WA-911_11890_CA_RPTS_20140711_MRP

ii

EXECUTIVE SUMMARY
The former Red Apple Market #15 site is located at 1109 US Highway 64 East in Plymouth, Washington
County, North Carolina. According to available information, two 550-gallon fuel oil, one 10,000-gallon
gasoline, three 4,000-gallon gasoline, one 10,000-gallon diesel, and one 2,000-gallon kerosene
underground storage tanks (USTs) were removed from the site in October 1993. Reportedly, a water
supply well, which its use has yet to be determined by NCDENR, is located approximately 750 feet
north/northwest of the site. Municipal water is available to all properties within the site vicinity. No
surface water bodies were identified within a 500-foot radius of the source area.

On June 20, 2014, twenty Type II monitoring wells (MW-1 through MW-5, MW-7 and MW-9 through
MW-22) and one Type III monitoring well (MW-8) were gauged, purged and sampled. Concentrations of
one or more individual BTEX constituents, naphthalene, isopropylbenzene, n-propylbenzene, 1,3,5-
trimethylbenzene and/or 1,2,4-trimethylbenzene that exceeded the maximum allowable concentrations
(MACs) specified in T15A NCAC 2L.0202 were reported in the ground water samples collected from
MW-1, MW-3, MW-4, MW-13 and MW-14.

GRI recommends that the use of the water supply well be determined by the NCDENR. Attempts should
be made to obtain an agreement from the well owner to abandon the water supply well. Regardless of the
use of the water supply well, results included in the March 14, 2014, Ground Water Monitoring and Fate
& Transport Model Report, the well is not considered to be at risk from this site. The site risk
classification should be lowered to Low Risk and the incident should be closed with the completion of
Notice of Residual Petroleum.

TABLE OF CONTENTS

FACILITY INFORMATION ................................................................................................................ i
EXECUTIVE SUMMARY.................................................................................................................... ii
1.0 SITE HISTORY AND CHARACTERIZATION .................................................................... 1
2.0 CURRENT SITE ASSESSMENT ............................................................................................ 1
3.0 GROUND WATER QUALITY ................................................................................................ 1
4.0 CONCLUSIONS AND RECOMMENDATIONS .................................................................... 2
5.0 LIMITATIONS ......................................................................................................................... 3

FIGURES
Figure 1: Site Location Map
Figure 2: Site Map
Figure 3: Water Table Surface Map
Figure 4: Ground Water Quality Map
Figure 5: Benzene Isoconcentration Map
Figure 6: Naphthalene Isoconcentration Map

TABLES

Table 1: Well Construction and Gauging Information
Table 2: Summary of Ground Water Sample Analytical Results

APPENDIX
Appendix A: Laboratory Report – Ground Water Samples

1
1.0 SITE HISTORY AND CHARACTERIZATION
According to the February 28, 2002, Quarterly Groundwater Monitoring Report submitted by NorthEast
Environmental, two 550-gallon fuel oil, one 10,000-gallon gasoline, three 4,000-gallon gasoline, one
10,000-gallon diesel, and one 2,000-gallon kerosene underground storage tanks (USTs) were removed
from the site in October 1993. A total of twenty-one Type II monitoring wells (MW-1 through MW-7
and MW-9 through MW-22) and one Type III monitoring well (MW-8) were installed at the site.
Monitoring well MW-6 was found destroyed during previous ground water assessment and corrective
action activities. A Corrective Action Plan, proposing natural attenuation, was approved for the site on
November 30, 1998. Previous activities were conducted by other consultants. Although Geological
Resources, Inc. (GRI) cannot verify the accuracy of information obtained from previous reports, for the
purposes of this report, it is assumed to be correct. Please refer to previous submittals for further
historical information regarding the site.

2.0 CURRENT SITE ASSESSMENT
The site is located at 1109 US Highway 64 East in Plymouth, Washington County, North Carolina
(Figure 1). This report presents the results of ground water assessment activities conducted on June 20,
2014, at the former Red Apple Market #15 site. The activities were conducted in accordance with GRI
Proposal No. 14-270, which was submitted to NCDENR on April 30, 2014 and approved as Task
Authorization No. 11890-020 on May 30, 2014. The purpose of the activities was to obtain current
ground water quality data for the site.

3.0 GROUND WATER QUALITY
On June 20, 2014, twenty Type II monitoring wells (MW-1 through MW-5, MW-7, MW-9 through MW-
22) and one Type III monitoring well (MW-8) were gauged, purged, and sampled. The depths to ground
water in the Type II monitoring wells during the June 2014 sampling event ranged from 7.70 to 10.93 feet
below the top of well casings. Ground water elevations in the Type II monitoring wells relative to a
temporary benchmark assumed by the previous consultant ranged from 89.10 to 89.59 feet. Based on
these data, the general ground water flow direction appears to be toward the west/northwest with an
apparent hydraulic mound in the vicinity of MW-4. The average horizontal hydraulic gradient across the
site was less than 0.01 feet per foot toward the west/northwest. The vertical hydraulic gradient between
paired wells MW-4 and MW-8 was approximately 0.02 feet per foot in the downward direction. A Site
Map showing the locations of the monitoring wells has been included as Figure 2. A Water Table

2
Surface Map based on the June 2014 sampling event is included as Figure 3. A summary of well
construction and gauging data is presented in Table 1.

Laboratory analyses were performed on the ground water samples collected from the monitoring wells
during the June 2014 sampling event for volatile organic compounds (VOCs) using EPA Method 6200B.
Concentrations of one or more individual BTEX constituents, naphthalene, isopropylbenzene, n-
propylbenzene, 1,3,5-trimethylbenzene and/or 1,2,4-trimethylbenzene that exceeded the maximum
allowable concentrations (MACs) specified in T15A NCAC 2L.0202 were reported in the ground water
samples collected from MW-1, MW-3, MW-4, MW-13 and MW-14. None of the reported contaminant
concentrations exceeded the gross contamination levels (GCLs). A summary of ground water sample
analytical results is presented in Table 2. A Ground Water Quality Map based on data collected during
the June 2014 sampling event is included as Figure 4. Inferred isoconcentration contours for benzene
and naphthalene are included as Figures 5 and 6, respectively. The laboratory report has been included
as Appendix A.

4.0 CONCLUSIONS AND RECOMMENDATIONS
 The average depth to ground water in the Type II monitoring wells in June 2014 was 9.80 feet.
The general ground water flow direction is toward the west/northwest with an average horizontal
hydraulic gradient of less than 0.01 feet per foot toward the west.
 Concentrations of one or more individual BTEX constituents, naphthalene, isopropylbenzene, n-
propylbenzene, 1,3,5-trimethylbenzene and/or 1,2,4-trimethylbenzene that exceeded the MACs
were reported in the ground water samples collected from MW-1, MW-3, MW-4, MW-13 and
MW-14. None of the reported contaminant concentrations exceeded the GCLs.
 The NCDENR incident manager identified a water supply well approximately 750 feet to the
north/northwest of the site. Based on the June 2014 ground water sampling data, it appears that
the water supply well is down gradient/cross gradient of the release. The usage of this well has
yet to be determined by the NCDENR. It is recommended that attempts should be made to
obtain an agreement from the well owner allowing the abandonment of the water supply well.
 Regardless of the use of the water supply well, results included in the March 14, 2014, Ground
Water Monitoring and Fate & Transport Model Report, the well is not considered to be at risk
from this site. The site risk classification should be lowered to Low Risk and the incident should
be closed with the completion of Notice of Residual Petroleum.

3
5.0 LIMITATIONS
This report has been prepared for the exclusive use of Red Apple Markets, Inc. for specific application to
the referenced site in Washington County, North Carolina. The assessment was conducted based on the
scope of work and level of effort desired by the NCDENR and with resources adequate only for that
scope of work. Our findings have been developed in accordance with generally accepted standards of
environmental practices in the State of North Carolina, available information, and our professional
judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would be
interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data. Please note that field data collected prior
to the June 2010 free product recovery event was not obtained under the supervision of GRI. Although
the accuracy of this information cannot be verified, for the purpose of this report GRI assumes that it is
correct.

FIGURES

TABLES
11/29/10 11.35 ---88.65
06/06/11 10.92 ---89.08
04/02/13 10.27 ---89.73
09/30/13 10.67 ---89.33
06/20/14 10.58 ---89.42
11/29/10 11.60 ---88.62
06/06/11 11.20 ---89.02
04/02/13 10.58 ---89.64
09/30/13 11.02 ---89.20
06/20/14 10.85 ---89.37
11/29/10 10.28 ---88.80
06/06/11 9.90 ---89.18
04/02/13 9.20 ---89.88
09/30/13 9.79 ---89.29
06/20/14 9.62 ---89.46
06/11/10 9.40 0.07 89.65
11/29/10 10.35 ---88.64
06/06/11 9.70 ---89.29
04/02/13 9.53 ---89.46
09/30/13 9.51 ---89.48
06/20/14 9.40 ---89.59
11/29/10 11.42 ---88.70
06/06/11 11.02 ---89.10
04/02/13 10.32 ---89.80
09/30/13 10.86 ---89.26
06/20/14 10.71 ---89.41
11/29/10 NM NM NM Damaged
06/06/11 NM NM NM Abandoned
11/29/10 9.43 ---88.73
06/06/11 9.07 ---89.09
04/02/13 8.46 ---89.70
09/30/13 8.98 ---89.18
06/20/14 8.85 ---89.31
11/29/10 10.10 ---88.70
06/06/11 9.90 ---88.90
04/02/13 9.14 ---89.66
09/30/13 9.69 ---89.11
06/20/14 9.65 ---89.15
11/29/10 10.32 ---88.73
06/06/11 9.92 ---89.13
04/02/13 8.23 ---90.82
09/30/13 9.80 ---89.25
06/20/14 9.60 ---89.45
Top of Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(feet)
Comments
99.02
MW-5
Ground
Water
Elevation (ft.)
100.222010 - 2010
Date: 07/08/14
Well
Installation
Date
Free
Product
Thickness
(ft.)
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET #15 (INCIDENT NO. 11890)
Facility ID # : 0-006313
Well ID
Date
Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft. BGS)
Bottom
of Well
(ft. BGS)
11/01/94MW-2
100.002010 - 201011/01/94MW-1
99.082010 - 201011/01/94MW-3
98.992010 - 201011/01/94MW-4
2010 - 201003/20/95MW-6
100.122010 - 201011/01/94
10 - 201003/20/95MW-7 20
MW-8 03/20/95 27 27 - 32 32 98.80
98.16
99.052010 - 201003/23/95MW-9
Page 1 of 3
Top of Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(feet)
Comments
Ground
Water
Elevation (ft.)
Date: 07/08/14
Well
Installation
Date
Free
Product
Thickness
(ft.)
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET #15 (INCIDENT NO. 11890)
Facility ID # : 0-006313
Well ID
Date
Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft. BGS)
Bottom
of Well
(ft. BGS)
11/29/10 10.77 ---88.65
06/06/11 10.32 ---89.10
04/02/13 9.68 ---89.74
09/30/13 10.18 ---89.24
06/20/14 9.88 ---89.54
11/29/10 10.77 ---88.65
06/06/11 10.33 ---89.09
04/02/13 9.67 ---89.75
09/30/13 10.21 ---89.21
06/20/14 9.98 ---89.44
11/29/10 10.58 ---88.63
06/06/11 10.20 ---89.01
04/02/13 9.51 ---89.70
09/30/13 10.07 ---89.14
06/20/14 9.91 ---89.30
11/29/10 11.50 ---88.62
06/06/11 11.10 ---89.02
04/02/13 10.42 ---89.70
09/30/13 10.91 ---89.21
06/20/14 10.76 ---89.36
11/29/10 11.37 ---88.61
06/06/11 10.95 ---89.03
04/02/13 10.30 ---89.68
09/30/13 10.81 ---89.17
06/20/14 10.63 ---89.35
11/29/10 9.40 ---88.53
06/06/11 8.93 ---89.00
04/02/13 8.41 ---89.52
09/30/13 8.80 ---89.13
06/20/14 8.56 ---89.37
11/29/10 9.79 ---88.57
06/06/11 9.30 ---89.06
04/02/13 8.70 ---89.66
09/30/13 9.19 ---89.17
06/20/14 8.93 ---89.43
11/29/10 8.50 ---88.52
06/06/11 8.03 ---88.99
04/02/13 7.44 ---89.58
09/30/13 7.91 ---89.11
06/20/14 7.70 ---89.32
11/29/10 11.65 ---88.59
06/06/11 11.25 ---88.99
04/02/13 10.61 ---89.63
09/30/13 11.10 ---89.14
06/20/14 10.93 ---89.31
MW-15
98.36
97.93188 - 18
MW-14 06/22/95 8 8 - 18
8 - 18806/22/95MW-13
10 - 201003/24/95MW-11
03/24/95MW-10 99.422010 - 2010
99.212010 - 201003/24/95MW-12
99.4220
18 99.98
100.1218
MW-17
MW-16 06/23/95 8 8 - 18 18
806/22/95
97.02155 - 15509/08/95
100.24188 - 18809/08/95MW-18
Page 2 of 3
Top of Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(feet)
Comments
Ground
Water
Elevation (ft.)
Date: 07/08/14
Well
Installation
Date
Free
Product
Thickness
(ft.)
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET #15 (INCIDENT NO. 11890)
Facility ID # : 0-006313
Well ID
Date
Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft. BGS)
Bottom
of Well
(ft. BGS)
11/29/10 11.28 ---88.61
06/06/11 10.89 ---89.00
04/02/13 10.24 ---89.65
09/30/13 10.77 ---89.12
06/20/14 10.59 ---89.30
11/29/10 10.60 ---88.56
06/06/11 10.22 ---88.94
04/02/13 9.57 ---89.59
09/30/13 10.05 ---89.11
06/20/14 9.92 ---89.24
11/29/10 10.17 ---88.25
06/06/11 9.73 ---88.69
04/02/13 9.17 ---89.25
09/30/13 9.54 ---88.88
06/20/14 9.32 ---89.10
06/06/11 9.74 ---88.92
04/02/13 9.14 ---89.52
09/30/13 9.51 ---89.15
06/20/14 9.34 ---89.32
Notes:
• ft BGS : feet below ground surface.
• NM: Not Measured.
• Top of Casing information and well construction details prior to June 2011 were obtained from the report titled 'Quartely Groundwater Sampling Event',
dated February 28, 2002 by Northeast Environmental, P.C. and well construction records.
98.66
99.16188 - 188
99.89188 - 18809/19/95MW-19
98.422010 - 201007/12/00MW-21
09/19/95MW-20
188 - 18806/06/11MW-22
Page 3 of 3
Date : 07/08/14
EPA
Method
504.1
EPA
Method
6010/303
0C
Well
ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 70 70 70 70 400 400 0.02 15 400 700 10,000 200
5,000 260,000 84,500 87,500 20,000 6,000 6,900 8,500 25,000 30,000 25,000 28,500 50 15,000 NE NE NE NE
11/29/10 <0.140 <0.190 0.378 J 0.820 J 6.15 20.1 <0.180 4.32 4.31 3.49 <0.180 0.491 J NR 26.1 <100 73.0 <80.0 505
06/06/11 <0.13 <0.13 <0.15 <0.30 5.8 2.2 0.28 J 1.7 0.38 J 0.22 J <0.10 <0.10 <0.0093 NR <100 89.6 J NR 101
04/02/13 <0.10 <0.10 <0.10 <0.22 3.7 1.9 0.43 J 3.1 0.63 0.31 J <0.10 0.11 J NR NR NR NR NR NR
09/30/13 <0.10 <0.10 0.19 J <0.22 2.5 9.8 0.99 4.4 3.1 2.9 <0.10 <0.10 NR NR NR NR NR NR
06/20/14 1.2 <0.10 <0.10 <0.20 2.9 6.6 1.6 4.9 3.7 4.4 <0.10 0.12 J NR NR NR NR NR NR
11/29/10 0.643 J <0.190 0.290 J 0.355 J 4.76 0.911 J <0.180 1.82 0.526 J <0.220 <0.180 <0.150 NR 10.6 113 59.9 <78.4 346
06/06/11 <0.13 <0.13 <0.15 <0.30 2.9 <0.10 <0.10 1.2 0.21 J <0.11 <0.10 <0.10 <0.0093 NR <100 94.8 J NR 104
04/02/13 0.74 <0.10 0.59 <0.22 2.7 <0.15 0.21 J 1.0 0.70 0.43 J <0.10 <0.10 NR NR NR NR NR NR
09/30/13 <0.10 <0.10 <0.10 <0.22 2.1 0.47 J <0.10 0.40 J <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
06/20/14 <0.10 <0.10 0.49 J <0.20 2.9 0.44 J <0.10 0.53 0.25 J 0.24 J <0.10 <0.10 NR NR NR NR NR NR
11/29/10 32.6 4.03 55.6 25.7 18.3 13.5 <0.360 1.41 J 7.29 12.5 5.28 5.37 NR 14.1 432 <160.0 <80.0 159
06/06/11 41.1 1.7 35.9 14.98 17.7 9.8 1.9 1.4 5.9 13.3 2.1 5.2 <0.0093 NR 503 243 NR 277
04/02/13 42.0 2.0 48.8 12.1 13.8 15.7 1.8 1.6 6.5 15.5 4.5 1.1 NR NR NR NR NR NR
09/30/13 47.7 4.1 60.9 20.0 11.7 16.7 1.8 1.4 6.3 17.2 3.5 2.5 NR NR NR NR NR NR
06/20/14 46.0 2.2 48.3 22.4 14.2 18.3 2.2 1.8 8.2 19.2 4.3 4.0 NR NR NR NR NR NR
EPA Method 6200B
IsopropylbenzeneContaminant of Concern
BenzeneTolueneMW-3 EthylbenzeneMW-1
TABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
RED APPLE MARKET #15 (INCIDENT NO. 11890)
MADEP Method EPH/VPH
LeadC5-C8 AliphaticsC9-C18 AliphaticsC19-C36 Aliphatics1,2,4-Trimethylbenzenesec-ButylbenzeneAnalytical Method 
Facility ID #: 0-006313
EDBn-ButylbenzeneNaphthalene1,3,5-TrimethylbenzeneC9-C22 Aromaticsn-PropylbenzeneGCL
2L Standard XylenesMTBEMW-2
Page 1 of 8
Date : 07/08/14
EPA
Method
504.1
EPA
Method
6010/303
0C
Well
ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 70 70 70 70 400 400 0.02 15 400 700 10,000 200
5,000 260,000 84,500 87,500 20,000 6,000 6,900 8,500 25,000 30,000 25,000 28,500 50 15,000 NE NE NE NE
EPA Method 6200B
IsopropylbenzeneContaminant of Concern
BenzeneTolueneEthylbenzeneTABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
RED APPLE MARKET #15 (INCIDENT NO. 11890)
MADEP Method EPH/VPH
LeadC5-C8 AliphaticsC9-C18 AliphaticsC19-C36 Aliphatics1,2,4-Trimethylbenzenesec-ButylbenzeneAnalytical Method 
Facility ID #: 0-006313
EDBn-ButylbenzeneNaphthalene1,3,5-TrimethylbenzeneC9-C22 Aromaticsn-PropylbenzeneGCL
2L Standard XylenesMTBE11/29/10 2,900 12,600 5,440 18,800 44.3 J 1,770 1,170 154 616 1,820 2,820 8,930 NR 5.82 27,300 16,500 <78.4 12,370
06/06/11 1,330 10,300 2,180 9,230 20.9 J 681 50.1 25.0 162 502 891 2,750 <0.0092 NR 26,900 20,500 NR 17,300
04/02/13 658 9,430 2,270 10,700 <25 853 37.8 J <25 136 473 837 3,150 NR NR NR NR NR NR
09/30/13 531 7,770 1,820 8,660 <25 492 <25 <25 85.9 J 285 582 2,390 NR NR NR NR NR NR
06/20/14 458 6,460 1,780 8,220 <2.5 511 23.1 15.2 121 379 628 2,340 NR NR NR NR NR NR
11/29/10 <0.140 <0.190 <0.150 <0.220 4.77 <0.500 <0.180 <0.140 <0.150 <0.220 <0.180 <0.150 NR 12.1 <100 <158.8 <78.4 <267
06/06/11 <0.13 <0.13 <0.15 <0.30 19.5 0.17 J <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 <0.0092 NR <100 <100 NR <100
04/02/13 <0.10 <0.10 <0.10 <0.22 24.2 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
09/30/13 <0.10 <0.10 <0.10 <0.22 14.0 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
06/20/14 <0.10 <0.10 <0.10 <0.20 13.2 0.41 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
11/29/10 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/06/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
04/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
MW-6
MW-5
MW-4
Page 2 of 8
Date : 07/08/14
EPA
Method
504.1
EPA
Method
6010/303
0C
Well
ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 70 70 70 70 400 400 0.02 15 400 700 10,000 200
5,000 260,000 84,500 87,500 20,000 6,000 6,900 8,500 25,000 30,000 25,000 28,500 50 15,000 NE NE NE NE
EPA Method 6200B
IsopropylbenzeneContaminant of Concern
BenzeneTolueneEthylbenzeneTABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
RED APPLE MARKET #15 (INCIDENT NO. 11890)
MADEP Method EPH/VPH
LeadC5-C8 AliphaticsC9-C18 AliphaticsC19-C36 Aliphatics1,2,4-Trimethylbenzenesec-ButylbenzeneAnalytical Method 
Facility ID #: 0-006313
EDBn-ButylbenzeneNaphthalene1,3,5-TrimethylbenzeneC9-C22 Aromaticsn-PropylbenzeneGCL
2L Standard XylenesMTBE11/29/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.150 <0.220 <0.180 <0.150 NR 27.8 <100 <157.7 <76.9 <263
06/06/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 <0.0094 NR <100 <100 NR <100
04/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
09/30/13 <0.10 <0.10 <0.10 <0.22 0.12 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
06/20/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
11/29/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.150 <0.220 <0.180 <0.150 NR 4.07 <100 <160.0 <80.0 <270
06/06/11 <0.13 <0.13 <0.15 <0.30 1.3 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 <0.0093 NR <100 <100 NR <100
04/02/13 <0.10 <0.10 <0.10 <0.22 1.5 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
09/30/13 <0.10 <0.10 <0.10 <0.22 1.2 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
06/20/14 0.12 J <0.10 <0.10 <0.20 2.3 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
11/29/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.150 <0.220 <0.180 <0.150 NR 14.6 <100 <160.0 <80.0 <270
06/06/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 <0.0095 NR <100 <100 NR <100
04/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
09/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
06/20/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
MW-8
MW-7
MW-9
Page 3 of 8
Date : 07/08/14
EPA
Method
504.1
EPA
Method
6010/303
0C
Well
ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 70 70 70 70 400 400 0.02 15 400 700 10,000 200
5,000 260,000 84,500 87,500 20,000 6,000 6,900 8,500 25,000 30,000 25,000 28,500 50 15,000 NE NE NE NE
EPA Method 6200B
IsopropylbenzeneContaminant of Concern
BenzeneTolueneEthylbenzeneTABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
RED APPLE MARKET #15 (INCIDENT NO. 11890)
MADEP Method EPH/VPH
LeadC5-C8 AliphaticsC9-C18 AliphaticsC19-C36 Aliphatics1,2,4-Trimethylbenzenesec-ButylbenzeneAnalytical Method 
Facility ID #: 0-006313
EDBn-ButylbenzeneNaphthalene1,3,5-TrimethylbenzeneC9-C22 Aromaticsn-PropylbenzeneGCL
2L Standard XylenesMTBE11/29/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.150 <0.220 <0.180 <0.150 NR 34.5 <100 <158.8 <78.4 <267
06/06/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 <0.0093 NR <100 <100 NR <100
04/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
09/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
06/20/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
11/29/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.150 <0.220 <0.180 <0.150 NR 8.02 <100 <158.8 <78.4 <267
06/06/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 <0.0094 NR <100 <100 NR <100
04/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
09/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
06/20/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
11/29/10 0.768 J <0.190 <0.150 0.364 J 4.25 <0.500 <0.180 <0.140 <0.150 <0.220 <0.180 <0.150 NR 43.6 <100 <158.8 <78.4 <267
06/06/11 0.99 <0.13 <0.15 <0.30 8.6 0.22 J <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 <0.019 NR <100 <100 NR <100
04/02/13 <0.10 <0.10 <0.10 <0.22 0.50 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
09/30/13 <0.10 <0.10 <0.10 <0.22 0.63 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
06/20/14 <0.10 <0.10 <0.10 <0.20 0.25 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
MW-12
MW-11
MW-10
Page 4 of 8
Date : 07/08/14
EPA
Method
504.1
EPA
Method
6010/303
0C
Well
ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 70 70 70 70 400 400 0.02 15 400 700 10,000 200
5,000 260,000 84,500 87,500 20,000 6,000 6,900 8,500 25,000 30,000 25,000 28,500 50 15,000 NE NE NE NE
EPA Method 6200B
IsopropylbenzeneContaminant of Concern
BenzeneTolueneEthylbenzeneTABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
RED APPLE MARKET #15 (INCIDENT NO. 11890)
MADEP Method EPH/VPH
LeadC5-C8 AliphaticsC9-C18 AliphaticsC19-C36 Aliphatics1,2,4-Trimethylbenzenesec-ButylbenzeneAnalytical Method 
Facility ID #: 0-006313
EDBn-ButylbenzeneNaphthalene1,3,5-TrimethylbenzeneC9-C22 Aromaticsn-PropylbenzeneGCL
2L Standard XylenesMTBE11/29/10 1,090 19.7 303 201 19.2 90.5 <1.80 4.16 J 30.9 53.3 9.40 J 9.03 J NR 12.0 1,860 505 <78.4 655
06/06/11 875 35.3 236 151.9 J 16.4 75.3 4.5 J 3.6 J 20.7 46.9 6.3 J 14.6 <0.0094 NR 2,080 1,080 NR 993
04/02/13 664 9.1 172 241 8.8 98.4 3.4 4.1 19.2 36.5 28.3 65.4 NR NR NR NR NR NR
09/30/13 334 1.9 93.2 115 6.7 78.6 2.7 3.2 12.3 22.8 8.2 36.9 NR NR NR NR NR NR
06/20/14 845 25.2 305 356 8.2 102 7.7 6.3 29.8 53.2 31.3 71.9 NR NR NR NR NR NR
11/29/10 398 4.91 J 114 67.6 8.73 40.6 <0.900 1.70 J 7.95 13.3 1.81 J 2.70 J NR 5.44 801 212 <76.9 446
06/06/11 238 3.2 64.2 34.0 12.4 29.6 1.2 1.4 5.9 11.8 1.1 1.5 <0.0092 NR 394 234 NR 235
04/02/13 96.1 2.4 54.3 20.1 7.7 23.8 1.7 2.2 6.0 13.0 1.3 2.5 NR NR NR NR NR NR
09/30/13 316 3.0 55.2 35.6 8.6 32.9 2.3 2.9 6.6 13.5 0.64 J 1.2 NR NR NR NR NR NR
06/20/14 85.9 1.3 28.7 8.1 5.4 11.2 0.97 1.3 3.0 6.4 0.13 J 0.34 J NR NR NR NR NR NR
11/29/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.150 <0.220 <0.180 <0.150 NR 5.49 <100 <157.7 <76.9 <263
06/06/11 <0.13 <0.13 <0.15 <0.30 0.64 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 <0.0094 NR <100 <100 NR <100
04/02/13 0.14 J <0.10 <0.10 <0.22 7.2 0.16 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
09/30/13 <0.10 <0.10 <0.10 <0.22 0.44 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
06/20/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
MW-13
MW-15
MW-14
Page 5 of 8
Date : 07/08/14
EPA
Method
504.1
EPA
Method
6010/303
0C
Well
ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 70 70 70 70 400 400 0.02 15 400 700 10,000 200
5,000 260,000 84,500 87,500 20,000 6,000 6,900 8,500 25,000 30,000 25,000 28,500 50 15,000 NE NE NE NE
EPA Method 6200B
IsopropylbenzeneContaminant of Concern
BenzeneTolueneEthylbenzeneTABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
RED APPLE MARKET #15 (INCIDENT NO. 11890)
MADEP Method EPH/VPH
LeadC5-C8 AliphaticsC9-C18 AliphaticsC19-C36 Aliphatics1,2,4-Trimethylbenzenesec-ButylbenzeneAnalytical Method 
Facility ID #: 0-006313
EDBn-ButylbenzeneNaphthalene1,3,5-TrimethylbenzeneC9-C22 Aromaticsn-PropylbenzeneGCL
2L Standard XylenesMTBE11/29/10 <0.140 0.326 J 0.391 J 2.00 <0.250 <0.500 <0.180 <0.140 <0.150 <0.220 0.438 J 1.54 NR 10.1 <100 <155.6 <74.1 <257
06/06/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 <0.0094 NR <100 <100 NR <100
04/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
09/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
06/20/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
11/29/10 <0.140 1.34 0.192 J 0.393 J <0.250 <0.500 <0.180 <0.140 <0.150 <0.220 <0.180 <0.150 NR 10.4 <100 <157.7 <76.9 <263
06/06/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 <0.0094 NR <100 <100 NR <100
04/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 0.12 J NR NR NR NR NR NR
09/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
06/20/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
11/29/10 <0.140 <0.190 <0.150 <0.220 13.2 <0.500 <0.180 <0.140 <0.150 <0.220 <0.180 <0.150 NR 23.3 <100 <158.8 <78.4 <267
06/06/11 <0.13 <0.13 <0.15 <0.20 11.7 0.14 J <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 <0.0093 NR <100 <100 NR <100
04/02/13 <0.10 <0.10 <0.10 <0.22 0.19 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
09/30/13 <0.10 <0.10 <0.10 <0.22 6.9 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
06/20/14 <0.10 <0.10 <0.10 <0.20 4.7 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
MW-18
MW-17
MW-16
Page 6 of 8
Date : 07/08/14
EPA
Method
504.1
EPA
Method
6010/303
0C
Well
ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 70 70 70 70 400 400 0.02 15 400 700 10,000 200
5,000 260,000 84,500 87,500 20,000 6,000 6,900 8,500 25,000 30,000 25,000 28,500 50 15,000 NE NE NE NE
EPA Method 6200B
IsopropylbenzeneContaminant of Concern
BenzeneTolueneEthylbenzeneTABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
RED APPLE MARKET #15 (INCIDENT NO. 11890)
MADEP Method EPH/VPH
LeadC5-C8 AliphaticsC9-C18 AliphaticsC19-C36 Aliphatics1,2,4-Trimethylbenzenesec-ButylbenzeneAnalytical Method 
Facility ID #: 0-006313
EDBn-ButylbenzeneNaphthalene1,3,5-TrimethylbenzeneC9-C22 Aromaticsn-PropylbenzeneGCL
2L Standard XylenesMTBE11/29/10 0.202 J <0.190 <0.150 <0.220 0.620 J <0.500 <0.180 <0.140 <0.150 <0.220 <0.180 <0.150 NR 15.8 <100 <66.2 <78.4 <267
06/06/11 <0.13 <0.13 <0.15 <0.30 0.35 J <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 <0.0092 NR <100 <100 NR <100
04/02/13 <0.10 <0.10 <0.10 <0.22 0.58 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
09/30/13 <0.10 <0.10 <0.10 <0.22 0.29 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
06/20/14 <0.10 <0.10 <0.10 <0.20 0.41 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
11/29/10 <0.140 <0.190 <0.150 <0.220 3.58 <0.500 <0.180 <0.140 <0.150 <0.220 <0.180 <0.150 NR 66.0 <100 <158.8 <78.4 <267
06/06/11 <0.13 <0.13 <0.15 <0.30 3.5 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 <0.0093 NR <100 <100 NR <100
04/02/13 <0.10 <0.10 <0.10 <0.22 1.1 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
09/30/13 <0.10 <0.10 <0.10 <0.22 0.57 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
06/20/14 <0.10 <0.10 <0.10 <0.20 0.56 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
11/29/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.150 <0.220 <0.180 <0.150 NR 25.2 <100 <158.8 <78.4 <267
06/06/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 <0.0092 NR <100 <100 NR <100
04/02/13 <0.10 <0.10 <0.10 <0.22 0.19 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
09/30/13 <0.10 <0.10 <0.10 <0.22 0.13 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
06/20/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
MW-20
MW-19
MW-21
Page 7 of 8
Date : 07/08/14
EPA
Method
504.1
EPA
Method
6010/303
0C
Well
ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 70 70 70 70 400 400 0.02 15 400 700 10,000 200
5,000 260,000 84,500 87,500 20,000 6,000 6,900 8,500 25,000 30,000 25,000 28,500 50 15,000 NE NE NE NE
EPA Method 6200B
IsopropylbenzeneContaminant of Concern
BenzeneTolueneEthylbenzeneTABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
RED APPLE MARKET #15 (INCIDENT NO. 11890)
MADEP Method EPH/VPH
LeadC5-C8 AliphaticsC9-C18 AliphaticsC19-C36 Aliphatics1,2,4-Trimethylbenzenesec-ButylbenzeneAnalytical Method 
Facility ID #: 0-006313
EDBn-ButylbenzeneNaphthalene1,3,5-TrimethylbenzeneC9-C22 Aromaticsn-PropylbenzeneGCL
2L Standard XylenesMTBE06/06/11 2.2 <0.13 <0.15 <0.30 34.5 0.26 J <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 <0.0094 NR <100 <100 NR <100
04/02/13 <0.10 <0.10 <0.10 <0.22 5.5 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
09/30/13 <0.10 <0.10 <0.10 <0.22 2.9 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
06/20/14 <0.10 <0.10 <0.10 <0.20 0.69 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
Notes:
• Results reported in µg/l (micrograms per liter).
• NE: Not established
• < : Less than the reporting limit specified in the laboratory report.
• Concentrations in bold face type exceeded the 2L standard.
• J: Estimated value.
• NS: Not Sampled; well abandoned.
• NR: Not Reported.
• For other compounds reported which did not exceed the 2L Standards, refer to the laboratory reports.
• GCL: Gross contamination level.
• 2L Standard: as specified in T15A NCAC 2L.0202.
MW-22
Page 8 of 8

APPENDIX

APPENDIX A
Laboratory Report – Ground Water Samples

07/03/14
Technical Report for
GRI (Geological Resources Inc.)
Ram 15, 1109 US 64 E, Plymouth, NC
11890
Accutest Job Number: FA16096
Sampling Date: 06/20/14
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
[e-mail]; [e-mail];
[e-mail]; [e-mail];
ATTN: William Regenthall
Total number of pages in report:
Certifications: FL (E83510), LA (03051), KS (E-10327), IA (366), IL (200063), NC (573), NJ (FL002), SC (96038001)
DoD ELAP (L-A-B L2229), CA (04226CA), TX (T104704404), PA (68-03573), VA (460177),
AK, AR, GA, KY, MA, NV, OK, UT, WA
This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone] • http://www.accutest.com
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Harry Behzadi, Ph.D.
Laboratory Director
Southeast
07/03/14
e-Hardcopy 2.0
Automated Report
89
Accutest Laboratories is the sole authority for authorizing edits or modifications to this
document. Unauthorized modification of this report is strictly prohibited.
1 of 89
FA16096
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................5
Section 3: Sample Results ........................................................................................................9
3.1: FA16096-1: MW-1 ........................................................................................................10
3.2: FA16096-2: MW-2 ........................................................................................................12
3.3: FA16096-3: MW-3 ........................................................................................................14
3.4: FA16096-4: MW-4 ........................................................................................................16
3.5: FA16096-5: MW-5 ........................................................................................................18
3.6: FA16096-6: MW-7 ........................................................................................................20
3.7: FA16096-7: MW-8 ........................................................................................................22
3.8: FA16096-8: MW-9 ........................................................................................................24
3.9: FA16096-9: MW-10 ......................................................................................................26
3.10: FA16096-10: MW-11 ..................................................................................................28
3.11: FA16096-11: MW-12 ..................................................................................................30
3.12: FA16096-12: MW-13 ..................................................................................................32
3.13: FA16096-13: MW-14 ..................................................................................................34
3.14: FA16096-14: MW-15 ..................................................................................................36
3.15: FA16096-15: MW-16 ..................................................................................................38
3.16: FA16096-16: MW-17 ..................................................................................................40
3.17: FA16096-17: MW-18 ..................................................................................................42
3.18: FA16096-18: MW-19 ..................................................................................................44
3.19: FA16096-19: MW-20 ..................................................................................................46
3.20: FA16096-20: MW-21 ..................................................................................................48
3.21: FA16096-21: MW-22 ..................................................................................................50
Section 4: Misc. Forms ............................................................................................................52
4.1: Chain of Custody ...........................................................................................................53
Section 5: GC/MS Volatiles - QC Data Summaries ..............................................................56
5.1: Method Blank Summary ................................................................................................57
5.2: Blank Spike Summary ...................................................................................................67
5.3: Matrix Spike Summary ..................................................................................................77
5.4: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................80
5.5: Duplicate Summary .......................................................................................................88 123452 of 89
FA16096
Accutest Laboratories
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA16096
Ram 15, 1109 US 64 E, Plymouth, NC
Project No: 11890
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA16096-1 06/20/14 11:11 JH 06/21/14 AQ Ground Water MW-1
FA16096-2 06/20/14 11:32 JH 06/21/14 AQ Ground Water MW-2
FA16096-3 06/20/14 11:23 JH 06/21/14 AQ Ground Water MW-3
FA16096-4 06/20/14 13:34 JH 06/21/14 AQ Ground Water MW-4
FA16096-5 06/20/14 10:25 JH 06/21/14 AQ Ground Water MW-5
FA16096-6 06/20/14 10:17 JH 06/21/14 AQ Ground Water MW-7
FA16096-7 06/20/14 13:18 JH 06/21/14 AQ Ground Water MW-8
FA16096-8 06/20/14 10:39 JH 06/21/14 AQ Ground Water MW-9
FA16096-9 06/20/14 10:50 JH 06/21/14 AQ Ground Water MW-10
FA16096-10 06/20/14 11:00 JH 06/21/14 AQ Ground Water MW-11
FA16096-11 06/20/14 12:52 JH 06/21/14 AQ Ground Water MW-12
FA16096-12 06/20/14 12:23 JH 06/21/14 AQ Ground Water MW-13
FA16096-13 06/20/14 11:44 JH 06/21/14 AQ Ground Water MW-14
3 of 89
FA16096 1
Accutest Laboratories
Sample Summary
(continued)
GRI (Geological Resources Inc.)
Job No:FA16096
Ram 15, 1109 US 64 E, Plymouth, NC
Project No: 11890
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA16096-14 06/20/14 09:45 JH 06/21/14 AQ Ground Water MW-15
FA16096-15 06/20/14 09:56 JH 06/21/14 AQ Ground Water MW-16
FA16096-16 06/20/14 10:07 JH 06/21/14 AQ Ground Water MW-17
FA16096-17 06/20/14 11:58 JH 06/21/14 AQ Ground Water MW-18
FA16096-18 06/20/14 12:09 JH 06/21/14 AQ Ground Water MW-19
FA16096-19 06/20/14 12:40 JH 06/21/14 AQ Ground Water MW-20
FA16096-20 06/20/14 09:21 JH 06/21/14 AQ Ground Water MW-21
FA16096-21 06/20/14 09:32 JH 06/21/14 AQ Ground Water MW-22
4 of 89
FA16096 1
Summary of Hits Page 1 of 4
Job Number:FA16096
Account:GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Collected:06/20/14
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA16096-1 MW-1
Benzene 1.2 0.50 0.10 ug/l SM 6200B
n-Butylbenzene 1.6 0.50 0.10 ug/l SM 6200B
sec-Butylbenzene 4.9 0.50 0.10 ug/l SM 6200B
tert-Butylbenzene 0.55 0.50 0.10 ug/l SM 6200B
Di-Isopropyl ether 1.5 0.50 0.10 ug/l SM 6200B
Isopropylbenzene 3.7 0.50 0.10 ug/l SM 6200B
Methyl chloride 0.12 J 0.50 0.10 ug/l SM 6200B
Methyl Tert Butyl Ether 2.9 0.50 0.10 ug/l SM 6200B
Naphthalene 6.6 0.50 0.10 ug/l SM 6200B
n-Propylbenzene 4.4 0.50 0.10 ug/l SM 6200B
1,2,4-Trimethylbenzene 0.12 J 0.50 0.10 ug/l SM 6200B
FA16096-2 MW-2
sec-Butylbenzene 0.53 0.50 0.10 ug/l SM 6200B
Di-Isopropyl ether 0.74 0.50 0.10 ug/l SM 6200B
Ethylbenzene 0.49 J 0.50 0.10 ug/l SM 6200B
Isopropylbenzene 0.25 J 0.50 0.10 ug/l SM 6200B
Methyl Tert Butyl Ether 2.9 0.50 0.10 ug/l SM 6200B
Naphthalene 0.44 J 0.50 0.10 ug/l SM 6200B
n-Propylbenzene 0.24 J 0.50 0.10 ug/l SM 6200B
FA16096-3 MW-3
Benzene 46.0 0.50 0.10 ug/l SM 6200B
n-Butylbenzene 2.2 0.50 0.10 ug/l SM 6200B
sec-Butylbenzene 1.8 0.50 0.10 ug/l SM 6200B
Di-Isopropyl ether 1.4 0.50 0.10 ug/l SM 6200B
Ethylbenzene 48.3 1.0 0.20 ug/l SM 6200B
Isopropylbenzene 8.2 0.50 0.10 ug/l SM 6200B
p-Isopropyltoluene 0.37 J 0.50 0.10 ug/l SM 6200B
Methyl Tert Butyl Ether 14.2 0.50 0.10 ug/l SM 6200B
Naphthalene 18.3 0.50 0.10 ug/l SM 6200B
n-Propylbenzene 19.2 0.50 0.10 ug/l SM 6200B
1,2,4-Trimethylbenzene 4.0 0.50 0.10 ug/l SM 6200B
1,3,5-Trimethylbenzene 4.3 0.50 0.10 ug/l SM 6200B
Toluene 2.2 0.50 0.10 ug/l SM 6200B
Xylene (total)22.4 1.5 0.20 ug/l SM 6200B
m,p-Xylene 20.5 1.0 0.10 ug/l SM 6200B
o-Xylene 1.9 0.50 0.10 ug/l SM 6200B
5 of 89
FA16096 2
Summary of Hits Page 2 of 4
Job Number:FA16096
Account:GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Collected:06/20/14
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA16096-4 MW-4
Benzene 458 13 2.5 ug/l SM 6200B
n-Butylbenzene 23.1 13 2.5 ug/l SM 6200B
sec-Butylbenzene 15.2 13 2.5 ug/l SM 6200B
Ethylbenzene 1780 100 20 ug/l SM 6200B
Isopropylbenzene 121 13 2.5 ug/l SM 6200B
p-Isopropyltoluene 8.6 J 13 2.5 ug/l SM 6200B
Naphthalene 511 13 2.5 ug/l SM 6200B
n-Propylbenzene 379 13 2.5 ug/l SM 6200B
Styrene 17.8 13 2.5 ug/l SM 6200B
1,2,4-Trimethylbenzene 2340 100 20 ug/l SM 6200B
1,3,5-Trimethylbenzene 628 13 2.5 ug/l SM 6200B
Toluene 6460 100 20 ug/l SM 6200B
Xylene (total)8220 300 40 ug/l SM 6200B
m,p-Xylene 5870 200 20 ug/l SM 6200B
o-Xylene 2350 100 20 ug/l SM 6200B
FA16096-5 MW-5
Methyl Tert Butyl Ether 13.2 0.50 0.10 ug/l SM 6200B
Naphthalene 0.41 J 0.50 0.10 ug/l SM 6200B
Tetrachloroethylene 0.72 0.50 0.10 ug/l SM 6200B
Trichloroethylene 0.28 J 0.50 0.10 ug/l SM 6200B
FA16096-6 MW-7
Tetrachloroethylene 0.55 0.50 0.10 ug/l SM 6200B
Trichloroethylene 0.17 J 0.50 0.10 ug/l SM 6200B
FA16096-7 MW-8
Benzene 0.12 J 0.50 0.10 ug/l SM 6200B
1,2-Dichloroethane 0.12 J 0.50 0.10 ug/l SM 6200B
Di-Isopropyl ether 0.32 J 0.50 0.10 ug/l SM 6200B
Methyl Tert Butyl Ether 2.3 0.50 0.10 ug/l SM 6200B
FA16096-8 MW-9
No hits reported in this sample.
FA16096-9 MW-10
No hits reported in this sample.
6 of 89
FA16096 2
Summary of Hits Page 3 of 4
Job Number:FA16096
Account:GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Collected:06/20/14
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA16096-10 MW-11
No hits reported in this sample.
FA16096-11 MW-12
Methyl Tert Butyl Ether 0.25 J 0.50 0.10 ug/l SM 6200B
FA16096-12 MW-13
Benzene 845 13 2.5 ug/l SM 6200B
n-Butylbenzene 7.7 0.50 0.10 ug/l SM 6200B
sec-Butylbenzene 6.3 0.50 0.10 ug/l SM 6200B
Di-Isopropyl ether 0.60 0.50 0.10 ug/l SM 6200B
Ethylbenzene 305 13 2.5 ug/l SM 6200B
Isopropylbenzene 29.8 0.50 0.10 ug/l SM 6200B
p-Isopropyltoluene 2.3 0.50 0.10 ug/l SM 6200B
Methyl Tert Butyl Ether 8.2 0.50 0.10 ug/l SM 6200B
Naphthalene 102 13 2.5 ug/l SM 6200B
n-Propylbenzene 53.2 13 2.5 ug/l SM 6200B
1,2,4-Trimethylbenzene 71.9 13 2.5 ug/l SM 6200B
1,3,5-Trimethylbenzene 31.3 0.50 0.10 ug/l SM 6200B
Toluene 25.2 0.50 0.10 ug/l SM 6200B
Xylene (total)356 38 5.0 ug/l SM 6200B
m,p-Xylene 356 25 2.5 ug/l SM 6200B
FA16096-13 MW-14
Benzene 85.9 1.0 0.20 ug/l SM 6200B
n-Butylbenzene 0.97 0.50 0.10 ug/l SM 6200B
sec-Butylbenzene 1.3 0.50 0.10 ug/l SM 6200B
Di-Isopropyl ether 1.8 0.50 0.10 ug/l SM 6200B
p-Dichlorobenzene 0.15 J 0.50 0.10 ug/l SM 6200B
Ethylbenzene 28.7 0.50 0.10 ug/l SM 6200B
Isopropylbenzene 3.0 0.50 0.10 ug/l SM 6200B
Methyl Tert Butyl Ether 5.4 0.50 0.10 ug/l SM 6200B
Naphthalene 11.2 0.50 0.10 ug/l SM 6200B
n-Propylbenzene 6.4 0.50 0.10 ug/l SM 6200B
1,2,4-Trimethylbenzene 0.34 J 0.50 0.10 ug/l SM 6200B
1,3,5-Trimethylbenzene 0.13 J 0.50 0.10 ug/l SM 6200B
Toluene 1.3 0.50 0.10 ug/l SM 6200B
Xylene (total)8.1 1.5 0.20 ug/l SM 6200B
m,p-Xylene 6.6 1.0 0.10 ug/l SM 6200B
o-Xylene 1.4 0.50 0.10 ug/l SM 6200B
7 of 89
FA16096 2
Summary of Hits Page 4 of 4
Job Number:FA16096
Account:GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Collected:06/20/14
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA16096-14 MW-15
Methyl chloride 0.11 J 0.50 0.10 ug/l SM 6200B
FA16096-15 MW-16
No hits reported in this sample.
FA16096-16 MW-17
Methyl chloride 0.16 J 0.50 0.10 ug/l SM 6200B
FA16096-17 MW-18
Chlorobenzene 20.4 0.50 0.10 ug/l SM 6200B
Di-Isopropyl ether 0.24 J 0.50 0.10 ug/l SM 6200B
p-Dichlorobenzene 8.5 0.50 0.10 ug/l SM 6200B
Methyl Tert Butyl Ether 4.7 0.50 0.10 ug/l SM 6200B
FA16096-18 MW-19
Chlorobenzene 2.6 0.50 0.10 ug/l SM 6200B
p-Dichlorobenzene 1.3 0.50 0.10 ug/l SM 6200B
Methyl Tert Butyl Ether 0.41 J 0.50 0.10 ug/l SM 6200B
FA16096-19 MW-20
Methyl Tert Butyl Ether 0.56 0.50 0.10 ug/l SM 6200B
FA16096-20 MW-21
Chlorobenzene 0.55 0.50 0.10 ug/l SM 6200B
Chloroform 6.5 0.50 0.10 ug/l SM 6200B
FA16096-21 MW-22
Chloroform 0.94 0.50 0.10 ug/l SM 6200B
Di-Isopropyl ether 0.17 J 0.50 0.10 ug/l SM 6200B
Methyl Tert Butyl Ether 0.69 0.50 0.10 ug/l SM 6200B
8 of 89
FA16096 2
Accutest Laboratories
Sample Results
Report of Analysis
Southeast
Section 3
9 of 89
FA16096 3
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-1
Lab Sample ID:FA16096-1 Date Sampled:06/20/14
Matrix:AQ - Ground Water Date Received:06/21/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0187854.D 1 06/30/14 TD n/a n/a VA1495
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 1.2 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene 1.6 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene 4.9 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene 0.55 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether 1.5 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 89
FA16096 33.1
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-1
Lab Sample ID:FA16096-1 Date Sampled:06/20/14
Matrix:AQ - Ground Water Date Received:06/21/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene 3.7 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride 0.12 0.50 0.10 ug/l J
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 2.9 0.50 0.10 ug/l
91-20-3 Naphthalene 6.6 0.50 0.10 ug/l
103-65-1 n-Propylbenzene 4.4 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene 0.12 0.50 0.10 ug/l J
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 109%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 89
FA16096 33.1
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-2
Lab Sample ID:FA16096-2 Date Sampled:06/20/14
Matrix:AQ - Ground Water Date Received:06/21/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0187855.D 1 07/01/14 TD n/a n/a VA1495
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene 0.53 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether 0.74 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 89
FA16096 33.2
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-2
Lab Sample ID:FA16096-2 Date Sampled:06/20/14
Matrix:AQ - Ground Water Date Received:06/21/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene 0.49 0.50 0.10 ug/l J
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene 0.25 0.50 0.10 ug/l J
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 2.9 0.50 0.10 ug/l
91-20-3 Naphthalene 0.44 0.50 0.10 ug/l J
103-65-1 n-Propylbenzene 0.24 0.50 0.10 ug/l J
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 104%70-130%
17060-07-0 1,2-Dichloroethane-D4 108%70-130%
2037-26-5 Toluene-D8 96%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
13 of 89
FA16096 33.2
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-3
Lab Sample ID:FA16096-3 Date Sampled:06/20/14
Matrix:AQ - Ground Water Date Received:06/21/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0187856.D 1 07/01/14 TD n/a n/a VA1495
Run #2 E031769.D 2 07/01/14 TD n/a n/a VE1062
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 46.0 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene 2.2 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene 1.8 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether 1.4 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
14 of 89
FA16096 33.3
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-3
Lab Sample ID:FA16096-3 Date Sampled:06/20/14
Matrix:AQ - Ground Water Date Received:06/21/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene 48.3 a 1.0 0.20 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene 8.2 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene 0.37 0.50 0.10 ug/l J
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 14.2 0.50 0.10 ug/l
91-20-3 Naphthalene 18.3 0.50 0.10 ug/l
103-65-1 n-Propylbenzene 19.2 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene 4.0 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene 4.3 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene 2.2 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)22.4 1.5 0.20 ug/l
m,p-Xylene 20.5 1.0 0.10 ug/l
95-47-6 o-Xylene 1.9 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%107%70-130%
17060-07-0 1,2-Dichloroethane-D4 107%113%70-130%
2037-26-5 Toluene-D8 98%95%70-130%
460-00-4 4-Bromofluorobenzene 102%101%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
15 of 89
FA16096 33.3
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-4
Lab Sample ID:FA16096-4 Date Sampled:06/20/14
Matrix:AQ - Ground Water Date Received:06/21/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0187857.D 25 07/01/14 TD n/a n/a VA1495
Run #2 A0187853.D 200 06/30/14 TD n/a n/a VA1495
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 458 13 2.5 ug/l
108-86-1 Bromobenzene ND 13 2.5 ug/l
74-97-5 Bromochloromethane ND 13 2.5 ug/l
75-27-4 Bromodichloromethane ND 13 2.5 ug/l
75-25-2 Bromoform ND 13 2.5 ug/l
104-51-8 n-Butylbenzene 23.1 13 2.5 ug/l
135-98-8 sec-Butylbenzene 15.2 13 2.5 ug/l
98-06-6 tert-Butylbenzene ND 13 2.5 ug/l
108-90-7 Chlorobenzene ND 13 2.5 ug/l
75-00-3 Chloroethane ND 13 3.1 ug/l
67-66-3 Chloroform ND 13 2.5 ug/l
95-49-8 o-Chlorotoluene ND 13 2.5 ug/l
106-43-4 p-Chlorotoluene ND 13 2.5 ug/l
56-23-5 Carbon tetrachloride ND 13 2.5 ug/l
75-34-3 1,1-Dichloroethane ND 13 2.5 ug/l
75-35-4 1,1-Dichloroethylene ND 13 2.5 ug/l
563-58-6 1,1-Dichloropropene ND 13 2.5 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 13 4.3 ug/l
106-93-4 1,2-Dibromoethane ND 13 2.5 ug/l
107-06-2 1,2-Dichloroethane ND 13 2.5 ug/l
78-87-5 1,2-Dichloropropane ND 13 2.5 ug/l
142-28-9 1,3-Dichloropropane ND 13 2.5 ug/l
108-20-3 Di-Isopropyl ether ND 13 2.5 ug/l
594-20-7 2,2-Dichloropropane ND 13 2.5 ug/l
124-48-1 Dibromochloromethane ND 13 2.5 ug/l
75-71-8 Dichlorodifluoromethane ND 13 2.5 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 13 2.5 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 13 2.5 ug/l
541-73-1 m-Dichlorobenzene ND 13 2.5 ug/l
95-50-1 o-Dichlorobenzene ND 13 2.5 ug/l
106-46-7 p-Dichlorobenzene ND 13 2.5 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 13 2.5 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
16 of 89
FA16096 33.4
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-4
Lab Sample ID:FA16096-4 Date Sampled:06/20/14
Matrix:AQ - Ground Water Date Received:06/21/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 13 2.5 ug/l
100-41-4 Ethylbenzene 1780 a 100 20 ug/l
87-68-3 Hexachlorobutadiene ND 13 2.5 ug/l
98-82-8 Isopropylbenzene 121 13 2.5 ug/l
99-87-6 p-Isopropyltoluene 8.6 13 2.5 ug/l J
74-83-9 Methyl bromide ND 13 2.5 ug/l
74-87-3 Methyl chloride ND 13 2.5 ug/l
74-95-3 Methylene bromide ND 13 2.5 ug/l
75-09-2 Methylene chloride ND 50 25 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 13 2.5 ug/l
91-20-3 Naphthalene 511 13 2.5 ug/l
103-65-1 n-Propylbenzene 379 13 2.5 ug/l
100-42-5 Styrene 17.8 13 2.5 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 13 2.5 ug/l
71-55-6 1,1,1-Trichloroethane ND 13 2.5 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 13 2.5 ug/l
79-00-5 1,1,2-Trichloroethane ND 13 2.6 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 13 2.5 ug/l
96-18-4 1,2,3-Trichloropropane ND 13 3.0 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 13 2.5 ug/l
95-63-6 1,2,4-Trimethylbenzene 2340 a 100 20 ug/l
108-67-8 1,3,5-Trimethylbenzene 628 13 2.5 ug/l
127-18-4 Tetrachloroethylene ND 13 2.5 ug/l
108-88-3 Toluene 6460 a 100 20 ug/l
79-01-6 Trichloroethylene ND 13 2.5 ug/l
75-69-4 Trichlorofluoromethane ND 13 2.5 ug/l
75-01-4 Vinyl chloride ND 13 2.5 ug/l
1330-20-7 Xylene (total)8220 a 300 40 ug/l
m,p-Xylene 5870 a 200 20 ug/l
95-47-6 o-Xylene 2350 a 100 20 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 98%100%70-130%
17060-07-0 1,2-Dichloroethane-D4 108%103%70-130%
2037-26-5 Toluene-D8 102%100%70-130%
460-00-4 4-Bromofluorobenzene 98%100%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
17 of 89
FA16096 33.4
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-5
Lab Sample ID:FA16096-5 Date Sampled:06/20/14
Matrix:AQ - Ground Water Date Received:06/21/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0187858.D 1 07/01/14 TD n/a n/a VA1495
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
18 of 89
FA16096 33.5
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-5
Lab Sample ID:FA16096-5 Date Sampled:06/20/14
Matrix:AQ - Ground Water Date Received:06/21/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 13.2 0.50 0.10 ug/l
91-20-3 Naphthalene 0.41 0.50 0.10 ug/l J
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene 0.72 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene 0.28 0.50 0.10 ug/l J
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
19 of 89
FA16096 33.5
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-7
Lab Sample ID:FA16096-6 Date Sampled:06/20/14
Matrix:AQ - Ground Water Date Received:06/21/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E031764.D 1 07/01/14 TD n/a n/a VE1062
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
20 of 89
FA16096 33.6
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-7
Lab Sample ID:FA16096-6 Date Sampled:06/20/14
Matrix:AQ - Ground Water Date Received:06/21/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene 0.55 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene 0.17 0.50 0.10 ug/l J
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
21 of 89
FA16096 33.6
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-8
Lab Sample ID:FA16096-7 Date Sampled:06/20/14
Matrix:AQ - Ground Water Date Received:06/21/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E031765.D 1 07/01/14 TD n/a n/a VE1062
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 0.12 0.50 0.10 ug/l J
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane 0.12 0.50 0.10 ug/l J
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether 0.32 0.50 0.10 ug/l J
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
22 of 89
FA16096 33.7
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-8
Lab Sample ID:FA16096-7 Date Sampled:06/20/14
Matrix:AQ - Ground Water Date Received:06/21/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 2.3 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
2037-26-5 Toluene-D8 89%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
23 of 89
FA16096 33.7
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-9
Lab Sample ID:FA16096-8 Date Sampled:06/20/14
Matrix:AQ - Ground Water Date Received:06/21/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E031766.D 1 07/01/14 TD n/a n/a VE1062
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
24 of 89
FA16096 33.8
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-9
Lab Sample ID:FA16096-8 Date Sampled:06/20/14
Matrix:AQ - Ground Water Date Received:06/21/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 105%70-130%
17060-07-0 1,2-Dichloroethane-D4 109%70-130%
2037-26-5 Toluene-D8 96%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
25 of 89
FA16096 33.8
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-10
Lab Sample ID:FA16096-9 Date Sampled:06/20/14
Matrix:AQ - Ground Water Date Received:06/21/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E031812.D 1 07/02/14 TD n/a n/a VE1063
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
26 of 89
FA16096 33.9
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-10
Lab Sample ID:FA16096-9 Date Sampled:06/20/14
Matrix:AQ - Ground Water Date Received:06/21/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 99%70-130%
2037-26-5 Toluene-D8 96%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
27 of 89
FA16096 33.9
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-11
Lab Sample ID:FA16096-10 Date Sampled:06/20/14
Matrix:AQ - Ground Water Date Received:06/21/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E031771.D 1 07/01/14 TD n/a n/a VE1062
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
28 of 89
FA16096 33.10
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-11
Lab Sample ID:FA16096-10 Date Sampled:06/20/14
Matrix:AQ - Ground Water Date Received:06/21/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 106%70-130%
17060-07-0 1,2-Dichloroethane-D4 108%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
29 of 89
FA16096 33.10
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-12
Lab Sample ID:FA16096-11 Date Sampled:06/20/14
Matrix:AQ - Ground Water Date Received:06/21/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0187876.D 1 07/01/14 TD n/a n/a VA1496
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
30 of 89
FA16096 33.11
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-12
Lab Sample ID:FA16096-11 Date Sampled:06/20/14
Matrix:AQ - Ground Water Date Received:06/21/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.25 0.50 0.10 ug/l J
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 109%70-130%
17060-07-0 1,2-Dichloroethane-D4 120%70-130%
2037-26-5 Toluene-D8 89%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
31 of 89
FA16096 33.11
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-13
Lab Sample ID:FA16096-12 Date Sampled:06/20/14
Matrix:AQ - Ground Water Date Received:06/21/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E031754.D 1 06/30/14 TD n/a n/a VE1061
Run #2 E031770.D 25 07/01/14 TD n/a n/a VE1062
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 845 a 13 2.5 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene 7.7 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene 6.3 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether 0.60 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
32 of 89
FA16096 33.12
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-13
Lab Sample ID:FA16096-12 Date Sampled:06/20/14
Matrix:AQ - Ground Water Date Received:06/21/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene 305 a 13 2.5 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene 29.8 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene 2.3 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 8.2 0.50 0.10 ug/l
91-20-3 Naphthalene 102 a 13 2.5 ug/l
103-65-1 n-Propylbenzene 53.2 a 13 2.5 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene 71.9 a 13 2.5 ug/l
108-67-8 1,3,5-Trimethylbenzene 31.3 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene 25.2 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)356 a 38 5.0 ug/l
m,p-Xylene 356 a 25 2.5 ug/l
95-47-6 o-Xylene ND a 13 2.5 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 95%103%70-130%
17060-07-0 1,2-Dichloroethane-D4 98%113%70-130%
2037-26-5 Toluene-D8 96%98%70-130%
460-00-4 4-Bromofluorobenzene 97%101%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
33 of 89
FA16096 33.12
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-14
Lab Sample ID:FA16096-13 Date Sampled:06/20/14
Matrix:AQ - Ground Water Date Received:06/21/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E031753.D 1 06/30/14 TD n/a n/a VE1061
Run #2 A0187867.D 2 07/01/14 TD n/a n/a VA1496
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 85.9 a 1.0 0.20 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene 0.97 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene 1.3 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether 1.8 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene 0.15 0.50 0.10 ug/l J
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
34 of 89
FA16096 33.13
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-14
Lab Sample ID:FA16096-13 Date Sampled:06/20/14
Matrix:AQ - Ground Water Date Received:06/21/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene 28.7 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene 3.0 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 5.4 0.50 0.10 ug/l
91-20-3 Naphthalene 11.2 0.50 0.10 ug/l
103-65-1 n-Propylbenzene 6.4 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene 0.34 0.50 0.10 ug/l J
108-67-8 1,3,5-Trimethylbenzene 0.13 0.50 0.10 ug/l J
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene 1.3 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)8.1 1.5 0.20 ug/l
m,p-Xylene 6.6 1.0 0.10 ug/l
95-47-6 o-Xylene 1.4 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%101%70-130%
17060-07-0 1,2-Dichloroethane-D4 107%110%70-130%
2037-26-5 Toluene-D8 97%99%70-130%
460-00-4 4-Bromofluorobenzene 99%100%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
35 of 89
FA16096 33.13
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-15
Lab Sample ID:FA16096-14 Date Sampled:06/20/14
Matrix:AQ - Ground Water Date Received:06/21/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0187868.D 1 07/01/14 TD n/a n/a VA1496
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
36 of 89
FA16096 33.14
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-15
Lab Sample ID:FA16096-14 Date Sampled:06/20/14
Matrix:AQ - Ground Water Date Received:06/21/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride 0.11 0.50 0.10 ug/l J
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 107%70-130%
2037-26-5 Toluene-D8 90%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
37 of 89
FA16096 33.14
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-16
Lab Sample ID:FA16096-15 Date Sampled:06/20/14
Matrix:AQ - Ground Water Date Received:06/21/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0187869.D 1 07/01/14 TD n/a n/a VA1496
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
38 of 89
FA16096 33.15
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-16
Lab Sample ID:FA16096-15 Date Sampled:06/20/14
Matrix:AQ - Ground Water Date Received:06/21/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 109%70-130%
2037-26-5 Toluene-D8 94%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
39 of 89
FA16096 33.15
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-17
Lab Sample ID:FA16096-16 Date Sampled:06/20/14
Matrix:AQ - Ground Water Date Received:06/21/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0187870.D 1 07/01/14 TD n/a n/a VA1496
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
40 of 89
FA16096 33.16
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-17
Lab Sample ID:FA16096-16 Date Sampled:06/20/14
Matrix:AQ - Ground Water Date Received:06/21/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride 0.16 0.50 0.10 ug/l J
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 111%70-130%
2037-26-5 Toluene-D8 87%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
41 of 89
FA16096 33.16
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-18
Lab Sample ID:FA16096-17 Date Sampled:06/20/14
Matrix:AQ - Ground Water Date Received:06/21/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0187871.D 1 07/01/14 TD n/a n/a VA1496
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene 20.4 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether 0.24 0.50 0.10 ug/l J
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene 8.5 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
42 of 89
FA16096 33.17
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-18
Lab Sample ID:FA16096-17 Date Sampled:06/20/14
Matrix:AQ - Ground Water Date Received:06/21/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 4.7 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 104%70-130%
17060-07-0 1,2-Dichloroethane-D4 112%70-130%
2037-26-5 Toluene-D8 96%70-130%
460-00-4 4-Bromofluorobenzene 103%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
43 of 89
FA16096 33.17
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-19
Lab Sample ID:FA16096-18 Date Sampled:06/20/14
Matrix:AQ - Ground Water Date Received:06/21/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0187872.D 1 07/01/14 TD n/a n/a VA1496
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene 2.6 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene 1.3 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
44 of 89
FA16096 33.18
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-19
Lab Sample ID:FA16096-18 Date Sampled:06/20/14
Matrix:AQ - Ground Water Date Received:06/21/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.41 0.50 0.10 ug/l J
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 104%70-130%
17060-07-0 1,2-Dichloroethane-D4 113%70-130%
2037-26-5 Toluene-D8 95%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
45 of 89
FA16096 33.18
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-20
Lab Sample ID:FA16096-19 Date Sampled:06/20/14
Matrix:AQ - Ground Water Date Received:06/21/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0187873.D 1 07/01/14 TD n/a n/a VA1496
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
46 of 89
FA16096 33.19
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-20
Lab Sample ID:FA16096-19 Date Sampled:06/20/14
Matrix:AQ - Ground Water Date Received:06/21/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.56 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 108%70-130%
17060-07-0 1,2-Dichloroethane-D4 118%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
47 of 89
FA16096 33.19
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-21
Lab Sample ID:FA16096-20 Date Sampled:06/20/14
Matrix:AQ - Ground Water Date Received:06/21/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0187874.D 1 07/01/14 TD n/a n/a VA1496
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene 0.55 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform 6.5 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
48 of 89
FA16096 33.20
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-21
Lab Sample ID:FA16096-20 Date Sampled:06/20/14
Matrix:AQ - Ground Water Date Received:06/21/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 109%70-130%
17060-07-0 1,2-Dichloroethane-D4 118%70-130%
2037-26-5 Toluene-D8 89%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
49 of 89
FA16096 33.20
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-22
Lab Sample ID:FA16096-21 Date Sampled:06/20/14
Matrix:AQ - Ground Water Date Received:06/21/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0187875.D 1 07/01/14 TD n/a n/a VA1496
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform 0.94 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether 0.17 0.50 0.10 ug/l J
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
50 of 89
FA16096 33.21
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-22
Lab Sample ID:FA16096-21 Date Sampled:06/20/14
Matrix:AQ - Ground Water Date Received:06/21/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 15, 1109 US 64 E, Plymouth, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.69 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 108%70-130%
17060-07-0 1,2-Dichloroethane-D4 120%70-130%
2037-26-5 Toluene-D8 86%70-130%
460-00-4 4-Bromofluorobenzene 104%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
51 of 89
FA16096 33.21
Accutest Laboratories
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Southeast
Section 4
52 of 89
FA16096 4
FA16096: Chain of Custody
Page 1 of 3
53 of 89
FA16096 44.1
FA16096: Chain of Custody
Page 2 of 3
54 of 89
FA16096 44.1
FA16096: Chain of Custody
Page 3 of 3
55 of 89
FA16096 44.1
Accutest Laboratories
GC/MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Southeast
Section 5
56 of 89
FA16096 5
Method Blank Summary Page 1 of 2
Job Number:FA16096
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1061-MB E031729.D 1 06/30/14 TD n/a n/a VE1061
The QC reported here applies to the following samples:Method: SM 6200B
FA16096-12, FA16096-13
CAS No.Compound Result RL MDL Units Q
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
57 of 89
FA16096 55.1.1
Method Blank Summary Page 2 of 2
Job Number:FA16096
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1061-MB E031729.D 1 06/30/14 TD n/a n/a VE1061
The QC reported here applies to the following samples:Method: SM 6200B
FA16096-12, FA16096-13
CAS No.Compound Result RL MDL Units Q
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 99%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
58 of 89
FA16096 55.1.1
Method Blank Summary Page 1 of 2
Job Number:FA16096
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1495-MB A0187840.D 1 06/30/14 TD n/a n/a VA1495
The QC reported here applies to the following samples:Method: SM 6200B
FA16096-1, FA16096-2, FA16096-3, FA16096-4, FA16096-5
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
59 of 89
FA16096 55.1.2
Method Blank Summary Page 2 of 2
Job Number:FA16096
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1495-MB A0187840.D 1 06/30/14 TD n/a n/a VA1495
The QC reported here applies to the following samples:Method: SM 6200B
FA16096-1, FA16096-2, FA16096-3, FA16096-4, FA16096-5
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
60 of 89
FA16096 55.1.2
Method Blank Summary Page 1 of 2
Job Number:FA16096
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1496-MB A0187866.D 1 07/01/14 TD n/a n/a VA1496
The QC reported here applies to the following samples:Method: SM 6200B
FA16096-11, FA16096-13, FA16096-14, FA16096-15, FA16096-16, FA16096-17, FA16096-18, FA16096-19, FA16096-
20, FA16096-21
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
61 of 89
FA16096 55.1.3
Method Blank Summary Page 2 of 2
Job Number:FA16096
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1496-MB A0187866.D 1 07/01/14 TD n/a n/a VA1496
The QC reported here applies to the following samples:Method: SM 6200B
FA16096-11, FA16096-13, FA16096-14, FA16096-15, FA16096-16, FA16096-17, FA16096-18, FA16096-19, FA16096-
20, FA16096-21
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
62 of 89
FA16096 55.1.3
Method Blank Summary Page 1 of 2
Job Number:FA16096
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1062-MB E031763.D 1 07/01/14 TD n/a n/a VE1062
The QC reported here applies to the following samples:Method: SM 6200B
FA16096-3, FA16096-6, FA16096-7, FA16096-8, FA16096-10, FA16096-12
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
63 of 89
FA16096 55.1.4
Method Blank Summary Page 2 of 2
Job Number:FA16096
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1062-MB E031763.D 1 07/01/14 TD n/a n/a VE1062
The QC reported here applies to the following samples:Method: SM 6200B
FA16096-3, FA16096-6, FA16096-7, FA16096-8, FA16096-10, FA16096-12
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 98%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
64 of 89
FA16096 55.1.4
Method Blank Summary Page 1 of 2
Job Number:FA16096
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1063-MB E031798.D 1 07/02/14 TD n/a n/a VE1063
The QC reported here applies to the following samples:Method: SM 6200B
FA16096-9
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
65 of 89
FA16096 55.1.5
Method Blank Summary Page 2 of 2
Job Number:FA16096
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1063-MB E031798.D 1 07/02/14 TD n/a n/a VE1063
The QC reported here applies to the following samples:Method: SM 6200B
FA16096-9
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 96%70-130%
17060-07-0 1,2-Dichloroethane-D4 94%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
66 of 89
FA16096 55.1.5
Blank Spike Summary Page 1 of 2
Job Number:FA16096
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1061-BS E031727.D 1 06/30/14 TD n/a n/a VE1061
The QC reported here applies to the following samples:Method: SM 6200B
FA16096-12, FA16096-13
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
108-86-1 Bromobenzene 10 9.2 92 70-130
74-97-5 Bromochloromethane 10 9.3 93 70-130
75-27-4 Bromodichloromethane 10 7.7 77 70-130
75-25-2 Bromoform 10 7.5 75 70-130
104-51-8 n-Butylbenzene 10 7.8 78 70-130
135-98-8 sec-Butylbenzene 10 8.8 88 70-130
98-06-6 tert-Butylbenzene 10 8.4 84 70-130
108-90-7 Chlorobenzene 10 10.1 101 70-130
75-00-3 Chloroethane 10 10.2 102 60-140
67-66-3 Chloroform 10 8.8 88 70-130
95-49-8 o-Chlorotoluene 10 9.7 97 70-130
106-43-4 p-Chlorotoluene 10 10 100 70-130
56-23-5 Carbon tetrachloride 10 8.1 81 70-130
75-34-3 1,1-Dichloroethane 10 9.4 94 70-130
75-35-4 1,1-Dichloroethylene 10 8.6 86 70-130
563-58-6 1,1-Dichloropropene 10 8.9 89 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 7.7 77 70-130
106-93-4 1,2-Dibromoethane 10 9.4 94 70-130
107-06-2 1,2-Dichloroethane 10 8.9 89 70-130
78-87-5 1,2-Dichloropropane 10 9.8 98 70-130
142-28-9 1,3-Dichloropropane 10 9.4 94 70-130
108-20-3 Di-Isopropyl ether 10 9.7 97 70-130
594-20-7 2,2-Dichloropropane 10 9.3 93 70-130
124-48-1 Dibromochloromethane 10 7.8 78 70-130
75-71-8 Dichlorodifluoromethane 10 8.8 88 60-140
156-59-2 cis-1,2-Dichloroethylene 10 9.4 94 70-130
10061-01-5 cis-1,3-Dichloropropene 10 7.6 76 70-130
541-73-1 m-Dichlorobenzene 10 8.9 89 70-130
95-50-1 o-Dichlorobenzene 10 9.7 97 70-130
106-46-7 p-Dichlorobenzene 10 9.1 91 70-130
156-60-5 trans-1,2-Dichloroethylene 10 9.2 92 70-130
10061-02-6 trans-1,3-Dichloropropene 10 8.7 87 70-130
100-41-4 Ethylbenzene 10 9.2 92 70-130
87-68-3 Hexachlorobutadiene 10 9.0 90 70-130
98-82-8 Isopropylbenzene 10 8.8 88 70-130
99-87-6 p-Isopropyltoluene 10 8.5 85 70-130
* = Outside of Control Limits.
67 of 89
FA16096 55.2.1
Blank Spike Summary Page 2 of 2
Job Number:FA16096
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1061-BS E031727.D 1 06/30/14 TD n/a n/a VE1061
The QC reported here applies to the following samples:Method: SM 6200B
FA16096-12, FA16096-13
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
74-83-9 Methyl bromide 10 10.6 106 60-140
74-87-3 Methyl chloride 10 11.4 114 60-140
74-95-3 Methylene bromide 10 8.9 89 70-130
75-09-2 Methylene chloride 10 8.7 87 70-130
1634-04-4 Methyl Tert Butyl Ether 10 8.8 88 70-130
91-20-3 Naphthalene 10 8.7 87 70-130
103-65-1 n-Propylbenzene 10 8.9 89 70-130
100-42-5 Styrene 10 7.8 78 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 9.4 94 70-130
71-55-6 1,1,1-Trichloroethane 10 9.0 90 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 9.1 91 70-130
79-00-5 1,1,2-Trichloroethane 10 9.2 92 70-130
87-61-6 1,2,3-Trichlorobenzene 10 8.6 86 70-130
96-18-4 1,2,3-Trichloropropane 10 9.1 91 70-130
120-82-1 1,2,4-Trichlorobenzene 10 7.7 77 70-130
95-63-6 1,2,4-Trimethylbenzene 10 7.9 79 70-130
108-67-8 1,3,5-Trimethylbenzene 10 7.7 77 70-130
127-18-4 Tetrachloroethylene 10 9.5 95 70-130
108-88-3 Toluene 10 9.3 93 70-130
79-01-6 Trichloroethylene 10 9.2 92 70-130
75-69-4 Trichlorofluoromethane 10 10.4 104 60-140
75-01-4 Vinyl chloride 10 11.6 116 60-140
1330-20-7 Xylene (total)30 25.4 85 70-130
m,p-Xylene 20 16.8 84 70-130
95-47-6 o-Xylene 10 8.6 86 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 97%70-130%
17060-07-0 1,2-Dichloroethane-D4 96%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 96%70-130%
* = Outside of Control Limits.
68 of 89
FA16096 55.2.1
Blank Spike Summary Page 1 of 2
Job Number:FA16096
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1495-BS A0187838.D 1 06/30/14 TD n/a n/a VA1495
The QC reported here applies to the following samples:Method: SM 6200B
FA16096-1, FA16096-2, FA16096-3, FA16096-4, FA16096-5
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 11.0 110 70-130
108-86-1 Bromobenzene 10 11.3 113 70-130
74-97-5 Bromochloromethane 10 10.9 109 70-130
75-27-4 Bromodichloromethane 10 10.9 109 70-130
75-25-2 Bromoform 10 11.2 112 70-130
104-51-8 n-Butylbenzene 10 11.2 112 70-130
135-98-8 sec-Butylbenzene 10 11.1 111 70-130
98-06-6 tert-Butylbenzene 10 11.1 111 70-130
108-90-7 Chlorobenzene 10 11.1 111 70-130
75-00-3 Chloroethane 10 9.5 95 60-140
67-66-3 Chloroform 10 10.9 109 70-130
95-49-8 o-Chlorotoluene 10 11.2 112 70-130
106-43-4 p-Chlorotoluene 10 11.2 112 70-130
56-23-5 Carbon tetrachloride 10 10.9 109 70-130
75-34-3 1,1-Dichloroethane 10 11.2 112 70-130
75-35-4 1,1-Dichloroethylene 10 10.9 109 70-130
563-58-6 1,1-Dichloropropene 10 11.1 111 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 10.9 109 70-130
106-93-4 1,2-Dibromoethane 10 11.2 112 70-130
107-06-2 1,2-Dichloroethane 10 11.1 111 70-130
78-87-5 1,2-Dichloropropane 10 11.0 110 70-130
142-28-9 1,3-Dichloropropane 10 11.0 110 70-130
108-20-3 Di-Isopropyl ether 10 11.2 112 70-130
594-20-7 2,2-Dichloropropane 10 10.4 104 70-130
124-48-1 Dibromochloromethane 10 11.1 111 70-130
75-71-8 Dichlorodifluoromethane 10 10.0 100 60-140
156-59-2 cis-1,2-Dichloroethylene 10 10.8 108 70-130
10061-01-5 cis-1,3-Dichloropropene 10 10.7 107 70-130
541-73-1 m-Dichlorobenzene 10 11.3 113 70-130
95-50-1 o-Dichlorobenzene 10 11.3 113 70-130
106-46-7 p-Dichlorobenzene 10 11.2 112 70-130
156-60-5 trans-1,2-Dichloroethylene 10 11.1 111 70-130
10061-02-6 trans-1,3-Dichloropropene 10 11.2 112 70-130
100-41-4 Ethylbenzene 10 11.1 111 70-130
87-68-3 Hexachlorobutadiene 10 11.6 116 70-130
98-82-8 Isopropylbenzene 10 11.1 111 70-130
* = Outside of Control Limits.
69 of 89
FA16096 55.2.2
Blank Spike Summary Page 2 of 2
Job Number:FA16096
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1495-BS A0187838.D 1 06/30/14 TD n/a n/a VA1495
The QC reported here applies to the following samples:Method: SM 6200B
FA16096-1, FA16096-2, FA16096-3, FA16096-4, FA16096-5
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 11.0 110 70-130
74-83-9 Methyl bromide 10 12.0 120 60-140
74-87-3 Methyl chloride 10 10.9 109 60-140
74-95-3 Methylene bromide 10 10.8 108 70-130
75-09-2 Methylene chloride 10 11.2 112 70-130
1634-04-4 Methyl Tert Butyl Ether 10 11.0 110 70-130
91-20-3 Naphthalene 10 11.8 118 70-130
103-65-1 n-Propylbenzene 10 11.1 111 70-130
100-42-5 Styrene 10 11.2 112 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 11.1 111 70-130
71-55-6 1,1,1-Trichloroethane 10 11.1 111 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 10.8 108 70-130
79-00-5 1,1,2-Trichloroethane 10 11.3 113 70-130
87-61-6 1,2,3-Trichlorobenzene 10 11.9 119 70-130
96-18-4 1,2,3-Trichloropropane 10 11.3 113 70-130
120-82-1 1,2,4-Trichlorobenzene 10 11.7 117 70-130
95-63-6 1,2,4-Trimethylbenzene 10 11.2 112 70-130
108-67-8 1,3,5-Trimethylbenzene 10 11.2 112 70-130
127-18-4 Tetrachloroethylene 10 11.0 110 70-130
108-88-3 Toluene 10 10.8 108 70-130
79-01-6 Trichloroethylene 10 11.5 115 70-130
75-69-4 Trichlorofluoromethane 10 10.6 106 60-140
75-01-4 Vinyl chloride 10 10.2 102 60-140
1330-20-7 Xylene (total)30 33.5 112 70-130
m,p-Xylene 20 22.4 112 70-130
95-47-6 o-Xylene 10 11.1 111 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
* = Outside of Control Limits.
70 of 89
FA16096 55.2.2
Blank Spike Summary Page 1 of 2
Job Number:FA16096
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1496-BS A0187864.D 1 07/01/14 TD n/a n/a VA1496
The QC reported here applies to the following samples:Method: SM 6200B
FA16096-11, FA16096-13, FA16096-14, FA16096-15, FA16096-16, FA16096-17, FA16096-18, FA16096-19, FA16096-
20, FA16096-21
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 8.6 86 70-130
108-86-1 Bromobenzene 10 8.3 83 70-130
74-97-5 Bromochloromethane 10 8.1 81 70-130
75-27-4 Bromodichloromethane 10 8.3 83 70-130
75-25-2 Bromoform 10 7.6 76 70-130
104-51-8 n-Butylbenzene 10 8.4 84 70-130
135-98-8 sec-Butylbenzene 10 9.4 94 70-130
98-06-6 tert-Butylbenzene 10 9.0 90 70-130
108-90-7 Chlorobenzene 10 9.0 90 70-130
75-00-3 Chloroethane 10 8.9 89 60-140
67-66-3 Chloroform 10 8.5 85 70-130
95-49-8 o-Chlorotoluene 10 9.0 90 70-130
106-43-4 p-Chlorotoluene 10 9.4 94 70-130
56-23-5 Carbon tetrachloride 10 8.5 85 70-130
75-34-3 1,1-Dichloroethane 10 8.7 87 70-130
75-35-4 1,1-Dichloroethylene 10 9.0 90 70-130
563-58-6 1,1-Dichloropropene 10 9.3 93 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 7.2 72 70-130
106-93-4 1,2-Dibromoethane 10 8.4 84 70-130
107-06-2 1,2-Dichloroethane 10 8.7 87 70-130
78-87-5 1,2-Dichloropropane 10 8.5 85 70-130
142-28-9 1,3-Dichloropropane 10 8.2 82 70-130
108-20-3 Di-Isopropyl ether 10 8.6 86 70-130
594-20-7 2,2-Dichloropropane 10 9.1 91 70-130
124-48-1 Dibromochloromethane 10 8.0 80 70-130
75-71-8 Dichlorodifluoromethane 10 7.1 71 60-140
156-59-2 cis-1,2-Dichloroethylene 10 8.5 85 70-130
10061-01-5 cis-1,3-Dichloropropene 10 8.0 80 70-130
541-73-1 m-Dichlorobenzene 10 9.1 91 70-130
95-50-1 o-Dichlorobenzene 10 8.8 88 70-130
106-46-7 p-Dichlorobenzene 10 8.3 83 70-130
156-60-5 trans-1,2-Dichloroethylene 10 9.0 90 70-130
10061-02-6 trans-1,3-Dichloropropene 10 8.9 89 70-130
100-41-4 Ethylbenzene 10 8.4 84 70-130
87-68-3 Hexachlorobutadiene 10 8.9 89 70-130
98-82-8 Isopropylbenzene 10 9.1 91 70-130
* = Outside of Control Limits.
71 of 89
FA16096 55.2.3
Blank Spike Summary Page 2 of 2
Job Number:FA16096
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1496-BS A0187864.D 1 07/01/14 TD n/a n/a VA1496
The QC reported here applies to the following samples:Method: SM 6200B
FA16096-11, FA16096-13, FA16096-14, FA16096-15, FA16096-16, FA16096-17, FA16096-18, FA16096-19, FA16096-
20, FA16096-21
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 9.1 91 70-130
74-83-9 Methyl bromide 10 11.2 112 60-140
74-87-3 Methyl chloride 10 10.0 100 60-140
74-95-3 Methylene bromide 10 8.2 82 70-130
75-09-2 Methylene chloride 10 9.0 90 70-130
1634-04-4 Methyl Tert Butyl Ether 10 8.0 80 70-130
91-20-3 Naphthalene 10 8.0 80 70-130
103-65-1 n-Propylbenzene 10 9.4 94 70-130
100-42-5 Styrene 10 8.1 81 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 8.3 83 70-130
71-55-6 1,1,1-Trichloroethane 10 8.7 87 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 7.9 79 70-130
79-00-5 1,1,2-Trichloroethane 10 8.2 82 70-130
87-61-6 1,2,3-Trichlorobenzene 10 8.3 83 70-130
96-18-4 1,2,3-Trichloropropane 10 7.8 78 70-130
120-82-1 1,2,4-Trichlorobenzene 10 8.3 83 70-130
95-63-6 1,2,4-Trimethylbenzene 10 8.3 83 70-130
108-67-8 1,3,5-Trimethylbenzene 10 8.2 82 70-130
127-18-4 Tetrachloroethylene 10 8.7 87 70-130
108-88-3 Toluene 10 8.2 82 70-130
79-01-6 Trichloroethylene 10 8.6 86 70-130
75-69-4 Trichlorofluoromethane 10 10 100 60-140
75-01-4 Vinyl chloride 10 9.4 94 60-140
1330-20-7 Xylene (total)30 26.6 89 70-130
m,p-Xylene 20 17.6 88 70-130
95-47-6 o-Xylene 10 8.9 89 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 107%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
* = Outside of Control Limits.
72 of 89
FA16096 55.2.3
Blank Spike Summary Page 1 of 2
Job Number:FA16096
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1062-BS E031761.D 1 07/01/14 TD n/a n/a VE1062
The QC reported here applies to the following samples:Method: SM 6200B
FA16096-3, FA16096-6, FA16096-7, FA16096-8, FA16096-10, FA16096-12
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 8.2 82 70-130
108-86-1 Bromobenzene 10 8.1 81 70-130
74-97-5 Bromochloromethane 10 8.3 83 70-130
75-27-4 Bromodichloromethane 10 7.6 76 70-130
75-25-2 Bromoform 10 7.2 72 70-130
104-51-8 n-Butylbenzene 10 7.8 78 70-130
135-98-8 sec-Butylbenzene 10 7.6 76 70-130
98-06-6 tert-Butylbenzene 10 7.3 73 70-130
108-90-7 Chlorobenzene 10 8.5 85 70-130
75-00-3 Chloroethane 10 8.9 89 60-140
67-66-3 Chloroform 10 7.5 75 70-130
95-49-8 o-Chlorotoluene 10 8.4 84 70-130
106-43-4 p-Chlorotoluene 10 8.8 88 70-130
56-23-5 Carbon tetrachloride 10 7.8 78 70-130
75-34-3 1,1-Dichloroethane 10 8.3 83 70-130
75-35-4 1,1-Dichloroethylene 10 7.2 72 70-130
563-58-6 1,1-Dichloropropene 10 7.4 74 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 7.2 72 70-130
106-93-4 1,2-Dibromoethane 10 8.1 81 70-130
107-06-2 1,2-Dichloroethane 10 7.9 79 70-130
78-87-5 1,2-Dichloropropane 10 8.5 85 70-130
142-28-9 1,3-Dichloropropane 10 8.1 81 70-130
108-20-3 Di-Isopropyl ether 10 8.3 83 70-130
594-20-7 2,2-Dichloropropane 10 8.0 80 70-130
124-48-1 Dibromochloromethane 10 7.8 78 70-130
75-71-8 Dichlorodifluoromethane 10 7.4 74 60-140
156-59-2 cis-1,2-Dichloroethylene 10 7.9 79 70-130
10061-01-5 cis-1,3-Dichloropropene 10 7.8 78 70-130
541-73-1 m-Dichlorobenzene 10 7.8 78 70-130
95-50-1 o-Dichlorobenzene 10 8.5 85 70-130
106-46-7 p-Dichlorobenzene 10 8.0 80 70-130
156-60-5 trans-1,2-Dichloroethylene 10 8.0 80 70-130
10061-02-6 trans-1,3-Dichloropropene 10 7.3 73 70-130
100-41-4 Ethylbenzene 10 7.8 78 70-130
87-68-3 Hexachlorobutadiene 10 7.9 79 70-130
98-82-8 Isopropylbenzene 10 7.2 72 70-130
* = Outside of Control Limits.
73 of 89
FA16096 55.2.4
Blank Spike Summary Page 2 of 2
Job Number:FA16096
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1062-BS E031761.D 1 07/01/14 TD n/a n/a VE1062
The QC reported here applies to the following samples:Method: SM 6200B
FA16096-3, FA16096-6, FA16096-7, FA16096-8, FA16096-10, FA16096-12
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 7.4 74 70-130
74-83-9 Methyl bromide 10 9.2 92 60-140
74-87-3 Methyl chloride 10 9.7 97 60-140
74-95-3 Methylene bromide 10 8.0 80 70-130
75-09-2 Methylene chloride 10 7.5 75 70-130
1634-04-4 Methyl Tert Butyl Ether 10 7.8 78 70-130
91-20-3 Naphthalene 10 7.9 79 70-130
103-65-1 n-Propylbenzene 10 7.7 77 70-130
100-42-5 Styrene 10 7.9 79 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 7.9 79 70-130
71-55-6 1,1,1-Trichloroethane 10 7.6 76 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 8.3 83 70-130
79-00-5 1,1,2-Trichloroethane 10 7.8 78 70-130
87-61-6 1,2,3-Trichlorobenzene 10 7.7 77 70-130
96-18-4 1,2,3-Trichloropropane 10 8.0 80 70-130
120-82-1 1,2,4-Trichlorobenzene 10 7.7 77 70-130
95-63-6 1,2,4-Trimethylbenzene 10 7.8 78 70-130
108-67-8 1,3,5-Trimethylbenzene 10 7.8 78 70-130
127-18-4 Tetrachloroethylene 10 8.0 80 70-130
108-88-3 Toluene 10 7.9 79 70-130
79-01-6 Trichloroethylene 10 8.0 80 70-130
75-69-4 Trichlorofluoromethane 10 8.9 89 60-140
75-01-4 Vinyl chloride 10 10.2 102 60-140
1330-20-7 Xylene (total)30 23.3 78 70-130
m,p-Xylene 20 16.1 81 70-130
95-47-6 o-Xylene 10 7.1 71 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 97%70-130%
17060-07-0 1,2-Dichloroethane-D4 94%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
* = Outside of Control Limits.
74 of 89
FA16096 55.2.4
Blank Spike Summary Page 1 of 2
Job Number:FA16096
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1063-BS E031796.D 1 07/02/14 TD n/a n/a VE1063
The QC reported here applies to the following samples:Method: SM 6200B
FA16096-9
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 10.9 109 70-130
108-86-1 Bromobenzene 10 10.9 109 70-130
74-97-5 Bromochloromethane 10 10.8 108 70-130
75-27-4 Bromodichloromethane 10 8.6 86 70-130
75-25-2 Bromoform 10 8.7 87 70-130
104-51-8 n-Butylbenzene 10 9.0 90 70-130
135-98-8 sec-Butylbenzene 10 10.3 103 70-130
98-06-6 tert-Butylbenzene 10 9.7 97 70-130
108-90-7 Chlorobenzene 10 11.4 114 70-130
75-00-3 Chloroethane 10 9.3 93 60-140
67-66-3 Chloroform 10 9.8 98 70-130
95-49-8 o-Chlorotoluene 10 11.2 112 70-130
106-43-4 p-Chlorotoluene 10 11.7 117 70-130
56-23-5 Carbon tetrachloride 10 8.7 87 70-130
75-34-3 1,1-Dichloroethane 10 10.6 106 70-130
75-35-4 1,1-Dichloroethylene 10 9.5 95 70-130
563-58-6 1,1-Dichloropropene 10 9.6 96 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 9.0 90 70-130
106-93-4 1,2-Dibromoethane 10 11.1 111 70-130
107-06-2 1,2-Dichloroethane 10 9.9 99 70-130
78-87-5 1,2-Dichloropropane 10 11.0 110 70-130
142-28-9 1,3-Dichloropropane 10 10.8 108 70-130
108-20-3 Di-Isopropyl ether 10 11.2 112 70-130
594-20-7 2,2-Dichloropropane 10 10.1 101 70-130
124-48-1 Dibromochloromethane 10 9.1 91 70-130
75-71-8 Dichlorodifluoromethane 10 7.0 70 60-140
156-59-2 cis-1,2-Dichloroethylene 10 10.9 109 70-130
10061-01-5 cis-1,3-Dichloropropene 10 8.8 88 70-130
541-73-1 m-Dichlorobenzene 10 10.5 105 70-130
95-50-1 o-Dichlorobenzene 10 11.6 116 70-130
106-46-7 p-Dichlorobenzene 10 10.7 107 70-130
156-60-5 trans-1,2-Dichloroethylene 10 10.3 103 70-130
10061-02-6 trans-1,3-Dichloropropene 10 9.7 97 70-130
100-41-4 Ethylbenzene 10 10.3 103 70-130
87-68-3 Hexachlorobutadiene 10 10.3 103 70-130
98-82-8 Isopropylbenzene 10 9.9 99 70-130
* = Outside of Control Limits.
75 of 89
FA16096 55.2.5
Blank Spike Summary Page 2 of 2
Job Number:FA16096
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1063-BS E031796.D 1 07/02/14 TD n/a n/a VE1063
The QC reported here applies to the following samples:Method: SM 6200B
FA16096-9
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 10 100 70-130
74-83-9 Methyl bromide 10 9.5 95 60-140
74-87-3 Methyl chloride 10 10.2 102 60-140
74-95-3 Methylene bromide 10 10.2 102 70-130
75-09-2 Methylene chloride 10 9.5 95 70-130
1634-04-4 Methyl Tert Butyl Ether 10 10.3 103 70-130
91-20-3 Naphthalene 10 10.6 106 70-130
103-65-1 n-Propylbenzene 10 10.4 104 70-130
100-42-5 Styrene 10 9.0 90 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 10.6 106 70-130
71-55-6 1,1,1-Trichloroethane 10 9.8 98 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 11.0 110 70-130
79-00-5 1,1,2-Trichloroethane 10 11.1 111 70-130
87-61-6 1,2,3-Trichlorobenzene 10 10.3 103 70-130
96-18-4 1,2,3-Trichloropropane 10 11.1 111 70-130
120-82-1 1,2,4-Trichlorobenzene 10 9.0 90 70-130
95-63-6 1,2,4-Trimethylbenzene 10 9.3 93 70-130
108-67-8 1,3,5-Trimethylbenzene 10 9.1 91 70-130
127-18-4 Tetrachloroethylene 10 10.8 108 70-130
108-88-3 Toluene 10 10.7 107 70-130
79-01-6 Trichloroethylene 10 10.3 103 70-130
75-69-4 Trichlorofluoromethane 10 8.8 88 60-140
75-01-4 Vinyl chloride 10 10 100 60-140
1330-20-7 Xylene (total)30 28.8 96 70-130
m,p-Xylene 20 19.1 96 70-130
95-47-6 o-Xylene 10 9.7 97 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 95%70-130%
17060-07-0 1,2-Dichloroethane-D4 91%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 96%70-130%
* = Outside of Control Limits.
76 of 89
FA16096 55.2.5
Matrix Spike Summary Page 1 of 3
Job Number:FA16096
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA16096-4MS A0187851.D 25 06/30/14 TD n/a n/a VA1495
FA16096-4 A0187857.D 25 07/01/14 TD n/a n/a VA1495
FA16096-4 A0187853.D 200 06/30/14 TD n/a n/a VA1495
The QC reported here applies to the following samples:Method: SM 6200B
FA16096-1, FA16096-2, FA16096-3, FA16096-4, FA16096-5
FA16096-4 Spike MS MS
CAS No.Compound ug/l Q ug/l ug/l %Limits
71-43-2 Benzene 458 250 749 116 70-130
108-86-1 Bromobenzene ND 250 263 105 70-130
74-97-5 Bromochloromethane ND 250 250 100 70-130
75-27-4 Bromodichloromethane ND 250 232 93 70-130
75-25-2 Bromoform ND 250 145 58*70-130
104-51-8 n-Butylbenzene 23.1 250 291 107 70-130
135-98-8 sec-Butylbenzene 15.2 250 319 122 70-130
98-06-6 tert-Butylbenzene ND 250 302 121 70-130
108-90-7 Chlorobenzene ND 250 274 110 70-130
75-00-3 Chloroethane ND 250 194 78 60-140
67-66-3 Chloroform ND 250 272 109 70-130
95-49-8 o-Chlorotoluene ND 250 365 146*70-130
106-43-4 p-Chlorotoluene ND 250 295 118 70-130
56-23-5 Carbon tetrachloride ND 250 256 102 70-130
75-34-3 1,1-Dichloroethane ND 250 261 104 70-130
75-35-4 1,1-Dichloroethylene ND 250 277 111 70-130
563-58-6 1,1-Dichloropropene ND 250 286 114 70-130
96-12-8 1,2-Dibromo-3-chloropropane ND 250 229 92 70-130
106-93-4 1,2-Dibromoethane ND 250 270 108 70-130
107-06-2 1,2-Dichloroethane ND 250 272 109 70-130
78-87-5 1,2-Dichloropropane ND 250 269 108 70-130
142-28-9 1,3-Dichloropropane ND 250 270 108 70-130
108-20-3 Di-Isopropyl ether ND 250 265 106 70-130
594-20-7 2,2-Dichloropropane ND 250 235 94 70-130
124-48-1 Dibromochloromethane ND 250 199 80 70-130
75-71-8 Dichlorodifluoromethane ND 250 154 62 60-140
156-59-2 cis-1,2-Dichloroethylene ND 250 265 106 70-130
10061-01-5 cis-1,3-Dichloropropene ND 250 243 97 70-130
541-73-1 m-Dichlorobenzene ND 250 292 117 70-130
95-50-1 o-Dichlorobenzene ND 250 283 113 70-130
106-46-7 p-Dichlorobenzene ND 250 257 103 70-130
156-60-5 trans-1,2-Dichloroethylene ND 250 275 110 70-130
10061-02-6 trans-1,3-Dichloropropene ND 250 282 113 70-130
100-41-4 Ethylbenzene 1780 b 250 2160 152* a 70-130
87-68-3 Hexachlorobutadiene ND 250 271 108 70-130
98-82-8 Isopropylbenzene 121 250 438 127 70-130
* = Outside of Control Limits.
77 of 89
FA16096 55.3.1
Matrix Spike Summary Page 2 of 3
Job Number:FA16096
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA16096-4MS A0187851.D 25 06/30/14 TD n/a n/a VA1495
FA16096-4 A0187857.D 25 07/01/14 TD n/a n/a VA1495
FA16096-4 A0187853.D 200 06/30/14 TD n/a n/a VA1495
The QC reported here applies to the following samples:Method: SM 6200B
FA16096-1, FA16096-2, FA16096-3, FA16096-4, FA16096-5
FA16096-4 Spike MS MS
CAS No.Compound ug/l Q ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 8.6 J 250 299 116 70-130
74-83-9 Methyl bromide ND 250 234 94 60-140
74-87-3 Methyl chloride ND 250 219 88 60-140
74-95-3 Methylene bromide ND 250 256 102 70-130
75-09-2 Methylene chloride ND 250 271 108 70-130
1634-04-4 Methyl Tert Butyl Ether ND 250 249 100 70-130
91-20-3 Naphthalene 511 250 832 128 70-130
103-65-1 n-Propylbenzene 379 250 697 127 70-130
100-42-5 Styrene 17.8 250 279 104 70-130
630-20-6 1,1,1,2-Tetrachloroethane ND 250 269 108 70-130
71-55-6 1,1,1-Trichloroethane ND 250 264 106 70-130
79-34-5 1,1,2,2-Tetrachloroethane ND 250 256 102 70-130
79-00-5 1,1,2-Trichloroethane ND 250 274 110 70-130
87-61-6 1,2,3-Trichlorobenzene ND 250 250 100 70-130
96-18-4 1,2,3-Trichloropropane ND 250 256 102 70-130
120-82-1 1,2,4-Trichlorobenzene ND 250 256 102 70-130
95-63-6 1,2,4-Trimethylbenzene 2340 b 250 2650 124 70-130
108-67-8 1,3,5-Trimethylbenzene 628 250 939 124 70-130
127-18-4 Tetrachloroethylene ND 250 287 115 70-130
108-88-3 Toluene 6460 b 250 5810 -260* a 70-130
79-01-6 Trichloroethylene ND 250 270 108 70-130
75-69-4 Trichlorofluoromethane ND 250 205 82 60-140
75-01-4 Vinyl chloride ND 250 205 82 60-140
1330-20-7 Xylene (total)8220 b 750 8560 45* a 70-130
m,p-Xylene 5870 b 500 5770 -20* a 70-130
95-47-6 o-Xylene 2350 b 250 2790 176* a 70-130
CAS No.Surrogate Recoveries MS FA16096-4 FA16096-4 Limits
1868-53-7 Dibromofluoromethane 96%98%100%70-130%
17060-07-0 1,2-Dichloroethane-D4 111%108%103%70-130%
2037-26-5 Toluene-D8 104%102%100%70-130%
460-00-4 4-Bromofluorobenzene 100%98%100%70-130%
(a) Outside control limits due to high level in sample relative to spike amount.
* = Outside of Control Limits.
78 of 89
FA16096 55.3.1
Matrix Spike Summary Page 3 of 3
Job Number:FA16096
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA16096-4MS A0187851.D 25 06/30/14 TD n/a n/a VA1495
FA16096-4 A0187857.D 25 07/01/14 TD n/a n/a VA1495
FA16096-4 A0187853.D 200 06/30/14 TD n/a n/a VA1495
The QC reported here applies to the following samples:Method: SM 6200B
FA16096-1, FA16096-2, FA16096-3, FA16096-4, FA16096-5
(b) Result is from Run #2.
* = Outside of Control Limits.
79 of 89
FA16096 55.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA16096
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA15875-9MS E031739.D 1 06/30/14 TD n/a n/a VE1061
FA15875-9MSD E031740.D 1 06/30/14 TD n/a n/a VE1061
FA15875-9 E031730.D 1 06/30/14 TD n/a n/a VE1061
The QC reported here applies to the following samples:Method: SM 6200B
FA16096-12, FA16096-13
FA15875-9 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
108-86-1 Bromobenzene ND 10 10.4 104 10 9.8 98 6 70-130/20
74-97-5 Bromochloromethane ND 10 10.7 107 10 10.1 101 6 70-130/20
75-27-4 Bromodichloromethane ND 10 9.8 98 10 8.8 88 11 70-130/20
75-25-2 Bromoform ND 10 8.7 87 10 7.7 77 12 70-130/20
104-51-8 n-Butylbenzene ND 10 8.7 87 10 8.4 84 4 70-130/20
135-98-8 sec-Butylbenzene ND 10 9.8 98 10 9.4 94 4 70-130/20
98-06-6 tert-Butylbenzene ND 10 9.9 99 10 9.1 91 8 70-130/20
108-90-7 Chlorobenzene ND 10 11.8 118 10 10.7 107 10 70-130/20
75-00-3 Chloroethane ND 10 10.2 102 10 9.2 92 10 60-140/20
67-66-3 Chloroform ND 10 11.0 110 10 10.1 101 9 70-130/20
95-49-8 o-Chlorotoluene ND 10 10.9 109 10 10.4 104 5 70-130/20
106-43-4 p-Chlorotoluene ND 10 11.4 114 10 10.7 107 6 70-130/20
56-23-5 Carbon tetrachloride ND 10 10.4 104 10 9.1 91 13 70-130/20
75-34-3 1,1-Dichloroethane ND 10 11.4 114 10 10.5 105 8 70-130/20
75-35-4 1,1-Dichloroethylene ND 10 10.8 108 10 9.8 98 10 70-130/20
563-58-6 1,1-Dichloropropene ND 10 10.5 105 10 9.6 96 9 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 10 9.0 90 10 8.9 89 1 70-130/20
106-93-4 1,2-Dibromoethane ND 10 10.9 109 10 10.2 102 7 70-130/20
107-06-2 1,2-Dichloroethane 0.28 J 10 12.0 117 10 11.0 107 9 70-130/20
78-87-5 1,2-Dichloropropane ND 10 11.0 110 10 10.4 104 6 70-130/20
142-28-9 1,3-Dichloropropane ND 10 10.6 106 10 10.0 100 6 70-130/20
108-20-3 Di-Isopropyl ether ND 10 11.2 112 10 10.4 104 7 70-130/20
594-20-7 2,2-Dichloropropane ND 10 12.1 121 10 10.7 107 12 70-130/20
124-48-1 Dibromochloromethane ND 10 9.3 93 10 8.1 81 14 70-130/20
75-71-8 Dichlorodifluoromethane ND 10 9.6 96 10 8.7 87 10 60-140/20
156-59-2 cis-1,2-Dichloroethylene ND 10 10.8 108 10 10.0 100 8 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 10 9.1 91 10 8.0 80 13 70-130/20
541-73-1 m-Dichlorobenzene ND 10 10.2 102 10 9.5 95 7 70-130/20
95-50-1 o-Dichlorobenzene ND 10 11.0 110 10 10.4 104 6 70-130/20
106-46-7 p-Dichlorobenzene ND 10 10.6 106 10 9.8 98 8 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 10 11.1 111 10 10.1 101 9 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 10 9.9 99 10 9.2 92 7 70-130/20
100-41-4 Ethylbenzene ND 10 10.6 106 10 9.9 99 7 70-130/20
87-68-3 Hexachlorobutadiene ND 10 10.1 101 10 9.9 99 2 70-130/20
98-82-8 Isopropylbenzene ND 10 10.4 104 10 9.5 95 9 70-130/20
99-87-6 p-Isopropyltoluene ND 10 9.6 96 10 9.1 91 5 70-130/20
* = Outside of Control Limits.
80 of 89
FA16096 55.4.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA16096
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA15875-9MS E031739.D 1 06/30/14 TD n/a n/a VE1061
FA15875-9MSD E031740.D 1 06/30/14 TD n/a n/a VE1061
FA15875-9 E031730.D 1 06/30/14 TD n/a n/a VE1061
The QC reported here applies to the following samples:Method: SM 6200B
FA16096-12, FA16096-13
FA15875-9 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
74-83-9 Methyl bromide ND 10 10.4 104 10 9.8 98 6 60-140/20
74-87-3 Methyl chloride ND 10 10.6 106 10 10.3 103 3 60-140/20
74-95-3 Methylene bromide ND 10 11.3 113 10 10.3 103 9 70-130/20
75-09-2 Methylene chloride ND 10 10.5 105 10 9.5 95 10 70-130/20
1634-04-4 Methyl Tert Butyl Ether 0.24 J 10 11.0 108 10 10.1 99 9 70-130/20
91-20-3 Naphthalene 0.20 J 10 9.7 95 10 9.5 93 2 70-130/20
103-65-1 n-Propylbenzene ND 10 9.9 99 10 9.4 94 5 70-130/20
100-42-5 Styrene ND 10 8.6 86 10 7.7 77 11 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 10 11.1 111 10 10 100 10 70-130/20
71-55-6 1,1,1-Trichloroethane ND 10 11.6 116 10 10.5 105 10 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 10 10.4 104 10 9.7 97 7 70-130/20
79-00-5 1,1,2-Trichloroethane ND 10 10.8 108 10 9.8 98 10 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 10 9.4 94 10 9.5 95 1 70-130/20
96-18-4 1,2,3-Trichloropropane ND 10 10.8 108 10 9.9 99 9 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 10 8.3 83 10 8.3 83 0 70-130/20
95-63-6 1,2,4-Trimethylbenzene 0.11 J 10 8.9 88 10 8.1 80 9 70-130/20
108-67-8 1,3,5-Trimethylbenzene ND 10 8.6 86 10 8.1 81 6 70-130/20
127-18-4 Tetrachloroethylene ND 10 11.2 112 10 10.3 103 8 70-130/20
108-88-3 Toluene ND 10 10.5 105 10 9.7 97 8 70-130/20
79-01-6 Trichloroethylene ND 10 11.1 111 10 10.2 102 8 70-130/20
75-69-4 Trichlorofluoromethane ND 10 11.3 113 10 10.1 101 11 60-140/20
75-01-4 Vinyl chloride ND 10 11.4 114 10 10.5 105 8 60-140/20
1330-20-7 Xylene (total)0.61 J 30 30.6 100 30 28.4 93 7 70-130/20
m,p-Xylene 0.22 J 20 20.1 99 20 18.7 92 7 70-130/20
95-47-6 o-Xylene 0.39 J 10 10.5 101 10 9.7 93 8 70-130/20
CAS No.Surrogate Recoveries MS MSD FA15875-9 Limits
1868-53-7 Dibromofluoromethane 104%102%101%70-130%
17060-07-0 1,2-Dichloroethane-D4 109%105%100%70-130%
2037-26-5 Toluene-D8 98%99%100%70-130%
460-00-4 4-Bromofluorobenzene 96%96%101%70-130%
* = Outside of Control Limits.
81 of 89
FA16096 55.4.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA16096
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA16096-16MS A0187879.D 1 07/01/14 TD n/a n/a VA1496
FA16096-16MSD A0187880.D 1 07/01/14 TD n/a n/a VA1496
FA16096-16 A0187870.D 1 07/01/14 TD n/a n/a VA1496
The QC reported here applies to the following samples:Method: SM 6200B
FA16096-11, FA16096-13, FA16096-14, FA16096-15, FA16096-16, FA16096-17, FA16096-18, FA16096-19, FA16096-
20, FA16096-21
FA16096-16 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene ND 10 10.4 104 10 9.4 94 10 70-130/20
108-86-1 Bromobenzene ND 10 10.1 101 10 9.0 90 12 70-130/20
74-97-5 Bromochloromethane ND 10 10.2 102 10 9.3 93 9 70-130/20
75-27-4 Bromodichloromethane ND 10 10.9 109 10 9.4 94 15 70-130/20
75-25-2 Bromoform ND 10 8.7 87 10 7.6 76 13 70-130/20
104-51-8 n-Butylbenzene ND 10 10.4 104 10 9.0 90 14 70-130/20
135-98-8 sec-Butylbenzene ND 10 11.3 113 10 10 100 12 70-130/20
98-06-6 tert-Butylbenzene ND 10 11.6 116 10 10.3 103 12 70-130/20
108-90-7 Chlorobenzene ND 10 10.9 109 10 9.8 98 11 70-130/20
75-00-3 Chloroethane ND 10 8.1 81 10 7.2 72 12 60-140/20
67-66-3 Chloroform ND 10 11.1 111 10 9.9 99 11 70-130/20
95-49-8 o-Chlorotoluene ND 10 11.1 111 10 9.8 98 12 70-130/20
106-43-4 p-Chlorotoluene ND 10 11.4 114 10 10.1 101 12 70-130/20
56-23-5 Carbon tetrachloride ND 10 11.2 112 10 9.7 97 14 70-130/20
75-34-3 1,1-Dichloroethane ND 10 11.1 111 10 10.1 101 9 70-130/20
75-35-4 1,1-Dichloroethylene ND 10 11.7 117 10 10.4 104 12 70-130/20
563-58-6 1,1-Dichloropropene ND 10 11.7 117 10 10.4 104 12 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 10 9.8 98 10 8.7 87 12 70-130/20
106-93-4 1,2-Dibromoethane ND 10 10.6 106 10 9.5 95 11 70-130/20
107-06-2 1,2-Dichloroethane ND 10 12.3 123 10 11.0 110 11 70-130/20
78-87-5 1,2-Dichloropropane ND 10 10.5 105 10 9.4 94 11 70-130/20
142-28-9 1,3-Dichloropropane ND 10 10.4 104 10 9.4 94 10 70-130/20
108-20-3 Di-Isopropyl ether ND 10 10.9 109 10 9.9 99 10 70-130/20
594-20-7 2,2-Dichloropropane ND 10 11.9 119 10 10.6 106 12 70-130/20
124-48-1 Dibromochloromethane ND 10 9.9 99 10 8.7 87 13 70-130/20
75-71-8 Dichlorodifluoromethane ND 10 7.2 72 10 6.5 65 10 60-140/20
156-59-2 cis-1,2-Dichloroethylene ND 10 10.3 103 10 9.3 93 10 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 10 9.7 97 10 8.5 85 13 70-130/20
541-73-1 m-Dichlorobenzene ND 10 11.1 111 10 10 100 10 70-130/20
95-50-1 o-Dichlorobenzene ND 10 10.8 108 10 9.6 96 12 70-130/20
106-46-7 p-Dichlorobenzene ND 10 10.2 102 10 9.0 90 13 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 10 11.5 115 10 10.1 101 13 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 10 11.3 113 10 9.8 98 14 70-130/20
100-41-4 Ethylbenzene ND 10 10.3 103 10 9.2 92 11 70-130/20
87-68-3 Hexachlorobutadiene ND 10 11.2 112 10 9.9 99 12 70-130/20
98-82-8 Isopropylbenzene ND 10 11.1 111 10 10.0 100 10 70-130/20
* = Outside of Control Limits.
82 of 89
FA16096 55.4.2
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA16096
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA16096-16MS A0187879.D 1 07/01/14 TD n/a n/a VA1496
FA16096-16MSD A0187880.D 1 07/01/14 TD n/a n/a VA1496
FA16096-16 A0187870.D 1 07/01/14 TD n/a n/a VA1496
The QC reported here applies to the following samples:Method: SM 6200B
FA16096-11, FA16096-13, FA16096-14, FA16096-15, FA16096-16, FA16096-17, FA16096-18, FA16096-19, FA16096-
20, FA16096-21
FA16096-16 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 10 10.7 107 10 9.4 94 13 70-130/20
74-83-9 Methyl bromide ND 10 10.4 104 10 9.4 94 10 60-140/20
74-87-3 Methyl chloride 0.16 J 10 9.5 93 10 8.6 84 10 60-140/20
74-95-3 Methylene bromide ND 10 10.8 108 10 9.7 97 11 70-130/20
75-09-2 Methylene chloride ND 10 11.9 119 10 10.6 106 12 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 10 10.1 101 10 9.2 92 9 70-130/20
91-20-3 Naphthalene ND 10 9.6 96 10 8.6 86 11 70-130/20
103-65-1 n-Propylbenzene ND 10 11.3 113 10 9.9 99 13 70-130/20
100-42-5 Styrene ND 10 7.8 78 10 6.3 63*21*70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 10 10.6 106 10 9.4 94 12 70-130/20
71-55-6 1,1,1-Trichloroethane ND 10 11.5 115 10 10.3 103 11 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 10 10 100 10 8.8 88 13 70-130/20
79-00-5 1,1,2-Trichloroethane ND 10 10.3 103 10 9.3 93 10 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 10 10.3 103 10 9.4 94 9 70-130/20
96-18-4 1,2,3-Trichloropropane ND 10 10.1 101 10 8.9 89 13 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 10 10.3 103 10 9.4 94 9 70-130/20
95-63-6 1,2,4-Trimethylbenzene ND 10 9.2 92 10 7.7 77 18 70-130/20
108-67-8 1,3,5-Trimethylbenzene ND 10 8.8 88 10 7.2 72 20 70-130/20
127-18-4 Tetrachloroethylene ND 10 10.6 106 10 9.6 96 10 70-130/20
108-88-3 Toluene ND 10 9.8 98 10 8.7 87 12 70-130/20
79-01-6 Trichloroethylene ND 10 11.0 110 10 9.8 98 12 70-130/20
75-69-4 Trichlorofluoromethane ND 10 10.3 103 10 9.2 92 11 60-140/20
75-01-4 Vinyl chloride ND 10 8.3 83 10 7.6 76 9 60-140/20
1330-20-7 Xylene (total)ND 30 31.3 104 30 27.4 91 13 70-130/20
m,p-Xylene ND 20 20.7 104 20 18.0 90 14 70-130/20
95-47-6 o-Xylene ND 10 10.6 106 10 9.4 94 12 70-130/20
CAS No.Surrogate Recoveries MS MSD FA16096-16 Limits
1868-53-7 Dibromofluoromethane 107%108%103%70-130%
17060-07-0 1,2-Dichloroethane-D4 124%122%111%70-130%
2037-26-5 Toluene-D8 98%99%87%70-130%
460-00-4 4-Bromofluorobenzene 101%101%100%70-130%
* = Outside of Control Limits.
83 of 89
FA16096 55.4.2
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA16096
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA16096-6MS E031774.D 1 07/01/14 TD n/a n/a VE1062
FA16096-6MSD E031775.D 1 07/01/14 TD n/a n/a VE1062
FA16096-6 E031764.D 1 07/01/14 TD n/a n/a VE1062
The QC reported here applies to the following samples:Method: SM 6200B
FA16096-3, FA16096-6, FA16096-7, FA16096-8, FA16096-10, FA16096-12
FA16096-6 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene ND 10 11.8 118 10 10.9 109 8 70-130/20
108-86-1 Bromobenzene ND 10 11.4 114 10 10.4 104 9 70-130/20
74-97-5 Bromochloromethane ND 10 11.7 117 10 10.9 109 7 70-130/20
75-27-4 Bromodichloromethane ND 10 9.8 98 10 8.8 88 11 70-130/20
75-25-2 Bromoform ND 10 8.8 88 10 7.9 79 11 70-130/20
104-51-8 n-Butylbenzene ND 10 8.7 87 10 8.3 83 5 70-130/20
135-98-8 sec-Butylbenzene ND 10 10.2 102 10 9.6 96 6 70-130/20
98-06-6 tert-Butylbenzene ND 10 10.0 100 10 9.4 94 6 70-130/20
108-90-7 Chlorobenzene ND 10 12.1 121 10 11.2 112 8 70-130/20
75-00-3 Chloroethane ND 10 9.6 96 10 9.4 94 2 60-140/20
67-66-3 Chloroform ND 10 11.0 110 10 10.2 102 8 70-130/20
95-49-8 o-Chlorotoluene ND 10 11.6 116 10 10.8 108 7 70-130/20
106-43-4 p-Chlorotoluene ND 10 12.3 123 10 11.2 112 9 70-130/20
56-23-5 Carbon tetrachloride ND 10 10.2 102 10 9.2 92 10 70-130/20
75-34-3 1,1-Dichloroethane ND 10 11.6 116 10 10.7 107 8 70-130/20
75-35-4 1,1-Dichloroethylene ND 10 11.0 110 10 10 100 10 70-130/20
563-58-6 1,1-Dichloropropene ND 10 10.6 106 10 9.8 98 8 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 10 10 100 10 9.2 92 8 70-130/20
106-93-4 1,2-Dibromoethane ND 10 11.5 115 10 10.6 106 8 70-130/20
107-06-2 1,2-Dichloroethane ND 10 11.3 113 10 10.6 106 6 70-130/20
78-87-5 1,2-Dichloropropane ND 10 11.6 116 10 11.1 111 4 70-130/20
142-28-9 1,3-Dichloropropane ND 10 11.5 115 10 10.5 105 9 70-130/20
108-20-3 Di-Isopropyl ether ND 10 11.8 118 10 11.1 111 6 70-130/20
594-20-7 2,2-Dichloropropane ND 10 11.8 118 10 10.7 107 10 70-130/20
124-48-1 Dibromochloromethane ND 10 9.2 92 10 8.4 84 9 70-130/20
75-71-8 Dichlorodifluoromethane ND 10 8.1 81 10 7.7 77 5 60-140/20
156-59-2 cis-1,2-Dichloroethylene ND 10 11.9 119 10 10.8 108 10 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 10 8.9 89 10 8.0 80 11 70-130/20
541-73-1 m-Dichlorobenzene ND 10 10.9 109 10 10.1 101 8 70-130/20
95-50-1 o-Dichlorobenzene ND 10 11.9 119 10 11.2 112 6 70-130/20
106-46-7 p-Dichlorobenzene ND 10 10.9 109 10 10.4 104 5 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 10 11.5 115 10 10.7 107 7 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 10 10.0 100 10 8.9 89 12 70-130/20
100-41-4 Ethylbenzene ND 10 10.9 109 10 10.0 100 9 70-130/20
87-68-3 Hexachlorobutadiene ND 10 8.9 89 10 8.9 89 0 70-130/20
98-82-8 Isopropylbenzene ND 10 10.4 104 10 9.5 95 9 70-130/20
* = Outside of Control Limits.
84 of 89
FA16096 55.4.3
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA16096
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA16096-6MS E031774.D 1 07/01/14 TD n/a n/a VE1062
FA16096-6MSD E031775.D 1 07/01/14 TD n/a n/a VE1062
FA16096-6 E031764.D 1 07/01/14 TD n/a n/a VE1062
The QC reported here applies to the following samples:Method: SM 6200B
FA16096-3, FA16096-6, FA16096-7, FA16096-8, FA16096-10, FA16096-12
FA16096-6 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 10 9.8 98 10 9.3 93 5 70-130/20
74-83-9 Methyl bromide ND 10 10.3 103 10 9.4 94 9 60-140/20
74-87-3 Methyl chloride ND 10 10.4 104 10 10.1 101 3 60-140/20
74-95-3 Methylene bromide ND 10 11.4 114 10 10.7 107 6 70-130/20
75-09-2 Methylene chloride ND 10 10.8 108 10 10.1 101 7 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 10 11.2 112 10 10.7 107 5 70-130/20
91-20-3 Naphthalene ND 10 10.1 101 10 10.2 102 1 70-130/20
103-65-1 n-Propylbenzene ND 10 10.6 106 10 9.8 98 8 70-130/20
100-42-5 Styrene ND 10 7.9 79 10 7.1 71 11 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 10 11.5 115 10 10.4 104 10 70-130/20
71-55-6 1,1,1-Trichloroethane ND 10 11.2 112 10 10.6 106 6 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 10 11.6 116 10 10.9 109 6 70-130/20
79-00-5 1,1,2-Trichloroethane ND 10 11.5 115 10 10.7 107 7 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 10 9.3 93 10 9.5 95 2 70-130/20
96-18-4 1,2,3-Trichloropropane ND 10 11.7 117 10 10.7 107 9 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 10 8.2 82 10 8.4 84 2 70-130/20
95-63-6 1,2,4-Trimethylbenzene ND 10 8.8 88 10 8.2 82 7 70-130/20
108-67-8 1,3,5-Trimethylbenzene ND 10 8.4 84 10 7.8 78 7 70-130/20
127-18-4 Tetrachloroethylene 0.55 10 11.9 114 10 11.0 105 8 70-130/20
108-88-3 Toluene ND 10 10.9 109 10 9.9 99 10 70-130/20
79-01-6 Trichloroethylene 0.17 J 10 11.6 114 10 10.6 104 9 70-130/20
75-69-4 Trichlorofluoromethane ND 10 9.8 98 10 9.2 92 6 60-140/20
75-01-4 Vinyl chloride ND 10 10.6 106 10 10.3 103 3 60-140/20
1330-20-7 Xylene (total)ND 30 29.4 98 30 27.1 90 8 70-130/20
m,p-Xylene ND 20 19.5 98 20 18.0 90 8 70-130/20
95-47-6 o-Xylene ND 10 9.9 99 10 9.1 91 8 70-130/20
CAS No.Surrogate Recoveries MS MSD FA16096-6 Limits
1868-53-7 Dibromofluoromethane 100%99%101%70-130%
17060-07-0 1,2-Dichloroethane-D4 101%99%102%70-130%
2037-26-5 Toluene-D8 97%96%97%70-130%
460-00-4 4-Bromofluorobenzene 97%98%100%70-130%
* = Outside of Control Limits.
85 of 89
FA16096 55.4.3
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA16096
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA16129-16MS E031814.D 1 07/02/14 TD n/a n/a VE1063
FA16129-16MSD E031815.D 1 07/02/14 TD n/a n/a VE1063
FA16129-16 E031810.D 1 07/02/14 TD n/a n/a VE1063
The QC reported here applies to the following samples:Method: SM 6200B
FA16096-9
FA16129-16 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene ND 10 10.0 100 10 9.9 99 1 70-130/20
108-86-1 Bromobenzene ND 10 9.9 99 10 9.9 99 0 70-130/20
74-97-5 Bromochloromethane ND 10 9.8 98 10 9.9 99 1 70-130/20
75-27-4 Bromodichloromethane ND 10 8.3 83 10 8.2 82 1 70-130/20
75-25-2 Bromoform ND 10 7.1 71 10 7.1 71 0 70-130/20
104-51-8 n-Butylbenzene ND 10 7.9 79 10 7.8 78 1 70-130/20
135-98-8 sec-Butylbenzene ND 10 9.4 94 10 9.1 91 3 70-130/20
98-06-6 tert-Butylbenzene ND 10 9.2 92 10 8.9 89 3 70-130/20
108-90-7 Chlorobenzene ND 10 10.8 108 10 11.0 110 2 70-130/20
75-00-3 Chloroethane ND 10 8.9 89 10 8.8 88 1 60-140/20
67-66-3 Chloroform ND 10 9.5 95 10 9.3 93 2 70-130/20
95-49-8 o-Chlorotoluene ND 10 10.3 103 10 10.2 102 1 70-130/20
106-43-4 p-Chlorotoluene ND 10 10.8 108 10 10.6 106 2 70-130/20
56-23-5 Carbon tetrachloride ND 10 8.8 88 10 8.4 84 5 70-130/20
75-34-3 1,1-Dichloroethane ND 10 10.1 101 10 9.8 98 3 70-130/20
75-35-4 1,1-Dichloroethylene ND 10 9.3 93 10 9.0 90 3 70-130/20
563-58-6 1,1-Dichloropropene ND 10 9.1 91 10 9.0 90 1 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 10 8.6 86 10 8.6 86 0 70-130/20
106-93-4 1,2-Dibromoethane ND 10 10.1 101 10 10.3 103 2 70-130/20
107-06-2 1,2-Dichloroethane ND 10 9.8 98 10 9.8 98 0 70-130/20
78-87-5 1,2-Dichloropropane ND 10 10.0 100 10 10.1 101 1 70-130/20
142-28-9 1,3-Dichloropropane ND 10 10.2 102 10 10.4 104 2 70-130/20
108-20-3 Di-Isopropyl ether ND 10 10.1 101 10 10.2 102 1 70-130/20
594-20-7 2,2-Dichloropropane ND 10 10.3 103 10 10.2 102 1 70-130/20
124-48-1 Dibromochloromethane ND 10 8.0 80 10 8.0 80 0 70-130/20
75-71-8 Dichlorodifluoromethane ND 10 8.9 89 10 8.3 83 7 60-140/20
156-59-2 cis-1,2-Dichloroethylene ND 10 10.0 100 10 9.8 98 2 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 10 7.9 79 10 7.7 77 3 70-130/20
541-73-1 m-Dichlorobenzene ND 10 9.5 95 10 9.6 96 1 70-130/20
95-50-1 o-Dichlorobenzene ND 10 10.5 105 10 10.5 105 0 70-130/20
106-46-7 p-Dichlorobenzene ND 10 9.8 98 10 9.8 98 0 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 10 9.9 99 10 9.5 95 4 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 10 9.0 90 10 9.1 91 1 70-130/20
100-41-4 Ethylbenzene ND 10 9.8 98 10 9.6 96 2 70-130/20
87-68-3 Hexachlorobutadiene ND 10 8.4 84 10 8.2 82 2 70-130/20
98-82-8 Isopropylbenzene ND 10 9.4 94 10 9.2 92 2 70-130/20
* = Outside of Control Limits.
86 of 89
FA16096 55.4.4
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA16096
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA16129-16MS E031814.D 1 07/02/14 TD n/a n/a VE1063
FA16129-16MSD E031815.D 1 07/02/14 TD n/a n/a VE1063
FA16129-16 E031810.D 1 07/02/14 TD n/a n/a VE1063
The QC reported here applies to the following samples:Method: SM 6200B
FA16096-9
FA16129-16 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 10 8.9 89 10 8.9 89 0 70-130/20
74-83-9 Methyl bromide ND 10 7.9 79 10 7.9 79 0 60-140/20
74-87-3 Methyl chloride 0.19 J 10 11.0 108 10 10.7 105 3 60-140/20
74-95-3 Methylene bromide ND 10 9.8 98 10 9.9 99 1 70-130/20
75-09-2 Methylene chloride ND 10 9.1 91 10 8.9 89 2 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 10 9.6 96 10 9.8 98 2 70-130/20
91-20-3 Naphthalene ND 10 9.0 90 10 9.1 91 1 70-130/20
103-65-1 n-Propylbenzene ND 10 9.5 95 10 9.4 94 1 70-130/20
100-42-5 Styrene ND 10 7.5 75 10 7.5 75 0 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 10 10.0 100 10 10.3 103 3 70-130/20
71-55-6 1,1,1-Trichloroethane ND 10 9.7 97 10 9.6 96 1 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 10 10.1 101 10 10.4 104 3 70-130/20
79-00-5 1,1,2-Trichloroethane ND 10 9.8 98 10 10.2 102 4 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 10 8.7 87 10 8.5 85 2 70-130/20
96-18-4 1,2,3-Trichloropropane ND 10 10.1 101 10 10.6 106 5 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 10 7.6 76 10 7.6 76 0 70-130/20
95-63-6 1,2,4-Trimethylbenzene ND 10 8.1 81 10 8.0 80 1 70-130/20
108-67-8 1,3,5-Trimethylbenzene ND 10 8.2 82 10 7.9 79 4 70-130/20
127-18-4 Tetrachloroethylene ND 10 10.2 102 10 10.1 101 1 70-130/20
108-88-3 Toluene ND 10 9.9 99 10 9.8 98 1 70-130/20
79-01-6 Trichloroethylene ND 10 9.8 98 10 9.4 94 4 70-130/20
75-69-4 Trichlorofluoromethane ND 10 8.1 81 10 7.9 79 2 60-140/20
75-01-4 Vinyl chloride ND 10 10 100 10 9.6 96 4 60-140/20
1330-20-7 Xylene (total)ND 30 27.2 91 30 27.0 90 1 70-130/20
m,p-Xylene ND 20 18.0 90 20 17.9 90 1 70-130/20
95-47-6 o-Xylene ND 10 9.2 92 10 9.2 92 0 70-130/20
CAS No.Surrogate Recoveries MS MSD FA16129-16 Limits
1868-53-7 Dibromofluoromethane 97%96%95%70-130%
17060-07-0 1,2-Dichloroethane-D4 98%96%89%70-130%
2037-26-5 Toluene-D8 99%99%97%70-130%
460-00-4 4-Bromofluorobenzene 97%97%97%70-130%
* = Outside of Control Limits.
87 of 89
FA16096 55.4.4
Duplicate Summary Page 1 of 2
Job Number:FA16096
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA16096-4DUP A0187852.D 200 06/30/14 TD n/a n/a VA1495
FA16096-4 A0187857.D 25 07/01/14 TD n/a n/a VA1495
FA16096-4 A0187853.D 200 06/30/14 TD n/a n/a VA1495
The QC reported here applies to the following samples:Method: SM 6200B
FA16096-1, FA16096-2, FA16096-3, FA16096-4, FA16096-5
FA16096-4 DUP
CAS No.Compound ug/l Q ug/l Q RPD Limits
71-43-2 Benzene 458 523 13 20
108-86-1 Bromobenzene ND ND nc 20
74-97-5 Bromochloromethane ND ND nc 20
75-27-4 Bromodichloromethane ND ND nc 20
75-25-2 Bromoform ND ND nc 20
104-51-8 n-Butylbenzene 23.1 31.5 J 31*20
135-98-8 sec-Butylbenzene 15.2 ND 200*20
98-06-6 tert-Butylbenzene ND ND nc 20
108-90-7 Chlorobenzene ND ND nc 20
75-00-3 Chloroethane ND ND nc 20
67-66-3 Chloroform ND ND nc 20
95-49-8 o-Chlorotoluene ND ND nc 20
106-43-4 p-Chlorotoluene ND ND nc 20
56-23-5 Carbon tetrachloride ND ND nc 20
75-34-3 1,1-Dichloroethane ND ND nc 20
75-35-4 1,1-Dichloroethylene ND ND nc 20
563-58-6 1,1-Dichloropropene ND ND nc 20
96-12-8 1,2-Dibromo-3-chloropropane ND ND nc 20
106-93-4 1,2-Dibromoethane ND ND nc 20
107-06-2 1,2-Dichloroethane ND ND nc 20
78-87-5 1,2-Dichloropropane ND ND nc 20
142-28-9 1,3-Dichloropropane ND ND nc 20
108-20-3 Di-Isopropyl ether ND ND nc 20
594-20-7 2,2-Dichloropropane ND ND nc 20
124-48-1 Dibromochloromethane ND ND nc 20
75-71-8 Dichlorodifluoromethane ND ND nc 20
156-59-2 cis-1,2-Dichloroethylene ND ND nc 20
10061-01-5 cis-1,3-Dichloropropene ND ND nc 20
541-73-1 m-Dichlorobenzene ND ND nc 20
95-50-1 o-Dichlorobenzene ND ND nc 20
106-46-7 p-Dichlorobenzene ND ND nc 20
156-60-5 trans-1,2-Dichloroethylene ND ND nc 20
10061-02-6 trans-1,3-Dichloropropene ND ND nc 20
100-41-4 Ethylbenzene 1780 a 1980 11 20
87-68-3 Hexachlorobutadiene ND ND nc 20
98-82-8 Isopropylbenzene 121 126 4 20
* = Outside of Control Limits.
88 of 89
FA16096 55.5.1
Duplicate Summary Page 2 of 2
Job Number:FA16096
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 15, 1109 US 64 E, Plymouth, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA16096-4DUP A0187852.D 200 06/30/14 TD n/a n/a VA1495
FA16096-4 A0187857.D 25 07/01/14 TD n/a n/a VA1495
FA16096-4 A0187853.D 200 06/30/14 TD n/a n/a VA1495
The QC reported here applies to the following samples:Method: SM 6200B
FA16096-1, FA16096-2, FA16096-3, FA16096-4, FA16096-5
FA16096-4 DUP
CAS No.Compound ug/l Q ug/l Q RPD Limits
99-87-6 p-Isopropyltoluene 8.6 J ND 200*20
74-83-9 Methyl bromide ND ND nc 20
74-87-3 Methyl chloride ND ND nc 20
74-95-3 Methylene bromide ND ND nc 20
75-09-2 Methylene chloride ND ND nc 20
1634-04-4 Methyl Tert Butyl Ether ND ND nc 20
91-20-3 Naphthalene 511 685 29*20
103-65-1 n-Propylbenzene 379 405 7 20
100-42-5 Styrene 17.8 25.4 J 35*20
630-20-6 1,1,1,2-Tetrachloroethane ND ND nc 20
71-55-6 1,1,1-Trichloroethane ND ND nc 20
79-34-5 1,1,2,2-Tetrachloroethane ND ND nc 20
79-00-5 1,1,2-Trichloroethane ND ND nc 20
87-61-6 1,2,3-Trichlorobenzene ND ND nc 20
96-18-4 1,2,3-Trichloropropane ND ND nc 20
120-82-1 1,2,4-Trichlorobenzene ND ND nc 20
95-63-6 1,2,4-Trimethylbenzene 2340 a 2640 12 20
108-67-8 1,3,5-Trimethylbenzene 628 713 13 20
127-18-4 Tetrachloroethylene ND ND nc 20
108-88-3 Toluene 6460 a 7170 10 20
79-01-6 Trichloroethylene ND ND nc 20
75-69-4 Trichlorofluoromethane ND ND nc 20
75-01-4 Vinyl chloride ND ND nc 20
1330-20-7 Xylene (total)8220 a 9130 10 20
m,p-Xylene 5870 a 6520 10 20
95-47-6 o-Xylene 2350 a 2610 10 20
CAS No.Surrogate Recoveries DUP FA16096-4 FA16096-4 Limits
1868-53-7 Dibromofluoromethane 98%98%100%70-130%
17060-07-0 1,2-Dichloroethane-D4 105%108%103%70-130%
2037-26-5 Toluene-D8 100%102%100%70-130%
460-00-4 4-Bromofluorobenzene 100%98%100%70-130%
(a) Result is from Run #2.
* = Outside of Control Limits.
89 of 89
FA16096 55.5.1