WA-926_11963_CA_RPTS_20190320_MRP

EXECUTIVE SUMMARY

The Todd’s Service Center and Bowen’s Grocery sites are located at the intersection of US Highway 17
and NC Highway 45 in Merry Hill, Bertie County, North Carolina. According to available information,
two 2,000-gallon gasoline, one 1,000-gallon gasoline, one 1,000-gallon diesel and one 550-gallon waste
oil USTs were reportedly removed from the Todd’s site in December 1993. A release at the site was
discovered when petroleum impacted soil was encountered during the UST closure event. In addition,
two 550-gallon gasoline USTs were removed from the Bowen’s site in December 1994. Another UST
incident (UST Incident Number 31939; Miller’s Country Store) is located adjacent to the Todd’s and
Bowen’s sites and is considered to be commingled with the Todd’s and Bowen’s contaminant plume(s).

The risk classification of the sites is high due to the presence of two out of service water supply wells that
were identified within a 250-foot radius of the site. Municipal water is available to the site and
surrounding properties.

Twelve Type II monitoring wells (MW-1A, MW-2, MW-4, MW-5, MW-11, MW-15, MW-22, MW-26,
MW-29, MW-36, MW-43 and MW-44) were gauged, purged and sampled on February 20, 2018.
Concentrations of requested method constituents that exceeded the Maximum Allowable Concentrations
specified in T15A NCAC 2L.0202 were reported in the ground water samples collected from MW-1A,
MW-2, MW-4, MW-5, MW-11, MW-15, MW-22, MW-26 and MW-29. None of the requested method
constituents exceeded the Gross Contamination Levels.

Upon conclusion of the February 2019 sampling event, the existing Oxygen Releasing Compound (ORC-
A) socks were reinstalled in MW-1A, MW-2, MW4, MW-15, MW-22 and MW-29.

Since the initialization of the ORC-A socks in July 2018, contaminant concentrations have increased in
MW-1A, MW-2 and MW-4 by 46.25%, 368.79%, 16.57%, respectively, and have decreased in MW-15,
MW-22 and MW-29 by 45.35%, 66.76% and 45.71%, respectively.

Based on this information, the site should remain high risk. The effectiveness of the ORC-A socks has
yet to be determined. Continued monitoring and replacement of the ORC-A socks is recommended. The
next semi-annual ground water monitoring event is tentatively scheduled for October 2019; additionally
replacement ORC-A socks should be installed in April 2019.

TABLE OF CONTENTS

1.0 SITE HISTORY AND CHARACTERIZATION ....................................................................... 1
2.0 CURRENT SITE ASSESSMENT ................................................................................................ 2
3.0 GROUND WATER QUALITY .................................................................................................... 2
4.0 CONCLUSIONS AND RECOMMENDATIONS ....................................................................... 3
5.0 LIMITATIONS .............................................................................................................................. 4

FIGURES
Figure 1: Site Location Map
Figure 2: Site Map
Figure 3: Water Table Surface Map
Figure 4: Ground Water Quality Map

TABLES
Table 1: Well Construction and Gauging Information
Table 2: Summary of Ground Water Sample Analytical Results
Table 2A: Summary of Field Parameters Results

APPENDICES
Appendix A: Miller’s Country Store Ground Water Gauging and Sample Information
Appendix B: Laboratory Report - Ground Water Samples

1

1.0 SITE HISTORY AND CHARACTERIZATION
The former Todd’s Service Center and Bowen’s Grocery sites are located at the intersection of US
Highway 17 and NC Highway 45 in Merry Hill, Bertie County, North Carolina (Figure 1). The subject
sites are former petroleum retail facilities. A produce stand now operates at the site. According to
available information, two 2,000-gallon gasoline, one 1,000-gallon gasoline, one 1,000-gallon diesel and
one 550-gallon waste oil underground storage tanks (USTs) were reportedly removed from the Todd’s
site in December 1993. A release at the Todd’s site was discovered when petroleum impacted soil was
encountered during the UST closure event. According to available information, two 550-gallon gasoline
USTs were removed from the Bowen’s site in December 1994. Concentrations of requested method
constituents that exceeded the applicable soil quality standards were reported in two soil samples
collected from the UST pit bottom. Additionally, an incident at the adjacent Miller’s Country Store site
(UST Incident Number 31939) is considered to be commingled with the Todd’s and Bowen’s
contaminant plume(s). Monitoring and remediation efforts for the three sites are conducted concurrently
at the request of the North Carolina Department of Environmental Quality (NCDEQ).

A total of fifty-two Type II (MW-1 through MW-5, MW-7 through MW-15, MW-15A, MW-16 through
MW-48, RW-1, OW-1, AS-1 and VE-1) and one Type III (MWD-6) monitoring wells have been installed
during past assessment activities for the Todd’s and Bowen’s sites. In addition, three Type II (MW-1M,
MW-2M and MW-3M) and one Type III (TW-1M) monitoring wells have been installed on the adjacent
Miller’s Country Store site. Due to changing site conditions and activities, several monitoring wells have
been destroyed and/or replaced. Destroyed monitoring wells include MW-1, MW-8, MW-9, MW-10,
MW-16, MW-18, MW-18A, MW-23, MW-25, MW-25A, MW-30 and MW-35. Replacement wells MW-
1A, MW-9A, MW-10A, MW-15A, MW-23A, MW-25B and MW-30A were installed during past
assessment activities and remain onsite.

The site risk classification is currently ranked High due to the presence of two water supply wells within a
250-foot radius of the site; however, these wells are not in use. Municipal water is available to the site
and surrounding properties. A Site Map showing the locations of monitoring wells and site structures is
included as Figure 2.

Please note that site activities prior to January 2007 were performed by previous consultants. Although
Geological Resources Inc. (GRI) cannot verify the accuracy of this information, for the purpose of this
report, it is assumed to be correct. Any inferences or interpretations made by GRI based on data that may

2

be incorrect are not the responsibility of GRI. Please refer to earlier submittals for additional information
regarding past assessment activities.

2.0 CURRENT SITE ASSESSMENT
The purpose of this report is to present the results of ground water sampling activities conducted on
February 20, 2019, at the site. The activities were conducted in accordance with GRI proposal number
19-071 which was submitted to NCDEQ on January 30, 2019, and approved as Task Authorization No.
11963-24 on February 11, 2019. The purpose of the scope of work was to obtain current ground water
quality data for the site and assess the effectiveness of the Oxygen Releasing Compound (ORC-A) treated
socks installed at the site in July 2018.

3.0 GROUND WATER QUALITY
Twelve Type II monitoring wells (MW-1A, MW-2, MW-4, MW-5, MW-11, MW-15, MW-22, MW-26,
MW-29, MW-36, MW-43 and MW-44) were gauged, purged and sampled on February 20, 2018. Due to
heavy rainstorms, MW-23A was under water and inaccessible. Please note, monitoring wells associated
with the Miller’s Country Store site (MW-1M, MW-2M, MW-3M and TW-1M) were gauged, purged and
sampled in conjunction with the Todd’s and Bowen’s February 2019 sampling event. Ground water
gauging and sampling information for the Miller’s Grocery site are included as Appendix A.

The depths to ground water in the Type II monitoring wells during the February 2019 sampling event
ranged from 6.40 to 18.91 feet below the tops of well casings. Ground water elevations in the Type II
monitoring wells relative to a temporary benchmark assumed by the previous consultant ranged from
75.84 to 81.93 feet. Based on this information, ground water flow across the site was generally toward
the southeast. The average horizontal hydraulic gradient was less than 0.01 feet per foot. A Water Table
Surface Map for the February 20, 2019, gauging event has been included as Figure 3. A summary of the
well construction and gauging information has been presented in Table 1.

Laboratory analyses were performed on the ground water samples collected from the monitoring wells
during the February 2019 sampling event for volatile organic compounds using EPA Method 6200B.
Concentrations of one or more BTEX constituents, MTBE, naphthalene, o-chlorotoluene, 1,2-
dichloroethane, 1,2-dichloropropane, isopropylbenzene, n-propylbenzene, 1,2,4-trimethylbenzene and/or
1,3,5-trimethylbenzene that exceeded the Maximum Allowable Concentrations (MACs) specified in
T15A NCAC 2L.0202 were reported in the ground water samples collected from MW-1A, MW-2, MW-4,
MW-5, MW-11, MW-15, MW-22, MW-26 and MW-29. The concentration of benzene reported in the

3

ground water sample collected from MW-1A exceeded the Gross Contamination Level (GCL). A Ground
Water Quality Map based on data from the February 20, 2019, sampling event has been included as
Figure 4. A summary of ground water sample analytical results is presented in Table 2. A complete
laboratory report has been included as Appendix B.

Field parameter data (dissolved oxygen, temperature, pH, conductivity and oxygen reduction potential)
were collected during the February 2019 sampling for use in the evaluation of the ORC-A sock
application. Field parameter results are tabulate in Table 2A. Upon conclusion of the February 2019
sampling event, ORC-A socks were reinstalled in MW-1A, MW-2, MW4, MW-15, MW-22 and MW-29.

Upon conclusion of the February 2019 sampling event, ORC-A socks were reinstalled in MW-1A, MW-
2, MW-4, MW-15, MW-22 and MW-29. Since the initialization of the ORC-A socks in July 2018,
contaminant concentrations in MW-1A have increased by 46.25% (47,623 µg/l in July 2018 to 69,649
µg/l in February 2019); contaminant concentrations in MW-2 have increased by 368.79% (3,630 µg/l in
July 2018 to 17,017 µg/l in February 2019); contaminant concentrations in MW-4 have increased by
16.57% (24,123 µg/l in July 2018 to 28,119.2 µg/l in February 2019); contaminant concentrations in
MW-15 have been decreased by 45.35% (1,409.1 µg/l in July 2018 to 770.1 µg/l in February 2019) ;
contaminant concentrations in MW-22 have been decreased by 66.76% (1,933 µg/l in July 2018 to 642.5
µg/l in February 2019) ; contaminant concentrations in MW-29 have been decreased by 45.71% (3,885.7
µg/l in July 2018 to 2,109.5 µg/l in February 2019).

4.0 CONCLUSIONS AND RECOMMENDATIONS
 The average depth to ground water in the Type II monitoring wells in July 2018 was 17.35 feet
below the tops of well casings. Ground water flow was generally toward the southeast with an
average horizontal hydraulic gradient of less than 0.01 feet per foot.
 Concentrations of one or more BTEX constituents, MTBE, naphthalene, o-chlorotoluene, 1,2-
dichloroethane, 1,2-dichloropropane, isopropylbenzene, n-propylbenzene, 1,2,4-trimethylbenzene
and/or 1,3,5-trimethylbenzene that exceeded the MACs were reported in the ground water
samples collected from MW-1A, MW-2, MW-4, MW-5, MW-11, MW-15, MW-22, MW-26 and
MW-29. The concentration of benzene reported in the ground water sample collected from MW-
1A exceeded the GCL.
 Upon conclusion of the February 2019 sampling event, ORC-A treated socks were reinstalled in
MW-1A, MW-2, MW4, MW-15, MW-22 and MW-29.

4

 Since the initialization of the ORC-A socks in July 2018, contaminant concentrations have
increased in MW-1A, MW-2 and MW-4 by 46.25%, 368.79%, 16.57%, respectively, and have
decreased in MW-15, MW-22 and MW-29 by 45.35%, 66.76% and 45.71%, respectively.
 Based on this information, the site should remain high risk. The effectiveness of the ORC-A
socks has yet to be determined. Continued monitoring and replacement of the ORC-A socks is
recommended. The next semi-annual ground water monitoring event is tentatively scheduled for
October 2019; additionally replacement ORC-A socks should be installed in April 2019.

5.0 LIMITATIONS
This report has been prepared for the exclusive use of North East Oil Company, Inc. for specific
application to the referenced site in Bertie County, North Carolina. The assessment was conducted based
on the scope of work and level of effort desired by NCDEQ and with resources adequate only for that
scope of work. Our findings have been developed in accordance with generally accepted standards of
environmental practices in the State of North Carolina, available information, and our professional
judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would be
interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from this data. Please note that field data collected prior
to the March 2007 sampling and updated receptor survey event was not obtained under the supervision of
GRI. Although the accuracy of these data cannot be verified, for the purpose of this report GRI assumes
that they are correct.

FIGURES

TABLES
Date: 03/04/19
11/01/07
09/16/09
09/20/10
10/27/11
01/07/13
11/01/07 99.34 21.00 ---78.34
07/20/09 22.00 0.01 78.01 Pre-MMPE
07/24/09 21.25 ---78.75 Post-MMPE
09/16/09 21.57 ---78.43
09/20/10 19.92 ---80.08
10/27/11 19.90 ---80.10
12/03/12 21.45 ---78.55 Pre-MMPE
12/07/12 20.50 ---79.50 Post-MMPE
01/07/13 21.47 ---78.53
06/24/13 21.09 ---78.91 Pre-MMPE
06/28/13 21.19 ---78.81 Post-MMPE
07/29/13 NM NM NM Not Found
05/19/14 19.54 ---80.46 Pre-MMPE
05/23/14 19.45 ---80.55 Post-MMPE
06/23/14 19.68 ---80.32
07/06/15 NM NM NM Not Found
01/27/16 20.13 ---79.87
08/01/16 19.58 ---80.42 Pre-AFVR
08/01/16 19.91 ---80.09 Post-AFVR
09/07/16 20.29 ---79.71
07/24/18 19.91 ---80.09
02/20/19 18.91 ---81.09
11/01/07 99.51 20.92 ---78.59
07/20/09 21.07 ---78.79 Pre-MMPE
07/24/09 21.34 ---78.52 Post-MMPE
09/16/09 21.48 ---78.38
09/20/10 19.83 ---80.03
10/27/11 19.86 ---80.00
12/03/12 21.37 ---78.49 Pre-MMPE
12/07/12 21.42 ---78.44 Post-MMPE
01/07/13 21.40 ---78.46
06/24/13 20.91 ---78.95 Pre-MMPE
06/28/13 21.06 ---78.80 Post-MMPE
07/29/13 20.43 ---79.43
05/19/14 19.49 ---80.37 Pre-MMPE
05/23/14 19.44 ---80.42 Post-MMPE
06/23/14 19.62 ---80.24
06/01/15 18.39 ---81.47 Pre-MMPE
06/05/15 18.51 ---81.35 Post-MMPE
07/06/15 19.13 ---80.73
01/27/16 20.07 ---79.79
09/07/16 20.13 ---79.73
07/24/18 19.80 ---80.06
02/20/19 18.87 ---80.99
11/01/07 99.59 20.86 ---78.73
09/16/09 21.40 ---78.56
09/20/10 19.74 ---80.22
10/27/11 19.70 ---80.26
01/07/13 21.27 ---78.69
07/29/13 20.31 ---79.65
05/19/14 19.40 ---80.56 Pre-MMPE
05/23/14 19.29 ---80.67 Post-MMPE
06/03/14 19.47 ---80.49
06/01/15 18.22 ---81.74 Pre-MMPE
06/05/15 18.34 ---81.62 Post-MMPE
07/06/15 18.98 ---80.98
01/27/16 19.89 ---80.07
MW-3 04/27/94 15 15-25
MW-1A 11/16/01
99.96
Well
Casing
Depth
(ft. BGS)
25
Comments
Casing
Collapsed
Casing
Collapsed
Casing
Collapsed
Casing
Collapsed
Casing
Collapsed
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
TODD'S SERVICE STATION & BOWEN'S GROCERY (INCIDENT NOS. 11963 & 13592)
Facility ID #: 0-022807 & 0-022804
Well ID
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(ft.)
Free Product
Thickness
(ft.)
Groundwater
Elevation
(ft.)
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Bottom
of Well
(ft. BGS)
MW-1 04/27/94 15 15-25
Screened
Interval
(x to y ft.
BGS)
25
20 20-30 30 100.00
MW-2 04/27/94 15 15-25 25 99.86
Page 1 of 6
Date: 03/04/19
Well
Casing
Depth
(ft. BGS)
Comments
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
TODD'S SERVICE STATION & BOWEN'S GROCERY (INCIDENT NOS. 11963 & 13592)
Facility ID #: 0-022807 & 0-022804
Well ID
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(ft.)
Free Product
Thickness
(ft.)
Groundwater
Elevation
(ft.)
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Bottom
of Well
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
11/01/07 99.57 20.60 ---78.99
09/16/09 NM NM NM
09/20/10 19.47 ---80.10
10/27/11 19.40 ---80.17
12/03/12 21.00 ---78.57 Pre-MMPE
12/07/12 21.06 ---78.51 Post-MMPE
01/07/13 21.03 ---78.54
06/24/13 20.55 ---79.02 Pre-MMPE
06/28/13 20.67 ---78.90 Post-MMPE
07/29/13 NM NM NM Not Found
06/23/14 19.19 ---80.38
07/06/15 18.73 ---80.84
01/27/16 19.64 ---79.93
08/01/16 19.11 ---80.46 Pre-AFVR
08/01/16 19.30 ---80.27 Post-AFVR
09/07/16 19.74 ---79.83
07/24/18 19.42 ---80.15
02/20/19 18.45 ---81.12
11/01/07 99.19 20.29 ---78.90
09/16/09 20.85 ---78.72
09/20/10 19.17 ---80.40
10/27/11 19.10 ---80.47
01/07/13 20.70 ---78.87
07/29/13 19.76 ---79.81
05/19/14 18.69 ---80.88 Pre-MMPE
05/23/14 18.58 ---80.99 Post-MMPE
06/23/14 18.83 ---80.74
07/06/15 18.38 ---81.19
01/27/16 19.25 ---80.32
07/24/18 19.07 ---80.50
02/20/19 18.03 ---81.54
11/01/07 99.27 21.20 ---78.07
09/16/09 21.06 ---78.60
09/20/10 19.74 ---79.92
10/27/11 19.48 ---80.18
01/07/13 21.04 ---78.62
07/29/13 NM NM NM Not Found
06/23/14 NM NM NM Not Found
11/01/07 99.00 20.41 ---78.59
09/16/09 20.96 ---78.44
09/20/10 19.31 ---80.09
10/27/11 19.32 ---80.08
01/07/13 20.84 ---78.56
07/29/13 20.40 ---79.00
06/23/14 19.07 ---80.33
07/06/15 18.59 ---80.81
11/01/07 99.28 20.63 ---78.65
09/16/09 21.20 ---78.47
09/20/10 19.55 ---80.12
10/27/11 19.48 ---80.19
01/07/13 21.07 ---78.60
07/29/13 NM NM NM Not Found
06/23/14 19.25 ---80.42
07/06/15 18.78 ---80.89
11/01/07 99.11 20.45 ---78.66
09/16/09 21.22 ---78.31
09/20/10 19.58 ---79.95
10/27/11 19.55 ---79.98
01/07/13 21.10 ---78.43
07/29/13 20.12 ---79.41
06/23/14 19.30 ---80.23
07/06/15 18.82 ---80.71
11/01/07 98.11 19.73 ---78.38
09/16/09 20.29 ---78.07
09/20/10 18.65 ---79.71
10/27/11 18.68 ---79.68
01/07/13 20.20 ---78.16
07/29/13 19.23 ---79.13
06/23/14 18.36 ---80.00
07/06/15 18.00 ---80.36
01/27/16 18.90 ---79.46
09/07/16 18.47 ---79.89
02/20/19 17.72 ---80.64
25 99.67MW-9A 10/31/07 15 15-25
25 99.53MW-10A 10/31/07
18 18-28 28 98.36
44 99.66
MW-7 11/24/95 18 18-28 28 99.40
15-25
39-44
15
MWD-6 11/22/95 39
MW-4 04/27/94 15 15-25
MW-11 12/01/95
25 99.57
MW-5 04/27/94 15 15-25 25 99.57
Page 2 of 6
Date: 03/04/19
Well
Casing
Depth
(ft. BGS)
Comments
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
TODD'S SERVICE STATION & BOWEN'S GROCERY (INCIDENT NOS. 11963 & 13592)
Facility ID #: 0-022807 & 0-022804
Well ID
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(ft.)
Free Product
Thickness
(ft.)
Groundwater
Elevation
(ft.)
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Bottom
of Well
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
11/01/07 98.28 19.92 ---78.36
07/20/09 20.03 ---78.63 Pre-MMPE
07/24/09 20.21 ---78.45 Post-MMPE
09/16/09 20.48 ---78.18
09/20/10 18.75 ---79.91
10/27/11 18.87 ---79.79
12/03/12 20.39 ---78.27 Pre-MMPE
12/07/12 20.45 ---78.21 Post-MMPE
01/07/13 20.40 ---78.26
06/24/13 19.83 ---78.83 Pre-MMPE
06/28/13 19.95 ---78.71 Post-MMPE
07/29/13 19.46 ---79.20
05/19/14 18.51 ---80.15 Pre-MMPE
05/23/14 18.43 ---80.23 Post-MMPE
06/23/14 NM NM NM Not Found
09/07/16 NM NM NM Destroyed
11/01/07 98.23 19.85 ---78.38
09/16/09 20.40 ---78.20
09/20/10 18.77 ---79.83
10/27/11 18.81 ---79.79
01/07/13 20.30 ---78.30
07/29/13 19.40 ---79.20
06/23/14 NM NM NM Not Found
11/01/07 98.90 20.17 ---78.73
09/16/09 20.71 ---78.61
09/20/10 19.07 ---80.25
10/27/11 19.01 ---80.31
12/03/12 20.59 ---78.73 Pre-MMPE
12/07/12 20.66 ---78.66 Post-MMPE
01/07/13 20.60 ---78.72
06/24/13 20.11 ---79.21 Pre-MMPE
06/28/13 20.23 ---79.09 Post-MMPE
07/29/13 NM NM NM Not Found
06/23/14 NM NM NM Not Found
07/06/15 18.30 ---81.02
06/23/14 18.94 ---NM
01/27/16 19.34 ---NM
07/24/18 19.46 ---NM
02/20/19 18.24 ---NM
11/01/07 99.34 20.42 ---78.92
09/16/09 20.97 ---78.76
09/20/10 19.23 ---80.50
10/27/11 19.20 ---80.53
01/07/13 20.51 ---79.22
07/29/13 NM NM NM Not Found
05/19/14 18.80 ---80.93 Pre-MMPE
05/23/14 18.78 ---80.95 Post-MMPE
06/23/14 NM NM NM Not Found
02/20/19 NM NM NM Not Found
11/01/07 98.66 20.26 ---78.40
09/16/09 20.89 ---78.06
09/20/10 19.22 ---79.73
10/27/11 19.22 ---79.73
01/07/13 20.78 ---78.17
07/29/13 19.84 ---79.11
06/23/14 19.00 ---79.95
07/06/15 18.56 ---80.39
11/01/07 98.08 19.57 ---78.51
09/16/09 20.13 ---78.41
09/20/10 18.50 ---80.04
10/27/11 18.51 ---80.03
01/07/13 20.00 ---78.54
07/29/13 NM NM NM Not Found
06/23/14 NM NM NM Not Found
11/01/07 98.23 20.12 ---78.11
09/16/09 20.73 ---77.90
09/20/10 19.10 ---79.53
10/27/11 19.14 ---79.49
01/07/13 20.65 ---77.98
07/29/13 19.76 ---78.87
06/23/14 18.98 ---79.25
07/06/15 18.50 ---80.13
NM2818-281812/08/95MW-15
28 98.66
04/22/96 18 18-28 28 98.63
18-28 28 98.95
MW-19 04/22/96 18 18-28 28 98.54
98.60
MW-14 11/28/95 15 15-25 25 99.32
15 15-25 25
MW-12 12/01/95 18 18-28
MW-13 11/30/95
MW-17 04/19/96 18
MW-20
MW-15A 11/01/07 15 15-25 99.7325
Page 3 of 6
Date: 03/04/19
Well
Casing
Depth
(ft. BGS)
Comments
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
TODD'S SERVICE STATION & BOWEN'S GROCERY (INCIDENT NOS. 11963 & 13592)
Facility ID #: 0-022807 & 0-022804
Well ID
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(ft.)
Free Product
Thickness
(ft.)
Groundwater
Elevation
(ft.)
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Bottom
of Well
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
11/01/07 100.03 20.57 ---79.46
09/16/09 21.18 ---79.21
09/20/10 19.41 ---80.98
10/27/11 19.25 ---81.14
01/07/13 20.95 ---79.44
07/29/13 20.84 ---79.55
06/23/14 18.99 ---81.40
11/01/07 99.07 20.10 ---78.97
09/16/09 20.62 ---78.90
09/20/10 18.94 ---80.58
10/27/11 18.91 ---80.61
01/07/13 20.49 ---79.03
07/29/13 19.44 ---80.08
05/19/14 18.41 ---81.11 Pre-MMPE
05/23/14 18.62 ---80.90 Post-MMPE
06/23/14 18.61 ---80.91
06/01/15 17.35 ---82.17 Pre-MMPE
06/05/15 17.65 ---81.87 Post-MMPE
07/06/15 18.14 ---81.38
01/27/16 19.02 ---80.50
07/24/18 17.78 ---81.74
02/20/19 17.76 ---81.76
11/01/07 98.90 20.14 ---78.76
09/16/09 20.69 ---78.80
09/20/10 18.95 ---80.54
10/27/11 18.92 ---80.57
01/07/13 20.54 ---78.95
07/29/13 19.46 ---80.03
06/23/14 18.66 ---80.83
07/06/15 18.19 ---81.30
01/27/16 19.05 ---80.44
02/20/19 NM NM NM Under Water
11/01/07 99.41 20.10 ---79.31
09/16/09 20.69 ---79.12
09/20/10 NM NM NM
11/01/07 98.43 20.42 ---78.01
09/16/09 21.01 ---77.88
09/20/10 19.38 ---79.51
10/27/11 19.50 ---79.39
01/07/13 20.92 ---77.97
07/29/13 20.07 ---78.82
06/23/14 19.31 ---79.58
07/06/15 18.80 ---80.09
07/24/18 19.54 ---79.35
11/01/07 97.29 19.57 ---77.72
09/16/09 20.13 ---77.57
09/20/10 18.58 ---79.12
10/27/11 18.65 ---79.05
01/07/13 20.07 ---77.63
07/29/13 19.30 ---78.40
18.24 ---79.46 Pre-AFVR
18.30 ---79.40 Post-AFVR
06/23/14 18.52 ---79.18
06/01/15 17.40 ---80.30 Pre-AFVR
06/01/15 17.44 ---80.26 Post-AFVR
07/06/15 18.05 ---79.65
01/27/16 18.90 ---78.80
09/07/16 18.98 ---78.72
02/20/19 17.87 ---79.83
11/01/07 98.36 NM NM NM Well Dry
09/16/09 NM NM NM Well Dry
09/20/10 NM NM NM Well Dry
10/27/11 NM NM NM Well Dry
01/07/13 17.25 ---81.53
07/29/13 NM NM NM Well Dry
06/23/14 NM NM NM Well Dry
07/06/15 NM NM NM Well Dry
11/01/07 95.54 18.14 ---77.40
09/16/09 NM NM NM
09/20/10 NM NM NM
10/27/11 NM NM NM
10/04/12 20.92 ---74.62 Pre-AFVR
10/04/12 20.93 ---74.61 Post-AFVR
01/07/13 NM NM NM
06/23/14 NM NM NM
05/22/14
MW-28 10/15/98 22 22-32 32
8 8-18MW-27 10/03/96
28
28
MW-22 09/24/96 18
99.81MW-24 09/25/96
MW-21 09/24/96 18 18-28 100.39
95.54
97.7028
15-25
30 99.49
18
18 18-28
MW-23A 11/01/07 20 20-30
MW-26 09/25/96 18 18-28
251511/01/07MW-25B
98.78
18-28 28 99.52
98.89
Page 4 of 6
Date: 03/04/19
Well
Casing
Depth
(ft. BGS)
Comments
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
TODD'S SERVICE STATION & BOWEN'S GROCERY (INCIDENT NOS. 11963 & 13592)
Facility ID #: 0-022807 & 0-022804
Well ID
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(ft.)
Free Product
Thickness
(ft.)
Groundwater
Elevation
(ft.)
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Bottom
of Well
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
11/01/07 97.70 20.25 ---77.45
09/16/09 20.85 ---77.30
09/20/10 19.31 ---78.84
10/27/11 19.47 ---78.68
20.81 ---77.34 Pre-AFVR
20.82 ---77.33 Post-AFVR
01/07/13 20.77 ---77.38
20.52 ---77.63 Pre-AFVR
20.52 ---77.63 Post-AFVR
07/29/13 20.05 ---78.10
18.88 ---79.27 Pre-AFVR
19.05 ---79.10 Post-AFVR
06/23/14 19.32 ---78.83
06/01/15 18.23 ---79.92 Pre-AFVR
06/01/15 18.23 ---79.92 Post-AFVR
07/06/15 19.32 ---78.83
01/27/16 19.67 ---78.48
09/07/16 19.77 ---78.38
07/24/18 19.50 ---78.65
02/20/19 18.73 ---79.42
11/01/07 96.32 19.34 ---76.98
09/16/09 19.88 ---76.85
09/20/10 NM NM NM
11/01/07 97.86 20.37 ---77.49
09/16/09 20.96 ---77.28
09/20/10 19.42 ---78.82
10/27/11 19.51 ---78.73
01/07/13 20.83 ---77.41
07/29/13 19.14 ---79.10
06/23/14 19.39 ---78.85
07/06/15 18.97 ---79.27
11/01/07 97.64 19.30 ---78.34
09/16/09 19.87 ---78.47
09/20/10 NM NM NM
11/01/07 94.72 18.32 ---76.40
09/16/09 18.81 ---76.38
09/20/10 17.51 ---77.68
10/27/11 17.68 ---77.51
01/07/13 18.78 ---76.41
07/29/13 18.31 ---76.88
06/23/14 17.68 ---77.51
07/06/15 17.30 ---77.89
01/27/16 17.95 ---77.24
09/07/16 18.07 ---77.12
11/01/07 NA 6.53 ------
09/16/09 7.03 ---75.21
09/20/10 6.40 ---75.84
10/27/11 6.47 ---75.77
01/07/13 7.23 ---75.01
07/29/13 6.95 ---75.29
06/23/14 6.69 ---75.55
07/06/15 6.47 ---75.77
07/24/18 6.39 ---75.85
02/20/19 6.40 ---75.84
09/16/09 20.36 ---79.16
09/20/10 NM NM NM
09/16/09 17.58 ---75.75
09/20/10 16.50 ---76.83
10/27/11 16.64 ---76.69
01/07/13 17.67 ---75.66
07/29/13 17.17 ---76.16
06/23/14 16.68 ---76.65
07/06/15 16.35 ---76.98
09/16/09 19.54 ---78.77
09/20/10 NM NM NM
09/16/09 24.24 ---77.82
09/20/10 NM NM NM
09/20/10 19.42 ---81.20
10/27/11 19.19 ---81.43
01/07/13 20.99 ---79.63
06/23/14 18.94 ---81.68
19
95.193020-302011/07/01
98.34
03/10/03 10
05/22/14
MW-36
19-29
20-30
MW-41 09/16/10 10 10-25 25 100.62
MW-40 09/16/09 10 10-25 25 102.06
MW-39 09/16/09 10 10-25 25 98.31
99.52
MW-38 09/16/09 10 10-25 25 93.33
MW-33 11/07/01 20 30
MW-34
MW-37 09/01/09 10 10-25 25
MW-31 02/28/01 20 20-30
29 96.73
30 98.24
MW-30A 03/19/01
25
12/04/12
06/26/13
MW-29 10/15/98 25-35 35 98.15
10-25 25 82.24
Page 5 of 6
Date: 03/04/19
Well
Casing
Depth
(ft. BGS)
Comments
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
TODD'S SERVICE STATION & BOWEN'S GROCERY (INCIDENT NOS. 11963 & 13592)
Facility ID #: 0-022807 & 0-022804
Well ID
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(ft.)
Free Product
Thickness
(ft.)
Groundwater
Elevation
(ft.)
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Bottom
of Well
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
09/20/10 19.74 ---81.01
10/27/11 19.60 ---81.15
01/07/13 21.27 ---79.48
07/29/13 20.13 ---80.62
06/23/14 19.30 ---81.45
07/06/15 18.91 ---81.84
09/20/10 19.15 ---79.47
10/27/11 19.27 ---79.35
01/07/13 20.55 ---78.07
07/29/13 19.85 ---78.77
06/23/14 19.09 ---79.53
07/06/15 18.58 ---80.04
07/24/18 19.23 ---79.39
02/20/19 18.42 ---80.20
09/20/10 18.81 ---78.38
10/27/11 18.92 ---78.27
01/07/13 20.19 ---77.00
07/29/13 19.55 ---77.64
06/23/14 18.86 ---78.33
07/06/15 18.42 ---78.77
07/24/18 19.11 ---78.08
02/20/19 18.81 ---78.38
09/20/10 18.10 ---78.15
10/27/11 18.31 ---77.94
01/07/13 19.52 ---76.73
07/29/13 14.48 ---81.77
06/23/14 18.22 ---78.03
07/06/15 17.76 ---78.49
09/20/10 17.59 ---77.88
10/27/11 17.77 ---77.70
01/07/13 18.94 ---76.53
07/29/13 18.41 ---77.06
06/23/14 17.71 ---77.76
07/06/15 17.29 ---78.18
09/20/10 17.62 ---77.47
10/27/11 17.79 ---77.30
01/07/13 18.91 ---76.18
07/29/13 18.38 ---76.71
06/23/14 17.79 ---77.30
07/06/15 17.44 ---77.65
09/20/10 14.57 ---76.59
10/27/11 14.70 ---76.46
01/07/13 15.61 ---75.55
07/29/13 15.24 ---75.92
06/23/14 14.80 ---76.36
07/06/15 14.48 ---76.68
11/01/07 NA 20.89 ------
09/16/09 NM NM NM
09/20/10 NM NM NM
10/27/11 NM NM NM
01/07/13 NM NM NM
07/29/13 NM NM NM
06/23/14 NM NM NM
Notes:
• Reference point for elevation measurements: assumed elevation 100.00 ft.
• If free product is present in a well, groundwater elevation calculated by: [Top of Casing Elevation - Depth to Water] + [free product thickness
x 0.8581].
• ft BGS: feet below ground surface.
• NA: Data not available.
• Top-of-casing elevations and well construction information for monitoring wells installed prior to 2007 reproduced from previous assessment
reports prepared by CES Engineering, P. C.
• Monitoring wells MW-9A, MW-10A, MW-15A and MW-25B were resurveyed on August 12, 2008 by GRI personnel.
• Monitoring wells MW-41 through MW-48 were surveyed on September 17, 2010 by GRI personnel.
MW-44 09/15/10 10 10-25 25 97.19
10 10-25 25 98.62
MW-42
100.033010-301007/22/03RW-1
• NM: Not Measured.
10-25
10-25
25
25
MW-46 09/15/10 10 10-25
95.09
91.16
MW-47
MW-48
09/15/10
09/15/10
10
10
25 95.47
MW-45 09/15/10 10 10-25 25 96.25
09/16/10 10 10-25 25 100.75
MW-43 09/15/10
Page 6 of 6
Date : 03/04/19
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NE
10/31/07 10,100 23,700 1,570 9,290 648 286 33.1 16.0 <5.00 71.6 13.0 14.1 166 988 309 39.8 NR NR NR
09/17/09 2,110 8,190 552 2,660 814 <100 <36.0 <28.0 <48.0 <30.0 <40.0 <40.0 <44.0 313 73.9 J 10.1 2,510 2,080 2,990
09/20/10 9,050 29,400 2,100 11,000 8,740 <250 <250 <250 <120 111 J <100 <100 221 J 1,530 398 J 31.8 NR NR NR
10/27/11 14,400 39,900 2,940 14,200 3,320 391 J <100 <100 <100 133 J <110 <100 262 J 1,840 439 J NR NR NR NR
01/07/13 4,940 25,700 1,980 10,400 2,710 327 <10 <10 <10 74.1 <10 <10 195 1,390 354 NR NR NR NR
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/24/14 9,320 36,700 3,200 16,300 6,320 556 20.4 J 16.8 J <10 143 19.4 J <10 362 2,800 698 NR NR NR NR
07/06/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/27/16 7,300 37,800 2,610 12,700 5,880 502 <63 <63 <63 103 J <63 <63 274 1,850 449 NS NS NS NS
09/07/16 10,500 56,000 3,740 19,800 5,610 1,420 <130 <130 <130 142 J <130 <130 358 J 2,270 595 NR NR NR NR
07/24/18 3,460 28,200 2,360 11,600 1,520 483 <63 <63 <63 103 J <63 <63 239 J 1730 455 NR NR NR NR
02/20/19 5,560 38,600 3,190 16,200 5,550 549 <130 <130 <130 159 J <130 <130 337 J 2,480 704 NR NR NR NR
10/31/07 10,600 39,000 2,420 11,300 1,870 439 37.8 <10.0 <10.0 86.0 11.2 <10.0 175 1,230 356 23.0 NR NR NR
09/17/09 5,830 28,800 2,110 10,600 660 376 <45.0 1,080 <60.0 91.6 J <50.0 <50.0 161 J 1,270 289 29.9 5,000 3,150 4,860
09/20/10 4,680 12,000 1,210 5,650 7,310 137 <50.0 <50.0 <24.0 41.3 J <20.0 <20.0 66.8 J 525 140 116 NR NR NR
10/27/11 3,940 15,000 1,170 6,410 897 149 <20 <20 <21 33.0 J <21 <20 74.8 J 634 144 NR NR NR NR
01/07/13 0.67 3.7 0.41 J 1.70 0.35 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 0.16 J <0.10 NR NR NR NR
07/30/13 3,130 22,300 1,620 8,970 952 265 <10 <10 <10 43.4 J <10 <10 93.2 825 179 NR NR NR NR
06/24/14 1,450 8,130 752 4,340 769 157 1.5 J 1.5 J <1.0 24.0 3.6 J <1.0 51.7 434 96.0 NR NR NR NR
07/06/15 2,290 11,100 1,420 7,930 4,540 248 <36 <35 <35 42.6 J <40 <31 98.2 J 900 208 NR NR NR NR
01/27/16 <0.13 0.16 J <0.13 <0.31 2.7 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
09/07/16 1.9 21.5 3.8 12.7 1.7 0.96 <0.13 <0.13 <0.13 0.16 J <0.13 <0.13 0.56 1.4 0.35 J NR NR NR NR
07/24/18 135 2,150 230 1,050 27.8 37.2 <6.3 <6.3 <6.3 9.9 J <6.3 <6.3 23.1 J 173 45.1 NR NR NR NR
02/20/19 700 10,700 910 4,560 218 J 147 J <63 <63 <63 <63 <63 <63 66.1 J 518 146 J NR NR NR NR
02/28/07 15.0 <0.500 3.36 1.43 <0.500 15.5 0.880 0.870 <0.500 2.24 <0.500 0.710 1.57 2.38 <0.500 15.9 NR NR NR
10/31/07 59.1 0.930 14.6 7.97 <0.500 16.4 4.10 4.09 <0.500 11.3 <0.500 4.09 9.58 3.22 4.16 29.9 NR NR NR
09/17/09 20.1 <0.190 2.31 <0.220 <0.250 1.58 <0.180 0.970 J <0.240 2.65 <0.200 <0.200 1.39 0.883 J <0.180 7.05 106 <100 <100
09/20/10 13.7 2.15 0.606 J 1.85 J <0.500 3.61 <1.00 <1.00 <0.480 2.69 <0.400 <0.400 0.776 J 0.488 J <0.360 14.3 NR NR NR
10/27/11 8.4 0.22 J 0.89 1.1 J <0.13 1.8 <0.10 0.42 J <0.10 1.6 <0.11 <0.10 0.93 0.19 J <0.10 NR NR NR NR
01/07/13 0.74 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 0.11 J <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/24/14 1.0 <0.10 <0.10 0.55 J <0.10 <0.10 <0.10 0.14 J <0.10 0.22 J 0.11 J <0.10 0.28 J 0.36 J 0.15 J NR NR NR NR
07/06/15 2.9 <0.17 <0.15 0.62 J <0.16 0.98 0.35 J 0.59 <0.14 0.79 <0.16 <0.12 0.63 1.7 0.16 J NR NR NR NR
01/27/16 0.45 J <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NRBenzene1,2,4-TrimethylbenzeneNaphthaleneXylenes TABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
TODD’S SERVICE CENTER & BOWEN’S GROCERY (INCIDENT NOS. 11963 & 13592)TolueneIPEContaminant of
Concern
C9-C12 AliphaticsC5-C8 AliphaticsLeadn-ButylbenzeneFacility ID #s: 0-022807 & 0-022804
Analytical Method
C9-C10 AromaticsIsopropylbenzeneMADEP Method VPHEPA Method 6200B
sec-ButylbenzeneEthylbenzenep-IsopropyltolueneMW-3 1,3,5-Trimethylbenzenen-Propylbenzene1,2-DibromoethaneMTBEMW-1A
MW-2
MAC (mg/l)
GCL (mg/l)
Page 1 of 12
Date : 03/04/19
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NEBenzene1,2,4-TrimethylbenzeneNaphthaleneXylenes TABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
TODD’S SERVICE CENTER & BOWEN’S GROCERY (INCIDENT NOS. 11963 & 13592)TolueneIPEContaminant of
Concern
C9-C12 AliphaticsC5-C8 AliphaticsLeadn-ButylbenzeneFacility ID #s: 0-022807 & 0-022804
Analytical Method
C9-C10 AromaticsIsopropylbenzeneMADEP Method VPHEPA Method 6200B
sec-ButylbenzeneEthylbenzenep-Isopropyltoluene1,3,5-Trimethylbenzenen-Propylbenzene1,2-DibromoethaneMTBEMAC (mg/l)
GCL (mg/l)
09/20/10 1,500 45,000 9,170 53,400 309 J 2,870 1,830 <500 <240 852 J <200 <200 2,410 21,900 5,330 30.6 NR NR NR
10/27/11 1,700 33,200 6,290 33,500 2,880 1,180 201 J 120 J <100 457 J <110 <100 1,290 8,760 2,370 NR NR NR NR
01/07/13 509 19,500 4,620 24,300 737 960 58.1 43.7 J <10 249 <10 22.7 J 761 4,610 1,340 NR NR NR NR
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/24/14 894 19,200 4,580 27,300 1,170 858 471 269 <2.5 725 7.6 J 144 920 6,200 1,730 NR NR NR NR
07/06/15 381 14,200 4,810 28,600 620 1,440 98.9 J 59.1 J <35 264 <40 34.7 J 763 7,110 1,890 NR NR NR NR
01/27/16 349 24,200 12,200 68,400 1,810 3,360 879 465 <63 1,170 <63 240 J 4,190 22,100 7,640 NR NR NR NR
09/07/16 146 J 13,000 5,710 35,100 184 J 1,500 260 159 J <63 388 <63 66.9 J 1,320 9,470 2,940 NR NR NR NR
07/24/18 115 4,380 2,900 16,100 <25 628 58.8 J 43.1 J <25 195 <25 <25 550 4,250 1,200 NR NR NR NR
02/20/19 292 3,170 2,670 21,200 79.2 J 708 52.4 J 42.6 J <31 180 <31 <31 457 5,500 1,580 NR NR NR NR
10/31/07 1,120 5,620 1,490 4,130 <5.00 283 36.3 17.0 <5.00 82.5 <5.00 20.2 141 682 287 16.0 NR NR NR
09/17/09 274 2,280 666 1,810 <10.0 168 <7.20 <5.60 <9.60 58.6 <8.00 <8.00 64.8 392 124 12.9 2,770 2,250 1,480
09/20/10 568 1,780 630 2,340 <5.00 95.9 40.7 <10.0 11.5 J 38.0 <4.00 <4.00 52.1 539 160 19.6 NR NR NR
10/27/11 130 456 267 617 <0.13 47.9 3.2 2.4 1.8 26.0 <0.11 3.3 34.0 108 32.8 NR NR NR NR
01/07/13 590 4,770 1,400 5,120 <1.0 391 9.0 8.8 4.9 J 80.0 <1.0 11.9 132 804 248 NR NR NR NR
07/30/13 69.0 705 485 1,670 <2.0 216 6.1 J 5.8 J <2.0 40.2 <2.0 8.0 J 70.3 314 121 NR NR NR NR
06/24/14 14.8 38.1 12.3 79.1 <0.10 8.7 0.29 J 0.26 J 0.30 J 1.8 <0.10 0.39 J 2.2 9.2 4.1 NR NR NR NR
07/06/15 5.3 40.7 9.2 38.4 <0.16 2.0 <0.14 <0.14 <0.14 0.55 <0.16 <0.12 0.86 3.4 1.3 NR NR NR NR
01/27/16 185 1,690 631 2,060 <3.1 187 5.4 J 4.8 J <3.1 40.6 <3.1 6.0 J 63.2 336 111 NR NR NR NR
07/24/18 168 1,860 553 1,930 <6.3 92.2 <6.3 <6.3 <6.3 37.0 <6.3 <6.3 55.1 239 85.3 NR NR NR NR
02/20/19 9.6 104 28.2 129 <0.31 8.3 <0.31 <0.31 <0.31 1.7 <0.31 <0.31 2.7 14.9 5.1 NR NR NR NR
10/31/07 2.72 3.43 <0.500 1.17 6.10 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 NR NR NR
09/17/09 0.627 J 0.602 J <0.150 <0.220 0.868 J <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.200 <0.150 <0.180 <1.50 <100 <100 <100
09/20/10 <0.700 2.84 J 1.23 J 2.21 J <1.25 <2.50 <2.50 <2.50 <1.20 <0.750 <1.00 <1.00 <1.10 0.756 J <0.900 6.89 NR NR NR
10/27/11 <0.13 0.52 <0.15 0.56 J <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 0.38 J 0.46 J <0.10 0.21 J 0.59 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
10/31/07 36.9 <0.500 14.6 <1.00 <0.500 6.30 1.63 2.71 <0.500 7.20 1.53 3.14 6.78 <0.500 <0.500 <5.00 NR NR NR
09/17/09 10.3 0.366 J 179 3.61 <0.250 58.7 <0.180 7.46 <0.240 57.3 1.75 0.588 J 93.3 2.06 0.795 J <1.50 758 489 481
09/20/10 1.91 <0.190 <0.150 <0.220 <0.250 <0.500 <0.500 <0.500 <0.240 0.485 J <0.200 <0.200 <0.220 <0.150 <0.180 25.0 NR NR NR
10/27/11 3.7 0.30 J <0.15 <0.30 <0.13 0.53 <0.10 0.41 J <0.10 0.77 0.26 J <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 19.1 <0.10 13.1 <0.22 0.33 J 3.0 1.3 2.9 <0.10 12.5 0.90 1.5 19.2 <0.10 <0.10 NR NR NR NR
07/30/13 7.3 <0.10 7.0 <0.22 0.43 J 1.5 0.46 J 0.78 <0.10 4.7 0.78 0.34 J 7.2 <0.10 <0.10 NR NR NR NR
06/24/14 0.16 J <0.10 0.15 J <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 0.13 J <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
MW-7
MW-4
MW-5
MWD-6
Page 2 of 12
Date : 03/04/19
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NEBenzene1,2,4-TrimethylbenzeneNaphthaleneXylenes TABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
TODD’S SERVICE CENTER & BOWEN’S GROCERY (INCIDENT NOS. 11963 & 13592)TolueneIPEContaminant of
Concern
C9-C12 AliphaticsC5-C8 AliphaticsLeadn-ButylbenzeneFacility ID #s: 0-022807 & 0-022804
Analytical Method
C9-C10 AromaticsIsopropylbenzeneMADEP Method VPHEPA Method 6200B
sec-ButylbenzeneEthylbenzenep-Isopropyltoluene1,3,5-Trimethylbenzenen-Propylbenzene1,2-DibromoethaneMTBEMAC (mg/l)
GCL (mg/l)
11/01/07 0.930 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 17.7 NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 1.79 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 11.3 <100 <100 <100
09/20/10 0.284 J <0.190 <0.150 <0.220 <0.250 <0.500 <0.500 <0.500 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 35.1 NR NR NR
10/27/11 0.55 0.23 J <0.15 0.46 J <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 0.12 J <0.10 NR NR NR NR
01/07/13 2.9 <0.10 <0.10 <0.22 0.11 J <0.15 <0.10 0.13 J <0.10 0.11 J <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/24/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 16.7 NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 7.29 <100 <100 <100
09/20/10 0.475 J 2.95 0.384 J 1.90 <0.250 <0.500 <0.500 <0.500 <0.240 <0.150 <0.200 <0.200 <0.220 0.503 J <0.180 27.9 NR NR NR
10/27/11 <0.13 0.14 J <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 0.11 J <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/24/14 <0.10 <0.10 <0.10 <0.20 <0.10 0.19 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
10/31/07 617 191 366 652 52.0 132 9.58 4.13 <0.500 28.5 0.640 5.68 43.6 199 81.9 7.17 NR NR NR
09/17/09 1,560 3,120 687 1,920 43.6 J 208 <18.0 <14.0 <24.0 53.3 J <20.0 <20.0 52.5 J 316 88.1 J 12.5 3,150 1,430 1,870
09/20/10 29.2 1.68 0.400 J 13.3 11.1 3.56 <0.500 <0.500 <0.240 1.53 <0.200 <0.200 0.304 J 5.78 <0.180 25.6 NR NR NR
10/27/11 3.4 <0.13 <0.15 <0.30 1.2 0.37 J <0.10 <0.10 <0.10 0.11 J <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 324 E 97.6 114 188.9 121 44.3 1.2 1.5 0.38 J 12.3 0.83 1.6 18.7 55.5 11.3 NR NR NR NR
07/30/13 276 194 66.4 249 98.8 36.9 0.89 0.97 0.30 J 8.6 0.61 1.1 12.7 39.6 7.7 NR NR NR NR
06/24/14 152 20.5 11.5 89.9 29.3 21.9 0.40 J 0.37 J 0.29 J 3.2 <0.10 0.65 3.6 14.9 1.9 NR NR NR NR
07/06/15 33.8 0.38 J 6.5 12.8 7.6 16.0 0.28 J 0.25 J <0.14 1.7 <0.16 0.55 2.2 4.4 <0.14 NR NR NR NR
01/27/16 225 310 144 467 6.7 68.1 1.4 J <1.3 <1.3 11.0 <1.3 2.1 J 15.8 98.9 23.2 NR NR NR NR
09/07/16 27.7 29.5 16.8 32.3 0.25 J 7.1 <0.13 <0.13 <0.13 1.1 <0.13 <0.13 1.5 3.7 0.73 NR NR NR NR
02/20/19 1.3 1.5 1.2 2.5 <0.13 0.20 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 0.35 J 0.14 J NR NR NR NR
11/01/07 8,470 20,300 2,100 8,390 9,250 449 27.3 8.19 <0.500 76.3 46.0 6.75 154 1,280 420 18.8 NR NR NR
09/17/09 2,560 8,380 778 2,500 330 <100 <36.0 <28.0 <48.0 <30.0 <40.0 <40.0 88.1 J 552 141 J 3.22 2,630 1,700 2,360
09/20/10 1,500 517 260 764 845 76.3 7.59 J <5.00 <2.40 17.7 <2.00 <2.00 32.3 174 65.7 74.5 NR NR NR
10/27/11 3,120 9,080 895 4,130 2,990 128 <20 <20 <21 35.1 J <21 <20 83.9 J 613 160 NR NR NR NR
01/07/13 4,010 15,500 1,400 6,790 1,790 235 <10 <10 <10 52.3 <10 <10 146 1,080 241 NR NR NR NR
07/30/13 1,640 6,850 785 3,230 1,140 152 <25 <25 <25 32.5 J <25 <25 89.0 J 503 126 J NR NR NR NR
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
09/07/16 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
MW-10A
MW-12
MW-9A
MW-11
Page 3 of 12
Date : 03/04/19
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NEBenzene1,2,4-TrimethylbenzeneNaphthaleneXylenes TABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
TODD’S SERVICE CENTER & BOWEN’S GROCERY (INCIDENT NOS. 11963 & 13592)TolueneIPEContaminant of
Concern
C9-C12 AliphaticsC5-C8 AliphaticsLeadn-ButylbenzeneFacility ID #s: 0-022807 & 0-022804
Analytical Method
C9-C10 AromaticsIsopropylbenzeneMADEP Method VPHEPA Method 6200B
sec-ButylbenzeneEthylbenzenep-Isopropyltoluene1,3,5-Trimethylbenzenen-Propylbenzene1,2-DibromoethaneMTBEMAC (mg/l)
GCL (mg/l)
11/01/07 12.9 <0.500 2.65 <1.00 <0.500 <5.00 <0.500 2.06 <0.500 2.57 <0.500 <0.500 2.69 <0.500 <0.500 45.0 NR NR NR
09/17/09 8.77 <0.190 43.7 <0.220 <0.250 3.50 <0.180 3.19 <0.240 20.3 <0.200 0.454 J 26.4 <0.150 0.624 J 12.1 246 179 183
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.500 <0.500 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 42.1 NR NR NR
10/27/11 0.15 J 0.24 J <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 1.2 <0.10 0.11 J <0.22 <0.10 <0.15 <0.10 0.20 J <0.10 0.34 J <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 0.83 0.14 J <0.10 <0.22 <0.10 <0.15 <0.10 0.11 J <0.10 0.33 J <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
02/28/07 199 2.45 88.3 101 14.8 63.7 8.79 4.09 <0.500 26.8 <0.500 6.02 20.5 104 36.3 47.6 NR NR NR
10/31/07 212 11.4 280 185 8.98 144 17.4 6.66 <0.500 46.8 <0.500 10.2 54.8 87.4 90.8 12.4 NR NR NR
09/17/09 153 193 261 200 3.32 J 143 <1.80 <1.40 <2.40 22.5 <2.00 <2.00 20.7 62.4 21.5 13.6 1,100 504 506
09/20/10 64.5 6.39 68.7 41.7 <0.250 66.9 2.58 1.94 <0.240 16.6 <0.200 0.391 J 12.3 24.4 0.665 J 50.2 NR NR NR
10/27/11 183 5.0 148 12.2 12.3 78.6 2.7 3.8 <0.52 32.0 <0.54 3.5 23.3 5.0 0.66 J NR NR NR NR
01/07/13 144 170 228 237.8 9.5 135 3.2 3.4 <0.50 26.5 <0.50 2.8 25.6 50.2 10.5 NR NR NR NR
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/06/15 0.89 0.34 J 2.3 2.1 0.20 J 1.5 <0.14 <0.14 <0.14 0.24 J <0.16 <0.12 0.29 J 0.51 0.16 J NR NR NR NR
06/24/14 38.8 282 213 1,120 <0.10 120 4.9 4.3 <0.10 24.8 <0.10 7.2 31.5 224 74.6 NS NS NS NS
01/27/16 114 535 638 1,840 <3.1 250 9.5 J 8.5 J <3.1 64.4 <3.1 11.7 J 95.3 398 177 NS NS NS NS
07/24/18 41.8 249 229 808 <1.3 81.3 5.2 5.0 <1.3 26.5 <1.3 6.0 41.9 201 73.5 NR NR NR NR
02/20/19 44.7 130 156 392 <0.63 47.4 3.3 2.8 <0.63 20.1 <0.63 3.1 29.6 38.4 15.8 NR NR NR NR
11/01/07 358 1,690 1,320 3,240 <0.500 358 36.4 12.0 <0.500 81.5 <0.500 17.1 116 721 333 56.4 NR NR NR
09/17/09 78.6 1,030 513 1,680 <5.00 170 <3.60 <2.80 <4.80 45.4 <4.00 <4.00 44.3 360 112 9.16 2,640 1,100 1,460
09/20/10 551 756 542 1,570 <50.0 343 J <36.0 <28.0 <48.0 576 <40.0 <40.0 413 482 313 64.5 NR NR NR
10/27/11 151 534 458 1,230 <2.6 150 7.1 J 5.5 J <2.1 44.5 <2.1 8.0 J 64.9 287 130 NR NR NR NR
01/07/13 59.0 477 353 885 <2.0 125 5.3 J 5.5 J <2.0 35.9 <2.0 5.1 J 50.7 172 101 NR NR NR NR
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/24/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
02/20/19 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 55.2 NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 2.79 <100 <100 <100
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 1.83 <0.500 <0.500 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 15.5 NR NR NR
10/27/11 <0.13 0.22 J <0.15 0.36 J <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 0.11 J <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
MW-17
MW-15
MW-14
MW-13
MW-15A
Page 4 of 12
Date : 03/04/19
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NEBenzene1,2,4-TrimethylbenzeneNaphthaleneXylenes TABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
TODD’S SERVICE CENTER & BOWEN’S GROCERY (INCIDENT NOS. 11963 & 13592)TolueneIPEContaminant of
Concern
C9-C12 AliphaticsC5-C8 AliphaticsLeadn-ButylbenzeneFacility ID #s: 0-022807 & 0-022804
Analytical Method
C9-C10 AromaticsIsopropylbenzeneMADEP Method VPHEPA Method 6200B
sec-ButylbenzeneEthylbenzenep-Isopropyltoluene1,3,5-Trimethylbenzenen-Propylbenzene1,2-DibromoethaneMTBEMAC (mg/l)
GCL (mg/l)
11/01/07 6.58 1.13 10.5 3.33 4.88 25.9 6.63 4.30 <0.500 13.2 0.630 2.50 7.16 2.52 <0.500 45.3 NR NR NR
09/17/09 <0.140 <0.190 37.7 22.6 <0.250 66.2 <0.180 3.38 <0.240 34.8 <0.200 <0.200 41.2 116 47.4 14.6 243 394 505
09/20/10 0.917 J <0.190 <0.150 0.270 J 1.51 1.64 2.65 1.35 <0.240 1.15 <0.200 <0.200 <0.220 <0.150 <0.180 49.2 NR NR NR
10/27/11 <0.13 0.24 J <0.15 0.56 J <0.13 0.25 J <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 0.23 J <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 7.5 12.5 0.12 J 40.4 2.4 2.6 <0.10 16.7 <0.10 0.87 10.4 47.0 1.0 NR NR NR NR
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
02/28/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 13.0 NR NR NR
11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 16.5 NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 1.32 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 <1.50 <100 <100 <100
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.500 <0.500 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 14.3 NR NR NR
10/27/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
02/28/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 30.6 NR NR NR
11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 2.69 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 17.4 NR NR NR
09/17/09 11.1 0.398 J 1.69 11.3 <0.250 <0.500 <0.180 <0.140 <0.240 0.773 J <0.200 <0.200 0.749 J 3.69 1.81 5.70 429 105 <100
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <1.00 1.20 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 8.09 NR NR NR
10/27/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/29/13 <0.10 0.11 J <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
02/28/07 291 387 345 1,020 34.5 35.3 19.1 6.00 <0.500 33.2 29.4 4.95 75.2 523 115 18.1 NR NR NR
10/31/07 95.7 1,020 795 2,820 <2.50 155 46.4 16.6 <2.50 79.4 <2.50 13.4 224 1,190 373 <5.00 NR NR NR
09/17/09 78.9 J 2,270 1,900 8,570 <50.0 324 <36.0 <28.0 <48.0 156 J <40.0 <40.0 305 2,430 558 3.75 4,900 5,980 393,000
09/20/10 158 58.2 188 156 16.9 20.8 24.0 15.9 <2.40 30.9 30.5 <2.00 60.6 288 53.9 37.2 NR NR NR
10/27/11 69.3 301 487 1,730 <2.6 78.9 16.6 12.7 <2.1 61.0 4.2 J 9.4 J 190 955 267 NR NR NR NR
01/07/13 90.4 261 1,180 4,820 29.5 240 27.3 24.5 <2.0 172 12.4 16.0 542 3,480 828 NR NR NR NR
07/30/13 91.0 199 648 2,480 9.7 J 115 27.0 22.5 J <5.0 99.2 12.5 J 15.6 J 382 1,680 486 NR NR NR NR
06/23/14 8.6 5.3 34.6 111 <0.10 6.4 4.2 3.3 <0.10 8.5 0.73 2.6 28.5 67.8 20.7 NR NR NR NR
07/06/15 12.6 17.4 97.2 379 <0.82 20.3 7.1 4.9 <0.71 13.1 <0.80 3.7 46.3 211 60.0 NR NR NR NR
01/27/16 37.2 82.2 445 1,710 <3.1 106 22.2 16.4 <3.1 47.2 <3.1 12.0 J 159 878 218 NR NR NR NR
07/24/18 5.4 26.0 421 1,390 <1.3 90.6 16.6 12.7 <1.3 58.6 <1.3 8.5 165 954 241 NR NR NR NR
02/20/19 1.6 J 4.2 J 143 465 <1.3 25.7 6.2 6.5 <1.3 20.2 <1.3 4.4 J 59.80 316 76.2 NR NR NR NR
MW-20
MW-22
MW-19
MW-21
Page 5 of 12
Date : 03/04/19
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NEBenzene1,2,4-TrimethylbenzeneNaphthaleneXylenes TABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
TODD’S SERVICE CENTER & BOWEN’S GROCERY (INCIDENT NOS. 11963 & 13592)TolueneIPEContaminant of
Concern
C9-C12 AliphaticsC5-C8 AliphaticsLeadn-ButylbenzeneFacility ID #s: 0-022807 & 0-022804
Analytical Method
C9-C10 AromaticsIsopropylbenzeneMADEP Method VPHEPA Method 6200B
sec-ButylbenzeneEthylbenzenep-Isopropyltoluene1,3,5-Trimethylbenzenen-Propylbenzene1,2-DibromoethaneMTBEMAC (mg/l)
GCL (mg/l)
02/28/07 7.39 <0.500 4.73 7.21 <0.500 <5.00 <0.500 0.590 <0.500 1.88 <0.500 0.990 2.42 17.4 2.49 16.2 NR NR NR
10/31/07 3.32 <0.500 1.98 2.58 <0.500 <5.00 <0.500 <0.500 <0.500 1.53 <0.500 <0.500 0.810 6.75 1.27 16.4 NR NR NR
09/17/09 3.86 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 0.792 J <0.200 <0.200 0.387 J 3.64 <0.180 18.7 <100 <100 <100
09/20/10 14.2 0.242 J 2.39 9.05 <0.250 6.07 2.53 3.44 <0.240 6.40 <0.200 0.580 J 1.64 20.4 1.69 20.9 NR NR NR
10/27/11 7.0 0.22 J 3.7 3.1 <0.13 2.3 <0.10 0.61 <0.10 2.0 <0.11 0.95 1.8 6.8 <0.10 NR NR NR NR
01/07/13 1.7 <0.10 <0.10 0.28 J <0.10 0.41 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 0.96 <0.10 NR NR NR NR
07/30/13 12.3 0.15 J 4.1 5.5 <0.10 3.5 <0.10 1.4 <0.10 3.6 0.16 J 1.8 4.4 15.8 <0.10 NR NR NR NR
06/24/14 7.4 <0.10 3.1 3.0 <0.10 2.3 <0.10 0.83 <0.10 2.1 <0.10 1.1 2.4 8.6 0.14 J NR NR NR NR
07/06/15 22.0 0.47 J 11.7 19.8 <0.16 12.7 0.14 J 1.4 <0.14 4.7 <0.16 2.6 5.0 36.5 1.0 NR NR NR NR
01/27/16 1.1 <0.13 0.21 J <0.31 <0.13 0.46 J <0.13 <0.13 <0.13 0.18 J <0.13 <0.13 0.19 J 0.19 J <0.13 NR NR NR NR
02/20/19 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
02/28/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 13.1 NR NR NR
11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 17.0 NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 4.67 <100 <100 <100
10/27/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
11/01/07 61.5 95.7 46.1 75.8 5.64 12.2 2.94 2.03 <0.500 3.77 5.95 <0.500 7.17 20.6 7.97 32.3 NR NR NR
09/17/09 11.5 <0.190 <0.150 <0.220 10.7 5.35 <0.180 <0.140 <0.240 0.515 J 12.7 <0.200 <0.220 <0.150 <0.180 8.33 <100 <100 <100
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <1.00 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 26.8 NR NR NR
10/27/11 <0.13 0.15 J <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 0.49 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 0.57 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/24/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
07/24/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
MW-23A
MW-25B
MW-24
Page 6 of 12
Date : 03/04/19
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NEBenzene1,2,4-TrimethylbenzeneNaphthaleneXylenes TABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
TODD’S SERVICE CENTER & BOWEN’S GROCERY (INCIDENT NOS. 11963 & 13592)TolueneIPEContaminant of
Concern
C9-C12 AliphaticsC5-C8 AliphaticsLeadn-ButylbenzeneFacility ID #s: 0-022807 & 0-022804
Analytical Method
C9-C10 AromaticsIsopropylbenzeneMADEP Method VPHEPA Method 6200B
sec-ButylbenzeneEthylbenzenep-Isopropyltoluene1,3,5-Trimethylbenzenen-Propylbenzene1,2-DibromoethaneMTBEMAC (mg/l)
GCL (mg/l)
02/28/07 4,210 2,780 1,120 2,200 2,350 1,690 12.8 4.70 3.71 53.9 11.0 3.30 96.9 594 143 6.94 NR NR NR
11/01/07 4,130 2,880 1,150 2,220 1,720 190 14.9 6.23 1.65 47.7 9.05 4.76 89.0 509 139 21.6 NR NR NR
09/17/09 3,910 6,350 952 2,950 1,730 172 <18.0 <14.0 <24.0 50.3 J <20.0 <20.0 75.4 J 424 117 4.19 1,950 1,670 83,000
09/20/10 25.1 <0.190 0.827 J <0.220 96.2 0.957 J <0.500 <0.500 <0.240 0.313 J <0.200 <0.200 <0.220 <0.150 <0.180 45.3 NR NR NR
10/27/11 4.1 0.22 J 0.54 <0.30 4.2 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 257 102 77.0 149.9 147 13.3 <1.0 <1.0 <1.0 4.7 J <1.0 <1.0 10.3 47.7 9.2 NR NR NR NR
07/30/13 180 173 40.7 120 188 7.3 <0.10 0.15 J <0.10 2.1 0.44 J <0.10 3.3 10.1 2.2 NR NR NR NR
06/23/14 14.6 1.6 1.5 4.7 86.5 0.46 J <0.10 <0.10 <0.10 0.15 J 0.13 J <0.10 0.13 J 0.73 <0.10 NR NR NR NR
07/06/15 2.4 <0.17 0.22 J <0.43 12.1 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
01/27/16 9.0 8.3 1.6 5.9 26.4 0.50 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 0.51 <0.13 NR NR NR NR
09/07/16 0.31 J <0.13 <0.13 <0.31 5.5 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
02/20/19 24.6 23.0 6.3 24.1 30.6 0.95 <0.13 <0.13 <0.13 0.37 J <0.13 <0.13 0.36 J 1.7 0.43 J NR NR NR NR
02/28/07 <0.500 <0.500 <0.500 <1.00 3.29 <5.00 <0.500 <0.500 <0.500 <0.500 2.81 <0.500 <0.500 <0.500 <0.500 9.40 NR NR NR
10/27/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 19.6 NR NR NR
10/27/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
02/28/07 692 90.3 93.4 81.7 120 15.4 3.91 2.96 <0.500 28.0 1.04 1.25 15.0 16.7 5.44 6.88 NR NR NR
11/01/07 3,810 2,110 788 1,580 1,370 148 13.7 6.32 <0.500 40.9 9.59 5.45 67.8 364 92.0 40.5 NR NR NR
09/17/09 2,860 5,780 696 2,320 869 127 <18.0 <14.0 <24.0 37.8 J <20.0 <20.0 61.2 J 370 91.5 J <1.50 1,690 1,280 1,800
09/20/10 1,140 939 266 636 402 <100 <18.0 <14.0 <24.0 28.8 J <20.0 <20.0 37.3 J 156 36.4 J 13.4 NR NR NR
10/28/11 2,130 1,340 487 762 1,060 80.2 6.4 J <5.1 <5.2 32.1 5.9 J <5.0 50.0 236 25.9 NR NR NR NR
01/07/13 2,110 6,130 731 3,300 1,110 150 <5.0 <5.0 <5.0 31.2 <5.0 <5.0 74.5 551 138 NR NR NR NR
07/30/13 1,420 3,280 438 1,590 858 78.8 <10 <10 <10 20.2 J <10 <10 43.0 J 289 69.7 NR NR NR NR
06/23/14 508 2,480 268 1,070 319 67.2 2.6 2.2 <0.10 19.9 1.4 1.4 38.7 206 42.7 NR NR NR NR
07/06/15 525 1,780 317 1,290 157 90.1 <7.2 <6.9 <7.1 21.4 J <8.0 <6.1 35.0 270 65.7 NR NR NR NR
01/27/16 550 1,370 337 1,380 138 106 <3.1 <3.1 <3.1 20.7 <3.1 <3.1 33.0 315 70.5 NR NR NR NR
09/07/16 647 1,330 408 1,920 317 93.4 <6.3 <6.3 <6.3 25.0 <6.3 <6.3 39.5 309 79.9 NR NR NR NR
07/24/18 677 291 409 1,800 627 81.7 <3.1 <3.1 <3.1 20.3 <3.1 <3.1 39.3 312 75.5 NR NR NR NR
02/20/19 343 124 243 1,110 231 58.5 1.7 J 2.4 J <1.3 19.1 <1.3 1.5 J 21.6 167 42.3 NR NR NR NR
MW-29
MW-26
MW-27
MW-28
Page 7 of 12
Date : 03/04/19
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NEBenzene1,2,4-TrimethylbenzeneNaphthaleneXylenes TABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
TODD’S SERVICE CENTER & BOWEN’S GROCERY (INCIDENT NOS. 11963 & 13592)TolueneIPEContaminant of
Concern
C9-C12 AliphaticsC5-C8 AliphaticsLeadn-ButylbenzeneFacility ID #s: 0-022807 & 0-022804
Analytical Method
C9-C10 AromaticsIsopropylbenzeneMADEP Method VPHEPA Method 6200B
sec-ButylbenzeneEthylbenzenep-Isopropyltoluene1,3,5-Trimethylbenzenen-Propylbenzene1,2-DibromoethaneMTBEMAC (mg/l)
GCL (mg/l)
02/28/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 69.0 NR NR NR
11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 218 NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 28.4 <100 <100 <100
10/27/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
02/28/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 12.2 NR NR NR
11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0500 <0.500 <0.500 90.3 NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 13.9 <100 <100 <100
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.500 <0.500 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 27.6 NR NR NR
10/27/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 91.1 NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 35.8 <100 <100 <100
10/27/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
02/28/07 97.3 <0.500 <0.500 <1.00 50.9 <5.00 <0.500 <0.500 <0.500 1.13 <0.500 <0.500 <0.500 <0.500 <0.500 58.8 NR NR NR
11/01/07 146 <0.500 <0.500 <1.00 60.8 <5.00 <0.500 <0.500 <0.500 2.00 <0.500 <0.500 <0.500 <0.500 <0.500 165 NR NR NR
09/17/09 102 <0.190 <0.150 <0.220 32.2 <0.500 <0.180 <0.140 <0.240 1.10 <0.200 <0.200 <0.220 <0.150 0.525 J 12.5 <100 <100 <100
09/20/10 72.4 0.908 J 4.77 4.41 78.0 4.60 0.382 J 0.303 J <0.480 2.50 <0.400 <0.400 1.21 J <0.300 <0.360 40.4 NR NR NR
10/28/11 0.13 J 0.15 J <0.15 <0.30 1.9 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 0.12 J <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 3.4 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 11.7 J <10 <10 <22 451 <15 <10 <10 <10 <10 <10 <10 <10 <10 <10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 2.2 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 3.9 <0.17 0.17 J <0.43 5.1 0.45 J <0.14 <0.14 <0.14 0.17 J <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
01/27/16 <0.13 <0.13 <0.13 <0.31 0.32 J 0.25 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
09/07/16 <0.13 <0.13 <0.13 <0.31 1.5 <0.13 <0.13 <0.13 <0.13 <0.13 0.43 J <0.13 <0.13 <0.13 <0.13 NR NR NR NR
MW-31
MW-33
MW-30A
MW-34
Page 8 of 12
Date : 03/04/19
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NEBenzene1,2,4-TrimethylbenzeneNaphthaleneXylenes TABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
TODD’S SERVICE CENTER & BOWEN’S GROCERY (INCIDENT NOS. 11963 & 13592)TolueneIPEContaminant of
Concern
C9-C12 AliphaticsC5-C8 AliphaticsLeadn-ButylbenzeneFacility ID #s: 0-022807 & 0-022804
Analytical Method
C9-C10 AromaticsIsopropylbenzeneMADEP Method VPHEPA Method 6200B
sec-ButylbenzeneEthylbenzenep-Isopropyltoluene1,3,5-Trimethylbenzenen-Propylbenzene1,2-DibromoethaneMTBEMAC (mg/l)
GCL (mg/l)
03/01/07 <0.500 <0.500 <0.500 <1.00 2.36 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 28.4 NR NR NR
11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 19.0 NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 3.75 <100 <100 <100
09/20/10 <0.140 <0.190 <0.150 <0.220 0.410 J <1.00 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 24.6 NR NR NR
10/28/11 <0.13 <0.13 <0.15 <0.30 0.25 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
07/24/18 <0.13 <0.13 <0.13 <0.25 1.0 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
02/20/19 <0.13 0.16 J <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 20.3 <100 <100 <100
10/27/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
09/17/09 <0.140 <0.190 <0.150 <0.220 3.07 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 39.4 <100 <100 <100
09/20/10 <0.140 <0.190 <0.150 <0.220 0.794 J <1.00 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 77.4 NR NR NR
10/28/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 25.8 <100 <100 <100
10/27/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
09/17/09 <0.140 1.82 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 14.0 <100 <100 <100
10/27/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <1.00 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 0.327 J <0.180 100 <100 <100 <100
10/27/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
MW-41
MW-37
MW-39
MW-36
MW-40
MW-38
Page 9 of 12
Date : 03/04/19
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NEBenzene1,2,4-TrimethylbenzeneNaphthaleneXylenes TABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
TODD’S SERVICE CENTER & BOWEN’S GROCERY (INCIDENT NOS. 11963 & 13592)TolueneIPEContaminant of
Concern
C9-C12 AliphaticsC5-C8 AliphaticsLeadn-ButylbenzeneFacility ID #s: 0-022807 & 0-022804
Analytical Method
C9-C10 AromaticsIsopropylbenzeneMADEP Method VPHEPA Method 6200B
sec-ButylbenzeneEthylbenzenep-Isopropyltoluene1,3,5-Trimethylbenzenen-Propylbenzene1,2-DibromoethaneMTBEMAC (mg/l)
GCL (mg/l)
09/20/10 6.54 1.30 17.4 77.1 <0.250 1.43 J 3.24 0.680 J <0.240 1.85 <0.200 <0.200 4.04 25.8 9.18 80.2 1,450 431 665
10/27/11 10.7 1.3 1.5 11.0 0.15 J 0.12 J 0.14 J <0.10 <0.10 0.21 J <0.11 <0.10 0.29 J 1.6 2.1 NR NR NR NR
01/07/13 18.1 3.1 10.7 39.9 <0.10 <0.15 0.15 J 0.18 J <0.10 1.1 <0.10 0.12 J 2.0 7.7 5.1 NR NR NR NR
07/29/13 5.6 0.31 J 0.27 J 3.5 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 0.41 J 1.1 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <1.00 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 78.5 <100 <100 <100
10/27/11 <0.13 0.19 J <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 0.11 J <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/24/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
07/24/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
02/20/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
09/20/10 20.4 0.447 J 4.18 1.01 8.18 <1.00 <0.180 <0.140 <0.240 1.11 <0.200 <0.200 0.961 J <0.150 <0.180 104 <100 <100 <100
10/28/11 11.4 0.22 J <0.15 0.36 J 4.8 <0.10 <0.10 <0.10 <0.10 0.24 J <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 5.3 <0.10 0.11 J <0.22 4.6 <0.15 <0.10 <0.10 <0.10 0.11 J <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 46.7 0.25 J 2.7 <0.22 11.9 <0.15 0.13 J 0.13 J <0.10 1.1 <0.10 <0.10 0.60 <0.10 <0.10 NR NR NR NR
06/23/14 1.2 <0.10 <0.10 <0.20 2.4 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
07/24/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
02/20/19 0.14 J <0.13 <0.13 <0.25 0.41 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <1.00 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 229 <100 <100 <100
10/28/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
09/20/10 1.17 <0.190 <0.150 0.276 J 1.99 <1.00 <0.180 <0.140 <0.240 0.415 J 2.32 <0.200 <0.220 <0.150 <0.180 106 <100 <100 <100
10/28/11 <0.13 0.14 J <0.15 0.48 J <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 0.17 J <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 0.17 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 0.25 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 0.40 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
MW-42
MW-45
MW-46
MW-43
MW-44
Page 10 of 12
Date : 03/04/19
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NEBenzene1,2,4-TrimethylbenzeneNaphthaleneXylenes TABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
TODD’S SERVICE CENTER & BOWEN’S GROCERY (INCIDENT NOS. 11963 & 13592)TolueneIPEContaminant of
Concern
C9-C12 AliphaticsC5-C8 AliphaticsLeadn-ButylbenzeneFacility ID #s: 0-022807 & 0-022804
Analytical Method
C9-C10 AromaticsIsopropylbenzeneMADEP Method VPHEPA Method 6200B
sec-ButylbenzeneEthylbenzenep-Isopropyltoluene1,3,5-Trimethylbenzenen-Propylbenzene1,2-DibromoethaneMTBEMAC (mg/l)
GCL (mg/l)
09/20/10 26.6 <0.190 <0.150 <0.220 12.0 <1.00 0.201 J 0.177 J <0.240 1.43 <0.200 <0.200 <0.220 <0.150 <0.180 116 <100 <100 <100
10/28/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 101 <0.50 <0.50 <1.08 11.0 <0.74 <0.50 <0.50 <0.50 1.8 J <0.50 <0.50 <0.50 <0.50 <0.50 NR NR NR NR
07/30/13 12.9 <0.10 <0.10 <0.22 1.9 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
09/20/10 <0.140 <0.190 <0.150 <0.220 0.502 J <1.00 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 49.9 <100 <100 <100
10/28/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 0.96 <0.10 <0.10 <0.22 1.6 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 0.18 J <0.10 <0.10 <0.22 0.38 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 0.69 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 9.6 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
11/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 NR NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 NR NR NR NR
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.500 <0.500 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 3.45 NR NR NR
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <1.00 0.189 J <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 2.44 J NR NR NR
10/28/11 <0.13 0.14 J <0.15 <0.30 <0.13 0.11 J <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
01/27/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
WSW-13
WSW-5
MW-47
MW-48
Page 11 of 12
Date : 03/04/19
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NEBenzene1,2,4-TrimethylbenzeneNaphthaleneXylenes TABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
TODD’S SERVICE CENTER & BOWEN’S GROCERY (INCIDENT NOS. 11963 & 13592)TolueneIPEContaminant of
Concern
C9-C12 AliphaticsC5-C8 AliphaticsLeadn-ButylbenzeneFacility ID #s: 0-022807 & 0-022804
Analytical Method
C9-C10 AromaticsIsopropylbenzeneMADEP Method VPHEPA Method 6200B
sec-ButylbenzeneEthylbenzenep-Isopropyltoluene1,3,5-Trimethylbenzenen-Propylbenzene1,2-DibromoethaneMTBEMAC (mg/l)
GCL (mg/l)
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
Notes:
• Results reported in µg/l (micrograms per liter).
• NE: Standard not established.
• Concentrations in bold face type exceeded the MACs.
• J: Estimated value.
• E: Value exceeds calibration range.
• <: Less than the method detection limit specified in the laboratory report.
• NR: Analysis not requested.
• NS: Not sampled.
• Concentrations of o-chlorotoluene (190 µg/l in MW-4), 1,2-dichloroethane (0.97 J µg/l in MW-15A and 2.0 J µg/l in MW-29) and 1,2-dichloropropane (0.69 J µg/l in MW-15A and 2.3 J µg/l in MW-29) that exceeded the MACs
• For other compounds detected that did not exceed the MAC, please refer to the laboratory reports.
were reported in the ground water samples collected on Februray 20, 2019.
WSW-18
• MAC: Maximum allowable concentration as specified in T15A NCAC 2L.0202.
• GCL: Gross contamination level.
Page 12 of 12
Date: 02/20/19 Facility ID #: 0-022807 & 0-022804
Well
ID
Date
Collected
(mm/dd/yy)
DO
(mg/l)pH Temperature
(o C)
Conductivity
(mS/cm)
ORP
(mV)
07/24/18 1.16 5.51 19.80 125 30.0
02/20/19 31.37 NM 18.08 245 47.1
07/24/18 2.06 5.82 19.94 195 106.0
02/20/19 17.33 NM 18.06 212 46.4
07/24/18 0.46 4.70 19.82 59 97.8
02/20/19 12.68 NM 18.07 214 46.0
07/24/18 0.50 5.51 20.04 98 45.2
02/20/19 24.44 NM 17.66 282 48.2
07/24/18 1.85 5.44 20.41 91 69.6
02/20/19 22.02 NM 17.48 129.7 46.5
07/24/18 1.08 6.03 22.00 189 35.9
02/20/19 24.35 NM 16.80 331 44.9
Notes:
MW-4
MW-15
MW-22
MW-29
• NM: Not measured; insufficient water volume; malfunctioned meter.
TABLE 2A
SUMMARY OF FIELD PARAMETER MEASUREMENTS
TODD’S SERVICE CENTER & BOWEN’S GROCERY (INCIDENT NOS. 11963 & 13592)
MW-1A
MW-2
1 of 1

APPENDICES

APPENDIX A
Miller’s County Store Ground Water Gauging and Sample Information
Date: 03/05/19
09/20/10 19.38 ---80.81
10/27/11 19.19 ---81.00
01/07/13 20.76 ---79.43
07/29/13 19.85 ---80.34
06/23/14 18.92 ---81.27
07/06/15 18.28 ---81.91
01/27/16 18.85 ---81.34
09/07/16 19.25 ---80.94
07/24/18 18.78 ---81.41
02/20/19 19.83 ---80.36
09/17/09 21.10 ---79.01
09/20/10 19.38 ---80.73
10/27/11 19.34 ---80.77
01/07/13 20.93 ---79.18
07/29/13 19.66 ---80.45
05/19/14 18.88 ---81.23 Pre-MMPE
05/23/14 19.21 ---80.90 Post-MMPE
06/23/14 19.06 ---81.05
06/01/15 17.75 ---82.36 Pre-MMPE
06/05/15 18.09 ---82.02 Post-MMPE
07/06/15 18.58 ---81.53
01/27/16 19.40 ---80.71
09/07/16 19.63 ---80.48
07/24/18 19.22 ---80.89
02/20/19 18.18 ---81.93
09/20/10 18.73 ---80.49
10/27/11 18.73 ---80.49
01/07/13 NM NM NM
07/29/13 19.35 ---79.87
05/19/14 18.26 ---80.96 Pre-MMPE
05/23/14 18.45 ---80.77 Post-MMPE
06/23/14 18.43 ---80.79
07/06/15 17.93 ---81.29
01/27/16 18.83 ---80.39
09/07/16 19.03 ---80.19
07/24/18 18.63 ---80.59
02/20/19 17.52 ---81.70
09/20/10 18.60 ---80.40
10/27/11 18.59 ---80.41
01/07/13 20.17 ---78.83
07/29/13 20.17 ---78.83
05/19/14 18.15 ---80.85 Pre-MMPE
05/23/14 18.26 ---80.74 Post-MMPE
06/23/14 18.31 ---80.69
06/01/15 17.07 ---81.93 Pre-MMPE
06/05/15 17.47 ---81.53 Post-MMPE
07/06/15 17.84 ---81.16
01/27/16 18.75 ---80.25
09/07/16 18.91 ---80.09
07/24/18 18.54 ---80.46
02/20/19 17.49 ---81.51
Notes:
• Reference point for elevation measurements: assumed elevation 100.00 ft.
• If free product is present in a well, groundwater elevation calculated by: [Top of Casing Elevation - Depth to Water] + [free product thickness
x 0.8581].
• ft BGS: feet below ground surface.
• NA: Data not available.
• Top-of-casing elevations relative to assumed datum of 100.00 feet.
25 99.22
MW-3M 09/16/10 10 10-25 25 99.00
45 100.19
MW-1M 09/17/09 10 10-25 25 100.11
TW-1M 09/15/10
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
Facility ID #: 0-022895
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(ft.)
Free Product
Thickness
(ft.)
Groundwater
Elevation
(ft.)
Comments
40 40-45
MW-2M 09/16/10 10 10-25
• NM: Not Measured.
Page 1 of 1
Date : 03/04/19
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NE
09/20/10 4.95 4.15 4.89 18.1 <0.500 <2.00 2.10 <0.280 <0.480 5.78 <0.400 <0.400 4.07 2.60 2.52 3.41 <100 <100 <100
10/27/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/24/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <3.4 570 <3.0 <8.6 <3.3 <2.4 <2.9 <2.8 <2.8 <2.4 <3.2 <2.4 <3.1 <2.7 <2.7 NR NR NR NR
01/27/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
09/07/16 <0.13 47.9 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
07/24/18 <0.13 6.0 0.66 1.7 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 0.50 0.15 J NR NR NR NR
02/20/19 <0.13 1.5 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
09/17/09 1,310 36,100 4,070 22,700 211 J 1,060 <90.0 4,200 <120 265 J <100 642 642 4,900 1,170 4.26 12,200 10,700 15,500
09/20/10 1,130 11,900 1,410 6,210 <100 1,640 608 <56.0 <96.0 1,150 792 <80.0 896 2,850 964 45.3 NR NR NR
10/27/11 1,460 24,100 3,970 22,300 244 J 1,000 <100 <100 <100 263 J 226 J <100 763 5,320 1,430 NR NR NR NR
01/07/13 528 16,300 3,830 21,920 45.6 1,000 50.6 27.8 <5.0 186 73.1 18.5 J 589 4,520 1,090 NR NR NR NR
07/30/13 982 23,500 3,030 15,600 208 J 523 <50 <50 <50 110 J 220 J <50 344 2,400 582 NR NR NR NR
06/24/14 1,210 10,600 2,990 21,600 273 1,930 240 128 J <25 296 491 90.4 J 1,140 11,100 3,000 NR NR NR NR
07/06/15 975 17,100 3,150 20,300 <82 1,100 <72 <69 <71 140 J <80 <61 427 4,270 1,040 NR NR NR NR
01/27/16 466 15,200 3,460 22,000 <25 2,280 421 166 <25 373 <25 113 1,400 12,600 3,340 NR NR NR NR
09/07/16 716 22,000 5,560 36,000 <63 2,350 370 167 J <63 415 <63 90.4 J 1,530 12,000 3,570 NR NR NR NR
07/24/18 150 6,550 972 6,560 <31 320 <31 <31 <31 47.5 J <31 <31 137 1,490 420 NR NR NR NR
02/20/19 251 13,200 2,240 18,300 <31 904 <31 <31 <31 100 J 62.5 J <31 243 3,650 903 NR NR NR NR
09/20/10 5.49 4.12 4.89 17.7 3.04 2.27 J 15.7 <0.280 <0.480 5.70 3.73 <0.400 4.07 5.24 6.11 33.2 496 <100 380
10/27/11 <0.13 0.37 J 0.26 J 1.4 J <0.13 0.24 J 6.9 2.6 <0.10 1.6 <0.11 0.59 0.13 J 0.95 3.2 NR NR NR NR
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/30/13 <0.10 0.16 J 0.85 1.9 <0.10 0.99 5.8 2.7 <0.10 2.2 <0.10 0.81 0.27 J 5.9 9.6 NR NR NR NR
06/24/14 <0.10 <0.10 <0.10 <0.20 <0.10 0.34 J 0.91 0.40 J <0.10 <0.10 <0.10 0.25 J <0.10 0.32 J 0.34 J NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 2.5 0.92 <0.14 <0.12 <0.16 0.50 <0.16 <0.14 0.34 J NR NR NR NR
01/27/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 2.8 0.84 <0.13 <0.13 <0.13 0.27 J <0.13 <0.13 0.35 J NR NR NR NR
09/07/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 5.8 1.9 <0.13 <0.13 <0.13 0.26 J <0.13 <0.13 0.45 J NR NR NR NR
07/24/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 4.0 1.4 <0.13 <0.13 <0.13 0.47 J <0.13 <0.13 0.24 J NR NR NR NR
02/20/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 2.6 0.66 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
TABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
Facility ID #s: 0-022895
Analytical Method
EPA Method 6200B MADEP Method VPH
Contaminant of
Concern
BenzeneTolueneEthylbenzeneXylenesMTBELeadC5-C8 AliphaticsNaphthalenen-Butylbenzenesec-Butylbenzene1,2-DibromoethaneIsopropylbenzeneIPEC9-C12 AliphaticsC9-C10 AromaticsMAC (mg/l)
GCL (mg/l)p-Isopropyltoluenen-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneTW-1M
MW-1M
MW-2M
Page 1 of 2
Date : 03/04/19
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NE
TABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
Facility ID #s: 0-022895
Analytical Method
EPA Method 6200B MADEP Method VPH
Contaminant of
Concern
BenzeneTolueneEthylbenzeneXylenesMTBELeadC5-C8 AliphaticsNaphthalenen-Butylbenzenesec-Butylbenzene1,2-DibromoethaneIsopropylbenzeneIPEC9-C12 AliphaticsC9-C10 AromaticsMAC (mg/l)
GCL (mg/l)p-Isopropyltoluenen-Propylbenzene1,2,4-Trimethylbenzene1,3,5-Trimethylbenzene09/20/10 1,090 4,890 1,020 3,150 159 J 601 J 439 <56.0 <96.0 1,150 641 <80.0 829 1,030 606 28.8 25,900 5,280 16,900
10/27/11 1,430 12,300 1,610 6,600 158 352 <25 <26 <26 91.4 J 116 J <25 207 1,360 363 NR NR NR NR
01/07/13 1,120 13,500 1,670 7,150 54.8 312 <10 <10 <10 64.6 131 <10 192 1,390 319 NR NR NR NR
07/30/13 472 6,790 1,080 4,000 <25 171 <25 <25 <25 45.6 J 54.3 J <25 131 811 195 NR NR NR NR
06/24/14 161 2,150 288 1,290 12.6 J 37.2 <5.0 <5.0 <5.0 13.3 J 18.9 J <5.0 29.4 276 78.1 NR NR NR NR
07/06/15 220 4,690 564 2,660 <33 98.1 J <29 <28 <28 25.9 J <32 <24 65.3 J 503 134 NR NR NR NR
01/27/16 659 16,600 1,690 7,720 <25 425 <25 <25 <25 72.4 J 60.0 J <25 203 1,430 340 NR NR NR NR
09/07/16 524 17,500 1,970 9,400 <63 334 <63 <63 <63 82.1 J 81.3 J <63 220 J 1,330 363 NR NR NR NR
07/24/18 246 9,980 1,190 5,130 <25 177 <25 <25 <25 46.6 J <25 <25 125 894 237 NR NR NR NR
02/20/19 43.3 2,360 221 1,080 <6.3 35.8 <6.3 <6.3 <6.3 8.5 J <6.3 <6.3 19.8 J 112 26.1 NR NR NR NR
Notes:
• Results reported in µg/l (micrograms per liter).
• NE: Standard not established.
• Concentrations in bold face type exceeded the MACs.
• J: Estimated value.
• E: Value exceeds calibration range.
• <: Less than the method detection limit specified in the laboratory report.
• NR: Analysis not requested.
• NS: Not sampled.
• For other compounds detected that did not exceed the MAC, please refer to the laboratory reports.
• MAC: Maximum allowable concentration as specified in T15A NCAC 2L.0202.
• GCL: Gross contamination level.
MW-3M
Page 2 of 2
Date: 03/05/19 Facility ID #: 0-022895
Well
ID
Date
Collected
(mm/dd/yy)
DO
(mg/l)pH Temperature
(o C)
Conductivity
(mS/cm)
ORP
(mV)
07/24/18 1.98 5.34 19.92 111 99.8
02/20/19 19.39 NM 18.05 309 48.5
07/24/18 0.73 5.72 19.32 138 15.8
02/20/19 20.87 NM 17.15 118 46.5
07/24/18 3.92 7.69 21.34 87 111.1
02/20/19 38.56 NM 17.04 1,728 46.9
Notes:
• NM: Not measured; insufficient water volume; disfunctional meter.
TABLE 2A
SUMMARY OF FIELD PARAMETER MEASUREMENTS
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
MW-1M
MW-3M
TW-1M
1 of 1

APPENDIX B
Laboratory Report – Ground Water Samples

03/01/19
Technical Report for
GRI (Geological Resources Inc.)
Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
11963/2458
SGS Job Number: FA61814
Sampling Date: 02/20/19
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
[e-mail]; [e-mail];
[e-mail]
ATTN: Nicole Long
Total number of pages in report:
Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AK, AR, IA, KY, MA, MS, ND, NH, NV, OK, OR, UT, WA, WV
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone]
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Caitlin Brice, M.S.
General Manager
Orlando, FL 03/01/19
e-Hardcopy 2.0
Automated Report
48
SGS is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
Review standard terms at: http://www.sgs.com/en/terms-and-conditions
The results set forth herein are provided by SGS North America Inc.
Please share your ideas about
how we can serve you better at:
[e-mail]
1 of 48
FA61814
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................8
3.1: FA61814-1: MW-1A .....................................................................................................9
3.2: FA61814-2: MW-2 ........................................................................................................11
3.3: FA61814-3: MW-4 ........................................................................................................13
3.4: FA61814-4: MW-5 ........................................................................................................15
3.5: FA61814-5: MW-11 ......................................................................................................17
3.6: FA61814-6: MW-15A ...................................................................................................19
3.7: FA61814-7: MW-22 ......................................................................................................21
3.8: FA61814-8: MW-26 ......................................................................................................23
3.9: FA61814-9: MW-29 ......................................................................................................25
3.10: FA61814-10: MW-36 ..................................................................................................27
3.11: FA61814-11: MW-43 ..................................................................................................29
3.12: FA61814-12: MW-44 ..................................................................................................31
Section 4: Misc. Forms ............................................................................................................33
4.1: Chain of Custody ...........................................................................................................34
Section 5: MS Volatiles - QC Data Summaries .....................................................................36
5.1: Method Blank Summary ................................................................................................37
5.2: Blank Spike Summary ...................................................................................................41
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................45 123452 of 48
FA61814
SGS North America Inc.
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA61814
Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Project No: 11963/2458
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA61814-1 02/20/19 12:07 ER 02/22/19 AQ Water MW-1A
FA61814-2 02/20/19 12:19 ER 02/22/19 AQ Water MW-2
FA61814-3 02/20/19 12:30 ER 02/22/19 AQ Water MW-4
FA61814-4 02/20/19 14:47 ER 02/22/19 AQ Water MW-5
FA61814-5 02/20/19 14:36 ER 02/22/19 AQ Water MW-11
FA61814-6 02/20/19 11:52 ER 02/22/19 AQ Water MW-15A
FA61814-7 02/20/19 11:38 ER 02/22/19 AQ Water MW-22
FA61814-8 02/20/19 14:06 ER 02/22/19 AQ Water MW-26
FA61814-9 02/20/19 12:58 ER 02/22/19 AQ Water MW-29
FA61814-10 02/20/19 13:43 ER 02/22/19 AQ Water MW-36
FA61814-11 02/20/19 14:18 ER 02/22/19 AQ Water MW-43
FA61814-12 02/20/19 13:56 ER 02/22/19 AQ Water MW-44
3 of 48
FA618141
Summary of Hits Page 1 of 4
Job Number:FA61814
Account:GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Collected:02/20/19
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA61814-1 MW-1A
Benzene 5560 500 130 ug/l SM 6200B
Ethylbenzene 3190 500 130 ug/l SM 6200B
Isopropylbenzene 159 J 500 130 ug/l SM 6200B
Methyl Tert Butyl Ether 5550 500 130 ug/l SM 6200B
Naphthalene 549 500 130 ug/l SM 6200B
n-Propylbenzene 337 J 500 130 ug/l SM 6200B
Toluene 38600 500 130 ug/l SM 6200B
1,2,4-Trimethylbenzene 2480 500 130 ug/l SM 6200B
1,3,5-Trimethylbenzene 704 500 130 ug/l SM 6200B
m,p-Xylene 10600 1000 130 ug/l SM 6200B
o-Xylene 5650 500 130 ug/l SM 6200B
Xylene (total)16200 1500 250 ug/l SM 6200B
FA61814-2 MW-2
Benzene 700 250 63 ug/l SM 6200B
Ethylbenzene 910 250 63 ug/l SM 6200B
Methyl Tert Butyl Ether 218 J 250 63 ug/l SM 6200B
Naphthalene 147 J 250 63 ug/l SM 6200B
n-Propylbenzene 66.1 J 250 63 ug/l SM 6200B
Toluene 10700 250 63 ug/l SM 6200B
1,2,4-Trimethylbenzene 518 250 63 ug/l SM 6200B
1,3,5-Trimethylbenzene 146 J 250 63 ug/l SM 6200B
m,p-Xylene 2960 500 63 ug/l SM 6200B
o-Xylene 1590 250 63 ug/l SM 6200B
Xylene (total)4560 750 130 ug/l SM 6200B
FA61814-3 MW-4
Benzene 292 130 31 ug/l SM 6200B
n-Butylbenzene 52.4 J 130 31 ug/l SM 6200B
sec-Butylbenzene 42.6 J 130 31 ug/l SM 6200B
o-Chlorotoluene 190 130 31 ug/l SM 6200B
Ethylbenzene 2670 130 31 ug/l SM 6200B
Isopropylbenzene 180 130 31 ug/l SM 6200B
Methyl Tert Butyl Ether 79.2 J 130 31 ug/l SM 6200B
Naphthalene 708 130 31 ug/l SM 6200B
n-Propylbenzene 457 130 31 ug/l SM 6200B
Toluene 3170 130 31 ug/l SM 6200B
1,2,4-Trimethylbenzene 5500 130 31 ug/l SM 6200B
1,3,5-Trimethylbenzene 1580 130 31 ug/l SM 6200B
m,p-Xylene 14300 250 31 ug/l SM 6200B
o-Xylene 6970 130 31 ug/l SM 6200B
4 of 48
FA618142
Summary of Hits Page 2 of 4
Job Number:FA61814
Account:GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Collected:02/20/19
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
Xylene (total)21200 380 63 ug/l SM 6200B
FA61814-4 MW-5
Benzene 9.6 1.3 0.31 ug/l SM 6200B
o-Chlorotoluene 0.60 J 1.3 0.31 ug/l SM 6200B
Ethylbenzene 28.2 1.3 0.31 ug/l SM 6200B
Isopropylbenzene 1.7 1.3 0.31 ug/l SM 6200B
Naphthalene 8.3 1.3 0.31 ug/l SM 6200B
n-Propylbenzene 2.7 1.3 0.31 ug/l SM 6200B
Toluene 104 1.3 0.31 ug/l SM 6200B
1,2,4-Trimethylbenzene 14.9 1.3 0.31 ug/l SM 6200B
1,3,5-Trimethylbenzene 5.1 1.3 0.31 ug/l SM 6200B
m,p-Xylene 90.9 2.5 0.31 ug/l SM 6200B
o-Xylene 38.5 1.3 0.31 ug/l SM 6200B
Xylene (total)129 3.8 0.63 ug/l SM 6200B
FA61814-5 MW-11
Benzene 1.3 0.50 0.13 ug/l SM 6200B
Ethylbenzene 1.2 0.50 0.13 ug/l SM 6200B
Naphthalene 0.20 J 0.50 0.13 ug/l SM 6200B
Toluene 1.5 0.50 0.13 ug/l SM 6200B
1,2,4-Trimethylbenzene 0.35 J 0.50 0.13 ug/l SM 6200B
1,3,5-Trimethylbenzene 0.14 J 0.50 0.13 ug/l SM 6200B
m,p-Xylene 1.7 1.0 0.13 ug/l SM 6200B
o-Xylene 0.89 0.50 0.13 ug/l SM 6200B
Xylene (total)2.5 1.5 0.25 ug/l SM 6200B
FA61814-6 MW-15A
Benzene 44.7 2.5 0.63 ug/l SM 6200B
n-Butylbenzene 3.3 2.5 0.63 ug/l SM 6200B
sec-Butylbenzene 2.8 2.5 0.63 ug/l SM 6200B
tert-Butylbenzene 0.66 J 2.5 0.63 ug/l SM 6200B
o-Chlorotoluene 1.9 J 2.5 0.63 ug/l SM 6200B
1,2-Dichloroethane 0.97 J 2.5 0.63 ug/l SM 6200B
1,2-Dichloropropane 0.69 J 2.5 0.63 ug/l SM 6200B
Ethylbenzene 156 2.5 0.63 ug/l SM 6200B
Isopropylbenzene 20.1 2.5 0.63 ug/l SM 6200B
p-Isopropyltoluene 3.1 2.5 0.63 ug/l SM 6200B
Naphthalene 47.4 2.5 0.63 ug/l SM 6200B
n-Propylbenzene 29.6 2.5 0.63 ug/l SM 6200B
Toluene 130 2.5 0.63 ug/l SM 6200B
1,2,4-Trimethylbenzene 38.4 2.5 0.63 ug/l SM 6200B
5 of 48
FA618142
Summary of Hits Page 3 of 4
Job Number:FA61814
Account:GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Collected:02/20/19
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
1,3,5-Trimethylbenzene 15.8 2.5 0.63 ug/l SM 6200B
m,p-Xylene 267 5.0 0.63 ug/l SM 6200B
o-Xylene 125 2.5 0.63 ug/l SM 6200B
Xylene (total)392 7.5 1.3 ug/l SM 6200B
FA61814-7 MW-22
Benzene 1.6 J 5.0 1.3 ug/l SM 6200B
n-Butylbenzene 6.2 5.0 1.3 ug/l SM 6200B
sec-Butylbenzene 6.5 5.0 1.3 ug/l SM 6200B
o-Chlorotoluene 8.5 5.0 1.3 ug/l SM 6200B
Ethylbenzene 143 5.0 1.3 ug/l SM 6200B
Isopropylbenzene 20.2 5.0 1.3 ug/l SM 6200B
p-Isopropyltoluene 4.4 J 5.0 1.3 ug/l SM 6200B
Naphthalene 25.7 5.0 1.3 ug/l SM 6200B
n-Propylbenzene 59.8 5.0 1.3 ug/l SM 6200B
Toluene 4.2 J 5.0 1.3 ug/l SM 6200B
1,2,4-Trimethylbenzene 316 5.0 1.3 ug/l SM 6200B
1,3,5-Trimethylbenzene 76.2 5.0 1.3 ug/l SM 6200B
m,p-Xylene 433 10 1.3 ug/l SM 6200B
o-Xylene 31.5 5.0 1.3 ug/l SM 6200B
Xylene (total)465 15 2.5 ug/l SM 6200B
FA61814-8 MW-26
Benzene 24.6 0.50 0.13 ug/l SM 6200B
Ethylbenzene 6.3 0.50 0.13 ug/l SM 6200B
Isopropylbenzene 0.37 J 0.50 0.13 ug/l SM 6200B
Methyl Chloride 0.47 J 0.50 0.20 ug/l SM 6200B
Methyl Tert Butyl Ether 30.6 0.50 0.13 ug/l SM 6200B
Naphthalene 0.95 0.50 0.13 ug/l SM 6200B
n-Propylbenzene 0.36 J 0.50 0.13 ug/l SM 6200B
Toluene 23.0 0.50 0.13 ug/l SM 6200B
1,2,4-Trimethylbenzene 1.7 0.50 0.13 ug/l SM 6200B
1,3,5-Trimethylbenzene 0.43 J 0.50 0.13 ug/l SM 6200B
m,p-Xylene 16.2 1.0 0.13 ug/l SM 6200B
o-Xylene 7.9 0.50 0.13 ug/l SM 6200B
Xylene (total)24.1 1.5 0.25 ug/l SM 6200B
FA61814-9 MW-29
Benzene 343 5.0 1.3 ug/l SM 6200B
n-Butylbenzene 1.7 J 5.0 1.3 ug/l SM 6200B
sec-Butylbenzene 2.4 J 5.0 1.3 ug/l SM 6200B
o-Chlorotoluene 4.7 J 5.0 1.3 ug/l SM 6200B
6 of 48
FA618142
Summary of Hits Page 4 of 4
Job Number:FA61814
Account:GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Collected:02/20/19
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
1,2-Dichloroethane 2.0 J 5.0 1.3 ug/l SM 6200B
1,2-Dichloropropane 2.3 J 5.0 1.3 ug/l SM 6200B
Ethylbenzene 243 5.0 1.3 ug/l SM 6200B
Isopropylbenzene 19.1 5.0 1.3 ug/l SM 6200B
p-Isopropyltoluene 1.5 J 5.0 1.3 ug/l SM 6200B
Methyl Tert Butyl Ether 231 5.0 1.3 ug/l SM 6200B
Naphthalene 58.5 5.0 1.3 ug/l SM 6200B
n-Propylbenzene 21.6 5.0 1.3 ug/l SM 6200B
Toluene 124 5.0 1.3 ug/l SM 6200B
1,2,4-Trimethylbenzene 167 5.0 1.3 ug/l SM 6200B
1,3,5-Trimethylbenzene 42.3 5.0 1.3 ug/l SM 6200B
m,p-Xylene 746 10 1.3 ug/l SM 6200B
o-Xylene 361 5.0 1.3 ug/l SM 6200B
Xylene (total)1110 15 2.5 ug/l SM 6200B
FA61814-10 MW-36
Toluene 0.16 J 0.50 0.13 ug/l SM 6200B
FA61814-11 MW-43
No hits reported in this sample.
FA61814-12 MW-44
Benzene 0.14 J 0.50 0.13 ug/l SM 6200B
Methyl Tert Butyl Ether 0.41 J 0.50 0.13 ug/l SM 6200B
7 of 48
FA618142
SGS North America Inc.
Sample Results
Report of Analysis
Orlando, FL
Section 3
8 of 48
FA618143
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-1A
Lab Sample ID:FA61814-1 Date Sampled:02/20/19
Matrix:AQ - Water Date Received:02/22/19
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E098112.D 1000 02/27/19 12:14 AB n/a n/a VE2080
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 5560 500 130 ug/l
108-86-1 Bromobenzene ND 500 130 ug/l
74-97-5 Bromochloromethane ND 500 130 ug/l
75-27-4 Bromodichloromethane ND 500 130 ug/l
75-25-2 Bromoform ND 500 130 ug/l
104-51-8 n-Butylbenzene ND 500 130 ug/l
135-98-8 sec-Butylbenzene ND 500 130 ug/l
98-06-6 tert-Butylbenzene ND 500 130 ug/l
56-23-5 Carbon Tetrachloride ND 500 130 ug/l
108-90-7 Chlorobenzene ND 500 130 ug/l
75-00-3 Chloroethane a ND 500 200 ug/l
67-66-3 Chloroform ND 500 130 ug/l
95-49-8 o-Chlorotoluene ND 500 130 ug/l
106-43-4 p-Chlorotoluene ND 500 130 ug/l
124-48-1 Dibromochloromethane ND 500 130 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 500 250 ug/l
106-93-4 1,2-Dibromoethane ND 500 130 ug/l
75-71-8 Dichlorodifluoromethane b ND 500 200 ug/l
95-50-1 1,2-Dichlorobenzene ND 500 130 ug/l
541-73-1 1,3-Dichlorobenzene ND 500 130 ug/l
106-46-7 1,4-Dichlorobenzene ND 500 130 ug/l
75-34-3 1,1-Dichloroethane ND 500 130 ug/l
107-06-2 1,2-Dichloroethane ND 500 130 ug/l
75-35-4 1,1-Dichloroethylene ND 500 130 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 500 130 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 500 130 ug/l
78-87-5 1,2-Dichloropropane ND 500 130 ug/l
142-28-9 1,3-Dichloropropane ND 500 130 ug/l
594-20-7 2,2-Dichloropropane ND 500 130 ug/l
563-58-6 1,1-Dichloropropene ND 500 130 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 500 130 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 500 130 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
9 of 48
FA6181433.1
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-1A
Lab Sample ID:FA61814-1 Date Sampled:02/20/19
Matrix:AQ - Water Date Received:02/22/19
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 500 130 ug/l
100-41-4 Ethylbenzene 3190 500 130 ug/l
87-68-3 Hexachlorobutadiene ND 500 130 ug/l
98-82-8 Isopropylbenzene 159 500 130 ug/l J
99-87-6 p-Isopropyltoluene ND 500 130 ug/l
74-83-9 Methyl Bromide ND 500 200 ug/l
74-87-3 Methyl Chloride ND 500 200 ug/l
74-95-3 Methylene Bromide ND 500 130 ug/l
75-09-2 Methylene Chloride ND 2000 1000 ug/l
1634-04-4 Methyl Tert Butyl Ether 5550 500 130 ug/l
91-20-3 Naphthalene 549 500 130 ug/l
103-65-1 n-Propylbenzene 337 500 130 ug/l J
100-42-5 Styrene ND 500 130 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 500 130 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 500 130 ug/l
127-18-4 Tetrachloroethylene ND 500 130 ug/l
108-88-3 Toluene 38600 500 130 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 500 130 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 500 130 ug/l
71-55-6 1,1,1-Trichloroethane ND 500 130 ug/l
79-00-5 1,1,2-Trichloroethane ND 500 130 ug/l
79-01-6 Trichloroethylene ND 500 130 ug/l
75-69-4 Trichlorofluoromethane ND 500 200 ug/l
96-18-4 1,2,3-Trichloropropane ND 500 130 ug/l
95-63-6 1,2,4-Trimethylbenzene 2480 500 130 ug/l
108-67-8 1,3,5-Trimethylbenzene 704 500 130 ug/l
75-01-4 Vinyl Chloride ND 500 130 ug/l
m,p-Xylene 10600 1000 130 ug/l
95-47-6 o-Xylene 5650 500 130 ug/l
1330-20-7 Xylene (total)16200 1500 250 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 112%70-130%
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 103%70-130%
(a) Associated BS recovery outside control limits.
(b) Associated BS recovery outside control limits. Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 48
FA6181433.1
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-2
Lab Sample ID:FA61814-2 Date Sampled:02/20/19
Matrix:AQ - Water Date Received:02/22/19
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E098113.D 500 02/27/19 12:39 AB n/a n/a VE2080
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 700 250 63 ug/l
108-86-1 Bromobenzene ND 250 63 ug/l
74-97-5 Bromochloromethane ND 250 63 ug/l
75-27-4 Bromodichloromethane ND 250 63 ug/l
75-25-2 Bromoform ND 250 63 ug/l
104-51-8 n-Butylbenzene ND 250 63 ug/l
135-98-8 sec-Butylbenzene ND 250 63 ug/l
98-06-6 tert-Butylbenzene ND 250 63 ug/l
56-23-5 Carbon Tetrachloride ND 250 63 ug/l
108-90-7 Chlorobenzene ND 250 63 ug/l
75-00-3 Chloroethane a ND 250 100 ug/l
67-66-3 Chloroform ND 250 63 ug/l
95-49-8 o-Chlorotoluene ND 250 63 ug/l
106-43-4 p-Chlorotoluene ND 250 63 ug/l
124-48-1 Dibromochloromethane ND 250 63 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 250 120 ug/l
106-93-4 1,2-Dibromoethane ND 250 63 ug/l
75-71-8 Dichlorodifluoromethane b ND 250 100 ug/l
95-50-1 1,2-Dichlorobenzene ND 250 63 ug/l
541-73-1 1,3-Dichlorobenzene ND 250 63 ug/l
106-46-7 1,4-Dichlorobenzene ND 250 63 ug/l
75-34-3 1,1-Dichloroethane ND 250 63 ug/l
107-06-2 1,2-Dichloroethane ND 250 63 ug/l
75-35-4 1,1-Dichloroethylene ND 250 63 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 250 63 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 250 63 ug/l
78-87-5 1,2-Dichloropropane ND 250 63 ug/l
142-28-9 1,3-Dichloropropane ND 250 63 ug/l
594-20-7 2,2-Dichloropropane ND 250 63 ug/l
563-58-6 1,1-Dichloropropene ND 250 63 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 250 63 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 250 63 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 48
FA6181433.2
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-2
Lab Sample ID:FA61814-2 Date Sampled:02/20/19
Matrix:AQ - Water Date Received:02/22/19
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 250 63 ug/l
100-41-4 Ethylbenzene 910 250 63 ug/l
87-68-3 Hexachlorobutadiene ND 250 63 ug/l
98-82-8 Isopropylbenzene ND 250 63 ug/l
99-87-6 p-Isopropyltoluene ND 250 63 ug/l
74-83-9 Methyl Bromide ND 250 100 ug/l
74-87-3 Methyl Chloride ND 250 100 ug/l
74-95-3 Methylene Bromide ND 250 63 ug/l
75-09-2 Methylene Chloride ND 1000 500 ug/l
1634-04-4 Methyl Tert Butyl Ether 218 250 63 ug/l J
91-20-3 Naphthalene 147 250 63 ug/l J
103-65-1 n-Propylbenzene 66.1 250 63 ug/l J
100-42-5 Styrene ND 250 63 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 250 63 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 250 63 ug/l
127-18-4 Tetrachloroethylene ND 250 63 ug/l
108-88-3 Toluene 10700 250 63 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 250 63 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 250 63 ug/l
71-55-6 1,1,1-Trichloroethane ND 250 63 ug/l
79-00-5 1,1,2-Trichloroethane ND 250 63 ug/l
79-01-6 Trichloroethylene ND 250 63 ug/l
75-69-4 Trichlorofluoromethane ND 250 100 ug/l
96-18-4 1,2,3-Trichloropropane ND 250 63 ug/l
95-63-6 1,2,4-Trimethylbenzene 518 250 63 ug/l
108-67-8 1,3,5-Trimethylbenzene 146 250 63 ug/l J
75-01-4 Vinyl Chloride ND 250 63 ug/l
m,p-Xylene 2960 500 63 ug/l
95-47-6 o-Xylene 1590 250 63 ug/l
1330-20-7 Xylene (total)4560 750 130 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 112%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 104%70-130%
(a) Associated BS recovery outside control limits.
(b) Associated BS recovery outside control limits. Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 48
FA6181433.2
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-4
Lab Sample ID:FA61814-3 Date Sampled:02/20/19
Matrix:AQ - Water Date Received:02/22/19
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E098114.D 250 02/27/19 13:03 AB n/a n/a VE2080
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 292 130 31 ug/l
108-86-1 Bromobenzene ND 130 31 ug/l
74-97-5 Bromochloromethane ND 130 31 ug/l
75-27-4 Bromodichloromethane ND 130 31 ug/l
75-25-2 Bromoform ND 130 31 ug/l
104-51-8 n-Butylbenzene 52.4 130 31 ug/l J
135-98-8 sec-Butylbenzene 42.6 130 31 ug/l J
98-06-6 tert-Butylbenzene ND 130 31 ug/l
56-23-5 Carbon Tetrachloride ND 130 31 ug/l
108-90-7 Chlorobenzene ND 130 31 ug/l
75-00-3 Chloroethane a ND 130 50 ug/l
67-66-3 Chloroform ND 130 31 ug/l
95-49-8 o-Chlorotoluene 190 130 31 ug/l
106-43-4 p-Chlorotoluene ND 130 31 ug/l
124-48-1 Dibromochloromethane ND 130 31 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 130 62 ug/l
106-93-4 1,2-Dibromoethane ND 130 31 ug/l
75-71-8 Dichlorodifluoromethane b ND 130 50 ug/l
95-50-1 1,2-Dichlorobenzene ND 130 31 ug/l
541-73-1 1,3-Dichlorobenzene ND 130 31 ug/l
106-46-7 1,4-Dichlorobenzene ND 130 31 ug/l
75-34-3 1,1-Dichloroethane ND 130 31 ug/l
107-06-2 1,2-Dichloroethane ND 130 31 ug/l
75-35-4 1,1-Dichloroethylene ND 130 31 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 130 31 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 130 31 ug/l
78-87-5 1,2-Dichloropropane ND 130 31 ug/l
142-28-9 1,3-Dichloropropane ND 130 31 ug/l
594-20-7 2,2-Dichloropropane ND 130 31 ug/l
563-58-6 1,1-Dichloropropene ND 130 31 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 130 31 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 130 31 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
13 of 48
FA6181433.3
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-4
Lab Sample ID:FA61814-3 Date Sampled:02/20/19
Matrix:AQ - Water Date Received:02/22/19
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 130 31 ug/l
100-41-4 Ethylbenzene 2670 130 31 ug/l
87-68-3 Hexachlorobutadiene ND 130 31 ug/l
98-82-8 Isopropylbenzene 180 130 31 ug/l
99-87-6 p-Isopropyltoluene ND 130 31 ug/l
74-83-9 Methyl Bromide ND 130 50 ug/l
74-87-3 Methyl Chloride ND 130 50 ug/l
74-95-3 Methylene Bromide ND 130 31 ug/l
75-09-2 Methylene Chloride ND 500 250 ug/l
1634-04-4 Methyl Tert Butyl Ether 79.2 130 31 ug/l J
91-20-3 Naphthalene 708 130 31 ug/l
103-65-1 n-Propylbenzene 457 130 31 ug/l
100-42-5 Styrene ND 130 31 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 130 31 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 130 31 ug/l
127-18-4 Tetrachloroethylene ND 130 31 ug/l
108-88-3 Toluene 3170 130 31 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 130 31 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 130 31 ug/l
71-55-6 1,1,1-Trichloroethane ND 130 31 ug/l
79-00-5 1,1,2-Trichloroethane ND 130 31 ug/l
79-01-6 Trichloroethylene ND 130 31 ug/l
75-69-4 Trichlorofluoromethane ND 130 50 ug/l
96-18-4 1,2,3-Trichloropropane ND 130 31 ug/l
95-63-6 1,2,4-Trimethylbenzene 5500 130 31 ug/l
108-67-8 1,3,5-Trimethylbenzene 1580 130 31 ug/l
75-01-4 Vinyl Chloride ND 130 31 ug/l
m,p-Xylene 14300 250 31 ug/l
95-47-6 o-Xylene 6970 130 31 ug/l
1330-20-7 Xylene (total)21200 380 63 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 113%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 104%70-130%
(a) Associated BS recovery outside control limits.
(b) Associated BS recovery outside control limits. Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
14 of 48
FA6181433.3
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-5
Lab Sample ID:FA61814-4 Date Sampled:02/20/19
Matrix:AQ - Water Date Received:02/22/19
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0217231.D 2.5 02/28/19 11:56 AB n/a n/a VA2537
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 9.6 1.3 0.31 ug/l
108-86-1 Bromobenzene ND 1.3 0.31 ug/l
74-97-5 Bromochloromethane ND 1.3 0.31 ug/l
75-27-4 Bromodichloromethane ND 1.3 0.31 ug/l
75-25-2 Bromoform ND 1.3 0.31 ug/l
104-51-8 n-Butylbenzene ND 1.3 0.31 ug/l
135-98-8 sec-Butylbenzene ND 1.3 0.31 ug/l
98-06-6 tert-Butylbenzene ND 1.3 0.31 ug/l
56-23-5 Carbon Tetrachloride ND 1.3 0.31 ug/l
108-90-7 Chlorobenzene ND 1.3 0.31 ug/l
75-00-3 Chloroethane ND 1.3 0.50 ug/l
67-66-3 Chloroform ND 1.3 0.31 ug/l
95-49-8 o-Chlorotoluene 0.60 1.3 0.31 ug/l J
106-43-4 p-Chlorotoluene ND 1.3 0.31 ug/l
124-48-1 Dibromochloromethane ND 1.3 0.31 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 1.3 0.62 ug/l
106-93-4 1,2-Dibromoethane ND 1.3 0.31 ug/l
75-71-8 Dichlorodifluoromethane a ND 1.3 0.50 ug/l
95-50-1 1,2-Dichlorobenzene ND 1.3 0.31 ug/l
541-73-1 1,3-Dichlorobenzene ND 1.3 0.31 ug/l
106-46-7 1,4-Dichlorobenzene ND 1.3 0.31 ug/l
75-34-3 1,1-Dichloroethane ND 1.3 0.31 ug/l
107-06-2 1,2-Dichloroethane ND 1.3 0.31 ug/l
75-35-4 1,1-Dichloroethylene ND 1.3 0.31 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 1.3 0.31 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 1.3 0.31 ug/l
78-87-5 1,2-Dichloropropane ND 1.3 0.31 ug/l
142-28-9 1,3-Dichloropropane ND 1.3 0.31 ug/l
594-20-7 2,2-Dichloropropane ND 1.3 0.31 ug/l
563-58-6 1,1-Dichloropropene ND 1.3 0.31 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 1.3 0.31 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 1.3 0.31 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
15 of 48
FA6181433.4
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-5
Lab Sample ID:FA61814-4 Date Sampled:02/20/19
Matrix:AQ - Water Date Received:02/22/19
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 1.3 0.31 ug/l
100-41-4 Ethylbenzene 28.2 1.3 0.31 ug/l
87-68-3 Hexachlorobutadiene ND 1.3 0.31 ug/l
98-82-8 Isopropylbenzene 1.7 1.3 0.31 ug/l
99-87-6 p-Isopropyltoluene ND 1.3 0.31 ug/l
74-83-9 Methyl Bromide ND 1.3 0.50 ug/l
74-87-3 Methyl Chloride ND 1.3 0.50 ug/l
74-95-3 Methylene Bromide ND 1.3 0.31 ug/l
75-09-2 Methylene Chloride ND 5.0 2.5 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 1.3 0.31 ug/l
91-20-3 Naphthalene 8.3 1.3 0.31 ug/l
103-65-1 n-Propylbenzene 2.7 1.3 0.31 ug/l
100-42-5 Styrene ND 1.3 0.31 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 1.3 0.31 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 1.3 0.31 ug/l
127-18-4 Tetrachloroethylene ND 1.3 0.31 ug/l
108-88-3 Toluene 104 1.3 0.31 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 1.3 0.31 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 1.3 0.31 ug/l
71-55-6 1,1,1-Trichloroethane ND 1.3 0.31 ug/l
79-00-5 1,1,2-Trichloroethane ND 1.3 0.31 ug/l
79-01-6 Trichloroethylene ND 1.3 0.31 ug/l
75-69-4 Trichlorofluoromethane ND 1.3 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 1.3 0.31 ug/l
95-63-6 1,2,4-Trimethylbenzene 14.9 1.3 0.31 ug/l
108-67-8 1,3,5-Trimethylbenzene 5.1 1.3 0.31 ug/l
75-01-4 Vinyl Chloride ND 1.3 0.31 ug/l
m,p-Xylene 90.9 2.5 0.31 ug/l
95-47-6 o-Xylene 38.5 1.3 0.31 ug/l
1330-20-7 Xylene (total)129 3.8 0.63 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 109%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 97%70-130%
(a) Associated CCV and BS outside control limits high.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
16 of 48
FA6181433.4
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-11
Lab Sample ID:FA61814-5 Date Sampled:02/20/19
Matrix:AQ - Water Date Received:02/22/19
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E098111.D 1 02/27/19 11:50 AB n/a n/a VE2080
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 1.3 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane a ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane b ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
17 of 48
FA6181433.5
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-11
Lab Sample ID:FA61814-5 Date Sampled:02/20/19
Matrix:AQ - Water Date Received:02/22/19
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene 1.2 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene 0.20 0.50 0.13 ug/l J
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene 1.5 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 0.35 0.50 0.13 ug/l J
108-67-8 1,3,5-Trimethylbenzene 0.14 0.50 0.13 ug/l J
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 1.7 1.0 0.13 ug/l
95-47-6 o-Xylene 0.89 0.50 0.13 ug/l
1330-20-7 Xylene (total)2.5 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 110%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 104%70-130%
(a) Associated BS recovery outside control limits.
(b) Associated BS recovery outside control limits. Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
18 of 48
FA6181433.5
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-15A
Lab Sample ID:FA61814-6 Date Sampled:02/20/19
Matrix:AQ - Water Date Received:02/22/19
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0217232.D 5 02/28/19 12:19 AB n/a n/a VA2537
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 44.7 2.5 0.63 ug/l
108-86-1 Bromobenzene ND 2.5 0.63 ug/l
74-97-5 Bromochloromethane ND 2.5 0.63 ug/l
75-27-4 Bromodichloromethane ND 2.5 0.63 ug/l
75-25-2 Bromoform ND 2.5 0.63 ug/l
104-51-8 n-Butylbenzene 3.3 2.5 0.63 ug/l
135-98-8 sec-Butylbenzene 2.8 2.5 0.63 ug/l
98-06-6 tert-Butylbenzene 0.66 2.5 0.63 ug/l J
56-23-5 Carbon Tetrachloride ND 2.5 0.63 ug/l
108-90-7 Chlorobenzene ND 2.5 0.63 ug/l
75-00-3 Chloroethane ND 2.5 1.0 ug/l
67-66-3 Chloroform ND 2.5 0.63 ug/l
95-49-8 o-Chlorotoluene 1.9 2.5 0.63 ug/l J
106-43-4 p-Chlorotoluene ND 2.5 0.63 ug/l
124-48-1 Dibromochloromethane ND 2.5 0.63 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 2.5 1.2 ug/l
106-93-4 1,2-Dibromoethane ND 2.5 0.63 ug/l
75-71-8 Dichlorodifluoromethane a ND 2.5 1.0 ug/l
95-50-1 1,2-Dichlorobenzene ND 2.5 0.63 ug/l
541-73-1 1,3-Dichlorobenzene ND 2.5 0.63 ug/l
106-46-7 1,4-Dichlorobenzene ND 2.5 0.63 ug/l
75-34-3 1,1-Dichloroethane ND 2.5 0.63 ug/l
107-06-2 1,2-Dichloroethane 0.97 2.5 0.63 ug/l J
75-35-4 1,1-Dichloroethylene ND 2.5 0.63 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 2.5 0.63 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 2.5 0.63 ug/l
78-87-5 1,2-Dichloropropane 0.69 2.5 0.63 ug/l J
142-28-9 1,3-Dichloropropane ND 2.5 0.63 ug/l
594-20-7 2,2-Dichloropropane ND 2.5 0.63 ug/l
563-58-6 1,1-Dichloropropene ND 2.5 0.63 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 2.5 0.63 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 2.5 0.63 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
19 of 48
FA6181433.6
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-15A
Lab Sample ID:FA61814-6 Date Sampled:02/20/19
Matrix:AQ - Water Date Received:02/22/19
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 2.5 0.63 ug/l
100-41-4 Ethylbenzene 156 2.5 0.63 ug/l
87-68-3 Hexachlorobutadiene ND 2.5 0.63 ug/l
98-82-8 Isopropylbenzene 20.1 2.5 0.63 ug/l
99-87-6 p-Isopropyltoluene 3.1 2.5 0.63 ug/l
74-83-9 Methyl Bromide ND 2.5 1.0 ug/l
74-87-3 Methyl Chloride ND 2.5 1.0 ug/l
74-95-3 Methylene Bromide ND 2.5 0.63 ug/l
75-09-2 Methylene Chloride ND 10 5.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 2.5 0.63 ug/l
91-20-3 Naphthalene 47.4 2.5 0.63 ug/l
103-65-1 n-Propylbenzene 29.6 2.5 0.63 ug/l
100-42-5 Styrene ND 2.5 0.63 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 2.5 0.63 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 2.5 0.63 ug/l
127-18-4 Tetrachloroethylene ND 2.5 0.63 ug/l
108-88-3 Toluene 130 2.5 0.63 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 2.5 0.63 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 2.5 0.63 ug/l
71-55-6 1,1,1-Trichloroethane ND 2.5 0.63 ug/l
79-00-5 1,1,2-Trichloroethane ND 2.5 0.63 ug/l
79-01-6 Trichloroethylene ND 2.5 0.63 ug/l
75-69-4 Trichlorofluoromethane ND 2.5 1.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.5 0.63 ug/l
95-63-6 1,2,4-Trimethylbenzene 38.4 2.5 0.63 ug/l
108-67-8 1,3,5-Trimethylbenzene 15.8 2.5 0.63 ug/l
75-01-4 Vinyl Chloride ND 2.5 0.63 ug/l
m,p-Xylene 267 5.0 0.63 ug/l
95-47-6 o-Xylene 125 2.5 0.63 ug/l
1330-20-7 Xylene (total)392 7.5 1.3 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 108%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
(a) Associated CCV and BS outside control limits high.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
20 of 48
FA6181433.6
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-22
Lab Sample ID:FA61814-7 Date Sampled:02/20/19
Matrix:AQ - Water Date Received:02/22/19
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0217233.D 10 02/28/19 12:42 AB n/a n/a VA2537
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 1.6 5.0 1.3 ug/l J
108-86-1 Bromobenzene ND 5.0 1.3 ug/l
74-97-5 Bromochloromethane ND 5.0 1.3 ug/l
75-27-4 Bromodichloromethane ND 5.0 1.3 ug/l
75-25-2 Bromoform ND 5.0 1.3 ug/l
104-51-8 n-Butylbenzene 6.2 5.0 1.3 ug/l
135-98-8 sec-Butylbenzene 6.5 5.0 1.3 ug/l
98-06-6 tert-Butylbenzene ND 5.0 1.3 ug/l
56-23-5 Carbon Tetrachloride ND 5.0 1.3 ug/l
108-90-7 Chlorobenzene ND 5.0 1.3 ug/l
75-00-3 Chloroethane ND 5.0 2.0 ug/l
67-66-3 Chloroform ND 5.0 1.3 ug/l
95-49-8 o-Chlorotoluene 8.5 5.0 1.3 ug/l
106-43-4 p-Chlorotoluene ND 5.0 1.3 ug/l
124-48-1 Dibromochloromethane ND 5.0 1.3 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 5.0 2.5 ug/l
106-93-4 1,2-Dibromoethane ND 5.0 1.3 ug/l
75-71-8 Dichlorodifluoromethane a ND 5.0 2.0 ug/l
95-50-1 1,2-Dichlorobenzene ND 5.0 1.3 ug/l
541-73-1 1,3-Dichlorobenzene ND 5.0 1.3 ug/l
106-46-7 1,4-Dichlorobenzene ND 5.0 1.3 ug/l
75-34-3 1,1-Dichloroethane ND 5.0 1.3 ug/l
107-06-2 1,2-Dichloroethane ND 5.0 1.3 ug/l
75-35-4 1,1-Dichloroethylene ND 5.0 1.3 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.3 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.3 ug/l
78-87-5 1,2-Dichloropropane ND 5.0 1.3 ug/l
142-28-9 1,3-Dichloropropane ND 5.0 1.3 ug/l
594-20-7 2,2-Dichloropropane ND 5.0 1.3 ug/l
563-58-6 1,1-Dichloropropene ND 5.0 1.3 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.3 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.3 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
21 of 48
FA6181433.7
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-22
Lab Sample ID:FA61814-7 Date Sampled:02/20/19
Matrix:AQ - Water Date Received:02/22/19
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 5.0 1.3 ug/l
100-41-4 Ethylbenzene 143 5.0 1.3 ug/l
87-68-3 Hexachlorobutadiene ND 5.0 1.3 ug/l
98-82-8 Isopropylbenzene 20.2 5.0 1.3 ug/l
99-87-6 p-Isopropyltoluene 4.4 5.0 1.3 ug/l J
74-83-9 Methyl Bromide ND 5.0 2.0 ug/l
74-87-3 Methyl Chloride ND 5.0 2.0 ug/l
74-95-3 Methylene Bromide ND 5.0 1.3 ug/l
75-09-2 Methylene Chloride ND 20 10 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 5.0 1.3 ug/l
91-20-3 Naphthalene 25.7 5.0 1.3 ug/l
103-65-1 n-Propylbenzene 59.8 5.0 1.3 ug/l
100-42-5 Styrene ND 5.0 1.3 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 5.0 1.3 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 1.3 ug/l
127-18-4 Tetrachloroethylene ND 5.0 1.3 ug/l
108-88-3 Toluene 4.2 5.0 1.3 ug/l J
87-61-6 1,2,3-Trichlorobenzene ND 5.0 1.3 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.3 ug/l
71-55-6 1,1,1-Trichloroethane ND 5.0 1.3 ug/l
79-00-5 1,1,2-Trichloroethane ND 5.0 1.3 ug/l
79-01-6 Trichloroethylene ND 5.0 1.3 ug/l
75-69-4 Trichlorofluoromethane ND 5.0 2.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 5.0 1.3 ug/l
95-63-6 1,2,4-Trimethylbenzene 316 5.0 1.3 ug/l
108-67-8 1,3,5-Trimethylbenzene 76.2 5.0 1.3 ug/l
75-01-4 Vinyl Chloride ND 5.0 1.3 ug/l
m,p-Xylene 433 10 1.3 ug/l
95-47-6 o-Xylene 31.5 5.0 1.3 ug/l
1330-20-7 Xylene (total)465 15 2.5 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 105%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 97%70-130%
(a) Associated CCV and BS outside control limits high.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
22 of 48
FA6181433.7
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-26
Lab Sample ID:FA61814-8 Date Sampled:02/20/19
Matrix:AQ - Water Date Received:02/22/19
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E098118.D 1 02/27/19 14:40 AB n/a n/a VE2080
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 24.6 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane a ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane b ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
23 of 48
FA6181433.8
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-26
Lab Sample ID:FA61814-8 Date Sampled:02/20/19
Matrix:AQ - Water Date Received:02/22/19
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene 6.3 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene 0.37 0.50 0.13 ug/l J
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride 0.47 0.50 0.20 ug/l J
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 30.6 0.50 0.13 ug/l
91-20-3 Naphthalene 0.95 0.50 0.13 ug/l
103-65-1 n-Propylbenzene 0.36 0.50 0.13 ug/l J
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene 23.0 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 1.7 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene 0.43 0.50 0.13 ug/l J
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 16.2 1.0 0.13 ug/l
95-47-6 o-Xylene 7.9 0.50 0.13 ug/l
1330-20-7 Xylene (total)24.1 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 104%70-130%
17060-07-0 1,2-Dichloroethane-D4 116%70-130%
2037-26-5 Toluene-D8 94%70-130%
460-00-4 4-Bromofluorobenzene 104%70-130%
(a) Associated BS recovery outside control limits.
(b) Associated BS recovery outside control limits. Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
24 of 48
FA6181433.8
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-29
Lab Sample ID:FA61814-9 Date Sampled:02/20/19
Matrix:AQ - Water Date Received:02/22/19
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0217234.D 10 02/28/19 13:05 AB n/a n/a VA2537
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 343 5.0 1.3 ug/l
108-86-1 Bromobenzene ND 5.0 1.3 ug/l
74-97-5 Bromochloromethane ND 5.0 1.3 ug/l
75-27-4 Bromodichloromethane ND 5.0 1.3 ug/l
75-25-2 Bromoform ND 5.0 1.3 ug/l
104-51-8 n-Butylbenzene 1.7 5.0 1.3 ug/l J
135-98-8 sec-Butylbenzene 2.4 5.0 1.3 ug/l J
98-06-6 tert-Butylbenzene ND 5.0 1.3 ug/l
56-23-5 Carbon Tetrachloride ND 5.0 1.3 ug/l
108-90-7 Chlorobenzene ND 5.0 1.3 ug/l
75-00-3 Chloroethane ND 5.0 2.0 ug/l
67-66-3 Chloroform ND 5.0 1.3 ug/l
95-49-8 o-Chlorotoluene 4.7 5.0 1.3 ug/l J
106-43-4 p-Chlorotoluene ND 5.0 1.3 ug/l
124-48-1 Dibromochloromethane ND 5.0 1.3 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 5.0 2.5 ug/l
106-93-4 1,2-Dibromoethane ND 5.0 1.3 ug/l
75-71-8 Dichlorodifluoromethane a ND 5.0 2.0 ug/l
95-50-1 1,2-Dichlorobenzene ND 5.0 1.3 ug/l
541-73-1 1,3-Dichlorobenzene ND 5.0 1.3 ug/l
106-46-7 1,4-Dichlorobenzene ND 5.0 1.3 ug/l
75-34-3 1,1-Dichloroethane ND 5.0 1.3 ug/l
107-06-2 1,2-Dichloroethane 2.0 5.0 1.3 ug/l J
75-35-4 1,1-Dichloroethylene ND 5.0 1.3 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.3 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.3 ug/l
78-87-5 1,2-Dichloropropane 2.3 5.0 1.3 ug/l J
142-28-9 1,3-Dichloropropane ND 5.0 1.3 ug/l
594-20-7 2,2-Dichloropropane ND 5.0 1.3 ug/l
563-58-6 1,1-Dichloropropene ND 5.0 1.3 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.3 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.3 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
25 of 48
FA6181433.9
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-29
Lab Sample ID:FA61814-9 Date Sampled:02/20/19
Matrix:AQ - Water Date Received:02/22/19
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 5.0 1.3 ug/l
100-41-4 Ethylbenzene 243 5.0 1.3 ug/l
87-68-3 Hexachlorobutadiene ND 5.0 1.3 ug/l
98-82-8 Isopropylbenzene 19.1 5.0 1.3 ug/l
99-87-6 p-Isopropyltoluene 1.5 5.0 1.3 ug/l J
74-83-9 Methyl Bromide ND 5.0 2.0 ug/l
74-87-3 Methyl Chloride ND 5.0 2.0 ug/l
74-95-3 Methylene Bromide ND 5.0 1.3 ug/l
75-09-2 Methylene Chloride ND 20 10 ug/l
1634-04-4 Methyl Tert Butyl Ether 231 5.0 1.3 ug/l
91-20-3 Naphthalene 58.5 5.0 1.3 ug/l
103-65-1 n-Propylbenzene 21.6 5.0 1.3 ug/l
100-42-5 Styrene ND 5.0 1.3 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 5.0 1.3 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 1.3 ug/l
127-18-4 Tetrachloroethylene ND 5.0 1.3 ug/l
108-88-3 Toluene 124 5.0 1.3 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 5.0 1.3 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.3 ug/l
71-55-6 1,1,1-Trichloroethane ND 5.0 1.3 ug/l
79-00-5 1,1,2-Trichloroethane ND 5.0 1.3 ug/l
79-01-6 Trichloroethylene ND 5.0 1.3 ug/l
75-69-4 Trichlorofluoromethane ND 5.0 2.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 5.0 1.3 ug/l
95-63-6 1,2,4-Trimethylbenzene 167 5.0 1.3 ug/l
108-67-8 1,3,5-Trimethylbenzene 42.3 5.0 1.3 ug/l
75-01-4 Vinyl Chloride ND 5.0 1.3 ug/l
m,p-Xylene 746 10 1.3 ug/l
95-47-6 o-Xylene 361 5.0 1.3 ug/l
1330-20-7 Xylene (total)1110 15 2.5 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 105%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
(a) Associated CCV and BS outside control limits high.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
26 of 48
FA6181433.9
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-36
Lab Sample ID:FA61814-10 Date Sampled:02/20/19
Matrix:AQ - Water Date Received:02/22/19
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E098125.D 1 02/27/19 17:30 AB n/a n/a VE2080
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane a ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane b ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
27 of 48
FA6181433.10
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-36
Lab Sample ID:FA61814-10 Date Sampled:02/20/19
Matrix:AQ - Water Date Received:02/22/19
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene 0.16 0.50 0.13 ug/l J
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 106%70-130%
17060-07-0 1,2-Dichloroethane-D4 114%70-130%
2037-26-5 Toluene-D8 94%70-130%
460-00-4 4-Bromofluorobenzene 103%70-130%
(a) Associated BS recovery outside control limits.
(b) Associated BS recovery outside control limits. Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
28 of 48
FA6181433.10
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-43
Lab Sample ID:FA61814-11 Date Sampled:02/20/19
Matrix:AQ - Water Date Received:02/22/19
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0217228.D 1 02/28/19 10:47 AB n/a n/a VA2537
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane a ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
29 of 48
FA6181433.11
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-43
Lab Sample ID:FA61814-11 Date Sampled:02/20/19
Matrix:AQ - Water Date Received:02/22/19
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
(a) Associated CCV and BS outside control limits high.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
30 of 48
FA6181433.11
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-44
Lab Sample ID:FA61814-12 Date Sampled:02/20/19
Matrix:AQ - Water Date Received:02/22/19
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0217229.D 1 02/28/19 11:10 AB n/a n/a VA2537
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 0.14 0.50 0.13 ug/l J
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane a ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
31 of 48
FA6181433.12
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-44
Lab Sample ID:FA61814-12 Date Sampled:02/20/19
Matrix:AQ - Water Date Received:02/22/19
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.41 0.50 0.13 ug/l J
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 104%70-130%
17060-07-0 1,2-Dichloroethane-D4 107%70-130%
2037-26-5 Toluene-D8 96%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
(a) Associated CCV and BS outside control limits high.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
32 of 48
FA6181433.12
SGS North America Inc.
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Orlando, FL
Section 4
33 of 48
FA618144
FA61814: Chain of Custody
Page 1 of 2
34 of 48
FA6181444.1
Job Number:FA61814 Client:GRI
Date / Time Received:2/22/2019 9:30:00 AM Delivery Method:FED EX
Project:2458
Airbill #'s:1015906913160003281100812575721450
Cooler Information
1. Custody Seals Present
2. Custody Seals Intact
4. Cooler temp verification
3. Temp criteria achieved
5. Cooler media
IR Gun
Ice (Bag)
Trip Blank Information
1. Trip Blank present / cooler
2. Trip Blank listed on COC
2. Samples preserved properly
Sample Information
1. Sample labels present on bottles
5. Sample recvd within HT
4. Condition of sample
3. Sufficient volume/containers recvd for analysis:
Intact
Comments SAMPLE #10 ID LABEL READS MW-35.
SM001Rev. Date 05/24/17
SGS Sample Receipt Summary
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
Cooler 1: (3.6);
Cooler 1: (3.4);
3. Type Of TB Received
W or S N/A
6. Dates/Times/IDs on COC match Sample Label
7. VOCs have headspace
8. Bottles received for unspecified tests
9. Compositing instructions clear
10. Voa Soil Kits/Jars received past 48hrs?
11. % Solids Jar received?
Misc. Information
25-Gram 5-GramNumber of Encores:Number of 5035 Field Kits:Number of Lab Filtered Metals:
Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify)
Y or N N/A
Y or N
Therm ID:IR 1; Therm CF:-0.2; # of Coolers:1
Y or N N/A
12. Residual Chlorine Present?
Residual Chlorine Test Strip Lot #:
Technician:Reviewer:SHAYLAP Date:Date:2/22/2019 9:30:00 AM
FA61814: Chain of Custody
Page 2 of 2
35 of 48
FA6181444.1
SGS North America Inc.
MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 5
36 of 48
FA618145
Method Blank Summary Page 1 of 2
Job Number:FA61814
Account:GRINCC GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2080-MB E098108.D 1 02/27/19 AB n/a n/a VE2080
The QC reported here applies to the following samples:Method: SM 6200B
FA61814-1, FA61814-2, FA61814-3, FA61814-5, FA61814-8, FA61814-10
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
37 of 48
FA6181455.1.1
Method Blank Summary Page 2 of 2
Job Number:FA61814
Account:GRINCC GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2080-MB E098108.D 1 02/27/19 AB n/a n/a VE2080
The QC reported here applies to the following samples:Method: SM 6200B
FA61814-1, FA61814-2, FA61814-3, FA61814-5, FA61814-8, FA61814-10
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 107%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 105%70-130%
38 of 48
FA6181455.1.1
Method Blank Summary Page 1 of 2
Job Number:FA61814
Account:GRINCC GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2537-MB A0217227.D 1 02/28/19 AB n/a n/a VA2537
The QC reported here applies to the following samples:Method: SM 6200B
FA61814-4, FA61814-6, FA61814-7, FA61814-9, FA61814-11, FA61814-12
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
39 of 48
FA6181455.1.2
Method Blank Summary Page 2 of 2
Job Number:FA61814
Account:GRINCC GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2537-MB A0217227.D 1 02/28/19 AB n/a n/a VA2537
The QC reported here applies to the following samples:Method: SM 6200B
FA61814-4, FA61814-6, FA61814-7, FA61814-9, FA61814-11, FA61814-12
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 107%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
40 of 48
FA6181455.1.2
Blank Spike Summary Page 1 of 2
Job Number:FA61814
Account:GRINCC GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2080-BS E098106.D 1 02/27/19 AB n/a n/a VE2080
The QC reported here applies to the following samples:Method: SM 6200B
FA61814-1, FA61814-2, FA61814-3, FA61814-5, FA61814-8, FA61814-10
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 9.6 96 70-130
108-86-1 Bromobenzene 10 9.9 99 70-130
74-97-5 Bromochloromethane 10 9.9 99 70-130
75-27-4 Bromodichloromethane 10 10 100 70-130
75-25-2 Bromoform 10 9.1 91 70-130
104-51-8 n-Butylbenzene 10 10.9 109 70-130
135-98-8 sec-Butylbenzene 10 10.6 106 70-130
98-06-6 tert-Butylbenzene 10 10.5 105 70-130
56-23-5 Carbon Tetrachloride 10 10.3 103 70-130
108-90-7 Chlorobenzene 10 9.6 96 70-130
75-00-3 Chloroethane 10 15.3 153*60-140
67-66-3 Chloroform 10 10.3 103 70-130
95-49-8 o-Chlorotoluene 10 10.3 103 70-130
106-43-4 p-Chlorotoluene 10 10.3 103 70-130
124-48-1 Dibromochloromethane 10 9.8 98 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 9.4 94 70-130
106-93-4 1,2-Dibromoethane 10 9.7 97 70-130
75-71-8 Dichlorodifluoromethane 10 15.2 152*60-140
95-50-1 1,2-Dichlorobenzene 10 9.7 97 70-130
541-73-1 1,3-Dichlorobenzene 10 10.1 101 70-130
106-46-7 1,4-Dichlorobenzene 10 9.8 98 70-130
75-34-3 1,1-Dichloroethane 10 10.1 101 70-130
107-06-2 1,2-Dichloroethane 10 10.0 100 70-130
75-35-4 1,1-Dichloroethylene 10 9.8 98 70-130
156-59-2 cis-1,2-Dichloroethylene 10 9.7 97 70-130
156-60-5 trans-1,2-Dichloroethylene 10 9.5 95 70-130
78-87-5 1,2-Dichloropropane 10 9.7 97 70-130
142-28-9 1,3-Dichloropropane 10 9.3 93 70-130
594-20-7 2,2-Dichloropropane 10 12.1 121 70-130
563-58-6 1,1-Dichloropropene 10 10.4 104 70-130
10061-01-5 cis-1,3-Dichloropropene 10 9.0 90 70-130
10061-02-6 trans-1,3-Dichloropropene 10 9.9 99 70-130
108-20-3 Di-Isopropyl Ether 10 9.7 97 70-130
100-41-4 Ethylbenzene 10 10.1 101 70-130
87-68-3 Hexachlorobutadiene 10 10.6 106 70-130
98-82-8 Isopropylbenzene 10 10.7 107 70-130
* = Outside of Control Limits.
41 of 48
FA6181455.2.1
Blank Spike Summary Page 2 of 2
Job Number:FA61814
Account:GRINCC GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2080-BS E098106.D 1 02/27/19 AB n/a n/a VE2080
The QC reported here applies to the following samples:Method: SM 6200B
FA61814-1, FA61814-2, FA61814-3, FA61814-5, FA61814-8, FA61814-10
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 10.6 106 70-130
74-83-9 Methyl Bromide 10 12.1 121 60-140
74-87-3 Methyl Chloride 10 12.9 129 60-140
74-95-3 Methylene Bromide 10 9.7 97 70-130
75-09-2 Methylene Chloride 10 9.0 90 70-130
1634-04-4 Methyl Tert Butyl Ether 10 10.0 100 70-130
91-20-3 Naphthalene 10 9.8 98 70-130
103-65-1 n-Propylbenzene 10 10.3 103 70-130
100-42-5 Styrene 10 9.9 99 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 9.9 99 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 10.2 102 70-130
127-18-4 Tetrachloroethylene 10 10.1 101 70-130
108-88-3 Toluene 10 9.8 98 70-130
87-61-6 1,2,3-Trichlorobenzene 10 9.9 99 70-130
120-82-1 1,2,4-Trichlorobenzene 10 9.9 99 70-130
71-55-6 1,1,1-Trichloroethane 10 10.5 105 70-130
79-00-5 1,1,2-Trichloroethane 10 9.7 97 70-130
79-01-6 Trichloroethylene 10 9.8 98 70-130
75-69-4 Trichlorofluoromethane 10 12.2 122 60-140
96-18-4 1,2,3-Trichloropropane 10 9.8 98 70-130
95-63-6 1,2,4-Trimethylbenzene 10 10 100 70-130
108-67-8 1,3,5-Trimethylbenzene 10 10.4 104 70-130
75-01-4 Vinyl Chloride 10 11.1 111 60-140
m,p-Xylene 20 20.2 101 70-130
95-47-6 o-Xylene 10 10 100 70-130
1330-20-7 Xylene (total)30 30.1 100 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 109%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 103%70-130%
* = Outside of Control Limits.
42 of 48
FA6181455.2.1
Blank Spike Summary Page 1 of 2
Job Number:FA61814
Account:GRINCC GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2537-BS A0217225.D 1 02/28/19 AB n/a n/a VA2537
The QC reported here applies to the following samples:Method: SM 6200B
FA61814-4, FA61814-6, FA61814-7, FA61814-9, FA61814-11, FA61814-12
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 9.6 96 70-130
108-86-1 Bromobenzene 10 9.2 92 70-130
74-97-5 Bromochloromethane 10 9.7 97 70-130
75-27-4 Bromodichloromethane 10 10.1 101 70-130
75-25-2 Bromoform 10 9.6 96 70-130
104-51-8 n-Butylbenzene 10 9.9 99 70-130
135-98-8 sec-Butylbenzene 10 9.7 97 70-130
98-06-6 tert-Butylbenzene 10 8.9 89 70-130
56-23-5 Carbon Tetrachloride 10 10.3 103 70-130
108-90-7 Chlorobenzene 10 9.5 95 70-130
75-00-3 Chloroethane 10 10.9 109 60-140
67-66-3 Chloroform 10 9.6 96 70-130
95-49-8 o-Chlorotoluene 10 9.4 94 70-130
106-43-4 p-Chlorotoluene 10 9.3 93 70-130
124-48-1 Dibromochloromethane 10 9.5 95 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 9.3 93 70-130
106-93-4 1,2-Dibromoethane 10 9.5 95 70-130
75-71-8 Dichlorodifluoromethane 10 19.1 191*60-140
95-50-1 1,2-Dichlorobenzene 10 9.5 95 70-130
541-73-1 1,3-Dichlorobenzene 10 9.9 99 70-130
106-46-7 1,4-Dichlorobenzene 10 9.6 96 70-130
75-34-3 1,1-Dichloroethane 10 9.7 97 70-130
107-06-2 1,2-Dichloroethane 10 9.4 94 70-130
75-35-4 1,1-Dichloroethylene 10 9.7 97 70-130
156-59-2 cis-1,2-Dichloroethylene 10 9.3 93 70-130
156-60-5 trans-1,2-Dichloroethylene 10 9.4 94 70-130
78-87-5 1,2-Dichloropropane 10 9.6 96 70-130
142-28-9 1,3-Dichloropropane 10 8.9 89 70-130
594-20-7 2,2-Dichloropropane 10 10.7 107 70-130
563-58-6 1,1-Dichloropropene 10 9.9 99 70-130
10061-01-5 cis-1,3-Dichloropropene 10 8.8 88 70-130
10061-02-6 trans-1,3-Dichloropropene 10 9.4 94 70-130
108-20-3 Di-Isopropyl Ether 10 9.6 96 70-130
100-41-4 Ethylbenzene 10 9.7 97 70-130
87-68-3 Hexachlorobutadiene 10 9.5 95 70-130
98-82-8 Isopropylbenzene 10 10.3 103 70-130
* = Outside of Control Limits.
43 of 48
FA6181455.2.2
Blank Spike Summary Page 2 of 2
Job Number:FA61814
Account:GRINCC GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2537-BS A0217225.D 1 02/28/19 AB n/a n/a VA2537
The QC reported here applies to the following samples:Method: SM 6200B
FA61814-4, FA61814-6, FA61814-7, FA61814-9, FA61814-11, FA61814-12
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 9.1 91 70-130
74-83-9 Methyl Bromide 10 9.5 95 60-140
74-87-3 Methyl Chloride 10 13.7 137 60-140
74-95-3 Methylene Bromide 10 9.4 94 70-130
75-09-2 Methylene Chloride 10 9.3 93 70-130
1634-04-4 Methyl Tert Butyl Ether 10 9.8 98 70-130
91-20-3 Naphthalene 10 8.5 85 70-130
103-65-1 n-Propylbenzene 10 9.4 94 70-130
100-42-5 Styrene 10 9.0 90 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 9.7 97 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 9.2 92 70-130
127-18-4 Tetrachloroethylene 10 10 100 70-130
108-88-3 Toluene 10 9.4 94 70-130
87-61-6 1,2,3-Trichlorobenzene 10 9.0 90 70-130
120-82-1 1,2,4-Trichlorobenzene 10 8.9 89 70-130
71-55-6 1,1,1-Trichloroethane 10 9.8 98 70-130
79-00-5 1,1,2-Trichloroethane 10 9.7 97 70-130
79-01-6 Trichloroethylene 10 9.6 96 70-130
75-69-4 Trichlorofluoromethane 10 11.2 112 60-140
96-18-4 1,2,3-Trichloropropane 10 8.9 89 70-130
95-63-6 1,2,4-Trimethylbenzene 10 9.1 91 70-130
108-67-8 1,3,5-Trimethylbenzene 10 9.5 95 70-130
75-01-4 Vinyl Chloride 10 13.3 133 60-140
m,p-Xylene 20 19.7 99 70-130
95-47-6 o-Xylene 10 9.6 96 70-130
1330-20-7 Xylene (total)30 29.3 98 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 95%70-130%
* = Outside of Control Limits.
44 of 48
FA6181455.2.2
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA61814
Account:GRINCC GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA61814-5MS E098119.D 5 02/27/19 AB n/a n/a VE2080
FA61814-5MSD E098120.D 5 02/27/19 AB n/a n/a VE2080
FA61814-5 E098111.D 1 02/27/19 AB n/a n/a VE2080
The QC reported here applies to the following samples:Method: SM 6200B
FA61814-1, FA61814-2, FA61814-3, FA61814-5, FA61814-8, FA61814-10
FA61814-5 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 1.3 50 46.9 91 50 48.4 94 3 70-130/20
108-86-1 Bromobenzene ND 50 47.0 94 50 49.0 98 4 70-130/20
74-97-5 Bromochloromethane ND 50 46.8 94 50 47.3 95 1 70-130/20
75-27-4 Bromodichloromethane ND 50 46.1 92 50 47.8 96 4 70-130/20
75-25-2 Bromoform ND 50 35.6 71 50 37.8 76 6 70-130/20
104-51-8 n-Butylbenzene ND 50 51.5 103 50 53.7 107 4 70-130/20
135-98-8 sec-Butylbenzene ND 50 51.4 103 50 53.2 106 3 70-130/20
98-06-6 tert-Butylbenzene ND 50 51.3 103 50 53.1 106 3 70-130/20
56-23-5 Carbon Tetrachloride ND 50 49.8 100 50 49.9 100 0 70-130/20
108-90-7 Chlorobenzene ND 50 46.1 92 50 47.7 95 3 70-130/20
75-00-3 Chloroethane ND 50 79.7 159*50 89.7 179*12 60-140/20
67-66-3 Chloroform ND 50 51.2 102 50 51.7 103 1 70-130/20
95-49-8 o-Chlorotoluene ND 50 50.0 100 50 51.7 103 3 70-130/20
106-43-4 p-Chlorotoluene ND 50 50.3 101 50 52.6 105 4 70-130/20
124-48-1 Dibromochloromethane ND 50 41.5 83 50 44.0 88 6 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 50 42.6 85 50 42.1 84 1 70-130/20
106-93-4 1,2-Dibromoethane ND 50 45.4 91 50 47.9 96 5 70-130/20
75-71-8 Dichlorodifluoromethane ND 50 82.4 165*50 88.5 177*7 60-140/20
95-50-1 1,2-Dichlorobenzene ND 50 45.3 91 50 47.7 95 5 70-130/20
541-73-1 1,3-Dichlorobenzene ND 50 47.8 96 50 50.6 101 6 70-130/20
106-46-7 1,4-Dichlorobenzene ND 50 46.6 93 50 48.4 97 4 70-130/20
75-34-3 1,1-Dichloroethane ND 50 49.3 99 50 50.2 100 2 70-130/20
107-06-2 1,2-Dichloroethane ND 50 50.7 101 50 51.4 103 1 70-130/20
75-35-4 1,1-Dichloroethylene ND 50 49.0 98 50 49.6 99 1 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 50 46.4 93 50 46.3 93 0 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 50 46.6 93 50 47.3 95 1 70-130/20
78-87-5 1,2-Dichloropropane ND 50 46.5 93 50 47.9 96 3 70-130/20
142-28-9 1,3-Dichloropropane ND 50 44.5 89 50 46.5 93 4 70-130/20
594-20-7 2,2-Dichloropropane ND 50 54.4 109 50 56.4 113 4 70-130/20
563-58-6 1,1-Dichloropropene ND 50 49.9 100 50 51.6 103 3 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 50 37.4 75 50 40.3 81 7 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 50 40.8 82 50 44.5 89 9 70-130/20
108-20-3 Di-Isopropyl Ether ND 50 47.1 94 50 48.1 96 2 70-130/20
100-41-4 Ethylbenzene 1.2 50 49.8 97 50 51.7 101 4 70-130/20
87-68-3 Hexachlorobutadiene ND 50 49.3 99 50 49.3 99 0 70-130/20
98-82-8 Isopropylbenzene ND 50 51.2 102 50 52.5 105 3 70-130/20
* = Outside of Control Limits.
45 of 48
FA6181455.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA61814
Account:GRINCC GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA61814-5MS E098119.D 5 02/27/19 AB n/a n/a VE2080
FA61814-5MSD E098120.D 5 02/27/19 AB n/a n/a VE2080
FA61814-5 E098111.D 1 02/27/19 AB n/a n/a VE2080
The QC reported here applies to the following samples:Method: SM 6200B
FA61814-1, FA61814-2, FA61814-3, FA61814-5, FA61814-8, FA61814-10
FA61814-5 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 50 50.4 101 50 52.4 105 4 70-130/20
74-83-9 Methyl Bromide ND 50 68.3 137 50 69.4 139 2 60-140/20
74-87-3 Methyl Chloride ND 50 67.8 136 50 71.3 143*5 60-140/20
74-95-3 Methylene Bromide ND 50 46.5 93 50 48.4 97 4 70-130/20
75-09-2 Methylene Chloride ND 50 50.3 101 50 50.0 100 1 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 50 46.5 93 50 48.7 97 5 70-130/20
91-20-3 Naphthalene 0.20 J 50 42.2 84 50 44.7 89 6 70-130/20
103-65-1 n-Propylbenzene ND 50 50.5 101 50 52.5 105 4 70-130/20
100-42-5 Styrene ND 50 46.4 93 50 48.1 96 4 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 50 46.1 92 50 47.7 95 3 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 50 47.8 96 50 50.5 101 5 70-130/20
127-18-4 Tetrachloroethylene ND 50 47.9 96 50 48.4 97 1 70-130/20
108-88-3 Toluene 1.5 50 48.0 93 50 49.5 96 3 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 50 42.3 85 50 44.0 88 4 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 50 43.7 87 50 45.9 92 5 70-130/20
71-55-6 1,1,1-Trichloroethane ND 50 51.7 103 50 52.2 104 1 70-130/20
79-00-5 1,1,2-Trichloroethane ND 50 45.6 91 50 48.0 96 5 70-130/20
79-01-6 Trichloroethylene ND 50 46.4 93 50 47.4 95 2 70-130/20
75-69-4 Trichlorofluoromethane ND 50 65.7 131 50 70.6 141*7 60-140/20
96-18-4 1,2,3-Trichloropropane ND 50 47.7 95 50 49.3 99 3 70-130/20
95-63-6 1,2,4-Trimethylbenzene 0.35 J 50 49.0 97 50 50.2 100 2 70-130/20
108-67-8 1,3,5-Trimethylbenzene 0.14 J 50 50.1 100 50 51.8 103 3 70-130/20
75-01-4 Vinyl Chloride ND 50 56.7 113 50 61.7 123 8 60-140/20
m,p-Xylene 1.7 100 101 99 100 103 101 2 70-130/20
95-47-6 o-Xylene 0.89 50 49.0 96 50 50.2 99 2 70-130/20
1330-20-7 Xylene (total)2.5 150 150 98 150 154 101 3 70-130/20
CAS No.Surrogate Recoveries MS MSD FA61814-5 Limits
1868-53-7 Dibromofluoromethane 106%105%102%70-130%
17060-07-0 1,2-Dichloroethane-D4 116%115%110%70-130%
2037-26-5 Toluene-D8 100%100%98%70-130%
460-00-4 4-Bromofluorobenzene 105%106%104%70-130%
* = Outside of Control Limits.
46 of 48
FA6181455.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA61814
Account:GRINCC GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA61814-11MS A0217236.D 5 02/28/19 AB n/a n/a VA2537
FA61814-11MSD A0217237.D 5 02/28/19 AB n/a n/a VA2537
FA61814-11 A0217228.D 1 02/28/19 AB n/a n/a VA2537
The QC reported here applies to the following samples:Method: SM 6200B
FA61814-4, FA61814-6, FA61814-7, FA61814-9, FA61814-11, FA61814-12
FA61814-11 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene ND 50 48.2 96 50 48.8 98 1 70-130/20
108-86-1 Bromobenzene ND 50 48.0 96 50 49.5 99 3 70-130/20
74-97-5 Bromochloromethane ND 50 49.1 98 50 48.7 97 1 70-130/20
75-27-4 Bromodichloromethane ND 50 48.0 96 50 48.4 97 1 70-130/20
75-25-2 Bromoform ND 50 40.5 81 50 42.3 85 4 70-130/20
104-51-8 n-Butylbenzene ND 50 48.5 97 50 48.6 97 0 70-130/20
135-98-8 sec-Butylbenzene ND 50 50.8 102 50 52.3 105 3 70-130/20
98-06-6 tert-Butylbenzene ND 50 46.3 93 50 47.9 96 3 70-130/20
56-23-5 Carbon Tetrachloride ND 50 51.5 103 50 52.2 104 1 70-130/20
108-90-7 Chlorobenzene ND 50 47.2 94 50 48.4 97 3 70-130/20
75-00-3 Chloroethane ND 50 56.2 112 50 56.8 114 1 60-140/20
67-66-3 Chloroform ND 50 49.7 99 50 50.4 101 1 70-130/20
95-49-8 o-Chlorotoluene ND 50 49.8 100 50 51.3 103 3 70-130/20
106-43-4 p-Chlorotoluene ND 50 48.0 96 50 50.3 101 5 70-130/20
124-48-1 Dibromochloromethane ND 50 42.3 85 50 43.8 88 3 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 50 44.0 88 50 44.4 89 1 70-130/20
106-93-4 1,2-Dibromoethane ND 50 43.9 88 50 45.3 91 3 70-130/20
75-71-8 Dichlorodifluoromethane ND 50 98.8 198*50 95.5 191*3 60-140/20
95-50-1 1,2-Dichlorobenzene ND 50 47.7 95 50 48.5 97 2 70-130/20
541-73-1 1,3-Dichlorobenzene ND 50 49.4 99 50 50.1 100 1 70-130/20
106-46-7 1,4-Dichlorobenzene ND 50 47.2 94 50 48.3 97 2 70-130/20
75-34-3 1,1-Dichloroethane ND 50 50.4 101 50 50.5 101 0 70-130/20
107-06-2 1,2-Dichloroethane ND 50 47.1 94 50 47.0 94 0 70-130/20
75-35-4 1,1-Dichloroethylene ND 50 50.3 101 50 49.8 100 1 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 50 47.4 95 50 48.1 96 1 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 50 47.7 95 50 48.8 98 2 70-130/20
78-87-5 1,2-Dichloropropane ND 50 47.1 94 50 47.6 95 1 70-130/20
142-28-9 1,3-Dichloropropane ND 50 42.1 84 50 43.3 87 3 70-130/20
594-20-7 2,2-Dichloropropane ND 50 56.1 112 50 55.6 111 1 70-130/20
563-58-6 1,1-Dichloropropene ND 50 50.3 101 50 51.0 102 1 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 50 37.2 74 50 38.3 77 3 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 50 42.0 84 50 43.7 87 4 70-130/20
108-20-3 Di-Isopropyl Ether ND 50 49.4 99 50 49.6 99 0 70-130/20
100-41-4 Ethylbenzene ND 50 49.1 98 50 50.4 101 3 70-130/20
87-68-3 Hexachlorobutadiene ND 50 48.5 97 50 49.0 98 1 70-130/20
98-82-8 Isopropylbenzene ND 50 53.3 107 50 53.6 107 1 70-130/20
* = Outside of Control Limits.
47 of 48
FA6181455.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA61814
Account:GRINCC GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA61814-11MS A0217236.D 5 02/28/19 AB n/a n/a VA2537
FA61814-11MSD A0217237.D 5 02/28/19 AB n/a n/a VA2537
FA61814-11 A0217228.D 1 02/28/19 AB n/a n/a VA2537
The QC reported here applies to the following samples:Method: SM 6200B
FA61814-4, FA61814-6, FA61814-7, FA61814-9, FA61814-11, FA61814-12
FA61814-11 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 50 47.6 95 50 49.4 99 4 70-130/20
74-83-9 Methyl Bromide ND 50 50.7 101 50 49.1 98 3 60-140/20
74-87-3 Methyl Chloride ND 50 69.7 139 50 69.6 139 0 60-140/20
74-95-3 Methylene Bromide ND 50 46.5 93 50 47.0 94 1 70-130/20
75-09-2 Methylene Chloride ND 50 51.0 102 50 50.3 101 1 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 50 49.4 99 50 49.4 99 0 70-130/20
91-20-3 Naphthalene ND 50 43.6 87 50 44.6 89 2 70-130/20
103-65-1 n-Propylbenzene ND 50 49.2 98 50 50.9 102 3 70-130/20
100-42-5 Styrene ND 50 44.4 89 50 45.6 91 3 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 50 49.7 99 50 50.7 101 2 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 50 48.4 97 50 49.2 98 2 70-130/20
127-18-4 Tetrachloroethylene ND 50 50.1 100 50 50.8 102 1 70-130/20
108-88-3 Toluene ND 50 47.0 94 50 48.4 97 3 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 50 47.0 94 50 48.7 97 4 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 50 46.7 93 50 47.9 96 3 70-130/20
71-55-6 1,1,1-Trichloroethane ND 50 51.1 102 50 50.5 101 1 70-130/20
79-00-5 1,1,2-Trichloroethane ND 50 46.8 94 50 47.1 94 1 70-130/20
79-01-6 Trichloroethylene ND 50 49.0 98 50 48.5 97 1 70-130/20
75-69-4 Trichlorofluoromethane ND 50 58.2 116 50 56.3 113 3 60-140/20
96-18-4 1,2,3-Trichloropropane ND 50 45.7 91 50 46.0 92 1 70-130/20
95-63-6 1,2,4-Trimethylbenzene ND 50 48.4 97 50 49.3 99 2 70-130/20
108-67-8 1,3,5-Trimethylbenzene ND 50 50.3 101 50 51.7 103 3 70-130/20
75-01-4 Vinyl Chloride ND 50 66.2 132 50 63.4 127 4 60-140/20
m,p-Xylene ND 100 99.8 100 100 101 101 1 70-130/20
95-47-6 o-Xylene ND 50 48.6 97 50 49.2 98 1 70-130/20
1330-20-7 Xylene (total)ND 150 148 99 150 151 101 2 70-130/20
CAS No.Surrogate Recoveries MS MSD FA61814-11 Limits
1868-53-7 Dibromofluoromethane 104%103%100%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%103%104%70-130%
2037-26-5 Toluene-D8 97%97%97%70-130%
460-00-4 4-Bromofluorobenzene 97%98%101%70-130%
* = Outside of Control Limits.
48 of 48
FA6181455.3.2