WA-1195_13993_CA_LAB_20201021_W OTHERS

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Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Report of Analysis
DEQ DWM
217 West Jones St.
Raleigh,NC 27603
Attention:Jared Edwards
Project Name:95818 Bay
Project Number:95818
Lot Number:VJ01071
Date Completed:10/20/2020
10/21/2020 9:31 AM
Approved and released by:
Project Manager II:Nisreen Saikaly
Page 1 of 60
PACE ANALYTICAL SERVICES,LLC
SC DHEC No:32010001 NELAC No:E87653 NC DENR No:329 NC Field Parameters No:5639
Pace Analytical Services,LLC (formerly Shealy Environmetal Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax [phone] www.pacelabs.com
Case Narrative
DEQ DWM
Lot Number:VJ01071
This Report of Analysis contains the analytical result(s)for the sample(s)listed on the Sample Summary
following this Case Narrative.The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt,sample analysis,and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI)standards,the Pace Analytical Services,LLC ("Pace")
Laboratory Quality Manual,standard operating procedures (SOPs),and Pace policies.Any exceptions to
the TNI standards,the Laboratory Quality Manual,SOPs or policies are qualified on the results page or
discussed below.
Where applicable,all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
SVOC
The following sample was diluted due to the nature of the sample matrix:VJ01071-001.The LOQ has
been elevated to reflect the dilution.
VOC
Internal standard response for the following samples exceeded the lower control limit:VJ01071-001,
VJ01071-002.Surrogate recovery was also outside control limits.The samples were re-analyzed with
concurring results for internal and surrogate recoveries.As such,the sample results may be biased high.
The original set of data has been reported
VPH
Surrogate recovery for the following samples was outside control limits:VJ01071-001,VJ01071-002.
Evidence of matrix interference is present;therefore,re-extraction and/or re-analysis was not performed.
Page 2 of 60
PACE ANALYTICAL SERVICES, LLC
Sample Summary
DEQ DWM
Lot Number: VJ01071

Sample Number Sample ID Matrix Date Sampled Date Received
001 09/29/2020 170095818 BAY #144 Solid 10/01/2020
002 09/29/2020 1840610 NC 343 SOUTH Solid 10/01/2020
003 09/30/2020 133013993 MW-1 Aqueous 10/01/2020
(3 samples)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 3 of 60
PACE ANALYTICAL SERVICES, LLC
Detection Summary
DEQ DWM
Lot Number: VJ01071

Sample Sample ID Matrix Parameter Method Result Q Units Page
001 95818 BAY #144 Solid C19 - C36 Aliphatics MADEP-EPH-12000 mg/kg 11
001 95818 BAY #144 Solid C9 - C12 Aliphatics MADEP-VPH-5.1 mg/kg 12
001 95818 BAY #144 Solid C9 - C10 Aromatics MADEP-VPH-7.6 mg/kg 13
002 610 NC 343 SOUTH Solid Acetone 8260D 70 ug/kg 14
002 610 NC 343 SOUTH Solid Pyrene 8270E 690 ug/kg 17
002 610 NC 343 SOUTH Solid C11 - C22 Aromatics MADEP-EPH-330 mg/kg 18
002 610 NC 343 SOUTH Solid C9 - C18 Aliphatics MADEP-EPH-410 mg/kg 19
002 610 NC 343 SOUTH Solid C19 - C36 Aliphatics MADEP-EPH-1900 mg/kg 19
002 610 NC 343 SOUTH Solid C9 - C12 Aliphatics MADEP-VPH-15 mg/kg 20
002 610 NC 343 SOUTH Solid C9 - C10 Aromatics MADEP-VPH-17 mg/kg 21
003 13993 MW-1 Aqueous Benzene SM 6200B-2600 ug/L 22
003 13993 MW-1 Aqueous n-Butylbenzene SM 6200B-40 ug/L 22
003 13993 MW-1 Aqueous Ethylbenzene SM 6200B-1600 ug/L 22
003 13993 MW-1 Aqueous Isopropylbenzene SM 6200B-110 ug/L 22
003 13993 MW-1 Aqueous Methyl tertiary butyl ether SM 6200B-120 ug/L 22
003 13993 MW-1 Aqueous Naphthalene SM 6200B-600 ug/L 22
003 13993 MW-1 Aqueous n-Propylbenzene SM 6200B-330 ug/L 22
003 13993 MW-1 Aqueous Toluene SM 6200B-47 ug/L 23
003 13993 MW-1 Aqueous 1,3,5-Trimethylbenzene SM 6200B-28 ug/L 23
003 13993 MW-1 Aqueous 1,2,4-Trimethylbenzene SM 6200B-100 ug/L 23
003 13993 MW-1 Aqueous m+p - Xylenes SM 6200B-210 ug/L 23
(21 detections)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 4 of 60
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
DEQ DWM
95818 BAY #144
VJ01071-001
09/29/2020 1700
10/01/2020
Solid
% Solids:95.4 10/02/2020 2342
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260D 1 10/03/2020 0002 STM 68713 5.26
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
Acetone 67-64-1 8260D ND 1ug/kg20
Benzene 71-43-2 8260D ND 1ug/kg5.0
Bromodichloromethane 75-27-4 8260D ND 1ug/kg5.0
Bromoform 75-25-2 8260D ND 1ug/kg5.0
Bromomethane (Methyl bromide)74-83-9 8260D ND 1ug/kg5.0
2-Butanone (MEK)78-93-3 8260D ND 1ug/kg20
Carbon disulfide 75-15-0 8260D ND 1ug/kg5.0
Carbon tetrachloride 56-23-5 8260D ND 1ug/kg5.0
Chlorobenzene 108-90-7 8260D ND 1ug/kg5.0
Chloroethane 75-00-3 8260D ND 1ug/kg5.0
Chloroform 67-66-3 8260D ND 1ug/kg5.0
Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/kg5.0
Cyclohexane 110-82-7 8260D ND 1ug/kg5.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/kg5.0
Dibromochloromethane 124-48-1 8260D ND 1ug/kg5.0
1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/kg5.0
1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/kg5.0
1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/kg5.0
1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/kg5.0
Dichlorodifluoromethane 75-71-8 8260D ND 1ug/kg5.0
1,1-Dichloroethane 75-34-3 8260D ND 1ug/kg5.0
1,2-Dichloroethane 107-06-2 8260D ND 1ug/kg5.0
1,1-Dichloroethene 75-35-4 8260D ND 1ug/kg5.0
cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/kg5.0
trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/kg5.0
1,2-Dichloropropane 78-87-5 8260D ND 1ug/kg5.0
cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/kg5.0
trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/kg5.0
Ethylbenzene 100-41-4 8260D ND 1ug/kg5.0
2-Hexanone 591-78-6 8260D ND 1ug/kg10
Isopropylbenzene 98-82-8 8260D ND 1ug/kg5.0
Methyl acetate 79-20-9 8260D ND 1ug/kg5.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260D ND 1ug/kg5.0
4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/kg10
Methylcyclohexane 108-87-2 8260D ND 1ug/kg5.0
Methylene chloride 75-09-2 8260D ND 1ug/kg5.0
Styrene 100-42-5 8260D ND 1ug/kg5.0
1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/kg5.0
Tetrachloroethene 127-18-4 8260D ND 1ug/kg5.0
Toluene 108-88-3 8260D ND 1ug/kg5.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/kg5.0
1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/kg5.0
1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/kg5.0
1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/kg5.0
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 5 of 60
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
DEQ DWM
95818 BAY #144
VJ01071-001
09/29/2020 1700
10/01/2020
Solid
% Solids:95.4 10/02/2020 2342
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260D 1 10/03/2020 0002 STM 68713 5.26
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
Trichloroethene 79-01-6 8260D ND 1ug/kg5.0
Trichlorofluoromethane 75-69-4 8260D ND 1ug/kg5.0
Vinyl chloride 75-01-4 8260D ND 1ug/kg5.0
Xylenes (total)1330-20-7 8260D ND 1ug/kg10
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 83 47-138
1,2-Dichloroethane-d4 120 53-142
Toluene-d8 N 176 68-124
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 6 of 60
Semivolatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
DEQ DWM
95818 BAY #144
VJ01071-001
09/29/2020 1700
10/01/2020
Solid
% Solids:95.4 10/02/2020 2342
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270E 100 10/15/2020 1629 SCD 10/05/2020 1530 68844
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
Acenaphthene 83-32-9 8270E ND 1ug/kg1400
Acenaphthylene 208-96-8 8270E ND 1ug/kg1400
Acetophenone 98-86-2 8270E ND 1ug/kg6600
Anthracene 120-12-7 8270E ND 1ug/kg1400
Atrazine 1912-24-9 8270E ND 1ug/kg6600
Benzaldehyde 100-52-7 8270E ND 1ug/kg6600
Benzo(a)anthracene 56-55-3 8270E ND 1ug/kg1400
Benzo(a)pyrene 50-32-8 8270E ND 1ug/kg1400
Benzo(b)fluoranthene 205-99-2 8270E ND 1ug/kg1400
Benzo(g,h,i)perylene 191-24-2 8270E ND 1ug/kg1400
Benzo(k)fluoranthene 207-08-9 8270E ND 1ug/kg1400
1,1'-Biphenyl 92-52-4 8270E ND 1ug/kg6600
4-Bromophenyl phenyl ether 101-55-3 8270E ND 1ug/kg6600
Butyl benzyl phthalate 85-68-7 8270E ND 1ug/kg6600
Caprolactam 105-60-2 8270E ND 1ug/kg6600
Carbazole 86-74-8 8270E ND 1ug/kg6600
bis (2-Chloro-1-methylethyl) ether 108-60-1 8270E ND 1ug/kg6600
4-Chloro-3-methyl phenol 59-50-7 8270E ND 1ug/kg6600
4-Chloroaniline 106-47-8 8270E ND 1ug/kg6600
bis(2-Chloroethoxy)methane 111-91-1 8270E ND 1ug/kg6600
bis(2-Chloroethyl)ether 111-44-4 8270E ND 1ug/kg6600
2-Chloronaphthalene 91-58-7 8270E ND 1ug/kg6600
2-Chlorophenol 95-57-8 8270E ND 1ug/kg6600
4-Chlorophenyl phenyl ether 7005-72-3 8270E ND 1ug/kg6600
Chrysene 218-01-9 8270E ND 1ug/kg1400
Dibenzo(a,h)anthracene 53-70-3 8270E ND 1ug/kg1400
Dibenzofuran 132-64-9 8270E ND 1ug/kg6600
3,3'-Dichlorobenzidine 91-94-1 8270E ND 1ug/kg6600
2,4-Dichlorophenol 120-83-2 8270E ND 1ug/kg6600
Diethylphthalate 84-66-2 8270E ND 1ug/kg6600
Dimethyl phthalate 131-11-3 8270E ND 1ug/kg6600
2,4-Dimethylphenol 105-67-9 8270E ND 1ug/kg6600
Di-n-butyl phthalate 84-74-2 8270E ND 1ug/kg6600
4,6-Dinitro-2-methylphenol 534-52-1 8270E ND 1ug/kg34000
2,4-Dinitrophenol 51-28-5 8270E ND 1ug/kg34000
2,4-Dinitrotoluene 121-14-2 8270E ND 1ug/kg14000
2,6-Dinitrotoluene 606-20-2 8270E ND 1ug/kg14000
Di-n-octylphthalate 117-84-0 8270E ND 1ug/kg6600
bis(2-Ethylhexyl)phthalate 117-81-7 8270E ND 1ug/kg34000
Fluoranthene 206-44-0 8270E ND 1ug/kg1400
Fluorene 86-73-7 8270E ND 1ug/kg1400
Hexachlorobenzene 118-74-1 8270E ND 1ug/kg6600
Hexachlorobutadiene 87-68-3 8270E ND 1ug/kg6600
Hexachlorocyclopentadiene 77-47-4 8270E ND 1ug/kg34000
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 7 of 60
Semivolatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
DEQ DWM
95818 BAY #144
VJ01071-001
09/29/2020 1700
10/01/2020
Solid
% Solids:95.4 10/02/2020 2342
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270E 100 10/15/2020 1629 SCD 10/05/2020 1530 68844
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
Hexachloroethane 67-72-1 8270E ND 1ug/kg6600
Indeno(1,2,3-c,d)pyrene 193-39-5 8270E ND 1ug/kg1400
Isophorone 78-59-1 8270E ND 1ug/kg6600
2-Methylnaphthalene 91-57-6 8270E ND 1ug/kg1400
2-Methylphenol 95-48-7 8270E ND 1ug/kg6600
3+4-Methylphenol 106-44-5 8270E ND 1ug/kg14000
Naphthalene 91-20-3 8270E ND 1ug/kg1400
2-Nitroaniline 88-74-4 8270E ND 1ug/kg14000
3-Nitroaniline 99-09-2 8270E ND 1ug/kg14000
4-Nitroaniline 100-01-6 8270E ND 1ug/kg14000
Nitrobenzene 98-95-3 8270E ND 1ug/kg6600
2-Nitrophenol 88-75-5 8270E ND 1ug/kg14000
4-Nitrophenol 100-02-7 8270E ND 1ug/kg34000
N-Nitrosodi-n-propylamine 621-64-7 8270E ND 1ug/kg6600
N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270E ND 1ug/kg6600
Pentachlorophenol 87-86-5 8270E ND 1ug/kg34000
Phenanthrene 85-01-8 8270E ND 1ug/kg1400
Phenol 108-95-2 8270E ND 1ug/kg6600
Pyrene 129-00-0 8270E ND 1ug/kg1400
2,4,5-Trichlorophenol 95-95-4 8270E ND 1ug/kg6600
2,4,6-Trichlorophenol 88-06-2 8270E ND 1ug/kg6600
AcceptanceRun 1
Surrogate Q % Recovery Limits
2-Fluorobiphenyl 100 33-102
2-Fluorophenol N 18 35-115
Nitrobenzene-d5 108 22-109
Phenol-d5 N 0.00 33-122
Terphenyl-d14 N 189 41-120
2,4,6-Tribromophenol 36 30-117
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 8 of 60
MA EPH (aromatics)
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
DEQ DWM
95818 BAY #144
VJ01071-001
09/29/2020 1700
10/01/2020
Solid
% Solids:95.4 10/02/2020 2342
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH-MADEP-EPH-04 50 10/07/2020 1638 JJG 10/06/2020 0828 68902
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
C11 - C22 Aromatics MADEP-EPH-04 ND 1mg/kg500
AcceptanceRun 1
Surrogate Q % Recovery Limits
2-Bromonaphthalene (fractionation 2)48 40-140
2-Fluorobiphenyl (fractionation 1)75 40-140
o - Terphenyl (aromatic)64 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 9 of 60
MA EPH (aliphatics)
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
DEQ DWM
95818 BAY #144
VJ01071-001
09/29/2020 1700
10/01/2020
Solid
% Solids:95.4 10/02/2020 2342
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH-MADEP-EPH-04 50 10/07/2020 1206 JJG 10/06/2020 0828 68901
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
C9 - C18 Aliphatics MADEP-EPH-04 ND 1mg/kg500
C19 - C36 Aliphatics MADEP-EPH-04 12000 1mg/kg500
AcceptanceRun 1
Surrogate Q % Recovery Limits
1-Chloro-octadecane (aliphatic)N 37 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 10 of 60
MADEP VPH (aliphatics)
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
DEQ DWM
95818 BAY #144
VJ01071-001
09/29/2020 1700
10/01/2020
Solid
% Solids:95.4 10/02/2020 2342
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-18-2.1 1 10/12/2020 1512 ECB 69569
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
C5 - C8 Aliphatics MADEP-VPH-18-ND 1mg/kg1.7
C9 - C12 Aliphatics MADEP-VPH-18-5.1 1mg/kg1.7
AcceptanceRun 1
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (FID)N 23 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 11 of 60
MADEP VPH (aromatics)
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
DEQ DWM
95818 BAY #144
VJ01071-001
09/29/2020 1700
10/01/2020
Solid
% Solids:95.4 10/02/2020 2342
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-18-2.1 1 10/12/2020 1512 ECB 69573
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
C9 - C10 Aromatics MADEP-VPH-18-7.6 1mg/kg0.55
AcceptanceRun 1
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (PID)N 12 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 12 of 60
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
DEQ DWM
610 NC 343 SOUTH
VJ01071-002
09/29/2020 1840
10/01/2020
Solid
% Solids:77.9 10/02/2020 2342
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260D 1 10/03/2020 0024 STM 68713 4.71
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
Acetone 67-64-1 8260D 70 1ug/kg27
Benzene 71-43-2 8260D ND 1ug/kg6.8
Bromodichloromethane 75-27-4 8260D ND 1ug/kg6.8
Bromoform 75-25-2 8260D ND 1ug/kg6.8
Bromomethane (Methyl bromide)74-83-9 8260D ND 1ug/kg6.8
2-Butanone (MEK)78-93-3 8260D ND 1ug/kg27
Carbon disulfide 75-15-0 8260D ND 1ug/kg6.8
Carbon tetrachloride 56-23-5 8260D ND 1ug/kg6.8
Chlorobenzene 108-90-7 8260D ND 1ug/kg6.8
Chloroethane 75-00-3 8260D ND 1ug/kg6.8
Chloroform 67-66-3 8260D ND 1ug/kg6.8
Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/kg6.8
Cyclohexane 110-82-7 8260D ND 1ug/kg6.8
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/kg6.8
Dibromochloromethane 124-48-1 8260D ND 1ug/kg6.8
1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/kg6.8
1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/kg6.8
1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/kg6.8
1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/kg6.8
Dichlorodifluoromethane 75-71-8 8260D ND 1ug/kg6.8
1,1-Dichloroethane 75-34-3 8260D ND 1ug/kg6.8
1,2-Dichloroethane 107-06-2 8260D ND 1ug/kg6.8
1,1-Dichloroethene 75-35-4 8260D ND 1ug/kg6.8
cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/kg6.8
trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/kg6.8
1,2-Dichloropropane 78-87-5 8260D ND 1ug/kg6.8
cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/kg6.8
trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/kg6.8
Ethylbenzene 100-41-4 8260D ND 1ug/kg6.8
2-Hexanone 591-78-6 8260D ND 1ug/kg14
Isopropylbenzene 98-82-8 8260D ND 1ug/kg6.8
Methyl acetate 79-20-9 8260D ND 1ug/kg6.8
Methyl tertiary butyl ether (MTBE)1634-04-4 8260D ND 1ug/kg6.8
4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/kg14
Methylcyclohexane 108-87-2 8260D ND 1ug/kg6.8
Methylene chloride 75-09-2 8260D ND 1ug/kg6.8
Styrene 100-42-5 8260D ND 1ug/kg6.8
1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/kg6.8
Tetrachloroethene 127-18-4 8260D ND 1ug/kg6.8
Toluene 108-88-3 8260D ND 1ug/kg6.8
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/kg6.8
1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/kg6.8
1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/kg6.8
1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/kg6.8
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 13 of 60
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
DEQ DWM
610 NC 343 SOUTH
VJ01071-002
09/29/2020 1840
10/01/2020
Solid
% Solids:77.9 10/02/2020 2342
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260D 1 10/03/2020 0024 STM 68713 4.71
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
Trichloroethene 79-01-6 8260D ND 1ug/kg6.8
Trichlorofluoromethane 75-69-4 8260D ND 1ug/kg6.8
Vinyl chloride 75-01-4 8260D ND 1ug/kg6.8
Xylenes (total)1330-20-7 8260D ND 1ug/kg14
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 88 47-138
1,2-Dichloroethane-d4 108 53-142
Toluene-d8 N 148 68-124
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 14 of 60
Semivolatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
DEQ DWM
610 NC 343 SOUTH
VJ01071-002
09/29/2020 1840
10/01/2020
Solid
% Solids:77.9 10/02/2020 2342
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270E 100 10/15/2020 1744 SCD 10/05/2020 1530 68844
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
Acenaphthene 83-32-9 8270E ND 1ug/kg330
Acenaphthylene 208-96-8 8270E ND 1ug/kg330
Acetophenone 98-86-2 8270E ND 1ug/kg1600
Anthracene 120-12-7 8270E ND 1ug/kg330
Atrazine 1912-24-9 8270E ND 1ug/kg1600
Benzaldehyde 100-52-7 8270E ND 1ug/kg1600
Benzo(a)anthracene 56-55-3 8270E ND 1ug/kg330
Benzo(a)pyrene 50-32-8 8270E ND 1ug/kg330
Benzo(b)fluoranthene 205-99-2 8270E ND 1ug/kg330
Benzo(g,h,i)perylene 191-24-2 8270E ND 1ug/kg330
Benzo(k)fluoranthene 207-08-9 8270E ND 1ug/kg330
1,1'-Biphenyl 92-52-4 8270E ND 1ug/kg1600
4-Bromophenyl phenyl ether 101-55-3 8270E ND 1ug/kg1600
Butyl benzyl phthalate 85-68-7 8270E ND 1ug/kg1600
Caprolactam 105-60-2 8270E ND 1ug/kg1600
Carbazole 86-74-8 8270E ND 1ug/kg1600
bis (2-Chloro-1-methylethyl) ether 108-60-1 8270E ND 1ug/kg1600
4-Chloro-3-methyl phenol 59-50-7 8270E ND 1ug/kg1600
4-Chloroaniline 106-47-8 8270E ND 1ug/kg1600
bis(2-Chloroethoxy)methane 111-91-1 8270E ND 1ug/kg1600
bis(2-Chloroethyl)ether 111-44-4 8270E ND 1ug/kg1600
2-Chloronaphthalene 91-58-7 8270E ND 1ug/kg1600
2-Chlorophenol 95-57-8 8270E ND 1ug/kg1600
4-Chlorophenyl phenyl ether 7005-72-3 8270E ND 1ug/kg1600
Chrysene 218-01-9 8270E ND 1ug/kg330
Dibenzo(a,h)anthracene 53-70-3 8270E ND 1ug/kg330
Dibenzofuran 132-64-9 8270E ND 1ug/kg1600
3,3'-Dichlorobenzidine 91-94-1 8270E ND 1ug/kg1600
2,4-Dichlorophenol 120-83-2 8270E ND 1ug/kg1600
Diethylphthalate 84-66-2 8270E ND 1ug/kg1600
Dimethyl phthalate 131-11-3 8270E ND 1ug/kg1600
2,4-Dimethylphenol 105-67-9 8270E ND 1ug/kg1600
Di-n-butyl phthalate 84-74-2 8270E ND 1ug/kg1600
4,6-Dinitro-2-methylphenol 534-52-1 8270E ND 1ug/kg8100
2,4-Dinitrophenol 51-28-5 8270E ND 1ug/kg8100
2,4-Dinitrotoluene 121-14-2 8270E ND 1ug/kg3300
2,6-Dinitrotoluene 606-20-2 8270E ND 1ug/kg3300
Di-n-octylphthalate 117-84-0 8270E ND 1ug/kg1600
bis(2-Ethylhexyl)phthalate 117-81-7 8270E ND 1ug/kg8100
Fluoranthene 206-44-0 8270E ND 1ug/kg330
Fluorene 86-73-7 8270E ND 1ug/kg330
Hexachlorobenzene 118-74-1 8270E ND 1ug/kg1600
Hexachlorobutadiene 87-68-3 8270E ND 1ug/kg1600
Hexachlorocyclopentadiene 77-47-4 8270E ND 1ug/kg8100
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 15 of 60
Semivolatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
DEQ DWM
610 NC 343 SOUTH
VJ01071-002
09/29/2020 1840
10/01/2020
Solid
% Solids:77.9 10/02/2020 2342
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270E 100 10/15/2020 1744 SCD 10/05/2020 1530 68844
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
Hexachloroethane 67-72-1 8270E ND 1ug/kg1600
Indeno(1,2,3-c,d)pyrene 193-39-5 8270E ND 1ug/kg330
Isophorone 78-59-1 8270E ND 1ug/kg1600
2-Methylnaphthalene 91-57-6 8270E ND 1ug/kg330
2-Methylphenol 95-48-7 8270E ND 1ug/kg1600
3+4-Methylphenol 106-44-5 8270E ND 1ug/kg3300
Naphthalene 91-20-3 8270E ND 1ug/kg330
2-Nitroaniline 88-74-4 8270E ND 1ug/kg3300
3-Nitroaniline 99-09-2 8270E ND 1ug/kg3300
4-Nitroaniline 100-01-6 8270E ND 1ug/kg3300
Nitrobenzene 98-95-3 8270E ND 1ug/kg1600
2-Nitrophenol 88-75-5 8270E ND 1ug/kg3300
4-Nitrophenol 100-02-7 8270E ND 1ug/kg8100
N-Nitrosodi-n-propylamine 621-64-7 8270E ND 1ug/kg1600
N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270E ND 1ug/kg1600
Pentachlorophenol 87-86-5 8270E ND 1ug/kg8100
Phenanthrene 85-01-8 8270E ND 1ug/kg330
Phenol 108-95-2 8270E ND 1ug/kg1600
Pyrene 129-00-0 8270E 690 1ug/kg330
2,4,5-Trichlorophenol 95-95-4 8270E ND 1ug/kg1600
2,4,6-Trichlorophenol 88-06-2 8270E ND 1ug/kg1600
AcceptanceRun 1
Surrogate Q % Recovery Limits
2-Fluorobiphenyl 92 33-102
2-Fluorophenol 56 35-115
Nitrobenzene-d5 N 126 22-109
Phenol-d5 76 33-122
Terphenyl-d14 104 41-120
2,4,6-Tribromophenol 41 30-117
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 16 of 60
MA EPH (aromatics)
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
DEQ DWM
610 NC 343 SOUTH
VJ01071-002
09/29/2020 1840
10/01/2020
Solid
% Solids:77.9 10/02/2020 2342
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH-MADEP-EPH-04 1 10/09/2020 1850 JJG 10/06/2020 0828 68902
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
C11 - C22 Aromatics MADEP-EPH-04 330 1mg/kg12
AcceptanceRun 1
Surrogate Q % Recovery Limits
2-Bromonaphthalene (fractionation 2)95 40-140
2-Fluorobiphenyl (fractionation 1)106 40-140
o - Terphenyl (aromatic)69 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 17 of 60
MA EPH (aliphatics)
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
DEQ DWM
610 NC 343 SOUTH
VJ01071-002
09/29/2020 1840
10/01/2020
Solid
% Solids:77.9 10/02/2020 2342
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH-MADEP-EPH-04 1 10/09/2020 1720 JJG 10/06/2020 0828 68901
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
C9 - C18 Aliphatics MADEP-EPH-04 410 1mg/kg12
C19 - C36 Aliphatics MADEP-EPH-04 1900 1mg/kg12
AcceptanceRun 1
Surrogate Q % Recovery Limits
1-Chloro-octadecane (aliphatic)66 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 18 of 60
MADEP VPH (aliphatics)
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
DEQ DWM
610 NC 343 SOUTH
VJ01071-002
09/29/2020 1840
10/01/2020
Solid
% Solids:77.9 10/02/2020 2342
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-18-2.1 1 10/12/2020 1540 ECB 69569
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
C5 - C8 Aliphatics MADEP-VPH-18-ND 1mg/kg2.5
C9 - C12 Aliphatics MADEP-VPH-18-15 1mg/kg2.5
AcceptanceRun 1
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (FID)N 45 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 19 of 60
MADEP VPH (aromatics)
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
DEQ DWM
610 NC 343 SOUTH
VJ01071-002
09/29/2020 1840
10/01/2020
Solid
% Solids:77.9 10/02/2020 2342
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-18-2.1 1 10/12/2020 1540 ECB 69573
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
C9 - C10 Aromatics MADEP-VPH-18-17 1mg/kg0.84
AcceptanceRun 1
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (PID)N 17 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 20 of 60
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
DEQ DWM
13993 MW-1
VJ01071-003
09/30/2020 1330
10/01/2020
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 50 10/08/2020 1934 TML 69252
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
Benzene 71-43-2 SM 6200B-2011 2600 1ug/L25
Bromobenzene 108-86-1 SM 6200B-2011 ND 1ug/L25
Bromochloromethane 74-97-5 SM 6200B-2011 ND 1ug/L25
Bromodichloromethane 75-27-4 SM 6200B-2011 ND 1ug/L25
Bromoform 75-25-2 SM 6200B-2011 ND 1ug/L25
Bromomethane (Methyl bromide)74-83-9 SM 6200B-2011 ND 1ug/L25
n-Butylbenzene 104-51-8 SM 6200B-2011 40 1ug/L25
sec-Butylbenzene 135-98-8 SM 6200B-2011 ND 1ug/L25
tert-Butylbenzene 98-06-6 SM 6200B-2011 ND 1ug/L25
Carbon tetrachloride 56-23-5 SM 6200B-2011 ND 1ug/L25
Chlorobenzene 108-90-7 SM 6200B-2011 ND 1ug/L25
Chloroethane 75-00-3 SM 6200B-2011 ND 1ug/L25
Chloroform 67-66-3 SM 6200B-2011 ND 1ug/L25
Chloromethane (Methyl chloride)74-87-3 SM 6200B-2011 ND 1ug/L25
2-Chlorotoluene 95-49-8 SM 6200B-2011 ND 1ug/L25
4-Chlorotoluene 106-43-4 SM 6200B-2011 ND 1ug/L25
Dibromochloromethane 124-48-1 SM 6200B-2011 ND 1ug/L25
1,2-Dibromoethane (EDB)106-93-4 SM 6200B-2011 ND 1ug/L25
Dibromomethane (Methylene bromide)74-95-3 SM 6200B-2011 ND 1ug/L25
1,2-Dichlorobenzene 95-50-1 SM 6200B-2011 ND 1ug/L25
1,3-Dichlorobenzene 541-73-1 SM 6200B-2011 ND 1ug/L25
1,4-Dichlorobenzene 106-46-7 SM 6200B-2011 ND 1ug/L25
Dichlorodifluoromethane 75-71-8 SM 6200B-2011 ND 1ug/L25
1,1-Dichloroethane 75-34-3 SM 6200B-2011 ND 1ug/L25
1,2-Dichloroethane 107-06-2 SM 6200B-2011 ND 1ug/L25
1,1-Dichloroethene 75-35-4 SM 6200B-2011 ND 1ug/L25
cis-1,2-Dichloroethene 156-59-2 SM 6200B-2011 ND 1ug/L25
trans-1,2-Dichloroethene 156-60-5 SM 6200B-2011 ND 1ug/L25
1,2-Dichloropropane 78-87-5 SM 6200B-2011 ND 1ug/L25
1,3-Dichloropropane 142-28-9 SM 6200B-2011 ND 1ug/L25
2,2-Dichloropropane 594-20-7 SM 6200B-2011 ND 1ug/L25
1,1-Dichloropropene 563-58-6 SM 6200B-2011 ND 1ug/L25
cis-1,3-Dichloropropene 10061-01-5 SM 6200B-2011 ND 1ug/L25
trans-1,3-Dichloropropene 10061-02-6 SM 6200B-2011 ND 1ug/L25
Diisopropyl ether (IPE)108-20-3 SM 6200B-2011 ND 1ug/L25
Ethylbenzene 100-41-4 SM 6200B-2011 1600 1ug/L25
Hexachlorobutadiene 87-68-3 SM 6200B-2011 ND 1ug/L25
Isopropylbenzene (Cumene)98-82-8 SM 6200B-2011 110 1ug/L25
p-Isopropyltoluene (p-Cymene)99-87-6 SM 6200B-2011 ND 1ug/L25
Methyl tertiary butyl ether (MTBE)1634-04-4 SM 6200B-2011 120 1ug/L25
Methylene chloride 75-09-2 SM 6200B-2011 ND 1ug/L25
Naphthalene 91-20-3 SM 6200B-2011 600 1ug/L25
n-Propylbenzene 103-65-1 SM 6200B-2011 330 1ug/L25
Styrene 100-42-5 SM 6200B-2011 ND 1ug/L25
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 21 of 60
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
DEQ DWM
13993 MW-1
VJ01071-003
09/30/2020 1330
10/01/2020
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 50 10/08/2020 1934 TML 69252
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
1,1,1,2-Tetrachloroethane 630-20-6 SM 6200B-2011 ND 1ug/L25
1,1,2,2-Tetrachloroethane 79-34-5 SM 6200B-2011 ND 1ug/L25
Tetrachloroethene 127-18-4 SM 6200B-2011 ND 1ug/L25
Toluene 108-88-3 SM 6200B-2011 47 1ug/L25
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 SM 6200B-2011 ND 1ug/L25
1,2,3-Trichlorobenzene 87-61-6 SM 6200B-2011 ND 1ug/L25
1,2,4-Trichlorobenzene 120-82-1 SM 6200B-2011 ND 1ug/L25
1,1,1-Trichloroethane 71-55-6 SM 6200B-2011 ND 1ug/L25
1,1,2-Trichloroethane 79-00-5 SM 6200B-2011 ND 1ug/L25
Trichloroethene 79-01-6 SM 6200B-2011 ND 1ug/L25
Trichlorofluoromethane 75-69-4 SM 6200B-2011 ND 1ug/L25
1,2,3-Trichloropropane 96-18-4 SM 6200B-2011 ND 1ug/L25
1,3,5-Trimethylbenzene (Mesitylene)108-67-8 SM 6200B-2011 28 1ug/L25
1,2,4-Trimethylbenzene 95-63-6 SM 6200B-2011 100 1ug/L25
Vinyl chloride 75-01-4 SM 6200B-2011 ND 1ug/L25
m+p - Xylenes 179601-23-1 SM 6200B-2011 210 1ug/L25
o - Xylenes 95-47-6 SM 6200B-2011 ND 1ug/L25
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 99 70-130
Bromofluorobenzene 88 70-130
Toluene-d8 97 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 22 of 60
QC Summary
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 23 of 60
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:VQ68713-001
68713 5035
Analytical Method:8260D
Matrix:Solid
Parameter Result Q LOQ Units Analysis DateDil
Acetone ND 10/02/2020 200320ug/kg1
Benzene ND 10/02/2020 20035.0 ug/kg1
Bromodichloromethane ND 10/02/2020 20035.0 ug/kg1
Bromoform ND 10/02/2020 20035.0 ug/kg1
Bromomethane (Methyl bromide)ND 10/02/2020 20035.0 ug/kg1
2-Butanone (MEK)ND 10/02/2020 200320ug/kg1
Carbon disulfide ND 10/02/2020 20035.0 ug/kg1
Carbon tetrachloride ND 10/02/2020 20035.0 ug/kg1
Chlorobenzene ND 10/02/2020 20035.0 ug/kg1
Chloroethane ND 10/02/2020 20035.0 ug/kg1
Chloroform ND 10/02/2020 20035.0 ug/kg1
Chloromethane (Methyl chloride)ND 10/02/2020 20035.0 ug/kg1
Cyclohexane ND 10/02/2020 20035.0 ug/kg1
1,2-Dibromo-3-chloropropane (DBCP)ND 10/02/2020 20035.0 ug/kg1
Dibromochloromethane ND 10/02/2020 20035.0 ug/kg1
1,2-Dibromoethane (EDB)ND 10/02/2020 20035.0 ug/kg1
1,2-Dichlorobenzene ND 10/02/2020 20035.0 ug/kg1
1,3-Dichlorobenzene ND 10/02/2020 20035.0 ug/kg1
1,4-Dichlorobenzene ND 10/02/2020 20035.0 ug/kg1
Dichlorodifluoromethane ND 10/02/2020 20035.0 ug/kg1
1,1-Dichloroethane ND 10/02/2020 20035.0 ug/kg1
1,2-Dichloroethane ND 10/02/2020 20035.0 ug/kg1
1,1-Dichloroethene ND 10/02/2020 20035.0 ug/kg1
cis-1,2-Dichloroethene ND 10/02/2020 20035.0 ug/kg1
trans-1,2-Dichloroethene ND 10/02/2020 20035.0 ug/kg1
1,2-Dichloropropane ND 10/02/2020 20035.0 ug/kg1
cis-1,3-Dichloropropene ND 10/02/2020 20035.0 ug/kg1
trans-1,3-Dichloropropene ND 10/02/2020 20035.0 ug/kg1
Ethylbenzene ND 10/02/2020 20035.0 ug/kg1
2-Hexanone ND 10/02/2020 200310ug/kg1
Isopropylbenzene ND 10/02/2020 20035.0 ug/kg1
Methyl acetate ND 10/02/2020 20035.0 ug/kg1
Methyl tertiary butyl ether (MTBE)ND 10/02/2020 20035.0 ug/kg1
4-Methyl-2-pentanone ND 10/02/2020 200310ug/kg1
Methylcyclohexane ND 10/02/2020 20035.0 ug/kg1
Methylene chloride ND 10/02/2020 20035.0 ug/kg1
Styrene ND 10/02/2020 20035.0 ug/kg1
1,1,2,2-Tetrachloroethane ND 10/02/2020 20035.0 ug/kg1
Tetrachloroethene ND 10/02/2020 20035.0 ug/kg1
Toluene ND 10/02/2020 20035.0 ug/kg1
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 10/02/2020 20035.0 ug/kg1
1,2,4-Trichlorobenzene ND 10/02/2020 20035.0 ug/kg1
1,1,1-Trichloroethane ND 10/02/2020 20035.0 ug/kg1
1,1,2-Trichloroethane ND 10/02/2020 20035.0 ug/kg1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 24 of 60
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:VQ68713-001
68713 5035
Analytical Method:8260D
Matrix:Solid
Parameter Result Q LOQ Units Analysis DateDil
Trichloroethene ND 10/02/2020 20035.0 ug/kg1
Trichlorofluoromethane ND 10/02/2020 20035.0 ug/kg1
Vinyl chloride ND 10/02/2020 20035.0 ug/kg1
Xylenes (total)ND 10/02/2020 200310ug/kg1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 117 47-138
1,2-Dichloroethane-d4 100 53-142
Toluene-d8 117 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 25 of 60
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:VQ68713-002
68713 5035
Analytical Method:8260D
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Acetone 93 10/02/2020 18469310060-1401
Benzene 53 10/02/2020 18461075070-1301
Bromodichloromethane 50 10/02/2020 18461015070-1301
Bromoform 53 10/02/2020 18461075070-1301
Bromomethane (Methyl bromide)44 10/02/2020 1846885070-1301
2-Butanone (MEK)110 10/02/2020 184610610060-1401
Carbon disulfide 55 10/02/2020 18461105070-1301
Carbon tetrachloride 51 10/02/2020 18461025070-1301
Chlorobenzene 53 10/02/2020 18461075070-1301
Chloroethane 44 10/02/2020 1846885070-1301
Chloroform 50 10/02/2020 18461015070-1301
Chloromethane (Methyl chloride)41 10/02/2020 1846815060-1401
Cyclohexane 53 10/02/2020 18461065070-1301
1,2-Dibromo-3-chloropropane (DBCP)51 10/02/2020 18461015070-1301
Dibromochloromethane 52 10/02/2020 18461045070-1301
1,2-Dibromoethane (EDB)53 10/02/2020 18461055070-1301
1,2-Dichlorobenzene 51 10/02/2020 18461035070-1301
1,3-Dichlorobenzene 55 10/02/2020 18461095070-1301
1,4-Dichlorobenzene 54 10/02/2020 18461085070-1301
Dichlorodifluoromethane 37 10/02/2020 1846735060-1401
1,1-Dichloroethane 53 10/02/2020 18461055070-1301
1,2-Dichloroethane 49 10/02/2020 1846985070-1301
1,1-Dichloroethene 55 10/02/2020 18461095070-1301
cis-1,2-Dichloroethene 51 10/02/2020 18461025070-1301
trans-1,2-Dichloroethene 53 10/02/2020 18461065070-1301
1,2-Dichloropropane 52 10/02/2020 18461045070-1301
cis-1,3-Dichloropropene 53 10/02/2020 18461055070-1301
trans-1,3-Dichloropropene 54 10/02/2020 18461075070-1301
Ethylbenzene 56 10/02/2020 18461115070-1301
2-Hexanone 110 10/02/2020 184611310070-1301
Isopropylbenzene 58 10/02/2020 18461165070-1301
Methyl acetate 56 10/02/2020 18461125070-1301
Methyl tertiary butyl ether (MTBE)49 10/02/2020 1846985070-1301
4-Methyl-2-pentanone 110 10/02/2020 184610710070-1301
Methylcyclohexane 57 10/02/2020 18461145070-1301
Methylene chloride 47 10/02/2020 1846945070-1301
Styrene 55 10/02/2020 18461105070-1301
1,1,2,2-Tetrachloroethane 51 10/02/2020 18461035070-1301
Tetrachloroethene 58 10/02/2020 18461165070-1301
Toluene 55 10/02/2020 18461095070-1301
1,1,2-Trichloro-1,2,2-Trifluoroethane 56 10/02/2020 18461115070-1301
1,2,4-Trichlorobenzene 59 10/02/2020 18461185070-1301
1,1,1-Trichloroethane 50 10/02/2020 18461015070-1301
1,1,2-Trichloroethane 52 10/02/2020 18461035070-1301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 26 of 60
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:VQ68713-002
68713 5035
Analytical Method:8260D
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Trichloroethene 54 10/02/2020 18461095070-1301
Trichlorofluoromethane 49 10/02/2020 1846985070-1301
Vinyl chloride 47 10/02/2020 1846935070-1301
Xylenes (total)110 10/02/2020 184611110070-1301
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 115 47-138
1,2-Dichloroethane-d4 97 53-142
Toluene-d8 110 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 27 of 60
Volatile Organic Compounds by GC/MS - LCSD
Batch:Prep Method:
Sample ID:VQ68713-003
68713 5035
Analytical Method:8260D
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/kg)(ug/kg)
Acetone 93 10/02/2020 19219310060-1400.23 201
Benzene 51 10/02/2020 19211035070-1303.9 201
Bromodichloromethane 49 10/02/2020 1921985070-1302.6 201
Bromoform 53 10/02/2020 19211075070-1300.069 201
Bromomethane (Methyl bromide)41 10/02/2020 1921835070-1306.0 201
2-Butanone (MEK)100 10/02/2020 192110310060-1403.3 201
Carbon disulfide 50 10/02/2020 19211015070-1308.3 201
Carbon tetrachloride 47 10/02/2020 1921955070-1307.2 201
Chlorobenzene 51 10/02/2020 19211035070-1304.1 201
Chloroethane 46 10/02/2020 1921925070-1303.8 201
Chloroform 48 10/02/2020 1921965070-1304.8 201
Chloromethane (Methyl chloride)38 10/02/2020 1921765060-1407.5 201
Cyclohexane 48 10/02/2020 1921965070-1309.2 201
1,2-Dibromo-3-chloropropane (DBCP)52 10/02/2020 19211055070-1303.6 201
Dibromochloromethane 51 10/02/2020 19211025070-1301.6 201
1,2-Dibromoethane (EDB)51 10/02/2020 19211035070-1302.2 201
1,2-Dichlorobenzene 52 10/02/2020 19211035070-1300.38 201
1,3-Dichlorobenzene 53 10/02/2020 19211065070-1303.5 201
1,4-Dichlorobenzene 52 10/02/2020 19211055070-1302.5 201
Dichlorodifluoromethane 33 10/02/2020 1921675060-1409.0 201
1,1-Dichloroethane 50 10/02/2020 19211005070-1305.1 201
1,2-Dichloroethane 49 10/02/2020 1921975070-1301.1 201
1,1-Dichloroethene 51 10/02/2020 19211015070-1307.7 201
cis-1,2-Dichloroethene 49 10/02/2020 1921975070-1304.6 201
trans-1,2-Dichloroethene 50 10/02/2020 19211005070-1306.3 201
1,2-Dichloropropane 51 10/02/2020 19211025070-1301.9 201
cis-1,3-Dichloropropene 51 10/02/2020 19211025070-1302.9 201
trans-1,3-Dichloropropene 52 10/02/2020 19211055070-1302.6 201
Ethylbenzene 53 10/02/2020 19211065070-1305.0 201
2-Hexanone 110 10/02/2020 192110910070-1303.9 201
Isopropylbenzene 53 10/02/2020 19211065070-1309.4 201
Methyl acetate 55 10/02/2020 19211095070-1302.3 201
Methyl tertiary butyl ether (MTBE)48 10/02/2020 1921955070-1302.6 201
4-Methyl-2-pentanone 100 10/02/2020 192110310070-1303.0 201
Methylcyclohexane 53 10/02/2020 19211055070-1307.5 201
Methylene chloride 45 10/02/2020 1921905070-1304.3 201
Styrene 53 10/02/2020 19211065070-1303.9 201
1,1,2,2-Tetrachloroethane 51 10/02/2020 19211035070-1300.088 201
Tetrachloroethene 54 10/02/2020 19211075070-1308.2 201
Toluene 52 10/02/2020 19211045070-1304.9 201
1,1,2-Trichloro-1,2,2-Trifluoroethane 51 10/02/2020 19211035070-1307.9 201
1,2,4-Trichlorobenzene 61 10/02/2020 19211215070-1302.7 201
1,1,1-Trichloroethane 47 10/02/2020 1921945070-1306.7 201
1,1,2-Trichloroethane 50 10/02/2020 19211015070-1302.3 201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 28 of 60
Volatile Organic Compounds by GC/MS - LCSD
Batch:Prep Method:
Sample ID:VQ68713-003
68713 5035
Analytical Method:8260D
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/kg)(ug/kg)
Trichloroethene 52 10/02/2020 19211045070-1305.0 201
Trichlorofluoromethane 43 10/02/2020 1921875070-13012 201
Vinyl chloride 43 10/02/2020 1921865070-1307.9 201
Xylenes (total)110 10/02/2020 192110610070-1305.0 201
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 105 47-138
1,2-Dichloroethane-d4 96 53-142
Toluene-d8 105 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 29 of 60
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:VQ69252-001
69252 SM 6200B-2011
Analytical Method:SM 6200B-2011
Matrix:Aqueous
Parameter Result Q LOQ Units Analysis DateDil
Benzene ND 10/08/2020 11060.50 ug/L1
Bromobenzene ND 10/08/2020 11060.50 ug/L1
Bromochloromethane ND 10/08/2020 11060.50 ug/L1
Bromodichloromethane ND 10/08/2020 11060.50 ug/L1
Bromoform ND 10/08/2020 11060.50 ug/L1
Bromomethane (Methyl bromide)ND 10/08/2020 11060.50 ug/L1
n-Butylbenzene ND 10/08/2020 11060.50 ug/L1
sec-Butylbenzene ND 10/08/2020 11060.50 ug/L1
tert-Butylbenzene ND 10/08/2020 11060.50 ug/L1
Carbon tetrachloride ND 10/08/2020 11060.50 ug/L1
Chlorobenzene ND 10/08/2020 11060.50 ug/L1
Chloroethane ND 10/08/2020 11060.50 ug/L1
Chloroform ND 10/08/2020 11060.50 ug/L1
Chloromethane (Methyl chloride)ND 10/08/2020 11060.50 ug/L1
2-Chlorotoluene ND 10/08/2020 11060.50 ug/L1
4-Chlorotoluene ND 10/08/2020 11060.50 ug/L1
Dibromochloromethane ND 10/08/2020 11060.50 ug/L1
1,2-Dibromoethane (EDB)ND 10/08/2020 11060.50 ug/L1
Dibromomethane (Methylene bromide)ND 10/08/2020 11060.50 ug/L1
1,2-Dichlorobenzene ND 10/08/2020 11060.50 ug/L1
1,3-Dichlorobenzene ND 10/08/2020 11060.50 ug/L1
1,4-Dichlorobenzene ND 10/08/2020 11060.50 ug/L1
Dichlorodifluoromethane ND 10/08/2020 11060.50 ug/L1
1,1-Dichloroethane ND 10/08/2020 11060.50 ug/L1
1,2-Dichloroethane ND 10/08/2020 11060.50 ug/L1
1,1-Dichloroethene ND 10/08/2020 11060.50 ug/L1
cis-1,2-Dichloroethene ND 10/08/2020 11060.50 ug/L1
trans-1,2-Dichloroethene ND 10/08/2020 11060.50 ug/L1
1,2-Dichloropropane ND 10/08/2020 11060.50 ug/L1
1,3-Dichloropropane ND 10/08/2020 11060.50 ug/L1
2,2-Dichloropropane ND 10/08/2020 11060.50 ug/L1
1,1-Dichloropropene ND 10/08/2020 11060.50 ug/L1
cis-1,3-Dichloropropene ND 10/08/2020 11060.50 ug/L1
trans-1,3-Dichloropropene ND 10/08/2020 11060.50 ug/L1
Diisopropyl ether (IPE)ND 10/08/2020 11060.50 ug/L1
Ethylbenzene ND 10/08/2020 11060.50 ug/L1
Hexachlorobutadiene ND 10/08/2020 11060.50 ug/L1
Isopropylbenzene (Cumene)ND 10/08/2020 11060.50 ug/L1
p-Isopropyltoluene (p-Cymene)ND 10/08/2020 11060.50 ug/L1
Methyl tertiary butyl ether (MTBE)ND 10/08/2020 11060.50 ug/L1
Methylene chloride ND 10/08/2020 11060.50 ug/L1
Naphthalene ND 10/08/2020 11060.50 ug/L1
n-Propylbenzene ND 10/08/2020 11060.50 ug/L1
Styrene ND 10/08/2020 11060.50 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 30 of 60
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:VQ69252-001
69252 SM 6200B-2011
Analytical Method:SM 6200B-2011
Matrix:Aqueous
Parameter Result Q LOQ Units Analysis DateDil
1,1,1,2-Tetrachloroethane ND 10/08/2020 11060.50 ug/L1
1,1,2,2-Tetrachloroethane ND 10/08/2020 11060.50 ug/L1
Tetrachloroethene ND 10/08/2020 11060.50 ug/L1
Toluene ND 10/08/2020 11060.50 ug/L1
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 10/08/2020 11060.50 ug/L1
1,2,3-Trichlorobenzene ND 10/08/2020 11060.50 ug/L1
1,2,4-Trichlorobenzene ND 10/08/2020 11060.50 ug/L1
1,1,1-Trichloroethane ND 10/08/2020 11060.50 ug/L1
1,1,2-Trichloroethane ND 10/08/2020 11060.50 ug/L1
Trichloroethene ND 10/08/2020 11060.50 ug/L1
Trichlorofluoromethane ND 10/08/2020 11060.50 ug/L1
1,2,3-Trichloropropane ND 10/08/2020 11060.50 ug/L1
1,3,5-Trimethylbenzene (Mesitylene)ND 10/08/2020 11060.50 ug/L1
1,2,4-Trimethylbenzene ND 10/08/2020 11060.50 ug/L1
Vinyl chloride ND 10/08/2020 11060.50 ug/L1
m+p - Xylenes ND 10/08/2020 11060.50 ug/L1
o - Xylenes ND 10/08/2020 11060.50 ug/L1
Surrogate Q % Rec Acceptance
Limit
1,2-Dichloroethane-d4 112 70-130
Bromofluorobenzene 96 70-130
Toluene-d8 104 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 31 of 60
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:VQ69252-002
69252 SM 6200B-2011
Analytical Method:SM 6200B-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Benzene 55 10/08/2020 09401095070-1301
Bromobenzene 51 10/08/2020 09401025070-1301
Bromochloromethane 56 10/08/2020 09401125070-1301
Bromodichloromethane 54 10/08/2020 09401095070-1301
Bromoform 46 10/08/2020 0940925070-1301
Bromomethane (Methyl bromide)52 10/08/2020 09401045060-1401
n-Butylbenzene 56 10/08/2020 09401115070-1301
sec-Butylbenzene 58 10/08/2020 09401165070-1301
tert-Butylbenzene 57 10/08/2020 09401145070-1301
Carbon tetrachloride 53 10/08/2020 09401075070-1301
Chlorobenzene 52 10/08/2020 09401045070-1301
Chloroethane 54 10/08/2020 09401085042-1631
Chloroform 55 10/08/2020 09401115070-1301
Chloromethane (Methyl chloride)50 10/08/2020 09401005020-1581
2-Chlorotoluene 53 10/08/2020 09401075070-1301
4-Chlorotoluene 53 10/08/2020 09401065070-1301
Dibromochloromethane 55 10/08/2020 09401105070-1301
1,2-Dibromoethane (EDB)53 10/08/2020 09401055070-1301
Dibromomethane (Methylene bromide)52 10/08/2020 09401055070-1301
1,2-Dichlorobenzene 52 10/08/2020 09401035070-1301
1,3-Dichlorobenzene 52 10/08/2020 09401045070-1301
1,4-Dichlorobenzene 49 10/08/2020 0940995070-1301
Dichlorodifluoromethane 50 10/08/2020 0940995060-1401
1,1-Dichloroethane 57 10/08/2020 09401145070-1301
1,2-Dichloroethane 52 10/08/2020 09401035070-1301
1,1-Dichloroethene 60 10/08/2020 09401205070-1301
cis-1,2-Dichloroethene 56 10/08/2020 09401135070-1301
trans-1,2-Dichloroethene 58 10/08/2020 09401175070-1301
1,2-Dichloropropane 53 10/08/2020 09401055070-1301
1,3-Dichloropropane 51 10/08/2020 09401035070-1301
2,2-Dichloropropane 56 10/08/2020 09401125070-1301
1,1-Dichloropropene 56 10/08/2020 09401135070-1301
cis-1,3-Dichloropropene 55 10/08/2020 09401115070-1301
trans-1,3-Dichloropropene 55 10/08/2020 09401105070-1301
Diisopropyl ether (IPE)57 10/08/2020 09401145070-1301
Ethylbenzene 55 10/08/2020 09401095070-1301
Hexachlorobutadiene 58 10/08/2020 09401165070-1301
Isopropylbenzene (Cumene)58 10/08/2020 09401155070-1301
p-Isopropyltoluene (p-Cymene)55 10/08/2020 09401105070-1301
Methyl tertiary butyl ether (MTBE)56 10/08/2020 09401125070-1301
Methylene chloride 54 10/08/2020 09401095070-1301
Naphthalene 59 10/08/2020 09401185050-1401
n-Propylbenzene 56 10/08/2020 09401135070-1301
Styrene 56 10/08/2020 09401125070-1301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 32 of 60
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:VQ69252-002
69252 SM 6200B-2011
Analytical Method:SM 6200B-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
1,1,1,2-Tetrachloroethane 56 10/08/2020 09401115070-1301
1,1,2,2-Tetrachloroethane 51 10/08/2020 09401035070-1301
Tetrachloroethene 55 10/08/2020 09401095070-1301
Toluene 54 10/08/2020 09401095070-1301
1,1,2-Trichloro-1,2,2-Trifluoroethane 56 10/08/2020 09401135070-1301
1,2,3-Trichlorobenzene 54 10/08/2020 09401095070-1301
1,2,4-Trichlorobenzene 56 10/08/2020 09401125070-1301
1,1,1-Trichloroethane 58 10/08/2020 09401155070-1301
1,1,2-Trichloroethane 52 10/08/2020 09401035070-1301
Trichloroethene 54 10/08/2020 09401085070-1301
Trichlorofluoromethane 52 10/08/2020 09401045060-1401
1,2,3-Trichloropropane 51 10/08/2020 09401025070-1301
1,3,5-Trimethylbenzene (Mesitylene)58 10/08/2020 09401165070-1301
1,2,4-Trimethylbenzene 57 10/08/2020 09401155070-1301
Vinyl chloride 51 10/08/2020 09401015060-1401
m+p - Xylenes 55 10/08/2020 09401105070-1301
o - Xylenes 56 10/08/2020 09401125070-1301
Surrogate Q % Rec Acceptance
Limit
1,2-Dichloroethane-d4 95 70-130
Bromofluorobenzene 90 70-130
Toluene-d8 95 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 33 of 60
Volatile Organic Compounds by GC/MS - MS
Batch:Prep Method:
Sample ID:VJ01071-003MS
69252 SM 6200B-2011
Analytical Method:SM 6200B-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(ug/L)(ug/L)(ug/L)
Benzene 5300 10/08/2020 1959107250070-130260050
Bromobenzene 2600 10/08/2020 1959106250070-130ND50
Bromochloromethane 2700 10/08/2020 1959109250070-130ND50
Bromodichloromethane 2800 10/08/2020 1959110250070-130ND50
Bromoform 2200 10/08/2020 195987250070-130ND50
Bromomethane (Methyl bromide)2700 10/08/2020 1959110250060-140ND50
n-Butylbenzene 2900 10/08/2020 1959113250070-1304050
sec-Butylbenzene 2900 10/08/2020 1959117250070-130ND50
tert-Butylbenzene 2900 10/08/2020 1959115250070-130ND50
Carbon tetrachloride 2700 10/08/2020 1959107250070-130ND50
Chlorobenzene 2600 10/08/2020 1959106250070-130ND50
Chloroethane 2900 10/08/2020 1959117250042-163ND50
Chloroform 2800 10/08/2020 1959111250070-130ND50
Chloromethane (Methyl chloride)2800 10/08/2020 1959113250020-158ND50
2-Chlorotoluene 2700 10/08/2020 1959109250070-130ND50
4-Chlorotoluene 2800 10/08/2020 1959111250070-130ND50
Dibromochloromethane 2700 10/08/2020 1959107250070-130ND50
1,2-Dibromoethane (EDB)2700 10/08/2020 1959108250070-130ND50
Dibromomethane (Methylene bromide)2700 10/08/2020 1959107250070-130ND50
1,2-Dichlorobenzene 2600 10/08/2020 1959105250070-130ND50
1,3-Dichlorobenzene 2700 10/08/2020 1959106250070-130ND50
1,4-Dichlorobenzene 2500 10/08/2020 1959100250070-130ND50
Dichlorodifluoromethane 2700 10/08/2020 1959108250060-140ND50
1,1-Dichloroethane 2800 10/08/2020 1959113250070-130ND50
1,2-Dichloroethane 2600 10/08/2020 1959106250070-130ND50
1,1-Dichloroethene 3000 10/08/2020 1959121250070-130ND50
cis-1,2-Dichloroethene 2700 10/08/2020 1959110250070-130ND50
trans-1,2-Dichloroethene 2800 10/08/2020 1959112250070-130ND50
1,2-Dichloropropane 2800 10/08/2020 1959112250070-130ND50
1,3-Dichloropropane 2700 10/08/2020 1959107250070-130ND50
2,2-Dichloropropane 2700 10/08/2020 1959108250070-130ND50
1,1-Dichloropropene 2800 10/08/2020 1959114250070-130ND50
cis-1,3-Dichloropropene 2700 10/08/2020 1959108250070-130ND50
trans-1,3-Dichloropropene 2600 10/08/2020 1959106250070-130ND50
Diisopropyl ether (IPE)2900 10/08/2020 1959116250070-130ND50
Ethylbenzene 4400 10/08/2020 1959112250070-130160050
Hexachlorobutadiene 2800 10/08/2020 1959111250070-130ND50
Isopropylbenzene (Cumene)3000 10/08/2020 1959115250070-13011050
p-Isopropyltoluene (p-Cymene)2800 10/08/2020 1959111250070-130ND50
Methyl tertiary butyl ether (MTBE)2800 10/08/2020 1959106250070-13012050
Methylene chloride 2700 10/08/2020 1959107250070-130ND50
Naphthalene 3600 10/08/2020 1959120250050-14060050
n-Propylbenzene 3300 10/08/2020 1959117250070-13033050
Styrene 2900 10/08/2020 1959115250070-130ND50
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 34 of 60
Volatile Organic Compounds by GC/MS - MS
Batch:Prep Method:
Sample ID:VJ01071-003MS
69252 SM 6200B-2011
Analytical Method:SM 6200B-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(ug/L)(ug/L)(ug/L)
1,1,1,2-Tetrachloroethane 2700 10/08/2020 1959109250070-130ND50
1,1,2,2-Tetrachloroethane 2800 10/08/2020 1959111250070-130ND50
Tetrachloroethene 2700 10/08/2020 1959109250070-130ND50
Toluene 2800 10/08/2020 1959112250070-1304750
1,1,2-Trichloro-1,2,2-Trifluoroethane 2900 10/08/2020 1959115250070-130ND50
1,2,3-Trichlorobenzene 2600 10/08/2020 1959104250070-130ND50
1,2,4-Trichlorobenzene 2700 10/08/2020 1959107250070-130ND50
1,1,1-Trichloroethane 2900 10/08/2020 1959117250070-130ND50
1,1,2-Trichloroethane 2700 10/08/2020 1959108250070-130ND50
Trichloroethene 2700 10/08/2020 1959107250070-130ND50
Trichlorofluoromethane 2700 10/08/2020 1959109250060-140ND50
1,2,3-Trichloropropane 2700 10/08/2020 1959107250070-130ND50
1,3,5-Trimethylbenzene (Mesitylene)2900 10/08/2020 1959117250070-1302850
1,2,4-Trimethylbenzene 3000 10/08/2020 1959117250070-13010050
Vinyl chloride 2900 10/08/2020 1959115250060-140ND50
m+p - Xylenes 3000 10/08/2020 1959113250070-13021050
o - Xylenes 2800 10/08/2020 1959112250070-130ND50
Surrogate Q % Rec Acceptance
Limit
1,2-Dichloroethane-d4 96 70-130
Bromofluorobenzene 92 70-130
Toluene-d8 98 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 35 of 60
Volatile Organic Compounds by GC/MS - MSD
Batch:Prep Method:
Sample ID:VJ01071-003MD
69252 SM 6200B-2011
Analytical Method:SM 6200B-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(ug/L)(ug/L)(ug/L)
Benzene 5300 10/08/2020 2024109250070-1301.3 20260050
Bromobenzene 2600 10/08/2020 2024103250070-1302.9 20ND50
Bromochloromethane 2700 10/08/2020 2024109250070-1300.61 20ND50
Bromodichloromethane 2800 10/08/2020 2024111250070-1300.80 20ND50
Bromoform 2200 10/08/2020 202489250070-1302.2 20ND50
Bromomethane (Methyl bromide)2800 10/08/2020 2024111250060-1401.3 20ND50
n-Butylbenzene 2800 10/08/2020 2024109250070-1303.4 204050
sec-Butylbenzene 2800 10/08/2020 2024114250070-1302.6 20ND50
tert-Butylbenzene 2800 10/08/2020 2024112250070-1302.4 20ND50
Carbon tetrachloride 2700 10/08/2020 2024109250070-1302.0 20ND50
Chlorobenzene 2700 10/08/2020 2024107250070-1300.74 20ND50
Chloroethane 3000 10/08/2020 2024118250042-1631.1 20ND50
Chloroform 2700 10/08/2020 2024110250070-1301.2 20ND50
Chloromethane (Methyl chloride)2800 10/08/2020 2024111250020-1581.5 20ND50
2-Chlorotoluene 2700 10/08/2020 2024107250070-1302.3 20ND50
4-Chlorotoluene 2700 10/08/2020 2024109250070-1301.7 20ND50
Dibromochloromethane 2700 10/08/2020 2024108250070-1300.72 20ND50
1,2-Dibromoethane (EDB)2700 10/08/2020 2024107250070-1300.89 20ND50
Dibromomethane (Methylene bromide)2600 10/08/2020 2024106250070-1300.86 20ND50
1,2-Dichlorobenzene 2600 10/08/2020 2024103250070-1302.4 20ND50
1,3-Dichlorobenzene 2600 10/08/2020 2024104250070-1301.8 20ND50
1,4-Dichlorobenzene 2500 10/08/2020 202499250070-1301.9 20ND50
Dichlorodifluoromethane 2700 10/08/2020 2024107250060-1401.2 20ND50
1,1-Dichloroethane 2800 10/08/2020 2024114250070-1300.33 20ND50
1,2-Dichloroethane 2600 10/08/2020 2024105250070-1301.1 20ND50
1,1-Dichloroethene 3100 10/08/2020 2024123250070-1301.4 20ND50
cis-1,2-Dichloroethene 2800 10/08/2020 2024110250070-1300.24 20ND50
trans-1,2-Dichloroethene 2900 10/08/2020 2024115250070-1302.2 20ND50
1,2-Dichloropropane 2800 10/08/2020 2024112250070-1300.59 20ND50
1,3-Dichloropropane 2600 10/08/2020 2024106250070-1301.2 20ND50
2,2-Dichloropropane 2400 10/08/2020 202495250070-13013 20ND50
1,1-Dichloropropene 2900 10/08/2020 2024114250070-1300.63 20ND50
cis-1,3-Dichloropropene 2700 10/08/2020 2024109250070-1301.7 20ND50
trans-1,3-Dichloropropene 2700 10/08/2020 2024106250070-1300.26 20ND50
Diisopropyl ether (IPE)2800 10/08/2020 2024114250070-1302.1 20ND50
Ethylbenzene 4500 10/08/2020 2024114250070-1301.4 20160050
Hexachlorobutadiene 2700 10/08/2020 2024108250070-1302.5 20ND50
Isopropylbenzene (Cumene)3000 10/08/2020 2024116250070-1300.47 2011050
p-Isopropyltoluene (p-Cymene)2700 10/08/2020 2024108250070-1302.9 20ND50
Methyl tertiary butyl ether (MTBE)2700 10/08/2020 2024104250070-1301.2 2012050
Methylene chloride 2700 10/08/2020 2024106250070-1301.0 20ND50
Naphthalene 3500 10/08/2020 2024117250050-1402.2 2060050
n-Propylbenzene 3200 10/08/2020 2024115250070-1301.6 2033050
Styrene 2900 10/08/2020 2024116250070-1300.49 20ND50
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 36 of 60
Volatile Organic Compounds by GC/MS - MSD
Batch:Prep Method:
Sample ID:VJ01071-003MD
69252 SM 6200B-2011
Analytical Method:SM 6200B-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(ug/L)(ug/L)(ug/L)
1,1,1,2-Tetrachloroethane 2700 10/08/2020 2024110250070-1300.89 20ND50
1,1,2,2-Tetrachloroethane 2600 10/08/2020 2024106250070-1304.6 20ND50
Tetrachloroethene 2800 10/08/2020 2024112250070-1302.8 20ND50
Toluene 2900 10/08/2020 2024113250070-1301.1 204750
1,1,2-Trichloro-1,2,2-Trifluoroethane 2900 10/08/2020 2024115250070-1300.60 20ND50
1,2,3-Trichlorobenzene 2600 10/08/2020 2024105250070-1300.61 20ND50
1,2,4-Trichlorobenzene 2600 10/08/2020 2024106250070-1301.3 20ND50
1,1,1-Trichloroethane 2900 10/08/2020 2024116250070-1300.89 20ND50
1,1,2-Trichloroethane 2700 10/08/2020 2024107250070-1301.6 20ND50
Trichloroethene 2700 10/08/2020 2024109250070-1301.7 20ND50
Trichlorofluoromethane 2800 10/08/2020 2024112250060-1401.9 20ND50
1,2,3-Trichloropropane 2600 10/08/2020 2024104250070-1303.2 20ND50
1,3,5-Trimethylbenzene (Mesitylene)2900 10/08/2020 2024114250070-1302.7 202850
1,2,4-Trimethylbenzene 2900 10/08/2020 2024114250070-1302.9 2010050
Vinyl chloride 2800 10/08/2020 2024113250060-1402.3 20ND50
m+p - Xylenes 3000 10/08/2020 2024113250070-1300.46 2021050
o - Xylenes 2800 10/08/2020 2024113250070-1301.2 20ND50
Surrogate Q % Rec Acceptance
Limit
1,2-Dichloroethane-d4 96 70-130
Bromofluorobenzene 92 70-130
Toluene-d8 99 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 37 of 60
Semivolatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Prep Date:
Sample ID:VQ68844-001
68844 3546
10/05/2020 1530Analytical Method:8270E
Matrix:Solid
Parameter Result Q LOQ Units Analysis DateDil
Acenaphthene ND 10/15/2020 17192.7 ug/kg1
Acenaphthylene ND 10/15/2020 17192.7 ug/kg1
Acetophenone ND 10/15/2020 171913ug/kg1
Anthracene ND 10/15/2020 17192.7 ug/kg1
Atrazine ND 10/15/2020 171913ug/kg1
Benzaldehyde ND 10/15/2020 171913ug/kg1
Benzo(a)anthracene ND 10/15/2020 17192.7 ug/kg1
Benzo(a)pyrene ND 10/15/2020 17192.7 ug/kg1
Benzo(b)fluoranthene ND 10/15/2020 17192.7 ug/kg1
Benzo(g,h,i)perylene ND 10/15/2020 17192.7 ug/kg1
Benzo(k)fluoranthene ND 10/15/2020 17192.7 ug/kg1
1,1'-Biphenyl ND 10/15/2020 171913ug/kg1
4-Bromophenyl phenyl ether ND 10/15/2020 171913ug/kg1
Butyl benzyl phthalate ND 10/15/2020 171913ug/kg1
Caprolactam ND 10/15/2020 171913ug/kg1
Carbazole ND 10/15/2020 171913ug/kg1
bis (2-Chloro-1-methylethyl) ether ND 10/15/2020 171913ug/kg1
4-Chloro-3-methyl phenol ND 10/15/2020 171913ug/kg1
4-Chloroaniline ND 10/15/2020 171913ug/kg1
bis(2-Chloroethoxy)methane ND 10/15/2020 171913ug/kg1
bis(2-Chloroethyl)ether ND 10/15/2020 171913ug/kg1
2-Chloronaphthalene ND 10/15/2020 171913ug/kg1
2-Chlorophenol ND 10/15/2020 171913ug/kg1
4-Chlorophenyl phenyl ether ND 10/15/2020 171913ug/kg1
Chrysene ND 10/15/2020 17192.7 ug/kg1
Dibenzo(a,h)anthracene ND 10/15/2020 17192.7 ug/kg1
Dibenzofuran ND 10/15/2020 171913ug/kg1
3,3'-Dichlorobenzidine ND 10/15/2020 171913ug/kg1
2,4-Dichlorophenol ND 10/15/2020 171913ug/kg1
Diethylphthalate ND 10/15/2020 171913ug/kg1
Dimethyl phthalate ND 10/15/2020 171913ug/kg1
2,4-Dimethylphenol ND 10/15/2020 171913ug/kg1
Di-n-butyl phthalate ND 10/15/2020 171913ug/kg1
4,6-Dinitro-2-methylphenol ND 10/15/2020 171967ug/kg1
2,4-Dinitrophenol ND 10/15/2020 171967ug/kg1
2,4-Dinitrotoluene ND 10/15/2020 171927ug/kg1
2,6-Dinitrotoluene ND 10/15/2020 171927ug/kg1
Di-n-octylphthalate ND 10/15/2020 171913ug/kg1
bis(2-Ethylhexyl)phthalate ND 10/15/2020 171967ug/kg1
Fluoranthene ND 10/15/2020 17192.7 ug/kg1
Fluorene ND 10/15/2020 17192.7 ug/kg1
Hexachlorobenzene ND 10/15/2020 171913ug/kg1
Hexachlorobutadiene ND 10/15/2020 171913ug/kg1
Hexachlorocyclopentadiene ND 10/15/2020 171967ug/kg1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 38 of 60
Semivolatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Prep Date:
Sample ID:VQ68844-001
68844 3546
10/05/2020 1530Analytical Method:8270E
Matrix:Solid
Parameter Result Q LOQ Units Analysis DateDil
Hexachloroethane ND 10/15/2020 171913ug/kg1
Indeno(1,2,3-c,d)pyrene ND 10/15/2020 17192.7 ug/kg1
Isophorone ND 10/15/2020 171913ug/kg1
2-Methylnaphthalene ND 10/15/2020 17192.7 ug/kg1
2-Methylphenol ND 10/15/2020 171913ug/kg1
3+4-Methylphenol ND 10/15/2020 171927ug/kg1
Naphthalene ND 10/15/2020 17192.7 ug/kg1
2-Nitroaniline ND 10/15/2020 171927ug/kg1
3-Nitroaniline ND 10/15/2020 171927ug/kg1
4-Nitroaniline ND 10/15/2020 171927ug/kg1
Nitrobenzene ND 10/15/2020 171913ug/kg1
2-Nitrophenol ND 10/15/2020 171927ug/kg1
4-Nitrophenol ND 10/15/2020 171967ug/kg1
N-Nitrosodi-n-propylamine ND 10/15/2020 171913ug/kg1
N-Nitrosodiphenylamine (Diphenylamine)ND 10/15/2020 171913ug/kg1
Pentachlorophenol ND 10/15/2020 171967ug/kg1
Phenanthrene ND 10/15/2020 17192.7 ug/kg1
Phenol ND 10/15/2020 171913ug/kg1
Pyrene ND 10/15/2020 17192.7 ug/kg1
2,4,5-Trichlorophenol ND 10/15/2020 171913ug/kg1
2,4,6-Trichlorophenol ND 10/15/2020 171913ug/kg1
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl 74 33-102
2-Fluorophenol 76 35-115
Nitrobenzene-d5 89 22-109
Phenol-d5 87 33-122
Terphenyl-d14 74 41-120
2,4,6-Tribromophenol 74 30-117
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 39 of 60
Semivolatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Prep Date:
Sample ID:VQ68844-002
68844 3546
10/05/2020 1530Analytical Method:8270E
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Acenaphthene 120 10/15/2020 13108913012-1111
Acenaphthylene 130 10/15/2020 13109513044-1221
Acetophenone 120 10/15/2020 13109313048-1111
Anthracene 120 10/15/2020 13109213016-1221
Atrazine 130 10/15/2020 131010013048-1161
Benzaldehyde 100 10/15/2020 13107713010-1101
Benzo(a)anthracene 120 10/15/2020 13108713040-1211
Benzo(a)pyrene 130 10/15/2020 13109813036-1141
Benzo(b)fluoranthene 130 10/15/2020 13109813038-1231
Benzo(g,h,i)perylene 75 10/15/2020 13105713043-1201
Benzo(k)fluoranthene 130 10/15/2020 13109813040-1261
1,1'-Biphenyl 120 10/15/2020 13108813049-1101
4-Bromophenyl phenyl ether 120 10/15/2020 13109113046-1181
Butyl benzyl phthalate 120 10/15/2020 13109313046-1281
Caprolactam 140 10/15/2020 131010613043-1211
Carbazole 130 10/15/2020 13109713047-1281
bis (2-Chloro-1-methylethyl) ether 130 10/15/2020 131010113031-1021
4-Chloro-3-methyl phenol 130 10/15/2020 13109513049-1181
4-Chloroaniline 56 10/15/2020 13104213017-1061
bis(2-Chloroethoxy)methane 110 10/15/2020 13108613039-1081
bis(2-Chloroethyl)ether 130 10/15/2020 13109513032-1051
2-Chloronaphthalene 120 10/15/2020 13108813031-1271
2-Chlorophenol 110 10/15/2020 13108613037-1061
4-Chlorophenyl phenyl ether 130 10/15/2020 13109613047-1161
Chrysene 120 10/15/2020 13109013041-1241
Dibenzo(a,h)anthracene 140 10/15/2020 131010513038-1251
Dibenzofuran 120 10/15/2020 13108913045-1121
3,3'-Dichlorobenzidine 99 10/15/2020 13107513010-1191
2,4-Dichlorophenol 120 10/15/2020 13109013041-1131
Diethylphthalate 120 10/15/2020 13109313049-1231
Dimethyl phthalate 120 10/15/2020 13109213048-1201
2,4-Dimethylphenol 140 10/15/2020 131010713033-1231
Di-n-butyl phthalate 130 10/15/2020 13109613051-1291
4,6-Dinitro-2-methylphenol 120 10/15/2020 13108813040-1301
2,4-Dinitrophenol 200 10/15/2020 13107627032-1151
2,4-Dinitrotoluene 140 10/15/2020 131010613048-1241
2,6-Dinitrotoluene 140 10/15/2020 131010313047-1251
Di-n-octylphthalate 140 10/15/2020 131010413049-1421
bis(2-Ethylhexyl)phthalate 140 10/15/2020 131010413045-1281
Fluoranthene 120 10/15/2020 13109213026-1331
Fluorene 120 10/15/2020 13108813019-1081
Hexachlorobenzene 120 10/15/2020 13109313044-1221
Hexachlorobutadiene 110 10/15/2020 13108513033-1031
Hexachlorocyclopentadiene 590 10/15/2020 13108967018-1211
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 40 of 60
Semivolatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Prep Date:
Sample ID:VQ68844-002
68844 3546
10/05/2020 1530Analytical Method:8270E
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Hexachloroethane 110 10/15/2020 13108313030-961
Indeno(1,2,3-c,d)pyrene 130 10/15/2020 131010113042-1231
Isophorone 140 10/15/2020 131010713041-1131
2-Methylnaphthalene 110 10/15/2020 13108313010-1071
2-Methylphenol 120 10/15/2020 13109013032-1071
3+4-Methylphenol 130 10/15/2020 13109913039-1081
Naphthalene 110 10/15/2020 13108113010-1121
2-Nitroaniline 150 10/15/2020 131011613045-1231
3-Nitroaniline 82 10/15/2020 13106213024-1271
4-Nitroaniline 120 10/15/2020 13108913048-1271
Nitrobenzene 130 10/15/2020 13109513033-1141
2-Nitrophenol 120 10/15/2020 13109313035-1081
4-Nitrophenol 230 10/15/2020 13108827018-1541
N-Nitrosodi-n-propylamine 140 10/15/2020 131010213032-1151
N-Nitrosodiphenylamine (Diphenylamine)130 10/15/2020 131010113053-1501
Pentachlorophenol 140 10/15/2020 13105127027-1381
Phenanthrene 110 10/15/2020 13108513016-1231
Phenol 130 10/15/2020 13109513036-1081
Pyrene 130 10/15/2020 13109513034-1211
2,4,5-Trichlorophenol 140 10/15/2020 131010713046-1221
2,4,6-Trichlorophenol 120 10/15/2020 13108713038-1151
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl 84 33-102
2-Fluorophenol 87 35-115
Nitrobenzene-d5 92 22-109
Phenol-d5 98 33-122
Terphenyl-d14 91 41-120
2,4,6-Tribromophenol 83 30-117
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 41 of 60
Semivolatile Organic Compounds by GC/MS - MS
Batch:Prep Method:
Prep Date:
Sample ID:VJ01071-001MS
68844 3546
10/05/2020 1530Analytical Method:8270E
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)(ug/kg)
Acenaphthene ND 10/15/2020 2128N0.00130 12-111ND100
Acenaphthylene ND 10/15/2020 2128N0.00130 44-122ND100
Acetophenone ND 10/15/2020 2128N0.00130 30-130ND100
Anthracene ND 10/15/2020 2128N0.00130 16-122ND100
Atrazine ND 10/15/2020 2128N0.00130 30-130ND100
Benzaldehyde ND 10/15/2020 2128N0.00130 10-110ND100
Benzo(a)anthracene ND 10/15/2020 2128N0.00130 40-121ND100
Benzo(a)pyrene ND 10/15/2020 2128N0.00130 36-114ND100
Benzo(b)fluoranthene ND 10/15/2020 2128N0.00130 38-123ND100
Benzo(g,h,i)perylene ND 10/15/2020 2128N0.00130 43-120ND100
Benzo(k)fluoranthene ND 10/15/2020 2128N0.00130 40-126ND100
1,1'-Biphenyl ND 10/15/2020 2128N0.00130 30-130ND100
4-Bromophenyl phenyl ether ND 10/15/2020 2128N0.00130 30-130ND100
Butyl benzyl phthalate ND 10/15/2020 2128N0.00130 30-130ND100
Caprolactam ND 10/15/2020 2128N0.00130 30-130ND100
Carbazole ND 10/15/2020 2128N0.00130 30-130ND100
bis (2-Chloro-1-methylethyl) ether ND 10/15/2020 2128N0.00130 30-130ND100
4-Chloro-3-methyl phenol ND 10/15/2020 2128N0.00130 30-130ND100
4-Chloroaniline ND 10/15/2020 2128N0.00130 17-106ND100
bis(2-Chloroethoxy)methane ND 10/15/2020 2128N0.00130 30-130ND100
bis(2-Chloroethyl)ether ND 10/15/2020 2128N0.00130 30-130ND100
2-Chloronaphthalene ND 10/15/2020 2128N0.00130 30-130ND100
2-Chlorophenol ND 10/15/2020 2128N0.00130 30-130ND100
4-Chlorophenyl phenyl ether ND 10/15/2020 2128N0.00130 30-130ND100
Chrysene ND 10/15/2020 2128N0.00130 41-124ND100
Dibenzo(a,h)anthracene ND 10/15/2020 2128N0.00130 38-125ND100
Dibenzofuran ND 10/15/2020 2128N0.00130 30-130ND100
3,3'-Dichlorobenzidine ND 10/15/2020 2128N0.00130 10-119ND100
2,4-Dichlorophenol ND 10/15/2020 2128N0.00130 30-130ND100
Diethylphthalate ND 10/15/2020 2128N0.00130 30-130ND100
Dimethyl phthalate ND 10/15/2020 2128N0.00130 30-130ND100
2,4-Dimethylphenol ND 10/15/2020 2128N0.00130 30-130ND100
Di-n-butyl phthalate ND 10/15/2020 2128N0.00130 30-130ND100
4,6-Dinitro-2-methylphenol ND 10/15/2020 2128N0.00130 30-130ND100
2,4-Dinitrophenol ND 10/15/2020 2128N0.00270 30-130ND100
2,4-Dinitrotoluene ND 10/15/2020 2128N0.00130 30-130ND100
2,6-Dinitrotoluene ND 10/15/2020 2128N0.00130 30-130ND100
Di-n-octylphthalate ND 10/15/2020 2128N0.00130 30-130ND100
bis(2-Ethylhexyl)phthalate 3800 10/15/2020 2128N287013030-130ND100
Fluoranthene ND 10/15/2020 2128N0.00130 26-133ND100
Fluorene ND 10/15/2020 2128N0.00130 19-108ND100
Hexachlorobenzene 130 10/15/2020 21289413030-130ND100
Hexachlorobutadiene ND 10/15/2020 2128N0.00130 30-130ND100
Hexachlorocyclopentadiene ND 10/15/2020 2128N0.00670 30-130ND100
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 42 of 60
Semivolatile Organic Compounds by GC/MS - MS
Batch:Prep Method:
Prep Date:
Sample ID:VJ01071-001MS
68844 3546
10/05/2020 1530Analytical Method:8270E
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)(ug/kg)
Hexachloroethane ND 10/15/2020 2128N0.00130 30-130ND100
Indeno(1,2,3-c,d)pyrene ND 10/15/2020 2128N0.00130 42-123ND100
Isophorone ND 10/15/2020 2128N0.00130 30-130ND100
2-Methylnaphthalene 1200 10/15/2020 2128N17313010-107ND100
2-Methylphenol ND 10/15/2020 2128N0.00130 30-130ND100
3+4-Methylphenol ND 10/15/2020 2128N0.00130 30-130ND100
Naphthalene ND 10/15/2020 2128N0.00130 10-112ND100
2-Nitroaniline ND 10/15/2020 2128N0.00130 30-130ND100
3-Nitroaniline ND 10/15/2020 2128N0.00130 30-130ND100
4-Nitroaniline ND 10/15/2020 2128N0.00130 30-130ND100
Nitrobenzene ND 10/15/2020 2128N0.00130 30-130ND100
2-Nitrophenol ND 10/15/2020 2128N0.00130 30-130ND100
4-Nitrophenol ND 10/15/2020 2128N0.00270 30-130ND100
N-Nitrosodi-n-propylamine 6900 10/15/2020 2128N517013030-130ND100
N-Nitrosodiphenylamine (Diphenylamine)ND 10/15/2020 2128N0.00130 30-130ND100
Pentachlorophenol 17000 10/15/2020 2128N641027030-130ND100
Phenanthrene ND 10/15/2020 2128N0.00130 16-123ND100
Phenol ND 10/15/2020 2128N0.00130 30-130ND100
Pyrene ND 10/15/2020 2128N0.00130 34-121ND100
2,4,5-Trichlorophenol ND 10/15/2020 2128N0.00130 30-130ND100
2,4,6-Trichlorophenol ND 10/15/2020 2128N0.00130 30-130ND100
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl N 108 33-102
2-Fluorophenol 40 35-115
Nitrobenzene-d5 N 197 22-109
Phenol-d5 84 33-122
Terphenyl-d14 N 246 41-120
2,4,6-Tribromophenol 31 30-117
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 43 of 60
Semivolatile Organic Compounds by GC/MS - MSD
Batch:Prep Method:
Prep Date:
Sample ID:VJ01071-001MD
68844 3546
10/05/2020 1530Analytical Method:8270E
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)(ug/kg)
Acenaphthene ND 10/15/2020 2152N0.00140 12-1110.00 30ND100
Acenaphthylene ND 10/15/2020 2152N0.00140 44-1220.00 30ND100
Acetophenone ND 10/15/2020 2152N0.00140 30-1300.00 40ND100
Anthracene ND 10/15/2020 2152N0.00140 16-1220.00 30ND100
Atrazine ND 10/15/2020 2152N0.00140 30-1300.00 40ND100
Benzaldehyde ND 10/15/2020 2152N0.00140 10-1100.00 40ND100
Benzo(a)anthracene ND 10/15/2020 2152N0.00140 40-1210.00 30ND100
Benzo(a)pyrene ND 10/15/2020 2152N0.00140 36-1140.00 30ND100
Benzo(b)fluoranthene ND 10/15/2020 2152N0.00140 38-1230.00 30ND100
Benzo(g,h,i)perylene ND 10/15/2020 2152N0.00140 43-1200.00 30ND100
Benzo(k)fluoranthene ND 10/15/2020 2152N0.00140 40-1260.00 30ND100
1,1'-Biphenyl ND 10/15/2020 2152N0.00140 30-1300.00 40ND100
4-Bromophenyl phenyl ether ND 10/15/2020 2152N0.00140 30-1300.00 40ND100
Butyl benzyl phthalate ND 10/15/2020 2152N0.00140 30-1300.00 40ND100
Caprolactam ND 10/15/2020 2152N0.00140 30-1300.00 40ND100
Carbazole ND 10/15/2020 2152N0.00140 30-1300.00 40ND100
bis (2-Chloro-1-methylethyl) ether ND 10/15/2020 2152N0.00140 30-1300.00 40ND100
4-Chloro-3-methyl phenol ND 10/15/2020 2152N0.00140 30-1300.00 40ND100
4-Chloroaniline ND 10/15/2020 2152N0.00140 17-1060.00 40ND100
bis(2-Chloroethoxy)methane ND 10/15/2020 2152N0.00140 30-1300.00 40ND100
bis(2-Chloroethyl)ether ND 10/15/2020 2152N0.00140 30-1300.00 40ND100
2-Chloronaphthalene ND 10/15/2020 2152N0.00140 30-1300.00 40ND100
2-Chlorophenol ND 10/15/2020 2152N0.00140 30-1300.00 40ND100
4-Chlorophenyl phenyl ether ND 10/15/2020 2152N0.00140 30-1300.00 40ND100
Chrysene ND 10/15/2020 2152N0.00140 41-1240.00 30ND100
Dibenzo(a,h)anthracene ND 10/15/2020 2152N0.00140 38-1250.00 30ND100
Dibenzofuran ND 10/15/2020 2152N0.00140 30-1300.00 40ND100
3,3'-Dichlorobenzidine ND 10/15/2020 2152N0.00140 10-1190.00 40ND100
2,4-Dichlorophenol ND 10/15/2020 2152N0.00140 30-1300.00 40ND100
Diethylphthalate ND 10/15/2020 2152N0.00140 30-1300.00 40ND100
Dimethyl phthalate ND 10/15/2020 2152N0.00140 30-1300.00 40ND100
2,4-Dimethylphenol ND 10/15/2020 2152N0.00140 30-1300.00 40ND100
Di-n-butyl phthalate ND 10/15/2020 2152N0.00140 30-1300.00 40ND100
4,6-Dinitro-2-methylphenol ND 10/15/2020 2152N0.00140 30-1300.00 40ND100
2,4-Dinitrophenol ND 10/15/2020 2152N0.00270 30-1300.00 40ND100
2,4-Dinitrotoluene ND 10/15/2020 2152N0.00140 30-1300.00 40ND100
2,6-Dinitrotoluene ND 10/15/2020 2152N0.00140 30-1300.00 40ND100
Di-n-octylphthalate ND 10/15/2020 2152N0.00140 30-1300.00 40ND100
bis(2-Ethylhexyl)phthalate 4200 10/15/2020 2152N304014030-1308.3 40ND100
Fluoranthene ND 10/15/2020 2152N0.00140 26-1330.00 30ND100
Fluorene ND 10/15/2020 2152N0.00140 19-1080.00 30ND100
Hexachlorobenzene ND 10/15/2020 2152N,+0.00140 30-130200 40ND100
Hexachlorobutadiene ND 10/15/2020 2152N0.00140 30-1300.00 40ND100
Hexachlorocyclopentadiene ND 10/15/2020 2152N0.00680 30-1300.00 40ND100
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 44 of 60
Semivolatile Organic Compounds by GC/MS - MSD
Batch:Prep Method:
Prep Date:
Sample ID:VJ01071-001MD
68844 3546
10/05/2020 1530Analytical Method:8270E
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)(ug/kg)
Hexachloroethane ND 10/15/2020 2152N0.00140 30-1300.00 40ND100
Indeno(1,2,3-c,d)pyrene ND 10/15/2020 2152N0.00140 42-1230.00 30ND100
Isophorone ND 10/15/2020 2152N0.00140 30-1300.00 40ND100
2-Methylnaphthalene 1300 10/15/2020 2152N21814010-1075.5 30ND100
2-Methylphenol ND 10/15/2020 2152N0.00140 30-1300.00 40ND100
3+4-Methylphenol ND 10/15/2020 2152N0.00140 30-1300.00 40ND100
Naphthalene ND 10/15/2020 2152N0.00140 10-1120.00 30ND100
2-Nitroaniline ND 10/15/2020 2152N0.00140 30-1300.00 40ND100
3-Nitroaniline ND 10/15/2020 2152N0.00140 30-1300.00 40ND100
4-Nitroaniline ND 10/15/2020 2152N0.00140 30-1300.00 40ND100
Nitrobenzene ND 10/15/2020 2152N0.00140 30-1300.00 40ND100
2-Nitrophenol ND 10/15/2020 2152N0.00140 30-1300.00 40ND100
4-Nitrophenol ND 10/15/2020 2152N0.00270 30-1300.00 40ND100
N-Nitrosodi-n-propylamine 7400 10/15/2020 2152N541014030-1307.2 40ND100
N-Nitrosodiphenylamine (Diphenylamine)ND 10/15/2020 2152N0.00140 30-1300.00 40ND100
Pentachlorophenol 16000 10/15/2020 2152N601027030-1303.9 40ND100
Phenanthrene ND 10/15/2020 2152N0.00140 16-1230.00 30ND100
Phenol ND 10/15/2020 2152N0.00140 30-1300.00 40ND100
Pyrene ND 10/15/2020 2152N0.00140 34-1210.00 30ND100
2,4,5-Trichlorophenol ND 10/15/2020 2152N0.00140 30-1300.00 40ND100
2,4,6-Trichlorophenol ND 10/15/2020 2152N0.00140 30-1300.00 40ND100
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl N 138 33-102
2-Fluorophenol 61 35-115
Nitrobenzene-d5 N 249 22-109
Phenol-d5 53 33-122
Terphenyl-d14 N 211 41-120
2,4,6-Tribromophenol 30 30-117
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 45 of 60
MA EPH (aliphatics) - MB
Batch:Prep Method:
Prep Date:
Sample ID:VQ68901-001
68901 MADEP-EPH-04
10/06/2020 0828Analytical Method:MADEP-EPH-04
Matrix:Solid
Parameter Result Q LOQ Units Analysis DateDil
C9 - C18 Aliphatics ND 10/07/2020 083710mg/kg1
C19 - C36 Aliphatics ND 10/07/2020 083710mg/kg1
Surrogate Q % Rec
Acceptance
Limit
1-Chloro-octadecane (aliphatic)86 40-140
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 46 of 60
MA EPH (aliphatics) - LCS
Batch:Prep Method:
Prep Date:
Sample ID:VQ68901-002
68901 MADEP-EPH-04
10/06/2020 0828Analytical Method:MADEP-EPH-04
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/kg)(mg/kg)
C9 - C18 Aliphatics 21 10/07/2020 0906693040-1401
C19 - C36 Aliphatics 36 10/07/2020 0906904040-1401
Surrogate Q % Rec
Acceptance
Limit
1-Chloro-octadecane (aliphatic)82 40-140
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 47 of 60
MA EPH (aliphatics) - LCSD
Batch:Prep Method:
Prep Date:
Sample ID:VQ68901-003
68901 MADEP-EPH-04
10/06/2020 0828Analytical Method:MADEP-EPH-04
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(mg/kg)(mg/kg)
C9 - C18 Aliphatics 20 10/07/2020 0936683040-1401.4 251
C19 - C36 Aliphatics 37 10/07/2020 0936924040-1401.8 251
Surrogate Q % Rec
Acceptance
Limit
1-Chloro-octadecane (aliphatic)83 40-140
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 48 of 60
MA EPH (aromatics) - MB
Batch:Prep Method:
Prep Date:
Sample ID:VQ68902-001
68902 MADEP-EPH-04
10/06/2020 0828Analytical Method:MADEP-EPH-04
Matrix:Solid
Parameter Result Q LOQ Units Analysis DateDil
C11 - C22 Aromatics ND 10/07/2020 130610mg/kg1
Surrogate Q % Rec
Acceptance
Limit
2-Bromonaphthalene (fractionation 2)88 40-140
2-Fluorobiphenyl (fractionation 1)97 40-140
o - Terphenyl (aromatic)83 40-140
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 49 of 60
MA EPH (aromatics) - LCS
Batch:Prep Method:
Prep Date:
Sample ID:VQ68902-002
68902 MADEP-EPH-04
10/06/2020 0828Analytical Method:MADEP-EPH-04
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/kg)(mg/kg)
C11 - C22 Aromatics 68 10/07/2020 1337808540-1401
Surrogate Q % Rec
Acceptance
Limit
2-Bromonaphthalene (fractionation 2)87 40-140
2-Fluorobiphenyl (fractionation 1)91 40-140
o - Terphenyl (aromatic)78 40-140
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 50 of 60
MA EPH (aromatics) - LCSD
Batch:Prep Method:
Prep Date:
Sample ID:VQ68902-003
68902 MADEP-EPH-04
10/06/2020 0828Analytical Method:MADEP-EPH-04
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(mg/kg)(mg/kg)
C11 - C22 Aromatics 73 10/07/2020 1407858540-1406.0 251
Surrogate Q % Rec
Acceptance
Limit
2-Bromonaphthalene (fractionation 2)93 40-140
2-Fluorobiphenyl (fractionation 1)99 40-140
o - Terphenyl (aromatic)81 40-140
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 51 of 60
MADEP VPH (aliphatics) - MB
Batch:Prep Method:
Sample ID:VQ69569-001
69569 VPH
Analytical Method:MADEP-VPH-18-2.1
Matrix:Solid
Parameter Result Q LOQ Units Analysis DateDil
C5 - C8 Aliphatics ND 10/12/2020 14093.8 mg/kg1
C9 - C12 Aliphatics ND 10/12/2020 14093.8 mg/kg1
Surrogate Q % Rec
Acceptance
Limit
2,5-Dibromotoluene (FID)92 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 52 of 60
MADEP VPH (aliphatics) - LCS
Batch:Prep Method:
Sample ID:VQ69569-002
69569 VPH
Analytical Method:MADEP-VPH-18-2.1
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/kg)(mg/kg)
C5 - C8 Aliphatics 6.9 10/12/2020 1313927.5 70-1301
C9 - C12 Aliphatics 8.8 10/12/2020 13131008.8 70-1301
Surrogate Q % Rec
Acceptance
Limit
2,5-Dibromotoluene (FID)94 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 53 of 60
MADEP VPH (aliphatics) - LCSD
Batch:Prep Method:
Sample ID:VQ69569-003
69569 VPH
Analytical Method:MADEP-VPH-18-2.1
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(mg/kg)(mg/kg)
C5 - C8 Aliphatics 6.6 10/12/2020 1341887.5 70-1304.1 251
C9 - C12 Aliphatics 8.8 10/12/2020 13411018.8 70-1300.17 251
Surrogate Q % Rec
Acceptance
Limit
2,5-Dibromotoluene (FID)91 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 54 of 60
MADEP VPH (aromatics) - MB
Batch:Prep Method:
Sample ID:VQ69573-001
69573 VPH
Analytical Method:MADEP-VPH-18-2.1
Matrix:Solid
Parameter Result Q LOQ Units Analysis DateDil
C9 - C10 Aromatics ND 10/12/2020 14091.3 mg/kg1
Surrogate Q % Rec
Acceptance
Limit
2,5-Dibromotoluene (PID)92 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 55 of 60
MADEP VPH (aromatics) - LCS
Batch:Prep Method:
Sample ID:VQ69573-002
69573 VPH
Analytical Method:MADEP-VPH-18-2.1
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/kg)(mg/kg)
C9 - C10 Aromatics 1.2 10/12/2020 1313961.3 70-1301
Surrogate Q % Rec
Acceptance
Limit
2,5-Dibromotoluene (PID)92 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 56 of 60
MADEP VPH (aromatics) - LCSD
Batch:Prep Method:
Sample ID:VQ69573-003
69573 VPH
Analytical Method:MADEP-VPH-18-2.1
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(mg/kg)(mg/kg)
C9 - C10 Aromatics 1.2 10/12/2020 1341961.3 70-1300.00 251
Surrogate Q % Rec
Acceptance
Limit
2,5-Dibromotoluene (PID)92 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

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Chain of Custody
and
Miscellaneous Documents
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

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PACE ANALYTICAL SERVICES, LLC

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 59 of 60
PACE ANALYTICAL SERVICES, LLC

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 60 of 60