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HomeMy WebLinkAboutWA-1119_13261_CA_RPTS_20211011_MRP 3502 Hayes Road • Monroe, North Carolina 28110 113 West Firetower Road, Suite G • Winterville, North Carolina 28590 Phone (704) 845-4010 • (888) 870-4133 • Fax (704) 845-4012 Engineering Certification: C-2727 • Geology Certification: C-127 Ground Water Monitoring Report September 2021 Perrytown Service Center 526 Sand Hill Road Colerain, Bertie County North Carolina Facility ID Number: 0-00-0000022792 Incident Number: 13261 GRI Project Number: 2858 Prepared for: Mr. Wood Beasley North East Oil Company, Inc. Post Office Box 1386 Ahoskie, North Carolina 27910 October 11, 2021 William Regenthal, P.G. Project Manager Brett Houghton Staff Scientist ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: October 11, 2021 Perrytown Service Center Project Manager: William Regenthal, P.G. GRI Project No. 2858 i SITE INFORMATION 1. Site Identification  Perrytown Service Center (Facility ID 0-00-0000022792)  Incident Number 13261 – High Risk (H135R)  Location of Source Area: 526 Sand Hill Road Colerain, NC 28677 Bertie County 36.138194°N, 76.803389°W (Topographical Map) 2. Information about Contacts Associated with the Leaking UST System UST Owner North East Oil Company, Inc. Post Office Box 1386 Ahoskie, North Carolina 27910 beah@bent-prises.com 252-398-6022 UST Operator North East Oil Company, Inc. Post Office Box 1386 Ahoskie, North Carolina 27910 beah@bent-prises.com 252-398-6022 Property Owner Stewart J. and William S. White 846 B Perrytown Road Colerain, North Carolina 27924 Email Unknown Phone No. Unknown Property Occupant Stewart J. and William S. White 846 B Perrytown Road Colerain, North Carolina 27924 Email Unknown Phone No. Unknown Consultant/Contractor Geological Resources, Inc. 3502 Hayes Road Monroe, NC 28110 wlr@geologicalresourcesinc.com 704-845-4010 Analytical Laboratory SGS North America, Inc. 4405 Vineland Road, Suite C-15 Orlando, Florida 32811 State Certification No. 573 (407) 425-6700 3. Information about Release  Release was discovered on February 9, 1993  An unknown amount of product was released from the leaking UST System  Two 1,000-gallon gasoline and one 550-gallon gasoline USTs were removed from the site in February 1993. One 2,000-gallon gasoline, one 3,000-gallon gasoline and one 2,000-gallon diesel USTs and associated pumps and product piping are active at the site. ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: October 11, 2021 Perrytown Service Center Project Manager: William Regenthal, P.G. GRI Project No. 2858 ii EXECUTIVE SUMMARY Perrytown Service Center is located at 526 Sand Hill Road in Colerain, Bertie County, North Carolina. The site is currently owned by Stewart J. and William S. White and operated as a petroleum retail facility. Unknown quantities of petroleum products were released to the subsurface. According to available information, two 1,000-gallon gasoline and one 550-gallon gasoline underground storage tanks were removed from the site in February 1993. One 2,000-gallon gasoline, one 3,000-gasoline and one 2,000- gallon diesel USTs remain in use at the site. The adjoining properties are a mixture of residential and commercial properties. One inactive water supply well (WSW-1) was identified within a 250-foot radius of the site. Two potable water supply wells (WSW-3 and WSW-8) were identified within a 1,000-foot radius of the site. Please note, WSW-1 was abandoned in January 2018. The site is currently ranked as high risk due to its proximity to potable water supply wells. Public water is available to the site and surrounding properties within a 1,500-foot radius of the site. On September 13, 2021, eleven monitoring wells and one recovery well were gauged, purged and sampled. Free product was not observed during the September 2021 sampling event. Water supply well WSW-2 was inaccessible and unable to be sampled in September 2021. Ground water samples collected from the monitoring wells were submitted for laboratory analyses using EPA Method 6200B. Concentrations of individual BTEX constituents, naphthalene, n-propylbenzene, methyl chloride, 1,2-DCA, p-isopropyltoluene, 1,2,4-trimethylbenzene and/or 1,3,5-trimethylbenzene that exceeded the MACs were reported in the ground water samples collected from MW-2, MW-9, MW-10, MW-12, MW-23 through MW-27, MW-29, and RW-1. All of the reported contaminant concentrations were less than the GCLs. Contaminant mass at the site has decreased by 64.2% since June 2020. Based on this information, WSW-3 appears to be up-gradient to the release and is no longer in use. The property where WSW-3 is located appears to be vacant and/or abandoned. An additional ground water sampling event including MW-16, MW-17 and MW-19 should be conducted in April 2022 in order to assess the risk to WSW-3. The stability of the contaminant plume should be evaluated. Following the next sampling event, if WSW-3 does not appear to be at risk and the plume is stable and/or decreasing, then the risk classification for the site should be reevaluated. ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: October 11, 2021 Perrytown Service Center Project Manager: William Regenthal, P.G. GRI Project No. 2858 iii ACRONYMS ACM: Asbestos Containing Materials AFVR: Aggressive Fluid-Vapor Recovery ARR: Acknowledgement of Report Receipt AS: Air Sparging AST: Aboveground Storage Tank ASTM: American Society for Testing and Materials BGS: Below Ground Surface CAP: Corrective Action Plan CFR: Code of Federal Regulations CSA: Comprehensive Site Assessment DPE: Dual Phase Extraction DRO: Total Petroleum Hydrocarbons Diesel Range Organics DWM: Division of Waste Management DWR: Department of Water Resources EPA: Environmental Protection Agency EPH: Extractible Petroleum Hydrocarbons ESA: Environmental Site Assessment GCL: Gross Contamination Level GRI: Geological Resources, Inc. GRO: Total Petroleum Hydrocarbons Gasoline Range Organics HERR: HAZMAT Emergency Response and Remediation, Inc. LSA: Limited Site Assessment MAC: Maximum Allowable Concentration as specified in T15A NCAC 2L.0202 MADEP: Massachusetts Department of Environmental Protection MCC: Maximum Contaminant Concentrations MMPE: Mobile Multi-Phase Extraction NAPL: Non-Aqueous Phase Liquid, “Free Product” NCDEQ: North Carolina Department of Environmental Quality NCDOT: North Carolina Department of Transportation NFA: Notice of No Further Action NORR: Notice of Regulatory Requirements NOV: Notice of Violation NPDES: National Pollutant Discharge Elimination System NRP: Notice of Residual Petroleum O&M: Operation and Maintenance PAHs: Polynuclear Aromatic Hydrocarbons PCA: Pre-Construction Assessment RAL: Regulatory Action Level SCLs: Soil Cleanup Level SPCC: Spill Prevention Control and Countermeasures SVE: Soil Vapor Extraction SVOCs: Semi-Volatile Organic Compounds SWPPP: Stormwater Pollution Prevention Plan TCLP: Toxicity Characteristic Leaching Procedure (EPA Method SW-846 1311) TOC: Top of Casing TPH: Total Petroleum Hydrocarbons USGS: United States Geological Survey UST: Underground Storage Tank UVF: Ultraviolet Fluorescence VOCs: Volatile Organic Compounds VPH: Volatile Petroleum Hydrocarbons ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: October 11, 2021 Perrytown Service Center Project Manager: William Regenthal, P.G. GRI Project No. 2858 TABLE OF CONTENTS SITE INFORMATION ............................................................................................................................ i EXECUTIVE SUMMARY ....................................................................................................................... ii ACRONYMS ....................................................................................................................................... iii 1.0 SITE HISTORY AND CHARACTERIZATION ...................................................................................1 2.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL ASSESSMENT INFORMATION ...................................................................................................2 3.0 FREE PRODUCT REMOVAL ........................................................................................................4 4.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS ..................................4 5.0 CONCLUSIONS .........................................................................................................................5 6.0 LIMITATIONS ...........................................................................................................................5 7.0 STATEMENTS AND CERTIFICATION ...........................................................................................5 FIGURES Figure 1: Site Location Map Figure 2: Site Map Figure 3: Site Vicinity Map Figure 4: Water Table Surface Map Figure 5: Ground Water Quality Map Figure 6: Contaminant Mass Area Map TABLES Table 1: UST Owner and Operator Information Table 2: UST System Information Table 3: Water Supply Well Information Table 4: Adjacent Property Owner Information Table 5: Well Construction and Gauging Information Table 6: Summary of Ground Water Sample Analytical Results APPENDICES Appendix A: State Correspondence Appendix B: Laboratory Report – Ground Water Samples Appendix C: Contaminant Mass Calculations ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: October 11, 2021 Perrytown Service Center Project Manager: William Regenthal, P.G. GRI Project No. 2858 1 1.0 SITE HISTORY AND CHARACTERIZATION GRI presents the results of the September 2021 ground water sampling event at the Perrytown Service Center site located at 526 Sand Hill Road in Colerain, Bertie County, North Carolina (Figure 1). These activities were conducted in accordance with GRI Proposal No. 21-568, which was submitted to NCDEQ on September 1, 2021, and was approved as Task Authorization No. 13261-50 on September 3, 2021. State correspondence has been included as Appendix A. The site is currently owned by Stewart J. and William S. White and operated as a petroleum retail facility. Unknown quantities of petroleum products were released to the subsurface. According to available information, two 1,000-gallon gasoline and one 550-gallon gasoline underground storage tanks were removed from the site in February 1993. One 2,000-gallon gasoline, one 3,000-gasoline and one 2,000- gallon diesel USTs remain in use at the site. UST owner/operator information and UST system information are included as Tables 1 and 2, respectively. The Registered Tank Report is shown below: On November 28, 2016, an update to the receptor survey was completed. The adjoining properties are a mixture of residential and commercial properties. One inactive water supply well (WSW-1) was identified within a 250-foot radius of the site. Two potable water supply wells (WSW-3 and WSW-8) were identified within a 1,000-foot radius of the site. Please note, WSW-1 was abandoned in January 2018. The property where WSW-3 is located is now vacant and/or abandoned, and the well is no longer in use. The site is currently ranked as high risk due to its proximity to potable water supply wells. Public water is available to the site and surrounding properties within a 1,500-foot radius of the site. No surface water bodies were identified within 500 feet of the site. A Site Vicinity Map showing the adjacent properties has been included as Figure 2. A Site Map showing the locations of the monitoring wells and the structures on-site ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: October 11, 2021 Perrytown Service Center Project Manager: William Regenthal, P.G. GRI Project No. 2858 2 has been included as Figure 3. Water supply well information is presented in Table 3. Adjacent property owner information is presented in Table 4. Please note that site activities conducted prior to the July 2009 updated receptor survey and ground water sampling event were conducted by past consultants. Although GRI cannot verify the accuracy of information obtained from previous reports, for the purposes of this report, it is assumed to be correct. Please refer to past submittals for further historical information regarding the site. A CAP proposing remediation of the site using a pump and treat system was completed in July 1998; however, no projected milestones were established, and the CAP has never been fully implemented. 2.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL ASSESSMENT INFORMATION On September 13, 2021, eleven Type II monitoring wells (MW-2, MW-9, MW-10, MW-12, MW-23 through MW- 27, MW-29 and MW-31) and one recovery well (RW-1) were gauged. Free product was not observed during the September 2021 gauging event. Please note, WSW-2 was inaccessible and could not be sampled. Depths to ground water in the Type II monitoring wells ranged from 5.90 feet to 6.75 feet below the tops of well casings. Ground water elevations in the Type II monitoring wells ranged from 93.26 feet to 93.94 feet. Ground water flow was generally toward the northwest with a horizontal gradient of less than 0.01 feet per foot. No vertical gradient could be calculated since no telescoping well was gauged. Well construction and gauging information is presented in Table 5. A Water Table Surface Map based on the Type II monitoring wells is included as Figure 4. A summary of the current ground water gauging data is shown below: Well ID Screened Interval (x to y ft. BGS) Bottom of Well (ft. BGS) Top of Casing Elevation (ft.) Depth to Water from Top of Casing (feet) Free Product Thickness (ft.) Ground Water Elevation (ft.) MW-2 6 - 16 16 99.68 5.98 --- 93.70 MW-9 5 - 15 15 100.13 6.70 --- 93.43 MW-10 5 – 15 15 99.95 6.38 --- 93.57 MW-12 5 - 15 15 100.11 6.17 --- 93.94 MW-23 2 - 15 15 100.09 6.50 --- 93.59 MW-24 3 - 13 13 99.57 6.18 --- 93.39 MW-25 5 - 15 15 100.15 6.75 --- 93.40 MW-26 5 - 15 15 99.97 6.53 --- 93.44 MW-27 5 - 15 15 99.41 5.90 --- 93.51 MW-29 1 - 10 10 99.37 6.11 --- 93.26 RW-1 4 – 29.5 29.5 99.98 5.83 --- 94.15 Ground water samples were collected from the monitoring wells on September 13, 2021 and were submitted for laboratory analyses using EPA Method 6200B. Concentrations of individual BTEX constituents, naphthalene, n-propylbenzene, methyl chloride, 1,2-DCA, p-isopropyltoluene, 1,2,4- trimethylbenzene and/or 1,3,5-trimethylbenzene that exceeded the MACs were reported in the ground water samples collected from MW-2, MW-9, MW-10, MW-12, MW-23 through MW-27, MW-29 and RW- 1. All of the reported contaminant concentrations were less than the GCLs. A summary of the analytical ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: October 11, 2021 Perrytown Service Center Project Manager: William Regenthal, P.G. GRI Project No. 2858 3 results for ground water samples collected on September 13, 2021, is presented in Table 6. A Ground Water Quality Map based on the September 2021 data is included as Figure 5. A complete report of laboratory analyses of the ground water samples collected from the monitoring wells during the September 2021 sampling event has been included as Appendix B. A summary of the current ground water analytical data is shown below: Contaminant of Concern  Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene Well ID MACs (mg/l) 1 600 600 500 20 6 GCL (mg/l) 5,000 260,000 80,000 50,000 20,000 6,000 MW-2 150 565 1,210 4,860 <6.3 413 MW-9 10.9 0.31 J 0.27 J 1.5 1.1 4.8 MW-10 96.1 70.2 742 1,010 <2.5 528 MW-12 5.4 23.5 50.3 90.5 <0.25 174 MW-23 171 1,490 356 1,150 <6.3 122 MW-24 144 4.6 J 373 137 101 161 MW-25 63.8 51 31 55.1 <0.25 13.5 MW-26 120 344 72.7 341 <1.3 28.1 MW-27 29.5 37.6 106 232 <0.31 43.0 MW-29 558 7.4 J 229 139 203 125 RW-1 36.9 68.9 138 119 <0.63 106 The baseline contaminant mass at the site was determined based on the total BTEX, MTBE and naphthalene concentrations from the June 2020 ground water sampling event, as well as the maximum historical water column height observed in the target area. The contaminant plume consists of one area (Area 1) based on the benzene concentrations during the June 2020 ground water sampling event. The contaminant mass has decreased by 64.2% in Area 1. Contaminant mass calculations have been included as Appendix C. A map of the contaminant mass areas has been included as Figure 6. A chart depicting the overall trend in contaminant mass is shown below: ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: October 11, 2021 Perrytown Service Center Project Manager: William Regenthal, P.G. GRI Project No. 2858 4 The site is located in the Coastal Plain Physiographic Province of North Carolina. The water table has a seasonal high depth to water of approximately 0.38 feet to 11.13 feet below ground surface (bgs). Please note that while free product recovery events have continued, the full scope of the CAP has not been implemented at the site. Please note that milestones were not established in the CAP. 3.0 FREE PRODUCT REMOVAL Free product has historically been present in MW-10 and RW-1. No free product has been observed at the site since March 2019. An absorbent boom was utilized in RW-1 between the March 2019 and June 2020 sampling events. Following the June 2020 sampling event, the absorbent boom was discarded. 4.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS MMPE events are being conducted at the site as the primary method of corrective action. Due to the site being in the active remediation phase, no natural attenuation monitoring plan is currently in place at the site. Contaminant reduction milestones were not proposed in the CAP. ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: October 11, 2021 Perrytown Service Center Project Manager: William Regenthal, P.G. GRI Project No. 2858 5 5.0 CONCLUSIONS  On September 13, 2021, eleven Type II monitoring wells and one recovery well were gauged, purged and sampled. Please note, WSW-2 was inaccessible and could not be sampled. Free product was not observed during the September 2021 sampling event. Ground water flow was generally toward the northwest with a horizontal gradient of less than 0.01 feet per foot.  Concentrations of individual BTEX constituents, naphthalene, n-propylbenzene, methyl chloride, 1,2-DCA, p-isopropyltoluene, 1,2,4-trimethylbenzene and/or 1,3,5-trimethylbenzene that exceeded the MACs were reported in the ground water samples collected from MW-2, MW-9, MW-10, MW-12, MW-23 through MW-27, MW-29 and RW-1. All of the reported contaminant concentrations were less than the GCLs.  Based on this information, WSW-3 appears to be up-gradient to the release and also is no longer in use. An additional ground water sampling event including MW-16, MW-17 and MW-19 should be conducted in April 2022 in order to assess the risk to WSW-3. The stability of the contaminant plume should be evaluated. Following the next sampling event, if WSW-3 does not appear to be at risk and the plume is stable and/or decreasing, then the risk classification for the site should be reevaluated. 6.0 LIMITATIONS This report has been prepared for the exclusive use of North East Oil Company, Inc. for specific application to the referenced site in Bertie County, North Carolina. The assessment was conducted based on the scope of work and level of effort desired by NCDEQ and with resources adequate only for that scope of work. Our findings have been developed in accordance with generally accepted standards of environmental practices in the State of North Carolina, available information, and our professional judgment. No other warranty is expressed or implied. The data that are presented in this report are indicative of conditions that existed at the precise locations sampled and at the time the samples were collected. In addition, the data obtained from samples would be interpreted as being meaningful with respect to parameters indicated in the laboratory report. No additional information can logically be inferred from these data. 7.0 STATEMENTS AND CERTIFICATION 1 Enter the date the monitoring report was due. n/a Will this report be submitted after the established due date? YES NO 2 Was any required information from the above template missing from this report? YES NO IF the answer to question #1 or# 2 is “YES”, please provide additional information in this cell to explain what was missing and why. 3 If applicable, will any of the proposed attenuation milestones under the schedule approved in the Corrective Action Plan not be met? (within a reasonable margin of error) YES NO FIGURES SITE WSW-1 S WSW-2 S WSW-3 "J WSW-4 S WSW-5 S WSW-6 S WSW-7 S"J WSW-8 WSW-9 S WSW-10 S WSW-11 S WSW-12 S WSW-13 SWSW-14S WSW-15 SWSW-16 S 6847865284 6847866968 684796041268478674466847865348 6847868505 6847868157 6847969986 6847852049 6847859549 6847763177 6847859549 6847861314 6847754976 6847756399 6847864298 6847857912 6847854913 6847976208 6847773180 6847962749 6847868100 6847756399 ³ 0 300 600150 Feet 1 INCH = 300 FEET 1,500-FOOT RADIUS 1,000-FOOT RADIUS 250-FOOT RADIUS Legend Parcel Boundary Road Centerline Pond or Lake FIGURE 2SITE VICINITY MAPPERRYTOWN SERVICE CENTER526 SAND HILL ROADCOLERAIN, BERTIE COUNTYNORTH CAROLINAINDICENT NO. 13261GRI PROJECT NO. 2858 PREPARED BY:GEOLOGICAL RESOURCES, INC.DECEMBER 13, 2016 NOTE:THIS MAP IS BASED ON DATA FROM THEBERTIE COUNTY GIS OF NC. 500-FOOT RADIUS Parcel ID Number6847867446 Water Supply Well Potable Non-Potable "J S TABLES UST ID Number 1A, 2A, and 3A Facility ID Number Owner or Operator? Owner/Operator UST ID Number 3 Facility ID Number Owner or Operator? Owner/Operator UST ID Number 1 & 2 Facility ID Number Owner or Operator? Owner/Operator UST ID Number 3 Facility ID Number Owner or Operator? Owner/Operator UST ID Number 1 & 2 Facility ID Number Owner or Operator? Owner/Operator Post Office Box 1386, Ahoskie, NC 27910 252-862-0236 Name of Owner or Operator Dates of Ownership / Operation Beasley Enterprises, Inc.04/23/1966 - 08/28/1990 Address Telephone Number Address Telephone Number Post Office Box 1386, Ahoskie, NC 27910 252-862-0236 0-022792 0-022792 Name of Owner or Operator Dates of Ownership / Operation Beasley Enterprises, Inc.04/18/1985 - 08/28/1990 526 Sand Hill Road, Colerain, NC 27924 NA Telephone Number TABLE 1 UST OWNER/OPERATOR INFORMATION PERRYTOWN SERVICE CENTER (INCIDENT NO. 13261) 526 Sand Hill Road, Colerain, NC 27924 NA 0-022792 Name of Owner or Operator Dates of Ownership / Operation Hughes Auto Inc.02/01/1991 - Current Address Hughes Auto Inc.08/28/1990 - 02/09/1993 Name of Owner or Operator Dates of Ownership / Operation Address Hughes Auto Inc.08/28/1990 - 02/09/1993 526 Sand Hill Road, Colerain, NC 27924 Telephone Number 0-022792 Name of Owner or Operator Dates of Ownership / Operation Address Telephone Number 0-022792 NA Page 1 of 1 Date: 06/18/20 Was Release Associated with UST System? (Yes / No) 1 Gasoline NA 1,000 04/23/1966 Single Wall Steel 64" x 72"Single Wall FRP Removed (02/09/93)Yes 1A Gasoline NA 2,000 02/01/1991 Single Wall Steel 64" x 12'Other Current No 2 Gasoline NA 550 04/23/1966 Single Wall Steel 46" x 74"Single Wall FRP Removed (02/09/93)Yes 2A Gasoline NA 3,000 02/01/1991 Single Wall Steel 64" x 18'Unknown Current No 3 Gasoline NA 1,000 04/18/1985 Single Wall Steel 64" x 72"Single Wall FRP Removed (02/09/93)Yes 3A Diesel NA 2,000 02/01/1991 Single Wall Steel 64" x 12'Unknown Current No Notes: • FRP: Fiberglass reinforced plastic. TABLE 2 UST SYSTEM INFORMATION PERRYTOWN SERVICE CENTER (INCIDENT NO. 13261) Facility ID # : 0-022792 Status of UST UST ID No. Current or Most Recent Contents Previous Contents Capacity (gallons) Date Installed Construction Details Tank Dimensions Description of Associated Product Piping and Pumps Page 1 of 1 Well #Parcel #Well Owner Owner's Mailing Address Water Supply Well Address Municipal Water Connection Well Use (Potable/ Agricultural, etc.) Distance/Direction from source area of release (ft.) WSW-1 6847-86-5284 Glenda B. Campbell 838 Perrytown Road Colerain, NC 27924 813 Bethany Church Road Colerain, NC 27294 NA Abandoned 250 SW WSW-2 6847-86-4298 Vallarie Baker Evans 403 Willow Branch Road Merry Hill, NC 27957 811 Bethany Church Road Colerain, NC 27294 Yes Not In Use 370 SW WSW-3 6847-86-8100 Vallarie Baker Evans 403 Willow Branch Road Merry Hill, NC 27957 812 Bethany Church Road Colerain, NC 27924 No Potable 360 SSE WSW-4 6847-85-7912 Carla C. Byrd 806 Bethany Church Road Colerain, NC 27924 806 Bethany Church Road Colerain, NC 27924 Yes Non-Potable 560 S WSW-5 6847-85-4913 Walter Bickett Perry, Jr.803 Bethany Church Road Colerain, NC 27924 803 Bethany Church Road Colerain, NC 27924 Yes Not In Use 625 SW WSW-6 6847-85-9549 Rachel H. Perry 802 Bethany Church Road Colerain, NC 27924 747 Bethany Church Road Colerain, NC 27924 Yes Not In Use 710 S WSW-7 6847-96-2749 Cordelia Cofield 515 Sand Hill Road Colerain, NC 27924 515 Sand Hill Road Colerain, NC 27924 Yes Not In Use 560 NE WSW-8 6847-75-4976 Dana Marie & Kelly Collier 9600 Larkview Court Fairfax Station, VA 22039 808 Perrytown Road Colerain, NC 27924 No Potable 910 W WSW-9 6847-96-9986 Willie C. Perry, Heirs 1632 US Highway 17 North Windsor, NC 27983 902 Perrytown Road Colerain, NC 27924 Yes Not In Use 1,430 E WSW-10 6847-85-2049 Bethany Baptist Church 736 Bethany Church Road Colerain, NC 27924 738 Bethany Cburch Road Colerain, NC 28294 Yes Not In Use 1,690 SSW WSW-11 6847-77-3180 Melinda Smth and Renardis Rhymer 15064 116th Road Jamaica, NY 11434 751 Perrytown Road Colerain, NC 27924 Yes Not In Use 1,530 NW WSW-12 6847-97-6208 Roberta Jenkins P.O. Box 984 Windsor, NC 27983 501 Sand Hill Road Colerain, NC 27924 Yes Non-Potable 1,120 NE WSW-13 No Non-Potable 300 W WSW-14 No Non-Potable 340 W WSW-15 No Non-Potable 1,400 SW WSW-16 No Non-Potable 1,430 SW • Water supply wells are keyed to Figure 2. TABLE 3 WATER SUPPLY WELL INFORMATION PERRYTOWN SERVICE STATION (INCIDENT NO. 13261) Date : 12/12/16 Facility ID #: 0-022792 6847-86-1314 Anthony Brian Hughson 749 Bethany Church Road Colerain, NC 27924 818 Perrytown Road Colerain, NC 27924 6847-75-6399 Allen Keith & Mary Hughson 750 Bethany Church Road Colerain, NC 27924 741 Bethany Church Road Colerain, NC 27924 Notes: Page 1 of 1 Date: 12/08/16 Facility ID # : 0-022792 6847-86-7446 (site)Stewart J. and William S. White 846B Perrytown Road Colerain, NC 27924 6847-86-6968 Dana Marie Collier 9600 Larkview Court Fairfax Station, VA 22039 6847-86-8505 Toby and Angela King 522 Sand Hill Road Colerain, NC 27924 6847-96-0412 Hope L. White 846B Perrytown Road Colerain, NC 27924 6847-86-8157 Wayne and Sharon Kelly 414 Sand Hill Road Colerain, NC 27924 6847-86-5348 Venell B. Byrum 809 Bethany Church Road Colerain, NC 27924 Note: • Properties are keyed to Figure 2. TABLE 4 ADJACENT PROPERTY OWNERS PERRYTOWN SERVICE STATION (INCIDENT NO. 13261) Parcel Number Owner/Occupant Name Address Page 1 of 1 Date: 09/28/2021 07/14/09 7.60 ─92.40 04/20/10 2.38 ─97.62 11/30/10 4.39 ─95.61 03/05/12 0.95 ─99.05 12/03/12 8.78 ─91.22 08/28/14 5.25 ─94.75 09/03/15 10.16 ─89.84 05/16/16 2.98 ─97.02 11/28/16 3.61 ─96.39 12/28/17 6.87 ─93.13 07/14/09 7.35 ─92.33 04/20/10 2.14 ─97.54 11/30/10 4.10 ─95.58 01/30/12 2.03 ─97.65 Before MMPE 02/03/12 2.72 ─96.96 After MMPE 03/05/12 0.63 ─99.05 12/03/12 8.46 ─91.22 08/28/14 5.05 ─94.63 09/03/15 9.86 ─89.82 04/11/16 2.44 ─97.24 Before MMPE 04/15/16 2.85 ─96.83 After MMPE 05/16/16 2.43 ─97.25 11/28/16 3.29 ─96.39 12/28/17 6.59 ─93.09 06/12/18 2.65 ─97.03 03/27/19 1.71 ─97.97 06/02/20 0.99 ─98.69 04/28/21 2.01 ─97.67 09/13/21 5.98 ─93.70 07/14/09 6.58 ─93.34 04/20/10 2.30 ─97.62 11/30/10 4.27 ─95.65 03/05/12 0.83 ─99.09 12/03/12 8.60 ─91.32 08/28/14 5.22 ─94.70 09/03/15 9.97 ─89.95 05/16/16 2.81 ─97.11 11/28/16 3.43 ─96.49 12/28/17 6.71 ─93.21 06/12/18 2.30 ─97.62 03/27/19 1.85 ─98.07 06/02/20 1.15 ─98.77 07/14/09 6.15 ─93.82 04/20/10 2.70 ─97.27 11/30/10 5.13 ─94.84 03/05/12 0.78 ─99.19 12/03/12 8.14 ─91.83 08/28/14 5.94 ─94.03 09/03/15 10.62 ─89.35 05/16/16 3.25 ─96.72 11/28/16 4.14 ─95.83 07/14/09 5.70 ─94.10 04/20/10 3.24 ─96.56 11/30/10 NM ─NM 03/05/12 NM ─NM 12/03/12 NM ─NM 08/28/14 NM ─NM 07/14/09 7.28 ─92.59 04/20/10 2.10 ─97.77 11/30/10 NM ─NM 03/05/12 NM ─NM 12/03/12 NM ─NM 08/28/14 NM ─NM 07/14/09 8.30 ─92.15 04/20/10 2.89 ─97.56 11/30/10 4.88 ─95.57 03/05/12 1.35 ─99.10 12/03/12 9.27 ─91.18 08/28/14 5.88 ─94.57 09/03/15 10.69 ─89.76 05/16/16 3.47 ─96.98 11/28/16 4.14 ─96.31 12/28/17 7.42 ─93.03 07/14/09 7.95 ─92.09 04/20/10 2.58 ─97.46 11/30/10 4.59 ─95.45 03/05/12 1.20 ─98.84 12/03/12 8.90 ─91.14 08/28/14 5.54 ─94.50 09/03/15 10.34 ─89.70 05/16/16 2.27 ─97.77 11/28/16 3.90 ─96.14 MW-8 07/01/96 5 5-15 15 100.04 MW-7 07/02/96 5 5-15 15 100.45 MW-6 07/01/96 5 5-15 15 99.87 MW-5 07/01/96 5 5-15 15 99.80 MW-4 (Deep)07/01/96 24 24-29 29 99.97 MW-3 08/02/94 6 6-16 16 99.92 MW-1 08/02/94 6 6-16 16 100.00 99.68166-16608/02/94MW-2 TABLE 5 WELL CONSTRUCTION & GAUGING INFORMATION PERRYTOWN SERVICE CENTER (INCIDENT NO. 13261) Facility ID # : 0-022792 Well ID Date Installed Date Water Level Measured Well Casing Depth (ft. BGS) Screened Interval (x to y ft. BGS) Bottom of Well (ft. BGS) Top of Casing Elevation (ft.) Depth to Water from Top of Casing (feet) Free Product Thickness (ft.) Ground Water Elevation (ft.) Comments Page 1 of 4 Date: 09/28/2021 TABLE 5 WELL CONSTRUCTION & GAUGING INFORMATION PERRYTOWN SERVICE CENTER (INCIDENT NO. 13261) Facility ID # : 0-022792 Well ID Date Installed Date Water Level Measured Well Casing Depth (ft. BGS) Screened Interval (x to y ft. BGS) Bottom of Well (ft. BGS) Top of Casing Elevation (ft.) Depth to Water from Top of Casing (feet) Free Product Thickness (ft.) Ground Water Elevation (ft.) Comments 07/14/09 8.12 ─92.01 04/20/10 2.68 ─97.45 11/30/10 4.69 ─95.44 03/05/12 1.19 ─98.94 12/03/12 9.03 ─91.10 08/28/14 5.70 ─94.43 09/03/15 10.49 ─89.64 04/11/16 3.03 ─97.10 Before MMPE 04/15/16 3.55 ─96.58 After MMPE 05/16/16 3.29 ─96.84 11/28/16 3.96 ─96.17 12/28/17 7.20 ─92.93 06/12/18 2.70 ─97.43 03/27/19 2.21 ─97.92 06/02/20 1.59 ─98.54 04/28/21 2.66 ─97.47 09/13/21 6.70 ─93.43 07/14/09 8.01 0.03 91.97 03/08/10 1.31 0.04 98.67 Before AFVR 03/08/10 2.56 ─97.39 After AFVR 04/20/10 2.43 ─97.52 11/30/10 4.38 ─95.57 01/30/12 2.43 ─97.52 Before MMPE 02/03/12 3.20 ─96.75 After MMPE 03/05/12 0.91 ─99.04 12/03/12 8.80 ─91.15 08/28/14 5.43 ─94.52 07/27/15 8.40 ─91.55 Before MMPE 07/31/15 8.95 ─91.00 After MMPE 09/03/15 10.88 0.77 89.73 04/11/16 2.82 0.06 97.18 Before MMPE 04/15/16 3.47 ─96.48 After MMPE 05/16/16 3.01 ─96.94 11/28/16 3.66 ─96.29 12/28/17 6.95 ─93.00 06/12/18 2.47 ─97.48 02/19/19 1.06 ─98.89 Before AFVR 02/19/19 NM NM NM After AFVR 03/27/19 2.03 ─97.92 06/02/20 1.27 ─98.68 04/28/21 2.40 ─97.55 09/13/21 6.38 ─93.57 07/14/09 NM ─NM 04/20/10 2.04 ─97.29 11/30/10 4.10 ─95.23 03/05/12 0.38 ─98.95 12/03/12 5.99 ─93.34 08/28/14 5.59 ─93.74 09/03/15 5.95 ─93.38 05/16/16 2.75 ─96.58 11/28/16 3.33 ─96.00 12/28/17 5.98 ─93.35 06/12/18 2.10 ─97.23 03/27/19 NM NM NM Not Located 06/02/20 NM NM NM Not Located 07/14/09 8.03 ─92.08 04/20/10 2.80 ─97.31 11/30/10 4.67 ─95.44 03/05/12 NM ─NM 12/03/12 NM ─NM 08/28/14 NM ─NM 12/28/17 7.23 ─92.88 06/12/18 2.66 ─97.45 03/27/19 2.02 ─98.09 04/28/21 2.81 ─97.30 09/13/21 6.17 ─93.94 07/14/09 NM ─NM 04/20/10 2.55 ─97.44 11/30/10 4.68 ─95.31 03/05/12 1.58 ─98.41 12/03/12 8.97 ─91.02 08/28/14 5.60 ─94.39 No Well Cap 09/03/15 10.31 ─89.68 05/16/16 2.99 ─97.00 11/28/16 3.58 ─96.41 MW-14 04/02/97 07/14/09 2 2-12 12 98.81 NM ─NM Destroyed 07/14/09 7.50 ─92.61 04/20/10 2.11 ─98.00 11/30/10 NM ─NM 03/05/12 NM ─NM 12/03/12 NM ─NM 08/28/14 NM ─NM 07/14/09 NM ─NM 04/20/10 2.17 ─97.51 11/30/10 NM ─NM 03/05/12 NM ─NM 12/03/12 NM ─NM 08/28/14 NM ─NM MW-16 04/01/97 2 2-12 12 99.68 MW-15 04/02/97 2 2-12 12 100.11 MW-13 09/13/96 1 1-11 11 99.99 MW-11 09/16/96 1.5 1.5-6.5 6.5 99.33 100.11155-15509/13/96MW-12 99.95155-15507/02/96MW-10 100.1315507/02/96MW-9 5-15 Page 2 of 4 Date: 09/28/2021 TABLE 5 WELL CONSTRUCTION & GAUGING INFORMATION PERRYTOWN SERVICE CENTER (INCIDENT NO. 13261) Facility ID # : 0-022792 Well ID Date Installed Date Water Level Measured Well Casing Depth (ft. BGS) Screened Interval (x to y ft. BGS) Bottom of Well (ft. BGS) Top of Casing Elevation (ft.) Depth to Water from Top of Casing (feet) Free Product Thickness (ft.) Ground Water Elevation (ft.) Comments 07/14/09 6.95 ─92.43 04/20/10 1.55 ─97.83 11/30/10 NM ─NM 03/05/12 NM ─NM 12/03/12 NM ─NM 08/28/14 NM ─NM 07/14/09 8.17 ─92.23 04/20/10 2.76 ─97.64 11/30/10 4.70 ─95.70 03/05/12 NM ─NM 12/03/12 NM ─NM 08/28/14 NM ─NM 07/14/09 NM ─NM 04/20/10 2.18 ─98.28 11/30/10 NM ─NM 03/05/12 NM ─NM 12/03/12 NM ─NM 08/28/14 NM ─NM 04/20/10 2.19 ─Unknown 11/30/10 NM ─NM 03/05/12 NM ─NM 12/03/12 NM ─NM 08/28/14 NM ─NM Not Located 04/20/10 3.24 ─97.47 11/30/10 5.25 ─95.46 03/05/12 NM ─NM 12/03/12 NM ─NM 08/28/14 NM ─NM 09/03/15 11.13 ─89.58 05/16/16 NM NM NM Not Located 11/28/16 4.54 ─96.17 12/28/17 7.80 ─92.91 06/12/18 3.43 ─97.28 03/27/19 2.76 ─-2.76 06/02/20 NM NM NM Not Located 04/28/21 NM NM NM Not Located 04/20/10 2.10 ─97.99 11/30/10 4.50 ─95.59 03/05/12 NM ─NM 12/03/12 NM ─NM 08/28/14 NM ─NM 09/03/15 10.39 ─89.70 05/16/16 NM NM NM Not Located 11/28/16 3.78 ─96.31 12/28/17 7.05 ─93.04 06/12/18 NM NM NM Not Located 03/27/19 1.98 ─-1.98 06/02/20 NM NM NM Not Located 04/28/21 3.72 ─96.37 09/13/21 6.50 ─93.59 11/30/10 4.29 ─95.28 03/05/12 0.75 ─98.82 12/03/12 8.58 ─90.99 08/28/14 5.38 ─94.19 09/03/15 9.97 ─89.60 05/16/16 3.16 ─96.41 11/28/16 3.53 ─96.04 12/28/17 6.73 ─92.84 06/12/18 2.38 ─97.19 03/27/19 1.71 ─-1.71 06/02/20 NM NM NM Not Located 04/28/21 2.40 ─97.17 09/13/21 6.18 ─93.39 11/30/10 4.89 ─95.26 03/05/12 1.45 ─98.70 12/03/12 9.08 ─91.07 08/28/14 5.80 ─94.35 09/03/15 10.48 ─89.67 05/16/16 3.14 ─97.01 11/28/16 3.78 ─96.37 06/12/18 2.66 ─97.49 03/27/19 2.36 ─97.79 06/02/20 1.87 ─98.28 04/28/21 2.64 ─97.51 09/13/21 6.75 ─93.40 11/30/10 4.59 ─95.38 01/30/12 2.42 ─97.55 Before MMPE 02/03/12 3.14 ─96.83 After MMPE 03/05/12 1.19 ─98.78 12/03/12 8.88 ─91.09 08/28/14 5.46 ─94.51 09/03/15 10.29 ─89.68 05/16/16 2.87 ─97.10 11/28/16 3.49 ─96.48 06/12/18 2.40 ─97.57 03/27/19 2.32 ─97.65 06/02/20 1.73 ─98.24 04/28/21 2.43 ─97.54 09/13/21 6.53 ─93.44 155-15511/30/10MW-26 99.97 100.15155-15511/30/10MW-25 99.57133-13311/30/10MW-24 100.09152-15204/05/10MW-23 MW-20 Unknown Unknown Unknown Unknown Unknown 100.71152-15204/05/10MW-22 MW-19 04/03/03 5 5-15 15 100.46 MW-18 04/01/97 2 2-12 12 100.40 MW-17 04/02/97 2 2-12 12 99.38 Page 3 of 4 Date: 09/28/2021 TABLE 5 WELL CONSTRUCTION & GAUGING INFORMATION PERRYTOWN SERVICE CENTER (INCIDENT NO. 13261) Facility ID # : 0-022792 Well ID Date Installed Date Water Level Measured Well Casing Depth (ft. BGS) Screened Interval (x to y ft. BGS) Bottom of Well (ft. BGS) Top of Casing Elevation (ft.) Depth to Water from Top of Casing (feet) Free Product Thickness (ft.) Ground Water Elevation (ft.) Comments 11/30/10 4.05 ─95.36 03/05/12 0.57 ─98.84 12/03/12 8.30 ─91.11 08/28/14 4.98 ─94.43 09/03/15 9.70 ─89.71 05/16/16 2.60 ─96.81 11/28/16 3.10 ─96.31 12/28/17 6.47 ─92.94 06/12/18 1.97 ─97.44 02/19/19 0.55 ─98.86 Before AFVR 02/19/19 NM NM NM After AFVR 03/27/19 1.34 ─98.07 06/02/20 0.86 ─98.55 04/28/21 2.00 ─97.41 09/13/21 5.90 ─93.51 03/05/12 1.15 ─98.26 12/03/12 8.40 ─91.01 08/28/14 4.98 ─94.43 09/03/15 7.19 ─92.22 05/16/16 2.61 ─96.80 11/28/16 3.18 ─96.23 12/28/17 6.50 ─92.91 03/05/12 0.68 ─98.69 12/03/12 8.28 ─91.09 08/28/14 5.38 ─93.99 09/03/15 9.80 ─89.57 04/28/21 2.11 ─97.26 09/13/21 6.11 ─93.26 03/05/12 0.93 ─98.21 12/03/12 8.05 ─91.09 08/28/14 5.05 ─94.09 09/03/15 8.84 ─90.30 MW-31 04/26/21 04/28/21 2 2-12 12 99.34 1.95 ─97.39 07/14/09 9.10 2.10 92.68 03/08/10 1.30 0.78 99.35 Before AFVR 03/08/10 1.92 ─98.06 After AFVR 04/20/10 1.87 0.02 98.13 11/30/10 NM ─NM 01/30/12 1.94 0.15 98.17 Before MMPE 02/03/12 2.61 ─97.37 After MMPE 03/05/12 0.40 ─99.58 12/03/12 8.23 0.04 91.78 07/31/14 4.85 0.15 95.26 Before AFVR 07/31/14 6.81 ─93.17 After AFVR 08/28/14 5.02 0.14 95.08 07/27/15 7.84 0.04 92.17 Before MMPE 07/31/15 8.02 ─91.96 After MMPE 09/03/15 9.76 0.06 90.27 04/11/16 2.14 ─97.84 Before MMPE 04/15/16 2.86 ─97.12 After MMPE 05/16/16 2.80 0.45 97.57 11/28/16 3.11 ─96.87 12/28/17 6.99 0.03 93.02 06/12/18 1.80 0.02 98.20 02/19/19 0.56 ─99.42 Before AFVR 02/19/19 NM NM NM After AFVR 03/27/19 1.45 0.01 98.54 06/02/20 0.71 ---99.27 04/28/21 1.82 ─98.16 09/13/21 5.83 ─94.15 07/14/09 9.03 ─92.48 04/20/10 2.45 ─99.06 11/30/10 NM ─NM 03/05/12 NM ─NM 12/03/12 NM ─NM 08/28/14 NM ─NM 07/14/09 7.34 ─92.62 04/20/10 2.11 ─97.85 11/30/10 NM ─NM 03/05/12 0.74 ─99.22 12/03/12 8.52 ─91.44 08/28/14 5.17 ─94.79 09/03/15 9.93 ─90.03 Notes: • Ground water elevation calculated for the presence of free product (where present) with an assumed density of 0.8581. • ft BGS : feet below ground surface. • NM: Not measured • Top of Casing information obtained from report titled 'Semi Annual Ground Water Monitoring Report', June 19, 2003 by CES Engineering, P.C. RW-3 03/05/02 5 5-30.5 30.5 99.96 RW-2 02/12/02 3 3-28.5 28.5 101.51 99.9829.54-29.5401/28/02RW-1 MW-30 03/05/12 1 1-10 10 99.14 99.37101-10103/05/12MW-29 MW-28 03/05/12 1 1-10 10 99.41 99.41155-15511/30/10MW-27 Page 4 of 4 Date : 09/28/2021 EPA Method 6010B Well IDDate Sampled1 600 600 500 20 6 70 70 70 70 400 400 15 1 30 400 700 10,000 200 5,000 260,000 80,000 50,000 20,000 6,000 5,90 8,800 30,500 26,100 24,500 25,000 15,000 1,000 12,000 NE NE NE NE 07/14/09 6.42 1.05 71.3 26.4 <0.330 60.3 <0.330 1.46 14.8 18.8 140 <0.330 59.4 3.74 J 3.30 J 186 313 <105 367 04/05/10 <0.500 <0.500 <0.500 <1.00 1.53 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 NR NR NR NR NR NR NR 12/01/10 20.3 4.90 J 180 105 1.45 J 66.5 3.47 J 3.39 J 12.7 18.8 235 3.94 J NR NR NR 674 587 <80.0 1,096 03/06/12 <0.13 <0.13 <0.15 <0.30 0.16 J <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR NR NR 12/03/12 1.4 <0.10 0.12 J <0.22 0.68 <0.15 0.77 0.66 5.5 0.21 J <0.10 <0.10 NR NR NR NR NR NR NR 08/28/14 2 0.19 J 24.5 3.4 0.13 J 5.7 0.21 J 0.27 J 3.2 4.6 6.1 <0.10 NR NR NR NR NR NR NR 09/03/15 0.20 J <0.17 1.2 1.4 J 0.19 J 0.6 <0.14 0.37 J 2.5 0.22 J <0.14 <0.14 NR NR NR NR NR NR NR 05/16/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR 11/28/16 1.5 0.23 J 21 10.5 <0.13 9.5 B <0.13 0.18 J 1.9 4.2 26 2.4 NR NR NR NR NR NR NR 12/28/17 0.7 <0.13 2.8 5.2 <0.13 10.7 0.44 J 0.47 J 4.1 5.5 32.1 0.93 NR NR NR NR NR NR NR 07/14/09 1,720 6,050 1,050 4,520 188 288 <16.5 <16.5 59.4 J 129 900 265 2.94 J 18.6 36.3 5,650 3,497 <105 4,218 04/05/10 1,820 6,560 1,410 6,190 210 286 59.0 <25.0 64.0 186 1,460 411 NR NR NR NR NR NR NR 12/01/10 1,500 3,890 780 3,980 306 337 23.9 J 17.2 J 94.2 J 75.2 J 763 193 NR NR NR 17,900 8,795 <80.0 5,226 03/06/12 399 932 103 1,970 41.8 179 3.6 J 4.2 J 11.8 18.6 813 247 NR NR NR NR NR NR NR 12/03/12 1,770 7,530 1,750 6,100 96.1 J 359 <20 <20 64.3 J 229 1,780 489 NR NR NR NR NR NR NR 08/28/14 145 587 790 2,110 <2.5 362 47.4 23 75.6 288 2,090 557 NR NR NR NR NR NR NR 09/03/15 1,680 8,080 1,240 5,150 87.0 J 258 <36 <35 46.5 J 154 1,080 288 NR NR NR NR NR NR NR 05/16/16 207 1,000 1,120 5,070 <6.3 369 B 28.6 13.3 J 60.9 230 1,980 533 NR NR NR NR NR NR NR 11/28/16 188 851 1,150 4,470 <6.3 379 42.8 22.7 J 82.2 276 2,220 654 NR NR NR NR NR NR NR 12/28/17 51.3 213 359 1,120 <1.3 111 7.9 3.8 J 18.5 62.3 500 147 NR NR NR NR NR NR NR 06/12/18 <0.13 <0.13 <0.13 <0.25 0.39 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR 03/27/19 360 1,730 1,510 7,480 <13 433 31.7 J 22.5 J 78.5 249 2,020 557 NR NR NR NR NR NR NR 06/02/20 159 738 935 4,150 <3.1 367 21.9 12.1 J 51.1 177 1,640 411 NR NR NR NR NR NR NR 04/29/21 258 1,180 1,390 6,280 <13 373 23.1 J 15.7 J 59.3 205 1,920 513 NR NR NR NR NR NR NR 09/13/21 150 565 1,210 4,860 <6.3 413 28.4 15.5 J 67.1 216 1,830 507 NR NR NR NR NR NR NRC19-C36 AliphaticsC9-C22 AromaticsMACs (mg/l) GCL (mg/l) MW-1 C5-C8 AliphaticsC9-C18 AliphaticsMTBEContaminant of Concern →BenzeneTolueneEthylbenzeneXylenes1,3,5-TrimethylbenzeneLead1-Methylnaphthalene2-MethylnaphthaleneNaphthalenen-Butylbenzenesec-ButylbeneneIsopropylbenzenen-Propylbenzene1,2,4-TrimethylbenzeneTABLE 6 SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS PERRYTOWN SERVICE CENTER (INCIDENT NO. 13261) Facility ID #: 0-022792 Analytical Method →EPA Method 6200B/EPA602 EPA Method 610 MADEP Methods VPH and EPH MW-2 Page 1 of 11 Date : 09/28/2021 EPA Method 6010B Well IDDate Sampled1 600 600 500 20 6 70 70 70 70 400 400 15 1 30 400 700 10,000 200 5,000 260,000 80,000 50,000 20,000 6,000 5,90 8,800 30,500 26,100 24,500 25,000 15,000 1,000 12,000 NE NE NE NEC19-C36 AliphaticsC9-C22 AromaticsMACs (mg/l) GCL (mg/l)C5-C8 AliphaticsC9-C18 AliphaticsMTBEContaminant of Concern →BenzeneTolueneEthylbenzeneXylenes1,3,5-TrimethylbenzeneLead1-Methylnaphthalene2-MethylnaphthaleneNaphthalenen-Butylbenzenesec-ButylbeneneIsopropylbenzenen-Propylbenzene1,2,4-TrimethylbenzeneTABLE 6 SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS PERRYTOWN SERVICE CENTER (INCIDENT NO. 13261) Facility ID #: 0-022792 Analytical Method →EPA Method 6200B/EPA602 EPA Method 610 MADEP Methods VPH and EPH 07/14/09 33.9 27.0 199 271 <0.330 105 <0.330 4.37 25.4 50.4 232 88.1 <1.50 11.5 J 22.4 881 1,303 <114 1,474 04/05/10 227 435 792 3,250 11.0 297 61.0 9.25 62.3 164 1,290 531 NR NR NR NR NR NR NR 12/01/10 31.6 23.2 301 489 <2.50 115 36.6 7.70 J 35.4 102 778 305 NR NR NR 2,190 2,458 154 5,303 03/06/12 7.3 2.4 J 108 23.2 <0.65 61.9 10 4.5 16.2 45.2 299 89.8 NR NR NR NR NR NR NR 12/03/12 61.1 52.6 624 1,010 <2.0 183 11.6 5.8 J 31.1 105 742 230 NR NR NR NR NR NR NR 08/28/14 6.9 3.3 158 53.6 <0.50 89.7 9.8 5.7 22.6 81.7 443 122 NR NR NR NR NR NR NR 09/03/15 48.5 50.6 525 855 2.3 J 172 8 5 29.9 89.7 568 123 NR NR NR NR NR NR NR 05/16/16 2.3 2 55.3 25.6 0.13 J 35.8 B 6.5 3.3 11 40.2 223 14.6 NR NR NR NR NR NR NR 11/28/16 7 8.4 180 232 <1.3 84.3 B 11.8 6.4 25.7 89.9 555 79.8 NR NR NR NR NR NR NR 12/28/17 5.7 5.3 254 229 <1.3 93.5 7.2 4.2 J 19.9 65.5 420 42.9 NR NR NR NR NR NR NR 06/12/18 19.4 27 224 540 <1.3 126 8.8 5.4 25.5 77 480 195 NR NR NR NR NR NR NR 03/27/19 5.2 4.6 61 30 <0.13 40.1 6.8 3.8 13.1 40.2 130 2 NR NR NR NR NR NR NR 06/02/20 1.0 0.83 18.8 8.3 <0.13 33.6 5.0 2.9 8.8 31.3 21.8 0.46 J NR NR NR NR NR NR NR 07/14/09 0.223 J <0.330 2.43 <1.33 8.45 3.63 <0.330 0.463 J 2.90 2.63 1.96 0.534 J <1.50 <0.600 <1.18 <100 <205 <105 <205 04/05/10 <0.500 <0.500 <0.500 <1.00 2.60 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 NR NR NR NR NR NR NR 12/01/10 <0.140 <0.190 0.161 J <0.220 2.09 <0.500 <0.180 <0.140 0.880 J 0.303 J <0.150 <0.180 NR NR NR <100 <160 <80.0 175 03/06/12 <0.13 <0.13 0.30 J <0.30 2.3 <0.10 <0.10 <0.10 0.40 J 0.36 J <0.10 <0.10 NR NR NR NR NR NR NR 12/03/12 0.52 <0.10 2.4 <0.22 2.2 <0.15 <0.10 <0.10 0.64 0.74 <0.10 <0.10 NR NR NR NR NR NR NR 08/28/14 3.2 0.20 J 6.4 2.2 2.4 0.81 <0.10 0.14 J 2.2 2.8 0.57 0.19 J NR NR NR NR NR NR NR 09/03/15 5.6 0.81 13.5 11.7 0.86 3.2 <0.14 <0.14 1.7 2.9 2.7 <0.14 NR NR NR NR NR NR NR 05/16/16 0.44 J <0.13 0.66 <0.31 1.3 <0.13 <0.13 <0.13 0.78 0.96 <0.13 <0.13 NR NR NR NR NR NR NR 11/28/16 0.40 J 0.15 J 0.67 1.4 J 1.2 0.20 J <0.13 <0.13 0.69 0.23 J 0.53 0.17 J NR NR NR NR NR NR NR 07/14/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <0.330 <0.330 <1.00 <0.330 <0.330 <0.330 32.5 <0.667 <1.31 <100 <205 <105 <205 04/05/10 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 NR NR NR NR NR NR NR 12/01/10 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 03/06/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 12/03/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 08/28/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 07/14/09 <0.200 4.00 <0.670 <1.33 <0.330 <1.00 <0.330 <0.330 <1.00 <0.330 <0.330 <0.330 3.08 <0.632 <1.24 <100 <208 <108 <208 04/05/10 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 NR NR NR NR NR NR NR 12/01/10 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 03/06/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 12/03/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 08/28/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS MW-3 MW-4 MW-5 MW-6 Page 2 of 11 Date : 09/28/2021 EPA Method 6010B Well IDDate Sampled1 600 600 500 20 6 70 70 70 70 400 400 15 1 30 400 700 10,000 200 5,000 260,000 80,000 50,000 20,000 6,000 5,90 8,800 30,500 26,100 24,500 25,000 15,000 1,000 12,000 NE NE NE NEC19-C36 AliphaticsC9-C22 AromaticsMACs (mg/l) GCL (mg/l)C5-C8 AliphaticsC9-C18 AliphaticsMTBEContaminant of Concern →BenzeneTolueneEthylbenzeneXylenes1,3,5-TrimethylbenzeneLead1-Methylnaphthalene2-MethylnaphthaleneNaphthalenen-Butylbenzenesec-ButylbeneneIsopropylbenzenen-Propylbenzene1,2,4-TrimethylbenzeneTABLE 6 SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS PERRYTOWN SERVICE CENTER (INCIDENT NO. 13261) Facility ID #: 0-022792 Analytical Method →EPA Method 6200B/EPA602 EPA Method 610 MADEP Methods VPH and EPH 07/14/09 <0.200 <0.330 11.6 11.3 <0.330 7.07 7.11 2.24 8.37 14.9 41.7 9.76 <1.50 <0.674 3.16 J 1,080 274 <108 245 04/05/10 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 2.39 0.810 <0.500 1.75 5.95 <0.500 NR NR NR NR NR NR NR 12/01/10 <0.700 <0.950 2.70 J <1.10 <1.25 8.74 4.45 J 1.39 J 5.22 7.07 32.1 13.4 NR NR NR 1,290 224 <80.0 468 03/06/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR NR NR 12/03/12 <0.10 <0.10 1.8 <0.22 <0.10 2.1 1.8 1.7 2.3 7.6 10 0.30 J NR NR NR NR NR NR NR 08/28/14 <0.10 <0.10 0.29 J <0.20 <0.10 0.71 0.85 0.56 0.47 J 2.6 2.2 <0.10 NR NR NR NR NR NR NR 09/03/15 <0.17 <0.17 0.16 J <0.43 <0.16 0.19 J 0.38 J 0.61 0.47 J 0.32 J 0.23 J <0.14 NR NR NR NR NR NR NR 05/16/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR 11/28/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 0.17 J 0.15 J <0.13 NR NR NR NR NR NR NR 12/28/17 <0.13 <0.13 <0.13 <0.25 <0.13 0.30 J 0.36 J 0.30 J 0.30 J 1.2 3.5 0.51 NR NR NR NR NR NR NR 07/14/09 12.6 1.94 <0.670 5.98 1.46 <1.00 <0.330 <0.330 <1.00 <0.330 0.968 J <0.330 9.65 <0.674 <1.32 <100 <205 <105 <205 04/05/10 70.7 <0.500 <0.500 <1.00 6.19 <5.00 <0.500 <0.500 0.980 <0.500 0.660 <0.500 NR NR NR NR NR NR NR 12/01/10 24.6 <0.950 <0.750 <1.10 17.0 <2.50 <0.900 <0.700 4.36 J <1.10 5.46 <0.900 NR NR NR 181 174 <80.0 <270 03/06/12 1.7 <0.13 <0.15 <0.30 4.1 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR NR NR 12/03/12 <0.10 <0.10 <0.10 <0.22 1.5 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR 08/28/14 36.8 0.13 J 0.22 J 1.2 J 6.9 1.2 0.16 J 0.46 J 0.40 J 0.15 J 0.91 <0.10 NR NR NR NR NR NR NR 09/03/15 2.8 <0.17 0.66 1.0 J 2.3 0.31 J <0.14 0.19 J 0.34 J <0.16 0.72 <0.14 NR NR NR NR NR NR NR 05/16/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR 11/28/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR 07/14/09 1,590 4,560 1,530 5,200 354 539 <13.2 <13.2 110 268 1,980 586 2.03 44.5 84.6 4,380 5,290 <105 6,915 04/05/10 1,830 6,290 1,500 5,650 328 520 64.2 13.7 86.6 252 1,790 485 NR NR NR NR NR NR NR 12/01/10 380 431 398 1,220 141 204 22.2 13.1 J 38.4 83.4 783 196 NR NR NR 6,780 4,316 <80.0 6,050 03/06/12 298 525 652 1,320 74.0 251 21.0 13.3 64.5 176 1,140 323 NR NR NR NR NR NR NR 12/03/12 2,380 6,270 1,180 3,740 323 350 <25 <25 60.5 J 232 1,570 405 NR NR NR NR NR NR NR 08/28/14 185 409 120 414 25.3 63.2 4.8 J 3.7 J 10.3 30.3 197 40.6 NR NR NR NR NR NR NR 09/03/15 3,990 13,000 1,540 5,870 126 J 323 <72 <69 62.9 J 181 J 1,140 321 NR NR NR NR NR NR NR 05/16/16 1.6 <0.13 <0.13 0.68 J 0.42 J 0.46 JB 0.27 J <0.13 <0.13 <0.13 0.24 J <0.13 NR NR NR NR NR NR NR 11/28/16 0.17 J <0.13 <0.13 <0.31 0.23 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR 12/28/17 243 370 99.1 336 9.1 26.5 1.6 J 1.4 J 4.7 J 11.3 109 26.6 NR NR NR NR NR NR NR 06/12/18 4.3 <0.13 0.42 J 10.3 0.57 2.8 0.17 J 0.15 J 0.57 0.47 J 10.8 0.37 J NR NR NR NR NR NR NR 03/27/19 137 85.6 648 1,770 <2.5 266 11.4 8.2 J 37 123 880 243 NR NR NR NR NR NR NR 06/02/20 22.5 104 80.3 219 <0.63 38.2 1.9 J 1.8 J 8.7 28.7 234 54.6 NR NR NR NR NR NR NR 04/29/21 42.7 3.7 152 292 <0.31 82.3 4.7 3.1 11.2 35.0 300 60.2 NR NR NR NR NR NR NR 09/13/21 10.9 0.31 J 0.27 J 1.5 1.1 4.8 0.14 J 0.27 J 0.41 J 0.14 J 0.65 0.16 J NR NR NR NR NR NR NR MW-9 MW-7 MW-8 Page 3 of 11 Date : 09/28/2021 EPA Method 6010B Well IDDate Sampled1 600 600 500 20 6 70 70 70 70 400 400 15 1 30 400 700 10,000 200 5,000 260,000 80,000 50,000 20,000 6,000 5,90 8,800 30,500 26,100 24,500 25,000 15,000 1,000 12,000 NE NE NE NEC19-C36 AliphaticsC9-C22 AromaticsMACs (mg/l) GCL (mg/l)C5-C8 AliphaticsC9-C18 AliphaticsMTBEContaminant of Concern →BenzeneTolueneEthylbenzeneXylenes1,3,5-TrimethylbenzeneLead1-Methylnaphthalene2-MethylnaphthaleneNaphthalenen-Butylbenzenesec-ButylbeneneIsopropylbenzenen-Propylbenzene1,2,4-TrimethylbenzeneTABLE 6 SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS PERRYTOWN SERVICE CENTER (INCIDENT NO. 13261) Facility ID #: 0-022792 Analytical Method →EPA Method 6200B/EPA602 EPA Method 610 MADEP Methods VPH and EPH 07/14/09 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP 04/05/10 437 1,520 674 3,490 148 423 78.8 35.2 70.3 131 1,430 346 NR NR NR NR NR NR NR 12/01/10 268 708 540 2,740 132 J 553 89.0 J 50.6 J 176 J 114 J 1,650 338 NR NR NR 7,880 167,800 238 46,200 03/06/12 316 982 776 2,850 24.2 360 25.0 25.7 62.0 123 1,080 359 NR NR NR NR NR NR NR 12/03/12 835 4,250 1,030 3,730 28.5 J 334 40.4 J 40.8 J 67.2 193 1,600 415 NR NR NR NR NR NR NR 08/28/14 789 3,160 954 3,910 69.2 478 17.9 J 20.1 J 41.8 J 127 1,320 364 NR NR NR NR NR NR NR 09/03/15 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP 05/16/16 252 624 1,130 5,120 11.4 J 897 B 99.3 71.3 97.1 366 3,940 1,250 NR NR NR NR NR NR NR 11/28/16 174 716 1,550 7,020 9.9 J 1,230 162 131 140 496 7,290 2,830 NR NR NR NR NR NR NR 12/28/17 554 1,410 1,040 3,100 36.7 690 194 117 151 561 2,840 920 NR NR NR NR NR NR NR 06/12/18 132 147 747 1,920 8.8 J 735 55.5 40.9 63.6 193 2,210 751 NR NR NR NR NR NR NR 02/19/19 253 762 873 2,100 10.8 528 NR NR NR NR NR NR NR NR NR NR NR NR NR 03/27/19 215 572 869 2,440 <3.1 895 94.5 68.7 130 419 1,500 1,220 NR NR NR NR NR NR NR 06/02/20 109 106 907 1,650 <2.5 626 32.4 28.7 63.6 205 1,850 685 NR NR NR NR NR NR NR 04/29/21 110 105 753 1,340 <2.5 386 14.2 12.5 34.1 113 1,680 395 NR NR NR NR NR NR NR 09/13/21 96.1 70.2 742 1,010 <2.5 528 34.8 24.6 50.7 167 1,590 562 NR NR NR NR NR NR NR 07/14/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 04/05/10 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 NR NR NR NR NR NR NR 12/01/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.150 <0.220 <0.150 <0.180 NR NR NR <100 268 <100 <312 03/06/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR NR NR 12/03/12 <0.10 0.31 J <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR 08/28/14 6 0.22 J <0.10 0.21 J 0.97 0.53 <0.10 <0.10 0.5 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR 09/03/15 <0.17 4.1 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.12 <0.16 <0.14 <0.14 NR NR NR NR NR NR NR 05/16/16 <0.13 1 <0.13 <0.31 0.18 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR 11/28/16 0.35 J <0.13 <0.13 <0.31 9.4 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR 12/28/17 0.46 J <0.13 <0.13 <0.25 0.45 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR 06/12/18 7 0.67 0.14 J <0.25 7.3 0.19 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR MW-11 MW-10 Page 4 of 11 Date : 09/28/2021 EPA Method 6010B Well IDDate Sampled1 600 600 500 20 6 70 70 70 70 400 400 15 1 30 400 700 10,000 200 5,000 260,000 80,000 50,000 20,000 6,000 5,90 8,800 30,500 26,100 24,500 25,000 15,000 1,000 12,000 NE NE NE NEC19-C36 AliphaticsC9-C22 AromaticsMACs (mg/l) GCL (mg/l)C5-C8 AliphaticsC9-C18 AliphaticsMTBEContaminant of Concern →BenzeneTolueneEthylbenzeneXylenes1,3,5-TrimethylbenzeneLead1-Methylnaphthalene2-MethylnaphthaleneNaphthalenen-Butylbenzenesec-ButylbeneneIsopropylbenzenen-Propylbenzene1,2,4-TrimethylbenzeneTABLE 6 SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS PERRYTOWN SERVICE CENTER (INCIDENT NO. 13261) Facility ID #: 0-022792 Analytical Method →EPA Method 6200B/EPA602 EPA Method 610 MADEP Methods VPH and EPH 07/14/09 24.2 28.0 107 222 <0.330 326 <0.330 13.1 31.9 31.7 289 97.7 <1.50 58.1 76.0 269 2,060 <105 2,173 04/05/10 22.3 2.32 105 112 1.30 536 25.2 16.6 34.2 43.9 385 117 NR NR NR NR NR NR NR 12/01/10 16.1 1.42 J 82.4 68.9 0.856 J 285 12.4 10.8 22.7 29.9 250 72.4 NR NR NR <100 1,254 <80.0 2,580 03/06/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 12/03/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 08/28/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 12/28/17 10.9 23.1 49.4 99 0.36 J 295 7.8 12.7 21.5 32.1 282 46.7 NR NR NR NR NR NR NR 06/12/18 7.6 2.5 J 29.2 42.1 <1.3 258 6.5 12.2 18.4 28.4 116 14.9 NR NR NR NR NR NR NR 03/27/19 5.5 0.82 J 29 48 <0.63 243 6.9 13.1 21.7 35.7 191 31.5 NR NR NR NR NR NR NR 04/29/21 4.8 3.1 25.3 21.0 <0.13 256 5.9 14.3 21.7 39.5 175 7.0 NR NR NR NR NR NR NR 09/13/21 5.4 23.5 50.3 90.5 <0.25 174 4.5 9.5 15.9 27.0 182 12.0 NR NR NR NR NR NR NR 07/14/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 04/05/10 <0.500 <0.500 <0.500 <1.00 6.59 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 NR NR NR NR NR NR NR 12/01/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.150 <0.220 <0.150 <0.180 NR NR NR <100 <160.0 <80.0 <270 03/06/12 <0.13 <0.13 <0.15 <0.30 0.86 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR NR NR 12/03/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR 08/28/14 2.9 J 203 2.7 J <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NR NR NR NR NR NR NR 09/03/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.12 <0.16 <0.14 <0.14 NR NR NR NR NR NR NR 05/16/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR 11/28/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR 07/14/09 <0.200 <0.330 <0.670 <1.33 <0.330 8.03 <0.330 <0.330 <1.00 <0.330 1.93 0.601 J 44.8 <0.682 <1.34 <100 <205 <105 <205 04/05/10 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 NR NR NR NR NR NR NR 12/01/10 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 03/06/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 12/03/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 08/28/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 07/14/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 04/05/10 1,230 12,200 3,280 17,100 <25.0 965 62.0 <25.0 138 326 2,760 686 NR NR NR NR NR NR NR 12/01/10 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 03/06/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 12/03/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 08/28/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS MW-13 MW-16 MW-12 MW-15 Page 5 of 11 Date : 09/28/2021 EPA Method 6010B Well IDDate Sampled1 600 600 500 20 6 70 70 70 70 400 400 15 1 30 400 700 10,000 200 5,000 260,000 80,000 50,000 20,000 6,000 5,90 8,800 30,500 26,100 24,500 25,000 15,000 1,000 12,000 NE NE NE NEC19-C36 AliphaticsC9-C22 AromaticsMACs (mg/l) GCL (mg/l)C5-C8 AliphaticsC9-C18 AliphaticsMTBEContaminant of Concern →BenzeneTolueneEthylbenzeneXylenes1,3,5-TrimethylbenzeneLead1-Methylnaphthalene2-MethylnaphthaleneNaphthalenen-Butylbenzenesec-ButylbeneneIsopropylbenzenen-Propylbenzene1,2,4-TrimethylbenzeneTABLE 6 SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS PERRYTOWN SERVICE CENTER (INCIDENT NO. 13261) Facility ID #: 0-022792 Analytical Method →EPA Method 6200B/EPA602 EPA Method 610 MADEP Methods VPH and EPH 07/14/09 <0.200 <0.330 <0.670 <1.33 <0.330 1.18 J <0.330 <0.330 <1.00 <0.330 <0.330 <0.330 51.7 <0.714 <1.40 <100 <205 <105 <205 04/05/10 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 NR NR NR NR NR NR NR 12/01/10 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 03/06/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 12/03/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 08/28/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 07/14/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <0.330 <0.330 <1.00 <0.330 <0.330 <0.330 21.6 <0.714 <1.40 <100 <205 <105 <205 04/05/10 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 NR NR NR NR NR NR NR 12/01/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.150 <0.220 <0.150 <0.180 NR NR NR <100 <160.0 <80.0 <270 03/06/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 12/03/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 08/28/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 07/14/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 04/05/10 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 NR NR NR NR NR NR NR 12/01/10 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 03/06/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 12/03/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 08/28/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 07/14/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 04/05/10 <0.500 0.620 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 NR NR NR NR NR NR NR 12/01/10 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 03/06/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 12/03/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 08/28/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS MW-17 MW-18 MW-19 MW-20 Page 6 of 11 Date : 09/28/2021 EPA Method 6010B Well IDDate Sampled1 600 600 500 20 6 70 70 70 70 400 400 15 1 30 400 700 10,000 200 5,000 260,000 80,000 50,000 20,000 6,000 5,90 8,800 30,500 26,100 24,500 25,000 15,000 1,000 12,000 NE NE NE NEC19-C36 AliphaticsC9-C22 AromaticsMACs (mg/l) GCL (mg/l)C5-C8 AliphaticsC9-C18 AliphaticsMTBEContaminant of Concern →BenzeneTolueneEthylbenzeneXylenes1,3,5-TrimethylbenzeneLead1-Methylnaphthalene2-MethylnaphthaleneNaphthalenen-Butylbenzenesec-ButylbeneneIsopropylbenzenen-Propylbenzene1,2,4-TrimethylbenzeneTABLE 6 SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS PERRYTOWN SERVICE CENTER (INCIDENT NO. 13261) Facility ID #: 0-022792 Analytical Method →EPA Method 6200B/EPA602 EPA Method 610 MADEP Methods VPH and EPH 04/05/10 153 516 481 1,420 35.6 229 71.6 11.8 95.0 299 1,940 567 NR NR NR NR NR NR NR 12/01/10 24.7 56.7 22.5 77.2 1.99 J 13.4 4.18 J <0.700 8.05 17.0 124 33.3 NR NR NR 631 280 <80.0 471 03/06/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 12/03/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 08/28/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 09/03/15 613 629 457 1,360 120 147 <2.9 <2.8 23.8 73 615 49.2 NR NR NR NR NR NR NR 05/16/16 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 11/28/16 1.1 1.1 0.51 0.69 J 0.39 J 0.26 J <0.13 <0.13 <0.13 0.15 J 0.34 J <0.13 NR NR NR NR NR NR NR 12/28/17 405 104 71.2 519 181 36.5 <1.3 <1.3 4.4 J 11.9 133 56 NR NR NR NR NR NR NR 06/12/18 201 359 199 536 31.6 88.1 2.2 J 1.7 J 17.9 56.9 429 106 NR NR NR NR NR NR NR 03/27/19 45.3 46.1 35 100 <0.13 10 0.31 J 0.23 J 2.5 6.9 37.7 6.9 NR NR NR NR NR NR NR 04/29/21 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 04/05/10 99.4 1,840 1,120 5,650 <2.50 648 146 21.0 112 394 1,880 746 NR NR NR NR NR NR NR 12/01/10 2.00 J 19.4 47.6 175 <1.25 19.9 6.05 <0.700 6.01 8.55 74.3 18.8 NR NR NR 505 358 <80.0 429 03/06/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 12/03/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 08/28/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 09/03/15 185 186 186 481 1.2 42.9 0.48 J 0.44 J 5.9 14.4 80.3 6 NR NR NR NR NR NR NR 05/16/16 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 11/28/16 13.7 3.1 45.3 91.4 <0.25 19.6 0.77 J 0.48 J 3.2 10.6 65 3.2 NR NR NR NR NR NR NR 12/28/17 101 117 109 246 5.1 38.7 0.71 J 0.70 J 4.2 12.1 95.2 15.7 NR NR NR NR NR NR NR 03/27/19 1.9 11 38.1 67.1 <0.25 17.3 2.5 1.1 4.3 15.5 72.2 14.2 NR NR NR NR NR NR NR 04/29/21 10.4 70.7 44 74.5 <0.25 15 0.65 J 0.45 J 2.8 9.2 23.4 2.1 NR NR NR NR NR NR NR 09/13/21 171 1,490 326 1,150 <6.3 122 <6.3 <6.3 11.1 J 33.0 255 43.2 NR NR NR NR NR NR NR MW-22 MW-23 Page 7 of 11 Date : 09/28/2021 EPA Method 6010B Well IDDate Sampled1 600 600 500 20 6 70 70 70 70 400 400 15 1 30 400 700 10,000 200 5,000 260,000 80,000 50,000 20,000 6,000 5,90 8,800 30,500 26,100 24,500 25,000 15,000 1,000 12,000 NE NE NE NEC19-C36 AliphaticsC9-C22 AromaticsMACs (mg/l) GCL (mg/l)C5-C8 AliphaticsC9-C18 AliphaticsMTBEContaminant of Concern →BenzeneTolueneEthylbenzeneXylenes1,3,5-TrimethylbenzeneLead1-Methylnaphthalene2-MethylnaphthaleneNaphthalenen-Butylbenzenesec-ButylbeneneIsopropylbenzenen-Propylbenzene1,2,4-TrimethylbenzeneTABLE 6 SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS PERRYTOWN SERVICE CENTER (INCIDENT NO. 13261) Facility ID #: 0-022792 Analytical Method →EPA Method 6200B/EPA602 EPA Method 610 MADEP Methods VPH and EPH 12/01/10 371 9.15 112 120 489 64.4 8.17 <0.700 16.9 18.2 67.8 42.3 NR NR NR 1,630 453.7 <80.0 734 03/06/12 53.5 0.60 J 0.65 J 0.28 J 74.5 1.5 <0.20 <0.20 1.7 0.98 J 0.25 J 0.63 J NR NR NR NR NR NR NR 12/03/12 <0.10 <0.10 <0.10 <0.22 12.3 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR 08/28/14 258 2.1 J 36.1 55.6 152 49.2 2.5 J 1.8 J 9.3 17.3 105 14.1 NR NR NR NR NR NR NR 09/03/15 269 2.3 J 136 94.3 123 57.4 3.3 J 2.8 J 12.7 36 220 39.3 NR NR NR NR NR NR NR 05/16/16 122 3.4 35 102 14.5 31.7 B 2.3 1.5 6.1 14.3 93.7 14.5 NR NR NR NR NR NR NR 11/28/16 114 2.6 165 168 124 87.4 4.5 3.4 18.2 46.4 251 59.8 NR NR NR NR NR NR NR 12/28/17 0.19 J <0.13 <0.13 <0.25 9.6 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR 06/12/18 181 49.7 434 878 114 172 9.8 6.8 39.6 96.7 623 146 NR NR NR NR NR NR NR 03/27/19 157 5.3 278 259 87.3 105 7.8 5.7 25.9 76.3 455 101 NR NR NR NR NR NR NR 04/29/21 160 81.2 380 485 55 132 6.4 5.1 24.0 82.7 495 98.2 NR NR NR NR NR NR NR 09/13/21 144 4.6 J 373 137 101 161 8.4 6.3 31.1 102 555 114 NR NR NR NR NR NR NR 12/01/10 218 376 73.1 270 88.8 30.4 4.16 J <1.40 9.14 J 7.65 J 64.1 14.3 NR NR NR 1,250 720 101 290 03/06/12 513 1,270 371 1,110 89.3 137 8.5 J <5.1 29.6 81.1 581 153 NR NR NR NR NR NR NR 12/03/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR 08/28/14 320 481 103 350 24.1 49.9 2.7 J 1.8 J 6.3 22.8 135 29.1 NR NR NR NR NR NR NR 09/03/15 61.2 2.6 6.6 17.9 4.6 6.7 0.27 J 0.23 J 0.75 1.1 8.1 1.1 NR NR NR NR NR NR NR 05/16/16 0.40 J <0.13 <0.13 <0.31 0.16 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR 11/28/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR 06/12/18 610 1,650 275 1,070 14.9 94.2 5.4 3.3 16.2 45.6 248 61.5 NR NR NR NR NR NR NR 03/27/19 2,340 8,490 1,220 4,670 <31 329 <31 <31 44.6 J 130 965 261 NR NR NR NR NR NR NR 06/02/20 1,300 6,330 948 3,560 <25 375 <25 <25 33.4 J 105 812 214 NR NR NR NR NR NR NR 04/29/21 573 1,740 580 1,770 <6.3 160 8.6 J 6.5 J 21.6 J 81.7 602 138 NR NR NR NR NR NR NR 09/13/21 63.8 51.0 31.0 55.1 <0.25 13.5 0.63 J 0.43 J 1.5 4.3 26.2 4.5 NR NR NR NR NR NR NR MW-25 MW-24 Page 8 of 11 Date : 09/28/2021 EPA Method 6010B Well IDDate Sampled1 600 600 500 20 6 70 70 70 70 400 400 15 1 30 400 700 10,000 200 5,000 260,000 80,000 50,000 20,000 6,000 5,90 8,800 30,500 26,100 24,500 25,000 15,000 1,000 12,000 NE NE NE NEC19-C36 AliphaticsC9-C22 AromaticsMACs (mg/l) GCL (mg/l)C5-C8 AliphaticsC9-C18 AliphaticsMTBEContaminant of Concern →BenzeneTolueneEthylbenzeneXylenes1,3,5-TrimethylbenzeneLead1-Methylnaphthalene2-MethylnaphthaleneNaphthalenen-Butylbenzenesec-ButylbeneneIsopropylbenzenen-Propylbenzene1,2,4-TrimethylbenzeneTABLE 6 SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS PERRYTOWN SERVICE CENTER (INCIDENT NO. 13261) Facility ID #: 0-022792 Analytical Method →EPA Method 6200B/EPA602 EPA Method 610 MADEP Methods VPH and EPH 12/01/10 844 1,460 335 1,070 283 101 16.1 J <2.80 27.1 36.9 272 53.9 NR NR NR 5,350 1,806.3 <80.0 1,532 03/06/12 2,580 5,970 887 3,280 318 260 <20 <20 50.3 J 125 926 252 NR NR NR NR NR NR NR 12/03/12 219 329 61.7 248 31.2 16.2 0.39 J 0.26 J 2.3 6.7 38.3 9.3 NR NR NR NR NR NR NR 08/28/14 29.6 41.3 9.5 54.2 3.1 4.9 0.13 J <0.10 0.73 1.3 8.5 1.7 NR NR NR NR NR NR NR 09/03/15 469 410 147 495 25.7 56.5 1.4 1.1 8.2 16.8 135 25.7 NR NR NR NR NR NR NR 05/16/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR 11/28/16 <0.13 <0.13 <0.13 <0.31 <0.13 0.17 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR 06/12/18 195 E 235 E 193 E 474 E 7.3 94.1 E 5.9 3.6 18.2 50.9 E 159 E 87.0 E NR NR NR NR NR NR NR 03/27/19 1,570 5,390 811 3,340 <25 209 <25 <25 31.0 J 79.7 J 730 215 NR NR NR NR NR NR NR 06/02/20 138 140 256 526 <1.3 90.6 3.1 J 2.1 J 11.6 37.4 290 68.3 NR NR NR NR NR NR NR 04/29/21 527 846 289 1,370 <3.1 93.4 4.4 J 3.3 J 16.0 40.4 361 80.5 NR NR NR NR NR NR NR 09/13/21 120 344 72.7 341 <1.3 28.1 <1.3 <1.3 3.2 J 7.8 69.2 16.3 NR NR NR NR NR NR NR 12/01/10 282 671 517 1,610 121 176 <1.80 6.02 J 46.5 109 761 209 NR NR NR 2,580 3,427.2 <80.0 3,872 03/06/12 177 88.8 279 762 132 79.6 3.4 J 2.7 J 15.6 30.1 333 90.3 NR NR NR NR NR NR NR 12/03/12 318 855 315 820 48.1 123 5.9 J 4.6 J 20.8 75.7 549 131 NR NR NR NR NR NR NR 08/28/14 128 374 307 803 32.6 127 7.1 4.9 J 24.9 94.8 520 127 NR NR NR NR NR NR NR 09/03/15 2.7 1.9 5.8 9.6 0.84 2.8 <0.14 <0.14 0.43 J 1.9 8.2 0.30 J NR NR NR NR NR NR NR 05/16/16 24 11.7 20.7 36 3.4 7.3 B 0.27 J 0.21 J 1.1 4.1 22.7 1.6 NR NR NR NR NR NR NR 11/28/16 170 592 248 624 10.8 195 6.5 4.6 21.8 67.4 466 104 NR NR NR NR NR NR NR 12/28/17 119 745 139 404 6.6 J 53.6 <2.5 <2.5 8.5 J 25.9 223 51 NR NR NR NR NR NR NR 06/12/18 125 563 412 1,380 23.8 166 3.9 J 3.1 J 17.8 53.5 428 106 NR NR NR NR NR NR NR 02/19/19 2.9 26 9 51.6 <0.13 9.1 NR NR NR NR NR NR NR NR NR NR NR NR NR 03/27/19 112 109 281 762 58.2 96 6.2 4.8 J 23 66.9 417 99.8 NR NR NR NR NR NR NR 06/02/20 860 4,990 1,080 3,670 <25 317 <25 <25 37.6 J 128 992 259 NR NR NR NR NR NR NR 04/29/21 79.9 970 173 574 20.7 50.3 <3.1 <3.1 8.1 J 26.5 253 63.7 NR NR NR NR NR NR NR 09/13/21 29.5 37.6 106 232 <0.31 43.0 2.0 1.8 10 33.3 206 50.5 NR NR NR NR NR NR NR 03/06/12 <0.13 <0.13 <0.15 <0.30 0.60 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR NR NR 12/03/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR 08/28/14 0.22 J 0.22 J <0.10 <0.20 0.37 J 0.20 J <0.10 <0.10 <0.10 <0.10 0.15 J <0.10 NR NR NR NR NR NR NR 09/03/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.12 <0.16 <0.14 <0.14 NR NR NR NR NR NR NR 05/16/16 <0.13 <0.13 <0.13 <0.31 3.1 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR 11/28/16 <0.13 <0.13 <0.13 <0.31 0.95 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR 12/28/17 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR MW-28 MW-27 MW-26 Page 9 of 11 Date : 09/28/2021 EPA Method 6010B Well IDDate Sampled1 600 600 500 20 6 70 70 70 70 400 400 15 1 30 400 700 10,000 200 5,000 260,000 80,000 50,000 20,000 6,000 5,90 8,800 30,500 26,100 24,500 25,000 15,000 1,000 12,000 NE NE NE NEC19-C36 AliphaticsC9-C22 AromaticsMACs (mg/l) GCL (mg/l)C5-C8 AliphaticsC9-C18 AliphaticsMTBEContaminant of Concern →BenzeneTolueneEthylbenzeneXylenes1,3,5-TrimethylbenzeneLead1-Methylnaphthalene2-MethylnaphthaleneNaphthalenen-Butylbenzenesec-ButylbeneneIsopropylbenzenen-Propylbenzene1,2,4-TrimethylbenzeneTABLE 6 SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS PERRYTOWN SERVICE CENTER (INCIDENT NO. 13261) Facility ID #: 0-022792 Analytical Method →EPA Method 6200B/EPA602 EPA Method 610 MADEP Methods VPH and EPH 03/06/12 1.6 <0.13 <0.15 <0.30 1.2 0.35 J <0.10 <0.10 0.15 J <0.11 <0.10 <0.10 NR NR NR NR NR NR NR 12/03/12 <0.10 <0.10 <0.10 <0.22 10.0 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR 08/28/14 439 33.3 371 452 99.8 224 8 4.7 49.2 109 522 173 NR NR NR NR NR NR NR 09/03/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 04/29/21 340 1.9 J 18.6 7.3 J 123 44.7 1.6 J 1.3 J 8.7 22.6 25.7 13.0 NS NS NS NS NS NS NS 09/13/21 558 7.4 J 229 139 203 125 6.5 J 4.7 J 25.9 88.2 148 111 NR NR NR NR NR NR NR 03/06/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR NR NR 12/03/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR 08/28/14 <0.10 <0.10 <0.10 <0.20 1 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR 09/03/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS MW-31 04/29/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NS NS NS NS NS NS NS 07/14/09 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP 04/05/10 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP 12/01/10 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 03/06/12 288 902 455 1,390 49.1 191 5.0 5.9 26.5 44.2 463 115 NR NR NR NR NR NR NR 12/03/12 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP 08/28/14 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP 09/03/15 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP 05/16/16 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP 11/28/16 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 12/28/17 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP 06/12/18 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP 02/19/19 35.2 52.8 66.1 172 2.7 45.8 NR NR NR NR NR NR NR NR NR NR NR NR NR 03/27/19 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP 06/02/20 15.3 3.0 43.9 36.1 <0.13 39.0 0.87 1.0 3.1 8.6 44.4 1.2 NR NR NR NR NR NR NR 04/29/21 30.7 58.4 145 182 <0.31 59.1 0.87 J 1.1 J 5.0 13.2 99.9 8.3 NS NS NS NS NS NS NS 09/13/21 36.9 68.9 138 119 <0.63 106 2.7 3.2 8.6 20.3 84.5 6.0 NS NS NS NS NS NS NS 07/14/09 1.62 0.477 J 1.07 J <1.33 1.97 <1.00 <0.330 <0.330 <1.00 <0.330 1.19 <0.330 18.8 NR NR <100 <211 <111 <211 04/05/10 643 15.0 128 250 652 61.6 3.54 1.36 10.2 19.1 151 11.7 NR NR NR NR NR NR NR 12/01/10 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 03/06/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 12/03/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 08/28/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS MW-29 RW-1 MW-30 RW-2 Page 10 of 11 Date : 09/28/2021 EPA Method 6010B Well IDDate Sampled1 600 600 500 20 6 70 70 70 70 400 400 15 1 30 400 700 10,000 200 5,000 260,000 80,000 50,000 20,000 6,000 5,90 8,800 30,500 26,100 24,500 25,000 15,000 1,000 12,000 NE NE NE NEC19-C36 AliphaticsC9-C22 AromaticsMACs (mg/l) GCL (mg/l)C5-C8 AliphaticsC9-C18 AliphaticsMTBEContaminant of Concern →BenzeneTolueneEthylbenzeneXylenes1,3,5-TrimethylbenzeneLead1-Methylnaphthalene2-MethylnaphthaleneNaphthalenen-Butylbenzenesec-ButylbeneneIsopropylbenzenen-Propylbenzene1,2,4-TrimethylbenzeneTABLE 6 SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS PERRYTOWN SERVICE CENTER (INCIDENT NO. 13261) Facility ID #: 0-022792 Analytical Method →EPA Method 6200B/EPA602 EPA Method 610 MADEP Methods VPH and EPH 07/14/09 496 1,770 902 5,250 <6.60 355 <6.60 <6.60 49.2 86.4 1,010 448 17.1 21.3 34.6 4,490 8,390 240 5,479 04/05/10 439 1,220 630 4,150 16.4 275 27.8 3.40 29.0 64.5 751 349 NR NR NR NR NR NR NR 12/01/10 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 03/06/12 193 611 714 3,160 <2.6 282 10.7 6.2 J 40.0 81.3 953 378 NR NR NR NR NR NR NR 12/03/12 285 1,440 984 5,160 <5.0 325 6.1 J <5.0 39.4 102 1,240 496 NR NR NR NR NR NR NR 08/28/14 311 1,350 1,310 6,670 <5.0 500 17.5 J 12.1 J 70.6 211 1,810 695 NR NR NR NR NR NR NR 09/03/15 136 494 475 2,760 1.8 J 268 7.4 4.2 J 25.3 73.3 917 349 NR NR NR NR NR NR NR 04/05/10 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 NR NR NR NR NR NR NR 12/01/10 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 03/06/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 12/03/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS Notes: • Results reported in µg/l (micrograms per liter). • 2L Standard: as specified in T15A NCAC 2L.0202. • GCL : Gross contamination level. • Concentrations in bold face type exceeded the 2L Standard. • Concentrations of methyl chloride (9.3 Jµg/l in MW-29), 1,2-dichloroethane (1.4 J µg/l in MW-24 and 5.4 J µg/l in MW-29) and p-isopropyltoluene (28.2 µg/l in MW-10) that exceeded the MACs were reported in the ground water sample collected on September 13, 2021. • NE: Standard not established. • NS: Not sampled. • J: Estimated value. • B: Contaminant present in laboratory blank. • E: Value exceeds calibration range. • <: Less than the reporting limit specified in the laboratory report. • For other compounds were detected that did not exceed the 2L Standard or for which no standard has been established, please refer to the laboratory report. RW-3 WSW-3 Page 11 of 11 APPENDICES APPENDIX A State Correspondence ROY COOPER Governor JOHN NICHOLSON Secretary MICHAEL SCOTT Director North Carolina Department of Environmental Quality | Division of Waste Management | UST Section Washington Regional Office | 943 Washington Square Mall | Washington, NC 27889 | (252) 946-6481 June 24, 2021 Lars Simonsen Registered Agent North East Oil Company 106 E. Queen Street P.O. Box 848 Edenton, NC 27932 Re: Notice of Regulatory Requirements 15A NCAC 2L .0106(c) Risk-based Assessment and Corrective Action for Petroleum Underground Storage Tanks Acknowledgement of Report Receipt Perrytown Service Center 526 Sand Hill Road Perrytown, NC 27983 Dear Mr. Simonsen: The UST Section, Division of Waste Management, is in receipt of the Groundwater Monitoring Report dated June 3, 2021 for field activities which were conducted in April 2021. The report was received June 3, 2021. The report indicates continued levels of groundwater contamination, however no free product or GCLs were present. · Continue sampling with the next event in October 2021. · Submit the results of the groundwater sampling activities in a letter report within 30 days of receipt of the analytical results. Because a release or discharge has been confirmed, a Licensed Geologist or a Professional Engineer, certified by the State of North Carolina, is required to prepare and certify all reports submitted to the Department in accordance with Title 15A NCAC 2L .0103(e) and 2L .0111(b). Failure to comply with the State's rules in the manner and time specified may result in the assessment of civil penalties and/or the use of other enforcement mechanisms. If you have any questions regarding the actions or the rules mentioned in this letter, please contact me at the address or telephone number listed below. If you have questions regarding the information contained in this letter, please contact me at the address or telephone number listed below. Sincerely, CJWelti Conrad J. Welti Hydrogeologist Washington Regional Office UST Section, Division of Waste Management, NCDEQ c: GRI, William Regenthal, via email Washington Regional Office | 943 Washington Square Mall | Washington, NC 27889 | (252) 946-6481 2858 Received SEP 07 2021 APPENDIX B Laboratory Report – Ground Water Samples 09/22/21 Technical Report for GRI (Geological Resources Inc.) Perrytown Service Center; 526 Sand Hill Rd, Colerain, NC 13261/2858 SGS Job Number: FA88905 Sampling Date: 09/13/21 Report to: GRI 3502 Hayes Rd Monroe, NC 28110 wlr@geologicalresourcesinc.com; carriekennedy@geologicalresourcesinc.com; jjr@geologicalresourcesinc.com ATTN: William Regenthal Total number of pages in report: Certifications: FL(E83510), LA(03051), KS(E-10327), NC(573), NJ(FL002), NY(12022), SC(96038001) DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177), AL, AK, AR, CT, IA, KY, MA, MI. MS, ND, NH, NV, OK, OR, UT, VT, WA, WV This report shall not be reproduced, except in its entirety, without the written approval of SGS. Test results relate only to samples analyzed. SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: 407-425-6700 • fax: 407-425-0707 Test results contained within this data package meet the requirements of the National Environmental Laboratory Accreditation Program and/or state specific certification programs as applicable. Client Service contact: Muna Mohammed 407-425-6700 Norm Farmer Technical Director Orlando, FL 09/22/21 e-Hardcopy 2.0 Automated Report 52 SGS is the sole authority for authorizing edits or modifications to this document. Unauthorized modification of this report is strictly prohibited. Review standard terms at: http://www.sgs.com/en/terms-and-conditions The results set forth herein are provided by SGS North America Inc. Please share your ideas about how we can serve you better at: EHS.US.CustomerCare@sgs.com 1 of 52 FA88905 Table of Contents -1- Sections: Section 1: Sample Summary ...................................................................................................3 Section 2: Summary of Hits ....................................................................................................4 Section 3: Sample Results ........................................................................................................9 3.1: FA88905-1: MW-2 ........................................................................................................10 3.2: FA88905-2: MW-9 ........................................................................................................12 3.3: FA88905-3: MW-10 ......................................................................................................14 3.4: FA88905-4: MW-12 ......................................................................................................17 3.5: FA88905-5: MW-23 ......................................................................................................20 3.6: FA88905-6: MW-24 ......................................................................................................22 3.7: FA88905-7: MW-25 ......................................................................................................25 3.8: FA88905-8: MW-26 ......................................................................................................28 3.9: FA88905-9: MW-27 ......................................................................................................30 3.10: FA88905-10: MW-29 ..................................................................................................33 3.11: FA88905-11: RW-1 .....................................................................................................35 Section 4: Misc. Forms ............................................................................................................37 4.1: Chain of Custody ...........................................................................................................38 Section 5: MS Volatiles - QC Data Summaries .....................................................................40 5.1: Method Blank Summary ................................................................................................41 5.2: Blank Spike Summary ...................................................................................................45 5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................49 123452 of 52 FA88905 SGS North America Inc. Sample Summary GRI (Geological Resources Inc.) Job No:FA88905 Perrytown Service Center; 526 Sand Hill Rd, Colerain, NC Project No: 13261/2858 Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID This report contains results reported as ND = Not detected. The following applies: Organics ND = Not detected above the MDL FA88905-1 09/13/21 09:22 JH 09/14/21 AQ Ground Water MW-2 FA88905-2 09/13/21 11:19 JH 09/14/21 AQ Ground Water MW-9 FA88905-3 09/13/21 11:30 JH 09/14/21 AQ Ground Water MW-10 FA88905-4 09/13/21 10:52 JH 09/14/21 AQ Ground Water MW-12 FA88905-5 09/13/21 10:33 JH 09/14/21 AQ Ground Water MW-23 FA88905-6 09/13/21 09:54 JH 09/14/21 AQ Ground Water MW-24 FA88905-7 09/13/21 09:35 JH 09/14/21 AQ Ground Water MW-25 FA88905-8 09/13/21 09:45 JH 09/14/21 AQ Ground Water MW-26 FA88905-9 09/13/21 11:07 JH 09/14/21 AQ Ground Water MW-27 FA88905-10 09/13/21 10:09 JH 09/14/21 AQ Ground Water MW-29 FA88905-11 09/13/21 11:50 JH 09/14/21 AQ Ground Water RW-1 3 of 52 FA889051 Summary of Hits Page 1 of 5 Job Number:FA88905 Account:GRI (Geological Resources Inc.) Project:Perrytown Service Center; 526 Sand Hill Rd, Colerain, NC Collected:09/13/21 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method FA88905-1 MW-2 Benzene 150 25 6.3 ug/l SM 6200B n-Butylbenzene 28.4 25 6.3 ug/l SM 6200B sec-Butylbenzene 15.5 J 25 6.3 ug/l SM 6200B Ethylbenzene 1210 25 6.3 ug/l SM 6200B Isopropylbenzene 67.1 25 6.3 ug/l SM 6200B p-Isopropyltoluene 10.0 J 25 6.3 ug/l SM 6200B Methylene Chloride a 69.4 JB 100 50 ug/l SM 6200B Naphthalene 413 25 6.3 ug/l SM 6200B n-Propylbenzene 216 25 6.3 ug/l SM 6200B Toluene 565 25 6.3 ug/l SM 6200B 1,2,4-Trimethylbenzene 1830 25 6.3 ug/l SM 6200B 1,3,5-Trimethylbenzene 507 25 6.3 ug/l SM 6200B m,p-Xylene 3550 50 6.3 ug/l SM 6200B o-Xylene 1310 25 6.3 ug/l SM 6200B Xylene (total)4860 75 13 ug/l SM 6200B FA88905-2 MW-9 Benzene 10.9 0.50 0.13 ug/l SM 6200B n-Butylbenzene 0.14 J 0.50 0.13 ug/l SM 6200B sec-Butylbenzene 0.27 J 0.50 0.13 ug/l SM 6200B Ethylbenzene 0.27 J 0.50 0.13 ug/l SM 6200B Isopropylbenzene 0.41 J 0.50 0.13 ug/l SM 6200B Methyl Tert Butyl Ether 1.1 0.50 0.13 ug/l SM 6200B Naphthalene 4.8 0.50 0.13 ug/l SM 6200B n-Propylbenzene 0.14 J 0.50 0.13 ug/l SM 6200B Toluene 0.31 J 0.50 0.13 ug/l SM 6200B 1,2,4-Trimethylbenzene 0.65 0.50 0.13 ug/l SM 6200B 1,3,5-Trimethylbenzene 0.16 J 0.50 0.13 ug/l SM 6200B m,p-Xylene 0.31 J 1.0 0.13 ug/l SM 6200B o-Xylene 1.1 0.50 0.13 ug/l SM 6200B Xylene (total)1.5 1.5 0.25 ug/l SM 6200B FA88905-3 MW-10 Benzene 96.1 10 2.5 ug/l SM 6200B n-Butylbenzene 34.8 10 2.5 ug/l SM 6200B sec-Butylbenzene 24.6 10 2.5 ug/l SM 6200B Ethylbenzene 742 10 2.5 ug/l SM 6200B Isopropylbenzene 50.7 10 2.5 ug/l SM 6200B p-Isopropyltoluene 28.2 10 2.5 ug/l SM 6200B Methylene Chloride a 29.1 JB 40 20 ug/l SM 6200B Naphthalene 528 10 2.5 ug/l SM 6200B 4 of 52 FA889052 Summary of Hits Page 2 of 5 Job Number:FA88905 Account:GRI (Geological Resources Inc.) Project:Perrytown Service Center; 526 Sand Hill Rd, Colerain, NC Collected:09/13/21 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method n-Propylbenzene 167 10 2.5 ug/l SM 6200B Toluene 70.2 10 2.5 ug/l SM 6200B 1,2,4-Trimethylbenzene 1590 25 6.3 ug/l SM 6200B 1,3,5-Trimethylbenzene 562 10 2.5 ug/l SM 6200B m,p-Xylene 596 20 2.5 ug/l SM 6200B o-Xylene 413 10 2.5 ug/l SM 6200B Xylene (total)1010 30 5.0 ug/l SM 6200B FA88905-4 MW-12 Benzene 5.4 1.0 0.25 ug/l SM 6200B n-Butylbenzene 4.5 1.0 0.25 ug/l SM 6200B sec-Butylbenzene 9.5 1.0 0.25 ug/l SM 6200B tert-Butylbenzene 2.8 1.0 0.25 ug/l SM 6200B Ethylbenzene 50.3 1.0 0.25 ug/l SM 6200B Isopropylbenzene 15.9 1.0 0.25 ug/l SM 6200B p-Isopropyltoluene 2.7 1.0 0.25 ug/l SM 6200B Methylene Chloride a 3.8 JB 4.0 2.0 ug/l SM 6200B Naphthalene 174 2.5 0.63 ug/l SM 6200B n-Propylbenzene 27.0 1.0 0.25 ug/l SM 6200B Toluene 23.5 1.0 0.25 ug/l SM 6200B 1,2,4-Trimethylbenzene 182 2.5 0.63 ug/l SM 6200B 1,3,5-Trimethylbenzene 12.0 1.0 0.25 ug/l SM 6200B m,p-Xylene 54.8 2.0 0.25 ug/l SM 6200B o-Xylene 35.7 1.0 0.25 ug/l SM 6200B Xylene (total)90.5 3.0 0.50 ug/l SM 6200B FA88905-5 MW-23 Benzene 171 25 6.3 ug/l SM 6200B Ethylbenzene 326 25 6.3 ug/l SM 6200B Isopropylbenzene 11.1 J 25 6.3 ug/l SM 6200B Methylene Chloride a 69.6 JB 100 50 ug/l SM 6200B Naphthalene 122 25 6.3 ug/l SM 6200B n-Propylbenzene 33.0 25 6.3 ug/l SM 6200B Toluene 1490 25 6.3 ug/l SM 6200B 1,2,4-Trimethylbenzene 255 25 6.3 ug/l SM 6200B 1,3,5-Trimethylbenzene 43.2 25 6.3 ug/l SM 6200B m,p-Xylene 653 50 6.3 ug/l SM 6200B o-Xylene 495 25 6.3 ug/l SM 6200B Xylene (total)1150 75 13 ug/l SM 6200B FA88905-6 MW-24 Benzene 144 5.0 1.3 ug/l SM 6200B 5 of 52 FA889052 Summary of Hits Page 3 of 5 Job Number:FA88905 Account:GRI (Geological Resources Inc.) Project:Perrytown Service Center; 526 Sand Hill Rd, Colerain, NC Collected:09/13/21 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method n-Butylbenzene 8.4 5.0 1.3 ug/l SM 6200B sec-Butylbenzene 6.3 5.0 1.3 ug/l SM 6200B 1,2-Dichloroethane 1.4 J 5.0 1.3 ug/l SM 6200B Di-Isopropyl Ether 2.4 J 5.0 1.3 ug/l SM 6200B Ethylbenzene 373 5.0 1.3 ug/l SM 6200B Isopropylbenzene 31.1 5.0 1.3 ug/l SM 6200B p-Isopropyltoluene 2.3 J 5.0 1.3 ug/l SM 6200B Methylene Chloride a 16.7 JB 20 10 ug/l SM 6200B Methyl Tert Butyl Ether 101 5.0 1.3 ug/l SM 6200B Naphthalene 161 5.0 1.3 ug/l SM 6200B n-Propylbenzene 102 5.0 1.3 ug/l SM 6200B Toluene 4.6 J 5.0 1.3 ug/l SM 6200B 1,2,4-Trimethylbenzene 555 10 2.5 ug/l SM 6200B 1,3,5-Trimethylbenzene 114 5.0 1.3 ug/l SM 6200B m,p-Xylene 19.3 10 1.3 ug/l SM 6200B o-Xylene 117 5.0 1.3 ug/l SM 6200B Xylene (total)137 15 2.5 ug/l SM 6200B FA88905-7 MW-25 Benzene b 63.8 1.0 0.25 ug/l SM 6200B n-Butylbenzene b 0.63 J 1.0 0.25 ug/l SM 6200B sec-Butylbenzene b 0.43 J 1.0 0.25 ug/l SM 6200B Ethylbenzene b 31.0 1.0 0.25 ug/l SM 6200B Isopropylbenzene b 1.5 1.0 0.25 ug/l SM 6200B Methylene Chloride c 3.7 JB 4.0 2.0 ug/l SM 6200B Naphthalene b 13.5 1.0 0.25 ug/l SM 6200B n-Propylbenzene b 4.3 1.0 0.25 ug/l SM 6200B Toluene b 51.0 1.0 0.25 ug/l SM 6200B 1,2,4-Trimethylbenzene b 26.2 1.0 0.25 ug/l SM 6200B 1,3,5-Trimethylbenzene b 4.5 1.0 0.25 ug/l SM 6200B m,p-Xylene b 17.5 2.0 0.25 ug/l SM 6200B o-Xylene b 37.6 1.0 0.25 ug/l SM 6200B Xylene (total) b 55.1 3.0 0.50 ug/l SM 6200B FA88905-8 MW-26 Benzene 120 5.0 1.3 ug/l SM 6200B Ethylbenzene 72.7 5.0 1.3 ug/l SM 6200B Isopropylbenzene 3.2 J 5.0 1.3 ug/l SM 6200B Methyl Chloride 2.4 J 5.0 2.0 ug/l SM 6200B Methylene Chloride a 15.7 JB 20 10 ug/l SM 6200B Naphthalene 28.1 5.0 1.3 ug/l SM 6200B n-Propylbenzene 7.8 5.0 1.3 ug/l SM 6200B Toluene 344 5.0 1.3 ug/l SM 6200B 6 of 52 FA889052 Summary of Hits Page 4 of 5 Job Number:FA88905 Account:GRI (Geological Resources Inc.) Project:Perrytown Service Center; 526 Sand Hill Rd, Colerain, NC Collected:09/13/21 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method 1,2,4-Trimethylbenzene 69.2 5.0 1.3 ug/l SM 6200B 1,3,5-Trimethylbenzene 16.3 5.0 1.3 ug/l SM 6200B m,p-Xylene 195 10 1.3 ug/l SM 6200B o-Xylene 147 5.0 1.3 ug/l SM 6200B Xylene (total)341 15 2.5 ug/l SM 6200B FA88905-9 MW-27 Benzene 29.5 1.3 0.31 ug/l SM 6200B n-Butylbenzene 2.0 1.3 0.31 ug/l SM 6200B sec-Butylbenzene 1.8 1.3 0.31 ug/l SM 6200B Ethylbenzene 106 1.3 0.31 ug/l SM 6200B Isopropylbenzene 10 1.3 0.31 ug/l SM 6200B p-Isopropyltoluene 0.84 J 1.3 0.31 ug/l SM 6200B Methylene Chloride a 5.4 JB 5.0 2.5 ug/l SM 6200B Naphthalene 43.0 1.3 0.31 ug/l SM 6200B n-Propylbenzene 33.3 1.3 0.31 ug/l SM 6200B Toluene 37.6 1.3 0.31 ug/l SM 6200B 1,2,4-Trimethylbenzene 206 2.5 0.63 ug/l SM 6200B 1,3,5-Trimethylbenzene 50.5 1.3 0.31 ug/l SM 6200B m,p-Xylene 127 2.5 0.31 ug/l SM 6200B o-Xylene 105 1.3 0.31 ug/l SM 6200B Xylene (total)232 3.8 0.63 ug/l SM 6200B FA88905-10 MW-29 Benzene 558 10 2.5 ug/l SM 6200B n-Butylbenzene 6.5 J 10 2.5 ug/l SM 6200B sec-Butylbenzene 4.7 J 10 2.5 ug/l SM 6200B 1,2-Dichloroethane 5.4 J 10 2.5 ug/l SM 6200B Di-Isopropyl Ether 5.9 J 10 2.5 ug/l SM 6200B Ethylbenzene 229 10 2.5 ug/l SM 6200B Isopropylbenzene 25.9 10 2.5 ug/l SM 6200B Methyl Chloride 9.3 J 10 4.0 ug/l SM 6200B Methylene Chloride a 41.8 JB 40 20 ug/l SM 6200B Methyl Tert Butyl Ether 203 10 2.5 ug/l SM 6200B Naphthalene 125 10 2.5 ug/l SM 6200B n-Propylbenzene 88.2 10 2.5 ug/l SM 6200B Toluene 7.4 J 10 2.5 ug/l SM 6200B 1,2,4-Trimethylbenzene 148 10 2.5 ug/l SM 6200B 1,3,5-Trimethylbenzene 111 10 2.5 ug/l SM 6200B o-Xylene 139 10 2.5 ug/l SM 6200B Xylene (total)139 30 5.0 ug/l SM 6200B 7 of 52 FA889052 Summary of Hits Page 5 of 5 Job Number:FA88905 Account:GRI (Geological Resources Inc.) Project:Perrytown Service Center; 526 Sand Hill Rd, Colerain, NC Collected:09/13/21 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method FA88905-11 RW-1 Benzene 36.9 2.5 0.63 ug/l SM 6200B n-Butylbenzene 2.7 2.5 0.63 ug/l SM 6200B sec-Butylbenzene 3.2 2.5 0.63 ug/l SM 6200B Ethylbenzene 138 2.5 0.63 ug/l SM 6200B Isopropylbenzene 8.6 2.5 0.63 ug/l SM 6200B p-Isopropyltoluene 0.99 J 2.5 0.63 ug/l SM 6200B Methylene Chloride a 10.6 JB 10 5.0 ug/l SM 6200B Naphthalene 106 2.5 0.63 ug/l SM 6200B n-Propylbenzene 20.3 2.5 0.63 ug/l SM 6200B Toluene 68.9 2.5 0.63 ug/l SM 6200B 1,2,4-Trimethylbenzene 84.5 2.5 0.63 ug/l SM 6200B 1,3,5-Trimethylbenzene 6.0 2.5 0.63 ug/l SM 6200B m,p-Xylene 51.7 5.0 0.63 ug/l SM 6200B o-Xylene 67.0 2.5 0.63 ug/l SM 6200B Xylene (total)119 7.5 1.3 ug/l SM 6200B (a) Suspected laboratory contaminant. (b) Results from different vials are not consistent; higher results were reported. (c) Results from different vials are not consistent; higher results were reported. Suspected laboratory contaminant. 8 of 52 FA889052 SGS North America Inc. Sample Results Report of Analysis Orlando, FL Section 3 9 of 52 FA889053 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID:MW-2 Lab Sample ID:FA88905-1 Date Sampled:09/13/21 Matrix:AQ - Ground Water Date Received:09/14/21 Method:SM 6200B Percent Solids:n/a Project:Perrytown Service Center; 526 Sand Hill Rd, Colerain, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 E108638.D 50 09/17/21 20:25 JL n/a n/a VE2547 Run #2 Purge Volume Run #1 10.0 ml Run #2 VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene 150 25 6.3 ug/l 108-86-1 Bromobenzene ND 25 6.3 ug/l 74-97-5 Bromochloromethane ND 25 6.3 ug/l 75-27-4 Bromodichloromethane ND 25 6.3 ug/l 75-25-2 Bromoform ND 25 6.3 ug/l 104-51-8 n-Butylbenzene 28.4 25 6.3 ug/l 135-98-8 sec-Butylbenzene 15.5 25 6.3 ug/l J 98-06-6 tert-Butylbenzene ND 25 6.3 ug/l 56-23-5 Carbon Tetrachloride ND 25 6.3 ug/l 108-90-7 Chlorobenzene ND 25 6.3 ug/l 75-00-3 Chloroethane a ND 25 10 ug/l 67-66-3 Chloroform ND 25 6.3 ug/l 95-49-8 o-Chlorotoluene ND 25 6.3 ug/l 106-43-4 p-Chlorotoluene ND 25 6.3 ug/l 124-48-1 Dibromochloromethane ND 25 6.3 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 25 12 ug/l 106-93-4 1,2-Dibromoethane ND 25 6.3 ug/l 75-71-8 Dichlorodifluoromethane ND 25 10 ug/l 95-50-1 1,2-Dichlorobenzene ND 25 6.3 ug/l 541-73-1 1,3-Dichlorobenzene ND 25 6.3 ug/l 106-46-7 1,4-Dichlorobenzene ND 25 6.3 ug/l 75-34-3 1,1-Dichloroethane a ND 25 6.3 ug/l 107-06-2 1,2-Dichloroethane ND 25 6.3 ug/l 75-35-4 1,1-Dichloroethylene a ND 25 6.3 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 25 6.3 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 25 6.3 ug/l 78-87-5 1,2-Dichloropropane ND 25 6.3 ug/l 142-28-9 1,3-Dichloropropane ND 25 6.3 ug/l 594-20-7 2,2-Dichloropropane ND 25 6.3 ug/l 563-58-6 1,1-Dichloropropene ND 25 6.3 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 25 6.3 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 25 6.3 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 10 of 52 FA8890533.1 SGS North America Inc. Report of Analysis Page 2 of 2 Client Sample ID:MW-2 Lab Sample ID:FA88905-1 Date Sampled:09/13/21 Matrix:AQ - Ground Water Date Received:09/14/21 Method:SM 6200B Percent Solids:n/a Project:Perrytown Service Center; 526 Sand Hill Rd, Colerain, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether ND 25 6.3 ug/l 100-41-4 Ethylbenzene 1210 25 6.3 ug/l 87-68-3 Hexachlorobutadiene ND 25 6.3 ug/l 98-82-8 Isopropylbenzene 67.1 25 6.3 ug/l 99-87-6 p-Isopropyltoluene 10.0 25 6.3 ug/l J 74-83-9 Methyl Bromide ND 25 10 ug/l 74-87-3 Methyl Chloride ND 25 10 ug/l 74-95-3 Methylene Bromide ND 25 6.3 ug/l 75-09-2 Methylene Chloride b 69.4 100 50 ug/l JB 1634-04-4 Methyl Tert Butyl Ether ND 25 6.3 ug/l 91-20-3 Naphthalene 413 25 6.3 ug/l 103-65-1 n-Propylbenzene 216 25 6.3 ug/l 100-42-5 Styrene ND 25 6.3 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 25 6.3 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 25 6.3 ug/l 127-18-4 Tetrachloroethylene ND 25 6.3 ug/l 108-88-3 Toluene 565 25 6.3 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 25 6.3 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 25 6.3 ug/l 71-55-6 1,1,1-Trichloroethane ND 25 6.3 ug/l 79-00-5 1,1,2-Trichloroethane ND 25 6.3 ug/l 79-01-6 Trichloroethylene ND 25 6.3 ug/l 75-69-4 Trichlorofluoromethane ND 25 10 ug/l 96-18-4 1,2,3-Trichloropropane ND 25 6.3 ug/l 95-63-6 1,2,4-Trimethylbenzene 1830 25 6.3 ug/l 108-67-8 1,3,5-Trimethylbenzene 507 25 6.3 ug/l 75-01-4 Vinyl Chloride ND 25 6.3 ug/l m,p-Xylene 3550 50 6.3 ug/l 95-47-6 o-Xylene 1310 25 6.3 ug/l 1330-20-7 Xylene (total)4860 75 13 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 97%70-130% 17060-07-0 1,2-Dichloroethane-D4 103%70-130% 2037-26-5 Toluene-D8 97%70-130% 460-00-4 4-Bromofluorobenzene 97%70-130% (a) Associated ECC outside of control limits high, sample was ND. (b) Suspected laboratory contaminant. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 11 of 52 FA8890533.1 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID:MW-9 Lab Sample ID:FA88905-2 Date Sampled:09/13/21 Matrix:AQ - Ground Water Date Received:09/14/21 Method:SM 6200B Percent Solids:n/a Project:Perrytown Service Center; 526 Sand Hill Rd, Colerain, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 E108595.D 1 09/16/21 12:40 JL n/a n/a VE2545 Run #2 Purge Volume Run #1 10.0 ml Run #2 VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene 10.9 0.50 0.13 ug/l 108-86-1 Bromobenzene ND 0.50 0.13 ug/l 74-97-5 Bromochloromethane ND 0.50 0.13 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l 75-25-2 Bromoform ND 0.50 0.13 ug/l 104-51-8 n-Butylbenzene 0.14 0.50 0.13 ug/l J 135-98-8 sec-Butylbenzene 0.27 0.50 0.13 ug/l J 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane ND 0.50 0.20 ug/l 67-66-3 Chloroform ND 0.50 0.13 ug/l 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l 75-71-8 Dichlorodifluoromethane a ND 0.50 0.20 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l 75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l 563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 12 of 52 FA8890533.2 SGS North America Inc. Report of Analysis Page 2 of 2 Client Sample ID:MW-9 Lab Sample ID:FA88905-2 Date Sampled:09/13/21 Matrix:AQ - Ground Water Date Received:09/14/21 Method:SM 6200B Percent Solids:n/a Project:Perrytown Service Center; 526 Sand Hill Rd, Colerain, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l 100-41-4 Ethylbenzene 0.27 0.50 0.13 ug/l J 87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l 98-82-8 Isopropylbenzene 0.41 0.50 0.13 ug/l J 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l 74-83-9 Methyl Bromide ND 0.50 0.20 ug/l 74-87-3 Methyl Chloride ND 0.50 0.20 ug/l 74-95-3 Methylene Bromide ND 0.50 0.13 ug/l 75-09-2 Methylene Chloride ND 2.0 1.0 ug/l B 1634-04-4 Methyl Tert Butyl Ether 1.1 0.50 0.13 ug/l 91-20-3 Naphthalene 4.8 0.50 0.13 ug/l 103-65-1 n-Propylbenzene 0.14 0.50 0.13 ug/l J 100-42-5 Styrene ND 0.50 0.13 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l 108-88-3 Toluene 0.31 0.50 0.13 ug/l J 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l 71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l 79-01-6 Trichloroethylene ND 0.50 0.13 ug/l 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l 95-63-6 1,2,4-Trimethylbenzene 0.65 0.50 0.13 ug/l 108-67-8 1,3,5-Trimethylbenzene 0.16 0.50 0.13 ug/l J 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l m,p-Xylene 0.31 1.0 0.13 ug/l J 95-47-6 o-Xylene 1.1 0.50 0.13 ug/l 1330-20-7 Xylene (total)1.5 1.5 0.25 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 97%70-130% 17060-07-0 1,2-Dichloroethane-D4 97%70-130% 2037-26-5 Toluene-D8 97%70-130% 460-00-4 4-Bromofluorobenzene 99%70-130% (a) Associated BS recovery outside control limits low. Sporadic marginal failure. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 13 of 52 FA8890533.2 SGS North America Inc. Report of Analysis Page 1 of 3 Client Sample ID:MW-10 Lab Sample ID:FA88905-3 Date Sampled:09/13/21 Matrix:AQ - Ground Water Date Received:09/14/21 Method:SM 6200B Percent Solids:n/a Project:Perrytown Service Center; 526 Sand Hill Rd, Colerain, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 E108597.D 20 09/16/21 13:25 JL n/a n/a VE2545 Run #2 E108632.D 50 09/17/21 18:11 JL n/a n/a VE2547 Purge Volume Run #1 10.0 ml Run #2 10.0 ml VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene 96.1 10 2.5 ug/l 108-86-1 Bromobenzene ND 10 2.5 ug/l 74-97-5 Bromochloromethane ND 10 2.5 ug/l 75-27-4 Bromodichloromethane ND 10 2.5 ug/l 75-25-2 Bromoform ND 10 2.5 ug/l 104-51-8 n-Butylbenzene 34.8 10 2.5 ug/l 135-98-8 sec-Butylbenzene 24.6 10 2.5 ug/l 98-06-6 tert-Butylbenzene ND 10 2.5 ug/l 56-23-5 Carbon Tetrachloride ND 10 2.5 ug/l 108-90-7 Chlorobenzene ND 10 2.5 ug/l 75-00-3 Chloroethane ND 10 4.0 ug/l 67-66-3 Chloroform ND 10 2.5 ug/l 95-49-8 o-Chlorotoluene ND 10 2.5 ug/l 106-43-4 p-Chlorotoluene ND 10 2.5 ug/l 124-48-1 Dibromochloromethane ND 10 2.5 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 10 4.9 ug/l 106-93-4 1,2-Dibromoethane ND 10 2.5 ug/l 75-71-8 Dichlorodifluoromethane a ND 10 4.0 ug/l 95-50-1 1,2-Dichlorobenzene ND 10 2.5 ug/l 541-73-1 1,3-Dichlorobenzene ND 10 2.5 ug/l 106-46-7 1,4-Dichlorobenzene ND 10 2.5 ug/l 75-34-3 1,1-Dichloroethane ND 10 2.5 ug/l 107-06-2 1,2-Dichloroethane ND 10 2.5 ug/l 75-35-4 1,1-Dichloroethylene ND 10 2.5 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 10 2.5 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 10 2.5 ug/l 78-87-5 1,2-Dichloropropane ND 10 2.5 ug/l 142-28-9 1,3-Dichloropropane ND 10 2.5 ug/l 594-20-7 2,2-Dichloropropane ND 10 2.5 ug/l 563-58-6 1,1-Dichloropropene ND 10 2.5 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 10 2.5 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 10 2.5 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 14 of 52 FA8890533.3 SGS North America Inc. Report of Analysis Page 2 of 3 Client Sample ID:MW-10 Lab Sample ID:FA88905-3 Date Sampled:09/13/21 Matrix:AQ - Ground Water Date Received:09/14/21 Method:SM 6200B Percent Solids:n/a Project:Perrytown Service Center; 526 Sand Hill Rd, Colerain, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether ND 10 2.5 ug/l 100-41-4 Ethylbenzene 742 10 2.5 ug/l 87-68-3 Hexachlorobutadiene ND 10 2.5 ug/l 98-82-8 Isopropylbenzene 50.7 10 2.5 ug/l 99-87-6 p-Isopropyltoluene 28.2 10 2.5 ug/l 74-83-9 Methyl Bromide ND 10 4.0 ug/l 74-87-3 Methyl Chloride ND 10 4.0 ug/l 74-95-3 Methylene Bromide ND 10 2.5 ug/l 75-09-2 Methylene Chloride b 29.1 40 20 ug/l JB 1634-04-4 Methyl Tert Butyl Ether ND 10 2.5 ug/l 91-20-3 Naphthalene 528 10 2.5 ug/l 103-65-1 n-Propylbenzene 167 10 2.5 ug/l 100-42-5 Styrene ND 10 2.5 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 10 2.5 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 10 2.5 ug/l 127-18-4 Tetrachloroethylene ND 10 2.5 ug/l 108-88-3 Toluene 70.2 10 2.5 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 10 2.5 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 10 2.5 ug/l 71-55-6 1,1,1-Trichloroethane ND 10 2.5 ug/l 79-00-5 1,1,2-Trichloroethane ND 10 2.5 ug/l 79-01-6 Trichloroethylene ND 10 2.5 ug/l 75-69-4 Trichlorofluoromethane ND 10 4.0 ug/l 96-18-4 1,2,3-Trichloropropane ND 10 2.5 ug/l 95-63-6 1,2,4-Trimethylbenzene 1590 c 25 6.3 ug/l 108-67-8 1,3,5-Trimethylbenzene 562 10 2.5 ug/l 75-01-4 Vinyl Chloride ND 10 2.5 ug/l m,p-Xylene 596 20 2.5 ug/l 95-47-6 o-Xylene 413 10 2.5 ug/l 1330-20-7 Xylene (total)1010 30 5.0 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 97%100%70-130% 17060-07-0 1,2-Dichloroethane-D4 97%109%70-130% 2037-26-5 Toluene-D8 97%96%70-130% 460-00-4 4-Bromofluorobenzene 100%95%70-130% (a) Associated BS recovery outside control limits low. Sporadic marginal failure. (b) Suspected laboratory contaminant. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 15 of 52 FA8890533.3 SGS North America Inc. Report of Analysis Page 3 of 3 Client Sample ID:MW-10 Lab Sample ID:FA88905-3 Date Sampled:09/13/21 Matrix:AQ - Ground Water Date Received:09/14/21 Method:SM 6200B Percent Solids:n/a Project:Perrytown Service Center; 526 Sand Hill Rd, Colerain, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q (c) Result is from Run# 2 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 16 of 52 FA8890533.3 SGS North America Inc. Report of Analysis Page 1 of 3 Client Sample ID:MW-12 Lab Sample ID:FA88905-4 Date Sampled:09/13/21 Matrix:AQ - Ground Water Date Received:09/14/21 Method:SM 6200B Percent Solids:n/a Project:Perrytown Service Center; 526 Sand Hill Rd, Colerain, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 E108598.D 2 09/16/21 13:47 JL n/a n/a VE2545 Run #2 E108633.D 5 09/17/21 18:34 JL n/a n/a VE2547 Purge Volume Run #1 10.0 ml Run #2 10.0 ml VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene 5.4 1.0 0.25 ug/l 108-86-1 Bromobenzene ND 1.0 0.25 ug/l 74-97-5 Bromochloromethane ND 1.0 0.25 ug/l 75-27-4 Bromodichloromethane ND 1.0 0.25 ug/l 75-25-2 Bromoform ND 1.0 0.25 ug/l 104-51-8 n-Butylbenzene 4.5 1.0 0.25 ug/l 135-98-8 sec-Butylbenzene 9.5 1.0 0.25 ug/l 98-06-6 tert-Butylbenzene 2.8 1.0 0.25 ug/l 56-23-5 Carbon Tetrachloride ND 1.0 0.25 ug/l 108-90-7 Chlorobenzene ND 1.0 0.25 ug/l 75-00-3 Chloroethane ND 1.0 0.40 ug/l 67-66-3 Chloroform ND 1.0 0.25 ug/l 95-49-8 o-Chlorotoluene ND 1.0 0.25 ug/l 106-43-4 p-Chlorotoluene ND 1.0 0.25 ug/l 124-48-1 Dibromochloromethane ND 1.0 0.25 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 1.0 0.49 ug/l 106-93-4 1,2-Dibromoethane ND 1.0 0.25 ug/l 75-71-8 Dichlorodifluoromethane a ND 1.0 0.40 ug/l 95-50-1 1,2-Dichlorobenzene ND 1.0 0.25 ug/l 541-73-1 1,3-Dichlorobenzene ND 1.0 0.25 ug/l 106-46-7 1,4-Dichlorobenzene ND 1.0 0.25 ug/l 75-34-3 1,1-Dichloroethane ND 1.0 0.25 ug/l 107-06-2 1,2-Dichloroethane ND 1.0 0.25 ug/l 75-35-4 1,1-Dichloroethylene ND 1.0 0.25 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 1.0 0.25 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 1.0 0.25 ug/l 78-87-5 1,2-Dichloropropane ND 1.0 0.25 ug/l 142-28-9 1,3-Dichloropropane ND 1.0 0.25 ug/l 594-20-7 2,2-Dichloropropane ND 1.0 0.25 ug/l 563-58-6 1,1-Dichloropropene ND 1.0 0.25 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 1.0 0.25 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 1.0 0.25 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 17 of 52 FA8890533.4 SGS North America Inc. Report of Analysis Page 2 of 3 Client Sample ID:MW-12 Lab Sample ID:FA88905-4 Date Sampled:09/13/21 Matrix:AQ - Ground Water Date Received:09/14/21 Method:SM 6200B Percent Solids:n/a Project:Perrytown Service Center; 526 Sand Hill Rd, Colerain, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether ND 1.0 0.25 ug/l 100-41-4 Ethylbenzene 50.3 1.0 0.25 ug/l 87-68-3 Hexachlorobutadiene ND 1.0 0.25 ug/l 98-82-8 Isopropylbenzene 15.9 1.0 0.25 ug/l 99-87-6 p-Isopropyltoluene 2.7 1.0 0.25 ug/l 74-83-9 Methyl Bromide ND 1.0 0.40 ug/l 74-87-3 Methyl Chloride ND 1.0 0.40 ug/l 74-95-3 Methylene Bromide ND 1.0 0.25 ug/l 75-09-2 Methylene Chloride b 3.8 4.0 2.0 ug/l JB 1634-04-4 Methyl Tert Butyl Ether ND 1.0 0.25 ug/l 91-20-3 Naphthalene 174 c 2.5 0.63 ug/l 103-65-1 n-Propylbenzene 27.0 1.0 0.25 ug/l 100-42-5 Styrene ND 1.0 0.25 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 1.0 0.25 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 0.25 ug/l 127-18-4 Tetrachloroethylene ND 1.0 0.25 ug/l 108-88-3 Toluene 23.5 1.0 0.25 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 1.0 0.25 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 1.0 0.25 ug/l 71-55-6 1,1,1-Trichloroethane ND 1.0 0.25 ug/l 79-00-5 1,1,2-Trichloroethane ND 1.0 0.25 ug/l 79-01-6 Trichloroethylene ND 1.0 0.25 ug/l 75-69-4 Trichlorofluoromethane ND 1.0 0.40 ug/l 96-18-4 1,2,3-Trichloropropane ND 1.0 0.25 ug/l 95-63-6 1,2,4-Trimethylbenzene 182 c 2.5 0.63 ug/l 108-67-8 1,3,5-Trimethylbenzene 12.0 1.0 0.25 ug/l 75-01-4 Vinyl Chloride ND 1.0 0.25 ug/l m,p-Xylene 54.8 2.0 0.25 ug/l 95-47-6 o-Xylene 35.7 1.0 0.25 ug/l 1330-20-7 Xylene (total)90.5 3.0 0.50 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 96%100%70-130% 17060-07-0 1,2-Dichloroethane-D4 96%105%70-130% 2037-26-5 Toluene-D8 95%95%70-130% 460-00-4 4-Bromofluorobenzene 100%96%70-130% (a) Associated BS recovery outside control limits low. Sporadic marginal failure. (b) Suspected laboratory contaminant. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 18 of 52 FA8890533.4 SGS North America Inc. Report of Analysis Page 3 of 3 Client Sample ID:MW-12 Lab Sample ID:FA88905-4 Date Sampled:09/13/21 Matrix:AQ - Ground Water Date Received:09/14/21 Method:SM 6200B Percent Solids:n/a Project:Perrytown Service Center; 526 Sand Hill Rd, Colerain, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q (c) Result is from Run# 2 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 19 of 52 FA8890533.4 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID:MW-23 Lab Sample ID:FA88905-5 Date Sampled:09/13/21 Matrix:AQ - Ground Water Date Received:09/14/21 Method:SM 6200B Percent Solids:n/a Project:Perrytown Service Center; 526 Sand Hill Rd, Colerain, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 E108634.D 50 09/17/21 18:56 JL n/a n/a VE2547 Run #2 Purge Volume Run #1 10.0 ml Run #2 VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene 171 25 6.3 ug/l 108-86-1 Bromobenzene ND 25 6.3 ug/l 74-97-5 Bromochloromethane ND 25 6.3 ug/l 75-27-4 Bromodichloromethane ND 25 6.3 ug/l 75-25-2 Bromoform ND 25 6.3 ug/l 104-51-8 n-Butylbenzene ND 25 6.3 ug/l 135-98-8 sec-Butylbenzene ND 25 6.3 ug/l 98-06-6 tert-Butylbenzene ND 25 6.3 ug/l 56-23-5 Carbon Tetrachloride ND 25 6.3 ug/l 108-90-7 Chlorobenzene ND 25 6.3 ug/l 75-00-3 Chloroethane a ND 25 10 ug/l 67-66-3 Chloroform ND 25 6.3 ug/l 95-49-8 o-Chlorotoluene ND 25 6.3 ug/l 106-43-4 p-Chlorotoluene ND 25 6.3 ug/l 124-48-1 Dibromochloromethane ND 25 6.3 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 25 12 ug/l 106-93-4 1,2-Dibromoethane ND 25 6.3 ug/l 75-71-8 Dichlorodifluoromethane ND 25 10 ug/l 95-50-1 1,2-Dichlorobenzene ND 25 6.3 ug/l 541-73-1 1,3-Dichlorobenzene ND 25 6.3 ug/l 106-46-7 1,4-Dichlorobenzene ND 25 6.3 ug/l 75-34-3 1,1-Dichloroethane a ND 25 6.3 ug/l 107-06-2 1,2-Dichloroethane ND 25 6.3 ug/l 75-35-4 1,1-Dichloroethylene a ND 25 6.3 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 25 6.3 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 25 6.3 ug/l 78-87-5 1,2-Dichloropropane ND 25 6.3 ug/l 142-28-9 1,3-Dichloropropane ND 25 6.3 ug/l 594-20-7 2,2-Dichloropropane ND 25 6.3 ug/l 563-58-6 1,1-Dichloropropene ND 25 6.3 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 25 6.3 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 25 6.3 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 20 of 52 FA8890533.5 SGS North America Inc. Report of Analysis Page 2 of 2 Client Sample ID:MW-23 Lab Sample ID:FA88905-5 Date Sampled:09/13/21 Matrix:AQ - Ground Water Date Received:09/14/21 Method:SM 6200B Percent Solids:n/a Project:Perrytown Service Center; 526 Sand Hill Rd, Colerain, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether ND 25 6.3 ug/l 100-41-4 Ethylbenzene 326 25 6.3 ug/l 87-68-3 Hexachlorobutadiene ND 25 6.3 ug/l 98-82-8 Isopropylbenzene 11.1 25 6.3 ug/l J 99-87-6 p-Isopropyltoluene ND 25 6.3 ug/l 74-83-9 Methyl Bromide ND 25 10 ug/l 74-87-3 Methyl Chloride ND 25 10 ug/l 74-95-3 Methylene Bromide ND 25 6.3 ug/l 75-09-2 Methylene Chloride b 69.6 100 50 ug/l JB 1634-04-4 Methyl Tert Butyl Ether ND 25 6.3 ug/l 91-20-3 Naphthalene 122 25 6.3 ug/l 103-65-1 n-Propylbenzene 33.0 25 6.3 ug/l 100-42-5 Styrene ND 25 6.3 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 25 6.3 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 25 6.3 ug/l 127-18-4 Tetrachloroethylene ND 25 6.3 ug/l 108-88-3 Toluene 1490 25 6.3 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 25 6.3 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 25 6.3 ug/l 71-55-6 1,1,1-Trichloroethane ND 25 6.3 ug/l 79-00-5 1,1,2-Trichloroethane ND 25 6.3 ug/l 79-01-6 Trichloroethylene ND 25 6.3 ug/l 75-69-4 Trichlorofluoromethane ND 25 10 ug/l 96-18-4 1,2,3-Trichloropropane ND 25 6.3 ug/l 95-63-6 1,2,4-Trimethylbenzene 255 25 6.3 ug/l 108-67-8 1,3,5-Trimethylbenzene 43.2 25 6.3 ug/l 75-01-4 Vinyl Chloride ND 25 6.3 ug/l m,p-Xylene 653 50 6.3 ug/l 95-47-6 o-Xylene 495 25 6.3 ug/l 1330-20-7 Xylene (total)1150 75 13 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 97%70-130% 17060-07-0 1,2-Dichloroethane-D4 101%70-130% 2037-26-5 Toluene-D8 97%70-130% 460-00-4 4-Bromofluorobenzene 98%70-130% (a) Associated ECC outside of control limits high, sample was ND. (b) Suspected laboratory contaminant. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 21 of 52 FA8890533.5 SGS North America Inc. Report of Analysis Page 1 of 3 Client Sample ID:MW-24 Lab Sample ID:FA88905-6 Date Sampled:09/13/21 Matrix:AQ - Ground Water Date Received:09/14/21 Method:SM 6200B Percent Solids:n/a Project:Perrytown Service Center; 526 Sand Hill Rd, Colerain, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 E108600.D 10 09/16/21 14:32 JL n/a n/a VE2545 Run #2 E108635.D 20 09/17/21 19:18 JL n/a n/a VE2547 Purge Volume Run #1 10.0 ml Run #2 10.0 ml VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene 144 5.0 1.3 ug/l 108-86-1 Bromobenzene ND 5.0 1.3 ug/l 74-97-5 Bromochloromethane ND 5.0 1.3 ug/l 75-27-4 Bromodichloromethane ND 5.0 1.3 ug/l 75-25-2 Bromoform ND 5.0 1.3 ug/l 104-51-8 n-Butylbenzene 8.4 5.0 1.3 ug/l 135-98-8 sec-Butylbenzene 6.3 5.0 1.3 ug/l 98-06-6 tert-Butylbenzene ND 5.0 1.3 ug/l 56-23-5 Carbon Tetrachloride ND 5.0 1.3 ug/l 108-90-7 Chlorobenzene ND 5.0 1.3 ug/l 75-00-3 Chloroethane ND 5.0 2.0 ug/l 67-66-3 Chloroform ND 5.0 1.3 ug/l 95-49-8 o-Chlorotoluene ND 5.0 1.3 ug/l 106-43-4 p-Chlorotoluene ND 5.0 1.3 ug/l 124-48-1 Dibromochloromethane ND 5.0 1.3 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 5.0 2.5 ug/l 106-93-4 1,2-Dibromoethane ND 5.0 1.3 ug/l 75-71-8 Dichlorodifluoromethane a ND 5.0 2.0 ug/l 95-50-1 1,2-Dichlorobenzene ND 5.0 1.3 ug/l 541-73-1 1,3-Dichlorobenzene ND 5.0 1.3 ug/l 106-46-7 1,4-Dichlorobenzene ND 5.0 1.3 ug/l 75-34-3 1,1-Dichloroethane ND 5.0 1.3 ug/l 107-06-2 1,2-Dichloroethane 1.4 5.0 1.3 ug/l J 75-35-4 1,1-Dichloroethylene ND 5.0 1.3 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.3 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.3 ug/l 78-87-5 1,2-Dichloropropane ND 5.0 1.3 ug/l 142-28-9 1,3-Dichloropropane ND 5.0 1.3 ug/l 594-20-7 2,2-Dichloropropane ND 5.0 1.3 ug/l 563-58-6 1,1-Dichloropropene ND 5.0 1.3 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.3 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.3 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 22 of 52 FA8890533.6 SGS North America Inc. Report of Analysis Page 2 of 3 Client Sample ID:MW-24 Lab Sample ID:FA88905-6 Date Sampled:09/13/21 Matrix:AQ - Ground Water Date Received:09/14/21 Method:SM 6200B Percent Solids:n/a Project:Perrytown Service Center; 526 Sand Hill Rd, Colerain, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether 2.4 5.0 1.3 ug/l J 100-41-4 Ethylbenzene 373 5.0 1.3 ug/l 87-68-3 Hexachlorobutadiene ND 5.0 1.3 ug/l 98-82-8 Isopropylbenzene 31.1 5.0 1.3 ug/l 99-87-6 p-Isopropyltoluene 2.3 5.0 1.3 ug/l J 74-83-9 Methyl Bromide ND 5.0 2.0 ug/l 74-87-3 Methyl Chloride ND 5.0 2.0 ug/l 74-95-3 Methylene Bromide ND 5.0 1.3 ug/l 75-09-2 Methylene Chloride b 16.7 20 10 ug/l JB 1634-04-4 Methyl Tert Butyl Ether 101 5.0 1.3 ug/l 91-20-3 Naphthalene 161 5.0 1.3 ug/l 103-65-1 n-Propylbenzene 102 5.0 1.3 ug/l 100-42-5 Styrene ND 5.0 1.3 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 5.0 1.3 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 1.3 ug/l 127-18-4 Tetrachloroethylene ND 5.0 1.3 ug/l 108-88-3 Toluene 4.6 5.0 1.3 ug/l J 87-61-6 1,2,3-Trichlorobenzene ND 5.0 1.3 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.3 ug/l 71-55-6 1,1,1-Trichloroethane ND 5.0 1.3 ug/l 79-00-5 1,1,2-Trichloroethane ND 5.0 1.3 ug/l 79-01-6 Trichloroethylene ND 5.0 1.3 ug/l 75-69-4 Trichlorofluoromethane ND 5.0 2.0 ug/l 96-18-4 1,2,3-Trichloropropane ND 5.0 1.3 ug/l 95-63-6 1,2,4-Trimethylbenzene 555 c 10 2.5 ug/l 108-67-8 1,3,5-Trimethylbenzene 114 5.0 1.3 ug/l 75-01-4 Vinyl Chloride ND 5.0 1.3 ug/l m,p-Xylene 19.3 10 1.3 ug/l 95-47-6 o-Xylene 117 5.0 1.3 ug/l 1330-20-7 Xylene (total)137 15 2.5 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 95%97%70-130% 17060-07-0 1,2-Dichloroethane-D4 94%102%70-130% 2037-26-5 Toluene-D8 99%97%70-130% 460-00-4 4-Bromofluorobenzene 99%96%70-130% (a) Associated BS recovery outside control limits low. Sporadic marginal failure. (b) Suspected laboratory contaminant. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 23 of 52 FA8890533.6 SGS North America Inc. Report of Analysis Page 3 of 3 Client Sample ID:MW-24 Lab Sample ID:FA88905-6 Date Sampled:09/13/21 Matrix:AQ - Ground Water Date Received:09/14/21 Method:SM 6200B Percent Solids:n/a Project:Perrytown Service Center; 526 Sand Hill Rd, Colerain, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q (c) Result is from Run# 2 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 24 of 52 FA8890533.6 SGS North America Inc. Report of Analysis Page 1 of 3 Client Sample ID:MW-25 Lab Sample ID:FA88905-7 Date Sampled:09/13/21 Matrix:AQ - Ground Water Date Received:09/14/21 Method:SM 6200B Percent Solids:n/a Project:Perrytown Service Center; 526 Sand Hill Rd, Colerain, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 a E108601.D 2 09/16/21 14:55 JL n/a n/a VE2545 Run #2 b E108636.D 2 09/17/21 19:40 JL n/a n/a VE2547 Purge Volume Run #1 10.0 ml Run #2 10.0 ml VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene 63.8 1.0 0.25 ug/l 108-86-1 Bromobenzene ND 1.0 0.25 ug/l 74-97-5 Bromochloromethane ND 1.0 0.25 ug/l 75-27-4 Bromodichloromethane ND 1.0 0.25 ug/l 75-25-2 Bromoform ND 1.0 0.25 ug/l 104-51-8 n-Butylbenzene 0.63 1.0 0.25 ug/l J 135-98-8 sec-Butylbenzene 0.43 1.0 0.25 ug/l J 98-06-6 tert-Butylbenzene ND 1.0 0.25 ug/l 56-23-5 Carbon Tetrachloride ND 1.0 0.25 ug/l 108-90-7 Chlorobenzene ND 1.0 0.25 ug/l 75-00-3 Chloroethane ND 1.0 0.40 ug/l 67-66-3 Chloroform ND 1.0 0.25 ug/l 95-49-8 o-Chlorotoluene ND 1.0 0.25 ug/l 106-43-4 p-Chlorotoluene ND 1.0 0.25 ug/l 124-48-1 Dibromochloromethane ND 1.0 0.25 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 1.0 0.49 ug/l 106-93-4 1,2-Dibromoethane ND 1.0 0.25 ug/l 75-71-8 Dichlorodifluoromethane c ND 1.0 0.40 ug/l 95-50-1 1,2-Dichlorobenzene ND 1.0 0.25 ug/l 541-73-1 1,3-Dichlorobenzene ND 1.0 0.25 ug/l 106-46-7 1,4-Dichlorobenzene ND 1.0 0.25 ug/l 75-34-3 1,1-Dichloroethane ND 1.0 0.25 ug/l 107-06-2 1,2-Dichloroethane ND 1.0 0.25 ug/l 75-35-4 1,1-Dichloroethylene ND 1.0 0.25 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 1.0 0.25 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 1.0 0.25 ug/l 78-87-5 1,2-Dichloropropane ND 1.0 0.25 ug/l 142-28-9 1,3-Dichloropropane ND 1.0 0.25 ug/l 594-20-7 2,2-Dichloropropane ND 1.0 0.25 ug/l 563-58-6 1,1-Dichloropropene ND 1.0 0.25 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 1.0 0.25 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 1.0 0.25 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 25 of 52 FA8890533.7 SGS North America Inc. Report of Analysis Page 2 of 3 Client Sample ID:MW-25 Lab Sample ID:FA88905-7 Date Sampled:09/13/21 Matrix:AQ - Ground Water Date Received:09/14/21 Method:SM 6200B Percent Solids:n/a Project:Perrytown Service Center; 526 Sand Hill Rd, Colerain, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether ND 1.0 0.25 ug/l 100-41-4 Ethylbenzene 31.0 1.0 0.25 ug/l 87-68-3 Hexachlorobutadiene ND 1.0 0.25 ug/l 98-82-8 Isopropylbenzene 1.5 1.0 0.25 ug/l 99-87-6 p-Isopropyltoluene ND 1.0 0.25 ug/l 74-83-9 Methyl Bromide ND 1.0 0.40 ug/l 74-87-3 Methyl Chloride ND 1.0 0.40 ug/l 74-95-3 Methylene Bromide ND 1.0 0.25 ug/l 75-09-2 Methylene Chloride d 3.7 4.0 2.0 ug/l JB 1634-04-4 Methyl Tert Butyl Ether ND 1.0 0.25 ug/l 91-20-3 Naphthalene 13.5 1.0 0.25 ug/l 103-65-1 n-Propylbenzene 4.3 1.0 0.25 ug/l 100-42-5 Styrene ND 1.0 0.25 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 1.0 0.25 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 0.25 ug/l 127-18-4 Tetrachloroethylene ND 1.0 0.25 ug/l 108-88-3 Toluene 51.0 1.0 0.25 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 1.0 0.25 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 1.0 0.25 ug/l 71-55-6 1,1,1-Trichloroethane ND 1.0 0.25 ug/l 79-00-5 1,1,2-Trichloroethane ND 1.0 0.25 ug/l 79-01-6 Trichloroethylene ND 1.0 0.25 ug/l 75-69-4 Trichlorofluoromethane ND 1.0 0.40 ug/l 96-18-4 1,2,3-Trichloropropane ND 1.0 0.25 ug/l 95-63-6 1,2,4-Trimethylbenzene 26.2 1.0 0.25 ug/l 108-67-8 1,3,5-Trimethylbenzene 4.5 1.0 0.25 ug/l 75-01-4 Vinyl Chloride ND 1.0 0.25 ug/l m,p-Xylene 17.5 2.0 0.25 ug/l 95-47-6 o-Xylene 37.6 1.0 0.25 ug/l 1330-20-7 Xylene (total)55.1 3.0 0.50 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 95%98%70-130% 17060-07-0 1,2-Dichloroethane-D4 94%103%70-130% 2037-26-5 Toluene-D8 97%94%70-130% 460-00-4 4-Bromofluorobenzene 98%96%70-130% (a) Results from different vials are not consistent; higher results were reported. (b) Results from different vials are not consistent; higher results were reported. Confirmation run. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 26 of 52 FA8890533.7 SGS North America Inc. Report of Analysis Page 3 of 3 Client Sample ID:MW-25 Lab Sample ID:FA88905-7 Date Sampled:09/13/21 Matrix:AQ - Ground Water Date Received:09/14/21 Method:SM 6200B Percent Solids:n/a Project:Perrytown Service Center; 526 Sand Hill Rd, Colerain, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q (c) Associated BS recovery outside control limits low. Sporadic marginal failure. (d) Suspected laboratory contaminant. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 27 of 52 FA8890533.7 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID:MW-26 Lab Sample ID:FA88905-8 Date Sampled:09/13/21 Matrix:AQ - Ground Water Date Received:09/14/21 Method:SM 6200B Percent Solids:n/a Project:Perrytown Service Center; 526 Sand Hill Rd, Colerain, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 E108602.D 10 09/16/21 15:17 JL n/a n/a VE2545 Run #2 Purge Volume Run #1 10.0 ml Run #2 VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene 120 5.0 1.3 ug/l 108-86-1 Bromobenzene ND 5.0 1.3 ug/l 74-97-5 Bromochloromethane ND 5.0 1.3 ug/l 75-27-4 Bromodichloromethane ND 5.0 1.3 ug/l 75-25-2 Bromoform ND 5.0 1.3 ug/l 104-51-8 n-Butylbenzene ND 5.0 1.3 ug/l 135-98-8 sec-Butylbenzene ND 5.0 1.3 ug/l 98-06-6 tert-Butylbenzene ND 5.0 1.3 ug/l 56-23-5 Carbon Tetrachloride ND 5.0 1.3 ug/l 108-90-7 Chlorobenzene ND 5.0 1.3 ug/l 75-00-3 Chloroethane ND 5.0 2.0 ug/l 67-66-3 Chloroform ND 5.0 1.3 ug/l 95-49-8 o-Chlorotoluene ND 5.0 1.3 ug/l 106-43-4 p-Chlorotoluene ND 5.0 1.3 ug/l 124-48-1 Dibromochloromethane ND 5.0 1.3 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 5.0 2.5 ug/l 106-93-4 1,2-Dibromoethane ND 5.0 1.3 ug/l 75-71-8 Dichlorodifluoromethane a ND 5.0 2.0 ug/l 95-50-1 1,2-Dichlorobenzene ND 5.0 1.3 ug/l 541-73-1 1,3-Dichlorobenzene ND 5.0 1.3 ug/l 106-46-7 1,4-Dichlorobenzene ND 5.0 1.3 ug/l 75-34-3 1,1-Dichloroethane ND 5.0 1.3 ug/l 107-06-2 1,2-Dichloroethane ND 5.0 1.3 ug/l 75-35-4 1,1-Dichloroethylene ND 5.0 1.3 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.3 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.3 ug/l 78-87-5 1,2-Dichloropropane ND 5.0 1.3 ug/l 142-28-9 1,3-Dichloropropane ND 5.0 1.3 ug/l 594-20-7 2,2-Dichloropropane ND 5.0 1.3 ug/l 563-58-6 1,1-Dichloropropene ND 5.0 1.3 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.3 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.3 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 28 of 52 FA8890533.8 SGS North America Inc. Report of Analysis Page 2 of 2 Client Sample ID:MW-26 Lab Sample ID:FA88905-8 Date Sampled:09/13/21 Matrix:AQ - Ground Water Date Received:09/14/21 Method:SM 6200B Percent Solids:n/a Project:Perrytown Service Center; 526 Sand Hill Rd, Colerain, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether ND 5.0 1.3 ug/l 100-41-4 Ethylbenzene 72.7 5.0 1.3 ug/l 87-68-3 Hexachlorobutadiene ND 5.0 1.3 ug/l 98-82-8 Isopropylbenzene 3.2 5.0 1.3 ug/l J 99-87-6 p-Isopropyltoluene ND 5.0 1.3 ug/l 74-83-9 Methyl Bromide ND 5.0 2.0 ug/l 74-87-3 Methyl Chloride 2.4 5.0 2.0 ug/l J 74-95-3 Methylene Bromide ND 5.0 1.3 ug/l 75-09-2 Methylene Chloride b 15.7 20 10 ug/l JB 1634-04-4 Methyl Tert Butyl Ether ND 5.0 1.3 ug/l 91-20-3 Naphthalene 28.1 5.0 1.3 ug/l 103-65-1 n-Propylbenzene 7.8 5.0 1.3 ug/l 100-42-5 Styrene ND 5.0 1.3 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 5.0 1.3 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 1.3 ug/l 127-18-4 Tetrachloroethylene ND 5.0 1.3 ug/l 108-88-3 Toluene 344 5.0 1.3 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 5.0 1.3 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.3 ug/l 71-55-6 1,1,1-Trichloroethane ND 5.0 1.3 ug/l 79-00-5 1,1,2-Trichloroethane ND 5.0 1.3 ug/l 79-01-6 Trichloroethylene ND 5.0 1.3 ug/l 75-69-4 Trichlorofluoromethane ND 5.0 2.0 ug/l 96-18-4 1,2,3-Trichloropropane ND 5.0 1.3 ug/l 95-63-6 1,2,4-Trimethylbenzene 69.2 5.0 1.3 ug/l 108-67-8 1,3,5-Trimethylbenzene 16.3 5.0 1.3 ug/l 75-01-4 Vinyl Chloride ND 5.0 1.3 ug/l m,p-Xylene 195 10 1.3 ug/l 95-47-6 o-Xylene 147 5.0 1.3 ug/l 1330-20-7 Xylene (total)341 15 2.5 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 94%70-130% 17060-07-0 1,2-Dichloroethane-D4 94%70-130% 2037-26-5 Toluene-D8 98%70-130% 460-00-4 4-Bromofluorobenzene 100%70-130% (a) Associated BS recovery outside control limits low. Sporadic marginal failure. (b) Suspected laboratory contaminant. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 29 of 52 FA8890533.8 SGS North America Inc. Report of Analysis Page 1 of 3 Client Sample ID:MW-27 Lab Sample ID:FA88905-9 Date Sampled:09/13/21 Matrix:AQ - Ground Water Date Received:09/14/21 Method:SM 6200B Percent Solids:n/a Project:Perrytown Service Center; 526 Sand Hill Rd, Colerain, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 E108603.D 2.5 09/16/21 15:42 JL n/a n/a VE2545 Run #2 E108637.D 5 09/17/21 20:03 JL n/a n/a VE2547 Purge Volume Run #1 10.0 ml Run #2 10.0 ml VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene 29.5 1.3 0.31 ug/l 108-86-1 Bromobenzene ND 1.3 0.31 ug/l 74-97-5 Bromochloromethane ND 1.3 0.31 ug/l 75-27-4 Bromodichloromethane ND 1.3 0.31 ug/l 75-25-2 Bromoform ND 1.3 0.31 ug/l 104-51-8 n-Butylbenzene 2.0 1.3 0.31 ug/l 135-98-8 sec-Butylbenzene 1.8 1.3 0.31 ug/l 98-06-6 tert-Butylbenzene ND 1.3 0.31 ug/l 56-23-5 Carbon Tetrachloride ND 1.3 0.31 ug/l 108-90-7 Chlorobenzene ND 1.3 0.31 ug/l 75-00-3 Chloroethane ND 1.3 0.50 ug/l 67-66-3 Chloroform ND 1.3 0.31 ug/l 95-49-8 o-Chlorotoluene ND 1.3 0.31 ug/l 106-43-4 p-Chlorotoluene ND 1.3 0.31 ug/l 124-48-1 Dibromochloromethane ND 1.3 0.31 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 1.3 0.62 ug/l 106-93-4 1,2-Dibromoethane ND 1.3 0.31 ug/l 75-71-8 Dichlorodifluoromethane a ND 1.3 0.50 ug/l 95-50-1 1,2-Dichlorobenzene ND 1.3 0.31 ug/l 541-73-1 1,3-Dichlorobenzene ND 1.3 0.31 ug/l 106-46-7 1,4-Dichlorobenzene ND 1.3 0.31 ug/l 75-34-3 1,1-Dichloroethane ND 1.3 0.31 ug/l 107-06-2 1,2-Dichloroethane ND 1.3 0.31 ug/l 75-35-4 1,1-Dichloroethylene ND 1.3 0.31 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 1.3 0.31 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 1.3 0.31 ug/l 78-87-5 1,2-Dichloropropane ND 1.3 0.31 ug/l 142-28-9 1,3-Dichloropropane ND 1.3 0.31 ug/l 594-20-7 2,2-Dichloropropane ND 1.3 0.31 ug/l 563-58-6 1,1-Dichloropropene ND 1.3 0.31 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 1.3 0.31 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 1.3 0.31 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 30 of 52 FA8890533.9 SGS North America Inc. Report of Analysis Page 2 of 3 Client Sample ID:MW-27 Lab Sample ID:FA88905-9 Date Sampled:09/13/21 Matrix:AQ - Ground Water Date Received:09/14/21 Method:SM 6200B Percent Solids:n/a Project:Perrytown Service Center; 526 Sand Hill Rd, Colerain, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether ND 1.3 0.31 ug/l 100-41-4 Ethylbenzene 106 1.3 0.31 ug/l 87-68-3 Hexachlorobutadiene ND 1.3 0.31 ug/l 98-82-8 Isopropylbenzene 10 1.3 0.31 ug/l 99-87-6 p-Isopropyltoluene 0.84 1.3 0.31 ug/l J 74-83-9 Methyl Bromide ND 1.3 0.50 ug/l 74-87-3 Methyl Chloride ND 1.3 0.50 ug/l 74-95-3 Methylene Bromide ND 1.3 0.31 ug/l 75-09-2 Methylene Chloride b 5.4 5.0 2.5 ug/l JB 1634-04-4 Methyl Tert Butyl Ether ND 1.3 0.31 ug/l 91-20-3 Naphthalene 43.0 1.3 0.31 ug/l 103-65-1 n-Propylbenzene 33.3 1.3 0.31 ug/l 100-42-5 Styrene ND 1.3 0.31 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 1.3 0.31 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 1.3 0.31 ug/l 127-18-4 Tetrachloroethylene ND 1.3 0.31 ug/l 108-88-3 Toluene 37.6 1.3 0.31 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 1.3 0.31 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 1.3 0.31 ug/l 71-55-6 1,1,1-Trichloroethane ND 1.3 0.31 ug/l 79-00-5 1,1,2-Trichloroethane ND 1.3 0.31 ug/l 79-01-6 Trichloroethylene ND 1.3 0.31 ug/l 75-69-4 Trichlorofluoromethane ND 1.3 0.50 ug/l 96-18-4 1,2,3-Trichloropropane ND 1.3 0.31 ug/l 95-63-6 1,2,4-Trimethylbenzene 206 c 2.5 0.63 ug/l 108-67-8 1,3,5-Trimethylbenzene 50.5 1.3 0.31 ug/l 75-01-4 Vinyl Chloride ND 1.3 0.31 ug/l m,p-Xylene 127 2.5 0.31 ug/l 95-47-6 o-Xylene 105 1.3 0.31 ug/l 1330-20-7 Xylene (total)232 3.8 0.63 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 94%101%70-130% 17060-07-0 1,2-Dichloroethane-D4 97%103%70-130% 2037-26-5 Toluene-D8 96%98%70-130% 460-00-4 4-Bromofluorobenzene 102%95%70-130% (a) Associated BS recovery outside control limits low. Sporadic marginal failure. (b) Suspected laboratory contaminant. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 31 of 52 FA8890533.9 SGS North America Inc. Report of Analysis Page 3 of 3 Client Sample ID:MW-27 Lab Sample ID:FA88905-9 Date Sampled:09/13/21 Matrix:AQ - Ground Water Date Received:09/14/21 Method:SM 6200B Percent Solids:n/a Project:Perrytown Service Center; 526 Sand Hill Rd, Colerain, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q (c) Result is from Run# 2 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 32 of 52 FA8890533.9 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID:MW-29 Lab Sample ID:FA88905-10 Date Sampled:09/13/21 Matrix:AQ - Ground Water Date Received:09/14/21 Method:SM 6200B Percent Solids:n/a Project:Perrytown Service Center; 526 Sand Hill Rd, Colerain, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 E108607.D 20 09/16/21 17:12 JL n/a n/a VE2545 Run #2 Purge Volume Run #1 10.0 ml Run #2 VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene 558 10 2.5 ug/l 108-86-1 Bromobenzene ND 10 2.5 ug/l 74-97-5 Bromochloromethane ND 10 2.5 ug/l 75-27-4 Bromodichloromethane ND 10 2.5 ug/l 75-25-2 Bromoform ND 10 2.5 ug/l 104-51-8 n-Butylbenzene 6.5 10 2.5 ug/l J 135-98-8 sec-Butylbenzene 4.7 10 2.5 ug/l J 98-06-6 tert-Butylbenzene ND 10 2.5 ug/l 56-23-5 Carbon Tetrachloride ND 10 2.5 ug/l 108-90-7 Chlorobenzene ND 10 2.5 ug/l 75-00-3 Chloroethane ND 10 4.0 ug/l 67-66-3 Chloroform ND 10 2.5 ug/l 95-49-8 o-Chlorotoluene ND 10 2.5 ug/l 106-43-4 p-Chlorotoluene ND 10 2.5 ug/l 124-48-1 Dibromochloromethane ND 10 2.5 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 10 4.9 ug/l 106-93-4 1,2-Dibromoethane ND 10 2.5 ug/l 75-71-8 Dichlorodifluoromethane a ND 10 4.0 ug/l 95-50-1 1,2-Dichlorobenzene ND 10 2.5 ug/l 541-73-1 1,3-Dichlorobenzene ND 10 2.5 ug/l 106-46-7 1,4-Dichlorobenzene ND 10 2.5 ug/l 75-34-3 1,1-Dichloroethane ND 10 2.5 ug/l 107-06-2 1,2-Dichloroethane 5.4 10 2.5 ug/l J 75-35-4 1,1-Dichloroethylene ND 10 2.5 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 10 2.5 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 10 2.5 ug/l 78-87-5 1,2-Dichloropropane ND 10 2.5 ug/l 142-28-9 1,3-Dichloropropane ND 10 2.5 ug/l 594-20-7 2,2-Dichloropropane ND 10 2.5 ug/l 563-58-6 1,1-Dichloropropene ND 10 2.5 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 10 2.5 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 10 2.5 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 33 of 52 FA8890533.10 SGS North America Inc. Report of Analysis Page 2 of 2 Client Sample ID:MW-29 Lab Sample ID:FA88905-10 Date Sampled:09/13/21 Matrix:AQ - Ground Water Date Received:09/14/21 Method:SM 6200B Percent Solids:n/a Project:Perrytown Service Center; 526 Sand Hill Rd, Colerain, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether 5.9 10 2.5 ug/l J 100-41-4 Ethylbenzene 229 10 2.5 ug/l 87-68-3 Hexachlorobutadiene ND 10 2.5 ug/l 98-82-8 Isopropylbenzene 25.9 10 2.5 ug/l 99-87-6 p-Isopropyltoluene ND 10 2.5 ug/l 74-83-9 Methyl Bromide ND 10 4.0 ug/l 74-87-3 Methyl Chloride 9.3 10 4.0 ug/l J 74-95-3 Methylene Bromide ND 10 2.5 ug/l 75-09-2 Methylene Chloride b 41.8 40 20 ug/l JB 1634-04-4 Methyl Tert Butyl Ether 203 10 2.5 ug/l 91-20-3 Naphthalene 125 10 2.5 ug/l 103-65-1 n-Propylbenzene 88.2 10 2.5 ug/l 100-42-5 Styrene ND 10 2.5 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 10 2.5 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 10 2.5 ug/l 127-18-4 Tetrachloroethylene ND 10 2.5 ug/l 108-88-3 Toluene 7.4 10 2.5 ug/l J 87-61-6 1,2,3-Trichlorobenzene ND 10 2.5 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 10 2.5 ug/l 71-55-6 1,1,1-Trichloroethane ND 10 2.5 ug/l 79-00-5 1,1,2-Trichloroethane ND 10 2.5 ug/l 79-01-6 Trichloroethylene ND 10 2.5 ug/l 75-69-4 Trichlorofluoromethane ND 10 4.0 ug/l 96-18-4 1,2,3-Trichloropropane ND 10 2.5 ug/l 95-63-6 1,2,4-Trimethylbenzene 148 10 2.5 ug/l 108-67-8 1,3,5-Trimethylbenzene 111 10 2.5 ug/l 75-01-4 Vinyl Chloride ND 10 2.5 ug/l m,p-Xylene ND 20 2.5 ug/l 95-47-6 o-Xylene 139 10 2.5 ug/l 1330-20-7 Xylene (total)139 30 5.0 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 95%70-130% 17060-07-0 1,2-Dichloroethane-D4 95%70-130% 2037-26-5 Toluene-D8 99%70-130% 460-00-4 4-Bromofluorobenzene 98%70-130% (a) Associated BS recovery outside control limits low. Sporadic marginal failure. (b) Suspected laboratory contaminant. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 34 of 52 FA8890533.10 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID:RW-1 Lab Sample ID:FA88905-11 Date Sampled:09/13/21 Matrix:AQ - Ground Water Date Received:09/14/21 Method:SM 6200B Percent Solids:n/a Project:Perrytown Service Center; 526 Sand Hill Rd, Colerain, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 E108608.D 5 09/16/21 17:35 JL n/a n/a VE2545 Run #2 Purge Volume Run #1 10.0 ml Run #2 VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene 36.9 2.5 0.63 ug/l 108-86-1 Bromobenzene ND 2.5 0.63 ug/l 74-97-5 Bromochloromethane ND 2.5 0.63 ug/l 75-27-4 Bromodichloromethane ND 2.5 0.63 ug/l 75-25-2 Bromoform ND 2.5 0.63 ug/l 104-51-8 n-Butylbenzene 2.7 2.5 0.63 ug/l 135-98-8 sec-Butylbenzene 3.2 2.5 0.63 ug/l 98-06-6 tert-Butylbenzene ND 2.5 0.63 ug/l 56-23-5 Carbon Tetrachloride ND 2.5 0.63 ug/l 108-90-7 Chlorobenzene ND 2.5 0.63 ug/l 75-00-3 Chloroethane ND 2.5 1.0 ug/l 67-66-3 Chloroform ND 2.5 0.63 ug/l 95-49-8 o-Chlorotoluene ND 2.5 0.63 ug/l 106-43-4 p-Chlorotoluene ND 2.5 0.63 ug/l 124-48-1 Dibromochloromethane ND 2.5 0.63 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 2.5 1.2 ug/l 106-93-4 1,2-Dibromoethane ND 2.5 0.63 ug/l 75-71-8 Dichlorodifluoromethane a ND 2.5 1.0 ug/l 95-50-1 1,2-Dichlorobenzene ND 2.5 0.63 ug/l 541-73-1 1,3-Dichlorobenzene ND 2.5 0.63 ug/l 106-46-7 1,4-Dichlorobenzene ND 2.5 0.63 ug/l 75-34-3 1,1-Dichloroethane ND 2.5 0.63 ug/l 107-06-2 1,2-Dichloroethane ND 2.5 0.63 ug/l 75-35-4 1,1-Dichloroethylene ND 2.5 0.63 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 2.5 0.63 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 2.5 0.63 ug/l 78-87-5 1,2-Dichloropropane ND 2.5 0.63 ug/l 142-28-9 1,3-Dichloropropane ND 2.5 0.63 ug/l 594-20-7 2,2-Dichloropropane ND 2.5 0.63 ug/l 563-58-6 1,1-Dichloropropene ND 2.5 0.63 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 2.5 0.63 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 2.5 0.63 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 35 of 52 FA8890533.11 SGS North America Inc. Report of Analysis Page 2 of 2 Client Sample ID:RW-1 Lab Sample ID:FA88905-11 Date Sampled:09/13/21 Matrix:AQ - Ground Water Date Received:09/14/21 Method:SM 6200B Percent Solids:n/a Project:Perrytown Service Center; 526 Sand Hill Rd, Colerain, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether ND 2.5 0.63 ug/l 100-41-4 Ethylbenzene 138 2.5 0.63 ug/l 87-68-3 Hexachlorobutadiene ND 2.5 0.63 ug/l 98-82-8 Isopropylbenzene 8.6 2.5 0.63 ug/l 99-87-6 p-Isopropyltoluene 0.99 2.5 0.63 ug/l J 74-83-9 Methyl Bromide ND 2.5 1.0 ug/l 74-87-3 Methyl Chloride ND 2.5 1.0 ug/l 74-95-3 Methylene Bromide ND 2.5 0.63 ug/l 75-09-2 Methylene Chloride b 10.6 10 5.0 ug/l JB 1634-04-4 Methyl Tert Butyl Ether ND 2.5 0.63 ug/l 91-20-3 Naphthalene 106 2.5 0.63 ug/l 103-65-1 n-Propylbenzene 20.3 2.5 0.63 ug/l 100-42-5 Styrene ND 2.5 0.63 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 2.5 0.63 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 2.5 0.63 ug/l 127-18-4 Tetrachloroethylene ND 2.5 0.63 ug/l 108-88-3 Toluene 68.9 2.5 0.63 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 2.5 0.63 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 2.5 0.63 ug/l 71-55-6 1,1,1-Trichloroethane ND 2.5 0.63 ug/l 79-00-5 1,1,2-Trichloroethane ND 2.5 0.63 ug/l 79-01-6 Trichloroethylene ND 2.5 0.63 ug/l 75-69-4 Trichlorofluoromethane ND 2.5 1.0 ug/l 96-18-4 1,2,3-Trichloropropane ND 2.5 0.63 ug/l 95-63-6 1,2,4-Trimethylbenzene 84.5 2.5 0.63 ug/l 108-67-8 1,3,5-Trimethylbenzene 6.0 2.5 0.63 ug/l 75-01-4 Vinyl Chloride ND 2.5 0.63 ug/l m,p-Xylene 51.7 5.0 0.63 ug/l 95-47-6 o-Xylene 67.0 2.5 0.63 ug/l 1330-20-7 Xylene (total)119 7.5 1.3 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 96%70-130% 17060-07-0 1,2-Dichloroethane-D4 96%70-130% 2037-26-5 Toluene-D8 99%70-130% 460-00-4 4-Bromofluorobenzene 99%70-130% (a) Associated BS recovery outside control limits low. Sporadic marginal failure. (b) Suspected laboratory contaminant. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 36 of 52 FA8890533.11 SGS North America Inc. Misc. Forms Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody Orlando, FL Section 4 37 of 52 FA889054 FA88905: Chain of Custody Page 1 of 2 38 of 52 FA8890544.1 Job Number:FA88905 Client:GRI Date / Time Received:9/14/2021 10:00:00 AM Delivery Method:FX Project:PERRYTOWN SERVICE CENTER Airbill #'s:7747 8670 7054 Cooler Information 1. Custody Seals Present 2. Custody Seals Intact 4. Cooler temp verification 3. Temp criteria achieved 5. Cooler media IR Gun Ice (Bag) Trip Blank Information 1. Trip Blank present / cooler 2. Trip Blank listed on COC 2. Samples preserved properly Sample Information 1. Sample labels present on bottles 5. Sample recvd within HT 4. Condition of sample 3. Sufficient volume/containers recvd for analysis: Intact Comments SM001Rev. Date 05/24/17 SGS Sample Receipt Summary Cooler Temps (Raw Measured) °C: Cooler Temps (Corrected) °C: Cooler 1: (0.0); Cooler 1: (0.2); 3. Type Of TB Received W or S N/A 6. Dates/Times/IDs on COC match Sample Label 7. VOCs have headspace 8. Bottles received for unspecified tests 9. Compositing instructions clear 10. Voa Soil Kits/Jars received past 48hrs? 11. % Solids Jar received? Misc. Information 25-Gram 5-GramNumber of Encores:Number of 5035 Field Kits:Number of Lab Filtered Metals: Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify) Y or N N/A Y or N Therm ID:IR 1; Therm CF:0.2; # of Coolers:1 Y or N N/A 12. Residual Chlorine Present? Residual Chlorine Test Strip Lot #: Technician:Reviewer:PETERH Date:Date:9/14/2021 10:00:00 A FA88905: Chain of Custody Page 2 of 2 39 of 52 FA8890544.1 SGS North America Inc. MS Volatiles QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries Orlando, FL Section 5 40 of 52 FA889055 Method Blank Summary Page 1 of 2 Job Number:FA88905 Account:GRINCC GRI (Geological Resources Inc.) Project:Perrytown Service Center; 526 Sand Hill Rd, Colerain, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VE2545-MB E108594.D 1 09/16/21 JL n/a n/a VE2545 The QC reported here applies to the following samples:Method: SM 6200B FA88905-2, FA88905-3, FA88905-4, FA88905-6, FA88905-7, FA88905-8, FA88905-9, FA88905-10, FA88905-11 CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.13 ug/l 108-86-1 Bromobenzene ND 0.50 0.13 ug/l 74-97-5 Bromochloromethane ND 0.50 0.13 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l 75-25-2 Bromoform ND 0.50 0.13 ug/l 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane ND 0.50 0.20 ug/l 67-66-3 Chloroform ND 0.50 0.13 ug/l 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l 75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l 75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l 563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l 108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l 100-41-4 Ethylbenzene ND 0.50 0.13 ug/l 87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l 41 of 52 FA8890555.1.1 Method Blank Summary Page 2 of 2 Job Number:FA88905 Account:GRINCC GRI (Geological Resources Inc.) Project:Perrytown Service Center; 526 Sand Hill Rd, Colerain, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VE2545-MB E108594.D 1 09/16/21 JL n/a n/a VE2545 The QC reported here applies to the following samples:Method: SM 6200B FA88905-2, FA88905-3, FA88905-4, FA88905-6, FA88905-7, FA88905-8, FA88905-9, FA88905-10, FA88905-11 CAS No.Compound Result RL MDL Units Q 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l 74-83-9 Methyl Bromide ND 0.50 0.20 ug/l 74-87-3 Methyl Chloride ND 0.50 0.20 ug/l 74-95-3 Methylene Bromide ND 0.50 0.13 ug/l 75-09-2 Methylene Chloride 1.6 2.0 1.0 ug/l J 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l 91-20-3 Naphthalene ND 0.50 0.13 ug/l 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l 100-42-5 Styrene ND 0.50 0.13 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l 108-88-3 Toluene ND 0.50 0.13 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l 71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l 79-01-6 Trichloroethylene ND 0.50 0.13 ug/l 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l m,p-Xylene ND 1.0 0.13 ug/l 95-47-6 o-Xylene ND 0.50 0.13 ug/l 1330-20-7 Xylene (total)ND 1.5 0.25 ug/l CAS No.Surrogate Recoveries Limits 1868-53-7 Dibromofluoromethane 96%70-130% 17060-07-0 1,2-Dichloroethane-D4 95%70-130% 2037-26-5 Toluene-D8 97%70-130% 460-00-4 4-Bromofluorobenzene 99%70-130% 42 of 52 FA8890555.1.1 Method Blank Summary Page 1 of 2 Job Number:FA88905 Account:GRINCC GRI (Geological Resources Inc.) Project:Perrytown Service Center; 526 Sand Hill Rd, Colerain, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VE2547-MB E108617.D 1 09/17/21 JL n/a n/a VE2547 The QC reported here applies to the following samples:Method: SM 6200B FA88905-1, FA88905-3, FA88905-4, FA88905-5, FA88905-6, FA88905-9 CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.13 ug/l 108-86-1 Bromobenzene ND 0.50 0.13 ug/l 74-97-5 Bromochloromethane ND 0.50 0.13 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l 75-25-2 Bromoform ND 0.50 0.13 ug/l 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane ND 0.50 0.20 ug/l 67-66-3 Chloroform ND 0.50 0.13 ug/l 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l 75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l 75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l 563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l 108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l 100-41-4 Ethylbenzene ND 0.50 0.13 ug/l 87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l 43 of 52 FA8890555.1.2 Method Blank Summary Page 2 of 2 Job Number:FA88905 Account:GRINCC GRI (Geological Resources Inc.) Project:Perrytown Service Center; 526 Sand Hill Rd, Colerain, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VE2547-MB E108617.D 1 09/17/21 JL n/a n/a VE2547 The QC reported here applies to the following samples:Method: SM 6200B FA88905-1, FA88905-3, FA88905-4, FA88905-5, FA88905-6, FA88905-9 CAS No.Compound Result RL MDL Units Q 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l 74-83-9 Methyl Bromide ND 0.50 0.20 ug/l 74-87-3 Methyl Chloride ND 0.50 0.20 ug/l 74-95-3 Methylene Bromide ND 0.50 0.13 ug/l 75-09-2 Methylene Chloride 1.6 2.0 1.0 ug/l J 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l 91-20-3 Naphthalene ND 0.50 0.13 ug/l 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l 100-42-5 Styrene ND 0.50 0.13 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l 108-88-3 Toluene ND 0.50 0.13 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l 71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l 79-01-6 Trichloroethylene ND 0.50 0.13 ug/l 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l m,p-Xylene ND 1.0 0.13 ug/l 95-47-6 o-Xylene ND 0.50 0.13 ug/l 1330-20-7 Xylene (total)ND 1.5 0.25 ug/l CAS No.Surrogate Recoveries Limits 1868-53-7 Dibromofluoromethane 98%70-130% 17060-07-0 1,2-Dichloroethane-D4 97%70-130% 2037-26-5 Toluene-D8 97%70-130% 460-00-4 4-Bromofluorobenzene 96%70-130% 44 of 52 FA8890555.1.2 Blank Spike Summary Page 1 of 2 Job Number:FA88905 Account:GRINCC GRI (Geological Resources Inc.) Project:Perrytown Service Center; 526 Sand Hill Rd, Colerain, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VE2545-BS E108592.D 1 09/16/21 JL n/a n/a VE2545 The QC reported here applies to the following samples:Method: SM 6200B FA88905-2, FA88905-3, FA88905-4, FA88905-6, FA88905-7, FA88905-8, FA88905-9, FA88905-10, FA88905-11 Spike BSP BSP CAS No.Compound ug/l ug/l %Limits 71-43-2 Benzene 10 9.6 96 70-130 108-86-1 Bromobenzene 10 9.6 96 70-130 74-97-5 Bromochloromethane 10 8.4 84 70-130 75-27-4 Bromodichloromethane 10 9.5 95 70-130 75-25-2 Bromoform 10 9.8 98 70-130 104-51-8 n-Butylbenzene 10 10.2 102 70-130 135-98-8 sec-Butylbenzene 10 10.8 108 70-130 98-06-6 tert-Butylbenzene 10 10 100 70-130 56-23-5 Carbon Tetrachloride 10 10 100 70-130 108-90-7 Chlorobenzene 10 9.7 97 70-130 75-00-3 Chloroethane 10 10.4 104 60-140 67-66-3 Chloroform 10 9.1 91 70-130 95-49-8 o-Chlorotoluene 10 9.8 98 70-130 106-43-4 p-Chlorotoluene 10 9.9 99 70-130 124-48-1 Dibromochloromethane 10 9.3 93 70-130 96-12-8 1,2-Dibromo-3-chloropropane 10 9.5 95 70-130 106-93-4 1,2-Dibromoethane 10 9.3 93 70-130 75-71-8 Dichlorodifluoromethane 10 5.7 57* a 60-140 95-50-1 1,2-Dichlorobenzene 10 9.6 96 70-130 541-73-1 1,3-Dichlorobenzene 10 10 100 70-130 106-46-7 1,4-Dichlorobenzene 10 9.6 96 70-130 75-34-3 1,1-Dichloroethane 10 9.8 98 70-130 107-06-2 1,2-Dichloroethane 10 8.6 86 70-130 75-35-4 1,1-Dichloroethylene 10 11.1 111 70-130 156-59-2 cis-1,2-Dichloroethylene 10 9.5 95 70-130 156-60-5 trans-1,2-Dichloroethylene 10 9.3 93 70-130 78-87-5 1,2-Dichloropropane 10 9.6 96 70-130 142-28-9 1,3-Dichloropropane 10 9.2 92 70-130 594-20-7 2,2-Dichloropropane 10 10.1 101 70-130 563-58-6 1,1-Dichloropropene 10 9.7 97 70-130 10061-01-5 cis-1,3-Dichloropropene 10 9.5 95 70-130 10061-02-6 trans-1,3-Dichloropropene 10 9.8 98 70-130 108-20-3 Di-Isopropyl Ether 10 8.9 89 70-130 100-41-4 Ethylbenzene 10 9.8 98 70-130 87-68-3 Hexachlorobutadiene 10 10.2 102 70-130 98-82-8 Isopropylbenzene 10 10.3 103 70-130 * = Outside of Control Limits. 45 of 52 FA8890555.2.1 Blank Spike Summary Page 2 of 2 Job Number:FA88905 Account:GRINCC GRI (Geological Resources Inc.) Project:Perrytown Service Center; 526 Sand Hill Rd, Colerain, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VE2545-BS E108592.D 1 09/16/21 JL n/a n/a VE2545 The QC reported here applies to the following samples:Method: SM 6200B FA88905-2, FA88905-3, FA88905-4, FA88905-6, FA88905-7, FA88905-8, FA88905-9, FA88905-10, FA88905-11 Spike BSP BSP CAS No.Compound ug/l ug/l %Limits 99-87-6 p-Isopropyltoluene 10 10.6 106 70-130 74-83-9 Methyl Bromide 10 7.4 74 60-140 74-87-3 Methyl Chloride 10 7.8 78 60-140 74-95-3 Methylene Bromide 10 8.8 88 70-130 75-09-2 Methylene Chloride 10 9.5 95 70-130 1634-04-4 Methyl Tert Butyl Ether 10 8.8 88 70-130 91-20-3 Naphthalene 10 9.8 98 70-130 103-65-1 n-Propylbenzene 10 10.3 103 70-130 100-42-5 Styrene 10 10.1 101 70-130 630-20-6 1,1,1,2-Tetrachloroethane 10 9.4 94 70-130 79-34-5 1,1,2,2-Tetrachloroethane 10 9.4 94 70-130 127-18-4 Tetrachloroethylene 10 10.0 100 70-130 108-88-3 Toluene 10 9.5 95 70-130 87-61-6 1,2,3-Trichlorobenzene 10 9.1 91 70-130 120-82-1 1,2,4-Trichlorobenzene 10 9.3 93 70-130 71-55-6 1,1,1-Trichloroethane 10 9.3 93 70-130 79-00-5 1,1,2-Trichloroethane 10 9.4 94 70-130 79-01-6 Trichloroethylene 10 10.1 101 70-130 75-69-4 Trichlorofluoromethane 10 8.6 86 60-140 96-18-4 1,2,3-Trichloropropane 10 9.2 92 70-130 95-63-6 1,2,4-Trimethylbenzene 10 9.9 99 70-130 108-67-8 1,3,5-Trimethylbenzene 10 9.9 99 70-130 75-01-4 Vinyl Chloride 10 8.2 82 60-140 m,p-Xylene 20 19.7 99 70-130 95-47-6 o-Xylene 10 9.8 98 70-130 1330-20-7 Xylene (total)30 29.5 98 70-130 CAS No.Surrogate Recoveries BSP Limits 1868-53-7 Dibromofluoromethane 95%70-130% 17060-07-0 1,2-Dichloroethane-D4 96%70-130% 2037-26-5 Toluene-D8 100%70-130% 460-00-4 4-Bromofluorobenzene 100%70-130% (a) Sporadic marginal failure. * = Outside of Control Limits. 46 of 52 FA8890555.2.1 Blank Spike Summary Page 1 of 2 Job Number:FA88905 Account:GRINCC GRI (Geological Resources Inc.) Project:Perrytown Service Center; 526 Sand Hill Rd, Colerain, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VE2547-BS E108615.D 1 09/17/21 JL n/a n/a VE2547 The QC reported here applies to the following samples:Method: SM 6200B FA88905-1, FA88905-3, FA88905-4, FA88905-5, FA88905-6, FA88905-9 Spike BSP BSP CAS No.Compound ug/l ug/l %Limits 71-43-2 Benzene 10 9.3 93 70-130 108-86-1 Bromobenzene 10 9.1 91 70-130 74-97-5 Bromochloromethane 10 8.2 82 70-130 75-27-4 Bromodichloromethane 10 9.0 90 70-130 75-25-2 Bromoform 10 9.1 91 70-130 104-51-8 n-Butylbenzene 10 9.6 96 70-130 135-98-8 sec-Butylbenzene 10 10.3 103 70-130 98-06-6 tert-Butylbenzene 10 9.7 97 70-130 56-23-5 Carbon Tetrachloride 10 9.7 97 70-130 108-90-7 Chlorobenzene 10 9.2 92 70-130 75-00-3 Chloroethane 10 11.6 116 60-140 67-66-3 Chloroform 10 9.0 90 70-130 95-49-8 o-Chlorotoluene 10 9.5 95 70-130 106-43-4 p-Chlorotoluene 10 9.4 94 70-130 124-48-1 Dibromochloromethane 10 8.5 85 70-130 96-12-8 1,2-Dibromo-3-chloropropane 10 9.2 92 70-130 106-93-4 1,2-Dibromoethane 10 8.7 87 70-130 75-71-8 Dichlorodifluoromethane 10 6.3 63 60-140 95-50-1 1,2-Dichlorobenzene 10 9.3 93 70-130 541-73-1 1,3-Dichlorobenzene 10 9.4 94 70-130 106-46-7 1,4-Dichlorobenzene 10 9.1 91 70-130 75-34-3 1,1-Dichloroethane 10 9.6 96 70-130 107-06-2 1,2-Dichloroethane 10 8.5 85 70-130 75-35-4 1,1-Dichloroethylene 10 10.7 107 70-130 156-59-2 cis-1,2-Dichloroethylene 10 9.3 93 70-130 156-60-5 trans-1,2-Dichloroethylene 10 9.1 91 70-130 78-87-5 1,2-Dichloropropane 10 9.0 90 70-130 142-28-9 1,3-Dichloropropane 10 8.4 84 70-130 594-20-7 2,2-Dichloropropane 10 9.9 99 70-130 563-58-6 1,1-Dichloropropene 10 9.3 93 70-130 10061-01-5 cis-1,3-Dichloropropene 10 8.7 87 70-130 10061-02-6 trans-1,3-Dichloropropene 10 9.1 91 70-130 108-20-3 Di-Isopropyl Ether 10 8.5 85 70-130 100-41-4 Ethylbenzene 10 9.4 94 70-130 87-68-3 Hexachlorobutadiene 10 9.7 97 70-130 98-82-8 Isopropylbenzene 10 9.8 98 70-130 * = Outside of Control Limits. 47 of 52 FA8890555.2.2 Blank Spike Summary Page 2 of 2 Job Number:FA88905 Account:GRINCC GRI (Geological Resources Inc.) Project:Perrytown Service Center; 526 Sand Hill Rd, Colerain, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VE2547-BS E108615.D 1 09/17/21 JL n/a n/a VE2547 The QC reported here applies to the following samples:Method: SM 6200B FA88905-1, FA88905-3, FA88905-4, FA88905-5, FA88905-6, FA88905-9 Spike BSP BSP CAS No.Compound ug/l ug/l %Limits 99-87-6 p-Isopropyltoluene 10 10.1 101 70-130 74-83-9 Methyl Bromide 10 8.5 85 60-140 74-87-3 Methyl Chloride 10 8.6 86 60-140 74-95-3 Methylene Bromide 10 8.5 85 70-130 75-09-2 Methylene Chloride 10 9.9 99 70-130 1634-04-4 Methyl Tert Butyl Ether 10 8.6 86 70-130 91-20-3 Naphthalene 10 9.4 94 70-130 103-65-1 n-Propylbenzene 10 9.9 99 70-130 100-42-5 Styrene 10 9.4 94 70-130 630-20-6 1,1,1,2-Tetrachloroethane 10 9.1 91 70-130 79-34-5 1,1,2,2-Tetrachloroethane 10 8.8 88 70-130 127-18-4 Tetrachloroethylene 10 9.4 94 70-130 108-88-3 Toluene 10 9.1 91 70-130 87-61-6 1,2,3-Trichlorobenzene 10 8.9 89 70-130 120-82-1 1,2,4-Trichlorobenzene 10 9.2 92 70-130 71-55-6 1,1,1-Trichloroethane 10 9.2 92 70-130 79-00-5 1,1,2-Trichloroethane 10 8.6 86 70-130 79-01-6 Trichloroethylene 10 9.9 99 70-130 75-69-4 Trichlorofluoromethane 10 9.7 97 60-140 96-18-4 1,2,3-Trichloropropane 10 8.9 89 70-130 95-63-6 1,2,4-Trimethylbenzene 10 9.5 95 70-130 108-67-8 1,3,5-Trimethylbenzene 10 9.6 96 70-130 75-01-4 Vinyl Chloride 10 8.7 87 60-140 m,p-Xylene 20 18.7 94 70-130 95-47-6 o-Xylene 10 9.5 95 70-130 1330-20-7 Xylene (total)30 28.2 94 70-130 CAS No.Surrogate Recoveries BSP Limits 1868-53-7 Dibromofluoromethane 97%70-130% 17060-07-0 1,2-Dichloroethane-D4 98%70-130% 2037-26-5 Toluene-D8 99%70-130% 460-00-4 4-Bromofluorobenzene 99%70-130% * = Outside of Control Limits. 48 of 52 FA8890555.2.2 Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2 Job Number:FA88905 Account:GRINCC GRI (Geological Resources Inc.) Project:Perrytown Service Center; 526 Sand Hill Rd, Colerain, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA88905-11MS E108609.D 5 09/16/21 JL n/a n/a VE2545 FA88905-11MSD E108610.D 5 09/16/21 JL n/a n/a VE2545 FA88905-11 E108608.D 5 09/16/21 JL n/a n/a VE2545 The QC reported here applies to the following samples:Method: SM 6200B FA88905-2, FA88905-3, FA88905-4, FA88905-6, FA88905-7, FA88905-8, FA88905-9, FA88905-10, FA88905-11 FA88905-11 Spike MS MS Spike MSD MSD Limits CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD 71-43-2 Benzene 36.9 50 82.0 90 50 80.6 87 2 70-130/20 108-86-1 Bromobenzene ND 50 44.3 89 50 43.2 86 3 70-130/20 74-97-5 Bromochloromethane ND 50 39.5 79 50 38.4 77 3 70-130/20 75-27-4 Bromodichloromethane ND 50 40.5 81 50 38.9 78 4 70-130/20 75-25-2 Bromoform ND 50 30.7 61*50 29.4 59*4 70-130/20 104-51-8 n-Butylbenzene 2.7 50 48.3 91 50 47.2 89 2 70-130/20 135-98-8 sec-Butylbenzene 3.2 50 52.4 98 50 51.3 96 2 70-130/20 98-06-6 tert-Butylbenzene ND 50 48.1 96 50 47.2 94 2 70-130/20 56-23-5 Carbon Tetrachloride ND 50 44.5 89 50 42.4 85 5 70-130/20 108-90-7 Chlorobenzene ND 50 43.4 87 50 42.9 86 1 70-130/20 75-00-3 Chloroethane ND 50 57.5 115 50 53.6 107 7 60-140/20 67-66-3 Chloroform ND 50 44.1 88 50 43.7 87 1 70-130/20 95-49-8 o-Chlorotoluene ND 50 46.4 93 50 45.6 91 2 70-130/20 106-43-4 p-Chlorotoluene ND 50 44.8 90 50 44.4 89 1 70-130/20 124-48-1 Dibromochloromethane ND 50 33.8 68*50 32.5 65*4 70-130/20 96-12-8 1,2-Dibromo-3-chloropropane ND 50 8.8 18*50 7.9 16*11 70-130/20 106-93-4 1,2-Dibromoethane ND 50 41.9 84 50 41.7 83 0 70-130/20 75-71-8 Dichlorodifluoromethane ND 50 31.8 64 50 30.7 61 4 60-140/20 95-50-1 1,2-Dichlorobenzene ND 50 45.0 90 50 44.3 89 2 70-130/20 541-73-1 1,3-Dichlorobenzene ND 50 46.1 92 50 45.4 91 2 70-130/20 106-46-7 1,4-Dichlorobenzene ND 50 44.3 89 50 43.4 87 2 70-130/20 75-34-3 1,1-Dichloroethane ND 50 45.8 92 50 45.0 90 2 70-130/20 107-06-2 1,2-Dichloroethane ND 50 40.1 80 50 39.4 79 2 70-130/20 75-35-4 1,1-Dichloroethylene ND 50 49.1 98 50 47.6 95 3 70-130/20 156-59-2 cis-1,2-Dichloroethylene ND 50 44.9 90 50 44.2 88 2 70-130/20 156-60-5 trans-1,2-Dichloroethylene ND 50 43.4 87 50 42.4 85 2 70-130/20 78-87-5 1,2-Dichloropropane ND 50 44.7 89 50 44.4 89 1 70-130/20 142-28-9 1,3-Dichloropropane ND 50 42.0 84 50 40.8 82 3 70-130/20 594-20-7 2,2-Dichloropropane ND 50 42.9 86 50 42.1 84 2 70-130/20 563-58-6 1,1-Dichloropropene ND 50 44.9 90 50 44.9 90 0 70-130/20 10061-01-5 cis-1,3-Dichloropropene ND 50 33.1 66*50 31.4 63*5 70-130/20 10061-02-6 trans-1,3-Dichloropropene ND 50 33.9 68*50 32.1 64*5 70-130/20 108-20-3 Di-Isopropyl Ether ND 50 41.2 82 50 40.4 81 2 70-130/20 100-41-4 Ethylbenzene 138 50 177 78 50 173 70 2 70-130/20 87-68-3 Hexachlorobutadiene ND 50 45.2 90 50 44.1 88 2 70-130/20 98-82-8 Isopropylbenzene 8.6 50 57.1 97 50 55.4 94 3 70-130/20 * = Outside of Control Limits. 49 of 52 FA8890555.3.1 Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2 Job Number:FA88905 Account:GRINCC GRI (Geological Resources Inc.) Project:Perrytown Service Center; 526 Sand Hill Rd, Colerain, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA88905-11MS E108609.D 5 09/16/21 JL n/a n/a VE2545 FA88905-11MSD E108610.D 5 09/16/21 JL n/a n/a VE2545 FA88905-11 E108608.D 5 09/16/21 JL n/a n/a VE2545 The QC reported here applies to the following samples:Method: SM 6200B FA88905-2, FA88905-3, FA88905-4, FA88905-6, FA88905-7, FA88905-8, FA88905-9, FA88905-10, FA88905-11 FA88905-11 Spike MS MS Spike MSD MSD Limits CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD 99-87-6 p-Isopropyltoluene 0.99 J 50 49.9 98 50 49.4 97 1 70-130/20 74-83-9 Methyl Bromide ND 50 40.4 81 50 39.7 79 2 60-140/20 74-87-3 Methyl Chloride ND 50 41.7 83 50 39.4 79 6 60-140/20 74-95-3 Methylene Bromide ND 50 41.7 83 50 41.0 82 2 70-130/20 75-09-2 Methylene Chloride 10.6 JB 50 44.8 68*50 47.7 74 6 70-130/20 1634-04-4 Methyl Tert Butyl Ether ND 50 45.3 91 50 44.7 89 1 70-130/20 91-20-3 Naphthalene 106 50 142 72 50 140 68* a 1 70-130/20 103-65-1 n-Propylbenzene 20.3 50 66.9 93 50 66.5 92 1 70-130/20 100-42-5 Styrene ND 50 37.1 74 50 36.4 73 2 70-130/20 630-20-6 1,1,1,2-Tetrachloroethane ND 50 43.3 87 50 42.8 86 1 70-130/20 79-34-5 1,1,2,2-Tetrachloroethane ND 50 44.0 88 50 44.5 89 1 70-130/20 127-18-4 Tetrachloroethylene ND 50 46.0 92 50 45.3 91 2 70-130/20 108-88-3 Toluene 68.9 50 113 88 50 110 82 3 70-130/20 87-61-6 1,2,3-Trichlorobenzene ND 50 46.1 92 50 44.9 90 3 70-130/20 120-82-1 1,2,4-Trichlorobenzene ND 50 47.7 95 50 46.0 92 4 70-130/20 71-55-6 1,1,1-Trichloroethane ND 50 43.9 88 50 43.0 86 2 70-130/20 79-00-5 1,1,2-Trichloroethane ND 50 42.1 84 50 42.2 84 0 70-130/20 79-01-6 Trichloroethylene ND 50 46.2 92 50 45.8 92 1 70-130/20 75-69-4 Trichlorofluoromethane ND 50 48.6 97 50 46.2 92 5 60-140/20 96-18-4 1,2,3-Trichloropropane ND 50 42.0 84 50 41.0 82 2 70-130/20 95-63-6 1,2,4-Trimethylbenzene 84.5 50 133 97 50 130 91 2 70-130/20 108-67-8 1,3,5-Trimethylbenzene 6.0 50 53.0 94 50 52.2 92 2 70-130/20 75-01-4 Vinyl Chloride ND 50 41.6 83 50 39.7 79 5 60-140/20 m,p-Xylene 51.7 100 144 92 100 141 89 2 70-130/20 95-47-6 o-Xylene 67.0 50 113 92 50 109 84 4 70-130/20 1330-20-7 Xylene (total)119 150 257 92 150 251 88 2 70-130/20 CAS No.Surrogate Recoveries MS MSD FA88905-11 Limits 1868-53-7 Dibromofluoromethane 96%96%96%70-130% 17060-07-0 1,2-Dichloroethane-D4 95%96%96%70-130% 2037-26-5 Toluene-D8 99%100%99%70-130% 460-00-4 4-Bromofluorobenzene 100%100%99%70-130% (a) Outside control limits due to high level in sample relative to spike amount. * = Outside of Control Limits. 50 of 52 FA8890555.3.1 Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2 Job Number:FA88905 Account:GRINCC GRI (Geological Resources Inc.) Project:Perrytown Service Center; 526 Sand Hill Rd, Colerain, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA88905-1MS E108639.D 50 09/17/21 JL n/a n/a VE2547 FA88905-1MSD E108640.D 50 09/17/21 JL n/a n/a VE2547 FA88905-1 E108638.D 50 09/17/21 JL n/a n/a VE2547 The QC reported here applies to the following samples:Method: SM 6200B FA88905-1, FA88905-3, FA88905-4, FA88905-5, FA88905-6, FA88905-9 FA88905-1 Spike MS MS Spike MSD MSD Limits CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD 71-43-2 Benzene 150 500 579 86 500 665 103 14 70-130/20 108-86-1 Bromobenzene ND 500 405 81 500 484 97 18 70-130/20 74-97-5 Bromochloromethane ND 500 365 73 500 448 90 20 70-130/20 75-27-4 Bromodichloromethane ND 500 411 82 500 513 103 22*70-130/20 75-25-2 Bromoform ND 500 410 82 500 512 102 22*70-130/20 104-51-8 n-Butylbenzene 28.4 500 463 87 500 553 105 18 70-130/20 135-98-8 sec-Butylbenzene 15.5 J 500 474 92 500 567 110 18 70-130/20 98-06-6 tert-Butylbenzene ND 500 442 88 500 544 109 21*70-130/20 56-23-5 Carbon Tetrachloride ND 500 444 89 500 554 111 22*70-130/20 108-90-7 Chlorobenzene ND 500 408 82 500 491 98 18 70-130/20 75-00-3 Chloroethane ND 500 941 188*500 919 184*2 60-140/20 67-66-3 Chloroform ND 500 420 84 500 513 103 20 70-130/20 95-49-8 o-Chlorotoluene ND 500 484 97 500 577 115 18 70-130/20 106-43-4 p-Chlorotoluene ND 500 416 83 500 507 101 20 70-130/20 124-48-1 Dibromochloromethane ND 500 389 78 500 478 96 21*70-130/20 96-12-8 1,2-Dibromo-3-chloropropane ND 500 79.2 16*500 536 107 149*70-130/20 106-93-4 1,2-Dibromoethane ND 500 404 81 500 485 97 18 70-130/20 75-71-8 Dichlorodifluoromethane ND 500 390 78 500 396 79 2 60-140/20 95-50-1 1,2-Dichlorobenzene ND 500 417 83 500 517 103 21*70-130/20 541-73-1 1,3-Dichlorobenzene ND 500 424 85 500 518 104 20 70-130/20 106-46-7 1,4-Dichlorobenzene ND 500 409 82 500 491 98 18 70-130/20 75-34-3 1,1-Dichloroethane ND 500 426 85 500 530 106 22*70-130/20 107-06-2 1,2-Dichloroethane ND 500 411 82 500 489 98 17 70-130/20 75-35-4 1,1-Dichloroethylene ND 500 478 96 500 737 147*43*70-130/20 156-59-2 cis-1,2-Dichloroethylene ND 500 408 82 500 504 101 21*70-130/20 156-60-5 trans-1,2-Dichloroethylene ND 500 410 82 500 499 100 20 70-130/20 78-87-5 1,2-Dichloropropane ND 500 414 83 500 518 104 22*70-130/20 142-28-9 1,3-Dichloropropane ND 500 395 79 500 463 93 16 70-130/20 594-20-7 2,2-Dichloropropane ND 500 393 79 500 501 100 24*70-130/20 563-58-6 1,1-Dichloropropene ND 500 427 85 500 515 103 19 70-130/20 10061-01-5 cis-1,3-Dichloropropene ND 500 377 75 500 473 95 23*70-130/20 10061-02-6 trans-1,3-Dichloropropene ND 500 402 80 500 481 96 18 70-130/20 108-20-3 Di-Isopropyl Ether ND 500 397 79 500 484 97 20 70-130/20 100-41-4 Ethylbenzene 1210 500 1700 98 500 1750 108 3 70-130/20 87-68-3 Hexachlorobutadiene ND 500 420 84 500 523 105 22*70-130/20 98-82-8 Isopropylbenzene 67.1 500 533 93 500 631 113 17 70-130/20 * = Outside of Control Limits. 51 of 52 FA8890555.3.2 Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2 Job Number:FA88905 Account:GRINCC GRI (Geological Resources Inc.) Project:Perrytown Service Center; 526 Sand Hill Rd, Colerain, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA88905-1MS E108639.D 50 09/17/21 JL n/a n/a VE2547 FA88905-1MSD E108640.D 50 09/17/21 JL n/a n/a VE2547 FA88905-1 E108638.D 50 09/17/21 JL n/a n/a VE2547 The QC reported here applies to the following samples:Method: SM 6200B FA88905-1, FA88905-3, FA88905-4, FA88905-5, FA88905-6, FA88905-9 FA88905-1 Spike MS MS Spike MSD MSD Limits CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD 99-87-6 p-Isopropyltoluene 10.0 J 500 459 90 500 558 110 19 70-130/20 74-83-9 Methyl Bromide ND 500 626 125 500 596 119 5 60-140/20 74-87-3 Methyl Chloride ND 500 533 107 500 525 105 2 60-140/20 74-95-3 Methylene Bromide ND 500 385 77 500 466 93 19 70-130/20 75-09-2 Methylene Chloride 69.4 JB 500 451 76 500 572 101 24*70-130/20 1634-04-4 Methyl Tert Butyl Ether ND 500 390 78 500 477 95 20 70-130/20 91-20-3 Naphthalene 413 500 886 95 500 999 117 12 70-130/20 103-65-1 n-Propylbenzene 216 500 691 95 500 781 113 12 70-130/20 100-42-5 Styrene ND 500 437 87 500 536 107 20 70-130/20 630-20-6 1,1,1,2-Tetrachloroethane ND 500 414 83 500 508 102 20 70-130/20 79-34-5 1,1,2,2-Tetrachloroethane ND 500 410 82 500 493 99 18 70-130/20 127-18-4 Tetrachloroethylene ND 500 423 85 500 514 103 19 70-130/20 108-88-3 Toluene 565 500 1020 91 500 1080 103 6 70-130/20 87-61-6 1,2,3-Trichlorobenzene ND 500 409 82 500 521 104 24*70-130/20 120-82-1 1,2,4-Trichlorobenzene ND 500 421 84 500 531 106 23*70-130/20 71-55-6 1,1,1-Trichloroethane ND 500 426 85 500 528 106 21*70-130/20 79-00-5 1,1,2-Trichloroethane ND 500 404 81 500 479 96 17 70-130/20 79-01-6 Trichloroethylene ND 500 450 90 500 545 109 19 70-130/20 75-69-4 Trichlorofluoromethane ND 500 703 141*500 701 140 0 60-140/20 96-18-4 1,2,3-Trichloropropane ND 500 394 79 500 494 99 23*70-130/20 95-63-6 1,2,4-Trimethylbenzene 1830 500 2430 120 500 2470 128 2 70-130/20 108-67-8 1,3,5-Trimethylbenzene 507 500 996 98 500 1070 113 7 70-130/20 75-01-4 Vinyl Chloride ND 500 476 95 500 504 101 6 60-140/20 m,p-Xylene 3550 1000 4540 99 1000 4570 102 1 70-130/20 95-47-6 o-Xylene 1310 500 1830 104 500 1870 112 2 70-130/20 1330-20-7 Xylene (total)4860 1500 6380 101 1500 6450 106 1 70-130/20 CAS No.Surrogate Recoveries MS MSD FA88905-1 Limits 1868-53-7 Dibromofluoromethane 98%98%97%70-130% 17060-07-0 1,2-Dichloroethane-D4 105%105%103%70-130% 2037-26-5 Toluene-D8 99%97%97%70-130% 460-00-4 4-Bromofluorobenzene 100%98%97%70-130% * = Outside of Control Limits. 52 of 52 FA8890555.3.2 APPENDIX C Contaminant Mass Calculations Area ID Well ID Area (ft²) Average Well Depth (ft.) Average Depth to Water (ft.) Water Column Height (ft) Volume (ft³) Volume (L) Effective Porosity Effective Volume (L) MW-2 MW-9 MW-10 MW-26 MW-27 RW-1 Area Date Well Benzene (μ/L) Toluene (μ/L) Ethylbenzene (μ/L) Xylenes (μ/L) MTBE (μ/L) Naphthalene (μ/L) Total (μ/L) DTW (ft.) Average Water Column Height (ft.) Total Average Mass (g)Percent Red.To Date Red. MW-2 159.00 738.00 935.00 4150.00 0.00 367.00 6349.00 0.99 MW-9 22.50 104.00 80.30 219.00 0.00 38.20 464.00 1.59 MW-10 109.00 106.00 907.00 1650.00 0.00 626.00 3398.00 1.27 MW-26 138.00 140.00 256.00 526.00 0.00 90.60 1150.60 1.73 MW-27 860.00 4990.00 1080.00 3670.00 0.00 317.00 10917.00 0.86 RW-1 15.30 3.00 43.90 36.10 0.00 39.00 137.30 0.71 Avg.217.30 1013.50 550.37 1708.52 0.00 246.30 3735.98 1.19 MW-2 258.00 1180.00 1390.00 6280.00 0.00 373.00 9481.00 2.01 MW-9 42.70 3.70 152.00 292.00 0.00 82.30 572.70 2.66 MW-10 110.00 105.00 753.00 1340.00 0.00 386.00 2694.00 2.40 MW-26 527.00 846.00 289.00 1370.00 0.00 93.40 3125.40 2.43 MW-27 79.90 970.00 173.00 574.00 20.70 50.30 1867.90 2.00 RW-1 30.70 58.40 145.00 182.00 0.00 59.10 475.20 1.82 Avg.174.72 527.18 483.67 1673.00 3.45 174.02 3036.03 2.22 MW-2 150.00 565.00 1210.00 4860.00 0.00 413.00 7198.00 5.98 MW-9 10.90 0.31 0.27 1.50 1.10 4.80 18.88 6.20 MW-10 96.10 70.20 742.00 1010.00 0.00 528.00 2446.30 6.38 MW-26 120.00 344.00 72.70 341.00 0.00 28.10 905.80 6.53 MW-27 29.50 37.60 106.00 232.00 0.00 43.00 448.10 5.90 RW-1 36.90 68.90 138.00 119.00 0.00 106.00 468.80 5.83 Avg.73.90 181.00 378.16 1093.92 0.18 187.15 1914.31 6.14 Date Average Water Column Height (ft.) 06/02/20 1.19 04/26/21 2.22 09/13/21 6.14 Notes: • FP: Free Product • Area of the contaminant plume is calculated from Figure 6 • Height of the water column is calculated by subtracting the average depth to water from the average well depth of the referenced monitoring wells • Volume of the contaminant plume is calculated by multiplying the area of the plume by the average height of the water column during each sampling event • Effective porosity is assumed based on the sub-surface soil profile obtained from well construction records and soil boring logs • Total mass was calculated by multiplying the total contaminant concentrations for the sampling event with effective volume • Contaminant mass cannot be calculated in wells containing FP; therefore, the total contaminant mass is based on the known concentrations in the area for each sampling event. • When areas couldn’t be sampled, the last known concentrations were used in the calculations. Area 1 09/13/21 64.2%53.0%1,971.8911.44 04/26/21 15.36 4,197.74 23.8%23.8% 16.39 236,802 6,705,486 1,475,2070.22 1972 64.2%64.2% Percent Reduction To Date --- Percent Reduction Compared to Previous Event --- Total Contaminant Mass (g) 5,511 23.8%23.8%4,198 APPENDIX C PERCENTAGE REDUCTIONS PERRYTOWN SERVICE CENTER (INCIDENT NO. 13261) Baseline Event 1 14,449.5 17.58 1.19 06/02/20 16.39 ------5,511.35