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Home My WebLink AboutWA-813_11174_CA_MRP_20220429 3502 Hayes Road • Monroe, North Carolina 28110 113 West Firetower Road, Suite G • Winterville, North Carolina 28590 Phone (704) 845-4010 • (888) 870-4133 • Fax (704) 845-4012 April 29, 2022 Ms. Carrie Stone North Carolina Department of Environmental Quality Washington Regional Office 943 Washington Square Mall Washington, North Carolina 27889 Re: Ground Water Monitoring Report February - March 2022 Everette’s Enterprises 1101 Dr. Martin Luther King, Jr. Drive Ahoskie, Hertford County North Carolina Facility ID Number: 0-00-0000009694 Incident Numbers: 11174 GRI Project Number: 2459 Dear Ms. Stone, Please find enclosed the referenced report for the above mentioned site. If you have any questions, please contact William Regenthal at 704-845-4010. Sincerely, Geological Resources, Inc. Leslie Maxtone-Graham Administrative Assistant Enclosure Cc: Ms. Bea Harrison, North East Oil Company, Inc., file 3502 Hayes Road • Monroe, North Carolina 28110 113 West Firetower Road, Suite G • Winterville, North Carolina 28590 Phone (704) 845-4010 • (888) 870-4133 • Fax (704) 845-4012 Ground Water Monitoring Report February - March 2022 Everette’s Enterprises 1101 Dr. Martin Luther King, Jr. Drive Ahoskie, Hertford County North Carolina Facility ID Number: 0-00-0000009694 Incident Number: 11174 GRI Project Number: 2459 Prepared for: North East Oil Company, Inc. Post Office Box 1386 Ahoskie, North Carolina 27910 April 29, 2022 William Regenthal Project Manager, P.G. Ethan Rogerson, G.I.T. Report Writer ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: April 29, 2022 Everette’s Enterprises Project Manager: William Regenthal GRI Project No. 2459 i SITE INFORMATION 1. Site Identification  Everette’s Enterprises (Facility ID 0-00-0000009694)  Incident Number 11174 – Intermediate Risk (I090R)  Location of Source Area: 1101 Dr. Martin Luther King, Jr. Drive Ahoskie, NC 27910 Hertford County 36.290639°N, 76.973306°W (Topographical Map) 2. Information about Contacts Associated with the Leaking UST System UST Owner North East Oil Company, Inc. Post Office Box 1386 Ahoskie, NC 27910 beah@bent-prises.com 252-862-0236 UST Operator North East Oil Company, Inc. Post Office Box 1386 Ahoskie, NC 27910 beah@bent-prises.com 252-862-0236 Property Owner Clyde W. Everett 414 Troy Street East Ahoskie, NC 27910 Email unknown Phone unknown Property Occupant Convenience Store 1101 Dr. Martin Luther King, Jr. Drive Ahoskie, NC 27910 Email unknown Phone unknown Consultant/Contractor Geological Resources, Inc. 3502 Hayes Road Monroe, NC 28110 wlr@geologicalresourcesinc.com 704-845-4010 Analytical Laboratory SGS North America, Inc. 4405 Vineland Road, Suite C-15 Orlando, FL 32811 State Certification No. 573 407-425-6700 3. Information about Release  Release was discovered in September 1993.  An unknown amount of product was released from the leaking UST System.  Three 1,000-gallon USTs removed in September 1993. ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: April 29, 2022 Everette’s Enterprises Project Manager: William Regenthal GRI Project No. 2459 ii EXECUTIVE SUMMARY The former Everette’s Enterprises is located at 1101 Dr. Martin Luther King, Jr. Drive in Ahoskie, Hertford County, North Carolina. The site is currently owned and operated by Clyde Everette as a convenience store. According to available information, a release was discovered at the site when three 1,000-gallon gasoline USTs were removed in September 1993. The adjoining properties are a mixture of commercial and residential properties. According to the information determined from historical information, no water supply wells were identified within 1,000 feet of the site. Public water is available to the site and surrounding properties. On February 23, 2022, an AFVR event was conducted at the site on monitoring wells MW-2 and MWD-24. Please note, prior to the start of the AFVR event, MW-3 was not located, and MWD-24 was connected as an extraction well in error. Prior to the start of the AFVR event, ground water samples were collected from MW-2 and MWD-24. Concentrations of individual BTEX constituents, MTBE and naphthalene that exceeded the MACs were reported in the ground water sample collected from MW-2 prior to the start of the AFVR event. The AFVR event lasted 7.5 hours, instead of the full 8 hours because the vacuum truck became full. A total of 2,576 gallons of affected ground water was recovered during the AFVR event. No measurable liquid free product was recovered during this AFVR event. At the conclusion of the event, no free product was measured in the vacuumed wells or any of the observation wells. The average fluid recovery rate was 343.33 gallons per hour. Based on mass-removal calculations an additional 0.19 pounds or 0.03 gallons of vapor phase hydrocarbons were removed at an average rate of less than 0.01 gallons per hour. On March 23, 2022, five Type II monitoring wells (MW-1, MW-2, MW-3, MW-13 and MW-15) were gauged, purged and sampled. Free product was not observed during the March 2022 sampling event. Concentrations of individual BTEX constituents, MTBE, naphthalene, EDB, 1,2-dichloroethane 1,1,2,2- tetrachloroethane, isopropylbenzene, n-propylbenzene, 1,2,4-trimethylbenzene and/or 1,3,5- trimethylbenzene that exceeded the MACs were reported in ground water samples collected from MW- 1, MW-2, MW-3 and MW-13. All reported contaminant concentrations were less than the GCLs. Based on this information, the AFVR event was effective in reducing the contaminant concentrations to less than GCLs. Ground water monitoring should continue at the site, to confirm the results of the March 2022 sampling event. The next ground water sampling event is tentatively scheduled for September 2022. If the contaminant concentrations remain less than the GCLs, an NRP should be filed, and the site closed with an NFA. ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: April 29, 2022 Everette’s Enterprises Project Manager: William Regenthal GRI Project No. 2459 iii ACRONYMS ACM: Asbestos Containing Materials AFVR: Aggressive Fluid-Vapor Recovery ARR: Acknowledgement of Report Receipt AS: Air Sparging AST: Aboveground Storage Tank ASTM: American Society for Testing and Materials BGS: Below Ground Surface CAP: Corrective Action Plan CFR: Code of Federal Regulations CSA: Comprehensive Site Assessment DPE: Dual Phase Extraction DRO: Total Petroleum Hydrocarbons Diesel Range Organics DWM: Division of Waste Management DWR: Department of Water Resources EPA: Environmental Protection Agency EPH: Extractible Petroleum Hydrocarbons ESA: Environmental Site Assessment GAS: Greenwood Applied Services, LLC GCL: Gross Contamination Level GRI: Geological Resources, Inc. GRO: Total Petroleum Hydrocarbons Gasoline Range Organics LSA: Limited Site Assessment MAC: Maximum Allowable Concentration as specified in T15A NCAC 2L.0202 MADEP: Massachusetts Department of Environmental Protection MCC: Maximum Contaminant Concentrations MMPE: Mobile Multi-Phase Extraction NAPL: Non-Aqueous Phase Liquid, “Free Product” NCDEQ: North Carolina Department of Environmental Quality NCDOT: North Carolina Department of Transportation NFA: Notice of No Further Action NORR: Notice of Regulatory Requirements NOV: Notice of Violation NPDES: National Pollutant Discharge Elimination System NRP: Notice of Residual Petroleum O&M: Operation and Maintenance PAHs: Polynuclear Aromatic Hydrocarbons PCA: Pre-Construction Assessment RAL: Regulatory Action Level SCLs: Soil Cleanup Level SPCC: Spill Prevention Control and Countermeasures SVE: Soil Vapor Extraction SVOCs: Semi-Volatile Organic Compounds SWPPP: Stormwater Pollution Prevention Plan TCLP: Toxicity Characteristic Leaching Procedure (EPA Method SW-846 1311) TOC: Top of Casing TPH: Total Petroleum Hydrocarbons USGS: United States Geological Survey UST: Underground Storage Tank UVF: Ultraviolet Fluorescence VOCs: Volatile Organic Compounds VPH: Volatile Petroleum Hydrocarbons ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: April 29, 2022 Everette’s Enterprises Project Manager: William Regenthal GRI Project No. 2459 TABLE OF CONTENTS SITE INFORMATION ............................................................................................................................ i EXECUTIVE SUMMARY ....................................................................................................................... ii ACRONYMS ....................................................................................................................................... iii 1.0 SITE HISTORY AND CHARACTERIZATION ...................................................................................1 2.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL ASSESSMENT INFORMATION ...................................................................................................2 3.0 AGGRESSIVE FLUID-VAPOR RECOVERY EVENT ..........................................................................4 4.0 CONCLUSIONS .........................................................................................................................5 5.0 LIMITATIONS ...........................................................................................................................6 6.0 STATEMENTS AND CERTIFICATION ...........................................................................................6 FIGURES Figure 1: Site Location Map Figure 2: Site Vicinity Map Figure 3: Site Map Figure 4: Water Table Surface Map Figure 5: Ground Water Quality Map Figure 6: Estimated Contaminant Mass Area TABLES Table 1: UST Owner and Operator Information Table 2: UST System Information Table 3: Adjacent Property Owner Information Table 4: Well Construction and Gauging Information Table 5: Summary of Ground Water Sample Analytical Results Table 6: Free Product Recovery Results Table 7: Free Product Recovery Event Information Table 8: Free Product Recovery Cost Summary APPENDICES Appendix A: State Correspondence Appendix B: Laboratory Reports – Ground Water Appendix C: AFVR Calculations and Disposal Manifest Appendix D: Contaminant Mass Calculations ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: April 29, 2022 Everette’s Enterprises Project Manager: William Regenthal GRI Project No. 2459 1 1.0 SITE HISTORY AND CHARACTERIZATION GRI presents the results of the February 2022 AFVR event and the March 2022 ground water sampling conducted at the Everette’s Enterprises site; located at 1101 Dr. Martin Luther King, Jr. Drive in Ahoskie, Hertford County, North Carolina (Figure 1). These activities were conducted in accordance with GRI Proposal No. 21-561, which was submitted to the NCDEQ on August 31, 2021, and was approved as Task Authorization No. 11174-29 on September 16, 2021. State correspondence has been included as Appendix A. The site is currently owned by Clyde W. Everette and is a convenience store. According to available information, three 1,000-gallon gasoline USTs were removed from the site in September 1993. A release was discovered at the site when petroleum impacted soil was encountered during the September 1993 UST closure event. UST owner/operator information and UST system information are included as Tables 1 and 2, respectively. The Registered Tank Report is shown below: The site and surrounding area are a mixture of residential and agricultural properties. The site is an active convenience store and is primarily capped with concrete. The overall topography at the site is relatively flat. Eighteen Type II monitoring wells (MW-1 through MW-4, MW-6 through MW-8 and MW-10 through MW-20) and two vertical extent ground water monitoring wells (MWD-5 and MWD-9) were installed at the site during previous ground water assessment activities conducted by CES Engineering, PC, between 1993 and 1995. Monitoring wells MW-21 through MW-23 were installed under the supervision of GRI in October 2012. Monitoring wells MWD-24 and MWD-25 were installed under the supervision of GRI in August 2013. On January 12, 2021, receptor information was updated for the site. No water supply wells were identified within 1,500 feet of the source area. No surface water bodies were identified within a 500-foot radius of the site. The site is located within the designated wellhead protection area for the Town of Ahoskie. ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: April 29, 2022 Everette’s Enterprises Project Manager: William Regenthal GRI Project No. 2459 2 Municipal water is available to the site and surrounding properties. Adjacent property owner information is presented in Table 3. A Site Vicinity Map showing the locations of adjacent properties has been included as Figure 2. A Site Map showing the locations of the monitoring wells and the structures on-site has been included as Figure 3. A CAP proposing removal of free product using a pump and treat system followed by natural attenuation was completed for the site in August 1996. Initially, the CAP was not approved when it was submitted in 1996, since the site was ranked low risk. The site was re-ranked intermediate risk in September 1998 and a CAP Addendum was completed in 2001. To date, the CAP has not been implemented. 2.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL ASSESSMENT INFORMATION On March 23, 2022, five Type II monitoring wells (MW-1, MW-2, MW-3, MW-13 and MW-15) were gauged, purged and sampled. Free product was not observed during the sampling event. Depths to ground water in the Type II monitoring wells ranged from 4.93 feet to 7.39 feet below the tops of well casings. Ground water elevations relative to a temporary benchmark of 100.00 feet ranged from 91.36 to 94.72 feet. Ground water flow was generally toward the northwest with a horizontal gradient of approximately 0.02 feet per foot. Well construction and gauging information is presented in Table 4. A Water Table Surface Map is included as Figure 4. A summary of the current ground water gauging data is shown below: Well ID Screened Interval (x to y ft. BGS) Bottom of Well (ft. BGS) Top of Casing Elevation (ft.) Depth to Water from Top of Casing (feet) Free Product Thickness (ft.) Ground Water Elevation (ft.) MW-1 6 - 16 16 100.00 5.28 --- 94.72 MW-2 6 - 16 16 99.63 4.93 --- 94.70 MW-3 6 - 16 16 99.54 4.94 --- 94.60 MW-13 6 - 16 16 98.86 7.50 --- 91.36 MW-15 6 - 16 16 99.31 7.39 --- 91.92 Ground water samples collected from the monitoring wells were submitted for laboratory analyses using EPA Method 6200B. Concentrations of individual BTEX constituents, MTBE, naphthalene, EDB, 1,2- dichloroethane 1,1,2,2-tetrachloroethane, isopropylbenzene, n-propylbenzene, 1,2,4-trimethylbenzene and/or 1,3,5-trimethylbenzene that exceeded the MACs were reported in ground water samples collected from MW-1, MW-2, MW-3 and MW-13. All reported contaminant concentrations were less than the GCLs. A summary of the analytical results for ground water samples collected on March 23, 2022, is presented in Table 5. A Ground Water Quality Map based on the March 2022 data is included as Figure 5. A complete report of laboratory analyses of the ground water samples collected from the monitoring wells during the March 2022 sampling event has been included as Appendix B. A summary of the current ground water analytical data is shown below: ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: April 29, 2022 Everette’s Enterprises Project Manager: William Regenthal GRI Project No. 2459 3 Contaminant of Concern  Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene Well ID MACs (mg/l) 1 600 600 500 20 6 GCL (mg/l) 5,000 260,000 80,000 50,000 20,000 6,000 MW-1 1,180 4,580 577 3,800 121 219 MW-2 3,460 10,100 1,180 6,260 1,610 244 MW-3 1,480 14,100 2,430 11,600 222 J 392 MW-13 11.8 1.4 0.58 J 3.8 68 5.9 MWD-15 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 The baseline contaminant mass at the site was determined based on the total BTEX, MTBE and naphthalene concentrations from the March 2011 ground water sampling event, as well as the maximum historical water column height observed in each area. The contaminant plume consists of one area of concern (Area 1) based on the benzene concentrations during the March 2011 ground water sampling event. The contaminant mass has decreased by 28.4% since March 2011. Contaminant mass calculations have been included as Appendix C. A map of the contaminant mass area has been included as Figure 6. A chart depicting the overall trend in contaminant mass is shown below: The site is located in the Coastal Plain Physiographic Province of North Carolina. The water table has a seasonal high depth to water of approximately 0.5 to 5 feet bgs. ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: April 29, 2022 Everette’s Enterprises Project Manager: William Regenthal GRI Project No. 2459 4 3.0 AGGRESSIVE FLUID-VAPOR RECOVERY EVENT An AFVR event was conducted at the site by GAS under the supervision of GRI on February 23, 2022. Monitoring wells MW-2 and MWD-24 were used as the extraction well during the March 2022 AFVR event. Please note, prior to the start of the AFVR event, MW-3 was not located, and MWD-24 was connected as an extraction well in error. Prior to the start of the AFVR event, ground water samples were collected from MW-2 and MWD-24. Concentrations of individual BTEX constituents, MTBE and naphthalene that exceeded the MACs were reported in the ground water sample collected from MW-2 prior to the start of the AFVR event. The concentration of benzene reported in the ground water sample collected prior to the start of the AFVR event exceeded the GCL. The AFVR equipment included a liquid ring pump, a 3,200-gallon capacity tanker, flexible vacuum hoses, 6-inch diameter discharge stack, 1.5-inch diameter PVC stinger pipes and associated couplings and pipe fittings to the wells. The AFVR system was rated at 680 cfm at 18 in. Hg. All extraction and observation wells were gauged prior to the start of the event. No free product was observed in MW-2 or MWD-24 prior to the start of the AFVR event. The initial stinger pipe depth was 6 feet in MW-2 and 16 feet in MWD-24. The AFVR event ran for 7.5 hours until the vacuum truck was deemed full and the event was shut down. Monitoring wells MW-2 and MWD-24 were vacuumed continuously for the 7.5 hour event. During the event, measurements of relative humidity, temperature, vacuum, exhaust velocity and off-gas concentrations were recorded at the discharge stack every 15 minutes for the first two hours and every 30 minutes thereafter. System vacuum measured constant at 27.0 in Hg. during the test. The effluent velocity ranged from 128.3 to 504.5 feet per minute. The system temperature ranged from 97.7 to 124.9°F and relative humidity ranged from 24.7 to 56.7 percent. The VOC off-gas concentrations ranged from 0.1 ppm to 12.7 ppm during the event. A total of 2,576 gallons of affected ground water was recovered during the AFVR event. At the conclusion of the event, no free product was measured in any of the wells associated with the AFVR event. A summary of the gauging data obtained before starting and at the conclusion of the AFVR event is presented in Table 4. A summary of the ground water sampling results collected prior to the start of the AFVR event is presented in Table 5. A complete laboratory report for ground water samples collected during the AFVR event is included in Appendix B. A copy of the AFVR report and calculations has been included as Appendix D. A summary of the gauging data for the February 2022 AFVR event has been listed below: Well ID Product Thickness before Recovery (feet) Product Thickness after Recovery (feet) Amount of Liquid Recovered (gallons) Amount of Product Recovered as Liquid (gallons) MW-2 0.00 0.00 2,576 0.00 MWD-24 0.00 0.00 The results of the AFVR event indicate that a total of 2,576 gallons of liquids were removed during the event. Of the total liquids extracted, no measurable free product was removed during the event. Based ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: April 29, 2022 Everette’s Enterprises Project Manager: William Regenthal GRI Project No. 2459 5 on 7.5 hours of operation, the average liquid recovery rate was 343.33 gallons per hour. An additional 0.03 gallons of vapor phase hydrocarbons were removed at an average rate of less than 0.01 gallons per hour. A summary of free product recovery data has been included as Table 6. Summaries of AFVR event information and cost analysis are provided in Tables 7 and 8, respectively. At the conclusion of the AFVR event, all wastewater was transported to a permitted facility for disposal. A copy of the disposal manifest is included in Appendix D. A summary of the free product recovery data from the October 2021 event is listed below: Well ID Average Effluent Velocity (ft/min) Average Effluent Temperature (°F) Average Effluent Concentration (ppm) Amount of Vaporized Product (gallons) Amount of Liquid Recovered (gallons) Amount of Product Recovered as Liquid (gallons) Total Amount of Product Recovered (gallons) MW-2 & MWD-24 290.00 107.10 7.50 0.03 2,576 0.00 0.03 Totals to Date 0.03 2,576 0.00 0.03 4.0 CONCLUSIONS  On March 23, 2022, five Type II monitoring wells were gauged, purged and sampled. Free product was not observed. Ground water flow was generally to the northwest with a horizontal gradient of approximately 0.02 feet per foot.  Concentrations of individual BTEX constituents, MTBE, naphthalene, EDB, 1,2-dichloroethane 1,1,2,2- tetrachloroethane, isopropylbenzene, n-propylbenzene, 1,2,4-trimethylbenzene and/or 1,3,5- trimethylbenzene that exceeded the MACs were reported in ground water samples collected from MW-1, MW-2, MW-3 and MW-13. None of the reported contaminant concentrations exceeded the GCLs.  Contaminant mass has decreased by 28.4% at the site since March 2011.  On February 23, 2022, an AFVR event was conducted on MW-2 and MWD-24. Please note, prior to the start of the AFVR event, MW-3 was not located, and MWD-24 was connected as an extraction well in error.  Concentrations of individual BTEX constituents, MTBE and naphthalene that exceeded the MACs were reported in the ground water sample collected from MW-2 prior to the start of the AFVR event. The concentration of benzene reported in the ground water sample collected prior to the start of the AFVR event exceeded the GCL.  A total of 2,576 gallons of affected ground water were recovered during the AFVR event. At the conclusion of the event, no free product was measured in any of the wells associated with the AFVR event. The average liquid recovery rate was 343.33 gallons per hour. An additional 0.03 gallons of vapor phase hydrocarbons were removed at an average rate of less than 0.01 gallons per hour.  The AFVR event was shut down after 7.5 hours of operation when the vacuum truck was deemed full.  Based on this information, the AFVR event was effective in reducing the contaminant concentrations to less than GCLs. Ground water monitoring should continue at the site, to confirm the results of the March 2022 sampling event. The next ground water sampling event is tentatively scheduled for ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: April 29, 2022 Everette’s Enterprises Project Manager: William Regenthal GRI Project No. 2459 6 September 2022. If the contaminant concentrations remain less than the GCLs, an NRP should be filed, and the site closed with an NFA. 5.0 LIMITATIONS This report has been prepared for the exclusive use of North East Oil Company, Inc. for specific application to the referenced site in Hertford County, North Carolina. The assessment was conducted based on the scope of work and level of effort desired by NCDEQ and with resources adequate only for that scope of work. Our findings have been developed in accordance with generally accepted standards of environmental practices in the State of North Carolina, available information, and our professional judgment. No other warranty is expressed or implied. The data that are presented in this report are indicative of conditions that existed at the precise locations sampled and at the time the samples were collected. In addition, the data obtained from samples would be interpreted as being meaningful with respect to parameters indicated in the laboratory report. No additional information can logically be inferred from these data. 6.0 STATEMENTS AND CERTIFICATION 1 Enter the date the monitoring report was due. n/a Will this report be submitted after the established due date? YES NO 2 Was any required information from the above template missing from this report? YES NO IF the answer to question #1 or# 2 is “YES”, please provide additional information in this cell to explain what was missing and why. 3 If applicable, will any of the proposed attenuation milestones under the schedule approved in the Corrective Action Plan not be met? (within a reasonable margin of error) YES NO IF the answer to question #3 is “NO”, skip to the certification under #8 below. IF the answer to question #3 is “YES”, please generally describe in this cell the possible reason(s) and outline proposed remedies. (This should be described in more detail in the report text above.) N/A 4 Does any known or suspected source zone soil contamination or free product remain outside of the assessed area that could be inhibiting natural attenuation? YES NO 5 Has there been an unexpected increase in contaminant mass sufficient to suggest a potential new release from a separate onsite or offsite source? YES NO IF the answer to either question #4 or #5 is “YES”, generally describe in this cell any actions recommended to further assess or clean up this known or suspected source. (This should be described in more detail in the report text above.) FIGURES SITE5993-70-2836 599 3-70-47625993-70-4927 5993-70-48285993-70-4980 D R . M A R T IN L U T H E R K IN G JR . D R IV ECATHERINE STREETMAPLE STREETTROY STREET MALIBU DRIVE MONOCO DRIVE DAVIS STREET PINE STREETSTATON AVENUE BAKER STREET G E R O CK STR E ET WILLIA M S STR EET M A N L EY AV E N U E TOWN OF AHOSKIE N E W S O M E S T R E E TPORTER S TR EETPATTERSON AVENUE H A RT S T R E E T CATHERINE CREEK ROADT RO Y S T R E E T TOWN OF AHOSKIESNIPES AVENUE H O LLO M A N AVENUE RHUE STREETHILL STREETALTON STREET ALTON STREET ROGERS STREET RICHARD STREET LASHLEY AVENUEFIGURE 2: SITE VICINITY MAPEVERETTE'S ENTERPRISES1101 N. CATHERINE CREEK ROADAHOSKIE, HERTFORD COUNTYNORTH CAROLINAINCIDENT NO. 11174GRI PROJECT NO. 2459 PREPARED BY:GEOLOGICAL RESOURCES, INC.JANUARY 22, 2021 ³ 0 300150Feet1 inch = 300 feet 1,500-FOOT RADIUS 500-FOOT RADIUS 1,000-FOOT RADIUS 250-FOOT RADIUS LEGEND Centerlines Hydrology Adjacent Properties nc_hertford_parcels_poly TABLES UST ID Number 1-3 Facility ID Number Owner or Operator? OwnerET One, Inc.05/07/1964 - 09/09/1993 Address Telephone Number Post Office Box 1386, Ahoskie, NC 27910 252-862-0236 Name of Owner or Operator Dates of Ownership / Operation TABLE 1 UST OWNER/OPERATOR INFORMATION EVERETTE'S ENTERPRISES (INCIDENT NO. 11174) 00-0-0000009694 Page 1 of 1 Date: 02/02/2021 Was Release Associated with UST System? (Yes / No) 1 Gasoline Gasoline 1,000 05/07/1964 Single Wall Steel Unknown Unknown Removed (09/09/93)Yes 2 Gasoline Gasoline 1,000 05/07/1964 Single Wall Steel Unknown Unknown Removed (09/09/93)Yes 3 Gasoline Gasoline 1,000 05/07/1964 Single Wall Steel Unknown Unknown Removed (09/09/93)Yes Tank Dimensions Description of Associated Product Piping and Pumps Status of UST TABLE 2 UST SYSTEM INFORMATION EVERETTE'S ENTERPRISES (INCIDENT NO. 11174) Facility ID #: 00-0-0000009694 UST ID No. Current or Most Recent Contents Previous Contents Capacity (gallons) Date Installed Construction Details Page 1 of 1 Date: 01/27/2021 Facility ID #: 00-0-0000009694 5993-70-4828 (site)Clyde W. Everett 414 Troy Street E Ahoskie, North Carolina 27910 5993-70-2836 C W Jones Heirs Post Office Box 368 Ahoskie, North Carolina 27910 5993-70-4927 County of Hertford 115 Justice Drive, Suite #1 Winton, North Carolina 27986 5993-70-4762 Keely P. Holley 1490 Hartford Terrace Alpharetta, Georgia 30004 5993-70-4980 Travis Harrell 106 Blacksmith Drive Ahoskie, North Carolina 27910 • Properties are keyed to Figure 3. • This information is based on the Hertford County GIS website. TABLE 3 ADJACENT PROPERTY OWNER INFORMATION EVERETTE'S ENTERPRISES (INCIDENT NO. 11174) PIN Number Property Owner Name Mailing Address Date: 04/22/22 Facility ID # : 00-0-0000009694 03/07/11 5.56 44.37 09/26/11 4.68 45.25 11/01/12 4.27 95.73 09/18/13 NM NM 04/03/14 5.12 94.88 01/06/15 5.20 94.80 01/12/21 4.92 95.08 03/23/22 5.28 94.72 03/07/11 5.26 42.91 09/26/11 4.37 43.80 11/01/12 3.96 95.67 09/18/13 7.62 92.01 04/03/14 4.95 94.68 01/06/15 4.78 94.85 01/12/21 5.11 94.52 02/23/22 5.09 94.54 Before AFVR 02/23/22 5.35 94.28 After AFVR 03/23/22 4.93 94.70 03/07/11 5.21 42.90 09/26/11 4.45 43.66 11/01/12 3.97 95.57 09/18/13 7.71 91.83 04/03/14 4.66 94.88 01/06/15 4.78 94.76 01/12/21 4.82 94.72 03/23/22 4.94 94.60 03/07/11 2.04 45.70 09/26/11 0.79 46.95 11/01/12 0.57 98.63 09/18/13 8.67 90.53 04/03/14 3.84 95.36 01/06/15 3.50 95.70 01/12/21 0.99 98.21 03/07/11 14.79 33.53 09/26/11 15.67 32.65 11/01/12 14.93 84.87 09/18/13 15.71 84.09 04/03/14 NM NM Not found 01/06/15 NM NM Under cement pad 03/07/11 4.45 43.57 09/26/11 2.45 45.57 11/01/12 0.80 98.64 09/18/13 NM NM 04/03/14 NM NM 01/06/15 0.82 98.62 03/07/11 5.69 43.12 09/26/11 4.65 44.16 11/01/12 4.26 95.94 09/18/13 8.21 91.99 04/03/14 5.06 95.14 01/06/15 5.15 95.05 01/12/21 4.90 95.30 03/07/11 5.11 43.04 09/26/11 4.24 43.91 11/01/12 3.52 96.07 09/18/13 7.52 92.07 04/03/14 4.77 94.82 01/06/15 4.67 94.92 01/12/21 4.59 95.00 03/07/11 15.47 32.72 09/26/11 16.40 31.79 11/01/12 15.75 83.90 09/18/13 16.60 83.05 04/03/14 14.74 84.91 01/06/15 NM NM Under cement pad 03/07/11 5.33 43.14 09/26/11 4.83 43.64 11/01/12 4.07 95.84 09/18/13 7.88 92.03 04/03/14 NM NM 01/06/15 4.97 94.94 01/12/21 4.89 95.02 MW-2 0.00 0.00 166-16611/04/93MW-3 99.54 0.00 11/04/93 49.93 48.17 166-16611/04/93 99.63 166-166 MW-1 100.00 0.00 0.00 0.00 0.00 6-16605/31/95 0.00 0.00 0.00 48.32 99.80 99.65 48.81 48.02 48.47 48.15 100.20 MW-4 404/20/94 3530-353004/21/94MWD-5 MW-8 Comments TABLE 4 WELL CONSTRUCTION AND GAUGING INFORMATION EVERETTE'S ENTERPRISES (INCIDENT NO. 11174) Well ID Date Installed (mm/dd/yy) Date Water Level Measured (mm/dd/yy) Screened Interval (x to y ft. BGS) Top of Casing Elevation* (ft.) Depth to Water from Top of Casing (ft.) Free Product Thickness (ft.) Groundwater Elevation (ft.) Well Casing Depth (ft. BGS) Bottom of Well (ft. BGS) 4 4-14 14 14 99.20 4-14 48.11 47.74 MW-10 06/02/95 6 6-16 16 99.91 99.44 14404/22/94MW-6 4-14 4540-454006/01/95MWD-9 48.19 99.59 16 MW-7 04/22/94 Page 1 of 3 Date: 04/22/22 Facility ID # : 00-0-0000009694 Comments TABLE 4 WELL CONSTRUCTION AND GAUGING INFORMATION EVERETTE'S ENTERPRISES (INCIDENT NO. 11174) Well ID Date Installed (mm/dd/yy) Date Water Level Measured (mm/dd/yy) Screened Interval (x to y ft. BGS) Top of Casing Elevation* (ft.) Depth to Water from Top of Casing (ft.) Free Product Thickness (ft.) Groundwater Elevation (ft.) Well Casing Depth (ft. BGS) Bottom of Well (ft. BGS) 03/07/11 4.78 42.87 09/26/11 5.85 41.80 11/01/12 3.93 95.18 09/18/13 7.24 91.87 04/03/14 4.24 94.87 01/06/15 4.78 94.33 01/12/21 5.12 93.99 03/07/11 8.25 39.25 09/26/11 8.80 38.70 11/01/12 6.06 92.92 09/18/13 10.10 88.88 04/03/14 6.05 92.93 01/06/15 7.41 91.57 01/12/21 5.23 93.75 09/26/11 47.39 9.55 37.84 10/29/12 7.78 91.08 09/18/13 11.85 87.01 04/03/14 6.96 91.90 01/06/15 7.41 91.45 01/12/21 6.62 92.24 03/23/22 7.50 91.36 03/07/11 8.51 39.23 09/26/11 8.95 38.79 11/01/12 6.17 93.03 09/18/13 9.66 89.54 04/03/14 5.81 93.39 01/06/15 7.48 91.72 03/07/11 8.13 39.72 09/26/11 8.37 39.48 11/01/12 5.89 93.42 09/18/13 NM NM 04/03/14 NM NM 01/06/15 7.64 91.67 03/23/22 7.39 91.92 03/07/11 7.75 39.42 09/26/11 0.76 46.41 11/01/12 0.58 98.14 09/18/13 9.56 89.16 04/03/14 NM NM 01/06/15 0.83 97.89 09/26/11 47.63 3.60 44.03 11/01/12 4.14 94.96 09/18/13 7.57 91.53 04/03/14 3.55 95.55 01/06/15 3.24 95.86 03/07/11 8.79 38.61 09/26/11 4.72 42.68 11/01/12 3.02 95.87 09/18/13 NM NM 04/03/14 NM NM 01/06/15 5.04 93.85 03/07/11 10.43 38.01 09/26/11 10.95 37.49 11/01/12 9.26 90.69 09/18/13 NM NM 04/03/14 NM NM Not found 01/06/15 9.42 90.53 11/01/12 6.01 93.15 09/18/13 10.31 88.85 04/03/14 5.88 93.28 01/06/15 7.33 91.83 11/01/12 6.71 92.41 09/18/13 10.03 89.09 04/03/14 NM NM 01/06/15 7.41 91.71 11/01/12 6.65 92.60 09/18/13 9.97 89.28 04/03/14 6.05 93.20 01/06/15 7.43 91.82 0.00 99.31 166-16606/07/95MW-15 6-16606/05/95 0.00 0.00MW-12 06/05/95 6 6-16 16 98.8616MW-13 0.00 0.00 0.00 99.25 99.12 99.20 47.65 98.98 0.00 0.00 0.00 99.11 0.00 MW-21 165.5-165.510/15/12MW-23 15 166-166MW-14 3-13 06/05/95 166-16 MW-17 99.95 155-15509/13/95MW-20 98.89 133-13309/13/95MW-18 99.10133-13 47.40 MW-11 6 MW-16 48.44 99.16165.5-165.5 47.50 47.74 47.85 06/05/95 47.17 98.72 13309/13/95 309/13/95 10/15/12 10/15/12MW-22 5.5-155.5 0.00 0.00 Page 2 of 3 Date: 04/22/22 Facility ID # : 00-0-0000009694 Comments TABLE 4 WELL CONSTRUCTION AND GAUGING INFORMATION EVERETTE'S ENTERPRISES (INCIDENT NO. 11174) Well ID Date Installed (mm/dd/yy) Date Water Level Measured (mm/dd/yy) Screened Interval (x to y ft. BGS) Top of Casing Elevation* (ft.) Depth to Water from Top of Casing (ft.) Free Product Thickness (ft.) Groundwater Elevation (ft.) Well Casing Depth (ft. BGS) Bottom of Well (ft. BGS) 09/18/13 16.86 83.05 04/03/14 15.01 84.90 01/06/15 16.15 83.76 01/12/21 14.12 85.79 02/23/22 15.07 84.84 Before AFVR 02/23/22 15.07 84.84 After AFVR 09/18/13 16.84 82.23 04/03/14 14.02 85.05 01/06/15 15.10 83.97 01/12/21 13.15 85.92 Notes: • * : Reference point for elevation measurements; assumed elevation 100.00 ft. • ft BGS : feet below ground surface. • NM: Not measured. • Top of Casing information obtained from January 19, 2012, survey completed by Roanoke Land Surveying and reproduced from reports prepared by CES Engineering, PC. MWD-25 08/21/13 45 45-50 50 99.07 0.00 0.0099.915045-504508/21/13MWD-24 Page 3 of 3 Date: 04/21/2022 Facility ID #: 00-0-0000009694 EPA Method 6010B/3030C 1 600 600 500 20 6 70 70 70 400 400 15 400 700 10,000 200 5,000 260,000 80,000 50,000 20,000 6,000 5,900 30,500 26,100 28,500 24,100 15,000 NE NE NE NE 03/02/11 1,630 6,890 1,160 6,950 224 401 124 J 109 J 275 2,220 583 NR NR NR NR NR 09/26/11 2,170 11,600 1,490 9,390 115 J 698 35.2 J 102 J 241 2,380 599 NR NR NR NR NR 11/01/12 1,340 10,600 1,350 8,580 42.5 J 514 25.4 J 57.3 J 171 1,990 457 NR NR NR NR NR 09/18/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 04/03/14 1,350 9,140 1,700 9,690 60.9 J 435 28.7 J 100 J 300 2,370 660 NR NR NR NR NR 01/06/15 2,030 12,700 1,970 11,300 102 470 29.5 J 124 251 2,780 546 NR NR NR NR NR 01/12/21 937 7,010 1,100 7,120 <25 374 <25 60.0 J 140 1,950 578 NR NR NR NR NR 03/23/22 1,180 4,580 577 3,800 121 219 19.7 42.6 72.7 1,080 322 NR NR NR NR NR 03/02/11 3,340 7,650 1,050 4,960 1,580 249 67.4 J 70.9 J 171 J 1,050 286 NR NR NR NR NR 09/26/11 7,470 20,400 2,080 10,920 1,490 840 35.4 121 301 2,370 584 NR NR NR NR NR 11/01/12 5,630 21,900 1,790 10,100 938 513 <50 70.6 J 226 J 1,670 393 NR NR NR NR NR 09/18/13 4,290 12,600 1,060 5,970 1,480 296 <10 40.1 J 118 958 214 21.2 15,100 2,782 J <100 4,422 J 04/03/14 1,580 4,390 555 4,200 391 485 20.4 J 40.3 J 113 1,090 286 NR NR NR NR NR 01/06/15 5,760 13,000 1,270 9,820 1,790 472 17.2 J 70.5 145 2,180 424 NR NR NR NR NR 01/12/21 5,060 15,500 2,370 11,700 2,270 626 <63 110 J 270 2,390 685 NR NR NR NR NR 02/23/22 5,670 16,700 2,160 10,600 2,380 521 NR NR NR NR NR NR NR NR NR NR 03/23/22 3,460 10,100 1,180 6,260 1,610 244 <31 49.0 J 128 J 1260 357 NR NR NR NR NR 03/02/11 7,700 26,900 2,970 15,500 3,670 621 104 J 163 J 364 2,830 716 NR NR NR NR NR 09/26/11 13,400 24,900 2,920 15,520 18,100 1,150 82.5 231 599 3,530 1,160 NR NR NR NR NR 11/01/12 9,170 32,500 3,230 16,400 4,890 692 <100 162 J 483 J 2,660 731 NR NR NR NR NR 09/18/13 6,970 15,500 1,930 9,080 4,040 404 <50 68.3 J 264 1,510 392 17.9 26,200 9,270 J <420 8,800 04/03/14 1,580 4,860 648 4,330 725 349 <20 33.0 J 94.3 J 1,190 310 NR NR NR NR NR 01/06/15 5,510 14,700 1,900 9,660 2,510 371 <20 99.7 J 215 1,960 374 NR NR NR NR NR 01/12/21 3,900 23,600 3,290 15,600 <63 611 <63 137 J 346 2,540 692 NR NR NR NR NR 03/23/22 1,480 14,100 2,430 11,600 222 J 392 <63 94.3 J 262 2050 572 NR NR NR NR NR 03/02/11 <0.140 0.353 J <0.150 0.505 J <0.250 <0.500 <0.180 <0.150 <0.220 0.190 J <0.180 NR NR NR NR NR 09/26/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 11/01/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/18/13 <0.10 <0.10 <0.10 <0.22 6.0 <0.15 <0.10 0.11 J <0.10 <0.10 <0.10 326 <35 <165 <130 <225 04/03/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 01/06/15 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 01/12/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR MW-2 MW-3 MW-1 GCL (mg/l) MW-4 n-PropylbenzeneContaminant of Concern BenzeneToluene2L Standard (mg/l)Naphthalenen-ButylbenzeneIsopropylbenzeneWell ID Date Collected (mm/dd/yy) TABLE 5 SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS EVERETTE'S ENTERPRISES (INCIDENT NO. 11174) MADEP Methods VPH and EPH LeadC5-C8 AliphaticsC9-C18 AliphaticsC19-C36 AliphaticsC9-C22 AromaticsMTBEEthylbenzeneXylenesEPA Methods 6200B 1,2,4-TrimethylbenzeneAnalytical Method 1,3,5-TrimethylbenzenePage 1 of 6 Date: 04/21/2022 Facility ID #: 00-0-0000009694 EPA Method 6010B/3030C 1 600 600 500 20 6 70 70 70 400 400 15 400 700 10,000 200 5,000 260,000 80,000 50,000 20,000 6,000 5,900 30,500 26,100 28,500 24,100 15,000 NE NE NE NEGCL (mg/l)n-PropylbenzeneContaminant of Concern BenzeneToluene2L Standard (mg/l)Naphthalenen-ButylbenzeneIsopropylbenzeneWell ID Date Collected (mm/dd/yy) TABLE 5 SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS EVERETTE'S ENTERPRISES (INCIDENT NO. 11174) MADEP Methods VPH and EPH LeadC5-C8 AliphaticsC9-C18 AliphaticsC19-C36 AliphaticsC9-C22 AromaticsMTBEEthylbenzeneXylenesEPA Methods 6200B 1,2,4-TrimethylbenzeneAnalytical Method 1,3,5-Trimethylbenzene03/02/11 <0.140 0.631 J <0.150 0.760 J 51.1 <0.500 <0.180 <0.150 <0.220 0.249 J <0.180 NR NR NR NR NR 09/26/11 <0.13 <0.13 <0.15 <0.30 28.1 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 11/01/12 <0.10 <0.10 <0.10 <0.22 33.3 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/18/13 <0.10 <0.10 <0.10 <0.22 38.2 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 21.6 <35 <145 <110 <195 04/03/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 01/06/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 03/02/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.150 <0.220 <0.150 <0.180 NR NR NR NR NR 09/26/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 11/01/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/18/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 04/03/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 01/06/15 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 03/02/11 <0.700 1.11 J <0.750 <1.10 <1.25 <2.50 <0.900 <0.750 <1.10 <0.750 <0.900 NR NR NR NR NR 09/26/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 11/01/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/18/13 <0.10 0.41 J <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 55.5 <35 <145 <110 <205 04/03/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 01/06/15 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 01/12/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR 03/02/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.150 <0.220 <0.150 <0.180 NR NR NR NR NR 09/26/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 11/01/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/18/13 <0.10 <0.10 <0.10 <0.22 0.55 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 6.3 <35 <145 <110 <205 04/03/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 01/06/15 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 01/12/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR 03/02/11 10.8 2.98 2.54 2.87 167 0.690 J <0.180 0.215 J 0.415 J 1.58 0.329 J NR NR NR NR NR 09/26/11 8.1 0.63 1.4 0.45 J 35.8 0.53 <0.10 <0.10 0.16 J <0.10 <0.10 NR NR NR NR NR 11/01/12 0.46 J 0.25 J <0.10 <0.22 194 0.17 J <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/18/13 11.1 <0.10 0.40 J 0.25 J 40.4 0.58 <0.10 <0.10 0.28 J 0.37 J <0.10 <5.0 <35 <145 <110 <195 04/03/14 <0.10 <0.10 <0.10 <0.20 2.4 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 01/06/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS MW-6 MWD-5 MW-7 MWD-9 MW-8 Page 2 of 6 Date: 04/21/2022 Facility ID #: 00-0-0000009694 EPA Method 6010B/3030C 1 600 600 500 20 6 70 70 70 400 400 15 400 700 10,000 200 5,000 260,000 80,000 50,000 20,000 6,000 5,900 30,500 26,100 28,500 24,100 15,000 NE NE NE NEGCL (mg/l)n-PropylbenzeneContaminant of Concern BenzeneToluene2L Standard (mg/l)Naphthalenen-ButylbenzeneIsopropylbenzeneWell ID Date Collected (mm/dd/yy) TABLE 5 SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS EVERETTE'S ENTERPRISES (INCIDENT NO. 11174) MADEP Methods VPH and EPH LeadC5-C8 AliphaticsC9-C18 AliphaticsC19-C36 AliphaticsC9-C22 AromaticsMTBEEthylbenzeneXylenesEPA Methods 6200B 1,2,4-TrimethylbenzeneAnalytical Method 1,3,5-Trimethylbenzene03/02/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.150 <0.220 <0.150 <0.180 NR NR NR NR NR 09/26/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 11/01/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/18/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 102 <35 <135 <100 <185 04/03/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 01/06/15 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 01/12/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR 03/02/11 738 27.3 125 61.7 390 39.1 <1.80 11.0 16.6 31.0 2.26 J NR NR NR NR NR 09/26/11 247 38.6 46.0 43.0 105 25.9 0.77 4.5 7.5 12.9 1.5 NR NR NR NR NR 11/01/12 0.87 <0.10 <0.10 <0.22 35.6 0.35 J <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/18/13 60.0 0.14 J 2.4 <0.22 138 4.3 <0.10 0.36 J 0.27 J <0.10 <0.10 8.0 74.5 J <135 <100 <185 04/03/14 <0.10 <0.10 <0.10 <0.20 92.1 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 01/06/15 0.50 <0.10 <0.10 <0.20 35.0 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 01/12/21 <0.13 <0.13 <0.13 <0.25 14.2 0.23 J <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR 03/02/11 156 <1.90 <1.50 <2.20 1,300 <5.00 <1.80 <1.50 <2.20 <1.50 <1.80 NR NR NR NR NR 09/26/11 63.8 0.69 7.9 0.99 J 327 4.3 0.21 J 2.3 1.5 0.30 J <0.10 NR NR NR NR NR 11/01/12 <2.0 <2.0 <2.0 <4.3 519 <3.0 <2.0 <2.0 <2.0 <2.0 <2.0 NR NR NR NR NR 09/18/13 <2.0 <2.0 <2.0 <4.3 476 <3.0 <2.0 <2.0 <2.0 <2.0 <2.0 147 <35 <135 <100 <185 04/03/14 34.8 <0.10 <0.10 <0.20 628 <0.10 <0.10 1.5 <0.10 <0.10 <0.10 NR NR NR NR NR 01/06/15 <0.10 <0.10 <0.10 <0.20 114 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 01/12/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR 09/26/11 701 20.9 68.0 106.3 818 28.5 1.7 11.4 12.4 42.5 1.9 NR NR NR NR NR 11/01/12 172 0.19 J 3.6 0.49 J 420 2.9 0.13 J 1.0 0.56 <0.10 <0.10 NR NR NR NR NR 09/18/13 1,310 30.0 344 553 1,040 91.7 <1.0 18.3 47.6 229 35.9 127 2,470 481 <110 775 04/03/14 14.8 <0.10 <0.10 1.2 J 225 1.6 <0.10 0.40 J <0.10 <0.10 <0.10 NR NR NR NR NR 01/06/15 3.7 <0.10 <0.10 <0.20 175 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 01/12/21 104 <0.31 4.2 10.7 106 17.5 1.2 J 6.0 9.3 4.5 <0.31 NR NR NR NR NR 03/23/22 11.8 1.4 0.58 J 3.8 68 5.9 0.61 J 2.5 4.3 3.4 0.42 J NR NR NR NR NR 03/02/11 <0.140 <0.190 <0.150 <0.220 0.411 J <0.500 <0.180 <0.150 <0.220 <0.150 <0.180 NR NR NR NR NR 09/26/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 11/01/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/18/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <5.0 <35 <145 <110 <195 04/03/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 01/06/15 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR MW-13 MW-11 MW-12 MW-14 MW-10 Page 3 of 6 Date: 04/21/2022 Facility ID #: 00-0-0000009694 EPA Method 6010B/3030C 1 600 600 500 20 6 70 70 70 400 400 15 400 700 10,000 200 5,000 260,000 80,000 50,000 20,000 6,000 5,900 30,500 26,100 28,500 24,100 15,000 NE NE NE NEGCL (mg/l)n-PropylbenzeneContaminant of Concern BenzeneToluene2L Standard (mg/l)Naphthalenen-ButylbenzeneIsopropylbenzeneWell ID Date Collected (mm/dd/yy) TABLE 5 SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS EVERETTE'S ENTERPRISES (INCIDENT NO. 11174) MADEP Methods VPH and EPH LeadC5-C8 AliphaticsC9-C18 AliphaticsC19-C36 AliphaticsC9-C22 AromaticsMTBEEthylbenzeneXylenesEPA Methods 6200B 1,2,4-TrimethylbenzeneAnalytical Method 1,3,5-Trimethylbenzene03/02/11 <0.140 3.44 0.660 J <0.220 <0.250 <0.500 <0.180 <0.150 <0.220 <0.150 <0.180 NR NR NR NR NR 09/26/11 <0.13 <0.13 3.4 <0.30 <0.13 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 11/01/12 <0.10 <0.10 0.32 J <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/18/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 04/03/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 01/06/15 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 03/23/22 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR 03/02/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.150 <0.220 <0.150 <0.180 NR NR NR NR NR 09/26/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 11/01/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/18/13 <0.10 0.16 J <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 63.0 <35 <145 <110 <205 04/03/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 01/06/15 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/26/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 11/01/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/18/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 311 <35 <145 <110 <195 04/03/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 01/06/15 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 03/02/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.150 <0.220 <0.150 <0.180 NR NR NR NR NR 09/26/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 11/01/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/18/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 04/03/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 01/06/15 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 03/02/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.150 <0.220 <0.150 <0.180 NR NR NR NR NR 09/26/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 11/01/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/18/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 04/03/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 01/06/15 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 11/01/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/18/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 56.5 <35 <145 <110 <195 04/03/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 01/06/15 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR MW-15 MW-20 MW-21 MW-17 MW-18 MW-16 Page 4 of 6 Date: 04/21/2022 Facility ID #: 00-0-0000009694 EPA Method 6010B/3030C 1 600 600 500 20 6 70 70 70 400 400 15 400 700 10,000 200 5,000 260,000 80,000 50,000 20,000 6,000 5,900 30,500 26,100 28,500 24,100 15,000 NE NE NE NEGCL (mg/l)n-PropylbenzeneContaminant of Concern BenzeneToluene2L Standard (mg/l)Naphthalenen-ButylbenzeneIsopropylbenzeneWell ID Date Collected (mm/dd/yy) TABLE 5 SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS EVERETTE'S ENTERPRISES (INCIDENT NO. 11174) MADEP Methods VPH and EPH LeadC5-C8 AliphaticsC9-C18 AliphaticsC19-C36 AliphaticsC9-C22 AromaticsMTBEEthylbenzeneXylenesEPA Methods 6200B 1,2,4-TrimethylbenzeneAnalytical Method 1,3,5-Trimethylbenzene11/01/12 <0.10 <0.10 <0.10 <0.22 17.9 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/18/13 <0.10 <0.10 <0.10 <0.22 53.2 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 9.3 <35 <165 <130 <225 04/03/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 01/06/15 <0.10 <0.10 <0.10 <0.20 5.7 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 11/01/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/18/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 17.2 <35 <135 <100 <185 04/03/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 01/06/15 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/18/13 1.6 <0.25 <0.25 <0.54 104 <0.37 <0.25 <0.25 <0.25 <0.25 <0.25 <5.0 <35 <145 <110 <195 04/03/14 <0.10 <0.10 <0.10 <0.20 170 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 01/06/15 0.39 J 1.3 0.19 J 0.82 J 114 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 01/12/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR 02/23/22 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 NR NR NR NR NR NR NR NR NR NR 09/18/13 0.20 J <0.10 <0.10 <0.22 28.4 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <5.0 <35 <145 <110 <195 04/03/14 <0.10 <0.10 <0.10 <0.20 229 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 01/06/15 <0.50 <0.50 <0.50 <1.0 243 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NR NR NR NR NR 01/12/21 <0.31 <0.31 <0.31 <0.63 107 <0.31 <0.31 <0.31 <0.31 <0.31 <0.31 NR NR NR NR NR Site Sink 03/02/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.150 <0.220 <0.150 <0.180 NR NR NR NR NR Vaughn Spigot 03/02/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.150 <0.220 <0.150 <0.180 NR NR NR NR NR Church Sink 03/02/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.150 <0.220 <0.150 <0.180 NR NR NR NR NR House 1 11/01/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR House 2 11/01/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR House 3 11/01/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR House 4 11/01/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR House 5 11/01/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 11/01/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 04/03/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 11/01/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 04/03/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR MW-23 MW-22 MWD-24 MWD-25 House 8 House 9 Page 5 of 6 Date: 04/21/2022 Facility ID #: 00-0-0000009694 EPA Method 6010B/3030C 1 600 600 500 20 6 70 70 70 400 400 15 400 700 10,000 200 5,000 260,000 80,000 50,000 20,000 6,000 5,900 30,500 26,100 28,500 24,100 15,000 NE NE NE NEGCL (mg/l)n-PropylbenzeneContaminant of Concern BenzeneToluene2L Standard (mg/l)Naphthalenen-ButylbenzeneIsopropylbenzeneWell ID Date Collected (mm/dd/yy) TABLE 5 SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS EVERETTE'S ENTERPRISES (INCIDENT NO. 11174) MADEP Methods VPH and EPH LeadC5-C8 AliphaticsC9-C18 AliphaticsC19-C36 AliphaticsC9-C22 AromaticsMTBEEthylbenzeneXylenesEPA Methods 6200B 1,2,4-TrimethylbenzeneAnalytical Method 1,3,5-TrimethylbenzeneTrip Blank 03/23/22 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR Notes: • Results reported in µg/l (micrograms per liter). • < : Less than the method detection limit specified in the laboratory report. • 2L Standard specified in T15A NCAC 2L.0202. • GCL: Gross contamination level. • NE: Not established. • NR: Not requested. • Concentrations in bold face type exceeded the 2L Standards. • Concentrations in bold face type and italics exceeded the GCLs. • J: Estimated concentration. • Please refer to the lab report for detectable concentrations which did not exceed the 2L Standards. • Concentrations of EDB, 1,2-dichloroethane and 1,1,2,2-tetrachloroethane, that exceeded the 2L Standard was reported in MW-1 and MW-2 during the March 2022 sampling event. Page 6 of 6 Date: 4/22/22 Method of Measurement: Well ID Product Type (gas, diesel, etc.) Date of Recovery (mm/dd/yy) Free Product Recovery Method* Casing Diameter (inches) Product Thickness before Recovery (feet) Product Thickness after Recovery (feet) Amount of Liquid Recovered (gallons) Amount of Product Recovered as Liquid (gallons) MW-2 & MW-24 Gasoline 02/23/22 AFVR 2 0.00 0.00 2,576 0.00 Notes : • *: Bailing, Skimming, Aggressive Fluid Vapor Recovery (AFVR), Mobile Multiphase Extraction (MMPE) • **: No free product was observed during initial gauging event; however, free product entered the well during purging activities. • Amount of Liquid Recovered (gallons) includes Total liquids (Water and Free Product) as indicated on Disposal Manifest. • Amount of Product Recovered (in gallons) includes only the volume of free product in the tanker at the end of the event (based on Disposal Manifest and/or Field Notes). • *Assumed recorded data was before FP recovery • NA: Information not available TABLE 6 FREE PRODUCT RECOVERY RESULTS EVERETTE'S ENTERPRISES (INCIDENT NO. 11174) Facility ID#: 00-0-0000009694 Interface probe at top-of-casing Page 1 of 1 Date: 4/22/22 MW-2 & MW-24 02/23/22 AFVR 290.00 107.10 7.50 0.03 2,576 0.00 0.03 0.03 2,576.00 0.00 0.03 Notes: • *: Bailing, Skimming, Aggressive Fluid Vapor Recovery (AFVR), Mobile Multiphase Extraction (MMPE) • Amount of Vaporized Product (in gallons) is based on Vapor Emissions Summary Sheet, = lbs emitted/6.25 • Amount of Liquid Recovered includes Total liquids (Water and Free Product) • Amount of Product Recovered as Liquid includes only the volume of free product at the end of the event • Total Amount of Product Recovered = Amount of Vaporized Product + Amount of Product Recovered as Liquid • Total Fluids Removed = Amount of Vaporized Product + Amount of Liquid Recovered • Information regarding historical free product recovery activities from other consulting companies were not included. SUMMARY OF FLUID REMOVAL TABLE 7 FREE PRODUCT RECOVERY EVENT INFORMATION EVERETTE'S ENTERPRISES (INCIDENT NO. 11174) Facility ID #: 00-0-0000009694 Well ID Date (mm/dd/yy) Product Recovery Method* Average Effluent Velocity (ft/min) Average Effluent Temperature (°F) Average Effluent Concentration (ppm) Amount of Vaporized Product (gallons) Amount of Liquid Recovered (gallons) Amount of Product Recovered as Liquid (gallons) Total Amount of Product Recovered (gallons) Totals Total To Date 2,576.03 0.03 Summary Total Fluids Removed (in gallons)Total Product Removed (in gallons) Current Event 2,576.03 0.03 Page 1 of 1 Date: 4/22/22 Wells Included in Event Product Recovery Method* Date of Event (mm/dd/yy) Total Amount of Free Product plus Ground Water Recovered (gallons) Cost of Free Product Recovery Event Cost Per Gallon (total fluids) MW-2 & MWD-24 AFVR 02/23/22 2,576.00 $3,183.10 $1.24 2,576.00 $3,183.10 $1.24 Notes: • Total Amount of Free Product Recovered = Amount of Vaporized Product + Amount of Product Recovered as Liquid TOTAL (to date) • Cost of Free Product Recovery Event includes supervision, travel, mileage, per diem, subcontractor costs, MMPE sampling, MMPE sampling analytical, report preparation (pre-2015 only) and project management. TABLE 8 FREE PRODUCT RECOVERY COST SUMMARY EVERETTE'S ENTERPRISES (INCIDENT NO. 11174) Facility ID #: 00-0-0000009694 Comments Cost per gallon for the event is based on a total volume of 2,575 gallons of liquid recovered. Page 1 of 1 APPENDICES APPENDIX A State Correspondence 2459 Received AUG 30 2021 2459 Received SEP 16 2021 APPENDIX B Laboratory Reports – Ground Water 03/07/22 Technical Report for GRI (Geological Resources Inc.) Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC 11174/2459 SGS Job Number: FA93395 Sampling Date: 02/23/22 Report to: GRI 3502 Hayes Rd Monroe, NC 28110 nml@geologicalresourcesinc.com; carriekennedy@geologicalresourcesinc.com; jjr@geologicalresourcesinc.com ATTN: Nicole Long Total number of pages in report: Certifications: FL(E83510), LA(03051), KS(E-10327), NC(573), NJ(FL002), NY(12022), SC(96038001) DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177), AL, AK, AR, CT, IA, KY, MA, MI. MS, ND, NH, NV, OK, OR, IL, UT, VT, WA, WI, WV This report shall not be reproduced, except in its entirety, without the written approval of SGS. Test results relate only to samples analyzed. SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: 407-425-6700 • fax: 407-425-0707 Test results contained within this data package meet the requirements of the National Environmental Laboratory Accreditation Program and/or state specific certification programs as applicable. Client Service contact: Muna Mohammed 407-425-6700 Norm Farmer Technical Director Orlando, FL 03/07/22 e-Hardcopy 2.0 Automated Report 14 SGS is the sole authority for authorizing edits or modifications to this document. Unauthorized modification of this report is strictly prohibited. Review standard terms at: http://www.sgs.com/en/terms-and-conditions The results set forth herein are provided by SGS North America Inc. Please share your ideas about how we can serve you better at: EHS.US.CustomerCare@sgs.com 1 of 14 FA93395 Table of Contents -1- Sections: Section 1: Sample Summary ...................................................................................................3 Section 2: Summary of Hits ....................................................................................................4 Section 3: Sample Results ........................................................................................................5 3.1: FA93395-1: MW-3 ........................................................................................................6 3.2: FA93395-2: MW-2 ........................................................................................................7 Section 4: Misc. Forms ............................................................................................................8 4.1: Chain of Custody ...........................................................................................................9 Section 5: MS Volatiles - QC Data Summaries .....................................................................11 5.1: Method Blank Summary ................................................................................................12 5.2: Blank Spike Summary ...................................................................................................13 5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................14 123452 of 14 FA93395 SGS North America Inc. Sample Summary GRI (Geological Resources Inc.) Job No:FA93395 Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC Project No: 11174/2459 Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID This report contains results reported as ND = Not detected. The following applies: Organics ND = Not detected above the MDL FA93395-1 02/23/22 08:11 JB 02/24/22 AQ Ground Water MW-3 FA93395-2 02/23/22 08:23 JB 02/24/22 AQ Ground Water MW-2 3 of 14 FA933951 Summary of Hits Page 1 of 1 Job Number:FA93395 Account:GRI (Geological Resources Inc.) Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC Collected:02/23/22 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method FA93395-1 MW-3 No hits reported in this sample. FA93395-2 MW-2 Benzene 5670 250 63 ug/l SM 6200B Ethylbenzene 2160 250 63 ug/l SM 6200B Methyl Tert Butyl Ether 2380 250 63 ug/l SM 6200B Naphthalene 521 250 63 ug/l SM 6200B Toluene 16700 250 63 ug/l SM 6200B Xylene (total)10600 750 130 ug/l SM 6200B 4 of 14 FA933952 SGS North America Inc. Sample Results Report of Analysis Orlando, FL Section 3 5 of 14 FA933953 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID:MW-3 Lab Sample ID:FA93395-1 Date Sampled:02/23/22 Matrix:AQ - Ground Water Date Received:02/24/22 Method:SM 6200B Percent Solids:n/a Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 A0230753.D 1 03/03/22 20:53 JL n/a n/a VA3078 Run #2 Purge Volume Run #1 10.0 ml Run #2 Purgeable Aromatics, Full List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l 100-41-4 Ethylbenzene ND 0.50 0.13 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l 91-20-3 Naphthalene ND 0.50 0.13 ug/l 108-88-3 Toluene ND 0.50 0.13 ug/l 1330-20-7 Xylene (total)ND 1.5 0.25 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 99%70-130% 17060-07-0 1,2-Dichloroethane-D4 101%70-130% 2037-26-5 Toluene-D8 100%70-130% 460-00-4 4-Bromofluorobenzene 101%70-130% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 6 of 14 FA9339533.1 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID:MW-2 Lab Sample ID:FA93395-2 Date Sampled:02/23/22 Matrix:AQ - Ground Water Date Received:02/24/22 Method:SM 6200B Percent Solids:n/a Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 A0230756.D 500 03/03/22 22:02 JL n/a n/a VA3078 Run #2 Purge Volume Run #1 10.0 ml Run #2 Purgeable Aromatics, Full List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene 5670 250 63 ug/l 108-90-7 Chlorobenzene ND 250 63 ug/l 95-50-1 1,2-Dichlorobenzene ND 250 63 ug/l 541-73-1 1,3-Dichlorobenzene ND 250 63 ug/l 106-46-7 1,4-Dichlorobenzene ND 250 63 ug/l 108-20-3 Di-Isopropyl Ether ND 250 63 ug/l 100-41-4 Ethylbenzene 2160 250 63 ug/l 1634-04-4 Methyl Tert Butyl Ether 2380 250 63 ug/l 91-20-3 Naphthalene 521 250 63 ug/l 108-88-3 Toluene 16700 250 63 ug/l 1330-20-7 Xylene (total)10600 750 130 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 100%70-130% 17060-07-0 1,2-Dichloroethane-D4 100%70-130% 2037-26-5 Toluene-D8 102%70-130% 460-00-4 4-Bromofluorobenzene 103%70-130% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 7 of 14 FA9339533.2 SGS North America Inc. Misc. Forms Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody Orlando, FL Section 4 8 of 14 FA933954 FA93395: Chain of Custody Page 1 of 2 9 of 14 FA9339544.1 Job Number:FA93395 Client:GEOLOGICAL RESOURCES INC. Date / Time Received:2/24/2022 11:10:00 AM Delivery Method:FEDEX Project:EVERETTE'S ENTERPRISES Airbill #'s:1009 6379 4050 Cooler Information 1. Custody Seals Present 2. Custody Seals Intact 4. Cooler temp verification 3. Temp criteria achieved 5. Cooler media IR Gun Ice (Bag) Trip Blank Information 1. Trip Blank present / cooler 2. Trip Blank listed on COC 2. Samples preserved properly Sample Information 1. Sample labels present on bottles 5. Sample recvd within HT 4. Condition of sample 3. Sufficient volume/containers recvd for analysis: Intact Comments SM001Rev. Date 05/24/17 SGS Sample Receipt Summary Cooler Temps (Raw Measured) °C: Cooler Temps (Corrected) °C: Cooler 1: (2.8); Cooler 1: (3.2); 3. Type Of TB Received W or S N/A 6. Dates/Times/IDs on COC match Sample Label 7. VOCs have headspace 8. Bottles received for unspecified tests 9. Compositing instructions clear 10. Voa Soil Kits/Jars received past 48hrs? 11. % Solids Jar received? Misc. Information 25-Gram 5-GramNumber of Encores:Number of 5035 Field Kits:Number of Lab Filtered Metals: Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify) Y or N N/A Y or N Therm ID:IR 1; Therm CF:0.4; # of Coolers:1 Y or N N/A 12. Residual Chlorine Present? Residual Chlorine Test Strip Lot #: Technician:Reviewer:SAMUELM Date:Date:2/24/2022 11:10:00 A FA93395: Chain of Custody Page 2 of 2 10 of 14 FA9339544.1 SGS North America Inc. MS Volatiles QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries Orlando, FL Section 5 11 of 14 FA933955 Method Blank Summary Page 1 of 1 Job Number:FA93395 Account:GRINCC GRI (Geological Resources Inc.) Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VA3078-MB A0230736.D 1 03/03/22 JL n/a n/a VA3078 The QC reported here applies to the following samples:Method: SM 6200B FA93395-1, FA93395-2 CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l 100-41-4 Ethylbenzene ND 0.50 0.13 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l 91-20-3 Naphthalene ND 0.50 0.13 ug/l 108-88-3 Toluene ND 0.50 0.13 ug/l 1330-20-7 Xylene (total)ND 1.5 0.25 ug/l CAS No.Surrogate Recoveries Limits 1868-53-7 Dibromofluoromethane 98%70-130% 17060-07-0 1,2-Dichloroethane-D4 100%70-130% 2037-26-5 Toluene-D8 101%70-130% 460-00-4 4-Bromofluorobenzene 101%70-130% 12 of 14 FA9339555.1.1 Blank Spike Summary Page 1 of 1 Job Number:FA93395 Account:GRINCC GRI (Geological Resources Inc.) Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VA3078-BS A0230734.D 1 03/03/22 JL n/a n/a VA3078 The QC reported here applies to the following samples:Method: SM 6200B FA93395-1, FA93395-2 Spike BSP BSP CAS No.Compound ug/l ug/l %Limits 71-43-2 Benzene 10 10.9 109 70-130 108-90-7 Chlorobenzene 10 10.6 106 70-130 95-50-1 1,2-Dichlorobenzene 10 10.9 109 70-130 541-73-1 1,3-Dichlorobenzene 10 11.1 111 70-130 106-46-7 1,4-Dichlorobenzene 10 10.5 105 70-130 108-20-3 Di-Isopropyl Ether 10 10.1 101 70-130 100-41-4 Ethylbenzene 10 11.2 112 70-130 1634-04-4 Methyl Tert Butyl Ether 10 9.7 97 70-130 91-20-3 Naphthalene 10 10.3 103 70-130 108-88-3 Toluene 10 11.0 110 70-130 1330-20-7 Xylene (total)30 34.5 115 70-130 CAS No.Surrogate Recoveries BSP Limits 1868-53-7 Dibromofluoromethane 100%70-130% 17060-07-0 1,2-Dichloroethane-D4 97%70-130% 2037-26-5 Toluene-D8 101%70-130% 460-00-4 4-Bromofluorobenzene 102%70-130% * = Outside of Control Limits. 13 of 14 FA9339555.2.1 Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1 Job Number:FA93395 Account:GRINCC GRI (Geological Resources Inc.) Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA93447-2MS A0230759.D 5 03/03/22 JL n/a n/a VA3078 FA93447-2MSD A0230760.D 5 03/03/22 JL n/a n/a VA3078 FA93447-2 A0230758.D 5 03/03/22 JL n/a n/a VA3078 The QC reported here applies to the following samples:Method: SM 6200B FA93395-1, FA93395-2 FA93447-2 Spike MS MS Spike MSD MSD Limits CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD 71-43-2 Benzene 98.9 50 149 100 50 151 104 1 70-130/20 108-90-7 Chlorobenzene ND 50 55.6 111 50 59.0 118 6 70-130/20 95-50-1 1,2-Dichlorobenzene ND 50 56.5 113 50 60.7 121 7 70-130/20 541-73-1 1,3-Dichlorobenzene ND 50 57.0 114 50 61.3 123 7 70-130/20 106-46-7 1,4-Dichlorobenzene ND 50 53.5 107 50 57.2 114 7 70-130/20 108-20-3 Di-Isopropyl Ether ND 50 52.4 105 50 56.6 113 8 70-130/20 100-41-4 Ethylbenzene 37.6 50 95.3 115 50 97.8 120 3 70-130/20 1634-04-4 Methyl Tert Butyl Ether ND 50 50.4 101 50 54.4 109 8 70-130/20 91-20-3 Naphthalene 4.3 50 59.9 111 50 65.6 123 9 70-130/20 108-88-3 Toluene 76.0 50 129 106 50 130 108 1 70-130/20 1330-20-7 Xylene (total)133 150 314 121 150 321 125 2 70-130/20 CAS No.Surrogate Recoveries MS MSD FA93447-2 Limits 1868-53-7 Dibromofluoromethane 100%98%102%70-130% 17060-07-0 1,2-Dichloroethane-D4 98%98%101%70-130% 2037-26-5 Toluene-D8 101%101%101%70-130% 460-00-4 4-Bromofluorobenzene 100%101%102%70-130% * = Outside of Control Limits. 14 of 14 FA9339555.3.1 04/11/22 Technical Report for GRI (Geological Resources Inc.) Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC 11174/2459 SGS Job Number: FA94246 Sampling Date: 03/23/22 Report to: GRI 3502 Hayes Rd Monroe, NC 28110 wlr@geologicalresourcesinc.com; carriekennedy@geologicalresourcesinc.com; jjr@geologicalresourcesinc.com ATTN: William Regenthal Total number of pages in report: Certifications: FL(E83510), LA(03051), KS(E-10327), NC(573), NJ(FL002), NY(12022), SC(96038001) DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177), AL, AK, AR, CT, IA, KY, MA, MI. MS, ND, NH, NV, OK, OR, IL, UT, VT, WA, WI, WV This report shall not be reproduced, except in its entirety, without the written approval of SGS. Test results relate only to samples analyzed. SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: 407-425-6700 • fax: 407-425-0707 Test results contained within this data package meet the requirements of the National Environmental Laboratory Accreditation Program and/or state specific certification programs as applicable. Client Service contact: Muna Mohammed 407-425-6700 Norm Farmer Technical Director Orlando, FL 04/11/22 e-Hardcopy 2.0 Automated Report 39 SGS is the sole authority for authorizing edits or modifications to this document. Unauthorized modification of this report is strictly prohibited. Review standard terms at: http://www.sgs.com/en/terms-and-conditions The results set forth herein are provided by SGS North America Inc. Please share your ideas about how we can serve you better at: EHS.US.CustomerCare@sgs.com 1 of 39 FA94246 Table of Contents -1- Sections: Section 1: Sample Summary ...................................................................................................3 Section 2: Summary of Hits ....................................................................................................4 Section 3: Sample Results ........................................................................................................6 3.1: FA94246-1: MW-1 ........................................................................................................7 3.2: FA94246-2: MW-2 ........................................................................................................10 3.3: FA94246-3: MW-3 ........................................................................................................12 3.4: FA94246-4: MW-13 ......................................................................................................14 3.5: FA94246-5: MW-15 ......................................................................................................16 3.6: FA94246-6: TRIP BLANK ...........................................................................................18 Section 4: Misc. Forms ............................................................................................................20 4.1: Chain of Custody ...........................................................................................................21 Section 5: MS Volatiles - QC Data Summaries .....................................................................23 5.1: Method Blank Summary ................................................................................................24 5.2: Blank Spike Summary ...................................................................................................29 5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................34 123452 of 39 FA94246 SGS North America Inc. Sample Summary GRI (Geological Resources Inc.) Job No:FA94246 Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC Project No: 11174/2459 Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID This report contains results reported as ND = Not detected. The following applies: Organics ND = Not detected above the MDL FA94246-1 03/23/22 10:07 JB 03/24/22 AQ Ground Water MW-1 FA94246-2 03/23/22 10:32 JB 03/24/22 AQ Ground Water MW-2 FA94246-3 03/23/22 10:51 JB 03/24/22 AQ Ground Water MW-3 FA94246-4 03/23/22 11:12 JB 03/24/22 AQ Ground Water MW-13 FA94246-5 03/23/22 11:27 JB 03/24/22 AQ Ground Water MW-15 FA94246-6 03/23/22 08:58 JB 03/24/22 AQ Trip Blank Water TRIP BLANK 3 of 39 FA942461 Summary of Hits Page 1 of 2 Job Number:FA94246 Account:GRI (Geological Resources Inc.) Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC Collected:03/23/22 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method FA94246-1 MW-1 Benzene 1180 50 13 ug/l SM 6200B n-Butylbenzene 19.7 0.50 0.13 ug/l SM 6200B sec-Butylbenzene 13.6 0.50 0.13 ug/l SM 6200B tert-Butylbenzene 0.83 0.50 0.13 ug/l SM 6200B Chloroethane 2.0 0.50 0.20 ug/l SM 6200B o-Chlorotoluene 40.9 0.50 0.13 ug/l SM 6200B 1,2-Dibromoethane 3.6 0.50 0.13 ug/l SM 6200B 1,2-Dichloroethane 8.3 0.50 0.13 ug/l SM 6200B 2,2-Dichloropropane 0.24 J 0.50 0.13 ug/l SM 6200B Di-Isopropyl Ether 2.7 0.50 0.13 ug/l SM 6200B Ethylbenzene 577 50 13 ug/l SM 6200B Isopropylbenzene 42.6 0.50 0.13 ug/l SM 6200B p-Isopropyltoluene 11.4 0.50 0.13 ug/l SM 6200B Methyl Chloride 2.6 0.50 0.20 ug/l SM 6200B Methyl Tert Butyl Ether 121 50 13 ug/l SM 6200B Naphthalene 219 50 13 ug/l SM 6200B n-Propylbenzene 72.7 50 13 ug/l SM 6200B Styrene 6.0 0.50 0.13 ug/l SM 6200B 1,1,2,2-Tetrachloroethane a 9.1 0.50 0.13 ug/l SM 6200B Toluene 4580 50 13 ug/l SM 6200B 1,2,4-Trimethylbenzene 1080 50 13 ug/l SM 6200B 1,3,5-Trimethylbenzene 322 50 13 ug/l SM 6200B m,p-Xylene 2600 100 13 ug/l SM 6200B o-Xylene 1200 50 13 ug/l SM 6200B Xylene (total)3800 150 25 ug/l SM 6200B FA94246-2 MW-2 Benzene b 3460 130 31 ug/l SM 6200B 1,2-Dichloroethane b 35.3 J 130 31 ug/l SM 6200B Ethylbenzene b 1180 130 31 ug/l SM 6200B Isopropylbenzene b 49.0 J 130 31 ug/l SM 6200B Methyl Tert Butyl Ether b 1610 130 31 ug/l SM 6200B Naphthalene b 244 130 31 ug/l SM 6200B n-Propylbenzene b 128 J 130 31 ug/l SM 6200B Toluene b 10100 130 31 ug/l SM 6200B 1,2,4-Trimethylbenzene b 1260 130 31 ug/l SM 6200B 1,3,5-Trimethylbenzene b 357 130 31 ug/l SM 6200B m,p-Xylene b 4410 250 31 ug/l SM 6200B o-Xylene b 1850 130 31 ug/l SM 6200B Xylene (total) b 6260 380 63 ug/l SM 6200B 4 of 39 FA942462 Summary of Hits Page 2 of 2 Job Number:FA94246 Account:GRI (Geological Resources Inc.) Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC Collected:03/23/22 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method FA94246-3 MW-3 Benzene b 1480 250 63 ug/l SM 6200B Ethylbenzene b 2430 250 63 ug/l SM 6200B Isopropylbenzene b 94.3 J 250 63 ug/l SM 6200B Methyl Tert Butyl Ether b 222 J 250 63 ug/l SM 6200B Naphthalene b 392 250 63 ug/l SM 6200B n-Propylbenzene b 262 250 63 ug/l SM 6200B Toluene b 14100 250 63 ug/l SM 6200B 1,2,4-Trimethylbenzene b 2050 250 63 ug/l SM 6200B 1,3,5-Trimethylbenzene b 572 250 63 ug/l SM 6200B m,p-Xylene b 7870 500 63 ug/l SM 6200B o-Xylene b 3770 250 63 ug/l SM 6200B Xylene (total) b 11600 750 130 ug/l SM 6200B FA94246-4 MW-13 Benzene b 11.8 1.0 0.25 ug/l SM 6200B n-Butylbenzene b 0.61 J 1.0 0.25 ug/l SM 6200B sec-Butylbenzene b 1.0 1.0 0.25 ug/l SM 6200B 1,2-Dichloroethane b 0.35 J 1.0 0.25 ug/l SM 6200B Di-Isopropyl Ether b 0.50 J 1.0 0.25 ug/l SM 6200B Ethylbenzene b 0.58 J 1.0 0.25 ug/l SM 6200B Isopropylbenzene b 2.5 1.0 0.25 ug/l SM 6200B Methyl Tert Butyl Ether b 68.0 1.0 0.25 ug/l SM 6200B Naphthalene b 5.9 1.0 0.25 ug/l SM 6200B n-Propylbenzene b 4.3 1.0 0.25 ug/l SM 6200B Toluene b 1.4 1.0 0.25 ug/l SM 6200B 1,2,4-Trimethylbenzene b 3.4 1.0 0.25 ug/l SM 6200B 1,3,5-Trimethylbenzene b 0.42 J 1.0 0.25 ug/l SM 6200B m,p-Xylene b 3.2 2.0 0.25 ug/l SM 6200B o-Xylene b 0.62 J 1.0 0.25 ug/l SM 6200B Xylene (total) b 3.8 3.0 0.50 ug/l SM 6200B FA94246-5 MW-15 No hits reported in this sample. FA94246-6 TRIP BLANK 2,2-Dichloropropane b 0.18 J 0.50 0.13 ug/l SM 6200B (a) Associated ECC outside of control limits high. (b) No ECC available for this run. Insufficient sample available for reanalysis. 5 of 39 FA942462 SGS North America Inc. Sample Results Report of Analysis Orlando, FL Section 3 6 of 39 FA942463 SGS North America Inc. Report of Analysis Page 1 of 3 Client Sample ID:MW-1 Lab Sample ID:FA94246-1 Date Sampled:03/23/22 Matrix:AQ - Ground Water Date Received:03/24/22 Method:SM 6200B Percent Solids:n/a Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 A0231336.D 1 03/30/22 19:55 SS n/a n/a VA3099 Run #2 A0231427.D 100 04/05/22 22:06 SS n/a n/a VA3104 Purge Volume Run #1 10.0 ml Run #2 10.0 ml VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene 1180 a 50 13 ug/l 108-86-1 Bromobenzene ND 0.50 0.13 ug/l 74-97-5 Bromochloromethane ND 0.50 0.13 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l 75-25-2 Bromoform b ND 0.50 0.13 ug/l 104-51-8 n-Butylbenzene 19.7 0.50 0.13 ug/l 135-98-8 sec-Butylbenzene 13.6 0.50 0.13 ug/l 98-06-6 tert-Butylbenzene 0.83 0.50 0.13 ug/l 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane 2.0 0.50 0.20 ug/l 67-66-3 Chloroform ND 0.50 0.13 ug/l 95-49-8 o-Chlorotoluene 40.9 0.50 0.13 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l 96-12-8 1,2-Dibromo-3-chloropropan b ND 0.50 0.25 ug/l 106-93-4 1,2-Dibromoethane 3.6 0.50 0.13 ug/l 75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l 107-06-2 1,2-Dichloroethane 8.3 0.50 0.13 ug/l 75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l 594-20-7 2,2-Dichloropropane 0.24 0.50 0.13 ug/l J 563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 7 of 39 FA9424633.1 SGS North America Inc. Report of Analysis Page 2 of 3 Client Sample ID:MW-1 Lab Sample ID:FA94246-1 Date Sampled:03/23/22 Matrix:AQ - Ground Water Date Received:03/24/22 Method:SM 6200B Percent Solids:n/a Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether 2.7 0.50 0.13 ug/l 100-41-4 Ethylbenzene 577 a 50 13 ug/l 87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l 98-82-8 Isopropylbenzene 42.6 0.50 0.13 ug/l 99-87-6 p-Isopropyltoluene 11.4 0.50 0.13 ug/l 74-83-9 Methyl Bromide ND 0.50 0.20 ug/l 74-87-3 Methyl Chloride 2.6 0.50 0.20 ug/l 74-95-3 Methylene Bromide ND 0.50 0.13 ug/l 75-09-2 Methylene Chloride ND 2.0 1.0 ug/l 1634-04-4 Methyl Tert Butyl Ether 121 a 50 13 ug/l 91-20-3 Naphthalene 219 a 50 13 ug/l 103-65-1 n-Propylbenzene 72.7 a 50 13 ug/l 100-42-5 Styrene 6.0 0.50 0.13 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l 79-34-5 1,1,2,2-Tetrachloroethane c 9.1 0.50 0.13 ug/l 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l 108-88-3 Toluene 4580 a 50 13 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l 71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l 79-01-6 Trichloroethylene ND 0.50 0.13 ug/l 75-69-4 Trichlorofluoromethane d ND 0.50 0.20 ug/l 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l 95-63-6 1,2,4-Trimethylbenzene 1080 a 50 13 ug/l 108-67-8 1,3,5-Trimethylbenzene 322 a 50 13 ug/l 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l m,p-Xylene 2600 a 100 13 ug/l 95-47-6 o-Xylene 1200 a 50 13 ug/l 1330-20-7 Xylene (total)3800 a 150 25 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 94%100%70-130% 17060-07-0 1,2-Dichloroethane-D4 122%98%70-130% 2037-26-5 Toluene-D8 103%100%70-130% 460-00-4 4-Bromofluorobenzene 119%96%70-130% (a) Result is from Run# 2 (b) Associated ECC outside of control limits high, sample was ND. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 8 of 39 FA9424633.1 SGS North America Inc. Report of Analysis Page 3 of 3 Client Sample ID:MW-1 Lab Sample ID:FA94246-1 Date Sampled:03/23/22 Matrix:AQ - Ground Water Date Received:03/24/22 Method:SM 6200B Percent Solids:n/a Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q (c) Associated ECC outside of control limits high. (d) Associated CCV and BS recovery outside control limits high, sample was ND. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 9 of 39 FA9424633.1 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID:MW-2 Lab Sample ID:FA94246-2 Date Sampled:03/23/22 Matrix:AQ - Ground Water Date Received:03/24/22 Method:SM 6200B Percent Solids:n/a Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 a A0231457.D 250 04/06/22 20:59 SS n/a n/a VA3106 Run #2 Purge Volume Run #1 10.0 ml Run #2 VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene 3460 130 31 ug/l 108-86-1 Bromobenzene ND 130 31 ug/l 74-97-5 Bromochloromethane ND 130 31 ug/l 75-27-4 Bromodichloromethane ND 130 31 ug/l 75-25-2 Bromoform ND 130 31 ug/l 104-51-8 n-Butylbenzene ND 130 31 ug/l 135-98-8 sec-Butylbenzene ND 130 31 ug/l 98-06-6 tert-Butylbenzene ND 130 31 ug/l 56-23-5 Carbon Tetrachloride ND 130 31 ug/l 108-90-7 Chlorobenzene ND 130 31 ug/l 75-00-3 Chloroethane b ND 130 50 ug/l 67-66-3 Chloroform ND 130 31 ug/l 95-49-8 o-Chlorotoluene ND 130 31 ug/l 106-43-4 p-Chlorotoluene ND 130 31 ug/l 124-48-1 Dibromochloromethane ND 130 31 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 130 62 ug/l 106-93-4 1,2-Dibromoethane ND 130 31 ug/l 75-71-8 Dichlorodifluoromethane ND 130 50 ug/l 95-50-1 1,2-Dichlorobenzene ND 130 31 ug/l 541-73-1 1,3-Dichlorobenzene ND 130 31 ug/l 106-46-7 1,4-Dichlorobenzene ND 130 31 ug/l 75-34-3 1,1-Dichloroethane ND 130 31 ug/l 107-06-2 1,2-Dichloroethane 35.3 130 31 ug/l J 75-35-4 1,1-Dichloroethylene ND 130 31 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 130 31 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 130 31 ug/l 78-87-5 1,2-Dichloropropane ND 130 31 ug/l 142-28-9 1,3-Dichloropropane ND 130 31 ug/l 594-20-7 2,2-Dichloropropane ND 130 31 ug/l 563-58-6 1,1-Dichloropropene ND 130 31 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 130 31 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 130 31 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 10 of 39 FA9424633.2 SGS North America Inc. Report of Analysis Page 2 of 2 Client Sample ID:MW-2 Lab Sample ID:FA94246-2 Date Sampled:03/23/22 Matrix:AQ - Ground Water Date Received:03/24/22 Method:SM 6200B Percent Solids:n/a Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether ND 130 31 ug/l 100-41-4 Ethylbenzene 1180 130 31 ug/l 87-68-3 Hexachlorobutadiene ND 130 31 ug/l 98-82-8 Isopropylbenzene 49.0 130 31 ug/l J 99-87-6 p-Isopropyltoluene ND 130 31 ug/l 74-83-9 Methyl Bromide ND 130 50 ug/l 74-87-3 Methyl Chloride ND 130 50 ug/l 74-95-3 Methylene Bromide ND 130 31 ug/l 75-09-2 Methylene Chloride ND 500 250 ug/l 1634-04-4 Methyl Tert Butyl Ether 1610 130 31 ug/l 91-20-3 Naphthalene 244 130 31 ug/l 103-65-1 n-Propylbenzene 128 130 31 ug/l J 100-42-5 Styrene ND 130 31 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 130 31 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 130 31 ug/l 127-18-4 Tetrachloroethylene ND 130 31 ug/l 108-88-3 Toluene 10100 130 31 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 130 31 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 130 31 ug/l 71-55-6 1,1,1-Trichloroethane ND 130 31 ug/l 79-00-5 1,1,2-Trichloroethane ND 130 31 ug/l 79-01-6 Trichloroethylene ND 130 31 ug/l 75-69-4 Trichlorofluoromethane ND 130 50 ug/l 96-18-4 1,2,3-Trichloropropane ND 130 31 ug/l 95-63-6 1,2,4-Trimethylbenzene 1260 130 31 ug/l 108-67-8 1,3,5-Trimethylbenzene 357 130 31 ug/l 75-01-4 Vinyl Chloride ND 130 31 ug/l m,p-Xylene 4410 250 31 ug/l 95-47-6 o-Xylene 1850 130 31 ug/l 1330-20-7 Xylene (total)6260 380 63 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 97%70-130% 17060-07-0 1,2-Dichloroethane-D4 104%70-130% 2037-26-5 Toluene-D8 102%70-130% 460-00-4 4-Bromofluorobenzene 100%70-130% (a) No ECC available for this run. Insufficient sample available for reanalysis. (b) Associated Initial Calibration outside control limits (%RSD > 15%); sample is ND. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 11 of 39 FA9424633.2 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID:MW-3 Lab Sample ID:FA94246-3 Date Sampled:03/23/22 Matrix:AQ - Ground Water Date Received:03/24/22 Method:SM 6200B Percent Solids:n/a Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 a A0231458.D 500 04/06/22 21:22 SS n/a n/a VA3106 Run #2 Purge Volume Run #1 10.0 ml Run #2 VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene 1480 250 63 ug/l 108-86-1 Bromobenzene ND 250 63 ug/l 74-97-5 Bromochloromethane ND 250 63 ug/l 75-27-4 Bromodichloromethane ND 250 63 ug/l 75-25-2 Bromoform ND 250 63 ug/l 104-51-8 n-Butylbenzene ND 250 63 ug/l 135-98-8 sec-Butylbenzene ND 250 63 ug/l 98-06-6 tert-Butylbenzene ND 250 63 ug/l 56-23-5 Carbon Tetrachloride ND 250 63 ug/l 108-90-7 Chlorobenzene ND 250 63 ug/l 75-00-3 Chloroethane b ND 250 100 ug/l 67-66-3 Chloroform ND 250 63 ug/l 95-49-8 o-Chlorotoluene ND 250 63 ug/l 106-43-4 p-Chlorotoluene ND 250 63 ug/l 124-48-1 Dibromochloromethane ND 250 63 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 250 120 ug/l 106-93-4 1,2-Dibromoethane ND 250 63 ug/l 75-71-8 Dichlorodifluoromethane ND 250 100 ug/l 95-50-1 1,2-Dichlorobenzene ND 250 63 ug/l 541-73-1 1,3-Dichlorobenzene ND 250 63 ug/l 106-46-7 1,4-Dichlorobenzene ND 250 63 ug/l 75-34-3 1,1-Dichloroethane ND 250 63 ug/l 107-06-2 1,2-Dichloroethane ND 250 63 ug/l 75-35-4 1,1-Dichloroethylene ND 250 63 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 250 63 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 250 63 ug/l 78-87-5 1,2-Dichloropropane ND 250 63 ug/l 142-28-9 1,3-Dichloropropane ND 250 63 ug/l 594-20-7 2,2-Dichloropropane ND 250 63 ug/l 563-58-6 1,1-Dichloropropene ND 250 63 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 250 63 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 250 63 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 12 of 39 FA9424633.3 SGS North America Inc. Report of Analysis Page 2 of 2 Client Sample ID:MW-3 Lab Sample ID:FA94246-3 Date Sampled:03/23/22 Matrix:AQ - Ground Water Date Received:03/24/22 Method:SM 6200B Percent Solids:n/a Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether ND 250 63 ug/l 100-41-4 Ethylbenzene 2430 250 63 ug/l 87-68-3 Hexachlorobutadiene ND 250 63 ug/l 98-82-8 Isopropylbenzene 94.3 250 63 ug/l J 99-87-6 p-Isopropyltoluene ND 250 63 ug/l 74-83-9 Methyl Bromide ND 250 100 ug/l 74-87-3 Methyl Chloride ND 250 100 ug/l 74-95-3 Methylene Bromide ND 250 63 ug/l 75-09-2 Methylene Chloride ND 1000 500 ug/l 1634-04-4 Methyl Tert Butyl Ether 222 250 63 ug/l J 91-20-3 Naphthalene 392 250 63 ug/l 103-65-1 n-Propylbenzene 262 250 63 ug/l 100-42-5 Styrene ND 250 63 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 250 63 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 250 63 ug/l 127-18-4 Tetrachloroethylene ND 250 63 ug/l 108-88-3 Toluene 14100 250 63 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 250 63 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 250 63 ug/l 71-55-6 1,1,1-Trichloroethane ND 250 63 ug/l 79-00-5 1,1,2-Trichloroethane ND 250 63 ug/l 79-01-6 Trichloroethylene ND 250 63 ug/l 75-69-4 Trichlorofluoromethane ND 250 100 ug/l 96-18-4 1,2,3-Trichloropropane ND 250 63 ug/l 95-63-6 1,2,4-Trimethylbenzene 2050 250 63 ug/l 108-67-8 1,3,5-Trimethylbenzene 572 250 63 ug/l 75-01-4 Vinyl Chloride ND 250 63 ug/l m,p-Xylene 7870 500 63 ug/l 95-47-6 o-Xylene 3770 250 63 ug/l 1330-20-7 Xylene (total)11600 750 130 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 102%70-130% 17060-07-0 1,2-Dichloroethane-D4 106%70-130% 2037-26-5 Toluene-D8 101%70-130% 460-00-4 4-Bromofluorobenzene 100%70-130% (a) No ECC available for this run. Insufficient sample available for reanalysis. (b) Associated Initial Calibration outside control limits (%RSD > 15%); sample is ND. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 13 of 39 FA9424633.3 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID:MW-13 Lab Sample ID:FA94246-4 Date Sampled:03/23/22 Matrix:AQ - Ground Water Date Received:03/24/22 Method:SM 6200B Percent Solids:n/a Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 a A0231459.D 2 04/06/22 21:44 SS n/a n/a VA3106 Run #2 Purge Volume Run #1 10.0 ml Run #2 VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene 11.8 1.0 0.25 ug/l 108-86-1 Bromobenzene ND 1.0 0.25 ug/l 74-97-5 Bromochloromethane ND 1.0 0.25 ug/l 75-27-4 Bromodichloromethane ND 1.0 0.25 ug/l 75-25-2 Bromoform ND 1.0 0.25 ug/l 104-51-8 n-Butylbenzene 0.61 1.0 0.25 ug/l J 135-98-8 sec-Butylbenzene 1.0 1.0 0.25 ug/l 98-06-6 tert-Butylbenzene ND 1.0 0.25 ug/l 56-23-5 Carbon Tetrachloride ND 1.0 0.25 ug/l 108-90-7 Chlorobenzene ND 1.0 0.25 ug/l 75-00-3 Chloroethane b ND 1.0 0.40 ug/l 67-66-3 Chloroform ND 1.0 0.25 ug/l 95-49-8 o-Chlorotoluene ND 1.0 0.25 ug/l 106-43-4 p-Chlorotoluene ND 1.0 0.25 ug/l 124-48-1 Dibromochloromethane ND 1.0 0.25 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 1.0 0.49 ug/l 106-93-4 1,2-Dibromoethane ND 1.0 0.25 ug/l 75-71-8 Dichlorodifluoromethane ND 1.0 0.40 ug/l 95-50-1 1,2-Dichlorobenzene ND 1.0 0.25 ug/l 541-73-1 1,3-Dichlorobenzene ND 1.0 0.25 ug/l 106-46-7 1,4-Dichlorobenzene ND 1.0 0.25 ug/l 75-34-3 1,1-Dichloroethane ND 1.0 0.25 ug/l 107-06-2 1,2-Dichloroethane 0.35 1.0 0.25 ug/l J 75-35-4 1,1-Dichloroethylene ND 1.0 0.25 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 1.0 0.25 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 1.0 0.25 ug/l 78-87-5 1,2-Dichloropropane ND 1.0 0.25 ug/l 142-28-9 1,3-Dichloropropane ND 1.0 0.25 ug/l 594-20-7 2,2-Dichloropropane ND 1.0 0.25 ug/l 563-58-6 1,1-Dichloropropene ND 1.0 0.25 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 1.0 0.25 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 1.0 0.25 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 14 of 39 FA9424633.4 SGS North America Inc. Report of Analysis Page 2 of 2 Client Sample ID:MW-13 Lab Sample ID:FA94246-4 Date Sampled:03/23/22 Matrix:AQ - Ground Water Date Received:03/24/22 Method:SM 6200B Percent Solids:n/a Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether 0.50 1.0 0.25 ug/l J 100-41-4 Ethylbenzene 0.58 1.0 0.25 ug/l J 87-68-3 Hexachlorobutadiene ND 1.0 0.25 ug/l 98-82-8 Isopropylbenzene 2.5 1.0 0.25 ug/l 99-87-6 p-Isopropyltoluene ND 1.0 0.25 ug/l 74-83-9 Methyl Bromide ND 1.0 0.40 ug/l 74-87-3 Methyl Chloride ND 1.0 0.40 ug/l 74-95-3 Methylene Bromide ND 1.0 0.25 ug/l 75-09-2 Methylene Chloride ND 4.0 2.0 ug/l 1634-04-4 Methyl Tert Butyl Ether 68.0 1.0 0.25 ug/l 91-20-3 Naphthalene 5.9 1.0 0.25 ug/l 103-65-1 n-Propylbenzene 4.3 1.0 0.25 ug/l 100-42-5 Styrene ND 1.0 0.25 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 1.0 0.25 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 0.25 ug/l 127-18-4 Tetrachloroethylene ND 1.0 0.25 ug/l 108-88-3 Toluene 1.4 1.0 0.25 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 1.0 0.25 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 1.0 0.25 ug/l 71-55-6 1,1,1-Trichloroethane ND 1.0 0.25 ug/l 79-00-5 1,1,2-Trichloroethane ND 1.0 0.25 ug/l 79-01-6 Trichloroethylene ND 1.0 0.25 ug/l 75-69-4 Trichlorofluoromethane ND 1.0 0.40 ug/l 96-18-4 1,2,3-Trichloropropane ND 1.0 0.25 ug/l 95-63-6 1,2,4-Trimethylbenzene 3.4 1.0 0.25 ug/l 108-67-8 1,3,5-Trimethylbenzene 0.42 1.0 0.25 ug/l J 75-01-4 Vinyl Chloride ND 1.0 0.25 ug/l m,p-Xylene 3.2 2.0 0.25 ug/l 95-47-6 o-Xylene 0.62 1.0 0.25 ug/l J 1330-20-7 Xylene (total)3.8 3.0 0.50 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 104%70-130% 17060-07-0 1,2-Dichloroethane-D4 107%70-130% 2037-26-5 Toluene-D8 99%70-130% 460-00-4 4-Bromofluorobenzene 99%70-130% (a) No ECC available for this run. Insufficient sample available for reanalysis. (b) Associated Initial Calibration outside control limits (%RSD > 15%); sample is ND. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 15 of 39 FA9424633.4 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID:MW-15 Lab Sample ID:FA94246-5 Date Sampled:03/23/22 Matrix:AQ - Ground Water Date Received:03/24/22 Method:SM 6200B Percent Solids:n/a Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 a A0231451.D 1 04/06/22 18:42 SS n/a n/a VA3106 Run #2 Purge Volume Run #1 10.0 ml Run #2 VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.13 ug/l 108-86-1 Bromobenzene ND 0.50 0.13 ug/l 74-97-5 Bromochloromethane ND 0.50 0.13 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l 75-25-2 Bromoform ND 0.50 0.13 ug/l 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane b ND 0.50 0.20 ug/l 67-66-3 Chloroform ND 0.50 0.13 ug/l 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l 75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l 75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l 563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 16 of 39 FA9424633.5 SGS North America Inc. Report of Analysis Page 2 of 2 Client Sample ID:MW-15 Lab Sample ID:FA94246-5 Date Sampled:03/23/22 Matrix:AQ - Ground Water Date Received:03/24/22 Method:SM 6200B Percent Solids:n/a Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l 100-41-4 Ethylbenzene ND 0.50 0.13 ug/l 87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l 74-83-9 Methyl Bromide ND 0.50 0.20 ug/l 74-87-3 Methyl Chloride ND 0.50 0.20 ug/l 74-95-3 Methylene Bromide ND 0.50 0.13 ug/l 75-09-2 Methylene Chloride ND 2.0 1.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l 91-20-3 Naphthalene ND 0.50 0.13 ug/l 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l 100-42-5 Styrene ND 0.50 0.13 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l 108-88-3 Toluene ND 0.50 0.13 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l 71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l 79-01-6 Trichloroethylene ND 0.50 0.13 ug/l 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l m,p-Xylene ND 1.0 0.13 ug/l 95-47-6 o-Xylene ND 0.50 0.13 ug/l 1330-20-7 Xylene (total)ND 1.5 0.25 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 103%70-130% 17060-07-0 1,2-Dichloroethane-D4 105%70-130% 2037-26-5 Toluene-D8 100%70-130% 460-00-4 4-Bromofluorobenzene 100%70-130% (a) No ECC available for this run. Insufficient sample available for reanalysis. (b) Associated Initial Calibration outside control limits (%RSD > 15%); sample is ND. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 17 of 39 FA9424633.5 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID:TRIP BLANK Lab Sample ID:FA94246-6 Date Sampled:03/23/22 Matrix:AQ - Trip Blank Water Date Received:03/24/22 Method:SM 6200B Percent Solids:n/a Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 a A0231449.D 1 04/06/22 17:56 SS n/a n/a VA3106 Run #2 Purge Volume Run #1 10.0 ml Run #2 VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.13 ug/l 108-86-1 Bromobenzene ND 0.50 0.13 ug/l 74-97-5 Bromochloromethane ND 0.50 0.13 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l 75-25-2 Bromoform ND 0.50 0.13 ug/l 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane b ND 0.50 0.20 ug/l 67-66-3 Chloroform ND 0.50 0.13 ug/l 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l 75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l 75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l 594-20-7 2,2-Dichloropropane 0.18 0.50 0.13 ug/l J 563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 18 of 39 FA9424633.6 SGS North America Inc. Report of Analysis Page 2 of 2 Client Sample ID:TRIP BLANK Lab Sample ID:FA94246-6 Date Sampled:03/23/22 Matrix:AQ - Trip Blank Water Date Received:03/24/22 Method:SM 6200B Percent Solids:n/a Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l 100-41-4 Ethylbenzene ND 0.50 0.13 ug/l 87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l 74-83-9 Methyl Bromide ND 0.50 0.20 ug/l 74-87-3 Methyl Chloride ND 0.50 0.20 ug/l 74-95-3 Methylene Bromide ND 0.50 0.13 ug/l 75-09-2 Methylene Chloride ND 2.0 1.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l 91-20-3 Naphthalene ND 0.50 0.13 ug/l 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l 100-42-5 Styrene ND 0.50 0.13 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l 108-88-3 Toluene ND 0.50 0.13 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l 71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l 79-01-6 Trichloroethylene ND 0.50 0.13 ug/l 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l m,p-Xylene ND 1.0 0.13 ug/l 95-47-6 o-Xylene ND 0.50 0.13 ug/l 1330-20-7 Xylene (total)ND 1.5 0.25 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 102%70-130% 17060-07-0 1,2-Dichloroethane-D4 102%70-130% 2037-26-5 Toluene-D8 100%70-130% 460-00-4 4-Bromofluorobenzene 100%70-130% (a) No ECC available for this run. Insufficient sample available for reanalysis. (b) Associated Initial Calibration outside control limits (%RSD > 15%); sample is ND. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 19 of 39 FA9424633.6 SGS North America Inc. Misc. Forms Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody Orlando, FL Section 4 20 of 39 FA942464 FA94246: Chain of Custody Page 1 of 2 21 of 39 FA9424644.1 Job Number:FA94246 Client:GRI Date / Time Received:3/24/2022 9:30:00 AM Delivery Method:FX Project:EVERET'S ENTERPRISE Airbill #'s:100963793123 Cooler Information 1. Custody Seals Present 2. Custody Seals Intact 4. Cooler temp verification 3. Temp criteria achieved 5. Cooler media IR Gun Ice (Bag) Trip Blank Information 1. Trip Blank present / cooler 2. Trip Blank listed on COC 2. Samples preserved properly Sample Information 1. Sample labels present on bottles 5. Sample recvd within HT 4. Condition of sample 3. Sufficient volume/containers recvd for analysis: Intact Comments SM001Rev. Date 05/24/17 SGS Sample Receipt Summary Cooler Temps (Raw Measured) °C: Cooler Temps (Corrected) °C: Cooler 1: (4.0); Cooler 1: (4.4); 3. Type Of TB Received W or S N/A 6. Dates/Times/IDs on COC match Sample Label 7. VOCs have headspace 8. Bottles received for unspecified tests 9. Compositing instructions clear 10. Voa Soil Kits/Jars received past 48hrs? 11. % Solids Jar received? Misc. Information 25-Gram 5-GramNumber of Encores:Number of 5035 Field Kits:Number of Lab Filtered Metals: Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify) Y or N N/A Y or N Therm ID:IR 1; Therm CF:0.4; # of Coolers:1 Y or N N/A 12. Residual Chlorine Present? Residual Chlorine Test Strip Lot #: Technician:Reviewer:NATHANS Date:Date:3/24/2022 9:30:00 AM FA94246: Chain of Custody Page 2 of 2 22 of 39 FA9424644.1 SGS North America Inc. MS Volatiles QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries Orlando, FL Section 5 23 of 39 FA942465 Method Blank Summary Page 1 of 2 Job Number:FA94246 Account:GRINCC GRI (Geological Resources Inc.) Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VA3099-MB A0231322.D 1 03/30/22 SS n/a n/a VA3099 The QC reported here applies to the following samples:Method: SM 6200B FA94246-1 CAS No.Compound Result RL MDL Units Q 108-86-1 Bromobenzene ND 0.50 0.13 ug/l 74-97-5 Bromochloromethane ND 0.50 0.13 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l 75-25-2 Bromoform ND 0.50 0.13 ug/l 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane ND 0.50 0.20 ug/l 67-66-3 Chloroform ND 0.50 0.13 ug/l 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l 75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l 75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l 563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l 108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l 87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l 74-83-9 Methyl Bromide ND 0.50 0.20 ug/l 24 of 39 FA9424655.1.1 Method Blank Summary Page 2 of 2 Job Number:FA94246 Account:GRINCC GRI (Geological Resources Inc.) Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VA3099-MB A0231322.D 1 03/30/22 SS n/a n/a VA3099 The QC reported here applies to the following samples:Method: SM 6200B FA94246-1 CAS No.Compound Result RL MDL Units Q 74-87-3 Methyl Chloride ND 0.50 0.20 ug/l 74-95-3 Methylene Bromide ND 0.50 0.13 ug/l 75-09-2 Methylene Chloride ND 2.0 1.0 ug/l 100-42-5 Styrene ND 0.50 0.13 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l 71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l 79-01-6 Trichloroethylene ND 0.50 0.13 ug/l 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l CAS No.Surrogate Recoveries Limits 1868-53-7 Dibromofluoromethane 101%70-130% 17060-07-0 1,2-Dichloroethane-D4 107%70-130% 2037-26-5 Toluene-D8 102%70-130% 460-00-4 4-Bromofluorobenzene 105%70-130% 25 of 39 FA9424655.1.1 Method Blank Summary Page 1 of 1 Job Number:FA94246 Account:GRINCC GRI (Geological Resources Inc.) Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VA3104-MB A0231413.D 1 04/05/22 SS n/a n/a VA3104 The QC reported here applies to the following samples:Method: SM 6200B FA94246-1 CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.13 ug/l 100-41-4 Ethylbenzene ND 0.50 0.13 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l 91-20-3 Naphthalene 0.16 0.50 0.13 ug/l J 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l 108-88-3 Toluene ND 0.50 0.13 ug/l 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l m,p-Xylene ND 1.0 0.13 ug/l 95-47-6 o-Xylene ND 0.50 0.13 ug/l 1330-20-7 Xylene (total)ND 1.5 0.25 ug/l CAS No.Surrogate Recoveries Limits 1868-53-7 Dibromofluoromethane 101%70-130% 17060-07-0 1,2-Dichloroethane-D4 98%70-130% 2037-26-5 Toluene-D8 99%70-130% 460-00-4 4-Bromofluorobenzene 97%70-130% 26 of 39 FA9424655.1.2 Method Blank Summary Page 1 of 2 Job Number:FA94246 Account:GRINCC GRI (Geological Resources Inc.) Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VA3106-MB A0231448.D 1 04/06/22 SS n/a n/a VA3106 The QC reported here applies to the following samples:Method: SM 6200B FA94246-2, FA94246-3, FA94246-4, FA94246-5, FA94246-6 CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.13 ug/l 108-86-1 Bromobenzene ND 0.50 0.13 ug/l 74-97-5 Bromochloromethane ND 0.50 0.13 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l 75-25-2 Bromoform ND 0.50 0.13 ug/l 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane ND 0.50 0.20 ug/l 67-66-3 Chloroform ND 0.50 0.13 ug/l 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l 75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l 75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l 563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l 108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l 100-41-4 Ethylbenzene ND 0.50 0.13 ug/l 87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l 27 of 39 FA9424655.1.3 Method Blank Summary Page 2 of 2 Job Number:FA94246 Account:GRINCC GRI (Geological Resources Inc.) Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VA3106-MB A0231448.D 1 04/06/22 SS n/a n/a VA3106 The QC reported here applies to the following samples:Method: SM 6200B FA94246-2, FA94246-3, FA94246-4, FA94246-5, FA94246-6 CAS No.Compound Result RL MDL Units Q 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l 74-83-9 Methyl Bromide ND 0.50 0.20 ug/l 74-87-3 Methyl Chloride ND 0.50 0.20 ug/l 74-95-3 Methylene Bromide ND 0.50 0.13 ug/l 75-09-2 Methylene Chloride ND 2.0 1.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l 91-20-3 Naphthalene ND 0.50 0.13 ug/l 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l 100-42-5 Styrene ND 0.50 0.13 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l 108-88-3 Toluene ND 0.50 0.13 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l 71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l 79-01-6 Trichloroethylene ND 0.50 0.13 ug/l 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l m,p-Xylene ND 1.0 0.13 ug/l 95-47-6 o-Xylene ND 0.50 0.13 ug/l 1330-20-7 Xylene (total)ND 1.5 0.25 ug/l CAS No.Surrogate Recoveries Limits 1868-53-7 Dibromofluoromethane 101%70-130% 17060-07-0 1,2-Dichloroethane-D4 103%70-130% 2037-26-5 Toluene-D8 100%70-130% 460-00-4 4-Bromofluorobenzene 100%70-130% 28 of 39 FA9424655.1.3 Blank Spike Summary Page 1 of 2 Job Number:FA94246 Account:GRINCC GRI (Geological Resources Inc.) Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VA3099-BS A0231320.D 1 03/30/22 SS n/a n/a VA3099 The QC reported here applies to the following samples:Method: SM 6200B FA94246-1 Spike BSP BSP CAS No.Compound ug/l ug/l %Limits 108-86-1 Bromobenzene 10 9.7 97 70-130 74-97-5 Bromochloromethane 10 8.1 81 70-130 75-27-4 Bromodichloromethane 10 10 100 70-130 75-25-2 Bromoform 10 9.1 91 70-130 104-51-8 n-Butylbenzene 10 10.2 102 70-130 135-98-8 sec-Butylbenzene 10 11.8 118 70-130 98-06-6 tert-Butylbenzene 10 11.1 111 70-130 56-23-5 Carbon Tetrachloride 10 10.6 106 70-130 108-90-7 Chlorobenzene 10 9.7 97 70-130 75-00-3 Chloroethane 10 10.9 109 60-140 67-66-3 Chloroform 10 9.6 96 70-130 95-49-8 o-Chlorotoluene 10 10.6 106 70-130 106-43-4 p-Chlorotoluene 10 10.5 105 70-130 124-48-1 Dibromochloromethane 10 9.4 94 70-130 96-12-8 1,2-Dibromo-3-chloropropane 10 10.0 100 70-130 106-93-4 1,2-Dibromoethane 10 9.5 95 70-130 75-71-8 Dichlorodifluoromethane 10 10.5 105 60-140 95-50-1 1,2-Dichlorobenzene 10 9.9 99 70-130 541-73-1 1,3-Dichlorobenzene 10 10.0 100 70-130 106-46-7 1,4-Dichlorobenzene 10 9.6 96 70-130 75-34-3 1,1-Dichloroethane 10 10.2 102 70-130 107-06-2 1,2-Dichloroethane 10 9.8 98 70-130 75-35-4 1,1-Dichloroethylene 10 10.8 108 70-130 156-59-2 cis-1,2-Dichloroethylene 10 9.7 97 70-130 156-60-5 trans-1,2-Dichloroethylene 10 10.4 104 70-130 78-87-5 1,2-Dichloropropane 10 10.3 103 70-130 142-28-9 1,3-Dichloropropane 10 9.7 97 70-130 594-20-7 2,2-Dichloropropane 10 10.7 107 70-130 563-58-6 1,1-Dichloropropene 10 10.9 109 70-130 10061-01-5 cis-1,3-Dichloropropene 10 10.4 104 70-130 10061-02-6 trans-1,3-Dichloropropene 10 10.4 104 70-130 108-20-3 Di-Isopropyl Ether 10 9.4 94 70-130 87-68-3 Hexachlorobutadiene 10 10.5 105 70-130 98-82-8 Isopropylbenzene 10 10.8 108 70-130 99-87-6 p-Isopropyltoluene 10 10.7 107 70-130 74-83-9 Methyl Bromide 10 11.2 112 60-140 * = Outside of Control Limits. 29 of 39 FA9424655.2.1 Blank Spike Summary Page 2 of 2 Job Number:FA94246 Account:GRINCC GRI (Geological Resources Inc.) Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VA3099-BS A0231320.D 1 03/30/22 SS n/a n/a VA3099 The QC reported here applies to the following samples:Method: SM 6200B FA94246-1 Spike BSP BSP CAS No.Compound ug/l ug/l %Limits 74-87-3 Methyl Chloride 10 10.6 106 60-140 74-95-3 Methylene Bromide 10 9.1 91 70-130 75-09-2 Methylene Chloride 10 9.9 99 70-130 100-42-5 Styrene 10 9.6 96 70-130 630-20-6 1,1,1,2-Tetrachloroethane 10 10.1 101 70-130 79-34-5 1,1,2,2-Tetrachloroethane 10 10.3 103 70-130 127-18-4 Tetrachloroethylene 10 9.9 99 70-130 87-61-6 1,2,3-Trichlorobenzene 10 9.6 96 70-130 120-82-1 1,2,4-Trichlorobenzene 10 9.7 97 70-130 71-55-6 1,1,1-Trichloroethane 10 10.0 100 70-130 79-00-5 1,1,2-Trichloroethane 10 9.9 99 70-130 79-01-6 Trichloroethylene 10 10.2 102 70-130 75-69-4 Trichlorofluoromethane 10 14.7 147*60-140 96-18-4 1,2,3-Trichloropropane 10 9.6 96 70-130 75-01-4 Vinyl Chloride 10 10.8 108 60-140 CAS No.Surrogate Recoveries BSP Limits 1868-53-7 Dibromofluoromethane 100%70-130% 17060-07-0 1,2-Dichloroethane-D4 102%70-130% 2037-26-5 Toluene-D8 100%70-130% 460-00-4 4-Bromofluorobenzene 102%70-130% * = Outside of Control Limits. 30 of 39 FA9424655.2.1 Blank Spike Summary Page 1 of 1 Job Number:FA94246 Account:GRINCC GRI (Geological Resources Inc.) Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VA3104-BS A0231412.D 1 04/05/22 SS n/a n/a VA3104 The QC reported here applies to the following samples:Method: SM 6200B FA94246-1 Spike BSP BSP CAS No.Compound ug/l ug/l %Limits 71-43-2 Benzene 10 10.5 105 70-130 100-41-4 Ethylbenzene 10 10.7 107 70-130 1634-04-4 Methyl Tert Butyl Ether 10 9.4 94 70-130 91-20-3 Naphthalene 10 9.4 94 70-130 103-65-1 n-Propylbenzene 10 10 100 70-130 108-88-3 Toluene 10 10.5 105 70-130 95-63-6 1,2,4-Trimethylbenzene 10 9.6 96 70-130 108-67-8 1,3,5-Trimethylbenzene 10 10.0 100 70-130 m,p-Xylene 20 20.1 101 70-130 95-47-6 o-Xylene 10 9.8 98 70-130 1330-20-7 Xylene (total)30 29.9 100 70-130 CAS No.Surrogate Recoveries BSP Limits 1868-53-7 Dibromofluoromethane 103%70-130% 17060-07-0 1,2-Dichloroethane-D4 94%70-130% 2037-26-5 Toluene-D8 99%70-130% 460-00-4 4-Bromofluorobenzene 97%70-130% * = Outside of Control Limits. 31 of 39 FA9424655.2.2 Blank Spike Summary Page 1 of 2 Job Number:FA94246 Account:GRINCC GRI (Geological Resources Inc.) Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VA3106-BS A0231446.D 1 04/06/22 SS n/a n/a VA3106 The QC reported here applies to the following samples:Method: SM 6200B FA94246-2, FA94246-3, FA94246-4, FA94246-5, FA94246-6 Spike BSP BSP CAS No.Compound ug/l ug/l %Limits 71-43-2 Benzene 10 10.6 106 70-130 108-86-1 Bromobenzene 10 9.7 97 70-130 74-97-5 Bromochloromethane 10 8.9 89 70-130 75-27-4 Bromodichloromethane 10 9.7 97 70-130 75-25-2 Bromoform 10 7.9 79 70-130 104-51-8 n-Butylbenzene 10 10.6 106 70-130 135-98-8 sec-Butylbenzene 10 11.1 111 70-130 98-06-6 tert-Butylbenzene 10 10.6 106 70-130 56-23-5 Carbon Tetrachloride 10 10.2 102 70-130 108-90-7 Chlorobenzene 10 9.7 97 70-130 75-00-3 Chloroethane 10 12.3 123 60-140 67-66-3 Chloroform 10 9.7 97 70-130 95-49-8 o-Chlorotoluene 10 10.2 102 70-130 106-43-4 p-Chlorotoluene 10 10.1 101 70-130 124-48-1 Dibromochloromethane 10 8.9 89 70-130 96-12-8 1,2-Dibromo-3-chloropropane 10 8.7 87 70-130 106-93-4 1,2-Dibromoethane 10 9.4 94 70-130 75-71-8 Dichlorodifluoromethane 10 9.3 93 60-140 95-50-1 1,2-Dichlorobenzene 10 9.7 97 70-130 541-73-1 1,3-Dichlorobenzene 10 10 100 70-130 106-46-7 1,4-Dichlorobenzene 10 9.9 99 70-130 75-34-3 1,1-Dichloroethane 10 10.5 105 70-130 107-06-2 1,2-Dichloroethane 10 9.7 97 70-130 75-35-4 1,1-Dichloroethylene 10 10.9 109 70-130 156-59-2 cis-1,2-Dichloroethylene 10 10.2 102 70-130 156-60-5 trans-1,2-Dichloroethylene 10 10.6 106 70-130 78-87-5 1,2-Dichloropropane 10 10.1 101 70-130 142-28-9 1,3-Dichloropropane 10 9.4 94 70-130 594-20-7 2,2-Dichloropropane 10 10.6 106 70-130 563-58-6 1,1-Dichloropropene 10 10.9 109 70-130 10061-01-5 cis-1,3-Dichloropropene 10 10.2 102 70-130 10061-02-6 trans-1,3-Dichloropropene 10 10.2 102 70-130 108-20-3 Di-Isopropyl Ether 10 10.0 100 70-130 100-41-4 Ethylbenzene 10 10.2 102 70-130 87-68-3 Hexachlorobutadiene 10 10.5 105 70-130 98-82-8 Isopropylbenzene 10 10.6 106 70-130 * = Outside of Control Limits. 32 of 39 FA9424655.2.3 Blank Spike Summary Page 2 of 2 Job Number:FA94246 Account:GRINCC GRI (Geological Resources Inc.) Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VA3106-BS A0231446.D 1 04/06/22 SS n/a n/a VA3106 The QC reported here applies to the following samples:Method: SM 6200B FA94246-2, FA94246-3, FA94246-4, FA94246-5, FA94246-6 Spike BSP BSP CAS No.Compound ug/l ug/l %Limits 99-87-6 p-Isopropyltoluene 10 10.9 109 70-130 74-83-9 Methyl Bromide 10 11.1 111 60-140 74-87-3 Methyl Chloride 10 11.2 112 60-140 74-95-3 Methylene Bromide 10 8.9 89 70-130 75-09-2 Methylene Chloride 10 9.6 96 70-130 1634-04-4 Methyl Tert Butyl Ether 10 9.6 96 70-130 91-20-3 Naphthalene 10 9.2 92 70-130 103-65-1 n-Propylbenzene 10 10.5 105 70-130 100-42-5 Styrene 10 9.4 94 70-130 630-20-6 1,1,1,2-Tetrachloroethane 10 9.6 96 70-130 79-34-5 1,1,2,2-Tetrachloroethane 10 9.4 94 70-130 127-18-4 Tetrachloroethylene 10 10.0 100 70-130 108-88-3 Toluene 10 10.2 102 70-130 87-61-6 1,2,3-Trichlorobenzene 10 10 100 70-130 120-82-1 1,2,4-Trichlorobenzene 10 10 100 70-130 71-55-6 1,1,1-Trichloroethane 10 10.3 103 70-130 79-00-5 1,1,2-Trichloroethane 10 9.5 95 70-130 79-01-6 Trichloroethylene 10 10.3 103 70-130 75-69-4 Trichlorofluoromethane 10 9.2 92 60-140 96-18-4 1,2,3-Trichloropropane 10 9.2 92 70-130 95-63-6 1,2,4-Trimethylbenzene 10 10.5 105 70-130 108-67-8 1,3,5-Trimethylbenzene 10 10.7 107 70-130 75-01-4 Vinyl Chloride 10 9.7 97 60-140 m,p-Xylene 20 20.7 104 70-130 95-47-6 o-Xylene 10 10.4 104 70-130 1330-20-7 Xylene (total)30 31.1 104 70-130 CAS No.Surrogate Recoveries BSP Limits 1868-53-7 Dibromofluoromethane 99%70-130% 17060-07-0 1,2-Dichloroethane-D4 100%70-130% 2037-26-5 Toluene-D8 100%70-130% 460-00-4 4-Bromofluorobenzene 101%70-130% * = Outside of Control Limits. 33 of 39 FA9424655.2.3 Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2 Job Number:FA94246 Account:GRINCC GRI (Geological Resources Inc.) Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA94161-1MS A0231345.D 2000 03/30/22 SS n/a n/a VA3099 FA94161-1MSD A0231346.D 2000 03/30/22 SS n/a n/a VA3099 FA94161-1 A0231344.D 2000 03/30/22 SS n/a n/a VA3099 The QC reported here applies to the following samples:Method: SM 6200B FA94246-1 FA94161-1 Spike MS MS Spike MSD MSD Limits CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD 108-86-1 Bromobenzene ND 20000 20200 101 20000 20800 104 3 70-130/20 74-97-5 Bromochloromethane ND 20000 17200 86 20000 17300 87 1 70-130/20 75-27-4 Bromodichloromethane ND 20000 20700 104 20000 21300 107 3 70-130/20 75-25-2 Bromoform ND 20000 18800 94 20000 19700 99 5 70-130/20 104-51-8 n-Butylbenzene ND 20000 19700 99 20000 20700 104 5 70-130/20 135-98-8 sec-Butylbenzene ND 20000 23700 119 20000 25200 126 6 70-130/20 98-06-6 tert-Butylbenzene ND 20000 23100 116 20000 24100 121 4 70-130/20 56-23-5 Carbon Tetrachloride ND 20000 21600 108 20000 22500 113 4 70-130/20 108-90-7 Chlorobenzene ND 20000 20200 101 20000 20700 104 2 70-130/20 75-00-3 Chloroethane ND 20000 20200 101 20000 29300 147*37*60-140/20 67-66-3 Chloroform ND 20000 19600 98 20000 20100 101 3 70-130/20 95-49-8 o-Chlorotoluene ND 20000 21900 110 20000 22600 113 3 70-130/20 106-43-4 p-Chlorotoluene ND 20000 21300 107 20000 21800 109 2 70-130/20 124-48-1 Dibromochloromethane ND 20000 19600 98 20000 20200 101 3 70-130/20 96-12-8 1,2-Dibromo-3-chloropropane ND 20000 20500 103 20000 21300 107 4 70-130/20 106-93-4 1,2-Dibromoethane ND 20000 19800 99 20000 20700 104 4 70-130/20 75-71-8 Dichlorodifluoromethane ND 20000 18200 91 20000 21900 110 18 60-140/20 95-50-1 1,2-Dichlorobenzene ND 20000 20500 103 20000 20900 105 2 70-130/20 541-73-1 1,3-Dichlorobenzene ND 20000 20600 103 20000 21200 106 3 70-130/20 106-46-7 1,4-Dichlorobenzene ND 20000 19600 98 20000 20000 100 2 70-130/20 75-34-3 1,1-Dichloroethane ND 20000 21000 105 20000 21200 106 1 70-130/20 107-06-2 1,2-Dichloroethane ND 20000 20100 101 20000 20500 103 2 70-130/20 75-35-4 1,1-Dichloroethylene ND 20000 21600 108 20000 22100 111 2 70-130/20 156-59-2 cis-1,2-Dichloroethylene ND 20000 20500 103 20000 20900 105 2 70-130/20 156-60-5 trans-1,2-Dichloroethylene ND 20000 21200 106 20000 21300 107 0 70-130/20 78-87-5 1,2-Dichloropropane ND 20000 21100 106 20000 21700 109 3 70-130/20 142-28-9 1,3-Dichloropropane ND 20000 20200 101 20000 20600 103 2 70-130/20 594-20-7 2,2-Dichloropropane ND 20000 18600 93 20000 18900 95 2 70-130/20 563-58-6 1,1-Dichloropropene ND 20000 22300 112 20000 22800 114 2 70-130/20 10061-01-5 cis-1,3-Dichloropropene ND 20000 20800 104 20000 21500 108 3 70-130/20 10061-02-6 trans-1,3-Dichloropropene ND 20000 20600 103 20000 21200 106 3 70-130/20 108-20-3 Di-Isopropyl Ether ND 20000 19900 100 20000 20500 103 3 70-130/20 87-68-3 Hexachlorobutadiene ND 20000 20500 103 20000 22300 112 8 70-130/20 98-82-8 Isopropylbenzene ND 20000 22800 114 20000 23900 120 5 70-130/20 99-87-6 p-Isopropyltoluene ND 20000 21500 108 20000 22800 114 6 70-130/20 74-83-9 Methyl Bromide ND 20000 20100 101 20000 24700 124 21*60-140/20 * = Outside of Control Limits. 34 of 39 FA9424655.3.1 Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2 Job Number:FA94246 Account:GRINCC GRI (Geological Resources Inc.) Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA94161-1MS A0231345.D 2000 03/30/22 SS n/a n/a VA3099 FA94161-1MSD A0231346.D 2000 03/30/22 SS n/a n/a VA3099 FA94161-1 A0231344.D 2000 03/30/22 SS n/a n/a VA3099 The QC reported here applies to the following samples:Method: SM 6200B FA94246-1 FA94161-1 Spike MS MS Spike MSD MSD Limits CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD 74-87-3 Methyl Chloride ND 20000 20600 103 20000 24100 121 16 60-140/20 74-95-3 Methylene Bromide ND 20000 18600 93 20000 19100 96 3 70-130/20 75-09-2 Methylene Chloride ND 20000 20700 104 20000 20800 104 0 70-130/20 100-42-5 Styrene ND 20000 20100 101 20000 20900 105 4 70-130/20 630-20-6 1,1,1,2-Tetrachloroethane ND 20000 21100 106 20000 22000 110 4 70-130/20 79-34-5 1,1,2,2-Tetrachloroethane ND 20000 22500 113 20000 23400 117 4 70-130/20 127-18-4 Tetrachloroethylene ND 20000 20300 102 20000 21000 105 3 70-130/20 87-61-6 1,2,3-Trichlorobenzene ND 20000 19500 98 20000 20300 102 4 70-130/20 120-82-1 1,2,4-Trichlorobenzene ND 20000 19900 100 20000 20500 103 3 70-130/20 71-55-6 1,1,1-Trichloroethane ND 20000 21000 105 20000 21200 106 1 70-130/20 79-00-5 1,1,2-Trichloroethane ND 20000 20300 102 20000 21000 105 3 70-130/20 79-01-6 Trichloroethylene ND 20000 20500 103 20000 20400 102 0 70-130/20 75-69-4 Trichlorofluoromethane ND 20000 25000 125 20000 30600 153*20 60-140/20 96-18-4 1,2,3-Trichloropropane ND 20000 19800 99 20000 20100 101 2 70-130/20 75-01-4 Vinyl Chloride ND 20000 18600 93 20000 23000 115 21*60-140/20 CAS No.Surrogate Recoveries MS MSD FA94161-1 Limits 1868-53-7 Dibromofluoromethane 102%101%96%70-130% 17060-07-0 1,2-Dichloroethane-D4 104%99%102%70-130% 2037-26-5 Toluene-D8 101%101%102%70-130% 460-00-4 4-Bromofluorobenzene 104%104%104%70-130% * = Outside of Control Limits. 35 of 39 FA9424655.3.1 Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1 Job Number:FA94246 Account:GRINCC GRI (Geological Resources Inc.) Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA94208-6MS A0231428.D 100 04/05/22 SS n/a n/a VA3104 FA94208-6MSD A0231429.D 100 04/05/22 SS n/a n/a VA3104 FA94208-6 a A0231424.D 100 04/05/22 SS n/a n/a VA3104 The QC reported here applies to the following samples:Method: SM 6200B FA94246-1 FA94208-6 Spike MS MS Spike MSD MSD Limits CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD 71-43-2 Benzene 1180 1000 2230 105 1000 2210 103 1 70-130/20 100-41-4 Ethylbenzene 300 1000 1360 106 1000 1340 104 1 70-130/20 1634-04-4 Methyl Tert Butyl Ether ND 1000 928 93 1000 936 94 1 70-130/20 91-20-3 Naphthalene 149 B 1000 1070 92 1000 1080 93 1 70-130/20 103-65-1 n-Propylbenzene 18.7 J 1000 982 96 1000 977 96 1 70-130/20 108-88-3 Toluene 3490 1000 4370 88 1000 4350 86 0 70-130/20 95-63-6 1,2,4-Trimethylbenzene 230 1000 1200 97 1000 1180 95 2 70-130/20 108-67-8 1,3,5-Trimethylbenzene 56.1 1000 1030 97 1000 1030 97 0 70-130/20 m,p-Xylene 1010 2000 2960 98 2000 2930 96 1 70-130/20 95-47-6 o-Xylene 537 1000 1520 98 1000 1520 98 0 70-130/20 1330-20-7 Xylene (total)1540 3000 4480 98 3000 4440 97 1 70-130/20 CAS No.Surrogate Recoveries MS MSD FA94208-6 Limits 1868-53-7 Dibromofluoromethane 104%104%99%70-130% 17060-07-0 1,2-Dichloroethane-D4 97%96%98%70-130% 2037-26-5 Toluene-D8 100%100%100%70-130% 460-00-4 4-Bromofluorobenzene 97%96%98%70-130% (a) Sample re-analyzed beyond hold time; reported results are considered minimum values. * = Outside of Control Limits. 36 of 39 FA9424655.3.2 Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3 Job Number:FA94246 Account:GRINCC GRI (Geological Resources Inc.) Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA94326-1MS A0231461.D 2000 04/07/22 SS n/a n/a VA3106 FA94326-1MSD A0231462.D 2000 04/07/22 SS n/a n/a VA3106 FA94326-1 a A0231460.D 2000 04/06/22 SS n/a n/a VA3106 The QC reported here applies to the following samples:Method: SM 6200B FA94246-2, FA94246-3, FA94246-4, FA94246-5, FA94246-6 FA94326-1 Spike MS MS Spike MSD MSD Limits CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD 71-43-2 Benzene 19900 20000 37600 89 20000 40200 102 7 70-130/20 108-86-1 Bromobenzene ND 20000 17200 86 20000 19400 97 12 70-130/20 74-97-5 Bromochloromethane ND 20000 15900 80 20000 18100 91 13 70-130/20 75-27-4 Bromodichloromethane ND 20000 18100 91 20000 20000 100 10 70-130/20 75-25-2 Bromoform ND 20000 15200 76 20000 16400 82 8 70-130/20 104-51-8 n-Butylbenzene ND 20000 17800 89 20000 21000 105 16 70-130/20 135-98-8 sec-Butylbenzene ND 20000 19300 97 20000 22200 111 14 70-130/20 98-06-6 tert-Butylbenzene ND 20000 18400 92 20000 21200 106 14 70-130/20 56-23-5 Carbon Tetrachloride ND 20000 19400 97 20000 21300 107 9 70-130/20 108-90-7 Chlorobenzene ND 20000 17500 88 20000 19800 99 12 70-130/20 75-00-3 Chloroethane ND 20000 34600 173*20000 28500 143*19 60-140/20 67-66-3 Chloroform ND 20000 17800 89 20000 20100 101 12 70-130/20 95-49-8 o-Chlorotoluene ND 20000 18100 91 20000 20600 103 13 70-130/20 106-43-4 p-Chlorotoluene ND 20000 18200 91 20000 20400 102 11 70-130/20 124-48-1 Dibromochloromethane ND 20000 16600 83 20000 18500 93 11 70-130/20 96-12-8 1,2-Dibromo-3-chloropropane ND 20000 16000 80 20000 18100 91 12 70-130/20 106-93-4 1,2-Dibromoethane ND 20000 17400 87 20000 19500 98 11 70-130/20 75-71-8 Dichlorodifluoromethane ND 20000 15600 78 20000 20500 103 27*60-140/20 95-50-1 1,2-Dichlorobenzene ND 20000 16700 84 20000 19400 97 15 70-130/20 541-73-1 1,3-Dichlorobenzene ND 20000 17400 87 20000 20000 100 14 70-130/20 106-46-7 1,4-Dichlorobenzene ND 20000 17400 87 20000 19700 99 12 70-130/20 75-34-3 1,1-Dichloroethane ND 20000 19500 98 20000 21800 109 11 70-130/20 107-06-2 1,2-Dichloroethane ND 20000 18100 91 20000 20100 101 10 70-130/20 75-35-4 1,1-Dichloroethylene ND 20000 20600 103 20000 22800 114 10 70-130/20 156-59-2 cis-1,2-Dichloroethylene ND 20000 18500 93 20000 20900 105 12 70-130/20 156-60-5 trans-1,2-Dichloroethylene ND 20000 20000 100 20000 22200 111 10 70-130/20 78-87-5 1,2-Dichloropropane ND 20000 18600 93 20000 20600 103 10 70-130/20 142-28-9 1,3-Dichloropropane ND 20000 17200 86 20000 19200 96 11 70-130/20 594-20-7 2,2-Dichloropropane ND 20000 18200 91 20000 22600 113 22*70-130/20 563-58-6 1,1-Dichloropropene ND 20000 19900 100 20000 22300 112 11 70-130/20 10061-01-5 cis-1,3-Dichloropropene ND 20000 18800 94 20000 20900 105 11 70-130/20 10061-02-6 trans-1,3-Dichloropropene ND 20000 18600 93 20000 20700 104 11 70-130/20 108-20-3 Di-Isopropyl Ether 456 J 20000 18800 92 20000 20900 102 11 70-130/20 100-41-4 Ethylbenzene 3450 20000 22000 93 20000 24400 105 10 70-130/20 87-68-3 Hexachlorobutadiene ND 20000 16900 85 20000 20800 104 21*70-130/20 98-82-8 Isopropylbenzene ND 20000 19000 95 20000 21700 109 13 70-130/20 * = Outside of Control Limits. 37 of 39 FA9424655.3.3 Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3 Job Number:FA94246 Account:GRINCC GRI (Geological Resources Inc.) Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA94326-1MS A0231461.D 2000 04/07/22 SS n/a n/a VA3106 FA94326-1MSD A0231462.D 2000 04/07/22 SS n/a n/a VA3106 FA94326-1 a A0231460.D 2000 04/06/22 SS n/a n/a VA3106 The QC reported here applies to the following samples:Method: SM 6200B FA94246-2, FA94246-3, FA94246-4, FA94246-5, FA94246-6 FA94326-1 Spike MS MS Spike MSD MSD Limits CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD 99-87-6 p-Isopropyltoluene ND 20000 19000 95 20000 22100 111 15 70-130/20 74-83-9 Methyl Bromide ND 20000 32300 162*20000 25700 129 23*60-140/20 74-87-3 Methyl Chloride ND 20000 19000 95 20000 23200 116 20 60-140/20 74-95-3 Methylene Bromide ND 20000 16500 83 20000 18400 92 11 70-130/20 75-09-2 Methylene Chloride ND 20000 18800 94 20000 21000 105 11 70-130/20 1634-04-4 Methyl Tert Butyl Ether 11600 20000 29000 87 20000 31700 101 9 70-130/20 91-20-3 Naphthalene 424 J 20000 14100 68*20000 18100 88 25*70-130/20 103-65-1 n-Propylbenzene 309 J 20000 18800 92 20000 21300 105 12 70-130/20 100-42-5 Styrene ND 20000 17000 85 20000 19000 95 11 70-130/20 630-20-6 1,1,1,2-Tetrachloroethane ND 20000 17600 88 20000 20000 100 13 70-130/20 79-34-5 1,1,2,2-Tetrachloroethane ND 20000 19500 98 20000 19300 97 1 70-130/20 127-18-4 Tetrachloroethylene ND 20000 17900 90 20000 20300 102 13 70-130/20 108-88-3 Toluene 58600 20000 69200 53* b 20000 72700 71 5 70-130/20 87-61-6 1,2,3-Trichlorobenzene ND 20000 14400 72 20000 19800 99 32*70-130/20 120-82-1 1,2,4-Trichlorobenzene ND 20000 15000 75 20000 20000 100 29*70-130/20 71-55-6 1,1,1-Trichloroethane ND 20000 18600 93 20000 21000 105 12 70-130/20 79-00-5 1,1,2-Trichloroethane ND 20000 17500 88 20000 19500 98 11 70-130/20 79-01-6 Trichloroethylene ND 20000 17700 89 20000 21000 105 17 70-130/20 75-69-4 Trichlorofluoromethane ND 20000 17600 88 20000 21600 108 20 60-140/20 96-18-4 1,2,3-Trichloropropane ND 20000 16800 84 20000 18400 92 9 70-130/20 95-63-6 1,2,4-Trimethylbenzene 2300 20000 20700 92 20000 23500 106 13 70-130/20 108-67-8 1,3,5-Trimethylbenzene 745 J 20000 19500 94 20000 22300 108 13 70-130/20 75-01-4 Vinyl Chloride ND 20000 16800 84 20000 21500 108 25*60-140/20 m,p-Xylene 14900 40000 51800 92 40000 56600 104 9 70-130/20 95-47-6 o-Xylene 7080 20000 25400 92 20000 28200 106 10 70-130/20 1330-20-7 Xylene (total)22000 60000 77300 92 60000 84800 105 9 70-130/20 CAS No.Surrogate Recoveries MS MSD FA94326-1 Limits 1868-53-7 Dibromofluoromethane 105%100%97%70-130% 17060-07-0 1,2-Dichloroethane-D4 101%100%106%70-130% 2037-26-5 Toluene-D8 100%100%101%70-130% 460-00-4 4-Bromofluorobenzene 100%99%99%70-130% (a) No ECC available for this run. Insufficient sample available for reanalysis. * = Outside of Control Limits. 38 of 39 FA9424655.3.3 Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3 Job Number:FA94246 Account:GRINCC GRI (Geological Resources Inc.) Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA94326-1MS A0231461.D 2000 04/07/22 SS n/a n/a VA3106 FA94326-1MSD A0231462.D 2000 04/07/22 SS n/a n/a VA3106 FA94326-1 a A0231460.D 2000 04/06/22 SS n/a n/a VA3106 The QC reported here applies to the following samples:Method: SM 6200B FA94246-2, FA94246-3, FA94246-4, FA94246-5, FA94246-6 (b) Outside control limits due to high level in sample relative to spike amount. * = Outside of Control Limits. 39 of 39 FA9424655.3.3 APPENDIX C Contaminant Mass Calculations Area ID Well ID Area (ft²) Average Well Depth (ft.) Average Depth to Water (ft.) Water Column Height (ft) Volume (ft³) Volume (L) Effective Porosity Effective Volume (L) MW-2 MW-3 Area Date Well Benzene (μ/L) Toluene (μ/L) Ethylbenzene (μ/L) Xylenes (μ/L) MTBE (μ/L) Naphthalene (μ/L) Total (μ/L) DTW (ft.) Average Water Column Height (ft.) Total Average Mass (g)Percent Red.To Date Red. MW-2 3340.00 7650.00 1050.00 4960.00 1580.00 249.00 18829.00 5.26 MW-3 7700.00 26900.00 2970.00 15500.00 3670.00 621.00 57361.00 5.21 Avg.5520.00 17275.00 2010.00 10230.00 2625.00 435.00 38095.00 5.24 MW-2 7470.00 20400.00 2080.00 10920.00 1490.00 840.00 43200.00 4.34 MW-3 13400.00 24900.00 2920.00 15520.00 18100.00 1150.00 75990.00 4.45 Avg.10435.00 22650.00 2500.00 13220.00 9795.00 995.00 59595.00 4.40 MW-2 5760.00 13000.00 1270.00 9820.00 1790.00 472.00 FP 4.78 MW-3 5510.00 14700.00 1900.00 9660.00 2510.00 371.00 34651.00 4.78 Avg.5635.00 13850.00 1585.00 9740.00 2150.00 421.50 34651.00 4.78 MW-2 5060.00 15500.00 2370.00 11700.00 2270.00 626.00 37526.00 5.11 MW-3 3900.00 23600.00 3290.00 15600.00 0.00 611.00 47001.00 4.82 Avg.4480.00 19550.00 2830.00 13650.00 1135.00 618.50 42263.50 4.97 MW-2 3460 10100 1180 6260 1610 244 22854.00 4.93 MW-3 1480 14100 2430 11600 222.00 392 30224.00 4.94 Avg.2470.00 12100.00 1805.00 8930.00 916.00 318.00 26539.00 4.94 Date Average Water Column Height (ft.) 03/07/11 10.77 09/26/11 11.61 01/06/15 11.22 01/12/21 11.04 03/23/22 11.07 Notes: • FP: Free Product • Area of the contaminant plume is calculated from Figure 6. • Height of the water column is calculated by subtracting the average depth to water from the average well depth of the referenced monitoring wells • Volume of the contaminant plume is calculated by multiplying the area of the plume by the average height of the water column during each sampling event • Effective porosity is assumed based on the sub-surface soil profile obtained from well construction records and soil boring logs • Total mass was calculated by multiplying the total contaminant concentrations for the sampling event with effective volume • Contaminant mass cannot be calculated in wells containing FP; therefore, the total contaminant mass is based on the known concentrations in the area for each sampling event. • When areas couldn’t be sampled, the last known concentrations were used in the calculations. 28.4 03/23/22 11.07 5,828.89 37.0% 5.2416 28.4% 5,828.89 37.0%28.4% 9,257.37 -20.0%-13.7% 13728 -68.6%-68.6% 7,717 43.8%5.2% Total Contaminant Mass (g) Percent Reduction Compared to Previous Event Percent Reduction To Date 8,140 ------ -68.6%-68.6% 43.8%5.2% 01/12/21 11.04 9,257.37 -20.0%-13.7% 01/06/15 11.22 7,717.18 09/26/11 11.61 13,727.92 APPENDIX C CONTAMINANT MASS CALCULATIONS EVERETTE'S ENTERPRISES (INCIDENT NO. 11174) Baseline Event 03/02/11 10.77 8,140.14 ------ 3,504.9 0.201 213,5811,067,90437,71310.76 APPENDIX D AFVR Calculations and Disposal Manifest Site Name:11174 Extraction Well(s):2 6 Date :02/23/22 Start Time :8:47 End Time :16:10 Frequency (min)Time Vacuum (in. of Hg) Exhaust Velocity (ft/min) Temperature (°F) Rel. Humidity (%) OVA (ppm) 0 8:47 27.0 504.5 119.6 48.0 12.7 15 9:02 27.0 128.3 120.2 41.2 12.6 30 9:17 27.0 204.9 105.2 45.9 10.4 45 9:32 27.0 302.7 102.0 53.2 12.5 60 9:47 27.0 365.0 100.9 56.7 11.2 75 10:02 27.0 270.0 97.7 54.2 8.8 90 10:17 27.0 363.0 100.6 48.6 11.6 105 10:32 27.0 319.0 96.1 54.1 10.4 120 10:47 27.0 335.0 98.8 47.1 10.2 150 11:17 27.0 325.0 98.8 49.9 11.2 180 11:47 27.0 297.0 100.0 47.9 9.7 210 12:17 27.0 335.0 101.1 43.9 10.3 240 12:47 27.0 364.0 99.9 35.9 0.9 270 13:17 27.0 367.0 120.9 36.7 0.8 300 13:47 27.0 208.9 118.9 24.7 2.1 330 14:17 27.0 315.6 109.6 36.0 3.2 360 14:47 27.0 178.9 110.7 34.8 3.1 390 15:17 27.0 209.0 103.9 32.9 5.3 420 15:47 27.0 209.9 112.1 33.5 3.8 450 16:17 27.0 204.9 124.9 30.9 0.1 480 16:47 Total Fluids Recovered (in gallons) : Total Product Recovered (in gallons) : Note: Take all the readings listed below every 15 minutes for the first 2 hours of the AFVR and every 30 minutes thereafter. 680 cfm @18 in. of HgBlower Specifications For Vacuum Truck (e.g: 2500 cfm @ 24 in. of Hg): 0 AGGRESSIVE FLUID VAPOR RECOVERY EVENT - DATA SHEET Diameter of Exhaust Stack (inches) : Greenwood Applied Services Geological Resources, Inc. Test Conducted By (AFVR Contractor): Test Supervised By (Consultant): 2,576 Everette's Enterprises Incident Number: Inner Dia. of Well (inches):MW-2 & MW-24 Page 1 of 2 Site Name:11174 Extraction Well(s):2 6 Date :02/23/22 Start Time :8:47 End Time :16:10 680 cfm @18 in. of HgBlower Specifications For Vacuum Truck (e.g: 2500 cfm @ 24 in. of Hg): AGGRESSIVE FLUID VAPOR RECOVERY EVENT - DATA SHEET Diameter of Exhaust Stack (inches) : Greenwood Applied Services Geological Resources, Inc. Test Conducted By (AFVR Contractor): Test Supervised By (Consultant): Everette's Enterprises Incident Number: Inner Dia. of Well (inches):MW-2 & MW-24 AFVR Well Obs. Well 1 Obs. Well 2 Obs. Well 3 Obs. Well 4 Well Name MW-2 & MW-24 MW-1 MW-4 MW-11 Diameter (in.)2 2 2 2 Distance from AFVR Well (ft)0 Frequency (min)Time MW-2 & MW-24 MW-1 MW-4 MW-11 Pre AFVR 7:30 5.09 & 15.07 5.42 2.15 4.72 60 9:47 6.16 2.19 5.34 120 10:47 6.02 2.19 5.55 180 11:47 6.37 2.18 5.64 240 12:47 6.01 2.18 5.45 300 13:47 5.79 2.15 6.16 360 14:47 5.80 2.13 5.17 420 15:47 5.91 2.11 5.22 480 16:47 Post AFVR 15:30 5.32 & 15.07 5.68 2.12 5.09 Note: Record water levels in Vacuum Well at start and end of AFVR. Record Water Levels in a few Observation Wells periodically (hourly during event) and at end of event. Depth to Water Measurements (in feet) Page 2 of 2 Site Name:11174 Extraction Well(s):2 6 Date:Start Time:End Time : AIR FLOW CALCULATIONS Date Time Vacuum (in. Hg) Velocity (ft/min) Pipe ID (in.) Temp (°F) Rel Humid (%) Water Vapor (%) Flow (DSCFM) 8:47 27.0 505 6 119.6 48.0 0.0392 87 9:02 27.0 128 6 120.2 41.2 0.0343 22 9:17 27.0 205 6 105.2 45.9 0.0238 37 9:32 27.0 303 6 102.0 53.2 0.0249 54 9:47 27.0 365 6 100.9 56.7 0.0256 66 10:02 27.0 270 6 97.7 54.2 0.0220 49 10:17 27.0 363 6 100.6 48.6 0.0217 66 10:32 27.0 319 6 96.1 54.1 0.0209 58 10:47 27.0 335 6 98.8 47.1 0.0199 61 11:17 27.0 325 6 98.8 49.9 0.0210 59 11:47 27.0 297 6 100.0 47.9 0.0210 54 12:17 27.0 335 6 101.1 43.9 0.0199 61 12:47 27.0 364 6 99.9 35.9 0.0157 66 13:17 27.0 367 6 120.9 36.7 0.0312 63 13:47 27.0 209 6 118.9 24.7 0.0197 37 14:17 27.0 316 6 109.6 36.0 0.0214 56 14:47 27.0 179 6 110.7 34.8 0.0215 32 15:17 27.0 209 6 103.9 32.9 0.0163 38 15:47 27.0 210 6 112.1 33.5 0.0216 37 16:17 27.0 205 6 124.9 30.9 0.0298 35 16:47 27.0 290 6 107.1 42.8 0.0236 52 NOTES Qstd = (1-Water Vapor) * velocity * (PI * (diameter/24)^2) * (528°R/(Temp + 460)) (DSCFM) Vacuum = The level of vacuum being applied should be recorded from the vacuum truck tank (inches of Hg) Velocity = The rate at which air flows is measured at the blower discharge piping (anemometer or pitot tube) Pipe ID = The inside diameter of the blower discharge piping (from the vacuum truck) Temperature = The temperature of the air stream exiting the blower discharge piping (dry bulb temp., in deg.°F) Relative humidity = The % relative humidity of the air stream exiting the blower discharge piping Water Vapor in % = Pounds of water per pound of dry air, derived from the Psychrometric chart (temp Vs relative humidity) DSCFM = Dry Standard Cubic Feet Per Minute AGGRESSIVE FLUID VAPOR RECOVERY EVENT - CALCULATIONS Averages Everette's Enterprises Blower Specifications For Vacuum Truck (e.g: 2500 cfm @ 24 in. of Hg):680 cfm @18 in. of Hg Test Conducted By (AFVR Contractor): Test Supervised By (Consultant): Greenwood Applied Services Geological Resources, Inc. Diameter of Exhaust Stack (inches) : Inner Dia. of Well (inches):MW-2 & MW-24 Incident Number: 02/23/22 74Site Elevation (feet): 16:108:4702/23/22 Page 1 of 2 Site Name:11174 Extraction Well(s):2 6 Date:Start Time:End Time : AGGRESSIVE FLUID VAPOR RECOVERY EVENT - CALCULATIONS Everette's Enterprises Blower Specifications For Vacuum Truck (e.g: 2500 cfm @ 24 in. of Hg):680 cfm @18 in. of Hg Test Conducted By (AFVR Contractor): Test Supervised By (Consultant): Greenwood Applied Services Geological Resources, Inc. Diameter of Exhaust Stack (inches) : Inner Dia. of Well (inches):MW-2 & MW-24 Incident Number: 74Site Elevation (feet): 16:108:4702/23/22 EMISSION CALCULATIONS Elapsed Time (min) Flow (DSCFM) PPM measured (ppm) K (#C-gas)PPMg Cg:m (mg/dsm^3) Cg (lb/dscf) PMRg (lb/hr) PMR (lb) 0 87 12.7 4 50.8 270.15 0.00001687 0.09 0.00 15 22 12.6 4 50.4 268.02 0.00001673 0.02 0.01 30 37 10.4 4 41.6 221.22 0.00001381 0.03 0.01 45 54 12.5 4 50.0 265.89 0.00001660 0.05 0.01 60 66 11.2 4 44.8 238.24 0.00001487 0.06 0.01 75 49 8.8 4 35.2 187.19 0.00001169 0.03 0.01 90 66 11.6 4 46.4 246.75 0.00001540 0.06 0.02 105 58 10.4 4 41.6 221.22 0.00001381 0.05 0.01 120 61 10.2 4 40.8 216.97 0.00001355 0.05 0.01 150 59 11.2 4 44.8 238.24 0.00001487 0.05 0.03 180 54 9.7 4 38.8 206.33 0.00001288 0.04 0.02 210 61 10.3 4 41.2 219.09 0.00001368 0.05 0.02 240 66 0.9 4 3.6 19.14 0.00000120 0.00 0.00 270 63 0.8 4 3.2 17.02 0.00000106 0.00 0.00 300 37 2.1 4 8.4 44.67 0.00000279 0.01 0.00 330 56 3.2 4 12.8 68.07 0.00000425 0.01 0.01 360 32 3.1 4 12.4 65.94 0.00000412 0.01 0.00 390 38 5.3 4 21.2 112.74 0.00000704 0.02 0.01 420 37 3.8 4 15.2 80.83 0.00000505 0.01 0.01 450 35 0.1 4 0.4 2.13 0.00000013 0.00 0.00 480 Averages 52 7.5 4.00 30.18 160.49 0.00 0.03 0.01 Total emissions (gal):0.03 Total emissions (lbs):0.19 NOTES PPM measured = Actual measurements (ppm) taken with a OVA or TVA at the blower discharge piping K = Number of carbons in calibration gas: (Methane K = 1, or Propane K = 3, or Hexane K = 6) PPMg = PPMv, Volumetric concentration as gasoline emission, dry basis at STP Cg:m = mg/dsm3, mass concentration of gasoline emission Mg = 128 mg/mg-mole, molecular weight of gasoline (this value may vary depending on contaminant) K3 = 24.07 dsm^3/1E6 mg-mole, mass to volume conversion factor at STP Cg = lb/dcsf, mass concentration of gasoline emission, dry basis at STP PMRg = lb/hr, pollutant mass removal rate of gasoline emission PMR = pollutant mass removal of gasoline emission over time EQUATIONS PPMg = PPM measured * K Cg:m = PPMg * (Mg / K3) Cg = Cg:m * 62.43E-09 lb-m^3/mg-ft^3 PMRg = Cg * Qstd * 60 min/hr PMR = PMRg * ((T2 - T1) / 60) Total emmissions (gal) = Total emmissions (lbs)/6.25 Page 2 of 2