WA-911_11890_CA_RPTS_20160210_MRP

EXECUTIVE SUMMARY
The former Red Apple Market #15 site is located at 1109 US Highway 64 East in Plymouth, Washington
County, North Carolina. According to available information, two 550-gallon fuel oil, one 10,000-gallon
gasoline, three 4,000-gallon gasoline, one 10,000-gallon diesel, and one 2,000-gallon kerosene
underground storage tanks (USTs) were removed from the site in October 1993. Reportedly, a water
supply well, which its use has yet to be determined by NCDEQ, is located approximately 750 feet
north/northwest of the site. Municipal water is available to all properties within the site vicinity. No
surface water bodies were identified within a 500-foot radius of the source area.

On January 28, 2016, eleven Type II monitoring wells (MW-1 through MW-5, MW-7, MW-13 through
MW-16 and MW -18) and one Type III monitoring well (MW-8) were gauged, purged and sampled.
Concentrations of requested method constituents that exceeded the Maximum Allowable Concentrations
(MACs) specified in T15A NCAC 2L.0202 were reported in the ground water samples collected from
MW-2, MW-3, MW-4, MW-13 and MW-14.

GRI recommends that the use of the water supply well be determined by NCDEQ. Regardless of the use
of the water supply well, the results of the March 14, 2014, Ground Water Monitoring and Fate &
Transport Model Report indicate that the well is not considered to be at risk from this site. The site risk
classification should be lowered to Low Risk and the incident should be closed with the completion of
Notice of Residual Petroleum.

TABLE OF CONTENTS

1.0 SITE HISTORY AND CHARACTERIZATION .................................................................... 1
2.0 CURRENT SITE ASSESSMENT ............................................................................................ 1
3.0 GROUND WATER QUALITY ................................................................................................ 1
4.0 CONCLUSIONS AND RECOMMENDATIONS .................................................................... 2
5.0 LIMITATIONS ......................................................................................................................... 3

FIGURES
Figure 1: Site Location Map
Figure 2: Site Map
Figure 3: Water Table Surface Map
Figure 4: Ground Water Quality Map
Figure 5: Benzene Isoconcentration Map
Figure 6: Naphthalene Isoconcentration Map

TABLES
Table 1: Well Construction and Gauging Information
Table 2: Summary of Ground Water Sample Analytical Results
APPENDICES
Appendix A: Laboratory Report – Ground Water Samples
Appendix B: Water Supply Well Abandonment Letters

1
1.0 SITE HISTORY AND CHARACTERIZATION
According to the February 28, 2002, Quarterly Groundwater Monitoring Report submitted by NorthEast
Environmental, two 550-gallon fuel oil, one 10,000-gallon gasoline, three 4,000-gallon gasoline, one
10,000-gallon diesel, and one 2,000-gallon kerosene underground storage tanks (USTs) were removed
from the site in October 1993. A total of twenty-one Type II monitoring wells (MW-1 through MW-7
and MW-9 through MW-22) and one Type III monitoring well (MW-8) were installed at the site.
Monitoring well MW-6 was found destroyed during previous ground water assessment and corrective
action activities. A Corrective Action Plan, proposing natural attenuation, was approved for the site on
November 30, 1998.

The site is currently ranked as High risk due to the presence of a water supply well, which its use has yet
to be determined by NCDEQ, located approximately 750 feet north/northwest of the site. Municipal
water is available to all properties within the site vicinity. No surface water bodies were identified within
a 500-foot radius of the source area.

Previous activities were conducted by other consultants. Although Geological Resources, Inc. (GRI)
cannot verify the accuracy of information obtained from previous reports, for the purposes of this report,
it is assumed to be correct. Please refer to previous submittals for further historical information regarding
the site.

2.0 CURRENT SITE ASSESSMENT
This report presents the results of ground water assessment activities conducted on January 28, 2016, at
the former Red Apple Market #15 site. The site is located at 1109 US Highway 64 East in Plymouth,
Washington County, North Carolina (Figure 1). The activities were conducted in accordance with GRI
proposal number 15-677, which was submitted to NCDEQ on October 30, 2015 and approved as Task
Authorization No. 11890-022 on November 19, 2015. The purpose of the activities was to obtain current
ground water quality data for the site.

3.0 GROUND WATER QUALITY
On January 28, 2016, eleven Type II monitoring wells (MW-1 through MW-5, MW-7, MW-13 through
MW-16, and MW -18) and one Type III monitoring well (MW-8) were gauged, purged and sampled.
Please note, MW-12 and MW-19 were not accessible and MW-22 was not located, therefore, these wells

2
were not sampled. The depths to ground water in the Type II monitoring wells during the January 2016
sampling event ranged from 7.80 to 10.02 feet below the tops of well casings. Ground water elevations in
the Type II monitoring wells relative to a temporary benchmark assumed by the previous consultant
ranged from 90.02 to 90.44 feet. Based on these data, the general ground water flow direction appears to
be toward the northwest. The average horizontal hydraulic gradient across the site was less than 0.01 feet
per foot. The vertical hydraulic gradient between paired wells MW-4 and MW-8 was approximately 0.01
feet per foot in the downward direction. A Site Map showing the locations of the monitoring wells has
been included as Figure 2. A Water Table Surface Map based on the January 2016 sampling event is
included as Figure 3. A summary of well construction and gauging data is presented in Table 1.

Laboratory analyses were performed on the ground water samples collected from the monitoring wells
during the January 2016 sampling event for volatile organic compounds using EPA Method 6200B.
Concentrations of one or more individual BTEX constituents, naphthalene, isopropylbenzene, n-
propylbenzene, 1,3,5-trimethylbenzene and/or 1,2,4-trimethylbenzene that exceeded the Maximum
Allowable Concentrations (MACs) specified in T15A NCAC 2L.0202 were reported in the ground water
samples collected from MW-2, MW-3, MW-4, MW-13 and MW-14. None of the reported contaminant
concentrations exceeded the Gross Contamination Levels (GCLs). A summary of ground water sample
analytical results is presented in Table 2. A Ground Water Quality Map based on data collected during
the January 2016 sampling event is included as Figure 4. Inferred isoconcentration contours for benzene
and naphthalene are included as Figures 5 and 6, respectively. The laboratory report has been included
as Appendix A.

During the current ground water monitoring event, three water supply well abandonment letters were
submitted to the owner of the Oliver Garage Well. To date, no response has been received from the
owner of the well. Copies of the submitted letters are included as Appendix B.
4.0 CONCLUSIONS AND RECOMMENDATIONS
 The average depth to ground water in the Type II monitoring wells in January 2016 was 9.13
feet. The general ground water flow direction is toward the northwest with an average horizontal
hydraulic gradient of less than 0.01 feet per foot. The average vertical gradient between paired
wells MW-4 and MW-8 was approximately 0.01 feet per foot downward.
 Concentrations of one or more individual BTEX constituents, naphthalene, isopropylbenzene, n-
propylbenzene, 1,3,5-trimethylbenzene and/or 1,2,4-trimethylbenzene that exceeded the MACs

3
were reported in the ground water samples collected from MW-2, MW-3, MW-4, MW-13 and
MW-14. None of the reported contaminant concentrations exceeded the GCLs.
 The NCDENR incident manager identified a water supply well approximately 750 feet to the
north/northwest of the site. Based on the January 2016 ground water sampling data, it appears
that the water supply well is down gradient/cross gradient of the release. The usage of this well
has yet to be determined by NCDEQ. Attempts were made to have the water supply well
abandoned. To date, no response has been received from the property owner.
 Regardless of the use of the water supply well, the results of the March 14, 2014, Ground Water
Monitoring and Fate & Transport Model Report indicate that the well is not considered to be at
risk from this site. The site risk classification should be lowered to Low Risk and the incident
should be closed with the completion of Notice of Residual Petroleum.

5.0 LIMITATIONS
This report has been prepared for the exclusive use of Red Apple Markets, Inc. for specific application to
the referenced site in Washington County, North Carolina. The assessment was conducted based on the
scope of work and level of effort desired by the NCDEQ and with resources adequate only for that scope
of work. Our findings have been developed in accordance with generally accepted standards of
environmental practices in the State of North Carolina, available information, and our professional
judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would be
interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data. Please note that field data collected prior
to the June 2010 free product recovery event was not obtained under the supervision of GRI. Although
the accuracy of this information cannot be verified, for the purpose of this report GRI assumes that it is
correct.

FIGURES

TABLES
11/29/10 11.35 ---88.65
06/06/11 10.92 ---89.08
04/02/13 10.27 ---89.73
09/30/13 10.67 ---89.33
06/20/14 10.58 ---89.42
01/28/16 9.78 ---90.22
11/29/10 11.60 ---88.62
06/06/11 11.20 ---89.02
04/02/13 10.58 ---89.64
09/30/13 11.02 ---89.20
06/20/14 10.85 ---89.37
01/28/16 10.02 ---90.20
11/29/10 10.28 ---88.80
06/06/11 9.90 ---89.18
04/02/13 9.20 ---89.88
09/30/13 9.79 ---89.29
06/20/14 9.62 ---89.46
01/28/16 8.64 ---90.44
06/11/10 9.40 0.07 89.65
11/29/10 10.35 ---88.64
06/06/11 9.70 ---89.29
04/02/13 9.53 ---89.46
09/30/13 9.51 ---89.48
06/20/14 9.40 ---89.59
01/28/16 8.56 ---90.43
11/29/10 11.42 ---88.70
06/06/11 11.02 ---89.10
04/02/13 10.32 ---89.80
09/30/13 10.86 ---89.26
06/20/14 10.71 ---89.41
01/28/16 9.84 ---90.28
11/29/10 NM NM NM Damaged
06/06/11 NM NM NM Abandoned
11/29/10 9.43 ---88.73
06/06/11 9.07 ---89.09
04/02/13 8.46 ---89.70
09/30/13 8.98 ---89.18
06/20/14 8.85 ---89.31
01/28/16 7.80 ---90.36
11/29/10 10.10 ---88.70
06/06/11 9.90 ---88.90
04/02/13 9.14 ---89.66
09/30/13 9.69 ---89.11
06/20/14 9.65 ---89.15
01/28/16 8.58 ---90.22
MW-1
2010 - 201011/01/94MW-3
100.002010 - 201011/01/94
1011/01/94MW-5
10 - 201011/01/94MW-2
MW-7
98.803227 - 322703/20/95MW-8
98.162010 - 201003/20/95
10 - 2010
1011/01/94MW-4
100.1220
20
Date: 02/02/16
Well
Installation
Date
Free
Product
Thickness
(ft.)
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET #15 (INCIDENT NO. 11890)
Facility ID # : 0-006313
Well ID
Date
Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft. BGS)
Bottom
of Well
(ft. BGS)
Top of Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(feet)
Comments
99.02
Ground
Water
Elevation
(ft.)
100.22
98.99
99.08
20
10 - 20
03/20/95MW-6
2010 - 20
Page 1 of 3
Date: 02/02/16
Well
Installation
Date
Free
Product
Thickness
(ft.)
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET #15 (INCIDENT NO. 11890)
Facility ID # : 0-006313
Well ID
Date
Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft. BGS)
Bottom
of Well
(ft. BGS)
Top of Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(feet)
Comments
Ground
Water
Elevation
(ft.)
11/29/10 10.32 ---88.73
06/06/11 9.92 ---89.13
04/02/13 8.23 ---90.82
09/30/13 9.80 ---89.25
06/20/14 9.60 ---89.45
11/29/10 10.77 ---88.65
06/06/11 10.32 ---89.10
04/02/13 9.68 ---89.74
09/30/13 10.18 ---89.24
06/20/14 9.88 ---89.54
11/29/10 10.77 ---88.65
06/06/11 10.33 ---89.09
04/02/13 9.67 ---89.75
09/30/13 10.21 ---89.21
06/20/14 9.98 ---89.44
11/29/10 10.58 ---88.63
06/06/11 10.20 ---89.01
04/02/13 9.51 ---89.70
09/30/13 10.07 ---89.14
06/20/14 9.91 ---89.30
01/28/16 NM NM NM Covered
11/29/10 11.50 ---88.62
06/06/11 11.10 ---89.02
04/02/13 10.42 ---89.70
09/30/13 10.91 ---89.21
06/20/14 10.76 ---89.36
01/28/16 9.83 ---90.29
11/29/10 11.37 ---88.61
06/06/11 10.95 ---89.03
04/02/13 10.30 ---89.68
09/30/13 10.81 ---89.17
06/20/14 10.63 ---89.35
01/28/16 9.74 ---90.24
11/29/10 9.40 ---88.53
06/06/11 8.93 ---89.00
04/02/13 8.41 ---89.52
09/30/13 8.80 ---89.13
06/20/14 8.56 ---89.37
01/28/16 7.91 ---90.02
11/29/10 9.79 ---88.57
06/06/11 9.30 ---89.06
04/02/13 8.70 ---89.66
09/30/13 9.19 ---89.17
06/20/14 8.93 ---89.43
01/28/16 8.26 ---90.10
99.98
100.12188 - 18806/22/95MW-13
188 - 18806/22/95MW-14
MW-15
98.36188 - 18806/23/95
03/23/95MW-9
MW-16
806/22/95
99.4220
99.422010 - 2010
10 - 2010
99.052010 - 2010
03/24/95MW-11
03/24/95MW-10
99.212010 - 2010
97.9318
MW-12 03/24/95
8 - 18
Page 2 of 3
Date: 02/02/16
Well
Installation
Date
Free
Product
Thickness
(ft.)
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET #15 (INCIDENT NO. 11890)
Facility ID # : 0-006313
Well ID
Date
Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft. BGS)
Bottom
of Well
(ft. BGS)
Top of Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(feet)
Comments
Ground
Water
Elevation
(ft.)
11/29/10 8.50 ---88.52
06/06/11 8.03 ---88.99
04/02/13 7.44 ---89.58
09/30/13 7.91 ---89.11
06/20/14 7.70 ---89.32
11/29/10 11.65 ---88.59
06/06/11 11.25 ---88.99
04/02/13 10.61 ---89.63
09/30/13 11.10 ---89.14
06/20/14 10.93 ---89.31
01/28/16 10.01 ---90.23
11/29/10 11.28 ---88.61
06/06/11 10.89 ---89.00
04/02/13 10.24 ---89.65
09/30/13 10.77 ---89.12
06/20/14 10.59 ---89.30
01/28/16 NM NM NM Covered
11/29/10 10.60 ---88.56
06/06/11 10.22 ---88.94
04/02/13 9.57 ---89.59
09/30/13 10.05 ---89.11
06/20/14 9.92 ---89.24
11/29/10 10.17 ---88.25
06/06/11 9.73 ---88.69
04/02/13 9.17 ---89.25
09/30/13 9.54 ---88.88
06/20/14 9.32 ---89.10
06/06/11 9.74 ---88.92
04/02/13 9.14 ---89.52
09/30/13 9.51 ---89.15
06/20/14 9.34 ---89.32
01/28/16 NM NM NM Not Found
Notes:
• ft BGS : feet below ground surface.
• NM: Not Measured.
• Top of Casing information and well construction details prior to June 2011 were obtained from the report titled 'Quartely Groundwater Sampling Event',
dated February 28, 2002 by Northeast Environmental, P.C. and well construction records.
07/12/00MW-21
09/19/95MW-20
09/08/95MW-18 100.24188 - 188
98.422010 - 2010
97.02155 - 15509/08/95
99.16188 - 188
99.89188 - 18809/19/95MW-19
MW-17
98.66188 - 18806/06/11MW-22
Page 3 of 3
Date : 02/05/16
EPA
Method
504.1
EPA
Method
6010B
Well
ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 70 70 70 70 400 400 0.02 15 400 700 10,000 200
5,000 260,000 84,500 87,500 20,000 6,000 6,900 8,500 25,000 30,000 25,000 28,500 50 15,000 NE NE NE NE
11/29/10 <0.140 <0.190 0.378 J 0.820 J 6.15 20.1 <0.180 4.32 4.31 3.49 <0.180 0.491 J NR 26.1 <100 73.0 <80.0 505
06/06/11 <0.13 <0.13 <0.15 <0.30 5.8 2.2 0.28 J 1.7 0.38 J 0.22 J <0.10 <0.10 <0.0093 NR <100 89.6 J NR 101
04/02/13 <0.10 <0.10 <0.10 <0.22 3.7 1.9 0.43 J 3.1 0.63 0.31 J <0.10 0.11 J NR NR NR NR NR NR
09/30/13 <0.10 <0.10 0.19 J <0.22 2.5 9.8 0.99 4.4 3.1 2.9 <0.10 <0.10 NR NR NR NR NR NR
06/20/14 1.2 <0.10 <0.10 <0.20 2.9 6.6 1.6 4.9 3.7 4.4 <0.10 0.12 J NR NR NR NR NR NR
01/28/16 <0.13 0.14 J <0.13 <0.31 2.0 <0.13 0.47 J 2.8 1.6 1.1 <0.13 <0.13 NR NR NR NR NR NR
11/29/10 0.643 J <0.190 0.290 J 0.355 J 4.76 0.911 J <0.180 1.82 0.526 J <0.220 <0.180 <0.150 NR 10.6 113 59.9 <78.4 346
06/06/11 <0.13 <0.13 <0.15 <0.30 2.9 <0.10 <0.10 1.2 0.21 J <0.11 <0.10 <0.10 <0.0093 NR <100 94.8 J NR 104
04/02/13 0.74 <0.10 0.59 <0.22 2.7 <0.15 0.21 J 1.0 0.70 0.43 J <0.10 <0.10 NR NR NR NR NR NR
09/30/13 <0.10 <0.10 <0.10 <0.22 2.1 0.47 J <0.10 0.40 J <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
06/20/14 <0.10 <0.10 0.49 J <0.20 2.9 0.44 J <0.10 0.53 0.25 J 0.24 J <0.10 <0.10 NR NR NR NR NR NR
01/28/16 2.0 0.16 J 0.73 0.75 J 5.8 2.0 0.16 J 1.1 0.65 0.46 J <0.13 0.74 NR NR NR NR NR NR
11/29/10 32.6 4.03 55.6 25.7 18.3 13.5 <0.360 1.41 J 7.29 12.5 5.28 5.37 NR 14.1 432 <160.0 <80.0 159
06/06/11 41.1 1.7 35.9 14.98 17.7 9.8 1.9 1.4 5.9 13.3 2.1 5.2 <0.0093 NR 503 243 NR 277
04/02/13 42.0 2.0 48.8 12.1 13.8 15.7 1.8 1.6 6.5 15.5 4.5 1.1 NR NR NR NR NR NR
09/30/13 47.7 4.1 60.9 20.0 11.7 16.7 1.8 1.4 6.3 17.2 3.5 2.5 NR NR NR NR NR NR
06/20/14 46.0 2.2 48.3 22.4 14.2 18.3 2.2 1.8 8.2 19.2 4.3 4.0 NR NR NR NR NR NR
01/28/16 17.2 1.7 23.3 5.2 4.9 11.3 1.6 1.3 4.5 10.2 0.88 0.62 NR NR NR NR NR NR
11/29/10 2,900 12,600 5,440 18,800 44.3 J 1,770 1,170 154 616 1,820 2,820 8,930 NR 5.82 27,300 16,500 <78.4 12,370
06/06/11 1,330 10,300 2,180 9,230 20.9 J 681 50.1 25.0 162 502 891 2,750 <0.0092 NR 26,900 20,500 NR 17,300
04/02/13 658 9,430 2,270 10,700 <25 853 37.8 J <25 136 473 837 3,150 NR NR NR NR NR NR
09/30/13 531 7,770 1,820 8,660 <25 492 <25 <25 85.9 J 285 582 2,390 NR NR NR NR NR NR
06/20/14 458 6,460 1,780 8,220 <2.5 511 23.1 15.2 121 379 628 2,340 NR NR NR NR NR NR
01/28/16 168 2,640 1,020 5,160 <13 523 69.9 31.7 J 101 365 865 2,690 NR NR NR NR NR NR
11/29/10 <0.140 <0.190 <0.150 <0.220 4.77 <0.500 <0.180 <0.140 <0.150 <0.220 <0.180 <0.150 NR 12.1 <100 <158.8 <78.4 <267
06/06/11 <0.13 <0.13 <0.15 <0.30 19.5 0.17 J <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 <0.0092 NR <100 <100 NR <100
04/02/13 <0.10 <0.10 <0.10 <0.22 24.2 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
09/30/13 <0.10 <0.10 <0.10 <0.22 14.0 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
06/20/14 <0.10 <0.10 <0.10 <0.20 13.2 0.41 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
01/28/16 <0.13 <0.13 <0.13 <0.31 2.3 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
11/29/10 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/06/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
04/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
GCL
MW-3
MW-2
MW-5
Facility ID #: 0-006313
EDBn-ButylbenzeneNaphthalene1,3,5-TrimethylbenzeneC9-C22 Aromaticsn-PropylbenzeneTABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
RED APPLE MARKET #15 (INCIDENT NO. 11890)
MADEP Methods VPH and EPH
LeadC5-C8 AliphaticsC9-C18 AliphaticsC19-C36 Aliphatics1,2,4-TrimethylbenzeneIsopropylbenzeneContaminant of Concern

MW-6 EthylbenzeneMTBEMW-1
MW-4
2L Standard BenzeneToluenesec-ButylbenzeneAnalytical Method EPA Method 6200B
XylenesPage 1 of 5
Date : 02/05/16
EPA
Method
504.1
EPA
Method
6010B
Well
ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 70 70 70 70 400 400 0.02 15 400 700 10,000 200
5,000 260,000 84,500 87,500 20,000 6,000 6,900 8,500 25,000 30,000 25,000 28,500 50 15,000 NE NE NE NEGCL
Facility ID #: 0-006313
EDBn-ButylbenzeneNaphthalene1,3,5-TrimethylbenzeneC9-C22 Aromaticsn-PropylbenzeneTABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
RED APPLE MARKET #15 (INCIDENT NO. 11890)
MADEP Methods VPH and EPH
LeadC5-C8 AliphaticsC9-C18 AliphaticsC19-C36 Aliphatics1,2,4-TrimethylbenzeneIsopropylbenzeneContaminant of Concern
EthylbenzeneMTBE2L Standard BenzeneToluenesec-ButylbenzeneAnalytical Method EPA Method 6200B
Xylenes11/29/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.150 <0.220 <0.180 <0.150 NR 27.8 <100 <157.7 <76.9 <263
06/06/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 <0.0094 NR <100 <100 NR <100
04/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
09/30/13 <0.10 <0.10 <0.10 <0.22 0.12 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
06/20/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
01/28/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
11/29/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.150 <0.220 <0.180 <0.150 NR 4.07 <100 <160.0 <80.0 <270
06/06/11 <0.13 <0.13 <0.15 <0.30 1.3 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 <0.0093 NR <100 <100 NR <100
04/02/13 <0.10 <0.10 <0.10 <0.22 1.5 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
09/30/13 <0.10 <0.10 <0.10 <0.22 1.2 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
06/20/14 0.12 J <0.10 <0.10 <0.20 2.3 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
01/28/16 <0.13 <0.13 <0.13 <0.31 8.8 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
11/29/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.150 <0.220 <0.180 <0.150 NR 14.6 <100 <160.0 <80.0 <270
06/06/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 <0.0095 NR <100 <100 NR <100
04/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
09/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
06/20/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
11/29/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.150 <0.220 <0.180 <0.150 NR 34.5 <100 <158.8 <78.4 <267
06/06/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 <0.0093 NR <100 <100 NR <100
04/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
09/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
06/20/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
11/29/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.150 <0.220 <0.180 <0.150 NR 8.02 <100 <158.8 <78.4 <267
06/06/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 <0.0094 NR <100 <100 NR <100
04/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
09/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
06/20/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
11/29/10 0.768 J <0.190 <0.150 0.364 J 4.25 <0.500 <0.180 <0.140 <0.150 <0.220 <0.180 <0.150 NR 43.6 <100 <158.8 <78.4 <267
06/06/11 0.99 <0.13 <0.15 <0.30 8.6 0.22 J <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 <0.019 NR <100 <100 NR <100
04/02/13 <0.10 <0.10 <0.10 <0.22 0.50 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
09/30/13 <0.10 <0.10 <0.10 <0.22 0.63 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
06/20/14 <0.10 <0.10 <0.10 <0.20 0.25 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
01/28/16 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
MW-11
MW-10
MW-9
MW-8
MW-7
MW-12
Page 2 of 5
Date : 02/05/16
EPA
Method
504.1
EPA
Method
6010B
Well
ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 70 70 70 70 400 400 0.02 15 400 700 10,000 200
5,000 260,000 84,500 87,500 20,000 6,000 6,900 8,500 25,000 30,000 25,000 28,500 50 15,000 NE NE NE NEGCL
Facility ID #: 0-006313
EDBn-ButylbenzeneNaphthalene1,3,5-TrimethylbenzeneC9-C22 Aromaticsn-PropylbenzeneTABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
RED APPLE MARKET #15 (INCIDENT NO. 11890)
MADEP Methods VPH and EPH
LeadC5-C8 AliphaticsC9-C18 AliphaticsC19-C36 Aliphatics1,2,4-TrimethylbenzeneIsopropylbenzeneContaminant of Concern
EthylbenzeneMTBE2L Standard BenzeneToluenesec-ButylbenzeneAnalytical Method EPA Method 6200B
Xylenes11/29/10 1,090 19.7 303 201 19.2 90.5 <1.80 4.16 J 30.9 53.3 9.40 J 9.03 J NR 12.0 1,860 505 <78.4 655
06/06/11 875 35.3 236 151.9 J 16.4 75.3 4.5 J 3.6 J 20.7 46.9 6.3 J 14.6 <0.0094 NR 2,080 1,080 NR 993
04/02/13 664 9.1 172 241 8.8 98.4 3.4 4.1 19.2 36.5 28.3 65.4 NR NR NR NR NR NR
09/30/13 334 1.9 93.2 115 6.7 78.6 2.7 3.2 12.3 22.8 8.2 36.9 NR NR NR NR NR NR
06/20/14 845 25.2 305 356 8.2 102 7.7 6.3 29.8 53.2 31.3 71.9 NR NR NR NR NR NR
01/28/16 270 4.0 J 72.1 83.8 3.7 J 44.1 2.4 J 2.5 J 7.7 12.3 6.0 6.9 NR NR NR NR NR NR
11/29/10 398 4.91 J 114 67.6 8.73 40.6 <0.900 1.70 J 7.95 13.3 1.81 J 2.70 J NR 5.44 801 212 <76.9 446
06/06/11 238 3.2 64.2 34.0 12.4 29.6 1.2 1.4 5.9 11.8 1.1 1.5 <0.0092 NR 394 234 NR 235
04/02/13 96.1 2.4 54.3 20.1 7.7 23.8 1.7 2.2 6.0 13.0 1.3 2.5 NR NR NR NR NR NR
09/30/13 316 3.0 55.2 35.6 8.6 32.9 2.3 2.9 6.6 13.5 0.64 J 1.2 NR NR NR NR NR NR
06/20/14 85.9 1.3 28.7 8.1 5.4 11.2 0.97 1.3 3.0 6.4 0.13 J 0.34 J NR NR NR NR NR NR
01/28/16 2,030 16.0 J 478 134 11.2 J 92.3 7.9 J 6.3 J 27.8 76.3 <6.3 <6.3 NR NR NR NR NR NR
11/29/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.150 <0.220 <0.180 <0.150 NR 5.49 <100 <157.7 <76.9 <263
06/06/11 <0.13 <0.13 <0.15 <0.30 0.64 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 <0.0094 NR <100 <100 NR <100
04/02/13 0.14 J <0.10 <0.10 <0.22 7.2 0.16 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
09/30/13 <0.10 <0.10 <0.10 <0.22 0.44 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
06/20/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
01/28/16 <0.13 <0.13 <0.13 <0.31 0.58 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
11/29/10 <0.140 0.326 J 0.391 J 2.00 <0.250 <0.500 <0.180 <0.140 <0.150 <0.220 0.438 J 1.54 NR 10.1 <100 <155.6 <74.1 <257
06/06/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 <0.0094 NR <100 <100 NR <100
04/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
09/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
06/20/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
01/28/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
11/29/10 <0.140 1.34 0.192 J 0.393 J <0.250 <0.500 <0.180 <0.140 <0.150 <0.220 <0.180 <0.150 NR 10.4 <100 <157.7 <76.9 <263
06/06/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 <0.0094 NR <100 <100 NR <100
04/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 0.12 J NR NR NR NR NR NR
09/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
06/20/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
MW-16
MW-15
MW-14
MW-13
MW-17
Page 3 of 5
Date : 02/05/16
EPA
Method
504.1
EPA
Method
6010B
Well
ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 70 70 70 70 400 400 0.02 15 400 700 10,000 200
5,000 260,000 84,500 87,500 20,000 6,000 6,900 8,500 25,000 30,000 25,000 28,500 50 15,000 NE NE NE NEGCL
Facility ID #: 0-006313
EDBn-ButylbenzeneNaphthalene1,3,5-TrimethylbenzeneC9-C22 Aromaticsn-PropylbenzeneTABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
RED APPLE MARKET #15 (INCIDENT NO. 11890)
MADEP Methods VPH and EPH
LeadC5-C8 AliphaticsC9-C18 AliphaticsC19-C36 Aliphatics1,2,4-TrimethylbenzeneIsopropylbenzeneContaminant of Concern
EthylbenzeneMTBE2L Standard BenzeneToluenesec-ButylbenzeneAnalytical Method EPA Method 6200B
Xylenes11/29/10 <0.140 <0.190 <0.150 <0.220 13.2 <0.500 <0.180 <0.140 <0.150 <0.220 <0.180 <0.150 NR 23.3 <100 <158.8 <78.4 <267
06/06/11 <0.13 <0.13 <0.15 <0.20 11.7 0.14 J <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 <0.0093 NR <100 <100 NR <100
04/02/13 <0.10 <0.10 <0.10 <0.22 0.19 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
09/30/13 <0.10 <0.10 <0.10 <0.22 6.9 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
06/20/14 <0.10 <0.10 <0.10 <0.20 4.7 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
01/28/16 <0.13 <0.13 <0.13 <0.31 2.4 0.17 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
11/29/10 0.202 J <0.190 <0.150 <0.220 0.620 J <0.500 <0.180 <0.140 <0.150 <0.220 <0.180 <0.150 NR 15.8 <100 <66.2 <78.4 <267
06/06/11 <0.13 <0.13 <0.15 <0.30 0.35 J <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 <0.0092 NR <100 <100 NR <100
04/02/13 <0.10 <0.10 <0.10 <0.22 0.58 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
09/30/13 <0.10 <0.10 <0.10 <0.22 0.29 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
06/20/14 <0.10 <0.10 <0.10 <0.20 0.41 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
01/28/16 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
11/29/10 <0.140 <0.190 <0.150 <0.220 3.58 <0.500 <0.180 <0.140 <0.150 <0.220 <0.180 <0.150 NR 66.0 <100 <158.8 <78.4 <267
06/06/11 <0.13 <0.13 <0.15 <0.30 3.5 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 <0.0093 NR <100 <100 NR <100
04/02/13 <0.10 <0.10 <0.10 <0.22 1.1 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
09/30/13 <0.10 <0.10 <0.10 <0.22 0.57 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
06/20/14 <0.10 <0.10 <0.10 <0.20 0.56 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
11/29/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.150 <0.220 <0.180 <0.150 NR 25.2 <100 <158.8 <78.4 <267
06/06/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 <0.0092 NR <100 <100 NR <100
04/02/13 <0.10 <0.10 <0.10 <0.22 0.19 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
09/30/13 <0.10 <0.10 <0.10 <0.22 0.13 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
06/20/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
MW-18
MW-20
MW-19
MW-21
Page 4 of 5
Date : 02/05/16
EPA
Method
504.1
EPA
Method
6010B
Well
ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 70 70 70 70 400 400 0.02 15 400 700 10,000 200
5,000 260,000 84,500 87,500 20,000 6,000 6,900 8,500 25,000 30,000 25,000 28,500 50 15,000 NE NE NE NEGCL
Facility ID #: 0-006313
EDBn-ButylbenzeneNaphthalene1,3,5-TrimethylbenzeneC9-C22 Aromaticsn-PropylbenzeneTABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
RED APPLE MARKET #15 (INCIDENT NO. 11890)
MADEP Methods VPH and EPH
LeadC5-C8 AliphaticsC9-C18 AliphaticsC19-C36 Aliphatics1,2,4-TrimethylbenzeneIsopropylbenzeneContaminant of Concern
EthylbenzeneMTBE2L Standard BenzeneToluenesec-ButylbenzeneAnalytical Method EPA Method 6200B
Xylenes06/06/11 2.2 <0.13 <0.15 <0.30 34.5 0.26 J <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 <0.0094 NR <100 <100 NR <100
04/02/13 <0.10 <0.10 <0.10 <0.22 5.5 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
09/30/13 <0.10 <0.10 <0.10 <0.22 2.9 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
06/20/14 <0.10 <0.10 <0.10 <0.20 0.69 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
01/28/16 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
Notes:
• Results reported in µg/l (micrograms per liter).
• NE: Not established
• < : Less than the reporting limit specified in the laboratory report.
• Concentrations in bold face type exceeded the 2L standard.
• J: Estimated value.
• NS: Not Sampled; well abandoned.
• NR: Not Reported.
• For other compounds reported which did not exceed the 2L Standards, refer to the laboratory reports.
• 2L Standard: as specified in T15A NCAC 2L.0202.
• GCL: Gross contamination level.
MW-22
Page 5 of 5

APPENDICES

APPENDIX A
Laboratory Report – Ground Water Samples
02/05/16
Technical Report for
GRI (Geological Resources Inc.)
Ram 15, 1109 US 64 E, Plymouth, NC
11890
Accutest Job Number: FA31078
Sampling Date: 01/28/16
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
[e-mail]; [e-mail];
[e-mail]; [e-mail]
ATTN: William Regenthall
Total number of pages in report:
Certifications: FL (E83510), LA (03051), KS (E-10327), IA (366), IL (200063), NC (573), NJ (FL002), SC (96038001)
DoD ELAP (L-A-B L2229), CA (2937), TX (T104704404), PA (68-03573), VA (460177),
AK, AR, GA, KY, MA, NV, OK, UT, WA
This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone] • http://www.accutest.com
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Norm Farmer
Technical Director
Southeast
02/05/16
e-Hardcopy 2.0
Automated Report
54
Accutest Laboratories is the sole authority for authorizing edits or modifications to this
document. Unauthorized modification of this report is strictly prohibited.
Effective January 1, 2016, SGS has acquired all of the assets of Accutest Laboratories and will continue to
operate as SGS-Accutest. SGS-Accutest is part of SGS, the world's leading inspection, verification, testing and
certification company.
1 of 54
FA31078
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................7
3.1: FA31078-1: MW-1 ........................................................................................................8
3.2: FA31078-2: MW-2 ........................................................................................................10
3.3: FA31078-3: MW-3 ........................................................................................................12
3.4: FA31078-4: MW-4 ........................................................................................................14
3.5: FA31078-5: MW-5 ........................................................................................................16
3.6: FA31078-6: MW-7 ........................................................................................................18
3.7: FA31078-7: MW-8 ........................................................................................................20
3.8: FA31078-8: MW-13 ......................................................................................................22
3.9: FA31078-9: MW-14 ......................................................................................................24
3.10: FA31078-10: MW-15 ..................................................................................................26
3.11: FA31078-11: MW-16 ..................................................................................................28
3.12: FA31078-12: MW-18 ..................................................................................................30
Section 4: Misc. Forms ............................................................................................................32
4.1: Chain of Custody ...........................................................................................................33
Section 5: GC/MS Volatiles - QC Data Summaries ..............................................................36
5.1: Method Blank Summary ................................................................................................37
5.2: Blank Spike Summary ...................................................................................................43
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................49 123452 of 54
FA31078
Accutest Laboratories
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA31078
Ram 15, 1109 US 64 E, Plymouth, NC
Project No: 11890
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA31078-1 01/28/16 10:42 HM 01/29/16 AQ Ground Water MW-1
FA31078-2 01/28/16 13:42 HM 01/29/16 AQ Ground Water MW-2
FA31078-3 01/28/16 11:25 HM 01/29/16 AQ Ground Water MW-3
FA31078-4 01/28/16 11:36 HM 01/29/16 AQ Ground Water MW-4
FA31078-5 01/28/16 10:54 HM 01/29/16 AQ Ground Water MW-5
FA31078-6 01/28/16 11:12 HM 01/29/16 AQ Ground Water MW-7
FA31078-7 01/28/16 11:52 HM 01/29/16 AQ Ground Water MW-8
FA31078-8 01/28/16 13:10 HM 01/29/16 AQ Ground Water MW-13
FA31078-9 01/28/16 13:33 HM 01/29/16 AQ Ground Water MW-14
FA31078-10 01/28/16 12:39 HM 01/29/16 AQ Ground Water MW-15
FA31078-11 01/28/16 12:51 HM 01/29/16 AQ Ground Water MW-16
FA31078-12 01/28/16 13:21 HM 01/29/16 AQ Ground Water MW-18
3 of 54
FA31078 1
Summary of Hits Page 1 of 3
Job Number:FA31078
Account:GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Collected:01/28/16
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA31078-1 MW-1
n-Butylbenzene 0.47 J 0.50 0.13 ug/l SM 6200B
sec-Butylbenzene 2.8 0.50 0.13 ug/l SM 6200B
tert-Butylbenzene 0.38 J 0.50 0.13 ug/l SM 6200B
Di-Isopropyl Ether 0.98 0.50 0.13 ug/l SM 6200B
Isopropylbenzene 1.6 0.50 0.13 ug/l SM 6200B
Methyl Tert Butyl Ether 2.0 0.50 0.13 ug/l SM 6200B
n-Propylbenzene 1.1 0.50 0.13 ug/l SM 6200B
Toluene 0.14 J 0.50 0.13 ug/l SM 6200B
FA31078-2 MW-2
Benzene 2.0 0.50 0.13 ug/l SM 6200B
n-Butylbenzene 0.16 J 0.50 0.13 ug/l SM 6200B
sec-Butylbenzene 1.1 0.50 0.13 ug/l SM 6200B
Di-Isopropyl Ether 1.6 0.50 0.13 ug/l SM 6200B
Ethylbenzene 0.73 0.50 0.13 ug/l SM 6200B
Isopropylbenzene 0.65 0.50 0.13 ug/l SM 6200B
Methyl Tert Butyl Ether 5.8 0.50 0.13 ug/l SM 6200B
Naphthalene 2.0 0.50 0.13 ug/l SM 6200B
n-Propylbenzene 0.46 J 0.50 0.13 ug/l SM 6200B
Toluene 0.16 J 0.50 0.13 ug/l SM 6200B
1,2,4-Trimethylbenzene 0.74 0.50 0.13 ug/l SM 6200B
m,p-Xylene 0.75 J 1.0 0.18 ug/l SM 6200B
Xylene (total)0.75 J 1.5 0.31 ug/l SM 6200B
FA31078-3 MW-3
Benzene 17.2 0.50 0.13 ug/l SM 6200B
n-Butylbenzene 1.6 0.50 0.13 ug/l SM 6200B
sec-Butylbenzene 1.3 0.50 0.13 ug/l SM 6200B
Di-Isopropyl Ether 0.81 0.50 0.13 ug/l SM 6200B
Ethylbenzene 23.3 0.50 0.13 ug/l SM 6200B
Isopropylbenzene 4.5 0.50 0.13 ug/l SM 6200B
p-Isopropyltoluene 0.14 J 0.50 0.13 ug/l SM 6200B
Methyl Tert Butyl Ether 4.9 0.50 0.13 ug/l SM 6200B
Naphthalene 11.3 0.50 0.13 ug/l SM 6200B
n-Propylbenzene 10.2 0.50 0.13 ug/l SM 6200B
Toluene 1.7 0.50 0.13 ug/l SM 6200B
1,2,4-Trimethylbenzene 0.62 0.50 0.13 ug/l SM 6200B
1,3,5-Trimethylbenzene 0.88 0.50 0.13 ug/l SM 6200B
m,p-Xylene 4.3 1.0 0.18 ug/l SM 6200B
o-Xylene 0.97 0.50 0.13 ug/l SM 6200B
Xylene (total)5.2 1.5 0.31 ug/l SM 6200B
4 of 54
FA31078 2
Summary of Hits Page 2 of 3
Job Number:FA31078
Account:GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Collected:01/28/16
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA31078-4 MW-4
Benzene 168 50 13 ug/l SM 6200B
n-Butylbenzene 69.9 50 13 ug/l SM 6200B
sec-Butylbenzene 31.7 J 50 13 ug/l SM 6200B
o-Chlorotoluene 98.2 50 13 ug/l SM 6200B
Ethylbenzene 1020 50 13 ug/l SM 6200B
Isopropylbenzene 101 50 13 ug/l SM 6200B
p-Isopropyltoluene 19.9 J 50 13 ug/l SM 6200B
Methylene Chloride 190 JB 200 100 ug/l SM 6200B
Naphthalene 523 50 13 ug/l SM 6200B
n-Propylbenzene 365 50 13 ug/l SM 6200B
Toluene 2640 50 13 ug/l SM 6200B
1,2,4-Trimethylbenzene 2690 50 13 ug/l SM 6200B
1,3,5-Trimethylbenzene 865 50 13 ug/l SM 6200B
m,p-Xylene 3740 100 18 ug/l SM 6200B
o-Xylene 1420 50 13 ug/l SM 6200B
Xylene (total)5160 150 31 ug/l SM 6200B
FA31078-5 MW-5
Methyl Tert Butyl Ether 2.3 0.50 0.13 ug/l SM 6200B
Tetrachloroethylene 0.66 0.50 0.13 ug/l SM 6200B
Trichloroethylene 0.21 J 0.50 0.13 ug/l SM 6200B
FA31078-6 MW-7
Tetrachloroethylene 0.27 J 0.50 0.13 ug/l SM 6200B
FA31078-7 MW-8
1,2-Dichloroethane 0.17 J 0.50 0.13 ug/l SM 6200B
Di-Isopropyl Ether 0.48 J 0.50 0.13 ug/l SM 6200B
Methyl Tert Butyl Ether 8.8 0.50 0.13 ug/l SM 6200B
FA31078-8 MW-13
Benzene 270 5.0 1.3 ug/l SM 6200B
n-Butylbenzene 2.4 J 5.0 1.3 ug/l SM 6200B
sec-Butylbenzene 2.5 J 5.0 1.3 ug/l SM 6200B
Ethylbenzene 72.1 5.0 1.3 ug/l SM 6200B
Isopropylbenzene 7.7 5.0 1.3 ug/l SM 6200B
Methylene Chloride 20.6 20 10 ug/l SM 6200B
Methyl Tert Butyl Ether 3.7 J 5.0 1.3 ug/l SM 6200B
5 of 54
FA31078 2
Summary of Hits Page 3 of 3
Job Number:FA31078
Account:GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Collected:01/28/16
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
Naphthalene 44.1 5.0 1.3 ug/l SM 6200B
n-Propylbenzene 12.3 5.0 1.3 ug/l SM 6200B
Toluene 4.0 J 5.0 1.3 ug/l SM 6200B
1,2,4-Trimethylbenzene 6.9 5.0 1.3 ug/l SM 6200B
1,3,5-Trimethylbenzene 6.0 5.0 1.3 ug/l SM 6200B
m,p-Xylene 83.8 10 1.8 ug/l SM 6200B
Xylene (total)83.8 15 3.1 ug/l SM 6200B
FA31078-9 MW-14
Benzene 2030 25 6.3 ug/l SM 6200B
n-Butylbenzene 7.9 J 25 6.3 ug/l SM 6200B
sec-Butylbenzene 6.3 J 25 6.3 ug/l SM 6200B
Ethylbenzene 478 25 6.3 ug/l SM 6200B
Isopropylbenzene 27.8 25 6.3 ug/l SM 6200B
Methylene Chloride 102 100 50 ug/l SM 6200B
Methyl Tert Butyl Ether 11.2 J 25 6.3 ug/l SM 6200B
Naphthalene 92.3 25 6.3 ug/l SM 6200B
n-Propylbenzene 76.3 25 6.3 ug/l SM 6200B
Toluene 16.0 J 25 6.3 ug/l SM 6200B
m,p-Xylene 126 50 9.2 ug/l SM 6200B
o-Xylene 8.2 J 25 6.3 ug/l SM 6200B
Xylene (total)134 75 15 ug/l SM 6200B
FA31078-10 MW-15
Methyl Tert Butyl Ether 0.58 0.50 0.13 ug/l SM 6200B
FA31078-11 MW-16
No hits reported in this sample.
FA31078-12 MW-18
Chlorobenzene 4.0 0.50 0.13 ug/l SM 6200B
1,4-Dichlorobenzene 3.9 0.50 0.13 ug/l SM 6200B
Methyl Tert Butyl Ether 2.4 0.50 0.13 ug/l SM 6200B
Naphthalene 0.17 J 0.50 0.13 ug/l SM 6200B
6 of 54
FA31078 2
Accutest Laboratories
Sample Results
Report of Analysis
Southeast
Section 3
7 of 54
FA31078 3
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-1
Lab Sample ID:FA31078-1 Date Sampled:01/28/16
Matrix:AQ - Ground Water Date Received:01/29/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0199098.D 1 02/01/16 TD n/a n/a VA1869
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene 0.47 0.50 0.13 ug/l J
135-98-8 sec-Butylbenzene 2.8 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene 0.38 0.50 0.13 ug/l J
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.29 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
8 of 54
FA31078 33.1
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-1
Lab Sample ID:FA31078-1 Date Sampled:01/28/16
Matrix:AQ - Ground Water Date Received:01/29/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 0.98 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene 1.6 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 2.0 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene 1.1 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene 0.14 0.50 0.13 ug/l J
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.14 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.18 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.31 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 93%70-130%
17060-07-0 1,2-Dichloroethane-D4 89%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
9 of 54
FA31078 33.1
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-2
Lab Sample ID:FA31078-2 Date Sampled:01/28/16
Matrix:AQ - Ground Water Date Received:01/29/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0199099.D 1 02/01/16 TD n/a n/a VA1869
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 2.0 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene 0.16 0.50 0.13 ug/l J
135-98-8 sec-Butylbenzene 1.1 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.29 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 54
FA31078 33.2
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-2
Lab Sample ID:FA31078-2 Date Sampled:01/28/16
Matrix:AQ - Ground Water Date Received:01/29/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 1.6 0.50 0.13 ug/l
100-41-4 Ethylbenzene 0.73 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene 0.65 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 5.8 0.50 0.13 ug/l
91-20-3 Naphthalene 2.0 0.50 0.13 ug/l
103-65-1 n-Propylbenzene 0.46 0.50 0.13 ug/l J
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene 0.16 0.50 0.13 ug/l J
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.14 ug/l
95-63-6 1,2,4-Trimethylbenzene 0.74 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 0.75 1.0 0.18 ug/l J
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)0.75 1.5 0.31 ug/l J
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 92%70-130%
17060-07-0 1,2-Dichloroethane-D4 89%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 54
FA31078 33.2
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-3
Lab Sample ID:FA31078-3 Date Sampled:01/28/16
Matrix:AQ - Ground Water Date Received:01/29/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0199100.D 1 02/01/16 TD n/a n/a VA1869
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 17.2 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene 1.6 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene 1.3 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.29 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 54
FA31078 33.3
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-3
Lab Sample ID:FA31078-3 Date Sampled:01/28/16
Matrix:AQ - Ground Water Date Received:01/29/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 0.81 0.50 0.13 ug/l
100-41-4 Ethylbenzene 23.3 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene 4.5 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene 0.14 0.50 0.13 ug/l J
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 4.9 0.50 0.13 ug/l
91-20-3 Naphthalene 11.3 0.50 0.13 ug/l
103-65-1 n-Propylbenzene 10.2 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene 1.7 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.14 ug/l
95-63-6 1,2,4-Trimethylbenzene 0.62 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene 0.88 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 4.3 1.0 0.18 ug/l
95-47-6 o-Xylene 0.97 0.50 0.13 ug/l
1330-20-7 Xylene (total)5.2 1.5 0.31 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 94%70-130%
17060-07-0 1,2-Dichloroethane-D4 90%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
13 of 54
FA31078 33.3
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-4
Lab Sample ID:FA31078-4 Date Sampled:01/28/16
Matrix:AQ - Ground Water Date Received:01/29/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0199101.D 100 02/01/16 TD n/a n/a VA1869
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 168 50 13 ug/l
108-86-1 Bromobenzene ND 50 13 ug/l
74-97-5 Bromochloromethane ND 50 13 ug/l
75-27-4 Bromodichloromethane ND 50 13 ug/l
75-25-2 Bromoform ND 50 13 ug/l
104-51-8 n-Butylbenzene 69.9 50 13 ug/l
135-98-8 sec-Butylbenzene 31.7 50 13 ug/l J
98-06-6 tert-Butylbenzene ND 50 13 ug/l
56-23-5 Carbon Tetrachloride ND 50 13 ug/l
108-90-7 Chlorobenzene ND 50 13 ug/l
75-00-3 Chloroethane ND 50 20 ug/l
67-66-3 Chloroform ND 50 13 ug/l
95-49-8 o-Chlorotoluene 98.2 50 13 ug/l
106-43-4 p-Chlorotoluene ND 50 13 ug/l
124-48-1 Dibromochloromethane ND 50 13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 50 29 ug/l
106-93-4 1,2-Dibromoethane ND 50 13 ug/l
75-71-8 Dichlorodifluoromethane ND 50 20 ug/l
95-50-1 1,2-Dichlorobenzene ND 50 13 ug/l
541-73-1 1,3-Dichlorobenzene ND 50 13 ug/l
106-46-7 1,4-Dichlorobenzene ND 50 13 ug/l
75-34-3 1,1-Dichloroethane ND 50 13 ug/l
107-06-2 1,2-Dichloroethane ND 50 13 ug/l
75-35-4 1,1-Dichloroethylene ND 50 13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 50 13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 50 13 ug/l
78-87-5 1,2-Dichloropropane ND 50 13 ug/l
142-28-9 1,3-Dichloropropane ND 50 13 ug/l
594-20-7 2,2-Dichloropropane ND 50 13 ug/l
563-58-6 1,1-Dichloropropene ND 50 13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 50 13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 50 13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
14 of 54
FA31078 33.4
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-4
Lab Sample ID:FA31078-4 Date Sampled:01/28/16
Matrix:AQ - Ground Water Date Received:01/29/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 50 13 ug/l
100-41-4 Ethylbenzene 1020 50 13 ug/l
87-68-3 Hexachlorobutadiene ND 50 13 ug/l
98-82-8 Isopropylbenzene 101 50 13 ug/l
99-87-6 p-Isopropyltoluene 19.9 50 13 ug/l J
74-83-9 Methyl Bromide ND 50 20 ug/l
74-87-3 Methyl Chloride ND 50 20 ug/l
74-95-3 Methylene Bromide ND 50 13 ug/l
75-09-2 Methylene Chloride 190 200 100 ug/l JB
1634-04-4 Methyl Tert Butyl Ether ND 50 13 ug/l
91-20-3 Naphthalene 523 50 13 ug/l
103-65-1 n-Propylbenzene 365 50 13 ug/l
100-42-5 Styrene ND 50 13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 50 13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 50 13 ug/l
127-18-4 Tetrachloroethylene ND 50 13 ug/l
108-88-3 Toluene 2640 50 13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 50 13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 50 13 ug/l
71-55-6 1,1,1-Trichloroethane ND 50 13 ug/l
79-00-5 1,1,2-Trichloroethane ND 50 13 ug/l
79-01-6 Trichloroethylene ND 50 13 ug/l
75-69-4 Trichlorofluoromethane ND 50 20 ug/l
96-18-4 1,2,3-Trichloropropane ND 50 14 ug/l
95-63-6 1,2,4-Trimethylbenzene 2690 50 13 ug/l
108-67-8 1,3,5-Trimethylbenzene 865 50 13 ug/l
75-01-4 Vinyl Chloride ND 50 13 ug/l
m,p-Xylene 3740 100 18 ug/l
95-47-6 o-Xylene 1420 50 13 ug/l
1330-20-7 Xylene (total)5160 150 31 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 91%70-130%
17060-07-0 1,2-Dichloroethane-D4 90%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
15 of 54
FA31078 33.4
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-5
Lab Sample ID:FA31078-5 Date Sampled:01/28/16
Matrix:AQ - Ground Water Date Received:01/29/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0199102.D 1 02/01/16 TD n/a n/a VA1869
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.29 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
16 of 54
FA31078 33.5
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-5
Lab Sample ID:FA31078-5 Date Sampled:01/28/16
Matrix:AQ - Ground Water Date Received:01/29/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 2.3 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene 0.66 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene 0.21 0.50 0.13 ug/l J
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.14 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.18 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.31 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 93%70-130%
17060-07-0 1,2-Dichloroethane-D4 89%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 97%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
17 of 54
FA31078 33.5
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-7
Lab Sample ID:FA31078-6 Date Sampled:01/28/16
Matrix:AQ - Ground Water Date Received:01/29/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E043731.D 1 02/02/16 TD n/a n/a VE1446
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.29 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
18 of 54
FA31078 33.6
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-7
Lab Sample ID:FA31078-6 Date Sampled:01/28/16
Matrix:AQ - Ground Water Date Received:01/29/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene 0.27 0.50 0.13 ug/l J
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.14 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.18 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.31 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
2037-26-5 Toluene-D8 94%70-130%
460-00-4 4-Bromofluorobenzene 104%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
19 of 54
FA31078 33.6
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-8
Lab Sample ID:FA31078-7 Date Sampled:01/28/16
Matrix:AQ - Ground Water Date Received:01/29/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E043732.D 1 02/02/16 TD n/a n/a VE1446
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.29 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane 0.17 0.50 0.13 ug/l J
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
20 of 54
FA31078 33.7
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-8
Lab Sample ID:FA31078-7 Date Sampled:01/28/16
Matrix:AQ - Ground Water Date Received:01/29/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 0.48 0.50 0.13 ug/l J
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 8.8 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.14 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.18 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.31 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 108%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 105%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
21 of 54
FA31078 33.7
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-13
Lab Sample ID:FA31078-8 Date Sampled:01/28/16
Matrix:AQ - Ground Water Date Received:01/29/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E043733.D 10 02/02/16 TD n/a n/a VE1446
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 270 5.0 1.3 ug/l
108-86-1 Bromobenzene ND 5.0 1.3 ug/l
74-97-5 Bromochloromethane ND 5.0 1.3 ug/l
75-27-4 Bromodichloromethane ND 5.0 1.3 ug/l
75-25-2 Bromoform ND 5.0 1.3 ug/l
104-51-8 n-Butylbenzene 2.4 5.0 1.3 ug/l J
135-98-8 sec-Butylbenzene 2.5 5.0 1.3 ug/l J
98-06-6 tert-Butylbenzene ND 5.0 1.3 ug/l
56-23-5 Carbon Tetrachloride ND 5.0 1.3 ug/l
108-90-7 Chlorobenzene ND 5.0 1.3 ug/l
75-00-3 Chloroethane ND 5.0 2.0 ug/l
67-66-3 Chloroform ND 5.0 1.3 ug/l
95-49-8 o-Chlorotoluene ND 5.0 1.3 ug/l
106-43-4 p-Chlorotoluene ND 5.0 1.3 ug/l
124-48-1 Dibromochloromethane ND 5.0 1.3 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 5.0 2.9 ug/l
106-93-4 1,2-Dibromoethane ND 5.0 1.3 ug/l
75-71-8 Dichlorodifluoromethane ND 5.0 2.0 ug/l
95-50-1 1,2-Dichlorobenzene ND 5.0 1.3 ug/l
541-73-1 1,3-Dichlorobenzene ND 5.0 1.3 ug/l
106-46-7 1,4-Dichlorobenzene ND 5.0 1.3 ug/l
75-34-3 1,1-Dichloroethane ND 5.0 1.3 ug/l
107-06-2 1,2-Dichloroethane ND 5.0 1.3 ug/l
75-35-4 1,1-Dichloroethylene ND 5.0 1.3 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.3 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.3 ug/l
78-87-5 1,2-Dichloropropane ND 5.0 1.3 ug/l
142-28-9 1,3-Dichloropropane ND 5.0 1.3 ug/l
594-20-7 2,2-Dichloropropane ND 5.0 1.3 ug/l
563-58-6 1,1-Dichloropropene ND 5.0 1.3 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.3 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.3 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
22 of 54
FA31078 33.8
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-13
Lab Sample ID:FA31078-8 Date Sampled:01/28/16
Matrix:AQ - Ground Water Date Received:01/29/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 5.0 1.3 ug/l
100-41-4 Ethylbenzene 72.1 5.0 1.3 ug/l
87-68-3 Hexachlorobutadiene ND 5.0 1.3 ug/l
98-82-8 Isopropylbenzene 7.7 5.0 1.3 ug/l
99-87-6 p-Isopropyltoluene ND 5.0 1.3 ug/l
74-83-9 Methyl Bromide ND 5.0 2.0 ug/l
74-87-3 Methyl Chloride ND 5.0 2.0 ug/l
74-95-3 Methylene Bromide ND 5.0 1.3 ug/l
75-09-2 Methylene Chloride 20.6 20 10 ug/l
1634-04-4 Methyl Tert Butyl Ether 3.7 5.0 1.3 ug/l J
91-20-3 Naphthalene 44.1 5.0 1.3 ug/l
103-65-1 n-Propylbenzene 12.3 5.0 1.3 ug/l
100-42-5 Styrene ND 5.0 1.3 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 5.0 1.3 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 1.3 ug/l
127-18-4 Tetrachloroethylene ND 5.0 1.3 ug/l
108-88-3 Toluene 4.0 5.0 1.3 ug/l J
87-61-6 1,2,3-Trichlorobenzene ND 5.0 1.3 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.3 ug/l
71-55-6 1,1,1-Trichloroethane ND 5.0 1.3 ug/l
79-00-5 1,1,2-Trichloroethane ND 5.0 1.3 ug/l
79-01-6 Trichloroethylene ND 5.0 1.3 ug/l
75-69-4 Trichlorofluoromethane ND 5.0 2.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 5.0 1.4 ug/l
95-63-6 1,2,4-Trimethylbenzene 6.9 5.0 1.3 ug/l
108-67-8 1,3,5-Trimethylbenzene 6.0 5.0 1.3 ug/l
75-01-4 Vinyl Chloride ND 5.0 1.3 ug/l
m,p-Xylene 83.8 10 1.8 ug/l
95-47-6 o-Xylene ND 5.0 1.3 ug/l
1330-20-7 Xylene (total)83.8 15 3.1 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 108%70-130%
17060-07-0 1,2-Dichloroethane-D4 113%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 103%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
23 of 54
FA31078 33.8
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-14
Lab Sample ID:FA31078-9 Date Sampled:01/28/16
Matrix:AQ - Ground Water Date Received:01/29/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E043734.D 50 02/02/16 TD n/a n/a VE1446
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 2030 25 6.3 ug/l
108-86-1 Bromobenzene ND 25 6.3 ug/l
74-97-5 Bromochloromethane ND 25 6.3 ug/l
75-27-4 Bromodichloromethane ND 25 6.3 ug/l
75-25-2 Bromoform ND 25 6.3 ug/l
104-51-8 n-Butylbenzene 7.9 25 6.3 ug/l J
135-98-8 sec-Butylbenzene 6.3 25 6.3 ug/l J
98-06-6 tert-Butylbenzene ND 25 6.3 ug/l
56-23-5 Carbon Tetrachloride ND 25 6.3 ug/l
108-90-7 Chlorobenzene ND 25 6.3 ug/l
75-00-3 Chloroethane ND 25 10 ug/l
67-66-3 Chloroform ND 25 6.3 ug/l
95-49-8 o-Chlorotoluene ND 25 6.3 ug/l
106-43-4 p-Chlorotoluene ND 25 6.3 ug/l
124-48-1 Dibromochloromethane ND 25 6.3 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 25 14 ug/l
106-93-4 1,2-Dibromoethane ND 25 6.3 ug/l
75-71-8 Dichlorodifluoromethane ND 25 10 ug/l
95-50-1 1,2-Dichlorobenzene ND 25 6.3 ug/l
541-73-1 1,3-Dichlorobenzene ND 25 6.3 ug/l
106-46-7 1,4-Dichlorobenzene ND 25 6.3 ug/l
75-34-3 1,1-Dichloroethane ND 25 6.3 ug/l
107-06-2 1,2-Dichloroethane ND 25 6.3 ug/l
75-35-4 1,1-Dichloroethylene ND 25 6.3 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 25 6.3 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 25 6.3 ug/l
78-87-5 1,2-Dichloropropane ND 25 6.3 ug/l
142-28-9 1,3-Dichloropropane ND 25 6.3 ug/l
594-20-7 2,2-Dichloropropane ND 25 6.3 ug/l
563-58-6 1,1-Dichloropropene ND 25 6.3 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 25 6.3 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 25 6.3 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
24 of 54
FA31078 33.9
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-14
Lab Sample ID:FA31078-9 Date Sampled:01/28/16
Matrix:AQ - Ground Water Date Received:01/29/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 25 6.3 ug/l
100-41-4 Ethylbenzene 478 25 6.3 ug/l
87-68-3 Hexachlorobutadiene ND 25 6.3 ug/l
98-82-8 Isopropylbenzene 27.8 25 6.3 ug/l
99-87-6 p-Isopropyltoluene ND 25 6.3 ug/l
74-83-9 Methyl Bromide ND 25 10 ug/l
74-87-3 Methyl Chloride ND 25 10 ug/l
74-95-3 Methylene Bromide ND 25 6.3 ug/l
75-09-2 Methylene Chloride 102 100 50 ug/l
1634-04-4 Methyl Tert Butyl Ether 11.2 25 6.3 ug/l J
91-20-3 Naphthalene 92.3 25 6.3 ug/l
103-65-1 n-Propylbenzene 76.3 25 6.3 ug/l
100-42-5 Styrene ND 25 6.3 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 25 6.3 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 25 6.3 ug/l
127-18-4 Tetrachloroethylene ND 25 6.3 ug/l
108-88-3 Toluene 16.0 25 6.3 ug/l J
87-61-6 1,2,3-Trichlorobenzene ND 25 6.3 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 25 6.3 ug/l
71-55-6 1,1,1-Trichloroethane ND 25 6.3 ug/l
79-00-5 1,1,2-Trichloroethane ND 25 6.3 ug/l
79-01-6 Trichloroethylene ND 25 6.3 ug/l
75-69-4 Trichlorofluoromethane ND 25 10 ug/l
96-18-4 1,2,3-Trichloropropane ND 25 7.0 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 25 6.3 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 25 6.3 ug/l
75-01-4 Vinyl Chloride ND 25 6.3 ug/l
m,p-Xylene 126 50 9.2 ug/l
95-47-6 o-Xylene 8.2 25 6.3 ug/l J
1330-20-7 Xylene (total)134 75 15 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 107%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 103%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
25 of 54
FA31078 33.9
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-15
Lab Sample ID:FA31078-10 Date Sampled:01/28/16
Matrix:AQ - Ground Water Date Received:01/29/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0199146.D 1 02/03/16 TD n/a n/a VA1871
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.29 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
26 of 54
FA31078 33.10
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-15
Lab Sample ID:FA31078-10 Date Sampled:01/28/16
Matrix:AQ - Ground Water Date Received:01/29/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.58 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.14 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.18 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.31 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 98%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
27 of 54
FA31078 33.10
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-16
Lab Sample ID:FA31078-11 Date Sampled:01/28/16
Matrix:AQ - Ground Water Date Received:01/29/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E043736.D 1 02/02/16 TD n/a n/a VE1446
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.29 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
28 of 54
FA31078 33.11
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-16
Lab Sample ID:FA31078-11 Date Sampled:01/28/16
Matrix:AQ - Ground Water Date Received:01/29/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.14 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.18 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.31 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 105%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
29 of 54
FA31078 33.11
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-18
Lab Sample ID:FA31078-12 Date Sampled:01/28/16
Matrix:AQ - Ground Water Date Received:01/29/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E043742.D 1 02/02/16 TD n/a n/a VE1446
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene 4.0 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.29 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene 3.9 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
30 of 54
FA31078 33.12
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-18
Lab Sample ID:FA31078-12 Date Sampled:01/28/16
Matrix:AQ - Ground Water Date Received:01/29/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 2.4 0.50 0.13 ug/l
91-20-3 Naphthalene 0.17 0.50 0.13 ug/l J
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.14 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.18 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.31 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 105%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
31 of 54
FA31078 33.12
Accutest Laboratories
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Southeast
Section 4
32 of 54
FA31078 4
FA31078: Chain of Custody
Page 1 of 3
33 of 54
FA31078 44.1
FA31078: Chain of Custody
Page 2 of 3
34 of 54
FA31078 44.1
FA31078: Chain of Custody
Page 3 of 3
35 of 54
FA31078 44.1
Accutest Laboratories
GC/MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Southeast
Section 5
36 of 54
FA31078 5
Method Blank Summary Page 1 of 2
Job Number:FA31078
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1869-MB A0199083.D 1 02/01/16 TD n/a n/a VA1869
The QC reported here applies to the following samples:Method: SM 6200B
FA31078-1, FA31078-2, FA31078-3, FA31078-4, FA31078-5
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.29 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
37 of 54
FA31078 55.1.1
Method Blank Summary Page 2 of 2
Job Number:FA31078
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1869-MB A0199083.D 1 02/01/16 TD n/a n/a VA1869
The QC reported here applies to the following samples:Method: SM 6200B
FA31078-1, FA31078-2, FA31078-3, FA31078-4, FA31078-5
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride 2.1 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.14 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.18 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.31 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 99%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
38 of 54
FA31078 55.1.1
Method Blank Summary Page 1 of 2
Job Number:FA31078
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1446-MB E043727.D 1 02/02/16 TD n/a n/a VE1446
The QC reported here applies to the following samples:Method: SM 6200B
FA31078-6, FA31078-7, FA31078-8, FA31078-9, FA31078-11, FA31078-12
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.29 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
39 of 54
FA31078 55.1.2
Method Blank Summary Page 2 of 2
Job Number:FA31078
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1446-MB E043727.D 1 02/02/16 TD n/a n/a VE1446
The QC reported here applies to the following samples:Method: SM 6200B
FA31078-6, FA31078-7, FA31078-8, FA31078-9, FA31078-11, FA31078-12
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.14 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.18 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.31 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 104%70-130%
40 of 54
FA31078 55.1.2
Method Blank Summary Page 1 of 2
Job Number:FA31078
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1871-MB A0199145.D 1 02/03/16 TD n/a n/a VA1871
The QC reported here applies to the following samples:Method: SM 6200B
FA31078-10
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.29 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
41 of 54
FA31078 55.1.3
Method Blank Summary Page 2 of 2
Job Number:FA31078
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1871-MB A0199145.D 1 02/03/16 TD n/a n/a VA1871
The QC reported here applies to the following samples:Method: SM 6200B
FA31078-10
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride 2.3 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.14 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.18 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.31 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 98%70-130%
17060-07-0 1,2-Dichloroethane-D4 95%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
42 of 54
FA31078 55.1.3
Blank Spike Summary Page 1 of 2
Job Number:FA31078
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1869-BS A0199081.D 1 02/01/16 TD n/a n/a VA1869
The QC reported here applies to the following samples:Method: SM 6200B
FA31078-1, FA31078-2, FA31078-3, FA31078-4, FA31078-5
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 11.5 115 70-130
108-86-1 Bromobenzene 10 11.1 111 70-130
74-97-5 Bromochloromethane 10 10.5 105 70-130
75-27-4 Bromodichloromethane 10 11.4 114 70-130
75-25-2 Bromoform 10 10.9 109 70-130
104-51-8 n-Butylbenzene 10 12.0 120 70-130
135-98-8 sec-Butylbenzene 10 12.2 122 70-130
98-06-6 tert-Butylbenzene 10 11.6 116 70-130
56-23-5 Carbon Tetrachloride 10 11.7 117 70-130
108-90-7 Chlorobenzene 10 11.1 111 70-130
75-00-3 Chloroethane 10 11.6 116 60-140
67-66-3 Chloroform 10 11.3 113 70-130
95-49-8 o-Chlorotoluene 10 11.7 117 70-130
106-43-4 p-Chlorotoluene 10 11.6 116 70-130
124-48-1 Dibromochloromethane 10 11.2 112 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 10.3 103 70-130
106-93-4 1,2-Dibromoethane 10 10.9 109 70-130
75-71-8 Dichlorodifluoromethane 10 10.9 109 60-140
95-50-1 1,2-Dichlorobenzene 10 11.3 113 70-130
541-73-1 1,3-Dichlorobenzene 10 11.6 116 70-130
106-46-7 1,4-Dichlorobenzene 10 11.1 111 70-130
75-34-3 1,1-Dichloroethane 10 11.7 117 70-130
107-06-2 1,2-Dichloroethane 10 10.5 105 70-130
75-35-4 1,1-Dichloroethylene 10 12.2 122 70-130
156-59-2 cis-1,2-Dichloroethylene 10 10.9 109 70-130
156-60-5 trans-1,2-Dichloroethylene 10 12.5 125 70-130
78-87-5 1,2-Dichloropropane 10 11.1 111 70-130
142-28-9 1,3-Dichloropropane 10 10.6 106 70-130
594-20-7 2,2-Dichloropropane 10 11.9 119 70-130
563-58-6 1,1-Dichloropropene 10 12.0 120 70-130
10061-01-5 cis-1,3-Dichloropropene 10 11.4 114 70-130
10061-02-6 trans-1,3-Dichloropropene 10 12.0 120 70-130
108-20-3 Di-Isopropyl Ether 10 10.7 107 70-130
100-41-4 Ethylbenzene 10 11.4 114 70-130
87-68-3 Hexachlorobutadiene 10 10.9 109 70-130
98-82-8 Isopropylbenzene 10 12.0 120 70-130
* = Outside of Control Limits.
43 of 54
FA31078 55.2.1
Blank Spike Summary Page 2 of 2
Job Number:FA31078
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1869-BS A0199081.D 1 02/01/16 TD n/a n/a VA1869
The QC reported here applies to the following samples:Method: SM 6200B
FA31078-1, FA31078-2, FA31078-3, FA31078-4, FA31078-5
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 11.8 118 70-130
74-83-9 Methyl Bromide 10 11.1 111 60-140
74-87-3 Methyl Chloride 10 11.2 112 60-140
74-95-3 Methylene Bromide 10 11.2 112 70-130
75-09-2 Methylene Chloride 10 12.0 120 70-130
1634-04-4 Methyl Tert Butyl Ether 10 10.6 106 70-130
91-20-3 Naphthalene 10 12.3 123 70-130
103-65-1 n-Propylbenzene 10 12.1 121 70-130
100-42-5 Styrene 10 11.6 116 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 11.2 112 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 10.7 107 70-130
127-18-4 Tetrachloroethylene 10 11.8 118 70-130
108-88-3 Toluene 10 11.2 112 70-130
87-61-6 1,2,3-Trichlorobenzene 10 11.2 112 70-130
120-82-1 1,2,4-Trichlorobenzene 10 11.4 114 70-130
71-55-6 1,1,1-Trichloroethane 10 11.6 116 70-130
79-00-5 1,1,2-Trichloroethane 10 10.9 109 70-130
79-01-6 Trichloroethylene 10 11.6 116 70-130
75-69-4 Trichlorofluoromethane 10 11.1 111 60-140
96-18-4 1,2,3-Trichloropropane 10 11.0 110 70-130
95-63-6 1,2,4-Trimethylbenzene 10 11.7 117 70-130
108-67-8 1,3,5-Trimethylbenzene 10 11.5 115 70-130
75-01-4 Vinyl Chloride 10 11.4 114 60-140
m,p-Xylene 20 23.1 116 70-130
95-47-6 o-Xylene 10 11.6 116 70-130
1330-20-7 Xylene (total)30 34.7 116 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 98%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
* = Outside of Control Limits.
44 of 54
FA31078 55.2.1
Blank Spike Summary Page 1 of 2
Job Number:FA31078
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1446-BS E043725.D 1 02/02/16 TD n/a n/a VE1446
The QC reported here applies to the following samples:Method: SM 6200B
FA31078-6, FA31078-7, FA31078-8, FA31078-9, FA31078-11, FA31078-12
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 10.1 101 70-130
108-86-1 Bromobenzene 10 9.9 99 70-130
74-97-5 Bromochloromethane 10 9.3 93 70-130
75-27-4 Bromodichloromethane 10 10.1 101 70-130
75-25-2 Bromoform 10 10 100 70-130
104-51-8 n-Butylbenzene 10 10.3 103 70-130
135-98-8 sec-Butylbenzene 10 10.4 104 70-130
98-06-6 tert-Butylbenzene 10 10.0 100 70-130
56-23-5 Carbon Tetrachloride 10 10.4 104 70-130
108-90-7 Chlorobenzene 10 9.6 96 70-130
75-00-3 Chloroethane 10 12.9 129 60-140
67-66-3 Chloroform 10 10.4 104 70-130
95-49-8 o-Chlorotoluene 10 10.3 103 70-130
106-43-4 p-Chlorotoluene 10 10.4 104 70-130
124-48-1 Dibromochloromethane 10 10.2 102 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 9.3 93 70-130
106-93-4 1,2-Dibromoethane 10 9.6 96 70-130
75-71-8 Dichlorodifluoromethane 10 12.0 120 60-140
95-50-1 1,2-Dichlorobenzene 10 9.9 99 70-130
541-73-1 1,3-Dichlorobenzene 10 10.3 103 70-130
106-46-7 1,4-Dichlorobenzene 10 9.9 99 70-130
75-34-3 1,1-Dichloroethane 10 10.6 106 70-130
107-06-2 1,2-Dichloroethane 10 9.9 99 70-130
75-35-4 1,1-Dichloroethylene 10 10.9 109 70-130
156-59-2 cis-1,2-Dichloroethylene 10 9.8 98 70-130
156-60-5 trans-1,2-Dichloroethylene 10 11.3 113 70-130
78-87-5 1,2-Dichloropropane 10 9.9 99 70-130
142-28-9 1,3-Dichloropropane 10 9.3 93 70-130
594-20-7 2,2-Dichloropropane 10 10.6 106 70-130
563-58-6 1,1-Dichloropropene 10 10.5 105 70-130
10061-01-5 cis-1,3-Dichloropropene 10 10.0 100 70-130
10061-02-6 trans-1,3-Dichloropropene 10 10.8 108 70-130
108-20-3 Di-Isopropyl Ether 10 9.6 96 70-130
100-41-4 Ethylbenzene 10 10.0 100 70-130
87-68-3 Hexachlorobutadiene 10 10 100 70-130
98-82-8 Isopropylbenzene 10 10.2 102 70-130
* = Outside of Control Limits.
45 of 54
FA31078 55.2.2
Blank Spike Summary Page 2 of 2
Job Number:FA31078
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1446-BS E043725.D 1 02/02/16 TD n/a n/a VE1446
The QC reported here applies to the following samples:Method: SM 6200B
FA31078-6, FA31078-7, FA31078-8, FA31078-9, FA31078-11, FA31078-12
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 10.2 102 70-130
74-83-9 Methyl Bromide 10 12.8 128 60-140
74-87-3 Methyl Chloride 10 12.4 124 60-140
74-95-3 Methylene Bromide 10 9.9 99 70-130
75-09-2 Methylene Chloride 10 10.5 105 70-130
1634-04-4 Methyl Tert Butyl Ether 10 9.3 93 70-130
91-20-3 Naphthalene 10 10.6 106 70-130
103-65-1 n-Propylbenzene 10 10.6 106 70-130
100-42-5 Styrene 10 10.2 102 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 9.9 99 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 9.5 95 70-130
127-18-4 Tetrachloroethylene 10 9.9 99 70-130
108-88-3 Toluene 10 9.4 94 70-130
87-61-6 1,2,3-Trichlorobenzene 10 10.2 102 70-130
120-82-1 1,2,4-Trichlorobenzene 10 10.0 100 70-130
71-55-6 1,1,1-Trichloroethane 10 10.3 103 70-130
79-00-5 1,1,2-Trichloroethane 10 9.6 96 70-130
79-01-6 Trichloroethylene 10 10.1 101 70-130
75-69-4 Trichlorofluoromethane 10 12.4 124 60-140
96-18-4 1,2,3-Trichloropropane 10 9.7 97 70-130
95-63-6 1,2,4-Trimethylbenzene 10 10.2 102 70-130
108-67-8 1,3,5-Trimethylbenzene 10 10.1 101 70-130
75-01-4 Vinyl Chloride 10 12.2 122 60-140
m,p-Xylene 20 20.3 102 70-130
95-47-6 o-Xylene 10 10 100 70-130
1330-20-7 Xylene (total)30 30.2 101 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
* = Outside of Control Limits.
46 of 54
FA31078 55.2.2
Blank Spike Summary Page 1 of 2
Job Number:FA31078
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1871-BS A0199158.D 1 02/03/16 TD n/a n/a VA1871
The QC reported here applies to the following samples:Method: SM 6200B
FA31078-10
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 10.1 101 70-130
108-86-1 Bromobenzene 10 10.0 100 70-130
74-97-5 Bromochloromethane 10 9.8 98 70-130
75-27-4 Bromodichloromethane 10 10.1 101 70-130
75-25-2 Bromoform 10 9.9 99 70-130
104-51-8 n-Butylbenzene 10 10.4 104 70-130
135-98-8 sec-Butylbenzene 10 10.5 105 70-130
98-06-6 tert-Butylbenzene 10 10.1 101 70-130
56-23-5 Carbon Tetrachloride 10 10.5 105 70-130
108-90-7 Chlorobenzene 10 9.9 99 70-130
75-00-3 Chloroethane 10 8.7 87 60-140
67-66-3 Chloroform 10 10.2 102 70-130
95-49-8 o-Chlorotoluene 10 10.3 103 70-130
106-43-4 p-Chlorotoluene 10 10.2 102 70-130
124-48-1 Dibromochloromethane 10 10.1 101 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 10.2 102 70-130
106-93-4 1,2-Dibromoethane 10 10 100 70-130
75-71-8 Dichlorodifluoromethane 10 8.5 85 60-140
95-50-1 1,2-Dichlorobenzene 10 10 100 70-130
541-73-1 1,3-Dichlorobenzene 10 10.1 101 70-130
106-46-7 1,4-Dichlorobenzene 10 9.8 98 70-130
75-34-3 1,1-Dichloroethane 10 10.1 101 70-130
107-06-2 1,2-Dichloroethane 10 9.8 98 70-130
75-35-4 1,1-Dichloroethylene 10 10.3 103 70-130
156-59-2 cis-1,2-Dichloroethylene 10 9.8 98 70-130
156-60-5 trans-1,2-Dichloroethylene 10 10.1 101 70-130
78-87-5 1,2-Dichloropropane 10 9.9 99 70-130
142-28-9 1,3-Dichloropropane 10 9.8 98 70-130
594-20-7 2,2-Dichloropropane 10 10.1 101 70-130
563-58-6 1,1-Dichloropropene 10 10.3 103 70-130
10061-01-5 cis-1,3-Dichloropropene 10 9.9 99 70-130
10061-02-6 trans-1,3-Dichloropropene 10 10.0 100 70-130
108-20-3 Di-Isopropyl Ether 10 9.9 99 70-130
100-41-4 Ethylbenzene 10 10.1 101 70-130
87-68-3 Hexachlorobutadiene 10 9.6 96 70-130
98-82-8 Isopropylbenzene 10 10.3 103 70-130
* = Outside of Control Limits.
47 of 54
FA31078 55.2.3
Blank Spike Summary Page 2 of 2
Job Number:FA31078
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1871-BS A0199158.D 1 02/03/16 TD n/a n/a VA1871
The QC reported here applies to the following samples:Method: SM 6200B
FA31078-10
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 10.4 104 70-130
74-83-9 Methyl Bromide 10 8.4 84 60-140
74-87-3 Methyl Chloride 10 9.0 90 60-140
74-95-3 Methylene Bromide 10 10.1 101 70-130
75-09-2 Methylene Chloride 10 11.1 111 70-130
1634-04-4 Methyl Tert Butyl Ether 10 10 100 70-130
91-20-3 Naphthalene 10 10.6 106 70-130
103-65-1 n-Propylbenzene 10 10.3 103 70-130
100-42-5 Styrene 10 10.4 104 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 10.0 100 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 10.2 102 70-130
127-18-4 Tetrachloroethylene 10 10.2 102 70-130
108-88-3 Toluene 10 9.9 99 70-130
87-61-6 1,2,3-Trichlorobenzene 10 10.3 103 70-130
120-82-1 1,2,4-Trichlorobenzene 10 10 100 70-130
71-55-6 1,1,1-Trichloroethane 10 10.3 103 70-130
79-00-5 1,1,2-Trichloroethane 10 10.0 100 70-130
79-01-6 Trichloroethylene 10 10.2 102 70-130
75-69-4 Trichlorofluoromethane 10 8.9 89 60-140
96-18-4 1,2,3-Trichloropropane 10 10 100 70-130
95-63-6 1,2,4-Trimethylbenzene 10 10.4 104 70-130
108-67-8 1,3,5-Trimethylbenzene 10 10.3 103 70-130
75-01-4 Vinyl Chloride 10 8.5 85 60-140
m,p-Xylene 20 20.4 102 70-130
95-47-6 o-Xylene 10 10 100 70-130
1330-20-7 Xylene (total)30 30.4 101 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
* = Outside of Control Limits.
48 of 54
FA31078 55.2.3
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA31078
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA31075-2MS A0199103.D 1 02/01/16 TD n/a n/a VA1869
FA31075-2MSD A0199104.D 1 02/01/16 TD n/a n/a VA1869
FA31075-2 A0199087.D 1 02/01/16 TD n/a n/a VA1869
The QC reported here applies to the following samples:Method: SM 6200B
FA31078-1, FA31078-2, FA31078-3, FA31078-4, FA31078-5
FA31075-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene ND 10 10.4 104 10 7.4 74 34*70-130/20
108-86-1 Bromobenzene ND 10 10.2 102 10 7.4 74 32*70-130/20
74-97-5 Bromochloromethane ND 10 9.1 91 10 6.9 69*28*70-130/20
75-27-4 Bromodichloromethane ND 10 9.7 97 10 6.8 68*35*70-130/20
75-25-2 Bromoform ND 10 8.6 86 10 6.4 64*29*70-130/20
104-51-8 n-Butylbenzene ND 10 10.3 103 10 7.1 71 37*70-130/20
135-98-8 sec-Butylbenzene ND 10 10.8 108 10 7.6 76 35*70-130/20
98-06-6 tert-Butylbenzene ND 10 10.3 103 10 7.3 73 34*70-130/20
56-23-5 Carbon Tetrachloride ND 10 9.7 97 10 6.6 66*38*70-130/20
108-90-7 Chlorobenzene ND 10 10.0 100 10 7.0 70 35*70-130/20
75-00-3 Chloroethane ND 10 14.1 141*10 9.9 99 35*60-140/20
67-66-3 Chloroform ND 10 9.9 99 10 7.2 72 32*70-130/20
95-49-8 o-Chlorotoluene ND 10 10.5 105 10 7.4 74 35*70-130/20
106-43-4 p-Chlorotoluene ND 10 10.4 104 10 7.3 73 35*70-130/20
124-48-1 Dibromochloromethane ND 10 9.2 92 10 6.6 66*33*70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 10 8.7 87 10 7.0 70 22*70-130/20
106-93-4 1,2-Dibromoethane ND 10 9.8 98 10 7.5 75 27*70-130/20
75-71-8 Dichlorodifluoromethane ND 10 12.2 122 10 8.5 85 36*60-140/20
95-50-1 1,2-Dichlorobenzene ND 10 10.2 102 10 7.4 74 32*70-130/20
541-73-1 1,3-Dichlorobenzene ND 10 10.5 105 10 7.4 74 35*70-130/20
106-46-7 1,4-Dichlorobenzene ND 10 10 100 10 7.1 71 34*70-130/20
75-34-3 1,1-Dichloroethane ND 10 10.5 105 10 7.5 75 33*70-130/20
107-06-2 1,2-Dichloroethane ND 10 9.0 90 10 6.9 69*26*70-130/20
75-35-4 1,1-Dichloroethylene ND 10 10.5 105 10 7.4 74 35*70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 10 9.8 98 10 7.0 70 33*70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 10 10.9 109 10 7.7 77 34*70-130/20
78-87-5 1,2-Dichloropropane ND 10 10.3 103 10 7.5 75 31*70-130/20
142-28-9 1,3-Dichloropropane ND 10 9.5 95 10 7.3 73 26*70-130/20
594-20-7 2,2-Dichloropropane ND 10 9.5 95 10 6.7 67*35*70-130/20
563-58-6 1,1-Dichloropropene ND 10 10.5 105 10 7.3 73 36*70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 10 10.0 100 10 7.0 70 35*70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 10 10.3 103 10 7.5 75 31*70-130/20
108-20-3 Di-Isopropyl Ether 1.1 10 10.4 93 10 7.6 65*31*70-130/20
100-41-4 Ethylbenzene ND 10 10.2 102 10 7.2 72 34*70-130/20
87-68-3 Hexachlorobutadiene ND 10 9.1 91 10 6.4 64*35*70-130/20
98-82-8 Isopropylbenzene ND 10 10.6 106 10 7.5 75 34*70-130/20
* = Outside of Control Limits.
49 of 54
FA31078 55.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA31078
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA31075-2MS A0199103.D 1 02/01/16 TD n/a n/a VA1869
FA31075-2MSD A0199104.D 1 02/01/16 TD n/a n/a VA1869
FA31075-2 A0199087.D 1 02/01/16 TD n/a n/a VA1869
The QC reported here applies to the following samples:Method: SM 6200B
FA31078-1, FA31078-2, FA31078-3, FA31078-4, FA31078-5
FA31075-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 10 10.6 106 10 7.4 74 36*70-130/20
74-83-9 Methyl Bromide ND 10 13.4 134 10 9.5 95 34*60-140/20
74-87-3 Methyl Chloride ND 10 13.1 131 10 8.8 88 39*60-140/20
74-95-3 Methylene Bromide ND 10 9.7 97 10 7.5 75 26*70-130/20
75-09-2 Methylene Chloride ND 10 8.5 85 10 6.3 63*30*70-130/20
1634-04-4 Methyl Tert Butyl Ether 41.3 10 54.6 133* a 10 41.6 3* a 27*70-130/20
91-20-3 Naphthalene ND 10 10.8 108 10 8.2 82 27*70-130/20
103-65-1 n-Propylbenzene ND 10 10.9 109 10 7.6 76 36*70-130/20
100-42-5 Styrene ND 10 9.4 94 10 6.5 65*36*70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 10 9.8 98 10 6.8 68*36*70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 10 9.5 95 10 7.6 76 22*70-130/20
127-18-4 Tetrachloroethylene ND 10 10.3 103 10 7.1 71 37*70-130/20
108-88-3 Toluene ND 10 10.2 102 10 7.4 74 32*70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 10 10 100 10 7.3 73 31*70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 10 10.0 100 10 7.3 73 31*70-130/20
71-55-6 1,1,1-Trichloroethane ND 10 9.9 99 10 6.9 69*36*70-130/20
79-00-5 1,1,2-Trichloroethane ND 10 10 100 10 7.5 75 29*70-130/20
79-01-6 Trichloroethylene ND 10 10.1 101 10 7.0 70 36*70-130/20
75-69-4 Trichlorofluoromethane ND 10 12.3 123 10 8.6 86 35*60-140/20
96-18-4 1,2,3-Trichloropropane ND 10 9.8 98 10 7.7 77 24*70-130/20
95-63-6 1,2,4-Trimethylbenzene ND 10 10.5 105 10 7.3 73 36*70-130/20
108-67-8 1,3,5-Trimethylbenzene ND 10 10.4 104 10 7.3 73 35*70-130/20
75-01-4 Vinyl Chloride ND 10 13.4 134 10 9.4 94 35*60-140/20
m,p-Xylene ND 20 20.6 103 20 14.6 73 34*70-130/20
95-47-6 o-Xylene ND 10 10.3 103 10 7.3 73 34*70-130/20
1330-20-7 Xylene (total)ND 30 30.9 103 30 21.9 73 34*70-130/20
CAS No.Surrogate Recoveries MS MSD FA31075-2 Limits
1868-53-7 Dibromofluoromethane 96%96%99%70-130%
17060-07-0 1,2-Dichloroethane-D4 91%98%98%70-130%
2037-26-5 Toluene-D8 99%97%99%70-130%
460-00-4 4-Bromofluorobenzene 99%99%99%70-130%
(a) Outside control limits due to high level in sample relative to spike amount.
* = Outside of Control Limits.
50 of 54
FA31078 55.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA31078
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA31078-6MS E043748.D 1 02/02/16 TD n/a n/a VE1446
FA31078-6MSD E043749.D 1 02/02/16 TD n/a n/a VE1446
FA31078-6 E043731.D 1 02/02/16 TD n/a n/a VE1446
The QC reported here applies to the following samples:Method: SM 6200B
FA31078-6, FA31078-7, FA31078-8, FA31078-9, FA31078-11, FA31078-12
FA31078-6 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene ND 10 11.4 114 10 10.9 109 4 70-130/20
108-86-1 Bromobenzene ND 10 11.2 112 10 10.7 107 5 70-130/20
74-97-5 Bromochloromethane ND 10 11.0 110 10 10.6 106 4 70-130/20
75-27-4 Bromodichloromethane ND 10 11.4 114 10 10.6 106 7 70-130/20
75-25-2 Bromoform ND 10 10.6 106 10 9.7 97 9 70-130/20
104-51-8 n-Butylbenzene ND 10 10.7 107 10 10.3 103 4 70-130/20
135-98-8 sec-Butylbenzene ND 10 11.3 113 10 10.8 108 5 70-130/20
98-06-6 tert-Butylbenzene ND 10 10.9 109 10 10.6 106 3 70-130/20
56-23-5 Carbon Tetrachloride ND 10 11.9 119 10 10.9 109 9 70-130/20
108-90-7 Chlorobenzene ND 10 10.9 109 10 10.5 105 4 70-130/20
75-00-3 Chloroethane ND 10 15.5 155*10 14.2 142*9 60-140/20
67-66-3 Chloroform ND 10 11.4 114 10 11.1 111 3 70-130/20
95-49-8 o-Chlorotoluene ND 10 11.1 111 10 10.7 107 4 70-130/20
106-43-4 p-Chlorotoluene ND 10 11.1 111 10 10.7 107 4 70-130/20
124-48-1 Dibromochloromethane ND 10 11.2 112 10 10.5 105 6 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 10 10.3 103 10 9.9 99 4 70-130/20
106-93-4 1,2-Dibromoethane ND 10 11.4 114 10 11.0 110 4 70-130/20
75-71-8 Dichlorodifluoromethane ND 10 13.7 137 10 13.0 130 5 60-140/20
95-50-1 1,2-Dichlorobenzene ND 10 11.1 111 10 10.8 108 3 70-130/20
541-73-1 1,3-Dichlorobenzene ND 10 11.4 114 10 11.0 110 4 70-130/20
106-46-7 1,4-Dichlorobenzene ND 10 10.9 109 10 10.5 105 4 70-130/20
75-34-3 1,1-Dichloroethane ND 10 11.5 115 10 11.0 110 4 70-130/20
107-06-2 1,2-Dichloroethane ND 10 10.9 109 10 10.6 106 3 70-130/20
75-35-4 1,1-Dichloroethylene ND 10 11.7 117 10 10.9 109 7 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 10 11.0 110 10 10.7 107 3 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 10 12.1 121 10 11.5 115 5 70-130/20
78-87-5 1,2-Dichloropropane ND 10 11.0 110 10 10.7 107 3 70-130/20
142-28-9 1,3-Dichloropropane ND 10 10.6 106 10 10.3 103 3 70-130/20
594-20-7 2,2-Dichloropropane ND 10 11.3 113 10 10.8 108 5 70-130/20
563-58-6 1,1-Dichloropropene ND 10 11.7 117 10 11.2 112 4 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 10 10.7 107 10 10.2 102 5 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 10 11.2 112 10 10.7 107 5 70-130/20
108-20-3 Di-Isopropyl Ether ND 10 10.4 104 10 10.1 101 3 70-130/20
100-41-4 Ethylbenzene ND 10 11.4 114 10 10.9 109 4 70-130/20
87-68-3 Hexachlorobutadiene ND 10 10.1 101 10 10.4 104 3 70-130/20
98-82-8 Isopropylbenzene ND 10 11.8 118 10 11.2 112 5 70-130/20
* = Outside of Control Limits.
51 of 54
FA31078 55.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA31078
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA31078-6MS E043748.D 1 02/02/16 TD n/a n/a VE1446
FA31078-6MSD E043749.D 1 02/02/16 TD n/a n/a VE1446
FA31078-6 E043731.D 1 02/02/16 TD n/a n/a VE1446
The QC reported here applies to the following samples:Method: SM 6200B
FA31078-6, FA31078-7, FA31078-8, FA31078-9, FA31078-11, FA31078-12
FA31078-6 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 10 11.1 111 10 10.6 106 5 70-130/20
74-83-9 Methyl Bromide ND 10 15.0 150*10 14.4 144*4 60-140/20
74-87-3 Methyl Chloride ND 10 13.0 130 10 12.8 128 2 60-140/20
74-95-3 Methylene Bromide ND 10 11.4 114 10 11.0 110 4 70-130/20
75-09-2 Methylene Chloride ND 10 8.9 89 10 8.6 86 3 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 10 10.9 109 10 10.3 103 6 70-130/20
91-20-3 Naphthalene ND 10 16.8 168*10 13.0 130 26*70-130/20
103-65-1 n-Propylbenzene ND 10 11.4 114 10 10.9 109 4 70-130/20
100-42-5 Styrene ND 10 10.6 106 10 9.6 96 10 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 10 11.8 118 10 11.1 111 6 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 10 10.5 105 10 10.0 100 5 70-130/20
127-18-4 Tetrachloroethylene 0.27 J 10 11.8 115 10 11.4 111 3 70-130/20
108-88-3 Toluene ND 10 10.9 109 10 10.5 105 4 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 10 10.7 107 10 11.4 114 6 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 10 10.7 107 10 11.0 110 3 70-130/20
71-55-6 1,1,1-Trichloroethane ND 10 11.9 119 10 11.2 112 6 70-130/20
79-00-5 1,1,2-Trichloroethane ND 10 11.2 112 10 10.7 107 5 70-130/20
79-01-6 Trichloroethylene ND 10 11.5 115 10 11.1 111 4 70-130/20
75-69-4 Trichlorofluoromethane ND 10 14.3 143*10 13.5 135 6 60-140/20
96-18-4 1,2,3-Trichloropropane ND 10 11.2 112 10 10.5 105 6 70-130/20
95-63-6 1,2,4-Trimethylbenzene ND 10 11.4 114 10 10.6 106 7 70-130/20
108-67-8 1,3,5-Trimethylbenzene ND 10 10.7 107 10 10.1 101 6 70-130/20
75-01-4 Vinyl Chloride ND 10 13.3 133 10 12.8 128 4 60-140/20
m,p-Xylene ND 20 23.7 119 20 22.3 112 6 70-130/20
95-47-6 o-Xylene ND 10 11.8 118 10 11.2 112 5 70-130/20
1330-20-7 Xylene (total)ND 30 35.5 118 30 33.5 112 6 70-130/20
CAS No.Surrogate Recoveries MS MSD FA31078-6 Limits
1868-53-7 Dibromofluoromethane 102%102%101%70-130%
17060-07-0 1,2-Dichloroethane-D4 98%98%104%70-130%
2037-26-5 Toluene-D8 98%98%94%70-130%
460-00-4 4-Bromofluorobenzene 97%97%104%70-130%
* = Outside of Control Limits.
52 of 54
FA31078 55.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA31078
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA31105-1MS A0199169.D 200 02/03/16 TD n/a n/a VA1871
FA31105-1MSD A0199170.D 200 02/03/16 TD n/a n/a VA1871
FA31105-1 A0199166.D 200 02/03/16 TD n/a n/a VA1871
The QC reported here applies to the following samples:Method: SM 6200B
FA31078-10
FA31105-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 3920 2000 6160 112 2000 6070 108 1 70-130/20
108-86-1 Bromobenzene ND 2000 2110 106 2000 2140 107 1 70-130/20
74-97-5 Bromochloromethane ND 2000 2040 102 2000 1970 99 3 70-130/20
75-27-4 Bromodichloromethane ND 2000 2280 114 2000 2230 112 2 70-130/20
75-25-2 Bromoform ND 2000 2070 104 2000 2080 104 0 70-130/20
104-51-8 n-Butylbenzene 70.4 J 2000 2270 110 2000 2270 110 0 70-130/20
135-98-8 sec-Butylbenzene 45.3 J 2000 2310 113 2000 2310 113 0 70-130/20
98-06-6 tert-Butylbenzene ND 2000 2220 111 2000 2210 111 0 70-130/20
56-23-5 Carbon Tetrachloride ND 2000 2330 117 2000 2240 112 4 70-130/20
108-90-7 Chlorobenzene ND 2000 2120 106 2000 2080 104 2 70-130/20
75-00-3 Chloroethane ND 2000 2590 130 2000 2600 130 0 60-140/20
67-66-3 Chloroform 42.5 J 2000 2280 112 2000 2210 108 3 70-130/20
95-49-8 o-Chlorotoluene ND 2000 2300 115 2000 2300 115 0 70-130/20
106-43-4 p-Chlorotoluene ND 2000 2170 109 2000 2190 110 1 70-130/20
124-48-1 Dibromochloromethane ND 2000 2210 111 2000 2190 110 1 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 2000 2250 113 2000 2270 114 1 70-130/20
106-93-4 1,2-Dibromoethane ND 2000 2080 104 2000 2110 106 1 70-130/20
75-71-8 Dichlorodifluoromethane ND 2000 2630 132 2000 2460 123 7 60-140/20
95-50-1 1,2-Dichlorobenzene ND 2000 2180 109 2000 2140 107 2 70-130/20
541-73-1 1,3-Dichlorobenzene ND 2000 2180 109 2000 2170 109 0 70-130/20
106-46-7 1,4-Dichlorobenzene ND 2000 2100 105 2000 2070 104 1 70-130/20
75-34-3 1,1-Dichloroethane ND 2000 2270 114 2000 2220 111 2 70-130/20
107-06-2 1,2-Dichloroethane ND 2000 2090 105 2000 2050 103 2 70-130/20
75-35-4 1,1-Dichloroethylene ND 2000 2400 120 2000 2310 116 4 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 2000 2070 104 2000 2030 102 2 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 2000 2380 119 2000 2340 117 2 70-130/20
78-87-5 1,2-Dichloropropane ND 2000 2170 109 2000 2150 108 1 70-130/20
142-28-9 1,3-Dichloropropane ND 2000 2010 101 2000 2020 101 0 70-130/20
594-20-7 2,2-Dichloropropane ND 2000 2030 102 2000 1980 99 2 70-130/20
563-58-6 1,1-Dichloropropene ND 2000 2260 113 2000 2220 111 2 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 2000 2180 109 2000 2120 106 3 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 2000 2270 114 2000 2280 114 0 70-130/20
108-20-3 Di-Isopropyl Ether ND 2000 2090 105 2000 2040 102 2 70-130/20
100-41-4 Ethylbenzene 2420 2000 4530 106 2000 4510 105 0 70-130/20
87-68-3 Hexachlorobutadiene ND 2000 1960 98 2000 1970 99 1 70-130/20
98-82-8 Isopropylbenzene 183 2000 2440 113 2000 2420 112 1 70-130/20
* = Outside of Control Limits.
53 of 54
FA31078 55.3.3
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA31078
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA31105-1MS A0199169.D 200 02/03/16 TD n/a n/a VA1871
FA31105-1MSD A0199170.D 200 02/03/16 TD n/a n/a VA1871
FA31105-1 A0199166.D 200 02/03/16 TD n/a n/a VA1871
The QC reported here applies to the following samples:Method: SM 6200B
FA31078-10
FA31105-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene 29.2 J 2000 2240 111 2000 2230 110 0 70-130/20
74-83-9 Methyl Bromide ND 2000 2570 129 2000 2540 127 1 60-140/20
74-87-3 Methyl Chloride ND 2000 2700 135 2000 2500 125 8 60-140/20
74-95-3 Methylene Bromide ND 2000 2230 112 2000 2150 108 4 70-130/20
75-09-2 Methylene Chloride 472 2000 2450 99 2000 2390 96 2 70-130/20
1634-04-4 Methyl Tert Butyl Ether 563 2000 2660 105 2000 2640 104 1 70-130/20
91-20-3 Naphthalene 546 2000 2970 121 2000 3020 124 2 70-130/20
103-65-1 n-Propylbenzene 371 2000 2650 114 2000 2650 114 0 70-130/20
100-42-5 Styrene ND 2000 2250 113 2000 2220 111 1 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 2000 2170 109 2000 2180 109 0 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 2000 2060 103 2000 2110 106 2 70-130/20
127-18-4 Tetrachloroethylene ND 2000 2190 110 2000 2150 108 2 70-130/20
108-88-3 Toluene 22500 E 2000 23900 70 2000 24200 85 1 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 2000 2170 109 2000 2180 109 0 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 2000 2170 109 2000 2150 108 1 70-130/20
71-55-6 1,1,1-Trichloroethane ND 2000 2240 112 2000 2180 109 3 70-130/20
79-00-5 1,1,2-Trichloroethane ND 2000 2240 112 2000 2260 113 1 70-130/20
79-01-6 Trichloroethylene ND 2000 2240 112 2000 2190 110 2 70-130/20
75-69-4 Trichlorofluoromethane ND 2000 2710 136 2000 2570 129 5 60-140/20
96-18-4 1,2,3-Trichloropropane ND 2000 2100 105 2000 2150 108 2 70-130/20
95-63-6 1,2,4-Trimethylbenzene 3030 2000 5140 106 2000 5170 107 1 70-130/20
108-67-8 1,3,5-Trimethylbenzene 727 2000 2910 109 2000 2940 111 1 70-130/20
75-01-4 Vinyl Chloride ND 2000 2640 132 2000 2560 128 3 60-140/20
m,p-Xylene 10200 4000 14000 95 4000 13900 93 1 70-130/20
95-47-6 o-Xylene 4860 2000 6980 106 2000 6950 105 0 70-130/20
1330-20-7 Xylene (total)15000 6000 21000 100 6000 20900 98 0 70-130/20
CAS No.Surrogate Recoveries MS MSD FA31105-1 Limits
1868-53-7 Dibromofluoromethane 103%101%103%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%100%104%70-130%
2037-26-5 Toluene-D8 98%100%99%70-130%
460-00-4 4-Bromofluorobenzene 100%99%99%70-130%
* = Outside of Control Limits.
54 of 54
FA31078 55.3.3

APPENDIX B
Water Supply Well Abandonment Letters

3502 Hayes Road • Monroe, North Carolina 28110
Phone [phone] • [phone] • Fax [phone]
November 20, 2015

Mr. William G. Oliver
1109 East Main Street
Plymouth, North Carolina 27962

Re: Well Abandonment
Parcel No. 6777.06-38-1411
Red Apple Market #15
US Highway 64 West
Plymouth, Washington County
Incident #: 11890
GRI Project #: 2970

Dear Mr. Oliver,

Geological Resources, Inc. (GRI) is conducting ground water assessment and remediation activities on
behalf of Red Apple Markets, Inc. to mitigate the effects of a petroleum release from underground storage
tanks (USTs) at the former Red Apple Market #15 site, located at 1109 US Highway 64 East, Plymouth,
North Carolina. As part of the assessment, GRI proposes to abandon all of the existing water supply
wells within a 1,000-foot radius of the source area to lower the risk classification of the release.

It is GRI’s understanding that you are the owner of the property identified as Washington County Parcel
No. 6777.06-38-1411 and that a water supply well use for a garage sink is located on this property. GRI,
on behalf of Red Apple Markets, Inc. is requesting your permission to abandon your water supply well.
The water supply well will be abandoned in accordance with established guidelines at no cost to you.
Please indicate in the spaces provided below if you will allow your water supply well to be abandoned.
We would greatly appreciate a response, even if you choose not to abandon your well at this time.

Your cooperation in this matter will be greatly appreciated. If you have any questions, please feel free to
contact the North Carolina Department of Environmental Quality (NCDEQ) incident manager, Bill Crew
at [phone] or me at [phone].

Sincerely,

William Regenthal, P.G.
Project Manager
cc: file

Well Abandonment Agreement
Red Apple Market #15
Page 2 of 2

3502 Hayes Road • Monroe, North Carolina 28110
Phone [phone] • [phone] • Fax [phone]

Yes, I agree to allow my water supply well to be abandoned.

No, I will not allow my water supply well to be abandoned.

Signature Date
(For Parcel No. 6777.06-38-1411)

______________________
Phone Number

____________________
Well Depth (if known)

Oliver Garage Well

3502 Hayes Road • Monroe, North Carolina 28110
Phone [phone] • [phone] • Fax [phone]
December 15, 2015

Mr. William G. Oliver
1109 East Main Street
Plymouth, North Carolina 27962

Re: Well Abandonment
Parcel No. 6777.06-38-1411
Red Apple Market #15
US Highway 64 West
Plymouth, Washington County
Incident #: 11890
GRI Project #: 2970

Dear Mr. Oliver,

Geological Resources, Inc. (GRI) is conducting ground water assessment and remediation activities on
behalf of Red Apple Markets, Inc. to mitigate the effects of a petroleum release from underground storage
tanks (USTs) at the former Red Apple Market #15 site, located at 1109 US Highway 64 East, Plymouth,
North Carolina. As part of the assessment, GRI proposes to abandon all of the existing water supply
wells within a 1,000-foot radius of the source area to lower the risk classification of the release.

It is GRI’s understanding that you are the owner of the property identified as Washington County Parcel
No. 6777.06-38-1411 and that a water supply well use for a garage sink is located on this property. GRI,
on behalf of Red Apple Markets, Inc. is requesting your permission to abandon your water supply well.
The water supply well will be abandoned in accordance with established guidelines at no cost to you.
Please indicate in the spaces provided below if you will allow your water supply well to be abandoned.
We would greatly appreciate a response, even if you choose not to abandon your well at this time.

Your cooperation in this matter will be greatly appreciated. If you have any questions, please feel free to
contact the North Carolina Department of Environmental Quality (NCDEQ) incident manager, Bill Crew
at [phone] or me at [phone].

Sincerely,

William Regenthal, P.G.
Project Manager
cc: file

Well Abandonment Agreement
Red Apple Market #15
Page 2 of 2

3502 Hayes Road • Monroe, North Carolina 28110
Phone [phone] • [phone] • Fax [phone]

Yes, I agree to allow my water supply well to be abandoned.

No, I will not allow my water supply well to be abandoned.

Signature Date
(For Parcel No. 6777.06-38-1411)

______________________
Phone Number

____________________
Well Depth (if known)

Oliver Garage Well

3502 Hayes Road • Monroe, North Carolina 28110
Phone [phone] • [phone] • Fax [phone]
January 19, 2016

Mr. William G. Oliver
1109 East Main Street
Plymouth, North Carolina 27962

Re: Well Abandonment – Third Attempt
Parcel No. 6777.06-38-1411
Red Apple Market #15
US Highway 64 West
Plymouth, Washington County
Incident #: 11890
GRI Project #: 2970

Dear Mr. Oliver,

Geological Resources, Inc. (GRI) is conducting ground water assessment and remediation activities on
behalf of Red Apple Markets, Inc. to mitigate the effects of a petroleum release from underground storage
tanks (USTs) at the former Red Apple Market #15 site, located at 1109 US Highway 64 East, Plymouth,
North Carolina. As part of the assessment, GRI proposes to abandon all of the existing water supply
wells within a 1,000-foot radius of the source area to lower the risk classification of the release.

It is GRI’s understanding that you are the owner of the property identified as Washington County Parcel
No. 6777.06-38-1411 and that a water supply well use for a garage sink is located on this property. GRI,
on behalf of Red Apple Markets, Inc. is requesting your permission to abandon your water supply well.
The water supply well will be abandoned in accordance with established guidelines at no cost to you.
Please indicate in the spaces provided below if you will allow your water supply well to be abandoned.
We would greatly appreciate a response, even if you choose not to abandon your well at this time.

Your cooperation in this matter will be greatly appreciated. If you have any questions, please feel free to
contact the North Carolina Department of Environmental Quality (NCDEQ) incident manager, Bill Crew
at [phone] or me at [phone].

Sincerely,

William Regenthal, P.G.
Project Manager
cc: file

Well Abandonment Agreement
Red Apple Market #15
Page 2 of 2

3502 Hayes Road • Monroe, North Carolina 28110
Phone [phone] • [phone] • Fax [phone]

Yes, I agree to allow my water supply well to be abandoned.

No, I will not allow my water supply well to be abandoned.

Signature Date
(For Parcel No. 6777.06-38-1411)

______________________
Phone Number

____________________
Well Depth (if known)

Oliver Garage Well