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HomeMy WebLinkAboutWA-813_11174_CA_MRP_20210202 3502 Hayes Road • Monroe, North Carolina 28110 113 West Firetower Road, Suite G • Winterville, North Carolina 28590 Phone (704) 845-4010 • (888) 870-4133 • Fax (704) 845-4012 February 3, 2021 Ms. Carrie Stone North Carolina Department of Environmental Quality Washington Regional Office 943 Washington Square Mall Washington, North Carolina 27889 Re: Ground Water Monitoring Report January 2020 Everette’s Enterprises 1101 Dr. Martin Luther King, Jr. Drive Ahoskie, Hertford County North Carolina Facility ID Number: 0-00-0000009694 Incident Number: 11174 GRI Project Number: 2459 Dear Ms. Stone, Please find enclosed the referenced report for the above mentioned site. If you have any questions, please contact William Regenthal at 704-845-4010. Sincerely, Geological Resources, Inc. Christa Benton Administrative Assistant Enclosure Cc: North East Oil Company, Inc., file 3502 Hayes Road • Monroe, North Carolina 28110 113 West Firetower Road, Suite G • Winterville, North Carolina 28590 Phone (704) 845-4010 • (888) 870-4133 • Fax (704) 845-4012 Ground Water Monitoring Report January 2021 Everette’s Enterprises 1101 Dr. Martin Luther King, Jr. Drive Ahoskie, Hertford County North Carolina Facility ID Number: 0-00-0000009694 Incident Number: 11174 GRI Project Number: 2459 Prepared for: North East Oil Company, Inc. Post Office Box 1386 Ahoskie, North Carolina 27910 February 2, 2021 William Regenthal, P. G. Project Manager Lisa Weathersby Report Writer ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: February 2, 2021 Everette’s Enterprises Project Manager: William Regenthal, P. G. GRI Project No. 2459 i SITE INFORMATION 1. Site Identification  Everette’s Enterprises (Facility ID 0-00-0000009694)  Incident Number 11174 – Intermediate Risk (I60R)  Location of Source Area: 1101 Dr. Martin Luther King, Jr. Drive Ahoskie, NC 27910 Hertford County 36.290639°N, 76.973306°W (Topographical Map) 2. Information about Contacts Associated with the Leaking UST System UST Owner North East Oil Company, Inc. Post Office Box 1386 Ahoskie, NC 27910 beah@bent-prises.com 252-862-0236 UST Operator North East Oil Company, Inc. Post Office Box 1386 Ahoskie, NC 27910 beah@bent-prises.com 252-862-0236 Property Owner Clyde W. Everett 414 Troy Street East Ahoskie, NC 27910 Email unknown Phone unknown Property Occupant Convenience Store 1101 Dr. Martin Luther King, Jr. Drive Ahoskie, NC 27910 Email unknown Phone unknown Consultant/Contractor Geological Resources, Inc. 3502 Hayes Road Monroe, NC 28110 wlr@geologicalresourcesinc.com 704-845-4010 Analytical Laboratory SGS- North America, Inc. 4405 Vineland Road, Suite C-15 Orlando, FL 32811 State Certification No. 573 407-425-6700 3. Information about Release  Release was discovered on September 1993  An unknown amount of product was released from the leaking UST System  Three 1,000-gallon USTs removed in September 1993 ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: February 2, 2021 Everette’s Enterprises Project Manager: William Regenthal, P. G. GRI Project No. 2459 ii EXECUTIVE SUMMARY The Everette's Enterprises convenience store is located at 1101 Dr. Martin Luther King, Jr. Drive in Ahoskie, Hertford County, North Carolina. The site is currently owned by Clyde W. Everette and is a convenience store. A release was discovered at the site when petroleum impacted soil was encountered during the September 1993 UST closure event. According to available information, three 1,000-gallon gasoline USTs were removed from the site in September 1993. According to the information determined during receptor survey activities, no water supply wells were identified within 1,500 feet of the source area during previous assessment activities. The site is located within a well head protection area. Municipal water is available to the site and surrounding properties within a 1,500-foot radius of the site. On January 12, 2021, ten Type II monitoring wells and two Type III monitoring wells were gauged, purged and sampled. Concentrations of individual BTEX constituents, MTBE, naphthalene, isopropylbenzene, n- propylbenzene, 1,2-dichloroethane, 1,2,4-trimethylbenzene and 1,3,5-trimethylbenzene that exceeded the Maximum Allowable Concentrations as specified in T15A NCAC 2L.0202 were reported in the ground water samples collected from MW-1, MW-2, MW-3, MW-13 and MWD-25. A concentration of benzene that exceeded the Gross Contamination Level (GCL) was reported in the ground water sample collected from MW-2. The estimated contaminant mass at the site has increased 13.7% since March 2011. Based on this information, the site should remain intermediate risk. GRI recommends that an Aggressive Fluid Vapor Recovery event should be conducted on MW-2 and MW-3 in order to reduce contaminant mass at the site. Ground water monitoring should continue with the next semi-annual ground water monitoring event tentatively scheduled for July 2021. ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: February 2, 2021 Everette’s Enterprises Project Manager: William Regenthal, P. G. GRI Project No. 2459 TABLE OF CONTENTS SITE INFORMATION ............................................................................................................................ i EXECUTIVE SUMMARY ....................................................................................................................... ii 1.0 SITE HISTORY AND CHARACTERIZATION ...................................................................................1 2.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL ASSESSMENT INFORMATION ...................................................................................................2 3.0 FREE PRODUCT REMOVAL ........................................................................................................4 4.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS ..................................4 5.0 CONCLUSIONS .........................................................................................................................5 6.0 LIMITATIONS ...........................................................................................................................5 7.0 STATEMENTS AND CERTIFICATION ...........................................................................................5 FIGURES Figure 1: Site Location Map Figure 2: Site Vicinity Map Figure 3: Site Map Figure 4: Ground Water Flow Map Figure 5: Ground Water Quality Map Figure 6: Benzene Isoconcentration Map Figure 7: Contaminant Mass Area Map TABLES Table 1: UST Owner and Operator Information Table 2: UST System Information Table 3: Adjacent Property Owner Information Table 4: Well Construction and Gauging Information Table 5: Summary of Ground Water Sample Analytical Results Table 5A: Summary of Field Parameters Results APPENDICES Appendix A: State Correspondence Appendix B: Property Cards Appendix C: Laboratory Report – Ground Water Samples Appendix D: Contaminant Mass Calculations ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: February 2, 2021 Everette’s Enterprises Project Manager: William Regenthal, P. G. GRI Project No. 2459 1 1.0 SITE HISTORY AND CHARACTERIZATION Geological Resources, Inc. (GRI) presents the results of the January 2021 updated receptor survey and ground water sampling event at the Everette’s Enterprises site; located at 1101 Dr. Martin Luther King, Jr. Drive in Ahoskie, Hertford County, North Carolina (Figure 1). These activities were conducted in accordance with GRI Proposal No. 20-712, which was submitted to the North Carolina Department of Environmental Quality (NCDEQ) on December 14, 2020, and was approved as Task Authorization No. 11174-28 on January 5, 2021. State correspondence has been included as Appendix A. The site is currently owned by Clyde W. Everette and is a convenience store. According to available information, three 1,000-gallon gasoline USTs were removed from the site in September 1993. A release was discovered at the site when petroleum impacted soil was encountered during the September 1993 UST closure event. UST owner/operator information and UST system information are included as Tables 1 and 2, respectively. The Registered Tank Report is shown below: The site and surrounding area are a mixture of residential and agricultural properties. The site is an active convenience store and is primarily capped with concrete. The overall topography at the site is relatively flat. Eighteen Type II monitoring wells (MW-1 through MW-4, MW-6 through MW-8 and MW-10 through MW-20) and two vertical extent ground water monitoring wells (MWD-5 and MWD-9) were installed at the site during previous ground water assessment activities conducted by CES Engineering, PC, between 1993 and 1995. Monitoring wells MW-21 through MW-23 were installed under the supervision of GRI in October 2012. Monitoring wells MWD-24 and MWD-25 were installed under the supervision of GRI in August 2013. On January 12, 2021, receptor information was updated for the site. No water supply wells were identified within 1,500 feet of the source area. No surface water bodies were identified within a 500-foot radius of the site. The site is located within the designated wellhead protection area for the Town of Ahoskie. Municipal water is available to the site and surrounding properties. Adjacent property owner information is presented in Table 3. A Site Vicinity Map showing the locations of adjacent properties has been included ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: February 2, 2021 Everette’s Enterprises Project Manager: William Regenthal, P. G. GRI Project No. 2459 2 as Figure 2. A Site Map showing the locations of the monitoring wells and the structures on-site has been included as Figure 3. Property cards for the site and adjacent properties are included as Appendix B. A Corrective Action Plan (CAP) proposing removal of free product using a pump and treat system followed by natural attenuation was completed for the site in August 1996. Initially, the CAP was not approved when it was submitted in 1996 since the site was ranked low risk. The site was re-ranked intermediate risk in September 1998 and a CAP Addendum was completed in 2001. To date, the CAP has not been implemented. 2.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL ASSESSMENT INFORMATION On January 12, 2021, ten Type II monitoring wells (MW-1 through MW-4, MW-7, WM-8, and MW-10 through MW-13) and two Type III monitoring wells (MWD-24 and MWD-25) were gauged, purged and sampled. Depths to ground water in the Type II monitoring wells ranged from 0.99 feet to 6.62 feet. Ground water elevations in the Type II monitoring wells ranged from 92.24 feet to 98.21 feet. Ground water flow was generally toward the southwest with an average hydraulic gradient of approximately 0.06 feet per foot. The average vertical gradient between paired wells MW-3 and MWD-24 was approximately 0.25 feet per foot downward. Well construction and gauging information is presented in Table 5. A Ground Water Flow Map is included as Figure 4. A summary of the current ground water gauging data is shown below: Well ID Screened Interval (x to y ft. BGS) Bottom of Well (ft. BGS) Top of Casing Elevation (ft.) Depth to Water from Top of Casing (feet) Free Product Thickness (ft.) Ground Water Elevation (ft.) MW-1 6 - 16 16 100.00 4.92 --- 95.08 MW-2 6 - 16 16 99.63 5.11 --- 94.52 MW-3 6 - 16 16 99.54 4.82 94.72 MW-4 4 - 14 14 99.20 0.99 98.21 MW-7 4 - 14 14 100.20 4.90 95.30 MW-8 6 - 16 16 99.59 4.59 95.00 MW-10 6 - 16 16 99.91 4.89 95.02 MW-11 6 - 16 16 99.11 5.12 93.99 MW-12 6 - 16 16 98.98 5.23 93.75 MW-13 6 - 16 16 98.86 6.62 92.24 MWD-24 45 - 50 50 99.91 14.12 --- 85.79 MWD-25 45 - 50 50 99.07 13.15 --- 85.92 Ground water samples collected from the monitoring wells were submitted for laboratory analyses using EPA Method 6200B. Concentrations of individual BTEX constituents, MTBE, naphthalene, isopropylbenzene, n-propylbenzene, 1,2-dichloroethane, 1,2,4-trimethylbenzene and 1,3,5- trimethylbenzene that exceeded the Maximum Allowable Concentrations (MACs) as specified in T15A NCAC 2L.0202 were reported in the ground water samples collected from MW-1, MW-2, MW-3, MW-13 and MWD-25. A concentration of benzene that exceeded the Gross Contamination Level (GCL) was reported in the ground water sample collected from MW-2. A summary of the analytical results for ground ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: February 2, 2021 Everette’s Enterprises Project Manager: William Regenthal, P. G. GRI Project No. 2459 3 water samples collected on January 12, 2021, is presented in Table 6. A Ground Water Quality Map based on the January 2021 data is included as Figure 5. A contaminant specific isoconcentration map for benzene is included as Figure 6. A complete report of laboratory analyses of the ground water samples collected from the monitoring wells during the January 2021 sampling event has been included as Appendix C. A summary of the current ground water analytical data is shown below: Contaminant of Concern  Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene Well ID MACs (mg/l) 1 600 600 500 20 6 GCL (mg/l) 5,000 260,000 84,500 85,500 20,000 6,000 MW-1 937 7,010 1,100 7,120 <25 374 MW-2 5,060 15,500 2,370 11,700 2,270 626 MW-3 3,900 23,600 3,290 15,600 <63 611 MW-4 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 MW-7 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 MW-8 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 MW-10 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 MW-11 <0.13 <0.13 <0.13 <0.25 14.2 0.23 J MW-12 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 MW-13 104 <0.31 4.2 10.7 106 17.5 MWD-24 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 MWD-25 <0.31 <0.31 <0.31 <0.63 107 <0.31 The baseline contaminant mass at the site was determined based on the total BTEX, MTBE and naphthalene concentrations from the March 2011 ground water sampling event, as well as the maximum historical water column height observed in each area. The contaminant plume consists of one area of concern (Area 1) based on the benzene concentrations during the March 2011 ground water sampling event. The contaminant mass has increased by 13.7% since March 2011. Contaminant mass calculations have been included as Appendix D. A map of the contaminant mass area has been included as Figure 7. A chart depicting the overall trend in contaminant mass is shown below: ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: February 2, 2021 Everette’s Enterprises Project Manager: William Regenthal, P. G. GRI Project No. 2459 4 A Corrective Action Plan (CAP) proposing removal of free product using a pump and treat system was completed for the site in August 1996. To date, the CAP has not been implemented. No contaminant reduction milestones were established in the CAP. The site is located in the Coastal Plain Physiographic Province of North Carolina. The seasonal high depth to water is approximately 0.5 to 8 feet below ground surface (bgs). 3.0 FREE PRODUCT REMOVAL Free product has been observed at the site during past ground water gauging events. Between January 2011 and February 2014, five Mobile Multi Phase Extraction (MMPE) events have been conducted at the site. A total of 66,486 gallons of petroleum impacted ground water was recovered by the MMPE events conducted between January 2011 and February 2014. A total of 125.48 gallons of vapor phase free product has been recovered during the MMPE events. No free product has been observed at the site since August 2013. 4.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS No natural attenuation monitoring plan is currently in place at the site. ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: February 2, 2021 Everette’s Enterprises Project Manager: William Regenthal, P. G. GRI Project No. 2459 5 5.0 CONCLUSIONS  On January 12, 2021, receptor information was updated for the site. No water supply wells were observed within a 1,500-foot radius of the site. No surface water bodies were observed within a 500-foot radius of the site. The site lies within the designated wellhead protection area for the Town of Ahoskie.  On January 12, 2021, ten Type II monitoring wells and two Type III monitoring wells were gauged, purged and sampled. Ground water flow was generally toward the southwest with a horizontal gradient of approximately 0.06 feet per foot. The average vertical gradient between paired wells MW-3 and MWD-24 was approximately 0.25 feet per foot downward.  Concentrations of individual BTEX constituents, MTBE, naphthalene, isopropylbenzene, n- propylbenzene, 1,2-dichloroethane, 1,2,4-trimethylbenzene and 1,3,5-trimethylbenzene that exceeded the MACs were reported in the reported in the ground water samples collected from MW-1, MW-2, MW-3, MW-13 and MWD-25. A concentration of benzene that exceeded the GCL was reported in the ground water sample collected from MW-2.  Contaminant mass has increased by 13.7% at the site since March 2011.  Based on this information, the site should remain intermediate risk. GRI recommends that an Aggressive Fluid Vapor Recovery event should be conducted on MW-2 and MW-3 in order to reduce contaminant mass at the site. Ground water monitoring should continue with the next semi-annual ground water monitoring event tentatively scheduled for July 2021. 6.0 LIMITATIONS This report has been prepared for the exclusive use of North East Oil Company, Inc. for specific application to the referenced site in Hertford County, North Carolina. The assessment was conducted based on the scope of work and level of effort desired by NCDEQ and with resources adequate only for that scope of work. Our findings have been developed in accordance with generally accepted standards of environmental practices in the State of North Carolina, available information, and our professional judgment. No other warranty is expressed or implied. The data that are presented in this report are indicative of conditions that existed at the precise locations sampled and at the time the samples were collected. In addition, the data obtained from samples would be interpreted as being meaningful with respect to parameters indicated in the laboratory report. No additional information can logically be inferred from these data. 7.0 STATEMENTS AND CERTIFICATION 1 Enter the date the monitoring report was due. N/A Will this report be submitted after the established due date? YES NO 2 Was any required information from the above template missing from this report? YES NO IF the answer to question #1 or# 2 is “YES”, please provide additional information in this cell to explain what was missing and why. FIGURES SITE5993-70-2836 599 3-70-47625993-70-4927 5993-70-48285993-70-4980 D R . M A R T IN L U T H E R K IN G JR . D R IV ECATHERINE STREETMAPLE STREETTROY STREET MALIBU DRIVE MONOCO DRIVE DAVIS STREET PINE STREETSTATON AVENUE BAKER STREET G E R O CK STR E ET WILLIA M S STR EET M A N L EY AV E N U E TOWN OF AHOSKIE N E W S O M E S T R E E TPORTER S TR EETPATTERSON AVENUE H A RT S T R E E T CATHERINE CREEK ROADT RO Y S T R E E T TOWN OF AHOSKIESNIPES AVENUE H O LLO M A N AVENUE RHUE STREETHILL STREETALTON STREET ALTON STREET ROGERS STREET RICHARD STREET LASHLEY AVENUEFIGURE 2: SITE VICINITY MAPEVERETTE'S ENTERPRISES1101 N. CATHERINE CREEK ROADAHOSKIE, HERTFORD COUNTYNORTH CAROLINAINCIDENT NO. 11174GRI PROJECT NO. 2459 PREPARED BY:GEOLOGICAL RESOURCES, INC.JANUARY 22, 2021 ³ 0 300150Feet1 inch = 300 feet 1,500-FOOT RADIUS 500-FOOT RADIUS 1,000-FOOT RADIUS 250-FOOT RADIUS LEGEND Centerlines Hydrology Adjacent Properties nc_hertford_parcels_poly TABLES UST ID Number 1-3 Facility ID Number Owner or Operator? OwnerET One, Inc.05/07/1964 - 09/09/1993 Address Telephone Number Post Office Box 1386, Ahoskie, NC 27910 252-862-0236 Name of Owner or Operator Dates of Ownership / Operation TABLE 1 UST OWNER/OPERATOR INFORMATION EVERETTE'S ENTERPRISES (INCIDENT NO. 11174) 00-0-0000009694 Page 1 of 1 Date: 02/02/2021 Was Release Associated with UST System? (Yes / No) 1 Gasoline Gasoline 1,000 05/07/1964 Single Wall Steel Unknown Unknown Removed (09/09/93)Yes 2 Gasoline Gasoline 1,000 05/07/1964 Single Wall Steel Unknown Unknown Removed (09/09/93)Yes 3 Gasoline Gasoline 1,000 05/07/1964 Single Wall Steel Unknown Unknown Removed (09/09/93)Yes Tank Dimensions Description of Associated Product Piping and Pumps Status of UST TABLE 2 UST SYSTEM INFORMATION EVERETTE'S ENTERPRISES (INCIDENT NO. 11174) Facility ID #: 00-0-0000009694 UST ID No. Current or Most Recent Contents Previous Contents Capacity (gallons) Date Installed Construction Details Page 1 of 1 Date: 01/27/2021 Facility ID #: 00-0-0000009694 5993-70-4828 (site)Clyde W. Everett 414 Troy Street E Ahoskie, North Carolina 27910 5993-70-2836 C W Jones Heirs Post Office Box 368 Ahoskie, North Carolina 27910 5993-70-4927 County of Hertford 115 Justice Drive, Suite #1 Winton, North Carolina 27986 5993-70-4762 Keely P. Holley 1490 Hartford Terrace Alpharetta, Georgia 30004 5993-70-4980 Travis Harrell 106 Blacksmith Drive Ahoskie, North Carolina 27910 • Properties are keyed to Figure 3. • This information is based on the Hertford County GIS website. TABLE 3 ADJACENT PROPERTY OWNER INFORMATION EVERETTE'S ENTERPRISES (INCIDENT NO. 11174) PIN Number Property Owner Name Mailing Address Date: 01/27/2021 Facility ID # : 00-0-0000009694 03/07/11 5.56 44.37 09/26/11 4.68 45.25 11/01/12 4.27 95.73 09/18/13 NM NM 04/03/14 5.12 94.88 01/06/15 5.20 94.80 01/12/21 4.92 95.08 03/07/11 5.26 42.91 09/26/11 4.37 43.80 11/01/12 3.96 95.67 09/18/13 7.62 92.01 04/03/14 4.95 94.68 01/06/15 4.78 94.85 01/12/21 5.11 94.52 03/07/11 5.21 42.90 09/26/11 4.45 43.66 11/01/12 3.97 95.57 09/18/13 7.71 91.83 04/03/14 4.66 94.88 01/06/15 4.78 94.76 01/12/21 4.82 94.72 03/07/11 2.04 45.70 09/26/11 0.79 46.95 11/01/12 0.57 98.63 09/18/13 8.67 90.53 04/03/14 3.84 95.36 01/06/15 3.50 95.70 01/12/21 0.99 98.21 03/07/11 14.79 33.53 09/26/11 15.67 32.65 11/01/12 14.93 84.87 09/18/13 15.71 84.09 04/03/14 NM NM Not found 01/06/15 NM NM Under cement pad 03/07/11 4.45 43.57 09/26/11 2.45 45.57 11/01/12 0.80 98.64 09/18/13 NM NM 04/03/14 NM NM 01/06/15 0.82 98.62 03/07/11 5.69 43.12 09/26/11 4.65 44.16 11/01/12 4.26 95.94 09/18/13 8.21 91.99 04/03/14 5.06 95.14 01/06/15 5.15 95.05 01/12/21 4.90 95.30 03/07/11 5.11 43.04 09/26/11 4.24 43.91 11/01/12 3.52 96.07 09/18/13 7.52 92.07 04/03/14 4.77 94.82 01/06/15 4.67 94.92 01/12/21 4.59 95.00 03/07/11 15.47 32.72 09/26/11 16.40 31.79 11/01/12 15.75 83.90 09/18/13 16.60 83.05 04/03/14 14.74 84.91 01/06/15 NM NM Under cement pad 03/07/11 5.33 43.14 09/26/11 4.83 43.64 11/01/12 4.07 95.84 09/18/13 7.88 92.03 04/03/14 NM NM 01/06/15 4.97 94.94 01/12/21 4.89 95.02 MW-1 11/04/93 6 MW-10 06/02/95 6 6-16 16 99.91 99.44 14404/22/94MW-6 4-14 4540-454006/01/95MWD-9 48.19 99.59 16 Comments TABLE 4 WELL CONSTRUCTION AND GAUGING INFORMATION EVERETTE'S ENTERPRISES (INCIDENT NO. 11174) Well ID Date Installed (mm/dd/yy) Date Water Level Measured (mm/dd/yy) Screened Interval (x to y ft. BGS) Top of Casing Elevation* (ft.) Depth to Water from Top of Casing (ft.) Free Product Thickness (ft.) Groundwater Elevation (ft.) Well Casing Depth (ft. BGS) Bottom of Well (ft. BGS) 0.00 0.00 0.00 48.32 99.80 99.65 48.81 48.02 48.47 48.15 MW-2 11/04/93 47.74 3530-353004/21/94MWD-5 MW-8 MW-4 404/20/94 MW-7 04/22/94 4 4-14 14 100.20 14 99.20 MW-3 11/04/93 6 6-16 99.54 16 4-14 48.11 6-16 16 100.00 6 6-16 16 99.63 49.93 48.17 6-16605/31/95 0.00 0.00 0.00 0.00 0.00 0.00 0.00 Page 1 of 3 Date: 01/27/2021 Facility ID # : 00-0-0000009694 Comments TABLE 4 WELL CONSTRUCTION AND GAUGING INFORMATION EVERETTE'S ENTERPRISES (INCIDENT NO. 11174) Well ID Date Installed (mm/dd/yy) Date Water Level Measured (mm/dd/yy) Screened Interval (x to y ft. BGS) Top of Casing Elevation* (ft.) Depth to Water from Top of Casing (ft.) Free Product Thickness (ft.) Groundwater Elevation (ft.) Well Casing Depth (ft. BGS) Bottom of Well (ft. BGS) 03/07/11 4.78 42.87 09/26/11 5.85 41.80 11/01/12 3.93 95.18 09/18/13 7.24 91.87 04/03/14 4.24 94.87 01/06/15 4.78 94.33 01/12/21 5.12 93.99 03/07/11 8.25 39.25 09/26/11 8.80 38.70 11/01/12 6.06 92.92 09/18/13 10.10 88.88 04/03/14 6.05 92.93 01/06/15 7.41 91.57 01/12/21 5.23 93.75 09/26/11 47.39 9.55 37.84 10/29/12 7.78 91.08 09/18/13 11.85 87.01 04/03/14 6.96 91.90 01/06/15 7.41 91.45 01/12/21 6.62 92.24 03/07/11 8.51 39.23 09/26/11 8.95 38.79 11/01/12 6.17 93.03 09/18/13 9.66 89.54 04/03/14 5.81 93.39 01/06/15 7.48 91.72 03/07/11 8.13 39.72 09/26/11 8.37 39.48 11/01/12 5.89 93.42 09/18/13 NM NM 04/03/14 NM NM 01/06/15 7.64 91.67 03/07/11 7.75 39.42 09/26/11 0.76 46.41 11/01/12 0.58 98.14 09/18/13 9.56 89.16 04/03/14 NM NM 01/06/15 0.83 97.89 09/26/11 47.63 3.60 44.03 11/01/12 4.14 94.96 09/18/13 7.57 91.53 04/03/14 3.55 95.55 01/06/15 3.24 95.86 03/07/11 8.79 38.61 09/26/11 4.72 42.68 11/01/12 3.02 95.87 09/18/13 NM NM 04/03/14 NM NM 01/06/15 5.04 93.85 03/07/11 10.43 38.01 09/26/11 10.95 37.49 11/01/12 9.26 90.69 09/18/13 NM NM 04/03/14 NM NM Not found 01/06/15 9.42 90.53 11/01/12 6.01 93.15 09/18/13 10.31 88.85 04/03/14 5.88 93.28 01/06/15 7.33 91.83 11/01/12 6.71 92.41 09/18/13 10.03 89.09 04/03/14 NM NM 01/06/15 7.41 91.71 11/01/12 6.65 92.60 09/18/13 9.97 89.28 04/03/14 6.05 93.20 01/06/15 7.43 91.82 MW-11 06/05/95 99.11 166-166 10/15/12MW-22 99.16165.5-165.5 47.50 47.74 47.85 06/05/95 47.17 98.72 13309/13/95MW-16 3-13 48.44 5.5-155.5 309/13/95MW-17 99.95 155-15509/13/95MW-20 98.89 133-13309/13/95MW-18 99.10133-13 47.40 10/15/12MW-21 5.5-165.510/15/12MW-23 15 0.00 0.00 0.00 0.00 0.00 99.25 99.12 99.20 47.65 99.31 98.98 16 16 0.00 0.00 0.00 0.00 6-16606/07/95MW-15 166-166MW-14 06/05/95 6 6-16 16 98.86 0.00 0.00 0.00 MW-12 06/05/95 6 6-16 16 MW-13 Page 2 of 3 Date: 01/27/2021 Facility ID # : 00-0-0000009694 Comments TABLE 4 WELL CONSTRUCTION AND GAUGING INFORMATION EVERETTE'S ENTERPRISES (INCIDENT NO. 11174) Well ID Date Installed (mm/dd/yy) Date Water Level Measured (mm/dd/yy) Screened Interval (x to y ft. BGS) Top of Casing Elevation* (ft.) Depth to Water from Top of Casing (ft.) Free Product Thickness (ft.) Groundwater Elevation (ft.) Well Casing Depth (ft. BGS) Bottom of Well (ft. BGS) 09/18/13 16.86 83.05 04/03/14 15.01 84.90 01/06/15 16.15 83.76 01/12/21 14.12 85.79 09/18/13 16.84 82.23 04/03/14 14.02 85.05 01/06/15 15.10 83.97 01/12/21 13.15 85.92 Notes: • * : Reference point for elevation measurements; assumed elevation 100.00 ft. • ft BGS : feet below ground surface. • NM: Not measured. • Top of Casing information obtained from January 19, 2012, survey completed by Roanoke Land Surveying and reproduced from reports prepared by CES Engineering, PC. 99.91MWD-24 08/21/13 45 45-50 50 MWD-25 08/21/13 45 45-50 50 99.07 0.00 0.00 Page 3 of 3 Date: 01/21/2021 Facility ID #: 0-009694 EPA Method 6010B/3030C 1 600 600 500 20 6 70 70 70 400 400 15 400 700 10,000 200 5,000 260,000 84,500 85,500 20,000 6,000 6,900 25,000 30,000 28,500 25,000 15,000 NE NE NE NE 03/02/11 1,630 6,890 1,160 6,950 224 401 124 J 109 J 275 2,220 583 NR NR NR NR NR 09/26/11 2,170 11,600 1,490 9,390 115 J 698 35.2 J 102 J 241 2,380 599 NR NR NR NR NR 11/01/12 1,340 10,600 1,350 8,580 42.5 J 514 25.4 J 57.3 J 171 1,990 457 NR NR NR NR NR 09/18/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 04/03/14 1,350 9,140 1,700 9,690 60.9 J 435 28.7 J 100 J 300 2,370 660 NR NR NR NR NR 01/06/15 2,030 12,700 1,970 11,300 102 470 29.5 J 124 251 2,780 546 NR NR NR NR NR 01/12/21 937 7,010 1,100 7,120 <25 374 <25 60.0 J 140 1,950 578 NR NR NR NR NR 03/02/11 3,340 7,650 1,050 4,960 1,580 249 67.4 J 70.9 J 171 J 1,050 286 NR NR NR NR NR 09/26/11 7,470 20,400 2,080 10,920 1,490 840 35.4 121 301 2,370 584 NR NR NR NR NR 11/01/12 5,630 21,900 1,790 10,100 938 513 <50 70.6 J 226 J 1,670 393 NR NR NR NR NR 09/18/13 4,290 12,600 1,060 5,970 1,480 296 <10 40.1 J 118 958 214 21.2 15,100 2,782 J <100 4,422 J 04/03/14 1,580 4,390 555 4,200 391 485 20.4 J 40.3 J 113 1,090 286 NR NR NR NR NR 01/06/15 5,760 13,000 1,270 9,820 1,790 472 17.2 J 70.5 145 2,180 424 NR NR NR NR NR 01/12/21 5,060 15,500 2,370 11,700 2,270 626 <63 110 J 270 2,390 685 NR NR NR NR NR 03/02/11 7,700 26,900 2,970 15,500 3,670 621 104 J 163 J 364 2,830 716 NR NR NR NR NR 09/26/11 13,400 24,900 2,920 15,520 18,100 1,150 82.5 231 599 3,530 1,160 NR NR NR NR NR 11/01/12 9,170 32,500 3,230 16,400 4,890 692 <100 162 J 483 J 2,660 731 NR NR NR NR NR 09/18/13 6,970 15,500 1,930 9,080 4,040 404 <50 68.3 J 264 1,510 392 17.9 26,200 9,270 J <420 8,800 04/03/14 1,580 4,860 648 4,330 725 349 <20 33.0 J 94.3 J 1,190 310 NR NR NR NR NR 01/06/15 5,510 14,700 1,900 9,660 2,510 371 <20 99.7 J 215 1,960 374 NR NR NR NR NR 01/12/21 3,900 23,600 3,290 15,600 <63 611 <63 137 J 346 2,540 692 NR NR NR NR NR 03/02/11 <0.140 0.353 J <0.150 0.505 J <0.250 <0.500 <0.180 <0.150 <0.220 0.190 J <0.180 NR NR NR NR NR 09/26/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 11/01/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/18/13 <0.10 <0.10 <0.10 <0.22 6.0 <0.15 <0.10 0.11 J <0.10 <0.10 <0.10 326 <35 <165 <130 <225 04/03/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 01/06/15 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 01/12/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR TABLE 5 SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS EVERETTE'S ENTERPRISES (INCIDENT NO. 11174) MADEP Methods VPH and EPH LeadC5-C8 AliphaticsC9-C18 AliphaticsC19-C36 AliphaticsC9-C22 AromaticsMTBEEthylbenzeneXylenesEPA Methods 6200B 1,2,4-TrimethylbenzeneAnalytical Method 1,3,5-Trimethylbenzenen-PropylbenzeneContaminant of Concern BenzeneToluene2L Standard (mg/l)Naphthalenen-ButylbenzeneIsopropylbenzeneWell ID Date Collected (mm/dd/yy) GCL (mg/l) MW-1 MW-2 MW-3 MW-4 Page 1 of 6 Date: 01/21/2021 Facility ID #: 0-009694 EPA Method 6010B/3030C 1 600 600 500 20 6 70 70 70 400 400 15 400 700 10,000 200 5,000 260,000 84,500 85,500 20,000 6,000 6,900 25,000 30,000 28,500 25,000 15,000 NE NE NE NE TABLE 5 SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS EVERETTE'S ENTERPRISES (INCIDENT NO. 11174) MADEP Methods VPH and EPH LeadC5-C8 AliphaticsC9-C18 AliphaticsC19-C36 AliphaticsC9-C22 AromaticsMTBEEthylbenzeneXylenesEPA Methods 6200B 1,2,4-TrimethylbenzeneAnalytical Method 1,3,5-Trimethylbenzenen-PropylbenzeneContaminant of Concern BenzeneToluene2L Standard (mg/l)Naphthalenen-ButylbenzeneIsopropylbenzeneWell ID Date Collected (mm/dd/yy) GCL (mg/l) 03/02/11 <0.140 0.631 J <0.150 0.760 J 51.1 <0.500 <0.180 <0.150 <0.220 0.249 J <0.180 NR NR NR NR NR 09/26/11 <0.13 <0.13 <0.15 <0.30 28.1 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 11/01/12 <0.10 <0.10 <0.10 <0.22 33.3 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/18/13 <0.10 <0.10 <0.10 <0.22 38.2 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 21.6 <35 <145 <110 <195 04/03/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 01/06/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 03/02/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.150 <0.220 <0.150 <0.180 NR NR NR NR NR 09/26/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 11/01/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/18/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 04/03/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 01/06/15 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 03/02/11 <0.700 1.11 J <0.750 <1.10 <1.25 <2.50 <0.900 <0.750 <1.10 <0.750 <0.900 NR NR NR NR NR 09/26/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 11/01/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/18/13 <0.10 0.41 J <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 55.5 <35 <145 <110 <205 04/03/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 01/06/15 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 01/12/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR 03/02/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.150 <0.220 <0.150 <0.180 NR NR NR NR NR 09/26/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 11/01/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/18/13 <0.10 <0.10 <0.10 <0.22 0.55 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 6.3 <35 <145 <110 <205 04/03/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 01/06/15 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 01/12/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR 03/02/11 10.8 2.98 2.54 2.87 167 0.690 J <0.180 0.215 J 0.415 J 1.58 0.329 J NR NR NR NR NR 09/26/11 8.1 0.63 1.4 0.45 J 35.8 0.53 <0.10 <0.10 0.16 J <0.10 <0.10 NR NR NR NR NR 11/01/12 0.46 J 0.25 J <0.10 <0.22 194 0.17 J <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/18/13 11.1 <0.10 0.40 J 0.25 J 40.4 0.58 <0.10 <0.10 0.28 J 0.37 J <0.10 <5.0 <35 <145 <110 <195 04/03/14 <0.10 <0.10 <0.10 <0.20 2.4 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 01/06/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS MW-8 MW-6 MWD-5 MW-7 MWD-9 Page 2 of 6 Date: 01/21/2021 Facility ID #: 0-009694 EPA Method 6010B/3030C 1 600 600 500 20 6 70 70 70 400 400 15 400 700 10,000 200 5,000 260,000 84,500 85,500 20,000 6,000 6,900 25,000 30,000 28,500 25,000 15,000 NE NE NE NE TABLE 5 SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS EVERETTE'S ENTERPRISES (INCIDENT NO. 11174) MADEP Methods VPH and EPH LeadC5-C8 AliphaticsC9-C18 AliphaticsC19-C36 AliphaticsC9-C22 AromaticsMTBEEthylbenzeneXylenesEPA Methods 6200B 1,2,4-TrimethylbenzeneAnalytical Method 1,3,5-Trimethylbenzenen-PropylbenzeneContaminant of Concern BenzeneToluene2L Standard (mg/l)Naphthalenen-ButylbenzeneIsopropylbenzeneWell ID Date Collected (mm/dd/yy) GCL (mg/l) 03/02/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.150 <0.220 <0.150 <0.180 NR NR NR NR NR 09/26/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 11/01/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/18/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 102 <35 <135 <100 <185 04/03/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 01/06/15 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 01/12/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR 03/02/11 738 27.3 125 61.7 390 39.1 <1.80 11.0 16.6 31.0 2.26 J NR NR NR NR NR 09/26/11 247 38.6 46.0 43.0 105 25.9 0.77 4.5 7.5 12.9 1.5 NR NR NR NR NR 11/01/12 0.87 <0.10 <0.10 <0.22 35.6 0.35 J <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/18/13 60.0 0.14 J 2.4 <0.22 138 4.3 <0.10 0.36 J 0.27 J <0.10 <0.10 8.0 74.5 J <135 <100 <185 04/03/14 <0.10 <0.10 <0.10 <0.20 92.1 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 01/06/15 0.50 <0.10 <0.10 <0.20 35.0 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 01/12/21 <0.13 <0.13 <0.13 <0.25 14.2 0.23 J <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR 03/02/11 156 <1.90 <1.50 <2.20 1,300 <5.00 <1.80 <1.50 <2.20 <1.50 <1.80 NR NR NR NR NR 09/26/11 63.8 0.69 7.9 0.99 J 327 4.3 0.21 J 2.3 1.5 0.30 J <0.10 NR NR NR NR NR 11/01/12 <2.0 <2.0 <2.0 <4.3 519 <3.0 <2.0 <2.0 <2.0 <2.0 <2.0 NR NR NR NR NR 09/18/13 <2.0 <2.0 <2.0 <4.3 476 <3.0 <2.0 <2.0 <2.0 <2.0 <2.0 147 <35 <135 <100 <185 04/03/14 34.8 <0.10 <0.10 <0.20 628 <0.10 <0.10 1.5 <0.10 <0.10 <0.10 NR NR NR NR NR 01/06/15 <0.10 <0.10 <0.10 <0.20 114 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 01/12/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR 09/26/11 701 20.9 68.0 106.3 818 28.5 1.7 11.4 12.4 42.5 1.9 NR NR NR NR NR 11/01/12 172 0.19 J 3.6 0.49 J 420 2.9 0.13 J 1.0 0.56 <0.10 <0.10 NR NR NR NR NR 09/18/13 1,310 30.0 344 553 1,040 91.7 <1.0 18.3 47.6 229 35.9 127 2,470 481 <110 775 04/03/14 14.8 <0.10 <0.10 1.2 J 225 1.6 <0.10 0.40 J <0.10 <0.10 <0.10 NR NR NR NR NR 01/06/15 3.7 <0.10 <0.10 <0.20 175 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 01/12/21 104 <0.31 4.2 10.7 106 17.5 1.2 J 6.0 9.3 4.5 <0.31 NR NR NR NR NR 03/02/11 <0.140 <0.190 <0.150 <0.220 0.411 J <0.500 <0.180 <0.150 <0.220 <0.150 <0.180 NR NR NR NR NR 09/26/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 11/01/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/18/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <5.0 <35 <145 <110 <195 04/03/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 01/06/15 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR MW-10 MW-11 MW-12 MW-13 MW-14 Page 3 of 6 Date: 01/21/2021 Facility ID #: 0-009694 EPA Method 6010B/3030C 1 600 600 500 20 6 70 70 70 400 400 15 400 700 10,000 200 5,000 260,000 84,500 85,500 20,000 6,000 6,900 25,000 30,000 28,500 25,000 15,000 NE NE NE NE TABLE 5 SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS EVERETTE'S ENTERPRISES (INCIDENT NO. 11174) MADEP Methods VPH and EPH LeadC5-C8 AliphaticsC9-C18 AliphaticsC19-C36 AliphaticsC9-C22 AromaticsMTBEEthylbenzeneXylenesEPA Methods 6200B 1,2,4-TrimethylbenzeneAnalytical Method 1,3,5-Trimethylbenzenen-PropylbenzeneContaminant of Concern BenzeneToluene2L Standard (mg/l)Naphthalenen-ButylbenzeneIsopropylbenzeneWell ID Date Collected (mm/dd/yy) GCL (mg/l) 03/02/11 <0.140 3.44 0.660 J <0.220 <0.250 <0.500 <0.180 <0.150 <0.220 <0.150 <0.180 NR NR NR NR NR 09/26/11 <0.13 <0.13 3.4 <0.30 <0.13 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 11/01/12 <0.10 <0.10 0.32 J <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/18/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 04/03/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 01/06/15 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 03/02/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.150 <0.220 <0.150 <0.180 NR NR NR NR NR 09/26/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 11/01/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/18/13 <0.10 0.16 J <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 63.0 <35 <145 <110 <205 04/03/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 01/06/15 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/26/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 11/01/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/18/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 311 <35 <145 <110 <195 04/03/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 01/06/15 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 03/02/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.150 <0.220 <0.150 <0.180 NR NR NR NR NR 09/26/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 11/01/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/18/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 04/03/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 01/06/15 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 03/02/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.150 <0.220 <0.150 <0.180 NR NR NR NR NR 09/26/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 11/01/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/18/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 04/03/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 01/06/15 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 11/01/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/18/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 56.5 <35 <145 <110 <195 04/03/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 01/06/15 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR MW-16 MW-15 MW-17 MW-18 MW-20 MW-21 Page 4 of 6 Date: 01/21/2021 Facility ID #: 0-009694 EPA Method 6010B/3030C 1 600 600 500 20 6 70 70 70 400 400 15 400 700 10,000 200 5,000 260,000 84,500 85,500 20,000 6,000 6,900 25,000 30,000 28,500 25,000 15,000 NE NE NE NE TABLE 5 SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS EVERETTE'S ENTERPRISES (INCIDENT NO. 11174) MADEP Methods VPH and EPH LeadC5-C8 AliphaticsC9-C18 AliphaticsC19-C36 AliphaticsC9-C22 AromaticsMTBEEthylbenzeneXylenesEPA Methods 6200B 1,2,4-TrimethylbenzeneAnalytical Method 1,3,5-Trimethylbenzenen-PropylbenzeneContaminant of Concern BenzeneToluene2L Standard (mg/l)Naphthalenen-ButylbenzeneIsopropylbenzeneWell ID Date Collected (mm/dd/yy) GCL (mg/l) 11/01/12 <0.10 <0.10 <0.10 <0.22 17.9 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/18/13 <0.10 <0.10 <0.10 <0.22 53.2 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 9.3 <35 <165 <130 <225 04/03/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 01/06/15 <0.10 <0.10 <0.10 <0.20 5.7 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 11/01/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/18/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 17.2 <35 <135 <100 <185 04/03/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 01/06/15 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/18/13 1.6 <0.25 <0.25 <0.54 104 <0.37 <0.25 <0.25 <0.25 <0.25 <0.25 <5.0 <35 <145 <110 <195 04/03/14 <0.10 <0.10 <0.10 <0.20 170 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 01/06/15 0.39 J 1.3 0.19 J 0.82 J 114 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 01/12/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR 09/18/13 0.20 J <0.10 <0.10 <0.22 28.4 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <5.0 <35 <145 <110 <195 04/03/14 <0.10 <0.10 <0.10 <0.20 229 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 01/06/15 <0.50 <0.50 <0.50 <1.0 243 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 NR NR NR NR NR 01/12/21 <0.31 <0.31 <0.31 <0.63 107 <0.31 <0.31 <0.31 <0.31 <0.31 <0.31 NR NR NR NR NR Site Sink 03/02/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.150 <0.220 <0.150 <0.180 NR NR NR NR NR Vaughn Spigot 03/02/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.150 <0.220 <0.150 <0.180 NR NR NR NR NR Church Sink 03/02/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.150 <0.220 <0.150 <0.180 NR NR NR NR NR House 1 11/01/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR House 2 11/01/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR House 3 11/01/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR House 4 11/01/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR House 5 11/01/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 11/01/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 04/03/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR MWD-25 House 8 MW-23 MW-22 MWD-24 Page 5 of 6 Date: 01/21/2021 Facility ID #: 0-009694 EPA Method 6010B/3030C 1 600 600 500 20 6 70 70 70 400 400 15 400 700 10,000 200 5,000 260,000 84,500 85,500 20,000 6,000 6,900 25,000 30,000 28,500 25,000 15,000 NE NE NE NE TABLE 5 SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS EVERETTE'S ENTERPRISES (INCIDENT NO. 11174) MADEP Methods VPH and EPH LeadC5-C8 AliphaticsC9-C18 AliphaticsC19-C36 AliphaticsC9-C22 AromaticsMTBEEthylbenzeneXylenesEPA Methods 6200B 1,2,4-TrimethylbenzeneAnalytical Method 1,3,5-Trimethylbenzenen-PropylbenzeneContaminant of Concern BenzeneToluene2L Standard (mg/l)Naphthalenen-ButylbenzeneIsopropylbenzeneWell ID Date Collected (mm/dd/yy) GCL (mg/l) 11/01/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 04/03/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR Notes: • Results reported in µg/l (micrograms per liter). • < : Less than the method detection limit specified in the laboratory report. • 2L Standard specified in T15A NCAC 2L.0202. • GCL: Gross contamination level. • NE: Not established. • NR: Not requested. • Concentrations in bold face type exceeded the 2L Standards. • Concentrations in bold face type and italics exceeded the GCLs. • J: Estimated concentration. • Please refer to the lab report for detectable concentrations which did not exceed the 2L Standards. • A concentration of 1,2-dichloroethane that exceeded the 2L Standard was reported in MW-13 during the January 2020 sampling event. House 9 Page 6 of 6 APPENDICES APPENDIX A State Correspondence December 8, 2020 North East Oil Company, Inc. c/o Mr. Lars Simonsen, Registered Agent Post Office Box 848 Edenton, North Carolina 27932 Re: Notice of Regulatory Requirements 15A NCAC 2L .0407(c) for Intermediate Risk Risk-based Assessment and Corrective Action For Petroleum Underground Storage Tanks Everette’s Enterprise 1101 N. Catherine Creek Rd., Ahoskie, NC Hertford County Incident Number: 11174 Risk Classification: Intermediate Ranking: I 90 R Dear Mr. Simonsen: Recent efforts to further promote cost effective assessment and remediation strategies at active Underground Storage Tank (UST) incident sites have produced sufficient results to allow for an expansion of the Commercial UST Cleanup Fund to capture additional sites. Effective November 19, 2020, the funding prioritization schedule for the Commercial Cleanup Fund has been adjusted to include all Intermediate Risk sites. The above referenced petroleum release (incident) has been classified as Intermediate Risk. The Department of Environmental Quality (Department) is directing you, as the owner and/or operator of the UST system, to complete certain tasks that are required by rule. Funding is potentially available. The Department needs updated information on the risks associated with your release which must be performed by a North Carolina Licensed Geologist or Professional Engineer. The Department will use this information to perform a risk evaluation. Please submit a completed pre-approval request within 14 days of receipt of this notice for the following work. The Current Electronic Pre-Approval Task Authorization can be found on the UST website at https://deq.nc.gov/about/divisions/waste-management/ust/trust- fund/reasonable-rate-documents. 2459 Received DEC 14 2020 Please complete the following requirements. 1. Sample the groundwater monitoring wells in the source area and include a couple down gradient wells. Submit samples or analysis using the appropriate methods. 2. Survey the surrounding area for water resources that could be at risk, such as water supply wells, lakes, streams, etc. (called receptors), to update any previous survey results. This survey is only required if the previous survey is more than five years old, or if the redevelopment of properties in the area could change the outcome of an updated survey. The Request for Water Supply Well Information template can be found in the Guidelines for Assessment and Corrective Action (appendices) in Appendix A on the UST website at http://deq.nc.gov/about/divisons/waste-management/ust/guidance-documents. The results from the monitoring well sampling and the survey information must be submitted in the format of a groundwater monitoring report prepared in accordance with 15A NCAC 2L .0407(c) for intermediate risk and the UST Section Assessment Guidelines within 60 days of receipt of this notice. The report template can be found in the Guidelines for Assessment (appendices) on the UST website at https://dec.nc.gov/about/divisions/waste-management/ust/guidance-documents. You may be eligible for reimbursement from the Leaking Underground Storage Tank Commercial Trust Fund for some or all of the costs for this and subsequent work (though deductibles and reasonable rate limits do apply). An eligibility determination is required for potential reimbursements. Please contact the Trust Fund Branch if you do not know your eligibility status. Reimbursement also requires prior written approval of the specific tasks and costs for the necessary work. Many environmental consulting firms that work in North Carolina can help you apply for funding and can prepare the necessary pre-approval and claim forms on your behalf for a small fee. Additionally, UST Section Trust Fund Branch staff can be reached directly at 919-707-8171 if you have any questions. Please let me know within 14 days if you intend to conduct the risk re-evaluation by submitting a pre- approval request. If you do not intend to do so, please provide reason(s) for not doing the work (for example, declaration of bankruptcy or dissolution of corporation, financial inability, etc.). Please note that, if for some reason the UST Section is required to use its own contractors to complete the assessment on your behalf, the State Trust Fund may seek to recover their costs from you for those expenses, unless you have provided proper documentation of financial hardship. I am available to answer any questions. Please contact me at the UST Regional Office address or phone number below. Sincerely, Carrie Stone Hydrogeologist Washington Regional Office UST Section, Division of Waste Management, NCDEQ cc: Hertford County Health Department William Regenthal, Geological Resources, Inc. (email) North East Oil Company, P.O. Box 1386, Ahoskie, NC 27910 Washington Regional Office | 943 Washington Square Mall | Washington, NC 27889 | (252) 946-6481 2459 Received JAN 07 2021 APPENDIX B Property Cards Property Summary Tax Year: 2021 Building Summary REID 5993704828000 PIN 5993-70- 4828 Property Owner EVERETTE, CLYDE W, JR;EVERETTE, ELESIA Location Address 100 HOLLOMAN AVE Property Description CC RD Owner's Mailing Address 414 TROY ST E AHOSKIE NC 27910 Administrative Data Plat Book & Page Old Map # Market Area CM-P Township AHOSKIE Planning Jurisdiction AHOSKIE,COUNTY City AHOSKIE Fire District Spec District Land Class COM History REID 1 History REID 2 Acreage 0 Permit Date Permit # Transfer Information Deed Date 1/22/1993 Deed Book 000488 Deed Page 00736 Revenue Stamps Package Sale Date Package Sale Price Land Sale Date Land Sale Price Improvement Summary Total Buildings 2 Total Units 0 Total Living Area 0 Total Gross Leasable Area 2,187 Property Value Total Appraised Land Value $13,855 Total Appraised Building Value $12,470 Total Appraised Misc Improvements Value $941 Total Cost Value $27,266 Total Appraised Value - Valued By Cost $27,266 Other Exemptions Exemption Desc Use Value Deferred Historic Value Deferred Total Deferred Value Total Taxable Value $27,266 Card 1 100 HOLLOMAN AVE Building Details Bldg Name OTHER Primary Occupancy Type COMMERCIAL Primary Occupancy 10-CONVENIENCE-STORE Primary Class Migration Primary Quality D-5 Year Built 1970 Effective Year 1970 Physical Depreciation (Rating)FAIR Physical Depreciation (% Bad)85 Economic Depreciation (% Bad)10 Functional Depreciation (% Bad)10 Gross Leasable Area (SQFT)1,553 Remodeled Year 1974 Total Stories 1 Building Total & Improvement Details Total Adjusted Replacement Cost New $1,572,452 Physical Depreciation (% Bad)FAIR 85 Depreciated Value $298,766 Economic Depreciation (% Bad)10 Functional Depreciation (% Bad)10 Total Depreciated Value $239,013 Market Area Factor 0.65 Building Value $10,083 Misc Improvements Value $941 Total Improvement Value $11,024 Assessed Land Value $13,855 Assessed Total Value $27,266 Card 2 100 HOLLOMAN AVE Addition Summary Story Type Code Area 1.00 ATTACHED ADDITION AA-A 160 1.00 OPEN PORCH OP-O 165 Section 1 Details Occupancy Type COMMERCIAL Air Conditioning Y Class Migration Depreciation 81% Depreciation FAIR Exterior Walls BR-BRICK EXTRA_FIXTURES 5 HALF_BATH 2 Heat F-FORCED-AIR Occupancy 10-CONVENIENCE- STORE Quality D-5 Roof Cover A-ASPHALT- SHINGLE Roof Type G-GABLE Building Sketch Photograph Building Details Bldg Name OTHER Primary Occupancy Type COMMERCIAL Primary Occupancy 11-COMMERCIAL Primary Class Migration Primary Quality D Building Total & Improvement Details Total Adjusted Replacement Cost New $32,334 Physical Depreciation (% Bad)FAIR 85 Depreciated Value $4,850 Economic Depreciation (% Bad)0 Functional Depreciation (% Bad)0 Addition Summary Story Type Code Area Year Built 1970 Effective Year 1970 Physical Depreciation (Rating)FAIR Physical Depreciation (% Bad)85 Economic Depreciation (% Bad)0 Functional Depreciation (% Bad)0 Gross Leasable Area (SQFT)634 Remodeled Year 0 Total Stories 1 Total Depreciated Value $4,850 Market Area Factor 0.65 Building Value $2,387 Misc Improvements Value Total Improvement Value $2,387 Assessed Land Value $13,855 Assessed Total Value $27,266 Section 1 Details Occupancy Type COMMERCIAL Air Conditioning Y Class Migration Depreciation 85% Depreciation FAIR Exterior Walls F-FRAME EXTRA_FIXTURES 6 HALF_BATH 2 Heat F-FORCED-AIR Interior Finish P-PANELING Occupancy 11-COMMERCIAL Quality D Roof Cover A-ASPHALT- SHINGLE Roof Type G-GABLE Building Sketch Photograph Misc Improvements Summary Land Summary Ownership History Notes Summary Card # Unit Quantity Measure Type Base Price Eff Year Phys Depr (% Bad) Econ Depr (% Bad) Funct Depr (% Bad) Common Interest (% Good)Value 1 2160 SIZE 88- PAVING/DRIVEWAY $387.00 1970 75 0 0 $941 Total Misc Improvements Value Assessed: $941 Zoning Soil Class Description Size Rate Depth Depth Factor Land Adjustment Land Value B-2 10-COMMERCIAL 82.66 FRONT FOOT PRICED $145 90 0.96 MARKET-90.00 $10,355 B-2 W-WATER 1.00 BY THE UNIT PRICE $1,000 0 0 $1,000 B-2 S-SEWER 1.00 BY THE UNIT PRICE $2,500 0 0 $2,500 Total Land Value Assessed: $13,855 Land Class: COM Deeded Acres: 0 Calculated Acres: 0.17 Owner Name Deed Type % Ownership Stamps Sale Price Book Page Deed Date Current EVERETTE, CLYDE W, JR/ EVERETTE, ELESIA DEED 100 0 000488 00736 1/22/1993 Building Card Date Line Notes P 2/1/2018 1 CC RD 1101 N DR MLK JR DR Property Summary Tax Year: 2021 Building Summary REID 5993704980000 PIN 5993-70-4980 Property Owner HARRELL, TRAVIS Location Address 1103 N DR MARTIN LUTHER KING JR DR Property Description CATHERINE CREEK RD Owner's Mailing Address 106 BLACKSMITH DR AHOSKIE NC 27910 Administrative Data Plat Book & Page Old Map # Market Area RS-P Township AHOSKIE Planning Jurisdiction AHOSKIE,COUNTY City Fire District Spec District Land Class RES History REID 1 History REID 2 Acreage 0 Permit Date Permit # Transfer Information Deed Date 6/27/2016 Deed Book 000783 Deed Page 00235 Revenue Stamps Package Sale Date 6/27/2016 Package Sale Price Land Sale Date Land Sale Price Improvement Summary Total Buildings 1 Total Units 0 Total Living Area 856 Total Gross Leasable Area 0 Property Value Total Appraised Land Value $6,578 Total Appraised Building Value $19,458 Total Appraised Misc Improvements Value Total Cost Value $26,036 Total Appraised Value - Valued By Cost $26,036 Other Exemptions Exemption Desc Use Value Deferred Historic Value Deferred Total Deferred Value Total Taxable Value $26,036 Card 1 1103 N DR MARTIN LUTHER KING JR DR Building Details Bldg Type RESIDENTIAL Units 0 Living Area (SQFT) 856 Number of Stories 1.00 Style C-CONVENTIONAL Foundation M-MASONERY Frame Exterior AV-ALUM/VNYL- SIDNG-F Const Type Heating N-NONE Air Cond AC-N Baths (Full)0 Baths (Half)1 Building Description Year Built 1950 Effective Year 1950 Additions 2 Remodeled 1960 Interior Adj Other Features Building Total & Improvement Details Grade D 78% Percent Complete 100 Total Adjusted Replacement Cost New $61,027 Physical Depreciation (% Bad)A 59% Depreciated Value $28,072 Economic Depreciation (% Bad) 0 Functional Depreciation (% Bad) 0 Total Depreciated Value $28,072 Market Area Factor 0.7 Building Value $19,458 Misc Improvements Value Total Improvement Value Misc Improvements Summary Land Summary Ownership History Addition Summary Story Type Code Area 1.00 OPEN PORCH OP-O 72 1.00 OPEN PORCH OP-O 90 Extra Fixtures 3 Total Plumbing Fixtures 5 Bedrooms 2 Floor P-PINE/PLYWOOD Roof Cover A-ASPHALT- SHINGLE Roof Type G-GABLE Main Body (SQFT)856 Assessed Land Value Assessed Total Value Building Sketch Photograph Card # Unit Quantity Measure Type Base Price Eff Year Phys Depr (% Bad) Econ Depr (% Bad) Funct Depr (% Bad) Common Interest (% Good)Value No Data Total Misc Improvements Value Assessed: Zoning Soil Class Description Size Rate Depth Depth Factor Land Adjustment Land Value R 9-RESIDENTIAL 50.00 FRONT FOOT PRICED $95 79 0.725 MARKET-90.00 $3,078 R W-WATER 1.00 BY THE UNIT PRICE $1,000 0 0 $1,000 R S-SEWER 1.00 BY THE UNIT PRICE $2,500 0 0 $2,500 Total Land Value Assessed: $6,578 Land Class: RES Deeded Acres: 0 Calculated Acres: 0.09 Notes Summary Owner Name Deed Type % Ownership Stamps Sale Price Book Page Deed DateOwner Name Deed Type % Ownership Stamps Sale Price Book Page Deed Date Current HARRELL, TRAVIS DEED 100 0 000783 00235 6/27/2016 1 Back HARRELL, TIMOTHY DEED 100 0 000661 00469 1/25/2006 2 Back HALL, PEARL S WILL 100 0 00002E 00059 3/8/2002 Building Card Date Line Notes P 2/1/2018 1 CATHERINE CREEK RD 1103 N DR MLK JR DR Property Summary Tax Year: 2021 Building Summary REID 5993704762000 PIN 5993-70- 4762 Property Owner HOLLEY, KEELY P Location Address 1100 A N DR MARTIN LUTHER KING JR DR Property Description C.C. RD.Owner's Mailing Address 1490 HARTFORD TERRACE ALPHARETTA GA 30004 Administrative Data Plat Book & Page Old Map # Market Area CM-P Township AHOSKIE Planning Jurisdiction AHOSKIE,COUNTY City AHOSKIE Fire District Spec District Land Class COM History REID 1 History REID 2 Acreage 0 Permit Date Permit # Transfer Information Deed Date 4/26/2010 Deed Book 000722 Deed Page 00776 Revenue Stamps Package Sale Date 4/26/2010 Package Sale Price Land Sale Date Land Sale Price Improvement Summary Total Buildings 1 Total Units 0 Total Living Area 1,680 Total Gross Leasable Area 0 Property Value Total Appraised Land Value $22,454 Total Appraised Building Value $1,035 Total Appraised Misc Improvements Value $942 Total Cost Value $24,431 Total Appraised Value - Valued By Cost $24,431 Other Exemptions Exemption Desc Use Value Deferred Historic Value Deferred Total Deferred Value Total Taxable Value $24,431 Card 1 1100 N DR MARTIN LUTHER KING JR DR Building Details Bldg Type RESIDENTIAL Units 0 Living Area (SQFT)1680 Number of Stories 2.00 Style C- CONVENTIONAL Foundation M-MASONERY Frame Exterior F-FRAME Const Type Heating N-NONE Air Cond AC-N Baths (Full)2 Baths (Half)0 Building Description Year Built 1930 Effective Year 1930 Additions 4 Remodeled 0 Interior Adj Other Features Building Total & Improvement Details Grade D+10 78% Percent Complete 100 Total Adjusted Replacement Cost New $192,180 Physical Depreciation (% Bad) U 99% Depreciated Value $1,922 Economic Depreciation (% Bad) 0 Functional Depreciation (% Bad) 20 Total Depreciated Value $1,538 Market Area Factor 0.65 Building Value $1,035 Misc Improvements Value $942 Misc Improvements Summary Land Summary Addition Summary Story Type Code Area 2.00 ENCLOSED PORCH EP-E 320 1.00 OPEN PORCH OP-O 48 1.00 ENCLOSED PORCH EP-E 24 1.00 OPEN PORCH OP-O 24 Extra Fixtures 8 Total Plumbing Fixtures 14 Bedrooms 6 Floor H-HARDWOOD Roof Cover M-METAL Roof Type G-GABLE Main Body (SQFT)1680 Total Improvement Value $1,884 Assessed Land Value Assessed Total Value Building Sketch Photograph Card # Unit Quantity Measure Type Base Price Eff Year Phys Depr (% Bad) Econ Depr (% Bad) Funct Depr (% Bad) Common Interest (% Good)Value 1 3800 SIZE 88- PAVING/DRIVEWAY $387.00 1930 90 0 0 $942 Total Misc Improvements Value Assessed: $942 Zoning Soil Class Description Size Rate Depth Depth Factor Land Adjustment Land Value B-2 9-RESIDENTIAL 200.00 FRONT FOOT PRICED $130 100 1 MARKET-90.00 $18,954 B-2 W-WATER 1.00 BY THE UNIT PRICE $1,000 0 0 $1,000 B-2 S-SEWER 1.00 BY THE UNIT PRICE $2,500 0 0 $2,500 Total Land Value Assessed: $22,454 Land Class: COM Deeded Acres: 0 Calculated Acres: 0.47 Ownership History Notes Summary Owner Name Deed Type % Ownership Stamps Sale Price Book Page Deed Date Current HOLLEY, KEELY P DEED 100 0 000722 00776 4/26/2010 1 Back PILLMON, SAM, ESTATE WILL 100 0 00096E 00139 7/7/1998 Building Card Date Line Notes P 2/1/2018 1 STORE USED FOR STORAGE P 2/1/2018 2 RENT 200 MO FOR APT P 2/1/2018 3 ALTERATIONS 1986 P 2/1/2018 4 C.C. RD. 1100 A-C N DR MLK JR DR Property Summary Tax Year: 2021 Building Summary REID 5993702836000 PIN 5993-70- 2836 Property Owner JONES, C W, HEIRS Location Address 1025 N DR MARTIN LUTHER KING JR DR Property Description C.C. RD.Owner's Mailing Address PO BOX 368 AHOSKIE NC 27910 Administrative Data Plat Book & Page Old Map # Market Area CM-P Township AHOSKIE Planning Jurisdiction AHOSKIE,COUNTY City Fire District Spec District Land Class COM History REID 1 History REID 2 Acreage 0 Permit Date Permit # Transfer Information Deed Date 1/1/1900 Deed Book 000000 Deed Page 00000 Revenue Stamps Package Sale Date Package Sale Price Land Sale Date Land Sale Price Improvement Summary Total Buildings 1 Total Units 0 Total Living Area 1,598 Total Gross Leasable Area 0 Property Value Total Appraised Land Value $24,003 Total Appraised Building Value $14,305 Total Appraised Misc Improvements Value Total Cost Value $38,308 Total Appraised Value - Valued By Cost $38,308 Other Exemptions Exemption Desc Use Value Deferred Historic Value Deferred Total Deferred Value Total Taxable Value $38,308 Card 1 1025 N DR MARTIN LUTHER KING JR DR Building Details Bldg Type RESIDENTIAL Units 0 Living Area (SQFT) 1598 Number of Stories 1.00 Style C-CONVENTIONAL Foundation P-PIER Frame Exterior AV-ALUM/VNYL- SIDNG-F Const Type Heating W-WALL/FLOOR- FURNACE Air Cond AC-N Building Description Year Built 1952 Effective Year 1952 Additions 1 Remodeled 1960 Interior Adj Other Features Building Total & Improvement Details Grade D-10 78% Percent Complete 100 Total Adjusted Replacement Cost New $102,925 Physical Depreciation (% Bad) F 77% Depreciated Value $27,790 Economic Depreciation (% Bad) 0 Functional Depreciation (% Bad) 0 Total Depreciated Value $27,790 Market Area Factor 0.65 Building Value $14,305 Misc Improvements Value Misc Improvements Summary Land Summary Addition Summary Story Type Code Area 1.00 ATTACHED ADDITION AA-A 279 Baths (Full)1 Baths (Half)0 Extra Fixtures 5 Total Plumbing Fixtures 8 Bedrooms 2 Floor P-PINE/PLYWOOD Roof Cover M-METAL Roof Type G-GABLE Main Body (SQFT) 1598 Total Improvement Value Assessed Land Value Assessed Total Value Building Sketch Photograph Card # Unit Quantity Measure Type Base Price Eff Year Phys Depr (% Bad) Econ Depr (% Bad) Funct Depr (% Bad) Common Interest (% Good)Value 1 1 SIZE SV-SOUND- VALUE 1952 0 0 0 Total Misc Improvements Value Assessed: Zoning Soil Class Description Size Rate Depth Depth Factor Land Adjustment Land Value R-6 9-RESIDENTIAL 220.00 FRONT FOOT PRICED $95 183 1.098 MARKET-90.00 $20,503 R-6 W-WATER 1.00 BY THE UNIT PRICE $1,000 0 0 $1,000 R-6 S-SEWER 1.00 BY THE UNIT PRICE $2,500 0 0 $2,500 Total Land Value Assessed: $24,003 Land Class: COM Deeded Acres: 0 Calculated Acres: 0.95 Ownership History Notes Summary Owner Name Deed Type % Ownership Stamps Sale Price Book Page Deed Date Current JONES, C W, HEIRS DEED 100 0 000000 00000 1/1/1900 Building Card Date Line Notes P 2/1/2018 1 596/637 THOMAS L JONES, SR & WF PAULA H JONES A 1/3 UNDIVIDED INTEREST P 2/1/2018 2 C.C. RD. 1003 &1025 N DR MLK JR DR Property Summary Tax Year: 2021 Building Summary Misc Improvements Summary REID 5993704927000 PIN 5993-70-4927 Property Owner COUNTY OF HERTFORD Location Address 102 HOLLOMAN AVE Property Description 102 FAIRGROUND RD Owner's Mailing Address 115 JUSTICE DR SUITE #1 WINTON NC 27986 Administrative Data Plat Book & Page Old Map # Market Area RS-P Township AHOSKIE Planning Jurisdiction AHOSKIE,COUNTY City Fire District Spec District Land Class RES History REID 1 History REID 2 Acreage 0 Permit Date Permit # Transfer Information Deed Date 5/30/2012 Deed Book 000743 Deed Page 00407 Revenue Stamps $12 Package Sale Date Package Sale Price Land Sale Date 5/30/2012 Land Sale Price $6,000 Improvement Summary Total Buildings 0 Total Units 0 Total Living Area 0 Total Gross Leasable Area 0 Property Value Total Appraised Land Value $10,572 Total Appraised Building Value Total Appraised Misc Improvements Value Total Cost Value $10,572 Total Appraised Value - Valued By Cost $10,572 Other Exemptions $10,572 Exemption Desc DEFAULT EXEMPTION Use Value Deferred Historic Value Deferred Total Deferred Value Total Taxable Value Photograph Card # Unit Quantity Measure Type Base Price Eff Year Phys Depr (% Bad) Econ Depr (% Bad) Funct Depr (% Bad) Common Interest (% Good)Value No Data Total Misc Improvements Value Assessed: Land Summary Ownership History Notes Summary Zoning Soil Class Description Size Rate Depth Depth Factor Land Adjustment Land Value R 9-RESIDENTIAL 92.94 FRONT FOOT PRICED $95 120 0.89 MARKET-90.00 $7,072 R W-WATER 1.00 BY THE UNIT PRICE $1,000 0 0 $1,000 R S-SEWER 1.00 BY THE UNIT PRICE $2,500 0 0 $2,500 Total Land Value Assessed: $10,572 Land Class: RES Deeded Acres: 0 Calculated Acres: 0.25 Owner Name Deed Type % Ownership Stamps Sale Price Book Page Deed Date Current COUNTY OF HERTFORD DEED 100 12 $6,000 000743 00407 5/30/2012 1 Back SIMMONS, MERVIN L HEIRS INTST 100 0 00089E 00042 2/28/1990 Building Card Date Line Notes P 2/1/2018 1 GS#01 P 2/1/2018 2 102 FAIRGROUND RD 102 HOLLOMAN AVE APPENDIX C Laboratory Report – Ground Water Samples 01/20/21 Technical Report for GRI (Geological Resources Inc.) Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC 11174/2459 SGS Job Number: FA82323 Sampling Date: 01/12/21 Report to: GRI 3502 Hayes Rd Monroe, NC 28110 nml@geologicalresourcesinc.com; carriekennedy@geologicalresourcesinc.com; jjr@geologicalresourcesinc.com ATTN: Nicole Long Total number of pages in report: Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(573), NJ(FL002), NY(12022), SC(96038001) DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177), AK, AR, IA, KY, MA, MS, ND, NH, NV, OK, OR, UT, WA, WV This report shall not be reproduced, except in its entirety, without the written approval of SGS. Test results relate only to samples analyzed. SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: 407-425-6700 • fax: 407-425-0707 Test results contained within this data package meet the requirements of the National Environmental Laboratory Accreditation Program and/or state specific certification programs as applicable. Client Service contact: Muna Mohammed 407-425-6700 Norm Farmer Technical Director Orlando, FL 01/20/21 e-Hardcopy 2.0 Automated Report 53 SGS is the sole authority for authorizing edits or modifications to this document. Unauthorized modification of this report is strictly prohibited. Review standard terms at: http://www.sgs.com/en/terms-and-conditions The results set forth herein are provided by SGS North America Inc. Please share your ideas about how we can serve you better at: EHS.US.CustomerCare@sgs.com 1 of 53 FA82323 Table of Contents -1- Sections: Section 1: Sample Summary ...................................................................................................3 Section 2: Summary of Hits ....................................................................................................4 Section 3: Sample Results ........................................................................................................7 3.1: FA82323-1: MW-1 ........................................................................................................8 3.2: FA82323-2: MW-2 ........................................................................................................10 3.3: FA82323-3: MW-3 ........................................................................................................12 3.4: FA82323-4: MW-7 ........................................................................................................14 3.5: FA82323-5: MW-8 ........................................................................................................16 3.6: FA82323-6: MW-10 ......................................................................................................18 3.7: FA82323-7: MW-11 ......................................................................................................20 3.8: FA82323-8: MW-12 ......................................................................................................22 3.9: FA82323-9: MW-13 ......................................................................................................24 3.10: FA82323-10: MW-24 ..................................................................................................26 3.11: FA82323-11: MW-25 ..................................................................................................28 3.12: FA82323-12: MW-4 ....................................................................................................30 Section 4: Misc. Forms ............................................................................................................32 4.1: Chain of Custody ...........................................................................................................33 Section 5: MS Volatiles - QC Data Summaries .....................................................................35 5.1: Method Blank Summary ................................................................................................36 5.2: Blank Spike Summary ...................................................................................................42 5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................48 123452 of 53 FA82323 SGS North America Inc. Sample Summary GRI (Geological Resources Inc.) Job No:FA82323 Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC Project No: 11174/2459 Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID This report contains results reported as ND = Not detected. The following applies: Organics ND = Not detected above the MDL FA82323-1 01/12/21 15:17 ER 01/13/21 AQ Ground Water MW-1 FA82323-2 01/12/21 15:07 ER 01/13/21 AQ Ground Water MW-2 FA82323-3 01/12/21 14:15 ER 01/13/21 AQ Ground Water MW-3 FA82323-4 01/12/21 14:26 ER 01/13/21 AQ Ground Water MW-7 FA82323-5 01/12/21 14:35 ER 01/13/21 AQ Ground Water MW-8 FA82323-6 01/12/21 14:46 ER 01/13/21 AQ Ground Water MW-10 FA82323-7 01/12/21 14:56 ER 01/13/21 AQ Ground Water MW-11 FA82323-8 01/12/21 15:27 ER 01/13/21 AQ Ground Water MW-12 FA82323-9 01/12/21 15:37 ER 01/13/21 AQ Ground Water MW-13 FA82323-10 01/12/21 14:05 ER 01/13/21 AQ Ground Water MW-24 FA82323-11 01/12/21 15:50 ER 01/13/21 AQ Ground Water MW-25 FA82323-12 01/12/21 16:03 ER 01/13/21 AQ Ground Water MW-4 3 of 53 FA823231 Summary of Hits Page 1 of 3 Job Number:FA82323 Account:GRI (Geological Resources Inc.) Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC Collected:01/12/21 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method FA82323-1 MW-1 Benzene 937 100 25 ug/l SM 6200B Ethylbenzene 1100 100 25 ug/l SM 6200B Isopropylbenzene 60.0 J 100 25 ug/l SM 6200B Naphthalene 374 100 25 ug/l SM 6200B n-Propylbenzene 140 100 25 ug/l SM 6200B Toluene 7010 100 25 ug/l SM 6200B 1,2,4-Trimethylbenzene 1950 100 25 ug/l SM 6200B 1,3,5-Trimethylbenzene 578 100 25 ug/l SM 6200B m,p-Xylene 4870 200 25 ug/l SM 6200B o-Xylene 2250 100 25 ug/l SM 6200B Xylene (total)7120 300 50 ug/l SM 6200B FA82323-2 MW-2 Benzene 5060 250 63 ug/l SM 6200B Ethylbenzene 2370 250 63 ug/l SM 6200B Isopropylbenzene 110 J 250 63 ug/l SM 6200B Methyl Tert Butyl Ether 2270 250 63 ug/l SM 6200B Naphthalene 626 250 63 ug/l SM 6200B n-Propylbenzene 270 250 63 ug/l SM 6200B Toluene 15500 250 63 ug/l SM 6200B 1,2,4-Trimethylbenzene 2390 250 63 ug/l SM 6200B 1,3,5-Trimethylbenzene 685 250 63 ug/l SM 6200B m,p-Xylene 8310 500 63 ug/l SM 6200B o-Xylene 3430 250 63 ug/l SM 6200B Xylene (total)11700 750 130 ug/l SM 6200B FA82323-3 MW-3 Benzene 3900 250 63 ug/l SM 6200B Ethylbenzene 3290 250 63 ug/l SM 6200B Isopropylbenzene 137 J 250 63 ug/l SM 6200B Naphthalene 611 250 63 ug/l SM 6200B n-Propylbenzene 346 250 63 ug/l SM 6200B Toluene 23600 250 63 ug/l SM 6200B 1,2,4-Trimethylbenzene 2540 250 63 ug/l SM 6200B 1,3,5-Trimethylbenzene 692 250 63 ug/l SM 6200B m,p-Xylene 10500 500 63 ug/l SM 6200B o-Xylene 5060 250 63 ug/l SM 6200B Xylene (total)15600 750 130 ug/l SM 6200B 4 of 53 FA823232 Summary of Hits Page 2 of 3 Job Number:FA82323 Account:GRI (Geological Resources Inc.) Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC Collected:01/12/21 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method FA82323-4 MW-7 No hits reported in this sample. FA82323-5 MW-8 No hits reported in this sample. FA82323-6 MW-10 No hits reported in this sample. FA82323-7 MW-11 Methyl Tert Butyl Ether 14.2 0.50 0.13 ug/l SM 6200B Naphthalene 0.23 J 0.50 0.13 ug/l SM 6200B FA82323-8 MW-12 No hits reported in this sample. FA82323-9 MW-13 Benzene 104 1.3 0.31 ug/l SM 6200B n-Butylbenzene 1.2 J 1.3 0.31 ug/l SM 6200B sec-Butylbenzene 1.7 1.3 0.31 ug/l SM 6200B 1,2-Dichloroethane 0.76 J 1.3 0.31 ug/l SM 6200B Di-Isopropyl Ether 0.84 J 1.3 0.31 ug/l SM 6200B Ethylbenzene 4.2 1.3 0.31 ug/l SM 6200B Isopropylbenzene 6.0 1.3 0.31 ug/l SM 6200B Methyl Tert Butyl Ether 106 1.3 0.31 ug/l SM 6200B Naphthalene 17.5 1.3 0.31 ug/l SM 6200B n-Propylbenzene 9.3 1.3 0.31 ug/l SM 6200B 1,2,4-Trimethylbenzene 4.5 1.3 0.31 ug/l SM 6200B m,p-Xylene 10.7 2.5 0.31 ug/l SM 6200B Xylene (total)10.7 3.8 0.63 ug/l SM 6200B FA82323-10 MW-24 No hits reported in this sample. FA82323-11 MW-25 Methyl Tert Butyl Ether 107 1.3 0.31 ug/l SM 6200B 5 of 53 FA823232 Summary of Hits Page 3 of 3 Job Number:FA82323 Account:GRI (Geological Resources Inc.) Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC Collected:01/12/21 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method FA82323-12 MW-4 No hits reported in this sample. 6 of 53 FA823232 SGS North America Inc. Sample Results Report of Analysis Orlando, FL Section 3 7 of 53 FA823233 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID:MW-1 Lab Sample ID:FA82323-1 Date Sampled:01/12/21 Matrix:AQ - Ground Water Date Received:01/13/21 Method:SM 6200B Percent Solids:n/a Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 A0225133.D 200 01/14/21 13:25 LR n/a n/a VA2848 Run #2 Purge Volume Run #1 10.0 ml Run #2 VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene 937 100 25 ug/l 108-86-1 Bromobenzene ND 100 25 ug/l 74-97-5 Bromochloromethane ND 100 25 ug/l 75-27-4 Bromodichloromethane ND 100 25 ug/l 75-25-2 Bromoform ND 100 25 ug/l 104-51-8 n-Butylbenzene ND 100 25 ug/l 135-98-8 sec-Butylbenzene ND 100 25 ug/l 98-06-6 tert-Butylbenzene ND 100 25 ug/l 56-23-5 Carbon Tetrachloride ND 100 25 ug/l 108-90-7 Chlorobenzene ND 100 25 ug/l 75-00-3 Chloroethane ND 100 40 ug/l 67-66-3 Chloroform ND 100 25 ug/l 95-49-8 o-Chlorotoluene ND 100 25 ug/l 106-43-4 p-Chlorotoluene ND 100 25 ug/l 124-48-1 Dibromochloromethane ND 100 25 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 100 49 ug/l 106-93-4 1,2-Dibromoethane ND 100 25 ug/l 75-71-8 Dichlorodifluoromethane ND 100 40 ug/l 95-50-1 1,2-Dichlorobenzene ND 100 25 ug/l 541-73-1 1,3-Dichlorobenzene ND 100 25 ug/l 106-46-7 1,4-Dichlorobenzene ND 100 25 ug/l 75-34-3 1,1-Dichloroethane ND 100 25 ug/l 107-06-2 1,2-Dichloroethane ND 100 25 ug/l 75-35-4 1,1-Dichloroethylene ND 100 25 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 100 25 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 100 25 ug/l 78-87-5 1,2-Dichloropropane ND 100 25 ug/l 142-28-9 1,3-Dichloropropane ND 100 25 ug/l 594-20-7 2,2-Dichloropropane ND 100 25 ug/l 563-58-6 1,1-Dichloropropene ND 100 25 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 100 25 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 100 25 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 8 of 53 FA8232333.1 SGS North America Inc. Report of Analysis Page 2 of 2 Client Sample ID:MW-1 Lab Sample ID:FA82323-1 Date Sampled:01/12/21 Matrix:AQ - Ground Water Date Received:01/13/21 Method:SM 6200B Percent Solids:n/a Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether ND 100 25 ug/l 100-41-4 Ethylbenzene 1100 100 25 ug/l 87-68-3 Hexachlorobutadiene ND 100 25 ug/l 98-82-8 Isopropylbenzene 60.0 100 25 ug/l J 99-87-6 p-Isopropyltoluene ND 100 25 ug/l 74-83-9 Methyl Bromide ND 100 40 ug/l 74-87-3 Methyl Chloride ND 100 40 ug/l 74-95-3 Methylene Bromide ND 100 25 ug/l 75-09-2 Methylene Chloride ND 400 200 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 100 25 ug/l 91-20-3 Naphthalene 374 100 25 ug/l 103-65-1 n-Propylbenzene 140 100 25 ug/l 100-42-5 Styrene ND 100 25 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 100 25 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 100 25 ug/l 127-18-4 Tetrachloroethylene ND 100 25 ug/l 108-88-3 Toluene 7010 100 25 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 100 25 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 100 25 ug/l 71-55-6 1,1,1-Trichloroethane ND 100 25 ug/l 79-00-5 1,1,2-Trichloroethane ND 100 25 ug/l 79-01-6 Trichloroethylene ND 100 25 ug/l 75-69-4 Trichlorofluoromethane ND 100 40 ug/l 96-18-4 1,2,3-Trichloropropane ND 100 25 ug/l 95-63-6 1,2,4-Trimethylbenzene 1950 100 25 ug/l 108-67-8 1,3,5-Trimethylbenzene 578 100 25 ug/l 75-01-4 Vinyl Chloride ND 100 25 ug/l m,p-Xylene 4870 200 25 ug/l 95-47-6 o-Xylene 2250 100 25 ug/l 1330-20-7 Xylene (total)7120 300 50 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 100%70-130% 17060-07-0 1,2-Dichloroethane-D4 105%70-130% 2037-26-5 Toluene-D8 99%70-130% 460-00-4 4-Bromofluorobenzene 100%70-130% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 9 of 53 FA8232333.1 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID:MW-2 Lab Sample ID:FA82323-2 Date Sampled:01/12/21 Matrix:AQ - Ground Water Date Received:01/13/21 Method:SM 6200B Percent Solids:n/a Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 A0225134.D 500 01/14/21 13:48 LR n/a n/a VA2848 Run #2 Purge Volume Run #1 10.0 ml Run #2 VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene 5060 250 63 ug/l 108-86-1 Bromobenzene ND 250 63 ug/l 74-97-5 Bromochloromethane ND 250 63 ug/l 75-27-4 Bromodichloromethane ND 250 63 ug/l 75-25-2 Bromoform ND 250 63 ug/l 104-51-8 n-Butylbenzene ND 250 63 ug/l 135-98-8 sec-Butylbenzene ND 250 63 ug/l 98-06-6 tert-Butylbenzene ND 250 63 ug/l 56-23-5 Carbon Tetrachloride ND 250 63 ug/l 108-90-7 Chlorobenzene ND 250 63 ug/l 75-00-3 Chloroethane ND 250 100 ug/l 67-66-3 Chloroform ND 250 63 ug/l 95-49-8 o-Chlorotoluene ND 250 63 ug/l 106-43-4 p-Chlorotoluene ND 250 63 ug/l 124-48-1 Dibromochloromethane ND 250 63 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 250 120 ug/l 106-93-4 1,2-Dibromoethane ND 250 63 ug/l 75-71-8 Dichlorodifluoromethane ND 250 100 ug/l 95-50-1 1,2-Dichlorobenzene ND 250 63 ug/l 541-73-1 1,3-Dichlorobenzene ND 250 63 ug/l 106-46-7 1,4-Dichlorobenzene ND 250 63 ug/l 75-34-3 1,1-Dichloroethane ND 250 63 ug/l 107-06-2 1,2-Dichloroethane ND 250 63 ug/l 75-35-4 1,1-Dichloroethylene ND 250 63 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 250 63 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 250 63 ug/l 78-87-5 1,2-Dichloropropane ND 250 63 ug/l 142-28-9 1,3-Dichloropropane ND 250 63 ug/l 594-20-7 2,2-Dichloropropane ND 250 63 ug/l 563-58-6 1,1-Dichloropropene ND 250 63 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 250 63 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 250 63 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 10 of 53 FA8232333.2 SGS North America Inc. Report of Analysis Page 2 of 2 Client Sample ID:MW-2 Lab Sample ID:FA82323-2 Date Sampled:01/12/21 Matrix:AQ - Ground Water Date Received:01/13/21 Method:SM 6200B Percent Solids:n/a Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether ND 250 63 ug/l 100-41-4 Ethylbenzene 2370 250 63 ug/l 87-68-3 Hexachlorobutadiene ND 250 63 ug/l 98-82-8 Isopropylbenzene 110 250 63 ug/l J 99-87-6 p-Isopropyltoluene ND 250 63 ug/l 74-83-9 Methyl Bromide ND 250 100 ug/l 74-87-3 Methyl Chloride ND 250 100 ug/l 74-95-3 Methylene Bromide ND 250 63 ug/l 75-09-2 Methylene Chloride ND 1000 500 ug/l 1634-04-4 Methyl Tert Butyl Ether 2270 250 63 ug/l 91-20-3 Naphthalene 626 250 63 ug/l 103-65-1 n-Propylbenzene 270 250 63 ug/l 100-42-5 Styrene ND 250 63 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 250 63 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 250 63 ug/l 127-18-4 Tetrachloroethylene ND 250 63 ug/l 108-88-3 Toluene 15500 250 63 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 250 63 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 250 63 ug/l 71-55-6 1,1,1-Trichloroethane ND 250 63 ug/l 79-00-5 1,1,2-Trichloroethane ND 250 63 ug/l 79-01-6 Trichloroethylene ND 250 63 ug/l 75-69-4 Trichlorofluoromethane ND 250 100 ug/l 96-18-4 1,2,3-Trichloropropane ND 250 63 ug/l 95-63-6 1,2,4-Trimethylbenzene 2390 250 63 ug/l 108-67-8 1,3,5-Trimethylbenzene 685 250 63 ug/l 75-01-4 Vinyl Chloride ND 250 63 ug/l m,p-Xylene 8310 500 63 ug/l 95-47-6 o-Xylene 3430 250 63 ug/l 1330-20-7 Xylene (total)11700 750 130 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 101%70-130% 17060-07-0 1,2-Dichloroethane-D4 103%70-130% 2037-26-5 Toluene-D8 101%70-130% 460-00-4 4-Bromofluorobenzene 94%70-130% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 11 of 53 FA8232333.2 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID:MW-3 Lab Sample ID:FA82323-3 Date Sampled:01/12/21 Matrix:AQ - Ground Water Date Received:01/13/21 Method:SM 6200B Percent Solids:n/a Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 A0225135.D 500 01/14/21 14:11 LR n/a n/a VA2848 Run #2 Purge Volume Run #1 10.0 ml Run #2 VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene 3900 250 63 ug/l 108-86-1 Bromobenzene ND 250 63 ug/l 74-97-5 Bromochloromethane ND 250 63 ug/l 75-27-4 Bromodichloromethane ND 250 63 ug/l 75-25-2 Bromoform ND 250 63 ug/l 104-51-8 n-Butylbenzene ND 250 63 ug/l 135-98-8 sec-Butylbenzene ND 250 63 ug/l 98-06-6 tert-Butylbenzene ND 250 63 ug/l 56-23-5 Carbon Tetrachloride ND 250 63 ug/l 108-90-7 Chlorobenzene ND 250 63 ug/l 75-00-3 Chloroethane ND 250 100 ug/l 67-66-3 Chloroform ND 250 63 ug/l 95-49-8 o-Chlorotoluene ND 250 63 ug/l 106-43-4 p-Chlorotoluene ND 250 63 ug/l 124-48-1 Dibromochloromethane ND 250 63 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 250 120 ug/l 106-93-4 1,2-Dibromoethane ND 250 63 ug/l 75-71-8 Dichlorodifluoromethane ND 250 100 ug/l 95-50-1 1,2-Dichlorobenzene ND 250 63 ug/l 541-73-1 1,3-Dichlorobenzene ND 250 63 ug/l 106-46-7 1,4-Dichlorobenzene ND 250 63 ug/l 75-34-3 1,1-Dichloroethane ND 250 63 ug/l 107-06-2 1,2-Dichloroethane ND 250 63 ug/l 75-35-4 1,1-Dichloroethylene ND 250 63 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 250 63 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 250 63 ug/l 78-87-5 1,2-Dichloropropane ND 250 63 ug/l 142-28-9 1,3-Dichloropropane ND 250 63 ug/l 594-20-7 2,2-Dichloropropane ND 250 63 ug/l 563-58-6 1,1-Dichloropropene ND 250 63 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 250 63 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 250 63 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 12 of 53 FA8232333.3 SGS North America Inc. Report of Analysis Page 2 of 2 Client Sample ID:MW-3 Lab Sample ID:FA82323-3 Date Sampled:01/12/21 Matrix:AQ - Ground Water Date Received:01/13/21 Method:SM 6200B Percent Solids:n/a Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether ND 250 63 ug/l 100-41-4 Ethylbenzene 3290 250 63 ug/l 87-68-3 Hexachlorobutadiene ND 250 63 ug/l 98-82-8 Isopropylbenzene 137 250 63 ug/l J 99-87-6 p-Isopropyltoluene ND 250 63 ug/l 74-83-9 Methyl Bromide ND 250 100 ug/l 74-87-3 Methyl Chloride ND 250 100 ug/l 74-95-3 Methylene Bromide ND 250 63 ug/l 75-09-2 Methylene Chloride ND 1000 500 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 250 63 ug/l 91-20-3 Naphthalene 611 250 63 ug/l 103-65-1 n-Propylbenzene 346 250 63 ug/l 100-42-5 Styrene ND 250 63 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 250 63 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 250 63 ug/l 127-18-4 Tetrachloroethylene ND 250 63 ug/l 108-88-3 Toluene 23600 250 63 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 250 63 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 250 63 ug/l 71-55-6 1,1,1-Trichloroethane ND 250 63 ug/l 79-00-5 1,1,2-Trichloroethane ND 250 63 ug/l 79-01-6 Trichloroethylene ND 250 63 ug/l 75-69-4 Trichlorofluoromethane ND 250 100 ug/l 96-18-4 1,2,3-Trichloropropane ND 250 63 ug/l 95-63-6 1,2,4-Trimethylbenzene 2540 250 63 ug/l 108-67-8 1,3,5-Trimethylbenzene 692 250 63 ug/l 75-01-4 Vinyl Chloride ND 250 63 ug/l m,p-Xylene 10500 500 63 ug/l 95-47-6 o-Xylene 5060 250 63 ug/l 1330-20-7 Xylene (total)15600 750 130 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 100%70-130% 17060-07-0 1,2-Dichloroethane-D4 104%70-130% 2037-26-5 Toluene-D8 101%70-130% 460-00-4 4-Bromofluorobenzene 98%70-130% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 13 of 53 FA8232333.3 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID:MW-7 Lab Sample ID:FA82323-4 Date Sampled:01/12/21 Matrix:AQ - Ground Water Date Received:01/13/21 Method:SM 6200B Percent Solids:n/a Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 A0225181.D 1 01/19/21 12:37 LR n/a n/a VA2850 Run #2 Purge Volume Run #1 10.0 ml Run #2 VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.13 ug/l 108-86-1 Bromobenzene ND 0.50 0.13 ug/l 74-97-5 Bromochloromethane ND 0.50 0.13 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l 75-25-2 Bromoform ND 0.50 0.13 ug/l 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane ND 0.50 0.20 ug/l 67-66-3 Chloroform ND 0.50 0.13 ug/l 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l 75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l 75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l 563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 14 of 53 FA8232333.4 SGS North America Inc. Report of Analysis Page 2 of 2 Client Sample ID:MW-7 Lab Sample ID:FA82323-4 Date Sampled:01/12/21 Matrix:AQ - Ground Water Date Received:01/13/21 Method:SM 6200B Percent Solids:n/a Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l 100-41-4 Ethylbenzene ND 0.50 0.13 ug/l 87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l 74-83-9 Methyl Bromide ND 0.50 0.20 ug/l 74-87-3 Methyl Chloride ND 0.50 0.20 ug/l 74-95-3 Methylene Bromide ND 0.50 0.13 ug/l 75-09-2 Methylene Chloride ND 2.0 1.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l 91-20-3 Naphthalene ND 0.50 0.13 ug/l 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l 100-42-5 Styrene ND 0.50 0.13 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l 108-88-3 Toluene ND 0.50 0.13 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l 71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l 79-01-6 Trichloroethylene ND 0.50 0.13 ug/l 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l m,p-Xylene ND 1.0 0.13 ug/l 95-47-6 o-Xylene ND 0.50 0.13 ug/l 1330-20-7 Xylene (total)ND 1.5 0.25 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 99%70-130% 17060-07-0 1,2-Dichloroethane-D4 101%70-130% 2037-26-5 Toluene-D8 101%70-130% 460-00-4 4-Bromofluorobenzene 100%70-130% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 15 of 53 FA8232333.4 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID:MW-8 Lab Sample ID:FA82323-5 Date Sampled:01/12/21 Matrix:AQ - Ground Water Date Received:01/13/21 Method:SM 6200B Percent Solids:n/a Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 E105727.D 1 01/20/21 13:06 LR n/a n/a VE2415 Run #2 Purge Volume Run #1 10.0 ml Run #2 VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.13 ug/l 108-86-1 Bromobenzene ND 0.50 0.13 ug/l 74-97-5 Bromochloromethane ND 0.50 0.13 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l 75-25-2 Bromoform ND 0.50 0.13 ug/l 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane ND 0.50 0.20 ug/l 67-66-3 Chloroform ND 0.50 0.13 ug/l 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l 75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l 75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l 563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l 10061-01-5 cis-1,3-Dichloropropene a ND 0.50 0.13 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 16 of 53 FA8232333.5 SGS North America Inc. Report of Analysis Page 2 of 2 Client Sample ID:MW-8 Lab Sample ID:FA82323-5 Date Sampled:01/12/21 Matrix:AQ - Ground Water Date Received:01/13/21 Method:SM 6200B Percent Solids:n/a Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l 100-41-4 Ethylbenzene ND 0.50 0.13 ug/l 87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l 74-83-9 Methyl Bromide ND 0.50 0.20 ug/l 74-87-3 Methyl Chloride ND 0.50 0.20 ug/l 74-95-3 Methylene Bromide ND 0.50 0.13 ug/l 75-09-2 Methylene Chloride ND 2.0 1.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l 91-20-3 Naphthalene ND 0.50 0.13 ug/l 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l 100-42-5 Styrene ND 0.50 0.13 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l 108-88-3 Toluene ND 0.50 0.13 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l 71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l 79-01-6 Trichloroethylene ND 0.50 0.13 ug/l 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l m,p-Xylene ND 1.0 0.13 ug/l 95-47-6 o-Xylene ND 0.50 0.13 ug/l 1330-20-7 Xylene (total)ND 1.5 0.25 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 104%70-130% 17060-07-0 1,2-Dichloroethane-D4 102%70-130% 2037-26-5 Toluene-D8 87%70-130% 460-00-4 4-Bromofluorobenzene 103%70-130% (a) Associated CCV outside of control limits high, sample was ND. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 17 of 53 FA8232333.5 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID:MW-10 Lab Sample ID:FA82323-6 Date Sampled:01/12/21 Matrix:AQ - Ground Water Date Received:01/13/21 Method:SM 6200B Percent Solids:n/a Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 A0225131.D 1 01/14/21 12:39 LR n/a n/a VA2848 Run #2 Purge Volume Run #1 10.0 ml Run #2 VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.13 ug/l 108-86-1 Bromobenzene ND 0.50 0.13 ug/l 74-97-5 Bromochloromethane ND 0.50 0.13 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l 75-25-2 Bromoform ND 0.50 0.13 ug/l 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane ND 0.50 0.20 ug/l 67-66-3 Chloroform ND 0.50 0.13 ug/l 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l 75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l 75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l 563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 18 of 53 FA8232333.6 SGS North America Inc. Report of Analysis Page 2 of 2 Client Sample ID:MW-10 Lab Sample ID:FA82323-6 Date Sampled:01/12/21 Matrix:AQ - Ground Water Date Received:01/13/21 Method:SM 6200B Percent Solids:n/a Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l 100-41-4 Ethylbenzene ND 0.50 0.13 ug/l 87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l 74-83-9 Methyl Bromide ND 0.50 0.20 ug/l 74-87-3 Methyl Chloride ND 0.50 0.20 ug/l 74-95-3 Methylene Bromide ND 0.50 0.13 ug/l 75-09-2 Methylene Chloride ND 2.0 1.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l 91-20-3 Naphthalene ND 0.50 0.13 ug/l 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l 100-42-5 Styrene ND 0.50 0.13 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l 108-88-3 Toluene ND 0.50 0.13 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l 71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l 79-01-6 Trichloroethylene ND 0.50 0.13 ug/l 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l m,p-Xylene ND 1.0 0.13 ug/l 95-47-6 o-Xylene ND 0.50 0.13 ug/l 1330-20-7 Xylene (total)ND 1.5 0.25 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 101%70-130% 17060-07-0 1,2-Dichloroethane-D4 103%70-130% 2037-26-5 Toluene-D8 100%70-130% 460-00-4 4-Bromofluorobenzene 97%70-130% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 19 of 53 FA8232333.6 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID:MW-11 Lab Sample ID:FA82323-7 Date Sampled:01/12/21 Matrix:AQ - Ground Water Date Received:01/13/21 Method:SM 6200B Percent Solids:n/a Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 A0225132.D 1 01/14/21 13:02 LR n/a n/a VA2848 Run #2 Purge Volume Run #1 10.0 ml Run #2 VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.13 ug/l 108-86-1 Bromobenzene ND 0.50 0.13 ug/l 74-97-5 Bromochloromethane ND 0.50 0.13 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l 75-25-2 Bromoform ND 0.50 0.13 ug/l 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane ND 0.50 0.20 ug/l 67-66-3 Chloroform ND 0.50 0.13 ug/l 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l 75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l 75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l 563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 20 of 53 FA8232333.7 SGS North America Inc. Report of Analysis Page 2 of 2 Client Sample ID:MW-11 Lab Sample ID:FA82323-7 Date Sampled:01/12/21 Matrix:AQ - Ground Water Date Received:01/13/21 Method:SM 6200B Percent Solids:n/a Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l 100-41-4 Ethylbenzene ND 0.50 0.13 ug/l 87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l 74-83-9 Methyl Bromide ND 0.50 0.20 ug/l 74-87-3 Methyl Chloride ND 0.50 0.20 ug/l 74-95-3 Methylene Bromide ND 0.50 0.13 ug/l 75-09-2 Methylene Chloride ND 2.0 1.0 ug/l 1634-04-4 Methyl Tert Butyl Ether 14.2 0.50 0.13 ug/l 91-20-3 Naphthalene 0.23 0.50 0.13 ug/l J 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l 100-42-5 Styrene ND 0.50 0.13 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l 108-88-3 Toluene ND 0.50 0.13 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l 71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l 79-01-6 Trichloroethylene ND 0.50 0.13 ug/l 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l m,p-Xylene ND 1.0 0.13 ug/l 95-47-6 o-Xylene ND 0.50 0.13 ug/l 1330-20-7 Xylene (total)ND 1.5 0.25 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 100%70-130% 17060-07-0 1,2-Dichloroethane-D4 104%70-130% 2037-26-5 Toluene-D8 96%70-130% 460-00-4 4-Bromofluorobenzene 98%70-130% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 21 of 53 FA8232333.7 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID:MW-12 Lab Sample ID:FA82323-8 Date Sampled:01/12/21 Matrix:AQ - Ground Water Date Received:01/13/21 Method:SM 6200B Percent Solids:n/a Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 A0225144.D 1 01/14/21 17:38 LR n/a n/a VA2848 Run #2 Purge Volume Run #1 10.0 ml Run #2 VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.13 ug/l 108-86-1 Bromobenzene ND 0.50 0.13 ug/l 74-97-5 Bromochloromethane ND 0.50 0.13 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l 75-25-2 Bromoform ND 0.50 0.13 ug/l 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane ND 0.50 0.20 ug/l 67-66-3 Chloroform ND 0.50 0.13 ug/l 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l 75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l 75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l 563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 22 of 53 FA8232333.8 SGS North America Inc. Report of Analysis Page 2 of 2 Client Sample ID:MW-12 Lab Sample ID:FA82323-8 Date Sampled:01/12/21 Matrix:AQ - Ground Water Date Received:01/13/21 Method:SM 6200B Percent Solids:n/a Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l 100-41-4 Ethylbenzene ND 0.50 0.13 ug/l 87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l 74-83-9 Methyl Bromide ND 0.50 0.20 ug/l 74-87-3 Methyl Chloride ND 0.50 0.20 ug/l 74-95-3 Methylene Bromide ND 0.50 0.13 ug/l 75-09-2 Methylene Chloride ND 2.0 1.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l 91-20-3 Naphthalene ND 0.50 0.13 ug/l 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l 100-42-5 Styrene ND 0.50 0.13 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l 108-88-3 Toluene ND 0.50 0.13 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l 71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l 79-01-6 Trichloroethylene ND 0.50 0.13 ug/l 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l m,p-Xylene ND 1.0 0.13 ug/l 95-47-6 o-Xylene ND 0.50 0.13 ug/l 1330-20-7 Xylene (total)ND 1.5 0.25 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 102%70-130% 17060-07-0 1,2-Dichloroethane-D4 104%70-130% 2037-26-5 Toluene-D8 100%70-130% 460-00-4 4-Bromofluorobenzene 97%70-130% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 23 of 53 FA8232333.8 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID:MW-13 Lab Sample ID:FA82323-9 Date Sampled:01/12/21 Matrix:AQ - Ground Water Date Received:01/13/21 Method:SM 6200B Percent Solids:n/a Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 A0225147.D 2.5 01/14/21 18:47 LR n/a n/a VA2848 Run #2 Purge Volume Run #1 10.0 ml Run #2 VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene 104 1.3 0.31 ug/l 108-86-1 Bromobenzene ND 1.3 0.31 ug/l 74-97-5 Bromochloromethane ND 1.3 0.31 ug/l 75-27-4 Bromodichloromethane ND 1.3 0.31 ug/l 75-25-2 Bromoform ND 1.3 0.31 ug/l 104-51-8 n-Butylbenzene 1.2 1.3 0.31 ug/l J 135-98-8 sec-Butylbenzene 1.7 1.3 0.31 ug/l 98-06-6 tert-Butylbenzene ND 1.3 0.31 ug/l 56-23-5 Carbon Tetrachloride ND 1.3 0.31 ug/l 108-90-7 Chlorobenzene ND 1.3 0.31 ug/l 75-00-3 Chloroethane ND 1.3 0.50 ug/l 67-66-3 Chloroform ND 1.3 0.31 ug/l 95-49-8 o-Chlorotoluene ND 1.3 0.31 ug/l 106-43-4 p-Chlorotoluene ND 1.3 0.31 ug/l 124-48-1 Dibromochloromethane ND 1.3 0.31 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 1.3 0.62 ug/l 106-93-4 1,2-Dibromoethane ND 1.3 0.31 ug/l 75-71-8 Dichlorodifluoromethane ND 1.3 0.50 ug/l 95-50-1 1,2-Dichlorobenzene ND 1.3 0.31 ug/l 541-73-1 1,3-Dichlorobenzene ND 1.3 0.31 ug/l 106-46-7 1,4-Dichlorobenzene ND 1.3 0.31 ug/l 75-34-3 1,1-Dichloroethane ND 1.3 0.31 ug/l 107-06-2 1,2-Dichloroethane 0.76 1.3 0.31 ug/l J 75-35-4 1,1-Dichloroethylene ND 1.3 0.31 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 1.3 0.31 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 1.3 0.31 ug/l 78-87-5 1,2-Dichloropropane ND 1.3 0.31 ug/l 142-28-9 1,3-Dichloropropane ND 1.3 0.31 ug/l 594-20-7 2,2-Dichloropropane ND 1.3 0.31 ug/l 563-58-6 1,1-Dichloropropene ND 1.3 0.31 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 1.3 0.31 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 1.3 0.31 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 24 of 53 FA8232333.9 SGS North America Inc. Report of Analysis Page 2 of 2 Client Sample ID:MW-13 Lab Sample ID:FA82323-9 Date Sampled:01/12/21 Matrix:AQ - Ground Water Date Received:01/13/21 Method:SM 6200B Percent Solids:n/a Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether 0.84 1.3 0.31 ug/l J 100-41-4 Ethylbenzene 4.2 1.3 0.31 ug/l 87-68-3 Hexachlorobutadiene ND 1.3 0.31 ug/l 98-82-8 Isopropylbenzene 6.0 1.3 0.31 ug/l 99-87-6 p-Isopropyltoluene ND 1.3 0.31 ug/l 74-83-9 Methyl Bromide ND 1.3 0.50 ug/l 74-87-3 Methyl Chloride ND 1.3 0.50 ug/l 74-95-3 Methylene Bromide ND 1.3 0.31 ug/l 75-09-2 Methylene Chloride ND 5.0 2.5 ug/l 1634-04-4 Methyl Tert Butyl Ether 106 1.3 0.31 ug/l 91-20-3 Naphthalene 17.5 1.3 0.31 ug/l 103-65-1 n-Propylbenzene 9.3 1.3 0.31 ug/l 100-42-5 Styrene ND 1.3 0.31 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 1.3 0.31 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 1.3 0.31 ug/l 127-18-4 Tetrachloroethylene ND 1.3 0.31 ug/l 108-88-3 Toluene ND 1.3 0.31 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 1.3 0.31 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 1.3 0.31 ug/l 71-55-6 1,1,1-Trichloroethane ND 1.3 0.31 ug/l 79-00-5 1,1,2-Trichloroethane ND 1.3 0.31 ug/l 79-01-6 Trichloroethylene ND 1.3 0.31 ug/l 75-69-4 Trichlorofluoromethane ND 1.3 0.50 ug/l 96-18-4 1,2,3-Trichloropropane ND 1.3 0.31 ug/l 95-63-6 1,2,4-Trimethylbenzene 4.5 1.3 0.31 ug/l 108-67-8 1,3,5-Trimethylbenzene ND 1.3 0.31 ug/l 75-01-4 Vinyl Chloride ND 1.3 0.31 ug/l m,p-Xylene 10.7 2.5 0.31 ug/l 95-47-6 o-Xylene ND 1.3 0.31 ug/l 1330-20-7 Xylene (total)10.7 3.8 0.63 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 106%70-130% 17060-07-0 1,2-Dichloroethane-D4 108%70-130% 2037-26-5 Toluene-D8 93%70-130% 460-00-4 4-Bromofluorobenzene 94%70-130% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 25 of 53 FA8232333.9 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID:MW-24 Lab Sample ID:FA82323-10 Date Sampled:01/12/21 Matrix:AQ - Ground Water Date Received:01/13/21 Method:SM 6200B Percent Solids:n/a Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 A0225145.D 1 01/14/21 18:00 LR n/a n/a VA2848 Run #2 Purge Volume Run #1 10.0 ml Run #2 VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.13 ug/l 108-86-1 Bromobenzene ND 0.50 0.13 ug/l 74-97-5 Bromochloromethane ND 0.50 0.13 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l 75-25-2 Bromoform ND 0.50 0.13 ug/l 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane ND 0.50 0.20 ug/l 67-66-3 Chloroform ND 0.50 0.13 ug/l 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l 75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l 75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l 563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 26 of 53 FA8232333.10 SGS North America Inc. Report of Analysis Page 2 of 2 Client Sample ID:MW-24 Lab Sample ID:FA82323-10 Date Sampled:01/12/21 Matrix:AQ - Ground Water Date Received:01/13/21 Method:SM 6200B Percent Solids:n/a Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l 100-41-4 Ethylbenzene ND 0.50 0.13 ug/l 87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l 74-83-9 Methyl Bromide ND 0.50 0.20 ug/l 74-87-3 Methyl Chloride ND 0.50 0.20 ug/l 74-95-3 Methylene Bromide ND 0.50 0.13 ug/l 75-09-2 Methylene Chloride ND 2.0 1.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l 91-20-3 Naphthalene ND 0.50 0.13 ug/l 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l 100-42-5 Styrene ND 0.50 0.13 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l 108-88-3 Toluene ND 0.50 0.13 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l 71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l 79-01-6 Trichloroethylene ND 0.50 0.13 ug/l 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l m,p-Xylene ND 1.0 0.13 ug/l 95-47-6 o-Xylene ND 0.50 0.13 ug/l 1330-20-7 Xylene (total)ND 1.5 0.25 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 103%70-130% 17060-07-0 1,2-Dichloroethane-D4 104%70-130% 2037-26-5 Toluene-D8 99%70-130% 460-00-4 4-Bromofluorobenzene 94%70-130% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 27 of 53 FA8232333.10 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID:MW-25 Lab Sample ID:FA82323-11 Date Sampled:01/12/21 Matrix:AQ - Ground Water Date Received:01/13/21 Method:SM 6200B Percent Solids:n/a Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 A0225148.D 2.5 01/14/21 19:10 LR n/a n/a VA2848 Run #2 Purge Volume Run #1 10.0 ml Run #2 VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene ND 1.3 0.31 ug/l 108-86-1 Bromobenzene ND 1.3 0.31 ug/l 74-97-5 Bromochloromethane ND 1.3 0.31 ug/l 75-27-4 Bromodichloromethane ND 1.3 0.31 ug/l 75-25-2 Bromoform ND 1.3 0.31 ug/l 104-51-8 n-Butylbenzene ND 1.3 0.31 ug/l 135-98-8 sec-Butylbenzene ND 1.3 0.31 ug/l 98-06-6 tert-Butylbenzene ND 1.3 0.31 ug/l 56-23-5 Carbon Tetrachloride ND 1.3 0.31 ug/l 108-90-7 Chlorobenzene ND 1.3 0.31 ug/l 75-00-3 Chloroethane ND 1.3 0.50 ug/l 67-66-3 Chloroform ND 1.3 0.31 ug/l 95-49-8 o-Chlorotoluene ND 1.3 0.31 ug/l 106-43-4 p-Chlorotoluene ND 1.3 0.31 ug/l 124-48-1 Dibromochloromethane ND 1.3 0.31 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 1.3 0.62 ug/l 106-93-4 1,2-Dibromoethane ND 1.3 0.31 ug/l 75-71-8 Dichlorodifluoromethane ND 1.3 0.50 ug/l 95-50-1 1,2-Dichlorobenzene ND 1.3 0.31 ug/l 541-73-1 1,3-Dichlorobenzene ND 1.3 0.31 ug/l 106-46-7 1,4-Dichlorobenzene ND 1.3 0.31 ug/l 75-34-3 1,1-Dichloroethane ND 1.3 0.31 ug/l 107-06-2 1,2-Dichloroethane ND 1.3 0.31 ug/l 75-35-4 1,1-Dichloroethylene ND 1.3 0.31 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 1.3 0.31 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 1.3 0.31 ug/l 78-87-5 1,2-Dichloropropane ND 1.3 0.31 ug/l 142-28-9 1,3-Dichloropropane ND 1.3 0.31 ug/l 594-20-7 2,2-Dichloropropane ND 1.3 0.31 ug/l 563-58-6 1,1-Dichloropropene ND 1.3 0.31 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 1.3 0.31 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 1.3 0.31 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 28 of 53 FA8232333.11 SGS North America Inc. Report of Analysis Page 2 of 2 Client Sample ID:MW-25 Lab Sample ID:FA82323-11 Date Sampled:01/12/21 Matrix:AQ - Ground Water Date Received:01/13/21 Method:SM 6200B Percent Solids:n/a Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether ND 1.3 0.31 ug/l 100-41-4 Ethylbenzene ND 1.3 0.31 ug/l 87-68-3 Hexachlorobutadiene ND 1.3 0.31 ug/l 98-82-8 Isopropylbenzene ND 1.3 0.31 ug/l 99-87-6 p-Isopropyltoluene ND 1.3 0.31 ug/l 74-83-9 Methyl Bromide ND 1.3 0.50 ug/l 74-87-3 Methyl Chloride ND 1.3 0.50 ug/l 74-95-3 Methylene Bromide ND 1.3 0.31 ug/l 75-09-2 Methylene Chloride ND 5.0 2.5 ug/l 1634-04-4 Methyl Tert Butyl Ether 107 1.3 0.31 ug/l 91-20-3 Naphthalene ND 1.3 0.31 ug/l 103-65-1 n-Propylbenzene ND 1.3 0.31 ug/l 100-42-5 Styrene ND 1.3 0.31 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 1.3 0.31 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 1.3 0.31 ug/l 127-18-4 Tetrachloroethylene ND 1.3 0.31 ug/l 108-88-3 Toluene ND 1.3 0.31 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 1.3 0.31 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 1.3 0.31 ug/l 71-55-6 1,1,1-Trichloroethane ND 1.3 0.31 ug/l 79-00-5 1,1,2-Trichloroethane ND 1.3 0.31 ug/l 79-01-6 Trichloroethylene ND 1.3 0.31 ug/l 75-69-4 Trichlorofluoromethane ND 1.3 0.50 ug/l 96-18-4 1,2,3-Trichloropropane ND 1.3 0.31 ug/l 95-63-6 1,2,4-Trimethylbenzene ND 1.3 0.31 ug/l 108-67-8 1,3,5-Trimethylbenzene ND 1.3 0.31 ug/l 75-01-4 Vinyl Chloride ND 1.3 0.31 ug/l m,p-Xylene ND 2.5 0.31 ug/l 95-47-6 o-Xylene ND 1.3 0.31 ug/l 1330-20-7 Xylene (total)ND 3.8 0.63 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 100%70-130% 17060-07-0 1,2-Dichloroethane-D4 105%70-130% 2037-26-5 Toluene-D8 99%70-130% 460-00-4 4-Bromofluorobenzene 100%70-130% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 29 of 53 FA8232333.11 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID:MW-4 Lab Sample ID:FA82323-12 Date Sampled:01/12/21 Matrix:AQ - Ground Water Date Received:01/13/21 Method:SM 6200B Percent Solids:n/a Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 A0225146.D 1 01/14/21 18:24 LR n/a n/a VA2848 Run #2 Purge Volume Run #1 10.0 ml Run #2 VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.13 ug/l 108-86-1 Bromobenzene ND 0.50 0.13 ug/l 74-97-5 Bromochloromethane ND 0.50 0.13 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l 75-25-2 Bromoform ND 0.50 0.13 ug/l 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane ND 0.50 0.20 ug/l 67-66-3 Chloroform ND 0.50 0.13 ug/l 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l 75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l 75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l 563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 30 of 53 FA8232333.12 SGS North America Inc. Report of Analysis Page 2 of 2 Client Sample ID:MW-4 Lab Sample ID:FA82323-12 Date Sampled:01/12/21 Matrix:AQ - Ground Water Date Received:01/13/21 Method:SM 6200B Percent Solids:n/a Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l 100-41-4 Ethylbenzene ND 0.50 0.13 ug/l 87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l 74-83-9 Methyl Bromide ND 0.50 0.20 ug/l 74-87-3 Methyl Chloride ND 0.50 0.20 ug/l 74-95-3 Methylene Bromide ND 0.50 0.13 ug/l 75-09-2 Methylene Chloride ND 2.0 1.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l 91-20-3 Naphthalene ND 0.50 0.13 ug/l 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l 100-42-5 Styrene ND 0.50 0.13 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l 108-88-3 Toluene ND 0.50 0.13 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l 71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l 79-01-6 Trichloroethylene ND 0.50 0.13 ug/l 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l m,p-Xylene ND 1.0 0.13 ug/l 95-47-6 o-Xylene ND 0.50 0.13 ug/l 1330-20-7 Xylene (total)ND 1.5 0.25 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 99%70-130% 17060-07-0 1,2-Dichloroethane-D4 105%70-130% 2037-26-5 Toluene-D8 96%70-130% 460-00-4 4-Bromofluorobenzene 101%70-130% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 31 of 53 FA8232333.12 SGS North America Inc. Misc. Forms Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody Orlando, FL Section 4 32 of 53 FA823234 FA82323: Chain of Custody Page 1 of 2 33 of 53 FA8232344.1 Job Number:FA82323 Client:GEOLOGICAL RESOURCES INC Date / Time Received:1/13/2021 10:15:00 AM Delivery Method:FED EX Project:EVERRETT'S ENTERPRISE Airbill #'s:100963779851 Cooler Information 1. Custody Seals Present 2. Custody Seals Intact 4. Cooler temp verification 3. Temp criteria achieved 5. Cooler media IR Gun Ice (Bag) Trip Blank Information 1. Trip Blank present / cooler 2. Trip Blank listed on COC 2. Samples preserved properly Sample Information 1. Sample labels present on bottles 5. Sample recvd within HT 4. Condition of sample 3. Sufficient volume/containers recvd for analysis: Intact Comments SM001Rev. Date 05/24/17 SGS Sample Receipt Summary Cooler Temps (Raw Measured) °C: Cooler Temps (Corrected) °C: Cooler 1: (3.2); Cooler 1: (3.4); 3. Type Of TB Received W or S N/A 6. Dates/Times/IDs on COC match Sample Label 7. VOCs have headspace 8. Bottles received for unspecified tests 9. Compositing instructions clear 10. Voa Soil Kits/Jars received past 48hrs? 11. % Solids Jar received? Misc. Information 25-Gram 5-GramNumber of Encores:Number of 5035 Field Kits:Number of Lab Filtered Metals: Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify) Y or N N/A Y or N Therm ID:IR 1; Therm CF:0.2; # of Coolers:1 Y or N N/A 12. Residual Chlorine Present? Residual Chlorine Test Strip Lot #: Technician:Reviewer:CARLOSD Date:Date:1/13/2021 10:15:00 A FA82323: Chain of Custody Page 2 of 2 34 of 53 FA8232344.1 SGS North America Inc. MS Volatiles QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries Orlando, FL Section 5 35 of 53 FA823235 Method Blank Summary Page 1 of 2 Job Number:FA82323 Account:GRINCC GRI (Geological Resources Inc.) Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VA2848-MB A0225129.D 1 01/14/21 LR n/a n/a VA2848 The QC reported here applies to the following samples:Method: SM 6200B FA82323-1, FA82323-2, FA82323-3, FA82323-6, FA82323-7, FA82323-8, FA82323-9, FA82323-10, FA82323-11, FA82323-12 CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.13 ug/l 108-86-1 Bromobenzene ND 0.50 0.13 ug/l 74-97-5 Bromochloromethane ND 0.50 0.13 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l 75-25-2 Bromoform ND 0.50 0.13 ug/l 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane ND 0.50 0.20 ug/l 67-66-3 Chloroform ND 0.50 0.13 ug/l 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l 75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l 75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l 563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l 108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l 100-41-4 Ethylbenzene ND 0.50 0.13 ug/l 87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l 36 of 53 FA8232355.1.1 Method Blank Summary Page 2 of 2 Job Number:FA82323 Account:GRINCC GRI (Geological Resources Inc.) Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VA2848-MB A0225129.D 1 01/14/21 LR n/a n/a VA2848 The QC reported here applies to the following samples:Method: SM 6200B FA82323-1, FA82323-2, FA82323-3, FA82323-6, FA82323-7, FA82323-8, FA82323-9, FA82323-10, FA82323-11, FA82323-12 CAS No.Compound Result RL MDL Units Q 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l 74-83-9 Methyl Bromide ND 0.50 0.20 ug/l 74-87-3 Methyl Chloride ND 0.50 0.20 ug/l 74-95-3 Methylene Bromide ND 0.50 0.13 ug/l 75-09-2 Methylene Chloride ND 2.0 1.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l 91-20-3 Naphthalene ND 0.50 0.13 ug/l 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l 100-42-5 Styrene ND 0.50 0.13 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l 108-88-3 Toluene ND 0.50 0.13 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l 71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l 79-01-6 Trichloroethylene ND 0.50 0.13 ug/l 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l m,p-Xylene ND 1.0 0.13 ug/l 95-47-6 o-Xylene ND 0.50 0.13 ug/l 1330-20-7 Xylene (total)ND 1.5 0.25 ug/l CAS No.Surrogate Recoveries Limits 1868-53-7 Dibromofluoromethane 100%70-130% 17060-07-0 1,2-Dichloroethane-D4 103%70-130% 2037-26-5 Toluene-D8 99%70-130% 460-00-4 4-Bromofluorobenzene 100%70-130% 37 of 53 FA8232355.1.1 Method Blank Summary Page 1 of 2 Job Number:FA82323 Account:GRINCC GRI (Geological Resources Inc.) Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VA2850-MB A0225179.D 1 01/19/21 LR n/a n/a VA2850 The QC reported here applies to the following samples:Method: SM 6200B FA82323-4 CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.13 ug/l 108-86-1 Bromobenzene ND 0.50 0.13 ug/l 74-97-5 Bromochloromethane ND 0.50 0.13 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l 75-25-2 Bromoform ND 0.50 0.13 ug/l 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane ND 0.50 0.20 ug/l 67-66-3 Chloroform ND 0.50 0.13 ug/l 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l 75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l 75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l 563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l 108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l 100-41-4 Ethylbenzene ND 0.50 0.13 ug/l 87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l 38 of 53 FA8232355.1.2 Method Blank Summary Page 2 of 2 Job Number:FA82323 Account:GRINCC GRI (Geological Resources Inc.) Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VA2850-MB A0225179.D 1 01/19/21 LR n/a n/a VA2850 The QC reported here applies to the following samples:Method: SM 6200B FA82323-4 CAS No.Compound Result RL MDL Units Q 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l 74-83-9 Methyl Bromide ND 0.50 0.20 ug/l 74-87-3 Methyl Chloride ND 0.50 0.20 ug/l 74-95-3 Methylene Bromide ND 0.50 0.13 ug/l 75-09-2 Methylene Chloride ND 2.0 1.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l 91-20-3 Naphthalene ND 0.50 0.13 ug/l 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l 100-42-5 Styrene ND 0.50 0.13 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l 108-88-3 Toluene ND 0.50 0.13 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l 71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l 79-01-6 Trichloroethylene ND 0.50 0.13 ug/l 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l m,p-Xylene ND 1.0 0.13 ug/l 95-47-6 o-Xylene ND 0.50 0.13 ug/l 1330-20-7 Xylene (total)ND 1.5 0.25 ug/l CAS No.Surrogate Recoveries Limits 1868-53-7 Dibromofluoromethane 98%70-130% 17060-07-0 1,2-Dichloroethane-D4 102%70-130% 2037-26-5 Toluene-D8 102%70-130% 460-00-4 4-Bromofluorobenzene 100%70-130% 39 of 53 FA8232355.1.2 Method Blank Summary Page 1 of 2 Job Number:FA82323 Account:GRINCC GRI (Geological Resources Inc.) Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VE2415-MB E105724.D 1 01/20/21 LR n/a n/a VE2415 The QC reported here applies to the following samples:Method: SM 6200B FA82323-5 CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.13 ug/l 108-86-1 Bromobenzene ND 0.50 0.13 ug/l 74-97-5 Bromochloromethane ND 0.50 0.13 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l 75-25-2 Bromoform ND 0.50 0.13 ug/l 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane ND 0.50 0.20 ug/l 67-66-3 Chloroform ND 0.50 0.13 ug/l 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l 75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l 75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l 563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l 108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l 100-41-4 Ethylbenzene ND 0.50 0.13 ug/l 87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l 40 of 53 FA8232355.1.3 Method Blank Summary Page 2 of 2 Job Number:FA82323 Account:GRINCC GRI (Geological Resources Inc.) Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VE2415-MB E105724.D 1 01/20/21 LR n/a n/a VE2415 The QC reported here applies to the following samples:Method: SM 6200B FA82323-5 CAS No.Compound Result RL MDL Units Q 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l 74-83-9 Methyl Bromide ND 0.50 0.20 ug/l 74-87-3 Methyl Chloride ND 0.50 0.20 ug/l 74-95-3 Methylene Bromide ND 0.50 0.13 ug/l 75-09-2 Methylene Chloride ND 2.0 1.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l 91-20-3 Naphthalene ND 0.50 0.13 ug/l 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l 100-42-5 Styrene ND 0.50 0.13 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l 108-88-3 Toluene ND 0.50 0.13 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l 71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l 79-01-6 Trichloroethylene ND 0.50 0.13 ug/l 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l m,p-Xylene ND 1.0 0.13 ug/l 95-47-6 o-Xylene ND 0.50 0.13 ug/l 1330-20-7 Xylene (total)ND 1.5 0.25 ug/l CAS No.Surrogate Recoveries Limits 1868-53-7 Dibromofluoromethane 102%70-130% 17060-07-0 1,2-Dichloroethane-D4 99%70-130% 2037-26-5 Toluene-D8 88%70-130% 460-00-4 4-Bromofluorobenzene 103%70-130% 41 of 53 FA8232355.1.3 Blank Spike Summary Page 1 of 2 Job Number:FA82323 Account:GRINCC GRI (Geological Resources Inc.) Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VA2848-BS A0225127.D 1 01/14/21 LR n/a n/a VA2848 The QC reported here applies to the following samples:Method: SM 6200B FA82323-1, FA82323-2, FA82323-3, FA82323-6, FA82323-7, FA82323-8, FA82323-9, FA82323-10, FA82323-11, FA82323-12 Spike BSP BSP CAS No.Compound ug/l ug/l %Limits 71-43-2 Benzene 10 10.3 103 70-130 108-86-1 Bromobenzene 10 9.7 97 70-130 74-97-5 Bromochloromethane 10 9.4 94 70-130 75-27-4 Bromodichloromethane 10 10.3 103 70-130 75-25-2 Bromoform 10 9.5 95 70-130 104-51-8 n-Butylbenzene 10 9.8 98 70-130 135-98-8 sec-Butylbenzene 10 10.6 106 70-130 98-06-6 tert-Butylbenzene 10 10 100 70-130 56-23-5 Carbon Tetrachloride 10 12.0 120 70-130 108-90-7 Chlorobenzene 10 9.8 98 70-130 75-00-3 Chloroethane 10 8.8 88 60-140 67-66-3 Chloroform 10 10.4 104 70-130 95-49-8 o-Chlorotoluene 10 9.6 96 70-130 106-43-4 p-Chlorotoluene 10 9.6 96 70-130 124-48-1 Dibromochloromethane 10 9.6 96 70-130 96-12-8 1,2-Dibromo-3-chloropropane 10 8.3 83 70-130 106-93-4 1,2-Dibromoethane 10 9.3 93 70-130 75-71-8 Dichlorodifluoromethane 10 9.3 93 60-140 95-50-1 1,2-Dichlorobenzene 10 9.4 94 70-130 541-73-1 1,3-Dichlorobenzene 10 9.7 97 70-130 106-46-7 1,4-Dichlorobenzene 10 9.5 95 70-130 75-34-3 1,1-Dichloroethane 10 10.9 109 70-130 107-06-2 1,2-Dichloroethane 10 9.6 96 70-130 75-35-4 1,1-Dichloroethylene 10 11.6 116 70-130 156-59-2 cis-1,2-Dichloroethylene 10 10.4 104 70-130 156-60-5 trans-1,2-Dichloroethylene 10 10.7 107 70-130 78-87-5 1,2-Dichloropropane 10 9.8 98 70-130 142-28-9 1,3-Dichloropropane 10 9.1 91 70-130 594-20-7 2,2-Dichloropropane 10 10.7 107 70-130 563-58-6 1,1-Dichloropropene 10 10.5 105 70-130 10061-01-5 cis-1,3-Dichloropropene 10 9.4 94 70-130 10061-02-6 trans-1,3-Dichloropropene 10 9.5 95 70-130 108-20-3 Di-Isopropyl Ether 10 9.2 92 70-130 100-41-4 Ethylbenzene 10 10.1 101 70-130 87-68-3 Hexachlorobutadiene 10 11.5 115 70-130 98-82-8 Isopropylbenzene 10 10.2 102 70-130 * = Outside of Control Limits. 42 of 53 FA8232355.2.1 Blank Spike Summary Page 2 of 2 Job Number:FA82323 Account:GRINCC GRI (Geological Resources Inc.) Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VA2848-BS A0225127.D 1 01/14/21 LR n/a n/a VA2848 The QC reported here applies to the following samples:Method: SM 6200B FA82323-1, FA82323-2, FA82323-3, FA82323-6, FA82323-7, FA82323-8, FA82323-9, FA82323-10, FA82323-11, FA82323-12 Spike BSP BSP CAS No.Compound ug/l ug/l %Limits 99-87-6 p-Isopropyltoluene 10 10.5 105 70-130 74-83-9 Methyl Bromide 10 8.3 83 60-140 74-87-3 Methyl Chloride 10 9.5 95 60-140 74-95-3 Methylene Bromide 10 9.5 95 70-130 75-09-2 Methylene Chloride 10 10.2 102 70-130 1634-04-4 Methyl Tert Butyl Ether 10 9.0 90 70-130 91-20-3 Naphthalene 10 9.2 92 70-130 103-65-1 n-Propylbenzene 10 10.0 100 70-130 100-42-5 Styrene 10 9.6 96 70-130 630-20-6 1,1,1,2-Tetrachloroethane 10 9.8 98 70-130 79-34-5 1,1,2,2-Tetrachloroethane 10 8.8 88 70-130 127-18-4 Tetrachloroethylene 10 11.1 111 70-130 108-88-3 Toluene 10 10 100 70-130 87-61-6 1,2,3-Trichlorobenzene 10 9.6 96 70-130 120-82-1 1,2,4-Trichlorobenzene 10 9.7 97 70-130 71-55-6 1,1,1-Trichloroethane 10 11.3 113 70-130 79-00-5 1,1,2-Trichloroethane 10 9.4 94 70-130 79-01-6 Trichloroethylene 10 10.4 104 70-130 75-69-4 Trichlorofluoromethane 10 11.4 114 60-140 96-18-4 1,2,3-Trichloropropane 10 9.0 90 70-130 95-63-6 1,2,4-Trimethylbenzene 10 9.4 94 70-130 108-67-8 1,3,5-Trimethylbenzene 10 9.8 98 70-130 75-01-4 Vinyl Chloride 10 9.7 97 60-140 m,p-Xylene 20 20.0 100 70-130 95-47-6 o-Xylene 10 9.7 97 70-130 1330-20-7 Xylene (total)30 29.7 99 70-130 CAS No.Surrogate Recoveries BSP Limits 1868-53-7 Dibromofluoromethane 103%70-130% 17060-07-0 1,2-Dichloroethane-D4 100%70-130% 2037-26-5 Toluene-D8 101%70-130% 460-00-4 4-Bromofluorobenzene 97%70-130% * = Outside of Control Limits. 43 of 53 FA8232355.2.1 Blank Spike Summary Page 1 of 2 Job Number:FA82323 Account:GRINCC GRI (Geological Resources Inc.) Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VA2850-BS A0225177.D 1 01/19/21 LR n/a n/a VA2850 The QC reported here applies to the following samples:Method: SM 6200B FA82323-4 Spike BSP BSP CAS No.Compound ug/l ug/l %Limits 71-43-2 Benzene 10 9.6 96 70-130 108-86-1 Bromobenzene 10 9.3 93 70-130 74-97-5 Bromochloromethane 10 9.0 90 70-130 75-27-4 Bromodichloromethane 10 9.7 97 70-130 75-25-2 Bromoform 10 8.4 84 70-130 104-51-8 n-Butylbenzene 10 9.5 95 70-130 135-98-8 sec-Butylbenzene 10 9.9 99 70-130 98-06-6 tert-Butylbenzene 10 9.5 95 70-130 56-23-5 Carbon Tetrachloride 10 10.5 105 70-130 108-90-7 Chlorobenzene 10 9.2 92 70-130 75-00-3 Chloroethane 10 7.5 75 60-140 67-66-3 Chloroform 10 9.4 94 70-130 95-49-8 o-Chlorotoluene 10 9.2 92 70-130 106-43-4 p-Chlorotoluene 10 9.3 93 70-130 124-48-1 Dibromochloromethane 10 9.2 92 70-130 96-12-8 1,2-Dibromo-3-chloropropane 10 8.4 84 70-130 106-93-4 1,2-Dibromoethane 10 9.3 93 70-130 75-71-8 Dichlorodifluoromethane 10 7.5 75 60-140 95-50-1 1,2-Dichlorobenzene 10 9.3 93 70-130 541-73-1 1,3-Dichlorobenzene 10 9.5 95 70-130 106-46-7 1,4-Dichlorobenzene 10 9.0 90 70-130 75-34-3 1,1-Dichloroethane 10 10.1 101 70-130 107-06-2 1,2-Dichloroethane 10 9.3 93 70-130 75-35-4 1,1-Dichloroethylene 10 10.1 101 70-130 156-59-2 cis-1,2-Dichloroethylene 10 9.7 97 70-130 156-60-5 trans-1,2-Dichloroethylene 10 9.9 99 70-130 78-87-5 1,2-Dichloropropane 10 9.4 94 70-130 142-28-9 1,3-Dichloropropane 10 9.1 91 70-130 594-20-7 2,2-Dichloropropane 10 10 100 70-130 563-58-6 1,1-Dichloropropene 10 9.6 96 70-130 10061-01-5 cis-1,3-Dichloropropene 10 8.9 89 70-130 10061-02-6 trans-1,3-Dichloropropene 10 9.2 92 70-130 108-20-3 Di-Isopropyl Ether 10 8.9 89 70-130 100-41-4 Ethylbenzene 10 9.3 93 70-130 87-68-3 Hexachlorobutadiene 10 10.2 102 70-130 98-82-8 Isopropylbenzene 10 9.5 95 70-130 * = Outside of Control Limits. 44 of 53 FA8232355.2.2 Blank Spike Summary Page 2 of 2 Job Number:FA82323 Account:GRINCC GRI (Geological Resources Inc.) Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VA2850-BS A0225177.D 1 01/19/21 LR n/a n/a VA2850 The QC reported here applies to the following samples:Method: SM 6200B FA82323-4 Spike BSP BSP CAS No.Compound ug/l ug/l %Limits 99-87-6 p-Isopropyltoluene 10 10.0 100 70-130 74-83-9 Methyl Bromide 10 7.5 75 60-140 74-87-3 Methyl Chloride 10 8.8 88 60-140 74-95-3 Methylene Bromide 10 9.1 91 70-130 75-09-2 Methylene Chloride 10 9.6 96 70-130 1634-04-4 Methyl Tert Butyl Ether 10 8.8 88 70-130 91-20-3 Naphthalene 10 9.2 92 70-130 103-65-1 n-Propylbenzene 10 9.4 94 70-130 100-42-5 Styrene 10 9.2 92 70-130 630-20-6 1,1,1,2-Tetrachloroethane 10 9.4 94 70-130 79-34-5 1,1,2,2-Tetrachloroethane 10 8.8 88 70-130 127-18-4 Tetrachloroethylene 10 10 100 70-130 108-88-3 Toluene 10 9.4 94 70-130 87-61-6 1,2,3-Trichlorobenzene 10 9.5 95 70-130 120-82-1 1,2,4-Trichlorobenzene 10 9.6 96 70-130 71-55-6 1,1,1-Trichloroethane 10 10 100 70-130 79-00-5 1,1,2-Trichloroethane 10 9.2 92 70-130 79-01-6 Trichloroethylene 10 9.4 94 70-130 75-69-4 Trichlorofluoromethane 10 9.2 92 60-140 96-18-4 1,2,3-Trichloropropane 10 9.1 91 70-130 95-63-6 1,2,4-Trimethylbenzene 10 9.1 91 70-130 108-67-8 1,3,5-Trimethylbenzene 10 9.4 94 70-130 75-01-4 Vinyl Chloride 10 8.7 87 60-140 m,p-Xylene 20 18.7 94 70-130 95-47-6 o-Xylene 10 9.3 93 70-130 1330-20-7 Xylene (total)30 28.0 93 70-130 CAS No.Surrogate Recoveries BSP Limits 1868-53-7 Dibromofluoromethane 100%70-130% 17060-07-0 1,2-Dichloroethane-D4 100%70-130% 2037-26-5 Toluene-D8 100%70-130% 460-00-4 4-Bromofluorobenzene 101%70-130% * = Outside of Control Limits. 45 of 53 FA8232355.2.2 Blank Spike Summary Page 1 of 2 Job Number:FA82323 Account:GRINCC GRI (Geological Resources Inc.) Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VE2415-BS E105722.D 1 01/20/21 LR n/a n/a VE2415 The QC reported here applies to the following samples:Method: SM 6200B FA82323-5 Spike BSP BSP CAS No.Compound ug/l ug/l %Limits 71-43-2 Benzene 10 11.2 112 70-130 108-86-1 Bromobenzene 10 8.5 85 70-130 74-97-5 Bromochloromethane 10 10.1 101 70-130 75-27-4 Bromodichloromethane 10 11.5 115 70-130 75-25-2 Bromoform 10 8.8 88 70-130 104-51-8 n-Butylbenzene 10 8.5 85 70-130 135-98-8 sec-Butylbenzene 10 9.0 90 70-130 98-06-6 tert-Butylbenzene 10 8.5 85 70-130 56-23-5 Carbon Tetrachloride 10 11.6 116 70-130 108-90-7 Chlorobenzene 10 8.6 86 70-130 75-00-3 Chloroethane 10 9.4 94 60-140 67-66-3 Chloroform 10 10.6 106 70-130 95-49-8 o-Chlorotoluene 10 8.4 84 70-130 106-43-4 p-Chlorotoluene 10 8.5 85 70-130 124-48-1 Dibromochloromethane 10 8.8 88 70-130 96-12-8 1,2-Dibromo-3-chloropropane 10 7.6 76 70-130 106-93-4 1,2-Dibromoethane 10 8.9 89 70-130 75-71-8 Dichlorodifluoromethane 10 8.4 84 60-140 95-50-1 1,2-Dichlorobenzene 10 7.8 78 70-130 541-73-1 1,3-Dichlorobenzene 10 8.4 84 70-130 106-46-7 1,4-Dichlorobenzene 10 8.4 84 70-130 75-34-3 1,1-Dichloroethane 10 11.4 114 70-130 107-06-2 1,2-Dichloroethane 10 10.3 103 70-130 75-35-4 1,1-Dichloroethylene 10 11.9 119 70-130 156-59-2 cis-1,2-Dichloroethylene 10 11.4 114 70-130 156-60-5 trans-1,2-Dichloroethylene 10 11.3 113 70-130 78-87-5 1,2-Dichloropropane 10 11.0 110 70-130 142-28-9 1,3-Dichloropropane 10 8.4 84 70-130 594-20-7 2,2-Dichloropropane 10 11.5 115 70-130 563-58-6 1,1-Dichloropropene 10 11.0 110 70-130 10061-01-5 cis-1,3-Dichloropropene 10 11.5 115 70-130 10061-02-6 trans-1,3-Dichloropropene 10 9.5 95 70-130 108-20-3 Di-Isopropyl Ether 10 9.9 99 70-130 100-41-4 Ethylbenzene 10 8.8 88 70-130 87-68-3 Hexachlorobutadiene 10 8.1 81 70-130 98-82-8 Isopropylbenzene 10 8.9 89 70-130 * = Outside of Control Limits. 46 of 53 FA8232355.2.3 Blank Spike Summary Page 2 of 2 Job Number:FA82323 Account:GRINCC GRI (Geological Resources Inc.) Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VE2415-BS E105722.D 1 01/20/21 LR n/a n/a VE2415 The QC reported here applies to the following samples:Method: SM 6200B FA82323-5 Spike BSP BSP CAS No.Compound ug/l ug/l %Limits 99-87-6 p-Isopropyltoluene 10 9.0 90 70-130 74-83-9 Methyl Bromide 10 8.4 84 60-140 74-87-3 Methyl Chloride 10 9.3 93 60-140 74-95-3 Methylene Bromide 10 10.7 107 70-130 75-09-2 Methylene Chloride 10 10.1 101 70-130 1634-04-4 Methyl Tert Butyl Ether 10 9.9 99 70-130 91-20-3 Naphthalene 10 7.8 78 70-130 103-65-1 n-Propylbenzene 10 8.6 86 70-130 100-42-5 Styrene 10 9.2 92 70-130 630-20-6 1,1,1,2-Tetrachloroethane 10 8.3 83 70-130 79-34-5 1,1,2,2-Tetrachloroethane 10 8.2 82 70-130 127-18-4 Tetrachloroethylene 10 9.3 93 70-130 108-88-3 Toluene 10 8.8 88 70-130 87-61-6 1,2,3-Trichlorobenzene 10 7.5 75 70-130 120-82-1 1,2,4-Trichlorobenzene 10 7.8 78 70-130 71-55-6 1,1,1-Trichloroethane 10 11.2 112 70-130 79-00-5 1,1,2-Trichloroethane 10 8.7 87 70-130 79-01-6 Trichloroethylene 10 11.3 113 70-130 75-69-4 Trichlorofluoromethane 10 9.8 98 60-140 96-18-4 1,2,3-Trichloropropane 10 8.4 84 70-130 95-63-6 1,2,4-Trimethylbenzene 10 8.3 83 70-130 108-67-8 1,3,5-Trimethylbenzene 10 8.6 86 70-130 75-01-4 Vinyl Chloride 10 9.6 96 60-140 m,p-Xylene 20 18.0 90 70-130 95-47-6 o-Xylene 10 8.7 87 70-130 1330-20-7 Xylene (total)30 26.7 89 70-130 CAS No.Surrogate Recoveries BSP Limits 1868-53-7 Dibromofluoromethane 104%70-130% 17060-07-0 1,2-Dichloroethane-D4 101%70-130% 2037-26-5 Toluene-D8 89%70-130% 460-00-4 4-Bromofluorobenzene 102%70-130% * = Outside of Control Limits. 47 of 53 FA8232355.2.3 Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2 Job Number:FA82323 Account:GRINCC GRI (Geological Resources Inc.) Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA82331-8MS A0225140.D 5 01/14/21 LR n/a n/a VA2848 FA82331-8MSD A0225141.D 5 01/14/21 LR n/a n/a VA2848 FA82331-8 A0225130.D 1 01/14/21 LR n/a n/a VA2848 The QC reported here applies to the following samples:Method: SM 6200B FA82323-1, FA82323-2, FA82323-3, FA82323-6, FA82323-7, FA82323-8, FA82323-9, FA82323-10, FA82323-11, FA82323-12 FA82331-8 Spike MS MS Spike MSD MSD Limits CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD 71-43-2 Benzene ND 50 50.8 102 50 53.3 107 5 70-130/20 108-86-1 Bromobenzene ND 50 49.4 99 50 50.4 101 2 70-130/20 74-97-5 Bromochloromethane ND 50 46.4 93 50 49.3 99 6 70-130/20 75-27-4 Bromodichloromethane ND 50 48.3 97 50 51.6 103 7 70-130/20 75-25-2 Bromoform ND 50 36.9 74 50 39.5 79 7 70-130/20 104-51-8 n-Butylbenzene ND 50 46.3 93 50 49.7 99 7 70-130/20 135-98-8 sec-Butylbenzene ND 50 51.8 104 50 54.6 109 5 70-130/20 98-06-6 tert-Butylbenzene ND 50 48.7 97 50 51.8 104 6 70-130/20 56-23-5 Carbon Tetrachloride ND 50 57.8 116 50 66.4 133*14 70-130/20 108-90-7 Chlorobenzene ND 50 48.7 97 50 50.8 102 4 70-130/20 75-00-3 Chloroethane ND 50 49.6 99 50 53.0 106 7 60-140/20 67-66-3 Chloroform ND 50 50.5 101 50 53.1 106 5 70-130/20 95-49-8 o-Chlorotoluene ND 50 47.8 96 50 50.0 100 4 70-130/20 106-43-4 p-Chlorotoluene ND 50 48.0 96 50 49.3 99 3 70-130/20 124-48-1 Dibromochloromethane ND 50 42.2 84 50 45.2 90 7 70-130/20 96-12-8 1,2-Dibromo-3-chloropropane ND 50 36.9 74 50 40.3 81 9 70-130/20 106-93-4 1,2-Dibromoethane ND 50 46.0 92 50 47.0 94 2 70-130/20 75-71-8 Dichlorodifluoromethane ND 50 45.4 91 50 53.1 106 16 60-140/20 95-50-1 1,2-Dichlorobenzene ND 50 45.6 91 50 48.9 98 7 70-130/20 541-73-1 1,3-Dichlorobenzene ND 50 47.9 96 50 50.2 100 5 70-130/20 106-46-7 1,4-Dichlorobenzene ND 50 46.7 93 50 48.6 97 4 70-130/20 75-34-3 1,1-Dichloroethane ND 50 52.9 106 50 56.4 113 6 70-130/20 107-06-2 1,2-Dichloroethane ND 50 48.7 97 50 50.0 100 3 70-130/20 75-35-4 1,1-Dichloroethylene ND 50 55.8 112 50 59.2 118 6 70-130/20 156-59-2 cis-1,2-Dichloroethylene ND 50 51.1 102 50 54.7 109 7 70-130/20 156-60-5 trans-1,2-Dichloroethylene ND 50 52.1 104 50 56.1 112 7 70-130/20 78-87-5 1,2-Dichloropropane ND 50 49.2 98 50 50.7 101 3 70-130/20 142-28-9 1,3-Dichloropropane ND 50 46.0 92 50 47.0 94 2 70-130/20 594-20-7 2,2-Dichloropropane ND 50 48.7 97 50 54.9 110 12 70-130/20 563-58-6 1,1-Dichloropropene ND 50 52.0 104 50 55.2 110 6 70-130/20 10061-01-5 cis-1,3-Dichloropropene ND 50 45.0 90 50 45.5 91 1 70-130/20 10061-02-6 trans-1,3-Dichloropropene ND 50 45.5 91 50 46.9 94 3 70-130/20 108-20-3 Di-Isopropyl Ether ND 50 44.8 90 50 47.4 95 6 70-130/20 100-41-4 Ethylbenzene ND 50 49.5 99 50 52.5 105 6 70-130/20 87-68-3 Hexachlorobutadiene ND 50 49.9 100 50 58.5 117 16 70-130/20 98-82-8 Isopropylbenzene ND 50 49.2 98 50 53.2 106 8 70-130/20 * = Outside of Control Limits. 48 of 53 FA8232355.3.1 Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2 Job Number:FA82323 Account:GRINCC GRI (Geological Resources Inc.) Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA82331-8MS A0225140.D 5 01/14/21 LR n/a n/a VA2848 FA82331-8MSD A0225141.D 5 01/14/21 LR n/a n/a VA2848 FA82331-8 A0225130.D 1 01/14/21 LR n/a n/a VA2848 The QC reported here applies to the following samples:Method: SM 6200B FA82323-1, FA82323-2, FA82323-3, FA82323-6, FA82323-7, FA82323-8, FA82323-9, FA82323-10, FA82323-11, FA82323-12 FA82331-8 Spike MS MS Spike MSD MSD Limits CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD 99-87-6 p-Isopropyltoluene ND 50 50.9 102 50 54.2 108 6 70-130/20 74-83-9 Methyl Bromide ND 50 53.0 106 50 54.0 108 2 60-140/20 74-87-3 Methyl Chloride ND 50 46.9 94 50 51.4 103 9 60-140/20 74-95-3 Methylene Bromide ND 50 47.9 96 50 49.2 98 3 70-130/20 75-09-2 Methylene Chloride ND 50 49.7 99 50 54.9 110 10 70-130/20 1634-04-4 Methyl Tert Butyl Ether ND 50 43.1 86 50 46.3 93 7 70-130/20 91-20-3 Naphthalene ND 50 39.8 80 50 46.2 92 15 70-130/20 103-65-1 n-Propylbenzene ND 50 49.8 100 50 51.8 104 4 70-130/20 100-42-5 Styrene ND 50 44.6 89 50 46.3 93 4 70-130/20 630-20-6 1,1,1,2-Tetrachloroethane ND 50 45.8 92 50 51.5 103 12 70-130/20 79-34-5 1,1,2,2-Tetrachloroethane ND 50 43.3 87 50 44.6 89 3 70-130/20 127-18-4 Tetrachloroethylene ND 50 54.7 109 50 58.6 117 7 70-130/20 108-88-3 Toluene ND 50 49.2 98 50 52.2 104 6 70-130/20 87-61-6 1,2,3-Trichlorobenzene ND 50 42.0 84 50 48.7 97 15 70-130/20 120-82-1 1,2,4-Trichlorobenzene ND 50 42.7 85 50 49.5 99 15 70-130/20 71-55-6 1,1,1-Trichloroethane ND 50 54.9 110 50 59.9 120 9 70-130/20 79-00-5 1,1,2-Trichloroethane ND 50 47.3 95 50 47.8 96 1 70-130/20 79-01-6 Trichloroethylene ND 50 51.0 102 50 53.6 107 5 70-130/20 75-69-4 Trichlorofluoromethane ND 50 57.4 115 50 67.2 134 16 60-140/20 96-18-4 1,2,3-Trichloropropane ND 50 44.7 89 50 46.1 92 3 70-130/20 95-63-6 1,2,4-Trimethylbenzene ND 50 46.0 92 50 48.7 97 6 70-130/20 108-67-8 1,3,5-Trimethylbenzene ND 50 48.5 97 50 51.0 102 5 70-130/20 75-01-4 Vinyl Chloride ND 50 46.8 94 50 54.8 110 16 60-140/20 m,p-Xylene ND 100 97.3 97 100 103 103 6 70-130/20 95-47-6 o-Xylene ND 50 46.9 94 50 50.6 101 8 70-130/20 1330-20-7 Xylene (total)ND 150 144 96 150 153 102 6 70-130/20 CAS No.Surrogate Recoveries MS MSD FA82331-8 Limits 1868-53-7 Dibromofluoromethane 102%103%100%70-130% 17060-07-0 1,2-Dichloroethane-D4 101%101%102%70-130% 2037-26-5 Toluene-D8 99%101%100%70-130% 460-00-4 4-Bromofluorobenzene 99%95%100%70-130% * = Outside of Control Limits. 49 of 53 FA8232355.3.1 Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2 Job Number:FA82323 Account:GRINCC GRI (Geological Resources Inc.) Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA82331-5MS A0225190.D 2000 01/19/21 LR n/a n/a VA2850 FA82331-5MSD A0225191.D 2000 01/19/21 LR n/a n/a VA2850 FA82331-5 A0225183.D 2000 01/19/21 LR n/a n/a VA2850 The QC reported here applies to the following samples:Method: SM 6200B FA82323-4 FA82331-5 Spike MS MS Spike MSD MSD Limits CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD 71-43-2 Benzene 13800 20000 34600 104 20000 33400 98 4 70-130/20 108-86-1 Bromobenzene ND 20000 19900 100 20000 19700 99 1 70-130/20 74-97-5 Bromochloromethane ND 20000 19700 99 20000 18800 94 5 70-130/20 75-27-4 Bromodichloromethane ND 20000 20400 102 20000 20300 102 0 70-130/20 75-25-2 Bromoform ND 20000 17900 90 20000 18100 91 1 70-130/20 104-51-8 n-Butylbenzene ND 20000 20500 103 20000 19400 97 6 70-130/20 135-98-8 sec-Butylbenzene ND 20000 21400 107 20000 20500 103 4 70-130/20 98-06-6 tert-Butylbenzene ND 20000 20700 104 20000 19700 99 5 70-130/20 56-23-5 Carbon Tetrachloride ND 20000 22500 113 20000 21900 110 3 70-130/20 108-90-7 Chlorobenzene ND 20000 19900 100 20000 19300 97 3 70-130/20 75-00-3 Chloroethane ND 20000 17900 90 20000 22300 112 22*60-140/20 67-66-3 Chloroform ND 20000 20600 103 20000 19800 99 4 70-130/20 95-49-8 o-Chlorotoluene ND 20000 20200 101 20000 19400 97 4 70-130/20 106-43-4 p-Chlorotoluene ND 20000 20100 101 20000 19600 98 3 70-130/20 124-48-1 Dibromochloromethane ND 20000 19500 98 20000 19100 96 2 70-130/20 96-12-8 1,2-Dibromo-3-chloropropane ND 20000 17700 89 20000 16500 83 7 70-130/20 106-93-4 1,2-Dibromoethane ND 20000 19200 96 20000 19100 96 1 70-130/20 75-71-8 Dichlorodifluoromethane ND 20000 15300 77 20000 17300 87 12 60-140/20 95-50-1 1,2-Dichlorobenzene ND 20000 20000 100 20000 19000 95 5 70-130/20 541-73-1 1,3-Dichlorobenzene ND 20000 20400 102 20000 19700 99 3 70-130/20 106-46-7 1,4-Dichlorobenzene ND 20000 19500 98 20000 18900 95 3 70-130/20 75-34-3 1,1-Dichloroethane ND 20000 22100 111 20000 21200 106 4 70-130/20 107-06-2 1,2-Dichloroethane ND 20000 20000 100 20000 19600 98 2 70-130/20 75-35-4 1,1-Dichloroethylene ND 20000 21900 110 20000 21000 105 4 70-130/20 156-59-2 cis-1,2-Dichloroethylene ND 20000 21500 108 20000 20300 102 6 70-130/20 156-60-5 trans-1,2-Dichloroethylene ND 20000 21500 108 20000 20500 103 5 70-130/20 78-87-5 1,2-Dichloropropane ND 20000 19900 100 20000 19500 98 2 70-130/20 142-28-9 1,3-Dichloropropane ND 20000 19000 95 20000 18800 94 1 70-130/20 594-20-7 2,2-Dichloropropane ND 20000 22600 113 20000 21000 105 7 70-130/20 563-58-6 1,1-Dichloropropene ND 20000 20700 104 20000 20000 100 3 70-130/20 10061-01-5 cis-1,3-Dichloropropene ND 20000 17800 89 20000 18000 90 1 70-130/20 10061-02-6 trans-1,3-Dichloropropene ND 20000 18200 91 20000 18200 91 0 70-130/20 108-20-3 Di-Isopropyl Ether 2250 20000 21700 97 20000 20800 93 4 70-130/20 100-41-4 Ethylbenzene 3340 20000 24000 103 20000 22800 97 5 70-130/20 87-68-3 Hexachlorobutadiene ND 20000 22000 110 20000 19800 99 11 70-130/20 98-82-8 Isopropylbenzene ND 20000 21300 107 20000 20000 100 6 70-130/20 * = Outside of Control Limits. 50 of 53 FA8232355.3.2 Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2 Job Number:FA82323 Account:GRINCC GRI (Geological Resources Inc.) Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA82331-5MS A0225190.D 2000 01/19/21 LR n/a n/a VA2850 FA82331-5MSD A0225191.D 2000 01/19/21 LR n/a n/a VA2850 FA82331-5 A0225183.D 2000 01/19/21 LR n/a n/a VA2850 The QC reported here applies to the following samples:Method: SM 6200B FA82323-4 FA82331-5 Spike MS MS Spike MSD MSD Limits CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD 99-87-6 p-Isopropyltoluene ND 20000 21900 110 20000 20800 104 5 70-130/20 74-83-9 Methyl Bromide ND 20000 21300 107 20000 22300 112 5 60-140/20 74-87-3 Methyl Chloride ND 20000 17600 88 20000 20600 103 16 60-140/20 74-95-3 Methylene Bromide ND 20000 19300 97 20000 19100 96 1 70-130/20 75-09-2 Methylene Chloride ND 20000 21100 106 20000 20000 100 5 70-130/20 1634-04-4 Methyl Tert Butyl Ether ND 20000 19000 95 20000 18200 91 4 70-130/20 91-20-3 Naphthalene 504 J 20000 20400 99 20000 18200 88 11 70-130/20 103-65-1 n-Propylbenzene 392 J 20000 20800 102 20000 20100 99 3 70-130/20 100-42-5 Styrene ND 20000 19900 100 20000 19400 97 3 70-130/20 630-20-6 1,1,1,2-Tetrachloroethane ND 20000 20600 103 20000 19500 98 5 70-130/20 79-34-5 1,1,2,2-Tetrachloroethane ND 20000 18800 94 20000 18000 90 4 70-130/20 127-18-4 Tetrachloroethylene ND 20000 22000 110 20000 20800 104 6 70-130/20 108-88-3 Toluene 67200 20000 88800 108 20000 83400 81 6 70-130/20 87-61-6 1,2,3-Trichlorobenzene ND 20000 20300 102 20000 18200 91 11 70-130/20 120-82-1 1,2,4-Trichlorobenzene ND 20000 21100 106 20000 18900 95 11 70-130/20 71-55-6 1,1,1-Trichloroethane ND 20000 22100 111 20000 21100 106 5 70-130/20 79-00-5 1,1,2-Trichloroethane ND 20000 19700 99 20000 19500 98 1 70-130/20 79-01-6 Trichloroethylene ND 20000 20100 101 20000 19700 99 2 70-130/20 75-69-4 Trichlorofluoromethane ND 20000 20000 100 20000 22700 114 13 60-140/20 96-18-4 1,2,3-Trichloropropane ND 20000 19000 95 20000 18900 95 1 70-130/20 95-63-6 1,2,4-Trimethylbenzene 2750 20000 23300 103 20000 21900 96 6 70-130/20 108-67-8 1,3,5-Trimethylbenzene 769 J 20000 21400 103 20000 20400 98 5 70-130/20 75-01-4 Vinyl Chloride ND 20000 17700 89 20000 19700 99 11 60-140/20 m,p-Xylene 11300 40000 53900 107 40000 51300 100 5 70-130/20 95-47-6 o-Xylene 5850 20000 27000 106 20000 25300 97 7 70-130/20 1330-20-7 Xylene (total)17100 60000 80900 106 60000 76600 99 5 70-130/20 CAS No.Surrogate Recoveries MS MSD FA82331-5 Limits 1868-53-7 Dibromofluoromethane 100%99%98%70-130% 17060-07-0 1,2-Dichloroethane-D4 99%100%102%70-130% 2037-26-5 Toluene-D8 102%99%103%70-130% 460-00-4 4-Bromofluorobenzene 98%101%99%70-130% * = Outside of Control Limits. 51 of 53 FA8232355.3.2 Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2 Job Number:FA82323 Account:GRINCC GRI (Geological Resources Inc.) Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA82422-1MS E105729.D 5 01/20/21 LR n/a n/a VE2415 FA82422-1MSD E105730.D 5 01/20/21 LR n/a n/a VE2415 FA82422-1 E105725.D 1 01/20/21 LR n/a n/a VE2415 The QC reported here applies to the following samples:Method: SM 6200B FA82323-5 FA82422-1 Spike MS MS Spike MSD MSD Limits CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD 71-43-2 Benzene ND 50 58.4 117 50 58.5 117 0 70-130/20 108-86-1 Bromobenzene ND 50 41.2 82 50 42.2 84 2 70-130/20 74-97-5 Bromochloromethane ND 50 53.0 106 50 52.8 106 0 70-130/20 75-27-4 Bromodichloromethane ND 50 54.5 109 50 54.9 110 1 70-130/20 75-25-2 Bromoform ND 50 36.0 72 50 36.7 73 2 70-130/20 104-51-8 n-Butylbenzene ND 50 42.5 85 50 43.4 87 2 70-130/20 135-98-8 sec-Butylbenzene ND 50 45.3 91 50 46.2 92 2 70-130/20 98-06-6 tert-Butylbenzene ND 50 42.8 86 50 43.7 87 2 70-130/20 56-23-5 Carbon Tetrachloride ND 50 60.4 121 50 60.4 121 0 70-130/20 108-90-7 Chlorobenzene ND 50 43.2 86 50 43.4 87 0 70-130/20 75-00-3 Chloroethane ND 50 62.5 125 50 53.3 107 16 60-140/20 67-66-3 Chloroform ND 50 57.5 115 50 57.2 114 1 70-130/20 95-49-8 o-Chlorotoluene ND 50 42.0 84 50 42.8 86 2 70-130/20 106-43-4 p-Chlorotoluene ND 50 42.2 84 50 43.0 86 2 70-130/20 124-48-1 Dibromochloromethane ND 50 38.8 78 50 39.2 78 1 70-130/20 96-12-8 1,2-Dibromo-3-chloropropane ND 50 38.8 78 50 38.7 77 0 70-130/20 106-93-4 1,2-Dibromoethane ND 50 42.6 85 50 43.1 86 1 70-130/20 75-71-8 Dichlorodifluoromethane ND 50 51.5 103 50 44.4 89 15 60-140/20 95-50-1 1,2-Dichlorobenzene ND 50 40.3 81 50 40.6 81 1 70-130/20 541-73-1 1,3-Dichlorobenzene ND 50 41.6 83 50 42.5 85 2 70-130/20 106-46-7 1,4-Dichlorobenzene ND 50 41.8 84 50 42.9 86 3 70-130/20 75-34-3 1,1-Dichloroethane 0.22 J 50 61.5 123 50 61.5 123 0 70-130/20 107-06-2 1,2-Dichloroethane ND 50 52.5 105 50 52.2 104 1 70-130/20 75-35-4 1,1-Dichloroethylene ND 50 64.1 128 50 63.7 127 1 70-130/20 156-59-2 cis-1,2-Dichloroethylene ND 50 61.1 122 50 61.1 122 0 70-130/20 156-60-5 trans-1,2-Dichloroethylene ND 50 60.8 122 50 59.7 119 2 70-130/20 78-87-5 1,2-Dichloropropane ND 50 54.7 109 50 55.1 110 1 70-130/20 142-28-9 1,3-Dichloropropane ND 50 40.5 81 50 40.3 81 0 70-130/20 594-20-7 2,2-Dichloropropane ND 50 62.6 125 50 61.3 123 2 70-130/20 563-58-6 1,1-Dichloropropene ND 50 57.7 115 50 57.7 115 0 70-130/20 10061-01-5 cis-1,3-Dichloropropene ND 50 52.3 105 50 52.9 106 1 70-130/20 10061-02-6 trans-1,3-Dichloropropene ND 50 43.8 88 50 43.9 88 0 70-130/20 108-20-3 Di-Isopropyl Ether ND 50 53.2 106 50 52.8 106 1 70-130/20 100-41-4 Ethylbenzene ND 50 45.0 90 50 45.3 91 1 70-130/20 87-68-3 Hexachlorobutadiene ND 50 41.5 83 50 41.6 83 0 70-130/20 98-82-8 Isopropylbenzene ND 50 46.6 93 50 46.6 93 0 70-130/20 * = Outside of Control Limits. 52 of 53 FA8232355.3.3 Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2 Job Number:FA82323 Account:GRINCC GRI (Geological Resources Inc.) Project:Everett's Enterprise; 1101 N Catherine Creek Rd, Ahoskie, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA82422-1MS E105729.D 5 01/20/21 LR n/a n/a VE2415 FA82422-1MSD E105730.D 5 01/20/21 LR n/a n/a VE2415 FA82422-1 E105725.D 1 01/20/21 LR n/a n/a VE2415 The QC reported here applies to the following samples:Method: SM 6200B FA82323-5 FA82422-1 Spike MS MS Spike MSD MSD Limits CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD 99-87-6 p-Isopropyltoluene ND 50 45.2 90 50 46.2 92 2 70-130/20 74-83-9 Methyl Bromide ND 50 54.9 110 50 48.2 96 13 60-140/20 74-87-3 Methyl Chloride ND 50 56.8 114 50 49.1 98 15 60-140/20 74-95-3 Methylene Bromide ND 50 55.0 110 50 54.1 108 2 70-130/20 75-09-2 Methylene Chloride ND 50 56.4 113 50 55.9 112 1 70-130/20 1634-04-4 Methyl Tert Butyl Ether ND 50 53.2 106 50 51.4 103 3 70-130/20 91-20-3 Naphthalene ND 50 39.8 80 50 39.3 79 1 70-130/20 103-65-1 n-Propylbenzene ND 50 43.2 86 50 43.9 88 2 70-130/20 100-42-5 Styrene ND 50 45.2 90 50 45.9 92 2 70-130/20 630-20-6 1,1,1,2-Tetrachloroethane ND 50 43.4 87 50 42.7 85 2 70-130/20 79-34-5 1,1,2,2-Tetrachloroethane ND 50 41.2 82 50 41.9 84 2 70-130/20 127-18-4 Tetrachloroethylene ND 50 47.4 95 50 47.4 95 0 70-130/20 108-88-3 Toluene ND 50 44.9 90 50 44.5 89 1 70-130/20 87-61-6 1,2,3-Trichlorobenzene ND 50 37.8 76 50 38.1 76 1 70-130/20 120-82-1 1,2,4-Trichlorobenzene ND 50 39.1 78 50 39.6 79 1 70-130/20 71-55-6 1,1,1-Trichloroethane ND 50 58.9 118 50 59.8 120 2 70-130/20 79-00-5 1,1,2-Trichloroethane ND 50 42.5 85 50 42.9 86 1 70-130/20 79-01-6 Trichloroethylene ND 50 58.1 116 50 58.4 117 1 70-130/20 75-69-4 Trichlorofluoromethane ND 50 60.1 120 50 51.8 104 15 60-140/20 96-18-4 1,2,3-Trichloropropane ND 50 41.3 83 50 41.3 83 0 70-130/20 95-63-6 1,2,4-Trimethylbenzene ND 50 42.1 84 50 42.7 85 1 70-130/20 108-67-8 1,3,5-Trimethylbenzene ND 50 43.6 87 50 44.5 89 2 70-130/20 75-01-4 Vinyl Chloride ND 50 59.2 118 50 51.5 103 14 60-140/20 m,p-Xylene ND 100 91.5 92 100 91.8 92 0 70-130/20 95-47-6 o-Xylene ND 50 45.0 90 50 45.3 91 1 70-130/20 1330-20-7 Xylene (total)ND 150 137 91 150 137 91 0 70-130/20 CAS No.Surrogate Recoveries MS MSD FA82422-1 Limits 1868-53-7 Dibromofluoromethane 107%106%104%70-130% 17060-07-0 1,2-Dichloroethane-D4 103%101%100%70-130% 2037-26-5 Toluene-D8 89%88%88%70-130% 460-00-4 4-Bromofluorobenzene 98%100%102%70-130% * = Outside of Control Limits. 53 of 53 FA8232355.3.3 APPENDIX D Contaminant Mass Calculations Area ID Well ID Area (ft²) Average Well Depth (ft.) Average Depth to Water (ft.) Water Column Height (ft) Volume (ft³) Volume (L) Effective Porosity Effective Volume (L) MW-2 MW-3 Area Date Well Benzene (μ/L) Toluene (μ/L) Ethylbenzene (μ/L) Xylenes (μ/L) MTBE (μ/L) Naphthalene (μ/L) Total (μ/L) DTW (ft.) Average Water Column Height (ft.) Total Average Mass (g)Percent Red.To Date Red. MW-2 3340.00 7650.00 1050.00 4960.00 1580.00 249.00 18829.00 5.26 MW-3 7700.00 26900.00 2970.00 15500.00 3670.00 621.00 57361.00 5.21 Avg.5520.00 17275.00 2010.00 10230.00 2625.00 435.00 38095.00 5.24 MW-2 7470.00 20400.00 2080.00 10920.00 1490.00 840.00 43200.00 4.34 MW-3 13400.00 24900.00 2920.00 15520.00 18100.00 1150.00 75990.00 4.45 Avg.10435.00 22650.00 2500.00 13220.00 9795.00 995.00 59595.00 4.40 MW-2 5760.00 13000.00 1270.00 9820.00 1790.00 472.00 FP 4.78 MW-3 5510.00 14700.00 1900.00 9660.00 2510.00 371.00 34651.00 4.78 Avg.5635.00 13850.00 1585.00 9740.00 2150.00 421.50 34651.00 4.78 MW-2 5060.00 15500.00 2370.00 11700.00 2270.00 626.00 37526.00 5.11 MW-3 3900.00 23600.00 3290.00 15600.00 0.00 611.00 47001.00 4.82 Avg.4480.00 19550.00 2830.00 13650.00 1135.00 618.50 42263.50 4.97 Date Average Water Column Height (ft.) 03/07/11 10.77 09/26/11 11.61 01/06/15 11.22 01/12/21 11.04 Notes: • FP: Free Product • Area of the contaminant plume is calculated from Figure 7 • Height of the water column is calculated by subtracting the average depth to water from the average well depth of the referenced monitoring wells • Volume of the contaminant plume is calculated by multiplying the area of the plume by the average height of the water column during each sampling event • Effective porosity is assumed based on the sub-surface soil profile obtained from well construction records and soil boring logs • Total mass was calculated by multiplying the total contaminant concentrations for the sampling event with effective volume • Contaminant mass cannot be calculated in wells containing FP; therefore, the total contaminant mass is based on the known concentrations in the area for each sampling event. • When areas couldn’t be sampled, the last known concentrations were used in the calculations. 3,504.9 0.201 213,5811,067,90437,71310.765.2416 9,257.37 -20.0%-13.7% 13728 -68.6%-68.6% 7,717 43.8%5.2% Total Contaminant Mass (g) Percent Reduction Compared to Previous Event Percent Reduction To Date 8,140 ------ 43.8%5.2% 01/12/21 11.04 9,257.37 -20.0%-13.7% ------ 09/26/11 11.61 13,727.92 -68.6%-68.6% Area 1 03/02/11 10.77 8,140.14 01/06/15 11.22 7,717.18 APPENDIX D CONTAMINANT MASS CALCULATIONS EVERETTE'S ENTERPRISES (INCIDENT NO. 11174) Baseline Event