WA-706_10000_CA_RPTS_20160127_MRP

EXECUTIVE SUMMARY

The former Peele’s Service Station site is located at 2675 Old US Highway 64, Jamesville, Martin
County, North Carolina. According to available information, a petroleum release at the site was
confirmed subsequent to the removal of one 1,000-gallon and one 550-gallon gasoline USTs in
September 1992. The site risk classification is currently ranked as high risk due to forty-seven potable
water supply wells being located within a 1,000-foot radius of the site.

On January 11, 2016, seven Type II monitoring wells were gauged, purged and sampled. Free product
was not observed in any of these wells during the January 2016 sampling event. Concentrations of
requested method constituents that exceeded the Maximum Allowable Concentrations (MACs) were
reported in the ground water samples collected from MW-2, MW-2R, MW-11 and MW-14. None of the
reported contaminant concentrations exceeded the Gross Contamination Levels.

Based on this information, a fate and transport model should be developed to determine if the
contaminant plume poses a significant risk the nearest down-gradient receptor. An updated receptor
survey should be completed during the next sampling event which is tentatively scheduled for July 2016.

TABLE OF CONTENTS

1.0 SITE HISTORY AND CHARACTERIZATION ...................................................................... 1
2.0 CURRENT SITE ACTIVITIES ................................................................................................. 1
3.0 GROUND WATER QUALITY ................................................................................................. 1
4.0 CONCLUSIONS AND RECOMMENDATIONS ..................................................................... 2
5.0 LIMITATIONS .......................................................................................................................... 2

FIGURES
Figure 1: Site Location Map
Figure 2: Site Map
Figure 3: Water Table Surface Map
Figure 4: Ground Water Quality Map

TABLES
Table 1: Well Construction and Gauging Information
Table 2: Summary of Ground Water Sample Analytical Results

APPENDIX
Appendix A: Laboratory Report – Ground Water Samples
1

1.0 SITE HISTORY AND CHARACTERIZATION
The former Peele’s Service Station site is located at 2675 Old US Highway 64, Jamesville, Martin
County, North Carolina (Figure 1). According to available information, one 1,000-gallon and one 550-
gallon gasoline underground storage tanks (USTs) were removed from the site on September 23, 1992.
Eighteen Type II monitoring wells (MW-1, MW-2, MW-2R, MW-3 through MW-4 and MW-6 through
MW-18) and one Type III monitoring well (MW-5) were installed at the site during previous ground
water assessment and corrective action activities. Previous activities were conducted by past consultants.
Although Geological Resources, Inc. (GRI) cannot verify the accuracy of information obtained from
previous reports, for the purposes of this report, it is assumed to be correct. Please refer to previous
submittals for further historical information regarding the site.

2.0 CURRENT SITE ACTIVITIES
The purpose of this report is to present the results of ground water monitoring activities conducted on
January 11, 2016 at the Peele’s Service Station site. The activities were conducted in accordance with
GRI proposal number 15-412, which was submitted to NCDEQ on July 6, 2015 and approved as Task
Authorization No. 10000-55 on July 7, 2015. The purpose of the activities was to obtain current ground
water quality data for the site.

3.0 GROUND WATER QUALITY
Seven Type II monitoring wells (MW-1, MW-2, MW-2R, MW-3, MW-11, MW-14 and MW-15) were
gauged, purged and sampled on January 11, 2016. No free product was observed in any of the monitoring
wells. Depths to ground water in the Type II monitoring wells measured on January 11, 2016 ranged
from 1.87 to 5.67 feet below the tops of well casings. Ground water elevations in the Type II monitoring
wells relative to a temporary benchmark assumed by the previous consultant ranged from 95.69 to 98.75
feet. Based on the January 2016 gauging data, the ground water flow across the site was generally toward
the northeast. The average horizontal hydraulic gradient in the vicinity of the source area was
approximately 0.02 feet per foot. A Site Map showing the locations of the monitoring and water supply
wells has been included as Figure 2. A Water Table Surface Map based on the January 2016 gauging
data is included as Figure 3. Well construction and gauging information is presented in Table 1.

Laboratory analyses were performed on the ground water samples collected from the above referenced
monitoring wells for volatile organic compounds using EPA Method 6200B. Concentrations of benzene,
xylenes, naphthalene, n-propylbenzene and/or 1,2,4-trimethylbenzene that exceeded the Maximum
2

Allowable Concentrations (MACs) specified in T15A NCAC 2L.0202 were reported in the ground water
samples collected from MW-2, MW-2R, MW-11 and MW-14. None of the reported contaminant
concentrations exceeded the Gross Contamination Levels (GCLs).

A Ground Water Quality Map based on data collected during the January 2016 sampling event is included
as Figure 4. A summary of ground water sample analytical results is presented in Table 2. A complete
laboratory report has been included as Appendix A.

4.0 CONCLUSIONS AND RECOMMENDATIONS
 The average depth to ground water in the Type II monitoring wells during the January 2016 sampling
event was 3.49 feet. Ground water flow across the site during the January 2016 sampling event was
generally toward the northeast with a horizontal hydraulic gradient in the vicinity of the source area
of approximately 0.02 feet per foot.
 Free product was not observed in any of the wells during the January 2016 sampling event.
 Concentrations of benzene, xylenes, naphthalene, n-propylbenzene and/or 1,2,4-trimethylbenzene that
exceeded the MACs were reported in the ground water samples collected from MW-2, MW-2R, MW-
11 and MW-14. None of the reported contaminant concentrations exceeded the GCLs.
 Based on this information, a fate and transport model should be developed to determine if the
contaminant plume poses a significant risk the nearest down-gradient receptor. An updated receptor
survey should be completed during the next sampling event which is tentatively scheduled for July
2016.

5.0 LIMITATIONS
This report has been prepared for the exclusive use of North East Oil Company, Inc. for specific
application to the referenced site in Martin County, North Carolina. The assessment was conducted based
on the scope of work and level of effort desired by NCDEQ and with resources adequate only for that
scope of work. Our findings have been developed in accordance with generally accepted standards of
environmental practices in the State of North Carolina, available information, and our professional
judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would be
interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data. Please note that field data collected prior
3

to the March 2007 updated receptor survey and ground water monitoring event were not obtained under
the supervision of GRI. Although the accuracy of this information cannot be verified, for the purpose of
this report GRI assumes that it is correct.

FIGURES

TABLES

03/01/07 3.32 0.00 97.04
08/13/07 DRY 0.00 NM
03/12/09 NM 0.00 NM
08/25/09 DRY 0.00 NM
12/08/11 10.17 0.00 90.19
06/13/12 6.98 0.00 93.38
03/07/13 4.33 0.00 96.03
10/02/13 9.19 0.00 91.17
04/02/14 3.41 0.00 96.95
09/30/14 5.98 0.00 94.38
04/01/15 1.87 0.00 98.49
01/11/16 2.60 0.00 97.76
03/01/07 2.63 0.00 97.91
08/13/07 DRY 0.00 NM
03/12/09 DRY 0.00 NM
08/25/09 DRY 0.00 NM
12/08/11 DRY 0.00 NM
06/13/12 7.07 0.00 93.47
03/07/13 2.60 0.00 97.94
10/02/13 DRY 0.00 NM
01/11/16 1.98 0.00 98.56
12/08/11 10.96 0.00 89.90
06/13/12 8.00 0.17 93.01
01/23/13 7.81 0.10 93.13 Before AFVR
01/23/13 10.05 0.00 90.81 After AFVR
03/07/13 5.66 0.44 95.58
08/27/13 5.73 0.25 95.34 Before AFVR
08/27/13 10.17 0.00 90.69 After AFVR
10/02/13 9.88 0.00 90.98
04/02/14 3.39 0.04 97.50
09/30/14 7.07 0.03 93.82
04/01/15 2.16 0.00 98.70
01/11/16 2.97 0.00 97.89
03/01/07 2.85 0.00 97.77
08/13/07 DRY 0.00 NM
03/12/09 DRY 0.00 NM
08/25/09 DRY 0.00 NM
12/08/11 DRY 0.00 NM
06/13/12 7.38 0.00 93.24
03/07/13 3.22 0.00 97.40
10/02/13 DRY 0.00 NM
01/11/16 1.87 0.00 98.75
03/01/07 3.70 0.00 97.01
08/13/07 DRY 0.00 NM
03/12/09 DRY 0.00 NM
08/25/09 DRY 0.00 NM
12/08/11 10.02 0.00 90.69
06/13/12 6.86 0.00 93.85
03/07/13 1.90 0.00 98.81
10/02/13 9.44 0.00 91.27
04/02/14 1.60 0.00 99.11
09/30/14 6.57 0.00 94.14
04/01/15 0.93 0.00 99.78
03/01/07 16.71 0.00 83.69
08/13/07 19.68 0.00 80.72
03/12/09 21.73 0.00 78.67
08/25/09 21.07 0.00 79.33
12/08/11 19.30 0.00 81.10
06/13/12 18.50 0.00 81.90
03/07/13 17.39 0.00 83.01
10/02/13 18.25 0.00 82.15
04/02/14 15.71 0.00 84.69
09/30/14 17.85 0.00 82.55
04/01/15 15.22 0.00 85.18
03/01/07 4.52 0.00 95.58
08/13/07 11.32 0.00 88.78
03/12/09 DRY 0.00 DRY
08/25/09 12.37 0.00 87.73
12/08/11 10.70 0.00 89.40
06/13/12 7.74 0.00 92.36
03/07/13 5.68 0.00 94.42
10/02/13 NM 0.00 NM
5 5 - 15 15 100.10
100.40
Well Casing
Depth
(ft. BGS)
Comments
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of Casing
Elevation*
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
Groundwater
Elevation*
(ft.)
100.71
100.86
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
PEELE'S SERVICE STATION (INCIDENT NO. 10000)
Facility ID#: 0-0013895Date: 01/12/16
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
5 - 15
MW-5 05/18/93 30 30 - 35
15
35
05/14/93 5
5
MW-6 05/17/93
01/26/93
MW-4
MW-1
100.54122 - 12201/27/93MW-2
100.36155 - 15
177 - 1712/08/11MW-2R 7
100.62122 - 12201/27/93MW-3
Page 1 of 3
Well Casing
Depth
(ft. BGS)
Comments
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of Casing
Elevation*
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
Groundwater
Elevation*
(ft.)
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
PEELE'S SERVICE STATION (INCIDENT NO. 10000)
Facility ID#: 0-0013895Date: 01/12/16
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
08/25/09 12.05 0.00 88.27
12/08/11 11.03 0.00 89.29
06/13/12 8.38 0.00 91.94
03/07/13 5.52 0.00 94.80
10/02/13 9.89 0.00 90.43
03/01/07 2.76 0.00 97.47
08/13/07 10.70 0.00 89.53
03/12/09 NM 0.00 NM
08/25/09 10.55 0.00 89.68
12/08/11 9.60 0.00 90.63
06/13/12 5.97 0.00 94.26
03/07/13 2.60 0.00 97.63
10/02/13 8.73 0.00 91.50
04/02/14 3.12 0.00 97.11
09/30/14 5.37 0.00 94.86
04/01/15 2.19 0.00 98.04
03/01/07 3.16 0.00 97.13
08/13/07 10.74 0.00 89.55
03/12/09 DRY 0.00 DRY
08/25/09 10.60 0.00 89.69
12/08/11 9.52 0.00 90.77
06/13/12 6.58 0.00 93.71
03/07/13 4.16 0.00 96.13
10/02/13 NM 0.00 NM
08/25/09 13.00 0.00 87.25
12/08/11 10.86 0.00 89.39
06/13/12 8.28 0.00 91.97
03/07/13 6.84 0.00 93.41
10/02/13 9.58 0.00 90.67
04/02/14 3.09 0.00 97.16
09/30/14 7.67 0.00 92.58
04/01/15 2.29 0.00 97.96
03/01/07 5.93 0.00 94.33
08/13/07 11.97 0.00 88.29
03/12/09 15.51 0.00 84.75
08/25/09 14.19 0.00 86.07
12/08/11 11.88 0.00 88.38
06/13/12 9.51 0.00 90.75
03/07/13 7.53 0.00 92.73
10/02/13 10.40 0.00 89.86
04/02/14 4.64 0.00 95.62
09/30/14 8.86 0.00 91.40
04/01/15 3.70 0.00 96.56
01/11/16 4.40 0.00 95.86
03/01/07 3.61 0.00 96.89
08/13/07 11.10 0.00 89.40
03/12/09 13.44 0.00 87.06
08/25/09 NM 0.00 NM
12/08/11 10.17 0.00 90.33
06/13/12 7.30 0.00 93.20
03/07/13 4.98 0.00 95.52
10/02/13 NM 0.00 NM
03/01/07 4.50 0.00 95.79
08/13/07 11.04 0.00 89.25
03/12/09 13.80 0.00 86.49
08/25/09 NM 0.00 NM
12/08/11 10.72 0.00 89.57
06/13/12 7.57 0.00 92.72
03/07/13 5.67 0.00 94.62
10/02/13 NM 0.00 NM
08/25/09 NM NM Not Located
12/08/11 NM NM Not Located
06/13/12 NM NM Not Located
03/07/13 NM NM Not Located
10/02/13 NM NM Not Located
04/02/14 5.78 0.00 95.63
09/30/14 10.23 0.00 91.18
04/01/15 4.89 0.00 96.52
01/11/16 5.67 0.00 95.74
15 100.23
100.29
15 100.29
100.25
MW-12 02/16/94 4 4 - 14 14 100.50
101.4118
5 - 15
18
100.322.5
5 5 - 15
MW-13 04/27/95 8 8 - 18
12
05/19/93
2.5 - 12
MW-9 05/19/93
MW-7 05/17/93
5
MW-8
MW-10 02/16/94
100.26144 - 14402/16/94MW-11
4 4 - 14 14
8 - 18804/27/95MW-14
Page 2 of 3
Well Casing
Depth
(ft. BGS)
Comments
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of Casing
Elevation*
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
Groundwater
Elevation*
(ft.)
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
PEELE'S SERVICE STATION (INCIDENT NO. 10000)
Facility ID#: 0-0013895Date: 01/12/16
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
08/25/09 NM NM Not Located
12/08/11 NM NM Not Located
06/13/12 NM NM Not Located
03/07/13 NM NM Not Located
10/02/13 NM NM Not Located
04/02/14 5.13 0.00 95.47
09/30/14 NM NM Not Located
04/01/15 4.48 0.00 96.12
01/11/16 4.91 0.00 95.69
08/25/09 NM NM Not Located
12/08/11 NM NM Not Located
06/13/12 NM NM Not Located
03/07/13 NM NM Not Located
10/02/13 NM NM Not Located
03/01/07 2.09 0.00 98.57
08/13/07 12.71 0.00 87.95
03/12/09 14.78 0.00 85.88
08/25/09 NM 0.00 NM
12/08/11 13.29 0.00 87.37
06/13/12 3.12 0.00 97.54
03/07/13 1.04 0.00 99.62
10/02/13 11.08 0.00 89.58
04/02/14 1.04 0.00 99.62
09/30/14 1.78 0.00 98.88
04/01/15 NM NM NM Under Puddle
03/01/07 8.37 0.00 92.51
08/13/07 12.93 0.00 87.95
03/12/09 17.02 0.00 83.86
08/25/09 NM 0.00 NM
12/08/11 14.45 0.00 86.43
06/13/12 11.92 0.00 88.96
03/07/13 10.25 0.00 90.63
10/02/13 11.41 0.00 89.47
04/02/14 6.63 0.00 94.25
09/30/14 10.88 0.00 90.00
04/01/15 5.54 0.00 95.34
Notes:
• * Top-of-casing elevation and well construction data is reproduced from the July 2005 monitoring report prepared by CES Engineering, PC; elevations
relative to a temporary benchmark with an assumed datum of 100.00 feet; data reported in feet.
• ** : If free product is present in a well, ground water elevation calculated by: [Top of Casing Elevation - Depth to Water] - [free product thickness x 0.8581]
• ft BGS : feet below ground surface
• NA: Not available.
• NM: Not measured; well not located.
15 100.88
18 100.87
15 100.66
MW-18 08/16/95 5 5 - 15
MW-16 04/27/95 8 8 - 18
5 5 - 15MW-17 08/16/95
100.6018804/27/95MW-15 8 - 18
Page 3 of 3
EPA
Method
6010B
Well
ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 70 400 400 15 400 700 10,000 200
5,000 260,000 84,500 85,500 20,000 6,000 70,000 28,500 25,000 15,000 NE NE NE NE
03/01/07 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 <1.00 NR NR NR NR NR NR NR
08/13/07 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/12/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
08/25/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
12/08/11 29.9 0.91 21.2 4.0 0.18 J 48.6 0.32 J 18.5 0.16 J NR NR NR NR NR
06/13/12 10.3 2.2 6.3 113 <0.13 54.7 <0.11 130 17.6 NR NR NR NR NR
03/07/13 4.6 2.7 4.3 215 <0.10 49.4 <0.10 162 30.7 NR NR NR NR NR
10/02/13 36.2 13.1 26.6 1,020 0.35 J 228 <0.10 973 214 NR NR NR NR NR
04/02/14 0.77 1.0 2.1 86.1 <0.10 33.4 <0.10 71.7 11.9 NR NR NR NR NR
09/30/14 1.9 J 3.4 J 5.7 326 <1.0 88.7 <1.0 331 56.6 NR NR NR NR NR
04/01/15 <0.17 <0.17 0.29 J 7.1 <0.16 3.3 <0.16 6.6 0.70 NR NR NR NR NR
01/11/16 <0.13 <0.13 <0.13 0.71 J <0.13 0.41 J <0.13 0.95 0.24 J NR NR NR NR NR
03/01/07 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 <1.00 NR NR NR NR NR NR NR
08/13/07 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/12/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
08/25/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/13/12 27.1 22.4 29.7 652 <1.3 60.7 <1.1 278 57.3 NR NR NR NR NR
03/07/13 1.7 3.1 1.1 21.7 <0.10 0.49 J <0.10 4.3 1.3 NR NR NR NR NR
10/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/11/16 2.8 0.23 J 1.0 3.6 <0.13 0.43 J <0.13 1.5 <0.13 NR NR NR NR NR
12/08/11 147 2,300 1,310 12,250 <6.5 670 <5.4 2,770 756 NR NR NR NR NR
06/13/12 FP FP FP FP FP FP FP FP FP FP FP FP FP FP
10/02/13 729 4,320 1,010 19,210 <25 814 <25 3,640 900 NR NR NR NR NR
04/02/14 FP FP FP FP FP FP FP FP FP FP FP FP FP FP
09/30/14 FP FP FP FP FP FP FP FP FP FP FP FP FP FP
04/01/15 26.2 399 88.6 1,720 <4.1 109 <4.0 641 201 NR NR NR NR NR
01/11/16 8.9 55.6 22.7 180 <0.13 23.0 <0.13 70.3 23.5 NR NR NR NR NR
03/01/07 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 <1.00 NR NR NR NR NR NR NR
08/13/07 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/12/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
08/25/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
12/08/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/13/12 1.4 2.8 8.3 117 <0.33 10.1 <0.27 63.2 23.7 NR NR NR NR NR
03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
10/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/11/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 0.14 J <0.13 NR NR NR NR NR
03/01/07 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 <1.00 NR NR NR NR NR NR NR
08/13/07 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/12/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
08/25/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
12/08/11 <0.13 0.80 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
06/13/12 <0.13 <0.13 <0.15 <0.30 <0.13 0.10 J <0.11 <0.10 <0.10 NR NR NR NR NR
03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
10/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
04/02/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR
09/30/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR
04/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR NR
03/01/07 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 <1.00 NR NR NR NR NR NR NR
08/13/07 1.72 <1.0 <1.0 <3.0 3.47 <1.0 0.16 I NR NR NR NR NR NR NR
03/12/09 2.0 J <0.70 1.2 J 2.7 J 3.6 J 4.0 JB <1.0 2.2 J 0.54 J 77.9 <100 <200 <100 <200
08/25/09 3.53 <0.330 <0.670 <1.33 4.68 <1.00 <1.67 <0.330 <0.330 103 <100 <195.2 <95.2 <195.2
12/08/11 <0.13 <0.13 <0.15 <0.30 0.26 J <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
06/13/12 0.31 J <0.13 <0.15 <0.30 <0.13 0.28 J <0.11 <0.10 <0.10 NR NR NR NR NR
03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
10/02/13 <0.10 <0.10 <0.10 <0.22 0.68 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
04/02/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR
09/30/14 <0.10 <0.10 <0.10 <0.20 0.61 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR
04/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR NR
03/01/07 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 <1.00 NR NR NR NR NR NR NR
08/13/07 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 <5 NR NR NR NR NR NR NR
03/12/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
08/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.67 <0.330 <0.330 2.85 <100 <100 NR <100
12/08/11 <0.13 3.8 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
06/13/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
10/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
Facility ID# 0-013895Date: 01/22/16
Analytical Method
→
GCL (µg/l)
MADEP Methods EPH & VPH
C19-C36 Aliphatics2L Standard (µg/l)EthylbenzeneTolueneLeadMW-3
MW-1
MW-2
MW-2R 1,2,4 -TrimethylbenzeneC9-C22 AromaticsBenzeneContaminant of Concern
→XylenesC9-C18 AliphaticsTABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
PEELE'S SERVICE STATION (INCIDENT NO. 10000)NaphthaleneC5-C8 AliphaticsMW-6
MW-5
MW-4
EPA Method 6200B
1,3,5 -TrimethylbenzeneIPEMTBEPage 1 of 4
EPA
Method
6010B
Well
ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 70 400 400 15 400 700 10,000 200
5,000 260,000 84,500 85,500 20,000 6,000 70,000 28,500 25,000 15,000 NE NE NE NE
Facility ID# 0-013895Date: 01/22/16
Analytical Method
→
GCL (µg/l)
MADEP Methods EPH & VPH
C19-C36 Aliphatics2L Standard (µg/l)EthylbenzeneTolueneLead1,2,4 -TrimethylbenzeneC9-C22 AromaticsBenzeneContaminant of Concern
→XylenesC9-C18 AliphaticsTABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
PEELE'S SERVICE STATION (INCIDENT NO. 10000)NaphthaleneC5-C8 AliphaticsEPA Method 6200B
1,3,5 -TrimethylbenzeneIPEMTBE08/25/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
12/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
06/13/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
10/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
03/01/07 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 <1.00 NR NR NR NR NR NR NR
08/13/07 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 <5.0 NR NR NR NR NR NR NR
03/12/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
08/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.67 <0.330 <0.330 3.02 <100 <100 NR <100
12/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
06/13/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
10/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
04/02/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR
09/30/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR
04/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR NR
03/01/07 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 <1.00 NR NR NR NR NR NR NR
09/07/07 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 <5.0 NR NR NR NR NR NR NR
03/12/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
08/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.67 <0.330 <0.330 3.12 <100 <100 NR <100
12/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
06/13/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
10/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
08/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.67 <0.330 <0.330 5.60 <100 <100 NR <100
12/08/11 <0.13 5.9 0.33 J 0.73 J <0.13 <0.10 <0.11 0.21 J <0.10 NR NR NR NR NR
06/13/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
10/02/13 <0.10 <0.10 <0.10 0.16 J <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
04/02/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR
09/30/14 <0.10 <0.10 <0.10 <0.20 <0.10 0.27 J <0.10 0.21 J <0.10 NR NR NR NR NR
04/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR NR
03/01/07 3.58 108 136 1,629 10.6 61.4 15.3 NR NR NR NR NR NR NR
08/13/07 14.2 187 736 9,010 31.3 428 11.2 NR NR NR NR NR NR NR
03/12/09 7.3 <0.70 <0.50 1.9 J 3.2 J 1.7 JB <1.0 0.72 J 1.2 J 2.8 J 176 133 <100 166
08/25/09 7.44 <0.330 1.62 J 7.99 <0.330 2.51 <1.67 1.90 0.332 J 11.6 111 296 <97.1 220
12/08/11 35.8 1.4 218 1,710 1.4 348 1.4 987 354 NR NR NR NR NR
06/13/12 10.6 2.3 J 64.0 429 <0.65 133 <0.54 443 104 NR NR NR NR NR
03/07/13 14.8 2.4 99.9 618 0.32 J 262 <0.10 796 130 NR NR NR NR NR
10/02/13 16.4 4.2 J 147 800 <2.5 248 <2.5 1,020 80.5 NR NR NR NR NR
04/02/14 13.1 3.2 125 916 0.31 J 242 <0.10 911 177 NR NR NR NR NR
09/30/14 6.7 0.61 J 27.9 172 <0.50 135 <0.50 194 20.9 NR NR NR NR NR
04/01/15 1.9 J 1.1 J 28.2 210 <0.82 87.0 <0.80 191 29.2 NR NR NR NR NR
01/11/16 3.4 J 4.0 J 150 1,080 <2.5 476 <2.5 1,420 318 NR NR NR NR NR
03/01/07 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 <1.00 NR NR NR NR NR NR NR
08/13/07 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 <5 NR NR NR NR NR NR NR
03/12/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <1.0 <0.70 <0.50 8.8 <100 <100 NR <100
08/25/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
12/08/11 <0.13 139 <0.15 <0.30 <0.13 0.17 J <0.11 <0.10 <0.10 NR NR NR NR NR
06/13/12 <0.65 <0.64 <0.73 <1.5 <0.65 <0.50 <0.54 <0.50 <0.50 NR NR NR NR NR
03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 0.16 J <0.10 <0.10 <0.10 NR NR NR NR NR
10/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/01/07 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 <1.00 NR NR NR NR NR NR NR
08/13/07 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 <5.0 NR NR NR NR NR NR NR
03/12/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
08/25/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
12/08/11 <0.13 11.0 0.27 J <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
06/13/12 <0.13 1.0 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
10/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
12/08/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/13/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
10/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
04/02/14 0.76 <0.10 <0.10 <0.20 2.2 1.8 2.1 <0.10 <0.10 NR NR NR NR NR
09/30/14 2.5 0.15 J <0.10 1.3 J 2.0 4.2 1.7 <0.10 0.10 J NR NR NR NR NR
04/01/15 <0.17 <0.17 <0.15 <0.43 0.72 <0.12 0.64 <0.14 <0.14 NR NR NR NR NR
01/11/16 2.2 <0.13 0.18 J 1.1 J 0.45 J 8.0 0.64 <0.13 <0.13 NR NR NR NR NR
MW-7
MW-11
MW-14
MW-12
MW-9
MW-8
MW-10
MW-13
Page 2 of 4
EPA
Method
6010B
Well
ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 70 400 400 15 400 700 10,000 200
5,000 260,000 84,500 85,500 20,000 6,000 70,000 28,500 25,000 15,000 NE NE NE NE
Facility ID# 0-013895Date: 01/22/16
Analytical Method
→
GCL (µg/l)
MADEP Methods EPH & VPH
C19-C36 Aliphatics2L Standard (µg/l)EthylbenzeneTolueneLead1,2,4 -TrimethylbenzeneC9-C22 AromaticsBenzeneContaminant of Concern
→XylenesC9-C18 AliphaticsTABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
PEELE'S SERVICE STATION (INCIDENT NO. 10000)NaphthaleneC5-C8 AliphaticsEPA Method 6200B
1,3,5 -TrimethylbenzeneIPEMTBE12/08/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/13/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
10/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
04/02/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR
09/30/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
04/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR NR
01/11/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR
12/08/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/13/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
10/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/01/07 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 <1.00 NR NR NR NR NR NR NR
08/13/07 <1.0 <1.0 <1.0 <3.0 <1.0 1.45 <5 NR NR NR NR NR NR NR
03/12/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <1.0 <0.70 <0.50 NR NR NR NR NR
08/25/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
12/08/11 <0.13 <0.13 <0.15 0.36 J <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
06/13/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
10/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 0.16 J <0.10 <0.10 <0.10 NR NR NR NR NR
04/02/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR
09/30/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR
04/01/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/01/07 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 <1.00 NR NR NR NR NR NR NR
08/13/07 <1.0 <1.0 <1.0 <3.0 1.34 <1.0 <5 NR NR NR NR NR NR NR
03/12/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <1.0 <0.70 <0.50 <2.0 <100 <200 <100 <200
08/25/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
12/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
06/13/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 0.21 J <0.10 <0.10 <0.10 NR NR NR NR NR
10/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
04/02/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR
09/30/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR
04/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR NR
06/13/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
10/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/12/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <1.0 <0.70 <0.50 NR NR NR NR NR
08/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.67 <0.330 <0.330 NR NR NR NR NR
12/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
06/13/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
10/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
04/02/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR
09/30/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR
04/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR NR
08/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.67 <0.330 <0.330 NR NR NR NR NR
12/08/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/13/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
10/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
04/02/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
09/30/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
04/01/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/13/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
10/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
04/02/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
09/30/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
04/01/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
08/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.67 <0.330 <0.330 NR NR NR NR NR
12/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
06/13/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
10/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
04/02/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR
09/30/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR
04/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR NR
WSW-3
MW-15
MW-18
MW-16
WSW-1
MW-17
WSW-6
WSW-5
WSW-2
Page 3 of 4
EPA
Method
6010B
Well
ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 70 400 400 15 400 700 10,000 200
5,000 260,000 84,500 85,500 20,000 6,000 70,000 28,500 25,000 15,000 NE NE NE NE
Facility ID# 0-013895Date: 01/22/16
Analytical Method
→
GCL (µg/l)
MADEP Methods EPH & VPH
C19-C36 Aliphatics2L Standard (µg/l)EthylbenzeneTolueneLead1,2,4 -TrimethylbenzeneC9-C22 AromaticsBenzeneContaminant of Concern
→XylenesC9-C18 AliphaticsTABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
PEELE'S SERVICE STATION (INCIDENT NO. 10000)NaphthaleneC5-C8 AliphaticsEPA Method 6200B
1,3,5 -TrimethylbenzeneIPEMTBE03/01/07 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
08/13/07 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 <5.0 NR NR NR NR NR NR NR
03/12/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <1.0 <0.70 <0.50 NR NR NR NR NR
08/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.67 <0.330 <0.330 NR NR NR NR NR
12/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
06/13/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
10/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
04/02/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR
09/30/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR
04/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR NR
03/01/07 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
08/13/07 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 <5 NR NR NR NR NR NR NR
03/12/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <1.0 <0.70 <0.50 NR NR NR NR NR
08/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.67 <0.330 <0.330 NR NR NR NR NR
12/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
06/13/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
10/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
04/02/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR
09/30/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR
04/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR NR
03/01/07 <0.500 <0.500 <0.500 <1.500 <0.500 <5.00 <0.500 NR <0.500 NR NR NR NR NR
08/13/07 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/12/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
08/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.67 <0.330 <0.330 NR NR NR NR NR
12/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
06/13/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
10/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
04/02/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR
09/30/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR
04/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR NR
06/13/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
10/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
04/02/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
09/30/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
08/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.67 <0.330 <0.330 NR NR NR NR NR
12/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
06/13/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
10/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
04/02/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR
09/30/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
04/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR NR
WSW-62 04/02/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR
Notes:
• Results reported in µg/L (micrograms per liter).
• NS: Not sampled; well dry, insufficient water to sample or not located.
• NE: Standard not established.
• The concentration of n-propylbenzene (142 µg/l) reported in MW-11 exceeded the MAC on January 11, 2016.
• For other compounds reported which did not exceed the 2L Standards, refer to the laboratory reports.
• Concentrations in bold face type exceeded the 2L standard.
• I or J: Estimated value between the MDL and PQL .
• NR : Analysis not requested.
• < : Less than the method detection limit specified in the laboratory report.
• GCL : Gross contamination level as specified in T15A NCAC 2L.0202.
WSW-7
• 2L Standard : Maximum allowable concentrations as specified in T15A NCAC 2L.0202.
WSW-8
WSW-41/ DW-3
WSW-56
WSW-55
Page 4 of 4

APPENDIX

APPENDIX A
Laboratory Report – Ground Water Samples
01/21/16
Technical Report for
GRI (Geological Resources Inc.)
Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
2516
Accutest Job Number: FA30657
Sampling Date: 01/11/16
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
[e-mail]; [e-mail];
[e-mail]; [e-mail];
ATTN: William Regenthall
Total number of pages in report:
Certifications: FL (E83510), LA (03051), KS (E-10327), IA (366), IL (200063), NC (573), NJ (FL002), SC (96038001)
DoD ELAP (L-A-B L2229), CA (2937), TX (T104704404), PA (68-03573), VA (460177),
AK, AR, GA, KY, MA, NV, OK, UT, WA
This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone] • http://www.accutest.com
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Norm Farmer
Technical Director
Southeast
01/21/16
e-Hardcopy 2.0
Automated Report
39
Accutest Laboratories is the sole authority for authorizing edits or modifications to this
document. Unauthorized modification of this report is strictly prohibited.
Effective January 1, 2016, SGS has acquired all of the assets of Accutest Laboratories and will continue to
operate as SGS-Accutest. SGS-Accutest is part of SGS, the world's leading inspection, verification, testing and
certification company.
1 of 39
FA30657
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................6
3.1: FA30657-1: MW-1 ........................................................................................................7
3.2: FA30657-2: MW-2 ........................................................................................................9
3.3: FA30657-3: MW-2R .....................................................................................................11
3.4: FA30657-4: MW-3 ........................................................................................................13
3.5: FA30657-5: MW-11 ......................................................................................................15
3.6: FA30657-6: MW-14 ......................................................................................................17
3.7: FA30657-7: MW-15 ......................................................................................................19
3.8: FA30657-8: TRIP BLANK ...........................................................................................21
Section 4: Misc. Forms ............................................................................................................23
4.1: Chain of Custody ...........................................................................................................24
Section 5: GC/MS Volatiles - QC Data Summaries ..............................................................27
5.1: Method Blank Summary ................................................................................................28
5.2: Blank Spike Summary ...................................................................................................32
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................36 123452 of 39
FA30657
Accutest Laboratories
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA30657
Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Project No: 2516
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA30657-1 01/11/16 11:50 HM 01/13/16 AQ Ground Water MW-1
FA30657-2 01/11/16 11:40 HM 01/13/16 AQ Ground Water MW-2
FA30657-3 01/11/16 11:29 HM 01/13/16 AQ Ground Water MW-2R
FA30657-4 01/11/16 11:19 HM 01/13/16 AQ Ground Water MW-3
FA30657-5 01/11/16 11:07 HM 01/13/16 AQ Ground Water MW-11
FA30657-6 01/11/16 10:39 HM 01/13/16 AQ Ground Water MW-14
FA30657-7 01/11/16 10:53 HM 01/13/16 AQ Ground Water MW-15
FA30657-8 01/11/16 00:00 HM 01/13/16 AQ Trip Blank Water TRIP BLANK
3 of 39
FA30657 1
Summary of Hits Page 1 of 2
Job Number:FA30657
Account:GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Collected:01/11/16
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA30657-1 MW-1
Naphthalene 0.41 J 0.50 0.13 ug/l SM 6200B
1,2,4-Trimethylbenzene 0.95 0.50 0.13 ug/l SM 6200B
1,3,5-Trimethylbenzene 0.24 J 0.50 0.13 ug/l SM 6200B
m,p-Xylene 0.38 J 1.0 0.18 ug/l SM 6200B
o-Xylene 0.33 J 0.50 0.13 ug/l SM 6200B
Xylene (total)0.71 J 1.5 0.31 ug/l SM 6200B
FA30657-2 MW-2
Benzene 2.8 0.50 0.13 ug/l SM 6200B
Ethylbenzene 1.0 0.50 0.13 ug/l SM 6200B
Naphthalene 0.43 J 0.50 0.13 ug/l SM 6200B
Toluene 0.23 J 0.50 0.13 ug/l SM 6200B
1,2,4-Trimethylbenzene 1.5 0.50 0.13 ug/l SM 6200B
m,p-Xylene 0.45 J 1.0 0.18 ug/l SM 6200B
o-Xylene 3.1 0.50 0.13 ug/l SM 6200B
Xylene (total)3.6 1.5 0.31 ug/l SM 6200B
FA30657-3 MW-2R
Benzene 8.9 0.50 0.13 ug/l SM 6200B
n-Butylbenzene 0.57 0.50 0.13 ug/l SM 6200B
sec-Butylbenzene 0.40 J 0.50 0.13 ug/l SM 6200B
Ethylbenzene 22.7 0.50 0.13 ug/l SM 6200B
Isopropylbenzene 1.2 0.50 0.13 ug/l SM 6200B
p-Isopropyltoluene 0.57 0.50 0.13 ug/l SM 6200B
Naphthalene 23.0 0.50 0.13 ug/l SM 6200B
n-Propylbenzene 4.3 0.50 0.13 ug/l SM 6200B
Styrene 0.24 J 0.50 0.13 ug/l SM 6200B
Toluene 55.6 1.0 0.25 ug/l SM 6200B
1,2,4-Trimethylbenzene 70.3 1.0 0.25 ug/l SM 6200B
1,3,5-Trimethylbenzene 23.5 0.50 0.13 ug/l SM 6200B
m,p-Xylene 96.4 2.0 0.37 ug/l SM 6200B
o-Xylene 83.6 1.0 0.25 ug/l SM 6200B
Xylene (total)180 3.0 0.62 ug/l SM 6200B
FA30657-4 MW-3
1,2,4-Trimethylbenzene 0.14 J 0.50 0.13 ug/l SM 6200B
FA30657-5 MW-11
Benzene 3.4 J 10 2.5 ug/l SM 6200B
4 of 39
FA30657 2
Summary of Hits Page 2 of 2
Job Number:FA30657
Account:GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Collected:01/11/16
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
n-Butylbenzene 16.7 10 2.5 ug/l SM 6200B
sec-Butylbenzene 14.7 10 2.5 ug/l SM 6200B
Ethylbenzene 150 10 2.5 ug/l SM 6200B
Isopropylbenzene 49.9 10 2.5 ug/l SM 6200B
p-Isopropyltoluene 9.1 J 10 2.5 ug/l SM 6200B
Methylene Chloride B 40 20 ug/l SM 6200B
Naphthalene 476 10 2.5 ug/l SM 6200B
n-Propylbenzene 142 10 2.5 ug/l SM 6200B
Toluene 4.0 J 10 2.5 ug/l SM 6200B
1,2,4-Trimethylbenzene 1420 25 6.3 ug/l SM 6200B
1,3,5-Trimethylbenzene 318 10 2.5 ug/l SM 6200B
m,p-Xylene 643 20 3.7 ug/l SM 6200B
o-Xylene 438 10 2.5 ug/l SM 6200B
Xylene (total)1080 30 6.2 ug/l SM 6200B
FA30657-6 MW-14
Benzene 2.2 0.50 0.13 ug/l SM 6200B
n-Butylbenzene 0.64 0.50 0.13 ug/l SM 6200B
sec-Butylbenzene 0.43 J 0.50 0.13 ug/l SM 6200B
Di-Isopropyl Ether 0.64 0.50 0.13 ug/l SM 6200B
Ethylbenzene 0.18 J 0.50 0.13 ug/l SM 6200B
Isopropylbenzene 1.4 0.50 0.13 ug/l SM 6200B
Methyl Tert Butyl Ether 0.45 J 0.50 0.13 ug/l SM 6200B
Naphthalene 8.0 0.50 0.13 ug/l SM 6200B
n-Propylbenzene 2.5 0.50 0.13 ug/l SM 6200B
o-Xylene 1.1 0.50 0.13 ug/l SM 6200B
Xylene (total)1.1 J 1.5 0.31 ug/l SM 6200B
FA30657-7 MW-15
No hits reported in this sample.
FA30657-8 TRIP BLANK
No hits reported in this sample.
5 of 39
FA30657 2
Accutest Laboratories
Sample Results
Report of Analysis
Southeast
Section 3
6 of 39
FA30657 3
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-1
Lab Sample ID:FA30657-1 Date Sampled:01/11/16
Matrix:AQ - Ground Water Date Received:01/13/16
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E043406.D 1 01/19/16 TD n/a n/a VE1436
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.29 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
7 of 39
FA30657 33.1
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-1
Lab Sample ID:FA30657-1 Date Sampled:01/11/16
Matrix:AQ - Ground Water Date Received:01/13/16
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene 0.41 0.50 0.13 ug/l J
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.14 ug/l
95-63-6 1,2,4-Trimethylbenzene 0.95 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene 0.24 0.50 0.13 ug/l J
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 0.38 1.0 0.18 ug/l J
95-47-6 o-Xylene 0.33 0.50 0.13 ug/l J
1330-20-7 Xylene (total)0.71 1.5 0.31 ug/l J
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 97%70-130%
17060-07-0 1,2-Dichloroethane-D4 105%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
8 of 39
FA30657 33.1
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-2
Lab Sample ID:FA30657-2 Date Sampled:01/11/16
Matrix:AQ - Ground Water Date Received:01/13/16
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E043408.D 1 01/19/16 TD n/a n/a VE1436
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 2.8 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.29 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
9 of 39
FA30657 33.2
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-2
Lab Sample ID:FA30657-2 Date Sampled:01/11/16
Matrix:AQ - Ground Water Date Received:01/13/16
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene 1.0 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene 0.43 0.50 0.13 ug/l J
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene 0.23 0.50 0.13 ug/l J
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.14 ug/l
95-63-6 1,2,4-Trimethylbenzene 1.5 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 0.45 1.0 0.18 ug/l J
95-47-6 o-Xylene 3.1 0.50 0.13 ug/l
1330-20-7 Xylene (total)3.6 1.5 0.31 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 98%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 106%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 39
FA30657 33.2
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-2R
Lab Sample ID:FA30657-3 Date Sampled:01/11/16
Matrix:AQ - Ground Water Date Received:01/13/16
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E043409.D 1 01/19/16 TD n/a n/a VE1436
Run #2 E043420.D 2 01/19/16 TD n/a n/a VE1436
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 8.9 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene 0.57 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene 0.40 0.50 0.13 ug/l J
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.29 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 39
FA30657 33.3
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-2R
Lab Sample ID:FA30657-3 Date Sampled:01/11/16
Matrix:AQ - Ground Water Date Received:01/13/16
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene 22.7 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene 1.2 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene 0.57 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene 23.0 0.50 0.13 ug/l
103-65-1 n-Propylbenzene 4.3 0.50 0.13 ug/l
100-42-5 Styrene 0.24 0.50 0.13 ug/l J
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene 55.6 a 1.0 0.25 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.14 ug/l
95-63-6 1,2,4-Trimethylbenzene 70.3 a 1.0 0.25 ug/l
108-67-8 1,3,5-Trimethylbenzene 23.5 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 96.4 a 2.0 0.37 ug/l
95-47-6 o-Xylene 83.6 a 1.0 0.25 ug/l
1330-20-7 Xylene (total)180 a 3.0 0.62 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 98%98%70-130%
17060-07-0 1,2-Dichloroethane-D4 107%103%70-130%
2037-26-5 Toluene-D8 95%96%70-130%
460-00-4 4-Bromofluorobenzene 104%102%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 39
FA30657 33.3
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-3
Lab Sample ID:FA30657-4 Date Sampled:01/11/16
Matrix:AQ - Ground Water Date Received:01/13/16
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E043440.D 1 01/20/16 TD n/a n/a VE1437
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.29 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
13 of 39
FA30657 33.4
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-3
Lab Sample ID:FA30657-4 Date Sampled:01/11/16
Matrix:AQ - Ground Water Date Received:01/13/16
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.14 ug/l
95-63-6 1,2,4-Trimethylbenzene 0.14 0.50 0.13 ug/l J
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.18 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.31 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 98%70-130%
17060-07-0 1,2-Dichloroethane-D4 105%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 106%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
14 of 39
FA30657 33.4
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-11
Lab Sample ID:FA30657-5 Date Sampled:01/11/16
Matrix:AQ - Ground Water Date Received:01/13/16
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E043411.D 20 01/19/16 TD n/a n/a VE1436
Run #2 E043421.D 50 01/19/16 TD n/a n/a VE1436
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 3.4 10 2.5 ug/l J
108-86-1 Bromobenzene ND 10 2.5 ug/l
74-97-5 Bromochloromethane ND 10 2.5 ug/l
75-27-4 Bromodichloromethane ND 10 2.5 ug/l
75-25-2 Bromoform ND 10 2.5 ug/l
104-51-8 n-Butylbenzene 16.7 10 2.5 ug/l
135-98-8 sec-Butylbenzene 14.7 10 2.5 ug/l
98-06-6 tert-Butylbenzene ND 10 2.5 ug/l
56-23-5 Carbon Tetrachloride ND 10 2.5 ug/l
108-90-7 Chlorobenzene ND 10 2.5 ug/l
75-00-3 Chloroethane ND 10 4.0 ug/l
67-66-3 Chloroform ND 10 2.5 ug/l
95-49-8 o-Chlorotoluene ND 10 2.5 ug/l
106-43-4 p-Chlorotoluene ND 10 2.5 ug/l
124-48-1 Dibromochloromethane ND 10 2.5 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 10 5.7 ug/l
106-93-4 1,2-Dibromoethane ND 10 2.5 ug/l
75-71-8 Dichlorodifluoromethane ND 10 4.0 ug/l
95-50-1 1,2-Dichlorobenzene ND 10 2.5 ug/l
541-73-1 1,3-Dichlorobenzene ND 10 2.5 ug/l
106-46-7 1,4-Dichlorobenzene ND 10 2.5 ug/l
75-34-3 1,1-Dichloroethane ND 10 2.5 ug/l
107-06-2 1,2-Dichloroethane ND 10 2.5 ug/l
75-35-4 1,1-Dichloroethylene ND 10 2.5 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 10 2.5 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 10 2.5 ug/l
78-87-5 1,2-Dichloropropane ND 10 2.5 ug/l
142-28-9 1,3-Dichloropropane ND 10 2.5 ug/l
594-20-7 2,2-Dichloropropane ND 10 2.5 ug/l
563-58-6 1,1-Dichloropropene ND 10 2.5 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 10 2.5 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 10 2.5 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
15 of 39
FA30657 33.5
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-11
Lab Sample ID:FA30657-5 Date Sampled:01/11/16
Matrix:AQ - Ground Water Date Received:01/13/16
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 10 2.5 ug/l
100-41-4 Ethylbenzene 150 10 2.5 ug/l
87-68-3 Hexachlorobutadiene ND 10 2.5 ug/l
98-82-8 Isopropylbenzene 49.9 10 2.5 ug/l
99-87-6 p-Isopropyltoluene 9.1 10 2.5 ug/l J
74-83-9 Methyl Bromide ND 10 4.0 ug/l
74-87-3 Methyl Chloride ND 10 4.0 ug/l
74-95-3 Methylene Bromide ND 10 2.5 ug/l
75-09-2 Methylene Chloride B 40 20 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 10 2.5 ug/l
91-20-3 Naphthalene 476 10 2.5 ug/l
103-65-1 n-Propylbenzene 142 10 2.5 ug/l
100-42-5 Styrene ND 10 2.5 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 10 2.5 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 10 2.5 ug/l
127-18-4 Tetrachloroethylene ND 10 2.5 ug/l
108-88-3 Toluene 4.0 10 2.5 ug/l J
87-61-6 1,2,3-Trichlorobenzene ND 10 2.5 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 10 2.5 ug/l
71-55-6 1,1,1-Trichloroethane ND 10 2.5 ug/l
79-00-5 1,1,2-Trichloroethane ND 10 2.5 ug/l
79-01-6 Trichloroethylene ND 10 2.5 ug/l
75-69-4 Trichlorofluoromethane ND 10 4.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 10 2.8 ug/l
95-63-6 1,2,4-Trimethylbenzene 1420 a 25 6.3 ug/l
108-67-8 1,3,5-Trimethylbenzene 318 10 2.5 ug/l
75-01-4 Vinyl Chloride ND 10 2.5 ug/l
m,p-Xylene 643 20 3.7 ug/l
95-47-6 o-Xylene 438 10 2.5 ug/l
1330-20-7 Xylene (total)1080 30 6.2 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 99%98%70-130%
17060-07-0 1,2-Dichloroethane-D4 109%103%70-130%
2037-26-5 Toluene-D8 97%97%70-130%
460-00-4 4-Bromofluorobenzene 106%102%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
16 of 39
FA30657 33.5
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-14
Lab Sample ID:FA30657-6 Date Sampled:01/11/16
Matrix:AQ - Ground Water Date Received:01/13/16
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E043413.D 1 01/19/16 TD n/a n/a VE1436
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 2.2 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene 0.64 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene 0.43 0.50 0.13 ug/l J
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.29 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
17 of 39
FA30657 33.6
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-14
Lab Sample ID:FA30657-6 Date Sampled:01/11/16
Matrix:AQ - Ground Water Date Received:01/13/16
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 0.64 0.50 0.13 ug/l
100-41-4 Ethylbenzene 0.18 0.50 0.13 ug/l J
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene 1.4 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.45 0.50 0.13 ug/l J
91-20-3 Naphthalene 8.0 0.50 0.13 ug/l
103-65-1 n-Propylbenzene 2.5 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.14 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.18 ug/l
95-47-6 o-Xylene 1.1 0.50 0.13 ug/l
1330-20-7 Xylene (total)1.1 1.5 0.31 ug/l J
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 108%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 106%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
18 of 39
FA30657 33.6
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-15
Lab Sample ID:FA30657-7 Date Sampled:01/11/16
Matrix:AQ - Ground Water Date Received:01/13/16
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E043415.D 1 01/19/16 TD n/a n/a VE1436
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.29 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
19 of 39
FA30657 33.7
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-15
Lab Sample ID:FA30657-7 Date Sampled:01/11/16
Matrix:AQ - Ground Water Date Received:01/13/16
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.14 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.18 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.31 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 98%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%70-130%
2037-26-5 Toluene-D8 95%70-130%
460-00-4 4-Bromofluorobenzene 108%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
20 of 39
FA30657 33.7
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:TRIP BLANK
Lab Sample ID:FA30657-8 Date Sampled:01/11/16
Matrix:AQ - Trip Blank Water Date Received:01/13/16
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E043407.D 1 01/19/16 TD n/a n/a VE1436
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.29 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
21 of 39
FA30657 33.8
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:TRIP BLANK
Lab Sample ID:FA30657-8 Date Sampled:01/11/16
Matrix:AQ - Trip Blank Water Date Received:01/13/16
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.14 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.18 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.31 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 98%70-130%
17060-07-0 1,2-Dichloroethane-D4 105%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 105%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
22 of 39
FA30657 33.8
Accutest Laboratories
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Southeast
Section 4
23 of 39
FA30657 4
FA30657: Chain of Custody
Page 1 of 3
24 of 39
FA30657 44.1
FA30657: Chain of Custody
Page 2 of 3
25 of 39
FA30657 44.1
FA30657: Chain of Custody
Page 3 of 3
26 of 39
FA30657 44.1
Accutest Laboratories
GC/MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Southeast
Section 5
27 of 39
FA30657 5
Method Blank Summary Page 1 of 2
Job Number:FA30657
Account:GRINCC GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1436-MB E043405.D 1 01/19/16 TD n/a n/a VE1436
The QC reported here applies to the following samples:Method: SM 6200B
FA30657-1, FA30657-2, FA30657-3, FA30657-5, FA30657-6, FA30657-7, FA30657-8
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.29 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
28 of 39
FA30657 55.1.1
Method Blank Summary Page 2 of 2
Job Number:FA30657
Account:GRINCC GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1436-MB E043405.D 1 01/19/16 TD n/a n/a VE1436
The QC reported here applies to the following samples:Method: SM 6200B
FA30657-1, FA30657-2, FA30657-3, FA30657-5, FA30657-6, FA30657-7, FA30657-8
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride 2.3 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.14 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.18 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.31 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 97%70-130%
17060-07-0 1,2-Dichloroethane-D4 105%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 106%70-130%
29 of 39
FA30657 55.1.1
Method Blank Summary Page 1 of 2
Job Number:FA30657
Account:GRINCC GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1437-MB E043439.D 1 01/20/16 TD n/a n/a VE1437
The QC reported here applies to the following samples:Method: SM 6200B
FA30657-4
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.29 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
30 of 39
FA30657 55.1.2
Method Blank Summary Page 2 of 2
Job Number:FA30657
Account:GRINCC GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1437-MB E043439.D 1 01/20/16 TD n/a n/a VE1437
The QC reported here applies to the following samples:Method: SM 6200B
FA30657-4
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride 2.1 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.14 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.18 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.31 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 97%70-130%
17060-07-0 1,2-Dichloroethane-D4 105%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 106%70-130%
31 of 39
FA30657 55.1.2
Blank Spike Summary Page 1 of 2
Job Number:FA30657
Account:GRINCC GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1436-BS E043403.D 1 01/19/16 TD n/a n/a VE1436
The QC reported here applies to the following samples:Method: SM 6200B
FA30657-1, FA30657-2, FA30657-3, FA30657-5, FA30657-6, FA30657-7, FA30657-8
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 7.6 76 70-130
108-86-1 Bromobenzene 10 7.5 75 70-130
74-97-5 Bromochloromethane 10 7.2 72 70-130
75-27-4 Bromodichloromethane 10 7.3 73 70-130
75-25-2 Bromoform 10 7.5 75 70-130
104-51-8 n-Butylbenzene 10 7.4 74 70-130
135-98-8 sec-Butylbenzene 10 7.7 77 70-130
98-06-6 tert-Butylbenzene 10 7.5 75 70-130
56-23-5 Carbon Tetrachloride 10 8.0 80 70-130
108-90-7 Chlorobenzene 10 7.4 74 70-130
75-00-3 Chloroethane 10 12.2 122 60-140
67-66-3 Chloroform 10 7.7 77 70-130
95-49-8 o-Chlorotoluene 10 7.9 79 70-130
106-43-4 p-Chlorotoluene 10 7.7 77 70-130
124-48-1 Dibromochloromethane 10 7.7 77 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 7.6 76 70-130
106-93-4 1,2-Dibromoethane 10 7.1 71 70-130
75-71-8 Dichlorodifluoromethane 10 11.7 117 60-140
95-50-1 1,2-Dichlorobenzene 10 7.3 73 70-130
541-73-1 1,3-Dichlorobenzene 10 7.5 75 70-130
106-46-7 1,4-Dichlorobenzene 10 7.4 74 70-130
75-34-3 1,1-Dichloroethane 10 8.2 82 70-130
107-06-2 1,2-Dichloroethane 10 7.9 79 70-130
75-35-4 1,1-Dichloroethylene 10 8.6 86 70-130
156-59-2 cis-1,2-Dichloroethylene 10 7.4 74 70-130
156-60-5 trans-1,2-Dichloroethylene 10 8.8 88 70-130
78-87-5 1,2-Dichloropropane 10 7.6 76 70-130
142-28-9 1,3-Dichloropropane 10 7.2 72 70-130
594-20-7 2,2-Dichloropropane 10 8.2 82 70-130
563-58-6 1,1-Dichloropropene 10 8.1 81 70-130
10061-01-5 cis-1,3-Dichloropropene 10 7.1 71 70-130
10061-02-6 trans-1,3-Dichloropropene 10 7.5 75 70-130
108-20-3 Di-Isopropyl Ether 10 7.5 75 70-130
100-41-4 Ethylbenzene 10 7.4 74 70-130
87-68-3 Hexachlorobutadiene 10 7.6 76 70-130
98-82-8 Isopropylbenzene 10 7.4 74 70-130
* = Outside of Control Limits.
32 of 39
FA30657 55.2.1
Blank Spike Summary Page 2 of 2
Job Number:FA30657
Account:GRINCC GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1436-BS E043403.D 1 01/19/16 TD n/a n/a VE1436
The QC reported here applies to the following samples:Method: SM 6200B
FA30657-1, FA30657-2, FA30657-3, FA30657-5, FA30657-6, FA30657-7, FA30657-8
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 7.4 74 70-130
74-83-9 Methyl Bromide 10 11.2 112 60-140
74-87-3 Methyl Chloride 10 11.9 119 60-140
74-95-3 Methylene Bromide 10 7.5 75 70-130
75-09-2 Methylene Chloride 10 9.7 97 70-130
1634-04-4 Methyl Tert Butyl Ether 10 7.2 72 70-130
91-20-3 Naphthalene 10 7.8 78 70-130
103-65-1 n-Propylbenzene 10 8.0 80 70-130
100-42-5 Styrene 10 7.1 71 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 7.1 71 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 8.2 82 70-130
127-18-4 Tetrachloroethylene 10 7.4 74 70-130
108-88-3 Toluene 10 8.6 86 70-130
87-61-6 1,2,3-Trichlorobenzene 10 7.9 79 70-130
120-82-1 1,2,4-Trichlorobenzene 10 7.5 75 70-130
71-55-6 1,1,1-Trichloroethane 10 7.9 79 70-130
79-00-5 1,1,2-Trichloroethane 10 7.2 72 70-130
79-01-6 Trichloroethylene 10 7.9 79 70-130
75-69-4 Trichlorofluoromethane 10 11.0 110 60-140
96-18-4 1,2,3-Trichloropropane 10 7.7 77 70-130
95-63-6 1,2,4-Trimethylbenzene 10 7.3 73 70-130
108-67-8 1,3,5-Trimethylbenzene 10 7.3 73 70-130
75-01-4 Vinyl Chloride 10 11.5 115 60-140
m,p-Xylene 20 14.7 74 70-130
95-47-6 o-Xylene 10 7.1 71 70-130
1330-20-7 Xylene (total)30 21.8 73 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 105%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 103%70-130%
* = Outside of Control Limits.
33 of 39
FA30657 55.2.1
Blank Spike Summary Page 1 of 2
Job Number:FA30657
Account:GRINCC GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1437-BS E043451.D 1 01/20/16 TD n/a n/a VE1437
The QC reported here applies to the following samples:Method: SM 6200B
FA30657-4
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 11.4 114 70-130
108-86-1 Bromobenzene 10 11.1 111 70-130
74-97-5 Bromochloromethane 10 11.6 116 70-130
75-27-4 Bromodichloromethane 10 10.8 108 70-130
75-25-2 Bromoform 10 9.0 90 70-130
104-51-8 n-Butylbenzene 10 11.8 118 70-130
135-98-8 sec-Butylbenzene 10 12.0 120 70-130
98-06-6 tert-Butylbenzene 10 11.8 118 70-130
56-23-5 Carbon Tetrachloride 10 12.0 120 70-130
108-90-7 Chlorobenzene 10 11.2 112 70-130
75-00-3 Chloroethane 10 11.1 111 60-140
67-66-3 Chloroform 10 11.7 117 70-130
95-49-8 o-Chlorotoluene 10 11.9 119 70-130
106-43-4 p-Chlorotoluene 10 11.5 115 70-130
124-48-1 Dibromochloromethane 10 10.1 101 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 9.3 93 70-130
106-93-4 1,2-Dibromoethane 10 11.1 111 70-130
75-71-8 Dichlorodifluoromethane 10 8.3 83 60-140
95-50-1 1,2-Dichlorobenzene 10 11.3 113 70-130
541-73-1 1,3-Dichlorobenzene 10 11.4 114 70-130
106-46-7 1,4-Dichlorobenzene 10 11.1 111 70-130
75-34-3 1,1-Dichloroethane 10 12.2 122 70-130
107-06-2 1,2-Dichloroethane 10 11.7 117 70-130
75-35-4 1,1-Dichloroethylene 10 12.7 127 70-130
156-59-2 cis-1,2-Dichloroethylene 10 11.5 115 70-130
156-60-5 trans-1,2-Dichloroethylene 10 12.5 125 70-130
78-87-5 1,2-Dichloropropane 10 11.6 116 70-130
142-28-9 1,3-Dichloropropane 10 11.4 114 70-130
594-20-7 2,2-Dichloropropane 10 11.9 119 70-130
563-58-6 1,1-Dichloropropene 10 11.9 119 70-130
10061-01-5 cis-1,3-Dichloropropene 10 10.5 105 70-130
10061-02-6 trans-1,3-Dichloropropene 10 10.9 109 70-130
108-20-3 Di-Isopropyl Ether 10 12.2 122 70-130
100-41-4 Ethylbenzene 10 11.4 114 70-130
87-68-3 Hexachlorobutadiene 10 11.9 119 70-130
98-82-8 Isopropylbenzene 10 11.4 114 70-130
* = Outside of Control Limits.
34 of 39
FA30657 55.2.2
Blank Spike Summary Page 2 of 2
Job Number:FA30657
Account:GRINCC GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1437-BS E043451.D 1 01/20/16 TD n/a n/a VE1437
The QC reported here applies to the following samples:Method: SM 6200B
FA30657-4
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 11.6 116 70-130
74-83-9 Methyl Bromide 10 10.5 105 60-140
74-87-3 Methyl Chloride 10 9.9 99 60-140
74-95-3 Methylene Bromide 10 11.0 110 70-130
75-09-2 Methylene Chloride 10 12.7 127 70-130
1634-04-4 Methyl Tert Butyl Ether 10 11.5 115 70-130
91-20-3 Naphthalene 10 11.3 113 70-130
103-65-1 n-Propylbenzene 10 11.8 118 70-130
100-42-5 Styrene 10 10.1 101 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 11.2 112 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 11.1 111 70-130
127-18-4 Tetrachloroethylene 10 11.3 113 70-130
108-88-3 Toluene 10 10.9 109 70-130
87-61-6 1,2,3-Trichlorobenzene 10 11.6 116 70-130
120-82-1 1,2,4-Trichlorobenzene 10 11.8 118 70-130
71-55-6 1,1,1-Trichloroethane 10 12.1 121 70-130
79-00-5 1,1,2-Trichloroethane 10 11.2 112 70-130
79-01-6 Trichloroethylene 10 11.7 117 70-130
75-69-4 Trichlorofluoromethane 10 10.9 109 60-140
96-18-4 1,2,3-Trichloropropane 10 10.5 105 70-130
95-63-6 1,2,4-Trimethylbenzene 10 11.4 114 70-130
108-67-8 1,3,5-Trimethylbenzene 10 11.6 116 70-130
75-01-4 Vinyl Chloride 10 10.2 102 60-140
m,p-Xylene 20 22.7 114 70-130
95-47-6 o-Xylene 10 11.1 111 70-130
1330-20-7 Xylene (total)30 33.8 113 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 107%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
* = Outside of Control Limits.
35 of 39
FA30657 55.2.2
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA30657
Account:GRINCC GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA30657-6MS E043430.D 1 01/19/16 TD n/a n/a VE1436
FA30657-6MSD E043431.D 1 01/19/16 TD n/a n/a VE1436
FA30657-6 E043413.D 1 01/19/16 TD n/a n/a VE1436
The QC reported here applies to the following samples:Method: SM 6200B
FA30657-1, FA30657-2, FA30657-3, FA30657-5, FA30657-6, FA30657-7, FA30657-8
FA30657-6 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 2.2 10 15.0 128 10 13.2 110 13 70-130/20
108-86-1 Bromobenzene ND 10 12.4 124 10 11.0 110 12 70-130/20
74-97-5 Bromochloromethane ND 10 12.1 121 10 11.4 114 6 70-130/20
75-27-4 Bromodichloromethane ND 10 12.1 121 10 10.8 108 11 70-130/20
75-25-2 Bromoform ND 10 8.4 84 10 8.2 82 2 70-130/20
104-51-8 n-Butylbenzene 0.64 10 13.2 126 10 10.7 101 21*70-130/20
135-98-8 sec-Butylbenzene 0.43 J 10 13.6 132*10 11.2 108 19 70-130/20
98-06-6 tert-Butylbenzene ND 10 12.9 129 10 10.9 109 17 70-130/20
56-23-5 Carbon Tetrachloride ND 10 13.7 137*10 11.6 116 17 70-130/20
108-90-7 Chlorobenzene ND 10 12.6 126 10 11.0 110 14 70-130/20
75-00-3 Chloroethane ND 10 14.6 146*10 12.5 125 15 60-140/20
67-66-3 Chloroform ND 10 13.3 133*10 11.8 118 12 70-130/20
95-49-8 o-Chlorotoluene ND 10 13.1 131*10 11.0 110 17 70-130/20
106-43-4 p-Chlorotoluene ND 10 12.7 127 10 10.7 107 17 70-130/20
124-48-1 Dibromochloromethane ND 10 10.5 105 10 9.7 97 8 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 10 10 100 10 9.7 97 3 70-130/20
106-93-4 1,2-Dibromoethane ND 10 12.2 122 10 11.9 119 2 70-130/20
75-71-8 Dichlorodifluoromethane ND 10 15.7 157*10 13.8 138 13 60-140/20
95-50-1 1,2-Dichlorobenzene ND 10 12.2 122 10 10.9 109 11 70-130/20
541-73-1 1,3-Dichlorobenzene ND 10 12.6 126 10 10.9 109 14 70-130/20
106-46-7 1,4-Dichlorobenzene ND 10 12.2 122 10 10.7 107 13 70-130/20
75-34-3 1,1-Dichloroethane ND 10 14.2 142*10 12.5 125 13 70-130/20
107-06-2 1,2-Dichloroethane ND 10 13.0 130 10 12.4 124 5 70-130/20
75-35-4 1,1-Dichloroethylene ND 10 14.8 148*10 12.9 129 14 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 10 12.7 127 10 11.1 111 13 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 10 15.2 152*10 13.1 131*15 70-130/20
78-87-5 1,2-Dichloropropane ND 10 13.4 134*10 12.0 120 11 70-130/20
142-28-9 1,3-Dichloropropane ND 10 12.2 122 10 11.7 117 4 70-130/20
594-20-7 2,2-Dichloropropane ND 10 13.3 133*10 11.6 116 14 70-130/20
563-58-6 1,1-Dichloropropene ND 10 14.1 141*10 12.3 123 14 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 10 11.3 113 10 10.1 101 11 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 10 12.1 121 10 11.0 110 10 70-130/20
108-20-3 Di-Isopropyl Ether 0.64 10 13.4 128 10 12.1 115 10 70-130/20
100-41-4 Ethylbenzene 0.18 J 10 13.0 128 10 11.3 111 14 70-130/20
87-68-3 Hexachlorobutadiene ND 10 11.5 115 10 9.7 97 17 70-130/20
98-82-8 Isopropylbenzene 1.4 10 14.4 130 10 12.2 108 17 70-130/20
* = Outside of Control Limits.
36 of 39
FA30657 55.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA30657
Account:GRINCC GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA30657-6MS E043430.D 1 01/19/16 TD n/a n/a VE1436
FA30657-6MSD E043431.D 1 01/19/16 TD n/a n/a VE1436
FA30657-6 E043413.D 1 01/19/16 TD n/a n/a VE1436
The QC reported here applies to the following samples:Method: SM 6200B
FA30657-1, FA30657-2, FA30657-3, FA30657-5, FA30657-6, FA30657-7, FA30657-8
FA30657-6 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 10 12.7 127 10 10.4 104 20 70-130/20
74-83-9 Methyl Bromide ND 10 13.1 131 10 11.6 116 12 60-140/20
74-87-3 Methyl Chloride ND 10 14.4 144*10 12.8 128 12 60-140/20
74-95-3 Methylene Bromide ND 10 12.7 127 10 12.4 124 2 70-130/20
75-09-2 Methylene Chloride ND 10 12.8 128 10 11.4 114 12 70-130/20
1634-04-4 Methyl Tert Butyl Ether 0.45 J 10 12.4 120 10 11.9 115 4 70-130/20
91-20-3 Naphthalene 8.0 10 19.7 117 10 19.5 115 1 70-130/20
103-65-1 n-Propylbenzene 2.5 10 15.6 131*10 13.0 105 18 70-130/20
100-42-5 Styrene ND 10 11.0 110 10 9.4 94 16 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 10 12.5 125 10 11.0 110 13 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 10 11.9 119 10 11.8 118 1 70-130/20
127-18-4 Tetrachloroethylene ND 10 13.1 131*10 11.3 113 15 70-130/20
108-88-3 Toluene ND 10 12.2 122 10 10.6 106 14 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 10 11.7 117 10 11.3 113 3 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 10 11.8 118 10 10.8 108 9 70-130/20
71-55-6 1,1,1-Trichloroethane ND 10 13.6 136*10 12.0 120 13 70-130/20
79-00-5 1,1,2-Trichloroethane ND 10 12.7 127 10 12.9 129 2 70-130/20
79-01-6 Trichloroethylene ND 10 13.7 137*10 11.9 119 14 70-130/20
75-69-4 Trichlorofluoromethane ND 10 14.2 142*10 12.5 125 13 60-140/20
96-18-4 1,2,3-Trichloropropane ND 10 11.3 113 10 11.4 114 1 70-130/20
95-63-6 1,2,4-Trimethylbenzene ND 10 12.4 124 10 10.4 104 18 70-130/20
108-67-8 1,3,5-Trimethylbenzene ND 10 12.4 124 10 10.2 102 19 70-130/20
75-01-4 Vinyl Chloride ND 10 14.6 146*10 13.1 131 11 60-140/20
m,p-Xylene ND 20 25.7 129 20 22.0 110 16 70-130/20
95-47-6 o-Xylene 1.1 10 13.5 124 10 11.7 106 14 70-130/20
1330-20-7 Xylene (total)1.1 J 30 39.2 127 30 33.6 108 15 70-130/20
CAS No.Surrogate Recoveries MS MSD FA30657-6 Limits
1868-53-7 Dibromofluoromethane 99%101%99%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%111%108%70-130%
2037-26-5 Toluene-D8 99%98%97%70-130%
460-00-4 4-Bromofluorobenzene 100%100%106%70-130%
* = Outside of Control Limits.
37 of 39
FA30657 55.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA30657
Account:GRINCC GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA30658-12MS E043465.D 1 01/20/16 TD n/a n/a VE1437
FA30658-12MSD E043466.D 1 01/20/16 TD n/a n/a VE1437
FA30658-12 E043445.D 1 01/20/16 TD n/a n/a VE1437
The QC reported here applies to the following samples:Method: SM 6200B
FA30657-4
FA30658-12 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene ND 10 13.3 133*10 11.8 118 12 70-130/20
108-86-1 Bromobenzene ND 10 13.3 133*10 11.0 110 19 70-130/20
74-97-5 Bromochloromethane ND 10 12.4 124 10 11.1 111 11 70-130/20
75-27-4 Bromodichloromethane ND 10 12.3 123 10 10.9 109 12 70-130/20
75-25-2 Bromoform ND 10 7.9 79 10 7.7 77 3 70-130/20
104-51-8 n-Butylbenzene ND 10 13.6 136*10 11.2 112 19 70-130/20
135-98-8 sec-Butylbenzene 1.0 10 15.2 142*10 12.4 114 20 70-130/20
98-06-6 tert-Butylbenzene 0.48 J 10 14.3 138*10 11.7 112 20 70-130/20
56-23-5 Carbon Tetrachloride ND 10 14.0 140*10 11.7 117 18 70-130/20
108-90-7 Chlorobenzene ND 10 12.9 129 10 11.2 112 14 70-130/20
75-00-3 Chloroethane ND 10 13.7 137 10 10.9 109 23*60-140/20
67-66-3 Chloroform ND 10 13.6 136*10 12.0 120 13 70-130/20
95-49-8 o-Chlorotoluene ND 10 14.2 142*10 11.4 114 22*70-130/20
106-43-4 p-Chlorotoluene ND 10 13.8 138*10 11.2 112 21*70-130/20
124-48-1 Dibromochloromethane ND 10 10.1 101 10 9.3 93 8 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 10 11.0 110 10 9.2 92 18 70-130/20
106-93-4 1,2-Dibromoethane ND 10 12.8 128 10 11.3 113 12 70-130/20
75-71-8 Dichlorodifluoromethane ND 10 11.1 111 10 9.5 95 16 60-140/20
95-50-1 1,2-Dichlorobenzene ND 10 13.1 131*10 11.0 110 17 70-130/20
541-73-1 1,3-Dichlorobenzene ND 10 13.5 135*10 11.2 112 19 70-130/20
106-46-7 1,4-Dichlorobenzene ND 10 13.1 131*10 10.9 109 18 70-130/20
75-34-3 1,1-Dichloroethane ND 10 14.7 147*10 12.8 128 14 70-130/20
107-06-2 1,2-Dichloroethane 0.22 J 10 13.9 137*10 12.6 124 10 70-130/20
75-35-4 1,1-Dichloroethylene ND 10 15.5 155*10 13.2 132*16 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 10 12.8 128 10 11.5 115 11 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 10 15.9 159*10 13.6 136*16 70-130/20
78-87-5 1,2-Dichloropropane ND 10 13.7 137*10 12.2 122 12 70-130/20
142-28-9 1,3-Dichloropropane ND 10 12.8 128 10 11.5 115 11 70-130/20
594-20-7 2,2-Dichloropropane ND 10 13.2 132*10 11.3 113 16 70-130/20
563-58-6 1,1-Dichloropropene ND 10 14.2 142*10 12.4 124 14 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 10 12.3 123 10 10.6 106 15 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 10 13.2 132*10 11.4 114 15 70-130/20
108-20-3 Di-Isopropyl Ether 16.6 10 31.1 145*10 27.5 109 12 70-130/20
100-41-4 Ethylbenzene 0.21 J 10 13.4 132*10 11.5 113 15 70-130/20
87-68-3 Hexachlorobutadiene ND 10 11.9 119 10 10.5 105 13 70-130/20
98-82-8 Isopropylbenzene 5.3 10 19.1 138*10 16.4 111 15 70-130/20
* = Outside of Control Limits.
38 of 39
FA30657 55.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA30657
Account:GRINCC GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA30658-12MS E043465.D 1 01/20/16 TD n/a n/a VE1437
FA30658-12MSD E043466.D 1 01/20/16 TD n/a n/a VE1437
FA30658-12 E043445.D 1 01/20/16 TD n/a n/a VE1437
The QC reported here applies to the following samples:Method: SM 6200B
FA30657-4
FA30658-12 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 10 13.3 133*10 10.8 108 21*70-130/20
74-83-9 Methyl Bromide ND 10 12.3 123 10 10.4 104 17 60-140/20
74-87-3 Methyl Chloride ND 10 11.8 118 10 10.1 101 16 60-140/20
74-95-3 Methylene Bromide ND 10 13.5 135*10 12.1 121 11 70-130/20
75-09-2 Methylene Chloride ND 10 13.8 138*10 11.9 119 15 70-130/20
1634-04-4 Methyl Tert Butyl Ether 0.34 J 10 12.9 126 10 11.7 114 10 70-130/20
91-20-3 Naphthalene 11.8 10 26.4 146*10 24.8 130 6 70-130/20
103-65-1 n-Propylbenzene 0.68 10 15.3 146*10 12.3 116 22*70-130/20
100-42-5 Styrene ND 10 10.8 108 10 8.9 89 19 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 10 12.7 127 10 10.9 109 15 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 10 15.2 152*10 13.2 132*14 70-130/20
127-18-4 Tetrachloroethylene ND 10 12.9 129 10 11.1 111 15 70-130/20
108-88-3 Toluene ND 10 12.3 123 10 10.7 107 14 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 10 12.3 123 10 11.7 117 5 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 10 12.4 124 10 11.3 113 9 70-130/20
71-55-6 1,1,1-Trichloroethane ND 10 14.0 140*10 12.1 121 15 70-130/20
79-00-5 1,1,2-Trichloroethane ND 10 13.6 136*10 12.2 122 11 70-130/20
79-01-6 Trichloroethylene ND 10 14.7 147*10 12.8 128 14 70-130/20
75-69-4 Trichlorofluoromethane ND 10 13.1 131 10 11.0 110 17 60-140/20
96-18-4 1,2,3-Trichloropropane ND 10 12.2 122 10 10.8 108 12 70-130/20
95-63-6 1,2,4-Trimethylbenzene 0.51 10 13.4 129 10 10.8 103 21*70-130/20
108-67-8 1,3,5-Trimethylbenzene ND 10 13.2 132*10 10.6 106 22*70-130/20
75-01-4 Vinyl Chloride ND 10 13.2 132 10 11.1 111 17 60-140/20
m,p-Xylene 0.19 J 20 26.3 131*20 22.4 111 16 70-130/20
95-47-6 o-Xylene 0.15 J 10 12.9 128 10 11.0 109 16 70-130/20
1330-20-7 Xylene (total)0.34 J 30 39.2 130 30 33.4 110 16 70-130/20
CAS No.Surrogate Recoveries MS MSD FA30658-12 Limits
1868-53-7 Dibromofluoromethane 100%101%99%70-130%
17060-07-0 1,2-Dichloroethane-D4 107%112%110%70-130%
2037-26-5 Toluene-D8 99%98%98%70-130%
460-00-4 4-Bromofluorobenzene 106%102%104%70-130%
* = Outside of Control Limits.
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FA30657 55.3.2