WA-722_10151_CA_RPTS_20180814_AFVR

EXECUTIVE SUMMARY

The former H & S Trading site is located at 211 Tunis Road in Tunis, Hertford County, North Carolina.
According to the available information, two 2,000-gallon gasoline, one 1,000-gallon gasoline and one
550-gallon kerosene underground storage tanks were removed from the site in October 1992. The site
risk classification is currently ranked as high risk based on the presence of potable water supply wells
within a 1,000-foot radius of the site.

On May 5, 2018, an Aggressive Fluid Vapor Recovery (AFVR) event was conducted on MW-1 and MW-
19. A total of 945 gallons of petroleum impacted ground water was removed during the event.

On June 11, 2018, six Type II monitoring wells and one recovery well were gauged, purged, and/or
sampled. A free product thicknesses of 0.14 feet was measured in MW-1. Concentrations of requested
method constituents that exceeded the applicable ground water quality standards were reported in the
samples collected from MW-2, MW-3, MW-5, MW-6, MW-19 and RW-2. None of the reported
contaminant concentrations exceeded the Gross Contamination Levels.

GRI recommends that the Corrective Action System (CAS) at the site should be evaluated including the
construction of the recovery wells. If the recovery wells are properly constructed to bracket the free
product zone, then the CAS could be enhanced in order to address the free product in MW-1. If the CAS
is not a feasible option for remediating the site, then additional AFVR and/or MMPE events should be
conducted in order to continue to remove free product. Until free product is no longer present and
contaminant concentrations remain above the applicable ground water quality standards, semi-annual
ground water monitoring should continue at the site. The next ground water sampling event is tentatively
scheduled for December 2018.

TABLE OF CONTENTS

1.0 SITE HISTORY AND CHARACTERIZATION ....................................................................... 1
2.0 CURRENT SITE ASSESSMENT ................................................................................................ 1
3.0 AFVR EVENT ................................................................................................................................ 1
4.0 GROUND WATER QUALITY .................................................................................................... 2
5.0 CORRECTIVE ACTION EVALUATION AND DISCUSSION .............................................. 3
6.0 CONCLUSIONS AND RECOMMENDATIONS ....................................................................... 4
7.0 LIMITATIONS .............................................................................................................................. 4

FIGURES
Figure 1: Site Location Map
Figure 2: Site Map
Figure 3: Water Table Surface Map
Figure 4: Ground Water Quality Map

TABLES
Table 1: Well Construction and Gauging Information
Table 2: Free Product Recovery Results
Table 3: Free Product Recovery Event Information
Table 4: Free Product Recovery Cost Summary
Table 5: Summary of Ground Water Sample Analytical Results

APPENDICES
Appendix A: AFVR Data and Calculations
Appendix B: Disposal Manifest
Appendix C: Laboratory Report – Ground Water Samples
1

1.0 SITE HISTORY AND CHARACTERIZATION
The former H & S Trading site is located at 211 Tunis Road in Tunis, Hertford County, North Carolina
(Figure 1). According to available information, two 2,000-gallon gasoline, one 1,000-gallon gasoline and
one 550-gallon kerosene underground storage tanks (USTs) were removed from the site in October 1992
by Coastal Environmental Services (Coastal). Nineteen Type II monitoring wells (MW-1 through MW-6
and MW-8 through MW-20) and one Type III monitoring well (MWD-7) were installed at the site during
previous ground water assessment and corrective action activities. Please note that MW-13 and MW-15
were found to be destroyed during past ground water monitoring activities. A ground water pump and
treat system was installed in March 1997 by CES Engineering, PC. (CES). Six recovery wells (RW-1
through RW-6) and two replacement recovery wells (RW-1A and RW-8) were also installed at the site
during corrective action implementation activities. The site risk classification is currently ranked as High
due to the presence of potable water supply wells within a 1,000-foot radius of the site.

Please note that some of the information contained in this report was obtained under the supervision of
Coastal, CES and others prior to May 2008. Although Geological Resources, Inc. (GRI) cannot verify the
accuracy of information obtained from previous reports, for the purposes of this report, it is assumed to be
correct. Please refer to previous submittals for further historical information regarding the site.

2.0 CURRENT SITE ASSESSMENT
The purpose of this report is to present the results of the Aggressive Fluid Vapor Recovery (AFVR) event
and ground water sampling activities conducted on May 5 and June 11, 2018, at the H & S Trading site.
The activities were conducted in accordance with GRI proposal number 17-525 which was submitted to
NCDEQ on September 15, 2017, and approved as Task Authorization No. 10151-57 on October 23, 2017.
The purpose of the activities was to remove free product, reduce contaminant concentrations and to obtain
current ground water quality data for the site.

3.0 AFVR EVENT
On May 5, 2018, Greenwood Applied Services, LLC (GAS) conducted an AFVR event on MW-1 and
MW-19. The AFVR equipment included a 3,500-gallon capacity vacuum truck, flexible vacuum hoses,
1-inch diameter PVC stinger pipes and associated couplings and pipe fittings to manifold to MW-1 and
MW-19. The AFVR system was rated at 680 CFM at 18in./Hg.

2

Monitoring wells MW-1 and MW-19 were gauged on May 5, 2018, prior to the event. A free product
thickness of 0.20 feet was observed in MW-1 prior to the start of the event. No free product was
measured in MW-19 prior to AFVR startup. A ground water sample was collected from MW-19 prior to
the AFVR startup. Concentrations of requested method constituents were reported in the ground water
sample collected from MW-19. Monitoring wells MW-1 and MW-19 were vacuumed continuously for 8
hours during the event. During the event, measurements of relative humidity, temperature, vacuum,
exhaust velocity and off-gas concentrations were recorded at the discharge stack every fifteen minutes for
the first two hours, then every thirty minutes for the remaining six hours. No measurable free product
was observed in MW-1 or MW-19 at the conclusion of the event. A Site Map showing the locations of
the monitoring wells and structures on-site is included as Figure 2. A summary of well construction and
gauging data obtained before start up and at the conclusion of the AFVR event is presented in Table 1. A
copy of the field data sheet and data calculations have been included as Appendix A.

The results of the AFVR event indicate that a total of 945 gallons of liquids were removed during the
event. No free product was observed in the tanker at the end of the event. Based on 8 hours of operation,
the average fluid recovery rate was 118.13 gallons per hour. Based on mass-removal calculations,
approximately 2.05 pounds or 0.33 gallons of vapor phase hydrocarbons were removed. For the May
2018 AFVR event, the cost per gallon of recovered petroleum affected ground water was $2.71. A
summary of free product recovery results has been included as Table 2. A summary of information
collected during the AFVR event, as well as a breakdown of fluids removed is included as Table 3. A
summary of costs associated with free product recovery is included as Table 4. A summary of ground
water sample analytical results for the ground water sample collected prior to the start of the AFVR event
is included as Table 5. At the conclusion of the AFVR event, all wastewater was transported to a
permitted facility for disposal. Copies of disposal manifests have been included as Appendix B. A
complete laboratory report for the ground water sample collected prior to the start of the AFVR event is
included as Appendix C.

4.0 GROUND WATER QUALITY
Six Type II monitoring wells (MW-1, MW-2, MW-3, MW-5, MW-6, and MW-19) and one recovery well
(RW-2) were gauged, purged and/or sampled on June 11, 2018. A free product thickness of 0.14 feet was
measured in MW-1. Depths to ground water in the Type II monitoring wells ranged from 17.98 to 29.90
feet below the tops of well casings. Ground water elevations relative to a temporary benchmark with an
assumed datum of 100.00 feet ranged from 72.23 to 78.95 feet. Ground water flow direction was
3

generally toward the southwest with an average horizontal hydraulic gradient of 0.21 feet per foot. The
vertical gradient between paired wells MW-1 and MWD-7 was not calculated during the June 2018
gauging event. A Water Table Surface Map is included as Figure 3. A summary of well construction
and gauging information is presented in Table 1.

Ground water samples collected during the June 2018 sampling event were submitted for laboratory
analyses of volatile organic compounds using EPA Method 6200B. Concentrations of benzene, MTBE,
naphthalene, methyl chloride, and/or 1,1,2,2-tetrachloroethane that exceeded the Maximum Allowable
Concentrations (MACs) specified in T15A NCAC 2L.0202 were reported in the ground water samples
collected from MW-2, MW-3, MW-5, MW-6, MW-19 and RW-2. None of the reported concentrations
exceeded the Gross Contamination Levels (GCLs). A Ground Water Quality Map based on data from the
June 2018 sampling event has been included as Figure 3. A summary of ground water sample analytical
results is presented in Table 2. The complete laboratory report has been included in Appendix C.

5.0 CORRECTIVE ACTION EVALUATION AND DISCUSSION
Corrective action activities completed at the site to date include the submission of a CAP in 1995, at least
five Mobile Multi-Phase Extraction (MMPE) events and at least three Aggressive Fluid-Vapor Recovery
(AFVR) events. Free product was noted in three different wells (MW-1, MW-19 and RW-2) between
2008 and 2018, and continues to be observed in MW-1.

The Corrective Action Plan (CAP) submitted in 1995 proposed the installation of a ground water Pump
and Treat system. The CAP was approved on March 4, 1996 and the Corrective Action System (CAS)
was installed in April 1997. Six recovery wells (RW-1 through RW-6) and two replacement recovery
wells (RW-1A and RW-8) were also installed at the site during corrective action implementation
activities. Well construction and screened interval information for the recovery wells is unavailable. The
CAS operated at the site between April 1997 and September 2005, and again from April 2009 to April
2010. Historical information regarding the operation of the CAS is limited, however, based on flow
meter readings, approximately 6,550,749 gallons of ground water are estimated to have been treated and
discharged by the CAS between 1997 to 2005 and 2009 to 2010.

Between July 2010 and May 2018, five MMPEs and three AFVRs have been conducted at the site. A
total of 61,668 gallons of petroleum impacted ground water has been removed from the site, including
4

47.57 gallons of liquid and vapor-phase free product. The total cost of the MMPE and AFVR events
between July 2010 and May 2018 is $69,497.00.

Free product continues to persist in MW-1, and contaminant concentrations in remaining wells continue
to fluctuate between historical levels.

6.0 CONCLUSIONS AND RECOMMENDATIONS
 A total of 945 gallons of petroleum impacted ground water was removed during the May 2018
AFVR event conducted on MW-1 and MW-19. A free product thickness of 0.20 feet was
observed in MW-1 prior to the start of the event. No measurable free product was observed in
MW-1 or MW-19 at the conclusion of the event.
 The average depth to ground water in the Type II monitoring wells in June 2018 was 22.47 feet.
 Concentrations of benzene, MTBE, naphthalene, methyl chloride and/or 1,1,2,2-
tetrachloroethane that exceeded the MACs were reported in the ground water samples collected
from MW-2, MW-3, MW-5, MW-6, MW-19, and RW-2. None of the reported concentrations
exceeded the GCLs.
 Corrective action activities conducted at the site to date include the operation of a Pump and
Treat CAS, at least five MMPEs and three AFVRs. Free product continues to persist in MW-1,
despite the ongoing remedial efforts at the site dating back to 1997.
 Based on this information, GRI recommends that the CAS at the site should be evaluated
including the construction of the recovery wells. If the recovery wells are properly constructed to
bracket the free product zone, then the CAS could be enhanced in order to address the free
product in MW-1. If the CAS is not a feasible option for remediating the site, then additional
AFVR and/or MMPE events should be conducted in order to continue to remove free product.
Until free product is no longer present and contaminant concentrations remain above the
applicable ground water quality standards, semi-annual ground water monitoring should continue
at the site. The next ground water sampling event is tentatively scheduled for December 2018.

7.0 LIMITATIONS
This report has been prepared for the exclusive use of North East Oil Company, Inc. for specific
application to the referenced site in Hertford County, North Carolina. The assessment was conducted
based on the scope of work and level of effort desired by NCDEQ and with resources adequate only for
that scope of work. Our findings have been developed in accordance with generally accepted standards of
5

environmental practices in the State of North Carolina, available information, and our professional
judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would be
interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data. Please note that field data collected prior
to the May 2008 sampling and updated receptor survey event was not obtained under the supervision of
GRI. Although the accuracy of this information cannot be verified, for the purpose of this report GRI
assumes that it is correct.

FIGURES

TABLES
05/21/08 22.63 0.26 77.59 ---
03/09/09 23.42 0.42 76.94 ---
06/23/09 24.53 0.80 76.16 ---
09/23/09 24.61 0.35 75.69 ---
12/28/09 23.47 0.32 76.80 ---
03/23/10 22.50 0.28 77.74 ---
07/19/10 23.75 0.57 76.74 Before MMPE
07/23/10 23.95 ---76.05 After MMPE
02/07/11 22.99 0.36 77.32 Before MMPE
02/11/11 22.94 ---77.06 After MMPE
03/24/11 22.93 0.29 77.32 ---
08/08/11 24.42 ---75.58 Before MMPE
08/12/11 25.22 0.34 74.78 After MMPE
09/13/11 23.73 0.72 76.89 ---
04/23/12 25.66 3.74 77.55 Before MMPE
04/27/12 24.70 1.01 76.17 After MMPE
05/29/12 23.52 0.80 77.17 ---
01/22/13 25.45 3.24 77.33 Before AFVR
01/22/13 26.60 2.00 75.12 After AFVR
02/25/13 24.37 2.28 77.59 ---
08/29/13 25.43 1.75 76.07 Before AFVR
08/29/13 24.58 0.71 76.03 After AFVR
10/02/13 25.34 1.25 75.73 ---
06/26/14 23.16 0.21 77.02 ---
01/28/15 23.19 0.06 76.86 ---
08/12/15 23.00 ---77.00 ---
01/21/16 22.32 ---77.68 Boom Removal
02/23/16 21.28 ---78.72 ---
11/21/16 21.62 0.11 78.47
07/20/17 22.54 0.16 77.60
05/05/18 22.85 0.20 77.32 Before AFVR
05/05/18 23.34 ---76.66 After AFVR
06/11/18 22.92 0.14 77.20
05/21/08 21.55 ---77.62 ---
03/09/09 22.21 ---76.96 ---
06/23/09 23.01 ---76.16 ---
09/23/09 23.37 ---75.80 ---
12/28/09 22.42 ---76.75 ---
03/23/10 21.11 ---78.06 ---
02/07/11 21.78 ---77.39 Before MMPE
02/11/11 22.11 ---77.06 After MMPE
03/24/11 21.79 ---77.38 ---
08/08/11 23.62 ---75.55 Before MMPE
08/12/11 24.09 ---75.08 After MMPE
09/13/11 22.22 ---76.95 ---
05/29/12 22.15 ---77.02 ---
02/25/13 21.61 ---77.56 ---
10/02/13 23.41 ---75.76 ---
06/26/14 22.06 ---77.11 ---
01/28/15 22.24 ---76.93 ---
08/12/15 22.09 ---77.08
02/23/16 20.42 ---78.75 ---
06/11/18 21.97 ---77.20
05/21/08 24.57 ---77.56 ---
03/09/09 25.16 ---76.97 ---
06/23/09 25.90 ---76.23 ---
09/23/09 26.37 ---75.76 ---
12/28/09 25.41 ---76.72 ---
03/23/10 24.24 ---77.89 ---
03/24/11 24.80 ---77.33 ---
09/13/11 25.20 ---76.93 ---
05/29/12 25.10 ---77.03 ---
02/25/13 24.56 ---77.57 ---
10/02/13 26.40 ---75.73 ---
06/26/14 25.03 ---77.10 ---
01/28/15 25.24 ---76.89 ---
08/12/15 25.07 ---77.06 ---
02/23/16 23.43 ---78.70 ---
06/11/18 29.90 ---72.23
102.133020 - 302001/22/93MW-3
99.173020 - 302001/21/93MW-2
Depth to
Water from
Top of Casing
(feet)
Free
Product
Thickness
(ft.)
Ground
Water
Elevation
(ft.)
100.003020 - 302001/19/93MW-1
Comments
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
H&S TRADING (INCIDENT NO. 10151)
Date: 07/03/18 Facility ID # : 0-009678
Well ID
Date
Installed
(mm/dd/yy)
Date
Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y
ft. BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Page 1 of 5
Depth to
Water from
Top of Casing
(feet)
Free
Product
Thickness
(ft.)
Ground
Water
Elevation
(ft.)
Comments
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
H&S TRADING (INCIDENT NO. 10151)
Date: 07/03/18 Facility ID # : 0-009678
Well ID
Date
Installed
(mm/dd/yy)
Date
Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y
ft. BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
05/21/08 20.36 ---77.60 ---
03/09/09 21.04 ---76.92 ---
06/23/09 21.60 ---76.36 ---
09/23/09 22.19 ---75.77 ---
12/28/09 20.68 ---77.28 ---
03/23/10 20.02 ---77.94 ---
03/24/11 20.58 ---77.38 ---
09/13/11 21.01 ---76.95 ---
05/29/12 20.82 ---77.14 ---
02/25/13 20.30 ---77.66 ---
10/02/13 NM NM NM Inaccessable
06/26/14 NM NM NM Inaccessable
01/28/15 NM NM NM Inaccessable
08/12/15 NM NM NM Inaccessable
05/21/08 17.58 ---77.18 ---
03/09/09 20.03 ---74.73 ---
06/23/09 17.41 ---77.35 ---
09/23/09 18.23 ---76.53 ---
12/28/09 16.27 ---78.49 ---
03/23/10 16.30 ---78.46 ---
03/24/11 17.63 ---77.13 ---
09/13/11 17.92 ---76.84 ---
05/29/12 17.78 ---76.98 ---
02/25/13 17.53 ---77.23 ---
10/02/13 18.59 ---76.17 ---
06/26/14 17.86 ---76.90 ---
01/28/15 18.04 ---76.72 ---
08/12/15 18.03 ---76.73 ---
02/23/16 16.45 ---78.31 ---
06/11/18 17.98 ---76.78
05/21/08 20.27 ---78.25 ---
03/09/09 20.61 ---77.91 ---
06/23/09 20.72 ---77.80 ---
09/23/09 20.61 ---77.91 ---
12/28/09 20.38 ---78.14 ---
03/23/10 19.77 ---78.75 ---
03/24/11 20.41 ---78.11 ---
09/13/11 20.55 ---77.97 ---
05/29/12 20.29 ---78.23 ---
02/25/13 20.31 ---78.21 ---
10/02/13 20.87 ---77.65 ---
06/26/14 20.46 ---78.06 ---
01/28/15 20.23 ---78.29 ---
08/12/15 20.58 ---77.94 ---
02/23/16 19.79 ---78.73 ---
06/11/18 20.65 ---77.87
05/21/08 24.05 ---75.51 ---
03/09/09 24.70 ---74.86 ---
06/23/09 24.45 ---75.11 ---
09/23/09 25.00 ---74.56 ---
12/28/09 24.18 ---75.38 ---
03/23/10 23.63 ---75.93 ---
03/24/11 24.24 ---75.32 ---
09/13/11 24.43 ---75.13 ---
05/29/12 24.55 ---75.01 ---
02/25/13 24.23 ---75.33 ---
06/26/14 24.18 ---75.38 ---
01/28/15 24.35 ---75.21 ---
08/12/15 24.13 ---75.43 ---
05/21/08 18.63 ---76.93 ---
03/09/09 18.95 ---76.61 ---
06/23/09 18.04 ---77.52 ---
09/23/09 19.00 ---76.56 ---
12/28/09 18.09 ---77.47 ---
03/23/10 17.25 ---78.31 ---
03/24/11 18.77 ---76.79 ---
09/13/11 18.81 ---76.75 ---
05/29/12 18.23 ---77.33 ---
02/25/13 18.31 ---77.25 ---
10/02/13 20.90 ---74.66 ---
06/26/14 18.98 ---76.58 ---
01/28/15 18.09 ---77.47 ---
08/12/15 19.08 ---76.48 ---
98.523020 - 305007/07/93MW-6
94.763020 - 302007/02/93MW-5
MW-4 07/01/93 20 20 - 30 30 97.96
MW-8 09/10/94 20 20 - 30 30 95.56
MWD-7 07/02/93 45 45 - 50 50 99.56
Page 2 of 5
Depth to
Water from
Top of Casing
(feet)
Free
Product
Thickness
(ft.)
Ground
Water
Elevation
(ft.)
Comments
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
H&S TRADING (INCIDENT NO. 10151)
Date: 07/03/18 Facility ID # : 0-009678
Well ID
Date
Installed
(mm/dd/yy)
Date
Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y
ft. BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
05/21/08 NM NM NM Not Located
03/09/09 5.58 ---75.53 ---
06/23/09 5.50 ---75.61 ---
09/23/09 6.72 ---74.39 ---
12/28/09 4.40 ---76.71 ---
03/23/10 3.93 ---77.18 ---
03/24/11 5.05 ---76.06 ---
09/13/11 5.57 ---75.54 ---
05/29/12 5.59 ---75.52 ---
02/25/13 4.74 ---76.37 ---
10/02/13 6.02 ---75.09 ---
06/26/14 4.62 ---76.49 ---
01/28/15 3.48 ---77.63 ---
08/12/15 6.48 ---74.63 ---
05/21/08 4.65 ---76.37 ---
03/09/09 4.77 ---76.25 ---
06/23/09 4.90 ---76.12 ---
09/23/09 6.34 ---74.68 ---
12/28/09 3.42 ---77.60 ---
03/23/10 2.81 ---78.21 ---
03/24/11 4.40 ---76.62 ---
09/13/11 4.95 ---76.07 ---
05/29/12 NM NM NM ---
06/26/14 NM NM NM ---
05/21/08 3.88 ---77.94 ---
03/09/09 3.52 ---78.30 ---
06/23/09 4.15 ---77.67 ---
09/23/09 5.10 ---76.72 ---
12/28/09 2.73 ---79.09 ---
03/23/10 2.39 ---79.43 ---
03/24/11 3.50 ---78.32 ---
09/13/11 3.52 ---78.30 ---
05/29/12 NM NM NM ---
06/26/14 NM NM NM ---
05/21/08 25.49 ---77.60 ---
03/09/09 26.18 ---76.91 ---
06/23/09 26.70 ---76.39 ---
09/23/09 27.82 ---75.27 ---
12/28/09 25.97 ---77.12 ---
03/23/10 24.92 ---78.17 ---
03/24/11 25.82 ---77.27 ---
09/13/11 26.50 ---76.59 ---
05/29/12 26.03 ---77.06 ---
02/25/13 25.64 ---77.45 ---
10/02/13 27.32 ---75.77 ---
06/26/14 25.98 ---77.11 ---
01/28/15 26.15 ---76.94 ---
08/12/15 25.98 ---77.11 ---
05/21/08 24.14 ---78.78 ---
03/09/09 24.72 ---78.20 ---
06/23/09 24.30 ---78.62 ---
09/23/09 25.00 ---77.92 ---
12/28/09 24.31 ---78.61 ---
03/23/10 23.23 ---79.69 ---
03/24/11 NM NM NM Not Located
09/13/11 NM NM NM Not Located
05/29/12 NM NM NM Not Located
06/26/14 NM NM NM Not Located
01/28/15 NM NM NM Not Located
05/21/08 19.95 ---77.41 ---
03/09/09 20.51 ---76.85 ---
06/23/09 21.09 ---76.27 ---
09/23/09 21.75 ---75.61 ---
12/28/09 20.17 ---77.19 ---
03/23/10 19.49 ---77.87 ---
03/24/11 20.13 ---77.23 ---
09/13/11 20.55 ---76.81 ---
05/29/12 NM NM NM ---
06/26/14 NM NM NM ---
MW-14 08/2002 25 25 - 35 35 97.36
MW-13 08/2002 25 25 - 35 35 102.92
MW-12 08/2002 25 25 - 35 35 103.09
MW-11 09/12/94 3 3 - 13 13 81.82
MW-10 09/12/94 3 3 - 13 13 81.02
MW-9 09/10/94 3 3 - 13 13 81.11
Page 3 of 5
Depth to
Water from
Top of Casing
(feet)
Free
Product
Thickness
(ft.)
Ground
Water
Elevation
(ft.)
Comments
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
H&S TRADING (INCIDENT NO. 10151)
Date: 07/03/18 Facility ID # : 0-009678
Well ID
Date
Installed
(mm/dd/yy)
Date
Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y
ft. BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
03/09/09 9.80 ---75.93 ---
06/23/09 9.56 ---76.17 ---
09/23/09 10.73 ---75.00 ---
12/28/09 8.88 ---76.85 ---
03/23/10 7.92 ---77.81 ---
03/24/11 9.50 ---76.23 ---
09/13/11 9.78 ---75.95 ---
05/29/12 9.73 ---76.00 ---
02/25/13 9.27 ---76.46 ---
10/02/13 11.43 ---74.30 ---
06/26/14 NM NM NM ---
01/28/15 NM NM NM Destroyed
08/12/15 NM NM NM Destroyed
03/09/09 20.10 ---77.35 ---
06/23/09 19.67 ---77.78 ---
09/23/09 20.30 ---77.15 ---
12/28/09 19.50 ---77.95 ---
03/23/10 18.50 ---78.95 ---
03/24/11 19.63 ---77.82 ---
09/13/11 19.95 ---77.50 ---
05/29/12 NM NM NM Destroyed
06/26/14 NM NM NM Destroyed
08/12/15 NM NM NM Destroyed
03/09/09 32.90 ---67.97 ---
06/23/09 22.36 ---78.51 ---
09/23/09 23.44 ---77.43 ---
12/28/09 22.32 ---78.55 ---
03/23/10 21.45 ---79.42 ---
03/24/11 22.37 ---78.50 ---
09/13/11 22.93 ---77.94 ---
05/29/12 NM NM NM Destroyed
06/26/14 NM NM NM Destroyed
08/12/15 NM NM NM Destroyed
12/28/09 2.21 ---76.99 ---
03/23/10 2.08 ---77.12 ---
03/24/11 3.50 ---75.70 ---
09/13/11 3.92 ---75.28 ---
05/29/12 3.88 ---75.32 ---
02/25/13 3.03 ---76.17 ---
10/02/13 7.53 ---71.67 ---
06/26/14 6.20 ---73.00 ---
01/28/15 4.57 ---74.63 ---
07/19/10 22.22 ---78.15 Before MMPE
07/23/10 23.46 0.01 76.92 After MMPE
02/07/11 21.57 ---78.80 Before MMPE
02/11/11 21.81 ---78.56 After MMPE
03/24/11 21.33 ---79.04 ---
08/08/11 21.84 0.01 78.53 Before MMPE
08/12/11 26.10 ---74.27 After MMPE
09/13/11 21.28 ---79.09 ---
04/23/12 21.85 0.01 78.53 Before MMPE
04/27/12 24.50 ---75.87 After MMPE
05/29/12 21.48 ---78.89 ---
02/25/13 21.20 0.02 79.19 ---
08/29/13 21.67 0.02 78.72 Before AFVR
08/29/13 24.09 ---76.28 After AFVR
10/02/13 21.87 0.02 78.52 ---
06/26/14 21.26 ---79.11 ---
01/28/15 21.80 0.02 78.59 ---
08/12/15 21.36 ---79.01 ---
01/21/16 21.32 ---79.05 Boom Removal
02/23/16 20.72 ---79.65 ---
11/21/16 21.02 0.02 79.37 ---
07/20/17 21.29 ---79.08
05/05/18 21.45 ---78.92 Before AFVR
05/05/18 23.55 ---76.82 After AFVR
06/11/18 21.42 ---78.95
03/24/11 20.94 ---78.80 ---
09/13/11 21.06 ---78.68 ---
05/29/12 21.06 ---78.68 ---
02/25/13 20.90 ---78.84 ---
10/02/13 NM NM NM Inaccessable
06/26/14 NS ---NS ---
01/28/15 NM NM NM Inaccessable
03/24/11 20.15 ---NM ---
09/13/11 20.49 ---NM ---
08/12/15 20.36 ---NM ---
RW-1 NA NA NA NA NM
MW-20 07/19/10 20 20 - 30 30 99.74
100.373020 - 302007/19/10MW-19
MW-18 12/15/09 5 5 - 15 15 79.20
MW-17 03/05/09 20 20 - 35 35 100.87
MW-16 03/06/09 13.6 13.6 - 28.6 28.6 97.45
MW-15 03/06/09 9 9 - 24 24 85.73
Page 4 of 5
Depth to
Water from
Top of Casing
(feet)
Free
Product
Thickness
(ft.)
Ground
Water
Elevation
(ft.)
Comments
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
H&S TRADING (INCIDENT NO. 10151)
Date: 07/03/18 Facility ID # : 0-009678
Well ID
Date
Installed
(mm/dd/yy)
Date
Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y
ft. BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
07/19/10 22.51 0.01 NM Before MMPE
07/23/10 17.30 ---NM After MMPE
02/07/11 21.44 ---NM Before MMPE
02/11/11 23.72 ---NM After MMPE
03/24/11 21.92 ---NM ---
09/13/11 22.34 ---NM ---
04/23/12 22.63 ---NM Before MMPE
04/27/12 22.60 ---NM After MMPE
05/29/12 22.26 ---NM ---
02/25/13 21.68 ---NM ---
06/26/14 22.20 ---NM ---
01/28/15 22.40 ---NM ---
08/12/15 22.22 ---NM ---
07/19/10 22.17 ---NM Before MMPE
07/23/10 22.86 ---NM After MMPE
02/07/11 21.90 ---NM Before MMPE
02/11/11 22.15 ---NM After MMPE
03/24/11 21.59 ---NM ---
09/13/11 22.05 0.04 NM ---
04/23/12 22.28 ---NM Before MMPE
04/27/12 22.73 ---NM After MMPE
05/29/12 21.92 ---NM ---
02/25/13 21.36 ---NM ---
10/02/13 23.28 0.05 NM ---
06/26/14 21.86 ---NM ---
01/28/15 22.02 ---NM ---
08/12/15 21.89 ---NM ---
01/21/16 21.23 ---NM Boom Removal
11/21/16 20.44 ---NM ---
07/20/17 21.29 ---NM
06/11/18 22.66 ---NM
03/24/11 17.31 ---NM ---
09/13/11 17.63 ---NM ---
05/29/12 17.49 ---NM ---
02/25/13 19.82 ---NM ---
06/26/14 17.53 ---NM ---
01/28/15 17.65 ---NM ---
08/12/15 17.60 ---NM ---
03/24/11 NM NM NM Pump Stuck
09/13/11 NM NM NM Pump Stuck
03/24/11 18.49 ---NM ---
09/13/11 17.64 ---NM ---
05/29/12 17.53 ---NM ---
02/25/13 17.00 ---NM ---
10/02/13 18.77 ---NM ---
06/26/14 17.51 ---NM ---
01/28/15 17.66 ---NM ---
08/12/15 17.58 ---NM ---
03/24/11 14.49 ---NM ---
09/13/11 15.19 ---NM ---
03/24/11 21.02 ---NM ---
09/13/11 21.45 ---NM ---
05/29/12 21.32 ---NM ---
02/25/13 20.77 ---NM ---
10/02/13 23.72 ---NM ---
06/26/14 21.27 ---NM ---
01/28/15 22.91 ---NM ---
Notes:
• *: Reference point for elevation measurements; assumed elevation 100.00 feet.
• **: If free product is present in a well, ground water elevation should be calculated by: (Top of Casing Elevation - Depth to Water) + (Free Product
Thickness x 0.8581)
• ft BGS : feet below ground surface.
• NM: Not Measured.
• Top of casing information for monitoring wells were obtained from the report titled ' Semi Annual Ground Water Monitoring Report' dated March 24, 2005
prepared by CES Engineering, P. C. Well construction information, where available, are obtained from well construction records, well identification tags and
field measurements.
• Please note that well construction information for MW-6 and MWD-7 did not match existing well construction records on file. Well construction details
for these wells and MW-12 through MW-14 are based on well identification tags and the gauged well depths.
• Monitoring wells MW-15 through MW-17 were installed by Greenwood Applies Services personnel. Top of casing elevations for these wells were
surveyed by GRI personnel during the March 2009 sampling event.
RW-8 NA NA NA NA NM
RW-6 NA NA NA NA NM
RW-5 NA NA NA NA NM
RW-4 NA NA NA NA NM
RW-3 NA NA NA NA NM
NMNANANANARW-2
RW-1A NA NA NA NA NM
Page 5 of 5
Method of Measurement:
Well ID Product Type
(gas, diesel, etc.)
Date of Recovery
(mm/dd/yy)
Free Product
Recovery
Method*
Casing
Diameter
(inches)
Product
Thickness
before Recovery
(feet)
Product
Thickness after
Recovery
(feet)
Amount of Liquid
Recovered
(gallons)
Amount of
Product
Recovered
(gallons)
MW-1 2 0.57 0.00
RW-1A 4 0.01 0.00
RW-2 4 0.00 0.00
MW-19 2 0.00 0.01
MW-1 2 0.36 0.00
MW-2 2 0.00 0.00
RW-1A 4 0.00 0.00
RW-2 4 0.00 0.00
MW-19 2 0.00 0.00
MW-1 2 0.00 0.34
MW-2 2 0.00 0.00
MW-9 2 0.01 0.01
MW-1 2 3.74 0.01
MW-19 2 0.01 0.00
RW-1A 4 0.00 0.00
RW-2 4 0.00 0.00
MW-1 Gasoline 01/22/13 AFVR 2 0.00 0.00 112 20
MW-1 2 1.75 0.71
MW-19 2 0.02 0.00
MW-1 2 1.46 0.26
MW-19 2 0.01 0.00
RW-2 2 0.00 0.00
MW-1 2 0.20 0.00
MW-19 2 0.00 0.00
Notes :
• *: Bailing, Skimming, Aggressive Fluid Vapor Recovery (AFVR), Mobile Multiphase Extraction (MMPE)
• Amount of Liquid Recovered (gallons) includes Total liquids (Water and Free Product) as indicated on Disposal Manifest.
• Amount of Product Recovered (in gallons) includes only the volume of free product in the tanker at the end of the event (based on Disposal Manifest
and/or Field Notes).
Gasoline 08/29/13 AFVR 20 0
Gasoline 04/07/14 - 04/11/14 MMPE 12,228 19
Gasoline 08/08/11-08/12/11 MMPE 9,964 0
Gasoline 04/23/12-04/27/12 MMPE 6,588 0
TABLE 2
FREE PRODUCT RECOVERY RESULTS
H&S TRADING (INCIDENT NO. 10151)
Date: 05/18/18 Facility ID#: 00-0-0000009678
Interface probe at top-of-casing
AFVR05/05/18Gasoline 0945
Gasoline 02/07/11-02/11/11 MMPE 15,541 0
Gasoline 07/19/10 - 07/23/10 MMPE 16,270 0
Page 1 of 1
MW-1, MW-2,
RW-1A, RW-2,
MW-19
02/07/11 - 02/11/11 MMPE 749.50 117.22 53.73 0.29 15,541 0 0.29
MW-1 01/22/13 AFVR 2,555.57 153.52 9.60 0.01 112 20 20.01
MW-1, MW-19 08/29/13 AFVR 3,488.57 214.90 32.26 0.05 20 0 0.05
MW-1, MW-19,
RW-2 04/07/14 - 04/11/14 MMPE 2,559.77 125.45 206.62 2.43 12,228 19 21.43
MW-1, MW-19 05/05/18 AFVR 1,236.81 83.19 22.67 0.33 945 0 0.33
8.57 61,668 39 47.57
Notes:
• *: Bailing, Skimming, Aggressive Fluid Vapor Recovery (AFVR), Mobile Multiphase Extraction (MMPE)
• Amount of Vaporized Product (in gallons) is based on Vapor Emissions Summary Sheet, = lbs emitted/6.25
• Amount of Liquid Recovered includes Total liquids (Water and Free Product) as indicated on Disposal Manifest.
• Amount of Product Recovered as Liquid includes only the volume of free product in the tanker at the end of the event (based on Disposal
Manifest and/or Field Notes).
• Total Amount of Product Recovered = Amount of Vaporized Product + Amount of Product Recovered as Liquid
• Total Fluids Removed = Amount of Vaporized Product + Amount of Liquid Recovered
• Information regarding historical free product recovery activities is not available.
Total To Date 61,676.57 47.57
SUMMARY OF FLUID REMOVAL
Summary Total Fluids Removed (in gallons)Total Product Removed (in gallons)
Current Event 945.33 0.33
Totals
64.38 0.49 9,964 0
291.05 2.06 6,588 0
0.49
MW-1, MW-19,
RW-1A, RW-2 04/23/12 - 04/27/12 MMPE 1,602.86 120.30
MW-1, MW-2,
MW-19 08/08/11 - 08/12/11 MMPE 1,886.50 137.95
2.06
117.61 2.91 16,270 0 2.91
Average
Effluent
Concentration
(ppm)
Amount of
Vaporized
Product
(gallons)
Amount of
Liquid
Recovered
(gallons)
Amount of
Product
Recovered as
Liquid
(gallons)
Total Amount
of Product
Recovered
(gallons)
MW-1, RW-1A,
RW-2, MW-19 07/19/10 - 07/23/10 MMPE 4,139.62 88.01
TABLE 3
FREE PRODUCT RECOVERY EVENT INFORMATION
H&S TRADING (INCIDENT NO. 10151)
Date: 05/18/18 Facility ID #: 00-0-0000009678
Well ID Date (mm/dd/yy)
Product
Recovery
Method*
Average
Effluent
Velocity
(ft/min)
Average
Effluent
Temperature
(°F)
Date: 07/03/18
Wells Included in
Event
Product
Recovery
Method*
Date of Event
(mm/dd/yy)
Total Amount of
Free Product plus
Ground Water
Recovered (gallons)
Cost of Free
Product Recovery
Event
Cost Per Gallon
(total liquids)
MW-1, RW-1A,
RW-2, MW-19 MMPE 07/19/10 -
07/23/10 16,272.91 $11,907.50 $0.73
MW-1, MW-2,
RW-1A, RW-2,
MW-19
MMPE 02/07/11 -
02/11/11 15,541.29 $13,470.25 $0.87
MW-1, MW-2,
MW-19 MMPE 08/08/11 -
08/12/11 9,964.49 $12,050.00 $1.21
MW-1, MW-19,
RW-1A, RW-2 MMPE 04/23/12 -
04/27/12 6,588.00 $9,643.00 $1.46
MW-1 AFVR 1/22/2013 132.01 $4,594.25 $34.80
MW-1, MW-19 AFVR 8/29/2013 20.05 $3,115.25 $155.37
MW-1, MW-19,
RW-2 MMPE 04/07/14 -
04/11/14 12,230.43 $12,155.00 $0.99
MW-1, MW-19 AFVR 5/5/2018 945.03 $2,561.75 $2.71
61,694.21 $69,497.00 $1.13
Notes:
• *: Bailing, Skimming, Aggressive Fluid Vapor Recovery (AFVR), Mobile Multiphase Extraction (MMPE)
• Total Amount of Free Product Recovered = Amount of Vaporized Product + Amount of Product Recovered as Liquid
• Cost of Free Product Recovery Event includes supervision, travel, mileage, per diem, subcontractor costs, report preparation and project management.
TOTAL (to date)
Cost per gallon for the event is based on a
total volume of 15,541.29 gallons of free
product and water.
Cost per gallon for the event is based on a
total volume of 9,964.49 gallons of free
product and water.
Cost per gallon for the event is based on a
total volume of 6,590.06 gallons of free
product and water.
Cost per gallon for the event is based on a
total volume of 132.01 gallons of free
product and water.
Cost per gallon for the event is based on a
total volume of 20.05 gallons of free
product and water.
Cost per gallon for the event is based on a
total volume of 12,230.43 gallons of free
product and water.
Cost per gallon for the event is based on a
total volume of 16,272.91 gallons of free
product and water.
Cost per gallon for the event is based on a
total volume of 945.33 gallons of free
product and water.
TABLE 4
FREE PRODUCT RECOVERY COST SUMMARY
H&S TRADING (INCIDENT NO. 10151)
Facility ID #: 00-0-0000009678
Comments
EPA Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 25,000 70,000 30,000 28,500 25,000 15,000 NE NE NE
05/21/08 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
03/09/09 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
06/23/09 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
09/23/09 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
12/28/09 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
03/23/10 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
03/24/11 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
09/13/11 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
05/29/12 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
02/25/13 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
10/02/13 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
06/26/14 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
01/28/15 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
08/12/15 29.0 J <17 1,230 1,710 63.8 2,270 426 <16 819 9,100 3,120 NR NR NR NR
02/23/16 <31 <31 1,840 917 51.8 J 4,880 753 <31 1,450 19,200 E 5,610 NR NR NR NR
11/21/16 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
07/20/17 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
05/04/18 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
06/11/18 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
05/21/08 <100 <100 <100 <300 5,800 185 <100 <500 <100 122 <100 4.09 2,140 3,000 <2,000
03/09/09 8.3 J <1.4 3.2 J 3.6 J 1,400 9.5 JB <1.1 <2.0 <1.5 20 6.2 J <3.0 <100 1,500 2,800
06/23/09 2.29 J <1.65 <3.35 5.62 J 2,290 8.42 J <5.00 <8.35 <1.65 14.7 5.36 <1.50 168 1,100 803
09/23/09 6.11 <0.190 5.68 7.47 1,260 11.1 1.68 2.22 2.87 32.3 11.4 <1.50 NR NR NR
12/28/09 6.93 <0.950 6.71 7.93 2,210 12.2 2.68 J 3.26 J 4.33 J 35.7 13.2 2.24 J NR NR NR
03/23/10 8.62 <3.80 52.8 57.7 2,980 44.4 6.03 J 8.70 J 6.06 J 49.7 9.45 J 2.03 NR NR NR
03/24/11 10.4 <1.90 69.4 125 3,840 112 12.5 7.45 J 13.8 341 81.6 NR 1,890 1,320 1,210
09/13/11 8.7 J <6.4 25.9 56.8 2,070 42.6 <5.0 5.4 J <5.4 93.6 34.7 <5.0 NR NR NR
05/29/12 <6.5 <6.4 18.3 J <15 2,350 21.8 J <5.0 6.2 J <5.4 45.6 <5.0 NR NR NR NR
02/25/13 7.0 <0.10 13.5 5.9 811 20.3 3.0 5.0 2.4 27.4 1.7 NR NR NR NR
10/02/13 2.2 <0.10 1.8 0.20 J 127 5.9 2.1 0.93 2.0 9.7 0.24 J NR NR NR NR
06/26/14 18.2 0.12 J 1.3 0.65 J 180 4.6 0.69 5.4 0.54 1.3 0.12 J NR NR NR NR
01/28/15 4.1 <0.17 0.16 J <0.43 19.2 <0.12 0.14 J 1.0 <0.16 <0.14 <0.14 NR NR NR NR
08/12/15 7.7 <0.17 3.2 0.45 J 42.4 5.4 1.4 3.5 0.88 4.6 0.26 J NR NR NR NR
02/23/16 5.0 <0.13 3.2 1.9 31.6 24.2 6.1 2.5 13.6 6.1 J 61.8 E NR NR NR NR
06/11/18 3.5 <0.13 3.2 0.56 J 8.4 19.5 4.1 2.2 4.4 16.4 0.61 NR NR NR NR
MW-1
MW-2 LeadMTBEC5-C8 AliphaticsC9-C12 AliphaticsC9-C10 Aromatics2L Standard (mg/l)
GCL (mg/l)NaphthaleneIsopropylbenzeneIPEn-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneContaminant of
Concern
BenzeneTolueneEthylbenzeneXylenesTABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
H&S TRADING (INCIDENT NO. 10151)
Date : 07/03/18 Facility ID # : 0-009678
Analytical Method
EPA Method 6200B MADEP Method VPH
Page 1 of 10
EPA Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 25,000 70,000 30,000 28,500 25,000 15,000 NE NE NELeadMTBEC5-C8 AliphaticsC9-C12 AliphaticsC9-C10 Aromatics2L Standard (mg/l)
GCL (mg/l)NaphthaleneIsopropylbenzeneIPEn-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneContaminant of
Concern
BenzeneTolueneEthylbenzeneXylenesTABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
H&S TRADING (INCIDENT NO. 10151)
Date : 07/03/18 Facility ID # : 0-009678
Analytical Method
EPA Method 6200B MADEP Method VPH
05/21/08 0.910 I <1.0 <1.0 <3.0 895 <1.0 0.510 I 2.37 I 0.350 I 1.13 0.480 I 16.3 112 173 <100
03/09/09 <0.60 <0.70 <0.50 <1.0 550 1.2 JB <0.55 <1.0 <0.75 <0.70 <0.50 4.1 <100 170 100
06/23/09 <0.400 <0.660 <1.34 <2.66 211 <2.00 <2.00 <3.34 <0.660 <0.660 <0.660 7.41 <100 <100 <100
09/23/09 <0.140 <0.190 <0.150 <0.220 250 <0.500 <0.150 0.718 J <0.220 <0.150 <0.180 18.6 NR NR NR
12/28/09 <0.140 <0.190 <0.150 <0.220 291 <0.500 <0.150 0.815 J <0.220 <0.150 <0.180 8.11 NR NR NR
03/23/10 <0.140 <0.190 <0.150 <0.220 359 <0.500 <0.150 1.32 <0.220 <0.150 <0.180 4.33 NR NR NR
03/24/11 <0.700 <0.950 <0.750 <1.10 882 <2.50 0.764 J 2.59 J <1.10 1.34 J <0.900 NR 522 105 122
09/13/11 0.36 J <0.13 <0.15 0.64 J 217 6.1 0.32 J 0.80 0.39 J 7.5 2.3 11.6 NR NR NR
05/29/12 <1.3 <1.3 <1.5 <3.0 434 <1.0 <1.0 1.6 J <1.1 <1.0 <1.0 NR NR NR NR
02/25/13 0.43 J <0.10 <0.10 <0.22 285 0.44 J 0.21 J 1.0 0.14 J 0.17 J <0.10 NR NR NR NR
10/02/13 1.8 J <0.50 <0.50 <1.1 145 1.4 J 0.67 J 1.6 J <0.50 0.77 J <0.50 NR NR NR NR
06/26/14 1.4 <0.10 0.30 J 0.27 J 245 0.97 0.79 2.7 0.78 2.0 0.22 J NR NR NR NR
01/28/15 0.61 J <0.42 <0.38 <1.1 119 0.98 J <0.30 0.92 J <0.39 <0.34 <0.34 NR NR NR NR
08/12/15 1.7 <0.17 <0.15 <0.43 139 1.2 0.60 2.0 0.55 2.2 0.57 NR NR NR NR
02/23/16 0.26 J <0.13 0.14 J <0.31 84.5 40.6 0.35 J 0.69 <0.13 7.4 1.6 NR NR NR NR
06/11/18 <0.13 <0.13 <0.13 <0.26 22.2 <0.13 <0.13 1.3 <0.13 <0.13 <0.13 NR NR NR NR
05/21/08 <1.0 <1.0 <1.0 <3.0 5.67 <1.0 <1.0 0.600 I <1.0 <1.0 <1.0 4.56 <100 <100 <100
03/09/09 <0.60 <0.70 <0.50 <1.0 4.2 J 0.82 JB <0.55 <1.0 <0.75 <0.70 <0.50 3.3 <100 <100 <100
06/23/09 <0.200 <0.330 <0.670 <1.33 10.3 <1.00 <1.00 <1.67 <0.330 1.09 0.440 J <1.50 <100 <100 <100
09/23/09 <0.140 <0.190 <0.150 <0.220 1.67 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 23.9 NR NR NR
12/28/09 <0.140 <0.190 <0.150 <0.220 1.02 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 30.3 NR NR NR
03/23/10 <0.140 <0.190 <0.150 <0.220 0.690 J <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 14.6 NR NR NR
03/24/11 <0.140 <0.190 <0.150 <0.220 0.766 J <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 NR <100 <100 <100
09/13/11 <0.13 <0.13 <0.15 <0.30 0.84 0.13 J <0.10 0.19 J <0.11 <0.10 <0.10 32.3 NR NR NR
05/29/12 <0.13 <0.13 <0.15 <0.30 0.81 <0.10 <0.10 0.14 J <0.11 <0.10 <0.10 NR NR NR NR
02/25/13 <0.10 <0.10 <0.10 <0.22 3.5 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
10/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/26/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/28/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
08/12/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
MW-3
MW-4
Page 2 of 10
EPA Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 25,000 70,000 30,000 28,500 25,000 15,000 NE NE NELeadMTBEC5-C8 AliphaticsC9-C12 AliphaticsC9-C10 Aromatics2L Standard (mg/l)
GCL (mg/l)NaphthaleneIsopropylbenzeneIPEn-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneContaminant of
Concern
BenzeneTolueneEthylbenzeneXylenesTABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
H&S TRADING (INCIDENT NO. 10151)
Date : 07/03/18 Facility ID # : 0-009678
Analytical Method
EPA Method 6200B MADEP Method VPH
05/21/08 8.87 <1.0 5.65 <3.0 246 12.2 9.84 21.1 9.09 <1.0 <1.0 25.6 871 134 251
03/09/09 120 19 J 560 2,000 1,700 140 B <2.2 18 J 92 710 140 5.4 260 2,400 2,100
06/23/09 153 <33.0 333 709 4,840 116 J <100 <167 59.4 J 249 191 2.93 J 365 839 1,340
09/23/09 131 34.2 1,310 4,860 6,460 250 112 17.8 J 212 1,490 295 37.7 NR NR NR
12/28/09 71.2 6.01 386 905 1,150 121 71.7 9.67 114 510 85.2 2.72 J NR NR NR
03/23/10 1.20 <0.190 1.87 1.16 66.0 1.61 2.02 <1.03 3.12 2.08 <0.180 5.63 NR NR NR
03/24/11 3.77 J <0.950 <0.750 <1.10 149 3.84 J 18.5 13.9 13.0 3.11 J <0.900 NR 533 <100 179
09/13/11 100 6.5 J 712 2,236 2,060 160 80.6 17.1 J 142 932 199 <5.0 NR NR NR
05/29/12 46.1 2.6 J 277 850 545 B 85.4 59.3 15.3 90.3 498 86.5 NR NR NR NR
02/25/13 6.9 <0.10 14.8 23.6 J 72.2 15.3 12.0 18.2 15.8 44.7 5.8 NR NR NR NR
10/02/13 25.9 0.67 188 366 764 50.9 40.3 16.9 53.0 277 39.8 NR NR NR NR
06/26/14 33.4 0.29 J 154 270 262 88.3 74.4 18.5 112 422 55.7 NR NR NR NR
01/28/15 28.6 <1.7 132 376 377 98.2 53.1 13.5 90.1 481 72.6 NR NR NR NR
08/12/15 3.1 0.28 J 4.1 16.6 65.7 16.5 19.0 15.9 20.1 45.8 8.6 NR NR NR NR
02/23/16 6.0 0.17 J 28.6 54.3 61.0 42.6 19.7 8.8 28.3 161 19.1 NR NR NR NR
06/11/18 9.3 <0.63 46.9 89.7 143 42.2 33.2 17.0 47.8 231 33.6 NR NR NR NR
05/21/08 <50 <50 <50 <150 2,120 <50 <50 <250 <50 <50 <50 8.96 1,400 1,100 <1,000
03/09/09 <4.8 <5.6 17 J 48 J 2,800 14 JB <4.4 <8.0 <6.0 23 J 5.1 J 3.8 <100 2,300 620
06/23/09 3.66 <1.65 <3.35 <6.65 2,590 5.49 J <5.00 <8.35 <1.65 <1.65 <1.65 <1.50 806 204 232
09/23/09 6.19 <0.190 10.0 9.05 2,880 13.1 2.12 10.3 2.61 7.78 0.960 J 11.3 NR NR NR
12/28/09 2.85 J <0.950 4.53 J 6.19 964 17.7 <0.750 6.02 1.84 J 5.24 <0.900 6.79 NR NR NR
03/23/10 3.94 <0.190 0.386 J <0.220 <0.250 <0.500 0.384 J 8.26 0.235 J <0.150 <0.180 <1.50 NR NR NR
03/24/11 6.15 J <1.90 2.46 J <2.20 361 <5.00 <1.50 7.90 J <2.20 2.44 J <1.80 NR 347 696 476
09/13/11 4.5 <0.64 2.5 1.4 J 140 2.0 J 0.70 J 5.7 0.66 J 1.6 J <0.50 <5.0 NR NR NR
05/29/12 5.5 <0.64 1.9 J <1.5 179 <0.50 0.73 J 7.5 <0.54 <0.50 <0.50 NR NR NR NR
02/25/13 5.1 <0.10 2.2 0.68 J 183 3.2 0.97 7.4 0.89 2.5 <0.10 NR NR NR NR
10/02/13 4.0 <0.10 0.39 J 0.48 J 70.1 1.3 0.28 J 5.1 0.14 J 0.30 J <0.10 NR NR NR NR
06/26/14 3.1 <0.10 0.34 J <0.20 46.4 0.73 0.31 J 6.4 0.15 J <0.10 <0.10 NR NR NR NR
01/28/15 3.6 <0.17 0.33 J <0.43 21.6 0.61 0.21 J 5.1 <0.16 <0.14 <0.14 NR NR NR NR
08/12/15 3.3 <0.17 0.58 <0.43 25.8 <0.12 0.36 J 5.2 0.20 J <0.14 <0.14 NR NR NR NR
02/23/16 2.7 <0.13 0.24 J <0.31 17.3 0.86 0.19 J 5.6 <0.13 <0.13 <0.13 NR NR NR NR
06/11/18 1.6 <0.13 <0.13 <0.26 14.3 <0.13 0.28 J 3.5 <0.13 <0.13 <0.13 NR NR NR NR
MW-6
MW-5
Page 3 of 10
EPA Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 25,000 70,000 30,000 28,500 25,000 15,000 NE NE NELeadMTBEC5-C8 AliphaticsC9-C12 AliphaticsC9-C10 Aromatics2L Standard (mg/l)
GCL (mg/l)NaphthaleneIsopropylbenzeneIPEn-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneContaminant of
Concern
BenzeneTolueneEthylbenzeneXylenesTABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
H&S TRADING (INCIDENT NO. 10151)
Date : 07/03/18 Facility ID # : 0-009678
Analytical Method
EPA Method 6200B MADEP Method VPH
05/21/08 <1.0 <1.0 <1.0 <3.0 5.13 <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 2.34 I <100 <100 <100
03/09/09 <0.60 <0.70 <0.50 1.3 J 5.6 0.81 JB <0.55 <1.0 <0.75 1.4 J <0.50 <3.0 <100 <100 <100
06/23/09 1.03 0.960 J <0.670 <1.33 17.1 <1.00 <1.00 <1.67 <0.330 0.344 J <0.330 <1.50 <100 251 <100
09/23/09 1.34 1.79 <0.150 1.96 20.1 1.54 <0.150 <0.200 <0.220 1.84 0.430 J <1.50 NR NR NR
12/28/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 2.07 J NR NR NR
03/23/10 <0.140 <0.190 <0.150 <0.220 0.789 J <0.500 <0.150 <0.200 <0.220 0.226 J <0.180 <1.50 NR NR NR
03/24/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 0.157 J <0.180 NR <100 <100 <100
09/13/11 <0.13 <0.13 0.44 J 3.26 J 1.6 7.8 0.30 J <0.11 0.70 16.3 6.6 <5.0 NR NR NR
05/29/12 <0.13 <0.13 <0.15 <0.30 0.23 J <0.10 <0.10 <0.11 <0.11 <0.10 <0.10 NR NR NR NR
02/25/13 0.12 J 0.58 0.13 J <0.22 5.2 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/26/14 <0.10 <0.10 <0.10 <0.20 0.47 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
01/28/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.12 <0.16 <0.16 <0.14 <0.14 NR NR NR NR
08/12/15 <0.17 <0.17 <0.15 <0.43 0.28 J <0.12 <0.12 <0.16 <0.16 <0.14 <0.14 NR NR NR NR
05/21/08 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 22.7 <100 <100 <100
03/09/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <0.55 <1.0 <0.75 <0.70 <0.50 3.4 <100 <100 <100
06/23/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.00 <1.67 <0.330 <0.330 <0.330 1.77 J <100 <100 <100
09/23/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 10.1 NR NR NR
12/28/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 9.75 NR NR NR
03/23/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 1.67 NR NR NR
03/24/11 <0.140 0.875 J <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 NR <100 <100 <100
09/13/11 <0.13 <0.13 6.7 <0.30 0.63 <0.10 <0.10 <0.11 <0.11 <0.10 <0.10 17.4 NR NR NR
05/29/12 <0.13 0.43 J <0.15 <0.30 7.4 <0.10 <0.10 <0.11 <0.11 <0.10 <0.10 NR NR NR NR
02/25/13 <0.10 <0.10 <0.10 <0.22 0.38 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
10/02/13 <0.10 <0.10 <0.10 <0.22 0.94 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/26/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
01/28/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.12 <0.16 <0.16 <0.14 <0.14 NR NR NR NR
08/12/15 <0.17 <0.17 <0.15 <0.43 0.38 J <0.12 <0.12 <0.16 <0.16 <0.14 <0.14 NR NR NR NR
MWD-7
MW-8
Page 4 of 10
EPA Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 25,000 70,000 30,000 28,500 25,000 15,000 NE NE NELeadMTBEC5-C8 AliphaticsC9-C12 AliphaticsC9-C10 Aromatics2L Standard (mg/l)
GCL (mg/l)NaphthaleneIsopropylbenzeneIPEn-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneContaminant of
Concern
BenzeneTolueneEthylbenzeneXylenesTABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
H&S TRADING (INCIDENT NO. 10151)
Date : 07/03/18 Facility ID # : 0-009678
Analytical Method
EPA Method 6200B MADEP Method VPH
05/21/08 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/09/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <0.55 <1.0 <0.75 <0.70 <0.50 17.5 <100 <100 <100
06/23/09 0.281 J 1.17 29.9 18.1 44.7 13.8 14.4 <1.67 22.8 34.2 28.7 8.54 108 264 253
09/23/09 <0.140 <0.190 <0.150 <0.220 37.9 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 29.6 NR NR NR
12/28/09 <0.140 0.487 J 15.2 8.92 17.4 3.24 9.28 <0.200 16.4 11.1 2.27 20.7 NR NR NR
03/23/10 <0.140 <0.190 <0.150 <0.220 4.21 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 9.11 NR NR NR
03/24/11 <0.140 <0.190 <0.150 <0.220 0.363 J <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 NR <100 <100 <100
09/13/11 <0.13 <0.13 <0.15 <0.30 1.3 <0.10 0.40 J <0.11 <0.11 <0.10 <0.10 21.3 NR NR NR
05/29/12 <0.13 <0.13 <0.15 <0.30 1.1 <0.10 <0.10 <0.11 <0.11 <0.10 <0.10 NR NR NR NR
02/25/13 <0.10 <0.10 <0.10 <0.22 18.5 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
10/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/26/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
01/28/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.12 <0.16 <0.16 <0.14 <0.14 NR NR NR NR
08/12/15 <0.17 <0.17 <0.15 <0.43 0.32 J <0.12 0.30 J <0.16 <0.16 <0.14 <0.14 NR NR NR NR
05/21/08 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 6.15 <100 <100 <100
03/09/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <0.55 <1.0 <0.75 <0.70 <0.50 11.0 <100 <100 <100
06/23/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.00 <1.67 <0.330 <0.330 <0.330 6.59 <100 <100 <100
09/23/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 21.0 NR NR NR
12/28/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 19.2 NR NR NR
03/23/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 14.4 NR NR NR
03/24/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 NR <100 <100 <100
09/13/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.11 <0.11 <0.10 <0.10 28.6 NR NR NR
05/29/12 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
05/21/08 <1.0 19.3 <1.0 <3.0 <1.0 <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 43.9 <100 <100 <100
03/09/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <0.55 <1.0 <0.75 <0.70 <0.50 11.1 <100 <100 <100
06/23/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.00 <1.67 <0.330 <0.330 <0.330 10.2 <100 <100 <100
09/23/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 51.5 NR NR NR
12/28/09 <0.140 30.1 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 16.2 NR NR NR
03/23/10 <0.140 4.22 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 7.83 NR NR NR
03/24/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 NR <100 <100 <100
09/13/11 <0.13 21.1 <0.15 <0.30 <0.13 <0.10 <0.10 <0.11 <0.11 <0.10 <0.10 20.7 NR NR NR
05/29/12 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
06/26/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
MW-9
MW-10
MW-11
Page 5 of 10
EPA Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 25,000 70,000 30,000 28,500 25,000 15,000 NE NE NELeadMTBEC5-C8 AliphaticsC9-C12 AliphaticsC9-C10 Aromatics2L Standard (mg/l)
GCL (mg/l)NaphthaleneIsopropylbenzeneIPEn-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneContaminant of
Concern
BenzeneTolueneEthylbenzeneXylenesTABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
H&S TRADING (INCIDENT NO. 10151)
Date : 07/03/18 Facility ID # : 0-009678
Analytical Method
EPA Method 6200B MADEP Method VPH
05/21/08 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 9.44 <100 <100 <100
03/09/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <0.55 <1.0 <0.75 <0.70 <0.50 12.3 <100 <100 <100
06/23/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.00 <1.67 <0.330 <0.330 <0.330 3.49 <100 <100 <100
09/23/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 27.8 NR NR NR
12/28/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 19.0 NR NR NR
03/23/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 0.767 J 0.309 J 14.9 NR NR NR
03/24/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 NR <100 <100 <100
09/13/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.11 <0.11 <0.10 <0.10 54.7 NR NR NR
05/29/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.11 <0.11 <0.10 <0.10 NR NR NR NR
02/25/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
10/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/26/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
01/28/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.12 <0.16 <0.16 <0.14 <0.14 NR NR NR NR
08/12/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.12 <0.16 <0.16 <0.14 <0.14 NR NR NR NR
05/21/08 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 26.8 <100 <100 <100
03/09/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <0.55 <1.0 <0.75 <0.70 <0.50 4.7 <100 <100 <100
06/23/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.00 <1.67 <0.330 <0.330 <0.330 4.39 <100 <100 <100
09/23/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 7.06 NR NR NR
12/28/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 16.9 NR NR NR
03/23/10 <0.140 0.298 J 0.443 J 2.69 <0.250 0.681 J 0.162 J <0.200 0.281 J 3.38 <0.180 8.30 NR NR NR
03/24/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
09/13/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
05/29/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/26/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
05/21/08 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 <1.0 <5.0 <1.0 0.470 I <1.0 80.3 <100 <100 <100
03/09/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <0.55 <1.0 <0.75 <0.70 <0.50 2.2 J <100 <100 <100
06/23/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.00 <1.67 <0.330 <0.330 <0.330 <1.50 <100 <100 <100
09/23/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 11.1 NR NR NR
12/28/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 6.13 NR NR NR
03/23/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 5.78 NR NR NR
03/24/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 NR <100 <100 <100
09/13/11 <0.13 <0.13 <0.15 <0.30 <0.13 0.33 J <0.10 <0.11 <0.11 0.14 J <0.10 <5.0 NR NR NR
05/29/12 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
06/26/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
MW-14
MW-13
MW-12
Page 6 of 10
EPA Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 25,000 70,000 30,000 28,500 25,000 15,000 NE NE NELeadMTBEC5-C8 AliphaticsC9-C12 AliphaticsC9-C10 Aromatics2L Standard (mg/l)
GCL (mg/l)NaphthaleneIsopropylbenzeneIPEn-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneContaminant of
Concern
BenzeneTolueneEthylbenzeneXylenesTABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
H&S TRADING (INCIDENT NO. 10151)
Date : 07/03/18 Facility ID # : 0-009678
Analytical Method
EPA Method 6200B MADEP Method VPH
03/09/09 17 <0.70 3.2 J 1.6 J 100 6.0 B 12 <1.0 10 8.1 2.7 J 23.5 <100 240 140
06/23/09 45.3 <0.660 <1.34 10 192 21.8 23.5 <3.34 17.4 4.74 5.96 4.59 569 499 390
09/23/09 28.3 <0.190 7.49 1.09 197 10.6 35.9 0.901 J 46.2 37.0 4.25 22.5 NR NR NR
12/28/09 3.92 <0.190 <0.150 <0.220 94.8 1.32 8.05 0.492 J 4.71 4.92 2.40 32.2 NR NR NR
03/23/10 4.44 <0.190 1.85 26.9 107 6.86 7.59 0.493 J 2.91 44.2 5.26 18.7 NR NR NR
03/24/11 5.79 <0.950 0.835 J <1.10 180 10.4 29.2 <1.00 16.3 26.1 7.95 NR 655 102 420
09/13/11 4.3 <0.13 3.4 3.1 104 8.5 19.9 0.70 10.6 20.8 0.52 16.2 NR NR NR
05/29/12 0.70 <0.13 <0.15 <0.30 40.7 0.28 J 6.1 0.30 J 1.8 1.5 <0.10 NR NR NR NR
02/25/13 1.7 <0.10 <0.10 <0.22 55.9 0.23 J 6.1 0.51 0.70 <0.10 <0.10 NR NR NR NR
10/02/13 5.3 <0.10 0.18 J <0.22 59.8 2.0 24.7 0.81 2.9 0.69 <0.10 NR NR NR NR
06/26/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
08/12/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/09/09 <1.2 <1.4 <1.0 <2.1 <1.0 <1.2 <1.1 <2.0 <1.5 <1.4 <1.0 368 NR NR NR
06/23/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.00 <1.67 <0.330 <0.330 <0.330 22.2 <100 <100 <100
09/23/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 38.6 NR NR NR
12/28/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 416 NR NR NR
03/23/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 23.5 NR NR NR
03/24/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 NR <100 <100 <100
09/13/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.11 <0.11 <0.10 <0.10 85.5 NR NR NR
05/29/12 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
06/26/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
08/12/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/09/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <0.55 <1.0 <0.75 <0.70 <0.50 <3.0 <100 <100 <100
06/23/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.00 <1.67 <0.330 <0.330 <0.330 13.4 <100 <100 <100
09/23/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 29.4 NR NR NR
12/28/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 6.52 NR NR NR
03/23/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 6.61 NR NR NR
03/24/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 NR <100 <100 <100
09/13/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.11 <0.11 <0.10 <0.10 7.7 NR NR NR
05/29/12 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
06/26/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
08/12/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
MW-15
MW-16
MW-17
Page 7 of 10
EPA Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 25,000 70,000 30,000 28,500 25,000 15,000 NE NE NELeadMTBEC5-C8 AliphaticsC9-C12 AliphaticsC9-C10 Aromatics2L Standard (mg/l)
GCL (mg/l)NaphthaleneIsopropylbenzeneIPEn-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneContaminant of
Concern
BenzeneTolueneEthylbenzeneXylenesTABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
H&S TRADING (INCIDENT NO. 10151)
Date : 07/03/18 Facility ID # : 0-009678
Analytical Method
EPA Method 6200B MADEP Method VPH
12/28/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 56.6 <150 <150 <100
03/23/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 25.2 NR NR NR
03/24/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 NR <100 <100 <100
09/13/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.11 <0.11 <0.10 <0.10 25.8 NR NR NR
05/29/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.11 <0.11 <0.10 <0.10 NR NR NR NR
02/25/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
10/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/26/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
01/28/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.12 <0.16 <0.16 <0.14 <0.14 NR NR NR NR
03/24/11 63.7 <9.50 63.6 484 1,790 513 28.3 J <10.0 53.2 743 200 NR 4,030 186,000 422,000
09/13/11 43.0 9.5 J 69.9 444 1,460 253 20.3 J 6.0 J 38.0 429 124 53.3 NR NR NR
05/29/12 97.5 68.8 1,650 10,700 1,930 4,150 747 <11 1,560 9,620 4,240 NR NR NR NR
02/25/13 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
10/02/13 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
06/26/14 21.5 0.44 J 21.8 86.9 611 50.2 6.0 2.8 10.4 97.4 26.4 NR NR NR NR
01/28/15 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
08/12/15 48.4 <0.17 47.9 87.9 1,490 41.2 27.2 7.1 29.3 260 46.9 NR NR NR NR
02/23/16 7.7 0.23 J 134 262 102 42.1 27.7 0.64 211 248 269 NR NR NR NR
11/21/16 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
07/20/17 3.8 <0.31 18.8 33.6 76.1 84.2 8.1 1.1 J 13.1 149 15.2 NR NR NR NR
05/04/18 3.9 <0.13 18.9 31.3 185 95.7 NR 5.2 NR NR NR NR NR NR NR
06/11/18 1.4 J <0.63 4.2 8.1 209 129 7.3 3.5 14.6 93.5 19.7 NR NR NR NR
03/24/11 <0.140 <0.190 <0.150 <0.220 2.88 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 NR <100 <100 <100
09/13/11 <0.13 <0.13 <0.15 <0.30 1.3 <0.10 <0.10 <0.11 <0.11 <0.10 <0.10 64.8 NR NR NR
05/29/12 <0.13 <0.13 <0.15 <0.30 0.40 J <0.10 <0.10 <0.11 <0.11 <0.10 <0.10 NR NR NR NR
02/25/13 <0.10 <0.10 <0.10 <0.22 16.8 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
10/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/26/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/24/11 <0.140 1.29 <0.150 <0.220 4.18 <0.500 <0.150 <0.200 <0.220 0.172 J <0.180 NR <100 <100 <100
09/13/11 <0.13 <0.13 <0.15 <0.30 0.84 <0.10 <0.10 <0.11 <0.11 <0.10 <0.10 18.3 NR NR NR
05/29/12 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
08/12/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.12 <0.16 <0.16 <0.14 <0.14 NR NR NR NR
MW-18
MW-19
MW-20
RW-1
Page 8 of 10
EPA Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 25,000 70,000 30,000 28,500 25,000 15,000 NE NE NELeadMTBEC5-C8 AliphaticsC9-C12 AliphaticsC9-C10 Aromatics2L Standard (mg/l)
GCL (mg/l)NaphthaleneIsopropylbenzeneIPEn-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneContaminant of
Concern
BenzeneTolueneEthylbenzeneXylenesTABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
H&S TRADING (INCIDENT NO. 10151)
Date : 07/03/18 Facility ID # : 0-009678
Analytical Method
EPA Method 6200B MADEP Method VPH
03/24/11 4.62 <0.190 0.917 J 0.612 J 573 1.60 0.908 J 2.55 0.489 J 0.759 J <0.180 NR 224 <100 <100
09/13/11 14.9 J <6.4 11.5 J 59.6 1,260 26.5 <5.0 6.9 J 6.8 J 112 40.8 <5.0 NR NR NR
05/29/12 7.7 <1.3 4.3 J 10.1 J 748 9.0 1.2 J 4.1 J 1.5 J 12.5 2.5 J NR NR NR NR
02/25/13 0.99 <0.10 0.66 0.75 J 381 3.0 0.97 3.2 1.4 1.7 0.32 J NR NR NR NR
10/02/13 18.1 <0.10 4.7 3.8 1,300 11.7 5.6 7.3 7.3 8.6 1.5 NR NR NR NR
06/26/14 1.8 J <1.0 2.3 J 7.3 J 271 17.5 1.6 J 4.7 2.4 J 27.7 8.7 NR NR NR NR
01/28/15 <0.17 <0.17 <0.15 <0.43 153 <0.12 <0.12 2.2 <0.16 <0.14 <0.14 NR NR NR NR
08/12/15 1.4 <0.17 0.29 J 1.5 281 6.7 2.0 5.1 2.3 7.4 1.4 NR NR NR NR
03/24/11 78.6 2.93 J 9.80 94.8 3,430 55.1 3.70 J 13.7 4.01 J 101 23.5 NR 1,690 1,190 809
09/13/11 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
05/29/12 51.9 <6.4 <7.3 15.2 J 2,830 6.6 J <5.0 14.5 J <5.4 11.8 J <5.0 NR NR NR NR
02/25/13 4.3 J <1.0 1.3 J 6.1 J 242 16.8 <1.0 10.9 <1.0 20.8 7.0 NR NR NR NR
10/02/13 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
06/26/14 44.3 4.7 J 5.9 J 23.8 969 17.9 <2.0 14.1 <2.0 33.8 27.3 NR NR NR NR
01/28/15 5.7 <1.7 <1.5 4.3 J 345 4.8 J <1.2 11.4 <1.6 6.5 9.4 NR NR NR NR
11/21/16 8.8 <0.13 1.0 4.2 43.2 5.9 0.61 7.7 0.58 8.5 6.0 NR NR NR NR
07/20/17 3.8 <0.13 <0.13 <0.25 84.8 1.9 0.14 J 7.8 <0.13 0.80 0.40 J NR NR NR NR
06/11/18 0.96 J <0.25 <0.25 <0.50 76.3 1.4 <0.25 7.4 <0.25 <0.25 <0.25 NR NR NR NR
03/24/11 <0.280 <0.380 <0.300 <0.440 18.2 <1.00 <0.300 0.552 J <0.440 0.354 J <0.360 NR <100 <100 <100
09/13/11 18.3 <0.13 9.2 <0.30 151 1.4 8.4 1.6 15.8 <0.10 <0.10 10.6 NR NR NR
05/29/12 0.38 J <0.13 <0.15 <0.30 4.1 <0.10 0.13 J 0.25 J <0.11 <0.10 <0.10 NR NR NR NR
02/25/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/26/14 <0.10 <0.10 <0.10 <0.20 2.7 <0.10 <0.10 0.34 J <0.10 <0.10 <0.10 NR NR NR NR
01/28/15 <0.17 <0.17 <0.15 <0.43 0.86 <0.12 0.20 J 0.28 J <0.16 <0.14 <0.14 NR NR NR NR
08/12/15 <0.17 <0.17 <0.15 <0.43 2.2 <0.12 <0.12 <0.16 <0.16 <0.14 <0.14 NR NR NR NR
03/24/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
09/13/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
05/29/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/24/11 3.06 <0.190 0.724 J 2.22 26.2 0.614 J 0.536 J 4.21 0.628 J 2.83 0.512 J NR 124 <100 <100
09/13/11 29.9 <0.13 4.6 4.32 J 293 4.5 5.7 6.3 4.7 13.1 1.0 6.7 NR NR NR
05/29/12 7.8 <0.13 <0.15 <0.30 132 0.12 J 0.68 5.4 <0.11 0.12 J <0.10 NR NR NR NR
02/25/13 <0.10 <0.10 <0.10 <0.22 1.2 <0.15 <0.10 2.5 <0.10 <0.10 <0.10 NR NR NR NR
10/02/13 141 94.1 390 1,650 1,440 97.4 30.6 6.5 48.5 458 88.6 NR NR NR NR
06/26/14 <0.10 <0.10 <0.10 <0.20 3.3 <0.10 <0.10 3.2 <0.10 <0.10 <0.10 NR NR NR NR
01/28/15 0.34 J <0.17 <0.15 <0.43 4.0 <0.12 0.25 J 2.7 <0.16 <0.14 <0.14 NR NR NR NR
08/12/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.12 1.9 <0.16 <0.14 <0.14 NR NR NR NR
RW-2
RW-1A
RW-3
RW-4
RW-5
Page 9 of 10
EPA Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 25,000 70,000 30,000 28,500 25,000 15,000 NE NE NELeadMTBEC5-C8 AliphaticsC9-C12 AliphaticsC9-C10 Aromatics2L Standard (mg/l)
GCL (mg/l)NaphthaleneIsopropylbenzeneIPEn-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneContaminant of
Concern
BenzeneTolueneEthylbenzeneXylenesTABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
H&S TRADING (INCIDENT NO. 10151)
Date : 07/03/18 Facility ID # : 0-009678
Analytical Method
EPA Method 6200B MADEP Method VPH
03/24/11 <0.140 <0.190 <0.150 <0.220 1.26 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 NR <100 <100 <100
09/13/11 <0.13 <0.13 <0.15 <0.30 0.31 J <0.10 <0.10 <0.11 <0.11 <0.10 <0.10 <5.0 NR NR NR
05/29/12 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
03/24/11 1.25 <0.190 <0.150 <0.220 89.8 <0.500 <0.150 0.923 J <0.220 <0.150 <0.180 NR <100 <100 <100
09/13/11 <0.13 <0.13 <0.15 <0.30 1.3 0.65 <0.10 0.38 J <0.11 0.27 J <0.10 5.3 NR NR NR
05/29/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
05/29/12 <0.13 <0.13 <0.15 <0.30 10.6 <0.10 <0.10 0.24 J <0.11 <0.10 <0.10 NR NR NR NR
02/25/13 6.6 <0.10 <0.10 <0.22 461 1.3 0.17 J 2.4 <0.10 0.12 J <0.10 NR NR NR NR
10/02/13 0.15 J <0.10 0.11 J 0.21 J 308 0.84 <0.10 1.7 <0.10 0.14 J <0.10 NR NR NR NR
06/26/14 0.28 J <0.10 <0.10 <0.20 10.7 <0.10 <0.10 0.15 J <0.10 <0.10 <0.10 NR NR NR NR
01/28/15 <0.17 <0.17 <0.15 <0.43 0.52 <0.12 <0.12 0.31 J <0.16 <0.14 <0.14 NR NR NR NR
02/23/16 <0.13 <0.13 <0.13 <0.31 <0.13 48.3 <0.13 <0.13 0.22 J 2.4 0.41 J NR NR NR NR
03/07/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
11/21/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
06/26/14 <0.10 <0.10 <0.10 <0.20 0.56 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
01/28/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.12 <0.16 <0.16 <0.14 <0.14 NR NR NR NR
Notes:
• Results reported in µg/l (micrograms per liter).
• 2L Standard: as specified in T15A NCAC 2L.0202.
• GCL: Gross contamination level.
• NE: Standard not established.
• FP: Free product.
• <: Less than the method detection limit specified in the laboratory report.
• Concentrations in bold face type exceeded the 2L Standard.
• I or J: Estimated value.
• A concentration of 1,1,2,2-tetrachloroethane (46.8 µg/l in MW-19) that exceeded the MAC was reported in the ground water sample collected on June 11, 2018.
• NS: Not requested.
• V or B: Present in laboratory blank.
• E: Indicates value exceeds calibration range.
• NS: Not sampled.
• For other compounds reported which did not exceed the 2L Standards, refer to the laboratory reports.
WSW-34
RW-6
RW-8
WSW-12
Page 10 of 10

APPENDICES

APPENDIX A
AFVR Data and Calculations
AGGRESSIVE FLUID VAPOR RECOVERY EVENT DATA SHEET
Site Name :H & S Trading
Incident Number :10151
Average Depth to Ground Water :22.41
Well Name:MW-1, MW-19 Inner Dia. of Well (inches):2
Blower Specifications For Vacuum Truck (e.g: 2500 cfm @ 24 in. of Hg) :680 cfm @ 18" of Hg
Diameter of Exhaust Stack (inches) :6
Start Time :08:15 Date :05/05/18
End Time :16:15
Note: Take all the readings listed below every 15 minutes for the first 2 hours of the test and every
30 minutes thereafter.
Test Conducted By (AFVR Contractor):Greenwood Applied Services, LLC
Test Supervised By (Consultant):Geological Resources, Inc.
Frequency Time Vacuum Exhaust Velocity Temperature Rel. Humidity OVA
(min)(in. of Hg)(ft/min)(°F)(%)(ppm)
0 8:15 26.00 1,338 76.2 81.7 158.2
15 8:30 26.00 1,322 76.2 66.9 56.9
30 8:45 26.00 1,704 84.5 69.1 45.5
45 9:00 26.00 1,320 84.4 61.5 25.3
60 9:15 26.00 1,339 83.4 62.5 22.1
75 9:30 26.00 1,440 83.2 58.6 16.7
90 9:45 26.00 1,436 85.7 55.3 14.5
105 10:00 26.00 1,419 85.9 53.7 12.9
120 10:15 26.00 1,392 86.1 62.6 12.4
150 10:45 26.00 1,308 89.4 42.7 10.5
180 11:15 26.00 1,344 82.0 58.3 13.1
210 11:45 26.00 1,258 89.8 59.7 11.9
240 12:15 26.00 1,081 86.0 62.1 12.1
270 12:45 26.00 1,024 86.6 60.2 11.3
300 13:15 26.00 850 82.1 56.6 10.0
330 13:45 26.00 1,057 81.4 62.2 10.5
360 14:15 26.00 1,045 79.9 64.9 6.8
390 14:45 26.00 1,157 86.6 56.7 7.3
420 15:15 26.00 1,019 81.6 56.5 8.5
450 15:45 26.00 1,061 79.3 63.2 5.1
480 16:15 24.00 1,059 76.6 57.8 4.5
Total Fluids Recovered (in gallons) :945
Total Product Recovered (in gallons) :0
AGGRESSIVE FLUID VAPOR RECOVERY EVENT DATA SHEET (Cont'd.)
Site Name :H & S Trading
Incident Number :10151
Well Name:MW-1, MW-19 Inner Dia. of Well (inches):2
Start Time :08:15 Date :5/5/2018
End Time :16:15
Note: Record water levels in Vacuum Well at start and end of Test. Record Water Levels in a few
Observation Wells periodically (hourly during event) and at end of event.
Test Conducted By (AFVR Contractor):Greenwood Applied Services, LLC
Test Supervised By (Consultant):Geological Resources, Inc.
Parameters AFVR Well 1 AFVR Well 2 Obs. Well 1 Obs. Well 2 Obs. Well 3
Well Name MW-1 MW-19 MW-2 MW-3 MW-6
Diameter (in.)2 2 2 2 2
Distance from 0
AFVR Well (ft)
Depth to Water Measurements (in feet)
Frequency Time Vacuum Well 1 Vacuum Well 2 Obs Well 1 Obs. Well 2 Obs. Well 3
(min)(ft.)(ft.)(ft.)(ft.)(ft.)
0 (Before Start)8:15 22.85 21.45 21.84 24.79 21.10
60 9:15 21.86 24.90 20.05
120 10:15 21.89 24.96 20.01
180 11:15 22.34 25.40 20.57
240 12:15 22.59 25.92 21.01
300 13:15 22.70 25.95 21.30
360 14:15 22.99 26.37 21.82
420 15:15 22.55 26.66 20.55
480 16:15 22.11 26.94 20.00
End of Event 16:15 23.34 23.55
43/50 50/28 75/90

APPENDIX B
Disposal Manifest

APPENDIX C
Laboratory Report – Ground Water Samples

07/12/18
Technical Report for
GRI (Geological Resources Inc.)
H&S Trading; 211 Tunis Rd, Tunis, NC
10151/2632
SGS Job Number: FA54012
Sampling Date: 05/04/18
Report to:
GRI
[e-mail]
[e-mail]; [e-mail]; [e-mail]
ATTN: William Regenthall
Total number of pages in report:
Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AK, AR, IA, KY, MA, MS, ND, NH, NV, OK, OR, UT, WA, WV
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone]
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Caitlin Brice, M.S.
General Manager
Orlando, FL 07/12/18
Reissue #1
e-Hardcopy 2.0
Automated Report
18
SGS is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
Review standard terms at: http://www.sgs.com/en/terms-and-conditions
The results set forth herein are provided by SGS North America Inc.
Please share your ideas about
how we can serve you better at:
[e-mail]
1 of 18
FA54012
Florida  4405 Vineland Road  Suite C-15  Orlando, FL 32811  tel: [phone]  fax: [phone]

July 12, 2018

Mr. William Regenthal
GRI
3502 Hayes Rd
Monroe, NC 28110

RE: SGS North America Inc. - Orlando job FA54012 Reissue

Dear Mr. Regenthal,

The final report for job number FA54012 has been edited to reflect requested corrections.
These edits have been incorporated into the revised report.

The sample ID has been revised.

SGS North America Inc. - Orlando apologies for any inconvenience this may have caused.
Please feel free to contact us if we can be of further assistance.

Sincerely,

SGS North America Inc. - Orlando

2 of 18
FA54012
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................4
Section 2: Summary of Hits ....................................................................................................5
Section 3: Sample Results ........................................................................................................6
3.1: FA54012-1: MW-19 ......................................................................................................7
Section 4: Misc. Forms ............................................................................................................8
4.1: Chain of Custody ...........................................................................................................9
Section 5: MS Volatiles - QC Data Summaries .....................................................................11
5.1: Method Blank Summary ................................................................................................12
5.2: Blank Spike Summary ...................................................................................................14
5.3: Matrix Spike Summary ..................................................................................................16
5.4: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................17
5.5: Duplicate Summary .......................................................................................................18 123453 of 18
FA54012
SGS North America Inc.
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA54012
H&S Trading; 211 Tunis Rd, Tunis, NC
Project No: 10151/2632
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA54012-1 05/04/18 08:00 WB 05/05/18 AQ Ground Water MW-19
4 of 18
FA540121
Summary of Hits Page 1 of 1
Job Number:FA54012
Account:GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Collected:05/04/18
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA54012-1 MW-19
Benzene 3.9 0.50 0.13 ug/l SM 6200B
Di-Isopropyl Ether 5.2 0.50 0.13 ug/l SM 6200B
Ethylbenzene 18.9 0.50 0.13 ug/l SM 6200B
Methyl Tert Butyl Ether 185 2.5 0.63 ug/l SM 6200B
Naphthalene 95.7 2.5 0.63 ug/l SM 6200B
Xylene (total)31.3 1.5 0.25 ug/l SM 6200B
5 of 18
FA540122
SGS North America Inc.
Sample Results
Report of Analysis
Orlando, FL
Section 3
6 of 18
FA540123
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:MW-19
Lab Sample ID:FA54012-1 Date Sampled:05/04/18
Matrix:AQ - Ground Water Date Received:05/05/18
Method:SM 6200B Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0213520.D 1 05/09/18 20:34 TD n/a n/a VA2388
Run #2 A0213581.D 5 05/11/18 19:06 TD n/a n/a VA2390
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
Purgeable Aromatics, Full List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 3.9 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether 5.2 0.50 0.13 ug/l
100-41-4 Ethylbenzene 18.9 0.50 0.13 ug/l
1634-04-4 Methyl Tert Butyl Ether 185 a 2.5 0.63 ug/l
91-20-3 Naphthalene 95.7 a 2.5 0.63 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)31.3 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 104%103%70-130%
17060-07-0 1,2-Dichloroethane-D4 101%98%70-130%
2037-26-5 Toluene-D8 95%96%70-130%
460-00-4 4-Bromofluorobenzene 101%111%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
7 of 18
FA5401233.1
SGS North America Inc.
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Orlando, FL
Section 4
8 of 18
FA540124
FA54012: Chain of Custody
Page 1 of 2
9 of 18
FA5401244.1
Job Number:FA54012 Client:GRI
Date / Time Received:5/5/2018 9:45:00 AM Delivery Method:FED EX
Project:2632
Airbill #'s:1015907080610003281100801301168859
Cooler Information
1. Custody Seals Present
2. Custody Seals Intact
4. Cooler temp verification
3. Temp criteria achieved
5. Cooler media
IR Gun
Ice (Bag)
Trip Blank Information
1. Trip Blank present / cooler
2. Trip Blank listed on COC
2. Samples preserved properly
Sample Information
1. Sample labels present on bottles
5. Sample recvd within HT
4. Condition of sample
3. Sufficient volume/containers recvd for analysis:
Intact
Comments
SM001Rev. Date 05/24/17
SGS Sample Receipt Summary
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
Cooler 1: (3.6);
Cooler 1: (4.0);
3. Type Of TB Received
W or S N/A
6. Dates/Times/IDs on COC match Sample Label
7. VOCs have headspace
8. Bottles received for unspecified tests
9. Compositing instructions clear
10. Voa Soil Kits/Jars received past 48hrs?
11. % Solids Jar received?
Misc. Information
25-Gram 5-GramNumber of Encores:Number of 5035 Field Kits:Number of Lab Filtered Metals:
Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify)
Y or N N/A
Y or N
Therm ID:IR 1; Therm CF:0.4; # of Coolers:1
Y or N N/A
12. Residual Chlorine Present?
Residual Chlorine Test Strip Lot #:
Technician:Reviewer:SHAYLAP SP Date:5/5/2018Date:5/5/2018 9:45:00 AM
FA54012: Chain of Custody
Page 2 of 2
10 of 18
FA5401244.1
SGS North America Inc.
MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 5
11 of 18
FA540125
Method Blank Summary Page 1 of 1
Job Number:FA54012
Account:GRINCC GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2388-MB A0213497.D 1 05/09/18 TD n/a n/a VA2388
The QC reported here applies to the following samples:Method: SM 6200B
FA54012-1
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 101%70-130%
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
12 of 18
FA5401255.1.1
Method Blank Summary Page 1 of 1
Job Number:FA54012
Account:GRINCC GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2390-MB A0213567.D 1 05/11/18 TD n/a n/a VA2390
The QC reported here applies to the following samples:Method: SM 6200B
FA54012-1
CAS No.Compound Result RL MDL Units Q
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 93%70-130%
17060-07-0 1,2-Dichloroethane-D4 82%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 96%70-130%
13 of 18
FA5401255.1.2
Blank Spike Summary Page 1 of 1
Job Number:FA54012
Account:GRINCC GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2388-BS a A0213495.D 1 05/09/18 TD n/a n/a VA2388
The QC reported here applies to the following samples:Method: SM 6200B
FA54012-1
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 10.6 106 70-130
108-90-7 Chlorobenzene 10 10.6 106 70-130
95-50-1 1,2-Dichlorobenzene 10 11.1 111 70-130
541-73-1 1,3-Dichlorobenzene 10 11.3 113 70-130
106-46-7 1,4-Dichlorobenzene 10 10.7 107 70-130
108-20-3 Di-Isopropyl Ether 10 10.5 105 70-130
100-41-4 Ethylbenzene 10 11.0 110 70-130
108-88-3 Toluene 10 10.8 108 70-130
1330-20-7 Xylene (total)30 32.8 109 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
(a) No NSD available for this run.
* = Outside of Control Limits.
14 of 18
FA5401255.2.1
Blank Spike Summary Page 1 of 1
Job Number:FA54012
Account:GRINCC GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2390-BS A0213565.D 1 05/11/18 TD n/a n/a VA2390
The QC reported here applies to the following samples:Method: SM 6200B
FA54012-1
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
1634-04-4 Methyl Tert Butyl Ether 10 11.0 110 70-130
91-20-3 Naphthalene 10 12.2 122 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 93%70-130%
17060-07-0 1,2-Dichloroethane-D4 82%70-130%
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
* = Outside of Control Limits.
15 of 18
FA5401255.2.2
Matrix Spike Summary Page 1 of 1
Job Number:FA54012
Account:GRINCC GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA53869-6MS A0213522.D 1 05/09/18 TD n/a n/a VA2388
FA53869-6 A0213504.D 1 05/09/18 TD n/a n/a VA2388
The QC reported here applies to the following samples:Method: SM 6200B
FA54012-1
FA53869-6 Spike MS MS
CAS No.Compound ug/l Q ug/l ug/l %Limits
71-43-2 Benzene ND 10 10.5 105 70-130
108-90-7 Chlorobenzene ND 10 10.4 104 70-130
95-50-1 1,2-Dichlorobenzene ND 10 11.0 110 70-130
541-73-1 1,3-Dichlorobenzene ND 10 11.1 111 70-130
106-46-7 1,4-Dichlorobenzene ND 10 10.5 105 70-130
108-20-3 Di-Isopropyl Ether ND 10 9.1 91 70-130
100-41-4 Ethylbenzene ND 10 10.9 109 70-130
108-88-3 Toluene ND 10 10.6 106 70-130
1330-20-7 Xylene (total)ND 30 32.5 108 70-130
CAS No.Surrogate Recoveries MS FA53869-6 Limits
1868-53-7 Dibromofluoromethane 94%99%70-130%
17060-07-0 1,2-Dichloroethane-D4 83%92%70-130%
2037-26-5 Toluene-D8 101%101%70-130%
460-00-4 4-Bromofluorobenzene 96%97%70-130%
* = Outside of Control Limits.
16 of 18
FA5401255.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1
Job Number:FA54012
Account:GRINCC GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA53998-10MS A0213583.D 1 05/11/18 TD n/a n/a VA2390
FA53998-10MSD A0213584.D 1 05/11/18 TD n/a n/a VA2390
FA53998-10 A0213570.D 1 05/11/18 TD n/a n/a VA2390
The QC reported here applies to the following samples:Method: SM 6200B
FA54012-1
FA53998-10 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
1634-04-4 Methyl Tert Butyl Ether ND 10 12.0 120 10 12.0 120 0 70-130/20
91-20-3 Naphthalene ND 10 13.5 135*10 11.2 112 19 70-130/20
CAS No.Surrogate Recoveries MS MSD FA53998-10 Limits
1868-53-7 Dibromofluoromethane 95%94%96%70-130%
17060-07-0 1,2-Dichloroethane-D4 83%82%86%70-130%
2037-26-5 Toluene-D8 100%101%94%70-130%
460-00-4 4-Bromofluorobenzene 96%97%95%70-130%
* = Outside of Control Limits.
17 of 18
FA5401255.4.1
Duplicate Summary Page 1 of 1
Job Number:FA54012
Account:GRINCC GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA54012-1DUP A0213521.D 1 05/09/18 TD n/a n/a VA2388
FA54012-1 A0213520.D 1 05/09/18 TD n/a n/a VA2388
The QC reported here applies to the following samples:Method: SM 6200B
FA54012-1
FA54012-1 DUP
CAS No.Compound ug/l Q ug/l Q RPD Limits
71-43-2 Benzene 3.9 3.9 0 20
108-90-7 Chlorobenzene ND ND nc 20
95-50-1 1,2-Dichlorobenzene ND ND nc 20
541-73-1 1,3-Dichlorobenzene ND ND nc 20
106-46-7 1,4-Dichlorobenzene ND ND nc 20
108-20-3 Di-Isopropyl Ether 5.2 4.8 8 20
100-41-4 Ethylbenzene 18.9 18.5 2 20
108-88-3 Toluene ND ND nc 20
1330-20-7 Xylene (total)31.3 30.2 4 20
CAS No.Surrogate Recoveries DUP FA54012-1 Limits
1868-53-7 Dibromofluoromethane 99%104%70-130%
17060-07-0 1,2-Dichloroethane-D4 89%101%70-130%
2037-26-5 Toluene-D8 97%95%70-130%
460-00-4 4-Bromofluorobenzene 100%101%70-130%
* = Outside of Control Limits.
18 of 18
FA5401255.5.1
06/29/18
Technical Report for
GRI (Geological Resources Inc.)
H&S Trading; 211 Tunis Rd, Tunis, NC
10151/2632
SGS Job Number: FA54988
Sampling Date: 06/11/18
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
[e-mail]; [e-mail];
[e-mail]; [e-mail]
ATTN: William Regenthall
Total number of pages in report:
Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AK, AR, IA, KY, MA, MS, ND, NH, NV, OK, OR, UT, WA, WV
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone]
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Caitlin Brice, M.S.
General Manager
Orlando, FL 06/29/18
e-Hardcopy 2.0
Automated Report
31
SGS is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
Review standard terms at: http://www.sgs.com/en/terms-and-conditions
The results set forth herein are provided by SGS North America Inc.
Please share your ideas about
how we can serve you better at:
[e-mail]
1 of 31
FA54988
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................6
3.1: FA54988-1: MW-2 ........................................................................................................7
3.2: FA54988-2: MW-3 ........................................................................................................9
3.3: FA54988-3: MW-5 ........................................................................................................11
3.4: FA54988-4: MW-6 ........................................................................................................13
3.5: FA54988-5: MW-19 ......................................................................................................15
3.6: FA54988-6: RW-2 .........................................................................................................17
Section 4: Misc. Forms ............................................................................................................19
4.1: Chain of Custody ...........................................................................................................20
Section 5: MS Volatiles - QC Data Summaries .....................................................................22
5.1: Method Blank Summary ................................................................................................23
5.2: Blank Spike Summary ...................................................................................................26
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................29 123452 of 31
FA54988
SGS North America Inc.
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA54988
H&S Trading; 211 Tunis Rd, Tunis, NC
Project No: 10151/2632
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA54988-1 06/11/18 12:45 WB 06/13/18 AQ Ground Water MW-2
FA54988-2 06/11/18 13:15 WB 06/13/18 AQ Ground Water MW-3
FA54988-3 06/11/18 13:05 WB 06/13/18 AQ Ground Water MW-5
FA54988-4 06/11/18 12:55 WB 06/13/18 AQ Ground Water MW-6
FA54988-5 06/11/18 13:30 WB 06/13/18 AQ Ground Water MW-19
FA54988-6 06/11/18 13:45 WB 06/13/18 AQ Ground Water RW-2
3 of 31
FA549881
Summary of Hits Page 1 of 2
Job Number:FA54988
Account:GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Collected:06/11/18
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA54988-1 MW-2
Benzene a 3.5 0.50 0.13 ug/l SM 6200B
n-Butylbenzene a 1.4 0.50 0.13 ug/l SM 6200B
sec-Butylbenzene a 3.6 0.50 0.13 ug/l SM 6200B
tert-Butylbenzene a 1.1 0.50 0.13 ug/l SM 6200B
Chloroethane a 0.20 J 0.50 0.20 ug/l SM 6200B
Di-Isopropyl Ether a 2.2 0.50 0.13 ug/l SM 6200B
Ethylbenzene a 3.2 0.50 0.13 ug/l SM 6200B
Isopropylbenzene a 4.1 0.50 0.13 ug/l SM 6200B
p-Isopropyltoluene a 0.25 J 0.50 0.13 ug/l SM 6200B
Methyl Tert Butyl Ether a 8.4 0.50 0.13 ug/l SM 6200B
Naphthalene a 19.5 0.50 0.13 ug/l SM 6200B
n-Propylbenzene a 4.4 0.50 0.13 ug/l SM 6200B
1,2,4-Trimethylbenzene a 16.4 0.50 0.13 ug/l SM 6200B
1,3,5-Trimethylbenzene a 0.61 0.50 0.13 ug/l SM 6200B
m,p-Xylene a 0.42 J 1.0 0.13 ug/l SM 6200B
o-Xylene a 0.14 J 0.50 0.13 ug/l SM 6200B
FA54988-2 MW-3
Di-Isopropyl Ether a 1.3 0.50 0.13 ug/l SM 6200B
Methyl Tert Butyl Ether a 22.2 0.50 0.13 ug/l SM 6200B
FA54988-3 MW-5
Benzene 9.3 2.5 0.63 ug/l SM 6200B
n-Butylbenzene 2.4 J 2.5 0.63 ug/l SM 6200B
sec-Butylbenzene 4.0 2.5 0.63 ug/l SM 6200B
Chloroethane 2.6 2.5 1.0 ug/l SM 6200B
Di-Isopropyl Ether 17.0 2.5 0.63 ug/l SM 6200B
Ethylbenzene 46.9 2.5 0.63 ug/l SM 6200B
Isopropylbenzene 33.2 2.5 0.63 ug/l SM 6200B
p-Isopropyltoluene 0.78 J 2.5 0.63 ug/l SM 6200B
Methyl Chloride 4.5 2.5 1.0 ug/l SM 6200B
Methyl Tert Butyl Ether 143 2.5 0.63 ug/l SM 6200B
Naphthalene 42.2 2.5 0.63 ug/l SM 6200B
n-Propylbenzene 47.8 2.5 0.63 ug/l SM 6200B
1,2,4-Trimethylbenzene 231 2.5 0.63 ug/l SM 6200B
1,3,5-Trimethylbenzene 33.6 2.5 0.63 ug/l SM 6200B
m,p-Xylene 89.7 5.0 0.63 ug/l SM 6200B
Xylene (total)89.7 7.5 1.3 ug/l SM 6200B
4 of 31
FA549882
Summary of Hits Page 2 of 2
Job Number:FA54988
Account:GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Collected:06/11/18
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA54988-4 MW-6
Benzene 1.6 0.50 0.13 ug/l SM 6200B
n-Butylbenzene 0.34 J 0.50 0.13 ug/l SM 6200B
sec-Butylbenzene 1.6 0.50 0.13 ug/l SM 6200B
tert-Butylbenzene 0.54 0.50 0.13 ug/l SM 6200B
Di-Isopropyl Ether 3.5 0.50 0.13 ug/l SM 6200B
Isopropylbenzene 0.28 J 0.50 0.13 ug/l SM 6200B
p-Isopropyltoluene 0.23 J 0.50 0.13 ug/l SM 6200B
Methyl Tert Butyl Ether 14.3 0.50 0.13 ug/l SM 6200B
FA54988-5 MW-19
Benzene a 1.4 J 2.5 0.63 ug/l SM 6200B
n-Butylbenzene a 30.4 2.5 0.63 ug/l SM 6200B
sec-Butylbenzene a 24.8 2.5 0.63 ug/l SM 6200B
Di-Isopropyl Ether a 3.5 2.5 0.63 ug/l SM 6200B
Ethylbenzene a 4.2 2.5 0.63 ug/l SM 6200B
Isopropylbenzene a 7.3 2.5 0.63 ug/l SM 6200B
p-Isopropyltoluene a 23.5 2.5 0.63 ug/l SM 6200B
Methyl Tert Butyl Ether a 209 2.5 0.63 ug/l SM 6200B
Naphthalene a 129 2.5 0.63 ug/l SM 6200B
n-Propylbenzene a 14.6 2.5 0.63 ug/l SM 6200B
1,1,2,2-Tetrachloroethane a 46.8 2.5 0.63 ug/l SM 6200B
1,2,4-Trimethylbenzene a 93.5 2.5 0.63 ug/l SM 6200B
1,3,5-Trimethylbenzene a 19.7 2.5 0.63 ug/l SM 6200B
m,p-Xylene a 6.6 5.0 0.63 ug/l SM 6200B
o-Xylene a 1.5 J 2.5 0.63 ug/l SM 6200B
Xylene (total) a 8.1 7.5 1.3 ug/l SM 6200B
FA54988-6 RW-2
Benzene a 0.96 J 1.0 0.25 ug/l SM 6200B
Di-Isopropyl Ether a 7.4 1.0 0.25 ug/l SM 6200B
Methyl Chloride a 0.79 J 1.0 0.40 ug/l SM 6200B
Methyl Tert Butyl Ether a 76.3 1.0 0.25 ug/l SM 6200B
Naphthalene a 1.4 1.0 0.25 ug/l SM 6200B
(a) Sample vial(s) contained significant headspace; reported results are considered minimum values.
5 of 31
FA549882
SGS North America Inc.
Sample Results
Report of Analysis
Orlando, FL
Section 3
6 of 31
FA549883
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-2
Lab Sample ID:FA54988-1 Date Sampled:06/11/18
Matrix:AQ - Ground Water Date Received:06/13/18
Method:SM 6200B Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a E058875.D 1 06/25/18 13:12 TD n/a n/a VE1985
Run #2 b A0214158.D 20 06/19/18 13:56 TD n/a n/a VA2411
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 3.5 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene 1.4 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene 3.6 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene 1.1 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane 0.20 0.50 0.20 ug/l J
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
7 of 31
FA5498833.1
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-2
Lab Sample ID:FA54988-1 Date Sampled:06/11/18
Matrix:AQ - Ground Water Date Received:06/13/18
Method:SM 6200B Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 2.2 0.50 0.13 ug/l
100-41-4 Ethylbenzene 3.2 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene 4.1 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene 0.25 0.50 0.13 ug/l J
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 8.4 0.50 0.13 ug/l
91-20-3 Naphthalene 19.5 0.50 0.13 ug/l
103-65-1 n-Propylbenzene 4.4 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene c ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 16.4 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene 0.61 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 0.42 1.0 0.13 ug/l J
95-47-6 o-Xylene 0.14 0.50 0.13 ug/l J
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%93%70-130%
17060-07-0 1,2-Dichloroethane-D4 101%86%70-130%
2037-26-5 Toluene-D8 95%100%70-130%
460-00-4 4-Bromofluorobenzene 98%99%70-130%
(a) Sample vial(s) contained significant headspace; reported results are considered minimum values.
(b) Confirmation run. IS failure.
(c) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
8 of 31
FA5498833.1
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-3
Lab Sample ID:FA54988-2 Date Sampled:06/11/18
Matrix:AQ - Ground Water Date Received:06/13/18
Method:SM 6200B Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a E058879.D 1 06/25/18 14:45 TD n/a n/a VE1985
Run #2 b A0214159.D 20 06/19/18 14:19 TD n/a n/a VA2411
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
9 of 31
FA5498833.2
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-3
Lab Sample ID:FA54988-2 Date Sampled:06/11/18
Matrix:AQ - Ground Water Date Received:06/13/18
Method:SM 6200B Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 1.3 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 22.2 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene c ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 97%93%70-130%
17060-07-0 1,2-Dichloroethane-D4 97%83%70-130%
2037-26-5 Toluene-D8 103%99%70-130%
460-00-4 4-Bromofluorobenzene 99%101%70-130%
(a) Sample vial(s) contained significant headspace; reported results are considered minimum values.
(b) Confirmation run. IS failure.
(c) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 31
FA5498833.2
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-5
Lab Sample ID:FA54988-3 Date Sampled:06/11/18
Matrix:AQ - Ground Water Date Received:06/13/18
Method:SM 6200B Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E058872.D 5 06/25/18 12:05 TD n/a n/a VE1985
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 9.3 2.5 0.63 ug/l
108-86-1 Bromobenzene ND 2.5 0.63 ug/l
74-97-5 Bromochloromethane ND 2.5 0.63 ug/l
75-27-4 Bromodichloromethane ND 2.5 0.63 ug/l
75-25-2 Bromoform ND 2.5 0.63 ug/l
104-51-8 n-Butylbenzene 2.4 2.5 0.63 ug/l J
135-98-8 sec-Butylbenzene 4.0 2.5 0.63 ug/l
98-06-6 tert-Butylbenzene ND 2.5 0.63 ug/l
56-23-5 Carbon Tetrachloride ND 2.5 0.63 ug/l
108-90-7 Chlorobenzene ND 2.5 0.63 ug/l
75-00-3 Chloroethane 2.6 2.5 1.0 ug/l
67-66-3 Chloroform ND 2.5 0.63 ug/l
95-49-8 o-Chlorotoluene ND 2.5 0.63 ug/l
106-43-4 p-Chlorotoluene ND 2.5 0.63 ug/l
124-48-1 Dibromochloromethane ND 2.5 0.63 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 2.5 1.2 ug/l
106-93-4 1,2-Dibromoethane ND 2.5 0.63 ug/l
75-71-8 Dichlorodifluoromethane ND 2.5 1.0 ug/l
95-50-1 1,2-Dichlorobenzene ND 2.5 0.63 ug/l
541-73-1 1,3-Dichlorobenzene ND 2.5 0.63 ug/l
106-46-7 1,4-Dichlorobenzene ND 2.5 0.63 ug/l
75-34-3 1,1-Dichloroethane ND 2.5 0.63 ug/l
107-06-2 1,2-Dichloroethane ND 2.5 0.63 ug/l
75-35-4 1,1-Dichloroethylene ND 2.5 0.63 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 2.5 0.63 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 2.5 0.63 ug/l
78-87-5 1,2-Dichloropropane ND 2.5 0.63 ug/l
142-28-9 1,3-Dichloropropane ND 2.5 0.63 ug/l
594-20-7 2,2-Dichloropropane ND 2.5 0.63 ug/l
563-58-6 1,1-Dichloropropene ND 2.5 0.63 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 2.5 0.63 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 2.5 0.63 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 31
FA5498833.3
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-5
Lab Sample ID:FA54988-3 Date Sampled:06/11/18
Matrix:AQ - Ground Water Date Received:06/13/18
Method:SM 6200B Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 17.0 2.5 0.63 ug/l
100-41-4 Ethylbenzene 46.9 2.5 0.63 ug/l
87-68-3 Hexachlorobutadiene ND 2.5 0.63 ug/l
98-82-8 Isopropylbenzene 33.2 2.5 0.63 ug/l
99-87-6 p-Isopropyltoluene 0.78 2.5 0.63 ug/l J
74-83-9 Methyl Bromide ND 2.5 1.0 ug/l
74-87-3 Methyl Chloride 4.5 2.5 1.0 ug/l
74-95-3 Methylene Bromide ND 2.5 0.63 ug/l
75-09-2 Methylene Chloride ND 10 5.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 143 2.5 0.63 ug/l
91-20-3 Naphthalene 42.2 2.5 0.63 ug/l
103-65-1 n-Propylbenzene 47.8 2.5 0.63 ug/l
100-42-5 Styrene ND 2.5 0.63 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 2.5 0.63 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 2.5 0.63 ug/l
127-18-4 Tetrachloroethylene ND 2.5 0.63 ug/l
108-88-3 Toluene ND 2.5 0.63 ug/l
87-61-6 1,2,3-Trichlorobenzene a ND 2.5 0.63 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 2.5 0.63 ug/l
71-55-6 1,1,1-Trichloroethane ND 2.5 0.63 ug/l
79-00-5 1,1,2-Trichloroethane ND 2.5 0.63 ug/l
79-01-6 Trichloroethylene ND 2.5 0.63 ug/l
75-69-4 Trichlorofluoromethane ND 2.5 1.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.5 0.63 ug/l
95-63-6 1,2,4-Trimethylbenzene 231 2.5 0.63 ug/l
108-67-8 1,3,5-Trimethylbenzene 33.6 2.5 0.63 ug/l
75-01-4 Vinyl Chloride ND 2.5 0.63 ug/l
m,p-Xylene 89.7 5.0 0.63 ug/l
95-47-6 o-Xylene ND 2.5 0.63 ug/l
1330-20-7 Xylene (total)89.7 7.5 1.3 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 104%70-130%
17060-07-0 1,2-Dichloroethane-D4 107%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 96%70-130%
(a) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 31
FA5498833.3
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-6
Lab Sample ID:FA54988-4 Date Sampled:06/11/18
Matrix:AQ - Ground Water Date Received:06/13/18
Method:SM 6200B Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E058881.D 1 06/25/18 15:31 TD n/a n/a VE1985
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 1.6 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene 0.34 0.50 0.13 ug/l J
135-98-8 sec-Butylbenzene 1.6 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene 0.54 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
13 of 31
FA5498833.4
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-6
Lab Sample ID:FA54988-4 Date Sampled:06/11/18
Matrix:AQ - Ground Water Date Received:06/13/18
Method:SM 6200B Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 3.5 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene 0.28 0.50 0.13 ug/l J
99-87-6 p-Isopropyltoluene 0.23 0.50 0.13 ug/l J
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 14.3 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene a ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 98%70-130%
17060-07-0 1,2-Dichloroethane-D4 99%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
(a) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
14 of 31
FA5498833.4
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-19
Lab Sample ID:FA54988-5 Date Sampled:06/11/18
Matrix:AQ - Ground Water Date Received:06/13/18
Method:SM 6200B Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a E058876.D 5 06/25/18 13:33 TD n/a n/a VE1985
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 1.4 2.5 0.63 ug/l J
108-86-1 Bromobenzene ND 2.5 0.63 ug/l
74-97-5 Bromochloromethane ND 2.5 0.63 ug/l
75-27-4 Bromodichloromethane ND 2.5 0.63 ug/l
75-25-2 Bromoform ND 2.5 0.63 ug/l
104-51-8 n-Butylbenzene 30.4 2.5 0.63 ug/l
135-98-8 sec-Butylbenzene 24.8 2.5 0.63 ug/l
98-06-6 tert-Butylbenzene ND 2.5 0.63 ug/l
56-23-5 Carbon Tetrachloride ND 2.5 0.63 ug/l
108-90-7 Chlorobenzene ND 2.5 0.63 ug/l
75-00-3 Chloroethane ND 2.5 1.0 ug/l
67-66-3 Chloroform ND 2.5 0.63 ug/l
95-49-8 o-Chlorotoluene ND 2.5 0.63 ug/l
106-43-4 p-Chlorotoluene ND 2.5 0.63 ug/l
124-48-1 Dibromochloromethane ND 2.5 0.63 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 2.5 1.2 ug/l
106-93-4 1,2-Dibromoethane ND 2.5 0.63 ug/l
75-71-8 Dichlorodifluoromethane ND 2.5 1.0 ug/l
95-50-1 1,2-Dichlorobenzene ND 2.5 0.63 ug/l
541-73-1 1,3-Dichlorobenzene ND 2.5 0.63 ug/l
106-46-7 1,4-Dichlorobenzene ND 2.5 0.63 ug/l
75-34-3 1,1-Dichloroethane ND 2.5 0.63 ug/l
107-06-2 1,2-Dichloroethane ND 2.5 0.63 ug/l
75-35-4 1,1-Dichloroethylene ND 2.5 0.63 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 2.5 0.63 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 2.5 0.63 ug/l
78-87-5 1,2-Dichloropropane ND 2.5 0.63 ug/l
142-28-9 1,3-Dichloropropane ND 2.5 0.63 ug/l
594-20-7 2,2-Dichloropropane ND 2.5 0.63 ug/l
563-58-6 1,1-Dichloropropene ND 2.5 0.63 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 2.5 0.63 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 2.5 0.63 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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FA5498833.5
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-19
Lab Sample ID:FA54988-5 Date Sampled:06/11/18
Matrix:AQ - Ground Water Date Received:06/13/18
Method:SM 6200B Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 3.5 2.5 0.63 ug/l
100-41-4 Ethylbenzene 4.2 2.5 0.63 ug/l
87-68-3 Hexachlorobutadiene ND 2.5 0.63 ug/l
98-82-8 Isopropylbenzene 7.3 2.5 0.63 ug/l
99-87-6 p-Isopropyltoluene 23.5 2.5 0.63 ug/l
74-83-9 Methyl Bromide ND 2.5 1.0 ug/l
74-87-3 Methyl Chloride ND 2.5 1.0 ug/l
74-95-3 Methylene Bromide ND 2.5 0.63 ug/l
75-09-2 Methylene Chloride ND 10 5.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 209 2.5 0.63 ug/l
91-20-3 Naphthalene 129 2.5 0.63 ug/l
103-65-1 n-Propylbenzene 14.6 2.5 0.63 ug/l
100-42-5 Styrene ND 2.5 0.63 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 2.5 0.63 ug/l
79-34-5 1,1,2,2-Tetrachloroethane 46.8 2.5 0.63 ug/l
127-18-4 Tetrachloroethylene ND 2.5 0.63 ug/l
108-88-3 Toluene ND 2.5 0.63 ug/l
87-61-6 1,2,3-Trichlorobenzene b ND 2.5 0.63 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 2.5 0.63 ug/l
71-55-6 1,1,1-Trichloroethane ND 2.5 0.63 ug/l
79-00-5 1,1,2-Trichloroethane ND 2.5 0.63 ug/l
79-01-6 Trichloroethylene ND 2.5 0.63 ug/l
75-69-4 Trichlorofluoromethane ND 2.5 1.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.5 0.63 ug/l
95-63-6 1,2,4-Trimethylbenzene 93.5 2.5 0.63 ug/l
108-67-8 1,3,5-Trimethylbenzene 19.7 2.5 0.63 ug/l
75-01-4 Vinyl Chloride ND 2.5 0.63 ug/l
m,p-Xylene 6.6 5.0 0.63 ug/l
95-47-6 o-Xylene 1.5 2.5 0.63 ug/l J
1330-20-7 Xylene (total)8.1 7.5 1.3 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 110%70-130%
(a) Sample vial(s) contained significant headspace; reported results are considered minimum values.
(b) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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FA5498833.5
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:RW-2
Lab Sample ID:FA54988-6 Date Sampled:06/11/18
Matrix:AQ - Ground Water Date Received:06/13/18
Method:SM 6200B Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a E058874.D 2 06/25/18 12:51 TD n/a n/a VE1985
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 0.96 1.0 0.25 ug/l J
108-86-1 Bromobenzene ND 1.0 0.25 ug/l
74-97-5 Bromochloromethane ND 1.0 0.25 ug/l
75-27-4 Bromodichloromethane ND 1.0 0.25 ug/l
75-25-2 Bromoform ND 1.0 0.25 ug/l
104-51-8 n-Butylbenzene ND 1.0 0.25 ug/l
135-98-8 sec-Butylbenzene ND 1.0 0.25 ug/l
98-06-6 tert-Butylbenzene ND 1.0 0.25 ug/l
56-23-5 Carbon Tetrachloride ND 1.0 0.25 ug/l
108-90-7 Chlorobenzene ND 1.0 0.25 ug/l
75-00-3 Chloroethane ND 1.0 0.40 ug/l
67-66-3 Chloroform ND 1.0 0.25 ug/l
95-49-8 o-Chlorotoluene ND 1.0 0.25 ug/l
106-43-4 p-Chlorotoluene ND 1.0 0.25 ug/l
124-48-1 Dibromochloromethane ND 1.0 0.25 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 1.0 0.49 ug/l
106-93-4 1,2-Dibromoethane ND 1.0 0.25 ug/l
75-71-8 Dichlorodifluoromethane ND 1.0 0.40 ug/l
95-50-1 1,2-Dichlorobenzene ND 1.0 0.25 ug/l
541-73-1 1,3-Dichlorobenzene ND 1.0 0.25 ug/l
106-46-7 1,4-Dichlorobenzene ND 1.0 0.25 ug/l
75-34-3 1,1-Dichloroethane ND 1.0 0.25 ug/l
107-06-2 1,2-Dichloroethane ND 1.0 0.25 ug/l
75-35-4 1,1-Dichloroethylene ND 1.0 0.25 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 1.0 0.25 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 1.0 0.25 ug/l
78-87-5 1,2-Dichloropropane ND 1.0 0.25 ug/l
142-28-9 1,3-Dichloropropane ND 1.0 0.25 ug/l
594-20-7 2,2-Dichloropropane ND 1.0 0.25 ug/l
563-58-6 1,1-Dichloropropene ND 1.0 0.25 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 1.0 0.25 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 1.0 0.25 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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FA5498833.6
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Report of Analysis Page 2 of 2
Client Sample ID:RW-2
Lab Sample ID:FA54988-6 Date Sampled:06/11/18
Matrix:AQ - Ground Water Date Received:06/13/18
Method:SM 6200B Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 7.4 1.0 0.25 ug/l
100-41-4 Ethylbenzene ND 1.0 0.25 ug/l
87-68-3 Hexachlorobutadiene ND 1.0 0.25 ug/l
98-82-8 Isopropylbenzene ND 1.0 0.25 ug/l
99-87-6 p-Isopropyltoluene ND 1.0 0.25 ug/l
74-83-9 Methyl Bromide ND 1.0 0.40 ug/l
74-87-3 Methyl Chloride 0.79 1.0 0.40 ug/l J
74-95-3 Methylene Bromide ND 1.0 0.25 ug/l
75-09-2 Methylene Chloride ND 4.0 2.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 76.3 1.0 0.25 ug/l
91-20-3 Naphthalene 1.4 1.0 0.25 ug/l
103-65-1 n-Propylbenzene ND 1.0 0.25 ug/l
100-42-5 Styrene ND 1.0 0.25 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 1.0 0.25 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 0.25 ug/l
127-18-4 Tetrachloroethylene ND 1.0 0.25 ug/l
108-88-3 Toluene ND 1.0 0.25 ug/l
87-61-6 1,2,3-Trichlorobenzene b ND 1.0 0.25 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 1.0 0.25 ug/l
71-55-6 1,1,1-Trichloroethane ND 1.0 0.25 ug/l
79-00-5 1,1,2-Trichloroethane ND 1.0 0.25 ug/l
79-01-6 Trichloroethylene ND 1.0 0.25 ug/l
75-69-4 Trichlorofluoromethane ND 1.0 0.40 ug/l
96-18-4 1,2,3-Trichloropropane ND 1.0 0.25 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 1.0 0.25 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 1.0 0.25 ug/l
75-01-4 Vinyl Chloride ND 1.0 0.25 ug/l
m,p-Xylene ND 2.0 0.25 ug/l
95-47-6 o-Xylene ND 1.0 0.25 ug/l
1330-20-7 Xylene (total)ND 3.0 0.50 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 97%70-130%
(a) Sample vial(s) contained significant headspace; reported results are considered minimum values.
(b) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
18 of 31
FA5498833.6
SGS North America Inc.
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Orlando, FL
Section 4
19 of 31
FA549884
FA54988: Chain of Custody
Page 1 of 2
20 of 31
FA5498844.1
Job Number:FA54988 Client:GRI
Date / Time Received:6/13/2018 9:00:00 AM Delivery Method:FED EX
Project:H+S TROODING
Airbill #'s:
Cooler Information
1. Custody Seals Present
2. Custody Seals Intact
4. Cooler temp verification
3. Temp criteria achieved
5. Cooler media
IR Gun
Ice (Bag)
Trip Blank Information
1. Trip Blank present / cooler
2. Trip Blank listed on COC
2. Samples preserved properly
Sample Information
1. Sample labels present on bottles
5. Sample recvd within HT
4. Condition of sample
3. Sufficient volume/containers recvd for analysis:
Intact
Comments
SM001Rev. Date 05/24/17
SGS Sample Receipt Summary
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
Cooler 1: (1.6);
Cooler 1: (2.0);
3. Type Of TB Received
W or S N/A
6. Dates/Times/IDs on COC match Sample Label
7. VOCs have headspace
8. Bottles received for unspecified tests
9. Compositing instructions clear
10. Voa Soil Kits/Jars received past 48hrs?
11. % Solids Jar received?
Misc. Information
25-Gram 5-GramNumber of Encores:Number of 5035 Field Kits:Number of Lab Filtered Metals:
Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify)
Y or N N/A
Y or N
Therm ID:IR 1; Therm CF:0.4; # of Coolers:1
Y or N N/A
12. Residual Chlorine Present?
Residual Chlorine Test Strip Lot #:
Technician:Reviewer:HEATHERW BR Date:6/13/2018Date:6/13/2018 9:00:00 AM
FA54988: Chain of Custody
Page 2 of 2
21 of 31
FA5498844.1
SGS North America Inc.
MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 5
22 of 31
FA549885
Method Blank Summary Page 1 of 1
Job Number:FA54988
Account:GRINCC GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2411-MB A0214156.D 1 06/19/18 TD n/a n/a VA2411
The QC reported here applies to the following samples:Method: SM 6200B
FA54988-1, FA54988-2
CAS No.Compound Result RL MDL Units Q
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 96%70-130%
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
23 of 31
FA5498855.1.1
Method Blank Summary Page 1 of 2
Job Number:FA54988
Account:GRINCC GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1985-MB E058867.D 1 06/25/18 TD n/a n/a VE1985
The QC reported here applies to the following samples:Method: SM 6200B
FA54988-1, FA54988-2, FA54988-3, FA54988-4, FA54988-5, FA54988-6
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
24 of 31
FA5498855.1.2
Method Blank Summary Page 2 of 2
Job Number:FA54988
Account:GRINCC GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1985-MB E058867.D 1 06/25/18 TD n/a n/a VE1985
The QC reported here applies to the following samples:Method: SM 6200B
FA54988-1, FA54988-2, FA54988-3, FA54988-4, FA54988-5, FA54988-6
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 104%70-130%
17060-07-0 1,2-Dichloroethane-D4 105%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 97%70-130%
25 of 31
FA5498855.1.2
Blank Spike Summary Page 1 of 1
Job Number:FA54988
Account:GRINCC GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2411-BS A0214154.D 1 06/19/18 TD n/a n/a VA2411
The QC reported here applies to the following samples:Method: SM 6200B
FA54988-1, FA54988-2
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 97%70-130%
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
* = Outside of Control Limits.
26 of 31
FA5498855.2.1
Blank Spike Summary Page 1 of 2
Job Number:FA54988
Account:GRINCC GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1985-BS E058865.D 1 06/25/18 TD n/a n/a VE1985
The QC reported here applies to the following samples:Method: SM 6200B
FA54988-1, FA54988-2, FA54988-3, FA54988-4, FA54988-5, FA54988-6
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 9.4 94 70-130
108-86-1 Bromobenzene 10 9.0 90 70-130
74-97-5 Bromochloromethane 10 9.6 96 70-130
75-27-4 Bromodichloromethane 10 9.6 96 70-130
75-25-2 Bromoform 10 9.2 92 70-130
104-51-8 n-Butylbenzene 10 9.7 97 70-130
135-98-8 sec-Butylbenzene 10 9.5 95 70-130
98-06-6 tert-Butylbenzene 10 9.0 90 70-130
56-23-5 Carbon Tetrachloride 10 9.7 97 70-130
108-90-7 Chlorobenzene 10 9.3 93 70-130
75-00-3 Chloroethane 10 11.9 119 60-140
67-66-3 Chloroform 10 9.2 92 70-130
95-49-8 o-Chlorotoluene 10 9.2 92 70-130
106-43-4 p-Chlorotoluene 10 9.2 92 70-130
124-48-1 Dibromochloromethane 10 9.7 97 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 8.8 88 70-130
106-93-4 1,2-Dibromoethane 10 8.8 88 70-130
75-71-8 Dichlorodifluoromethane 10 9.9 99 60-140
95-50-1 1,2-Dichlorobenzene 10 9.2 92 70-130
541-73-1 1,3-Dichlorobenzene 10 9.5 95 70-130
106-46-7 1,4-Dichlorobenzene 10 9.1 91 70-130
75-34-3 1,1-Dichloroethane 10 9.8 98 70-130
107-06-2 1,2-Dichloroethane 10 9.4 94 70-130
75-35-4 1,1-Dichloroethylene 10 10.1 101 70-130
156-59-2 cis-1,2-Dichloroethylene 10 9.3 93 70-130
156-60-5 trans-1,2-Dichloroethylene 10 9.6 96 70-130
78-87-5 1,2-Dichloropropane 10 9.5 95 70-130
142-28-9 1,3-Dichloropropane 10 8.6 86 70-130
594-20-7 2,2-Dichloropropane 10 10.2 102 70-130
563-58-6 1,1-Dichloropropene 10 9.4 94 70-130
10061-01-5 cis-1,3-Dichloropropene 10 9.3 93 70-130
10061-02-6 trans-1,3-Dichloropropene 10 9.4 94 70-130
108-20-3 Di-Isopropyl Ether 10 9.7 97 70-130
100-41-4 Ethylbenzene 10 9.4 94 70-130
87-68-3 Hexachlorobutadiene 10 10.3 103 70-130
98-82-8 Isopropylbenzene 10 9.9 99 70-130
* = Outside of Control Limits.
27 of 31
FA5498855.2.2
Blank Spike Summary Page 2 of 2
Job Number:FA54988
Account:GRINCC GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1985-BS E058865.D 1 06/25/18 TD n/a n/a VE1985
The QC reported here applies to the following samples:Method: SM 6200B
FA54988-1, FA54988-2, FA54988-3, FA54988-4, FA54988-5, FA54988-6
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 9.5 95 70-130
74-83-9 Methyl Bromide 10 8.7 87 60-140
74-87-3 Methyl Chloride 10 11.2 112 60-140
74-95-3 Methylene Bromide 10 9.1 91 70-130
75-09-2 Methylene Chloride 10 9.9 99 70-130
1634-04-4 Methyl Tert Butyl Ether 10 9.5 95 70-130
91-20-3 Naphthalene 10 10.7 107 70-130
103-65-1 n-Propylbenzene 10 9.2 92 70-130
100-42-5 Styrene 10 9.3 93 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 9.8 98 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 9.3 93 70-130
127-18-4 Tetrachloroethylene 10 9.5 95 70-130
108-88-3 Toluene 10 9.4 94 70-130
87-61-6 1,2,3-Trichlorobenzene 10 13.0 130 70-130
120-82-1 1,2,4-Trichlorobenzene 10 10.4 104 70-130
71-55-6 1,1,1-Trichloroethane 10 9.5 95 70-130
79-00-5 1,1,2-Trichloroethane 10 9.3 93 70-130
79-01-6 Trichloroethylene 10 9.0 90 70-130
75-69-4 Trichlorofluoromethane 10 10.1 101 60-140
96-18-4 1,2,3-Trichloropropane 10 8.7 87 70-130
95-63-6 1,2,4-Trimethylbenzene 10 9.1 91 70-130
108-67-8 1,3,5-Trimethylbenzene 10 9.3 93 70-130
75-01-4 Vinyl Chloride 10 9.3 93 60-140
m,p-Xylene 20 18.8 94 70-130
95-47-6 o-Xylene 10 9.2 92 70-130
1330-20-7 Xylene (total)30 28.0 93 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 95%70-130%
* = Outside of Control Limits.
28 of 31
FA5498855.2.2
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1
Job Number:FA54988
Account:GRINCC GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA55045-4MS A0214179.D 50 06/19/18 TD n/a n/a VA2411
FA55045-4MSD A0214180.D 50 06/19/18 TD n/a n/a VA2411
FA55045-4 a A0214170.D 50 06/19/18 TD n/a n/a VA2411
The QC reported here applies to the following samples:Method: SM 6200B
FA54988-1, FA54988-2
FA55045-4 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
CAS No.Surrogate Recoveries MS MSD FA55045-4 Limits
1868-53-7 Dibromofluoromethane 84%84%87%70-130%
17060-07-0 1,2-Dichloroethane-D4 71%70%72%70-130%
2037-26-5 Toluene-D8 104%104%102%70-130%
460-00-4 4-Bromofluorobenzene 101%102%99%70-130%
(a) Confirmation run.
* = Outside of Control Limits.
29 of 31
FA5498855.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA54988
Account:GRINCC GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA55243-11MS E058884.D 1 06/25/18 TD n/a n/a VE1985
FA55243-11MSD E058885.D 1 06/25/18 TD n/a n/a VE1985
FA55243-11 E058878.D 1 06/25/18 TD n/a n/a VE1985
The QC reported here applies to the following samples:Method: SM 6200B
FA54988-1, FA54988-2, FA54988-3, FA54988-4, FA54988-5, FA54988-6
FA55243-11 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene ND 10 9.2 92 10 8.4 84 9 70-130/20
108-86-1 Bromobenzene ND 10 8.7 87 10 8.4 84 4 70-130/20
74-97-5 Bromochloromethane ND 10 9.2 92 10 8.7 87 6 70-130/20
75-27-4 Bromodichloromethane ND 10 8.6 86 10 7.9 79 8 70-130/20
75-25-2 Bromoform ND 10 7.4 74 10 6.8 68*8 70-130/20
104-51-8 n-Butylbenzene ND 10 9.6 96 10 8.7 87 10 70-130/20
135-98-8 sec-Butylbenzene ND 10 9.5 95 10 8.5 85 11 70-130/20
98-06-6 tert-Butylbenzene ND 10 8.9 89 10 8.0 80 11 70-130/20
56-23-5 Carbon Tetrachloride ND 10 8.6 86 10 7.4 74 15 70-130/20
108-90-7 Chlorobenzene ND 10 9.1 91 10 8.5 85 7 70-130/20
75-00-3 Chloroethane ND 10 12.8 128 10 11.1 111 14 60-140/20
67-66-3 Chloroform ND 10 8.7 87 10 7.9 79 10 70-130/20
95-49-8 o-Chlorotoluene ND 10 9.2 92 10 8.4 84 9 70-130/20
106-43-4 p-Chlorotoluene ND 10 9.0 90 10 8.4 84 7 70-130/20
124-48-1 Dibromochloromethane ND 10 8.2 82 10 7.8 78 5 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 10 8.6 86 10 8.4 84 2 70-130/20
106-93-4 1,2-Dibromoethane ND 10 8.4 84 10 8.3 83 1 70-130/20
75-71-8 Dichlorodifluoromethane ND 10 8.7 87 10 7.6 76 13 60-140/20
95-50-1 1,2-Dichlorobenzene ND 10 9.0 90 10 8.6 86 5 70-130/20
541-73-1 1,3-Dichlorobenzene ND 10 9.3 93 10 8.6 86 8 70-130/20
106-46-7 1,4-Dichlorobenzene ND 10 9.0 90 10 8.4 84 7 70-130/20
75-34-3 1,1-Dichloroethane ND 10 9.6 96 10 8.6 86 11 70-130/20
107-06-2 1,2-Dichloroethane ND 10 8.5 85 10 8.3 83 2 70-130/20
75-35-4 1,1-Dichloroethylene ND 10 9.5 95 10 8.2 82 15 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 10 9.1 91 10 8.2 82 10 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 10 9.3 93 10 8.3 83 11 70-130/20
78-87-5 1,2-Dichloropropane ND 10 9.2 92 10 8.7 87 6 70-130/20
142-28-9 1,3-Dichloropropane ND 10 8.3 83 10 8.3 83 0 70-130/20
594-20-7 2,2-Dichloropropane ND 10 9.5 95 10 8.2 82 15 70-130/20
563-58-6 1,1-Dichloropropene ND 10 9.3 93 10 8.1 81 14 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 10 8.0 80 10 7.1 71 12 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 10 8.5 85 10 7.7 77 10 70-130/20
108-20-3 Di-Isopropyl Ether ND 10 9.6 96 10 9.0 90 6 70-130/20
100-41-4 Ethylbenzene ND 10 9.2 92 10 8.4 84 9 70-130/20
87-68-3 Hexachlorobutadiene ND 10 10 100 10 8.8 88 13 70-130/20
98-82-8 Isopropylbenzene ND 10 9.8 98 10 8.8 88 11 70-130/20
* = Outside of Control Limits.
30 of 31
FA5498855.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA54988
Account:GRINCC GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA55243-11MS E058884.D 1 06/25/18 TD n/a n/a VE1985
FA55243-11MSD E058885.D 1 06/25/18 TD n/a n/a VE1985
FA55243-11 E058878.D 1 06/25/18 TD n/a n/a VE1985
The QC reported here applies to the following samples:Method: SM 6200B
FA54988-1, FA54988-2, FA54988-3, FA54988-4, FA54988-5, FA54988-6
FA55243-11 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 10 9.5 95 10 8.5 85 11 70-130/20
74-83-9 Methyl Bromide ND 10 9.8 98 10 8.7 87 12 60-140/20
74-87-3 Methyl Chloride ND 10 9.8 98 10 8.0 80 20 60-140/20
74-95-3 Methylene Bromide ND 10 8.5 85 10 8.3 83 2 70-130/20
75-09-2 Methylene Chloride ND 10 9.4 94 10 8.7 87 8 70-130/20
1634-04-4 Methyl Tert Butyl Ether 1.8 10 11.4 96 10 11.0 92 4 70-130/20
91-20-3 Naphthalene ND 10 11.0 110 10 10.6 106 4 70-130/20
103-65-1 n-Propylbenzene ND 10 9.1 91 10 8.2 82 10 70-130/20
100-42-5 Styrene ND 10 8.9 89 10 8.3 83 7 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 10 9.3 93 10 8.5 85 9 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 10 9.1 91 10 9.1 91 0 70-130/20
127-18-4 Tetrachloroethylene ND 10 9.2 92 10 8.2 82 11 70-130/20
108-88-3 Toluene ND 10 9.3 93 10 8.6 86 8 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 10 12.9 129 10 12.2 122 6 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 10 10.5 105 10 9.8 98 7 70-130/20
71-55-6 1,1,1-Trichloroethane ND 10 8.7 87 10 7.6 76 13 70-130/20
79-00-5 1,1,2-Trichloroethane ND 10 8.9 89 10 8.9 89 0 70-130/20
79-01-6 Trichloroethylene ND 10 8.5 85 10 7.6 76 11 70-130/20
75-69-4 Trichlorofluoromethane ND 10 9.3 93 10 8.0 80 15 60-140/20
96-18-4 1,2,3-Trichloropropane ND 10 8.3 83 10 8.3 83 0 70-130/20
95-63-6 1,2,4-Trimethylbenzene ND 10 9.0 90 10 8.3 83 8 70-130/20
108-67-8 1,3,5-Trimethylbenzene ND 10 9.4 94 10 8.5 85 10 70-130/20
75-01-4 Vinyl Chloride ND 10 9.7 97 10 8.3 83 16 60-140/20
m,p-Xylene ND 20 18.6 93 20 17.0 85 9 70-130/20
95-47-6 o-Xylene ND 10 9.1 91 10 8.3 83 9 70-130/20
1330-20-7 Xylene (total)ND 30 27.7 92 30 25.3 84 9 70-130/20
CAS No.Surrogate Recoveries MS MSD FA55243-11 Limits
1868-53-7 Dibromofluoromethane 98%97%98%70-130%
17060-07-0 1,2-Dichloroethane-D4 99%99%97%70-130%
2037-26-5 Toluene-D8 102%102%100%70-130%
460-00-4 4-Bromofluorobenzene 97%97%96%70-130%
* = Outside of Control Limits.
31 of 31
FA5498855.3.2