WA-765_10673_CA_MRP_20161028

EXECUTIVE SUMMARY
The former Red Apple Market #3 site is located at 1332 East Memorial Drive in Ahoskie, Hertford County,
North Carolina. According to available information, two 12,000-gallon gasoline, one 8,000-gallon gasoline
and one 550-gallon kerosene underground storage tanks were removed from the site on June 3, 1993. Forty
monitoring wells have been installed on the site and adjacent properties during past ground water assessment
and corrective action activities. Free product had been previously measured in MW-7, MW-8 and MW-15.

On October 13, 2016, five monitoring wells were gauged, purged and sampled. Concentrations of requested
method constituents that exceeded the Maximum Allowable Concentrations specified in T15A NCAC 2L.0202
were reported in the ground water samples collected from MW-2, MW-7, MW-8 and MW-9. The
concentration of benzene reported in MW-7 exceeded the Gross Contamination Level (GCL).

On October 13, 2016, contaminant absorbent BioSocks were installed in MW-2, MW-7, and MW-8 following
the completion of the ground water sampling event.

Based on the October 2016 sampling results, GRI recommends that additional MMPE events should be
conducted on MW-7 in order to reduce contaminant concentrations at the site. Additionally, soil samples
should be collected in the vicinity of MW-7 in order to obtain current soil quality information for the site.
Semi-annual ground water monitoring should continue at the site until contaminant concentrations are reduced
to below the GCLs. The next semi-annual ground water monitoring event is tentatively scheduled for April
2017.

TABLE OF CONTENTS

1.0 SITE HISTORY AND CHARACTERIZATION .................................................................... 1
2.0 CURRENT SITE ASSESSMENT ............................................................................................ 1
3.0 GROUND WATER QUALITY ................................................................................................ 1
4.0 CONCLUSIONS AND RECOMMENDATIONS .................................................................... 2
5.0 LIMITATIONS ........................................................................................................................ 3

FIGURES
Figure 1: Site Location Map
Figure 2: Site Map
Figure 3: Water Table Surface Map
Figure 4: Ground Water Quality Map

TABLES
Table 1: Well Construction and Gauging Information
Table 2: Laboratory Analytical Results – Ground Water Samples

APPENDIX
Appendix A: Laboratory Report - Ground Water Samples

1

1.0 SITE HISTORY AND CHARACTERIZATION
According to available information, two 12,000-gallon gasoline, one 8,000-gallon gasoline and one 550-
gallon kerosene underground storage tanks (USTs) were removed from the site on June 3, 1993, by
Coastal Environmental Services (Coastal). Forty monitoring wells have been installed on the site and
adjacent properties during past ground water assessment and corrective action activities. The site is
currently ranked as Intermediate risk due to the presence of free product that was historically measured in
MW-7, MW-8 and MW-15. Mobile Multi-Phase Extraction (MMPE) events have been conducted at the
site in March 2011, July 2012 and July 2013. In addition, an Aggressive Fluid-Vapor Recovery (AFVR)
event was conducted in June 2014. The site is also located within the designated wellhead protection area
for the Town of Ahoskie.

Previous activities were conducted by Coastal and Northeast Environmental, P.C. (Northeast). Although
Geological Resources, Inc. (GRI) cannot verify the accuracy of information obtained from previous
reports, for the purposes of this report, it is assumed to be correct. Please refer to previous submittals for
further historical information regarding the site.

2.0 CURRENT SITE ASSESSMENT
This report presents the results of ground water assessment activities conducted on October 13, 2016 at
the former Red Apple Market #3 site located at 1332 East Memorial Drive in Ahoskie, Hertford County,
North Carolina (Figure 1). The activities were conducted in accordance with GRI proposal number 16-
119, which was submitted to NCDEQ on February 10, 2016, and approved as Task Authorization No.
10673-15 on March 17, 2016. The purpose of the activities was to install contaminant absorbent
BioSocks and to obtain current ground water quality data for the site.

3.0 GROUND WATER QUALITY
Five monitoring wells (MW-1A, MW-2, MW-7, MW-8, and MW-9) were gauged, purged and sampled
on October 13, 2016. Please note, MW-5, MW-13, and MW-15 were not found and therefore could not
be sampled. The depths to ground water in the Type II monitoring wells during the October 2016
sampling event ranged from 7.46 to 8.17 feet below the tops of well casings. Ground water elevations in
the Type II monitoring wells relative to a temporary benchmark with an assumed datum of 100.00 feet
ranged from 92.13 to 92.61 feet. Based on this information, ground water flow across the site was
generally toward the northeast. The horizontal hydraulic gradient across the site was less than 0.01 feet
per foot. A Site Map showing the locations of monitoring wells and structures onsite is included as

2

Figure 2. A Water Table Surface Map for the October 2016 sampling event has been included as Figure
3. Well construction and gauging information are presented in Table 1.

Laboratory analyses were performed on the ground water samples collected from the monitoring wells
during the October 2016 sampling event for volatile organic compounds using EPA Method 6200B.
Concentrations of one or more BTEX constituents, MTBE, naphthalene, n-butylbenzene, sec-
butylbenzene, EDB, 1,2-DCA, isopropylbenzene, IPE, n-propylbenzene, styrene, tetrachloroethene, 1,2,4-
trimethylbenzene and/or 1,3,5-trimethylbenzene that exceeded the Maximum Allowable Concentrations
(MACs) specified in T15A NCAC 2L.0202 were reported in the ground water samples collected from
MW-2, MW-7, MW-8 and MW-9. The concentration of benzene reported in MW-7 exceeded the Gross
Contamination Level (GCL). A Ground Water Quality Map based on data from the October 2016
sampling event has been included as Figure 4. A summary of ground water sample analytical results is
presented in Table 2. A complete laboratory report has been included in Appendix A.

Following the conclusion of the October 2016 sampling event, contaminant absorbent BioSocks were
installed in MW-2, MW-7 and MW-8.

4.0 CONCLUSIONS AND RECOMMENDATIONS
 The average depth to ground water in the monitoring wells during the October 2016 sampling
event was 7.72 feet. Ground water flow during the October 2016 sampling event was generally
toward the northeast with an average horizontal hydraulic gradient of less than 0.01 feet per foot.
 Concentrations of one or more BTEX constituents, MTBE, naphthalene, n-butylbenzene, sec-
butylbenzene, EDB, 1,2-DCA, isopropylbenzene, IPE, n-propylbenzene, styrene,
tetrachloroethene, 1,2,4-trimethylbenzene and/or 1,3,5-trimethylbenzene that exceeded the MACs
were reported in the ground water samples collected from MW-2, MW-7, MW-8 and MW-9.
 The concentration of benzene reported in MW-7 exceeded the GCL.
 Contaminant absorbent BioSocks were installed in MW-2, MW-7 and MW-8 upon completion of
the October 2016 sampling event.
 Based on the October 2016 sampling results, GRI recommends that additional MMPE events
should be conducted on MW-7 in order to reduce contaminant concentrations at the site.
Additionally, soil samples should be collected in the vicinity of MW-7 in order to obtain current
soil quality information for the site. Semi-annual ground water monitoring should continue at the
site until contaminant concentrations are reduced to below the GCLs. The next semi-annual
ground water monitoring event is tentatively scheduled for April 2017.

3

5.0 LIMITATIONS
This report has been prepared for the exclusive use of North East Oil Company, Inc. for specific
application to the referenced site in Hertford County, North Carolina. The assessment was conducted
based on the scope of work and level of effort desired by NCDEQ and with resources adequate only for
that scope of work. Our findings have been developed in accordance with generally accepted standards of
environmental practices in the State of North Carolina, available information, and our professional
judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would be
interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data. Please note that field data collected prior
to the May 2008 sampling and updated receptor survey event were not obtained under the supervision of
GRI. Although the accuracy of these data cannot be verified, for the purpose of this report GRI assumes
that they are correct.

FIGURES

TABLES
MW-1 Unknown 04/23/08 NA NA NA 99.29 9.43 0.00 89.86      
01/07/09 9.94 0.00 89.35
05/11/10 8.89 0.00 90.40
05/02/11 8.90 0.00 91.10
07/23/12 9.39 0.00 89.90 Before MMPE
07/27/12 9.49 0.00 89.80 After MMPE
08/28/12 9.10 0.00 90.90
08/19/13 9.42 0.00 90.58
07/08/14 9.13 0.00 90.87
03/24/15 8.02 0.00 91.98
01/11/16 8.25 0.00 91.75
10/13/16 7.87 0.00 92.13
04/23/08 9.85 0.00 90.25
10.28 0.00 89.82 Before AFVR
10.35 0.01 89.76 After AFVR
01/07/09 10.40 0.00 89.70
05/11/10 9.45 0.00 90.65
03/28/11 9.53 0.00 90.57 Before MMPE
04/01/11 9.50 0.00 90.60 After MMPE
05/02/11 9.38 0.00 91.03
07/23/12 9.89 0.00 90.52 Before MMPE
07/27/12 10.12 0.00 90.29 After MMPE
08/28/12 9.52 0.00 90.89
07/15/13 9.30 0.00 91.11 Before MMPE
07/19/13 9.90 0.00 90.51 After MMPE
08/19/13 NM NM NM
9.21 0.00 91.20 Before AFVR
9.73 0.00 90.68 After AFVR
07/08/14 9.69 0.00 90.72
03/24/15 8.01 0.00 92.40
12/07/15 9.30 0.00 91.11 Before MMPE
12/11/15 9.55 0.00 90.86 After MMPE
01/11/16 8.79 0.00 91.62
10/13/16 8.17 0.00 92.24
MW-3 Unknown 04/23/08 NA NA NA 99.93 10.03 0.00 89.90
01/07/09 10.55 0.00 89.38
05/11/10 9.59 0.00 90.34
05/02/11 9.52 0.00 91.03
07/23/12 10.24 0.00 90.31 Before MMPE
07/27/12 10.24 0.00 90.31 After MMPE
08/28/12 9.65 0.00 90.90
08/19/13 10.01 0.00 90.54
07/08/14 9.80 0.00 90.75
03/24/15 8.56 0.00 91.99
01/11/16 8.83 0.00 91.72
04/23/08 9.39 0.00 90.30
01/07/09 9.93 0.00 89.76
05/11/10 9.75 0.00 89.94
05/02/11 9.53 0.00 90.57
08/28/12 9.62 0.00 90.48
08/19/13 NM NM NM
04/23/08 NM NM NM Not Located
01/07/09 NM NM NM Not Located
05/02/11 NM NM NM Covered
08/28/12 NM NM NM Covered
08/19/13 NM NM NM No Access
07/08/14 NM NM NM Not Located
04/23/08 NM NM NM Not Located
01/07/09 9.52 0.00 89.59
05/11/10 8.68 0.00 90.43
05/02/11 8.61 0.00 90.77
08/28/12 8.64 0.00 90.74
08/19/13 9.26 0.00 90.12
07/08/14 8.92 0.00 90.46
03/24/15 7.64 0.00 91.74
01/11/16 7.80 0.00 91.58
8-18809/15/93
100.10
NM
MW-2
100.00
18.4NANAUnknownMW-1A
16
Date Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
25
6 6-16
Date: 10/18/16
20 20-25
99.11
01/07/94MW-6
Well ID Date Installed
(mm/dd/yy)
Top of Casing
Elevation*
(ft.)
Depth to
Water from
Top of
Casing
(ft.)
Screened
Interval
(x to y ft. 
BGS)
Bottom of
Well
(ft. BGS)
99.29
Free Product
Thickness
(ft.)
100.41
99.42
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET #3 (INCIDENT NO. 10673)
Facility ID # : 0-017539
Groundwater
Elevation
(ft.)
Comments
99.93
99.69
100.55
20NANAUnknown
100.10
18
08/13/08
99.38
166-166
MW-3A
06/05/14
MW-5 01/07/94
MWD-4 01/07/94
Page 1 of 5
Date Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Date: 10/18/16
Well ID Date Installed
(mm/dd/yy)
Top of Casing
Elevation*
(ft.)
Depth to
Water from
Top of
Casing
(ft.)
Screened
Interval
(x to y ft. 
BGS)
Bottom of
Well
(ft. BGS)
Free Product
Thickness
(ft.)
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET #3 (INCIDENT NO. 10673)
Facility ID # : 0-017539
Groundwater
Elevation
(ft.)
Comments
04/23/08 NM NM NM Not Located
10.30 0.00 89.17 Before AFVR
10.27 0.71 89.81 After AFVR
10.80 1.11 89.62 Before AFVR
10.53 0.01 88.95 After AFVR
01/07/09 10.25 0.45 89.61
04/05/10 8.10 0.31 91.64 Before MMPE
04/09/10 8.80 0.00 90.67 After MMPE
05/11/10 8.90 0.00 90.57
03/28/11 9.02 0.02 90.47 Before MMPE
04/01/11 9.09 0.00 90.38 After MMPE
05/02/11 8.85 0.00 91.12
07/23/12 9.34 0.00 90.63 Before MMPE
07/27/12 9.57 0.00 90.40 After MMPE
08/28/12 8.97 0.00 91.00
07/15/13 8.77 0.00 91.20 Before MMPE
07/19/13 9.17 0.00 90.80 After MMPE
08/19/13 9.43 0.00 90.54
8.73 0.07 91.30 Before AFVR
9.12 0.00 90.85 After AFVR
07/08/14 9.11 0.00 90.86
03/24/15 6.88 0.00 93.09
12/07/15 8.79 0.00 91.18 Before MMPE
12/11/15 9.12 0.00 90.85 After MMPE
01/11/16 8.13 0.00 91.84
10/13/16 7.61 0.00 92.36
04/23/08 10.64 1.71 89.97
11.10 1.80 89.58 Before AFVR
9.71 0.30 89.69 After AFVR
11.40 1.82 89.30 Before AFVR
9.99 0.00 89.15 After AFVR
01/07/09 10.50 0.90 89.41
04/05/10 7.71 0.00 91.43 Before MMPE
04/09/10 8.60 0.00 90.54 After MMPE
05/11/10 8.80 0.00 90.34
03/28/11 9.05 0.21 90.27 Before MMPE
04/01/11 9.92 0.00 89.22 After MMPE
05/02/11 8.78 0.03 91.05
07/23/12 9.29 0.06 90.56 Before MMPE
07/27/12 9.43 0.00 90.37 After MMPE
08/28/12 8.80 0.00 91.00
08/19/13 9.33 0.00 90.47
07/08/14 9.05 0.00 90.75
03/24/15 7.79 0.00 92.01
10/13/16 7.47 0.00 92.33
04/23/08 NM NM NM Not Located
01/07/09 NM NM NM Not Located
05/11/10 NM NM NM Under Junk Cars
05/02/11 NM NM NM Under Junk Cars
07/23/12 9.29 0.00 90.78 Before MMPE
07/27/12 9.39 0.00 90.68 After MMPE
08/28/12 8.77 0.00 91.30
08/19/13 9.41 0.00 90.66
07/08/14 9.09 0.00 90.98
03/24/15 7.76 0.00 92.31
01/11/16 8.00 0.00 92.07
10/13/16 7.46 0.00 92.61
04/23/08 7.04 0.00 90.58
01/07/09 7.70 0.00 89.92
05/11/10 7.18 0.00 90.44
05/02/11 7.04 0.00 90.43
08/28/12 6.95 0.00 90.52
08/19/13 7.71 0.00 89.76
07/08/14 7.43 0.00 90.04
03/24/15 6.08 0.00 91.39
04/23/08 8.69 0.00 90.26
01/07/09 9.42 0.00 89.53
05/11/10 8.71 0.00 90.24
05/02/11 8.57 0.00 90.73
08/28/12 8.46 0.00 90.84
08/19/13 9.23 0.00 90.07
07/08/14 8.96 0.00 90.34
03/24/15 7.57 0.00 91.73
04/23/08 8.25 0.00 90.39      
01/07/09 8.95 0.00 89.69
05/11/10 8.12 0.00 90.52
05/02/11 8.05 0.00 90.47
08/28/12 8.05 0.00 90.47
08/19/13 8.64 0.00 89.88
07/08/14 8.40 0.00 90.12
03/24/15 7.13 0.00 91.39
01/10/94MW-9
166-16601/10/94MW-7
166
01/10/94
06/05/14
6-16
16
99.47
98.95
99.15
99.30
100.07
MW-12
6 6-16
MW-10
MW-8
99.80
166-166
6-16
98.52
98.64
NA NA
97.47
16
97.62
Unknown NA
MW-11 11/25/94
11/25/94 6
99.14
08/13/08
12/29/08
12/29/08
08/13/08
99.97
Page 2 of 5
Date Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Date: 10/18/16
Well ID Date Installed
(mm/dd/yy)
Top of Casing
Elevation*
(ft.)
Depth to
Water from
Top of
Casing
(ft.)
Screened
Interval
(x to y ft. 
BGS)
Bottom of
Well
(ft. BGS)
Free Product
Thickness
(ft.)
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET #3 (INCIDENT NO. 10673)
Facility ID # : 0-017539
Groundwater
Elevation
(ft.)
Comments
04/23/08 NM NM NM Not Located
01/07/09 9.45 0.00 89.37
05/11/10 8.27 0.00 90.55
05/02/11 8.50 0.00 90.99
03/28/11 8.61 0.00 90.88 Before MMPE
04/01/11 8.72 0.00 90.77 After MMPE
08/28/12 8.51 0.00 90.98
08/19/13 9.12 0.00 90.37
07/08/14 8.81 0.00 90.68
03/24/15 NM NM NM Not Located
04/23/08 9.11 0.00 90.07      
01/07/09 9.73 0.00 89.45
05/11/10 8.69 0.00 90.49
05/02/11 8.66 0.00 91.19
08/28/12 8.77 0.00 91.08
08/19/13 9.29 0.00 90.56
07/08/14 8.96 0.00 90.89
03/24/15 7.67 0.00 92.18
01/11/16 7.94 0.00 91.91
04/23/08 9.06 0.00 89.98      
01/07/09 9.76 0.03 89.31
05/11/10 9.07 0.00 89.97
05/02/11 8.94 0.00 90.82
08/28/12 8.80 0.00 90.96
08/19/13 9.67 0.00 90.09
07/08/14 NM NM NM Behind Locked Fence
03/24/15 NM NM NM Behind Locked Fence
MW-16 Unknown 04/23/08 NA NA NA 97.03 6.26 0.00 90.77      
01/07/09 6.78 0.00 90.25
05/12/10 6.91 0.00 90.12
05/02/11 6.68 0.00 90.26
08/28/12 6.25 0.00 90.69
08/19/13 7.42 0.00 89.52
07/08/14 NM NM NM Not Located
03/24/15 NM NM NM Not Located
04/23/08 9.18 0.00 90.05      
01/07/09 9.79 0.00 89.44
05/11/10 8.54 0.00 90.69
05/02/11 8.59 0.00 91.39
08/28/12 8.76 0.00 91.22
08/19/13 9.16 0.00 90.82
07/08/14 8.68 0.00 91.30
03/24/15 7.59 0.00 92.39
01/11/16 7.89 0.00 92.09
04/23/08 7.25 0.00 89.47      
01/07/09 7.80 0.00 88.92
05/02/11 6.79 0.00 90.66
08/28/12 7.00 0.00 90.45
08/19/13 7.23 0.00 90.22
07/08/14 7.00 0.00 90.45
03/24/15 6.09 0.00 91.36
04/23/08 7.76 0.00 89.29
01/07/09 8.38 0.00 88.67
05/12/10 7.56 0.00 89.49
05/02/11 7.49 0.00 90.31
08/28/12 7.66 0.00 90.14
08/19/13 8.02 0.00 89.78
07/08/14 7.77 0.00 90.03
03/24/15 6.91 0.00 90.89
04/23/08 9.29 0.00 90.13
01/07/09 9.92 0.00 89.50
05/11/10 8.65 0.00 90.77
05/02/11 8.74 0.00 91.38
08/28/12 8.95 0.00 91.17
08/19/13 9.29 0.00 90.83
07/08/14 8.96 0.00 91.16
03/24/15 7.79 0.00 92.33
04/23/08 9.29 0.00 90.12
01/07/09 9.98 0.00 89.43
05/02/11 8.77 0.00 91.34
08/28/12 8.93 0.00 91.18
08/19/13 9.34 0.00 90.77
07/08/14 8.88 0.00 91.23
03/24/15 7.74 0.00 92.37
04/23/08 8.39 0.00 89.85
01/07/09 8.94 0.00 89.30
05/12/10 8.24 0.00 90.00
05/02/11 8.15 0.00 89.97
08/28/12 8.25 0.00 89.87
08/19/13 8.65 0.00 89.47
07/08/14 8.41 0.00 89.71
03/24/15 7.53 0.00 90.59
96.94
20NA
MW-19
6 6-16
99.04
98.82
99.18
6
99.98
97.03
99.23
99.76
1605/15/96
16
97.45
97.80
NA
6
11/25/94MW-13 6 6-16
99.85
16
99.49
11/25/94
MW-17
6MW-14
6-16
100.12
MW-18 05/17/96
05/17/96 6-16 16
16MW-20 05/18/96
7-17 17
MW-21 05/18/96 6 6-16 16
MW-22
98.12
08/07/00 7
166-16
166-16
96.72
100.11
97.05
99.41
99.42
98.24
6-16
MW-16A
605/17/96
6MW-15
Unknown
Page 3 of 5
Date Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Date: 10/18/16
Well ID Date Installed
(mm/dd/yy)
Top of Casing
Elevation*
(ft.)
Depth to
Water from
Top of
Casing
(ft.)
Screened
Interval
(x to y ft. 
BGS)
Bottom of
Well
(ft. BGS)
Free Product
Thickness
(ft.)
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET #3 (INCIDENT NO. 10673)
Facility ID # : 0-017539
Groundwater
Elevation
(ft.)
Comments
04/23/08 7.11 0.00 89.87
01/07/09 7.62 0.00 89.36
05/12/10 6.85 0.00 90.13
05/02/11 6.79 0.00 90.09
08/28/12 6.94 0.00 89.94
08/19/13 NM NM NM
04/23/08 NM NM NM Not Located
01/07/09 4.72 0.00 90.78
05/12/10 NM NM NM Not Located
05/02/11 5.12 0.00 90.25
08/28/12 4.32 0.00 91.05
08/19/13 5.83 0.00 89.54
07/08/14 5.64 0.00 89.73
03/24/15 NM NM NM Not Located
04/23/08 1.70 0.00 93.66
01/07/09 2.39 0.00 92.97
05/02/11 4.32 0.00 90.89
08/28/12 NM NM NM Not Located
08/19/13 6.14 0.00 89.07
07/08/14 4.89 0.00 90.32
03/24/15 2.30 0.00 92.91
04/23/08 8.71 0.00 90.81
01/07/09 9.50 0.00 90.02
05/02/11 8.92 0.00 90.47
08/28/12 8.53 0.00 90.86
08/19/13 9.64 0.00 89.75
07/08/14 9.39 0.00 90.00
03/24/15 NM NM NM Not Located
04/23/08 NM NM NM Not Located
01/07/09 7.55 0.00 90.21
05/02/11 7.40 0.00 90.23
08/28/12 6.74 0.00 90.89
08/19/13 NM NM NM
04/23/08 9.53 0.00 89.48
01/07/09 10.00 0.00 89.01
05/02/11 9.30 0.00 89.60
08/28/12 9.42 0.00 89.48
08/19/13 NM NM NM
03/24/15 8.88 0.00 90.02
04/23/08 NM NM NM Not Located
01/07/09 11.58 0.00 88.43
05/12/10 12.01 0.00 88.00
05/02/11 11.53 0.00 88.40
08/28/12 10.97 0.00 88.96
08/19/13 12.49 0.00 87.44
07/08/14 12.14 0.00 87.79
03/24/15 10.56 0.00 89.37
04/23/08 NM NM NM Not Located
01/07/09 NM NM NM Not Located
05/12/10 NM NM NM Not Located
05/02/11 NM NM NM Destroyed
08/28/12 NM NM NM Destroyed
04/23/08 NM NM NM Not Located
01/07/09 6.63 0.00 90.14
05/12/10 6.47 0.00 90.30
05/02/11 6.35 0.00 90.27
08/28/12 NM NM NM Not Located
08/19/13 NM NM NM
03/24/15 5.24 0.00 91.38
04/23/08 10.15 0.00 90.15
01/07/09 10.72 0.00 89.58
05/12/10 9.37 0.00 90.93
05/02/11 9.49 0.00 91.55
08/28/12 9.70 0.00 91.34
08/19/13 NM NM NM
03/24/15 NM NM NM Not Located
04/23/08 NM NM NM Not Located
01/07/09 4.42 0.00 NA
05/12/10 5.66 0.00 NA
05/02/11 4.90 0.00 87.52
08/28/12 3.38 0.00 89.04
08/19/13 5.85 0.00 86.57
07/08/14 5.70 0.00 86.72
03/24/15 3.60 0.00 88.82
05/12/10 96.60 9.29 0.00 87.31
05/02/11 8.70 0.00 87.76
08/28/12 7.90 0.00 88.56
08/19/13 9.68 0.00 86.78
07/08/14 9.38 0.00 87.08
03/24/15 7.66 0.00 88.80
MW-32
98.90
96.88
95.50
101.04
18NANA
MW-23
MW-25 08/07/00 5 5-15
08/07/00 7 7-17
5MW-24 08/07/00
MW-26 08/08/00 5 15
5-15
10-20.5 20.00
99.39
99.52
5-15
15
95.21
MW-27 05/02/01 5 5-15 15
MW-29 05/01/01
MW-28 05/01/01 10
15
MW-30 05/01/01
NA
MW-34
MW-33
MW-31
15-25
05/02/01 5 5-15 15
96.62
96.98
95.36
97.76
100.01
99.01
95.37
93.19
15
25
97.63
NA
92.42
17
15
Unknown NA NA
99.93
5 5-20 96.4620
100.30
5 5-15
NM
Unknown
96.77
03/11/10
Page 4 of 5
Date Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Date: 10/18/16
Well ID Date Installed
(mm/dd/yy)
Top of Casing
Elevation*
(ft.)
Depth to
Water from
Top of
Casing
(ft.)
Screened
Interval
(x to y ft. 
BGS)
Bottom of
Well
(ft. BGS)
Free Product
Thickness
(ft.)
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET #3 (INCIDENT NO. 10673)
Facility ID # : 0-017539
Groundwater
Elevation
(ft.)
Comments
05/12/10 99.13 8.73 0.00 90.40
05/02/11 8.60 0.00 90.48
08/28/12 8.27 0.00 90.81
08/19/13 NM NM NM
05/12/10 100.56 9.33 0.00 91.23
05/02/11 9.35 0.00 91.04
08/28/12 9.54 0.00 90.85
08/19/13 NM NM NM
05/02/11 7.96 0.00 86.01
08/28/12 6.07 0.00 87.90
08/19/13 NM NM NM
03/24/15 5.80 0.00 88.17
05/02/11 6.31 0.00 87.00
08/28/12 5.34 0.00 87.97
08/19/13 NM NM NM
03/24/15 5.22 0.00 88.09
05/02/11 8.18 0.00 89.09
08/28/12 6.90 0.00 90.37
08/19/13 NM NM NM
03/24/15 7.40 0.00 89.87
05/02/11 8.69 0.00 91.21
08/28/12 8.78 0.00 91.12
08/19/13 9.27 0.00 90.63
07/08/14 8.88 0.00 91.02
03/24/15 7.63 0.00 92.27
Notes:
•  * : Reference point for elevation measurements, Assumed elevation 100.00 ft.
•  If free product is present in a well, groundwater elevation should be calculated by: [Top of Casing Elevation - Depth to Water] + [free product thickness 
   x 0.8581].
•  ft BGS : feet below ground surface.
•  NA: Not available.
•  NM: Not measured; well could not be located or was inaccessible.
5-15505/02/11MW-38
15 93.97
97.2715
93.3115
5-15 15 99.90
5
•  Top of casing elevations were surveyed by Coastal Engineering & Surveying, Inc. in May 2011.
MW-40 05/02/11 5
166-16
03/11/10 6
03/11/10
100.39
05/02/11 5
99.08
MW-37 5-15
MW-36 16
6
MW-39 05/02/11 5-15
6-16
MW-35
Page 5 of 5
EPAMethod6010BWell IDDate Collected (mm/dd/yy)1 600 600 500 20 6 0.6 70 70 0.4 70 70 70 0.7 400 400 15 400 700 200 700 10,000 2005,000 260,000 84,500 85,500 20,000 6,000 NE 6,900 8,500 400 25,000 70,000 30,000 700 28,500 25,000 15,000 NE NE NE NE NE NEMW-1 04/23/08 <0.31 0.620 I 1.14 4.63 <0.1217.3<0.14 1.16 0.900 I <0.12 0.380 I <0.15 1.02 <0.33 10.2 2.2333.5<100 <100 1943,0201,1102,76001/09/09 0.65 J <0.70 0.60 J 1.9 J 1.7 J 2.3 JB <0.90 12 B <0.70 <1.1 <0.55 <1.0 <0.75 <0.80 1.1 J <0.5027.5<100 <100 <100 <105 <105 <10505/12/10 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.50039.9<100 <100 <100 <97.1 <97.1 <97.105/02/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR08/19/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.1030.0<35 <35 <35 <110 <110 <16007/09/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 58.3 <35 <35 <35 <100 <100 <150 03/24/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.15 <0.14 <0.14 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NR01/11/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR10/13/16 <0.13 0.39 J <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR04/23/081,100446 203599 427 186<1.4 <3.9 <4.77.90 I18.6 15.4 I 27.9 <3.3 248 70.416.3 4,120<1001,680133 <75 17001/09/0941028 31 80110 95 B<1.8 <1.7 2.5 J3.2 J9.8 J 14 J 6.6 J <1.6 21 6.4 J 14.81,820241247<100 <100 12405/12/104,030 2,610 1,040 2,820 785 478<0.500 34.2 8.27 <0.500 59.3 59.6121<0.50075330415.6 17,300 2,550 2,680<100 <10023005/02/116,0709,230 1,370 4,839 1,260 256<29 <25 <2647.6 J34.6 J 55.5 J118 J<34848256 NR NR NR NR NR NR NR08/28/126,6309,660 1,450 5,110 1,320 400<23 <20 <20 <33 41.4 J 62.1 J128<27932275 NR NR NR NR NR NR NR08/19/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS07/09/143,030 2,060 1,160 2,500 759 372 <10 <10 <10 <10 44.5 J 39.7 J138 <10 685 232 <5.0 6,620<3502,630 1,550<400 <600 03/24/151,730 1,260155791 734 131<1.5 2.1 J <1.4 4.0 J11.6 33.5 24.9 <1.5 194 67.2 NR NR NR NR NR NR NR01/11/162,480 2,220 261 1,530 887 117 <13 <13 <13 16.4 J13.9 J 39.9 J 32.9 J <13 288 86.7 NR NR NR NR NR NR NR10/13/162,400 921 198 1,260 781 154 <6.3 <6.3 <6.3 7.1 J13.2 J 31.8 30.5 <6.3 264 76.2 NR NR NR NR NR NR NRMW-3 04/23/08 <0.31 <0.28 <0.31 1.39 I 5.30 <0.411.13<0.39 <0.47 <0.12 <0.24 1.45 I <0.30 <0.33 0.860 I 0.290 I48.0<100 <100 <100 <75 <75 77.001/09/092.2 J<0.70 <0.50 <1.0 1.8 J 3.8 JB <0.90 <0.85 <0.70 <1.1 <0.55 2.7 J <0.75 <0.80 <0.70 <0.5021.1<100 <100 <100 <105 <105 <10505/12/101.66<0.500 <0.500 <1.00 4.10 <5.00 <0.500 <0.500 <0.5000.910<0.500 5.11 <0.500 <0.500 <0.500 <0.50034.9<100 <100 <100 <99.0 <99.0 <99.005/02/113.6<0.13 <0.15 <0.30 3.4 0.17 J <0.12 <0.10 0.19 J1.4<0.10 7.3 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR08/28/1211.50.28 J <0.15 1.2 J 1.8 0.37 J <0.12 <0.10 0.44 J0.870.50 3.6 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR08/19/1360.02.3 6.0 2.9 5.8 3.0 <0.10 0.27 J 1.61.43.8 8.3 1.9 <0.10 0.19 J 0.21 J 7.8 220 148 149 128 J <100 <16007/09/14 0.85 <0.10 <0.10 <0.20 3.3 0.17 J <0.10 <0.10 0.38 J0.63 0.13 J 3.5 <0.10 <0.10 <0.10 <0.10 10.8 60.8 J <35 <35 <100 <100 213 03/24/152.6<0.17 <0.15 <0.43 0.41 J 0.15 J0.81<0.14 <0.14 <0.16 <0.12 0.34 J <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NR01/11/164.1 <0.13 <0.13 <0.31 1.4 0.18 J1.3 <0.13 <0.13 0.29 J <0.13 0.87 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR04/23/08 <0.31 <0.28 <0.31 <1.2 0.650 I <0.410.810<0.39 <0.47 <0.12 <0.24 <0.15 <0.30 <0.33 <0.26 <0.27 6.06 <100 <100 <100 <75 76.6 77.301/09/09 <0.60 <0.70 <0.50 <1.0 <0.50 1.1 JB0.93 J12 B <0.70 <1.1 <0.55 <1.0 <0.75 <0.80 <0.70 <0.50 <1.5 <100 <100 <100 <100 <100 <10005/12/10 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 10.8 <100 <100 <100 <99.0 <99.0 <99.005/02/11 <0.13 <0.13 <0.15 <0.30 0.39 J <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR08/28/12 <0.13 <0.13 <0.15 <0.30 0.51 <0.103.7<0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR08/19/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NSMW-5 04/23/08 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS04/23/08 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NSContaminant of Concern LeadNaphthaleneIPETolueneEthylbenzeneXylenesTetrachloroethenen-PropylbenzeneMTBEC9-C18 AliphaticsC9-C12 Aliphatics1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneC5-C8 AliphaticsC11-C22 AromaticsC19-C36 AliphaticsC9-C10 AromaticsTABLE 2 SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS RED APPLE MARKET #3 (INCIDENT NO. 10673)Analytical MethodDate: 10/27/16Facility ID #: 0-017539EPA Method 6200BMADEP Methods VPH and EPHBenzeneIsopropylbenzenen-ButylbenzeneBromodichloromethanesec-Butylbenzene1,2-DichloroethaneMWD-42L Standard (g/l)GCL (g/l)MW-1AMW-2MW-3APage 1 of 9
EPAMethod6010BWell IDDate Collected (mm/dd/yy)1 600 600 500 20 6 0.6 70 70 0.4 70 70 70 0.7 400 400 15 400 700 200 700 10,000 2005,000 260,000 84,500 85,500 20,000 6,000 NE 6,900 8,500 400 25,000 70,000 30,000 700 28,500 25,000 15,000 NE NE NE NE NE NEContaminant of Concern LeadNaphthaleneIPETolueneEthylbenzeneXylenesTetrachloroethenen-PropylbenzeneMTBEC9-C18 AliphaticsC9-C12 Aliphatics1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneC5-C8 AliphaticsC11-C22 AromaticsC19-C36 AliphaticsC9-C10 AromaticsTABLE 2 SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS RED APPLE MARKET #3 (INCIDENT NO. 10673)Analytical MethodDate: 10/27/16Facility ID #: 0-017539EPA Method 6200BMADEP Methods VPH and EPHBenzeneIsopropylbenzenen-ButylbenzeneBromodichloromethanesec-Butylbenzene1,2-Dichloroethane2L Standard (g/l)GCL (g/l)01/09/0948076 8.0 J 1601,200 36 B<1.8 <1.7 <1.4133.2 J 28 J <1.5 <1.6 43 6.3 J 13.9 <500 223 160 <105 <105 <10505/12/103.410.770 <0.500 <1.0037.8<5.00 <0.500 <0.500 <0.500 <0.500 <0.500 1.23 <0.500 <0.500 <0.500 <0.50045.9<100 <100 <100 <99.0 <99.0 <99.005/02/11 0.26 J <0.13 <0.15 <0.30 11.3 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR08/28/1272480 37.9 4181,040 42.5<2.3 <2.0 <2.011.34.2 J 30.6 3.6 J <2.7 82.9 13.6 NR NR NR NR NR NR NR08/19/13 0.19 J <0.10 <0.10 <0.2221.6<0.15 <0.10 <0.10 <0.10 <0.10 <0.10 0.45 J <0.10 <0.10 <0.10 <0.1039.1<35 <35 <35 <110 <110 <16007/09/142.2 0.92 0.64 0.83 J28.8 0.56 <0.10 <0.10 <0.10 <0.10 0.14 J 0.83 <0.10 <0.10 0.32 J <0.10 76.9 <35 <35 <35 <100 <100 <150 03/24/15 <0.17 <0.17 <0.15 <0.43 0.33 J <0.12 <0.15 <0.14 <0.14 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NR01/11/16 0.59 <0.13 <0.13 <0.31 90.1 0.14 J <0.13 <0.13 <0.13 2.3 <0.13 4.2 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR04/28/08 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS01/07/09FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP05/12/1013,10031,400 5,480 25,000 5,960 1,850<0.50019637.4 <0.500144 194 1,770<0.5004,850 3,160 142 83,800 24,000 20,000 16,5002267,39005/02/1112,00047,400 3,490 17,980 5,860 819<29126 J48.4 J258 172 177 631<344,970 1,280NR NR NR NR NR NR NR08/28/1210,80025,600 2,980 14,500 4,470 638<120 <100 <100276 J<100137 J 335 J<1402,410 607NR NR NR NR NR NR NR08/19/137,14017,600 1,920 11,600 2,540 384<10 19.0 J 11.7 J13966.387.9 253<101,890 446 124 13,100 16,800 7,290 J 3,930<10033907/09/148,36018,600 2,030 10,100 4,240 465 <5.0 23.8 J 14.2 J204 84.7 146 300 <5.0 2,000 499 270 17,300<1,8006,960 3,500<400 639 J03/24/1511,50023,800 3,190 18,000 6,290 1,110<74 104 J<69 270 182 J 273 645<74 4,730 1,300NR NR NR NR NR NR NR01/11/1613,800 31,700 6,140 31,800 4,400 2,550 <31 520 214 250 484 227 2,010 <31 5,470 3,740 NR NR NR NR NR NR NR10/13/168,660 24,600 3,790 22,100 3,770 2,080 <63 190 J 95.6 J 215 J 221 J 167 J 918 <63 7,440 2,140 NR NR NR NR NR NR NR04/23/08FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP01/07/09FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP05/12/10777148 131 340185 417<0.500135 75.0<0.500 52.4 50.795.8 3.30380 148 12.23,740 1,780 1,940 231,000 50,800 88,20005/02/11FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FPNR NR NR NR NR NR NR08/28/1237758.3 69.8 17794.5 269<1.2 12.2 15.014.416.2 17.3 26.11.5 J200 52.2 NR NR NR NR NR NR NR08/19/1332911.5 42.9 82.5106 141<1.0 13.1 17.814.314.4 18.4 25.63.0 J116 19.722.6 544 J 2,500 1,580 90,800 25,600 15,20007/09/14274 9.3 43.7 87.1 217 197 <1.0 40.8 45.3 22.5 25.4 32.4 38.3 3.0 J189 54.2 12.1 1,140 J 4,310 4,730 74,300 29,500 36,80003/24/151017.2 9.5 40.221.4 115<0.74 8.0 10.93.79.8 4.7 11.31.5 J79.0 24.1 NR NR NR NR NR NR NR01/11/16 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS10/13/16198 2.9 14.0 37.7 14.8 101 <0.63 5.0 8.2 3.4 6.4 5.4 7.7 1.3 J61.1 15.8 NR NR NR NR NR NR NR04/23/08 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS08/28/12319237 5991,150<1.3237<1.2 62.2 27.1 <1.675.16.4339<1.41,930 651NR NR NR NR NR NR NR08/19/1315398.9 4321,270 20.7 229<1.012654.26.1 133<1.0419<1.01,190 673 15.4 4,170 J 5,640 7,010 5,910227967 J07/09/14201 142 488 981 6.4 J205 <2.5 183 68.2 <2.5 112 3.1 J542 <2.5 1,830 968 48.9 6,360<1,8006,600 17,1001,930 J2,88003/24/15164149 3431,0806.7 J136<3.7 54.9 24.5 <4.1 65.2 <4.0 291<3.7 2,820 E 1,150NR NR NR NR NR NR NR01/11/16349 160 405 1,160 26.6 J 352 <13 414 128 <13 133 <13 770 <13 <13 1,320 NR NR NR NR NR NR NR10/13/16123 22.6 146 326 12.1 113 <1.3 33.3 15.6 4.2 J36.8 6.0 170 <1.3 1,010 E290 NR NR NR NR NR NR NR04/23/08205 L0.690 I <0.31 22.5 17.445.2<0.14 0.530 I <0.472.442.50 4.51 I <0.303.881.12 <0.2733.3 527187 <100 308 72334501/07/09160<0.70 <0.50 31 <0.5038 B<0.90 13 <0.70 <1.1 4.0 J 4.5 J <0.752.4 J1.0 J <0.5029.6 536<100 <100 <111 <111249MW-6MW-7MW-8MW-9Page 2 of 9
EPAMethod6010BWell IDDate Collected (mm/dd/yy)1 600 600 500 20 6 0.6 70 70 0.4 70 70 70 0.7 400 400 15 400 700 200 700 10,000 2005,000 260,000 84,500 85,500 20,000 6,000 NE 6,900 8,500 400 25,000 70,000 30,000 700 28,500 25,000 15,000 NE NE NE NE NE NEContaminant of Concern LeadNaphthaleneIPETolueneEthylbenzeneXylenesTetrachloroethenen-PropylbenzeneMTBEC9-C18 AliphaticsC9-C12 Aliphatics1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneC5-C8 AliphaticsC11-C22 AromaticsC19-C36 AliphaticsC9-C10 AromaticsTABLE 2 SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS RED APPLE MARKET #3 (INCIDENT NO. 10673)Analytical MethodDate: 10/27/16Facility ID #: 0-017539EPA Method 6200BMADEP Methods VPH and EPHBenzeneIsopropylbenzenen-ButylbenzeneBromodichloromethanesec-Butylbenzene1,2-Dichloroethane2L Standard (g/l)GCL (g/l)05/12/1013.3<0.500 <0.500 1.69 0.810 <5.00 <0.500 <0.500 <0.500 <0.500 0.540 <0.500 <0.500 <0.500 <0.500 <0.50037.9122 <100 <100 <99.0 <99.0 <99.005/03/117.7<0.13 <0.15 2.7 0.82 1.1 <0.12 <0.10 <0.10 0.19 J 0.19 J 0.23 J <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR08/28/1270.50.25 J <0.15 28.2 3.817.8<0.13 0.46 J 0.32 J0.942.8 1.5 <0.11 0.23 J 0.88 <0.10 NR NR NR NR NR NR NR08/19/136.5<0.10 <0.10 1.2 J 0.77 1.2 <0.10 <0.10 <0.10 0.26 J 0.45 J 0.36 J <0.10 <0.10 <0.10 <0.10 14.9 <35 <35 <35 <110 <110 <16007/08/1426.3 0.16 J <0.10 3.0 0.91 7.0 <0.10 0.20 J 0.17 J 0.27 J 1.6 0.46 J <0.10 <0.10 0.30 J <0.10 85.0 148 <35 <35 <100 <100 465 03/24/152.1<0.17 <0.15 0.79 J 0.81 0.61 <0.15 <0.14 <0.14 <0.16 0.23 J 0.36 J <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NR04/23/08 <0.31 <0.28 <0.31 <1.2 <0.12 <0.41 <0.14 <0.39 <0.47 <0.12 <0.24 <0.15 <0.30 <0.33 <0.26 <0.2733.7<100 <100 <100 133 147 12201/07/09272.7 J 3.5 J 2.9 J <0.5018 B<0.90 <0.85 <0.70 <1.1 1.9 J <1.0 <0.75 <0.80 1.0 J 1.3 J77.3253 <100 <100 <111 <11126205/12/10126522 176 206 2.2573.5<0.500 3.94 1.48 <0.500 13.9 1.43 23.2 <0.500 54.4 10.840.1 3,590314389<99.0 <99.0 <99.005/03/11105 1,090237534<3.343.0<2.9 <2.5 <2.6 <4.1 6.3 J <2.7 19.7 <3.4 102 12.9 J NR NR NR NR NR NR NR08/28/127.015.5 8.4 17.1 <0.13 4.3 <0.12 <0.10 <0.10 <0.16 0.41 J <0.11 0.81 <0.14 2.9 <0.10 NR NR NR NR NR NR NR08/19/1328.6260 69.4 139 <1.020.4<1.0 <1.0 <1.0 <1.0 3.2 J <1.0 6.9 <1.0 38.0 7.449.8291 222 127 107 J <100 <15007/08/1442.8 284 74.7 167 <0.10 30.6 <0.10 1.0 0.52 <0.10 4.3 0.14 J 10.4 <0.10 38.6 4.5 111 902 <35241 <100 <100 <150 03/24/15 <0.17 0.65 <0.15 <0.43 <0.16 <0.12 <0.15 <0.14 <0.14 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NR04/23/08108<1.4 <1.6 <5.8415 9.30<0.70 <2.0 <2.46.75<1.2 4.30 I <1.5 <1.7 1.70 I <1.4 6.07 225 122 <100 361 20644001/07/0992<0.70 <0.50 2.5 J820 8.2 B<0.90 <0.85 <0.70161.2 J 13 J <0.75 <0.80 <0.70 <0.5023.5 10,100<100 <100 <111 <111 <11105/12/1017.1<0.500 <0.500 <1.00357<5.00 <0.500 <0.500 <0.5009.90<0.500 8.94 <0.500 <0.500 <0.500 <0.50023.9316 <100 <100 <100 <100 <10005/03/117.6<1.3 <1.5 <3.0461<1.0 <1.2 <1.0 <1.07.5<1.0 10.1 <1.1 <1.4 <1.0 <1.0 NR NR NR NR NR NR NR08/28/128.9<0.13 <0.15 <0.301140.87 <0.12 <0.10 <0.103.10.13 J 2.5 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR08/19/1337.5<1.0 <1.0 <2.23263.4 J <1.0 <1.0 <1.08.2<1.0 7.9 <1.0 <1.0 2.2 J <1.0 6.7 <35 <35 <35 <100 <100 <150 07/08/1427.9 0.12 J <0.10 1.4 J492 2.6 <0.10 <0.10 0.39 J10.8 0.61 12.9 <0.10 <0.10 <0.10 <0.10 34.6 <70 <70 <70 <100 <100 162 J03/24/1514.70.59 <0.15 1.0 J1181.6 <0.15 <0.14 0.26 J7.80.50 7.1 <0.16 0.19 J <0.14 <0.14 NR NR NR NR NR NR NR04/23/08 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS01/09/0970140 53 140 4.5 J34 B<0.90 <0.85 <0.70 <1.1 5.1 5.6 J 6.63.1 J47 14 4.8 272 157 119 <105 <105 <10505/12/10234200 217 323 2.0794.5<0.500 11.0 2.70 <0.500 17.1 20.2 34.91.31153 64.1 6.401,590513609<99.0 <99.0 <99.005/02/11158168 138 198.1 0.94 J57.3<0.59 1.5 J 0.92 J4.17.9 9.3 20.80.76 J98.4 31.9 NR NR NR NR NR NR NR08/28/1297.076.7 96.8 113 0.8046.9<0.12 0.94 1.03.46.0 9.0 7.61.220.6 6.5 NR NR NR NR NR NR NR08/19/1336.039.6 30.8 64.0 0.26 J24.4<0.10 0.73 0.731.33.8 3.0 3.61.311.7 2.054.5106 202 127 <100 <100 <150 07/09/1445.7 12.3 27.0 54.1 0.44 J22.7 <0.10 0.65 0.67 1.5 3.6 3.9 2.9 1.4 13.2 3.0 28.5 133 <35 61.9 J <95 <95 145 JMW-11MW-12MW-13MW-10Page 3 of 9
EPAMethod6010BWell IDDate Collected (mm/dd/yy)1 600 600 500 20 6 0.6 70 70 0.4 70 70 70 0.7 400 400 15 400 700 200 700 10,000 2005,000 260,000 84,500 85,500 20,000 6,000 NE 6,900 8,500 400 25,000 70,000 30,000 700 28,500 25,000 15,000 NE NE NE NE NE NEContaminant of Concern LeadNaphthaleneIPETolueneEthylbenzeneXylenesTetrachloroethenen-PropylbenzeneMTBEC9-C18 AliphaticsC9-C12 Aliphatics1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneC5-C8 AliphaticsC11-C22 AromaticsC19-C36 AliphaticsC9-C10 AromaticsTABLE 2 SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS RED APPLE MARKET #3 (INCIDENT NO. 10673)Analytical MethodDate: 10/27/16Facility ID #: 0-017539EPA Method 6200BMADEP Methods VPH and EPHBenzeneIsopropylbenzenen-ButylbenzeneBromodichloromethanesec-Butylbenzene1,2-Dichloroethane2L Standard (g/l)GCL (g/l)04/24/08 0.510 I <0.28 <0.31 <1.2 <0.12 <0.41 <0.14 <0.39 <0.47 <0.12 <0.24 0.330 I <0.300.790 I<0.26 <0.27238<100 <100 <100 <75 130 <5001/09/09 1.0 J 1.1 J 0.54 J <1.0 <0.50 3.2 JB <0.90 <0.85 <0.70 <1.1 <0.55 <1.0 <0.751.5 J<0.70 <0.5080.4<100 <100 <100 <105 <105 <10505/12/1023.50.710 0.620 6.97 <0.50019.6<0.500 <0.500 0.980 <0.500 2.44 3.36 0.6001.662.69 <0.50077.6<100 <100 <100 <99.0 <99.0 <99.005/02/1128.83.0 16.8 30.0 <0.1315.9<0.12 0.25 J 1.21.12.7 3.4 2.81.314.7 4.3 NR NR NR NR NR NR NR08/28/1257.71.9 60.6 33.5 0.21 J26.7<0.12 0.60 2.61.54.4 4.4 8.0 0.63 37.7 6.7 NR NR NR NR NR NR NR08/19/1310.90.40 J 12.7 9.3 <0.106.5<0.10 0.12 J 0.740.46 J1.0 1.5 2.00.777.5 1.394.836.8 J 72.0 J 58.6 J <100 193 J <150 07/09/1412.5 0.27 J 4.3 8.3 0.13 J7.7 <0.10 <0.10 1.5 0.63 1.2 2.2 0.70 0.77 4.1 0.59 46.4 51.2 J <35 37.4 J <95 <95 <140 03/24/1531.21.3 2.2 13.4 <0.16 4.4 <0.15 <0.14 1.51.11.6 3.8 0.57 0.30 J 4.9 0.90 NR NR NR NR NR NR NR01/11/1679.8 1.1 27.9 32.5 0.29 J29.6 <0.13 0.61 1.9 2.0 7.4 6.8 5.9 0.33 J 35.0 3.9 NR NR NR NR NR NR NR04/24/08 <0.31 <0.28 <0.31 <1.2 <0.12 <0.41 <0.14 <0.39 <0.47 <0.12 <0.24 <0.15 <0.30 <0.33 <0.26 <0.2760.1<100 <100 <100 370 6,66064201/07/09FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP05/12/10 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.50052.8<100 <100 <100 <100 <100 <10005/02/11 <0.13 <0.13 <0.15 <0.30 <0.13 0.23 J <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR08/19/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 6.0 <35 <35 <35 <110 <110 <160 07/08/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NSMW-16 04/23/084.17<0.28 <0.31 <1.2 0.580 I 0.770 I <0.14 <0.39 <0.47 <0.12 0.370 I 0.290 I <0.30 <0.33 0.280 I <0.2715.3<100 <100 <100 205 46627901/07/0915<0.70 <0.50 <1.0 1.5 J 2.8 JB <0.90 <0.85 <0.70 <1.1 1.6 J 1.1 J <0.75 <0.80 <0.70 <0.5015.7117 <100 <100 <111 <111 <11105/12/10 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.50034.0<100 <100 <100 <105 <105 <10505/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR08/28/12 0.57 <0.13 <0.15 <0.30 0.13 J 0.12 J <0.12 <0.10 <0.10 <0.16 <0.10 0.17 J <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR08/19/1310.80.16 J <0.10 0.40 J 0.29 J 1.7 <0.10 <0.10 0.23 J 0.17 J 1.6 0.31 J <0.10 <0.10 <0.10 <0.10 12.4 63.6 J <35 <35 <100 <100 <160 07/08/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS04/24/0817648.6 39.4 84.8 5.42 1.65 <0.14 0.610 I 0.540 I2.572.55 4.07 I 6.10 <0.33 42.9 13.421.0 851<10020493.1 94.2 96.001/09/095211 12 13 J <0.50 1.4 JB <0.90 <0.85 <0.70 <1.1 1.4 J <1.0 2.4 J <0.80 10 2.0 J 4.8465<100 <100 <100 <100 <10005/12/101154.08 11.5 9.63 5.62 <5.00 <0.500 0.840 0.580 <0.500 2.31 4.03 2.97 <0.500 15.0 1.6837.7 867<100 <100 <100 <100 <10005/02/111387.3 17.1 10.0 J 2.7 1.2 J <0.59 <0.50 <0.511.2 J1.0 J 2.2 J 2.9 <0.69 7.5 1.9 J NR NR NR NR NR NR NR08/28/121072.4 15.6 6.4 2.2 0.49 J <0.12 0.24 J 0.31 J0.901.1 2.0 2.8 0.35 J 6.9 2.3 NR NR NR NR NR NR NR08/19/1333.10.54 7.3 2.5 0.94 0.20 J <0.10 0.18 J 0.22 J0.42 J0.72 0.96 2.0 0.20 J 2.8 1.318.190.5 J 56.4 J <35 <100 <100 <160 07/09/1439.7 0.40 J 3.5 1.2 J 1.3 0.35 J <0.10 <0.10 0.20 J0.41 J0.45 J 1.4 0.82 0.27 J 2.7 0.61 11.3 86.4 J <35 <35 <96 <96 <140 03/24/151834.0 4.7 <2.2 4.5 2.1 J <0.74 <0.72 <0.69 2.1 J0.94 J 3.5 1.2 J <0.74 5.2 <0.68 NR NR NR NR NR NR NR01/11/165.6 <0.13 0.18 J <0.31 0.58 <0.13 <0.13 <0.13 <0.13 0.24 J 0.23 J 0.74 <0.13 0.31 J 0.78 <0.13 NR NR NR NR NR NR NRMW-16AMW-14MW-17MW-15Page 4 of 9
EPAMethod6010BWell IDDate Collected (mm/dd/yy)1 600 600 500 20 6 0.6 70 70 0.4 70 70 70 0.7 400 400 15 400 700 200 700 10,000 2005,000 260,000 84,500 85,500 20,000 6,000 NE 6,900 8,500 400 25,000 70,000 30,000 700 28,500 25,000 15,000 NE NE NE NE NE NEContaminant of Concern LeadNaphthaleneIPETolueneEthylbenzeneXylenesTetrachloroethenen-PropylbenzeneMTBEC9-C18 AliphaticsC9-C12 Aliphatics1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneC5-C8 AliphaticsC11-C22 AromaticsC19-C36 AliphaticsC9-C10 AromaticsTABLE 2 SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS RED APPLE MARKET #3 (INCIDENT NO. 10673)Analytical MethodDate: 10/27/16Facility ID #: 0-017539EPA Method 6200BMADEP Methods VPH and EPHBenzeneIsopropylbenzenen-ButylbenzeneBromodichloromethanesec-Butylbenzene1,2-Dichloroethane2L Standard (g/l)GCL (g/l)04/24/08 <0.31 <0.28 <0.31 <1.2 <0.12 <0.41 <0.14 <0.39 <0.47 <0.12 <0.24 <0.15 <0.30 <0.33 <0.26 <0.2720.4<100 <100 <100 167 21221601/09/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <0.90 <0.85 <0.70 <1.1 <0.55 <1.0 <0.75 <0.80 <0.70 <0.50 13.8 <100 <100 <100 <105 <105 <10505/12/10 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR08/19/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.1015.6<35 <35 <35 <110 <110 <160 07/08/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 29.9 <35 <35 <35 <99 <99 <150 03/24/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.15 <0.14 <0.14 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NR04/24/082860.320 I <0.31 4.89197 12.9<0.14 <0.39 <0.4710.51.97 14.3 <0.30 <0.33 <0.26 <0.27 7.21539117 <100 152 196 17901/09/09130<0.70 <0.50 3.0 J78 6.7 B<0.90 <0.85 <0.704.5 J1.3 J 11 J <0.75 <0.80 <0.70 <0.50 13.1461<100 <100 <105 <105 <10505/12/10119<0.500 <0.500 3.94224 7.61<0.500 <0.500 0.5209.431.72 11.6 <0.500 <0.500 <0.500 <0.500 12.8445<100 <100 <103 <103 <10305/03/1142.2<0.13 <0.15 0.34 J1002.7 <0.12 <0.10 0.14 J3.00.15 J 6.6 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR08/28/1228.0<0.13 <0.15 0.62 J1022.3 <0.12 <0.10 0.26 J7.80.13 J 7.8 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR08/19/138.6<0.10 <0.10 0.26 J75.50.44 J <0.10 <0.10 0.37 J2.10.23 J 8.5 <0.10 <0.10 <0.10 <0.10 14.0 36.3 J <35 <35 <100 <100 <150 07/08/149.3 <0.10 <0.10 0.41 J120 0.37 J <0.10 <0.10 0.59 1.7 0.63 10.1 <0.10 <0.10 <0.10 <0.10 25.9 87.7 J <35 <35 <99 <99 249 03/24/154.3<0.83 <0.76 <2.2 211<0.61 <0.74 <0.72 0.73 J2.51.4 J 12.0 <0.78 <0.74 <0.68 <0.68 NR NR NR NR NR NR NR04/24/08 <0.31 <0.28 <0.31 <1.2 <0.12 <0.41 <0.14 <0.39 <0.47 <0.12 <0.24 <0.15 <0.30 <0.33 <0.26 <0.2734.1<100 <100 <100 <75 <75 <5001/09/091.4 J<0.70 <0.50 <1.0 <0.50 0.67 JB <0.90 <0.85 <0.70 <1.1 <0.55 <1.0 <0.75 <0.80 <0.70 <0.5024.0<100 <100 <100 <105 <105 <10505/12/10 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.50044.2<100 <100 <100 <102 <102 <10205/02/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 0.45 J <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR08/19/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.1028.2<35 <35 <35 <100 <100 <150 07/09/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 60.3 <35 <35 <35 <96 <96 <140 03/24/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.15 <0.14 <0.14 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NR04/24/08 <0.31 <0.28 <0.31 <1.2 <0.12 <0.41 <0.14 <0.39 <0.47 <0.12 <0.24 <0.15 <0.30 0.410 I <0.26 <0.2732.9<100 <100 <100 <75 <75 <5001/09/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <0.90 <0.85 <0.70 <1.1 <0.55 <1.0 <0.75 <0.80 <0.70 <0.5053.0<100 <100 <100 <105 <105 <10505/02/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.105.6<0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR08/19/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.1039.1<35 <35 <35 <100 <100 <150 07/09/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 75.2 <35 <35 <35 <96 <96 141 J03/24/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.15 <0.14 <0.14 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NRMW-21MW-19MW-20MW-18Page 5 of 9
EPAMethod6010BWell IDDate Collected (mm/dd/yy)1 600 600 500 20 6 0.6 70 70 0.4 70 70 70 0.7 400 400 15 400 700 200 700 10,000 2005,000 260,000 84,500 85,500 20,000 6,000 NE 6,900 8,500 400 25,000 70,000 30,000 700 28,500 25,000 15,000 NE NE NE NE NE NEContaminant of Concern LeadNaphthaleneIPETolueneEthylbenzeneXylenesTetrachloroethenen-PropylbenzeneMTBEC9-C18 AliphaticsC9-C12 Aliphatics1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneC5-C8 AliphaticsC11-C22 AromaticsC19-C36 AliphaticsC9-C10 AromaticsTABLE 2 SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS RED APPLE MARKET #3 (INCIDENT NO. 10673)Analytical MethodDate: 10/27/16Facility ID #: 0-017539EPA Method 6200BMADEP Methods VPH and EPHBenzeneIsopropylbenzenen-ButylbenzeneBromodichloromethanesec-Butylbenzene1,2-Dichloroethane2L Standard (g/l)GCL (g/l)04/24/0819.2<0.28 <0.31 <1.2 9.01 1.54 <0.14 <0.39 <0.471.35<0.24 1.96 I <0.30 <0.33 <0.26 <0.2724.6<100 <100 <100 <75 90.9 <5001/09/09 <0.60 <0.70 <0.50 <1.0 3.2 J <0.60 <0.90 <0.85 <0.70 <1.1 <0.55 <1.0 <0.75 <0.80 <0.70 <0.5025.6<100 <100 <100 <105 <105 <10505/12/103.90<0.500 <0.500 <1.00 6.17 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 1.14 <0.500 <0.500 <0.500 <0.50021.5<100 <100 <100 <108 <108 <10805/03/11 0.33 J <0.13 <0.15 <0.30 5.3 <0.10 <0.12 <0.10 <0.10 0.38 J <0.10 0.58 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR08/28/12 <0.13 <0.13 <0.15 <0.30 2.8 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR08/19/13 <0.10 <0.10 <0.10 <0.22 1.5 <0.15 <0.10 <0.10 <0.10 0.25 J <0.10 0.64 <0.10 <0.10 <0.10 <0.1018.2<35 <35 <35 <110 <110 <160 07/08/14 0.13 J <0.10 <0.10 <0.20 1.5 <0.10 <0.10 <0.10 <0.10 0.23 J <0.10 0.76 <0.10 <0.10 <0.10 <0.10 29.0 <35 <35 <35 <200 827 716 03/24/151.1<0.17 <0.15 <0.43 2.9 <0.12 <0.15 <0.14 <0.14 0.23 J <0.12 0.88 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NR04/24/08 <0.31 <0.28 <0.31 <1.2 0.380 I <0.41 <0.14 <0.39 <0.47 <0.12 <0.24 <0.15 <0.30 <0.33 <0.26 <0.2732.7<100 <100 <100 <75 <75 <5001/09/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <0.90 <0.85 <0.70 <1.1 <0.55 <1.0 <0.75 <0.80 <0.70 <0.5040.0<100 <100 <100 <105 <105 <10505/12/10 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.50060.9<100 <100 <100 <108 <108 <10805/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR08/19/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS04/24/08 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS01/07/09 0.68 J <0.70 <0.50 <1.0 <0.50 0.68 JB <0.90 <0.85 <0.70 <1.1 <0.55 <1.0 <0.75 <0.80 <0.70 <0.5017.1<100 <100 <100 <111 <111 <11105/12/10 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR08/19/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.1018.6<35 <35 <35 <110 <110 <160 07/08/14 <0.10 0.11 J <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 6.6 <35 <35 <35 <100 <100 <150 04/23/08 <0.31 <0.28 <0.31 <1.2 <0.12 0.800 I <0.14 <0.39 <0.47 <0.12 <0.24 <0.15 <0.30 <0.33 <0.26 <0.27 9.66 <100 <100 <100 96.4 88.3 13301/09/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <0.90 <0.85 <0.70 <1.1 <0.55 <1.0 <0.75 <0.80 <0.70 <0.50 14.6 <100 <100 <100 <105 <105 <10505/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR08/28/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS08/19/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.1017.0<35 <35 <35 <110 <110 <170 07/08/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 32.5 <35 <35 <35 <99 <99 <150 03/24/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.15 <0.14 <0.14 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NR04/23/08 <0.31 <0.28 <0.31 <1.2 <0.12 <0.41 <0.14 <0.39 <0.47 <0.12 <0.24 <0.15 <0.30 <0.33 <0.26 <0.2742.4<100 <100 <100 <75 <75 87.201/07/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <0.90 <0.85 <0.70 <1.1 <0.55 <1.0 <0.75 <0.80 <0.70 <0.5038.3<100 <100 <100 <111 <111 <11105/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.100.42 J<0.10 <0.11 <0.110.93<0.10 <0.10 NR NR NR NR NR NR NR08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 0.48 J <0.10 <0.10 NR NR NR NR NR NR NR08/19/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 0.40 J <0.10 <0.1032.8<35 <35 <35 <110 <110 <160 07/08/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 0.31 J <0.10 0.74 <0.10 0.29 J <0.10 <0.10 41.0 <35 <35 <35 <100 <100 <150 MW-23MW-22MW-26MW-24MW-25Page 6 of 9
EPAMethod6010BWell IDDate Collected (mm/dd/yy)1 600 600 500 20 6 0.6 70 70 0.4 70 70 70 0.7 400 400 15 400 700 200 700 10,000 2005,000 260,000 84,500 85,500 20,000 6,000 NE 6,900 8,500 400 25,000 70,000 30,000 700 28,500 25,000 15,000 NE NE NE NE NE NEContaminant of Concern LeadNaphthaleneIPETolueneEthylbenzeneXylenesTetrachloroethenen-PropylbenzeneMTBEC9-C18 AliphaticsC9-C12 Aliphatics1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneC5-C8 AliphaticsC11-C22 AromaticsC19-C36 AliphaticsC9-C10 AromaticsTABLE 2 SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS RED APPLE MARKET #3 (INCIDENT NO. 10673)Analytical MethodDate: 10/27/16Facility ID #: 0-017539EPA Method 6200BMADEP Methods VPH and EPHBenzeneIsopropylbenzenen-ButylbenzeneBromodichloromethanesec-Butylbenzene1,2-Dichloroethane2L Standard (g/l)GCL (g/l)04/24/08 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS01/07/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <0.90 <0.85 <0.70 <1.1 <0.55 <1.0 <0.75 <0.80 <0.70 <0.5053.5<100 <100 <100 <111 <111 <11105/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR08/19/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS04/24/08 <0.31 <0.28 <0.31 <1.2 0.680 I <0.41 <0.14 <0.39 <0.47 <0.12 <0.24 <0.15 <0.30 <0.33 <0.26 <0.2759.1<100 <100 <100 <75 94.6 <5001/09/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <0.90 <0.85 <0.70 <1.1 <0.55 <1.0 <0.75 <0.80 <0.70 <0.5040.4<100 <100 <100 <105 <105 <10505/03/11 <0.13 <0.13 <0.15 <0.30 0.20 J <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 0.22 J <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR08/19/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS03/24/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.15 <0.14 <0.14 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NR04/24/08 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS01/09/09200<0.70 <0.50 4.0 J <0.5028 B<0.90 13 B 0.75 J <1.1 3.7 J <1.0 <0.752.1 J<0.70 <0.50 3.5627<100 <100 <105 <105 <10505/12/10149<0.500 <0.500 2.52 3.7920.0<0.500 0.520 <0.500 <0.500 3.59 1.72 <0.5001.11<0.500 <0.50015.7 519<100 <100 <108 <108 <10805/03/1135.3<0.13 <0.15 0.35 J 1.4 2.7 <0.12 <0.10 <0.100.41 J0.61 0.47 J <0.11 0.24 J <0.10 <0.10 NR NR NR NR NR NR NR08/28/126.2<0.13 <0.15 <0.30 1.7 0.39 J <0.12 <0.10 <0.100.41 J0.43 J 0.37 J <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR08/19/13 1.0 <0.10 <0.10 <0.22 1.6 <0.15 <0.10 <0.10 <0.100.47 J<0.10 0.49 J <0.10 <0.10 <0.10 <0.10 7.7 <35 <35 <35 <110 <110 <160 07/08/14 <0.10 <0.10 <0.10 <0.20 1.7 <0.10 <0.10 <0.10 <0.10 0.38 J <0.10 0.41 J <0.10 <0.10 <0.10 <0.10 20.9 <35 <35 <35 <100 <100 <150 03/24/15 <0.17 <0.17 <0.15 <0.43 0.34 J <0.12 <0.15 <0.14 <0.14 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NRMW-30 04/24/08 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS04/24/08 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS01/07/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <0.90 <0.85 <0.70 <1.1 <0.55 <1.0 <0.75 <0.80 <0.70 <0.50 11.0 <100 <100 <100 <111 <111 <11105/12/10 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.50069.9<100 <100 <100 <108 <108 <10805/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR08/28/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS08/19/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS03/24/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.15 <0.14 <0.14 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NR04/24/08 <0.31 <0.28 <0.31 <1.2 <0.12 <0.41 <0.14 <0.39 <0.47 <0.12 <0.24 <0.15 <0.30 <0.33 <0.26 <0.2741.6<100 <100 <100 <75 94.6 88.101/09/091.7 J<0.70 <0.50 <1.0 <0.50 2.7 JB <0.90 <0.85 <0.70 <1.1 <0.55 <1.0 <0.75 <0.80 <70 <0.5029.1<100 <100 <100 <105 <105 <10505/12/10 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.50046.8<100 <100 <100 <108 <108 <10805/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 0.29 J <0.10 <0.10 NR NR NR NR NR NR NR08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 0.28 J <0.10 <0.10 NR NR NR NR NR NR NR08/19/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NSMW-27MW-32MW-28MW-29MW-31Page 7 of 9
EPAMethod6010BWell IDDate Collected (mm/dd/yy)1 600 600 500 20 6 0.6 70 70 0.4 70 70 70 0.7 400 400 15 400 700 200 700 10,000 2005,000 260,000 84,500 85,500 20,000 6,000 NE 6,900 8,500 400 25,000 70,000 30,000 700 28,500 25,000 15,000 NE NE NE NE NE NEContaminant of Concern LeadNaphthaleneIPETolueneEthylbenzeneXylenesTetrachloroethenen-PropylbenzeneMTBEC9-C18 AliphaticsC9-C12 Aliphatics1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneC5-C8 AliphaticsC11-C22 AromaticsC19-C36 AliphaticsC9-C10 AromaticsTABLE 2 SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS RED APPLE MARKET #3 (INCIDENT NO. 10673)Analytical MethodDate: 10/27/16Facility ID #: 0-017539EPA Method 6200BMADEP Methods VPH and EPHBenzeneIsopropylbenzenen-ButylbenzeneBromodichloromethanesec-Butylbenzene1,2-Dichloroethane2L Standard (g/l)GCL (g/l)04/24/08 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS01/09/09 <0.60 <0.70 <0.50 <1.0 <0.50 0.84 JB <0.90 <0.85 <0.70 <1.1 <0.55 <1.0 <0.75 <0.80 <0.70 <0.5018.9<100 <100 <100 <105 <105 <10505/12/101.41<0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.50045.0<100 <100 <100 <111 <111 <11105/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR08/19/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.1028.7<35 <35 <35 <110 <110 <160 07/08/14 <0.10 0.34 J <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 76.4 <35 <35 <35 <100 <100 <150 03/24/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.15 <0.14 <0.14 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NR05/12/1059.1<0.500 <0.500 <1.00 1.37 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 1.17 <0.5006.52<0.500 <0.500146120 <100 <100 <118 <118 <11805/03/1141.5<0.13 <0.15 0.12 J 1.0 3.3 <0.12 <0.10 <0.10 0.38 J 0.14 J 0.62 <0.114.9<0.10 <0.10 NR NR NR NR NR NR NR08/28/128.6<0.13 <0.15 <0.30 0.31 J 0.69 <0.12 <.010 <0.10 <0.16 <0.10 0.18 J <0.111.1<0.10 <0.10 NR NR NR NR NR NR NR08/19/1310.6<0.10 <0.10 <0.22 0.63 1.2 <0.10 <0.10 <0.10 0.26 J <0.10 0.47 J <0.101.6<0.10 <0.10 12.3 <35 <35 <35 <110 <110 <160 07/08/146.2 0.11 J <0.10 <0.20 0.58 0.80 <0.10 <0.10 <0.10 0.22 J <0.10 0.45 J <0.10 1.1 <0.10 <0.10 46.8 <35 <35 <35 <99 <99 <150 03/24/15 0.49 J <0.17 <0.15 <0.43 0.39 J <0.12 <0.15 <0.14 <0.14 <0.16 <0.12 0.27 J <0.16 0.53 <0.14 <0.14 NR NR NR NR NR NR NR05/12/10 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500381<100 <100 <100 <121 <121 <12105/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR08/19/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS05/12/10 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500314<100 <100 <100 <118 <118 <11805/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR08/19/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS05/03/113.4<0.13 <0.15 <0.30 0.29 J 0.19 J <0.12 <0.10 <0.10 <0.16 <0.10 0.19 J <0.111.1<0.10 <0.10 NR NR NR NR NR NR NR08/28/12 0.47 J <0.13 <0.15 <0.30 0.21 J <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 0.16 J <0.11 0.69 <0.10 <0.10 NR NR NR NR NR NR NR08/19/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS03/24/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.15 <0.14 <0.14 <0.16 <0.12 <0.16 <0.16 0.17 J <0.14 <0.14 NR NR NR NR NR NR NR05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR08/19/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS03/24/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.15 <0.14 <0.14 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NR05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR08/19/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS03/24/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.15 <0.14 <0.14 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NRMW-36MW-39MW-33MW-34MW-37MW-38MW-35Page 8 of 9
EPAMethod6010BWell IDDate Collected (mm/dd/yy)1 600 600 500 20 6 0.6 70 70 0.4 70 70 70 0.7 400 400 15 400 700 200 700 10,000 2005,000 260,000 84,500 85,500 20,000 6,000 NE 6,900 8,500 400 25,000 70,000 30,000 700 28,500 25,000 15,000 NE NE NE NE NE NEContaminant of Concern LeadNaphthaleneIPETolueneEthylbenzeneXylenesTetrachloroethenen-PropylbenzeneMTBEC9-C18 AliphaticsC9-C12 Aliphatics1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneC5-C8 AliphaticsC11-C22 AromaticsC19-C36 AliphaticsC9-C10 AromaticsTABLE 2 SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS RED APPLE MARKET #3 (INCIDENT NO. 10673)Analytical MethodDate: 10/27/16Facility ID #: 0-017539EPA Method 6200BMADEP Methods VPH and EPHBenzeneIsopropylbenzenen-ButylbenzeneBromodichloromethanesec-Butylbenzene1,2-Dichloroethane2L Standard (g/l)GCL (g/l)05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.103.3<0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR08/19/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.150.81<0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.1081.7<35 <35 <35 <110 <110 <160 07/09/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 0.21 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 129 <35 <35 <35 <97 <97 <150 03/24/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.15 <0.14 <0.14 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NRSpigot -1 05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.1010.4<0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NRSpigot-2 05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.103.4<0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NRSpigot-3 05/03/11 <0.13 <0.13 <0.15 <0.30 0.19 J <0.108.3<0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NRSpigot-4 05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.106.5<0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NRSpigot-5 05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.106.7<0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NRSpigot-6 05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 0.18 J7.7<0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NRSpigot-7 05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.107.5<0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NRSpigot-8 05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.106.7<0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NRNotes:•Results reported in g/l (micrograms per liter).• 2L Standard: as specified in T15A NCAC 2L.0202•GCL : Gross contamination level.•Less than the method detection limit specified in the laboratory report.• Concentrations in bold face type exceeded the 2L Standards; concentrations in italics exceeded the GCLs.• FP: Free Product.• NE: Not established.• NS: Not sampled; well not located.• NR: Analyses not requested.• J or I: Estimated value.• B: Present in laboratory blank.• E: Value exceeded laboratory calibration range.• Concentrations of 1,2-dibromoethane (92.6 J µg/l in MW-7) and styrene (100 J µg/l in MW-7) that exceeded the MACs were reported in the ground water samples collected on October 13, 2016.• Refer to laboratory report for other compounds detected which did not exceed the 2L Standards.MW-40Page 9 of 9

APPENDIX

APPENDIX A
Laboratory Report – Ground Water Samples

10/25/16
Technical Report for
GRI (Geological Resources Inc.)
Ram 3; 1332 E Memorial Dr, Ahoskie, NC
10673/2677
SGS Accutest Job Number: FA37833
Sampling Date: 10/13/16
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
[e-mail]; [e-mail];
[e-mail]; [e-mail]
ATTN: William Regenthal
Total number of pages in report:
Certifications: FL (E83510), LA (03051), KS (E-10327), IA (366), IL (200063), NC (573), NJ (FL002), SC (96038001)
DoD ELAP (L-A-B L2229), CA (2937), TX (T104704404), PA (68-03573), VA (460177),
AK, AR, GA, KY, MA, NV, OK, UT, WA
This report shall not be reproduced, except in its entirety, without the written approval of SGS Accutest.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone] • http://www.accutest.com
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Norm Farmer
Technical Director
Southeast 10/25/16
e-Hardcopy 2.0
Automated Report
34
SGS Accutest is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
1 of 34
FA37833
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................6
3.1: FA37833-1: MW-8 ........................................................................................................7
3.2: FA37833-2: MW-7 ........................................................................................................9
3.3: FA37833-3: MW-2 ........................................................................................................11
3.4: FA37833-4: MW-1A .....................................................................................................13
3.5: FA37833-5: MW-9 ........................................................................................................15
Section 4: Misc. Forms ............................................................................................................17
4.1: Chain of Custody ...........................................................................................................18
Section 5: GC/MS Volatiles - QC Data Summaries ..............................................................21
5.1: Method Blank Summary ................................................................................................22
5.2: Blank Spike Summary ...................................................................................................26
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................30 123452 of 34
FA37833
SGS Accutest
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA37833
Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Project No: 10673/2677
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA37833-1 10/13/16 14:33 JRW 10/17/16 AQ Ground Water MW-8
FA37833-2 10/13/16 14:46 JRW 10/17/16 AQ Ground Water MW-7
FA37833-3 10/13/16 14:57 JRW 10/17/16 AQ Ground Water MW-2
FA37833-4 10/13/16 15:11 JRW 10/17/16 AQ Ground Water MW-1A
FA37833-5 10/13/16 16:03 JRW 10/17/16 AQ Ground Water MW-9
3 of 34
FA378331
Summary of Hits Page 1 of 2
Job Number:FA37833
Account:GRI (Geological Resources Inc.)
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Collected:10/13/16
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA37833-1 MW-8
Benzene 198 2.5 0.63 ug/l SM 6200B
n-Butylbenzene 5.0 2.5 0.63 ug/l SM 6200B
sec-Butylbenzene 8.2 2.5 0.63 ug/l SM 6200B
1,2-Dichloroethane 3.4 2.5 0.63 ug/l SM 6200B
Di-Isopropyl Ether 5.4 2.5 0.63 ug/l SM 6200B
Ethylbenzene 14.0 2.5 0.63 ug/l SM 6200B
Isopropylbenzene 6.4 2.5 0.63 ug/l SM 6200B
p-Isopropyltoluene 3.9 2.5 0.63 ug/l SM 6200B
Methyl Tert Butyl Ether 14.8 2.5 0.63 ug/l SM 6200B
Naphthalene 101 2.5 0.63 ug/l SM 6200B
n-Propylbenzene 7.7 2.5 0.63 ug/l SM 6200B
Tetrachloroethylene 1.3 J 2.5 0.63 ug/l SM 6200B
Toluene 2.9 2.5 0.63 ug/l SM 6200B
1,2,4-Trimethylbenzene 61.1 2.5 0.63 ug/l SM 6200B
1,3,5-Trimethylbenzene 15.8 2.5 0.63 ug/l SM 6200B
m,p-Xylene 31.0 5.0 0.92 ug/l SM 6200B
o-Xylene 6.8 2.5 0.63 ug/l SM 6200B
Xylene (total)37.7 7.5 1.5 ug/l SM 6200B
FA37833-2 MW-7
Benzene 8660 250 63 ug/l SM 6200B
n-Butylbenzene 190 J 250 63 ug/l SM 6200B
sec-Butylbenzene 95.6 J 250 63 ug/l SM 6200B
1,2-Dibromoethane 92.6 J 250 63 ug/l SM 6200B
1,2-Dichloroethane 215 J 250 63 ug/l SM 6200B
Di-Isopropyl Ether 167 J 250 63 ug/l SM 6200B
Ethylbenzene 3790 250 63 ug/l SM 6200B
Isopropylbenzene 221 J 250 63 ug/l SM 6200B
Methyl Tert Butyl Ether 3770 250 63 ug/l SM 6200B
Naphthalene 2080 250 63 ug/l SM 6200B
n-Propylbenzene 918 250 63 ug/l SM 6200B
Styrene 100 J 250 63 ug/l SM 6200B
Toluene 24600 250 63 ug/l SM 6200B
1,2,4-Trimethylbenzene 7440 250 63 ug/l SM 6200B
1,3,5-Trimethylbenzene 2140 250 63 ug/l SM 6200B
m,p-Xylene 15300 500 92 ug/l SM 6200B
o-Xylene 6760 250 63 ug/l SM 6200B
Xylene (total)22100 750 150 ug/l SM 6200B
FA37833-3 MW-2
Benzene 2400 25 6.3 ug/l SM 6200B
4 of 34
FA378332
Summary of Hits Page 2 of 2
Job Number:FA37833
Account:GRI (Geological Resources Inc.)
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Collected:10/13/16
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
1,2-Dichloroethane 7.1 J 25 6.3 ug/l SM 6200B
Di-Isopropyl Ether 31.8 25 6.3 ug/l SM 6200B
Ethylbenzene 198 25 6.3 ug/l SM 6200B
Isopropylbenzene 13.2 J 25 6.3 ug/l SM 6200B
Methyl Tert Butyl Ether 781 25 6.3 ug/l SM 6200B
Naphthalene 154 25 6.3 ug/l SM 6200B
n-Propylbenzene 30.5 25 6.3 ug/l SM 6200B
Toluene 921 25 6.3 ug/l SM 6200B
1,2,4-Trimethylbenzene 264 25 6.3 ug/l SM 6200B
1,3,5-Trimethylbenzene 76.2 25 6.3 ug/l SM 6200B
m,p-Xylene 1090 50 9.2 ug/l SM 6200B
o-Xylene 175 25 6.3 ug/l SM 6200B
Xylene (total)1260 75 15 ug/l SM 6200B
FA37833-4 MW-1A
Toluene 0.39 J 0.50 0.13 ug/l SM 6200B
m,p-Xylene 0.23 J 1.0 0.18 ug/l SM 6200B
FA37833-5 MW-9
Benzene 123 5.0 1.3 ug/l SM 6200B
n-Butylbenzene 33.3 5.0 1.3 ug/l SM 6200B
sec-Butylbenzene 15.6 5.0 1.3 ug/l SM 6200B
Chloroethane 8.7 5.0 2.0 ug/l SM 6200B
1,2-Dichloroethane 4.2 J 5.0 1.3 ug/l SM 6200B
Di-Isopropyl Ether 6.0 5.0 1.3 ug/l SM 6200B
Ethylbenzene 146 5.0 1.3 ug/l SM 6200B
Isopropylbenzene 36.8 5.0 1.3 ug/l SM 6200B
p-Isopropyltoluene 9.1 5.0 1.3 ug/l SM 6200B
Methyl Chloride 3.5 J 5.0 2.0 ug/l SM 6200B
Methyl Tert Butyl Ether 12.1 5.0 1.3 ug/l SM 6200B
Naphthalene 113 5.0 1.3 ug/l SM 6200B
n-Propylbenzene 170 5.0 1.3 ug/l SM 6200B
Styrene 1.8 J 5.0 1.3 ug/l SM 6200B
Toluene 22.6 5.0 1.3 ug/l SM 6200B
1,2,4-Trimethylbenzene a 1010 E 10 2.5 ug/l SM 6200B
1,3,5-Trimethylbenzene 290 5.0 1.3 ug/l SM 6200B
m,p-Xylene 264 10 1.8 ug/l SM 6200B
o-Xylene 61.5 5.0 1.3 ug/l SM 6200B
Xylene (total)326 15 3.1 ug/l SM 6200B
(a) No sample available for reanalysis.
5 of 34
FA378332
SGS Accutest
Sample Results
Report of Analysis
Southeast
Section 3
6 of 34
FA378333
SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID:MW-8
Lab Sample ID:FA37833-1 Date Sampled:10/13/16
Matrix:AQ - Ground Water Date Received:10/17/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E048807.D 5 10/21/16 MM n/a n/a VE1618
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 198 2.5 0.63 ug/l
108-86-1 Bromobenzene ND 2.5 0.63 ug/l
74-97-5 Bromochloromethane ND 2.5 0.63 ug/l
75-27-4 Bromodichloromethane ND 2.5 0.63 ug/l
75-25-2 Bromoform ND 2.5 0.63 ug/l
104-51-8 n-Butylbenzene 5.0 2.5 0.63 ug/l
135-98-8 sec-Butylbenzene 8.2 2.5 0.63 ug/l
98-06-6 tert-Butylbenzene ND 2.5 0.63 ug/l
56-23-5 Carbon Tetrachloride ND 2.5 0.63 ug/l
108-90-7 Chlorobenzene ND 2.5 0.63 ug/l
75-00-3 Chloroethane ND 2.5 1.0 ug/l
67-66-3 Chloroform ND 2.5 0.63 ug/l
95-49-8 o-Chlorotoluene ND 2.5 0.63 ug/l
106-43-4 p-Chlorotoluene ND 2.5 0.63 ug/l
124-48-1 Dibromochloromethane ND 2.5 0.63 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 2.5 1.4 ug/l
106-93-4 1,2-Dibromoethane ND 2.5 0.63 ug/l
75-71-8 Dichlorodifluoromethane ND 2.5 1.0 ug/l
95-50-1 1,2-Dichlorobenzene ND 2.5 0.63 ug/l
541-73-1 1,3-Dichlorobenzene ND 2.5 0.63 ug/l
106-46-7 1,4-Dichlorobenzene ND 2.5 0.63 ug/l
75-34-3 1,1-Dichloroethane ND 2.5 0.63 ug/l
107-06-2 1,2-Dichloroethane 3.4 2.5 0.63 ug/l
75-35-4 1,1-Dichloroethylene ND 2.5 0.63 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 2.5 0.63 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 2.5 0.63 ug/l
78-87-5 1,2-Dichloropropane ND 2.5 0.63 ug/l
142-28-9 1,3-Dichloropropane ND 2.5 0.63 ug/l
594-20-7 2,2-Dichloropropane ND 2.5 0.63 ug/l
563-58-6 1,1-Dichloropropene ND 2.5 0.63 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 2.5 0.63 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 2.5 0.63 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
7 of 34
FA3783333.1
SGS Accutest
Report of Analysis Page 2 of 2
Client Sample ID:MW-8
Lab Sample ID:FA37833-1 Date Sampled:10/13/16
Matrix:AQ - Ground Water Date Received:10/17/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 5.4 2.5 0.63 ug/l
100-41-4 Ethylbenzene 14.0 2.5 0.63 ug/l
87-68-3 Hexachlorobutadiene ND 2.5 0.63 ug/l
98-82-8 Isopropylbenzene 6.4 2.5 0.63 ug/l
99-87-6 p-Isopropyltoluene 3.9 2.5 0.63 ug/l
74-83-9 Methyl Bromide ND 2.5 1.0 ug/l
74-87-3 Methyl Chloride ND 2.5 1.0 ug/l
74-95-3 Methylene Bromide ND 2.5 0.63 ug/l
75-09-2 Methylene Chloride ND 10 5.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 14.8 2.5 0.63 ug/l
91-20-3 Naphthalene 101 2.5 0.63 ug/l
103-65-1 n-Propylbenzene 7.7 2.5 0.63 ug/l
100-42-5 Styrene ND 2.5 0.63 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 2.5 0.63 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 2.5 0.63 ug/l
127-18-4 Tetrachloroethylene 1.3 2.5 0.63 ug/l J
108-88-3 Toluene 2.9 2.5 0.63 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 2.5 0.63 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 2.5 0.63 ug/l
71-55-6 1,1,1-Trichloroethane ND 2.5 0.63 ug/l
79-00-5 1,1,2-Trichloroethane ND 2.5 0.63 ug/l
79-01-6 Trichloroethylene ND 2.5 0.63 ug/l
75-69-4 Trichlorofluoromethane ND 2.5 1.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.5 0.70 ug/l
95-63-6 1,2,4-Trimethylbenzene 61.1 2.5 0.63 ug/l
108-67-8 1,3,5-Trimethylbenzene 15.8 2.5 0.63 ug/l
75-01-4 Vinyl Chloride ND 2.5 0.63 ug/l
m,p-Xylene 31.0 5.0 0.92 ug/l
95-47-6 o-Xylene 6.8 2.5 0.63 ug/l
1330-20-7 Xylene (total)37.7 7.5 1.5 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
8 of 34
FA3783333.1
SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID:MW-7
Lab Sample ID:FA37833-2 Date Sampled:10/13/16
Matrix:AQ - Ground Water Date Received:10/17/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E048731.D 500 10/18/16 MM n/a n/a VE1615
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 8660 250 63 ug/l
108-86-1 Bromobenzene ND 250 63 ug/l
74-97-5 Bromochloromethane ND 250 63 ug/l
75-27-4 Bromodichloromethane ND 250 63 ug/l
75-25-2 Bromoform ND 250 63 ug/l
104-51-8 n-Butylbenzene 190 250 63 ug/l J
135-98-8 sec-Butylbenzene 95.6 250 63 ug/l J
98-06-6 tert-Butylbenzene ND 250 63 ug/l
56-23-5 Carbon Tetrachloride ND 250 63 ug/l
108-90-7 Chlorobenzene ND 250 63 ug/l
75-00-3 Chloroethane ND 250 100 ug/l
67-66-3 Chloroform ND 250 63 ug/l
95-49-8 o-Chlorotoluene ND 250 63 ug/l
106-43-4 p-Chlorotoluene ND 250 63 ug/l
124-48-1 Dibromochloromethane ND 250 63 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 250 140 ug/l
106-93-4 1,2-Dibromoethane 92.6 250 63 ug/l J
75-71-8 Dichlorodifluoromethane ND 250 100 ug/l
95-50-1 1,2-Dichlorobenzene ND 250 63 ug/l
541-73-1 1,3-Dichlorobenzene ND 250 63 ug/l
106-46-7 1,4-Dichlorobenzene ND 250 63 ug/l
75-34-3 1,1-Dichloroethane ND 250 63 ug/l
107-06-2 1,2-Dichloroethane 215 250 63 ug/l J
75-35-4 1,1-Dichloroethylene ND 250 63 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 250 63 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 250 63 ug/l
78-87-5 1,2-Dichloropropane ND 250 63 ug/l
142-28-9 1,3-Dichloropropane ND 250 63 ug/l
594-20-7 2,2-Dichloropropane ND 250 63 ug/l
563-58-6 1,1-Dichloropropene ND 250 63 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 250 63 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 250 63 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
9 of 34
FA3783333.2
SGS Accutest
Report of Analysis Page 2 of 2
Client Sample ID:MW-7
Lab Sample ID:FA37833-2 Date Sampled:10/13/16
Matrix:AQ - Ground Water Date Received:10/17/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 167 250 63 ug/l J
100-41-4 Ethylbenzene 3790 250 63 ug/l
87-68-3 Hexachlorobutadiene ND 250 63 ug/l
98-82-8 Isopropylbenzene 221 250 63 ug/l J
99-87-6 p-Isopropyltoluene ND 250 63 ug/l
74-83-9 Methyl Bromide ND 250 100 ug/l
74-87-3 Methyl Chloride ND 250 100 ug/l
74-95-3 Methylene Bromide ND 250 63 ug/l
75-09-2 Methylene Chloride ND 1000 500 ug/l
1634-04-4 Methyl Tert Butyl Ether 3770 250 63 ug/l
91-20-3 Naphthalene 2080 250 63 ug/l
103-65-1 n-Propylbenzene 918 250 63 ug/l
100-42-5 Styrene 100 250 63 ug/l J
630-20-6 1,1,1,2-Tetrachloroethane ND 250 63 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 250 63 ug/l
127-18-4 Tetrachloroethylene ND 250 63 ug/l
108-88-3 Toluene 24600 250 63 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 250 63 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 250 63 ug/l
71-55-6 1,1,1-Trichloroethane ND 250 63 ug/l
79-00-5 1,1,2-Trichloroethane ND 250 63 ug/l
79-01-6 Trichloroethylene ND 250 63 ug/l
75-69-4 Trichlorofluoromethane ND 250 100 ug/l
96-18-4 1,2,3-Trichloropropane ND 250 70 ug/l
95-63-6 1,2,4-Trimethylbenzene 7440 250 63 ug/l
108-67-8 1,3,5-Trimethylbenzene 2140 250 63 ug/l
75-01-4 Vinyl Chloride ND 250 63 ug/l
m,p-Xylene 15300 500 92 ug/l
95-47-6 o-Xylene 6760 250 63 ug/l
1330-20-7 Xylene (total)22100 750 150 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 34
FA3783333.2
SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID:MW-2
Lab Sample ID:FA37833-3 Date Sampled:10/13/16
Matrix:AQ - Ground Water Date Received:10/17/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E048808.D 50 10/21/16 MM n/a n/a VE1618
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 2400 25 6.3 ug/l
108-86-1 Bromobenzene ND 25 6.3 ug/l
74-97-5 Bromochloromethane ND 25 6.3 ug/l
75-27-4 Bromodichloromethane ND 25 6.3 ug/l
75-25-2 Bromoform ND 25 6.3 ug/l
104-51-8 n-Butylbenzene ND 25 6.3 ug/l
135-98-8 sec-Butylbenzene ND 25 6.3 ug/l
98-06-6 tert-Butylbenzene ND 25 6.3 ug/l
56-23-5 Carbon Tetrachloride ND 25 6.3 ug/l
108-90-7 Chlorobenzene ND 25 6.3 ug/l
75-00-3 Chloroethane ND 25 10 ug/l
67-66-3 Chloroform ND 25 6.3 ug/l
95-49-8 o-Chlorotoluene ND 25 6.3 ug/l
106-43-4 p-Chlorotoluene ND 25 6.3 ug/l
124-48-1 Dibromochloromethane ND 25 6.3 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 25 14 ug/l
106-93-4 1,2-Dibromoethane ND 25 6.3 ug/l
75-71-8 Dichlorodifluoromethane ND 25 10 ug/l
95-50-1 1,2-Dichlorobenzene ND 25 6.3 ug/l
541-73-1 1,3-Dichlorobenzene ND 25 6.3 ug/l
106-46-7 1,4-Dichlorobenzene ND 25 6.3 ug/l
75-34-3 1,1-Dichloroethane ND 25 6.3 ug/l
107-06-2 1,2-Dichloroethane 7.1 25 6.3 ug/l J
75-35-4 1,1-Dichloroethylene ND 25 6.3 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 25 6.3 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 25 6.3 ug/l
78-87-5 1,2-Dichloropropane ND 25 6.3 ug/l
142-28-9 1,3-Dichloropropane ND 25 6.3 ug/l
594-20-7 2,2-Dichloropropane ND 25 6.3 ug/l
563-58-6 1,1-Dichloropropene ND 25 6.3 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 25 6.3 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 25 6.3 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 34
FA3783333.3
SGS Accutest
Report of Analysis Page 2 of 2
Client Sample ID:MW-2
Lab Sample ID:FA37833-3 Date Sampled:10/13/16
Matrix:AQ - Ground Water Date Received:10/17/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 31.8 25 6.3 ug/l
100-41-4 Ethylbenzene 198 25 6.3 ug/l
87-68-3 Hexachlorobutadiene ND 25 6.3 ug/l
98-82-8 Isopropylbenzene 13.2 25 6.3 ug/l J
99-87-6 p-Isopropyltoluene ND 25 6.3 ug/l
74-83-9 Methyl Bromide ND 25 10 ug/l
74-87-3 Methyl Chloride ND 25 10 ug/l
74-95-3 Methylene Bromide ND 25 6.3 ug/l
75-09-2 Methylene Chloride ND 100 50 ug/l
1634-04-4 Methyl Tert Butyl Ether 781 25 6.3 ug/l
91-20-3 Naphthalene 154 25 6.3 ug/l
103-65-1 n-Propylbenzene 30.5 25 6.3 ug/l
100-42-5 Styrene ND 25 6.3 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 25 6.3 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 25 6.3 ug/l
127-18-4 Tetrachloroethylene ND 25 6.3 ug/l
108-88-3 Toluene 921 25 6.3 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 25 6.3 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 25 6.3 ug/l
71-55-6 1,1,1-Trichloroethane ND 25 6.3 ug/l
79-00-5 1,1,2-Trichloroethane ND 25 6.3 ug/l
79-01-6 Trichloroethylene ND 25 6.3 ug/l
75-69-4 Trichlorofluoromethane ND 25 10 ug/l
96-18-4 1,2,3-Trichloropropane ND 25 7.0 ug/l
95-63-6 1,2,4-Trimethylbenzene 264 25 6.3 ug/l
108-67-8 1,3,5-Trimethylbenzene 76.2 25 6.3 ug/l
75-01-4 Vinyl Chloride ND 25 6.3 ug/l
m,p-Xylene 1090 50 9.2 ug/l
95-47-6 o-Xylene 175 25 6.3 ug/l
1330-20-7 Xylene (total)1260 75 15 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 97%70-130%
17060-07-0 1,2-Dichloroethane-D4 97%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 34
FA3783333.3
SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID:MW-1A
Lab Sample ID:FA37833-4 Date Sampled:10/13/16
Matrix:AQ - Ground Water Date Received:10/17/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E048733.D 1 10/18/16 MM n/a n/a VE1615
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.29 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
13 of 34
FA3783333.4
SGS Accutest
Report of Analysis Page 2 of 2
Client Sample ID:MW-1A
Lab Sample ID:FA37833-4 Date Sampled:10/13/16
Matrix:AQ - Ground Water Date Received:10/17/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene 0.39 0.50 0.13 ug/l J
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.14 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 0.23 1.0 0.18 ug/l J
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.31 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
14 of 34
FA3783333.4
SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID:MW-9
Lab Sample ID:FA37833-5 Date Sampled:10/13/16
Matrix:AQ - Ground Water Date Received:10/17/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E048734.D 10 10/18/16 MM n/a n/a VE1615
Run #2 E048809.D 20 10/21/16 MM n/a n/a VE1618
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 123 5.0 1.3 ug/l
108-86-1 Bromobenzene ND 5.0 1.3 ug/l
74-97-5 Bromochloromethane ND 5.0 1.3 ug/l
75-27-4 Bromodichloromethane ND 5.0 1.3 ug/l
75-25-2 Bromoform ND 5.0 1.3 ug/l
104-51-8 n-Butylbenzene 33.3 5.0 1.3 ug/l
135-98-8 sec-Butylbenzene 15.6 5.0 1.3 ug/l
98-06-6 tert-Butylbenzene ND 5.0 1.3 ug/l
56-23-5 Carbon Tetrachloride ND 5.0 1.3 ug/l
108-90-7 Chlorobenzene ND 5.0 1.3 ug/l
75-00-3 Chloroethane 8.7 5.0 2.0 ug/l
67-66-3 Chloroform ND 5.0 1.3 ug/l
95-49-8 o-Chlorotoluene ND 5.0 1.3 ug/l
106-43-4 p-Chlorotoluene ND 5.0 1.3 ug/l
124-48-1 Dibromochloromethane ND 5.0 1.3 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 5.0 2.9 ug/l
106-93-4 1,2-Dibromoethane ND 5.0 1.3 ug/l
75-71-8 Dichlorodifluoromethane ND 5.0 2.0 ug/l
95-50-1 1,2-Dichlorobenzene ND 5.0 1.3 ug/l
541-73-1 1,3-Dichlorobenzene ND 5.0 1.3 ug/l
106-46-7 1,4-Dichlorobenzene ND 5.0 1.3 ug/l
75-34-3 1,1-Dichloroethane ND 5.0 1.3 ug/l
107-06-2 1,2-Dichloroethane 4.2 5.0 1.3 ug/l J
75-35-4 1,1-Dichloroethylene ND 5.0 1.3 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.3 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.3 ug/l
78-87-5 1,2-Dichloropropane ND 5.0 1.3 ug/l
142-28-9 1,3-Dichloropropane ND 5.0 1.3 ug/l
594-20-7 2,2-Dichloropropane ND 5.0 1.3 ug/l
563-58-6 1,1-Dichloropropene ND 5.0 1.3 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.3 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.3 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
15 of 34
FA3783333.5
SGS Accutest
Report of Analysis Page 2 of 2
Client Sample ID:MW-9
Lab Sample ID:FA37833-5 Date Sampled:10/13/16
Matrix:AQ - Ground Water Date Received:10/17/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 6.0 5.0 1.3 ug/l
100-41-4 Ethylbenzene 146 5.0 1.3 ug/l
87-68-3 Hexachlorobutadiene ND 5.0 1.3 ug/l
98-82-8 Isopropylbenzene 36.8 5.0 1.3 ug/l
99-87-6 p-Isopropyltoluene 9.1 5.0 1.3 ug/l
74-83-9 Methyl Bromide ND 5.0 2.0 ug/l
74-87-3 Methyl Chloride 3.5 5.0 2.0 ug/l J
74-95-3 Methylene Bromide ND 5.0 1.3 ug/l
75-09-2 Methylene Chloride ND 20 10 ug/l
1634-04-4 Methyl Tert Butyl Ether 12.1 5.0 1.3 ug/l
91-20-3 Naphthalene 113 5.0 1.3 ug/l
103-65-1 n-Propylbenzene 170 5.0 1.3 ug/l
100-42-5 Styrene 1.8 5.0 1.3 ug/l J
630-20-6 1,1,1,2-Tetrachloroethane ND 5.0 1.3 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 1.3 ug/l
127-18-4 Tetrachloroethylene ND 5.0 1.3 ug/l
108-88-3 Toluene 22.6 5.0 1.3 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 5.0 1.3 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.3 ug/l
71-55-6 1,1,1-Trichloroethane ND 5.0 1.3 ug/l
79-00-5 1,1,2-Trichloroethane ND 5.0 1.3 ug/l
79-01-6 Trichloroethylene ND 5.0 1.3 ug/l
75-69-4 Trichlorofluoromethane ND 5.0 2.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 5.0 1.4 ug/l
95-63-6 1,2,4-Trimethylbenzene a 1010 b 10 2.5 ug/l E
108-67-8 1,3,5-Trimethylbenzene 290 5.0 1.3 ug/l
75-01-4 Vinyl Chloride ND 5.0 1.3 ug/l
m,p-Xylene 264 10 1.8 ug/l
95-47-6 o-Xylene 61.5 5.0 1.3 ug/l
1330-20-7 Xylene (total)326 15 3.1 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%99%70-130%
17060-07-0 1,2-Dichloroethane-D4 108%98%70-130%
2037-26-5 Toluene-D8 100%99%70-130%
460-00-4 4-Bromofluorobenzene 102%100%70-130%
(a) No sample available for reanalysis.
(b) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
16 of 34
FA3783333.5
SGS Accutest
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Southeast
Section 4
17 of 34
FA378334
FA37833: Chain of Custody
Page 1 of 3
18 of 34
FA3783344.1
FA37833: Chain of Custody
Page 2 of 3
19 of 34
FA3783344.1
FA37833: Chain of Custody
Page 3 of 3
20 of 34
FA3783344.1
SGS Accutest
GC/MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Southeast
Section 5
21 of 34
FA378335
Method Blank Summary Page 1 of 2
Job Number:FA37833
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1615-MB E048717.D 1 10/18/16 MM n/a n/a VE1615
The QC reported here applies to the following samples:Method: SM 6200B
FA37833-2, FA37833-4, FA37833-5
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.29 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
22 of 34
FA3783355.1.1
Method Blank Summary Page 2 of 2
Job Number:FA37833
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1615-MB E048717.D 1 10/18/16 MM n/a n/a VE1615
The QC reported here applies to the following samples:Method: SM 6200B
FA37833-2, FA37833-4, FA37833-5
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.14 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.18 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.31 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%70-130%
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 103%70-130%
23 of 34
FA3783355.1.1
Method Blank Summary Page 1 of 2
Job Number:FA37833
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1618-MB E048800.D 1 10/21/16 MM n/a n/a VE1618
The QC reported here applies to the following samples:Method: SM 6200B
FA37833-1, FA37833-3, FA37833-5
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.29 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
24 of 34
FA3783355.1.2
Method Blank Summary Page 2 of 2
Job Number:FA37833
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1618-MB E048800.D 1 10/21/16 MM n/a n/a VE1618
The QC reported here applies to the following samples:Method: SM 6200B
FA37833-1, FA37833-3, FA37833-5
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.14 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.18 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.31 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
25 of 34
FA3783355.1.2
Blank Spike Summary Page 1 of 2
Job Number:FA37833
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1615-BS E048716.D 1 10/18/16 MM n/a n/a VE1615
The QC reported here applies to the following samples:Method: SM 6200B
FA37833-2, FA37833-4, FA37833-5
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 9.6 96 70-130
108-86-1 Bromobenzene 10 10.1 101 70-130
74-97-5 Bromochloromethane 10 9.7 97 70-130
75-27-4 Bromodichloromethane 10 9.9 99 70-130
75-25-2 Bromoform 10 8.8 88 70-130
104-51-8 n-Butylbenzene 10 9.9 99 70-130
135-98-8 sec-Butylbenzene 10 11.2 112 70-130
98-06-6 tert-Butylbenzene 10 10.1 101 70-130
56-23-5 Carbon Tetrachloride 10 9.1 91 70-130
108-90-7 Chlorobenzene 10 10.4 104 70-130
75-00-3 Chloroethane 10 10.5 105 60-140
67-66-3 Chloroform 10 9.8 98 70-130
95-49-8 o-Chlorotoluene 10 10.7 107 70-130
106-43-4 p-Chlorotoluene 10 10.6 106 70-130
124-48-1 Dibromochloromethane 10 10.0 100 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 9.4 94 70-130
106-93-4 1,2-Dibromoethane 10 9.9 99 70-130
75-71-8 Dichlorodifluoromethane 10 13.0 130 60-140
95-50-1 1,2-Dichlorobenzene 10 10.2 102 70-130
541-73-1 1,3-Dichlorobenzene 10 10.5 105 70-130
106-46-7 1,4-Dichlorobenzene 10 10 100 70-130
75-34-3 1,1-Dichloroethane 10 10.1 101 70-130
107-06-2 1,2-Dichloroethane 10 10.1 101 70-130
75-35-4 1,1-Dichloroethylene 10 10.3 103 70-130
156-59-2 cis-1,2-Dichloroethylene 10 9.5 95 70-130
156-60-5 trans-1,2-Dichloroethylene 10 10.8 108 70-130
78-87-5 1,2-Dichloropropane 10 9.3 93 70-130
142-28-9 1,3-Dichloropropane 10 9.2 92 70-130
594-20-7 2,2-Dichloropropane 10 10.2 102 70-130
563-58-6 1,1-Dichloropropene 10 9.9 99 70-130
10061-01-5 cis-1,3-Dichloropropene 10 9.9 99 70-130
10061-02-6 trans-1,3-Dichloropropene 10 9.9 99 70-130
108-20-3 Di-Isopropyl Ether 10 9.5 95 70-130
100-41-4 Ethylbenzene 10 10.0 100 70-130
87-68-3 Hexachlorobutadiene 10 10.6 106 70-130
98-82-8 Isopropylbenzene 10 10.3 103 70-130
* = Outside of Control Limits.
26 of 34
FA3783355.2.1
Blank Spike Summary Page 2 of 2
Job Number:FA37833
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1615-BS E048716.D 1 10/18/16 MM n/a n/a VE1615
The QC reported here applies to the following samples:Method: SM 6200B
FA37833-2, FA37833-4, FA37833-5
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 10.4 104 70-130
74-83-9 Methyl Bromide 10 12.2 122 60-140
74-87-3 Methyl Chloride 10 10.5 105 60-140
74-95-3 Methylene Bromide 10 9.8 98 70-130
75-09-2 Methylene Chloride 10 9.8 98 70-130
1634-04-4 Methyl Tert Butyl Ether 10 9.7 97 70-130
91-20-3 Naphthalene 10 10.7 107 70-130
103-65-1 n-Propylbenzene 10 10.9 109 70-130
100-42-5 Styrene 10 9.4 94 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 10.1 101 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 9.3 93 70-130
127-18-4 Tetrachloroethylene 10 10.4 104 70-130
108-88-3 Toluene 10 9.8 98 70-130
87-61-6 1,2,3-Trichlorobenzene 10 9.9 99 70-130
120-82-1 1,2,4-Trichlorobenzene 10 10.2 102 70-130
71-55-6 1,1,1-Trichloroethane 10 9.6 96 70-130
79-00-5 1,1,2-Trichloroethane 10 9.5 95 70-130
79-01-6 Trichloroethylene 10 9.8 98 70-130
75-69-4 Trichlorofluoromethane 10 10.9 109 60-140
96-18-4 1,2,3-Trichloropropane 10 9.8 98 70-130
95-63-6 1,2,4-Trimethylbenzene 10 10.2 102 70-130
108-67-8 1,3,5-Trimethylbenzene 10 10.7 107 70-130
75-01-4 Vinyl Chloride 10 11.4 114 60-140
m,p-Xylene 20 21.2 106 70-130
95-47-6 o-Xylene 10 9.7 97 70-130
1330-20-7 Xylene (total)30 30.9 103 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 107%70-130%
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
* = Outside of Control Limits.
27 of 34
FA3783355.2.1
Blank Spike Summary Page 1 of 2
Job Number:FA37833
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1618-BS E048799.D 1 10/21/16 MM n/a n/a VE1618
The QC reported here applies to the following samples:Method: SM 6200B
FA37833-1, FA37833-3, FA37833-5
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 10.4 104 70-130
108-86-1 Bromobenzene 10 10.1 101 70-130
74-97-5 Bromochloromethane 10 10.4 104 70-130
75-27-4 Bromodichloromethane 10 10.3 103 70-130
75-25-2 Bromoform 10 9.3 93 70-130
104-51-8 n-Butylbenzene 10 10.5 105 70-130
135-98-8 sec-Butylbenzene 10 11.4 114 70-130
98-06-6 tert-Butylbenzene 10 10.3 103 70-130
56-23-5 Carbon Tetrachloride 10 11.3 113 70-130
108-90-7 Chlorobenzene 10 10.8 108 70-130
75-00-3 Chloroethane 10 10.7 107 60-140
67-66-3 Chloroform 10 10.4 104 70-130
95-49-8 o-Chlorotoluene 10 10.7 107 70-130
106-43-4 p-Chlorotoluene 10 10.5 105 70-130
124-48-1 Dibromochloromethane 10 9.6 96 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 9.2 92 70-130
106-93-4 1,2-Dibromoethane 10 10.1 101 70-130
75-71-8 Dichlorodifluoromethane 10 8.0 80 60-140
95-50-1 1,2-Dichlorobenzene 10 10.3 103 70-130
541-73-1 1,3-Dichlorobenzene 10 10.5 105 70-130
106-46-7 1,4-Dichlorobenzene 10 10.2 102 70-130
75-34-3 1,1-Dichloroethane 10 11.0 110 70-130
107-06-2 1,2-Dichloroethane 10 10 100 70-130
75-35-4 1,1-Dichloroethylene 10 11.8 118 70-130
156-59-2 cis-1,2-Dichloroethylene 10 10.2 102 70-130
156-60-5 trans-1,2-Dichloroethylene 10 11.9 119 70-130
78-87-5 1,2-Dichloropropane 10 9.9 99 70-130
142-28-9 1,3-Dichloropropane 10 9.3 93 70-130
594-20-7 2,2-Dichloropropane 10 11.3 113 70-130
563-58-6 1,1-Dichloropropene 10 10.7 107 70-130
10061-01-5 cis-1,3-Dichloropropene 10 9.6 96 70-130
10061-02-6 trans-1,3-Dichloropropene 10 10.3 103 70-130
108-20-3 Di-Isopropyl Ether 10 10.3 103 70-130
100-41-4 Ethylbenzene 10 10.4 104 70-130
87-68-3 Hexachlorobutadiene 10 11.0 110 70-130
98-82-8 Isopropylbenzene 10 10.7 107 70-130
* = Outside of Control Limits.
28 of 34
FA3783355.2.2
Blank Spike Summary Page 2 of 2
Job Number:FA37833
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1618-BS E048799.D 1 10/21/16 MM n/a n/a VE1618
The QC reported here applies to the following samples:Method: SM 6200B
FA37833-1, FA37833-3, FA37833-5
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 10.7 107 70-130
74-83-9 Methyl Bromide 10 10.7 107 60-140
74-87-3 Methyl Chloride 10 9.4 94 60-140
74-95-3 Methylene Bromide 10 10.1 101 70-130
75-09-2 Methylene Chloride 10 10.7 107 70-130
1634-04-4 Methyl Tert Butyl Ether 10 9.9 99 70-130
91-20-3 Naphthalene 10 9.9 99 70-130
103-65-1 n-Propylbenzene 10 11.1 111 70-130
100-42-5 Styrene 10 9.7 97 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 10.6 106 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 9.5 95 70-130
127-18-4 Tetrachloroethylene 10 11.0 110 70-130
108-88-3 Toluene 10 10.4 104 70-130
87-61-6 1,2,3-Trichlorobenzene 10 10.2 102 70-130
120-82-1 1,2,4-Trichlorobenzene 10 10.2 102 70-130
71-55-6 1,1,1-Trichloroethane 10 10.6 106 70-130
79-00-5 1,1,2-Trichloroethane 10 9.9 99 70-130
79-01-6 Trichloroethylene 10 10.7 107 70-130
75-69-4 Trichlorofluoromethane 10 10.5 105 60-140
96-18-4 1,2,3-Trichloropropane 10 9.9 99 70-130
95-63-6 1,2,4-Trimethylbenzene 10 10.3 103 70-130
108-67-8 1,3,5-Trimethylbenzene 10 10.7 107 70-130
75-01-4 Vinyl Chloride 10 10.5 105 60-140
m,p-Xylene 20 21.7 109 70-130
95-47-6 o-Xylene 10 10.0 100 70-130
1330-20-7 Xylene (total)30 31.7 106 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
* = Outside of Control Limits.
29 of 34
FA3783355.2.2
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA37833
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA37775-1MS E048738.D 1 10/18/16 MM n/a n/a VE1615
FA37775-1MSD E048739.D 1 10/18/16 MM n/a n/a VE1615
FA37775-1 E048718.D 1 10/18/16 MM n/a n/a VE1615
The QC reported here applies to the following samples:Method: SM 6200B
FA37833-2, FA37833-4, FA37833-5
FA37775-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene ND 10 9.7 97 10 9.3 93 4 70-130/20
108-86-1 Bromobenzene ND 10 10.8 108 10 9.3 93 15 70-130/20
74-97-5 Bromochloromethane ND 10 9.7 97 10 9.4 94 3 70-130/20
75-27-4 Bromodichloromethane ND 10 9.1 91 10 8.5 85 7 70-130/20
75-25-2 Bromoform ND 10 6.2 62*10 6.0 60*3 70-130/20
104-51-8 n-Butylbenzene ND 10 9.9 99 10 8.9 89 11 70-130/20
135-98-8 sec-Butylbenzene ND 10 11.6 116 10 10.2 102 13 70-130/20
98-06-6 tert-Butylbenzene ND 10 10.4 104 10 9.1 91 13 70-130/20
56-23-5 Carbon Tetrachloride ND 10 8.6 86 10 7.6 76 12 70-130/20
108-90-7 Chlorobenzene ND 10 10.6 106 10 9.9 99 7 70-130/20
75-00-3 Chloroethane ND 10 9.3 93 10 9.0 90 3 60-140/20
67-66-3 Chloroform 0.18 J 10 9.8 96 10 9.4 92 4 70-130/20
95-49-8 o-Chlorotoluene ND 10 11.1 111 10 9.7 97 13 70-130/20
106-43-4 p-Chlorotoluene ND 10 11.0 110 10 9.7 97 13 70-130/20
124-48-1 Dibromochloromethane ND 10 8.3 83 10 7.8 78 6 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 10 9.7 97 10 8.8 88 10 70-130/20
106-93-4 1,2-Dibromoethane ND 10 10.0 100 10 9.5 95 5 70-130/20
75-71-8 Dichlorodifluoromethane ND 10 11.8 118 10 11.3 113 4 60-140/20
95-50-1 1,2-Dichlorobenzene ND 10 10.6 106 10 9.4 94 12 70-130/20
541-73-1 1,3-Dichlorobenzene ND 10 10.6 106 10 9.5 95 11 70-130/20
106-46-7 1,4-Dichlorobenzene ND 10 10.3 103 10 9.1 91 12 70-130/20
75-34-3 1,1-Dichloroethane ND 10 10.3 103 10 9.7 97 6 70-130/20
107-06-2 1,2-Dichloroethane ND 10 9.7 97 10 9.3 93 4 70-130/20
75-35-4 1,1-Dichloroethylene ND 10 10 100 10 9.5 95 5 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 10 9.8 98 10 9.3 93 5 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 10 10.8 108 10 10.2 102 6 70-130/20
78-87-5 1,2-Dichloropropane ND 10 9.7 97 10 9.1 91 6 70-130/20
142-28-9 1,3-Dichloropropane ND 10 9.3 93 10 8.9 89 4 70-130/20
594-20-7 2,2-Dichloropropane ND 10 9.2 92 10 8.7 87 6 70-130/20
563-58-6 1,1-Dichloropropene ND 10 9.9 99 10 9.2 92 7 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 10 8.9 89 10 8.1 81 9 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 10 8.8 88 10 8.0 80 10 70-130/20
108-20-3 Di-Isopropyl Ether ND 10 9.5 95 10 9.3 93 2 70-130/20
100-41-4 Ethylbenzene ND 10 10.3 103 10 9.7 97 6 70-130/20
87-68-3 Hexachlorobutadiene ND 10 10.2 102 10 9.4 94 8 70-130/20
98-82-8 Isopropylbenzene ND 10 10.5 105 10 9.7 97 8 70-130/20
* = Outside of Control Limits.
30 of 34
FA3783355.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA37833
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA37775-1MS E048738.D 1 10/18/16 MM n/a n/a VE1615
FA37775-1MSD E048739.D 1 10/18/16 MM n/a n/a VE1615
FA37775-1 E048718.D 1 10/18/16 MM n/a n/a VE1615
The QC reported here applies to the following samples:Method: SM 6200B
FA37833-2, FA37833-4, FA37833-5
FA37775-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 10 10.6 106 10 9.3 93 13 70-130/20
74-83-9 Methyl Bromide ND 10 11.5 115 10 11.5 115 0 60-140/20
74-87-3 Methyl Chloride ND 10 9.8 98 10 9.6 96 2 60-140/20
74-95-3 Methylene Bromide ND 10 9.8 98 10 9.4 94 4 70-130/20
75-09-2 Methylene Chloride ND 10 9.5 95 10 9.3 93 2 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 10 9.7 97 10 9.5 95 2 70-130/20
91-20-3 Naphthalene ND 10 12.2 122 10 11.0 110 10 70-130/20
103-65-1 n-Propylbenzene ND 10 11.4 114 10 9.9 99 14 70-130/20
100-42-5 Styrene ND 10 9.2 92 10 8.8 88 4 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 10 10.3 103 10 9.4 94 9 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 10 9.9 99 10 8.9 89 11 70-130/20
127-18-4 Tetrachloroethylene ND 10 10.4 104 10 9.5 95 9 70-130/20
108-88-3 Toluene ND 10 10.2 102 10 9.4 94 8 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 10 10.1 101 10 9.7 97 4 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 10 10.3 103 10 9.8 98 5 70-130/20
71-55-6 1,1,1-Trichloroethane ND 10 9.5 95 10 8.9 89 7 70-130/20
79-00-5 1,1,2-Trichloroethane ND 10 9.8 98 10 9.2 92 6 70-130/20
79-01-6 Trichloroethylene ND 10 9.8 98 10 9.2 92 6 70-130/20
75-69-4 Trichlorofluoromethane ND 10 9.9 99 10 9.4 94 5 60-140/20
96-18-4 1,2,3-Trichloropropane ND 10 10.1 101 10 9.2 92 9 70-130/20
95-63-6 1,2,4-Trimethylbenzene ND 10 10.4 104 10 9.3 93 11 70-130/20
108-67-8 1,3,5-Trimethylbenzene ND 10 11.1 111 10 9.9 99 11 70-130/20
75-01-4 Vinyl Chloride ND 10 10.2 102 10 10.2 102 0 60-140/20
m,p-Xylene ND 20 21.7 109 20 20.1 101 8 70-130/20
95-47-6 o-Xylene ND 10 10 100 10 9.4 94 6 70-130/20
1330-20-7 Xylene (total)ND 30 31.6 105 30 29.4 98 7 70-130/20
CAS No.Surrogate Recoveries MS MSD FA37775-1 Limits
1868-53-7 Dibromofluoromethane 98%100%101%70-130%
17060-07-0 1,2-Dichloroethane-D4 101%105%107%70-130%
2037-26-5 Toluene-D8 101%100%101%70-130%
460-00-4 4-Bromofluorobenzene 104%101%102%70-130%
* = Outside of Control Limits.
31 of 34
FA3783355.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3
Job Number:FA37833
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA37889-9MS E048823.D 100 10/21/16 MM n/a n/a VE1618
FA37889-9MSD E048824.D 100 10/21/16 MM n/a n/a VE1618
FA37889-9 a E048818.D 100 10/21/16 MM n/a n/a VE1618
The QC reported here applies to the following samples:Method: SM 6200B
FA37833-1, FA37833-3, FA37833-5
FA37889-9 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 898 1000 1840 94 1000 1730 83 6 70-130/20
108-86-1 Bromobenzene ND 1000 1010 101 1000 888 89 13 70-130/20
74-97-5 Bromochloromethane ND 1000 974 97 1000 922 92 5 70-130/20
75-27-4 Bromodichloromethane ND 1000 985 99 1000 930 93 6 70-130/20
75-25-2 Bromoform ND 1000 891 89 1000 814 81 9 70-130/20
104-51-8 n-Butylbenzene ND 1000 978 98 1000 864 86 12 70-130/20
135-98-8 sec-Butylbenzene ND 1000 1120 112 1000 984 98 13 70-130/20
98-06-6 tert-Butylbenzene ND 1000 997 100 1000 877 88 13 70-130/20
56-23-5 Carbon Tetrachloride ND 1000 1070 107 1000 978 98 9 70-130/20
108-90-7 Chlorobenzene ND 1000 964 96 1000 896 90 7 70-130/20
75-00-3 Chloroethane ND 1000 1030 103 1000 893 89 14 60-140/20
67-66-3 Chloroform ND 1000 985 99 1000 930 93 6 70-130/20
95-49-8 o-Chlorotoluene ND 1000 1090 109 1000 948 95 14 70-130/20
106-43-4 p-Chlorotoluene ND 1000 1040 104 1000 901 90 14 70-130/20
124-48-1 Dibromochloromethane ND 1000 918 92 1000 847 85 8 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 1000 940 94 1000 828 83 13 70-130/20
106-93-4 1,2-Dibromoethane ND 1000 963 96 1000 924 92 4 70-130/20
75-71-8 Dichlorodifluoromethane ND 1000 731 73 1000 675 68 8 60-140/20
95-50-1 1,2-Dichlorobenzene ND 1000 997 100 1000 885 89 12 70-130/20
541-73-1 1,3-Dichlorobenzene ND 1000 1020 102 1000 906 91 12 70-130/20
106-46-7 1,4-Dichlorobenzene ND 1000 997 100 1000 871 87 13 70-130/20
75-34-3 1,1-Dichloroethane ND 1000 1040 104 1000 980 98 6 70-130/20
107-06-2 1,2-Dichloroethane ND 1000 949 95 1000 903 90 5 70-130/20
75-35-4 1,1-Dichloroethylene ND 1000 1080 108 1000 1020 102 6 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 1000 957 96 1000 913 91 5 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 1000 1120 112 1000 1050 105 6 70-130/20
78-87-5 1,2-Dichloropropane ND 1000 948 95 1000 903 90 5 70-130/20
142-28-9 1,3-Dichloropropane ND 1000 900 90 1000 845 85 6 70-130/20
594-20-7 2,2-Dichloropropane ND 1000 990 99 1000 909 91 9 70-130/20
563-58-6 1,1-Dichloropropene ND 1000 1020 102 1000 943 94 8 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 1000 894 89 1000 864 86 3 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 1000 969 97 1000 905 91 7 70-130/20
108-20-3 Di-Isopropyl Ether ND 1000 980 98 1000 941 94 4 70-130/20
100-41-4 Ethylbenzene 877 1000 1830 95 1000 1710 83 7 70-130/20
87-68-3 Hexachlorobutadiene ND 1000 997 100 1000 913 91 9 70-130/20
98-82-8 Isopropylbenzene 36.5 J 1000 1040 100 1000 958 92 8 70-130/20
* = Outside of Control Limits.
32 of 34
FA3783355.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3
Job Number:FA37833
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA37889-9MS E048823.D 100 10/21/16 MM n/a n/a VE1618
FA37889-9MSD E048824.D 100 10/21/16 MM n/a n/a VE1618
FA37889-9 a E048818.D 100 10/21/16 MM n/a n/a VE1618
The QC reported here applies to the following samples:Method: SM 6200B
FA37833-1, FA37833-3, FA37833-5
FA37889-9 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 1000 998 100 1000 881 88 12 70-130/20
74-83-9 Methyl Bromide ND 1000 956 96 1000 881 88 8 60-140/20
74-87-3 Methyl Chloride ND 1000 871 87 1000 813 81 7 60-140/20
74-95-3 Methylene Bromide ND 1000 961 96 1000 909 91 6 70-130/20
75-09-2 Methylene Chloride ND 1000 951 95 1000 899 90 6 70-130/20
1634-04-4 Methyl Tert Butyl Ether 75.6 1000 1020 94 1000 979 90 4 70-130/20
91-20-3 Naphthalene 104 1000 1070 97 1000 1010 91 6 70-130/20
103-65-1 n-Propylbenzene 119 1000 1220 110 1000 1060 94 14 70-130/20
100-42-5 Styrene ND 1000 933 93 1000 874 87 7 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 1000 1010 101 1000 957 96 5 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 1000 933 93 1000 819 82 13 70-130/20
127-18-4 Tetrachloroethylene ND 1000 1050 105 1000 968 97 8 70-130/20
108-88-3 Toluene 2270 1000 3070 80 1000 2830 56* b 8 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 1000 940 94 1000 903 90 4 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 1000 957 96 1000 901 90 6 70-130/20
71-55-6 1,1,1-Trichloroethane ND 1000 1010 101 1000 940 94 7 70-130/20
79-00-5 1,1,2-Trichloroethane ND 1000 954 95 1000 897 90 6 70-130/20
79-01-6 Trichloroethylene ND 1000 1020 102 1000 946 95 8 70-130/20
75-69-4 Trichlorofluoromethane ND 1000 993 99 1000 898 90 10 60-140/20
96-18-4 1,2,3-Trichloropropane ND 1000 974 97 1000 851 85 13 70-130/20
95-63-6 1,2,4-Trimethylbenzene 667 1000 1660 99 1000 1460 79 13 70-130/20
108-67-8 1,3,5-Trimethylbenzene 173 1000 1230 106 1000 1080 91 13 70-130/20
75-01-4 Vinyl Chloride ND 1000 1010 101 1000 931 93 8 60-140/20
m,p-Xylene 2440 2000 4330 95 2000 4020 79 7 70-130/20
95-47-6 o-Xylene 954 1000 1900 95 1000 1780 83 7 70-130/20
1330-20-7 Xylene (total)3390 3000 6230 95 3000 5790 80 7 70-130/20
CAS No.Surrogate Recoveries MS MSD FA37889-9 Limits
1868-53-7 Dibromofluoromethane 102%102%99%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%105%98%70-130%
2037-26-5 Toluene-D8 99%98%100%70-130%
460-00-4 4-Bromofluorobenzene 101%98%100%70-130%
(a) Confirmation run.
* = Outside of Control Limits.
33 of 34
FA3783355.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number:FA37833
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA37889-9MS E048823.D 100 10/21/16 MM n/a n/a VE1618
FA37889-9MSD E048824.D 100 10/21/16 MM n/a n/a VE1618
FA37889-9 a E048818.D 100 10/21/16 MM n/a n/a VE1618
The QC reported here applies to the following samples:Method: SM 6200B
FA37833-1, FA37833-3, FA37833-5
(b) Outside control limits due to high level in sample relative to spike amount.
* = Outside of Control Limits.
34 of 34
FA3783355.3.2