WA-706_10000_CA_RPTS_20141016_MRP

10/13/14
Technical Report for
GRI (Geological Resources Inc.)
Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
2516
Accutest Job Number: FA18806
Sampling Date: 09/30/14
Report to:
GRI
[e-mail]
[e-mail]; [e-mail]; [e-mail]; [e-mail]
ATTN: William Regenthall
Total number of pages in report:
Certifications: FL (E83510), LA (03051), KS (E-10327), IA (366), IL (200063), NC (573), NJ (FL002), SC (96038001)
DoD ELAP (L-A-B L2229), CA (04226CA), TX (T104704404), PA (68-03573), VA (460177),
AK, AR, GA, KY, MA, NV, OK, UT, WA
This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone] • http://www.accutest.com
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Norm Farmer
Technical Director
Southeast
10/13/14
Reissue #1
e-Hardcopy 2.0
Automated Report
55
Accutest Laboratories is the sole authority for authorizing edits or modifications to this
document. Unauthorized modification of this report is strictly prohibited.
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FA18806
Florida  4405 Vineland Road  Suite C-15  Orlando, FL 32811  tel: [phone]  fax: [phone]  htpp://www.accutest.com www.accutest.com

October 13, 2014

Ms. Angela Roach
Geological Resources Inc
2301 F. Crown Point EX Dr
Charlotte, NC 28207

RE: Accutest job FA18806 Reissue

Dear Ms. Roach,

The final report for job number FA18806 has been edited to reflect requested corrections.
These edits have been incorporated into the revised report.

The sample ID has been revised.

Accutest apologies for any inconvenience this may have caused. Please feel free to contact
us if we can be of further assistance.

Sincerely,

Accutest Laboratories, SE

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FA18806
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................4
Section 2: Summary of Hits ....................................................................................................6
Section 3: Sample Results ........................................................................................................9
3.1: FA18806-1: MW-1 ........................................................................................................10
3.2: FA18806-2: MW-4 ........................................................................................................12
3.3: FA18806-3: MW-5 ........................................................................................................14
3.4: FA18806-4: MW-8 ........................................................................................................16
3.5: FA18806-5: MW-10 ......................................................................................................18
3.6: FA18806-6: MW-11 ......................................................................................................20
3.7: FA18806-7: MW-14 ......................................................................................................22
3.8: FA18806-8: MW-17 ......................................................................................................24
3.9: FA18806-9: MW-18 ......................................................................................................26
3.10: FA18806-10: WSW-2 .................................................................................................28
3.11: FA18806-11: WSW-6 ..................................................................................................30
3.12: FA18806-12: WSW-7 .................................................................................................32
3.13: FA18806-13: WSW-8 .................................................................................................34
3.14: FA18806-14: WSW-41 ...............................................................................................36
Section 4: Misc. Forms ............................................................................................................38
4.1: Chain of Custody ...........................................................................................................39
Section 5: GC/MS Volatiles - QC Data Summaries ..............................................................43
5.1: Method Blank Summary ................................................................................................44
5.2: Blank Spike Summary ...................................................................................................48
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................52 123453 of 55
FA18806
Accutest Laboratories
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA18806
Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Project No: 2516
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA18806-1 09/30/14 09:41 HM 10/01/14 AQ Ground Water MW-1
FA18806-2 09/30/14 09:57 HM 10/01/14 AQ Ground Water MW-4
FA18806-3 09/30/14 09:50 HM 10/01/14 AQ Ground Water MW-5
FA18806-4 09/30/14 09:30 HM 10/01/14 AQ Ground Water MW-8
FA18806-5 09/30/14 10:23 HM 10/01/14 AQ Ground Water MW-10
FA18806-6 09/30/14 10:16 HM 10/01/14 AQ Ground Water MW-11
FA18806-7 09/30/14 10:50 HM 10/01/14 AQ Ground Water MW-14
FA18806-8 09/30/14 11:28 HM 10/01/14 AQ Ground Water MW-17
FA18806-9 09/30/14 11:37 HM 10/01/14 AQ Ground Water MW-18
FA18806-10 09/30/14 12:15 HM 10/01/14 AQ Ground Water WSW-2
FA18806-11 09/30/14 12:08 HM 10/01/14 AQ Ground Water WSW-6
FA18806-12 09/30/14 12:01 HM 10/01/14 AQ Ground Water WSW-7
FA18806-13 09/30/14 11:55 HM 10/01/14 AQ Ground Water WSW-8
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FA18806 1
Accutest Laboratories
Sample Summary
(continued)
GRI (Geological Resources Inc.)
Job No:FA18806
Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Project No: 2516
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA18806-14 09/30/14 11:41 HM 10/01/14 AQ Ground Water WSW-41
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FA18806 1
Summary of Hits Page 1 of 3
Job Number:FA18806
Account:GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Collected:09/30/14
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA18806-1 MW-1
Benzene 1.9 J 5.0 1.0 ug/l SM 6200B
sec-Butylbenzene 1.4 J 5.0 1.0 ug/l SM 6200B
Ethylbenzene 5.7 5.0 1.0 ug/l SM 6200B
Isopropylbenzene 2.3 J 5.0 1.0 ug/l SM 6200B
p-Isopropyltoluene 1.3 J 5.0 1.0 ug/l SM 6200B
Naphthalene 88.7 5.0 1.0 ug/l SM 6200B
n-Propylbenzene 3.5 J 5.0 1.0 ug/l SM 6200B
1,2,4-Trimethylbenzene 331 5.0 1.0 ug/l SM 6200B
1,3,5-Trimethylbenzene 56.6 5.0 1.0 ug/l SM 6200B
Toluene 3.4 J 5.0 1.0 ug/l SM 6200B
Xylene (total)326 15 2.0 ug/l SM 6200B
m,p-Xylene 95.6 10 1.0 ug/l SM 6200B
o-Xylene 231 5.0 1.0 ug/l SM 6200B
FA18806-2 MW-4
Methyl chloride 0.10 J 0.50 0.10 ug/l SM 6200B
FA18806-3 MW-5
Methyl chloride 0.19 J 0.50 0.10 ug/l SM 6200B
Methyl Tert Butyl Ether 0.61 0.50 0.10 ug/l SM 6200B
Tetrachloroethylene 0.34 J 0.50 0.10 ug/l SM 6200B
FA18806-4 MW-8
Methyl chloride 0.15 J 0.50 0.10 ug/l SM 6200B
FA18806-5 MW-10
p-Isopropyltoluene 1.3 0.50 0.10 ug/l SM 6200B
Methyl chloride 0.24 J 0.50 0.10 ug/l SM 6200B
Naphthalene 0.27 J 0.50 0.10 ug/l SM 6200B
1,2,4-Trimethylbenzene 0.21 J 0.50 0.10 ug/l SM 6200B
FA18806-6 MW-11
Benzene 6.7 2.5 0.50 ug/l SM 6200B
n-Butylbenzene 2.8 2.5 0.50 ug/l SM 6200B
sec-Butylbenzene 4.7 2.5 0.50 ug/l SM 6200B
Ethylbenzene 27.9 2.5 0.50 ug/l SM 6200B
Isopropylbenzene 23.1 2.5 0.50 ug/l SM 6200B
p-Isopropyltoluene 2.0 J 2.5 0.50 ug/l SM 6200B
6 of 55
FA18806 2
Summary of Hits Page 2 of 3
Job Number:FA18806
Account:GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Collected:09/30/14
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
Naphthalene 135 2.5 0.50 ug/l SM 6200B
n-Propylbenzene 44.0 2.5 0.50 ug/l SM 6200B
1,2,4-Trimethylbenzene 194 2.5 0.50 ug/l SM 6200B
1,3,5-Trimethylbenzene 20.9 2.5 0.50 ug/l SM 6200B
Toluene 0.61 J 2.5 0.50 ug/l SM 6200B
Xylene (total)172 7.5 1.0 ug/l SM 6200B
m,p-Xylene 152 5.0 0.50 ug/l SM 6200B
o-Xylene 19.6 2.5 0.50 ug/l SM 6200B
FA18806-7 MW-14
Benzene 2.5 0.50 0.10 ug/l SM 6200B
sec-Butylbenzene 0.19 J 0.50 0.10 ug/l SM 6200B
Di-Isopropyl ether 1.7 0.50 0.10 ug/l SM 6200B
Isopropylbenzene 1.4 0.50 0.10 ug/l SM 6200B
Methyl chloride 0.12 J 0.50 0.10 ug/l SM 6200B
Methyl Tert Butyl Ether 2.0 0.50 0.10 ug/l SM 6200B
Naphthalene 4.2 0.50 0.10 ug/l SM 6200B
n-Propylbenzene 1.0 0.50 0.10 ug/l SM 6200B
1,3,5-Trimethylbenzene 0.10 J 0.50 0.10 ug/l SM 6200B
Toluene 0.15 J 0.50 0.10 ug/l SM 6200B
Xylene (total)1.3 J 1.5 0.20 ug/l SM 6200B
m,p-Xylene 0.23 J 1.0 0.10 ug/l SM 6200B
o-Xylene 1.1 0.50 0.10 ug/l SM 6200B
FA18806-8 MW-17
Methyl chloride 0.14 J 0.50 0.10 ug/l SM 6200B
FA18806-9 MW-18
Methyl chloride 0.15 J 0.50 0.10 ug/l SM 6200B
FA18806-10 WSW-2
No hits reported in this sample.
FA18806-11 WSW-6
Methyl chloride 0.22 J 0.50 0.10 ug/l SM 6200B
FA18806-12 WSW-7
Methyl chloride 0.19 J 0.50 0.10 ug/l SM 6200B
Trichloroethylene 0.22 J 0.50 0.10 ug/l SM 6200B
7 of 55
FA18806 2
Summary of Hits Page 3 of 3
Job Number:FA18806
Account:GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Collected:09/30/14
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA18806-13 WSW-8
Methyl chloride 0.14 J 0.50 0.10 ug/l SM 6200B
FA18806-14 WSW-41
Methyl chloride 0.27 J 0.50 0.10 ug/l SM 6200B
Trichloroethylene 0.30 J 0.50 0.10 ug/l SM 6200B
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FA18806 2
Accutest Laboratories
Sample Results
Report of Analysis
Southeast
Section 3
9 of 55
FA18806 3
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-1
Lab Sample ID:FA18806-1 Date Sampled:09/30/14
Matrix:AQ - Ground Water Date Received:10/01/14
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E033700.D 10 10/06/14 EG n/a n/a VE1124
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 1.9 5.0 1.0 ug/l J
108-86-1 Bromobenzene ND 5.0 1.0 ug/l
74-97-5 Bromochloromethane ND 5.0 1.0 ug/l
75-27-4 Bromodichloromethane ND 5.0 1.0 ug/l
75-25-2 Bromoform ND 5.0 1.0 ug/l
104-51-8 n-Butylbenzene ND 5.0 1.0 ug/l
135-98-8 sec-Butylbenzene 1.4 5.0 1.0 ug/l J
98-06-6 tert-Butylbenzene ND 5.0 1.0 ug/l
108-90-7 Chlorobenzene ND 5.0 1.0 ug/l
75-00-3 Chloroethane ND 5.0 1.2 ug/l
67-66-3 Chloroform ND 5.0 1.0 ug/l
95-49-8 o-Chlorotoluene ND 5.0 1.0 ug/l
106-43-4 p-Chlorotoluene ND 5.0 1.0 ug/l
56-23-5 Carbon tetrachloride ND 5.0 1.0 ug/l
75-34-3 1,1-Dichloroethane ND 5.0 1.0 ug/l
75-35-4 1,1-Dichloroethylene ND 5.0 1.0 ug/l
563-58-6 1,1-Dichloropropene ND 5.0 1.0 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 5.0 1.7 ug/l
106-93-4 1,2-Dibromoethane ND 5.0 1.0 ug/l
107-06-2 1,2-Dichloroethane ND 5.0 1.0 ug/l
78-87-5 1,2-Dichloropropane ND 5.0 1.0 ug/l
142-28-9 1,3-Dichloropropane ND 5.0 1.0 ug/l
108-20-3 Di-Isopropyl ether ND 5.0 1.0 ug/l
594-20-7 2,2-Dichloropropane ND 5.0 1.0 ug/l
124-48-1 Dibromochloromethane ND 5.0 1.0 ug/l
75-71-8 Dichlorodifluoromethane ND 5.0 1.0 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.0 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.0 ug/l
541-73-1 m-Dichlorobenzene ND 5.0 1.0 ug/l
95-50-1 o-Dichlorobenzene ND 5.0 1.0 ug/l
106-46-7 p-Dichlorobenzene ND 5.0 1.0 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.0 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 55
FA18806 33.1
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-1
Lab Sample ID:FA18806-1 Date Sampled:09/30/14
Matrix:AQ - Ground Water Date Received:10/01/14
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.0 ug/l
100-41-4 Ethylbenzene 5.7 5.0 1.0 ug/l
87-68-3 Hexachlorobutadiene ND 5.0 1.0 ug/l
98-82-8 Isopropylbenzene 2.3 5.0 1.0 ug/l J
99-87-6 p-Isopropyltoluene 1.3 5.0 1.0 ug/l J
74-83-9 Methyl bromide ND 5.0 1.0 ug/l
74-87-3 Methyl chloride ND 5.0 1.0 ug/l
74-95-3 Methylene bromide ND 5.0 1.0 ug/l
75-09-2 Methylene chloride ND 20 10 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 5.0 1.0 ug/l
91-20-3 Naphthalene 88.7 5.0 1.0 ug/l
103-65-1 n-Propylbenzene 3.5 5.0 1.0 ug/l J
100-42-5 Styrene ND 5.0 1.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 5.0 1.0 ug/l
71-55-6 1,1,1-Trichloroethane ND 5.0 1.0 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 1.0 ug/l
79-00-5 1,1,2-Trichloroethane ND 5.0 1.1 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 5.0 1.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 5.0 1.2 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.0 ug/l
95-63-6 1,2,4-Trimethylbenzene 331 5.0 1.0 ug/l
108-67-8 1,3,5-Trimethylbenzene 56.6 5.0 1.0 ug/l
127-18-4 Tetrachloroethylene ND 5.0 1.0 ug/l
108-88-3 Toluene 3.4 5.0 1.0 ug/l J
79-01-6 Trichloroethylene ND 5.0 1.0 ug/l
75-69-4 Trichlorofluoromethane ND 5.0 1.0 ug/l
75-01-4 Vinyl chloride ND 5.0 1.0 ug/l
1330-20-7 Xylene (total)326 15 2.0 ug/l
m,p-Xylene 95.6 10 1.0 ug/l
95-47-6 o-Xylene 231 5.0 1.0 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 113%70-130%
17060-07-0 1,2-Dichloroethane-D4 113%70-130%
2037-26-5 Toluene-D8 96%70-130%
460-00-4 4-Bromofluorobenzene 91%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 55
FA18806 33.1
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-4
Lab Sample ID:FA18806-2 Date Sampled:09/30/14
Matrix:AQ - Ground Water Date Received:10/01/14
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E033701.D 1 10/06/14 EG n/a n/a VE1124
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 55
FA18806 33.2
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-4
Lab Sample ID:FA18806-2 Date Sampled:09/30/14
Matrix:AQ - Ground Water Date Received:10/01/14
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride 0.10 0.50 0.10 ug/l J
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 113%70-130%
17060-07-0 1,2-Dichloroethane-D4 111%70-130%
2037-26-5 Toluene-D8 95%70-130%
460-00-4 4-Bromofluorobenzene 95%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
13 of 55
FA18806 33.2
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-5
Lab Sample ID:FA18806-3 Date Sampled:09/30/14
Matrix:AQ - Ground Water Date Received:10/01/14
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E033702.D 1 10/06/14 EG n/a n/a VE1124
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
14 of 55
FA18806 33.3
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-5
Lab Sample ID:FA18806-3 Date Sampled:09/30/14
Matrix:AQ - Ground Water Date Received:10/01/14
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride 0.19 0.50 0.10 ug/l J
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.61 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene 0.34 0.50 0.10 ug/l J
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 114%70-130%
17060-07-0 1,2-Dichloroethane-D4 114%70-130%
2037-26-5 Toluene-D8 86%70-130%
460-00-4 4-Bromofluorobenzene 93%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
15 of 55
FA18806 33.3
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-8
Lab Sample ID:FA18806-4 Date Sampled:09/30/14
Matrix:AQ - Ground Water Date Received:10/01/14
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E033703.D 1 10/06/14 EG n/a n/a VE1124
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
16 of 55
FA18806 33.4
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-8
Lab Sample ID:FA18806-4 Date Sampled:09/30/14
Matrix:AQ - Ground Water Date Received:10/01/14
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride 0.15 0.50 0.10 ug/l J
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 113%70-130%
17060-07-0 1,2-Dichloroethane-D4 114%70-130%
2037-26-5 Toluene-D8 92%70-130%
460-00-4 4-Bromofluorobenzene 94%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
17 of 55
FA18806 33.4
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-10
Lab Sample ID:FA18806-5 Date Sampled:09/30/14
Matrix:AQ - Ground Water Date Received:10/01/14
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E033704.D 1 10/06/14 EG n/a n/a VE1124
Run #2 a E033729.D 1 10/07/14 EG n/a n/a VE1125
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
18 of 55
FA18806 33.5
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-10
Lab Sample ID:FA18806-5 Date Sampled:09/30/14
Matrix:AQ - Ground Water Date Received:10/01/14
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene 1.3 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride 0.24 0.50 0.10 ug/l J
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene 0.27 0.50 0.10 ug/l J
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene 0.21 0.50 0.10 ug/l J
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 115%110%70-130%
17060-07-0 1,2-Dichloroethane-D4 117%111%70-130%
2037-26-5 Toluene-D8 91%95%70-130%
460-00-4 4-Bromofluorobenzene 87%92%70-130%
(a) Confirmation run for internal standard areas.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
19 of 55
FA18806 33.5
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-11
Lab Sample ID:FA18806-6 Date Sampled:09/30/14
Matrix:AQ - Ground Water Date Received:10/01/14
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E033708.D 5 10/06/14 EG n/a n/a VE1124
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 6.7 2.5 0.50 ug/l
108-86-1 Bromobenzene ND 2.5 0.50 ug/l
74-97-5 Bromochloromethane ND 2.5 0.50 ug/l
75-27-4 Bromodichloromethane ND 2.5 0.50 ug/l
75-25-2 Bromoform ND 2.5 0.50 ug/l
104-51-8 n-Butylbenzene 2.8 2.5 0.50 ug/l
135-98-8 sec-Butylbenzene 4.7 2.5 0.50 ug/l
98-06-6 tert-Butylbenzene ND 2.5 0.50 ug/l
108-90-7 Chlorobenzene ND 2.5 0.50 ug/l
75-00-3 Chloroethane ND 2.5 0.61 ug/l
67-66-3 Chloroform ND 2.5 0.50 ug/l
95-49-8 o-Chlorotoluene ND 2.5 0.50 ug/l
106-43-4 p-Chlorotoluene ND 2.5 0.50 ug/l
56-23-5 Carbon tetrachloride ND 2.5 0.50 ug/l
75-34-3 1,1-Dichloroethane ND 2.5 0.50 ug/l
75-35-4 1,1-Dichloroethylene ND 2.5 0.50 ug/l
563-58-6 1,1-Dichloropropene ND 2.5 0.50 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 2.5 0.86 ug/l
106-93-4 1,2-Dibromoethane ND 2.5 0.50 ug/l
107-06-2 1,2-Dichloroethane ND 2.5 0.50 ug/l
78-87-5 1,2-Dichloropropane ND 2.5 0.50 ug/l
142-28-9 1,3-Dichloropropane ND 2.5 0.50 ug/l
108-20-3 Di-Isopropyl ether ND 2.5 0.50 ug/l
594-20-7 2,2-Dichloropropane ND 2.5 0.50 ug/l
124-48-1 Dibromochloromethane ND 2.5 0.50 ug/l
75-71-8 Dichlorodifluoromethane ND 2.5 0.50 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 2.5 0.50 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 2.5 0.50 ug/l
541-73-1 m-Dichlorobenzene ND 2.5 0.50 ug/l
95-50-1 o-Dichlorobenzene ND 2.5 0.50 ug/l
106-46-7 p-Dichlorobenzene ND 2.5 0.50 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 2.5 0.50 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
20 of 55
FA18806 33.6
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-11
Lab Sample ID:FA18806-6 Date Sampled:09/30/14
Matrix:AQ - Ground Water Date Received:10/01/14
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 2.5 0.50 ug/l
100-41-4 Ethylbenzene 27.9 2.5 0.50 ug/l
87-68-3 Hexachlorobutadiene ND 2.5 0.50 ug/l
98-82-8 Isopropylbenzene 23.1 2.5 0.50 ug/l
99-87-6 p-Isopropyltoluene 2.0 2.5 0.50 ug/l J
74-83-9 Methyl bromide ND 2.5 0.50 ug/l
74-87-3 Methyl chloride ND 2.5 0.50 ug/l
74-95-3 Methylene bromide ND 2.5 0.50 ug/l
75-09-2 Methylene chloride ND 10 5.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 2.5 0.50 ug/l
91-20-3 Naphthalene 135 2.5 0.50 ug/l
103-65-1 n-Propylbenzene 44.0 2.5 0.50 ug/l
100-42-5 Styrene ND 2.5 0.50 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 2.5 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 2.5 0.50 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 2.5 0.50 ug/l
79-00-5 1,1,2-Trichloroethane ND 2.5 0.53 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 2.5 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.5 0.59 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 2.5 0.50 ug/l
95-63-6 1,2,4-Trimethylbenzene 194 2.5 0.50 ug/l
108-67-8 1,3,5-Trimethylbenzene 20.9 2.5 0.50 ug/l
127-18-4 Tetrachloroethylene ND 2.5 0.50 ug/l
108-88-3 Toluene 0.61 2.5 0.50 ug/l J
79-01-6 Trichloroethylene ND 2.5 0.50 ug/l
75-69-4 Trichlorofluoromethane ND 2.5 0.50 ug/l
75-01-4 Vinyl chloride ND 2.5 0.50 ug/l
1330-20-7 Xylene (total)172 7.5 1.0 ug/l
m,p-Xylene 152 5.0 0.50 ug/l
95-47-6 o-Xylene 19.6 2.5 0.50 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 107%70-130%
17060-07-0 1,2-Dichloroethane-D4 107%70-130%
2037-26-5 Toluene-D8 96%70-130%
460-00-4 4-Bromofluorobenzene 95%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
21 of 55
FA18806 33.6
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-14
Lab Sample ID:FA18806-7 Date Sampled:09/30/14
Matrix:AQ - Ground Water Date Received:10/01/14
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E033709.D 1 10/06/14 EG n/a n/a VE1124
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 2.5 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene 0.19 0.50 0.10 ug/l J
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether 1.7 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
22 of 55
FA18806 33.7
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-14
Lab Sample ID:FA18806-7 Date Sampled:09/30/14
Matrix:AQ - Ground Water Date Received:10/01/14
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene 1.4 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride 0.12 0.50 0.10 ug/l J
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 2.0 0.50 0.10 ug/l
91-20-3 Naphthalene 4.2 0.50 0.10 ug/l
103-65-1 n-Propylbenzene 1.0 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene 0.10 0.50 0.10 ug/l J
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene 0.15 0.50 0.10 ug/l J
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)1.3 1.5 0.20 ug/l J
m,p-Xylene 0.23 1.0 0.10 ug/l J
95-47-6 o-Xylene 1.1 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 105%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
2037-26-5 Toluene-D8 95%70-130%
460-00-4 4-Bromofluorobenzene 96%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
23 of 55
FA18806 33.7
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-17
Lab Sample ID:FA18806-8 Date Sampled:09/30/14
Matrix:AQ - Ground Water Date Received:10/01/14
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E033710.D 1 10/06/14 EG n/a n/a VE1124
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
24 of 55
FA18806 33.8
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-17
Lab Sample ID:FA18806-8 Date Sampled:09/30/14
Matrix:AQ - Ground Water Date Received:10/01/14
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride 0.14 0.50 0.10 ug/l J
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 107%70-130%
17060-07-0 1,2-Dichloroethane-D4 105%70-130%
2037-26-5 Toluene-D8 94%70-130%
460-00-4 4-Bromofluorobenzene 96%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
25 of 55
FA18806 33.8
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-18
Lab Sample ID:FA18806-9 Date Sampled:09/30/14
Matrix:AQ - Ground Water Date Received:10/01/14
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E033711.D 1 10/06/14 EG n/a n/a VE1124
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
26 of 55
FA18806 33.9
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-18
Lab Sample ID:FA18806-9 Date Sampled:09/30/14
Matrix:AQ - Ground Water Date Received:10/01/14
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride 0.15 0.50 0.10 ug/l J
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 110%70-130%
17060-07-0 1,2-Dichloroethane-D4 111%70-130%
2037-26-5 Toluene-D8 95%70-130%
460-00-4 4-Bromofluorobenzene 96%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
27 of 55
FA18806 33.9
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:WSW-2
Lab Sample ID:FA18806-10 Date Sampled:09/30/14
Matrix:AQ - Ground Water Date Received:10/01/14
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E033712.D 1 10/06/14 EG n/a n/a VE1124
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
28 of 55
FA18806 33.10
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:WSW-2
Lab Sample ID:FA18806-10 Date Sampled:09/30/14
Matrix:AQ - Ground Water Date Received:10/01/14
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 111%70-130%
17060-07-0 1,2-Dichloroethane-D4 112%70-130%
2037-26-5 Toluene-D8 93%70-130%
460-00-4 4-Bromofluorobenzene 95%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
29 of 55
FA18806 33.10
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:WSW-6
Lab Sample ID:FA18806-11 Date Sampled:09/30/14
Matrix:AQ - Ground Water Date Received:10/01/14
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E033713.D 1 10/06/14 EG n/a n/a VE1124
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
30 of 55
FA18806 33.11
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:WSW-6
Lab Sample ID:FA18806-11 Date Sampled:09/30/14
Matrix:AQ - Ground Water Date Received:10/01/14
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride 0.22 0.50 0.10 ug/l J
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 115%70-130%
17060-07-0 1,2-Dichloroethane-D4 114%70-130%
2037-26-5 Toluene-D8 91%70-130%
460-00-4 4-Bromofluorobenzene 95%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
31 of 55
FA18806 33.11
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:WSW-7
Lab Sample ID:FA18806-12 Date Sampled:09/30/14
Matrix:AQ - Ground Water Date Received:10/01/14
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E033714.D 1 10/06/14 EG n/a n/a VE1124
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
32 of 55
FA18806 33.12
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:WSW-7
Lab Sample ID:FA18806-12 Date Sampled:09/30/14
Matrix:AQ - Ground Water Date Received:10/01/14
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride 0.19 0.50 0.10 ug/l J
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene 0.22 0.50 0.10 ug/l J
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 113%70-130%
17060-07-0 1,2-Dichloroethane-D4 114%70-130%
2037-26-5 Toluene-D8 94%70-130%
460-00-4 4-Bromofluorobenzene 95%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
33 of 55
FA18806 33.12
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:WSW-8
Lab Sample ID:FA18806-13 Date Sampled:09/30/14
Matrix:AQ - Ground Water Date Received:10/01/14
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E033715.D 1 10/06/14 EG n/a n/a VE1124
Run #2 a E033730.D 1 10/07/14 EG n/a n/a VE1125
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
34 of 55
FA18806 33.13
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:WSW-8
Lab Sample ID:FA18806-13 Date Sampled:09/30/14
Matrix:AQ - Ground Water Date Received:10/01/14
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride 0.14 0.50 0.10 ug/l J
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 115%114%70-130%
17060-07-0 1,2-Dichloroethane-D4 116%114%70-130%
2037-26-5 Toluene-D8 94%93%70-130%
460-00-4 4-Bromofluorobenzene 94%97%70-130%
(a) Confirmation run for internal standard areas.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
35 of 55
FA18806 33.13
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:WSW-41
Lab Sample ID:FA18806-14 Date Sampled:09/30/14
Matrix:AQ - Ground Water Date Received:10/01/14
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0189966.D 1 10/08/14 EG n/a n/a VA1564
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
36 of 55
FA18806 33.14
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:WSW-41
Lab Sample ID:FA18806-14 Date Sampled:09/30/14
Matrix:AQ - Ground Water Date Received:10/01/14
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride 0.27 0.50 0.10 ug/l J
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene 0.30 0.50 0.10 ug/l J
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 107%70-130%
17060-07-0 1,2-Dichloroethane-D4 108%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 104%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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FA18806 33.14
Accutest Laboratories
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Southeast
Section 4
38 of 55
FA18806 4
FA18806: Chain of Custody
Page 1 of 4
39 of 55
FA18806 44.1
FA18806: Chain of Custody
Page 2 of 4
40 of 55
FA18806 44.1
FA18806: Chain of Custody
Page 3 of 4
41 of 55
FA18806 44.1
FA18806: Chain of Custody
Page 4 of 4
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FA18806 44.1
Accutest Laboratories
GC/MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Southeast
Section 5
43 of 55
FA18806 5
Method Blank Summary Page 1 of 2
Job Number:FA18806
Account:GRINCC GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1124-MB E033695.D 1 10/06/14 EG n/a n/a VE1124
The QC reported here applies to the following samples:Method: SM 6200B
FA18806-1, FA18806-2, FA18806-3, FA18806-4, FA18806-5, FA18806-6, FA18806-7, FA18806-8, FA18806-9,
FA18806-10, FA18806-11, FA18806-12, FA18806-13
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
44 of 55
FA18806 55.1.1
Method Blank Summary Page 2 of 2
Job Number:FA18806
Account:GRINCC GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1124-MB E033695.D 1 10/06/14 EG n/a n/a VE1124
The QC reported here applies to the following samples:Method: SM 6200B
FA18806-1, FA18806-2, FA18806-3, FA18806-4, FA18806-5, FA18806-6, FA18806-7, FA18806-8, FA18806-9,
FA18806-10, FA18806-11, FA18806-12, FA18806-13
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
45 of 55
FA18806 55.1.1
Method Blank Summary Page 1 of 2
Job Number:FA18806
Account:GRINCC GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1564-MB A0189963.D 1 10/08/14 EG n/a n/a VA1564
The QC reported here applies to the following samples:Method: SM 6200B
FA18806-14
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
46 of 55
FA18806 55.1.2
Method Blank Summary Page 2 of 2
Job Number:FA18806
Account:GRINCC GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1564-MB A0189963.D 1 10/08/14 EG n/a n/a VA1564
The QC reported here applies to the following samples:Method: SM 6200B
FA18806-14
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 98%70-130%
17060-07-0 1,2-Dichloroethane-D4 99%70-130%
2037-26-5 Toluene-D8 102%70-130%
460-00-4 4-Bromofluorobenzene 104%70-130%
47 of 55
FA18806 55.1.2
Blank Spike Summary Page 1 of 2
Job Number:FA18806
Account:GRINCC GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1124-BS E033693.D 1 10/06/14 EG n/a n/a VE1124
The QC reported here applies to the following samples:Method: SM 6200B
FA18806-1, FA18806-2, FA18806-3, FA18806-4, FA18806-5, FA18806-6, FA18806-7, FA18806-8, FA18806-9,
FA18806-10, FA18806-11, FA18806-12, FA18806-13
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 10.9 109 70-130
108-86-1 Bromobenzene 10 11.6 116 70-130
74-97-5 Bromochloromethane 10 11.9 119 70-130
75-27-4 Bromodichloromethane 10 11.8 118 70-130
75-25-2 Bromoform 10 11.8 118 70-130
104-51-8 n-Butylbenzene 10 10.9 109 70-130
135-98-8 sec-Butylbenzene 10 12.4 124 70-130
98-06-6 tert-Butylbenzene 10 12.4 124 70-130
108-90-7 Chlorobenzene 10 11.9 119 70-130
75-00-3 Chloroethane 10 12.4 124 60-140
67-66-3 Chloroform 10 11.5 115 70-130
95-49-8 o-Chlorotoluene 10 11.8 118 70-130
106-43-4 p-Chlorotoluene 10 12.0 120 70-130
56-23-5 Carbon tetrachloride 10 12.8 128 70-130
75-34-3 1,1-Dichloroethane 10 10.9 109 70-130
75-35-4 1,1-Dichloroethylene 10 12.1 121 70-130
563-58-6 1,1-Dichloropropene 10 12.0 120 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 9.9 99 70-130
106-93-4 1,2-Dibromoethane 10 11.0 110 70-130
107-06-2 1,2-Dichloroethane 10 11.6 116 70-130
78-87-5 1,2-Dichloropropane 10 10.2 102 70-130
142-28-9 1,3-Dichloropropane 10 10.1 101 70-130
108-20-3 Di-Isopropyl ether 10 9.6 96 70-130
594-20-7 2,2-Dichloropropane 10 12.5 125 70-130
124-48-1 Dibromochloromethane 10 11.6 116 70-130
75-71-8 Dichlorodifluoromethane 10 10.7 107 60-140
156-59-2 cis-1,2-Dichloroethylene 10 11.2 112 70-130
10061-01-5 cis-1,3-Dichloropropene 10 10.8 108 70-130
541-73-1 m-Dichlorobenzene 10 12.6 126 70-130
95-50-1 o-Dichlorobenzene 10 12.4 124 70-130
106-46-7 p-Dichlorobenzene 10 11.5 115 70-130
156-60-5 trans-1,2-Dichloroethylene 10 11.0 110 70-130
10061-02-6 trans-1,3-Dichloropropene 10 11.5 115 70-130
100-41-4 Ethylbenzene 10 11.0 110 70-130
87-68-3 Hexachlorobutadiene 10 13.5 135*70-130
98-82-8 Isopropylbenzene 10 12.8 128 70-130
* = Outside of Control Limits.
48 of 55
FA18806 55.2.1
Blank Spike Summary Page 2 of 2
Job Number:FA18806
Account:GRINCC GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1124-BS E033693.D 1 10/06/14 EG n/a n/a VE1124
The QC reported here applies to the following samples:Method: SM 6200B
FA18806-1, FA18806-2, FA18806-3, FA18806-4, FA18806-5, FA18806-6, FA18806-7, FA18806-8, FA18806-9,
FA18806-10, FA18806-11, FA18806-12, FA18806-13
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 12.6 126 70-130
74-83-9 Methyl bromide 10 13.6 136 60-140
74-87-3 Methyl chloride 10 9.6 96 60-140
74-95-3 Methylene bromide 10 11.3 113 70-130
75-09-2 Methylene chloride 10 9.3 93 70-130
1634-04-4 Methyl Tert Butyl Ether 10 10.9 109 70-130
91-20-3 Naphthalene 10 10.9 109 70-130
103-65-1 n-Propylbenzene 10 12.0 120 70-130
100-42-5 Styrene 10 11.4 114 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 11.9 119 70-130
71-55-6 1,1,1-Trichloroethane 10 12.6 126 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 9.6 96 70-130
79-00-5 1,1,2-Trichloroethane 10 10.2 102 70-130
87-61-6 1,2,3-Trichlorobenzene 10 11.8 118 70-130
96-18-4 1,2,3-Trichloropropane 10 11.1 111 70-130
120-82-1 1,2,4-Trichlorobenzene 10 11.8 118 70-130
95-63-6 1,2,4-Trimethylbenzene 10 11.5 115 70-130
108-67-8 1,3,5-Trimethylbenzene 10 11.3 113 70-130
127-18-4 Tetrachloroethylene 10 12.4 124 70-130
108-88-3 Toluene 10 10.4 104 70-130
79-01-6 Trichloroethylene 10 11.8 118 70-130
75-69-4 Trichlorofluoromethane 10 12.9 129 60-140
75-01-4 Vinyl chloride 10 11.4 114 60-140
1330-20-7 Xylene (total)30 35.7 119 70-130
m,p-Xylene 20 23.7 119 70-130
95-47-6 o-Xylene 10 12.1 121 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 107%70-130%
17060-07-0 1,2-Dichloroethane-D4 109%70-130%
2037-26-5 Toluene-D8 95%70-130%
460-00-4 4-Bromofluorobenzene 93%70-130%
* = Outside of Control Limits.
49 of 55
FA18806 55.2.1
Blank Spike Summary Page 1 of 2
Job Number:FA18806
Account:GRINCC GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1564-BS A0189961.D 1 10/08/14 EG n/a n/a VA1564
The QC reported here applies to the following samples:Method: SM 6200B
FA18806-14
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 10.1 101 70-130
108-86-1 Bromobenzene 10 9.9 99 70-130
74-97-5 Bromochloromethane 10 10.0 100 70-130
75-27-4 Bromodichloromethane 10 10.1 101 70-130
75-25-2 Bromoform 10 9.1 91 70-130
104-51-8 n-Butylbenzene 10 10.5 105 70-130
135-98-8 sec-Butylbenzene 10 11.8 118 70-130
98-06-6 tert-Butylbenzene 10 11.7 117 70-130
108-90-7 Chlorobenzene 10 10.4 104 70-130
75-00-3 Chloroethane 10 10.9 109 60-140
67-66-3 Chloroform 10 9.2 92 70-130
95-49-8 o-Chlorotoluene 10 10.8 108 70-130
106-43-4 p-Chlorotoluene 10 11.3 113 70-130
56-23-5 Carbon tetrachloride 10 10.7 107 70-130
75-34-3 1,1-Dichloroethane 10 10.0 100 70-130
75-35-4 1,1-Dichloroethylene 10 10.8 108 70-130
563-58-6 1,1-Dichloropropene 10 11.2 112 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 8.6 86 70-130
106-93-4 1,2-Dibromoethane 10 9.8 98 70-130
107-06-2 1,2-Dichloroethane 10 9.9 99 70-130
78-87-5 1,2-Dichloropropane 10 9.8 98 70-130
142-28-9 1,3-Dichloropropane 10 9.6 96 70-130
108-20-3 Di-Isopropyl ether 10 10.1 101 70-130
594-20-7 2,2-Dichloropropane 10 11.2 112 70-130
124-48-1 Dibromochloromethane 10 9.9 99 70-130
75-71-8 Dichlorodifluoromethane 10 11.2 112 60-140
156-59-2 cis-1,2-Dichloroethylene 10 10 100 70-130
10061-01-5 cis-1,3-Dichloropropene 10 10.1 101 70-130
541-73-1 m-Dichlorobenzene 10 10.9 109 70-130
95-50-1 o-Dichlorobenzene 10 10.4 104 70-130
106-46-7 p-Dichlorobenzene 10 9.6 96 70-130
156-60-5 trans-1,2-Dichloroethylene 10 10 100 70-130
10061-02-6 trans-1,3-Dichloropropene 10 10.9 109 70-130
100-41-4 Ethylbenzene 10 10.2 102 70-130
87-68-3 Hexachlorobutadiene 10 10.5 105 70-130
98-82-8 Isopropylbenzene 10 11.7 117 70-130
* = Outside of Control Limits.
50 of 55
FA18806 55.2.2
Blank Spike Summary Page 2 of 2
Job Number:FA18806
Account:GRINCC GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1564-BS A0189961.D 1 10/08/14 EG n/a n/a VA1564
The QC reported here applies to the following samples:Method: SM 6200B
FA18806-14
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 11.7 117 70-130
74-83-9 Methyl bromide 10 10.6 106 60-140
74-87-3 Methyl chloride 10 10.7 107 60-140
74-95-3 Methylene bromide 10 9.9 99 70-130
75-09-2 Methylene chloride 10 9.3 93 70-130
1634-04-4 Methyl Tert Butyl Ether 10 9.9 99 70-130
91-20-3 Naphthalene 10 9.4 94 70-130
103-65-1 n-Propylbenzene 10 11.3 113 70-130
100-42-5 Styrene 10 10.5 105 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 10.0 100 70-130
71-55-6 1,1,1-Trichloroethane 10 10.6 106 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 9.4 94 70-130
79-00-5 1,1,2-Trichloroethane 10 9.5 95 70-130
87-61-6 1,2,3-Trichlorobenzene 10 9.5 95 70-130
96-18-4 1,2,3-Trichloropropane 10 9.3 93 70-130
120-82-1 1,2,4-Trichlorobenzene 10 9.8 98 70-130
95-63-6 1,2,4-Trimethylbenzene 10 10.5 105 70-130
108-67-8 1,3,5-Trimethylbenzene 10 10.4 104 70-130
127-18-4 Tetrachloroethylene 10 10.4 104 70-130
108-88-3 Toluene 10 9.9 99 70-130
79-01-6 Trichloroethylene 10 10 100 70-130
75-69-4 Trichlorofluoromethane 10 11.5 115 60-140
75-01-4 Vinyl chloride 10 11.5 115 60-140
1330-20-7 Xylene (total)30 32.8 109 70-130
m,p-Xylene 20 21.6 108 70-130
95-47-6 o-Xylene 10 11.2 112 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
* = Outside of Control Limits.
51 of 55
FA18806 55.2.2
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA18806
Account:GRINCC GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA18669-7MS E033705.D 20 10/06/14 EG n/a n/a VE1124
FA18669-7MSD E033706.D 20 10/06/14 EG n/a n/a VE1124
FA18669-7 a E033696.D 20 10/06/14 EG n/a n/a VE1124
The QC reported here applies to the following samples:Method: SM 6200B
FA18806-1, FA18806-2, FA18806-3, FA18806-4, FA18806-5, FA18806-6, FA18806-7, FA18806-8, FA18806-9,
FA18806-10, FA18806-11, FA18806-12, FA18806-13
FA18669-7 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 16.3 200 231 107 200 230 107 0 70-130/20
108-86-1 Bromobenzene ND 200 229 115 200 229 115 0 70-130/20
74-97-5 Bromochloromethane ND 200 244 122 200 238 119 2 70-130/20
75-27-4 Bromodichloromethane ND 200 236 118 200 215 108 9 70-130/20
75-25-2 Bromoform ND 200 185 93 200 182 91 2 70-130/20
104-51-8 n-Butylbenzene 5.2 J 200 227 111 200 226 110 0 70-130/20
135-98-8 sec-Butylbenzene 2.7 J 200 250 124 200 251 124 0 70-130/20
98-06-6 tert-Butylbenzene ND 200 253 127 200 255 128 1 70-130/20
108-90-7 Chlorobenzene ND 200 238 119 200 237 119 0 70-130/20
75-00-3 Chloroethane ND 200 236 118 200 238 119 1 60-140/20
67-66-3 Chloroform ND 200 242 121 200 232 116 4 70-130/20
95-49-8 o-Chlorotoluene ND 200 247 124 200 248 124 0 70-130/20
106-43-4 p-Chlorotoluene ND 200 235 118 200 236 118 0 70-130/20
56-23-5 Carbon tetrachloride ND 200 280 140*200 249 125 12 70-130/20
75-34-3 1,1-Dichloroethane ND 200 221 111 200 218 109 1 70-130/20
75-35-4 1,1-Dichloroethylene ND 200 254 127 200 249 125 2 70-130/20
563-58-6 1,1-Dichloropropene ND 200 252 126 200 246 123 2 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 200 200 100 200 214 107 7 70-130/20
106-93-4 1,2-Dibromoethane ND 200 217 109 200 223 112 3 70-130/20
107-06-2 1,2-Dichloroethane ND 200 249 125 200 240 120 4 70-130/20
78-87-5 1,2-Dichloropropane ND 200 200 100 200 202 101 1 70-130/20
142-28-9 1,3-Dichloropropane ND 200 203 102 200 203 102 0 70-130/20
108-20-3 Di-Isopropyl ether ND 200 189 95 200 191 96 1 70-130/20
594-20-7 2,2-Dichloropropane ND 200 273 137*200 265 133*3 70-130/20
124-48-1 Dibromochloromethane ND 200 201 101 200 192 96 5 70-130/20
75-71-8 Dichlorodifluoromethane ND 200 242 121 200 231 116 5 60-140/20
156-59-2 cis-1,2-Dichloroethylene ND 200 223 112 200 225 113 1 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 200 205 103 200 186 93 10 70-130/20
541-73-1 m-Dichlorobenzene ND 200 249 125 200 248 124 0 70-130/20
95-50-1 o-Dichlorobenzene ND 200 247 124 200 248 124 0 70-130/20
106-46-7 p-Dichlorobenzene ND 200 227 114 200 225 113 1 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 200 225 113 200 219 110 3 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 200 219 110 200 207 104 6 70-130/20
100-41-4 Ethylbenzene 54.5 200 277 111 200 276 111 0 70-130/20
87-68-3 Hexachlorobutadiene ND 200 276 138*200 277 139*0 70-130/20
98-82-8 Isopropylbenzene 10.2 200 271 130 200 270 130 0 70-130/20
* = Outside of Control Limits.
52 of 55
FA18806 55.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA18806
Account:GRINCC GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA18669-7MS E033705.D 20 10/06/14 EG n/a n/a VE1124
FA18669-7MSD E033706.D 20 10/06/14 EG n/a n/a VE1124
FA18669-7 a E033696.D 20 10/06/14 EG n/a n/a VE1124
The QC reported here applies to the following samples:Method: SM 6200B
FA18806-1, FA18806-2, FA18806-3, FA18806-4, FA18806-5, FA18806-6, FA18806-7, FA18806-8, FA18806-9,
FA18806-10, FA18806-11, FA18806-12, FA18806-13
FA18669-7 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene 2.1 J 200 256 127 200 256 127 0 70-130/20
74-83-9 Methyl bromide ND 200 267 134 200 265 133 1 60-140/20
74-87-3 Methyl chloride ND 200 187 94 200 189 95 1 60-140/20
74-95-3 Methylene bromide ND 200 241 121 200 233 117 3 70-130/20
75-09-2 Methylene chloride ND 200 191 96 200 190 95 1 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 200 218 109 200 222 111 2 70-130/20
91-20-3 Naphthalene 66.8 200 287 110 200 305 119 6 70-130/20
103-65-1 n-Propylbenzene 31.7 200 268 118 200 269 119 0 70-130/20
100-42-5 Styrene 2.4 J 200 228 113 200 230 114 1 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 200 242 121 200 237 119 2 70-130/20
71-55-6 1,1,1-Trichloroethane ND 200 274 137*200 266 133*3 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 200 187 94 200 197 99 5 70-130/20
79-00-5 1,1,2-Trichloroethane ND 200 200 100 200 202 101 1 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 200 230 115 200 242 121 5 70-130/20
96-18-4 1,2,3-Trichloropropane ND 200 217 109 200 223 112 3 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 200 238 119 200 246 123 3 70-130/20
95-63-6 1,2,4-Trimethylbenzene 478 200 677 100 200 674 98 0 70-130/20
108-67-8 1,3,5-Trimethylbenzene 116 200 336 110 200 338 111 1 70-130/20
127-18-4 Tetrachloroethylene ND 200 256 128 200 250 125 2 70-130/20
108-88-3 Toluene 51.7 200 253 101 200 258 103 2 70-130/20
79-01-6 Trichloroethylene ND 200 242 121 200 232 116 4 70-130/20
75-69-4 Trichlorofluoromethane ND 200 294 147*200 275 138 7 60-140/20
75-01-4 Vinyl chloride ND 200 217 109 200 226 113 4 60-140/20
1330-20-7 Xylene (total)494 600 1210 119 600 1200 118 1 70-130/20
m,p-Xylene 346 400 811 116 400 803 114 1 70-130/20
95-47-6 o-Xylene 148 200 398 125 200 398 125 0 70-130/20
CAS No.Surrogate Recoveries MS MSD FA18669-7 Limits
1868-53-7 Dibromofluoromethane 113%108%108%70-130%
17060-07-0 1,2-Dichloroethane-D4 118%112%109%70-130%
2037-26-5 Toluene-D8 93%93%95%70-130%
460-00-4 4-Bromofluorobenzene 91%94%94%70-130%
(a) Sample vial(s) contained significant headspace; reported results are considered minimum values.
* = Outside of Control Limits.
53 of 55
FA18806 55.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA18806
Account:GRINCC GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA18807-2MS A0189972.D 5 10/08/14 EG n/a n/a VA1564
FA18807-2MSD A0189973.D 5 10/08/14 EG n/a n/a VA1564
FA18807-2 A0189968.D 5 10/08/14 EG n/a n/a VA1564
The QC reported here applies to the following samples:Method: SM 6200B
FA18806-14
FA18807-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 3.2 50 51.7 97 50 50.9 95 2 70-130/20
108-86-1 Bromobenzene ND 50 46.2 92 50 46.3 93 0 70-130/20
74-97-5 Bromochloromethane ND 50 50.5 101 50 48.6 97 4 70-130/20
75-27-4 Bromodichloromethane ND 50 49.0 98 50 45.1 90 8 70-130/20
75-25-2 Bromoform ND 50 34.6 69*50 35.4 71 2 70-130/20
104-51-8 n-Butylbenzene 2.2 J 50 54.4 104 50 53.4 102 2 70-130/20
135-98-8 sec-Butylbenzene 2.8 50 58.7 112 50 58.6 112 0 70-130/20
98-06-6 tert-Butylbenzene ND 50 55.9 112 50 55.5 111 1 70-130/20
108-90-7 Chlorobenzene ND 50 50.4 101 50 50.5 101 0 70-130/20
75-00-3 Chloroethane ND 50 51.6 103 50 53.0 106 3 60-140/20
67-66-3 Chloroform ND 50 47.5 95 50 45.4 91 5 70-130/20
95-49-8 o-Chlorotoluene ND 50 51.7 103 50 51.1 102 1 70-130/20
106-43-4 p-Chlorotoluene ND 50 52.3 105 50 52.2 104 0 70-130/20
56-23-5 Carbon tetrachloride ND 50 53.9 108 50 48.9 98 10 70-130/20
75-34-3 1,1-Dichloroethane ND 50 50.8 102 50 49.8 100 2 70-130/20
75-35-4 1,1-Dichloroethylene ND 50 54.3 109 50 52.8 106 3 70-130/20
563-58-6 1,1-Dichloropropene ND 50 54.5 109 50 52.3 105 4 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 50 47.0 94 50 45.6 91 3 70-130/20
106-93-4 1,2-Dibromoethane ND 50 46.7 93 50 47.2 94 1 70-130/20
107-06-2 1,2-Dichloroethane ND 50 51.8 104 50 49.4 99 5 70-130/20
78-87-5 1,2-Dichloropropane ND 50 47.7 95 50 47.9 96 0 70-130/20
142-28-9 1,3-Dichloropropane ND 50 46.1 92 50 46.5 93 1 70-130/20
108-20-3 Di-Isopropyl ether ND 50 49.3 99 50 49.1 98 0 70-130/20
594-20-7 2,2-Dichloropropane ND 50 54.8 110 50 52.4 105 4 70-130/20
124-48-1 Dibromochloromethane ND 50 40.9 82 50 40.9 82 0 70-130/20
75-71-8 Dichlorodifluoromethane ND 50 53.8 108 50 52.7 105 2 60-140/20
156-59-2 cis-1,2-Dichloroethylene ND 50 48.9 98 50 48.3 97 1 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 50 44.7 89 50 40.8 82 9 70-130/20
541-73-1 m-Dichlorobenzene ND 50 51.1 102 50 51.0 102 0 70-130/20
95-50-1 o-Dichlorobenzene ND 50 50.3 101 50 50.0 100 1 70-130/20
106-46-7 p-Dichlorobenzene ND 50 45.6 91 50 45.6 91 0 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 50 50.7 101 50 48.5 97 4 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 50 50.9 102 50 47.8 96 6 70-130/20
100-41-4 Ethylbenzene 157 50 194 74 50 193 72 1 70-130/20
87-68-3 Hexachlorobutadiene ND 50 53.5 107 50 52.6 105 2 70-130/20
98-82-8 Isopropylbenzene 23.3 50 82.2 118 50 81.0 115 1 70-130/20
* = Outside of Control Limits.
54 of 55
FA18806 55.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA18806
Account:GRINCC GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA18807-2MS A0189972.D 5 10/08/14 EG n/a n/a VA1564
FA18807-2MSD A0189973.D 5 10/08/14 EG n/a n/a VA1564
FA18807-2 A0189968.D 5 10/08/14 EG n/a n/a VA1564
The QC reported here applies to the following samples:Method: SM 6200B
FA18806-14
FA18807-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 50 54.4 109 50 54.8 110 1 70-130/20
74-83-9 Methyl bromide ND 50 51.1 102 50 51.7 103 1 60-140/20
74-87-3 Methyl chloride ND 50 46.2 92 50 50.6 101 9 60-140/20
74-95-3 Methylene bromide ND 50 50.9 102 50 47.9 96 6 70-130/20
75-09-2 Methylene chloride ND 50 49.5 99 50 47.5 95 4 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 50 49.0 98 50 48.9 98 0 70-130/20
91-20-3 Naphthalene 3.5 50 52.6 98 50 53.4 100 2 70-130/20
103-65-1 n-Propylbenzene 51.5 50 96.7 90 50 97.3 92 1 70-130/20
100-42-5 Styrene ND 50 47.9 96 50 48.4 97 1 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 50 49.0 98 50 47.4 95 3 70-130/20
71-55-6 1,1,1-Trichloroethane ND 50 53.6 107 50 50.7 101 6 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 50 44.3 89 50 44.9 90 1 70-130/20
79-00-5 1,1,2-Trichloroethane ND 50 46.1 92 50 46.5 93 1 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 50 48.7 97 50 49.4 99 1 70-130/20
96-18-4 1,2,3-Trichloropropane ND 50 45.6 91 50 45.6 91 0 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 50 51.4 103 50 51.7 103 1 70-130/20
95-63-6 1,2,4-Trimethylbenzene 2.4 J 50 53.2 102 50 53.0 101 0 70-130/20
108-67-8 1,3,5-Trimethylbenzene ND 50 48.5 97 50 48.3 97 0 70-130/20
127-18-4 Tetrachloroethylene ND 50 50.3 101 50 49.5 99 2 70-130/20
108-88-3 Toluene 1.1 J 50 46.8 91 50 47.6 93 2 70-130/20
79-01-6 Trichloroethylene ND 50 49.8 100 50 48.1 96 3 70-130/20
75-69-4 Trichlorofluoromethane ND 50 57.8 116 50 53.5 107 8 60-140/20
75-01-4 Vinyl chloride ND 50 48.7 97 50 53.8 108 10 60-140/20
1330-20-7 Xylene (total)3.6 J 150 160 104 150 160 104 0 70-130/20
m,p-Xylene 2.4 J 100 105 103 100 104 102 1 70-130/20
95-47-6 o-Xylene 1.2 J 50 54.5 107 50 55.5 109 2 70-130/20
CAS No.Surrogate Recoveries MS MSD FA18807-2 Limits
1868-53-7 Dibromofluoromethane 109%105%111%70-130%
17060-07-0 1,2-Dichloroethane-D4 115%106%110%70-130%
2037-26-5 Toluene-D8 95%98%97%70-130%
460-00-4 4-Bromofluorobenzene 98%99%103%70-130%
* = Outside of Control Limits.
55 of 55
FA18806 55.3.2