WA-722_10151_CA_MRP_20220411

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
April 12, 2022

Ms. Carrie Stone
North Carolina Department of
Environmental Quality
Washington Regional Office
943 Washington Square Mall
Washington, North Carolina 27889

Re: Ground Water Monitoring Report
February 2022
H&S Trading
211 Tunis Road
Tunis, Hertford County
North Carolina
Facility ID Number: 0-00-0000009678
Incident Numbers: 10151
GRI Project Number: 2632

Dear Ms. Stone,

Please find enclosed the referenced report for the above mentioned site.
If you have any questions, please contact Ethan Rogerson at 704-845-4010.

Sincerely,
Geological Resources, Inc.

Leslie Maxtone-Graham
Administrative Assistant

Enclosure

Cc: Ms. Bea Harrison, North East Oil Company, Inc., file

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
Engineering Certification: C-2727 • Geology Certification: C-127
Ground Water and Soil Sampling Report
February 2022
H&S Trading
211 Tunis Road
Tunis, Hertford County
North Carolina
Facility ID Number: 0-00-0000009678
Incident Number: 10151
GRI Project Number: 2632

Prepared for:

North East Oil Company, Inc.
Post Office Box 1386
Ahoskie, North Carolina 28352

April 11, 2022

Ethan Rogerson, G.I.T.
Project Manager
William Regenthal, P.G.
Report Editor

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water and Soil Sampling Report
Prepared on: April 11, 2022 H&S Trading
Project Manager: Ethan Rogerson, G.I.T. GRI Project No. 2632
i
EXECUTIVE SUMMARY
H&S Trading is located at 211 Tunis Road in Tunis, Hertford County, North Carolina. The site is currently
owned by Canal Cove Center and was formerly operated as a petroleum retail facility. The former UST
system was owned by North East Oil Company, Inc. One 2,000-gallon gasoline, one 1,000-gallon gasoline,
and one 550-gallon kerosene USTs were removed from the site in October 1992, at which time petroleum
contamination was discovered. The adjoining properties are residential. According to the information
determined during receptor survey activities, thirty-eight water supply wells were identified within a
1,500-foot radius of the site. Three water supply wells that are not currently in use (WSW-1, WSW-34, and
WSW-35) are located within a 250-foot radius of the site. Additionally, seven potable wells (WSW-11,
WSW-12, WSW-25, WSW-26, WSW-29, WSW-30 and WSW-31) were located within 1,000 feet of the site.
Public water is available to the site and surrounding properties within a 1,500-foot radius of the site.

A CAP that proposed the operation of a pump and treat CAS was completed on July 12, 1995 and approved
by NCDEQ on March 4, 1996. According to available information, the CAS operated at the site from April
1997 to September 2005, and again from April 2009 to April 2010.

On February 28, 2022, two temporary monitoring wells (TMW-1 and TMW-2) were installed to total
depths of 30 feet BGS, each. Soil samples were collected from TMW-1 and TMW-2 at intervals of 2 feet
until reaching a total depth of 30 feet BGS, each. A total of 30 soil samples were collected and analyzed
for TPH-GRO and TPH-DRO using UVF technology. Concentrations of GRO and/or DRO reported in the soil
samples collected from TMW-1-10, TMW-1-12, TMW-1-14, TMW-1-16, TMW-1-18, TMW-1-20, TMW-1-
22, TMW-1-30, TMW-2-8, TMW-2-12, TMW-2-14, TMW-2-20 and TMW-2-22 exceeded the RALs.

Soil samples were collected from TMW-1 and TMW-2 at 22 and 30 feet BGS, each, and were submitted
for laboratory analyses of grain size. Soil at the site is consistent with silty, clayey sand and sandy, silty
clay.

On February 28 and March 3, 2022, eight monitoring wells, two recovery wells, two temporary wells and
two water supply wells were gauged, purged and/or sampled. Concentrations of benzene, MTBE, n-
butylbenzene, sec-butylbenzene, n-propylbenzene, isopropylbenzene, p-isopropyltoluene and/or 1,2,4-
trimethylbenzene that exceeded the MACs were reported in the ground water samples collected from
MW-1, MW-5, MW-19, TMW-1 and TMW-2. All of the reported contaminant concentrations were less
than GCLs. Free product was not observed.

Contaminant mass at the site has decreased by 68% since the August 2015 baseline assessment.

Based on this information, the site risk classification should remain classified as high risk. A feasibility
study should be conducted to discuss the most cost-effective remedial strategy for the site moving
forward, including; excavation of contaminated soil, injection of remedial solutions into the water table
and refurbishing/reconnecting to the pump and treatment system. Comparisons of the costs of proposed

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water and Soil Sampling Report
Prepared on: April 11, 2022 H&S Trading
Project Manager: Ethan Rogerson, G.I.T. GRI Project No. 2632
ii
remedial strategies should be included in the Feasibility Study Report. In the interim, quarterly ground
water monitoring, including the collection of natural attenuation parameters. The quarterly data
collection be conducted in order to gather sufficient would be needed to accurately complete a Fate and
Transport model. The next ground water sampling event is tentatively scheduled for June 2022.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water and Soil Sampling Report
Prepared on: April 11, 2022 H&S Trading
Project Manager: Ethan Rogerson, G.I.T. GRI Project No. 2632
iii
SITE INFORMATION
1. Site Identification
 H&S Trading (Facility ID 0-00-0000009678)
 Incident Number 10151 – High Risk (H195R)
 Location of Source Area: 211 Tunis Road
Tunis, NC 28677
Hertford County
36.380111°N, 76.890417°W (Topographical Map)
2. Information about Contacts Associated with the Leaking UST System

UST Owner
North East Oil Company, Inc.
Post Office Box 1386
Ahoskie, NC 28352
[e-mail]
252-862-0236

UST Operator
North East Oil Company, Inc.
Post Office Box 1386
Ahoskie, NC 28352
[e-mail]
252-862-0236

Property Owner
Canal Cove Center
17383 Kennedy Drive
N. Redington Beach, FL 33708
Email unknown
Phone unknown

Property Occupant
H & S Trading
211 Tunis Road
Tunis, NC 28314
Email unknown
Phone unknown

Consultant/Contractor
Geological Resources, Inc.
3502 Hayes Road
Monroe, NC 28110
[e-mail]
704-845-4010

Analytical Laboratory
SGS- North America, Inc.
4405 Vineland Road, Suite C-15
Orlando, FL 32811
State Certification No. 573
407-425-6700
3. Information about Release
 Release was discovered in October 1992.
 An unknown amount of product was released from the leaking UST System
 Two 2,000-gallon gasoline, one 1,000-gallon gasoline, and one 550-gallon kerosene USTs were
removed from the site in October 1992.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water and Soil Sampling Report
Prepared on: April 11, 2022 H&S Trading
Project Manager: Ethan Rogerson, G.I.T. GRI Project No. 2632
iv
ACRONYMS
ACM: Asbestos Containing Materials
AFVR: Aggressive Fluid-Vapor Recovery
ARR: Acknowledgement of Report Receipt
AS: Air Sparging
AST: Aboveground Storage Tank
ASTM: American Society for Testing and
Materials
BGS: Below Ground Surface
CAP: Corrective Action Plan
CFR: Code of Federal Regulations
CSA: Comprehensive Site Assessment
DPE: Dual Phase Extraction
DRO: Total Petroleum Hydrocarbons Diesel
Range Organics
DWM: Division of Waste Management
DWR: Department of Water Resources
EPA: Environmental Protection Agency
EPH: Extractible Petroleum Hydrocarbons
ESA: Environmental Site Assessment
GCL: Gross Contamination Level
GRI: Geological Resources, Inc.
GRO: Total Petroleum Hydrocarbons
Gasoline Range Organics
LSA: Limited Site Assessment
MAC: Maximum Allowable Concentration as
specified in T15A NCAC 2L.0202
MADEP: Massachusetts Department of
Environmental Protection
MCC: Maximum Contaminant Concentrations
MMPE: Mobile Multi-Phase Extraction
NAPL: Non-Aqueous Phase Liquid, “Free
Product”
NCDEQ: North Carolina Department of
Environmental Quality
NCDOT: North Carolina Department of
Transportation
NFA: Notice of No Further Action
NORR: Notice of Regulatory Requirements
NOV: Notice of Violation
NPDES: National Pollutant Discharge
Elimination System
NRP: Notice of Residual Petroleum
O&M: Operation and Maintenance
PAHs: Polynuclear Aromatic Hydrocarbons
PCA: Pre-Construction Assessment
RAL: Regulatory Action Level
SCLs: Soil Cleanup Level
SPCC: Spill Prevention Control and
Countermeasures
SVE: Soil Vapor Extraction
SVOCs: Semi-Volatile Organic Compounds
SWPPP: Stormwater Pollution Prevention Plan
TCLP: Toxicity Characteristic Leaching
Procedure (EPA Method SW-846 1311)
TOC: Top of Casing
TPH: Total Petroleum Hydrocarbons
USGS: United States Geological Survey
UST: Underground Storage Tank
UVF: Ultraviolet Fluorescence
VOCs: Volatile Organic Compounds
VPH: Volatile Petroleum Hydrocarbons

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water and Soil Sampling Report
Prepared on: April 11, 2022 H&S Trading
Project Manager: Ethan Rogerson, G.I.T. GRI Project No. 2632
TABLE OF CONTENTS
EXECUTIVE SUMMARY ....................................................................................................................... i
SITE INFORMATION ........................................................................................................................... iii
ACRONYMS ....................................................................................................................................... iv
1.0 SITE HISTORY AND CHARACTERIZATION ...................................................................................1
2.0 MONITORING WELL INSTALLATION ..........................................................................................2
3.0 SOIL QUALITY INFORMATION ..................................................................................................2
4.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL
ASSESSMENT INFORMATION ...................................................................................................3
5.0 FREE PRODUCT REMOVAL ........................................................................................................5
6.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS ..................................5
7.0 CONCLUSIONS .........................................................................................................................5
8.0 LIMITATIONS ...........................................................................................................................6
9.0 STATEMENTS AND CERTIFICATION ...........................................................................................6

FIGURES
Figure 1: Site Location Map
Figure 2: Site Vicinity Map
Figure 3: Site Map
Figure 4: Soil Quality Map
Figure 5: Water Table Surface Map
Figure 6: Ground Water Quality Map
Figure 7: Estimated Contaminant Mass Area Map

TABLES
Table 1: UST Owner and Operator Information
Table 2: UST System Information
Table 3: Adjacent Property Owner Information
Table 4: Water Supply Well Information
Table 5: Well Construction and Gauging Information
Table 6: Summary of Soil Sample Analytical Results
Table 7: Summary of Ground Water Sample Analytical Results
Table 7A: Summary of Natural Attenuation Parameter Results

APPENDICES
Appendix A: State Correspondence
Appendix B: Subsurface Logs
Appendix C: UVF Report – Soil Samples
Appendix D: Laboratory Report – Ground Water
Appendix E: Contaminant Mass Calculations

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water and Soil Sampling Report
Prepared on: April 11, 2022 H&S Trading
Project Manager: Ethan Rogerson, G.I.T. GRI Project No. 2632
1
1.0 SITE HISTORY AND CHARACTERIZATION
GRI presents the results of the February 2022 soil and ground water sampling event at the H&S Trading
site; located at 211 Tunis Road in Tunis, Hertford County, North Carolina (Figure 1). These activities were
conducted in accordance with GRI Proposal No. 21-661, which was submitted to NCDEQ on November 1,
2021, and was approved as Task Authorization No. 10151-64 on February 14, 2022. State correspondence
is included as Appendix A.

The site is currently owned by Canal Cove Center and formerly operated as a petroleum retail facility. One
2,000-gallon gasoline, one 1,000-gallon gasoline, and one 550-gallon kerosene USTs were removed from
the site in October 1992 at which time petroleum contamination was discovered. UST owner/operator
information and UST system information are included as Tables 1 and 2, respectively. The Registered
Tank Report is shown below:

The site and surrounding area consist of residential properties. The site contains one building and is
primarily capped with gravel and grass. The overall topography at the site is relatively flat. No surface
water bodies were identified within a 500-foot radius of the site. Nineteen Type II monitoring wells (MW-
1 through MW-6 and MW-8 through MW-20), one Type III monitoring well (MWD-7) and eight recovery
wells (RW-1, RW-1A, RW-2 through RW- 6 and RW-8) were installed at the site during previous ground
water assessment activities.

On August 12, 2015, GRI personnel conducted a receptor survey at the site. Thirty-eight water supply
wells were identified within a 1,500-foot radius of the site. Three water supply wells that are not currently
in use (WSW-1, WSW-34, and WSW-35) are located within a 250-foot radius of the site. Additionally,
seven potable wells (WSW-11, WSW-12, WSW-25, WSW-26, WSW-29, WSW-30, and WSW-31) were
located within 1,000 feet of the site. Municipal water is available to the site and surrounding properties.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water and Soil Sampling Report
Prepared on: April 11, 2022 H&S Trading
Project Manager: Ethan Rogerson, G.I.T. GRI Project No. 2632
2
Adjacent property owner information is presented in Table 3. Water supply well information is presented
in Table 4. A Site Vicinity Map showing the locations of water supply wells and adjacent properties has
been included as Figure 2. A Site Map showing the locations of the monitoring wells and the structures
on-site has been included as Figure 3.

A CAP that proposed the operation of a pump and treat corrective action system CAS was completed on
July 12, 1995, and approved by NCDEQ on March 4, 1996. According to available information, the CAS
operated at the site from April 1997 to September 2005, and again from April 2009 to April 2010.
2.0 MONITORING WELL INSTALLATION
On February 28, 2022, two temporary monitoring wells (TMW-1 and TMW-2) were installed in the area
of MW-1 and MW-19. Well construction and gauging information for the permanent wells on-site is
presented in Table 5. The locations of the temporary wells are shown on Figure 3. Copies of the
subsurface logs have been included in Appendix B.
3.0 SOIL QUALITY INFORMATION
On February 28, 2022, soil samples were collected from TMW-1 and TMW-2 in intervals of 2 feet until
reaching a total depth of 30 feet BGS, each. A total of 30 soil samples were collected and analyzed for
TPH-GRO and TPH-DRO using UVF technology. Concentrations of GRO and/or DRO reported in the soil
samples collected from TMW-1-10, TMW-1-12, TMW-1-14, TMW-1-16, TMW-1-18, TMW-1-20, TMW-1-
22, TMW-1-30, TMW-2-8, TMW-2-12, TMW-2-14, TMW-2-20 and TMW-2-22 exceeded the RALs.

Additionally, during the installation of the temporary monitoring wells, grain size samples were collected
at 22 feet and 30 feet BGS from both TMW-1 and TMW-2. Soil at the site is consistent with silty, clayey
sand and sandy, silty clay.

A summary of the analytical results for soil samples collected in February 2022 is presented in Table 6. A
Soil Quality Map based on the February 2022 data is included as Figure 4. A complete report of laboratory
analyses of the soil samples collected in February 2022 has been included as Appendix C. A summary of
the current soil analytical data is shown below: Sample ID Sample Depth (ft-BGS) Gasoline-Range TPH Diesel-Range TPH Soil to Water MCC (mg/kg) 50 100
TMW-1-2 2 <10 1.6
TMW-1-4 4 <10 1.28
TMW-1-6 6 <10 1.28
TMW-1-8 8 <10 1.32
TMW-1-10 10 172 42
TMW-1-12 12 179 45
TMW-1-14 14 182 48
TMW-1-16 16 188 58
TMW-1-18 18 243 73
TMW-1-20 20 129 57

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water and Soil Sampling Report
Prepared on: April 11, 2022 H&S Trading
Project Manager: Ethan Rogerson, G.I.T. GRI Project No. 2632
3 Sample ID Sample Depth (ft-BGS) Gasoline-Range TPH Diesel-Range TPH TMW-1-22 22 155 39
TMW-1-24 24 45 5
TMW-1-26 26 2 2
TMW-1-28 28 19.4 8.72
TMW-1-30 30 137 43
TMW-2-2 2 <2 1.68
TMW-2-4 4 <2 1.56
TMW-2-6 6 4.36 2.72
TMW-2-8 8 1,091 381
TMW-2-10 10 25 4
TMW-2-12 12 405 125
TMW-2-14 14 364 123
TMW-2-16 16 42 4
TMW-2-18 18 46 15
TMW-2-20 20 316 128
TMW-2-22 22 93 37
TMW-2-24 24 36 13
TMW-2-26 26 15.4 9.08
TMW-2-28 28 6.32 4.88
TMW-2-30 30 3.44 3.08
TMW-1-28 DUP 16 <2 2
4.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL
ASSESSMENT INFORMATION
On February 28 and March 3, 2022, eight monitoring wells, two recovery wells, two temporary wells and
two water supply wells were gauged, purged and/or sampled. No free product was observed. Depths to
ground water in the Type II monitoring wells ranged from 18.11 feet to 26.52 feet below the tops of well
casings. Ground water elevations in the Type II monitoring wells ranged from 74.71 feet to 78.71 feet.
Ground water flow was generally convergent in the area of MW-2 with a horizontal gradient of
approximately 0.06 feet per foot. Well construction and gauging information is presented in Table 5. A
Water Table Surface Map based on the Type II monitoring wells is included as Figure 5. A summary of
the current ground water gauging data is shown below:
Well ID
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(feet)
Free
Product
Thickness
(ft.)
Ground
Water
Elevation
(ft.)
MW-1 20-30 30 100.00 23.25 --- 76.75
MW-2 20 - 30 30 99.17 24.46 --- 74.71
MW-3 20 - 30 30 102.13 25.41 --- 76.72
MW-5 20 - 30 30 94.76 18.11 --- 76.65
MW-6 20 - 30 30 98.52 20.60 --- 77.92
MW-12 25 - 35 35 103.09 26.52 --- 76.57
MW-14 25 - 35 35 97.36 20.71 --- 76.65
MW-19 20 - 30 30 100.37 21.66 --- 78.71
RW-1A NA NA NM 22.52 --- NM
RW-2 NA NA NM 22.19 --- NM

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water and Soil Sampling Report
Prepared on: April 11, 2022 H&S Trading
Project Manager: Ethan Rogerson, G.I.T. GRI Project No. 2632
4
Ground water samples collected from the monitoring wells were submitted for laboratory analyses using
EPA Method 6200B. Concentrations of benzene, MTBE, n-butylbenzene, sec-butylbenzene, n-
propylbenzene, isopropylbenzene, p-isopropyltoluene and/or 1,2,4-trimethylbenzene that exceeded the
MACs were reported in the ground water samples collected from MW-1, MW-5, MW-19, TMW-1 and
TMW-2. All of the reported contaminant concentration were less than the GCLs. A summary of the
analytical results for ground water samples collected on February 28 and March 2, 2022, is presented in
Table 7. A summary of natural attenuation parameter results is presented in Table 7A. A Ground Water
Quality Map based on February 28 and March 2, 2022, data is included as Figure 5. A complete report of
laboratory analyses of the ground water samples collected from the monitoring wells during the February
and March 2022 sampling event has been included as Appendix D. A summary of the current ground
water analytical data is shown below:

Contaminant
of Concern  Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene Well
ID
MACs (μg/l) 1 600 600 500 20 6
GCL (μg/l) 5,000 260,000 80,000 50,000 20,000 6,000
MW-1 4.9 J <3.1 524 <6.3 5.2 J 1,610
MW-2 <0.13 <0.13 <0.13 <0.25 5.4 <0.13
MW-3 <0.13 <0.13 <0.13 <0.25 1.0 <0.13
MW-5 1.1 <0.13 1.6 3.2 20.6 1.8
MW-6 <0.13 <0.13 <0.13 <0.25 17.2 0.22 J
MW-12 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13
MW-14 <0.13 <0.13 <0.13 <0.25 <0.13 0.14 J
MW-19 5.7 <0.13 7.3 2.1 330 64.1
RW-1A 0.32 J <0.13 <0.13 <0.25 7.1 2.9
RW-2 0.32 J <0.13 <0.13 <0.25 7.1 2.9
TMW-1 0.61 J <0.31 1.5 13.4 115 29.4
TMW-2 30.6 <3.1 97.5 493 2,650 19.0

The baseline contaminant mass at the site was determined based on the total BTEX, MTBE and
naphthalene concentrations from the August 2015 ground water sampling event as well as the maximum
historical water column height observed in each area. The contaminant plume was divided into four areas
(Areas 1 and 2) based on the benzene concentrations during the August 2015 ground water sampling
event. The contaminant mass has been reduced by 68% since August 2015. Contaminant mass
calculations have been included as Appendix E. A map of the contaminant mass areas has been included
as Figure 6. A chart depicting the overall declining trend in contaminant mass is shown below:

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water and Soil Sampling Report
Prepared on: April 11, 2022 H&S Trading
Project Manager: Ethan Rogerson, G.I.T. GRI Project No. 2632
5

The site is located in the Coastal Plain Physiographic Province of North Carolina. The water table has a
seasonal high depth to water of approximately twenty-one to twenty-nine feet BGS.
5.0 FREE PRODUCT REMOVAL
Free product has not been observed in MW-1 since February 2019.
6.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS
No natural attenuation monitoring plan is currently in place at the site.
7.0 CONCLUSIONS
 On February 28, 2022, two temporary monitoring wells (TMW-1 and TMW-2) were installed to
total depths of 30 feet BGS, each.
 Concentrations of GRO and/or DRO reported in the soil samples collected from TMW-1-10, TMW-
1-12, TMW-1-14, TMW-1-16, TMW-1-18, TMW-1-20, TMW-1-22, TMW-1-30, TMW-2-8, TMW-2-
12, TMW-2-14, TMW-2-20 and TMW-2-22 exceeded the RALs.
 Grain size samples were taken at 22 feet and 30 feet BGS from both TMW-1 and TMW-2. Soil at
the site is consistent with silty, clayey sand and sandy, silty clay.
 Concentrations of benzene, MTBE, n-butylbenzene, sec-butylbenzene, n-propylbenzene,
isopropylbenzene, p-isopropyltoluene and/or 1,2,4-trimethylbenzene that exceeded the MACs
were reported in the ground water samples collected from MW-1, MW-5, MW-19, TMW-1 and
TMW-2. All of the reported contaminant concentrations were less than the GCLs.
 The contaminant mass has been reduced by 68% since August 2015.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water and Soil Sampling Report
Prepared on: April 11, 2022 H&S Trading
Project Manager: Ethan Rogerson, G.I.T. GRI Project No. 2632
6
 Based on this information, the site risk classification should remain classified as high risk. A
feasibility study should be conducted to discuss the most cost-effective remedial strategy for the
site moving forward, including; excavation of contaminated soil, injection of remedial solutions
into the water table and refurbishing/reconnecting to the pump and treatment system.
Comparisons of the costs of proposed remedial strategies should be included in the Feasibility
Study Report. In the interim, quarterly ground water monitoring, including the collection of
natural attenuation parameters. The quarterly data collection be conducted in order to gather
sufficient would be needed to accurately complete a Fate and Transport model. The next ground
water sampling event is tentatively scheduled for June 2022.
8.0 LIMITATIONS
This report has been prepared for the exclusive use of North East Oil Company, Inc. for specific application
to the referenced site in Hertford County, North Carolina. The assessment was conducted based on the
scope of work and level of effort desired by NCDEQ and with resources adequate only for that scope of
work. Our findings have been developed in accordance with generally accepted standards of
environmental practices in the State of North Carolina, available information, and our professional
judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would
be interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data.
9.0 STATEMENTS AND CERTIFICATION
1 Enter the date the monitoring report was due. n/a Will this report be submitted after the
established due date?
YES NO
2 Was any required information from the above template missing from this report? YES NO
IF the answer to question #1 or# 2 is “YES”, please provide additional information in this cell to explain
what was missing and why.
3 If applicable, will any of the proposed attenuation milestones under the schedule approved
in the Corrective Action Plan not be met? (within a reasonable margin of error)
YES NO
IF the answer to question #3 is “NO”, skip to the certification under #8 below.
IF the answer to question #3 is “YES”, please generally describe in this cell the possible reason(s) and
outline proposed remedies. (This should be described in more detail in the report text above.)

N/A
4 Does any known or suspected source zone soil contamination or free product remain
outside of the assessed area that could be inhibiting natural attenuation?
YES NO
5 Has there been an unexpected increase in contaminant mass sufficient to suggest a
potential new release from a separate onsite or offsite source?
YES NO

FIGURES

TABLES
UST ID Number 1 Facility ID Number
Owner or Operator?
Owner/OperatorET One, Inc.04/30/83 - 10/15/92
Address Telephone Number
Post Office Box 1386, Ahoskie, NC 27910 252-862-0236
TABLE 1
UST OWNER/OPERATOR INFORMATION
H&S TRADING (INCIDENT NO. 10151)
0-009678
Name of Owner or Operator Dates of Ownership / Operation
Date: 09/16/19 Facility ID #s: 0-006978
Was Release
Associated
with UST
System?
(Yes / No)
1 Gasoline,
Gas Mix 2,000 04/30/83 Single Wall Steel 64" x 12'Unknown Removed
(10/15/92)Yes
2 Gasoline,
Gas Mix 2,000 04/30/83 Single Wall Steel 64" x 12'Unknown Removed
(10/15/92)Yes
3 Gasoline,
Gas Mix 1,000 04/30/83 Single Wall Steel 64" x 72"Unknown Removed
(10/15/92)Yes
4 Kerosene 550 04/30/83 Single Wall Steel 46" x 74"Unknown Removed
(10/15/92)Yes
Status
of
UST
TABLE 2
UST SYSTEM INFORMATION
H&S TRADING (INCIDENT NO. 10151)
UST
ID
No.
Current
or Most
Recent
Contents
Capacity
(gallons)
Date
Installed
Construction
Details
Tank
Dimensions
Description of
Associated
Product Piping
and
Pumps
Date: 08/20/15 Facility ID # : 0-009678
6926-13-1905 (Site)Canal Cove Center 17383 Kennedy Drive
N. Redington Beach, Florida 33708
6926-14-0160 Leeds, Robert Eugene 1448 NC Highway 11 N
Aulander, North Carolina 27805
6926-13-3662 Francis, B M 203 Chalon Drive
Cary, North Carolina 27511
6926-13-0823 Fenn, David 207 Tunis Road
Winton, North Carolina 27986
6926-14-0013 White, Miriam Phelps 1103 Haledon Road
Chesapeake, Virginia 23320
6926-14-1082 Jinks, Dan 805 Fort Totten Drive
New Bern, North Carolina 28560
6926-14-2633 Anthony E. Stephenson 248 Tuscarora Beach Road
Winton, North Carolina 27986
Note:
• Properties are keyed to Figure 2.
TABLE 3
ADJACENT PROPERTY OWNER INFORMATION
H&S TRADING (INCIDENT NO. 10151)
Tax Pin Number/ Map ID Owner/Occupant Name Address
Well #Parcel #Well Owner Mailing Address Well Location Address
Municipal
Water
(Yes/No)
Potable/
Non Potable
Distance from
source area of
release
(ft.)
WSW-1 6926-14-2142 O'Brien, David Francis 4113 Emberhill Lane
Chesapeake, Virginia 23321
215 Tunis Road
Winton, North Carolina 27986 Yes Non Potable ~170 NE
WSW-2 6926-14-5022 Deason, Marlon Poe, Jr.501 Hampton Place, Apt. 2
Portsmouth, Virginia 23704
218 Tunis Road
Winton, NC 27986 Yes Non Potable ~400 NE
WSW-3 6926-14-6644 Zartman, Debra D.105 Seabreeze Lane
Suffolk, Virginia 23435
107 River Drive
Winton, North Carolina 27986 Yes Non Potable ~840 NE
WSW-4 6926-14-7766 Wallace, David Lee 113 River Drive
Winton, North Carolina 27986
113 River Drive
Winton, North Carolina 27986 Yes Non Potable ~1,020 NE
WSW-5 6926-14-4681 Felton, Norman 230 Tunis Road
Winton, North Carolina 27986
230 Tunis Road
Winton, North Carolina 27986 Yes Non Potable ~710 NE
WSW-6 6926-14-2356 Freeman, Morris Lee Post Office Box 785
Ahoskie, North Carolina 27910
225 Tunis Road
Winton, North Carolina 27986 Yes Non Potable ~550 NE
WSW-7 6926-14-3524 Parks, Robert Williams 3648 Wright Road
Portsmouth, Virginia 23703
227 Tunis Road
Winton, North Carolina 27986 Yes Non Potable ~710 NE
WSW-8 6926-14-5710 O'Brien, David Francis 4113 Emberhill Lane
Chesapeake, Virginia 23321
102 Freeman Drive
Winton, North Carolina 27986 Yes Non Potable ~840 NE
WSW-9 6926-14-2633 Stephenson, Anthony E.248 Tuscarora Beach Road
Winton, North Carolina 27986
111 Tunis Fishery Road
Winton, North Carolina 27986 Yes Non Potable ~1,460 NE
WSW-10 6926-14-7203 Hobbs, Jerry Michael 104 Sea Gull Lane
Winton, North Carolina 27986
104 Sea Gull Lane
Winton, North Carolina 27986 Yes Non Potable ~620 NE
WSW-11 No Potable ~570 E
WSW-12 No Potable ~630 E
WSW-13 6926-15-8150 Dewey, Charles P. and Laurie E.17383 Kennedy Drive
N. Redington Beach, Florida 33708
118 Freeman Drive
Winton, North Carolina 27986 Yes Non Potable ~1,340 NE
WSW-14 6926-02-7816 Lewis, Ethel Marie and Clary, William M.142 Tunis Road
Winton, North Carolina 27986
142 Tunis Road
Winton, North Carolina 27986 Yes Non Potable ~1,160 SW
WSW-15 6926-02-7785 Hawk, Thomas L. and Yoder, Barbara M.106 Church Drive
Winton, North Carolina 27986
106 Church Drive
Winton, North Carolina 27986 Yes Non Potable ~1,280 SW
WSW-16 6926-12-2831 Lewis, Ethel Marie and Clary, William M.142 Tunis Road
Winton, North Carolina 27986
108 Church Drive
Winton, North Carolina 27986 Yes Non Potable ~1,080 S
WSW-17 &
WSW-19 6926-13-3031 Taylor, Alice Carol Castellow 234 Castelow Road
Cofield, North Carolina 27922
106 Church Drive
Winton, North Carolina 27986 Yes Non Potable ~850 S
~1,060 SE
WSW-18 6926-12-0931 Ward, William Preston, Sr.114 Church Drive
Winton, North Carolina 27986
114 Church Drive
Winton, North Carolina 27986 Yes Non Potable ~1,020 S
WSW-20 6926-02-8562 Chambers, Michael 314 Willoughby Road
Ahoskie, North Carolina 27910
138 Tunis Road
Winton, North Carolina 27986 Yes Non Potable ~1,410 SW
WSW-21 6926-02-3672 Manley, Ulysses Dupree 11572 226th Street
Cambria Heights, New York 11411
135 Tunis Road
Winton, North Carolina 27986 Yes Non Potable ~1,460 SW
TABLE 4
WATER SUPPLY WELL INFORMATION
H&S TRADING (INCIDENT NO. 10151)
Date : 08/20/15 Facility ID #: 0-009678
6926-13-8489 Information Not Available Information Not Available Trailer Park - Sandy Drive
Winton, North Carolina 27986
Page 1 of 2
Well #Parcel #Well Owner Mailing Address Well Location Address
Municipal
Water
(Yes/No)
Potable/
Non Potable
Distance from
source area of
release
(ft.)
TABLE 4
WATER SUPPLY WELL INFORMATION
H&S TRADING (INCIDENT NO. 10151)
Date : 08/20/15 Facility ID #: 0-009678
WSW-22 6926-02-4860 Sanders, Darlene Matthews 137 Tunis Road
Winton, North Carolina 27986
137 Tunis Road
Winton, North Carolina 27986 Yes Non Potable ~1,310 SW
WSW-23 6926-03-5072 Ballistic Enterprises, LLC 327 NC Highway 42
Ahoskie, North Carolina 27910
143 Tunis Road
Winton, North Carolina 27986 Yes Non Potable ~1,060 SW
WSW-24 6926-03-6133 Bradshaw, Jackie Doyle 101 Tryon Street
Atlantic Beach, North Carolina 28512
145 Tunis Road
Winton, North Carolina 27986 Yes Non Potable ~930 SW
WSW-25 6926-03-6275 Hodges, Dennis Clifton 147 Tunis Road
Winton, North Carolina 27986
147 Tunis Road
Winton, North Carolina 27986 No Potable ~790 SW
WSW-26 6926-13-0201 Burnette, Bobby W. and Linda P.152 Tunis Road
Winton, North Carolina 27986
152 Tunis Road
Winton, North Carolina 27986 No Potable ~700 S
WSW-27 6926-03-9101 Stephens, Lynwood and Betty 150 Tunis Road
Winton, North Carolina 27986
150 Tunis Road
Winton, North Carolina 27986 Yes Non Potable ~820 SW
WSW-28
WSW-33 6926-03-8437 Byrom, Aaron Thomas, III Post Office Box 625
Ahoskie, North Carolina 27910
153 Tunis Road
Winton, North Carolina 27986 Yes Non Potable ~620 SW
~560 SW
WSW-29 6926-03-7353 Harmon, Frances M.149 Tunis Road
Winton, North Carolina 27986
149 Tunis Road
Winton, North Carolina 27986 No Potable ~710 SW
WSW-30 6926-03-7434 Powell, Rany Alan 153 Tunis Road
Winton, North Carolina 27986
153 Tunis Road
Winton, North Carolina 27986 No Potable ~630 SW
WSW-31 6926-13-1313 Taylor, Carroll R. and Nancy 202 Tunis Road
Winton, North Carolina 27986
202 Tunis Road
Winton, North Carolina 27986 No Potable ~550 S
WSW-32 6926-03-8566 Padgett, Terri Lynn and Steeley, Stanley Post Office Box 1515
Ahoskie, North Carolina 27910
201 Tunis Road
Winton, North Carolina 27986 Yes Non Potable ~450 SW
WSW-34 6926-03-9752 Parker, Benjamin Samuel, Jr.Post Office Box 63
Harrellsville, North Carolina 27942
205 Tunis Road
Winton, North Carolina 27986 Yes Non Potable ~250 SW
WSW-35 6926-13-0823 Fenn, David 207 Tunis Road
Winton, North Carolina 27986
207 Tunis Road
Winton, North Carolina 27986 Yes Non Potable ~230 SW
WSW-36 6926-04-7287 Tapscott, Melissa Post Office Box 327
Cofield, North Carolina 27922
118 Tunis Road
Winton, North Carolina 27986 Yes Non Potable ~610 SW
WSW-37 6926-14-4877 Conner, Joyce J.108 Pembroke Circle
Edenton, North Carolina 27932
104 Freeman Drive
Winton, North Carolina 27986 Yes Non Potable ~1,010 NE
WSW-38 6926-15-5061 Jones, G. Wesley and Jean D.110 Freeman Drive
Winton, North Carolina 27986
110 Freeman Drive
Winton, North Carolina 27986 Yes Non Potable ~1,140 NE
Note:
• Water supply wells are keyed to Figure 2.
Page 2 of 2
05/21/08 22.63 0.26 77.59 ---
03/09/09 23.42 0.42 76.94 ---
06/23/09 24.53 0.80 76.16 ---
09/23/09 24.61 0.35 75.69 ---
12/28/09 23.47 0.32 76.80 ---
03/23/10 22.50 0.28 77.74 ---
07/19/10 23.75 0.57 76.74 Before MMPE
07/23/10 23.95 ---76.05 After MMPE
02/07/11 22.99 0.36 77.32 Before MMPE
02/11/11 22.94 ---77.06 After MMPE
03/24/11 22.93 0.29 77.32 ---
08/08/11 24.42 ---75.58 Before MMPE
08/12/11 25.22 0.34 74.78 After MMPE
09/13/11 23.73 0.72 76.89 ---
04/23/12 25.66 3.74 77.55 Before MMPE
04/27/12 24.70 1.01 76.17 After MMPE
05/29/12 23.52 0.80 77.17 ---
01/22/13 25.45 3.24 77.33 Before AFVR
01/22/13 26.60 2.00 75.12 After AFVR
02/25/13 24.37 2.28 77.59 ---
08/29/13 25.43 1.75 76.07 Before AFVR
08/29/13 24.58 0.71 76.03 After AFVR
10/02/13 25.34 1.25 75.73 ---
06/26/14 23.16 0.21 77.02 ---
01/28/15 23.19 0.06 76.86 ---
08/12/15 23.00 ---77.00 ---
01/21/16 22.32 ---77.68 Boom Removal
02/23/16 21.28 ---78.72 ---
11/21/16 21.62 0.11 78.47 ---
07/20/17 22.54 0.16 77.60 ---
05/05/18 22.85 0.20 77.32 Before AFVR
05/05/18 23.34 ---76.66 After AFVR
06/11/18 22.92 0.14 77.20 ---
02/04/19 22.53 0.06 77.52 ---
08/06/19 23.22 ---76.78 ---
02/18/20 22.93 ---77.07 ---
10/21/20 23.53 ---76.47 ---
02/28/22 23.25 ---76.75
05/21/08 21.55 ---77.62 ---
03/09/09 22.21 ---76.96 ---
06/23/09 23.01 ---76.16 ---
09/23/09 23.37 ---75.80 ---
12/28/09 22.42 ---76.75 ---
03/23/10 21.11 ---78.06 ---
02/07/11 21.78 ---77.39 Before MMPE
02/11/11 22.11 ---77.06 After MMPE
03/24/11 21.79 ---77.38 ---
08/08/11 23.62 ---75.55 Before MMPE
08/12/11 24.09 ---75.08 After MMPE
09/13/11 22.22 ---76.95 ---
05/29/12 22.15 ---77.02 ---
02/25/13 21.61 ---77.56 ---
10/02/13 23.41 ---75.76 ---
06/26/14 22.06 ---77.11 ---
01/28/15 22.24 ---76.93 ---
08/12/15 22.09 ---77.08 ---
02/23/16 20.42 ---78.75 ---
06/11/18 21.97 ---77.20 ---
02/04/19 21.58 ---77.59 ---
08/06/19 22.33 ---76.84 ---
02/28/22 24.46 ---74.71 ---
05/21/08 24.57 ---77.56 ---
03/09/09 25.16 ---76.97 ---
06/23/09 25.90 ---76.23 ---
09/23/09 26.37 ---75.76 ---
12/28/09 25.41 ---76.72 ---
03/23/10 24.24 ---77.89 ---
03/24/11 24.80 ---77.33 ---
09/13/11 25.20 ---76.93 ---
05/29/12 25.10 ---77.03 ---
02/25/13 24.56 ---77.57 ---
10/02/13 26.40 ---75.73 ---
06/26/14 25.03 ---77.10 ---
01/28/15 25.24 ---76.89 ---
08/12/15 25.07 ---77.06 ---
02/23/16 23.43 ---78.70 ---
06/11/18 29.90 ---72.23 ---
02/04/19 24.57 ---77.56 ---
08/06/19 25.30 ---76.83 ---
02/28/22 25.41 ---76.72 ---
102.133020 - 3020
100.003020 - 302001/19/93MW-1
99.173020 - 302001/21/93MW-2
01/22/93MW-3
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
H&S TRADING (INCIDENT NO. 10151)
Date: 03/17/22 Facility ID # : 0-009678
Well ID
Date
Installed
(mm/dd/yy)
Date
Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y
ft. BGS)
Bottom
of Well
(ft. BGS)
Top of Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(feet)
Free Product
Thickness
(ft.)
Ground
Water
Elevation (ft.)
Comments
Page 1 of 5
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
H&S TRADING (INCIDENT NO. 10151)
Date: 03/17/22 Facility ID # : 0-009678
Well ID
Date
Installed
(mm/dd/yy)
Date
Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y
ft. BGS)
Bottom
of Well
(ft. BGS)
Top of Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(feet)
Free Product
Thickness
(ft.)
Ground
Water
Elevation (ft.)
Comments
05/21/08 20.36 ---77.60 ---
03/09/09 21.04 ---76.92 ---
06/23/09 21.60 ---76.36 ---
09/23/09 22.19 ---75.77 ---
12/28/09 20.68 ---77.28 ---
03/23/10 20.02 ---77.94 ---
03/24/11 20.58 ---77.38 ---
09/13/11 21.01 ---76.95 ---
05/29/12 20.82 ---77.14 ---
02/25/13 20.30 ---77.66 ---
10/02/13 NM NM NM Inaccessable
06/26/14 NM NM NM Inaccessable
01/28/15 NM NM NM Inaccessable
08/12/15 NM NM NM Inaccessable
05/21/08 17.58 ---77.18 ---
03/09/09 20.03 ---74.73 ---
06/23/09 17.41 ---77.35 ---
09/23/09 18.23 ---76.53 ---
12/28/09 16.27 ---78.49 ---
03/23/10 16.30 ---78.46 ---
03/24/11 17.63 ---77.13 ---
09/13/11 17.92 ---76.84 ---
05/29/12 17.78 ---76.98 ---
02/25/13 17.53 ---77.23 ---
10/02/13 18.59 ---76.17 ---
06/26/14 17.86 ---76.90 ---
01/28/15 18.04 ---76.72 ---
08/12/15 18.03 ---76.73 ---
02/23/16 16.45 ---78.31 ---
06/11/18 17.98 ---76.78 ---
02/04/19 17.63 ---77.13 ---
08/06/19 18.32 ---76.44 ---
02/28/22 18.11 ---76.65 ---
05/21/08 20.27 ---78.25 ---
03/09/09 20.61 ---77.91 ---
06/23/09 20.72 ---77.80 ---
09/23/09 20.61 ---77.91 ---
12/28/09 20.38 ---78.14 ---
03/23/10 19.77 ---78.75 ---
03/24/11 20.41 ---78.11 ---
09/13/11 20.55 ---77.97 ---
05/29/12 20.29 ---78.23 ---
02/25/13 20.31 ---78.21 ---
10/02/13 20.87 ---77.65 ---
06/26/14 20.46 ---78.06 ---
01/28/15 20.23 ---78.29 ---
08/12/15 20.58 ---77.94 ---
02/23/16 19.79 ---78.73 ---
06/11/18 20.65 ---77.87 ---
02/04/19 20.38 ---78.14 ---
08/06/19 20.74 ---77.78 ---
02/28/22 20.60 ---77.92 ---
05/21/08 24.05 ---75.51 ---
03/09/09 24.70 ---74.86 ---
06/23/09 24.45 ---75.11 ---
09/23/09 25.00 ---74.56 ---
12/28/09 24.18 ---75.38 ---
03/23/10 23.63 ---75.93 ---
03/24/11 24.24 ---75.32 ---
09/13/11 24.43 ---75.13 ---
05/29/12 24.55 ---75.01 ---
02/25/13 24.23 ---75.33 ---
06/26/14 24.18 ---75.38 ---
01/28/15 24.35 ---75.21 ---
08/12/15 24.13 ---75.43 ---
05/21/08 18.63 ---76.93 ---
03/09/09 18.95 ---76.61 ---
06/23/09 18.04 ---77.52 ---
09/23/09 19.00 ---76.56 ---
12/28/09 18.09 ---77.47 ---
03/23/10 17.25 ---78.31 ---
03/24/11 18.77 ---76.79 ---
09/13/11 18.81 ---76.75 ---
05/29/12 18.23 ---77.33 ---
02/25/13 18.31 ---77.25 ---
10/02/13 20.90 ---74.66 ---
06/26/14 18.98 ---76.58 ---
01/28/15 18.09 ---77.47 ---
08/12/15 19.08 ---76.48 ---
98.5230
30 97.96
30 95.56
MWD-7 07/02/93 45 45 - 50 50 99.56
MW-8 09/10/94 20 20 - 30
20 - 302007/02/93MW-5
07/01/93MW-4 20 20 - 30
20 - 302007/07/93MW-6
94.7630
Page 2 of 5
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
H&S TRADING (INCIDENT NO. 10151)
Date: 03/17/22 Facility ID # : 0-009678
Well ID
Date
Installed
(mm/dd/yy)
Date
Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y
ft. BGS)
Bottom
of Well
(ft. BGS)
Top of Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(feet)
Free Product
Thickness
(ft.)
Ground
Water
Elevation (ft.)
Comments
05/21/08 NM NM NM Not Located
03/09/09 5.58 ---75.53 ---
06/23/09 5.50 ---75.61 ---
09/23/09 6.72 ---74.39 ---
12/28/09 4.40 ---76.71 ---
03/23/10 3.93 ---77.18 ---
03/24/11 5.05 ---76.06 ---
09/13/11 5.57 ---75.54 ---
05/29/12 5.59 ---75.52 ---
02/25/13 4.74 ---76.37 ---
10/02/13 6.02 ---75.09 ---
06/26/14 4.62 ---76.49 ---
01/28/15 3.48 ---77.63 ---
08/12/15 6.48 ---74.63 ---
05/21/08 4.65 ---76.37 ---
03/09/09 4.77 ---76.25 ---
06/23/09 4.90 ---76.12 ---
09/23/09 6.34 ---74.68 ---
12/28/09 3.42 ---77.60 ---
03/23/10 2.81 ---78.21 ---
03/24/11 4.40 ---76.62 ---
09/13/11 4.95 ---76.07 ---
05/29/12 NM NM NM ---
06/26/14 NM NM NM ---
05/21/08 3.88 ---77.94 ---
03/09/09 3.52 ---78.30 ---
06/23/09 4.15 ---77.67 ---
09/23/09 5.10 ---76.72 ---
12/28/09 2.73 ---79.09 ---
03/23/10 2.39 ---79.43 ---
03/24/11 3.50 ---78.32 ---
09/13/11 3.52 ---78.30 ---
05/29/12 NM NM NM ---
06/26/14 NM NM NM ---
05/21/08 25.49 ---77.60 ---
03/09/09 26.18 ---76.91 ---
06/23/09 26.70 ---76.39 ---
09/23/09 27.82 ---75.27 ---
12/28/09 25.97 ---77.12 ---
03/23/10 24.92 ---78.17 ---
03/24/11 25.82 ---77.27 ---
09/13/11 26.50 ---76.59 ---
05/29/12 26.03 ---77.06 ---
02/25/13 25.64 ---77.45 ---
10/02/13 27.32 ---75.77 ---
06/26/14 25.98 ---77.11 ---
01/28/15 26.15 ---76.94 ---
08/12/15 25.98 ---77.11 ---
02/28/22 26.52 ---76.57 ---
05/21/08 24.14 ---78.78 ---
03/09/09 24.72 ---78.20 ---
06/23/09 24.30 ---78.62 ---
09/23/09 25.00 ---77.92 ---
12/28/09 24.31 ---78.61 ---
03/23/10 23.23 ---79.69 ---
03/24/11 NM NM NM Not Located
09/13/11 NM NM NM Not Located
05/29/12 NM NM NM Not Located
06/26/14 NM NM NM Not Located
01/28/15 NM NM NM Not Located
05/21/08 19.95 ---77.41 ---
03/09/09 20.51 ---76.85 ---
06/23/09 21.09 ---76.27 ---
09/23/09 21.75 ---75.61 ---
12/28/09 20.17 ---77.19 ---
03/23/10 19.49 ---77.87 ---
03/24/11 20.13 ---77.23 ---
09/13/11 20.55 ---76.81 ---
05/29/12 NM NM NM ---
06/26/14 NM NM NM ---
02/28/22 20.71 ---76.65 ---
97.363525 - 352508/2002MW-14
MW-10 09/12/94
MW-9 09/10/94
13 81.02
3 3 - 13 13 81.11
2508/2002MW-12
3 3 - 13
MW-11 09/12/94 3 3 - 13 13 81.82
25 25 - 35 35 102.92MW-13 08/2002
103.093525 - 35
Page 3 of 5
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
H&S TRADING (INCIDENT NO. 10151)
Date: 03/17/22 Facility ID # : 0-009678
Well ID
Date
Installed
(mm/dd/yy)
Date
Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y
ft. BGS)
Bottom
of Well
(ft. BGS)
Top of Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(feet)
Free Product
Thickness
(ft.)
Ground
Water
Elevation (ft.)
Comments
03/09/09 9.80 ---75.93 ---
06/23/09 9.56 ---76.17 ---
09/23/09 10.73 ---75.00 ---
12/28/09 8.88 ---76.85 ---
03/23/10 7.92 ---77.81 ---
03/24/11 9.50 ---76.23 ---
09/13/11 9.78 ---75.95 ---
05/29/12 9.73 ---76.00 ---
02/25/13 9.27 ---76.46 ---
10/02/13 11.43 ---74.30 ---
06/26/14 NM NM NM ---
01/28/15 NM NM NM Destroyed
08/12/15 NM NM NM Destroyed
03/09/09 20.10 ---77.35 ---
06/23/09 19.67 ---77.78 ---
09/23/09 20.30 ---77.15 ---
12/28/09 19.50 ---77.95 ---
03/23/10 18.50 ---78.95 ---
03/24/11 19.63 ---77.82 ---
09/13/11 19.95 ---77.50 ---
05/29/12 NM NM NM Destroyed
06/26/14 NM NM NM Destroyed
08/12/15 NM NM NM Destroyed
03/09/09 32.90 ---67.97 ---
06/23/09 22.36 ---78.51 ---
09/23/09 23.44 ---77.43 ---
12/28/09 22.32 ---78.55 ---
03/23/10 21.45 ---79.42 ---
03/24/11 22.37 ---78.50 ---
09/13/11 22.93 ---77.94 ---
05/29/12 NM NM NM Destroyed
06/26/14 NM NM NM Destroyed
08/12/15 NM NM NM Destroyed
12/28/09 2.21 ---76.99 ---
03/23/10 2.08 ---77.12 ---
03/24/11 3.50 ---75.70 ---
09/13/11 3.92 ---75.28 ---
05/29/12 3.88 ---75.32 ---
02/25/13 3.03 ---76.17 ---
10/02/13 7.53 ---71.67 ---
06/26/14 6.20 ---73.00 ---
01/28/15 4.57 ---74.63 ---
07/19/10 22.22 ---78.15 Before MMPE
07/23/10 23.46 0.01 76.92 After MMPE
02/07/11 21.57 ---78.80 Before MMPE
02/11/11 21.81 ---78.56 After MMPE
03/24/11 21.33 ---79.04 ---
08/08/11 21.84 0.01 78.53 Before MMPE
08/12/11 26.10 ---74.27 After MMPE
09/13/11 21.28 ---79.09 ---
04/23/12 21.85 0.01 78.53 Before MMPE
04/27/12 24.50 ---75.87 After MMPE
05/29/12 21.48 ---78.89 ---
02/25/13 21.20 0.02 79.19 ---
08/29/13 21.67 0.02 78.72 Before AFVR
08/29/13 24.09 ---76.28 After AFVR
10/02/13 21.87 0.02 78.52 ---
06/26/14 21.26 ---79.11 ---
01/28/15 21.80 0.02 78.59 ---
08/12/15 21.36 ---79.01 ---
01/21/16 21.32 ---79.05 Boom Removal
02/23/16 20.72 ---79.65 ---
11/21/16 21.02 0.02 79.37 ---
07/20/17 21.29 ---79.08 ---
05/05/18 21.45 ---78.92 Before AFVR
05/05/18 23.55 ---76.82 After AFVR
06/11/18 21.42 ---78.95 ---
02/04/19 21.47 ---78.90 ---
08/06/19 21.13 ---79.24 ---
02/18/20 21.68 ---78.69 ---
10/21/20 21.36 ---79.01 ---
02/28/22 21.66 ---78.71 ---
03/24/11 20.94 ---78.80 ---
09/13/11 21.06 ---78.68 ---
05/29/12 21.06 ---78.68 ---
02/25/13 20.90 ---78.84 ---
10/02/13 NM NM NM Inaccessable
06/26/14 NS ---NS ---
01/28/15 NM NM NM Inaccessable
03/24/11 20.15 ---NM ---
09/13/11 20.49 ---NM ---
08/12/15 20.36 ---NM ---
MW-17 03/05/09 20
100.373020 - 302007/19/10MW-19
MW-18
MW-16 03/06/09 13.6 13.6 - 28.6 28.6 97.45
MW-15 03/06/09 9
5 5 - 15 15 79.20
RW-1 NA
MW-20 07/19/10 20 20 - 30 30 99.74
12/15/09
9 - 24 24 85.73
NA NA NA NM
20 - 35 35 100.87
Page 4 of 5
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
H&S TRADING (INCIDENT NO. 10151)
Date: 03/17/22 Facility ID # : 0-009678
Well ID
Date
Installed
(mm/dd/yy)
Date
Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y
ft. BGS)
Bottom
of Well
(ft. BGS)
Top of Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(feet)
Free Product
Thickness
(ft.)
Ground
Water
Elevation (ft.)
Comments
07/19/10 22.51 0.01 NM Before MMPE
07/23/10 17.30 ---NM After MMPE
02/07/11 21.44 ---NM Before MMPE
02/11/11 23.72 ---NM After MMPE
03/24/11 21.92 ---NM ---
09/13/11 22.34 ---NM ---
04/23/12 22.63 ---NM Before MMPE
04/27/12 22.60 ---NM After MMPE
05/29/12 22.26 ---NM ---
02/25/13 21.68 ---NM ---
06/26/14 22.20 ---NM ---
01/28/15 22.40 ---NM ---
08/12/15 22.22 ---NM ---
02/28/22 22.52 ---NM ---
07/19/10 22.17 ---NM Before MMPE
07/23/10 22.86 ---NM After MMPE
02/07/11 21.90 ---NM Before MMPE
02/11/11 22.15 ---NM After MMPE
03/24/11 21.59 ---NM ---
09/13/11 22.05 0.04 NM ---
04/23/12 22.28 ---NM Before MMPE
04/27/12 22.73 ---NM After MMPE
05/29/12 21.92 ---NM ---
02/25/13 21.36 ---NM ---
10/02/13 23.28 0.05 NM ---
06/26/14 21.86 ---NM ---
01/28/15 22.02 ---NM ---
08/12/15 21.89 ---NM ---
01/21/16 21.23 ---NM Boom Removal
11/21/16 20.44 ---NM ---
07/20/17 21.29 ---NM ---
06/11/18 22.66 ---NM ---
02/04/19 21.38 ---NM ---
08/06/19 22.14 ---NM ---
02/18/20 21.83 ---NM ---
10/21/20 22.55 ---NM ---
02/28/22 22.19 ---NM ---
03/24/11 17.31 ---NM ---
09/13/11 17.63 ---NM ---
05/29/12 17.49 ---NM ---
02/25/13 19.82 ---NM ---
06/26/14 17.53 ---NM ---
01/28/15 17.65 ---NM ---
08/12/15 17.60 ---NM ---
03/24/11 NM NM NM Pump Stuck
09/13/11 NM NM NM Pump Stuck
03/24/11 18.49 ---NM ---
09/13/11 17.64 ---NM ---
05/29/12 17.53 ---NM ---
02/25/13 17.00 ---NM ---
10/02/13 18.77 ---NM ---
06/26/14 17.51 ---NM ---
01/28/15 17.66 ---NM ---
08/12/15 17.58 ---NM ---
03/24/11 14.49 ---NM ---
09/13/11 15.19 ---NM ---
03/24/11 21.02 ---NM ---
09/13/11 21.45 ---NM ---
05/29/12 21.32 ---NM ---
02/25/13 20.77 ---NM ---
10/02/13 23.72 ---NM ---
06/26/14 21.27 ---NM ---
01/28/15 22.91 ---NM ---
Notes:
• *: Reference point for elevation measurements; assumed elevation 100.00 feet.
• **: If free product is present in a well, ground water elevation should be calculated by: (Top of Casing Elevation - Depth to Water) + (Free Product
Thickness x 0.8581)
• ft BGS : feet below ground surface.
• NM: Not Measured.
• Top of casing information for monitoring wells were obtained from the report titled ' Semi Annual Ground Water Monitoring Report' dated March 24, 2005
prepared by CES Engineering, P. C. Well construction information, where available, are obtained from well construction records, well identification tags and
field measurements.
• Please note that well construction information for MW-6 and MWD-7 did not match existing well construction records on file. Well construction details
for these wells and MW-12 through MW-14 are based on well identification tags and the gauged well depths.
• Monitoring wells MW-15 through MW-17 were installed by Greenwood Applies Services personnel. Top of casing elevations for these wells were
surveyed by GRI personnel during the March 2009 sampling event.
RW-2
NMNANANANARW-1A
RW-3 NA NA NA NA NM
NA
RW-5 NA NA NA NA NM
RW-4 NA NA NA NA NM
RW-8 NA NA NA NA NM
RW-6 NA NA NA NA NM
NMNANANA
Page 5 of 5
Date: 03/17/22 Facility ID #: 00-0-0000018273
5030/
8015D
3550/
8015C
50 100
NE NE
NE NE
TMW-1-2 02/28/22 2 <10 1.6
TMW-1-4 02/28/22 4 <10 1.28
TMW-1-6 02/28/22 6 <10 1.28
TMW-1-8 02/28/22 8 <10 1.32
TMW-1-10 02/28/22 10 172 42
TMW-1-12 02/28/22 12 179 45
TMW-1-14 02/28/22 14 182 48
TMW-1-16 02/28/22 16 188 58
TMW-1-18 02/28/22 18 243 73
TMW-1-20 02/28/22 20 129 57
TMW-1-22 02/28/22 22 155 39
TMW-1-24 02/28/22 24 45 5
TMW-1-26 02/28/22 26 2 2
TMW-1-28 02/28/22 28 19.4 8.72
TMW-1-30 02/28/22 30 137 43
TMW-2-2 02/28/22 2 <2 1.68
TMW-2-4 02/28/22 4 <2 1.56
TMW-2-6 02/28/22 6 4.36 2.72
TMW-2-8 02/28/22 8 1,091 381
TMW-2-10 02/28/22 10 25 4
TMW-2-12 02/28/22 12 405 125
TMW-2-14 02/28/22 14 364 123
TMW-2-16 02/28/22 16 42 4
TMW-2-18 02/28/22 18 46 15
TMW-2-20 02/28/22 20 316 128
TMW-2-22 02/28/22 22 93 37
TMW-2-24 02/28/22 24 36 13
TMW-2-26 02/28/22 26 15.4 9.08
TMW-2-28 02/28/22 28 6.32 4.88
TMW-2-30 02/28/22 30 3.44 3.08
TMW-1-28 DUP 02/28/22 16 <2 2
Notes:
• Results reported in mg/kg (milligrams per kilograms)
• ft-BGS: feet below ground surface.
• RAL: Regulatory Action Level.
• MCCs: Maximum Contaminant Concentrations.
• SCLs: Soil Cleanup Levels.
• < : Less than the method detection limit specified in the
laboratory report
• Concentrations in bold face type exceeded the RAL or the
soil-to-water MCC.
• NE: Not Established
• NR: Not Requested.
RAL (mg/kg)
Soil to Water MCC (mg/kg)
Residential SCLs (mg/kg)Sample IDDate Collected (mm/dd/yy)Sample Depth(ft-BGS)Gasoline-Range TPHDiesel-Range TPHTABLE 6
SUMMARY OF SOIL SAMPLE ANALYTICAL RESULTS
H&S TRADING (INCIDENT NO. 10151)
Analytical Method 
Page 1 of 1
EPA Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 70 400 400 15 400 700 200
5,000 260,000 80,000 50,000 20,000 6,000 30,500 70,000 26,100 28,500 24,100 15,000 NE NE NE
05/21/08 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
03/09/09 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
06/23/09 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
09/23/09 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
12/28/09 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
03/23/10 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
03/24/11 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
09/13/11 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
05/29/12 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
02/25/13 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
10/02/13 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
06/26/14 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
01/28/15 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
08/12/15 29.0 J <17 1,230 1,710 63.8 2,270 426 <16 819 9,100 3,120 NR NR NR NR
02/23/16 <31 <31 1,840 917 51.8 J 4,880 753 <31 1,450 19,200 E 5,610 NR NR NR NR
11/21/16 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
07/20/17 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
05/04/18 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
06/11/18 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
02/04/19 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
08/06/19 26.1 J <13 788 <25 14.2 J 1,650 352 <13 704 8,770 <13 NR NR NR NR
02/18/20 10.9 J <6.3 187 <13 12.1 J 369 60.4 <6.3 104 1,400 <6.3 NR NR NR NR
10/21/20 11.5 <2.5 166 <5.0 19.9 437 46.8 <2.5 86.0 808 <2.5 NR NR NR NR
02/28/22 4.9 J <3.1 524 <6.3 5.2 J 1,610 362 <3.1 706 2,130 E <3.1 NR NR NR NR
05/21/08 <100 <100 <100 <300 5,800 185 <100 <500 <100 122 <100 4.09 2,140 3,000 <2,000
03/09/09 8.3 J <1.4 3.2 J 3.6 J 1,400 9.5 JB <1.1 <2.0 <1.5 20 6.2 J <3.0 <100 1,500 2,800
06/23/09 2.29 J <1.65 <3.35 5.62 J 2,290 8.42 J <5.00 <8.35 <1.65 14.7 5.36 <1.50 168 1,100 803
09/23/09 6.11 <0.190 5.68 7.47 1,260 11.1 1.68 2.22 2.87 32.3 11.4 <1.50 NR NR NR
12/28/09 6.93 <0.950 6.71 7.93 2,210 12.2 2.68 J 3.26 J 4.33 J 35.7 13.2 2.24 J NR NR NR
03/23/10 8.62 <3.80 52.8 57.7 2,980 44.4 6.03 J 8.70 J 6.06 J 49.7 9.45 J 2.03 NR NR NR
03/24/11 10.4 <1.90 69.4 125 3,840 112 12.5 7.45 J 13.8 341 81.6 NR 1,890 1,320 1,210
09/13/11 8.7 J <6.4 25.9 56.8 2,070 42.6 <5.0 5.4 J <5.4 93.6 34.7 <5.0 NR NR NR
05/29/12 <6.5 <6.4 18.3 J <15 2,350 21.8 J <5.0 6.2 J <5.4 45.6 <5.0 NR NR NR NR
02/25/13 7.0 <0.10 13.5 5.9 811 20.3 3.0 5.0 2.4 27.4 1.7 NR NR NR NR
10/02/13 2.2 <0.10 1.8 0.20 J 127 5.9 2.1 0.93 2.0 9.7 0.24 J NR NR NR NR
06/26/14 18.2 0.12 J 1.3 0.65 J 180 4.6 0.69 5.4 0.54 1.3 0.12 J NR NR NR NR
01/28/15 4.1 <0.17 0.16 J <0.43 19.2 <0.12 0.14 J 1.0 <0.16 <0.14 <0.14 NR NR NR NR
08/12/15 7.7 <0.17 3.2 0.45 J 42.4 5.4 1.4 3.5 0.88 4.6 0.26 J NR NR NR NR
02/23/16 5.0 <0.13 3.2 1.9 31.6 24.2 6.1 2.5 13.6 6.1 J 61.8 E NR NR NR NR
06/11/18 3.5 <0.13 3.2 0.56 J 8.4 19.5 4.1 2.2 4.4 16.4 0.61 NR NR NR NR
02/04/19 6.2 <0.13 1.2 0.77 J 8.5 12.7 4.9 2.7 4.5 10.6 1.6 NR NR NR NR
08/06/19 2.0 <0.13 <0.13 0.34 J 4.5 4.2 3.5 0.81 4.1 4.5 0.69 NR NR NR NR
02/28/22 <0.13 <0.13 <0.13 <0.25 5.4 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
MW-1
MW-2 LeadMTBETABLE 7
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
H&S TRADING (INCIDENT NO. 10151)
Date : 03/23/21 Facility ID # : 0-009678
Analytical Method
EPA Method 6200B MADEP Method VPH
C5-C8 AliphaticsC9-C12 AliphaticsC9-C10 Aromaticsn-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneMAC (μg/l)
GCL (mg/l)NaphthaleneIsopropylbenzeneIPEContaminant of Concern
BenzeneTolueneEthylbenzeneXylenesPage 1 of 10
EPA Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 70 400 400 15 400 700 200
5,000 260,000 80,000 50,000 20,000 6,000 30,500 70,000 26,100 28,500 24,100 15,000 NE NE NELeadMTBETABLE 7
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
H&S TRADING (INCIDENT NO. 10151)
Date : 03/23/21 Facility ID # : 0-009678
Analytical Method
EPA Method 6200B MADEP Method VPH
C5-C8 AliphaticsC9-C12 AliphaticsC9-C10 Aromaticsn-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneMAC (μg/l)
GCL (mg/l)NaphthaleneIsopropylbenzeneIPEContaminant of Concern
BenzeneTolueneEthylbenzeneXylenes05/21/08 0.910 I <1.0 <1.0 <3.0 895 <1.0 0.510 I 2.37 I 0.350 I 1.13 0.480 I 16.3 112 173 <100
03/09/09 <0.60 <0.70 <0.50 <1.0 550 1.2 JB <0.55 <1.0 <0.75 <0.70 <0.50 4.1 <100 170 100
06/23/09 <0.400 <0.660 <1.34 <2.66 211 <2.00 <2.00 <3.34 <0.660 <0.660 <0.660 7.41 <100 <100 <100
09/23/09 <0.140 <0.190 <0.150 <0.220 250 <0.500 <0.150 0.718 J <0.220 <0.150 <0.180 18.6 NR NR NR
12/28/09 <0.140 <0.190 <0.150 <0.220 291 <0.500 <0.150 0.815 J <0.220 <0.150 <0.180 8.11 NR NR NR
03/23/10 <0.140 <0.190 <0.150 <0.220 359 <0.500 <0.150 1.32 <0.220 <0.150 <0.180 4.33 NR NR NR
03/24/11 <0.700 <0.950 <0.750 <1.10 882 <2.50 0.764 J 2.59 J <1.10 1.34 J <0.900 NR 522 105 122
09/13/11 0.36 J <0.13 <0.15 0.64 J 217 6.1 0.32 J 0.80 0.39 J 7.5 2.3 11.6 NR NR NR
05/29/12 <1.3 <1.3 <1.5 <3.0 434 <1.0 <1.0 1.6 J <1.1 <1.0 <1.0 NR NR NR NR
02/25/13 0.43 J <0.10 <0.10 <0.22 285 0.44 J 0.21 J 1.0 0.14 J 0.17 J <0.10 NR NR NR NR
10/02/13 1.8 J <0.50 <0.50 <1.1 145 1.4 J 0.67 J 1.6 J <0.50 0.77 J <0.50 NR NR NR NR
06/26/14 1.4 <0.10 0.30 J 0.27 J 245 0.97 0.79 2.7 0.78 2.0 0.22 J NR NR NR NR
01/28/15 0.61 J <0.42 <0.38 <1.1 119 0.98 J <0.30 0.92 J <0.39 <0.34 <0.34 NR NR NR NR
08/12/15 1.7 <0.17 <0.15 <0.43 139 1.2 0.60 2.0 0.55 2.2 0.57 NR NR NR NR
02/23/16 0.26 J <0.13 0.14 J <0.31 84.5 40.6 0.35 J 0.69 <0.13 7.4 1.6 NR NR NR NR
06/11/18 <0.13 <0.13 <0.13 <0.26 22.2 <0.13 <0.13 1.3 <0.13 <0.13 <0.13 NR NR NR NR
02/04/19 0.46 J <0.13 <0.13 <0.25 6.1 0.33 J 0.16 J 0.69 0.18 J 0.50 0.18 J NR NR NR NR
08/06/19 0.85 <0.13 <0.13 <0.25 6.4 0.62 0.20 J 0.81 0.25 J 0.61 0.25 J NR NR NR NR
02/28/22 <0.13 <0.13 <0.13 <0.25 1.0 <0.13 <0.13 0.26 J <0.13 <0.13 <0.13 NR NR NR NR
05/21/08 <1.0 <1.0 <1.0 <3.0 5.67 <1.0 <1.0 0.600 I <1.0 <1.0 <1.0 4.56 <100 <100 <100
03/09/09 <0.60 <0.70 <0.50 <1.0 4.2 J 0.82 JB <0.55 <1.0 <0.75 <0.70 <0.50 3.3 <100 <100 <100
06/23/09 <0.200 <0.330 <0.670 <1.33 10.3 <1.00 <1.00 <1.67 <0.330 1.09 0.440 J <1.50 <100 <100 <100
09/23/09 <0.140 <0.190 <0.150 <0.220 1.67 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 23.9 NR NR NR
12/28/09 <0.140 <0.190 <0.150 <0.220 1.02 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 30.3 NR NR NR
03/23/10 <0.140 <0.190 <0.150 <0.220 0.690 J <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 14.6 NR NR NR
03/24/11 <0.140 <0.190 <0.150 <0.220 0.766 J <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 NR <100 <100 <100
09/13/11 <0.13 <0.13 <0.15 <0.30 0.84 0.13 J <0.10 0.19 J <0.11 <0.10 <0.10 32.3 NR NR NR
05/29/12 <0.13 <0.13 <0.15 <0.30 0.81 <0.10 <0.10 0.14 J <0.11 <0.10 <0.10 NR NR NR NR
02/25/13 <0.10 <0.10 <0.10 <0.22 3.5 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
10/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/26/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/28/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
08/12/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
MW-3
MW-4
Page 2 of 10
EPA Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 70 400 400 15 400 700 200
5,000 260,000 80,000 50,000 20,000 6,000 30,500 70,000 26,100 28,500 24,100 15,000 NE NE NELeadMTBETABLE 7
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
H&S TRADING (INCIDENT NO. 10151)
Date : 03/23/21 Facility ID # : 0-009678
Analytical Method
EPA Method 6200B MADEP Method VPH
C5-C8 AliphaticsC9-C12 AliphaticsC9-C10 Aromaticsn-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneMAC (μg/l)
GCL (mg/l)NaphthaleneIsopropylbenzeneIPEContaminant of Concern
BenzeneTolueneEthylbenzeneXylenes05/21/08 8.87 <1.0 5.65 <3.0 246 12.2 9.84 21.1 9.09 <1.0 <1.0 25.6 871 134 251
03/09/09 120 19 J 560 2,000 1,700 140 B <2.2 18 J 92 710 140 5.4 260 2,400 2,100
06/23/09 153 <33.0 333 709 4,840 116 J <100 <167 59.4 J 249 191 2.93 J 365 839 1,340
09/23/09 131 34.2 1,310 4,860 6,460 250 112 17.8 J 212 1,490 295 37.7 NR NR NR
12/28/09 71.2 6.01 386 905 1,150 121 71.7 9.67 114 510 85.2 2.72 J NR NR NR
03/23/10 1.20 <0.190 1.87 1.16 66.0 1.61 2.02 <1.03 3.12 2.08 <0.180 5.63 NR NR NR
03/24/11 3.77 J <0.950 <0.750 <1.10 149 3.84 J 18.5 13.9 13.0 3.11 J <0.900 NR 533 <100 179
09/13/11 100 6.5 J 712 2,236 2,060 160 80.6 17.1 J 142 932 199 <5.0 NR NR NR
05/29/12 46.1 2.6 J 277 850 545 B 85.4 59.3 15.3 90.3 498 86.5 NR NR NR NR
02/25/13 6.9 <0.10 14.8 23.6 J 72.2 15.3 12.0 18.2 15.8 44.7 5.8 NR NR NR NR
10/02/13 25.9 0.67 188 366 764 50.9 40.3 16.9 53.0 277 39.8 NR NR NR NR
06/26/14 33.4 0.29 J 154 270 262 88.3 74.4 18.5 112 422 55.7 NR NR NR NR
01/28/15 28.6 <1.7 132 376 377 98.2 53.1 13.5 90.1 481 72.6 NR NR NR NR
08/12/15 3.1 0.28 J 4.1 16.6 65.7 16.5 19.0 15.9 20.1 45.8 8.6 NR NR NR NR
02/23/16 6.0 0.17 J 28.6 54.3 61.0 42.6 19.7 8.8 28.3 161 19.1 NR NR NR NR
06/11/18 9.3 <0.63 46.9 89.7 143 42.2 33.2 17.0 47.8 231 33.6 NR NR NR NR
02/04/19 3.3 0.18 J 8.3 19.6 31.0 8.6 10.4 18.9 8.1 58.2 7.3 NR NR NR NR
08/06/19 0.13 J 0.13 J 0.21 J 1.0 J 42.1 4.6 7.7 15.3 8.2 32.0 1.8 NR NR NR NR
02/28/22 1.1 <0.13 1.6 3.2 20.6 1.8 4.2 16.5 3.2 25.8 2.1 NR NR NR NR
05/21/08 <50 <50 <50 <150 2,120 <50 <50 <250 <50 <50 <50 8.96 1,400 1,100 <1,000
03/09/09 <4.8 <5.6 17 J 48 J 2,800 14 JB <4.4 <8.0 <6.0 23 J 5.1 J 3.8 <100 2,300 620
06/23/09 3.66 <1.65 <3.35 <6.65 2,590 5.49 J <5.00 <8.35 <1.65 <1.65 <1.65 <1.50 806 204 232
09/23/09 6.19 <0.190 10.0 9.05 2,880 13.1 2.12 10.3 2.61 7.78 0.960 J 11.3 NR NR NR
12/28/09 2.85 J <0.950 4.53 J 6.19 964 17.7 <0.750 6.02 1.84 J 5.24 <0.900 6.79 NR NR NR
03/23/10 3.94 <0.190 0.386 J <0.220 <0.250 <0.500 0.384 J 8.26 0.235 J <0.150 <0.180 <1.50 NR NR NR
03/24/11 6.15 J <1.90 2.46 J <2.20 361 <5.00 <1.50 7.90 J <2.20 2.44 J <1.80 NR 347 696 476
09/13/11 4.5 <0.64 2.5 1.4 J 140 2.0 J 0.70 J 5.7 0.66 J 1.6 J <0.50 <5.0 NR NR NR
05/29/12 5.5 <0.64 1.9 J <1.5 179 <0.50 0.73 J 7.5 <0.54 <0.50 <0.50 NR NR NR NR
02/25/13 5.1 <0.10 2.2 0.68 J 183 3.2 0.97 7.4 0.89 2.5 <0.10 NR NR NR NR
10/02/13 4.0 <0.10 0.39 J 0.48 J 70.1 1.3 0.28 J 5.1 0.14 J 0.30 J <0.10 NR NR NR NR
06/26/14 3.1 <0.10 0.34 J <0.20 46.4 0.73 0.31 J 6.4 0.15 J <0.10 <0.10 NR NR NR NR
01/28/15 3.6 <0.17 0.33 J <0.43 21.6 0.61 0.21 J 5.1 <0.16 <0.14 <0.14 NR NR NR NR
08/12/15 3.3 <0.17 0.58 <0.43 25.8 <0.12 0.36 J 5.2 0.20 J <0.14 <0.14 NR NR NR NR
02/23/16 2.7 <0.13 0.24 J <0.31 17.3 0.86 0.19 J 5.6 <0.13 <0.13 <0.13 NR NR NR NR
06/11/18 1.6 <0.13 <0.13 <0.26 14.3 <0.13 0.28 J 3.5 <0.13 <0.13 <0.13 NR NR NR NR
02/04/19 1.4 <0.13 <0.13 0.26 J 28.6 0.63 0.41 J 4.7 0.20 J 0.24 J <0.13 NR NR NR NR
08/06/19 0.21 J <0.13 <0.13 <0.25 29.1 <0.13 0.29 J 4.3 <0.13 <0.13 <0.13 NR NR NR NR
02/28/22 <0.13 <0.13 <0.13 <0.25 17.2 0.22 J 0.24 J 3.5 <0.13 <0.13 <0.13 NR NR NR NR
MW-6
MW-5
Page 3 of 10
EPA Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 70 400 400 15 400 700 200
5,000 260,000 80,000 50,000 20,000 6,000 30,500 70,000 26,100 28,500 24,100 15,000 NE NE NELeadMTBETABLE 7
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
H&S TRADING (INCIDENT NO. 10151)
Date : 03/23/21 Facility ID # : 0-009678
Analytical Method
EPA Method 6200B MADEP Method VPH
C5-C8 AliphaticsC9-C12 AliphaticsC9-C10 Aromaticsn-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneMAC (μg/l)
GCL (mg/l)NaphthaleneIsopropylbenzeneIPEContaminant of Concern
BenzeneTolueneEthylbenzeneXylenes05/21/08 <1.0 <1.0 <1.0 <3.0 5.13 <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 2.34 I <100 <100 <100
03/09/09 <0.60 <0.70 <0.50 1.3 J 5.6 0.81 JB <0.55 <1.0 <0.75 1.4 J <0.50 <3.0 <100 <100 <100
06/23/09 1.03 0.960 J <0.670 <1.33 17.1 <1.00 <1.00 <1.67 <0.330 0.344 J <0.330 <1.50 <100 251 <100
09/23/09 1.34 1.79 <0.150 1.96 20.1 1.54 <0.150 <0.200 <0.220 1.84 0.430 J <1.50 NR NR NR
12/28/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 2.07 J NR NR NR
03/23/10 <0.140 <0.190 <0.150 <0.220 0.789 J <0.500 <0.150 <0.200 <0.220 0.226 J <0.180 <1.50 NR NR NR
03/24/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 0.157 J <0.180 NR <100 <100 <100
09/13/11 <0.13 <0.13 0.44 J 3.26 J 1.6 7.8 0.30 J <0.11 0.70 16.3 6.6 <5.0 NR NR NR
05/29/12 <0.13 <0.13 <0.15 <0.30 0.23 J <0.10 <0.10 <0.11 <0.11 <0.10 <0.10 NR NR NR NR
02/25/13 0.12 J 0.58 0.13 J <0.22 5.2 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/26/14 <0.10 <0.10 <0.10 <0.20 0.47 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
01/28/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.12 <0.16 <0.16 <0.14 <0.14 NR NR NR NR
08/12/15 <0.17 <0.17 <0.15 <0.43 0.28 J <0.12 <0.12 <0.16 <0.16 <0.14 <0.14 NR NR NR NR
05/21/08 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 22.7 <100 <100 <100
03/09/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <0.55 <1.0 <0.75 <0.70 <0.50 3.4 <100 <100 <100
06/23/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.00 <1.67 <0.330 <0.330 <0.330 1.77 J <100 <100 <100
09/23/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 10.1 NR NR NR
12/28/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 9.75 NR NR NR
03/23/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 1.67 NR NR NR
03/24/11 <0.140 0.875 J <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 NR <100 <100 <100
09/13/11 <0.13 <0.13 6.7 <0.30 0.63 <0.10 <0.10 <0.11 <0.11 <0.10 <0.10 17.4 NR NR NR
05/29/12 <0.13 0.43 J <0.15 <0.30 7.4 <0.10 <0.10 <0.11 <0.11 <0.10 <0.10 NR NR NR NR
02/25/13 <0.10 <0.10 <0.10 <0.22 0.38 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
10/02/13 <0.10 <0.10 <0.10 <0.22 0.94 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/26/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
01/28/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.12 <0.16 <0.16 <0.14 <0.14 NR NR NR NR
08/12/15 <0.17 <0.17 <0.15 <0.43 0.38 J <0.12 <0.12 <0.16 <0.16 <0.14 <0.14 NR NR NR NR
MWD-7
MW-8
Page 4 of 10
EPA Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 70 400 400 15 400 700 200
5,000 260,000 80,000 50,000 20,000 6,000 30,500 70,000 26,100 28,500 24,100 15,000 NE NE NELeadMTBETABLE 7
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
H&S TRADING (INCIDENT NO. 10151)
Date : 03/23/21 Facility ID # : 0-009678
Analytical Method
EPA Method 6200B MADEP Method VPH
C5-C8 AliphaticsC9-C12 AliphaticsC9-C10 Aromaticsn-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneMAC (μg/l)
GCL (mg/l)NaphthaleneIsopropylbenzeneIPEContaminant of Concern
BenzeneTolueneEthylbenzeneXylenes05/21/08 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/09/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <0.55 <1.0 <0.75 <0.70 <0.50 17.5 <100 <100 <100
06/23/09 0.281 J 1.17 29.9 18.1 44.7 13.8 14.4 <1.67 22.8 34.2 28.7 8.54 108 264 253
09/23/09 <0.140 <0.190 <0.150 <0.220 37.9 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 29.6 NR NR NR
12/28/09 <0.140 0.487 J 15.2 8.92 17.4 3.24 9.28 <0.200 16.4 11.1 2.27 20.7 NR NR NR
03/23/10 <0.140 <0.190 <0.150 <0.220 4.21 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 9.11 NR NR NR
03/24/11 <0.140 <0.190 <0.150 <0.220 0.363 J <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 NR <100 <100 <100
09/13/11 <0.13 <0.13 <0.15 <0.30 1.3 <0.10 0.40 J <0.11 <0.11 <0.10 <0.10 21.3 NR NR NR
05/29/12 <0.13 <0.13 <0.15 <0.30 1.1 <0.10 <0.10 <0.11 <0.11 <0.10 <0.10 NR NR NR NR
02/25/13 <0.10 <0.10 <0.10 <0.22 18.5 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
10/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/26/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
01/28/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.12 <0.16 <0.16 <0.14 <0.14 NR NR NR NR
08/12/15 <0.17 <0.17 <0.15 <0.43 0.32 J <0.12 0.30 J <0.16 <0.16 <0.14 <0.14 NR NR NR NR
05/21/08 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 6.15 <100 <100 <100
03/09/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <0.55 <1.0 <0.75 <0.70 <0.50 11.0 <100 <100 <100
06/23/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.00 <1.67 <0.330 <0.330 <0.330 6.59 <100 <100 <100
09/23/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 21.0 NR NR NR
12/28/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 19.2 NR NR NR
03/23/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 14.4 NR NR NR
03/24/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 NR <100 <100 <100
09/13/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.11 <0.11 <0.10 <0.10 28.6 NR NR NR
05/29/12 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
05/21/08 <1.0 19.3 <1.0 <3.0 <1.0 <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 43.9 <100 <100 <100
03/09/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <0.55 <1.0 <0.75 <0.70 <0.50 11.1 <100 <100 <100
06/23/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.00 <1.67 <0.330 <0.330 <0.330 10.2 <100 <100 <100
09/23/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 51.5 NR NR NR
12/28/09 <0.140 30.1 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 16.2 NR NR NR
03/23/10 <0.140 4.22 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 7.83 NR NR NR
03/24/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 NR <100 <100 <100
09/13/11 <0.13 21.1 <0.15 <0.30 <0.13 <0.10 <0.10 <0.11 <0.11 <0.10 <0.10 20.7 NR NR NR
05/29/12 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
06/26/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
MW-9
MW-10
MW-11
Page 5 of 10
EPA Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 70 400 400 15 400 700 200
5,000 260,000 80,000 50,000 20,000 6,000 30,500 70,000 26,100 28,500 24,100 15,000 NE NE NELeadMTBETABLE 7
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
H&S TRADING (INCIDENT NO. 10151)
Date : 03/23/21 Facility ID # : 0-009678
Analytical Method
EPA Method 6200B MADEP Method VPH
C5-C8 AliphaticsC9-C12 AliphaticsC9-C10 Aromaticsn-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneMAC (μg/l)
GCL (mg/l)NaphthaleneIsopropylbenzeneIPEContaminant of Concern
BenzeneTolueneEthylbenzeneXylenes05/21/08 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 9.44 <100 <100 <100
03/09/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <0.55 <1.0 <0.75 <0.70 <0.50 12.3 <100 <100 <100
06/23/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.00 <1.67 <0.330 <0.330 <0.330 3.49 <100 <100 <100
09/23/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 27.8 NR NR NR
12/28/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 19.0 NR NR NR
03/23/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 0.767 J 0.309 J 14.9 NR NR NR
03/24/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 NR <100 <100 <100
09/13/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.11 <0.11 <0.10 <0.10 54.7 NR NR NR
05/29/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.11 <0.11 <0.10 <0.10 NR NR NR NR
02/25/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
10/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/26/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
01/28/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.12 <0.16 <0.16 <0.14 <0.14 NR NR NR NR
08/12/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.12 <0.16 <0.16 <0.14 <0.14 NR NR NR NR
02/28/22 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
05/21/08 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 26.8 <100 <100 <100
03/09/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <0.55 <1.0 <0.75 <0.70 <0.50 4.7 <100 <100 <100
06/23/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.00 <1.67 <0.330 <0.330 <0.330 4.39 <100 <100 <100
09/23/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 7.06 NR NR NR
12/28/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 16.9 NR NR NR
03/23/10 <0.140 0.298 J 0.443 J 2.69 <0.250 0.681 J 0.162 J <0.200 0.281 J 3.38 <0.180 8.30 NR NR NR
03/24/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
09/13/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
05/29/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/26/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
05/21/08 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 <1.0 <5.0 <1.0 0.470 I <1.0 80.3 <100 <100 <100
03/09/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <0.55 <1.0 <0.75 <0.70 <0.50 2.2 J <100 <100 <100
06/23/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.00 <1.67 <0.330 <0.330 <0.330 <1.50 <100 <100 <100
09/23/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 11.1 NR NR NR
12/28/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 6.13 NR NR NR
03/23/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 5.78 NR NR NR
03/24/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 NR <100 <100 <100
09/13/11 <0.13 <0.13 <0.15 <0.30 <0.13 0.33 J <0.10 <0.11 <0.11 0.14 J <0.10 <5.0 NR NR NR
05/29/12 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
06/26/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
02/28/22 <0.13 <0.13 <0.13 <0.25 <0.13 0.14 J <0.13 <0.13 <0.13 0.14 J <0.13 NR NR NR NR
MW-12
MW-13
MW-14
Page 6 of 10
EPA Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 70 400 400 15 400 700 200
5,000 260,000 80,000 50,000 20,000 6,000 30,500 70,000 26,100 28,500 24,100 15,000 NE NE NELeadMTBETABLE 7
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
H&S TRADING (INCIDENT NO. 10151)
Date : 03/23/21 Facility ID # : 0-009678
Analytical Method
EPA Method 6200B MADEP Method VPH
C5-C8 AliphaticsC9-C12 AliphaticsC9-C10 Aromaticsn-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneMAC (μg/l)
GCL (mg/l)NaphthaleneIsopropylbenzeneIPEContaminant of Concern
BenzeneTolueneEthylbenzeneXylenes03/09/09 17 <0.70 3.2 J 1.6 J 100 6.0 B 12 <1.0 10 8.1 2.7 J 23.5 <100 240 140
06/23/09 45.3 <0.660 <1.34 10 192 21.8 23.5 <3.34 17.4 4.74 5.96 4.59 569 499 390
09/23/09 28.3 <0.190 7.49 1.09 197 10.6 35.9 0.901 J 46.2 37.0 4.25 22.5 NR NR NR
12/28/09 3.92 <0.190 <0.150 <0.220 94.8 1.32 8.05 0.492 J 4.71 4.92 2.40 32.2 NR NR NR
03/23/10 4.44 <0.190 1.85 26.9 107 6.86 7.59 0.493 J 2.91 44.2 5.26 18.7 NR NR NR
03/24/11 5.79 <0.950 0.835 J <1.10 180 10.4 29.2 <1.00 16.3 26.1 7.95 NR 655 102 420
09/13/11 4.3 <0.13 3.4 3.1 104 8.5 19.9 0.70 10.6 20.8 0.52 16.2 NR NR NR
05/29/12 0.70 <0.13 <0.15 <0.30 40.7 0.28 J 6.1 0.30 J 1.8 1.5 <0.10 NR NR NR NR
02/25/13 1.7 <0.10 <0.10 <0.22 55.9 0.23 J 6.1 0.51 0.70 <0.10 <0.10 NR NR NR NR
10/02/13 5.3 <0.10 0.18 J <0.22 59.8 2.0 24.7 0.81 2.9 0.69 <0.10 NR NR NR NR
06/26/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
08/12/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/09/09 <1.2 <1.4 <1.0 <2.1 <1.0 <1.2 <1.1 <2.0 <1.5 <1.4 <1.0 368 NR NR NR
06/23/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.00 <1.67 <0.330 <0.330 <0.330 22.2 <100 <100 <100
09/23/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 38.6 NR NR NR
12/28/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 416 NR NR NR
03/23/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 23.5 NR NR NR
03/24/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 NR <100 <100 <100
09/13/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.11 <0.11 <0.10 <0.10 85.5 NR NR NR
05/29/12 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
06/26/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
08/12/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/09/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <0.55 <1.0 <0.75 <0.70 <0.50 <3.0 <100 <100 <100
06/23/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.00 <1.67 <0.330 <0.330 <0.330 13.4 <100 <100 <100
09/23/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 29.4 NR NR NR
12/28/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 6.52 NR NR NR
03/23/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 6.61 NR NR NR
03/24/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 NR <100 <100 <100
09/13/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.11 <0.11 <0.10 <0.10 7.7 NR NR NR
05/29/12 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
06/26/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
08/12/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
12/28/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 56.6 <150 <150 <100
03/23/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 25.2 NR NR NR
03/24/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 NR <100 <100 <100
09/13/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.11 <0.11 <0.10 <0.10 25.8 NR NR NR
05/29/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.11 <0.11 <0.10 <0.10 NR NR NR NR
02/25/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
10/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/26/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
01/28/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.12 <0.16 <0.16 <0.14 <0.14 NR NR NR NR
MW-18
MW-15
MW-16
MW-17
Page 7 of 10
EPA Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 70 400 400 15 400 700 200
5,000 260,000 80,000 50,000 20,000 6,000 30,500 70,000 26,100 28,500 24,100 15,000 NE NE NELeadMTBETABLE 7
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
H&S TRADING (INCIDENT NO. 10151)
Date : 03/23/21 Facility ID # : 0-009678
Analytical Method
EPA Method 6200B MADEP Method VPH
C5-C8 AliphaticsC9-C12 AliphaticsC9-C10 Aromaticsn-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneMAC (μg/l)
GCL (mg/l)NaphthaleneIsopropylbenzeneIPEContaminant of Concern
BenzeneTolueneEthylbenzeneXylenes03/24/11 63.7 <9.50 63.6 484 1,790 513 28.3 J <10.0 53.2 743 200 NR 4,030 186,000 422,000
09/13/11 43.0 9.5 J 69.9 444 1,460 253 20.3 J 6.0 J 38.0 429 124 53.3 NR NR NR
05/29/12 97.5 68.8 1,650 10,700 1,930 4,150 747 <11 1,560 9,620 4,240 NR NR NR NR
02/25/13 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
10/02/13 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
06/26/14 21.5 0.44 J 21.8 86.9 611 50.2 6.0 2.8 10.4 97.4 26.4 NR NR NR NR
01/28/15 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
08/12/15 48.4 <0.17 47.9 87.9 1,490 41.2 27.2 7.1 29.3 260 46.9 NR NR NR NR
02/23/16 7.7 0.23 J 134 262 102 42.1 27.7 0.64 211 248 269 NR NR NR NR
11/21/16 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
07/20/17 3.8 <0.31 18.8 33.6 76.1 84.2 8.1 1.1 J 13.1 149 15.2 NR NR NR NR
05/04/18 3.9 <0.13 18.9 31.3 185 95.7 NR 5.2 NR NR NR NR NR NR NR
06/11/18 1.4 J <0.63 4.2 8.1 209 129 7.3 3.5 14.6 93.5 19.7 NR NR NR NR
02/04/19 5.5 <1.3 16.1 18.0 97.4 112 16.3 5.9 26.7 178 31.7 NS NS NS NS
08/06/19 4.2 <0.13 14.7 20.3 140 194 20.8 6.4 34.8 263 39.7 NS NS NS NS
02/18/20 4.0 J <1.3 12.6 17.1 242 139 28.5 7.2 49.6 293 <1.3 NS NS NS NS
10/21/20 4.6 J <1.3 3.6 J 2.6 J 458 100 15.3 9.5 25.6 129 18.9 NR NR NR NR
02/28/22 5.7 <0.13 7.3 2.1 330 64.1 17.1 9.5 21.4 69.2 10.6 NR NR NR NR
03/24/11 <0.140 <0.190 <0.150 <0.220 2.88 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 NR <100 <100 <100
09/13/11 <0.13 <0.13 <0.15 <0.30 1.3 <0.10 <0.10 <0.11 <0.11 <0.10 <0.10 64.8 NR NR NR
05/29/12 <0.13 <0.13 <0.15 <0.30 0.40 J <0.10 <0.10 <0.11 <0.11 <0.10 <0.10 NR NR NR NR
02/25/13 <0.10 <0.10 <0.10 <0.22 16.8 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
10/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/26/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/24/11 <0.140 1.29 <0.150 <0.220 4.18 <0.500 <0.150 <0.200 <0.220 0.172 J <0.180 NR <100 <100 <100
09/13/11 <0.13 <0.13 <0.15 <0.30 0.84 <0.10 <0.10 <0.11 <0.11 <0.10 <0.10 18.3 NR NR NR
05/29/12 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
08/12/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.12 <0.16 <0.16 <0.14 <0.14 NR NR NR NR
03/24/11 4.62 <0.190 0.917 J 0.612 J 573 1.60 0.908 J 2.55 0.489 J 0.759 J <0.180 NR 224 <100 <100
09/13/11 14.9 J <6.4 11.5 J 59.6 1,260 26.5 <5.0 6.9 J 6.8 J 112 40.8 <5.0 NR NR NR
05/29/12 7.7 <1.3 4.3 J 10.1 J 748 9.0 1.2 J 4.1 J 1.5 J 12.5 2.5 J NR NR NR NR
02/25/13 0.99 <0.10 0.66 0.75 J 381 3.0 0.97 3.2 1.4 1.7 0.32 J NR NR NR NR
10/02/13 18.1 <0.10 4.7 3.8 1,300 11.7 5.6 7.3 7.3 8.6 1.5 NR NR NR NR
06/26/14 1.8 J <1.0 2.3 J 7.3 J 271 17.5 1.6 J 4.7 2.4 J 27.7 8.7 NR NR NR NR
01/28/15 <0.17 <0.17 <0.15 <0.43 153 <0.12 <0.12 2.2 <0.16 <0.14 <0.14 NR NR NR NR
08/12/15 1.4 <0.17 0.29 J 1.5 281 6.7 2.0 5.1 2.3 7.4 1.4 NR NR NR NR
02/28/22 0.32 J <0.13 <0.13 <0.25 7.1 2.9 2.6 7.9 1.0 1.2 0.16 J NR NR NR NR
MW-20
RW-1
MW-19
RW-1A
Page 8 of 10
EPA Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 70 400 400 15 400 700 200
5,000 260,000 80,000 50,000 20,000 6,000 30,500 70,000 26,100 28,500 24,100 15,000 NE NE NELeadMTBETABLE 7
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
H&S TRADING (INCIDENT NO. 10151)
Date : 03/23/21 Facility ID # : 0-009678
Analytical Method
EPA Method 6200B MADEP Method VPH
C5-C8 AliphaticsC9-C12 AliphaticsC9-C10 Aromaticsn-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneMAC (μg/l)
GCL (mg/l)NaphthaleneIsopropylbenzeneIPEContaminant of Concern
BenzeneTolueneEthylbenzeneXylenes03/24/11 78.6 2.93 J 9.80 94.8 3,430 55.1 3.70 J 13.7 4.01 J 101 23.5 NR 1,690 1,190 809
09/13/11 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
05/29/12 51.9 <6.4 <7.3 15.2 J 2,830 6.6 J <5.0 14.5 J <5.4 11.8 J <5.0 NR NR NR NR
02/25/13 4.3 J <1.0 1.3 J 6.1 J 242 16.8 <1.0 10.9 <1.0 20.8 7.0 NR NR NR NR
10/02/13 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
06/26/14 44.3 4.7 J 5.9 J 23.8 969 17.9 <2.0 14.1 <2.0 33.8 27.3 NR NR NR NR
01/28/15 5.7 <1.7 <1.5 4.3 J 345 4.8 J <1.2 11.4 <1.6 6.5 9.4 NR NR NR NR
11/21/16 8.8 <0.13 1.0 4.2 43.2 5.9 0.61 7.7 0.58 8.5 6.0 NR NR NR NR
07/20/17 3.8 <0.13 <0.13 <0.25 84.8 1.9 0.14 J 7.8 <0.13 0.80 0.40 J NR NR NR NR
06/11/18 0.96 J <0.25 <0.25 <0.50 76.3 1.4 <0.25 7.4 <0.25 <0.25 <0.25 NR NR NR NR
02/04/19 4.2 <0.63 0.70 J 5.8 J 68.5 8.9 1.4 J 11.6 1.2 J 20.4 18.5 NS NS NS NS
08/06/19 5.0 <0.13 <0.13 2.7 128 9.2 1.0 14.0 0.99 16.6 11.7 NS NS NS NS
02/18/20 1.6 <0.31 <0.31 1.3 J 118 4.2 0.58 J 11.2 0.56 J 9.8 9.2 NS NS NS NS
10/21/20 24.5 <1.3 <1.3 <2.5 357 11.9 <1.3 15.6 <1.3 7.4 5.8 NR NR NR NR
02/28/22 0.32 J <0.13 <0.13 <0.25 7.1 2.9 2.6 7.9 1.0 1.2 0.16 J NR NR NR NR
03/24/11 <0.280 <0.380 <0.300 <0.440 18.2 <1.00 <0.300 0.552 J <0.440 0.354 J <0.360 NR <100 <100 <100
09/13/11 18.3 <0.13 9.2 <0.30 151 1.4 8.4 1.6 15.8 <0.10 <0.10 10.6 NR NR NR
05/29/12 0.38 J <0.13 <0.15 <0.30 4.1 <0.10 0.13 J 0.25 J <0.11 <0.10 <0.10 NR NR NR NR
02/25/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/26/14 <0.10 <0.10 <0.10 <0.20 2.7 <0.10 <0.10 0.34 J <0.10 <0.10 <0.10 NR NR NR NR
01/28/15 <0.17 <0.17 <0.15 <0.43 0.86 <0.12 0.20 J 0.28 J <0.16 <0.14 <0.14 NR NR NR NR
08/12/15 <0.17 <0.17 <0.15 <0.43 2.2 <0.12 <0.12 <0.16 <0.16 <0.14 <0.14 NR NR NR NR
03/24/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
09/13/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
05/29/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/24/11 3.06 <0.190 0.724 J 2.22 26.2 0.614 J 0.536 J 4.21 0.628 J 2.83 0.512 J NR 124 <100 <100
09/13/11 29.9 <0.13 4.6 4.32 J 293 4.5 5.7 6.3 4.7 13.1 1.0 6.7 NR NR NR
05/29/12 7.8 <0.13 <0.15 <0.30 132 0.12 J 0.68 5.4 <0.11 0.12 J <0.10 NR NR NR NR
02/25/13 <0.10 <0.10 <0.10 <0.22 1.2 <0.15 <0.10 2.5 <0.10 <0.10 <0.10 NR NR NR NR
10/02/13 141 94.1 390 1,650 1,440 97.4 30.6 6.5 48.5 458 88.6 NR NR NR NR
06/26/14 <0.10 <0.10 <0.10 <0.20 3.3 <0.10 <0.10 3.2 <0.10 <0.10 <0.10 NR NR NR NR
01/28/15 0.34 J <0.17 <0.15 <0.43 4.0 <0.12 0.25 J 2.7 <0.16 <0.14 <0.14 NR NR NR NR
08/12/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.12 1.9 <0.16 <0.14 <0.14 NR NR NR NR
03/24/11 <0.140 <0.190 <0.150 <0.220 1.26 <0.500 <0.150 <0.200 <0.220 <0.150 <0.180 NR <100 <100 <100
09/13/11 <0.13 <0.13 <0.15 <0.30 0.31 J <0.10 <0.10 <0.11 <0.11 <0.10 <0.10 <5.0 NR NR NR
05/29/12 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
03/24/11 1.25 <0.190 <0.150 <0.220 89.8 <0.500 <0.150 0.923 J <0.220 <0.150 <0.180 NR <100 <100 <100
09/13/11 <0.13 <0.13 <0.15 <0.30 1.3 0.65 <0.10 0.38 J <0.11 0.27 J <0.10 5.3 NR NR NR
05/29/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
05/29/12 <0.13 <0.13 <0.15 <0.30 10.6 <0.10 <0.10 0.24 J <0.11 <0.10 <0.10 NR NR NR NR
02/25/13 6.6 <0.10 <0.10 <0.22 461 1.3 0.17 J 2.4 <0.10 0.12 J <0.10 NR NR NR NR
10/02/13 0.15 J <0.10 0.11 J 0.21 J 308 0.84 <0.10 1.7 <0.10 0.14 J <0.10 NR NR NR NR
06/26/14 0.28 J <0.10 <0.10 <0.20 10.7 <0.10 <0.10 0.15 J <0.10 <0.10 <0.10 NR NR NR NR
01/28/15 <0.17 <0.17 <0.15 <0.43 0.52 <0.12 <0.12 0.31 J <0.16 <0.14 <0.14 NR NR NR NR
RW-3
RW-4
RW-5
RW-6
RW-8
RW-2
Page 9 of 10
EPA Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 70 400 400 15 400 700 200
5,000 260,000 80,000 50,000 20,000 6,000 30,500 70,000 26,100 28,500 24,100 15,000 NE NE NELeadMTBETABLE 7
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
H&S TRADING (INCIDENT NO. 10151)
Date : 03/23/21 Facility ID # : 0-009678
Analytical Method
EPA Method 6200B MADEP Method VPH
C5-C8 AliphaticsC9-C12 AliphaticsC9-C10 Aromaticsn-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneMAC (μg/l)
GCL (mg/l)NaphthaleneIsopropylbenzeneIPEContaminant of Concern
BenzeneTolueneEthylbenzeneXylenes02/23/16 <0.13 <0.13 <0.13 <0.31 <0.13 48.3 <0.13 <0.13 0.22 J 2.4 0.41 J NR NR NR NR
03/07/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
11/21/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
WSW-32 02/28/22 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
06/26/14 <0.10 <0.10 <0.10 <0.20 0.56 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
01/28/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.12 <0.16 <0.16 <0.14 <0.14 NR NR NR NR
02/28/22 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
TMW-1 02/28/22 0.61 J <0.31 1.5 13.4 115 29.4 1.4 0.74 J 2.3 58.5 20.3 NR NR NR NR
TMW-2 03/02/22 30.6 <3.1 97.5 493 2,650 19.0 4.6 J 11.1 J 19.2 220 92.5 NR NR NR NR
Trip Blank 02/28/22 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
Notes:
• Results reported in µg/l (micrograms per liter).
• MAC: Maximum Allowable Concentration as specified in T15A NCAC 2L.0202.
• GCL: Gross contamination level.
• NE: Standard not established.
• FP: Free product.
• <: Less than the method detection limit specified in the laboratory report.
• Concentrations in bold face type exceeded the 2L Standard.
• I or J: Estimated value.
• Concentrations of n-butylbenzene, sec-butylbenzene and p-isopropyltoluene that exceeded the MACs were reported in the ground water samples collected from MW-1 on 03/02/22.
• NS: Not requested.
• V or B: Present in laboratory blank.
• E: Indicates value exceeds calibration range.
• NS: Not sampled.
• For other compounds reported which did not exceed the 2L Standards, refer to the laboratory reports.
WSW-34
WSW-12
Page 10 of 10
Well No.Sampled Date
(mm/dd/yy)
DO
(mg/L)Temp (oC)pH ORP
(mv)
Methane
(μg/L)
Nitrate
(μg/L)
Sulfate
(μg/L)
Ferrous Iron
(μg/L)
MW-1 01/05/22 5.97 15.82 7.24 ---767 340 5,500 9,500
MW-2 01/05/22 4.47 15.76 7.22 115.1 95.3 120 12,000 110
MW-3 01/05/22 2.30 15.7 7.06 116.3 485 220 3,400 590
MW-5 01/05/22 2.53 16.59 7.09 113.2 351 <100 <2,000 4,100
MW-6 01/05/22 1.75 15.68 7.11 116.1 839 <100 <2,000 6,900
MW-12 01/05/22 6.61 15.50 7.11 115.8 1.1 <100 9,400 <500
MW-19 01/05/22 3.01 16.44 7.08 114.7 6,140 <100 <2,000 6,500
Notes:
Method SM 3500 Fe-D. Field measurements of dissolved oxygen, temperature, pH and ORP were collected during sampling using a field
• NS: Not sampled; Low sample volume prohibited parameters being collected.
TABLE 7A
SUMMARY OF NATURAL ATTENUATION PARAMETER RESULTS
H&S TRADING (INCIDENT NO. 10151)
Date: 04/5/2022 Facility ID # : 0-009678
• Analyses for nitrate and sulfate by Method SW846/9056; analyses for methane by Method RSK 175; analyses for ferrous iron by EPA
meter.
• <: Less than the method detection limit specified in the laboratory report.
• J: Estimated concentration.
• NR: Not requested.
• FP: Free Product.

APPENDICES

APPENDIX A
State Correspondence
2632 Received JAN 2902021
2632 Received FEB 15 2022

APPENDIX B
Subsurface Logs

Geological Resources, Inc.Phone:[phone]
3502 Hayes Road Fax:[phone]
Monroe, NC 28110
SUBSURFACE LOG
Project H&S Trading
Address 211 Tunis Road, Tunis, NC
Boring Number TMW-1 Date Drilled
Sample Method Grab Drilling Method 6" Solid Stem
Completion DetailsWell installed at completion to a total depth of 30 feet with a 20 foot screened interval
Driller Justin Radford (GRI)Log By AJ Discepolo
Lab Sample OVA
Depth Sample Interval(ft)ppm LITHOLOGY
0
2 2
4 4
6 6
8 8
10 10

12 12
14 14
16 16

18 18
20 20
22 Grain Size 22

24 24
26 26
28 28

30 Grain Size 30
32
34

36
Boring terminated at 30'; abandoned with bentonite and
soil cuttings upon sample collection.
20' - 25'; Gray clay
25' - 30'; Gray clay
15' - 20'; Course sand (wet)
5' - 10'; Course sand
10' -15'; Course sand (wet)
02/28/22
0 - 5'; Brown silt
Geological Resources, Inc.Phone:[phone]
3502 Hayes Road Fax:[phone]
Monroe, NC 28110
SUBSURFACE LOG
Project H&S Trading
Address 211 Tunis Road, Tunis, NC
Boring Number TMW-2 Date Drilled
Sample Method Grab Drilling Method 6" Solid Stem
Completion DetailsWell installed at completion to a total depth of 30 feet with a 20 foot screened interval
Driller Justin Radford (GRI)Log By AJ Discepolo
Lab Sample OVA
Depth Sample Interval(ft)ppm LITHOLOGY
0
2 2
4 4
6 6
8 8
10 10

12 12
14 14
16 16

18 18
20 20
22 Grain Size 22

24 24
26 26
28 28

30 Grain Size 30
32
34

36
02/28/22
0 - 5'; Brown silt
15' - 20'; Course sand
5' - 10'; Tan silty sand
10' -12'; Gray silty sand
12' - 15'; Tan course sand
20' - 25'; Gray clay
25' - 30'; Gray clay
Boring terminated at 30'; abandoned with bentonite and
soil cuttings upon sample collection.

APPENDIX C
UVF Report – Soil Samples

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
Engineering Certification: C-2727 • Geology Certification: C-127
UVF Trilogy Analytical Report

Samples Collected: February 28, 2022
Samples Analyzed: March 2, 2022
Site Name: H & S Trading
Site Address: 211 Tunis Road, Tunis, NC
GRI Project Number: 2632

March 2, 2022

Ethan Rogerson, GIT
Operator

Technical Procedures
Sample Collection and Handling
Soil samples may be collected using any acceptable procedure. Sampler must use a clean pair of nitrile
gloves for each sample collected. The sample will be placed in a clean, sealable bag (ziplock). Once
collected, the sample must be analyzed immediately or placed on ice. The sample may be kept on ice for
up to 48 hours prior to UVF analyses. If the sample cannot be analyzed within 48 hours, the sample may
be extracted and kept at 4 degrees C for up to 14 days. Proper chain-of-custody procedures must be
followed.
Calibration
The UFV Trilogy has standard calibrations stored for the following analysis:
 GRO
 DRO
 Total PAH
 Target PAH
 Heavy PAH
Prior to use, calibration standards are used to perform a 5-point verification on the factory stored
calibrations for GRO and DRO. The calibration standards used are as follows:
GRO
 0.5 ppm
 1 ppm
 3 ppm
 5 ppm
 10 ppm
DRO
 0.1 ppm
 0.5 ppm
 1 ppm
 3 ppm
 5 ppm
Operation
Sample Extraction
 5mg of soil are weighed into a clean extraction jar
 Methanol is added to the extraction jar to create a 2x or 4x dilution
o 2x Dilution: 10 mL of methanol
o 4x Dilution: 20 mL of methanol
 The extraction jar is shaken for several minutes to thoroughly mix the soil with solvent
(methanol)
 The mixture is allowed to settle for several minutes
 A clean syringe is used to draw liquid from the extraction jar
 A clean filter is attached to the end of the syringe and the liquid dispensed through the filter
into a clean test tube
 This liquid is referred to as the extraction
Dilution Preparation
 An adjustable micropipette is used to precisely measure out the amount of extract needed for
the dilution
Technical Procedures
 The measured out amount of the extract is added to a clean test tube and methanol is added
dilute the extract. Examples of dilutions are shown below:

Extract Amount
500 μL
200 μL
100 μL
50 μL
25 μL

Add Solvent to the
5 mL line
5 mL line
5 mL line
5 mL line
5 mL line
2x Extract
Dilution Factor
20x
50x
100x
200x
400x
4x Extract
Dilution Factor
40x
100x
200x
400x
800x

Sample Analyzation
 The dilution is shaken to thoroughly mix, then poured into a clean glass cuvette
 The desired module is inserted into the UVF Trilogy and the corresponding factory calibration is
selected
 “Measure Fluorescence” is pressed on the touchscreen and the reading is recorded
 The reading should be between the concentrations of the calibration standards (GRO: 0.5-10
ppm; DRO 0.1-5 ppm)
o Reading below the calibration standard range are recorded as below the detection limit
 Detection Limit = (lower range of calibration standards range) x dilution factor
(i.e. a GRO sample with a 100x dilution factor has a detection limit of 50 ppm)
o Readings above the calibration standard range should be further diluted and reanalyzed
o Negative readings are an indication of quenching (see below)
 The reading is multiplied by the dilution factor to calculate the final concentration
 Check suspected contaminated samples for quenching by running additional dilutions
o According to the siteLAB Quick Reference Guide:
“Quenching” can occur when the detector is swamped by too many hydrocarbons or
organic interferences, producing low or negative concentrations. Test the sample at
multiple dilutions to confirm results are linear and accurate.”
QA/QC
Calibration
 The UFV Trilogy will be calibrated daily prior to use
 The calibration results will be saved and entered into the calibration log
Method Blank
 A method blank of methanol will be analyzed following calibration and following the last sample
analyzed for each site
Duplicates
 One duplicate will be analyzed for every 20 samples
 The duplicate will be prepared from the extract of the sample and diluted to the same factor as
the sample analyzed
Project Name:Date Collected:
Project Number:Date Analyzed:
Project Manager:Sampler:
Sample ID Matrix Dilution
Factor x
GRO
Output
(ppm)
=GRO Value
(mg/Kg)
Dilution
Factor x
DRO
Output
(ppm)
=DRO Value
(mg/Kg)
TMW-1-2 Soil 4 0.36 <2 4 0.4 1.6
TMW-1-4 Soil 4 0.29 <2 4 0.32 1.28
TMW-1-6 Soil 4 0.3 <2 4 0.32 1.28
TMW-1-8 Soil 4 0.36 <2 4 0.33 1.32
TMW-1-10 Soil 100 1.72 172 100 0.42 42
TMW-1-12 Soil 100 1.79 179 100 0.45 45
TMW-1-14 Soil 100 1.82 182 100 0.48 48
TMW-1-16 Soil 100 1.88 188 100 0.58 58
TMW-1-18 Soil 100 2.43 243 100 0.73 73
TMW-1-20 Soil 100 1.29 129 100 0.57 57
TMW-1-22 Soil 100 1.55 155 100 0.39 39
TMW-1-24 Soil 100 0.45 <50 100 0.05 <10
TMW-1-26 Soil 4 0.5 2 4 0.5 2
TMW-1-28 Soil 4 4.85 19.4 4 2.18 8.72
TMW-1-30 Soil 100 1.37 137 100 0.43 43
Dup TMW-1-26 Soil 4 0.47 <2 4 0.5 2
TMW-2-2 Soil 4 0.39 <2 4 0.42 1.68
TMW-2-4 Soil 4 0.35 <2 4 0.39 1.56
TMW-2-6 Soil 4 1.09 4.36 4 0.68 2.72
TMW-2-8 Soil 100 10.91 1091 100 3.81 381
TMW-2-10 Soil 100 0.25 25 100 0.04 <10
TMW-2-12 Soil 100 4.05 405 100 1.25 125
TMW-2-14 Soil 100 3.64 364 100 1.23 123
TMW-2-16 Soil 100 0.42 <50 100 0.44 44
TMW-2-18 Soil 100 0.46 <50 100 0.15 15
TMW-2-20 Soil 100 3.16 316 100 1.28 128
TMW-2-22 Soil 100 0.93 93 100 0.37 37
TMW-2-24 Soil 100 0.36 <50 100 0.13 13
TMW-2-26 Soil 4 3.85 15.4 4 2.27 9.08
TMW-2-28 Soil 4 1.58 6.32 4 1.22 4.88
TMW-2-30 Soil 4 0.86 3.44 4 0.77 3.08
UVF Analytical Report
siteLAB UVF Trilogy
3/2/2022
2/28/2022
AJ Discepolo
H & S Trading
2632
Ethan Rogerson
Site:
H S Trading
Report Date:
03/02/2022
Page:
1 of 1

APPENDIX D
Laboratory Report – Ground Water
03/23/22
Technical Report for
GRI (Geological Resources Inc.)
H&S Trading; 211 Tunis Rd, Tunis, NC
10151/2632
SGS Job Number: FA93495
Sampling Date: 02/28/22
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
[e-mail]; [e-mail];
[e-mail]; [e-mail]
ATTN: William Regenthall
Total number of pages in report:
Certifications: FL(E83510), LA(03051), KS(E-10327), NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AL, AK, AR, CT, IA, KY, MA, MI. MS, ND, NH, NV, OK, OR, IL, UT, VT, WA, WI, WV
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone]
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Norm Farmer
Technical Director
Orlando, FL 03/23/22
e-Hardcopy 2.0
Automated Report
97
SGS is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
Review standard terms at: http://www.sgs.com/en/terms-and-conditions
The results set forth herein are provided by SGS North America Inc.
Please share your ideas about
how we can serve you better at:
[e-mail]
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FA93495
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Case Narrative/Conformance Summary ..............................................................5
Section 3: Summary of Hits ....................................................................................................8
Section 4: Sample Results ........................................................................................................14
4.1: FA93495-1: MW-1 ........................................................................................................15
4.2: FA93495-2: MW-2 ........................................................................................................20
4.3: FA93495-3: MW-3 ........................................................................................................24
4.4: FA93495-4: MW-6 ........................................................................................................28
4.5: FA93495-5: MW-12 ......................................................................................................32
4.6: FA93495-6: MW-19 ......................................................................................................36
4.7: FA93495-7: MW-5 ........................................................................................................40
4.8: FA93495-8: MW-14 ......................................................................................................44
4.9: FA93495-9: TMW-1 .....................................................................................................46
4.10: FA93495-10: TRIP BLANK .......................................................................................48
4.11: FA93495-11: RW-1A ..................................................................................................50
4.12: FA93495-12: RW-2 .....................................................................................................52
4.13: FA93495-13: WSW-34 ...............................................................................................54
4.14: FA93495-14: WSW-32 ...............................................................................................56
4.15: FA93495-15: TMW-1-22 ............................................................................................58
4.16: FA93495-16: TMW-1-30 ............................................................................................59
4.17: FA93495-17: TMW-2-22 ............................................................................................60
4.18: FA93495-18: TMW-2-30 ............................................................................................61
Section 5: Misc. Forms ............................................................................................................62
5.1: Chain of Custody ...........................................................................................................63
Section 6: MS Volatiles - QC Data Summaries .....................................................................66
6.1: Method Blank Summary ................................................................................................67
6.2: Blank Spike Summary ...................................................................................................71
6.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................75
Section 7: GC Volatiles - QC Data Summaries .....................................................................79
7.1: Method Blank Summary ................................................................................................80
7.2: Blank Spike/Blank Spike Duplicate Summary ..............................................................82
7.3: Matrix Spike Summary ..................................................................................................84
7.4: Duplicate Summary .......................................................................................................86
Section 8: General Chemistry - QC Data Summaries ..........................................................88
8.1: Method Blank and Spike Results Summary ..................................................................89
8.2: Duplicate Results Summary ..........................................................................................90
8.3: Matrix Spike Results Summary .....................................................................................91
8.4: Matrix Spike Duplicate Results Summary ....................................................................92
Section 9: Misc. Forms (SGS Dayton, NJ) .............................................................................93
9.1: Chain of Custody ...........................................................................................................94
Section 10: General Chemistry - QC Data (SGS Dayton, NJ) .............................................96
10.1: Duplicate Results Summary ........................................................................................97 123456789102 of 97
FA93495
SGS North America Inc.
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA93495
H&S Trading; 211 Tunis Rd, Tunis, NC
Project No: 10151/2632
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
This report contains results reported as ND = Not detected. The following applies:
Organics ND = Not detected above the MDL
FA93495-1 02/28/22 12:33 JBAD 03/01/22 AQ Ground Water MW-1
FA93495-2 02/28/22 12:44 JBAD 03/01/22 AQ Ground Water MW-2
FA93495-3 02/28/22 13:24 JBAD 03/01/22 AQ Ground Water MW-3
FA93495-4 02/28/22 13:45 JBAD 03/01/22 AQ Ground Water MW-6
FA93495-5 02/28/22 13:51 JBAD 03/01/22 AQ Ground Water MW-12
FA93495-6 02/28/22 14:14 JBAD 03/01/22 AQ Ground Water MW-19
FA93495-7 02/28/22 14:20 JBAD 03/01/22 AQ Ground Water MW-5
FA93495-8 02/28/22 14:43 JBAD 03/01/22 AQ Ground Water MW-14
FA93495-9 02/28/22 14:48 JBAD 03/01/22 AQ Ground Water TMW-1
FA93495-10 02/28/22 08:26 JBAD 03/01/22 AQ Trip Blank Water TRIP BLANK
FA93495-11 02/28/22 15:04 JBAD 03/01/22 AQ Ground Water RW-1A
FA93495-12 02/28/22 15:23 JBAD 03/01/22 AQ Ground Water RW-2
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
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FA934951
SGS North America Inc.
Sample Summary
(continued)
GRI (Geological Resources Inc.)
Job No:FA93495
H&S Trading; 211 Tunis Rd, Tunis, NC
Project No: 10151/2632
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA93495-13 02/28/22 15:24 JBAD 03/01/22 AQ Ground Water WSW-34
FA93495-14 02/28/22 15:34 JBAD 03/01/22 AQ Ground Water WSW-32
FA93495-15 02/28/22 11:18 JBAD 03/01/22 SO Soil TMW-1-22
FA93495-16 02/28/22 11:23 JBAD 03/01/22 SO Soil TMW-1-30
FA93495-17 02/28/22 11:41 JBAD 03/01/22 SO Soil TMW-2-22
FA93495-18 02/28/22 11:47 JBAD 03/01/22 SO Soil TMW-2-30
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
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SAMPLE DELIVERY GROUP CASE NARRATIVE
Client: GRI (Geological Resources Inc.) Job No: FA93495
Site: H&S Trading; 211 Tunis Rd, Tunis, NC Report Date 3/23/2022 1:40:47 PM

On 03/01/2022, 17 Sample(s), 1 Trip Blank(s) and 0 Field Blank(s) were received at SGS North America Inc - Orlando. at a
maximum corrected temperature of 3.4 C. Samples were intact and chemically preserved, unless noted below. A SGS North America
Inc. - Orlando Job Number of FA93495 was assigned to the project. Laboratory sample ID, client sample ID and dates of sample
collection are detailed in the report’s Results Summary Section. Specified quality control criteria were achieved for this job except as noted
below. For more information, please refer to the analytical results and QC summary pages.

MS Volatiles By Method SM 6200B Matrix: AQ Batch ID: VA3083
Sample(s) FA93495-12MS, FA93495-12MSD were used as the QC samples indicated.
Sample(s) FA93495-1 have compounds reported with “E” qualifiers indicating estimated value exceeding calibration range. Matrix Spike Recovery(s) for Chloroethane, Methyl Bromide, Trichlorofluoromethane are outside control limits. Probable cause is due to matrix interference.
Matrix Spike Duplicate Recovery(s) for Methyl Tert Butyl Ether are outside control limits. Probable cause is due to matrix interference.
RPD(s) for MSD for Chloroethane, Methyl Bromide, Trichlorofluoromethane are outside control limits for sample FA93495-12MSD. Probable cause is due to sample non-homogeneity.
FA93495-1 for 1,2,4-Trimethylbenzene: No sample available for reanalysis. FA93495-1 for Bromoform: Associated CCV outside of control limits high, sample was ND.
FA93495-1: Results from different vials are not consistent; higher results were reported.
FA93495-3 for Bromoform: Associated CCV outside of control limits high, sample was ND.
FA93495-4 for Bromoform: Associated CCV outside of control limits high, sample was ND.
FA93495-5 for Bromoform: Associated CCV outside of control limits high, sample was ND. FA93495-6 for Bromoform: Associated CCV outside of control limits high, sample was ND.
FA93495-7 for Bromoform: Associated CCV outside of control limits high, sample was ND. FA93495-8 for Bromoform: Associated CCV outside of control limits high, sample was ND.
FA93495-9 for Bromoform: Associated CCV outside of control limits high, sample was ND. FA93495-10 for Bromoform: Associated CCV outside of control limits high, sample was ND.
FA93495-11 for Bromoform: Associated CCV outside of control limits high, sample was ND. FA93495-12 for Bromoform: Associated CCV outside of control limits high, sample was ND.
FA93495-13 for Bromoform: Associated CCV outside of control limits high, sample was ND. FA93495-14 for Bromoform: Associated CCV outside of control limits high, sample was ND.
Matrix: AQ Batch ID: VA3087
Sample(s) FA93619-3MS, FA93619-3MSD were used as the QC samples indicated. Matrix Spike Recovery(s) for 1,1-Dichloropropene, 1,3,5-Trimethylbenzene, Isopropylbenzene, m,p-Xylene, n-Propylbenzene, o-Xylene, p-Isopropyltoluene, sec-Butylbenzene, tert-Butylbenzene, Xylene (total) are outside control limits. Probable cause is due to matrix interference.
Sample(s) FA93495-1 have surrogates outside control limits.
FA93495-1: Results from different vials are not consistent; higher results were reported.
GC Volatiles By Method RSKSOP-147/175 Matrix: AQ Batch ID: G1R284
Sample(s) FA93558-4DUP, FA93558-4MS were used as the QC samples indicated.
RPD(s) for Duplicate for Methane are outside control limits for sample FA93558-4DUP. Probable cause is due to sample non-homogeneity.
Matrix: AQ Batch ID: GLL2694
Sample(s) FA93495-1DUP, FA93495-2MS were used as the QC samples indicated.
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General Chemistry By Method ASTM D422-63
Matrix: SO Batch ID: N:GP38862 FA93495-15 for % Gravel: Analysis performed at SGS Dayton, NJ.
FA93495-15 for % Sand: Analysis performed at SGS Dayton, NJ. FA93495-15 for % Silt, Clay, Colloids: Analysis performed at SGS Dayton, NJ.
FA93495-15 for 0.0015 mm (Hydrometer): Analysis performed at SGS Dayton, NJ. FA93495-15 for 0.005 mm (Hydrometer): Analysis performed at SGS Dayton, NJ.
FA93495-15 for 0.030 mm (Hydrometer): Analysis performed at SGS Dayton, NJ. FA93495-15 for 0.375 Inch Sieve: Analysis performed at SGS Dayton, NJ.
FA93495-15 for 0.75 Inch Sieve: Analysis performed at SGS Dayton, NJ. FA93495-15 for 1.5 Inch Sieve: Analysis performed at SGS Dayton, NJ.
FA93495-15 for 3 Inch Sieve: Analysis performed at SGS Dayton, NJ. FA93495-15 for No.10 Sieve (2.00 mm): Analysis performed at SGS Dayton, NJ.
FA93495-15 for No.100 Sieve (0.15 mm): Analysis performed at SGS Dayton, NJ.
FA93495-15 for No.16 Sieve (1.18 mm): Analysis performed at SGS Dayton, NJ.
FA93495-15 for No.200 Sieve (0.075 mm): Analysis performed at SGS Dayton, NJ.
FA93495-15 for No.30 Sieve (0.60 mm): Analysis performed at SGS Dayton, NJ.
FA93495-15 for No.4 Sieve (4.75 mm): Analysis performed at SGS Dayton, NJ.
FA93495-15 for No.50 Sieve (0.30 mm): Analysis performed at SGS Dayton, NJ. FA93495-15 for No.8 Sieve (2.36 mm): Analysis performed at SGS Dayton, NJ.
FA93495-16 for % Gravel: Analysis performed at SGS Dayton, NJ. FA93495-16 for % Sand: Analysis performed at SGS Dayton, NJ.
FA93495-16 for % Silt, Clay, Colloids: Analysis performed at SGS Dayton, NJ. FA93495-16 for 0.0015 mm (Hydrometer): Analysis performed at SGS Dayton, NJ.
FA93495-16 for 0.005 mm (Hydrometer): Analysis performed at SGS Dayton, NJ. FA93495-16 for 0.030 mm (Hydrometer): Analysis performed at SGS Dayton, NJ.
FA93495-16 for 0.375 Inch Sieve: Analysis performed at SGS Dayton, NJ.
FA93495-16 for 0.75 Inch Sieve: Analysis performed at SGS Dayton, NJ.
FA93495-16 for 1.5 Inch Sieve: Analysis performed at SGS Dayton, NJ.
FA93495-16 for 3 Inch Sieve: Analysis performed at SGS Dayton, NJ.
FA93495-16 for No.10 Sieve (2.00 mm): Analysis performed at SGS Dayton, NJ.
FA93495-16 for No.100 Sieve (0.15 mm): Analysis performed at SGS Dayton, NJ. FA93495-16 for No.16 Sieve (1.18 mm): Analysis performed at SGS Dayton, NJ.
FA93495-16 for No.200 Sieve (0.075 mm): Analysis performed at SGS Dayton, NJ. FA93495-16 for No.30 Sieve (0.60 mm): Analysis performed at SGS Dayton, NJ.
FA93495-16 for No.4 Sieve (4.75 mm): Analysis performed at SGS Dayton, NJ. FA93495-16 for No.50 Sieve (0.30 mm): Analysis performed at SGS Dayton, NJ.
FA93495-16 for No.8 Sieve (2.36 mm): Analysis performed at SGS Dayton, NJ. FA93495-17 for % Gravel: Analysis performed at SGS Dayton, NJ.
FA93495-17 for % Sand: Analysis performed at SGS Dayton, NJ.
FA93495-17 for % Silt, Clay, Colloids: Analysis performed at SGS Dayton, NJ.
FA93495-17 for 0.0015 mm (Hydrometer): Analysis performed at SGS Dayton, NJ. FA93495-17 for 0.005 mm (Hydrometer): Analysis performed at SGS Dayton, NJ.
FA93495-17 for 0.030 mm (Hydrometer): Analysis performed at SGS Dayton, NJ.
FA93495-17 for 0.375 Inch Sieve: Analysis performed at SGS Dayton, NJ. FA93495-17 for 0.75 Inch Sieve: Analysis performed at SGS Dayton, NJ.
FA93495-17 for 1.5 Inch Sieve: Analysis performed at SGS Dayton, NJ.
FA93495-17 for 3 Inch Sieve: Analysis performed at SGS Dayton, NJ.
FA93495-17 for No.10 Sieve (2.00 mm): Analysis performed at SGS Dayton, NJ.
FA93495-17 for No.100 Sieve (0.15 mm): Analysis performed at SGS Dayton, NJ.
FA93495-17 for No.16 Sieve (1.18 mm): Analysis performed at SGS Dayton, NJ.
FA93495-17 for No.200 Sieve (0.075 mm): Analysis performed at SGS Dayton, NJ. FA93495-17 for No.30 Sieve (0.60 mm): Analysis performed at SGS Dayton, NJ.
FA93495-17 for No.4 Sieve (4.75 mm): Analysis performed at SGS Dayton, NJ.
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FA934952
FA93495-17 for No.50 Sieve (0.30 mm): Analysis performed at SGS Dayton, NJ.
FA93495-17 for No.8 Sieve (2.36 mm): Analysis performed at SGS Dayton, NJ. FA93495-18 for % Gravel: Analysis performed at SGS Dayton, NJ.
FA93495-18 for % Sand: Analysis performed at SGS Dayton, NJ.
FA93495-18 for % Silt, Clay, Colloids: Analysis performed at SGS Dayton, NJ.
FA93495-18 for 0.0015 mm (Hydrometer): Analysis performed at SGS Dayton, NJ.
FA93495-18 for 0.005 mm (Hydrometer): Analysis performed at SGS Dayton, NJ.
FA93495-18 for 0.030 mm (Hydrometer): Analysis performed at SGS Dayton, NJ.
FA93495-18 for 0.375 Inch Sieve: Analysis performed at SGS Dayton, NJ. FA93495-18 for 0.75 Inch Sieve: Analysis performed at SGS Dayton, NJ.
FA93495-18 for 1.5 Inch Sieve: Analysis performed at SGS Dayton, NJ. FA93495-18 for 3 Inch Sieve: Analysis performed at SGS Dayton, NJ.
FA93495-18 for No.10 Sieve (2.00 mm): Analysis performed at SGS Dayton, NJ. FA93495-18 for No.100 Sieve (0.15 mm): Analysis performed at SGS Dayton, NJ.
FA93495-18 for No.16 Sieve (1.18 mm): Analysis performed at SGS Dayton, NJ. FA93495-18 for No.200 Sieve (0.075 mm): Analysis performed at SGS Dayton, NJ.
FA93495-18 for No.30 Sieve (0.60 mm): Analysis performed at SGS Dayton, NJ. FA93495-18 for No.4 Sieve (4.75 mm): Analysis performed at SGS Dayton, NJ.
FA93495-18 for No.50 Sieve (0.30 mm): Analysis performed at SGS Dayton, NJ. FA93495-18 for No.8 Sieve (2.36 mm): Analysis performed at SGS Dayton, NJ.
General Chemistry By Method EPA 300/SW846 9056A Matrix: AQ Batch ID: GP37459
Sample(s) FA93495-1MS, FA93495-1MSD were used as the QC samples for Nitrogen, Nitrate, Sulfate, Nitrogen, Nitrate.
General Chemistry By Method SM3500FE B-11
Matrix: AQ Batch ID: GN90760
Sample(s) FA93495-1DUP were used as the QC samples for Iron, Ferrous. FA93495-1 for Iron, Ferrous: Field analysis required. Received out of hold time and analyzed by request.
FA93495-2 for Iron, Ferrous: Field analysis required. Received out of hold time and analyzed by request.
FA93495-3 for Iron, Ferrous: Field analysis required. Received out of hold time and analyzed by request.
FA93495-4 for Iron, Ferrous: Field analysis required. Received out of hold time and analyzed by request.
FA93495-5 for Iron, Ferrous: Field analysis required. Received out of hold time and analyzed by request.
FA93495-6 for Iron, Ferrous: Field analysis required. Received out of hold time and analyzed by request.
FA93495-7 for Iron, Ferrous: Field analysis required. Received out of hold time and analyzed by request.
SGS North America Inc. - Orlando certifies that data reported for samples received, listed on the associated custody chain or
analytical task order, were produced to specifications meeting the Quality System precision, accuracy and completeness objectives
except as noted. Estimated non-standard method measurement uncertainty data is available on request, based on quality control bias
and implicit for standard methods. Acceptable uncertainty requires tested parameter quality control data to meet method criteria. SGS
North America Inc.- Orlando is not responsible for data quality assumptions if partial reports are used and recommends that this
report be used in its entirety.

Narrative prepared by:

______________________________________
Ariel Hartney, Client Services (signature on file)
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Summary of Hits Page 1 of 6
Job Number:FA93495
Account:GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Collected:02/28/22
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA93495-1 MW-1
Benzene a 4.9 J 13 3.1 ug/l SM 6200B
n-Butylbenzene a 1040 25 6.3 ug/l SM 6200B
sec-Butylbenzene a 965 25 6.3 ug/l SM 6200B
tert-Butylbenzene a 20.3 13 3.1 ug/l SM 6200B
Ethylbenzene a 524 25 6.3 ug/l SM 6200B
Isopropylbenzene a 362 25 6.3 ug/l SM 6200B
p-Isopropyltoluene a 985 25 6.3 ug/l SM 6200B
Methyl Tert Butyl Ether a 5.2 J 13 3.1 ug/l SM 6200B
Naphthalene a 1610 25 6.3 ug/l SM 6200B
n-Propylbenzene a 706 25 6.3 ug/l SM 6200B
1,2,4-Trimethylbenzene b 2130 E 13 3.1 ug/l SM 6200B
Methane 767 0.50 0.16 ug/l RSKSOP-147/175
Iron, Ferrous c 9.5 1.0 mg/l SM3500FE B-11
Nitrogen, Nitrate 0.34 0.10 mg/l EPA 300/SW846 9056A
Sulfate 5.5 2.0 mg/l EPA 300/SW846 9056A
FA93495-2 MW-2
Methyl Tert Butyl Ether 5.4 0.50 0.13 ug/l SM 6200B
Methane 95.3 0.50 0.16 ug/l RSKSOP-147/175
Iron, Ferrous c 0.11 0.10 mg/l SM3500FE B-11
Nitrogen, Nitrate 0.12 0.10 mg/l EPA 300/SW846 9056A
Sulfate 12.0 2.0 mg/l EPA 300/SW846 9056A
FA93495-3 MW-3
sec-Butylbenzene 0.52 0.50 0.13 ug/l SM 6200B
Di-Isopropyl Ether 0.26 J 0.50 0.13 ug/l SM 6200B
Methyl Tert Butyl Ether 1.0 0.50 0.13 ug/l SM 6200B
Methane 485 0.50 0.16 ug/l RSKSOP-147/175
Iron, Ferrous c 0.59 0.50 mg/l SM3500FE B-11
Nitrogen, Nitrate 0.22 0.10 mg/l EPA 300/SW846 9056A
Sulfate 3.4 2.0 mg/l EPA 300/SW846 9056A
FA93495-4 MW-6
sec-Butylbenzene 1.9 0.50 0.13 ug/l SM 6200B
tert-Butylbenzene 0.66 0.50 0.13 ug/l SM 6200B
Di-Isopropyl Ether 3.5 0.50 0.13 ug/l SM 6200B
Isopropylbenzene 0.24 J 0.50 0.13 ug/l SM 6200B
Methyl Tert Butyl Ether 17.2 0.50 0.13 ug/l SM 6200B
Naphthalene 0.22 J 0.50 0.13 ug/l SM 6200B
Methane 839 0.50 0.16 ug/l RSKSOP-147/175
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Summary of Hits Page 2 of 6
Job Number:FA93495
Account:GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Collected:02/28/22
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
Iron, Ferrous c 6.9 1.0 mg/l SM3500FE B-11
FA93495-5 MW-12
Methane 1.1 0.50 0.16 ug/l RSKSOP-147/175
Sulfate 9.4 2.0 mg/l EPA 300/SW846 9056A
FA93495-6 MW-19
Benzene 5.7 0.50 0.13 ug/l SM 6200B
n-Butylbenzene 15.6 0.50 0.13 ug/l SM 6200B
sec-Butylbenzene 21.4 0.50 0.13 ug/l SM 6200B
Chloroethane 0.50 0.50 0.20 ug/l SM 6200B
Di-Isopropyl Ether 9.5 0.50 0.13 ug/l SM 6200B
Ethylbenzene 7.3 0.50 0.13 ug/l SM 6200B
Isopropylbenzene 17.1 0.50 0.13 ug/l SM 6200B
p-Isopropyltoluene 16.0 0.50 0.13 ug/l SM 6200B
Methyl Tert Butyl Ether 330 5.0 1.3 ug/l SM 6200B
Naphthalene 64.1 5.0 1.3 ug/l SM 6200B
n-Propylbenzene 21.4 0.50 0.13 ug/l SM 6200B
1,2,4-Trimethylbenzene 69.2 5.0 1.3 ug/l SM 6200B
1,3,5-Trimethylbenzene 10.6 0.50 0.13 ug/l SM 6200B
m,p-Xylene 2.1 1.0 0.13 ug/l SM 6200B
Xylene (total)2.1 1.5 0.25 ug/l SM 6200B
Methane 6140 5.0 1.6 ug/l RSKSOP-147/175
Iron, Ferrous c 6.5 1.0 mg/l SM3500FE B-11
FA93495-7 MW-5
Benzene 1.1 0.50 0.13 ug/l SM 6200B
n-Butylbenzene 0.30 J 0.50 0.13 ug/l SM 6200B
sec-Butylbenzene 1.3 0.50 0.13 ug/l SM 6200B
tert-Butylbenzene 0.55 0.50 0.13 ug/l SM 6200B
Di-Isopropyl Ether 16.5 0.50 0.13 ug/l SM 6200B
Ethylbenzene 1.6 0.50 0.13 ug/l SM 6200B
Isopropylbenzene 4.2 0.50 0.13 ug/l SM 6200B
Methyl Tert Butyl Ether 20.6 0.50 0.13 ug/l SM 6200B
Naphthalene 1.8 0.50 0.13 ug/l SM 6200B
n-Propylbenzene 3.2 0.50 0.13 ug/l SM 6200B
1,2,4-Trimethylbenzene 25.8 0.50 0.13 ug/l SM 6200B
1,3,5-Trimethylbenzene 2.1 0.50 0.13 ug/l SM 6200B
m,p-Xylene 3.2 1.0 0.13 ug/l SM 6200B
Xylene (total)3.2 1.5 0.25 ug/l SM 6200B
Methane 351 0.50 0.16 ug/l RSKSOP-147/175
Iron, Ferrous c 4.1 1.0 mg/l SM3500FE B-11
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Summary of Hits Page 3 of 6
Job Number:FA93495
Account:GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Collected:02/28/22
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA93495-8 MW-14
Naphthalene 0.14 J 0.50 0.13 ug/l SM 6200B
1,2,4-Trimethylbenzene 0.14 J 0.50 0.13 ug/l SM 6200B
FA93495-9 TMW-1
Benzene 0.61 J 1.3 0.31 ug/l SM 6200B
n-Butylbenzene 1.5 1.3 0.31 ug/l SM 6200B
sec-Butylbenzene 2.6 1.3 0.31 ug/l SM 6200B
tert-Butylbenzene 0.55 J 1.3 0.31 ug/l SM 6200B
Di-Isopropyl Ether 0.74 J 1.3 0.31 ug/l SM 6200B
Ethylbenzene 1.5 1.3 0.31 ug/l SM 6200B
Isopropylbenzene 1.4 1.3 0.31 ug/l SM 6200B
p-Isopropyltoluene 3.4 1.3 0.31 ug/l SM 6200B
Methyl Tert Butyl Ether 115 1.3 0.31 ug/l SM 6200B
Naphthalene 29.4 1.3 0.31 ug/l SM 6200B
n-Propylbenzene 2.3 1.3 0.31 ug/l SM 6200B
1,2,4-Trimethylbenzene 58.5 1.3 0.31 ug/l SM 6200B
1,3,5-Trimethylbenzene 20.3 1.3 0.31 ug/l SM 6200B
m,p-Xylene 6.7 2.5 0.31 ug/l SM 6200B
o-Xylene 6.7 1.3 0.31 ug/l SM 6200B
Xylene (total)13.4 3.8 0.63 ug/l SM 6200B
FA93495-10 TRIP BLANK
No hits reported in this sample.
FA93495-11 RW-1A
Benzene 0.32 J 0.50 0.13 ug/l SM 6200B
n-Butylbenzene 0.60 0.50 0.13 ug/l SM 6200B
sec-Butylbenzene 3.7 0.50 0.13 ug/l SM 6200B
tert-Butylbenzene 0.82 0.50 0.13 ug/l SM 6200B
Chloroethane 0.68 0.50 0.20 ug/l SM 6200B
Di-Isopropyl Ether 7.9 0.50 0.13 ug/l SM 6200B
Isopropylbenzene 2.6 0.50 0.13 ug/l SM 6200B
p-Isopropyltoluene 0.77 0.50 0.13 ug/l SM 6200B
Methyl Chloride 0.46 J 0.50 0.20 ug/l SM 6200B
Methyl Tert Butyl Ether 7.1 0.50 0.13 ug/l SM 6200B
Naphthalene 2.9 0.50 0.13 ug/l SM 6200B
n-Propylbenzene 1.0 0.50 0.13 ug/l SM 6200B
1,2,4-Trimethylbenzene 1.2 0.50 0.13 ug/l SM 6200B
1,3,5-Trimethylbenzene 0.16 J 0.50 0.13 ug/l SM 6200B
10 of 97
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Summary of Hits Page 4 of 6
Job Number:FA93495
Account:GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Collected:02/28/22
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA93495-12 RW-2
Benzene 5.8 2.5 0.63 ug/l SM 6200B
n-Butylbenzene 2.0 J 2.5 0.63 ug/l SM 6200B
sec-Butylbenzene 3.9 2.5 0.63 ug/l SM 6200B
Chloroethane 1.4 J 2.5 1.0 ug/l SM 6200B
Di-Isopropyl Ether 10.1 2.5 0.63 ug/l SM 6200B
Isopropylbenzene 1.0 J 2.5 0.63 ug/l SM 6200B
p-Isopropyltoluene 9.2 2.5 0.63 ug/l SM 6200B
Methyl Chloride 2.2 J 2.5 1.0 ug/l SM 6200B
Methyl Tert Butyl Ether 127 2.5 0.63 ug/l SM 6200B
Naphthalene 8.2 2.5 0.63 ug/l SM 6200B
n-Propylbenzene 0.82 J 2.5 0.63 ug/l SM 6200B
1,2,4-Trimethylbenzene 13.4 2.5 0.63 ug/l SM 6200B
1,3,5-Trimethylbenzene 10.3 2.5 0.63 ug/l SM 6200B
FA93495-13 WSW-34
No hits reported in this sample.
FA93495-14 WSW-32
No hits reported in this sample.
FA93495-15 TMW-1-22
3 Inch Sieve d 100 %ASTM D422-63
1.5 Inch Sieve d 100 %ASTM D422-63
0.75 Inch Sieve d 100 %ASTM D422-63
0.375 Inch Sieve d 92.8 %ASTM D422-63
No.4 Sieve (4.75 mm) d 92.5 %ASTM D422-63
No.8 Sieve (2.36 mm) d 92.2 %ASTM D422-63
No.10 Sieve (2.00 mm) d 91.6 %ASTM D422-63
No.16 Sieve (1.18 mm) d 90.6 %ASTM D422-63
No.30 Sieve (0.60 mm) d 86.5 %ASTM D422-63
No.50 Sieve (0.30 mm) d 78.2 %ASTM D422-63
No.100 Sieve (0.15 mm) d 71.9 %ASTM D422-63
No.200 Sieve (0.075 mm) d 69.5 %ASTM D422-63
0.030 mm (Hydrometer) d 64 %ASTM D422-63
0.005 mm (Hydrometer) d 42 %ASTM D422-63
0.0015 mm (Hydrometer) d 26 %ASTM D422-63
% Gravel d 7.5 %ASTM D422-63
% Sand d 23.0 %ASTM D422-63
% Silt, Clay, Colloids d 69.5 %ASTM D422-63
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Summary of Hits Page 5 of 6
Job Number:FA93495
Account:GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Collected:02/28/22
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA93495-16 TMW-1-30
3 Inch Sieve d 100 %ASTM D422-63
1.5 Inch Sieve d 100 %ASTM D422-63
0.75 Inch Sieve d 100 %ASTM D422-63
0.375 Inch Sieve d 100 %ASTM D422-63
No.4 Sieve (4.75 mm) d 100 %ASTM D422-63
No.8 Sieve (2.36 mm) d 98.4 %ASTM D422-63
No.10 Sieve (2.00 mm) d 96.9 %ASTM D422-63
No.16 Sieve (1.18 mm) d 96.2 %ASTM D422-63
No.30 Sieve (0.60 mm) d 92.4 %ASTM D422-63
No.50 Sieve (0.30 mm) d 85.6 %ASTM D422-63
No.100 Sieve (0.15 mm) d 79.2 %ASTM D422-63
No.200 Sieve (0.075 mm) d 75.5 %ASTM D422-63
0.030 mm (Hydrometer) d 64 %ASTM D422-63
0.005 mm (Hydrometer) d 36 %ASTM D422-63
0.0015 mm (Hydrometer) d 14 %ASTM D422-63
% Sand d 24.5 %ASTM D422-63
% Silt, Clay, Colloids d 75.5 %ASTM D422-63
FA93495-17 TMW-2-22
3 Inch Sieve d 100 %ASTM D422-63
1.5 Inch Sieve d 100 %ASTM D422-63
0.75 Inch Sieve d 100 %ASTM D422-63
0.375 Inch Sieve d 100 %ASTM D422-63
No.4 Sieve (4.75 mm) d 98.5 %ASTM D422-63
No.8 Sieve (2.36 mm) d 97.8 %ASTM D422-63
No.10 Sieve (2.00 mm) d 97.5 %ASTM D422-63
No.16 Sieve (1.18 mm) d 95.9 %ASTM D422-63
No.30 Sieve (0.60 mm) d 89.2 %ASTM D422-63
No.50 Sieve (0.30 mm) d 71.1 %ASTM D422-63
No.100 Sieve (0.15 mm) d 47.4 %ASTM D422-63
No.200 Sieve (0.075 mm) d 42.4 %ASTM D422-63
0.030 mm (Hydrometer) d 38.4 %ASTM D422-63
0.005 mm (Hydrometer) d 24.7 %ASTM D422-63
0.0015 mm (Hydrometer) d 16.2 %ASTM D422-63
% Gravel d 1.5 %ASTM D422-63
% Sand d 56.1 %ASTM D422-63
% Silt, Clay, Colloids d 42.4 %ASTM D422-63
FA93495-18 TMW-2-30
3 Inch Sieve d 100 %ASTM D422-63
12 of 97
FA934953
Summary of Hits Page 6 of 6
Job Number:FA93495
Account:GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Collected:02/28/22
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
1.5 Inch Sieve d 100 %ASTM D422-63
0.75 Inch Sieve d 100 %ASTM D422-63
0.375 Inch Sieve d 100 %ASTM D422-63
No.4 Sieve (4.75 mm) d 100 %ASTM D422-63
No.8 Sieve (2.36 mm) d 100 %ASTM D422-63
No.10 Sieve (2.00 mm) d 100 %ASTM D422-63
No.16 Sieve (1.18 mm) d 99.9 %ASTM D422-63
No.30 Sieve (0.60 mm) d 99.0 %ASTM D422-63
No.50 Sieve (0.30 mm) d 96.4 %ASTM D422-63
No.100 Sieve (0.15 mm) d 90.0 %ASTM D422-63
No.200 Sieve (0.075 mm) d 84.3 %ASTM D422-63
0.030 mm (Hydrometer) d 64 %ASTM D422-63
0.005 mm (Hydrometer) d 42 %ASTM D422-63
0.0015 mm (Hydrometer) d 26 %ASTM D422-63
% Sand d 15.7 %ASTM D422-63
% Silt, Clay, Colloids d 84.3 %ASTM D422-63
(a) Results from different vials are not consistent; higher results were reported.
(b) Results from different vials are not consistent; higher results were reported. No sample available for
reanalysis.
(c) Field analysis required. Received out of hold time and analyzed by request.
(d) Analysis performed at SGS Dayton, NJ.
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Sample Results
Report of Analysis
Orlando, FL
Section 4
14 of 97
FA934954
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW-1
Lab Sample ID:FA93495-1 Date Sampled:02/28/22
Matrix:AQ - Ground Water Date Received:03/01/22
Method:SM 6200B Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a A0230878.D 25 03/09/22 21:53 JL n/a n/a VA3083
Run #2 a A0230973.D 50 03/14/22 17:02 JL n/a n/a VA3087
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 4.9 13 3.1 ug/l J
108-86-1 Bromobenzene ND 13 3.1 ug/l
74-97-5 Bromochloromethane ND 13 3.1 ug/l
75-27-4 Bromodichloromethane ND 13 3.1 ug/l
75-25-2 Bromoform b ND 13 3.1 ug/l
104-51-8 n-Butylbenzene 1040 c 25 6.3 ug/l
135-98-8 sec-Butylbenzene 965 c 25 6.3 ug/l
98-06-6 tert-Butylbenzene 20.3 13 3.1 ug/l
56-23-5 Carbon Tetrachloride ND 13 3.1 ug/l
108-90-7 Chlorobenzene ND 13 3.1 ug/l
75-00-3 Chloroethane ND 13 5.0 ug/l
67-66-3 Chloroform ND 13 3.1 ug/l
95-49-8 o-Chlorotoluene ND 13 3.1 ug/l
106-43-4 p-Chlorotoluene ND 13 3.1 ug/l
124-48-1 Dibromochloromethane ND 13 3.1 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 13 6.2 ug/l
106-93-4 1,2-Dibromoethane ND 13 3.1 ug/l
75-71-8 Dichlorodifluoromethane ND 13 5.0 ug/l
95-50-1 1,2-Dichlorobenzene ND 13 3.1 ug/l
541-73-1 1,3-Dichlorobenzene ND 13 3.1 ug/l
106-46-7 1,4-Dichlorobenzene ND 13 3.1 ug/l
75-34-3 1,1-Dichloroethane ND 13 3.1 ug/l
107-06-2 1,2-Dichloroethane ND 13 3.1 ug/l
75-35-4 1,1-Dichloroethylene ND 13 3.1 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 13 3.1 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 13 3.1 ug/l
78-87-5 1,2-Dichloropropane ND 13 3.1 ug/l
142-28-9 1,3-Dichloropropane ND 13 3.1 ug/l
594-20-7 2,2-Dichloropropane ND 13 3.1 ug/l
563-58-6 1,1-Dichloropropene ND 13 3.1 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 13 3.1 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 13 3.1 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
15 of 97
FA9349544.1
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW-1
Lab Sample ID:FA93495-1 Date Sampled:02/28/22
Matrix:AQ - Ground Water Date Received:03/01/22
Method:SM 6200B Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 13 3.1 ug/l
100-41-4 Ethylbenzene 524 c 25 6.3 ug/l
87-68-3 Hexachlorobutadiene ND 13 3.1 ug/l
98-82-8 Isopropylbenzene 362 c 25 6.3 ug/l
99-87-6 p-Isopropyltoluene 985 c 25 6.3 ug/l
74-83-9 Methyl Bromide ND 13 5.0 ug/l
74-87-3 Methyl Chloride ND 13 5.0 ug/l
74-95-3 Methylene Bromide ND 13 3.1 ug/l
75-09-2 Methylene Chloride ND 50 25 ug/l
1634-04-4 Methyl Tert Butyl Ether 5.2 13 3.1 ug/l J
91-20-3 Naphthalene 1610 c 25 6.3 ug/l
103-65-1 n-Propylbenzene 706 c 25 6.3 ug/l
100-42-5 Styrene ND 13 3.1 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 13 3.1 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 13 3.1 ug/l
127-18-4 Tetrachloroethylene ND 13 3.1 ug/l
108-88-3 Toluene ND 13 3.1 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 13 3.1 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 13 3.1 ug/l
71-55-6 1,1,1-Trichloroethane ND 13 3.1 ug/l
79-00-5 1,1,2-Trichloroethane ND 13 3.1 ug/l
79-01-6 Trichloroethylene ND 13 3.1 ug/l
75-69-4 Trichlorofluoromethane ND 13 5.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 13 3.1 ug/l
95-63-6 1,2,4-Trimethylbenzene d 2130 13 3.1 ug/l E
108-67-8 1,3,5-Trimethylbenzene ND 13 3.1 ug/l
75-01-4 Vinyl Chloride ND 13 3.1 ug/l
m,p-Xylene ND 25 3.1 ug/l
95-47-6 o-Xylene ND 13 3.1 ug/l
1330-20-7 Xylene (total)ND 38 6.3 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 104%106%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%106%70-130%
2037-26-5 Toluene-D8 96%97%70-130%
460-00-4 4-Bromofluorobenzene 100%160% e 70-130%
(a) Results from different vials are not consistent; higher results were reported.
(b) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW-1
Lab Sample ID:FA93495-1 Date Sampled:02/28/22
Matrix:AQ - Ground Water Date Received:03/01/22
Method:SM 6200B Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
(c) Result is from Run# 2
(d) No sample available for reanalysis.
(e) Outside control limits.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
17 of 97
FA9349544.1
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:MW-1
Lab Sample ID:FA93495-1 Date Sampled:02/28/22
Matrix:AQ - Ground Water Date Received:03/01/22
Method:RSKSOP-147/175 Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LL77563.D 1 03/02/22 12:33 TD n/a n/a GLL2694
Run #2
Initial Volume Headspace Volume Volume Injected Temperature
Run #1 38.0 ml 5.0 ml 500 ul 20 Deg. C
Run #2
CAS No.Compound Result RL MDL Units Q
74-82-8 Methane 767 0.50 0.16 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
18 of 97
FA9349544.1
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:MW-1
Lab Sample ID:FA93495-1 Date Sampled:02/28/22
Matrix:AQ - Ground Water Date Received:03/01/22
Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Iron, Ferrous a 9.5 1.0 mg/l 10 03/08/22 13:00 FN SM3500FE B-11
Nitrogen, Nitrate 0.34 0.10 mg/l 1 03/01/22 11:51 JB EPA 300/SW846 9056A
Sulfate 5.5 2.0 mg/l 1 03/01/22 11:51 JB EPA 300/SW846 9056A
(a) Field analysis required. Received out of hold time and analyzed by request.
RL = Reporting Limit
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SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-2
Lab Sample ID:FA93495-2 Date Sampled:02/28/22
Matrix:AQ - Ground Water Date Received:03/01/22
Method:SM 6200B Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0230967.D 1 03/14/22 14:45 JL n/a n/a VA3087
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
20 of 97
FA9349544.2
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-2
Lab Sample ID:FA93495-2 Date Sampled:02/28/22
Matrix:AQ - Ground Water Date Received:03/01/22
Method:SM 6200B Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 5.4 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 104%70-130%
17060-07-0 1,2-Dichloroethane-D4 105%70-130%
2037-26-5 Toluene-D8 96%70-130%
460-00-4 4-Bromofluorobenzene 95%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
21 of 97
FA9349544.2
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:MW-2
Lab Sample ID:FA93495-2 Date Sampled:02/28/22
Matrix:AQ - Ground Water Date Received:03/01/22
Method:RSKSOP-147/175 Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LL77566.D 1 03/02/22 13:38 TD n/a n/a GLL2694
Run #2
Initial Volume Headspace Volume Volume Injected Temperature
Run #1 38.0 ml 5.0 ml 500 ul 20 Deg. C
Run #2
CAS No.Compound Result RL MDL Units Q
74-82-8 Methane 95.3 0.50 0.16 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
22 of 97
FA9349544.2
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:MW-2
Lab Sample ID:FA93495-2 Date Sampled:02/28/22
Matrix:AQ - Ground Water Date Received:03/01/22
Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Iron, Ferrous a 0.11 0.10 mg/l 1 03/08/22 13:00 FN SM3500FE B-11
Nitrogen, Nitrate 0.12 0.10 mg/l 1 03/01/22 13:00 JB EPA 300/SW846 9056A
Sulfate 12.0 2.0 mg/l 1 03/01/22 13:00 JB EPA 300/SW846 9056A
(a) Field analysis required. Received out of hold time and analyzed by request.
RL = Reporting Limit
23 of 97
FA9349544.2
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-3
Lab Sample ID:FA93495-3 Date Sampled:02/28/22
Matrix:AQ - Ground Water Date Received:03/01/22
Method:SM 6200B Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0230864.D 1 03/09/22 16:33 JL n/a n/a VA3083
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform a ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene 0.52 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
24 of 97
FA9349544.3
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-3
Lab Sample ID:FA93495-3 Date Sampled:02/28/22
Matrix:AQ - Ground Water Date Received:03/01/22
Method:SM 6200B Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 0.26 0.50 0.13 ug/l J
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 1.0 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
2037-26-5 Toluene-D8 93%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
(a) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
25 of 97
FA9349544.3
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:MW-3
Lab Sample ID:FA93495-3 Date Sampled:02/28/22
Matrix:AQ - Ground Water Date Received:03/01/22
Method:RSKSOP-147/175 Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LL77567.D 1 03/02/22 13:47 TD n/a n/a GLL2694
Run #2
Initial Volume Headspace Volume Volume Injected Temperature
Run #1 38.0 ml 5.0 ml 500 ul 20 Deg. C
Run #2
CAS No.Compound Result RL MDL Units Q
74-82-8 Methane 485 0.50 0.16 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
26 of 97
FA9349544.3
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:MW-3
Lab Sample ID:FA93495-3 Date Sampled:02/28/22
Matrix:AQ - Ground Water Date Received:03/01/22
Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Iron, Ferrous a 0.59 0.50 mg/l 5 03/08/22 13:00 FN SM3500FE B-11
Nitrogen, Nitrate 0.22 0.10 mg/l 1 03/01/22 13:23 JB EPA 300/SW846 9056A
Sulfate 3.4 2.0 mg/l 1 03/01/22 13:23 JB EPA 300/SW846 9056A
(a) Field analysis required. Received out of hold time and analyzed by request.
RL = Reporting Limit
27 of 97
FA9349544.3
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-6
Lab Sample ID:FA93495-4 Date Sampled:02/28/22
Matrix:AQ - Ground Water Date Received:03/01/22
Method:SM 6200B Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0230865.D 1 03/09/22 16:55 JL n/a n/a VA3083
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform a ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene 1.9 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene 0.66 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
28 of 97
FA9349544.4
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-6
Lab Sample ID:FA93495-4 Date Sampled:02/28/22
Matrix:AQ - Ground Water Date Received:03/01/22
Method:SM 6200B Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 3.5 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene 0.24 0.50 0.13 ug/l J
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 17.2 0.50 0.13 ug/l
91-20-3 Naphthalene 0.22 0.50 0.13 ug/l J
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 104%70-130%
(a) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
29 of 97
FA9349544.4
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:MW-6
Lab Sample ID:FA93495-4 Date Sampled:02/28/22
Matrix:AQ - Ground Water Date Received:03/01/22
Method:RSKSOP-147/175 Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LL77568.D 1 03/02/22 13:59 TD n/a n/a GLL2694
Run #2
Initial Volume Headspace Volume Volume Injected Temperature
Run #1 38.0 ml 5.0 ml 500 ul 20 Deg. C
Run #2
CAS No.Compound Result RL MDL Units Q
74-82-8 Methane 839 0.50 0.16 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
30 of 97
FA9349544.4
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:MW-6
Lab Sample ID:FA93495-4 Date Sampled:02/28/22
Matrix:AQ - Ground Water Date Received:03/01/22
Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Iron, Ferrous a 6.9 1.0 mg/l 10 03/08/22 13:00 FN SM3500FE B-11
Nitrogen, Nitrate <0.10 0.10 mg/l 1 03/01/22 13:46 JB EPA 300/SW846 9056A
Sulfate <2.0 2.0 mg/l 1 03/01/22 13:46 JB EPA 300/SW846 9056A
(a) Field analysis required. Received out of hold time and analyzed by request.
RL = Reporting Limit
31 of 97
FA9349544.4
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-12
Lab Sample ID:FA93495-5 Date Sampled:02/28/22
Matrix:AQ - Ground Water Date Received:03/01/22
Method:SM 6200B Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0230866.D 1 03/09/22 17:18 JL n/a n/a VA3083
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform a ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
32 of 97
FA9349544.5
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-12
Lab Sample ID:FA93495-5 Date Sampled:02/28/22
Matrix:AQ - Ground Water Date Received:03/01/22
Method:SM 6200B Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 101%70-130%
2037-26-5 Toluene-D8 95%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
(a) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
33 of 97
FA9349544.5
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:MW-12
Lab Sample ID:FA93495-5 Date Sampled:02/28/22
Matrix:AQ - Ground Water Date Received:03/01/22
Method:RSKSOP-147/175 Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LL77569.D 1 03/02/22 14:09 TD n/a n/a GLL2694
Run #2
Initial Volume Headspace Volume Volume Injected Temperature
Run #1 38.0 ml 5.0 ml 500 ul 20 Deg. C
Run #2
CAS No.Compound Result RL MDL Units Q
74-82-8 Methane 1.1 0.50 0.16 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
34 of 97
FA9349544.5
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:MW-12
Lab Sample ID:FA93495-5 Date Sampled:02/28/22
Matrix:AQ - Ground Water Date Received:03/01/22
Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Iron, Ferrous a <0.50 0.50 mg/l 5 03/08/22 13:00 FN SM3500FE B-11
Nitrogen, Nitrate <0.10 0.10 mg/l 1 03/01/22 14:09 JB EPA 300/SW846 9056A
Sulfate 9.4 2.0 mg/l 1 03/01/22 14:09 JB EPA 300/SW846 9056A
(a) Field analysis required. Received out of hold time and analyzed by request.
RL = Reporting Limit
35 of 97
FA9349544.5
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-19
Lab Sample ID:FA93495-6 Date Sampled:02/28/22
Matrix:AQ - Ground Water Date Received:03/01/22
Method:SM 6200B Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0230867.D 1 03/09/22 17:41 JL n/a n/a VA3083
Run #2 A0230987.D 10 03/14/22 22:24 JL n/a n/a VA3087
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 5.7 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform a ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene 15.6 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene 21.4 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane 0.50 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
36 of 97
FA9349544.6
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-19
Lab Sample ID:FA93495-6 Date Sampled:02/28/22
Matrix:AQ - Ground Water Date Received:03/01/22
Method:SM 6200B Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 9.5 0.50 0.13 ug/l
100-41-4 Ethylbenzene 7.3 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene 17.1 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene 16.0 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 330 b 5.0 1.3 ug/l
91-20-3 Naphthalene 64.1 b 5.0 1.3 ug/l
103-65-1 n-Propylbenzene 21.4 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 69.2 b 5.0 1.3 ug/l
108-67-8 1,3,5-Trimethylbenzene 10.6 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 2.1 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)2.1 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%101%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%101%70-130%
2037-26-5 Toluene-D8 97%99%70-130%
460-00-4 4-Bromofluorobenzene 120%103%70-130%
(a) Associated CCV outside of control limits high, sample was ND.
(b) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
37 of 97
FA9349544.6
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:MW-19
Lab Sample ID:FA93495-6 Date Sampled:02/28/22
Matrix:AQ - Ground Water Date Received:03/01/22
Method:RSKSOP-147/175 Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 1R7499.D 10 03/04/22 16:20 TD n/a n/a G1R284
Run #2
Initial Volume Headspace Volume Volume Injected Temperature
Run #1 38.0 ml 5.0 ml 500 ul 20 Deg. C
Run #2
CAS No.Compound Result RL MDL Units Q
74-82-8 Methane 6140 5.0 1.6 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
38 of 97
FA9349544.6
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:MW-19
Lab Sample ID:FA93495-6 Date Sampled:02/28/22
Matrix:AQ - Ground Water Date Received:03/01/22
Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Iron, Ferrous a 6.5 1.0 mg/l 10 03/08/22 13:00 FN SM3500FE B-11
Nitrogen, Nitrate <0.10 0.10 mg/l 1 03/01/22 14:32 JB EPA 300/SW846 9056A
Sulfate <2.0 2.0 mg/l 1 03/01/22 14:32 JB EPA 300/SW846 9056A
(a) Field analysis required. Received out of hold time and analyzed by request.
RL = Reporting Limit
39 of 97
FA9349544.6
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-5
Lab Sample ID:FA93495-7 Date Sampled:02/28/22
Matrix:AQ - Ground Water Date Received:03/01/22
Method:SM 6200B Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0230868.D 1 03/09/22 18:03 JL n/a n/a VA3083
Run #2 A0230968.D 1 03/14/22 15:07 JL n/a n/a VA3087
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 1.1 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform a ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene 0.30 0.50 0.13 ug/l J
135-98-8 sec-Butylbenzene 1.3 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene 0.55 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
40 of 97
FA9349544.7
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-5
Lab Sample ID:FA93495-7 Date Sampled:02/28/22
Matrix:AQ - Ground Water Date Received:03/01/22
Method:SM 6200B Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 16.5 0.50 0.13 ug/l
100-41-4 Ethylbenzene 1.6 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene 4.2 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 20.6 0.50 0.13 ug/l
91-20-3 Naphthalene 1.8 b 0.50 0.13 ug/l
103-65-1 n-Propylbenzene 3.2 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 25.8 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene 2.1 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 3.2 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)3.2 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 98%99%70-130%
17060-07-0 1,2-Dichloroethane-D4 97%101%70-130%
2037-26-5 Toluene-D8 97%96%70-130%
460-00-4 4-Bromofluorobenzene 102%100%70-130%
(a) Associated CCV outside of control limits high, sample was ND.
(b) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
41 of 97
FA9349544.7
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:MW-5
Lab Sample ID:FA93495-7 Date Sampled:02/28/22
Matrix:AQ - Ground Water Date Received:03/01/22
Method:RSKSOP-147/175 Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 LL77571.D 1 03/02/22 14:33 TD n/a n/a GLL2694
Run #2
Initial Volume Headspace Volume Volume Injected Temperature
Run #1 38.0 ml 5.0 ml 500 ul 20 Deg. C
Run #2
CAS No.Compound Result RL MDL Units Q
74-82-8 Methane 351 0.50 0.16 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
42 of 97
FA9349544.7
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:MW-5
Lab Sample ID:FA93495-7 Date Sampled:02/28/22
Matrix:AQ - Ground Water Date Received:03/01/22
Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Iron, Ferrous a 4.1 1.0 mg/l 10 03/08/22 13:00 FN SM3500FE B-11
Nitrogen, Nitrate <0.10 0.10 mg/l 1 03/01/22 15:42 JB EPA 300/SW846 9056A
Sulfate <2.0 2.0 mg/l 1 03/01/22 15:42 JB EPA 300/SW846 9056A
(a) Field analysis required. Received out of hold time and analyzed by request.
RL = Reporting Limit
43 of 97
FA9349544.7
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-14
Lab Sample ID:FA93495-8 Date Sampled:02/28/22
Matrix:AQ - Ground Water Date Received:03/01/22
Method:SM 6200B Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0230869.D 1 03/09/22 18:26 JL n/a n/a VA3083
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform a ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
44 of 97
FA9349544.8
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-14
Lab Sample ID:FA93495-8 Date Sampled:02/28/22
Matrix:AQ - Ground Water Date Received:03/01/22
Method:SM 6200B Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene 0.14 0.50 0.13 ug/l J
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 0.14 0.50 0.13 ug/l J
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 98%70-130%
17060-07-0 1,2-Dichloroethane-D4 99%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
(a) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
45 of 97
FA9349544.8
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:TMW-1
Lab Sample ID:FA93495-9 Date Sampled:02/28/22
Matrix:AQ - Ground Water Date Received:03/01/22
Method:SM 6200B Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0230880.D 2.5 03/09/22 22:38 JL n/a n/a VA3083
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 0.61 1.3 0.31 ug/l J
108-86-1 Bromobenzene ND 1.3 0.31 ug/l
74-97-5 Bromochloromethane ND 1.3 0.31 ug/l
75-27-4 Bromodichloromethane ND 1.3 0.31 ug/l
75-25-2 Bromoform a ND 1.3 0.31 ug/l
104-51-8 n-Butylbenzene 1.5 1.3 0.31 ug/l
135-98-8 sec-Butylbenzene 2.6 1.3 0.31 ug/l
98-06-6 tert-Butylbenzene 0.55 1.3 0.31 ug/l J
56-23-5 Carbon Tetrachloride ND 1.3 0.31 ug/l
108-90-7 Chlorobenzene ND 1.3 0.31 ug/l
75-00-3 Chloroethane ND 1.3 0.50 ug/l
67-66-3 Chloroform ND 1.3 0.31 ug/l
95-49-8 o-Chlorotoluene ND 1.3 0.31 ug/l
106-43-4 p-Chlorotoluene ND 1.3 0.31 ug/l
124-48-1 Dibromochloromethane ND 1.3 0.31 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 1.3 0.62 ug/l
106-93-4 1,2-Dibromoethane ND 1.3 0.31 ug/l
75-71-8 Dichlorodifluoromethane ND 1.3 0.50 ug/l
95-50-1 1,2-Dichlorobenzene ND 1.3 0.31 ug/l
541-73-1 1,3-Dichlorobenzene ND 1.3 0.31 ug/l
106-46-7 1,4-Dichlorobenzene ND 1.3 0.31 ug/l
75-34-3 1,1-Dichloroethane ND 1.3 0.31 ug/l
107-06-2 1,2-Dichloroethane ND 1.3 0.31 ug/l
75-35-4 1,1-Dichloroethylene ND 1.3 0.31 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 1.3 0.31 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 1.3 0.31 ug/l
78-87-5 1,2-Dichloropropane ND 1.3 0.31 ug/l
142-28-9 1,3-Dichloropropane ND 1.3 0.31 ug/l
594-20-7 2,2-Dichloropropane ND 1.3 0.31 ug/l
563-58-6 1,1-Dichloropropene ND 1.3 0.31 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 1.3 0.31 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 1.3 0.31 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
46 of 97
FA9349544.9
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:TMW-1
Lab Sample ID:FA93495-9 Date Sampled:02/28/22
Matrix:AQ - Ground Water Date Received:03/01/22
Method:SM 6200B Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 0.74 1.3 0.31 ug/l J
100-41-4 Ethylbenzene 1.5 1.3 0.31 ug/l
87-68-3 Hexachlorobutadiene ND 1.3 0.31 ug/l
98-82-8 Isopropylbenzene 1.4 1.3 0.31 ug/l
99-87-6 p-Isopropyltoluene 3.4 1.3 0.31 ug/l
74-83-9 Methyl Bromide ND 1.3 0.50 ug/l
74-87-3 Methyl Chloride ND 1.3 0.50 ug/l
74-95-3 Methylene Bromide ND 1.3 0.31 ug/l
75-09-2 Methylene Chloride ND 5.0 2.5 ug/l
1634-04-4 Methyl Tert Butyl Ether 115 1.3 0.31 ug/l
91-20-3 Naphthalene 29.4 1.3 0.31 ug/l
103-65-1 n-Propylbenzene 2.3 1.3 0.31 ug/l
100-42-5 Styrene ND 1.3 0.31 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 1.3 0.31 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 1.3 0.31 ug/l
127-18-4 Tetrachloroethylene ND 1.3 0.31 ug/l
108-88-3 Toluene ND 1.3 0.31 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 1.3 0.31 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 1.3 0.31 ug/l
71-55-6 1,1,1-Trichloroethane ND 1.3 0.31 ug/l
79-00-5 1,1,2-Trichloroethane ND 1.3 0.31 ug/l
79-01-6 Trichloroethylene ND 1.3 0.31 ug/l
75-69-4 Trichlorofluoromethane ND 1.3 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 1.3 0.31 ug/l
95-63-6 1,2,4-Trimethylbenzene 58.5 1.3 0.31 ug/l
108-67-8 1,3,5-Trimethylbenzene 20.3 1.3 0.31 ug/l
75-01-4 Vinyl Chloride ND 1.3 0.31 ug/l
m,p-Xylene 6.7 2.5 0.31 ug/l
95-47-6 o-Xylene 6.7 1.3 0.31 ug/l
1330-20-7 Xylene (total)13.4 3.8 0.63 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 97%70-130%
(a) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
47 of 97
FA9349544.9
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:TRIP BLANK
Lab Sample ID:FA93495-10 Date Sampled:02/28/22
Matrix:AQ - Trip Blank Water Date Received:03/01/22
Method:SM 6200B Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0230860.D 1 03/09/22 15:02 JL n/a n/a VA3083
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform a ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
48 of 97
FA9349544.10
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:TRIP BLANK
Lab Sample ID:FA93495-10 Date Sampled:02/28/22
Matrix:AQ - Trip Blank Water Date Received:03/01/22
Method:SM 6200B Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 101%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
(a) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
49 of 97
FA9349544.10
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:RW-1A
Lab Sample ID:FA93495-11 Date Sampled:02/28/22
Matrix:AQ - Ground Water Date Received:03/01/22
Method:SM 6200B Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0230872.D 1 03/09/22 19:35 JL n/a n/a VA3083
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 0.32 0.50 0.13 ug/l J
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform a ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene 0.60 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene 3.7 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene 0.82 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane 0.68 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
50 of 97
FA9349544.11
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:RW-1A
Lab Sample ID:FA93495-11 Date Sampled:02/28/22
Matrix:AQ - Ground Water Date Received:03/01/22
Method:SM 6200B Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 7.9 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene 2.6 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene 0.77 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride 0.46 0.50 0.20 ug/l J
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 7.1 0.50 0.13 ug/l
91-20-3 Naphthalene 2.9 0.50 0.13 ug/l
103-65-1 n-Propylbenzene 1.0 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 1.2 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene 0.16 0.50 0.13 ug/l J
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 99%70-130%
2037-26-5 Toluene-D8 95%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
(a) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
51 of 97
FA9349544.11
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:RW-2
Lab Sample ID:FA93495-12 Date Sampled:02/28/22
Matrix:AQ - Ground Water Date Received:03/01/22
Method:SM 6200B Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0230881.D 5 03/09/22 23:01 JL n/a n/a VA3083
Run #2 A0230984.D 5 03/14/22 21:16 JL n/a n/a VA3087
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 5.8 2.5 0.63 ug/l
108-86-1 Bromobenzene ND 2.5 0.63 ug/l
74-97-5 Bromochloromethane ND 2.5 0.63 ug/l
75-27-4 Bromodichloromethane ND 2.5 0.63 ug/l
75-25-2 Bromoform a ND 2.5 0.63 ug/l
104-51-8 n-Butylbenzene 2.0 2.5 0.63 ug/l J
135-98-8 sec-Butylbenzene 3.9 2.5 0.63 ug/l
98-06-6 tert-Butylbenzene ND 2.5 0.63 ug/l
56-23-5 Carbon Tetrachloride ND 2.5 0.63 ug/l
108-90-7 Chlorobenzene ND 2.5 0.63 ug/l
75-00-3 Chloroethane 1.4 2.5 1.0 ug/l J
67-66-3 Chloroform ND 2.5 0.63 ug/l
95-49-8 o-Chlorotoluene ND 2.5 0.63 ug/l
106-43-4 p-Chlorotoluene ND 2.5 0.63 ug/l
124-48-1 Dibromochloromethane ND 2.5 0.63 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 2.5 1.2 ug/l
106-93-4 1,2-Dibromoethane ND 2.5 0.63 ug/l
75-71-8 Dichlorodifluoromethane ND 2.5 1.0 ug/l
95-50-1 1,2-Dichlorobenzene ND 2.5 0.63 ug/l
541-73-1 1,3-Dichlorobenzene ND 2.5 0.63 ug/l
106-46-7 1,4-Dichlorobenzene ND 2.5 0.63 ug/l
75-34-3 1,1-Dichloroethane ND 2.5 0.63 ug/l
107-06-2 1,2-Dichloroethane ND 2.5 0.63 ug/l
75-35-4 1,1-Dichloroethylene ND 2.5 0.63 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 2.5 0.63 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 2.5 0.63 ug/l
78-87-5 1,2-Dichloropropane ND 2.5 0.63 ug/l
142-28-9 1,3-Dichloropropane ND 2.5 0.63 ug/l
594-20-7 2,2-Dichloropropane ND 2.5 0.63 ug/l
563-58-6 1,1-Dichloropropene ND 2.5 0.63 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 2.5 0.63 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 2.5 0.63 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
52 of 97
FA9349544.12
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:RW-2
Lab Sample ID:FA93495-12 Date Sampled:02/28/22
Matrix:AQ - Ground Water Date Received:03/01/22
Method:SM 6200B Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 10.1 2.5 0.63 ug/l
100-41-4 Ethylbenzene ND 2.5 0.63 ug/l
87-68-3 Hexachlorobutadiene ND 2.5 0.63 ug/l
98-82-8 Isopropylbenzene 1.0 2.5 0.63 ug/l J
99-87-6 p-Isopropyltoluene 9.2 2.5 0.63 ug/l
74-83-9 Methyl Bromide ND 2.5 1.0 ug/l
74-87-3 Methyl Chloride 2.2 2.5 1.0 ug/l J
74-95-3 Methylene Bromide ND 2.5 0.63 ug/l
75-09-2 Methylene Chloride ND 10 5.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 127 2.5 0.63 ug/l
91-20-3 Naphthalene 8.2 b 2.5 0.63 ug/l
103-65-1 n-Propylbenzene 0.82 2.5 0.63 ug/l J
100-42-5 Styrene ND 2.5 0.63 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 2.5 0.63 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 2.5 0.63 ug/l
127-18-4 Tetrachloroethylene ND 2.5 0.63 ug/l
108-88-3 Toluene ND 2.5 0.63 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 2.5 0.63 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 2.5 0.63 ug/l
71-55-6 1,1,1-Trichloroethane ND 2.5 0.63 ug/l
79-00-5 1,1,2-Trichloroethane ND 2.5 0.63 ug/l
79-01-6 Trichloroethylene ND 2.5 0.63 ug/l
75-69-4 Trichlorofluoromethane ND 2.5 1.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.5 0.63 ug/l
95-63-6 1,2,4-Trimethylbenzene 13.4 2.5 0.63 ug/l
108-67-8 1,3,5-Trimethylbenzene 10.3 2.5 0.63 ug/l
75-01-4 Vinyl Chloride ND 2.5 0.63 ug/l
m,p-Xylene ND 5.0 0.63 ug/l
95-47-6 o-Xylene ND 2.5 0.63 ug/l
1330-20-7 Xylene (total)ND 7.5 1.3 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 104%101%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%98%70-130%
2037-26-5 Toluene-D8 99%98%70-130%
460-00-4 4-Bromofluorobenzene 103%103%70-130%
(a) Associated CCV outside of control limits high, sample was ND.
(b) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
53 of 97
FA9349544.12
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:WSW-34
Lab Sample ID:FA93495-13 Date Sampled:02/28/22
Matrix:AQ - Ground Water Date Received:03/01/22
Method:SM 6200B Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0230873.D 1 03/09/22 19:58 JL n/a n/a VA3083
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform a ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
54 of 97
FA9349544.13
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:WSW-34
Lab Sample ID:FA93495-13 Date Sampled:02/28/22
Matrix:AQ - Ground Water Date Received:03/01/22
Method:SM 6200B Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 98%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
(a) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
55 of 97
FA9349544.13
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:WSW-32
Lab Sample ID:FA93495-14 Date Sampled:02/28/22
Matrix:AQ - Ground Water Date Received:03/01/22
Method:SM 6200B Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0230874.D 1 03/09/22 20:21 JL n/a n/a VA3083
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform a ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
56 of 97
FA9349544.14
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:WSW-32
Lab Sample ID:FA93495-14 Date Sampled:02/28/22
Matrix:AQ - Ground Water Date Received:03/01/22
Method:SM 6200B Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 101%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
(a) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
57 of 97
FA9349544.14
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:TMW-1-22
Lab Sample ID:FA93495-15 Date Sampled:02/28/22
Matrix:SO - Soil Date Received:03/01/22
Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Particle Size Analysis (Sieve and Hydrometer Testing)
3 Inch Sieve a 100 %1 03/22/22 14:39 ANJ ASTM D422-63
1.5 Inch Sieve a 100 %1 03/22/22 14:39 ANJ ASTM D422-63
0.75 Inch Sieve a 100 %1 03/22/22 14:39 ANJ ASTM D422-63
0.375 Inch Sieve a 92.8 %1 03/22/22 14:39 ANJ ASTM D422-63
No.4 Sieve (4.75 mm) a 92.5 %1 03/22/22 14:39 ANJ ASTM D422-63
No.8 Sieve (2.36 mm) a 92.2 %1 03/22/22 14:39 ANJ ASTM D422-63
No.10 Sieve (2.00 mm) a 91.6 %1 03/22/22 14:39 ANJ ASTM D422-63
No.16 Sieve (1.18 mm) a 90.6 %1 03/22/22 14:39 ANJ ASTM D422-63
No.30 Sieve (0.60 mm) a 86.5 %1 03/22/22 14:39 ANJ ASTM D422-63
No.50 Sieve (0.30 mm) a 78.2 %1 03/22/22 14:39 ANJ ASTM D422-63
No.100 Sieve (0.15 mm) a 71.9 %1 03/22/22 14:39 ANJ ASTM D422-63
No.200 Sieve (0.075 mm) a 69.5 %1 03/22/22 14:39 ANJ ASTM D422-63
0.030 mm (Hydrometer) a 64 %1 03/22/22 14:39 ANJ ASTM D422-63
0.005 mm (Hydrometer) a 42 %1 03/22/22 14:39 ANJ ASTM D422-63
0.0015 mm (Hydrometer) a 26 %1 03/22/22 14:39 ANJ ASTM D422-63
% Gravel a 7.5 %1 03/22/22 14:39 ANJ ASTM D422-63
% Sand a 23.0 %1 03/22/22 14:39 ANJ ASTM D422-63
% Silt, Clay, Colloids a 69.5 %1 03/22/22 14:39 ANJ ASTM D422-63
(a) Analysis performed at SGS Dayton, NJ.
RL = Reporting Limit
58 of 97
FA9349544.15
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:TMW-1-30
Lab Sample ID:FA93495-16 Date Sampled:02/28/22
Matrix:SO - Soil Date Received:03/01/22
Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Particle Size Analysis (Sieve and Hydrometer Testing)
3 Inch Sieve a 100 %1 03/22/22 14:39 ANJ ASTM D422-63
1.5 Inch Sieve a 100 %1 03/22/22 14:39 ANJ ASTM D422-63
0.75 Inch Sieve a 100 %1 03/22/22 14:39 ANJ ASTM D422-63
0.375 Inch Sieve a 100 %1 03/22/22 14:39 ANJ ASTM D422-63
No.4 Sieve (4.75 mm) a 100 %1 03/22/22 14:39 ANJ ASTM D422-63
No.8 Sieve (2.36 mm) a 98.4 %1 03/22/22 14:39 ANJ ASTM D422-63
No.10 Sieve (2.00 mm) a 96.9 %1 03/22/22 14:39 ANJ ASTM D422-63
No.16 Sieve (1.18 mm) a 96.2 %1 03/22/22 14:39 ANJ ASTM D422-63
No.30 Sieve (0.60 mm) a 92.4 %1 03/22/22 14:39 ANJ ASTM D422-63
No.50 Sieve (0.30 mm) a 85.6 %1 03/22/22 14:39 ANJ ASTM D422-63
No.100 Sieve (0.15 mm) a 79.2 %1 03/22/22 14:39 ANJ ASTM D422-63
No.200 Sieve (0.075 mm) a 75.5 %1 03/22/22 14:39 ANJ ASTM D422-63
0.030 mm (Hydrometer) a 64 %1 03/22/22 14:39 ANJ ASTM D422-63
0.005 mm (Hydrometer) a 36 %1 03/22/22 14:39 ANJ ASTM D422-63
0.0015 mm (Hydrometer) a 14 %1 03/22/22 14:39 ANJ ASTM D422-63
% Gravel a 0.0 %1 03/22/22 14:39 ANJ ASTM D422-63
% Sand a 24.5 %1 03/22/22 14:39 ANJ ASTM D422-63
% Silt, Clay, Colloids a 75.5 %1 03/22/22 14:39 ANJ ASTM D422-63
(a) Analysis performed at SGS Dayton, NJ.
RL = Reporting Limit
59 of 97
FA9349544.16
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:TMW-2-22
Lab Sample ID:FA93495-17 Date Sampled:02/28/22
Matrix:SO - Soil Date Received:03/01/22
Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Particle Size Analysis (Sieve and Hydrometer Testing)
3 Inch Sieve a 100 %1 03/22/22 14:39 ANJ ASTM D422-63
1.5 Inch Sieve a 100 %1 03/22/22 14:39 ANJ ASTM D422-63
0.75 Inch Sieve a 100 %1 03/22/22 14:39 ANJ ASTM D422-63
0.375 Inch Sieve a 100 %1 03/22/22 14:39 ANJ ASTM D422-63
No.4 Sieve (4.75 mm) a 98.5 %1 03/22/22 14:39 ANJ ASTM D422-63
No.8 Sieve (2.36 mm) a 97.8 %1 03/22/22 14:39 ANJ ASTM D422-63
No.10 Sieve (2.00 mm) a 97.5 %1 03/22/22 14:39 ANJ ASTM D422-63
No.16 Sieve (1.18 mm) a 95.9 %1 03/22/22 14:39 ANJ ASTM D422-63
No.30 Sieve (0.60 mm) a 89.2 %1 03/22/22 14:39 ANJ ASTM D422-63
No.50 Sieve (0.30 mm) a 71.1 %1 03/22/22 14:39 ANJ ASTM D422-63
No.100 Sieve (0.15 mm) a 47.4 %1 03/22/22 14:39 ANJ ASTM D422-63
No.200 Sieve (0.075 mm) a 42.4 %1 03/22/22 14:39 ANJ ASTM D422-63
0.030 mm (Hydrometer) a 38.4 %1 03/22/22 14:39 ANJ ASTM D422-63
0.005 mm (Hydrometer) a 24.7 %1 03/22/22 14:39 ANJ ASTM D422-63
0.0015 mm (Hydrometer) a 16.2 %1 03/22/22 14:39 ANJ ASTM D422-63
% Gravel a 1.5 %1 03/22/22 14:39 ANJ ASTM D422-63
% Sand a 56.1 %1 03/22/22 14:39 ANJ ASTM D422-63
% Silt, Clay, Colloids a 42.4 %1 03/22/22 14:39 ANJ ASTM D422-63
(a) Analysis performed at SGS Dayton, NJ.
RL = Reporting Limit
60 of 97
FA9349544.17
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:TMW-2-30
Lab Sample ID:FA93495-18 Date Sampled:02/28/22
Matrix:SO - Soil Date Received:03/01/22
Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Particle Size Analysis (Sieve and Hydrometer Testing)
3 Inch Sieve a 100 %1 03/22/22 14:39 ANJ ASTM D422-63
1.5 Inch Sieve a 100 %1 03/22/22 14:39 ANJ ASTM D422-63
0.75 Inch Sieve a 100 %1 03/22/22 14:39 ANJ ASTM D422-63
0.375 Inch Sieve a 100 %1 03/22/22 14:39 ANJ ASTM D422-63
No.4 Sieve (4.75 mm) a 100 %1 03/22/22 14:39 ANJ ASTM D422-63
No.8 Sieve (2.36 mm) a 100 %1 03/22/22 14:39 ANJ ASTM D422-63
No.10 Sieve (2.00 mm) a 100 %1 03/22/22 14:39 ANJ ASTM D422-63
No.16 Sieve (1.18 mm) a 99.9 %1 03/22/22 14:39 ANJ ASTM D422-63
No.30 Sieve (0.60 mm) a 99.0 %1 03/22/22 14:39 ANJ ASTM D422-63
No.50 Sieve (0.30 mm) a 96.4 %1 03/22/22 14:39 ANJ ASTM D422-63
No.100 Sieve (0.15 mm) a 90.0 %1 03/22/22 14:39 ANJ ASTM D422-63
No.200 Sieve (0.075 mm) a 84.3 %1 03/22/22 14:39 ANJ ASTM D422-63
0.030 mm (Hydrometer) a 64 %1 03/22/22 14:39 ANJ ASTM D422-63
0.005 mm (Hydrometer) a 42 %1 03/22/22 14:39 ANJ ASTM D422-63
0.0015 mm (Hydrometer) a 26 %1 03/22/22 14:39 ANJ ASTM D422-63
% Gravel a 0.0 %1 03/22/22 14:39 ANJ ASTM D422-63
% Sand a 15.7 %1 03/22/22 14:39 ANJ ASTM D422-63
% Silt, Clay, Colloids a 84.3 %1 03/22/22 14:39 ANJ ASTM D422-63
(a) Analysis performed at SGS Dayton, NJ.
RL = Reporting Limit
61 of 97
FA9349544.18
SGS North America Inc.
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Orlando, FL
Section 5
62 of 97
FA934955
FA93495: Chain of Custody
Page 1 of 3
63 of 97
FA9349555.1
FA93495: Chain of Custody
Page 2 of 3
64 of 97
FA9349555.1
Job Number:FA93495 Client:GEOLOGICAL RESOURCES INC
Date / Time Received:3/1/2022 9:50:00 AM Delivery Method:FEDEX
Project:H & S TRUDING
Airbill #'s:100963795387
Cooler Information
1. Custody Seals Present
2. Custody Seals Intact
4. Cooler temp verification
3. Temp criteria achieved
5. Cooler media
IR Gun
Ice (Bag)
Trip Blank Information
1. Trip Blank present / cooler
2. Trip Blank listed on COC
2. Samples preserved properly
Sample Information
1. Sample labels present on bottles
5. Sample recvd within HT
4. Condition of sample
3. Sufficient volume/containers recvd for analysis:
Intact
Comments
SM001Rev. Date 05/24/17
SGS Sample Receipt Summary
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
Cooler 1: (3.0);
Cooler 1: (3.4);
3. Type Of TB Received
W or S N/A
6. Dates/Times/IDs on COC match Sample Label
7. VOCs have headspace
8. Bottles received for unspecified tests
9. Compositing instructions clear
10. Voa Soil Kits/Jars received past 48hrs?
11. % Solids Jar received?
Misc. Information
25-Gram 5-GramNumber of Encores:Number of 5035 Field Kits:Number of Lab Filtered Metals:
Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify)
Y or N N/A
Y or N
Therm ID:IR 1; Therm CF:0.4; # of Coolers:1
Y or N N/A
12. Residual Chlorine Present?
Residual Chlorine Test Strip Lot #:
Technician:Reviewer:DEVANO Date:Date:3/1/2022 9:50:00 AM
FA93495: Chain of Custody
Page 3 of 3
65 of 97
FA9349555.1
SGS North America Inc.
MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 6
66 of 97
FA934956
Method Blank Summary Page 1 of 2
Job Number:FA93495
Account:GRINCC GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA3083-MB A0230859.D 1 03/09/22 JL n/a n/a VA3083
The QC reported here applies to the following samples:Method: SM 6200B
FA93495-1, FA93495-3, FA93495-4, FA93495-5, FA93495-6, FA93495-7, FA93495-8, FA93495-9, FA93495-10,
FA93495-11, FA93495-12, FA93495-13, FA93495-14
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
67 of 97
FA9349566.1.1
Method Blank Summary Page 2 of 2
Job Number:FA93495
Account:GRINCC GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA3083-MB A0230859.D 1 03/09/22 JL n/a n/a VA3083
The QC reported here applies to the following samples:Method: SM 6200B
FA93495-1, FA93495-3, FA93495-4, FA93495-5, FA93495-6, FA93495-7, FA93495-8, FA93495-9, FA93495-10,
FA93495-11, FA93495-12, FA93495-13, FA93495-14
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
68 of 97
FA9349566.1.1
Method Blank Summary Page 1 of 2
Job Number:FA93495
Account:GRINCC GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA3087-MB A0230964.D 1 03/14/22 JL n/a n/a VA3087
The QC reported here applies to the following samples:Method: SM 6200B
FA93495-1, FA93495-2, FA93495-6, FA93495-7, FA93495-12
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
69 of 97
FA9349566.1.2
Method Blank Summary Page 2 of 2
Job Number:FA93495
Account:GRINCC GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA3087-MB A0230964.D 1 03/14/22 JL n/a n/a VA3087
The QC reported here applies to the following samples:Method: SM 6200B
FA93495-1, FA93495-2, FA93495-6, FA93495-7, FA93495-12
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
70 of 97
FA9349566.1.2
Blank Spike Summary Page 1 of 2
Job Number:FA93495
Account:GRINCC GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA3083-BS A0230857.D 1 03/09/22 JL n/a n/a VA3083
The QC reported here applies to the following samples:Method: SM 6200B
FA93495-1, FA93495-3, FA93495-4, FA93495-5, FA93495-6, FA93495-7, FA93495-8, FA93495-9, FA93495-10,
FA93495-11, FA93495-12, FA93495-13, FA93495-14
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 9.5 95 70-130
108-86-1 Bromobenzene 10 9.4 94 70-130
74-97-5 Bromochloromethane 10 8.0 80 70-130
75-27-4 Bromodichloromethane 10 9.2 92 70-130
75-25-2 Bromoform 10 9.0 90 70-130
104-51-8 n-Butylbenzene 10 9.3 93 70-130
135-98-8 sec-Butylbenzene 10 10.8 108 70-130
98-06-6 tert-Butylbenzene 10 10.1 101 70-130
56-23-5 Carbon Tetrachloride 10 9.9 99 70-130
108-90-7 Chlorobenzene 10 9.2 92 70-130
75-00-3 Chloroethane 10 10.6 106 60-140
67-66-3 Chloroform 10 8.8 88 70-130
95-49-8 o-Chlorotoluene 10 9.7 97 70-130
106-43-4 p-Chlorotoluene 10 9.5 95 70-130
124-48-1 Dibromochloromethane 10 9.0 90 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 8.7 87 70-130
106-93-4 1,2-Dibromoethane 10 9.1 91 70-130
75-71-8 Dichlorodifluoromethane 10 11.1 111 60-140
95-50-1 1,2-Dichlorobenzene 10 9.4 94 70-130
541-73-1 1,3-Dichlorobenzene 10 9.6 96 70-130
106-46-7 1,4-Dichlorobenzene 10 9.1 91 70-130
75-34-3 1,1-Dichloroethane 10 9.2 92 70-130
107-06-2 1,2-Dichloroethane 10 8.8 88 70-130
75-35-4 1,1-Dichloroethylene 10 9.8 98 70-130
156-59-2 cis-1,2-Dichloroethylene 10 9.5 95 70-130
156-60-5 trans-1,2-Dichloroethylene 10 9.4 94 70-130
78-87-5 1,2-Dichloropropane 10 9.2 92 70-130
142-28-9 1,3-Dichloropropane 10 8.9 89 70-130
594-20-7 2,2-Dichloropropane 10 9.5 95 70-130
563-58-6 1,1-Dichloropropene 10 10 100 70-130
10061-01-5 cis-1,3-Dichloropropene 10 9.7 97 70-130
10061-02-6 trans-1,3-Dichloropropene 10 9.5 95 70-130
108-20-3 Di-Isopropyl Ether 10 8.7 87 70-130
100-41-4 Ethylbenzene 10 9.6 96 70-130
87-68-3 Hexachlorobutadiene 10 10.6 106 70-130
98-82-8 Isopropylbenzene 10 10.4 104 70-130
* = Outside of Control Limits.
71 of 97
FA9349566.2.1
Blank Spike Summary Page 2 of 2
Job Number:FA93495
Account:GRINCC GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA3083-BS A0230857.D 1 03/09/22 JL n/a n/a VA3083
The QC reported here applies to the following samples:Method: SM 6200B
FA93495-1, FA93495-3, FA93495-4, FA93495-5, FA93495-6, FA93495-7, FA93495-8, FA93495-9, FA93495-10,
FA93495-11, FA93495-12, FA93495-13, FA93495-14
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 9.9 99 70-130
74-83-9 Methyl Bromide 10 11.2 112 60-140
74-87-3 Methyl Chloride 10 10.2 102 60-140
74-95-3 Methylene Bromide 10 8.4 84 70-130
75-09-2 Methylene Chloride 10 9.6 96 70-130
1634-04-4 Methyl Tert Butyl Ether 10 8.4 84 70-130
91-20-3 Naphthalene 10 9.1 91 70-130
103-65-1 n-Propylbenzene 10 9.9 99 70-130
100-42-5 Styrene 10 9.2 92 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 9.8 98 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 8.9 89 70-130
127-18-4 Tetrachloroethylene 10 9.7 97 70-130
108-88-3 Toluene 10 9.4 94 70-130
87-61-6 1,2,3-Trichlorobenzene 10 9.6 96 70-130
120-82-1 1,2,4-Trichlorobenzene 10 9.9 99 70-130
71-55-6 1,1,1-Trichloroethane 10 9.4 94 70-130
79-00-5 1,1,2-Trichloroethane 10 8.9 89 70-130
79-01-6 Trichloroethylene 10 9.6 96 70-130
75-69-4 Trichlorofluoromethane 10 13.3 133 60-140
96-18-4 1,2,3-Trichloropropane 10 8.9 89 70-130
95-63-6 1,2,4-Trimethylbenzene 10 9.1 91 70-130
108-67-8 1,3,5-Trimethylbenzene 10 10.1 101 70-130
75-01-4 Vinyl Chloride 10 10.8 108 60-140
m,p-Xylene 20 19.6 98 70-130
95-47-6 o-Xylene 10 9.9 99 70-130
1330-20-7 Xylene (total)30 29.4 98 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 97%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
* = Outside of Control Limits.
72 of 97
FA9349566.2.1
Blank Spike Summary Page 1 of 2
Job Number:FA93495
Account:GRINCC GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA3087-BS A0230962.D 1 03/14/22 JL n/a n/a VA3087
The QC reported here applies to the following samples:Method: SM 6200B
FA93495-1, FA93495-2, FA93495-6, FA93495-7, FA93495-12
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 11.6 116 70-130
108-86-1 Bromobenzene 10 11.2 112 70-130
74-97-5 Bromochloromethane 10 9.6 96 70-130
75-27-4 Bromodichloromethane 10 11.3 113 70-130
75-25-2 Bromoform 10 11.0 110 70-130
104-51-8 n-Butylbenzene 10 11.2 112 70-130
135-98-8 sec-Butylbenzene 10 13.0 130 70-130
98-06-6 tert-Butylbenzene 10 12.3 123 70-130
56-23-5 Carbon Tetrachloride 10 12.2 122 70-130
108-90-7 Chlorobenzene 10 11.1 111 70-130
75-00-3 Chloroethane 10 9.2 92 60-140
67-66-3 Chloroform 10 10.7 107 70-130
95-49-8 o-Chlorotoluene 10 11.6 116 70-130
106-43-4 p-Chlorotoluene 10 11.5 115 70-130
124-48-1 Dibromochloromethane 10 10.9 109 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 10.6 106 70-130
106-93-4 1,2-Dibromoethane 10 11.0 110 70-130
75-71-8 Dichlorodifluoromethane 10 9.6 96 60-140
95-50-1 1,2-Dichlorobenzene 10 11.3 113 70-130
541-73-1 1,3-Dichlorobenzene 10 11.4 114 70-130
106-46-7 1,4-Dichlorobenzene 10 10.9 109 70-130
75-34-3 1,1-Dichloroethane 10 11.2 112 70-130
107-06-2 1,2-Dichloroethane 10 10.6 106 70-130
75-35-4 1,1-Dichloroethylene 10 11.8 118 70-130
156-59-2 cis-1,2-Dichloroethylene 10 11.3 113 70-130
156-60-5 trans-1,2-Dichloroethylene 10 11.5 115 70-130
78-87-5 1,2-Dichloropropane 10 11.3 113 70-130
142-28-9 1,3-Dichloropropane 10 10.8 108 70-130
594-20-7 2,2-Dichloropropane 10 11.9 119 70-130
563-58-6 1,1-Dichloropropene 10 12.1 121 70-130
10061-01-5 cis-1,3-Dichloropropene 10 11.8 118 70-130
10061-02-6 trans-1,3-Dichloropropene 10 11.8 118 70-130
108-20-3 Di-Isopropyl Ether 10 10.4 104 70-130
100-41-4 Ethylbenzene 10 11.6 116 70-130
87-68-3 Hexachlorobutadiene 10 12.4 124 70-130
98-82-8 Isopropylbenzene 10 12.6 126 70-130
* = Outside of Control Limits.
73 of 97
FA9349566.2.2
Blank Spike Summary Page 2 of 2
Job Number:FA93495
Account:GRINCC GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA3087-BS A0230962.D 1 03/14/22 JL n/a n/a VA3087
The QC reported here applies to the following samples:Method: SM 6200B
FA93495-1, FA93495-2, FA93495-6, FA93495-7, FA93495-12
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 12.1 121 70-130
74-83-9 Methyl Bromide 10 10 100 60-140
74-87-3 Methyl Chloride 10 9.1 91 60-140
74-95-3 Methylene Bromide 10 10.2 102 70-130
75-09-2 Methylene Chloride 10 10.6 106 70-130
1634-04-4 Methyl Tert Butyl Ether 10 10.1 101 70-130
91-20-3 Naphthalene 10 10.6 106 70-130
103-65-1 n-Propylbenzene 10 11.8 118 70-130
100-42-5 Styrene 10 11.1 111 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 11.8 118 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 11.0 110 70-130
127-18-4 Tetrachloroethylene 10 11.6 116 70-130
108-88-3 Toluene 10 11.4 114 70-130
87-61-6 1,2,3-Trichlorobenzene 10 11.1 111 70-130
120-82-1 1,2,4-Trichlorobenzene 10 11.5 115 70-130
71-55-6 1,1,1-Trichloroethane 10 11.5 115 70-130
79-00-5 1,1,2-Trichloroethane 10 10.8 108 70-130
79-01-6 Trichloroethylene 10 11.4 114 70-130
75-69-4 Trichlorofluoromethane 10 12.6 126 60-140
96-18-4 1,2,3-Trichloropropane 10 10.6 106 70-130
95-63-6 1,2,4-Trimethylbenzene 10 11.1 111 70-130
108-67-8 1,3,5-Trimethylbenzene 10 12.3 123 70-130
75-01-4 Vinyl Chloride 10 9.9 99 60-140
m,p-Xylene 20 23.8 119 70-130
95-47-6 o-Xylene 10 11.9 119 70-130
1330-20-7 Xylene (total)30 35.7 119 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 97%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
* = Outside of Control Limits.
74 of 97
FA9349566.2.2
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA93495
Account:GRINCC GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA93495-12MS A0230882.D 5 03/09/22 JL n/a n/a VA3083
FA93495-12MSD A0230883.D 5 03/09/22 JL n/a n/a VA3083
FA93495-12 A0230881.D 5 03/09/22 JL n/a n/a VA3083
The QC reported here applies to the following samples:Method: SM 6200B
FA93495-1, FA93495-3, FA93495-4, FA93495-5, FA93495-6, FA93495-7, FA93495-8, FA93495-9, FA93495-10,
FA93495-11, FA93495-12, FA93495-13, FA93495-14
FA93495-12 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 5.8 50 63.6 116 50 61.9 112 3 70-130/20
108-86-1 Bromobenzene ND 50 55.1 110 50 52.6 105 5 70-130/20
74-97-5 Bromochloromethane ND 50 47.3 95 50 46.0 92 3 70-130/20
75-27-4 Bromodichloromethane ND 50 49.6 99 50 47.8 96 4 70-130/20
75-25-2 Bromoform ND 50 36.0 72 50 36.0 72 0 70-130/20
104-51-8 n-Butylbenzene 2.0 J 50 50.4 97 50 49.5 95 2 70-130/20
135-98-8 sec-Butylbenzene 3.9 50 63.8 120 50 61.2 115 4 70-130/20
98-06-6 tert-Butylbenzene ND 50 61.5 123 50 58.5 117 5 70-130/20
56-23-5 Carbon Tetrachloride ND 50 55.6 111 50 54.6 109 2 70-130/20
108-90-7 Chlorobenzene ND 50 54.7 109 50 52.6 105 4 70-130/20
75-00-3 Chloroethane 1.4 J 50 79.1 155*50 48.3 94 48*60-140/20
67-66-3 Chloroform ND 50 52.8 106 50 50.7 101 4 70-130/20
95-49-8 o-Chlorotoluene ND 50 58.1 116 50 55.7 111 4 70-130/20
106-43-4 p-Chlorotoluene ND 50 55.0 110 50 53.3 107 3 70-130/20
124-48-1 Dibromochloromethane ND 50 43.8 88 50 42.2 84 4 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 50 57.3 115 50 58.5 117 2 70-130/20
106-93-4 1,2-Dibromoethane ND 50 55.3 111 50 54.2 108 2 70-130/20
75-71-8 Dichlorodifluoromethane ND 50 63.6 127 50 52.4 105 19 60-140/20
95-50-1 1,2-Dichlorobenzene ND 50 55.6 111 50 54.4 109 2 70-130/20
541-73-1 1,3-Dichlorobenzene ND 50 55.0 110 50 53.7 107 2 70-130/20
106-46-7 1,4-Dichlorobenzene ND 50 51.5 103 50 49.9 100 3 70-130/20
75-34-3 1,1-Dichloroethane ND 50 55.3 111 50 53.5 107 3 70-130/20
107-06-2 1,2-Dichloroethane ND 50 52.1 104 50 50.8 102 3 70-130/20
75-35-4 1,1-Dichloroethylene ND 50 57.7 115 50 55.6 111 4 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 50 56.2 112 50 55.1 110 2 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 50 56.1 112 50 54.5 109 3 70-130/20
78-87-5 1,2-Dichloropropane ND 50 54.7 109 50 53.4 107 2 70-130/20
142-28-9 1,3-Dichloropropane ND 50 53.3 107 50 52.5 105 2 70-130/20
594-20-7 2,2-Dichloropropane ND 50 50.0 100 50 48.6 97 3 70-130/20
563-58-6 1,1-Dichloropropene ND 50 60.1 120 50 58.0 116 4 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 50 50.8 102 50 49.5 99 3 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 50 51.9 104 50 50.2 100 3 70-130/20
108-20-3 Di-Isopropyl Ether 10.1 50 64.5 109 50 63.0 106 2 70-130/20
100-41-4 Ethylbenzene ND 50 57.3 115 50 55.8 112 3 70-130/20
87-68-3 Hexachlorobutadiene ND 50 45.9 92 50 44.9 90 2 70-130/20
98-82-8 Isopropylbenzene 1.0 J 50 64.1 126 50 62.5 123 3 70-130/20
* = Outside of Control Limits.
75 of 97
FA9349566.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA93495
Account:GRINCC GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA93495-12MS A0230882.D 5 03/09/22 JL n/a n/a VA3083
FA93495-12MSD A0230883.D 5 03/09/22 JL n/a n/a VA3083
FA93495-12 A0230881.D 5 03/09/22 JL n/a n/a VA3083
The QC reported here applies to the following samples:Method: SM 6200B
FA93495-1, FA93495-3, FA93495-4, FA93495-5, FA93495-6, FA93495-7, FA93495-8, FA93495-9, FA93495-10,
FA93495-11, FA93495-12, FA93495-13, FA93495-14
FA93495-12 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene 9.2 50 62.7 107 50 61.7 105 2 70-130/20
74-83-9 Methyl Bromide ND 50 73.7 147*50 51.3 103 36*60-140/20
74-87-3 Methyl Chloride 2.2 J 50 60.1 116 50 49.9 95 19 60-140/20
74-95-3 Methylene Bromide ND 50 49.8 100 50 48.9 98 2 70-130/20
75-09-2 Methylene Chloride ND 50 51.1 102 50 49.9 100 2 70-130/20
1634-04-4 Methyl Tert Butyl Ether 127 50 191 128 50 195 136* a 2 70-130/20
91-20-3 Naphthalene 12.0 50 65.7 107 50 66.6 109 1 70-130/20
103-65-1 n-Propylbenzene 0.82 J 50 58.9 116 50 56.4 111 4 70-130/20
100-42-5 Styrene ND 50 55.1 110 50 53.8 108 2 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 50 57.7 115 50 55.8 112 3 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 50 63.7 127 50 57.0 114 11 70-130/20
127-18-4 Tetrachloroethylene ND 50 55.9 112 50 54.6 109 2 70-130/20
108-88-3 Toluene ND 50 56.9 114 50 55.0 110 3 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 50 56.2 112 50 56.4 113 0 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 50 55.7 111 50 56.0 112 1 70-130/20
71-55-6 1,1,1-Trichloroethane ND 50 55.6 111 50 54.1 108 3 70-130/20
79-00-5 1,1,2-Trichloroethane ND 50 56.8 114 50 56.1 112 1 70-130/20
79-01-6 Trichloroethylene ND 50 51.5 103 50 52.0 104 1 70-130/20
75-69-4 Trichlorofluoromethane ND 50 75.2 150*50 59.6 119 23*60-140/20
96-18-4 1,2,3-Trichloropropane ND 50 54.4 109 50 51.6 103 5 70-130/20
95-63-6 1,2,4-Trimethylbenzene 13.4 50 66.7 107 50 65.4 104 2 70-130/20
108-67-8 1,3,5-Trimethylbenzene 10.3 50 70.0 119 50 68.4 116 2 70-130/20
75-01-4 Vinyl Chloride ND 50 61.5 123 50 52.8 106 15 60-140/20
m,p-Xylene ND 100 119 119 100 115 115 3 70-130/20
95-47-6 o-Xylene ND 50 61.2 122 50 59.1 118 3 70-130/20
1330-20-7 Xylene (total)ND 150 180 120 150 174 116 3 70-130/20
CAS No.Surrogate Recoveries MS MSD FA93495-12 Limits
1868-53-7 Dibromofluoromethane 103%100%104%70-130%
17060-07-0 1,2-Dichloroethane-D4 95%96%100%70-130%
2037-26-5 Toluene-D8 100%100%99%70-130%
460-00-4 4-Bromofluorobenzene 104%102%103%70-130%
(a) Outside control limits due to high level in sample relative to spike amount.
* = Outside of Control Limits.
76 of 97
FA9349566.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA93495
Account:GRINCC GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA93619-3MS A0230988.D 5 03/14/22 JL n/a n/a VA3087
FA93619-3MSD A0230989.D 5 03/14/22 JL n/a n/a VA3087
FA93619-3 A0230966.D 1 03/14/22 JL n/a n/a VA3087
The QC reported here applies to the following samples:Method: SM 6200B
FA93495-1, FA93495-2, FA93495-6, FA93495-7, FA93495-12
FA93619-3 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene ND 50 63.9 128 50 56.5 113 12 70-130/20
108-86-1 Bromobenzene ND 50 60.8 122 50 54.0 108 12 70-130/20
74-97-5 Bromochloromethane ND 50 53.0 106 50 46.9 94 12 70-130/20
75-27-4 Bromodichloromethane ND 50 59.6 119 50 51.6 103 14 70-130/20
75-25-2 Bromoform ND 50 51.6 103 50 45.2 90 13 70-130/20
104-51-8 n-Butylbenzene ND 50 60.0 120 50 53.1 106 12 70-130/20
135-98-8 sec-Butylbenzene ND 50 71.4 143*50 63.0 126 13 70-130/20
98-06-6 tert-Butylbenzene ND 50 68.2 136*50 59.9 120 13 70-130/20
56-23-5 Carbon Tetrachloride ND 50 63.7 127 50 57.6 115 10 70-130/20
108-90-7 Chlorobenzene ND 50 60.7 121 50 54.0 108 12 70-130/20
75-00-3 Chloroethane ND 50 40.4 81 50 46.9 94 15 60-140/20
67-66-3 Chloroform ND 50 58.4 117 50 51.4 103 13 70-130/20
95-49-8 o-Chlorotoluene ND 50 63.5 127 50 56.6 113 11 70-130/20
106-43-4 p-Chlorotoluene ND 50 62.8 126 50 55.9 112 12 70-130/20
124-48-1 Dibromochloromethane ND 50 54.7 109 50 48.1 96 13 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 50 60.7 121 50 52.2 104 15 70-130/20
106-93-4 1,2-Dibromoethane ND 50 61.5 123 50 54.6 109 12 70-130/20
75-71-8 Dichlorodifluoromethane ND 50 46.6 93 50 52.7 105 12 60-140/20
95-50-1 1,2-Dichlorobenzene ND 50 62.1 124 50 54.8 110 12 70-130/20
541-73-1 1,3-Dichlorobenzene ND 50 62.8 126 50 55.6 111 12 70-130/20
106-46-7 1,4-Dichlorobenzene ND 50 58.3 117 50 52.2 104 11 70-130/20
75-34-3 1,1-Dichloroethane ND 50 61.6 123 50 54.5 109 12 70-130/20
107-06-2 1,2-Dichloroethane ND 50 58.3 117 50 51.4 103 13 70-130/20
75-35-4 1,1-Dichloroethylene ND 50 63.7 127 50 56.5 113 12 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 50 63.5 127 50 55.3 111 14 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 50 62.5 125 50 55.1 110 13 70-130/20
78-87-5 1,2-Dichloropropane ND 50 63.0 126 50 55.4 111 13 70-130/20
142-28-9 1,3-Dichloropropane ND 50 59.8 120 50 53.0 106 12 70-130/20
594-20-7 2,2-Dichloropropane ND 50 60.7 121 50 51.9 104 16 70-130/20
563-58-6 1,1-Dichloropropene ND 50 66.6 133*50 59.0 118 12 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 50 60.6 121 50 53.5 107 12 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 50 60.7 121 50 53.5 107 13 70-130/20
108-20-3 Di-Isopropyl Ether ND 50 58.8 118 50 52.0 104 12 70-130/20
100-41-4 Ethylbenzene ND 50 64.1 128 50 56.6 113 12 70-130/20
87-68-3 Hexachlorobutadiene ND 50 65.0 130 50 56.6 113 14 70-130/20
98-82-8 Isopropylbenzene ND 50 70.2 140*50 62.1 124 12 70-130/20
* = Outside of Control Limits.
77 of 97
FA9349566.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA93495
Account:GRINCC GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA93619-3MS A0230988.D 5 03/14/22 JL n/a n/a VA3087
FA93619-3MSD A0230989.D 5 03/14/22 JL n/a n/a VA3087
FA93619-3 A0230966.D 1 03/14/22 JL n/a n/a VA3087
The QC reported here applies to the following samples:Method: SM 6200B
FA93495-1, FA93495-2, FA93495-6, FA93495-7, FA93495-12
FA93619-3 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 50 66.6 133*50 58.3 117 13 70-130/20
74-83-9 Methyl Bromide ND 50 42.6 85 50 49.5 99 15 60-140/20
74-87-3 Methyl Chloride ND 50 44.5 89 50 52.1 104 16 60-140/20
74-95-3 Methylene Bromide ND 50 56.0 112 50 49.2 98 13 70-130/20
75-09-2 Methylene Chloride ND 50 57.4 115 50 50.9 102 12 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 50 56.8 114 50 50.0 100 13 70-130/20
91-20-3 Naphthalene ND 50 62.2 124 50 53.5 107 15 70-130/20
103-65-1 n-Propylbenzene ND 50 65.3 131*50 58.2 116 11 70-130/20
100-42-5 Styrene ND 50 62.2 124 50 54.3 109 14 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 50 64.7 129 50 56.3 113 14 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 50 63.4 127 50 56.1 112 12 70-130/20
127-18-4 Tetrachloroethylene ND 50 63.0 126 50 56.1 112 12 70-130/20
108-88-3 Toluene ND 50 63.6 127 50 56.7 113 11 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 50 63.2 126 50 53.8 108 16 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 50 65.0 130 50 56.2 112 15 70-130/20
71-55-6 1,1,1-Trichloroethane ND 50 62.6 125 50 55.6 111 12 70-130/20
79-00-5 1,1,2-Trichloroethane ND 50 60.4 121 50 52.8 106 13 70-130/20
79-01-6 Trichloroethylene ND 50 60.3 121 50 53.3 107 12 70-130/20
75-69-4 Trichlorofluoromethane ND 50 54.2 108 50 63.5 127 16 60-140/20
96-18-4 1,2,3-Trichloropropane ND 50 58.8 118 50 51.4 103 13 70-130/20
95-63-6 1,2,4-Trimethylbenzene ND 50 60.5 121 50 53.7 107 12 70-130/20
108-67-8 1,3,5-Trimethylbenzene ND 50 67.0 134*50 59.7 119 12 70-130/20
75-01-4 Vinyl Chloride ND 50 45.8 92 50 52.9 106 14 60-140/20
m,p-Xylene ND 100 132 132*100 116 116 13 70-130/20
95-47-6 o-Xylene ND 50 67.4 135*50 59.5 119 12 70-130/20
1330-20-7 Xylene (total)ND 150 199 133*150 176 117 12 70-130/20
CAS No.Surrogate Recoveries MS MSD FA93619-3 Limits
1868-53-7 Dibromofluoromethane 99%99%102%70-130%
17060-07-0 1,2-Dichloroethane-D4 96%95%104%70-130%
2037-26-5 Toluene-D8 100%100%100%70-130%
460-00-4 4-Bromofluorobenzene 102%102%98%70-130%
* = Outside of Control Limits.
78 of 97
FA9349566.3.2
SGS North America Inc.
GC Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 7
79 of 97
FA934957
Method Blank Summary Page 1 of 1
Job Number:FA93495
Account:GRINCC GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
GLL2694-MB LL77557.D 1 03/02/22 TD n/a n/a GLL2694
The QC reported here applies to the following samples:Method: RSKSOP-147/175
FA93495-1, FA93495-2, FA93495-3, FA93495-4, FA93495-5, FA93495-6, FA93495-7
CAS No.Compound Result RL MDL Units Q
74-82-8 Methane ND 0.50 0.16 ug/l
80 of 97
FA9349577.1.1
Method Blank Summary Page 1 of 1
Job Number:FA93495
Account:GRINCC GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
G1R284-MB 1R7480.D 1 03/04/22 TD n/a n/a G1R284
The QC reported here applies to the following samples:Method: RSKSOP-147/175
FA93495-6
CAS No.Compound Result RL MDL Units Q
74-82-8 Methane ND 0.50 0.16 ug/l
81 of 97
FA9349577.1.2
Blank Spike/Blank Spike Duplicate Summary Page 1 of 1
Job Number:FA93495
Account:GRINCC GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
GLL2694-BS LL77554.D 1 03/02/22 TD n/a n/a GLL2694
GLL2694-BSD LL77555.D 1 03/02/22 TD n/a n/a GLL2694
The QC reported here applies to the following samples:Method: RSKSOP-147/175
FA93495-1, FA93495-2, FA93495-3, FA93495-4, FA93495-5, FA93495-6, FA93495-7
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/l ug/l %ug/l %RPD Rec/RPD
74-82-8 Methane 108 105 97 119 110 13 62-139/30
* = Outside of Control Limits.
82 of 97
FA9349577.2.1
Blank Spike/Blank Spike Duplicate Summary Page 1 of 1
Job Number:FA93495
Account:GRINCC GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
G1R284-BS 1R7477.D 1 03/04/22 TD n/a n/a G1R284
G1R284-BSD 1R7481.D 1 03/04/22 TD n/a n/a G1R284
The QC reported here applies to the following samples:Method: RSKSOP-147/175
FA93495-6
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/l ug/l %ug/l %RPD Rec/RPD
74-82-8 Methane 108 104 96 110 102 6 62-139/30
* = Outside of Control Limits.
83 of 97
FA9349577.2.2
Matrix Spike Summary Page 1 of 1
Job Number:FA93495
Account:GRINCC GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA93495-2MS LL77573.D 1 03/02/22 TD n/a n/a GLL2694
FA93495-2 LL77566.D 1 03/02/22 TD n/a n/a GLL2694
The QC reported here applies to the following samples:Method: RSKSOP-147/175
FA93495-1, FA93495-2, FA93495-3, FA93495-4, FA93495-5, FA93495-6, FA93495-7
FA93495-2 Spike MS MS
CAS No.Compound ug/l Q ug/l ug/l %Limits
74-82-8 Methane 95.3 108 208 104 62-139
* = Outside of Control Limits.
84 of 97
FA9349577.3.1
Matrix Spike Summary Page 1 of 1
Job Number:FA93495
Account:GRINCC GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA93558-4MS 1R7496.D 1 03/04/22 TD n/a n/a G1R284
FA93558-4 1R7490.D 1 03/04/22 TD n/a n/a G1R284
The QC reported here applies to the following samples:Method: RSKSOP-147/175
FA93495-6
FA93558-4 Spike MS MS
CAS No.Compound ug/l Q ug/l ug/l %Limits
74-82-8 Methane 0.32 J 108 122 113 62-139
* = Outside of Control Limits.
85 of 97
FA9349577.3.2
Duplicate Summary Page 1 of 1
Job Number:FA93495
Account:GRINCC GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA93495-1DUP LL77572.D 1 03/02/22 TD n/a n/a GLL2694
FA93495-1 LL77563.D 1 03/02/22 TD n/a n/a GLL2694
The QC reported here applies to the following samples:Method: RSKSOP-147/175
FA93495-1, FA93495-2, FA93495-3, FA93495-4, FA93495-5, FA93495-6, FA93495-7
FA93495-1 DUP
CAS No.Compound ug/l Q ug/l Q RPD Limits
74-82-8 Methane 767 711 8 30
* = Outside of Control Limits.
86 of 97
FA9349577.4.1
Duplicate Summary Page 1 of 1
Job Number:FA93495
Account:GRINCC GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA93558-4DUP 1R7495.D 1 03/04/22 TD n/a n/a G1R284
FA93558-4 1R7490.D 1 03/04/22 TD n/a n/a G1R284
The QC reported here applies to the following samples:Method: RSKSOP-147/175
FA93495-6
FA93558-4 DUP
CAS No.Compound ug/l Q ug/l Q RPD Limits
74-82-8 Methane 0.32 J 0.18 J 56*30
* = Outside of Control Limits.
87 of 97
FA9349577.4.2
SGS North America Inc.
General Chemistry
QC Data Summaries
Includes the following where applicable:
• Method Blank and Blank Spike Summaries
• Duplicate Summaries
• Matrix Spike Summaries
Orlando, FL
Section 8
88 of 97
FA934958
METHOD BLANK AND SPIKE RESULTS SUMMARY
GENERAL CHEMISTRY
Login Number: FA93495
Account: GRINCC - GRI (Geological Resources Inc.)
Project: H&S Trading; 211 Tunis Rd, Tunis, NC
MB Spike BSP BSP QC
Analyte Batch ID RL Result Units Amount Result %Recov Limits
Chloride GP37459/GN90696 2.0 0.0 mg/l 50 50.5 101.0 90-110%
Iron, Ferrous GN90760 0.10 0.0 mg/l 0.500 0.50 100.8 82-115%
Nitrogen, Nitrate GP37459/GN90696 0.10 0.0 mg/l 2.5 2.44 97.6 90-110%
Sulfate GP37459/GN90696 2.0 0.0 mg/l 50 51.0 102.0 90-110%
Associated Samples:
Batch GN90760: FA93495-1, FA93495-2, FA93495-3, FA93495-4, FA93495-5, FA93495-6, FA93495-7
Batch GP37459: FA93495-1, FA93495-2, FA93495-3, FA93495-4, FA93495-5, FA93495-6, FA93495-7
(*) Outside of QC limits
__________________________________________________________________________________________________________________________
Page 1
89 of 97
FA9349588.1
DUPLICATE RESULTS SUMMARY
GENERAL CHEMISTRY
Login Number: FA93495
Account: GRINCC - GRI (Geological Resources Inc.)
Project: H&S Trading; 211 Tunis Rd, Tunis, NC
QC Original DUP QC
Analyte Batch ID Sample Units Result Result RPD Limits
Iron, Ferrous GN90760 FA93495-1 mg/l 9.5 9.4 1.0 0-31%
Associated Samples:
Batch GN90760: FA93495-1, FA93495-2, FA93495-3, FA93495-4, FA93495-5, FA93495-6, FA93495-7
(*) Outside of QC limits
__________________________________________________________________________________________________________________________
Page 1
90 of 97
FA9349588.2
MATRIX SPIKE RESULTS SUMMARY
GENERAL CHEMISTRY
Login Number: FA93495
Account: GRINCC - GRI (Geological Resources Inc.)
Project: H&S Trading; 211 Tunis Rd, Tunis, NC
QC Original Spike MS QC
Analyte Batch ID Sample Units Result Amount Result %Rec Limits
Chloride GP37459/GN90696 FA93495-1 mg/l 18.0 50 65.6 95.2 90-110%
Nitrogen, Nitrate GP37459/GN90696 FA93495-1 mg/l 0.34 2.5 2.7 94.4 90-110%
Sulfate GP37459/GN90696 FA93495-1 mg/l 5.5 50 56.5 102.0 90-110%
Associated Samples:
Batch GP37459: FA93495-1, FA93495-2, FA93495-3, FA93495-4, FA93495-5, FA93495-6, FA93495-7
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
__________________________________________________________________________________________________________________________
Page 1
91 of 97
FA9349588.3
MATRIX SPIKE DUPLICATE RESULTS SUMMARY
GENERAL CHEMISTRY
Login Number: FA93495
Account: GRINCC - GRI (Geological Resources Inc.)
Project: H&S Trading; 211 Tunis Rd, Tunis, NC
QC Original Spike MSD QC
Analyte Batch ID Sample Units Result Amount Result RPD Limit
Chloride GP37459/GN90696 FA93495-1 mg/l 18.0 50 65.5 0.2 15%
Nitrogen, Nitrate GP37459/GN90696 FA93495-1 mg/l 0.34 2.5 2.7 0.0 15%
Sulfate GP37459/GN90696 FA93495-1 mg/l 5.5 50 56.5 0.0 15%
Associated Samples:
Batch GP37459: FA93495-1, FA93495-2, FA93495-3, FA93495-4, FA93495-5, FA93495-6, FA93495-7
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
__________________________________________________________________________________________________________________________
Page 1
92 of 97
FA9349588.4
SGS North America Inc.
Misc. Forms
Custody Documents and Other Forms
(SGS Dayton, NJ)
Includes the following where applicable:
• Chain of Custody
Orlando, FL
Section 9
93 of 97
FA934959
)1) CHAIN OF CUSTODY
SGS North America Inc. -Orlando
Page 1of2
FED-EX Tracking# Bottle Order Control # 1 t:..100 ·7~( )j "3"'-ib
SGS Quote# SGS Job# FA93495
---- ------
Client I Reporting Information Project Information Reauested Analvsis I see TEST CODE sheet} Matrix Codes
Company Name: Project Name:
SGS North America Inc. H&S Trading; 211 Tunis Rd, Tunis, NC DW -Drinking Water
GW -Ground Water
Street Address Street WW-Water
4405 Vineland Rd, Suite C-15 SW -Surtace Water Billing Information ( if different from Report to) SO· Soil City State Zip City State Company Name SL-Sludge
Orlando FL 32811 SEO-Sediment
QI. Oil Project Contact E-mail Project# Street Address LIQ -Other liquid
[e-mail] AIR-Air
Phone# Fax# Client Purchase Order# City State Zip SOL -Other Solid
WP-Wipe
407-425-6700 FB-Field Blank
Sample«s) Name(s) Phone Project Manager Attention: EB-Equipment Blank
RB-Rinse Blank JBAD TB-Trip Blank
CoHection Number of preserved Bottles en "' z ~ ~ I 0: ;;:;: SGS Sampled I 8 ~ "' 0 0 z 0 0 D:'. Sample# Field ID I Point of Collection MEOH/01 Vial# Date Time by Matrix #of bottles ~ ~ z 0 6 "' z t9 LAB USE ONLY I I z " "'
15 TMW-1-22 2/28/22 11:18:00AN JBAD so 1 x x \)\Tl.l -"' 16 TMW-1-30 2/28/22 11:23:00 AN JBAD so 1 x x
17 TMW-2-22 2/28/22 11:41:00 AN JBAD so 1 x x
18 TMW-2-30 2/28/22 11:47:00 AN JBAD so 1 x x
Turnaround Time (Business days) Data Deliverable Information Comments I Special Instructions
Approved By (SGS PM)' I Date' D Commercial "A" (Level 1) D State Forms Send to N.J... 0 Standard 10 Day (business) CJ Commercial "B" ( Level 2) 0 EDD Format
0 5 Business Days RUSH D REDT1 ( Level 3) 0 Other lniaaf~GC rA-D 3 Business Days RUSH D FUL T1 ( Level 4) D 0 2 Business Days RUSH D Commercial "C" 00 (.;l l.aiMf Yerlfca1iain O 1 Business Day EMERGENCY Commercial "A"= Results Onl
00 other 21 Commercial "B" = Results + QC Summary
Emergency & Rush T/A data available via Lablink Approval needed for RUSH/Emergency TAT Commercial "C" = Results + QC Summary + Partial Raw data htto://www.sos.com/en/terms-and-conditions
Sample Custody must be documented below each time samples change possession, including courier delivery.
1 Ref:ij~~ D]l~i;7 I 7:u.; Received By~ Relinquished By: D~/?62:~ ;eceived By' ()..J\1¥V\Q./,,L ~~ 1 ·-e/~ 2 rJ~<--Date Time: f I Relinquished by Sampler: Received By: Relinquished By: Date Time: Received By:
3 3 4 4 /
Relinquished by: Date Time: Received By: Custody Seal # D Intact Preserved where applicable o~ Cooler TempJ., ,
5 5 D D 1 • .., ~~ Not intact Therm ID •i.)
FA93495: Chain of Custody
Page 1 of 2
SGS Dayton, NJ
94 of 97
FA9349599.1
Job Number:FA93495 Client:
Date / Time Received:3/3/2022 10:10:00 AM Delivery Method:Fed Ex
Project:
4. No. Coolers:1
Airbill #'s:5700 7347 8346
Cooler Security
1. Custody Seals Present:
Y or N
2. Custody Seals Intact:
3. COC Present:
4. Smpl Dates/Time OK
2. Cooler temp verification:
Cooler Temperature Y or N
1. Temp criteria achieved:
3. Cooler media:
IR Gun
Ice (Bag)
Quality Control Preservation Y or N N/A
1. Trip Blank present / cooler:
2. Trip Blank listed on COC:
3. Samples preserved properly:
4. VOCs headspace free:
Sample Integrity - Documentation Y or N
1. Sample labels present on bottles:
2. Container labeling complete:
3. Sample container label / COC agree:
Sample Integrity - Condition Y or N
1. Sample recvd within HT:
3. Condition of sample:
2. All containers accounted for:
Sample Integrity - Instructions
1. Analysis requested is clear:
2. Bottles received for unspecified tests
3. Sufficient volume recvd for analysis:
4. Compositing instructions clear:
5. Filtering instructions clear:
Intact
Y or N
Comments
Y or N N/A
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
Cooler 1: (3.5);
Cooler 1: (1.9);
SM089-03Rev. Date 12/7/17
SGS Sample Receipt Summary
Test Strip Lot #s:pH 1-12:231619 pH 12+:203117A Other: (Specify)
FA93495: Chain of Custody
Page 2 of 2
95 of 97
FA9349599.1
SGS North America Inc.
General Chemistry
QC Data Summaries
(SGS Dayton, NJ)
Includes the following where applicable:
• Method Blank and Blank Spike Summaries
• Duplicate Summaries
• Matrix Spike Summaries
Orlando, FL
Section 10
96 of 97
FA9349510
DUPLICATE RESULTS SUMMARY
GENERAL CHEMISTRY
Login Number: FA93495
Account: ALSE - SGS Orlando, FL
Project: GRINCC: H&S Trading; 211 Tunis Rd, Tunis, NC
QC Original DUP QC
Analyte Batch ID Sample Units Result Result RPD Limits
% Gravel GP38862/GN27477 FA93495-17 % 1.5 1.5 -0.7 0-41%
% Sand GP38862/GN27477 FA93495-17 % 56.1 54.4 -3.1 0-16%
% Silt, Clay, Colloids GP38862/GN27477 FA93495-17 % 42.4 44.1 4.0 0-40%
0.0015 mm (Hydrometer) GP38862/GN27477 FA93495-17 % 16.2 16.2 -0.1 0-45%
0.005 mm (Hydrometer) GP38862/GN27477 FA93495-17 % 24.7 24.7 -0.1 0-48%
0.030 mm (Hydrometer) GP38862/GN27477 FA93495-17 % 38.4 40.1 4.3 0-36%
0.375 Inch Sieve GP38862/GN27477 FA93495-17 % 100 100 0.0 0-14%
0.75 Inch Sieve GP38862/GN27477 FA93495-17 % 100 100 0.0 0-9%
1.5 Inch Sieve GP38862/GN27477 FA93495-17 % 100 100 0.0 0-20%
3 Inch Sieve GP38862/GN27477 FA93495-17 % 100 100 0.0 0-20%
No.10 Sieve (2.00 mm) GP38862/GN27477 FA93495-17 % 97.5 97.5 0.0 0-14%
No.100 Sieve (0.15 mm) GP38862/GN27477 FA93495-17 % 47.4 49.2 3.7 0-31%
No.16 Sieve (1.18 mm) GP38862/GN27477 FA93495-17 % 95.9 95.7 -0.3 0-17%
No.200 Sieve (0.075 mm) GP38862/GN27477 FA93495-17 % 42.4 44.1 4.3 0-40%
No.30 Sieve (0.60 mm) GP38862/GN27477 FA93495-17 % 89.2 88.1 -1.2 0-21%
No.4 Sieve (4.75 mm) GP38862/GN27477 FA93495-17 % 98.5 98.5 0.0 0-13%
No.50 Sieve (0.30 mm) GP38862/GN27477 FA93495-17 % 71.1 71.5 0.6 0-30%
No.8 Sieve (2.36 mm) GP38862/GN27477 FA93495-17 % 97.8 97.8 0.0 0-14%
Associated Samples:
Batch GP38862: FA93495-15, FA93495-16, FA93495-17, FA93495-18
(*) Outside of QC limits
__________________________________________________________________________________________________________________________
Page 1
97 of 97
FA934951010.1
03/21/22
Technical Report for
GRI (Geological Resources Inc.)
H&S Trading; 211 Tunis Rd, Tunis, NC
10151/2632
SGS Job Number: FA93564
Sampling Date: 03/02/22
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
[e-mail]; [e-mail];
[e-mail]; [e-mail]
ATTN: William Regenthall
Total number of pages in report:
Certifications: FL(E83510), LA(03051), KS(E-10327), NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AL, AK, AR, CT, IA, KY, MA, MI. MS, ND, NH, NV, OK, OR, IL, UT, VT, WA, WI, WV
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone]
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Norm Farmer
Technical Director
Orlando, FL 03/21/22
e-Hardcopy 2.0
Automated Report
20
SGS is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
Review standard terms at: http://www.sgs.com/en/terms-and-conditions
The results set forth herein are provided by SGS North America Inc.
Please share your ideas about
how we can serve you better at:
[e-mail]
1 of 20
FA93564
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................5
3.1: FA93564-1: TMW-2 .....................................................................................................6
Section 4: Misc. Forms ............................................................................................................8
4.1: Chain of Custody ...........................................................................................................9
Section 5: MS Volatiles - QC Data Summaries .....................................................................11
5.1: Method Blank Summary ................................................................................................12
5.2: Blank Spike Summary ...................................................................................................15
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................18 123452 of 20
FA93564
SGS North America Inc.
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA93564
H&S Trading; 211 Tunis Rd, Tunis, NC
Project No: 10151/2632
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
This report contains results reported as ND = Not detected. The following applies:
Organics ND = Not detected above the MDL
FA93564-1 03/02/22 15:19 JB 03/03/22 AQ Ground Water TMW-2
3 of 20
FA935641
Summary of Hits Page 1 of 1
Job Number:FA93564
Account:GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Collected:03/02/22
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA93564-1 TMW-2
Benzene 30.6 13 3.1 ug/l SM 6200B
sec-Butylbenzene 5.5 J 13 3.1 ug/l SM 6200B
Di-Isopropyl Ether 11.1 J 13 3.1 ug/l SM 6200B
Ethylbenzene 97.5 13 3.1 ug/l SM 6200B
Isopropylbenzene 11.0 J 13 3.1 ug/l SM 6200B
p-Isopropyltoluene 4.6 J 13 3.1 ug/l SM 6200B
Methyl Tert Butyl Ether 2650 50 13 ug/l SM 6200B
Naphthalene 19.0 13 3.1 ug/l SM 6200B
n-Propylbenzene 19.2 13 3.1 ug/l SM 6200B
1,2,4-Trimethylbenzene 220 13 3.1 ug/l SM 6200B
1,3,5-Trimethylbenzene 92.5 13 3.1 ug/l SM 6200B
m,p-Xylene 404 25 3.1 ug/l SM 6200B
o-Xylene 88.8 13 3.1 ug/l SM 6200B
Xylene (total)493 38 6.3 ug/l SM 6200B
4 of 20
FA935642
SGS North America Inc.
Sample Results
Report of Analysis
Orlando, FL
Section 3
5 of 20
FA935643
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:TMW-2
Lab Sample ID:FA93564-1 Date Sampled:03/02/22
Matrix:AQ - Ground Water Date Received:03/03/22
Method:SM 6200B Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0230924.D 25 03/11/22 01:19 JL n/a n/a VA3085
Run #2 A0231014.D 100 03/15/22 19:15 JL n/a n/a VA3088
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 30.6 13 3.1 ug/l
108-86-1 Bromobenzene ND 13 3.1 ug/l
74-97-5 Bromochloromethane ND 13 3.1 ug/l
75-27-4 Bromodichloromethane ND 13 3.1 ug/l
75-25-2 Bromoform ND 13 3.1 ug/l
104-51-8 n-Butylbenzene ND 13 3.1 ug/l
135-98-8 sec-Butylbenzene 5.5 13 3.1 ug/l J
98-06-6 tert-Butylbenzene ND 13 3.1 ug/l
56-23-5 Carbon Tetrachloride ND 13 3.1 ug/l
108-90-7 Chlorobenzene ND 13 3.1 ug/l
75-00-3 Chloroethane ND 13 5.0 ug/l
67-66-3 Chloroform ND 13 3.1 ug/l
95-49-8 o-Chlorotoluene ND 13 3.1 ug/l
106-43-4 p-Chlorotoluene ND 13 3.1 ug/l
124-48-1 Dibromochloromethane ND 13 3.1 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 13 6.2 ug/l
106-93-4 1,2-Dibromoethane ND 13 3.1 ug/l
75-71-8 Dichlorodifluoromethane ND 13 5.0 ug/l
95-50-1 1,2-Dichlorobenzene ND 13 3.1 ug/l
541-73-1 1,3-Dichlorobenzene ND 13 3.1 ug/l
106-46-7 1,4-Dichlorobenzene ND 13 3.1 ug/l
75-34-3 1,1-Dichloroethane ND 13 3.1 ug/l
107-06-2 1,2-Dichloroethane ND 13 3.1 ug/l
75-35-4 1,1-Dichloroethylene ND 13 3.1 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 13 3.1 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 13 3.1 ug/l
78-87-5 1,2-Dichloropropane ND 13 3.1 ug/l
142-28-9 1,3-Dichloropropane ND 13 3.1 ug/l
594-20-7 2,2-Dichloropropane ND 13 3.1 ug/l
563-58-6 1,1-Dichloropropene ND 13 3.1 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 13 3.1 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 13 3.1 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
6 of 20
FA9356433.1
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:TMW-2
Lab Sample ID:FA93564-1 Date Sampled:03/02/22
Matrix:AQ - Ground Water Date Received:03/03/22
Method:SM 6200B Percent Solids:n/a
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 11.1 13 3.1 ug/l J
100-41-4 Ethylbenzene 97.5 13 3.1 ug/l
87-68-3 Hexachlorobutadiene ND 13 3.1 ug/l
98-82-8 Isopropylbenzene 11.0 13 3.1 ug/l J
99-87-6 p-Isopropyltoluene 4.6 13 3.1 ug/l J
74-83-9 Methyl Bromide ND 13 5.0 ug/l
74-87-3 Methyl Chloride ND 13 5.0 ug/l
74-95-3 Methylene Bromide ND 13 3.1 ug/l
75-09-2 Methylene Chloride ND 50 25 ug/l
1634-04-4 Methyl Tert Butyl Ether 2650 a 50 13 ug/l
91-20-3 Naphthalene 19.0 13 3.1 ug/l
103-65-1 n-Propylbenzene 19.2 13 3.1 ug/l
100-42-5 Styrene ND 13 3.1 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 13 3.1 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 13 3.1 ug/l
127-18-4 Tetrachloroethylene ND 13 3.1 ug/l
108-88-3 Toluene ND 13 3.1 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 13 3.1 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 13 3.1 ug/l
71-55-6 1,1,1-Trichloroethane ND 13 3.1 ug/l
79-00-5 1,1,2-Trichloroethane ND 13 3.1 ug/l
79-01-6 Trichloroethylene ND 13 3.1 ug/l
75-69-4 Trichlorofluoromethane b ND 13 5.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 13 3.1 ug/l
95-63-6 1,2,4-Trimethylbenzene 220 13 3.1 ug/l
108-67-8 1,3,5-Trimethylbenzene 92.5 13 3.1 ug/l
75-01-4 Vinyl Chloride ND 13 3.1 ug/l
m,p-Xylene 404 25 3.1 ug/l
95-47-6 o-Xylene 88.8 13 3.1 ug/l
1330-20-7 Xylene (total)493 38 6.3 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%101%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%103%70-130%
2037-26-5 Toluene-D8 101%100%70-130%
460-00-4 4-Bromofluorobenzene 97%100%70-130%
(a) Result is from Run# 2
(b) Associated BS recovery outside control limits high, sample is ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
7 of 20
FA9356433.1
SGS North America Inc.
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Orlando, FL
Section 4
8 of 20
FA935644
FA93564: Chain of Custody
Page 1 of 2
9 of 20
FA9356444.1
Job Number:FA93564 Client:GEOLOGICAL RESOURCES, INC.
Date / Time Received:3/3/2022 9:45:00 AM Delivery Method:FEDEX
Project:H&S TRADING
Airbill #'s:1009 6379 5516
Cooler Information
1. Custody Seals Present
2. Custody Seals Intact
4. Cooler temp verification
3. Temp criteria achieved
5. Cooler media
IR Gun
Ice (Bag)
Trip Blank Information
1. Trip Blank present / cooler
2. Trip Blank listed on COC
2. Samples preserved properly
Sample Information
1. Sample labels present on bottles
5. Sample recvd within HT
4. Condition of sample
3. Sufficient volume/containers recvd for analysis:
Intact
Comments
SM001Rev. Date 05/24/17
SGS Sample Receipt Summary
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
Cooler 1: (2.8);
Cooler 1: (3.2);
3. Type Of TB Received
W or S N/A
6. Dates/Times/IDs on COC match Sample Label
7. VOCs have headspace
8. Bottles received for unspecified tests
9. Compositing instructions clear
10. Voa Soil Kits/Jars received past 48hrs?
11. % Solids Jar received?
Misc. Information
25-Gram 5-GramNumber of Encores:Number of 5035 Field Kits:Number of Lab Filtered Metals:
Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify)
Y or N N/A
Y or N
Therm ID:IR 1; Therm CF:0.4; # of Coolers:1
Y or N N/A
12. Residual Chlorine Present?
Residual Chlorine Test Strip Lot #:
Technician:Reviewer:SAMUELM Date:Date:3/3/2022 9:45:00 AM
FA93564: Chain of Custody
Page 2 of 2
10 of 20
FA9356444.1
SGS North America Inc.
MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 5
11 of 20
FA935645
Method Blank Summary Page 1 of 2
Job Number:FA93564
Account:GRINCC GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA3085-MB A0230902.D 1 03/10/22 JL n/a n/a VA3085
The QC reported here applies to the following samples:Method: SM 6200B
FA93564-1
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
12 of 20
FA9356455.1.1
Method Blank Summary Page 2 of 2
Job Number:FA93564
Account:GRINCC GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA3085-MB A0230902.D 1 03/10/22 JL n/a n/a VA3085
The QC reported here applies to the following samples:Method: SM 6200B
FA93564-1
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 101%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
13 of 20
FA9356455.1.1
Method Blank Summary Page 1 of 1
Job Number:FA93564
Account:GRINCC GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA3088-MB A0230996.D 1 03/15/22 JL n/a n/a VA3088
The QC reported here applies to the following samples:Method: SM 6200B
FA93564-1
CAS No.Compound Result RL MDL Units Q
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 97%70-130%
17060-07-0 1,2-Dichloroethane-D4 99%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
14 of 20
FA9356455.1.2
Blank Spike Summary Page 1 of 2
Job Number:FA93564
Account:GRINCC GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA3085-BS A0230900.D 1 03/10/22 JL n/a n/a VA3085
The QC reported here applies to the following samples:Method: SM 6200B
FA93564-1
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 10.4 104 70-130
108-86-1 Bromobenzene 10 10.1 101 70-130
74-97-5 Bromochloromethane 10 8.5 85 70-130
75-27-4 Bromodichloromethane 10 9.9 99 70-130
75-25-2 Bromoform 10 9.4 94 70-130
104-51-8 n-Butylbenzene 10 10.2 102 70-130
135-98-8 sec-Butylbenzene 10 11.9 119 70-130
98-06-6 tert-Butylbenzene 10 11.2 112 70-130
56-23-5 Carbon Tetrachloride 10 10.6 106 70-130
108-90-7 Chlorobenzene 10 9.9 99 70-130
75-00-3 Chloroethane 10 12.0 120 60-140
67-66-3 Chloroform 10 9.5 95 70-130
95-49-8 o-Chlorotoluene 10 10.5 105 70-130
106-43-4 p-Chlorotoluene 10 10.4 104 70-130
124-48-1 Dibromochloromethane 10 9.6 96 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 9.3 93 70-130
106-93-4 1,2-Dibromoethane 10 9.8 98 70-130
75-71-8 Dichlorodifluoromethane 10 11.8 118 60-140
95-50-1 1,2-Dichlorobenzene 10 10.3 103 70-130
541-73-1 1,3-Dichlorobenzene 10 10.4 104 70-130
106-46-7 1,4-Dichlorobenzene 10 9.9 99 70-130
75-34-3 1,1-Dichloroethane 10 10.1 101 70-130
107-06-2 1,2-Dichloroethane 10 9.6 96 70-130
75-35-4 1,1-Dichloroethylene 10 10.5 105 70-130
156-59-2 cis-1,2-Dichloroethylene 10 10.3 103 70-130
156-60-5 trans-1,2-Dichloroethylene 10 10.3 103 70-130
78-87-5 1,2-Dichloropropane 10 10.1 101 70-130
142-28-9 1,3-Dichloropropane 10 9.7 97 70-130
594-20-7 2,2-Dichloropropane 10 10.6 106 70-130
563-58-6 1,1-Dichloropropene 10 11.0 110 70-130
10061-01-5 cis-1,3-Dichloropropene 10 10.5 105 70-130
10061-02-6 trans-1,3-Dichloropropene 10 10.4 104 70-130
108-20-3 Di-Isopropyl Ether 10 9.4 94 70-130
100-41-4 Ethylbenzene 10 10.4 104 70-130
87-68-3 Hexachlorobutadiene 10 11.6 116 70-130
98-82-8 Isopropylbenzene 10 11.3 113 70-130
* = Outside of Control Limits.
15 of 20
FA9356455.2.1
Blank Spike Summary Page 2 of 2
Job Number:FA93564
Account:GRINCC GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA3085-BS A0230900.D 1 03/10/22 JL n/a n/a VA3085
The QC reported here applies to the following samples:Method: SM 6200B
FA93564-1
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 11.0 110 70-130
74-83-9 Methyl Bromide 10 12.0 120 60-140
74-87-3 Methyl Chloride 10 10.9 109 60-140
74-95-3 Methylene Bromide 10 9.1 91 70-130
75-09-2 Methylene Chloride 10 9.6 96 70-130
91-20-3 Naphthalene 10 10.2 102 70-130
103-65-1 n-Propylbenzene 10 10.8 108 70-130
100-42-5 Styrene 10 10 100 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 10.4 104 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 9.8 98 70-130
127-18-4 Tetrachloroethylene 10 10.4 104 70-130
108-88-3 Toluene 10 10.3 103 70-130
87-61-6 1,2,3-Trichlorobenzene 10 10.6 106 70-130
120-82-1 1,2,4-Trichlorobenzene 10 10.9 109 70-130
71-55-6 1,1,1-Trichloroethane 10 10.1 101 70-130
79-00-5 1,1,2-Trichloroethane 10 9.7 97 70-130
79-01-6 Trichloroethylene 10 10.3 103 70-130
75-69-4 Trichlorofluoromethane 10 14.4 144*60-140
96-18-4 1,2,3-Trichloropropane 10 9.5 95 70-130
95-63-6 1,2,4-Trimethylbenzene 10 10 100 70-130
108-67-8 1,3,5-Trimethylbenzene 10 11.1 111 70-130
75-01-4 Vinyl Chloride 10 11.8 118 60-140
m,p-Xylene 20 21.4 107 70-130
95-47-6 o-Xylene 10 10.7 107 70-130
1330-20-7 Xylene (total)30 32.1 107 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 97%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
* = Outside of Control Limits.
16 of 20
FA9356455.2.1
Blank Spike Summary Page 1 of 1
Job Number:FA93564
Account:GRINCC GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA3088-BS A0230994.D 1 03/15/22 JL n/a n/a VA3088
The QC reported here applies to the following samples:Method: SM 6200B
FA93564-1
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
1634-04-4 Methyl Tert Butyl Ether 10 9.5 95 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 96%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
* = Outside of Control Limits.
17 of 20
FA9356455.2.2
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA93564
Account:GRINCC GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA93564-1MS A0230925.D 25 03/11/22 JL n/a n/a VA3085
FA93564-1MSD A0230926.D 25 03/11/22 JL n/a n/a VA3085
FA93564-1 A0230924.D 25 03/11/22 JL n/a n/a VA3085
The QC reported here applies to the following samples:Method: SM 6200B
FA93564-1
FA93564-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 30.6 250 332 121 250 304 109 9 70-130/20
108-86-1 Bromobenzene ND 250 281 112 250 259 104 8 70-130/20
74-97-5 Bromochloromethane ND 250 243 97 250 223 89 9 70-130/20
75-27-4 Bromodichloromethane ND 250 283 113 250 257 103 10 70-130/20
75-25-2 Bromoform ND 250 253 101 250 229 92 10 70-130/20
104-51-8 n-Butylbenzene ND 250 281 112 250 260 104 8 70-130/20
135-98-8 sec-Butylbenzene 5.5 J 250 334 131*250 308 121 8 70-130/20
98-06-6 tert-Butylbenzene ND 250 317 127 250 290 116 9 70-130/20
56-23-5 Carbon Tetrachloride ND 250 302 121 250 279 112 8 70-130/20
108-90-7 Chlorobenzene ND 250 283 113 250 258 103 9 70-130/20
75-00-3 Chloroethane ND 250 305 122 250 303 121 1 60-140/20
67-66-3 Chloroform ND 250 278 111 250 254 102 9 70-130/20
95-49-8 o-Chlorotoluene ND 250 312 125 250 287 115 8 70-130/20
106-43-4 p-Chlorotoluene ND 250 286 114 250 267 107 7 70-130/20
124-48-1 Dibromochloromethane ND 250 267 107 250 241 96 10 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 250 275 110 250 252 101 9 70-130/20
106-93-4 1,2-Dibromoethane ND 250 273 109 250 253 101 8 70-130/20
75-71-8 Dichlorodifluoromethane ND 250 303 121 250 310 124 2 60-140/20
95-50-1 1,2-Dichlorobenzene ND 250 287 115 250 268 107 7 70-130/20
541-73-1 1,3-Dichlorobenzene ND 250 288 115 250 266 106 8 70-130/20
106-46-7 1,4-Dichlorobenzene ND 250 274 110 250 253 101 8 70-130/20
75-34-3 1,1-Dichloroethane ND 250 292 117 250 268 107 9 70-130/20
107-06-2 1,2-Dichloroethane ND 250 282 113 250 255 102 10 70-130/20
75-35-4 1,1-Dichloroethylene ND 250 311 124 250 283 113 9 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 250 293 117 250 265 106 10 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 250 296 118 250 271 108 9 70-130/20
78-87-5 1,2-Dichloropropane ND 250 288 115 250 261 104 10 70-130/20
142-28-9 1,3-Dichloropropane ND 250 270 108 250 251 100 7 70-130/20
594-20-7 2,2-Dichloropropane ND 250 266 106 250 242 97 9 70-130/20
563-58-6 1,1-Dichloropropene ND 250 314 126 250 284 114 10 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 250 282 113 250 259 104 9 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 250 282 113 250 259 104 9 70-130/20
108-20-3 Di-Isopropyl Ether 11.1 J 250 286 110 250 263 101 8 70-130/20
100-41-4 Ethylbenzene 97.5 250 399 121 250 373 110 7 70-130/20
87-68-3 Hexachlorobutadiene ND 250 308 123 250 282 113 9 70-130/20
98-82-8 Isopropylbenzene 11.0 J 250 330 128 250 306 118 8 70-130/20
* = Outside of Control Limits.
18 of 20
FA9356455.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA93564
Account:GRINCC GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA93564-1MS A0230925.D 25 03/11/22 JL n/a n/a VA3085
FA93564-1MSD A0230926.D 25 03/11/22 JL n/a n/a VA3085
FA93564-1 A0230924.D 25 03/11/22 JL n/a n/a VA3085
The QC reported here applies to the following samples:Method: SM 6200B
FA93564-1
FA93564-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene 4.6 J 250 305 120 250 283 111 7 70-130/20
74-83-9 Methyl Bromide ND 250 326 130 250 324 130 1 60-140/20
74-87-3 Methyl Chloride ND 250 294 118 250 298 119 1 60-140/20
74-95-3 Methylene Bromide ND 250 260 104 250 236 94 10 70-130/20
75-09-2 Methylene Chloride ND 250 282 113 250 263 105 7 70-130/20
91-20-3 Naphthalene 19.0 250 305 114 250 286 107 6 70-130/20
103-65-1 n-Propylbenzene 19.2 250 324 122 250 300 112 8 70-130/20
100-42-5 Styrene ND 250 280 112 250 256 102 9 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 250 292 117 250 266 106 9 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 250 288 115 250 266 106 8 70-130/20
127-18-4 Tetrachloroethylene ND 250 285 114 250 266 106 7 70-130/20
108-88-3 Toluene ND 250 298 119 250 274 110 8 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 250 292 117 250 268 107 9 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 250 299 120 250 274 110 9 70-130/20
71-55-6 1,1,1-Trichloroethane ND 250 293 117 250 267 107 9 70-130/20
79-00-5 1,1,2-Trichloroethane ND 250 280 112 250 257 103 9 70-130/20
79-01-6 Trichloroethylene ND 250 285 114 250 262 105 8 70-130/20
75-69-4 Trichlorofluoromethane ND 250 391 156*250 388 155*1 60-140/20
96-18-4 1,2,3-Trichloropropane ND 250 270 108 250 254 102 6 70-130/20
95-63-6 1,2,4-Trimethylbenzene 220 250 526 122 250 497 111 6 70-130/20
108-67-8 1,3,5-Trimethylbenzene 92.5 250 410 127 250 386 117 6 70-130/20
75-01-4 Vinyl Chloride ND 250 313 125 250 317 127 1 60-140/20
m,p-Xylene 404 500 1020 123 500 952 110 7 70-130/20
95-47-6 o-Xylene 88.8 250 402 125 250 375 114 7 70-130/20
1330-20-7 Xylene (total)493 750 1420 124 750 1330 112 7 70-130/20
CAS No.Surrogate Recoveries MS MSD FA93564-1 Limits
1868-53-7 Dibromofluoromethane 101%101%101%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%100%104%70-130%
2037-26-5 Toluene-D8 99%100%101%70-130%
460-00-4 4-Bromofluorobenzene 100%101%97%70-130%
* = Outside of Control Limits.
19 of 20
FA9356455.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1
Job Number:FA93564
Account:GRINCC GRI (Geological Resources Inc.)
Project:H&S Trading; 211 Tunis Rd, Tunis, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA93564-1MS A0231015.D 100 03/15/22 JL n/a n/a VA3088
FA93564-1MSD A0231016.D 100 03/15/22 JL n/a n/a VA3088
FA93564-1 A0231014.D 100 03/15/22 JL n/a n/a VA3088
The QC reported here applies to the following samples:Method: SM 6200B
FA93564-1
FA93564-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
1634-04-4 Methyl Tert Butyl Ether 2650 1000 3770 112 1000 3780 113 0 70-130/20
CAS No.Surrogate Recoveries MS MSD FA93564-1 Limits
1868-53-7 Dibromofluoromethane 100%100%101%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%100%103%70-130%
2037-26-5 Toluene-D8 99%99%100%70-130%
460-00-4 4-Bromofluorobenzene 100%101%100%70-130%
* = Outside of Control Limits.
20 of 20
FA9356455.3.2

APPENDIX E
Contaminant Mass Calculations
Area ID Well ID Area
(ft²)
Average Well
Depth
(ft.)
Average
Depth to
Water
(ft.)
Water Column
Height
(ft)
Volume
(ft³)
Volume
(L)
Effective
Porosity
Effective
Volume
(L)
MW-1
MW-2
MW-19
MW-5
MW-6
Area Date Well Benzene
(μ/L)
Toluene
(μ/L)
Ethylbenzene
(μ/L)
Xylenes
(μ/L)
MTBE
(μ/L)
Naphthalene
(μ/L)
Total
(μ/L)
DTW
(ft.)
Average Water
Column Height
(ft.)
Total Average
Mass
(g)
Percent Red.To Date Red.
MW-1 29 0.00 1,230 1,710 63.8 2,270 5302.80 23.00
MW-2 7.7 0.00 3.2 0.45 42.4 5.4 59.15 22.09
MW-19 48.4 0.00 47.9 87.9 1,490 41.2 1715.40 21.36
Avg.28 0.00 427 599 532 772 2359.12 22.15
MW-1 0.00 0.00 1,840 917 51.80 4,880 7688.80 21.28
MW-2 5.0 0.00 3.2 1.9 31.6 24.2 65.90 20.42
MW-19 7.7 0.23 134 262 102 42.1 548.03 20.72
Avg.4.23 0.08 659 394 62 1,649 2767.58 20.81
MW-1 26.1 0.00 788 0.00 14.20 1,650 2478.30 23.22
MW-2 2.00 0.00 0.00 0.34 4.50 4.2 11.04 22.33
MW-19 4.20 0.00 14.7 20 140 194 373.20 21.13
Avg.11 0.00 268 7 53 616 954.18 22.23
MW-1 4.9 0.00 524 0.00 5.20 1,610 2144.10 23.25
MW-2 0.00 0.00 0.00 0.00 5.4 0 5.40 24.46
MW-19 5.70 0.00 7.3 2.1 330 64.1 409.20 21.66
Avg.3.5 0.00 177.1 0.7 114 558 852.90 23.12
02/23/16
204,649 5,795,015 579,501
APPENDIX E
PERCENTAGE REDUCTIONS
H&S TRADING (INCIDENT NO. 10151)
Baseline Event
0.10
4 19,144 30 19.31 10.69
7.85 30,874
65.32 20.9%68.3%
08/12/15
1 303,933.02 22.15
7.77
6.88
874,259 87,426
206.25 ------
Area 1
283.36 -37.4%-37.4%
82.61 70.8%59.9%08/06/19
02/28/22
7.85
9.19
Area ID Well ID Area
(ft²)
Average Well
Depth
(ft.)
Average
Depth to
Water
(ft.)
Water Column
Height
(ft)
Volume
(ft³)
Volume
(L)
Effective
Porosity
Effective
Volume
(L)
MW-1
MW-2
MW-19
MW-5
MW-6
Area Date Well Benzene
(μ/L)
Toluene
(μ/L)
Ethylbenzene
(μ/L)
Xylenes
(μ/L)
MTBE
(μ/L)
Naphthalene
(μ/L)
Total
(μ/L)
DTW
(ft.)
Average Water
Column Height
(ft.)
Total Average
Mass
(g)
Percent Red.To Date Red.
204,649 5,795,015 579,501
APPENDIX E
PERCENTAGE REDUCTIONS
H&S TRADING (INCIDENT NO. 10151)
Baseline Event
0.10
4 19,144 30 19.31 10.69
7.85 30,8741303,933.02 22.15 874,259 87,426
MW-5 3.10 0.28 4.10 16.60 65.70 16.50 106.28 18.03
MW-6 3.30 0.00 0.58 0.00 25.80 0.00 29.68 20.58
Avg.3.20 0.14 2.34 8.30 45.75 8.25 67.98 19.31
MW-5 6.00 0.17 28.60 54.30 61.00 42.60 192.67 16.45
MW-6 2.70 0.00 0.24 0.00 17.30 0.86 21.10 19.79
Avg.4.35 0.09 14.42 27.15 39.15 21.73 106.89 18.12
MW-5 0.13 0.13 0.21 1.00 42.10 4.60 48.17 18.32
MW-6 0.21 0.00 0.00 0.00 29.10 0.00 29.31 20.74
Avg.0.17 0.07 0.11 0.50 35.60 2.30 38.74 19.53
MW-5 1.10 0.00 1.60 3.20 20.60 1.80 28.30 18.11
MW-6 0.00 0.00 0.00 0.00 17.20 0.22 17.42 20.60
Avg.0.55 0.00 0.80 1.60 18.90 1.01 22.86 19.36
Date
Average Water
Column Height
(ft.)
08/12/15 9.27
02/23/16 10.54
08/06/19 9.12
02/28/22 8.76
Notes:
• FP: Free Product
• Area of the contaminant plume is calculated from Figure 7
• Height of the water column is calculated by subtracting the average depth to water from the average well depth of the referenced monitoring wells
• Volume of the contaminant plume is calculated by multiplying the area of the plume by the average height of the water column during each sampling event
• Effective porosity is assumed based on the sub-surface soil profile obtained from well construction records and soil boring logs
• Total mass was calculated by multiplying the total contaminant concentrations for the sampling event with effective volume
• Contaminant mass cannot be calculated in wells containing FP; therefore, the total contaminant mass is based on the known concentrations in the area for each sampling event.
• When areas couldn’t be sampled, the last known concentrations were used in the calculations.
02/23/16 11.88 68.84
10.47 21.99 68.1%44.2%
08/12/15 10.70 39.41 ------
Percent Reduction Compared
to Previous Event Percent Reduction To Date
246 ------
Total Contaminant Mass
(g)
79 68.0%68%
352 -43.4%-43%
105 70.3%57%
Area 2
02/28/22 10.65 13.19 40.0%66.5%
-74.7%-74.7%
08/06/19