WA-1121_13273_CA_RPTS_20220428_MRP

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]

April 28, 2022

Mr. Jared Edwards
North Carolina Department of
Environmental Quality
Washington Regional Office
943 Washington Square Mall
Washington, North Carolina 27889

Re: Ground Water Monitoring Report
March 2022
Hak’s Store
901 Washington Street
Plymouth, Washington County
North Carolina
Facility ID Number: 0-00-0000006287
Incident Numbers: 13273
GRI Project Number: 2264

Dear Mr. Edwards,

Please find enclosed the referenced report, for the above mentioned site.
If you have any questions, please contact Ethan Rogerson at 704-845-4010.

Sincerely,
Geological Resources, Inc.

Leslie Maxtone-Graham
Administrative Assistant

Enclosure

Cc: Ms. Bea Harrison; North East Oil Company, Inc., file

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
Engineering Certification: C-2727 • Geology Certification: C-127
Ground Water Monitoring Report
March 2022
Hak’s Store
901 Washington Street
Plymouth, Washington County
North Carolina
Facility ID Number: 0-00-0000006287
Incident Number: 13273
GRI Project Number: 2266

Prepared for:

North East Oil Company, Inc.
Post Office Box 1386
Ahoskie, North Carolina 27910

April 28, 2022

Ethan Rogerson, G.I.T.
Project Manager
William Regenthal, P.G.
Report Editor

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: April 28, 2022 Hak’s Store
Project Manager: Ethan Rogerson GRI Project No. 2266
i
SITE INFORMATION
1. Site Identification
 Hak’s Store (Facility ID 0-00-0000006287)
 Incident Number 13273 – H190D
 Location of Source Area: 901 Washington Street
Plymouth, NC 27910
Washington County
35.85325°N, 76.743611°W (Topographical Map)
2. Information about Contacts Associated with the Leaking UST System

UST Owner
North East Oil Company, Inc.
Post Office Box 1386
Ahoskie, North Carolina 27910
[e-mail]
252-862-0236

UST Operator
North East Oil Company, Inc.
Post Office Box 1386
Ahoskie, North Carolina 27910
[e-mail]
252-862-0236

Property Owner
Aref Ali Saleh
112 Gen Pettigrew Drive
Plymouth, North Carolina 27962
Email - Unknown
Phone - Unknown

Property Occupant
Kwik Shop
901 Washington Street
Plymouth, North Carolina 27962
Email - Unknown
Phone - Unknown

Consultant/Contractor
Geological Resources, Inc.
3502 Hayes Road
Monroe, NC 28110
[e-mail]
704-845-4010

Analytical Laboratory
SGS North America, Inc.
4405 Vineland Road, Suite C-15
Orlando, Florida 32811
State Certification No. 573
407-425-6700
3. Information about Release
 Release was discovered on November 17, 1994
 An unknown amount of product was released from the leaking UST System
 Two 4,000-gallon gasoline USTs were removed from the site in November 1992.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: April 28, 2022 Hak’s Store
Project Manager: Ethan Rogerson GRI Project No. 2266
ii
EXECUTIVE SUMMARY
The former Hak’s Store is located at 901 Washington Street in Plymouth, Washington County, North
Carolina. The site is currently owned and operated by Aref Saleh as a convenience store. A release was
confirmed at the site following the removal of two 4,000-gallon gasoline USTs in November 1994. No
USTs are active at the site. The adjoining properties are a mixture of residential and commercial
properties. Four water supply wells (PSW-2, PSW-3, WSW-4, and WSW-5) were identified within a 1,500-
foot radius of the site during past receptor survey activities. Of the four identified, one active municipal
water supply well (PSW-2) is located approximately 325 feet from the site. WSW-4 (formerly Nicholson)
is located within a 250-foot radius of the site, but is inactive. Please note that PSW-1 identified in previous
assessment activities has been abandoned. In addition, WSW-5 is used for non-potable purposes and is
located greater than 250 feet from the site. The site is located within a designated wellhead protection
area. Municipal water is available to the site and surrounding properties. Despite the presence of water
supply wells in the vicinity of the site, the risk classification for the incident was lowered by the NCDEQ
regional supervisor from high risk to intermediate risk in June 2016. The site risk classification was raised
to high risk in February 2022 by NCDEQ.

A CAP proposing the remediation of the site using a combination of MMPE events and two AS/SVE systems
was submitted to NCDEQ on January 10, 2014. The CAP was approved by NCDEQ on February 5, 2014.

On March 17, 2022, eleven monitoring wells and two observation wells were gauged, purged and sampled
in accordance with NCDEQ guidelines. Concentrations of individual BTEX constituents, MTBE,
naphthalene, o-chlorotoluene, o-dichlorobenzene, isopropylbenzene, n-propylbenzene, 1,2,4-
trimethylbenzene and/or 1,3,5-trimethylbenzene that exceeded the MACs were reported in the ground
water samples collected from MW-1, MW-2, MW-5, MW-11, MW-14, MW-24, OW-4 and OW-5. All
reported contaminant concentrations were less than the GCLs.

Contaminant mass at the site has decreased 37.2% between September 2009 and March 2022. Please
note, this is an estimated contaminant mass area, a more accurate contaminant mass area can be
determined with a more comprehensive ground water sampling event.

GRI recommends that the January 10, 2014, CAP be implemented. Until corrective action can be
implemented, semi-annual ground water monitoring should continue at the site. The next semi-annual
sampling event is tentatively scheduled for September 2022 and should include all monitoring wells
associated with the incident in order to determine the current breadth of the contaminant plume for the
site.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: April 28, 2022 Hak’s Store
Project Manager: Ethan Rogerson GRI Project No. 2266
iii
ACRONYMS
ACM: Asbestos Containing Materials
AFVR: Aggressive Fluid-Vapor Recovery
ARR: Acknowledgement of Report Receipt
AS: Air Sparging
AST: Aboveground Storage Tank
ASTM: American Society for Testing and
Materials
BGS: Below Ground Surface
CAP: Corrective Action Plan
CFR: Code of Federal Regulations
CSA: Comprehensive Site Assessment
DPE: Dual Phase Extraction
DRO: Total Petroleum Hydrocarbons Diesel
Range Organics
DWM: Division of Waste Management
DWR: Department of Water Resources
EPA: Environmental Protection Agency
EPH: Extractible Petroleum Hydrocarbons
ESA: Environmental Site Assessment
GCL: Gross Contamination Level
GRI: Geological Resources, Inc.
GRO: Total Petroleum Hydrocarbons
Gasoline Range Organics
LSA: Limited Site Assessment
MAC: Maximum Allowable Concentration as
specified in T15A NCAC 2L.0202
MADEP: Massachusetts Department of
Environmental Protection
MCC: Maximum Contaminant Concentrations
MMPE: Mobile Multi-Phase Extraction
NAPL: Non-Aqueous Phase Liquid, “Free
Product”
NCDEQ: North Carolina Department of
Environmental Quality

NCDOT: North Carolina Department of
Transportation
NFA: Notice of No Further Action
NORR: Notice of Regulatory Requirements
NOV: Notice of Violation
NPDES: National Pollutant Discharge
Elimination System
NRP: Notice of Residual Petroleum
O&M: Operation and Maintenance
PAHs: Polynuclear Aromatic Hydrocarbons
PCA: Pre-Construction Assessment
RAL: Regulatory Action Level
SCLs: Soil Cleanup Level
SPCC: Spill Prevention Control and
Countermeasures
SVE: Soil Vapor Extraction
SVOCs: Semi-Volatile Organic Compounds
SWPPP: Stormwater Pollution Prevention Plan
TCLP: Toxicity Characteristic Leaching
Procedure (EPA Method SW-846 1311)
TOC: Top of Casing
TPH: Total Petroleum Hydrocarbons
USGS: United States Geological Survey
UST: Underground Storage Tank
UVF: Ultraviolet Fluorescence
VOCs: Volatile Organic Compounds
VPH: Volatile Petroleum Hydrocarbons

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: April 28, 2022 Hak’s Store
Project Manager: Ethan Rogerson GRI Project No. 2266
TABLE OF CONTENTS
SITE INFORMATION ............................................................................................................................ i
EXECUTIVE SUMMARY ....................................................................................................................... ii
ACRONYMS ....................................................................................................................................... iii
1.0 SITE HISTORY AND CHARACTERIZATION ...................................................................................1
2.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL
ASSESSMENT INFORMATION ...................................................................................................2
3.0 FREE PRODUCT REMOVAL ........................................................................................................4
4.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS ..................................4
5.0 CONCLUSIONS .........................................................................................................................5
6.0 LIMITATIONS ...........................................................................................................................5
7.0 STATEMENTS AND CERTIFICATION ...........................................................................................5

FIGURES
Figure 1: Site Location Map
Figure 2: Site Map
Figure 3: Site Vicinity Map
Figure 4: Water Table Surface Map
Figure 5: Ground Water Quality Map
Figure 6: Estimated Contaminant Mass Area Map

TABLES
Table 1: UST Owner and Operator Information
Table 2: UST System Information
Table 3: Adjacent Property Owner Information
Table 4: Water Supply Well Information
Table 5: Well Construction and Gauging Information
Table 6: Summary of Ground Water Sample Analytical Results

APPENDICES
Appendix A: State Correspondence
Appendix B: Laboratory Report – Ground Water Samples
Appendix C: Contaminant Mass Calculations

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: April 28, 2022 Hak’s Store
Project Manager: Ethan Rogerson GRI Project No. 2266
1
1.0 SITE HISTORY AND CHARACTERIZATION
GRI presents the results of the March 2022 ground water sampling activities at the Hak’s Store site;
located at 901 Washington Street in Plymouth, Washington County, North Carolina (Figure 1). These
activities were conducted in accordance with GRI Proposal No. 22-140, which was submitted to the North
Carolina Department of Environmental Quality (NCDEQ) on February 21, 2022, and was approved as Task
Authorization No. 13273-26 on February 24, 2022. State correspondence has been included as Appendix
A.

The site is currently owned by Harrell Enterprises, Inc. and is operated as a Kwik Shop convenience store.
According to available information, two 4,000-gallon gasoline USTs were removed from the site in
November 1994. UST owner/operator information and UST system information are included as Tables 1
and 2, respectively. The Registered Tank Report is shown below:

The site and surrounding area are a mixture of single-family residential and commercial properties. The
site contains one building and is primarily capped with grass, concrete and asphalt. The overall
topography at the site is relatively flat. A total of forty-three Type II monitoring wells (MW-1, MW-2, MW-
3, MW-5, MW-6R, MW-7R, MW-8 through MW-15, MW-16R, MW-17R, MW-18, MW-19R, MW-20
through MW-29, MW-32 and MW-38 through MW-52), eight Type III monitoring wells (MWD-4, MWD-
30, MWD-31, MWD-33, MWD-34 through MWD-37), six observation wells (OW-1 through OW-6) and one
air sparge well (AS-1) were installed at the site during past ground water assessment activities. Please
note, MW-26 was noted to have been abandoned during prior assessment activities. A CAP proposing the
remediation of the site using a combination of MMPE events and two AS/SVE systems was submitted to
NCDEQ on January 10, 2014. The CAP was approved by NCDEQ on February 5, 2014. A Site Map showing
the locations of the monitoring wells and the structures on-site has been included as Figure 2.

Four water supply wells (PSW-2, PSW-3, WSW-4, and WSW-5) were identified within a 1,500-foot radius
of the site during past receptor survey activities. Of the four identified wells, one active municipal water

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: April 28, 2022 Hak’s Store
Project Manager: Ethan Rogerson GRI Project No. 2266
2
supply well (PSW-2) is located approximately 325 feet from the site. WSW-4 (formerly Nicholson) is
located within a 250-foot radius of the site but is inactive. Please note that PSW-1 identified in previous
assessment activities has been abandoned. In addition, WSW-5 is used for non-potable purposes and is
located greater than 250 feet from the site. The site is located within a designated wellhead protection
area. Municipal water is available to the site and surrounding properties. On June 21, 2016, NCDEQ issued
a NORR which lowered the risk classification of the incident to Intermediate risk. The NORR indicated that
PSW-2 was located up-gradient and/or cross gradient of the contaminant plume. The site risk
classification was raised to high risk in February 2022 by NCDEQ. Adjacent property owner information is
presented in Table 3. Water supply well information is presented in Table 4. A Site Vicinity Map showing
the adjacent properties has been included as Figure 3.

Assessment activities conducted prior to March 2007 were performed by past consultants. Although GRI
cannot verify the accuracy of information obtained from previous reports, for the purposes of this report,
it is assumed to be correct. Please refer to previous submittals for further historical information regarding
the site.
2.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL
ASSESSMENT INFORMATION
On March 17, 2022, nine Type II monitoring wells (MW-1, MW-2, MW-9, MW-3, MW-5, MW-11, MW-14,
MW-15, MW-24 and MW-39), two Type III monitoring wells (MWD-4 and MWD-37) and two observation
wells (OW-4 and OW-5) were gauged, purged and sampled. Depths to ground water in the Type II
monitoring wells ranged from 8.06 feet to 10.21 feet below the tops of well casings. Ground water
elevations in the Type II monitoring wells ranged from 88.70 feet to 89.82 feet. Ground water flow at the
site is generally toward the northeast with a horizontal gradient of less than 0.01 feet per foot. The vertical
hydraulic gradient calculated for paired wells MW-1/MWD-4 was approximately 0.01 feet per foot in the
downward direction. Please note, the depth to water in MW-39 appears to be an anomaly and was not
considered when calculating ground water flow direction and hydraulic gradient. Well construction and
gauging information is presented in Table 5. A Water Table Surface Map based on the Type II monitoring
wells is included as Figure 4. A summary of the current ground water gauging data is shown below:
Well ID
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(feet)
Free
Product
Thickness
(ft.)
Ground
Water
Elevation
(ft.)
MW-1 5-15 15 99.80 9.98 --- 89.82
MW-2 5-15 15 99.71 10.08 --- 89.63
MW-3 5-15 15 99.98 10.21 --- 89.77
MWD-4 24-29 29 99.53 9.86 --- 89.67
MW-5 6-16 16 99.63 10.13 --- 89.50
MW-11 2-12 12 97.51 8.06 --- 89.45
MW-14 6-16 16 98.67 9.21 --- 89.46
MW-15 6-16 16 98.37 8.61 --- 89.76
MW-24 8-18 18 96.36 7.66 --- 88.70
MWD-37 NA NA 98.12 8.56 --- 89.56
MW-39 3-18 18 97.04 6.59 --- 90.45
OW-4 4-14 4 99.77 10.16 --- 89.61

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: April 28, 2022 Hak’s Store
Project Manager: Ethan Rogerson GRI Project No. 2266
3
Well ID
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(feet)
Free
Product
Thickness
(ft.)
Ground
Water
Elevation
(ft.)
OW-5 4-14 4 99.54 9.88 --- 89.66

Ground water samples collected from the monitoring and observation wells were submitted for
laboratory analyses of volatile organic compounds using EPA Method 6200B. Concentrations of individual
BTEX constituents, MTBE, naphthalene, o-chlorotoluene, o-dichlorobenzene, isopropylbenzene, n-
propylbenzene, 1,2,4-trimethylbenzene and/or 1,3,5-trimethylbenzene that exceeded the MACs were
reported in the ground water samples collected from MW-1, MW-2, MW-5, MW-11, MW-14, MW-24,
OW-4 and OW-5. All of the reported contaminant concentrations were less than the GCLs. A summary
of the analytical results for ground water samples collected on March 17, 2022, is presented in Table 6. A
Ground Water Quality Map based on the March 2022 data is included as Figure 5. A complete report of
laboratory analyses of the ground water samples collected from the monitoring wells during the March
2022 sampling event has been included as Appendix B. A summary of the current ground water analytical
data is shown below:

Contaminant of
Concern  Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene Well
ID
MACs (mg/l) 1 600 600 500 20 6
GCL (mg/l) 5,000 260,000 80,000 50,000 20,000 6,000
MW-1 26.2 J 7,770 2,560 18,300 <630 645
MW-2 <31 <31 119 J 334 J <31 103 J
MW-3 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13
MWD-4 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13
MW-5 448 16,900 4,400 31,400 525 742 J
MW-11 1.3 1.4 1.4 1.8 J 104 <6.3
MW-14 2,130 J 35,600 2,780 J 19,200 273 J 739
MW-15 <1.3 <1.3 <1.3 <2.5 <1.3 <1.3
MW-24 2.7 J 0.65 0.19 J 4.7 20.3 0.41 J
MWD-37 0.14 J 3.5 0.52 2.8 0.21 J 0.17 J
MW-39 <0.25 <0.25 <0.25 <0.50 4.5 <0.25
OW-4 1,220 J 6,170 2,850 15,500 1,700 417 J
OW-5 455 19,300 2,060 J 20,800 <1,300 835

The baseline contaminant mass at the site was determined based on the total BTEX, MTBE and
naphthalene concentrations from the September 2009 ground water sampling event. The estimated
contaminant plume area is based on the March 2022 ground water sampling event. Please note, this is
an estimated contaminant mass area; a more accurate contaminant mass area can be determined with a
more comprehensive ground water sampling event. The contaminant mass at the site has decreased by
approximately 37.2%. Contaminant mass calculations have been included as Appendix C. A map of the

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: April 28, 2022 Hak’s Store
Project Manager: Ethan Rogerson GRI Project No. 2266
4
contaminant mass area has been included as Figure 6. A chart depicting the overall trend in contaminant
mass is shown below:

The site is located in the Coastal Plain Physiographic Province of North Carolina. The water table has a
seasonal high depth to water of approximately 1 to 9 feet BGS. Free product has not been observed
since August 2011.

Please note that milestones were not established in the January 2014 CAP.
3.0 FREE PRODUCT REMOVAL
Free product has historically been present in MW-1, MW-2 and MW-5. One AFVR event was conducted
in August 2009. A total of 1.12 gallons of liquid and vapor phase free product has been removed from the
site since 2009. No free product has been observed since 2011.
4.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS
No natural attenuation monitoring plan is currently in place at the site. No contaminant reduction
milestones were presented in the January 2014 CAP.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: April 28, 2022 Hak’s Store
Project Manager: Ethan Rogerson GRI Project No. 2266
5
5.0 CONCLUSIONS
 On March 15, 2022, eleven monitoring wells and two observation wells and were gauged, purged
and sampled. Ground water flow was generally toward the northeast with a horizontal gradient
of less than 0.01 feet per foot. The vertical gradient between paired wells MW-1/MWD-4 was
approximately 0.01 feet per foot in the downward direction.
 Concentrations of individual BTEX constituents, MTBE, naphthalene, o-chlorotoluene, o-
dichlorobenzene, isopropylbenzene, n-propylbenzene, 1,2,4-trimethylbenzene and/or 1,3,5-
trimethylbenzene that exceeded the MACs were reported in the ground water samples collected
from MW-1, MW-2, MW-5, MW-11, MW-14, MW-24, OW-4 and OW-5. All reported contaminant
concentrations were less than the GCLs.
 Contaminant mass at the site has decreased 37.2% between September 2009 and March 2022.
Please note, this is an estimated contaminant mass area, a more accurate contaminant mass area
can be determined with a more comprehensive ground water sampling event.
 The site risk classification was raised to high risk in February 2022 by NCDEQ.
 GRI recommends that the January 10, 2014, CAP be implemented. Until corrective action can be
implemented, semi-annual ground water monitoring should continue at the site. The next semi-
annual sampling event is tentatively scheduled for September 2022 and should include all
monitoring wells associated with the incident in order to determine the current breadth of the
contaminant plume for the site.
6.0 LIMITATIONS
This report has been prepared for the exclusive use of North East Oil Company, Inc. for specific application
to the referenced site in Washington County, North Carolina. The assessment was conducted based on
the scope of work and level of effort desired by NCDEQ and with resources adequate only for that scope
of work. Our findings have been developed in accordance with generally accepted standards of
environmental practices in the State of North Carolina, available information, and our professional
judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would
be interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data.

7.0 STATEMENTS AND CERTIFICATION
1 Enter the date the monitoring report was due. n/a Will this report be submitted after the
established due date?
YES NO
2 Was any required information from the above template missing from this report? YES NO

FIGURES
!H
!H
"J
"J
DH
SITE EDGE OF PLUME
NC HWY 32 SOLD ROPER RD
IDA ST
HAZEL STWA
S
HIN
G
T
O
N S
T
ROOSEVELT AVHILLARD DRHILLY CRSHELLY DRWEST AVE
J
E
F
F
E
R
S
O
N S
T FORE ST R D
LATHAM AV
NC HWY 45 SPAMELA STR H O DES D RB
RIN
K
L
E
Y P
L
A
C
E
HOPKINS LN
CANAL ST
A A RO N S T
SAMANT
HA DRCART PATHUS HW Y 64 WCONABY CRK - PEACOCK SWAMPCONABY CREEK RUN OF PERSIMMON SWAMPPSW-3
PSW-2
WSW-5
WSW-4
PSW-1
6767930094
6767911880
6767836541
6767836341
6767
8
3
92466
7
6
7
8
3
61
5
7
67678391956767837191
6767834588
6767837179
³
FIGURE 3: SITE VICINITY MAPHAK'S STORE901 WASHINGTON STREETPLYMOUTH, WASHINGTON COUNTYNORTH CAROLINAINCIDENT NO. 13273
PREPARED BY:GEOLOGICAL RESOURCES, INC.OCTOBER 21, 2009
0 300150Feet
1 inch equals 300 feet
1,500-FOOT RADIUS
1,000-FOOT RADIUS 500-FOOT RADIUS
Legend
DH Water Supply Well (Abandoned)
"J Water Supply Well (Private)
!H Water Supply Well (Public)
CREEKS
centerline
parcels
6767837179 PIN Number

TABLES
UST ID Number 1 - 2 Facility ID Number
Owner or Operator?
Owner/Operator
TABLE 1
UST OWNER/OPERATOR INFORMATION
HAK'S STORE (INCIDENT NO. 13273)
00-0-0000006287
Name of Owner or Operator Dates of Ownership / Operation
E T Six Inc 03/02/1970 - 11/17/1994
Address
Unknown Unkown
Telephone Number
Page 1 of 1
Date: 04/18/22 Facility ID # : 00-0-0000006287
Was Release
Associated
with UST
System?
(Yes / No)
1 Gasoline,
Gas Mix 4,000 03/02/70 Single Wall Steel unknown unknown Removed
(11/17/94)Yes
2 Gasoline,
Gas Mix 4,000 03/02/70 Single Wall Steel unknown unknown Removed
(11/17/94)Yes
Tank
Dimensions
Description of
Associated
Product Piping
and
Pumps
TABLE 2
UST SYSTEM INFORMATION
HAK'S STORE (INCIDENT NO. 13273)
Status
of
UST
UST
ID
No.
Current
or Most
Recent
Contents
Capacity
(gallons)
Date
Installed
Construction
Details
Page 1 of 1
Date: 10/12/09 Facility ID # : 00-0-0000006287
6767837179 (site)Gerald & Cindy Furlough 173 Country Lane
Plymouth, NC 27962
6767837191 James F. Porter, Jr P.O. Box 477
Plymouth, NC 27962
6767836157 Mamie Lee Terry 103 Hazel Street
Plymouth, NC 27962
6767836341 Billy & Lucy Nicholson 815 Washington Street
Plymouth, NC 27962
6767839246 and 6767839195 Deloris K. Peele 816 Washington Street
Plymouth, NC 27962
6767930094 Town of Plymouth 124 East Water Street
Plymouth, NC 27962
Tax Pin Number/ Map ID Owner/Occupant Name Address
TABLE 3
PROPERTY OWNERS/OCCUPANTS
HAK'S STORE (INCIDENT NO. 13273)
Date: 10/12/09 Facility ID #: 00-0-0000006287
Well ID Parcel ID No.Well Owner Mailing Address Well Use
(Potable/ Agriculture, etc.)
Public Water
Connected
Distance from
source area of
release
(ft.)
PSW-1 6767930094 Town of Plymouth 124 East Water Street
Plymouth, NC 27962 Abandoned Unknown ~235' SE
PSW-2 6767836541 Town of Plymouth 124 East Water Street
Plymouth, NC 27962 Active/Potable/Municipal Unknown ~325' NNW
PSW-3 6767911880 Town of Plymouth 124 East Water Street
Plymouth, NC 27962 Active/Potable/Municipal Unknown ~1,390' SSE
WSW-4 6767836341 Billy & Lucy Nicholson 815 Washington Street
Plymouth, NC 27962 Inactive Unknown ~135' NW
WSW-5 6767834588 Paula S. Snider 8385 135th Street West
Apple Valley, MN 55124 Irrigation Unknown ~500' NW
Notes:
• Water supply wells are shown on Figure 3
• Ft. BGS : Feet below ground surface
TABLE 4
WATER SUPPLY WELL INFORMATION
HAK'S STORE (INCIDENT NO. 13273)
Page 1 of 1
Date: 04/18/22
03/07/07 9.72 90.28
08/08/07 10.94 0.04 89.09
08/20/09 10.62 0.13 89.49
08/20/09 10.50 89.50
09/23/09 10.76 89.24
08/11/10 11.00 89.00
09/06/12 10.23 89.57
08/21/13 9.67 90.13
03/03/16 9.01 90.79
10/31/17 10.38 89.42
09/10/18 9.61 90.19
02/18/19 9.17 90.63
03/17/22 9.98 89.82
03/07/07 9.73 90.34
08/08/07 11.13 0.19 89.10
08/20/09 10.77 0.22 89.49
08/20/09 10.51 89.56
09/23/09 10.81 89.26
08/11/10 11.05 0.03 89.05
08/19/11 11.20 0.05 88.91
09/06/12 10.30 89.41
08/21/13 9.77 89.94
10/31/17 10.43 89.28
03/17/22 10.08 89.63
03/07/07 9.86 90.37
08/08/07 11.10 89.13
09/23/09 10.95 89.28
08/11/10 11.18 89.05
09/06/12 10.44 89.54
08/21/13 9.87 90.11
03/03/16 9.15 90.83
03/17/22 10.21 89.77
03/07/07 NF NM NM
08/08/07 10.64 89.16
09/23/09 10.71 89.09
08/11/10 10.97 88.83
09/06/12 10.11 89.42
08/21/13 9.55 89.98
03/17/22 9.86 89.67
03/07/07 9.75 90.18
08/08/07 11.02 0.07 88.97
09/23/09 10.82 89.11
08/11/10 11.07 88.86
09/06/12 10.34 89.29
08/21/13 9.75 89.88
03/03/16 9.11 90.52
02/28/17 10.12 89.51
10/31/17 10.46 89.17
09/10/18 9.68 89.95
03/17/22 10.13 89.50
03/07/07 10.43 90.40
08/08/07 11.58 89.25
09/06/12 NM NM NM
03/03/16 9.70 90.92
09/23/09 11.55 89.39
08/11/10 11.73 89.21
09/06/12 11.04 89.56
08/21/13 10.46 90.14
03/07/07 NF NA
08/08/07 11.76 89.41
09/23/09 11.71 89.52
08/11/10 11.92 89.31
09/06/12 11.30 89.71
08/21/13 10.68 90.33
5NAMW-2
99.98
155 - 155NAMW-3
100.23
100.07
99.71
155 - 15
Facility ID # : 00-0-0000006287
99.80
155 - 155NAMW-1
MW-7R 08/17/09 3 3 - 18 18
101.23
101.01
MW-7 NA 2 2 - 12 12 101.17
MW-6R 08/17/09 3 3 - 18 18
100.94
100.60
MW-6 NA 2 2 - 12 12
100.83
100.62
99.93
99.80
99.53
2924 - 2924NAMWD-4
99.63
166 - 166NAMW-5
Free
Product
Thickness
(ft.)
Ground
Water
Elevation
(ft.)
100.00
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
HAK'S STORE (INCIDENT NO. 13273)
Well
ID
Date
Installed
(mm/dd/yy)
Date
Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y
ft. BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth
to Water
from Top
of Casing
(ft.)
Page 1 of 6
Date: 04/18/22 Facility ID # : 00-0-0000006287
Free
Product
Thickness
(ft.)
Ground
Water
Elevation
(ft.)
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
HAK'S STORE (INCIDENT NO. 13273)
Well
ID
Date
Installed
(mm/dd/yy)
Date
Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y
ft. BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth
to Water
from Top
of Casing
(ft.)
03/07/07 9.92 90.42
08/08/07 11.14 89.20
09/23/09 11.00 89.34
08/11/10 11.23 89.11
09/06/12 10.48 89.71
08/21/13 9.89 90.30
03/07/07 9.48 90.15
08/08/07 10.70 88.93
09/23/09 10.54 89.09
08/11/10 10.81 88.82
09/06/12 10.04 89.30
08/21/13 9.55 89.79
10/31/17 10.20 89.14
03/07/07 NF NM NM
08/08/07 10.40 88.95
09/23/09 10.12 89.23
08/11/10 10.23 89.12
09/06/12 9.61 89.38
08/21/13 8.99 90.00
03/07/07 NF NM NM
08/08/07 9.08 89.03
09/23/09 8.85 89.26
08/11/10 9.30 88.81
09/06/12 8.16 89.35
08/21/13 7.87 89.64
03/03/16 6.91 90.60
03/17/22 8.06 89.45
03/07/07 9.02 90.33
08/08/07 10.22 89.13
09/23/09 10.12 89.23
08/11/10 10.31 89.04
09/06/12 9.63 89.48
08/21/13 9.02 90.09
03/08/07 NF NM NM
08/08/07 9.30 88.84
09/23/09 9.36 88.78
08/11/10 9.66 88.48
09/06/12 8.81 89.13
08/21/13 8.42 89.52
03/03/16 7.82 90.12
03/07/07 8.91 90.11
08/08/07 10.14 0.03 88.91
09/23/09 9.93 89.09
08/11/10 10.21 88.81
09/06/12 9.44 89.23
08/21/13 8.83 89.84
03/03/16 8.25 90.42
02/28/17 9.28 89.39
10/31/17 9.55 89.12
09/10/18 8.84 89.83
02/18/19 8.31 90.36
01/09/20 9.42 89.25
02/09/21 8.41 90.26
03/17/22 9.21 89.46
03/07/07 8.62 90.02
08/08/07 9.83 88.81
09/23/09 9.67 88.97
08/11/10 8.92 89.72
09/06/12 9.10 89.27
08/21/13 8.55 89.82
03/03/16 7.92 90.45
09/10/18 8.56 89.81
02/18/19 8.05 90.32
03/17/22 8.61 89.76
2NAMW-11
98.67
166 - 166NAMW-14
MW-12 NA 2 2 - 12 12
99.35
99.11
98.11
97.51
122 - 12
98.64
98.37
166 - 16
99.02
MW-13 NA 6 6 - 16 16
98.14
97.94
6NAMW-15
MW-10 NA 6 6 - 16 16
99.35
98.99
MW-9 NA 4 4 - 14 14
99.63
99.34
MW-8 NA 6 6 - 16 16
100.34
100.19
Page 2 of 6
Date: 04/18/22 Facility ID # : 00-0-0000006287
Free
Product
Thickness
(ft.)
Ground
Water
Elevation
(ft.)
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
HAK'S STORE (INCIDENT NO. 13273)
Well
ID
Date
Installed
(mm/dd/yy)
Date
Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y
ft. BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth
to Water
from Top
of Casing
(ft.)
03/08/07 6.23 90.12
08/08/07 7.75 88.60
09/06/12 96.11 NM NM NM
09/23/09 7.76 88.76
08/11/10 8.22 88.30
09/06/12 7.34 88.88
08/21/13 6.92 89.30
03/03/16 6.35 89.87
03/08/07 DRY NM NM
08/08/07 DRY NM NM
09/23/09 7.87 88.47
08/11/10 8.36 87.98
09/06/12 7.44 88.79
08/21/13 7.03 89.20
03/08/07 7.18 89.51
08/08/07 8.31 88.38
09/24/09 8.06 88.63
08/11/10 8.48 88.21
09/06/12 7.58 88.85
08/21/13 7.10 89.33
03/08/07 4.08 92.28
08/08/07 DRY NM NM
09/24/09 7.65 88.62
08/11/10 8.13 88.14
09/06/12 7.21 88.70
08/21/13 6.79 89.12
03/03/16 6.32 89.59
03/07/07 1.25 96.37
08/08/07 8.90 88.72
09/24/09 8.60 89.02
08/11/10 8.77 88.85
09/06/12 3.02 94.35
08/21/13 NM NM NM
03/07/07 NF NM NM
08/08/07 9.85 88.15
09/24/09 9.69 88.31
08/11/10 10.05 87.95
09/06/12 9.28 88.96
08/21/13 8.87 89.37
03/07/07 NF NM NM
08/08/07 7.60 87.83
09/24/09 7.29 88.14
08/11/10 7.68 87.75
09/06/12 6.48 88.89
08/21/13 5.44 89.93
03/07/07 8.75 89.07
08/08/07 10.03 87.79
09/24/09 9.77 88.05
08/11/10 10.19 87.63
09/06/12 9.30 88.45
08/21/13 8.88 88.87
03/08/07 7.62 88.93
08/08/07 8.64 87.91
09/24/09 8.34 88.21
08/11/10 8.82 87.73
09/06/12 7.87 88.49
08/21/13 7.55 88.81
03/03/16 7.12 89.24
09/10/18 7.73 88.63
03/17/22 7.66 88.70
03/08/07 6.09 89.49
08/08/07 7.54 88.04
09/24/09 7.12 88.46
08/11/10 7.97 87.61
09/06/12 6.23 89.10
08/21/13 5.07 90.26
MW-22 NA 4 4 - 9 9
95.43
95.37
MW-21 NA 7.5 7.5 - 12.5 12.5
98.00
98.24
MW-25 NA 6 6 - 11 11
95.58
95.33
96.55
MW-23 NA 7 7 - 17 17
97.82
97.75
96.36
188 - 188NAMW-24
NA 5 5 - 10 10
97.62
97.37
MW-19R 08/17/09 3 3 - 18 18
96.27
95.91
MW-20
MW-19 NA 3 3 - 8 8 96.36
MW-18 NA 5 5 - 10 10
96.69
96.43
MW-17R 08/17/09 3 3 - 18 18
96.34
96.23
MW-17 NA 4 4 - 9 9 96.51
MW-16R 08/17/09 5 5 - 15 15
96.52
96.22
MW-16 NA 3 3 - 8 8 96.35
Page 3 of 6
Date: 04/18/22 Facility ID # : 00-0-0000006287
Free
Product
Thickness
(ft.)
Ground
Water
Elevation
(ft.)
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
HAK'S STORE (INCIDENT NO. 13273)
Well
ID
Date
Installed
(mm/dd/yy)
Date
Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y
ft. BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth
to Water
from Top
of Casing
(ft.)
03/08/07 4.08 91.84
08/08/07 10.00 85.92
09/24/09 9.81 86.11
08/11/10 10.13 85.79
09/06/12 9.31 90.10
08/21/13 8.76 90.65
03/08/07 NF NM NM
08/08/07 8.86 85.42
09/24/09 8.58 85.70
08/11/10 8.11 86.17
09/06/12 8.32 88.99
08/21/13 7.89 89.42
03/07/07 NM NM NM
08/08/07 7.57 84.87
09/24/09 7.41 85.03
08/11/10 7.68 84.76
09/06/12 6.72 88.30
08/21/13 6.34 88.68
03/03/16 6.02 89.00
03/07/07 10.14 89.57
08/08/07 11.10 88.61
09/23/09 11.43 88.28
08/11/10 9.88 89.83
09/06/12 10.65 88.96
08/21/13 9.40 90.21
03/07/07 13.12 86.58
08/08/07 15.30 84.40
09/23/09 14.77 84.93
08/11/10 14.87 84.83
09/06/12 13.85 85.54
08/21/13 8.31 91.08
03/08/07 7.25 85.40
08/08/07 8.22 84.43
09/24/09 7.77 84.88
08/11/10 8.45 84.20
09/06/12 7.30 88.00
08/21/13 7.11 88.19
03/08/07 7.12 85.64
08/08/07 8.18 84.58
09/24/09 7.71 85.05
08/11/10 8.40 84.36
09/06/12 7.48 87.86
08/21/13 7.09 88.25
03/08/07 7.90 88.18
08/08/07 7.95 88.13
09/24/09 7.70 88.38
08/11/10 8.18 87.90
09/06/12 7.22 88.57
08/21/13 6.83 88.96
03/03/16 6.35 89.44
03/08/07 6.55 89.73
08/08/07 7.76 88.52
09/23/09 7.49 88.79
08/11/10 7.99 88.29
09/06/12 7.03 89.00
08/21/13 5.23 90.80
10/31/17 7.16 88.87
03/07/07 7.95 89.60
08/08/07 8.83 88.72
09/23/09 8.67 88.88
08/11/10 8.95 88.60
09/06/12 8.20 89.16
08/21/13 7.64 89.72
10/31/17 8.23 89.13
MWD-36 NA NA NA NA
97.55
97.36
MWD-35 NA NA NA NA
96.28
96.03
MWD-34 NA NA NA NA
96.08
95.79
MWD-33 NA NA NA NA
92.76
95.34
MW-32 NA NA NA NA
92.65
95.30
MWD-31 NA 117 117 - 122 122
99.70
99.39
MWD-30 NA 87 87 - 92 92
99.71
99.61
MW-29 NA 7.5 7.5 - 12.5 12.5
92.44
95.02
MW-28 NA 7.5 7.5 - 12.5 12.5
94.28
97.31
MW-27 NA 7.5 7.5 - 12.5 12.5
95.92
99.41
Page 4 of 6
Date: 04/18/22 Facility ID # : 00-0-0000006287
Free
Product
Thickness
(ft.)
Ground
Water
Elevation
(ft.)
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
HAK'S STORE (INCIDENT NO. 13273)
Well
ID
Date
Installed
(mm/dd/yy)
Date
Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y
ft. BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth
to Water
from Top
of Casing
(ft.)
03/07/07 8.35 90.04
08/08/07 9.53 88.86
09/24/09 9.40 88.99
08/11/10 9.69 88.70
09/06/12 8.90 89.22
08/21/13 8.35 89.77
03/03/16 7.71 90.41
10/31/17 9.01 89.11
09/10/18 8.41 89.71
01/09/20 8.91 89.21
02/09/21 7.94 90.18
03/17/22 8.56 89.56
09/23/09 8.60 88.54
08/11/10 8.99 88.15
09/06/12 8.13 88.79
08/21/13 NM NM NM
09/23/09 8.25 89.09
08/11/10 8.71 88.63
09/06/12 7.94 89.10
08/21/13 7.70 89.34
03/03/16 6.34 90.70
02/28/17 7.01 90.03
10/31/17 8.11 88.93
09/10/18 7.74 89.30
03/17/22 6.59 90.45
08/11/10 90.74 6.79 83.95
09/06/12 3.25 90.17
08/21/13 2.80 90.62
03/03/16 2.96 90.46
08/11/10 93.47 10.05 83.42
09/06/12 6.63 89.53
08/21/13 4.70 91.46
08/11/10 96.97 12.60 84.37
09/06/12 11.77 87.95
08/21/13 11.31 88.41
08/11/10 93.55 9.15 84.40
09/06/12 8.12 88.04
08/21/13 7.83 88.33
08/11/10 95.43 11.12 84.31
09/06/12 10.13 87.98
08/21/13 9.88 88.23
08/11/10 95.28 11.06 84.22
09/06/12 10.05 87.87
08/21/13 9.80 88.12
08/11/10 93.93 9.80 84.13
09/06/12 8.78 87.81
08/21/13
09/06/12 9.21 87.64
08/21/13 9.02 87.83
03/03/16 8.80 88.05
09/06/12 8.90 87.74
08/21/13 8.68 87.96
03/03/16 8.47 88.17
09/06/12 5.75 88.40
08/21/13 5.97 88.18
09/06/12 4.05 87.86
08/21/13 3.79 88.12
09/06/12 3.50 87.94
08/21/13 3.17 88.27
09/06/12 4.80 88.16
08/21/13 4.50 88.46
09/06/12 10.55 89.52
08/21/13 9.91 90.16
OW-1 06/20/13 08/21/13 4 4 - 14 14 99.89 9.75 90.14
NANAMWD-37
97.04
183 - 18308/18/09MW-39
RW-1 NA NA NA ~24 100.07
MW-52 09/05/12 3 3 - 13 13 92.96
MW-51 09/05/12 3 3 - 13 13 91.44
MW-50 09/05/12 3.5 3.5 - 13.5 13.5 91.91
MW-49 09/05/12 3.5 3.5 - 13.5 13.5 94.15
MW-48 09/05/12 5 5 - 15 15 96.64
Destroyed
MW-47 09/05/12 4 4 - 14 14 96.85
MW-46 08/03/10 2 2 - 12 12 96.59
MW-45 08/04/10 2 2 - 12 12 97.92
MW-44 08/04/10 2 2 - 12 12 98.11
MW-43 08/04/10 2 2 - 12 12 96.16
MW-42 08/04/10 5 5 - 10 10 99.72
MW-41 08/04/10 5 5 - 10 10 96.16
MW-40 08/04/10 2 2 - 12 12 93.42
97.34
MW-38 08/18/09 3 3 - 18 18
97.14
96.92
98.39
98.12
NANA
Page 5 of 6
Date: 04/18/22 Facility ID # : 00-0-0000006287
Free
Product
Thickness
(ft.)
Ground
Water
Elevation
(ft.)
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
HAK'S STORE (INCIDENT NO. 13273)
Well
ID
Date
Installed
(mm/dd/yy)
Date
Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y
ft. BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth
to Water
from Top
of Casing
(ft.)
08/21/13 9.84 90.09
03/03/16 9.15 90.78
OW-3 06/20/13 08/21/13 4 4 - 14 14 99.84 9.84 90.00
08/21/13 9.80 89.97
03/03/16 9.12 90.65
03/17/22 10.16 89.61
08/21/13 9.56 89.98
03/03/16 8.88 90.66
02/28/17 9.90 89.64
10/31/17 10.24 89.30
09/10/18 9.23 90.31
02/18/19 9.03 90.51
03/17/22 9.88 89.66
OW-6 06/20/13 08/21/13 4 4 - 14 14 99.27 9.26 90.01
08/21/13 9.82 90.02
03/03/16 9.15 90.69
VE-1 06/20/13 08/21/13 3 3 - 8 8 99.92 NM NM NM
Notes:
06/20/13OW-5
99.77144 - 14406/20/13OW-4
4 - 144
OW-2 06/20/13 4 4 - 14 14
• NA: Not available
• NM: Not measured
• NF: Not found
• Top-of-casing elevation and well construction data is reproduced from the July 2005 moniotring report prepared by CES
Engineering, PC; elevations relative to a temporary benchmark with an assumed datum of 100.00 feet; data reported in feet.
• Top-of-casing elevations were remeasured on 09/25/12 by Coastal Engineering and Surveying, Inc.
• If free product is present in a well, ground water elevation is calculated by: [Top of Casing Elevation - Depth
to Water] + [free product thickness x 0.8581]
• ft BGS : feet below ground surface
AS-1 06/20/13 15 15 - 20 20 99.84
99.5414
99.93
Page 6 of 6
Date: 04/18/22
EPA
Method
6010B
Well
ID
Date
Collected
1 600 600 500 20 6 70 70 70 70 25 70 400 400 15
5,000 260,000 80,000 50,000 20,000 6,000 5,900 8,800 14,750 30,500 11,700 26,100 28,500 24,100 15,000
03/07/07 2,840 46,800 4,410 27,500 8.47 2,050 268 106 <0.500 273 192 765 1,360 5,190 171
08/09/07 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
09/23/09 1,850 41,500 4,280 31,500 <62.5 1,330 <45.0 <35.0 <47.5 215 J <50.0 454 1,130 5,100 163
08/12/10 754 19,600 2,320 19,000 <25.0 883 <50.0 34.0 J <19.0 114 <20.0 249 665 3,150 135
09/07/12 510 21,700 3,910 30,000 <65 973 68.7 J <51 <50 165 J <50 539 1,510 6,270 NR
08/22/13 1,160 21,100 1,870 33,700 26.4 J 1,010 30.3 J 27.1 J <10 92.7 19.2 J 267 1,430 4,930 NR
03/03/16 843 18,500 1,980 35,900 <63 1,470 119 J 78.1 J <63 146 J <63 494 2,540 9,540 NR
10/31/17 27.7 J 4,700 2,820 20,300 <25 714 71.3 J 53.0 J <25 204 <25 617 1,520 6,000 NR
09/10/18 141 14,800 3,540 29,800 <31 1,030 41.4 J 34.5 J <31 175 <31 479 1,530 5,950 NR
02/18/19 197 J 15,400 2,220 26,300 <63 892 <63 <63 <63 118 J <63 283 1,330 4,770 NR
03/17/22 26.2 J 7,770 2,560 18,300 <630 645 19.7 J 23.0 J <630 125 <630 354 1,140 J 2,670 NR
03/07/07 5.73 86.5 2,240 9,710 <0.500 896 183 46.0 0.580 261 <0.500 817 1,380 4,640 25.2
08/09/07 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
09/23/09 71.1 J 697 2,870 13,800 <50.0 896 <36.0 <28.0 <38.0 288 <40.0 <44.0 1,300 5,600 15.7
08/12/10 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
09/07/12 <26 <26 1,640 7,110 <26 513 43.5 J 34.3 J <20 206 <20 736 1,250 5,000 NR
08/22/13 <10 57.2 1,050 4,530 <10 365 56.9 42.5 J <10 204 25.7 J 682 1,210 4,000 NR
10/31/17 <13 52.1 396 1,610 <13 544 65.4 47.1 J <13 133 21.9 J 517 819 3,110 NR
03/17/22 <31 <31 119 J 334 J <31 103 J 35.0 J 41.7 J <31 96.2 J <31 465 824 2,720 NR
MW-1
MW-2
GCL (µg/l)p-Isopropyltoluenen-Propylbenzene1,3,5-Trimethylbenzene2L Standard (µg/l)Naphthalenen-Butylbenzenesec-Butylbenzenetert-ButylbenzeneTABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
HAK'S STORE (INCIDENT NO. 13273)
Facility ID # : 00-0-0000006287
Analytical Method
→EPA Method 6200B
Contaminant of Concern
→BenzeneTolueneEthylbenzeneXylenesMTBE1,2,4-TrimethylbenzeneLeadIsopropylbenzenePage 1 of 11
Date: 04/18/22
EPA
Method
6010B
Well
ID
Date
Collected
1 600 600 500 20 6 70 70 70 70 25 70 400 400 15
5,000 260,000 80,000 50,000 20,000 6,000 5,900 8,800 14,750 30,500 11,700 26,100 28,500 24,100 15,000GCL (µg/l)p-Isopropyltoluenen-Propylbenzene1,3,5-Trimethylbenzene2L Standard (µg/l)Naphthalenen-Butylbenzenesec-Butylbenzenetert-ButylbenzeneTABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
HAK'S STORE (INCIDENT NO. 13273)
Facility ID # : 00-0-0000006287
Analytical Method
→EPA Method 6200B
Contaminant of Concern
→BenzeneTolueneEthylbenzeneXylenesMTBE1,2,4-TrimethylbenzeneLeadIsopropylbenzene03/07/07 <0.500 <0.500 <0.500 <1.00 2.36 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 10.6
08/09/07 <0.500 <0.500 <0.500 <1.00 2.34 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 23.0
09/23/09 1.21 0.356 J <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.190 0.694 J <0.200 0.425 J <0.180 <0.150 9.42
08/12/10 <0.140 <0.500 0.162 J 1.05 <0.250 0.722 J 1.08 0.263 J <0.190 0.208 J <0.200 0.732 J 1.56 4.93 11.2
09/07/12 0.19 J <0.13 <0.15 <0.30 0.23 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR
08/22/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR
03/03/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
03/17/22 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
03/07/07 NF NF NF NF NF NF NF NF NF NF NF NF NF NF NF
08/09/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00
09/23/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 <0.150 9.14
08/12/10 <0.140 <0.500 <0.150 0.431 J <0.250 <0.500 <0.500 0.143 J <0.190 <0.150 <0.200 0.313 J 0.515 J 1.64 73.1
09/07/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR
08/22/13 0.15 J 0.87 0.15 J 0.58 J 0.19 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR
03/17/22 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
03/07/07 11,200 36,200 4,000 21,400 2,010 1,390 400 46.1 <0.500 179 26.0 926 1,160 4,200 61.6
08/09/07 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
09/23/09 4,940 29,500 2,830 19,400 1,220 1,040 <36.0 <28.0 <38.0 195 J <40.0 553 1,240 4,960 46.1
08/12/10 2,120 12,100 1,360 8,540 266 J 1,450 <500 <140 <190 <150 <200 258 J 497 J 2,250 35.0
09/07/12 3,540 20,400 2,570 18,500 1,060 767 <50 <51 <50 101 J <50 315 732 3,110 NR
08/23/13 3,620 15,000 1,950 18,900 761 881 35.8 J 23.2 J <10 117 13.0 J 367 916 3,600 NR
03/03/16 2,840 15,100 1,900 20,800 981 1,210 107 J 64.1 J <63 145 J <63 479 1,440 5,710 NR
02/28/17 1,200 20,300 2,150 15,100 187 J 720 <63 <63 <63 63.2 J <63 193 J 544 2,470 NR
10/31/17 567 16,700 1,930 13,300 281 599 26.1 J 18.1 J <13 89.2 <13 263 727 2,930 NR
09/10/18 1,280 23,300 2,280 22,300 367 1,210 127 J 65.2 J <63 169 J <63 523 1,570 5,890 NR
03/17/22 448 16,900 4,400 31,400 525 742 J <630 <630 <630 115 J <630 293 1,660 J 4,410 NR
MW-3
MW-5
MWD-4
Page 2 of 11
Date: 04/18/22
EPA
Method
6010B
Well
ID
Date
Collected
1 600 600 500 20 6 70 70 70 70 25 70 400 400 15
5,000 260,000 80,000 50,000 20,000 6,000 5,900 8,800 14,750 30,500 11,700 26,100 28,500 24,100 15,000GCL (µg/l)p-Isopropyltoluenen-Propylbenzene1,3,5-Trimethylbenzene2L Standard (µg/l)Naphthalenen-Butylbenzenesec-Butylbenzenetert-ButylbenzeneTABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
HAK'S STORE (INCIDENT NO. 13273)
Facility ID # : 00-0-0000006287
Analytical Method
→EPA Method 6200B
Contaminant of Concern
→BenzeneTolueneEthylbenzeneXylenesMTBE1,2,4-TrimethylbenzeneLeadIsopropylbenzene03/07/07 <0.500 2.52 1.06 5.63 <0.500 <5.00 0.590 <0.500 <0.500 <0.500 <0.500 0.680 1.25 3.58 372
08/09/07 DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY
03/03/16 <0.13 6.3 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
09/23/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 <0.150 67.5
08/12/10 <0.140 <0.500 <0.150 <0.220 <0.250 <0.500 <0.500 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 <0.150 15.2
09/07/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR
08/23/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR
03/07/07 NF NF NF NF NF NF NF NF NF NF NF NF NF NF NF
08/09/07 DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY
09/23/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 <0.150 211
08/12/10 <0.140 <0.500 <0.150 <0.220 <0.250 <0.500 <0.500 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 <0.150 97.0
09/07/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR
08/23/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR
03/07/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 48.2
08/09/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 20.4
09/23/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 <0.150 35.2
08/12/10 <0.140 <0.500 <0.150 <0.220 <0.250 <0.500 <0.500 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 <0.150 36.5
09/07/12 <0.13 <0.13 <0.15 <0.30 0.26 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR
08/22/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR
03/07/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 78.3
08/09/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 60.6
09/23/09 0.913 J 7.69 1.65 11.5 <0.250 <0.500 <0.180 <0.140 <0.190 <0.150 <0.200 0.699 J 1.52 4.87 10.6
08/12/10 <0.140 <0.500 <0.150 <0.220 <0.250 <0.500 <0.500 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 <0.150 11.1
09/07/12 0.14 J 0.36 J <0.15 0.51 J <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR
08/23/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR
10/31/17 <0.13 0.17 J <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
03/07/07 NF NF NF NF NF NF NF NF NF NF NF NF NF NF NF
08/09/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 12.7
09/23/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 <0.150 246
08/11/10 <0.140 0.199 J <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 0.165 J 108
09/07/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR
08/23/13 <0.10 64.2 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 12.6 <0.10 <0.10 <0.10 NR
MW-10
MW-9
MW-6
MW-6R
MW-7
MW-7R
MW-8
Page 3 of 11
Date: 04/18/22
EPA
Method
6010B
Well
ID
Date
Collected
1 600 600 500 20 6 70 70 70 70 25 70 400 400 15
5,000 260,000 80,000 50,000 20,000 6,000 5,900 8,800 14,750 30,500 11,700 26,100 28,500 24,100 15,000GCL (µg/l)p-Isopropyltoluenen-Propylbenzene1,3,5-Trimethylbenzene2L Standard (µg/l)Naphthalenen-Butylbenzenesec-Butylbenzenetert-ButylbenzeneTABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
HAK'S STORE (INCIDENT NO. 13273)
Facility ID # : 00-0-0000006287
Analytical Method
→EPA Method 6200B
Contaminant of Concern
→BenzeneTolueneEthylbenzeneXylenesMTBE1,2,4-TrimethylbenzeneLeadIsopropylbenzene03/07/07 NF NF NF NF NF NF NF NF NF NF NF NF NF NF NF
08/09/07 10,000 1,830 1,360 4,840 8,910 241 <10.0 <10.0 <10.0 80.0 <10.0 113 179 667 82.1
09/23/09 202 118 79.4 260 649 23.6 <0.180 <0.140 20.1 2.37 <0.200 6.01 6.82 47.8 151
08/12/10 137 7.24 J 37.6 76.7 1,960 9.17 J <5.00 <1.40 <1.90 <1.50 <2.00 3.69 J 2.66 J 21.2 103
09/06/12 18.5 J <6.4 <7.3 <15 1,690 <5.0 <5.0 <5.1 <5.0 <5.0 <5.0 <5.4 <5.0 <5.0 NR
08/23/13 21.4 J 6.1 J <5.0 <11 1,620 <7.4 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 NR
03/03/16 6.6 <0.13 <0.13 <0.31 579 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
03/17/22 1.3 1.4 1.4 1.8 J 104 <6.3 <6.3 0.54 J <6.3 <6.3 <6.3 <6.3 <6.3 0.65 J NR
03/07/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 28.1
08/09/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00
09/23/09 0.223 J 0.586 J <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 <0.150 23.6
08/12/10 <0.140 <0.500 <0.150 <0.220 <0.250 <0.500 <0.500 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 <0.150 10.5
09/07/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR
08/23/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR
03/08/07 NF NF NF NF NF NF NF NF NF NF NF NF NF NF NF
08/09/07 26.9 1.20 41.6 44.0 26.3 11.4 4.79 1.98 <0.500 5.16 0.800 15.8 13.4 67.0 58.0
09/23/09 67.9 2.23 16.3 6.91 107 23.2 <0.180 2.36 <0.190 10.8 <0.200 4.22 0.747 J 17.3 38.7
08/12/10 721 2,520 899 4,010 365 304 24.5 9.78 J <1.90 48.0 10.7 124 218 971 37.0
09/06/12 76.7 9.8 106 240 44.5 41.1 3.8 3.0 <0.10 11.3 1.3 33.1 33.9 112 NR
08/23/13 78.4 3.4 182 83.5 89.9 38.1 8.3 7.1 0.16 J 21.1 2.8 67.1 17.6 142 NR
03/03/16 46.6 2.3 89.1 57.6 97.6 44.8 6.1 4.8 <0.13 13.0 1.8 33.7 16.3 59.2 NR
03/07/07 16,900 42,900 4,520 27,300 2,210 2,340 499 79.6 <0.500 253 170 804 1,830 6,200 38.6
08/09/07 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
09/23/09 7,020 32,700 4,210 22,700 615 1,250 <36.0 <28.0 <38.0 192 J <40.0 480 1,240 4,960 41.3
08/12/10 4,430 16,700 1,810 9,810 995 829 <50.0 15.2 J <19.0 80.4 J 25.8 J 197 467 2,010 30.3
09/06/12 6,700 35,300 4,200 22,600 837 752 <50 <51 <50 116 J <50 391 784 3,360 NR
08/23/13 6,150 24,700 3,050 23,800 1,710 1,140 37.3 J 24.0 J <10 136 14.8 J 436 1,130 4,210 NR
03/03/16 5,600 13,900 801 23,200 2,090 3,900 258 114 J <63 100 J 63.6 J 312 3,300 10,100 NR
02/28/17 5,410 31,700 2,310 13,400 458 J 600 <130 <130 <130 <130 <130 209 J 571 1,880 NR
10/31/17 2,350 17,900 1,580 9,380 239 J 522 26.2 17.4 <0.63 114 11.4 167 J 550 1,830 NR
09/10/18 4,920 46,800 4,120 21,300 263 726 <63 <63 <63 136 J <63 378 826 3,200 NR
02/18/19 6.8 42.5 9.8 75.6 12.4 4.2 <0.63 <0.63 <0.63 <0.63 <0.63 1.5 J 3.5 14.4 NR
01/09/20 3,290 45,600 4,600 23,100 229 J 635 <130 <130 <130 148 J <130 386 J 811 3,070 NR
02/09/21 5,020 34,600 3,210 18,900 <130 625 <130 <130 <130 <130 <130 302 J 780 2,520 NR
03/17/22 2,130 J 35,600 2,780 J 19,200 273 J 739 <1,300 <1,300 <1,300 136 J <1,300 367 J 817 2,920 NR
MW-11
MW-12
MW-13
MW-14
Page 4 of 11
Date: 04/18/22
EPA
Method
6010B
Well
ID
Date
Collected
1 600 600 500 20 6 70 70 70 70 25 70 400 400 15
5,000 260,000 80,000 50,000 20,000 6,000 5,900 8,800 14,750 30,500 11,700 26,100 28,500 24,100 15,000GCL (µg/l)p-Isopropyltoluenen-Propylbenzene1,3,5-Trimethylbenzene2L Standard (µg/l)Naphthalenen-Butylbenzenesec-Butylbenzenetert-ButylbenzeneTABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
HAK'S STORE (INCIDENT NO. 13273)
Facility ID # : 00-0-0000006287
Analytical Method
→EPA Method 6200B
Contaminant of Concern
→BenzeneTolueneEthylbenzeneXylenesMTBE1,2,4-TrimethylbenzeneLeadIsopropylbenzene03/07/07 11,300 26,400 2,710 14,000 4,850 11,200 <0.500 12.6 <0.500 83.0 5.91 366 766 2,880 37.8
08/09/07 12,900 33,300 2,990 16,300 3,690 609 183 <25.0 <25.0 198 <25.0 305 558 2,050 38.5
09/23/09 6,400 17,300 1,930 11,900 3,050 615 <18.0 <14.0 <19.0 89.7 J <20.0 218 479 2,120 30.9
08/12/10 2,500 7,380 598 4,040 2,590 628 <250 <70.0 <95.0 <75.0 <100 111 J 188 J 842 37.8
09/06/12 1,340 4,920 820 6,840 780 262 <10 <10 <10 32.5 J <10 105 254 1,090 NR
08/23/13 1,200 4,820 1,100 8,490 574 380 13.0 J <10 <10 61.7 <10 184 380 1,520 NR
03/03/16 125 124 42.9 272 111 19.7 <0.63 0.78 J <0.63 2.8 <0.63 6.7 10.2 49.2 NR
09/10/18 166 1,040 417 3,200 49.8 191 4.4 J 4.2 J <3.1 23.5 <3.1 67.9 131 620 NR
02/18/19 5,310 37,200 3,640 19,900 848 726 <130 <130 <130 <130 <130 341 J 908 3,110 NR
03/17/22 <1.3 <1.3 <1.3 <2.5 <1.3 <1.3 <1.3 <1.3 <1.3 <1.3 <1.3 <1.3 <1.3 <1.3 NR
03/08/07 9.46 <0.500 3.66 1.61 17.1 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 1.24 91.7
08/09/07 DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY
09/23/09 105 11.3 58.1 106 214 31.0 <0.180 0.521 J <0.190 3.59 <0.200 5.80 5.60 25.0 175
08/11/10 95.4 12.2 <0.750 114 517 26.7 <0.900 1.32 J <0.950 <0.750 <1.00 3.92 J 7.91 50.1 51.4
09/06/12 395 16.0 153 1,000 495 103 2.2 J 2.3 J <1.0 11.2 <1.0 17.2 61.5 205 NR
08/23/13 202 13.0 46.1 503 99.4 58.1 1.4 2.2 <0.10 7.9 0.77 6.6 28.9 107 NR
03/03/16 201 6.6 70.9 444 129 63.6 1.1 J 1.2 J <0.63 5.6 <0.63 8.3 28.5 100 NR
03/08/07 DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY
08/09/07 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
09/23/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 <0.150 105
08/11/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 <0.150 70.0
09/06/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR
08/23/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR
03/08/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 24.5
08/09/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00
09/24/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 <0.150 8.73
08/11/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 <0.150 30.1
09/06/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR
08/23/13 <0.10 <0.10 <0.10 <0.22 0.13 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR
03/08/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 22.8
08/09/07 DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY
09/24/09 <0.140 <0.190 <0.150 <0.220 1.19 <0.500 <0.180 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 <0.150 248
08/11/10 <0.140 <0.190 <0.150 <0.220 9.07 <0.500 <0.180 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 <0.150 23.4
09/06/12 0.21 J <0.13 <0.15 <0.30 35.9 0.17 J <0.10 0.13 J <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR
08/23/13 <0.10 <0.10 <0.10 <0.22 13.9 <0.15 <0.10 0.22 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR
03/03/16 <0.13 <0.13 <0.13 <0.31 0.56 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
MW-16
MW-16R
MW-17
MW-17R
MW-18
MW-19
MW-19R
MW-15
Page 5 of 11
Date: 04/18/22
EPA
Method
6010B
Well
ID
Date
Collected
1 600 600 500 20 6 70 70 70 70 25 70 400 400 15
5,000 260,000 80,000 50,000 20,000 6,000 5,900 8,800 14,750 30,500 11,700 26,100 28,500 24,100 15,000GCL (µg/l)p-Isopropyltoluenen-Propylbenzene1,3,5-Trimethylbenzene2L Standard (µg/l)Naphthalenen-Butylbenzenesec-Butylbenzenetert-ButylbenzeneTABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
HAK'S STORE (INCIDENT NO. 13273)
Facility ID # : 00-0-0000006287
Analytical Method
→EPA Method 6200B
Contaminant of Concern
→BenzeneTolueneEthylbenzeneXylenesMTBE1,2,4-TrimethylbenzeneLeadIsopropylbenzene03/07/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 498
08/09/07 64.6 0.830 1.52 19.1 5.91 <5.00 1.36 <0.500 <0.500 <0.500 <0.500 0.550 2.22 7.87 565
09/24/09 0.672 J <0.190 <0.150 <0.220 0.470 J <0.500 <0.180 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 <0.150 465
08/11/10 147 42.0 71.1 241 236 20.3 <0.360 1.31 J <0.380 5.24 <0.400 7.01 9.50 43.2 132
09/06/12 <0.13 91.9 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR
03/07/07 NF NF NF NF NF NF NF NF NF NF NF NF NF NF NF
08/09/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 149
09/24/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 <0.150 <1.50
08/11/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 <0.150 2.08 J
09/07/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR
08/23/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR
03/07/07 NF NF NF NF NF NF NF NF NF NF NF NF NF NF NF
08/09/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 26.1
09/24/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 <0.150 84.0
08/11/10 <0.140 0.537 J 0.510 J <0.220 <0.250 <0.500 <0.180 <0.140 <0.190 <0.150 <0.200 8.39 <0.180 0.155 J 136
09/06/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR
08/23/13 <0.10 0.17 J <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 0.58 <0.10 <0.10 NR
03/07/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 25.8
08/09/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 53.5
09/24/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 <0.150 1.73 J
08/11/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 <0.150 7.48
09/06/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR
08/23/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR
03/08/07 106 <0.500 <0.500 24.5 258 6.34 <0.500 0.560 <0.500 2.19 <0.500 <0.500 0.500 2.99 31.1
08/09/07 189 0.710 <0.500 18.6 161 8.40 1.39 0.960 <0.500 5.79 <0.500 <0.500 0.500 0.870 70.0
09/24/09 14.2 3.23 <0.150 <0.220 273 1.46 0.628 J 1.41 <0.190 6.53 <0.200 0.359 J <0.180 <0.150 33.5
08/11/10 4.69 <0.190 <0.150 <0.220 91.6 <0.500 <0.180 0.456 J <0.190 0.745 J <0.200 <0.220 <0.180 <0.150 25.8
09/06/12 6.1 0.40 J 0.26 J 1.2 J 182 0.77 0.19 J 0.61 <0.10 1.5 <0.10 <0.11 <0.10 <0.10 NR
08/23/13 10.1 0.87 0.40 J 1.8 171 1.8 0.20 J 0.85 <0.10 1.4 <0.10 0.12 J <0.10 0.34 J NR
03/03/16 4.9 0.30 J 0.58 1.3 J 61.9 2.1 <0.13 0.28 J <0.13 0.58 <0.13 <0.13 <0.13 <0.13 NR
09/10/18 1.7 <0.13 <0.13 <0.25 71.3 0.42 J <0.13 0.54 <0.13 0.25 J 6.1 <0.13 <0.13 <0.13 NR
03/17/22 2.7 J 0.65 0.19 J 4.7 20.3 0.41 J <1.3 0.21 J <1.3 0.19 J 0.69 <1.3 0.13 J <1.3 NR
MW-24
MW-20
MW-21
MW-22
MW-23
Page 6 of 11
Date: 04/18/22
EPA
Method
6010B
Well
ID
Date
Collected
1 600 600 500 20 6 70 70 70 70 25 70 400 400 15
5,000 260,000 80,000 50,000 20,000 6,000 5,900 8,800 14,750 30,500 11,700 26,100 28,500 24,100 15,000GCL (µg/l)p-Isopropyltoluenen-Propylbenzene1,3,5-Trimethylbenzene2L Standard (µg/l)Naphthalenen-Butylbenzenesec-Butylbenzenetert-ButylbenzeneTABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
HAK'S STORE (INCIDENT NO. 13273)
Facility ID # : 00-0-0000006287
Analytical Method
→EPA Method 6200B
Contaminant of Concern
→BenzeneTolueneEthylbenzeneXylenesMTBE1,2,4-TrimethylbenzeneLeadIsopropylbenzene03/08/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 42.1
08/09/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 92.8
09/24/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 <0.150 27.9
08/11/10 <0.140 <0.190 <0.150 <0.220 8.98 <0.500 <0.180 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 <0.150 15.9
09/06/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR
08/23/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR
03/08/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 24.9
08/09/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 249
09/24/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 <0.150 152
08/12/10 <0.140 <0.500 <0.150 <0.220 <0.250 <0.500 <0.500 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 0.182 J 7.53
09/06/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR
08/23/13 <0.10 <0.10 <0.10 <0.22 <0.10 0.18 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR
03/08/07 NF NF NF NF NF NF NF NF NF NF NF NF NF NF NF
08/09/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 155
09/24/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.190 <0.150 11.5 <0.220 <0.180 <0.150 18.5
08/11/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 <0.150 78.1
09/06/12 <0.13 0.85 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR
08/23/13 <0.10 74.1 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 1.0 <0.10 <0.10 <0.10 NR
03/07/07 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
08/09/07 9.61 <0.500 <0.500 <1.00 5,120 <5.00 <0.500 <0.500 <0.500 4.48 <0.500 <0.500 <0.500 <0.500 154
09/24/09 7.31 J <3.80 <3.00 <4.40 2,570 <10.0 <3.60 <2.80 <3.80 <3.00 <4.00 <4.40 <3.60 <3.00 242
08/11/10 1.66 J <1.90 <1.50 <2.20 1,250 <5.00 <1.80 <1.40 <1.90 <1.50 <2.00 <2.20 <1.80 <1.50 108
09/06/12 <0.13 <0.13 <0.15 <0.30 253 <0.10 <0.10 0.23 J <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR
08/23/13 <1.0 <1.0 <1.0 <2.2 224 <1.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NR
03/03/16 <0.13 <0.13 <0.13 <0.31 127 <0.13 <0.13 0.15 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
03/07/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00
08/09/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 98.7
09/23/09 <0.140 0.348 J <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 <0.150 <1.50
08/11/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 <0.150 1.55 J
09/07/12 0.19 J <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR
08/22/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR
03/07/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00
08/09/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00
09/23/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 <0.150 <1.50
08/11/10 0.150 J <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 <0.150 <1.50
09/07/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR
08/22/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR
MW-25
MW-27
MW-28
MW-29
MWD-30
MWD-31
Page 7 of 11
Date: 04/18/22
EPA
Method
6010B
Well
ID
Date
Collected
1 600 600 500 20 6 70 70 70 70 25 70 400 400 15
5,000 260,000 80,000 50,000 20,000 6,000 5,900 8,800 14,750 30,500 11,700 26,100 28,500 24,100 15,000GCL (µg/l)p-Isopropyltoluenen-Propylbenzene1,3,5-Trimethylbenzene2L Standard (µg/l)Naphthalenen-Butylbenzenesec-Butylbenzenetert-ButylbenzeneTABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
HAK'S STORE (INCIDENT NO. 13273)
Facility ID # : 00-0-0000006287
Analytical Method
→EPA Method 6200B
Contaminant of Concern
→BenzeneTolueneEthylbenzeneXylenesMTBE1,2,4-TrimethylbenzeneLeadIsopropylbenzene03/08/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 0.520 52.0
08/09/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 135
09/24/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 <0.150 149
08/11/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 <0.150 29.7
09/06/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR
08/23/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR
03/08/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00
08/09/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00
09/24/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 <0.150 <1.50
08/11/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 <0.150 1.72 J
09/06/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR
08/22/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR
03/08/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 0.650 <5.00
08/09/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00
09/24/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 <0.150 <1.50
08/11/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 <0.150 1.61 J
09/06/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR
08/22/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR
03/03/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
03/08/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00
08/09/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00
09/23/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 <0.150 10.1
08/11/10 <0.140 1.20 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 <0.150 43.0
09/06/12 <0.13 0.24 J <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR
08/22/13 <0.10 0.35 J <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR
03/07/07 <0.500 0.640 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00
08/09/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00
09/23/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 <0.150 <1.50
08/12/10 <0.140 <0.500 <0.150 <0.220 <0.250 <0.500 <0.500 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 0.152 J <1.50
09/06/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR
08/22/13 <0.10 0.11 J <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR
MW-32
MWD-33
MWD-34
MWD-35
MWD-36
Page 8 of 11
Date: 04/18/22
EPA
Method
6010B
Well
ID
Date
Collected
1 600 600 500 20 6 70 70 70 70 25 70 400 400 15
5,000 260,000 80,000 50,000 20,000 6,000 5,900 8,800 14,750 30,500 11,700 26,100 28,500 24,100 15,000GCL (µg/l)p-Isopropyltoluenen-Propylbenzene1,3,5-Trimethylbenzene2L Standard (µg/l)Naphthalenen-Butylbenzenesec-Butylbenzenetert-ButylbenzeneTABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
HAK'S STORE (INCIDENT NO. 13273)
Facility ID # : 00-0-0000006287
Analytical Method
→EPA Method 6200B
Contaminant of Concern
→BenzeneTolueneEthylbenzeneXylenesMTBE1,2,4-TrimethylbenzeneLeadIsopropylbenzene03/07/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00
08/09/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00
09/24/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 <0.150 <1.50
08/12/10 <0.140 <0.500 <0.150 <0.220 <0.250 <0.500 <0.500 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 <0.150 <1.50
09/06/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR
08/22/13 709 2,440 524 4,610 404 156 4.4 J 4.1 J <2.5 25.1 <2.5 84.2 152 665 NR
03/03/16 <0.13 <0.13 <0.13 <0.31 0.16 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
09/10/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
01/09/20 <0.13 1.6 0.20 J 0.92 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
02/09/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
03/17/22 0.14 J 3.5 0.52 2.8 0.21 J 0.17 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 0.22 J 0.52 NR
09/24/09 97.4 5.33 20.0 58.2 94.7 8.31 <0.180 0.463 J <0.190 2.41 <0.200 1.96 2.26 10.3 194
08/11/10 23.9 J <19.0 <15.0 <22.0 34.3 J <50.0 <18.0 <14.0 <19.0 <15.0 <20.0 <22.0 <18.0 <15.0 410
09/06/12 72.8 8.7 25.5 105 148 12.2 0.26 J 0.69 <0.10 1.8 <0.10 3.0 3.0 18.9 NR
09/24/09 394 70.1 59.7 206 1,050 14.2 <1.80 <1.40 <1.90 4.71 J <2.00 5.76 J 7.65 J 27.7 278
08/12/10 199 61.7 33.5 117 2,770 8.14 <2.50 <0.700 <0.950 2.45 J <1.00 3.50 J 5.27 17.1 119
09/06/12 68.2 <2.6 9.3 J 37.4 2,490 4.8 J <2.0 <2.0 <2.0 <2.0 <2.0 <2.1 <2.0 4.4 J NR
08/23/13 53.7 12.4 J 11.7 J 42.2 J 3,370 <15 <10 <10 <10 <10 <10 <10 <10 <10 NR
03/03/16 <1.3 <1.3 <1.3 <3.1 1,550 2.3 J <1.3 <1.3 <1.3 <1.3 <1.3 <1.3 <1.3 <1.3 NR
02/28/17 <1.3 <1.3 <1.3 <2.5 1,060 <1.3 <1.3 <1.3 <1.3 <1.3 <1.3 <1.3 <1.3 <1.3 NR
10/31/17 20.0 1.1 3.7 26.6 196 3.6 <0.13 0.24 J <0.13 1.5 <0.13 0.58 1.1 2.2 NR
09/10/18 23.6 2.2 5.1 34.7 82.8 3.0 <0.31 <0.31 <0.31 1.2 J <0.31 0.65 J 1.3 3.3 NR
03/17/22 <0.25 <0.25 <0.25 <0.50 4.5 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 NR
08/11/10 <0.700 <0.950 <0.750 <1.10 851 <2.50 <0.900 <0.700 <0.950 <0.750 <1.00 <1.10 <0.900 <0.750 374
09/06/12 <0.13 <0.13 <0.15 <0.30 130 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR
08/23/13 <0.10 <0.10 <0.10 <0.22 35.8 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR
03/03/16 <0.13 <0.13 <0.13 <0.31 6.8 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
08/11/10 2.23 J <0.950 <0.750 <1.10 1,250 <2.50 <0.900 <0.700 <0.950 <0.750 <1.00 <1.10 <0.900 <0.750 3.70
09/06/12 <0.13 <0.13 <0.15 <0.30 4.6 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR
08/22/13 <0.10 <0.10 <0.10 <0.22 0.13 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR
08/11/10 <0.700 <0.950 <0.750 <1.10 530 <2.50 <0.900 <0.700 <0.950 <0.750 <1.00 <1.10 <0.900 <0.750 54.2
09/06/12 <0.13 <0.13 <0.15 <0.30 308 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR
08/22/13 0.11 J 0.16 J <0.10 <0.22 169 0.24 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR
08/11/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 0.154 J 129
09/06/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR
08/23/13 <0.10 <0.10 0.11 J <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR
MW-38
MW-40
MW-41
MW-42
MW-43
MW-39
MWD-37
Page 9 of 11
Date: 04/18/22
EPA
Method
6010B
Well
ID
Date
Collected
1 600 600 500 20 6 70 70 70 70 25 70 400 400 15
5,000 260,000 80,000 50,000 20,000 6,000 5,900 8,800 14,750 30,500 11,700 26,100 28,500 24,100 15,000GCL (µg/l)p-Isopropyltoluenen-Propylbenzene1,3,5-Trimethylbenzene2L Standard (µg/l)Naphthalenen-Butylbenzenesec-Butylbenzenetert-ButylbenzeneTABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
HAK'S STORE (INCIDENT NO. 13273)
Facility ID # : 00-0-0000006287
Analytical Method
→EPA Method 6200B
Contaminant of Concern
→BenzeneTolueneEthylbenzeneXylenesMTBE1,2,4-TrimethylbenzeneLeadIsopropylbenzene08/11/10 <0.140 <0.190 <0.150 0.569 J 0.967 J <0.500 <0.180 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 0.337 J 81.3
09/06/12 <0.13 <0.13 <0.15 <0.30 0.39 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR
08/23/13 <0.10 <0.10 <0.10 <0.22 0.47 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR
08/11/10 <0.700 <0.950 <0.750 <1.10 455 <2.50 <0.900 <0.700 <0.950 <0.750 <1.00 <1.10 <0.900 0.875 J 90.0
09/06/12 <0.13 <0.13 <0.15 <0.30 124 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR
08/23/13 <0.10 <0.10 <0.10 <0.22 127 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR
08/11/10 <0.140 <0.190 <0.150 0.330 J 0.474 J <0.500 <0.180 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 0.259 J 2.89
09/06/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR
09/06/12 <0.13 0.20 J <0.15 <0.30 0.32 J <0.10 <0.10 <0.10 <0.10 <0.10 0.49 J <0.11 <0.10 <0.10 NR
08/22/13 <0.10 <0.10 <0.10 <0.22 21.6 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR
03/03/16 <0.13 <0.13 <0.13 <0.31 5.1 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
09/06/12 <0.13 32.3 0.29 J <0.30 3.8 <0.10 <0.10 <0.10 <0.10 <0.10 1.5 <0.11 <0.10 <0.10 NR
08/22/13 <0.10 <0.10 <0.10 <0.22 2.0 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR
03/03/16 <0.13 <0.13 <0.13 <0.31 4.1 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
09/06/12 <0.13 33.2 0.87 <0.30 0.18 J <0.10 <0.10 <0.10 <0.10 <0.10 75.6 0.30 J <0.10 <0.10 NR
08/22/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR
09/06/12 <0.13 1.4 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 0.27 J <0.11 <0.10 <0.10 NR
08/22/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR
09/06/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR
08/22/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR
09/06/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR
08/22/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR
09/07/12 2.8 J 52.7 409 1,770 <2.6 105 2.7 J 3.0 J <2.0 22.6 <2.0 65.1 115 571 NR
08/22/13 3.4 13.2 124 527 <0.10 35.8 1.3 1.6 <0.10 11.0 0.63 28.8 26.2 105 NR
03/07/07 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
08/09/07 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/07/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00
08/09/07 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
09/24/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 <0.150 <1.50
08/12/10 <0.140 <0.500 <0.150 <0.220 <0.250 <0.500 <0.500 <0.140 <0.190 <0.150 <0.200 <0.220 <0.180 <0.150 49.9
09/07/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR
OW-1 08/22/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR
08/23/13 19.8 J 467 2,140 10,400 <10 505 39.4 J 32.3 J <10 211 17.3 J 721 1,070 4,050 NR
03/03/16 <3.1 93.0 1,350 6,380 <3.1 485 73.5 46.6 <3.1 197 23.2 626 919 3,490 NR
OW-3 08/23/13 870 10,800 3,620 19,000 <25 528 <25 <25 <25 159 <25 488 758 3,320 NR
OW-2
PWS-2
MW-44
MW-45
MW-46
MW-47
MW-48
MW-49
MW-50
MW-51
MW-52
RW-1
PWS-1
Page 10 of 11
Date: 04/18/22
EPA
Method
6010B
Well
ID
Date
Collected
1 600 600 500 20 6 70 70 70 70 25 70 400 400 15
5,000 260,000 80,000 50,000 20,000 6,000 5,900 8,800 14,750 30,500 11,700 26,100 28,500 24,100 15,000GCL (µg/l)p-Isopropyltoluenen-Propylbenzene1,3,5-Trimethylbenzene2L Standard (µg/l)Naphthalenen-Butylbenzenesec-Butylbenzenetert-ButylbenzeneTABLE 6
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
HAK'S STORE (INCIDENT NO. 13273)
Facility ID # : 00-0-0000006287
Analytical Method
→EPA Method 6200B
Contaminant of Concern
→BenzeneTolueneEthylbenzeneXylenesMTBE1,2,4-TrimethylbenzeneLeadIsopropylbenzene08/23/13 1,780 20,500 4,820 27,600 754 881 <50 <50 <50 201 J <50 577 964 4,170 NR
03/03/16 842 22,400 13,000 67,800 200 4,920 1,220 597 <31 1,600 288 6,120 9,850 27,100 NR
03/17/22 1,220 J 6,170 2,850 15,500 1,700 417 J <310 <310 <310 143 <310 379 J 1,210 J 3,450 NR
08/23/13 4,240 40,600 3,990 24,700 199 J 697 <50 <50 <50 167 J <50 456 835 3,640 NR
03/03/16 4,310 51,000 6,250 29,700 208 1,910 227 130 <25 430 59.2 J 1,460 2,480 9,340 NR
02/28/17 1,780 43,500 7,520 41,700 <130 1,830 367 J 175 J <130 460 J <130 1,830 3,550 14,000 NR
10/31/17 767 24,600 4,210 22,000 42.8 J 770 <13 26.4 J <13 202 <13 571 1,130 4,820 NR
09/10/18 1,110 29,600 3,940 22,000 <63 763 <63 <63 <63 212 J <63 571 1,100 4,630 NR
02/18/19 767 23,700 3,190 18,300 <63 616 <63 <63 <63 172 J <63 432 915 3,640 NR
03/17/22 455 19,300 2,060 J 20,800 <1,300 835 <1,300 <1,300 <1,300 175 J <1,300 479 995 3,900 NR
OW-6 08/22/13 5.2 <0.10 <0.10 <0.22 0.38 J <0.15 <0.10 0.27 J <0.10 0.28 J <0.10 0.17 J <0.10 <0.10 NR
08/22/13 1.8 50.2 55.0 348 <0.10 15.0 14.7 9.6 <0.10 15.1 4.0 68.4 92.1 95.0 NR
03/03/16 <0.13 0.86 0.71 6.0 <0.13 0.46 J <0.13 <0.13 <0.13 0.13 J <0.13 0.17 J 0.52 1.5 NR
Notes:
• NE: Not established.
• FP : Free product.
• NF : Not found.
• DRY: Monitoring well was either dry or did not yield a sufficient volume of water for analysis.
• NS: Not sampled.
• J: Estimated value.
• Concentrations of o-chlorotoluene (332 J µg/l in MW-14), o-dichlorobenzene (658 J µg/l in MW-5 and 364 J µg/l in OW-4) and o-dichlorobenzene
(10,200 µg/l in MW-14) that exceeded the 2L Standard were reported in the ground water samples collected on 03/17/22
• For other contaminant concentrations that did not exceed the MACs, please refer to the laboratory report.
• GCL : Gross contamination level as specified in T15A NCAC 2L.0202.
• Concentrations in bold face type exceeded the 2L standard as specified in T15A NCAC 2L.0202; Concentrations in italics exceeded the GCLs.
• < : Less than the method detection limit specified in the laboratory report.
AS-1
• Results reported in µg/L.
• 2L Standard : Maximum allowable concentrations as specified in T15A NCAC 2L.0202.
OW-4
OW-5
Page 11 of 11

APPENDICES

APPENDIX A
State Correspondence
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GHWHUPLQHG WR EH DQ HPHUJHQF UHSRQH RU DRFLDWHG LW ULN DHPHQW LH WH /LPLWHG 6LWH
2266 Received FEB 19 2021
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2266 Received FEB 25 2022

APPENDIX B
Laboratory Report – Ground Water Samples
04/08/22
Technical Report for
GRI (Geological Resources Inc.)
Haks' Store; 901 Washington St, Plymouth, NC
2266
SGS Job Number: FA94049
Sampling Date: 03/17/22
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28207
[e-mail]; [e-mail];
[e-mail]; [e-mail]
ATTN: Justin Radford
Total number of pages in report:
Certifications: FL(E83510), LA(03051), KS(E-10327), NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AL, AK, AR, CT, IA, KY, MA, MI. MS, ND, NH, NV, OK, OR, IL, UT, VT, WA, WI, WV
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone]
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Norm Farmer
Technical Director
Orlando, FL 04/08/22
e-Hardcopy 2.0
Automated Report
57
SGS is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
Review standard terms at: http://www.sgs.com/en/terms-and-conditions
The results set forth herein are provided by SGS North America Inc.
Please share your ideas about
how we can serve you better at:
[e-mail]
1 of 57
FA94049
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................5
Section 3: Sample Results ........................................................................................................9
3.1: FA94049-1: MW-37 ......................................................................................................10
3.2: FA94049-2: MW-1 ........................................................................................................12
3.3: FA94049-3: MW-2 ........................................................................................................14
3.4: FA94049-4: MW-3 ........................................................................................................16
3.5: FA94049-5: MWD-4 .....................................................................................................18
3.6: FA94049-6: MW-5 ........................................................................................................20
3.7: FA94049-7: OW-4 ........................................................................................................23
3.8: FA94049-8: OW-5 ........................................................................................................26
3.9: FA94049-9: MW-24 ......................................................................................................29
3.10: FA94049-10: MW-39 ..................................................................................................31
3.11: FA94049-11: MW-11 ..................................................................................................33
3.12: FA94049-12: MW-14 ..................................................................................................36
3.13: FA94049-13: MW-15 ..................................................................................................39
Section 4: Misc. Forms ............................................................................................................41
4.1: Chain of Custody ...........................................................................................................42
Section 5: MS Volatiles - QC Data Summaries .....................................................................45
5.1: Method Blank Summary ................................................................................................46
5.2: Blank Spike Summary ...................................................................................................50
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................54 123452 of 57
FA94049
SGS North America Inc.
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA94049
Haks' Store; 901 Washington St, Plymouth, NC
Project No: 2266
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
This report contains results reported as ND = Not detected. The following applies:
Organics ND = Not detected above the MDL
FA94049-1 03/17/22 10:37 JB 03/18/22 AQ Ground Water MW-37
FA94049-2 03/17/22 10:46 JB 03/18/22 AQ Ground Water MW-1
FA94049-3 03/17/22 10:58 JB 03/18/22 AQ Ground Water MW-2
FA94049-4 03/17/22 11:09 JB 03/18/22 AQ Ground Water MW-3
FA94049-5 03/17/22 11:25 JB 03/18/22 AQ Ground Water MWD-4
FA94049-6 03/17/22 11:36 JB 03/18/22 AQ Ground Water MW-5
FA94049-7 03/17/22 11:41 JB 03/18/22 AQ Ground Water OW-4
FA94049-8 03/17/22 11:52 JB 03/18/22 AQ Ground Water OW-5
FA94049-9 03/17/22 12:13 JB 03/18/22 AQ Ground Water MW-24
FA94049-10 03/17/22 12:27 JB 03/18/22 AQ Ground Water MW-39
FA94049-11 03/17/22 12:43 JB 03/18/22 AQ Ground Water MW-11
FA94049-12 03/17/22 12:57 JB 03/18/22 AQ Ground Water MW-14
3 of 57
FA940491
SGS North America Inc.
Sample Summary
(continued)
GRI (Geological Resources Inc.)
Job No:FA94049
Haks' Store; 901 Washington St, Plymouth, NC
Project No: 2266
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA94049-13 03/17/22 13:06 JB 03/18/22 AQ Ground Water MW-15
4 of 57
FA940491
Summary of Hits Page 1 of 4
Job Number:FA94049
Account:GRI (Geological Resources Inc.)
Project:Haks' Store; 901 Washington St, Plymouth, NC
Collected:03/17/22
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA94049-1 MW-37
Benzene 0.14 J 0.50 0.13 ug/l SM 6200B
Ethylbenzene 0.52 0.50 0.13 ug/l SM 6200B
Methyl Tert Butyl Ether 0.21 J 0.50 0.13 ug/l SM 6200B
Naphthalene 0.17 J 0.50 0.13 ug/l SM 6200B
Toluene 3.5 0.50 0.13 ug/l SM 6200B
1,2,4-Trimethylbenzene 0.52 0.50 0.13 ug/l SM 6200B
1,3,5-Trimethylbenzene 0.22 J 0.50 0.13 ug/l SM 6200B
m,p-Xylene 1.9 1.0 0.13 ug/l SM 6200B
o-Xylene 0.90 0.50 0.13 ug/l SM 6200B
Xylene (total)2.8 1.5 0.25 ug/l SM 6200B
FA94049-2 MW-1
Benzene a 26.2 J 50 13 ug/l SM 6200B
n-Butylbenzene a 19.7 J 50 13 ug/l SM 6200B
sec-Butylbenzene a 23.0 J 50 13 ug/l SM 6200B
Ethylbenzene 2560 2500 630 ug/l SM 6200B
Isopropylbenzene a 125 50 13 ug/l SM 6200B
Naphthalene a 645 50 13 ug/l SM 6200B
n-Propylbenzene a 354 50 13 ug/l SM 6200B
Styrene a 17.7 J 50 13 ug/l SM 6200B
Toluene 7770 2500 630 ug/l SM 6200B
1,2,4-Trimethylbenzene 2670 2500 630 ug/l SM 6200B
1,3,5-Trimethylbenzene 1140 J 2500 630 ug/l SM 6200B
m,p-Xylene 12200 5000 630 ug/l SM 6200B
o-Xylene 6080 2500 630 ug/l SM 6200B
Xylene (total)18300 7500 1300 ug/l SM 6200B
FA94049-3 MW-2
n-Butylbenzene 35.0 J 130 31 ug/l SM 6200B
sec-Butylbenzene 41.7 J 130 31 ug/l SM 6200B
o-Chlorotoluene b 97.3 J 130 31 ug/l SM 6200B
Ethylbenzene 119 J 130 31 ug/l SM 6200B
Isopropylbenzene 96.2 J 130 31 ug/l SM 6200B
Naphthalene 103 J 130 31 ug/l SM 6200B
n-Propylbenzene 465 130 31 ug/l SM 6200B
1,2,4-Trimethylbenzene 2720 130 31 ug/l SM 6200B
1,3,5-Trimethylbenzene 824 130 31 ug/l SM 6200B
m,p-Xylene 334 250 31 ug/l SM 6200B
Xylene (total)334 J 380 63 ug/l SM 6200B
5 of 57
FA940492
Summary of Hits Page 2 of 4
Job Number:FA94049
Account:GRI (Geological Resources Inc.)
Project:Haks' Store; 901 Washington St, Plymouth, NC
Collected:03/17/22
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA94049-4 MW-3
No hits reported in this sample.
FA94049-5 MWD-4
No hits reported in this sample.
FA94049-6 MW-5
Benzene a 448 250 63 ug/l SM 6200B
1,2-Dichlorobenzene b 658 J 2500 630 ug/l SM 6200B
Ethylbenzene 4400 2500 630 ug/l SM 6200B
Isopropylbenzene a 115 J 250 63 ug/l SM 6200B
Methyl Tert Butyl Ether a 525 250 63 ug/l SM 6200B
Naphthalene 742 J 2500 630 ug/l SM 6200B
n-Propylbenzene a 293 250 63 ug/l SM 6200B
Toluene 16900 2500 630 ug/l SM 6200B
1,2,4-Trimethylbenzene 4410 2500 630 ug/l SM 6200B
1,3,5-Trimethylbenzene 1660 J 2500 630 ug/l SM 6200B
m,p-Xylene 21600 5000 630 ug/l SM 6200B
o-Xylene 9830 2500 630 ug/l SM 6200B
Xylene (total)31400 7500 1300 ug/l SM 6200B
FA94049-7 OW-4
Benzene 1220 J 1300 310 ug/l SM 6200B
1,2-Dichlorobenzene b 364 J 1300 310 ug/l SM 6200B
Ethylbenzene 2850 1300 310 ug/l SM 6200B
Isopropylbenzene a 143 130 31 ug/l SM 6200B
Methyl Tert Butyl Ether 1700 1300 310 ug/l SM 6200B
Naphthalene 417 J 1300 310 ug/l SM 6200B
n-Propylbenzene 379 J 1300 310 ug/l SM 6200B
Toluene 6170 1300 310 ug/l SM 6200B
1,2,4-Trimethylbenzene 3450 1300 310 ug/l SM 6200B
1,3,5-Trimethylbenzene 1210 J 1300 310 ug/l SM 6200B
m,p-Xylene 11200 2500 310 ug/l SM 6200B
o-Xylene 4310 1300 310 ug/l SM 6200B
Xylene (total)15500 3800 630 ug/l SM 6200B
FA94049-8 OW-5
Benzene c 455 250 63 ug/l SM 6200B
Ethylbenzene 2060 J 5000 1300 ug/l SM 6200B
Isopropylbenzene a 175 J 250 63 ug/l SM 6200B
6 of 57
FA940492
Summary of Hits Page 3 of 4
Job Number:FA94049
Account:GRI (Geological Resources Inc.)
Project:Haks' Store; 901 Washington St, Plymouth, NC
Collected:03/17/22
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
Naphthalene c 835 250 63 ug/l SM 6200B
n-Propylbenzene c 479 250 63 ug/l SM 6200B
Toluene 19300 5000 1300 ug/l SM 6200B
1,2,4-Trimethylbenzene c 3900 250 63 ug/l SM 6200B
1,3,5-Trimethylbenzene c 995 250 63 ug/l SM 6200B
m,p-Xylene c 14000 500 63 ug/l SM 6200B
o-Xylene c 6780 250 63 ug/l SM 6200B
Xylene (total) c 20800 750 130 ug/l SM 6200B
FA94049-9 MW-24
Benzene 2.7 J 5.0 1.3 ug/l SM 6200B
sec-Butylbenzene a 0.21 J 0.50 0.13 ug/l SM 6200B
Di-Isopropyl Ether a 0.13 J 0.50 0.13 ug/l SM 6200B
Ethylbenzene a 0.19 J 0.50 0.13 ug/l SM 6200B
Isopropylbenzene a 0.19 J 0.50 0.13 ug/l SM 6200B
p-Isopropyltoluene a 0.69 0.50 0.13 ug/l SM 6200B
Methyl Tert Butyl Ether 20.3 5.0 1.3 ug/l SM 6200B
Naphthalene a 0.41 J 0.50 0.13 ug/l SM 6200B
Toluene a 0.65 0.50 0.13 ug/l SM 6200B
1,3,5-Trimethylbenzene a 0.13 J 0.50 0.13 ug/l SM 6200B
m,p-Xylene a 2.0 1.0 0.13 ug/l SM 6200B
o-Xylene a 2.7 0.50 0.13 ug/l SM 6200B
Xylene (total) a 4.7 1.5 0.25 ug/l SM 6200B
FA94049-10 MW-39
Di-Isopropyl Ether 0.78 J 1.0 0.25 ug/l SM 6200B
Methylene Chloride b 3.2 JB 4.0 2.0 ug/l SM 6200B
Methyl Tert Butyl Ether 4.5 1.0 0.25 ug/l SM 6200B
FA94049-11 MW-11
Benzene a 1.3 1.3 0.31 ug/l SM 6200B
sec-Butylbenzene a 0.54 J 1.3 0.31 ug/l SM 6200B
Ethylbenzene a 1.4 1.3 0.31 ug/l SM 6200B
Methylene Chloride b 51.7 JB 100 50 ug/l SM 6200B
Methyl Tert Butyl Ether 104 25 6.3 ug/l SM 6200B
Toluene a 1.4 1.3 0.31 ug/l SM 6200B
1,2,4-Trimethylbenzene a 0.65 J 1.3 0.31 ug/l SM 6200B
m,p-Xylene a 0.96 J 2.5 0.31 ug/l SM 6200B
o-Xylene a 0.79 J 1.3 0.31 ug/l SM 6200B
Xylene (total) a 1.8 J 3.8 0.63 ug/l SM 6200B
7 of 57
FA940492
Summary of Hits Page 4 of 4
Job Number:FA94049
Account:GRI (Geological Resources Inc.)
Project:Haks' Store; 901 Washington St, Plymouth, NC
Collected:03/17/22
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA94049-12 MW-14
Benzene 2130 J 5000 1300 ug/l SM 6200B
o-Chlorotoluene a 332 J 500 130 ug/l SM 6200B
Ethylbenzene 2780 J 5000 1300 ug/l SM 6200B
Isopropylbenzene a 136 J 500 130 ug/l SM 6200B
Methyl Tert Butyl Ether a 273 J 500 130 ug/l SM 6200B
Naphthalene a 739 500 130 ug/l SM 6200B
n-Propylbenzene a 367 J 500 130 ug/l SM 6200B
Toluene 35600 5000 1300 ug/l SM 6200B
1,2,4-Trimethylbenzene a 2920 500 130 ug/l SM 6200B
1,3,5-Trimethylbenzene a 817 500 130 ug/l SM 6200B
m,p-Xylene a 12800 1000 130 ug/l SM 6200B
o-Xylene a 6410 500 130 ug/l SM 6200B
Xylene (total) a 19200 1500 250 ug/l SM 6200B
FA94049-13 MW-15
Methylene Chloride b 10.1 JB 20 10 ug/l SM 6200B
(a) Sample re-analyzed beyond hold time; reported results are considered minimum values.
(b) Confirmed ND by reanalysis beyond hold-time.
(c) Sample re-analyzed beyond hold time; reported results are considered minimum values. Results from different
vials are not consistent; higher results were reported.
8 of 57
FA940492
SGS North America Inc.
Sample Results
Report of Analysis
Orlando, FL
Section 3
9 of 57
FA940493
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-37
Lab Sample ID:FA94049-1 Date Sampled:03/17/22
Matrix:AQ - Ground Water Date Received:03/18/22
Method:SM 6200B Percent Solids:n/a
Project:Haks' Store; 901 Washington St, Plymouth, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0231264.D 1 03/28/22 17:20 SS n/a n/a VA3097
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 0.14 0.50 0.13 ug/l J
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 57
FA9404933.1
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-37
Lab Sample ID:FA94049-1 Date Sampled:03/17/22
Matrix:AQ - Ground Water Date Received:03/18/22
Method:SM 6200B Percent Solids:n/a
Project:Haks' Store; 901 Washington St, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene 0.52 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.21 0.50 0.13 ug/l J
91-20-3 Naphthalene 0.17 0.50 0.13 ug/l J
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene 3.5 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 0.52 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene 0.22 0.50 0.13 ug/l J
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 1.9 1.0 0.13 ug/l
95-47-6 o-Xylene 0.90 0.50 0.13 ug/l
1330-20-7 Xylene (total)2.8 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 103%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 57
FA9404933.1
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-1
Lab Sample ID:FA94049-2 Date Sampled:03/17/22
Matrix:AQ - Ground Water Date Received:03/18/22
Method:SM 6200B Percent Solids:n/a
Project:Haks' Store; 901 Washington St, Plymouth, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a A0231381.D 100 04/04/22 15:55 SS n/a n/a VA3102
Run #2 A0231308.D 5000 03/29/22 21:54 SS n/a n/a VA3098
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 26.2 50 13 ug/l J
108-86-1 Bromobenzene ND b 2500 630 ug/l
74-97-5 Bromochloromethane ND b 2500 630 ug/l
75-27-4 Bromodichloromethane ND b 2500 630 ug/l
75-25-2 Bromoform ND b 2500 630 ug/l
104-51-8 n-Butylbenzene 19.7 50 13 ug/l J
135-98-8 sec-Butylbenzene 23.0 50 13 ug/l J
98-06-6 tert-Butylbenzene ND b 2500 630 ug/l
56-23-5 Carbon Tetrachloride ND b 2500 630 ug/l
108-90-7 Chlorobenzene ND b 2500 630 ug/l
75-00-3 Chloroethane ND b 2500 1000 ug/l
67-66-3 Chloroform ND b 2500 630 ug/l
95-49-8 o-Chlorotoluene ND b 2500 630 ug/l
106-43-4 p-Chlorotoluene ND b 2500 630 ug/l
124-48-1 Dibromochloromethane ND b 2500 630 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND b 2500 1200 ug/l
106-93-4 1,2-Dibromoethane ND b 2500 630 ug/l
75-71-8 Dichlorodifluoromethane ND b 2500 1000 ug/l
95-50-1 1,2-Dichlorobenzene ND b 2500 630 ug/l
541-73-1 1,3-Dichlorobenzene ND b 2500 630 ug/l
106-46-7 1,4-Dichlorobenzene ND b 2500 630 ug/l
75-34-3 1,1-Dichloroethane ND b 2500 630 ug/l
107-06-2 1,2-Dichloroethane ND b 2500 630 ug/l
75-35-4 1,1-Dichloroethylene ND b 2500 630 ug/l
156-59-2 cis-1,2-Dichloroethylene ND b 2500 630 ug/l
156-60-5 trans-1,2-Dichloroethylene ND b 2500 630 ug/l
78-87-5 1,2-Dichloropropane ND b 2500 630 ug/l
142-28-9 1,3-Dichloropropane ND b 2500 630 ug/l
594-20-7 2,2-Dichloropropane ND b 2500 630 ug/l
563-58-6 1,1-Dichloropropene ND b 2500 630 ug/l
10061-01-5 cis-1,3-Dichloropropene ND b 2500 630 ug/l
10061-02-6 trans-1,3-Dichloropropene ND b 2500 630 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 57
FA9404933.2
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-1
Lab Sample ID:FA94049-2 Date Sampled:03/17/22
Matrix:AQ - Ground Water Date Received:03/18/22
Method:SM 6200B Percent Solids:n/a
Project:Haks' Store; 901 Washington St, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND b 2500 630 ug/l
100-41-4 Ethylbenzene 2560 b 2500 630 ug/l
87-68-3 Hexachlorobutadiene ND b 2500 630 ug/l
98-82-8 Isopropylbenzene 125 50 13 ug/l
99-87-6 p-Isopropyltoluene ND b 2500 630 ug/l
74-83-9 Methyl Bromide ND b 2500 1000 ug/l
74-87-3 Methyl Chloride ND b 2500 1000 ug/l
74-95-3 Methylene Bromide ND b 2500 630 ug/l
75-09-2 Methylene Chloride ND b 10000 5000 ug/l
1634-04-4 Methyl Tert Butyl Ether ND b 2500 630 ug/l
91-20-3 Naphthalene 645 50 13 ug/l
103-65-1 n-Propylbenzene 354 50 13 ug/l
100-42-5 Styrene 17.7 50 13 ug/l J
630-20-6 1,1,1,2-Tetrachloroethane ND b 2500 630 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND b 2500 630 ug/l
127-18-4 Tetrachloroethylene ND b 2500 630 ug/l
108-88-3 Toluene 7770 b 2500 630 ug/l
87-61-6 1,2,3-Trichlorobenzene ND b 2500 630 ug/l
120-82-1 1,2,4-Trichlorobenzene ND b 2500 630 ug/l
71-55-6 1,1,1-Trichloroethane ND b 2500 630 ug/l
79-00-5 1,1,2-Trichloroethane ND b 2500 630 ug/l
79-01-6 Trichloroethylene ND b 2500 630 ug/l
75-69-4 Trichlorofluoromethane ND b 2500 1000 ug/l
96-18-4 1,2,3-Trichloropropane ND b 2500 630 ug/l
95-63-6 1,2,4-Trimethylbenzene 2670 b 2500 630 ug/l
108-67-8 1,3,5-Trimethylbenzene 1140 b 2500 630 ug/l J
75-01-4 Vinyl Chloride ND b 2500 630 ug/l
m,p-Xylene 12200 b 5000 630 ug/l
95-47-6 o-Xylene 6080 b 2500 630 ug/l
1330-20-7 Xylene (total)18300 b 7500 1300 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 98%104%70-130%
17060-07-0 1,2-Dichloroethane-D4 98%108%70-130%
2037-26-5 Toluene-D8 99%101%70-130%
460-00-4 4-Bromofluorobenzene 97%104%70-130%
(a) Sample re-analyzed beyond hold time; reported results are considered minimum values.
(b) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
13 of 57
FA9404933.2
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-2
Lab Sample ID:FA94049-3 Date Sampled:03/17/22
Matrix:AQ - Ground Water Date Received:03/18/22
Method:SM 6200B Percent Solids:n/a
Project:Haks' Store; 901 Washington St, Plymouth, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0231306.D 250 03/29/22 21:08 SS n/a n/a VA3098
Run #2 a A0231385.D 100 04/04/22 17:27 SS n/a n/a VA3102
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 130 31 ug/l
108-86-1 Bromobenzene ND 130 31 ug/l
74-97-5 Bromochloromethane ND 130 31 ug/l
75-27-4 Bromodichloromethane ND 130 31 ug/l
75-25-2 Bromoform ND 130 31 ug/l
104-51-8 n-Butylbenzene 35.0 130 31 ug/l J
135-98-8 sec-Butylbenzene 41.7 130 31 ug/l J
98-06-6 tert-Butylbenzene ND 130 31 ug/l
56-23-5 Carbon Tetrachloride ND 130 31 ug/l
108-90-7 Chlorobenzene ND 130 31 ug/l
75-00-3 Chloroethane ND 130 50 ug/l
67-66-3 Chloroform ND 130 31 ug/l
95-49-8 o-Chlorotoluene b 97.3 130 31 ug/l J
106-43-4 p-Chlorotoluene ND 130 31 ug/l
124-48-1 Dibromochloromethane ND 130 31 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 130 62 ug/l
106-93-4 1,2-Dibromoethane ND 130 31 ug/l
75-71-8 Dichlorodifluoromethane ND 130 50 ug/l
95-50-1 1,2-Dichlorobenzene ND 130 31 ug/l
541-73-1 1,3-Dichlorobenzene ND 130 31 ug/l
106-46-7 1,4-Dichlorobenzene ND 130 31 ug/l
75-34-3 1,1-Dichloroethane ND 130 31 ug/l
107-06-2 1,2-Dichloroethane ND 130 31 ug/l
75-35-4 1,1-Dichloroethylene ND 130 31 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 130 31 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 130 31 ug/l
78-87-5 1,2-Dichloropropane ND 130 31 ug/l
142-28-9 1,3-Dichloropropane ND 130 31 ug/l
594-20-7 2,2-Dichloropropane ND 130 31 ug/l
563-58-6 1,1-Dichloropropene ND 130 31 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 130 31 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 130 31 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
14 of 57
FA9404933.3
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-2
Lab Sample ID:FA94049-3 Date Sampled:03/17/22
Matrix:AQ - Ground Water Date Received:03/18/22
Method:SM 6200B Percent Solids:n/a
Project:Haks' Store; 901 Washington St, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 130 31 ug/l
100-41-4 Ethylbenzene 119 130 31 ug/l J
87-68-3 Hexachlorobutadiene ND 130 31 ug/l
98-82-8 Isopropylbenzene 96.2 130 31 ug/l J
99-87-6 p-Isopropyltoluene ND 130 31 ug/l
74-83-9 Methyl Bromide ND 130 50 ug/l
74-87-3 Methyl Chloride ND 130 50 ug/l
74-95-3 Methylene Bromide ND 130 31 ug/l
75-09-2 Methylene Chloride ND 500 250 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 130 31 ug/l
91-20-3 Naphthalene 103 130 31 ug/l J
103-65-1 n-Propylbenzene 465 130 31 ug/l
100-42-5 Styrene ND 130 31 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 130 31 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 130 31 ug/l
127-18-4 Tetrachloroethylene ND 130 31 ug/l
108-88-3 Toluene ND 130 31 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 130 31 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 130 31 ug/l
71-55-6 1,1,1-Trichloroethane ND 130 31 ug/l
79-00-5 1,1,2-Trichloroethane ND 130 31 ug/l
79-01-6 Trichloroethylene ND 130 31 ug/l
75-69-4 Trichlorofluoromethane ND 130 50 ug/l
96-18-4 1,2,3-Trichloropropane ND 130 31 ug/l
95-63-6 1,2,4-Trimethylbenzene 2720 130 31 ug/l
108-67-8 1,3,5-Trimethylbenzene 824 130 31 ug/l
75-01-4 Vinyl Chloride ND 130 31 ug/l
m,p-Xylene 334 250 31 ug/l
95-47-6 o-Xylene ND 130 31 ug/l
1330-20-7 Xylene (total)334 380 63 ug/l J
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 99%98%70-130%
17060-07-0 1,2-Dichloroethane-D4 107%100%70-130%
2037-26-5 Toluene-D8 101%100%70-130%
460-00-4 4-Bromofluorobenzene 98%94%70-130%
(a) Confirmation run beyond holdtime.
(b) Confirmed ND by reanalysis beyond hold-time.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
15 of 57
FA9404933.3
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-3
Lab Sample ID:FA94049-4 Date Sampled:03/17/22
Matrix:AQ - Ground Water Date Received:03/18/22
Method:SM 6200B Percent Solids:n/a
Project:Haks' Store; 901 Washington St, Plymouth, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0231290.D 1 03/29/22 14:58 SS n/a n/a VA3098
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
16 of 57
FA9404933.4
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-3
Lab Sample ID:FA94049-4 Date Sampled:03/17/22
Matrix:AQ - Ground Water Date Received:03/18/22
Method:SM 6200B Percent Solids:n/a
Project:Haks' Store; 901 Washington St, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
2037-26-5 Toluene-D8 91%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
17 of 57
FA9404933.4
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MWD-4
Lab Sample ID:FA94049-5 Date Sampled:03/17/22
Matrix:AQ - Ground Water Date Received:03/18/22
Method:SM 6200B Percent Solids:n/a
Project:Haks' Store; 901 Washington St, Plymouth, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0231291.D 1 03/29/22 15:21 SS n/a n/a VA3098
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
18 of 57
FA9404933.5
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MWD-4
Lab Sample ID:FA94049-5 Date Sampled:03/17/22
Matrix:AQ - Ground Water Date Received:03/18/22
Method:SM 6200B Percent Solids:n/a
Project:Haks' Store; 901 Washington St, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 105%70-130%
2037-26-5 Toluene-D8 85%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
19 of 57
FA9404933.5
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW-5
Lab Sample ID:FA94049-6 Date Sampled:03/17/22
Matrix:AQ - Ground Water Date Received:03/18/22
Method:SM 6200B Percent Solids:n/a
Project:Haks' Store; 901 Washington St, Plymouth, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a A0231394.D 500 04/04/22 20:53 SS n/a n/a VA3102
Run #2 A0231309.D 5000 03/29/22 22:17 SS n/a n/a VA3098
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 448 250 63 ug/l
108-86-1 Bromobenzene ND b 2500 630 ug/l
74-97-5 Bromochloromethane ND b 2500 630 ug/l
75-27-4 Bromodichloromethane ND b 2500 630 ug/l
75-25-2 Bromoform ND b 2500 630 ug/l
104-51-8 n-Butylbenzene ND b 2500 630 ug/l
135-98-8 sec-Butylbenzene ND b 2500 630 ug/l
98-06-6 tert-Butylbenzene ND b 2500 630 ug/l
56-23-5 Carbon Tetrachloride ND b 2500 630 ug/l
108-90-7 Chlorobenzene ND b 2500 630 ug/l
75-00-3 Chloroethane ND b 2500 1000 ug/l
67-66-3 Chloroform ND b 2500 630 ug/l
95-49-8 o-Chlorotoluene ND b 2500 630 ug/l
106-43-4 p-Chlorotoluene ND b 2500 630 ug/l
124-48-1 Dibromochloromethane ND b 2500 630 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND b 2500 1200 ug/l
106-93-4 1,2-Dibromoethane ND b 2500 630 ug/l
75-71-8 Dichlorodifluoromethane ND b 2500 1000 ug/l
95-50-1 1,2-Dichlorobenzene c 658 b 2500 630 ug/l J
541-73-1 1,3-Dichlorobenzene ND b 2500 630 ug/l
106-46-7 1,4-Dichlorobenzene ND b 2500 630 ug/l
75-34-3 1,1-Dichloroethane ND b 2500 630 ug/l
107-06-2 1,2-Dichloroethane ND b 2500 630 ug/l
75-35-4 1,1-Dichloroethylene ND b 2500 630 ug/l
156-59-2 cis-1,2-Dichloroethylene ND b 2500 630 ug/l
156-60-5 trans-1,2-Dichloroethylene ND b 2500 630 ug/l
78-87-5 1,2-Dichloropropane ND b 2500 630 ug/l
142-28-9 1,3-Dichloropropane ND b 2500 630 ug/l
594-20-7 2,2-Dichloropropane ND b 2500 630 ug/l
563-58-6 1,1-Dichloropropene ND b 2500 630 ug/l
10061-01-5 cis-1,3-Dichloropropene ND b 2500 630 ug/l
10061-02-6 trans-1,3-Dichloropropene ND b 2500 630 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
20 of 57
FA9404933.6
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW-5
Lab Sample ID:FA94049-6 Date Sampled:03/17/22
Matrix:AQ - Ground Water Date Received:03/18/22
Method:SM 6200B Percent Solids:n/a
Project:Haks' Store; 901 Washington St, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND b 2500 630 ug/l
100-41-4 Ethylbenzene 4400 b 2500 630 ug/l
87-68-3 Hexachlorobutadiene ND b 2500 630 ug/l
98-82-8 Isopropylbenzene 115 250 63 ug/l J
99-87-6 p-Isopropyltoluene ND b 2500 630 ug/l
74-83-9 Methyl Bromide ND b 2500 1000 ug/l
74-87-3 Methyl Chloride ND b 2500 1000 ug/l
74-95-3 Methylene Bromide ND b 2500 630 ug/l
75-09-2 Methylene Chloride ND b 10000 5000 ug/l
1634-04-4 Methyl Tert Butyl Ether 525 250 63 ug/l
91-20-3 Naphthalene 742 b 2500 630 ug/l J
103-65-1 n-Propylbenzene 293 250 63 ug/l
100-42-5 Styrene ND b 2500 630 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND b 2500 630 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND b 2500 630 ug/l
127-18-4 Tetrachloroethylene ND b 2500 630 ug/l
108-88-3 Toluene 16900 b 2500 630 ug/l
87-61-6 1,2,3-Trichlorobenzene ND b 2500 630 ug/l
120-82-1 1,2,4-Trichlorobenzene ND b 2500 630 ug/l
71-55-6 1,1,1-Trichloroethane ND b 2500 630 ug/l
79-00-5 1,1,2-Trichloroethane ND b 2500 630 ug/l
79-01-6 Trichloroethylene ND b 2500 630 ug/l
75-69-4 Trichlorofluoromethane ND b 2500 1000 ug/l
96-18-4 1,2,3-Trichloropropane ND b 2500 630 ug/l
95-63-6 1,2,4-Trimethylbenzene 4410 b 2500 630 ug/l
108-67-8 1,3,5-Trimethylbenzene 1660 b 2500 630 ug/l J
75-01-4 Vinyl Chloride ND b 2500 630 ug/l
m,p-Xylene 21600 b 5000 630 ug/l
95-47-6 o-Xylene 9830 b 2500 630 ug/l
1330-20-7 Xylene (total)31400 b 7500 1300 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 97%102%70-130%
17060-07-0 1,2-Dichloroethane-D4 98%108%70-130%
2037-26-5 Toluene-D8 99%101%70-130%
460-00-4 4-Bromofluorobenzene 98%102%70-130%
(a) Sample re-analyzed beyond hold time; reported results are considered minimum values.
(b) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
21 of 57
FA9404933.6
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW-5
Lab Sample ID:FA94049-6 Date Sampled:03/17/22
Matrix:AQ - Ground Water Date Received:03/18/22
Method:SM 6200B Percent Solids:n/a
Project:Haks' Store; 901 Washington St, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
(c) Confirmed ND by reanalysis beyond hold-time.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
22 of 57
FA9404933.6
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:OW-4
Lab Sample ID:FA94049-7 Date Sampled:03/17/22
Matrix:AQ - Ground Water Date Received:03/18/22
Method:SM 6200B Percent Solids:n/a
Project:Haks' Store; 901 Washington St, Plymouth, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a A0231386.D 250 04/04/22 17:50 SS n/a n/a VA3102
Run #2 A0231307.D 2500 03/29/22 21:31 SS n/a n/a VA3098
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 1220 b 1300 310 ug/l J
108-86-1 Bromobenzene ND b 1300 310 ug/l
74-97-5 Bromochloromethane ND b 1300 310 ug/l
75-27-4 Bromodichloromethane ND b 1300 310 ug/l
75-25-2 Bromoform ND b 1300 310 ug/l
104-51-8 n-Butylbenzene ND b 1300 310 ug/l
135-98-8 sec-Butylbenzene ND b 1300 310 ug/l
98-06-6 tert-Butylbenzene ND b 1300 310 ug/l
56-23-5 Carbon Tetrachloride ND b 1300 310 ug/l
108-90-7 Chlorobenzene ND b 1300 310 ug/l
75-00-3 Chloroethane ND b 1300 500 ug/l
67-66-3 Chloroform ND b 1300 310 ug/l
95-49-8 o-Chlorotoluene ND b 1300 310 ug/l
106-43-4 p-Chlorotoluene ND b 1300 310 ug/l
124-48-1 Dibromochloromethane ND b 1300 310 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND b 1300 620 ug/l
106-93-4 1,2-Dibromoethane ND b 1300 310 ug/l
75-71-8 Dichlorodifluoromethane ND b 1300 500 ug/l
95-50-1 1,2-Dichlorobenzene c 364 b 1300 310 ug/l J
541-73-1 1,3-Dichlorobenzene ND b 1300 310 ug/l
106-46-7 1,4-Dichlorobenzene ND b 1300 310 ug/l
75-34-3 1,1-Dichloroethane ND b 1300 310 ug/l
107-06-2 1,2-Dichloroethane ND b 1300 310 ug/l
75-35-4 1,1-Dichloroethylene ND b 1300 310 ug/l
156-59-2 cis-1,2-Dichloroethylene ND b 1300 310 ug/l
156-60-5 trans-1,2-Dichloroethylene ND b 1300 310 ug/l
78-87-5 1,2-Dichloropropane ND b 1300 310 ug/l
142-28-9 1,3-Dichloropropane ND b 1300 310 ug/l
594-20-7 2,2-Dichloropropane ND b 1300 310 ug/l
563-58-6 1,1-Dichloropropene ND b 1300 310 ug/l
10061-01-5 cis-1,3-Dichloropropene ND b 1300 310 ug/l
10061-02-6 trans-1,3-Dichloropropene ND b 1300 310 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
23 of 57
FA9404933.7
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:OW-4
Lab Sample ID:FA94049-7 Date Sampled:03/17/22
Matrix:AQ - Ground Water Date Received:03/18/22
Method:SM 6200B Percent Solids:n/a
Project:Haks' Store; 901 Washington St, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND b 1300 310 ug/l
100-41-4 Ethylbenzene 2850 b 1300 310 ug/l
87-68-3 Hexachlorobutadiene ND b 1300 310 ug/l
98-82-8 Isopropylbenzene 143 130 31 ug/l
99-87-6 p-Isopropyltoluene ND b 1300 310 ug/l
74-83-9 Methyl Bromide ND b 1300 500 ug/l
74-87-3 Methyl Chloride ND b 1300 500 ug/l
74-95-3 Methylene Bromide ND b 1300 310 ug/l
75-09-2 Methylene Chloride ND b 5000 2500 ug/l
1634-04-4 Methyl Tert Butyl Ether 1700 b 1300 310 ug/l
91-20-3 Naphthalene 417 b 1300 310 ug/l J
103-65-1 n-Propylbenzene 379 b 1300 310 ug/l J
100-42-5 Styrene ND b 1300 310 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND b 1300 310 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND b 1300 310 ug/l
127-18-4 Tetrachloroethylene ND b 1300 310 ug/l
108-88-3 Toluene 6170 b 1300 310 ug/l
87-61-6 1,2,3-Trichlorobenzene ND b 1300 310 ug/l
120-82-1 1,2,4-Trichlorobenzene ND b 1300 310 ug/l
71-55-6 1,1,1-Trichloroethane ND b 1300 310 ug/l
79-00-5 1,1,2-Trichloroethane ND b 1300 310 ug/l
79-01-6 Trichloroethylene ND b 1300 310 ug/l
75-69-4 Trichlorofluoromethane ND b 1300 500 ug/l
96-18-4 1,2,3-Trichloropropane ND b 1300 310 ug/l
95-63-6 1,2,4-Trimethylbenzene 3450 b 1300 310 ug/l
108-67-8 1,3,5-Trimethylbenzene 1210 b 1300 310 ug/l J
75-01-4 Vinyl Chloride ND b 1300 310 ug/l
m,p-Xylene 11200 b 2500 310 ug/l
95-47-6 o-Xylene 4310 b 1300 310 ug/l
1330-20-7 Xylene (total)15500 b 3800 630 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 99%101%70-130%
17060-07-0 1,2-Dichloroethane-D4 99%107%70-130%
2037-26-5 Toluene-D8 99%101%70-130%
460-00-4 4-Bromofluorobenzene 97%102%70-130%
(a) Sample re-analyzed beyond hold time; reported results are considered minimum values.
(b) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
24 of 57
FA9404933.7
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:OW-4
Lab Sample ID:FA94049-7 Date Sampled:03/17/22
Matrix:AQ - Ground Water Date Received:03/18/22
Method:SM 6200B Percent Solids:n/a
Project:Haks' Store; 901 Washington St, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
(c) Confirmed ND by reanalysis beyond hold-time.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
25 of 57
FA9404933.7
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:OW-5
Lab Sample ID:FA94049-8 Date Sampled:03/17/22
Matrix:AQ - Ground Water Date Received:03/18/22
Method:SM 6200B Percent Solids:n/a
Project:Haks' Store; 901 Washington St, Plymouth, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a A0231393.D 500 04/04/22 20:30 SS n/a n/a VA3102
Run #2 A0231310.D 10000 03/29/22 22:40 SS n/a n/a VA3098
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene b 455 250 63 ug/l
108-86-1 Bromobenzene ND c 5000 1300 ug/l
74-97-5 Bromochloromethane ND c 5000 1300 ug/l
75-27-4 Bromodichloromethane ND c 5000 1300 ug/l
75-25-2 Bromoform ND c 5000 1300 ug/l
104-51-8 n-Butylbenzene ND c 5000 1300 ug/l
135-98-8 sec-Butylbenzene ND c 5000 1300 ug/l
98-06-6 tert-Butylbenzene ND c 5000 1300 ug/l
56-23-5 Carbon Tetrachloride ND c 5000 1300 ug/l
108-90-7 Chlorobenzene ND c 5000 1300 ug/l
75-00-3 Chloroethane ND c 5000 2000 ug/l
67-66-3 Chloroform ND c 5000 1300 ug/l
95-49-8 o-Chlorotoluene ND c 5000 1300 ug/l
106-43-4 p-Chlorotoluene ND c 5000 1300 ug/l
124-48-1 Dibromochloromethane ND c 5000 1300 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND c 5000 2500 ug/l
106-93-4 1,2-Dibromoethane ND c 5000 1300 ug/l
75-71-8 Dichlorodifluoromethane ND c 5000 2000 ug/l
95-50-1 1,2-Dichlorobenzene ND c 5000 1300 ug/l
541-73-1 1,3-Dichlorobenzene ND c 5000 1300 ug/l
106-46-7 1,4-Dichlorobenzene ND c 5000 1300 ug/l
75-34-3 1,1-Dichloroethane ND c 5000 1300 ug/l
107-06-2 1,2-Dichloroethane ND c 5000 1300 ug/l
75-35-4 1,1-Dichloroethylene ND c 5000 1300 ug/l
156-59-2 cis-1,2-Dichloroethylene ND c 5000 1300 ug/l
156-60-5 trans-1,2-Dichloroethylene ND c 5000 1300 ug/l
78-87-5 1,2-Dichloropropane ND c 5000 1300 ug/l
142-28-9 1,3-Dichloropropane ND c 5000 1300 ug/l
594-20-7 2,2-Dichloropropane ND c 5000 1300 ug/l
563-58-6 1,1-Dichloropropene ND c 5000 1300 ug/l
10061-01-5 cis-1,3-Dichloropropene ND c 5000 1300 ug/l
10061-02-6 trans-1,3-Dichloropropene ND c 5000 1300 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
26 of 57
FA9404933.8
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:OW-5
Lab Sample ID:FA94049-8 Date Sampled:03/17/22
Matrix:AQ - Ground Water Date Received:03/18/22
Method:SM 6200B Percent Solids:n/a
Project:Haks' Store; 901 Washington St, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND c 5000 1300 ug/l
100-41-4 Ethylbenzene 2060 c 5000 1300 ug/l J
87-68-3 Hexachlorobutadiene ND c 5000 1300 ug/l
98-82-8 Isopropylbenzene 175 250 63 ug/l J
99-87-6 p-Isopropyltoluene ND c 5000 1300 ug/l
74-83-9 Methyl Bromide ND c 5000 2000 ug/l
74-87-3 Methyl Chloride ND c 5000 2000 ug/l
74-95-3 Methylene Bromide ND c 5000 1300 ug/l
75-09-2 Methylene Chloride ND c 20000 10000 ug/l
1634-04-4 Methyl Tert Butyl Ether ND c 5000 1300 ug/l
91-20-3 Naphthalene b 835 250 63 ug/l
103-65-1 n-Propylbenzene b 479 250 63 ug/l
100-42-5 Styrene ND c 5000 1300 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND c 5000 1300 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND c 5000 1300 ug/l
127-18-4 Tetrachloroethylene ND c 5000 1300 ug/l
108-88-3 Toluene 19300 c 5000 1300 ug/l
87-61-6 1,2,3-Trichlorobenzene ND c 5000 1300 ug/l
120-82-1 1,2,4-Trichlorobenzene ND c 5000 1300 ug/l
71-55-6 1,1,1-Trichloroethane ND c 5000 1300 ug/l
79-00-5 1,1,2-Trichloroethane ND c 5000 1300 ug/l
79-01-6 Trichloroethylene ND c 5000 1300 ug/l
75-69-4 Trichlorofluoromethane ND c 5000 2000 ug/l
96-18-4 1,2,3-Trichloropropane ND c 5000 1300 ug/l
95-63-6 1,2,4-Trimethylbenzene b 3900 250 63 ug/l
108-67-8 1,3,5-Trimethylbenzene b 995 250 63 ug/l
75-01-4 Vinyl Chloride ND c 5000 1300 ug/l
m,p-Xylene b 14000 500 63 ug/l
95-47-6 o-Xylene b 6780 250 63 ug/l
1330-20-7 Xylene (total) b 20800 750 130 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 99%100%70-130%
17060-07-0 1,2-Dichloroethane-D4 97%109%70-130%
2037-26-5 Toluene-D8 99%102%70-130%
460-00-4 4-Bromofluorobenzene 100%104%70-130%
(a) Sample re-analyzed beyond hold time; reported results are considered minimum values.
(b) Results from different vials are not consistent; higher results were reported.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
27 of 57
FA9404933.8
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:OW-5
Lab Sample ID:FA94049-8 Date Sampled:03/17/22
Matrix:AQ - Ground Water Date Received:03/18/22
Method:SM 6200B Percent Solids:n/a
Project:Haks' Store; 901 Washington St, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
(c) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
28 of 57
FA9404933.8
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-24
Lab Sample ID:FA94049-9 Date Sampled:03/17/22
Matrix:AQ - Ground Water Date Received:03/18/22
Method:SM 6200B Percent Solids:n/a
Project:Haks' Store; 901 Washington St, Plymouth, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a A0231378.D 1 04/04/22 14:46 SS n/a n/a VA3102
Run #2 A0231296.D 10 03/29/22 17:15 SS n/a n/a VA3098
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 2.7 b 5.0 1.3 ug/l J
108-86-1 Bromobenzene ND b 5.0 1.3 ug/l
74-97-5 Bromochloromethane ND b 5.0 1.3 ug/l
75-27-4 Bromodichloromethane ND b 5.0 1.3 ug/l
75-25-2 Bromoform ND b 5.0 1.3 ug/l
104-51-8 n-Butylbenzene ND b 5.0 1.3 ug/l
135-98-8 sec-Butylbenzene 0.21 0.50 0.13 ug/l J
98-06-6 tert-Butylbenzene ND b 5.0 1.3 ug/l
56-23-5 Carbon Tetrachloride ND b 5.0 1.3 ug/l
108-90-7 Chlorobenzene ND b 5.0 1.3 ug/l
75-00-3 Chloroethane ND b 5.0 2.0 ug/l
67-66-3 Chloroform ND b 5.0 1.3 ug/l
95-49-8 o-Chlorotoluene ND b 5.0 1.3 ug/l
106-43-4 p-Chlorotoluene ND b 5.0 1.3 ug/l
124-48-1 Dibromochloromethane ND b 5.0 1.3 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND b 5.0 2.5 ug/l
106-93-4 1,2-Dibromoethane ND b 5.0 1.3 ug/l
75-71-8 Dichlorodifluoromethane ND b 5.0 2.0 ug/l
95-50-1 1,2-Dichlorobenzene ND b 5.0 1.3 ug/l
541-73-1 1,3-Dichlorobenzene ND b 5.0 1.3 ug/l
106-46-7 1,4-Dichlorobenzene ND b 5.0 1.3 ug/l
75-34-3 1,1-Dichloroethane ND b 5.0 1.3 ug/l
107-06-2 1,2-Dichloroethane ND b 5.0 1.3 ug/l
75-35-4 1,1-Dichloroethylene ND b 5.0 1.3 ug/l
156-59-2 cis-1,2-Dichloroethylene ND b 5.0 1.3 ug/l
156-60-5 trans-1,2-Dichloroethylene ND b 5.0 1.3 ug/l
78-87-5 1,2-Dichloropropane ND b 5.0 1.3 ug/l
142-28-9 1,3-Dichloropropane ND b 5.0 1.3 ug/l
594-20-7 2,2-Dichloropropane ND b 5.0 1.3 ug/l
563-58-6 1,1-Dichloropropene ND b 5.0 1.3 ug/l
10061-01-5 cis-1,3-Dichloropropene ND b 5.0 1.3 ug/l
10061-02-6 trans-1,3-Dichloropropene ND b 5.0 1.3 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
29 of 57
FA9404933.9
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-24
Lab Sample ID:FA94049-9 Date Sampled:03/17/22
Matrix:AQ - Ground Water Date Received:03/18/22
Method:SM 6200B Percent Solids:n/a
Project:Haks' Store; 901 Washington St, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 0.13 0.50 0.13 ug/l J
100-41-4 Ethylbenzene 0.19 0.50 0.13 ug/l J
87-68-3 Hexachlorobutadiene ND b 5.0 1.3 ug/l
98-82-8 Isopropylbenzene 0.19 0.50 0.13 ug/l J
99-87-6 p-Isopropyltoluene 0.69 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND b 5.0 2.0 ug/l
74-87-3 Methyl Chloride ND b 5.0 2.0 ug/l
74-95-3 Methylene Bromide ND b 5.0 1.3 ug/l
75-09-2 Methylene Chloride ND b 20 10 ug/l
1634-04-4 Methyl Tert Butyl Ether 20.3 b 5.0 1.3 ug/l
91-20-3 Naphthalene 0.41 0.50 0.13 ug/l J
103-65-1 n-Propylbenzene ND b 5.0 1.3 ug/l
100-42-5 Styrene ND b 5.0 1.3 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND b 5.0 1.3 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND b 5.0 1.3 ug/l
127-18-4 Tetrachloroethylene ND b 5.0 1.3 ug/l
108-88-3 Toluene 0.65 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND b 5.0 1.3 ug/l
120-82-1 1,2,4-Trichlorobenzene ND b 5.0 1.3 ug/l
71-55-6 1,1,1-Trichloroethane ND b 5.0 1.3 ug/l
79-00-5 1,1,2-Trichloroethane ND b 5.0 1.3 ug/l
79-01-6 Trichloroethylene ND b 5.0 1.3 ug/l
75-69-4 Trichlorofluoromethane ND b 5.0 2.0 ug/l
96-18-4 1,2,3-Trichloropropane ND b 5.0 1.3 ug/l
95-63-6 1,2,4-Trimethylbenzene ND b 5.0 1.3 ug/l
108-67-8 1,3,5-Trimethylbenzene 0.13 0.50 0.13 ug/l J
75-01-4 Vinyl Chloride ND b 5.0 1.3 ug/l
m,p-Xylene 2.0 1.0 0.13 ug/l
95-47-6 o-Xylene 2.7 0.50 0.13 ug/l
1330-20-7 Xylene (total)4.7 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%100%70-130%
17060-07-0 1,2-Dichloroethane-D4 98%105%70-130%
2037-26-5 Toluene-D8 91%101%70-130%
460-00-4 4-Bromofluorobenzene 96%102%70-130%
(a) Sample re-analyzed beyond hold time; reported results are considered minimum values.
(b) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
30 of 57
FA9404933.9
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-39
Lab Sample ID:FA94049-10 Date Sampled:03/17/22
Matrix:AQ - Ground Water Date Received:03/18/22
Method:SM 6200B Percent Solids:n/a
Project:Haks' Store; 901 Washington St, Plymouth, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0231295.D 2 03/29/22 16:52 SS n/a n/a VA3098
Run #2 a A0231389.D 2 04/04/22 18:59 SS n/a n/a VA3102
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 1.0 0.25 ug/l
108-86-1 Bromobenzene ND 1.0 0.25 ug/l
74-97-5 Bromochloromethane ND 1.0 0.25 ug/l
75-27-4 Bromodichloromethane ND 1.0 0.25 ug/l
75-25-2 Bromoform ND 1.0 0.25 ug/l
104-51-8 n-Butylbenzene ND 1.0 0.25 ug/l
135-98-8 sec-Butylbenzene ND 1.0 0.25 ug/l
98-06-6 tert-Butylbenzene ND 1.0 0.25 ug/l
56-23-5 Carbon Tetrachloride ND 1.0 0.25 ug/l
108-90-7 Chlorobenzene ND 1.0 0.25 ug/l
75-00-3 Chloroethane ND 1.0 0.40 ug/l
67-66-3 Chloroform ND 1.0 0.25 ug/l
95-49-8 o-Chlorotoluene ND 1.0 0.25 ug/l
106-43-4 p-Chlorotoluene ND 1.0 0.25 ug/l
124-48-1 Dibromochloromethane ND 1.0 0.25 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 1.0 0.49 ug/l
106-93-4 1,2-Dibromoethane ND 1.0 0.25 ug/l
75-71-8 Dichlorodifluoromethane ND 1.0 0.40 ug/l
95-50-1 1,2-Dichlorobenzene ND 1.0 0.25 ug/l
541-73-1 1,3-Dichlorobenzene ND 1.0 0.25 ug/l
106-46-7 1,4-Dichlorobenzene ND 1.0 0.25 ug/l
75-34-3 1,1-Dichloroethane ND 1.0 0.25 ug/l
107-06-2 1,2-Dichloroethane ND 1.0 0.25 ug/l
75-35-4 1,1-Dichloroethylene ND 1.0 0.25 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 1.0 0.25 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 1.0 0.25 ug/l
78-87-5 1,2-Dichloropropane ND 1.0 0.25 ug/l
142-28-9 1,3-Dichloropropane ND 1.0 0.25 ug/l
594-20-7 2,2-Dichloropropane ND 1.0 0.25 ug/l
563-58-6 1,1-Dichloropropene ND 1.0 0.25 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 1.0 0.25 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 1.0 0.25 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
31 of 57
FA9404933.10
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-39
Lab Sample ID:FA94049-10 Date Sampled:03/17/22
Matrix:AQ - Ground Water Date Received:03/18/22
Method:SM 6200B Percent Solids:n/a
Project:Haks' Store; 901 Washington St, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 0.78 1.0 0.25 ug/l J
100-41-4 Ethylbenzene ND 1.0 0.25 ug/l
87-68-3 Hexachlorobutadiene ND 1.0 0.25 ug/l
98-82-8 Isopropylbenzene ND 1.0 0.25 ug/l
99-87-6 p-Isopropyltoluene ND 1.0 0.25 ug/l
74-83-9 Methyl Bromide ND 1.0 0.40 ug/l
74-87-3 Methyl Chloride ND 1.0 0.40 ug/l
74-95-3 Methylene Bromide ND 1.0 0.25 ug/l
75-09-2 Methylene Chloride b 3.2 4.0 2.0 ug/l JB
1634-04-4 Methyl Tert Butyl Ether 4.5 1.0 0.25 ug/l
91-20-3 Naphthalene ND 1.0 0.25 ug/l
103-65-1 n-Propylbenzene ND 1.0 0.25 ug/l
100-42-5 Styrene ND 1.0 0.25 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 1.0 0.25 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 0.25 ug/l
127-18-4 Tetrachloroethylene ND 1.0 0.25 ug/l
108-88-3 Toluene ND 1.0 0.25 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 1.0 0.25 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 1.0 0.25 ug/l
71-55-6 1,1,1-Trichloroethane ND 1.0 0.25 ug/l
79-00-5 1,1,2-Trichloroethane ND 1.0 0.25 ug/l
79-01-6 Trichloroethylene ND 1.0 0.25 ug/l
75-69-4 Trichlorofluoromethane ND 1.0 0.40 ug/l
96-18-4 1,2,3-Trichloropropane ND 1.0 0.25 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 1.0 0.25 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 1.0 0.25 ug/l
75-01-4 Vinyl Chloride ND 1.0 0.25 ug/l
m,p-Xylene ND 2.0 0.25 ug/l
95-47-6 o-Xylene ND 1.0 0.25 ug/l
1330-20-7 Xylene (total)ND 3.0 0.50 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 99%98%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%101%70-130%
2037-26-5 Toluene-D8 100%98%70-130%
460-00-4 4-Bromofluorobenzene 103%96%70-130%
(a) Confirmation run beyond holdtime.
(b) Confirmed ND by reanalysis beyond hold-time.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
32 of 57
FA9404933.10
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW-11
Lab Sample ID:FA94049-11 Date Sampled:03/17/22
Matrix:AQ - Ground Water Date Received:03/18/22
Method:SM 6200B Percent Solids:n/a
Project:Haks' Store; 901 Washington St, Plymouth, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a A0231390.D 2.5 04/04/22 19:22 SS n/a n/a VA3102
Run #2 A0231299.D 50 03/29/22 18:28 SS n/a n/a VA3098
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 1.3 1.3 0.31 ug/l
108-86-1 Bromobenzene ND b 25 6.3 ug/l
74-97-5 Bromochloromethane ND b 25 6.3 ug/l
75-27-4 Bromodichloromethane ND b 25 6.3 ug/l
75-25-2 Bromoform ND b 25 6.3 ug/l
104-51-8 n-Butylbenzene ND b 25 6.3 ug/l
135-98-8 sec-Butylbenzene 0.54 1.3 0.31 ug/l J
98-06-6 tert-Butylbenzene ND b 25 6.3 ug/l
56-23-5 Carbon Tetrachloride ND b 25 6.3 ug/l
108-90-7 Chlorobenzene ND b 25 6.3 ug/l
75-00-3 Chloroethane ND b 25 10 ug/l
67-66-3 Chloroform ND b 25 6.3 ug/l
95-49-8 o-Chlorotoluene ND b 25 6.3 ug/l
106-43-4 p-Chlorotoluene ND b 25 6.3 ug/l
124-48-1 Dibromochloromethane ND b 25 6.3 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND b 25 12 ug/l
106-93-4 1,2-Dibromoethane ND b 25 6.3 ug/l
75-71-8 Dichlorodifluoromethane ND b 25 10 ug/l
95-50-1 1,2-Dichlorobenzene ND b 25 6.3 ug/l
541-73-1 1,3-Dichlorobenzene ND b 25 6.3 ug/l
106-46-7 1,4-Dichlorobenzene ND b 25 6.3 ug/l
75-34-3 1,1-Dichloroethane ND b 25 6.3 ug/l
107-06-2 1,2-Dichloroethane ND b 25 6.3 ug/l
75-35-4 1,1-Dichloroethylene ND b 25 6.3 ug/l
156-59-2 cis-1,2-Dichloroethylene ND b 25 6.3 ug/l
156-60-5 trans-1,2-Dichloroethylene ND b 25 6.3 ug/l
78-87-5 1,2-Dichloropropane ND b 25 6.3 ug/l
142-28-9 1,3-Dichloropropane ND b 25 6.3 ug/l
594-20-7 2,2-Dichloropropane ND b 25 6.3 ug/l
563-58-6 1,1-Dichloropropene ND b 25 6.3 ug/l
10061-01-5 cis-1,3-Dichloropropene ND b 25 6.3 ug/l
10061-02-6 trans-1,3-Dichloropropene ND b 25 6.3 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
33 of 57
FA9404933.11
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW-11
Lab Sample ID:FA94049-11 Date Sampled:03/17/22
Matrix:AQ - Ground Water Date Received:03/18/22
Method:SM 6200B Percent Solids:n/a
Project:Haks' Store; 901 Washington St, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND b 25 6.3 ug/l
100-41-4 Ethylbenzene 1.4 1.3 0.31 ug/l
87-68-3 Hexachlorobutadiene ND b 25 6.3 ug/l
98-82-8 Isopropylbenzene ND b 25 6.3 ug/l
99-87-6 p-Isopropyltoluene ND b 25 6.3 ug/l
74-83-9 Methyl Bromide ND b 25 10 ug/l
74-87-3 Methyl Chloride ND b 25 10 ug/l
74-95-3 Methylene Bromide ND b 25 6.3 ug/l
75-09-2 Methylene Chloride c 51.7 b 100 50 ug/l JB
1634-04-4 Methyl Tert Butyl Ether 104 b 25 6.3 ug/l
91-20-3 Naphthalene ND b 25 6.3 ug/l
103-65-1 n-Propylbenzene ND b 25 6.3 ug/l
100-42-5 Styrene ND b 25 6.3 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND b 25 6.3 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND b 25 6.3 ug/l
127-18-4 Tetrachloroethylene ND b 25 6.3 ug/l
108-88-3 Toluene 1.4 1.3 0.31 ug/l
87-61-6 1,2,3-Trichlorobenzene ND b 25 6.3 ug/l
120-82-1 1,2,4-Trichlorobenzene ND b 25 6.3 ug/l
71-55-6 1,1,1-Trichloroethane ND b 25 6.3 ug/l
79-00-5 1,1,2-Trichloroethane ND b 25 6.3 ug/l
79-01-6 Trichloroethylene ND b 25 6.3 ug/l
75-69-4 Trichlorofluoromethane ND b 25 10 ug/l
96-18-4 1,2,3-Trichloropropane ND b 25 6.3 ug/l
95-63-6 1,2,4-Trimethylbenzene 0.65 1.3 0.31 ug/l J
108-67-8 1,3,5-Trimethylbenzene ND b 25 6.3 ug/l
75-01-4 Vinyl Chloride ND b 25 6.3 ug/l
m,p-Xylene 0.96 2.5 0.31 ug/l J
95-47-6 o-Xylene 0.79 1.3 0.31 ug/l J
1330-20-7 Xylene (total)1.8 3.8 0.63 ug/l J
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%101%70-130%
17060-07-0 1,2-Dichloroethane-D4 101%106%70-130%
2037-26-5 Toluene-D8 99%101%70-130%
460-00-4 4-Bromofluorobenzene 97%103%70-130%
(a) Sample re-analyzed beyond hold time; reported results are considered minimum values.
(b) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
34 of 57
FA9404933.11
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW-11
Lab Sample ID:FA94049-11 Date Sampled:03/17/22
Matrix:AQ - Ground Water Date Received:03/18/22
Method:SM 6200B Percent Solids:n/a
Project:Haks' Store; 901 Washington St, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
(c) Confirmed ND by reanalysis beyond hold-time.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
35 of 57
FA9404933.11
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW-14
Lab Sample ID:FA94049-12 Date Sampled:03/17/22
Matrix:AQ - Ground Water Date Received:03/18/22
Method:SM 6200B Percent Solids:n/a
Project:Haks' Store; 901 Washington St, Plymouth, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a A0231395.D 1000 04/04/22 21:16 SS n/a n/a VA3102
Run #2 A0231311.D 10000 03/29/22 23:04 SS n/a n/a VA3098
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 2130 b 5000 1300 ug/l J
108-86-1 Bromobenzene ND b 5000 1300 ug/l
74-97-5 Bromochloromethane ND b 5000 1300 ug/l
75-27-4 Bromodichloromethane ND b 5000 1300 ug/l
75-25-2 Bromoform ND b 5000 1300 ug/l
104-51-8 n-Butylbenzene ND b 5000 1300 ug/l
135-98-8 sec-Butylbenzene ND b 5000 1300 ug/l
98-06-6 tert-Butylbenzene ND b 5000 1300 ug/l
56-23-5 Carbon Tetrachloride ND b 5000 1300 ug/l
108-90-7 Chlorobenzene ND b 5000 1300 ug/l
75-00-3 Chloroethane ND b 5000 2000 ug/l
67-66-3 Chloroform ND b 5000 1300 ug/l
95-49-8 o-Chlorotoluene 332 500 130 ug/l J
106-43-4 p-Chlorotoluene ND b 5000 1300 ug/l
124-48-1 Dibromochloromethane ND b 5000 1300 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND b 5000 2500 ug/l
106-93-4 1,2-Dibromoethane ND b 5000 1300 ug/l
75-71-8 Dichlorodifluoromethane ND b 5000 2000 ug/l
95-50-1 1,2-Dichlorobenzene ND b 5000 1300 ug/l
541-73-1 1,3-Dichlorobenzene ND b 5000 1300 ug/l
106-46-7 1,4-Dichlorobenzene ND b 5000 1300 ug/l
75-34-3 1,1-Dichloroethane ND b 5000 1300 ug/l
107-06-2 1,2-Dichloroethane ND b 5000 1300 ug/l
75-35-4 1,1-Dichloroethylene ND b 5000 1300 ug/l
156-59-2 cis-1,2-Dichloroethylene ND b 5000 1300 ug/l
156-60-5 trans-1,2-Dichloroethylene ND b 5000 1300 ug/l
78-87-5 1,2-Dichloropropane ND b 5000 1300 ug/l
142-28-9 1,3-Dichloropropane ND b 5000 1300 ug/l
594-20-7 2,2-Dichloropropane ND b 5000 1300 ug/l
563-58-6 1,1-Dichloropropene ND b 5000 1300 ug/l
10061-01-5 cis-1,3-Dichloropropene ND b 5000 1300 ug/l
10061-02-6 trans-1,3-Dichloropropene ND b 5000 1300 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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FA9404933.12
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW-14
Lab Sample ID:FA94049-12 Date Sampled:03/17/22
Matrix:AQ - Ground Water Date Received:03/18/22
Method:SM 6200B Percent Solids:n/a
Project:Haks' Store; 901 Washington St, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND b 5000 1300 ug/l
100-41-4 Ethylbenzene 2780 b 5000 1300 ug/l J
87-68-3 Hexachlorobutadiene ND b 5000 1300 ug/l
98-82-8 Isopropylbenzene 136 500 130 ug/l J
99-87-6 p-Isopropyltoluene ND b 5000 1300 ug/l
74-83-9 Methyl Bromide ND b 5000 2000 ug/l
74-87-3 Methyl Chloride ND b 5000 2000 ug/l
74-95-3 Methylene Bromide ND b 5000 1300 ug/l
75-09-2 Methylene Chloride c 10200 b 20000 10000 ug/l
1634-04-4 Methyl Tert Butyl Ether 273 500 130 ug/l J
91-20-3 Naphthalene 739 500 130 ug/l
103-65-1 n-Propylbenzene 367 500 130 ug/l J
100-42-5 Styrene ND b 5000 1300 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND b 5000 1300 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND b 5000 1300 ug/l
127-18-4 Tetrachloroethylene ND b 5000 1300 ug/l
108-88-3 Toluene 35600 b 5000 1300 ug/l
87-61-6 1,2,3-Trichlorobenzene ND b 5000 1300 ug/l
120-82-1 1,2,4-Trichlorobenzene ND b 5000 1300 ug/l
71-55-6 1,1,1-Trichloroethane ND b 5000 1300 ug/l
79-00-5 1,1,2-Trichloroethane ND b 5000 1300 ug/l
79-01-6 Trichloroethylene ND b 5000 1300 ug/l
75-69-4 Trichlorofluoromethane ND b 5000 2000 ug/l
96-18-4 1,2,3-Trichloropropane ND b 5000 1300 ug/l
95-63-6 1,2,4-Trimethylbenzene 2920 500 130 ug/l
108-67-8 1,3,5-Trimethylbenzene 817 500 130 ug/l
75-01-4 Vinyl Chloride ND b 5000 1300 ug/l
m,p-Xylene 12800 1000 130 ug/l
95-47-6 o-Xylene 6410 500 130 ug/l
1330-20-7 Xylene (total)19200 1500 250 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%101%70-130%
17060-07-0 1,2-Dichloroethane-D4 98%109%70-130%
2037-26-5 Toluene-D8 99%102%70-130%
460-00-4 4-Bromofluorobenzene 99%102%70-130%
(a) Sample re-analyzed beyond hold time; reported results are considered minimum values.
(b) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
37 of 57
FA9404933.12
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW-14
Lab Sample ID:FA94049-12 Date Sampled:03/17/22
Matrix:AQ - Ground Water Date Received:03/18/22
Method:SM 6200B Percent Solids:n/a
Project:Haks' Store; 901 Washington St, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
(c) Confirmed ND by reanalysis beyond hold-time.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
38 of 57
FA9404933.12
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-15
Lab Sample ID:FA94049-13 Date Sampled:03/17/22
Matrix:AQ - Ground Water Date Received:03/18/22
Method:SM 6200B Percent Solids:n/a
Project:Haks' Store; 901 Washington St, Plymouth, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0231297.D 10 03/29/22 17:38 SS n/a n/a VA3098
Run #2 a A0231379.D 1 04/04/22 15:09 SS n/a n/a VA3102
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 5.0 1.3 ug/l
108-86-1 Bromobenzene ND 5.0 1.3 ug/l
74-97-5 Bromochloromethane ND 5.0 1.3 ug/l
75-27-4 Bromodichloromethane ND 5.0 1.3 ug/l
75-25-2 Bromoform ND 5.0 1.3 ug/l
104-51-8 n-Butylbenzene ND 5.0 1.3 ug/l
135-98-8 sec-Butylbenzene ND 5.0 1.3 ug/l
98-06-6 tert-Butylbenzene ND 5.0 1.3 ug/l
56-23-5 Carbon Tetrachloride ND 5.0 1.3 ug/l
108-90-7 Chlorobenzene ND 5.0 1.3 ug/l
75-00-3 Chloroethane ND 5.0 2.0 ug/l
67-66-3 Chloroform ND 5.0 1.3 ug/l
95-49-8 o-Chlorotoluene ND 5.0 1.3 ug/l
106-43-4 p-Chlorotoluene ND 5.0 1.3 ug/l
124-48-1 Dibromochloromethane ND 5.0 1.3 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 5.0 2.5 ug/l
106-93-4 1,2-Dibromoethane ND 5.0 1.3 ug/l
75-71-8 Dichlorodifluoromethane ND 5.0 2.0 ug/l
95-50-1 1,2-Dichlorobenzene ND 5.0 1.3 ug/l
541-73-1 1,3-Dichlorobenzene ND 5.0 1.3 ug/l
106-46-7 1,4-Dichlorobenzene ND 5.0 1.3 ug/l
75-34-3 1,1-Dichloroethane ND 5.0 1.3 ug/l
107-06-2 1,2-Dichloroethane ND 5.0 1.3 ug/l
75-35-4 1,1-Dichloroethylene ND 5.0 1.3 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.3 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.3 ug/l
78-87-5 1,2-Dichloropropane ND 5.0 1.3 ug/l
142-28-9 1,3-Dichloropropane ND 5.0 1.3 ug/l
594-20-7 2,2-Dichloropropane ND 5.0 1.3 ug/l
563-58-6 1,1-Dichloropropene ND 5.0 1.3 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.3 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.3 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
39 of 57
FA9404933.13
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-15
Lab Sample ID:FA94049-13 Date Sampled:03/17/22
Matrix:AQ - Ground Water Date Received:03/18/22
Method:SM 6200B Percent Solids:n/a
Project:Haks' Store; 901 Washington St, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 5.0 1.3 ug/l
100-41-4 Ethylbenzene ND 5.0 1.3 ug/l
87-68-3 Hexachlorobutadiene ND 5.0 1.3 ug/l
98-82-8 Isopropylbenzene ND 5.0 1.3 ug/l
99-87-6 p-Isopropyltoluene ND 5.0 1.3 ug/l
74-83-9 Methyl Bromide ND 5.0 2.0 ug/l
74-87-3 Methyl Chloride ND 5.0 2.0 ug/l
74-95-3 Methylene Bromide ND 5.0 1.3 ug/l
75-09-2 Methylene Chloride b 10.1 20 10 ug/l JB
1634-04-4 Methyl Tert Butyl Ether ND 5.0 1.3 ug/l
91-20-3 Naphthalene ND 5.0 1.3 ug/l
103-65-1 n-Propylbenzene ND 5.0 1.3 ug/l
100-42-5 Styrene ND 5.0 1.3 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 5.0 1.3 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 1.3 ug/l
127-18-4 Tetrachloroethylene ND 5.0 1.3 ug/l
108-88-3 Toluene ND 5.0 1.3 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 5.0 1.3 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.3 ug/l
71-55-6 1,1,1-Trichloroethane ND 5.0 1.3 ug/l
79-00-5 1,1,2-Trichloroethane ND 5.0 1.3 ug/l
79-01-6 Trichloroethylene ND 5.0 1.3 ug/l
75-69-4 Trichlorofluoromethane ND 5.0 2.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 5.0 1.3 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 5.0 1.3 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 5.0 1.3 ug/l
75-01-4 Vinyl Chloride ND 5.0 1.3 ug/l
m,p-Xylene ND 10 1.3 ug/l
95-47-6 o-Xylene ND 5.0 1.3 ug/l
1330-20-7 Xylene (total)ND 15 2.5 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%100%70-130%
17060-07-0 1,2-Dichloroethane-D4 107%100%70-130%
2037-26-5 Toluene-D8 100%91%70-130%
460-00-4 4-Bromofluorobenzene 104%96%70-130%
(a) Confirmation run beyond holdtime.
(b) Confirmed ND by reanalysis beyond hold-time.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
40 of 57
FA9404933.13
SGS North America Inc.
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Orlando, FL
Section 4
41 of 57
FA940494
FA94049: Chain of Custody
Page 1 of 3
42 of 57
FA9404944.1
FA94049: Chain of Custody
Page 2 of 3
43 of 57
FA9404944.1
Job Number:FA94049 Client:GEOLOGICAL RESOURCES INC.
Date / Time Received:3/18/2022 10:00:00 AM Delivery Method:FEDEX
Project:HAK'S STORE
Airbill #'s:1009 6379 5777
Cooler Information
1. Custody Seals Present
2. Custody Seals Intact
4. Cooler temp verification
3. Temp criteria achieved
5. Cooler media
IR Gun
Ice (Bag)
Trip Blank Information
1. Trip Blank present / cooler
2. Trip Blank listed on COC
2. Samples preserved properly
Sample Information
1. Sample labels present on bottles
5. Sample recvd within HT
4. Condition of sample
3. Sufficient volume/containers recvd for analysis:
Intact
Comments
SM001Rev. Date 05/24/17
SGS Sample Receipt Summary
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
Cooler 1: (3.2);
Cooler 1: (3.6);
3. Type Of TB Received
W or S N/A
6. Dates/Times/IDs on COC match Sample Label
7. VOCs have headspace
8. Bottles received for unspecified tests
9. Compositing instructions clear
10. Voa Soil Kits/Jars received past 48hrs?
11. % Solids Jar received?
Misc. Information
25-Gram 5-GramNumber of Encores:Number of 5035 Field Kits:Number of Lab Filtered Metals:
Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify)
Y or N N/A
Y or N
Therm ID:IR 1; Therm CF:0.4; # of Coolers:1
Y or N N/A
12. Residual Chlorine Present?
Residual Chlorine Test Strip Lot #:
Technician:Reviewer:SAMUELM Date:Date:3/18/2022 10:00:00 A
FA94049: Chain of Custody
Page 3 of 3
44 of 57
FA9404944.1
SGS North America Inc.
MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 5
45 of 57
FA940495
Method Blank Summary Page 1 of 2
Job Number:FA94049
Account:GRINCC GRI (Geological Resources Inc.)
Project:Haks' Store; 901 Washington St, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA3097-MB A0231259.D 1 03/28/22 SS n/a n/a VA3097
The QC reported here applies to the following samples:Method: SM 6200B
FA94049-1
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
46 of 57
FA9404955.1.1
Method Blank Summary Page 2 of 2
Job Number:FA94049
Account:GRINCC GRI (Geological Resources Inc.)
Project:Haks' Store; 901 Washington St, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA3097-MB A0231259.D 1 03/28/22 SS n/a n/a VA3097
The QC reported here applies to the following samples:Method: SM 6200B
FA94049-1
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride 2.6 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 97%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
47 of 57
FA9404955.1.1
Method Blank Summary Page 1 of 2
Job Number:FA94049
Account:GRINCC GRI (Geological Resources Inc.)
Project:Haks' Store; 901 Washington St, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA3098-MB A0231289.D 1 03/29/22 SS n/a n/a VA3098
The QC reported here applies to the following samples:Method: SM 6200B
FA94049-2, FA94049-3, FA94049-4, FA94049-5, FA94049-6, FA94049-7, FA94049-8, FA94049-9, FA94049-10,
FA94049-11, FA94049-12, FA94049-13
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
48 of 57
FA9404955.1.2
Method Blank Summary Page 2 of 2
Job Number:FA94049
Account:GRINCC GRI (Geological Resources Inc.)
Project:Haks' Store; 901 Washington St, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA3098-MB A0231289.D 1 03/29/22 SS n/a n/a VA3098
The QC reported here applies to the following samples:Method: SM 6200B
FA94049-2, FA94049-3, FA94049-4, FA94049-5, FA94049-6, FA94049-7, FA94049-8, FA94049-9, FA94049-10,
FA94049-11, FA94049-12, FA94049-13
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride 3.4 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
49 of 57
FA9404955.1.2
Blank Spike Summary Page 1 of 2
Job Number:FA94049
Account:GRINCC GRI (Geological Resources Inc.)
Project:Haks' Store; 901 Washington St, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA3097-BS A0231257.D 1 03/28/22 SS n/a n/a VA3097
The QC reported here applies to the following samples:Method: SM 6200B
FA94049-1
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 9.8 98 70-130
108-86-1 Bromobenzene 10 9.4 94 70-130
74-97-5 Bromochloromethane 10 7.9 79 70-130
75-27-4 Bromodichloromethane 10 9.3 93 70-130
75-25-2 Bromoform 10 9.3 93 70-130
104-51-8 n-Butylbenzene 10 9.6 96 70-130
135-98-8 sec-Butylbenzene 10 11.1 111 70-130
98-06-6 tert-Butylbenzene 10 10.5 105 70-130
56-23-5 Carbon Tetrachloride 10 10.1 101 70-130
108-90-7 Chlorobenzene 10 9.4 94 70-130
75-00-3 Chloroethane 10 8.7 87 60-140
67-66-3 Chloroform 10 8.9 89 70-130
95-49-8 o-Chlorotoluene 10 9.9 99 70-130
106-43-4 p-Chlorotoluene 10 9.8 98 70-130
124-48-1 Dibromochloromethane 10 9.2 92 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 9.0 90 70-130
106-93-4 1,2-Dibromoethane 10 9.3 93 70-130
75-71-8 Dichlorodifluoromethane 10 9.4 94 60-140
95-50-1 1,2-Dichlorobenzene 10 9.5 95 70-130
541-73-1 1,3-Dichlorobenzene 10 9.7 97 70-130
106-46-7 1,4-Dichlorobenzene 10 9.2 92 70-130
75-34-3 1,1-Dichloroethane 10 9.4 94 70-130
107-06-2 1,2-Dichloroethane 10 8.9 89 70-130
75-35-4 1,1-Dichloroethylene 10 9.7 97 70-130
156-59-2 cis-1,2-Dichloroethylene 10 9.5 95 70-130
156-60-5 trans-1,2-Dichloroethylene 10 9.6 96 70-130
78-87-5 1,2-Dichloropropane 10 9.6 96 70-130
142-28-9 1,3-Dichloropropane 10 9.2 92 70-130
594-20-7 2,2-Dichloropropane 10 9.6 96 70-130
563-58-6 1,1-Dichloropropene 10 10.1 101 70-130
10061-01-5 cis-1,3-Dichloropropene 10 10 100 70-130
10061-02-6 trans-1,3-Dichloropropene 10 9.7 97 70-130
108-20-3 Di-Isopropyl Ether 10 8.9 89 70-130
100-41-4 Ethylbenzene 10 9.8 98 70-130
87-68-3 Hexachlorobutadiene 10 10.3 103 70-130
98-82-8 Isopropylbenzene 10 10.7 107 70-130
* = Outside of Control Limits.
50 of 57
FA9404955.2.1
Blank Spike Summary Page 2 of 2
Job Number:FA94049
Account:GRINCC GRI (Geological Resources Inc.)
Project:Haks' Store; 901 Washington St, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA3097-BS A0231257.D 1 03/28/22 SS n/a n/a VA3097
The QC reported here applies to the following samples:Method: SM 6200B
FA94049-1
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 10.3 103 70-130
74-83-9 Methyl Bromide 10 8.9 89 60-140
74-87-3 Methyl Chloride 10 9.3 93 60-140
74-95-3 Methylene Bromide 10 8.5 85 70-130
75-09-2 Methylene Chloride 10 9.2 92 70-130
1634-04-4 Methyl Tert Butyl Ether 10 8.5 85 70-130
91-20-3 Naphthalene 10 9.1 91 70-130
103-65-1 n-Propylbenzene 10 10.2 102 70-130
100-42-5 Styrene 10 9.4 94 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 9.8 98 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 9.3 93 70-130
127-18-4 Tetrachloroethylene 10 9.7 97 70-130
108-88-3 Toluene 10 9.8 98 70-130
87-61-6 1,2,3-Trichlorobenzene 10 9.5 95 70-130
120-82-1 1,2,4-Trichlorobenzene 10 9.8 98 70-130
71-55-6 1,1,1-Trichloroethane 10 9.5 95 70-130
79-00-5 1,1,2-Trichloroethane 10 9.3 93 70-130
79-01-6 Trichloroethylene 10 9.5 95 70-130
75-69-4 Trichlorofluoromethane 10 11.8 118 60-140
96-18-4 1,2,3-Trichloropropane 10 8.9 89 70-130
95-63-6 1,2,4-Trimethylbenzene 10 9.3 93 70-130
108-67-8 1,3,5-Trimethylbenzene 10 10.5 105 70-130
75-01-4 Vinyl Chloride 10 9.4 94 60-140
m,p-Xylene 20 20.0 100 70-130
95-47-6 o-Xylene 10 10.1 101 70-130
1330-20-7 Xylene (total)30 30.2 101 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 98%70-130%
17060-07-0 1,2-Dichloroethane-D4 96%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 103%70-130%
* = Outside of Control Limits.
51 of 57
FA9404955.2.1
Blank Spike Summary Page 1 of 2
Job Number:FA94049
Account:GRINCC GRI (Geological Resources Inc.)
Project:Haks' Store; 901 Washington St, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA3098-BS A0231287.D 1 03/29/22 SS n/a n/a VA3098
The QC reported here applies to the following samples:Method: SM 6200B
FA94049-2, FA94049-3, FA94049-4, FA94049-5, FA94049-6, FA94049-7, FA94049-8, FA94049-9, FA94049-10,
FA94049-11, FA94049-12, FA94049-13
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 11.0 110 70-130
108-86-1 Bromobenzene 10 10.4 104 70-130
74-97-5 Bromochloromethane 10 8.8 88 70-130
75-27-4 Bromodichloromethane 10 10.6 106 70-130
75-25-2 Bromoform 10 9.9 99 70-130
104-51-8 n-Butylbenzene 10 10.8 108 70-130
135-98-8 sec-Butylbenzene 10 12.4 124 70-130
98-06-6 tert-Butylbenzene 10 11.7 117 70-130
56-23-5 Carbon Tetrachloride 10 11.3 113 70-130
108-90-7 Chlorobenzene 10 10.4 104 70-130
75-00-3 Chloroethane 10 9.7 97 60-140
67-66-3 Chloroform 10 9.9 99 70-130
95-49-8 o-Chlorotoluene 10 11.2 112 70-130
106-43-4 p-Chlorotoluene 10 11.1 111 70-130
124-48-1 Dibromochloromethane 10 10.2 102 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 10.4 104 70-130
106-93-4 1,2-Dibromoethane 10 10.3 103 70-130
75-71-8 Dichlorodifluoromethane 10 9.6 96 60-140
95-50-1 1,2-Dichlorobenzene 10 10.6 106 70-130
541-73-1 1,3-Dichlorobenzene 10 10.8 108 70-130
106-46-7 1,4-Dichlorobenzene 10 10.2 102 70-130
75-34-3 1,1-Dichloroethane 10 10.6 106 70-130
107-06-2 1,2-Dichloroethane 10 10.2 102 70-130
75-35-4 1,1-Dichloroethylene 10 11.1 111 70-130
156-59-2 cis-1,2-Dichloroethylene 10 10.7 107 70-130
156-60-5 trans-1,2-Dichloroethylene 10 10.8 108 70-130
78-87-5 1,2-Dichloropropane 10 11.0 110 70-130
142-28-9 1,3-Dichloropropane 10 10.4 104 70-130
594-20-7 2,2-Dichloropropane 10 11.2 112 70-130
563-58-6 1,1-Dichloropropene 10 11.5 115 70-130
10061-01-5 cis-1,3-Dichloropropene 10 11.1 111 70-130
10061-02-6 trans-1,3-Dichloropropene 10 11.1 111 70-130
108-20-3 Di-Isopropyl Ether 10 10.2 102 70-130
100-41-4 Ethylbenzene 10 11.1 111 70-130
87-68-3 Hexachlorobutadiene 10 11.3 113 70-130
98-82-8 Isopropylbenzene 10 11.9 119 70-130
* = Outside of Control Limits.
52 of 57
FA9404955.2.2
Blank Spike Summary Page 2 of 2
Job Number:FA94049
Account:GRINCC GRI (Geological Resources Inc.)
Project:Haks' Store; 901 Washington St, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA3098-BS A0231287.D 1 03/29/22 SS n/a n/a VA3098
The QC reported here applies to the following samples:Method: SM 6200B
FA94049-2, FA94049-3, FA94049-4, FA94049-5, FA94049-6, FA94049-7, FA94049-8, FA94049-9, FA94049-10,
FA94049-11, FA94049-12, FA94049-13
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 11.4 114 70-130
74-83-9 Methyl Bromide 10 9.6 96 60-140
74-87-3 Methyl Chloride 10 9.5 95 60-140
74-95-3 Methylene Bromide 10 9.5 95 70-130
75-09-2 Methylene Chloride 10 10.3 103 70-130
1634-04-4 Methyl Tert Butyl Ether 10 9.6 96 70-130
91-20-3 Naphthalene 10 10.3 103 70-130
103-65-1 n-Propylbenzene 10 11.5 115 70-130
100-42-5 Styrene 10 10.6 106 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 11.0 110 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 10.8 108 70-130
127-18-4 Tetrachloroethylene 10 10.8 108 70-130
108-88-3 Toluene 10 11.0 110 70-130
87-61-6 1,2,3-Trichlorobenzene 10 10.6 106 70-130
120-82-1 1,2,4-Trichlorobenzene 10 10.9 109 70-130
71-55-6 1,1,1-Trichloroethane 10 10.7 107 70-130
79-00-5 1,1,2-Trichloroethane 10 10.4 104 70-130
79-01-6 Trichloroethylene 10 10.7 107 70-130
75-69-4 Trichlorofluoromethane 10 12.9 129 60-140
96-18-4 1,2,3-Trichloropropane 10 9.9 99 70-130
95-63-6 1,2,4-Trimethylbenzene 10 10.5 105 70-130
108-67-8 1,3,5-Trimethylbenzene 10 11.7 117 70-130
75-01-4 Vinyl Chloride 10 10.1 101 60-140
m,p-Xylene 20 22.7 114 70-130
95-47-6 o-Xylene 10 11.3 113 70-130
1330-20-7 Xylene (total)30 34.0 113 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 99%70-130%
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 103%70-130%
* = Outside of Control Limits.
53 of 57
FA9404955.2.2
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA94049
Account:GRINCC GRI (Geological Resources Inc.)
Project:Haks' Store; 901 Washington St, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA94208-2MS A0231281.D 500 03/28/22 SS n/a n/a VA3097
FA94208-2MSD A0231282.D 500 03/29/22 SS n/a n/a VA3097
FA94208-2 A0231278.D 500 03/28/22 SS n/a n/a VA3097
The QC reported here applies to the following samples:Method: SM 6200B
FA94049-1
FA94208-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 5600 5000 10400 96 5000 10600 100 2 70-130/20
108-86-1 Bromobenzene ND 5000 4740 95 5000 4920 98 4 70-130/20
74-97-5 Bromochloromethane ND 5000 3940 79 5000 4100 82 4 70-130/20
75-27-4 Bromodichloromethane ND 5000 4690 94 5000 4920 98 5 70-130/20
75-25-2 Bromoform ND 5000 4260 85 5000 4590 92 7 70-130/20
104-51-8 n-Butylbenzene ND 5000 4660 93 5000 4940 99 6 70-130/20
135-98-8 sec-Butylbenzene ND 5000 5590 112 5000 5900 118 5 70-130/20
98-06-6 tert-Butylbenzene ND 5000 5310 106 5000 5610 112 5 70-130/20
56-23-5 Carbon Tetrachloride ND 5000 4960 99 5000 5280 106 6 70-130/20
108-90-7 Chlorobenzene ND 5000 4710 94 5000 4900 98 4 70-130/20
75-00-3 Chloroethane ND 5000 5010 100 5000 6510 130 26*60-140/20
67-66-3 Chloroform ND 5000 4550 91 5000 4750 95 4 70-130/20
95-49-8 o-Chlorotoluene 95.0 J 5000 5210 102 5000 5420 107 4 70-130/20
106-43-4 p-Chlorotoluene ND 5000 4930 99 5000 5150 103 4 70-130/20
124-48-1 Dibromochloromethane ND 5000 4530 91 5000 4720 94 4 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 5000 4710 94 5000 5000 100 6 70-130/20
106-93-4 1,2-Dibromoethane ND 5000 4610 92 5000 4850 97 5 70-130/20
75-71-8 Dichlorodifluoromethane ND 5000 4500 90 5000 5610 112 22*60-140/20
95-50-1 1,2-Dichlorobenzene ND 5000 4820 96 5000 4970 99 3 70-130/20
541-73-1 1,3-Dichlorobenzene ND 5000 4880 98 5000 5070 101 4 70-130/20
106-46-7 1,4-Dichlorobenzene ND 5000 4570 91 5000 4790 96 5 70-130/20
75-34-3 1,1-Dichloroethane ND 5000 4760 95 5000 5030 101 6 70-130/20
107-06-2 1,2-Dichloroethane ND 5000 4590 92 5000 4810 96 5 70-130/20
75-35-4 1,1-Dichloroethylene ND 5000 4980 100 5000 5170 103 4 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 5000 4750 95 5000 4960 99 4 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 5000 4890 98 5000 5090 102 4 70-130/20
78-87-5 1,2-Dichloropropane ND 5000 4810 96 5000 5060 101 5 70-130/20
142-28-9 1,3-Dichloropropane ND 5000 4620 92 5000 4830 97 4 70-130/20
594-20-7 2,2-Dichloropropane ND 5000 4280 86 5000 4540 91 6 70-130/20
563-58-6 1,1-Dichloropropene ND 5000 5190 104 5000 5410 108 4 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 5000 4730 95 5000 5040 101 6 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 5000 4710 94 5000 4950 99 5 70-130/20
108-20-3 Di-Isopropyl Ether ND 5000 4530 91 5000 4750 95 5 70-130/20
100-41-4 Ethylbenzene 2540 5000 7510 99 5000 7720 104 3 70-130/20
87-68-3 Hexachlorobutadiene ND 5000 4950 99 5000 5230 105 6 70-130/20
98-82-8 Isopropylbenzene 100 J 5000 5410 106 5000 5720 112 6 70-130/20
* = Outside of Control Limits.
54 of 57
FA9404955.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA94049
Account:GRINCC GRI (Geological Resources Inc.)
Project:Haks' Store; 901 Washington St, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA94208-2MS A0231281.D 500 03/28/22 SS n/a n/a VA3097
FA94208-2MSD A0231282.D 500 03/29/22 SS n/a n/a VA3097
FA94208-2 A0231278.D 500 03/28/22 SS n/a n/a VA3097
The QC reported here applies to the following samples:Method: SM 6200B
FA94049-1
FA94208-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 5000 4990 100 5000 5280 106 6 70-130/20
74-83-9 Methyl Bromide ND 5000 5000 100 5000 6150 123 21*60-140/20
74-87-3 Methyl Chloride ND 5000 4970 99 5000 6050 121 20 60-140/20
74-95-3 Methylene Bromide ND 5000 4290 86 5000 4450 89 4 70-130/20
75-09-2 Methylene Chloride ND 5000 4860 97 5000 5180 104 6 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 5000 4180 84 5000 4400 88 5 70-130/20
91-20-3 Naphthalene 474 5000 5050 92 5000 5340 97 6 70-130/20
103-65-1 n-Propylbenzene 341 5000 5550 104 5000 5770 109 4 70-130/20
100-42-5 Styrene ND 5000 4790 96 5000 4950 99 3 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 5000 4940 99 5000 5240 105 6 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 5000 5280 106 5000 5500 110 4 70-130/20
127-18-4 Tetrachloroethylene ND 5000 4820 96 5000 4990 100 3 70-130/20
108-88-3 Toluene 22700 5000 26200 70 5000 26500 76 1 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 5000 4730 95 5000 4910 98 4 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 5000 4900 98 5000 5110 102 4 70-130/20
71-55-6 1,1,1-Trichloroethane ND 5000 4780 96 5000 5030 101 5 70-130/20
79-00-5 1,1,2-Trichloroethane ND 5000 4680 94 5000 4920 98 5 70-130/20
79-01-6 Trichloroethylene ND 5000 4650 93 5000 4850 97 4 70-130/20
75-69-4 Trichlorofluoromethane ND 5000 5970 119 5000 7520 150*23*60-140/20
96-18-4 1,2,3-Trichloropropane ND 5000 4580 92 5000 4760 95 4 70-130/20
95-63-6 1,2,4-Trimethylbenzene 2760 5000 7750 100 5000 7990 105 3 70-130/20
108-67-8 1,3,5-Trimethylbenzene 803 5000 6130 107 5000 6430 113 5 70-130/20
75-01-4 Vinyl Chloride ND 5000 4540 91 5000 5760 115 24*60-140/20
m,p-Xylene 9220 10000 19100 99 10000 19600 104 3 70-130/20
95-47-6 o-Xylene 4840 5000 9910 101 5000 10100 105 2 70-130/20
1330-20-7 Xylene (total)14100 15000 29000 99 15000 29700 104 2 70-130/20
CAS No.Surrogate Recoveries MS MSD FA94208-2 Limits
1868-53-7 Dibromofluoromethane 103%103%100%70-130%
17060-07-0 1,2-Dichloroethane-D4 99%99%101%70-130%
2037-26-5 Toluene-D8 102%102%101%70-130%
460-00-4 4-Bromofluorobenzene 103%103%103%70-130%
* = Outside of Control Limits.
55 of 57
FA9404955.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA94049
Account:GRINCC GRI (Geological Resources Inc.)
Project:Haks' Store; 901 Washington St, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA94049-2MS A0231312.D 5000 03/29/22 SS n/a n/a VA3098
FA94049-2MSD A0231313.D 5000 03/29/22 SS n/a n/a VA3098
FA94049-2 A0231308.D 5000 03/29/22 SS n/a n/a VA3098
The QC reported here applies to the following samples:Method: SM 6200B
FA94049-2, FA94049-3, FA94049-4, FA94049-5, FA94049-6, FA94049-7, FA94049-8, FA94049-9, FA94049-10,
FA94049-11, FA94049-12, FA94049-13
FA94049-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene ND 50000 52800 106 50000 52400 105 1 70-130/20
108-86-1 Bromobenzene ND 50000 48400 97 50000 48700 97 1 70-130/20
74-97-5 Bromochloromethane ND 50000 40800 82 50000 41000 82 0 70-130/20
75-27-4 Bromodichloromethane ND 50000 50000 100 50000 50300 101 1 70-130/20
75-25-2 Bromoform ND 50000 44200 88 50000 44400 89 0 70-130/20
104-51-8 n-Butylbenzene ND 50000 47800 96 50000 47100 94 1 70-130/20
135-98-8 sec-Butylbenzene ND 50000 57300 115 50000 56700 113 1 70-130/20
98-06-6 tert-Butylbenzene ND 50000 55400 111 50000 55300 111 0 70-130/20
56-23-5 Carbon Tetrachloride ND 50000 53700 107 50000 52900 106 2 70-130/20
108-90-7 Chlorobenzene ND 50000 48900 98 50000 49200 98 1 70-130/20
75-00-3 Chloroethane ND 50000 51800 104 50000 56700 113 9 60-140/20
67-66-3 Chloroform ND 50000 48700 97 50000 48100 96 1 70-130/20
95-49-8 o-Chlorotoluene ND 50000 53700 107 50000 53300 107 1 70-130/20
106-43-4 p-Chlorotoluene ND 50000 52200 104 50000 51700 103 1 70-130/20
124-48-1 Dibromochloromethane ND 50000 46200 92 50000 46600 93 1 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 50000 47200 94 50000 47500 95 1 70-130/20
106-93-4 1,2-Dibromoethane ND 50000 46100 92 50000 48200 96 4 70-130/20
75-71-8 Dichlorodifluoromethane ND 50000 48000 96 50000 53200 106 10 60-140/20
95-50-1 1,2-Dichlorobenzene ND 50000 49500 99 50000 49500 99 0 70-130/20
541-73-1 1,3-Dichlorobenzene ND 50000 50000 100 50000 49900 100 0 70-130/20
106-46-7 1,4-Dichlorobenzene ND 50000 48200 96 50000 47800 96 1 70-130/20
75-34-3 1,1-Dichloroethane ND 50000 51600 103 50000 51700 103 0 70-130/20
107-06-2 1,2-Dichloroethane ND 50000 49800 100 50000 49900 100 0 70-130/20
75-35-4 1,1-Dichloroethylene ND 50000 54700 109 50000 54400 109 1 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 50000 49000 98 50000 49100 98 0 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 50000 52100 104 50000 52100 104 0 70-130/20
78-87-5 1,2-Dichloropropane ND 50000 51500 103 50000 51800 104 1 70-130/20
142-28-9 1,3-Dichloropropane ND 50000 47300 95 50000 49000 98 4 70-130/20
594-20-7 2,2-Dichloropropane ND 50000 45000 90 50000 44100 88 2 70-130/20
563-58-6 1,1-Dichloropropene ND 50000 54100 108 50000 53500 107 1 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 50000 49700 99 50000 50000 100 1 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 50000 49200 98 50000 50000 100 2 70-130/20
108-20-3 Di-Isopropyl Ether ND 50000 47100 94 50000 48600 97 3 70-130/20
100-41-4 Ethylbenzene 2560 50000 54400 104 50000 54600 104 0 70-130/20
87-68-3 Hexachlorobutadiene ND 50000 49700 99 50000 47900 96 4 70-130/20
98-82-8 Isopropylbenzene ND 50000 53600 107 50000 53600 107 0 70-130/20
* = Outside of Control Limits.
56 of 57
FA9404955.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA94049
Account:GRINCC GRI (Geological Resources Inc.)
Project:Haks' Store; 901 Washington St, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA94049-2MS A0231312.D 5000 03/29/22 SS n/a n/a VA3098
FA94049-2MSD A0231313.D 5000 03/29/22 SS n/a n/a VA3098
FA94049-2 A0231308.D 5000 03/29/22 SS n/a n/a VA3098
The QC reported here applies to the following samples:Method: SM 6200B
FA94049-2, FA94049-3, FA94049-4, FA94049-5, FA94049-6, FA94049-7, FA94049-8, FA94049-9, FA94049-10,
FA94049-11, FA94049-12, FA94049-13
FA94049-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 50000 51900 104 50000 51300 103 1 70-130/20
74-83-9 Methyl Bromide ND 50000 53000 106 50000 56600 113 7 60-140/20
74-87-3 Methyl Chloride ND 50000 48300 97 50000 56800 114 16 60-140/20
74-95-3 Methylene Bromide ND 50000 45300 91 50000 46000 92 2 70-130/20
75-09-2 Methylene Chloride ND 50000 53400 107 50000 53300 107 0 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 50000 43700 87 50000 44300 89 1 70-130/20
91-20-3 Naphthalene ND 50000 44500 89 50000 45300 91 2 70-130/20
103-65-1 n-Propylbenzene ND 50000 54000 108 50000 53800 108 0 70-130/20
100-42-5 Styrene ND 50000 47900 96 50000 48000 96 0 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 50000 51300 103 50000 51500 103 0 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 50000 50700 101 50000 51700 103 2 70-130/20
127-18-4 Tetrachloroethylene ND 50000 48400 97 50000 48800 98 1 70-130/20
108-88-3 Toluene 7770 50000 58300 101 50000 58600 102 1 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 50000 47500 95 50000 47400 95 0 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 50000 47200 94 50000 46700 93 1 70-130/20
71-55-6 1,1,1-Trichloroethane ND 50000 50900 102 50000 51300 103 1 70-130/20
79-00-5 1,1,2-Trichloroethane ND 50000 49300 99 50000 50400 101 2 70-130/20
79-01-6 Trichloroethylene ND 50000 51600 103 50000 50900 102 1 70-130/20
75-69-4 Trichlorofluoromethane ND 50000 67600 135 50000 72200 144*7 60-140/20
96-18-4 1,2,3-Trichloropropane ND 50000 48800 98 50000 48900 98 0 70-130/20
95-63-6 1,2,4-Trimethylbenzene 2670 50000 53400 101 50000 52700 100 1 70-130/20
108-67-8 1,3,5-Trimethylbenzene 1140 J 50000 55500 109 50000 55200 108 1 70-130/20
75-01-4 Vinyl Chloride ND 50000 48800 98 50000 53500 107 9 60-140/20
m,p-Xylene 12200 100000 120000 108 100000 120000 108 0 70-130/20
95-47-6 o-Xylene 6080 50000 59300 106 50000 59400 107 0 70-130/20
1330-20-7 Xylene (total)18300 150000 179000 107 150000 180000 108 1 70-130/20
CAS No.Surrogate Recoveries MS MSD FA94049-2 Limits
1868-53-7 Dibromofluoromethane 101%101%104%70-130%
17060-07-0 1,2-Dichloroethane-D4 105%104%108%70-130%
2037-26-5 Toluene-D8 99%100%101%70-130%
460-00-4 4-Bromofluorobenzene 102%102%104%70-130%
* = Outside of Control Limits.
57 of 57
FA9404955.3.2

APPENDIX C
Contaminant Mass Calculations

Area ID Well ID Area
(ft²)
Average Well
Depth
(ft.)
Average
Depth to
Water
(ft.)
Water Column
Height
(ft)
Volume
(ft³)
Volume
(L)
Effective
Porosity
Effective
Volume
(L)
1
MW-1, MW-2, MW-
5, MW-11, MW-14
& MW-15
12,242.7 15.00 9.35 5.65 69,171 1,958,715 0.20 391,743
Area Date Well Benzene
(μ/L)
Toluene
(μ/L)
Ethylbenzene
(μ/L)
Xylenes
(μ/L)
MTBE
(μ/L)
Naphthalene
(μ/L)
Total
(μ/L)
DTW
(ft.)
Average Water
Column Height
(ft.)
Total Average
Mass
(g)
Percent Red.To Date Red.
MW-1 1850 41,500 4,280 31,500 0 1330 80460.00 10.76
MW-2 71.1 697 2,870 13,800 0 896 18334.10 10.81
MW-5 4940 29,500 2,830 19,400 1220 1040 58930.00 10.82
MW-11 202 118 79.4 260 649 23.6 1332.00 8.85
MW-14 7020 32,700 4,210 22,700 615 1250 68495.00 9.93
MW-15 6400 17,300 1,930 11,900 3050 615 41195.00 9.67
Avg.3413.9 20302.5 2699.9 16593.3 922.3 859.1 44791.02 10.14
MW-1 26.2 7,770 2,560 18,300 0 645 29301.20 9.98
MW-2 0 0 119 334 0 103 556.00 10.08
MW-5 448 16,900 4,400 31,400 525 742 54415.00 10.13
MW-11 1.3 1.4 1.4 1.8 104 0 109.90 8.06
MW-14 2,130 35,600 2,780 19,200 273 739 60722.00 9.21
MW-15 0 0 0 0 0 0 0.00 8.61
Avg.434.25 10045.23 1643.4 11539.3 150.33 371.5 24184.02 9.35
Date
Average Water
Column Height
(ft.)
09/23/09 4.86
03/17/22 5.66
Notes:
• FP: Free Product
• Area of the contaminant plume is calculated from Figure 6.
• Height of the water column is calculated by subtracting the average depth to water from the average well depth of the referenced monitoring wells
• Volume of the contaminant plume is calculated by multiplying the area of the plume by the average height of the water column during each sampling event
• Effective porosity is assumed based on the sub-surface soil profile obtained from well construction records and soil boring logs
• Total mass was calculated by multiplying the total contaminant concentrations for the sampling event with effective volume
• Contaminant mass cannot be calculated in wells containing FP; therefore, the total contaminant mass is based on the known concentrations in the area for each sampling event.
• When areas couldn’t be sampled, the last known concentrations were used in the calculations.
15,093.15
9,482.305.66
APPENDIX C
CONTAMINANT MASS CALCULATIONS
HAK'S STORE (INCIDENT NO. 13273)
Baseline Event
37.2%
15,093 ------
Total Contaminant Mass
(g)
09/23/09 ------
03/17/22 37.2%37.2%
4.86
Area 1
Percent Reduction Compared
to Previous Event Percent Reduction To Date
9,482 37.2%