516722-02 GW Richardson 07/18/22 09:40 07/20/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Petroleum Hydrocarbons by Method MADEPV WG1899531 1 07/23/22 20:06 07/23/22 20:06 ADM Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1899800 1 07/23/22 13:09 07/23/22 13:09 TJJ Mt. Juliet, TN
TPH by Method MADEPE WG1902170 1 07/27/22 18:04 07/29/22 18:36 DMG Mt. Juliet, TN
TPH by Method MADEPE WG1902170 1 07/27/22 18:04 07/29/22 20:32 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1899773 1 07/22/22 16:28 07/27/22 18:08 ADF Mt. Juliet, TN
Collected by Collected date/time Received date/time
USTG480-MW11 L1516722-03 GW Richardson 07/18/22 10:00 07/20/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Petroleum Hydrocarbons by Method MADEPV WG1899531 1 07/23/22 22:17 07/23/22 22:17 ADM Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1899800 1 07/23/22 13:29 07/23/22 13:29 TJJ Mt. Juliet, TN
TPH by Method MADEPE WG1902170 1 07/27/22 18:04 07/29/22 18:59 DMG Mt. Juliet, TN
TPH by Method MADEPE WG1902170 1 07/27/22 18:04 07/29/22 20:09 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1899773 1.11 07/22/22 16:28 07/23/22 20:00 ADF Mt. Juliet, TN
Collected by Collected date/time Received date/time
USTTC341-MW05 L1516722-04 GW Richardson 07/18/22 10:45 07/20/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Petroleum Hydrocarbons by Method MADEPV WG1899531 1 07/23/22 22:49 07/23/22 22:49 ADM Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1899800 1 07/23/22 13:49 07/23/22 13:49 TJJ Mt. Juliet, TN
TPH by Method MADEPE WG1902170 1 07/27/22 18:04 07/29/22 19:23 DMG Mt. Juliet, TN
TPH by Method MADEPE WG1902170 1 07/27/22 18:04 07/29/22 19:46 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1899773 1 07/22/22 16:28 07/23/22 13:44 ADF Mt. Juliet, TN
Collected by Collected date/time Received date/time
USTG480-MW27 L1516722-05 GW Richardson 07/18/22 10:52 07/20/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Petroleum Hydrocarbons by Method MADEPV WG1899531 1 07/23/22 23:22 07/23/22 23:22 ADM Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1899800 1 07/23/22 14:09 07/23/22 14:09 TJJ Mt. Juliet, TN
TPH by Method MADEPE WG1902750 1 07/28/22 07:52 08/01/22 14:18 DMG Mt. Juliet, TN
TPH by Method MADEPE WG1902750 1 07/28/22 07:52 08/01/22 15:48 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1899773 1 07/22/22 16:28 07/27/22 18:30 ADF Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
USTTC341-MW14R L1516722-06 GW Richardson 07/18/22 11:16 07/20/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Petroleum Hydrocarbons by Method MADEPV WG1899531 10 07/24/22 02:06 07/24/22 02:06 ADM Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1899800 10 07/23/22 18:16 07/23/22 18:16 TJJ Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1901311 10 07/27/22 00:30 07/27/22 00:30 ADM Mt. Juliet, TN
TPH by Method MADEPE WG1902750 1 07/28/22 07:52 08/01/22 13:55 JDG Mt. Juliet, TN
TPH by Method MADEPE WG1902750 1 07/28/22 07:52 08/02/22 12:53 JDG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1899773 5 07/22/22 16:28 07/23/22 15:35 ADF Mt. Juliet, TN
Collected by Collected date/time Received date/time
USTG480-MW02 L1516722-07 GW Richardson 07/18/22 11:48 07/20/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Petroleum Hydrocarbons by Method MADEPV WG1901087 10 07/29/22 19:20 07/29/22 19:20 ADM Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1899800 25 07/23/22 18:36 07/23/22 18:36 TJJ Mt. Juliet, TN
TPH by Method MADEPE WG1902750 1 07/28/22 07:52 08/01/22 13:33 DMG Mt. Juliet, TN
TPH by Method MADEPE WG1902750 1 07/28/22 07:52 08/01/22 16:32 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1899773 5 07/22/22 16:28 07/23/22 14:51 ADF Mt. Juliet, TN
Collected by Collected date/time Received date/time
USTTC341-MW08 L1516722-08 GW Richardson 07/18/22 12:05 07/20/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Petroleum Hydrocarbons by Method MADEPV WG1899531 1 07/23/22 23:55 07/23/22 23:55 ADM Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1899800 1 07/23/22 14:30 07/23/22 14:30 TJJ Mt. Juliet, TN
TPH by Method MADEPE WG1902750 1 07/28/22 07:52 08/01/22 13:11 DMG Mt. Juliet, TN
TPH by Method MADEPE WG1902750 1 07/28/22 07:52 08/01/22 16:55 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1899773 1 07/22/22 16:28 07/23/22 18:10 ADF Mt. Juliet, TN
Collected by Collected date/time Received date/time
USTG480-MW25 L1516722-09 GW Richardson 07/18/22 12:51 07/20/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Petroleum Hydrocarbons by Method MADEPV WG1899531 1 07/24/22 00:27 07/24/22 00:27 ADM Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1899800 1 07/23/22 14:50 07/23/22 14:50 TJJ Mt. Juliet, TN
TPH by Method MADEPE WG1902750 1 07/28/22 07:52 08/01/22 12:49 DMG Mt. Juliet, TN
TPH by Method MADEPE WG1902750 1 07/28/22 07:52 08/01/22 17:17 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1899773 1 07/22/22 16:28 07/23/22 18:54 ADF Mt. Juliet, TN
Collected by Collected date/time Received date/time
USTTC341-MW17 L1516722-10 GW Richardson 07/18/22 12:52 07/20/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Petroleum Hydrocarbons by Method MADEPV WG1899531 1 07/24/22 01:00 07/24/22 01:00 ADM Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1899800 1 07/23/22 15:11 07/23/22 15:11 TJJ Mt. Juliet, TN
TPH by Method MADEPE WG1902750 1 07/28/22 07:52 08/01/22 12:27 DMG Mt. Juliet, TN
TPH by Method MADEPE WG1902750 1 07/28/22 07:52 08/01/22 17:39 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1899773 1.11 07/22/22 16:28 07/23/22 13:22 ADF Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
USTTC341-MW13 L1516722-11 GW Richardson 07/18/22 13:25 07/20/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Petroleum Hydrocarbons by Method MADEPV WG1899531 1 07/24/22 01:33 07/24/22 01:33 ADM Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1899800 1 07/23/22 15:32 07/23/22 15:32 TJJ Mt. Juliet, TN
TPH by Method MADEPE WG1902750 1 07/28/22 07:52 08/01/22 12:04 DMG Mt. Juliet, TN
TPH by Method MADEPE WG1902750 1 07/28/22 07:52 08/01/22 18:01 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1899773 1 07/22/22 16:28 07/23/22 18:32 ADF Mt. Juliet, TN
Collected by Collected date/time Received date/time
USTG480-MW06 L1516722-12 GW Richardson 07/18/22 14:02 07/20/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Petroleum Hydrocarbons by Method MADEPV WG1903201 1 07/31/22 22:23 07/31/22 22:23 DWR Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1899800 25 07/23/22 18:57 07/23/22 18:57 TJJ Mt. Juliet, TN
TPH by Method MADEPE WG1902750 1 07/28/22 07:52 08/01/22 11:42 DMG Mt. Juliet, TN
TPH by Method MADEPE WG1902750 1 07/28/22 07:52 08/01/22 18:24 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1899773 1 07/22/22 16:28 07/23/22 19:16 ADF Mt. Juliet, TN
Collected by Collected date/time Received date/time
USTG480-MW23 L1516722-13 GW Richardson 07/18/22 14:04 07/20/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Petroleum Hydrocarbons by Method MADEPV WG1902102 10 07/30/22 05:09 07/30/22 05:09 ADM Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1899800 10 07/23/22 19:17 07/23/22 19:17 TJJ Mt. Juliet, TN
TPH by Method MADEPE WG1902750 1 07/28/22 07:52 08/01/22 11:20 DMG Mt. Juliet, TN
TPH by Method MADEPE WG1902750 1 07/28/22 07:52 08/01/22 18:46 DMG Mt. Juliet, TN
TPH by Method MADEPE WG1902750 10 07/28/22 07:52 08/03/22 08:15 JDG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1899773 1 07/22/22 16:28 07/23/22 19:38 ADF Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Heather J Wagner
Project Manager
Report Revision History
Level II Report - Version 1: 08/03/22 15:52
Project Narrative
Due to multiple preparation procedures, calculated analytes are not reported in the quality control samples for EPH and VPH
Methods.

Revised Report: Revised to include 1-methylnaphthalene and 2-methylnaphthalene under method 625.1. This report replaces
the report issued 8/3/2022.
Method 625.1: Samples in WG1899773 are reporting with failures in the LCS against DOD limits. Recoveries are within laboratory
historical limits. Samples in WG1901744 are reporting with multiple marginally low failures in the LCS against our historical limits
and several more marginal failures against DOD/625.1 specific limits. Re-extraction is not a viable option as samples are now past
holding time.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Heather J Wagner
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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□ □ □
□ □ □ □ □
SAMPLE RESULTS - 01
L1516722
USTG480-MW12
Collected date/time: 07/18/22 09:30
Volatile Petroleum Hydrocarbons by Method MADEPV
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics C5-C8 ALI
UNADJ 67.0 U 33.3 67.0 100 1 07/23/2022 19:34 WG1899531
Unadjusted C9-C12 Aliphatics C9-C12 ALI
UNADJ 62.2 J 33.3 67.0 134 1 07/23/2022 19:34 WG1899531
Unadjusted C9-C10 Aromatics C9-C10 ARO
UNADJ 67.0 U 33.3 67.0 100 1 07/23/2022 19:34 WG1899531
Total VPH VPH 150 U 66.7 150 300 1 07/23/2022 19:34 WG1899531
(S) 2,5-Dibromotoluene(FID)615-59-8 103 70.0-130 07/23/2022 19:34 WG1899531
(S) 2,5-Dibromotoluene(PID)615-59-8 102 70.0-130 07/23/2022 19:34 WG1899531
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acetone 67-64-1 25.0 U 11.3 25.0 50.0 1 07/23/2022 12:48 WG1899800
Acrolein 107-02-8 25.0 U 2.54 25.0 50.0 1 07/23/2022 12:48 WG1899800
Acrylonitrile 107-13-1 5.00 U 0.671 5.00 10.0 1 07/23/2022 12:48 WG1899800
Benzene 71-43-2 0.500 U 0.0941 0.500 1.00 1 07/23/2022 12:48 WG1899800
Bromobenzene 108-86-1 0.500 C4 J4 U 0.118 0.500 1.00 1 07/23/2022 12:48 WG1899800
Bromodichloromethane 75-27-4 0.500 U 0.136 0.500 1.00 1 07/23/2022 12:48 WG1899800
Bromoform 75-25-2 0.500 U 0.129 0.500 1.00 1 07/23/2022 12:48 WG1899800
Bromomethane 74-83-9 2.00 U 0.605 2.00 5.00 1 07/23/2022 12:48 WG1899800
n-Butylbenzene 104-51-8 0.500 U 0.157 0.500 1.00 1 07/23/2022 12:48 WG1899800
sec-Butylbenzene 135-98-8 0.287 J 0.125 0.500 1.00 1 07/23/2022 12:48 WG1899800
tert-Butylbenzene 98-06-6 0.500 U 0.127 0.500 1.00 1 07/23/2022 12:48 WG1899800
Carbon tetrachloride 56-23-5 0.500 U 0.128 0.500 1.00 1 07/23/2022 12:48 WG1899800
Chlorobenzene 108-90-7 0.500 U 0.116 0.500 1.00 1 07/23/2022 12:48 WG1899800
Chlorodibromomethane 124-48-1 0.500 U 0.140 0.500 1.00 1 07/23/2022 12:48 WG1899800
Chloroethane 75-00-3 2.00 U 0.192 2.00 5.00 1 07/23/2022 12:48 WG1899800
Chloroform 67-66-3 2.00 U 0.111 2.00 5.00 1 07/23/2022 12:48 WG1899800
Chloromethane 74-87-3 2.00 U 0.960 2.00 4.00 1 07/23/2022 12:48 WG1899800
2-Chlorotoluene 95-49-8 0.500 U 0.106 0.500 1.00 1 07/23/2022 12:48 WG1899800
4-Chlorotoluene 106-43-4 0.500 U 0.114 0.500 1.00 1 07/23/2022 12:48 WG1899800
1,2-Dibromo-3-Chloropropane 96-12-8 2.00 U 0.276 2.00 5.00 1 07/23/2022 12:48 WG1899800
1,2-Dibromoethane 106-93-4 0.500 U 0.126 0.500 1.00 1 07/23/2022 12:48 WG1899800
Dibromomethane 74-95-3 0.500 U 0.122 0.500 1.00 1 07/23/2022 12:48 WG1899800
1,2-Dichlorobenzene 95-50-1 0.500 U 0.107 0.500 1.00 1 07/23/2022 12:48 WG1899800
1,3-Dichlorobenzene 541-73-1 0.500 U 0.110 0.500 1.00 1 07/23/2022 12:48 WG1899800
1,4-Dichlorobenzene 106-46-7 0.500 U 0.120 0.500 1.00 1 07/23/2022 12:48 WG1899800
Dichlorodifluoromethane 75-71-8 2.00 U 0.374 2.00 5.00 1 07/23/2022 12:48 WG1899800
1,1-Dichloroethane 75-34-3 0.500 U 0.100 0.500 1.00 1 07/23/2022 12:48 WG1899800
1,2-Dichloroethane 107-06-2 0.500 U 0.0819 0.500 1.00 1 07/23/2022 12:48 WG1899800
1,1-Dichloroethene 75-35-4 0.500 U 0.188 0.500 1.00 1 07/23/2022 12:48 WG1899800
cis-1,2-Dichloroethene 156-59-2 0.500 U 0.126 0.500 1.00 1 07/23/2022 12:48 WG1899800
trans-1,2-Dichloroethene 156-60-5 0.500 U 0.149 0.500 1.00 1 07/23/2022 12:48 WG1899800
1,2-Dichloropropane 78-87-5 0.500 U 0.149 0.500 1.00 1 07/23/2022 12:48 WG1899800
1,1-Dichloropropene 563-58-6 0.500 U 0.142 0.500 1.00 1 07/23/2022 12:48 WG1899800
1,3-Dichloropropane 142-28-9 0.500 U 0.110 0.500 1.00 1 07/23/2022 12:48 WG1899800
2,2-Dichloropropane 594-20-7 0.500 U 0.161 0.500 1.00 1 07/23/2022 12:48 WG1899800
Di-isopropyl ether 108-20-3 0.500 U 0.105 0.500 1.00 1 07/23/2022 12:48 WG1899800
Ethylbenzene 100-41-4 0.500 U 0.137 0.500 1.00 1 07/23/2022 12:48 WG1899800
Hexachloro-1,3-butadiene 87-68-3 0.750 U 0.337 0.750 1.50 1 07/23/2022 12:48 WG1899800
Isopropylbenzene 98-82-8 0.288 J 0.105 0.500 1.00 1 07/23/2022 12:48 WG1899800
p-Isopropyltoluene 99-87-6 0.500 U 0.120 0.500 1.00 1 07/23/2022 12:48 WG1899800
2-Butanone (MEK)78-93-3 5.00 U 1.19 5.00 10.0 1 07/23/2022 12:48 WG1899800
Methylene Chloride 75-09-2 2.00 U 0.430 2.00 5.00 1 07/23/2022 12:48 WG1899800
4-Methyl-2-pentanone (MIBK)108-10-1 5.00 U 0.478 5.00 10.0 1 07/23/2022 12:48 WG1899800
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 15:39 7 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 16:01 7 of 65
--------------=---□
□ □ □
==============~~~~~=----□ □ □ □
SAMPLE RESULTS - 01
L1516722
USTG480-MW12
Collected date/time: 07/18/22 09:30
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Methyl tert-butyl ether 1634-04-4 0.500 U 0.101 0.500 1.00 1 07/23/2022 12:48 WG1899800
Naphthalene 91-20-3 2.00 U 1.00 2.00 5.00 1 07/23/2022 12:48 WG1899800
n-Propylbenzene 103-65-1 0.500 C4 J4 U 0.0993 0.500 1.00 1 07/23/2022 12:48 WG1899800
Styrene 100-42-5 0.500 U 0.118 0.500 1.00 1 07/23/2022 12:48 WG1899800
1,1,1,2-Tetrachloroethane 630-20-6 0.500 U 0.147 0.500 1.00 1 07/23/2022 12:48 WG1899800
1,1,2,2-Tetrachloroethane 79-34-5 0.500 U 0.133 0.500 1.00 1 07/23/2022 12:48 WG1899800
Tetrachloroethene 127-18-4 0.600 U 0.300 0.600 1.20 1 07/23/2022 12:48 WG1899800
Toluene 108-88-3 0.600 U 0.278 0.600 1.20 1 07/23/2022 12:48 WG1899800
1,2,3-Trichlorobenzene 87-61-6 0.500 C4 U 0.230 0.500 1.00 1 07/23/2022 12:48 WG1899800
1,2,4-Trichlorobenzene 120-82-1 1.00 U 0.481 1.00 2.00 1 07/23/2022 12:48 WG1899800
1,1,1-Trichloroethane 71-55-6 0.500 U 0.149 0.500 1.00 1 07/23/2022 12:48 WG1899800
1,1,2-Trichloroethane 79-00-5 0.500 U 0.158 0.500 1.00 1 07/23/2022 12:48 WG1899800
Trichloroethene 79-01-6 0.500 U 0.190 0.500 1.00 1 07/23/2022 12:48 WG1899800
Trichlorofluoromethane 75-69-4 2.00 U 0.160 2.00 5.00 1 07/23/2022 12:48 WG1899800
1,2,3-Trichloropropane 96-18-4 1.00 U 0.237 1.00 2.50 1 07/23/2022 12:48 WG1899800
1,2,4-Trimethylbenzene 95-63-6 1.00 U 0.322 1.00 2.00 1 07/23/2022 12:48 WG1899800
1,3,5-Trimethylbenzene 108-67-8 0.500 U 0.104 0.500 1.00 1 07/23/2022 12:48 WG1899800
Vinyl chloride 75-01-4 0.500 U 0.234 0.500 1.00 1 07/23/2022 12:48 WG1899800
o-Xylene 95-47-6 0.500 U 0.174 0.500 1.00 1 07/23/2022 12:48 WG1899800
m&p-Xylenes 1330-20-7 1.00 U 0.430 1.00 2.00 1 07/23/2022 12:48 WG1899800
(S) Toluene-d8 2037-26-5 106 89.0-112 07/23/2022 12:48 WG1899800
(S) 4-Bromofluorobenzene 460-00-4 92.0 85.0-114 07/23/2022 12:48 WG1899800
(S) 1,2-Dichloroethane-d4 17060-07-0 95.5 81.0-118 07/23/2022 12:48 WG1899800
TPH by Method MADEPE
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics C9-C18 ALI
UNADJ 67.0 U 33.3 67.0 134 1 07/29/2022 18:13 WG1902170
Unadjusted C19-C36 Aliphatics C19-C36 ALI
UNADJ 37.1 B J 33.3 67.0 134 1 07/29/2022 18:13 WG1902170
Unadjusted C11-C22 Aromatics C11-C22 ARO
UNADJ 79.8 B J 33.3 67.0 134 1 07/29/2022 20:55 WG1902170
Unadjusted Total Petroleum
Hydrocarbons TPH UNADJ 117 B J 33.3 67.0 134 1 07/29/2022 20:55 WG1902170
(S) o-Terphenyl 84-15-1 71.5 40.0-140 07/29/2022 20:55 WG1902170
(S) 1-Chloro-octadecane 3386-33-2 57.1 40.0-140 07/29/2022 18:13 WG1902170
(S) 2-Fluorobiphenyl 321-60-8 94.5 40.0-140 07/29/2022 20:55 WG1902170
(S) 2-Bromonaphthalene 580-13-2 94.1 40.0-140 07/29/2022 20:55 WG1902170
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acenaphthene 83-32-9 0.276 J J4 0.0886 0.500 1.00 1 07/23/2022 14:06 WG1899773
Acenaphthylene 208-96-8 0.500 U 0.0921 0.500 1.00 1 07/23/2022 14:06 WG1899773
Anthracene 120-12-7 0.500 J4 U 0.0804 0.500 1.00 1 07/23/2022 14:06 WG1899773
Benzidine 92-87-5 7.50 U 3.74 7.50 15.0 1 07/23/2022 14:06 WG1899773
Benzo(a)anthracene 56-55-3 0.500 U 0.199 0.500 1.00 1 07/23/2022 14:06 WG1899773
Benzo(b)fluoranthene 205-99-2 0.500 U 0.130 0.500 1.00 1 07/23/2022 14:06 WG1899773
Benzo(k)fluoranthene 207-08-9 0.500 U 0.120 0.500 1.00 1 07/23/2022 14:06 WG1899773
Benzo(g,h,i)perylene 191-24-2 0.500 U 0.121 0.500 1.00 1 07/23/2022 14:06 WG1899773
Benzo(a)pyrene 50-32-8 0.500 U 0.0381 0.500 1.00 1 07/23/2022 14:06 WG1899773
Bis(2-chlorethoxy)methane 111-91-1 5.00 J4 U 0.116 5.00 10.0 1 07/23/2022 14:06 WG1899773
Bis(2-chloroethyl)ether 111-44-4 5.00 J4 U 0.137 5.00 10.0 1 07/23/2022 14:06 WG1899773
2,2-Oxybis(1-Chloropropane)108-60-1 5.00 J4 U 0.210 5.00 10.0 1 07/23/2022 14:06 WG1899773
4-Bromophenyl-phenylether 101-55-3 5.00 U 0.0877 5.00 10.0 1 07/23/2022 14:06 WG1899773
2-Chloronaphthalene 91-58-7 0.500 U 0.0648 0.500 1.00 1 07/23/2022 14:06 WG1899773
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 15:39 8 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 16:01 8 of 65
====================----□ □ □ □
□ □ □ □
SAMPLE RESULTS - 01
L1516722
USTG480-MW12
Collected date/time: 07/18/22 09:30
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
4-Chlorophenyl-phenylether 7005-72-3 5.00 U 0.0926 5.00 10.0 1 07/23/2022 14:06 WG1899773
Chrysene 218-01-9 0.500 U 0.130 0.500 1.00 1 07/23/2022 14:06 WG1899773
Dibenz(a,h)anthracene 53-70-3 0.500 U 0.0644 0.500 1.00 1 07/23/2022 14:06 WG1899773
3,3-Dichlorobenzidine 91-94-1 5.00 U 0.212 5.00 10.0 1 07/23/2022 14:06 WG1899773
2,4-Dinitrotoluene 121-14-2 5.00 U 0.0983 5.00 10.0 1 07/23/2022 14:06 WG1899773
2,6-Dinitrotoluene 606-20-2 5.00 U 0.250 5.00 10.0 1 07/23/2022 14:06 WG1899773
Fluoranthene 206-44-0 0.500 U 0.102 0.500 1.00 1 07/23/2022 14:06 WG1899773
Fluorene 86-73-7 0.272 J 0.0844 0.500 1.00 1 07/23/2022 14:06 WG1899773
Hexachlorobenzene 118-74-1 0.500 U 0.0755 0.500 1.00 1 07/23/2022 14:06 WG1899773
Hexachloro-1,3-butadiene 87-68-3 5.00 U 0.0968 5.00 10.0 1 07/23/2022 14:06 WG1899773
Hexachlorocyclopentadiene 77-47-4 5.00 U 0.0598 5.00 10.0 1 07/23/2022 14:06 WG1899773
Hexachloroethane 67-72-1 5.00 U 0.127 5.00 10.0 1 07/23/2022 14:06 WG1899773
Indeno(1,2,3-cd)pyrene 193-39-5 0.600 U 0.279 0.600 1.20 1 07/23/2022 14:06 WG1899773
Isophorone 78-59-1 5.00 U 0.143 5.00 10.0 1 07/23/2022 14:06 WG1899773
Naphthalene 91-20-3 0.430 J J4 0.159 0.500 1.00 1 07/23/2022 14:06 WG1899773
Nitrobenzene 98-95-3 5.00 J4 U 0.297 5.00 10.0 1 07/23/2022 14:06 WG1899773
n-Nitrosodimethylamine 62-75-9 1.28 J 0.998 5.00 10.0 1 07/23/2022 14:06 WG1899773
n-Nitrosodiphenylamine 86-30-6 5.00 J4 U 2.37 5.00 10.0 1 07/23/2022 14:06 WG1899773
n-Nitrosodi-n-propylamine 621-64-7 5.00 J4 U 0.261 5.00 10.0 1 07/23/2022 14:06 WG1899773
Phenanthrene 85-01-8 0.500 J4 U 0.112 0.500 1.00 1 07/23/2022 14:06 WG1899773
Benzylbutyl phthalate 85-68-7 2.00 U 0.765 2.00 4.00 1 07/23/2022 14:06 WG1899773
Bis(2-ethylhexyl)phthalate 117-81-7 2.00 U 0.895 2.00 4.00 1 07/23/2022 14:06 WG1899773
Di-n-butyl phthalate 84-74-2 1.50 U 0.453 1.50 3.00 1 07/23/2022 14:06 WG1899773
Diethyl phthalate 84-66-2 1.50 U 0.287 1.50 3.00 1 07/23/2022 14:06 WG1899773
Dimethyl phthalate 131-11-3 1.50 U 0.260 1.50 3.00 1 07/23/2022 14:06 WG1899773
Di-n-octyl phthalate 117-84-0 2.00 U 0.932 2.00 4.00 1 07/23/2022 14:06 WG1899773
Pyrene 129-00-0 0.500 J4 U 0.107 0.500 1.00 1 07/23/2022 14:06 WG1899773
1,2,4-Trichlorobenzene 120-82-1 5.00 U 0.0698 5.00 10.0 1 07/23/2022 14:06 WG1899773
4-Chloro-3-methylphenol 59-50-7 5.00 U 0.131 5.00 10.0 1 07/23/2022 14:06 WG1899773
2-Chlorophenol 95-57-8 5.00 J4 U 0.133 5.00 10.0 1 07/23/2022 14:06 WG1899773
2,4-Dichlorophenol 120-83-2 5.00 J4 U 0.102 5.00 10.0 1 07/23/2022 14:06 WG1899773
2,4-Dimethylphenol 105-67-9 5.00 U 0.0636 5.00 10.0 1 07/23/2022 14:06 WG1899773
4,6-Dinitro-2-methylphenol 534-52-1 5.00 U 1.12 5.00 10.0 1 07/23/2022 14:06 WG1899773
2,4-Dinitrophenol 51-28-5 15.0 U 5.93 15.0 30.0 1 07/23/2022 14:06 WG1899773
2-Nitrophenol 88-75-5 5.00 J4 U 0.117 5.00 10.0 1 07/23/2022 14:06 WG1899773
4-Nitrophenol 100-02-7 5.00 U 0.143 5.00 10.0 1 07/23/2022 14:06 WG1899773
Pentachlorophenol 87-86-5 5.00 U 0.313 5.00 10.0 1 07/23/2022 14:06 WG1899773
Phenol 108-95-2 10.0 U 4.33 10.0 20.0 1 07/23/2022 14:06 WG1899773
2,4,6-Trichlorophenol 88-06-2 5.00 U 0.100 5.00 10.0 1 07/23/2022 14:06 WG1899773
1-Methylnaphthalene 90-12-0 0.816 J 0.0790 0.500 1.00 1 07/23/2022 14:06 WG1899773
2-Methylnaphthalene 91-57-6 0.128 J 0.117 0.500 1.00 1 07/23/2022 14:06 WG1899773
(S) Nitrobenzene-d5 4165-60-0 58.2 0.000 44.0-120 07/23/2022 14:06 WG1899773
(S) 2-Fluorobiphenyl 321-60-8 58.8 0.000 44.0-119 07/23/2022 14:06 WG1899773
(S) p-Terphenyl-d14 1718-51-0 57.4 0.000 50.0-134 07/23/2022 14:06 WG1899773
(S) Phenol-d5 4165-62-2 16.5 0.000 10.0-67.0 07/23/2022 14:06 WG1899773
(S) 2-Fluorophenol 367-12-4 26.1 0.000 19.0-119 07/23/2022 14:06 WG1899773
(S) 2,4,6-Tribromophenol 118-79-6 66.5 0.000 43.0-140 07/23/2022 14:06 WG1899773
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 15:39 9 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 16:01 9 of 65
====================----□ □ □ □
□ □ □ □
SAMPLE RESULTS - 02
L1516722
USTTC341-MW01
Collected date/time: 07/18/22 09:40
Volatile Petroleum Hydrocarbons by Method MADEPV
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics C5-C8 ALI
UNADJ 67.0 U 33.3 67.0 100 1 07/23/2022 20:06 WG1899531
Unadjusted C9-C12 Aliphatics C9-C12 ALI
UNADJ 67.8 J 33.3 67.0 134 1 07/23/2022 20:06 WG1899531
Unadjusted C9-C10 Aromatics C9-C10 ARO
UNADJ 78.2 J 33.3 67.0 100 1 07/23/2022 20:06 WG1899531
Total VPH VPH 146 J 66.7 150 300 1 07/23/2022 20:06 WG1899531
(S) 2,5-Dibromotoluene(FID)615-59-8 124 70.0-130 07/23/2022 20:06 WG1899531
(S) 2,5-Dibromotoluene(PID)615-59-8 107 70.0-130 07/23/2022 20:06 WG1899531
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acetone 67-64-1 12.1 J 11.3 25.0 50.0 1 07/23/2022 13:09 WG1899800
Acrolein 107-02-8 25.0 U 2.54 25.0 50.0 1 07/23/2022 13:09 WG1899800
Acrylonitrile 107-13-1 5.00 U 0.671 5.00 10.0 1 07/23/2022 13:09 WG1899800
Benzene 71-43-2 0.280 J 0.0941 0.500 1.00 1 07/23/2022 13:09 WG1899800
Bromobenzene 108-86-1 0.500 C4 J4 U 0.118 0.500 1.00 1 07/23/2022 13:09 WG1899800
Bromodichloromethane 75-27-4 0.500 U 0.136 0.500 1.00 1 07/23/2022 13:09 WG1899800
Bromoform 75-25-2 0.500 U 0.129 0.500 1.00 1 07/23/2022 13:09 WG1899800
Bromomethane 74-83-9 2.00 U 0.605 2.00 5.00 1 07/23/2022 13:09 WG1899800
n-Butylbenzene 104-51-8 0.500 U 0.157 0.500 1.00 1 07/23/2022 13:09 WG1899800
sec-Butylbenzene 135-98-8 0.297 J 0.125 0.500 1.00 1 07/23/2022 13:09 WG1899800
tert-Butylbenzene 98-06-6 0.158 J 0.127 0.500 1.00 1 07/23/2022 13:09 WG1899800
Carbon tetrachloride 56-23-5 0.500 U 0.128 0.500 1.00 1 07/23/2022 13:09 WG1899800
Chlorobenzene 108-90-7 0.500 U 0.116 0.500 1.00 1 07/23/2022 13:09 WG1899800
Chlorodibromomethane 124-48-1 0.500 U 0.140 0.500 1.00 1 07/23/2022 13:09 WG1899800
Chloroethane 75-00-3 2.00 U 0.192 2.00 5.00 1 07/23/2022 13:09 WG1899800
Chloroform 67-66-3 2.00 U 0.111 2.00 5.00 1 07/23/2022 13:09 WG1899800
Chloromethane 74-87-3 2.00 U 0.960 2.00 4.00 1 07/23/2022 13:09 WG1899800
2-Chlorotoluene 95-49-8 0.500 U 0.106 0.500 1.00 1 07/23/2022 13:09 WG1899800
4-Chlorotoluene 106-43-4 0.500 U 0.114 0.500 1.00 1 07/23/2022 13:09 WG1899800
1,2-Dibromo-3-Chloropropane 96-12-8 2.00 U 0.276 2.00 5.00 1 07/23/2022 13:09 WG1899800
1,2-Dibromoethane 106-93-4 0.500 U 0.126 0.500 1.00 1 07/23/2022 13:09 WG1899800
Dibromomethane 74-95-3 0.500 U 0.122 0.500 1.00 1 07/23/2022 13:09 WG1899800
1,2-Dichlorobenzene 95-50-1 0.500 U 0.107 0.500 1.00 1 07/23/2022 13:09 WG1899800
1,3-Dichlorobenzene 541-73-1 0.500 U 0.110 0.500 1.00 1 07/23/2022 13:09 WG1899800
1,4-Dichlorobenzene 106-46-7 0.500 U 0.120 0.500 1.00 1 07/23/2022 13:09 WG1899800
Dichlorodifluoromethane 75-71-8 2.00 U 0.374 2.00 5.00 1 07/23/2022 13:09 WG1899800
1,1-Dichloroethane 75-34-3 0.500 U 0.100 0.500 1.00 1 07/23/2022 13:09 WG1899800
1,2-Dichloroethane 107-06-2 0.500 U 0.0819 0.500 1.00 1 07/23/2022 13:09 WG1899800
1,1-Dichloroethene 75-35-4 0.500 U 0.188 0.500 1.00 1 07/23/2022 13:09 WG1899800
cis-1,2-Dichloroethene 156-59-2 0.500 U 0.126 0.500 1.00 1 07/23/2022 13:09 WG1899800
trans-1,2-Dichloroethene 156-60-5 0.500 U 0.149 0.500 1.00 1 07/23/2022 13:09 WG1899800
1,2-Dichloropropane 78-87-5 0.500 U 0.149 0.500 1.00 1 07/23/2022 13:09 WG1899800
1,1-Dichloropropene 563-58-6 0.500 U 0.142 0.500 1.00 1 07/23/2022 13:09 WG1899800
1,3-Dichloropropane 142-28-9 0.500 U 0.110 0.500 1.00 1 07/23/2022 13:09 WG1899800
2,2-Dichloropropane 594-20-7 0.500 U 0.161 0.500 1.00 1 07/23/2022 13:09 WG1899800
Di-isopropyl ether 108-20-3 0.500 U 0.105 0.500 1.00 1 07/23/2022 13:09 WG1899800
Ethylbenzene 100-41-4 1.10 0.137 0.500 1.00 1 07/23/2022 13:09 WG1899800
Hexachloro-1,3-butadiene 87-68-3 0.750 U 0.337 0.750 1.50 1 07/23/2022 13:09 WG1899800
Isopropylbenzene 98-82-8 1.23 0.105 0.500 1.00 1 07/23/2022 13:09 WG1899800
p-Isopropyltoluene 99-87-6 0.128 J 0.120 0.500 1.00 1 07/23/2022 13:09 WG1899800
2-Butanone (MEK)78-93-3 2.11 J 1.19 5.00 10.0 1 07/23/2022 13:09 WG1899800
Methylene Chloride 75-09-2 2.00 U 0.430 2.00 5.00 1 07/23/2022 13:09 WG1899800
4-Methyl-2-pentanone (MIBK)108-10-1 5.00 U 0.478 5.00 10.0 1 07/23/2022 13:09 WG1899800
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 15:39 10 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 16:01 10 of 65
--------------=---□
□ □ □
==============~~~~~=----□ □ □ □
SAMPLE RESULTS - 02
L1516722
USTTC341-MW01
Collected date/time: 07/18/22 09:40
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Methyl tert-butyl ether 1634-04-4 0.500 U 0.101 0.500 1.00 1 07/23/2022 13:09 WG1899800
Naphthalene 91-20-3 3.36 J 1.00 2.00 5.00 1 07/23/2022 13:09 WG1899800
n-Propylbenzene 103-65-1 1.48 C4 J4 0.0993 0.500 1.00 1 07/23/2022 13:09 WG1899800
Styrene 100-42-5 0.500 U 0.118 0.500 1.00 1 07/23/2022 13:09 WG1899800
1,1,1,2-Tetrachloroethane 630-20-6 0.500 U 0.147 0.500 1.00 1 07/23/2022 13:09 WG1899800
1,1,2,2-Tetrachloroethane 79-34-5 0.500 U 0.133 0.500 1.00 1 07/23/2022 13:09 WG1899800
Tetrachloroethene 127-18-4 0.600 U 0.300 0.600 1.20 1 07/23/2022 13:09 WG1899800
Toluene 108-88-3 0.600 U 0.278 0.600 1.20 1 07/23/2022 13:09 WG1899800
1,2,3-Trichlorobenzene 87-61-6 0.500 C4 U 0.230 0.500 1.00 1 07/23/2022 13:09 WG1899800
1,2,4-Trichlorobenzene 120-82-1 1.00 U 0.481 1.00 2.00 1 07/23/2022 13:09 WG1899800
1,1,1-Trichloroethane 71-55-6 0.500 U 0.149 0.500 1.00 1 07/23/2022 13:09 WG1899800
1,1,2-Trichloroethane 79-00-5 0.500 U 0.158 0.500 1.00 1 07/23/2022 13:09 WG1899800
Trichloroethene 79-01-6 0.500 U 0.190 0.500 1.00 1 07/23/2022 13:09 WG1899800
Trichlorofluoromethane 75-69-4 2.00 U 0.160 2.00 5.00 1 07/23/2022 13:09 WG1899800
1,2,3-Trichloropropane 96-18-4 1.00 U 0.237 1.00 2.50 1 07/23/2022 13:09 WG1899800
1,2,4-Trimethylbenzene 95-63-6 1.00 U 0.322 1.00 2.00 1 07/23/2022 13:09 WG1899800
1,3,5-Trimethylbenzene 108-67-8 0.500 U 0.104 0.500 1.00 1 07/23/2022 13:09 WG1899800
Vinyl chloride 75-01-4 0.500 U 0.234 0.500 1.00 1 07/23/2022 13:09 WG1899800
o-Xylene 95-47-6 0.500 U 0.174 0.500 1.00 1 07/23/2022 13:09 WG1899800
m&p-Xylenes 1330-20-7 1.00 U 0.430 1.00 2.00 1 07/23/2022 13:09 WG1899800
(S) Toluene-d8 2037-26-5 105 89.0-112 07/23/2022 13:09 WG1899800
(S) 4-Bromofluorobenzene 460-00-4 90.3 85.0-114 07/23/2022 13:09 WG1899800
(S) 1,2-Dichloroethane-d4 17060-07-0 95.7 81.0-118 07/23/2022 13:09 WG1899800
TPH by Method MADEPE
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics C9-C18 ALI
UNADJ 160 33.3 67.0 134 1 07/29/2022 18:36 WG1902170
Unadjusted C19-C36 Aliphatics C19-C36 ALI
UNADJ 98.0 B J 33.3 67.0 134 1 07/29/2022 18:36 WG1902170
Unadjusted C11-C22 Aromatics C11-C22 ARO
UNADJ 252 B 33.3 67.0 134 1 07/29/2022 20:32 WG1902170
Unadjusted Total Petroleum
Hydrocarbons TPH UNADJ 510 33.3 67.0 134 1 07/29/2022 20:32 WG1902170
(S) o-Terphenyl 84-15-1 64.2 40.0-140 07/29/2022 20:32 WG1902170
(S) 1-Chloro-octadecane 3386-33-2 56.3 40.0-140 07/29/2022 18:36 WG1902170
(S) 2-Fluorobiphenyl 321-60-8 78.1 40.0-140 07/29/2022 20:32 WG1902170
(S) 2-Bromonaphthalene 580-13-2 79.4 40.0-140 07/29/2022 20:32 WG1902170
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acenaphthene 83-32-9 0.423 J J4 0.0886 0.500 1.00 1 07/27/2022 18:08 WG1899773
Acenaphthylene 208-96-8 0.500 U 0.0921 0.500 1.00 1 07/27/2022 18:08 WG1899773
Anthracene 120-12-7 0.500 J4 U 0.0804 0.500 1.00 1 07/27/2022 18:08 WG1899773
Benzidine 92-87-5 7.50 U 3.74 7.50 15.0 1 07/27/2022 18:08 WG1899773
Benzo(a)anthracene 56-55-3 0.500 U 0.199 0.500 1.00 1 07/27/2022 18:08 WG1899773
Benzo(b)fluoranthene 205-99-2 0.500 U 0.130 0.500 1.00 1 07/27/2022 18:08 WG1899773
Benzo(k)fluoranthene 207-08-9 0.500 U 0.120 0.500 1.00 1 07/27/2022 18:08 WG1899773
Benzo(g,h,i)perylene 191-24-2 0.500 U 0.121 0.500 1.00 1 07/27/2022 18:08 WG1899773
Benzo(a)pyrene 50-32-8 0.500 U 0.0381 0.500 1.00 1 07/27/2022 18:08 WG1899773
Bis(2-chlorethoxy)methane 111-91-1 5.00 J4 U 0.116 5.00 10.0 1 07/27/2022 18:08 WG1899773
Bis(2-chloroethyl)ether 111-44-4 5.00 J4 U 0.137 5.00 10.0 1 07/27/2022 18:08 WG1899773
2,2-Oxybis(1-Chloropropane)108-60-1 5.00 J4 U 0.210 5.00 10.0 1 07/27/2022 18:08 WG1899773
4-Bromophenyl-phenylether 101-55-3 5.00 U 0.0877 5.00 10.0 1 07/27/2022 18:08 WG1899773
2-Chloronaphthalene 91-58-7 0.500 U 0.0648 0.500 1.00 1 07/27/2022 18:08 WG1899773
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 15:39 11 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 16:01 11 of 65
====================----□ □ □ □
□ □ □ □
SAMPLE RESULTS - 02
L1516722
USTTC341-MW01
Collected date/time: 07/18/22 09:40
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
4-Chlorophenyl-phenylether 7005-72-3 5.00 U 0.0926 5.00 10.0 1 07/27/2022 18:08 WG1899773
Chrysene 218-01-9 0.500 U 0.130 0.500 1.00 1 07/27/2022 18:08 WG1899773
Dibenz(a,h)anthracene 53-70-3 0.500 U 0.0644 0.500 1.00 1 07/27/2022 18:08 WG1899773
3,3-Dichlorobenzidine 91-94-1 5.00 U 0.212 5.00 10.0 1 07/27/2022 18:08 WG1899773
2,4-Dinitrotoluene 121-14-2 5.00 U 0.0983 5.00 10.0 1 07/27/2022 18:08 WG1899773
2,6-Dinitrotoluene 606-20-2 5.00 U 0.250 5.00 10.0 1 07/27/2022 18:08 WG1899773
Fluoranthene 206-44-0 0.500 U 0.102 0.500 1.00 1 07/27/2022 18:08 WG1899773
Fluorene 86-73-7 0.532 J 0.0844 0.500 1.00 1 07/27/2022 18:08 WG1899773
Hexachlorobenzene 118-74-1 0.500 U 0.0755 0.500 1.00 1 07/27/2022 18:08 WG1899773
Hexachloro-1,3-butadiene 87-68-3 5.00 U 0.0968 5.00 10.0 1 07/27/2022 18:08 WG1899773
Hexachlorocyclopentadiene 77-47-4 5.00 U 0.0598 5.00 10.0 1 07/27/2022 18:08 WG1899773
Hexachloroethane 67-72-1 5.00 U 0.127 5.00 10.0 1 07/27/2022 18:08 WG1899773
Indeno(1,2,3-cd)pyrene 193-39-5 0.600 U 0.279 0.600 1.20 1 07/27/2022 18:08 WG1899773
Isophorone 78-59-1 5.00 U 0.143 5.00 10.0 1 07/27/2022 18:08 WG1899773
Naphthalene 91-20-3 0.572 J J4 0.159 0.500 1.00 1 07/27/2022 18:08 WG1899773
Nitrobenzene 98-95-3 5.00 J4 U 0.297 5.00 10.0 1 07/27/2022 18:08 WG1899773
n-Nitrosodimethylamine 62-75-9 5.00 U 0.998 5.00 10.0 1 07/27/2022 18:08 WG1899773
n-Nitrosodiphenylamine 86-30-6 5.00 J4 U 2.37 5.00 10.0 1 07/27/2022 18:08 WG1899773
n-Nitrosodi-n-propylamine 621-64-7 5.00 J4 U 0.261 5.00 10.0 1 07/27/2022 18:08 WG1899773
Phenanthrene 85-01-8 0.500 J4 U 0.112 0.500 1.00 1 07/27/2022 18:08 WG1899773
Benzylbutyl phthalate 85-68-7 2.00 U 0.765 2.00 4.00 1 07/27/2022 18:08 WG1899773
Bis(2-ethylhexyl)phthalate 117-81-7 2.00 U 0.895 2.00 4.00 1 07/27/2022 18:08 WG1899773
Di-n-butyl phthalate 84-74-2 1.50 U 0.453 1.50 3.00 1 07/27/2022 18:08 WG1899773
Diethyl phthalate 84-66-2 1.50 U 0.287 1.50 3.00 1 07/27/2022 18:08 WG1899773
Dimethyl phthalate 131-11-3 1.50 U 0.260 1.50 3.00 1 07/27/2022 18:08 WG1899773
Di-n-octyl phthalate 117-84-0 2.00 U 0.932 2.00 4.00 1 07/27/2022 18:08 WG1899773
Pyrene 129-00-0 0.500 J4 U 0.107 0.500 1.00 1 07/27/2022 18:08 WG1899773
1,2,4-Trichlorobenzene 120-82-1 5.00 U 0.0698 5.00 10.0 1 07/27/2022 18:08 WG1899773
4-Chloro-3-methylphenol 59-50-7 5.00 U 0.131 5.00 10.0 1 07/27/2022 18:08 WG1899773
2-Chlorophenol 95-57-8 5.00 J4 U 0.133 5.00 10.0 1 07/27/2022 18:08 WG1899773
2,4-Dichlorophenol 120-83-2 5.00 J4 U 0.102 5.00 10.0 1 07/27/2022 18:08 WG1899773
2,4-Dimethylphenol 105-67-9 5.00 U 0.0636 5.00 10.0 1 07/27/2022 18:08 WG1899773
4,6-Dinitro-2-methylphenol 534-52-1 5.00 U 1.12 5.00 10.0 1 07/27/2022 18:08 WG1899773
2,4-Dinitrophenol 51-28-5 15.0 U 5.93 15.0 30.0 1 07/27/2022 18:08 WG1899773
2-Nitrophenol 88-75-5 5.00 J4 U 0.117 5.00 10.0 1 07/27/2022 18:08 WG1899773
4-Nitrophenol 100-02-7 5.00 U 0.143 5.00 10.0 1 07/27/2022 18:08 WG1899773
Pentachlorophenol 87-86-5 5.00 U 0.313 5.00 10.0 1 07/27/2022 18:08 WG1899773
Phenol 108-95-2 10.0 U 4.33 10.0 20.0 1 07/27/2022 18:08 WG1899773
2,4,6-Trichlorophenol 88-06-2 5.00 U 0.100 5.00 10.0 1 07/27/2022 18:08 WG1899773
1-Methylnaphthalene 90-12-0 3.70 0.0790 0.500 1.00 1 07/27/2022 18:08 WG1899773
2-Methylnaphthalene 91-57-6 0.616 J 0.117 0.500 1.00 1 07/27/2022 18:08 WG1899773
(S) Nitrobenzene-d5 4165-60-0 56.2 0.000 44.0-120 07/27/2022 18:08 WG1899773
(S) 2-Fluorobiphenyl 321-60-8 48.6 0.000 44.0-119 07/27/2022 18:08 WG1899773
(S) p-Terphenyl-d14 1718-51-0 50.9 0.000 50.0-134 07/27/2022 18:08 WG1899773
(S) Phenol-d5 4165-62-2 14.3 0.000 10.0-67.0 07/27/2022 18:08 WG1899773
(S) 2-Fluorophenol 367-12-4 22.4 0.000 19.0-119 07/27/2022 18:08 WG1899773
(S) 2,4,6-Tribromophenol 118-79-6 68.7 0.000 43.0-140 07/27/2022 18:08 WG1899773
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 15:39 12 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 16:01 12 of 65
====================----□ □ □ □
□ □ □ □
SAMPLE RESULTS - 03
L1516722
USTG480-MW11
Collected date/time: 07/18/22 10:00
Volatile Petroleum Hydrocarbons by Method MADEPV
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics C5-C8 ALI
UNADJ 42.0 J 33.3 67.0 100 1 07/23/2022 22:17 WG1899531
Unadjusted C9-C12 Aliphatics C9-C12 ALI
UNADJ 254 33.3 67.0 134 1 07/23/2022 22:17 WG1899531
Unadjusted C9-C10 Aromatics C9-C10 ARO
UNADJ 344 33.3 67.0 100 1 07/23/2022 22:17 WG1899531
Total VPH VPH 640 66.7 150 300 1 07/23/2022 22:17 WG1899531
(S) 2,5-Dibromotoluene(FID)615-59-8 119 70.0-130 07/23/2022 22:17 WG1899531
(S) 2,5-Dibromotoluene(PID)615-59-8 106 70.0-130 07/23/2022 22:17 WG1899531
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acetone 67-64-1 11.6 J 11.3 25.0 50.0 1 07/23/2022 13:29 WG1899800
Acrolein 107-02-8 25.0 U 2.54 25.0 50.0 1 07/23/2022 13:29 WG1899800
Acrylonitrile 107-13-1 5.00 U 0.671 5.00 10.0 1 07/23/2022 13:29 WG1899800
Benzene 71-43-2 0.423 J 0.0941 0.500 1.00 1 07/23/2022 13:29 WG1899800
Bromobenzene 108-86-1 0.500 C4 J4 U 0.118 0.500 1.00 1 07/23/2022 13:29 WG1899800
Bromodichloromethane 75-27-4 0.500 U 0.136 0.500 1.00 1 07/23/2022 13:29 WG1899800
Bromoform 75-25-2 0.500 U 0.129 0.500 1.00 1 07/23/2022 13:29 WG1899800
Bromomethane 74-83-9 2.00 U 0.605 2.00 5.00 1 07/23/2022 13:29 WG1899800
n-Butylbenzene 104-51-8 0.500 U 0.157 0.500 1.00 1 07/23/2022 13:29 WG1899800
sec-Butylbenzene 135-98-8 0.448 J 0.125 0.500 1.00 1 07/23/2022 13:29 WG1899800
tert-Butylbenzene 98-06-6 0.505 J 0.127 0.500 1.00 1 07/23/2022 13:29 WG1899800
Carbon tetrachloride 56-23-5 0.500 U 0.128 0.500 1.00 1 07/23/2022 13:29 WG1899800
Chlorobenzene 108-90-7 0.500 U 0.116 0.500 1.00 1 07/23/2022 13:29 WG1899800
Chlorodibromomethane 124-48-1 0.500 U 0.140 0.500 1.00 1 07/23/2022 13:29 WG1899800
Chloroethane 75-00-3 2.00 U 0.192 2.00 5.00 1 07/23/2022 13:29 WG1899800
Chloroform 67-66-3 2.00 U 0.111 2.00 5.00 1 07/23/2022 13:29 WG1899800
Chloromethane 74-87-3 2.00 U 0.960 2.00 4.00 1 07/23/2022 13:29 WG1899800
2-Chlorotoluene 95-49-8 0.500 U 0.106 0.500 1.00 1 07/23/2022 13:29 WG1899800
4-Chlorotoluene 106-43-4 0.500 U 0.114 0.500 1.00 1 07/23/2022 13:29 WG1899800
1,2-Dibromo-3-Chloropropane 96-12-8 2.00 U 0.276 2.00 5.00 1 07/23/2022 13:29 WG1899800
1,2-Dibromoethane 106-93-4 0.500 U 0.126 0.500 1.00 1 07/23/2022 13:29 WG1899800
Dibromomethane 74-95-3 0.500 U 0.122 0.500 1.00 1 07/23/2022 13:29 WG1899800
1,2-Dichlorobenzene 95-50-1 0.500 U 0.107 0.500 1.00 1 07/23/2022 13:29 WG1899800
1,3-Dichlorobenzene 541-73-1 0.500 U 0.110 0.500 1.00 1 07/23/2022 13:29 WG1899800
1,4-Dichlorobenzene 106-46-7 0.500 U 0.120 0.500 1.00 1 07/23/2022 13:29 WG1899800
Dichlorodifluoromethane 75-71-8 2.00 U 0.374 2.00 5.00 1 07/23/2022 13:29 WG1899800
1,1-Dichloroethane 75-34-3 0.500 U 0.100 0.500 1.00 1 07/23/2022 13:29 WG1899800
1,2-Dichloroethane 107-06-2 0.500 U 0.0819 0.500 1.00 1 07/23/2022 13:29 WG1899800
1,1-Dichloroethene 75-35-4 0.500 U 0.188 0.500 1.00 1 07/23/2022 13:29 WG1899800
cis-1,2-Dichloroethene 156-59-2 0.500 U 0.126 0.500 1.00 1 07/23/2022 13:29 WG1899800
trans-1,2-Dichloroethene 156-60-5 0.500 U 0.149 0.500 1.00 1 07/23/2022 13:29 WG1899800
1,2-Dichloropropane 78-87-5 0.500 U 0.149 0.500 1.00 1 07/23/2022 13:29 WG1899800
1,1-Dichloropropene 563-58-6 0.500 U 0.142 0.500 1.00 1 07/23/2022 13:29 WG1899800
1,3-Dichloropropane 142-28-9 0.500 U 0.110 0.500 1.00 1 07/23/2022 13:29 WG1899800
2,2-Dichloropropane 594-20-7 0.500 U 0.161 0.500 1.00 1 07/23/2022 13:29 WG1899800
Di-isopropyl ether 108-20-3 0.500 U 0.105 0.500 1.00 1 07/23/2022 13:29 WG1899800
Ethylbenzene 100-41-4 15.3 0.137 0.500 1.00 1 07/23/2022 13:29 WG1899800
Hexachloro-1,3-butadiene 87-68-3 0.750 U 0.337 0.750 1.50 1 07/23/2022 13:29 WG1899800
Isopropylbenzene 98-82-8 14.0 0.105 0.500 1.00 1 07/23/2022 13:29 WG1899800
p-Isopropyltoluene 99-87-6 0.381 J 0.120 0.500 1.00 1 07/23/2022 13:29 WG1899800
2-Butanone (MEK)78-93-3 1.70 J 1.19 5.00 10.0 1 07/23/2022 13:29 WG1899800
Methylene Chloride 75-09-2 2.00 U 0.430 2.00 5.00 1 07/23/2022 13:29 WG1899800
4-Methyl-2-pentanone (MIBK)108-10-1 5.00 U 0.478 5.00 10.0 1 07/23/2022 13:29 WG1899800
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 15:39 13 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 16:01 13 of 65
--------------=---□
□ □ □
==============~~~~~=----□ □ □ □
SAMPLE RESULTS - 03
L1516722
USTG480-MW11
Collected date/time: 07/18/22 10:00
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Methyl tert-butyl ether 1634-04-4 0.500 U 0.101 0.500 1.00 1 07/23/2022 13:29 WG1899800
Naphthalene 91-20-3 72.7 1.00 2.00 5.00 1 07/23/2022 13:29 WG1899800
n-Propylbenzene 103-65-1 15.5 C4 J4 0.0993 0.500 1.00 1 07/23/2022 13:29 WG1899800
Styrene 100-42-5 0.500 U 0.118 0.500 1.00 1 07/23/2022 13:29 WG1899800
1,1,1,2-Tetrachloroethane 630-20-6 0.500 U 0.147 0.500 1.00 1 07/23/2022 13:29 WG1899800
1,1,2,2-Tetrachloroethane 79-34-5 0.500 U 0.133 0.500 1.00 1 07/23/2022 13:29 WG1899800
Tetrachloroethene 127-18-4 0.600 U 0.300 0.600 1.20 1 07/23/2022 13:29 WG1899800
Toluene 108-88-3 0.641 J 0.278 0.600 1.20 1 07/23/2022 13:29 WG1899800
1,2,3-Trichlorobenzene 87-61-6 0.500 C4 U 0.230 0.500 1.00 1 07/23/2022 13:29 WG1899800
1,2,4-Trichlorobenzene 120-82-1 1.00 U 0.481 1.00 2.00 1 07/23/2022 13:29 WG1899800
1,1,1-Trichloroethane 71-55-6 0.500 U 0.149 0.500 1.00 1 07/23/2022 13:29 WG1899800
1,1,2-Trichloroethane 79-00-5 0.500 U 0.158 0.500 1.00 1 07/23/2022 13:29 WG1899800
Trichloroethene 79-01-6 0.500 U 0.190 0.500 1.00 1 07/23/2022 13:29 WG1899800
Trichlorofluoromethane 75-69-4 2.00 U 0.160 2.00 5.00 1 07/23/2022 13:29 WG1899800
1,2,3-Trichloropropane 96-18-4 1.00 U 0.237 1.00 2.50 1 07/23/2022 13:29 WG1899800
1,2,4-Trimethylbenzene 95-63-6 1.00 U 0.322 1.00 2.00 1 07/23/2022 13:29 WG1899800
1,3,5-Trimethylbenzene 108-67-8 0.500 U 0.104 0.500 1.00 1 07/23/2022 13:29 WG1899800
Vinyl chloride 75-01-4 0.500 U 0.234 0.500 1.00 1 07/23/2022 13:29 WG1899800
o-Xylene 95-47-6 1.46 0.174 0.500 1.00 1 07/23/2022 13:29 WG1899800
m&p-Xylenes 1330-20-7 0.504 J 0.430 1.00 2.00 1 07/23/2022 13:29 WG1899800
(S) Toluene-d8 2037-26-5 103 89.0-112 07/23/2022 13:29 WG1899800
(S) 4-Bromofluorobenzene 460-00-4 90.1 85.0-114 07/23/2022 13:29 WG1899800
(S) 1,2-Dichloroethane-d4 17060-07-0 93.5 81.0-118 07/23/2022 13:29 WG1899800
TPH by Method MADEPE
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics C9-C18 ALI
UNADJ 123 J 33.3 67.0 134 1 07/29/2022 18:59 WG1902170
Unadjusted C19-C36 Aliphatics C19-C36 ALI
UNADJ 56.2 B J 33.3 67.0 134 1 07/29/2022 18:59 WG1902170
Unadjusted C11-C22 Aromatics C11-C22 ARO
UNADJ 650 33.3 67.0 134 1 07/29/2022 20:09 WG1902170
Unadjusted Total Petroleum
Hydrocarbons TPH UNADJ 829 33.3 67.0 134 1 07/29/2022 20:09 WG1902170
(S) o-Terphenyl 84-15-1 62.1 40.0-140 07/29/2022 20:09 WG1902170
(S) 1-Chloro-octadecane 3386-33-2 52.3 40.0-140 07/29/2022 18:59 WG1902170
(S) 2-Fluorobiphenyl 321-60-8 133 40.0-140 07/29/2022 20:09 WG1902170
(S) 2-Bromonaphthalene 580-13-2 82.0 40.0-140 07/29/2022 20:09 WG1902170
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acenaphthene 83-32-9 2.35 J4 0.0983 0.555 1.11 1.11 07/23/2022 20:00 WG1899773
Acenaphthylene 208-96-8 0.555 U 0.102 0.555 1.11 1.11 07/23/2022 20:00 WG1899773
Anthracene 120-12-7 0.249 J J4 0.0892 0.555 1.11 1.11 07/23/2022 20:00 WG1899773
Benzidine 92-87-5 8.33 U 4.15 8.33 16.7 1.11 07/23/2022 20:00 WG1899773
Benzo(a)anthracene 56-55-3 0.555 U 0.221 0.555 1.11 1.11 07/23/2022 20:00 WG1899773
Benzo(b)fluoranthene 205-99-2 0.555 U 0.144 0.555 1.11 1.11 07/23/2022 20:00 WG1899773
Benzo(k)fluoranthene 207-08-9 0.555 U 0.133 0.555 1.11 1.11 07/23/2022 20:00 WG1899773
Benzo(g,h,i)perylene 191-24-2 0.555 U 0.134 0.555 1.11 1.11 07/23/2022 20:00 WG1899773
Benzo(a)pyrene 50-32-8 0.555 U 0.0423 0.555 1.11 1.11 07/23/2022 20:00 WG1899773
Bis(2-chlorethoxy)methane 111-91-1 5.55 J4 U 0.129 5.55 11.1 1.11 07/23/2022 20:00 WG1899773
Bis(2-chloroethyl)ether 111-44-4 5.55 J4 U 0.152 5.55 11.1 1.11 07/23/2022 20:00 WG1899773
2,2-Oxybis(1-Chloropropane)108-60-1 5.55 J4 U 0.233 5.55 11.1 1.11 07/23/2022 20:00 WG1899773
4-Bromophenyl-phenylether 101-55-3 5.55 U 0.0973 5.55 11.1 1.11 07/23/2022 20:00 WG1899773
2-Chloronaphthalene 91-58-7 0.555 U 0.0719 0.555 1.11 1.11 07/23/2022 20:00 WG1899773
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 15:39 14 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 16:01 14 of 65
====================----□ □ □ □
□ □ □ □
SAMPLE RESULTS - 03
L1516722
USTG480-MW11
Collected date/time: 07/18/22 10:00
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
4-Chlorophenyl-phenylether 7005-72-3 5.55 U 0.103 5.55 11.1 1.11 07/23/2022 20:00 WG1899773
Chrysene 218-01-9 0.555 U 0.144 0.555 1.11 1.11 07/23/2022 20:00 WG1899773
Dibenz(a,h)anthracene 53-70-3 0.555 U 0.0715 0.555 1.11 1.11 07/23/2022 20:00 WG1899773
3,3-Dichlorobenzidine 91-94-1 5.55 U 0.235 5.55 11.1 1.11 07/23/2022 20:00 WG1899773
2,4-Dinitrotoluene 121-14-2 5.55 U 0.109 5.55 11.1 1.11 07/23/2022 20:00 WG1899773
2,6-Dinitrotoluene 606-20-2 5.55 U 0.278 5.55 11.1 1.11 07/23/2022 20:00 WG1899773
Fluoranthene 206-44-0 0.555 U 0.113 0.555 1.11 1.11 07/23/2022 20:00 WG1899773
Fluorene 86-73-7 3.22 0.0937 0.555 1.11 1.11 07/23/2022 20:00 WG1899773
Hexachlorobenzene 118-74-1 0.555 U 0.0838 0.555 1.11 1.11 07/23/2022 20:00 WG1899773
Hexachloro-1,3-butadiene 87-68-3 5.55 U 0.107 5.55 11.1 1.11 07/23/2022 20:00 WG1899773
Hexachlorocyclopentadiene 77-47-4 5.55 U 0.0664 5.55 11.1 1.11 07/23/2022 20:00 WG1899773
Hexachloroethane 67-72-1 5.55 U 0.141 5.55 11.1 1.11 07/23/2022 20:00 WG1899773
Indeno(1,2,3-cd)pyrene 193-39-5 0.666 U 0.310 0.666 1.33 1.11 07/23/2022 20:00 WG1899773
Isophorone 78-59-1 5.55 U 0.159 5.55 11.1 1.11 07/23/2022 20:00 WG1899773
Naphthalene 91-20-3 32.1 J4 0.176 0.555 1.11 1.11 07/23/2022 20:00 WG1899773
Nitrobenzene 98-95-3 5.55 J4 U 0.330 5.55 11.1 1.11 07/23/2022 20:00 WG1899773
n-Nitrosodimethylamine 62-75-9 5.55 U 1.11 5.55 11.1 1.11 07/23/2022 20:00 WG1899773
n-Nitrosodiphenylamine 86-30-6 5.55 J4 U 2.63 5.55 11.1 1.11 07/23/2022 20:00 WG1899773
n-Nitrosodi-n-propylamine 621-64-7 5.55 J4 U 0.290 5.55 11.1 1.11 07/23/2022 20:00 WG1899773
Phenanthrene 85-01-8 2.92 J4 0.124 0.555 1.11 1.11 07/23/2022 20:00 WG1899773
Benzylbutyl phthalate 85-68-7 2.22 U 0.849 2.22 4.44 1.11 07/23/2022 20:00 WG1899773
Bis(2-ethylhexyl)phthalate 117-81-7 2.22 U 0.993 2.22 4.44 1.11 07/23/2022 20:00 WG1899773
Di-n-butyl phthalate 84-74-2 1.67 U 0.503 1.67 3.33 1.11 07/23/2022 20:00 WG1899773
Diethyl phthalate 84-66-2 1.67 U 0.319 1.67 3.33 1.11 07/23/2022 20:00 WG1899773
Dimethyl phthalate 131-11-3 1.67 U 0.289 1.67 3.33 1.11 07/23/2022 20:00 WG1899773
Di-n-octyl phthalate 117-84-0 2.22 U 1.03 2.22 4.44 1.11 07/23/2022 20:00 WG1899773
Pyrene 129-00-0 0.555 J4 U 0.119 0.555 1.11 1.11 07/23/2022 20:00 WG1899773
1,2,4-Trichlorobenzene 120-82-1 5.55 U 0.0775 5.55 11.1 1.11 07/23/2022 20:00 WG1899773
4-Chloro-3-methylphenol 59-50-7 5.55 U 0.145 5.55 11.1 1.11 07/23/2022 20:00 WG1899773
2-Chlorophenol 95-57-8 5.55 J4 U 0.148 5.55 11.1 1.11 07/23/2022 20:00 WG1899773
2,4-Dichlorophenol 120-83-2 5.55 J4 U 0.113 5.55 11.1 1.11 07/23/2022 20:00 WG1899773
2,4-Dimethylphenol 105-67-9 5.55 U 0.0706 5.55 11.1 1.11 07/23/2022 20:00 WG1899773
4,6-Dinitro-2-methylphenol 534-52-1 5.55 U 1.24 5.55 11.1 1.11 07/23/2022 20:00 WG1899773
2,4-Dinitrophenol 51-28-5 16.7 U 6.58 16.7 33.3 1.11 07/23/2022 20:00 WG1899773
2-Nitrophenol 88-75-5 5.55 J4 U 0.130 5.55 11.1 1.11 07/23/2022 20:00 WG1899773
4-Nitrophenol 100-02-7 5.55 U 0.159 5.55 11.1 1.11 07/23/2022 20:00 WG1899773
Pentachlorophenol 87-86-5 5.55 U 0.347 5.55 11.1 1.11 07/23/2022 20:00 WG1899773
Phenol 108-95-2 11.1 U 4.81 11.1 22.2 1.11 07/23/2022 20:00 WG1899773
2,4,6-Trichlorophenol 88-06-2 5.55 U 0.111 5.55 11.1 1.11 07/23/2022 20:00 WG1899773
1-Methylnaphthalene 90-12-0 74.8 0.0877 0.555 1.11 1.11 07/23/2022 20:00 WG1899773
2-Methylnaphthalene 91-57-6 5.68 0.130 0.555 1.11 1.11 07/23/2022 20:00 WG1899773
(S) Nitrobenzene-d5 4165-60-0 56.9 0.000 44.0-120 07/23/2022 20:00 WG1899773
(S) 2-Fluorobiphenyl 321-60-8 50.5 0.000 44.0-119 07/23/2022 20:00 WG1899773
(S) p-Terphenyl-d14 1718-51-0 58.1 0.000 50.0-134 07/23/2022 20:00 WG1899773
(S) Phenol-d5 4165-62-2 22.2 0.000 10.0-67.0 07/23/2022 20:00 WG1899773
(S) 2-Fluorophenol 367-12-4 30.7 0.000 19.0-119 07/23/2022 20:00 WG1899773
(S) 2,4,6-Tribromophenol 118-79-6 65.8 0.000 43.0-140 07/23/2022 20:00 WG1899773
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 15:39 15 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 16:01 15 of 65
====================----□ □ □ □
□ □ □ □
SAMPLE RESULTS - 04
L1516722
USTTC341-MW05
Collected date/time: 07/18/22 10:45
Volatile Petroleum Hydrocarbons by Method MADEPV
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics C5-C8 ALI
UNADJ 67.0 U 33.3 67.0 100 1 07/23/2022 22:49 WG1899531
Unadjusted C9-C12 Aliphatics C9-C12 ALI
UNADJ 128 J 33.3 67.0 134 1 07/23/2022 22:49 WG1899531
Unadjusted C9-C10 Aromatics C9-C10 ARO
UNADJ 60.7 J 33.3 67.0 100 1 07/23/2022 22:49 WG1899531
Total VPH VPH 189 J 66.7 150 300 1 07/23/2022 22:49 WG1899531
(S) 2,5-Dibromotoluene(FID)615-59-8 108 70.0-130 07/23/2022 22:49 WG1899531
(S) 2,5-Dibromotoluene(PID)615-59-8 103 70.0-130 07/23/2022 22:49 WG1899531
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acetone 67-64-1 25.0 U 11.3 25.0 50.0 1 07/23/2022 13:49 WG1899800
Acrolein 107-02-8 25.0 U 2.54 25.0 50.0 1 07/23/2022 13:49 WG1899800
Acrylonitrile 107-13-1 5.00 U 0.671 5.00 10.0 1 07/23/2022 13:49 WG1899800
Benzene 71-43-2 0.500 U 0.0941 0.500 1.00 1 07/23/2022 13:49 WG1899800
Bromobenzene 108-86-1 0.500 C4 J4 U 0.118 0.500 1.00 1 07/23/2022 13:49 WG1899800
Bromodichloromethane 75-27-4 0.500 U 0.136 0.500 1.00 1 07/23/2022 13:49 WG1899800
Bromoform 75-25-2 0.500 U 0.129 0.500 1.00 1 07/23/2022 13:49 WG1899800
Bromomethane 74-83-9 2.00 U 0.605 2.00 5.00 1 07/23/2022 13:49 WG1899800
n-Butylbenzene 104-51-8 0.500 U 0.157 0.500 1.00 1 07/23/2022 13:49 WG1899800
sec-Butylbenzene 135-98-8 0.858 J 0.125 0.500 1.00 1 07/23/2022 13:49 WG1899800
tert-Butylbenzene 98-06-6 0.567 J 0.127 0.500 1.00 1 07/23/2022 13:49 WG1899800
Carbon tetrachloride 56-23-5 0.500 U 0.128 0.500 1.00 1 07/23/2022 13:49 WG1899800
Chlorobenzene 108-90-7 0.500 U 0.116 0.500 1.00 1 07/23/2022 13:49 WG1899800
Chlorodibromomethane 124-48-1 0.500 U 0.140 0.500 1.00 1 07/23/2022 13:49 WG1899800
Chloroethane 75-00-3 2.00 U 0.192 2.00 5.00 1 07/23/2022 13:49 WG1899800
Chloroform 67-66-3 2.00 U 0.111 2.00 5.00 1 07/23/2022 13:49 WG1899800
Chloromethane 74-87-3 2.00 U 0.960 2.00 4.00 1 07/23/2022 13:49 WG1899800
2-Chlorotoluene 95-49-8 0.500 U 0.106 0.500 1.00 1 07/23/2022 13:49 WG1899800
4-Chlorotoluene 106-43-4 0.500 U 0.114 0.500 1.00 1 07/23/2022 13:49 WG1899800
1,2-Dibromo-3-Chloropropane 96-12-8 2.00 U 0.276 2.00 5.00 1 07/23/2022 13:49 WG1899800
1,2-Dibromoethane 106-93-4 0.500 U 0.126 0.500 1.00 1 07/23/2022 13:49 WG1899800
Dibromomethane 74-95-3 0.500 U 0.122 0.500 1.00 1 07/23/2022 13:49 WG1899800
1,2-Dichlorobenzene 95-50-1 0.500 U 0.107 0.500 1.00 1 07/23/2022 13:49 WG1899800
1,3-Dichlorobenzene 541-73-1 0.500 U 0.110 0.500 1.00 1 07/23/2022 13:49 WG1899800
1,4-Dichlorobenzene 106-46-7 0.500 U 0.120 0.500 1.00 1 07/23/2022 13:49 WG1899800
Dichlorodifluoromethane 75-71-8 2.00 U 0.374 2.00 5.00 1 07/23/2022 13:49 WG1899800
1,1-Dichloroethane 75-34-3 0.500 U 0.100 0.500 1.00 1 07/23/2022 13:49 WG1899800
1,2-Dichloroethane 107-06-2 0.500 U 0.0819 0.500 1.00 1 07/23/2022 13:49 WG1899800
1,1-Dichloroethene 75-35-4 0.500 U 0.188 0.500 1.00 1 07/23/2022 13:49 WG1899800
cis-1,2-Dichloroethene 156-59-2 0.500 U 0.126 0.500 1.00 1 07/23/2022 13:49 WG1899800
trans-1,2-Dichloroethene 156-60-5 0.500 U 0.149 0.500 1.00 1 07/23/2022 13:49 WG1899800
1,2-Dichloropropane 78-87-5 0.500 U 0.149 0.500 1.00 1 07/23/2022 13:49 WG1899800
1,1-Dichloropropene 563-58-6 0.500 U 0.142 0.500 1.00 1 07/23/2022 13:49 WG1899800
1,3-Dichloropropane 142-28-9 0.500 U 0.110 0.500 1.00 1 07/23/2022 13:49 WG1899800
2,2-Dichloropropane 594-20-7 0.500 U 0.161 0.500 1.00 1 07/23/2022 13:49 WG1899800
Di-isopropyl ether 108-20-3 0.500 U 0.105 0.500 1.00 1 07/23/2022 13:49 WG1899800
Ethylbenzene 100-41-4 0.500 U 0.137 0.500 1.00 1 07/23/2022 13:49 WG1899800
Hexachloro-1,3-butadiene 87-68-3 0.750 U 0.337 0.750 1.50 1 07/23/2022 13:49 WG1899800
Isopropylbenzene 98-82-8 0.242 J 0.105 0.500 1.00 1 07/23/2022 13:49 WG1899800
p-Isopropyltoluene 99-87-6 0.500 U 0.120 0.500 1.00 1 07/23/2022 13:49 WG1899800
2-Butanone (MEK)78-93-3 5.00 U 1.19 5.00 10.0 1 07/23/2022 13:49 WG1899800
Methylene Chloride 75-09-2 2.00 U 0.430 2.00 5.00 1 07/23/2022 13:49 WG1899800
4-Methyl-2-pentanone (MIBK)108-10-1 5.00 U 0.478 5.00 10.0 1 07/23/2022 13:49 WG1899800
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 15:39 16 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 16:01 16 of 65
--------------=---□
□ □ □
==============~~~~~=----□ □ □ □
SAMPLE RESULTS - 04
L1516722
USTTC341-MW05
Collected date/time: 07/18/22 10:45
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Methyl tert-butyl ether 1634-04-4 0.500 U 0.101 0.500 1.00 1 07/23/2022 13:49 WG1899800
Naphthalene 91-20-3 2.76 J 1.00 2.00 5.00 1 07/23/2022 13:49 WG1899800
n-Propylbenzene 103-65-1 0.500 C4 J4 U 0.0993 0.500 1.00 1 07/23/2022 13:49 WG1899800
Styrene 100-42-5 0.500 U 0.118 0.500 1.00 1 07/23/2022 13:49 WG1899800
1,1,1,2-Tetrachloroethane 630-20-6 0.500 U 0.147 0.500 1.00 1 07/23/2022 13:49 WG1899800
1,1,2,2-Tetrachloroethane 79-34-5 0.500 U 0.133 0.500 1.00 1 07/23/2022 13:49 WG1899800
Tetrachloroethene 127-18-4 0.600 U 0.300 0.600 1.20 1 07/23/2022 13:49 WG1899800
Toluene 108-88-3 0.600 U 0.278 0.600 1.20 1 07/23/2022 13:49 WG1899800
1,2,3-Trichlorobenzene 87-61-6 0.500 C4 U 0.230 0.500 1.00 1 07/23/2022 13:49 WG1899800
1,2,4-Trichlorobenzene 120-82-1 1.00 U 0.481 1.00 2.00 1 07/23/2022 13:49 WG1899800
1,1,1-Trichloroethane 71-55-6 0.500 U 0.149 0.500 1.00 1 07/23/2022 13:49 WG1899800
1,1,2-Trichloroethane 79-00-5 0.500 U 0.158 0.500 1.00 1 07/23/2022 13:49 WG1899800
Trichloroethene 79-01-6 0.500 U 0.190 0.500 1.00 1 07/23/2022 13:49 WG1899800
Trichlorofluoromethane 75-69-4 2.00 U 0.160 2.00 5.00 1 07/23/2022 13:49 WG1899800
1,2,3-Trichloropropane 96-18-4 1.00 U 0.237 1.00 2.50 1 07/23/2022 13:49 WG1899800
1,2,4-Trimethylbenzene 95-63-6 1.00 U 0.322 1.00 2.00 1 07/23/2022 13:49 WG1899800
1,3,5-Trimethylbenzene 108-67-8 0.500 U 0.104 0.500 1.00 1 07/23/2022 13:49 WG1899800
Vinyl chloride 75-01-4 0.500 U 0.234 0.500 1.00 1 07/23/2022 13:49 WG1899800
o-Xylene 95-47-6 0.500 U 0.174 0.500 1.00 1 07/23/2022 13:49 WG1899800
m&p-Xylenes 1330-20-7 1.00 U 0.430 1.00 2.00 1 07/23/2022 13:49 WG1899800
(S) Toluene-d8 2037-26-5 107 89.0-112 07/23/2022 13:49 WG1899800
(S) 4-Bromofluorobenzene 460-00-4 91.4 85.0-114 07/23/2022 13:49 WG1899800
(S) 1,2-Dichloroethane-d4 17060-07-0 97.0 81.0-118 07/23/2022 13:49 WG1899800
TPH by Method MADEPE
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics C9-C18 ALI
UNADJ 60.1 J 33.3 67.0 134 1 07/29/2022 19:23 WG1902170
Unadjusted C19-C36 Aliphatics C19-C36 ALI
UNADJ 639 33.3 67.0 134 1 07/29/2022 19:23 WG1902170
Unadjusted C11-C22 Aromatics C11-C22 ARO
UNADJ 77.6 B J 33.3 67.0 134 1 07/29/2022 19:46 WG1902170
Unadjusted Total Petroleum
Hydrocarbons TPH UNADJ 777 33.3 67.0 134 1 07/29/2022 19:46 WG1902170
(S) o-Terphenyl 84-15-1 67.6 40.0-140 07/29/2022 19:46 WG1902170
(S) 1-Chloro-octadecane 3386-33-2 62.8 40.0-140 07/29/2022 19:23 WG1902170
(S) 2-Fluorobiphenyl 321-60-8 85.8 40.0-140 07/29/2022 19:46 WG1902170
(S) 2-Bromonaphthalene 580-13-2 84.4 40.0-140 07/29/2022 19:46 WG1902170
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acenaphthene 83-32-9 0.500 J4 U 0.0886 0.500 1.00 1 07/23/2022 13:44 WG1899773
Acenaphthylene 208-96-8 0.500 U 0.0921 0.500 1.00 1 07/23/2022 13:44 WG1899773
Anthracene 120-12-7 0.500 J4 U 0.0804 0.500 1.00 1 07/23/2022 13:44 WG1899773
Benzidine 92-87-5 7.50 U 3.74 7.50 15.0 1 07/23/2022 13:44 WG1899773
Benzo(a)anthracene 56-55-3 0.500 U 0.199 0.500 1.00 1 07/23/2022 13:44 WG1899773
Benzo(b)fluoranthene 205-99-2 0.500 U 0.130 0.500 1.00 1 07/23/2022 13:44 WG1899773
Benzo(k)fluoranthene 207-08-9 0.500 U 0.120 0.500 1.00 1 07/23/2022 13:44 WG1899773
Benzo(g,h,i)perylene 191-24-2 0.500 U 0.121 0.500 1.00 1 07/23/2022 13:44 WG1899773
Benzo(a)pyrene 50-32-8 0.500 U 0.0381 0.500 1.00 1 07/23/2022 13:44 WG1899773
Bis(2-chlorethoxy)methane 111-91-1 5.00 J4 U 0.116 5.00 10.0 1 07/23/2022 13:44 WG1899773
Bis(2-chloroethyl)ether 111-44-4 5.00 J4 U 0.137 5.00 10.0 1 07/23/2022 13:44 WG1899773
2,2-Oxybis(1-Chloropropane)108-60-1 5.00 J4 U 0.210 5.00 10.0 1 07/23/2022 13:44 WG1899773
4-Bromophenyl-phenylether 101-55-3 5.00 U 0.0877 5.00 10.0 1 07/23/2022 13:44 WG1899773
2-Chloronaphthalene 91-58-7 0.500 U 0.0648 0.500 1.00 1 07/23/2022 13:44 WG1899773
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 15:39 17 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 16:01 17 of 65
====================----□ □ □ □
□ □ □ □
SAMPLE RESULTS - 04
L1516722
USTTC341-MW05
Collected date/time: 07/18/22 10:45
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
4-Chlorophenyl-phenylether 7005-72-3 5.00 U 0.0926 5.00 10.0 1 07/23/2022 13:44 WG1899773
Chrysene 218-01-9 0.500 U 0.130 0.500 1.00 1 07/23/2022 13:44 WG1899773
Dibenz(a,h)anthracene 53-70-3 0.500 U 0.0644 0.500 1.00 1 07/23/2022 13:44 WG1899773
3,3-Dichlorobenzidine 91-94-1 5.00 U 0.212 5.00 10.0 1 07/23/2022 13:44 WG1899773
2,4-Dinitrotoluene 121-14-2 5.00 U 0.0983 5.00 10.0 1 07/23/2022 13:44 WG1899773
2,6-Dinitrotoluene 606-20-2 5.00 U 0.250 5.00 10.0 1 07/23/2022 13:44 WG1899773
Fluoranthene 206-44-0 0.500 U 0.102 0.500 1.00 1 07/23/2022 13:44 WG1899773
Fluorene 86-73-7 0.500 U 0.0844 0.500 1.00 1 07/23/2022 13:44 WG1899773
Hexachlorobenzene 118-74-1 0.500 U 0.0755 0.500 1.00 1 07/23/2022 13:44 WG1899773
Hexachloro-1,3-butadiene 87-68-3 5.00 U 0.0968 5.00 10.0 1 07/23/2022 13:44 WG1899773
Hexachlorocyclopentadiene 77-47-4 5.00 U 0.0598 5.00 10.0 1 07/23/2022 13:44 WG1899773
Hexachloroethane 67-72-1 5.00 U 0.127 5.00 10.0 1 07/23/2022 13:44 WG1899773
Indeno(1,2,3-cd)pyrene 193-39-5 0.600 U 0.279 0.600 1.20 1 07/23/2022 13:44 WG1899773
Isophorone 78-59-1 5.00 U 0.143 5.00 10.0 1 07/23/2022 13:44 WG1899773
Naphthalene 91-20-3 0.469 J J4 0.159 0.500 1.00 1 07/23/2022 13:44 WG1899773
Nitrobenzene 98-95-3 5.00 J4 U 0.297 5.00 10.0 1 07/23/2022 13:44 WG1899773
n-Nitrosodimethylamine 62-75-9 5.00 U 0.998 5.00 10.0 1 07/23/2022 13:44 WG1899773
n-Nitrosodiphenylamine 86-30-6 5.00 J4 U 2.37 5.00 10.0 1 07/23/2022 13:44 WG1899773
n-Nitrosodi-n-propylamine 621-64-7 5.00 J4 U 0.261 5.00 10.0 1 07/23/2022 13:44 WG1899773
Phenanthrene 85-01-8 0.500 J4 U 0.112 0.500 1.00 1 07/23/2022 13:44 WG1899773
Benzylbutyl phthalate 85-68-7 2.00 U 0.765 2.00 4.00 1 07/23/2022 13:44 WG1899773
Bis(2-ethylhexyl)phthalate 117-81-7 2.00 U 0.895 2.00 4.00 1 07/23/2022 13:44 WG1899773
Di-n-butyl phthalate 84-74-2 1.50 U 0.453 1.50 3.00 1 07/23/2022 13:44 WG1899773
Diethyl phthalate 84-66-2 1.50 U 0.287 1.50 3.00 1 07/23/2022 13:44 WG1899773
Dimethyl phthalate 131-11-3 1.50 U 0.260 1.50 3.00 1 07/23/2022 13:44 WG1899773
Di-n-octyl phthalate 117-84-0 2.00 U 0.932 2.00 4.00 1 07/23/2022 13:44 WG1899773
Pyrene 129-00-0 0.500 J4 U 0.107 0.500 1.00 1 07/23/2022 13:44 WG1899773
1,2,4-Trichlorobenzene 120-82-1 5.00 U 0.0698 5.00 10.0 1 07/23/2022 13:44 WG1899773
4-Chloro-3-methylphenol 59-50-7 5.00 U 0.131 5.00 10.0 1 07/23/2022 13:44 WG1899773
2-Chlorophenol 95-57-8 5.00 J4 U 0.133 5.00 10.0 1 07/23/2022 13:44 WG1899773
2,4-Dichlorophenol 120-83-2 5.00 J4 U 0.102 5.00 10.0 1 07/23/2022 13:44 WG1899773
2,4-Dimethylphenol 105-67-9 5.00 U 0.0636 5.00 10.0 1 07/23/2022 13:44 WG1899773
4,6-Dinitro-2-methylphenol 534-52-1 5.00 U 1.12 5.00 10.0 1 07/23/2022 13:44 WG1899773
2,4-Dinitrophenol 51-28-5 15.0 U 5.93 15.0 30.0 1 07/23/2022 13:44 WG1899773
2-Nitrophenol 88-75-5 5.00 J4 U 0.117 5.00 10.0 1 07/23/2022 13:44 WG1899773
4-Nitrophenol 100-02-7 5.00 U 0.143 5.00 10.0 1 07/23/2022 13:44 WG1899773
Pentachlorophenol 87-86-5 5.00 U 0.313 5.00 10.0 1 07/23/2022 13:44 WG1899773
Phenol 108-95-2 10.0 U 4.33 10.0 20.0 1 07/23/2022 13:44 WG1899773
2,4,6-Trichlorophenol 88-06-2 5.00 U 0.100 5.00 10.0 1 07/23/2022 13:44 WG1899773
1-Methylnaphthalene 90-12-0 0.286 J 0.0790 0.500 1.00 1 07/23/2022 13:44 WG1899773
2-Methylnaphthalene 91-57-6 0.500 U 0.117 0.500 1.00 1 07/23/2022 13:44 WG1899773
(S) Nitrobenzene-d5 4165-60-0 40.0 J2 0.000 44.0-120 07/23/2022 13:44 WG1899773
(S) 2-Fluorobiphenyl 321-60-8 36.7 J2 0.000 44.0-119 07/23/2022 13:44 WG1899773
(S) p-Terphenyl-d14 1718-51-0 37.0 J2 0.000 50.0-134 07/23/2022 13:44 WG1899773
(S) Phenol-d5 4165-62-2 14.0 0.000 10.0-67.0 07/23/2022 13:44 WG1899773
(S) 2-Fluorophenol 367-12-4 19.5 0.000 19.0-119 07/23/2022 13:44 WG1899773
(S) 2,4,6-Tribromophenol 118-79-6 42.2 J2 0.000 43.0-140 07/23/2022 13:44 WG1899773
Sample Narrative:
L1516722-04 WG1899773: Surrogate recovery within historical limits.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 15:39 18 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 16:01 18 of 65
====================----□ □ □ □
□ □ □ □
SAMPLE RESULTS - 05
L1516722
USTG480-MW27
Collected date/time: 07/18/22 10:52
Volatile Petroleum Hydrocarbons by Method MADEPV
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics C5-C8 ALI
UNADJ 60.4 J 33.3 67.0 100 1 07/23/2022 23:22 WG1899531
Unadjusted C9-C12 Aliphatics C9-C12 ALI
UNADJ 179 33.3 67.0 134 1 07/23/2022 23:22 WG1899531
Unadjusted C9-C10 Aromatics C9-C10 ARO
UNADJ 217 33.3 67.0 100 1 07/23/2022 23:22 WG1899531
Total VPH VPH 456 66.7 150 300 1 07/23/2022 23:22 WG1899531
(S) 2,5-Dibromotoluene(FID)615-59-8 122 70.0-130 07/23/2022 23:22 WG1899531
(S) 2,5-Dibromotoluene(PID)615-59-8 100 70.0-130 07/23/2022 23:22 WG1899531
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acetone 67-64-1 30.5 J 11.3 25.0 50.0 1 07/23/2022 14:09 WG1899800
Acrolein 107-02-8 25.0 U 2.54 25.0 50.0 1 07/23/2022 14:09 WG1899800
Acrylonitrile 107-13-1 5.00 U 0.671 5.00 10.0 1 07/23/2022 14:09 WG1899800
Benzene 71-43-2 0.372 J 0.0941 0.500 1.00 1 07/23/2022 14:09 WG1899800
Bromobenzene 108-86-1 0.500 C4 J4 U 0.118 0.500 1.00 1 07/23/2022 14:09 WG1899800
Bromodichloromethane 75-27-4 0.500 U 0.136 0.500 1.00 1 07/23/2022 14:09 WG1899800
Bromoform 75-25-2 0.500 U 0.129 0.500 1.00 1 07/23/2022 14:09 WG1899800
Bromomethane 74-83-9 2.00 U 0.605 2.00 5.00 1 07/23/2022 14:09 WG1899800
n-Butylbenzene 104-51-8 0.500 U 0.157 0.500 1.00 1 07/23/2022 14:09 WG1899800
sec-Butylbenzene 135-98-8 1.17 0.125 0.500 1.00 1 07/23/2022 14:09 WG1899800
tert-Butylbenzene 98-06-6 0.309 J 0.127 0.500 1.00 1 07/23/2022 14:09 WG1899800
Carbon tetrachloride 56-23-5 0.500 U 0.128 0.500 1.00 1 07/23/2022 14:09 WG1899800
Chlorobenzene 108-90-7 0.500 U 0.116 0.500 1.00 1 07/23/2022 14:09 WG1899800
Chlorodibromomethane 124-48-1 0.500 U 0.140 0.500 1.00 1 07/23/2022 14:09 WG1899800
Chloroethane 75-00-3 2.00 U 0.192 2.00 5.00 1 07/23/2022 14:09 WG1899800
Chloroform 67-66-3 2.00 U 0.111 2.00 5.00 1 07/23/2022 14:09 WG1899800
Chloromethane 74-87-3 2.00 U 0.960 2.00 4.00 1 07/23/2022 14:09 WG1899800
2-Chlorotoluene 95-49-8 0.500 U 0.106 0.500 1.00 1 07/23/2022 14:09 WG1899800
4-Chlorotoluene 106-43-4 0.500 U 0.114 0.500 1.00 1 07/23/2022 14:09 WG1899800
1,2-Dibromo-3-Chloropropane 96-12-8 2.00 U 0.276 2.00 5.00 1 07/23/2022 14:09 WG1899800
1,2-Dibromoethane 106-93-4 0.500 U 0.126 0.500 1.00 1 07/23/2022 14:09 WG1899800
Dibromomethane 74-95-3 0.500 U 0.122 0.500 1.00 1 07/23/2022 14:09 WG1899800
1,2-Dichlorobenzene 95-50-1 0.500 U 0.107 0.500 1.00 1 07/23/2022 14:09 WG1899800
1,3-Dichlorobenzene 541-73-1 0.500 U 0.110 0.500 1.00 1 07/23/2022 14:09 WG1899800
1,4-Dichlorobenzene 106-46-7 0.500 U 0.120 0.500 1.00 1 07/23/2022 14:09 WG1899800
Dichlorodifluoromethane 75-71-8 2.00 U 0.374 2.00 5.00 1 07/23/2022 14:09 WG1899800
1,1-Dichloroethane 75-34-3 0.500 U 0.100 0.500 1.00 1 07/23/2022 14:09 WG1899800
1,2-Dichloroethane 107-06-2 0.500 U 0.0819 0.500 1.00 1 07/23/2022 14:09 WG1899800
1,1-Dichloroethene 75-35-4 0.500 U 0.188 0.500 1.00 1 07/23/2022 14:09 WG1899800
cis-1,2-Dichloroethene 156-59-2 0.500 U 0.126 0.500 1.00 1 07/23/2022 14:09 WG1899800
trans-1,2-Dichloroethene 156-60-5 0.500 U 0.149 0.500 1.00 1 07/23/2022 14:09 WG1899800
1,2-Dichloropropane 78-87-5 0.500 U 0.149 0.500 1.00 1 07/23/2022 14:09 WG1899800
1,1-Dichloropropene 563-58-6 0.500 U 0.142 0.500 1.00 1 07/23/2022 14:09 WG1899800
1,3-Dichloropropane 142-28-9 0.500 U 0.110 0.500 1.00 1 07/23/2022 14:09 WG1899800
2,2-Dichloropropane 594-20-7 0.500 U 0.161 0.500 1.00 1 07/23/2022 14:09 WG1899800
Di-isopropyl ether 108-20-3 0.500 U 0.105 0.500 1.00 1 07/23/2022 14:09 WG1899800
Ethylbenzene 100-41-4 1.91 0.137 0.500 1.00 1 07/23/2022 14:09 WG1899800
Hexachloro-1,3-butadiene 87-68-3 0.750 U 0.337 0.750 1.50 1 07/23/2022 14:09 WG1899800
Isopropylbenzene 98-82-8 1.82 0.105 0.500 1.00 1 07/23/2022 14:09 WG1899800
p-Isopropyltoluene 99-87-6 5.41 0.120 0.500 1.00 1 07/23/2022 14:09 WG1899800
2-Butanone (MEK)78-93-3 2.29 J 1.19 5.00 10.0 1 07/23/2022 14:09 WG1899800
Methylene Chloride 75-09-2 2.00 U 0.430 2.00 5.00 1 07/23/2022 14:09 WG1899800
4-Methyl-2-pentanone (MIBK)108-10-1 5.00 U 0.478 5.00 10.0 1 07/23/2022 14:09 WG1899800
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 15:39 19 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 16:01 19 of 65
--------------=---□
□ □ □
==============~~~~~=----□ □ □ □
SAMPLE RESULTS - 05
L1516722
USTG480-MW27
Collected date/time: 07/18/22 10:52
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Methyl tert-butyl ether 1634-04-4 0.500 U 0.101 0.500 1.00 1 07/23/2022 14:09 WG1899800
Naphthalene 91-20-3 33.7 1.00 2.00 5.00 1 07/23/2022 14:09 WG1899800
n-Propylbenzene 103-65-1 2.25 C4 J4 0.0993 0.500 1.00 1 07/23/2022 14:09 WG1899800
Styrene 100-42-5 0.500 U 0.118 0.500 1.00 1 07/23/2022 14:09 WG1899800
1,1,1,2-Tetrachloroethane 630-20-6 0.500 U 0.147 0.500 1.00 1 07/23/2022 14:09 WG1899800
1,1,2,2-Tetrachloroethane 79-34-5 0.500 U 0.133 0.500 1.00 1 07/23/2022 14:09 WG1899800
Tetrachloroethene 127-18-4 0.600 U 0.300 0.600 1.20 1 07/23/2022 14:09 WG1899800
Toluene 108-88-3 1.01 J 0.278 0.600 1.20 1 07/23/2022 14:09 WG1899800
1,2,3-Trichlorobenzene 87-61-6 0.500 C4 U 0.230 0.500 1.00 1 07/23/2022 14:09 WG1899800
1,2,4-Trichlorobenzene 120-82-1 1.00 U 0.481 1.00 2.00 1 07/23/2022 14:09 WG1899800
1,1,1-Trichloroethane 71-55-6 0.500 U 0.149 0.500 1.00 1 07/23/2022 14:09 WG1899800
1,1,2-Trichloroethane 79-00-5 0.500 U 0.158 0.500 1.00 1 07/23/2022 14:09 WG1899800
Trichloroethene 79-01-6 0.500 U 0.190 0.500 1.00 1 07/23/2022 14:09 WG1899800
Trichlorofluoromethane 75-69-4 2.00 U 0.160 2.00 5.00 1 07/23/2022 14:09 WG1899800
1,2,3-Trichloropropane 96-18-4 1.00 U 0.237 1.00 2.50 1 07/23/2022 14:09 WG1899800
1,2,4-Trimethylbenzene 95-63-6 1.00 U 0.322 1.00 2.00 1 07/23/2022 14:09 WG1899800
1,3,5-Trimethylbenzene 108-67-8 0.155 J 0.104 0.500 1.00 1 07/23/2022 14:09 WG1899800
Vinyl chloride 75-01-4 0.500 U 0.234 0.500 1.00 1 07/23/2022 14:09 WG1899800
o-Xylene 95-47-6 0.500 U 0.174 0.500 1.00 1 07/23/2022 14:09 WG1899800
m&p-Xylenes 1330-20-7 1.00 U 0.430 1.00 2.00 1 07/23/2022 14:09 WG1899800
(S) Toluene-d8 2037-26-5 100 89.0-112 07/23/2022 14:09 WG1899800
(S) 4-Bromofluorobenzene 460-00-4 87.7 85.0-114 07/23/2022 14:09 WG1899800
(S) 1,2-Dichloroethane-d4 17060-07-0 92.2 81.0-118 07/23/2022 14:09 WG1899800
TPH by Method MADEPE
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics C9-C18 ALI
UNADJ 2000 33.3 67.0 134 1 08/01/2022 15:48 WG1902750
Unadjusted C19-C36 Aliphatics C19-C36 ALI
UNADJ 652 33.3 67.0 134 1 08/01/2022 15:48 WG1902750
Unadjusted C11-C22 Aromatics C11-C22 ARO
UNADJ 1100 33.3 67.0 134 1 08/01/2022 14:18 WG1902750
Unadjusted Total Petroleum
Hydrocarbons TPH UNADJ 3750 33.3 67.0 134 1 08/01/2022 15:48 WG1902750
(S) o-Terphenyl 84-15-1 78.0 40.0-140 08/01/2022 14:18 WG1902750
(S) 1-Chloro-octadecane 3386-33-2 60.3 40.0-140 08/01/2022 15:48 WG1902750
(S) 2-Fluorobiphenyl 321-60-8 89.2 40.0-140 08/01/2022 14:18 WG1902750
(S) 2-Bromonaphthalene 580-13-2 83.9 40.0-140 08/01/2022 14:18 WG1902750
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acenaphthene 83-32-9 1.60 J4 0.0886 0.500 1.00 1 07/27/2022 18:30 WG1899773
Acenaphthylene 208-96-8 0.500 U 0.0921 0.500 1.00 1 07/27/2022 18:30 WG1899773
Anthracene 120-12-7 0.500 J4 U 0.0804 0.500 1.00 1 07/27/2022 18:30 WG1899773
Benzidine 92-87-5 7.50 U 3.74 7.50 15.0 1 07/27/2022 18:30 WG1899773
Benzo(a)anthracene 56-55-3 0.500 U 0.199 0.500 1.00 1 07/27/2022 18:30 WG1899773
Benzo(b)fluoranthene 205-99-2 0.500 U 0.130 0.500 1.00 1 07/27/2022 18:30 WG1899773
Benzo(k)fluoranthene 207-08-9 0.500 U 0.120 0.500 1.00 1 07/27/2022 18:30 WG1899773
Benzo(g,h,i)perylene 191-24-2 0.500 U 0.121 0.500 1.00 1 07/27/2022 18:30 WG1899773
Benzo(a)pyrene 50-32-8 0.500 U 0.0381 0.500 1.00 1 07/27/2022 18:30 WG1899773
Bis(2-chlorethoxy)methane 111-91-1 5.00 J4 U 0.116 5.00 10.0 1 07/27/2022 18:30 WG1899773
Bis(2-chloroethyl)ether 111-44-4 5.00 J4 U 0.137 5.00 10.0 1 07/27/2022 18:30 WG1899773
2,2-Oxybis(1-Chloropropane)108-60-1 5.00 J4 U 0.210 5.00 10.0 1 07/27/2022 18:30 WG1899773
4-Bromophenyl-phenylether 101-55-3 5.00 U 0.0877 5.00 10.0 1 07/27/2022 18:30 WG1899773
2-Chloronaphthalene 91-58-7 0.500 U 0.0648 0.500 1.00 1 07/27/2022 18:30 WG1899773
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 15:39 20 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 16:01 20 of 65
====================----□ □ □ □
□ □ □ □
SAMPLE RESULTS - 05
L1516722
USTG480-MW27
Collected date/time: 07/18/22 10:52
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
4-Chlorophenyl-phenylether 7005-72-3 5.00 U 0.0926 5.00 10.0 1 07/27/2022 18:30 WG1899773
Chrysene 218-01-9 0.500 U 0.130 0.500 1.00 1 07/27/2022 18:30 WG1899773
Dibenz(a,h)anthracene 53-70-3 0.500 U 0.0644 0.500 1.00 1 07/27/2022 18:30 WG1899773
3,3-Dichlorobenzidine 91-94-1 5.00 U 0.212 5.00 10.0 1 07/27/2022 18:30 WG1899773
2,4-Dinitrotoluene 121-14-2 5.00 U 0.0983 5.00 10.0 1 07/27/2022 18:30 WG1899773
2,6-Dinitrotoluene 606-20-2 5.00 U 0.250 5.00 10.0 1 07/27/2022 18:30 WG1899773
Fluoranthene 206-44-0 0.167 J 0.102 0.500 1.00 1 07/27/2022 18:30 WG1899773
Fluorene 86-73-7 2.48 0.0844 0.500 1.00 1 07/27/2022 18:30 WG1899773
Hexachlorobenzene 118-74-1 0.500 U 0.0755 0.500 1.00 1 07/27/2022 18:30 WG1899773
Hexachloro-1,3-butadiene 87-68-3 5.00 U 0.0968 5.00 10.0 1 07/27/2022 18:30 WG1899773
Hexachlorocyclopentadiene 77-47-4 5.00 U 0.0598 5.00 10.0 1 07/27/2022 18:30 WG1899773
Hexachloroethane 67-72-1 5.00 U 0.127 5.00 10.0 1 07/27/2022 18:30 WG1899773
Indeno(1,2,3-cd)pyrene 193-39-5 0.600 U 0.279 0.600 1.20 1 07/27/2022 18:30 WG1899773
Isophorone 78-59-1 5.00 U 0.143 5.00 10.0 1 07/27/2022 18:30 WG1899773
Naphthalene 91-20-3 4.77 J4 0.159 0.500 1.00 1 07/27/2022 18:30 WG1899773
Nitrobenzene 98-95-3 5.00 J4 U 0.297 5.00 10.0 1 07/27/2022 18:30 WG1899773
n-Nitrosodimethylamine 62-75-9 5.00 U 0.998 5.00 10.0 1 07/27/2022 18:30 WG1899773
n-Nitrosodiphenylamine 86-30-6 5.00 J4 U 2.37 5.00 10.0 1 07/27/2022 18:30 WG1899773
n-Nitrosodi-n-propylamine 621-64-7 5.00 J4 U 0.261 5.00 10.0 1 07/27/2022 18:30 WG1899773
Phenanthrene 85-01-8 3.53 J4 0.112 0.500 1.00 1 07/27/2022 18:30 WG1899773
Benzylbutyl phthalate 85-68-7 2.00 U 0.765 2.00 4.00 1 07/27/2022 18:30 WG1899773
Bis(2-ethylhexyl)phthalate 117-81-7 22.9 0.895 2.00 4.00 1 07/27/2022 18:30 WG1899773
Di-n-butyl phthalate 84-74-2 1.50 U 0.453 1.50 3.00 1 07/27/2022 18:30 WG1899773
Diethyl phthalate 84-66-2 1.50 U 0.287 1.50 3.00 1 07/27/2022 18:30 WG1899773
Dimethyl phthalate 131-11-3 1.50 U 0.260 1.50 3.00 1 07/27/2022 18:30 WG1899773
Di-n-octyl phthalate 117-84-0 2.00 U 0.932 2.00 4.00 1 07/27/2022 18:30 WG1899773
Pyrene 129-00-0 0.337 J J4 0.107 0.500 1.00 1 07/27/2022 18:30 WG1899773
1,2,4-Trichlorobenzene 120-82-1 5.00 U 0.0698 5.00 10.0 1 07/27/2022 18:30 WG1899773
4-Chloro-3-methylphenol 59-50-7 5.00 U 0.131 5.00 10.0 1 07/27/2022 18:30 WG1899773
2-Chlorophenol 95-57-8 5.00 J4 U 0.133 5.00 10.0 1 07/27/2022 18:30 WG1899773
2,4-Dichlorophenol 120-83-2 5.00 J4 U 0.102 5.00 10.0 1 07/27/2022 18:30 WG1899773
2,4-Dimethylphenol 105-67-9 5.00 U 0.0636 5.00 10.0 1 07/27/2022 18:30 WG1899773
4,6-Dinitro-2-methylphenol 534-52-1 5.00 U 1.12 5.00 10.0 1 07/27/2022 18:30 WG1899773
2,4-Dinitrophenol 51-28-5 15.0 U 5.93 15.0 30.0 1 07/27/2022 18:30 WG1899773
2-Nitrophenol 88-75-5 5.00 J4 U 0.117 5.00 10.0 1 07/27/2022 18:30 WG1899773
4-Nitrophenol 100-02-7 5.00 U 0.143 5.00 10.0 1 07/27/2022 18:30 WG1899773
Pentachlorophenol 87-86-5 5.00 U 0.313 5.00 10.0 1 07/27/2022 18:30 WG1899773
Phenol 108-95-2 10.0 U 4.33 10.0 20.0 1 07/27/2022 18:30 WG1899773
2,4,6-Trichlorophenol 88-06-2 5.00 U 0.100 5.00 10.0 1 07/27/2022 18:30 WG1899773
1-Methylnaphthalene 90-12-0 16.4 0.0790 0.500 1.00 1 07/27/2022 18:30 WG1899773
2-Methylnaphthalene 91-57-6 13.4 0.117 0.500 1.00 1 07/27/2022 18:30 WG1899773
(S) Nitrobenzene-d5 4165-60-0 20.8 J2 0.000 44.0-120 07/27/2022 18:30 WG1899773
(S) 2-Fluorobiphenyl 321-60-8 32.5 J2 0.000 44.0-119 07/27/2022 18:30 WG1899773
(S) p-Terphenyl-d14 1718-51-0 55.2 0.000 50.0-134 07/27/2022 18:30 WG1899773
(S) Phenol-d5 4165-62-2 9.01 J2 0.000 10.0-67.0 07/27/2022 18:30 WG1899773
(S) 2-Fluorophenol 367-12-4 11.0 J2 0.000 19.0-119 07/27/2022 18:30 WG1899773
(S) 2,4,6-Tribromophenol 118-79-6 60.4 0.000 43.0-140 07/27/2022 18:30 WG1899773
Sample Narrative:
L1516722-05 WG1899773: Sample produced heavy emulsion during Extraction process, low surr/spike recoveries due to matrix
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 15:39 21 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 16:01 21 of 65
====================----□ □ □ □
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SAMPLE RESULTS - 06
L1516722
USTTC341-MW14R
Collected date/time: 07/18/22 11:16
Volatile Petroleum Hydrocarbons by Method MADEPV
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics C5-C8 ALI
UNADJ 670 U 333 670 1000 10 07/24/2022 02:06 WG1899531
Unadjusted C9-C12 Aliphatics C9-C12 ALI
UNADJ 522 J 333 670 1340 10 07/24/2022 02:06 WG1899531
Unadjusted C9-C10 Aromatics C9-C10 ARO
UNADJ 508 J 333 670 1000 10 07/24/2022 02:06 WG1899531
Total VPH VPH 1030 J 667 1500 3000 10 07/24/2022 02:06 WG1899531
(S) 2,5-Dibromotoluene(FID)615-59-8 113 70.0-130 07/24/2022 02:06 WG1899531
(S) 2,5-Dibromotoluene(PID)615-59-8 106 70.0-130 07/24/2022 02:06 WG1899531
Sample Narrative:
L1516722-06 WG1899531: Lowest possible dilution due to sample foaming.
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acetone 67-64-1 1590 113 250 500 10 07/23/2022 18:16 WG1899800
Acrolein 107-02-8 250 U 25.4 250 500 10 07/23/2022 18:16 WG1899800
Acrylonitrile 107-13-1 50.0 U 6.71 50.0 100 10 07/23/2022 18:16 WG1899800
Benzene 71-43-2 8.07 J 0.941 5.00 10.0 10 07/23/2022 18:16 WG1899800
Bromobenzene 108-86-1 5.00 C4 J4 U 1.18 5.00 10.0 10 07/23/2022 18:16 WG1899800
Bromodichloromethane 75-27-4 5.00 U 1.36 5.00 10.0 10 07/23/2022 18:16 WG1899800
Bromoform 75-25-2 5.00 U 1.29 5.00 10.0 10 07/23/2022 18:16 WG1899800
Bromomethane 74-83-9 20.0 U 6.05 20.0 50.0 10 07/23/2022 18:16 WG1899800
n-Butylbenzene 104-51-8 5.00 U 1.57 5.00 10.0 10 07/23/2022 18:16 WG1899800
sec-Butylbenzene 135-98-8 3.07 J 1.25 5.00 10.0 10 07/23/2022 18:16 WG1899800
tert-Butylbenzene 98-06-6 5.00 U 1.27 5.00 10.0 10 07/23/2022 18:16 WG1899800
Carbon tetrachloride 56-23-5 5.00 U 1.28 5.00 10.0 10 07/23/2022 18:16 WG1899800
Chlorobenzene 108-90-7 5.00 U 1.16 5.00 10.0 10 07/23/2022 18:16 WG1899800
Chlorodibromomethane 124-48-1 5.00 U 1.40 5.00 10.0 10 07/23/2022 18:16 WG1899800
Chloroethane 75-00-3 20.0 U 1.92 20.0 50.0 10 07/23/2022 18:16 WG1899800
Chloroform 67-66-3 20.0 U 1.11 20.0 50.0 10 07/23/2022 18:16 WG1899800
Chloromethane 74-87-3 20.0 U 9.60 20.0 40.0 10 07/23/2022 18:16 WG1899800
2-Chlorotoluene 95-49-8 5.00 U 1.06 5.00 10.0 10 07/23/2022 18:16 WG1899800
4-Chlorotoluene 106-43-4 5.00 U 1.14 5.00 10.0 10 07/23/2022 18:16 WG1899800
1,2-Dibromo-3-Chloropropane 96-12-8 20.0 U 2.76 20.0 50.0 10 07/23/2022 18:16 WG1899800
1,2-Dibromoethane 106-93-4 5.00 U 1.26 5.00 10.0 10 07/23/2022 18:16 WG1899800
Dibromomethane 74-95-3 5.00 U 1.22 5.00 10.0 10 07/23/2022 18:16 WG1899800
1,2-Dichlorobenzene 95-50-1 5.00 U 1.07 5.00 10.0 10 07/23/2022 18:16 WG1899800
1,3-Dichlorobenzene 541-73-1 5.00 U 1.10 5.00 10.0 10 07/23/2022 18:16 WG1899800
1,4-Dichlorobenzene 106-46-7 5.00 U 1.20 5.00 10.0 10 07/23/2022 18:16 WG1899800
Dichlorodifluoromethane 75-71-8 20.0 U 3.74 20.0 50.0 10 07/23/2022 18:16 WG1899800
1,1-Dichloroethane 75-34-3 5.00 U 1.00 5.00 10.0 10 07/23/2022 18:16 WG1899800
1,2-Dichloroethane 107-06-2 5.00 U 0.819 5.00 10.0 10 07/23/2022 18:16 WG1899800
1,1-Dichloroethene 75-35-4 5.00 U 1.88 5.00 10.0 10 07/23/2022 18:16 WG1899800
cis-1,2-Dichloroethene 156-59-2 5.00 U 1.26 5.00 10.0 10 07/23/2022 18:16 WG1899800
trans-1,2-Dichloroethene 156-60-5 5.00 U 1.49 5.00 10.0 10 07/23/2022 18:16 WG1899800
1,2-Dichloropropane 78-87-5 5.00 U 1.49 5.00 10.0 10 07/23/2022 18:16 WG1899800
1,1-Dichloropropene 563-58-6 5.00 U 1.42 5.00 10.0 10 07/23/2022 18:16 WG1899800
1,3-Dichloropropane 142-28-9 5.00 U 1.10 5.00 10.0 10 07/23/2022 18:16 WG1899800
2,2-Dichloropropane 594-20-7 5.00 U 1.61 5.00 10.0 10 07/23/2022 18:16 WG1899800
Di-isopropyl ether 108-20-3 5.00 U 1.05 5.00 10.0 10 07/23/2022 18:16 WG1899800
Ethylbenzene 100-41-4 20.5 1.37 5.00 10.0 10 07/27/2022 00:30 WG1901311
Hexachloro-1,3-butadiene 87-68-3 7.50 U 3.37 7.50 15.0 10 07/23/2022 18:16 WG1899800
Isopropylbenzene 98-82-8 15.2 1.05 5.00 10.0 10 07/23/2022 18:16 WG1899800
p-Isopropyltoluene 99-87-6 3.21 J 1.20 5.00 10.0 10 07/23/2022 18:16 WG1899800
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 15:39 22 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 16:01 22 of 65
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SAMPLE RESULTS - 06
L1516722
USTTC341-MW14R
Collected date/time: 07/18/22 11:16
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
2-Butanone (MEK)78-93-3 30.2 J 11.9 50.0 100 10 07/23/2022 18:16 WG1899800
Methylene Chloride 75-09-2 20.0 U 4.30 20.0 50.0 10 07/23/2022 18:16 WG1899800
4-Methyl-2-pentanone (MIBK)108-10-1 50.0 U 4.78 50.0 100 10 07/23/2022 18:16 WG1899800
Methyl tert-butyl ether 1634-04-4 5.00 U 1.01 5.00 10.0 10 07/23/2022 18:16 WG1899800
Naphthalene 91-20-3 145 10.0 20.0 50.0 10 07/23/2022 18:16 WG1899800
n-Propylbenzene 103-65-1 18.0 C4 J4 0.993 5.00 10.0 10 07/23/2022 18:16 WG1899800
Styrene 100-42-5 5.00 U 1.18 5.00 10.0 10 07/23/2022 18:16 WG1899800
1,1,1,2-Tetrachloroethane 630-20-6 5.00 U 1.47 5.00 10.0 10 07/23/2022 18:16 WG1899800
1,1,2,2-Tetrachloroethane 79-34-5 5.00 U 1.33 5.00 10.0 10 07/23/2022 18:16 WG1899800
Tetrachloroethene 127-18-4 6.00 U 3.00 6.00 12.0 10 07/23/2022 18:16 WG1899800
Toluene 108-88-3 6.00 U 2.78 6.00 12.0 10 07/23/2022 18:16 WG1899800
1,2,3-Trichlorobenzene 87-61-6 5.00 C4 U 2.30 5.00 10.0 10 07/23/2022 18:16 WG1899800
1,2,4-Trichlorobenzene 120-82-1 10.0 U 4.81 10.0 20.0 10 07/23/2022 18:16 WG1899800
1,1,1-Trichloroethane 71-55-6 5.00 U 1.49 5.00 10.0 10 07/23/2022 18:16 WG1899800
1,1,2-Trichloroethane 79-00-5 5.00 U 1.58 5.00 10.0 10 07/23/2022 18:16 WG1899800
Trichloroethene 79-01-6 5.00 U 1.90 5.00 10.0 10 07/23/2022 18:16 WG1899800
Trichlorofluoromethane 75-69-4 20.0 U 1.60 20.0 50.0 10 07/23/2022 18:16 WG1899800
1,2,3-Trichloropropane 96-18-4 10.0 U 2.37 10.0 25.0 10 07/23/2022 18:16 WG1899800
1,2,4-Trimethylbenzene 95-63-6 18.0 J 3.22 10.0 20.0 10 07/23/2022 18:16 WG1899800
1,3,5-Trimethylbenzene 108-67-8 5.00 U 1.04 5.00 10.0 10 07/23/2022 18:16 WG1899800
Vinyl chloride 75-01-4 5.00 U 2.34 5.00 10.0 10 07/23/2022 18:16 WG1899800
o-Xylene 95-47-6 5.00 U 1.74 5.00 10.0 10 07/23/2022 18:16 WG1899800
m&p-Xylenes 1330-20-7 16.0 J 4.30 10.0 20.0 10 07/23/2022 18:16 WG1899800
(S) Toluene-d8 2037-26-5 106 89.0-112 07/23/2022 18:16 WG1899800
(S) Toluene-d8 2037-26-5 104 89.0-112 07/27/2022 00:30 WG1901311
(S) 4-Bromofluorobenzene 460-00-4 86.9 85.0-114 07/23/2022 18:16 WG1899800
(S) 4-Bromofluorobenzene 460-00-4 106 85.0-114 07/27/2022 00:30 WG1901311
(S) 1,2-Dichloroethane-d4 17060-07-0 94.8 81.0-118 07/23/2022 18:16 WG1899800
(S) 1,2-Dichloroethane-d4 17060-07-0 103 81.0-118 07/27/2022 00:30 WG1901311
TPH by Method MADEPE
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics C9-C18 ALI
UNADJ 585 33.3 67.0 134 1 08/02/2022 12:53 WG1902750
Unadjusted C19-C36 Aliphatics C19-C36 ALI
UNADJ 186 B 33.3 67.0 134 1 08/02/2022 12:53 WG1902750
Unadjusted C11-C22 Aromatics C11-C22 ARO
UNADJ 1010 33.3 67.0 134 1 08/01/2022 13:55 WG1902750
Unadjusted Total Petroleum
Hydrocarbons TPH UNADJ 1780 33.3 67.0 134 1 08/01/2022 13:55 WG1902750
(S) o-Terphenyl 84-15-1 64.4 40.0-140 08/01/2022 13:55 WG1902750
(S) 1-Chloro-octadecane 3386-33-2 47.8 40.0-140 08/02/2022 12:53 WG1902750
(S) 2-Fluorobiphenyl 321-60-8 88.1 40.0-140 08/01/2022 13:55 WG1902750
(S) 2-Bromonaphthalene 580-13-2 82.4 40.0-140 08/01/2022 13:55 WG1902750
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acenaphthene 83-32-9 2.49 J J4 0.443 2.50 5.00 5 07/23/2022 15:35 WG1899773
Acenaphthylene 208-96-8 2.50 U 0.461 2.50 5.00 5 07/23/2022 15:35 WG1899773
Anthracene 120-12-7 2.50 J4 U 0.402 2.50 5.00 5 07/23/2022 15:35 WG1899773
Benzidine 92-87-5 37.5 U 18.7 37.5 75.0 5 07/23/2022 15:35 WG1899773
Benzo(a)anthracene 56-55-3 2.50 U 0.995 2.50 5.00 5 07/23/2022 15:35 WG1899773
Benzo(b)fluoranthene 205-99-2 2.50 U 0.650 2.50 5.00 5 07/23/2022 15:35 WG1899773
Benzo(k)fluoranthene 207-08-9 2.50 U 0.600 2.50 5.00 5 07/23/2022 15:35 WG1899773
Benzo(g,h,i)perylene 191-24-2 2.50 U 0.605 2.50 5.00 5 07/23/2022 15:35 WG1899773
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 15:39 23 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 16:01 23 of 65
====================----□ □ □ □
□ □ □ □
SAMPLE RESULTS - 06
L1516722
USTTC341-MW14R
Collected date/time: 07/18/22 11:16
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Benzo(a)pyrene 50-32-8 2.50 U 0.191 2.50 5.00 5 07/23/2022 15:35 WG1899773
Bis(2-chlorethoxy)methane 111-91-1 25.0 J4 U 0.580 25.0 50.0 5 07/23/2022 15:35 WG1899773
Bis(2-chloroethyl)ether 111-44-4 25.0 J4 U 0.685 25.0 50.0 5 07/23/2022 15:35 WG1899773
2,2-Oxybis(1-Chloropropane)108-60-1 25.0 J4 U 1.05 25.0 50.0 5 07/23/2022 15:35 WG1899773
4-Bromophenyl-phenylether 101-55-3 25.0 U 0.439 25.0 50.0 5 07/23/2022 15:35 WG1899773
2-Chloronaphthalene 91-58-7 2.50 U 0.324 2.50 5.00 5 07/23/2022 15:35 WG1899773
4-Chlorophenyl-phenylether 7005-72-3 25.0 U 0.463 25.0 50.0 5 07/23/2022 15:35 WG1899773
Chrysene 218-01-9 2.50 U 0.650 2.50 5.00 5 07/23/2022 15:35 WG1899773
Dibenz(a,h)anthracene 53-70-3 2.50 U 0.322 2.50 5.00 5 07/23/2022 15:35 WG1899773
3,3-Dichlorobenzidine 91-94-1 25.0 U 1.06 25.0 50.0 5 07/23/2022 15:35 WG1899773
2,4-Dinitrotoluene 121-14-2 25.0 U 0.491 25.0 50.0 5 07/23/2022 15:35 WG1899773
2,6-Dinitrotoluene 606-20-2 25.0 U 1.25 25.0 50.0 5 07/23/2022 15:35 WG1899773
Fluoranthene 206-44-0 2.50 U 0.510 2.50 5.00 5 07/23/2022 15:35 WG1899773
Fluorene 86-73-7 2.45 J 0.422 2.50 5.00 5 07/23/2022 15:35 WG1899773
Hexachlorobenzene 118-74-1 2.50 U 0.378 2.50 5.00 5 07/23/2022 15:35 WG1899773
Hexachloro-1,3-butadiene 87-68-3 25.0 U 0.484 25.0 50.0 5 07/23/2022 15:35 WG1899773
Hexachlorocyclopentadiene 77-47-4 25.0 U 0.299 25.0 50.0 5 07/23/2022 15:35 WG1899773
Hexachloroethane 67-72-1 25.0 U 0.635 25.0 50.0 5 07/23/2022 15:35 WG1899773
Indeno(1,2,3-cd)pyrene 193-39-5 3.00 U 1.40 3.00 6.00 5 07/23/2022 15:35 WG1899773
Isophorone 78-59-1 25.0 U 0.715 25.0 50.0 5 07/23/2022 15:35 WG1899773
Naphthalene 91-20-3 26.3 J4 0.795 2.50 5.00 5 07/23/2022 15:35 WG1899773
Nitrobenzene 98-95-3 25.0 J4 U 1.48 25.0 50.0 5 07/23/2022 15:35 WG1899773
n-Nitrosodimethylamine 62-75-9 25.0 U 4.99 25.0 50.0 5 07/23/2022 15:35 WG1899773
n-Nitrosodiphenylamine 86-30-6 25.0 J4 U 11.9 25.0 50.0 5 07/23/2022 15:35 WG1899773
n-Nitrosodi-n-propylamine 621-64-7 25.0 J4 U 1.31 25.0 50.0 5 07/23/2022 15:35 WG1899773
Phenanthrene 85-01-8 1.72 J J4 0.560 2.50 5.00 5 07/23/2022 15:35 WG1899773
Benzylbutyl phthalate 85-68-7 10.0 U 3.83 10.0 20.0 5 07/23/2022 15:35 WG1899773
Bis(2-ethylhexyl)phthalate 117-81-7 10.0 U 4.48 10.0 20.0 5 07/23/2022 15:35 WG1899773
Di-n-butyl phthalate 84-74-2 7.50 U 2.27 7.50 15.0 5 07/23/2022 15:35 WG1899773
Diethyl phthalate 84-66-2 7.50 U 1.43 7.50 15.0 5 07/23/2022 15:35 WG1899773
Dimethyl phthalate 131-11-3 7.50 U 1.30 7.50 15.0 5 07/23/2022 15:35 WG1899773
Di-n-octyl phthalate 117-84-0 10.0 U 4.66 10.0 20.0 5 07/23/2022 15:35 WG1899773
Pyrene 129-00-0 2.50 J4 U 0.535 2.50 5.00 5 07/23/2022 15:35 WG1899773
1,2,4-Trichlorobenzene 120-82-1 25.0 U 0.349 25.0 50.0 5 07/23/2022 15:35 WG1899773
4-Chloro-3-methylphenol 59-50-7 25.0 U 0.655 25.0 50.0 5 07/23/2022 15:35 WG1899773
2-Chlorophenol 95-57-8 25.0 J4 U 0.665 25.0 50.0 5 07/23/2022 15:35 WG1899773
2,4-Dichlorophenol 120-83-2 25.0 J4 U 0.510 25.0 50.0 5 07/23/2022 15:35 WG1899773
2,4-Dimethylphenol 105-67-9 25.0 U 0.318 25.0 50.0 5 07/23/2022 15:35 WG1899773
4,6-Dinitro-2-methylphenol 534-52-1 25.0 U 5.60 25.0 50.0 5 07/23/2022 15:35 WG1899773
2,4-Dinitrophenol 51-28-5 75.0 U 29.7 75.0 150 5 07/23/2022 15:35 WG1899773
2-Nitrophenol 88-75-5 25.0 J4 U 0.585 25.0 50.0 5 07/23/2022 15:35 WG1899773
4-Nitrophenol 100-02-7 25.0 U 0.715 25.0 50.0 5 07/23/2022 15:35 WG1899773
Pentachlorophenol 87-86-5 25.0 U 1.57 25.0 50.0 5 07/23/2022 15:35 WG1899773
Phenol 108-95-2 50.0 U 21.7 50.0 100 5 07/23/2022 15:35 WG1899773
2,4,6-Trichlorophenol 88-06-2 25.0 U 0.500 25.0 50.0 5 07/23/2022 15:35 WG1899773
1-Methylnaphthalene 90-12-0 25.8 0.395 2.50 5.00 5 07/23/2022 15:35 WG1899773
2-Methylnaphthalene 91-57-6 20.5 0.585 2.50 5.00 5 07/23/2022 15:35 WG1899773
(S) Nitrobenzene-d5 4165-60-0 28.8 J2 0.000 44.0-120 07/23/2022 15:35 WG1899773
(S) 2-Fluorobiphenyl 321-60-8 41.5 J2 0.000 44.0-119 07/23/2022 15:35 WG1899773
(S) p-Terphenyl-d14 1718-51-0 52.2 0.000 50.0-134 07/23/2022 15:35 WG1899773
(S) Phenol-d5 4165-62-2 12.1 0.000 10.0-67.0 07/23/2022 15:35 WG1899773
(S) 2-Fluorophenol 367-12-4 11.2 J2 0.000 19.0-119 07/23/2022 15:35 WG1899773
(S) 2,4,6-Tribromophenol 118-79-6 57.7 0.000 43.0-140 07/23/2022 15:35 WG1899773
Sample Narrative:
L1516722-06 WG1899773: Dilution due to matrix. Surrogate recovery within historical limits.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 15:39 24 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 16:01 24 of 65
====================----□ □ □ □
□ □ □ □
SAMPLE RESULTS - 07
L1516722
USTG480-MW02
Collected date/time: 07/18/22 11:48
Volatile Petroleum Hydrocarbons by Method MADEPV
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics C5-C8 ALI
UNADJ 518 J 333 670 1000 10 07/29/2022 19:20 WG1901087
Unadjusted C9-C12 Aliphatics C9-C12 ALI
UNADJ 1690 B 333 670 1340 10 07/29/2022 19:20 WG1901087
Unadjusted C9-C10 Aromatics C9-C10 ARO
UNADJ 1550 333 670 1000 10 07/29/2022 19:20 WG1901087
Total VPH VPH 3760 667 1500 3000 10 07/29/2022 19:20 WG1901087
(S) 2,5-Dibromotoluene(FID)615-59-8 91.1 70.0-130 07/29/2022 19:20 WG1901087
(S) 2,5-Dibromotoluene(PID)615-59-8 90.4 70.0-130 07/29/2022 19:20 WG1901087
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acetone 67-64-1 625 U 282 625 1250 25 07/23/2022 18:36 WG1899800
Acrolein 107-02-8 625 U 63.5 625 1250 25 07/23/2022 18:36 WG1899800
Acrylonitrile 107-13-1 125 U 16.8 125 250 25 07/23/2022 18:36 WG1899800
Benzene 71-43-2 169 2.35 12.5 25.0 25 07/23/2022 18:36 WG1899800
Bromobenzene 108-86-1 12.5 C4 J4 U 2.95 12.5 25.0 25 07/23/2022 18:36 WG1899800
Bromodichloromethane 75-27-4 12.5 U 3.40 12.5 25.0 25 07/23/2022 18:36 WG1899800
Bromoform 75-25-2 12.5 U 3.22 12.5 25.0 25 07/23/2022 18:36 WG1899800
Bromomethane 74-83-9 50.0 U 15.1 50.0 125 25 07/23/2022 18:36 WG1899800
n-Butylbenzene 104-51-8 12.5 U 3.93 12.5 25.0 25 07/23/2022 18:36 WG1899800
sec-Butylbenzene 135-98-8 11.0 J 3.13 12.5 25.0 25 07/23/2022 18:36 WG1899800
tert-Butylbenzene 98-06-6 12.5 U 3.18 12.5 25.0 25 07/23/2022 18:36 WG1899800
Carbon tetrachloride 56-23-5 12.5 U 3.20 12.5 25.0 25 07/23/2022 18:36 WG1899800
Chlorobenzene 108-90-7 12.5 U 2.90 12.5 25.0 25 07/23/2022 18:36 WG1899800
Chlorodibromomethane 124-48-1 12.5 U 3.50 12.5 25.0 25 07/23/2022 18:36 WG1899800
Chloroethane 75-00-3 50.0 U 4.80 50.0 125 25 07/23/2022 18:36 WG1899800
Chloroform 67-66-3 50.0 U 2.78 50.0 125 25 07/23/2022 18:36 WG1899800
Chloromethane 74-87-3 50.0 U 24.0 50.0 100 25 07/23/2022 18:36 WG1899800
2-Chlorotoluene 95-49-8 12.5 U 2.65 12.5 25.0 25 07/23/2022 18:36 WG1899800
4-Chlorotoluene 106-43-4 12.5 U 2.85 12.5 25.0 25 07/23/2022 18:36 WG1899800
1,2-Dibromo-3-Chloropropane 96-12-8 50.0 U 6.90 50.0 125 25 07/23/2022 18:36 WG1899800
1,2-Dibromoethane 106-93-4 12.5 U 3.15 12.5 25.0 25 07/23/2022 18:36 WG1899800
Dibromomethane 74-95-3 12.5 U 3.05 12.5 25.0 25 07/23/2022 18:36 WG1899800
1,2-Dichlorobenzene 95-50-1 12.5 U 2.68 12.5 25.0 25 07/23/2022 18:36 WG1899800
1,3-Dichlorobenzene 541-73-1 12.5 U 2.75 12.5 25.0 25 07/23/2022 18:36 WG1899800
1,4-Dichlorobenzene 106-46-7 12.5 U 3.00 12.5 25.0 25 07/23/2022 18:36 WG1899800
Dichlorodifluoromethane 75-71-8 50.0 U 9.35 50.0 125 25 07/23/2022 18:36 WG1899800
1,1-Dichloroethane 75-34-3 12.5 U 2.50 12.5 25.0 25 07/23/2022 18:36 WG1899800
1,2-Dichloroethane 107-06-2 12.5 U 2.05 12.5 25.0 25 07/23/2022 18:36 WG1899800
1,1-Dichloroethene 75-35-4 12.5 U 4.70 12.5 25.0 25 07/23/2022 18:36 WG1899800
cis-1,2-Dichloroethene 156-59-2 12.5 U 3.15 12.5 25.0 25 07/23/2022 18:36 WG1899800
trans-1,2-Dichloroethene 156-60-5 12.5 U 3.73 12.5 25.0 25 07/23/2022 18:36 WG1899800
1,2-Dichloropropane 78-87-5 12.5 U 3.73 12.5 25.0 25 07/23/2022 18:36 WG1899800
1,1-Dichloropropene 563-58-6 12.5 U 3.55 12.5 25.0 25 07/23/2022 18:36 WG1899800
1,3-Dichloropropane 142-28-9 12.5 U 2.75 12.5 25.0 25 07/23/2022 18:36 WG1899800
2,2-Dichloropropane 594-20-7 12.5 U 4.03 12.5 25.0 25 07/23/2022 18:36 WG1899800
Di-isopropyl ether 108-20-3 12.5 U 2.63 12.5 25.0 25 07/23/2022 18:36 WG1899800
Ethylbenzene 100-41-4 270 3.43 12.5 25.0 25 07/23/2022 18:36 WG1899800
Hexachloro-1,3-butadiene 87-68-3 18.8 U 8.43 18.8 37.5 25 07/23/2022 18:36 WG1899800
Isopropylbenzene 98-82-8 40.0 2.63 12.5 25.0 25 07/23/2022 18:36 WG1899800
p-Isopropyltoluene 99-87-6 22.5 J 3.00 12.5 25.0 25 07/23/2022 18:36 WG1899800
2-Butanone (MEK)78-93-3 125 U 29.8 125 250 25 07/23/2022 18:36 WG1899800
Methylene Chloride 75-09-2 50.0 U 10.7 50.0 125 25 07/23/2022 18:36 WG1899800
4-Methyl-2-pentanone (MIBK)108-10-1 125 U 12.0 125 250 25 07/23/2022 18:36 WG1899800
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 15:39 25 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 16:01 25 of 65
--------------=---□
□ □ □
==============~~~~~=----□ □ □ □
SAMPLE RESULTS - 07
L1516722
USTG480-MW02
Collected date/time: 07/18/22 11:48
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Methyl tert-butyl ether 1634-04-4 12.5 U 2.53 12.5 25.0 25 07/23/2022 18:36 WG1899800
Naphthalene 91-20-3 550 25.0 50.0 125 25 07/23/2022 18:36 WG1899800
n-Propylbenzene 103-65-1 50.5 C4 J4 2.48 12.5 25.0 25 07/23/2022 18:36 WG1899800
Styrene 100-42-5 12.5 U 2.95 12.5 25.0 25 07/23/2022 18:36 WG1899800
1,1,1,2-Tetrachloroethane 630-20-6 12.5 U 3.68 12.5 25.0 25 07/23/2022 18:36 WG1899800
1,1,2,2-Tetrachloroethane 79-34-5 12.5 U 3.33 12.5 25.0 25 07/23/2022 18:36 WG1899800
Tetrachloroethene 127-18-4 15.0 U 7.50 15.0 30.0 25 07/23/2022 18:36 WG1899800
Toluene 108-88-3 15.0 U 6.95 15.0 30.0 25 07/23/2022 18:36 WG1899800
1,2,3-Trichlorobenzene 87-61-6 12.5 C4 U 5.75 12.5 25.0 25 07/23/2022 18:36 WG1899800
1,2,4-Trichlorobenzene 120-82-1 25.0 U 12.0 25.0 50.0 25 07/23/2022 18:36 WG1899800
1,1,1-Trichloroethane 71-55-6 12.5 U 3.73 12.5 25.0 25 07/23/2022 18:36 WG1899800
1,1,2-Trichloroethane 79-00-5 12.5 U 3.95 12.5 25.0 25 07/23/2022 18:36 WG1899800
Trichloroethene 79-01-6 12.5 U 4.75 12.5 25.0 25 07/23/2022 18:36 WG1899800
Trichlorofluoromethane 75-69-4 50.0 U 4.00 50.0 125 25 07/23/2022 18:36 WG1899800
1,2,3-Trichloropropane 96-18-4 25.0 U 5.93 25.0 62.5 25 07/23/2022 18:36 WG1899800
1,2,4-Trimethylbenzene 95-63-6 286 8.05 25.0 50.0 25 07/23/2022 18:36 WG1899800
1,3,5-Trimethylbenzene 108-67-8 80.0 2.60 12.5 25.0 25 07/23/2022 18:36 WG1899800
Vinyl chloride 75-01-4 12.5 U 5.85 12.5 25.0 25 07/23/2022 18:36 WG1899800
o-Xylene 95-47-6 12.5 U 4.35 12.5 25.0 25 07/23/2022 18:36 WG1899800
m&p-Xylenes 1330-20-7 398 10.7 25.0 50.0 25 07/23/2022 18:36 WG1899800
(S) Toluene-d8 2037-26-5 105 89.0-112 07/23/2022 18:36 WG1899800
(S) 4-Bromofluorobenzene 460-00-4 87.1 85.0-114 07/23/2022 18:36 WG1899800
(S) 1,2-Dichloroethane-d4 17060-07-0 95.6 81.0-118 07/23/2022 18:36 WG1899800
TPH by Method MADEPE
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics C9-C18 ALI
UNADJ 106 J 33.3 67.0 134 1 08/01/2022 16:32 WG1902750
Unadjusted C19-C36 Aliphatics C19-C36 ALI
UNADJ 67.0 U 33.3 67.0 134 1 08/01/2022 16:32 WG1902750
Unadjusted C11-C22 Aromatics C11-C22 ARO
UNADJ 2360 33.3 67.0 134 1 08/01/2022 13:33 WG1902750
Unadjusted Total Petroleum
Hydrocarbons TPH UNADJ 2470 33.3 67.0 134 1 08/01/2022 16:32 WG1902750
(S) o-Terphenyl 84-15-1 83.3 40.0-140 08/01/2022 13:33 WG1902750
(S) 1-Chloro-octadecane 3386-33-2 73.3 40.0-140 08/01/2022 16:32 WG1902750
(S) 2-Fluorobiphenyl 321-60-8 91.8 40.0-140 08/01/2022 13:33 WG1902750
(S) 2-Bromonaphthalene 580-13-2 89.8 40.0-140 08/01/2022 13:33 WG1902750
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acenaphthene 83-32-9 1.82 J J4 0.443 2.50 5.00 5 07/23/2022 14:51 WG1899773
Acenaphthylene 208-96-8 2.50 U 0.461 2.50 5.00 5 07/23/2022 14:51 WG1899773
Anthracene 120-12-7 2.50 J4 U 0.402 2.50 5.00 5 07/23/2022 14:51 WG1899773
Benzidine 92-87-5 37.5 U 18.7 37.5 75.0 5 07/23/2022 14:51 WG1899773
Benzo(a)anthracene 56-55-3 2.50 U 0.995 2.50 5.00 5 07/23/2022 14:51 WG1899773
Benzo(b)fluoranthene 205-99-2 2.50 U 0.650 2.50 5.00 5 07/23/2022 14:51 WG1899773
Benzo(k)fluoranthene 207-08-9 2.50 U 0.600 2.50 5.00 5 07/23/2022 14:51 WG1899773
Benzo(g,h,i)perylene 191-24-2 2.50 U 0.605 2.50 5.00 5 07/23/2022 14:51 WG1899773
Benzo(a)pyrene 50-32-8 2.50 U 0.191 2.50 5.00 5 07/23/2022 14:51 WG1899773
Bis(2-chlorethoxy)methane 111-91-1 25.0 J4 U 0.580 25.0 50.0 5 07/23/2022 14:51 WG1899773
Bis(2-chloroethyl)ether 111-44-4 25.0 J4 U 0.685 25.0 50.0 5 07/23/2022 14:51 WG1899773
2,2-Oxybis(1-Chloropropane)108-60-1 25.0 J4 U 1.05 25.0 50.0 5 07/23/2022 14:51 WG1899773
4-Bromophenyl-phenylether 101-55-3 25.0 U 0.439 25.0 50.0 5 07/23/2022 14:51 WG1899773
2-Chloronaphthalene 91-58-7 2.50 U 0.324 2.50 5.00 5 07/23/2022 14:51 WG1899773
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 15:39 26 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 16:01 26 of 65
====================----□ □ □ □
□ □ □ □
SAMPLE RESULTS - 07
L1516722
USTG480-MW02
Collected date/time: 07/18/22 11:48
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
4-Chlorophenyl-phenylether 7005-72-3 25.0 U 0.463 25.0 50.0 5 07/23/2022 14:51 WG1899773
Chrysene 218-01-9 2.50 U 0.650 2.50 5.00 5 07/23/2022 14:51 WG1899773
Dibenz(a,h)anthracene 53-70-3 2.50 U 0.322 2.50 5.00 5 07/23/2022 14:51 WG1899773
3,3-Dichlorobenzidine 91-94-1 25.0 U 1.06 25.0 50.0 5 07/23/2022 14:51 WG1899773
2,4-Dinitrotoluene 121-14-2 25.0 U 0.491 25.0 50.0 5 07/23/2022 14:51 WG1899773
2,6-Dinitrotoluene 606-20-2 25.0 U 1.25 25.0 50.0 5 07/23/2022 14:51 WG1899773
Fluoranthene 206-44-0 2.50 U 0.510 2.50 5.00 5 07/23/2022 14:51 WG1899773
Fluorene 86-73-7 2.52 J 0.422 2.50 5.00 5 07/23/2022 14:51 WG1899773
Hexachlorobenzene 118-74-1 2.50 U 0.378 2.50 5.00 5 07/23/2022 14:51 WG1899773
Hexachloro-1,3-butadiene 87-68-3 25.0 U 0.484 25.0 50.0 5 07/23/2022 14:51 WG1899773
Hexachlorocyclopentadiene 77-47-4 25.0 U 0.299 25.0 50.0 5 07/23/2022 14:51 WG1899773
Hexachloroethane 67-72-1 25.0 U 0.635 25.0 50.0 5 07/23/2022 14:51 WG1899773
Indeno(1,2,3-cd)pyrene 193-39-5 3.00 U 1.40 3.00 6.00 5 07/23/2022 14:51 WG1899773
Isophorone 78-59-1 25.0 U 0.715 25.0 50.0 5 07/23/2022 14:51 WG1899773
Naphthalene 91-20-3 113 J4 0.795 2.50 5.00 5 07/23/2022 14:51 WG1899773
Nitrobenzene 98-95-3 25.0 J4 U 1.48 25.0 50.0 5 07/23/2022 14:51 WG1899773
n-Nitrosodimethylamine 62-75-9 6.22 J 4.99 25.0 50.0 5 07/23/2022 14:51 WG1899773
n-Nitrosodiphenylamine 86-30-6 25.0 J4 U 11.9 25.0 50.0 5 07/23/2022 14:51 WG1899773
n-Nitrosodi-n-propylamine 621-64-7 25.0 J4 U 1.31 25.0 50.0 5 07/23/2022 14:51 WG1899773
Phenanthrene 85-01-8 1.54 J J4 0.560 2.50 5.00 5 07/23/2022 14:51 WG1899773
Benzylbutyl phthalate 85-68-7 10.0 U 3.83 10.0 20.0 5 07/23/2022 14:51 WG1899773
Bis(2-ethylhexyl)phthalate 117-81-7 10.0 U 4.48 10.0 20.0 5 07/23/2022 14:51 WG1899773
Di-n-butyl phthalate 84-74-2 7.50 U 2.27 7.50 15.0 5 07/23/2022 14:51 WG1899773
Diethyl phthalate 84-66-2 7.50 U 1.43 7.50 15.0 5 07/23/2022 14:51 WG1899773
Dimethyl phthalate 131-11-3 7.50 U 1.30 7.50 15.0 5 07/23/2022 14:51 WG1899773
Di-n-octyl phthalate 117-84-0 10.0 U 4.66 10.0 20.0 5 07/23/2022 14:51 WG1899773
Pyrene 129-00-0 2.50 J4 U 0.535 2.50 5.00 5 07/23/2022 14:51 WG1899773
1,2,4-Trichlorobenzene 120-82-1 25.0 U 0.349 25.0 50.0 5 07/23/2022 14:51 WG1899773
4-Chloro-3-methylphenol 59-50-7 25.0 U 0.655 25.0 50.0 5 07/23/2022 14:51 WG1899773
2-Chlorophenol 95-57-8 25.0 J4 U 0.665 25.0 50.0 5 07/23/2022 14:51 WG1899773
2,4-Dichlorophenol 120-83-2 25.0 J4 U 0.510 25.0 50.0 5 07/23/2022 14:51 WG1899773
2,4-Dimethylphenol 105-67-9 25.0 U 0.318 25.0 50.0 5 07/23/2022 14:51 WG1899773
4,6-Dinitro-2-methylphenol 534-52-1 25.0 U 5.60 25.0 50.0 5 07/23/2022 14:51 WG1899773
2,4-Dinitrophenol 51-28-5 75.0 U 29.7 75.0 150 5 07/23/2022 14:51 WG1899773
2-Nitrophenol 88-75-5 25.0 J4 U 0.585 25.0 50.0 5 07/23/2022 14:51 WG1899773
4-Nitrophenol 100-02-7 25.0 U 0.715 25.0 50.0 5 07/23/2022 14:51 WG1899773
Pentachlorophenol 87-86-5 25.0 U 1.57 25.0 50.0 5 07/23/2022 14:51 WG1899773
Phenol 108-95-2 50.0 U 21.7 50.0 100 5 07/23/2022 14:51 WG1899773
2,4,6-Trichlorophenol 88-06-2 25.0 U 0.500 25.0 50.0 5 07/23/2022 14:51 WG1899773
1-Methylnaphthalene 90-12-0 75.8 0.395 2.50 5.00 5 07/23/2022 14:51 WG1899773
2-Methylnaphthalene 91-57-6 111 0.585 2.50 5.00 5 07/23/2022 14:51 WG1899773
(S) Nitrobenzene-d5 4165-60-0 23.2 J2 0.000 44.0-120 07/23/2022 14:51 WG1899773
(S) 2-Fluorobiphenyl 321-60-8 29.7 J2 0.000 44.0-119 07/23/2022 14:51 WG1899773
(S) p-Terphenyl-d14 1718-51-0 37.4 J2 0.000 50.0-134 07/23/2022 14:51 WG1899773
(S) Phenol-d5 4165-62-2 9.01 J2 0.000 10.0-67.0 07/23/2022 14:51 WG1899773
(S) 2-Fluorophenol 367-12-4 9.12 J2 0.000 19.0-119 07/23/2022 14:51 WG1899773
(S) 2,4,6-Tribromophenol 118-79-6 33.6 J2 0.000 43.0-140 07/23/2022 14:51 WG1899773
Sample Narrative:
L1516722-07 WG1899773: Sample produced emulsion during Extraction process, low surr/spike recoveries due to matrix.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 15:39 27 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 16:01 27 of 65
====================----□ □ □ □
□ □ □ □
SAMPLE RESULTS - 08
L1516722
USTTC341-MW08
Collected date/time: 07/18/22 12:05
Volatile Petroleum Hydrocarbons by Method MADEPV
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics C5-C8 ALI
UNADJ 67.0 U 33.3 67.0 100 1 07/23/2022 23:55 WG1899531
Unadjusted C9-C12 Aliphatics C9-C12 ALI
UNADJ 111 J 33.3 67.0 134 1 07/23/2022 23:55 WG1899531
Unadjusted C9-C10 Aromatics C9-C10 ARO
UNADJ 67.0 U 33.3 67.0 100 1 07/23/2022 23:55 WG1899531
Total VPH VPH 111 J 66.7 150 300 1 07/23/2022 23:55 WG1899531
(S) 2,5-Dibromotoluene(FID)615-59-8 110 70.0-130 07/23/2022 23:55 WG1899531
(S) 2,5-Dibromotoluene(PID)615-59-8 106 70.0-130 07/23/2022 23:55 WG1899531
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acetone 67-64-1 25.0 U 11.3 25.0 50.0 1 07/23/2022 14:30 WG1899800
Acrolein 107-02-8 25.0 U 2.54 25.0 50.0 1 07/23/2022 14:30 WG1899800
Acrylonitrile 107-13-1 5.00 U 0.671 5.00 10.0 1 07/23/2022 14:30 WG1899800
Benzene 71-43-2 0.500 U 0.0941 0.500 1.00 1 07/23/2022 14:30 WG1899800
Bromobenzene 108-86-1 0.500 C4 J4 U 0.118 0.500 1.00 1 07/23/2022 14:30 WG1899800
Bromodichloromethane 75-27-4 0.500 U 0.136 0.500 1.00 1 07/23/2022 14:30 WG1899800
Bromoform 75-25-2 0.500 U 0.129 0.500 1.00 1 07/23/2022 14:30 WG1899800
Bromomethane 74-83-9 2.00 U 0.605 2.00 5.00 1 07/23/2022 14:30 WG1899800
n-Butylbenzene 104-51-8 0.500 U 0.157 0.500 1.00 1 07/23/2022 14:30 WG1899800
sec-Butylbenzene 135-98-8 0.500 U 0.125 0.500 1.00 1 07/23/2022 14:30 WG1899800
tert-Butylbenzene 98-06-6 0.500 U 0.127 0.500 1.00 1 07/23/2022 14:30 WG1899800
Carbon tetrachloride 56-23-5 0.500 U 0.128 0.500 1.00 1 07/23/2022 14:30 WG1899800
Chlorobenzene 108-90-7 0.500 U 0.116 0.500 1.00 1 07/23/2022 14:30 WG1899800
Chlorodibromomethane 124-48-1 0.500 U 0.140 0.500 1.00 1 07/23/2022 14:30 WG1899800
Chloroethane 75-00-3 2.00 U 0.192 2.00 5.00 1 07/23/2022 14:30 WG1899800
Chloroform 67-66-3 2.00 U 0.111 2.00 5.00 1 07/23/2022 14:30 WG1899800
Chloromethane 74-87-3 2.00 U 0.960 2.00 4.00 1 07/23/2022 14:30 WG1899800
2-Chlorotoluene 95-49-8 0.500 U 0.106 0.500 1.00 1 07/23/2022 14:30 WG1899800
4-Chlorotoluene 106-43-4 0.500 U 0.114 0.500 1.00 1 07/23/2022 14:30 WG1899800
1,2-Dibromo-3-Chloropropane 96-12-8 2.00 U 0.276 2.00 5.00 1 07/23/2022 14:30 WG1899800
1,2-Dibromoethane 106-93-4 0.500 U 0.126 0.500 1.00 1 07/23/2022 14:30 WG1899800
Dibromomethane 74-95-3 0.500 U 0.122 0.500 1.00 1 07/23/2022 14:30 WG1899800
1,2-Dichlorobenzene 95-50-1 0.500 U 0.107 0.500 1.00 1 07/23/2022 14:30 WG1899800
1,3-Dichlorobenzene 541-73-1 0.500 U 0.110 0.500 1.00 1 07/23/2022 14:30 WG1899800
1,4-Dichlorobenzene 106-46-7 0.500 U 0.120 0.500 1.00 1 07/23/2022 14:30 WG1899800
Dichlorodifluoromethane 75-71-8 2.00 U 0.374 2.00 5.00 1 07/23/2022 14:30 WG1899800
1,1-Dichloroethane 75-34-3 0.500 U 0.100 0.500 1.00 1 07/23/2022 14:30 WG1899800
1,2-Dichloroethane 107-06-2 0.500 U 0.0819 0.500 1.00 1 07/23/2022 14:30 WG1899800
1,1-Dichloroethene 75-35-4 0.500 U 0.188 0.500 1.00 1 07/23/2022 14:30 WG1899800
cis-1,2-Dichloroethene 156-59-2 0.500 U 0.126 0.500 1.00 1 07/23/2022 14:30 WG1899800
trans-1,2-Dichloroethene 156-60-5 0.500 U 0.149 0.500 1.00 1 07/23/2022 14:30 WG1899800
1,2-Dichloropropane 78-87-5 0.500 U 0.149 0.500 1.00 1 07/23/2022 14:30 WG1899800
1,1-Dichloropropene 563-58-6 0.500 U 0.142 0.500 1.00 1 07/23/2022 14:30 WG1899800
1,3-Dichloropropane 142-28-9 0.500 U 0.110 0.500 1.00 1 07/23/2022 14:30 WG1899800
2,2-Dichloropropane 594-20-7 0.500 U 0.161 0.500 1.00 1 07/23/2022 14:30 WG1899800
Di-isopropyl ether 108-20-3 0.500 U 0.105 0.500 1.00 1 07/23/2022 14:30 WG1899800
Ethylbenzene 100-41-4 0.500 U 0.137 0.500 1.00 1 07/23/2022 14:30 WG1899800
Hexachloro-1,3-butadiene 87-68-3 0.750 U 0.337 0.750 1.50 1 07/23/2022 14:30 WG1899800
Isopropylbenzene 98-82-8 0.500 U 0.105 0.500 1.00 1 07/23/2022 14:30 WG1899800
p-Isopropyltoluene 99-87-6 0.500 U 0.120 0.500 1.00 1 07/23/2022 14:30 WG1899800
2-Butanone (MEK)78-93-3 5.00 U 1.19 5.00 10.0 1 07/23/2022 14:30 WG1899800
Methylene Chloride 75-09-2 2.00 U 0.430 2.00 5.00 1 07/23/2022 14:30 WG1899800
4-Methyl-2-pentanone (MIBK)108-10-1 5.00 U 0.478 5.00 10.0 1 07/23/2022 14:30 WG1899800
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 15:39 28 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 16:01 28 of 65
--------------=---□
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SAMPLE RESULTS - 08
L1516722
USTTC341-MW08
Collected date/time: 07/18/22 12:05
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Methyl tert-butyl ether 1634-04-4 0.500 U 0.101 0.500 1.00 1 07/23/2022 14:30 WG1899800
Naphthalene 91-20-3 1.27 J 1.00 2.00 5.00 1 07/23/2022 14:30 WG1899800
n-Propylbenzene 103-65-1 0.500 C4 J4 U 0.0993 0.500 1.00 1 07/23/2022 14:30 WG1899800
Styrene 100-42-5 0.500 U 0.118 0.500 1.00 1 07/23/2022 14:30 WG1899800
1,1,1,2-Tetrachloroethane 630-20-6 0.500 U 0.147 0.500 1.00 1 07/23/2022 14:30 WG1899800
1,1,2,2-Tetrachloroethane 79-34-5 0.500 U 0.133 0.500 1.00 1 07/23/2022 14:30 WG1899800
Tetrachloroethene 127-18-4 0.600 U 0.300 0.600 1.20 1 07/23/2022 14:30 WG1899800
Toluene 108-88-3 0.600 U 0.278 0.600 1.20 1 07/23/2022 14:30 WG1899800
1,2,3-Trichlorobenzene 87-61-6 0.500 C4 U 0.230 0.500 1.00 1 07/23/2022 14:30 WG1899800
1,2,4-Trichlorobenzene 120-82-1 1.00 U 0.481 1.00 2.00 1 07/23/2022 14:30 WG1899800
1,1,1-Trichloroethane 71-55-6 0.500 U 0.149 0.500 1.00 1 07/23/2022 14:30 WG1899800
1,1,2-Trichloroethane 79-00-5 0.500 U 0.158 0.500 1.00 1 07/23/2022 14:30 WG1899800
Trichloroethene 79-01-6 0.500 U 0.190 0.500 1.00 1 07/23/2022 14:30 WG1899800
Trichlorofluoromethane 75-69-4 2.00 U 0.160 2.00 5.00 1 07/23/2022 14:30 WG1899800
1,2,3-Trichloropropane 96-18-4 1.00 U 0.237 1.00 2.50 1 07/23/2022 14:30 WG1899800
1,2,4-Trimethylbenzene 95-63-6 1.00 U 0.322 1.00 2.00 1 07/23/2022 14:30 WG1899800
1,3,5-Trimethylbenzene 108-67-8 0.500 U 0.104 0.500 1.00 1 07/23/2022 14:30 WG1899800
Vinyl chloride 75-01-4 0.500 U 0.234 0.500 1.00 1 07/23/2022 14:30 WG1899800
o-Xylene 95-47-6 0.500 U 0.174 0.500 1.00 1 07/23/2022 14:30 WG1899800
m&p-Xylenes 1330-20-7 1.00 U 0.430 1.00 2.00 1 07/23/2022 14:30 WG1899800
(S) Toluene-d8 2037-26-5 103 89.0-112 07/23/2022 14:30 WG1899800
(S) 4-Bromofluorobenzene 460-00-4 90.1 85.0-114 07/23/2022 14:30 WG1899800
(S) 1,2-Dichloroethane-d4 17060-07-0 97.3 81.0-118 07/23/2022 14:30 WG1899800
TPH by Method MADEPE
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics C9-C18 ALI
UNADJ 67.0 U 33.3 67.0 134 1 08/01/2022 16:55 WG1902750
Unadjusted C19-C36 Aliphatics C19-C36 ALI
UNADJ 115 B J 33.3 67.0 134 1 08/01/2022 16:55 WG1902750
Unadjusted C11-C22 Aromatics C11-C22 ARO
UNADJ 62.2 B J 33.3 67.0 134 1 08/01/2022 13:11 WG1902750
Unadjusted Total Petroleum
Hydrocarbons TPH UNADJ 177 B 33.3 67.0 134 1 08/01/2022 16:55 WG1902750
(S) o-Terphenyl 84-15-1 71.5 40.0-140 08/01/2022 13:11 WG1902750
(S) 1-Chloro-octadecane 3386-33-2 59.9 40.0-140 08/01/2022 16:55 WG1902750
(S) 2-Fluorobiphenyl 321-60-8 90.6 40.0-140 08/01/2022 13:11 WG1902750
(S) 2-Bromonaphthalene 580-13-2 87.4 40.0-140 08/01/2022 13:11 WG1902750
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acenaphthene 83-32-9 0.500 J4 U 0.0886 0.500 1.00 1 07/23/2022 18:10 WG1899773
Acenaphthylene 208-96-8 0.500 U 0.0921 0.500 1.00 1 07/23/2022 18:10 WG1899773
Anthracene 120-12-7 0.500 J4 U 0.0804 0.500 1.00 1 07/23/2022 18:10 WG1899773
Benzidine 92-87-5 7.50 U 3.74 7.50 15.0 1 07/23/2022 18:10 WG1899773
Benzo(a)anthracene 56-55-3 0.500 U 0.199 0.500 1.00 1 07/23/2022 18:10 WG1899773
Benzo(b)fluoranthene 205-99-2 0.500 U 0.130 0.500 1.00 1 07/23/2022 18:10 WG1899773
Benzo(k)fluoranthene 207-08-9 0.500 U 0.120 0.500 1.00 1 07/23/2022 18:10 WG1899773
Benzo(g,h,i)perylene 191-24-2 0.500 U 0.121 0.500 1.00 1 07/23/2022 18:10 WG1899773
Benzo(a)pyrene 50-32-8 0.500 U 0.0381 0.500 1.00 1 07/23/2022 18:10 WG1899773
Bis(2-chlorethoxy)methane 111-91-1 5.00 J4 U 0.116 5.00 10.0 1 07/23/2022 18:10 WG1899773
Bis(2-chloroethyl)ether 111-44-4 5.00 J4 U 0.137 5.00 10.0 1 07/23/2022 18:10 WG1899773
2,2-Oxybis(1-Chloropropane)108-60-1 5.00 J4 U 0.210 5.00 10.0 1 07/23/2022 18:10 WG1899773
4-Bromophenyl-phenylether 101-55-3 5.00 U 0.0877 5.00 10.0 1 07/23/2022 18:10 WG1899773
2-Chloronaphthalene 91-58-7 0.500 U 0.0648 0.500 1.00 1 07/23/2022 18:10 WG1899773
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 15:39 29 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 16:01 29 of 65
====================----□ □ □ □
□ □ □ □
SAMPLE RESULTS - 08
L1516722
USTTC341-MW08
Collected date/time: 07/18/22 12:05
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
4-Chlorophenyl-phenylether 7005-72-3 5.00 U 0.0926 5.00 10.0 1 07/23/2022 18:10 WG1899773
Chrysene 218-01-9 0.500 U 0.130 0.500 1.00 1 07/23/2022 18:10 WG1899773
Dibenz(a,h)anthracene 53-70-3 0.500 U 0.0644 0.500 1.00 1 07/23/2022 18:10 WG1899773
3,3-Dichlorobenzidine 91-94-1 5.00 U 0.212 5.00 10.0 1 07/23/2022 18:10 WG1899773
2,4-Dinitrotoluene 121-14-2 5.00 U 0.0983 5.00 10.0 1 07/23/2022 18:10 WG1899773
2,6-Dinitrotoluene 606-20-2 5.00 U 0.250 5.00 10.0 1 07/23/2022 18:10 WG1899773
Fluoranthene 206-44-0 0.500 U 0.102 0.500 1.00 1 07/23/2022 18:10 WG1899773
Fluorene 86-73-7 0.500 U 0.0844 0.500 1.00 1 07/23/2022 18:10 WG1899773
Hexachlorobenzene 118-74-1 0.500 U 0.0755 0.500 1.00 1 07/23/2022 18:10 WG1899773
Hexachloro-1,3-butadiene 87-68-3 5.00 U 0.0968 5.00 10.0 1 07/23/2022 18:10 WG1899773
Hexachlorocyclopentadiene 77-47-4 5.00 U 0.0598 5.00 10.0 1 07/23/2022 18:10 WG1899773
Hexachloroethane 67-72-1 5.00 U 0.127 5.00 10.0 1 07/23/2022 18:10 WG1899773
Indeno(1,2,3-cd)pyrene 193-39-5 0.600 U 0.279 0.600 1.20 1 07/23/2022 18:10 WG1899773
Isophorone 78-59-1 5.00 U 0.143 5.00 10.0 1 07/23/2022 18:10 WG1899773
Naphthalene 91-20-3 0.500 J4 U 0.159 0.500 1.00 1 07/23/2022 18:10 WG1899773
Nitrobenzene 98-95-3 5.00 J4 U 0.297 5.00 10.0 1 07/23/2022 18:10 WG1899773
n-Nitrosodimethylamine 62-75-9 5.00 U 0.998 5.00 10.0 1 07/23/2022 18:10 WG1899773
n-Nitrosodiphenylamine 86-30-6 5.00 J4 U 2.37 5.00 10.0 1 07/23/2022 18:10 WG1899773
n-Nitrosodi-n-propylamine 621-64-7 5.00 J4 U 0.261 5.00 10.0 1 07/23/2022 18:10 WG1899773
Phenanthrene 85-01-8 0.500 J4 U 0.112 0.500 1.00 1 07/23/2022 18:10 WG1899773
Benzylbutyl phthalate 85-68-7 2.00 U 0.765 2.00 4.00 1 07/23/2022 18:10 WG1899773
Bis(2-ethylhexyl)phthalate 117-81-7 2.00 U 0.895 2.00 4.00 1 07/23/2022 18:10 WG1899773
Di-n-butyl phthalate 84-74-2 1.50 U 0.453 1.50 3.00 1 07/23/2022 18:10 WG1899773
Diethyl phthalate 84-66-2 1.50 U 0.287 1.50 3.00 1 07/23/2022 18:10 WG1899773
Dimethyl phthalate 131-11-3 1.50 U 0.260 1.50 3.00 1 07/23/2022 18:10 WG1899773
Di-n-octyl phthalate 117-84-0 2.00 U 0.932 2.00 4.00 1 07/23/2022 18:10 WG1899773
Pyrene 129-00-0 0.500 J4 U 0.107 0.500 1.00 1 07/23/2022 18:10 WG1899773
1,2,4-Trichlorobenzene 120-82-1 5.00 U 0.0698 5.00 10.0 1 07/23/2022 18:10 WG1899773
4-Chloro-3-methylphenol 59-50-7 5.00 U 0.131 5.00 10.0 1 07/23/2022 18:10 WG1899773
2-Chlorophenol 95-57-8 5.00 J4 U 0.133 5.00 10.0 1 07/23/2022 18:10 WG1899773
2,4-Dichlorophenol 120-83-2 5.00 J4 U 0.102 5.00 10.0 1 07/23/2022 18:10 WG1899773
2,4-Dimethylphenol 105-67-9 5.00 U 0.0636 5.00 10.0 1 07/23/2022 18:10 WG1899773
4,6-Dinitro-2-methylphenol 534-52-1 5.00 U 1.12 5.00 10.0 1 07/23/2022 18:10 WG1899773
2,4-Dinitrophenol 51-28-5 15.0 U 5.93 15.0 30.0 1 07/23/2022 18:10 WG1899773
2-Nitrophenol 88-75-5 5.00 J4 U 0.117 5.00 10.0 1 07/23/2022 18:10 WG1899773
4-Nitrophenol 100-02-7 5.00 U 0.143 5.00 10.0 1 07/23/2022 18:10 WG1899773
Pentachlorophenol 87-86-5 5.00 U 0.313 5.00 10.0 1 07/23/2022 18:10 WG1899773
Phenol 108-95-2 10.0 U 4.33 10.0 20.0 1 07/23/2022 18:10 WG1899773
2,4,6-Trichlorophenol 88-06-2 5.00 U 0.100 5.00 10.0 1 07/23/2022 18:10 WG1899773
1-Methylnaphthalene 90-12-0 0.500 U 0.0790 0.500 1.00 1 07/23/2022 18:10 WG1899773
2-Methylnaphthalene 91-57-6 0.500 U 0.117 0.500 1.00 1 07/23/2022 18:10 WG1899773
(S) Nitrobenzene-d5 4165-60-0 12.7 J2 0.000 44.0-120 07/23/2022 18:10 WG1899773
(S) 2-Fluorobiphenyl 321-60-8 13.7 J2 0.000 44.0-119 07/23/2022 18:10 WG1899773
(S) p-Terphenyl-d14 1718-51-0 53.1 0.000 50.0-134 07/23/2022 18:10 WG1899773
(S) Phenol-d5 4165-62-2 8.35 J2 0.000 10.0-67.0 07/23/2022 18:10 WG1899773
(S) 2-Fluorophenol 367-12-4 9.62 J2 0.000 19.0-119 07/23/2022 18:10 WG1899773
(S) 2,4,6-Tribromophenol 118-79-6 49.5 0.000 43.0-140 07/23/2022 18:10 WG1899773
Sample Narrative:
L1516722-08 WG1899773: Duplicate Analysis performed due to surrogate failure. Results confirm; reporting in hold data
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 15:39 30 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 16:01 30 of 65
====================----□ □ □ □
□ □ □ □
SAMPLE RESULTS - 09
L1516722
USTG480-MW25
Collected date/time: 07/18/22 12:51
Volatile Petroleum Hydrocarbons by Method MADEPV
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics C5-C8 ALI
UNADJ 67.0 U 33.3 67.0 100 1 07/24/2022 00:27 WG1899531
Unadjusted C9-C12 Aliphatics C9-C12 ALI
UNADJ 58.3 J 33.3 67.0 134 1 07/24/2022 00:27 WG1899531
Unadjusted C9-C10 Aromatics C9-C10 ARO
UNADJ 67.0 U 33.3 67.0 100 1 07/24/2022 00:27 WG1899531
Total VPH VPH 150 U 66.7 150 300 1 07/24/2022 00:27 WG1899531
(S) 2,5-Dibromotoluene(FID)615-59-8 108 70.0-130 07/24/2022 00:27 WG1899531
(S) 2,5-Dibromotoluene(PID)615-59-8 106 70.0-130 07/24/2022 00:27 WG1899531
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acetone 67-64-1 25.0 U 11.3 25.0 50.0 1 07/23/2022 14:50 WG1899800
Acrolein 107-02-8 25.0 U 2.54 25.0 50.0 1 07/23/2022 14:50 WG1899800
Acrylonitrile 107-13-1 5.00 U 0.671 5.00 10.0 1 07/23/2022 14:50 WG1899800
Benzene 71-43-2 1.10 0.0941 0.500 1.00 1 07/23/2022 14:50 WG1899800
Bromobenzene 108-86-1 0.500 C4 J4 U 0.118 0.500 1.00 1 07/23/2022 14:50 WG1899800
Bromodichloromethane 75-27-4 0.500 U 0.136 0.500 1.00 1 07/23/2022 14:50 WG1899800
Bromoform 75-25-2 0.500 U 0.129 0.500 1.00 1 07/23/2022 14:50 WG1899800
Bromomethane 74-83-9 2.00 U 0.605 2.00 5.00 1 07/23/2022 14:50 WG1899800
n-Butylbenzene 104-51-8 0.500 U 0.157 0.500 1.00 1 07/23/2022 14:50 WG1899800
sec-Butylbenzene 135-98-8 0.500 U 0.125 0.500 1.00 1 07/23/2022 14:50 WG1899800
tert-Butylbenzene 98-06-6 0.500 U 0.127 0.500 1.00 1 07/23/2022 14:50 WG1899800
Carbon tetrachloride 56-23-5 0.500 U 0.128 0.500 1.00 1 07/23/2022 14:50 WG1899800
Chlorobenzene 108-90-7 0.500 U 0.116 0.500 1.00 1 07/23/2022 14:50 WG1899800
Chlorodibromomethane 124-48-1 0.500 U 0.140 0.500 1.00 1 07/23/2022 14:50 WG1899800
Chloroethane 75-00-3 2.00 U 0.192 2.00 5.00 1 07/23/2022 14:50 WG1899800
Chloroform 67-66-3 2.00 U 0.111 2.00 5.00 1 07/23/2022 14:50 WG1899800
Chloromethane 74-87-3 2.00 U 0.960 2.00 4.00 1 07/23/2022 14:50 WG1899800
2-Chlorotoluene 95-49-8 0.500 U 0.106 0.500 1.00 1 07/23/2022 14:50 WG1899800
4-Chlorotoluene 106-43-4 0.500 U 0.114 0.500 1.00 1 07/23/2022 14:50 WG1899800
1,2-Dibromo-3-Chloropropane 96-12-8 2.00 U 0.276 2.00 5.00 1 07/23/2022 14:50 WG1899800
1,2-Dibromoethane 106-93-4 0.500 U 0.126 0.500 1.00 1 07/23/2022 14:50 WG1899800
Dibromomethane 74-95-3 0.500 U 0.122 0.500 1.00 1 07/23/2022 14:50 WG1899800
1,2-Dichlorobenzene 95-50-1 0.500 U 0.107 0.500 1.00 1 07/23/2022 14:50 WG1899800
1,3-Dichlorobenzene 541-73-1 0.500 U 0.110 0.500 1.00 1 07/23/2022 14:50 WG1899800
1,4-Dichlorobenzene 106-46-7 0.500 U 0.120 0.500 1.00 1 07/23/2022 14:50 WG1899800
Dichlorodifluoromethane 75-71-8 2.00 U 0.374 2.00 5.00 1 07/23/2022 14:50 WG1899800
1,1-Dichloroethane 75-34-3 0.500 U 0.100 0.500 1.00 1 07/23/2022 14:50 WG1899800
1,2-Dichloroethane 107-06-2 0.500 U 0.0819 0.500 1.00 1 07/23/2022 14:50 WG1899800
1,1-Dichloroethene 75-35-4 0.500 U 0.188 0.500 1.00 1 07/23/2022 14:50 WG1899800
cis-1,2-Dichloroethene 156-59-2 1.68 0.126 0.500 1.00 1 07/23/2022 14:50 WG1899800
trans-1,2-Dichloroethene 156-60-5 1.70 0.149 0.500 1.00 1 07/23/2022 14:50 WG1899800
1,2-Dichloropropane 78-87-5 0.500 U 0.149 0.500 1.00 1 07/23/2022 14:50 WG1899800
1,1-Dichloropropene 563-58-6 0.500 U 0.142 0.500 1.00 1 07/23/2022 14:50 WG1899800
1,3-Dichloropropane 142-28-9 0.500 U 0.110 0.500 1.00 1 07/23/2022 14:50 WG1899800
2,2-Dichloropropane 594-20-7 0.500 U 0.161 0.500 1.00 1 07/23/2022 14:50 WG1899800
Di-isopropyl ether 108-20-3 5.69 0.105 0.500 1.00 1 07/23/2022 14:50 WG1899800
Ethylbenzene 100-41-4 0.578 J 0.137 0.500 1.00 1 07/23/2022 14:50 WG1899800
Hexachloro-1,3-butadiene 87-68-3 0.750 U 0.337 0.750 1.50 1 07/23/2022 14:50 WG1899800
Isopropylbenzene 98-82-8 0.500 U 0.105 0.500 1.00 1 07/23/2022 14:50 WG1899800
p-Isopropyltoluene 99-87-6 0.500 U 0.120 0.500 1.00 1 07/23/2022 14:50 WG1899800
2-Butanone (MEK)78-93-3 5.00 U 1.19 5.00 10.0 1 07/23/2022 14:50 WG1899800
Methylene Chloride 75-09-2 2.00 U 0.430 2.00 5.00 1 07/23/2022 14:50 WG1899800
4-Methyl-2-pentanone (MIBK)108-10-1 5.00 U 0.478 5.00 10.0 1 07/23/2022 14:50 WG1899800
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 15:39 31 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 16:01 31 of 65
--------------=---□
□ □ □
==============~~~~~=----□ □ □ □
SAMPLE RESULTS - 09
L1516722
USTG480-MW25
Collected date/time: 07/18/22 12:51
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Methyl tert-butyl ether 1634-04-4 0.500 U 0.101 0.500 1.00 1 07/23/2022 14:50 WG1899800
Naphthalene 91-20-3 1.33 J 1.00 2.00 5.00 1 07/23/2022 14:50 WG1899800
n-Propylbenzene 103-65-1 0.408 C4 J J4 0.0993 0.500 1.00 1 07/23/2022 14:50 WG1899800
Styrene 100-42-5 0.500 U 0.118 0.500 1.00 1 07/23/2022 14:50 WG1899800
1,1,1,2-Tetrachloroethane 630-20-6 0.500 U 0.147 0.500 1.00 1 07/23/2022 14:50 WG1899800
1,1,2,2-Tetrachloroethane 79-34-5 0.500 U 0.133 0.500 1.00 1 07/23/2022 14:50 WG1899800
Tetrachloroethene 127-18-4 0.600 U 0.300 0.600 1.20 1 07/23/2022 14:50 WG1899800
Toluene 108-88-3 0.600 U 0.278 0.600 1.20 1 07/23/2022 14:50 WG1899800
1,2,3-Trichlorobenzene 87-61-6 0.500 C4 U 0.230 0.500 1.00 1 07/23/2022 14:50 WG1899800
1,2,4-Trichlorobenzene 120-82-1 1.00 U 0.481 1.00 2.00 1 07/23/2022 14:50 WG1899800
1,1,1-Trichloroethane 71-55-6 0.500 U 0.149 0.500 1.00 1 07/23/2022 14:50 WG1899800
1,1,2-Trichloroethane 79-00-5 0.500 U 0.158 0.500 1.00 1 07/23/2022 14:50 WG1899800
Trichloroethene 79-01-6 0.500 U 0.190 0.500 1.00 1 07/23/2022 14:50 WG1899800
Trichlorofluoromethane 75-69-4 2.00 U 0.160 2.00 5.00 1 07/23/2022 14:50 WG1899800
1,2,3-Trichloropropane 96-18-4 1.00 U 0.237 1.00 2.50 1 07/23/2022 14:50 WG1899800
1,2,4-Trimethylbenzene 95-63-6 0.374 J 0.322 1.00 2.00 1 07/23/2022 14:50 WG1899800
1,3,5-Trimethylbenzene 108-67-8 0.116 J 0.104 0.500 1.00 1 07/23/2022 14:50 WG1899800
Vinyl chloride 75-01-4 16.2 0.234 0.500 1.00 1 07/23/2022 14:50 WG1899800
o-Xylene 95-47-6 0.500 U 0.174 0.500 1.00 1 07/23/2022 14:50 WG1899800
m&p-Xylenes 1330-20-7 0.679 J 0.430 1.00 2.00 1 07/23/2022 14:50 WG1899800
(S) Toluene-d8 2037-26-5 104 89.0-112 07/23/2022 14:50 WG1899800
(S) 4-Bromofluorobenzene 460-00-4 90.5 85.0-114 07/23/2022 14:50 WG1899800
(S) 1,2-Dichloroethane-d4 17060-07-0 90.9 81.0-118 07/23/2022 14:50 WG1899800
TPH by Method MADEPE
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics C9-C18 ALI
UNADJ 67.0 U 33.3 67.0 134 1 08/01/2022 17:17 WG1902750
Unadjusted C19-C36 Aliphatics C19-C36 ALI
UNADJ 51.9 B J 33.3 67.0 134 1 08/01/2022 17:17 WG1902750
Unadjusted C11-C22 Aromatics C11-C22 ARO
UNADJ 55.2 B J 33.3 67.0 134 1 08/01/2022 12:49 WG1902750
Unadjusted Total Petroleum
Hydrocarbons TPH UNADJ 107 B J 33.3 67.0 134 1 08/01/2022 17:17 WG1902750
(S) o-Terphenyl 84-15-1 80.5 40.0-140 08/01/2022 12:49 WG1902750
(S) 1-Chloro-octadecane 3386-33-2 63.7 40.0-140 08/01/2022 17:17 WG1902750
(S) 2-Fluorobiphenyl 321-60-8 97.3 40.0-140 08/01/2022 12:49 WG1902750
(S) 2-Bromonaphthalene 580-13-2 94.0 40.0-140 08/01/2022 12:49 WG1902750
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acenaphthene 83-32-9 0.500 J4 U 0.0886 0.500 1.00 1 07/23/2022 18:54 WG1899773
Acenaphthylene 208-96-8 0.500 U 0.0921 0.500 1.00 1 07/23/2022 18:54 WG1899773
Anthracene 120-12-7 0.500 J4 U 0.0804 0.500 1.00 1 07/23/2022 18:54 WG1899773
Benzidine 92-87-5 7.50 U 3.74 7.50 15.0 1 07/23/2022 18:54 WG1899773
Benzo(a)anthracene 56-55-3 0.500 U 0.199 0.500 1.00 1 07/23/2022 18:54 WG1899773
Benzo(b)fluoranthene 205-99-2 0.500 U 0.130 0.500 1.00 1 07/23/2022 18:54 WG1899773
Benzo(k)fluoranthene 207-08-9 0.500 U 0.120 0.500 1.00 1 07/23/2022 18:54 WG1899773
Benzo(g,h,i)perylene 191-24-2 0.500 U 0.121 0.500 1.00 1 07/23/2022 18:54 WG1899773
Benzo(a)pyrene 50-32-8 0.500 U 0.0381 0.500 1.00 1 07/23/2022 18:54 WG1899773
Bis(2-chlorethoxy)methane 111-91-1 5.00 J4 U 0.116 5.00 10.0 1 07/23/2022 18:54 WG1899773
Bis(2-chloroethyl)ether 111-44-4 5.00 J4 U 0.137 5.00 10.0 1 07/23/2022 18:54 WG1899773
2,2-Oxybis(1-Chloropropane)108-60-1 5.00 J4 U 0.210 5.00 10.0 1 07/23/2022 18:54 WG1899773
4-Bromophenyl-phenylether 101-55-3 5.00 U 0.0877 5.00 10.0 1 07/23/2022 18:54 WG1899773
2-Chloronaphthalene 91-58-7 0.500 U 0.0648 0.500 1.00 1 07/23/2022 18:54 WG1899773
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 15:39 32 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 16:01 32 of 65
====================----□ □ □ □
□ □ □ □
SAMPLE RESULTS - 09
L1516722
USTG480-MW25
Collected date/time: 07/18/22 12:51
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
4-Chlorophenyl-phenylether 7005-72-3 5.00 U 0.0926 5.00 10.0 1 07/23/2022 18:54 WG1899773
Chrysene 218-01-9 0.500 U 0.130 0.500 1.00 1 07/23/2022 18:54 WG1899773
Dibenz(a,h)anthracene 53-70-3 0.500 U 0.0644 0.500 1.00 1 07/23/2022 18:54 WG1899773
3,3-Dichlorobenzidine 91-94-1 5.00 U 0.212 5.00 10.0 1 07/23/2022 18:54 WG1899773
2,4-Dinitrotoluene 121-14-2 5.00 U 0.0983 5.00 10.0 1 07/23/2022 18:54 WG1899773
2,6-Dinitrotoluene 606-20-2 5.00 U 0.250 5.00 10.0 1 07/23/2022 18:54 WG1899773
Fluoranthene 206-44-0 0.500 U 0.102 0.500 1.00 1 07/23/2022 18:54 WG1899773
Fluorene 86-73-7 0.500 U 0.0844 0.500 1.00 1 07/23/2022 18:54 WG1899773
Hexachlorobenzene 118-74-1 0.500 U 0.0755 0.500 1.00 1 07/23/2022 18:54 WG1899773
Hexachloro-1,3-butadiene 87-68-3 5.00 U 0.0968 5.00 10.0 1 07/23/2022 18:54 WG1899773
Hexachlorocyclopentadiene 77-47-4 5.00 U 0.0598 5.00 10.0 1 07/23/2022 18:54 WG1899773
Hexachloroethane 67-72-1 5.00 U 0.127 5.00 10.0 1 07/23/2022 18:54 WG1899773
Indeno(1,2,3-cd)pyrene 193-39-5 0.600 U 0.279 0.600 1.20 1 07/23/2022 18:54 WG1899773
Isophorone 78-59-1 5.00 U 0.143 5.00 10.0 1 07/23/2022 18:54 WG1899773
Naphthalene 91-20-3 0.478 J J4 0.159 0.500 1.00 1 07/23/2022 18:54 WG1899773
Nitrobenzene 98-95-3 5.00 J4 U 0.297 5.00 10.0 1 07/23/2022 18:54 WG1899773
n-Nitrosodimethylamine 62-75-9 5.00 U 0.998 5.00 10.0 1 07/23/2022 18:54 WG1899773
n-Nitrosodiphenylamine 86-30-6 5.00 J4 U 2.37 5.00 10.0 1 07/23/2022 18:54 WG1899773
n-Nitrosodi-n-propylamine 621-64-7 5.00 J4 U 0.261 5.00 10.0 1 07/23/2022 18:54 WG1899773
Phenanthrene 85-01-8 0.500 J4 U 0.112 0.500 1.00 1 07/23/2022 18:54 WG1899773
Benzylbutyl phthalate 85-68-7 2.00 U 0.765 2.00 4.00 1 07/23/2022 18:54 WG1899773
Bis(2-ethylhexyl)phthalate 117-81-7 2.00 U 0.895 2.00 4.00 1 07/23/2022 18:54 WG1899773
Di-n-butyl phthalate 84-74-2 1.50 U 0.453 1.50 3.00 1 07/23/2022 18:54 WG1899773
Diethyl phthalate 84-66-2 1.50 U 0.287 1.50 3.00 1 07/23/2022 18:54 WG1899773
Dimethyl phthalate 131-11-3 1.50 U 0.260 1.50 3.00 1 07/23/2022 18:54 WG1899773
Di-n-octyl phthalate 117-84-0 2.00 U 0.932 2.00 4.00 1 07/23/2022 18:54 WG1899773
Pyrene 129-00-0 0.500 J4 U 0.107 0.500 1.00 1 07/23/2022 18:54 WG1899773
1,2,4-Trichlorobenzene 120-82-1 5.00 U 0.0698 5.00 10.0 1 07/23/2022 18:54 WG1899773
4-Chloro-3-methylphenol 59-50-7 5.00 U 0.131 5.00 10.0 1 07/23/2022 18:54 WG1899773
2-Chlorophenol 95-57-8 5.00 J4 U 0.133 5.00 10.0 1 07/23/2022 18:54 WG1899773
2,4-Dichlorophenol 120-83-2 5.00 J4 U 0.102 5.00 10.0 1 07/23/2022 18:54 WG1899773
2,4-Dimethylphenol 105-67-9 5.00 U 0.0636 5.00 10.0 1 07/23/2022 18:54 WG1899773
4,6-Dinitro-2-methylphenol 534-52-1 5.00 U 1.12 5.00 10.0 1 07/23/2022 18:54 WG1899773
2,4-Dinitrophenol 51-28-5 15.0 U 5.93 15.0 30.0 1 07/23/2022 18:54 WG1899773
2-Nitrophenol 88-75-5 5.00 J4 U 0.117 5.00 10.0 1 07/23/2022 18:54 WG1899773
4-Nitrophenol 100-02-7 5.00 U 0.143 5.00 10.0 1 07/23/2022 18:54 WG1899773
Pentachlorophenol 87-86-5 5.00 U 0.313 5.00 10.0 1 07/23/2022 18:54 WG1899773
Phenol 108-95-2 10.0 U 4.33 10.0 20.0 1 07/23/2022 18:54 WG1899773
2,4,6-Trichlorophenol 88-06-2 5.00 U 0.100 5.00 10.0 1 07/23/2022 18:54 WG1899773
1-Methylnaphthalene 90-12-0 0.279 J 0.0790 0.500 1.00 1 07/23/2022 18:54 WG1899773
2-Methylnaphthalene 91-57-6 0.309 J 0.117 0.500 1.00 1 07/23/2022 18:54 WG1899773
(S) Nitrobenzene-d5 4165-60-0 30.0 J2 0.000 44.0-120 07/23/2022 18:54 WG1899773
(S) 2-Fluorobiphenyl 321-60-8 33.5 J2 0.000 44.0-119 07/23/2022 18:54 WG1899773
(S) p-Terphenyl-d14 1718-51-0 46.2 J2 0.000 50.0-134 07/23/2022 18:54 WG1899773
(S) Phenol-d5 4165-62-2 12.8 0.000 10.0-67.0 07/23/2022 18:54 WG1899773
(S) 2-Fluorophenol 367-12-4 16.5 J2 0.000 19.0-119 07/23/2022 18:54 WG1899773
(S) 2,4,6-Tribromophenol 118-79-6 58.2 0.000 43.0-140 07/23/2022 18:54 WG1899773
Sample Narrative:
L1516722-09 WG1899773: Surrogate recovery within historical limits.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 15:39 33 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 16:01 33 of 65
====================----□ □ □ □
□ □ □ □
SAMPLE RESULTS - 10
L1516722
USTTC341-MW17
Collected date/time: 07/18/22 12:52
Volatile Petroleum Hydrocarbons by Method MADEPV
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics C5-C8 ALI
UNADJ 67.0 U 33.3 67.0 100 1 07/24/2022 01:00 WG1899531
Unadjusted C9-C12 Aliphatics C9-C12 ALI
UNADJ 37.7 J 33.3 67.0 134 1 07/24/2022 01:00 WG1899531
Unadjusted C9-C10 Aromatics C9-C10 ARO
UNADJ 67.0 U 33.3 67.0 100 1 07/24/2022 01:00 WG1899531
Total VPH VPH 150 U 66.7 150 300 1 07/24/2022 01:00 WG1899531
(S) 2,5-Dibromotoluene(FID)615-59-8 108 70.0-130 07/24/2022 01:00 WG1899531
(S) 2,5-Dibromotoluene(PID)615-59-8 106 70.0-130 07/24/2022 01:00 WG1899531
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acetone 67-64-1 25.0 U 11.3 25.0 50.0 1 07/23/2022 15:11 WG1899800
Acrolein 107-02-8 25.0 U 2.54 25.0 50.0 1 07/23/2022 15:11 WG1899800
Acrylonitrile 107-13-1 5.00 U 0.671 5.00 10.0 1 07/23/2022 15:11 WG1899800
Benzene 71-43-2 0.500 U 0.0941 0.500 1.00 1 07/23/2022 15:11 WG1899800
Bromobenzene 108-86-1 0.500 C4 J4 U 0.118 0.500 1.00 1 07/23/2022 15:11 WG1899800
Bromodichloromethane 75-27-4 0.500 U 0.136 0.500 1.00 1 07/23/2022 15:11 WG1899800
Bromoform 75-25-2 0.500 U 0.129 0.500 1.00 1 07/23/2022 15:11 WG1899800
Bromomethane 74-83-9 2.00 U 0.605 2.00 5.00 1 07/23/2022 15:11 WG1899800
n-Butylbenzene 104-51-8 0.500 U 0.157 0.500 1.00 1 07/23/2022 15:11 WG1899800
sec-Butylbenzene 135-98-8 0.500 U 0.125 0.500 1.00 1 07/23/2022 15:11 WG1899800
tert-Butylbenzene 98-06-6 0.500 U 0.127 0.500 1.00 1 07/23/2022 15:11 WG1899800
Carbon tetrachloride 56-23-5 0.500 U 0.128 0.500 1.00 1 07/23/2022 15:11 WG1899800
Chlorobenzene 108-90-7 0.500 U 0.116 0.500 1.00 1 07/23/2022 15:11 WG1899800
Chlorodibromomethane 124-48-1 0.500 U 0.140 0.500 1.00 1 07/23/2022 15:11 WG1899800
Chloroethane 75-00-3 2.00 U 0.192 2.00 5.00 1 07/23/2022 15:11 WG1899800
Chloroform 67-66-3 2.00 U 0.111 2.00 5.00 1 07/23/2022 15:11 WG1899800
Chloromethane 74-87-3 2.00 U 0.960 2.00 4.00 1 07/23/2022 15:11 WG1899800
2-Chlorotoluene 95-49-8 0.500 U 0.106 0.500 1.00 1 07/23/2022 15:11 WG1899800
4-Chlorotoluene 106-43-4 0.500 U 0.114 0.500 1.00 1 07/23/2022 15:11 WG1899800
1,2-Dibromo-3-Chloropropane 96-12-8 2.00 U 0.276 2.00 5.00 1 07/23/2022 15:11 WG1899800
1,2-Dibromoethane 106-93-4 0.500 U 0.126 0.500 1.00 1 07/23/2022 15:11 WG1899800
Dibromomethane 74-95-3 0.500 U 0.122 0.500 1.00 1 07/23/2022 15:11 WG1899800
1,2-Dichlorobenzene 95-50-1 0.500 U 0.107 0.500 1.00 1 07/23/2022 15:11 WG1899800
1,3-Dichlorobenzene 541-73-1 0.500 U 0.110 0.500 1.00 1 07/23/2022 15:11 WG1899800
1,4-Dichlorobenzene 106-46-7 0.500 U 0.120 0.500 1.00 1 07/23/2022 15:11 WG1899800
Dichlorodifluoromethane 75-71-8 2.00 U 0.374 2.00 5.00 1 07/23/2022 15:11 WG1899800
1,1-Dichloroethane 75-34-3 0.500 U 0.100 0.500 1.00 1 07/23/2022 15:11 WG1899800
1,2-Dichloroethane 107-06-2 0.500 U 0.0819 0.500 1.00 1 07/23/2022 15:11 WG1899800
1,1-Dichloroethene 75-35-4 0.500 U 0.188 0.500 1.00 1 07/23/2022 15:11 WG1899800
cis-1,2-Dichloroethene 156-59-2 0.500 U 0.126 0.500 1.00 1 07/23/2022 15:11 WG1899800
trans-1,2-Dichloroethene 156-60-5 0.500 U 0.149 0.500 1.00 1 07/23/2022 15:11 WG1899800
1,2-Dichloropropane 78-87-5 0.500 U 0.149 0.500 1.00 1 07/23/2022 15:11 WG1899800
1,1-Dichloropropene 563-58-6 0.500 U 0.142 0.500 1.00 1 07/23/2022 15:11 WG1899800
1,3-Dichloropropane 142-28-9 0.500 U 0.110 0.500 1.00 1 07/23/2022 15:11 WG1899800
2,2-Dichloropropane 594-20-7 0.500 U 0.161 0.500 1.00 1 07/23/2022 15:11 WG1899800
Di-isopropyl ether 108-20-3 0.500 U 0.105 0.500 1.00 1 07/23/2022 15:11 WG1899800
Ethylbenzene 100-41-4 0.500 U 0.137 0.500 1.00 1 07/23/2022 15:11 WG1899800
Hexachloro-1,3-butadiene 87-68-3 0.750 U 0.337 0.750 1.50 1 07/23/2022 15:11 WG1899800
Isopropylbenzene 98-82-8 0.500 U 0.105 0.500 1.00 1 07/23/2022 15:11 WG1899800
p-Isopropyltoluene 99-87-6 0.500 U 0.120 0.500 1.00 1 07/23/2022 15:11 WG1899800
2-Butanone (MEK)78-93-3 5.00 U 1.19 5.00 10.0 1 07/23/2022 15:11 WG1899800
Methylene Chloride 75-09-2 2.00 U 0.430 2.00 5.00 1 07/23/2022 15:11 WG1899800
4-Methyl-2-pentanone (MIBK)108-10-1 5.00 U 0.478 5.00 10.0 1 07/23/2022 15:11 WG1899800
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 15:39 34 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 16:01 34 of 65
--------------=---□
□ □ □
==============~~~~~=----□ □ □ □
SAMPLE RESULTS - 10
L1516722
USTTC341-MW17
Collected date/time: 07/18/22 12:52
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Methyl tert-butyl ether 1634-04-4 0.500 U 0.101 0.500 1.00 1 07/23/2022 15:11 WG1899800
Naphthalene 91-20-3 2.00 U 1.00 2.00 5.00 1 07/23/2022 15:11 WG1899800
n-Propylbenzene 103-65-1 0.500 C4 J4 U 0.0993 0.500 1.00 1 07/23/2022 15:11 WG1899800
Styrene 100-42-5 0.500 U 0.118 0.500 1.00 1 07/23/2022 15:11 WG1899800
1,1,1,2-Tetrachloroethane 630-20-6 0.500 U 0.147 0.500 1.00 1 07/23/2022 15:11 WG1899800
1,1,2,2-Tetrachloroethane 79-34-5 0.500 U 0.133 0.500 1.00 1 07/23/2022 15:11 WG1899800
Tetrachloroethene 127-18-4 0.600 U 0.300 0.600 1.20 1 07/23/2022 15:11 WG1899800
Toluene 108-88-3 0.600 U 0.278 0.600 1.20 1 07/23/2022 15:11 WG1899800
1,2,3-Trichlorobenzene 87-61-6 0.500 C4 U 0.230 0.500 1.00 1 07/23/2022 15:11 WG1899800
1,2,4-Trichlorobenzene 120-82-1 1.00 U 0.481 1.00 2.00 1 07/23/2022 15:11 WG1899800
1,1,1-Trichloroethane 71-55-6 0.500 U 0.149 0.500 1.00 1 07/23/2022 15:11 WG1899800
1,1,2-Trichloroethane 79-00-5 0.500 U 0.158 0.500 1.00 1 07/23/2022 15:11 WG1899800
Trichloroethene 79-01-6 0.500 U 0.190 0.500 1.00 1 07/23/2022 15:11 WG1899800
Trichlorofluoromethane 75-69-4 2.00 U 0.160 2.00 5.00 1 07/23/2022 15:11 WG1899800
1,2,3-Trichloropropane 96-18-4 1.00 U 0.237 1.00 2.50 1 07/23/2022 15:11 WG1899800
1,2,4-Trimethylbenzene 95-63-6 1.00 U 0.322 1.00 2.00 1 07/23/2022 15:11 WG1899800
1,3,5-Trimethylbenzene 108-67-8 0.500 U 0.104 0.500 1.00 1 07/23/2022 15:11 WG1899800
Vinyl chloride 75-01-4 0.500 U 0.234 0.500 1.00 1 07/23/2022 15:11 WG1899800
o-Xylene 95-47-6 0.500 U 0.174 0.500 1.00 1 07/23/2022 15:11 WG1899800
m&p-Xylenes 1330-20-7 1.00 U 0.430 1.00 2.00 1 07/23/2022 15:11 WG1899800
(S) Toluene-d8 2037-26-5 111 89.0-112 07/23/2022 15:11 WG1899800
(S) 4-Bromofluorobenzene 460-00-4 91.9 85.0-114 07/23/2022 15:11 WG1899800
(S) 1,2-Dichloroethane-d4 17060-07-0 94.2 81.0-118 07/23/2022 15:11 WG1899800
TPH by Method MADEPE
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics C9-C18 ALI
UNADJ 67.0 U 33.3 67.0 134 1 08/01/2022 17:39 WG1902750
Unadjusted C19-C36 Aliphatics C19-C36 ALI
UNADJ 36.6 B J 33.3 67.0 134 1 08/01/2022 17:39 WG1902750
Unadjusted C11-C22 Aromatics C11-C22 ARO
UNADJ 47.2 B J 33.3 67.0 134 1 08/01/2022 12:27 WG1902750
Unadjusted Total Petroleum
Hydrocarbons TPH UNADJ 83.8 B J 33.3 67.0 134 1 08/01/2022 17:39 WG1902750
(S) o-Terphenyl 84-15-1 81.3 40.0-140 08/01/2022 12:27 WG1902750
(S) 1-Chloro-octadecane 3386-33-2 64.4 40.0-140 08/01/2022 17:39 WG1902750
(S) 2-Fluorobiphenyl 321-60-8 97.1 40.0-140 08/01/2022 12:27 WG1902750
(S) 2-Bromonaphthalene 580-13-2 93.9 40.0-140 08/01/2022 12:27 WG1902750
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acenaphthene 83-32-9 0.555 J4 U 0.0983 0.555 1.11 1.11 07/23/2022 13:22 WG1899773
Acenaphthylene 208-96-8 0.555 U 0.102 0.555 1.11 1.11 07/23/2022 13:22 WG1899773
Anthracene 120-12-7 0.555 J4 U 0.0892 0.555 1.11 1.11 07/23/2022 13:22 WG1899773
Benzidine 92-87-5 8.33 U 4.15 8.33 16.7 1.11 07/23/2022 13:22 WG1899773
Benzo(a)anthracene 56-55-3 0.555 U 0.221 0.555 1.11 1.11 07/23/2022 13:22 WG1899773
Benzo(b)fluoranthene 205-99-2 0.555 U 0.144 0.555 1.11 1.11 07/23/2022 13:22 WG1899773
Benzo(k)fluoranthene 207-08-9 0.555 U 0.133 0.555 1.11 1.11 07/23/2022 13:22 WG1899773
Benzo(g,h,i)perylene 191-24-2 0.555 U 0.134 0.555 1.11 1.11 07/23/2022 13:22 WG1899773
Benzo(a)pyrene 50-32-8 0.555 U 0.0423 0.555 1.11 1.11 07/23/2022 13:22 WG1899773
Bis(2-chlorethoxy)methane 111-91-1 5.55 J4 U 0.129 5.55 11.1 1.11 07/23/2022 13:22 WG1899773
Bis(2-chloroethyl)ether 111-44-4 5.55 J4 U 0.152 5.55 11.1 1.11 07/23/2022 13:22 WG1899773
2,2-Oxybis(1-Chloropropane)108-60-1 5.55 J4 U 0.233 5.55 11.1 1.11 07/23/2022 13:22 WG1899773
4-Bromophenyl-phenylether 101-55-3 5.55 U 0.0973 5.55 11.1 1.11 07/23/2022 13:22 WG1899773
2-Chloronaphthalene 91-58-7 0.555 U 0.0719 0.555 1.11 1.11 07/23/2022 13:22 WG1899773
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 15:39 35 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 16:01 35 of 65
====================----□ □ □ □
□ □ □ □
SAMPLE RESULTS - 10
L1516722
USTTC341-MW17
Collected date/time: 07/18/22 12:52
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
4-Chlorophenyl-phenylether 7005-72-3 5.55 U 0.103 5.55 11.1 1.11 07/23/2022 13:22 WG1899773
Chrysene 218-01-9 0.555 U 0.144 0.555 1.11 1.11 07/23/2022 13:22 WG1899773
Dibenz(a,h)anthracene 53-70-3 0.555 U 0.0715 0.555 1.11 1.11 07/23/2022 13:22 WG1899773
3,3-Dichlorobenzidine 91-94-1 5.55 U 0.235 5.55 11.1 1.11 07/23/2022 13:22 WG1899773
2,4-Dinitrotoluene 121-14-2 5.55 U 0.109 5.55 11.1 1.11 07/23/2022 13:22 WG1899773
2,6-Dinitrotoluene 606-20-2 5.55 U 0.278 5.55 11.1 1.11 07/23/2022 13:22 WG1899773
Fluoranthene 206-44-0 0.555 U 0.113 0.555 1.11 1.11 07/23/2022 13:22 WG1899773
Fluorene 86-73-7 0.555 U 0.0937 0.555 1.11 1.11 07/23/2022 13:22 WG1899773
Hexachlorobenzene 118-74-1 0.555 U 0.0838 0.555 1.11 1.11 07/23/2022 13:22 WG1899773
Hexachloro-1,3-butadiene 87-68-3 5.55 U 0.107 5.55 11.1 1.11 07/23/2022 13:22 WG1899773
Hexachlorocyclopentadiene 77-47-4 5.55 U 0.0664 5.55 11.1 1.11 07/23/2022 13:22 WG1899773
Hexachloroethane 67-72-1 5.55 U 0.141 5.55 11.1 1.11 07/23/2022 13:22 WG1899773
Indeno(1,2,3-cd)pyrene 193-39-5 0.666 U 0.310 0.666 1.33 1.11 07/23/2022 13:22 WG1899773
Isophorone 78-59-1 5.55 U 0.159 5.55 11.1 1.11 07/23/2022 13:22 WG1899773
Naphthalene 91-20-3 0.555 J4 U 0.176 0.555 1.11 1.11 07/23/2022 13:22 WG1899773
Nitrobenzene 98-95-3 5.55 J4 U 0.330 5.55 11.1 1.11 07/23/2022 13:22 WG1899773
n-Nitrosodimethylamine 62-75-9 5.55 U 1.11 5.55 11.1 1.11 07/23/2022 13:22 WG1899773
n-Nitrosodiphenylamine 86-30-6 5.55 J4 U 2.63 5.55 11.1 1.11 07/23/2022 13:22 WG1899773
n-Nitrosodi-n-propylamine 621-64-7 5.55 J4 U 0.290 5.55 11.1 1.11 07/23/2022 13:22 WG1899773
Phenanthrene 85-01-8 0.555 J4 U 0.124 0.555 1.11 1.11 07/23/2022 13:22 WG1899773
Benzylbutyl phthalate 85-68-7 2.22 U 0.849 2.22 4.44 1.11 07/23/2022 13:22 WG1899773
Bis(2-ethylhexyl)phthalate 117-81-7 2.22 U 0.993 2.22 4.44 1.11 07/23/2022 13:22 WG1899773
Di-n-butyl phthalate 84-74-2 1.67 U 0.503 1.67 3.33 1.11 07/23/2022 13:22 WG1899773
Diethyl phthalate 84-66-2 1.67 U 0.319 1.67 3.33 1.11 07/23/2022 13:22 WG1899773
Dimethyl phthalate 131-11-3 1.67 U 0.289 1.67 3.33 1.11 07/23/2022 13:22 WG1899773
Di-n-octyl phthalate 117-84-0 2.22 U 1.03 2.22 4.44 1.11 07/23/2022 13:22 WG1899773
Pyrene 129-00-0 0.555 J4 U 0.119 0.555 1.11 1.11 07/23/2022 13:22 WG1899773
1,2,4-Trichlorobenzene 120-82-1 5.55 U 0.0775 5.55 11.1 1.11 07/23/2022 13:22 WG1899773
4-Chloro-3-methylphenol 59-50-7 5.55 U 0.145 5.55 11.1 1.11 07/23/2022 13:22 WG1899773
2-Chlorophenol 95-57-8 5.55 J4 U 0.148 5.55 11.1 1.11 07/23/2022 13:22 WG1899773
2,4-Dichlorophenol 120-83-2 5.55 J4 U 0.113 5.55 11.1 1.11 07/23/2022 13:22 WG1899773
2,4-Dimethylphenol 105-67-9 5.55 U 0.0706 5.55 11.1 1.11 07/23/2022 13:22 WG1899773
4,6-Dinitro-2-methylphenol 534-52-1 5.55 U 1.24 5.55 11.1 1.11 07/23/2022 13:22 WG1899773
2,4-Dinitrophenol 51-28-5 16.7 U 6.58 16.7 33.3 1.11 07/23/2022 13:22 WG1899773
2-Nitrophenol 88-75-5 5.55 J4 U 0.130 5.55 11.1 1.11 07/23/2022 13:22 WG1899773
4-Nitrophenol 100-02-7 5.55 U 0.159 5.55 11.1 1.11 07/23/2022 13:22 WG1899773
Pentachlorophenol 87-86-5 5.55 U 0.347 5.55 11.1 1.11 07/23/2022 13:22 WG1899773
Phenol 108-95-2 11.1 U 4.81 11.1 22.2 1.11 07/23/2022 13:22 WG1899773
2,4,6-Trichlorophenol 88-06-2 5.55 U 0.111 5.55 11.1 1.11 07/23/2022 13:22 WG1899773
1-Methylnaphthalene 90-12-0 0.555 U 0.0877 0.555 1.11 1.11 07/23/2022 13:22 WG1899773
2-Methylnaphthalene 91-57-6 0.555 U 0.130 0.555 1.11 1.11 07/23/2022 13:22 WG1899773
(S) Nitrobenzene-d5 4165-60-0 26.5 J2 0.000 44.0-120 07/23/2022 13:22 WG1899773
(S) 2-Fluorobiphenyl 321-60-8 28.8 J2 0.000 44.0-119 07/23/2022 13:22 WG1899773
(S) p-Terphenyl-d14 1718-51-0 47.0 J2 0.000 50.0-134 07/23/2022 13:22 WG1899773
(S) Phenol-d5 4165-62-2 15.1 0.000 10.0-67.0 07/23/2022 13:22 WG1899773
(S) 2-Fluorophenol 367-12-4 21.0 0.000 19.0-119 07/23/2022 13:22 WG1899773
(S) 2,4,6-Tribromophenol 118-79-6 42.8 J2 0.000 43.0-140 07/23/2022 13:22 WG1899773
Sample Narrative:
L1516722-10 WG1899773: Surrogate recovery within historical limits.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 15:39 36 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 16:01 36 of 65
====================----□ □ □ □
□ □ □ □
SAMPLE RESULTS - 11
L1516722
USTTC341-MW13
Collected date/time: 07/18/22 13:25
Volatile Petroleum Hydrocarbons by Method MADEPV
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics C5-C8 ALI
UNADJ 67.0 U 33.3 67.0 100 1 07/24/2022 01:33 WG1899531
Unadjusted C9-C12 Aliphatics C9-C12 ALI
UNADJ 67.0 U 33.3 67.0 134 1 07/24/2022 01:33 WG1899531
Unadjusted C9-C10 Aromatics C9-C10 ARO
UNADJ 67.0 U 33.3 67.0 100 1 07/24/2022 01:33 WG1899531
Total VPH VPH 150 U 66.7 150 300 1 07/24/2022 01:33 WG1899531
(S) 2,5-Dibromotoluene(FID)615-59-8 106 70.0-130 07/24/2022 01:33 WG1899531
(S) 2,5-Dibromotoluene(PID)615-59-8 105 70.0-130 07/24/2022 01:33 WG1899531
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acetone 67-64-1 25.0 U 11.3 25.0 50.0 1 07/23/2022 15:32 WG1899800
Acrolein 107-02-8 25.0 U 2.54 25.0 50.0 1 07/23/2022 15:32 WG1899800
Acrylonitrile 107-13-1 5.00 U 0.671 5.00 10.0 1 07/23/2022 15:32 WG1899800
Benzene 71-43-2 0.500 U 0.0941 0.500 1.00 1 07/23/2022 15:32 WG1899800
Bromobenzene 108-86-1 0.500 C4 J4 U 0.118 0.500 1.00 1 07/23/2022 15:32 WG1899800
Bromodichloromethane 75-27-4 0.500 U 0.136 0.500 1.00 1 07/23/2022 15:32 WG1899800
Bromoform 75-25-2 0.500 U 0.129 0.500 1.00 1 07/23/2022 15:32 WG1899800
Bromomethane 74-83-9 2.00 U 0.605 2.00 5.00 1 07/23/2022 15:32 WG1899800
n-Butylbenzene 104-51-8 0.500 U 0.157 0.500 1.00 1 07/23/2022 15:32 WG1899800
sec-Butylbenzene 135-98-8 0.500 U 0.125 0.500 1.00 1 07/23/2022 15:32 WG1899800
tert-Butylbenzene 98-06-6 0.500 U 0.127 0.500 1.00 1 07/23/2022 15:32 WG1899800
Carbon tetrachloride 56-23-5 0.500 U 0.128 0.500 1.00 1 07/23/2022 15:32 WG1899800
Chlorobenzene 108-90-7 0.500 U 0.116 0.500 1.00 1 07/23/2022 15:32 WG1899800
Chlorodibromomethane 124-48-1 0.500 U 0.140 0.500 1.00 1 07/23/2022 15:32 WG1899800
Chloroethane 75-00-3 2.00 U 0.192 2.00 5.00 1 07/23/2022 15:32 WG1899800
Chloroform 67-66-3 2.00 U 0.111 2.00 5.00 1 07/23/2022 15:32 WG1899800
Chloromethane 74-87-3 2.00 U 0.960 2.00 4.00 1 07/23/2022 15:32 WG1899800
2-Chlorotoluene 95-49-8 0.500 U 0.106 0.500 1.00 1 07/23/2022 15:32 WG1899800
4-Chlorotoluene 106-43-4 0.500 U 0.114 0.500 1.00 1 07/23/2022 15:32 WG1899800
1,2-Dibromo-3-Chloropropane 96-12-8 2.00 U 0.276 2.00 5.00 1 07/23/2022 15:32 WG1899800
1,2-Dibromoethane 106-93-4 0.500 U 0.126 0.500 1.00 1 07/23/2022 15:32 WG1899800
Dibromomethane 74-95-3 0.500 U 0.122 0.500 1.00 1 07/23/2022 15:32 WG1899800
1,2-Dichlorobenzene 95-50-1 0.500 U 0.107 0.500 1.00 1 07/23/2022 15:32 WG1899800
1,3-Dichlorobenzene 541-73-1 0.500 U 0.110 0.500 1.00 1 07/23/2022 15:32 WG1899800
1,4-Dichlorobenzene 106-46-7 0.500 U 0.120 0.500 1.00 1 07/23/2022 15:32 WG1899800
Dichlorodifluoromethane 75-71-8 2.00 U 0.374 2.00 5.00 1 07/23/2022 15:32 WG1899800
1,1-Dichloroethane 75-34-3 0.500 U 0.100 0.500 1.00 1 07/23/2022 15:32 WG1899800
1,2-Dichloroethane 107-06-2 0.500 U 0.0819 0.500 1.00 1 07/23/2022 15:32 WG1899800
1,1-Dichloroethene 75-35-4 0.500 U 0.188 0.500 1.00 1 07/23/2022 15:32 WG1899800
cis-1,2-Dichloroethene 156-59-2 0.500 U 0.126 0.500 1.00 1 07/23/2022 15:32 WG1899800
trans-1,2-Dichloroethene 156-60-5 0.500 U 0.149 0.500 1.00 1 07/23/2022 15:32 WG1899800
1,2-Dichloropropane 78-87-5 0.500 U 0.149 0.500 1.00 1 07/23/2022 15:32 WG1899800
1,1-Dichloropropene 563-58-6 0.500 U 0.142 0.500 1.00 1 07/23/2022 15:32 WG1899800
1,3-Dichloropropane 142-28-9 0.500 U 0.110 0.500 1.00 1 07/23/2022 15:32 WG1899800
2,2-Dichloropropane 594-20-7 0.500 U 0.161 0.500 1.00 1 07/23/2022 15:32 WG1899800
Di-isopropyl ether 108-20-3 0.500 U 0.105 0.500 1.00 1 07/23/2022 15:32 WG1899800
Ethylbenzene 100-41-4 0.500 U 0.137 0.500 1.00 1 07/23/2022 15:32 WG1899800
Hexachloro-1,3-butadiene 87-68-3 0.750 U 0.337 0.750 1.50 1 07/23/2022 15:32 WG1899800
Isopropylbenzene 98-82-8 0.500 U 0.105 0.500 1.00 1 07/23/2022 15:32 WG1899800
p-Isopropyltoluene 99-87-6 0.500 U 0.120 0.500 1.00 1 07/23/2022 15:32 WG1899800
2-Butanone (MEK)78-93-3 5.00 U 1.19 5.00 10.0 1 07/23/2022 15:32 WG1899800
Methylene Chloride 75-09-2 2.00 U 0.430 2.00 5.00 1 07/23/2022 15:32 WG1899800
4-Methyl-2-pentanone (MIBK)108-10-1 5.00 U 0.478 5.00 10.0 1 07/23/2022 15:32 WG1899800
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 15:39 37 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 16:01 37 of 65
--------------=---□
□ □ □
==============~~~~~=----□ □ □ □
SAMPLE RESULTS - 11
L1516722
USTTC341-MW13
Collected date/time: 07/18/22 13:25
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Methyl tert-butyl ether 1634-04-4 0.500 U 0.101 0.500 1.00 1 07/23/2022 15:32 WG1899800
Naphthalene 91-20-3 2.00 U 1.00 2.00 5.00 1 07/23/2022 15:32 WG1899800
n-Propylbenzene 103-65-1 0.500 C4 J4 U 0.0993 0.500 1.00 1 07/23/2022 15:32 WG1899800
Styrene 100-42-5 0.500 U 0.118 0.500 1.00 1 07/23/2022 15:32 WG1899800
1,1,1,2-Tetrachloroethane 630-20-6 0.500 U 0.147 0.500 1.00 1 07/23/2022 15:32 WG1899800
1,1,2,2-Tetrachloroethane 79-34-5 0.500 U 0.133 0.500 1.00 1 07/23/2022 15:32 WG1899800
Tetrachloroethene 127-18-4 0.600 U 0.300 0.600 1.20 1 07/23/2022 15:32 WG1899800
Toluene 108-88-3 0.600 U 0.278 0.600 1.20 1 07/23/2022 15:32 WG1899800
1,2,3-Trichlorobenzene 87-61-6 0.500 C4 U 0.230 0.500 1.00 1 07/23/2022 15:32 WG1899800
1,2,4-Trichlorobenzene 120-82-1 1.00 U 0.481 1.00 2.00 1 07/23/2022 15:32 WG1899800
1,1,1-Trichloroethane 71-55-6 0.500 U 0.149 0.500 1.00 1 07/23/2022 15:32 WG1899800
1,1,2-Trichloroethane 79-00-5 0.500 U 0.158 0.500 1.00 1 07/23/2022 15:32 WG1899800
Trichloroethene 79-01-6 0.500 U 0.190 0.500 1.00 1 07/23/2022 15:32 WG1899800
Trichlorofluoromethane 75-69-4 2.00 U 0.160 2.00 5.00 1 07/23/2022 15:32 WG1899800
1,2,3-Trichloropropane 96-18-4 1.00 U 0.237 1.00 2.50 1 07/23/2022 15:32 WG1899800
1,2,4-Trimethylbenzene 95-63-6 1.00 U 0.322 1.00 2.00 1 07/23/2022 15:32 WG1899800
1,3,5-Trimethylbenzene 108-67-8 0.500 U 0.104 0.500 1.00 1 07/23/2022 15:32 WG1899800
Vinyl chloride 75-01-4 0.500 U 0.234 0.500 1.00 1 07/23/2022 15:32 WG1899800
o-Xylene 95-47-6 0.500 U 0.174 0.500 1.00 1 07/23/2022 15:32 WG1899800
m&p-Xylenes 1330-20-7 1.00 U 0.430 1.00 2.00 1 07/23/2022 15:32 WG1899800
(S) Toluene-d8 2037-26-5 99.6 89.0-112 07/23/2022 15:32 WG1899800
(S) 4-Bromofluorobenzene 460-00-4 85.6 85.0-114 07/23/2022 15:32 WG1899800
(S) 1,2-Dichloroethane-d4 17060-07-0 92.5 81.0-118 07/23/2022 15:32 WG1899800
TPH by Method MADEPE
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics C9-C18 ALI
UNADJ 67.0 U 33.3 67.0 134 1 08/01/2022 18:01 WG1902750
Unadjusted C19-C36 Aliphatics C19-C36 ALI
UNADJ 34.9 B J 33.3 67.0 134 1 08/01/2022 18:01 WG1902750
Unadjusted C11-C22 Aromatics C11-C22 ARO
UNADJ 41.7 B J 33.3 67.0 134 1 08/01/2022 12:04 WG1902750
Unadjusted Total Petroleum
Hydrocarbons TPH UNADJ 76.6 B J 33.3 67.0 134 1 08/01/2022 18:01 WG1902750
(S) o-Terphenyl 84-15-1 79.6 40.0-140 08/01/2022 12:04 WG1902750
(S) 1-Chloro-octadecane 3386-33-2 59.9 40.0-140 08/01/2022 18:01 WG1902750
(S) 2-Fluorobiphenyl 321-60-8 91.7 40.0-140 08/01/2022 12:04 WG1902750
(S) 2-Bromonaphthalene 580-13-2 88.8 40.0-140 08/01/2022 12:04 WG1902750
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acenaphthene 83-32-9 0.500 J4 U 0.0886 0.500 1.00 1 07/23/2022 18:32 WG1899773
Acenaphthylene 208-96-8 0.500 U 0.0921 0.500 1.00 1 07/23/2022 18:32 WG1899773
Anthracene 120-12-7 0.500 J4 U 0.0804 0.500 1.00 1 07/23/2022 18:32 WG1899773
Benzidine 92-87-5 7.50 U 3.74 7.50 15.0 1 07/23/2022 18:32 WG1899773
Benzo(a)anthracene 56-55-3 0.500 U 0.199 0.500 1.00 1 07/23/2022 18:32 WG1899773
Benzo(b)fluoranthene 205-99-2 0.500 U 0.130 0.500 1.00 1 07/23/2022 18:32 WG1899773
Benzo(k)fluoranthene 207-08-9 0.500 U 0.120 0.500 1.00 1 07/23/2022 18:32 WG1899773
Benzo(g,h,i)perylene 191-24-2 0.500 U 0.121 0.500 1.00 1 07/23/2022 18:32 WG1899773
Benzo(a)pyrene 50-32-8 0.500 U 0.0381 0.500 1.00 1 07/23/2022 18:32 WG1899773
Bis(2-chlorethoxy)methane 111-91-1 5.00 J4 U 0.116 5.00 10.0 1 07/23/2022 18:32 WG1899773
Bis(2-chloroethyl)ether 111-44-4 5.00 J4 U 0.137 5.00 10.0 1 07/23/2022 18:32 WG1899773
2,2-Oxybis(1-Chloropropane)108-60-1 5.00 J4 U 0.210 5.00 10.0 1 07/23/2022 18:32 WG1899773
4-Bromophenyl-phenylether 101-55-3 5.00 U 0.0877 5.00 10.0 1 07/23/2022 18:32 WG1899773
2-Chloronaphthalene 91-58-7 0.500 U 0.0648 0.500 1.00 1 07/23/2022 18:32 WG1899773
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 15:39 38 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 16:01 38 of 65
====================----□ □ □ □
□ □ □ □
SAMPLE RESULTS - 11
L1516722
USTTC341-MW13
Collected date/time: 07/18/22 13:25
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
4-Chlorophenyl-phenylether 7005-72-3 5.00 U 0.0926 5.00 10.0 1 07/23/2022 18:32 WG1899773
Chrysene 218-01-9 0.500 U 0.130 0.500 1.00 1 07/23/2022 18:32 WG1899773
Dibenz(a,h)anthracene 53-70-3 0.500 U 0.0644 0.500 1.00 1 07/23/2022 18:32 WG1899773
3,3-Dichlorobenzidine 91-94-1 5.00 U 0.212 5.00 10.0 1 07/23/2022 18:32 WG1899773
2,4-Dinitrotoluene 121-14-2 5.00 U 0.0983 5.00 10.0 1 07/23/2022 18:32 WG1899773
2,6-Dinitrotoluene 606-20-2 5.00 U 0.250 5.00 10.0 1 07/23/2022 18:32 WG1899773
Fluoranthene 206-44-0 0.500 U 0.102 0.500 1.00 1 07/23/2022 18:32 WG1899773
Fluorene 86-73-7 0.500 U 0.0844 0.500 1.00 1 07/23/2022 18:32 WG1899773
Hexachlorobenzene 118-74-1 0.500 U 0.0755 0.500 1.00 1 07/23/2022 18:32 WG1899773
Hexachloro-1,3-butadiene 87-68-3 5.00 U 0.0968 5.00 10.0 1 07/23/2022 18:32 WG1899773
Hexachlorocyclopentadiene 77-47-4 5.00 U 0.0598 5.00 10.0 1 07/23/2022 18:32 WG1899773
Hexachloroethane 67-72-1 5.00 U 0.127 5.00 10.0 1 07/23/2022 18:32 WG1899773
Indeno(1,2,3-cd)pyrene 193-39-5 0.600 U 0.279 0.600 1.20 1 07/23/2022 18:32 WG1899773
Isophorone 78-59-1 5.00 U 0.143 5.00 10.0 1 07/23/2022 18:32 WG1899773
Naphthalene 91-20-3 0.500 J4 U 0.159 0.500 1.00 1 07/23/2022 18:32 WG1899773
Nitrobenzene 98-95-3 5.00 J4 U 0.297 5.00 10.0 1 07/23/2022 18:32 WG1899773
n-Nitrosodimethylamine 62-75-9 5.00 U 0.998 5.00 10.0 1 07/23/2022 18:32 WG1899773
n-Nitrosodiphenylamine 86-30-6 5.00 J4 U 2.37 5.00 10.0 1 07/23/2022 18:32 WG1899773
n-Nitrosodi-n-propylamine 621-64-7 5.00 J4 U 0.261 5.00 10.0 1 07/23/2022 18:32 WG1899773
Phenanthrene 85-01-8 0.500 J4 U 0.112 0.500 1.00 1 07/23/2022 18:32 WG1899773
Benzylbutyl phthalate 85-68-7 2.00 U 0.765 2.00 4.00 1 07/23/2022 18:32 WG1899773
Bis(2-ethylhexyl)phthalate 117-81-7 2.00 U 0.895 2.00 4.00 1 07/23/2022 18:32 WG1899773
Di-n-butyl phthalate 84-74-2 1.50 U 0.453 1.50 3.00 1 07/23/2022 18:32 WG1899773
Diethyl phthalate 84-66-2 1.50 U 0.287 1.50 3.00 1 07/23/2022 18:32 WG1899773
Dimethyl phthalate 131-11-3 1.50 U 0.260 1.50 3.00 1 07/23/2022 18:32 WG1899773
Di-n-octyl phthalate 117-84-0 2.00 U 0.932 2.00 4.00 1 07/23/2022 18:32 WG1899773
Pyrene 129-00-0 0.500 J4 U 0.107 0.500 1.00 1 07/23/2022 18:32 WG1899773
1,2,4-Trichlorobenzene 120-82-1 5.00 U 0.0698 5.00 10.0 1 07/23/2022 18:32 WG1899773
4-Chloro-3-methylphenol 59-50-7 5.00 U 0.131 5.00 10.0 1 07/23/2022 18:32 WG1899773
2-Chlorophenol 95-57-8 5.00 J4 U 0.133 5.00 10.0 1 07/23/2022 18:32 WG1899773
2,4-Dichlorophenol 120-83-2 5.00 J4 U 0.102 5.00 10.0 1 07/23/2022 18:32 WG1899773
2,4-Dimethylphenol 105-67-9 5.00 U 0.0636 5.00 10.0 1 07/23/2022 18:32 WG1899773
4,6-Dinitro-2-methylphenol 534-52-1 5.00 U 1.12 5.00 10.0 1 07/23/2022 18:32 WG1899773
2,4-Dinitrophenol 51-28-5 15.0 U 5.93 15.0 30.0 1 07/23/2022 18:32 WG1899773
2-Nitrophenol 88-75-5 5.00 J4 U 0.117 5.00 10.0 1 07/23/2022 18:32 WG1899773
4-Nitrophenol 100-02-7 5.00 U 0.143 5.00 10.0 1 07/23/2022 18:32 WG1899773
Pentachlorophenol 87-86-5 5.00 U 0.313 5.00 10.0 1 07/23/2022 18:32 WG1899773
Phenol 108-95-2 10.0 U 4.33 10.0 20.0 1 07/23/2022 18:32 WG1899773
2,4,6-Trichlorophenol 88-06-2 5.00 U 0.100 5.00 10.0 1 07/23/2022 18:32 WG1899773
1-Methylnaphthalene 90-12-0 0.500 U 0.0790 0.500 1.00 1 07/23/2022 18:32 WG1899773
2-Methylnaphthalene 91-57-6 0.500 U 0.117 0.500 1.00 1 07/23/2022 18:32 WG1899773
(S) Nitrobenzene-d5 4165-60-0 23.7 J2 0.000 44.0-120 07/23/2022 18:32 WG1899773
(S) 2-Fluorobiphenyl 321-60-8 28.7 J2 0.000 44.0-119 07/23/2022 18:32 WG1899773
(S) p-Terphenyl-d14 1718-51-0 58.2 0.000 50.0-134 07/23/2022 18:32 WG1899773
(S) Phenol-d5 4165-62-2 12.5 0.000 10.0-67.0 07/23/2022 18:32 WG1899773
(S) 2-Fluorophenol 367-12-4 18.0 J2 0.000 19.0-119 07/23/2022 18:32 WG1899773
(S) 2,4,6-Tribromophenol 118-79-6 55.5 0.000 43.0-140 07/23/2022 18:32 WG1899773
Sample Narrative:
L1516722-11 WG1899773: Duplicate Analysis performed due to surrogate failure. Results confirm; reporting in hold data
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 15:39 39 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 16:01 39 of 65
====================----□ □ □ □
□ □ □ □
SAMPLE RESULTS - 12
L1516722
USTG480-MW06
Collected date/time: 07/18/22 14:02
Volatile Petroleum Hydrocarbons by Method MADEPV
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics C5-C8 ALI
UNADJ 387 33.3 67.0 134 1 07/31/2022 22:23 WG1903201
Unadjusted C9-C12 Aliphatics C9-C12 ALI
UNADJ 1130 33.3 67.0 134 1 07/31/2022 22:23 WG1903201
Unadjusted C9-C10 Aromatics C9-C10 ARO
UNADJ 815 33.3 67.0 134 1 07/31/2022 22:23 WG1903201
Total VPH VPH 2330 66.7 150 300 1 07/31/2022 22:23 WG1903201
(S) 2,5-Dibromotoluene(FID)615-59-8 116 70.0-130 07/31/2022 22:23 WG1903201
(S) 2,5-Dibromotoluene(PID)615-59-8 87.6 70.0-130 07/31/2022 22:23 WG1903201
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acetone 67-64-1 625 U 282 625 1250 25 07/23/2022 18:57 WG1899800
Acrolein 107-02-8 625 U 63.5 625 1250 25 07/23/2022 18:57 WG1899800
Acrylonitrile 107-13-1 125 U 16.8 125 250 25 07/23/2022 18:57 WG1899800
Benzene 71-43-2 148 2.35 12.5 25.0 25 07/23/2022 18:57 WG1899800
Bromobenzene 108-86-1 12.5 C4 J4 U 2.95 12.5 25.0 25 07/23/2022 18:57 WG1899800
Bromodichloromethane 75-27-4 12.5 U 3.40 12.5 25.0 25 07/23/2022 18:57 WG1899800
Bromoform 75-25-2 12.5 U 3.22 12.5 25.0 25 07/23/2022 18:57 WG1899800
Bromomethane 74-83-9 50.0 U 15.1 50.0 125 25 07/23/2022 18:57 WG1899800
n-Butylbenzene 104-51-8 12.5 U 3.93 12.5 25.0 25 07/23/2022 18:57 WG1899800
sec-Butylbenzene 135-98-8 12.5 U 3.13 12.5 25.0 25 07/23/2022 18:57 WG1899800
tert-Butylbenzene 98-06-6 12.5 U 3.18 12.5 25.0 25 07/23/2022 18:57 WG1899800
Carbon tetrachloride 56-23-5 12.5 U 3.20 12.5 25.0 25 07/23/2022 18:57 WG1899800
Chlorobenzene 108-90-7 12.5 U 2.90 12.5 25.0 25 07/23/2022 18:57 WG1899800
Chlorodibromomethane 124-48-1 12.5 U 3.50 12.5 25.0 25 07/23/2022 18:57 WG1899800
Chloroethane 75-00-3 50.0 U 4.80 50.0 125 25 07/23/2022 18:57 WG1899800
Chloroform 67-66-3 50.0 U 2.78 50.0 125 25 07/23/2022 18:57 WG1899800
Chloromethane 74-87-3 50.0 U 24.0 50.0 100 25 07/23/2022 18:57 WG1899800
2-Chlorotoluene 95-49-8 4.66 J 2.65 12.5 25.0 25 07/23/2022 18:57 WG1899800
4-Chlorotoluene 106-43-4 12.5 U 2.85 12.5 25.0 25 07/23/2022 18:57 WG1899800
1,2-Dibromo-3-Chloropropane 96-12-8 50.0 U 6.90 50.0 125 25 07/23/2022 18:57 WG1899800
1,2-Dibromoethane 106-93-4 12.5 U 3.15 12.5 25.0 25 07/23/2022 18:57 WG1899800
Dibromomethane 74-95-3 12.5 U 3.05 12.5 25.0 25 07/23/2022 18:57 WG1899800
1,2-Dichlorobenzene 95-50-1 12.5 U 2.68 12.5 25.0 25 07/23/2022 18:57 WG1899800
1,3-Dichlorobenzene 541-73-1 12.5 U 2.75 12.5 25.0 25 07/23/2022 18:57 WG1899800
1,4-Dichlorobenzene 106-46-7 12.5 U 3.00 12.5 25.0 25 07/23/2022 18:57 WG1899800
Dichlorodifluoromethane 75-71-8 50.0 U 9.35 50.0 125 25 07/23/2022 18:57 WG1899800
1,1-Dichloroethane 75-34-3 12.5 U 2.50 12.5 25.0 25 07/23/2022 18:57 WG1899800
1,2-Dichloroethane 107-06-2 12.5 U 2.05 12.5 25.0 25 07/23/2022 18:57 WG1899800
1,1-Dichloroethene 75-35-4 12.5 U 4.70 12.5 25.0 25 07/23/2022 18:57 WG1899800
cis-1,2-Dichloroethene 156-59-2 12.5 U 3.15 12.5 25.0 25 07/23/2022 18:57 WG1899800
trans-1,2-Dichloroethene 156-60-5 12.5 U 3.73 12.5 25.0 25 07/23/2022 18:57 WG1899800
1,2-Dichloropropane 78-87-5 12.5 U 3.73 12.5 25.0 25 07/23/2022 18:57 WG1899800
1,1-Dichloropropene 563-58-6 12.5 U 3.55 12.5 25.0 25 07/23/2022 18:57 WG1899800
1,3-Dichloropropane 142-28-9 12.5 U 2.75 12.5 25.0 25 07/23/2022 18:57 WG1899800
2,2-Dichloropropane 594-20-7 12.5 U 4.03 12.5 25.0 25 07/23/2022 18:57 WG1899800
Di-isopropyl ether 108-20-3 12.5 U 2.63 12.5 25.0 25 07/23/2022 18:57 WG1899800
Ethylbenzene 100-41-4 192 3.43 12.5 25.0 25 07/23/2022 18:57 WG1899800
Hexachloro-1,3-butadiene 87-68-3 18.8 U 8.43 18.8 37.5 25 07/23/2022 18:57 WG1899800
Isopropylbenzene 98-82-8 21.2 J 2.63 12.5 25.0 25 07/23/2022 18:57 WG1899800
p-Isopropyltoluene 99-87-6 12.5 J 3.00 12.5 25.0 25 07/23/2022 18:57 WG1899800
2-Butanone (MEK)78-93-3 125 U 29.8 125 250 25 07/23/2022 18:57 WG1899800
Methylene Chloride 75-09-2 50.0 U 10.7 50.0 125 25 07/23/2022 18:57 WG1899800
4-Methyl-2-pentanone (MIBK)108-10-1 125 U 12.0 125 250 25 07/23/2022 18:57 WG1899800
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 15:39 40 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 16:01 40 of 65
--------------=---□
□ □ □
==============~~~~~=----□ □ □ □
SAMPLE RESULTS - 12
L1516722
USTG480-MW06
Collected date/time: 07/18/22 14:02
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Methyl tert-butyl ether 1634-04-4 12.5 U 2.53 12.5 25.0 25 07/23/2022 18:57 WG1899800
Naphthalene 91-20-3 319 25.0 50.0 125 25 07/23/2022 18:57 WG1899800
n-Propylbenzene 103-65-1 27.2 C4 J4 2.48 12.5 25.0 25 07/23/2022 18:57 WG1899800
Styrene 100-42-5 12.5 U 2.95 12.5 25.0 25 07/23/2022 18:57 WG1899800
1,1,1,2-Tetrachloroethane 630-20-6 12.5 U 3.68 12.5 25.0 25 07/23/2022 18:57 WG1899800
1,1,2,2-Tetrachloroethane 79-34-5 12.5 U 3.33 12.5 25.0 25 07/23/2022 18:57 WG1899800
Tetrachloroethene 127-18-4 15.0 U 7.50 15.0 30.0 25 07/23/2022 18:57 WG1899800
Toluene 108-88-3 15.0 U 6.95 15.0 30.0 25 07/23/2022 18:57 WG1899800
1,2,3-Trichlorobenzene 87-61-6 12.5 C4 U 5.75 12.5 25.0 25 07/23/2022 18:57 WG1899800
1,2,4-Trichlorobenzene 120-82-1 25.0 U 12.0 25.0 50.0 25 07/23/2022 18:57 WG1899800
1,1,1-Trichloroethane 71-55-6 12.5 U 3.73 12.5 25.0 25 07/23/2022 18:57 WG1899800
1,1,2-Trichloroethane 79-00-5 12.5 U 3.95 12.5 25.0 25 07/23/2022 18:57 WG1899800
Trichloroethene 79-01-6 12.5 U 4.75 12.5 25.0 25 07/23/2022 18:57 WG1899800
Trichlorofluoromethane 75-69-4 50.0 U 4.00 50.0 125 25 07/23/2022 18:57 WG1899800
1,2,3-Trichloropropane 96-18-4 25.0 U 5.93 25.0 62.5 25 07/23/2022 18:57 WG1899800
1,2,4-Trimethylbenzene 95-63-6 147 8.05 25.0 50.0 25 07/23/2022 18:57 WG1899800
1,3,5-Trimethylbenzene 108-67-8 41.6 2.60 12.5 25.0 25 07/23/2022 18:57 WG1899800
Vinyl chloride 75-01-4 12.5 U 5.85 12.5 25.0 25 07/23/2022 18:57 WG1899800
o-Xylene 95-47-6 12.5 U 4.35 12.5 25.0 25 07/23/2022 18:57 WG1899800
m&p-Xylenes 1330-20-7 267 10.7 25.0 50.0 25 07/23/2022 18:57 WG1899800
(S) Toluene-d8 2037-26-5 102 89.0-112 07/23/2022 18:57 WG1899800
(S) 4-Bromofluorobenzene 460-00-4 86.7 85.0-114 07/23/2022 18:57 WG1899800
(S) 1,2-Dichloroethane-d4 17060-07-0 94.3 81.0-118 07/23/2022 18:57 WG1899800
TPH by Method MADEPE
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics C9-C18 ALI
UNADJ 63.8 J 33.3 67.0 134 1 08/01/2022 18:24 WG1902750
Unadjusted C19-C36 Aliphatics C19-C36 ALI
UNADJ 67.0 U 33.3 67.0 134 1 08/01/2022 18:24 WG1902750
Unadjusted C11-C22 Aromatics C11-C22 ARO
UNADJ 1030 33.3 67.0 134 1 08/01/2022 11:42 WG1902750
Unadjusted Total Petroleum
Hydrocarbons TPH UNADJ 1090 33.3 67.0 134 1 08/01/2022 18:24 WG1902750
(S) o-Terphenyl 84-15-1 83.5 40.0-140 08/01/2022 11:42 WG1902750
(S) 1-Chloro-octadecane 3386-33-2 72.4 40.0-140 08/01/2022 18:24 WG1902750
(S) 2-Fluorobiphenyl 321-60-8 91.1 40.0-140 08/01/2022 11:42 WG1902750
(S) 2-Bromonaphthalene 580-13-2 91.7 40.0-140 08/01/2022 11:42 WG1902750
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acenaphthene 83-32-9 0.972 J J4 0.0886 0.500 1.00 1 07/23/2022 19:16 WG1899773
Acenaphthylene 208-96-8 0.500 U 0.0921 0.500 1.00 1 07/23/2022 19:16 WG1899773
Anthracene 120-12-7 0.500 J4 U 0.0804 0.500 1.00 1 07/23/2022 19:16 WG1899773
Benzidine 92-87-5 7.50 U 3.74 7.50 15.0 1 07/23/2022 19:16 WG1899773
Benzo(a)anthracene 56-55-3 0.500 U 0.199 0.500 1.00 1 07/23/2022 19:16 WG1899773
Benzo(b)fluoranthene 205-99-2 0.500 U 0.130 0.500 1.00 1 07/23/2022 19:16 WG1899773
Benzo(k)fluoranthene 207-08-9 0.500 U 0.120 0.500 1.00 1 07/23/2022 19:16 WG1899773
Benzo(g,h,i)perylene 191-24-2 0.500 U 0.121 0.500 1.00 1 07/23/2022 19:16 WG1899773
Benzo(a)pyrene 50-32-8 0.500 U 0.0381 0.500 1.00 1 07/23/2022 19:16 WG1899773
Bis(2-chlorethoxy)methane 111-91-1 5.00 J4 U 0.116 5.00 10.0 1 07/23/2022 19:16 WG1899773
Bis(2-chloroethyl)ether 111-44-4 5.00 J4 U 0.137 5.00 10.0 1 07/23/2022 19:16 WG1899773
2,2-Oxybis(1-Chloropropane)108-60-1 5.00 J4 U 0.210 5.00 10.0 1 07/23/2022 19:16 WG1899773
4-Bromophenyl-phenylether 101-55-3 5.00 U 0.0877 5.00 10.0 1 07/23/2022 19:16 WG1899773
2-Chloronaphthalene 91-58-7 0.500 U 0.0648 0.500 1.00 1 07/23/2022 19:16 WG1899773
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 15:39 41 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 16:01 41 of 65
====================----□ □ □ □
□ □ □ □
SAMPLE RESULTS - 12
L1516722
USTG480-MW06
Collected date/time: 07/18/22 14:02
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
4-Chlorophenyl-phenylether 7005-72-3 5.00 U 0.0926 5.00 10.0 1 07/23/2022 19:16 WG1899773
Chrysene 218-01-9 0.500 U 0.130 0.500 1.00 1 07/23/2022 19:16 WG1899773
Dibenz(a,h)anthracene 53-70-3 0.500 U 0.0644 0.500 1.00 1 07/23/2022 19:16 WG1899773
3,3-Dichlorobenzidine 91-94-1 5.00 U 0.212 5.00 10.0 1 07/23/2022 19:16 WG1899773
2,4-Dinitrotoluene 121-14-2 5.00 U 0.0983 5.00 10.0 1 07/23/2022 19:16 WG1899773
2,6-Dinitrotoluene 606-20-2 5.00 U 0.250 5.00 10.0 1 07/23/2022 19:16 WG1899773
Fluoranthene 206-44-0 0.500 U 0.102 0.500 1.00 1 07/23/2022 19:16 WG1899773
Fluorene 86-73-7 0.711 J 0.0844 0.500 1.00 1 07/23/2022 19:16 WG1899773
Hexachlorobenzene 118-74-1 0.500 U 0.0755 0.500 1.00 1 07/23/2022 19:16 WG1899773
Hexachloro-1,3-butadiene 87-68-3 5.00 U 0.0968 5.00 10.0 1 07/23/2022 19:16 WG1899773
Hexachlorocyclopentadiene 77-47-4 5.00 U 0.0598 5.00 10.0 1 07/23/2022 19:16 WG1899773
Hexachloroethane 67-72-1 5.00 U 0.127 5.00 10.0 1 07/23/2022 19:16 WG1899773
Indeno(1,2,3-cd)pyrene 193-39-5 0.600 U 0.279 0.600 1.20 1 07/23/2022 19:16 WG1899773
Isophorone 78-59-1 5.00 U 0.143 5.00 10.0 1 07/23/2022 19:16 WG1899773
Naphthalene 91-20-3 59.1 J4 0.159 0.500 1.00 1 07/23/2022 19:16 WG1899773
Nitrobenzene 98-95-3 5.00 J4 U 0.297 5.00 10.0 1 07/23/2022 19:16 WG1899773
n-Nitrosodimethylamine 62-75-9 5.00 U 0.998 5.00 10.0 1 07/23/2022 19:16 WG1899773
n-Nitrosodiphenylamine 86-30-6 5.00 J4 U 2.37 5.00 10.0 1 07/23/2022 19:16 WG1899773
n-Nitrosodi-n-propylamine 621-64-7 5.00 J4 U 0.261 5.00 10.0 1 07/23/2022 19:16 WG1899773
Phenanthrene 85-01-8 0.407 J J4 0.112 0.500 1.00 1 07/23/2022 19:16 WG1899773
Benzylbutyl phthalate 85-68-7 2.00 U 0.765 2.00 4.00 1 07/23/2022 19:16 WG1899773
Bis(2-ethylhexyl)phthalate 117-81-7 2.00 U 0.895 2.00 4.00 1 07/23/2022 19:16 WG1899773
Di-n-butyl phthalate 84-74-2 1.50 U 0.453 1.50 3.00 1 07/23/2022 19:16 WG1899773
Diethyl phthalate 84-66-2 1.50 U 0.287 1.50 3.00 1 07/23/2022 19:16 WG1899773
Dimethyl phthalate 131-11-3 1.50 U 0.260 1.50 3.00 1 07/23/2022 19:16 WG1899773
Di-n-octyl phthalate 117-84-0 2.00 U 0.932 2.00 4.00 1 07/23/2022 19:16 WG1899773
Pyrene 129-00-0 0.500 J4 U 0.107 0.500 1.00 1 07/23/2022 19:16 WG1899773
1,2,4-Trichlorobenzene 120-82-1 5.00 U 0.0698 5.00 10.0 1 07/23/2022 19:16 WG1899773
4-Chloro-3-methylphenol 59-50-7 5.00 U 0.131 5.00 10.0 1 07/23/2022 19:16 WG1899773
2-Chlorophenol 95-57-8 5.00 J4 U 0.133 5.00 10.0 1 07/23/2022 19:16 WG1899773
2,4-Dichlorophenol 120-83-2 5.00 J4 U 0.102 5.00 10.0 1 07/23/2022 19:16 WG1899773
2,4-Dimethylphenol 105-67-9 0.509 J 0.0636 5.00 10.0 1 07/23/2022 19:16 WG1899773
4,6-Dinitro-2-methylphenol 534-52-1 5.00 U 1.12 5.00 10.0 1 07/23/2022 19:16 WG1899773
2,4-Dinitrophenol 51-28-5 15.0 U 5.93 15.0 30.0 1 07/23/2022 19:16 WG1899773
2-Nitrophenol 88-75-5 5.00 J4 U 0.117 5.00 10.0 1 07/23/2022 19:16 WG1899773
4-Nitrophenol 100-02-7 5.00 U 0.143 5.00 10.0 1 07/23/2022 19:16 WG1899773
Pentachlorophenol 87-86-5 5.00 U 0.313 5.00 10.0 1 07/23/2022 19:16 WG1899773
Phenol 108-95-2 10.0 U 4.33 10.0 20.0 1 07/23/2022 19:16 WG1899773
2,4,6-Trichlorophenol 88-06-2 5.00 U 0.100 5.00 10.0 1 07/23/2022 19:16 WG1899773
1-Methylnaphthalene 90-12-0 26.4 0.0790 0.500 1.00 1 07/23/2022 19:16 WG1899773
2-Methylnaphthalene 91-57-6 36.2 0.117 0.500 1.00 1 07/23/2022 19:16 WG1899773
(S) Nitrobenzene-d5 4165-60-0 25.5 J2 0.000 44.0-120 07/23/2022 19:16 WG1899773
(S) 2-Fluorobiphenyl 321-60-8 25.6 J2 0.000 44.0-119 07/23/2022 19:16 WG1899773
(S) p-Terphenyl-d14 1718-51-0 39.8 J2 0.000 50.0-134 07/23/2022 19:16 WG1899773
(S) Phenol-d5 4165-62-2 7.58 J2 0.000 10.0-67.0 07/23/2022 19:16 WG1899773
(S) 2-Fluorophenol 367-12-4 10.5 J2 0.000 19.0-119 07/23/2022 19:16 WG1899773
(S) 2,4,6-Tribromophenol 118-79-6 48.2 0.000 43.0-140 07/23/2022 19:16 WG1899773
Sample Narrative:
L1516722-12 WG1899773: Sample produced heavy emulsion during Extraction process, low surr/spike recoveries due to matrix
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 15:39 42 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 16:01 42 of 65
====================----□ □ □ □
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SAMPLE RESULTS - 13
L1516722
USTG480-MW23
Collected date/time: 07/18/22 14:04
Volatile Petroleum Hydrocarbons by Method MADEPV
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics C5-C8 ALI
UNADJ 670 U 333 670 1000 10 07/30/2022 05:09 WG1902102
Unadjusted C9-C12 Aliphatics C9-C12 ALI
UNADJ 708 B J 333 670 1340 10 07/30/2022 05:09 WG1902102
Unadjusted C9-C10 Aromatics C9-C10 ARO
UNADJ 670 U 333 670 1000 10 07/30/2022 05:09 WG1902102
Total VPH VPH 708 J 667 1500 3000 10 07/30/2022 05:09 WG1902102
(S) 2,5-Dibromotoluene(FID)615-59-8 105 70.0-130 07/30/2022 05:09 WG1902102
(S) 2,5-Dibromotoluene(PID)615-59-8 103 70.0-130 07/30/2022 05:09 WG1902102
Sample Narrative:
L1516722-13 WG1902102: Lowest possible dilution due to sample foaming.
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acetone 67-64-1 250 U 113 250 500 10 07/23/2022 19:17 WG1899800
Acrolein 107-02-8 250 U 25.4 250 500 10 07/23/2022 19:17 WG1899800
Acrylonitrile 107-13-1 50.0 U 6.71 50.0 100 10 07/23/2022 19:17 WG1899800
Benzene 71-43-2 5.00 U 0.941 5.00 10.0 10 07/23/2022 19:17 WG1899800
Bromobenzene 108-86-1 5.00 C4 J4 U 1.18 5.00 10.0 10 07/23/2022 19:17 WG1899800
Bromodichloromethane 75-27-4 5.00 U 1.36 5.00 10.0 10 07/23/2022 19:17 WG1899800
Bromoform 75-25-2 5.00 U 1.29 5.00 10.0 10 07/23/2022 19:17 WG1899800
Bromomethane 74-83-9 20.0 U 6.05 20.0 50.0 10 07/23/2022 19:17 WG1899800
n-Butylbenzene 104-51-8 5.00 U 1.57 5.00 10.0 10 07/23/2022 19:17 WG1899800
sec-Butylbenzene 135-98-8 5.00 U 1.25 5.00 10.0 10 07/23/2022 19:17 WG1899800
tert-Butylbenzene 98-06-6 5.00 U 1.27 5.00 10.0 10 07/23/2022 19:17 WG1899800
Carbon tetrachloride 56-23-5 5.00 U 1.28 5.00 10.0 10 07/23/2022 19:17 WG1899800
Chlorobenzene 108-90-7 5.00 U 1.16 5.00 10.0 10 07/23/2022 19:17 WG1899800
Chlorodibromomethane 124-48-1 5.00 U 1.40 5.00 10.0 10 07/23/2022 19:17 WG1899800
Chloroethane 75-00-3 20.0 U 1.92 20.0 50.0 10 07/23/2022 19:17 WG1899800
Chloroform 67-66-3 20.0 U 1.11 20.0 50.0 10 07/23/2022 19:17 WG1899800
Chloromethane 74-87-3 20.0 U 9.60 20.0 40.0 10 07/23/2022 19:17 WG1899800
2-Chlorotoluene 95-49-8 5.00 U 1.06 5.00 10.0 10 07/23/2022 19:17 WG1899800
4-Chlorotoluene 106-43-4 5.00 U 1.14 5.00 10.0 10 07/23/2022 19:17 WG1899800
1,2-Dibromo-3-Chloropropane 96-12-8 20.0 U 2.76 20.0 50.0 10 07/23/2022 19:17 WG1899800
1,2-Dibromoethane 106-93-4 5.00 U 1.26 5.00 10.0 10 07/23/2022 19:17 WG1899800
Dibromomethane 74-95-3 5.00 U 1.22 5.00 10.0 10 07/23/2022 19:17 WG1899800
1,2-Dichlorobenzene 95-50-1 5.00 U 1.07 5.00 10.0 10 07/23/2022 19:17 WG1899800
1,3-Dichlorobenzene 541-73-1 5.00 U 1.10 5.00 10.0 10 07/23/2022 19:17 WG1899800
1,4-Dichlorobenzene 106-46-7 5.00 U 1.20 5.00 10.0 10 07/23/2022 19:17 WG1899800
Dichlorodifluoromethane 75-71-8 20.0 U 3.74 20.0 50.0 10 07/23/2022 19:17 WG1899800
1,1-Dichloroethane 75-34-3 5.00 U 1.00 5.00 10.0 10 07/23/2022 19:17 WG1899800
1,2-Dichloroethane 107-06-2 5.00 U 0.819 5.00 10.0 10 07/23/2022 19:17 WG1899800
1,1-Dichloroethene 75-35-4 5.00 U 1.88 5.00 10.0 10 07/23/2022 19:17 WG1899800
cis-1,2-Dichloroethene 156-59-2 5.00 U 1.26 5.00 10.0 10 07/23/2022 19:17 WG1899800
trans-1,2-Dichloroethene 156-60-5 5.00 U 1.49 5.00 10.0 10 07/23/2022 19:17 WG1899800
1,2-Dichloropropane 78-87-5 5.00 U 1.49 5.00 10.0 10 07/23/2022 19:17 WG1899800
1,1-Dichloropropene 563-58-6 5.00 U 1.42 5.00 10.0 10 07/23/2022 19:17 WG1899800
1,3-Dichloropropane 142-28-9 5.00 U 1.10 5.00 10.0 10 07/23/2022 19:17 WG1899800
2,2-Dichloropropane 594-20-7 5.00 U 1.61 5.00 10.0 10 07/23/2022 19:17 WG1899800
Di-isopropyl ether 108-20-3 5.00 U 1.05 5.00 10.0 10 07/23/2022 19:17 WG1899800
Ethylbenzene 100-41-4 5.38 J 1.37 5.00 10.0 10 07/23/2022 19:17 WG1899800
Hexachloro-1,3-butadiene 87-68-3 7.50 U 3.37 7.50 15.0 10 07/23/2022 19:17 WG1899800
Isopropylbenzene 98-82-8 6.61 J 1.05 5.00 10.0 10 07/23/2022 19:17 WG1899800
p-Isopropyltoluene 99-87-6 5.00 U 1.20 5.00 10.0 10 07/23/2022 19:17 WG1899800
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 15:39 43 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 16:01 43 of 65
--------------=---□
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□
SAMPLE RESULTS - 13
L1516722
USTG480-MW23
Collected date/time: 07/18/22 14:04
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
2-Butanone (MEK)78-93-3 50.0 U 11.9 50.0 100 10 07/23/2022 19:17 WG1899800
Methylene Chloride 75-09-2 20.0 U 4.30 20.0 50.0 10 07/23/2022 19:17 WG1899800
4-Methyl-2-pentanone (MIBK)108-10-1 50.0 U 4.78 50.0 100 10 07/23/2022 19:17 WG1899800
Methyl tert-butyl ether 1634-04-4 5.00 U 1.01 5.00 10.0 10 07/23/2022 19:17 WG1899800
Naphthalene 91-20-3 136 10.0 20.0 50.0 10 07/23/2022 19:17 WG1899800
n-Propylbenzene 103-65-1 9.89 C4 J J4 0.993 5.00 10.0 10 07/23/2022 19:17 WG1899800
Styrene 100-42-5 5.00 U 1.18 5.00 10.0 10 07/23/2022 19:17 WG1899800
1,1,1,2-Tetrachloroethane 630-20-6 5.00 U 1.47 5.00 10.0 10 07/23/2022 19:17 WG1899800
1,1,2,2-Tetrachloroethane 79-34-5 5.00 U 1.33 5.00 10.0 10 07/23/2022 19:17 WG1899800
Tetrachloroethene 127-18-4 6.00 U 3.00 6.00 12.0 10 07/23/2022 19:17 WG1899800
Toluene 108-88-3 6.00 U 2.78 6.00 12.0 10 07/23/2022 19:17 WG1899800
1,2,3-Trichlorobenzene 87-61-6 5.00 C4 U 2.30 5.00 10.0 10 07/23/2022 19:17 WG1899800
1,2,4-Trichlorobenzene 120-82-1 10.0 U 4.81 10.0 20.0 10 07/23/2022 19:17 WG1899800
1,1,1-Trichloroethane 71-55-6 5.00 U 1.49 5.00 10.0 10 07/23/2022 19:17 WG1899800
1,1,2-Trichloroethane 79-00-5 5.00 U 1.58 5.00 10.0 10 07/23/2022 19:17 WG1899800
Trichloroethene 79-01-6 5.00 U 1.90 5.00 10.0 10 07/23/2022 19:17 WG1899800
Trichlorofluoromethane 75-69-4 20.0 U 1.60 20.0 50.0 10 07/23/2022 19:17 WG1899800
1,2,3-Trichloropropane 96-18-4 10.0 U 2.37 10.0 25.0 10 07/23/2022 19:17 WG1899800
1,2,4-Trimethylbenzene 95-63-6 10.6 J 3.22 10.0 20.0 10 07/23/2022 19:17 WG1899800
1,3,5-Trimethylbenzene 108-67-8 6.06 J 1.04 5.00 10.0 10 07/23/2022 19:17 WG1899800
Vinyl chloride 75-01-4 5.00 U 2.34 5.00 10.0 10 07/23/2022 19:17 WG1899800
o-Xylene 95-47-6 5.00 U 1.74 5.00 10.0 10 07/23/2022 19:17 WG1899800
m&p-Xylenes 1330-20-7 5.98 J 4.30 10.0 20.0 10 07/23/2022 19:17 WG1899800
(S) Toluene-d8 2037-26-5 101 89.0-112 07/23/2022 19:17 WG1899800
(S) 4-Bromofluorobenzene 460-00-4 86.8 85.0-114 07/23/2022 19:17 WG1899800
(S) 1,2-Dichloroethane-d4 17060-07-0 101 81.0-118 07/23/2022 19:17 WG1899800
TPH by Method MADEPE
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics C9-C18 ALI
UNADJ 10600 333 670 1340 10 08/03/2022 08:15 WG1902750
Unadjusted C19-C36 Aliphatics C19-C36 ALI
UNADJ 1810 33.3 67.0 134 1 08/01/2022 18:46 WG1902750
Unadjusted C11-C22 Aromatics C11-C22 ARO
UNADJ 5290 33.3 67.0 134 1 08/01/2022 11:20 WG1902750
Unadjusted Total Petroleum
Hydrocarbons TPH UNADJ 17700 333 670 1340 10 08/03/2022 08:15 WG1902750
(S) o-Terphenyl 84-15-1 82.0 40.0-140 08/01/2022 11:20 WG1902750
(S) 1-Chloro-octadecane 3386-33-2 56.9 40.0-140 08/03/2022 08:15 WG1902750
(S) 1-Chloro-octadecane 3386-33-2 50.9 40.0-140 08/01/2022 18:46 WG1902750
(S) 2-Fluorobiphenyl 321-60-8 99.1 40.0-140 08/01/2022 11:20 WG1902750
(S) 2-Bromonaphthalene 580-13-2 89.0 40.0-140 08/01/2022 11:20 WG1902750
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acenaphthene 83-32-9 1.06 J4 0.0886 0.500 1.00 1 07/23/2022 19:38 WG1899773
Acenaphthylene 208-96-8 0.500 U 0.0921 0.500 1.00 1 07/23/2022 19:38 WG1899773
Anthracene 120-12-7 0.500 J4 U 0.0804 0.500 1.00 1 07/23/2022 19:38 WG1899773
Benzidine 92-87-5 7.50 U 3.74 7.50 15.0 1 07/23/2022 19:38 WG1899773
Benzo(a)anthracene 56-55-3 0.500 U 0.199 0.500 1.00 1 07/23/2022 19:38 WG1899773
Benzo(b)fluoranthene 205-99-2 0.500 U 0.130 0.500 1.00 1 07/23/2022 19:38 WG1899773
Benzo(k)fluoranthene 207-08-9 0.500 U 0.120 0.500 1.00 1 07/23/2022 19:38 WG1899773
Benzo(g,h,i)perylene 191-24-2 0.500 U 0.121 0.500 1.00 1 07/23/2022 19:38 WG1899773
Benzo(a)pyrene 50-32-8 0.500 U 0.0381 0.500 1.00 1 07/23/2022 19:38 WG1899773
Bis(2-chlorethoxy)methane 111-91-1 5.00 J4 U 0.116 5.00 10.0 1 07/23/2022 19:38 WG1899773
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 15:39 44 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 16:01 44 of 65
====================----□ □ □ □
□ □ □ □
SAMPLE RESULTS - 13
L1516722
USTG480-MW23
Collected date/time: 07/18/22 14:04
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Bis(2-chloroethyl)ether 111-44-4 5.00 J4 U 0.137 5.00 10.0 1 07/23/2022 19:38 WG1899773
2,2-Oxybis(1-Chloropropane)108-60-1 5.00 J4 U 0.210 5.00 10.0 1 07/23/2022 19:38 WG1899773
4-Bromophenyl-phenylether 101-55-3 5.00 U 0.0877 5.00 10.0 1 07/23/2022 19:38 WG1899773
2-Chloronaphthalene 91-58-7 0.500 U 0.0648 0.500 1.00 1 07/23/2022 19:38 WG1899773
4-Chlorophenyl-phenylether 7005-72-3 5.00 U 0.0926 5.00 10.0 1 07/23/2022 19:38 WG1899773
Chrysene 218-01-9 0.500 U 0.130 0.500 1.00 1 07/23/2022 19:38 WG1899773
Dibenz(a,h)anthracene 53-70-3 0.500 U 0.0644 0.500 1.00 1 07/23/2022 19:38 WG1899773
3,3-Dichlorobenzidine 91-94-1 5.00 U 0.212 5.00 10.0 1 07/23/2022 19:38 WG1899773
2,4-Dinitrotoluene 121-14-2 5.00 U 0.0983 5.00 10.0 1 07/23/2022 19:38 WG1899773
2,6-Dinitrotoluene 606-20-2 5.00 U 0.250 5.00 10.0 1 07/23/2022 19:38 WG1899773
Fluoranthene 206-44-0 0.500 U 0.102 0.500 1.00 1 07/23/2022 19:38 WG1899773
Fluorene 86-73-7 1.77 0.0844 0.500 1.00 1 07/23/2022 19:38 WG1899773
Hexachlorobenzene 118-74-1 0.500 U 0.0755 0.500 1.00 1 07/23/2022 19:38 WG1899773
Hexachloro-1,3-butadiene 87-68-3 5.00 U 0.0968 5.00 10.0 1 07/23/2022 19:38 WG1899773
Hexachlorocyclopentadiene 77-47-4 5.00 U 0.0598 5.00 10.0 1 07/23/2022 19:38 WG1899773
Hexachloroethane 67-72-1 5.00 U 0.127 5.00 10.0 1 07/23/2022 19:38 WG1899773
Indeno(1,2,3-cd)pyrene 193-39-5 0.600 U 0.279 0.600 1.20 1 07/23/2022 19:38 WG1899773
Isophorone 78-59-1 5.00 U 0.143 5.00 10.0 1 07/23/2022 19:38 WG1899773
Naphthalene 91-20-3 23.7 J4 0.159 0.500 1.00 1 07/23/2022 19:38 WG1899773
Nitrobenzene 98-95-3 5.00 J4 U 0.297 5.00 10.0 1 07/23/2022 19:38 WG1899773
n-Nitrosodimethylamine 62-75-9 5.00 U 0.998 5.00 10.0 1 07/23/2022 19:38 WG1899773
n-Nitrosodiphenylamine 86-30-6 5.00 J4 U 2.37 5.00 10.0 1 07/23/2022 19:38 WG1899773
n-Nitrosodi-n-propylamine 621-64-7 5.00 J4 U 0.261 5.00 10.0 1 07/23/2022 19:38 WG1899773
Phenanthrene 85-01-8 1.54 J4 0.112 0.500 1.00 1 07/23/2022 19:38 WG1899773
Benzylbutyl phthalate 85-68-7 2.00 U 0.765 2.00 4.00 1 07/23/2022 19:38 WG1899773
Bis(2-ethylhexyl)phthalate 117-81-7 2.00 U 0.895 2.00 4.00 1 07/23/2022 19:38 WG1899773
Di-n-butyl phthalate 84-74-2 1.50 U 0.453 1.50 3.00 1 07/23/2022 19:38 WG1899773
Diethyl phthalate 84-66-2 1.50 U 0.287 1.50 3.00 1 07/23/2022 19:38 WG1899773
Dimethyl phthalate 131-11-3 1.50 U 0.260 1.50 3.00 1 07/23/2022 19:38 WG1899773
Di-n-octyl phthalate 117-84-0 2.00 U 0.932 2.00 4.00 1 07/23/2022 19:38 WG1899773
Pyrene 129-00-0 0.500 J4 U 0.107 0.500 1.00 1 07/23/2022 19:38 WG1899773
1,2,4-Trichlorobenzene 120-82-1 5.00 U 0.0698 5.00 10.0 1 07/23/2022 19:38 WG1899773
4-Chloro-3-methylphenol 59-50-7 5.00 U 0.131 5.00 10.0 1 07/23/2022 19:38 WG1899773
2-Chlorophenol 95-57-8 5.00 J4 U 0.133 5.00 10.0 1 07/23/2022 19:38 WG1899773
2,4-Dichlorophenol 120-83-2 5.00 J4 U 0.102 5.00 10.0 1 07/23/2022 19:38 WG1899773
2,4-Dimethylphenol 105-67-9 5.00 U 0.0636 5.00 10.0 1 07/23/2022 19:38 WG1899773
4,6-Dinitro-2-methylphenol 534-52-1 5.00 U 1.12 5.00 10.0 1 07/23/2022 19:38 WG1899773
2,4-Dinitrophenol 51-28-5 15.0 U 5.93 15.0 30.0 1 07/23/2022 19:38 WG1899773
2-Nitrophenol 88-75-5 5.00 J4 U 0.117 5.00 10.0 1 07/23/2022 19:38 WG1899773
4-Nitrophenol 100-02-7 5.00 U 0.143 5.00 10.0 1 07/23/2022 19:38 WG1899773
Pentachlorophenol 87-86-5 5.00 U 0.313 5.00 10.0 1 07/23/2022 19:38 WG1899773
Phenol 108-95-2 10.0 U 4.33 10.0 20.0 1 07/23/2022 19:38 WG1899773
2,4,6-Trichlorophenol 88-06-2 5.00 U 0.100 5.00 10.0 1 07/23/2022 19:38 WG1899773
1-Methylnaphthalene 90-12-0 28.6 0.0790 0.500 1.00 1 07/23/2022 19:38 WG1899773
2-Methylnaphthalene 91-57-6 20.3 0.117 0.500 1.00 1 07/23/2022 19:38 WG1899773
(S) Nitrobenzene-d5 4165-60-0 39.5 J2 0.000 44.0-120 07/23/2022 19:38 WG1899773
(S) 2-Fluorobiphenyl 321-60-8 42.8 J2 0.000 44.0-119 07/23/2022 19:38 WG1899773
(S) p-Terphenyl-d14 1718-51-0 57.7 0.000 50.0-134 07/23/2022 19:38 WG1899773
(S) Phenol-d5 4165-62-2 15.5 0.000 10.0-67.0 07/23/2022 19:38 WG1899773
(S) 2-Fluorophenol 367-12-4 20.1 0.000 19.0-119 07/23/2022 19:38 WG1899773
(S) 2,4,6-Tribromophenol 118-79-6 64.5 0.000 43.0-140 07/23/2022 19:38 WG1899773
Sample Narrative:
L1516722-13 WG1899773: Surrogate recovery within historical limits.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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QUALITY CONTROL SUMMARYWG1899531
Volatile Petroleum Hydrocarbons by Method MADEPV L1516722-01,02,03,04,05,06,08,09,10,11
Method Blank (MB)
(MB) R3819297-3 07/23/22 14:40
MB Result MB Qualifier MB DL MB LOD MB LOQ
Analyte ug/l ug/l ug/l ug/l
Unadjusted C5-C8 Aliphatics 67.0 U 33.3 67.0 100
Unadjusted C9-C12 Aliphatics 67.0 U 33.3 67.0 134
Unadjusted C9-C10 Aromatics 67.0 U 33.3 67.0 100
Total VPH 150 U 66.7 150 300
(S) 2,5-Dibromotoluene(FID)102 70.0-130
(S) 2,5-Dibromotoluene(PID)102 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3819297-1 07/23/22 12:29 • (LCSD) R3819297-2 07/23/22 13:01
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C5-C8 Aliphatics 1200 980 1000 81.7 83.3 70.0-130 2.02 50
Unadjusted C9-C12 Aliphatics 1400 1310 1300 93.6 92.9 70.0-130 0.766 50
Unadjusted C9-C10 Aromatics 200 205 203 103 101 70.0-130 0.980 50
Total VPH 2800 2500 2500 89.3 89.3 70.0-130 0.000 50
(S) 2,5-Dibromotoluene(FID) 98.8 100 70.0-130
(S) 2,5-Dibromotoluene(PID) 100 102 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 16:01 46 of 65
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QUALITY CONTROL SUMMARYWG1901087
Volatile Petroleum Hydrocarbons by Method MADEPV L1516722-07
Method Blank (MB)
(MB) R3820885-3 07/29/22 17:09
MB Result MB Qualifier MB DL MB LOD MB LOQ
Analyte ug/l ug/l ug/l ug/l
Unadjusted C5-C8 Aliphatics 67.0 U 33.3 67.0 100
Unadjusted C9-C12 Aliphatics 40.5 J 33.3 67.0 134
Unadjusted C9-C10 Aromatics 67.0 U 33.3 67.0 100
Total VPH 150 U 66.7 150 300
(S) 2,5-Dibromotoluene(FID)89.1 70.0-130
(S) 2,5-Dibromotoluene(PID)93.1 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3820885-1 07/29/22 14:59 • (LCSD) R3820885-2 07/29/22 15:31
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C5-C8 Aliphatics 1200 1010 969 84.2 80.7 70.0-130 4.14 50
Unadjusted C9-C12 Aliphatics 1400 1190 1210 85.0 86.4 70.0-130 1.67 50
Unadjusted C9-C10 Aromatics 200 192 194 96.0 97.0 70.0-130 1.04 50
Total VPH 2800 2390 2370 85.4 84.6 70.0-130 0.840 50
(S) 2,5-Dibromotoluene(FID) 91.5 86.4 70.0-130
(S) 2,5-Dibromotoluene(PID) 93.9 90.4 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 16:01 47 of 65
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QUALITY CONTROL SUMMARYWG1902102
Volatile Petroleum Hydrocarbons by Method MADEPV L1516722-13
Method Blank (MB)
(MB) R3820886-3 07/29/22 17:09
MB Result MB Qualifier MB DL MB LOD MB LOQ
Analyte ug/l ug/l ug/l ug/l
Unadjusted C5-C8 Aliphatics 67.0 U 33.3 67.0 100
Unadjusted C9-C12 Aliphatics 40.5 J 33.3 67.0 134
Unadjusted C9-C10 Aromatics 67.0 U 33.3 67.0 100
Total VPH 150 U 66.7 150 300
(S) 2,5-Dibromotoluene(FID)89.1 70.0-130
(S) 2,5-Dibromotoluene(PID)93.1 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3820886-1 07/29/22 14:59 • (LCSD) R3820886-2 07/29/22 15:31
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C5-C8 Aliphatics 1200 1010 969 84.2 80.7 70.0-130 4.14 50
Unadjusted C9-C12 Aliphatics 1400 1190 1210 85.0 86.4 70.0-130 1.67 50
Unadjusted C9-C10 Aromatics 200 192 194 96.0 97.0 70.0-130 1.04 50
Total VPH 2800 2390 2370 85.4 84.6 70.0-130 0.840 50
(S) 2,5-Dibromotoluene(FID) 91.5 86.4 70.0-130
(S) 2,5-Dibromotoluene(PID) 93.9 90.4 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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QUALITY CONTROL SUMMARYWG1903201
Volatile Petroleum Hydrocarbons by Method MADEPV L1516722-12
Method Blank (MB)
(MB) R3821181-3 07/31/22 11:29
MB Result MB Qualifier MB DL MB LOD MB LOQ
Analyte ug/l ug/l ug/l ug/l
Unadjusted C5-C8 Aliphatics 67.0 U 33.3 67.0 134
Unadjusted C9-C12 Aliphatics 42.3 J 33.3 67.0 134
Unadjusted C9-C10 Aromatics 67.0 U 33.3 67.0 134
Total VPH 150 U 66.7 150 300
(S) 2,5-Dibromotoluene(FID)96.3 70.0-130
(S) 2,5-Dibromotoluene(PID)101 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3821181-1 07/31/22 09:18 • (LCSD) R3821181-2 07/31/22 09:51
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C5-C8 Aliphatics 1200 1100 1140 91.7 95.0 70.0-130 3.57 50
Unadjusted C9-C12 Aliphatics 1400 1150 1180 82.1 84.3 70.0-130 2.58 50
Unadjusted C9-C10 Aromatics 200 185 186 92.5 93.0 70.0-130 0.539 50
Total VPH 2800 2440 2510 87.1 89.6 70.0-130 2.83 50
(S) 2,5-Dibromotoluene(FID) 94.6 95.6 70.0-130
(S) 2,5-Dibromotoluene(PID) 95.1 95.0 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 15:39 49 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 16:01 49 of 65
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QUALITY CONTROL SUMMARYWG1899800
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1516722-01,02,03,04,05,06,07,08,09,10,11,12,13
Method Blank (MB)
(MB) R3819458-3 07/23/22 10:04
MB Result MB Qualifier MB DL MB LOD MB LOQ
Analyte ug/l ug/l ug/l ug/l
Acetone 25.0 U 11.3 25.0 50.0
Acrolein 25.0 U 2.54 25.0 50.0
Acrylonitrile 5.00 U 0.671 5.00 10.0
Benzene 0.500 U 0.0941 0.500 1.00
Bromobenzene 0.500 U 0.118 0.500 1.00
Bromodichloromethane 0.500 U 0.136 0.500 1.00
Bromoform 0.500 U 0.129 0.500 1.00
Bromomethane 2.00 U 0.605 2.00 5.00
n-Butylbenzene 0.500 U 0.157 0.500 1.00
sec-Butylbenzene 0.500 U 0.125 0.500 1.00
tert-Butylbenzene 0.500 U 0.127 0.500 1.00
Carbon tetrachloride 0.500 U 0.128 0.500 1.00
Chlorobenzene 0.500 U 0.116 0.500 1.00
Chlorodibromomethane 0.500 U 0.140 0.500 1.00
Chloroethane 2.00 U 0.192 2.00 5.00
Chloroform 2.00 U 0.111 2.00 5.00
Chloromethane 2.00 U 0.960 2.00 4.00
2-Chlorotoluene 0.500 U 0.106 0.500 1.00
4-Chlorotoluene 0.500 U 0.114 0.500 1.00
1,2-Dibromo-3-Chloropropane 2.00 U 0.276 2.00 5.00
1,2-Dibromoethane 0.500 U 0.126 0.500 1.00
Dibromomethane 0.500 U 0.122 0.500 1.00
1,2-Dichlorobenzene 0.500 U 0.107 0.500 1.00
1,3-Dichlorobenzene 0.500 U 0.110 0.500 1.00
1,4-Dichlorobenzene 0.500 U 0.120 0.500 1.00
Dichlorodifluoromethane 2.00 U 0.374 2.00 5.00
1,1-Dichloroethane 0.500 U 0.100 0.500 1.00
1,2-Dichloroethane 0.500 U 0.0819 0.500 1.00
1,1-Dichloroethene 0.500 U 0.188 0.500 1.00
cis-1,2-Dichloroethene 0.500 U 0.126 0.500 1.00
trans-1,2-Dichloroethene 0.500 U 0.149 0.500 1.00
1,2-Dichloropropane 0.500 U 0.149 0.500 1.00
1,1-Dichloropropene 0.500 U 0.142 0.500 1.00
1,3-Dichloropropane 0.500 U 0.110 0.500 1.00
2,2-Dichloropropane 0.500 U 0.161 0.500 1.00
Di-isopropyl ether 0.500 U 0.105 0.500 1.00
Ethylbenzene 0.500 U 0.137 0.500 1.00
Hexachloro-1,3-butadiene 0.750 U 0.337 0.750 1.50
Isopropylbenzene 0.500 U 0.105 0.500 1.00
p-Isopropyltoluene 0.500 U 0.120 0.500 1.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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QUALITY CONTROL SUMMARYWG1899800
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1516722-01,02,03,04,05,06,07,08,09,10,11,12,13
Method Blank (MB)
(MB) R3819458-3 07/23/22 10:04
MB Result MB Qualifier MB DL MB LOD MB LOQ
Analyte ug/l ug/l ug/l ug/l
2-Butanone (MEK)5.00 U 1.19 5.00 10.0
Methylene Chloride 2.00 U 0.430 2.00 5.00
4-Methyl-2-pentanone (MIBK)5.00 U 0.478 5.00 10.0
Methyl tert-butyl ether 0.500 U 0.101 0.500 1.00
Naphthalene 2.00 U 1.00 2.00 5.00
n-Propylbenzene 0.500 U 0.0993 0.500 1.00
Styrene 0.500 U 0.118 0.500 1.00
1,1,1,2-Tetrachloroethane 0.500 U 0.147 0.500 1.00
1,1,2,2-Tetrachloroethane 0.500 U 0.133 0.500 1.00
Tetrachloroethene 0.600 U 0.300 0.600 1.20
Toluene 0.600 U 0.278 0.600 1.20
1,2,3-Trichlorobenzene 0.500 U 0.230 0.500 1.00
1,2,4-Trichlorobenzene 1.00 U 0.481 1.00 2.00
1,1,1-Trichloroethane 0.500 U 0.149 0.500 1.00
1,1,2-Trichloroethane 0.500 U 0.158 0.500 1.00
Trichloroethene 0.500 U 0.190 0.500 1.00
Trichlorofluoromethane 2.00 U 0.160 2.00 5.00
1,2,3-Trichloropropane 1.00 U 0.237 1.00 2.50
1,2,4-Trimethylbenzene 1.00 U 0.322 1.00 2.00
1,3,5-Trimethylbenzene 0.500 U 0.104 0.500 1.00
Vinyl chloride 0.500 U 0.234 0.500 1.00
o-Xylene 0.500 U 0.174 0.500 1.00
m&p-Xylenes 1.00 U 0.430 1.00 2.00
(S) Toluene-d8 105 89.0-112
(S) 4-Bromofluorobenzene 91.6 85.0-114
(S) 1,2-Dichloroethane-d4 95.3 81.0-118
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3819458-1 07/23/22 09:02 • (LCSD) R3819458-2 07/23/22 09:23
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Acetone 25.0 21.0 22.3 84.0 89.2 39.0-160 6.00 20
Acrolein 25.0 23.1 22.1 92.4 88.4 39.0-155 4.42 20
Acrylonitrile 25.0 21.9 22.2 87.6 88.8 63.0-135 1.36 20
Benzene 5.00 5.23 4.78 105 95.6 79.0-120 8.99 20
Bromobenzene 5.00 3.99 4.04 79.8 80.8 80.0-120 J4 1.25 20
Bromodichloromethane 5.00 4.61 4.57 92.2 91.4 79.0-125 0.871 20
Bromoform 5.00 4.11 4.09 82.2 81.8 66.0-130 0.488 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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QUALITY CONTROL SUMMARYWG1899800
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1516722-01,02,03,04,05,06,07,08,09,10,11,12,13
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3819458-1 07/23/22 09:02 • (LCSD) R3819458-2 07/23/22 09:23
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Bromomethane 5.00 4.87 4.89 97.4 97.8 53.0-141 0.410 20
n-Butylbenzene 5.00 4.39 4.20 87.8 84.0 75.0-128 4.42 20
sec-Butylbenzene 5.00 4.71 4.49 94.2 89.8 77.0-126 4.78 20
tert-Butylbenzene 5.00 4.85 4.47 97.0 89.4 78.0-124 8.15 20
Carbon tetrachloride 5.00 5.14 5.02 103 100 72.0-136 2.36 20
Chlorobenzene 5.00 4.77 4.72 95.4 94.4 82.0-118 1.05 20
Chlorodibromomethane 5.00 4.94 4.53 98.8 90.6 74.0-126 8.66 20
Chloroethane 5.00 4.57 4.09 91.4 81.8 60.0-138 11.1 20
Chloroform 5.00 4.55 4.44 91.0 88.8 79.0-124 2.45 20
Chloromethane 5.00 4.59 4.49 91.8 89.8 50.0-139 2.20 20
2-Chlorotoluene 5.00 4.62 4.55 92.4 91.0 79.0-122 1.53 20
4-Chlorotoluene 5.00 4.74 4.39 94.8 87.8 78.0-122 7.67 20
1,2-Dibromo-3-Chloropropane 5.00 4.33 4.56 86.6 91.2 62.0-128 5.17 20
1,2-Dibromoethane 5.00 5.46 5.15 109 103 77.0-121 5.84 20
Dibromomethane 5.00 4.63 4.58 92.6 91.6 79.0-123 1.09 20
1,2-Dichlorobenzene 5.00 4.59 4.68 91.8 93.6 80.0-119 1.94 20
1,3-Dichlorobenzene 5.00 4.68 4.80 93.6 96.0 80.0-119 2.53 20
1,4-Dichlorobenzene 5.00 4.54 4.61 90.8 92.2 79.0-118 1.53 20
Dichlorodifluoromethane 5.00 5.97 5.82 119 116 32.0-152 2.54 20
1,1-Dichloroethane 5.00 4.97 4.67 99.4 93.4 77.0-125 6.22 20
1,2-Dichloroethane 5.00 4.77 4.93 95.4 98.6 73.0-128 3.30 20
1,1-Dichloroethene 5.00 4.68 4.86 93.6 97.2 71.0-131 3.77 20
cis-1,2-Dichloroethene 5.00 5.03 4.60 101 92.0 78.0-123 8.93 20
trans-1,2-Dichloroethene 5.00 4.96 4.95 99.2 99.0 75.0-124 0.202 20
1,2-Dichloropropane 5.00 5.27 4.84 105 96.8 78.0-122 8.51 20
1,1-Dichloropropene 5.00 5.38 4.99 108 99.8 79.0-125 7.52 20
1,3-Dichloropropane 5.00 5.32 5.40 106 108 80.0-119 1.49 20
2,2-Dichloropropane 5.00 4.74 4.28 94.8 85.6 60.0-139 10.2 20
Di-isopropyl ether 5.00 4.55 4.44 91.0 88.8 67.0-128 2.45 20
Ethylbenzene 5.00 4.76 4.56 95.2 91.2 79.0-121 4.29 20
Hexachloro-1,3-butadiene 5.00 4.32 3.95 86.4 79.0 66.0-134 8.95 20
Isopropylbenzene 5.00 4.92 4.68 98.4 93.6 72.0-131 5.00 20
p-Isopropyltoluene 5.00 4.57 4.48 91.4 89.6 77.0-127 1.99 20
2-Butanone (MEK)25.0 22.9 23.3 91.6 93.2 56.0-143 1.73 20
Methylene Chloride 5.00 4.92 4.68 98.4 93.6 74.0-124 5.00 20
4-Methyl-2-pentanone (MIBK)25.0 22.9 22.6 91.6 90.4 67.0-130 1.32 20
Methyl tert-butyl ether 5.00 4.84 4.64 96.8 92.8 71.0-124 4.22 20
Naphthalene 5.00 4.38 4.27 87.6 85.4 61.0-128 2.54 20
n-Propylbenzene 5.00 3.75 3.46 75.0 69.2 76.0-126 J4 J4 8.04 20
Styrene 5.00 4.80 4.66 96.0 93.2 78.0-123 2.96 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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QUALITY CONTROL SUMMARYWG1899800
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1516722-01,02,03,04,05,06,07,08,09,10,11,12,13
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3819458-1 07/23/22 09:02 • (LCSD) R3819458-2 07/23/22 09:23
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
1,1,1,2-Tetrachloroethane 5.00 5.03 5.14 101 103 78.0-124 2.16 20
1,1,2,2-Tetrachloroethane 5.00 4.31 4.09 86.2 81.8 71.0-121 5.24 20
Tetrachloroethene 5.00 5.32 4.78 106 95.6 74.0-129 10.7 20
Toluene 5.00 5.06 4.95 101 99.0 80.0-121 2.20 20
1,2,3-Trichlorobenzene 5.00 3.95 3.87 79.0 77.4 69.0-129 2.05 20
1,2,4-Trichlorobenzene 5.00 4.63 4.32 92.6 86.4 69.0-130 6.93 20
1,1,1-Trichloroethane 5.00 5.02 4.49 100 89.8 74.0-131 11.1 20
1,1,2-Trichloroethane 5.00 5.04 5.07 101 101 80.0-119 0.593 20
Trichloroethene 5.00 4.87 4.87 97.4 97.4 79.0-123 0.000 20
Trichlorofluoromethane 5.00 5.16 4.73 103 94.6 65.0-141 8.70 20
1,2,3-Trichloropropane 5.00 4.96 4.79 99.2 95.8 73.0-122 3.49 20
1,2,4-Trimethylbenzene 5.00 4.55 4.44 91.0 88.8 76.0-124 2.45 20
1,3,5-Trimethylbenzene 5.00 4.94 4.78 98.8 95.6 75.0-124 3.29 20
Vinyl chloride 5.00 4.83 4.68 96.6 93.6 58.0-137 3.15 20
o-Xylene 5.00 4.81 4.56 96.2 91.2 78.0-122 5.34 20
m&p-Xylenes 10.0 9.75 9.49 97.5 94.9 80.0-121 2.70 20
(S) Toluene-d8 103 102 89.0-112
(S) 4-Bromofluorobenzene 91.1 89.4 85.0-114
(S) 1,2-Dichloroethane-d4 98.7 97.6 81.0-118
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1901311
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1516722-06
Method Blank (MB)
(MB) R3819504-3 07/26/22 22:37
MB Result MB Qualifier MB DL MB LOD MB LOQ
Analyte ug/l ug/l ug/l ug/l
Ethylbenzene 0.500 U 0.137 0.500 1.00
(S) Toluene-d8 112 89.0-112
(S) 4-Bromofluorobenzene 105 85.0-114
(S) 1,2-Dichloroethane-d4 105 81.0-118
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3819504-1 07/26/22 21:38 • (LCSD) R3819504-2 07/26/22 21:58
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Ethylbenzene 5.00 5.42 5.48 108 110 79.0-121 1.10 20
(S) Toluene-d8 102 104 89.0-112
(S) 4-Bromofluorobenzene 97.8 101 85.0-114
(S) 1,2-Dichloroethane-d4 105 109 81.0-118
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1902170
TPH by Method MADEPE L1516722-01,02,03,04
Method Blank (MB)
(MB) R3821118-1 07/29/22 10:22
MB Result MB Qualifier MB DL MB LOD MB LOQ
Analyte ug/l ug/l ug/l ug/l
Unadjusted C9-C18 Aliphatics 67.0 U 33.3 67.0 134
Unadjusted C19-C36 Aliphatics 44.0 J 33.3 67.0 134
Unadjusted Total Petroleum
Hydrocarbons 44.0 J 33.3 67.0 134
(S) 1-Chloro-octadecane 75.3 40.0-140
Method Blank (MB)
(MB) R3821118-4 07/29/22 11:32
MB Result MB Qualifier MB DL MB LOD MB LOQ
Analyte ug/l ug/l ug/l ug/l
Unadjusted C11-C22 Aromatics 40.4 J 33.3 67.0 134
Unadjusted Total Petroleum
Hydrocarbons 40.4 J 33.3 67.0 134
(S) o-Terphenyl 83.0 40.0-140
(S) 2-Fluorobiphenyl 84.1 40.0-140
(S) 2-Bromonaphthalene 84.4 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3821118-2 07/29/22 10:45 • (LCSD) R3821118-3 07/29/22 11:09
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C9-C18 Aliphatics 600 382 377 63.7 62.8 40.0-140 1.32 25
Unadjusted C19-C36 Aliphatics 800 774 771 96.8 96.4 40.0-140 0.388 25
(S) 1-Chloro-octadecane 79.6 78.5 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3821118-5 07/29/22 11:55 • (LCSD) R3821118-6 07/29/22 12:19
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C11-C22 Aromatics 1700 1480 1320 87.1 77.6 40.0-140 11.4 25
(S) o-Terphenyl 85.5 76.4 40.0-140
(S) 2-Fluorobiphenyl 90.1 81.6 40.0-140
(S) 2-Bromonaphthalene 89.6 81.3 40.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1902750
TPH by Method MADEPE L1516722-05,06,07,08,09,10,11,12,13
Method Blank (MB)
(MB) R3821161-1 07/29/22 21:23
MB Result MB Qualifier MB DL MB LOD MB LOQ
Analyte ug/l ug/l ug/l ug/l
Unadjusted C9-C18 Aliphatics 67.0 U 33.3 67.0 134
Unadjusted C19-C36 Aliphatics 60.7 J 33.3 67.0 134
Unadjusted Total Petroleum
Hydrocarbons 60.7 J 33.3 67.0 134
(S) 1-Chloro-octadecane 71.1 40.0-140
Method Blank (MB)
(MB) R3821559-1 08/01/22 09:07
MB Result MB Qualifier MB DL MB LOD MB LOQ
Analyte ug/l ug/l ug/l ug/l
Unadjusted C11-C22 Aromatics 49.2 J 33.3 67.0 134
Unadjusted Total Petroleum
Hydrocarbons 49.2 J 33.3 67.0 134
(S) o-Terphenyl 77.6 40.0-140
(S) 2-Fluorobiphenyl 86.6 40.0-140
(S) 2-Bromonaphthalene 83.9 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3821161-2 07/29/22 21:46 • (LCSD) R3821161-3 07/29/22 22:08
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C9-C18 Aliphatics 600 337 336 56.2 56.0 40.0-140 0.297 25
Unadjusted C19-C36 Aliphatics 800 629 656 78.6 82.0 40.0-140 4.20 25
(S) 1-Chloro-octadecane 70.1 72.5 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3821559-2 08/01/22 09:29 • (LCSD) R3821559-3 08/01/22 09:51
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C11-C22 Aromatics 1700 1590 1650 93.5 97.1 40.0-140 3.70 25
(S) o-Terphenyl 85.4 86.3 40.0-140
(S) 2-Fluorobiphenyl 92.8 95.0 40.0-140
(S) 2-Bromonaphthalene 89.4 91.6 40.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1899773
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1516722-01,02,03,04,05,06,07,08,09,10,11,12,13
Method Blank (MB)
(MB) R3819642-2 07/23/22 13:00
MB Result MB Qualifier MB DL MB LOD MB LOQ
Analyte ug/l ug/l ug/l ug/l
Acenaphthene 0.500 U 0.0886 0.500 1.00
Acenaphthylene 0.500 U 0.0921 0.500 1.00
Anthracene 0.500 U 0.0804 0.500 1.00
Benzidine 7.50 U 3.74 7.50 15.0
Benzo(a)anthracene 0.500 U 0.199 0.500 1.00
Benzo(b)fluoranthene 0.500 U 0.130 0.500 1.00
Benzo(k)fluoranthene 0.500 U 0.120 0.500 1.00
Benzo(g,h,i)perylene 0.500 U 0.121 0.500 1.00
Benzo(a)pyrene 0.500 U 0.0381 0.500 1.00
Bis(2-chlorethoxy)methane 5.00 U 0.116 5.00 10.0
Bis(2-chloroethyl)ether 5.00 U 0.137 5.00 10.0
2,2-Oxybis(1-Chloropropane)5.00 U 0.210 5.00 10.0
4-Bromophenyl-phenylether 5.00 U 0.0877 5.00 10.0
2-Chloronaphthalene 0.500 U 0.0648 0.500 1.00
4-Chlorophenyl-phenylether 5.00 U 0.0926 5.00 10.0
Chrysene 0.500 U 0.130 0.500 1.00
Dibenz(a,h)anthracene 0.500 U 0.0644 0.500 1.00
3,3-Dichlorobenzidine 5.00 U 0.212 5.00 10.0
2,4-Dinitrotoluene 5.00 U 0.0983 5.00 10.0
2,6-Dinitrotoluene 5.00 U 0.250 5.00 10.0
Fluoranthene 0.500 U 0.102 0.500 1.00
Fluorene 0.500 U 0.0844 0.500 1.00
Hexachlorobenzene 0.500 U 0.0755 0.500 1.00
Hexachloro-1,3-butadiene 5.00 U 0.0968 5.00 10.0
Hexachlorocyclopentadiene 5.00 U 0.0598 5.00 10.0
Hexachloroethane 5.00 U 0.127 5.00 10.0
Indeno(1,2,3-cd)pyrene 0.600 U 0.279 0.600 1.20
Isophorone 5.00 U 0.143 5.00 10.0
Naphthalene 0.500 U 0.159 0.500 1.00
Nitrobenzene 5.00 U 0.297 5.00 10.0
n-Nitrosodimethylamine 5.00 U 0.998 5.00 10.0
n-Nitrosodiphenylamine 5.00 U 2.37 5.00 10.0
n-Nitrosodi-n-propylamine 5.00 U 0.261 5.00 10.0
Phenanthrene 0.500 U 0.112 0.500 1.00
Benzylbutyl phthalate 2.00 U 0.765 2.00 4.00
Bis(2-ethylhexyl)phthalate 2.00 U 0.895 2.00 4.00
Di-n-butyl phthalate 1.50 U 0.453 1.50 3.00
Diethyl phthalate 1.50 U 0.287 1.50 3.00
Dimethyl phthalate 1.50 U 0.260 1.50 3.00
Di-n-octyl phthalate 2.00 U 0.932 2.00 4.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1899773
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1516722-01,02,03,04,05,06,07,08,09,10,11,12,13
Method Blank (MB)
(MB) R3819642-2 07/23/22 13:00
MB Result MB Qualifier MB DL MB LOD MB LOQ
Analyte ug/l ug/l ug/l ug/l
Pyrene 0.500 U 0.107 0.500 1.00
1,2,4-Trichlorobenzene 5.00 U 0.0698 5.00 10.0
4-Chloro-3-methylphenol 5.00 U 0.131 5.00 10.0
2-Chlorophenol 5.00 U 0.133 5.00 10.0
2,4-Dichlorophenol 5.00 U 0.102 5.00 10.0
2,4-Dimethylphenol 5.00 U 0.0636 5.00 10.0
4,6-Dinitro-2-methylphenol 5.00 U 1.12 5.00 10.0
2,4-Dinitrophenol 15.0 U 5.93 15.0 30.0
2-Nitrophenol 5.00 U 0.117 5.00 10.0
4-Nitrophenol 5.00 U 0.143 5.00 10.0
Pentachlorophenol 5.00 U 0.313 5.00 10.0
Phenol 10.0 U 4.33 10.0 20.0
2,4,6-Trichlorophenol 5.00 U 0.100 5.00 10.0
1-Methylnaphthalene 0.500 U 0.0790 0.500 1.00
2-Methylnaphthalene 0.500 U 0.117 0.500 1.00
(S) Nitrobenzene-d5 51.0 44.0-120
(S) 2-Fluorobiphenyl 52.4 44.0-119
(S) p-Terphenyl-d14 55.6 50.0-134
(S) Phenol-d5 13.7 10.0-67.0
(S) 2-Fluorophenol 21.7 19.0-119
(S) 2,4,6-Tribromophenol 54.5 43.0-140
Laboratory Control Sample (LCS)
(LCS) R3819642-1 07/23/22 12:38
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Acenaphthene 50.0 23.2 46.4 47.0-122 J4
Acenaphthylene 50.0 23.8 47.6 41.0-130
Anthracene 50.0 26.7 53.4 57.0-123 J4
Benzidine 100 16.7 16.7 10.0-165
Benzo(a)anthracene 50.0 33.2 66.4 58.0-125
Benzo(b)fluoranthene 50.0 33.2 66.4 53.0-131
Benzo(k)fluoranthene 50.0 32.2 64.4 57.0-129
Benzo(g,h,i)perylene 50.0 33.1 66.2 50.0-134
Benzo(a)pyrene 50.0 36.4 72.8 54.0-128
Bis(2-chlorethoxy)methane 50.0 20.1 40.2 48.0-120 J4
Bis(2-chloroethyl)ether 50.0 17.4 34.8 43.0-118 J4
2,2-Oxybis(1-Chloropropane)50.0 15.9 31.8 37.0-130 J4
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1899773
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1516722-01,02,03,04,05,06,07,08,09,10,11,12,13
Laboratory Control Sample (LCS)
(LCS) R3819642-1 07/23/22 12:38
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
4-Bromophenyl-phenylether 50.0 31.0 62.0 55.0-124
2-Chloronaphthalene 50.0 21.3 42.6 40.0-116
4-Chlorophenyl-phenylether 50.0 31.6 63.2 53.0-121
Chrysene 50.0 34.0 68.0 59.0-123
Dibenz(a,h)anthracene 50.0 33.2 66.4 51.0-134
3,3-Dichlorobenzidine 100 52.5 52.5 27.0-129
2,4-Dinitrotoluene 50.0 32.3 64.6 57.0-128
2,6-Dinitrotoluene 50.0 28.8 57.6 57.0-124
Fluoranthene 50.0 31.9 63.8 57.0-128
Fluorene 50.0 27.4 54.8 52.0-124
Hexachlorobenzene 50.0 29.9 59.8 53.0-125
Hexachloro-1,3-butadiene 50.0 21.6 43.2 22.0-124
Hexachlorocyclopentadiene 50.0 13.6 27.2 10.0-121
Hexachloroethane 50.0 14.2 28.4 21.0-115
Indeno(1,2,3-cd)pyrene 50.0 34.4 68.8 52.0-134
Isophorone 50.0 21.3 42.6 42.0-124
Naphthalene 50.0 18.1 36.2 40.0-121 J4
Nitrobenzene 50.0 20.4 40.8 45.0-121 J4
n-Nitrosodimethylamine 50.0 18.9 37.8 10.0-121
n-Nitrosodiphenylamine 50.0 20.3 40.6 51.0-123 J4
n-Nitrosodi-n-propylamine 50.0 21.0 42.0 49.0-119 J4
Phenanthrene 50.0 26.6 53.2 59.0-120 J4
Benzylbutyl phthalate 50.0 29.5 59.0 53.0-134
Bis(2-ethylhexyl)phthalate 50.0 29.1 58.2 55.0-135
Di-n-butyl phthalate 50.0 30.1 60.2 59.0-127
Diethyl phthalate 50.0 30.6 61.2 56.0-125
Dimethyl phthalate 50.0 29.5 59.0 45.0-127
Di-n-octyl phthalate 50.0 31.4 62.8 51.0-140
Pyrene 50.0 29.3 58.6 65.0-129 J4
1,2,4-Trichlorobenzene 50.0 20.5 41.0 29.0-116
4-Chloro-3-methylphenol 50.0 26.7 53.4 52.0-119
2-Chlorophenol 50.0 14.4 28.8 38.0-117 J4
2,4-Dichlorophenol 50.0 20.5 41.0 47.0-121 J4
2,4-Dimethylphenol 50.0 21.4 42.8 31.0-124
4,6-Dinitro-2-methylphenol 50.0 33.8 67.6 44.0-137
2,4-Dinitrophenol 50.0 34.1 68.2 23.0-143
2-Nitrophenol 50.0 21.5 43.0 47.0-123 J4
4-Nitrophenol 50.0 13.9 27.8 10.0-120
Pentachlorophenol 50.0 30.2 60.4 35.0-138
Phenol 50.0 7.57 15.1 10.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1899773
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1516722-01,02,03,04,05,06,07,08,09,10,11,12,13
Laboratory Control Sample (LCS)
(LCS) R3819642-1 07/23/22 12:38
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
2,4,6-Trichlorophenol 50.0 27.1 54.2 53.0-123
1-Methylnaphthalene 50.0 22.8 45.6 41.0-119
2-Methylnaphthalene 50.0 21.6 43.2 40.0-121
(S) Nitrobenzene-d5 39.2 44.0-120 J2
(S) 2-Fluorobiphenyl 47.8 44.0-119
(S) p-Terphenyl-d14 59.4 50.0-134
(S) Phenol-d5 14.5 10.0-67.0
(S) 2-Fluorophenol 18.1 19.0-119 J2
(S) 2,4,6-Tribromophenol 62.5 43.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
DL Detection Limit.
LOD Limit of Detection.
LOQ Limit of Quantitation.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
B The same analyte is found in the associated blank.
C4 The reported concentration is an estimate. The continuing calibration standard associated with this data responded low.
Data is likely to show a low bias concerning the result.
J The identification of the analyte is acceptable; the reported value is an estimate.
J2 Surrogate recovery limits have been exceeded; values are outside lower control limits.
J4 The associated batch QC was outside the established quality control range for accuracy.
U Below Detectable Limits: Indicates that the analyte was not detected.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 15:39 62 of 65
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1516722 08/08/22 16:01 62 of 65
Company Name/Address: Billing Information: . --•···'· r ("--t::i.in.nr In~ c;on,~tj,,.n Chain of Custody Page_ of -
Cherokee Nation 3S Christi Mahagan 0res
10838 E. Marshall St. Chk
~E~:o,c1~c, 10838 E. Marshall St. Suite 240
Suite 240 Tulsa, OK 74116
Tulsa . OK 74116
Report to: Email To: [e-mail] MT JULIET, TN
1206S ltbl"On llld Mount .h.o ~-TN 37122
Kevin DeFosset Submoltot111 Uimpie "'' this (ha,n of <uitocty
col\JttlutH .ctinow1td1fne:nt ,nd 1cttpt1nct of the
Project Description: City/State~ ~, Please Circle: u Pact ltnns 11\d Col'ld hons fovnd at
TC-341 Collected 1P e,.vr.J_ PT MT CT ET l: https //',rlfo ~•~ tom/hubf',l~Htlndard u .D terms pdf I "' • r
Phone· Client Proiect # Lab Project # Ill I E l,[S\~fr\.~ CHENATTOK-LEJEUNE ... "O SDG #
q 1a -tt1'i-.b~6x 721102-Q. "O ~ u 0 <( E ~ M012 z :I: I 0 I~ Collected by (print): Site/Facility ID# / P.O # .D .D .D E ..;r
'f:,, t..~d S6V---re-<,'/ E ,-.. E
<( <( ~ <( Acctnum: CHENATTOK
1512~!' Quote # E ...J ~ E Rush? (Lab MUST Be Notified) .-i N ilemplate:T211580 0
Same Day _ fr;e Day 0 <( 0 ..;r 0 ~ '° Prelol!in: P933086
_ 5 Day (Rad Only) .-i <( _Next Day Date Results Needed I 8 ~ 1~1M1m~lo -() I . ely _Two Day _ 10 Day (Rad Only) No. .-1 Q.
Packed on Ice N y~ _Three Day vi UJ N :c
of N > '° Q.
'° 1/l > > Shipp~d Via: FedEX Ground
Sample ID Comp/Grab Matrix• Depth Date Time ntrs 0 0 0 0
0 0 0 0 Remarks I Sampl .. (lab onlyl
0 0 0 0
>-7/(9./12-nq~ ~ U5'I_l11-'-{.80-MWL2.~ GW ;( )t y "-/}\ . n94D q ✓ 'I-. 'x ' cf'-£.l.S-r-r c.'3'1{ -M~ / GW
v5"TC:,'-l'JO-JY1W!/ GW (000 q v K V V 0)
ll__5_fl"C-34{-mwoS GW f o'{<:, 'l v X. 'v ~ >."I
_v57Ci'l<"tO -mw:i.1 GW ro5Z.. q ',( X V '11' £
_ v m c.. 3'-l J_-11-{ M~ f!.. II I ' q 'I x , '
GW \I V 6L
,_ U'ST<=t~O -tYILtJD2. GW I l'(<i ~ y x. y y' ,.'l
V IT7C.3'{{-MWO<g GW (2.05 q X ~ x V' ~
~UITG,'{<i0~:15 GW 12.51 '1 )( x.. ' d, )( V
vs,~c 1'1( -f'rlWl7 GW 126l 4 J(_ \I :)(... )l t,o
• Matrix: Remarks: S~tolt B~~~i~t ~h~~~
SS • Soil AIR -Air F • Filter pH ___ Temp ___ CCC Seal Pre ent/Intact: _NP Y N
GW . Groundwater B • Bioassay
CCC Signed hccurate: ~y -N
WW -Wastewater Flow Other Bottles arrive intac•: y =N ------Correct bottles used y _N
DW • Drinking Water Samples returned via:
Sufficient volu~e sent: _Y _N
OT· Other Tracking# lf A,1211,0.bl~
UPS FedEx Courier VOA z-ro Headspare: /y N
Reli~ a;:;:i ~ # Date: Time: Received by: (Signature) Tnp Blank Receive(. 'l~o Preservation Correct/Cheesed: ~N
--, /1 q /Zt>11-4 ~eoH
RAD Screer. <0.5 mR/hr: N
~ i I oCJ
Re~d by : (S1gnaere) Date: Time Received by: (Signature) Temp: ·c Bottles Recctved If preservation required by Login: Date/Time \\~ A
Relinquished by : (Signature) Date: Time:
Re'?r/Jh-;/1/(/}
•~-• ,
:rli01-ri TimiffllU Hold:
I Condi79
NCF / 0 .. , V ~, V --. '
Comp•ny N•me/Address: Billing Information: I A :.I·-'-rnnt:11 ~ .... I o .... ·--·-•ivP Chain of Custody P•ge_ of -
Cherokee Nation 3S Christi Mahagan ?res
10838 E. Marshall St. Chk ff!.~~-·~"~· 10838 E. Marshall St. Suite 240
Suite 240 Tulsa, OK 74116
Tulsa. OK 74116
Report to: Email [e-mail] MT JULIET, TN
Kevin Defosset U06S Ltb,al"lo;)tl "d Mount Jw 1tt, TN l7122
Submitt,n1 • u,npt,e v,,1 lhes chain of custody
Project Description: City/State lt-1 'e.vn.l. Please Circle: u tonst,h,tt, kk~.ct,ment ind 6Cuptlt'l(t of the
Collected: (A.vi,r,O
Pu.t Terms ind Concfotions found al
TC-341 PT MT CT ET :I: httpl //t,r,fo s,Ktl.abs com/hubh/,.1--~rd• u i., terms pelf
Client Proiect # Lall' Project # VI I
Phone: Ill E U~l \o/1,'\; ...
9 IO -478 -'~6 s; 22//07-CHENATTOK-LEJEUNE CL "O <{ SDG #
0 "O E u z ~ I
Coe:d by (print): Site/Facility ID# P.O.# .D ~ 0 ~ Table# ~
\ c..l-..o.f'dSff"V"--, -re -s'( I E E --E
<{ <{ ... <{ Acctnum: CHENATTOK ....'.., ~ z?.DE #,J' -
Rush? (Lab MUST Be Notified) Quote# E rl N E Template T211580 0
_S•meD•y _FiveD•y 0 <{ 0 .: 0 ~ ~ Prelo11in: P933086
_Next Day _ S Day (R•d Only) Date Results Needed rl <{
I 8 ~ i~m h~~gne~~ l-f) _Two Day _ 10 Day (Rad Only) No. rl CL
Packed on Ice N Y .15... _Three Day 1/'J UJ N I of N > IO CL
t ntrs lO V) > > Shipp d Via: F ~dEX Ground
Sample ID Comp/Grab Matrix• Depth Date Time 0 0 0 0
0 0 0 0 Rem,rt.s I Samplt # (1,b only)
0 0 0 0 .-------
vmc.'3lfl-Mwl.3.. GW -,/f6(1.1-l~ZS ~ " t.. x x
vs-rc;,4 %0 -MWOfo (;v-,) 1/t<;tz.,Z. {'{OZ. <t " y y k'
u5,Gt<iO -mwz3 GvJ 7/t~/t1 (46Lt '1 y )t ',( x
'-
---
-
-
• Matrix: Remarks: S:im~l~ B~r~!~t Cbt~?i
SS • Soil AIR· Air F • Filter pH ---Temp ___ COC See~ Present/Intact :lP Y N
GW • Groundwater B • Bioassay
coc s,g~ed/Accurate:
~' WW • Wastewater Flow Other Bottles arrive intact: l _N ------Correc: bottles used· y _N
OW • Drinking Water Samples returned via: Su!ficien• volume sent: y _N
OT· Other UPS FedEx Courier Tracking# If APPlicable Lf VOA Zero Headspace: N
~;~~ Date: Time: Received by· (Signature) Trip Blank Received· Yes/ No Preservation Correct/Ctec,ed: y ~
---, It 9 lz:,_ HCL/ MeoH RAO Screen <0 .5 mR/hr: ?-=N
I //)0 TBR
~,shed by: (S~ature) Date: Time· Received by: (Signature) Temp: ·c Bottles Rece,ved: If preservation required by Login: Date/Time
.,...,
Relinquished by: (Signature) Date: Time: 7/0~~ I) ~ liol iz Timcf/(JJ
Hold: Condition:
NCF / (U
, -~ V V I '
I
•
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AQ/_ Q 0
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rt-Ii'-(T \)-0--cS CY" ~ 3 tr cs-__. --3 --8 5:::) ~ 0 ~ cs--
6" ~ ---r ~ t\---t; --Cl-\f) \J' \r)
\0 •)
ANALYTICAL REPORT
August 10, 2022
Cherokee Nation 3S
Sample Delivery Group:L1517739
Samples Received:07/22/2022
Project Number:221102
Description:TC-341
Site:TC-341
Report To:Kevin DeFosset
10838 E. Marshall St.
Suite 240
Tulsa, OK 74116
Entire Report Reviewed By:
August 10, 2022
[Preliminary Report]
Heather J Wagner
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 1 of 84
August 10, 2022
Heather J Wagner
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 1 of 84
p eAnalytical "
I _J
□ □ □ □ □ □ □ □
TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 7
Sr: Sample Results 8
USTG480-MW19 L1517739-01 8
USTG480-MW16 L1517739-02 11
USTTC341-MW18 L1517739-03 14
USTG480-MW17 L1517739-04 17
USTG480-MW13 L1517739-05 20
USTG480-MW18 L1517739-06 23
USTTC341-MW15R L1517739-07 26
USTG480-MW08 L1517739-08 29
USTG480-MW20 L1517739-09 32
USTG480-MW29 L1517739-10 35
USTG480-MW07 L1517739-11 38
IR35-MW67AR L1517739-12 41
USTG480-MW26 L1517739-13 44
USTG480-MW30 L1517739-14 47
USTG480-MW33R L1517739-15 50
USTG480-MW14 L1517739-16 53
USTG480-MW28 L1517739-17 56
Qc: Quality Control Summary 59
Volatile Petroleum Hydrocarbons by Method MADEPV 59
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 62
TPH by Method MADEPE 67
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 71
Gl: Glossary of Terms 80
Al: Accreditations & Locations 81
Sc: Sample Chain of Custody 82
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 2 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 2 of 84
□
□ □ □ □ □ □ □
SAMPLE SUMMARY
Collected by Collected date/time Received date/time
USTG480-MW19 L1517739-01 GW Richardson 07/20/22 09:55 07/22/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Petroleum Hydrocarbons by Method MADEPV WG1902102 1 07/29/22 20:25 07/29/22 20:25 ADM Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1900597 1 07/25/22 17:27 07/25/22 17:27 JHH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1905109 1 08/03/22 20:36 08/03/22 20:36 JHH Mt. Juliet, TN
TPH by Method MADEPE WG1902750 1 07/28/22 07:52 08/01/22 22:28 DMG Mt. Juliet, TN
TPH by Method MADEPE WG1902750 1 07/28/22 07:52 08/02/22 05:29 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1900474 1 07/27/22 10:26 07/27/22 18:53 JNJ Mt. Juliet, TN
Collected by Collected date/time Received date/time
USTG480-MW16 L1517739-02 GW Richardson 07/20/22 10:10 07/22/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Petroleum Hydrocarbons by Method MADEPV WG1902102 1 07/29/22 20:58 07/29/22 20:58 ADM Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1900597 1 07/25/22 17:48 07/25/22 17:48 JHH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1905109 1 08/03/22 20:57 08/03/22 20:57 JHH Mt. Juliet, TN
TPH by Method MADEPE WG1902750 1 07/28/22 07:52 08/01/22 22:50 DMG Mt. Juliet, TN
TPH by Method MADEPE WG1902750 1 07/28/22 07:52 08/02/22 05:06 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1900474 1 07/27/22 10:26 07/27/22 20:21 JNJ Mt. Juliet, TN
Collected by Collected date/time Received date/time
USTTC341-MW18 L1517739-03 GW Richardson 07/20/22 10:12 07/22/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Petroleum Hydrocarbons by Method MADEPV WG1902102 1 07/29/22 21:30 07/29/22 21:30 ADM Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1900597 1 07/25/22 18:09 07/25/22 18:09 JHH Mt. Juliet, TN
TPH by Method MADEPE WG1902750 1 07/28/22 07:52 08/01/22 23:12 DMG Mt. Juliet, TN
TPH by Method MADEPE WG1902750 1 07/28/22 07:52 08/02/22 04:44 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1900474 1 07/27/22 10:26 07/27/22 22:12 JNJ Mt. Juliet, TN
Collected by Collected date/time Received date/time
USTG480-MW17 L1517739-04 GW Richardson 07/20/22 11:00 07/22/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Petroleum Hydrocarbons by Method MADEPV WG1902102 1 07/29/22 22:03 07/29/22 22:03 ADM Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1900597 1 07/25/22 18:30 07/25/22 18:30 JHH Mt. Juliet, TN
TPH by Method MADEPE WG1902750 1 07/28/22 07:52 08/01/22 23:34 DMG Mt. Juliet, TN
TPH by Method MADEPE WG1902750 1 07/28/22 07:52 08/02/22 13:15 JDG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1900474 1 07/27/22 10:26 07/27/22 21:28 JNJ Mt. Juliet, TN
Collected by Collected date/time Received date/time
USTG480-MW13 L1517739-05 GW Richardson 07/20/22 11:30 07/22/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Petroleum Hydrocarbons by Method MADEPV WG1902102 10 07/30/22 05:42 07/30/22 05:42 ADM Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1900597 10 07/25/22 22:22 07/25/22 22:22 JHH Mt. Juliet, TN
TPH by Method MADEPE WG1902750 1 07/28/22 07:52 08/01/22 23:56 DMG Mt. Juliet, TN
TPH by Method MADEPE WG1902750 1 07/28/22 07:52 08/02/22 04:00 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1900474 1 07/27/22 10:26 08/01/22 19:25 AGW Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 3 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 3 of 84
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□ □ -----------□
□ □ □
SAMPLE SUMMARY
Collected by Collected date/time Received date/time
USTG480-MW18 L1517739-06 GW Richardson 07/20/22 11:45 07/22/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Petroleum Hydrocarbons by Method MADEPV WG1902102 1 07/29/22 22:36 07/29/22 22:36 ADM Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1900597 1 07/25/22 18:52 07/25/22 18:52 JHH Mt. Juliet, TN
TPH by Method MADEPE WG1902750 1 07/28/22 07:52 08/02/22 00:18 DMG Mt. Juliet, TN
TPH by Method MADEPE WG1902750 1 07/28/22 07:52 08/02/22 03:38 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1900474 1 07/27/22 10:26 07/27/22 19:15 AO Mt. Juliet, TN
Collected by Collected date/time Received date/time
USTTC341-MW15R L1517739-07 GW Richardson 07/20/22 11:52 07/22/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Petroleum Hydrocarbons by Method MADEPV WG1902102 1 07/30/22 04:37 07/30/22 04:37 ADM Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1900597 1 07/25/22 19:13 07/25/22 19:13 JHH Mt. Juliet, TN
TPH by Method MADEPE WG1902750 1 07/28/22 07:52 08/02/22 00:41 DMG Mt. Juliet, TN
TPH by Method MADEPE WG1902750 1 07/28/22 07:52 08/02/22 02:09 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1900474 1 07/27/22 10:26 07/27/22 19:37 AO Mt. Juliet, TN
Collected by Collected date/time Received date/time
USTG480-MW08 L1517739-08 GW Richardson 07/20/22 12:30 07/22/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Petroleum Hydrocarbons by Method MADEPV WG1902102 20 07/30/22 06:15 07/30/22 06:15 ADM Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1900597 20 07/25/22 22:43 07/25/22 22:43 JHH Mt. Juliet, TN
TPH by Method MADEPE WG1902750 1 07/28/22 07:52 08/02/22 01:03 DMG Mt. Juliet, TN
TPH by Method MADEPE WG1902750 10 07/28/22 07:52 08/03/22 08:37 JDG Mt. Juliet, TN
TPH by Method MADEPE WG1902750 10 07/28/22 07:52 08/03/22 08:59 JDG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1900474 5 07/27/22 10:26 07/27/22 23:17 JNJ Mt. Juliet, TN
Collected by Collected date/time Received date/time
USTG480-MW20 L1517739-09 GW Richardson 07/20/22 13:01 07/22/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Petroleum Hydrocarbons by Method MADEPV WG1902102 10 07/30/22 06:48 07/30/22 06:48 ADM Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1900597 10 07/25/22 23:04 07/25/22 23:04 GLN Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1905109 10 08/04/22 02:41 08/04/22 02:41 JHH Mt. Juliet, TN
TPH by Method MADEPE WG1904482 1 08/02/22 09:02 08/03/22 04:39 JDG Mt. Juliet, TN
TPH by Method MADEPE WG1904482 1 08/02/22 09:02 08/03/22 10:03 JDG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1900474 5 07/27/22 10:26 08/01/22 20:52 AGW Mt. Juliet, TN
Collected by Collected date/time Received date/time
USTG480-MW29 L1517739-10 GW Richardson 07/20/22 13:35 07/22/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Petroleum Hydrocarbons by Method MADEPV WG1903095 1 07/31/22 14:13 07/31/22 14:13 DWR Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1900597 1 07/25/22 19:33 07/25/22 19:33 GLN Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1905109 20 08/04/22 03:02 08/04/22 03:02 JHH Mt. Juliet, TN
TPH by Method MADEPE WG1904482 1 08/02/22 09:02 08/03/22 05:02 JDG Mt. Juliet, TN
TPH by Method MADEPE WG1904482 1 08/02/22 09:02 08/03/22 10:27 JDG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1900474 1 07/27/22 10:26 07/27/22 21:06 JNJ Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 4 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 4 of 84
-----------□ -----------□
□ □ -----------□
□ □ □
SAMPLE SUMMARY
Collected by Collected date/time Received date/time
USTG480-MW07 L1517739-11 GW Richardson 07/20/22 13:45 07/22/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Petroleum Hydrocarbons by Method MADEPV WG1903095 1 07/31/22 14:46 07/31/22 14:46 DWR Mt. Juliet, TN
Volatile Petroleum Hydrocarbons by Method MADEPV WG1903796 5 08/03/22 09:35 08/03/22 09:35 MGF Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1900597 1 07/25/22 19:55 07/25/22 19:55 GLN Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1905109 10 08/04/22 03:24 08/04/22 03:24 JHH Mt. Juliet, TN
TPH by Method MADEPE WG1904482 1 08/02/22 09:02 08/03/22 05:25 JDG Mt. Juliet, TN
TPH by Method MADEPE WG1904482 1 08/02/22 09:02 08/03/22 10:50 JDG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1900474 1 07/27/22 10:26 07/27/22 21:50 JNJ Mt. Juliet, TN
Collected by Collected date/time Received date/time
IR35-MW67AR L1517739-12 GW Richardson 07/20/22 14:32 07/22/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Petroleum Hydrocarbons by Method MADEPV WG1903095 1 07/31/22 15:18 07/31/22 15:18 DWR Mt. Juliet, TN
Volatile Petroleum Hydrocarbons by Method MADEPV WG1903796 5 08/03/22 10:07 08/03/22 10:07 MGF Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1900597 1 07/25/22 20:15 07/25/22 20:15 GLN Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1905109 10 08/04/22 03:45 08/04/22 03:45 JHH Mt. Juliet, TN
TPH by Method MADEPE WG1904482 1 08/02/22 09:02 08/03/22 05:49 JDG Mt. Juliet, TN
TPH by Method MADEPE WG1904482 1 08/02/22 09:02 08/03/22 11:13 JDG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1900474 1.05 07/27/22 10:26 07/27/22 22:33 JNJ Mt. Juliet, TN
Collected by Collected date/time Received date/time
USTG480-MW26 L1517739-13 GW Richardson 07/20/22 15:00 07/22/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Petroleum Hydrocarbons by Method MADEPV WG1903095 1 07/31/22 15:51 07/31/22 15:51 DWR Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1900597 1 07/25/22 20:36 07/25/22 20:36 JHH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1905109 1 08/03/22 21:19 08/03/22 21:19 JHH Mt. Juliet, TN
TPH by Method MADEPE WG1904482 1 08/02/22 09:02 08/03/22 06:12 JDG Mt. Juliet, TN
TPH by Method MADEPE WG1904482 1 08/02/22 09:02 08/03/22 11:37 JDG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1900474 1 07/27/22 10:26 08/01/22 19:03 AGW Mt. Juliet, TN
Collected by Collected date/time Received date/time
USTG480-MW30 L1517739-14 GW Richardson 07/20/22 15:00 07/22/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Petroleum Hydrocarbons by Method MADEPV WG1903095 1 07/31/22 16:24 07/31/22 16:24 DWR Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1900597 1 07/25/22 20:58 07/25/22 20:58 JHH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1905109 1 08/03/22 21:40 08/03/22 21:40 JHH Mt. Juliet, TN
TPH by Method MADEPE WG1904482 1 08/02/22 09:02 08/03/22 06:35 JDG Mt. Juliet, TN
TPH by Method MADEPE WG1904482 1 08/02/22 09:02 08/03/22 12:04 JDG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1900474 1 07/27/22 10:26 07/27/22 20:43 JNJ Mt. Juliet, TN
Collected by Collected date/time Received date/time
USTG480-MW33R L1517739-15 GW Richardson 07/20/22 15:27 07/22/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Petroleum Hydrocarbons by Method MADEPV WG1903095 1 07/31/22 16:57 07/31/22 16:57 DWR Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1900597 1 07/25/22 21:19 07/25/22 21:19 JHH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1905109 1 08/03/22 22:01 08/03/22 22:01 JHH Mt. Juliet, TN
TPH by Method MADEPE WG1904482 1 08/02/22 09:02 08/03/22 06:58 JDG Mt. Juliet, TN
TPH by Method MADEPE WG1904482 1 08/02/22 09:02 08/03/22 12:27 JDG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1900474 1 07/27/22 10:26 07/27/22 19:59 JNJ Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
USTG480-MW14 L1517739-16 GW Richardson 07/21/22 09:30 07/22/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Petroleum Hydrocarbons by Method MADEPV WG1903095 1 07/31/22 17:29 07/31/22 17:29 DWR Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1900597 1 07/25/22 21:40 07/25/22 21:40 JHH Mt. Juliet, TN
TPH by Method MADEPE WG1905723 1 08/04/22 10:49 08/06/22 01:55 DMG Mt. Juliet, TN
TPH by Method MADEPE WG1905723 1 08/04/22 10:49 08/06/22 03:50 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1901647 1 07/26/22 14:29 08/01/22 18:20 AGW Mt. Juliet, TN
Collected by Collected date/time Received date/time
USTG480-MW28 L1517739-17 GW Richardson 07/21/22 11:00 07/22/22 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Petroleum Hydrocarbons by Method MADEPV WG1903796 1 08/03/22 09:02 08/03/22 09:02 MGF Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 WG1900597 10 07/25/22 23:24 07/25/22 23:24 JHH Mt. Juliet, TN
TPH by Method MADEPE WG1905723 1 08/04/22 10:49 08/06/22 02:18 DMG Mt. Juliet, TN
TPH by Method MADEPE WG1905723 1 08/04/22 10:49 08/06/22 04:13 DMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1901647 1 07/26/22 14:29 08/01/22 18:42 AGW Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Heather J Wagner
Project Manager
Project Narrative
Due to multiple preparation procedures, calculated analytes are not reported in the quality control samples for EPH and VPH
Methods.

Method 625.1: Samples in WG1900474 are reporting with failures in the LCS against DOD limits. Recoveries are within laboratory
historical limits.
Method 6200: Samples USTG480-MW20 (L1517739-09), USTG480-MW29 (L1517739-10), USTG480-MW07 (L1517739-11),
IR35-MW67AR (L1517739-12) were re-analyzed out of hold due to failing QC in the initial in hold run.
Sample Delivery Group (SDG) Narrative
An aliquot for analysis was taken from the original container received due to the level of sediment present in the sample.
Rinsing of the original sample container for inclusion in the sample extraction was not performed.
Lab Sample ID Project Sample ID Method
L1517739-05 USTG480-MW13 MADEPE
L1517739-09 USTG480-MW20 MADEPE
L1517739-10 USTG480-MW29 MADEPE
L1517739-11 USTG480-MW07 MADEPE
L1517739-12 IR35-MW67AR MADEPE
L1517739-13 USTG480-MW26 MADEPE
L1517739-14 USTG480-MW30 MADEPE
L1517739-15 USTG480-MW33R MADEPE
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Heather J Wagner
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 01
L1517739
USTG480-MW19
Collected date/time: 07/20/22 09:55
Volatile Petroleum Hydrocarbons by Method MADEPV
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics C5-C8 ALI
UNADJ 67.0 U 33.3 67.0 100 1 07/29/2022 20:25 WG1902102
Unadjusted C9-C12 Aliphatics C9-C12 ALI
UNADJ 37.5 B J 33.3 67.0 134 1 07/29/2022 20:25 WG1902102
Unadjusted C9-C10 Aromatics C9-C10 ARO
UNADJ 67.0 U 33.3 67.0 100 1 07/29/2022 20:25 WG1902102
Total VPH VPH 150 U 66.7 150 300 1 07/29/2022 20:25 WG1902102
(S) 2,5-Dibromotoluene(FID)615-59-8 94.7 70.0-130 07/29/2022 20:25 WG1902102
(S) 2,5-Dibromotoluene(PID)615-59-8 97.0 70.0-130 07/29/2022 20:25 WG1902102
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acetone 67-64-1 25.0 J3 U 11.3 25.0 50.0 1 07/25/2022 17:27 WG1900597
Acrolein 107-02-8 25.0 C4 U 2.54 25.0 50.0 1 07/25/2022 17:27 WG1900597
Acrylonitrile 107-13-1 5.00 J4 U 0.671 5.00 10.0 1 07/25/2022 17:27 WG1900597
Benzene 71-43-2 0.500 U 0.0941 0.500 1.00 1 07/25/2022 17:27 WG1900597
Bromobenzene 108-86-1 0.500 U 0.118 0.500 1.00 1 07/25/2022 17:27 WG1900597
Bromodichloromethane 75-27-4 0.500 U 0.136 0.500 1.00 1 07/25/2022 17:27 WG1900597
Bromoform 75-25-2 0.500 U 0.129 0.500 1.00 1 07/25/2022 17:27 WG1900597
Bromomethane 74-83-9 2.00 U 0.605 2.00 5.00 1 07/25/2022 17:27 WG1900597
n-Butylbenzene 104-51-8 0.500 U 0.157 0.500 1.00 1 07/25/2022 17:27 WG1900597
sec-Butylbenzene 135-98-8 0.500 U 0.125 0.500 1.00 1 07/25/2022 17:27 WG1900597
tert-Butylbenzene 98-06-6 0.500 U 0.127 0.500 1.00 1 07/25/2022 17:27 WG1900597
Carbon tetrachloride 56-23-5 0.500 U 0.128 0.500 1.00 1 07/25/2022 17:27 WG1900597
Chlorobenzene 108-90-7 0.500 U 0.116 0.500 1.00 1 07/25/2022 17:27 WG1900597
Chlorodibromomethane 124-48-1 0.500 U 0.140 0.500 1.00 1 07/25/2022 17:27 WG1900597
Chloroethane 75-00-3 2.00 U 0.192 2.00 5.00 1 07/25/2022 17:27 WG1900597
Chloroform 67-66-3 2.00 U 0.111 2.00 5.00 1 07/25/2022 17:27 WG1900597
Chloromethane 74-87-3 2.00 U 0.960 2.00 4.00 1 07/25/2022 17:27 WG1900597
2-Chlorotoluene 95-49-8 0.500 U 0.106 0.500 1.00 1 07/25/2022 17:27 WG1900597
4-Chlorotoluene 106-43-4 0.500 U 0.114 0.500 1.00 1 07/25/2022 17:27 WG1900597
1,2-Dibromo-3-Chloropropane 96-12-8 2.00 U 0.276 2.00 5.00 1 07/25/2022 17:27 WG1900597
1,2-Dibromoethane 106-93-4 0.500 U 0.126 0.500 1.00 1 07/25/2022 17:27 WG1900597
Dibromomethane 74-95-3 0.500 U 0.122 0.500 1.00 1 07/25/2022 17:27 WG1900597
1,2-Dichlorobenzene 95-50-1 0.500 U 0.107 0.500 1.00 1 07/25/2022 17:27 WG1900597
1,3-Dichlorobenzene 541-73-1 0.500 U 0.110 0.500 1.00 1 07/25/2022 17:27 WG1900597
1,4-Dichlorobenzene 106-46-7 0.500 U 0.120 0.500 1.00 1 07/25/2022 17:27 WG1900597
Dichlorodifluoromethane 75-71-8 2.00 U 0.374 2.00 5.00 1 07/25/2022 17:27 WG1900597
1,1-Dichloroethane 75-34-3 0.500 U 0.100 0.500 1.00 1 07/25/2022 17:27 WG1900597
1,2-Dichloroethane 107-06-2 0.500 U 0.0819 0.500 1.00 1 07/25/2022 17:27 WG1900597
1,1-Dichloroethene 75-35-4 0.500 U 0.188 0.500 1.00 1 07/25/2022 17:27 WG1900597
cis-1,2-Dichloroethene 156-59-2 0.500 U 0.126 0.500 1.00 1 07/25/2022 17:27 WG1900597
trans-1,2-Dichloroethene 156-60-5 0.500 U 0.149 0.500 1.00 1 07/25/2022 17:27 WG1900597
1,2-Dichloropropane 78-87-5 0.500 U 0.149 0.500 1.00 1 07/25/2022 17:27 WG1900597
1,1-Dichloropropene 563-58-6 0.500 U 0.142 0.500 1.00 1 07/25/2022 17:27 WG1900597
1,3-Dichloropropane 142-28-9 0.500 U 0.110 0.500 1.00 1 07/25/2022 17:27 WG1900597
2,2-Dichloropropane 594-20-7 0.500 U 0.161 0.500 1.00 1 07/25/2022 17:27 WG1900597
Di-isopropyl ether 108-20-3 0.500 U 0.105 0.500 1.00 1 07/25/2022 17:27 WG1900597
Ethylbenzene 100-41-4 0.500 U 0.137 0.500 1.00 1 07/25/2022 17:27 WG1900597
Hexachloro-1,3-butadiene 87-68-3 0.750 J3 U 0.337 0.750 1.50 1 07/25/2022 17:27 WG1900597
Isopropylbenzene 98-82-8 0.500 U 0.105 0.500 1.00 1 07/25/2022 17:27 WG1900597
p-Isopropyltoluene 99-87-6 0.500 U 0.120 0.500 1.00 1 07/25/2022 17:27 WG1900597
2-Butanone (MEK)78-93-3 5.00 U 1.19 5.00 10.0 1 07/25/2022 17:27 WG1900597
Methylene Chloride 75-09-2 2.00 U 0.430 2.00 5.00 1 07/25/2022 17:27 WG1900597
4-Methyl-2-pentanone (MIBK)108-10-1 5.00 U 0.478 5.00 10.0 1 07/25/2022 17:27 WG1900597
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 01
L1517739
USTG480-MW19
Collected date/time: 07/20/22 09:55
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Methyl tert-butyl ether 1634-04-4 0.500 U 0.101 0.500 1.00 1 07/25/2022 17:27 WG1900597
Naphthalene 91-20-3 2.00 U 1.00 2.00 5.00 1 08/03/2022 20:36 WG1905109
n-Propylbenzene 103-65-1 0.500 U 0.0993 0.500 1.00 1 08/03/2022 20:36 WG1905109
Styrene 100-42-5 0.500 U 0.118 0.500 1.00 1 07/25/2022 17:27 WG1900597
1,1,1,2-Tetrachloroethane 630-20-6 0.500 U 0.147 0.500 1.00 1 07/25/2022 17:27 WG1900597
1,1,2,2-Tetrachloroethane 79-34-5 0.500 U 0.133 0.500 1.00 1 07/25/2022 17:27 WG1900597
Tetrachloroethene 127-18-4 0.600 U 0.300 0.600 1.20 1 07/25/2022 17:27 WG1900597
Toluene 108-88-3 0.600 U 0.278 0.600 1.20 1 07/25/2022 17:27 WG1900597
1,2,3-Trichlorobenzene 87-61-6 0.500 U 0.230 0.500 1.00 1 07/25/2022 17:27 WG1900597
1,2,4-Trichlorobenzene 120-82-1 1.00 U 0.481 1.00 2.00 1 07/25/2022 17:27 WG1900597
1,1,1-Trichloroethane 71-55-6 0.500 U 0.149 0.500 1.00 1 07/25/2022 17:27 WG1900597
1,1,2-Trichloroethane 79-00-5 0.500 U 0.158 0.500 1.00 1 07/25/2022 17:27 WG1900597
Trichloroethene 79-01-6 0.500 U 0.190 0.500 1.00 1 07/25/2022 17:27 WG1900597
Trichlorofluoromethane 75-69-4 2.00 U 0.160 2.00 5.00 1 07/25/2022 17:27 WG1900597
1,2,3-Trichloropropane 96-18-4 1.00 U 0.237 1.00 2.50 1 07/25/2022 17:27 WG1900597
1,2,4-Trimethylbenzene 95-63-6 1.00 U 0.322 1.00 2.00 1 08/03/2022 20:36 WG1905109
1,3,5-Trimethylbenzene 108-67-8 0.500 U 0.104 0.500 1.00 1 08/03/2022 20:36 WG1905109
Vinyl chloride 75-01-4 0.500 U 0.234 0.500 1.00 1 07/25/2022 17:27 WG1900597
o-Xylene 95-47-6 0.500 U 0.174 0.500 1.00 1 08/03/2022 20:36 WG1905109
m&p-Xylenes 1330-20-7 1.00 U 0.430 1.00 2.00 1 08/03/2022 20:36 WG1905109
(S) Toluene-d8 2037-26-5 102 89.0-112 07/25/2022 17:27 WG1900597
(S) Toluene-d8 2037-26-5 102 89.0-112 08/03/2022 20:36 WG1905109
(S) 4-Bromofluorobenzene 460-00-4 96.5 85.0-114 07/25/2022 17:27 WG1900597
(S) 4-Bromofluorobenzene 460-00-4 102 85.0-114 08/03/2022 20:36 WG1905109
(S) 1,2-Dichloroethane-d4 17060-07-0 97.6 81.0-118 07/25/2022 17:27 WG1900597
(S) 1,2-Dichloroethane-d4 17060-07-0 86.9 81.0-118 08/03/2022 20:36 WG1905109
TPH by Method MADEPE
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics C9-C18 ALI
UNADJ 67.0 U 33.3 67.0 134 1 08/01/2022 22:28 WG1902750
Unadjusted C19-C36 Aliphatics C19-C36 ALI
UNADJ 35.0 B J 33.3 67.0 134 1 08/01/2022 22:28 WG1902750
Unadjusted C11-C22 Aromatics C11-C22 ARO
UNADJ 67.1 B J 33.3 67.0 134 1 08/02/2022 05:29 WG1902750
Unadjusted Total Petroleum
Hydrocarbons TPH UNADJ 102 B J 33.3 67.0 134 1 08/02/2022 05:29 WG1902750
(S) o-Terphenyl 84-15-1 67.2 40.0-140 08/02/2022 05:29 WG1902750
(S) 1-Chloro-octadecane 3386-33-2 55.0 40.0-140 08/01/2022 22:28 WG1902750
(S) 2-Fluorobiphenyl 321-60-8 89.8 40.0-140 08/02/2022 05:29 WG1902750
(S) 2-Bromonaphthalene 580-13-2 86.7 40.0-140 08/02/2022 05:29 WG1902750
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acenaphthene 83-32-9 0.500 U 0.0886 0.500 1.00 1 07/27/2022 18:53 WG1900474
Acenaphthylene 208-96-8 0.500 U 0.0921 0.500 1.00 1 07/27/2022 18:53 WG1900474
Anthracene 120-12-7 0.500 J4 U 0.0804 0.500 1.00 1 07/27/2022 18:53 WG1900474
Benzidine 92-87-5 7.50 J4 U 3.74 7.50 15.0 1 07/27/2022 18:53 WG1900474
Benzo(a)anthracene 56-55-3 0.500 U 0.199 0.500 1.00 1 07/27/2022 18:53 WG1900474
Benzo(b)fluoranthene 205-99-2 0.500 U 0.130 0.500 1.00 1 07/27/2022 18:53 WG1900474
Benzo(k)fluoranthene 207-08-9 0.500 U 0.120 0.500 1.00 1 07/27/2022 18:53 WG1900474
Benzo(g,h,i)perylene 191-24-2 0.500 U 0.121 0.500 1.00 1 07/27/2022 18:53 WG1900474
Benzo(a)pyrene 50-32-8 0.500 U 0.0381 0.500 1.00 1 07/27/2022 18:53 WG1900474
Bis(2-chlorethoxy)methane 111-91-1 5.00 J4 U 0.116 5.00 10.0 1 07/27/2022 18:53 WG1900474
Bis(2-chloroethyl)ether 111-44-4 5.00 J4 U 0.137 5.00 10.0 1 07/27/2022 18:53 WG1900474
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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SAMPLE RESULTS - 01
L1517739
USTG480-MW19
Collected date/time: 07/20/22 09:55
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
2,2-Oxybis(1-Chloropropane)108-60-1 5.00 J4 U 0.210 5.00 10.0 1 07/27/2022 18:53 WG1900474
4-Bromophenyl-phenylether 101-55-3 5.00 U 0.0877 5.00 10.0 1 07/27/2022 18:53 WG1900474
2-Chloronaphthalene 91-58-7 0.500 U 0.0648 0.500 1.00 1 07/27/2022 18:53 WG1900474
4-Chlorophenyl-phenylether 7005-72-3 5.00 U 0.0926 5.00 10.0 1 07/27/2022 18:53 WG1900474
Chrysene 218-01-9 0.500 U 0.130 0.500 1.00 1 07/27/2022 18:53 WG1900474
Dibenz(a,h)anthracene 53-70-3 0.500 U 0.0644 0.500 1.00 1 07/27/2022 18:53 WG1900474
3,3-Dichlorobenzidine 91-94-1 5.00 U 0.212 5.00 10.0 1 07/27/2022 18:53 WG1900474
2,4-Dinitrotoluene 121-14-2 5.00 U 0.0983 5.00 10.0 1 07/27/2022 18:53 WG1900474
2,6-Dinitrotoluene 606-20-2 5.00 J4 U 0.250 5.00 10.0 1 07/27/2022 18:53 WG1900474
Fluoranthene 206-44-0 0.500 J4 U 0.102 0.500 1.00 1 07/27/2022 18:53 WG1900474
Fluorene 86-73-7 0.500 U 0.0844 0.500 1.00 1 07/27/2022 18:53 WG1900474
Hexachlorobenzene 118-74-1 0.500 U 0.0755 0.500 1.00 1 07/27/2022 18:53 WG1900474
Hexachloro-1,3-butadiene 87-68-3 5.00 U 0.0968 5.00 10.0 1 07/27/2022 18:53 WG1900474
Hexachlorocyclopentadiene 77-47-4 5.00 U 0.0598 5.00 10.0 1 07/27/2022 18:53 WG1900474
Hexachloroethane 67-72-1 5.00 U 0.127 5.00 10.0 1 07/27/2022 18:53 WG1900474
Indeno(1,2,3-cd)pyrene 193-39-5 0.600 U 0.279 0.600 1.20 1 07/27/2022 18:53 WG1900474
Isophorone 78-59-1 5.00 U 0.143 5.00 10.0 1 07/27/2022 18:53 WG1900474
Naphthalene 91-20-3 0.500 J4 U 0.159 0.500 1.00 1 07/27/2022 18:53 WG1900474
Nitrobenzene 98-95-3 5.00 J4 U 0.297 5.00 10.0 1 07/27/2022 18:53 WG1900474
n-Nitrosodimethylamine 62-75-9 5.00 U 0.998 5.00 10.0 1 07/27/2022 18:53 WG1900474
n-Nitrosodiphenylamine 86-30-6 5.00 U 2.37 5.00 10.0 1 07/27/2022 18:53 WG1900474
n-Nitrosodi-n-propylamine 621-64-7 5.00 J4 U 0.261 5.00 10.0 1 07/27/2022 18:53 WG1900474
Phenanthrene 85-01-8 0.500 J4 U 0.112 0.500 1.00 1 07/27/2022 18:53 WG1900474
Benzylbutyl phthalate 85-68-7 2.00 U 0.765 2.00 4.00 1 07/27/2022 18:53 WG1900474
Bis(2-ethylhexyl)phthalate 117-81-7 2.00 J4 U 0.895 2.00 4.00 1 07/27/2022 18:53 WG1900474
Di-n-butyl phthalate 84-74-2 1.50 J4 U 0.453 1.50 3.00 1 07/27/2022 18:53 WG1900474
Diethyl phthalate 84-66-2 1.50 J4 U 0.287 1.50 3.00 1 07/27/2022 18:53 WG1900474
Dimethyl phthalate 131-11-3 1.50 U 0.260 1.50 3.00 1 07/27/2022 18:53 WG1900474
Di-n-octyl phthalate 117-84-0 2.00 U 0.932 2.00 4.00 1 07/27/2022 18:53 WG1900474
Pyrene 129-00-0 0.500 J4 U 0.107 0.500 1.00 1 07/27/2022 18:53 WG1900474
1,2,4-Trichlorobenzene 120-82-1 5.00 U 0.0698 5.00 10.0 1 07/27/2022 18:53 WG1900474
4-Chloro-3-methylphenol 59-50-7 5.00 J4 U 0.131 5.00 10.0 1 07/27/2022 18:53 WG1900474
2-Chlorophenol 95-57-8 5.00 J4 U 0.133 5.00 10.0 1 07/27/2022 18:53 WG1900474
2,4-Dichlorophenol 120-83-2 5.00 J4 U 0.102 5.00 10.0 1 07/27/2022 18:53 WG1900474
2,4-Dimethylphenol 105-67-9 5.00 U 0.0636 5.00 10.0 1 07/27/2022 18:53 WG1900474
4,6-Dinitro-2-methylphenol 534-52-1 5.00 U 1.12 5.00 10.0 1 07/27/2022 18:53 WG1900474
2,4-Dinitrophenol 51-28-5 15.0 U 5.93 15.0 30.0 1 07/27/2022 18:53 WG1900474
2-Nitrophenol 88-75-5 5.00 J4 U 0.117 5.00 10.0 1 07/27/2022 18:53 WG1900474
4-Nitrophenol 100-02-7 5.00 U 0.143 5.00 10.0 1 07/27/2022 18:53 WG1900474
Pentachlorophenol 87-86-5 5.00 U 0.313 5.00 10.0 1 07/27/2022 18:53 WG1900474
Phenol 108-95-2 10.0 U 4.33 10.0 20.0 1 07/27/2022 18:53 WG1900474
2,4,6-Trichlorophenol 88-06-2 5.00 U 0.100 5.00 10.0 1 07/27/2022 18:53 WG1900474
(S) Nitrobenzene-d5 4165-60-0 33.7 J2 0.000 44.0-120 07/27/2022 18:53 WG1900474
(S) 2-Fluorobiphenyl 321-60-8 40.3 J2 0.000 44.0-119 07/27/2022 18:53 WG1900474
(S) p-Terphenyl-d14 1718-51-0 56.3 0.000 50.0-134 07/27/2022 18:53 WG1900474
(S) Phenol-d5 4165-62-2 10.2 0.000 10.0-67.0 07/27/2022 18:53 WG1900474
(S) 2-Fluorophenol 367-12-4 14.5 J2 0.000 19.0-119 07/27/2022 18:53 WG1900474
(S) 2,4,6-Tribromophenol 118-79-6 54.2 0.000 43.0-140 07/27/2022 18:53 WG1900474
Sample Narrative:
L1517739-01 WG1900474: Surrogate recovery within historical limits.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 10 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 10 of 84
====================----□ □ □ □
□ □ □ □
SAMPLE RESULTS - 02
L1517739
USTG480-MW16
Collected date/time: 07/20/22 10:10
Volatile Petroleum Hydrocarbons by Method MADEPV
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics C5-C8 ALI
UNADJ 67.0 U 33.3 67.0 100 1 07/29/2022 20:58 WG1902102
Unadjusted C9-C12 Aliphatics C9-C12 ALI
UNADJ 40.3 B J 33.3 67.0 134 1 07/29/2022 20:58 WG1902102
Unadjusted C9-C10 Aromatics C9-C10 ARO
UNADJ 67.0 U 33.3 67.0 100 1 07/29/2022 20:58 WG1902102
Total VPH VPH 150 U 66.7 150 300 1 07/29/2022 20:58 WG1902102
(S) 2,5-Dibromotoluene(FID)615-59-8 94.2 70.0-130 07/29/2022 20:58 WG1902102
(S) 2,5-Dibromotoluene(PID)615-59-8 97.2 70.0-130 07/29/2022 20:58 WG1902102
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acetone 67-64-1 13.2 J J3 11.3 25.0 50.0 1 07/25/2022 17:48 WG1900597
Acrolein 107-02-8 25.0 C4 U 2.54 25.0 50.0 1 07/25/2022 17:48 WG1900597
Acrylonitrile 107-13-1 5.00 J4 U 0.671 5.00 10.0 1 07/25/2022 17:48 WG1900597
Benzene 71-43-2 0.119 J 0.0941 0.500 1.00 1 07/25/2022 17:48 WG1900597
Bromobenzene 108-86-1 0.500 U 0.118 0.500 1.00 1 07/25/2022 17:48 WG1900597
Bromodichloromethane 75-27-4 0.500 U 0.136 0.500 1.00 1 07/25/2022 17:48 WG1900597
Bromoform 75-25-2 0.500 U 0.129 0.500 1.00 1 07/25/2022 17:48 WG1900597
Bromomethane 74-83-9 2.00 U 0.605 2.00 5.00 1 07/25/2022 17:48 WG1900597
n-Butylbenzene 104-51-8 0.500 U 0.157 0.500 1.00 1 07/25/2022 17:48 WG1900597
sec-Butylbenzene 135-98-8 0.500 U 0.125 0.500 1.00 1 07/25/2022 17:48 WG1900597
tert-Butylbenzene 98-06-6 0.500 U 0.127 0.500 1.00 1 07/25/2022 17:48 WG1900597
Carbon tetrachloride 56-23-5 0.500 U 0.128 0.500 1.00 1 07/25/2022 17:48 WG1900597
Chlorobenzene 108-90-7 0.500 U 0.116 0.500 1.00 1 07/25/2022 17:48 WG1900597
Chlorodibromomethane 124-48-1 0.500 U 0.140 0.500 1.00 1 07/25/2022 17:48 WG1900597
Chloroethane 75-00-3 2.00 U 0.192 2.00 5.00 1 07/25/2022 17:48 WG1900597
Chloroform 67-66-3 2.00 U 0.111 2.00 5.00 1 07/25/2022 17:48 WG1900597
Chloromethane 74-87-3 2.00 U 0.960 2.00 4.00 1 07/25/2022 17:48 WG1900597
2-Chlorotoluene 95-49-8 0.500 U 0.106 0.500 1.00 1 07/25/2022 17:48 WG1900597
4-Chlorotoluene 106-43-4 0.500 U 0.114 0.500 1.00 1 07/25/2022 17:48 WG1900597
1,2-Dibromo-3-Chloropropane 96-12-8 2.00 U 0.276 2.00 5.00 1 07/25/2022 17:48 WG1900597
1,2-Dibromoethane 106-93-4 0.500 U 0.126 0.500 1.00 1 07/25/2022 17:48 WG1900597
Dibromomethane 74-95-3 0.500 U 0.122 0.500 1.00 1 07/25/2022 17:48 WG1900597
1,2-Dichlorobenzene 95-50-1 0.500 U 0.107 0.500 1.00 1 07/25/2022 17:48 WG1900597
1,3-Dichlorobenzene 541-73-1 0.500 U 0.110 0.500 1.00 1 07/25/2022 17:48 WG1900597
1,4-Dichlorobenzene 106-46-7 0.500 U 0.120 0.500 1.00 1 07/25/2022 17:48 WG1900597
Dichlorodifluoromethane 75-71-8 2.00 U 0.374 2.00 5.00 1 07/25/2022 17:48 WG1900597
1,1-Dichloroethane 75-34-3 0.500 U 0.100 0.500 1.00 1 07/25/2022 17:48 WG1900597
1,2-Dichloroethane 107-06-2 0.500 U 0.0819 0.500 1.00 1 07/25/2022 17:48 WG1900597
1,1-Dichloroethene 75-35-4 0.500 U 0.188 0.500 1.00 1 07/25/2022 17:48 WG1900597
cis-1,2-Dichloroethene 156-59-2 3.07 0.126 0.500 1.00 1 07/25/2022 17:48 WG1900597
trans-1,2-Dichloroethene 156-60-5 0.500 U 0.149 0.500 1.00 1 07/25/2022 17:48 WG1900597
1,2-Dichloropropane 78-87-5 0.500 U 0.149 0.500 1.00 1 07/25/2022 17:48 WG1900597
1,1-Dichloropropene 563-58-6 0.500 U 0.142 0.500 1.00 1 07/25/2022 17:48 WG1900597
1,3-Dichloropropane 142-28-9 0.500 U 0.110 0.500 1.00 1 07/25/2022 17:48 WG1900597
2,2-Dichloropropane 594-20-7 0.500 U 0.161 0.500 1.00 1 07/25/2022 17:48 WG1900597
Di-isopropyl ether 108-20-3 0.500 U 0.105 0.500 1.00 1 07/25/2022 17:48 WG1900597
Ethylbenzene 100-41-4 0.500 U 0.137 0.500 1.00 1 07/25/2022 17:48 WG1900597
Hexachloro-1,3-butadiene 87-68-3 0.750 J3 U 0.337 0.750 1.50 1 07/25/2022 17:48 WG1900597
Isopropylbenzene 98-82-8 0.500 U 0.105 0.500 1.00 1 07/25/2022 17:48 WG1900597
p-Isopropyltoluene 99-87-6 0.500 U 0.120 0.500 1.00 1 07/25/2022 17:48 WG1900597
2-Butanone (MEK)78-93-3 5.00 U 1.19 5.00 10.0 1 07/25/2022 17:48 WG1900597
Methylene Chloride 75-09-2 2.00 U 0.430 2.00 5.00 1 07/25/2022 17:48 WG1900597
4-Methyl-2-pentanone (MIBK)108-10-1 5.00 U 0.478 5.00 10.0 1 07/25/2022 17:48 WG1900597
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 11 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 11 of 84
--------------=---□
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SAMPLE RESULTS - 02
L1517739
USTG480-MW16
Collected date/time: 07/20/22 10:10
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Methyl tert-butyl ether 1634-04-4 0.500 U 0.101 0.500 1.00 1 07/25/2022 17:48 WG1900597
Naphthalene 91-20-3 2.00 U 1.00 2.00 5.00 1 07/25/2022 17:48 WG1900597
n-Propylbenzene 103-65-1 0.500 U 0.0993 0.500 1.00 1 07/25/2022 17:48 WG1900597
Styrene 100-42-5 0.500 U 0.118 0.500 1.00 1 07/25/2022 17:48 WG1900597
1,1,1,2-Tetrachloroethane 630-20-6 0.500 U 0.147 0.500 1.00 1 07/25/2022 17:48 WG1900597
1,1,2,2-Tetrachloroethane 79-34-5 0.500 U 0.133 0.500 1.00 1 07/25/2022 17:48 WG1900597
Tetrachloroethene 127-18-4 0.600 U 0.300 0.600 1.20 1 07/25/2022 17:48 WG1900597
Toluene 108-88-3 0.600 U 0.278 0.600 1.20 1 07/25/2022 17:48 WG1900597
1,2,3-Trichlorobenzene 87-61-6 0.500 U 0.230 0.500 1.00 1 07/25/2022 17:48 WG1900597
1,2,4-Trichlorobenzene 120-82-1 1.00 U 0.481 1.00 2.00 1 07/25/2022 17:48 WG1900597
1,1,1-Trichloroethane 71-55-6 0.500 U 0.149 0.500 1.00 1 07/25/2022 17:48 WG1900597
1,1,2-Trichloroethane 79-00-5 0.500 U 0.158 0.500 1.00 1 07/25/2022 17:48 WG1900597
Trichloroethene 79-01-6 0.500 U 0.190 0.500 1.00 1 07/25/2022 17:48 WG1900597
Trichlorofluoromethane 75-69-4 2.00 U 0.160 2.00 5.00 1 07/25/2022 17:48 WG1900597
1,2,3-Trichloropropane 96-18-4 1.00 U 0.237 1.00 2.50 1 07/25/2022 17:48 WG1900597
1,2,4-Trimethylbenzene 95-63-6 1.00 U 0.322 1.00 2.00 1 07/25/2022 17:48 WG1900597
1,3,5-Trimethylbenzene 108-67-8 0.500 U 0.104 0.500 1.00 1 07/25/2022 17:48 WG1900597
Vinyl chloride 75-01-4 3.95 0.234 0.500 1.00 1 08/03/2022 20:57 WG1905109
o-Xylene 95-47-6 0.500 U 0.174 0.500 1.00 1 07/25/2022 17:48 WG1900597
m&p-Xylenes 1330-20-7 1.00 U 0.430 1.00 2.00 1 07/25/2022 17:48 WG1900597
(S) Toluene-d8 2037-26-5 96.8 89.0-112 07/25/2022 17:48 WG1900597
(S) Toluene-d8 2037-26-5 103 89.0-112 08/03/2022 20:57 WG1905109
(S) 4-Bromofluorobenzene 460-00-4 94.4 85.0-114 07/25/2022 17:48 WG1900597
(S) 4-Bromofluorobenzene 460-00-4 103 85.0-114 08/03/2022 20:57 WG1905109
(S) 1,2-Dichloroethane-d4 17060-07-0 105 81.0-118 07/25/2022 17:48 WG1900597
(S) 1,2-Dichloroethane-d4 17060-07-0 87.1 81.0-118 08/03/2022 20:57 WG1905109
TPH by Method MADEPE
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics C9-C18 ALI
UNADJ 67.0 U 33.3 67.0 134 1 08/01/2022 22:50 WG1902750
Unadjusted C19-C36 Aliphatics C19-C36 ALI
UNADJ 33.3 J 33.3 67.0 134 1 08/01/2022 22:50 WG1902750
Unadjusted C11-C22 Aromatics C11-C22 ARO
UNADJ 47.3 B J 33.3 67.0 134 1 08/02/2022 05:06 WG1902750
Unadjusted Total Petroleum
Hydrocarbons TPH UNADJ 80.6 B J 33.3 67.0 134 1 08/02/2022 05:06 WG1902750
(S) o-Terphenyl 84-15-1 77.3 40.0-140 08/02/2022 05:06 WG1902750
(S) 1-Chloro-octadecane 3386-33-2 64.2 40.0-140 08/01/2022 22:50 WG1902750
(S) 2-Fluorobiphenyl 321-60-8 94.4 40.0-140 08/02/2022 05:06 WG1902750
(S) 2-Bromonaphthalene 580-13-2 91.1 40.0-140 08/02/2022 05:06 WG1902750
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acenaphthene 83-32-9 0.500 U 0.0886 0.500 1.00 1 07/27/2022 20:21 WG1900474
Acenaphthylene 208-96-8 0.500 U 0.0921 0.500 1.00 1 07/27/2022 20:21 WG1900474
Anthracene 120-12-7 0.500 J4 U 0.0804 0.500 1.00 1 07/27/2022 20:21 WG1900474
Benzidine 92-87-5 7.50 J4 U 3.74 7.50 15.0 1 07/27/2022 20:21 WG1900474
Benzo(a)anthracene 56-55-3 0.500 U 0.199 0.500 1.00 1 07/27/2022 20:21 WG1900474
Benzo(b)fluoranthene 205-99-2 0.500 U 0.130 0.500 1.00 1 07/27/2022 20:21 WG1900474
Benzo(k)fluoranthene 207-08-9 0.500 U 0.120 0.500 1.00 1 07/27/2022 20:21 WG1900474
Benzo(g,h,i)perylene 191-24-2 0.500 U 0.121 0.500 1.00 1 07/27/2022 20:21 WG1900474
Benzo(a)pyrene 50-32-8 0.500 U 0.0381 0.500 1.00 1 07/27/2022 20:21 WG1900474
Bis(2-chlorethoxy)methane 111-91-1 5.00 J4 U 0.116 5.00 10.0 1 07/27/2022 20:21 WG1900474
Bis(2-chloroethyl)ether 111-44-4 5.00 J4 U 0.137 5.00 10.0 1 07/27/2022 20:21 WG1900474
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 12 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 12 of 84
====================----□ □ □ □
□ □ □ □
SAMPLE RESULTS - 02
L1517739
USTG480-MW16
Collected date/time: 07/20/22 10:10
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
2,2-Oxybis(1-Chloropropane)108-60-1 5.00 J4 U 0.210 5.00 10.0 1 07/27/2022 20:21 WG1900474
4-Bromophenyl-phenylether 101-55-3 5.00 U 0.0877 5.00 10.0 1 07/27/2022 20:21 WG1900474
2-Chloronaphthalene 91-58-7 0.500 U 0.0648 0.500 1.00 1 07/27/2022 20:21 WG1900474
4-Chlorophenyl-phenylether 7005-72-3 5.00 U 0.0926 5.00 10.0 1 07/27/2022 20:21 WG1900474
Chrysene 218-01-9 0.500 U 0.130 0.500 1.00 1 07/27/2022 20:21 WG1900474
Dibenz(a,h)anthracene 53-70-3 0.500 U 0.0644 0.500 1.00 1 07/27/2022 20:21 WG1900474
3,3-Dichlorobenzidine 91-94-1 5.00 U 0.212 5.00 10.0 1 07/27/2022 20:21 WG1900474
2,4-Dinitrotoluene 121-14-2 5.00 U 0.0983 5.00 10.0 1 07/27/2022 20:21 WG1900474
2,6-Dinitrotoluene 606-20-2 5.00 J4 U 0.250 5.00 10.0 1 07/27/2022 20:21 WG1900474
Fluoranthene 206-44-0 0.500 J4 U 0.102 0.500 1.00 1 07/27/2022 20:21 WG1900474
Fluorene 86-73-7 0.500 U 0.0844 0.500 1.00 1 07/27/2022 20:21 WG1900474
Hexachlorobenzene 118-74-1 0.500 U 0.0755 0.500 1.00 1 07/27/2022 20:21 WG1900474
Hexachloro-1,3-butadiene 87-68-3 5.00 U 0.0968 5.00 10.0 1 07/27/2022 20:21 WG1900474
Hexachlorocyclopentadiene 77-47-4 5.00 U 0.0598 5.00 10.0 1 07/27/2022 20:21 WG1900474
Hexachloroethane 67-72-1 5.00 U 0.127 5.00 10.0 1 07/27/2022 20:21 WG1900474
Indeno(1,2,3-cd)pyrene 193-39-5 0.600 U 0.279 0.600 1.20 1 07/27/2022 20:21 WG1900474
Isophorone 78-59-1 5.00 U 0.143 5.00 10.0 1 07/27/2022 20:21 WG1900474
Naphthalene 91-20-3 0.500 J4 U 0.159 0.500 1.00 1 07/27/2022 20:21 WG1900474
Nitrobenzene 98-95-3 5.00 J4 U 0.297 5.00 10.0 1 07/27/2022 20:21 WG1900474
n-Nitrosodimethylamine 62-75-9 5.00 U 0.998 5.00 10.0 1 07/27/2022 20:21 WG1900474
n-Nitrosodiphenylamine 86-30-6 5.00 U 2.37 5.00 10.0 1 07/27/2022 20:21 WG1900474
n-Nitrosodi-n-propylamine 621-64-7 5.00 J4 U 0.261 5.00 10.0 1 07/27/2022 20:21 WG1900474
Phenanthrene 85-01-8 0.500 J4 U 0.112 0.500 1.00 1 07/27/2022 20:21 WG1900474
Benzylbutyl phthalate 85-68-7 2.00 U 0.765 2.00 4.00 1 07/27/2022 20:21 WG1900474
Bis(2-ethylhexyl)phthalate 117-81-7 2.00 J4 U 0.895 2.00 4.00 1 07/27/2022 20:21 WG1900474
Di-n-butyl phthalate 84-74-2 1.50 J4 U 0.453 1.50 3.00 1 07/27/2022 20:21 WG1900474
Diethyl phthalate 84-66-2 1.50 J4 U 0.287 1.50 3.00 1 07/27/2022 20:21 WG1900474
Dimethyl phthalate 131-11-3 1.50 U 0.260 1.50 3.00 1 07/27/2022 20:21 WG1900474
Di-n-octyl phthalate 117-84-0 2.00 U 0.932 2.00 4.00 1 07/27/2022 20:21 WG1900474
Pyrene 129-00-0 0.500 J4 U 0.107 0.500 1.00 1 07/27/2022 20:21 WG1900474
1,2,4-Trichlorobenzene 120-82-1 5.00 U 0.0698 5.00 10.0 1 07/27/2022 20:21 WG1900474
4-Chloro-3-methylphenol 59-50-7 5.00 J4 U 0.131 5.00 10.0 1 07/27/2022 20:21 WG1900474
2-Chlorophenol 95-57-8 5.00 J4 U 0.133 5.00 10.0 1 07/27/2022 20:21 WG1900474
2,4-Dichlorophenol 120-83-2 5.00 J4 U 0.102 5.00 10.0 1 07/27/2022 20:21 WG1900474
2,4-Dimethylphenol 105-67-9 5.00 U 0.0636 5.00 10.0 1 07/27/2022 20:21 WG1900474
4,6-Dinitro-2-methylphenol 534-52-1 5.00 U 1.12 5.00 10.0 1 07/27/2022 20:21 WG1900474
2,4-Dinitrophenol 51-28-5 15.0 U 5.93 15.0 30.0 1 07/27/2022 20:21 WG1900474
2-Nitrophenol 88-75-5 5.00 J4 U 0.117 5.00 10.0 1 07/27/2022 20:21 WG1900474
4-Nitrophenol 100-02-7 5.00 U 0.143 5.00 10.0 1 07/27/2022 20:21 WG1900474
Pentachlorophenol 87-86-5 5.00 U 0.313 5.00 10.0 1 07/27/2022 20:21 WG1900474
Phenol 108-95-2 10.0 U 4.33 10.0 20.0 1 07/27/2022 20:21 WG1900474
2,4,6-Trichlorophenol 88-06-2 5.00 U 0.100 5.00 10.0 1 07/27/2022 20:21 WG1900474
(S) Nitrobenzene-d5 4165-60-0 42.0 J2 0.000 44.0-120 07/27/2022 20:21 WG1900474
(S) 2-Fluorobiphenyl 321-60-8 47.9 0.000 44.0-119 07/27/2022 20:21 WG1900474
(S) p-Terphenyl-d14 1718-51-0 61.0 0.000 50.0-134 07/27/2022 20:21 WG1900474
(S) Phenol-d5 4165-62-2 13.1 0.000 10.0-67.0 07/27/2022 20:21 WG1900474
(S) 2-Fluorophenol 367-12-4 17.8 J2 0.000 19.0-119 07/27/2022 20:21 WG1900474
(S) 2,4,6-Tribromophenol 118-79-6 71.4 0.000 43.0-140 07/27/2022 20:21 WG1900474
Sample Narrative:
L1517739-02 WG1900474: Surrogate recovery within historical limits.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 13 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 13 of 84
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SAMPLE RESULTS - 03
L1517739
USTTC341-MW18
Collected date/time: 07/20/22 10:12
Volatile Petroleum Hydrocarbons by Method MADEPV
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics C5-C8 ALI
UNADJ 69.2 J 33.3 67.0 100 1 07/29/2022 21:30 WG1902102
Unadjusted C9-C12 Aliphatics C9-C12 ALI
UNADJ 128 B J 33.3 67.0 134 1 07/29/2022 21:30 WG1902102
Unadjusted C9-C10 Aromatics C9-C10 ARO
UNADJ 122 33.3 67.0 100 1 07/29/2022 21:30 WG1902102
Total VPH VPH 319 66.7 150 300 1 07/29/2022 21:30 WG1902102
(S) 2,5-Dibromotoluene(FID)615-59-8 101 70.0-130 07/29/2022 21:30 WG1902102
(S) 2,5-Dibromotoluene(PID)615-59-8 95.9 70.0-130 07/29/2022 21:30 WG1902102
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acetone 67-64-1 22.6 J J3 11.3 25.0 50.0 1 07/25/2022 18:09 WG1900597
Acrolein 107-02-8 25.0 C4 U 2.54 25.0 50.0 1 07/25/2022 18:09 WG1900597
Acrylonitrile 107-13-1 5.00 J4 U 0.671 5.00 10.0 1 07/25/2022 18:09 WG1900597
Benzene 71-43-2 19.7 0.0941 0.500 1.00 1 07/25/2022 18:09 WG1900597
Bromobenzene 108-86-1 0.500 U 0.118 0.500 1.00 1 07/25/2022 18:09 WG1900597
Bromodichloromethane 75-27-4 0.500 U 0.136 0.500 1.00 1 07/25/2022 18:09 WG1900597
Bromoform 75-25-2 0.500 U 0.129 0.500 1.00 1 07/25/2022 18:09 WG1900597
Bromomethane 74-83-9 2.00 U 0.605 2.00 5.00 1 07/25/2022 18:09 WG1900597
n-Butylbenzene 104-51-8 1.08 0.157 0.500 1.00 1 07/25/2022 18:09 WG1900597
sec-Butylbenzene 135-98-8 1.61 0.125 0.500 1.00 1 07/25/2022 18:09 WG1900597
tert-Butylbenzene 98-06-6 0.257 J 0.127 0.500 1.00 1 07/25/2022 18:09 WG1900597
Carbon tetrachloride 56-23-5 0.500 U 0.128 0.500 1.00 1 07/25/2022 18:09 WG1900597
Chlorobenzene 108-90-7 0.500 U 0.116 0.500 1.00 1 07/25/2022 18:09 WG1900597
Chlorodibromomethane 124-48-1 0.500 U 0.140 0.500 1.00 1 07/25/2022 18:09 WG1900597
Chloroethane 75-00-3 2.00 U 0.192 2.00 5.00 1 07/25/2022 18:09 WG1900597
Chloroform 67-66-3 2.00 U 0.111 2.00 5.00 1 07/25/2022 18:09 WG1900597
Chloromethane 74-87-3 2.00 U 0.960 2.00 4.00 1 07/25/2022 18:09 WG1900597
2-Chlorotoluene 95-49-8 0.500 U 0.106 0.500 1.00 1 07/25/2022 18:09 WG1900597
4-Chlorotoluene 106-43-4 0.500 U 0.114 0.500 1.00 1 07/25/2022 18:09 WG1900597
1,2-Dibromo-3-Chloropropane 96-12-8 2.00 U 0.276 2.00 5.00 1 07/25/2022 18:09 WG1900597
1,2-Dibromoethane 106-93-4 0.500 U 0.126 0.500 1.00 1 07/25/2022 18:09 WG1900597
Dibromomethane 74-95-3 0.500 U 0.122 0.500 1.00 1 07/25/2022 18:09 WG1900597
1,2-Dichlorobenzene 95-50-1 0.500 U 0.107 0.500 1.00 1 07/25/2022 18:09 WG1900597
1,3-Dichlorobenzene 541-73-1 0.500 U 0.110 0.500 1.00 1 07/25/2022 18:09 WG1900597
1,4-Dichlorobenzene 106-46-7 0.500 U 0.120 0.500 1.00 1 07/25/2022 18:09 WG1900597
Dichlorodifluoromethane 75-71-8 2.00 U 0.374 2.00 5.00 1 07/25/2022 18:09 WG1900597
1,1-Dichloroethane 75-34-3 0.500 U 0.100 0.500 1.00 1 07/25/2022 18:09 WG1900597
1,2-Dichloroethane 107-06-2 0.500 U 0.0819 0.500 1.00 1 07/25/2022 18:09 WG1900597
1,1-Dichloroethene 75-35-4 0.500 U 0.188 0.500 1.00 1 07/25/2022 18:09 WG1900597
cis-1,2-Dichloroethene 156-59-2 0.332 J 0.126 0.500 1.00 1 07/25/2022 18:09 WG1900597
trans-1,2-Dichloroethene 156-60-5 0.500 U 0.149 0.500 1.00 1 07/25/2022 18:09 WG1900597
1,2-Dichloropropane 78-87-5 0.500 U 0.149 0.500 1.00 1 07/25/2022 18:09 WG1900597
1,1-Dichloropropene 563-58-6 0.500 U 0.142 0.500 1.00 1 07/25/2022 18:09 WG1900597
1,3-Dichloropropane 142-28-9 0.500 U 0.110 0.500 1.00 1 07/25/2022 18:09 WG1900597
2,2-Dichloropropane 594-20-7 0.500 U 0.161 0.500 1.00 1 07/25/2022 18:09 WG1900597
Di-isopropyl ether 108-20-3 2.31 0.105 0.500 1.00 1 07/25/2022 18:09 WG1900597
Ethylbenzene 100-41-4 2.85 0.137 0.500 1.00 1 07/25/2022 18:09 WG1900597
Hexachloro-1,3-butadiene 87-68-3 0.750 J3 U 0.337 0.750 1.50 1 07/25/2022 18:09 WG1900597
Isopropylbenzene 98-82-8 7.39 0.105 0.500 1.00 1 07/25/2022 18:09 WG1900597
p-Isopropyltoluene 99-87-6 0.500 U 0.120 0.500 1.00 1 07/25/2022 18:09 WG1900597
2-Butanone (MEK)78-93-3 5.00 U 1.19 5.00 10.0 1 07/25/2022 18:09 WG1900597
Methylene Chloride 75-09-2 2.00 U 0.430 2.00 5.00 1 07/25/2022 18:09 WG1900597
4-Methyl-2-pentanone (MIBK)108-10-1 5.00 U 0.478 5.00 10.0 1 07/25/2022 18:09 WG1900597
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 14 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 14 of 84
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SAMPLE RESULTS - 03
L1517739
USTTC341-MW18
Collected date/time: 07/20/22 10:12
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Methyl tert-butyl ether 1634-04-4 0.500 U 0.101 0.500 1.00 1 07/25/2022 18:09 WG1900597
Naphthalene 91-20-3 52.7 1.00 2.00 5.00 1 07/25/2022 18:09 WG1900597
n-Propylbenzene 103-65-1 9.85 0.0993 0.500 1.00 1 07/25/2022 18:09 WG1900597
Styrene 100-42-5 0.500 U 0.118 0.500 1.00 1 07/25/2022 18:09 WG1900597
1,1,1,2-Tetrachloroethane 630-20-6 0.500 U 0.147 0.500 1.00 1 07/25/2022 18:09 WG1900597
1,1,2,2-Tetrachloroethane 79-34-5 0.500 U 0.133 0.500 1.00 1 07/25/2022 18:09 WG1900597
Tetrachloroethene 127-18-4 0.600 U 0.300 0.600 1.20 1 07/25/2022 18:09 WG1900597
Toluene 108-88-3 3.52 0.278 0.600 1.20 1 07/25/2022 18:09 WG1900597
1,2,3-Trichlorobenzene 87-61-6 0.500 U 0.230 0.500 1.00 1 07/25/2022 18:09 WG1900597
1,2,4-Trichlorobenzene 120-82-1 1.00 U 0.481 1.00 2.00 1 07/25/2022 18:09 WG1900597
1,1,1-Trichloroethane 71-55-6 0.500 U 0.149 0.500 1.00 1 07/25/2022 18:09 WG1900597
1,1,2-Trichloroethane 79-00-5 0.500 U 0.158 0.500 1.00 1 07/25/2022 18:09 WG1900597
Trichloroethene 79-01-6 0.500 U 0.190 0.500 1.00 1 07/25/2022 18:09 WG1900597
Trichlorofluoromethane 75-69-4 2.00 U 0.160 2.00 5.00 1 07/25/2022 18:09 WG1900597
1,2,3-Trichloropropane 96-18-4 1.00 U 0.237 1.00 2.50 1 07/25/2022 18:09 WG1900597
1,2,4-Trimethylbenzene 95-63-6 3.43 0.322 1.00 2.00 1 07/25/2022 18:09 WG1900597
1,3,5-Trimethylbenzene 108-67-8 0.542 J 0.104 0.500 1.00 1 07/25/2022 18:09 WG1900597
Vinyl chloride 75-01-4 0.500 U 0.234 0.500 1.00 1 07/25/2022 18:09 WG1900597
o-Xylene 95-47-6 1.66 0.174 0.500 1.00 1 07/25/2022 18:09 WG1900597
m&p-Xylenes 1330-20-7 3.31 0.430 1.00 2.00 1 07/25/2022 18:09 WG1900597
(S) Toluene-d8 2037-26-5 97.6 89.0-112 07/25/2022 18:09 WG1900597
(S) 4-Bromofluorobenzene 460-00-4 97.8 85.0-114 07/25/2022 18:09 WG1900597
(S) 1,2-Dichloroethane-d4 17060-07-0 101 81.0-118 07/25/2022 18:09 WG1900597
TPH by Method MADEPE
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics C9-C18 ALI
UNADJ 1040 33.3 67.0 134 1 08/01/2022 23:12 WG1902750
Unadjusted C19-C36 Aliphatics C19-C36 ALI
UNADJ 244 B 33.3 67.0 134 1 08/01/2022 23:12 WG1902750
Unadjusted C11-C22 Aromatics C11-C22 ARO
UNADJ 727 33.3 67.0 134 1 08/02/2022 04:44 WG1902750
Unadjusted Total Petroleum
Hydrocarbons TPH UNADJ 2010 33.3 67.0 134 1 08/02/2022 04:44 WG1902750
(S) o-Terphenyl 84-15-1 67.5 40.0-140 08/02/2022 04:44 WG1902750
(S) 1-Chloro-octadecane 3386-33-2 48.0 40.0-140 08/01/2022 23:12 WG1902750
(S) 2-Fluorobiphenyl 321-60-8 91.6 40.0-140 08/02/2022 04:44 WG1902750
(S) 2-Bromonaphthalene 580-13-2 87.4 40.0-140 08/02/2022 04:44 WG1902750
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acenaphthene 83-32-9 0.571 J 0.0886 0.500 1.00 1 07/27/2022 22:12 WG1900474
Acenaphthylene 208-96-8 0.500 U 0.0921 0.500 1.00 1 07/27/2022 22:12 WG1900474
Anthracene 120-12-7 0.500 J4 U 0.0804 0.500 1.00 1 07/27/2022 22:12 WG1900474
Benzidine 92-87-5 7.50 J4 U 3.74 7.50 15.0 1 07/27/2022 22:12 WG1900474
Benzo(a)anthracene 56-55-3 0.500 U 0.199 0.500 1.00 1 07/27/2022 22:12 WG1900474
Benzo(b)fluoranthene 205-99-2 0.500 U 0.130 0.500 1.00 1 07/27/2022 22:12 WG1900474
Benzo(k)fluoranthene 207-08-9 0.500 U 0.120 0.500 1.00 1 07/27/2022 22:12 WG1900474
Benzo(g,h,i)perylene 191-24-2 0.500 U 0.121 0.500 1.00 1 07/27/2022 22:12 WG1900474
Benzo(a)pyrene 50-32-8 0.500 U 0.0381 0.500 1.00 1 07/27/2022 22:12 WG1900474
Bis(2-chlorethoxy)methane 111-91-1 5.00 J4 U 0.116 5.00 10.0 1 07/27/2022 22:12 WG1900474
Bis(2-chloroethyl)ether 111-44-4 5.00 J4 U 0.137 5.00 10.0 1 07/27/2022 22:12 WG1900474
2,2-Oxybis(1-Chloropropane)108-60-1 5.00 J4 U 0.210 5.00 10.0 1 07/27/2022 22:12 WG1900474
4-Bromophenyl-phenylether 101-55-3 5.00 U 0.0877 5.00 10.0 1 07/27/2022 22:12 WG1900474
2-Chloronaphthalene 91-58-7 0.500 U 0.0648 0.500 1.00 1 07/27/2022 22:12 WG1900474
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 15 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 15 of 84
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SAMPLE RESULTS - 03
L1517739
USTTC341-MW18
Collected date/time: 07/20/22 10:12
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
4-Chlorophenyl-phenylether 7005-72-3 5.00 U 0.0926 5.00 10.0 1 07/27/2022 22:12 WG1900474
Chrysene 218-01-9 0.500 U 0.130 0.500 1.00 1 07/27/2022 22:12 WG1900474
Dibenz(a,h)anthracene 53-70-3 0.500 U 0.0644 0.500 1.00 1 07/27/2022 22:12 WG1900474
3,3-Dichlorobenzidine 91-94-1 5.00 U 0.212 5.00 10.0 1 07/27/2022 22:12 WG1900474
2,4-Dinitrotoluene 121-14-2 5.00 U 0.0983 5.00 10.0 1 07/27/2022 22:12 WG1900474
2,6-Dinitrotoluene 606-20-2 5.00 J4 U 0.250 5.00 10.0 1 07/27/2022 22:12 WG1900474
Fluoranthene 206-44-0 0.180 J J4 0.102 0.500 1.00 1 07/27/2022 22:12 WG1900474
Fluorene 86-73-7 1.06 0.0844 0.500 1.00 1 07/27/2022 22:12 WG1900474
Hexachlorobenzene 118-74-1 0.500 U 0.0755 0.500 1.00 1 07/27/2022 22:12 WG1900474
Hexachloro-1,3-butadiene 87-68-3 5.00 U 0.0968 5.00 10.0 1 07/27/2022 22:12 WG1900474
Hexachlorocyclopentadiene 77-47-4 5.00 U 0.0598 5.00 10.0 1 07/27/2022 22:12 WG1900474
Hexachloroethane 67-72-1 5.00 U 0.127 5.00 10.0 1 07/27/2022 22:12 WG1900474
Indeno(1,2,3-cd)pyrene 193-39-5 0.600 U 0.279 0.600 1.20 1 07/27/2022 22:12 WG1900474
Isophorone 78-59-1 5.00 U 0.143 5.00 10.0 1 07/27/2022 22:12 WG1900474
Naphthalene 91-20-3 0.500 J4 U 0.159 0.500 1.00 1 07/27/2022 22:12 WG1900474
Nitrobenzene 98-95-3 5.00 J4 U 0.297 5.00 10.0 1 07/27/2022 22:12 WG1900474
n-Nitrosodimethylamine 62-75-9 5.00 U 0.998 5.00 10.0 1 07/27/2022 22:12 WG1900474
n-Nitrosodiphenylamine 86-30-6 5.00 U 2.37 5.00 10.0 1 07/27/2022 22:12 WG1900474
n-Nitrosodi-n-propylamine 621-64-7 5.00 J4 U 0.261 5.00 10.0 1 07/27/2022 22:12 WG1900474
Phenanthrene 85-01-8 2.45 J4 0.112 0.500 1.00 1 07/27/2022 22:12 WG1900474
Benzylbutyl phthalate 85-68-7 2.00 U 0.765 2.00 4.00 1 07/27/2022 22:12 WG1900474
Bis(2-ethylhexyl)phthalate 117-81-7 2.00 J4 U 0.895 2.00 4.00 1 07/27/2022 22:12 WG1900474
Di-n-butyl phthalate 84-74-2 1.50 J4 U 0.453 1.50 3.00 1 07/27/2022 22:12 WG1900474
Diethyl phthalate 84-66-2 1.50 J4 U 0.287 1.50 3.00 1 07/27/2022 22:12 WG1900474
Dimethyl phthalate 131-11-3 1.50 U 0.260 1.50 3.00 1 07/27/2022 22:12 WG1900474
Di-n-octyl phthalate 117-84-0 2.00 U 0.932 2.00 4.00 1 07/27/2022 22:12 WG1900474
Pyrene 129-00-0 0.295 J J4 0.107 0.500 1.00 1 07/27/2022 22:12 WG1900474
1,2,4-Trichlorobenzene 120-82-1 5.00 U 0.0698 5.00 10.0 1 07/27/2022 22:12 WG1900474
4-Chloro-3-methylphenol 59-50-7 5.00 J4 U 0.131 5.00 10.0 1 07/27/2022 22:12 WG1900474
2-Chlorophenol 95-57-8 5.00 J4 U 0.133 5.00 10.0 1 07/27/2022 22:12 WG1900474
2,4-Dichlorophenol 120-83-2 5.00 J4 U 0.102 5.00 10.0 1 07/27/2022 22:12 WG1900474
2,4-Dimethylphenol 105-67-9 5.00 U 0.0636 5.00 10.0 1 07/27/2022 22:12 WG1900474
4,6-Dinitro-2-methylphenol 534-52-1 5.00 U 1.12 5.00 10.0 1 07/27/2022 22:12 WG1900474
2,4-Dinitrophenol 51-28-5 15.0 U 5.93 15.0 30.0 1 07/27/2022 22:12 WG1900474
2-Nitrophenol 88-75-5 5.00 J4 U 0.117 5.00 10.0 1 07/27/2022 22:12 WG1900474
4-Nitrophenol 100-02-7 5.00 U 0.143 5.00 10.0 1 07/27/2022 22:12 WG1900474
Pentachlorophenol 87-86-5 5.00 U 0.313 5.00 10.0 1 07/27/2022 22:12 WG1900474
Phenol 108-95-2 10.0 U 4.33 10.0 20.0 1 07/27/2022 22:12 WG1900474
2,4,6-Trichlorophenol 88-06-2 5.00 U 0.100 5.00 10.0 1 07/27/2022 22:12 WG1900474
(S) Nitrobenzene-d5 4165-60-0 44.3 0.000 44.0-120 07/27/2022 22:12 WG1900474
(S) 2-Fluorobiphenyl 321-60-8 58.2 0.000 44.0-119 07/27/2022 22:12 WG1900474
(S) p-Terphenyl-d14 1718-51-0 59.9 0.000 50.0-134 07/27/2022 22:12 WG1900474
(S) Phenol-d5 4165-62-2 12.2 0.000 10.0-67.0 07/27/2022 22:12 WG1900474
(S) 2-Fluorophenol 367-12-4 17.1 J2 0.000 19.0-119 07/27/2022 22:12 WG1900474
(S) 2,4,6-Tribromophenol 118-79-6 64.5 0.000 43.0-140 07/27/2022 22:12 WG1900474
Sample Narrative:
L1517739-03 WG1900474: Surrogate recovery within historical limits.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 16 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 16 of 84
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SAMPLE RESULTS - 04
L1517739
USTG480-MW17
Collected date/time: 07/20/22 11:00
Volatile Petroleum Hydrocarbons by Method MADEPV
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics C5-C8 ALI
UNADJ 67.0 U 33.3 67.0 100 1 07/29/2022 22:03 WG1902102
Unadjusted C9-C12 Aliphatics C9-C12 ALI
UNADJ 73.9 B J 33.3 67.0 134 1 07/29/2022 22:03 WG1902102
Unadjusted C9-C10 Aromatics C9-C10 ARO
UNADJ 67.0 U 33.3 67.0 100 1 07/29/2022 22:03 WG1902102
Total VPH VPH 73.9 J 66.7 150 300 1 07/29/2022 22:03 WG1902102
(S) 2,5-Dibromotoluene(FID)615-59-8 96.9 70.0-130 07/29/2022 22:03 WG1902102
(S) 2,5-Dibromotoluene(PID)615-59-8 97.9 70.0-130 07/29/2022 22:03 WG1902102
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acetone 67-64-1 15.1 J J3 11.3 25.0 50.0 1 07/25/2022 18:30 WG1900597
Acrolein 107-02-8 25.0 C4 U 2.54 25.0 50.0 1 07/25/2022 18:30 WG1900597
Acrylonitrile 107-13-1 5.00 J4 U 0.671 5.00 10.0 1 07/25/2022 18:30 WG1900597
Benzene 71-43-2 0.500 U 0.0941 0.500 1.00 1 07/25/2022 18:30 WG1900597
Bromobenzene 108-86-1 0.500 U 0.118 0.500 1.00 1 07/25/2022 18:30 WG1900597
Bromodichloromethane 75-27-4 0.500 U 0.136 0.500 1.00 1 07/25/2022 18:30 WG1900597
Bromoform 75-25-2 0.500 U 0.129 0.500 1.00 1 07/25/2022 18:30 WG1900597
Bromomethane 74-83-9 2.00 U 0.605 2.00 5.00 1 07/25/2022 18:30 WG1900597
n-Butylbenzene 104-51-8 0.500 U 0.157 0.500 1.00 1 07/25/2022 18:30 WG1900597
sec-Butylbenzene 135-98-8 0.141 J 0.125 0.500 1.00 1 07/25/2022 18:30 WG1900597
tert-Butylbenzene 98-06-6 0.500 U 0.127 0.500 1.00 1 07/25/2022 18:30 WG1900597
Carbon tetrachloride 56-23-5 0.500 U 0.128 0.500 1.00 1 07/25/2022 18:30 WG1900597
Chlorobenzene 108-90-7 0.500 U 0.116 0.500 1.00 1 07/25/2022 18:30 WG1900597
Chlorodibromomethane 124-48-1 0.500 U 0.140 0.500 1.00 1 07/25/2022 18:30 WG1900597
Chloroethane 75-00-3 2.00 U 0.192 2.00 5.00 1 07/25/2022 18:30 WG1900597
Chloroform 67-66-3 2.00 U 0.111 2.00 5.00 1 07/25/2022 18:30 WG1900597
Chloromethane 74-87-3 2.00 U 0.960 2.00 4.00 1 07/25/2022 18:30 WG1900597
2-Chlorotoluene 95-49-8 0.500 U 0.106 0.500 1.00 1 07/25/2022 18:30 WG1900597
4-Chlorotoluene 106-43-4 0.500 U 0.114 0.500 1.00 1 07/25/2022 18:30 WG1900597
1,2-Dibromo-3-Chloropropane 96-12-8 2.00 U 0.276 2.00 5.00 1 07/25/2022 18:30 WG1900597
1,2-Dibromoethane 106-93-4 0.500 U 0.126 0.500 1.00 1 07/25/2022 18:30 WG1900597
Dibromomethane 74-95-3 0.500 U 0.122 0.500 1.00 1 07/25/2022 18:30 WG1900597
1,2-Dichlorobenzene 95-50-1 0.500 U 0.107 0.500 1.00 1 07/25/2022 18:30 WG1900597
1,3-Dichlorobenzene 541-73-1 0.500 U 0.110 0.500 1.00 1 07/25/2022 18:30 WG1900597
1,4-Dichlorobenzene 106-46-7 0.500 U 0.120 0.500 1.00 1 07/25/2022 18:30 WG1900597
Dichlorodifluoromethane 75-71-8 2.00 U 0.374 2.00 5.00 1 07/25/2022 18:30 WG1900597
1,1-Dichloroethane 75-34-3 0.500 U 0.100 0.500 1.00 1 07/25/2022 18:30 WG1900597
1,2-Dichloroethane 107-06-2 0.500 U 0.0819 0.500 1.00 1 07/25/2022 18:30 WG1900597
1,1-Dichloroethene 75-35-4 0.500 U 0.188 0.500 1.00 1 07/25/2022 18:30 WG1900597
cis-1,2-Dichloroethene 156-59-2 0.500 U 0.126 0.500 1.00 1 07/25/2022 18:30 WG1900597
trans-1,2-Dichloroethene 156-60-5 0.500 U 0.149 0.500 1.00 1 07/25/2022 18:30 WG1900597
1,2-Dichloropropane 78-87-5 0.500 U 0.149 0.500 1.00 1 07/25/2022 18:30 WG1900597
1,1-Dichloropropene 563-58-6 0.500 U 0.142 0.500 1.00 1 07/25/2022 18:30 WG1900597
1,3-Dichloropropane 142-28-9 0.500 U 0.110 0.500 1.00 1 07/25/2022 18:30 WG1900597
2,2-Dichloropropane 594-20-7 0.500 U 0.161 0.500 1.00 1 07/25/2022 18:30 WG1900597
Di-isopropyl ether 108-20-3 0.500 U 0.105 0.500 1.00 1 07/25/2022 18:30 WG1900597
Ethylbenzene 100-41-4 0.500 U 0.137 0.500 1.00 1 07/25/2022 18:30 WG1900597
Hexachloro-1,3-butadiene 87-68-3 0.750 J3 U 0.337 0.750 1.50 1 07/25/2022 18:30 WG1900597
Isopropylbenzene 98-82-8 0.165 J 0.105 0.500 1.00 1 07/25/2022 18:30 WG1900597
p-Isopropyltoluene 99-87-6 0.500 U 0.120 0.500 1.00 1 07/25/2022 18:30 WG1900597
2-Butanone (MEK)78-93-3 5.00 U 1.19 5.00 10.0 1 07/25/2022 18:30 WG1900597
Methylene Chloride 75-09-2 2.00 U 0.430 2.00 5.00 1 07/25/2022 18:30 WG1900597
4-Methyl-2-pentanone (MIBK)108-10-1 5.00 U 0.478 5.00 10.0 1 07/25/2022 18:30 WG1900597
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 17 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 17 of 84
--------------=---□
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==============~~~~~=----□ □ □ □
SAMPLE RESULTS - 04
L1517739
USTG480-MW17
Collected date/time: 07/20/22 11:00
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Methyl tert-butyl ether 1634-04-4 0.500 U 0.101 0.500 1.00 1 07/25/2022 18:30 WG1900597
Naphthalene 91-20-3 2.87 J 1.00 2.00 5.00 1 07/25/2022 18:30 WG1900597
n-Propylbenzene 103-65-1 0.146 J 0.0993 0.500 1.00 1 07/25/2022 18:30 WG1900597
Styrene 100-42-5 0.500 U 0.118 0.500 1.00 1 07/25/2022 18:30 WG1900597
1,1,1,2-Tetrachloroethane 630-20-6 0.500 U 0.147 0.500 1.00 1 07/25/2022 18:30 WG1900597
1,1,2,2-Tetrachloroethane 79-34-5 0.500 U 0.133 0.500 1.00 1 07/25/2022 18:30 WG1900597
Tetrachloroethene 127-18-4 0.600 U 0.300 0.600 1.20 1 07/25/2022 18:30 WG1900597
Toluene 108-88-3 0.600 U 0.278 0.600 1.20 1 07/25/2022 18:30 WG1900597
1,2,3-Trichlorobenzene 87-61-6 0.500 U 0.230 0.500 1.00 1 07/25/2022 18:30 WG1900597
1,2,4-Trichlorobenzene 120-82-1 1.00 U 0.481 1.00 2.00 1 07/25/2022 18:30 WG1900597
1,1,1-Trichloroethane 71-55-6 0.500 U 0.149 0.500 1.00 1 07/25/2022 18:30 WG1900597
1,1,2-Trichloroethane 79-00-5 0.500 U 0.158 0.500 1.00 1 07/25/2022 18:30 WG1900597
Trichloroethene 79-01-6 0.500 U 0.190 0.500 1.00 1 07/25/2022 18:30 WG1900597
Trichlorofluoromethane 75-69-4 2.00 U 0.160 2.00 5.00 1 07/25/2022 18:30 WG1900597
1,2,3-Trichloropropane 96-18-4 1.00 U 0.237 1.00 2.50 1 07/25/2022 18:30 WG1900597
1,2,4-Trimethylbenzene 95-63-6 1.00 U 0.322 1.00 2.00 1 07/25/2022 18:30 WG1900597
1,3,5-Trimethylbenzene 108-67-8 0.500 U 0.104 0.500 1.00 1 07/25/2022 18:30 WG1900597
Vinyl chloride 75-01-4 0.500 U 0.234 0.500 1.00 1 07/25/2022 18:30 WG1900597
o-Xylene 95-47-6 0.500 U 0.174 0.500 1.00 1 07/25/2022 18:30 WG1900597
m&p-Xylenes 1330-20-7 1.00 U 0.430 1.00 2.00 1 07/25/2022 18:30 WG1900597
(S) Toluene-d8 2037-26-5 100 89.0-112 07/25/2022 18:30 WG1900597
(S) 4-Bromofluorobenzene 460-00-4 94.2 85.0-114 07/25/2022 18:30 WG1900597
(S) 1,2-Dichloroethane-d4 17060-07-0 103 81.0-118 07/25/2022 18:30 WG1900597
TPH by Method MADEPE
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics C9-C18 ALI
UNADJ 145 33.3 67.0 134 1 08/01/2022 23:34 WG1902750
Unadjusted C19-C36 Aliphatics C19-C36 ALI
UNADJ 54.6 B J 33.3 67.0 134 1 08/01/2022 23:34 WG1902750
Unadjusted C11-C22 Aromatics C11-C22 ARO
UNADJ 142 B 33.3 67.0 134 1 08/02/2022 13:15 WG1902750
Unadjusted Total Petroleum
Hydrocarbons TPH UNADJ 342 B 33.3 67.0 134 1 08/02/2022 13:15 WG1902750
(S) o-Terphenyl 84-15-1 66.0 40.0-140 08/02/2022 13:15 WG1902750
(S) 1-Chloro-octadecane 3386-33-2 45.2 40.0-140 08/01/2022 23:34 WG1902750
(S) 2-Fluorobiphenyl 321-60-8 90.7 40.0-140 08/02/2022 13:15 WG1902750
(S) 2-Bromonaphthalene 580-13-2 87.6 40.0-140 08/02/2022 13:15 WG1902750
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acenaphthene 83-32-9 0.500 U 0.0886 0.500 1.00 1 07/27/2022 21:28 WG1900474
Acenaphthylene 208-96-8 0.500 U 0.0921 0.500 1.00 1 07/27/2022 21:28 WG1900474
Anthracene 120-12-7 0.500 J4 U 0.0804 0.500 1.00 1 07/27/2022 21:28 WG1900474
Benzidine 92-87-5 7.50 J4 U 3.74 7.50 15.0 1 07/27/2022 21:28 WG1900474
Benzo(a)anthracene 56-55-3 0.500 U 0.199 0.500 1.00 1 07/27/2022 21:28 WG1900474
Benzo(b)fluoranthene 205-99-2 0.500 U 0.130 0.500 1.00 1 07/27/2022 21:28 WG1900474
Benzo(k)fluoranthene 207-08-9 0.500 U 0.120 0.500 1.00 1 07/27/2022 21:28 WG1900474
Benzo(g,h,i)perylene 191-24-2 0.500 U 0.121 0.500 1.00 1 07/27/2022 21:28 WG1900474
Benzo(a)pyrene 50-32-8 0.500 U 0.0381 0.500 1.00 1 07/27/2022 21:28 WG1900474
Bis(2-chlorethoxy)methane 111-91-1 5.00 J4 U 0.116 5.00 10.0 1 07/27/2022 21:28 WG1900474
Bis(2-chloroethyl)ether 111-44-4 5.00 J4 U 0.137 5.00 10.0 1 07/27/2022 21:28 WG1900474
2,2-Oxybis(1-Chloropropane)108-60-1 5.00 J4 U 0.210 5.00 10.0 1 07/27/2022 21:28 WG1900474
4-Bromophenyl-phenylether 101-55-3 5.00 U 0.0877 5.00 10.0 1 07/27/2022 21:28 WG1900474
2-Chloronaphthalene 91-58-7 0.500 U 0.0648 0.500 1.00 1 07/27/2022 21:28 WG1900474
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 18 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 18 of 84
====================----□ □ □ □
□ □ □ □
SAMPLE RESULTS - 04
L1517739
USTG480-MW17
Collected date/time: 07/20/22 11:00
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
4-Chlorophenyl-phenylether 7005-72-3 5.00 U 0.0926 5.00 10.0 1 07/27/2022 21:28 WG1900474
Chrysene 218-01-9 0.500 U 0.130 0.500 1.00 1 07/27/2022 21:28 WG1900474
Dibenz(a,h)anthracene 53-70-3 0.500 U 0.0644 0.500 1.00 1 07/27/2022 21:28 WG1900474
3,3-Dichlorobenzidine 91-94-1 5.00 U 0.212 5.00 10.0 1 07/27/2022 21:28 WG1900474
2,4-Dinitrotoluene 121-14-2 5.00 U 0.0983 5.00 10.0 1 07/27/2022 21:28 WG1900474
2,6-Dinitrotoluene 606-20-2 5.00 J4 U 0.250 5.00 10.0 1 07/27/2022 21:28 WG1900474
Fluoranthene 206-44-0 0.500 J4 U 0.102 0.500 1.00 1 07/27/2022 21:28 WG1900474
Fluorene 86-73-7 0.500 U 0.0844 0.500 1.00 1 07/27/2022 21:28 WG1900474
Hexachlorobenzene 118-74-1 0.500 U 0.0755 0.500 1.00 1 07/27/2022 21:28 WG1900474
Hexachloro-1,3-butadiene 87-68-3 5.00 U 0.0968 5.00 10.0 1 07/27/2022 21:28 WG1900474
Hexachlorocyclopentadiene 77-47-4 5.00 U 0.0598 5.00 10.0 1 07/27/2022 21:28 WG1900474
Hexachloroethane 67-72-1 5.00 U 0.127 5.00 10.0 1 07/27/2022 21:28 WG1900474
Indeno(1,2,3-cd)pyrene 193-39-5 0.600 U 0.279 0.600 1.20 1 07/27/2022 21:28 WG1900474
Isophorone 78-59-1 5.00 U 0.143 5.00 10.0 1 07/27/2022 21:28 WG1900474
Naphthalene 91-20-3 0.262 J J4 0.159 0.500 1.00 1 07/27/2022 21:28 WG1900474
Nitrobenzene 98-95-3 5.00 J4 U 0.297 5.00 10.0 1 07/27/2022 21:28 WG1900474
n-Nitrosodimethylamine 62-75-9 5.00 U 0.998 5.00 10.0 1 07/27/2022 21:28 WG1900474
n-Nitrosodiphenylamine 86-30-6 5.00 U 2.37 5.00 10.0 1 07/27/2022 21:28 WG1900474
n-Nitrosodi-n-propylamine 621-64-7 5.00 J4 U 0.261 5.00 10.0 1 07/27/2022 21:28 WG1900474
Phenanthrene 85-01-8 0.500 J4 U 0.112 0.500 1.00 1 07/27/2022 21:28 WG1900474
Benzylbutyl phthalate 85-68-7 2.00 U 0.765 2.00 4.00 1 07/27/2022 21:28 WG1900474
Bis(2-ethylhexyl)phthalate 117-81-7 2.00 J4 U 0.895 2.00 4.00 1 07/27/2022 21:28 WG1900474
Di-n-butyl phthalate 84-74-2 1.50 J4 U 0.453 1.50 3.00 1 07/27/2022 21:28 WG1900474
Diethyl phthalate 84-66-2 1.50 J4 U 0.287 1.50 3.00 1 07/27/2022 21:28 WG1900474
Dimethyl phthalate 131-11-3 1.50 U 0.260 1.50 3.00 1 07/27/2022 21:28 WG1900474
Di-n-octyl phthalate 117-84-0 2.00 U 0.932 2.00 4.00 1 07/27/2022 21:28 WG1900474
Pyrene 129-00-0 0.500 J4 U 0.107 0.500 1.00 1 07/27/2022 21:28 WG1900474
1,2,4-Trichlorobenzene 120-82-1 5.00 U 0.0698 5.00 10.0 1 07/27/2022 21:28 WG1900474
4-Chloro-3-methylphenol 59-50-7 5.00 J4 U 0.131 5.00 10.0 1 07/27/2022 21:28 WG1900474
2-Chlorophenol 95-57-8 5.00 J4 U 0.133 5.00 10.0 1 07/27/2022 21:28 WG1900474
2,4-Dichlorophenol 120-83-2 5.00 J4 U 0.102 5.00 10.0 1 07/27/2022 21:28 WG1900474
2,4-Dimethylphenol 105-67-9 5.00 U 0.0636 5.00 10.0 1 07/27/2022 21:28 WG1900474
4,6-Dinitro-2-methylphenol 534-52-1 5.00 U 1.12 5.00 10.0 1 07/27/2022 21:28 WG1900474
2,4-Dinitrophenol 51-28-5 15.0 U 5.93 15.0 30.0 1 07/27/2022 21:28 WG1900474
2-Nitrophenol 88-75-5 5.00 J4 U 0.117 5.00 10.0 1 07/27/2022 21:28 WG1900474
4-Nitrophenol 100-02-7 5.00 U 0.143 5.00 10.0 1 07/27/2022 21:28 WG1900474
Pentachlorophenol 87-86-5 5.00 U 0.313 5.00 10.0 1 07/27/2022 21:28 WG1900474
Phenol 108-95-2 10.0 U 4.33 10.0 20.0 1 07/27/2022 21:28 WG1900474
2,4,6-Trichlorophenol 88-06-2 5.00 U 0.100 5.00 10.0 1 07/27/2022 21:28 WG1900474
(S) Nitrobenzene-d5 4165-60-0 56.0 0.000 44.0-120 07/27/2022 21:28 WG1900474
(S) 2-Fluorobiphenyl 321-60-8 57.3 0.000 44.0-119 07/27/2022 21:28 WG1900474
(S) p-Terphenyl-d14 1718-51-0 52.2 0.000 50.0-134 07/27/2022 21:28 WG1900474
(S) Phenol-d5 4165-62-2 14.3 0.000 10.0-67.0 07/27/2022 21:28 WG1900474
(S) 2-Fluorophenol 367-12-4 21.1 0.000 19.0-119 07/27/2022 21:28 WG1900474
(S) 2,4,6-Tribromophenol 118-79-6 67.6 0.000 43.0-140 07/27/2022 21:28 WG1900474
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 19 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 19 of 84
====================----□ □ □ □
□ □ □ □
SAMPLE RESULTS - 05
L1517739
USTG480-MW13
Collected date/time: 07/20/22 11:30
Volatile Petroleum Hydrocarbons by Method MADEPV
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics C5-C8 ALI
UNADJ 670 U 333 670 1000 10 07/30/2022 05:42 WG1902102
Unadjusted C9-C12 Aliphatics C9-C12 ALI
UNADJ 755 B J 333 670 1340 10 07/30/2022 05:42 WG1902102
Unadjusted C9-C10 Aromatics C9-C10 ARO
UNADJ 835 J 333 670 1000 10 07/30/2022 05:42 WG1902102
Total VPH VPH 1590 J 667 1500 3000 10 07/30/2022 05:42 WG1902102
(S) 2,5-Dibromotoluene(FID)615-59-8 107 70.0-130 07/30/2022 05:42 WG1902102
(S) 2,5-Dibromotoluene(PID)615-59-8 100 70.0-130 07/30/2022 05:42 WG1902102
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acetone 67-64-1 132 J J3 113 250 500 10 07/25/2022 22:22 WG1900597
Acrolein 107-02-8 250 C4 U 25.4 250 500 10 07/25/2022 22:22 WG1900597
Acrylonitrile 107-13-1 50.0 J4 U 6.71 50.0 100 10 07/25/2022 22:22 WG1900597
Benzene 71-43-2 7.38 J 0.941 5.00 10.0 10 07/25/2022 22:22 WG1900597
Bromobenzene 108-86-1 5.00 U 1.18 5.00 10.0 10 07/25/2022 22:22 WG1900597
Bromodichloromethane 75-27-4 5.00 U 1.36 5.00 10.0 10 07/25/2022 22:22 WG1900597
Bromoform 75-25-2 5.00 U 1.29 5.00 10.0 10 07/25/2022 22:22 WG1900597
Bromomethane 74-83-9 20.0 U 6.05 20.0 50.0 10 07/25/2022 22:22 WG1900597
n-Butylbenzene 104-51-8 4.05 J 1.57 5.00 10.0 10 07/25/2022 22:22 WG1900597
sec-Butylbenzene 135-98-8 4.21 J 1.25 5.00 10.0 10 07/25/2022 22:22 WG1900597
tert-Butylbenzene 98-06-6 1.70 J 1.27 5.00 10.0 10 07/25/2022 22:22 WG1900597
Carbon tetrachloride 56-23-5 5.00 U 1.28 5.00 10.0 10 07/25/2022 22:22 WG1900597
Chlorobenzene 108-90-7 5.00 U 1.16 5.00 10.0 10 07/25/2022 22:22 WG1900597
Chlorodibromomethane 124-48-1 5.00 U 1.40 5.00 10.0 10 07/25/2022 22:22 WG1900597
Chloroethane 75-00-3 20.0 U 1.92 20.0 50.0 10 07/25/2022 22:22 WG1900597
Chloroform 67-66-3 20.0 U 1.11 20.0 50.0 10 07/25/2022 22:22 WG1900597
Chloromethane 74-87-3 20.0 U 9.60 20.0 40.0 10 07/25/2022 22:22 WG1900597
2-Chlorotoluene 95-49-8 5.00 U 1.06 5.00 10.0 10 07/25/2022 22:22 WG1900597
4-Chlorotoluene 106-43-4 5.00 U 1.14 5.00 10.0 10 07/25/2022 22:22 WG1900597
1,2-Dibromo-3-Chloropropane 96-12-8 20.0 U 2.76 20.0 50.0 10 07/25/2022 22:22 WG1900597
1,2-Dibromoethane 106-93-4 5.00 U 1.26 5.00 10.0 10 07/25/2022 22:22 WG1900597
Dibromomethane 74-95-3 5.00 U 1.22 5.00 10.0 10 07/25/2022 22:22 WG1900597
1,2-Dichlorobenzene 95-50-1 5.00 U 1.07 5.00 10.0 10 07/25/2022 22:22 WG1900597
1,3-Dichlorobenzene 541-73-1 5.00 U 1.10 5.00 10.0 10 07/25/2022 22:22 WG1900597
1,4-Dichlorobenzene 106-46-7 5.00 U 1.20 5.00 10.0 10 07/25/2022 22:22 WG1900597
Dichlorodifluoromethane 75-71-8 20.0 U 3.74 20.0 50.0 10 07/25/2022 22:22 WG1900597
1,1-Dichloroethane 75-34-3 5.00 U 1.00 5.00 10.0 10 07/25/2022 22:22 WG1900597
1,2-Dichloroethane 107-06-2 5.00 U 0.819 5.00 10.0 10 07/25/2022 22:22 WG1900597
1,1-Dichloroethene 75-35-4 5.00 U 1.88 5.00 10.0 10 07/25/2022 22:22 WG1900597
cis-1,2-Dichloroethene 156-59-2 5.00 U 1.26 5.00 10.0 10 07/25/2022 22:22 WG1900597
trans-1,2-Dichloroethene 156-60-5 5.00 U 1.49 5.00 10.0 10 07/25/2022 22:22 WG1900597
1,2-Dichloropropane 78-87-5 5.00 U 1.49 5.00 10.0 10 07/25/2022 22:22 WG1900597
1,1-Dichloropropene 563-58-6 5.00 U 1.42 5.00 10.0 10 07/25/2022 22:22 WG1900597
1,3-Dichloropropane 142-28-9 5.00 U 1.10 5.00 10.0 10 07/25/2022 22:22 WG1900597
2,2-Dichloropropane 594-20-7 5.00 U 1.61 5.00 10.0 10 07/25/2022 22:22 WG1900597
Di-isopropyl ether 108-20-3 5.00 U 1.05 5.00 10.0 10 07/25/2022 22:22 WG1900597
Ethylbenzene 100-41-4 20.1 1.37 5.00 10.0 10 07/25/2022 22:22 WG1900597
Hexachloro-1,3-butadiene 87-68-3 7.50 J3 U 3.37 7.50 15.0 10 07/25/2022 22:22 WG1900597
Isopropylbenzene 98-82-8 7.17 J 1.05 5.00 10.0 10 07/25/2022 22:22 WG1900597
p-Isopropyltoluene 99-87-6 4.70 J 1.20 5.00 10.0 10 07/25/2022 22:22 WG1900597
2-Butanone (MEK)78-93-3 50.0 U 11.9 50.0 100 10 07/25/2022 22:22 WG1900597
Methylene Chloride 75-09-2 20.0 U 4.30 20.0 50.0 10 07/25/2022 22:22 WG1900597
4-Methyl-2-pentanone (MIBK)108-10-1 50.0 U 4.78 50.0 100 10 07/25/2022 22:22 WG1900597
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 20 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 20 of 84
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□ □ □
==============~~~~~=----□ □ □ □
SAMPLE RESULTS - 05
L1517739
USTG480-MW13
Collected date/time: 07/20/22 11:30
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Methyl tert-butyl ether 1634-04-4 5.00 U 1.01 5.00 10.0 10 07/25/2022 22:22 WG1900597
Naphthalene 91-20-3 227 10.0 20.0 50.0 10 07/25/2022 22:22 WG1900597
n-Propylbenzene 103-65-1 11.1 0.993 5.00 10.0 10 07/25/2022 22:22 WG1900597
Styrene 100-42-5 5.00 U 1.18 5.00 10.0 10 07/25/2022 22:22 WG1900597
1,1,1,2-Tetrachloroethane 630-20-6 5.00 U 1.47 5.00 10.0 10 07/25/2022 22:22 WG1900597
1,1,2,2-Tetrachloroethane 79-34-5 5.00 U 1.33 5.00 10.0 10 07/25/2022 22:22 WG1900597
Tetrachloroethene 127-18-4 6.00 U 3.00 6.00 12.0 10 07/25/2022 22:22 WG1900597
Toluene 108-88-3 6.00 U 2.78 6.00 12.0 10 07/25/2022 22:22 WG1900597
1,2,3-Trichlorobenzene 87-61-6 5.00 U 2.30 5.00 10.0 10 07/25/2022 22:22 WG1900597
1,2,4-Trichlorobenzene 120-82-1 10.0 U 4.81 10.0 20.0 10 07/25/2022 22:22 WG1900597
1,1,1-Trichloroethane 71-55-6 5.00 U 1.49 5.00 10.0 10 07/25/2022 22:22 WG1900597
1,1,2-Trichloroethane 79-00-5 5.00 U 1.58 5.00 10.0 10 07/25/2022 22:22 WG1900597
Trichloroethene 79-01-6 5.00 U 1.90 5.00 10.0 10 07/25/2022 22:22 WG1900597
Trichlorofluoromethane 75-69-4 20.0 U 1.60 20.0 50.0 10 07/25/2022 22:22 WG1900597
1,2,3-Trichloropropane 96-18-4 10.0 U 2.37 10.0 25.0 10 07/25/2022 22:22 WG1900597
1,2,4-Trimethylbenzene 95-63-6 69.0 3.22 10.0 20.0 10 07/25/2022 22:22 WG1900597
1,3,5-Trimethylbenzene 108-67-8 31.1 1.04 5.00 10.0 10 07/25/2022 22:22 WG1900597
Vinyl chloride 75-01-4 5.00 U 2.34 5.00 10.0 10 07/25/2022 22:22 WG1900597
o-Xylene 95-47-6 5.94 J 1.74 5.00 10.0 10 07/25/2022 22:22 WG1900597
m&p-Xylenes 1330-20-7 25.7 4.30 10.0 20.0 10 07/25/2022 22:22 WG1900597
(S) Toluene-d8 2037-26-5 95.7 89.0-112 07/25/2022 22:22 WG1900597
(S) 4-Bromofluorobenzene 460-00-4 100 85.0-114 07/25/2022 22:22 WG1900597
(S) 1,2-Dichloroethane-d4 17060-07-0 100 81.0-118 07/25/2022 22:22 WG1900597
TPH by Method MADEPE
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics C9-C18 ALI
UNADJ 1910 33.3 67.0 134 1 08/01/2022 23:56 WG1902750
Unadjusted C19-C36 Aliphatics C19-C36 ALI
UNADJ 397 B 33.3 67.0 134 1 08/01/2022 23:56 WG1902750
Unadjusted C11-C22 Aromatics C11-C22 ARO
UNADJ 2050 33.3 67.0 134 1 08/02/2022 04:00 WG1902750
Unadjusted Total Petroleum
Hydrocarbons TPH UNADJ 4360 33.3 67.0 134 1 08/02/2022 04:00 WG1902750
(S) o-Terphenyl 84-15-1 58.9 40.0-140 08/02/2022 04:00 WG1902750
(S) 1-Chloro-octadecane 3386-33-2 39.8 J2 40.0-140 08/01/2022 23:56 WG1902750
(S) 2-Fluorobiphenyl 321-60-8 85.1 40.0-140 08/02/2022 04:00 WG1902750
(S) 2-Bromonaphthalene 580-13-2 78.8 40.0-140 08/02/2022 04:00 WG1902750
Sample Narrative:
L1517739-05 WG1902750: Sample produced total emulsion during Extraction process, low surr/spike recoveries due to matrix.
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acenaphthene 83-32-9 1.67 0.0886 0.500 1.00 1 08/01/2022 19:25 WG1900474
Acenaphthylene 208-96-8 0.500 U 0.0921 0.500 1.00 1 08/01/2022 19:25 WG1900474
Anthracene 120-12-7 0.519 J J4 0.0804 0.500 1.00 1 08/01/2022 19:25 WG1900474
Benzidine 92-87-5 7.50 J4 U 3.74 7.50 15.0 1 08/01/2022 19:25 WG1900474
Benzo(a)anthracene 56-55-3 0.500 U 0.199 0.500 1.00 1 08/01/2022 19:25 WG1900474
Benzo(b)fluoranthene 205-99-2 0.500 U 0.130 0.500 1.00 1 08/01/2022 19:25 WG1900474
Benzo(k)fluoranthene 207-08-9 0.500 U 0.120 0.500 1.00 1 08/01/2022 19:25 WG1900474
Benzo(g,h,i)perylene 191-24-2 0.500 U 0.121 0.500 1.00 1 08/01/2022 19:25 WG1900474
Benzo(a)pyrene 50-32-8 0.500 U 0.0381 0.500 1.00 1 08/01/2022 19:25 WG1900474
Bis(2-chlorethoxy)methane 111-91-1 5.00 J4 U 0.116 5.00 10.0 1 08/01/2022 19:25 WG1900474
Bis(2-chloroethyl)ether 111-44-4 5.00 J4 U 0.137 5.00 10.0 1 08/01/2022 19:25 WG1900474
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 21 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 21 of 84
====================----□ □ □ □
□ □ □ □
SAMPLE RESULTS - 05
L1517739
USTG480-MW13
Collected date/time: 07/20/22 11:30
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
2,2-Oxybis(1-Chloropropane)108-60-1 5.00 J4 U 0.210 5.00 10.0 1 08/01/2022 19:25 WG1900474
4-Bromophenyl-phenylether 101-55-3 5.00 U 0.0877 5.00 10.0 1 08/01/2022 19:25 WG1900474
2-Chloronaphthalene 91-58-7 0.500 U 0.0648 0.500 1.00 1 08/01/2022 19:25 WG1900474
4-Chlorophenyl-phenylether 7005-72-3 5.00 U 0.0926 5.00 10.0 1 08/01/2022 19:25 WG1900474
Chrysene 218-01-9 0.500 U 0.130 0.500 1.00 1 08/01/2022 19:25 WG1900474
Dibenz(a,h)anthracene 53-70-3 0.500 U 0.0644 0.500 1.00 1 08/01/2022 19:25 WG1900474
3,3-Dichlorobenzidine 91-94-1 5.00 U 0.212 5.00 10.0 1 08/01/2022 19:25 WG1900474
2,4-Dinitrotoluene 121-14-2 5.00 U 0.0983 5.00 10.0 1 08/01/2022 19:25 WG1900474
2,6-Dinitrotoluene 606-20-2 5.00 J4 U 0.250 5.00 10.0 1 08/01/2022 19:25 WG1900474
Fluoranthene 206-44-0 0.500 J4 U 0.102 0.500 1.00 1 08/01/2022 19:25 WG1900474
Fluorene 86-73-7 3.30 0.0844 0.500 1.00 1 08/01/2022 19:25 WG1900474
Hexachlorobenzene 118-74-1 0.500 U 0.0755 0.500 1.00 1 08/01/2022 19:25 WG1900474
Hexachloro-1,3-butadiene 87-68-3 5.00 U 0.0968 5.00 10.0 1 08/01/2022 19:25 WG1900474
Hexachlorocyclopentadiene 77-47-4 5.00 C6 U 0.0598 5.00 10.0 1 08/01/2022 19:25 WG1900474
Hexachloroethane 67-72-1 5.00 U 0.127 5.00 10.0 1 08/01/2022 19:25 WG1900474
Indeno(1,2,3-cd)pyrene 193-39-5 0.600 U 0.279 0.600 1.20 1 08/01/2022 19:25 WG1900474
Isophorone 78-59-1 5.00 U 0.143 5.00 10.0 1 08/01/2022 19:25 WG1900474
Naphthalene 91-20-3 34.4 J4 0.159 0.500 1.00 1 08/01/2022 19:25 WG1900474
Nitrobenzene 98-95-3 5.00 J4 U 0.297 5.00 10.0 1 08/01/2022 19:25 WG1900474
n-Nitrosodimethylamine 62-75-9 5.00 U 0.998 5.00 10.0 1 08/01/2022 19:25 WG1900474
n-Nitrosodiphenylamine 86-30-6 5.00 U 2.37 5.00 10.0 1 08/01/2022 19:25 WG1900474
n-Nitrosodi-n-propylamine 621-64-7 5.00 J4 U 0.261 5.00 10.0 1 08/01/2022 19:25 WG1900474
Phenanthrene 85-01-8 4.83 J4 0.112 0.500 1.00 1 08/01/2022 19:25 WG1900474
Benzylbutyl phthalate 85-68-7 2.00 U 0.765 2.00 4.00 1 08/01/2022 19:25 WG1900474
Bis(2-ethylhexyl)phthalate 117-81-7 2.00 J4 U 0.895 2.00 4.00 1 08/01/2022 19:25 WG1900474
Di-n-butyl phthalate 84-74-2 1.50 J4 U 0.453 1.50 3.00 1 08/01/2022 19:25 WG1900474
Diethyl phthalate 84-66-2 1.50 J4 U 0.287 1.50 3.00 1 08/01/2022 19:25 WG1900474
Dimethyl phthalate 131-11-3 1.50 U 0.260 1.50 3.00 1 08/01/2022 19:25 WG1900474
Di-n-octyl phthalate 117-84-0 2.00 U 0.932 2.00 4.00 1 08/01/2022 19:25 WG1900474
Pyrene 129-00-0 0.187 J J4 0.107 0.500 1.00 1 08/01/2022 19:25 WG1900474
1,2,4-Trichlorobenzene 120-82-1 5.00 U 0.0698 5.00 10.0 1 08/01/2022 19:25 WG1900474
4-Chloro-3-methylphenol 59-50-7 5.00 J4 U 0.131 5.00 10.0 1 08/01/2022 19:25 WG1900474
2-Chlorophenol 95-57-8 5.00 J4 U 0.133 5.00 10.0 1 08/01/2022 19:25 WG1900474
2,4-Dichlorophenol 120-83-2 5.00 J4 U 0.102 5.00 10.0 1 08/01/2022 19:25 WG1900474
2,4-Dimethylphenol 105-67-9 5.00 U 0.0636 5.00 10.0 1 08/01/2022 19:25 WG1900474
4,6-Dinitro-2-methylphenol 534-52-1 5.00 U 1.12 5.00 10.0 1 08/01/2022 19:25 WG1900474
2,4-Dinitrophenol 51-28-5 15.0 U 5.93 15.0 30.0 1 08/01/2022 19:25 WG1900474
2-Nitrophenol 88-75-5 5.00 J4 U 0.117 5.00 10.0 1 08/01/2022 19:25 WG1900474
4-Nitrophenol 100-02-7 5.00 U 0.143 5.00 10.0 1 08/01/2022 19:25 WG1900474
Pentachlorophenol 87-86-5 5.00 U 0.313 5.00 10.0 1 08/01/2022 19:25 WG1900474
Phenol 108-95-2 5.37 J 4.33 10.0 20.0 1 08/01/2022 19:25 WG1900474
2,4,6-Trichlorophenol 88-06-2 5.00 U 0.100 5.00 10.0 1 08/01/2022 19:25 WG1900474
1-Methylnaphthalene 90-12-0 51.8 0.0790 0.500 1.00 1 08/01/2022 19:25 WG1900474
2-Methylnaphthalene 91-57-6 55.2 0.117 0.500 1.00 1 08/01/2022 19:25 WG1900474
(S) Nitrobenzene-d5 4165-60-0 23.2 J2 0.000 44.0-120 08/01/2022 19:25 WG1900474
(S) 2-Fluorobiphenyl 321-60-8 24.6 J2 0.000 44.0-119 08/01/2022 19:25 WG1900474
(S) p-Terphenyl-d14 1718-51-0 28.8 J2 0.000 50.0-134 08/01/2022 19:25 WG1900474
(S) Phenol-d5 4165-62-2 9.70 J2 0.000 10.0-67.0 08/01/2022 19:25 WG1900474
(S) 2-Fluorophenol 367-12-4 10.7 J2 0.000 19.0-119 08/01/2022 19:25 WG1900474
(S) 2,4,6-Tribromophenol 118-79-6 37.3 J2 0.000 43.0-140 08/01/2022 19:25 WG1900474
Sample Narrative:
L1517739-05 WG1900474: Sample produced total emulsion during Extraction process, low surr/spike recoveries due to matrix.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 22 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 22 of 84
====================----□ □ □ □
□ □ □ □
SAMPLE RESULTS - 06
L1517739
USTG480-MW18
Collected date/time: 07/20/22 11:45
Volatile Petroleum Hydrocarbons by Method MADEPV
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics C5-C8 ALI
UNADJ 67.0 U 33.3 67.0 100 1 07/29/2022 22:36 WG1902102
Unadjusted C9-C12 Aliphatics C9-C12 ALI
UNADJ 47.8 B J 33.3 67.0 134 1 07/29/2022 22:36 WG1902102
Unadjusted C9-C10 Aromatics C9-C10 ARO
UNADJ 67.0 U 33.3 67.0 100 1 07/29/2022 22:36 WG1902102
Total VPH VPH 150 U 66.7 150 300 1 07/29/2022 22:36 WG1902102
(S) 2,5-Dibromotoluene(FID)615-59-8 93.3 70.0-130 07/29/2022 22:36 WG1902102
(S) 2,5-Dibromotoluene(PID)615-59-8 96.0 70.0-130 07/29/2022 22:36 WG1902102
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acetone 67-64-1 25.0 J3 U 11.3 25.0 50.0 1 07/25/2022 18:52 WG1900597
Acrolein 107-02-8 25.0 C4 U 2.54 25.0 50.0 1 07/25/2022 18:52 WG1900597
Acrylonitrile 107-13-1 5.00 J4 U 0.671 5.00 10.0 1 07/25/2022 18:52 WG1900597
Benzene 71-43-2 0.500 U 0.0941 0.500 1.00 1 07/25/2022 18:52 WG1900597
Bromobenzene 108-86-1 0.500 U 0.118 0.500 1.00 1 07/25/2022 18:52 WG1900597
Bromodichloromethane 75-27-4 0.500 U 0.136 0.500 1.00 1 07/25/2022 18:52 WG1900597
Bromoform 75-25-2 0.500 U 0.129 0.500 1.00 1 07/25/2022 18:52 WG1900597
Bromomethane 74-83-9 2.00 U 0.605 2.00 5.00 1 07/25/2022 18:52 WG1900597
n-Butylbenzene 104-51-8 0.500 U 0.157 0.500 1.00 1 07/25/2022 18:52 WG1900597
sec-Butylbenzene 135-98-8 0.500 U 0.125 0.500 1.00 1 07/25/2022 18:52 WG1900597
tert-Butylbenzene 98-06-6 0.500 U 0.127 0.500 1.00 1 07/25/2022 18:52 WG1900597
Carbon tetrachloride 56-23-5 0.500 U 0.128 0.500 1.00 1 07/25/2022 18:52 WG1900597
Chlorobenzene 108-90-7 0.500 U 0.116 0.500 1.00 1 07/25/2022 18:52 WG1900597
Chlorodibromomethane 124-48-1 0.500 U 0.140 0.500 1.00 1 07/25/2022 18:52 WG1900597
Chloroethane 75-00-3 2.00 U 0.192 2.00 5.00 1 07/25/2022 18:52 WG1900597
Chloroform 67-66-3 2.00 U 0.111 2.00 5.00 1 07/25/2022 18:52 WG1900597
Chloromethane 74-87-3 2.00 U 0.960 2.00 4.00 1 07/25/2022 18:52 WG1900597
2-Chlorotoluene 95-49-8 0.500 U 0.106 0.500 1.00 1 07/25/2022 18:52 WG1900597
4-Chlorotoluene 106-43-4 0.500 U 0.114 0.500 1.00 1 07/25/2022 18:52 WG1900597
1,2-Dibromo-3-Chloropropane 96-12-8 2.00 U 0.276 2.00 5.00 1 07/25/2022 18:52 WG1900597
1,2-Dibromoethane 106-93-4 0.500 U 0.126 0.500 1.00 1 07/25/2022 18:52 WG1900597
Dibromomethane 74-95-3 0.500 U 0.122 0.500 1.00 1 07/25/2022 18:52 WG1900597
1,2-Dichlorobenzene 95-50-1 0.500 U 0.107 0.500 1.00 1 07/25/2022 18:52 WG1900597
1,3-Dichlorobenzene 541-73-1 0.500 U 0.110 0.500 1.00 1 07/25/2022 18:52 WG1900597
1,4-Dichlorobenzene 106-46-7 0.500 U 0.120 0.500 1.00 1 07/25/2022 18:52 WG1900597
Dichlorodifluoromethane 75-71-8 2.00 U 0.374 2.00 5.00 1 07/25/2022 18:52 WG1900597
1,1-Dichloroethane 75-34-3 0.500 U 0.100 0.500 1.00 1 07/25/2022 18:52 WG1900597
1,2-Dichloroethane 107-06-2 0.500 U 0.0819 0.500 1.00 1 07/25/2022 18:52 WG1900597
1,1-Dichloroethene 75-35-4 0.500 U 0.188 0.500 1.00 1 07/25/2022 18:52 WG1900597
cis-1,2-Dichloroethene 156-59-2 0.500 U 0.126 0.500 1.00 1 07/25/2022 18:52 WG1900597
trans-1,2-Dichloroethene 156-60-5 0.500 U 0.149 0.500 1.00 1 07/25/2022 18:52 WG1900597
1,2-Dichloropropane 78-87-5 0.500 U 0.149 0.500 1.00 1 07/25/2022 18:52 WG1900597
1,1-Dichloropropene 563-58-6 0.500 U 0.142 0.500 1.00 1 07/25/2022 18:52 WG1900597
1,3-Dichloropropane 142-28-9 0.500 U 0.110 0.500 1.00 1 07/25/2022 18:52 WG1900597
2,2-Dichloropropane 594-20-7 0.500 U 0.161 0.500 1.00 1 07/25/2022 18:52 WG1900597
Di-isopropyl ether 108-20-3 0.500 U 0.105 0.500 1.00 1 07/25/2022 18:52 WG1900597
Ethylbenzene 100-41-4 0.500 U 0.137 0.500 1.00 1 07/25/2022 18:52 WG1900597
Hexachloro-1,3-butadiene 87-68-3 0.750 J3 U 0.337 0.750 1.50 1 07/25/2022 18:52 WG1900597
Isopropylbenzene 98-82-8 0.500 U 0.105 0.500 1.00 1 07/25/2022 18:52 WG1900597
p-Isopropyltoluene 99-87-6 0.500 U 0.120 0.500 1.00 1 07/25/2022 18:52 WG1900597
2-Butanone (MEK)78-93-3 5.00 U 1.19 5.00 10.0 1 07/25/2022 18:52 WG1900597
Methylene Chloride 75-09-2 2.00 U 0.430 2.00 5.00 1 07/25/2022 18:52 WG1900597
4-Methyl-2-pentanone (MIBK)108-10-1 5.00 U 0.478 5.00 10.0 1 07/25/2022 18:52 WG1900597
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 23 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 23 of 84
--------------=---□
□ □ □
==============~~~~~=----□ □ □ □
SAMPLE RESULTS - 06
L1517739
USTG480-MW18
Collected date/time: 07/20/22 11:45
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Methyl tert-butyl ether 1634-04-4 0.500 U 0.101 0.500 1.00 1 07/25/2022 18:52 WG1900597
Naphthalene 91-20-3 2.00 U 1.00 2.00 5.00 1 07/25/2022 18:52 WG1900597
n-Propylbenzene 103-65-1 0.500 U 0.0993 0.500 1.00 1 07/25/2022 18:52 WG1900597
Styrene 100-42-5 0.500 U 0.118 0.500 1.00 1 07/25/2022 18:52 WG1900597
1,1,1,2-Tetrachloroethane 630-20-6 0.500 U 0.147 0.500 1.00 1 07/25/2022 18:52 WG1900597
1,1,2,2-Tetrachloroethane 79-34-5 0.500 U 0.133 0.500 1.00 1 07/25/2022 18:52 WG1900597
Tetrachloroethene 127-18-4 0.600 U 0.300 0.600 1.20 1 07/25/2022 18:52 WG1900597
Toluene 108-88-3 0.600 U 0.278 0.600 1.20 1 07/25/2022 18:52 WG1900597
1,2,3-Trichlorobenzene 87-61-6 0.500 U 0.230 0.500 1.00 1 07/25/2022 18:52 WG1900597
1,2,4-Trichlorobenzene 120-82-1 1.00 U 0.481 1.00 2.00 1 07/25/2022 18:52 WG1900597
1,1,1-Trichloroethane 71-55-6 0.500 U 0.149 0.500 1.00 1 07/25/2022 18:52 WG1900597
1,1,2-Trichloroethane 79-00-5 0.500 U 0.158 0.500 1.00 1 07/25/2022 18:52 WG1900597
Trichloroethene 79-01-6 0.500 U 0.190 0.500 1.00 1 07/25/2022 18:52 WG1900597
Trichlorofluoromethane 75-69-4 2.00 U 0.160 2.00 5.00 1 07/25/2022 18:52 WG1900597
1,2,3-Trichloropropane 96-18-4 1.00 U 0.237 1.00 2.50 1 07/25/2022 18:52 WG1900597
1,2,4-Trimethylbenzene 95-63-6 1.00 U 0.322 1.00 2.00 1 07/25/2022 18:52 WG1900597
1,3,5-Trimethylbenzene 108-67-8 0.500 U 0.104 0.500 1.00 1 07/25/2022 18:52 WG1900597
Vinyl chloride 75-01-4 0.500 U 0.234 0.500 1.00 1 07/25/2022 18:52 WG1900597
o-Xylene 95-47-6 0.500 U 0.174 0.500 1.00 1 07/25/2022 18:52 WG1900597
m&p-Xylenes 1330-20-7 1.00 U 0.430 1.00 2.00 1 07/25/2022 18:52 WG1900597
(S) Toluene-d8 2037-26-5 96.8 89.0-112 07/25/2022 18:52 WG1900597
(S) 4-Bromofluorobenzene 460-00-4 101 85.0-114 07/25/2022 18:52 WG1900597
(S) 1,2-Dichloroethane-d4 17060-07-0 104 81.0-118 07/25/2022 18:52 WG1900597
TPH by Method MADEPE
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics C9-C18 ALI
UNADJ 67.0 U 33.3 67.0 134 1 08/02/2022 00:18 WG1902750
Unadjusted C19-C36 Aliphatics C19-C36 ALI
UNADJ 67.0 U 33.3 67.0 134 1 08/02/2022 00:18 WG1902750
Unadjusted C11-C22 Aromatics C11-C22 ARO
UNADJ 46.2 B J 33.3 67.0 134 1 08/02/2022 03:38 WG1902750
Unadjusted Total Petroleum
Hydrocarbons TPH UNADJ 46.2 B J 33.3 67.0 134 1 08/02/2022 00:18 WG1902750
(S) o-Terphenyl 84-15-1 76.3 40.0-140 08/02/2022 03:38 WG1902750
(S) 1-Chloro-octadecane 3386-33-2 58.7 40.0-140 08/02/2022 00:18 WG1902750
(S) 2-Fluorobiphenyl 321-60-8 96.1 40.0-140 08/02/2022 03:38 WG1902750
(S) 2-Bromonaphthalene 580-13-2 92.7 40.0-140 08/02/2022 03:38 WG1902750
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acenaphthene 83-32-9 0.500 U 0.0886 0.500 1.00 1 07/27/2022 19:15 WG1900474
Acenaphthylene 208-96-8 0.500 U 0.0921 0.500 1.00 1 07/27/2022 19:15 WG1900474
Anthracene 120-12-7 0.500 J4 U 0.0804 0.500 1.00 1 07/27/2022 19:15 WG1900474
Benzidine 92-87-5 7.50 J4 U 3.74 7.50 15.0 1 07/27/2022 19:15 WG1900474
Benzo(a)anthracene 56-55-3 0.500 U 0.199 0.500 1.00 1 07/27/2022 19:15 WG1900474
Benzo(b)fluoranthene 205-99-2 0.500 U 0.130 0.500 1.00 1 07/27/2022 19:15 WG1900474
Benzo(k)fluoranthene 207-08-9 0.500 U 0.120 0.500 1.00 1 07/27/2022 19:15 WG1900474
Benzo(g,h,i)perylene 191-24-2 0.500 U 0.121 0.500 1.00 1 07/27/2022 19:15 WG1900474
Benzo(a)pyrene 50-32-8 0.500 U 0.0381 0.500 1.00 1 07/27/2022 19:15 WG1900474
Bis(2-chlorethoxy)methane 111-91-1 5.00 J4 U 0.116 5.00 10.0 1 07/27/2022 19:15 WG1900474
Bis(2-chloroethyl)ether 111-44-4 5.00 J4 U 0.137 5.00 10.0 1 07/27/2022 19:15 WG1900474
2,2-Oxybis(1-Chloropropane)108-60-1 5.00 J4 U 0.210 5.00 10.0 1 07/27/2022 19:15 WG1900474
4-Bromophenyl-phenylether 101-55-3 5.00 U 0.0877 5.00 10.0 1 07/27/2022 19:15 WG1900474
2-Chloronaphthalene 91-58-7 0.500 U 0.0648 0.500 1.00 1 07/27/2022 19:15 WG1900474
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 24 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 24 of 84
====================----□ □ □ □
□ □ □ □
SAMPLE RESULTS - 06
L1517739
USTG480-MW18
Collected date/time: 07/20/22 11:45
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
4-Chlorophenyl-phenylether 7005-72-3 5.00 U 0.0926 5.00 10.0 1 07/27/2022 19:15 WG1900474
Chrysene 218-01-9 0.500 U 0.130 0.500 1.00 1 07/27/2022 19:15 WG1900474
Dibenz(a,h)anthracene 53-70-3 0.500 U 0.0644 0.500 1.00 1 07/27/2022 19:15 WG1900474
3,3-Dichlorobenzidine 91-94-1 5.00 U 0.212 5.00 10.0 1 07/27/2022 19:15 WG1900474
2,4-Dinitrotoluene 121-14-2 5.00 U 0.0983 5.00 10.0 1 07/27/2022 19:15 WG1900474
2,6-Dinitrotoluene 606-20-2 5.00 J4 U 0.250 5.00 10.0 1 07/27/2022 19:15 WG1900474
Fluoranthene 206-44-0 0.500 J4 U 0.102 0.500 1.00 1 07/27/2022 19:15 WG1900474
Fluorene 86-73-7 0.500 U 0.0844 0.500 1.00 1 07/27/2022 19:15 WG1900474
Hexachlorobenzene 118-74-1 0.500 U 0.0755 0.500 1.00 1 07/27/2022 19:15 WG1900474
Hexachloro-1,3-butadiene 87-68-3 5.00 U 0.0968 5.00 10.0 1 07/27/2022 19:15 WG1900474
Hexachlorocyclopentadiene 77-47-4 5.00 U 0.0598 5.00 10.0 1 07/27/2022 19:15 WG1900474
Hexachloroethane 67-72-1 5.00 U 0.127 5.00 10.0 1 07/27/2022 19:15 WG1900474
Indeno(1,2,3-cd)pyrene 193-39-5 0.600 U 0.279 0.600 1.20 1 07/27/2022 19:15 WG1900474
Isophorone 78-59-1 5.00 U 0.143 5.00 10.0 1 07/27/2022 19:15 WG1900474
Naphthalene 91-20-3 0.500 J4 U 0.159 0.500 1.00 1 07/27/2022 19:15 WG1900474
Nitrobenzene 98-95-3 5.00 J4 U 0.297 5.00 10.0 1 07/27/2022 19:15 WG1900474
n-Nitrosodimethylamine 62-75-9 5.00 U 0.998 5.00 10.0 1 07/27/2022 19:15 WG1900474
n-Nitrosodiphenylamine 86-30-6 5.00 U 2.37 5.00 10.0 1 07/27/2022 19:15 WG1900474
n-Nitrosodi-n-propylamine 621-64-7 5.00 J4 U 0.261 5.00 10.0 1 07/27/2022 19:15 WG1900474
Phenanthrene 85-01-8 0.500 J4 U 0.112 0.500 1.00 1 07/27/2022 19:15 WG1900474
Benzylbutyl phthalate 85-68-7 2.00 U 0.765 2.00 4.00 1 07/27/2022 19:15 WG1900474
Bis(2-ethylhexyl)phthalate 117-81-7 2.00 J4 U 0.895 2.00 4.00 1 07/27/2022 19:15 WG1900474
Di-n-butyl phthalate 84-74-2 1.50 J4 U 0.453 1.50 3.00 1 07/27/2022 19:15 WG1900474
Diethyl phthalate 84-66-2 1.50 J4 U 0.287 1.50 3.00 1 07/27/2022 19:15 WG1900474
Dimethyl phthalate 131-11-3 1.50 U 0.260 1.50 3.00 1 07/27/2022 19:15 WG1900474
Di-n-octyl phthalate 117-84-0 2.00 U 0.932 2.00 4.00 1 07/27/2022 19:15 WG1900474
Pyrene 129-00-0 0.500 J4 U 0.107 0.500 1.00 1 07/27/2022 19:15 WG1900474
1,2,4-Trichlorobenzene 120-82-1 5.00 U 0.0698 5.00 10.0 1 07/27/2022 19:15 WG1900474
4-Chloro-3-methylphenol 59-50-7 5.00 J4 U 0.131 5.00 10.0 1 07/27/2022 19:15 WG1900474
2-Chlorophenol 95-57-8 5.00 J4 U 0.133 5.00 10.0 1 07/27/2022 19:15 WG1900474
2,4-Dichlorophenol 120-83-2 5.00 J4 U 0.102 5.00 10.0 1 07/27/2022 19:15 WG1900474
2,4-Dimethylphenol 105-67-9 5.00 U 0.0636 5.00 10.0 1 07/27/2022 19:15 WG1900474
4,6-Dinitro-2-methylphenol 534-52-1 5.00 U 1.12 5.00 10.0 1 07/27/2022 19:15 WG1900474
2,4-Dinitrophenol 51-28-5 15.0 U 5.93 15.0 30.0 1 07/27/2022 19:15 WG1900474
2-Nitrophenol 88-75-5 5.00 J4 U 0.117 5.00 10.0 1 07/27/2022 19:15 WG1900474
4-Nitrophenol 100-02-7 5.00 U 0.143 5.00 10.0 1 07/27/2022 19:15 WG1900474
Pentachlorophenol 87-86-5 5.00 U 0.313 5.00 10.0 1 07/27/2022 19:15 WG1900474
Phenol 108-95-2 10.0 U 4.33 10.0 20.0 1 07/27/2022 19:15 WG1900474
2,4,6-Trichlorophenol 88-06-2 5.00 U 0.100 5.00 10.0 1 07/27/2022 19:15 WG1900474
1-Methylnaphthalene 90-12-0 0.500 U 0.0790 0.500 1.00 1 07/27/2022 19:15 WG1900474
2-Methylnaphthalene 91-57-6 0.500 U 0.117 0.500 1.00 1 07/27/2022 19:15 WG1900474
(S) Nitrobenzene-d5 4165-60-0 36.6 J2 0.000 44.0-120 07/27/2022 19:15 WG1900474
(S) 2-Fluorobiphenyl 321-60-8 38.7 J2 0.000 44.0-119 07/27/2022 19:15 WG1900474
(S) p-Terphenyl-d14 1718-51-0 54.2 0.000 50.0-134 07/27/2022 19:15 WG1900474
(S) Phenol-d5 4165-62-2 9.51 J2 0.000 10.0-67.0 07/27/2022 19:15 WG1900474
(S) 2-Fluorophenol 367-12-4 14.5 J2 0.000 19.0-119 07/27/2022 19:15 WG1900474
(S) 2,4,6-Tribromophenol 118-79-6 61.0 0.000 43.0-140 07/27/2022 19:15 WG1900474
Sample Narrative:
L1517739-06 WG1900474: Duplicate Analysis performed due to surrogate failure. Results confirm; reporting in hold data
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 25 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 25 of 84
====================----□ □ □ □
□ □ □ □
SAMPLE RESULTS - 07
L1517739
USTTC341-MW15R
Collected date/time: 07/20/22 11:52
Volatile Petroleum Hydrocarbons by Method MADEPV
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics C5-C8 ALI
UNADJ 67.0 U 33.3 67.0 100 1 07/30/2022 04:37 WG1902102
Unadjusted C9-C12 Aliphatics C9-C12 ALI
UNADJ 67.0 U 33.3 67.0 134 1 07/30/2022 04:37 WG1902102
Unadjusted C9-C10 Aromatics C9-C10 ARO
UNADJ 67.0 U 33.3 67.0 100 1 07/30/2022 04:37 WG1902102
Total VPH VPH 150 U 66.7 150 300 1 07/30/2022 04:37 WG1902102
(S) 2,5-Dibromotoluene(FID)615-59-8 104 70.0-130 07/30/2022 04:37 WG1902102
(S) 2,5-Dibromotoluene(PID)615-59-8 104 70.0-130 07/30/2022 04:37 WG1902102
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acetone 67-64-1 25.0 J3 U 11.3 25.0 50.0 1 07/25/2022 19:13 WG1900597
Acrolein 107-02-8 25.0 C4 U 2.54 25.0 50.0 1 07/25/2022 19:13 WG1900597
Acrylonitrile 107-13-1 5.00 J4 U 0.671 5.00 10.0 1 07/25/2022 19:13 WG1900597
Benzene 71-43-2 0.500 U 0.0941 0.500 1.00 1 07/25/2022 19:13 WG1900597
Bromobenzene 108-86-1 0.500 U 0.118 0.500 1.00 1 07/25/2022 19:13 WG1900597
Bromodichloromethane 75-27-4 0.500 U 0.136 0.500 1.00 1 07/25/2022 19:13 WG1900597
Bromoform 75-25-2 0.500 U 0.129 0.500 1.00 1 07/25/2022 19:13 WG1900597
Bromomethane 74-83-9 2.00 U 0.605 2.00 5.00 1 07/25/2022 19:13 WG1900597
n-Butylbenzene 104-51-8 0.500 U 0.157 0.500 1.00 1 07/25/2022 19:13 WG1900597
sec-Butylbenzene 135-98-8 0.500 U 0.125 0.500 1.00 1 07/25/2022 19:13 WG1900597
tert-Butylbenzene 98-06-6 0.500 U 0.127 0.500 1.00 1 07/25/2022 19:13 WG1900597
Carbon tetrachloride 56-23-5 0.500 U 0.128 0.500 1.00 1 07/25/2022 19:13 WG1900597
Chlorobenzene 108-90-7 0.500 U 0.116 0.500 1.00 1 07/25/2022 19:13 WG1900597
Chlorodibromomethane 124-48-1 0.500 U 0.140 0.500 1.00 1 07/25/2022 19:13 WG1900597
Chloroethane 75-00-3 2.00 U 0.192 2.00 5.00 1 07/25/2022 19:13 WG1900597
Chloroform 67-66-3 2.00 U 0.111 2.00 5.00 1 07/25/2022 19:13 WG1900597
Chloromethane 74-87-3 2.00 U 0.960 2.00 4.00 1 07/25/2022 19:13 WG1900597
2-Chlorotoluene 95-49-8 0.500 U 0.106 0.500 1.00 1 07/25/2022 19:13 WG1900597
4-Chlorotoluene 106-43-4 0.500 U 0.114 0.500 1.00 1 07/25/2022 19:13 WG1900597
1,2-Dibromo-3-Chloropropane 96-12-8 2.00 U 0.276 2.00 5.00 1 07/25/2022 19:13 WG1900597
1,2-Dibromoethane 106-93-4 0.500 U 0.126 0.500 1.00 1 07/25/2022 19:13 WG1900597
Dibromomethane 74-95-3 0.500 U 0.122 0.500 1.00 1 07/25/2022 19:13 WG1900597
1,2-Dichlorobenzene 95-50-1 0.500 U 0.107 0.500 1.00 1 07/25/2022 19:13 WG1900597
1,3-Dichlorobenzene 541-73-1 0.500 U 0.110 0.500 1.00 1 07/25/2022 19:13 WG1900597
1,4-Dichlorobenzene 106-46-7 0.500 U 0.120 0.500 1.00 1 07/25/2022 19:13 WG1900597
Dichlorodifluoromethane 75-71-8 2.00 U 0.374 2.00 5.00 1 07/25/2022 19:13 WG1900597
1,1-Dichloroethane 75-34-3 0.500 U 0.100 0.500 1.00 1 07/25/2022 19:13 WG1900597
1,2-Dichloroethane 107-06-2 0.500 U 0.0819 0.500 1.00 1 07/25/2022 19:13 WG1900597
1,1-Dichloroethene 75-35-4 0.500 U 0.188 0.500 1.00 1 07/25/2022 19:13 WG1900597
cis-1,2-Dichloroethene 156-59-2 0.500 U 0.126 0.500 1.00 1 07/25/2022 19:13 WG1900597
trans-1,2-Dichloroethene 156-60-5 0.500 U 0.149 0.500 1.00 1 07/25/2022 19:13 WG1900597
1,2-Dichloropropane 78-87-5 0.500 U 0.149 0.500 1.00 1 07/25/2022 19:13 WG1900597
1,1-Dichloropropene 563-58-6 0.500 U 0.142 0.500 1.00 1 07/25/2022 19:13 WG1900597
1,3-Dichloropropane 142-28-9 0.500 U 0.110 0.500 1.00 1 07/25/2022 19:13 WG1900597
2,2-Dichloropropane 594-20-7 0.500 U 0.161 0.500 1.00 1 07/25/2022 19:13 WG1900597
Di-isopropyl ether 108-20-3 0.292 J 0.105 0.500 1.00 1 07/25/2022 19:13 WG1900597
Ethylbenzene 100-41-4 0.500 U 0.137 0.500 1.00 1 07/25/2022 19:13 WG1900597
Hexachloro-1,3-butadiene 87-68-3 0.750 J3 U 0.337 0.750 1.50 1 07/25/2022 19:13 WG1900597
Isopropylbenzene 98-82-8 0.500 U 0.105 0.500 1.00 1 07/25/2022 19:13 WG1900597
p-Isopropyltoluene 99-87-6 0.500 U 0.120 0.500 1.00 1 07/25/2022 19:13 WG1900597
2-Butanone (MEK)78-93-3 5.00 U 1.19 5.00 10.0 1 07/25/2022 19:13 WG1900597
Methylene Chloride 75-09-2 2.00 U 0.430 2.00 5.00 1 07/25/2022 19:13 WG1900597
4-Methyl-2-pentanone (MIBK)108-10-1 5.00 U 0.478 5.00 10.0 1 07/25/2022 19:13 WG1900597
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 26 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 26 of 84
--------------=---□
□ □ □
==============~~~~~=----□ □ □ □
SAMPLE RESULTS - 07
L1517739
USTTC341-MW15R
Collected date/time: 07/20/22 11:52
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Methyl tert-butyl ether 1634-04-4 0.500 U 0.101 0.500 1.00 1 07/25/2022 19:13 WG1900597
Naphthalene 91-20-3 2.00 U 1.00 2.00 5.00 1 07/25/2022 19:13 WG1900597
n-Propylbenzene 103-65-1 0.500 U 0.0993 0.500 1.00 1 07/25/2022 19:13 WG1900597
Styrene 100-42-5 0.500 U 0.118 0.500 1.00 1 07/25/2022 19:13 WG1900597
1,1,1,2-Tetrachloroethane 630-20-6 0.500 U 0.147 0.500 1.00 1 07/25/2022 19:13 WG1900597
1,1,2,2-Tetrachloroethane 79-34-5 0.500 U 0.133 0.500 1.00 1 07/25/2022 19:13 WG1900597
Tetrachloroethene 127-18-4 0.600 U 0.300 0.600 1.20 1 07/25/2022 19:13 WG1900597
Toluene 108-88-3 0.600 U 0.278 0.600 1.20 1 07/25/2022 19:13 WG1900597
1,2,3-Trichlorobenzene 87-61-6 0.500 U 0.230 0.500 1.00 1 07/25/2022 19:13 WG1900597
1,2,4-Trichlorobenzene 120-82-1 1.00 U 0.481 1.00 2.00 1 07/25/2022 19:13 WG1900597
1,1,1-Trichloroethane 71-55-6 0.500 U 0.149 0.500 1.00 1 07/25/2022 19:13 WG1900597
1,1,2-Trichloroethane 79-00-5 0.500 U 0.158 0.500 1.00 1 07/25/2022 19:13 WG1900597
Trichloroethene 79-01-6 0.500 U 0.190 0.500 1.00 1 07/25/2022 19:13 WG1900597
Trichlorofluoromethane 75-69-4 2.00 U 0.160 2.00 5.00 1 07/25/2022 19:13 WG1900597
1,2,3-Trichloropropane 96-18-4 1.00 U 0.237 1.00 2.50 1 07/25/2022 19:13 WG1900597
1,2,4-Trimethylbenzene 95-63-6 1.00 U 0.322 1.00 2.00 1 07/25/2022 19:13 WG1900597
1,3,5-Trimethylbenzene 108-67-8 0.500 U 0.104 0.500 1.00 1 07/25/2022 19:13 WG1900597
Vinyl chloride 75-01-4 0.500 U 0.234 0.500 1.00 1 07/25/2022 19:13 WG1900597
o-Xylene 95-47-6 0.500 U 0.174 0.500 1.00 1 07/25/2022 19:13 WG1900597
m&p-Xylenes 1330-20-7 1.00 U 0.430 1.00 2.00 1 07/25/2022 19:13 WG1900597
(S) Toluene-d8 2037-26-5 100 89.0-112 07/25/2022 19:13 WG1900597
(S) 4-Bromofluorobenzene 460-00-4 100 85.0-114 07/25/2022 19:13 WG1900597
(S) 1,2-Dichloroethane-d4 17060-07-0 103 81.0-118 07/25/2022 19:13 WG1900597
TPH by Method MADEPE
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics C9-C18 ALI
UNADJ 67.0 U 33.3 67.0 134 1 08/02/2022 00:41 WG1902750
Unadjusted C19-C36 Aliphatics C19-C36 ALI
UNADJ 34.8 B J 33.3 67.0 134 1 08/02/2022 00:41 WG1902750
Unadjusted C11-C22 Aromatics C11-C22 ARO
UNADJ 53.6 B J 33.3 67.0 134 1 08/02/2022 02:09 WG1902750
Unadjusted Total Petroleum
Hydrocarbons TPH UNADJ 88.4 B J 33.3 67.0 134 1 08/02/2022 02:09 WG1902750
(S) o-Terphenyl 84-15-1 74.2 40.0-140 08/02/2022 02:09 WG1902750
(S) 1-Chloro-octadecane 3386-33-2 60.4 40.0-140 08/02/2022 00:41 WG1902750
(S) 2-Fluorobiphenyl 321-60-8 89.7 40.0-140 08/02/2022 02:09 WG1902750
(S) 2-Bromonaphthalene 580-13-2 86.7 40.0-140 08/02/2022 02:09 WG1902750
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acenaphthene 83-32-9 0.500 U 0.0886 0.500 1.00 1 07/27/2022 19:37 WG1900474
Acenaphthylene 208-96-8 0.500 U 0.0921 0.500 1.00 1 07/27/2022 19:37 WG1900474
Anthracene 120-12-7 0.500 J4 U 0.0804 0.500 1.00 1 07/27/2022 19:37 WG1900474
Benzidine 92-87-5 7.50 J4 U 3.74 7.50 15.0 1 07/27/2022 19:37 WG1900474
Benzo(a)anthracene 56-55-3 0.500 U 0.199 0.500 1.00 1 07/27/2022 19:37 WG1900474
Benzo(b)fluoranthene 205-99-2 0.500 U 0.130 0.500 1.00 1 07/27/2022 19:37 WG1900474
Benzo(k)fluoranthene 207-08-9 0.500 U 0.120 0.500 1.00 1 07/27/2022 19:37 WG1900474
Benzo(g,h,i)perylene 191-24-2 0.500 U 0.121 0.500 1.00 1 07/27/2022 19:37 WG1900474
Benzo(a)pyrene 50-32-8 0.500 U 0.0381 0.500 1.00 1 07/27/2022 19:37 WG1900474
Bis(2-chlorethoxy)methane 111-91-1 5.00 J4 U 0.116 5.00 10.0 1 07/27/2022 19:37 WG1900474
Bis(2-chloroethyl)ether 111-44-4 5.00 J4 U 0.137 5.00 10.0 1 07/27/2022 19:37 WG1900474
2,2-Oxybis(1-Chloropropane)108-60-1 5.00 J4 U 0.210 5.00 10.0 1 07/27/2022 19:37 WG1900474
4-Bromophenyl-phenylether 101-55-3 5.00 U 0.0877 5.00 10.0 1 07/27/2022 19:37 WG1900474
2-Chloronaphthalene 91-58-7 0.500 U 0.0648 0.500 1.00 1 07/27/2022 19:37 WG1900474
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 27 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 27 of 84
====================----□ □ □ □
□ □ □ □
SAMPLE RESULTS - 07
L1517739
USTTC341-MW15R
Collected date/time: 07/20/22 11:52
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
4-Chlorophenyl-phenylether 7005-72-3 5.00 U 0.0926 5.00 10.0 1 07/27/2022 19:37 WG1900474
Chrysene 218-01-9 0.500 U 0.130 0.500 1.00 1 07/27/2022 19:37 WG1900474
Dibenz(a,h)anthracene 53-70-3 0.500 U 0.0644 0.500 1.00 1 07/27/2022 19:37 WG1900474
3,3-Dichlorobenzidine 91-94-1 5.00 U 0.212 5.00 10.0 1 07/27/2022 19:37 WG1900474
2,4-Dinitrotoluene 121-14-2 5.00 U 0.0983 5.00 10.0 1 07/27/2022 19:37 WG1900474
2,6-Dinitrotoluene 606-20-2 5.00 J4 U 0.250 5.00 10.0 1 07/27/2022 19:37 WG1900474
Fluoranthene 206-44-0 0.500 J4 U 0.102 0.500 1.00 1 07/27/2022 19:37 WG1900474
Fluorene 86-73-7 0.500 U 0.0844 0.500 1.00 1 07/27/2022 19:37 WG1900474
Hexachlorobenzene 118-74-1 0.500 U 0.0755 0.500 1.00 1 07/27/2022 19:37 WG1900474
Hexachloro-1,3-butadiene 87-68-3 5.00 U 0.0968 5.00 10.0 1 07/27/2022 19:37 WG1900474
Hexachlorocyclopentadiene 77-47-4 5.00 U 0.0598 5.00 10.0 1 07/27/2022 19:37 WG1900474
Hexachloroethane 67-72-1 5.00 U 0.127 5.00 10.0 1 07/27/2022 19:37 WG1900474
Indeno(1,2,3-cd)pyrene 193-39-5 0.600 U 0.279 0.600 1.20 1 07/27/2022 19:37 WG1900474
Isophorone 78-59-1 5.00 U 0.143 5.00 10.0 1 07/27/2022 19:37 WG1900474
Naphthalene 91-20-3 0.500 J4 U 0.159 0.500 1.00 1 07/27/2022 19:37 WG1900474
Nitrobenzene 98-95-3 5.00 J4 U 0.297 5.00 10.0 1 07/27/2022 19:37 WG1900474
n-Nitrosodimethylamine 62-75-9 5.00 U 0.998 5.00 10.0 1 07/27/2022 19:37 WG1900474
n-Nitrosodiphenylamine 86-30-6 5.00 U 2.37 5.00 10.0 1 07/27/2022 19:37 WG1900474
n-Nitrosodi-n-propylamine 621-64-7 5.00 J4 U 0.261 5.00 10.0 1 07/27/2022 19:37 WG1900474
Phenanthrene 85-01-8 0.500 J4 U 0.112 0.500 1.00 1 07/27/2022 19:37 WG1900474
Benzylbutyl phthalate 85-68-7 2.00 U 0.765 2.00 4.00 1 07/27/2022 19:37 WG1900474
Bis(2-ethylhexyl)phthalate 117-81-7 2.00 J4 U 0.895 2.00 4.00 1 07/27/2022 19:37 WG1900474
Di-n-butyl phthalate 84-74-2 1.50 J4 U 0.453 1.50 3.00 1 07/27/2022 19:37 WG1900474
Diethyl phthalate 84-66-2 1.50 J4 U 0.287 1.50 3.00 1 07/27/2022 19:37 WG1900474
Dimethyl phthalate 131-11-3 1.50 U 0.260 1.50 3.00 1 07/27/2022 19:37 WG1900474
Di-n-octyl phthalate 117-84-0 2.00 U 0.932 2.00 4.00 1 07/27/2022 19:37 WG1900474
Pyrene 129-00-0 0.500 J4 U 0.107 0.500 1.00 1 07/27/2022 19:37 WG1900474
1,2,4-Trichlorobenzene 120-82-1 5.00 U 0.0698 5.00 10.0 1 07/27/2022 19:37 WG1900474
4-Chloro-3-methylphenol 59-50-7 5.00 J4 U 0.131 5.00 10.0 1 07/27/2022 19:37 WG1900474
2-Chlorophenol 95-57-8 5.00 J4 U 0.133 5.00 10.0 1 07/27/2022 19:37 WG1900474
2,4-Dichlorophenol 120-83-2 5.00 J4 U 0.102 5.00 10.0 1 07/27/2022 19:37 WG1900474
2,4-Dimethylphenol 105-67-9 5.00 U 0.0636 5.00 10.0 1 07/27/2022 19:37 WG1900474
4,6-Dinitro-2-methylphenol 534-52-1 5.00 U 1.12 5.00 10.0 1 07/27/2022 19:37 WG1900474
2,4-Dinitrophenol 51-28-5 15.0 U 5.93 15.0 30.0 1 07/27/2022 19:37 WG1900474
2-Nitrophenol 88-75-5 5.00 J4 U 0.117 5.00 10.0 1 07/27/2022 19:37 WG1900474
4-Nitrophenol 100-02-7 5.00 U 0.143 5.00 10.0 1 07/27/2022 19:37 WG1900474
Pentachlorophenol 87-86-5 5.00 U 0.313 5.00 10.0 1 07/27/2022 19:37 WG1900474
Phenol 108-95-2 10.0 U 4.33 10.0 20.0 1 07/27/2022 19:37 WG1900474
2,4,6-Trichlorophenol 88-06-2 5.00 U 0.100 5.00 10.0 1 07/27/2022 19:37 WG1900474
1-Methylnaphthalene 90-12-0 0.500 U 0.0790 0.500 1.00 1 07/27/2022 19:37 WG1900474
2-Methylnaphthalene 91-57-6 0.500 U 0.117 0.500 1.00 1 07/27/2022 19:37 WG1900474
(S) Nitrobenzene-d5 4165-60-0 5.41 J2 0.000 44.0-120 07/27/2022 19:37 WG1900474
(S) 2-Fluorobiphenyl 321-60-8 5.40 J2 0.000 44.0-119 07/27/2022 19:37 WG1900474
(S) p-Terphenyl-d14 1718-51-0 7.31 J2 0.000 50.0-134 07/27/2022 19:37 WG1900474
(S) Phenol-d5 4165-62-2 1.71 J2 0.000 10.0-67.0 07/27/2022 19:37 WG1900474
(S) 2-Fluorophenol 367-12-4 2.67 J2 0.000 19.0-119 07/27/2022 19:37 WG1900474
(S) 2,4,6-Tribromophenol 118-79-6 7.50 J2 0.000 43.0-140 07/27/2022 19:37 WG1900474
Sample Narrative:
L1517739-07 WG1900474: Duplicate Analysis performed due to surrogate failure. Results confirm; reporting in hold data
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 28 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 28 of 84
====================----□ □ □ □
□ □ □ □
SAMPLE RESULTS - 08
L1517739
USTG480-MW08
Collected date/time: 07/20/22 12:30
Volatile Petroleum Hydrocarbons by Method MADEPV
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics C5-C8 ALI
UNADJ 16100 666 1340 2000 20 07/30/2022 06:15 WG1902102
Unadjusted C9-C12 Aliphatics C9-C12 ALI
UNADJ 2150 B J 666 1340 2680 20 07/30/2022 06:15 WG1902102
Unadjusted C9-C10 Aromatics C9-C10 ARO
UNADJ 1920 J 666 1340 2000 20 07/30/2022 06:15 WG1902102
Total VPH VPH 20200 1330 3000 6000 20 07/30/2022 06:15 WG1902102
(S) 2,5-Dibromotoluene(FID)615-59-8 109 70.0-130 07/30/2022 06:15 WG1902102
(S) 2,5-Dibromotoluene(PID)615-59-8 101 70.0-130 07/30/2022 06:15 WG1902102
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acetone 67-64-1 500 J3 U 226 500 1000 20 07/25/2022 22:43 WG1900597
Acrolein 107-02-8 500 C4 U 50.8 500 1000 20 07/25/2022 22:43 WG1900597
Acrylonitrile 107-13-1 100 J4 U 13.4 100 200 20 07/25/2022 22:43 WG1900597
Benzene 71-43-2 119 1.88 10.0 20.0 20 07/25/2022 22:43 WG1900597
Bromobenzene 108-86-1 10.0 U 2.36 10.0 20.0 20 07/25/2022 22:43 WG1900597
Bromodichloromethane 75-27-4 10.0 U 2.72 10.0 20.0 20 07/25/2022 22:43 WG1900597
Bromoform 75-25-2 10.0 U 2.58 10.0 20.0 20 07/25/2022 22:43 WG1900597
Bromomethane 74-83-9 40.0 U 12.1 40.0 100 20 07/25/2022 22:43 WG1900597
n-Butylbenzene 104-51-8 10.1 J 3.14 10.0 20.0 20 07/25/2022 22:43 WG1900597
sec-Butylbenzene 135-98-8 10.9 J 2.50 10.0 20.0 20 07/25/2022 22:43 WG1900597
tert-Butylbenzene 98-06-6 2.80 J 2.54 10.0 20.0 20 07/25/2022 22:43 WG1900597
Carbon tetrachloride 56-23-5 10.0 U 2.56 10.0 20.0 20 07/25/2022 22:43 WG1900597
Chlorobenzene 108-90-7 10.0 U 2.32 10.0 20.0 20 07/25/2022 22:43 WG1900597
Chlorodibromomethane 124-48-1 10.0 U 2.80 10.0 20.0 20 07/25/2022 22:43 WG1900597
Chloroethane 75-00-3 40.0 U 3.84 40.0 100 20 07/25/2022 22:43 WG1900597
Chloroform 67-66-3 40.0 U 2.22 40.0 100 20 07/25/2022 22:43 WG1900597
Chloromethane 74-87-3 40.0 U 19.2 40.0 80.0 20 07/25/2022 22:43 WG1900597
2-Chlorotoluene 95-49-8 10.0 U 2.12 10.0 20.0 20 07/25/2022 22:43 WG1900597
4-Chlorotoluene 106-43-4 10.0 U 2.28 10.0 20.0 20 07/25/2022 22:43 WG1900597
1,2-Dibromo-3-Chloropropane 96-12-8 40.0 U 5.52 40.0 100 20 07/25/2022 22:43 WG1900597
1,2-Dibromoethane 106-93-4 10.0 U 2.52 10.0 20.0 20 07/25/2022 22:43 WG1900597
Dibromomethane 74-95-3 10.0 U 2.44 10.0 20.0 20 07/25/2022 22:43 WG1900597
1,2-Dichlorobenzene 95-50-1 10.0 U 2.14 10.0 20.0 20 07/25/2022 22:43 WG1900597
1,3-Dichlorobenzene 541-73-1 10.0 U 2.20 10.0 20.0 20 07/25/2022 22:43 WG1900597
1,4-Dichlorobenzene 106-46-7 10.0 U 2.40 10.0 20.0 20 07/25/2022 22:43 WG1900597
Dichlorodifluoromethane 75-71-8 40.0 U 7.48 40.0 100 20 07/25/2022 22:43 WG1900597
1,1-Dichloroethane 75-34-3 10.0 U 2.00 10.0 20.0 20 07/25/2022 22:43 WG1900597
1,2-Dichloroethane 107-06-2 10.0 U 1.64 10.0 20.0 20 07/25/2022 22:43 WG1900597
1,1-Dichloroethene 75-35-4 10.0 U 3.76 10.0 20.0 20 07/25/2022 22:43 WG1900597
cis-1,2-Dichloroethene 156-59-2 10.0 U 2.52 10.0 20.0 20 07/25/2022 22:43 WG1900597
trans-1,2-Dichloroethene 156-60-5 10.0 U 2.98 10.0 20.0 20 07/25/2022 22:43 WG1900597
1,2-Dichloropropane 78-87-5 10.0 U 2.98 10.0 20.0 20 07/25/2022 22:43 WG1900597
1,1-Dichloropropene 563-58-6 10.0 U 2.84 10.0 20.0 20 07/25/2022 22:43 WG1900597
1,3-Dichloropropane 142-28-9 10.0 U 2.20 10.0 20.0 20 07/25/2022 22:43 WG1900597
2,2-Dichloropropane 594-20-7 10.0 U 3.22 10.0 20.0 20 07/25/2022 22:43 WG1900597
Di-isopropyl ether 108-20-3 10.0 U 2.10 10.0 20.0 20 07/25/2022 22:43 WG1900597
Ethylbenzene 100-41-4 203 2.74 10.0 20.0 20 07/25/2022 22:43 WG1900597
Hexachloro-1,3-butadiene 87-68-3 15.0 J3 U 6.74 15.0 30.0 20 07/25/2022 22:43 WG1900597
Isopropylbenzene 98-82-8 43.9 2.10 10.0 20.0 20 07/25/2022 22:43 WG1900597
p-Isopropyltoluene 99-87-6 9.42 J 2.40 10.0 20.0 20 07/25/2022 22:43 WG1900597
2-Butanone (MEK)78-93-3 100 U 23.8 100 200 20 07/25/2022 22:43 WG1900597
Methylene Chloride 75-09-2 40.0 U 8.60 40.0 100 20 07/25/2022 22:43 WG1900597
4-Methyl-2-pentanone (MIBK)108-10-1 100 U 9.56 100 200 20 07/25/2022 22:43 WG1900597
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 29 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 29 of 84
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==============~~~~~=----□ □ □ □
SAMPLE RESULTS - 08
L1517739
USTG480-MW08
Collected date/time: 07/20/22 12:30
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Methyl tert-butyl ether 1634-04-4 10.0 U 2.02 10.0 20.0 20 07/25/2022 22:43 WG1900597
Naphthalene 91-20-3 606 20.0 40.0 100 20 07/25/2022 22:43 WG1900597
n-Propylbenzene 103-65-1 65.8 1.99 10.0 20.0 20 07/25/2022 22:43 WG1900597
Styrene 100-42-5 10.0 U 2.36 10.0 20.0 20 07/25/2022 22:43 WG1900597
1,1,1,2-Tetrachloroethane 630-20-6 10.0 U 2.94 10.0 20.0 20 07/25/2022 22:43 WG1900597
1,1,2,2-Tetrachloroethane 79-34-5 10.0 U 2.66 10.0 20.0 20 07/25/2022 22:43 WG1900597
Tetrachloroethene 127-18-4 12.0 U 6.00 12.0 24.0 20 07/25/2022 22:43 WG1900597
Toluene 108-88-3 12.0 U 5.56 12.0 24.0 20 07/25/2022 22:43 WG1900597
1,2,3-Trichlorobenzene 87-61-6 10.0 U 4.60 10.0 20.0 20 07/25/2022 22:43 WG1900597
1,2,4-Trichlorobenzene 120-82-1 20.0 U 9.62 20.0 40.0 20 07/25/2022 22:43 WG1900597
1,1,1-Trichloroethane 71-55-6 10.0 U 2.98 10.0 20.0 20 07/25/2022 22:43 WG1900597
1,1,2-Trichloroethane 79-00-5 10.0 U 3.16 10.0 20.0 20 07/25/2022 22:43 WG1900597
Trichloroethene 79-01-6 10.0 U 3.80 10.0 20.0 20 07/25/2022 22:43 WG1900597
Trichlorofluoromethane 75-69-4 40.0 U 3.20 40.0 100 20 07/25/2022 22:43 WG1900597
1,2,3-Trichloropropane 96-18-4 20.0 U 4.74 20.0 50.0 20 07/25/2022 22:43 WG1900597
1,2,4-Trimethylbenzene 95-63-6 214 6.44 20.0 40.0 20 07/25/2022 22:43 WG1900597
1,3,5-Trimethylbenzene 108-67-8 43.8 2.08 10.0 20.0 20 07/25/2022 22:43 WG1900597
Vinyl chloride 75-01-4 10.0 U 4.68 10.0 20.0 20 07/25/2022 22:43 WG1900597
o-Xylene 95-47-6 7.90 J 3.48 10.0 20.0 20 07/25/2022 22:43 WG1900597
m&p-Xylenes 1330-20-7 118 8.60 20.0 40.0 20 07/25/2022 22:43 WG1900597
(S) Toluene-d8 2037-26-5 95.9 89.0-112 07/25/2022 22:43 WG1900597
(S) 4-Bromofluorobenzene 460-00-4 104 85.0-114 07/25/2022 22:43 WG1900597
(S) 1,2-Dichloroethane-d4 17060-07-0 106 81.0-118 07/25/2022 22:43 WG1900597
TPH by Method MADEPE
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics C9-C18 ALI
UNADJ 17500 333 670 1340 10 08/03/2022 08:37 WG1902750
Unadjusted C19-C36 Aliphatics C19-C36 ALI
UNADJ 3250 33.3 67.0 134 1 08/02/2022 01:03 WG1902750
Unadjusted C11-C22 Aromatics C11-C22 ARO
UNADJ 14900 333 670 1340 10 08/03/2022 08:59 WG1902750
Unadjusted Total Petroleum
Hydrocarbons TPH UNADJ 35700 333 670 1340 10 08/03/2022 08:59 WG1902750
(S) o-Terphenyl 84-15-1 84.4 40.0-140 08/03/2022 08:59 WG1902750
(S) 1-Chloro-octadecane 3386-33-2 52.0 40.0-140 08/03/2022 08:37 WG1902750
(S) 1-Chloro-octadecane 3386-33-2 52.3 40.0-140 08/02/2022 01:03 WG1902750
(S) 2-Fluorobiphenyl 321-60-8 110 40.0-140 08/03/2022 08:59 WG1902750
(S) 2-Bromonaphthalene 580-13-2 94.5 40.0-140 08/03/2022 08:59 WG1902750
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acenaphthene 83-32-9 17.7 0.443 2.50 5.00 5 07/27/2022 23:17 WG1900474
Acenaphthylene 208-96-8 2.50 U 0.461 2.50 5.00 5 07/27/2022 23:17 WG1900474
Anthracene 120-12-7 2.50 J4 U 0.402 2.50 5.00 5 07/27/2022 23:17 WG1900474
Benzidine 92-87-5 37.5 J4 U 18.7 37.5 75.0 5 07/27/2022 23:17 WG1900474
Benzo(a)anthracene 56-55-3 2.50 U 0.995 2.50 5.00 5 07/27/2022 23:17 WG1900474
Benzo(b)fluoranthene 205-99-2 2.50 U 0.650 2.50 5.00 5 07/27/2022 23:17 WG1900474
Benzo(k)fluoranthene 207-08-9 2.50 U 0.600 2.50 5.00 5 07/27/2022 23:17 WG1900474
Benzo(g,h,i)perylene 191-24-2 2.50 U 0.605 2.50 5.00 5 07/27/2022 23:17 WG1900474
Benzo(a)pyrene 50-32-8 2.50 U 0.191 2.50 5.00 5 07/27/2022 23:17 WG1900474
Bis(2-chlorethoxy)methane 111-91-1 25.0 J4 U 0.580 25.0 50.0 5 07/27/2022 23:17 WG1900474
Bis(2-chloroethyl)ether 111-44-4 25.0 J4 U 0.685 25.0 50.0 5 07/27/2022 23:17 WG1900474
2,2-Oxybis(1-Chloropropane)108-60-1 25.0 J4 U 1.05 25.0 50.0 5 07/27/2022 23:17 WG1900474
4-Bromophenyl-phenylether 101-55-3 25.0 U 0.439 25.0 50.0 5 07/27/2022 23:17 WG1900474
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 30 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 30 of 84
====================----□ □ □ □
□ □ □ □
SAMPLE RESULTS - 08
L1517739
USTG480-MW08
Collected date/time: 07/20/22 12:30
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
2-Chloronaphthalene 91-58-7 2.50 U 0.324 2.50 5.00 5 07/27/2022 23:17 WG1900474
4-Chlorophenyl-phenylether 7005-72-3 25.0 U 0.463 25.0 50.0 5 07/27/2022 23:17 WG1900474
Chrysene 218-01-9 2.50 U 0.650 2.50 5.00 5 07/27/2022 23:17 WG1900474
Dibenz(a,h)anthracene 53-70-3 2.50 U 0.322 2.50 5.00 5 07/27/2022 23:17 WG1900474
3,3-Dichlorobenzidine 91-94-1 25.0 U 1.06 25.0 50.0 5 07/27/2022 23:17 WG1900474
2,4-Dinitrotoluene 121-14-2 25.0 U 0.491 25.0 50.0 5 07/27/2022 23:17 WG1900474
2,6-Dinitrotoluene 606-20-2 25.0 J4 U 1.25 25.0 50.0 5 07/27/2022 23:17 WG1900474
Fluoranthene 206-44-0 0.994 J J4 0.510 2.50 5.00 5 07/27/2022 23:17 WG1900474
Fluorene 86-73-7 22.3 0.422 2.50 5.00 5 07/27/2022 23:17 WG1900474
Hexachlorobenzene 118-74-1 2.50 U 0.378 2.50 5.00 5 07/27/2022 23:17 WG1900474
Hexachloro-1,3-butadiene 87-68-3 25.0 U 0.484 25.0 50.0 5 07/27/2022 23:17 WG1900474
Hexachlorocyclopentadiene 77-47-4 25.0 U 0.299 25.0 50.0 5 07/27/2022 23:17 WG1900474
Hexachloroethane 67-72-1 25.0 U 0.635 25.0 50.0 5 07/27/2022 23:17 WG1900474
Indeno(1,2,3-cd)pyrene 193-39-5 3.00 U 1.40 3.00 6.00 5 07/27/2022 23:17 WG1900474
Isophorone 78-59-1 25.0 U 0.715 25.0 50.0 5 07/27/2022 23:17 WG1900474
Naphthalene 91-20-3 289 J4 0.795 2.50 5.00 5 07/27/2022 23:17 WG1900474
Nitrobenzene 98-95-3 25.0 J4 U 1.48 25.0 50.0 5 07/27/2022 23:17 WG1900474
n-Nitrosodimethylamine 62-75-9 25.0 U 4.99 25.0 50.0 5 07/27/2022 23:17 WG1900474
n-Nitrosodiphenylamine 86-30-6 25.0 U 11.9 25.0 50.0 5 07/27/2022 23:17 WG1900474
n-Nitrosodi-n-propylamine 621-64-7 25.0 J4 U 1.31 25.0 50.0 5 07/27/2022 23:17 WG1900474
Phenanthrene 85-01-8 47.5 J4 0.560 2.50 5.00 5 07/27/2022 23:17 WG1900474
Benzylbutyl phthalate 85-68-7 10.0 U 3.83 10.0 20.0 5 07/27/2022 23:17 WG1900474
Bis(2-ethylhexyl)phthalate 117-81-7 10.0 J4 U 4.48 10.0 20.0 5 07/27/2022 23:17 WG1900474
Di-n-butyl phthalate 84-74-2 7.50 J4 U 2.27 7.50 15.0 5 07/27/2022 23:17 WG1900474
Diethyl phthalate 84-66-2 7.50 J4 U 1.43 7.50 15.0 5 07/27/2022 23:17 WG1900474
Dimethyl phthalate 131-11-3 7.50 U 1.30 7.50 15.0 5 07/27/2022 23:17 WG1900474
Di-n-octyl phthalate 117-84-0 10.0 U 4.66 10.0 20.0 5 07/27/2022 23:17 WG1900474
Pyrene 129-00-0 1.72 J J4 0.535 2.50 5.00 5 07/27/2022 23:17 WG1900474
1,2,4-Trichlorobenzene 120-82-1 25.0 U 0.349 25.0 50.0 5 07/27/2022 23:17 WG1900474
4-Chloro-3-methylphenol 59-50-7 25.0 J4 U 0.655 25.0 50.0 5 07/27/2022 23:17 WG1900474
2-Chlorophenol 95-57-8 25.0 J4 U 0.665 25.0 50.0 5 07/27/2022 23:17 WG1900474
2,4-Dichlorophenol 120-83-2 25.0 J4 U 0.510 25.0 50.0 5 07/27/2022 23:17 WG1900474
2,4-Dimethylphenol 105-67-9 25.0 U 0.318 25.0 50.0 5 07/27/2022 23:17 WG1900474
4,6-Dinitro-2-methylphenol 534-52-1 25.0 U 5.60 25.0 50.0 5 07/27/2022 23:17 WG1900474
2,4-Dinitrophenol 51-28-5 75.0 U 29.7 75.0 150 5 07/27/2022 23:17 WG1900474
2-Nitrophenol 88-75-5 25.0 J4 U 0.585 25.0 50.0 5 07/27/2022 23:17 WG1900474
4-Nitrophenol 100-02-7 25.0 U 0.715 25.0 50.0 5 07/27/2022 23:17 WG1900474
Pentachlorophenol 87-86-5 25.0 U 1.57 25.0 50.0 5 07/27/2022 23:17 WG1900474
Phenol 108-95-2 50.0 U 21.7 50.0 100 5 07/27/2022 23:17 WG1900474
2,4,6-Trichlorophenol 88-06-2 25.0 U 0.500 25.0 50.0 5 07/27/2022 23:17 WG1900474
(S) Nitrobenzene-d5 4165-60-0 52.1 0.000 44.0-120 07/27/2022 23:17 WG1900474
(S) 2-Fluorobiphenyl 321-60-8 87.1 0.000 44.0-119 07/27/2022 23:17 WG1900474
(S) p-Terphenyl-d14 1718-51-0 70.1 0.000 50.0-134 07/27/2022 23:17 WG1900474
(S) Phenol-d5 4165-62-2 22.4 0.000 10.0-67.0 07/27/2022 23:17 WG1900474
(S) 2-Fluorophenol 367-12-4 28.4 0.000 19.0-119 07/27/2022 23:17 WG1900474
(S) 2,4,6-Tribromophenol 118-79-6 97.0 0.000 43.0-140 07/27/2022 23:17 WG1900474
Sample Narrative:
L1517739-08 WG1900474: Dilution due to matrix.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 31 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 31 of 84
====================----□ □ □ □
□ □ □ □
SAMPLE RESULTS - 09
L1517739
USTG480-MW20
Collected date/time: 07/20/22 13:01
Volatile Petroleum Hydrocarbons by Method MADEPV
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics C5-C8 ALI
UNADJ 439 J 333 670 1000 10 07/30/2022 06:48 WG1902102
Unadjusted C9-C12 Aliphatics C9-C12 ALI
UNADJ 1420 B 333 670 1340 10 07/30/2022 06:48 WG1902102
Unadjusted C9-C10 Aromatics C9-C10 ARO
UNADJ 1160 333 670 1000 10 07/30/2022 06:48 WG1902102
Total VPH VPH 3020 667 1500 3000 10 07/30/2022 06:48 WG1902102
(S) 2,5-Dibromotoluene(FID)615-59-8 110 70.0-130 07/30/2022 06:48 WG1902102
(S) 2,5-Dibromotoluene(PID)615-59-8 102 70.0-130 07/30/2022 06:48 WG1902102
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acetone 67-64-1 542 Q 113 250 500 10 08/04/2022 02:41 WG1905109
Acrolein 107-02-8 250 C4 U 25.4 250 500 10 07/25/2022 23:04 WG1900597
Acrylonitrile 107-13-1 50.0 J4 U 6.71 50.0 100 10 07/25/2022 23:04 WG1900597
Benzene 71-43-2 61.1 0.941 5.00 10.0 10 07/25/2022 23:04 WG1900597
Bromobenzene 108-86-1 5.00 U 1.18 5.00 10.0 10 07/25/2022 23:04 WG1900597
Bromodichloromethane 75-27-4 5.00 U 1.36 5.00 10.0 10 07/25/2022 23:04 WG1900597
Bromoform 75-25-2 5.00 U 1.29 5.00 10.0 10 07/25/2022 23:04 WG1900597
Bromomethane 74-83-9 20.0 U 6.05 20.0 50.0 10 07/25/2022 23:04 WG1900597
n-Butylbenzene 104-51-8 5.99 J 1.57 5.00 10.0 10 07/25/2022 23:04 WG1900597
sec-Butylbenzene 135-98-8 7.59 J 1.25 5.00 10.0 10 07/25/2022 23:04 WG1900597
tert-Butylbenzene 98-06-6 1.64 J 1.27 5.00 10.0 10 07/25/2022 23:04 WG1900597
Carbon tetrachloride 56-23-5 5.00 U 1.28 5.00 10.0 10 07/25/2022 23:04 WG1900597
Chlorobenzene 108-90-7 5.00 U 1.16 5.00 10.0 10 07/25/2022 23:04 WG1900597
Chlorodibromomethane 124-48-1 5.00 U 1.40 5.00 10.0 10 07/25/2022 23:04 WG1900597
Chloroethane 75-00-3 20.0 U 1.92 20.0 50.0 10 07/25/2022 23:04 WG1900597
Chloroform 67-66-3 20.0 U 1.11 20.0 50.0 10 07/25/2022 23:04 WG1900597
Chloromethane 74-87-3 20.0 U 9.60 20.0 40.0 10 07/25/2022 23:04 WG1900597
2-Chlorotoluene 95-49-8 5.00 U 1.06 5.00 10.0 10 07/25/2022 23:04 WG1900597
4-Chlorotoluene 106-43-4 5.00 U 1.14 5.00 10.0 10 07/25/2022 23:04 WG1900597
1,2-Dibromo-3-Chloropropane 96-12-8 20.0 U 2.76 20.0 50.0 10 07/25/2022 23:04 WG1900597
1,2-Dibromoethane 106-93-4 5.00 U 1.26 5.00 10.0 10 07/25/2022 23:04 WG1900597
Dibromomethane 74-95-3 5.00 U 1.22 5.00 10.0 10 07/25/2022 23:04 WG1900597
1,2-Dichlorobenzene 95-50-1 5.00 U 1.07 5.00 10.0 10 07/25/2022 23:04 WG1900597
1,3-Dichlorobenzene 541-73-1 5.00 U 1.10 5.00 10.0 10 07/25/2022 23:04 WG1900597
1,4-Dichlorobenzene 106-46-7 5.00 U 1.20 5.00 10.0 10 07/25/2022 23:04 WG1900597
Dichlorodifluoromethane 75-71-8 20.0 U 3.74 20.0 50.0 10 07/25/2022 23:04 WG1900597
1,1-Dichloroethane 75-34-3 5.00 U 1.00 5.00 10.0 10 07/25/2022 23:04 WG1900597
1,2-Dichloroethane 107-06-2 5.00 U 0.819 5.00 10.0 10 07/25/2022 23:04 WG1900597
1,1-Dichloroethene 75-35-4 5.00 U 1.88 5.00 10.0 10 07/25/2022 23:04 WG1900597
cis-1,2-Dichloroethene 156-59-2 5.00 U 1.26 5.00 10.0 10 07/25/2022 23:04 WG1900597
trans-1,2-Dichloroethene 156-60-5 5.00 U 1.49 5.00 10.0 10 07/25/2022 23:04 WG1900597
1,2-Dichloropropane 78-87-5 5.00 U 1.49 5.00 10.0 10 07/25/2022 23:04 WG1900597
1,1-Dichloropropene 563-58-6 5.00 U 1.42 5.00 10.0 10 07/25/2022 23:04 WG1900597
1,3-Dichloropropane 142-28-9 5.00 U 1.10 5.00 10.0 10 07/25/2022 23:04 WG1900597
2,2-Dichloropropane 594-20-7 5.00 U 1.61 5.00 10.0 10 07/25/2022 23:04 WG1900597
Di-isopropyl ether 108-20-3 5.00 U 1.05 5.00 10.0 10 07/25/2022 23:04 WG1900597
Ethylbenzene 100-41-4 156 1.37 5.00 10.0 10 07/25/2022 23:04 WG1900597
Hexachloro-1,3-butadiene 87-68-3 7.50 J3 U 3.37 7.50 15.0 10 07/25/2022 23:04 WG1900597
Isopropylbenzene 98-82-8 25.8 1.05 5.00 10.0 10 07/25/2022 23:04 WG1900597
p-Isopropyltoluene 99-87-6 7.43 J 1.20 5.00 10.0 10 07/25/2022 23:04 WG1900597
2-Butanone (MEK)78-93-3 23.7 J 11.9 50.0 100 10 07/25/2022 23:04 WG1900597
Methylene Chloride 75-09-2 20.0 U 4.30 20.0 50.0 10 07/25/2022 23:04 WG1900597
4-Methyl-2-pentanone (MIBK)108-10-1 50.0 U 4.78 50.0 100 10 07/25/2022 23:04 WG1900597
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 32 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 32 of 84
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==============~~~~~=----□ □ □ □
SAMPLE RESULTS - 09
L1517739
USTG480-MW20
Collected date/time: 07/20/22 13:01
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Methyl tert-butyl ether 1634-04-4 5.00 U 1.01 5.00 10.0 10 07/25/2022 23:04 WG1900597
Naphthalene 91-20-3 479 10.0 20.0 50.0 10 07/25/2022 23:04 WG1900597
n-Propylbenzene 103-65-1 39.8 0.993 5.00 10.0 10 07/25/2022 23:04 WG1900597
Styrene 100-42-5 5.00 U 1.18 5.00 10.0 10 07/25/2022 23:04 WG1900597
1,1,1,2-Tetrachloroethane 630-20-6 5.00 U 1.47 5.00 10.0 10 07/25/2022 23:04 WG1900597
1,1,2,2-Tetrachloroethane 79-34-5 5.00 U 1.33 5.00 10.0 10 07/25/2022 23:04 WG1900597
Tetrachloroethene 127-18-4 6.00 U 3.00 6.00 12.0 10 07/25/2022 23:04 WG1900597
Toluene 108-88-3 5.01 J 2.78 6.00 12.0 10 07/25/2022 23:04 WG1900597
1,2,3-Trichlorobenzene 87-61-6 5.00 U 2.30 5.00 10.0 10 07/25/2022 23:04 WG1900597
1,2,4-Trichlorobenzene 120-82-1 10.0 U 4.81 10.0 20.0 10 07/25/2022 23:04 WG1900597
1,1,1-Trichloroethane 71-55-6 5.00 U 1.49 5.00 10.0 10 07/25/2022 23:04 WG1900597
1,1,2-Trichloroethane 79-00-5 5.00 U 1.58 5.00 10.0 10 07/25/2022 23:04 WG1900597
Trichloroethene 79-01-6 5.00 U 1.90 5.00 10.0 10 07/25/2022 23:04 WG1900597
Trichlorofluoromethane 75-69-4 20.0 U 1.60 20.0 50.0 10 07/25/2022 23:04 WG1900597
1,2,3-Trichloropropane 96-18-4 10.0 U 2.37 10.0 25.0 10 07/25/2022 23:04 WG1900597
1,2,4-Trimethylbenzene 95-63-6 194 3.22 10.0 20.0 10 07/25/2022 23:04 WG1900597
1,3,5-Trimethylbenzene 108-67-8 66.6 1.04 5.00 10.0 10 07/25/2022 23:04 WG1900597
Vinyl chloride 75-01-4 5.00 U 2.34 5.00 10.0 10 07/25/2022 23:04 WG1900597
o-Xylene 95-47-6 60.1 1.74 5.00 10.0 10 07/25/2022 23:04 WG1900597
m&p-Xylenes 1330-20-7 153 4.30 10.0 20.0 10 07/25/2022 23:04 WG1900597
(S) Toluene-d8 2037-26-5 99.2 89.0-112 07/25/2022 23:04 WG1900597
(S) Toluene-d8 2037-26-5 104 89.0-112 08/04/2022 02:41 WG1905109
(S) 4-Bromofluorobenzene 460-00-4 103 85.0-114 07/25/2022 23:04 WG1900597
(S) 4-Bromofluorobenzene 460-00-4 99.6 85.0-114 08/04/2022 02:41 WG1905109
(S) 1,2-Dichloroethane-d4 17060-07-0 110 81.0-118 07/25/2022 23:04 WG1900597
(S) 1,2-Dichloroethane-d4 17060-07-0 86.3 81.0-118 08/04/2022 02:41 WG1905109
TPH by Method MADEPE
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics C9-C18 ALI
UNADJ 1200 33.3 67.0 134 1 08/03/2022 04:39 WG1904482
Unadjusted C19-C36 Aliphatics C19-C36 ALI
UNADJ 198 B 33.3 67.0 134 1 08/03/2022 04:39 WG1904482
Unadjusted C11-C22 Aromatics C11-C22 ARO
UNADJ 1600 33.3 67.0 134 1 08/03/2022 10:03 WG1904482
Unadjusted Total Petroleum
Hydrocarbons TPH UNADJ 3000 33.3 67.0 134 1 08/03/2022 10:03 WG1904482
(S) o-Terphenyl 84-15-1 66.4 40.0-140 08/03/2022 10:03 WG1904482
(S) 1-Chloro-octadecane 3386-33-2 54.5 40.0-140 08/03/2022 04:39 WG1904482
(S) 2-Fluorobiphenyl 321-60-8 78.4 40.0-140 08/03/2022 10:03 WG1904482
(S) 2-Bromonaphthalene 580-13-2 72.0 40.0-140 08/03/2022 10:03 WG1904482
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acenaphthene 83-32-9 2.58 J 0.443 2.50 5.00 5 08/01/2022 20:52 WG1900474
Acenaphthylene 208-96-8 2.50 U 0.461 2.50 5.00 5 08/01/2022 20:52 WG1900474
Anthracene 120-12-7 0.594 J J4 0.402 2.50 5.00 5 08/01/2022 20:52 WG1900474
Benzidine 92-87-5 37.5 J4 U 18.7 37.5 75.0 5 08/01/2022 20:52 WG1900474
Benzo(a)anthracene 56-55-3 2.50 U 0.995 2.50 5.00 5 08/01/2022 20:52 WG1900474
Benzo(b)fluoranthene 205-99-2 2.50 U 0.650 2.50 5.00 5 08/01/2022 20:52 WG1900474
Benzo(k)fluoranthene 207-08-9 2.50 U 0.600 2.50 5.00 5 08/01/2022 20:52 WG1900474
Benzo(g,h,i)perylene 191-24-2 2.50 U 0.605 2.50 5.00 5 08/01/2022 20:52 WG1900474
Benzo(a)pyrene 50-32-8 2.50 U 0.191 2.50 5.00 5 08/01/2022 20:52 WG1900474
Bis(2-chlorethoxy)methane 111-91-1 25.0 J4 U 0.580 25.0 50.0 5 08/01/2022 20:52 WG1900474
Bis(2-chloroethyl)ether 111-44-4 25.0 J4 U 0.685 25.0 50.0 5 08/01/2022 20:52 WG1900474
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 33 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 33 of 84
====================----□ □ □ □
□ □ □ □
SAMPLE RESULTS - 09
L1517739
USTG480-MW20
Collected date/time: 07/20/22 13:01
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
2,2-Oxybis(1-Chloropropane)108-60-1 25.0 J4 U 1.05 25.0 50.0 5 08/01/2022 20:52 WG1900474
4-Bromophenyl-phenylether 101-55-3 25.0 U 0.439 25.0 50.0 5 08/01/2022 20:52 WG1900474
2-Chloronaphthalene 91-58-7 2.50 U 0.324 2.50 5.00 5 08/01/2022 20:52 WG1900474
4-Chlorophenyl-phenylether 7005-72-3 25.0 U 0.463 25.0 50.0 5 08/01/2022 20:52 WG1900474
Chrysene 218-01-9 2.50 U 0.650 2.50 5.00 5 08/01/2022 20:52 WG1900474
Dibenz(a,h)anthracene 53-70-3 2.50 U 0.322 2.50 5.00 5 08/01/2022 20:52 WG1900474
3,3-Dichlorobenzidine 91-94-1 25.0 U 1.06 25.0 50.0 5 08/01/2022 20:52 WG1900474
2,4-Dinitrotoluene 121-14-2 25.0 U 0.491 25.0 50.0 5 08/01/2022 20:52 WG1900474
2,6-Dinitrotoluene 606-20-2 25.0 J4 U 1.25 25.0 50.0 5 08/01/2022 20:52 WG1900474
Fluoranthene 206-44-0 2.50 J4 U 0.510 2.50 5.00 5 08/01/2022 20:52 WG1900474
Fluorene 86-73-7 4.08 J 0.422 2.50 5.00 5 08/01/2022 20:52 WG1900474
Hexachlorobenzene 118-74-1 2.50 U 0.378 2.50 5.00 5 08/01/2022 20:52 WG1900474
Hexachloro-1,3-butadiene 87-68-3 25.0 U 0.484 25.0 50.0 5 08/01/2022 20:52 WG1900474
Hexachlorocyclopentadiene 77-47-4 25.0 C6 U 0.299 25.0 50.0 5 08/01/2022 20:52 WG1900474
Hexachloroethane 67-72-1 25.0 U 0.635 25.0 50.0 5 08/01/2022 20:52 WG1900474
Indeno(1,2,3-cd)pyrene 193-39-5 3.00 U 1.40 3.00 6.00 5 08/01/2022 20:52 WG1900474
Isophorone 78-59-1 25.0 U 0.715 25.0 50.0 5 08/01/2022 20:52 WG1900474
Naphthalene 91-20-3 99.5 J4 0.795 2.50 5.00 5 08/01/2022 20:52 WG1900474
Nitrobenzene 98-95-3 25.0 J4 U 1.48 25.0 50.0 5 08/01/2022 20:52 WG1900474
n-Nitrosodimethylamine 62-75-9 25.0 U 4.99 25.0 50.0 5 08/01/2022 20:52 WG1900474
n-Nitrosodiphenylamine 86-30-6 25.0 U 11.9 25.0 50.0 5 08/01/2022 20:52 WG1900474
n-Nitrosodi-n-propylamine 621-64-7 25.0 J4 U 1.31 25.0 50.0 5 08/01/2022 20:52 WG1900474
Phenanthrene 85-01-8 4.35 J J4 0.560 2.50 5.00 5 08/01/2022 20:52 WG1900474
Benzylbutyl phthalate 85-68-7 10.0 U 3.83 10.0 20.0 5 08/01/2022 20:52 WG1900474
Bis(2-ethylhexyl)phthalate 117-81-7 10.0 J4 U 4.48 10.0 20.0 5 08/01/2022 20:52 WG1900474
Di-n-butyl phthalate 84-74-2 7.50 J4 U 2.27 7.50 15.0 5 08/01/2022 20:52 WG1900474
Diethyl phthalate 84-66-2 7.50 J4 U 1.43 7.50 15.0 5 08/01/2022 20:52 WG1900474
Dimethyl phthalate 131-11-3 7.50 U 1.30 7.50 15.0 5 08/01/2022 20:52 WG1900474
Di-n-octyl phthalate 117-84-0 10.0 U 4.66 10.0 20.0 5 08/01/2022 20:52 WG1900474
Pyrene 129-00-0 2.50 J4 U 0.535 2.50 5.00 5 08/01/2022 20:52 WG1900474
1,2,4-Trichlorobenzene 120-82-1 25.0 U 0.349 25.0 50.0 5 08/01/2022 20:52 WG1900474
4-Chloro-3-methylphenol 59-50-7 25.0 J4 U 0.655 25.0 50.0 5 08/01/2022 20:52 WG1900474
2-Chlorophenol 95-57-8 25.0 J4 U 0.665 25.0 50.0 5 08/01/2022 20:52 WG1900474
2,4-Dichlorophenol 120-83-2 25.0 J4 U 0.510 25.0 50.0 5 08/01/2022 20:52 WG1900474
2,4-Dimethylphenol 105-67-9 25.0 U 0.318 25.0 50.0 5 08/01/2022 20:52 WG1900474
4,6-Dinitro-2-methylphenol 534-52-1 25.0 U 5.60 25.0 50.0 5 08/01/2022 20:52 WG1900474
2,4-Dinitrophenol 51-28-5 75.0 U 29.7 75.0 150 5 08/01/2022 20:52 WG1900474
2-Nitrophenol 88-75-5 25.0 J4 U 0.585 25.0 50.0 5 08/01/2022 20:52 WG1900474
4-Nitrophenol 100-02-7 25.0 U 0.715 25.0 50.0 5 08/01/2022 20:52 WG1900474
Pentachlorophenol 87-86-5 25.0 U 1.57 25.0 50.0 5 08/01/2022 20:52 WG1900474
Phenol 108-95-2 50.0 U 21.7 50.0 100 5 08/01/2022 20:52 WG1900474
2,4,6-Trichlorophenol 88-06-2 25.0 U 0.500 25.0 50.0 5 08/01/2022 20:52 WG1900474
1-Methylnaphthalene 90-12-0 82.7 0.395 2.50 5.00 5 08/01/2022 20:52 WG1900474
2-Methylnaphthalene 91-57-6 94.5 0.585 2.50 5.00 5 08/01/2022 20:52 WG1900474
(S) Nitrobenzene-d5 4165-60-0 44.4 0.000 44.0-120 08/01/2022 20:52 WG1900474
(S) 2-Fluorobiphenyl 321-60-8 46.7 0.000 44.0-119 08/01/2022 20:52 WG1900474
(S) p-Terphenyl-d14 1718-51-0 61.6 0.000 50.0-134 08/01/2022 20:52 WG1900474
(S) Phenol-d5 4165-62-2 22.2 0.000 10.0-67.0 08/01/2022 20:52 WG1900474
(S) 2-Fluorophenol 367-12-4 20.1 0.000 19.0-119 08/01/2022 20:52 WG1900474
(S) 2,4,6-Tribromophenol 118-79-6 67.5 0.000 43.0-140 08/01/2022 20:52 WG1900474
Sample Narrative:
L1517739-09 WG1900474: Dilution due to matrix.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 34 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 34 of 84
====================----□ □ □ □
□ □ □ □
SAMPLE RESULTS - 10
L1517739
USTG480-MW29
Collected date/time: 07/20/22 13:35
Volatile Petroleum Hydrocarbons by Method MADEPV
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics C5-C8 ALI
UNADJ 554 33.3 67.0 134 1 07/31/2022 14:13 WG1903095
Unadjusted C9-C12 Aliphatics C9-C12 ALI
UNADJ 692 33.3 67.0 134 1 07/31/2022 14:13 WG1903095
Unadjusted C9-C10 Aromatics C9-C10 ARO
UNADJ 778 33.3 67.0 134 1 07/31/2022 14:13 WG1903095
Total VPH VPH 2020 66.7 150 300 1 07/31/2022 14:13 WG1903095
(S) 2,5-Dibromotoluene(FID)615-59-8 144 J1 70.0-130 07/31/2022 14:13 WG1903095
(S) 2,5-Dibromotoluene(PID)615-59-8 82.8 70.0-130 07/31/2022 14:13 WG1903095
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acetone 67-64-1 25.0 J3 U 11.3 25.0 50.0 1 07/25/2022 19:33 WG1900597
Acrolein 107-02-8 25.0 C4 U 2.54 25.0 50.0 1 07/25/2022 19:33 WG1900597
Acrylonitrile 107-13-1 5.00 J4 U 0.671 5.00 10.0 1 07/25/2022 19:33 WG1900597
Benzene 71-43-2 540 Q 1.88 10.0 20.0 20 08/04/2022 03:02 WG1905109
Bromobenzene 108-86-1 0.500 U 0.118 0.500 1.00 1 07/25/2022 19:33 WG1900597
Bromodichloromethane 75-27-4 0.500 U 0.136 0.500 1.00 1 07/25/2022 19:33 WG1900597
Bromoform 75-25-2 0.500 U 0.129 0.500 1.00 1 07/25/2022 19:33 WG1900597
Bromomethane 74-83-9 2.00 U 0.605 2.00 5.00 1 07/25/2022 19:33 WG1900597
n-Butylbenzene 104-51-8 17.8 0.157 0.500 1.00 1 07/25/2022 19:33 WG1900597
sec-Butylbenzene 135-98-8 18.8 0.125 0.500 1.00 1 07/25/2022 19:33 WG1900597
tert-Butylbenzene 98-06-6 1.51 0.127 0.500 1.00 1 07/25/2022 19:33 WG1900597
Carbon tetrachloride 56-23-5 0.500 U 0.128 0.500 1.00 1 07/25/2022 19:33 WG1900597
Chlorobenzene 108-90-7 0.500 U 0.116 0.500 1.00 1 07/25/2022 19:33 WG1900597
Chlorodibromomethane 124-48-1 0.500 U 0.140 0.500 1.00 1 07/25/2022 19:33 WG1900597
Chloroethane 75-00-3 2.00 U 0.192 2.00 5.00 1 07/25/2022 19:33 WG1900597
Chloroform 67-66-3 2.00 U 0.111 2.00 5.00 1 07/25/2022 19:33 WG1900597
Chloromethane 74-87-3 2.00 U 0.960 2.00 4.00 1 07/25/2022 19:33 WG1900597
2-Chlorotoluene 95-49-8 0.500 U 0.106 0.500 1.00 1 07/25/2022 19:33 WG1900597
4-Chlorotoluene 106-43-4 0.500 U 0.114 0.500 1.00 1 07/25/2022 19:33 WG1900597
1,2-Dibromo-3-Chloropropane 96-12-8 2.00 U 0.276 2.00 5.00 1 07/25/2022 19:33 WG1900597
1,2-Dibromoethane 106-93-4 0.500 U 0.126 0.500 1.00 1 07/25/2022 19:33 WG1900597
Dibromomethane 74-95-3 0.500 U 0.122 0.500 1.00 1 07/25/2022 19:33 WG1900597
1,2-Dichlorobenzene 95-50-1 0.500 U 0.107 0.500 1.00 1 07/25/2022 19:33 WG1900597
1,3-Dichlorobenzene 541-73-1 0.500 U 0.110 0.500 1.00 1 07/25/2022 19:33 WG1900597
1,4-Dichlorobenzene 106-46-7 0.500 U 0.120 0.500 1.00 1 07/25/2022 19:33 WG1900597
Dichlorodifluoromethane 75-71-8 2.00 U 0.374 2.00 5.00 1 07/25/2022 19:33 WG1900597
1,1-Dichloroethane 75-34-3 0.500 U 0.100 0.500 1.00 1 07/25/2022 19:33 WG1900597
1,2-Dichloroethane 107-06-2 0.500 U 0.0819 0.500 1.00 1 07/25/2022 19:33 WG1900597
1,1-Dichloroethene 75-35-4 0.500 U 0.188 0.500 1.00 1 07/25/2022 19:33 WG1900597
cis-1,2-Dichloroethene 156-59-2 5.69 0.126 0.500 1.00 1 07/25/2022 19:33 WG1900597
trans-1,2-Dichloroethene 156-60-5 0.500 U 0.149 0.500 1.00 1 07/25/2022 19:33 WG1900597
1,2-Dichloropropane 78-87-5 0.500 U 0.149 0.500 1.00 1 07/25/2022 19:33 WG1900597
1,1-Dichloropropene 563-58-6 0.500 U 0.142 0.500 1.00 1 07/25/2022 19:33 WG1900597
1,3-Dichloropropane 142-28-9 0.500 U 0.110 0.500 1.00 1 07/25/2022 19:33 WG1900597
2,2-Dichloropropane 594-20-7 0.500 U 0.161 0.500 1.00 1 07/25/2022 19:33 WG1900597
Di-isopropyl ether 108-20-3 3.74 0.105 0.500 1.00 1 07/25/2022 19:33 WG1900597
Ethylbenzene 100-41-4 173 Q 2.74 10.0 20.0 20 08/04/2022 03:02 WG1905109
Hexachloro-1,3-butadiene 87-68-3 0.750 J3 U 0.337 0.750 1.50 1 07/25/2022 19:33 WG1900597
Isopropylbenzene 98-82-8 81.6 0.105 0.500 1.00 1 07/25/2022 19:33 WG1900597
p-Isopropyltoluene 99-87-6 4.68 0.120 0.500 1.00 1 07/25/2022 19:33 WG1900597
2-Butanone (MEK)78-93-3 5.00 U 1.19 5.00 10.0 1 07/25/2022 19:33 WG1900597
Methylene Chloride 75-09-2 2.00 U 0.430 2.00 5.00 1 07/25/2022 19:33 WG1900597
4-Methyl-2-pentanone (MIBK)108-10-1 5.00 U 0.478 5.00 10.0 1 07/25/2022 19:33 WG1900597
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 35 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 35 of 84
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SAMPLE RESULTS - 10
L1517739
USTG480-MW29
Collected date/time: 07/20/22 13:35
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Methyl tert-butyl ether 1634-04-4 0.500 U 0.101 0.500 1.00 1 07/25/2022 19:33 WG1900597
Naphthalene 91-20-3 923 Q 20.0 40.0 100 20 08/04/2022 03:02 WG1905109
n-Propylbenzene 103-65-1 157 Q 1.99 10.0 20.0 20 08/04/2022 03:02 WG1905109
Styrene 100-42-5 0.500 U 0.118 0.500 1.00 1 07/25/2022 19:33 WG1900597
1,1,1,2-Tetrachloroethane 630-20-6 0.500 U 0.147 0.500 1.00 1 07/25/2022 19:33 WG1900597
1,1,2,2-Tetrachloroethane 79-34-5 0.500 U 0.133 0.500 1.00 1 07/25/2022 19:33 WG1900597
Tetrachloroethene 127-18-4 0.600 U 0.300 0.600 1.20 1 07/25/2022 19:33 WG1900597
Toluene 108-88-3 3.33 0.278 0.600 1.20 1 07/25/2022 19:33 WG1900597
1,2,3-Trichlorobenzene 87-61-6 0.500 U 0.230 0.500 1.00 1 07/25/2022 19:33 WG1900597
1,2,4-Trichlorobenzene 120-82-1 1.00 U 0.481 1.00 2.00 1 07/25/2022 19:33 WG1900597
1,1,1-Trichloroethane 71-55-6 0.500 U 0.149 0.500 1.00 1 07/25/2022 19:33 WG1900597
1,1,2-Trichloroethane 79-00-5 0.500 U 0.158 0.500 1.00 1 07/25/2022 19:33 WG1900597
Trichloroethene 79-01-6 0.500 U 0.190 0.500 1.00 1 07/25/2022 19:33 WG1900597
Trichlorofluoromethane 75-69-4 2.00 U 0.160 2.00 5.00 1 07/25/2022 19:33 WG1900597
1,2,3-Trichloropropane 96-18-4 1.00 U 0.237 1.00 2.50 1 07/25/2022 19:33 WG1900597
1,2,4-Trimethylbenzene 95-63-6 9.31 0.322 1.00 2.00 1 07/25/2022 19:33 WG1900597
1,3,5-Trimethylbenzene 108-67-8 0.670 J 0.104 0.500 1.00 1 07/25/2022 19:33 WG1900597
Vinyl chloride 75-01-4 9.53 J Q 4.68 10.0 20.0 20 08/04/2022 03:02 WG1905109
o-Xylene 95-47-6 3.19 0.174 0.500 1.00 1 07/25/2022 19:33 WG1900597
m&p-Xylenes 1330-20-7 14.9 0.430 1.00 2.00 1 07/25/2022 19:33 WG1900597
(S) Toluene-d8 2037-26-5 97.4 89.0-112 07/25/2022 19:33 WG1900597
(S) Toluene-d8 2037-26-5 106 89.0-112 08/04/2022 03:02 WG1905109
(S) 4-Bromofluorobenzene 460-00-4 103 85.0-114 07/25/2022 19:33 WG1900597
(S) 4-Bromofluorobenzene 460-00-4 106 85.0-114 08/04/2022 03:02 WG1905109
(S) 1,2-Dichloroethane-d4 17060-07-0 101 81.0-118 07/25/2022 19:33 WG1900597
(S) 1,2-Dichloroethane-d4 17060-07-0 86.0 81.0-118 08/04/2022 03:02 WG1905109
TPH by Method MADEPE
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics C9-C18 ALI
UNADJ 72.1 J 33.3 67.0 134 1 08/03/2022 05:02 WG1904482
Unadjusted C19-C36 Aliphatics C19-C36 ALI
UNADJ 38.1 B J 33.3 67.0 134 1 08/03/2022 05:02 WG1904482
Unadjusted C11-C22 Aromatics C11-C22 ARO
UNADJ 1610 33.3 67.0 134 1 08/03/2022 10:27 WG1904482
Unadjusted Total Petroleum
Hydrocarbons TPH UNADJ 1720 33.3 67.0 134 1 08/03/2022 10:27 WG1904482
(S) o-Terphenyl 84-15-1 66.3 40.0-140 08/03/2022 10:27 WG1904482
(S) 1-Chloro-octadecane 3386-33-2 65.3 40.0-140 08/03/2022 05:02 WG1904482
(S) 2-Fluorobiphenyl 321-60-8 82.3 40.0-140 08/03/2022 10:27 WG1904482
(S) 2-Bromonaphthalene 580-13-2 73.0 40.0-140 08/03/2022 10:27 WG1904482
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acenaphthene 83-32-9 3.69 0.0886 0.500 1.00 1 07/27/2022 21:06 WG1900474
Acenaphthylene 208-96-8 0.500 U 0.0921 0.500 1.00 1 07/27/2022 21:06 WG1900474
Anthracene 120-12-7 0.395 J J4 0.0804 0.500 1.00 1 07/27/2022 21:06 WG1900474
Benzidine 92-87-5 7.50 J4 U 3.74 7.50 15.0 1 07/27/2022 21:06 WG1900474
Benzo(a)anthracene 56-55-3 0.500 U 0.199 0.500 1.00 1 07/27/2022 21:06 WG1900474
Benzo(b)fluoranthene 205-99-2 0.500 U 0.130 0.500 1.00 1 07/27/2022 21:06 WG1900474
Benzo(k)fluoranthene 207-08-9 0.500 U 0.120 0.500 1.00 1 07/27/2022 21:06 WG1900474
Benzo(g,h,i)perylene 191-24-2 0.500 U 0.121 0.500 1.00 1 07/27/2022 21:06 WG1900474
Benzo(a)pyrene 50-32-8 0.500 U 0.0381 0.500 1.00 1 07/27/2022 21:06 WG1900474
Bis(2-chlorethoxy)methane 111-91-1 5.00 J4 U 0.116 5.00 10.0 1 07/27/2022 21:06 WG1900474
Bis(2-chloroethyl)ether 111-44-4 5.00 J4 U 0.137 5.00 10.0 1 07/27/2022 21:06 WG1900474
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 36 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 36 of 84
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SAMPLE RESULTS - 10
L1517739
USTG480-MW29
Collected date/time: 07/20/22 13:35
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
2,2-Oxybis(1-Chloropropane)108-60-1 5.00 J4 U 0.210 5.00 10.0 1 07/27/2022 21:06 WG1900474
4-Bromophenyl-phenylether 101-55-3 5.00 U 0.0877 5.00 10.0 1 07/27/2022 21:06 WG1900474
2-Chloronaphthalene 91-58-7 0.500 U 0.0648 0.500 1.00 1 07/27/2022 21:06 WG1900474
4-Chlorophenyl-phenylether 7005-72-3 5.00 U 0.0926 5.00 10.0 1 07/27/2022 21:06 WG1900474
Chrysene 218-01-9 0.500 U 0.130 0.500 1.00 1 07/27/2022 21:06 WG1900474
Dibenz(a,h)anthracene 53-70-3 0.500 U 0.0644 0.500 1.00 1 07/27/2022 21:06 WG1900474
3,3-Dichlorobenzidine 91-94-1 5.00 U 0.212 5.00 10.0 1 07/27/2022 21:06 WG1900474
2,4-Dinitrotoluene 121-14-2 5.00 U 0.0983 5.00 10.0 1 07/27/2022 21:06 WG1900474
2,6-Dinitrotoluene 606-20-2 5.00 J4 U 0.250 5.00 10.0 1 07/27/2022 21:06 WG1900474
Fluoranthene 206-44-0 0.500 J4 U 0.102 0.500 1.00 1 07/27/2022 21:06 WG1900474
Fluorene 86-73-7 4.84 0.0844 0.500 1.00 1 07/27/2022 21:06 WG1900474
Hexachlorobenzene 118-74-1 0.500 U 0.0755 0.500 1.00 1 07/27/2022 21:06 WG1900474
Hexachloro-1,3-butadiene 87-68-3 5.00 U 0.0968 5.00 10.0 1 07/27/2022 21:06 WG1900474
Hexachlorocyclopentadiene 77-47-4 5.00 U 0.0598 5.00 10.0 1 07/27/2022 21:06 WG1900474
Hexachloroethane 67-72-1 5.00 U 0.127 5.00 10.0 1 07/27/2022 21:06 WG1900474
Indeno(1,2,3-cd)pyrene 193-39-5 0.600 U 0.279 0.600 1.20 1 07/27/2022 21:06 WG1900474
Isophorone 78-59-1 5.00 U 0.143 5.00 10.0 1 07/27/2022 21:06 WG1900474
Naphthalene 91-20-3 185 J4 0.159 0.500 1.00 1 07/27/2022 21:06 WG1900474
Nitrobenzene 98-95-3 5.00 J4 U 0.297 5.00 10.0 1 07/27/2022 21:06 WG1900474
n-Nitrosodimethylamine 62-75-9 5.00 U 0.998 5.00 10.0 1 07/27/2022 21:06 WG1900474
n-Nitrosodiphenylamine 86-30-6 5.00 U 2.37 5.00 10.0 1 07/27/2022 21:06 WG1900474
n-Nitrosodi-n-propylamine 621-64-7 5.00 J4 U 0.261 5.00 10.0 1 07/27/2022 21:06 WG1900474
Phenanthrene 85-01-8 5.42 J4 0.112 0.500 1.00 1 07/27/2022 21:06 WG1900474
Benzylbutyl phthalate 85-68-7 2.00 U 0.765 2.00 4.00 1 07/27/2022 21:06 WG1900474
Bis(2-ethylhexyl)phthalate 117-81-7 2.00 J4 U 0.895 2.00 4.00 1 07/27/2022 21:06 WG1900474
Di-n-butyl phthalate 84-74-2 1.50 J4 U 0.453 1.50 3.00 1 07/27/2022 21:06 WG1900474
Diethyl phthalate 84-66-2 1.50 J4 U 0.287 1.50 3.00 1 07/27/2022 21:06 WG1900474
Dimethyl phthalate 131-11-3 1.50 U 0.260 1.50 3.00 1 07/27/2022 21:06 WG1900474
Di-n-octyl phthalate 117-84-0 2.00 U 0.932 2.00 4.00 1 07/27/2022 21:06 WG1900474
Pyrene 129-00-0 0.500 J4 U 0.107 0.500 1.00 1 07/27/2022 21:06 WG1900474
1,2,4-Trichlorobenzene 120-82-1 5.00 U 0.0698 5.00 10.0 1 07/27/2022 21:06 WG1900474
4-Chloro-3-methylphenol 59-50-7 5.00 J4 U 0.131 5.00 10.0 1 07/27/2022 21:06 WG1900474
2-Chlorophenol 95-57-8 5.00 J4 U 0.133 5.00 10.0 1 07/27/2022 21:06 WG1900474
2,4-Dichlorophenol 120-83-2 5.00 J4 U 0.102 5.00 10.0 1 07/27/2022 21:06 WG1900474
2,4-Dimethylphenol 105-67-9 5.00 U 0.0636 5.00 10.0 1 07/27/2022 21:06 WG1900474
4,6-Dinitro-2-methylphenol 534-52-1 5.00 U 1.12 5.00 10.0 1 07/27/2022 21:06 WG1900474
2,4-Dinitrophenol 51-28-5 15.0 U 5.93 15.0 30.0 1 07/27/2022 21:06 WG1900474
2-Nitrophenol 88-75-5 5.00 J4 U 0.117 5.00 10.0 1 07/27/2022 21:06 WG1900474
4-Nitrophenol 100-02-7 5.00 U 0.143 5.00 10.0 1 07/27/2022 21:06 WG1900474
Pentachlorophenol 87-86-5 5.00 U 0.313 5.00 10.0 1 07/27/2022 21:06 WG1900474
Phenol 108-95-2 10.0 U 4.33 10.0 20.0 1 07/27/2022 21:06 WG1900474
2,4,6-Trichlorophenol 88-06-2 5.00 U 0.100 5.00 10.0 1 07/27/2022 21:06 WG1900474
(S) Nitrobenzene-d5 4165-60-0 46.6 0.000 44.0-120 07/27/2022 21:06 WG1900474
(S) 2-Fluorobiphenyl 321-60-8 49.5 0.000 44.0-119 07/27/2022 21:06 WG1900474
(S) p-Terphenyl-d14 1718-51-0 60.4 0.000 50.0-134 07/27/2022 21:06 WG1900474
(S) Phenol-d5 4165-62-2 14.1 0.000 10.0-67.0 07/27/2022 21:06 WG1900474
(S) 2-Fluorophenol 367-12-4 22.9 0.000 19.0-119 07/27/2022 21:06 WG1900474
(S) 2,4,6-Tribromophenol 118-79-6 76.9 0.000 43.0-140 07/27/2022 21:06 WG1900474
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 37 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 37 of 84
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SAMPLE RESULTS - 11
L1517739
USTG480-MW07
Collected date/time: 07/20/22 13:45
Volatile Petroleum Hydrocarbons by Method MADEPV
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics C5-C8 ALI
UNADJ 336 33.3 67.0 134 1 07/31/2022 14:46 WG1903095
Unadjusted C9-C12 Aliphatics C9-C12 ALI
UNADJ 1230 33.3 67.0 134 1 07/31/2022 14:46 WG1903095
Unadjusted C9-C10 Aromatics C9-C10 ARO
UNADJ 1000 167 335 670 5 08/03/2022 09:35 WG1903796
Total VPH VPH 2570 B 333 750 1500 5 08/03/2022 09:35 WG1903796
(S) 2,5-Dibromotoluene(FID)615-59-8 146 J1 70.0-130 07/31/2022 14:46 WG1903095
(S) 2,5-Dibromotoluene(FID)615-59-8 101 70.0-130 08/03/2022 09:35 WG1903796
(S) 2,5-Dibromotoluene(PID)615-59-8 81.1 70.0-130 07/31/2022 14:46 WG1903095
(S) 2,5-Dibromotoluene(PID)615-59-8 88.0 70.0-130 08/03/2022 09:35 WG1903796
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acetone 67-64-1 25.0 J3 U 11.3 25.0 50.0 1 07/25/2022 19:55 WG1900597
Acrolein 107-02-8 25.0 C4 U 2.54 25.0 50.0 1 07/25/2022 19:55 WG1900597
Acrylonitrile 107-13-1 5.00 J4 U 0.671 5.00 10.0 1 07/25/2022 19:55 WG1900597
Benzene 71-43-2 63.5 Q 0.941 5.00 10.0 10 08/04/2022 03:24 WG1905109
Bromobenzene 108-86-1 0.500 U 0.118 0.500 1.00 1 07/25/2022 19:55 WG1900597
Bromodichloromethane 75-27-4 0.500 U 0.136 0.500 1.00 1 07/25/2022 19:55 WG1900597
Bromoform 75-25-2 0.500 U 0.129 0.500 1.00 1 07/25/2022 19:55 WG1900597
Bromomethane 74-83-9 2.00 U 0.605 2.00 5.00 1 07/25/2022 19:55 WG1900597
n-Butylbenzene 104-51-8 10.8 0.157 0.500 1.00 1 07/25/2022 19:55 WG1900597
sec-Butylbenzene 135-98-8 15.2 0.125 0.500 1.00 1 07/25/2022 19:55 WG1900597
tert-Butylbenzene 98-06-6 0.500 U 0.127 0.500 1.00 1 07/25/2022 19:55 WG1900597
Carbon tetrachloride 56-23-5 0.500 U 0.128 0.500 1.00 1 07/25/2022 19:55 WG1900597
Chlorobenzene 108-90-7 0.500 U 0.116 0.500 1.00 1 07/25/2022 19:55 WG1900597
Chlorodibromomethane 124-48-1 0.500 U 0.140 0.500 1.00 1 07/25/2022 19:55 WG1900597
Chloroethane 75-00-3 2.00 U 0.192 2.00 5.00 1 07/25/2022 19:55 WG1900597
Chloroform 67-66-3 2.00 U 0.111 2.00 5.00 1 07/25/2022 19:55 WG1900597
Chloromethane 74-87-3 2.00 U 0.960 2.00 4.00 1 07/25/2022 19:55 WG1900597
2-Chlorotoluene 95-49-8 0.500 U 0.106 0.500 1.00 1 07/25/2022 19:55 WG1900597
4-Chlorotoluene 106-43-4 0.500 U 0.114 0.500 1.00 1 07/25/2022 19:55 WG1900597
1,2-Dibromo-3-Chloropropane 96-12-8 2.00 U 0.276 2.00 5.00 1 07/25/2022 19:55 WG1900597
1,2-Dibromoethane 106-93-4 0.500 U 0.126 0.500 1.00 1 07/25/2022 19:55 WG1900597
Dibromomethane 74-95-3 0.500 U 0.122 0.500 1.00 1 07/25/2022 19:55 WG1900597
1,2-Dichlorobenzene 95-50-1 0.500 U 0.107 0.500 1.00 1 07/25/2022 19:55 WG1900597
1,3-Dichlorobenzene 541-73-1 0.500 U 0.110 0.500 1.00 1 07/25/2022 19:55 WG1900597
1,4-Dichlorobenzene 106-46-7 0.500 U 0.120 0.500 1.00 1 07/25/2022 19:55 WG1900597
Dichlorodifluoromethane 75-71-8 2.00 U 0.374 2.00 5.00 1 07/25/2022 19:55 WG1900597
1,1-Dichloroethane 75-34-3 0.500 U 0.100 0.500 1.00 1 07/25/2022 19:55 WG1900597
1,2-Dichloroethane 107-06-2 0.500 U 0.0819 0.500 1.00 1 07/25/2022 19:55 WG1900597
1,1-Dichloroethene 75-35-4 0.500 U 0.188 0.500 1.00 1 07/25/2022 19:55 WG1900597
cis-1,2-Dichloroethene 156-59-2 0.317 J 0.126 0.500 1.00 1 07/25/2022 19:55 WG1900597
trans-1,2-Dichloroethene 156-60-5 0.500 U 0.149 0.500 1.00 1 07/25/2022 19:55 WG1900597
1,2-Dichloropropane 78-87-5 0.500 U 0.149 0.500 1.00 1 07/25/2022 19:55 WG1900597
1,1-Dichloropropene 563-58-6 0.500 U 0.142 0.500 1.00 1 07/25/2022 19:55 WG1900597
1,3-Dichloropropane 142-28-9 0.500 U 0.110 0.500 1.00 1 07/25/2022 19:55 WG1900597
2,2-Dichloropropane 594-20-7 0.500 U 0.161 0.500 1.00 1 07/25/2022 19:55 WG1900597
Di-isopropyl ether 108-20-3 0.645 J 0.105 0.500 1.00 1 07/25/2022 19:55 WG1900597
Ethylbenzene 100-41-4 47.0 Q 1.37 5.00 10.0 10 08/04/2022 03:24 WG1905109
Hexachloro-1,3-butadiene 87-68-3 0.750 J3 U 0.337 0.750 1.50 1 07/25/2022 19:55 WG1900597
Isopropylbenzene 98-82-8 65.5 0.105 0.500 1.00 1 07/25/2022 19:55 WG1900597
p-Isopropyltoluene 99-87-6 11.7 0.120 0.500 1.00 1 07/25/2022 19:55 WG1900597
2-Butanone (MEK)78-93-3 5.00 U 1.19 5.00 10.0 1 07/25/2022 19:55 WG1900597
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 38 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 38 of 84
--------------=---□
□ □ □
□
======-=--=--=--=--=--=---=----=----=-----=-----=-----=-------=-~~ □ □ □
SAMPLE RESULTS - 11
L1517739
USTG480-MW07
Collected date/time: 07/20/22 13:45
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Methylene Chloride 75-09-2 2.00 U 0.430 2.00 5.00 1 07/25/2022 19:55 WG1900597
4-Methyl-2-pentanone (MIBK)108-10-1 5.00 U 0.478 5.00 10.0 1 07/25/2022 19:55 WG1900597
Methyl tert-butyl ether 1634-04-4 0.500 U 0.101 0.500 1.00 1 07/25/2022 19:55 WG1900597
Naphthalene 91-20-3 286 Q 10.0 20.0 50.0 10 08/04/2022 03:24 WG1905109
n-Propylbenzene 103-65-1 88.7 0.0993 0.500 1.00 1 07/25/2022 19:55 WG1900597
Styrene 100-42-5 0.500 U 0.118 0.500 1.00 1 07/25/2022 19:55 WG1900597
1,1,1,2-Tetrachloroethane 630-20-6 0.500 U 0.147 0.500 1.00 1 07/25/2022 19:55 WG1900597
1,1,2,2-Tetrachloroethane 79-34-5 0.500 U 0.133 0.500 1.00 1 07/25/2022 19:55 WG1900597
Tetrachloroethene 127-18-4 0.600 U 0.300 0.600 1.20 1 07/25/2022 19:55 WG1900597
Toluene 108-88-3 0.734 J 0.278 0.600 1.20 1 07/25/2022 19:55 WG1900597
1,2,3-Trichlorobenzene 87-61-6 0.500 U 0.230 0.500 1.00 1 07/25/2022 19:55 WG1900597
1,2,4-Trichlorobenzene 120-82-1 1.00 U 0.481 1.00 2.00 1 07/25/2022 19:55 WG1900597
1,1,1-Trichloroethane 71-55-6 0.500 U 0.149 0.500 1.00 1 07/25/2022 19:55 WG1900597
1,1,2-Trichloroethane 79-00-5 0.500 U 0.158 0.500 1.00 1 07/25/2022 19:55 WG1900597
Trichloroethene 79-01-6 0.500 U 0.190 0.500 1.00 1 07/25/2022 19:55 WG1900597
Trichlorofluoromethane 75-69-4 2.00 U 0.160 2.00 5.00 1 07/25/2022 19:55 WG1900597
1,2,3-Trichloropropane 96-18-4 1.00 U 0.237 1.00 2.50 1 07/25/2022 19:55 WG1900597
1,2,4-Trimethylbenzene 95-63-6 136 Q 3.22 10.0 20.0 10 08/04/2022 03:24 WG1905109
1,3,5-Trimethylbenzene 108-67-8 15.0 0.104 0.500 1.00 1 07/25/2022 19:55 WG1900597
Vinyl chloride 75-01-4 0.500 U 0.234 0.500 1.00 1 07/25/2022 19:55 WG1900597
o-Xylene 95-47-6 2.32 0.174 0.500 1.00 1 07/25/2022 19:55 WG1900597
m&p-Xylenes 1330-20-7 143 0.430 1.00 2.00 1 07/25/2022 19:55 WG1900597
(S) Toluene-d8 2037-26-5 97.5 89.0-112 07/25/2022 19:55 WG1900597
(S) Toluene-d8 2037-26-5 100 89.0-112 08/04/2022 03:24 WG1905109
(S) 4-Bromofluorobenzene 460-00-4 103 85.0-114 07/25/2022 19:55 WG1900597
(S) 4-Bromofluorobenzene 460-00-4 102 85.0-114 08/04/2022 03:24 WG1905109
(S) 1,2-Dichloroethane-d4 17060-07-0 104 81.0-118 07/25/2022 19:55 WG1900597
(S) 1,2-Dichloroethane-d4 17060-07-0 86.1 81.0-118 08/04/2022 03:24 WG1905109
TPH by Method MADEPE
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics C9-C18 ALI
UNADJ 335 33.3 67.0 134 1 08/03/2022 05:25 WG1904482
Unadjusted C19-C36 Aliphatics C19-C36 ALI
UNADJ 87.6 B J 33.3 67.0 134 1 08/03/2022 05:25 WG1904482
Unadjusted C11-C22 Aromatics C11-C22 ARO
UNADJ 1730 33.3 67.0 134 1 08/03/2022 10:50 WG1904482
Unadjusted Total Petroleum
Hydrocarbons TPH UNADJ 2150 33.3 67.0 134 1 08/03/2022 10:50 WG1904482
(S) o-Terphenyl 84-15-1 72.4 40.0-140 08/03/2022 10:50 WG1904482
(S) 1-Chloro-octadecane 3386-33-2 70.4 40.0-140 08/03/2022 05:25 WG1904482
(S) 2-Fluorobiphenyl 321-60-8 82.5 40.0-140 08/03/2022 10:50 WG1904482
(S) 2-Bromonaphthalene 580-13-2 72.3 40.0-140 08/03/2022 10:50 WG1904482
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acenaphthene 83-32-9 4.18 0.0886 0.500 1.00 1 07/27/2022 21:50 WG1900474
Acenaphthylene 208-96-8 0.500 U 0.0921 0.500 1.00 1 07/27/2022 21:50 WG1900474
Anthracene 120-12-7 0.500 J4 U 0.0804 0.500 1.00 1 07/27/2022 21:50 WG1900474
Benzidine 92-87-5 7.50 J4 U 3.74 7.50 15.0 1 07/27/2022 21:50 WG1900474
Benzo(a)anthracene 56-55-3 0.500 U 0.199 0.500 1.00 1 07/27/2022 21:50 WG1900474
Benzo(b)fluoranthene 205-99-2 0.500 U 0.130 0.500 1.00 1 07/27/2022 21:50 WG1900474
Benzo(k)fluoranthene 207-08-9 0.500 U 0.120 0.500 1.00 1 07/27/2022 21:50 WG1900474
Benzo(g,h,i)perylene 191-24-2 0.500 U 0.121 0.500 1.00 1 07/27/2022 21:50 WG1900474
Benzo(a)pyrene 50-32-8 0.500 U 0.0381 0.500 1.00 1 07/27/2022 21:50 WG1900474
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 39 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 39 of 84
====================----□ □ □ □
□ □ □ □
SAMPLE RESULTS - 11
L1517739
USTG480-MW07
Collected date/time: 07/20/22 13:45
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Bis(2-chlorethoxy)methane 111-91-1 5.00 J4 U 0.116 5.00 10.0 1 07/27/2022 21:50 WG1900474
Bis(2-chloroethyl)ether 111-44-4 5.00 J4 U 0.137 5.00 10.0 1 07/27/2022 21:50 WG1900474
2,2-Oxybis(1-Chloropropane)108-60-1 5.00 J4 U 0.210 5.00 10.0 1 07/27/2022 21:50 WG1900474
4-Bromophenyl-phenylether 101-55-3 5.00 U 0.0877 5.00 10.0 1 07/27/2022 21:50 WG1900474
2-Chloronaphthalene 91-58-7 0.500 U 0.0648 0.500 1.00 1 07/27/2022 21:50 WG1900474
4-Chlorophenyl-phenylether 7005-72-3 5.00 U 0.0926 5.00 10.0 1 07/27/2022 21:50 WG1900474
Chrysene 218-01-9 0.500 U 0.130 0.500 1.00 1 07/27/2022 21:50 WG1900474
Dibenz(a,h)anthracene 53-70-3 0.500 U 0.0644 0.500 1.00 1 07/27/2022 21:50 WG1900474
3,3-Dichlorobenzidine 91-94-1 5.00 U 0.212 5.00 10.0 1 07/27/2022 21:50 WG1900474
2,4-Dinitrotoluene 121-14-2 5.00 U 0.0983 5.00 10.0 1 07/27/2022 21:50 WG1900474
2,6-Dinitrotoluene 606-20-2 5.00 J4 U 0.250 5.00 10.0 1 07/27/2022 21:50 WG1900474
Fluoranthene 206-44-0 0.500 J4 U 0.102 0.500 1.00 1 07/27/2022 21:50 WG1900474
Fluorene 86-73-7 4.81 0.0844 0.500 1.00 1 07/27/2022 21:50 WG1900474
Hexachlorobenzene 118-74-1 0.500 U 0.0755 0.500 1.00 1 07/27/2022 21:50 WG1900474
Hexachloro-1,3-butadiene 87-68-3 5.00 U 0.0968 5.00 10.0 1 07/27/2022 21:50 WG1900474
Hexachlorocyclopentadiene 77-47-4 5.00 U 0.0598 5.00 10.0 1 07/27/2022 21:50 WG1900474
Hexachloroethane 67-72-1 5.00 U 0.127 5.00 10.0 1 07/27/2022 21:50 WG1900474
Indeno(1,2,3-cd)pyrene 193-39-5 0.600 U 0.279 0.600 1.20 1 07/27/2022 21:50 WG1900474
Isophorone 78-59-1 5.00 U 0.143 5.00 10.0 1 07/27/2022 21:50 WG1900474
Naphthalene 91-20-3 195 J4 0.159 0.500 1.00 1 07/27/2022 21:50 WG1900474
Nitrobenzene 98-95-3 5.00 J4 U 0.297 5.00 10.0 1 07/27/2022 21:50 WG1900474
n-Nitrosodimethylamine 62-75-9 5.00 U 0.998 5.00 10.0 1 07/27/2022 21:50 WG1900474
n-Nitrosodiphenylamine 86-30-6 5.00 U 2.37 5.00 10.0 1 07/27/2022 21:50 WG1900474
n-Nitrosodi-n-propylamine 621-64-7 5.00 J4 U 0.261 5.00 10.0 1 07/27/2022 21:50 WG1900474
Phenanthrene 85-01-8 4.16 J4 0.112 0.500 1.00 1 07/27/2022 21:50 WG1900474
Benzylbutyl phthalate 85-68-7 2.00 U 0.765 2.00 4.00 1 07/27/2022 21:50 WG1900474
Bis(2-ethylhexyl)phthalate 117-81-7 2.00 J4 U 0.895 2.00 4.00 1 07/27/2022 21:50 WG1900474
Di-n-butyl phthalate 84-74-2 1.50 J4 U 0.453 1.50 3.00 1 07/27/2022 21:50 WG1900474
Diethyl phthalate 84-66-2 1.50 J4 U 0.287 1.50 3.00 1 07/27/2022 21:50 WG1900474
Dimethyl phthalate 131-11-3 1.50 U 0.260 1.50 3.00 1 07/27/2022 21:50 WG1900474
Di-n-octyl phthalate 117-84-0 2.00 U 0.932 2.00 4.00 1 07/27/2022 21:50 WG1900474
Pyrene 129-00-0 0.500 J4 U 0.107 0.500 1.00 1 07/27/2022 21:50 WG1900474
1,2,4-Trichlorobenzene 120-82-1 5.00 U 0.0698 5.00 10.0 1 07/27/2022 21:50 WG1900474
4-Chloro-3-methylphenol 59-50-7 5.00 J4 U 0.131 5.00 10.0 1 07/27/2022 21:50 WG1900474
2-Chlorophenol 95-57-8 5.00 J4 U 0.133 5.00 10.0 1 07/27/2022 21:50 WG1900474
2,4-Dichlorophenol 120-83-2 5.00 J4 U 0.102 5.00 10.0 1 07/27/2022 21:50 WG1900474
2,4-Dimethylphenol 105-67-9 5.00 U 0.0636 5.00 10.0 1 07/27/2022 21:50 WG1900474
4,6-Dinitro-2-methylphenol 534-52-1 5.00 U 1.12 5.00 10.0 1 07/27/2022 21:50 WG1900474
2,4-Dinitrophenol 51-28-5 15.0 U 5.93 15.0 30.0 1 07/27/2022 21:50 WG1900474
2-Nitrophenol 88-75-5 5.00 J4 U 0.117 5.00 10.0 1 07/27/2022 21:50 WG1900474
4-Nitrophenol 100-02-7 5.00 U 0.143 5.00 10.0 1 07/27/2022 21:50 WG1900474
Pentachlorophenol 87-86-5 5.00 U 0.313 5.00 10.0 1 07/27/2022 21:50 WG1900474
Phenol 108-95-2 10.0 U 4.33 10.0 20.0 1 07/27/2022 21:50 WG1900474
2,4,6-Trichlorophenol 88-06-2 5.00 U 0.100 5.00 10.0 1 07/27/2022 21:50 WG1900474
(S) Nitrobenzene-d5 4165-60-0 60.0 0.000 44.0-120 07/27/2022 21:50 WG1900474
(S) 2-Fluorobiphenyl 321-60-8 63.1 0.000 44.0-119 07/27/2022 21:50 WG1900474
(S) p-Terphenyl-d14 1718-51-0 60.1 0.000 50.0-134 07/27/2022 21:50 WG1900474
(S) Phenol-d5 4165-62-2 16.1 0.000 10.0-67.0 07/27/2022 21:50 WG1900474
(S) 2-Fluorophenol 367-12-4 26.5 0.000 19.0-119 07/27/2022 21:50 WG1900474
(S) 2,4,6-Tribromophenol 118-79-6 85.5 0.000 43.0-140 07/27/2022 21:50 WG1900474
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 40 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 40 of 84
====================----□ □ □ □
□ □ □ □
SAMPLE RESULTS - 12
L1517739
IR35-MW67AR
Collected date/time: 07/20/22 14:32
Volatile Petroleum Hydrocarbons by Method MADEPV
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics C5-C8 ALI
UNADJ 491 33.3 67.0 134 1 07/31/2022 15:18 WG1903095
Unadjusted C9-C12 Aliphatics C9-C12 ALI
UNADJ 1450 33.3 67.0 134 1 07/31/2022 15:18 WG1903095
Unadjusted C9-C10 Aromatics C9-C10 ARO
UNADJ 914 167 335 670 5 08/03/2022 10:07 WG1903796
Total VPH VPH 2860 B 333 750 1500 5 08/03/2022 10:07 WG1903796
(S) 2,5-Dibromotoluene(FID)615-59-8 144 J1 70.0-130 07/31/2022 15:18 WG1903095
(S) 2,5-Dibromotoluene(FID)615-59-8 97.9 70.0-130 08/03/2022 10:07 WG1903796
(S) 2,5-Dibromotoluene(PID)615-59-8 80.3 70.0-130 07/31/2022 15:18 WG1903095
(S) 2,5-Dibromotoluene(PID)615-59-8 87.8 70.0-130 08/03/2022 10:07 WG1903796
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acetone 67-64-1 25.0 J3 U 11.3 25.0 50.0 1 07/25/2022 20:15 WG1900597
Acrolein 107-02-8 25.0 C4 U 2.54 25.0 50.0 1 07/25/2022 20:15 WG1900597
Acrylonitrile 107-13-1 5.00 J4 U 0.671 5.00 10.0 1 07/25/2022 20:15 WG1900597
Benzene 71-43-2 203 Q 0.941 5.00 10.0 10 08/04/2022 03:45 WG1905109
Bromobenzene 108-86-1 0.500 U 0.118 0.500 1.00 1 07/25/2022 20:15 WG1900597
Bromodichloromethane 75-27-4 0.500 U 0.136 0.500 1.00 1 07/25/2022 20:15 WG1900597
Bromoform 75-25-2 0.500 U 0.129 0.500 1.00 1 07/25/2022 20:15 WG1900597
Bromomethane 74-83-9 2.00 U 0.605 2.00 5.00 1 07/25/2022 20:15 WG1900597
n-Butylbenzene 104-51-8 12.3 0.157 0.500 1.00 1 07/25/2022 20:15 WG1900597
sec-Butylbenzene 135-98-8 16.6 0.125 0.500 1.00 1 07/25/2022 20:15 WG1900597
tert-Butylbenzene 98-06-6 1.25 0.127 0.500 1.00 1 07/25/2022 20:15 WG1900597
Carbon tetrachloride 56-23-5 0.500 U 0.128 0.500 1.00 1 07/25/2022 20:15 WG1900597
Chlorobenzene 108-90-7 0.500 U 0.116 0.500 1.00 1 07/25/2022 20:15 WG1900597
Chlorodibromomethane 124-48-1 0.500 U 0.140 0.500 1.00 1 07/25/2022 20:15 WG1900597
Chloroethane 75-00-3 2.00 U 0.192 2.00 5.00 1 07/25/2022 20:15 WG1900597
Chloroform 67-66-3 2.00 U 0.111 2.00 5.00 1 07/25/2022 20:15 WG1900597
Chloromethane 74-87-3 2.00 U 0.960 2.00 4.00 1 07/25/2022 20:15 WG1900597
2-Chlorotoluene 95-49-8 0.500 U 0.106 0.500 1.00 1 07/25/2022 20:15 WG1900597
4-Chlorotoluene 106-43-4 0.500 U 0.114 0.500 1.00 1 07/25/2022 20:15 WG1900597
1,2-Dibromo-3-Chloropropane 96-12-8 2.00 U 0.276 2.00 5.00 1 07/25/2022 20:15 WG1900597
1,2-Dibromoethane 106-93-4 0.500 U 0.126 0.500 1.00 1 07/25/2022 20:15 WG1900597
Dibromomethane 74-95-3 0.500 U 0.122 0.500 1.00 1 07/25/2022 20:15 WG1900597
1,2-Dichlorobenzene 95-50-1 0.500 U 0.107 0.500 1.00 1 07/25/2022 20:15 WG1900597
1,3-Dichlorobenzene 541-73-1 0.500 U 0.110 0.500 1.00 1 07/25/2022 20:15 WG1900597
1,4-Dichlorobenzene 106-46-7 0.500 U 0.120 0.500 1.00 1 07/25/2022 20:15 WG1900597
Dichlorodifluoromethane 75-71-8 2.00 U 0.374 2.00 5.00 1 07/25/2022 20:15 WG1900597
1,1-Dichloroethane 75-34-3 0.500 U 0.100 0.500 1.00 1 07/25/2022 20:15 WG1900597
1,2-Dichloroethane 107-06-2 0.500 U 0.0819 0.500 1.00 1 07/25/2022 20:15 WG1900597
1,1-Dichloroethene 75-35-4 0.500 U 0.188 0.500 1.00 1 07/25/2022 20:15 WG1900597
cis-1,2-Dichloroethene 156-59-2 0.500 U 0.126 0.500 1.00 1 07/25/2022 20:15 WG1900597
trans-1,2-Dichloroethene 156-60-5 0.500 U 0.149 0.500 1.00 1 07/25/2022 20:15 WG1900597
1,2-Dichloropropane 78-87-5 0.500 U 0.149 0.500 1.00 1 07/25/2022 20:15 WG1900597
1,1-Dichloropropene 563-58-6 0.500 U 0.142 0.500 1.00 1 07/25/2022 20:15 WG1900597
1,3-Dichloropropane 142-28-9 0.500 U 0.110 0.500 1.00 1 07/25/2022 20:15 WG1900597
2,2-Dichloropropane 594-20-7 0.500 U 0.161 0.500 1.00 1 07/25/2022 20:15 WG1900597
Di-isopropyl ether 108-20-3 0.500 U 0.105 0.500 1.00 1 07/25/2022 20:15 WG1900597
Ethylbenzene 100-41-4 312 Q 1.37 5.00 10.0 10 08/04/2022 03:45 WG1905109
Hexachloro-1,3-butadiene 87-68-3 0.750 J3 U 0.337 0.750 1.50 1 07/25/2022 20:15 WG1900597
Isopropylbenzene 98-82-8 59.4 0.105 0.500 1.00 1 07/25/2022 20:15 WG1900597
p-Isopropyltoluene 99-87-6 13.9 0.120 0.500 1.00 1 07/25/2022 20:15 WG1900597
2-Butanone (MEK)78-93-3 1.30 J 1.19 5.00 10.0 1 07/25/2022 20:15 WG1900597
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 41 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 41 of 84
--------------=---□
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□
======-=--=--=--=--=--=---=----=----=-----=-----=-----=-------=-~~ □ □ □
SAMPLE RESULTS - 12
L1517739
IR35-MW67AR
Collected date/time: 07/20/22 14:32
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Methylene Chloride 75-09-2 2.00 U 0.430 2.00 5.00 1 07/25/2022 20:15 WG1900597
4-Methyl-2-pentanone (MIBK)108-10-1 5.00 U 0.478 5.00 10.0 1 07/25/2022 20:15 WG1900597
Methyl tert-butyl ether 1634-04-4 0.500 U 0.101 0.500 1.00 1 07/25/2022 20:15 WG1900597
Naphthalene 91-20-3 523 Q 10.0 20.0 50.0 10 08/04/2022 03:45 WG1905109
n-Propylbenzene 103-65-1 80.7 0.0993 0.500 1.00 1 07/25/2022 20:15 WG1900597
Styrene 100-42-5 0.500 U 0.118 0.500 1.00 1 07/25/2022 20:15 WG1900597
1,1,1,2-Tetrachloroethane 630-20-6 0.500 U 0.147 0.500 1.00 1 07/25/2022 20:15 WG1900597
1,1,2,2-Tetrachloroethane 79-34-5 0.500 U 0.133 0.500 1.00 1 07/25/2022 20:15 WG1900597
Tetrachloroethene 127-18-4 0.600 U 0.300 0.600 1.20 1 07/25/2022 20:15 WG1900597
Toluene 108-88-3 5.22 0.278 0.600 1.20 1 07/25/2022 20:15 WG1900597
1,2,3-Trichlorobenzene 87-61-6 0.500 U 0.230 0.500 1.00 1 07/25/2022 20:15 WG1900597
1,2,4-Trichlorobenzene 120-82-1 1.00 U 0.481 1.00 2.00 1 07/25/2022 20:15 WG1900597
1,1,1-Trichloroethane 71-55-6 0.500 U 0.149 0.500 1.00 1 07/25/2022 20:15 WG1900597
1,1,2-Trichloroethane 79-00-5 0.500 U 0.158 0.500 1.00 1 07/25/2022 20:15 WG1900597
Trichloroethene 79-01-6 0.500 U 0.190 0.500 1.00 1 07/25/2022 20:15 WG1900597
Trichlorofluoromethane 75-69-4 2.00 U 0.160 2.00 5.00 1 07/25/2022 20:15 WG1900597
1,2,3-Trichloropropane 96-18-4 1.00 U 0.237 1.00 2.50 1 07/25/2022 20:15 WG1900597
1,2,4-Trimethylbenzene 95-63-6 261 Q 3.22 10.0 20.0 10 08/04/2022 03:45 WG1905109
1,3,5-Trimethylbenzene 108-67-8 3.25 0.104 0.500 1.00 1 07/25/2022 20:15 WG1900597
Vinyl chloride 75-01-4 0.500 U 0.234 0.500 1.00 1 07/25/2022 20:15 WG1900597
o-Xylene 95-47-6 0.775 J 0.174 0.500 1.00 1 07/25/2022 20:15 WG1900597
m&p-Xylenes 1330-20-7 161 0.430 1.00 2.00 1 07/25/2022 20:15 WG1900597
(S) Toluene-d8 2037-26-5 100 89.0-112 07/25/2022 20:15 WG1900597
(S) Toluene-d8 2037-26-5 103 89.0-112 08/04/2022 03:45 WG1905109
(S) 4-Bromofluorobenzene 460-00-4 101 85.0-114 07/25/2022 20:15 WG1900597
(S) 4-Bromofluorobenzene 460-00-4 99.9 85.0-114 08/04/2022 03:45 WG1905109
(S) 1,2-Dichloroethane-d4 17060-07-0 99.0 81.0-118 07/25/2022 20:15 WG1900597
(S) 1,2-Dichloroethane-d4 17060-07-0 87.3 81.0-118 08/04/2022 03:45 WG1905109
TPH by Method MADEPE
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics C9-C18 ALI
UNADJ 397 33.3 67.0 134 1 08/03/2022 05:49 WG1904482
Unadjusted C19-C36 Aliphatics C19-C36 ALI
UNADJ 89.2 B J 33.3 67.0 134 1 08/03/2022 05:49 WG1904482
Unadjusted C11-C22 Aromatics C11-C22 ARO
UNADJ 1790 33.3 67.0 134 1 08/03/2022 11:13 WG1904482
Unadjusted Total Petroleum
Hydrocarbons TPH UNADJ 2280 33.3 67.0 134 1 08/03/2022 11:13 WG1904482
(S) o-Terphenyl 84-15-1 70.4 40.0-140 08/03/2022 11:13 WG1904482
(S) 1-Chloro-octadecane 3386-33-2 72.9 40.0-140 08/03/2022 05:49 WG1904482
(S) 2-Fluorobiphenyl 321-60-8 77.6 40.0-140 08/03/2022 11:13 WG1904482
(S) 2-Bromonaphthalene 580-13-2 69.6 40.0-140 08/03/2022 11:13 WG1904482
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acenaphthene 83-32-9 3.15 0.0930 0.525 1.05 1.05 07/27/2022 22:33 WG1900474
Acenaphthylene 208-96-8 0.525 U 0.0967 0.525 1.05 1.05 07/27/2022 22:33 WG1900474
Anthracene 120-12-7 0.525 J4 U 0.0844 0.525 1.05 1.05 07/27/2022 22:33 WG1900474
Benzidine 92-87-5 7.88 J4 U 3.93 7.88 15.8 1.05 07/27/2022 22:33 WG1900474
Benzo(a)anthracene 56-55-3 0.525 U 0.209 0.525 1.05 1.05 07/27/2022 22:33 WG1900474
Benzo(b)fluoranthene 205-99-2 0.292 J 0.136 0.525 1.05 1.05 07/27/2022 22:33 WG1900474
Benzo(k)fluoranthene 207-08-9 0.525 U 0.126 0.525 1.05 1.05 07/27/2022 22:33 WG1900474
Benzo(g,h,i)perylene 191-24-2 0.160 J 0.127 0.525 1.05 1.05 07/27/2022 22:33 WG1900474
Benzo(a)pyrene 50-32-8 0.178 J 0.0400 0.525 1.05 1.05 07/27/2022 22:33 WG1900474
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 42 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 42 of 84
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SAMPLE RESULTS - 12
L1517739
IR35-MW67AR
Collected date/time: 07/20/22 14:32
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Bis(2-chlorethoxy)methane 111-91-1 5.25 J4 U 0.122 5.25 10.5 1.05 07/27/2022 22:33 WG1900474
Bis(2-chloroethyl)ether 111-44-4 5.25 J4 U 0.144 5.25 10.5 1.05 07/27/2022 22:33 WG1900474
2,2-Oxybis(1-Chloropropane)108-60-1 5.25 J4 U 0.221 5.25 10.5 1.05 07/27/2022 22:33 WG1900474
4-Bromophenyl-phenylether 101-55-3 5.25 U 0.0921 5.25 10.5 1.05 07/27/2022 22:33 WG1900474
2-Chloronaphthalene 91-58-7 0.525 U 0.0680 0.525 1.05 1.05 07/27/2022 22:33 WG1900474
4-Chlorophenyl-phenylether 7005-72-3 5.25 U 0.0972 5.25 10.5 1.05 07/27/2022 22:33 WG1900474
Chrysene 218-01-9 0.525 U 0.136 0.525 1.05 1.05 07/27/2022 22:33 WG1900474
Dibenz(a,h)anthracene 53-70-3 0.525 U 0.0676 0.525 1.05 1.05 07/27/2022 22:33 WG1900474
3,3-Dichlorobenzidine 91-94-1 5.25 U 0.223 5.25 10.5 1.05 07/27/2022 22:33 WG1900474
2,4-Dinitrotoluene 121-14-2 5.25 U 0.103 5.25 10.5 1.05 07/27/2022 22:33 WG1900474
2,6-Dinitrotoluene 606-20-2 5.25 J4 U 0.263 5.25 10.5 1.05 07/27/2022 22:33 WG1900474
Fluoranthene 206-44-0 0.148 J J4 0.107 0.525 1.05 1.05 07/27/2022 22:33 WG1900474
Fluorene 86-73-7 4.32 0.0886 0.525 1.05 1.05 07/27/2022 22:33 WG1900474
Hexachlorobenzene 118-74-1 0.525 U 0.0793 0.525 1.05 1.05 07/27/2022 22:33 WG1900474
Hexachloro-1,3-butadiene 87-68-3 5.25 U 0.102 5.25 10.5 1.05 07/27/2022 22:33 WG1900474
Hexachlorocyclopentadiene 77-47-4 5.25 U 0.0628 5.25 10.5 1.05 07/27/2022 22:33 WG1900474
Hexachloroethane 67-72-1 5.25 U 0.133 5.25 10.5 1.05 07/27/2022 22:33 WG1900474
Indeno(1,2,3-cd)pyrene 193-39-5 0.630 U 0.293 0.630 1.26 1.05 07/27/2022 22:33 WG1900474
Isophorone 78-59-1 5.25 U 0.150 5.25 10.5 1.05 07/27/2022 22:33 WG1900474
Naphthalene 91-20-3 174 J4 0.167 0.525 1.05 1.05 07/27/2022 22:33 WG1900474
Nitrobenzene 98-95-3 5.25 J4 U 0.312 5.25 10.5 1.05 07/27/2022 22:33 WG1900474
n-Nitrosodimethylamine 62-75-9 5.25 U 1.05 5.25 10.5 1.05 07/27/2022 22:33 WG1900474
n-Nitrosodiphenylamine 86-30-6 5.25 U 2.49 5.25 10.5 1.05 07/27/2022 22:33 WG1900474
n-Nitrosodi-n-propylamine 621-64-7 5.25 J4 U 0.274 5.25 10.5 1.05 07/27/2022 22:33 WG1900474
Phenanthrene 85-01-8 5.13 J4 0.118 0.525 1.05 1.05 07/27/2022 22:33 WG1900474
Benzylbutyl phthalate 85-68-7 2.10 U 0.803 2.10 4.20 1.05 07/27/2022 22:33 WG1900474
Bis(2-ethylhexyl)phthalate 117-81-7 0.940 J J4 0.940 2.10 4.20 1.05 07/27/2022 22:33 WG1900474
Di-n-butyl phthalate 84-74-2 1.58 J4 U 0.476 1.58 3.15 1.05 07/27/2022 22:33 WG1900474
Diethyl phthalate 84-66-2 1.58 J4 U 0.301 1.58 3.15 1.05 07/27/2022 22:33 WG1900474
Dimethyl phthalate 131-11-3 1.58 U 0.273 1.58 3.15 1.05 07/27/2022 22:33 WG1900474
Di-n-octyl phthalate 117-84-0 2.10 U 0.979 2.10 4.20 1.05 07/27/2022 22:33 WG1900474
Pyrene 129-00-0 0.210 J J4 0.112 0.525 1.05 1.05 07/27/2022 22:33 WG1900474
1,2,4-Trichlorobenzene 120-82-1 5.25 U 0.0733 5.25 10.5 1.05 07/27/2022 22:33 WG1900474
4-Chloro-3-methylphenol 59-50-7 5.25 J4 U 0.138 5.25 10.5 1.05 07/27/2022 22:33 WG1900474
2-Chlorophenol 95-57-8 5.25 J4 U 0.140 5.25 10.5 1.05 07/27/2022 22:33 WG1900474
2,4-Dichlorophenol 120-83-2 5.25 J4 U 0.107 5.25 10.5 1.05 07/27/2022 22:33 WG1900474
2,4-Dimethylphenol 105-67-9 5.25 U 0.0668 5.25 10.5 1.05 07/27/2022 22:33 WG1900474
4,6-Dinitro-2-methylphenol 534-52-1 5.25 U 1.18 5.25 10.5 1.05 07/27/2022 22:33 WG1900474
2,4-Dinitrophenol 51-28-5 15.8 U 6.23 15.8 31.5 1.05 07/27/2022 22:33 WG1900474
2-Nitrophenol 88-75-5 5.25 J4 U 0.123 5.25 10.5 1.05 07/27/2022 22:33 WG1900474
4-Nitrophenol 100-02-7 5.25 U 0.150 5.25 10.5 1.05 07/27/2022 22:33 WG1900474
Pentachlorophenol 87-86-5 5.25 U 0.329 5.25 10.5 1.05 07/27/2022 22:33 WG1900474
Phenol 108-95-2 10.5 U 4.55 10.5 21.0 1.05 07/27/2022 22:33 WG1900474
2,4,6-Trichlorophenol 88-06-2 5.25 U 0.105 5.25 10.5 1.05 07/27/2022 22:33 WG1900474
(S) Nitrobenzene-d5 4165-60-0 46.6 0.000 44.0-120 07/27/2022 22:33 WG1900474
(S) 2-Fluorobiphenyl 321-60-8 52.0 0.000 44.0-119 07/27/2022 22:33 WG1900474
(S) p-Terphenyl-d14 1718-51-0 57.9 0.000 50.0-134 07/27/2022 22:33 WG1900474
(S) Phenol-d5 4165-62-2 14.0 0.000 10.0-67.0 07/27/2022 22:33 WG1900474
(S) 2-Fluorophenol 367-12-4 21.7 0.000 19.0-119 07/27/2022 22:33 WG1900474
(S) 2,4,6-Tribromophenol 118-79-6 65.2 0.000 43.0-140 07/27/2022 22:33 WG1900474
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 43 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 43 of 84
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SAMPLE RESULTS - 13
L1517739
USTG480-MW26
Collected date/time: 07/20/22 15:00
Volatile Petroleum Hydrocarbons by Method MADEPV
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics C5-C8 ALI
UNADJ 107 J 33.3 67.0 134 1 07/31/2022 15:51 WG1903095
Unadjusted C9-C12 Aliphatics C9-C12 ALI
UNADJ 303 B 33.3 67.0 134 1 07/31/2022 15:51 WG1903095
Unadjusted C9-C10 Aromatics C9-C10 ARO
UNADJ 353 33.3 67.0 134 1 07/31/2022 15:51 WG1903095
Total VPH VPH 763 66.7 150 300 1 07/31/2022 15:51 WG1903095
(S) 2,5-Dibromotoluene(FID)615-59-8 120 70.0-130 07/31/2022 15:51 WG1903095
(S) 2,5-Dibromotoluene(PID)615-59-8 87.8 70.0-130 07/31/2022 15:51 WG1903095
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acetone 67-64-1 25.0 J3 U 11.3 25.0 50.0 1 07/25/2022 20:36 WG1900597
Acrolein 107-02-8 25.0 C4 U 2.54 25.0 50.0 1 07/25/2022 20:36 WG1900597
Acrylonitrile 107-13-1 5.00 J4 U 0.671 5.00 10.0 1 07/25/2022 20:36 WG1900597
Benzene 71-43-2 0.287 J 0.0941 0.500 1.00 1 08/03/2022 21:19 WG1905109
Bromobenzene 108-86-1 0.500 U 0.118 0.500 1.00 1 07/25/2022 20:36 WG1900597
Bromodichloromethane 75-27-4 0.500 U 0.136 0.500 1.00 1 07/25/2022 20:36 WG1900597
Bromoform 75-25-2 0.500 U 0.129 0.500 1.00 1 07/25/2022 20:36 WG1900597
Bromomethane 74-83-9 2.00 U 0.605 2.00 5.00 1 07/25/2022 20:36 WG1900597
n-Butylbenzene 104-51-8 4.60 0.157 0.500 1.00 1 07/25/2022 20:36 WG1900597
sec-Butylbenzene 135-98-8 4.24 0.125 0.500 1.00 1 07/25/2022 20:36 WG1900597
tert-Butylbenzene 98-06-6 0.828 J 0.127 0.500 1.00 1 07/25/2022 20:36 WG1900597
Carbon tetrachloride 56-23-5 0.500 U 0.128 0.500 1.00 1 07/25/2022 20:36 WG1900597
Chlorobenzene 108-90-7 0.500 U 0.116 0.500 1.00 1 07/25/2022 20:36 WG1900597
Chlorodibromomethane 124-48-1 0.500 U 0.140 0.500 1.00 1 07/25/2022 20:36 WG1900597
Chloroethane 75-00-3 2.00 U 0.192 2.00 5.00 1 07/25/2022 20:36 WG1900597
Chloroform 67-66-3 2.00 U 0.111 2.00 5.00 1 07/25/2022 20:36 WG1900597
Chloromethane 74-87-3 2.00 U 0.960 2.00 4.00 1 07/25/2022 20:36 WG1900597
2-Chlorotoluene 95-49-8 0.500 U 0.106 0.500 1.00 1 07/25/2022 20:36 WG1900597
4-Chlorotoluene 106-43-4 0.500 U 0.114 0.500 1.00 1 07/25/2022 20:36 WG1900597
1,2-Dibromo-3-Chloropropane 96-12-8 2.00 U 0.276 2.00 5.00 1 07/25/2022 20:36 WG1900597
1,2-Dibromoethane 106-93-4 0.500 U 0.126 0.500 1.00 1 07/25/2022 20:36 WG1900597
Dibromomethane 74-95-3 0.500 U 0.122 0.500 1.00 1 07/25/2022 20:36 WG1900597
1,2-Dichlorobenzene 95-50-1 0.500 U 0.107 0.500 1.00 1 07/25/2022 20:36 WG1900597
1,3-Dichlorobenzene 541-73-1 0.500 U 0.110 0.500 1.00 1 07/25/2022 20:36 WG1900597
1,4-Dichlorobenzene 106-46-7 0.500 U 0.120 0.500 1.00 1 07/25/2022 20:36 WG1900597
Dichlorodifluoromethane 75-71-8 2.00 U 0.374 2.00 5.00 1 07/25/2022 20:36 WG1900597
1,1-Dichloroethane 75-34-3 0.500 U 0.100 0.500 1.00 1 07/25/2022 20:36 WG1900597
1,2-Dichloroethane 107-06-2 0.500 U 0.0819 0.500 1.00 1 07/25/2022 20:36 WG1900597
1,1-Dichloroethene 75-35-4 0.500 U 0.188 0.500 1.00 1 07/25/2022 20:36 WG1900597
cis-1,2-Dichloroethene 156-59-2 0.500 U 0.126 0.500 1.00 1 07/25/2022 20:36 WG1900597
trans-1,2-Dichloroethene 156-60-5 0.500 U 0.149 0.500 1.00 1 07/25/2022 20:36 WG1900597
1,2-Dichloropropane 78-87-5 0.500 U 0.149 0.500 1.00 1 07/25/2022 20:36 WG1900597
1,1-Dichloropropene 563-58-6 0.500 U 0.142 0.500 1.00 1 07/25/2022 20:36 WG1900597
1,3-Dichloropropane 142-28-9 0.500 U 0.110 0.500 1.00 1 07/25/2022 20:36 WG1900597
2,2-Dichloropropane 594-20-7 0.500 U 0.161 0.500 1.00 1 07/25/2022 20:36 WG1900597
Di-isopropyl ether 108-20-3 0.500 U 0.105 0.500 1.00 1 07/25/2022 20:36 WG1900597
Ethylbenzene 100-41-4 0.216 J 0.137 0.500 1.00 1 08/03/2022 21:19 WG1905109
Hexachloro-1,3-butadiene 87-68-3 0.750 J3 U 0.337 0.750 1.50 1 07/25/2022 20:36 WG1900597
Isopropylbenzene 98-82-8 12.3 0.105 0.500 1.00 1 07/25/2022 20:36 WG1900597
p-Isopropyltoluene 99-87-6 3.85 0.120 0.500 1.00 1 07/25/2022 20:36 WG1900597
2-Butanone (MEK)78-93-3 5.00 U 1.19 5.00 10.0 1 07/25/2022 20:36 WG1900597
Methylene Chloride 75-09-2 2.00 U 0.430 2.00 5.00 1 07/25/2022 20:36 WG1900597
4-Methyl-2-pentanone (MIBK)108-10-1 5.00 U 0.478 5.00 10.0 1 07/25/2022 20:36 WG1900597
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 44 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 44 of 84
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SAMPLE RESULTS - 13
L1517739
USTG480-MW26
Collected date/time: 07/20/22 15:00
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Methyl tert-butyl ether 1634-04-4 0.500 U 0.101 0.500 1.00 1 07/25/2022 20:36 WG1900597
Naphthalene 91-20-3 2.00 U 1.00 2.00 5.00 1 08/03/2022 21:19 WG1905109
n-Propylbenzene 103-65-1 19.6 0.0993 0.500 1.00 1 07/25/2022 20:36 WG1900597
Styrene 100-42-5 0.500 U 0.118 0.500 1.00 1 07/25/2022 20:36 WG1900597
1,1,1,2-Tetrachloroethane 630-20-6 0.500 U 0.147 0.500 1.00 1 07/25/2022 20:36 WG1900597
1,1,2,2-Tetrachloroethane 79-34-5 0.500 U 0.133 0.500 1.00 1 07/25/2022 20:36 WG1900597
Tetrachloroethene 127-18-4 0.600 U 0.300 0.600 1.20 1 07/25/2022 20:36 WG1900597
Toluene 108-88-3 0.394 J 0.278 0.600 1.20 1 07/25/2022 20:36 WG1900597
1,2,3-Trichlorobenzene 87-61-6 0.500 U 0.230 0.500 1.00 1 07/25/2022 20:36 WG1900597
1,2,4-Trichlorobenzene 120-82-1 1.00 U 0.481 1.00 2.00 1 07/25/2022 20:36 WG1900597
1,1,1-Trichloroethane 71-55-6 0.500 U 0.149 0.500 1.00 1 07/25/2022 20:36 WG1900597
1,1,2-Trichloroethane 79-00-5 0.500 U 0.158 0.500 1.00 1 07/25/2022 20:36 WG1900597
Trichloroethene 79-01-6 0.500 U 0.190 0.500 1.00 1 07/25/2022 20:36 WG1900597
Trichlorofluoromethane 75-69-4 2.00 U 0.160 2.00 5.00 1 07/25/2022 20:36 WG1900597
1,2,3-Trichloropropane 96-18-4 1.00 U 0.237 1.00 2.50 1 07/25/2022 20:36 WG1900597
1,2,4-Trimethylbenzene 95-63-6 1.00 U 0.322 1.00 2.00 1 08/03/2022 21:19 WG1905109
1,3,5-Trimethylbenzene 108-67-8 0.500 U 0.104 0.500 1.00 1 07/25/2022 20:36 WG1900597
Vinyl chloride 75-01-4 0.500 U 0.234 0.500 1.00 1 07/25/2022 20:36 WG1900597
o-Xylene 95-47-6 0.711 J 0.174 0.500 1.00 1 08/03/2022 21:19 WG1905109
m&p-Xylenes 1330-20-7 1.00 U 0.430 1.00 2.00 1 08/03/2022 21:19 WG1905109
(S) Toluene-d8 2037-26-5 98.9 89.0-112 07/25/2022 20:36 WG1900597
(S) Toluene-d8 2037-26-5 107 89.0-112 08/03/2022 21:19 WG1905109
(S) 4-Bromofluorobenzene 460-00-4 99.2 85.0-114 07/25/2022 20:36 WG1900597
(S) 4-Bromofluorobenzene 460-00-4 108 85.0-114 08/03/2022 21:19 WG1905109
(S) 1,2-Dichloroethane-d4 17060-07-0 106 81.0-118 07/25/2022 20:36 WG1900597
(S) 1,2-Dichloroethane-d4 17060-07-0 86.6 81.0-118 08/03/2022 21:19 WG1905109
TPH by Method MADEPE
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics C9-C18 ALI
UNADJ 1330 33.3 67.0 134 1 08/03/2022 06:12 WG1904482
Unadjusted C19-C36 Aliphatics C19-C36 ALI
UNADJ 333 B 33.3 67.0 134 1 08/03/2022 06:12 WG1904482
Unadjusted C11-C22 Aromatics C11-C22 ARO
UNADJ 1610 33.3 67.0 134 1 08/03/2022 11:37 WG1904482
Unadjusted Total Petroleum
Hydrocarbons TPH UNADJ 3270 33.3 67.0 134 1 08/03/2022 11:37 WG1904482
(S) o-Terphenyl 84-15-1 72.7 40.0-140 08/03/2022 11:37 WG1904482
(S) 1-Chloro-octadecane 3386-33-2 64.4 40.0-140 08/03/2022 06:12 WG1904482
(S) 2-Fluorobiphenyl 321-60-8 87.6 40.0-140 08/03/2022 11:37 WG1904482
(S) 2-Bromonaphthalene 580-13-2 80.6 40.0-140 08/03/2022 11:37 WG1904482
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acenaphthene 83-32-9 2.44 0.0886 0.500 1.00 1 08/01/2022 19:03 WG1900474
Acenaphthylene 208-96-8 0.500 U 0.0921 0.500 1.00 1 08/01/2022 19:03 WG1900474
Anthracene 120-12-7 0.323 J J4 0.0804 0.500 1.00 1 08/01/2022 19:03 WG1900474
Benzidine 92-87-5 7.50 J4 U 3.74 7.50 15.0 1 08/01/2022 19:03 WG1900474
Benzo(a)anthracene 56-55-3 0.500 U 0.199 0.500 1.00 1 08/01/2022 19:03 WG1900474
Benzo(b)fluoranthene 205-99-2 0.500 U 0.130 0.500 1.00 1 08/01/2022 19:03 WG1900474
Benzo(k)fluoranthene 207-08-9 0.500 U 0.120 0.500 1.00 1 08/01/2022 19:03 WG1900474
Benzo(g,h,i)perylene 191-24-2 0.500 U 0.121 0.500 1.00 1 08/01/2022 19:03 WG1900474
Benzo(a)pyrene 50-32-8 0.500 U 0.0381 0.500 1.00 1 08/01/2022 19:03 WG1900474
Bis(2-chlorethoxy)methane 111-91-1 5.00 J4 U 0.116 5.00 10.0 1 08/01/2022 19:03 WG1900474
Bis(2-chloroethyl)ether 111-44-4 5.00 J4 U 0.137 5.00 10.0 1 08/01/2022 19:03 WG1900474
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 45 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 45 of 84
====================----□ □ □ □
□ □ □ □
SAMPLE RESULTS - 13
L1517739
USTG480-MW26
Collected date/time: 07/20/22 15:00
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
2,2-Oxybis(1-Chloropropane)108-60-1 5.00 J4 U 0.210 5.00 10.0 1 08/01/2022 19:03 WG1900474
4-Bromophenyl-phenylether 101-55-3 5.00 U 0.0877 5.00 10.0 1 08/01/2022 19:03 WG1900474
2-Chloronaphthalene 91-58-7 0.500 U 0.0648 0.500 1.00 1 08/01/2022 19:03 WG1900474
4-Chlorophenyl-phenylether 7005-72-3 5.00 U 0.0926 5.00 10.0 1 08/01/2022 19:03 WG1900474
Chrysene 218-01-9 0.500 U 0.130 0.500 1.00 1 08/01/2022 19:03 WG1900474
Dibenz(a,h)anthracene 53-70-3 0.500 U 0.0644 0.500 1.00 1 08/01/2022 19:03 WG1900474
3,3-Dichlorobenzidine 91-94-1 5.00 U 0.212 5.00 10.0 1 08/01/2022 19:03 WG1900474
2,4-Dinitrotoluene 121-14-2 5.00 U 0.0983 5.00 10.0 1 08/01/2022 19:03 WG1900474
2,6-Dinitrotoluene 606-20-2 5.00 J4 U 0.250 5.00 10.0 1 08/01/2022 19:03 WG1900474
Fluoranthene 206-44-0 0.500 J4 U 0.102 0.500 1.00 1 08/01/2022 19:03 WG1900474
Fluorene 86-73-7 3.89 0.0844 0.500 1.00 1 08/01/2022 19:03 WG1900474
Hexachlorobenzene 118-74-1 0.500 U 0.0755 0.500 1.00 1 08/01/2022 19:03 WG1900474
Hexachloro-1,3-butadiene 87-68-3 5.00 U 0.0968 5.00 10.0 1 08/01/2022 19:03 WG1900474
Hexachlorocyclopentadiene 77-47-4 5.00 C6 U 0.0598 5.00 10.0 1 08/01/2022 19:03 WG1900474
Hexachloroethane 67-72-1 5.00 U 0.127 5.00 10.0 1 08/01/2022 19:03 WG1900474
Indeno(1,2,3-cd)pyrene 193-39-5 0.600 U 0.279 0.600 1.20 1 08/01/2022 19:03 WG1900474
Isophorone 78-59-1 5.00 U 0.143 5.00 10.0 1 08/01/2022 19:03 WG1900474
Naphthalene 91-20-3 0.500 J4 U 0.159 0.500 1.00 1 08/01/2022 19:03 WG1900474
Nitrobenzene 98-95-3 5.00 J4 U 0.297 5.00 10.0 1 08/01/2022 19:03 WG1900474
n-Nitrosodimethylamine 62-75-9 5.00 U 0.998 5.00 10.0 1 08/01/2022 19:03 WG1900474
n-Nitrosodiphenylamine 86-30-6 5.00 U 2.37 5.00 10.0 1 08/01/2022 19:03 WG1900474
n-Nitrosodi-n-propylamine 621-64-7 5.00 J4 U 0.261 5.00 10.0 1 08/01/2022 19:03 WG1900474
Phenanthrene 85-01-8 2.50 J4 0.112 0.500 1.00 1 08/01/2022 19:03 WG1900474
Benzylbutyl phthalate 85-68-7 2.00 U 0.765 2.00 4.00 1 08/01/2022 19:03 WG1900474
Bis(2-ethylhexyl)phthalate 117-81-7 2.00 J4 U 0.895 2.00 4.00 1 08/01/2022 19:03 WG1900474
Di-n-butyl phthalate 84-74-2 1.50 J4 U 0.453 1.50 3.00 1 08/01/2022 19:03 WG1900474
Diethyl phthalate 84-66-2 1.50 J4 U 0.287 1.50 3.00 1 08/01/2022 19:03 WG1900474
Dimethyl phthalate 131-11-3 1.50 U 0.260 1.50 3.00 1 08/01/2022 19:03 WG1900474
Di-n-octyl phthalate 117-84-0 2.00 U 0.932 2.00 4.00 1 08/01/2022 19:03 WG1900474
Pyrene 129-00-0 0.500 J4 U 0.107 0.500 1.00 1 08/01/2022 19:03 WG1900474
1,2,4-Trichlorobenzene 120-82-1 5.00 U 0.0698 5.00 10.0 1 08/01/2022 19:03 WG1900474
4-Chloro-3-methylphenol 59-50-7 5.00 J4 U 0.131 5.00 10.0 1 08/01/2022 19:03 WG1900474
2-Chlorophenol 95-57-8 5.00 J4 U 0.133 5.00 10.0 1 08/01/2022 19:03 WG1900474
2,4-Dichlorophenol 120-83-2 5.00 J4 U 0.102 5.00 10.0 1 08/01/2022 19:03 WG1900474
2,4-Dimethylphenol 105-67-9 5.00 U 0.0636 5.00 10.0 1 08/01/2022 19:03 WG1900474
4,6-Dinitro-2-methylphenol 534-52-1 5.00 U 1.12 5.00 10.0 1 08/01/2022 19:03 WG1900474
2,4-Dinitrophenol 51-28-5 15.0 U 5.93 15.0 30.0 1 08/01/2022 19:03 WG1900474
2-Nitrophenol 88-75-5 5.00 J4 U 0.117 5.00 10.0 1 08/01/2022 19:03 WG1900474
4-Nitrophenol 100-02-7 5.00 U 0.143 5.00 10.0 1 08/01/2022 19:03 WG1900474
Pentachlorophenol 87-86-5 5.00 U 0.313 5.00 10.0 1 08/01/2022 19:03 WG1900474
Phenol 108-95-2 10.0 U 4.33 10.0 20.0 1 08/01/2022 19:03 WG1900474
2,4,6-Trichlorophenol 88-06-2 5.00 U 0.100 5.00 10.0 1 08/01/2022 19:03 WG1900474
1-Methylnaphthalene 90-12-0 46.6 0.0790 0.500 1.00 1 08/01/2022 19:03 WG1900474
2-Methylnaphthalene 91-57-6 41.2 0.117 0.500 1.00 1 08/01/2022 19:03 WG1900474
(S) Nitrobenzene-d5 4165-60-0 52.0 0.000 44.0-120 08/01/2022 19:03 WG1900474
(S) 2-Fluorobiphenyl 321-60-8 53.7 0.000 44.0-119 08/01/2022 19:03 WG1900474
(S) p-Terphenyl-d14 1718-51-0 60.6 0.000 50.0-134 08/01/2022 19:03 WG1900474
(S) Phenol-d5 4165-62-2 17.3 0.000 10.0-67.0 08/01/2022 19:03 WG1900474
(S) 2-Fluorophenol 367-12-4 21.2 0.000 19.0-119 08/01/2022 19:03 WG1900474
(S) 2,4,6-Tribromophenol 118-79-6 77.0 0.000 43.0-140 08/01/2022 19:03 WG1900474
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 46 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 46 of 84
====================----□ □ □ □
□ □ □ □
SAMPLE RESULTS - 14
L1517739
USTG480-MW30
Collected date/time: 07/20/22 15:00
Volatile Petroleum Hydrocarbons by Method MADEPV
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics C5-C8 ALI
UNADJ 35.4 J 33.3 67.0 134 1 07/31/2022 16:24 WG1903095
Unadjusted C9-C12 Aliphatics C9-C12 ALI
UNADJ 138 B 33.3 67.0 134 1 07/31/2022 16:24 WG1903095
Unadjusted C9-C10 Aromatics C9-C10 ARO
UNADJ 59.1 J 33.3 67.0 134 1 07/31/2022 16:24 WG1903095
Total VPH VPH 233 J 66.7 150 300 1 07/31/2022 16:24 WG1903095
(S) 2,5-Dibromotoluene(FID)615-59-8 96.8 70.0-130 07/31/2022 16:24 WG1903095
(S) 2,5-Dibromotoluene(PID)615-59-8 93.6 70.0-130 07/31/2022 16:24 WG1903095
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acetone 67-64-1 25.0 J3 U 11.3 25.0 50.0 1 07/25/2022 20:58 WG1900597
Acrolein 107-02-8 25.0 C4 U 2.54 25.0 50.0 1 07/25/2022 20:58 WG1900597
Acrylonitrile 107-13-1 5.00 J4 U 0.671 5.00 10.0 1 07/25/2022 20:58 WG1900597
Benzene 71-43-2 2.00 0.0941 0.500 1.00 1 07/25/2022 20:58 WG1900597
Bromobenzene 108-86-1 0.500 U 0.118 0.500 1.00 1 07/25/2022 20:58 WG1900597
Bromodichloromethane 75-27-4 0.500 U 0.136 0.500 1.00 1 07/25/2022 20:58 WG1900597
Bromoform 75-25-2 0.500 U 0.129 0.500 1.00 1 07/25/2022 20:58 WG1900597
Bromomethane 74-83-9 2.00 U 0.605 2.00 5.00 1 07/25/2022 20:58 WG1900597
n-Butylbenzene 104-51-8 0.500 U 0.157 0.500 1.00 1 07/25/2022 20:58 WG1900597
sec-Butylbenzene 135-98-8 0.261 J 0.125 0.500 1.00 1 07/25/2022 20:58 WG1900597
tert-Butylbenzene 98-06-6 0.224 J 0.127 0.500 1.00 1 07/25/2022 20:58 WG1900597
Carbon tetrachloride 56-23-5 0.500 U 0.128 0.500 1.00 1 07/25/2022 20:58 WG1900597
Chlorobenzene 108-90-7 0.500 U 0.116 0.500 1.00 1 07/25/2022 20:58 WG1900597
Chlorodibromomethane 124-48-1 0.500 U 0.140 0.500 1.00 1 07/25/2022 20:58 WG1900597
Chloroethane 75-00-3 2.00 U 0.192 2.00 5.00 1 07/25/2022 20:58 WG1900597
Chloroform 67-66-3 2.00 U 0.111 2.00 5.00 1 07/25/2022 20:58 WG1900597
Chloromethane 74-87-3 2.00 U 0.960 2.00 4.00 1 07/25/2022 20:58 WG1900597
2-Chlorotoluene 95-49-8 0.500 U 0.106 0.500 1.00 1 07/25/2022 20:58 WG1900597
4-Chlorotoluene 106-43-4 0.500 U 0.114 0.500 1.00 1 07/25/2022 20:58 WG1900597
1,2-Dibromo-3-Chloropropane 96-12-8 2.00 U 0.276 2.00 5.00 1 07/25/2022 20:58 WG1900597
1,2-Dibromoethane 106-93-4 0.500 U 0.126 0.500 1.00 1 07/25/2022 20:58 WG1900597
Dibromomethane 74-95-3 0.500 U 0.122 0.500 1.00 1 07/25/2022 20:58 WG1900597
1,2-Dichlorobenzene 95-50-1 0.500 U 0.107 0.500 1.00 1 07/25/2022 20:58 WG1900597
1,3-Dichlorobenzene 541-73-1 0.500 U 0.110 0.500 1.00 1 07/25/2022 20:58 WG1900597
1,4-Dichlorobenzene 106-46-7 0.500 U 0.120 0.500 1.00 1 07/25/2022 20:58 WG1900597
Dichlorodifluoromethane 75-71-8 2.00 U 0.374 2.00 5.00 1 07/25/2022 20:58 WG1900597
1,1-Dichloroethane 75-34-3 0.500 U 0.100 0.500 1.00 1 07/25/2022 20:58 WG1900597
1,2-Dichloroethane 107-06-2 0.500 U 0.0819 0.500 1.00 1 07/25/2022 20:58 WG1900597
1,1-Dichloroethene 75-35-4 0.500 U 0.188 0.500 1.00 1 07/25/2022 20:58 WG1900597
cis-1,2-Dichloroethene 156-59-2 0.267 J 0.126 0.500 1.00 1 07/25/2022 20:58 WG1900597
trans-1,2-Dichloroethene 156-60-5 0.500 U 0.149 0.500 1.00 1 07/25/2022 20:58 WG1900597
1,2-Dichloropropane 78-87-5 0.500 U 0.149 0.500 1.00 1 07/25/2022 20:58 WG1900597
1,1-Dichloropropene 563-58-6 0.500 U 0.142 0.500 1.00 1 07/25/2022 20:58 WG1900597
1,3-Dichloropropane 142-28-9 0.500 U 0.110 0.500 1.00 1 07/25/2022 20:58 WG1900597
2,2-Dichloropropane 594-20-7 0.500 U 0.161 0.500 1.00 1 07/25/2022 20:58 WG1900597
Di-isopropyl ether 108-20-3 0.711 J 0.105 0.500 1.00 1 07/25/2022 20:58 WG1900597
Ethylbenzene 100-41-4 0.500 U 0.137 0.500 1.00 1 08/03/2022 21:40 WG1905109
Hexachloro-1,3-butadiene 87-68-3 0.750 J3 U 0.337 0.750 1.50 1 07/25/2022 20:58 WG1900597
Isopropylbenzene 98-82-8 0.582 J 0.105 0.500 1.00 1 07/25/2022 20:58 WG1900597
p-Isopropyltoluene 99-87-6 0.172 J 0.120 0.500 1.00 1 07/25/2022 20:58 WG1900597
2-Butanone (MEK)78-93-3 5.00 U 1.19 5.00 10.0 1 07/25/2022 20:58 WG1900597
Methylene Chloride 75-09-2 0.524 J 0.430 2.00 5.00 1 07/25/2022 20:58 WG1900597
4-Methyl-2-pentanone (MIBK)108-10-1 5.00 U 0.478 5.00 10.0 1 07/25/2022 20:58 WG1900597
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 47 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 47 of 84
--------------=---□
□ □ □
==============~~~~~=----□ □ □ □
SAMPLE RESULTS - 14
L1517739
USTG480-MW30
Collected date/time: 07/20/22 15:00
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Methyl tert-butyl ether 1634-04-4 0.500 U 0.101 0.500 1.00 1 07/25/2022 20:58 WG1900597
Naphthalene 91-20-3 2.00 U 1.00 2.00 5.00 1 08/03/2022 21:40 WG1905109
n-Propylbenzene 103-65-1 0.456 J 0.0993 0.500 1.00 1 07/25/2022 20:58 WG1900597
Styrene 100-42-5 0.500 U 0.118 0.500 1.00 1 07/25/2022 20:58 WG1900597
1,1,1,2-Tetrachloroethane 630-20-6 0.500 U 0.147 0.500 1.00 1 07/25/2022 20:58 WG1900597
1,1,2,2-Tetrachloroethane 79-34-5 0.500 U 0.133 0.500 1.00 1 07/25/2022 20:58 WG1900597
Tetrachloroethene 127-18-4 0.600 U 0.300 0.600 1.20 1 07/25/2022 20:58 WG1900597
Toluene 108-88-3 0.600 U 0.278 0.600 1.20 1 07/25/2022 20:58 WG1900597
1,2,3-Trichlorobenzene 87-61-6 0.500 U 0.230 0.500 1.00 1 07/25/2022 20:58 WG1900597
1,2,4-Trichlorobenzene 120-82-1 1.00 U 0.481 1.00 2.00 1 07/25/2022 20:58 WG1900597
1,1,1-Trichloroethane 71-55-6 0.500 U 0.149 0.500 1.00 1 07/25/2022 20:58 WG1900597
1,1,2-Trichloroethane 79-00-5 0.500 U 0.158 0.500 1.00 1 07/25/2022 20:58 WG1900597
Trichloroethene 79-01-6 0.500 U 0.190 0.500 1.00 1 07/25/2022 20:58 WG1900597
Trichlorofluoromethane 75-69-4 2.00 U 0.160 2.00 5.00 1 07/25/2022 20:58 WG1900597
1,2,3-Trichloropropane 96-18-4 1.00 U 0.237 1.00 2.50 1 07/25/2022 20:58 WG1900597
1,2,4-Trimethylbenzene 95-63-6 1.00 U 0.322 1.00 2.00 1 08/03/2022 21:40 WG1905109
1,3,5-Trimethylbenzene 108-67-8 0.500 U 0.104 0.500 1.00 1 07/25/2022 20:58 WG1900597
Vinyl chloride 75-01-4 14.5 0.234 0.500 1.00 1 08/03/2022 21:40 WG1905109
o-Xylene 95-47-6 0.500 U 0.174 0.500 1.00 1 07/25/2022 20:58 WG1900597
m&p-Xylenes 1330-20-7 1.00 U 0.430 1.00 2.00 1 07/25/2022 20:58 WG1900597
(S) Toluene-d8 2037-26-5 96.9 89.0-112 07/25/2022 20:58 WG1900597
(S) Toluene-d8 2037-26-5 104 89.0-112 08/03/2022 21:40 WG1905109
(S) 4-Bromofluorobenzene 460-00-4 101 85.0-114 07/25/2022 20:58 WG1900597
(S) 4-Bromofluorobenzene 460-00-4 106 85.0-114 08/03/2022 21:40 WG1905109
(S) 1,2-Dichloroethane-d4 17060-07-0 104 81.0-118 07/25/2022 20:58 WG1900597
(S) 1,2-Dichloroethane-d4 17060-07-0 87.3 81.0-118 08/03/2022 21:40 WG1905109
TPH by Method MADEPE
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics C9-C18 ALI
UNADJ 67.0 U 33.3 67.0 134 1 08/03/2022 06:35 WG1904482
Unadjusted C19-C36 Aliphatics C19-C36 ALI
UNADJ 67.0 U 33.3 67.0 134 1 08/03/2022 06:35 WG1904482
Unadjusted C11-C22 Aromatics C11-C22 ARO
UNADJ 47.6 B J 33.3 67.0 134 1 08/03/2022 12:04 WG1904482
Unadjusted Total Petroleum
Hydrocarbons TPH UNADJ 47.6 B J 33.3 67.0 134 1 08/03/2022 06:35 WG1904482
(S) o-Terphenyl 84-15-1 76.5 40.0-140 08/03/2022 12:04 WG1904482
(S) 1-Chloro-octadecane 3386-33-2 57.9 40.0-140 08/03/2022 06:35 WG1904482
(S) 2-Fluorobiphenyl 321-60-8 88.3 40.0-140 08/03/2022 12:04 WG1904482
(S) 2-Bromonaphthalene 580-13-2 87.6 40.0-140 08/03/2022 12:04 WG1904482
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acenaphthene 83-32-9 0.500 U 0.0886 0.500 1.00 1 07/27/2022 20:43 WG1900474
Acenaphthylene 208-96-8 0.500 U 0.0921 0.500 1.00 1 07/27/2022 20:43 WG1900474
Anthracene 120-12-7 0.500 J4 U 0.0804 0.500 1.00 1 07/27/2022 20:43 WG1900474
Benzidine 92-87-5 7.50 J4 U 3.74 7.50 15.0 1 07/27/2022 20:43 WG1900474
Benzo(a)anthracene 56-55-3 0.500 U 0.199 0.500 1.00 1 07/27/2022 20:43 WG1900474
Benzo(b)fluoranthene 205-99-2 0.500 U 0.130 0.500 1.00 1 07/27/2022 20:43 WG1900474
Benzo(k)fluoranthene 207-08-9 0.500 U 0.120 0.500 1.00 1 07/27/2022 20:43 WG1900474
Benzo(g,h,i)perylene 191-24-2 0.500 U 0.121 0.500 1.00 1 07/27/2022 20:43 WG1900474
Benzo(a)pyrene 50-32-8 0.500 U 0.0381 0.500 1.00 1 07/27/2022 20:43 WG1900474
Bis(2-chlorethoxy)methane 111-91-1 5.00 J4 U 0.116 5.00 10.0 1 07/27/2022 20:43 WG1900474
Bis(2-chloroethyl)ether 111-44-4 5.00 J4 U 0.137 5.00 10.0 1 07/27/2022 20:43 WG1900474
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 48 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 48 of 84
====================----□ □ □ □
□ □ □ □
SAMPLE RESULTS - 14
L1517739
USTG480-MW30
Collected date/time: 07/20/22 15:00
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
2,2-Oxybis(1-Chloropropane)108-60-1 5.00 J4 U 0.210 5.00 10.0 1 07/27/2022 20:43 WG1900474
4-Bromophenyl-phenylether 101-55-3 5.00 U 0.0877 5.00 10.0 1 07/27/2022 20:43 WG1900474
2-Chloronaphthalene 91-58-7 0.500 U 0.0648 0.500 1.00 1 07/27/2022 20:43 WG1900474
4-Chlorophenyl-phenylether 7005-72-3 5.00 U 0.0926 5.00 10.0 1 07/27/2022 20:43 WG1900474
Chrysene 218-01-9 0.500 U 0.130 0.500 1.00 1 07/27/2022 20:43 WG1900474
Dibenz(a,h)anthracene 53-70-3 0.500 U 0.0644 0.500 1.00 1 07/27/2022 20:43 WG1900474
3,3-Dichlorobenzidine 91-94-1 5.00 U 0.212 5.00 10.0 1 07/27/2022 20:43 WG1900474
2,4-Dinitrotoluene 121-14-2 5.00 U 0.0983 5.00 10.0 1 07/27/2022 20:43 WG1900474
2,6-Dinitrotoluene 606-20-2 5.00 J4 U 0.250 5.00 10.0 1 07/27/2022 20:43 WG1900474
Fluoranthene 206-44-0 0.500 J4 U 0.102 0.500 1.00 1 07/27/2022 20:43 WG1900474
Fluorene 86-73-7 0.500 U 0.0844 0.500 1.00 1 07/27/2022 20:43 WG1900474
Hexachlorobenzene 118-74-1 0.500 U 0.0755 0.500 1.00 1 07/27/2022 20:43 WG1900474
Hexachloro-1,3-butadiene 87-68-3 5.00 U 0.0968 5.00 10.0 1 07/27/2022 20:43 WG1900474
Hexachlorocyclopentadiene 77-47-4 5.00 U 0.0598 5.00 10.0 1 07/27/2022 20:43 WG1900474
Hexachloroethane 67-72-1 5.00 U 0.127 5.00 10.0 1 07/27/2022 20:43 WG1900474
Indeno(1,2,3-cd)pyrene 193-39-5 0.600 U 0.279 0.600 1.20 1 07/27/2022 20:43 WG1900474
Isophorone 78-59-1 5.00 U 0.143 5.00 10.0 1 07/27/2022 20:43 WG1900474
Naphthalene 91-20-3 0.355 J J4 0.159 0.500 1.00 1 07/27/2022 20:43 WG1900474
Nitrobenzene 98-95-3 5.00 J4 U 0.297 5.00 10.0 1 07/27/2022 20:43 WG1900474
n-Nitrosodimethylamine 62-75-9 5.00 U 0.998 5.00 10.0 1 07/27/2022 20:43 WG1900474
n-Nitrosodiphenylamine 86-30-6 5.00 U 2.37 5.00 10.0 1 07/27/2022 20:43 WG1900474
n-Nitrosodi-n-propylamine 621-64-7 5.00 J4 U 0.261 5.00 10.0 1 07/27/2022 20:43 WG1900474
Phenanthrene 85-01-8 0.500 J4 U 0.112 0.500 1.00 1 07/27/2022 20:43 WG1900474
Benzylbutyl phthalate 85-68-7 2.00 U 0.765 2.00 4.00 1 07/27/2022 20:43 WG1900474
Bis(2-ethylhexyl)phthalate 117-81-7 2.00 J4 U 0.895 2.00 4.00 1 07/27/2022 20:43 WG1900474
Di-n-butyl phthalate 84-74-2 1.50 J4 U 0.453 1.50 3.00 1 07/27/2022 20:43 WG1900474
Diethyl phthalate 84-66-2 1.50 J4 U 0.287 1.50 3.00 1 07/27/2022 20:43 WG1900474
Dimethyl phthalate 131-11-3 1.50 U 0.260 1.50 3.00 1 07/27/2022 20:43 WG1900474
Di-n-octyl phthalate 117-84-0 2.00 U 0.932 2.00 4.00 1 07/27/2022 20:43 WG1900474
Pyrene 129-00-0 0.500 J4 U 0.107 0.500 1.00 1 07/27/2022 20:43 WG1900474
1,2,4-Trichlorobenzene 120-82-1 5.00 U 0.0698 5.00 10.0 1 07/27/2022 20:43 WG1900474
4-Chloro-3-methylphenol 59-50-7 5.00 J4 U 0.131 5.00 10.0 1 07/27/2022 20:43 WG1900474
2-Chlorophenol 95-57-8 5.00 J4 U 0.133 5.00 10.0 1 07/27/2022 20:43 WG1900474
2,4-Dichlorophenol 120-83-2 5.00 J4 U 0.102 5.00 10.0 1 07/27/2022 20:43 WG1900474
2,4-Dimethylphenol 105-67-9 5.00 U 0.0636 5.00 10.0 1 07/27/2022 20:43 WG1900474
4,6-Dinitro-2-methylphenol 534-52-1 5.00 U 1.12 5.00 10.0 1 07/27/2022 20:43 WG1900474
2,4-Dinitrophenol 51-28-5 15.0 U 5.93 15.0 30.0 1 07/27/2022 20:43 WG1900474
2-Nitrophenol 88-75-5 5.00 J4 U 0.117 5.00 10.0 1 07/27/2022 20:43 WG1900474
4-Nitrophenol 100-02-7 5.00 U 0.143 5.00 10.0 1 07/27/2022 20:43 WG1900474
Pentachlorophenol 87-86-5 5.00 U 0.313 5.00 10.0 1 07/27/2022 20:43 WG1900474
Phenol 108-95-2 10.0 U 4.33 10.0 20.0 1 07/27/2022 20:43 WG1900474
2,4,6-Trichlorophenol 88-06-2 5.00 U 0.100 5.00 10.0 1 07/27/2022 20:43 WG1900474
(S) Nitrobenzene-d5 4165-60-0 45.1 0.000 44.0-120 07/27/2022 20:43 WG1900474
(S) 2-Fluorobiphenyl 321-60-8 51.2 0.000 44.0-119 07/27/2022 20:43 WG1900474
(S) p-Terphenyl-d14 1718-51-0 62.9 0.000 50.0-134 07/27/2022 20:43 WG1900474
(S) Phenol-d5 4165-62-2 11.7 0.000 10.0-67.0 07/27/2022 20:43 WG1900474
(S) 2-Fluorophenol 367-12-4 17.0 J2 0.000 19.0-119 07/27/2022 20:43 WG1900474
(S) 2,4,6-Tribromophenol 118-79-6 65.4 0.000 43.0-140 07/27/2022 20:43 WG1900474
Sample Narrative:
L1517739-14 WG1900474: Surrogate recovery within historical limits.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 49 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 49 of 84
====================----□ □ □ □
□ □ □ □
SAMPLE RESULTS - 15
L1517739
USTG480-MW33R
Collected date/time: 07/20/22 15:27
Volatile Petroleum Hydrocarbons by Method MADEPV
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics C5-C8 ALI
UNADJ 67.0 U 33.3 67.0 134 1 07/31/2022 16:57 WG1903095
Unadjusted C9-C12 Aliphatics C9-C12 ALI
UNADJ 90.2 B J 33.3 67.0 134 1 07/31/2022 16:57 WG1903095
Unadjusted C9-C10 Aromatics C9-C10 ARO
UNADJ 67.0 U 33.3 67.0 134 1 07/31/2022 16:57 WG1903095
Total VPH VPH 90.2 J 66.7 150 300 1 07/31/2022 16:57 WG1903095
(S) 2,5-Dibromotoluene(FID)615-59-8 95.7 70.0-130 07/31/2022 16:57 WG1903095
(S) 2,5-Dibromotoluene(PID)615-59-8 95.9 70.0-130 07/31/2022 16:57 WG1903095
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acetone 67-64-1 25.0 J3 U 11.3 25.0 50.0 1 07/25/2022 21:19 WG1900597
Acrolein 107-02-8 25.0 C4 U 2.54 25.0 50.0 1 07/25/2022 21:19 WG1900597
Acrylonitrile 107-13-1 5.00 J4 U 0.671 5.00 10.0 1 07/25/2022 21:19 WG1900597
Benzene 71-43-2 0.500 U 0.0941 0.500 1.00 1 07/25/2022 21:19 WG1900597
Bromobenzene 108-86-1 0.500 U 0.118 0.500 1.00 1 07/25/2022 21:19 WG1900597
Bromodichloromethane 75-27-4 0.500 U 0.136 0.500 1.00 1 07/25/2022 21:19 WG1900597
Bromoform 75-25-2 0.500 U 0.129 0.500 1.00 1 07/25/2022 21:19 WG1900597
Bromomethane 74-83-9 2.00 U 0.605 2.00 5.00 1 07/25/2022 21:19 WG1900597
n-Butylbenzene 104-51-8 0.220 J 0.157 0.500 1.00 1 07/25/2022 21:19 WG1900597
sec-Butylbenzene 135-98-8 0.453 J 0.125 0.500 1.00 1 07/25/2022 21:19 WG1900597
tert-Butylbenzene 98-06-6 0.500 U 0.127 0.500 1.00 1 07/25/2022 21:19 WG1900597
Carbon tetrachloride 56-23-5 0.500 U 0.128 0.500 1.00 1 07/25/2022 21:19 WG1900597
Chlorobenzene 108-90-7 0.500 U 0.116 0.500 1.00 1 07/25/2022 21:19 WG1900597
Chlorodibromomethane 124-48-1 0.500 U 0.140 0.500 1.00 1 07/25/2022 21:19 WG1900597
Chloroethane 75-00-3 2.00 U 0.192 2.00 5.00 1 07/25/2022 21:19 WG1900597
Chloroform 67-66-3 2.00 U 0.111 2.00 5.00 1 07/25/2022 21:19 WG1900597
Chloromethane 74-87-3 2.00 U 0.960 2.00 4.00 1 07/25/2022 21:19 WG1900597
2-Chlorotoluene 95-49-8 0.500 U 0.106 0.500 1.00 1 07/25/2022 21:19 WG1900597
4-Chlorotoluene 106-43-4 0.500 U 0.114 0.500 1.00 1 07/25/2022 21:19 WG1900597
1,2-Dibromo-3-Chloropropane 96-12-8 2.00 U 0.276 2.00 5.00 1 07/25/2022 21:19 WG1900597
1,2-Dibromoethane 106-93-4 0.500 U 0.126 0.500 1.00 1 07/25/2022 21:19 WG1900597
Dibromomethane 74-95-3 0.500 U 0.122 0.500 1.00 1 07/25/2022 21:19 WG1900597
1,2-Dichlorobenzene 95-50-1 0.500 U 0.107 0.500 1.00 1 07/25/2022 21:19 WG1900597
1,3-Dichlorobenzene 541-73-1 0.500 U 0.110 0.500 1.00 1 07/25/2022 21:19 WG1900597
1,4-Dichlorobenzene 106-46-7 0.500 U 0.120 0.500 1.00 1 07/25/2022 21:19 WG1900597
Dichlorodifluoromethane 75-71-8 2.00 U 0.374 2.00 5.00 1 07/25/2022 21:19 WG1900597
1,1-Dichloroethane 75-34-3 0.500 U 0.100 0.500 1.00 1 07/25/2022 21:19 WG1900597
1,2-Dichloroethane 107-06-2 0.500 U 0.0819 0.500 1.00 1 07/25/2022 21:19 WG1900597
1,1-Dichloroethene 75-35-4 0.500 U 0.188 0.500 1.00 1 07/25/2022 21:19 WG1900597
cis-1,2-Dichloroethene 156-59-2 0.500 U 0.126 0.500 1.00 1 07/25/2022 21:19 WG1900597
trans-1,2-Dichloroethene 156-60-5 0.500 U 0.149 0.500 1.00 1 07/25/2022 21:19 WG1900597
1,2-Dichloropropane 78-87-5 0.500 U 0.149 0.500 1.00 1 07/25/2022 21:19 WG1900597
1,1-Dichloropropene 563-58-6 0.500 U 0.142 0.500 1.00 1 07/25/2022 21:19 WG1900597
1,3-Dichloropropane 142-28-9 0.500 U 0.110 0.500 1.00 1 07/25/2022 21:19 WG1900597
2,2-Dichloropropane 594-20-7 0.500 U 0.161 0.500 1.00 1 07/25/2022 21:19 WG1900597
Di-isopropyl ether 108-20-3 0.500 U 0.105 0.500 1.00 1 07/25/2022 21:19 WG1900597
Ethylbenzene 100-41-4 0.500 U 0.137 0.500 1.00 1 07/25/2022 21:19 WG1900597
Hexachloro-1,3-butadiene 87-68-3 0.750 J3 U 0.337 0.750 1.50 1 07/25/2022 21:19 WG1900597
Isopropylbenzene 98-82-8 0.372 J 0.105 0.500 1.00 1 07/25/2022 21:19 WG1900597
p-Isopropyltoluene 99-87-6 0.500 U 0.120 0.500 1.00 1 07/25/2022 21:19 WG1900597
2-Butanone (MEK)78-93-3 5.00 U 1.19 5.00 10.0 1 07/25/2022 21:19 WG1900597
Methylene Chloride 75-09-2 2.00 U 0.430 2.00 5.00 1 07/25/2022 21:19 WG1900597
4-Methyl-2-pentanone (MIBK)108-10-1 5.00 U 0.478 5.00 10.0 1 07/25/2022 21:19 WG1900597
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 50 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 50 of 84
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SAMPLE RESULTS - 15
L1517739
USTG480-MW33R
Collected date/time: 07/20/22 15:27
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Methyl tert-butyl ether 1634-04-4 0.500 U 0.101 0.500 1.00 1 07/25/2022 21:19 WG1900597
Naphthalene 91-20-3 2.00 U 1.00 2.00 5.00 1 08/03/2022 22:01 WG1905109
n-Propylbenzene 103-65-1 0.380 J 0.0993 0.500 1.00 1 07/25/2022 21:19 WG1900597
Styrene 100-42-5 0.500 U 0.118 0.500 1.00 1 07/25/2022 21:19 WG1900597
1,1,1,2-Tetrachloroethane 630-20-6 0.500 U 0.147 0.500 1.00 1 07/25/2022 21:19 WG1900597
1,1,2,2-Tetrachloroethane 79-34-5 0.500 U 0.133 0.500 1.00 1 07/25/2022 21:19 WG1900597
Tetrachloroethene 127-18-4 0.600 U 0.300 0.600 1.20 1 07/25/2022 21:19 WG1900597
Toluene 108-88-3 0.600 U 0.278 0.600 1.20 1 07/25/2022 21:19 WG1900597
1,2,3-Trichlorobenzene 87-61-6 0.500 U 0.230 0.500 1.00 1 07/25/2022 21:19 WG1900597
1,2,4-Trichlorobenzene 120-82-1 1.00 U 0.481 1.00 2.00 1 07/25/2022 21:19 WG1900597
1,1,1-Trichloroethane 71-55-6 0.500 U 0.149 0.500 1.00 1 07/25/2022 21:19 WG1900597
1,1,2-Trichloroethane 79-00-5 0.500 U 0.158 0.500 1.00 1 07/25/2022 21:19 WG1900597
Trichloroethene 79-01-6 0.500 U 0.190 0.500 1.00 1 07/25/2022 21:19 WG1900597
Trichlorofluoromethane 75-69-4 2.00 U 0.160 2.00 5.00 1 07/25/2022 21:19 WG1900597
1,2,3-Trichloropropane 96-18-4 1.00 U 0.237 1.00 2.50 1 07/25/2022 21:19 WG1900597
1,2,4-Trimethylbenzene 95-63-6 1.00 U 0.322 1.00 2.00 1 07/25/2022 21:19 WG1900597
1,3,5-Trimethylbenzene 108-67-8 0.500 U 0.104 0.500 1.00 1 07/25/2022 21:19 WG1900597
Vinyl chloride 75-01-4 0.500 U 0.234 0.500 1.00 1 07/25/2022 21:19 WG1900597
o-Xylene 95-47-6 0.500 U 0.174 0.500 1.00 1 07/25/2022 21:19 WG1900597
m&p-Xylenes 1330-20-7 1.00 U 0.430 1.00 2.00 1 07/25/2022 21:19 WG1900597
(S) Toluene-d8 2037-26-5 95.4 89.0-112 07/25/2022 21:19 WG1900597
(S) Toluene-d8 2037-26-5 103 89.0-112 08/03/2022 22:01 WG1905109
(S) 4-Bromofluorobenzene 460-00-4 98.0 85.0-114 07/25/2022 21:19 WG1900597
(S) 4-Bromofluorobenzene 460-00-4 104 85.0-114 08/03/2022 22:01 WG1905109
(S) 1,2-Dichloroethane-d4 17060-07-0 104 81.0-118 07/25/2022 21:19 WG1900597
(S) 1,2-Dichloroethane-d4 17060-07-0 89.1 81.0-118 08/03/2022 22:01 WG1905109
TPH by Method MADEPE
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics C9-C18 ALI
UNADJ 67.0 U 33.3 67.0 134 1 08/03/2022 06:58 WG1904482
Unadjusted C19-C36 Aliphatics C19-C36 ALI
UNADJ 35.4 B J 33.3 67.0 134 1 08/03/2022 06:58 WG1904482
Unadjusted C11-C22 Aromatics C11-C22 ARO
UNADJ 71.1 B J 33.3 67.0 134 1 08/03/2022 12:27 WG1904482
Unadjusted Total Petroleum
Hydrocarbons TPH UNADJ 107 B J 33.3 67.0 134 1 08/03/2022 12:27 WG1904482
(S) o-Terphenyl 84-15-1 73.0 40.0-140 08/03/2022 12:27 WG1904482
(S) 1-Chloro-octadecane 3386-33-2 58.1 40.0-140 08/03/2022 06:58 WG1904482
(S) 2-Fluorobiphenyl 321-60-8 83.2 40.0-140 08/03/2022 12:27 WG1904482
(S) 2-Bromonaphthalene 580-13-2 82.7 40.0-140 08/03/2022 12:27 WG1904482
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acenaphthene 83-32-9 0.500 U 0.0886 0.500 1.00 1 07/27/2022 19:59 WG1900474
Acenaphthylene 208-96-8 0.500 U 0.0921 0.500 1.00 1 07/27/2022 19:59 WG1900474
Anthracene 120-12-7 0.500 J4 U 0.0804 0.500 1.00 1 07/27/2022 19:59 WG1900474
Benzidine 92-87-5 7.50 J4 U 3.74 7.50 15.0 1 07/27/2022 19:59 WG1900474
Benzo(a)anthracene 56-55-3 0.500 U 0.199 0.500 1.00 1 07/27/2022 19:59 WG1900474
Benzo(b)fluoranthene 205-99-2 0.500 U 0.130 0.500 1.00 1 07/27/2022 19:59 WG1900474
Benzo(k)fluoranthene 207-08-9 0.500 U 0.120 0.500 1.00 1 07/27/2022 19:59 WG1900474
Benzo(g,h,i)perylene 191-24-2 0.500 U 0.121 0.500 1.00 1 07/27/2022 19:59 WG1900474
Benzo(a)pyrene 50-32-8 0.500 U 0.0381 0.500 1.00 1 07/27/2022 19:59 WG1900474
Bis(2-chlorethoxy)methane 111-91-1 5.00 J4 U 0.116 5.00 10.0 1 07/27/2022 19:59 WG1900474
Bis(2-chloroethyl)ether 111-44-4 5.00 J4 U 0.137 5.00 10.0 1 07/27/2022 19:59 WG1900474
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 51 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 51 of 84
====================----□ □ □ □
□ □ □ □
SAMPLE RESULTS - 15
L1517739
USTG480-MW33R
Collected date/time: 07/20/22 15:27
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
2,2-Oxybis(1-Chloropropane)108-60-1 5.00 J4 U 0.210 5.00 10.0 1 07/27/2022 19:59 WG1900474
4-Bromophenyl-phenylether 101-55-3 5.00 U 0.0877 5.00 10.0 1 07/27/2022 19:59 WG1900474
2-Chloronaphthalene 91-58-7 0.500 U 0.0648 0.500 1.00 1 07/27/2022 19:59 WG1900474
4-Chlorophenyl-phenylether 7005-72-3 5.00 U 0.0926 5.00 10.0 1 07/27/2022 19:59 WG1900474
Chrysene 218-01-9 0.500 U 0.130 0.500 1.00 1 07/27/2022 19:59 WG1900474
Dibenz(a,h)anthracene 53-70-3 0.500 U 0.0644 0.500 1.00 1 07/27/2022 19:59 WG1900474
3,3-Dichlorobenzidine 91-94-1 5.00 U 0.212 5.00 10.0 1 07/27/2022 19:59 WG1900474
2,4-Dinitrotoluene 121-14-2 5.00 U 0.0983 5.00 10.0 1 07/27/2022 19:59 WG1900474
2,6-Dinitrotoluene 606-20-2 5.00 J4 U 0.250 5.00 10.0 1 07/27/2022 19:59 WG1900474
Fluoranthene 206-44-0 0.500 J4 U 0.102 0.500 1.00 1 07/27/2022 19:59 WG1900474
Fluorene 86-73-7 0.113 J 0.0844 0.500 1.00 1 07/27/2022 19:59 WG1900474
Hexachlorobenzene 118-74-1 0.500 U 0.0755 0.500 1.00 1 07/27/2022 19:59 WG1900474
Hexachloro-1,3-butadiene 87-68-3 5.00 U 0.0968 5.00 10.0 1 07/27/2022 19:59 WG1900474
Hexachlorocyclopentadiene 77-47-4 5.00 U 0.0598 5.00 10.0 1 07/27/2022 19:59 WG1900474
Hexachloroethane 67-72-1 5.00 U 0.127 5.00 10.0 1 07/27/2022 19:59 WG1900474
Indeno(1,2,3-cd)pyrene 193-39-5 0.600 U 0.279 0.600 1.20 1 07/27/2022 19:59 WG1900474
Isophorone 78-59-1 5.00 U 0.143 5.00 10.0 1 07/27/2022 19:59 WG1900474
Naphthalene 91-20-3 0.212 J J4 0.159 0.500 1.00 1 07/27/2022 19:59 WG1900474
Nitrobenzene 98-95-3 5.00 J4 U 0.297 5.00 10.0 1 07/27/2022 19:59 WG1900474
n-Nitrosodimethylamine 62-75-9 5.00 U 0.998 5.00 10.0 1 07/27/2022 19:59 WG1900474
n-Nitrosodiphenylamine 86-30-6 5.00 U 2.37 5.00 10.0 1 07/27/2022 19:59 WG1900474
n-Nitrosodi-n-propylamine 621-64-7 5.00 J4 U 0.261 5.00 10.0 1 07/27/2022 19:59 WG1900474
Phenanthrene 85-01-8 0.500 J4 U 0.112 0.500 1.00 1 07/27/2022 19:59 WG1900474
Benzylbutyl phthalate 85-68-7 2.00 U 0.765 2.00 4.00 1 07/27/2022 19:59 WG1900474
Bis(2-ethylhexyl)phthalate 117-81-7 2.00 J4 U 0.895 2.00 4.00 1 07/27/2022 19:59 WG1900474
Di-n-butyl phthalate 84-74-2 1.50 J4 U 0.453 1.50 3.00 1 07/27/2022 19:59 WG1900474
Diethyl phthalate 84-66-2 1.50 J4 U 0.287 1.50 3.00 1 07/27/2022 19:59 WG1900474
Dimethyl phthalate 131-11-3 1.50 U 0.260 1.50 3.00 1 07/27/2022 19:59 WG1900474
Di-n-octyl phthalate 117-84-0 2.00 U 0.932 2.00 4.00 1 07/27/2022 19:59 WG1900474
Pyrene 129-00-0 0.500 J4 U 0.107 0.500 1.00 1 07/27/2022 19:59 WG1900474
1,2,4-Trichlorobenzene 120-82-1 5.00 U 0.0698 5.00 10.0 1 07/27/2022 19:59 WG1900474
4-Chloro-3-methylphenol 59-50-7 5.00 J4 U 0.131 5.00 10.0 1 07/27/2022 19:59 WG1900474
2-Chlorophenol 95-57-8 5.00 J4 U 0.133 5.00 10.0 1 07/27/2022 19:59 WG1900474
2,4-Dichlorophenol 120-83-2 5.00 J4 U 0.102 5.00 10.0 1 07/27/2022 19:59 WG1900474
2,4-Dimethylphenol 105-67-9 5.00 U 0.0636 5.00 10.0 1 07/27/2022 19:59 WG1900474
4,6-Dinitro-2-methylphenol 534-52-1 5.00 U 1.12 5.00 10.0 1 07/27/2022 19:59 WG1900474
2,4-Dinitrophenol 51-28-5 15.0 U 5.93 15.0 30.0 1 07/27/2022 19:59 WG1900474
2-Nitrophenol 88-75-5 5.00 J4 U 0.117 5.00 10.0 1 07/27/2022 19:59 WG1900474
4-Nitrophenol 100-02-7 5.00 U 0.143 5.00 10.0 1 07/27/2022 19:59 WG1900474
Pentachlorophenol 87-86-5 5.00 U 0.313 5.00 10.0 1 07/27/2022 19:59 WG1900474
Phenol 108-95-2 10.0 U 4.33 10.0 20.0 1 07/27/2022 19:59 WG1900474
2,4,6-Trichlorophenol 88-06-2 5.00 U 0.100 5.00 10.0 1 07/27/2022 19:59 WG1900474
(S) Nitrobenzene-d5 4165-60-0 44.7 0.000 44.0-120 07/27/2022 19:59 WG1900474
(S) 2-Fluorobiphenyl 321-60-8 53.6 0.000 44.0-119 07/27/2022 19:59 WG1900474
(S) p-Terphenyl-d14 1718-51-0 60.4 0.000 50.0-134 07/27/2022 19:59 WG1900474
(S) Phenol-d5 4165-62-2 14.9 0.000 10.0-67.0 07/27/2022 19:59 WG1900474
(S) 2-Fluorophenol 367-12-4 23.1 0.000 19.0-119 07/27/2022 19:59 WG1900474
(S) 2,4,6-Tribromophenol 118-79-6 71.0 0.000 43.0-140 07/27/2022 19:59 WG1900474
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 52 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 52 of 84
====================----□ □ □ □
□ □ □ □
SAMPLE RESULTS - 16
L1517739
USTG480-MW14
Collected date/time: 07/21/22 09:30
Volatile Petroleum Hydrocarbons by Method MADEPV
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics C5-C8 ALI
UNADJ 67.0 U 33.3 67.0 134 1 07/31/2022 17:29 WG1903095
Unadjusted C9-C12 Aliphatics C9-C12 ALI
UNADJ 54.7 B J 33.3 67.0 134 1 07/31/2022 17:29 WG1903095
Unadjusted C9-C10 Aromatics C9-C10 ARO
UNADJ 67.0 U 33.3 67.0 134 1 07/31/2022 17:29 WG1903095
Total VPH VPH 150 U 66.7 150 300 1 07/31/2022 17:29 WG1903095
(S) 2,5-Dibromotoluene(FID)615-59-8 94.2 70.0-130 07/31/2022 17:29 WG1903095
(S) 2,5-Dibromotoluene(PID)615-59-8 96.1 70.0-130 07/31/2022 17:29 WG1903095
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acetone 67-64-1 25.0 J3 U 11.3 25.0 50.0 1 07/25/2022 21:40 WG1900597
Acrolein 107-02-8 25.0 C4 U 2.54 25.0 50.0 1 07/25/2022 21:40 WG1900597
Acrylonitrile 107-13-1 5.00 J4 U 0.671 5.00 10.0 1 07/25/2022 21:40 WG1900597
Benzene 71-43-2 0.500 U 0.0941 0.500 1.00 1 07/25/2022 21:40 WG1900597
Bromobenzene 108-86-1 0.500 U 0.118 0.500 1.00 1 07/25/2022 21:40 WG1900597
Bromodichloromethane 75-27-4 0.500 U 0.136 0.500 1.00 1 07/25/2022 21:40 WG1900597
Bromoform 75-25-2 0.500 U 0.129 0.500 1.00 1 07/25/2022 21:40 WG1900597
Bromomethane 74-83-9 2.00 U 0.605 2.00 5.00 1 07/25/2022 21:40 WG1900597
n-Butylbenzene 104-51-8 0.500 U 0.157 0.500 1.00 1 07/25/2022 21:40 WG1900597
sec-Butylbenzene 135-98-8 0.500 U 0.125 0.500 1.00 1 07/25/2022 21:40 WG1900597
tert-Butylbenzene 98-06-6 0.500 U 0.127 0.500 1.00 1 07/25/2022 21:40 WG1900597
Carbon tetrachloride 56-23-5 0.500 U 0.128 0.500 1.00 1 07/25/2022 21:40 WG1900597
Chlorobenzene 108-90-7 0.500 U 0.116 0.500 1.00 1 07/25/2022 21:40 WG1900597
Chlorodibromomethane 124-48-1 0.500 U 0.140 0.500 1.00 1 07/25/2022 21:40 WG1900597
Chloroethane 75-00-3 2.00 U 0.192 2.00 5.00 1 07/25/2022 21:40 WG1900597
Chloroform 67-66-3 2.00 U 0.111 2.00 5.00 1 07/25/2022 21:40 WG1900597
Chloromethane 74-87-3 2.00 U 0.960 2.00 4.00 1 07/25/2022 21:40 WG1900597
2-Chlorotoluene 95-49-8 0.500 U 0.106 0.500 1.00 1 07/25/2022 21:40 WG1900597
4-Chlorotoluene 106-43-4 0.500 U 0.114 0.500 1.00 1 07/25/2022 21:40 WG1900597
1,2-Dibromo-3-Chloropropane 96-12-8 2.00 U 0.276 2.00 5.00 1 07/25/2022 21:40 WG1900597
1,2-Dibromoethane 106-93-4 0.500 U 0.126 0.500 1.00 1 07/25/2022 21:40 WG1900597
Dibromomethane 74-95-3 0.500 U 0.122 0.500 1.00 1 07/25/2022 21:40 WG1900597
1,2-Dichlorobenzene 95-50-1 0.500 U 0.107 0.500 1.00 1 07/25/2022 21:40 WG1900597
1,3-Dichlorobenzene 541-73-1 0.500 U 0.110 0.500 1.00 1 07/25/2022 21:40 WG1900597
1,4-Dichlorobenzene 106-46-7 0.500 U 0.120 0.500 1.00 1 07/25/2022 21:40 WG1900597
Dichlorodifluoromethane 75-71-8 2.00 U 0.374 2.00 5.00 1 07/25/2022 21:40 WG1900597
1,1-Dichloroethane 75-34-3 0.500 U 0.100 0.500 1.00 1 07/25/2022 21:40 WG1900597
1,2-Dichloroethane 107-06-2 0.500 U 0.0819 0.500 1.00 1 07/25/2022 21:40 WG1900597
1,1-Dichloroethene 75-35-4 0.500 U 0.188 0.500 1.00 1 07/25/2022 21:40 WG1900597
cis-1,2-Dichloroethene 156-59-2 0.500 U 0.126 0.500 1.00 1 07/25/2022 21:40 WG1900597
trans-1,2-Dichloroethene 156-60-5 0.500 U 0.149 0.500 1.00 1 07/25/2022 21:40 WG1900597
1,2-Dichloropropane 78-87-5 0.500 U 0.149 0.500 1.00 1 07/25/2022 21:40 WG1900597
1,1-Dichloropropene 563-58-6 0.500 U 0.142 0.500 1.00 1 07/25/2022 21:40 WG1900597
1,3-Dichloropropane 142-28-9 0.500 U 0.110 0.500 1.00 1 07/25/2022 21:40 WG1900597
2,2-Dichloropropane 594-20-7 0.500 U 0.161 0.500 1.00 1 07/25/2022 21:40 WG1900597
Di-isopropyl ether 108-20-3 0.500 U 0.105 0.500 1.00 1 07/25/2022 21:40 WG1900597
Ethylbenzene 100-41-4 0.500 U 0.137 0.500 1.00 1 07/25/2022 21:40 WG1900597
Hexachloro-1,3-butadiene 87-68-3 0.750 J3 U 0.337 0.750 1.50 1 07/25/2022 21:40 WG1900597
Isopropylbenzene 98-82-8 0.500 U 0.105 0.500 1.00 1 07/25/2022 21:40 WG1900597
p-Isopropyltoluene 99-87-6 0.500 U 0.120 0.500 1.00 1 07/25/2022 21:40 WG1900597
2-Butanone (MEK)78-93-3 5.00 U 1.19 5.00 10.0 1 07/25/2022 21:40 WG1900597
Methylene Chloride 75-09-2 2.00 U 0.430 2.00 5.00 1 07/25/2022 21:40 WG1900597
4-Methyl-2-pentanone (MIBK)108-10-1 5.00 U 0.478 5.00 10.0 1 07/25/2022 21:40 WG1900597
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 53 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 53 of 84
--------------=---□
□ □ □
==============~~~~~=----□ □ □ □
SAMPLE RESULTS - 16
L1517739
USTG480-MW14
Collected date/time: 07/21/22 09:30
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Methyl tert-butyl ether 1634-04-4 0.500 U 0.101 0.500 1.00 1 07/25/2022 21:40 WG1900597
Naphthalene 91-20-3 2.00 U 1.00 2.00 5.00 1 07/25/2022 21:40 WG1900597
n-Propylbenzene 103-65-1 0.500 U 0.0993 0.500 1.00 1 07/25/2022 21:40 WG1900597
Styrene 100-42-5 0.500 U 0.118 0.500 1.00 1 07/25/2022 21:40 WG1900597
1,1,1,2-Tetrachloroethane 630-20-6 0.500 U 0.147 0.500 1.00 1 07/25/2022 21:40 WG1900597
1,1,2,2-Tetrachloroethane 79-34-5 0.500 U 0.133 0.500 1.00 1 07/25/2022 21:40 WG1900597
Tetrachloroethene 127-18-4 0.600 U 0.300 0.600 1.20 1 07/25/2022 21:40 WG1900597
Toluene 108-88-3 0.600 U 0.278 0.600 1.20 1 07/25/2022 21:40 WG1900597
1,2,3-Trichlorobenzene 87-61-6 0.500 U 0.230 0.500 1.00 1 07/25/2022 21:40 WG1900597
1,2,4-Trichlorobenzene 120-82-1 1.00 U 0.481 1.00 2.00 1 07/25/2022 21:40 WG1900597
1,1,1-Trichloroethane 71-55-6 0.500 U 0.149 0.500 1.00 1 07/25/2022 21:40 WG1900597
1,1,2-Trichloroethane 79-00-5 0.500 U 0.158 0.500 1.00 1 07/25/2022 21:40 WG1900597
Trichloroethene 79-01-6 0.500 U 0.190 0.500 1.00 1 07/25/2022 21:40 WG1900597
Trichlorofluoromethane 75-69-4 2.00 U 0.160 2.00 5.00 1 07/25/2022 21:40 WG1900597
1,2,3-Trichloropropane 96-18-4 1.00 U 0.237 1.00 2.50 1 07/25/2022 21:40 WG1900597
1,2,4-Trimethylbenzene 95-63-6 1.00 U 0.322 1.00 2.00 1 07/25/2022 21:40 WG1900597
1,3,5-Trimethylbenzene 108-67-8 0.500 U 0.104 0.500 1.00 1 07/25/2022 21:40 WG1900597
Vinyl chloride 75-01-4 0.500 U 0.234 0.500 1.00 1 07/25/2022 21:40 WG1900597
o-Xylene 95-47-6 0.500 U 0.174 0.500 1.00 1 07/25/2022 21:40 WG1900597
m&p-Xylenes 1330-20-7 1.00 U 0.430 1.00 2.00 1 07/25/2022 21:40 WG1900597
(S) Toluene-d8 2037-26-5 97.1 89.0-112 07/25/2022 21:40 WG1900597
(S) 4-Bromofluorobenzene 460-00-4 102 85.0-114 07/25/2022 21:40 WG1900597
(S) 1,2-Dichloroethane-d4 17060-07-0 107 81.0-118 07/25/2022 21:40 WG1900597
TPH by Method MADEPE
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics C9-C18 ALI
UNADJ 67.0 U 33.3 67.0 134 1 08/06/2022 01:55 WG1905723
Unadjusted C19-C36 Aliphatics C19-C36 ALI
UNADJ 67.0 U 33.3 67.0 134 1 08/06/2022 01:55 WG1905723
Unadjusted C11-C22 Aromatics C11-C22 ARO
UNADJ 67.0 U 33.3 67.0 134 1 08/06/2022 03:50 WG1905723
Unadjusted Total Petroleum
Hydrocarbons TPH UNADJ 67.0 U 33.3 67.0 134 1 08/06/2022 01:55 WG1905723
(S) o-Terphenyl 84-15-1 64.4 40.0-140 08/06/2022 03:50 WG1905723
(S) 1-Chloro-octadecane 3386-33-2 48.7 40.0-140 08/06/2022 01:55 WG1905723
(S) 2-Fluorobiphenyl 321-60-8 87.9 40.0-140 08/06/2022 03:50 WG1905723
(S) 2-Bromonaphthalene 580-13-2 87.2 40.0-140 08/06/2022 03:50 WG1905723
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acenaphthene 83-32-9 0.500 U 0.0886 0.500 1.00 1 08/01/2022 18:20 WG1901647
Acenaphthylene 208-96-8 0.500 U 0.0921 0.500 1.00 1 08/01/2022 18:20 WG1901647
Anthracene 120-12-7 0.500 U 0.0804 0.500 1.00 1 08/01/2022 18:20 WG1901647
Benzidine 92-87-5 7.50 U 3.74 7.50 15.0 1 08/01/2022 18:20 WG1901647
Benzo(a)anthracene 56-55-3 0.500 U 0.199 0.500 1.00 1 08/01/2022 18:20 WG1901647
Benzo(b)fluoranthene 205-99-2 0.500 U 0.130 0.500 1.00 1 08/01/2022 18:20 WG1901647
Benzo(k)fluoranthene 207-08-9 0.500 U 0.120 0.500 1.00 1 08/01/2022 18:20 WG1901647
Benzo(g,h,i)perylene 191-24-2 0.500 U 0.121 0.500 1.00 1 08/01/2022 18:20 WG1901647
Benzo(a)pyrene 50-32-8 0.500 U 0.0381 0.500 1.00 1 08/01/2022 18:20 WG1901647
Bis(2-chlorethoxy)methane 111-91-1 5.00 U 0.116 5.00 10.0 1 08/01/2022 18:20 WG1901647
Bis(2-chloroethyl)ether 111-44-4 5.00 U 0.137 5.00 10.0 1 08/01/2022 18:20 WG1901647
2,2-Oxybis(1-Chloropropane)108-60-1 5.00 U 0.210 5.00 10.0 1 08/01/2022 18:20 WG1901647
4-Bromophenyl-phenylether 101-55-3 5.00 U 0.0877 5.00 10.0 1 08/01/2022 18:20 WG1901647
2-Chloronaphthalene 91-58-7 0.500 U 0.0648 0.500 1.00 1 08/01/2022 18:20 WG1901647
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 54 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 54 of 84
====================----□ □ □ □
□ □ □ □
SAMPLE RESULTS - 16
L1517739
USTG480-MW14
Collected date/time: 07/21/22 09:30
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
4-Chlorophenyl-phenylether 7005-72-3 5.00 U 0.0926 5.00 10.0 1 08/01/2022 18:20 WG1901647
Chrysene 218-01-9 0.500 U 0.130 0.500 1.00 1 08/01/2022 18:20 WG1901647
Dibenz(a,h)anthracene 53-70-3 0.500 U 0.0644 0.500 1.00 1 08/01/2022 18:20 WG1901647
3,3-Dichlorobenzidine 91-94-1 5.00 U 0.212 5.00 10.0 1 08/01/2022 18:20 WG1901647
2,4-Dinitrotoluene 121-14-2 5.00 U 0.0983 5.00 10.0 1 08/01/2022 18:20 WG1901647
2,6-Dinitrotoluene 606-20-2 5.00 U 0.250 5.00 10.0 1 08/01/2022 18:20 WG1901647
Fluoranthene 206-44-0 0.500 U 0.102 0.500 1.00 1 08/01/2022 18:20 WG1901647
Fluorene 86-73-7 0.500 U 0.0844 0.500 1.00 1 08/01/2022 18:20 WG1901647
Hexachlorobenzene 118-74-1 0.500 U 0.0755 0.500 1.00 1 08/01/2022 18:20 WG1901647
Hexachloro-1,3-butadiene 87-68-3 5.00 U 0.0968 5.00 10.0 1 08/01/2022 18:20 WG1901647
Hexachlorocyclopentadiene 77-47-4 5.00 C6 U 0.0598 5.00 10.0 1 08/01/2022 18:20 WG1901647
Hexachloroethane 67-72-1 5.00 U 0.127 5.00 10.0 1 08/01/2022 18:20 WG1901647
Indeno(1,2,3-cd)pyrene 193-39-5 0.600 U 0.279 0.600 1.20 1 08/01/2022 18:20 WG1901647
Isophorone 78-59-1 5.00 U 0.143 5.00 10.0 1 08/01/2022 18:20 WG1901647
Naphthalene 91-20-3 0.500 U 0.159 0.500 1.00 1 08/01/2022 18:20 WG1901647
Nitrobenzene 98-95-3 5.00 U 0.297 5.00 10.0 1 08/01/2022 18:20 WG1901647
n-Nitrosodimethylamine 62-75-9 5.00 U 0.998 5.00 10.0 1 08/01/2022 18:20 WG1901647
n-Nitrosodiphenylamine 86-30-6 5.00 U 2.37 5.00 10.0 1 08/01/2022 18:20 WG1901647
n-Nitrosodi-n-propylamine 621-64-7 5.00 U 0.261 5.00 10.0 1 08/01/2022 18:20 WG1901647
Phenanthrene 85-01-8 0.500 U 0.112 0.500 1.00 1 08/01/2022 18:20 WG1901647
Benzylbutyl phthalate 85-68-7 2.00 U 0.765 2.00 4.00 1 08/01/2022 18:20 WG1901647
Bis(2-ethylhexyl)phthalate 117-81-7 2.00 U 0.895 2.00 4.00 1 08/01/2022 18:20 WG1901647
Di-n-butyl phthalate 84-74-2 1.50 U 0.453 1.50 3.00 1 08/01/2022 18:20 WG1901647
Diethyl phthalate 84-66-2 1.50 U 0.287 1.50 3.00 1 08/01/2022 18:20 WG1901647
Dimethyl phthalate 131-11-3 1.50 U 0.260 1.50 3.00 1 08/01/2022 18:20 WG1901647
Di-n-octyl phthalate 117-84-0 2.00 U 0.932 2.00 4.00 1 08/01/2022 18:20 WG1901647
Pyrene 129-00-0 0.500 U 0.107 0.500 1.00 1 08/01/2022 18:20 WG1901647
1,2,4-Trichlorobenzene 120-82-1 5.00 U 0.0698 5.00 10.0 1 08/01/2022 18:20 WG1901647
4-Chloro-3-methylphenol 59-50-7 5.00 U 0.131 5.00 10.0 1 08/01/2022 18:20 WG1901647
2-Chlorophenol 95-57-8 5.00 U 0.133 5.00 10.0 1 08/01/2022 18:20 WG1901647
2,4-Dichlorophenol 120-83-2 5.00 U 0.102 5.00 10.0 1 08/01/2022 18:20 WG1901647
2,4-Dimethylphenol 105-67-9 5.00 U 0.0636 5.00 10.0 1 08/01/2022 18:20 WG1901647
4,6-Dinitro-2-methylphenol 534-52-1 5.00 U 1.12 5.00 10.0 1 08/01/2022 18:20 WG1901647
2,4-Dinitrophenol 51-28-5 15.0 U 5.93 15.0 30.0 1 08/01/2022 18:20 WG1901647
2-Nitrophenol 88-75-5 5.00 U 0.117 5.00 10.0 1 08/01/2022 18:20 WG1901647
4-Nitrophenol 100-02-7 5.00 U 0.143 5.00 10.0 1 08/01/2022 18:20 WG1901647
Pentachlorophenol 87-86-5 5.00 U 0.313 5.00 10.0 1 08/01/2022 18:20 WG1901647
Phenol 108-95-2 10.0 U 4.33 10.0 20.0 1 08/01/2022 18:20 WG1901647
2,4,6-Trichlorophenol 88-06-2 5.00 U 0.100 5.00 10.0 1 08/01/2022 18:20 WG1901647
1-Methylnaphthalene 90-12-0 0.500 U 0.0790 0.500 1.00 1 08/01/2022 18:20 WG1901647
2-Methylnaphthalene 91-57-6 0.500 U 0.117 0.500 1.00 1 08/01/2022 18:20 WG1901647
(S) Nitrobenzene-d5 4165-60-0 60.9 0.000 44.0-120 08/01/2022 18:20 WG1901647
(S) 2-Fluorobiphenyl 321-60-8 55.0 0.000 44.0-119 08/01/2022 18:20 WG1901647
(S) p-Terphenyl-d14 1718-51-0 65.8 0.000 50.0-134 08/01/2022 18:20 WG1901647
(S) Phenol-d5 4165-62-2 33.2 0.000 10.0-67.0 08/01/2022 18:20 WG1901647
(S) 2-Fluorophenol 367-12-4 33.2 0.000 19.0-119 08/01/2022 18:20 WG1901647
(S) 2,4,6-Tribromophenol 118-79-6 84.5 0.000 43.0-140 08/01/2022 18:20 WG1901647
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 55 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 55 of 84
====================----□ □ □ □
□ □ □ □
SAMPLE RESULTS - 17
L1517739
USTG480-MW28
Collected date/time: 07/21/22 11:00
Volatile Petroleum Hydrocarbons by Method MADEPV
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics C5-C8 ALI
UNADJ 185 B 33.3 67.0 134 1 08/03/2022 09:02 WG1903796
Unadjusted C9-C12 Aliphatics C9-C12 ALI
UNADJ 599 33.3 67.0 134 1 08/03/2022 09:02 WG1903796
Unadjusted C9-C10 Aromatics C9-C10 ARO
UNADJ 701 33.3 67.0 134 1 08/03/2022 09:02 WG1903796
Total VPH VPH 1490 66.7 150 300 1 08/03/2022 09:02 WG1903796
(S) 2,5-Dibromotoluene(FID)615-59-8 122 70.0-130 08/03/2022 09:02 WG1903796
(S) 2,5-Dibromotoluene(PID)615-59-8 83.3 70.0-130 08/03/2022 09:02 WG1903796
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acetone 67-64-1 250 J3 U 113 250 500 10 07/25/2022 23:24 WG1900597
Acrolein 107-02-8 250 C4 U 25.4 250 500 10 07/25/2022 23:24 WG1900597
Acrylonitrile 107-13-1 50.0 J4 U 6.71 50.0 100 10 07/25/2022 23:24 WG1900597
Benzene 71-43-2 80.4 0.941 5.00 10.0 10 07/25/2022 23:24 WG1900597
Bromobenzene 108-86-1 5.00 U 1.18 5.00 10.0 10 07/25/2022 23:24 WG1900597
Bromodichloromethane 75-27-4 5.00 U 1.36 5.00 10.0 10 07/25/2022 23:24 WG1900597
Bromoform 75-25-2 5.00 U 1.29 5.00 10.0 10 07/25/2022 23:24 WG1900597
Bromomethane 74-83-9 20.0 U 6.05 20.0 50.0 10 07/25/2022 23:24 WG1900597
n-Butylbenzene 104-51-8 7.09 J 1.57 5.00 10.0 10 07/25/2022 23:24 WG1900597
sec-Butylbenzene 135-98-8 8.01 J 1.25 5.00 10.0 10 07/25/2022 23:24 WG1900597
tert-Butylbenzene 98-06-6 1.51 J 1.27 5.00 10.0 10 07/25/2022 23:24 WG1900597
Carbon tetrachloride 56-23-5 5.00 U 1.28 5.00 10.0 10 07/25/2022 23:24 WG1900597
Chlorobenzene 108-90-7 5.00 U 1.16 5.00 10.0 10 07/25/2022 23:24 WG1900597
Chlorodibromomethane 124-48-1 5.00 U 1.40 5.00 10.0 10 07/25/2022 23:24 WG1900597
Chloroethane 75-00-3 20.0 U 1.92 20.0 50.0 10 07/25/2022 23:24 WG1900597
Chloroform 67-66-3 20.0 U 1.11 20.0 50.0 10 07/25/2022 23:24 WG1900597
Chloromethane 74-87-3 20.0 U 9.60 20.0 40.0 10 07/25/2022 23:24 WG1900597
2-Chlorotoluene 95-49-8 5.00 U 1.06 5.00 10.0 10 07/25/2022 23:24 WG1900597
4-Chlorotoluene 106-43-4 5.00 U 1.14 5.00 10.0 10 07/25/2022 23:24 WG1900597
1,2-Dibromo-3-Chloropropane 96-12-8 20.0 U 2.76 20.0 50.0 10 07/25/2022 23:24 WG1900597
1,2-Dibromoethane 106-93-4 5.00 U 1.26 5.00 10.0 10 07/25/2022 23:24 WG1900597
Dibromomethane 74-95-3 5.00 U 1.22 5.00 10.0 10 07/25/2022 23:24 WG1900597
1,2-Dichlorobenzene 95-50-1 5.00 U 1.07 5.00 10.0 10 07/25/2022 23:24 WG1900597
1,3-Dichlorobenzene 541-73-1 5.00 U 1.10 5.00 10.0 10 07/25/2022 23:24 WG1900597
1,4-Dichlorobenzene 106-46-7 5.00 U 1.20 5.00 10.0 10 07/25/2022 23:24 WG1900597
Dichlorodifluoromethane 75-71-8 20.0 U 3.74 20.0 50.0 10 07/25/2022 23:24 WG1900597
1,1-Dichloroethane 75-34-3 5.00 U 1.00 5.00 10.0 10 07/25/2022 23:24 WG1900597
1,2-Dichloroethane 107-06-2 5.00 U 0.819 5.00 10.0 10 07/25/2022 23:24 WG1900597
1,1-Dichloroethene 75-35-4 5.00 U 1.88 5.00 10.0 10 07/25/2022 23:24 WG1900597
cis-1,2-Dichloroethene 156-59-2 5.00 U 1.26 5.00 10.0 10 07/25/2022 23:24 WG1900597
trans-1,2-Dichloroethene 156-60-5 5.00 U 1.49 5.00 10.0 10 07/25/2022 23:24 WG1900597
1,2-Dichloropropane 78-87-5 5.00 U 1.49 5.00 10.0 10 07/25/2022 23:24 WG1900597
1,1-Dichloropropene 563-58-6 5.00 U 1.42 5.00 10.0 10 07/25/2022 23:24 WG1900597
1,3-Dichloropropane 142-28-9 5.00 U 1.10 5.00 10.0 10 07/25/2022 23:24 WG1900597
2,2-Dichloropropane 594-20-7 5.00 U 1.61 5.00 10.0 10 07/25/2022 23:24 WG1900597
Di-isopropyl ether 108-20-3 5.00 U 1.05 5.00 10.0 10 07/25/2022 23:24 WG1900597
Ethylbenzene 100-41-4 42.7 1.37 5.00 10.0 10 07/25/2022 23:24 WG1900597
Hexachloro-1,3-butadiene 87-68-3 7.50 J3 U 3.37 7.50 15.0 10 07/25/2022 23:24 WG1900597
Isopropylbenzene 98-82-8 31.0 1.05 5.00 10.0 10 07/25/2022 23:24 WG1900597
p-Isopropyltoluene 99-87-6 7.42 J 1.20 5.00 10.0 10 07/25/2022 23:24 WG1900597
2-Butanone (MEK)78-93-3 50.0 U 11.9 50.0 100 10 07/25/2022 23:24 WG1900597
Methylene Chloride 75-09-2 20.0 U 4.30 20.0 50.0 10 07/25/2022 23:24 WG1900597
4-Methyl-2-pentanone (MIBK)108-10-1 50.0 U 4.78 50.0 100 10 07/25/2022 23:24 WG1900597
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 56 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 56 of 84
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SAMPLE RESULTS - 17
L1517739
USTG480-MW28
Collected date/time: 07/21/22 11:00
Volatile Organic Compounds (GC/MS) by Method 6200B-2011
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Methyl tert-butyl ether 1634-04-4 5.00 U 1.01 5.00 10.0 10 07/25/2022 23:24 WG1900597
Naphthalene 91-20-3 446 10.0 20.0 50.0 10 07/25/2022 23:24 WG1900597
n-Propylbenzene 103-65-1 46.0 0.993 5.00 10.0 10 07/25/2022 23:24 WG1900597
Styrene 100-42-5 5.00 U 1.18 5.00 10.0 10 07/25/2022 23:24 WG1900597
1,1,1,2-Tetrachloroethane 630-20-6 5.00 U 1.47 5.00 10.0 10 07/25/2022 23:24 WG1900597
1,1,2,2-Tetrachloroethane 79-34-5 5.00 U 1.33 5.00 10.0 10 07/25/2022 23:24 WG1900597
Tetrachloroethene 127-18-4 6.00 U 3.00 6.00 12.0 10 07/25/2022 23:24 WG1900597
Toluene 108-88-3 6.00 U 2.78 6.00 12.0 10 07/25/2022 23:24 WG1900597
1,2,3-Trichlorobenzene 87-61-6 5.00 U 2.30 5.00 10.0 10 07/25/2022 23:24 WG1900597
1,2,4-Trichlorobenzene 120-82-1 10.0 U 4.81 10.0 20.0 10 07/25/2022 23:24 WG1900597
1,1,1-Trichloroethane 71-55-6 5.00 U 1.49 5.00 10.0 10 07/25/2022 23:24 WG1900597
1,1,2-Trichloroethane 79-00-5 5.00 U 1.58 5.00 10.0 10 07/25/2022 23:24 WG1900597
Trichloroethene 79-01-6 5.00 U 1.90 5.00 10.0 10 07/25/2022 23:24 WG1900597
Trichlorofluoromethane 75-69-4 20.0 U 1.60 20.0 50.0 10 07/25/2022 23:24 WG1900597
1,2,3-Trichloropropane 96-18-4 10.0 U 2.37 10.0 25.0 10 07/25/2022 23:24 WG1900597
1,2,4-Trimethylbenzene 95-63-6 216 3.22 10.0 20.0 10 07/25/2022 23:24 WG1900597
1,3,5-Trimethylbenzene 108-67-8 26.8 1.04 5.00 10.0 10 07/25/2022 23:24 WG1900597
Vinyl chloride 75-01-4 5.00 U 2.34 5.00 10.0 10 07/25/2022 23:24 WG1900597
o-Xylene 95-47-6 4.28 J 1.74 5.00 10.0 10 07/25/2022 23:24 WG1900597
m&p-Xylenes 1330-20-7 110 4.30 10.0 20.0 10 07/25/2022 23:24 WG1900597
(S) Toluene-d8 2037-26-5 98.1 89.0-112 07/25/2022 23:24 WG1900597
(S) 4-Bromofluorobenzene 460-00-4 102 85.0-114 07/25/2022 23:24 WG1900597
(S) 1,2-Dichloroethane-d4 17060-07-0 104 81.0-118 07/25/2022 23:24 WG1900597
TPH by Method MADEPE
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics C9-C18 ALI
UNADJ 2120 33.3 67.0 134 1 08/06/2022 02:18 WG1905723
Unadjusted C19-C36 Aliphatics C19-C36 ALI
UNADJ 420 33.3 67.0 134 1 08/06/2022 02:18 WG1905723
Unadjusted C11-C22 Aromatics C11-C22 ARO
UNADJ 2110 33.3 67.0 134 1 08/06/2022 04:13 WG1905723
Unadjusted Total Petroleum
Hydrocarbons TPH UNADJ 4650 33.3 67.0 134 1 08/06/2022 04:13 WG1905723
(S) o-Terphenyl 84-15-1 71.1 40.0-140 08/06/2022 04:13 WG1905723
(S) 1-Chloro-octadecane 3386-33-2 63.0 40.0-140 08/06/2022 02:18 WG1905723
(S) 2-Fluorobiphenyl 321-60-8 83.2 40.0-140 08/06/2022 04:13 WG1905723
(S) 2-Bromonaphthalene 580-13-2 76.9 40.0-140 08/06/2022 04:13 WG1905723
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
Acenaphthene 83-32-9 3.25 0.0886 0.500 1.00 1 08/01/2022 18:42 WG1901647
Acenaphthylene 208-96-8 0.500 U 0.0921 0.500 1.00 1 08/01/2022 18:42 WG1901647
Anthracene 120-12-7 0.665 J 0.0804 0.500 1.00 1 08/01/2022 18:42 WG1901647
Benzidine 92-87-5 7.50 U 3.74 7.50 15.0 1 08/01/2022 18:42 WG1901647
Benzo(a)anthracene 56-55-3 0.500 U 0.199 0.500 1.00 1 08/01/2022 18:42 WG1901647
Benzo(b)fluoranthene 205-99-2 0.500 U 0.130 0.500 1.00 1 08/01/2022 18:42 WG1901647
Benzo(k)fluoranthene 207-08-9 0.500 U 0.120 0.500 1.00 1 08/01/2022 18:42 WG1901647
Benzo(g,h,i)perylene 191-24-2 0.500 U 0.121 0.500 1.00 1 08/01/2022 18:42 WG1901647
Benzo(a)pyrene 50-32-8 0.500 U 0.0381 0.500 1.00 1 08/01/2022 18:42 WG1901647
Bis(2-chlorethoxy)methane 111-91-1 5.00 U 0.116 5.00 10.0 1 08/01/2022 18:42 WG1901647
Bis(2-chloroethyl)ether 111-44-4 5.00 U 0.137 5.00 10.0 1 08/01/2022 18:42 WG1901647
2,2-Oxybis(1-Chloropropane)108-60-1 5.00 U 0.210 5.00 10.0 1 08/01/2022 18:42 WG1901647
4-Bromophenyl-phenylether 101-55-3 5.00 U 0.0877 5.00 10.0 1 08/01/2022 18:42 WG1901647
2-Chloronaphthalene 91-58-7 0.500 U 0.0648 0.500 1.00 1 08/01/2022 18:42 WG1901647
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 57 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 57 of 84
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SAMPLE RESULTS - 17
L1517739
USTG480-MW28
Collected date/time: 07/21/22 11:00
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
CAS #Result Qualifier DL LOD LOQ Dilution Analysis Batch
Analyte ug/l ug/l ug/l ug/l date / time
4-Chlorophenyl-phenylether 7005-72-3 5.00 U 0.0926 5.00 10.0 1 08/01/2022 18:42 WG1901647
Chrysene 218-01-9 0.500 U 0.130 0.500 1.00 1 08/01/2022 18:42 WG1901647
Dibenz(a,h)anthracene 53-70-3 0.500 U 0.0644 0.500 1.00 1 08/01/2022 18:42 WG1901647
3,3-Dichlorobenzidine 91-94-1 5.00 U 0.212 5.00 10.0 1 08/01/2022 18:42 WG1901647
2,4-Dinitrotoluene 121-14-2 5.00 U 0.0983 5.00 10.0 1 08/01/2022 18:42 WG1901647
2,6-Dinitrotoluene 606-20-2 5.00 U 0.250 5.00 10.0 1 08/01/2022 18:42 WG1901647
Fluoranthene 206-44-0 0.106 J 0.102 0.500 1.00 1 08/01/2022 18:42 WG1901647
Fluorene 86-73-7 5.26 0.0844 0.500 1.00 1 08/01/2022 18:42 WG1901647
Hexachlorobenzene 118-74-1 0.500 U 0.0755 0.500 1.00 1 08/01/2022 18:42 WG1901647
Hexachloro-1,3-butadiene 87-68-3 5.00 U 0.0968 5.00 10.0 1 08/01/2022 18:42 WG1901647
Hexachlorocyclopentadiene 77-47-4 5.00 C6 U 0.0598 5.00 10.0 1 08/01/2022 18:42 WG1901647
Hexachloroethane 67-72-1 5.00 U 0.127 5.00 10.0 1 08/01/2022 18:42 WG1901647
Indeno(1,2,3-cd)pyrene 193-39-5 0.600 U 0.279 0.600 1.20 1 08/01/2022 18:42 WG1901647
Isophorone 78-59-1 5.00 U 0.143 5.00 10.0 1 08/01/2022 18:42 WG1901647
Naphthalene 91-20-3 111 0.159 0.500 1.00 1 08/01/2022 18:42 WG1901647
Nitrobenzene 98-95-3 5.00 U 0.297 5.00 10.0 1 08/01/2022 18:42 WG1901647
n-Nitrosodimethylamine 62-75-9 5.00 U 0.998 5.00 10.0 1 08/01/2022 18:42 WG1901647
n-Nitrosodiphenylamine 86-30-6 5.00 U 2.37 5.00 10.0 1 08/01/2022 18:42 WG1901647
n-Nitrosodi-n-propylamine 621-64-7 5.00 U 0.261 5.00 10.0 1 08/01/2022 18:42 WG1901647
Phenanthrene 85-01-8 6.55 0.112 0.500 1.00 1 08/01/2022 18:42 WG1901647
Benzylbutyl phthalate 85-68-7 2.00 U 0.765 2.00 4.00 1 08/01/2022 18:42 WG1901647
Bis(2-ethylhexyl)phthalate 117-81-7 2.00 U 0.895 2.00 4.00 1 08/01/2022 18:42 WG1901647
Di-n-butyl phthalate 84-74-2 1.50 U 0.453 1.50 3.00 1 08/01/2022 18:42 WG1901647
Diethyl phthalate 84-66-2 1.50 U 0.287 1.50 3.00 1 08/01/2022 18:42 WG1901647
Dimethyl phthalate 131-11-3 1.50 U 0.260 1.50 3.00 1 08/01/2022 18:42 WG1901647
Di-n-octyl phthalate 117-84-0 2.00 U 0.932 2.00 4.00 1 08/01/2022 18:42 WG1901647
Pyrene 129-00-0 0.215 J 0.107 0.500 1.00 1 08/01/2022 18:42 WG1901647
1,2,4-Trichlorobenzene 120-82-1 5.00 U 0.0698 5.00 10.0 1 08/01/2022 18:42 WG1901647
4-Chloro-3-methylphenol 59-50-7 5.00 U 0.131 5.00 10.0 1 08/01/2022 18:42 WG1901647
2-Chlorophenol 95-57-8 5.00 U 0.133 5.00 10.0 1 08/01/2022 18:42 WG1901647
2,4-Dichlorophenol 120-83-2 5.00 U 0.102 5.00 10.0 1 08/01/2022 18:42 WG1901647
2,4-Dimethylphenol 105-67-9 5.00 U 0.0636 5.00 10.0 1 08/01/2022 18:42 WG1901647
4,6-Dinitro-2-methylphenol 534-52-1 5.00 U 1.12 5.00 10.0 1 08/01/2022 18:42 WG1901647
2,4-Dinitrophenol 51-28-5 15.0 U 5.93 15.0 30.0 1 08/01/2022 18:42 WG1901647
2-Nitrophenol 88-75-5 5.00 U 0.117 5.00 10.0 1 08/01/2022 18:42 WG1901647
4-Nitrophenol 100-02-7 5.00 U 0.143 5.00 10.0 1 08/01/2022 18:42 WG1901647
Pentachlorophenol 87-86-5 5.00 U 0.313 5.00 10.0 1 08/01/2022 18:42 WG1901647
Phenol 108-95-2 10.0 U 4.33 10.0 20.0 1 08/01/2022 18:42 WG1901647
2,4,6-Trichlorophenol 88-06-2 5.00 U 0.100 5.00 10.0 1 08/01/2022 18:42 WG1901647
1-Methylnaphthalene 90-12-0 93.5 0.0790 0.500 1.00 1 08/01/2022 18:42 WG1901647
2-Methylnaphthalene 91-57-6 118 0.117 0.500 1.00 1 08/01/2022 18:42 WG1901647
(S) Nitrobenzene-d5 4165-60-0 55.6 0.000 44.0-120 08/01/2022 18:42 WG1901647
(S) 2-Fluorobiphenyl 321-60-8 52.7 0.000 44.0-119 08/01/2022 18:42 WG1901647
(S) p-Terphenyl-d14 1718-51-0 56.9 0.000 50.0-134 08/01/2022 18:42 WG1901647
(S) Phenol-d5 4165-62-2 33.6 0.000 10.0-67.0 08/01/2022 18:42 WG1901647
(S) 2-Fluorophenol 367-12-4 32.4 0.000 19.0-119 08/01/2022 18:42 WG1901647
(S) 2,4,6-Tribromophenol 118-79-6 77.5 0.000 43.0-140 08/01/2022 18:42 WG1901647
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 58 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 58 of 84
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QUALITY CONTROL SUMMARYWG1902102
Volatile Petroleum Hydrocarbons by Method MADEPV L1517739-01,02,03,04,05,06,07,08,09
Method Blank (MB)
(MB) R3820886-3 07/29/22 17:09
MB Result MB Qualifier MB DL MB LOD MB LOQ
Analyte ug/l ug/l ug/l ug/l
Unadjusted C5-C8 Aliphatics 67.0 U 33.3 67.0 100
Unadjusted C9-C12 Aliphatics 40.5 J 33.3 67.0 134
Unadjusted C9-C10 Aromatics 67.0 U 33.3 67.0 100
Total VPH 150 U 66.7 150 300
(S) 2,5-Dibromotoluene(FID)89.1 70.0-130
(S) 2,5-Dibromotoluene(PID)93.1 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3820886-1 07/29/22 14:59 • (LCSD) R3820886-2 07/29/22 15:31
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C5-C8 Aliphatics 1200 1010 969 84.2 80.7 70.0-130 4.14 50
Unadjusted C9-C12 Aliphatics 1400 1190 1210 85.0 86.4 70.0-130 1.67 50
Unadjusted C9-C10 Aromatics 200 192 194 96.0 97.0 70.0-130 1.04 50
Total VPH 2800 2390 2370 85.4 84.6 70.0-130 0.840 50
(S) 2,5-Dibromotoluene(FID) 91.5 86.4 70.0-130
(S) 2,5-Dibromotoluene(PID) 93.9 90.4 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 59 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 59 of 84
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QUALITY CONTROL SUMMARYWG1903095
Volatile Petroleum Hydrocarbons by Method MADEPV L1517739-10,11,12,13,14,15,16
Method Blank (MB)
(MB) R3821180-3 07/31/22 11:29
MB Result MB Qualifier MB DL MB LOD MB LOQ
Analyte ug/l ug/l ug/l ug/l
Unadjusted C5-C8 Aliphatics 67.0 U 33.3 67.0 134
Unadjusted C9-C12 Aliphatics 42.3 J 33.3 67.0 134
Unadjusted C9-C10 Aromatics 67.0 U 33.3 67.0 134
Total VPH 150 U 66.7 150 300
(S) 2,5-Dibromotoluene(FID)96.3 70.0-130
(S) 2,5-Dibromotoluene(PID)101 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3821180-1 07/31/22 09:18 • (LCSD) R3821180-2 07/31/22 09:51
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C5-C8 Aliphatics 1200 1100 1140 91.7 95.0 70.0-130 3.57 50
Unadjusted C9-C12 Aliphatics 1400 1150 1180 82.1 84.3 70.0-130 2.58 50
Unadjusted C9-C10 Aromatics 200 185 186 92.5 93.0 70.0-130 0.539 50
Total VPH 2800 2440 2510 87.1 89.6 70.0-130 2.83 50
(S) 2,5-Dibromotoluene(FID) 94.6 95.6 70.0-130
(S) 2,5-Dibromotoluene(PID) 95.1 95.0 70.0-130
L1517888-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1517888-01 07/31/22 18:02 • (MS) R3821180-4 08/01/22 00:02 • (MSD) R3821180-5 08/01/22 00:35
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Unadjusted C5-C8 Aliphatics 1200 116 1020 1200 75.3 90.3 1 70.0-130 16.2 50
Unadjusted C9-C12 Aliphatics 1400 67.0 1120 1430 80.0 102 1 70.0-130 24.3 50
Unadjusted C9-C10 Aromatics 200 37.5 196 237 79.2 99.8 1 70.0-130 18.9 50
Total VPH 2800 150 2340 2870 83.6 103 1 70.0-130 20.3 50
(S) 2,5-Dibromotoluene(FID) 92.9 97.8 70.0-130
(S) 2,5-Dibromotoluene(PID) 91.5 93.4 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 60 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 60 of 84
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QUALITY CONTROL SUMMARYWG1903796
Volatile Petroleum Hydrocarbons by Method MADEPV L1517739-11,12,17
Method Blank (MB)
(MB) R3822160-3 08/02/22 21:30
MB Result MB Qualifier MB DL MB LOD MB LOQ
Analyte ug/l ug/l ug/l ug/l
Unadjusted C5-C8 Aliphatics 53.5 J 33.3 67.0 134
Unadjusted C9-C12 Aliphatics 44.7 J 33.3 67.0 134
Unadjusted C9-C10 Aromatics 67.0 U 33.3 67.0 134
Total VPH 98.2 J 66.7 150 300
(S) 2,5-Dibromotoluene(FID)86.1 70.0-130
(S) 2,5-Dibromotoluene(PID)90.1 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3822160-1 08/02/22 19:19 • (LCSD) R3822160-2 08/02/22 19:51
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C5-C8 Aliphatics 1200 1010 988 84.2 82.3 70.0-130 2.20 50
Unadjusted C9-C12 Aliphatics 1400 1200 1210 85.7 86.4 70.0-130 0.830 50
Unadjusted C9-C10 Aromatics 200 181 181 90.5 90.5 70.0-130 0.000 50
Total VPH 2800 2390 2380 85.4 85.0 70.0-130 0.419 50
(S) 2,5-Dibromotoluene(FID) 86.1 86.1 70.0-130
(S) 2,5-Dibromotoluene(PID) 90.0 90.2 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:02 61 of 84
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Cherokee Nation 3S 221102 L1517739 08/10/22 17:57 61 of 84
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QUALITY CONTROL SUMMARYWG1900597
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1517739-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17
Method Blank (MB)
(MB) R3822215-3 07/25/22 16:23
MB Result MB Qualifier MB DL MB LOD MB LOQ
Analyte ug/l ug/l ug/l ug/l
Acetone 25.0 U 11.3 25.0 50.0
Acrolein 25.0 U 2.54 25.0 50.0
Acrylonitrile 5.00 U 0.671 5.00 10.0
Benzene 0.500 U 0.0941 0.500 1.00
Bromobenzene 0.500 U 0.118 0.500 1.00
Bromodichloromethane 0.500 U 0.136 0.500 1.00
Bromoform 0.500 U 0.129 0.500 1.00
Bromomethane 2.00 U 0.605 2.00 5.00
n-Butylbenzene 0.500 U 0.157 0.500 1.00
sec-Butylbenzene 0.500 U 0.125 0.500 1.00
tert-Butylbenzene 0.500 U 0.127 0.500 1.00
Carbon tetrachloride 0.500 U 0.128 0.500 1.00
Chlorobenzene 0.500 U 0.116 0.500 1.00
Chlorodibromomethane 0.500 U 0.140 0.500 1.00
Chloroethane 2.00 U 0.192 2.00 5.00
Chloroform 2.00 U 0.111 2.00 5.00
Chloromethane 2.00 U 0.960 2.00 4.00
2-Chlorotoluene 0.500 U 0.106 0.500 1.00
4-Chlorotoluene 0.500 U 0.114 0.500 1.00
1,2-Dibromo-3-Chloropropane 2.00 U 0.276 2.00 5.00
1,2-Dibromoethane 0.500 U 0.126 0.500 1.00
Dibromomethane 0.500 U 0.122 0.500 1.00
1,2-Dichlorobenzene 0.500 U 0.107 0.500 1.00
1,3-Dichlorobenzene 0.500 U 0.110 0.500 1.00
1,4-Dichlorobenzene 0.500 U 0.120 0.500 1.00
Dichlorodifluoromethane 2.00 U 0.374 2.00 5.00
1,1-Dichloroethane 0.500 U 0.100 0.500 1.00
1,2-Dichloroethane 0.500 U 0.0819 0.500 1.00
1,1-Dichloroethene 0.500 U 0.188 0.500 1.00
cis-1,2-Dichloroethene 0.500 U 0.126 0.500 1.00
trans-1,2-Dichloroethene 0.500 U 0.149 0.500 1.00
1,2-Dichloropropane 0.500 U 0.149 0.500 1.00
1,1-Dichloropropene 0.500 U 0.142 0.500 1.00
1,3-Dichloropropane 0.500 U 0.110 0.500 1.00
2,2-Dichloropropane 0.500 U 0.161 0.500 1.00
Di-isopropyl ether 0.500 U 0.105 0.500 1.00
Ethylbenzene 0.500 U 0.137 0.500 1.00
Hexachloro-1,3-butadiene 0.750 U 0.337 0.750 1.50
Isopropylbenzene 0.500 U 0.105 0.500 1.00
p-Isopropyltoluene 0.500 U 0.120 0.500 1.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1900597
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1517739-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17
Method Blank (MB)
(MB) R3822215-3 07/25/22 16:23
MB Result MB Qualifier MB DL MB LOD MB LOQ
Analyte ug/l ug/l ug/l ug/l
2-Butanone (MEK)5.00 U 1.19 5.00 10.0
Methylene Chloride 2.00 U 0.430 2.00 5.00
4-Methyl-2-pentanone (MIBK)5.00 U 0.478 5.00 10.0
Methyl tert-butyl ether 0.500 U 0.101 0.500 1.00
Naphthalene 2.00 U 1.00 2.00 5.00
n-Propylbenzene 0.500 U 0.0993 0.500 1.00
Styrene 0.500 U 0.118 0.500 1.00
1,1,1,2-Tetrachloroethane 0.500 U 0.147 0.500 1.00
1,1,2,2-Tetrachloroethane 0.500 U 0.133 0.500 1.00
Tetrachloroethene 0.600 U 0.300 0.600 1.20
Toluene 0.600 U 0.278 0.600 1.20
1,2,3-Trichlorobenzene 0.500 U 0.230 0.500 1.00
1,2,4-Trichlorobenzene 1.00 U 0.481 1.00 2.00
1,1,1-Trichloroethane 0.500 U 0.149 0.500 1.00
1,1,2-Trichloroethane 0.500 U 0.158 0.500 1.00
Trichloroethene 0.500 U 0.190 0.500 1.00
Trichlorofluoromethane 2.00 U 0.160 2.00 5.00
1,2,3-Trichloropropane 1.00 U 0.237 1.00 2.50
1,2,4-Trimethylbenzene 1.00 U 0.322 1.00 2.00
1,3,5-Trimethylbenzene 0.500 U 0.104 0.500 1.00
Vinyl chloride 0.500 U 0.234 0.500 1.00
o-Xylene 0.500 U 0.174 0.500 1.00
m&p-Xylene 1.00 U 0.430 1.00 2.00
(S) Toluene-d8 96.5 89.0-112
(S) 4-Bromofluorobenzene 99.0 85.0-114
(S) 1,2-Dichloroethane-d4 100 81.0-118
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3822215-1 07/25/22 13:42 • (LCSD) R3822215-2 07/25/22 14:03
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Acetone 25.0 30.8 39.3 123 157 39.0-160 J3 24.3 20
Acrolein 25.0 17.3 17.1 69.2 68.4 39.0-155 1.16 20
Acrylonitrile 25.0 37.7 35.0 151 140 63.0-135 J4 J4 7.43 20
Benzene 5.00 5.23 5.18 105 104 79.0-120 0.961 20
Bromobenzene 5.00 5.52 5.71 110 114 80.0-120 3.38 20
Bromodichloromethane 5.00 5.56 5.13 111 103 79.0-125 8.04 20
Bromoform 5.00 5.59 5.31 112 106 66.0-130 5.14 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1900597
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1517739-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3822215-1 07/25/22 13:42 • (LCSD) R3822215-2 07/25/22 14:03
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Bromomethane 5.00 6.56 6.57 131 131 53.0-141 0.152 20
n-Butylbenzene 5.00 5.40 5.85 108 117 75.0-128 8.00 20
sec-Butylbenzene 5.00 5.05 5.67 101 113 77.0-126 11.6 20
tert-Butylbenzene 5.00 4.52 4.71 90.4 94.2 78.0-124 4.12 20
Carbon tetrachloride 5.00 5.57 5.68 111 114 72.0-136 1.96 20
Chlorobenzene 5.00 5.36 5.29 107 106 82.0-118 1.31 20
Chlorodibromomethane 5.00 5.65 5.37 113 107 74.0-126 5.08 20
Chloroethane 5.00 6.45 6.66 129 133 60.0-138 3.20 20
Chloroform 5.00 5.04 4.97 101 99.4 79.0-124 1.40 20
Chloromethane 5.00 5.62 5.64 112 113 50.0-139 0.355 20
2-Chlorotoluene 5.00 5.61 5.83 112 117 79.0-122 3.85 20
4-Chlorotoluene 5.00 5.24 5.46 105 109 78.0-122 4.11 20
1,2-Dibromo-3-Chloropropane 5.00 6.00 4.96 120 99.2 62.0-128 19.0 20
1,2-Dibromoethane 5.00 5.40 5.14 108 103 77.0-121 4.93 20
Dibromomethane 5.00 5.19 5.17 104 103 79.0-123 0.386 20
1,2-Dichlorobenzene 5.00 5.97 5.87 119 117 80.0-119 1.69 20
1,3-Dichlorobenzene 5.00 5.17 5.42 103 108 80.0-119 4.72 20
1,4-Dichlorobenzene 5.00 5.62 5.22 112 104 79.0-118 7.38 20
Dichlorodifluoromethane 5.00 5.64 6.02 113 120 32.0-152 6.52 20
1,1-Dichloroethane 5.00 5.26 5.20 105 104 77.0-125 1.15 20
1,2-Dichloroethane 5.00 6.00 6.02 120 120 73.0-128 0.333 20
1,1-Dichloroethene 5.00 5.59 5.66 112 113 71.0-131 1.24 20
cis-1,2-Dichloroethene 5.00 4.97 4.92 99.4 98.4 78.0-123 1.01 20
trans-1,2-Dichloroethene 5.00 5.12 4.97 102 99.4 75.0-124 2.97 20
1,2-Dichloropropane 5.00 5.47 5.25 109 105 78.0-122 4.10 20
1,1-Dichloropropene 5.00 5.02 4.73 100 94.6 79.0-125 5.95 20
1,3-Dichloropropane 5.00 5.50 5.27 110 105 80.0-119 4.27 20
2,2-Dichloropropane 5.00 4.97 5.10 99.4 102 60.0-139 2.58 20
Di-isopropyl ether 5.00 5.46 5.25 109 105 67.0-128 3.92 20
Ethylbenzene 5.00 5.21 5.06 104 101 79.0-121 2.92 20
Hexachloro-1,3-butadiene 5.00 4.11 5.04 82.2 101 66.0-134 J3 20.3 20
Isopropylbenzene 5.00 5.32 5.21 106 104 72.0-131 2.09 20
p-Isopropyltoluene 5.00 5.00 5.28 100 106 77.0-127 5.45 20
2-Butanone (MEK)25.0 26.8 29.2 107 117 56.0-143 8.57 20
Methylene Chloride 5.00 5.35 5.18 107 104 74.0-124 3.23 20
4-Methyl-2-pentanone (MIBK)25.0 31.4 29.9 126 120 67.0-130 4.89 20
Methyl tert-butyl ether 5.00 5.08 5.31 102 106 71.0-124 4.43 20
Naphthalene 5.00 5.49 5.55 110 111 61.0-128 1.09 20
n-Propylbenzene 5.00 5.61 5.60 112 112 76.0-126 0.178 20
Styrene 5.00 5.50 5.29 110 106 78.0-123 3.89 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1900597
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1517739-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3822215-1 07/25/22 13:42 • (LCSD) R3822215-2 07/25/22 14:03
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
1,1,1,2-Tetrachloroethane 5.00 5.19 5.13 104 103 78.0-124 1.16 20
1,1,2,2-Tetrachloroethane 5.00 5.94 5.67 119 113 71.0-121 4.65 20
Tetrachloroethene 5.00 5.73 5.73 115 115 74.0-129 0.000 20
Toluene 5.00 5.11 4.82 102 96.4 80.0-121 5.84 20
1,2,3-Trichlorobenzene 5.00 5.14 5.34 103 107 69.0-129 3.82 20
1,2,4-Trichlorobenzene 5.00 5.11 5.49 102 110 69.0-130 7.17 20
1,1,1-Trichloroethane 5.00 5.25 5.13 105 103 74.0-131 2.31 20
1,1,2-Trichloroethane 5.00 5.63 4.85 113 97.0 80.0-119 14.9 20
Trichloroethene 5.00 5.11 4.96 102 99.2 79.0-123 2.98 20
Trichlorofluoromethane 5.00 6.24 6.24 125 125 65.0-141 0.000 20
1,2,3-Trichloropropane 5.00 6.02 5.70 120 114 73.0-122 5.46 20
1,2,4-Trimethylbenzene 5.00 5.25 5.39 105 108 76.0-124 2.63 20
1,3,5-Trimethylbenzene 5.00 5.16 5.29 103 106 75.0-124 2.49 20
Vinyl chloride 5.00 6.42 6.45 128 129 58.0-137 0.466 20
o-Xylene 5.00 5.38 5.24 108 105 78.0-122 2.64 20
m&p-Xylene 10.0 10.5 10.0 105 100 80.0-121 4.88 20
(S) Toluene-d8 99.2 96.0 89.0-112
(S) 4-Bromofluorobenzene 97.6 96.8 85.0-114
(S) 1,2-Dichloroethane-d4 106 108 81.0-118
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1905109
Volatile Organic Compounds (GC/MS) by Method 6200B-2011 L1517739-01,02,09,10,11,12,13,14,15
Method Blank (MB)
(MB) R3823486-3 08/03/22 19:51
MB Result MB Qualifier MB DL MB LOD MB LOQ
Analyte ug/l ug/l ug/l ug/l
Acetone 25.0 U 11.3 25.0 50.0
Benzene 0.500 U 0.0941 0.500 1.00
Ethylbenzene 0.500 U 0.137 0.500 1.00
Naphthalene 2.00 U 1.00 2.00 5.00
n-Propylbenzene 0.500 U 0.0993 0.500 1.00
1,2,4-Trimethylbenzene 1.00 U 0.322 1.00 2.00
1,3,5-Trimethylbenzene 0.500 U 0.104 0.500 1.00
Vinyl chloride 0.500 U 0.234 0.500 1.00
o-Xylene 0.500 U 0.174 0.500 1.00
m&p-Xylene 1.00 U 0.430 1.00 2.00
(S) Toluene-d8 103 89.0-112
(S) 4-Bromofluorobenzene 102 85.0-114
(S) 1,2-Dichloroethane-d4 89.7 81.0-118
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3823486-1 08/03/22 18:05 • (LCSD) R3823486-2 08/03/22 18:26
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Acetone 25.0 21.7 21.9 86.8 87.6 39.0-160 0.917 20
Benzene 5.00 5.85 5.60 117 112 79.0-120 4.37 20
Ethylbenzene 5.00 5.81 5.27 116 105 79.0-121 9.75 20
Naphthalene 5.00 4.20 4.43 84.0 88.6 61.0-128 5.33 20
n-Propylbenzene 5.00 5.87 5.49 117 110 76.0-126 6.69 20
1,2,4-Trimethylbenzene 5.00 5.29 4.96 106 99.2 76.0-124 6.44 20
1,3,5-Trimethylbenzene 5.00 5.53 5.18 111 104 75.0-124 6.54 20
Vinyl chloride 5.00 5.27 4.62 105 92.4 58.0-137 13.1 20
o-Xylene 5.00 5.37 5.10 107 102 78.0-122 5.16 20
m&p-Xylene 10.0 11.3 10.7 113 107 80.0-121 5.45 20
(S) Toluene-d8 102 104 89.0-112
(S) 4-Bromofluorobenzene 103 106 85.0-114
(S) 1,2-Dichloroethane-d4 90.0 92.7 81.0-118
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1902750
TPH by Method MADEPE L1517739-01,02,03,04,05,06,07,08
Method Blank (MB)
(MB) R3821161-1 07/29/22 21:23
MB Result MB Qualifier MB DL MB LOD MB LOQ
Analyte ug/l ug/l ug/l ug/l
Unadjusted C9-C18 Aliphatics 67.0 U 33.3 67.0 134
Unadjusted C19-C36 Aliphatics 60.7 J 33.3 67.0 134
Unadjusted Total Petroleum
Hydrocarbons 60.7 J 33.3 67.0 134
(S) 1-Chloro-octadecane 71.1 40.0-140
Method Blank (MB)
(MB) R3821559-1 08/01/22 09:07
MB Result MB Qualifier MB DL MB LOD MB LOQ
Analyte ug/l ug/l ug/l ug/l
Unadjusted C11-C22 Aromatics 49.2 J 33.3 67.0 134
Unadjusted Total Petroleum
Hydrocarbons 49.2 J 33.3 67.0 134
(S) o-Terphenyl 77.6 40.0-140
(S) 2-Fluorobiphenyl 86.6 40.0-140
(S) 2-Bromonaphthalene 83.9 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3821161-2 07/29/22 21:46 • (LCSD) R3821161-3 07/29/22 22:08
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C9-C18 Aliphatics 600 337 336 56.2 56.0 40.0-140 0.297 25
Unadjusted C19-C36 Aliphatics 800 629 656 78.6 82.0 40.0-140 4.20 25
(S) 1-Chloro-octadecane 70.1 72.5 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3821559-2 08/01/22 09:29 • (LCSD) R3821559-3 08/01/22 09:51
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C11-C22 Aromatics 1700 1590 1650 93.5 97.1 40.0-140 3.70 25
(S) o-Terphenyl 85.4 86.3 40.0-140
(S) 2-Fluorobiphenyl 92.8 95.0 40.0-140
(S) 2-Bromonaphthalene 89.4 91.6 40.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1904482
TPH by Method MADEPE L1517739-09,10,11,12,13,14,15
Method Blank (MB)
(MB) R3822298-1 08/03/22 02:20
MB Result MB Qualifier MB DL MB LOD MB LOQ
Analyte ug/l ug/l ug/l ug/l
Unadjusted C9-C18 Aliphatics 67.0 U 33.3 67.0 134
Unadjusted C19-C36 Aliphatics 67.2 J 33.3 67.0 134
Unadjusted Total Petroleum
Hydrocarbons 67.2 J 33.3 67.0 134
(S) 1-Chloro-octadecane 82.1 40.0-140
Method Blank (MB)
(MB) R3822298-4 08/03/22 03:30
MB Result MB Qualifier MB DL MB LOD MB LOQ
Analyte ug/l ug/l ug/l ug/l
Unadjusted C11-C22 Aromatics 46.1 J 33.3 67.0 134
Unadjusted Total Petroleum
Hydrocarbons 46.1 J 33.3 67.0 134
(S) o-Terphenyl 77.0 40.0-140
(S) 2-Fluorobiphenyl 79.9 40.0-140
(S) 2-Bromonaphthalene 79.6 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3822298-2 08/03/22 02:43 • (LCSD) R3822298-3 08/03/22 03:07
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C9-C18 Aliphatics 600 351 381 58.5 63.5 40.0-140 8.20 25
Unadjusted C19-C36 Aliphatics 800 695 731 86.9 91.4 40.0-140 5.05 25
(S) 1-Chloro-octadecane 76.0 81.0 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3822298-5 08/03/22 03:53 • (LCSD) R3822298-6 08/03/22 04:16
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C11-C22 Aromatics 1700 1270 1560 74.7 91.8 40.0-140 20.5 25
(S) o-Terphenyl 75.6 90.6 40.0-140
(S) 2-Fluorobiphenyl 83.6 91.5 40.0-140
(S) 2-Bromonaphthalene 83.0 92.0 40.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1904482
TPH by Method MADEPE L1517739-09,10,11,12,13,14,15
L1517787-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1517787-05 08/03/22 15:59 • (MS) R3822298-7 08/03/22 16:22 • (MSD) R3822298-8 08/03/22 16:46
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Unadjusted C9-C18 Aliphatics 1200 134 805 762 67.1 63.5 2 40.0-140 5.49 50
Unadjusted C19-C36 Aliphatics 1600 119 1470 1460 84.4 83.8 2 40.0-140 0.683 50
(S) 1-Chloro-octadecane 68.1 67.5 40.0-140
Sample Narrative:
OS: Dilution due to sample volume.
L1517787-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1517787-05 08/04/22 07:34 • (MS) R3822298-9 08/04/22 07:57 • (MSD) R3822298-10 08/04/22 08:20
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Unadjusted C11-C22 Aromatics 3400 75.3 2750 2870 78.7 82.2 2 40.0-140 4.27 50
(S) o-Terphenyl 78.7 83.7 40.0-140
(S) 2-Fluorobiphenyl 88.7 91.9 40.0-140
(S) 2-Bromonaphthalene 88.1 91.9 40.0-140
Sample Narrative:
OS: Dilution due to sample volume.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1905723
TPH by Method MADEPE L1517739-16,17
Method Blank (MB)
(MB) R3823605-1 08/05/22 23:14
MB Result MB Qualifier MB DL MB LOD MB LOQ
Analyte ug/l ug/l ug/l ug/l
Unadjusted C9-C18 Aliphatics 67.0 U 33.3 67.0 134
Unadjusted C19-C36 Aliphatics 37.3 J 33.3 67.0 134
Unadjusted Total Petroleum
Hydrocarbons 37.3 J 33.3 67.0 134
(S) 1-Chloro-octadecane 71.0 40.0-140
Method Blank (MB)
(MB) R3823605-4 08/06/22 00:23
MB Result MB Qualifier MB DL MB LOD MB LOQ
Analyte ug/l ug/l ug/l ug/l
Unadjusted C11-C22 Aromatics 35.6 J 33.3 67.0 134
Unadjusted Total Petroleum
Hydrocarbons 35.6 J 33.3 67.0 134
(S) o-Terphenyl 85.6 40.0-140
(S) 2-Fluorobiphenyl 87.3 40.0-140
(S) 2-Bromonaphthalene 86.5 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3823605-2 08/05/22 23:37 • (LCSD) R3823605-3 08/06/22 00:00
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C9-C18 Aliphatics 600 323 321 53.8 53.5 40.0-140 0.621 25
Unadjusted C19-C36 Aliphatics 800 575 606 71.9 75.8 40.0-140 5.25 25
(S) 1-Chloro-octadecane 69.0 72.6 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3823605-5 08/06/22 00:46 • (LCSD) R3823605-6 08/06/22 01:09
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C11-C22 Aromatics 1700 1350 1340 79.4 78.8 40.0-140 0.743 25
(S) o-Terphenyl 79.5 79.0 40.0-140
(S) 2-Fluorobiphenyl 89.0 92.5 40.0-140
(S) 2-Bromonaphthalene 89.1 92.6 40.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1900474
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1517739-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15
Method Blank (MB)
(MB) R3821233-2 07/27/22 17:01
MB Result MB Qualifier MB DL MB LOD MB LOQ
Analyte ug/l ug/l ug/l ug/l
Acenaphthene 0.500 U 0.0886 0.500 1.00
Acenaphthylene 0.500 U 0.0921 0.500 1.00
Anthracene 0.500 U 0.0804 0.500 1.00
Benzidine 7.50 U 3.74 7.50 15.0
Benzo(a)anthracene 0.500 U 0.199 0.500 1.00
Benzo(b)fluoranthene 0.500 U 0.130 0.500 1.00
Benzo(k)fluoranthene 0.500 U 0.120 0.500 1.00
Benzo(g,h,i)perylene 0.500 U 0.121 0.500 1.00
Benzo(a)pyrene 0.500 U 0.0381 0.500 1.00
Bis(2-chlorethoxy)methane 5.00 U 0.116 5.00 10.0
Bis(2-chloroethyl)ether 5.00 U 0.137 5.00 10.0
2,2-Oxybis(1-Chloropropane)5.00 U 0.210 5.00 10.0
4-Bromophenyl-phenylether 5.00 U 0.0877 5.00 10.0
2-Chloronaphthalene 0.500 U 0.0648 0.500 1.00
4-Chlorophenyl-phenylether 5.00 U 0.0926 5.00 10.0
Chrysene 0.500 U 0.130 0.500 1.00
Dibenz(a,h)anthracene 0.500 U 0.0644 0.500 1.00
3,3-Dichlorobenzidine 5.00 U 0.212 5.00 10.0
2,4-Dinitrotoluene 5.00 U 0.0983 5.00 10.0
2,6-Dinitrotoluene 5.00 U 0.250 5.00 10.0
Fluoranthene 0.500 U 0.102 0.500 1.00
Fluorene 0.500 U 0.0844 0.500 1.00
Hexachlorobenzene 0.500 U 0.0755 0.500 1.00
Hexachloro-1,3-butadiene 5.00 U 0.0968 5.00 10.0
Hexachlorocyclopentadiene 5.00 U 0.0598 5.00 10.0
Hexachloroethane 5.00 U 0.127 5.00 10.0
Indeno(1,2,3-cd)pyrene 0.600 U 0.279 0.600 1.20
Isophorone 5.00 U 0.143 5.00 10.0
Naphthalene 0.500 U 0.159 0.500 1.00
Nitrobenzene 5.00 U 0.297 5.00 10.0
n-Nitrosodimethylamine 5.00 U 0.998 5.00 10.0
n-Nitrosodiphenylamine 5.00 U 2.37 5.00 10.0
n-Nitrosodi-n-propylamine 5.00 U 0.261 5.00 10.0
Phenanthrene 0.500 U 0.112 0.500 1.00
Benzylbutyl phthalate 2.00 U 0.765 2.00 4.00
Bis(2-ethylhexyl)phthalate 2.00 U 0.895 2.00 4.00
Di-n-butyl phthalate 1.50 U 0.453 1.50 3.00
Diethyl phthalate 1.50 U 0.287 1.50 3.00
Dimethyl phthalate 1.50 U 0.260 1.50 3.00
Di-n-octyl phthalate 2.00 U 0.932 2.00 4.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1900474
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1517739-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15
Method Blank (MB)
(MB) R3821233-2 07/27/22 17:01
MB Result MB Qualifier MB DL MB LOD MB LOQ
Analyte ug/l ug/l ug/l ug/l
Pyrene 0.500 U 0.107 0.500 1.00
1,2,4-Trichlorobenzene 5.00 U 0.0698 5.00 10.0
4-Chloro-3-methylphenol 5.00 U 0.131 5.00 10.0
2-Chlorophenol 5.00 U 0.133 5.00 10.0
2,4-Dichlorophenol 5.00 U 0.102 5.00 10.0
2,4-Dimethylphenol 5.00 U 0.0636 5.00 10.0
4,6-Dinitro-2-methylphenol 5.00 U 1.12 5.00 10.0
2,4-Dinitrophenol 15.0 U 5.93 15.0 30.0
2-Nitrophenol 5.00 U 0.117 5.00 10.0
4-Nitrophenol 5.00 U 0.143 5.00 10.0
Pentachlorophenol 5.00 U 0.313 5.00 10.0
Phenol 10.0 U 4.33 10.0 20.0
2,4,6-Trichlorophenol 5.00 U 0.100 5.00 10.0
1-Methylnaphthalene 0.500 U 0.0790 0.500 1.00
2-Methylnaphthalene 0.500 U 0.117 0.500 1.00
(S) Nitrobenzene-d5 23.4 J2 44.0-120
(S) 2-Fluorobiphenyl 26.2 J2 44.0-119
(S) p-Terphenyl-d14 45.6 J2 50.0-134
(S) Phenol-d5 9.45 J2 10.0-67.0
(S) 2-Fluorophenol 13.6 J2 19.0-119
(S) 2,4,6-Tribromophenol 44.1 43.0-140
Laboratory Control Sample (LCS)
(LCS) R3821233-1 07/27/22 16:39
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Acenaphthene 50.0 24.4 48.8 47.0-122
Acenaphthylene 50.0 24.7 49.4 41.0-130
Anthracene 50.0 26.6 53.2 57.0-123 J4
Benzidine 100 0.634 0.634 10.0-165 J4
Benzo(a)anthracene 50.0 30.9 61.8 58.0-125
Benzo(b)fluoranthene 50.0 30.3 60.6 53.0-131
Benzo(k)fluoranthene 50.0 29.9 59.8 57.0-129
Benzo(g,h,i)perylene 50.0 30.4 60.8 50.0-134
Benzo(a)pyrene 50.0 32.1 64.2 54.0-128
Bis(2-chlorethoxy)methane 50.0 21.2 42.4 48.0-120 J4
Bis(2-chloroethyl)ether 50.0 15.4 30.8 43.0-118 J4
2,2-Oxybis(1-Chloropropane)50.0 15.2 30.4 37.0-130 J4
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1900474
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1517739-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15
Laboratory Control Sample (LCS)
(LCS) R3821233-1 07/27/22 16:39
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
4-Bromophenyl-phenylether 50.0 34.2 68.4 55.0-124
2-Chloronaphthalene 50.0 23.5 47.0 40.0-116
4-Chlorophenyl-phenylether 50.0 31.2 62.4 53.0-121
Chrysene 50.0 31.4 62.8 59.0-123
Dibenz(a,h)anthracene 50.0 30.3 60.6 51.0-134
3,3-Dichlorobenzidine 100 60.8 60.8 27.0-129
2,4-Dinitrotoluene 50.0 28.8 57.6 57.0-128
2,6-Dinitrotoluene 50.0 28.0 56.0 57.0-124 J4
Fluoranthene 50.0 27.9 55.8 57.0-128 J4
Fluorene 50.0 27.1 54.2 52.0-124
Hexachlorobenzene 50.0 33.7 67.4 53.0-125
Hexachloro-1,3-butadiene 50.0 22.7 45.4 22.0-124
Hexachlorocyclopentadiene 50.0 10.2 20.4 10.0-121
Hexachloroethane 50.0 13.4 26.8 21.0-115
Indeno(1,2,3-cd)pyrene 50.0 30.9 61.8 52.0-134
Isophorone 50.0 22.4 44.8 42.0-124
Naphthalene 50.0 16.7 33.4 40.0-121 J4
Nitrobenzene 50.0 19.9 39.8 45.0-121 J4
n-Nitrosodimethylamine 50.0 15.8 31.6 10.0-121
n-Nitrosodiphenylamine 50.0 25.8 51.6 51.0-123
n-Nitrosodi-n-propylamine 50.0 21.2 42.4 49.0-119 J4
Phenanthrene 50.0 26.3 52.6 59.0-120 J4
Benzylbutyl phthalate 50.0 27.7 55.4 53.0-134
Bis(2-ethylhexyl)phthalate 50.0 25.8 51.6 55.0-135 J4
Di-n-butyl phthalate 50.0 26.0 52.0 59.0-127 J4
Diethyl phthalate 50.0 27.5 55.0 56.0-125 J4
Dimethyl phthalate 50.0 28.4 56.8 45.0-127
Di-n-octyl phthalate 50.0 27.0 54.0 51.0-140
Pyrene 50.0 29.8 59.6 65.0-129 J4
1,2,4-Trichlorobenzene 50.0 19.3 38.6 29.0-116
4-Chloro-3-methylphenol 50.0 24.8 49.6 52.0-119 J4
2-Chlorophenol 50.0 15.4 30.8 38.0-117 J4
2,4-Dichlorophenol 50.0 22.7 45.4 47.0-121 J4
2,4-Dimethylphenol 50.0 24.7 49.4 31.0-124
4,6-Dinitro-2-methylphenol 50.0 32.8 65.6 44.0-137
2,4-Dinitrophenol 50.0 24.4 48.8 23.0-143
2-Nitrophenol 50.0 22.3 44.6 47.0-123 J4
4-Nitrophenol 50.0 9.97 19.9 10.0-120
Pentachlorophenol 50.0 28.9 57.8 35.0-138
Phenol 50.0 7.69 15.4 10.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1900474
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1517739-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15
Laboratory Control Sample (LCS)
(LCS) R3821233-1 07/27/22 16:39
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
2,4,6-Trichlorophenol 50.0 33.6 67.2 53.0-123
1-Methylnaphthalene 50.0 21.3 42.6 41.0-119
2-Methylnaphthalene 50.0 20.4 40.8 40.0-121
(S) Nitrobenzene-d5 39.2 44.0-120 J2
(S) 2-Fluorobiphenyl 52.7 44.0-119
(S) p-Terphenyl-d14 57.4 50.0-134
(S) Phenol-d5 15.2 10.0-67.0
(S) 2-Fluorophenol 20.2 19.0-119
(S) 2,4,6-Tribromophenol 73.0 43.0-140
L1517659-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1517659-01 08/03/22 20:23 • (MS) R3822444-1 08/03/22 20:45 • (MSD) R3822444-2 08/03/22 21:06
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Acenaphthene 50.0 0.500 21.0 21.7 42.0 43.4 1 47.0-122 J6 J6 3.28 20
Acenaphthylene 50.0 0.500 21.2 22.1 42.4 44.2 1 41.0-130 4.16 20
Anthracene 50.0 0.500 26.2 25.7 52.4 51.4 1 57.0-123 J6 J6 1.93 20
Benzidine 100 7.50 15.8 22.4 15.8 22.4 1 10.0-165 J3 34.6 20
Benzo(a)anthracene 50.0 0.500 29.8 28.2 59.6 56.4 1 58.0-125 J6 5.52 20
Benzo(b)fluoranthene 50.0 0.500 30.8 28.5 61.6 57.0 1 53.0-131 7.76 20
Benzo(k)fluoranthene 50.0 0.500 29.8 28.6 59.6 57.2 1 57.0-129 4.11 20
Benzo(g,h,i)perylene 50.0 0.500 23.9 21.9 47.8 43.8 1 50.0-134 J6 J6 8.73 20
Benzo(a)pyrene 50.0 0.500 32.0 31.6 64.0 63.2 1 54.0-128 1.26 20
Bis(2-chlorethoxy)methane 50.0 5.00 19.1 21.1 38.2 42.2 1 48.0-120 J6 J6 9.95 20
Bis(2-chloroethyl)ether 50.0 5.00 17.8 18.5 35.6 37.0 1 43.0-118 J6 J6 3.86 20
2,2-Oxybis(1-Chloropropane)50.0 5.00 15.3 16.3 30.6 32.6 1 37.0-130 J6 J6 6.33 20
4-Bromophenyl-phenylether 50.0 5.00 23.0 23.3 46.0 46.6 1 55.0-124 J6 J6 1.30 20
2-Chloronaphthalene 50.0 0.500 17.8 19.3 35.6 38.6 1 40.0-116 J6 J6 8.09 20
4-Chlorophenyl-phenylether 50.0 5.00 22.0 22.8 44.0 45.6 1 53.0-121 J6 J6 3.57 20
Chrysene 50.0 0.500 27.8 26.6 55.6 53.2 1 59.0-123 J6 J6 4.41 20
Dibenz(a,h)anthracene 50.0 0.500 23.3 22.1 46.6 44.2 1 51.0-134 J6 J6 5.29 20
3,3-Dichlorobenzidine 100 5.00 44.1 42.6 44.1 42.6 1 27.0-129 3.46 20
2,4-Dinitrotoluene 50.0 5.00 31.4 30.7 62.8 61.4 1 57.0-128 2.25 20
2,6-Dinitrotoluene 50.0 5.00 26.2 26.9 52.4 53.8 1 57.0-124 J6 J6 2.64 20
Fluoranthene 50.0 0.500 27.0 25.7 54.0 51.4 1 57.0-128 J6 J6 4.93 20
Fluorene 50.0 0.500 23.7 24.3 47.4 48.6 1 52.0-124 J6 J6 2.50 20
Hexachlorobenzene 50.0 0.500 21.2 22.0 42.4 44.0 1 53.0-125 J6 J6 3.70 20
Hexachloro-1,3-butadiene 50.0 5.00 11.8 12.1 23.6 24.2 1 22.0-124 2.51 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1900474
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1517739-01,02,03,04,05,06,07,08,09,10,11,12,13,14,15
L1517659-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1517659-01 08/03/22 20:23 • (MS) R3822444-1 08/03/22 20:45 • (MSD) R3822444-2 08/03/22 21:06
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Hexachlorocyclopentadiene 50.0 5.00 3.41 3.30 6.82 6.60 1 10.0-121 J6 J6 3.28 20
Hexachloroethane 50.0 5.00 13.3 12.8 26.6 25.6 1 21.0-115 3.83 20
Indeno(1,2,3-cd)pyrene 50.0 0.600 23.5 22.5 47.0 45.0 1 52.0-134 J6 J6 4.35 20
Isophorone 50.0 5.00 18.6 20.0 37.2 40.0 1 42.0-124 J6 J6 7.25 20
Naphthalene 50.0 0.500 15.9 16.4 31.8 32.8 1 40.0-121 J6 J6 3.10 20
Nitrobenzene 50.0 5.00 16.2 16.8 32.4 33.6 1 45.0-121 J6 J6 3.64 20
n-Nitrosodimethylamine 50.0 5.00 14.0 16.3 28.0 32.6 1 10.0-121 15.2 20
n-Nitrosodiphenylamine 50.0 5.00 26.8 26.1 53.6 52.2 1 51.0-123 2.65 20
n-Nitrosodi-n-propylamine 50.0 5.00 21.4 23.6 42.8 47.2 1 49.0-119 J6 J6 9.78 20
Phenanthrene 50.0 0.500 25.4 25.4 50.8 50.8 1 59.0-120 J6 J6 0.000 20
Benzylbutyl phthalate 50.0 2.00 36.0 34.4 72.0 68.8 1 53.0-134 4.55 20
Bis(2-ethylhexyl)phthalate 50.0 2.00 28.9 28.0 57.8 56.0 1 55.0-135 3.16 20
Di-n-butyl phthalate 50.0 1.50 30.3 28.5 60.6 57.0 1 59.0-127 J6 6.12 20
Diethyl phthalate 50.0 1.50 25.9 26.5 51.8 53.0 1 56.0-125 J6 J6 2.29 20
Dimethyl phthalate 50.0 1.50 24.6 25.3 49.2 50.6 1 45.0-127 2.81 20
Di-n-octyl phthalate 50.0 2.00 27.4 28.1 54.8 56.2 1 51.0-140 2.52 20
Pyrene 50.0 0.500 33.6 31.8 67.2 63.6 1 65.0-129 J6 5.50 20
1,2,4-Trichlorobenzene 50.0 5.00 13.2 13.5 26.4 27.0 1 29.0-116 J6 J6 2.25 20
4-Chloro-3-methylphenol 50.0 5.00 23.9 23.1 47.8 46.2 1 52.0-119 J6 J6 3.40 20
2-Chlorophenol 50.0 5.00 12.6 12.1 25.2 24.2 1 38.0-117 J6 J6 4.05 20
2,4-Dichlorophenol 50.0 5.00 16.8 16.0 33.6 32.0 1 47.0-121 J6 J6 4.88 20
2,4-Dimethylphenol 50.0 5.00 17.6 20.0 35.2 40.0 1 31.0-124 12.8 20
4,6-Dinitro-2-methylphenol 50.0 5.00 33.4 28.9 66.8 57.8 1 44.0-137 14.4 20
2,4-Dinitrophenol 50.0 15.0 33.4 25.5 66.8 51.0 1 23.0-143 J3 26.8 20
2-Nitrophenol 50.0 5.00 16.2 15.8 32.4 31.6 1 47.0-123 J6 J6 2.50 20
4-Nitrophenol 50.0 5.00 6.84 3.85 13.7 7.70 1 10.0-120 J3 J6 55.9 20
Pentachlorophenol 50.0 5.00 22.7 18.3 45.4 36.6 1 35.0-138 J3 21.5 20
Phenol 50.0 10.0 7.05 7.22 14.1 14.4 1 10.0-120 2.38 20
2,4,6-Trichlorophenol 50.0 5.00 20.0 17.7 40.0 35.4 1 53.0-123 J6 J6 12.2 20
1-Methylnaphthalene 50.0 18.6 19.4 37.2 38.8 1 41.0-119 J6 J6 4.21 20
2-Methylnaphthalene 50.0 0.500 17.2 18.1 34.4 36.2 1 40.0-121 J6 J6 5.10 20
(S) Nitrobenzene-d5 30.0 32.8 44.0-120 J2 J2
(S) 2-Fluorobiphenyl 33.5 38.4 44.0-119 J2 J2
(S) p-Terphenyl-d14 50.5 54.2 50.0-134
(S) Phenol-d5 12.3 14.3 10.0-67.0
(S) 2-Fluorophenol 14.1 14.8 19.0-119 J2 J2
(S) 2,4,6-Tribromophenol 35.6 34.3 43.0-140 J2 J2
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1901647
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1517739-16,17
Method Blank (MB)
(MB) R3822146-2 08/01/22 12:51
MB Result MB Qualifier MB DL MB LOD MB LOQ
Analyte ug/l ug/l ug/l ug/l
Acenaphthene 0.500 U 0.0886 0.500 1.00
Acenaphthylene 0.500 U 0.0921 0.500 1.00
Anthracene 0.500 U 0.0804 0.500 1.00
Benzidine 7.50 U 3.74 7.50 15.0
Benzo(a)anthracene 0.500 U 0.199 0.500 1.00
Benzo(b)fluoranthene 0.500 U 0.130 0.500 1.00
Benzo(k)fluoranthene 0.500 U 0.120 0.500 1.00
Benzo(g,h,i)perylene 0.500 U 0.121 0.500 1.00
Benzo(a)pyrene 0.500 U 0.0381 0.500 1.00
Bis(2-chlorethoxy)methane 5.00 U 0.116 5.00 10.0
Bis(2-chloroethyl)ether 5.00 U 0.137 5.00 10.0
2,2-Oxybis(1-Chloropropane)5.00 U 0.210 5.00 10.0
4-Bromophenyl-phenylether 5.00 U 0.0877 5.00 10.0
2-Chloronaphthalene 0.500 U 0.0648 0.500 1.00
4-Chlorophenyl-phenylether 5.00 U 0.0926 5.00 10.0
Chrysene 0.500 U 0.130 0.500 1.00
Dibenz(a,h)anthracene 0.500 U 0.0644 0.500 1.00
3,3-Dichlorobenzidine 5.00 U 0.212 5.00 10.0
2,4-Dinitrotoluene 5.00 U 0.0983 5.00 10.0
2,6-Dinitrotoluene 5.00 U 0.250 5.00 10.0
Fluoranthene 0.500 U 0.102 0.500 1.00
Fluorene 0.500 U 0.0844 0.500 1.00
Hexachlorobenzene 0.500 U 0.0755 0.500 1.00
Hexachloro-1,3-butadiene 5.00 U 0.0968 5.00 10.0
Hexachlorocyclopentadiene 5.00 U 0.0598 5.00 10.0
Hexachloroethane 5.00 U 0.127 5.00 10.0
Indeno(1,2,3-cd)pyrene 0.600 U 0.279 0.600 1.20
Isophorone 5.00 U 0.143 5.00 10.0
Naphthalene 0.500 U 0.159 0.500 1.00
Nitrobenzene 5.00 U 0.297 5.00 10.0
n-Nitrosodimethylamine 5.00 U 0.998 5.00 10.0
n-Nitrosodiphenylamine 5.00 U 2.37 5.00 10.0
n-Nitrosodi-n-propylamine 5.00 U 0.261 5.00 10.0
Phenanthrene 0.500 U 0.112 0.500 1.00
Benzylbutyl phthalate 2.00 U 0.765 2.00 4.00
Bis(2-ethylhexyl)phthalate 2.00 U 0.895 2.00 4.00
Di-n-butyl phthalate 1.50 U 0.453 1.50 3.00
Diethyl phthalate 1.50 U 0.287 1.50 3.00
Dimethyl phthalate 1.50 U 0.260 1.50 3.00
Di-n-octyl phthalate 2.00 U 0.932 2.00 4.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1901647
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1517739-16,17
Method Blank (MB)
(MB) R3822146-2 08/01/22 12:51
MB Result MB Qualifier MB DL MB LOD MB LOQ
Analyte ug/l ug/l ug/l ug/l
Pyrene 0.500 U 0.107 0.500 1.00
1,2,4-Trichlorobenzene 5.00 U 0.0698 5.00 10.0
4-Chloro-3-methylphenol 5.00 U 0.131 5.00 10.0
2-Chlorophenol 5.00 U 0.133 5.00 10.0
2,4-Dichlorophenol 5.00 U 0.102 5.00 10.0
2,4-Dimethylphenol 5.00 U 0.0636 5.00 10.0
4,6-Dinitro-2-methylphenol 5.00 U 1.12 5.00 10.0
2,4-Dinitrophenol 15.0 U 5.93 15.0 30.0
2-Nitrophenol 5.00 U 0.117 5.00 10.0
4-Nitrophenol 5.00 U 0.143 5.00 10.0
Pentachlorophenol 5.00 U 0.313 5.00 10.0
Phenol 10.0 U 4.33 10.0 20.0
2,4,6-Trichlorophenol 5.00 U 0.100 5.00 10.0
1-Methylnaphthalene 0.500 U 0.0790 0.500 1.00
2-Methylnaphthalene 0.500 U 0.117 0.500 1.00
(S) Nitrobenzene-d5 63.1 44.0-120
(S) 2-Fluorobiphenyl 58.9 44.0-119
(S) p-Terphenyl-d14 65.6 50.0-134
(S) Phenol-d5 30.8 10.0-67.0
(S) 2-Fluorophenol 34.6 19.0-119
(S) 2,4,6-Tribromophenol 80.5 43.0-140
Laboratory Control Sample (LCS)
(LCS) R3822146-1 08/01/22 12:29
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Acenaphthene 50.0 32.8 65.6 47.0-122
Acenaphthylene 50.0 33.9 67.8 41.0-130
Anthracene 50.0 34.8 69.6 57.0-123
Benzidine 100 18.6 18.6 10.0-165
Benzo(a)anthracene 50.0 38.2 76.4 58.0-125
Benzo(b)fluoranthene 50.0 36.0 72.0 53.0-131
Benzo(k)fluoranthene 50.0 34.5 69.0 57.0-129
Benzo(g,h,i)perylene 50.0 34.4 68.8 50.0-134
Benzo(a)pyrene 50.0 37.3 74.6 54.0-128
Bis(2-chlorethoxy)methane 50.0 35.2 70.4 48.0-120
Bis(2-chloroethyl)ether 50.0 30.6 61.2 43.0-118
2,2-Oxybis(1-Chloropropane)50.0 29.0 58.0 37.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1901647
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1517739-16,17
Laboratory Control Sample (LCS)
(LCS) R3822146-1 08/01/22 12:29
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
4-Bromophenyl-phenylether 50.0 38.5 77.0 55.0-124
2-Chloronaphthalene 50.0 32.2 64.4 40.0-116
4-Chlorophenyl-phenylether 50.0 39.3 78.6 53.0-121
Chrysene 50.0 35.8 71.6 59.0-123
Dibenz(a,h)anthracene 50.0 34.6 69.2 51.0-134
3,3-Dichlorobenzidine 100 75.2 75.2 27.0-129
2,4-Dinitrotoluene 50.0 44.5 89.0 57.0-128
2,6-Dinitrotoluene 50.0 40.6 81.2 57.0-124
Fluoranthene 50.0 39.2 78.4 57.0-128
Fluorene 50.0 34.9 69.8 52.0-124
Hexachlorobenzene 50.0 38.5 77.0 53.0-125
Hexachloro-1,3-butadiene 50.0 38.8 77.6 22.0-124
Hexachlorocyclopentadiene 50.0 9.32 18.6 10.0-121
Hexachloroethane 50.0 30.3 60.6 21.0-115
Indeno(1,2,3-cd)pyrene 50.0 34.9 69.8 52.0-134
Isophorone 50.0 36.3 72.6 42.0-124
Naphthalene 50.0 31.8 63.6 40.0-121
Nitrobenzene 50.0 35.4 70.8 45.0-121
n-Nitrosodimethylamine 50.0 26.5 53.0 10.0-121
n-Nitrosodiphenylamine 50.0 33.6 67.2 51.0-123
n-Nitrosodi-n-propylamine 50.0 39.7 79.4 49.0-119
Phenanthrene 50.0 34.0 68.0 59.0-120
Benzylbutyl phthalate 50.0 36.8 73.6 53.0-134
Bis(2-ethylhexyl)phthalate 50.0 35.3 70.6 55.0-135
Di-n-butyl phthalate 50.0 39.1 78.2 59.0-127
Diethyl phthalate 50.0 41.7 83.4 56.0-125
Dimethyl phthalate 50.0 39.2 78.4 45.0-127
Di-n-octyl phthalate 50.0 35.6 71.2 51.0-140
Pyrene 50.0 35.1 70.2 65.0-129
1,2,4-Trichlorobenzene 50.0 33.4 66.8 29.0-116
4-Chloro-3-methylphenol 50.0 39.9 79.8 52.0-119
2-Chlorophenol 50.0 26.7 53.4 38.0-117
2,4-Dichlorophenol 50.0 35.7 71.4 47.0-121
2,4-Dimethylphenol 50.0 32.1 64.2 31.0-124
4,6-Dinitro-2-methylphenol 50.0 50.4 101 44.0-137
2,4-Dinitrophenol 50.0 54.3 109 23.0-143
2-Nitrophenol 50.0 36.5 73.0 47.0-123
4-Nitrophenol 50.0 17.0 34.0 10.0-120
Pentachlorophenol 50.0 43.9 87.8 35.0-138
Phenol 50.0 15.6 31.2 10.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1901647
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1517739-16,17
Laboratory Control Sample (LCS)
(LCS) R3822146-1 08/01/22 12:29
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
2,4,6-Trichlorophenol 50.0 38.6 77.2 53.0-123
1-Methylnaphthalene 50.0 36.2 72.4 41.0-119
2-Methylnaphthalene 50.0 34.4 68.8 40.0-121
(S) Nitrobenzene-d5 69.4 44.0-120
(S) 2-Fluorobiphenyl 66.8 44.0-119
(S) p-Terphenyl-d14 67.9 50.0-134
(S) Phenol-d5 27.7 10.0-67.0
(S) 2-Fluorophenol 37.0 19.0-119
(S) 2,4,6-Tribromophenol 90.5 43.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
DL Detection Limit.
LOD Limit of Detection.
LOQ Limit of Quantitation.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
B The same analyte is found in the associated blank.
C4 The reported concentration is an estimate. The continuing calibration standard associated with this data responded low.
Data is likely to show a low bias concerning the result.
C6 The initial calibration verification standard (SSCV) associated with this data responded low.
J The identification of the analyte is acceptable; the reported value is an estimate.
J1 Surrogate recovery limits have been exceeded; values are outside upper control limits.
J2 Surrogate recovery limits have been exceeded; values are outside lower control limits.
J3 The associated batch QC was outside the established quality control range for precision.
J4 The associated batch QC was outside the established quality control range for accuracy.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low.
Q Sample was prepared and/or analyzed past holding time as defined in the method. Concentrations should be considered minimum values.
U Below Detectable Limits: Indicates that the analyte was not detected.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Company Name/Addre,.. 81 ',ng Information· a ·-L..t. rnnt:ainpr / o... p--•rup Chain of Custody P•ge_of_
Cherokee Nation 3S Christi Mahagan Pres .,l
10838 E. Marshall St. Chk ~ ff'!E~ .. v,,~. 10838 E. Marshall St. Suite 240
Suite 240 Tulsa, OK 74116
Tulsa. OK 74116
Report to: Email To: [e-mail] MT JULIET, TN
Kevin DeFosset 120(.S lebari.<ln Ad Mount M itt. T"' J7U2
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10838 E. Marshall St. Chk ~ r?!!£~.G~IEHCE 10838 E. Marshall St. Suite 240
Suite 240 Tulsa, OK 74116
Tulsa. OK 74116
Report to: Ema,I To: kevin.defosset~cherokee-federal.com MT JULIET, TN
Kevin Defosset 1206SL•banon,-_d M< 1t>u1 .. 1,1Nl7122
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SS · Soil AIR -Air F · Filter pH ___ Temp ___ COC Sea! Present/Intact: _·t N
GW • Groundwater B · Bioassay COC S1g0 Pd/Aecurate: -,=~ WW • Wastewater Flow Other Bettles arrive intac•: ------Correct bottles used,
OW • Drinking Water Samples returned v,a: ufficiec.t v?lurne sent, -_N
OT-Other UPS FedEx Courier Tracking# If APPl1cab!e j ~ VOA Zero Headspace:
Rel~~~(/2/ /
Date: Time: Received by· (Signature) Trip Blank Received: Yes I No Preservat ~ C rrect Checked:
'r1 lzl I ?P'l2 HCL/ MeoH RA Screen <C.5 mR/hr: J-N
TBR
Rel~d by : (SiRn-tre) Date Time Received by: {Signature) Temp: ·c Bottles Received If preservation required by Login: Date/Time
Relinquished by : {Signature) Date. Time: ~b by: {Signature) Oat Time: Hold: I Condition:
L -, 9 Z'Z. ~Z. ,tl) NCF / f!J
I
2022 Annual Monitoring Report – TC-341
MCAS New River, NC

APPENDIX D

Contaminants of Concern vs. Time Charts
(.'\ (HEROKEENATION™ ~ 3 S-Support, Service & Solutions
* Charts have been modified to show recent, relevant data.
50
100
150
200
250
300
350
400
450
Contaminant Concentrationug/LSample Date
USTG480-MW02
Benzene
1-
Methylnaphthalene
2-
Methylnaphthalene
Naphthalene
(SVOC)
0
50
100
150
200
250
Contaminant Concentrationug/LSample Date
USTG480-MW06
Benzene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene (SVOC)
0
100
200
300
400
500
600
700
Contaminant Concentrationug/LSample Date
IR35-MW67AR
Benzene
1-
Methylnaphthalene
2-
Methylnaphthalene
Naphthalene
(SVOC)
* Charts have been modified to show recent, relevant data.
0
50
100
150
200
250
Contaminant Concentrationug/LSample Date
USTG480-MW11
Benzene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene (SVOC)
0
20
40
60
80
100
120
140
160
180
Contaminant Concentrationug/LSample Date
USTG480-MW13
Benzene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene (SVOC)
0
50
100
150
200
250
300
Contaminant Concentrationug/LSample Date
USTG480-MW23
Benzene
1-
Methylnaphthalene
2-
Methylnaphthalene
Naphthalene
(SVOC)
-
* Charts have been modified to show recent, relevant data.
0
0.5
1
1.5
2
2.5
3
3.5
4
4.5
Contaminant Concentrationug/LSample Date
USTG480-MW25
Benzene
0
200
400
600
800
1000
1200
1400
1600
1800
Contaminant Concentrationug/LSample Date
USTG480-MW26
Benzene
1-
Methylnaphthalene
2-
Methylnaphthalene
Naphthalene
(SVOC)
0
50
100150
200
250
300350
400
450500
Contaminant Concentrationug/LSample Date
USTG480-MW27
1-
Methylnaphthalene
2-
Methylnaphthalene
Naphthalene (SVOC)
* Charts have been modified to show recent, relevant data.
0
100
200
300
400
500
600
Contaminant Concentrationug/LSample Date
USTG480-MW29
Benzene
1-
Methylnaphthalene
2-
Methylnaphthalene
Naphthalene (SVOC)
0
50
100
150
200
250
7/25/2013 7/13/2016 7/17/2019 7/26/2021Contaminant Concentrationug/LSample Date
USTG480-MW30
Benzene
0
50
100
150
200
Contaminant Concentrationug/LSample Date
USTTC341-MW14
Benzene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene (SVOC)
-...,._
* Charts have been modified to show recent, relevant data.
0.0
50.0
100.0
150.0200.0250.0
300.0
350.0
400.0
450.0
500.0
Contaminant Concentrationug/LSample Date
USTTC341-MW18
Benzene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene (SVOC)
2022 Annual Monitoring Report – TC-341
MCAS New River, NC

APPENDIX E

Mann-Kendall Trend Analysis
(.'\ (HEROKEENATION™ ~ 3 S-Support, Service & Solutions
Mann-Kendall Concentration Trend Analysis for Benzene
2022 Annual Monitoring Report
TC-341 Site
Sampling Event IR35-MW67AR
USTG480-
MW01
USTG480-
MW02
USTG480-
MW04R
USTG480-
MW09R
USTG480-
MW10
USTG480-
MW17
USTG480-
MW27
1 162 0.84 170 29 0.78 34 28 15
2 149 18 180 35 1.84 82 26 5.9
3 163 11 200 26 0.065 54.2 31 3
4 154 0.0595 257 19.8 1.1 61.9 10.8 1.5
5 202 4.6 144 28.4 0.219 55.2 11.1 6.9
6 81.1 0.23 146 40.2 68.1 3 3.5
7 203 0.18 154 30.2 39.8 4.74 0.86
8 0.04705 167 0.753 2.03
9 185 0.04705 1.05
10 169 0.372
11
12
13
14
15
Coefficient of Variation 0.26 1.53 0.19 0.22 0.89 0.29 0.96 1.1
Mann-Kendall Statistic (S) 5 -16 -1 3 -2 1 -28 -29
Confidence Factor 71.9% 96.9% 50.0% 61.4% 59.2% 50.0% 99.9%99.5%
Concentration Trend No Trend Decreasing Stable No Trend Stable No Trend Decreasing Decreasing
Sampling Event USTG480-
MW29
USTG480-
MW30
USTG480-
MW31
USTTC341-
MW14/R
USTTC341-
MW18
USTG480-
MW25*
1 190 120 170 24 29.2 2.2
2 300 8.6 220 20.1 2.1 3
3 300 6.5 240 8.6 17.5 4
4 213 3.55 197 6.7 2.15 2.61
5 6.8 197 196 17.7 9.22 2.9
6 112 0.065 167 3.33 19.7 3.4
7 153 1.1 109 5.87 3
8 245 0.53 180 8.07 2.52
9 192 0.349 0.167
10 540 2 1.1
11
12
13
14
15
Coefficient of Variation 0.63 2.01 0.21 0.65 0.81 0.45
Mann-Kendall Statistic (S) 4 -23 -12 -16 1 -14
Confidence Factor 60.3% 97.7% 91.1% 96.9% 50.0% 87.3%
Concentration Trend No Trend Decreasing
Probably
Decreasing Decreasing No Trend Stable
NOTES:
Non-detect results are represented by half the detection limit, or 0.5 ug/L if detection limit was not available.
Analytical results are presented in chronological order from oldest to most recent.
Analytical results are from 2013 to present.
* Intermediate depth well
Benzene Concentration (ug/L)
Benzene Concentration (ug/L)
Page 1 of 1
Mann-Kendall Concentration Trend Analysis for Naphthalene
2022 Annual Monitoring Report
TC-341 Site
Sampling Event IR35-MW67AR
USTG480-
MW01
USTG480-
MW02
USTG480-
MW04R
USTG480-
MW09R
USTG480-
MW10
USTG480-
MW11
USTG480-
MW17
1 397 38 200 190 5.5 88 130 57
2 460 120 320 87 13.2 160 57 89
3 369 19 560 9.89 10.5 126 10.6 17
4 361 0.625 124 60.4 43.9 407 228 17.1
5 265 60.7 296 63.4 3.59 285 184 35.8
6 291 7.5 183 77.4 237 88.3 2.5
7 174 5.5 314 86.1 68.8 77.4 0.0795
8 0.196 228 80.9 0.414
9 208 32.1 0.262
10 113
11
12
13
14
15
Coefficient of Variation 0.29 1.32 0.51 0.66 1.07 0.62 0.71 1.27
Mann-Kendall Statistic (S) -17 -16 -13 -1 0 1 -8 -24
Confidence Factor 99.5% 96.9% 85.4% 50.0% 40.8% 50.0% 76.2%99.4%
Concentration Trend Decreasing Decreasing Stable Stable No Trend No Trend Stable Decreasing
Sampling Event USTG480-
MW27
USTG480-
MW29
USTG480-
MW31
USTTC341-
MW14/R
USTTC341-
MW18
1 180 400 180 730 397
2 210 430 430 88 90.3
3 390 420 70 163 37.7
4 150 117 88.6 106 4.17
5 284 0.61 158 172 4.26
6 238 249 199 22.9 0.0795
7 187 239 291 53.1
8 131 177 223 26.3
9 95.5 184
10 4.77 185
11
12
13
14
15
Coefficient of Variation 0.56 0.58 0.56 1.37 1.74
Mann-Kendall Statistic (S) -23 -15 8 -14 -13
Confidence Factor 97.7% 89.2% 80.1% 94.6% 99.2%
Concentration Trend Decreasing Stable No Trend
Probably
Decreasing Decreasing
NOTES:
Non-detect results are represented by half the detection limit, or 0.5 ug/L if detection limit was not available.
Analytical results are presented in chronological order from oldest to most recent.
Analytical results are from 2013 to present.
* Intermediate depth well
Naphthalene Concentration (ug/L)
Naphthalene Concentration (ug/L)
Page 1 of 1