WA-762_10670_CA_MRP_20140911

Groundwater Monitoring Report
Union Country Cupboard
836 NC Highway 461
Union (Ahoskie), North Carolina
ATC Project No. 45.36019.1012
September 11, 2014

TABLE OF CONTENTS

1.0 INTRODUCTION ....................................................................................................... 1
2.0 SITE BACKGROUND ................................................................................................ 1
3.0 LIMITED RECEPTOR SURVEY ............................................................................. 4
4.0 GROUNDWATER MONITORING .......................................................................... 4
4.1 Groundwater Elevations ...................................................................................... 4
4.2 Groundwater Analytical Results .......................................................................... 4
5.0 CONCLUSIONS .......................................................................................................... 5

TABLES

Table 1 Water Supply Well Information
Table 2 Monitoring Well Construction Details
Table 3 Historical Groundwater Elevation Data
Table 4 Groundwater Analytical Data
Table 5 Historical Groundwater Analytical Data

FIGURES

Figure 1 Site Topographic Map
Figure 2 Site Map
Figure 3 Water Supply Well Location Map
Figure 4 Groundwater Contour Map
Figure 5 Dissolved Contaminants of Concern Concentration Map

APPENDICES

Appendix A Laboratory Analytical Results

Groundwater Monitoring Report September 11, 2014
NCDENR Incident No. 10670 ATC Project No. 45.36019.1012
Page 1
1.0 INTRODUCTION

ATC Associates of North Carolina, P.C. (ATC), on behalf of North East Oil Company, Inc., is
submitting this groundwater monitoring report for Union Country Cupboard located at 836 North
Carolina Highway 461 in Union (Ahoskie), North Carolina (Incident # 10670). The scope of
services included groundwater elevation monitoring, groundwater sampling, laboratory testing,
and report preparation. The report documents the results of groundwater sampling event
performed on June 15, 2014.

2.0 SITE BACKGROUND

Union Country Cupboard (Incident #10670) store is not currently operating. The site is located
at 836 North Carolina Highway 461 in Union (Ahoskie), Hertford County, North Carolina. The
site consists of a single-story building. A site topographic map is presented as Figure 1, a site
map is presented as Figure 2, and a water supply well map is presented as Figure 3.

On May 21, 1993, Coastal Environmental Services, Inc. (CES) conducted underground storage
tank (UST) closure and soil quality assessment activities at the site. The closure and assessment
activities were conducted in conjunction with the removal of one 1,000-gallon and one 550-
gallon gasoline USTs. As part of the closure, existing USTs were removed and soil in the
immediate vicinity of the tanks was analyzed for Total Petroleum Hydrocarbons (TPH). The
analytical results indicated that the soil surrounding the tanks was contaminated with petroleum
hydrocarbons at concentrations exceeding the state’s action limit of 10 milligrams per kilogram
(mg/kg).

On September 23, 1993, CES conducted a Phase I Groundwater Quality Assessment to determine
the presence of groundwater contamination. The assessment included the installation of three
monitoring wells (MW-1 through MW-3) and the collection of groundwater samples for
laboratory analysis. The analytical results indicated that dissolved phase hydrocarbons were
present above the 2L standards in monitoring well MW-3.

Groundwater Monitoring Report September 11, 2014
NCDENR Incident No. 10670 ATC Project No. 45.36019.1012
Page 2
CES conducted a Phase II Groundwater Quality Assessment at the site on February 22, 1994, to
help determine the lateral extent of the contaminant plume. The assessment included the
installation of two additional monitoring wells (MW-4 and MW-5) and the collection of
groundwater samples for laboratory analysis. The analytical results indicated that dissolved
phase hydrocarbons were present above the 2L standards in monitoring wells MW-1 through
MW-5.

On June 14 through 16, 1994, CES conducted a Phase III Groundwater Quality Assessment at the
site to help define the lateral and vertical extent of the contaminant plume. This assessment
included the installation of three additional monitoring wells (MW-6D through MW-8) and the
collection of groundwater samples for laboratory analysis. The analytical results indicated that
dissolved phase hydrocarbons were present above the 2L standards in monitoring wells MW-1
through MW-6.

A Phase IV Groundwater Quality Assessment was conducted on October 3, 10, and 11, 1995 to
further delineate the lateral extent of the dissolved contaminant plume. The assessment included
the installation of monitoring wells MW-9 through MW-14 and the collection of groundwater
samples for analytical testing. The analytical results indicated that dissolved phase hydrocarbons
were present above the 2L standards in monitoring wells MW-1, MW-3, MW-4, MW-5, and
MW-9.

A Comprehensive Site Assessment (CSA) summarizing the activities to date was submitted to
NCDENR on January 18, 1996. No additional information was collected for the preparation of
the CSA. A Corrective Action Plan (CAP) was submitted to NCDENR on June 15, 1997. The
CAP recommended Monitored Natural Attenuation as the remedial strategy for the site.
Groundwater was collected from the monitoring wells associated with the site quarterly in
August and November 1997; February, May, August, and November 1998; February and May
1999; August 2002; and February 2003. Site activities were suspended due to the funding by the
State Trust Fund.

Groundwater Monitoring Report September 11, 2014
NCDENR Incident No. 10670 ATC Project No. 45.36019.1012
Page 3
On March 25, 2009, Geologic Resources, Inc. advanced five soil borings (SB-1 through SB-5) in
the vicinity of the former tank pit. In addition, Geologic Resources, Inc. supervised the
installation of monitoring wells MW-15, MW-16, MW-17, and MW-18D.

A Notice of Regulatory Requirement (NORR) was issued on June 19, 2009, requesting a
continuation of semi-annual monitoring, replacement of MW-3, soil delineation, a mobile multi-
phase extraction (MMPE) event be performed on MW-4, and continue efforts to abandon water
supply wells in the area. On December 18, 2009, a Notice of Violation (NOV) was issued for
failure to submit a groundwater monitoring report.

In December 2009, North East Oil Company, Inc. awarded an environmental services contract to
ATC for continuing environmental assessment services at the site. In April 2010, ATC
performed an updated receptor survey, free product recovery via Mobile Multi-Phase Extraction
(MMPE), monitoring well installation, and groundwater sampling. The results of the assessment
activities were documented in a Groundwater Monitoring Report dated May 27, 2010. ATC
performed risk-based soil sampling and groundwater sampling in November 2010 and presented
the results in a Groundwater Monitoring Report dated February 1, 2011.

ATC performed a groundwater sampling event in May 2011 and submitted a Groundwater
Sampling Report to NCDENR on July 21, 2011. On August 12, 2011, NCDENR issued a letter
requesting the continued groundwater sampling, performing an MMPE event on MW-4 and a
limited excavation near MW-4. In December 2011, ATC performed an MMPE event on MW-4
in order to reduce the contaminant concentrations.

This report documents the results of the June 15, 2014 groundwater sampling event.

Groundwater Monitoring Report September 11, 2014
NCDENR Incident No. 10670 ATC Project No. 45.36019.1012
Page 4
3.0 LIMITED RECEPTOR SURVEY

On June 15, 2014, ATC performed a limited water supply well survey at the three properties
identified as having water supply wells in prior receptor surveys. Based on the field survey, three
water supply wells were observed within 1,500 feet of the site. All three properties were confirmed
to be connected to the municipal water supply on July 7, 2014.
• 838 NC Highway 461 (Inactive) – Well owned by James and Glenna Sullins and is located
130 feet from the site.
• 107 Liverman Mill Road (Inactive) – Well owned by Patricia Vann Blount and is located
275 feet from the site.
• Liverman Road (Inactive) – Well owned by Beatrice Blount and is located 350 feet from the
site.

A water supply well location map is presented as Figure 3. Water supply well information is
presented in Table 1.
4.0 GROUNDWATER MONITORING

4.1 Groundwater Elevations

On June 15, 2014, ATC collected static water level measurements from monitoring wells MW-2,
RMW-3, MW-4, MW-5, MW-6D, MW-8A, MW-9, MW-12, MW-16, MW-17, and MW-18D.
Monitoring well construction information is included in Table 2. Depth to water measurements
were collected using an electronic oil/water interface probe. Historical groundwater elevations
are included in Table 3. The groundwater depths were converted to relative elevations using an
assumed datum of 100 feet relative to an arbitrary on-site benchmark. A groundwater elevation
contour map is included as Figure 4. Based on the groundwater level measurements, groundwater
flows west across the site.

4.2 Groundwater Analytical Results

On June 15, 2014, groundwater samples were collected from monitoring wells MW-2, RMW-3,
MW-4, MW-5, MW-6D, MW-8A, MW-9, MW-12, MW-16, MW-17, and MW-18D.
Groundwater samples were collected into laboratory-approved containers, packed in ice and
delivered under chain-of-custody to Accutest Laboratories in Orlando, Florida, for analyses.
Groundwater samples were analyzed for volatile organic compounds (VOCs) by Method 6200B.
Groundwater Monitoring Report September 11, 2014
NCDENR Incident No. 10670 ATC Project No. 45.36019.1012
Page 5
A summary of the recent groundwater analytical data is presented in Table 4 and a historical
summary of groundwater analytical data is presented in Table 5.

The laboratory analytical results from the June 15, 2014, sampling event indicates that the
following compounds exceed the Title 15A NCAC 2L.0202 (2L) standards:

• Benzene, Toluene, Ethylbenzene, Total Xylenes: MW-4
• MTBE: MW-4
• Naphthalene: MW-4
• 1,2-Dichloroethane: RMW-3, MW-4 and MW-6D
• n-propylbenzene: MW-4
• 1,2,4-trimethylbenzene: MW-4

A concentration map is included as Figure 5. A copy of the laboratory analytical report is included
as Appendix A.

5.0 CONCLUSIONS

ATC has performed a groundwater sampling event at the Union Country Cupboard facility in
Union (Ahoskie), North Carolina. Based on field activities, observations, and groundwater
analytical results, ATC concludes the following:

• Three inactive water supply wells are located within 500 feet of the site. Based on the
presence of the water supply wells, the site risk ranking is High.
• Depth to groundwater measurements ranged from 2.32 feet to 14.50 feet below ground
surface in MW-18D and MW-9, respectively. The inferred shallow groundwater flow
direction across the site is historically to the west.
• The property owner at the site has changed. Mr. Sherwood Brown is the new owner.
Groundwater Monitoring Report September 11, 2014
NCDENR Incident No. 10670 ATC Project No. 45.36019.1012
Page 6
• The groundwater analytical results indicated that benzene, toluene, ethylbenzene, total
xylenes, MTBE, naphthalene, 1,2-dichloroethane, n-propylbenzene, and 1,2,4-
trimethylbenzene exceeded the NC 2L Standards.

ATC recommends continued semi-annual sampling, abandonment of the water supply wells
within 500 feet of the property, and performing a limited soil excavation near MW-4.

TABLES
TABLE 1
WATER SUPPLY WELL INFORMATION
UNION COUNTRY CUPBOARD
836 NC ROUTE 461
UNION, HERTFORD COUNTY, NC
NCDENR INCIDENT NO. 10670
ATC PROJECT NO. 45.36019.0012
5984-16-6159 James and Glenna
Sullins
838 NC
Hwy 461
252-209-
4464 Inactive Unknown Unknown Unknown Unknown 130 Downgradient
5984-16-6313 Patricia Vann Blount
(owner)
107
Liverman
Mill Road
252-332-
6677 Inactive Unknown Unknown Unknown Unknown 275 Downgradient
5984-16-5389 Beatrice Blount Heirs
(owner)
Liverman
Road
302-654-
7375 Inactive Unknown Unknown Unknown Unknown 350 Cross-gradient
ft BGS = feet below ground surface
Well #
Well Owner/ User
(indicate which)Address
Phone
Number
Well
Screen
Interval (x
to y ft.
BGS)
Distance
from source
area of
release (ft.)
Up or
downgradientWell Use
Well
Depth (ft
BGS)
Type of
Well
Well
Casing
Depth (ft.
BGS)
TABLE 2
MONITORING WELL CONSTRUCTION DETAILS
UNION COUNTRY CUPBOARD
836 NC ROUTE 461
UNION, HERTFORD COUNTY, NC
NCDENR INCIDENT NO. 10670
ATC PROJECT NO. 45.36019.0012
Page 2 of 33
Depth of
Water (feet)
Groundwater
Elevation (feet)
MW-1 10/15/1993 2 8-18 18 100.00
MW-2 10/15/1993 2 8-18 18 100.06 2.47 97.59
RMW-3 4/26/2010 2 10-25 25 100.16 11.70 88.46
MW-4 2/22/1994 2 8-18 18 100.18 2.80 97.38
MW-5 2/22/1994 2 8-18 20 100.18 2.53 97.65
MW-6D 6/14/1994 2 30-35 35 100.66 12.63 88.03
MW-7 6/15/1994 2 8-18 18 99.72 NL NL
MW-8A 10/8/1997 2 10-20 20 99.74 10.56 89.18
MW-9 10/10/1995 2 10-20 20 99.19 14.50 84.69
MW-10 10/3/1995 2 10-20 20 99.47 NL NL
MW-11 10/3/1995 2 11-21 21 99.02 NL NL
MW-12 10/11/1995 2 10-20 20 99.70 9.91 89.79
MW-13 10/11/1995 2 10-20 19 99.77 NL NM
MW-14A 7/18/2002 2 Unknown 20 99.15 NL NM
MW-15 3/25/2009 2 10-20 20 99.26 NL NM
MW-16 3/25/2009 2 10-20 20 100.10 2.41 97.69
MW-17 3/25/2009 2 10-20 20 100.14 9.00 91.14
MW-18 3/25/2009 2 34-39 39 99.85 2.32 97.53
Notes:
1. Elevations are referenced to an arbitrary on-site benchmark of 100.00 feet.
2. NM =Not Measured
Destroyed
Depth of Well
(feet)
Top of Casing
(feet)
Date Measured: 6/15/2014
Monitoring
Well ID Date Installed
Well Casing
Diameter
(Inches)
Screened
Interval
(feet)
TABLE 3HISTORICAL GROUNDWATER ELEVATION DATA
UNION COUNTRY CUPBOARD
836 NC ROUTE 461
UNION, HERTFORD COUNTY, NORTH CAROLINA
NCDENR INCIDENT NO. 10670
ATC PROJECT NO. 45.36019.0012
Page 3 of 33
Well ID Date
Top of Casing
Elevation (Feet)
Depth to Water
(Feet)
Depth to
Product (Feet)
Groundwater
Elevation (Feet)
MW-1 09/27/93 100.00 11.00 ND 89.00
03/07/94 100.00 11.00 ND 89.00
07/01/94 100.00 11.33 ND 88.67
10/23/95 100.00 13.00 ND 87.0002/11/97 100.00 11.00 ND 89.00
08/27/97 100.00 13.00 ND 87.00
11/20/97 100.00 13.46 ND 86.54
02/10/98 100.00 11.21 ND 88.7905/05/98 100.00 11.32 ND 88.68
08/04/98 100.00 11.84 ND 88.16
11/02/98 100.00 13.20 ND 86.80
08/23/99 100.00 12.78 ND 87.2202/03/00 100.00 10.22 ND 89.7805/01/00 100.00 NR NR NA
08/21/00 100.00 11.70 ND 88.30
11/10/00 100.00 11.10 ND 88.9002/02/01 100.00 11.35 ND 88.6505/14/01 100.00 10.08 ND 89.92
08/04/01 100.00 12.38 ND 87.62
02/26/02 100.00 13.22 ND 86.7808/19/02 100.00 14.30 ND 85.7002/05/03 100.00 12.28 ND 87.72
07/01/08 100.00 7.77 ND 92.23
03/25/09 100.00 8.42 ND 91.5804/22/10 100.00 6.03 ND 93.9711/30/10 100.00 7.91 ND 92.09
05/25/11 100.00 6.33 ND 93.6704/09/12 100.00
Notes:MW - Type II monitoring well
MWD - Type II vertical extent monitoring well
NS - Not Surveyed
NM - Not MeasuredNA - Not Available
ND - Not Detected
Destroyed
TABLE 3HISTORICAL GROUNDWATER ELEVATION DATA
UNION COUNTRY CUPBOARD
836 NC ROUTE 461
UNION, HERTFORD COUNTY, NORTH CAROLINA
NCDENR INCIDENT NO. 10670
ATC PROJECT NO. 45.36019.0012
Page 4 of 33
Well ID Date
Top of Casing
Elevation (Feet)
Depth to Water
(Feet)
Depth to
Product (Feet)
Groundwater
Elevation (Feet)
MW-2 09/27/93 100.06 11.40 ND 88.66
03/07/94 100.06 12.12 ND 87.94
07/01/94 100.06 12.00 ND 88.06
10/23/95 100.06 13.75 ND 86.3102/11/97 100.06 NM ND NA
08/27/97 100.06 NM ND NA
11/20/97 100.06 12.96 ND 87.10
02/10/98 100.06 11.89 ND 88.1705/05/98 100.06 11.26 ND 88.80
08/04/98 100.06 12.27 ND 87.79
11/02/98 100.06 11.30 ND 88.76
08/23/99 100.06 12.85 ND 87.2102/03/00 100.06 11.25 ND 88.81
05/01/00 100.06 NR NR NA
08/21/00 100.06 11.48 ND 88.58
11/10/00 100.06 4.70 ND 95.3602/02/01 100.06 10.85 ND 89.2105/14/01 100.06 12.08 ND 87.98
08/04/01 100.06 11.62 ND 88.44
02/26/02 100.06 12.25 ND 87.8108/19/02 100.06 13.85 ND 86.2102/05/03 100.06 12.49 ND 87.57
07/01/08 100.06 6.98 ND 93.08
03/25/09 100.06 6.30 ND 93.7604/22/10 100.06 NM NM NA11/30/10 100.06 NM NM NA
05/25/11 100.06 5.85 ND 94.21
04/09/12 100.06 NR NR NA06/15/14 100.06 2.47 NR 97.59
Notes:
MW - Type II monitoring well
MWD - Type II vertical extent monitoring well
NS - Not SurveyedNM - Not Measured
NA - Not Available
ND - Not Detected
TABLE 3HISTORICAL GROUNDWATER ELEVATION DATA
UNION COUNTRY CUPBOARD
836 NC ROUTE 461
UNION, HERTFORD COUNTY, NORTH CAROLINA
NCDENR INCIDENT NO. 10670
ATC PROJECT NO. 45.36019.0012
Page 5 of 33
Well ID Date
Top of Casing
Elevation (Feet)
Depth to Water
(Feet)
Depth to
Product (Feet)
Groundwater
Elevation (Feet)
MW-3 09/27/93 100.31 10.73 ND 89.58
03/07/94 100.31 12.11 ND 88.20
07/01/94 100.31 12.02 ND 88.29
10/23/95 100.31 13.93 ND 86.3802/11/97 100.31 11.21 ND 89.10
08/27/97 100.31 14.00 ND 86.31
11/20/97 100.31 12.76 ND 87.55
02/10/98 100.31 11.71 ND 88.6005/05/98 100.31 10.25 ND 90.06
08/04/98 100.31 11.29 ND 89.02
11/02/98 100.31 12.39 ND 87.92
08/23/99 100.31 12.48 ND 87.8302/03/00 100.31 9.98 ND 90.33
05/01/00 100.31 NR NR NA
08/21/00 100.31 9.80 ND 90.51
11/10/00 100.31 9.04 ND 91.2702/02/01 100.31 10.61 ND 89.7005/14/01 100.31 12.16 ND 88.15
08/04/01 100.31 12.05 ND 88.26
02/26/02 100.31 10.45 ND 89.8608/19/02 100.31 13.60 ND 86.7102/05/03 100.31 12.67 ND 87.64
07/01/08 100.31 NM NM NA
03/25/09 100.31 NM NM NARMW-3 04/22/10 NS 11.33 NM NA11/30/10 100.16 12.87 ND 87.29
05/25/11 100.16 12.25 ND 87.91
04/09/12 100.16 13.20 ND 86.9606/15/14 100.16 11.70 ND 88.46
Notes:
MW - Type II monitoring well
MWD - Type II vertical extent monitoring well
NS - Not SurveyedNM - Not Measured
NA - Not Available
ND - Not Detected
TABLE 3HISTORICAL GROUNDWATER ELEVATION DATA
UNION COUNTRY CUPBOARD
836 NC ROUTE 461
UNION, HERTFORD COUNTY, NORTH CAROLINA
NCDENR INCIDENT NO. 10670
ATC PROJECT NO. 45.36019.0012
Page 6 of 33
Well ID Date
Top of Casing
Elevation (Feet)
Depth to Water
(Feet)
Depth to
Product (Feet)
Groundwater
Elevation (Feet)
MW-4 03/07/94 100.18 9.98 ND 90.20
07/01/94 100.18 9.99 ND 90.19
10/23/95 100.18 12.39 ND 87.79
02/11/97 100.18 12.43 ND 87.7508/27/97 100.18 14.31 ND 85.87
11/20/97 100.18 14.98 ND 85.20
02/10/98 100.18 12.55 ND 87.63
05/05/98 100.18 8.89 ND 91.2908/04/98 100.18 10.03 ND 90.15
11/02/98 100.18 13.06 ND 87.12
08/23/99 100.18 13.43 ND 86.75
02/03/00 100.18 12.04 ND 88.1405/01/00 100.18 9.22 ND 90.96
08/21/00 100.18 12.82 ND 87.36
11/10/00 100.18 9.26 ND 90.92
02/02/01 100.18 12.14 ND 88.0405/14/01 100.18 7.29 ND 92.8908/04/01 100.18 12.42 ND 87.76
02/26/02 100.18 11.92 ND 88.26
08/19/02 100.18 14.20 ND 85.9802/05/03 100.18 12.42 ND 87.7607/01/08 100.18 7.39 ND 92.79
03/25/09 100.18 5.09 ND 95.09
04/22/10 100.18 6.28 ND 93.9011/30/10 100.18 8.22 ND 91.9605/25/11 100.18 6.20 ND 93.98
04/09/12 100.18 6.55 ND 93.6306/15/14 100.18 2.80 ND 97.38
Notes:MW - Type II monitoring well
MWD - Type II vertical extent monitoring well
NS - Not Surveyed
NM - Not MeasuredNA - Not Available
ND - Not Detected
TABLE 3HISTORICAL GROUNDWATER ELEVATION DATA
UNION COUNTRY CUPBOARD
836 NC ROUTE 461
UNION, HERTFORD COUNTY, NORTH CAROLINA
NCDENR INCIDENT NO. 10670
ATC PROJECT NO. 45.36019.0012
Page 7 of 33
Well ID Date
Top of Casing
Elevation (Feet)
Depth to Water
(Feet)
Depth to
Product (Feet)
Groundwater
Elevation (Feet)
MW-5 03/07/94 100.18 9.03 ND 91.15
07/01/94 100.18 10.15 ND 90.03
10/23/95 100.18 12.55 ND 87.63
02/11/97 100.18 9.87 ND 90.3108/27/97 100.18 9.85 ND 90.33
11/20/97 100.18 11.40 ND 88.78
02/10/98 100.18 9.79 ND 90.39
05/05/98 100.18 8.78 ND 91.4008/04/98 100.18 9.68 ND 90.50
11/02/98 100.18 11.85 ND 88.33
08/23/99 100.18 11.13 ND 89.05
02/03/00 100.18 8.13 ND 92.0505/01/00 100.18 NR NR NA
08/21/00 100.18 8.88 ND 91.30
11/10/00 100.18 9.83 ND 90.35
02/02/01 100.18 9.54 ND 90.6405/14/01 100.18 9.10 ND 91.0808/04/01 100.18 9.85 ND 90.33
02/26/02 100.18 10.04 ND 90.14
08/19/02 100.18 12.10 ND 88.0802/05/03 100.18 9.49 ND 90.6907/01/08 100.18 6.98 ND 93.20
03/25/09 100.18 6.52 ND 93.66
04/22/10 100.18 5.92 ND 94.2611/30/10 100.18 7.05 ND 93.1305/25/11 100.18 6.01 ND 94.17
04/09/12 100.18 6.45 ND 93.7306/15/14 100.18 2.53 ND 97.65
Notes:MW - Type II monitoring well
MWD - Type II vertical extent monitoring well
NS - Not Surveyed
NM - Not MeasuredNA - Not Available
ND - Not Detected
TABLE 3HISTORICAL GROUNDWATER ELEVATION DATA
UNION COUNTRY CUPBOARD
836 NC ROUTE 461
UNION, HERTFORD COUNTY, NORTH CAROLINA
NCDENR INCIDENT NO. 10670
ATC PROJECT NO. 45.36019.0012
Page 8 of 33
Well ID Date
Top of Casing
Elevation (Feet)
Depth to Water
(Feet)
Depth to
Product (Feet)
Groundwater
Elevation (Feet)
MW-6D 07/01/94 100.66 12.04 ND 88.62
10/23/95 100.66 14.22 ND 86.44
02/11/97 100.66 12.60 ND 88.06
08/27/97 100.66 12.98 ND 87.6811/20/97 100.66 13.67 ND 86.99
02/10/98 100.66 12.40 ND 88.26
05/05/98 100.66 11.30 ND 89.36
08/04/98 100.66 12.37 ND 88.2911/02/98 100.66 13.18 ND 87.48
08/23/99 100.66 13.38 ND 87.28
02/03/00 100.66 12.11 ND 88.55
05/01/00 100.66 12.26 ND 88.4008/21/00 100.66 11.26 ND 89.40
11/10/00 100.66 12.24 ND 88.42
02/02/01 100.66 12.03 ND 88.63
05/14/01 100.66 12.92 ND 87.7408/04/01 100.66 12.45 ND 88.2102/26/02 100.66 13.46 ND 87.20
08/19/02 100.66 14.45 ND 86.21
02/05/03 100.66 13.57 ND 87.0907/01/08 100.66 13.13 ND 87.5303/25/09 100.66 13.70 ND 86.96
04/22/10 100.66 11.75 ND 88.91
11/30/10 100.66 13.62 ND 87.0405/25/11 100.66 12.95 ND 87.7104/09/12 100.66 NR NR NA06/15/14 100.66 12.63 NR 88.03
Notes:
MW - Type II monitoring wellMWD - Type II vertical extent monitoring well
NS - Not Surveyed
NM - Not Measured
NA - Not AvailableND - Not Detected
TABLE 3HISTORICAL GROUNDWATER ELEVATION DATA
UNION COUNTRY CUPBOARD
836 NC ROUTE 461
UNION, HERTFORD COUNTY, NORTH CAROLINA
NCDENR INCIDENT NO. 10670
ATC PROJECT NO. 45.36019.0012
Page 9 of 33
Well ID Date
Top of Casing
Elevation (Feet)
Depth to Water
(Feet)
Depth to
Product (Feet)
Groundwater
Elevation (Feet)
MW-7 07/01/94 99.72 11.05 ND 88.67
10/23/95 99.72 13.00 ND 86.72
02/11/97 99.72 12.20 ND 87.52
08/27/97 99.72 11.92 ND 87.8011/20/97 99.72 12.85 ND 86.87
02/10/98 99.72 11.46 ND 88.26
05/05/98 99.72 10.30 ND 89.42
08/04/98 99.72 NM NM NA11/02/98 99.72 11.70 ND 88.02
08/23/99 99.72 12.19 ND 87.53
02/03/00 99.72 10.28 ND 89.44
05/01/00 99.72 NR NR NA08/21/00 99.72 10.37 ND 89.35
11/10/00 99.72 9.80 ND 89.92
02/02/01 99.72 10.95 ND 88.77
05/14/01 99.72 13.78 ND 85.9408/04/01 99.72 13.49 ND 86.2302/26/02 99.72 12.39 ND 87.33
08/19/02 99.72 13.54 ND 86.18
02/05/03 99.72 12.63 ND 87.0907/01/08 99.72 NM NM NA03/25/09 99.72 12.72 ND 87.00
04/22/10 99.72 NM NM NA
11/30/10 99.72 NM NM NA05/25/11 99.72 NM NM NA04/09/12 99.72 NR NR NA06/15/14 99.72 NM NR NA
Notes:
MW - Type II monitoring wellMWD - Type II vertical extent monitoring well
NS - Not Surveyed
NM - Not Measured
NA - Not AvailableND - Not Detected
TABLE 3HISTORICAL GROUNDWATER ELEVATION DATA
UNION COUNTRY CUPBOARD
836 NC ROUTE 461
UNION, HERTFORD COUNTY, NORTH CAROLINA
NCDENR INCIDENT NO. 10670
ATC PROJECT NO. 45.36019.0012
Page 10 of 33
Well ID Date
Top of Casing
Elevation (Feet)
Depth to Water
(Feet)
Depth to
Product (Feet)
Groundwater
Elevation (Feet)
MW-8 07/01/94 99.74 11.09 ND 88.6510/23/95 Destroyed Destroyed Destroyed Destroyed
MW-8A 02/10/98 99.74 10.87 ND 88.87
05/05/98 99.74 11.05 ND 88.6908/04/98 99.74 12.88 ND 86.86
11/02/98 99.74 13.35 ND 86.39
08/23/99 99.74 13.38 ND 86.36
02/03/00 99.74 11.19 ND 88.5505/01/00 99.74 12.24 ND 87.50
08/21/00 99.74 8.92 ND 90.82
11/10/00 99.74 12.20 ND 87.54
02/02/01 99.74 12.14 ND 87.6005/14/01 99.74 11.91 ND 87.83
08/04/01 99.74 12.46 ND 87.28
02/26/02 99.74 12.55 ND 87.19
08/19/02 99.74 13.74 ND 86.0002/05/03 99.74 12.21 ND 87.5307/01/08 99.74 12.84 ND 86.90
03/25/09 99.74 11.30 ND 88.44
04/22/10 99.74 10.00 ND 89.7411/30/10 99.74 12.83 ND 86.9105/25/11 99.74 11.33 ND 88.41
04/09/12 99.74 NM NM NA06/15/14 99.74 10.56 NR 89.18
Notes:MW - Type II monitoring well
MWD - Type II vertical extent monitoring well
NS - Not Surveyed
NM - Not MeasuredNA - Not Available
ND - Not Detected
TABLE 3HISTORICAL GROUNDWATER ELEVATION DATA
UNION COUNTRY CUPBOARD
836 NC ROUTE 461
UNION, HERTFORD COUNTY, NORTH CAROLINA
NCDENR INCIDENT NO. 10670
ATC PROJECT NO. 45.36019.0012
Page 11 of 33
Well ID Date
Top of Casing
Elevation (Feet)
Depth to Water
(Feet)
Depth to
Product (Feet)
Groundwater
Elevation (Feet)
MW-9 10/23/95 99.19 12.77 ND 86.42
02/11/97 99.19 10.30 ND 88.89
08/27/97 99.19 12.55 ND 86.64
11/20/97 99.19 NM ND NA02/10/98 99.19 10.84 ND 88.35
05/05/98 99.19 11.55 ND 87.64
08/04/98 99.19 10.72 ND 88.47
11/02/98 99.19 11.70 ND 87.4908/23/99 99.19 11.71 ND 87.48
02/03/00 99.19 9.34 ND 89.85
05/01/00 99.19 NR NR NA
08/21/00 99.19 11.78 ND 87.4111/10/00 99.19 9.72 ND 89.47
02/02/01 99.19 10.95 ND 88.24
05/14/01 99.19 9.91 ND 89.28
08/04/01 99.19 10.36 ND 88.8302/26/02 99.19 12.58 ND 86.6108/19/02 99.19 13.50 ND 85.69
02/05/03 99.19 11.76 ND 87.43
07/01/08 99.19 12.51 ND 86.6803/25/09 99.19 11.10 ND 88.0904/22/10 99.19 NM NM NA
11/30/10 99.19 16.15 ND 83.04
05/25/11 99.19 15.17 ND 84.0204/09/12 99.19 NM NM NA06/15/14 99.19 14.50 ND 84.69
Notes:
MW - Type II monitoring well
MWD - Type II vertical extent monitoring wellNS - Not Surveyed
NM - Not Measured
NA - Not Available
ND - Not Detected
TABLE 3HISTORICAL GROUNDWATER ELEVATION DATA
UNION COUNTRY CUPBOARD
836 NC ROUTE 461
UNION, HERTFORD COUNTY, NORTH CAROLINA
NCDENR INCIDENT NO. 10670
ATC PROJECT NO. 45.36019.0012
Page 12 of 33
Well ID Date
Top of Casing
Elevation (Feet)
Depth to Water
(Feet)
Depth to
Product (Feet)
Groundwater
Elevation (Feet)
MW-10 10/23/95 99.47 13.33 ND 86.14
02/11/97 99.47 8.67 ND 90.80
08/27/97 99.47 12.35 ND 87.12
11/20/97 99.47 12.25 ND 87.2202/10/98 99.47 11.38 ND 88.09
05/05/98 99.47 9.65 ND 89.82
08/04/98 99.47 10.71 ND 88.76
11/02/98 99.47 11.60 ND 87.8708/23/99 99.47 11.73 ND 87.74
02/03/00 99.47 9.32 ND 90.15
05/01/00 99.47 NR NR NA
08/21/00 99.47 9.27 ND 90.2011/10/00 99.47 8.86 ND 90.61
02/02/01 99.47 9.25 ND 90.22
05/14/01 99.47 10.45 ND 89.02
08/04/01 99.47 12.56 ND 86.9102/26/02 99.47 11.14 ND 88.3308/19/02 99.47 12.70 ND 86.77
02/05/03 99.47 8.23 ND 91.24
07/01/08 99.47 NM NM NA03/25/09 99.47 NM NM NA04/22/10 99.47 NM NM NA
11/30/10 99.47 NM NM NA
05/25/11 99.47 NM NM NA04/09/12 99.47 NM NM NA06/15/14 99.47 NM NM NA
Notes:
MW - Type II monitoring well
MWD - Type II vertical extent monitoring wellNS - Not Surveyed
NM - Not Measured
NA - Not Available
ND - Not Detected
TABLE 3HISTORICAL GROUNDWATER ELEVATION DATA
UNION COUNTRY CUPBOARD
836 NC ROUTE 461
UNION, HERTFORD COUNTY, NORTH CAROLINA
NCDENR INCIDENT NO. 10670
ATC PROJECT NO. 45.36019.0012
Page 13 of 33
Well ID Date
Top of Casing
Elevation (Feet)
Depth to Water
(Feet)
Depth to
Product (Feet)
Groundwater
Elevation (Feet)
MW-11 10/23/95 99.02 13.81 ND 85.21
02/11/97 99.02 10.62 ND 88.40
08/27/97 99.02 13.92 ND 85.10
11/20/97 99.02 13.06 ND 85.9602/10/98 99.02 11.45 ND 87.57
05/05/98 99.02 10.72 ND 88.30
08/04/98 99.02 11.35 ND 87.67
11/02/98 99.02 12.40 ND 86.6208/23/99 99.02 13.22 ND 85.80
02/03/00 99.02 10.08 ND 88.94
05/01/00 99.02 10.35 ND 88.67
08/21/00 99.02 10.39 ND 88.6311/10/00 99.02 10.32 ND 88.70
02/02/01 99.02 10.23 ND 88.79
05/14/01 99.02 9.98 ND 89.04
08/04/01 99.02 10.64 ND 88.3802/26/02 99.02 11.51 ND 87.5108/19/02 99.02 13.25 ND 85.77
02/05/03 99.02 11.92 ND 87.10
07/01/08 99.02 9.97 ND 89.0503/25/09 99.02 10.10 ND 88.9204/22/10 99.02 9.25 ND 89.77
11/30/10 99.02 11.98 ND 87.04
05/25/11 99.02 9.30 ND 89.7204/09/12 99.02 NM NM NA06/15/14 99.02 NM NM NA
Notes:
MW - Type II monitoring well
MWD - Type II vertical extent monitoring wellNS - Not Surveyed
NM - Not Measured
NA - Not Available
ND - Not Detected
TABLE 3HISTORICAL GROUNDWATER ELEVATION DATA
UNION COUNTRY CUPBOARD
836 NC ROUTE 461
UNION, HERTFORD COUNTY, NORTH CAROLINA
NCDENR INCIDENT NO. 10670
ATC PROJECT NO. 45.36019.0012
Page 14 of 33
Well ID Date
Top of Casing
Elevation (Feet)
Depth to Water
(Feet)
Depth to
Product (Feet)
Groundwater
Elevation (Feet)
MW-12 10/23/95 99.70 15.48 ND 84.22
02/11/97 99.70 11.58 ND 88.12
08/27/97 99.70 13.35 ND 86.35
11/20/97 99.70 13.62 ND 86.0802/10/98 99.70 12.18 ND 87.52
05/05/98 99.70 10.95 ND 88.75
08/04/98 99.70 12.26 ND 87.44
11/02/98 99.70 13.30 ND 86.4008/23/99 99.70 13.61 ND 86.09
02/03/00 99.70 10.98 ND 88.72
05/01/00 99.70 11.17 ND 88.53
08/21/00 99.70 10.99 ND 88.7111/10/00 99.70 11.12 ND 88.58
02/02/01 99.70 10.65 ND 89.05
05/14/01 99.70 11.35 ND 88.35
08/04/01 99.70 13.47 ND 86.2302/26/02 99.70 12.71 ND 86.9908/19/02 99.70 11.50 ND 88.20
02/05/03 99.70 12.69 ND 87.01
04/22/10 99.70 11.40 ND 88.3011/30/10 99.70 13.25 ND 86.4505/25/11 99.70 11.98 ND 87.72
04/09/12 99.70 NR NR NA06/15/14 99.70 9.91 NR 89.79
Notes:MW - Type II monitoring well
MWD - Type II vertical extent monitoring well
NS - Not Surveyed
NM - Not MeasuredNA - Not Available
ND - Not Detected
TABLE 3HISTORICAL GROUNDWATER ELEVATION DATA
UNION COUNTRY CUPBOARD
836 NC ROUTE 461
UNION, HERTFORD COUNTY, NORTH CAROLINA
NCDENR INCIDENT NO. 10670
ATC PROJECT NO. 45.36019.0012
Page 15 of 33
Well ID Date
Top of Casing
Elevation (Feet)
Depth to Water
(Feet)
Depth to
Product (Feet)
Groundwater
Elevation (Feet)
MW-13 10/23/95 99.77 13.32 ND 86.45
02/11/97 99.77 11.18 ND 88.59
08/27/97 99.77 13.40 ND 86.37
11/20/97 99.77 12.92 ND 86.8502/10/98 99.77 13.39 ND 86.38
05/05/98 99.77 12.60 ND 87.17
08/04/98 99.77 12.80 ND 86.97
11/02/98 99.77 13.35 ND 86.4208/23/99 99.77 13.36 ND 86.41
02/03/00 99.77 12.40 ND 87.37
05/01/00 99.77 NR NR NA
08/21/00 99.77 11.86 ND 87.9111/10/00 99.77 10.48 ND 89.29
02/02/01 99.77 11.35 ND 88.42
05/14/01 99.77 13.30 ND 86.47
08/04/01 99.77 12.59 ND 87.1802/26/02 99.77 14.25 ND 85.5208/19/02 99.77 13.85 ND 85.92
02/05/03 99.77 13.33 ND 86.44
07/01/08 99.77 11.39 ND 88.3803/25/09 99.77 13.91 ND 85.8604/22/10 99.77 11.72 ND 88.05
11/30/10 99.77 12.30 ND 87.47
05/25/11 99.77 12.18 ND 87.5904/09/12 99.77 NM NM NA06/15/14 99.77 NM NM NA
Notes:
MW - Type II monitoring well
MWD - Type II vertical extent monitoring wellNS - Not Surveyed
NM - Not Measured
NA - Not Available
ND - Not Detected
TABLE 3HISTORICAL GROUNDWATER ELEVATION DATA
UNION COUNTRY CUPBOARD
836 NC ROUTE 461
UNION, HERTFORD COUNTY, NORTH CAROLINA
NCDENR INCIDENT NO. 10670
ATC PROJECT NO. 45.36019.0012
Page 16 of 33
Well ID Date
Top of Casing
Elevation (Feet)
Depth to Water
(Feet)
Depth to
Product (Feet)
Groundwater
Elevation (Feet)
MW-14 10/23/95 99.15 13.20 ND 85.95
02/11/97 99.15 11.58 ND 87.57
08/27/97 99.15 10.74 ND 88.41
11/20/97 99.15 12.01 ND 87.1402/10/98 99.15 12.79 ND 86.36
05/05/98 99.15 12.35 ND 86.80
08/04/98 99.15 11.76 ND 87.39
11/02/98 99.15 13.30 ND 85.8508/23/99 99.15 Destroyed NA NA
MW-14A 08/19/02 99.15 14.40 ND 84.75
02/05/03 99.15 12.13 ND 87.02
07/01/08 99.15 11.75 ND 87.4003/25/09 99.15 12.44 ND 86.71
04/22/10 99.15 10.27 ND 88.88
11/30/10 99.15 12.45 ND 86.70
05/25/11 99.15 NM NM NA04/09/12 99.15 NM NM NA06/15/14 99.15 NM NM NA
MW-15 03/25/09 99.26 10.95 ND 88.3106/15/14 99.26 NM NM NA
MW-16 03/25/09 100.10 6.50 ND 93.6006/15/14 100.10 2.41 ND 97.69
MW-17 03/25/09 100.14 17.10 ND 83.0406/15/14 100.14 9.00 ND 91.14
MW-18D 03/25/09 99.85 13.71 NR 86.1406/15/14 99.85 2.32 ND 97.53
Notes:
MW - Type II monitoring well
MWD - Type II vertical extent monitoring wellNS - Not Surveyed
NM - Not Measured
NA - Not Available
ND - Not Detected
TABLE 4
GROUNDWATER ANALYTICAL DATA
UNION COUNTRY CUPBOARD
836 NC ROUTE 461
UNION, HERTFORD COUNTY, NC
NCDENR INCIDENT NO. 10670
ATC PROJECT NO. 45.36019.0012
Well ID
Date Collected
MW-2 6/15/2014 <0.50 <0.50 <0.50 <1.5 <0.50 <0.50 <0.50 <10 <0.50 <0.50 <0.50 <0.50 <0.50 <2.5 <0.50 <0.50 <0.50
RMW-3 6/15/2014 0.25 J <0.50 <0.50 <1.5 9.6 0.20 J 1.1 10.5 <0.50 0.63 2.8 0.61 <0.50 <2.5 <0.50 <0.50 <0.50
MW-4 6/15/2014 3,350 1,180 757 2,000 4,990 14.5 223 <100 4.5 J 3.9 J 5.3 33.5 2.1 J 47.9 75.1 490 106
MW-5 6/15/2014 <0.50 <0.50 <0.50 <1.5 0.26 J <0.50 <0.50 <10 <0.50 <0.50 <0.50 <0.50 <0.50 <2.5 <0.50 <0.50 <0.50
MW-6D 6/15/2014 0.38 J <0.50 <0.50 <1.5 12.5 0.18 J <0.50 <10 <0.50 <0.50 0.41 J <0.50 <0.50 <2.5 <0.50 <0.50 <0.50
MW-8A 6/15/2014 <0.50 <0.50 <0.50 <1.5 <0.50 <0.50 <0.50 <10 <0.50 <0.50 <0.50 <0.50 <0.50 <2.5 <0.50 <0.50 <0.50
MW-9 6/15/2014 <0.50 <0.50 <0.50 <1.5 <0.50 <0.50 <0.50 <10 <0.50 <0.50 <0.50 <0.50 <0.50 <2.5 <0.50 <0.50 <0.50
MW-12 6/15/2014 <0.50 <0.50 <0.50 <1.5 <0.50 <0.50 <0.50 <10 <0.50 <0.50 <0.50 <0.50 <0.50 <2.5 <0.50 <0.50 <0.50
MW-16 6/15/2014 <0.50 <0.50 <0.50 <1.5 <0.50 <0.50 <0.50 <10 <0.50 <0.50 <0.50 <0.50 <0.50 <2.5 <0.50 <0.50 <0.50
MW-17 6/15/2014 <0.50 <0.50 <0.50 <1.5 13.1 0.11 J <0.50 <10 <0.50 <0.50 <0.50 <0.50 <0.50 <2.5 <0.50 <0.50 <0.50
MW-18D 6/15/2014 0.17 J <0.50 <0.50 <1.5 1.6 <0.50 <0.50 <10 <0.50 <0.50 <0.50 <0.50 <0.50 <2.5 <0.50 <0.50 <0.50
1 600 600 500 20 70 6 6,000 70 70 0.4 70 25 4,000 70 400 400
5,000 260,000 85,400 85,500 20,000 70,000 6,000 6,000,000 6,900 8,500 400 25,000 11,700 NE 30,000 28,500 25,000
Notes:
1. "<" or ND = Not detected at or above the laboratory detection limit.
2. Concentrations are reported in micrograms per liter (µg/l) = parts per billion.
3. Concentrations in bold print equal or exceed the NCDENR 2L Standard (2L).
4. NCDENR = North Carolina Department of Environment and Natural Resources.
5. GCL = Gross Contaminantion Level.
6. NE = Not Established.
7. MTBE = Methyl Tertiary Butyl Ether.
8. Gross Contamination Levels for Groundwater are referenced in the "Guidelines for Assessment and Corrective Action for UST Releases", July 2008, Table 2, updated January 2010 n-PropylbenzeneMethyl ethyl ketonesec-Butylbenzenen-Butylbenzene1,2,4-Trimethylbenzene1,3,5-Trimethylbenzene6200BAnalytical Method
Contaminant of Concern
BenzeneTolueneIsopropyl etherAcetoneNaphthalenep-IsopropyltolueneIsopropylbenzene2L Standard (µg/l)
GCL (µg/l)EthylbenzeneTotal XylenesMTBE1,2-Dichloroethane
TABLE 5
HISTORICAL GROUNDWATER ANALYTICAL DATA
UNION COUNTRY CUPBOARD
836 NC ROUTE 461
UNION, HERTFORD COUNTY, NC
NCDENR INCIDENT NO. 10670
ATC PROJECT NO. 45.36019.0012
Page 18 of 33BenzeneTolueneEthylbenzeneTotal XylenesMTBEIPELeadBoring ID Sample Date ug/l ug/l ug/l ug/l ug/l ug/l ug/l9/27/1993 BQL BQL BQL 2 BQL NA NA
3/7/1994 69.2 BQL 2 3 BQL NA NA
07/01/94 12.4 BQL BQL BQL BQL NA NA
10/23/95 24 BQL BQL BQL BQL NA NA02/11/97 31 4 2 6 3 NA 51
08/27/97 35 BQL BQL BQL BQL NA 91
11/20/97 6.9 BQL BQL BQL BQL NA 120
02/10/98 18 BQL BQL BQL BQL NA BQL
05/06/98 38 3 3.9 10 BQL NA 3908/04/98 64 2 7 19 5 BQL 170
11/02/98 4.1 2 BQL BQL BQL BQL 200
02/01/99 11 BQL BQL 1 1.8 BQL 6105/03/99 91 82 98 262 BQL BQL 5802/09/01 130 48 160 420 BQL NR NR
08/24/01 200 150 230 580 BQL NR NR
02/26/02 96 36 24 82 BQL NR NR
08/19/02 67 3 14 35 <2.0 NR NR02/05/03 100 27 21 72 18 NR NR
07/01/08 <0.31 <0.28 <0.31 <1.2 104 0.24 108
03/25/09 <0.55 <0.50 <0.65 <1.1 57 <1.0 9.1
4/22/2010 0.3 <0.1 1.2 0.98 37 0.11 98.411/30/2010 0.16 <0.1 0.41 <0.1 13 <0.1 15.7
5/25/2011 1.2 <0.1 4 10.5 9.9 <0.2 1954/9/2012
1 600 600 500 20 70 15
5,000 260,000 85,400 85,500 20,000 70,000 15,000
Notes:
1. "<" or ND = Not detected at or above the laboratory detection limit.
2. Concentrations are reported in micrograms per liter (ug/l) = parts per billion.
3. Concentrations in bold print equal or exceed the NCDENR 2L Standard (2L).
4. NCDENR = North Carolina Department of Environment and Natural Resources.
5. GCL = Gross Contaminantion Level.
6. MTBE = Methyl Tertiary Butyl Ether.
7. Gross Contamination Levels for Groundwater are referenced in the "Guidelines for Assessment and Corrective Action
for UST Releases", July 2008, Table 2, updated January 2010.
8. BQL = Below Quantitative Levels
9. NA = Not Analyzed
10. NR = Not Reported
Contaminant of Concern
NCDENR 2L Standard
GCL
MW-1
Destroyed
TABLE 5
HISTORICAL GROUNDWATER ANALYTICAL DATA
UNION COUNTRY CUPBOARD
836 NC ROUTE 461
UNION, HERTFORD COUNTY, NC
NCDENR INCIDENT NO. 10670
ATC PROJECT NO. 45.36019.0012
Page 19 of 33BenzeneTolueneEthylbenzeneTotal XylenesMTBEIPELeadBoring ID Sample Date ug/l ug/l ug/l ug/l ug/l ug/l ug/l
Contaminant of Concern
9/27/1993 BQL BQL BQL BQL BQL NA NA
3/7/1994 89 BQL BQL BQL BQL NA NA
07/01/94 2 BQL BQL BQL BQL NA NA
10/23/95 BQL BQL BQL BQL BQL NA NA
11/20/97 BQL BQL BQL BQL BQL NA 11
02/10/98 4 BQL BQL BQL BQL NA 11
05/06/98 BQL BQL BQL BQL BQL NA BQL
08/04/98 BQL BQL BQL BQL BQL BQL 1611/02/98 BQL BQL BQL BQL BQL BQL 4602/01/99 3.6 BQL BQL BQL BQL BQL 37
05/03/99 BQL BQL BQL BQL BQL BQL BQL
02/09/01 23 BQL 3.1 2.1 BQL NR NR
08/24/01 34 BQL BQL 4.5 BQL NR NR02/26/02 19 BQL 1.7 BQL BQL NR NR
08/19/02 1.3 <1.0 <1.0 <1.0 <1.0 NR NR
02/05/03 13 1.2 39 6.3 <5.0 NR NR
07/01/08 <0.31 <0.28 <0.31 <1.2 <0.12 <0.15 47.903/25/09 <0.55 <0.50 <0.65 <1.1 <0.50 <1.0 3.5
4/22/2010 NS NS NS NS NS NS NS
11/30/2010 NS NS NS NS NS NS NS
5/25/2011 <0.1 <0.1 <0.2 <0.2 <0.2 <0.2 37.24/9/2012 NS NS NS NS NS NS NS6/15/2014 <0.50 <0.50 <0.50 <1.5 <0.50 <0.50 NA
1 600 600 500 20 70 15
5,000 260,000 85,400 85,500 20,000 70,000 15,000
Notes:
1. "<" or ND = Not detected at or above the laboratory detection limit.
2. Concentrations are reported in micrograms per liter (ug/l) = parts per billion.
3. Concentrations in bold print equal or exceed the NCDENR 2L Standard (2L).
4. NCDENR = North Carolina Department of Environment and Natural Resources.
5. GCL = Gross Contaminantion Level.
6. MTBE = Methyl Tertiary Butyl Ether.
7. Gross Contamination Levels for Groundwater are referenced in the "Guidelines for Assessment and Corrective Action
for UST Releases", July 2008, Table 2, updated January 2010.
8. MW-3 was replaced on 4/26/2010
9. BQL = Below Quantitative Levels
10. NA = Not Analyzed
11. NR = Not Reported
MW-2
NCDENR 2L Standard
GCL
TABLE 5
HISTORICAL GROUNDWATER ANALYTICAL DATA
UNION COUNTRY CUPBOARD
836 NC ROUTE 461
UNION, HERTFORD COUNTY, NC
NCDENR INCIDENT NO. 10670
ATC PROJECT NO. 45.36019.0012
Page 20 of 33BenzeneTolueneEthylbenzeneTotal XylenesMTBEIPELeadBoring ID Sample Date ug/l ug/l ug/l ug/l ug/l ug/l ug/l
Contaminant of Concern
9/27/1993 3.77 3.39 2.29 5.16 BQL NA NA
3/7/1994 539 154 32.4 106 BQL NA NA
07/01/94 239 BQL 4.3 12.7 6.41 NA NA
10/23/95 160 3.5 3.9 17 BQL NA NA02/11/97 460 11 BQL 12 BQL NA 32
08/27/97 580 <10 <10 44 10 NA 82
11/20/97 270 BQL 43 13 BQL NA 92
02/10/98 90 BQL 4 18 BQL NA 15
05/06/98 1,800 140 160 420 BQL NA BQL08/04/98 1,100 100 270 1,940 250 170 14
11/02/98 490 86 BQL BQL BQL BQL 73
02/01/99 170 61 24 69 BQL BQL 2605/03/99 1,100 150 170 500 BQL BQL 1411/01/99 1,700 14 13 45 BQL BQL NR
02/09/01 2,400 160 230 570 BQL NR NR
08/24/01 1,600 65 160 260 BQL NR NR
02/26/02 680 34 50 104 BQL NR NR08/19/02 340 <10 15 <10 <10 NR NR
02/05/03 780 57 81 180 56 NR NR
4/22/2010 0.96 <0.1 0.61 0.12 7.4 0.31 234
11/30/2010 <0.1 <0.1 <0.1 <0.1 13 0.41 6145/25/2011 1.3 <0.1 <0.2 <0.2 16 0.39 223
4/9/2012 0.11 <0.1 <0.1 <0.3 14 0.32 NA6/15/2014 0.25 J <0.50 <0.50 <1.5 9.6 0.20 J NA
1 600 600 500 20 70 15
5,000 260,000 85,400 85,500 20,000 70,000 15,000
Notes:
1. "<" or ND = Not detected at or above the laboratory detection limit.
2. Concentrations are reported in micrograms per liter (ug/l) = parts per billion.
3. Concentrations in bold print equal or exceed the NCDENR 2L Standard (2L).
4. NCDENR = North Carolina Department of Environment and Natural Resources.
5. GCL = Gross Contaminantion Level.
6. MTBE = Methyl Tertiary Butyl Ether.
7. Gross Contamination Levels for Groundwater are referenced in the "Guidelines for Assessment and Corrective Action
for UST Releases", July 2008, Table 2, updated January 2010.
8. BQL = Below Quantitative Levels
9. NA = Not Analyzed
10. NR = Not Reported
MW-3
RMW-3
NCDENR 2L Standard
GCL
TABLE 5
HISTORICAL GROUNDWATER ANALYTICAL DATA
UNION COUNTRY CUPBOARD
836 NC ROUTE 461
UNION, HERTFORD COUNTY, NC
NCDENR INCIDENT NO. 10670
ATC PROJECT NO. 45.36019.0012
Page 21 of 33BenzeneTolueneEthylbenzeneTotal XylenesMTBEIPELeadBoring ID Sample Date ug/l ug/l ug/l ug/l ug/l ug/l ug/l
Contaminant of Concern
3/7/1994 3,124 4,270 659 3,200 6,330 NA NA
07/01/94 4,020 2,100 290 1,070 1,840 NA NA
10/23/95 5,100 940 220 440 19,000 NA NA
02/11/97 3,600 1,700 BQL 1,600 16,000 NA 13.608/27/97 4,400 560 260 440 20,000 NA 103
11/20/97 8,400 1,200 2,000 2,900 25,000 NA 42
02/10/98 12,000 8,200 BQL BQL 38,000 NA 19
05/06/98 9,500 4,400 1,400 4,200 20,000 NA 1708/04/98 18,000 9,200 1,800 7,900 68,000 BQL 3811/02/98 8,300 3,200 1,400 3,700 10,000 BQL 82
02/01/99 4,100 1,400 600 1,620 30,000 BQL 47
05/03/99 11,000 3,600 1,400 4,400 34,000 BQL 2408/23/99 8,800 560 BQL 670 20,000 NR NR11/01/99 7,400 1,000 830 1,630 15,000 BQL NR
02/03/00 9,000 2,200 1,100 3,100 22,000 NR NR
05/01/00 11,000 4,100 1,600 5,700 26,000 NR NR
08/21/00 7,100 1,200 980 2,710 16,000 NR NR11/10/00 8,600 940 1,100 2,530 20,000 NR NR
02/02/01 11,000 3,400 1,500 4,600 25,000 NR NR
05/14/01 9,800 11,000 2,000 7,800 28,000 NR NR
08/24/01 2,700 980 BQL 2,580 7,100 NR NR02/26/02 10,000 6,800 2,000 7,700 34,000 NR NR
08/19/02 8,000 1,900 1,500 3,530 17,000 NR NR
02/05/03 9,400 4,100 1,600 5,000 20,000 NR NR
07/01/08 2,480 524 361 975 9,860 12.9 70.403/25/09 1,800 660 390 1,200 8,100 <20 1.7J
4/22/2010 620 190 80 238 9,500 9.4 74.3
11/30/2010 2,300 50 57 87 5,900 9.8 76.9
5/25/2011 2,800 750 440 1,430 8,400 <10 15.54/9/2012 1,900 120 380 670 4,400 <10 NA6/15/2014 3,350 1,180 757 2,000 4,990 14.5 NA
1 600 600 500 20 70 15
5,000 260,000 85,400 85,500 20,000 70,000 15,000
Notes:
1. "<" or ND = Not detected at or above the laboratory detection limit.
2. Concentrations are reported in micrograms per liter (ug/l) = parts per billion.
3. Concentrations in bold print equal or exceed the NCDENR 2L Standard (2L).
4. NCDENR = North Carolina Department of Environment and Natural Resources.
5. GCL = Gross Contaminantion Level.
6. MTBE = Methyl Tertiary Butyl Ether.
7. Gross Contamination Levels for Groundwater are referenced in the "Guidelines for Assessment and Corrective Action
for UST Releases", July 2008, Table 2, updated January 2010.
8. BQL = Below Quantitative Levels
9. NA = Not Analyzed
10. NR = Not Reported
NCDENR 2L Standard
GCL
MW-4
TABLE 5
HISTORICAL GROUNDWATER ANALYTICAL DATA
UNION COUNTRY CUPBOARD
836 NC ROUTE 461
UNION, HERTFORD COUNTY, NC
NCDENR INCIDENT NO. 10670
ATC PROJECT NO. 45.36019.0012
Page 22 of 33BenzeneTolueneEthylbenzeneTotal XylenesMTBEIPELeadBoring ID Sample Date ug/l ug/l ug/l ug/l ug/l ug/l ug/l
Contaminant of Concern
3/7/1994 8.17 BQL BQL 1.42 BQL NA NA
07/01/94 76.8 BQL BQL BQL BQL NA NA
10/23/95 32 1 BQL 1 9.7 NA NA
02/11/97 45 3 4 20 BQL NA BQL08/27/97 140 6 8 84 <2.0 NA BQL
11/20/97 170 10 8.2 38 BQL NA 20
02/10/98 68 8 12 75 BQL NA BQL
05/06/98 86 2.8 12 45 BQL NA BQL
08/04/98 290 4 32 82 12 6 2811/02/98 130 14 65 68 BQL BQL 79
02/01/99 220 8.6 58 62.6 11 BQL 18
05/03/99 120 7.4 41 45.6 12 BQL BQL
11/01/99 190 BQL 57 32 31 BQL NR02/09/01 88 1.6 13 17.9 BQL NR NR
08/24/01 170 20 48 112 BQL NR NR
02/26/02 160 BQL 31 38 BQL NR NR
08/19/02 16 <1.0 4.8 2.4 <1.0 NR NR02/05/03 380 31 150 190 <50 NR NR
07/01/08 <0.31 <0.28 <0.31 <1.2 23.6 <0.15 <2.2
03/25/09 <0.55 <0.50 <0.65 <1.1 8.0 <1.0 20.4
4/22/2010 <0.1 <0.1 <0.1 <0.2 3.8 <0.1 43811/30/2010 <0.1 <0.1 <0.1 <0.1 2.8 <0.1 2.61
5/25/2011 <0.1 <0.1 <0.2 <0.2 1.3 <0.2 <10
4/9/2012 <0.1 <0.1 <0.1 <0.3 0.9 <0.2 NA6/15/2014 <0.50 <0.50 <0.50 <1.5 0.26 J <0.50 NA
1 600 600 500 20 70 15
5,000 260,000 85,400 85,500 20,000 70,000 15,000
Notes:
1. "<" or ND = Not detected at or above the laboratory detection limit.
2. Concentrations are reported in micrograms per liter (ug/l) = parts per billion.
3. Concentrations in bold print equal or exceed the NCDENR 2L Standard (2L).
4. NCDENR = North Carolina Department of Environment and Natural Resources.
5. GCL = Gross Contaminantion Level.
6. MTBE = Methyl Tertiary Butyl Ether.
7. Gross Contamination Levels for Groundwater are referenced in the "Guidelines for Assessment and Corrective Action
for UST Releases", July 2008, Table 2, updated January 2010.
8. BQL = Below Quantitative Levels
9. NA = Not Analyzed
10. NR = Not Reported
NCDENR 2L Standard
GCL
MW-5
TABLE 5
HISTORICAL GROUNDWATER ANALYTICAL DATA
UNION COUNTRY CUPBOARD
836 NC ROUTE 461
UNION, HERTFORD COUNTY, NC
NCDENR INCIDENT NO. 10670
ATC PROJECT NO. 45.36019.0012
Page 23 of 33BenzeneTolueneEthylbenzeneTotal XylenesMTBEIPELeadBoring ID Sample Date ug/l ug/l ug/l ug/l ug/l ug/l ug/l
Contaminant of Concern
07/01/94 7 BQL 2.05 9 BQL NA NA
10/23/95 BQL BQL BQL BQL BQL NA NA
02/11/97 BQL BQL BQL BQL BQL NA BQL
08/27/97 BQL BQL BQL BQL BQL NA BQL
11/20/97 BQL BQL BQL BQL BQL NA BQL
02/10/98 BQL BQL BQL BQL BQL NA BQL
05/06/98 BQL BQL BQL BQL BQL NA BQL
08/04/98 BQL BQL BQL BQL BQL BQL BQL
11/02/98 BQL BQL BQL BQL BQL BQL BQL02/01/99 2.2 1.9 1.2 8 BQL BQL BQL
05/03/99 BQL BQL BQL BQL BQL BQL BQL
08/23/99 BQL BQL BQL BQL BQL NR NR
11/01/99 1.6 BQL BQL BQL BQL BQL NR02/03/00 BQL BQL BQL BQL BQL NR NR
05/01/00 BQL BQL BQL BQL BQL NR NR
08/21/00 BQL BQL BQL BQL BQL NR NR
11/10/00 BQL BQL BQL BQL BQL NR NR02/02/01 2.1 2.1 BQL 2.4 5.7 NR NR
08/24/01 BQL BQL BQL BQL BQL NR NR
08/19/02 <1.0 <1.0 <1.0 <1.0 <1.0 NR NR
02/05/03 <1.0 <1.0 <1.0 <3.0 <5.0 NR NR07/01/08 0.81 <0.28 <0.31 <1.2 15.6 <0.15 <2.2
03/25/09 1.0J 0.60J <0.65 <1.1 35 <1.0 9.6
4/22/2010 12 0.1 1.3 4.2 27 0.2 6.96
11/30/2010 1.6 0.25 0.3 0.47 38 0.36 4.215/25/2011 <0.1 <0.1 <0.2 <0.2 27 0.32 <10
4/9/2012 NS NS NS NS NS NS NS6/15/2014 0.38 J <0.50 <0.50 <1.5 12.5 0.18 J NA
1 600 600 500 20 70 15
5,000 260,000 85,400 85,500 20,000 70,000 15,000
Notes:
1. "<" or ND = Not detected at or above the laboratory detection limit.
2. Concentrations are reported in micrograms per liter (ug/l) = parts per billion.
3. Concentrations in bold print equal or exceed the NCDENR 2L Standard (2L).
4. NCDENR = North Carolina Department of Environment and Natural Resources.
5. GCL = Gross Contaminantion Level.
6. MTBE = Methyl Tertiary Butyl Ether.
7. Gross Contamination Levels for Groundwater are referenced in the "Guidelines for Assessment and Corrective Action
for UST Releases", July 2008, Table 2, updated January 2010.
8. BQL = Below Quantitative Levels
9. NA = Not Analyzed
10. NR = Not Reported
GCL
MW-6D
NCDENR 2L Standard
TABLE 5
HISTORICAL GROUNDWATER ANALYTICAL DATA
UNION COUNTRY CUPBOARD
836 NC ROUTE 461
UNION, HERTFORD COUNTY, NC
NCDENR INCIDENT NO. 10670
ATC PROJECT NO. 45.36019.0012
Page 24 of 33BenzeneTolueneEthylbenzeneTotal XylenesMTBEIPELeadBoring ID Sample Date ug/l ug/l ug/l ug/l ug/l ug/l ug/l
Contaminant of Concern
07/01/94 BQL BQL BQL BQL BQL NA NA
10/23/95 BQL BQL BQL BQL BQL NA NA
02/11/97 BQL BQL BQL BQL BQL NA BQL
08/27/97 BQL BQL BQL BQL BQL NA 13111/20/97 BQL BQL BQL BQL BQL NA 120
02/10/98 BQL BQL BQL BQL BQL NA 52
05/06/98 BQL BQL BQL BQL BQL NA 37
11/02/98 BQL BQL BQL BQL BQL BQL 6702/01/99 BQL BQL BQL BQL BQL BQL 5705/03/99 BQL BQL BQL BQL BQL BQL 13
11/01/99 BQL BQL BQL BQL BQL BQL NR
02/09/01 BQL BQL BQL BQL BQL NR NR
08/24/01 BQL BQL BQL BQL BQL NR NR08/19/02 <1.0 <1.0 <1.0 <1.0 <1.0 NR NR
02/05/03 <1.0 <1.0 <1.0 <3.0 <5.0 NR NR
07/01/08 NS NS NS NS NS NS NS
03/25/09 <0.55 <0.50 <0.65 <1.1 <0.50 <1.0 51.04/22/2010 NS NS NS NS NS NS NS
11/30/2010 NS NS NS NS NS NS NS
5/25/2011 NS NS NS NS NS NS NS
4/9/2012 NS NS NS NS NS NS NS6/15/2014 NS NS NS NS NS NS NS
1 600 600 500 20 70 15
5,000 260,000 85,400 85,500 20,000 70,000 15,000
Notes:
1. "<" or ND = Not detected at or above the laboratory detection limit.
2. Concentrations are reported in micrograms per liter (ug/l) = parts per billion.
3. Concentrations in bold print equal or exceed the NCDENR 2L Standard (2L).
4. NCDENR = North Carolina Department of Environment and Natural Resources.
5. GCL = Gross Contaminantion Level.
6. MTBE = Methyl Tertiary Butyl Ether.
7. Gross Contamination Levels for Groundwater are referenced in the "Guidelines for Assessment and Corrective Action
for UST Releases", July 2008, Table 2, updated January 2010.
8. BQL = Below Quantitative Levels
9. NA = Not Analyzed
10. NR = Not Reported
MW-7
NCDENR 2L Standard
GCL
TABLE 5
HISTORICAL GROUNDWATER ANALYTICAL DATA
UNION COUNTRY CUPBOARD
836 NC ROUTE 461
UNION, HERTFORD COUNTY, NC
NCDENR INCIDENT NO. 10670
ATC PROJECT NO. 45.36019.0012
Page 25 of 33BenzeneTolueneEthylbenzeneTotal XylenesMTBEIPELeadBoring ID Sample Date ug/l ug/l ug/l ug/l ug/l ug/l ug/l
Contaminant of Concern
07/01/94 BQL BQL BQL BQL BQL NA NA
11/20/97 BQL BQL BQL BQL BQL NA BQL
Destroyed NA NA NA NA NA NA NA
02/10/98 BQL BQL BQL BQL BQL NA 12
05/06/98 BQL BQL BQL BQL BQL NA 21
08/04/98 BQL BQL BQL BQL BQL BQL 35
11/02/98 BQL BQL BQL BQL BQL BQL 160
02/01/99 BQL BQL BQL BQL BQL BQL 1705/03/99 BQL BQL BQL BQL BQL BQL BQL08/23/99 BQL BQL BQL BQL BQL NR NR
11/01/99 BQL BQL BQL BQL BQL BQL NR
02/03/00 BQL BQL BQL BQL BQL NR NR
05/01/00 BQL BQL BQL BQL BQL NR NR08/21/00 BQL BQL BQL BQL BQL NR NR
11/10/00 BQL BQL BQL BQL BQL NR NR
02/02/01 BQL BQL BQL BQL BQL NR NR
05/14/01 BQL BQL BQL BQL BQL NR NR08/24/01 BQL BQL BQL BQL BQL NR NR
08/19/02 <1.0 <1.0 <1.0 <1.0 <1.0 NR NR
02/05/03 <1.0 <1.0 <1.0 <3.0 <5.0 NR NR
07/01/08 <0.31 <0.28 <0.31 <1.2 0.13J <0.15 14003/25/09 <0.55 <0.50 <0.65 <1.1 <0.50 <1.0 9.9
4/22/2010 <0.1 <0.1 <0.1 <0.2 <0.2 <0.1 48
11/30/2010 <0.1 <0.1 <0.1 <0.1 <0.2 <0.1 177
5/25/2011 <0.1 <0.1 <0.2 <0.2 0.5 <0.2 84.24/9/2012 NS NS NS NS NS NS NS6/15/2014 <0.50 <0.50 <0.50 <1.5 <0.50 <0.50 NA
1 600 600 500 20 70 15
5,000 260,000 85,400 85,500 20,000 70,000 15,000
Notes:
1. "<" or ND = Not detected at or above the laboratory detection limit.
2. Concentrations are reported in micrograms per liter (ug/l) = parts per billion.
3. Concentrations in bold print equal or exceed the NCDENR 2L Standard (2L).
4. NCDENR = North Carolina Department of Environment and Natural Resources.
5. GCL = Gross Contaminantion Level.
6. MTBE = Methyl Tertiary Butyl Ether.
7. Gross Contamination Levels for Groundwater are referenced in the "Guidelines for Assessment and Corrective Action
for UST Releases", July 2008, Table 2, updated January 2010.
8. BQL = Below Quantitative Levels
9. NA = Not Analyzed
10. NR = Not Reported
GCL
NCDENR 2L Standard
MW-8A
TABLE 5
HISTORICAL GROUNDWATER ANALYTICAL DATA
UNION COUNTRY CUPBOARD
836 NC ROUTE 461
UNION, HERTFORD COUNTY, NC
NCDENR INCIDENT NO. 10670
ATC PROJECT NO. 45.36019.0012
Page 26 of 33BenzeneTolueneEthylbenzeneTotal XylenesMTBEIPELeadBoring ID Sample Date ug/l ug/l ug/l ug/l ug/l ug/l ug/l
Contaminant of Concern
10/23/95 1.4 8.6 1.4 10 BQL NA NA
02/11/97 BQL 1.3 BQL BQL BQL NA 72.9
08/27/97 BQL BQL BQL BQL BQL NA 72.4
11/20/97 BQL BQL BQL BQL BQL NA 14002/10/98 BQL BQL BQL BQL BQL NA 38
05/06/98 BQL BQL BQL BQL BQL NA BQL
08/04/98 BQL BQL BQL BQL BQL BQL 73
11/02/98 BQL BQL BQL BQL BQL BQL 8002/01/99 BQL BQL BQL BQL BQL BQL 7505/03/99 BQL BQL BQL BQL BQL BQL 37
11/01/99 BQL BQL BQL BQL BQL BQL NR
02/09/01 BQL BQL BQL BQL BQL NR NR
08/24/01 BQL BQL BQL BQL BQL NR NR08/19/02 <1.0 <1.0 <1.0 <1.0 <1.0 NR NR
02/05/03 <1.0 <1.0 <1.0 <3.0 <5.0 NR NR
07/01/08 <0.31 <0.28 <0.31 <1.2 <0.12 <0.15 118
03/25/09 <0.55 <0.50 <0.65 <1.1 <0.50 <1.0 12.94/22/2010 NS NS NS NS NS NS NS
11/30/2010 <0.1 <0.1 <0.1 <0.1 <0.2 <0.1 34.8
5/25/2011 <0.1 <0.1 <0.2 <0.2 <0.2 <0.2 16.8
4/9/2012 NS NS NS NS NS NS NS6/15/2014 <0.50 <0.50 <0.50 <1.5 <0.50 <0.50 NA
1 600 600 500 20 70 15
5,000 260,000 85,400 85,500 20,000 70,000 15,000
Notes:
1. "<" or ND = Not detected at or above the laboratory detection limit.
2. Concentrations are reported in micrograms per liter (ug/l) = parts per billion.
3. Concentrations in bold print equal or exceed the NCDENR 2L Standard (2L).
4. NCDENR = North Carolina Department of Environment and Natural Resources.
5. GCL = Gross Contaminantion Level.
6. MTBE = Methyl Tertiary Butyl Ether.
7. Gross Contamination Levels for Groundwater are referenced in the "Guidelines for Assessment and Corrective Action
for UST Releases", July 2008, Table 2, updated January 2010.
8. BQL = Below Quantitative Levels
9. NA = Not Analyzed
10. NR = Not Reported
MW-9
NCDENR 2L Standard
GCL
TABLE 5
HISTORICAL GROUNDWATER ANALYTICAL DATA
UNION COUNTRY CUPBOARD
836 NC ROUTE 461
UNION, HERTFORD COUNTY, NC
NCDENR INCIDENT NO. 10670
ATC PROJECT NO. 45.36019.0012
Page 27 of 33BenzeneTolueneEthylbenzeneTotal XylenesMTBEIPELeadBoring ID Sample Date ug/l ug/l ug/l ug/l ug/l ug/l ug/l
Contaminant of Concern
10/23/95 BQL BQL BQL BQL BQL NA NA
02/11/97 BQL 1.8 BQL BQL BQL NA BQL
08/27/97 BQL BQL BQL BQL BQL NA BQL
11/20/97 BQL BQL BQL BQL BQL NA BQL
02/10/98 BQL BQL BQL BQL BQL NA BQL
05/06/98 BQL BQL BQL BQL BQL NA 61
08/04/98 BQL BQL BQL BQL BQL BQL BQL11/02/98 BQL BQL BQL BQL BQL BQL 1305/03/99 BQL BQL BQL BQL BQL BQL BQL
11/01/99 BQL BQL BQL BQL BQL BQL NR
02/09/01 BQL BQL BQL BQL BQL NR NR
08/24/01 BQL BQL BQL BQL BQL NR NR08/19/02 <1.0 <1.0 <1.0 <1.0 <1.0 NR NR
02/05/03 <1.0 <1.0 <1.0 <3.0 <5.0 NR NR
07/01/08 NS NS NS NS NS NS NS
03/25/09 NS NS NS NS NS NS NS4/22/2010 NS NS NS NS NS NS NS
11/30/2010 NS NS NS NS NS NS NS
5/25/2011 NS NS NS NS NS NS NS
4/9/2012 NS NS NS NS NS NS NS6/15/2014 NS NS NS NS NS NS NS
1 600 600 500 20 70 15
5,000 260,000 85,400 85,500 20,000 70,000 15,000
Notes:
1. "<" or ND = Not detected at or above the laboratory detection limit.
2. Concentrations are reported in micrograms per liter (ug/l) = parts per billion.
3. Concentrations in bold print equal or exceed the NCDENR 2L Standard (2L).
4. NCDENR = North Carolina Department of Environment and Natural Resources.
5. GCL = Gross Contaminantion Level.
6. MTBE = Methyl Tertiary Butyl Ether.
7. Gross Contamination Levels for Groundwater are referenced in the "Guidelines for Assessment and Corrective Action
for UST Releases", July 2008, Table 2, updated January 2010.
8. BQL = Below Quantitative Levels
9. NA = Not Analyzed
10. NR = Not Reported
GCL
NCDENR 2L Standard
MW-10
TABLE 5
HISTORICAL GROUNDWATER ANALYTICAL DATA
UNION COUNTRY CUPBOARD
836 NC ROUTE 461
UNION, HERTFORD COUNTY, NC
NCDENR INCIDENT NO. 10670
ATC PROJECT NO. 45.36019.0012
Page 28 of 33BenzeneTolueneEthylbenzeneTotal XylenesMTBEIPELeadBoring ID Sample Date ug/l ug/l ug/l ug/l ug/l ug/l ug/l
Contaminant of Concern
10/23/95 BQL BQL BQL BQL BQL NA NA
02/11/97 BQL BQL BQL BQL BQL NA BQL
08/27/97 BQL BQL BQL BQL BQL NA BQL
11/20/97 BQL BQL BQL BQL BQL NA BQL
02/10/98 BQL BQL BQL BQL BQL NA BQL
05/06/98 BQL BQL BQL BQL BQL NA BQL
08/04/98 BQL BQL BQL BQL BQL BQL 10
11/02/98 BQL BQL BQL BQL BQL BQL BQL
02/01/99 BQL BQL BQL BQL BQL BQL BQL05/03/99 BQL BQL BQL BQL BQL BQL 10
08/23/99 BQL BQL BQL BQL BQL NR NR
11/01/99 BQL BQL BQL BQL BQL BQL NR
02/03/00 BQL BQL BQL BQL BQL NR NR05/01/00 BQL BQL BQL BQL BQL NR NR
08/21/00 BQL BQL BQL BQL BQL NR NR
11/10/00 BQL BQL BQL BQL BQL NR NR
02/02/01 BQL BQL BQL BQL BQL NR NR05/14/01 BQL BQL BQL BQL BQL NR NR
08/24/01 BQL BQL BQL BQL BQL NR NR
08/19/02 <1.0 <1.0 <1.0 <1.0 <1.0 NR NR
02/05/03 <1.0 <1.0 1.2 <3.0 <5.0 NR NR07/01/08 <0.31 <0.28 <0.31 <1.2 <0.12 <0.15 28.7
03/25/09 <0.55 <0.50 <0.65 <1.1 <0.50 <1.0 6.6
4/22/2010 <0.1 <0.1 <0.1 <0.2 <0.2 <0.1 10.8
11/30/2010 0.13 <0.1 <0.1 <0.1 <0.2 <0.1 8.45/25/2011 <0.1 <0.1 <0.2 <0.2 <0.2 <0.2 <10
4/9/2012 NS NS NS NS NS NS NS6/15/2014 NS NS NS NS NS NS NS
1 600 600 500 20 70 15
5,000 260,000 85,400 85,500 20,000 70,000 15,000
Notes:
1. "<" or ND = Not detected at or above the laboratory detection limit.
2. Concentrations are reported in micrograms per liter (ug/l) = parts per billion.
3. Concentrations in bold print equal or exceed the NCDENR 2L Standard (2L).
4. NCDENR = North Carolina Department of Environment and Natural Resources.
5. GCL = Gross Contaminantion Level.
6. MTBE = Methyl Tertiary Butyl Ether.
7. Gross Contamination Levels for Groundwater are referenced in the "Guidelines for Assessment and Corrective Action
for UST Releases", July 2008, Table 2, updated January 2010.
8. BQL = Below Quantitative Levels
9. NA = Not Analyzed
10. NR = Not Reported
NCDENR 2L Standard
GCL
MW-11
TABLE 5
HISTORICAL GROUNDWATER ANALYTICAL DATA
UNION COUNTRY CUPBOARD
836 NC ROUTE 461
UNION, HERTFORD COUNTY, NC
NCDENR INCIDENT NO. 10670
ATC PROJECT NO. 45.36019.0012
Page 29 of 33BenzeneTolueneEthylbenzeneTotal XylenesMTBEIPELeadBoring ID Sample Date ug/l ug/l ug/l ug/l ug/l ug/l ug/l
Contaminant of Concern
10/23/95 BQL BQL BQL BQL BQL NA NA
02/11/97 BQL BQL BQL BQL BQL NA BQL
08/27/97 BQL BQL BQL BQL BQL NA 15.7
11/20/97 BQL BQL BQL BQL BQL NA 14
02/10/98 BQL BQL BQL BQL BQL NA BQL
05/06/98 BQL BQL BQL BQL BQL NA BQL
08/04/98 BQL BQL BQL BQL BQL BQL 24
11/02/98 BQL BQL BQL BQL BQL BQL 3602/01/99 BQL BQL BQL BQL BQL BQL 1205/03/99 BQL BQL BQL BQL BQL BQL 10
08/23/99 BQL BQL BQL BQL BQL NR NR
11/01/99 BQL BQL BQL BQL BQL BQL NR
02/03/00 BQL BQL BQL BQL BQL NR NR05/01/00 BQL BQL BQL BQL BQL NR NR
08/21/00 BQL BQL BQL BQL BQL NR NR
11/10/00 BQL BQL BQL BQL BQL NR NR
02/02/01 BQL BQL BQL BQL BQL NR NR05/14/01 BQL BQL BQL BQL BQL NR NR
08/24/01 BQL BQL BQL BQL BQL NR NR
08/19/02 <1.0 <1.0 <1.0 <1.0 <1.0 NR NR
02/05/03 <1.0 <1.0 <1.0 <3.0 <5.0 NR NR07/01/08 <0.31 <0.28 <0.31 <1.2 <0.12 <0.15 57.2
03/25/09 <0.55 <0.50 <0.65 <1.1 <0.50 <1.0 13.9
4/22/2010 <0.1 <0.1 <0.1 <0.2 <0.2 <0.1 17.1
11/30/2010 <0.1 <0.1 <0.1 <0.1 <0.2 <0.1 96.35/25/2011 <0.1 <0.1 <0.2 <0.2 <0.2 <0.2 38.4
4/9/2012 NS NS NS NS NS NS NS6/15/2014 <0.50 <0.50 <0.50 <1.5 <0.50 <0.50 NA
1 600 600 500 20 70 15
5,000 260,000 85,400 85,500 20,000 70,000 15,000
Notes:
1. "<" or ND = Not detected at or above the laboratory detection limit.
2. Concentrations are reported in micrograms per liter (ug/l) = parts per billion.
3. Concentrations in bold print equal or exceed the NCDENR 2L Standard (2L).
4. NCDENR = North Carolina Department of Environment and Natural Resources.
5. GCL = Gross Contaminantion Level.
6. MTBE = Methyl Tertiary Butyl Ether.
7. Gross Contamination Levels for Groundwater are referenced in the "Guidelines for Assessment and Corrective Action
for UST Releases", July 2008, Table 2, updated January 2010.
8. BQL = Below Quantitative Levels
9. NA = Not Analyzed
10. NR = Not Reported
MW-12
NCDENR 2L Standard
GCL
TABLE 5
HISTORICAL GROUNDWATER ANALYTICAL DATA
UNION COUNTRY CUPBOARD
836 NC ROUTE 461
UNION, HERTFORD COUNTY, NC
NCDENR INCIDENT NO. 10670
ATC PROJECT NO. 45.36019.0012
Page 30 of 33BenzeneTolueneEthylbenzeneTotal XylenesMTBEIPELeadBoring ID Sample Date ug/l ug/l ug/l ug/l ug/l ug/l ug/l
Contaminant of Concern
10/23/95 BQL BQL BQL BQL BQL NA NA
08/27/97 BQL BQL BQL BQL BQL NA 11.5
11/20/97 BQL BQL BQL BQL BQL NA BQL
02/10/98 BQL BQL BQL BQL BQL NA BQL
05/06/98 BQL BQL BQL BQL BQL NA BQL
08/04/98 BQL BQL BQL BQL BQL BQL BQL
11/02/98 BQL BQL BQL BQL BQL BQL BQL
02/01/99 BQL BQL BQL BQL BQL BQL BQL
05/03/99 BQL BQL BQL BQL BQL BQL BQL11/01/99 BQL BQL BQL BQL BQL BQL NR
02/09/01 BQL BQL BQL BQL BQL NR NR
08/24/01 BQL BQL BQL BQL BQL NR NR
08/19/02 <1.0 <1.0 <1.0 <1.0 <1.0 NR NR02/05/03 <1.0 <1.0 <1.0 <3.0 <5.0 NR NR
07/01/08 <0.31 <0.28 <0.31 <1.2 <0.12 <0.15 24.8
03/25/09 <0.55 <0.50 <0.65 <1.1 <0.50 <1.0 6.0
4/22/2010 <0.1 <0.1 <0.1 <0.1 <0.2 <0.1 <411/30/2010 <0.1 <0.1 <0.1 <0.1 <0.2 <0.1 11
5/25/2011 <0.1 <0.1 <0.2 <0.2 <0.2 <0.2 <10
4/9/2012 NS NS NS NS NS NS NS6/15/2014 NS NS NS NS NS NS NS
1 600 600 500 20 70 15
5,000 260,000 85,400 85,500 20,000 70,000 15,000
Notes:
1. "<" or ND = Not detected at or above the laboratory detection limit.
2. Concentrations are reported in micrograms per liter (ug/l) = parts per billion.
3. Concentrations in bold print equal or exceed the NCDENR 2L Standard (2L).
4. NCDENR = North Carolina Department of Environment and Natural Resources.
5. GCL = Gross Contaminantion Level.
6. MTBE = Methyl Tertiary Butyl Ether.
7. Gross Contamination Levels for Groundwater are referenced in the "Guidelines for Assessment and Corrective Action
for UST Releases", July 2008, Table 2, updated January 2010.
8. BQL = Below Quantitative Levels
9. NA = Not Analyzed
10. NR = Not Reported
GCL
NCDENR 2L Standard
MW-13
TABLE 5
HISTORICAL GROUNDWATER ANALYTICAL DATA
UNION COUNTRY CUPBOARD
836 NC ROUTE 461
UNION, HERTFORD COUNTY, NC
NCDENR INCIDENT NO. 10670
ATC PROJECT NO. 45.36019.0012
Page 31 of 33BenzeneTolueneEthylbenzeneTotal XylenesMTBEIPELeadBoring ID Sample Date ug/l ug/l ug/l ug/l ug/l ug/l ug/l
Contaminant of Concern
10/23/95 BQL BQL BQL BQL BQL NA NA
08/27/97 BQL BQL BQL BQL BQL NA BQL
11/20/97 BQL BQL BQL BQL BQL NA BQL
02/10/98 BQL BQL BQL BQL BQL NA BQL
05/06/98 BQL BQL BQL BQL BQL NA BQL
08/04/98 BQL BQL BQL BQL BQL BQL 14
11/02/98 BQL BQL BQL BQL BQL BQL 13
02/01/99 BQL BQL BQL BQL BQL BQL 5805/03/99 BQL 4 BQL BQL BQL BQL 6408/19/02 <1.0 <1.0 <1.0 1.9 <1.0 NR NR
02/05/03 <1.0 <1.0 <1.0 <3.0 <5.0 NR NR
07/01/08 <0.31 <0.28 <0.31 <1.2 <0.12 <0.15 12.6
03/25/09 <0.55 <0.50 <0.65 <1.1 <0.50 <1.0 20.64/22/2010 <0.1 <0.1 <0.1 <0.2 <0.2 <0.1 11.3
11/30/2010 <0.1 <0.1 <0.1 <0.1 <0.2 <0.1 5.86
5/25/2011 NS NS NS NS NS NS NS
4/9/2012 NS NS NS NS NS NS NS6/15/2014 NS NS NS NS NS NS NS
MW-15 03/25/09 <0.55 <0.50 <0.65 <1.1 <0.50 <1.0 49.2
4/22/2010 NS NS NS NS NS NS NS
11/30/2010 NS NS NS NS NS NS NS5/25/2011 NS NS NS NS NS NS NS
4/9/2012 NS NS NS NS NS NS NS6/15/2014 NS NS NS NS NS NS NS
1 600 600 500 20 70 15
5,000 260,000 85,400 85,500 20,000 70,000 15,000
Notes:
1. "<" or ND = Not detected at or above the laboratory detection limit.
2. Concentrations are reported in micrograms per liter (ug/l) = parts per billion.
3. Concentrations in bold print equal or exceed the NCDENR 2L Standard (2L).
4. NCDENR = North Carolina Department of Environment and Natural Resources.
5. GCL = Gross Contaminantion Level.
6. MTBE = Methyl Tertiary Butyl Ether.
7. Gross Contamination Levels for Groundwater are referenced in the "Guidelines for Assessment and Corrective Action
for UST Releases", July 2008, Table 2, updated January 2010.
8. BQL = Below Quantitative Levels
9. NA = Not Analyzed
10. NR = Not Reported
11. NS = Not Sampled
GCL
MW-14A
NCDENR 2L Standard
TABLE 5
HISTORICAL GROUNDWATER ANALYTICAL DATA
UNION COUNTRY CUPBOARD
836 NC ROUTE 461
UNION, HERTFORD COUNTY, NC
NCDENR INCIDENT NO. 10670
ATC PROJECT NO. 45.36019.0012
Page 32 of 33BenzeneTolueneEthylbenzeneTotal XylenesMTBEIPELeadBoring ID Sample Date ug/l ug/l ug/l ug/l ug/l ug/l ug/l
Contaminant of Concern
MW-16 03/25/09 <0.55 <0.50 <0.65 <1.1 <0.50 <1.0 7.5
4/22/2010 NS NS NS NS NS NS NS
11/30/2010 NS NS NS NS NS NS NS
5/25/2011 NS NS NS NS NS NS NS
4/9/2012 NS NS NS NS NS NS NS6/15/2014 <0.50 <0.50 <0.50 <1.5 <0.50 <0.50 NA
MW-17 03/25/09 <0.55 <0.50 <0.65 <1.1 0.75J <1.0 1.5
4/22/2010 NS NS NS NS NS NS NS
11/30/2010 NS NS NS NS NS NS NS5/25/2011 NS NS NS NS NS NS NS
4/9/2012 NS NS NS NS NS NS NS6/15/2014 <0.50 <0.50 <0.50 <1.5 13.1 0.11 J NA
MW-18D 03/25/09 <0.55 <0.50 <0.65 <1.1 <0.50 <1.0 25.34/22/2010 NS NS NS NS NS NS NS
11/30/2010 NS NS NS NS NS NS NS
5/25/2011 NS NS NS NS NS NS NS
4/9/2012 NS NS NS NS NS NS NS6/15/2014 0.17 J <0.50 <0.50 <1.5 1.6 <0.50 NA
1 600 600 500 20 70 15
5,000 260,000 85,400 85,500 20,000 70,000 15,000
Notes:
1. "<" or ND = Not detected at or above the laboratory detection limit.
2. Concentrations are reported in micrograms per liter (ug/l) = parts per billion.
3. Concentrations in bold print equal or exceed the NCDENR 2L Standard (2L).
4. NCDENR = North Carolina Department of Environment and Natural Resources.
5. GCL = Gross Contaminantion Level.
6. MTBE = Methyl Tertiary Butyl Ether.
7. Gross Contamination Levels for Groundwater are referenced in the "Guidelines for Assessment and Corrective Action
for UST Releases", July 2008, Table 2, updated January 2010.
8. BQL = Below Quantitative Levels
9. NA = Not Analyzed
10. NR = Not Reported
11. NS = Not Sampled
NCDENR 2L Standard
GCL

FIGURES
2725 E. Millbrook Road, Ste 121
Raleigh, NC 27604
[phone]
PROJECT NO: 45.36019.0012
DATE: 5/2010 REVIEWED BY: EAA
UNION COUNTRY CUPBOARD
836 NC HIGHWAY (PARCEL # 5984-16-8149)
UNION (AHOSKIE), HERTFORD COUNTY,
NORTH CAROLINA
SOURCE: 1985 TOPOGRAPHIC MAP - TERRASERVER-USA.COM.
SCALE: SEE ABOVE
SITE
FIGURE 1: SITE TOPOGRAPHIC MAP

2725 E. Millbrook Road, Ste 121
Raleigh, NC 27604
[phone]
PROJECT NO: 45.36019.0012
DATE: 5/2010 REVIEWED BY: EAA
UNION COUNTRY CUPBOARD
836 US HIGHWAY 461 (PARCEL # 5984-16-8149)
UNION (AHOSKIE), HERTFORD COUNTY,
NORTH CAROLINA SCALE: SEE ABOVE
FIGURE 3: WATER SUPPLY WELL LOCATION MAP
SITE
1,500 feet
Inactive Well (Sullins)
Inactive Water Supply Well
Inactive Well (Blount)
Inactive Well (Blount Heirs)

APPENDIX A
LABORATORY ANALYTICAL RESULTS
08/04/14
Technical Report for
Cardno ATC Associates
Union Country Cupboard; 836 NC Rt 461, Union, NC
45.36019.0012
Accutest Job Number: FA15868
Sampling Date: 06/15/14
Report to:
Cardno ATC Associates
[e-mail]
ATTN: Liz Allyn
Total number of pages in report:
Certifications: FL (E83510), LA (03051), KS (E-10327), IA (366), IL (200063), NC (573), NJ (FL002), SC (96038001)
DoD ELAP (L-A-B L2229), CA (04226CA), TX (T104704404), PA (68-03573), VA (460177),
AK, AR, GA, KY, MA, NV, OK, UT, WA
This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone] • http://www.accutest.com
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Harry Behzadi, Ph.D.
Laboratory Director
Southeast
08/04/14
Reissue #1
e-Hardcopy 2.0
Automated Report
45
Accutest Laboratories is the sole authority for authorizing edits or modifications to this
document. Unauthorized modification of this report is strictly prohibited.
1 of 45
FA15868
Florida  4405 Vineland Road  Suite C-15  Orlando, FL 32811  tel: [phone]  fax: [phone]  htpp://www.accutest.com www.accutest.com

August 4, 2014

Ms. Liz Allyn
Cardno ATC
2725 East Millbrook
Suite 121
Raleigh, NC 27604

RE: Accutest job FA15868 Reissue

Dear Ms. Allyn,

The final report for job number FA15868 has been edited to reflect requested corrections.
These edits have been incorporated into the revised report.

The Sample ID has been revised.

Accutest apologies for any inconvenience this may have caused. Please feel free to contact
us if we can be of further assistance.

Sincerely,

Accutest Laboratories, SE

2 of 45
FA15868
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................4
Section 2: Summary of Hits ....................................................................................................5
Section 3: Sample Results ........................................................................................................7
3.1: FA15868-1: MW-18 ......................................................................................................8
3.2: FA15868-2: MW-2 ........................................................................................................10
3.3: FA15868-3: RMW-3 .....................................................................................................12
3.4: FA15868-4: MW-4 ........................................................................................................14
3.5: FA15868-5: MW-5 ........................................................................................................17
3.6: FA15868-6: MW-6D .....................................................................................................19
3.7: FA15868-7: MW-8A .....................................................................................................21
3.8: FA15868-8: MW-9 ........................................................................................................23
3.9: FA15868-9: MW-12 ......................................................................................................25
3.10: FA15868-10: MW-16 ..................................................................................................27
3.11: FA15868-11: MW-17 ..................................................................................................29
Section 4: Misc. Forms ............................................................................................................31
4.1: Chain of Custody ...........................................................................................................32
Section 5: GC/MS Volatiles - QC Data Summaries ..............................................................36
5.1: Method Blank Summary ................................................................................................37
5.2: Blank Spike Summary ...................................................................................................40
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................43 123453 of 45
FA15868
Accutest Laboratories
Sample Summary
Cardno ATC Associates
Job No:FA15868
Union Country Cupboard; 836 NC Rt 461, Union, NC
Project No: 45.36019.0012
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA15868-1 06/15/14 11:45 EA 06/17/14 AQ Ground Water MW-18
FA15868-2 06/15/14 11:00 EA 06/17/14 AQ Ground Water MW-2
FA15868-3 06/15/14 13:15 EA 06/17/14 AQ Ground Water RMW-3
FA15868-4 06/15/14 15:05 EA 06/17/14 AQ Ground Water MW-4
FA15868-5 06/15/14 12:15 EA 06/17/14 AQ Ground Water MW-5
FA15868-6 06/15/14 15:40 EA 06/17/14 AQ Ground Water MW-6D
FA15868-7 06/15/14 14:15 EA 06/17/14 AQ Ground Water MW-8A
FA15868-8 06/15/14 14:00 EA 06/17/14 AQ Ground Water MW-9
FA15868-9 06/15/14 16:00 EA 06/17/14 AQ Ground Water MW-12
FA15868-10 06/15/14 12:45 EA 06/17/14 AQ Ground Water MW-16
FA15868-11 06/15/14 14:45 EA 06/17/14 AQ Ground Water MW-17
4 of 45
FA15868 1
Summary of Hits Page 1 of 2
Job Number:FA15868
Account:Cardno ATC Associates
Project:Union Country Cupboard; 836 NC Rt 461, Union, NC
Collected:06/15/14
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA15868-1 MW-18
Benzene 0.17 J 0.50 0.10 ug/l SM 6200B
Methyl Tert Butyl Ether 1.6 0.50 0.10 ug/l SM 6200B
FA15868-2 MW-2
No hits reported in this sample.
FA15868-3 RMW-3
Acetone 10.5 10 1.0 ug/l SM 6200B
Benzene 0.25 J 0.50 0.10 ug/l SM 6200B
sec-Butylbenzene 0.63 0.50 0.10 ug/l SM 6200B
1,2-Dichloroethane 2.8 0.50 0.10 ug/l SM 6200B
Di-Isopropyl ether 0.20 J 0.50 0.10 ug/l SM 6200B
Isopropylbenzene 0.61 0.50 0.10 ug/l SM 6200B
Methyl Tert Butyl Ether 9.6 0.50 0.10 ug/l SM 6200B
Naphthalene 1.1 0.50 0.10 ug/l SM 6200B
FA15868-4 MW-4
Benzene 3350 50 10 ug/l SM 6200B
n-Butylbenzene 4.5 J 5.0 1.0 ug/l SM 6200B
sec-Butylbenzene 3.9 J 5.0 1.0 ug/l SM 6200B
1,2-Dichloroethane 5.3 5.0 1.0 ug/l SM 6200B
Di-Isopropyl ether 14.5 5.0 1.0 ug/l SM 6200B
Ethylbenzene 757 50 10 ug/l SM 6200B
Isopropylbenzene 33.5 5.0 1.0 ug/l SM 6200B
p-Isopropyltoluene 2.1 J 5.0 1.0 ug/l SM 6200B
Methyl ethyl ketone 47.9 25 6.8 ug/l SM 6200B
Methyl Tert Butyl Ether 4990 50 10 ug/l SM 6200B
Naphthalene 223 5.0 1.0 ug/l SM 6200B
n-Propylbenzene 75.1 5.0 1.0 ug/l SM 6200B
1,2,4-Trimethylbenzene 490 5.0 1.0 ug/l SM 6200B
1,3,5-Trimethylbenzene 106 5.0 1.0 ug/l SM 6200B
Toluene 1180 50 10 ug/l SM 6200B
Xylene (total)2000 150 20 ug/l SM 6200B
m,p-Xylene 1340 100 10 ug/l SM 6200B
o-Xylene 655 50 10 ug/l SM 6200B
FA15868-5 MW-5
Methyl Tert Butyl Ether 0.26 J 0.50 0.10 ug/l SM 6200B
5 of 45
FA15868 2
Summary of Hits Page 2 of 2
Job Number:FA15868
Account:Cardno ATC Associates
Project:Union Country Cupboard; 836 NC Rt 461, Union, NC
Collected:06/15/14
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA15868-6 MW-6D
Benzene 0.38 J 0.50 0.10 ug/l SM 6200B
1,2-Dichloroethane 0.41 J 0.50 0.10 ug/l SM 6200B
Di-Isopropyl ether 0.18 J 0.50 0.10 ug/l SM 6200B
Methyl Tert Butyl Ether 12.5 0.50 0.10 ug/l SM 6200B
FA15868-7 MW-8A
No hits reported in this sample.
FA15868-8 MW-9
No hits reported in this sample.
FA15868-9 MW-12
No hits reported in this sample.
FA15868-10 MW-16
No hits reported in this sample.
FA15868-11 MW-17
Di-Isopropyl ether 0.11 J 0.50 0.10 ug/l SM 6200B
Methyl Tert Butyl Ether 13.1 0.50 0.10 ug/l SM 6200B
6 of 45
FA15868 2
Accutest Laboratories
Sample Results
Report of Analysis
Southeast
Section 3
7 of 45
FA15868 3
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-18
Lab Sample ID:FA15868-1 Date Sampled:06/15/14
Matrix:AQ - Ground Water Date Received:06/17/14
Method:SM 6200B Percent Solids:n/a
Project:Union Country Cupboard; 836 NC Rt 461, Union, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E031621.D 1 06/26/14 TD n/a n/a VE1058
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 10 1.0 ug/l
71-43-2 Benzene 0.17 0.50 0.10 ug/l J
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
8 of 45
FA15868 33.1
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-18
Lab Sample ID:FA15868-1 Date Sampled:06/15/14
Matrix:AQ - Ground Water Date Received:06/17/14
Method:SM 6200B Percent Solids:n/a
Project:Union Country Cupboard; 836 NC Rt 461, Union, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
64-17-5 Ethyl Alcohol ND 100 26 ug/l
591-78-6 2-Hexanone ND 5.0 0.50 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
108-10-1 4-Methyl-2-pentanone ND 2.5 0.50 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
78-93-3 Methyl ethyl ketone ND 2.5 0.68 ug/l
1634-04-4 Methyl Tert Butyl Ether 1.6 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
108-05-4 Vinyl Acetate ND 5.0 0.18 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
2037-26-5 Toluene-D8 89%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
9 of 45
FA15868 33.1
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-2
Lab Sample ID:FA15868-2 Date Sampled:06/15/14
Matrix:AQ - Ground Water Date Received:06/17/14
Method:SM 6200B Percent Solids:n/a
Project:Union Country Cupboard; 836 NC Rt 461, Union, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E031622.D 1 06/26/14 TD n/a n/a VE1058
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 10 1.0 ug/l
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 45
FA15868 33.2
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-2
Lab Sample ID:FA15868-2 Date Sampled:06/15/14
Matrix:AQ - Ground Water Date Received:06/17/14
Method:SM 6200B Percent Solids:n/a
Project:Union Country Cupboard; 836 NC Rt 461, Union, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
64-17-5 Ethyl Alcohol ND 100 26 ug/l
591-78-6 2-Hexanone ND 5.0 0.50 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
108-10-1 4-Methyl-2-pentanone ND 2.5 0.50 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
78-93-3 Methyl ethyl ketone ND 2.5 0.68 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
108-05-4 Vinyl Acetate ND 5.0 0.18 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
2037-26-5 Toluene-D8 94%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 45
FA15868 33.2
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:RMW-3
Lab Sample ID:FA15868-3 Date Sampled:06/15/14
Matrix:AQ - Ground Water Date Received:06/17/14
Method:SM 6200B Percent Solids:n/a
Project:Union Country Cupboard; 836 NC Rt 461, Union, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E031623.D 1 06/26/14 TD n/a n/a VE1058
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 10.5 10 1.0 ug/l
71-43-2 Benzene 0.25 0.50 0.10 ug/l J
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene 0.63 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane 2.8 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether 0.20 0.50 0.10 ug/l J
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 45
FA15868 33.3
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:RMW-3
Lab Sample ID:FA15868-3 Date Sampled:06/15/14
Matrix:AQ - Ground Water Date Received:06/17/14
Method:SM 6200B Percent Solids:n/a
Project:Union Country Cupboard; 836 NC Rt 461, Union, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
64-17-5 Ethyl Alcohol ND 100 26 ug/l
591-78-6 2-Hexanone ND 5.0 0.50 ug/l
98-82-8 Isopropylbenzene 0.61 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
108-10-1 4-Methyl-2-pentanone ND 2.5 0.50 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
78-93-3 Methyl ethyl ketone ND 2.5 0.68 ug/l
1634-04-4 Methyl Tert Butyl Ether 9.6 0.50 0.10 ug/l
91-20-3 Naphthalene 1.1 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
108-05-4 Vinyl Acetate ND 5.0 0.18 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%70-130%
2037-26-5 Toluene-D8 96%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
13 of 45
FA15868 33.3
Accutest Laboratories
Report of Analysis Page 1 of 3
Client Sample ID:MW-4
Lab Sample ID:FA15868-4 Date Sampled:06/15/14
Matrix:AQ - Ground Water Date Received:06/17/14
Method:SM 6200B Percent Solids:n/a
Project:Union Country Cupboard; 836 NC Rt 461, Union, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E031624.D 10 06/26/14 TD n/a n/a VE1058
Run #2 E031625.D 100 06/26/14 TD n/a n/a VE1058
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 100 10 ug/l
71-43-2 Benzene 3350 a 50 10 ug/l
108-86-1 Bromobenzene ND 5.0 1.0 ug/l
74-97-5 Bromochloromethane ND 5.0 1.0 ug/l
75-27-4 Bromodichloromethane ND 5.0 1.0 ug/l
75-25-2 Bromoform ND 5.0 1.0 ug/l
104-51-8 n-Butylbenzene 4.5 5.0 1.0 ug/l J
135-98-8 sec-Butylbenzene 3.9 5.0 1.0 ug/l J
98-06-6 tert-Butylbenzene ND 5.0 1.0 ug/l
108-90-7 Chlorobenzene ND 5.0 1.0 ug/l
75-00-3 Chloroethane ND 5.0 1.2 ug/l
67-66-3 Chloroform ND 5.0 1.0 ug/l
95-49-8 o-Chlorotoluene ND 5.0 1.0 ug/l
106-43-4 p-Chlorotoluene ND 5.0 1.0 ug/l
56-23-5 Carbon tetrachloride ND 5.0 1.0 ug/l
75-34-3 1,1-Dichloroethane ND 5.0 1.0 ug/l
75-35-4 1,1-Dichloroethylene ND 5.0 1.0 ug/l
563-58-6 1,1-Dichloropropene ND 5.0 1.0 ug/l
106-93-4 1,2-Dibromoethane ND 5.0 1.0 ug/l
107-06-2 1,2-Dichloroethane 5.3 5.0 1.0 ug/l
78-87-5 1,2-Dichloropropane ND 5.0 1.0 ug/l
142-28-9 1,3-Dichloropropane ND 5.0 1.0 ug/l
108-20-3 Di-Isopropyl ether 14.5 5.0 1.0 ug/l
594-20-7 2,2-Dichloropropane ND 5.0 1.0 ug/l
124-48-1 Dibromochloromethane ND 5.0 1.0 ug/l
75-71-8 Dichlorodifluoromethane ND 5.0 1.0 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.0 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.0 ug/l
541-73-1 m-Dichlorobenzene ND 5.0 1.0 ug/l
95-50-1 o-Dichlorobenzene ND 5.0 1.0 ug/l
106-46-7 p-Dichlorobenzene ND 5.0 1.0 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.0 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
14 of 45
FA15868 33.4
Accutest Laboratories
Report of Analysis Page 2 of 3
Client Sample ID:MW-4
Lab Sample ID:FA15868-4 Date Sampled:06/15/14
Matrix:AQ - Ground Water Date Received:06/17/14
Method:SM 6200B Percent Solids:n/a
Project:Union Country Cupboard; 836 NC Rt 461, Union, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.0 ug/l
100-41-4 Ethylbenzene 757 a 50 10 ug/l
64-17-5 Ethyl Alcohol ND 1000 260 ug/l
591-78-6 2-Hexanone ND 50 5.0 ug/l
98-82-8 Isopropylbenzene 33.5 5.0 1.0 ug/l
99-87-6 p-Isopropyltoluene 2.1 5.0 1.0 ug/l J
108-10-1 4-Methyl-2-pentanone ND 25 5.0 ug/l
74-83-9 Methyl bromide ND 5.0 1.0 ug/l
74-87-3 Methyl chloride ND 5.0 1.0 ug/l
75-09-2 Methylene chloride ND 20 10 ug/l
78-93-3 Methyl ethyl ketone 47.9 25 6.8 ug/l
1634-04-4 Methyl Tert Butyl Ether 4990 a 50 10 ug/l
91-20-3 Naphthalene 223 5.0 1.0 ug/l
103-65-1 n-Propylbenzene 75.1 5.0 1.0 ug/l
100-42-5 Styrene ND 5.0 1.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 5.0 1.0 ug/l
71-55-6 1,1,1-Trichloroethane ND 5.0 1.0 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 1.0 ug/l
79-00-5 1,1,2-Trichloroethane ND 5.0 1.1 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 5.0 1.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 5.0 1.2 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.0 ug/l
95-63-6 1,2,4-Trimethylbenzene 490 5.0 1.0 ug/l
108-67-8 1,3,5-Trimethylbenzene 106 5.0 1.0 ug/l
127-18-4 Tetrachloroethylene ND 5.0 1.0 ug/l
108-88-3 Toluene 1180 a 50 10 ug/l
79-01-6 Trichloroethylene ND 5.0 1.0 ug/l
75-69-4 Trichlorofluoromethane ND 5.0 1.0 ug/l
75-01-4 Vinyl chloride ND 5.0 1.0 ug/l
108-05-4 Vinyl Acetate ND 50 1.8 ug/l
1330-20-7 Xylene (total)2000 a 150 20 ug/l
m,p-Xylene 1340 a 100 10 ug/l
95-47-6 o-Xylene 655 a 50 10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 98%99%70-130%
17060-07-0 1,2-Dichloroethane-D4 105%101%70-130%
2037-26-5 Toluene-D8 97%102%70-130%
460-00-4 4-Bromofluorobenzene 98%99%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
15 of 45
FA15868 33.4
Accutest Laboratories
Report of Analysis Page 3 of 3
Client Sample ID:MW-4
Lab Sample ID:FA15868-4 Date Sampled:06/15/14
Matrix:AQ - Ground Water Date Received:06/17/14
Method:SM 6200B Percent Solids:n/a
Project:Union Country Cupboard; 836 NC Rt 461, Union, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
16 of 45
FA15868 33.4
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-5
Lab Sample ID:FA15868-5 Date Sampled:06/15/14
Matrix:AQ - Ground Water Date Received:06/17/14
Method:SM 6200B Percent Solids:n/a
Project:Union Country Cupboard; 836 NC Rt 461, Union, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E031626.D 1 06/26/14 TD n/a n/a VE1058
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 10 1.0 ug/l
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
17 of 45
FA15868 33.5
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-5
Lab Sample ID:FA15868-5 Date Sampled:06/15/14
Matrix:AQ - Ground Water Date Received:06/17/14
Method:SM 6200B Percent Solids:n/a
Project:Union Country Cupboard; 836 NC Rt 461, Union, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
64-17-5 Ethyl Alcohol ND 100 26 ug/l
591-78-6 2-Hexanone ND 5.0 0.50 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
108-10-1 4-Methyl-2-pentanone ND 2.5 0.50 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
78-93-3 Methyl ethyl ketone ND 2.5 0.68 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.26 0.50 0.10 ug/l J
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
108-05-4 Vinyl Acetate ND 5.0 0.18 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 104%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%70-130%
2037-26-5 Toluene-D8 92%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
18 of 45
FA15868 33.5
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-6D
Lab Sample ID:FA15868-6 Date Sampled:06/15/14
Matrix:AQ - Ground Water Date Received:06/17/14
Method:SM 6200B Percent Solids:n/a
Project:Union Country Cupboard; 836 NC Rt 461, Union, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E031627.D 1 06/26/14 TD n/a n/a VE1058
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 10 1.0 ug/l
71-43-2 Benzene 0.38 0.50 0.10 ug/l J
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane 0.41 0.50 0.10 ug/l J
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether 0.18 0.50 0.10 ug/l J
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
19 of 45
FA15868 33.6
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-6D
Lab Sample ID:FA15868-6 Date Sampled:06/15/14
Matrix:AQ - Ground Water Date Received:06/17/14
Method:SM 6200B Percent Solids:n/a
Project:Union Country Cupboard; 836 NC Rt 461, Union, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
64-17-5 Ethyl Alcohol ND 100 26 ug/l
591-78-6 2-Hexanone ND 5.0 0.50 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
108-10-1 4-Methyl-2-pentanone ND 2.5 0.50 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
78-93-3 Methyl ethyl ketone ND 2.5 0.68 ug/l
1634-04-4 Methyl Tert Butyl Ether 12.5 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
108-05-4 Vinyl Acetate ND 5.0 0.18 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%70-130%
2037-26-5 Toluene-D8 92%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
20 of 45
FA15868 33.6
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-8A
Lab Sample ID:FA15868-7 Date Sampled:06/15/14
Matrix:AQ - Ground Water Date Received:06/17/14
Method:SM 6200B Percent Solids:n/a
Project:Union Country Cupboard; 836 NC Rt 461, Union, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E031628.D 1 06/26/14 TD n/a n/a VE1058
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 10 1.0 ug/l
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
21 of 45
FA15868 33.7
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-8A
Lab Sample ID:FA15868-7 Date Sampled:06/15/14
Matrix:AQ - Ground Water Date Received:06/17/14
Method:SM 6200B Percent Solids:n/a
Project:Union Country Cupboard; 836 NC Rt 461, Union, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
64-17-5 Ethyl Alcohol ND 100 26 ug/l
591-78-6 2-Hexanone ND 5.0 0.50 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
108-10-1 4-Methyl-2-pentanone ND 2.5 0.50 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
78-93-3 Methyl ethyl ketone ND 2.5 0.68 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
108-05-4 Vinyl Acetate ND 5.0 0.18 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 105%70-130%
17060-07-0 1,2-Dichloroethane-D4 108%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
22 of 45
FA15868 33.7
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-9
Lab Sample ID:FA15868-8 Date Sampled:06/15/14
Matrix:AQ - Ground Water Date Received:06/17/14
Method:SM 6200B Percent Solids:n/a
Project:Union Country Cupboard; 836 NC Rt 461, Union, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E031631.D 1 06/26/14 TD n/a n/a VE1058
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 10 1.0 ug/l
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
23 of 45
FA15868 33.8
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-9
Lab Sample ID:FA15868-8 Date Sampled:06/15/14
Matrix:AQ - Ground Water Date Received:06/17/14
Method:SM 6200B Percent Solids:n/a
Project:Union Country Cupboard; 836 NC Rt 461, Union, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
64-17-5 Ethyl Alcohol ND 100 26 ug/l
591-78-6 2-Hexanone ND 5.0 0.50 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
108-10-1 4-Methyl-2-pentanone ND 2.5 0.50 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
78-93-3 Methyl ethyl ketone ND 2.5 0.68 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
108-05-4 Vinyl Acetate ND 5.0 0.18 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 105%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 103%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
24 of 45
FA15868 33.8
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-12
Lab Sample ID:FA15868-9 Date Sampled:06/15/14
Matrix:AQ - Ground Water Date Received:06/17/14
Method:SM 6200B Percent Solids:n/a
Project:Union Country Cupboard; 836 NC Rt 461, Union, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E031636.D 1 06/26/14 TD n/a n/a VE1058
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 10 1.0 ug/l
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
25 of 45
FA15868 33.9
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-12
Lab Sample ID:FA15868-9 Date Sampled:06/15/14
Matrix:AQ - Ground Water Date Received:06/17/14
Method:SM 6200B Percent Solids:n/a
Project:Union Country Cupboard; 836 NC Rt 461, Union, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
64-17-5 Ethyl Alcohol ND 100 26 ug/l
591-78-6 2-Hexanone ND 5.0 0.50 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
108-10-1 4-Methyl-2-pentanone ND 2.5 0.50 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
78-93-3 Methyl ethyl ketone ND 2.5 0.68 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
108-05-4 Vinyl Acetate ND 5.0 0.18 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%70-130%
2037-26-5 Toluene-D8 93%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
26 of 45
FA15868 33.9
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-16
Lab Sample ID:FA15868-10 Date Sampled:06/15/14
Matrix:AQ - Ground Water Date Received:06/17/14
Method:SM 6200B Percent Solids:n/a
Project:Union Country Cupboard; 836 NC Rt 461, Union, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E031637.D 1 06/26/14 TD n/a n/a VE1058
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 10 1.0 ug/l
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
27 of 45
FA15868 33.10
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-16
Lab Sample ID:FA15868-10 Date Sampled:06/15/14
Matrix:AQ - Ground Water Date Received:06/17/14
Method:SM 6200B Percent Solids:n/a
Project:Union Country Cupboard; 836 NC Rt 461, Union, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
64-17-5 Ethyl Alcohol ND 100 26 ug/l
591-78-6 2-Hexanone ND 5.0 0.50 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
108-10-1 4-Methyl-2-pentanone ND 2.5 0.50 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
78-93-3 Methyl ethyl ketone ND 2.5 0.68 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
108-05-4 Vinyl Acetate ND 5.0 0.18 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 105%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
28 of 45
FA15868 33.10
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-17
Lab Sample ID:FA15868-11 Date Sampled:06/15/14
Matrix:AQ - Ground Water Date Received:06/17/14
Method:SM 6200B Percent Solids:n/a
Project:Union Country Cupboard; 836 NC Rt 461, Union, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E031632.D 1 06/26/14 TD n/a n/a VE1058
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 10 1.0 ug/l
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether 0.11 0.50 0.10 ug/l J
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
29 of 45
FA15868 33.11
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-17
Lab Sample ID:FA15868-11 Date Sampled:06/15/14
Matrix:AQ - Ground Water Date Received:06/17/14
Method:SM 6200B Percent Solids:n/a
Project:Union Country Cupboard; 836 NC Rt 461, Union, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
64-17-5 Ethyl Alcohol ND 100 26 ug/l
591-78-6 2-Hexanone ND 5.0 0.50 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
108-10-1 4-Methyl-2-pentanone ND 2.5 0.50 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
78-93-3 Methyl ethyl ketone ND 2.5 0.68 ug/l
1634-04-4 Methyl Tert Butyl Ether 13.1 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
108-05-4 Vinyl Acetate ND 5.0 0.18 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
30 of 45
FA15868 33.11
Accutest Laboratories
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Southeast
Section 4
31 of 45
FA15868 4
FA15868: Chain of Custody
Page 1 of 4
32 of 45
FA15868 44.1
FA15868: Chain of Custody
Page 2 of 4
33 of 45
FA15868 44.1
FA15868: Chain of Custody
Page 3 of 4
34 of 45
FA15868 44.1
FA15868: Chain of Custody
Page 4 of 4
35 of 45
FA15868 44.1
Accutest Laboratories
GC/MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Southeast
Section 5
36 of 45
FA15868 5
Method Blank Summary Page 1 of 3
Job Number:FA15868
Account:ATCNCR Cardno ATC Associates
Project:Union Country Cupboard; 836 NC Rt 461, Union, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1058-MB E031619.D 1 06/26/14 TD n/a n/a VE1058
The QC reported here applies to the following samples:Method: SM 6200B
FA15868-1, FA15868-2, FA15868-3, FA15868-4, FA15868-5, FA15868-6, FA15868-7, FA15868-8, FA15868-9,
FA15868-10, FA15868-11
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 10 1.0 ug/l
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
64-17-5 Ethyl Alcohol ND 100 26 ug/l
591-78-6 2-Hexanone ND 5.0 0.50 ug/l
37 of 45
FA15868 55.1.1
Method Blank Summary Page 2 of 3
Job Number:FA15868
Account:ATCNCR Cardno ATC Associates
Project:Union Country Cupboard; 836 NC Rt 461, Union, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1058-MB E031619.D 1 06/26/14 TD n/a n/a VE1058
The QC reported here applies to the following samples:Method: SM 6200B
FA15868-1, FA15868-2, FA15868-3, FA15868-4, FA15868-5, FA15868-6, FA15868-7, FA15868-8, FA15868-9,
FA15868-10, FA15868-11
CAS No.Compound Result RL MDL Units Q
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
108-10-1 4-Methyl-2-pentanone ND 2.5 0.50 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
78-93-3 Methyl ethyl ketone ND 2.5 0.68 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
108-05-4 Vinyl Acetate ND 5.0 0.18 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 97%70-130%
17060-07-0 1,2-Dichloroethane-D4 99%70-130%
2037-26-5 Toluene-D8 101%70-130%
38 of 45
FA15868 55.1.1
Method Blank Summary Page 3 of 3
Job Number:FA15868
Account:ATCNCR Cardno ATC Associates
Project:Union Country Cupboard; 836 NC Rt 461, Union, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1058-MB E031619.D 1 06/26/14 TD n/a n/a VE1058
The QC reported here applies to the following samples:Method: SM 6200B
FA15868-1, FA15868-2, FA15868-3, FA15868-4, FA15868-5, FA15868-6, FA15868-7, FA15868-8, FA15868-9,
FA15868-10, FA15868-11
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 102%70-130%
39 of 45
FA15868 55.1.1
Blank Spike Summary Page 1 of 3
Job Number:FA15868
Account:ATCNCR Cardno ATC Associates
Project:Union Country Cupboard; 836 NC Rt 461, Union, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1058-BS E031617.D 1 06/26/14 TD n/a n/a VE1058
The QC reported here applies to the following samples:Method: SM 6200B
FA15868-1, FA15868-2, FA15868-3, FA15868-4, FA15868-5, FA15868-6, FA15868-7, FA15868-8, FA15868-9,
FA15868-10, FA15868-11
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
67-64-1 Acetone 50 63.6 127 70-130
71-43-2 Benzene 10 9.8 98 70-130
108-86-1 Bromobenzene 10 9.9 99 70-130
74-97-5 Bromochloromethane 10 9.6 96 70-130
75-27-4 Bromodichloromethane 10 8.1 81 70-130
75-25-2 Bromoform 10 7.9 79 70-130
104-51-8 n-Butylbenzene 10 8.0 80 70-130
135-98-8 sec-Butylbenzene 10 9.1 91 70-130
98-06-6 tert-Butylbenzene 10 8.8 88 70-130
108-90-7 Chlorobenzene 10 10.3 103 70-130
75-00-3 Chloroethane 10 9.0 90 60-140
67-66-3 Chloroform 10 9.2 92 70-130
95-49-8 o-Chlorotoluene 10 10.1 101 70-130
106-43-4 p-Chlorotoluene 10 10.4 104 70-130
56-23-5 Carbon tetrachloride 10 8.3 83 70-130
75-34-3 1,1-Dichloroethane 10 9.6 96 70-130
75-35-4 1,1-Dichloroethylene 10 8.7 87 70-130
563-58-6 1,1-Dichloropropene 10 8.9 89 70-130
106-93-4 1,2-Dibromoethane 10 9.7 97 70-130
107-06-2 1,2-Dichloroethane 10 9.4 94 70-130
78-87-5 1,2-Dichloropropane 10 10 100 70-130
142-28-9 1,3-Dichloropropane 10 9.7 97 70-130
108-20-3 Di-Isopropyl ether 10 9.9 99 70-130
594-20-7 2,2-Dichloropropane 10 9.7 97 70-130
124-48-1 Dibromochloromethane 10 8.3 83 70-130
75-71-8 Dichlorodifluoromethane 10 8.2 82 60-140
156-59-2 cis-1,2-Dichloroethylene 10 9.5 95 70-130
10061-01-5 cis-1,3-Dichloropropene 10 8.1 81 70-130
541-73-1 m-Dichlorobenzene 10 9.2 92 70-130
95-50-1 o-Dichlorobenzene 10 10.2 102 70-130
106-46-7 p-Dichlorobenzene 10 9.5 95 70-130
156-60-5 trans-1,2-Dichloroethylene 10 9.5 95 70-130
10061-02-6 trans-1,3-Dichloropropene 10 9.1 91 70-130
100-41-4 Ethylbenzene 10 9.5 95 70-130
64-17-5 Ethyl Alcohol 500 523 105 70-130
591-78-6 2-Hexanone 50 59.8 120 70-130
* = Outside of Control Limits.
40 of 45
FA15868 55.2.1
Blank Spike Summary Page 2 of 3
Job Number:FA15868
Account:ATCNCR Cardno ATC Associates
Project:Union Country Cupboard; 836 NC Rt 461, Union, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1058-BS E031617.D 1 06/26/14 TD n/a n/a VE1058
The QC reported here applies to the following samples:Method: SM 6200B
FA15868-1, FA15868-2, FA15868-3, FA15868-4, FA15868-5, FA15868-6, FA15868-7, FA15868-8, FA15868-9,
FA15868-10, FA15868-11
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
98-82-8 Isopropylbenzene 10 9.1 91 70-130
99-87-6 p-Isopropyltoluene 10 8.8 88 70-130
108-10-1 4-Methyl-2-pentanone 50 63.7 127 70-130
74-83-9 Methyl bromide 10 9.3 93 60-140
74-87-3 Methyl chloride 10 9.4 94 60-140
75-09-2 Methylene chloride 10 8.6 86 70-130
78-93-3 Methyl ethyl ketone 50 52.9 106 70-130
1634-04-4 Methyl Tert Butyl Ether 10 9.3 93 70-130
91-20-3 Naphthalene 10 9.3 93 70-130
103-65-1 n-Propylbenzene 10 9.3 93 70-130
100-42-5 Styrene 10 8.0 80 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 9.7 97 70-130
71-55-6 1,1,1-Trichloroethane 10 9.2 92 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 9.6 96 70-130
79-00-5 1,1,2-Trichloroethane 10 9.3 93 70-130
87-61-6 1,2,3-Trichlorobenzene 10 9.2 92 70-130
96-18-4 1,2,3-Trichloropropane 10 9.7 97 70-130
120-82-1 1,2,4-Trichlorobenzene 10 8.2 82 70-130
95-63-6 1,2,4-Trimethylbenzene 10 8.2 82 70-130
108-67-8 1,3,5-Trimethylbenzene 10 8.1 81 70-130
127-18-4 Tetrachloroethylene 10 10.1 101 70-130
108-88-3 Toluene 10 9.7 97 70-130
79-01-6 Trichloroethylene 10 9.6 96 70-130
75-69-4 Trichlorofluoromethane 10 9.0 90 60-140
75-01-4 Vinyl chloride 10 9.8 98 60-140
108-05-4 Vinyl Acetate 50 56.0 112 70-130
1330-20-7 Xylene (total)30 26.6 89 70-130
m,p-Xylene 20 17.7 89 70-130
95-47-6 o-Xylene 10 8.9 89 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 97%70-130%
17060-07-0 1,2-Dichloroethane-D4 97%70-130%
2037-26-5 Toluene-D8 99%70-130%
* = Outside of Control Limits.
41 of 45
FA15868 55.2.1
Blank Spike Summary Page 3 of 3
Job Number:FA15868
Account:ATCNCR Cardno ATC Associates
Project:Union Country Cupboard; 836 NC Rt 461, Union, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1058-BS E031617.D 1 06/26/14 TD n/a n/a VE1058
The QC reported here applies to the following samples:Method: SM 6200B
FA15868-1, FA15868-2, FA15868-3, FA15868-4, FA15868-5, FA15868-6, FA15868-7, FA15868-8, FA15868-9,
FA15868-10, FA15868-11
CAS No.Surrogate Recoveries BSP Limits
460-00-4 4-Bromofluorobenzene 98%70-130%
* = Outside of Control Limits.
42 of 45
FA15868 55.2.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3
Job Number:FA15868
Account:ATCNCR Cardno ATC Associates
Project:Union Country Cupboard; 836 NC Rt 461, Union, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA15868-6MS E031633.D 1 06/26/14 TD n/a n/a VE1058
FA15868-6MSD E031634.D 1 06/26/14 TD n/a n/a VE1058
FA15868-6 E031627.D 1 06/26/14 TD n/a n/a VE1058
The QC reported here applies to the following samples:Method: SM 6200B
FA15868-1, FA15868-2, FA15868-3, FA15868-4, FA15868-5, FA15868-6, FA15868-7, FA15868-8, FA15868-9,
FA15868-10, FA15868-11
FA15868-6 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
67-64-1 Acetone ND 50 30.2 60*50 30.7 61*2 70-130/20
71-43-2 Benzene 0.38 J 10 10.0 96 10 10.2 98 2 70-130/20
108-86-1 Bromobenzene ND 10 9.5 95 10 10.1 101 6 70-130/20
74-97-5 Bromochloromethane ND 10 9.3 93 10 9.4 94 1 70-130/20
75-27-4 Bromodichloromethane ND 10 8.2 82 10 8.2 82 0 70-130/20
75-25-2 Bromoform ND 10 6.6 66*10 6.7 67*2 70-130/20
104-51-8 n-Butylbenzene ND 10 8.0 80 10 7.9 79 1 70-130/20
135-98-8 sec-Butylbenzene ND 10 8.8 88 10 9.0 90 2 70-130/20
98-06-6 tert-Butylbenzene ND 10 9.1 91 10 9.0 90 1 70-130/20
108-90-7 Chlorobenzene ND 10 10.2 102 10 10.5 105 3 70-130/20
75-00-3 Chloroethane ND 10 7.6 76 10 7.7 77 1 60-140/20
67-66-3 Chloroform ND 10 9.8 98 10 9.3 93 5 70-130/20
95-49-8 o-Chlorotoluene ND 10 9.8 98 10 10.0 100 2 70-130/20
106-43-4 p-Chlorotoluene ND 10 10.2 102 10 10.5 105 3 70-130/20
56-23-5 Carbon tetrachloride ND 10 9.2 92 10 8.9 89 3 70-130/20
75-34-3 1,1-Dichloroethane ND 10 10.1 101 10 10 100 1 70-130/20
75-35-4 1,1-Dichloroethylene ND 10 9.6 96 10 9.4 94 2 70-130/20
563-58-6 1,1-Dichloropropene ND 10 9.3 93 10 9.1 91 2 70-130/20
106-93-4 1,2-Dibromoethane ND 10 9.4 94 10 10 100 6 70-130/20
107-06-2 1,2-Dichloroethane 0.41 J 10 11.0 106 10 10.4 100 6 70-130/20
78-87-5 1,2-Dichloropropane ND 10 9.9 99 10 10 100 1 70-130/20
142-28-9 1,3-Dichloropropane ND 10 9.4 94 10 9.9 99 5 70-130/20
108-20-3 Di-Isopropyl ether 0.18 J 10 9.8 96 10 10.1 99 3 70-130/20
594-20-7 2,2-Dichloropropane ND 10 10.5 105 10 10.6 106 1 70-130/20
124-48-1 Dibromochloromethane ND 10 7.5 75 10 7.4 74 1 70-130/20
75-71-8 Dichlorodifluoromethane ND 10 7.4 74 10 7.1 71 4 60-140/20
156-59-2 cis-1,2-Dichloroethylene ND 10 9.4 94 10 10.1 101 7 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 10 7.6 76 10 7.8 78 3 70-130/20
541-73-1 m-Dichlorobenzene ND 10 9.1 91 10 9.5 95 4 70-130/20
95-50-1 o-Dichlorobenzene ND 10 10.0 100 10 10.5 105 5 70-130/20
106-46-7 p-Dichlorobenzene ND 10 9.3 93 10 9.8 98 5 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 10 9.9 99 10 9.9 99 0 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 10 8.7 87 10 8.8 88 1 70-130/20
100-41-4 Ethylbenzene ND 10 9.4 94 10 9.4 94 0 70-130/20
64-17-5 Ethyl Alcohol ND 500 534 107 500 560 112 5 70-130/20
591-78-6 2-Hexanone ND 50 40.9 82 50 42.2 84 3 70-130/20
* = Outside of Control Limits.
43 of 45
FA15868 55.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3
Job Number:FA15868
Account:ATCNCR Cardno ATC Associates
Project:Union Country Cupboard; 836 NC Rt 461, Union, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA15868-6MS E031633.D 1 06/26/14 TD n/a n/a VE1058
FA15868-6MSD E031634.D 1 06/26/14 TD n/a n/a VE1058
FA15868-6 E031627.D 1 06/26/14 TD n/a n/a VE1058
The QC reported here applies to the following samples:Method: SM 6200B
FA15868-1, FA15868-2, FA15868-3, FA15868-4, FA15868-5, FA15868-6, FA15868-7, FA15868-8, FA15868-9,
FA15868-10, FA15868-11
FA15868-6 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
98-82-8 Isopropylbenzene ND 10 8.9 89 10 8.9 89 0 70-130/20
99-87-6 p-Isopropyltoluene ND 10 8.5 85 10 8.7 87 2 70-130/20
108-10-1 4-Methyl-2-pentanone ND 50 49.7 99 50 51.6 103 4 70-130/20
74-83-9 Methyl bromide ND 10 7.9 79 10 7.9 79 0 60-140/20
74-87-3 Methyl chloride ND 10 7.8 78 10 8.1 81 4 60-140/20
75-09-2 Methylene chloride ND 10 9.3 93 10 9.4 94 1 70-130/20
78-93-3 Methyl ethyl ketone ND 50 31.8 64*50 33.0 66*4 70-130/20
1634-04-4 Methyl Tert Butyl Ether 12.5 10 21.0 85 10 21.5 90 2 70-130/20
91-20-3 Naphthalene ND 10 9.4 94 10 9.4 94 0 70-130/20
103-65-1 n-Propylbenzene ND 10 8.9 89 10 9.1 91 2 70-130/20
100-42-5 Styrene ND 10 6.2 62*10 6.4 64*3 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 10 9.9 99 10 10.0 100 1 70-130/20
71-55-6 1,1,1-Trichloroethane ND 10 10.2 102 10 9.9 99 3 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 10 9.3 93 10 9.9 99 6 70-130/20
79-00-5 1,1,2-Trichloroethane ND 10 9.4 94 10 10 100 6 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 10 9.5 95 10 9.3 93 2 70-130/20
96-18-4 1,2,3-Trichloropropane ND 10 9.3 93 10 10 100 7 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 10 8.4 84 10 8.3 83 1 70-130/20
95-63-6 1,2,4-Trimethylbenzene ND 10 7.1 71 10 7.5 75 5 70-130/20
108-67-8 1,3,5-Trimethylbenzene ND 10 7.1 71 10 7.3 73 3 70-130/20
127-18-4 Tetrachloroethylene ND 10 10.1 101 10 10.1 101 0 70-130/20
108-88-3 Toluene ND 10 9.0 90 10 9.3 93 3 70-130/20
79-01-6 Trichloroethylene ND 10 10 100 10 9.7 97 3 70-130/20
75-69-4 Trichlorofluoromethane ND 10 8.1 81 10 7.8 78 4 60-140/20
75-01-4 Vinyl chloride ND 10 7.9 79 10 8.0 80 1 60-140/20
108-05-4 Vinyl Acetate ND 50 58.2 116 50 58.8 118 1 70-130/20
1330-20-7 Xylene (total)ND 30 25.6 85 30 25.8 86 1 70-130/20
m,p-Xylene ND 20 17.0 85 20 17.2 86 1 70-130/20
95-47-6 o-Xylene ND 10 8.6 86 10 8.6 86 0 70-130/20
CAS No.Surrogate Recoveries MS MSD FA15868-6 Limits
1868-53-7 Dibromofluoromethane 105%99%101%70-130%
17060-07-0 1,2-Dichloroethane-D4 111%100%106%70-130%
2037-26-5 Toluene-D8 97%99%92%70-130%
* = Outside of Control Limits.
44 of 45
FA15868 55.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number:FA15868
Account:ATCNCR Cardno ATC Associates
Project:Union Country Cupboard; 836 NC Rt 461, Union, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA15868-6MS E031633.D 1 06/26/14 TD n/a n/a VE1058
FA15868-6MSD E031634.D 1 06/26/14 TD n/a n/a VE1058
FA15868-6 E031627.D 1 06/26/14 TD n/a n/a VE1058
The QC reported here applies to the following samples:Method: SM 6200B
FA15868-1, FA15868-2, FA15868-3, FA15868-4, FA15868-5, FA15868-6, FA15868-7, FA15868-8, FA15868-9,
FA15868-10, FA15868-11
CAS No.Surrogate Recoveries MS MSD FA15868-6 Limits
460-00-4 4-Bromofluorobenzene 95%99%99%70-130%
* = Outside of Control Limits.
45 of 45
FA15868 55.3.1