WA-765_10673_CA_RPTS_20190416_AFVR

EXECUTIVE SUMMARY

The former Red Apple Market # 3 site is located at 1332 East Memorial Drive in Ahoskie, Hertford
County, North Carolina. According to available information, two 12,000-gallon gasoline, one 8,000-
gallon gasoline and one 550-gallon kerosene underground storage tanks were removed from the site on
June 3, 1993. Forty monitoring wells have been installed at the site and adjacent properties during past
ground water assessment and corrective action activities. Free product had been previously measured in
monitoring wells MW-7, MW-8 and MW-15.

An Aggressive Fluid-Vapor Recovery (AFVR) event was conducted on MW-7 on February 20, 2019. A
ground water sample was collected from MW-7 prior to the start of the AFVR event. Concentrations of
requested method constituents that exceeded the applicable ground water quality standards were reported
in the ground water sample collected from MW-7.

The results of the AFVR event indicate that 2,533 gallons of petroleum impacted ground water were
removed during the event. No measurable liquid product was observed in the storage tanker at the
conclusion of the event. Approximately 1.92 gallons of vapor-phase free product were removed during
the AFVR event.

On March 27, 2019, three monitoring wells were gauged, purged and sampled. No free product was
observed in any of the wells in March 2019. Concentrations of requested method constituents that
exceeded the Maximum Allowable Concentrations specified in T15A NCAC 2L.0202 were reported in
the ground water samples collected from MW-2, MW-7 and MW-8. The concentration of benzene
reported in the ground water sample collected from MW-7 exceeded the Gross Contamination Level
(GCL).

Based on this information, it appears that the AFVR event was successful in removing vapor phase free
product from the site. GRI recommends that semi-annual ground water sampling events should continue
at the site until contaminant concentrations do not exceed the GCLs. The next ground water sampling
event is tentatively scheduled for September 2019.

TABLE OF CONTENTS

1.0 SITE HISTORY AND CHARACTERIZATION ....................................................................... 1
2.0 CURRENT SITE ASSESSMENT ................................................................................................ 1
3.0 AFVR EVENT ................................................................................................................................ 1
4.0 GROUND WATER QUALITY .................................................................................................... 2
5.0 CONCLUSIONS AND RECOMMENDATIONS ....................................................................... 3
6.0 LIMITATIONS .............................................................................................................................. 4

FIGURES
Figure 1: Site Location Map
Figure 2: Site Map
Figure 3: Ground Water Flow Map
Figure 4: Ground Water Quality Map

TABLES

Table 1: Well Construction and Gauging Information
Table 2: Free Product Recovery Results
Table 3: Free Product Recovery Event Information
Table 4: Free Product Recovery Cost Summary
Table 5: Summary of Ground Water Sample Analytical Results
APPENDICES
Appendix A: AFVR Data and Calculations
Appendix B: Disposal Manifest
Appendix C: Laboratory Reports – Ground Water Samples

1
1.0 SITE HISTORY AND CHARACTERIZATION
According to available information, two 12,000-gallon gasoline, one 8,000-gallon gasoline and one 550-
gallon kerosene underground storage tanks (USTs) were removed from the site on June 3, 1993. Forty
monitoring wells have been installed at the site and adjacent properties during past ground water
assessment and corrective action activities. The site is currently ranked as Intermediate risk due to the
historical presence of free product and/or contaminant concentrations that exceeded the Gross
Contamination Levels (GCLs) that were observed in MW-7, MW-8 and/or MW-15. The site is located
within the designated wellhead protection area for the Town of Ahoskie.

Site activities performed prior to May 2008 were conducted by previous consultants. Although
Geological Resources, Inc. (GRI) cannot verify the accuracy of information obtained from previous
reports, for the purposes of this report, it is assumed to be correct. Please refer to previous submittals for
further historical information regarding the site.

2.0 CURRENT SITE ASSESSMENT
This report presents the results of Aggressive Fluid-Vapor Recovery (AFVR) and ground water
assessment activities conducted between February 20 and March 27, 2019 at the former Red Apple
Market # 3 site located at 1332 East Memorial Drive in Ahoskie, Hertford County, North Carolina
(Figure 1). The activities were conducted in accordance with GRI proposal number 18-534, which was
submitted to NCDEQ on January 29, 2019, and approved as Task Authorization No. 10673-18 on January
29, 2019. The purpose of the activities was to reduce contaminant concentrations for the site.

3.0 AFVR EVENT
On February 20, 2019, an AFVR event was conducted by Greenwood Applied Services, LLC (GAS),
under the supervision of GRI personnel. The AFVR equipment included a vacuum truck, flexible
vacuum hoses, 1-inch diameter PVC stinger pipes and associated couplings and pipe fittings needed to
connect to MW-7. The vacuum truck had a storage capacity of 3,500 gallons and was rated at 680 CFM
at 18 in /Hg.

Prior to the event, MW-7 was gauged, purged and sampled. The collected ground water sample was
submitted for laboratory analyses of volatile organic compounds (VOCs) using EPA Method 602.
Concentrations of requested method constituents that exceeded the applicable ground water quality

2
standards were reported in the ground water sample collected from MW-7. Monitoring wells MW-2,
MW-8 and MW-17 were used as observation wells.

During the event, which was conducted for approximately 8 hours, measurements of vacuum, relative
humidity, temperature, exhaust air velocity and off-gas concentrations were recorded at 15-minute
intervals for the first two hours and every 30 minutes thereafter. No measurable free product was
reported at the conclusion of the event. A summary of well construction information and ground water
gauging data is presented in Table 1. Copies of the AFVR data and calculations have been included as
Appendix A.

The results of the AFVR event indicate that a total of 2,533 gallons of liquid were removed during the 8-
hour event. During the AFVR’s 8 hours of operation, the average fluid recovery rate was 294.38 gallons
per hour. Based on mass-removal calculations, 12.02 pounds or 1.92 gallons of vapor phase
hydrocarbons were removed. Based on 8 hours of operation, an average of 0.24 gallons of vapor phase
free product was removed per hour by the AFVR event. Based on the February 2019 AFVR event, the
cost per gallon of fluids recovered was $1.23. A Site Map showing the locations of the monitoring wells
and the structures on-site and on surrounding properties has been included as Figure 2. A summary of
the free product recovery results is presented in Table 2. A summary of information collected during the
AFVR event as well as a breakdown of fluids removed is included in Table 3. A summary of costs
associated with free product and total fluids recover is included in Table 4. A summary of the ground
water sample results obtained prior to the start of the AFVR event is included as Table 5. At the
conclusion of the AFVR event, all wastewater and product were transported to a permitted facility for
disposal. A copy of the disposal manifest has been included as Appendix B. A copy of the laboratory
report for the ground water sample collected prior to the start of the AFVR event is included as Appendix
C.

4.0 GROUNDWATER QUALITY
Three Type II monitoring wells (MW-2, MW-7 and MW-8) were gauged, purged and sampled on March
27, 2019. The depths to ground water in the Type II monitoring wells during the March 2019 sampling
event ranged from 7.46 to 7.94 feet below the tops of well casings. Ground water elevations in the Type
II monitoring wells relative to a benchmark of 100.00 feet ranged from 91.97 to 92.95 feet. Based on this
information, ground water flow in the vicinity of the source area was generally toward the north with an
average horizontal hydraulic gradient of approximately 0.01 feet per foot. A Ground Water Flow Map

3
based on the March 27, 2019, gauging event has been included as Figure 3. A summary of well
construction and gauging information is presented in Table 1.

Laboratory analyses were performed on the ground water samples collected from the monitoring wells for
VOCs using EPA Method 6200B.

Concentrations of individual BTEX constituents, MTBE, naphthalene, n-butylbenzene, 1,2-
dichloroethane, isopropylbenzene, IPE, n-propylbenzene, 1,2,4-trimethylbenzene and/or 1,3,5-
trimethylbenzene that exceeded the Maximum Allowable Concentrations (MACs) specified in T15A
NCAC 2L.0202 were reported in the ground water samples collected from MW-2, MW-7 and MW-8.
The concentration of benzene reported in the ground water sample collected from MW-7 exceeded the
GCL. A Ground Water Quality Map based on data from the March 2019 sampling event has been
included as Figure 4. A summary of ground water sample analytical results is presented in Table 5. A
complete copy of the laboratory report has been included in Appendix C.

5.0 CONCLUSIONS AND RECOMMENDATIONS
 Concentrations of requested method constituents that exceeded the applicable ground water
quality standards were reported in the ground water sample collected from MW-7 prior to the
start of the AFVR event.
 A total of 2,533 gallons of petroleum impacted ground water was removed during the February
2019 AFVR event. No measurable free product was observed in MW-7 during the event.
Approximately 1.92 gallons of vapor-phase free product were removed during the AFVR event.
No liquid free product was observed in the storage tanker at the conclusion of the event.
 Concentrations of individual BTEX constituents, MTBE, naphthalene, n-butylbenzene, 1,2-
dichloroethane, isopropylbenzene, IPE, n-propylbenzene, 1,2,4-trimethylbenzene and/or 1,3,5-
trimethylbenzene that exceeded the MACs were reported in the ground water samples collected
from MW-2, MW-7 and MW-8. The concentration of benzene reported in the ground water
sample collected from MW-7 exceeded the GCL.
 Based on this information, it appears that the AFVR event was successful in removing vapor
phase free product from the site. GRI recommends that semi-annual ground water sampling
events should continue at the site until contaminant concentrations do not exceed the GCLs. The
next semi-annual ground water sampling event is tentatively scheduled for September 2019.

4
6.0 LIMITATIONS
This report has been prepared for the exclusive use of North East Oil Company, Inc. for specific
application to the referenced site in Hertford County, North Carolina. The assessment was conducted
based on the scope of work and level of effort desired by NCDEQ and with resources adequate only for
that scope of work. Our findings have been developed in accordance with generally accepted standards of
environmental practices in the State of North Carolina, available information, and our professional
judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would be
interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data. Please note that field data collected prior
to the May 2008 sampling and updated receptor survey event were not obtained under the supervision of
GRI. Although the accuracy of these data cannot be verified, for the purpose of this report GRI assumes
that they are correct.

FIGURES

TABLES
MW-1 Unknown 04/23/08 NA NA NA 99.29 9.43 0.00 89.86      
01/07/09 9.94 0.00 89.35
05/11/10 8.89 0.00 90.40
05/02/11 8.90 0.00 91.10
07/23/12 9.39 0.00 89.90 Before MMPE
07/27/12 9.49 0.00 89.80 After MMPE
08/28/12 9.10 0.00 90.90
08/19/13 9.42 0.00 90.58
07/08/14 9.13 0.00 90.87
03/24/15 8.02 0.00 91.98
01/11/16 8.25 0.00 91.75
04/23/08 9.85 0.00 90.25
10.28 0.00 89.82 Before AFVR
10.35 0.01 89.76 After AFVR
01/07/09 10.40 0.00 89.70
05/11/10 9.45 0.00 90.65
03/28/11 9.53 0.00 90.57 Before MMPE
04/01/11 9.50 0.00 90.60 After MMPE
05/02/11 9.38 0.00 91.03
07/23/12 9.89 0.00 90.52 Before MMPE
07/27/12 10.12 0.00 90.29 After MMPE
08/28/12 9.52 0.00 90.89
07/15/13 9.30 0.00 91.11 Before MMPE
07/19/13 9.90 0.00 90.51 After MMPE
08/19/13 NM NM NM
9.21 0.00 91.20 Before AFVR
9.73 0.00 90.68 After AFVR
07/08/14 9.69 0.00 90.72
03/24/15 8.01 0.00 92.40
12/07/15 9.30 0.00 91.11 Before MMPE
12/11/15 9.55 0.00 90.86 After MMPE
01/11/16 8.79 0.00 91.62
06/11/18 9.00 0.00 91.41
03/27/19 7.46 0.00 92.95
MW-3 Unknown 04/23/08 NA NA NA 99.93 10.03 0.00 89.90
01/07/09 10.55 0.00 89.38
05/11/10 9.59 0.00 90.34
05/02/11 9.52 0.00 91.03
07/23/12 10.24 0.00 90.31 Before MMPE
07/27/12 10.24 0.00 90.31 After MMPE
08/28/12 9.65 0.00 90.90
08/19/13 10.01 0.00 90.54
07/08/14 9.80 0.00 90.75
03/24/15 8.56 0.00 91.99
01/11/16 8.83 0.00 91.72
04/23/08 9.39 0.00 90.30
01/07/09 9.93 0.00 89.76
05/11/10 9.75 0.00 89.94
05/02/11 9.53 0.00 90.57
08/28/12 9.62 0.00 90.48
08/19/13 NM NM NM
04/23/08 NM NM NM Not Located
01/07/09 NM NM NM Not Located
05/02/11 NM NM NM Covered
08/28/12 NM NM NM Covered
08/19/13 NM NM NM No Access
07/08/14 NM NM NM Not Located
04/23/08 NM NM NM Not Located
01/07/09 9.52 0.00 89.59
05/11/10 8.68 0.00 90.43
05/02/11 8.61 0.00 90.77
08/28/12 8.64 0.00 90.74
08/19/13 9.26 0.00 90.12
07/08/14 8.92 0.00 90.46
03/24/15 7.64 0.00 91.74
01/11/16 7.80 0.00 91.58
100.41
188-18809/15/93MW-2
6
25
16
MW-3A
08/13/08
100.10
6-16
100.10
99.93
99.69
100.55
20NANAUnknown
166-166
NM
18.4NANAUnknownMW-1A
MWD-4
06/05/14
Date
Installed
(mm/dd/yy)
Top of Casing
Elevation*
(ft.)
Depth to
Water from
Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
99.42
99.29
100.00
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET #3 (INCIDENT NO. 10673)
Facility ID # : 0-017539
Groundwater
Elevation*
(ft.)
CommentsWell ID
Screened
Interval
(x to y ft. 
BGS)
Bottom of
Well
(ft. BGS)
MW-5 01/07/94
01/07/94MW-6
99.38
Date: 04/05/19
20 20-25
99.11
Date Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
01/07/94
Page 1 of 5
Date
Installed
(mm/dd/yy)
Top of Casing
Elevation*
(ft.)
Depth to
Water from
Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET #3 (INCIDENT NO. 10673)
Facility ID # : 0-017539
Groundwater
Elevation*
(ft.)
CommentsWell ID
Screened
Interval
(x to y ft. 
BGS)
Bottom of
Well
(ft. BGS)
Date: 04/05/19
Date Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
04/23/08 NM NM NM Not Located
10.30 0.00 89.17 Before AFVR
10.27 0.71 89.81 After AFVR
10.80 1.11 89.62 Before AFVR
10.53 0.01 88.95 After AFVR
01/07/09 10.25 0.45 89.61
04/05/10 8.10 0.31 91.64 Before MMPE
04/09/10 8.80 0.00 90.67 After MMPE
05/11/10 8.90 0.00 90.57
03/28/11 9.02 0.02 90.47 Before MMPE
04/01/11 9.09 0.00 90.38 After MMPE
05/02/11 8.85 0.00 91.12
07/23/12 9.34 0.00 90.63 Before MMPE
07/27/12 9.57 0.00 90.40 After MMPE
08/28/12 8.97 0.00 91.00
07/15/13 8.77 0.00 91.20 Before MMPE
07/19/13 9.17 0.00 90.80 After MMPE
08/19/13 9.43 0.00 90.54
8.73 0.07 91.30 Before AFVR
9.12 0.00 90.85 After AFVR
07/08/14 9.11 0.00 90.86
03/24/15 6.88 0.00 93.09
12/07/15 8.79 0.00 91.18 Before MMPE
12/11/15 9.12 0.00 90.85 After MMPE
01/11/16 8.13 0.00 91.84
05/02/18 8.45 0.00 91.52 Before AFVR
05/02/18 9.11 0.00 90.86 After AFVR
06/11/18 8.48 0.00 91.49
7.86 0.00 92.11 Before AFVR
7.86 0.00 92.11 After AFVR
03/27/19 7.83 0.00 92.14
04/23/08 10.64 1.71 89.97
11.10 1.80 89.58 Before AFVR
9.71 0.30 89.69 After AFVR
11.40 1.82 89.30 Before AFVR
9.99 0.00 89.15 After AFVR
01/07/09 10.50 0.90 89.41
04/05/10 7.71 0.00 91.43 Before MMPE
04/09/10 8.60 0.00 90.54 After MMPE
05/11/10 8.80 0.00 90.34
03/28/11 9.05 0.21 90.27 Before MMPE
04/01/11 9.92 0.00 89.22 After MMPE
05/02/11 8.78 0.03 91.05
07/23/12 9.29 0.06 90.56 Before MMPE
07/27/12 9.43 0.00 90.37 After MMPE
08/28/12 8.80 0.00 91.00
08/19/13 9.33 0.00 90.47
07/08/14 9.05 0.00 90.75
03/24/15 7.79 0.00 92.01
06/11/18 8.35 0.00 91.45
03/27/19 7.83 0.00 91.97
04/23/08 NM NM NM Not Located
01/07/09 NM NM NM Not Located
05/11/10 NM NM NM Under Junk Cars
05/02/11 NM NM NM Under Junk Cars
07/23/12 9.29 0.00 90.78 Before MMPE
07/27/12 9.39 0.00 90.68 After MMPE
08/28/12 8.77 0.00 91.30
08/19/13 9.41 0.00 90.66
07/08/14 9.09 0.00 90.98
03/24/15 7.76 0.00 92.31
01/11/16 8.00 0.00 92.07
04/23/08 7.04 0.00 90.58
01/07/09 7.70 0.00 89.92
05/11/10 7.18 0.00 90.44
05/02/11 7.04 0.00 90.43
08/28/12 6.95 0.00 90.52
08/19/13 7.71 0.00 89.76
07/08/14 7.43 0.00 90.04
03/24/15 6.08 0.00 91.39
04/23/08 8.69 0.00 90.26
01/07/09 9.42 0.00 89.53
05/11/10 8.71 0.00 90.24
05/02/11 8.57 0.00 90.73
08/28/12 8.46 0.00 90.84
08/19/13 9.23 0.00 90.07
07/08/14 8.96 0.00 90.34
03/24/15 7.57 0.00 91.73
99.80
166-16601/10/94MW-8
99.97
MW-7
02/20/19
01/10/94 6 6-16 16
08/13/08
12/29/08
06/05/14
12/29/08
08/13/08
NA
97.47
98.95
99.15
6
99.14
16MW-11 11/25/94
NA NA
6
99.30
97.62
100.07
166-16
99.47
MW-9 01/10/94
MW-10 Unknown
6-16
Page 2 of 5
Date
Installed
(mm/dd/yy)
Top of Casing
Elevation*
(ft.)
Depth to
Water from
Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET #3 (INCIDENT NO. 10673)
Facility ID # : 0-017539
Groundwater
Elevation*
(ft.)
CommentsWell ID
Screened
Interval
(x to y ft. 
BGS)
Bottom of
Well
(ft. BGS)
Date: 04/05/19
Date Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
04/23/08 8.25 0.00 90.39      
01/07/09 8.95 0.00 89.69
05/11/10 8.12 0.00 90.52
05/02/11 8.05 0.00 90.47
08/28/12 8.05 0.00 90.47
08/19/13 8.64 0.00 89.88
07/08/14 8.40 0.00 90.12
03/24/15 7.13 0.00 91.39
04/23/08 NM NM NM Not Located
01/07/09 9.45 0.00 89.37
05/11/10 8.27 0.00 90.55
05/02/11 8.50 0.00 90.99
03/28/11 8.61 0.00 90.88 Before MMPE
04/01/11 8.72 0.00 90.77 After MMPE
08/28/12 8.51 0.00 90.98
08/19/13 9.12 0.00 90.37
07/08/14 8.81 0.00 90.68
03/24/15 NM NM NM Not Located
04/23/08 9.11 0.00 90.07      
01/07/09 9.73 0.00 89.45
05/11/10 8.69 0.00 90.49
05/02/11 8.66 0.00 91.19
08/28/12 8.77 0.00 91.08
08/19/13 9.29 0.00 90.56
07/08/14 8.96 0.00 90.89
03/24/15 7.67 0.00 92.18
01/11/16 7.94 0.00 91.91
04/23/08 9.06 0.00 89.98      
01/07/09 9.76 0.03 89.31
05/11/10 9.07 0.00 89.97
05/02/11 8.94 0.00 90.82
08/28/12 8.80 0.00 90.96
08/19/13 9.67 0.00 90.09
07/08/14 NM NM NM Behind Locked Fence
03/24/15 NM NM NM Behind Locked Fence
MW-16 Unknown 04/23/08 NA NA NA 97.03 6.26 0.00 90.77      
01/07/09 6.78 0.00 90.25
05/12/10 6.91 0.00 90.12
05/02/11 6.68 0.00 90.26
08/28/12 6.25 0.00 90.69
08/19/13 7.42 0.00 89.52
07/08/14 NM NM NM Not Located
03/24/15 NM NM NM Not Located
04/23/08 9.18 0.00 90.05      
01/07/09 9.79 0.00 89.44
05/11/10 8.54 0.00 90.69
05/02/11 8.59 0.00 91.39
08/28/12 8.76 0.00 91.22
08/19/13 9.16 0.00 90.82
07/08/14 8.68 0.00 91.30
03/24/15 7.59 0.00 92.39
01/11/16 7.89 0.00 92.09
04/23/08 7.25 0.00 89.47      
01/07/09 7.80 0.00 88.92
05/02/11 6.79 0.00 90.66
08/28/12 7.00 0.00 90.45
08/19/13 7.23 0.00 90.22
07/08/14 7.00 0.00 90.45
03/24/15 6.09 0.00 91.36
04/23/08 7.76 0.00 89.29
01/07/09 8.38 0.00 88.67
05/12/10 7.56 0.00 89.49
05/02/11 7.49 0.00 90.31
08/28/12 7.66 0.00 90.14
08/19/13 8.02 0.00 89.78
07/08/14 7.77 0.00 90.03
03/24/15 6.91 0.00 90.89
04/23/08 9.29 0.00 90.13
01/07/09 9.92 0.00 89.50
05/11/10 8.65 0.00 90.77
05/02/11 8.74 0.00 91.38
08/28/12 8.95 0.00 91.17
08/19/13 9.29 0.00 90.83
07/08/14 8.96 0.00 91.16
03/24/15 7.79 0.00 92.33
04/23/08 9.29 0.00 90.12
01/07/09 9.98 0.00 89.43
05/02/11 8.77 0.00 91.34
08/28/12 8.93 0.00 91.18
08/19/13 9.34 0.00 90.77
07/08/14 8.88 0.00 91.23
03/24/15 7.74 0.00 92.37
16
99.98
6 16
11/25/94 6
96.72
100.11
16
99.41
99.42
6 6-16 16
100.12
6-16
05/17/96 6-16 16
16
16
6
6 6-16MW-18 05/17/96
11/25/94
MW-16A
6-16
97.05
99.85
16
99.49
6
6
6-16
16
6-16
6-16
98.52
98.64
97.45
97.80
99.76
96.94
20
99.04
98.82
99.18
97.03
99.23
MW-19
MW-20 05/18/96 6
MW-21 05/18/96
NANAUnknown
MW-17 05/17/96 6 6-16
05/15/96
MW-14
11/25/94MW-13
MW-15
MW-12
Page 3 of 5
Date
Installed
(mm/dd/yy)
Top of Casing
Elevation*
(ft.)
Depth to
Water from
Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET #3 (INCIDENT NO. 10673)
Facility ID # : 0-017539
Groundwater
Elevation*
(ft.)
CommentsWell ID
Screened
Interval
(x to y ft. 
BGS)
Bottom of
Well
(ft. BGS)
Date: 04/05/19
Date Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
04/23/08 8.39 0.00 89.85
01/07/09 8.94 0.00 89.30
05/12/10 8.24 0.00 90.00
05/02/11 8.15 0.00 89.97
08/28/12 8.25 0.00 89.87
08/19/13 8.65 0.00 89.47
07/08/14 8.41 0.00 89.71
03/24/15 7.53 0.00 90.59
04/23/08 7.11 0.00 89.87
01/07/09 7.62 0.00 89.36
05/12/10 6.85 0.00 90.13
05/02/11 6.79 0.00 90.09
08/28/12 6.94 0.00 89.94
08/19/13 NM NM NM
04/23/08 NM NM NM Not Located
01/07/09 4.72 0.00 90.78
05/12/10 NM NM NM Not Located
05/02/11 5.12 0.00 90.25
08/28/12 4.32 0.00 91.05
08/19/13 5.83 0.00 89.54
07/08/14 5.64 0.00 89.73
03/24/15 NM NM NM Not Located
04/23/08 1.70 0.00 93.66
01/07/09 2.39 0.00 92.97
05/02/11 4.32 0.00 90.89
08/28/12 NM NM NM Not Located
08/19/13 6.14 0.00 89.07
07/08/14 4.89 0.00 90.32
03/24/15 2.30 0.00 92.91
04/23/08 8.71 0.00 90.81
01/07/09 9.50 0.00 90.02
05/02/11 8.92 0.00 90.47
08/28/12 8.53 0.00 90.86
08/19/13 9.64 0.00 89.75
07/08/14 9.39 0.00 90.00
03/24/15 NM NM NM Not Located
04/23/08 NM NM NM Not Located
01/07/09 7.55 0.00 90.21
05/02/11 7.40 0.00 90.23
08/28/12 6.74 0.00 90.89
08/19/13 NM NM NM
04/23/08 9.53 0.00 89.48
01/07/09 10.00 0.00 89.01
05/02/11 9.30 0.00 89.60
08/28/12 9.42 0.00 89.48
08/19/13 NM NM NM
03/24/15 8.88 0.00 90.02
04/23/08 NM NM NM Not Located
01/07/09 11.58 0.00 88.43
05/12/10 12.01 0.00 88.00
05/02/11 11.53 0.00 88.40
08/28/12 10.97 0.00 88.96
08/19/13 12.49 0.00 87.44
07/08/14 12.14 0.00 87.79
03/24/15 10.56 0.00 89.37
04/23/08 NM NM NM Not Located
01/07/09 NM NM NM Not Located
05/12/10 NM NM NM Not Located
05/02/11 NM NM NM Destroyed
08/28/12 NM NM NM Destroyed
04/23/08 NM NM NM Not Located
01/07/09 6.63 0.00 90.14
05/12/10 6.47 0.00 90.30
05/02/11 6.35 0.00 90.27
08/28/12 NM NM NM Not Located
08/19/13 NM NM NM
03/24/15 5.24 0.00 91.38
04/23/08 10.15 0.00 90.15
01/07/09 10.72 0.00 89.58
05/12/10 9.37 0.00 90.93
05/02/11 9.49 0.00 91.55
08/28/12 9.70 0.00 91.34
08/19/13 NM NM NM
03/24/15 NM NM NM Not Located
04/23/08 NM NM NM Not Located
01/07/09 4.42 0.00 NA
05/12/10 5.66 0.00 NA
05/02/11 4.90 0.00 87.52
08/28/12 3.38 0.00 89.04
08/19/13 5.85 0.00 86.57
07/08/14 5.70 0.00 86.72
03/24/15 3.60 0.00 88.82
5 5-15
Unknown
MW-30
MW-33
96.77
100.01
MW-29
NA NA
25
15
96.62
5 5-15
NM
Unknown NA NA NA
92.42
93.19
98.24
15
97.63
95.36
97.76
5-15
05/01/01
20.00
15
15
5
96.98
99.01
99.93
MW-27 05/02/01
NA
MW-31
15-25
MW-28 05/01/01 10 10-20.5
05/01/01
05/02/01
15
95.21
98.12
17
15
95.37
MW-26 08/08/00 5 15
99.39
99.52
5-15
MW-25 08/07/00 5 5-15
08/07/00 7 7-17
MW-24 08/07/00
MW-22 08/07/00 7
5-155
7-17
MW-23
96.88
95.50
17
101.04
18
98.90
100.30
MW-32
Page 4 of 5
Date
Installed
(mm/dd/yy)
Top of Casing
Elevation*
(ft.)
Depth to
Water from
Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET #3 (INCIDENT NO. 10673)
Facility ID # : 0-017539
Groundwater
Elevation*
(ft.)
CommentsWell ID
Screened
Interval
(x to y ft. 
BGS)
Bottom of
Well
(ft. BGS)
Date: 04/05/19
Date Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
05/12/10 96.60 9.29 0.00 87.31
05/02/11 8.70 0.00 87.76
08/28/12 7.90 0.00 88.56
08/19/13 9.68 0.00 86.78
07/08/14 9.38 0.00 87.08
03/24/15 7.66 0.00 88.80
05/12/10 99.13 8.73 0.00 90.40
05/02/11 8.60 0.00 90.48
08/28/12 8.27 0.00 90.81
08/19/13 NM NM NM
05/12/10 100.56 9.33 0.00 91.23
05/02/11 9.35 0.00 91.04
08/28/12 9.54 0.00 90.85
08/19/13 NM NM NM
05/02/11 7.96 0.00 86.01
08/28/12 6.07 0.00 87.90
08/19/13 NM NM NM
03/24/15 5.80 0.00 88.17
05/02/11 6.31 0.00 87.00
08/28/12 5.34 0.00 87.97
08/19/13 NM NM NM
03/24/15 5.22 0.00 88.09
05/02/11 8.18 0.00 89.09
08/28/12 6.90 0.00 90.37
08/19/13 NM NM NM
03/24/15 7.40 0.00 89.87
05/02/11 8.69 0.00 91.21
08/28/12 8.78 0.00 91.12
08/19/13 9.27 0.00 90.63
07/08/14 8.88 0.00 91.02
03/24/15 7.63 0.00 92.27
Notes:
•  * : Reference point for elevation measurements, Assumed elevation 100.00 ft.
•  ** : If free product is present in a well, groundwater elevation should be calculated by: [Top of Casing Elevation - Depth to Water] + [free product thickness 
   x 0.8581].
•  ft BGS : feet below ground surface.
•  NA: Not available.
•  NM: Not measured; well could not be located or was inaccessible.
MW-39 05/02/11 5-15
6-16 16
MW-35
05/02/11 5MW-37 5-15
MW-36
20
6 6-16
03/11/10 96.46
03/11/10 6
03/11/10 16
5 5-20
•  Top of casing elevations were surveyed by Coastal Engineering & Surveying, Inc. in May 2011.
MW-40 05/02/11 5
MW-34
5
05/02/11MW-38
99.08
5
5-15 15 99.90
100.39
15 93.97
97.2715
5-15 93.3115
Page 5 of 5
Date: 04/05/19
Method of Measurement:
Well ID Product Type
(gas, diesel, etc.)
Date of
Recovery
(mm/dd/yy)
Free Product
Recovery
Method*
Casing
Diameter
(inches)
Product
Thickness Before
Recovery
(feet)
Product
Thickness After
Recovery
(feet)
Amount of Liquid
Recovered
(gallons)
Amount of
Product
Recovered
(gallons)
MW-8 08/13/08 AFVR 2 1.80 0.30 350 6.60
MW-7 2 1.11 0.01
MW-8 2 1.82 0.01
MW-7 2 0.31 -
MW-8 2 --
MW-2 2 --
MW-7 2 0.02 -
MW-8 2 0.21 -
MW-2 2 --
MW-7 2 --
MW-8 2 0.06 -
MW-2 2 --
MW-7 2 --
MW-2 2 --
MW-7 2 0.07 -
MW-2 2 --
MW-7 2 --
MW-7 05/02/18 AFVR 2 --2,735 0.00
MW-7 02/20/19 AFVR 2 --2,533 0.00
Notes :
• *: Bailing, Skimming, Aggressive Fluid Vapor Recovery (AFVR), Mobile Multiphase Extraction (MMPE)
• Amount of Liquid Recovered (gallons) includes Total liquids (Water and Free Product) as indicated on Disposal Manifest.
• Amount of Product Recovered (in gallons) includes only the volume of free product in the tanker at the end of the event (based on Disposal
Manifest and/or Field Notes).
06/05/14 AFVR 2,964 0.00
12/07/15 to
12/11/15 MMPE 18,657 0.00
14,774 0.00
07/15/13 to
07/19/13 MMPE 14,135 0.00
07/23/12 to
07/27/12 MMPE
TABLE 2
FREE PRODUCT RECOVERY RESULTS
RED APPLE MARKET #3 (INCIDENT NO. 10673)
Interface probe at top-of-casing
03/28/11 to
04/01/11 MMPE 14,454 0.00
Facility ID#: 0-017539
Gasoline and
Kerosene
12/29/08 AFVR 3,078 2.80
04/05/10 to
04/09/10 0.0014,915MMPE
Date: 04/05/19
MW-8 08/13/08 AFVR 7,805.81 227.76 67.18 2.30 350 6.60 8.90
MW-7
MW-8
MW-7
MW-8
MW-2
MW-7
MW-8
MW-2
MW-7
MW-8
MW-2
MW-7
MW-2
MW-7
MW-2
MW-7
MW-7 05/02/18 AFVR 999.00 78.31 121.38 1.26 2,735 0.00 1.26
MW-7 02/20/19 AFVR 1,428.00 66.63 65.68 1.92 2,533 0.00 1.92
72.67 88,595 9.40 82.07
Notes:
• *: Bailing, Skimming, Aggressive Fluid Vapor Recovery (AFVR), Mobile Multiphase Extraction (MMPE)
• Amount of Vaporized Product (in gallons) is based on Vapor Emissions Summary Sheet, = lbs emitted/6.25
• Amount of Liquid Recovered includes Total liquids (Water and Free Product) as indicated on Disposal Manifest.
• Amount of Product Recovered as Liquid includes only the volume of free product in the tanker at the end of the event (based on Disposal
Manifest and/or Field Notes).
• Total Amount of Product Recovered = Amount of Vaporized Product + Amount of Product Recovered as Liquid
• Total Fluids Removed = Amount of Vaporized Product + Amount of Liquid Recovered
• Information regarding historical free product recovery activities is not available.
224.93 48.76 18,657
Current Event 2,534.92 1.92
MMPE 2,260.75 59.23 0.00
Total To Date 88,667.668 82.07
0.72
Totals
SUMMARY OF FLUID REMOVAL
Summary Total Fluids Removed (in gallons)Total Product Removed (in gallons)
12/07/15 to
12/11/15
3.16
06/05/14 AFVR 3,933.00 224.52 60.38 0.72 2,964 0.00
0.00 6.12
07/15/13 to
07/19/13 MMPE 3,949.00 151.34 326.61 3.16 14,135 0.00
14,454 0.00 2.33
07/23/12 to
07/27/12 MMPE 4,218.27 147.48 301.57 6.12 14,774
Amount of
Vaporized
Product
(gallons)
Amount of
Liquid
Recovered
(gallons)
Amount of
Product
Recovered as
Liquid
(gallons)
Total Amount of
Product
Recovered
(gallons)
03/28/11 to
04/01/11 MMPE 927.60 104.2 431.5 2.33
48.76
TABLE 3
FREE PRODUCT RECOVERY EVENT INFORMATION
RED APPLE MARKET #3 (INCIDENT NO. 10673)
Well ID Date
(mm/dd/yy)
Product
Recovery
Method*
Average
Effluent
Velocity
(ft/min)
Average
Effluent
Temperature
(°F)
Average
Effluent
Concentration
(ppm)
Facility ID #: 0-017539
3.17
5.72
0.00
2.80
14,915
3,078
3.17
2.92
196.93
385.75
139.93
189.78
6,787.80
6,674.00
MMPE
AFVR
04/05/10 to
04/09/10
12/29/08
Date: 04/05/19
Wells Included in
Event
Product
Recovery
Method*
Date of Event
(mm/dd/yy)
Total Fluids
Recovered (gallons)
Cost of Free
Product Recovery
Event
Cost Per
Gallon
MW-7, MW-8 MMPE 04/05/10 to
04/09/10 14,918.17 $10,182.65 $0.68
MW-2, MW-7,
MW-8 MMPE 03/28/11 to
04/01/11 14,460.99 $11,351.50 $0.78
MW-2, MW-7,
MW-8 MMPE 07/23/12 to
07/27/12 14,780.12 $11,598.50 $0.78
MW-2 and MW-7 MMPE 07/15/13 to
07/19/13 14,138.16 $11,355.65 $0.80
MW-2 and MW-7 AFVR 06/05/14 2,964.72 $3,093.45 $1.04
MW-2 and MW-7 MMPE 12/07/15 to
12/11/15 18,705.76 $11,773.50 $0.63
MW-7 AFVR 05/02/18 2,735.31 $3,488.25 $1.28
MW-7 AFVR 02/20/19 2,534.92 $3,117.55 $1.23
85,238.15 $65,961.05 $0.77
Notes:
• *: Bailing, Skimming, Aggressive Fluid Vapor Recovery (AFVR), Mobile Multiphase Extraction (MMPE)
• Total Amount of Free Product Recovered = Amount of Vaporized Product + Amount of Product Recovered as Liquid
• Cost of Free Product Recovery Event includes supervision, travel, mileage, per diem, subcontractor costs, report preparation and project management.
TABLE 4
FREE PRODUCT RECOVERY COST SUMMARY
RED APPLE MARKET #3 (INCIDENT NO. 10673)
Comments
Facility ID #: 0-017539
TOTAL (to date)
EPA
Method
6010B
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.6 70 70 0.4 70 70 70 0.7 400 400 15 400 700 700 10,000 200 200
5,000 260,000 84,500 85,500 20,000 6,000 NE 6,900 8,500 400 25,000 70,000 30,000 700 28,500 25,000 15,000 NE NE NE NE NE NE
MW-1 04/23/08 <0.31 0.620 I 1.14 4.63 <0.12 17.3 <0.14 1.16 0.900 I <0.12 0.380 I <0.15 1.02 <0.33 10.2 2.23 33.5 <100 <100 3,020 1,110 194 2,760
01/09/09 0.65 J <0.70 0.60 J 1.9 J 1.7 J 2.3 JB <0.90 12 B <0.70 <1.1 <0.55 <1.0 <0.75 <0.80 1.1 J <0.50 27.5 <100 <100 <105 <105 <100 <105
05/12/10 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 39.9 <100 <100 <97.1 <97.1 <100 <97.1
05/02/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 30.0 <35 <35 <110 <110 <35 <160
07/09/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 58.3 <35 <35 <100 <100 <35 <150
03/24/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.15 <0.14 <0.14 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NR
01/11/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
04/23/08 1,100 446 203 599 427 186 <1.4 <3.9 <4.7 7.90 I 18.6 15.4 I 27.9 <3.3 248 70.4 16.3 4,120 <100 133 <75 1,680 170
01/09/09 410 28 31 80 110 95 B <1.8 <1.7 2.5 J 3.2 J 9.8 J 14 J 6.6 J <1.6 21 6.4 J 14.8 1,820 241 <100 <100 247 124
05/12/10 4,030 2,610 1,040 2,820 785 478 <0.500 34.2 8.27 <0.500 59.3 59.6 121 <0.500 753 304 15.6 17,300 2,550 <100 <100 2,680 230
05/02/11 6,070 9,230 1,370 4,839 1,260 256 <29 <25 <26 47.6 J 34.6 J 55.5 J 118 J <34 848 256 NR NR NR NR NR NR NR
08/28/12 6,630 9,660 1,450 5,110 1,320 400 <23 <20 <20 <33 41.4 J 62.1 J 128 <27 932 275 NR NR NR NR NR NR NR
08/19/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/09/14 3,030 2,060 1,160 2,500 759 372 <10 <10 <10 <10 44.5 J 39.7 J 138 <10 685 232 <5.0 6,620 <350 1,550 <400 2,630 <600
03/24/15 1,730 1,260 155 791 734 131 <1.5 2.1 J <1.4 4.0 J 11.6 33.5 24.9 <1.5 194 67.2 NR NR NR NR NR NR NR
01/11/16 2,480 2,220 261 1,530 887 117 <13 <13 <13 16.4 J 13.9 J 39.9 J 32.9 J <13 288 86.7 NR NR NR NR NR NR NR
06/11/18 2,270 1,170 367 953 444 128 <13 <13 <13 <13 <13 40.3 J 23.7 J <13 115 40.4 J NR NR NR NR NR NR NR
03/27/19 4,440 3,760 573 1,960 809 239 <13 <13 <13 <13 25.1 J 42.3 J 49.3 J <13 305 105 NR NR NR NR NR NR NR
MW-3 04/23/08 <0.31 <0.28 <0.31 1.39 I 5.30 <0.41 1.13 <0.39 <0.47 <0.12 <0.24 1.45 I <0.30 <0.33 0.860 I 0.290 I 48.0 <100 <100 <75 <75 <100 77.0
01/09/09 2.2 J <0.70 <0.50 <1.0 1.8 J 3.8 JB <0.90 <0.85 <0.70 <1.1 <0.55 2.7 J <0.75 <0.80 <0.70 <0.50 21.1 <100 <100 <105 <105 <100 <105
05/12/10 1.66 <0.500 <0.500 <1.00 4.10 <5.00 <0.500 <0.500 <0.500 0.910 <0.500 5.11 <0.500 <0.500 <0.500 <0.500 34.9 <100 <100 <99.0 <99.0 <100 <99.0
05/02/11 3.6 <0.13 <0.15 <0.30 3.4 0.17 J <0.12 <0.10 0.19 J 1.4 <0.10 7.3 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 11.5 0.28 J <0.15 1.2 J 1.8 0.37 J <0.12 <0.10 0.44 J 0.87 0.50 3.6 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 60.0 2.3 6.0 2.9 5.8 3.0 <0.10 0.27 J 1.6 1.4 3.8 8.3 1.9 <0.10 0.19 J 0.21 J 7.8 220 148 128 J <100 149 <160
07/09/14 0.85 <0.10 <0.10 <0.20 3.3 0.17 J <0.10 <0.10 0.38 J 0.63 0.13 J 3.5 <0.10 <0.10 <0.10 <0.10 10.8 60.8 J <35 <100 <100 <35 213
03/24/15 2.6 <0.17 <0.15 <0.43 0.41 J 0.15 J 0.81 <0.14 <0.14 <0.16 <0.12 0.34 J <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NR
01/11/16 4.1 <0.13 <0.13 <0.31 1.4 0.18 J 1.3 <0.13 <0.13 0.29 J <0.13 0.87 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
MW-3A
MW-1A
2L Standard (mg/l)
GCL (mg/l)
MW-2 BenzeneIsopropylbenzenen-ButylbenzeneBromodichloromethanesec-Butylbenzene1,2-Dichloroethanen-PropylbenzeneMTBETABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
RED APPLE MARKET #3 (INCIDENT NO. 10673)
Analytical Method

Date: 04/05/19 Facility ID #: 0-017539
EPA Method 6200B MADEP Methods VPH and EPH
C9-C12 Aliphatics1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneC5-C8 AliphaticsC11-C22 AromaticsC19-C36 AliphaticsContaminant of
Concern C9-C10 AromaticsLeadNaphthaleneIPETolueneEthylbenzeneXylenesTetrachloroetheneC9-C18 AliphaticsPage 1 of 10
EPA
Method
6010B
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.6 70 70 0.4 70 70 70 0.7 400 400 15 400 700 700 10,000 200 200
5,000 260,000 84,500 85,500 20,000 6,000 NE 6,900 8,500 400 25,000 70,000 30,000 700 28,500 25,000 15,000 NE NE NE NE NE NE
2L Standard (mg/l)
GCL (mg/l)BenzeneIsopropylbenzenen-ButylbenzeneBromodichloromethanesec-Butylbenzene1,2-Dichloroethanen-PropylbenzeneMTBETABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
RED APPLE MARKET #3 (INCIDENT NO. 10673)
Analytical Method

Date: 04/05/19 Facility ID #: 0-017539
EPA Method 6200B MADEP Methods VPH and EPH
C9-C12 Aliphatics1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneC5-C8 AliphaticsC11-C22 AromaticsC19-C36 AliphaticsContaminant of
Concern C9-C10 AromaticsLeadNaphthaleneIPETolueneEthylbenzeneXylenesTetrachloroetheneC9-C18 Aliphatics04/23/08 <0.31 <0.28 <0.31 <1.2 0.650 I <0.41 0.810 <0.39 <0.47 <0.12 <0.24 <0.15 <0.30 <0.33 <0.26 <0.27 6.06 <100 <100 <75 76.6 <100 77.3
01/09/09 <0.60 <0.70 <0.50 <1.0 <0.50 1.1 JB 0.93 J 12 B <0.70 <1.1 <0.55 <1.0 <0.75 <0.80 <0.70 <0.50 <1.5 <100 <100 <100 <100 <100 <100
05/12/10 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 10.8 <100 <100 <99.0 <99.0 <100 <99.0
05/02/11 <0.13 <0.13 <0.15 <0.30 0.39 J <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 <0.13 <0.13 <0.15 <0.30 0.51 <0.10 3.7 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
MW-5 04/23/08 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
04/23/08 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/09/09 480 76 8.0 J 160 1,200 36 B <1.8 <1.7 <1.4 13 3.2 J 28 J <1.5 <1.6 43 6.3 J 13.9 <500 223 <105 <105 160 <105
05/12/10 3.41 0.770 <0.500 <1.00 37.8 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 1.23 <0.500 <0.500 <0.500 <0.500 45.9 <100 <100 <99.0 <99.0 <100 <99.0
05/02/11 0.26 J <0.13 <0.15 <0.30 11.3 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 724 80 37.9 418 1,040 42.5 <2.3 <2.0 <2.0 11.3 4.2 J 30.6 3.6 J <2.7 82.9 13.6 NR NR NR NR NR NR NR
08/19/13 0.19 J <0.10 <0.10 <0.22 21.6 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 0.45 J <0.10 <0.10 <0.10 <0.10 39.1 <35 <35 <110 <110 <35 <160
07/09/14 2.2 0.92 0.64 0.83 J 28.8 0.56 <0.10 <0.10 <0.10 <0.10 0.14 J 0.83 <0.10 <0.10 0.32 J <0.10 76.9 <35 <35 <100 <100 <35 <150
03/24/15 <0.17 <0.17 <0.15 <0.43 0.33 J <0.12 <0.15 <0.14 <0.14 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NR
01/11/16 0.59 <0.13 <0.13 <0.31 90.1 0.14 J <0.13 <0.13 <0.13 2.3 <0.13 4.2 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
04/28/08 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/07/09 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
05/12/10 13,100 31,400 5,480 25,000 5,960 1,850 <0.500 196 37.4 <0.500 144 194 1,770 <0.500 4,850 3,160 142 83,800 24,000 16,500 226 20,000 7,390
05/02/11 12,000 47,400 3,490 17,980 5,860 819 <29 126 J 48.4 J 258 172 177 631 <34 4,970 1,280 NR NR NR NR NR NR NR
08/28/12 10,800 25,600 2,980 14,500 4,470 638 <120 <100 <100 276 J <100 137 J 335 J <140 2,410 607 NR NR NR NR NR NR NR
08/19/13 7,140 17,600 1,920 11,600 2,540 384 <10 19.0 J 11.7 J 139 66.3 87.9 253 <10 1,890 446 124 13,100 16,800 3,930 <100 7,290 J 339
07/09/14 8,360 18,600 2,030 10,100 4,240 465 <5.0 23.8 J 14.2 J 204 84.7 146 300 <5.0 2,000 499 270 17,300 <1,800 3,500 <400 6,960 639 J
03/24/15 11,500 23,800 3,190 18,000 6,290 1,110 <74 104 J <69 270 182 J 273 645 <74 4,730 1,300 NR NR NR NR NR NR NR
01/11/16 13,800 31,700 6,140 31,800 4,400 2,550 <31 520 214 250 484 227 2,010 <31 5,470 3,740 NR NR NR NR NR NR NR
05/02/18 14,900 36,000 3,110 16,600 6,500 761 NR NR NR NR NR 323 NR NR NR NR NR NR NR NR NR NR NR
06/11/18 9,630 22,600 2,680 14,000 4,070 1,070 <25 54.1 J 27.1 J 231 114 204 344 <25 2,910 793 NR NR NR NR NR NR NR
02/20/19 9,700 23,700 2,450 13,100 3,300 836 NR NR NR NR NR 195 J NR NR NR NR NR NR NR NR NR NR NR
03/27/19 7,990 20,500 2,650 13,400 2,060 681 <63 74.7 J <63 142 J 133 J 131 J 429 <63 3,290 961 NR NR NR NR NR NR NR
04/23/08 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
01/07/09 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
05/12/10 777 148 131 340 185 417 <0.500 135 75.0 <0.500 52.4 50.7 95.8 3.30 380 148 12.2 3,740 1,780 231,000 50,800 1,940 88,200
MW-6
MWD-4
MW-7
Page 2 of 10
EPA
Method
6010B
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.6 70 70 0.4 70 70 70 0.7 400 400 15 400 700 700 10,000 200 200
5,000 260,000 84,500 85,500 20,000 6,000 NE 6,900 8,500 400 25,000 70,000 30,000 700 28,500 25,000 15,000 NE NE NE NE NE NE
2L Standard (mg/l)
GCL (mg/l)BenzeneIsopropylbenzenen-ButylbenzeneBromodichloromethanesec-Butylbenzene1,2-Dichloroethanen-PropylbenzeneMTBETABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
RED APPLE MARKET #3 (INCIDENT NO. 10673)
Analytical Method

Date: 04/05/19 Facility ID #: 0-017539
EPA Method 6200B MADEP Methods VPH and EPH
C9-C12 Aliphatics1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneC5-C8 AliphaticsC11-C22 AromaticsC19-C36 AliphaticsContaminant of
Concern C9-C10 AromaticsLeadNaphthaleneIPETolueneEthylbenzeneXylenesTetrachloroetheneC9-C18 Aliphatics05/02/11 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP NR NR NR NR NR NR NR
08/28/12 377 58.3 69.8 177 94.5 269 <1.2 12.2 15.0 14.4 16.2 17.3 26.1 1.5 J 200 52.2 NR NR NR NR NR NR NR
08/19/13 329 11.5 42.9 82.5 106 141 <1.0 13.1 17.8 14.3 14.4 18.4 25.6 3.0 J 116 19.7 22.6 544 J 2,500 90,800 25,600 1,580 15,200
07/09/14 274 9.3 43.7 87.1 217 197 <1.0 40.8 45.3 22.5 25.4 32.4 38.3 3.0 J 189 54.2 12.1 1,140 J 4,310 74,300 29,500 4,730 36,800
03/24/15 101 7.2 9.5 40.2 21.4 115 <0.74 8.0 10.9 3.7 9.8 4.7 11.3 1.5 J 79.0 24.1 NR NR NR NR NR NR NR
01/11/16 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/11/18 127 1.3 J 6.9 29.4 40.4 110 <0.63 3.4 5.3 5.5 5.1 9.9 5.5 1.1 J 52.5 13.1 NR NR NR NR NR NR NR
03/27/19 127 2.3 J 41.9 139 22.5 254 <1.3 19.0 22.9 3.5 J 22.3 6.6 30.1 <1.3 219 54.4 NR NR NR NR NR NR NR
04/23/08 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
08/28/12 319 237 599 1,150 <1.3 237 <1.2 62.2 27.1 <1.6 75.1 6.4 339 <1.4 1,930 651 NR NR NR NR NR NR NR
08/19/13 153 98.9 432 1,270 20.7 229 <1.0 126 54.2 6.1 133 <1.0 419 <1.0 1,190 673 15.4 4,170 J 5,640 5,910 227 7,010 967 J
07/09/14 201 142 488 981 6.4 J 205 <2.5 183 68.2 <2.5 112 3.1 J 542 <2.5 1,830 968 48.9 6,360 <1,800 17,100 1,930 J 6,600 2,880
03/24/15 164 149 343 1,080 6.7 J 136 <3.7 54.9 24.5 <4.1 65.2 <4.0 291 <3.7 2,820 E 1,150 NR NR NR NR NR NR NR
01/11/16 349 160 405 1,160 26.6 J 352 <13 414 128 <13 133 <13 770 <13 <13 1,320 NR NR NR NR NR NR NR
04/23/08 205 L 0.690 I <0.31 22.5 17.4 45.2 <0.14 0.530 I <0.47 2.44 2.50 4.51 I <0.30 3.88 1.12 <0.27 33.3 527 187 308 723 <100 345
01/07/09 160 <0.70 <0.50 31 <0.50 38 B <0.90 13 <0.70 <1.1 4.0 J 4.5 J <0.75 2.4 J 1.0 J <0.50 29.6 536 <100 <111 <111 <100 249
05/12/10 13.3 <0.500 <0.500 1.69 0.810 <5.00 <0.500 <0.500 <0.500 <0.500 0.540 <0.500 <0.500 <0.500 <0.500 <0.500 37.9 122 <100 <99.0 <99.0 <100 <99.0
05/03/11 7.7 <0.13 <0.15 2.7 0.82 1.1 <0.12 <0.10 <0.10 0.19 J 0.19 J 0.23 J <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 70.5 0.25 J <0.15 28.2 3.8 17.8 <0.13 0.46 J 0.32 J 0.94 2.8 1.5 <0.11 0.23 J 0.88 <0.10 NR NR NR NR NR NR NR
08/19/13 6.5 <0.10 <0.10 1.2 J 0.77 1.2 <0.10 <0.10 <0.10 0.26 J 0.45 J 0.36 J <0.10 <0.10 <0.10 <0.10 14.9 <35 <35 <110 <110 <35 <160
07/08/14 26.3 0.16 J <0.10 3.0 0.91 7.0 <0.10 0.20 J 0.17 J 0.27 J 1.6 0.46 J <0.10 <0.10 0.30 J <0.10 85.0 148 <35 <100 <100 <35 465
03/24/15 2.1 <0.17 <0.15 0.79 J 0.81 0.61 <0.15 <0.14 <0.14 <0.16 0.23 J 0.36 J <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NR
04/23/08 <0.31 <0.28 <0.31 <1.2 <0.12 <0.41 <0.14 <0.39 <0.47 <0.12 <0.24 <0.15 <0.30 <0.33 <0.26 <0.27 33.7 <100 <100 133 147 <100 122
01/07/09 27 2.7 J 3.5 J 2.9 J <0.50 18 B <0.90 <0.85 <0.70 <1.1 1.9 J <1.0 <0.75 <0.80 1.0 J 1.3 J 77.3 253 <100 <111 <111 <100 262
05/12/10 126 522 176 206 2.25 73.5 <0.500 3.94 1.48 <0.500 13.9 1.43 23.2 <0.500 54.4 10.8 40.1 3,590 314 <99.0 <99.0 389 <99.0
05/03/11 105 1,090 237 534 <3.3 43.0 <2.9 <2.5 <2.6 <4.1 6.3 J <2.7 19.7 <3.4 102 12.9 J NR NR NR NR NR NR NR
08/28/12 7.0 15.5 8.4 17.1 <0.13 4.3 <0.12 <0.10 <0.10 <0.16 0.41 J <0.11 0.81 <0.14 2.9 <0.10 NR NR NR NR NR NR NR
08/19/13 28.6 260 69.4 139 <1.0 20.4 <1.0 <1.0 <1.0 <1.0 3.2 J <1.0 6.9 <1.0 38.0 7.4 49.8 291 222 107 J <100 127 <150
07/08/14 42.8 284 74.7 167 <0.10 30.6 <0.10 1.0 0.52 <0.10 4.3 0.14 J 10.4 <0.10 38.6 4.5 111 902 <35 <100 <100 241 <150
03/24/15 <0.17 0.65 <0.15 <0.43 <0.16 <0.12 <0.15 <0.14 <0.14 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NR
MW-9
MW-11
MW-8
MW-10
Page 3 of 10
EPA
Method
6010B
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.6 70 70 0.4 70 70 70 0.7 400 400 15 400 700 700 10,000 200 200
5,000 260,000 84,500 85,500 20,000 6,000 NE 6,900 8,500 400 25,000 70,000 30,000 700 28,500 25,000 15,000 NE NE NE NE NE NE
2L Standard (mg/l)
GCL (mg/l)BenzeneIsopropylbenzenen-ButylbenzeneBromodichloromethanesec-Butylbenzene1,2-Dichloroethanen-PropylbenzeneMTBETABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
RED APPLE MARKET #3 (INCIDENT NO. 10673)
Analytical Method

Date: 04/05/19 Facility ID #: 0-017539
EPA Method 6200B MADEP Methods VPH and EPH
C9-C12 Aliphatics1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneC5-C8 AliphaticsC11-C22 AromaticsC19-C36 AliphaticsContaminant of
Concern C9-C10 AromaticsLeadNaphthaleneIPETolueneEthylbenzeneXylenesTetrachloroetheneC9-C18 Aliphatics04/23/08 108 <1.4 <1.6 <5.8 415 9.30 <0.70 <2.0 <2.4 6.75 <1.2 4.30 I <1.5 <1.7 1.70 I <1.4 6.07 225 122 361 206 <100 440
01/07/09 92 <0.70 <0.50 2.5 J 820 8.2 B <0.90 <0.85 <0.70 16 1.2 J 13 J <0.75 <0.80 <0.70 <0.50 23.5 10,100 <100 <111 <111 <100 <111
05/12/10 17.1 <0.500 <0.500 <1.00 357 <5.00 <0.500 <0.500 <0.500 9.90 <0.500 8.94 <0.500 <0.500 <0.500 <0.500 23.9 316 <100 <100 <100 <100 <100
05/03/11 7.6 <1.3 <1.5 <3.0 461 <1.0 <1.2 <1.0 <1.0 7.5 <1.0 10.1 <1.1 <1.4 <1.0 <1.0 NR NR NR NR NR NR NR
08/28/12 8.9 <0.13 <0.15 <0.30 114 0.87 <0.12 <0.10 <0.10 3.1 0.13 J 2.5 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 37.5 <1.0 <1.0 <2.2 326 3.4 J <1.0 <1.0 <1.0 8.2 <1.0 7.9 <1.0 <1.0 2.2 J <1.0 6.7 <35 <35 <100 <100 <35 <150
07/08/14 27.9 0.12 J <0.10 1.4 J 492 2.6 <0.10 <0.10 0.39 J 10.8 0.61 12.9 <0.10 <0.10 <0.10 <0.10 34.6 <70 <70 <100 <100 <70 162 J
03/24/15 14.7 0.59 <0.15 1.0 J 118 1.6 <0.15 <0.14 0.26 J 7.8 0.50 7.1 <0.16 0.19 J <0.14 <0.14 NR NR NR NR NR NR NR
04/23/08 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/09/09 70 140 53 140 4.5 J 34 B <0.90 <0.85 <0.70 <1.1 5.1 5.6 J 6.6 3.1 J 47 14 4.8 272 157 <105 <105 119 <105
05/12/10 234 200 217 323 2.07 94.5 <0.500 11.0 2.70 <0.500 17.1 20.2 34.9 1.31 153 64.1 6.40 1,590 513 <99.0 <99.0 609 <99.0
05/02/11 158 168 138 198.1 0.94 J 57.3 <0.59 1.5 J 0.92 J 4.1 7.9 9.3 20.8 0.76 J 98.4 31.9 NR NR NR NR NR NR NR
08/28/12 97.0 76.7 96.8 113 0.80 46.9 <0.12 0.94 1.0 3.4 6.0 9.0 7.6 1.2 20.6 6.5 NR NR NR NR NR NR NR
08/19/13 36.0 39.6 30.8 64.0 0.26 J 24.4 <0.10 0.73 0.73 1.3 3.8 3.0 3.6 1.3 11.7 2.0 54.5 106 202 <100 <100 127 <150
07/09/14 45.7 12.3 27.0 54.1 0.44 J 22.7 <0.10 0.65 0.67 1.5 3.6 3.9 2.9 1.4 13.2 3.0 28.5 133 <35 <95 <95 61.9 J 145 J
04/24/08 0.510 I <0.28 <0.31 <1.2 <0.12 <0.41 <0.14 <0.39 <0.47 <0.12 <0.24 0.330 I <0.30 0.790 I <0.26 <0.27 238 <100 <100 <75 130 <100 <50
01/09/09 1.0 J 1.1 J 0.54 J <1.0 <0.50 3.2 JB <0.90 <0.85 <0.70 <1.1 <0.55 <1.0 <0.75 1.5 J <0.70 <0.50 80.4 <100 <100 <105 <105 <100 <105
05/12/10 23.5 0.710 0.620 6.97 <0.500 19.6 <0.500 <0.500 0.980 <0.500 2.44 3.36 0.600 1.66 2.69 <0.500 77.6 <100 <100 <99.0 <99.0 <100 <99.0
05/02/11 28.8 3.0 16.8 30.0 <0.13 15.9 <0.12 0.25 J 1.2 1.1 2.7 3.4 2.8 1.3 14.7 4.3 NR NR NR NR NR NR NR
08/28/12 57.7 1.9 60.6 33.5 0.21 J 26.7 <0.12 0.60 2.6 1.5 4.4 4.4 8.0 0.63 37.7 6.7 NR NR NR NR NR NR NR
08/19/13 10.9 0.40 J 12.7 9.3 <0.10 6.5 <0.10 0.12 J 0.74 0.46 J 1.0 1.5 2.0 0.77 7.5 1.3 94.8 36.8 J 72.0 J <100 193 J 58.6 J <150
07/09/14 12.5 0.27 J 4.3 8.3 0.13 J 7.7 <0.10 <0.10 1.5 0.63 1.2 2.2 0.70 0.77 4.1 0.59 46.4 51.2 J <35 <95 <95 37.4 J <140
03/24/15 31.2 1.3 2.2 13.4 <0.16 4.4 <0.15 <0.14 1.5 1.1 1.6 3.8 0.57 0.30 J 4.9 0.90 NR NR NR NR NR NR NR
01/11/16 79.8 1.1 27.9 32.5 0.29 J 29.6 <0.13 0.61 1.9 2.0 7.4 6.8 5.9 0.33 J 35.0 3.9 NR NR NR NR NR NR NR
04/24/08 <0.31 <0.28 <0.31 <1.2 <0.12 <0.41 <0.14 <0.39 <0.47 <0.12 <0.24 <0.15 <0.30 <0.33 <0.26 <0.27 60.1 <100 <100 370 6,660 <100 642
01/07/09 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
05/12/10 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 52.8 <100 <100 <100 <100 <100 <100
05/02/11 <0.13 <0.13 <0.15 <0.30 <0.13 0.23 J <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 6.0 <35 <35 <110 <110 <35 <160
07/08/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
MW-16 04/23/08 4.17 <0.28 <0.31 <1.2 0.580 I 0.770 I <0.14 <0.39 <0.47 <0.12 0.370 I 0.290 I <0.30 <0.33 0.280 I <0.27 15.3 <100 <100 205 466 <100 279
MW-12
MW-14
MW-13
MW-15
Page 4 of 10
EPA
Method
6010B
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.6 70 70 0.4 70 70 70 0.7 400 400 15 400 700 700 10,000 200 200
5,000 260,000 84,500 85,500 20,000 6,000 NE 6,900 8,500 400 25,000 70,000 30,000 700 28,500 25,000 15,000 NE NE NE NE NE NE
2L Standard (mg/l)
GCL (mg/l)BenzeneIsopropylbenzenen-ButylbenzeneBromodichloromethanesec-Butylbenzene1,2-Dichloroethanen-PropylbenzeneMTBETABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
RED APPLE MARKET #3 (INCIDENT NO. 10673)
Analytical Method

Date: 04/05/19 Facility ID #: 0-017539
EPA Method 6200B MADEP Methods VPH and EPH
C9-C12 Aliphatics1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneC5-C8 AliphaticsC11-C22 AromaticsC19-C36 AliphaticsContaminant of
Concern C9-C10 AromaticsLeadNaphthaleneIPETolueneEthylbenzeneXylenesTetrachloroetheneC9-C18 Aliphatics01/07/09 15 <0.70 <0.50 <1.0 1.5 J 2.8 JB <0.90 <0.85 <0.70 <1.1 1.6 J 1.1 J <0.75 <0.80 <0.70 <0.50 15.7 117 <100 <111 <111 <100 <111
05/12/10 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 34.0 <100 <100 <105 <105 <100 <105
05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 0.57 <0.13 <0.15 <0.30 0.13 J 0.12 J <0.12 <0.10 <0.10 <0.16 <0.10 0.17 J <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 10.8 0.16 J <0.10 0.40 J 0.29 J 1.7 <0.10 <0.10 0.23 J 0.17 J 1.6 0.31 J <0.10 <0.10 <0.10 <0.10 12.4 63.6 J <35 <100 <100 <35 <160
07/08/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
04/24/08 176 48.6 39.4 84.8 5.42 1.65 <0.14 0.610 I 0.540 I 2.57 2.55 4.07 I 6.10 <0.33 42.9 13.4 21.0 851 <100 93.1 94.2 204 96.0
01/09/09 52 11 12 13 J <0.50 1.4 JB <0.90 <0.85 <0.70 <1.1 1.4 J <1.0 2.4 J <0.80 10 2.0 J 4.8 465 <100 <100 <100 <100 <100
05/12/10 115 4.08 11.5 9.63 5.62 <5.00 <0.500 0.840 0.580 <0.500 2.31 4.03 2.97 <0.500 15.0 1.68 37.7 867 <100 <100 <100 <100 <100
05/02/11 138 7.3 17.1 10.0 J 2.7 1.2 J <0.59 <0.50 <0.51 1.2 J 1.0 J 2.2 J 2.9 <0.69 7.5 1.9 J NR NR NR NR NR NR NR
08/28/12 107 2.4 15.6 6.4 2.2 0.49 J <0.12 0.24 J 0.31 J 0.90 1.1 2.0 2.8 0.35 J 6.9 2.3 NR NR NR NR NR NR NR
08/19/13 33.1 0.54 7.3 2.5 0.94 0.20 J <0.10 0.18 J 0.22 J 0.42 J 0.72 0.96 2.0 0.20 J 2.8 1.3 18.1 90.5 J 56.4 J <100 <100 <35 <160
07/09/14 39.7 0.40 J 3.5 1.2 J 1.3 0.35 J <0.10 <0.10 0.20 J 0.41 J 0.45 J 1.4 0.82 0.27 J 2.7 0.61 11.3 86.4 J <35 <96 <96 <35 <140
03/24/15 183 4.0 4.7 <2.2 4.5 2.1 J <0.74 <0.72 <0.69 2.1 J 0.94 J 3.5 1.2 J <0.74 5.2 <0.68 NR NR NR NR NR NR NR
01/11/16 5.6 <0.13 0.18 J <0.31 0.58 <0.13 <0.13 <0.13 <0.13 0.24 J 0.23 J 0.74 <0.13 0.31 J 0.78 <0.13 NR NR NR NR NR NR NR
04/24/08 <0.31 <0.28 <0.31 <1.2 <0.12 <0.41 <0.14 <0.39 <0.47 <0.12 <0.24 <0.15 <0.30 <0.33 <0.26 <0.27 20.4 <100 <100 167 212 <100 216
01/09/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <0.90 <0.85 <0.70 <1.1 <0.55 <1.0 <0.75 <0.80 <0.70 <0.50 13.8 <100 <100 <105 <105 <100 <105
05/12/10 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 15.6 <35 <35 <110 <110 <35 <160
07/08/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 29.9 <35 <35 <99 <99 <35 <150
03/24/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.15 <0.14 <0.14 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NR
04/24/08 286 0.320 I <0.31 4.89 197 12.9 <0.14 <0.39 <0.47 10.5 1.97 14.3 <0.30 <0.33 <0.26 <0.27 7.21 539 117 152 196 <100 179
01/09/09 130 <0.70 <0.50 3.0 J 78 6.7 B <0.90 <0.85 <0.70 4.5 J 1.3 J 11 J <0.75 <0.80 <0.70 <0.50 13.1 461 <100 <105 <105 <100 <105
05/12/10 119 <0.500 <0.500 3.94 224 7.61 <0.500 <0.500 0.520 9.43 1.72 11.6 <0.500 <0.500 <0.500 <0.500 12.8 445 <100 <103 <103 <100 <103
05/03/11 42.2 <0.13 <0.15 0.34 J 100 2.7 <0.12 <0.10 0.14 J 3.0 0.15 J 6.6 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 28.0 <0.13 <0.15 0.62 J 102 2.3 <0.12 <0.10 0.26 J 7.8 0.13 J 7.8 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 8.6 <0.10 <0.10 0.26 J 75.5 0.44 J <0.10 <0.10 0.37 J 2.1 0.23 J 8.5 <0.10 <0.10 <0.10 <0.10 14.0 36.3 J <35 <100 <100 <35 <150
07/08/14 9.3 <0.10 <0.10 0.41 J 120 0.37 J <0.10 <0.10 0.59 1.7 0.63 10.1 <0.10 <0.10 <0.10 <0.10 25.9 87.7 J <35 <99 <99 <35 249
03/24/15 4.3 <0.83 <0.76 <2.2 211 <0.61 <0.74 <0.72 0.73 J 2.5 1.4 J 12.0 <0.78 <0.74 <0.68 <0.68 NR NR NR NR NR NR NR
MW-17
MW-19
MW-16A
MW-18
Page 5 of 10
EPA
Method
6010B
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.6 70 70 0.4 70 70 70 0.7 400 400 15 400 700 700 10,000 200 200
5,000 260,000 84,500 85,500 20,000 6,000 NE 6,900 8,500 400 25,000 70,000 30,000 700 28,500 25,000 15,000 NE NE NE NE NE NE
2L Standard (mg/l)
GCL (mg/l)BenzeneIsopropylbenzenen-ButylbenzeneBromodichloromethanesec-Butylbenzene1,2-Dichloroethanen-PropylbenzeneMTBETABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
RED APPLE MARKET #3 (INCIDENT NO. 10673)
Analytical Method

Date: 04/05/19 Facility ID #: 0-017539
EPA Method 6200B MADEP Methods VPH and EPH
C9-C12 Aliphatics1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneC5-C8 AliphaticsC11-C22 AromaticsC19-C36 AliphaticsContaminant of
Concern C9-C10 AromaticsLeadNaphthaleneIPETolueneEthylbenzeneXylenesTetrachloroetheneC9-C18 Aliphatics04/24/08 <0.31 <0.28 <0.31 <1.2 <0.12 <0.41 <0.14 <0.39 <0.47 <0.12 <0.24 <0.15 <0.30 <0.33 <0.26 <0.27 34.1 <100 <100 <75 <75 <100 <50
01/09/09 1.4 J <0.70 <0.50 <1.0 <0.50 0.67 JB <0.90 <0.85 <0.70 <1.1 <0.55 <1.0 <0.75 <0.80 <0.70 <0.50 24.0 <100 <100 <105 <105 <100 <105
05/12/10 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 44.2 <100 <100 <102 <102 <100 <102
05/02/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 0.45 J <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 28.2 <35 <35 <100 <100 <35 <150
07/09/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 60.3 <35 <35 <96 <96 <35 <140
03/24/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.15 <0.14 <0.14 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NR
04/24/08 <0.31 <0.28 <0.31 <1.2 <0.12 <0.41 <0.14 <0.39 <0.47 <0.12 <0.24 <0.15 <0.30 0.410 I <0.26 <0.27 32.9 <100 <100 <75 <75 <100 <50
01/09/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <0.90 <0.85 <0.70 <1.1 <0.55 <1.0 <0.75 <0.80 <0.70 <0.50 53.0 <100 <100 <105 <105 <100 <105
05/02/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 5.6 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 39.1 <35 <35 <100 <100 <35 <150
07/09/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 75.2 <35 <35 <96 <96 <35 141 J
03/24/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.15 <0.14 <0.14 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NR
04/24/08 19.2 <0.28 <0.31 <1.2 9.01 1.54 <0.14 <0.39 <0.47 1.35 <0.24 1.96 I <0.30 <0.33 <0.26 <0.27 24.6 <100 <100 <75 90.9 <100 <50
01/09/09 <0.60 <0.70 <0.50 <1.0 3.2 J <0.60 <0.90 <0.85 <0.70 <1.1 <0.55 <1.0 <0.75 <0.80 <0.70 <0.50 25.6 <100 <100 <105 <105 <100 <105
05/12/10 3.90 <0.500 <0.500 <1.00 6.17 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 1.14 <0.500 <0.500 <0.500 <0.500 21.5 <100 <100 <108 <108 <100 <108
05/03/11 0.33 J <0.13 <0.15 <0.30 5.3 <0.10 <0.12 <0.10 <0.10 0.38 J <0.10 0.58 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 <0.13 <0.13 <0.15 <0.30 2.8 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 <0.10 <0.10 <0.10 <0.22 1.5 <0.15 <0.10 <0.10 <0.10 0.25 J <0.10 0.64 <0.10 <0.10 <0.10 <0.10 18.2 <35 <35 <110 <110 <35 <160
07/08/14 0.13 J <0.10 <0.10 <0.20 1.5 <0.10 <0.10 <0.10 <0.10 0.23 J <0.10 0.76 <0.10 <0.10 <0.10 <0.10 29.0 <35 <35 <200 827 <35 716
03/24/15 1.1 <0.17 <0.15 <0.43 2.9 <0.12 <0.15 <0.14 <0.14 0.23 J <0.12 0.88 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NR
04/24/08 <0.31 <0.28 <0.31 <1.2 0.380 I <0.41 <0.14 <0.39 <0.47 <0.12 <0.24 <0.15 <0.30 <0.33 <0.26 <0.27 32.7 <100 <100 <75 <75 <100 <50
01/09/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <0.90 <0.85 <0.70 <1.1 <0.55 <1.0 <0.75 <0.80 <0.70 <0.50 40.0 <100 <100 <105 <105 <100 <105
05/12/10 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 60.9 <100 <100 <108 <108 <100 <108
05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
MW-20
MW-21
MW-22
MW-23
Page 6 of 10
EPA
Method
6010B
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.6 70 70 0.4 70 70 70 0.7 400 400 15 400 700 700 10,000 200 200
5,000 260,000 84,500 85,500 20,000 6,000 NE 6,900 8,500 400 25,000 70,000 30,000 700 28,500 25,000 15,000 NE NE NE NE NE NE
2L Standard (mg/l)
GCL (mg/l)BenzeneIsopropylbenzenen-ButylbenzeneBromodichloromethanesec-Butylbenzene1,2-Dichloroethanen-PropylbenzeneMTBETABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
RED APPLE MARKET #3 (INCIDENT NO. 10673)
Analytical Method

Date: 04/05/19 Facility ID #: 0-017539
EPA Method 6200B MADEP Methods VPH and EPH
C9-C12 Aliphatics1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneC5-C8 AliphaticsC11-C22 AromaticsC19-C36 AliphaticsContaminant of
Concern C9-C10 AromaticsLeadNaphthaleneIPETolueneEthylbenzeneXylenesTetrachloroetheneC9-C18 Aliphatics04/24/08 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/07/09 0.68 J <0.70 <0.50 <1.0 <0.50 0.68 JB <0.90 <0.85 <0.70 <1.1 <0.55 <1.0 <0.75 <0.80 <0.70 <0.50 17.1 <100 <100 <111 <111 <100 <111
05/12/10 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 18.6 <35 <35 <110 <110 <35 <160
07/08/14 <0.10 0.11 J <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 6.6 <35 <35 <100 <100 <35 <150
04/23/08 <0.31 <0.28 <0.31 <1.2 <0.12 0.800 I <0.14 <0.39 <0.47 <0.12 <0.24 <0.15 <0.30 <0.33 <0.26 <0.27 9.66 <100 <100 96.4 88.3 <100 133
01/09/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <0.90 <0.85 <0.70 <1.1 <0.55 <1.0 <0.75 <0.80 <0.70 <0.50 14.6 <100 <100 <105 <105 <100 <105
05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
08/19/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 17.0 <35 <35 <110 <110 <35 <170
07/08/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 32.5 <35 <35 <99 <99 <35 <150
03/24/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.15 <0.14 <0.14 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NR
04/23/08 <0.31 <0.28 <0.31 <1.2 <0.12 <0.41 <0.14 <0.39 <0.47 <0.12 <0.24 <0.15 <0.30 <0.33 <0.26 <0.27 42.4 <100 <100 <75 <75 <100 87.2
01/07/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <0.90 <0.85 <0.70 <1.1 <0.55 <1.0 <0.75 <0.80 <0.70 <0.50 38.3 <100 <100 <111 <111 <100 <111
05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 0.42 J <0.10 <0.11 <0.11 0.93 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 0.48 J <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 0.40 J <0.10 <0.10 32.8 <35 <35 <110 <110 <35 <160
07/08/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 0.31 J <0.10 0.74 <0.10 0.29 J <0.10 <0.10 41.0 <35 <35 <100 <100 <35 <150
04/24/08 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/07/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <0.90 <0.85 <0.70 <1.1 <0.55 <1.0 <0.75 <0.80 <0.70 <0.50 53.5 <100 <100 <111 <111 <100 <111
05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
04/24/08 <0.31 <0.28 <0.31 <1.2 0.680 I <0.41 <0.14 <0.39 <0.47 <0.12 <0.24 <0.15 <0.30 <0.33 <0.26 <0.27 59.1 <100 <100 <75 94.6 <100 <50
01/09/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <0.90 <0.85 <0.70 <1.1 <0.55 <1.0 <0.75 <0.80 <0.70 <0.50 40.4 <100 <100 <105 <105 <100 <105
05/03/11 <0.13 <0.13 <0.15 <0.30 0.20 J <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 0.22 J <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/24/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.15 <0.14 <0.14 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NR
MW-26
MW-27
MW-24
MW-25
MW-28
Page 7 of 10
EPA
Method
6010B
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.6 70 70 0.4 70 70 70 0.7 400 400 15 400 700 700 10,000 200 200
5,000 260,000 84,500 85,500 20,000 6,000 NE 6,900 8,500 400 25,000 70,000 30,000 700 28,500 25,000 15,000 NE NE NE NE NE NE
2L Standard (mg/l)
GCL (mg/l)BenzeneIsopropylbenzenen-ButylbenzeneBromodichloromethanesec-Butylbenzene1,2-Dichloroethanen-PropylbenzeneMTBETABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
RED APPLE MARKET #3 (INCIDENT NO. 10673)
Analytical Method

Date: 04/05/19 Facility ID #: 0-017539
EPA Method 6200B MADEP Methods VPH and EPH
C9-C12 Aliphatics1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneC5-C8 AliphaticsC11-C22 AromaticsC19-C36 AliphaticsContaminant of
Concern C9-C10 AromaticsLeadNaphthaleneIPETolueneEthylbenzeneXylenesTetrachloroetheneC9-C18 Aliphatics04/24/08 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/09/09 200 <0.70 <0.50 4.0 J <0.50 28 B <0.90 13 B 0.75 J <1.1 3.7 J <1.0 <0.75 2.1 J <0.70 <0.50 3.5 627 <100 <105 <105 <100 <105
05/12/10 149 <0.500 <0.500 2.52 3.79 20.0 <0.500 0.520 <0.500 <0.500 3.59 1.72 <0.500 1.11 <0.500 <0.500 15.7 519 <100 <108 <108 <100 <108
05/03/11 35.3 <0.13 <0.15 0.35 J 1.4 2.7 <0.12 <0.10 <0.10 0.41 J 0.61 0.47 J <0.11 0.24 J <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 6.2 <0.13 <0.15 <0.30 1.7 0.39 J <0.12 <0.10 <0.10 0.41 J 0.43 J 0.37 J <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 1.0 <0.10 <0.10 <0.22 1.6 <0.15 <0.10 <0.10 <0.10 0.47 J <0.10 0.49 J <0.10 <0.10 <0.10 <0.10 7.7 <35 <35 <110 <110 <35 <160
07/08/14 <0.10 <0.10 <0.10 <0.20 1.7 <0.10 <0.10 <0.10 <0.10 0.38 J <0.10 0.41 J <0.10 <0.10 <0.10 <0.10 20.9 <35 <35 <100 <100 <35 <150
03/24/15 <0.17 <0.17 <0.15 <0.43 0.34 J <0.12 <0.15 <0.14 <0.14 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NR
MW-30 04/24/08 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
04/24/08 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/07/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <0.90 <0.85 <0.70 <1.1 <0.55 <1.0 <0.75 <0.80 <0.70 <0.50 11.0 <100 <100 <111 <111 <100 <111
05/12/10 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 69.9 <100 <100 <108 <108 <100 <108
05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
08/19/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/24/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.15 <0.14 <0.14 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NR
04/24/08 <0.31 <0.28 <0.31 <1.2 <0.12 <0.41 <0.14 <0.39 <0.47 <0.12 <0.24 <0.15 <0.30 <0.33 <0.26 <0.27 41.6 <100 <100 <75 94.6 <100 88.1
01/09/09 1.7 J <0.70 <0.50 <1.0 <0.50 2.7 JB <0.90 <0.85 <0.70 <1.1 <0.55 <1.0 <0.75 <0.80 <70 <0.50 29.1 <100 <100 <105 <105 <100 <105
05/12/10 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 46.8 <100 <100 <108 <108 <100 <108
05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 0.29 J <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 0.28 J <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
04/24/08 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/09/09 <0.60 <0.70 <0.50 <1.0 <0.50 0.84 JB <0.90 <0.85 <0.70 <1.1 <0.55 <1.0 <0.75 <0.80 <0.70 <0.50 18.9 <100 <100 <105 <105 <100 <105
05/12/10 1.41 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 45.0 <100 <100 <111 <111 <100 <111
05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 28.7 <35 <35 <110 <110 <35 <160
07/08/14 <0.10 0.34 J <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 76.4 <35 <35 <100 <100 <35 <150
03/24/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.15 <0.14 <0.14 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NR
MW-29
MW-31
MW-33
MW-32
Page 8 of 10
EPA
Method
6010B
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.6 70 70 0.4 70 70 70 0.7 400 400 15 400 700 700 10,000 200 200
5,000 260,000 84,500 85,500 20,000 6,000 NE 6,900 8,500 400 25,000 70,000 30,000 700 28,500 25,000 15,000 NE NE NE NE NE NE
2L Standard (mg/l)
GCL (mg/l)BenzeneIsopropylbenzenen-ButylbenzeneBromodichloromethanesec-Butylbenzene1,2-Dichloroethanen-PropylbenzeneMTBETABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
RED APPLE MARKET #3 (INCIDENT NO. 10673)
Analytical Method

Date: 04/05/19 Facility ID #: 0-017539
EPA Method 6200B MADEP Methods VPH and EPH
C9-C12 Aliphatics1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneC5-C8 AliphaticsC11-C22 AromaticsC19-C36 AliphaticsContaminant of
Concern C9-C10 AromaticsLeadNaphthaleneIPETolueneEthylbenzeneXylenesTetrachloroetheneC9-C18 Aliphatics05/12/10 59.1 <0.500 <0.500 <1.00 1.37 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 1.17 <0.500 6.52 <0.500 <0.500 146 120 <100 <118 <118 <100 <118
05/03/11 41.5 <0.13 <0.15 0.12 J 1.0 3.3 <0.12 <0.10 <0.10 0.38 J 0.14 J 0.62 <0.11 4.9 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 8.6 <0.13 <0.15 <0.30 0.31 J 0.69 <0.12 <.010 <0.10 <0.16 <0.10 0.18 J <0.11 1.1 <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 10.6 <0.10 <0.10 <0.22 0.63 1.2 <0.10 <0.10 <0.10 0.26 J <0.10 0.47 J <0.10 1.6 <0.10 <0.10 12.3 <35 <35 <110 <110 <35 <160
07/08/14 6.2 0.11 J <0.10 <0.20 0.58 0.80 <0.10 <0.10 <0.10 0.22 J <0.10 0.45 J <0.10 1.1 <0.10 <0.10 46.8 <35 <35 <99 <99 <35 <150
03/24/15 0.49 J <0.17 <0.15 <0.43 0.39 J <0.12 <0.15 <0.14 <0.14 <0.16 <0.12 0.27 J <0.16 0.53 <0.14 <0.14 NR NR NR NR NR NR NR
05/12/10 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 381 <100 <100 <121 <121 <100 <121
05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
05/12/10 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 314 <100 <100 <118 <118 <100 <118
05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
05/03/11 3.4 <0.13 <0.15 <0.30 0.29 J 0.19 J <0.12 <0.10 <0.10 <0.16 <0.10 0.19 J <0.11 1.1 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 0.47 J <0.13 <0.15 <0.30 0.21 J <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 0.16 J <0.11 0.69 <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/24/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.15 <0.14 <0.14 <0.16 <0.12 <0.16 <0.16 0.17 J <0.14 <0.14 NR NR NR NR NR NR NR
05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/24/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.15 <0.14 <0.14 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NR
05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/24/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.15 <0.14 <0.14 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NR
MW-34
MW-37
MW-38
MW-35
MW-36
MW-39
Page 9 of 10
EPA
Method
6010B
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.6 70 70 0.4 70 70 70 0.7 400 400 15 400 700 700 10,000 200 200
5,000 260,000 84,500 85,500 20,000 6,000 NE 6,900 8,500 400 25,000 70,000 30,000 700 28,500 25,000 15,000 NE NE NE NE NE NE
2L Standard (mg/l)
GCL (mg/l)BenzeneIsopropylbenzenen-ButylbenzeneBromodichloromethanesec-Butylbenzene1,2-Dichloroethanen-PropylbenzeneMTBETABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
RED APPLE MARKET #3 (INCIDENT NO. 10673)
Analytical Method

Date: 04/05/19 Facility ID #: 0-017539
EPA Method 6200B MADEP Methods VPH and EPH
C9-C12 Aliphatics1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneC5-C8 AliphaticsC11-C22 AromaticsC19-C36 AliphaticsContaminant of
Concern C9-C10 AromaticsLeadNaphthaleneIPETolueneEthylbenzeneXylenesTetrachloroetheneC9-C18 Aliphatics05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 3.3 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 0.81 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 81.7 <35 <35 <110 <110 <35 <160
07/09/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 0.21 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 129 <35 <35 <97 <97 <35 <150
03/24/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.15 <0.14 <0.14 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NR
Spigot -1 05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 10.4 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
Spigot-2 05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 3.4 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
Spigot-3 05/03/11 <0.13 <0.13 <0.15 <0.30 0.19 J <0.10 8.3 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
Spigot-4 05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 6.5 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
Spigot-5 05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 6.7 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
Spigot-6 05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 0.18 J 7.7 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
Spigot-7 05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 7.5 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
Spigot-8 05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 6.7 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
Notes:
• Results reported in mg/l (micrograms per liter).
• 2L Standard: as specified in T15A NCAC 2L.0202
• GCL : Gross contamination level.
• < : Less than the method detection limit specified in the laboratory report.
• Concentrations in bold face type exceeded the 2L Standards; concentrations in italics exceeded the GCLs.
• FP: Free Product.
• NE: Not established.
• NS: Not sampled; well not located.
• NR: Analyses not requested.
• J or I: Estimated value.
• B: Present in laboratory blank.
• 02/20/19 sample collected pre-AFVR event.
• Refer to laboratory report for other compounds detected which did not exceed the 2L Standards.
MW-40
Page 10 of 10

APPENDICES

APPENDIX A
AFVR Data and Calculations
AGGRESSIVE FLUID VAPOR RECOVERY EVENT DATA SHEET
Site Name :RAM #3
Incident Number :10673
Average Depth to Ground Water :7.94 ft
Well Name:Inner Dia. of Well (inches):2
Blower Specifications For Vacuum Truck (e.g: 2500 cfm @ 24 in. of Hg) :680 cfm @ 18" of Hg
Diameter of Exhaust Stack (inches) :6
Start Time :7:30 Date :02/20/19
End Time :15:30
Note: Take all the readings listed below every 15 minutes for the first 2 hours of the test and every
30 minutes thereafter.
Test Conducted By (AFVR Contractor):Greenwood Applied Services
Test Supervised By (Consultant):Geological Resources, Inc.
Frequency Time Vacuum
Exhaust
Velocity Temperature Rel. Humidity OVA
(min)(in. of Hg)(ft/min)(°F)(%)(ppm)
0 7:30 26.0 1,616 65.3 24.9 52.5
15 7:45 26.0 1,559 65.0 43.1 50.0
30 8:00 26.0 1,369 51.5 47.0 51.7
45 8:15 26.5 1,418 61.7 42.3 61.2
60 8:30 26.5 1,279 63.0 36.8 65.6
75 8:45 26.5 1,399 59.1 34.0 70.3
90 9:00 26.5 1,317 62.5 32.8 74.9
105 9:15 26.5 1,279 64.6 33.7 60.5
120 9:30 26.5 1,343 66.2 27.1 72.5
150 10:00 26.5 1,397 67.1 31.0 63.7
180 10:30 26.5 1,283 67.5 34.9 84.7
210 11:00 26.5 1,460 66.8 38.3 77.2
240 11:30 26.5 1,327 69.1 41.5 78.7
270 12:00 26.5 1,446 69.3 40.0 75.9
300 12:30 26.5 1,595 77.0 49.7 73.5
330 13:00 26.5 1,526 71.0 38.1 75.9
360 13:30 26.5 1,513 73.0 38.1 67.7
390 14:00 26.5 1,429 72.9 36.8 75.6
420 14:30 26.5 1,463 69.8 39.1 74.4
450 15:00 26.5 1,703 69.0 41.6 70.8
480 15:30 26.5 1,404 67.0 36.8 1.9
Total Fluids Recovered (in gallons) :2,533
Total Product Recovered (in gallons) :1.92
MW-7
AGGRESSIVE FLUID VAPOR RECOVERY EVENT DATA SHEET (Cont'd.)
Site Name :RAM #3
Incident Number :10673
Well Name:Inner Dia. of Well (inches):2.00
Start Time :7:30 Date :02/20/19
End Time :15:30
Note: Record water levels in Vacuum Well at start and end of Test. Record Water Levels in a few
Observation Wells periodically (hourly during event) and at end of event.
Test Conducted By (AFVR Contractor):Greenwood Applied Services
Test Supervised By (Consultant):Geological Resources, Inc.
Parameters AFVR Well Obs. Well 1 Obs. Well 2 Obs. Well 3 Obs. Well 4
Well Name MW-7 MW-2 MW-8 MW-17
Diameter (in.)2 2 2 2
Distance from
AFVR Well (ft)
Depth to Water Measurements (in feet)
Frequency Time AFVR Well Obs Well 1 Obs. Well 2 Obs. Well 3 Obs. Well 4
(min)(ft.)(ft.)(ft.)(ft.)(ft.)
0 (Before Start)7:30 7.86 8.46 7.80 7.65
60 8:30 ---------
120 9:30 8.78 8.00 7.84
180 10:30 8.85 8.10 7.80
240 11:30 8.90 8.10 7.82
300 12:30 8.90 8.10 7.82
360 13:30 8.91 8.10 7.83
420 14:30 8.91 8.10 7.82
480 15:30 8.93 8.10 7.80
End of Test 7.86
0 55 55 110
MW-7
AGGRESSIVE FLUID VAPOR RECOVERY EVENT
SITE NAME:RAM #3 Date: 2/20/2019
INCIDENT NUMBER:10673
AVERAGE DEPTH TO GROUNDWATER:7.94 ft
DESCRIBE SOIL IN THE SATURATED ZONE:
INDICATE AVERAGE HYDRAULIC CONDUCTIVITY unknown
IDENTIFY THE WELL AND THE I.D. OF EACH WELL USED FOR AFVR:
PROVIDE BLOWER SPECIFICATIONS OF THE VACUUM TRUCK (cfm @ in Hg):680 cfm @ 18" of Hg
DRY STANDARD CUBIC FEET PER MINUTE (DSCFM) AIR FLOW CALCULATIONS (Qstd)
Vacuum Velocity Pipe ID Temp Rel Humid Water Qstd
(inches of Hg)(ft/min)(in)(°F)(%)Vapor (%)(flow)
02/20/19 7:30 26.0 1,616 6 65.3 24.9 0.0033 318
02/20/19 7:45 26.0 1,559 6 65.0 43.1 0.0056 306
02/20/19 8:00 26.0 1,369 6 51.5 47.0 0.0038 276
02/20/19 8:15 26.5 1,418 6 61.7 42.3 0.0049 280
02/20/19 8:30 26.5 1,279 6 63.0 36.8 0.0045 252
02/20/19 8:45 26.5 1,399 6 59.1 34.0 0.0036 278
02/20/19 9:00 26.5 1,317 6 62.5 32.8 0.0039 260
02/20/19 9:15 26.5 1,279 6 64.6 33.7 0.0043 252
02/20/19 9:30 26.5 1,343 6 66.2 27.1 0.0037 264
02/20/19 10:00 26.5 1,397 6 67.1 31.0 0.0044 274
06/05/14 10:30 26.5 1,283 6 67.5 34.9 0.0050 251
02/20/19 11:00 26.5 1,460 6 66.8 38.3 0.0053 286
02/20/19 11:30 26.5 1,327 6 69.1 41.5 0.0063 258
02/20/19 12:00 26.5 1,446 6 69.3 40.0 0.0061 281
02/20/19 12:30 26.5 1,595 6 77.0 49.7 0.0098 305
02/20/19 13:00 26.5 1,526 6 71.0 38.1 0.0061 296
02/20/19 13:30 26.5 1,513 6 73.0 38.1 0.0066 292
02/20/19 14:00 26.5 1,429 6 72.9 36.8 0.0063 276
02/20/19 14:30 26.5 1,463 6 69.8 39.1 0.0060 285
02/20/19 15:00 26.5 1,703 6 69.0 41.6 0.0063 332
02/20/19 15:30 26.5 1,404 6 67.0 36.8 0.0052 275
Averages NA 26.4 1,428 6 66.63 37.4 0.0053 279.55
NOTES
Qstd = Flow at DSCFM
Vacuum = The level of vacuum being applied should be recorded from the vacuum truck tank (inches of Hg)
Velocity = The rate at which air flows is measured at the blower discharge piping (anemometer or pitot tube)
Pipe ID = The inside diameter of the blower discharge piping (from the vacuum truck)
Temperature = The temperature of the air stream exiting the blower discharge piping (dry bulb temp., in deg.°F)
Relative humidity = The % relative humidity of the air stream exiting the blower discharge piping
Water Vapor in % = Pounds of water per pound of dry air, derived from the Psychrometric chart
(temp Vs relative humidity)
EQUATION
Qstd = (1-Water Vapor) * velocity * (PI * (diameter/24)^2) * (528°R/(Temp + 460))
MW-7
Date Time
EMISSION CALCULATIONS
0 318 52.5 4 210.0 1,116.74 6.97183E-05 1.33 0.00
15 306 50.0 4 200.0 1,063.56 6.63983E-05 1.22 0.30
30 276 51.7 4 206.8 1,099.73 6.86559E-05 1.14 0.28
45 280 61.2 4 244.8 1,301.80 0.000081272 1.37 0.34
60 252 65.6 4 262.4 1,395.40 0.000087115 1.32 0.33
75 278 70.3 4 281.2 1,495.37 0.000093356 1.56 0.39
90 260 74.9 4 299.6 1,593.22 0.000099465 1.55 0.39
105 252 60.5 4 242.0 1,286.91 0.000080342 1.21 0.30
120 264 72.5 4 290.0 1,542.17 0.000096278 1.52 0.38
150 274 63.7 4 254.8 1,354.98 0.000084591 1.39 0.69
180 252 84.7 4 338.8 1,801.68 0.000112479 1.70 0.85
210 286 77.2 4 308.8 1,642.14 0.000102519 1.76 0.88
240 258 78.7 4 314.8 1,674.05 0.000104511 1.62 0.81
270 281 75.9 4 303.6 1,614.49 0.000100793 1.70 0.85
300 305 73.5 4 294.0 1,563.44 0.000097606 1.79 0.89
330 296 75.9 4 303.6 1,614.49 0.000100793 1.79 0.90
360 292 67.7 4 270.8 1,440.07 0.000089903 1.58 0.79
390 276 75.6 4 302.4 1,608.11 0.000100394 1.66 0.83
420 285 74.4 4 297.6 1,582.58 0.000098801 1.69 0.84
450 332 70.8 4 283.2 1,506.01 0.000094020 1.87 0.94
480 275 1.9 4 7.6 40.42 0.000002523 0.04 0.02
Averages 280.91 65.68 4.00 262.70 1,397.02 0.00 1.47 0.57
Total emissions in pounds 12.02
NOTES
PPM measured = Actual measurements (ppm) taken with a OVA or TVA at the blower discharge piping
K = Number of carbons in calibration gas: (Methane K = 1, or Propane K = 3, or Hexane K = 6)
PPMg = PPMv, Volumetric concentration as gasoline emission, dry basis at STP
Cg:m = mg/dsm3, mass concentration of gasoline emission
Mg = 128 mg/mg-mole, molecular weight of gasoline (this value may vary depending on contaminant)
K3 = 24.07 dsm^3/1E6 mg-mole, mass to volume conversion factor at STP
Cg = lb/dcsf, mass concentration of gasoline emission, dry basis at STP
PMRg = lb/hr, pollutant mass removal rate of gasoline emission
PMR = pollutant mass removal of gasoline emission over time
EQUATIONS
PPMg = PPM measured * K
Cg:m = PPMg * (Mg / K3)
Cg = Cg:m * 62.43E-09 lb-m^3/mg-ft^3
PMRg = Cg * Qstd * 60 min/hr
PMR = PMRg * ((T2 - T1) / 60)
K
(#C-gas)PPMg Cg:m
(mg/dsm^3)
Cg
(lb/dscf)
PMRg
(lb/hr)
Elapsed
Time
(min)
Flow
(DSCFM)
PMR
(lb)
PPM
measured
(ppm)

APPENDIX B
Disposal Manifest

APPENDIX C
Laboratory Reports – Ground Water Samples
02/27/19
Technical Report for
GRI (Geological Resources Inc.)
Ram 3; 1332 E Memorial Dr, Ahoskie, NC
10673/2677
SGS Job Number: FA61789
Sampling Date: 02/20/19
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
[e-mail]; [e-mail];
[e-mail]; [e-mail]
ATTN: William Regenthal
Total number of pages in report:
Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AK, AR, IA, KY, MA, MS, ND, NH, NV, OK, OR, UT, WA, WV
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone]
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Caitlin Brice, M.S.
General Manager
Orlando, FL 02/27/19
e-Hardcopy 2.0
Automated Report
13
SGS is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
Review standard terms at: http://www.sgs.com/en/terms-and-conditions
The results set forth herein are provided by SGS North America Inc.
Please share your ideas about
how we can serve you better at:
[e-mail]
1 of 13
FA61789
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................5
3.1: FA61789-1: MW-7 ........................................................................................................6
Section 4: Misc. Forms ............................................................................................................7
4.1: Chain of Custody ...........................................................................................................8
Section 5: MS Volatiles - QC Data Summaries .....................................................................10
5.1: Method Blank Summary ................................................................................................11
5.2: Blank Spike Summary ...................................................................................................12
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................13 123452 of 13
FA61789
SGS North America Inc.
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA61789
Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Project No: 10673/2677
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA61789-1 02/20/19 07:19 MS 02/22/19 AQ Ground Water MW-7
3 of 13
FA617891
Summary of Hits Page 1 of 1
Job Number:FA61789
Account:GRI (Geological Resources Inc.)
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Collected:02/20/19
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA61789-1 MW-7
Benzene 9700 250 63 ug/l SM 6200B
Di-Isopropyl Ether 195 J 250 63 ug/l SM 6200B
Ethylbenzene 2450 250 63 ug/l SM 6200B
Methyl Tert Butyl Ether 3300 250 63 ug/l SM 6200B
Naphthalene 836 250 63 ug/l SM 6200B
Toluene 23700 250 63 ug/l SM 6200B
Xylene (total)13100 750 130 ug/l SM 6200B
4 of 13
FA617892
SGS North America Inc.
Sample Results
Report of Analysis
Orlando, FL
Section 3
5 of 13
FA617893
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:MW-7
Lab Sample ID:FA61789-1 Date Sampled:02/20/19
Matrix:AQ - Ground Water Date Received:02/22/19
Method:SM 6200B Percent Solids:n/a
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0217176.D 500 02/26/19 13:17 AB n/a n/a VA2535
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
Purgeable Aromatics, Full List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 9700 250 63 ug/l
108-90-7 Chlorobenzene ND 250 63 ug/l
95-50-1 1,2-Dichlorobenzene ND 250 63 ug/l
541-73-1 1,3-Dichlorobenzene ND 250 63 ug/l
106-46-7 1,4-Dichlorobenzene ND 250 63 ug/l
108-20-3 Di-Isopropyl Ether 195 250 63 ug/l J
100-41-4 Ethylbenzene 2450 250 63 ug/l
1634-04-4 Methyl Tert Butyl Ether 3300 250 63 ug/l
91-20-3 Naphthalene 836 250 63 ug/l
108-88-3 Toluene 23700 250 63 ug/l
1330-20-7 Xylene (total)13100 750 130 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 92%70-130%
17060-07-0 1,2-Dichloroethane-D4 92%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
6 of 13
FA6178933.1
SGS North America Inc.
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Orlando, FL
Section 4
7 of 13
FA617894
FA61789: Chain of Custody
Page 1 of 2
8 of 13
FA6178944.1
Job Number:FA61789 Client:GRI
Date / Time Received:2/22/2019 9:30:00 AM Delivery Method:FED EX
Project:RAM #3
Airbill #'s:N/A
Cooler Information
1. Custody Seals Present
2. Custody Seals Intact
4. Cooler temp verification
3. Temp criteria achieved
5. Cooler media
IR Gun
Ice (Bag)
Trip Blank Information
1. Trip Blank present / cooler
2. Trip Blank listed on COC
2. Samples preserved properly
Sample Information
1. Sample labels present on bottles
5. Sample recvd within HT
4. Condition of sample
3. Sufficient volume/containers recvd for analysis:
Intact
Comments
SM001Rev. Date 05/24/17
SGS Sample Receipt Summary
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
Cooler 1: (2.1);
Cooler 1: (1.9);
3. Type Of TB Received
W or S N/A
6. Dates/Times/IDs on COC match Sample Label
7. VOCs have headspace
8. Bottles received for unspecified tests
9. Compositing instructions clear
10. Voa Soil Kits/Jars received past 48hrs?
11. % Solids Jar received?
Misc. Information
25-Gram 5-GramNumber of Encores:Number of 5035 Field Kits:Number of Lab Filtered Metals:
Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify)
Y or N N/A
Y or N
Therm ID:IR 1; Therm CF:-0.2; # of Coolers:1
Y or N N/A
12. Residual Chlorine Present?
Residual Chlorine Test Strip Lot #:
Technician:Reviewer:SHAYLAP Date:Date:2/22/2019 9:30:00 AM
FA61789: Chain of Custody
Page 2 of 2
9 of 13
FA6178944.1
SGS North America Inc.
MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 5
10 of 13
FA617895
Method Blank Summary Page 1 of 1
Job Number:FA61789
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2535-MB A0217167.D 1 02/26/19 AB n/a n/a VA2535
The QC reported here applies to the following samples:Method: SM 6200B
FA61789-1
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
11 of 13
FA6178955.1.1
Blank Spike Summary Page 1 of 1
Job Number:FA61789
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2535-BS A0217165.D 1 02/26/19 AB n/a n/a VA2535
The QC reported here applies to the following samples:Method: SM 6200B
FA61789-1
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 9.6 96 70-130
108-90-7 Chlorobenzene 10 9.6 96 70-130
95-50-1 1,2-Dichlorobenzene 10 9.5 95 70-130
541-73-1 1,3-Dichlorobenzene 10 9.9 99 70-130
106-46-7 1,4-Dichlorobenzene 10 9.4 94 70-130
108-20-3 Di-Isopropyl Ether 10 9.7 97 70-130
100-41-4 Ethylbenzene 10 9.9 99 70-130
1634-04-4 Methyl Tert Butyl Ether 10 9.9 99 70-130
91-20-3 Naphthalene 10 9.1 91 70-130
108-88-3 Toluene 10 9.7 97 70-130
1330-20-7 Xylene (total)30 30.0 100 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 97%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 97%70-130%
* = Outside of Control Limits.
12 of 13
FA6178955.2.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1
Job Number:FA61789
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA61777-2MS A0217177.D 5 02/26/19 AB n/a n/a VA2535
FA61777-2MSD A0217178.D 5 02/26/19 AB n/a n/a VA2535
FA61777-2 A0217170.D 1 02/26/19 AB n/a n/a VA2535
The QC reported here applies to the following samples:Method: SM 6200B
FA61789-1
FA61777-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 12.0 50 60.9 98 50 60.5 97 1 70-130/20
108-90-7 Chlorobenzene ND 50 50.6 101 50 50.2 100 1 70-130/20
95-50-1 1,2-Dichlorobenzene ND 50 50.0 100 50 50.0 100 0 70-130/20
541-73-1 1,3-Dichlorobenzene ND 50 52.4 105 50 52.4 105 0 70-130/20
106-46-7 1,4-Dichlorobenzene ND 50 49.7 99 50 49.8 100 0 70-130/20
108-20-3 Di-Isopropyl Ether 14.9 50 70.2 111 50 63.0 96 11 70-130/20
100-41-4 Ethylbenzene ND 50 52.2 104 50 52.3 105 0 70-130/20
1634-04-4 Methyl Tert Butyl Ether 47.9 50 99.3 103 50 92.7 90 7 70-130/20
91-20-3 Naphthalene 2.9 50 50.8 96 50 52.9 100 4 70-130/20
108-88-3 Toluene 0.25 J 50 51.6 103 50 50.8 101 2 70-130/20
1330-20-7 Xylene (total)0.80 J 150 159 105 150 159 105 0 70-130/20
CAS No.Surrogate Recoveries MS MSD FA61777-2 Limits
1868-53-7 Dibromofluoromethane 98%99%101%70-130%
17060-07-0 1,2-Dichloroethane-D4 92%92%100%70-130%
2037-26-5 Toluene-D8 100%99%98%70-130%
460-00-4 4-Bromofluorobenzene 97%97%99%70-130%
* = Outside of Control Limits.
13 of 13
FA6178955.3.1
04/03/19
Technical Report for
GRI (Geological Resources Inc.)
Ram 3; 1332 E Memorial Dr, Ahoskie, NC
10673/2677
SGS Job Number: FA62782
Sampling Date: 03/27/19
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
[e-mail]; [e-mail];
[e-mail]; [e-mail]
ATTN: William Regenthal
Total number of pages in report:
Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AK, AR, IA, KY, MA, MS, ND, NH, NV, OK, OR, UT, WA, WV
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone]
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Caitlin Brice, M.S.
General Manager
Orlando, FL 04/03/19
e-Hardcopy 2.0
Automated Report
28
SGS is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
Review standard terms at: http://www.sgs.com/en/terms-and-conditions
The results set forth herein are provided by SGS North America Inc.
Please share your ideas about
how we can serve you better at:
[e-mail]
1 of 28
FA62782
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................6
3.1: FA62782-1: MW-2 ........................................................................................................7
3.2: FA62782-2: MW-7 ........................................................................................................9
3.3: FA62782-3: MW-8 ........................................................................................................11
Section 4: Misc. Forms ............................................................................................................13
4.1: Chain of Custody ...........................................................................................................14
Section 5: MS Volatiles - QC Data Summaries .....................................................................16
5.1: Method Blank Summary ................................................................................................17
5.2: Blank Spike Summary ...................................................................................................21
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................25 123452 of 28
FA62782
SGS North America Inc.
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA62782
Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Project No: 10673/2677
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA62782-1 03/27/19 15:06 ER 03/28/19 AQ Ground Water MW-2
FA62782-2 03/27/19 15:20 ER 03/28/19 AQ Ground Water MW-7
FA62782-3 03/27/19 15:33 ER 03/28/19 AQ Ground Water MW-8
3 of 28
FA627821
Summary of Hits Page 1 of 2
Job Number:FA62782
Account:GRI (Geological Resources Inc.)
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Collected:03/27/19
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA62782-1 MW-2
Benzene 4440 50 13 ug/l SM 6200B
o-Chlorotoluene 13.0 J 50 13 ug/l SM 6200B
Di-Isopropyl Ether 42.3 J 50 13 ug/l SM 6200B
Ethylbenzene 573 50 13 ug/l SM 6200B
Isopropylbenzene 25.1 J 50 13 ug/l SM 6200B
Methylene Chloride a 128 JB 200 100 ug/l SM 6200B
Methyl Tert Butyl Ether 809 50 13 ug/l SM 6200B
Naphthalene 239 50 13 ug/l SM 6200B
n-Propylbenzene 49.3 J 50 13 ug/l SM 6200B
Toluene 3760 50 13 ug/l SM 6200B
1,2,4-Trimethylbenzene 305 50 13 ug/l SM 6200B
1,3,5-Trimethylbenzene 105 50 13 ug/l SM 6200B
m,p-Xylene 1640 100 13 ug/l SM 6200B
o-Xylene 323 50 13 ug/l SM 6200B
Xylene (total)1960 150 25 ug/l SM 6200B
FA62782-2 MW-7
Benzene 7990 250 63 ug/l SM 6200B
n-Butylbenzene 74.7 J 250 63 ug/l SM 6200B
o-Chlorotoluene 113 J 250 63 ug/l SM 6200B
1,2-Dichloroethane 142 J 250 63 ug/l SM 6200B
Di-Isopropyl Ether 131 J 250 63 ug/l SM 6200B
Ethylbenzene 2650 250 63 ug/l SM 6200B
Isopropylbenzene 133 J 250 63 ug/l SM 6200B
Methylene Chloride a 609 JB 1000 500 ug/l SM 6200B
Methyl Tert Butyl Ether 2060 250 63 ug/l SM 6200B
Naphthalene 681 250 63 ug/l SM 6200B
n-Propylbenzene 429 250 63 ug/l SM 6200B
Toluene 20500 250 63 ug/l SM 6200B
1,2,4-Trimethylbenzene 3290 250 63 ug/l SM 6200B
1,3,5-Trimethylbenzene 961 250 63 ug/l SM 6200B
m,p-Xylene 9390 500 63 ug/l SM 6200B
o-Xylene 4020 250 63 ug/l SM 6200B
Xylene (total)13400 750 130 ug/l SM 6200B
FA62782-3 MW-8
Benzene 127 5.0 1.3 ug/l SM 6200B
n-Butylbenzene 19.0 5.0 1.3 ug/l SM 6200B
sec-Butylbenzene 22.9 5.0 1.3 ug/l SM 6200B
o-Chlorotoluene 6.6 5.0 1.3 ug/l SM 6200B
1,2-Dichloroethane 3.5 J 5.0 1.3 ug/l SM 6200B
4 of 28
FA627822
Summary of Hits Page 2 of 2
Job Number:FA62782
Account:GRI (Geological Resources Inc.)
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Collected:03/27/19
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
Di-Isopropyl Ether 6.6 5.0 1.3 ug/l SM 6200B
Ethylbenzene 41.9 5.0 1.3 ug/l SM 6200B
Isopropylbenzene 22.3 5.0 1.3 ug/l SM 6200B
p-Isopropyltoluene 12.4 5.0 1.3 ug/l SM 6200B
Methylene Chloride a 12.8 J 20 10 ug/l SM 6200B
Methyl Tert Butyl Ether 22.5 5.0 1.3 ug/l SM 6200B
Naphthalene 254 5.0 1.3 ug/l SM 6200B
n-Propylbenzene 30.1 5.0 1.3 ug/l SM 6200B
Toluene 2.3 J 5.0 1.3 ug/l SM 6200B
1,2,4-Trimethylbenzene 219 5.0 1.3 ug/l SM 6200B
1,3,5-Trimethylbenzene 54.4 5.0 1.3 ug/l SM 6200B
m,p-Xylene 126 10 1.3 ug/l SM 6200B
o-Xylene 13.0 5.0 1.3 ug/l SM 6200B
Xylene (total)139 15 2.5 ug/l SM 6200B
(a) Suspected laboratory contaminant.
5 of 28
FA627822
SGS North America Inc.
Sample Results
Report of Analysis
Orlando, FL
Section 3
6 of 28
FA627823
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-2
Lab Sample ID:FA62782-1 Date Sampled:03/27/19
Matrix:AQ - Ground Water Date Received:03/28/19
Method:SM 6200B Percent Solids:n/a
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E098466.D 100 04/02/19 16:31 AB n/a n/a VE2096
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 4440 50 13 ug/l
108-86-1 Bromobenzene ND 50 13 ug/l
74-97-5 Bromochloromethane ND 50 13 ug/l
75-27-4 Bromodichloromethane ND 50 13 ug/l
75-25-2 Bromoform ND 50 13 ug/l
104-51-8 n-Butylbenzene ND 50 13 ug/l
135-98-8 sec-Butylbenzene ND 50 13 ug/l
98-06-6 tert-Butylbenzene ND 50 13 ug/l
56-23-5 Carbon Tetrachloride ND 50 13 ug/l
108-90-7 Chlorobenzene ND 50 13 ug/l
75-00-3 Chloroethane ND 50 20 ug/l
67-66-3 Chloroform ND 50 13 ug/l
95-49-8 o-Chlorotoluene 13.0 50 13 ug/l J
106-43-4 p-Chlorotoluene ND 50 13 ug/l
124-48-1 Dibromochloromethane ND 50 13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 50 25 ug/l
106-93-4 1,2-Dibromoethane ND 50 13 ug/l
75-71-8 Dichlorodifluoromethane ND 50 20 ug/l
95-50-1 1,2-Dichlorobenzene ND 50 13 ug/l
541-73-1 1,3-Dichlorobenzene ND 50 13 ug/l
106-46-7 1,4-Dichlorobenzene ND 50 13 ug/l
75-34-3 1,1-Dichloroethane ND 50 13 ug/l
107-06-2 1,2-Dichloroethane ND 50 13 ug/l
75-35-4 1,1-Dichloroethylene ND 50 13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 50 13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 50 13 ug/l
78-87-5 1,2-Dichloropropane ND 50 13 ug/l
142-28-9 1,3-Dichloropropane ND 50 13 ug/l
594-20-7 2,2-Dichloropropane ND 50 13 ug/l
563-58-6 1,1-Dichloropropene ND 50 13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 50 13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 50 13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
7 of 28
FA6278233.1
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-2
Lab Sample ID:FA62782-1 Date Sampled:03/27/19
Matrix:AQ - Ground Water Date Received:03/28/19
Method:SM 6200B Percent Solids:n/a
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 42.3 50 13 ug/l J
100-41-4 Ethylbenzene 573 50 13 ug/l
87-68-3 Hexachlorobutadiene ND 50 13 ug/l
98-82-8 Isopropylbenzene 25.1 50 13 ug/l J
99-87-6 p-Isopropyltoluene ND 50 13 ug/l
74-83-9 Methyl Bromide ND 50 20 ug/l
74-87-3 Methyl Chloride ND 50 20 ug/l
74-95-3 Methylene Bromide ND 50 13 ug/l
75-09-2 Methylene Chloride a 128 200 100 ug/l JB
1634-04-4 Methyl Tert Butyl Ether 809 50 13 ug/l
91-20-3 Naphthalene 239 50 13 ug/l
103-65-1 n-Propylbenzene 49.3 50 13 ug/l J
100-42-5 Styrene ND 50 13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 50 13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 50 13 ug/l
127-18-4 Tetrachloroethylene ND 50 13 ug/l
108-88-3 Toluene 3760 50 13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 50 13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 50 13 ug/l
71-55-6 1,1,1-Trichloroethane ND 50 13 ug/l
79-00-5 1,1,2-Trichloroethane ND 50 13 ug/l
79-01-6 Trichloroethylene ND 50 13 ug/l
75-69-4 Trichlorofluoromethane ND 50 20 ug/l
96-18-4 1,2,3-Trichloropropane ND 50 13 ug/l
95-63-6 1,2,4-Trimethylbenzene 305 50 13 ug/l
108-67-8 1,3,5-Trimethylbenzene 105 50 13 ug/l
75-01-4 Vinyl Chloride b ND 50 13 ug/l
m,p-Xylene 1640 100 13 ug/l
95-47-6 o-Xylene 323 50 13 ug/l
1330-20-7 Xylene (total)1960 150 25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
2037-26-5 Toluene-D8 95%70-130%
460-00-4 4-Bromofluorobenzene 97%70-130%
(a) Suspected laboratory contaminant.
(b) Associated BS recovery outside control limits.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
8 of 28
FA6278233.1
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-7
Lab Sample ID:FA62782-2 Date Sampled:03/27/19
Matrix:AQ - Ground Water Date Received:03/28/19
Method:SM 6200B Percent Solids:n/a
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E098467.D 500 04/02/19 16:56 AB n/a n/a VE2096
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 7990 250 63 ug/l
108-86-1 Bromobenzene ND 250 63 ug/l
74-97-5 Bromochloromethane ND 250 63 ug/l
75-27-4 Bromodichloromethane ND 250 63 ug/l
75-25-2 Bromoform ND 250 63 ug/l
104-51-8 n-Butylbenzene 74.7 250 63 ug/l J
135-98-8 sec-Butylbenzene ND 250 63 ug/l
98-06-6 tert-Butylbenzene ND 250 63 ug/l
56-23-5 Carbon Tetrachloride ND 250 63 ug/l
108-90-7 Chlorobenzene ND 250 63 ug/l
75-00-3 Chloroethane ND 250 100 ug/l
67-66-3 Chloroform ND 250 63 ug/l
95-49-8 o-Chlorotoluene 113 250 63 ug/l J
106-43-4 p-Chlorotoluene ND 250 63 ug/l
124-48-1 Dibromochloromethane ND 250 63 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 250 120 ug/l
106-93-4 1,2-Dibromoethane ND 250 63 ug/l
75-71-8 Dichlorodifluoromethane ND 250 100 ug/l
95-50-1 1,2-Dichlorobenzene ND 250 63 ug/l
541-73-1 1,3-Dichlorobenzene ND 250 63 ug/l
106-46-7 1,4-Dichlorobenzene ND 250 63 ug/l
75-34-3 1,1-Dichloroethane ND 250 63 ug/l
107-06-2 1,2-Dichloroethane 142 250 63 ug/l J
75-35-4 1,1-Dichloroethylene ND 250 63 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 250 63 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 250 63 ug/l
78-87-5 1,2-Dichloropropane ND 250 63 ug/l
142-28-9 1,3-Dichloropropane ND 250 63 ug/l
594-20-7 2,2-Dichloropropane ND 250 63 ug/l
563-58-6 1,1-Dichloropropene ND 250 63 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 250 63 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 250 63 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
9 of 28
FA6278233.2
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-7
Lab Sample ID:FA62782-2 Date Sampled:03/27/19
Matrix:AQ - Ground Water Date Received:03/28/19
Method:SM 6200B Percent Solids:n/a
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 131 250 63 ug/l J
100-41-4 Ethylbenzene 2650 250 63 ug/l
87-68-3 Hexachlorobutadiene ND 250 63 ug/l
98-82-8 Isopropylbenzene 133 250 63 ug/l J
99-87-6 p-Isopropyltoluene ND 250 63 ug/l
74-83-9 Methyl Bromide ND 250 100 ug/l
74-87-3 Methyl Chloride ND 250 100 ug/l
74-95-3 Methylene Bromide ND 250 63 ug/l
75-09-2 Methylene Chloride a 609 1000 500 ug/l JB
1634-04-4 Methyl Tert Butyl Ether 2060 250 63 ug/l
91-20-3 Naphthalene 681 250 63 ug/l
103-65-1 n-Propylbenzene 429 250 63 ug/l
100-42-5 Styrene ND 250 63 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 250 63 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 250 63 ug/l
127-18-4 Tetrachloroethylene ND 250 63 ug/l
108-88-3 Toluene 20500 250 63 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 250 63 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 250 63 ug/l
71-55-6 1,1,1-Trichloroethane ND 250 63 ug/l
79-00-5 1,1,2-Trichloroethane ND 250 63 ug/l
79-01-6 Trichloroethylene ND 250 63 ug/l
75-69-4 Trichlorofluoromethane ND 250 100 ug/l
96-18-4 1,2,3-Trichloropropane ND 250 63 ug/l
95-63-6 1,2,4-Trimethylbenzene 3290 250 63 ug/l
108-67-8 1,3,5-Trimethylbenzene 961 250 63 ug/l
75-01-4 Vinyl Chloride b ND 250 63 ug/l
m,p-Xylene 9390 500 63 ug/l
95-47-6 o-Xylene 4020 250 63 ug/l
1330-20-7 Xylene (total)13400 750 130 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
2037-26-5 Toluene-D8 95%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
(a) Suspected laboratory contaminant.
(b) Associated BS recovery outside control limits.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 28
FA6278233.2
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-8
Lab Sample ID:FA62782-3 Date Sampled:03/27/19
Matrix:AQ - Ground Water Date Received:03/28/19
Method:SM 6200B Percent Solids:n/a
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0217525.D 10 04/01/19 18:24 AB n/a n/a VA2549
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 127 5.0 1.3 ug/l
108-86-1 Bromobenzene ND 5.0 1.3 ug/l
74-97-5 Bromochloromethane ND 5.0 1.3 ug/l
75-27-4 Bromodichloromethane ND 5.0 1.3 ug/l
75-25-2 Bromoform ND 5.0 1.3 ug/l
104-51-8 n-Butylbenzene 19.0 5.0 1.3 ug/l
135-98-8 sec-Butylbenzene 22.9 5.0 1.3 ug/l
98-06-6 tert-Butylbenzene ND 5.0 1.3 ug/l
56-23-5 Carbon Tetrachloride ND 5.0 1.3 ug/l
108-90-7 Chlorobenzene ND 5.0 1.3 ug/l
75-00-3 Chloroethane ND 5.0 2.0 ug/l
67-66-3 Chloroform ND 5.0 1.3 ug/l
95-49-8 o-Chlorotoluene 6.6 5.0 1.3 ug/l
106-43-4 p-Chlorotoluene ND 5.0 1.3 ug/l
124-48-1 Dibromochloromethane ND 5.0 1.3 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 5.0 2.5 ug/l
106-93-4 1,2-Dibromoethane ND 5.0 1.3 ug/l
75-71-8 Dichlorodifluoromethane ND 5.0 2.0 ug/l
95-50-1 1,2-Dichlorobenzene ND 5.0 1.3 ug/l
541-73-1 1,3-Dichlorobenzene ND 5.0 1.3 ug/l
106-46-7 1,4-Dichlorobenzene ND 5.0 1.3 ug/l
75-34-3 1,1-Dichloroethane ND 5.0 1.3 ug/l
107-06-2 1,2-Dichloroethane 3.5 5.0 1.3 ug/l J
75-35-4 1,1-Dichloroethylene ND 5.0 1.3 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.3 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.3 ug/l
78-87-5 1,2-Dichloropropane ND 5.0 1.3 ug/l
142-28-9 1,3-Dichloropropane ND 5.0 1.3 ug/l
594-20-7 2,2-Dichloropropane ND 5.0 1.3 ug/l
563-58-6 1,1-Dichloropropene ND 5.0 1.3 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.3 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.3 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 28
FA6278233.3
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-8
Lab Sample ID:FA62782-3 Date Sampled:03/27/19
Matrix:AQ - Ground Water Date Received:03/28/19
Method:SM 6200B Percent Solids:n/a
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 6.6 5.0 1.3 ug/l
100-41-4 Ethylbenzene 41.9 5.0 1.3 ug/l
87-68-3 Hexachlorobutadiene ND 5.0 1.3 ug/l
98-82-8 Isopropylbenzene 22.3 5.0 1.3 ug/l
99-87-6 p-Isopropyltoluene 12.4 5.0 1.3 ug/l
74-83-9 Methyl Bromide ND 5.0 2.0 ug/l
74-87-3 Methyl Chloride ND 5.0 2.0 ug/l
74-95-3 Methylene Bromide ND 5.0 1.3 ug/l
75-09-2 Methylene Chloride a 12.8 20 10 ug/l J
1634-04-4 Methyl Tert Butyl Ether 22.5 5.0 1.3 ug/l
91-20-3 Naphthalene 254 5.0 1.3 ug/l
103-65-1 n-Propylbenzene 30.1 5.0 1.3 ug/l
100-42-5 Styrene ND 5.0 1.3 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 5.0 1.3 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 1.3 ug/l
127-18-4 Tetrachloroethylene ND 5.0 1.3 ug/l
108-88-3 Toluene 2.3 5.0 1.3 ug/l J
87-61-6 1,2,3-Trichlorobenzene ND 5.0 1.3 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.3 ug/l
71-55-6 1,1,1-Trichloroethane ND 5.0 1.3 ug/l
79-00-5 1,1,2-Trichloroethane ND 5.0 1.3 ug/l
79-01-6 Trichloroethylene ND 5.0 1.3 ug/l
75-69-4 Trichlorofluoromethane ND 5.0 2.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 5.0 1.3 ug/l
95-63-6 1,2,4-Trimethylbenzene 219 5.0 1.3 ug/l
108-67-8 1,3,5-Trimethylbenzene 54.4 5.0 1.3 ug/l
75-01-4 Vinyl Chloride ND 5.0 1.3 ug/l
m,p-Xylene 126 10 1.3 ug/l
95-47-6 o-Xylene 13.0 5.0 1.3 ug/l
1330-20-7 Xylene (total)139 15 2.5 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 104%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
(a) Suspected laboratory contaminant.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 28
FA6278233.3
SGS North America Inc.
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Orlando, FL
Section 4
13 of 28
FA627824
FA62782: Chain of Custody
Page 1 of 2
14 of 28
FA6278244.1
Job Number:FA62782 Client:GRI
Date / Time Received:3/28/2019 9:45:00 AM Delivery Method:FED EX
Project:2677
Airbill #'s:1015899924060003281100812565573201
Cooler Information
1. Custody Seals Present
2. Custody Seals Intact
4. Cooler temp verification
3. Temp criteria achieved
5. Cooler media
IR Gun
Ice (Bag)
Trip Blank Information
1. Trip Blank present / cooler
2. Trip Blank listed on COC
2. Samples preserved properly
Sample Information
1. Sample labels present on bottles
5. Sample recvd within HT
4. Condition of sample
3. Sufficient volume/containers recvd for analysis:
Intact
Comments
SM001Rev. Date 05/24/17
SGS Sample Receipt Summary
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
Cooler 1: (0.7);
Cooler 1: (1.1);
3. Type Of TB Received
W or S N/A
6. Dates/Times/IDs on COC match Sample Label
7. VOCs have headspace
8. Bottles received for unspecified tests
9. Compositing instructions clear
10. Voa Soil Kits/Jars received past 48hrs?
11. % Solids Jar received?
Misc. Information
25-Gram 5-GramNumber of Encores:Number of 5035 Field Kits:Number of Lab Filtered Metals:
Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify)
Y or N N/A
Y or N
Therm ID:IR 1; Therm CF:0.4; # of Coolers:1
Y or N N/A
12. Residual Chlorine Present?
Residual Chlorine Test Strip Lot #:
Technician:Reviewer:SHAYLAP Date:Date:3/28/2019 9:45:00 AM
FA62782: Chain of Custody
Page 2 of 2
15 of 28
FA6278244.1
SGS North America Inc.
MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 5
16 of 28
FA627825
Method Blank Summary Page 1 of 2
Job Number:FA62782
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2549-MB A0217505.D 1 04/01/19 AB n/a n/a VA2549
The QC reported here applies to the following samples:Method: SM 6200B
FA62782-3
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
17 of 28
FA6278255.1.1
Method Blank Summary Page 2 of 2
Job Number:FA62782
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2549-MB A0217505.D 1 04/01/19 AB n/a n/a VA2549
The QC reported here applies to the following samples:Method: SM 6200B
FA62782-3
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
18 of 28
FA6278255.1.1
Method Blank Summary Page 1 of 2
Job Number:FA62782
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2096-MB E098452.D 1 04/02/19 AB n/a n/a VE2096
The QC reported here applies to the following samples:Method: SM 6200B
FA62782-1, FA62782-2
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
19 of 28
FA6278255.1.2
Method Blank Summary Page 2 of 2
Job Number:FA62782
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2096-MB E098452.D 1 04/02/19 AB n/a n/a VE2096
The QC reported here applies to the following samples:Method: SM 6200B
FA62782-1, FA62782-2
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride 1.0 2.0 1.0 ug/l J
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 105%70-130%
17060-07-0 1,2-Dichloroethane-D4 113%70-130%
2037-26-5 Toluene-D8 95%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
20 of 28
FA6278255.1.2
Blank Spike Summary Page 1 of 2
Job Number:FA62782
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2549-BS A0217503.D 1 04/01/19 AB n/a n/a VA2549
The QC reported here applies to the following samples:Method: SM 6200B
FA62782-3
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 9.5 95 70-130
108-86-1 Bromobenzene 10 8.7 87 70-130
74-97-5 Bromochloromethane 10 8.7 87 70-130
75-27-4 Bromodichloromethane 10 8.9 89 70-130
75-25-2 Bromoform 10 8.4 84 70-130
104-51-8 n-Butylbenzene 10 8.9 89 70-130
135-98-8 sec-Butylbenzene 10 8.7 87 70-130
98-06-6 tert-Butylbenzene 10 8.3 83 70-130
56-23-5 Carbon Tetrachloride 10 10.1 101 70-130
108-90-7 Chlorobenzene 10 9.0 90 70-130
75-00-3 Chloroethane 10 9.6 96 60-140
67-66-3 Chloroform 10 9.4 94 70-130
95-49-8 o-Chlorotoluene 10 9.2 92 70-130
106-43-4 p-Chlorotoluene 10 8.9 89 70-130
124-48-1 Dibromochloromethane 10 8.8 88 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 8.3 83 70-130
106-93-4 1,2-Dibromoethane 10 8.3 83 70-130
75-71-8 Dichlorodifluoromethane 10 6.5 65 60-140
95-50-1 1,2-Dichlorobenzene 10 8.9 89 70-130
541-73-1 1,3-Dichlorobenzene 10 9.2 92 70-130
106-46-7 1,4-Dichlorobenzene 10 8.7 87 70-130
75-34-3 1,1-Dichloroethane 10 10.0 100 70-130
107-06-2 1,2-Dichloroethane 10 8.6 86 70-130
75-35-4 1,1-Dichloroethylene 10 10.2 102 70-130
156-59-2 cis-1,2-Dichloroethylene 10 9.6 96 70-130
156-60-5 trans-1,2-Dichloroethylene 10 10.1 101 70-130
78-87-5 1,2-Dichloropropane 10 9.3 93 70-130
142-28-9 1,3-Dichloropropane 10 8.0 80 70-130
594-20-7 2,2-Dichloropropane 10 10.3 103 70-130
563-58-6 1,1-Dichloropropene 10 10.1 101 70-130
10061-01-5 cis-1,3-Dichloropropene 10 7.9 79 70-130
10061-02-6 trans-1,3-Dichloropropene 10 8.0 80 70-130
108-20-3 Di-Isopropyl Ether 10 8.8 88 70-130
100-41-4 Ethylbenzene 10 9.1 91 70-130
87-68-3 Hexachlorobutadiene 10 9.4 94 70-130
98-82-8 Isopropylbenzene 10 9.1 91 70-130
* = Outside of Control Limits.
21 of 28
FA6278255.2.1
Blank Spike Summary Page 2 of 2
Job Number:FA62782
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2549-BS A0217503.D 1 04/01/19 AB n/a n/a VA2549
The QC reported here applies to the following samples:Method: SM 6200B
FA62782-3
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 8.8 88 70-130
74-83-9 Methyl Bromide 10 8.4 84 60-140
74-87-3 Methyl Chloride 10 9.6 96 60-140
74-95-3 Methylene Bromide 10 8.8 88 70-130
75-09-2 Methylene Chloride 10 9.8 98 70-130
1634-04-4 Methyl Tert Butyl Ether 10 8.8 88 70-130
91-20-3 Naphthalene 10 8.2 82 70-130
103-65-1 n-Propylbenzene 10 9.3 93 70-130
100-42-5 Styrene 10 8.2 82 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 9.1 91 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 8.6 86 70-130
127-18-4 Tetrachloroethylene 10 9.6 96 70-130
108-88-3 Toluene 10 9.0 90 70-130
87-61-6 1,2,3-Trichlorobenzene 10 8.9 89 70-130
120-82-1 1,2,4-Trichlorobenzene 10 9.0 90 70-130
71-55-6 1,1,1-Trichloroethane 10 9.7 97 70-130
79-00-5 1,1,2-Trichloroethane 10 8.7 87 70-130
79-01-6 Trichloroethylene 10 9.3 93 70-130
75-69-4 Trichlorofluoromethane 10 9.5 95 60-140
96-18-4 1,2,3-Trichloropropane 10 8.1 81 70-130
95-63-6 1,2,4-Trimethylbenzene 10 8.3 83 70-130
108-67-8 1,3,5-Trimethylbenzene 10 8.6 86 70-130
75-01-4 Vinyl Chloride 10 9.2 92 60-140
m,p-Xylene 20 18.6 93 70-130
95-47-6 o-Xylene 10 9.0 90 70-130
1330-20-7 Xylene (total)30 27.6 92 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 97%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
* = Outside of Control Limits.
22 of 28
FA6278255.2.1
Blank Spike Summary Page 1 of 2
Job Number:FA62782
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2096-BS E098450.D 1 04/02/19 AB n/a n/a VE2096
The QC reported here applies to the following samples:Method: SM 6200B
FA62782-1, FA62782-2
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 10.4 104 70-130
108-86-1 Bromobenzene 10 9.3 93 70-130
74-97-5 Bromochloromethane 10 9.5 95 70-130
75-27-4 Bromodichloromethane 10 11.4 114 70-130
75-25-2 Bromoform 10 9.9 99 70-130
104-51-8 n-Butylbenzene 10 10.7 107 70-130
135-98-8 sec-Butylbenzene 10 10.5 105 70-130
98-06-6 tert-Butylbenzene 10 10.4 104 70-130
56-23-5 Carbon Tetrachloride 10 12.9 129 70-130
108-90-7 Chlorobenzene 10 9.7 97 70-130
75-00-3 Chloroethane 10 10.1 101 60-140
67-66-3 Chloroform 10 10.9 109 70-130
95-49-8 o-Chlorotoluene 10 9.9 99 70-130
106-43-4 p-Chlorotoluene 10 9.8 98 70-130
124-48-1 Dibromochloromethane 10 10.0 100 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 9.5 95 70-130
106-93-4 1,2-Dibromoethane 10 9.5 95 70-130
75-71-8 Dichlorodifluoromethane 10 9.9 99 60-140
95-50-1 1,2-Dichlorobenzene 10 9.5 95 70-130
541-73-1 1,3-Dichlorobenzene 10 9.8 98 70-130
106-46-7 1,4-Dichlorobenzene 10 9.4 94 70-130
75-34-3 1,1-Dichloroethane 10 11.0 110 70-130
107-06-2 1,2-Dichloroethane 10 10.9 109 70-130
75-35-4 1,1-Dichloroethylene 10 11.0 110 70-130
156-59-2 cis-1,2-Dichloroethylene 10 10.3 103 70-130
156-60-5 trans-1,2-Dichloroethylene 10 10.7 107 70-130
78-87-5 1,2-Dichloropropane 10 10.1 101 70-130
142-28-9 1,3-Dichloropropane 10 9.3 93 70-130
594-20-7 2,2-Dichloropropane 10 12.6 126 70-130
563-58-6 1,1-Dichloropropene 10 11.5 115 70-130
10061-01-5 cis-1,3-Dichloropropene 10 9.9 99 70-130
10061-02-6 trans-1,3-Dichloropropene 10 10.2 102 70-130
108-20-3 Di-Isopropyl Ether 10 9.3 93 70-130
100-41-4 Ethylbenzene 10 10.4 104 70-130
87-68-3 Hexachlorobutadiene 10 9.8 98 70-130
98-82-8 Isopropylbenzene 10 11.2 112 70-130
* = Outside of Control Limits.
23 of 28
FA6278255.2.2
Blank Spike Summary Page 2 of 2
Job Number:FA62782
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2096-BS E098450.D 1 04/02/19 AB n/a n/a VE2096
The QC reported here applies to the following samples:Method: SM 6200B
FA62782-1, FA62782-2
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 10.7 107 70-130
74-83-9 Methyl Bromide 10 10.3 103 60-140
74-87-3 Methyl Chloride 10 13.3 133 60-140
74-95-3 Methylene Bromide 10 10.2 102 70-130
75-09-2 Methylene Chloride 10 10.4 104 70-130
1634-04-4 Methyl Tert Butyl Ether 10 10 100 70-130
91-20-3 Naphthalene 10 9.2 92 70-130
103-65-1 n-Propylbenzene 10 10 100 70-130
100-42-5 Styrene 10 10.2 102 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 11.0 110 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 9.6 96 70-130
127-18-4 Tetrachloroethylene 10 10.5 105 70-130
108-88-3 Toluene 10 9.7 97 70-130
87-61-6 1,2,3-Trichlorobenzene 10 9.2 92 70-130
120-82-1 1,2,4-Trichlorobenzene 10 9.2 92 70-130
71-55-6 1,1,1-Trichloroethane 10 12.0 120 70-130
79-00-5 1,1,2-Trichloroethane 10 9.6 96 70-130
79-01-6 Trichloroethylene 10 10.7 107 70-130
75-69-4 Trichlorofluoromethane 10 9.2 92 60-140
96-18-4 1,2,3-Trichloropropane 10 9.4 94 70-130
95-63-6 1,2,4-Trimethylbenzene 10 9.8 98 70-130
108-67-8 1,3,5-Trimethylbenzene 10 10.2 102 70-130
75-01-4 Vinyl Chloride 10 14.1 141*60-140
m,p-Xylene 20 20.8 104 70-130
95-47-6 o-Xylene 10 10.4 104 70-130
1330-20-7 Xylene (total)30 31.2 104 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 107%70-130%
17060-07-0 1,2-Dichloroethane-D4 114%70-130%
2037-26-5 Toluene-D8 96%70-130%
460-00-4 4-Bromofluorobenzene 97%70-130%
* = Outside of Control Limits.
24 of 28
FA6278255.2.2
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA62782
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA62787-1MS A0217516.D 5 04/01/19 AB n/a n/a VA2549
FA62787-1MSD A0217517.D 5 04/01/19 AB n/a n/a VA2549
FA62787-1 A0217506.D 1 04/01/19 AB n/a n/a VA2549
The QC reported here applies to the following samples:Method: SM 6200B
FA62782-3
FA62787-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 2.4 50 54.3 104 50 52.6 100 3 70-130/20
108-86-1 Bromobenzene ND 50 48.1 96 50 47.2 94 2 70-130/20
74-97-5 Bromochloromethane ND 50 48.2 96 50 47.4 95 2 70-130/20
75-27-4 Bromodichloromethane ND 50 46.0 92 50 44.7 89 3 70-130/20
75-25-2 Bromoform ND 50 38.5 77 50 37.0 74 4 70-130/20
104-51-8 n-Butylbenzene 0.25 J 50 49.5 99 50 48.6 97 2 70-130/20
135-98-8 sec-Butylbenzene 0.52 50 49.3 98 50 48.5 96 2 70-130/20
98-06-6 tert-Butylbenzene ND 50 45.9 92 50 45.7 91 0 70-130/20
56-23-5 Carbon Tetrachloride ND 50 51.6 103 50 49.7 99 4 70-130/20
108-90-7 Chlorobenzene ND 50 49.7 99 50 48.4 97 3 70-130/20
75-00-3 Chloroethane ND 50 45.7 91 50 53.3 107 15 60-140/20
67-66-3 Chloroform ND 50 50.1 100 50 48.6 97 3 70-130/20
95-49-8 o-Chlorotoluene ND 50 50.6 101 50 49.8 100 2 70-130/20
106-43-4 p-Chlorotoluene ND 50 49.6 99 50 49.0 98 1 70-130/20
124-48-1 Dibromochloromethane ND 50 43.5 87 50 42.6 85 2 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 50 43.6 87 50 44.4 89 2 70-130/20
106-93-4 1,2-Dibromoethane ND 50 46.2 92 50 45.4 91 2 70-130/20
75-71-8 Dichlorodifluoromethane ND 50 32.2 64 50 36.8 74 13 60-140/20
95-50-1 1,2-Dichlorobenzene ND 50 48.7 97 50 48.0 96 1 70-130/20
541-73-1 1,3-Dichlorobenzene ND 50 49.9 100 50 49.5 99 1 70-130/20
106-46-7 1,4-Dichlorobenzene ND 50 47.2 94 50 46.2 92 2 70-130/20
75-34-3 1,1-Dichloroethane ND 50 54.0 108 50 52.5 105 3 70-130/20
107-06-2 1,2-Dichloroethane ND 50 44.5 89 50 44.8 90 1 70-130/20
75-35-4 1,1-Dichloroethylene ND 50 55.2 110 50 53.0 106 4 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 50 52.8 106 50 51.2 102 3 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 50 54.4 109 50 52.6 105 3 70-130/20
78-87-5 1,2-Dichloropropane ND 50 50.4 101 50 48.8 98 3 70-130/20
142-28-9 1,3-Dichloropropane ND 50 44.3 89 50 44.1 88 0 70-130/20
594-20-7 2,2-Dichloropropane ND 50 53.2 106 50 51.0 102 4 70-130/20
563-58-6 1,1-Dichloropropene ND 50 54.5 109 50 53.3 107 2 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 50 38.4 77 50 37.2 74 3 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 50 40.5 81 50 39.7 79 2 70-130/20
108-20-3 Di-Isopropyl Ether ND 50 48.0 96 50 47.2 94 2 70-130/20
100-41-4 Ethylbenzene ND 50 50.9 102 50 49.1 98 4 70-130/20
87-68-3 Hexachlorobutadiene ND 50 52.4 105 50 51.5 103 2 70-130/20
98-82-8 Isopropylbenzene 0.42 J 50 52.3 104 50 50.6 100 3 70-130/20
* = Outside of Control Limits.
25 of 28
FA6278255.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA62782
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA62787-1MS A0217516.D 5 04/01/19 AB n/a n/a VA2549
FA62787-1MSD A0217517.D 5 04/01/19 AB n/a n/a VA2549
FA62787-1 A0217506.D 1 04/01/19 AB n/a n/a VA2549
The QC reported here applies to the following samples:Method: SM 6200B
FA62782-3
FA62787-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 50 49.6 99 50 48.7 97 2 70-130/20
74-83-9 Methyl Bromide ND 50 40.9 82 50 46.4 93 13 60-140/20
74-87-3 Methyl Chloride ND 50 46.8 94 50 52.7 105 12 60-140/20
74-95-3 Methylene Bromide ND 50 47.4 95 50 47.8 96 1 70-130/20
75-09-2 Methylene Chloride ND 50 53.3 107 50 51.5 103 3 70-130/20
1634-04-4 Methyl Tert Butyl Ether 3.3 50 50.5 94 50 48.6 91 4 70-130/20
91-20-3 Naphthalene ND 50 48.3 97 50 48.5 97 0 70-130/20
103-65-1 n-Propylbenzene 0.50 50 52.2 103 50 51.4 102 2 70-130/20
100-42-5 Styrene ND 50 45.8 92 50 44.0 88 4 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 50 49.6 99 50 47.8 96 4 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 50 48.3 97 50 47.4 95 2 70-130/20
127-18-4 Tetrachloroethylene ND 50 52.4 105 50 51.6 103 2 70-130/20
108-88-3 Toluene ND 50 50.6 101 50 49.4 99 2 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 50 49.3 99 50 50.2 100 2 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 50 51.7 103 50 51.6 103 0 70-130/20
71-55-6 1,1,1-Trichloroethane ND 50 50.3 101 50 49.2 98 2 70-130/20
79-00-5 1,1,2-Trichloroethane ND 50 49.3 99 50 49.3 99 0 70-130/20
79-01-6 Trichloroethylene ND 50 49.2 98 50 49.0 98 0 70-130/20
75-69-4 Trichlorofluoromethane ND 50 42.0 84 50 50.0 100 17 60-140/20
96-18-4 1,2,3-Trichloropropane ND 50 44.6 89 50 44.7 89 0 70-130/20
95-63-6 1,2,4-Trimethylbenzene ND 50 46.2 92 50 45.1 90 2 70-130/20
108-67-8 1,3,5-Trimethylbenzene ND 50 47.9 96 50 47.3 95 1 70-130/20
75-01-4 Vinyl Chloride ND 50 47.2 94 50 54.3 109 14 60-140/20
m,p-Xylene ND 100 103 103 100 100 100 3 70-130/20
95-47-6 o-Xylene ND 50 51.4 103 50 50.0 100 3 70-130/20
1330-20-7 Xylene (total)ND 150 154 103 150 150 100 3 70-130/20
CAS No.Surrogate Recoveries MS MSD FA62787-1 Limits
1868-53-7 Dibromofluoromethane 101%99%101%70-130%
17060-07-0 1,2-Dichloroethane-D4 91%93%102%70-130%
2037-26-5 Toluene-D8 99%99%96%70-130%
460-00-4 4-Bromofluorobenzene 97%99%103%70-130%
* = Outside of Control Limits.
26 of 28
FA6278255.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA62782
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA62787-5MS E098461.D 5 04/02/19 AB n/a n/a VE2096
FA62787-5MSD E098462.D 5 04/02/19 AB n/a n/a VE2096
FA62787-5 E098453.D 1 04/02/19 AB n/a n/a VE2096
The QC reported here applies to the following samples:Method: SM 6200B
FA62782-1, FA62782-2
FA62787-5 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 15.6 50 65.1 99 50 66.3 101 2 70-130/20
108-86-1 Bromobenzene ND 50 48.2 96 50 49.7 99 3 70-130/20
74-97-5 Bromochloromethane ND 50 48.7 97 50 49.9 100 2 70-130/20
75-27-4 Bromodichloromethane ND 50 48.8 98 50 49.2 98 1 70-130/20
75-25-2 Bromoform ND 50 29.5 59*50 29.8 60*1 70-130/20
104-51-8 n-Butylbenzene 3.6 50 57.2 107 50 58.1 109 2 70-130/20
135-98-8 sec-Butylbenzene 7.2 50 60.1 106 50 61.0 108 1 70-130/20
98-06-6 tert-Butylbenzene 1.8 50 54.0 104 50 54.8 106 1 70-130/20
56-23-5 Carbon Tetrachloride ND 50 58.9 118 50 59.0 118 0 70-130/20
108-90-7 Chlorobenzene ND 50 49.7 99 50 50.4 101 1 70-130/20
75-00-3 Chloroethane ND 50 63.6 127 50 63.3 127 0 60-140/20
67-66-3 Chloroform 0.92 50 53.1 104 50 53.3 105 0 70-130/20
95-49-8 o-Chlorotoluene ND 50 50.2 100 50 51.4 103 2 70-130/20
106-43-4 p-Chlorotoluene ND 50 50.2 100 50 50.8 102 1 70-130/20
124-48-1 Dibromochloromethane ND 50 37.5 75 50 37.7 75 1 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 50 44.4 89 50 50.7 101 13 70-130/20
106-93-4 1,2-Dibromoethane ND 50 48.2 96 50 49.8 100 3 70-130/20
75-71-8 Dichlorodifluoromethane ND 50 43.6 87 50 43.9 88 1 60-140/20
95-50-1 1,2-Dichlorobenzene ND 50 48.2 96 50 49.5 99 3 70-130/20
541-73-1 1,3-Dichlorobenzene ND 50 50.1 100 50 51.5 103 3 70-130/20
106-46-7 1,4-Dichlorobenzene ND 50 47.7 95 50 48.5 97 2 70-130/20
75-34-3 1,1-Dichloroethane ND 50 53.6 107 50 55.5 111 3 70-130/20
107-06-2 1,2-Dichloroethane ND 50 49.6 99 50 50.6 101 2 70-130/20
75-35-4 1,1-Dichloroethylene ND 50 51.9 104 50 52.3 105 1 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 50 52.2 104 50 54.3 109 4 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 50 51.5 103 50 52.4 105 2 70-130/20
78-87-5 1,2-Dichloropropane ND 50 50.9 102 50 52.8 106 4 70-130/20
142-28-9 1,3-Dichloropropane ND 50 46.6 93 50 48.0 96 3 70-130/20
594-20-7 2,2-Dichloropropane ND 50 57.5 115 50 57.3 115 0 70-130/20
563-58-6 1,1-Dichloropropene ND 50 57.3 115 50 57.9 116 1 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 50 45.3 91 50 43.2 86 5 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 50 46.4 93 50 44.5 89 4 70-130/20
108-20-3 Di-Isopropyl Ether 4.3 50 49.9 91 50 50.2 92 1 70-130/20
100-41-4 Ethylbenzene 0.30 J 50 52.9 105 50 53.5 106 1 70-130/20
87-68-3 Hexachlorobutadiene ND 50 49.8 100 50 51.9 104 4 70-130/20
98-82-8 Isopropylbenzene 16.5 50 70.6 108 50 71.3 110 1 70-130/20
* = Outside of Control Limits.
27 of 28
FA6278255.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA62782
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA62787-5MS E098461.D 5 04/02/19 AB n/a n/a VE2096
FA62787-5MSD E098462.D 5 04/02/19 AB n/a n/a VE2096
FA62787-5 E098453.D 1 04/02/19 AB n/a n/a VE2096
The QC reported here applies to the following samples:Method: SM 6200B
FA62782-1, FA62782-2
FA62787-5 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 50 54.3 109 50 56.2 112 3 70-130/20
74-83-9 Methyl Bromide ND 50 51.9 104 50 51.2 102 1 60-140/20
74-87-3 Methyl Chloride ND 50 52.8 106 50 46.8 94 12 60-140/20
74-95-3 Methylene Bromide ND 50 49.8 100 50 51.0 102 2 70-130/20
75-09-2 Methylene Chloride ND 50 51.5 103 50 51.7 103 0 70-130/20
1634-04-4 Methyl Tert Butyl Ether 32.4 50 74.9 85 50 75.2 86 0 70-130/20
91-20-3 Naphthalene 1.9 50 48.7 94 50 52.5 101 8 70-130/20
103-65-1 n-Propylbenzene 29.4 50 74.8 91 50 75.9 93 1 70-130/20
100-42-5 Styrene ND 50 50.0 100 50 50.2 100 0 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 50 55.9 112 50 55.7 111 0 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 50 48.3 97 50 50.6 101 5 70-130/20
127-18-4 Tetrachloroethylene ND 50 54.2 108 50 54.8 110 1 70-130/20
108-88-3 Toluene 1.3 50 51.3 100 50 51.9 101 1 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 50 45.5 91 50 48.0 96 5 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 50 48.0 96 50 50.2 100 4 70-130/20
71-55-6 1,1,1-Trichloroethane ND 50 56.3 113 50 57.3 115 2 70-130/20
79-00-5 1,1,2-Trichloroethane ND 50 47.0 94 50 49.8 100 6 70-130/20
79-01-6 Trichloroethylene ND 50 53.2 106 50 54.2 108 2 70-130/20
75-69-4 Trichlorofluoromethane ND 50 42.6 85 50 43.4 87 2 60-140/20
96-18-4 1,2,3-Trichloropropane ND 50 47.0 94 50 48.3 97 3 70-130/20
95-63-6 1,2,4-Trimethylbenzene 0.17 J 50 50.5 101 50 51.3 102 2 70-130/20
108-67-8 1,3,5-Trimethylbenzene ND 50 52.6 105 50 53.3 107 1 70-130/20
75-01-4 Vinyl Chloride ND 50 69.6 139 50 68.6 137 1 60-140/20
m,p-Xylene 0.31 J 100 106 106 100 106 106 0 70-130/20
95-47-6 o-Xylene 0.91 50 53.3 105 50 54.0 106 1 70-130/20
1330-20-7 Xylene (total)1.2 J 150 159 105 150 160 106 1 70-130/20
CAS No.Surrogate Recoveries MS MSD FA62787-5 Limits
1868-53-7 Dibromofluoromethane 103%102%105%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%105%117%70-130%
2037-26-5 Toluene-D8 96%96%95%70-130%
460-00-4 4-Bromofluorobenzene 98%98%101%70-130%
* = Outside of Control Limits.
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