WA-1010_12511_CA_RPTS_20201207_MRP

GROUNDWATER MONITORING REPORT

BP SERVICE CENTER
4673 US HIGHWAY 117 NORTH, PIKEVILLE, WAYNE COUNTY, NC 27863
GROUNDWATER INCIDENT #: 12511
FACILITY ID #: 0-006989

DECEMBER 7, 2020

UST OWNER/OPERATOR:
MARY P. PENDER (DECEASED)

PROPERTY OWNER:
DANNY S. PENDER
603 FOXWOOD DRIVE, GOLDSBORO, NC 27530-8461
PHONE NUMBER: [phone]

CONSULTANT:
HENRY NEMARGUT ENGINEERING SERVICES
2211 CHESTNUT STREET, WILMINGTON, NC 28405
PHONE NUMBER: [phone]

RELEASE INFORMATION:
DATE DISCOVERED: 12/27/93
ESTIMATED QUANTITY OF RELEASE: UNKNOWN
CAUSE OF RELEASE: UNKNOWN
SOURCE OF RELEASE: UST SYSTEM
SIZE AND CONTENTS: (2) 6,000 GAL + (1) 3,000 GAL GASOLINE USTS
LATITUDE: N 35o 29'17"; LONGITUDE: W 77o 58’55”

The Monitoring Report for this site has been prepared by Henry Nemargut Engineering
Services. All engineering work performed on this project was conducted under my direct
supervision:

Henry Nemargut, P.E.
Henry Nemargut Engineering Services
North Carolina License #17669

December 7, 2020

Danny S. Pender
603 Foxwood Drive
Goldsboro, NC 27530-8461

Reference: Groundwater Monitoring Report
BP Service Center
4673 US Highway 117 North
Pikeville, Wayne County, North Carolina 27863
Incident #12511; Facility ID #0-006989
Risk Classification: High

Dear Mr. Pender:

Please find enclosed a report summarizing groundwater monitoring activities conducted at the
above referenced facility. Previous assessment activities at this site revealed a release of
petroleum in groundwater in the vicinity of the former location of a gasoline UST and dispenser
island. Fifteen on and off site monitor wells and three local supply/irrigation wells were sampled
in September, 2020 to evaluate the site for the presence of dissolved gasoline constituents. Other
activities included removal of nutrient socks in on-site and off-site monitoring wells due to
NCDEQ policy changes. The findings of this investigation are summarized herein.
Mr. Pender, if you have questions regarding this report please contact my office.
Sincerely,

Henry Nemargut, P.E.
Henry Nemargut Engineering Services

B. EXECUTIVE SUMMARY
1. Free Product: Free product has never been detected in any monitor well, boring, or excavation at the site.

2. Contaminant Mass: Based on the soil & groundwater data from the post soil remediation soil assessment and the initial 2013 post soil remediation groundwater assessment, the estimated total contaminant mass at this site during initial investigations was 184 lbs of total petroleum mass, which includes an estimated 24.5 lbs of petroleum dissolved into the aqueous phase at this site. The latest groundwater monitoring event conducted on September 24, 2020 indicates that an estimated 3.23 lbs of petroleum contaminant mass remains dissolved in groundwater at the site based on analytical data. Current data indicates a 86.9% contaminant decrease in dissolved aqueous phase petroleum mass has occurred at the site, due to soil remediation, natural processes and use of nutrient socks.

3. Maximum Concentrations of Dissolved Groundwater Contaminants:

Current Groundwater Maximums:
Contaminant Result Well ID 2L Standard Benzene 18.8 ug/L (MW-7) 1 ug/L Naphthalene 45.6 ug/L (MW-7) 70 ug/L 1,2 - Dichloroethane 4.1 ug/L (MW-3) 0.4 ug/L 1,2 - Dichloropropane 2.0 ug/L (SW-1) 0.6 ug/L MTBE 110 ug/L (MW-1) 20 ug/L Total 6200B 889 ug/L (MW-7) NSE No other compounds exceeded 2L Standards for 6200B compounds during the latest groundwater monitoring event for this site. Benzene was noted at levels above its GCL in dispenser source area monitoring well MW-8 prior to soil remediation activities conducted in October, 2012. 4. Extent of Dissolved Groundwater Contamination: The plume of dissolved groundwater contamination appears to be reducing at this site. Historically, the plume was centered on the source area around the front dispensers and USTs removed in 1987, with the highest amount of contamination present in MW-8 removed via remedial excavation. Currently, 2L Violations are present in both the south and northwest directions at relatively low levels compared to the maximum historical contaminant concentrations. Seasonal groundwater tables have caused migration of contaminants originating from this site towards the south and northwest during wet and dry seasons. 5. Maximum Soil Contaminant Concentrations (Following over-excavation conducted in October 2012): Contaminant Result Sample ID Lowest MSCC Benzene 0.967 mg/kg (E2) 0.0056 mg/kg Naphthalene 1.54 mg/kg (W2) 0.16 mg/kg 1,2,4-Trimethylbenzene 10.5 mg/kg (W2) 8.5 mg/kg MTBE 0.683 mg/kg (E3) 0.091 mg/kg C5-C8 Aliphatics 96.3 mg/kg (W4) 68 mg/kg C9-C18 Aliphatics 51.4 mg/kg (W4) 540 mg/kg C9-C22 Aromatics 54 mg/kg (W4) 31 mg/kg
Approximately 50 cubic yards of contaminated soil was removed and disposed of from the 3,000 gallon gasoline UST excavation in 1994. In October, 2012 an additional 2443.38 tons of contaminated soils were removed and disposed of from the front dispenser island/UST area. Remaining contaminated soils are predominantly located beneath the on-site building structure. Based on the high risk classification for this site, lowest MSCC standards apply for this site. 6. Remedial Action Plan:
No CAP has been developed for this site. The NCDEQ Washington Regional Office has approved the experimental use of nutrient socks at this site to evaluate their effectiveness on contaminant reduction at this site. Nutrient socks have been installed at this site on the following dates: March 9, 2017 (nutrient only) November 2, 2017 (nutrient only) May 19, 2018 (nutrient + nutrient/oxygenating) The data collected from this latest sampling event indicates that the addition of nutrient socks at this site have been effective in reducing remnant dissolved constituent concentrations at this site. It is recommended that nutrient socks replacement be continued at this site based on evaluation of contaminant reductions noted in wells in which socks were utilized.
7. Impacted Receptors:

The water supply well (SW-1) formerly serving the NC Historic Sites Vehicle
Maintenance facility (now vacant) routinely contained 1,2-Dichloropropane
during testing through 2016 and was found to contain 1,2-DCA at a concentration
of 2.0 ug/l during this latest monitoring event. The maximum level of 1,2-
Dichloropropane observed at this site was 2.2 ug/l during testing on May 15, 2015
and August 17, 2016. The 2L Standard for 1,2-Dichloropropane is 0.6 ug/l. 1.2-
Dichloropropane has never been detected at a concentration above detection limits
in any monitoring well at the BP Service Center site or in any other local supply
well tested during the monitoring events conducted in conjunction with the
investigation of this release.

Other wells that have been tested during the monitoring history of this site include
irrigation wells IW-3 (Mattie Artis Residence) and IW-4 (Tedaro Reid
Residence), and supply well SW-8 which serves Judee’s Hair Salon. At no time
during historical testing have any 6200B compounds been detected in any of these
wells. No other supply wells have been tested in conjunction with this release.

TABLE OF CONTENTS

Section Page 1.0 Site History and Characterization 1.1 Introduction .................................................................... 1 1.2 Scope of Services ........................................................... 2 2.0 Presentation of Current Site Assessment Information / Comparison to Historical Assessment Information 2.1 Historical Soil Assessment Information ........................ 2 2.2 Well Sock Installation .................................................... 2 2.3 Groundwater Flow Direction and Gradient ................... 3 2.4 Monitor Well Sampling and Analyses ........................... 3 2.5 Monitor Well Sampling and Analyses ........................... 3 2.6 Regional / Site Geology and Hydrogeology .................. 4 2.7 Plume Development ....................................................... 5 3.0 Monitored Natural Attenuation 3.1 Natural Source Zone Depletion Status ........................... 5 4.0 Conclusions 4.1 General Summary .......................................................... 6 4.2 Recommendations .......................................................... 6 4.3 Limitations ..................................................................... 6 5.0 Statements and Certification 5.1 Statements ...................................................................... 7 5.2 Certification ................................................................... 7

LIST OF FIGURES Figure 1: Project Location Figure 2: Receptor Map Figure 3: Soil Concentrations Map Figure 4: Site Layout, Former UST, and Monitor Well Locations Figure 5: Potentiometric Surface Map (9/24/20) Figure 6: Shallow Well Benzene Isoconcentration Map Figure 7: Shallow Well Naphthalene Isoconcentration Map Figure 8: Shallow Well MTBE Isoconcentration Map Figure 9: Shallow Well 1,2-DCA Isoconcentration Map Figure10: Shallow Well Total 6200B Isoconcentration Map Figure10H: Baseline Shallow Well Total 6200B Isoconcentration Map

LIST OF TABLES Table 1: Site History Table 2: Summary of Soil Analytical Results
Table 3: Monitoring Well Information and Groundwater Elevations Table 4: Summary of Groundwater Analytical Results Table 5: Water Supply Well Information Table 6: Mass Calculation Table Table 7: Historical Water Analytical Summary

APPENDICES

Appendix A: Laboratory Analytical Results

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GROUNDWATER MONITORING REPORT BP Service Center 4673 US Highway 117 North, Pikeville, North Carolina
1.0 Site History and Characterization

1.1 Introduction

Danny S. Pender is the property owner of a site which was formerly operated as the BP
Service Center facility located at 4673 US Highway 117 North in Pikeville, North
Carolina. Figure 1 illustrates the location of this facility on the Northeast Goldsboro
Quadrangle U.S.G.S. Topo Map. This facility contains one permanent structure which is
used as a gasoline convenience store. The site formerly contained (2) 6,000 gallon
gasoline USTs which were removed from this facility in 1987 (T1/T2) and (1) 3,000
gallon gasoline UST which was removed from this facility on December 27, 1993 (T3).
A release was noted from UST #T3 during 1993 closure activities. Assessment activities
including initial site characterization activities conducted in 1994, and comprehensive
site assessment conducted at this site in 2010 have been conducted at this site. Most
recently, secondary sources (contaminated soil) were removed from the site in the former
pump island area in October, 2012. Table 1 contains a history of the USTs formerly
operated at this facility. Figure 2 illustrates the layout of this site, the UST locations, and
the monitor well locations. The site currently contains (2) 6,000 gallon ASTs. These
ASTs and associated piping underwent integrity testing prior to submittal of an
application for eligibility of this site onto the NCDEQ Trust Fund. All ASTs and
associated piping passed integrity tests which confirm that they have not contributed to
the contamination noted at this site.
The site has been ranked as High Risk based on potable supply wells located within
1,000’ and irrigation wells located within 250’ of the release source at this facility.
Information about the supply wells is contained in Table 5. Supply well SW-1 located at
the site of the NC Historic Sites Vehicle Maintenance facility (now vacant) routinely
contained 1,2-Dichloropropane during testing through 2016, but has not been tested
during 2017-2018 since the facility is currently vacant and the water supply is not being
used. The maximum level of 1,2-Dichloropropane observed at this site was 2.2 ug/l
during testing on May 15, 2015 and August 17, 2016. The 2L Standard for 1,2-
Dichloropropane is 0.6 ug/l. The other irrigation and supply wells within 250’ of the
petroleum release source area have never indicated impact by petroleum compounds
during routine monitoring events conducted at this facility. Table 5 contains ownership
information for local water supply wells with their locations depicted graphically on
Figure 2.
No CAP has been developed for this site. The NCDEQ Washington Regional Office has
approved the experimental use of nutrient socks at this site to evaluate their effectiveness
on contaminant reduction at this site. Nutrient socks were first introduced on this site on
March 9, 2017, with replacement on a 6 month basis. Evaluation of the effectiveness of
sock addition indicates that addition of these nutrient socks is contributing to contaminant
reduction at this site.
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1.2 Scope of Services

Contained herein are the results of a groundwater sampling event as approved by the
NCDEQ. This Groundwater Monitoring Report contains documentation concerning the
following activities which have been conducted at this facility:

o Sampling of fifteen monitor wells and three supply wells conducted by Henry Nemargut Engineering on September 24, 2020

o Laboratory analyses of groundwater samples conducted by Pace Analytical, Inc. of Huntersville, NC.

o Removal of nutrient and oxygenating nutrient socks at this site. 2.0 Presentation of Current Site Assessment Information / Comparison to Historical Assessment Information 2.1 Historical Soil Assessment Information
On October 10-15, 2012, during the excavation of 2443.38 tons of impacted soils from
the front UST/dispenser island area, soil samples were collected from in-situ soils at the
limits of excavation at the site. The in-situ wall soil samples collected at the limits of the
remedial excavation were submitted to SGS North America, Inc. for analyses by EPA
Method 8260 (by Method 5035 sample preparation) and MADEP methods for Volatile
Petroleum Hydrocarbons (VPH). The soil samples were obtained as specified in the
collection, preservation, and handling section of the specific method. Each container was
labeled with sample location, analyses to be performed, time, date, and the sampler's
name. They were then placed in a cooler and chilled with ice to approximately 4oC in
preparation for transportation to the analytical laboratory utilizing EPA approved chain of
custody procedures.
Laboratory analytical results for the risk-based soil samples collected at the limits of the
remedial excavation indicate that contaminants at this site have been remediated to below
the Residential Maximum Soil Contaminant Concentrations (MSCCs). 6
compounds/compound groups were noted at the site above Lowest MSCCs in samples
obtained from the walls of the remedial excavation. These compounds included Benzene,
Naphthalene, 1,2,4-Trimethylbenzene, MTBE, C5-C8 Volatile Aliphatics, and C9-C22
Aromatics. VPH sample results were at their highest in the west wall samples were
further over-excavation was not possible due to the location of the building structure
Figure 3 illustrates the locations of the risk-based soil samples collected at the subject
site, and Table 2 summarizes the laboratory results for the “Risk-Based” soil samples
from 4673 US Highway 117 North in Pikeville, NC. Laboratory analytical reports and
the chain of custody records for the soil samples collected at the project site in
conjunction with abatement activities are contained in the November 2, 2012 IAA report
submitted for this site.
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Results from the closure of the 3 USTs removed from this site in 1987-1993 did not
include any collection of risk-based results since the risk based rules were first developed
in 1998.

2.2 Well Sock Installation

On September 24, 2020, nutrient socks were removed from wells MW-3, 9, 12, 14, 16 &
17, with oxygenating/nutrient socks removed from monitoring wells MW1, MW-2, MW-
7, & MW-18. The purpose of introduction of these socks was to provide nutrients and
oxygen necessary for bio-degradation process within the contaminant plume at the site.
The socks were not replaced due to recent NCDEQ policy changes.

2.3 Ground Water Flow Direction and Gradient

In order to estimate the groundwater flow direction in the vicinity of the petroleum
release, elevations of the monitor well casings were measured using surveying
equipment. Static water levels were obtained from the monitor wells and the data was
used to compute a potentiometric surface map. Figure 5 illustrates the current
potentiometric surface map as calculated based on the measurements obtained on
September 24, 2020.
Groundwater data and monitoring well information were also used to estimate the
hydraulic gradient at the project site. Using the horizontal distance between the monitor
wells and the static water levels, the groundwater was calculated to flow in multiple
directions away from mounding noted in the former UST pit/soil remediation area. The
predominant flow directions are toward the south with a hydraulic gradient of
approximately 0.011 ft/ft and towards the west/northwest with a gradient of 0.0035 ft/ft.
Groundwater elevation data from VEW-1 suggests a vertically downward gradient exists
in the source area of this release site.
2.4 Monitor Well Sampling and Analyses

On September 24, 2020, monitor wells MW-1, MW-2, MW-3, MW-4, MW-7, MW-8A,
MW-9, MW-12, MW-13, MW-14, MW-15, MW-16, MW-17, MW-18, &VEW-1 were
sampled for analyses utilizing EPA Method 6200B plus MTBE and IPE. Before
collecting the samples the monitor wells were purged by removing a minimum of three
well volumes to ensure that the samples were representative of the actual groundwater
conditions. The wells were developed using disposable plastic bailers suspended with
unused nylon string.
All samples were placed in laboratory supplied glassware, labeled with sample location,
analysis to be performed, time, date and sampler's name. The sample jars were then
immediately placed in a cooler, chilled with ice to approximately 4oC in preparation of
transportation to an analytical laboratory utilizing EPA approved chain-of-custody
procedures.
Page - 4

Laboratory analytical results indicate the presence of 4 compounds above the current
listed 2L Standards in the monitor well network at this site. Total 6200B compounds
were detected at a maximum level of 889 ug/l in well MW-7. Benzene was detected at a
maximum concentration of 18.8 ug/l in MW-7, above its 2L standard of 1 ug/l but below
its GCL of 5,000 ug/l. No GCL violations were noted at the site. Naphthalene was
detected at a maximum concentration of 45.6 ug/l in monitoring well MW-7, and MTBE
was noted at a maximum level of 110 ug/l in well MW-1 above its 2L Standard of 20
ug/l. 1,2-DCA was noted present above 2L Standards in 6 monitoring wells at the site
with a maximum concentration noted in MW-3 at a level of 4.1 ug/l. Table 4 summarizes
the laboratory analytical results, and Appendix A contains a copy of the laboratory
analytical report and chain of custody records. Figure 6 contains a benzene iso-
concentration map, Figure 7 illustrates the estimated naphthatlene concentration map,
Figure 8 illustrates the MTBE isoconcentration for the site, and Figure 9 illustrates the
1,2-DCA isoconcentration map. Figures 10 and 10H illustrate the current Total 6200B
and baseline historical Total 6200B isoconcentration maps which were prepared for mass
calculation purposes.

2.5 Supply Well Sampling and Analyses

On September 24, 2020, three off-site area supply wells were sampled for analyses
utilizing EPA Methods 6200B plus MTBE, IPE, & EDB. Before sampling, the supply
wells were purged by pumping from the wells for approximately 10 minutes to ensure
that the samples were representative of the actual groundwater conditions. After
pumping, the flowrate was reduced for collection of samples. Samples were obtained
from spigots closest to the various supply wells. The three supply wells sampled
included: SW-1 owned by Travis Thigpen, formerly operated by the NC State Historic
Mechanics Shop (not rented at this time); IW-3 owned by Mattie Artis used for irrigation
purposes; and SW-8, owned by David Daw, used as a water source at JuDee’s Hair &
Body.

All samples were placed in laboratory supplied glassware, labeled with sample location,
analysis to be performed, time, date and sampler's name. The sample jars were then
immediately placed in a cooler, chilled with ice to approximately 4oC in preparation of
transportation to an analytical laboratory utilizing EPA approved chain-of-custody
procedures.

Laboratory analytical results failed to indicate the presence of any compounds above
laboratory detection limits in supply wells IW-3 and SW-8 sampled on September 24,
2020. Supply well SW-1 owned by Travis Thigpen indicated the presence of 1,2-
Dichloropropane at a concentration of 2.0 ug/l, above its 2L Standard of 0.6 ug/l. Table 4
summarizes the laboratory analytical results, and Appendix A contains a copy of the
laboratory analytical report and chain of custody records. Table 5 summarizes supply
well owner information.

Page - 5
2.6 Regional / Site Geology and Hydrogeology
The site is situated in the Coastal Plain Physiographic Province. According to the
Geological Map of North Carolina local geology of the region is called the Yorktown
Formation and Duplin Formation consisting of fossiliferous clay with varying amounts of
fine grained sands commonly concentrated in lenses. Bedrock was not encountered to a
depth of 55 feet below surface which was the maximum depth explored during the
subsurface investigation. The soils at the project site consist predominantly of clays &
silts with sand at shallow depths (<12’ deep) with sands with varying amounts of silt &
clay at greater depths (>12’ deep).

Groundwater is noted to be flowing predominantly towards the south according to the
estimated potentiometric surface map based on September 24, 2020 measurements. The
average potentiometric surface gradient has been calculated at approximately 0.0074 ft/ft
as observed on this date. Three single well rising head tests or "slug tests" were
performed on MW-7, MW-9 and MW-12 to determine the saturated hydraulic
conductivity of the water table aquifer. The method of Bouwer and Rice (Bouwer and
Rice, 1989, 1976) was chosen to reduce the slug test data. A computer program
developed by the Geraghty & Miller Modeling Group named AQTESOLV was used to
estimate the aquifer parameters. Results of the slug tests indicated a hydraulic
conductivity of 1.104 x10-4 feet/minute for MW-7, 2.822 x10-4 feet/minute for MW-9,
and 7.227 x 10-4 feet/minute for MW-12. These results are consistent with published
values for silty sand and silt, loess (Freeze & Cherry, 1979).
Average groundwater flow velocity at the site is calculated to be 1.66 x 10-5 feet/minute
(11.0 feet/year). Flow through the sandy lenses at the site is estimated to be over 20
ft/minute, based on data from MW-12.

2.7 Plume Development

In prior sampling events conducted at the site, contaminants have been reported above 2L
Standards in on-site and off-site monitoring wells and in off-site water supply wells. The
Travis Thigpen well (SW-1) is no longer being used since the previous tenant vacated the
property.

The contaminant concentrations in well MW-18 downgradient of the source area during
wet seasons had continually decreased since the initial sampling event conducted on
April 18, 2013 through the 2015 sampling event, most likely due to soil remediation. The
latest 4 sampling events indicate continued decreases in the MW-18 BTEX level since
the 2015 spike, with a historical low noted in the latest 9/24/20 sampling event. Total
BTEX concentrations in groundwater in the pump island source area, previously above
its GCL for benzene, have remained below detection limits in MW-8A as a result of soil
remediation.

The groundwater flow direction was predominantly towards the south during the
September 24, 2020 sampling event. Seasonal BTEX increases in the south direction
Page - 6
towards MW-7 and MW-2 are generally noted during dry seasons. In general,
contaminant concentrations appear to be reducing at site in all wells. Historical analytical
laboratory data are summarized in detail in Table 7. Installation of nutrient socks in
monitoring wells MW-1, MW-2, MW-3, MW-7, MW-9, MW-14, MW-12, MW-16,
MW-17 & MW-18 appear to have accelerated natural processes in these monitoring
wells. 3.0 Monitored Natural Attenuation 3.1 Natural Source Zone Depletion Status
Historically, GCL violations for benzene were noted in monitoring well MW-8 prior to
IAA soil excavation conducted in 2012. The groundwater contaminant plume appears to
have migrated both to the south and to the northwest, most likely due to observed
fluctuations in flow directions noted during wet and dry seasons. Please note, not all of
the on-site monitoring wells were sampled as part of this groundwater monitoring event
due to a scope modification requested by the NCDEQ. However, based on the results of
previous groundwater sampling events, it appears that the groundwater contaminant
plume has been adequately defined in the direction of local receptors. Targeted
petroleum concentrations detected in the groundwater samples collected from the select
monitoring wells within the plume appear to be decreasing significantly since the last
groundwater sampling event in 2018. The size and orientation of the groundwater plume
appears to be relatively unchanged since the previous sampling event based on the
sampling of the select monitoring wells.
Appendix E contains a copy of the laboratory report and the chain-of-custody record for
the groundwater samples obtained on September 24, 2020. 4.0 Conclusions

4.1 General Summary

A Groundwater Monitoring event at BP Service Center located at 4673 US Highway 117
North in Pikeville, NC has been completed. From a review of all information gathered
during this monitoring project, Henry Nemargut Engineering makes the following
conclusions:

o 4 compounds above the current listed 2L Standards in the monitor well network at
this site during the sampling event conducted on September 24, 2020. Benzene
was detected at a maximum concentration of 18.8 ug/l in MW-7, above its 2L
standard of 1 ug/l but below its GCL of 5,000 ug/l. No GCL violations were
noted at the site. Naphthalene was detected at a maximum concentration of 45.6
ug/l in monitoring well MW-7, and MTBE was noted at a maximum level of 110
ug/l in well MW-1 above its 2L Standard of 20 ug/l. 1,2-DCA was noted present
above 2L Standards in 6 monitoring wells at the site with a maximum
concentration noted in MW-3 at a level of 4.1 ug/l

Page - 7
o Three nearby in-use water supply wells were sampled on September 24, 2020: SW-1 owned by Travis Thigpen, formerly operated by the NC State Historic Mechanics Shop (not rented at this time); IW-3 owned by Mattie Artis used for irrigation purposes; and SW-8, owned by David Daw, used as a water source at JuDee’s Hair & Body. Laboratory analytical results failed to indicate the presence of any compounds above laboratory detection limits in supply wells IW-3 and SW-8 sampled on September 24, 2020. Supply well SW-1 owned by Travis Thigpen indicated the presence of 1,2-Dichloropropane at a concentration of 2.0 ug/l, above its 2L Standard of 0.6 ug/l.

o On September 24, 2020, nutrient socks were removed from all monitoring wells at this site due to NCDEQ policy changes.

o Based on the results of previous groundwater sampling events, it appears that the groundwater contaminant plume has been adequately defined in the direction of local receptors. Historical groundwater data suggests that removal of secondary sources at this site in 2012 significantly reduced the dissolved contaminant plume at this site. Installation of nutrient socks in monitoring wells MW-1, MW-2, MW-3, MW-7, MW-9, MW-14, MW-12, MW-16, MW-17 & MW-18 appear to have accelerated natural processes in these monitoring wells.

4.2 Recommendations

Based on information obtained during this sampling event, Henry Nemargut Engineering
Services makes the following recommendations for this site:

o Semi-annual monitoring should be continued at this site.

o Nutrient socks should be replaced on a semi-annual basis at this site since
groundwater data suggests that socks are assisting in contaminant concentration
reductions.
A copy of this monitoring report has been forwarded to the following address:

Jared Edwards
NCDEQ-WaRO UST Section
943 Washington Square Mall
Washington, NC 27889 4.3 Limitations
This report has been prepared for the exclusive use of Danny S. Pender for the specific application to the referenced site located in Wayne County, North Carolina. The assessment was conducted based on the scope of work and level of effort desired by the client. Our findings have been developed in accordance with generally accepted standards in the practice of Groundwater Monitoring Reports in the State of North Carolina, available information, and our professional judgment. No other warranty is expressed or implied.

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The data presented in this report are indicative of conditions that existed at the precise locations sampled and at the time the samples were collected. Additionally, the data obtained from the samples would be interpreted as meaningful with respect to the parameters indicated in the laboratory reports. No additional information can be logically inferred from this data. 5.0 Statements and Certification 5.1 Statements No deadline was established for the monitoring report at this site. Will this report be submitted after the established due date? No Was any required information from the template missing from this report? No If applicable, will any of the proposed attenuation milestones under the schedule approved in the Corrective Action Plan not be met? Not Applicable, no CAP has been prepared for this site. Does any known or suspected source zone soil contamination or free product remain outside of the assessed area that could be inhibiting natural attenuation? No Has there been an unexpected increase in contaminant mass sufficient to suggest a potential new release from a separate onsite or offsite source? No 5.2 Certification I, Henry Nemargut, a Professional Engineer, do certify that the information contained in this report is correct and accurate to the best of my knowledge.
Henry Nemargut, P.E.
Henry Nemargut Engineering Services
North Carolina License #17669

FIGURES

TABLES

TABLE 1: SITE HISTORY
BP SERVICE CENTER
4673 US HWY 117 NORTH, PIKEVILLE, NC 27863

Property Ownership:

Danny S. Pender
603 Foxwood Drive
Goldsboro, NC 27530-8461
3/25/2011 to present

UST Ownership:

Tank owner:

Mary and Denton Pender (both deceased)
Original tank owners

UST Information:

Tank Inst. Size Closure UST Tank
No Date (Gal) Date Status Contents

T1 4/27/72 6,000 1/4/87 Removed Gasoline
T2 4/27/72 6,000 1/4/87 Removed Gasoline
T3 4/25/82 3,000 1/14/94 Removed Gasoline

BP Service HIST
Sample Location N E1 W1 E2 W2 W3 Lowest MSCC Ind/Comm MSCC Residential MSCCDate10/10/2012 10/10/2012 10/10/2012 10/11/2012 10/11/2012 10/12/2012 (note units) (note units) (note units)Sample depth8' 8' 8' 8' 8' 8' Method 8260 (ug/kg)Benzene29 818 955 967BDL BDL 5.6 164,000.0 18,000Methyl Ethyl Ketone BDL BDL BDL BDL BDL BDL 16,000 245,280,000 7,821,000Methyl Isobutyl Ketone BDL BDL BDL BDL BDL BDL NSE NSE NSEMethyl Butyl Ketone BDL BDL BDL BDL BDL BDL NSE NSE NSEn-Butylbenzene BDL BDL BDL BDL BDL BDL 4,300 16,350,000 626,000sec-Butylbenzene BDL BDL BDL BDL BDL BDL 3,300 16,350,000 626,000Ethylbenzene 16.8 428 503 450 1860 642 4,900 40,000,000 1,560,000Isopropylbenzene BDL BDL BDL BDL 319 BDL 2,000 40,880,000 1,564,000p-Isopropyltoluene BDL BDL BDL BDL 403 BDL NSE NSE NSENaphthalene 46.5202105 1211540 541160 8176000 313,000Acetone BDL BDL BDL BDL BDL BDL 24,000 360,000,000 14,000,000n-Propylbenzene BDL BDL 56.2 BDL 1400 249 2,000 16,350,000 626,000Toluene 52.3 53.8 BDL BDL BDL BDL 4,300 32,000,000 1,200,0001,2,4-Trimethylbenzene 28.5 424 404 249105001680 8,500 20,440,000 782,0001,3,5-Trimethylbenzene 5.74 116 102 80.4 3010 476 8,300 20,440,000 782,000MTBE 49.2375 597 614BDL BDL 91 3,100,000 350,000Methylene ChlorideBDLBDLBDLBDLBDLBDL20763,00085,000StyreneBDLBDLBDLBDLBDLBDL1,50081,760,0003,128,000Xylenes (total)87.3520611497211022604,60081,760,0003,129,000Method 8270 (ug/kg)ChryseneNRNRNRNRNRNR39,000780,00088,000Benzoic AcidNRNRNRNRNRNR120,000163,520,00062,571,000Phenanthrene NR NR NR NR NR NR 56,000 12,264,000 469,000Pyrene NR NR NR NR NR NR 270,000 12,264,000 469,0002-Methylnapthalene NR NR NR NR NR NR 3,600 1,635,000 63,000Naphthalene NR NR NR NR NR NR 160 8176000 313,000Aliphatic Fraction Classes (mg/kg) C5 - C8 Volatile Aliphatics BDL BDL BDL BDL 38.3 19.4 68 24,528 939C9 - C12 Volatile Aliphatics BDL BDL BDL BDL 16 16.9 NSE NSE NSEC9-C18 Extractable Aliphatics NR NR NR NR NR NR NSE NSE NSEC9-C18 Aliphatics (total) BDL BDL BDL BDL 16 16.9 540 40,000 1,500C19-C36 Extractable Aliphatics NR NR NR NR NR NR NSE 810,000 31,000Aromatic Fraction Classes (mg/kg) C9 - C10 Volatile AromaticsBDLBDLBDLBDL27.517.3NSENSENSEC11 - C22 Extractable AromaticsNRNRNRNRNRNRNSENSENSEC9 - C22 Aromatics (total)BDLBDLBDLBDL27.517.33112264469BDL = below detection limits NR = analyses not requested NSE = no standard establishedTABLE 2Laboratory Analytical Results - Risk Based Soil SamplesBP Service Center, 4673 Hwy 117, Pikeville, NC 27863
Sample Location E4 W4 E3 S1 S2 Lowest MSCC Ind/Comm MSCC Residential MSCCDate10/13/2012 10/13/2012 10/15/2012 10/15/2012 10/15/2012 (note units) (note units) (note units)Sample depth8' 8' 8' 8' 8' Method 8260 (ug/kg)Benzene BDL79.8BDL BDL BDL 5.6 164,000.0 18,000Methyl Ethyl Ketone BDL BDL BDL BDL BDL 16,000 245,280,000 7,821,000Methyl Isobutyl Ketone BDL BDL BDL BDL BDL NSE NSE NSEMethyl Butyl Ketone BDL BDL BDL BDL BDL NSE NSE NSEn-Butylbenzene BDL BDL BDL BDL BDL 4,300 16,350,000 626,000sec-Butylbenzene BDL BDL BDL BDL BDL 3,300 16,350,000 626,000Ethylbenzene BDL 512 BDL 8.16 BDL 4,900 40,000,000 1,560,000Isopropylbenzene BDL 43 BDL BDL BDL 2,000 40,880,000 1,564,000p-Isopropyltoluene BDL BDL BDL BDL BDL NSE NSE NSENaphthalene BDL177BDL 6.68 BDL 160 8176000 313,000Acetone BDL BDL BDL BDL BDL 24,000 360,000,000 14,000,000n-Propylbenzene BDL BDL BDL BDL BDL 2,000 16,350,000 626,000Toluene BDL BDL BDL 6.41 BDL 4,300 32,000,000 1,200,0001,2,4-Trimethylbenzene BDL 881 BDL 6.36 BDL 8,500 20,440,000 782,0001,3,5-Trimethylbenzene BDL 217 BDL BDL BDL 8,300 20,440,000 782,000MTBE114BDL68336.643891 3,100,000 350,000tert-butylbenzeneBDLBDLBDLBDLBDL3,40016,350,000626,0001,2-DibromoethaneBDLBDLBDLBDLBDLNSENSENSEXylenes (total)BDL1120BDL28.8BDL4,60081,760,0003,129,000Method 8270 (ug/kg)ChryseneNRNRNRNRNR39,000780,00088,000Benzoic AcidNRNRNRNRNR120,000163,520,00062,571,000PhenanthreneNRNRNRNRNR56,00012,264,000469,000PyreneNRNRNRNRNR270,00012,264,000469,0002-Methylnapthalene NR NR NR NR NR 3,600 1,635,000 63,000Naphthalene NR NR NR NR NR 160 8176000 313,000Aliphatic Fraction Classes (mg/kg) C5 - C8 Volatile Aliphatics BDL96.3BDL BDL BDL 68 24,528 939C9 - C12 Volatile Aliphatics BDL 51.4 BDL BDL BDL NSE NSE NSEC9-C18 Extractable Aliphatics NR NR NR NR NR NSE NSE NSEC9-C18 Aliphatics (total) BDL 51.4 BDL BDL BDL 540 40,000 1,500C19-C36 Extractable Aliphatics NR NR NR NR NR NSE 810,000 31,000Aromatic Fraction Classes (mg/kg) C9 - C10 Volatile Aromatics BDL 54 BDL BDL BDL NSE NSE NSEC11 - C22 Extractable Aromatics NR NR NR NR NR NSE NSE NSEC9 - C22 Aromatics (total)BDL54BDLBDLBDL3112264469BDL = below detection limitsNR = analyses not requestedNSE = no standard establishedTABLE 2 (Continued)Laboratory Analytical Results - Risk Based Soil SamplesBP Service Center, 4673 Hwy 117, Pikeville, NC 27863
TABLE 3Monitoring Well Information and Groundwater ElevationsBP Service Center4673 US Hwy 117 North, Goldsboro, NCWell Number Top of Casing Elevation Top of Screen Elevation Bottom of Screen Elevation Depth to Water Groundwater ElevationMW-1 98.12 93.12 78.12 2.67 95.45MW-2 98.49 93.49 78.49 3.52 94.97MW-3 100.00 95.00 80.00 3.96 96.04MW-4 99.95 94.95 79.95 4.56 95.39MW-5 98.06 93.06 78.06 1.51 96.55MW-6 98.68 93.68 78.68 n/a #VALUE!MW-7 96.74 91.74 76.74 1.72 95.02MW-8A 97.66 95.16 80.16 1.41 96.25MW-9 96.73 94.23 76.73 1.38 95.35MW-10 95.68 93.18 75.68 n/a #VALUE!MW-11 96.84 94.34 77.84 n/a #VALUE!MW-12 97.98 95.48 77.98 2.42 95.56MW-13 98.68 96.18 78.18 2.51 96.17MW-14 98.90 96.40 78.40 3.33 95.57MW-15 98.44 95.44 78.44 3.00 95.44MW-16 97.62 94.62 77.62 2.21 95.41MW-17 97.33 92.33 77.33 1.96 95.37MW-18 97.99 95.49 70.49 1.80 96.19VEW-198.0958.0948.096.7991.30All measurements taken in feet and based on an arbitrary benchmark of 100.00 feet at MW-3Groundwater levels measured on 9/24/20BP Service
Constituent MW-1 MW-2 MW-3 MW-4 GCL 2L Standard

Date 9/24/20 9/24/20 9/24/20 9/24/20
Method 6210D (ug/L)
Benzene 13.1 0.97 4.7 BDL 5,000 1
Toluene BDL BDL 0.97 BDL 260,000 600
Ethylbenzene 6 BDL 3.9 BDL 84,500 600
Xylenes (total) 0.56 BDL BDL BDL 85,500 500
BTEX (total) 19.66 0.97 9.57 0 NSE NSE
p-Isopropyltoluene BDL BDL BDL BDL NSE NSE
Isopropylbenzene 2.2 0.52 11.6 BDL 25,000 70
Chloromethane BDL BDL BDL BDL 3,000 3
Naphthalene 8.7 BDL 9.7 BDL 6,000 6
n-propylbenzene 2.7 BDL 3.1 BDL 30,000 70
n-butylbenzene BDL BDL BDL BDL 6,900 70
sec-Butylbenzene BDL BDL 3.6 BDL 15,000 70
tert-Butylbenzene BDL BDL BDL BDL 15,000 70
Acetone BDL BDL BDL BDL 6,000,000 6,000
MTBE 110 6.7 2.1 BDL 20,000 20
1,2-Dichloroethane 0.84 0.9 4.1 BDL 400 0.4
Isopropyl Ether (IPE) 0.99 BDL BDL BDL 70,000 70
trans-1,2-Dichloroethene BDL BDL BDL BDL 100,000 100
1,2,4-Trimethylbenzene 2.5 BDL BDL BDL 28,500 400
1,3,5-Trimethylbenzene BDL BDL BDL BDL 25,000 400
Total 6200B 147.59 9.09 43.77 0 NSE NSE
Aliphatic Fraction Classes (ug/L)
C5-C8 Volatile Aliphatics N/A N/A N/A N/A NSE 420
C9-C12 Volatile Aliphatics N/A N/A N/A N/A NSE NSE
C9-C18 Extractable Aliphatics N/A N/A N/A N/A NSE 4,200
C9-C18 Aliphatics (total) N/A N/A N/A N/A NSE 4,200
C19-C36 Extractable Aliphatics N/A N/A N/A N/A NSE 42,000
Aromatic Fraction Classes (ug/L)
C9-C10 Volatile Aromatics N/A N/A N/A N/A NSE NSE
C11-C22 Extractable Aromatics N/A N/A N/A N/A NSE NSE
C9-C22 Aromatics (total)N/A N/A N/A N/A NSE 210
N/A = Not Analyzed
BDL = Below Detection Limits
NSE = No Standard Established
TABLE 4
SUMMARY OF GROUNDWATER ANALYTICAL RESULTS
BP SERVICE CENTER
4673 US HWY 117 NORTH, GOLDSBORO, NC
Constituent MW-7 MW-8A MW-9 MW-12 GCL 2L Standard

Date 9/24/20 9/24/20 9/24/20 9/24/20
Method 6210D (ug/L)
Benzene 18.8 BDL BDL BDL 5,000 1
Toluene BDL BDL BDL BDL 260,000 600
Ethylbenzene 163 BDL BDL BDL 84,500 600
Xylenes (total) 195.2 BDL BDL BDL 85,500 500
BTEX (total) 377 0 0 0 NSE NSE
p-Isopropyltoluene BDL BDL BDL BDL NSE NSE
Isopropylbenzene 26.2 BDL BDL BDL 25,000 70
Methylene Chloride BDL BDL BDL BDL 5,000 5
Naphthalene 45.6 BDL BDL BDL 6,000 6
n-propylbenzene BDL BDL BDL BDL 30,000 70
n-butylbenzene BDL BDL BDL BDL 6,900 70
sec-Butylbenzene BDL BDL BDL BDL 15,000 70
tert-Butylbenzene BDL BDL BDL BDL 15,000 70
MTBE BDL 12.9 BDL 1.3 20,000 20
1,2-Dichloroethane BDL 0.6 0.82 BDL 400 0.4
Acetone BDL BDL BDL BDL 6,000,000 6000
Isopropyl Ether (IPE) BDL BDL BDL BDL 70,000 70
trans-1,2-Dichloroethene BDL BDL BDL BDL 100,000 100
1,2,4-Trimethylbenzene 348 BDL BDL BDL 28,500 400
1,3,5-Trimethylbenzene 91.9 BDL BDL BDL 25,000 400
Total 6200B 888.7 13.5 0.82 1.3 NSE NSE
Aliphatic Fraction Classes (ug/L)
C5-C8 Volatile Aliphatics N/A N/A N/A N/A NSE 420
C9-C12 Volatile Aliphatics N/A N/A N/A N/A NSE NSE
C9-C18 Extractable Aliphatics N/A N/A N/A N/A NSE 4,200
C9-C18 Aliphatics (total) N/A N/A N/A N/A NSE 4,200
C19-C36 Extractable Aliphatics N/A N/A N/A N/A NSE 42,000
Aromatic Fraction Classes (ug/L)
C9-C10 Volatile Aromatics N/A N/A N/A N/A NSE NSE
C11-C22 Extractable Aromatics N/A N/A N/A N/A NSE NSE
C9-C22 Aromatics (total)N/A N/A N/A N/A NSE 210
N/A = Not Analyzed
BDL = Below Detection Limits
NSE = No Standard Established
TABLE 4 (Continued)
SUMMARY OF GROUNDWATER ANALYTICAL RESULTS
BP SERVICE CENTER
4673 US HWY 117 NORTH, GOLDSBORO, NC
Constituent MW-13 MW-14 MW-15 MW-16 GCL 2L Standard

Date 9/24/20 9/24/20 9/24/20 9/24/20
Method 6210D (ug/L)
Benzene BDL BDL BDL BDL 5,000 1
Toluene BDL BDL BDL BDL 260,000 600
Ethylbenzene BDL BDL 0.78 BDL 84,500 600
Xylenes (total) BDL BDL BDL BDL 85,500 500
BTEX (total) 0 0 0.78 0 NSE NSE
p-Isopropyltoluene BDL BDL BDL BDL NSE NSE
Isopropylbenzene BDL BDL BDL 0.76 25,000 70
Acetone BDL BDL BDL BDL 6,000,000 6,000
Naphthalene BDL BDL BDL 7.7 6,000 6
n-propylbenzene BDL BDL 0.6 1 30,000 70
n-butylbenzene BDL BDL BDL BDL 6,900 70
sec-Butylbenzene BDL BDL BDL BDL 15,000 70
tert-Butylbenzene BDL BDL BDL BDL 15,000 70
MTBE BDL BDL BDL BDL 20,000 20
1,2-Dichloropropane BDL BDL BDL BDL 600 0.6
Isopropyl Ether (IPE) BDL BDL BDL BDL 70,000 70
1,2-Dichloroethane BDL BDL BDL BDL 400 0.4
1,2,4-Trimethylbenzene BDL BDL 1.1 BDL 28,500 400
1,3,5-Trimethylbenzene BDL BDL BDL BDL 25,000 400
Total 6200B 0 0 2.48 9.46 NSE NSE
Aliphatic Fraction Classes (ug/L)
C5-C8 Volatile Aliphatics N/A N/A N/A N/A NSE 420
C9-C12 Volatile Aliphatics N/A N/A N/A N/A NSE NSE
C9-C18 Extractable Aliphatics N/A N/A N/A N/A NSE 4,200
C9-C18 Aliphatics (total) N/A N/A N/A N/A NSE 4,200
C19-C36 Extractable Aliphatics N/A N/A N/A N/A NSE 42,000
Aromatic Fraction Classes (ug/L)
C9-C10 Volatile Aromatics N/A N/A N/A N/A NSE NSE
C11-C22 Extractable Aromatics N/A N/A N/A N/A NSE NSE
C9-C22 Aromatics (total)N/A N/A N/A N/A NSE 210
N/A = Not Analyzed
BDL = Below Detection Limits
NSE = No Standard Established
TABLE 4 (Continued)
SUMMARY OF GROUNDWATER ANALYTICAL RESULTS
BP SERVICE CENTER
4673 US HWY 117 NORTH, GOLDSBORO, NC
Constituent MW-17 MW-18 VEW-1 SW-1 GCL 2L Standard

Date 9/24/20 9/24/20 9/24/20 9/24/20
Method 6210D (ug/L)
Benzene BDL 3.9 BDL BDL 5,000 1
Toluene BDL BDL BDL BDL 260,000 600
Ethylbenzene BDL 6.8 BDL BDL 84,500 600
Xylenes (total) BDL BDL BDL BDL 85,500 500
BTEX (total) 0 10.7 0 0 NSE NSE
p-Isopropyltoluene BDL BDL BDL BDL NSE NSE
Isopropylbenzene BDL 2.2 BDL BDL 25,000 70
Acetone BDL BDL BDL BDL 6,000,000 6,000
Naphthalene BDL 4.8 BDL BDL 6,000 6
n-propylbenzene BDL 5.2 BDL BDL 30,000 70
n-butylbenzene BDL BDL BDL BDL 6,900 70
sec-Butylbenzene BDL 1.9 BDL BDL 15,000 70
tert-Butylbenzene BDL 0.74 BDL BDL 15,000 70
MTBE BDL 81.8 BDL BDL 20,000 20
1,2-Dichloropropane BDL BDL BDL 2 600 0.6
Isopropyl Ether (IPE) BDL BDL BDL BDL 70,000 70
1,2-Dichloroethane BDL 0.98 BDL BDL 400 0.4
1,2,4-Trimethylbenzene BDL 0.64 BDL BDL 28,500 400
1,3,5-Trimethylbenzene BDL BDL BDL BDL 25,000 400
Total 6200B 0 108.96 0 2 NSE NSE
Aliphatic Fraction Classes (ug/L)
C5-C8 Volatile Aliphatics N/A N/A N/A N/A NSE 420
C9-C12 Volatile Aliphatics N/A N/A N/A N/A NSE NSE
C9-C18 Extractable Aliphatics N/A N/A N/A N/A NSE 4,200
C9-C18 Aliphatics (total) N/A N/A N/A N/A NSE 4,200
C19-C36 Extractable Aliphatics N/A N/A N/A N/A NSE 42,000
Aromatic Fraction Classes (ug/L)
C9-C10 Volatile Aromatics N/A N/A N/A N/A NSE NSE
C11-C22 Extractable Aromatics N/A N/A N/A N/A NSE NSE
C9-C22 Aromatics (total)N/A N/A N/A N/A NSE 210
N/A = Not Analyzed
BDL = Below Detection Limits
NSE = No Standard Established
TABLE 4 (Continued)
SUMMARY OF GROUNDWATER ANALYTICAL RESULTS
BP SERVICE CENTER
4673 US HWY 117 NORTH, GOLDSBORO, NC
Constituent IW-3 SW-8 GCL 2L Standard

Date 9/24/20 9/24/20
Method 6210D (ug/L)
Benzene BDL BDL 5,000 1
Toluene BDL BDL 260,000 600
Ethylbenzene BDL BDL 84,500 600
Xylenes (total) BDL BDL 85,500 500
BTEX (total) 0 0 NSE NSE
p-Isopropyltoluene BDL BDL NSE NSE
Isopropylbenzene BDL BDL 25,000 70
Acetone BDL BDL 6,000,000 6,000
Naphthalene BDL BDL 6,000 6
n-propylbenzene BDL BDL 30,000 70
n-butylbenzene BDL BDL 6,900 70
sec-Butylbenzene BDL BDL 15,000 70
tert-Butylbenzene BDL BDL 15,000 70
MTBE BDL BDL 20,000 20
1,2-Dichloropropane BDL BDL 600 0.6
Isopropyl Ether (IPE) BDL BDL 70,000 70
1,2-Dichloroethane BDL BDL 400 0.4
1,2,4-Trimethylbenzene BDL BDL 28,500 400
1,3,5-Trimethylbenzene BDL BDL 25,000 400
Total 6200B 0 0 NSE NSE
Aliphatic Fraction Classes (ug/L)
C5-C8 Volatile Aliphatics N/A N/A NSE 420
C9-C12 Volatile Aliphatics N/A N/A NSE NSE
C9-C18 Extractable Aliphatics N/A N/A NSE 4,200
C9-C18 Aliphatics (total) N/A N/A NSE 4,200
C19-C36 Extractable Aliphatics N/A N/A NSE 42,000
Aromatic Fraction Classes (ug/L)
C9-C10 Volatile Aromatics N/A N/A NSE NSE
C11-C22 Extractable Aromatics N/A N/A NSE NSE
C9-C22 Aromatics (total)N/A N/A NSE 210
N/A = Not Analyzed
BDL = Below Detection Limits
NSE = No Standard Established
TABLE 4 (Continued)
SUMMARY OF GROUNDWATER ANALYTICAL RESULTS
BP SERVICE CENTER
4673 US HWY 117 NORTH, GOLDSBORO, NC
TABLE 5SUPPLY WELL INFORMATION1,500' RADIUSB.P. Service Center4673 US 117 N., Pikevile, NCUST Incident No. 0‐0069891Well Identification SW‐1IW‐2IW‐3IW‐4IW‐7PIN Number 3603247015 3603246379 3603237868 3603239839 3603248382PIN Address Pearl & Railroad St.Pearl St. (Rear)(PO Box 71)129 Pearl St. (Rear) 4667 N. US 117 HY 4691 US 117N Pikeville, NC 27863 Pikeville, NC 27863 Pikeville, NC 27863 Pikeville, NC 27863 Pikeville, NC 27863Owner Name Pearl St Prop. of Pikevil Francis E. SuggsMattie Artis & C. B. HortonTedaro Reid Andrea CostonOwner Address 457 Washington St 150 Vance St. 129 Pearl St. (Rear) PO Box 506 4691 US 117NPikeville, NC 27863 Goldsboro, NC 27534 Pikeville, NC 27863 Pikeville, NC 27863 Pikeville, NC 27863OccupantUnoccupied Vacant Mattie Artis Tedaro Reid Apple Dumpling Day CareTelephone # 919.733.7862 xt 241 919.734.7220 919.736.1622 919.736.7887 919.242.5555Use Potable ‐Bathroom Not in use Washing Cars Not in use Not in UseDistance 165' 340' 215' 135' 360'City/County Water? NO Unknown Yes Yes YesDepth of Well Unknown 30' Unknown Unknown UnknownWell Diameter Unknown Unknown Unknown Unknown UnknownWell Yield Unknown Unknown Unknown Unknown UnknownDepth to Pump Unknown Unknown Unknown Unknown UnknownDepth of Casing Unknown Unknown Unknown Unknown UnknownStatic Water Unknown Unknown Unknown Unknown UnknownBPS Well
TABLE 5SUPPLY WELL INFORMATION1,500' RADIUSB.P. Service Center4673 US 117 N., Pikevile, NCUST Incident No. 0‐0069892Well Identification SW‐8SW‐4IW‐6IW‐ 9IW‐10PIN Number 3603249413 36032382833603257054 3603258053 3603259063PIN Address 4697 US 117 N 4611 US 117N125 Booker St. 102 Booker St. NW 107 Booker St.Pikeville, NC 27863 Pikeville, NC 27863Pikeville, NC 27863 Pikeville, NC 27863 Pikeville, NC 27863Owner Name David E. Daw Sr. Morris ReedWillie Walker Leon & Kay N. Cox Joseph T. & C.F. CoreOwner Address 139 Zekes Lane PO Box 25531125 Booker St. 102 Booker St. PO Box 452Goldsboro, NC  27534 Raleigh, NC  27611Pikeville, NC 27863 Pikeville, NC 27863 Pikeville, NC 27863Occupant JuDee's Hair & Body Morris ReedDora B. Williams Kaye Cox Joseph Thurman CoreTelephone # 919.242.5652 (919) 215‐5057 (919) 242‐5697 (919) 766‐3050 (919) 242‐4466Use Potable PotableNot in Use Not in Use Not in UseDistance 380' 810'990' 980' 980'City Water? YesNO Yes Yes YesDepth of Well Unknown UnknownUnknown Unknown UnknownWell Diameter Unknown UnknownUnknown Unknown UnknownWell Yield Unknown UnknownUnknown Unknown UnknownDepth to Pump Unknown UnknownUnknown Unknown UnknownDepth of Casing Unknown UnknownUnknown Unknown UnknownStatic Water Unknown UnknownUnknown Unknown UnknownBPS Well
Estimated Area  (Ft2) Est. Thickness  (ft) Avg Cont. Level (ppm) Est. Cont. Mass (lbs) EstimatedDate Zone Soil in Soil in Soil in Soil in Soil in Soil in Soil in Soil in Total Massof Isonconcen. Source Smear Source Smear Source Smear Source Smear Measurement Designation Area Zone GH2O Area Zone GH2O Area Zone GH2O Area Zone GH2O in Lbs2013 Cal. Year UST source 450 550 7500 5 5 15 150 400 10 37.5 122.2 17.545 177.26752013 Cal. Year Downgrad. Area 0 0 30000 0 0 15 0 0 1 0 0 7.0181 7.01811Date Totals 37.5 122.2 24.563 184.285619/24/2020 UST source 450 550 800 5 5 15 150 400 5 37.5 122.2 0.9357 160.657979/24/2020 Downgrad. Area 0 0 9800 0 0 15 0 0 1 0 0 2.2926 2.2925826Date Totals 37.5 122.2 3.2283 162.95055% Mass Reduction 0 0.8686 0.1157717Estimated Soil Porosity = 0.25Estimated Soil Density = 1.5 tons/cubic yardTABLE 6 - MASS CALCULATION TABLEBP Service Center, 4673 US Hwy 117 North, Pikeville, NC  27863Estimated Soil Density  1.5 tons/cubic yardSoil CalculationsArea x Thickness x Density/27 x 2000lbs/ton x contaminated fraction (ppm) Groundwater Calculations 6200B compounds assumed to represent 10% of total dissolved organic compoundsArea x Thickness x porosity x 7.48 gallons/cu.ft. x 8.34 lbs/gallon x contaminated fraction (ppm)
Benzene Toluene Ethyl- Xylenes Isopropyl Isopropyl Napht n-propyl 1,2-Dich MTBE 1,2,4-tri- 1,3,5-tri- Total
Well Date Benzene benzene ether halene benzene loroeth methylbenz methylbenz 6200B
# Sampled (ug/l) (ug/l) (ug/l) (ug/l) (ug/l) (ug/l) (ug/l) (ug/l) (ug/l) (ug/l) (ug/l) (ug/l) (ug/l)
NC 2L Standard 1 600 600 500 70 70 6 70 0.4 20 400 400 NSE
NC GCL Standard 5000 260,000 84,500 85,500 25,000 70,000 6,000 30,000 400 20,000 28,500 25,000 NSE
MW-1 7/8/2008 760 16 710 670 65 BDL 200 160 27 12 740 220 3,580
3/31/2010 690 1 320 84 39 3 100 76 BDL 9 110 9 1,442
8/6/2010 760 19 930 970 69 3 250 200 21 34 980 330 4,566
10/6/2011 110 BDL 12 16 7 BDL 22 38 8.9 29 25 BDL 268
4/18/2013 90 1898014 1 33 31 3.7 48 110 40 541
10/29/2013 106 BDL 124 143 14 BDL 57 32 3.3 51 152 36 718
7/30/2014 100 2 77 26 9 BDL 28 18 11.8 29 41 15 357
5/15/2015 142 BDL 14 BDL 9 1 21 10 9 18 1 BDL 225
8/17/2016 62.3 BDL 18 4 6 2 17 9 3.2 138 5 1 264
3/9/2017 54.7 BDL 30 13 7 2 22 11 3 215 19 2 378
11/2/2017 22 BDL 11 BDL 4 3 12 6 2.5 280 1 BDL 342
5/19/2018 41.8 BDL 15 4 5 1 14 6 1.4 149 6 2 246
9/24/2020 13.1 BDL 6 1 2 1 9 3 0.84 110 3 BDL 148
MW-2 7/8/2008 14 BDL 3 2 43 BDL 44 20 3.3 22 6 BDL 158
3/31/2010 11 BDL 3 BDL 2 BDL BDL BDL 3.2 24 2 BDL 45
8/6/2010 210 4 97 34 13 BDL 48 23 570 34 5 543
10/6/2011 100 1 74 6 22 1 43 38 3.2 60 62 1 410
4/18/2013 21 BDL 12 5 6 1 10 9 3.6 42 7 BDL 117
10/29/2013 23.4 BDL BDL 3 6 BDL 17 10 1.7 42 5 1 109
7/30/2014 145 BDL 149 8 39 1 113 100 1.1 34 47 BDL 636
5/15/2015 6.3 BDL 1 BDL 3 BDL 5 2 3.1 27 1 BDL 47
8/17/2016 48.9 BDL 45 1 21 BDL 45 32 2.1 27 9 BDL 230
3/9/2017 26.1 7 19 1 12 BDL 27 16 2.3 21 1 BDL 131
11/2/2017 29 9 9 7 5 BDL 17 6 1.6 32 BDL BDL 116
5/19/2018 34.5 4 29 BDL 12 BDL 32 20 2.7 26 1 BDL 161
9/24/2020 0.97 BDL BDL BDL 1 BDL BDL BDL 0.9 7 BDL BDL 9
MW-3 7/8/2008 100 BDL 49 157 43 1 77 83 12 13 16 13 564
3/31/2010 47 13 2 BDL 11 BDL 48 15 14 10 4 2 165
8/6/2010 37 BDL 23 2 30 BDL 67 64 9.8 10 1 2 245
10/6/2011 15 BDL 14 BDL 20 BDL 27 48 3.9 3 BDL BDL 131
4/18/2013 13 BDL 14 4 12 BDL 20 15 5.9 4 13 3 105
10/29/2013 3.6 BDL 3 BDL 5 BDL 8 6 2.8 2 BDL BDL 31
7/30/2014 4.9 BDL 8 BDL 13 BDL 13 21 1.3 1 BDL BDL 62
5/15/2015 10.5 BDL 8 BDL 5 BDL 11 8 4.1 3 2 BDL 51
8/17/2016 10.1 BDL 11 BDL 23 BDL 23 BDL 4 32 1 76
3/9/2017 2.8 BDL 2 BDL 5 BDL 4 BDL 4.4 BDL BDL BDL 18
11/2/2017 4 7 5 1 10 BDL 11 6 4.4 3 BDL BDL 51
5/19/2018 5.5 2 4 BDL 8 BDL 9 3 4 3 1 BDL 38
9/24/2020 4.7 1 4 BDL 12 BDL 10 3 4.1 2 BDL BDL 40
MW-4 7/8/2008 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
3/31/2010 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
8/6/2010 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
10/6/2011 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
4/18/2013 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
10/29/2013 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
7/30/2014 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
5/15/2015 190 32116 5 1 71 8 BDL 178 11 3 506
8/17/2016 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
9/24/2020 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
0
MW-5 7/8/2008 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
3/31/2010 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
8/6/2010 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
10/6/2011 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
4/18/2013 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
10/29/2013 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
7/30/2014 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
5/15/2015 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
0
MW-6 7/8/2008 BDL BDL BDL BDL BDL 1 BDL BDL 2.1 29 BDL BDL 32
3/31/2010 BDL BDL BDL BDL BDL BDL BDL BDL BDL 22 BDL BDL 22
8/6/2010 BDL BDL BDL BDL BDL 1 BDL BDL 1.8 49 BDL BDL 52
10/6/2011 BDL BDL BDL BDL BDL BDL BDL BDL 1.2 30 BDL BDL 31
4/18/2013 BDL BDL BDL BDL BDL BDL BDL BDL 0.76 25 BDL BDL 26
TABLE 7: SUMMARY OF GROUNDWATER ANALYTICAL RESULTS
BP Service Center, 4673 US Hwy 117 North, Pikeville, NC 27863
10/29/2013 BDL BDL BDL BDL BDL BDL BDL BDL 0.86 26 BDL BDL 26
7/30/2014 BDL BDL BDL BDL BDL BDL BDL BDL BDL 25 BDL BDL 25
5/15/2015 BDL BDL BDL BDL BDL BDL BDL BDL BDL 27 BDL BDL 27
0
MW-7 7/8/2008 270 180 1,000 3,130 210 8 170 470 BDL 230 2,500 580 8,748
3/31/2010 370 120 1,700 3,880 180 BDL 270 430 BDL 200 2,000 510 9,660
8/6/2010 320 95 1,300 3,100 160 BDL 290 400 BDL 140 1,800 500 8,105
10/6/2011 270 48 140 2,000 130 BDL 260 190 BDL 78 1,500 410 5,026
4/18/2013 200 22 1,200 1,900 140 BDL 220 300 BDL 41 2,100 540 6,663
10/29/2013 85.1 10 335 BDL 40 BDL 159 79 BDL 18 1,050 334 2,110
7/30/2014 120 8 639 831 114 BDL 185 276 BDL 22 1,120 351 3,666
5/15/2015 159 4 327 376 91 6 88 122 4 367 480 160 2,184
8/17/2016 135 4 405 598 95 3 149 206 3.2 20 986 296 2,899
3/9/2017 88.8 3 79 321 19 BDL 75 25 2.6 23 402 145 1,183
11/2/2017 110 BDL 400 550 60 BDL 130 110 BDL BDL 620 190 2,170
5/19/2018 23 2 143 172 29 BDL 51 68 BDL 6 220 49 764
9/24/2020 18.8 BDL 163 195 26 BDL 46 BDL BDL BDL 348 92 889
MW-8 9/14/2009 5400 9,900 4,000 18,500 150 BDL 620 400 130 5,800 4,300 1,100 50,300
3/31/2010 7200 12,000 3,200 13,900 97 BDL 480 310 BDL 9,200 2,700 710 49,797
8/6/2010 9100 12,000 5,400 21,000 97 BDL 1,000 670 140 8,300 6,000 1,600 65,307
10/6/2011 7100 9,400 3,400 14,000 BDL BDL 920 340 65 7,700 3,400 860 47,185
8A 4/18/2013 BDL BDL BDL BDL BDL 1 BDL BDL 4.5 230 BDL BDL 235
10/29/2013 BDL BDL BDL BDL BDL BDL BDL BDL 0.66 17 BDL BDL 18
7/30/2014 BDL BDL BDL BDL BDL BDL BDL BDL 0.91 27 BDL BDL 28
5/15/2015 BDL BDL BDL BDL 1 BDL BDL BDL 4.1 107 BDL BDL 112
8/17/2016 BDL BDL BDL BDL BDL BDL BDL BDL BDL 9 BDL BDL 9
9/24/2020 BDL BDL BDL BDL BDL BDL BDL BDL 0.6 13 BDL BDL 14
MW-9 9/14/2009 9.1 BDL BDL BDL 2 2 BDL BDL 11 BDL BDL BDL 24
3/31/2010 3.7 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 4
8/6/2010 6.3 BDL BDL BDL BDL BDL 3 BDL 0.66 BDL BDL BDL 10
10/6/2011 5.4 BDL BDL BDL BDL BDL BDL BDL 0.94 BDL BDL BDL 6
4/18/2013 0.58 BDL BDL BDL BDL 1 BDL BDL 3.9 BDL BDL BDL 6
10/29/2013 0.64 BDL BDL BDL BDL BDL BDL BDL 18.7 1 BDL BDL 20
7/30/2014 2.6 BDL BDL BDL 4 10 BDL BDL 39.6 BDL BDL BDL 56
5/15/2015 1.8 BDL BDL BDL BDL BDL BDL BDL 14.6 1 BDL BDL 17
8/17/2016 1.9 BDL BDL BDL 5 BDL BDL BDL 17.5 1 BDL BDL 25
3/9/2017 BDL BDL BDL BDL 1 BDL BDL BDL 7.4 BDL BDL BDL 8
11/2/2017 3 2 BDL BDL BDL 1 BDL BDL 2.2 1 BDL BDL 8
5/19/2018 1.8 BDL BDL BDL BDL BDL BDL BDL 1 BDL BDL BDL 3
9/24/2020 BDL BDL BDL BDL BDL BDL BDL BDL 0.82 BDL BDL BDL 1
MW-10 9/14/2009 BDL 1 BDL 1 BDL BDL BDL BDL BDL BDL BDL BDL 2
3/31/2010 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
8/6/2010 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
10/6/2011 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
4/18/2013 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
10/29/2013 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
7/30/2014 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
5/15/2015 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
8/17/2016 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
0
MW-11 9/14/2009 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
3/31/2010 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
8/6/2010 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
10/6/2011 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
4/18/2013 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
10/29/2013 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
7/30/2014 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
5/15/2015 780 5221458 8 290 125 BDL 1,770 2 5 3,078
8/17/2016 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
0
MW-12 9/14/2009 180 2 27 1 5 BDL 6 6 19 BDL BDL BDL 245
3/31/2010 1.6 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 2
8/6/2010 8.6 BDL BDL BDL BDL 2 BDL BDL BDL 3 BDL BDL 13
10/6/2011 2.3 BDL BDL BDL BDL BDL BDL BDL 4.2 2 BDL BDL 8
4/18/2013 BDL BDL BDL BDL BDL BDL BDL BDL 0.69 2 BDL BDL 3
10/29/2013 8.4 BDL BDL 1 3 BDL BDL BDL 9.9 8 BDL BDL 30
7/30/2014 0.84 BDL BDL BDL BDL BDL BDL BDL 2.5 1 BDL BDL 4
5/15/2015 0.82 BDL BDL BDL BDL BDL BDL BDL 1.8 BDL BDL BDL 3
11/2/2017 0.59 BDL BDL BDL 1 1 BDL BDL 1.6 10 BDL BDL 14
5/19/2018 BDL BDL BDL BDL BDL BDL BDL BDL BDL 4 BDL BDL 4
9/24/2020 BDL BDL BDL BDL BDL BDL BDL BDL BDL 1 BDL BDL 1
MW-13 12/17/2009 2.9 24 1 1 BDL BDL 10 BDL BDL BDL 1 BDL 40
3/31/2010 BDL 51 BDL BDL BDL BDL BDL BDL BDL BDL 1 BDL 52
8/6/2010 BDL 76 BDL BDL BDL BDL BDL BDL BDL BDL 1 BDL 77
10/6/2011 3.1 6 BDL BDL BDL BDL 7 BDL BDL BDL BDL BDL 16
4/18/2013 BDL 2 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 2
10/29/2013 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
7/30/2014 BDL 9 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 9
5/15/2015 BDL 11 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 11
9/24/2020 BDL BDL BDL BDL BDL BDL BDL BDL 1.3 BDL BDL BDL 1
MW-14 12/17/2009 11 2 5 3 1 BDL 160 3 BDL BDL 22 BDL 207
3/31/2010 3.2 BDL 27 BDL BDL BDL 410 15 BDL BDL 85 5 546
8/6/2010 3.1 BDL 16 2 5 BDL 360 7 BDL BDL 55 1 448
10/6/2011 1.5 BDL 6 1 3 BDL 190 4 BDL BDL 590 98 892
4/18/2013 1 BDL 3 BDL 2 BDL 88 BDL BDL BDL 10 1 104
10/29/2013 2.1 BDL 8 BDL BDL BDL 196 5 BDL BDL 27 BDL 237
7/30/2014 0.58 BDL 2 BDL 1 BDL 44 2 BDL BDL 5 BDL 55
5/15/2015 0.64 BDL 3 BDL 2 BDL 50 1 BDL BDL 9 BDL 65
3/9/2017 BDL 2 1 BDL 1 BDL 4 1 BDL BDL BDL BDL 8
11/2/2017 BDL BDL 3 BDL 2 BDL 11 3 BDL BDL 6 BDL 26
5/19/2018 BDL BDL 1 BDL 1 BDL 11 1 BDL BDL 1 BDL 14
9/24/2020 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
MW-15 8/6/2010 5.6 3 260 160 28 BDL 160 76 BDL BDL 90 41 824
10/6/2011 0.68 2 380 470 44 BDL 320 120 BDL BDL BDL BDL 1,337
4/18/2013 BDL BDL 37 12 9 BDL 53 17 BDL BDL 49 9 186
10/29/2013 BDL BDL 300 420 35 BDL 307 85 BDL BDL BDL BDL 1,147
7/30/2014 BDL BDL 11 25 4 BDL 35 6 BDL BDL 27 5 113
5/15/2015 BDL BDL 9 BDL 2 BDL 14 4 BDL BDL 2 BDL 31
3/9/2017 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
9/24/2020 BDL BDL 1 BDL BDL BDL BDL 1 BDL BDL 1 BDL 2
MW-16 8/6/2010 4.7 2 4 7 1 BDL 26 1 BDL BDL 3 1 50
10/6/2011 3.1 BDL 13 1 3 BDL 220 27 BDL BDL 20 BDL 287
4/18/2013 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
10/29/2013 0.6 BDL 1 BDL 2 BDL 43 2 BDL BDL 2 BDL 50
7/30/2014 0.89 BDL 6 1 10 BDL 139 13 BDL BDL 5 1 176
5/15/2015 0.95 BDL 1 BDL 4 BDL 79 4 BDL BDL 4 BDL 93
3/9/2017 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
11/2/2017 BDL BDL BDL BDL BDL BDL 31 2 BDL BDL BDL BDL 33
5/19/2018 BDL BDL BDL BDL BDL BDL 3 BDL BDL BDL BDL BDL 3
9/24/2020 BDL BDL BDL BDL 1 BDL 8 1 BDL BDL BDL BDL 9
MW-17 8/6/2010 3.4 1 3 4 BDL BDL 28 1 BDL BDL 2 BDL 42
10/6/2011 2.4 BDL BDL BDL BDL BDL 32 BDL BDL BDL BDL BDL 34
4/18/2013 0.75 BDL BDL BDL BDL BDL 19 BDL BDL BDL BDL BDL 20
10/29/2013 0.94 BDL BDL BDL BDL BDL 16 BDL BDL BDL BDL BDL 17
7/30/2014 2.3 BDL BDL BDL BDL BDL 68 BDL BDL BDL BDL BDL 70
5/15/2015 0.9 BDL BDL BDL BDL BDL 40 BDL BDL BDL BDL BDL 40
3/9/2017 BDL BDL BDL BDL BDL BDL 23 BDL BDL BDL BDL BDL 23
11/2/2017 BDL BDL BDL BDL BDL BDL 1 BDL BDL BDL BDL BDL 1
5/19/2018 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
9/24/2020 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
MW-18 4/18/2013 470 5 240 50 30 BDL 100 74 14 460 92 26 1,561
10/29/2013 187 BDL 100 6 13 BDL 65 34 5.9 294 BDL BDL 705
7/30/2014 55.7 1 3 BDL BDL BDL 16 8 0.58 161 4 BDL 248
5/15/2015 24.7 BDL 10 BDL 3 BDL 540.86 130 BDL BDL 177
8/17/2016 144 BDL 105 BDL 21 BDL 63 46 6.8 360 2 BDL 748
3/9/2017 88.3 BDL 62 6 11 BDL 45 20 5.2 385 12 2 637
11/2/2017 59 1393 7 1 47 13 7.1 420 7 1 605
5/19/2018 95 1656 12BDL 40 27 5.2 236 15 9 511
9/24/2020 3.9 BDL 7 BDL 2 BDL 550.98 82 1 BDL 106
VEW-1 12/17/2009 3.7 BDL 1 BDL BDL BDL BDL BDL BDL BDL BDL BDL 5
3/31/2010 2.4 6 2 6 BDL BDL BDL BDL BDL BDL 2 2 19
8/6/2010 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
10/6/2011 BDL BDL BDL BDL BDL BDL 1 BDL BDL BDL BDL BDL 1
4/18/2013 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
10/29/2013 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
7/30/2014 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
5/15/2015 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
9/24/2020 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0
BDL = Below Detection Limits
NSE = No Standard Established
N/A = Not Applicable

APPENDIX A

LABORATORY ANALYTICAL RESULTS
#=CL#
October 02, 2020
LIMS USE: FR - HENRY NEMARGUT
LIMS OBJECT ID: 92497598
92497598
Project:
Pace Project No.:
RE:
Henry Nemargut
Henry Nemargut Engineering
2211 Chestnut Street
Wilmington, NC 28405
BP Service Center
Dear Henry Nemargut:
Enclosed are the analytical results for sample(s) received by the laboratory on September 25, 2020. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Bonnie Vang
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 58
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92497598
BP Service Center
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 58
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92497598
BP Service Center
Lab ID Sample ID Matrix Date Collected Date Received
92497598001 MW-1 Water 09/24/20 08:00 09/25/20 08:00
92497598002 MW-2 Water 09/24/20 08:20 09/25/20 08:00
92497598003 MW-3 Water 09/24/20 08:40 09/25/20 08:00
92497598004 MW-4 Water 09/24/20 09:05 09/25/20 08:00
92497598005 MW-7 Water 09/24/20 09:30 09/25/20 08:00
92497598006 MW-8A Water 09/24/20 10:00 09/25/20 08:00
92497598007 MW-9 Water 09/24/20 10:25 09/25/20 08:00
92497598008 MW-12 Water 09/24/20 10:50 09/25/20 08:00
92497598009 MW-13 Water 09/24/20 11:20 09/25/20 08:00
92497598010 MW-14 Water 09/24/20 12:00 09/25/20 08:00
92497598011 MW-15 Water 09/24/20 12:30 09/25/20 08:00
92497598012 MW-16 Water 09/24/20 12:50 09/25/20 08:00
92497598013 MW-17 Water 09/24/20 13:15 09/25/20 08:00
92497598014 MW-18 Water 09/24/20 13:45 09/25/20 08:00
92497598015 VEW-1 Water 09/24/20 14:45 09/25/20 08:00
92497598016 SW-1 Water 09/24/20 15:00 09/25/20 08:00
92497598017 IW-3 Water 09/24/20 15:15 09/25/20 08:00
92497598018 SW-8 Water 09/24/20 15:35 09/25/20 08:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 58
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92497598
BP Service Center
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92497598001 MW-1 SM 6200B 63 PASI-CCL
92497598002 MW-2 SM 6200B 63 PASI-CSAS
92497598003 MW-3 SM 6200B 63 PASI-CCL
92497598004 MW-4 SM 6200B 63 PASI-CCL
92497598005 MW-7 SM 6200B 63 PASI-CSAS
92497598006 MW-8A SM 6200B 63 PASI-CCL
92497598007 MW-9 SM 6200B 63 PASI-CCL
92497598008 MW-12 SM 6200B 63 PASI-CCL
92497598009 MW-13 SM 6200B 63 PASI-CCL
92497598010 MW-14 SM 6200B 63 PASI-CSAS
92497598011 MW-15 SM 6200B 63 PASI-CSAS
92497598012 MW-16 SM 6200B 63 PASI-CCL
92497598013 MW-17 SM 6200B 63 PASI-CCL
92497598014 MW-18 SM 6200B 63 PASI-CSAS
92497598015 VEW-1 SM 6200B 63 PASI-CCL
92497598016 SW-1 SM 6200B 63 PASI-CCL
92497598017 IW-3 SM 6200B 63 PASI-CCL
92497598018 SW-8 SM 6200B 63 PASI-CCL
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 58
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92497598
BP Service Center
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92497598001 MW-1
Benzene 13.1 ug/L 09/29/20 22:470.50SM 6200B
1,2-Dichloroethane 0.84 ug/L 09/29/20 22:470.50SM 6200B
Diisopropyl ether 0.99 ug/L 09/29/20 22:470.50SM 6200B
Ethylbenzene 6.0 ug/L 09/29/20 22:470.50SM 6200B
Isopropylbenzene (Cumene)2.2 ug/L 09/29/20 22:470.50SM 6200B
Methyl-tert-butyl ether 110 ug/L 09/29/20 22:470.50SM 6200B
Naphthalene 8.7 ug/L 09/29/20 22:472.0SM 6200B
n-Propylbenzene 2.7 ug/L 09/29/20 22:470.50SM 6200B
1,2,4-Trimethylbenzene 2.5 ug/L 09/29/20 22:470.50SM 6200B
o-Xylene 0.56 ug/L 09/29/20 22:470.50SM 6200B
92497598002 MW-2
Benzene 0.97 ug/L 10/01/20 00:100.50SM 6200B
1,2-Dichloroethane 0.90 ug/L 10/01/20 00:100.50SM 6200B
Isopropylbenzene (Cumene)0.52 ug/L 10/01/20 00:100.50SM 6200B
Methyl-tert-butyl ether 6.7 ug/L 10/01/20 00:100.50SM 6200B
92497598003 MW-3
Benzene 4.7 ug/L 09/29/20 21:150.50SM 6200B
sec-Butylbenzene 3.6 ug/L 09/29/20 21:150.50SM 6200B
1,2-Dichloroethane 4.1 ug/L 09/29/20 21:150.50SM 6200B
Ethylbenzene 3.9 ug/L 09/29/20 21:150.50SM 6200B
Isopropylbenzene (Cumene)11.6 ug/L 09/29/20 21:150.50SM 6200B
Methyl-tert-butyl ether 2.1 ug/L 09/29/20 21:150.50SM 6200B
Naphthalene 9.7 ug/L 09/29/20 21:152.0SM 6200B
n-Propylbenzene 3.1 ug/L 09/29/20 21:150.50SM 6200B
Toluene 0.97 ug/L 09/29/20 21:150.50SM 6200B
92497598005 MW-7
Benzene 18.8 ug/L 10/01/20 01:552.0SM 6200B
Ethylbenzene 163 ug/L 10/01/20 01:552.0SM 6200B
Isopropylbenzene (Cumene)26.2 ug/L 10/01/20 01:552.0SM 6200B
Naphthalene 45.6 ug/L 10/01/20 01:558.0SM 6200B
1,2,4-Trimethylbenzene 348 ug/L 10/01/20 01:552.0SM 6200B
1,3,5-Trimethylbenzene 91.9 ug/L 10/01/20 01:552.0SM 6200B
m&p-Xylene 151 ug/L 10/01/20 01:554.0SM 6200B
o-Xylene 44.2 ug/L 10/01/20 01:552.0SM 6200B
92497598006 MW-8A
1,2-Dichloroethane 0.60 ug/L 09/29/20 19:070.50SM 6200B
Methyl-tert-butyl ether 12.9 ug/L 09/29/20 19:070.50SM 6200B
92497598007 MW-9
1,2-Dichloroethane 0.82 ug/L 09/29/20 19:260.50SM 6200B
92497598008 MW-12
Methyl-tert-butyl ether 1.3 ug/L 09/29/20 17:540.50SM 6200B
92497598011 MW-15
Ethylbenzene 0.78 ug/L 10/01/20 00:450.50SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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Page 5 of 58
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92497598
BP Service Center
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92497598011 MW-15
n-Propylbenzene 0.60 ug/L 10/01/20 00:450.50SM 6200B
1,2,4-Trimethylbenzene 1.1 ug/L 10/01/20 00:450.50SM 6200B
92497598012 MW-16
Isopropylbenzene (Cumene)0.76 ug/L 09/29/20 20:570.50SM 6200B
Naphthalene 7.7 ug/L 09/29/20 20:572.0SM 6200B
n-Propylbenzene 1.0 ug/L 09/29/20 20:570.50SM 6200B
92497598014 MW-18
Benzene 3.9 ug/L 10/01/20 01:020.50SM 6200B
sec-Butylbenzene 1.9 ug/L 10/01/20 01:020.50SM 6200B
tert-Butylbenzene 0.74 ug/L 10/01/20 01:020.50SM 6200B
1,2-Dichloroethane 0.98 ug/L 10/01/20 01:020.50SM 6200B
Ethylbenzene 6.8 ug/L 10/01/20 01:020.50SM 6200B
Isopropylbenzene (Cumene)2.2 ug/L 10/01/20 01:020.50SM 6200B
Methyl-tert-butyl ether 81.8 ug/L 10/01/20 01:020.50SM 6200B
Naphthalene 4.8 ug/L 10/01/20 01:022.0SM 6200B
n-Propylbenzene 5.2 ug/L 10/01/20 01:020.50SM 6200B
1,2,4-Trimethylbenzene 0.64 ug/L 10/01/20 01:020.50SM 6200B
92497598016 SW-1
1,2-Dichloropropane 2.0 ug/L 09/29/20 20:390.50SM 6200B
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 6 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92497598
BP Service Center
Sample:MW-1 Lab ID:92497598001 Collected:09/24/20 08:00 Received:09/25/20 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 13.1 ug/L 09/29/20 22:47 71-43-20.50 1
Bromobenzene ND ug/L 09/29/20 22:47 108-86-10.50 1
Bromochloromethane ND ug/L 09/29/20 22:47 74-97-50.50 1
Bromodichloromethane ND ug/L 09/29/20 22:47 75-27-40.50 1
Bromoform ND ug/L 09/29/20 22:47 75-25-20.50 1
Bromomethane ND ug/L 09/29/20 22:47 74-83-95.0 1
n-Butylbenzene ND ug/L 09/29/20 22:47 104-51-80.50 1
sec-Butylbenzene ND ug/L 09/29/20 22:47 135-98-80.50 1
tert-Butylbenzene ND ug/L 09/29/20 22:47 98-06-60.50 1
Carbon tetrachloride ND ug/L 09/29/20 22:47 56-23-50.50 1
Chlorobenzene ND ug/L 09/29/20 22:47 108-90-70.50 1
Chloroethane ND ug/L 09/29/20 22:47 75-00-31.0 1
Chloroform ND ug/L 09/29/20 22:47 67-66-30.50 1
Chloromethane ND ug/L 09/29/20 22:47 74-87-31.0 1
2-Chlorotoluene ND ug/L 09/29/20 22:47 95-49-80.50 1
4-Chlorotoluene ND ug/L 09/29/20 22:47 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 09/29/20 22:47 96-12-81.0 1
Dibromochloromethane ND ug/L 09/29/20 22:47 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 09/29/20 22:47 106-93-40.50 1
Dibromomethane ND ug/L 09/29/20 22:47 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 09/29/20 22:47 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 09/29/20 22:47 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 09/29/20 22:47 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 09/29/20 22:47 75-71-80.50 1
1,1-Dichloroethane ND ug/L 09/29/20 22:47 75-34-30.50 1
1,2-Dichloroethane 0.84 ug/L 09/29/20 22:47 107-06-20.50 1
1,1-Dichloroethene ND ug/L 09/29/20 22:47 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 09/29/20 22:47 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 09/29/20 22:47 156-60-50.50 1
1,2-Dichloropropane ND ug/L 09/29/20 22:47 78-87-50.50 1
1,3-Dichloropropane ND ug/L 09/29/20 22:47 142-28-90.50 1
2,2-Dichloropropane ND ug/L 09/29/20 22:47 594-20-70.50 1
1,1-Dichloropropene ND ug/L 09/29/20 22:47 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 09/29/20 22:47 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 09/29/20 22:47 10061-02-60.50 1
Diisopropyl ether 0.99 ug/L 09/29/20 22:47 108-20-30.50 1
Ethylbenzene 6.0 ug/L 09/29/20 22:47 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 09/29/20 22:47 87-68-32.0 1
Isopropylbenzene (Cumene)2.2 ug/L 09/29/20 22:47 98-82-80.50 1
Methylene Chloride ND ug/L 09/29/20 22:47 75-09-22.0 1
Methyl-tert-butyl ether 110 ug/L 09/29/20 22:47 1634-04-40.50 1
Naphthalene 8.7 ug/L 09/29/20 22:47 91-20-32.0 1
n-Propylbenzene 2.7 ug/L 09/29/20 22:47 103-65-10.50 1
Styrene ND ug/L 09/29/20 22:47 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 09/29/20 22:47 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 09/29/20 22:47 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2020 12:21 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
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Page 7 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92497598
BP Service Center
Sample:MW-1 Lab ID:92497598001 Collected:09/24/20 08:00 Received:09/25/20 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 09/29/20 22:47 127-18-40.50 1
Toluene ND ug/L 09/29/20 22:47 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 09/29/20 22:47 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 09/29/20 22:47 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 09/29/20 22:47 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 09/29/20 22:47 79-00-50.50 1
Trichloroethene ND ug/L 09/29/20 22:47 79-01-60.50 1
Trichlorofluoromethane ND ug/L 09/29/20 22:47 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 09/29/20 22:47 96-18-40.50 1
1,2,4-Trimethylbenzene 2.5 ug/L 09/29/20 22:47 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 09/29/20 22:47 108-67-80.50 1
Vinyl chloride ND ug/L 09/29/20 22:47 75-01-41.0 1
m&p-Xylene ND ug/L 09/29/20 22:47 179601-23-11.0 1
o-Xylene 0.56 ug/L 09/29/20 22:47 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)99 %09/29/20 22:47 17060-07-070-130 1
4-Bromofluorobenzene (S)98 %09/29/20 22:47 460-00-470-130 1
Toluene-d8 (S)102 %09/29/20 22:47 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2020 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 8 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92497598
BP Service Center
Sample:MW-2 Lab ID:92497598002 Collected:09/24/20 08:20 Received:09/25/20 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 0.97 ug/L 10/01/20 00:10 71-43-20.50 1
Bromobenzene ND ug/L 10/01/20 00:10 108-86-10.50 1
Bromochloromethane ND ug/L 10/01/20 00:10 74-97-50.50 1
Bromodichloromethane ND ug/L 10/01/20 00:10 75-27-40.50 1
Bromoform ND ug/L 10/01/20 00:10 75-25-20.50 1
Bromomethane ND ug/L 10/01/20 00:10 74-83-95.0 1
n-Butylbenzene ND ug/L 10/01/20 00:10 104-51-80.50 1
sec-Butylbenzene ND ug/L 10/01/20 00:10 135-98-80.50 1
tert-Butylbenzene ND ug/L 10/01/20 00:10 98-06-60.50 1
Carbon tetrachloride ND ug/L 10/01/20 00:10 56-23-50.50 1
Chlorobenzene ND ug/L 10/01/20 00:10 108-90-70.50 1
Chloroethane ND ug/L 10/01/20 00:10 75-00-31.0 1
Chloroform ND ug/L 10/01/20 00:10 67-66-30.50 1
Chloromethane ND ug/L 10/01/20 00:10 74-87-31.0 1
2-Chlorotoluene ND ug/L 10/01/20 00:10 95-49-80.50 1
4-Chlorotoluene ND ug/L 10/01/20 00:10 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 10/01/20 00:10 96-12-81.0 1
Dibromochloromethane ND ug/L 10/01/20 00:10 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 10/01/20 00:10 106-93-40.50 1
Dibromomethane ND ug/L 10/01/20 00:10 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 10/01/20 00:10 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 10/01/20 00:10 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 10/01/20 00:10 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 10/01/20 00:10 75-71-80.50 1
1,1-Dichloroethane ND ug/L 10/01/20 00:10 75-34-30.50 1
1,2-Dichloroethane 0.90 ug/L 10/01/20 00:10 107-06-20.50 1
1,1-Dichloroethene ND ug/L 10/01/20 00:10 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 10/01/20 00:10 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 10/01/20 00:10 156-60-50.50 1
1,2-Dichloropropane ND ug/L 10/01/20 00:10 78-87-50.50 1
1,3-Dichloropropane ND ug/L 10/01/20 00:10 142-28-90.50 1
2,2-Dichloropropane ND ug/L 10/01/20 00:10 594-20-70.50 1
1,1-Dichloropropene ND ug/L 10/01/20 00:10 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 10/01/20 00:10 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 10/01/20 00:10 10061-02-60.50 1
Diisopropyl ether ND ug/L 10/01/20 00:10 108-20-30.50 1
Ethylbenzene ND ug/L 10/01/20 00:10 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 10/01/20 00:10 87-68-32.0 1
Isopropylbenzene (Cumene)0.52 ug/L 10/01/20 00:10 98-82-80.50 1
Methylene Chloride ND ug/L 10/01/20 00:10 75-09-22.0 1
Methyl-tert-butyl ether 6.7 ug/L 10/01/20 00:10 1634-04-40.50 1
Naphthalene ND ug/L 10/01/20 00:10 91-20-32.0 1
n-Propylbenzene ND ug/L 10/01/20 00:10 103-65-10.50 1
Styrene ND ug/L 10/01/20 00:10 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 10/01/20 00:10 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 10/01/20 00:10 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2020 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92497598
BP Service Center
Sample:MW-2 Lab ID:92497598002 Collected:09/24/20 08:20 Received:09/25/20 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 10/01/20 00:10 127-18-40.50 1
Toluene ND ug/L 10/01/20 00:10 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 10/01/20 00:10 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 10/01/20 00:10 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 10/01/20 00:10 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 10/01/20 00:10 79-00-50.50 1
Trichloroethene ND ug/L 10/01/20 00:10 79-01-60.50 1
Trichlorofluoromethane ND ug/L 10/01/20 00:10 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/01/20 00:10 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 10/01/20 00:10 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 10/01/20 00:10 108-67-80.50 1
Vinyl chloride ND ug/L 10/01/20 00:10 75-01-41.0 1
m&p-Xylene ND ug/L 10/01/20 00:10 179601-23-11.0 1
o-Xylene ND ug/L 10/01/20 00:10 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)106 %10/01/20 00:10 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %10/01/20 00:10 460-00-470-130 1
Toluene-d8 (S)103 %10/01/20 00:10 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2020 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92497598
BP Service Center
Sample:MW-3 Lab ID:92497598003 Collected:09/24/20 08:40 Received:09/25/20 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 4.7 ug/L 09/29/20 21:15 71-43-20.50 1
Bromobenzene ND ug/L 09/29/20 21:15 108-86-10.50 1
Bromochloromethane ND ug/L 09/29/20 21:15 74-97-50.50 1
Bromodichloromethane ND ug/L 09/29/20 21:15 75-27-40.50 1
Bromoform ND ug/L 09/29/20 21:15 75-25-20.50 1
Bromomethane ND ug/L 09/29/20 21:15 74-83-95.0 1
n-Butylbenzene ND ug/L 09/29/20 21:15 104-51-80.50 1
sec-Butylbenzene 3.6 ug/L 09/29/20 21:15 135-98-80.50 1
tert-Butylbenzene ND ug/L 09/29/20 21:15 98-06-60.50 1
Carbon tetrachloride ND ug/L 09/29/20 21:15 56-23-50.50 1
Chlorobenzene ND ug/L 09/29/20 21:15 108-90-70.50 1
Chloroethane ND ug/L 09/29/20 21:15 75-00-31.0 1
Chloroform ND ug/L 09/29/20 21:15 67-66-30.50 1
Chloromethane ND ug/L 09/29/20 21:15 74-87-31.0 1
2-Chlorotoluene ND ug/L 09/29/20 21:15 95-49-80.50 1
4-Chlorotoluene ND ug/L 09/29/20 21:15 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 09/29/20 21:15 96-12-81.0 1
Dibromochloromethane ND ug/L 09/29/20 21:15 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 09/29/20 21:15 106-93-40.50 1
Dibromomethane ND ug/L 09/29/20 21:15 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 09/29/20 21:15 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 09/29/20 21:15 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 09/29/20 21:15 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 09/29/20 21:15 75-71-80.50 1
1,1-Dichloroethane ND ug/L 09/29/20 21:15 75-34-30.50 1
1,2-Dichloroethane 4.1 ug/L 09/29/20 21:15 107-06-20.50 1
1,1-Dichloroethene ND ug/L 09/29/20 21:15 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 09/29/20 21:15 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 09/29/20 21:15 156-60-50.50 1
1,2-Dichloropropane ND ug/L 09/29/20 21:15 78-87-50.50 1
1,3-Dichloropropane ND ug/L 09/29/20 21:15 142-28-90.50 1
2,2-Dichloropropane ND ug/L 09/29/20 21:15 594-20-70.50 1
1,1-Dichloropropene ND ug/L 09/29/20 21:15 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 09/29/20 21:15 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 09/29/20 21:15 10061-02-60.50 1
Diisopropyl ether ND ug/L 09/29/20 21:15 108-20-30.50 1
Ethylbenzene 3.9 ug/L 09/29/20 21:15 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 09/29/20 21:15 87-68-32.0 1
Isopropylbenzene (Cumene)11.6 ug/L 09/29/20 21:15 98-82-80.50 1
Methylene Chloride ND ug/L 09/29/20 21:15 75-09-22.0 1
Methyl-tert-butyl ether 2.1 ug/L 09/29/20 21:15 1634-04-40.50 1
Naphthalene 9.7 ug/L 09/29/20 21:15 91-20-32.0 1
n-Propylbenzene 3.1 ug/L 09/29/20 21:15 103-65-10.50 1
Styrene ND ug/L 09/29/20 21:15 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 09/29/20 21:15 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 09/29/20 21:15 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2020 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92497598
BP Service Center
Sample:MW-3 Lab ID:92497598003 Collected:09/24/20 08:40 Received:09/25/20 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 09/29/20 21:15 127-18-40.50 1
Toluene 0.97 ug/L 09/29/20 21:15 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 09/29/20 21:15 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 09/29/20 21:15 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 09/29/20 21:15 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 09/29/20 21:15 79-00-50.50 1
Trichloroethene ND ug/L 09/29/20 21:15 79-01-60.50 1
Trichlorofluoromethane ND ug/L 09/29/20 21:15 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 09/29/20 21:15 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 09/29/20 21:15 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 09/29/20 21:15 108-67-80.50 1
Vinyl chloride ND ug/L 09/29/20 21:15 75-01-41.0 1
m&p-Xylene ND ug/L 09/29/20 21:15 179601-23-11.0 1
o-Xylene ND ug/L 09/29/20 21:15 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)100 %09/29/20 21:15 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %09/29/20 21:15 460-00-470-130 1
Toluene-d8 (S)98 %09/29/20 21:15 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2020 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92497598
BP Service Center
Sample:MW-4 Lab ID:92497598004 Collected:09/24/20 09:05 Received:09/25/20 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 09/29/20 20:20 71-43-20.50 1
Bromobenzene ND ug/L 09/29/20 20:20 108-86-10.50 1
Bromochloromethane ND ug/L 09/29/20 20:20 74-97-50.50 1
Bromodichloromethane ND ug/L 09/29/20 20:20 75-27-40.50 1
Bromoform ND ug/L 09/29/20 20:20 75-25-20.50 1
Bromomethane ND ug/L 09/29/20 20:20 74-83-95.0 1
n-Butylbenzene ND ug/L 09/29/20 20:20 104-51-80.50 1
sec-Butylbenzene ND ug/L 09/29/20 20:20 135-98-80.50 1
tert-Butylbenzene ND ug/L 09/29/20 20:20 98-06-60.50 1
Carbon tetrachloride ND ug/L 09/29/20 20:20 56-23-50.50 1
Chlorobenzene ND ug/L 09/29/20 20:20 108-90-70.50 1
Chloroethane ND ug/L 09/29/20 20:20 75-00-31.0 1
Chloroform ND ug/L 09/29/20 20:20 67-66-30.50 1
Chloromethane ND ug/L 09/29/20 20:20 74-87-31.0 1
2-Chlorotoluene ND ug/L 09/29/20 20:20 95-49-80.50 1
4-Chlorotoluene ND ug/L 09/29/20 20:20 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 09/29/20 20:20 96-12-81.0 1
Dibromochloromethane ND ug/L 09/29/20 20:20 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 09/29/20 20:20 106-93-40.50 1
Dibromomethane ND ug/L 09/29/20 20:20 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 09/29/20 20:20 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 09/29/20 20:20 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 09/29/20 20:20 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 09/29/20 20:20 75-71-80.50 1
1,1-Dichloroethane ND ug/L 09/29/20 20:20 75-34-30.50 1
1,2-Dichloroethane ND ug/L 09/29/20 20:20 107-06-20.50 1
1,1-Dichloroethene ND ug/L 09/29/20 20:20 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 09/29/20 20:20 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 09/29/20 20:20 156-60-50.50 1
1,2-Dichloropropane ND ug/L 09/29/20 20:20 78-87-50.50 1
1,3-Dichloropropane ND ug/L 09/29/20 20:20 142-28-90.50 1
2,2-Dichloropropane ND ug/L 09/29/20 20:20 594-20-70.50 1
1,1-Dichloropropene ND ug/L 09/29/20 20:20 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 09/29/20 20:20 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 09/29/20 20:20 10061-02-60.50 1
Diisopropyl ether ND ug/L 09/29/20 20:20 108-20-30.50 1
Ethylbenzene ND ug/L 09/29/20 20:20 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 09/29/20 20:20 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 09/29/20 20:20 98-82-80.50 1
Methylene Chloride ND ug/L 09/29/20 20:20 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 09/29/20 20:20 1634-04-40.50 1
Naphthalene ND ug/L 09/29/20 20:20 91-20-32.0 1
n-Propylbenzene ND ug/L 09/29/20 20:20 103-65-10.50 1
Styrene ND ug/L 09/29/20 20:20 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 09/29/20 20:20 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 09/29/20 20:20 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2020 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92497598
BP Service Center
Sample:MW-4 Lab ID:92497598004 Collected:09/24/20 09:05 Received:09/25/20 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 09/29/20 20:20 127-18-40.50 1
Toluene ND ug/L 09/29/20 20:20 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 09/29/20 20:20 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 09/29/20 20:20 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 09/29/20 20:20 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 09/29/20 20:20 79-00-50.50 1
Trichloroethene ND ug/L 09/29/20 20:20 79-01-60.50 1
Trichlorofluoromethane ND ug/L 09/29/20 20:20 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 09/29/20 20:20 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 09/29/20 20:20 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 09/29/20 20:20 108-67-80.50 1
Vinyl chloride ND ug/L 09/29/20 20:20 75-01-41.0 1
m&p-Xylene ND ug/L 09/29/20 20:20 179601-23-11.0 1
o-Xylene ND ug/L 09/29/20 20:20 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)99 %09/29/20 20:20 17060-07-070-130 1
4-Bromofluorobenzene (S)98 %09/29/20 20:20 460-00-470-130 1
Toluene-d8 (S)101 %09/29/20 20:20 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2020 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92497598
BP Service Center
Sample:MW-7 Lab ID:92497598005 Collected:09/24/20 09:30 Received:09/25/20 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 18.8 ug/L 10/01/20 01:55 71-43-22.0 4
Bromobenzene ND ug/L 10/01/20 01:55 108-86-12.0 4
Bromochloromethane ND ug/L 10/01/20 01:55 74-97-52.0 4
Bromodichloromethane ND ug/L 10/01/20 01:55 75-27-42.0 4
Bromoform ND ug/L 10/01/20 01:55 75-25-22.0 4
Bromomethane ND ug/L 10/01/20 01:55 74-83-920.0 4
n-Butylbenzene ND ug/L 10/01/20 01:55 104-51-82.0 4
sec-Butylbenzene ND ug/L 10/01/20 01:55 135-98-82.0 4
tert-Butylbenzene ND ug/L 10/01/20 01:55 98-06-62.0 4
Carbon tetrachloride ND ug/L 10/01/20 01:55 56-23-52.0 4
Chlorobenzene ND ug/L 10/01/20 01:55 108-90-72.0 4
Chloroethane ND ug/L 10/01/20 01:55 75-00-34.0 4
Chloroform ND ug/L 10/01/20 01:55 67-66-32.0 4
Chloromethane ND ug/L 10/01/20 01:55 74-87-34.0 4
2-Chlorotoluene ND ug/L 10/01/20 01:55 95-49-82.0 4
4-Chlorotoluene ND ug/L 10/01/20 01:55 106-43-42.0 4
1,2-Dibromo-3-chloropropane ND ug/L 10/01/20 01:55 96-12-84.0 4
Dibromochloromethane ND ug/L 10/01/20 01:55 124-48-12.0 4
1,2-Dibromoethane (EDB)ND ug/L 10/01/20 01:55 106-93-42.0 4
Dibromomethane ND ug/L 10/01/20 01:55 74-95-32.0 4
1,2-Dichlorobenzene ND ug/L 10/01/20 01:55 95-50-12.0 4
1,3-Dichlorobenzene ND ug/L 10/01/20 01:55 541-73-12.0 4
1,4-Dichlorobenzene ND ug/L 10/01/20 01:55 106-46-72.0 4
Dichlorodifluoromethane ND ug/L 10/01/20 01:55 75-71-82.0 4
1,1-Dichloroethane ND ug/L 10/01/20 01:55 75-34-32.0 4
1,2-Dichloroethane ND ug/L 10/01/20 01:55 107-06-22.0 4
1,1-Dichloroethene ND ug/L 10/01/20 01:55 75-35-42.0 4
cis-1,2-Dichloroethene ND ug/L 10/01/20 01:55 156-59-22.0 4
trans-1,2-Dichloroethene ND ug/L 10/01/20 01:55 156-60-52.0 4
1,2-Dichloropropane ND ug/L 10/01/20 01:55 78-87-52.0 4
1,3-Dichloropropane ND ug/L 10/01/20 01:55 142-28-92.0 4
2,2-Dichloropropane ND ug/L 10/01/20 01:55 594-20-72.0 4
1,1-Dichloropropene ND ug/L 10/01/20 01:55 563-58-62.0 4
cis-1,3-Dichloropropene ND ug/L 10/01/20 01:55 10061-01-52.0 4
trans-1,3-Dichloropropene ND ug/L 10/01/20 01:55 10061-02-62.0 4
Diisopropyl ether ND ug/L 10/01/20 01:55 108-20-32.0 4
Ethylbenzene 163 ug/L 10/01/20 01:55 100-41-42.0 4
Hexachloro-1,3-butadiene ND ug/L 10/01/20 01:55 87-68-38.0 4
Isopropylbenzene (Cumene)26.2 ug/L 10/01/20 01:55 98-82-82.0 4
Methylene Chloride ND ug/L 10/01/20 01:55 75-09-28.0 4
Methyl-tert-butyl ether ND ug/L 10/01/20 01:55 1634-04-42.0 4
Naphthalene 45.6 ug/L 10/01/20 01:55 91-20-38.0 4
n-Propylbenzene ND ug/L 10/01/20 01:55 103-65-12.0 4
Styrene ND ug/L 10/01/20 01:55 100-42-52.0 4
1,1,1,2-Tetrachloroethane ND ug/L 10/01/20 01:55 630-20-62.0 4
1,1,2,2-Tetrachloroethane ND ug/L 10/01/20 01:55 79-34-52.0 4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2020 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92497598
BP Service Center
Sample:MW-7 Lab ID:92497598005 Collected:09/24/20 09:30 Received:09/25/20 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 10/01/20 01:55 127-18-42.0 4
Toluene ND ug/L 10/01/20 01:55 108-88-32.0 4
1,2,3-Trichlorobenzene ND ug/L 10/01/20 01:55 87-61-68.0 4
1,2,4-Trichlorobenzene ND ug/L 10/01/20 01:55 120-82-18.0 4
1,1,1-Trichloroethane ND ug/L 10/01/20 01:55 71-55-62.0 4
1,1,2-Trichloroethane ND ug/L 10/01/20 01:55 79-00-52.0 4
Trichloroethene ND ug/L 10/01/20 01:55 79-01-62.0 4
Trichlorofluoromethane ND ug/L 10/01/20 01:55 75-69-44.0 4
1,2,3-Trichloropropane ND ug/L 10/01/20 01:55 96-18-42.0 4
1,2,4-Trimethylbenzene 348 ug/L 10/01/20 01:55 95-63-62.0 4
1,3,5-Trimethylbenzene 91.9 ug/L 10/01/20 01:55 108-67-82.0 4
Vinyl chloride ND ug/L 10/01/20 01:55 75-01-44.0 4
m&p-Xylene 151 ug/L 10/01/20 01:55 179601-23-14.0 4
o-Xylene 44.2 ug/L 10/01/20 01:55 95-47-62.0 4
Surrogates
1,2-Dichloroethane-d4 (S)103 %10/01/20 01:55 17060-07-070-130 4
4-Bromofluorobenzene (S)93 %10/01/20 01:55 460-00-470-130 4
Toluene-d8 (S)101 %10/01/20 01:55 2037-26-570-130 4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2020 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92497598
BP Service Center
Sample:MW-8A Lab ID:92497598006 Collected:09/24/20 10:00 Received:09/25/20 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 09/29/20 19:07 71-43-20.50 1
Bromobenzene ND ug/L 09/29/20 19:07 108-86-10.50 1
Bromochloromethane ND ug/L 09/29/20 19:07 74-97-50.50 1
Bromodichloromethane ND ug/L 09/29/20 19:07 75-27-40.50 1
Bromoform ND ug/L 09/29/20 19:07 75-25-20.50 1
Bromomethane ND ug/L 09/29/20 19:07 74-83-95.0 1
n-Butylbenzene ND ug/L 09/29/20 19:07 104-51-80.50 1
sec-Butylbenzene ND ug/L 09/29/20 19:07 135-98-80.50 1
tert-Butylbenzene ND ug/L 09/29/20 19:07 98-06-60.50 1
Carbon tetrachloride ND ug/L 09/29/20 19:07 56-23-50.50 1
Chlorobenzene ND ug/L 09/29/20 19:07 108-90-70.50 1
Chloroethane ND ug/L 09/29/20 19:07 75-00-31.0 1
Chloroform ND ug/L 09/29/20 19:07 67-66-30.50 1
Chloromethane ND ug/L 09/29/20 19:07 74-87-31.0 1
2-Chlorotoluene ND ug/L 09/29/20 19:07 95-49-80.50 1
4-Chlorotoluene ND ug/L 09/29/20 19:07 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 09/29/20 19:07 96-12-81.0 1
Dibromochloromethane ND ug/L 09/29/20 19:07 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 09/29/20 19:07 106-93-40.50 1
Dibromomethane ND ug/L 09/29/20 19:07 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 09/29/20 19:07 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 09/29/20 19:07 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 09/29/20 19:07 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 09/29/20 19:07 75-71-80.50 1
1,1-Dichloroethane ND ug/L 09/29/20 19:07 75-34-30.50 1
1,2-Dichloroethane 0.60 ug/L 09/29/20 19:07 107-06-20.50 1
1,1-Dichloroethene ND ug/L 09/29/20 19:07 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 09/29/20 19:07 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 09/29/20 19:07 156-60-50.50 1
1,2-Dichloropropane ND ug/L 09/29/20 19:07 78-87-50.50 1
1,3-Dichloropropane ND ug/L 09/29/20 19:07 142-28-90.50 1
2,2-Dichloropropane ND ug/L 09/29/20 19:07 594-20-70.50 1
1,1-Dichloropropene ND ug/L 09/29/20 19:07 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 09/29/20 19:07 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 09/29/20 19:07 10061-02-60.50 1
Diisopropyl ether ND ug/L 09/29/20 19:07 108-20-30.50 1
Ethylbenzene ND ug/L 09/29/20 19:07 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 09/29/20 19:07 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 09/29/20 19:07 98-82-80.50 1
Methylene Chloride ND ug/L 09/29/20 19:07 75-09-22.0 1
Methyl-tert-butyl ether 12.9 ug/L 09/29/20 19:07 1634-04-40.50 1
Naphthalene ND ug/L 09/29/20 19:07 91-20-32.0 1
n-Propylbenzene ND ug/L 09/29/20 19:07 103-65-10.50 1
Styrene ND ug/L 09/29/20 19:07 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 09/29/20 19:07 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 09/29/20 19:07 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2020 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92497598
BP Service Center
Sample:MW-8A Lab ID:92497598006 Collected:09/24/20 10:00 Received:09/25/20 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 09/29/20 19:07 127-18-40.50 1
Toluene ND ug/L 09/29/20 19:07 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 09/29/20 19:07 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 09/29/20 19:07 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 09/29/20 19:07 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 09/29/20 19:07 79-00-50.50 1
Trichloroethene ND ug/L 09/29/20 19:07 79-01-60.50 1
Trichlorofluoromethane ND ug/L 09/29/20 19:07 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 09/29/20 19:07 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 09/29/20 19:07 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 09/29/20 19:07 108-67-80.50 1
Vinyl chloride ND ug/L 09/29/20 19:07 75-01-41.0 1
m&p-Xylene ND ug/L 09/29/20 19:07 179601-23-11.0 1
o-Xylene ND ug/L 09/29/20 19:07 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)100 %09/29/20 19:07 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %09/29/20 19:07 460-00-470-130 1
Toluene-d8 (S)102 %09/29/20 19:07 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2020 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92497598
BP Service Center
Sample:MW-9 Lab ID:92497598007 Collected:09/24/20 10:25 Received:09/25/20 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 09/29/20 19:26 71-43-20.50 1
Bromobenzene ND ug/L 09/29/20 19:26 108-86-10.50 1
Bromochloromethane ND ug/L 09/29/20 19:26 74-97-50.50 1
Bromodichloromethane ND ug/L 09/29/20 19:26 75-27-40.50 1
Bromoform ND ug/L 09/29/20 19:26 75-25-20.50 1
Bromomethane ND ug/L 09/29/20 19:26 74-83-95.0 1
n-Butylbenzene ND ug/L 09/29/20 19:26 104-51-80.50 1
sec-Butylbenzene ND ug/L 09/29/20 19:26 135-98-80.50 1
tert-Butylbenzene ND ug/L 09/29/20 19:26 98-06-60.50 1
Carbon tetrachloride ND ug/L 09/29/20 19:26 56-23-50.50 1
Chlorobenzene ND ug/L 09/29/20 19:26 108-90-70.50 1
Chloroethane ND ug/L 09/29/20 19:26 75-00-31.0 1
Chloroform ND ug/L 09/29/20 19:26 67-66-30.50 1
Chloromethane ND ug/L 09/29/20 19:26 74-87-31.0 1
2-Chlorotoluene ND ug/L 09/29/20 19:26 95-49-80.50 1
4-Chlorotoluene ND ug/L 09/29/20 19:26 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 09/29/20 19:26 96-12-81.0 1
Dibromochloromethane ND ug/L 09/29/20 19:26 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 09/29/20 19:26 106-93-40.50 1
Dibromomethane ND ug/L 09/29/20 19:26 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 09/29/20 19:26 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 09/29/20 19:26 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 09/29/20 19:26 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 09/29/20 19:26 75-71-80.50 1
1,1-Dichloroethane ND ug/L 09/29/20 19:26 75-34-30.50 1
1,2-Dichloroethane 0.82 ug/L 09/29/20 19:26 107-06-20.50 1
1,1-Dichloroethene ND ug/L 09/29/20 19:26 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 09/29/20 19:26 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 09/29/20 19:26 156-60-50.50 1
1,2-Dichloropropane ND ug/L 09/29/20 19:26 78-87-50.50 1
1,3-Dichloropropane ND ug/L 09/29/20 19:26 142-28-90.50 1
2,2-Dichloropropane ND ug/L 09/29/20 19:26 594-20-70.50 1
1,1-Dichloropropene ND ug/L 09/29/20 19:26 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 09/29/20 19:26 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 09/29/20 19:26 10061-02-60.50 1
Diisopropyl ether ND ug/L 09/29/20 19:26 108-20-30.50 1
Ethylbenzene ND ug/L 09/29/20 19:26 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 09/29/20 19:26 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 09/29/20 19:26 98-82-80.50 1
Methylene Chloride ND ug/L 09/29/20 19:26 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 09/29/20 19:26 1634-04-40.50 1
Naphthalene ND ug/L 09/29/20 19:26 91-20-32.0 1
n-Propylbenzene ND ug/L 09/29/20 19:26 103-65-10.50 1
Styrene ND ug/L 09/29/20 19:26 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 09/29/20 19:26 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 09/29/20 19:26 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2020 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92497598
BP Service Center
Sample:MW-9 Lab ID:92497598007 Collected:09/24/20 10:25 Received:09/25/20 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 09/29/20 19:26 127-18-40.50 1
Toluene ND ug/L 09/29/20 19:26 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 09/29/20 19:26 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 09/29/20 19:26 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 09/29/20 19:26 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 09/29/20 19:26 79-00-50.50 1
Trichloroethene ND ug/L 09/29/20 19:26 79-01-60.50 1
Trichlorofluoromethane ND ug/L 09/29/20 19:26 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 09/29/20 19:26 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 09/29/20 19:26 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 09/29/20 19:26 108-67-80.50 1
Vinyl chloride ND ug/L 09/29/20 19:26 75-01-41.0 1
m&p-Xylene ND ug/L 09/29/20 19:26 179601-23-11.0 1
o-Xylene ND ug/L 09/29/20 19:26 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)102 %09/29/20 19:26 17060-07-070-130 1
4-Bromofluorobenzene (S)100 %09/29/20 19:26 460-00-470-130 1
Toluene-d8 (S)102 %09/29/20 19:26 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2020 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92497598
BP Service Center
Sample:MW-12 Lab ID:92497598008 Collected:09/24/20 10:50 Received:09/25/20 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 09/29/20 17:54 71-43-20.50 1
Bromobenzene ND ug/L 09/29/20 17:54 108-86-10.50 1
Bromochloromethane ND ug/L 09/29/20 17:54 74-97-50.50 1
Bromodichloromethane ND ug/L 09/29/20 17:54 75-27-40.50 1
Bromoform ND ug/L 09/29/20 17:54 75-25-20.50 1
Bromomethane ND ug/L 09/29/20 17:54 74-83-95.0 1
n-Butylbenzene ND ug/L 09/29/20 17:54 104-51-80.50 1
sec-Butylbenzene ND ug/L 09/29/20 17:54 135-98-80.50 1
tert-Butylbenzene ND ug/L 09/29/20 17:54 98-06-60.50 1
Carbon tetrachloride ND ug/L 09/29/20 17:54 56-23-50.50 1
Chlorobenzene ND ug/L 09/29/20 17:54 108-90-70.50 1
Chloroethane ND ug/L 09/29/20 17:54 75-00-31.0 1
Chloroform ND ug/L 09/29/20 17:54 67-66-30.50 1
Chloromethane ND ug/L 09/29/20 17:54 74-87-31.0 1
2-Chlorotoluene ND ug/L 09/29/20 17:54 95-49-80.50 1
4-Chlorotoluene ND ug/L 09/29/20 17:54 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 09/29/20 17:54 96-12-81.0 1
Dibromochloromethane ND ug/L 09/29/20 17:54 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 09/29/20 17:54 106-93-40.50 1
Dibromomethane ND ug/L 09/29/20 17:54 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 09/29/20 17:54 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 09/29/20 17:54 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 09/29/20 17:54 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 09/29/20 17:54 75-71-80.50 1
1,1-Dichloroethane ND ug/L 09/29/20 17:54 75-34-30.50 1
1,2-Dichloroethane ND ug/L 09/29/20 17:54 107-06-20.50 1
1,1-Dichloroethene ND ug/L 09/29/20 17:54 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 09/29/20 17:54 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 09/29/20 17:54 156-60-50.50 1
1,2-Dichloropropane ND ug/L 09/29/20 17:54 78-87-50.50 1
1,3-Dichloropropane ND ug/L 09/29/20 17:54 142-28-90.50 1
2,2-Dichloropropane ND ug/L 09/29/20 17:54 594-20-70.50 1
1,1-Dichloropropene ND ug/L 09/29/20 17:54 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 09/29/20 17:54 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 09/29/20 17:54 10061-02-60.50 1
Diisopropyl ether ND ug/L 09/29/20 17:54 108-20-30.50 1
Ethylbenzene ND ug/L 09/29/20 17:54 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 09/29/20 17:54 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 09/29/20 17:54 98-82-80.50 1
Methylene Chloride ND ug/L 09/29/20 17:54 75-09-22.0 1
Methyl-tert-butyl ether 1.3 ug/L 09/29/20 17:54 1634-04-40.50 1
Naphthalene ND ug/L 09/29/20 17:54 91-20-32.0 1
n-Propylbenzene ND ug/L 09/29/20 17:54 103-65-10.50 1
Styrene ND ug/L 09/29/20 17:54 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 09/29/20 17:54 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 09/29/20 17:54 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2020 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92497598
BP Service Center
Sample:MW-12 Lab ID:92497598008 Collected:09/24/20 10:50 Received:09/25/20 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 09/29/20 17:54 127-18-40.50 1
Toluene ND ug/L 09/29/20 17:54 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 09/29/20 17:54 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 09/29/20 17:54 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 09/29/20 17:54 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 09/29/20 17:54 79-00-50.50 1
Trichloroethene ND ug/L 09/29/20 17:54 79-01-60.50 1
Trichlorofluoromethane ND ug/L 09/29/20 17:54 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 09/29/20 17:54 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 09/29/20 17:54 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 09/29/20 17:54 108-67-80.50 1
Vinyl chloride ND ug/L 09/29/20 17:54 75-01-41.0 1
m&p-Xylene ND ug/L 09/29/20 17:54 179601-23-11.0 1
o-Xylene ND ug/L 09/29/20 17:54 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)96 %09/29/20 17:54 17060-07-070-130 1
4-Bromofluorobenzene (S)98 %09/29/20 17:54 460-00-470-130 1
Toluene-d8 (S)100 %09/29/20 17:54 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2020 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92497598
BP Service Center
Sample:MW-13 Lab ID:92497598009 Collected:09/24/20 11:20 Received:09/25/20 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 09/29/20 19:44 71-43-20.50 1
Bromobenzene ND ug/L 09/29/20 19:44 108-86-10.50 1
Bromochloromethane ND ug/L 09/29/20 19:44 74-97-50.50 1
Bromodichloromethane ND ug/L 09/29/20 19:44 75-27-40.50 1
Bromoform ND ug/L 09/29/20 19:44 75-25-20.50 1
Bromomethane ND ug/L 09/29/20 19:44 74-83-95.0 1
n-Butylbenzene ND ug/L 09/29/20 19:44 104-51-80.50 1
sec-Butylbenzene ND ug/L 09/29/20 19:44 135-98-80.50 1
tert-Butylbenzene ND ug/L 09/29/20 19:44 98-06-60.50 1
Carbon tetrachloride ND ug/L 09/29/20 19:44 56-23-50.50 1
Chlorobenzene ND ug/L 09/29/20 19:44 108-90-70.50 1
Chloroethane ND ug/L 09/29/20 19:44 75-00-31.0 1
Chloroform ND ug/L 09/29/20 19:44 67-66-30.50 1
Chloromethane ND ug/L 09/29/20 19:44 74-87-31.0 1
2-Chlorotoluene ND ug/L 09/29/20 19:44 95-49-80.50 1
4-Chlorotoluene ND ug/L 09/29/20 19:44 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 09/29/20 19:44 96-12-81.0 1
Dibromochloromethane ND ug/L 09/29/20 19:44 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 09/29/20 19:44 106-93-40.50 1
Dibromomethane ND ug/L 09/29/20 19:44 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 09/29/20 19:44 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 09/29/20 19:44 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 09/29/20 19:44 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 09/29/20 19:44 75-71-80.50 1
1,1-Dichloroethane ND ug/L 09/29/20 19:44 75-34-30.50 1
1,2-Dichloroethane ND ug/L 09/29/20 19:44 107-06-20.50 1
1,1-Dichloroethene ND ug/L 09/29/20 19:44 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 09/29/20 19:44 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 09/29/20 19:44 156-60-50.50 1
1,2-Dichloropropane ND ug/L 09/29/20 19:44 78-87-50.50 1
1,3-Dichloropropane ND ug/L 09/29/20 19:44 142-28-90.50 1
2,2-Dichloropropane ND ug/L 09/29/20 19:44 594-20-70.50 1
1,1-Dichloropropene ND ug/L 09/29/20 19:44 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 09/29/20 19:44 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 09/29/20 19:44 10061-02-60.50 1
Diisopropyl ether ND ug/L 09/29/20 19:44 108-20-30.50 1
Ethylbenzene ND ug/L 09/29/20 19:44 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 09/29/20 19:44 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 09/29/20 19:44 98-82-80.50 1
Methylene Chloride ND ug/L 09/29/20 19:44 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 09/29/20 19:44 1634-04-40.50 1
Naphthalene ND ug/L 09/29/20 19:44 91-20-32.0 1
n-Propylbenzene ND ug/L 09/29/20 19:44 103-65-10.50 1
Styrene ND ug/L 09/29/20 19:44 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 09/29/20 19:44 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 09/29/20 19:44 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2020 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92497598
BP Service Center
Sample:MW-13 Lab ID:92497598009 Collected:09/24/20 11:20 Received:09/25/20 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 09/29/20 19:44 127-18-40.50 1
Toluene ND ug/L 09/29/20 19:44 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 09/29/20 19:44 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 09/29/20 19:44 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 09/29/20 19:44 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 09/29/20 19:44 79-00-50.50 1
Trichloroethene ND ug/L 09/29/20 19:44 79-01-60.50 1
Trichlorofluoromethane ND ug/L 09/29/20 19:44 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 09/29/20 19:44 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 09/29/20 19:44 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 09/29/20 19:44 108-67-80.50 1
Vinyl chloride ND ug/L 09/29/20 19:44 75-01-41.0 1
m&p-Xylene ND ug/L 09/29/20 19:44 179601-23-11.0 1
o-Xylene ND ug/L 09/29/20 19:44 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)99 %09/29/20 19:44 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %09/29/20 19:44 460-00-470-130 1
Toluene-d8 (S)101 %09/29/20 19:44 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2020 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92497598
BP Service Center
Sample:MW-14 Lab ID:92497598010 Collected:09/24/20 12:00 Received:09/25/20 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 10/01/20 00:27 71-43-20.50 1
Bromobenzene ND ug/L 10/01/20 00:27 108-86-10.50 1
Bromochloromethane ND ug/L 10/01/20 00:27 74-97-50.50 1
Bromodichloromethane ND ug/L 10/01/20 00:27 75-27-40.50 1
Bromoform ND ug/L 10/01/20 00:27 75-25-20.50 1
Bromomethane ND ug/L 10/01/20 00:27 74-83-95.0 1
n-Butylbenzene ND ug/L 10/01/20 00:27 104-51-80.50 1
sec-Butylbenzene ND ug/L 10/01/20 00:27 135-98-80.50 1
tert-Butylbenzene ND ug/L 10/01/20 00:27 98-06-60.50 1
Carbon tetrachloride ND ug/L 10/01/20 00:27 56-23-50.50 1
Chlorobenzene ND ug/L 10/01/20 00:27 108-90-70.50 1
Chloroethane ND ug/L 10/01/20 00:27 75-00-31.0 1
Chloroform ND ug/L 10/01/20 00:27 67-66-30.50 1
Chloromethane ND ug/L 10/01/20 00:27 74-87-31.0 1
2-Chlorotoluene ND ug/L 10/01/20 00:27 95-49-80.50 1
4-Chlorotoluene ND ug/L 10/01/20 00:27 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 10/01/20 00:27 96-12-81.0 1
Dibromochloromethane ND ug/L 10/01/20 00:27 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 10/01/20 00:27 106-93-40.50 1
Dibromomethane ND ug/L 10/01/20 00:27 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 10/01/20 00:27 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 10/01/20 00:27 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 10/01/20 00:27 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 10/01/20 00:27 75-71-80.50 1
1,1-Dichloroethane ND ug/L 10/01/20 00:27 75-34-30.50 1
1,2-Dichloroethane ND ug/L 10/01/20 00:27 107-06-20.50 1
1,1-Dichloroethene ND ug/L 10/01/20 00:27 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 10/01/20 00:27 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 10/01/20 00:27 156-60-50.50 1
1,2-Dichloropropane ND ug/L 10/01/20 00:27 78-87-50.50 1
1,3-Dichloropropane ND ug/L 10/01/20 00:27 142-28-90.50 1
2,2-Dichloropropane ND ug/L 10/01/20 00:27 594-20-70.50 1
1,1-Dichloropropene ND ug/L 10/01/20 00:27 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 10/01/20 00:27 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 10/01/20 00:27 10061-02-60.50 1
Diisopropyl ether ND ug/L 10/01/20 00:27 108-20-30.50 1
Ethylbenzene ND ug/L 10/01/20 00:27 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 10/01/20 00:27 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 10/01/20 00:27 98-82-80.50 1
Methylene Chloride ND ug/L 10/01/20 00:27 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 10/01/20 00:27 1634-04-40.50 1
Naphthalene ND ug/L 10/01/20 00:27 91-20-32.0 1
n-Propylbenzene ND ug/L 10/01/20 00:27 103-65-10.50 1
Styrene ND ug/L 10/01/20 00:27 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 10/01/20 00:27 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 10/01/20 00:27 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2020 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92497598
BP Service Center
Sample:MW-14 Lab ID:92497598010 Collected:09/24/20 12:00 Received:09/25/20 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 10/01/20 00:27 127-18-40.50 1
Toluene ND ug/L 10/01/20 00:27 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 10/01/20 00:27 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 10/01/20 00:27 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 10/01/20 00:27 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 10/01/20 00:27 79-00-50.50 1
Trichloroethene ND ug/L 10/01/20 00:27 79-01-60.50 1
Trichlorofluoromethane ND ug/L 10/01/20 00:27 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/01/20 00:27 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 10/01/20 00:27 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 10/01/20 00:27 108-67-80.50 1
Vinyl chloride ND ug/L 10/01/20 00:27 75-01-41.0 1
m&p-Xylene ND ug/L 10/01/20 00:27 179601-23-11.0 1
o-Xylene ND ug/L 10/01/20 00:27 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)106 %10/01/20 00:27 17060-07-070-130 1
4-Bromofluorobenzene (S)100 %10/01/20 00:27 460-00-470-130 1
Toluene-d8 (S)105 %10/01/20 00:27 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2020 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92497598
BP Service Center
Sample:MW-15 Lab ID:92497598011 Collected:09/24/20 12:30 Received:09/25/20 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 10/01/20 00:45 71-43-20.50 1
Bromobenzene ND ug/L 10/01/20 00:45 108-86-10.50 1
Bromochloromethane ND ug/L 10/01/20 00:45 74-97-50.50 1
Bromodichloromethane ND ug/L 10/01/20 00:45 75-27-40.50 1
Bromoform ND ug/L 10/01/20 00:45 75-25-20.50 1
Bromomethane ND ug/L 10/01/20 00:45 74-83-95.0 1
n-Butylbenzene ND ug/L 10/01/20 00:45 104-51-80.50 1
sec-Butylbenzene ND ug/L 10/01/20 00:45 135-98-80.50 1
tert-Butylbenzene ND ug/L 10/01/20 00:45 98-06-60.50 1
Carbon tetrachloride ND ug/L 10/01/20 00:45 56-23-50.50 1
Chlorobenzene ND ug/L 10/01/20 00:45 108-90-70.50 1
Chloroethane ND ug/L 10/01/20 00:45 75-00-31.0 1
Chloroform ND ug/L 10/01/20 00:45 67-66-30.50 1
Chloromethane ND ug/L 10/01/20 00:45 74-87-31.0 1
2-Chlorotoluene ND ug/L 10/01/20 00:45 95-49-80.50 1
4-Chlorotoluene ND ug/L 10/01/20 00:45 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 10/01/20 00:45 96-12-81.0 1
Dibromochloromethane ND ug/L 10/01/20 00:45 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 10/01/20 00:45 106-93-40.50 1
Dibromomethane ND ug/L 10/01/20 00:45 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 10/01/20 00:45 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 10/01/20 00:45 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 10/01/20 00:45 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 10/01/20 00:45 75-71-80.50 1
1,1-Dichloroethane ND ug/L 10/01/20 00:45 75-34-30.50 1
1,2-Dichloroethane ND ug/L 10/01/20 00:45 107-06-20.50 1
1,1-Dichloroethene ND ug/L 10/01/20 00:45 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 10/01/20 00:45 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 10/01/20 00:45 156-60-50.50 1
1,2-Dichloropropane ND ug/L 10/01/20 00:45 78-87-50.50 1
1,3-Dichloropropane ND ug/L 10/01/20 00:45 142-28-90.50 1
2,2-Dichloropropane ND ug/L 10/01/20 00:45 594-20-70.50 1
1,1-Dichloropropene ND ug/L 10/01/20 00:45 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 10/01/20 00:45 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 10/01/20 00:45 10061-02-60.50 1
Diisopropyl ether ND ug/L 10/01/20 00:45 108-20-30.50 1
Ethylbenzene 0.78 ug/L 10/01/20 00:45 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 10/01/20 00:45 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 10/01/20 00:45 98-82-80.50 1
Methylene Chloride ND ug/L 10/01/20 00:45 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 10/01/20 00:45 1634-04-40.50 1
Naphthalene ND ug/L 10/01/20 00:45 91-20-32.0 1
n-Propylbenzene 0.60 ug/L 10/01/20 00:45 103-65-10.50 1
Styrene ND ug/L 10/01/20 00:45 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 10/01/20 00:45 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 10/01/20 00:45 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2020 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92497598
BP Service Center
Sample:MW-15 Lab ID:92497598011 Collected:09/24/20 12:30 Received:09/25/20 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 10/01/20 00:45 127-18-40.50 1
Toluene ND ug/L 10/01/20 00:45 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 10/01/20 00:45 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 10/01/20 00:45 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 10/01/20 00:45 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 10/01/20 00:45 79-00-50.50 1
Trichloroethene ND ug/L 10/01/20 00:45 79-01-60.50 1
Trichlorofluoromethane ND ug/L 10/01/20 00:45 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/01/20 00:45 96-18-40.50 1
1,2,4-Trimethylbenzene 1.1 ug/L 10/01/20 00:45 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 10/01/20 00:45 108-67-80.50 1
Vinyl chloride ND ug/L 10/01/20 00:45 75-01-41.0 1
m&p-Xylene ND ug/L 10/01/20 00:45 179601-23-11.0 1
o-Xylene ND ug/L 10/01/20 00:45 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)104 %10/01/20 00:45 17060-07-070-130 1
4-Bromofluorobenzene (S)101 %10/01/20 00:45 460-00-470-130 1
Toluene-d8 (S)104 %10/01/20 00:45 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2020 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92497598
BP Service Center
Sample:MW-16 Lab ID:92497598012 Collected:09/24/20 12:50 Received:09/25/20 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 09/29/20 20:57 71-43-20.50 1
Bromobenzene ND ug/L 09/29/20 20:57 108-86-10.50 1
Bromochloromethane ND ug/L 09/29/20 20:57 74-97-50.50 1
Bromodichloromethane ND ug/L 09/29/20 20:57 75-27-40.50 1
Bromoform ND ug/L 09/29/20 20:57 75-25-20.50 1
Bromomethane ND ug/L 09/29/20 20:57 74-83-95.0 1
n-Butylbenzene ND ug/L 09/29/20 20:57 104-51-80.50 1
sec-Butylbenzene ND ug/L 09/29/20 20:57 135-98-80.50 1
tert-Butylbenzene ND ug/L 09/29/20 20:57 98-06-60.50 1
Carbon tetrachloride ND ug/L 09/29/20 20:57 56-23-50.50 1
Chlorobenzene ND ug/L 09/29/20 20:57 108-90-70.50 1
Chloroethane ND ug/L 09/29/20 20:57 75-00-31.0 1
Chloroform ND ug/L 09/29/20 20:57 67-66-30.50 1
Chloromethane ND ug/L 09/29/20 20:57 74-87-31.0 1
2-Chlorotoluene ND ug/L 09/29/20 20:57 95-49-80.50 1
4-Chlorotoluene ND ug/L 09/29/20 20:57 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 09/29/20 20:57 96-12-81.0 1
Dibromochloromethane ND ug/L 09/29/20 20:57 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 09/29/20 20:57 106-93-40.50 1
Dibromomethane ND ug/L 09/29/20 20:57 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 09/29/20 20:57 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 09/29/20 20:57 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 09/29/20 20:57 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 09/29/20 20:57 75-71-80.50 1
1,1-Dichloroethane ND ug/L 09/29/20 20:57 75-34-30.50 1
1,2-Dichloroethane ND ug/L 09/29/20 20:57 107-06-20.50 1
1,1-Dichloroethene ND ug/L 09/29/20 20:57 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 09/29/20 20:57 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 09/29/20 20:57 156-60-50.50 1
1,2-Dichloropropane ND ug/L 09/29/20 20:57 78-87-50.50 1
1,3-Dichloropropane ND ug/L 09/29/20 20:57 142-28-90.50 1
2,2-Dichloropropane ND ug/L 09/29/20 20:57 594-20-70.50 1
1,1-Dichloropropene ND ug/L 09/29/20 20:57 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 09/29/20 20:57 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 09/29/20 20:57 10061-02-60.50 1
Diisopropyl ether ND ug/L 09/29/20 20:57 108-20-30.50 1
Ethylbenzene ND ug/L 09/29/20 20:57 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 09/29/20 20:57 87-68-32.0 1
Isopropylbenzene (Cumene)0.76 ug/L 09/29/20 20:57 98-82-80.50 1
Methylene Chloride ND ug/L 09/29/20 20:57 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 09/29/20 20:57 1634-04-40.50 1
Naphthalene 7.7 ug/L 09/29/20 20:57 91-20-32.0 1
n-Propylbenzene 1.0 ug/L 09/29/20 20:57 103-65-10.50 1
Styrene ND ug/L 09/29/20 20:57 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 09/29/20 20:57 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 09/29/20 20:57 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2020 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92497598
BP Service Center
Sample:MW-16 Lab ID:92497598012 Collected:09/24/20 12:50 Received:09/25/20 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 09/29/20 20:57 127-18-40.50 1
Toluene ND ug/L 09/29/20 20:57 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 09/29/20 20:57 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 09/29/20 20:57 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 09/29/20 20:57 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 09/29/20 20:57 79-00-50.50 1
Trichloroethene ND ug/L 09/29/20 20:57 79-01-60.50 1
Trichlorofluoromethane ND ug/L 09/29/20 20:57 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 09/29/20 20:57 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 09/29/20 20:57 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 09/29/20 20:57 108-67-80.50 1
Vinyl chloride ND ug/L 09/29/20 20:57 75-01-41.0 1
m&p-Xylene ND ug/L 09/29/20 20:57 179601-23-11.0 1
o-Xylene ND ug/L 09/29/20 20:57 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)100 %09/29/20 20:57 17060-07-070-130 1
4-Bromofluorobenzene (S)97 %09/29/20 20:57 460-00-470-130 1
Toluene-d8 (S)102 %09/29/20 20:57 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2020 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92497598
BP Service Center
Sample:MW-17 Lab ID:92497598013 Collected:09/24/20 13:15 Received:09/25/20 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 09/29/20 18:12 71-43-20.50 1
Bromobenzene ND ug/L 09/29/20 18:12 108-86-10.50 1
Bromochloromethane ND ug/L 09/29/20 18:12 74-97-50.50 1
Bromodichloromethane ND ug/L 09/29/20 18:12 75-27-40.50 1
Bromoform ND ug/L 09/29/20 18:12 75-25-20.50 1
Bromomethane ND ug/L 09/29/20 18:12 74-83-95.0 1
n-Butylbenzene ND ug/L 09/29/20 18:12 104-51-80.50 1
sec-Butylbenzene ND ug/L 09/29/20 18:12 135-98-80.50 1
tert-Butylbenzene ND ug/L 09/29/20 18:12 98-06-60.50 1
Carbon tetrachloride ND ug/L 09/29/20 18:12 56-23-50.50 1
Chlorobenzene ND ug/L 09/29/20 18:12 108-90-70.50 1
Chloroethane ND ug/L 09/29/20 18:12 75-00-31.0 1
Chloroform ND ug/L 09/29/20 18:12 67-66-30.50 1
Chloromethane ND ug/L 09/29/20 18:12 74-87-31.0 1
2-Chlorotoluene ND ug/L 09/29/20 18:12 95-49-80.50 1
4-Chlorotoluene ND ug/L 09/29/20 18:12 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 09/29/20 18:12 96-12-81.0 1
Dibromochloromethane ND ug/L 09/29/20 18:12 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 09/29/20 18:12 106-93-40.50 1
Dibromomethane ND ug/L 09/29/20 18:12 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 09/29/20 18:12 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 09/29/20 18:12 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 09/29/20 18:12 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 09/29/20 18:12 75-71-80.50 1
1,1-Dichloroethane ND ug/L 09/29/20 18:12 75-34-30.50 1
1,2-Dichloroethane ND ug/L 09/29/20 18:12 107-06-20.50 1
1,1-Dichloroethene ND ug/L 09/29/20 18:12 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 09/29/20 18:12 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 09/29/20 18:12 156-60-50.50 1
1,2-Dichloropropane ND ug/L 09/29/20 18:12 78-87-50.50 1
1,3-Dichloropropane ND ug/L 09/29/20 18:12 142-28-90.50 1
2,2-Dichloropropane ND ug/L 09/29/20 18:12 594-20-70.50 1
1,1-Dichloropropene ND ug/L 09/29/20 18:12 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 09/29/20 18:12 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 09/29/20 18:12 10061-02-60.50 1
Diisopropyl ether ND ug/L 09/29/20 18:12 108-20-30.50 1
Ethylbenzene ND ug/L 09/29/20 18:12 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 09/29/20 18:12 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 09/29/20 18:12 98-82-80.50 1
Methylene Chloride ND ug/L 09/29/20 18:12 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 09/29/20 18:12 1634-04-40.50 1
Naphthalene ND ug/L 09/29/20 18:12 91-20-32.0 1
n-Propylbenzene ND ug/L 09/29/20 18:12 103-65-10.50 1
Styrene ND ug/L 09/29/20 18:12 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 09/29/20 18:12 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 09/29/20 18:12 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2020 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92497598
BP Service Center
Sample:MW-17 Lab ID:92497598013 Collected:09/24/20 13:15 Received:09/25/20 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 09/29/20 18:12 127-18-40.50 1
Toluene ND ug/L 09/29/20 18:12 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 09/29/20 18:12 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 09/29/20 18:12 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 09/29/20 18:12 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 09/29/20 18:12 79-00-50.50 1
Trichloroethene ND ug/L 09/29/20 18:12 79-01-60.50 1
Trichlorofluoromethane ND ug/L 09/29/20 18:12 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 09/29/20 18:12 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 09/29/20 18:12 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 09/29/20 18:12 108-67-80.50 1
Vinyl chloride ND ug/L 09/29/20 18:12 75-01-41.0 1
m&p-Xylene ND ug/L 09/29/20 18:12 179601-23-11.0 1
o-Xylene ND ug/L 09/29/20 18:12 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)99 %09/29/20 18:12 17060-07-070-130 1
4-Bromofluorobenzene (S)97 %09/29/20 18:12 460-00-470-130 1
Toluene-d8 (S)102 %09/29/20 18:12 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2020 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92497598
BP Service Center
Sample:MW-18 Lab ID:92497598014 Collected:09/24/20 13:45 Received:09/25/20 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 3.9 ug/L 10/01/20 01:02 71-43-20.50 1
Bromobenzene ND ug/L 10/01/20 01:02 108-86-10.50 1
Bromochloromethane ND ug/L 10/01/20 01:02 74-97-50.50 1
Bromodichloromethane ND ug/L 10/01/20 01:02 75-27-40.50 1
Bromoform ND ug/L 10/01/20 01:02 75-25-20.50 1
Bromomethane ND ug/L 10/01/20 01:02 74-83-95.0 1
n-Butylbenzene ND ug/L 10/01/20 01:02 104-51-80.50 1
sec-Butylbenzene 1.9 ug/L 10/01/20 01:02 135-98-80.50 1
tert-Butylbenzene 0.74 ug/L 10/01/20 01:02 98-06-60.50 1
Carbon tetrachloride ND ug/L 10/01/20 01:02 56-23-50.50 1
Chlorobenzene ND ug/L 10/01/20 01:02 108-90-70.50 1
Chloroethane ND ug/L 10/01/20 01:02 75-00-31.0 1
Chloroform ND ug/L 10/01/20 01:02 67-66-30.50 1
Chloromethane ND ug/L 10/01/20 01:02 74-87-31.0 1
2-Chlorotoluene ND ug/L 10/01/20 01:02 95-49-80.50 1
4-Chlorotoluene ND ug/L 10/01/20 01:02 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 10/01/20 01:02 96-12-81.0 1
Dibromochloromethane ND ug/L 10/01/20 01:02 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 10/01/20 01:02 106-93-40.50 1
Dibromomethane ND ug/L 10/01/20 01:02 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 10/01/20 01:02 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 10/01/20 01:02 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 10/01/20 01:02 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 10/01/20 01:02 75-71-80.50 1
1,1-Dichloroethane ND ug/L 10/01/20 01:02 75-34-30.50 1
1,2-Dichloroethane 0.98 ug/L 10/01/20 01:02 107-06-20.50 1
1,1-Dichloroethene ND ug/L 10/01/20 01:02 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 10/01/20 01:02 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 10/01/20 01:02 156-60-50.50 1
1,2-Dichloropropane ND ug/L 10/01/20 01:02 78-87-50.50 1
1,3-Dichloropropane ND ug/L 10/01/20 01:02 142-28-90.50 1
2,2-Dichloropropane ND ug/L 10/01/20 01:02 594-20-70.50 1
1,1-Dichloropropene ND ug/L 10/01/20 01:02 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 10/01/20 01:02 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 10/01/20 01:02 10061-02-60.50 1
Diisopropyl ether ND ug/L 10/01/20 01:02 108-20-30.50 1
Ethylbenzene 6.8 ug/L 10/01/20 01:02 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 10/01/20 01:02 87-68-32.0 1
Isopropylbenzene (Cumene)2.2 ug/L 10/01/20 01:02 98-82-80.50 1
Methylene Chloride ND ug/L 10/01/20 01:02 75-09-22.0 1
Methyl-tert-butyl ether 81.8 ug/L 10/01/20 01:02 1634-04-40.50 1
Naphthalene 4.8 ug/L 10/01/20 01:02 91-20-32.0 1
n-Propylbenzene 5.2 ug/L 10/01/20 01:02 103-65-10.50 1
Styrene ND ug/L 10/01/20 01:02 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 10/01/20 01:02 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 10/01/20 01:02 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2020 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92497598
BP Service Center
Sample:MW-18 Lab ID:92497598014 Collected:09/24/20 13:45 Received:09/25/20 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 10/01/20 01:02 127-18-40.50 1
Toluene ND ug/L 10/01/20 01:02 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 10/01/20 01:02 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 10/01/20 01:02 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 10/01/20 01:02 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 10/01/20 01:02 79-00-50.50 1
Trichloroethene ND ug/L 10/01/20 01:02 79-01-60.50 1
Trichlorofluoromethane ND ug/L 10/01/20 01:02 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/01/20 01:02 96-18-40.50 1
1,2,4-Trimethylbenzene 0.64 ug/L 10/01/20 01:02 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 10/01/20 01:02 108-67-80.50 1
Vinyl chloride ND ug/L 10/01/20 01:02 75-01-41.0 1
m&p-Xylene ND ug/L 10/01/20 01:02 179601-23-11.0 1
o-Xylene ND ug/L 10/01/20 01:02 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)105 %10/01/20 01:02 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %10/01/20 01:02 460-00-470-130 1
Toluene-d8 (S)102 %10/01/20 01:02 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2020 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92497598
BP Service Center
Sample:VEW-1 Lab ID:92497598015 Collected:09/24/20 14:45 Received:09/25/20 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 09/29/20 20:02 71-43-20.50 1
Bromobenzene ND ug/L 09/29/20 20:02 108-86-10.50 1
Bromochloromethane ND ug/L 09/29/20 20:02 74-97-50.50 1
Bromodichloromethane ND ug/L 09/29/20 20:02 75-27-40.50 1
Bromoform ND ug/L 09/29/20 20:02 75-25-20.50 1
Bromomethane ND ug/L 09/29/20 20:02 74-83-95.0 1
n-Butylbenzene ND ug/L 09/29/20 20:02 104-51-80.50 1
sec-Butylbenzene ND ug/L 09/29/20 20:02 135-98-80.50 1
tert-Butylbenzene ND ug/L 09/29/20 20:02 98-06-60.50 1
Carbon tetrachloride ND ug/L 09/29/20 20:02 56-23-50.50 1
Chlorobenzene ND ug/L 09/29/20 20:02 108-90-70.50 1
Chloroethane ND ug/L 09/29/20 20:02 75-00-31.0 1
Chloroform ND ug/L 09/29/20 20:02 67-66-30.50 1
Chloromethane ND ug/L 09/29/20 20:02 74-87-31.0 1
2-Chlorotoluene ND ug/L 09/29/20 20:02 95-49-80.50 1
4-Chlorotoluene ND ug/L 09/29/20 20:02 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 09/29/20 20:02 96-12-81.0 1
Dibromochloromethane ND ug/L 09/29/20 20:02 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 09/29/20 20:02 106-93-40.50 1
Dibromomethane ND ug/L 09/29/20 20:02 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 09/29/20 20:02 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 09/29/20 20:02 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 09/29/20 20:02 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 09/29/20 20:02 75-71-80.50 1
1,1-Dichloroethane ND ug/L 09/29/20 20:02 75-34-30.50 1
1,2-Dichloroethane ND ug/L 09/29/20 20:02 107-06-20.50 1
1,1-Dichloroethene ND ug/L 09/29/20 20:02 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 09/29/20 20:02 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 09/29/20 20:02 156-60-50.50 1
1,2-Dichloropropane ND ug/L 09/29/20 20:02 78-87-50.50 1
1,3-Dichloropropane ND ug/L 09/29/20 20:02 142-28-90.50 1
2,2-Dichloropropane ND ug/L 09/29/20 20:02 594-20-70.50 1
1,1-Dichloropropene ND ug/L 09/29/20 20:02 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 09/29/20 20:02 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 09/29/20 20:02 10061-02-60.50 1
Diisopropyl ether ND ug/L 09/29/20 20:02 108-20-30.50 1
Ethylbenzene ND ug/L 09/29/20 20:02 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 09/29/20 20:02 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 09/29/20 20:02 98-82-80.50 1
Methylene Chloride ND ug/L 09/29/20 20:02 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 09/29/20 20:02 1634-04-40.50 1
Naphthalene ND ug/L 09/29/20 20:02 91-20-32.0 1
n-Propylbenzene ND ug/L 09/29/20 20:02 103-65-10.50 1
Styrene ND ug/L 09/29/20 20:02 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 09/29/20 20:02 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 09/29/20 20:02 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2020 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92497598
BP Service Center
Sample:VEW-1 Lab ID:92497598015 Collected:09/24/20 14:45 Received:09/25/20 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 09/29/20 20:02 127-18-40.50 1
Toluene ND ug/L 09/29/20 20:02 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 09/29/20 20:02 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 09/29/20 20:02 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 09/29/20 20:02 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 09/29/20 20:02 79-00-50.50 1
Trichloroethene ND ug/L 09/29/20 20:02 79-01-60.50 1
Trichlorofluoromethane ND ug/L 09/29/20 20:02 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 09/29/20 20:02 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 09/29/20 20:02 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 09/29/20 20:02 108-67-80.50 1
Vinyl chloride ND ug/L 09/29/20 20:02 75-01-41.0 1
m&p-Xylene ND ug/L 09/29/20 20:02 179601-23-11.0 1
o-Xylene ND ug/L 09/29/20 20:02 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)104 %09/29/20 20:02 17060-07-070-130 1
4-Bromofluorobenzene (S)98 %09/29/20 20:02 460-00-470-130 1
Toluene-d8 (S)102 %09/29/20 20:02 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2020 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92497598
BP Service Center
Sample:SW-1 Lab ID:92497598016 Collected:09/24/20 15:00 Received:09/25/20 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 09/29/20 20:39 71-43-20.50 1
Bromobenzene ND ug/L 09/29/20 20:39 108-86-10.50 1
Bromochloromethane ND ug/L 09/29/20 20:39 74-97-50.50 1
Bromodichloromethane ND ug/L 09/29/20 20:39 75-27-40.50 1
Bromoform ND ug/L 09/29/20 20:39 75-25-20.50 1
Bromomethane ND ug/L 09/29/20 20:39 74-83-95.0 1
n-Butylbenzene ND ug/L 09/29/20 20:39 104-51-80.50 1
sec-Butylbenzene ND ug/L 09/29/20 20:39 135-98-80.50 1
tert-Butylbenzene ND ug/L 09/29/20 20:39 98-06-60.50 1
Carbon tetrachloride ND ug/L 09/29/20 20:39 56-23-50.50 1
Chlorobenzene ND ug/L 09/29/20 20:39 108-90-70.50 1
Chloroethane ND ug/L 09/29/20 20:39 75-00-31.0 1
Chloroform ND ug/L 09/29/20 20:39 67-66-30.50 1
Chloromethane ND ug/L 09/29/20 20:39 74-87-31.0 1
2-Chlorotoluene ND ug/L 09/29/20 20:39 95-49-80.50 1
4-Chlorotoluene ND ug/L 09/29/20 20:39 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 09/29/20 20:39 96-12-81.0 1
Dibromochloromethane ND ug/L 09/29/20 20:39 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 09/29/20 20:39 106-93-40.50 1
Dibromomethane ND ug/L 09/29/20 20:39 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 09/29/20 20:39 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 09/29/20 20:39 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 09/29/20 20:39 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 09/29/20 20:39 75-71-80.50 1
1,1-Dichloroethane ND ug/L 09/29/20 20:39 75-34-30.50 1
1,2-Dichloroethane ND ug/L 09/29/20 20:39 107-06-20.50 1
1,1-Dichloroethene ND ug/L 09/29/20 20:39 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 09/29/20 20:39 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 09/29/20 20:39 156-60-50.50 1
1,2-Dichloropropane 2.0 ug/L 09/29/20 20:39 78-87-50.50 1
1,3-Dichloropropane ND ug/L 09/29/20 20:39 142-28-90.50 1
2,2-Dichloropropane ND ug/L 09/29/20 20:39 594-20-70.50 1
1,1-Dichloropropene ND ug/L 09/29/20 20:39 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 09/29/20 20:39 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 09/29/20 20:39 10061-02-60.50 1
Diisopropyl ether ND ug/L 09/29/20 20:39 108-20-30.50 1
Ethylbenzene ND ug/L 09/29/20 20:39 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 09/29/20 20:39 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 09/29/20 20:39 98-82-80.50 1
Methylene Chloride ND ug/L 09/29/20 20:39 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 09/29/20 20:39 1634-04-40.50 1
Naphthalene ND ug/L 09/29/20 20:39 91-20-32.0 1
n-Propylbenzene ND ug/L 09/29/20 20:39 103-65-10.50 1
Styrene ND ug/L 09/29/20 20:39 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 09/29/20 20:39 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 09/29/20 20:39 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2020 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92497598
BP Service Center
Sample:SW-1 Lab ID:92497598016 Collected:09/24/20 15:00 Received:09/25/20 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 09/29/20 20:39 127-18-40.50 1
Toluene ND ug/L 09/29/20 20:39 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 09/29/20 20:39 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 09/29/20 20:39 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 09/29/20 20:39 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 09/29/20 20:39 79-00-50.50 1
Trichloroethene ND ug/L 09/29/20 20:39 79-01-60.50 1
Trichlorofluoromethane ND ug/L 09/29/20 20:39 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 09/29/20 20:39 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 09/29/20 20:39 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 09/29/20 20:39 108-67-80.50 1
Vinyl chloride ND ug/L 09/29/20 20:39 75-01-41.0 1
m&p-Xylene ND ug/L 09/29/20 20:39 179601-23-11.0 1
o-Xylene ND ug/L 09/29/20 20:39 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)101 %09/29/20 20:39 17060-07-070-130 1
4-Bromofluorobenzene (S)98 %09/29/20 20:39 460-00-470-130 1
Toluene-d8 (S)102 %09/29/20 20:39 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2020 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92497598
BP Service Center
Sample:IW-3 Lab ID:92497598017 Collected:09/24/20 15:15 Received:09/25/20 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 09/29/20 18:31 71-43-20.50 1
Bromobenzene ND ug/L 09/29/20 18:31 108-86-10.50 1
Bromochloromethane ND ug/L 09/29/20 18:31 74-97-50.50 1
Bromodichloromethane ND ug/L 09/29/20 18:31 75-27-40.50 1
Bromoform ND ug/L 09/29/20 18:31 75-25-20.50 1
Bromomethane ND ug/L 09/29/20 18:31 74-83-95.0 1
n-Butylbenzene ND ug/L 09/29/20 18:31 104-51-80.50 1
sec-Butylbenzene ND ug/L 09/29/20 18:31 135-98-80.50 1
tert-Butylbenzene ND ug/L 09/29/20 18:31 98-06-60.50 1
Carbon tetrachloride ND ug/L 09/29/20 18:31 56-23-50.50 1
Chlorobenzene ND ug/L 09/29/20 18:31 108-90-70.50 1
Chloroethane ND ug/L 09/29/20 18:31 75-00-31.0 1
Chloroform ND ug/L 09/29/20 18:31 67-66-30.50 1
Chloromethane ND ug/L 09/29/20 18:31 74-87-31.0 1
2-Chlorotoluene ND ug/L 09/29/20 18:31 95-49-80.50 1
4-Chlorotoluene ND ug/L 09/29/20 18:31 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 09/29/20 18:31 96-12-81.0 1
Dibromochloromethane ND ug/L 09/29/20 18:31 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 09/29/20 18:31 106-93-40.50 1
Dibromomethane ND ug/L 09/29/20 18:31 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 09/29/20 18:31 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 09/29/20 18:31 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 09/29/20 18:31 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 09/29/20 18:31 75-71-80.50 1
1,1-Dichloroethane ND ug/L 09/29/20 18:31 75-34-30.50 1
1,2-Dichloroethane ND ug/L 09/29/20 18:31 107-06-20.50 1
1,1-Dichloroethene ND ug/L 09/29/20 18:31 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 09/29/20 18:31 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 09/29/20 18:31 156-60-50.50 1
1,2-Dichloropropane ND ug/L 09/29/20 18:31 78-87-50.50 1
1,3-Dichloropropane ND ug/L 09/29/20 18:31 142-28-90.50 1
2,2-Dichloropropane ND ug/L 09/29/20 18:31 594-20-70.50 1
1,1-Dichloropropene ND ug/L 09/29/20 18:31 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 09/29/20 18:31 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 09/29/20 18:31 10061-02-60.50 1
Diisopropyl ether ND ug/L 09/29/20 18:31 108-20-30.50 1
Ethylbenzene ND ug/L 09/29/20 18:31 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 09/29/20 18:31 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 09/29/20 18:31 98-82-80.50 1
Methylene Chloride ND ug/L 09/29/20 18:31 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 09/29/20 18:31 1634-04-40.50 1
Naphthalene ND ug/L 09/29/20 18:31 91-20-32.0 1
n-Propylbenzene ND ug/L 09/29/20 18:31 103-65-10.50 1
Styrene ND ug/L 09/29/20 18:31 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 09/29/20 18:31 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 09/29/20 18:31 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2020 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92497598
BP Service Center
Sample:IW-3 Lab ID:92497598017 Collected:09/24/20 15:15 Received:09/25/20 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 09/29/20 18:31 127-18-40.50 1
Toluene ND ug/L 09/29/20 18:31 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 09/29/20 18:31 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 09/29/20 18:31 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 09/29/20 18:31 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 09/29/20 18:31 79-00-50.50 1
Trichloroethene ND ug/L 09/29/20 18:31 79-01-60.50 1
Trichlorofluoromethane ND ug/L 09/29/20 18:31 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 09/29/20 18:31 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 09/29/20 18:31 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 09/29/20 18:31 108-67-80.50 1
Vinyl chloride ND ug/L 09/29/20 18:31 75-01-41.0 1
m&p-Xylene ND ug/L 09/29/20 18:31 179601-23-11.0 1
o-Xylene ND ug/L 09/29/20 18:31 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)99 %09/29/20 18:31 17060-07-070-130 1
4-Bromofluorobenzene (S)98 %09/29/20 18:31 460-00-470-130 1
Toluene-d8 (S)102 %09/29/20 18:31 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2020 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92497598
BP Service Center
Sample:SW-8 Lab ID:92497598018 Collected:09/24/20 15:35 Received:09/25/20 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 09/29/20 18:49 71-43-20.50 1
Bromobenzene ND ug/L 09/29/20 18:49 108-86-10.50 1
Bromochloromethane ND ug/L 09/29/20 18:49 74-97-50.50 1
Bromodichloromethane ND ug/L 09/29/20 18:49 75-27-40.50 1
Bromoform ND ug/L 09/29/20 18:49 75-25-20.50 1
Bromomethane ND ug/L 09/29/20 18:49 74-83-95.0 1
n-Butylbenzene ND ug/L 09/29/20 18:49 104-51-80.50 1
sec-Butylbenzene ND ug/L 09/29/20 18:49 135-98-80.50 1
tert-Butylbenzene ND ug/L 09/29/20 18:49 98-06-60.50 1
Carbon tetrachloride ND ug/L 09/29/20 18:49 56-23-50.50 1
Chlorobenzene ND ug/L 09/29/20 18:49 108-90-70.50 1
Chloroethane ND ug/L 09/29/20 18:49 75-00-31.0 1
Chloroform ND ug/L 09/29/20 18:49 67-66-30.50 1
Chloromethane ND ug/L 09/29/20 18:49 74-87-31.0 1
2-Chlorotoluene ND ug/L 09/29/20 18:49 95-49-80.50 1
4-Chlorotoluene ND ug/L 09/29/20 18:49 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 09/29/20 18:49 96-12-81.0 1
Dibromochloromethane ND ug/L 09/29/20 18:49 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 09/29/20 18:49 106-93-40.50 1
Dibromomethane ND ug/L 09/29/20 18:49 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 09/29/20 18:49 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 09/29/20 18:49 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 09/29/20 18:49 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 09/29/20 18:49 75-71-80.50 1
1,1-Dichloroethane ND ug/L 09/29/20 18:49 75-34-30.50 1
1,2-Dichloroethane ND ug/L 09/29/20 18:49 107-06-20.50 1
1,1-Dichloroethene ND ug/L 09/29/20 18:49 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 09/29/20 18:49 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 09/29/20 18:49 156-60-50.50 1
1,2-Dichloropropane ND ug/L 09/29/20 18:49 78-87-50.50 1
1,3-Dichloropropane ND ug/L 09/29/20 18:49 142-28-90.50 1
2,2-Dichloropropane ND ug/L 09/29/20 18:49 594-20-70.50 1
1,1-Dichloropropene ND ug/L 09/29/20 18:49 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 09/29/20 18:49 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 09/29/20 18:49 10061-02-60.50 1
Diisopropyl ether ND ug/L 09/29/20 18:49 108-20-30.50 1
Ethylbenzene ND ug/L 09/29/20 18:49 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 09/29/20 18:49 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 09/29/20 18:49 98-82-80.50 1
Methylene Chloride ND ug/L 09/29/20 18:49 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 09/29/20 18:49 1634-04-40.50 1
Naphthalene ND ug/L 09/29/20 18:49 91-20-32.0 1
n-Propylbenzene ND ug/L 09/29/20 18:49 103-65-10.50 1
Styrene ND ug/L 09/29/20 18:49 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 09/29/20 18:49 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 09/29/20 18:49 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2020 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 58
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92497598
BP Service Center
Sample:SW-8 Lab ID:92497598018 Collected:09/24/20 15:35 Received:09/25/20 08:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 09/29/20 18:49 127-18-40.50 1
Toluene ND ug/L 09/29/20 18:49 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 09/29/20 18:49 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 09/29/20 18:49 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 09/29/20 18:49 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 09/29/20 18:49 79-00-50.50 1
Trichloroethene ND ug/L 09/29/20 18:49 79-01-60.50 1
Trichlorofluoromethane ND ug/L 09/29/20 18:49 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 09/29/20 18:49 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 09/29/20 18:49 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 09/29/20 18:49 108-67-80.50 1
Vinyl chloride ND ug/L 09/29/20 18:49 75-01-41.0 1
m&p-Xylene ND ug/L 09/29/20 18:49 179601-23-11.0 1
o-Xylene ND ug/L 09/29/20 18:49 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)100 %09/29/20 18:49 17060-07-070-130 1
4-Bromofluorobenzene (S)98 %09/29/20 18:49 460-00-470-130 1
Toluene-d8 (S)102 %09/29/20 18:49 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2020 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 58
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92497598
BP Service Center
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
569694
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92497598001, 92497598003, 92497598004, 92497598006, 92497598007, 92497598008, 92497598009,
92497598012, 92497598013, 92497598015, 92497598016, 92497598017, 92497598018
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3017981
Associated Lab Samples:92497598001, 92497598003, 92497598004, 92497598006, 92497598007, 92497598008, 92497598009,
92497598012, 92497598013, 92497598015, 92497598016, 92497598017, 92497598018
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 09/29/20 17:36
1,1,1-Trichloroethane ug/L ND 0.50 09/29/20 17:36
1,1,2,2-Tetrachloroethane ug/L ND 0.50 09/29/20 17:36
1,1,2-Trichloroethane ug/L ND 0.50 09/29/20 17:36
1,1-Dichloroethane ug/L ND 0.50 09/29/20 17:36
1,1-Dichloroethene ug/L ND 0.50 09/29/20 17:36
1,1-Dichloropropene ug/L ND 0.50 09/29/20 17:36
1,2,3-Trichlorobenzene ug/L ND 2.0 09/29/20 17:36
1,2,3-Trichloropropane ug/L ND 0.50 09/29/20 17:36
1,2,4-Trichlorobenzene ug/L ND 2.0 09/29/20 17:36
1,2,4-Trimethylbenzene ug/L ND 0.50 09/29/20 17:36
1,2-Dibromo-3-chloropropane ug/L ND 1.0 09/29/20 17:36
1,2-Dibromoethane (EDB)ug/L ND 0.50 09/29/20 17:36
1,2-Dichlorobenzene ug/L ND 0.50 09/29/20 17:36
1,2-Dichloroethane ug/L ND 0.50 09/29/20 17:36
1,2-Dichloropropane ug/L ND 0.50 09/29/20 17:36
1,3,5-Trimethylbenzene ug/L ND 0.50 09/29/20 17:36
1,3-Dichlorobenzene ug/L ND 0.50 09/29/20 17:36
1,3-Dichloropropane ug/L ND 0.50 09/29/20 17:36
1,4-Dichlorobenzene ug/L ND 0.50 09/29/20 17:36
2,2-Dichloropropane ug/L ND 0.50 09/29/20 17:36
2-Chlorotoluene ug/L ND 0.50 09/29/20 17:36
4-Chlorotoluene ug/L ND 0.50 09/29/20 17:36
Benzene ug/L ND 0.50 09/29/20 17:36
Bromobenzene ug/L ND 0.50 09/29/20 17:36
Bromochloromethane ug/L ND 0.50 09/29/20 17:36
Bromodichloromethane ug/L ND 0.50 09/29/20 17:36
Bromoform ug/L ND 0.50 09/29/20 17:36
Bromomethane ug/L ND 5.0 09/29/20 17:36
Carbon tetrachloride ug/L ND 0.50 09/29/20 17:36
Chlorobenzene ug/L ND 0.50 09/29/20 17:36
Chloroethane ug/L ND 1.0 09/29/20 17:36
Chloroform ug/L ND 0.50 09/29/20 17:36
Chloromethane ug/L ND 1.0 09/29/20 17:36
cis-1,2-Dichloroethene ug/L ND 0.50 09/29/20 17:36
cis-1,3-Dichloropropene ug/L ND 0.50 09/29/20 17:36
Dibromochloromethane ug/L ND 0.50 09/29/20 17:36
Dibromomethane ug/L ND 0.50 09/29/20 17:36
Dichlorodifluoromethane ug/L ND 0.50 09/29/20 17:36
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2020 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 58
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92497598
BP Service Center
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3017981
Associated Lab Samples:92497598001, 92497598003, 92497598004, 92497598006, 92497598007, 92497598008, 92497598009,
92497598012, 92497598013, 92497598015, 92497598016, 92497598017, 92497598018
Matrix:Water
Analyzed
Diisopropyl ether ug/L ND 0.50 09/29/20 17:36
Ethylbenzene ug/L ND 0.50 09/29/20 17:36
Hexachloro-1,3-butadiene ug/L ND 2.0 09/29/20 17:36
Isopropylbenzene (Cumene)ug/L ND 0.50 09/29/20 17:36
m&p-Xylene ug/L ND 1.0 09/29/20 17:36
Methyl-tert-butyl ether ug/L ND 0.50 09/29/20 17:36
Methylene Chloride ug/L ND 2.0 09/29/20 17:36
n-Butylbenzene ug/L ND 0.50 09/29/20 17:36
n-Propylbenzene ug/L ND 0.50 09/29/20 17:36
Naphthalene ug/L ND 2.0 09/29/20 17:36
o-Xylene ug/L ND 0.50 09/29/20 17:36
sec-Butylbenzene ug/L ND 0.50 09/29/20 17:36
Styrene ug/L ND 0.50 09/29/20 17:36
tert-Butylbenzene ug/L ND 0.50 09/29/20 17:36
Tetrachloroethene ug/L ND 0.50 09/29/20 17:36
Toluene ug/L ND 0.50 09/29/20 17:36
trans-1,2-Dichloroethene ug/L ND 0.50 09/29/20 17:36
trans-1,3-Dichloropropene ug/L ND 0.50 09/29/20 17:36
Trichloroethene ug/L ND 0.50 09/29/20 17:36
Trichlorofluoromethane ug/L ND 1.0 09/29/20 17:36
Vinyl chloride ug/L ND 1.0 09/29/20 17:36
1,2-Dichloroethane-d4 (S)%98 70-130 09/29/20 17:36
4-Bromofluorobenzene (S)%98 70-130 09/29/20 17:36
Toluene-d8 (S)%100 70-130 09/29/20 17:36
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3017982LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 52.350 105 60-140
1,1,1-Trichloroethane ug/L 53.850 108 60-140
1,1,2,2-Tetrachloroethane ug/L 49.450 99 60-140
1,1,2-Trichloroethane ug/L 51.050 102 60-140
1,1-Dichloroethane ug/L 51.650 103 60-140
1,1-Dichloroethene ug/L 55.250 110 60-140
1,1-Dichloropropene ug/L 54.650 109 60-140
1,2,3-Trichlorobenzene ug/L 57.750 115 60-140
1,2,3-Trichloropropane ug/L 49.250 98 60-140
1,2,4-Trichlorobenzene ug/L 56.050 112 60-140
1,2,4-Trimethylbenzene ug/L 50.350 101 60-140
1,2-Dibromo-3-chloropropane ug/L 55.150 110 60-140
1,2-Dibromoethane (EDB)ug/L 50.850 102 60-140
1,2-Dichlorobenzene ug/L 51.450 103 60-140
1,2-Dichloroethane ug/L 48.050 96 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2020 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 58
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92497598
BP Service Center
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3017982LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichloropropane ug/L 53.350 107 60-140
1,3,5-Trimethylbenzene ug/L 50.650 101 60-140
1,3-Dichlorobenzene ug/L 51.350 103 60-140
1,3-Dichloropropane ug/L 52.750 105 60-140
1,4-Dichlorobenzene ug/L 51.250 102 60-140
2,2-Dichloropropane ug/L 55.750 111 60-140
2-Chlorotoluene ug/L 50.950 102 60-140
4-Chlorotoluene ug/L 50.250 100 60-140
Benzene ug/L 51.050 102 60-140
Bromobenzene ug/L 49.150 98 60-140
Bromochloromethane ug/L 52.150 104 60-140
Bromodichloromethane ug/L 49.350 99 60-140
Bromoform ug/L 52.950 106 60-140
Bromomethane ug/L 65.150 130 60-140
Carbon tetrachloride ug/L 52.450 105 60-140
Chlorobenzene ug/L 49.650 99 60-140
Chloroethane ug/L 35.150 70 60-140
Chloroform ug/L 52.050 104 60-140
Chloromethane ug/L 44.850 90 60-140
cis-1,2-Dichloroethene ug/L 51.950 104 60-140
cis-1,3-Dichloropropene ug/L 55.450 111 60-140
Dibromochloromethane ug/L 54.150 108 60-140
Dibromomethane ug/L 50.050 100 60-140
Dichlorodifluoromethane ug/L 43.950 88 60-140
Diisopropyl ether ug/L 50.050 100 60-140
Ethylbenzene ug/L 49.850 100 60-140
Hexachloro-1,3-butadiene ug/L 52.250 104 60-140
Isopropylbenzene (Cumene)ug/L 51.050 102 60-140
m&p-Xylene ug/L 101100 101 60-140
Methyl-tert-butyl ether ug/L 50.950 102 60-140
Methylene Chloride ug/L 50.950 102 60-140
n-Butylbenzene ug/L 51.350 103 60-140
n-Propylbenzene ug/L 50.250 100 60-140
Naphthalene ug/L 58.450 117 60-140
o-Xylene ug/L 50.450 101 60-140
sec-Butylbenzene ug/L 50.150 100 60-140
Styrene ug/L 52.750 105 60-140
tert-Butylbenzene ug/L 42.250 84 60-140
Tetrachloroethene ug/L 50.350 101 60-140
Toluene ug/L 49.850 100 60-140
trans-1,2-Dichloroethene ug/L 54.150 108 60-140
trans-1,3-Dichloropropene ug/L 53.750 107 60-140
Trichloroethene ug/L 53.850 108 60-140
Trichlorofluoromethane ug/L 44.550 89 60-140
Vinyl chloride ug/L 46.350 93 60-140
1,2-Dichloroethane-d4 (S)%94 70-130
4-Bromofluorobenzene (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2020 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 58
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92497598
BP Service Center
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3017982LABORATORY CONTROL SAMPLE:
LCSSpike
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3017983MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92497598008
3017984
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 94 60-140107 13 3020ND18.9 21.4
1,1,1-Trichloroethane ug/L 20 104 60-140118 13 3020ND20.7 23.6
1,1,2,2-Tetrachloroethane ug/L 20 101 60-140110 8 3020ND20.2 22.0
1,1,2-Trichloroethane ug/L 20 99 60-140111 12 3020ND19.7 22.2
1,1-Dichloroethane ug/L 20 102 60-140113 10 3020ND20.5 22.6
1,1-Dichloroethene ug/L 20 109 60-140116 6 3020ND21.9 23.2
1,1-Dichloropropene ug/L 20 105 60-140117 11 3020ND20.9 23.4
1,2,3-Trichlorobenzene ug/L 20 91 60-140101 10 3020ND18.2 20.2
1,2,3-Trichloropropane ug/L 20 95 60-140105 10 3020ND18.9 20.9
1,2,4-Trichlorobenzene ug/L 20 84 60-14099 16 3020ND16.7 19.7
1,2,4-Trimethylbenzene ug/L 20 85 60-14096 13 3020ND17.0 19.3
1,2-Dibromo-3-
chloropropane ug/L 20 107 60-140106 1 3020ND21.4 21.3
1,2-Dibromoethane (EDB)ug/L 20 101 60-140109 8 3020ND20.1 21.8
1,2-Dichlorobenzene ug/L 20 87 60-140101 15 3020ND17.3 20.1
1,2-Dichloroethane ug/L 20 94 60-140107 13 3020ND18.7 21.4
1,2-Dichloropropane ug/L 20 103 60-140118 13 3020ND20.7 23.5
1,3,5-Trimethylbenzene ug/L 20 87 60-14097 11 3020ND17.4 19.4
1,3-Dichlorobenzene ug/L 20 85 60-14098 14 3020ND17.0 19.5
1,3-Dichloropropane ug/L 20 100 60-140111 10 3020ND20.0 22.2
1,4-Dichlorobenzene ug/L 20 88 60-14093 6 3020ND17.7 18.7
2,2-Dichloropropane ug/L 20 88 60-140100 13 3020ND17.5 19.9
2-Chlorotoluene ug/L 20 84 60-14095 12 3020ND16.8 19.0
4-Chlorotoluene ug/L 20 87 60-14096 10 3020ND17.4 19.1
Benzene ug/L 20 100 60-140113 12 3020ND20.0 22.5
Bromobenzene ug/L 20 91 60-14099 8 3020ND18.3 19.9
Bromochloromethane ug/L 20 105 60-140117 11 3020ND21.0 23.3
Bromodichloromethane ug/L 20 93 60-140105 12 3020ND18.5 21.0
Bromoform ug/L 20 102 60-140112 9 3020ND20.4 22.4
Bromomethane ug/L 20 84 60-140101 19 3020ND16.8 20.2
Carbon tetrachloride ug/L 20 105 60-140117 11 3020ND21.0 23.4
Chlorobenzene ug/L 20 93 60-140104 11 3020ND18.5 20.8
Chloroethane ug/L 20 90 60-140106 16 3020ND18.0 21.2
Chloroform ug/L 20 92 60-140110 18 3020ND18.4 22.0
Chloromethane ug/L 20 82 60-14095 15 3020ND16.5 19.1
cis-1,2-Dichloroethene ug/L 20 101 60-140116 14 3020ND20.1 23.1
cis-1,3-Dichloropropene ug/L 20 102 60-140116 12 3020ND20.4 23.1
Dibromochloromethane ug/L 20 98 60-140108 9 3020ND19.7 21.6
Dibromomethane ug/L 20 105 60-140118 12 3020ND21.0 23.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2020 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 58
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92497598
BP Service Center
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3017983MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92497598008
3017984
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Dichlorodifluoromethane ug/L 20 88 60-140101 14 3020ND17.6 20.2
Diisopropyl ether ug/L 20 95 60-140107 12 3020ND19.1 21.4
Ethylbenzene ug/L 20 90 60-140101 12 3020ND18.0 20.3
Hexachloro-1,3-butadiene ug/L 20 74 60-14093 23 3020ND14.8 18.6
Isopropylbenzene
(Cumene)
ug/L 20 88 60-140102 15 3020ND17.6 20.4
m&p-Xylene ug/L 40 89 60-140103 14 3040ND35.8 41.0
Methyl-tert-butyl ether ug/L 20 102 60-140114 11 30201.3 21.7 24.2
Methylene Chloride ug/L 20 99 60-140113 13 3020ND19.7 22.6
n-Butylbenzene ug/L 20 82 60-14092 11 3020ND16.4 18.3
n-Propylbenzene ug/L 20 87 60-14096 10 3020ND17.3 19.2
Naphthalene ug/L 20 92 60-140104 12 3020ND18.4 20.7
o-Xylene ug/L 20 89 60-140102 13 3020ND17.8 20.4
sec-Butylbenzene ug/L 20 87 60-14098 12 3020ND17.4 19.6
Styrene ug/L 20 91 60-140103 13 3020ND18.2 20.7
tert-Butylbenzene ug/L 20 74 60-14083 12 3020ND14.7 16.7
Tetrachloroethene ug/L 20 95 60-140104 9 3020ND19.0 20.8
Toluene ug/L 20 93 60-140105 12 3020ND18.6 21.0
trans-1,2-Dichloroethene ug/L 20 104 60-140118 12 3020ND20.9 23.5
trans-1,3-Dichloropropene ug/L 20 97 60-140109 11 3020ND19.4 21.8
Trichloroethene ug/L 20 104 60-140118 13 3020ND20.8 23.6
Trichlorofluoromethane ug/L 20 88 60-140107 19 3020ND17.6 21.4
Vinyl chloride ug/L 20 89 60-140101 13 3020ND17.8 20.3
1,2-Dichloroethane-d4 (S)%101 70-130103
4-Bromofluorobenzene (S)%98 70-130102
Toluene-d8 (S)%100 70-130101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2020 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 58
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92497598
BP Service Center
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
570101
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92497598002, 92497598005, 92497598010, 92497598011, 92497598014
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3020098
Associated Lab Samples:92497598002, 92497598005, 92497598010, 92497598011, 92497598014
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 09/30/20 22:07
1,1,1-Trichloroethane ug/L ND 0.50 09/30/20 22:07
1,1,2,2-Tetrachloroethane ug/L ND 0.50 09/30/20 22:07
1,1,2-Trichloroethane ug/L ND 0.50 09/30/20 22:07
1,1-Dichloroethane ug/L ND 0.50 09/30/20 22:07
1,1-Dichloroethene ug/L ND 0.50 09/30/20 22:07
1,1-Dichloropropene ug/L ND 0.50 09/30/20 22:07
1,2,3-Trichlorobenzene ug/L ND 2.0 09/30/20 22:07
1,2,3-Trichloropropane ug/L ND 0.50 09/30/20 22:07
1,2,4-Trichlorobenzene ug/L ND 2.0 09/30/20 22:07
1,2,4-Trimethylbenzene ug/L ND 0.50 09/30/20 22:07
1,2-Dibromo-3-chloropropane ug/L ND 1.0 09/30/20 22:07
1,2-Dibromoethane (EDB)ug/L ND 0.50 09/30/20 22:07
1,2-Dichlorobenzene ug/L ND 0.50 09/30/20 22:07
1,2-Dichloroethane ug/L ND 0.50 09/30/20 22:07
1,2-Dichloropropane ug/L ND 0.50 09/30/20 22:07
1,3,5-Trimethylbenzene ug/L ND 0.50 09/30/20 22:07
1,3-Dichlorobenzene ug/L ND 0.50 09/30/20 22:07
1,3-Dichloropropane ug/L ND 0.50 09/30/20 22:07
1,4-Dichlorobenzene ug/L ND 0.50 09/30/20 22:07
2,2-Dichloropropane ug/L ND 0.50 09/30/20 22:07
2-Chlorotoluene ug/L ND 0.50 09/30/20 22:07
4-Chlorotoluene ug/L ND 0.50 09/30/20 22:07
Benzene ug/L ND 0.50 09/30/20 22:07
Bromobenzene ug/L ND 0.50 09/30/20 22:07
Bromochloromethane ug/L ND 0.50 09/30/20 22:07
Bromodichloromethane ug/L ND 0.50 09/30/20 22:07
Bromoform ug/L ND 0.50 09/30/20 22:07
Bromomethane ug/L ND 5.0 09/30/20 22:07
Carbon tetrachloride ug/L ND 0.50 09/30/20 22:07
Chlorobenzene ug/L ND 0.50 09/30/20 22:07
Chloroethane ug/L ND 1.0 09/30/20 22:07
Chloroform ug/L ND 0.50 09/30/20 22:07
Chloromethane ug/L ND 1.0 09/30/20 22:07
cis-1,2-Dichloroethene ug/L ND 0.50 09/30/20 22:07
cis-1,3-Dichloropropene ug/L ND 0.50 09/30/20 22:07
Dibromochloromethane ug/L ND 0.50 09/30/20 22:07
Dibromomethane ug/L ND 0.50 09/30/20 22:07
Dichlorodifluoromethane ug/L ND 0.50 09/30/20 22:07
Diisopropyl ether ug/L ND 0.50 09/30/20 22:07
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2020 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 58
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92497598
BP Service Center
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3020098
Associated Lab Samples:92497598002, 92497598005, 92497598010, 92497598011, 92497598014
Matrix:Water
Analyzed
Ethylbenzene ug/L ND 0.50 09/30/20 22:07
Hexachloro-1,3-butadiene ug/L ND 2.0 09/30/20 22:07
Isopropylbenzene (Cumene)ug/L ND 0.50 09/30/20 22:07
m&p-Xylene ug/L ND 1.0 09/30/20 22:07
Methyl-tert-butyl ether ug/L ND 0.50 09/30/20 22:07
Methylene Chloride ug/L ND 2.0 09/30/20 22:07
n-Butylbenzene ug/L ND 0.50 09/30/20 22:07
n-Propylbenzene ug/L ND 0.50 09/30/20 22:07
Naphthalene ug/L ND 2.0 09/30/20 22:07
o-Xylene ug/L ND 0.50 09/30/20 22:07
sec-Butylbenzene ug/L ND 0.50 09/30/20 22:07
Styrene ug/L ND 0.50 09/30/20 22:07
tert-Butylbenzene ug/L ND 0.50 09/30/20 22:07
Tetrachloroethene ug/L ND 0.50 09/30/20 22:07
Toluene ug/L ND 0.50 09/30/20 22:07
trans-1,2-Dichloroethene ug/L ND 0.50 09/30/20 22:07
trans-1,3-Dichloropropene ug/L ND 0.50 09/30/20 22:07
Trichloroethene ug/L ND 0.50 09/30/20 22:07
Trichlorofluoromethane ug/L ND 1.0 09/30/20 22:07
Vinyl chloride ug/L ND 1.0 09/30/20 22:07
1,2-Dichloroethane-d4 (S)%103 70-130 09/30/20 22:07
4-Bromofluorobenzene (S)%100 70-130 09/30/20 22:07
Toluene-d8 (S)%104 70-130 09/30/20 22:07
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3020099LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 52.450 105 60-140
1,1,1-Trichloroethane ug/L 52.450 105 60-140
1,1,2,2-Tetrachloroethane ug/L 51.550 103 60-140
1,1,2-Trichloroethane ug/L 51.350 103 60-140
1,1-Dichloroethane ug/L 50.550 101 60-140
1,1-Dichloroethene ug/L 54.050 108 60-140
1,1-Dichloropropene ug/L 52.450 105 60-140
1,2,3-Trichlorobenzene ug/L 50.750 101 60-140
1,2,3-Trichloropropane ug/L 49.250 98 60-140
1,2,4-Trichlorobenzene ug/L 50.050 100 60-140
1,2,4-Trimethylbenzene ug/L 44.550 89 60-140
1,2-Dibromo-3-chloropropane ug/L 50.350 101 60-140
1,2-Dibromoethane (EDB)ug/L 53.750 107 60-140
1,2-Dichlorobenzene ug/L 48.250 96 60-140
1,2-Dichloroethane ug/L 46.850 94 60-140
1,2-Dichloropropane ug/L 52.550 105 60-140
1,3,5-Trimethylbenzene ug/L 47.050 94 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2020 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 58
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92497598
BP Service Center
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3020099LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 46.150 92 60-140
1,3-Dichloropropane ug/L 52.650 105 60-140
1,4-Dichlorobenzene ug/L 49.850 100 60-140
2,2-Dichloropropane ug/L 50.750 101 60-140
2-Chlorotoluene ug/L 44.650 89 60-140
4-Chlorotoluene ug/L 47.350 95 60-140
Benzene ug/L 50.450 101 60-140
Bromobenzene ug/L 48.550 97 60-140
Bromochloromethane ug/L 53.350 107 60-140
Bromodichloromethane ug/L 48.250 96 60-140
Bromoform ug/L 57.250 114 60-140
Bromomethane ug/L 49.750 99 60-140
Carbon tetrachloride ug/L 51.850 104 60-140
Chlorobenzene ug/L 48.850 98 60-140
Chloroethane ug/L 45.150 90 60-140
Chloroform ug/L 51.050 102 60-140
Chloromethane ug/L 40.250 80 60-140
cis-1,2-Dichloroethene ug/L 50.650 101 60-140
cis-1,3-Dichloropropene ug/L 55.950 112 60-140
Dibromochloromethane ug/L 53.550 107 60-140
Dibromomethane ug/L 52.250 104 60-140
Dichlorodifluoromethane ug/L 40.750 81 60-140
Diisopropyl ether ug/L 49.550 99 60-140
Ethylbenzene ug/L 47.950 96 60-140
Hexachloro-1,3-butadiene ug/L 45.550 91 60-140
Isopropylbenzene (Cumene)ug/L 48.950 98 60-140
m&p-Xylene ug/L 96.0100 96 60-140
Methyl-tert-butyl ether ug/L 52.250 104 60-140
Methylene Chloride ug/L 50.750 101 60-140
n-Butylbenzene ug/L 46.150 92 60-140
n-Propylbenzene ug/L 45.050 90 60-140
Naphthalene ug/L 49.950 100 60-140
o-Xylene ug/L 48.850 98 60-140
sec-Butylbenzene ug/L 46.750 93 60-140
Styrene ug/L 51.350 103 60-140
tert-Butylbenzene ug/L 38.650 77 60-140
Tetrachloroethene ug/L 49.950 100 60-140
Toluene ug/L 46.850 94 60-140
trans-1,2-Dichloroethene ug/L 53.250 106 60-140
trans-1,3-Dichloropropene ug/L 54.450 109 60-140
Trichloroethene ug/L 53.150 106 60-140
Trichlorofluoromethane ug/L 42.050 84 60-140
Vinyl chloride ug/L 43.150 86 60-140
1,2-Dichloroethane-d4 (S)%96 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/02/2020 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 58
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92497598
BP Service Center
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3020100MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92497365003
3020101
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 200 105 60-14097 9 30200ND211193
1,1,1-Trichloroethane ug/L 200 119 60-140110 8 30200ND237219
1,1,2,2-Tetrachloroethane ug/L 200 109 60-140105 4 30200ND218210
1,1,2-Trichloroethane ug/L 200 109 60-140101 8 30200ND217201
1,1-Dichloroethane ug/L 200 115 60-140107 7 30200ND230214
1,1-Dichloroethene ug/L 200 128 60-140117 9 30200ND256234
1,1-Dichloropropene ug/L 200 121 60-140111 9 30200ND242221
1,2,3-Trichlorobenzene ug/L 200 84 60-14087 3 30200ND169175
1,2,3-Trichloropropane ug/L 200 106 60-140102 5 30200ND213203
1,2,4-Trichlorobenzene ug/L 200 83 60-14082 1 30200ND167165
1,2,4-Trimethylbenzene ug/L 200 80 60-14074 6 3020024.6 185 173
1,2-Dibromo-3-
chloropropane ug/L 200 110 60-140109 1 30200ND219218
1,2-Dibromoethane (EDB)ug/L 200 111 60-140106 5 30200ND223211
1,2-Dichlorobenzene ug/L 200 96 60-14089 8 30200ND192177
1,2-Dichloroethane ug/L 200 107 60-14097 9 30200ND213194
1,2-Dichloropropane ug/L 200 117 60-140106 10 30200ND234212
1,3,5-Trimethylbenzene ug/L 200 94 60-14089 6 30200ND187177
1,3-Dichlorobenzene ug/L 200 93 60-14087 6 30200ND186175
1,3-Dichloropropane ug/L 200 112 60-140103 8 30200ND224207
1,4-Dichlorobenzene ug/L 200 93 60-14091 3 30200ND186182
2,2-Dichloropropane ug/L 200 104 60-14096 8 30200ND209192
2-Chlorotoluene ug/L 200 92 60-14088 5 30200ND185175
4-Chlorotoluene ug/L 200 96 60-14087 10 30200ND191174
Benzene ug/L 200 114 60-140103 9 302006.7 234 213
Bromobenzene ug/L 200 98 60-14095 3 30200ND197190
Bromochloromethane ug/L 200 121 60-140112 8 30200ND243223
Bromodichloromethane ug/L 200 103 60-14095 8 30200ND206190
Bromoform ug/L 200 109 60-140103 5 30200ND218207
Bromomethane ug/L 200 68 60-14079 14 30200ND137158
Carbon tetrachloride ug/L 200 117 60-140107 9 30200ND235214
Chlorobenzene ug/L 200 104 60-14096 8 30200ND209193
Chloroethane ug/L 200 109 60-14098 10 30200ND218197
Chloroform ug/L 200 117 60-140105 10 30200ND233210
Chloromethane ug/L 200 90 60-14086 5 30200ND181172
cis-1,2-Dichloroethene ug/L 200 114 60-140106 8 30200ND229212
cis-1,3-Dichloropropene ug/L 200 115 60-140105 10 30200ND230209
Dibromochloromethane ug/L 200 108 60-140102 5 30200ND215205
Dibromomethane ug/L 200 120 60-140105 13 30200ND240210
Dichlorodifluoromethane ug/L 200 99 60-14091 9 30200ND198182
Diisopropyl ether ug/L 200 111 60-14099 10 3020035.1 257 234
Ethylbenzene ug/L 200 102 60-14093 9 302006.2 210 193
Hexachloro-1,3-butadiene ug/L 200 83 60-14078 7 30200ND167156
Isopropylbenzene(Cumene)ug/L 200 99 60-14091 8 302007.8 206 190
m&p-Xylene ug/L 400 102 60-14096 7 30400ND409382
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/02/2020 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 58
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92497598
BP Service Center
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3020100MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92497365003
3020101
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Methyl-tert-butyl ether ug/L 200 115 60-140105 9 302005.8 237 216
Methylene Chloride ug/L 200 116 60-140108 7 30200ND233216
n-Butylbenzene ug/L 200 85 60-14083 3 30200ND171166
n-Propylbenzene ug/L 200 91 60-14087 4 3020016.7 198 191
Naphthalene ug/L 200 85 60-14084 1 3020044.4 214 212
o-Xylene ug/L 200 101 60-14094 7 30200ND202187
sec-Butylbenzene ug/L 200 92 60-14090 2 30200ND184181
Styrene ug/L 200 106 60-14098 9 30200ND213195
tert-Butylbenzene ug/L 200 77 60-14076 1 30200ND154152
Tetrachloroethene ug/L 200 109 60-140102 6 30200ND218204
Toluene ug/L 200 107 60-14097 10 30200ND214193
trans-1,2-Dichloroethene ug/L 200 120 60-140108 10 30200ND240217
trans-1,3-Dichloropropene ug/L 200 108 60-140100 8 30200ND216200
Trichloroethene ug/L 200 119 60-140109 9 30200ND239217
Trichlorofluoromethane ug/L 200 103 60-14094 9 30200ND206188
Vinyl chloride ug/L 200 101 60-14094 8 30200ND203188
1,2-Dichloroethane-d4 (S)%105 70-130105
4-Bromofluorobenzene (S)%101 70-130100
Toluene-d8 (S)%101 70-130100
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/02/2020 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 58
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92497598
BP Service Center
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/02/2020 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 58
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92497598
BP Service Center
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92497598001 569694MW-1 SM 6200B
92497598002 570101MW-2 SM 6200B
92497598003 569694MW-3 SM 6200B
92497598004 569694MW-4 SM 6200B
92497598005 570101MW-7 SM 6200B
92497598006 569694MW-8A SM 6200B
92497598007 569694MW-9 SM 6200B
92497598008 569694MW-12 SM 6200B
92497598009 569694MW-13 SM 6200B
92497598010 570101MW-14 SM 6200B
92497598011 570101MW-15 SM 6200B
92497598012 569694MW-16 SM 6200B
92497598013 569694MW-17 SM 6200B
92497598014 570101MW-18 SM 6200B
92497598015 569694VEW-1 SM 6200B
92497598016 569694SW-1 SM 6200B
92497598017 569694IW-3 SM 6200B
92497598018 569694SW-8 SM 6200B
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/02/2020 12:21 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 58
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