WA-769_10679_CA_RPTS_20180314_MRP

EXECUTIVE SUMMARY

The former Sunrise BP site is located at 2005 East Ash Street in Goldsboro, Wayne County, North
Carolina. The adjoining properties are commercial and residential. No potable water supply wells were
identified within a 1,000-foot radius of the site. Municipal water is available to the site and surrounding
properties. The site has a risk classification because free product is present in monitoring wells MW-1
and MW-8A.

In August 2017, the sorbent socks were removed from monitoring wells. On February 6, 2018, four
monitoring wells (MW-1, MW-2A, MW-8A, and MW-9) were gauged, purged and/or sampled.
Concentrations of requested method constituents that exceeded the Maximum Allowable Concentrations
specified in T15A NCAC 2L.0202 were reported in the ground water samples collected from MW-1,
MW-2A, MW-8A, and MW-9. None of the reported contaminant concentrations exceeded the Gross
Contamination Levels. Therefore, no further assessment should be required.

TABLE OF CONTENTS

1.0 SITE HISTORY AND CHARACTERIZATION .................................................................... 1
2.0 CURRENT SITE ASSESSMENT ............................................................................................ 1
3.0 GROUND WATER QUALITY ................................................................................................ 1
4.0 CONCLUSIONS AND RECOMMENDATIONS .................................................................... 2
5.0 LIMITATIONS ......................................................................................................................... 2
FIGURES
Figure 1: Site Location Map
Figure 2: Site Vicinity Map
Figure 3: Site Map
Figure 4: Water Table Surface Map
Figure 5: Ground Water Quality Map

TABLES

Table 1: Well Construction and Gauging Information
Table 2: Summary of Ground Water Sample Analytical Results

APPENDIX
Appendix A: Laboratory Analytical Report – Ground Water Sample

1
1.0 SITE HISTORY AND CHARACTERIZATION
The Former Sunrise BP site is located at 2005 East Ash Street in Goldsboro, Wayne County, North
Carolina (Figures 1 and 2). According to available information, four 3,000-gallon and one 6,000-gallon
gasoline underground storage tanks (USTs) were removed from the site in May 1993. A total of eighteen
Type II monitoring wells (MW-1, MW-2A, MW-3A, MW-4 through MW-7, MW-8A, and MW-9
through MW-18) and two Type III monitoring wells (TW-1 and TW-2) were installed at the site during
past ground water assessment activities. According to the historical information, monitoring wells MW-
6, MW-7, and TW-1 have been destroyed. Previous assessment and remediation activities were
conducted by other consultants. Geological Resources, Inc. (GRI) cannot verify the accuracy of
information obtained from previous reports, but for the purposes of this report, it is assumed to be correct.
Please refer to previous submittals for further historical information regarding the site.

2.0 CURRENT SITE ASSESSMENT
This report presents the results of ground water sampling activities conducted on February 6, 2018 at the
Former Sunrise BP site in Goldsboro, Wayne County, North Carolina (Figures 1 and 2). The activities
were conducted in accordance with GRI Proposal Number 17-627 which was submitted to the North
Carolina Department of Environmental Quality (NCDEQ) on January 11, 2018, and approved as Task
Authorization Number 10679-29 on January 18, 2018. The purpose of the scope of work was to obtain
current ground water quality data for the site since removing sorbent socks in August 2017.

3.0 GROUND WATER QUALITY
Four Type II monitoring wells (MW-1, MW-2A, MW-8A, and MW-9) were gauged on February 6, 2018.
The depths to ground water in the Type II monitoring wells gauged during the February 2018 sampling
event ranged from 6.07 to 6.63 feet below the tops of well casings. Ground water elevations in the Type
II monitoring wells relative to a temporary benchmark with an assumed datum of 100.00 feet ranged from
93.93 to 94.81 feet. A Site Map showing the location of the monitoring wells has been included as
Figure 3. A Water Table Surface Map has been included as Figure 4. A summary of well construction
information and ground water elevation data is presented in Table 1.

Laboratory analyses were performed on the ground water samples for volatile organic compounds using
EPA Method 602. Concentrations of BTEX constituents, MTBE, and/or naphthalene that exceeded the
maximum allowable concentrations (MACs) specified in T15A NCAC 2L.0202 (2L) were reported in the

2
ground water samples collected from MW-1, MW-2A, MW-8A, and MW-9. None of the reported
concentrations exceeded the Gross Contamination Levels (GCLs). A Ground Water Quality Map based
on data from the February 2018 sampling event has been included as Figure 5. A summary of ground
water sample analytical results is presented in Table 2. A copy of the complete laboratory analytical
report has been included as Appendix A.

4.0 CONCLUSIONS AND RECOMMENDATIONS
 In August 2017, sorbent socks were removed from monitoring wells.
 In February 2018, monitoring wells MW-1, MW-2A, MW-8A, and MW-9 were gauged and
sampled. The average depth to ground water in the Type II monitoring wells in February 2018
was 6.25 feet.
 Concentrations of BTEX constituents, MTBE, and/or naphthalene that exceeded the MACs were
reported in the ground water samples collected from MW-1, MW-2A, MW-8A, and MW-9.
 None of the reported concentrations exceeded the GCLs. Therefore, no further assessment should
be required.

5.0 LIMITATIONS
This report has been prepared for the exclusive use of Castleberry’s, Inc. for specific application to the
referenced site in Wayne County, North Carolina. The assessment was conducted based on the scope of
work and level of effort desired by the NCDEQ and with resources adequate only for that scope of work.
Our findings have been developed in accordance with generally accepted standards of environmental
practices in the State of North Carolina, available information, and our professional judgment. No other
warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would be
interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data. Please note that field data collected prior
to the November 2009 receptor survey update, free product evaluation, and ground water sampling events
were not obtained under the supervision of GRI. Although the accuracy of this information cannot be
verified, for the purpose of this report GRI assumes that it is correct.

FIGURES
"J
SITE
ASH ST
BEST STROSE ST
WALNUT ST TAYLOR STCLAIBORNE STPALM ST
RANDOLPH STMULBERRY ST
RIDGEWOOD DRMADISON AVSPENCE AVEVERGREEN AV OVERBROOK RDPEACHTREE ST
PINE ST
HILLDALE LN
HILLCREST DRDURANT STDENTON PLPEACHTREE ST
DURANT STUt Stoney CreekUt
3509834917
35098378763509836709
350983553735098346603509836515WSW-13509835039³
FIGURE 2: SITE VICINITY MAPSUNRISE BP2005 EAST ASH STREETGOLDSBORO, WAYNE COUNTYNORTH CAROLINAINCIDENT NO. 10679
PREPARED BY:GEOLOGICAL RESOURCES, INC.NOVEMBER 24, 2009
0 300150Feet
1 inch equals 300 feet
1,500-FOOT RADIUS 1,000-FOOT RADIUS
250-FOOT RADIUS
Legend
"J Water Supply Well
All_Ditches_Streams_Rivers
Wayne_Centerlines_master
parcels_view
3509836709 PIN Number

TABLES
Date: 02/21/18
11/30/09 6.85 0.02 93.17
06/07/10 7.73 0.17 92.42
11/24/10 7.75 0.06 92.30 Before FP Eval
11/24/10 7.73 0.00 92.27 After FP Eval
07/27/11 9.07 0.06 90.98
02/13/12 7.77 0.00 92.23 Before MMPE
02/17/12 9.21 0.00 90.79 After MMPE
03/20/12 7.23 0.09 92.85
10/26/12 8.72 0.09 91.36
11/21/12 8.74 0.01 91.27
12/12/12 8.51 0.01 91.50
01/22/13 7.60 0.00 92.40
02/25/13 6.72 0.01 93.29
03/25/13 7.09 0.14 93.03
08/06/13 6.60 0.00 93.40
12/04/13 6.72 0.00 93.28
02/07/14 5.95 0.00 94.05
03/17/14 5.77 0.00 94.23
05/28/14 6.58 0.00 93.42 Before AFVR
05/28/14 7.41 0.23 92.79 After AFVR
12/03/14 6.72 0.00 93.28
03/24/15 5.36 0.00 94.64 Before AFVR
03/24/15 5.76 0.00 94.24 After AFVR
04/21/15 4.91 0.00 95.09
08/07/15 8.38 0.25 91.83
01/22/16 5.56 0.02 94.46
05/26/16 6.78 0.00 93.22
11/01/16 6.28 0.00 93.72
07/17/17 7.83 0.12 92.27
02/06/18 6.07 0.00 93.93
11/30/09 6.96 0.00 93.97
11/24/10 7.79 0.00 93.14
07/27/11 9.11 0.00 91.82
02/13/12 7.90 0.00 93.03 Before MMPE
02/17/12 9.96 0.00 90.97 After MMPE
03/20/12 7.30 0.00 93.63
05/28/14 6.23 0.00 94.70 Before AFVR
05/28/14 6.69 0.00 94.24 After AFVR
12/03/14 6.88 0.00 94.05
03/24/15 5.04 0.00 95.89 Before AFVR
03/24/15 5.49 0.00 95.44 After AFVR
08/07/15 8.43 0.02 92.52
01/22/16 5.48 0.00 95.45
05/26/16 6.65 0.00 94.28
11/01/16 6.05 0.00 94.88
07/17/17 7.67 0.00 93.26
02/06/18 6.12 0.00 94.81
11/30/09 6.64 0.00 NM
07/27/11 8.93 0.00 NM
03/20/12 6.96 0.00 NM
11/30/09 6.70 0.00 94.82
07/27/11 8.73 0.00 92.79
03/20/12 7.02 0.00 94.50
MW-5 11/30/09 3 3 - 18 18 99.13 NM NM NM Destroyed
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
SUNRISE BP (INCIDENT NO. 10679)
Facility ID #: 0-006025
Well ID
Date Water
Level
Measured
(mm/dd/yy)
Well Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom of
Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of
Casing
(ft.)
Free
Product
Thickness
(ft.)
Ground
Water
Elevation
(ft.)
Comments
MW-4 3 3 - 18 18 101.52
MW-3A 5 5 - 15 15 NM
100.93155 - 155MW-2A
100.00177 - 177MW-1
Page 1 of 3
Date: 02/21/18
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
SUNRISE BP (INCIDENT NO. 10679)
Facility ID #: 0-006025
Well ID
Date Water
Level
Measured
(mm/dd/yy)
Well Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom of
Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of
Casing
(ft.)
Free
Product
Thickness
(ft.)
Ground
Water
Elevation
(ft.)
Comments
11/30/09 7.08 0.11 93.22
06/07/10 7.69 0.00 92.52
11/24/10 7.80 0.00 92.41
07/27/11 9.13 0.00 91.08
02/13/12 7.89 0.00 92.32 Before MMPE
02/17/12 9.01 0.00 91.20 After MMPE
03/20/12 7.35 0.10 92.95
10/26/12 8.76 0.01 91.46
11/21/12 8.86 0.01 91.36
12/12/12 8.67 0.01 91.55
01/22/13 7.73 0.00 92.48
02/25/13 7.05 0.22 93.35
03/25/13 7.28 0.23 93.13
08/06/13 6.94 0.39 93.60
12/04/13 7.05 0.34 93.45
02/07/14 6.39 0.11 93.91
03/17/14 5.79 0.04 94.45
05/28/14 6.91 0.32 93.57 Before AFVR
05/28/14 8.28 0.00 91.93 After AFVR
06/30/14 7.28 0.00 92.93
12/03/14 6.87 0.04 93.37
03/24/15 5.37 0.00 94.84 Before AFVR
03/24/15 5.89 0.00 94.32 After AFVR
04/21/15 4.99 0.00 95.22
08/07/15 8.26 0.00 91.95
01/22/16 5.60 0.00 94.61
05/26/16 6.83 0.05 93.42
11/01/16 6.26 0.00 93.95
07/17/17 7.81 0.03 92.43
02/06/18 6.19 0.00 94.02
11/30/09 7.34 0.00 93.71
07/27/11 9.43 0.00 91.62
03/20/12 7.62 0.00 93.43
05/28/14 6.72 0.00 94.33 Before AFVR
05/28/14 7.00 0.00 94.05 After AFVR
04/21/15 5.27 0.00 95.78
05/26/16 6.73 0.00 94.32
07/17/17 7.95 0.00 93.10
02/06/18 6.63 0.00 94.42
11/30/09 5.00 0.00 92.63
07/27/11 7.20 0.00 90.43
03/20/12 5.23 0.00 92.40 abandoned
11/30/09 7.03 0.00 93.19
07/27/11 9.27 0.00 90.95
03/20/12 7.20 0.00 93.02
11/01/16 6.11 0.00 94.11
11/30/09 5.68 0.00 92.39
07/27/11 8.00 0.00 90.07
03/20/12 6.02 0.00 92.05
11/30/09 4.60 0.00 91.96
07/27/11 6.80 0.00 89.76
03/20/12 4.87 0.00 91.69
11/30/09 3.06 0.00 91.94
07/27/11 5.40 0.00 89.60
03/20/12 3.33 0.00 91.67
11/30/09 4.40 0.00 91.67
07/27/11 6.51 0.00 89.56
03/20/12 4.63 0.00 91.44
11/30/09 5.60 0.00 92.78
07/27/11 7.70 0.00 90.68
03/20/12 5.87 0.00 92.51
11/30/09 3.50 0.00 92.82
07/27/11 5.95 0.00 90.37
03/20/12 3.73 0.00 92.59
11/01/16 3.01 0.00 93.31
11/30/09 5.30 0.00 93.29
07/27/11 7.55 0.00 91.04
03/20/12 5.63 0.00 92.96 abandoned
MW-18 2 2 - 14 14 98.59
MW-16 2 2 - 14 14 98.38
96.3262 - 62MW-17
MW-15 2 2 - 8 8 96.07
MW-14 2 2 - 6.5 6.5 95.00
MW-13 1.5 1.5 - 9 9 96.56
MW-12 1.5 1.5 - 9.5 9.5 98.07
100.22101 - 101MW-11
MW-10 3 3 - 18 18 97.63
101.05183 - 183MW-9
100.21183 - 183MW-8A
Page 2 of 3
Date: 02/21/18
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
SUNRISE BP (INCIDENT NO. 10679)
Facility ID #: 0-006025
Well ID
Date Water
Level
Measured
(mm/dd/yy)
Well Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom of
Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of
Casing
(ft.)
Free
Product
Thickness
(ft.)
Ground
Water
Elevation
(ft.)
Comments
11/30/09 7.93 0.00 92.56
07/27/11 10.15 0.00 90.34
03/20/12 8.18 0.00 92.31
Notes:
• **: If free product is present in a well, ground water elevation should be calculated by: (Top of Casing Elevation - Depth to Water) +
(Free Product Thickness x 0.8581)
• ft BGS : feet below ground surface
• NM: Not measured.
TW-2 29 29 - 34 34 100.49
Page 3 of 3
Date: 02/28/18
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6
5,000 260,000 84,500 85,500 20,000 6,000
12/01/09 FP FP FP FP FP FP
06/07/10 FP FP FP FP FP FP
07/27/11 FP FP FP FP FP FP
03/20/12 FP FP FP FP FP FP
08/06/13 1,450 3,960 1,970 9,320 111 645
03/17/14 1,200 2,830 1,830 9,560 105 674
12/03/14 1,100 2,070 2,060 10,900 85.2 897
04/21/15 686 1,380 1,490 5,880 54.8 531
08/07/15 FP FP FP FP FP FP
05/26/16 1,410 1,690 4,440 20,100 70.8 J 2,050
07/17/17 FP FP FP FP FP FP
02/06/18 679 482 1,390 4,870 46.3 765
07/27/11 750 918 189 1,508 14.2 97.1
03/20/12 147 539 327 1,780 <2.6 149
12/03/14 1,960 10,400 3,130 13,800 37.5 J 1,420
08/07/15 FP FP FP FP FP FP
05/26/16 914 5,370 2,080 11,900 <25 1,230
07/17/17 1,220 5,230 1,060 5,700 15.1 J 467
02/06/18 108 142 68.6 945 <2.5 219
07/27/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10
03/20/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10
07/27/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10
03/20/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10
12/01/09 FP FP FP FP FP FP
07/27/11 2,550 7,970 2,100 8,730 141 830
03/20/12 FP FP FP FP FP FP
08/06/13 FP FP FP FP FP FP
03/17/14 FP FP FP FP FP FP
06/30/14 1,260 5,880 2,340 11,800 32.0 J 1,050
12/03/14 FP FP FP FP FP FP
04/21/15 1,360 7,840 2,630 15,000 39.0 J 1,060
08/07/15 665 2,770 1,860 7,840 15.7 J 932
05/26/16 FP FP FP FP FP FP
07/17/17 FP FP FP FP FP FP
02/06/18 1,200 3,720 2,140 9,670 <13 1,020
07/27/11 161 317 94.0 1,050 1.7 J 45.4
03/20/12 61.3 107 119 506 <1.3 57.5
04/21/15 13.5 10.0 110 203 <0.82 94.3
05/26/16 851 1,090 1,990 9,800 <13 2,230
07/17/17 58.7 56.7 158 714 <1.3 203
02/06/18 27.8 91.3 57.9 297 <0.31 65.2
07/27/11 <0.13 0.24 J 0.83 0.72 J 5.8 7.9
03/20/12 0.65 1.4 10.2 3.8 6.1 7.7
07/27/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10
03/20/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10
07/27/11 <0.13 <0.13 <0.15 <0.30 1.3 <0.10
03/20/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10
07/27/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10
03/20/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10
07/27/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10
03/20/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10
07/27/11 <0.13 <0.13 <0.15 <0.30 3.8 <0.10
03/20/12 <0.13 <0.13 <0.15 <0.30 0.38 J <0.10
07/27/11 0.23 J 0.44 J <0.15 <0.30 0.75 <0.10
03/20/12 <0.13 <0.13 <0.15 <0.30 2.2 <0.10
TABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
SUNRISE BP (INCIDENT NO. 10769)
Analytical Method SM 6200B/602
Facility ID No. 0-006025
Contaminant of Concern
BenzeneTolueneEthylbenzeneTotal XylenesMethyl-tert-butyl ether(MTBE)NaphthaleneMW-15
MW-16
MW-2A
MW-3A
MW-4
MW-11
MW-12
MW-13
MW-9
MW-8A
MW-14
2L Standard (µg/l)
GCL (µg/l)
MW-1
MW-10
Page 1 of 2
Date: 02/28/18
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6
5,000 260,000 84,500 85,500 20,000 6,000
TABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
SUNRISE BP (INCIDENT NO. 10769)
Analytical Method SM 6200B/602
Facility ID No. 0-006025
Contaminant of Concern
BenzeneTolueneEthylbenzeneTotal XylenesMethyl-tert-butyl ether(MTBE)Naphthalene2L Standard (µg/l)
GCL (µg/l)
07/27/11 89.1 0.49 J 21.8 25.0 25.0 2.6
03/20/12 <0.13 <0.13 <0.15 <0.13 <0.13 <0.10
07/27/11 61.1 4.1 53.8 28.3 28.3 112
03/20/12 15.3 2.6 5.6 14.3 14.3 40.2
07/27/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10
03/20/12 <0.13 <0.13 <0.15 0.41 J <0.13 0.31 J
Notes:
• Results reported in micrograms per liter (µg/l).
• < : Less than the method detection limit specified in the laboratory report.
• 2L Standard specified in T15A NCAC 2L.0202.
• GCL: Gross contamination level.
• FP: Free Product
• Concentrations in bold face type exceeded the 2L standards.
• Refer to laboratory report for detected constituents that did not exceed the MACs, or for which no
standard has been established.
MW-17
MW-18
TW-2
Page 2 of 2

APPENDIX

APPENDIX A
Laboratory Analytical Report – Ground Water Sample
02/16/18
Technical Report for
GRI (Geological Resources Inc.)
Sunrise BP; 2005 E Ash St, Goldsboro, NC
10679/2907
SGS Job Number: FA51609
Sampling Date: 02/06/18
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
[e-mail]; [e-mail];
[e-mail]; [e-mail]
ATTN: Rae Brown
Total number of pages in report:
Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AK, AR, IA, KY, MA, MS, ND, NH, NV, OK, OR, UT, WA, WV
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone]
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Caitlin Brice, M.S.
General Manager
Orlando, FL 02/16/18
e-Hardcopy 2.0
Automated Report
19
SGS is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
Review standard terms at: http://www.sgs.com/en/terms-and-conditions
The results set forth herein are provided by SGS North America Inc.
1 of 19
FA51609
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................5
3.1: FA51609-1: MW-1 ........................................................................................................6
3.2: FA51609-2: MW-2A .....................................................................................................7
3.3: FA51609-3: MW-8A .....................................................................................................8
3.4: FA51609-4: MW-9 ........................................................................................................9
Section 4: Misc. Forms ............................................................................................................10
4.1: Chain of Custody ...........................................................................................................11
Section 5: MS Volatiles - QC Data Summaries .....................................................................13
5.1: Method Blank Summary ................................................................................................14
5.2: Blank Spike Summary ...................................................................................................16
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................18 123452 of 19
FA51609
SGS North America Inc.
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA51609
Sunrise BP; 2005 E Ash St, Goldsboro, NC
Project No: 10679/2907
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA51609-1 02/06/18 13:45 WR 02/07/18 AQ Ground Water MW-1
FA51609-2 02/06/18 13:19 WR 02/07/18 AQ Ground Water MW-2A
FA51609-3 02/06/18 13:36 WR 02/07/18 AQ Ground Water MW-8A
FA51609-4 02/06/18 13:05 WR 02/07/18 AQ Ground Water MW-9
3 of 19
FA516091
Summary of Hits Page 1 of 1
Job Number:FA51609
Account:GRI (Geological Resources Inc.)
Project:Sunrise BP; 2005 E Ash St, Goldsboro, NC
Collected:02/06/18
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA51609-1 MW-1
Benzene 679 25 6.3 ug/l SM 6200B
Ethylbenzene 1390 25 6.3 ug/l SM 6200B
Methyl Tert Butyl Ether 46.3 25 6.3 ug/l SM 6200B
Naphthalene 765 25 6.3 ug/l SM 6200B
Toluene 482 25 6.3 ug/l SM 6200B
Xylene (total)4870 75 13 ug/l SM 6200B
FA51609-2 MW-2A
Benzene 108 10 2.5 ug/l SM 6200B
Ethylbenzene 68.6 10 2.5 ug/l SM 6200B
Naphthalene 219 10 2.5 ug/l SM 6200B
Toluene 142 10 2.5 ug/l SM 6200B
Xylene (total)945 30 5.0 ug/l SM 6200B
FA51609-3 MW-8A
Benzene 1200 50 13 ug/l SM 6200B
Ethylbenzene 2140 50 13 ug/l SM 6200B
Naphthalene 1020 50 13 ug/l SM 6200B
Toluene 3720 50 13 ug/l SM 6200B
Xylene (total)9670 150 25 ug/l SM 6200B
FA51609-4 MW-9
Benzene 27.8 1.3 0.31 ug/l SM 6200B
Ethylbenzene 57.9 1.3 0.31 ug/l SM 6200B
Naphthalene 65.2 1.3 0.31 ug/l SM 6200B
Toluene 91.3 1.3 0.31 ug/l SM 6200B
Xylene (total)297 3.8 0.63 ug/l SM 6200B
4 of 19
FA516092
SGS North America Inc.
Sample Results
Report of Analysis
Orlando, FL
Section 3
5 of 19
FA516093
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:MW-1
Lab Sample ID:FA51609-1 Date Sampled:02/06/18
Matrix:AQ - Ground Water Date Received:02/07/18
Method:SM 6200B Percent Solids:n/a
Project:Sunrise BP; 2005 E Ash St, Goldsboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0211624.D 50 02/12/18 23:34 TD n/a n/a VA2317
Run #2 E056964.D 200 02/09/18 19:47 TD n/a n/a VE1915
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
Purgeable Aromatics, Full List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 679 25 6.3 ug/l
108-90-7 Chlorobenzene ND 25 6.3 ug/l
95-50-1 1,2-Dichlorobenzene ND 25 6.3 ug/l
541-73-1 1,3-Dichlorobenzene ND 25 6.3 ug/l
106-46-7 1,4-Dichlorobenzene ND 25 6.3 ug/l
108-20-3 Di-Isopropyl Ether ND 25 6.3 ug/l
100-41-4 Ethylbenzene 1390 25 6.3 ug/l
1634-04-4 Methyl Tert Butyl Ether 46.3 25 6.3 ug/l
91-20-3 Naphthalene 765 25 6.3 ug/l
108-88-3 Toluene 482 25 6.3 ug/l
1330-20-7 Xylene (total)4870 75 13 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 90%97%70-130%
17060-07-0 1,2-Dichloroethane-D4 85%101%70-130%
2037-26-5 Toluene-D8 100%106%70-130%
460-00-4 4-Bromofluorobenzene 100%100%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
6 of 19
FA5160933.1
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:MW-2A
Lab Sample ID:FA51609-2 Date Sampled:02/06/18
Matrix:AQ - Ground Water Date Received:02/07/18
Method:SM 6200B Percent Solids:n/a
Project:Sunrise BP; 2005 E Ash St, Goldsboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0211625.D 20 02/12/18 23:56 TD n/a n/a VA2317
Run #2 a E056965.D 250 02/09/18 20:11 TD n/a n/a VE1915
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
Purgeable Aromatics, Full List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 108 10 2.5 ug/l
108-90-7 Chlorobenzene ND 10 2.5 ug/l
95-50-1 1,2-Dichlorobenzene ND 10 2.5 ug/l
541-73-1 1,3-Dichlorobenzene ND 10 2.5 ug/l
106-46-7 1,4-Dichlorobenzene ND 10 2.5 ug/l
108-20-3 Di-Isopropyl Ether ND 10 2.5 ug/l
100-41-4 Ethylbenzene 68.6 10 2.5 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 10 2.5 ug/l
91-20-3 Naphthalene 219 10 2.5 ug/l
108-88-3 Toluene 142 10 2.5 ug/l
1330-20-7 Xylene (total)945 30 5.0 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 91%97%70-130%
17060-07-0 1,2-Dichloroethane-D4 83%101%70-130%
2037-26-5 Toluene-D8 100%106%70-130%
460-00-4 4-Bromofluorobenzene 100%103%70-130%
(a) Confirmation run.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
7 of 19
FA5160933.2
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:MW-8A
Lab Sample ID:FA51609-3 Date Sampled:02/06/18
Matrix:AQ - Ground Water Date Received:02/07/18
Method:SM 6200B Percent Solids:n/a
Project:Sunrise BP; 2005 E Ash St, Goldsboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0211626.D 100 02/13/18 00:19 TD n/a n/a VA2317
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
Purgeable Aromatics, Full List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 1200 50 13 ug/l
108-90-7 Chlorobenzene ND 50 13 ug/l
95-50-1 1,2-Dichlorobenzene ND 50 13 ug/l
541-73-1 1,3-Dichlorobenzene ND 50 13 ug/l
106-46-7 1,4-Dichlorobenzene ND 50 13 ug/l
108-20-3 Di-Isopropyl Ether ND 50 13 ug/l
100-41-4 Ethylbenzene 2140 50 13 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 50 13 ug/l
91-20-3 Naphthalene 1020 50 13 ug/l
108-88-3 Toluene 3720 50 13 ug/l
1330-20-7 Xylene (total)9670 150 25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 88%70-130%
17060-07-0 1,2-Dichloroethane-D4 81%70-130%
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
8 of 19
FA5160933.3
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:MW-9
Lab Sample ID:FA51609-4 Date Sampled:02/06/18
Matrix:AQ - Ground Water Date Received:02/07/18
Method:SM 6200B Percent Solids:n/a
Project:Sunrise BP; 2005 E Ash St, Goldsboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0211627.D 2.5 02/13/18 00:43 TD n/a n/a VA2317
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
Purgeable Aromatics, Full List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 27.8 1.3 0.31 ug/l
108-90-7 Chlorobenzene ND 1.3 0.31 ug/l
95-50-1 1,2-Dichlorobenzene ND 1.3 0.31 ug/l
541-73-1 1,3-Dichlorobenzene ND 1.3 0.31 ug/l
106-46-7 1,4-Dichlorobenzene ND 1.3 0.31 ug/l
108-20-3 Di-Isopropyl Ether ND 1.3 0.31 ug/l
100-41-4 Ethylbenzene 57.9 1.3 0.31 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 1.3 0.31 ug/l
91-20-3 Naphthalene 65.2 1.3 0.31 ug/l
108-88-3 Toluene 91.3 1.3 0.31 ug/l
1330-20-7 Xylene (total)297 3.8 0.63 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 91%70-130%
17060-07-0 1,2-Dichloroethane-D4 81%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
9 of 19
FA5160933.4
SGS North America Inc.
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Orlando, FL
Section 4
10 of 19
FA516094
FA51609: Chain of Custody
Page 1 of 2
11 of 19
FA5160944.1
Job Number:FA51609 Client:GRI
Date / Time Received:2/7/2018 10:15:00 AM Delivery Method:FED EX
Project:2907
Airbill #'s:1015899950910003281100811062251986
Cooler Information
1. Custody Seals Present
2. Custody Seals Intact
4. Cooler temp verification
3. Temp criteria achieved
5. Cooler media
IR Gun
Ice (Bag)
Trip Blank Information
1. Trip Blank present / cooler
2. Trip Blank listed on COC
2. Samples preserved properly
Sample Information
1. Sample labels present on bottles
5. Sample recvd within HT
4. Condition of sample
3. Sufficient volume/containers recvd for analysis:
Intact
Comments
SM001Rev. Date 05/24/17
SGS Sample Receipt Summary
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
Cooler 1: (3.8);
Cooler 1: (4.2);
3. Type Of TB Received
W or S N/A
6. Dates/Times/IDs on COC match Sample Label
7. VOCs have headspace
8. Bottles received for unspecified tests
9. Compositing instructions clear
10. Voa Soil Kits/Jars received past 48hrs?
11. % Solids Jar received?
Misc. Information
25-Gram 5-GramNumber of Encores:Number of 5035 Field Kits:Number of Lab Filtered Metals:
Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify)
Y or N N/A
Y or N
Therm ID:IR 1; Therm CF:0.4; # of Coolers:1
Y or N N/A
12. Residual Chlorine Present?
Residual Chlorine Test Strip Lot #:
Technician:Reviewer:SHAYLAP P.H Date:2/7/2018Date:2/7/2018 10:15:00 AM
FA51609: Chain of Custody
Page 2 of 2
12 of 19
FA5160944.1
SGS North America Inc.
MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 5
13 of 19
FA516095
Method Blank Summary Page 1 of 1
Job Number:FA51609
Account:GRINCC GRI (Geological Resources Inc.)
Project:Sunrise BP; 2005 E Ash St, Goldsboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1915-MB E056953.D 1 02/09/18 TD n/a n/a VE1915
The QC reported here applies to the following samples:Method: SM 6200B
FA51609-1
CAS No.Compound Result RL MDL Units Q
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 96%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
2037-26-5 Toluene-D8 105%70-130%
460-00-4 4-Bromofluorobenzene 103%70-130%
14 of 19
FA5160955.1.1
Method Blank Summary Page 1 of 1
Job Number:FA51609
Account:GRINCC GRI (Geological Resources Inc.)
Project:Sunrise BP; 2005 E Ash St, Goldsboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2317-MB A0211610.D 1 02/12/18 TD n/a n/a VA2317
The QC reported here applies to the following samples:Method: SM 6200B
FA51609-1, FA51609-2, FA51609-3, FA51609-4
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
15 of 19
FA5160955.1.2
Blank Spike Summary Page 1 of 1
Job Number:FA51609
Account:GRINCC GRI (Geological Resources Inc.)
Project:Sunrise BP; 2005 E Ash St, Goldsboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1915-BS E056951.D 1 02/09/18 TD n/a n/a VE1915
The QC reported here applies to the following samples:Method: SM 6200B
FA51609-1
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
2037-26-5 Toluene-D8 104%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
* = Outside of Control Limits.
16 of 19
FA5160955.2.1
Blank Spike Summary Page 1 of 1
Job Number:FA51609
Account:GRINCC GRI (Geological Resources Inc.)
Project:Sunrise BP; 2005 E Ash St, Goldsboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2317-BS A0211611.D 1 02/12/18 TD n/a n/a VA2317
The QC reported here applies to the following samples:Method: SM 6200B
FA51609-1, FA51609-2, FA51609-3, FA51609-4
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 10.9 109 70-130
108-90-7 Chlorobenzene 10 10.8 108 70-130
95-50-1 1,2-Dichlorobenzene 10 11.0 110 70-130
541-73-1 1,3-Dichlorobenzene 10 11.0 110 70-130
106-46-7 1,4-Dichlorobenzene 10 10.7 107 70-130
108-20-3 Di-Isopropyl Ether 10 11.0 110 70-130
100-41-4 Ethylbenzene 10 10.8 108 70-130
1634-04-4 Methyl Tert Butyl Ether 10 11.0 110 70-130
91-20-3 Naphthalene 10 9.5 95 70-130
108-88-3 Toluene 10 10.6 106 70-130
1330-20-7 Xylene (total)30 32.5 108 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
* = Outside of Control Limits.
17 of 19
FA5160955.2.2
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1
Job Number:FA51609
Account:GRINCC GRI (Geological Resources Inc.)
Project:Sunrise BP; 2005 E Ash St, Goldsboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA51609-2MS E056968.D 250 02/09/18 TD n/a n/a VE1915
FA51609-2MSD E056969.D 250 02/09/18 TD n/a n/a VE1915
FA51609-2 a E056965.D 250 02/09/18 TD n/a n/a VE1915
The QC reported here applies to the following samples:Method: SM 6200B
FA51609-1
FA51609-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
CAS No.Surrogate Recoveries MS MSD FA51609-2 Limits
1868-53-7 Dibromofluoromethane 96%96%97%70-130%
17060-07-0 1,2-Dichloroethane-D4 101%100%101%70-130%
2037-26-5 Toluene-D8 103%105%106%70-130%
460-00-4 4-Bromofluorobenzene 101%102%103%70-130%
(a) Confirmation run.
* = Outside of Control Limits.
18 of 19
FA5160955.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1
Job Number:FA51609
Account:GRINCC GRI (Geological Resources Inc.)
Project:Sunrise BP; 2005 E Ash St, Goldsboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA51641-5MS A0211630.D 25 02/13/18 TD n/a n/a VA2317
FA51641-5MSD A0211631.D 25 02/13/18 TD n/a n/a VA2317
FA51641-5 A0211612.D 25 02/12/18 TD n/a n/a VA2317
The QC reported here applies to the following samples:Method: SM 6200B
FA51609-1, FA51609-2, FA51609-3, FA51609-4
FA51641-5 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 13 U 250 274 110 250 270 108 1 70-130/20
108-90-7 Chlorobenzene 13 U 250 266 106 250 260 104 2 70-130/20
95-50-1 1,2-Dichlorobenzene 13 U 250 262 105 250 261 104 0 70-130/20
541-73-1 1,3-Dichlorobenzene 13 U 250 272 109 250 266 106 2 70-130/20
106-46-7 1,4-Dichlorobenzene 13 U 250 255 102 250 251 100 2 70-130/20
108-20-3 Di-Isopropyl Ether 13 U 250 230 92 250 230 92 0 70-130/20
100-41-4 Ethylbenzene 14.9 250 278 105 250 273 103 2 70-130/20
1634-04-4 Methyl Tert Butyl Ether 13 U 250 232 93 250 231 92 0 70-130/20
91-20-3 Naphthalene 83.9 250 305 88 250 326 97 7 70-130/20
108-88-3 Toluene 19.3 250 291 109 250 286 107 2 70-130/20
1330-20-7 Xylene (total)76.6 750 867 105 750 852 103 2 70-130/20
CAS No.Surrogate Recoveries MS MSD FA51641-5 Limits
1868-53-7 Dibromofluoromethane 91%91%103%70-130%
17060-07-0 1,2-Dichloroethane-D4 82%82%102%70-130%
2037-26-5 Toluene-D8 101%101%97%70-130%
460-00-4 4-Bromofluorobenzene 101%100%99%70-130%
* = Outside of Control Limits.
19 of 19
FA5160955.3.2