The URL can be used to link to this page

Home My WebLink AboutWA-706_10000_CA_HRE_20060425 3502 Hayes Road • Monroe, North Carolina 28110 113 West Firetower Road, Suite G • Winterville, North Carolina 28590 Phone (704) 845-4010 • (888) 870-4133 • Fax (704) 845-4012 February 13, 2023 Ms. Allison Ward North Carolina Department of Environmental Quality Washington Regional Office 943 Washington Square Mall Washington, North Carolina 27889 Re: Ground Water Monitoring Report January 2023 Peele’s Service Station 2675 Old US Highway 64 Jamesville, Martin County North Carolina Facility ID Number: 0-00-000013895 Incident Number: 10000 GRI Project Number: 2516 Dear Ms. Ward, Please find enclosed the referenced report for the abovementioned site. If you have any questions, please contact Ethan Rogerson at 704-845-4010. Sincerely, Geological Resources, Inc. Leslie Maxtone-Graham Administrative Assistant Enclosure Cc: North East Oil Company, Inc., file 3502 Hayes Road • Monroe, North Carolina 28110 113 West Firetower Road, Suite G • Winterville, North Carolina 28590 Phone (704) 845-4010 • (888) 870-4133 • Fax (704) 845-4012 Engineering Certification: C-2727 • Geology Certification: C-127 Ground Water Monitoring Report January 2023 Peele’s Service Station 2675 Old US Highway 64 Jamesville, Martin County North Carolina Facility ID Number: 0-00-0000013895 Incident Number: 10000 GRI Project Number: 2516 Prepared for: North East Oil Company, Inc. Post Office Box 1386 Ahoskie, North Carolina 27910 February 13, 2023 Ethan Rogerson, G.I.T. Project Manager Colton Coolbaugh Report Writer ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: February 13, 2023 Peele’s Service Station Project Manager: Ethan Rogerson, G.I.T. GRI Project No. 2516 i SITE INFORMATION 1. Site Identification  Peele’s Service Station (Facility ID 0-00-0000013895)  Incident Number 10000 – High Risk (H285R)  Location of Source Area: 2675 Old US Highway 64 Jamesville, NC 28677 Martin County 35.8222805°N, 76.8156861°W (Topographical Map) 2. Information about Contacts Associated with the Leaking UST System UST Owner North East Oil Company, Inc. Post Office Box 1386 Ahoskie, NC 27910 beah@bent-prises.com 252-398-6022 UST Operator North East Oil Company, Inc. Post Office Box 1386 Ahoskie, NC 27910 beah@bent-prises.com 252-398-6022 Property Owner Tyese La Starr Jordan 3201 Piney Woods Road Jamesville, NC 27846 Email Unknown Phone No. Unknown Property Occupant Tyese La Starr Jordan 3201 Piney Woods Road Jamesville, NC 27846 Email Unknown Phone No. Unknown Consultant/Contractor Geological Resources, Inc. 3502 Hayes Road Monroe, NC 28110 egr@geologicalresourcesinc.com 704-845-4010 Analytical Laboratory SGS North America, Inc. 4405 Vineland Road, Suite C-15 Orlando, FL 32811 State Certification No. 573 407-425-6700 3. Information about Release  Release was discovered in September 1992  An unknown amount of product was released from the leaking UST System  One 1,000-gallon gasoline and one 550-gallon gasoline USTs were removed from the site in September 1992. ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: February 13, 2023 Peele’s Service Station Project Manager: Ethan Rogerson, G.I.T. GRI Project No. 2516 ii EXECUTIVE SUMMARY Peele’s Service Station is located at 2675 Old US Highway 64 in Jamesville, Martin County, North Carolina. The site is currently a residential property owned by Tyese La Starr Jordan. According to available information, a petroleum release at the site was confirmed subsequent to the removal of one 1,000-gallon and one 550-gallon gasoline USTs in September 1992. The adjoining properties are residential properties. The site risk classification is currently ranked as high risk due to forty-seven potable water supply wells being located within a 1,000-foot radius of the site. Receptor information was updated for the site on March 4, 2021. Forty-five potable water supply wells were observed within a 1,000-foot radius of the site. No surface water bodies were identified within a 500-foot radius of the site. The site does not lie within a designated wellhead protection area. On January 11, 2023, fourteen monitoring wells were gauged, purged and/or sampled. Please note, monitoring wells MW-8, MW-10, MW-12, MW-13 and MW-16 were not located; MW-2, MW-3, MW-4, MW-6, MW-7 and MW-14 were dry and were not sampled. Concentrations of benzene, xylenes and/or naphthalene that exceeded the MACs were reported in the ground water samples collected from MW-1, MW-2R and MW-11. All of the reported contaminant concentrations were less than the GCLs. Contaminant mass at the site has decreased by 81.7% between April 2015 and January 2023. Free product has not been observed at the site since 2014. The Contaminant Fate & Transport model proposed for the January 2023 sampling event could not be completed due to the drop in water level and subsequent dry monitoring wells. Based on this information, the risk classification for the site should remain high risk. Quarterly sampling should be conducted on MW-1, MW-2R, MW-11, MW-14 and MW-18 until the water table is high enough to collect sufficient data for a Contaminant Fate & Transport model. If the model results are favorable, the incident may close with the filing of a NRP on the deed of the subject property. The next sampling event is tentatively scheduled for April 2023 and should include a comprehensive sampling event to satisfy model requirements. ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: February 13, 2023 Peele’s Service Station Project Manager: Ethan Rogerson, G.I.T. GRI Project No. 2516 iii ACRONYMS ACM: Asbestos Containing Materials AFVR: Aggressive Fluid-Vapor Recovery ARR: Acknowledgement of Report Receipt AS: Air Sparging AST: Aboveground Storage Tank ASTM: American Society for Testing and Materials BGS: Below Ground Surface CAP: Corrective Action Plan CFR: Code of Federal Regulations CSA: Comprehensive Site Assessment DPE: Dual Phase Extraction DRO: Total Petroleum Hydrocarbons Diesel Range Organics DWM: Division of Waste Management DWR: Department of Water Resources EPA: Environmental Protection Agency EPH: Extractible Petroleum Hydrocarbons ESA: Environmental Site Assessment GCL: Gross Contamination Level GRI: Geological Resources, Inc. GRO: Total Petroleum Hydrocarbons Gasoline Range Organics LSA: Limited Site Assessment MAC: Maximum Allowable Concentration as specified in T15A NCAC 2L.0202 MADEP: Massachusetts Department of Environmental Protection MCC: Maximum Contaminant Concentrations MMPE: Mobile Multi-Phase Extraction NAPL: Non-Aqueous Phase Liquid, “Free Product” NCDEQ: North Carolina Department of Environmental Quality NCDOT: North Carolina Department of Transportation NFA: Notice of No Further Action NORR: Notice of Regulatory Requirements NOV: Notice of Violation NPDES: National Pollutant Discharge Elimination System NRP: Notice of Residual Petroleum O&M: Operation and Maintenance PAHs: Polynuclear Aromatic Hydrocarbons PCA: Pre-Construction Assessment RAL: Regulatory Action Level SCLs: Soil Cleanup Level SPCC: Spill Prevention Control and Countermeasures SVE: Soil Vapor Extraction SVOCs: Semi-Volatile Organic Compounds SWPPP: Stormwater Pollution Prevention Plan TCLP: Toxicity Characteristic Leaching Procedure (EPA Method SW-846 1311) TOC: Top of Casing TPH: Total Petroleum Hydrocarbons USGS: United States Geological Survey UST: Underground Storage Tank UVF: Ultraviolet Fluorescence VOCs: Volatile Organic Compounds VPH: Volatile Petroleum Hydrocarbons ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: February 13, 2023 Peele’s Service Station Project Manager: Ethan Rogerson, G.I.T. GRI Project No. 2516 TABLE OF CONTENTS SITE INFORMATION ............................................................................................................................ i EXECUTIVE SUMMARY ....................................................................................................................... ii ACRONYMS ....................................................................................................................................... iii 1.0 SITE HISTORY AND CHARACTERIZATION ...................................................................................1 2.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL ASSESSMENT INFORMATION ...................................................................................................2 3.0 WATER SUPPLY WELL INFORMATION .......................................................................................5 4.0 FREE PRODUCT REMOVAL ........................................................................................................5 5.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS ..................................5 6.0 CONCLUSIONS .........................................................................................................................5 7.0 LIMITATIONS ...........................................................................................................................5 8.0 STATEMENTS AND CERTIFICATION ...........................................................................................6 FIGURES Figure 1: Site Location Map Figure 2: Site Vicinity Map Figure 3: Site Map Figure 4: Water Table Surface Map Figure 5: Ground Water Quality Map Figure 6: Estimated Contaminant Mass Area Map TABLES Table 1: UST Owner and Operator Information Table 2: UST System Information Table 3: Water Supply Well Information Table 4: Adjacent Property Owner Information Table 5: Well Construction and Gauging Information Table 6: Summary of Ground Water Sample Analytical Results APPENDICES Appendix A: State Correspondence Appendix B: Laboratory Report – Ground Water Samples Appendix C: Contaminant Mass Calculations Appendix D: Water Supply Well Abandonment Agreement Letters ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: February 13, 2023 Peele’s Service Station Project Manager: Ethan Rogerson, G.I.T. GRI Project No. 2516 1 1.0 SITE HISTORY AND CHARACTERIZATION GRI presents the results of the January 2023 ground water sampling event at the Peele’s Service Station site; located at 2675 Old US Highway 64 in Jamesville, Martin County, North Carolina (Figure 1). These activities were conducted in accordance with GRI Proposal No. 22-828, which was submitted to NCDEQ on December 20, 2022, and was approved as Task Authorization No. 10000-64 on January 3, 2022. State correspondence has been included as Appendix A. The site is currently owned by Tyese La Starr Jordan. According to available information, one 1,000-gallon and one 550-gallon gasoline USTs were removed from the site on September 23, 1992. UST owner/operator information and UST system information are included as Tables 1 and 2, respectively. The Registered Tank Report is shown below: The site and surrounding area are residential properties. The site parcel contains two buildings (residential home and former store) and is primarily capped with grass, gravel and asphalt. The overall topography at the site is relatively flat. No surface water bodies were identified within a 500-foot radius of the site. Eighteen Type II monitoring wells (MW-1, MW-2, MW-2R, MW-3 through MW-4 and MW-6 through MW-18) and one Type III monitoring well (MW-5) were installed at the site during previous ground water assessment and corrective action activities. On March 3, 2021, receptor information was updated for the site. Sixty-two water supply wells were identified within a 1,500-foot radius of the site. Of the identified water supply wells, forty-five are located within a 1,000-foot radius of the site. Three of the water supply wells are located within a 250-foot radius of the site. During the January 2023 sampling event, water supply well locations were measured with a GPS device and corrected locations of the wells were subsequently mapped. It was confirmed that WSW- 3 and WSW-62 have been partially filled and are considered to have been destroyed. The residence associated with these water supply wells is abandoned and the property has been overgrown with trees and brush. Municipal water is not available to the site or surrounding properties. Water supply well ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: February 13, 2023 Peele’s Service Station Project Manager: Ethan Rogerson, G.I.T. GRI Project No. 2516 2 information is presented in Table 3. Adjacent property owner information is presented in Table 4. A Site Vicinity Map showing the adjacent properties has been included as Figure 2. A Site Map showing the locations of the monitoring wells and the structures on-site has been included as Figure 3. Photos of WSW-3 and WSW-62 are included below: In 1996 a CAP was submitted for the site by a past consultant. No milestones were presented in the 1996 CAP. Although GRI cannot verify the accuracy of information obtained from previous reports, for the purposes of this report, it is assumed to be correct. Please refer to previous submittals for further historical information regarding the site. 2.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL ASSESSMENT INFORMATION On January 11, 2023, fourteen monitoring wells (MW-1, MW-2, MW-2R, MW-3 through MW-7, MW-9, MW-11, MW-14, MW-15, MW-17 and MW-18) were gauged, purged and/or sampled. Please note, monitoring wells (MW-8, MW-10, MW-12, MW-13 and MW-16) were not located. Free product was not observed in any of the monitoring wells. Monitoring wells MW-2, MW-3, MW-4, MW-6, MW-7 and MW- 14 were dry and were not sampled. Depths to ground water in the Type II monitoring wells ranged from 11.11 feet to 15.02 feet below the tops of well casings. Ground water elevations in the Type II monitoring wells ranged from 85.82 feet to 89.18 feet. Please note, the depth to water recorded for MW-17 is considered to be anomalous and was not considered for calculation of ground water flow direction or hydraulic gradient. Ground water flow across the site was generally toward the northeast with a horizontal gradient of less than 0.01 feet per foot. The vertical hydraulic gradient calculated for paired wells MW-1 and MW-5 was approximately 0.43 feet per foot in the downward direction. Well construction and gauging information is presented in Table 5. A Water Table Surface Map based on the Type II monitoring wells is included as Figure 4. A summary of the current ground water gauging data is shown below: ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: February 13, 2023 Peele’s Service Station Project Manager: Ethan Rogerson, G.I.T. GRI Project No. 2516 3 Well ID Screened Interval (x to y ft. BGS) Bottom of Well (ft. BGS) Top of Casing Elevation (ft.) Depth to Water from Top of Casing (feet) Free Product Thickness (ft.) Ground Water Elevation (ft.) MW-1 5 - 15 15 100.36 11.79 0.00 88.57 MW-2 2 - 12 12 100.54 Dry Dry Dry MW-2R 7 - 17 17 100.86 12.65 0.00 88.21 MW-3 2 – 12 12 100.62 Dry Dry Dry MW-4 5 – 15 15 100.71 Dry Dry Dry MW-5 30 – 35 35 100.40 20.06 0.00 80.34 MW-6 5 -15 15 100.10 Dry Dry Dry MW-7 2.5 – 12 12 100.32 Dry Dry Dry MW-8 5 - 15 15 100.23 NM 0.00 NM MW-9 5 - 15 15 100.29 11.11 0.00 89.18 MW-10 4 - 14 14 100.25 NM 0.00 NM MW-11 4 - 14 14 100.26 13.64 0.00 86.62 MW-12 4 – 14 14 100.50 NM 0.00 NM MW-13 8 - 18 18 100.29 NM 0.00 NM MW-14 8 - 18 18 101.41 Dry Dry Dry MW-15 8 – 18 18 100.60 13.78 0.00 86.82 MW-16 8 – 18 18 100.87 NM 0.00 NM MW-17 5 – 15 15 100.66 5.43 0.00 95.23 MW-18 5 - 15 15 100.88 15.02 0.00 85.86 Ground water samples collected from the monitoring wells were submitted for laboratory analyses using EPA Method 6200B. Concentrations of benzene, xylenes and/or naphthalene that exceeded the MACs were reported in the ground water samples collected from MW-1, MW-2R and MW-11. All of the reported contaminant concentrations were less than the GCLs. A summary of the analytical results for ground water samples collected on January 11, 2023, is presented in Table 6. A Ground Water Quality Map based on the January 2023 data is included as Figure 5. A complete report of laboratory analyses of the ground water samples collected from the monitoring wells during the January 2023 sampling event has been included as Appendix B. A summary of the current ground water analytical data is shown below: Contaminant of Concern  Be n z e n e To l u e n e Et h y l b e n z e n e Xy l e n e s MT B E Na p h t h a l e n e Well ID MACs (mg/l) 1 600 600 500 20 6 GCL (mg/l) 5,000 260,000 84,500 85,500 20,000 6,000 MW-1 4.6 0.76 6.4 3.6 <0.13 16.9 MW-2 NS NS NS NS NS NS MW-2R 74.1 88.2 21.2 1,270 <3.1 8.8 J MW-3 NS NS NS NS NS NS MW-4 NS NS NS NS NS NS MW-5 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 MW-6 NS NS NS NS NS NS MW-7 NS NS NS NS NS NS MW-8 NS NS NS NS NS NS MW-9 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: February 13, 2023 Peele’s Service Station Project Manager: Ethan Rogerson, G.I.T. GRI Project No. 2516 4 Contaminant of Concern  Be n z e n e To l u e n e Et h y l b e n z e n e Xy l e n e s MT B E Na p h t h a l e n e Well ID MACs (mg/l) 1 600 600 500 20 6 GCL (mg/l) 5,000 260,000 84,500 85,500 20,000 6,000 MW-10 NS NS NS NS NS NS MW-11 7.9 J <3.1 49.1 245 <3.1 210 MW-12 NS NS NS NS NS NS MW-13 NS NS NS NS NS NS MW-14 NS NS NS NS NS NS MW-15 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 MW-16 NS NS NS NS NS NS MW-17 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 MW-18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 Trip Blank <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 The baseline contaminant mass at the site was determined based on the total BTEX, MTBE and naphthalene concentrations from the April 2015 ground water sampling event as well as the maximum historical water column height observed in the target area. The contaminant plume consists of one area (Area 1) based on the benzene concentrations during the April 2015 ground water sampling event. The contaminant mass has decreased by 87.1% in Area 1. Please note, the Contaminant Fate and Transport Model proposed for the January 2023 sampling event could not be completed due to the drop in ground water elevation at the site. Contaminant mass calculations have been included as Appendix C. A map of the contaminant mass areas has been included as Figure 6. A chart depicting the overall trend in contaminant mass is shown below: ___________________________________________________________________________________________ Prepared by: Geological Resources, Inc. Ground Water Monitoring Report Prepared on: February 13, 2023 Peele’s Service Station Project Manager: Ethan Rogerson, G.I.T. GRI Project No. 2516 5 The site is located in the Coastal Plain Physiographic Province of North Carolina. The water table has a seasonal high depth to water of approximately eight to twelve feet bgs. 3.0 WATER SUPPLY WELL INFORMATION On January 11, 2023, water supply wells WSW-3 and WSW-62 were confirmed to have been destroyed. During field activities, a well abandonment agreement was left at the residence of WSW-1. Additional Well abandonment agreements were sent to the property owner via certified mail on January 24, 2023, and January 31, 2023. To date, responses regarding approval to abandon WSW-1 have not been received. Copies of the submitted water supply well abandonment agreement letters are included as Appendix D. 4.0 FREE PRODUCT REMOVAL Free product has historically been present in MW-2R. There has not been any measurable free product in MW-2R since 2014. 5.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS No natural attenuation monitoring plan is currently in place at the site. 6.0 CONCLUSIONS  Ground water flow across the site was generally toward the northeast during the January 2022 sampling event. The horizontal hydraulic gradient across the site was less than 0.01 feet per foot. The vertical gradient was approximately 0.43 feet per foot in the downward direction.  Concentrations of benzene, xylenes and/or naphthalene that exceeded the MACs were reported in the ground water samples collected from MW-1, MW-2R and MW-11. All of the reported contaminant concentrations were less than the GCLs.  Contaminant mass at the site has decreased by 87.1% between April 2015 and January 2023.  Free product has not been observed at the site since 2014.  The Contaminant Fate & Transport Model proposed for the January 2023 sampling event could not be completed due to the drop in ground water elevation at the site.  Based on this information, the risk classification for the site should remain high risk. Quarterly sampling should be conducted on monitoring wells MW-1, MW-2R, MW-11, MW-14 and MW-18 until the water table is high enough to collect sufficient data for a Contaminant Fate & Transport model. If the model results are favorable, the incident may close with the filing of a NRP on the deed of the subject property. The next sampling event is tentatively scheduled for April 2023 and should include a comprehensive sampling event to satisfy model requirements. 7.0 LIMITATIONS This report has been prepared for the exclusive use of North East Oil Company, Inc. for specific application to the referenced site in Martin County, North Carolina. The assessment was conducted based on the scope of work and level of effort desired by NCDEQ and with resources adequate only for that scope of work. Our findings have been developed in accordance with generally accepted standards of environmental practices in the State of North Carolina, available information, and our professional judgment. No other warranty is expressed or implied. FIGURES "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J"J "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J "J"J "J "J "J "J"J "J "J "J "J "J "J "J "J SITE 6746-73-3574 6746-60-7784 6746-81-3879 6746-81-3710 6746-81-2680 6746-81-1248 6746-81-1129 6746-81-2417 6746-72-7149 6746-60-9317 6746-81-2891 6746-71-5500 6746-61-9026 6746-70-3123 6746-82-0127 6746-81-2563 6746-71-1252 6746-70-4263 6746-71-6043 6746-70-1479 6746-61-7204 6746-71-6828 6746-71-6199 6746-71-0040 6746-70-3480 6746-72-6099 6746-60-8993 6746-80-2304 6746-82-1349 6746-71-8597 6746-70-2628 6746-70-8496 6746-71-5786 6746-71-6969 6746-71-5657 6746-71-9952 6746-82-3332 6746-70-3287 6746-72-8484 6746-70-5546 6746-82-3112 6746-71-4353 6746-72-7477 6746-70-3926 6746-70-3817 6746-70-69026746-70-5885 6746-82-0298 6746-71-4201 6746-71-3066 6746-71-0392 6746-71-6145 6746-82-2274 6746-71-40196746-71-3122 6746-82-3251 6746-82-1296 6746-70-0706 WSW-9 WSW-8 WSW-7 WSW-6 WSW-5 WSW-4 WSW-3 WSW-2 WSW-1 WSW-63 WSW-62 WSW-61 WSW-60 WSW-59WSW-58WSW-57 WSW-56 WSW-55 WSW-54 WSW-53 WSW-52 WSW-51 WSW-50 WSW-49 WSW-48 WSW-47 WSW-46 WSW-45 WSW-44 WSW-43 WSW-42 WSW-41 WSW-40 WSW-39 WSW-38 WSW-37 WSW-36 WSW-35WSW-34 WSW-33 WSW-32 WSW-31 WSW-30 WSW-29 WSW-28WSW-27 WSW-26 WSW-25 WSW-24 WSW-23 WSW-22 WSW-21 WSW-20 WSW-19 WSW-18 WSW-17 WSW-16 WSW-15 WSW-14 WSW-13 WSW-12WSW-11 WSW-10 64 Swinson Road Rosewood Lane Uniontown Road Coburn Road 64 64 Swinson Road FIGURE 2: SITE VICINITY MAPPEELE'S SERVICE STATION2675 OLD U.S. HIGHWAY 64JAMESVILLE, MARTIN COUNTYNORTH CAROLINAINCIDENT NO. 10000GRI PROJECT NO. 2516 PREPARED BY:GEOLOGICAL RESOURCES, INC.NOVEMBER 18, 2011REVISED: APRIL 8, 2021 ³ 0 300150Feet1 inch = 300 feet 1,500-FOOT RADIUS 1,000-FOOT RADIUS 250-FOOT RADIUS 500-FOOT RADIUS LEGEND !H Water Supply Well (Non-Potable) "J Water Supply Well (Potable) Roads Surface Water Bodies Well Owners and Adjacent Properties Parcels TABLES UST ID Number 1 Facility ID Number Owner or Operator? Owner/Operator UST ID Number 2 Facility ID Number Owner or Operator? Owner/OperatorE T SIX INC 03/07/1980 - 09/23/1992 Highway 42 West, Ahoskie, NC 27910 00-0-0000013895 Name of Owner or Operator Dates of Ownership / Operation Address Telephone Number Unknown Highway 42 West, Ahoskie, NC 27910 Unknown Telephone Number TABLE 1 UST OWNER/OPERATOR INFORMATION PEELE'S SERVICE STATION (INCIDENT NO. 10000) 00-0-0000013895 Name of Owner or Operator Dates of Ownership / Operation E T SIX INC 03/12/1961 - 09/23/1992 Address Page 1 of 1 Date: 07/22/2020 Was Release Associated with UST System? (Yes / No) 1 Gasoline 1,000 3/12/1961 Single Wall Steel 64" x 72"Single Wall Steel Removed Yes 2 Gasoline 550 3/7/1980 Single Wall Steel 46" x 74"Single Wall Steel Removed Yes Notes: • FRP: Fiberglass reinforced plastic. TABLE 2 UST SYSTEM INFORMATION PEELE'S SERVICE STATION (INCIDENT NO. 10000) Status of UST UST ID No. Current or Most Recent Contents Capacity (gallons) Date Installed Construction Details Tank Dimensions Description of Associated Product Piping and Pumps Facility ID # : 00-0-0000013895 Page 1 of 1 Facility ID # : 00-0-0000013895 Well ID.Parcel ID No.Well Owner Mailing Address Well Use (Potable / Non- Potable etc.) Distance from source area of release (ft.) WSW-1/DW-1 6746-71-5657 Evangeline M. Patterson 3759 Brennan Avenue Norfolk, VA 23502 Potable ~150 NW WSW-2 6746-71-5500 (site)Tyese Lastarr Jordan 3201 Piney Woods Road Jamesville, NC 27846 Potable ~60 SW WSW-3/DW-2 6746-71-5786 Mittie and Theatris Taper Heirs c/o Treva Alston 13123 Winding Trail Road Laurel, MD 20707 Destroyed ~240 N WSW-4 6746-71-4201 Vivian R. & Nataniel Birth, Et Als 1732 Farmington Road Rocky Mount, NC 27801 Potable ~340 SW WSW-5 6746-81-1129 Daniel and Flora Boston 404 Winessett Circle Plymouth, NC 27962 Potable ~250 SE WSW-6 6746-71-8597 Harry, Linda & Lynette Ghee 2024 Ashridge Drive Fayetteville, NC 28304 Potable ~320 NE WSW-7 6746-81-2417 Soloman Keyes Estate c/o Regina K Keyes 2720 Old US Highway 64 Jamesville, NC 27846 Potable ~270 NE WSW-8 6746-81-2563 Gerald Keyes 2736 Old US Highway 64 Jamesville, NC 27846 Potable ~320 NE WSW-9 6746-71-6199 Claven James Heirs c/o Charmayne Purkett 2646 Old US Highway 64 Jamesville, NC 27846 Potable ~340 SE WSW-10 6746-71-6145 Enrique & Annie Benita Ellin 54 East Porthaven Way Clayton, NC 27527 Not In Use ~400 SE WSW-11 Potable ~510 S WSW-12 Potable ~520 SE WSW-13 6746-70-6902 Christopher Keller 2590 Old US Highway 64 Jamesville, NC 27846 Potable ~570 S WSW-14 6746-70-5885 Potable ~640 S WSW-19 6746-70-3817 Potable ~660 SE WSW-15 6746-71-4019 Loretta Carter 612 Weathervane Way Rocky Mounty, NC 27803 Potable ~400 S WSW-16 6746-71-3122 Emily Rodgers 2605 Old US Highway 64 Jamesville, NC 27846 Potable ~420 SW WSW-17 6746-71-3066 Charles E. Peele 2601 Old US Highway 64 Jamesville, NC 27846 Potable ~480 SW WSW-18 6746-70-3926 David and Sherry Cook Post Office Box 594 Plymouth, NC 27962 Potable ~560 S WSW-20 6746-70-2628 Fractal Realty, LLC 5906 Blanco River Pass Austin, TX 78749 Potable ~820 SW WSW-21 6746-70-1479 Vera J. Brown c/o Ethel B. Murrell 1507 Golf Course Drive Mitchellville, MD 20721 Potable ~1,050 SW WSW-22 Potable ~1,370 SW WSW-23 Potable ~1,420 SW WSW-24 6746-70-3480 Rosalind J. Minor (et al)1910 Old US Highway 64 Jamesville, NC 27846 Potable ~1,030 S WSW-25 6746-70-4263 Portia Harris 1080 Union Town Road Jamesville, NC 27846 Potable ~1,290 S WSW-26 6746-70-3123 Hosea James (Heirs)2444 Old US Highway 64 Jamesville, NC 27846 Potable ~1,400 S WSW-27 6746-70-5546 William Earl & Alfreda Moore 1031 Union Town Road Jamesville, NC 27846 Potable ~980 SE WSW-28 6746-70-8496 Hattie L. Simpson 1100 Rosewood Lane Jamesville, NC 27846 Potable ~1,080 SE WSW-29 6746-80-2304 Deborah Davenport 1170 Rosewood Lane Jamesville, NC 27846 Potable ~1,390 SE WSW-30 6746-60-7784 Cottie Peele (Heirs) 1858 Swinson Road Jamesville, NC 27846 Potable ~1,110 SW WSW-31 6746-70-0706 Jonah and Katherine Peele Heirs 1858 Swinson Road Jamesville, NC 27846 Potable ~980 SW WSW-32 6746-70-0833 Jeremiah Peele (Heirs)1858 Swinson Road Jamesville, NC 27846 Potable ~900 SW WSW-33 Potable ~980 SW WSW-34 Potable ~940 SW WSW-35 Potable ~890 SW WSW-36 6746-71-0040 Freedomhill Properties, LLC 3420 Pump Road Henrico, VA 23233 Potable ~810 SW WSW-37 6746-61-9026 Carolyn R. Moore Meekins 1814 Swinson Road Jamesville, NC 27846 Potable ~760 SW WSW-38 6746-61-7204 Helen Louise Gibson 1794 Swinson Road Jamesville, NC 27846 Potable ~840 SW WSW-39 6746-71-1252 Aaron Biggs (Heirs) c/o Emily Rodgers 2605 Old US Highway 64 Jamesville, NC 27846 Potable ~470 SW WSW-40 6746-71-0392 Manique S. Billups 1781 Swinson Road Jamesville, NC 27846 Potable ~460 SW 6746-60-9317 TABLE 3 WATER SUPPLY WELL INFORMATION PEELE'S SERVICE STATION (INCIDENT NO. 10000) Date: 04/08/2021 6746-71-6043 Dollie Armstrong Heirs c/o Charmayne Simpson Post Office Box 392 Jamesville, NC 27846 Gregory Kent (Heirs)2578 Old US Highway 64 Jamesville, NC 27846 William C. Brooks Jr.109 East Street Windsor, NC 27893 6746-60-8993 Verna Mae Moore 1850 Swinson Road Jamesville, NC 27846 Page 1 of 2 Facility ID # : 00-0-0000013895 Well ID.Parcel ID No.Well Owner Mailing Address Well Use (Potable / Non- Potable etc.) Distance from source area of release (ft.) TABLE 3 WATER SUPPLY WELL INFORMATION PEELE'S SERVICE STATION (INCIDENT NO. 10000) Date: 04/08/2021 WSW-41/ DW-3 6746-71-6828 Shelbert & Honora Manning 1317 Mill Road Jamesville, NC 27846 Potable ~380 NE WSW-42 6746-71-6969 Abram Lightfoot 165 Cranes Nest Drive Franklinton, NC 27525 Potable ~510 NE WSW-43 6746-72-6099 Oscar Lee Cross 2807 Old US Highway 64 Jamesville, NC 27846 Potable ~620 NE WSW-44 6746-72-7149 Promise Land Church of Christ 2817 Old US Highway 64 Jamesville, NC 27846 Potable ~720 NE WSW-45 6746-72-7477 Dana and Jane Thayer 2881 Old US Highway 64 Jamesville, NC 27846 Potable ~960 NE WSW-46 6746-72-8484 Lucretta Biggs (Heirs) c/o Joseph Biggs 2887 Old US Highway 64 Jamesville, NC 27846 Potable ~1,030 NE WSW-47 6746-82-1349 Shirley Gloria Jean Keyes (et al)1539 Black Jack Simpson Road Greenville, NC 27858 Potable ~1,060 NE WSW-48 Potable ~1,120 NE WSW-49 Potable ~1,150 NE WSW-50 6746-82-0298 Hilton Keyes 1021 Apple Lane Jamesville, NC 27846 Potable ~960 NE WSW-51 6746-82-0127 Kenneth C. Moore 2840 Old US Highway 64 Jamesville, NC 27846 Potable ~800 NE WSW-52 6746-81-3879 Cartina M Chesson 2808 Old US Highway 64 Jamesville, NC 27846 Potable ~680 NE WSW-53 6746-71-9952 Javon L. Webb 118 North Chase Drive Concord, NC 28027 Potable ~590 NE WSW-54 6746-81-2891 Wanda Hooper and Adrina S. Moore Post Office Box 430 Jamesville, NC 27846 Potable ~690 NE WSW-55 6746-81-3710 Pearlie Mae & Richard Moore 1362 Albany Avenue Brooklyn, NY 11203 Potable ~470 NE WSW-56 6746-81-2680 Glennie James 19 Bryant Road Turnersville, NJ 08012 Potable ~380 NE WSW-57 6746-82-1296 Tara A. Counts 1047 Apple Lane Jamesville, NC 27846 Potable ~1,020 NE WSW-58 6746-82-2274 Aubrey Ray Clark 1065 Apple Lane Jamesville, NC 27846 Potable ~1,040 NE WSW-59 6746-82-3251 Joyce Dianne James 2444 Old US Highway 64 Jamesville, NC 27846 Potable ~1,070 NE WSW-60 6746-82-3112 Joyce J. Spruill, Et Als 112A Albemarle Drive Plymouth, NC 27962 Potable ~940 NE WSW-61 6746-70-3287 Ida Mae James Heirs 1858 Swinson Road Jamesville, NC 27846 Potable ~1,240 S WSW-62 6746-71-5786 Mittie and Theatris Taper Heirs c/o Treva Alston 13123 Winding Trail Road Laurel, MD 20707 Destroyed ~280 N WSW-63 6746-71-4353 Valerie Rena Horton 2661 Old US Highway 64 Jamesville, NC 27846 Potable ~170 SW Note: • Water supply wells are keyed to Figure 2. 6746-82-3332 Shirley Mae Keyes 2880 Old US Highway 64 Jamesville, NC 27846 Page 2 of 2 Date: 04/08/2021 Facility ID # : 00-0-0000013895 Parcel Number Owner Name Address 6746-71-5500 (Site)Tyese Lastarr Jordan 3201 Piney Woods Road Jamesville, NC 27846 6746-71-4353 Valerie Rena Horton 2661 Old U.S. Highway 64 Jamesville, NC 27846 6746-73-3574 R. G., Jr. and Shelba Coburn 1474 Swinson Road Jamesville, NC 27846 6746-71-5657 Evangeline M. Patterson 3759 Brennan Avenue Norfolk, VA 23502 6746-71-8597 Harry, Linda & Lynette Ghee 2024 Ashridge Drive Fayetteville, NC 28304 6746-81-1248 6746-81-1129 Note: • Properties are keyed to Figure 2. TABLE 4 ADJACENT PROPERTY OWNER INFORMATION PEELE'S SERVICE STATION (INCIDENT NO. 10000) Daniel and Flora Boston 406 Winessett Circle Plymouth, NC 27962 Page 1 of 1 Date: 02/08/2023 Well ID Date Installed (m/dd/yy) Date Water Level Measured (m/dd/yy) Well Casing Depth (ft. BGS) Screened Interval (x to y ft. BGS) Bottom of Well (ft. BGS) Top of Casing Elevation (ft.) Depth to Water from Top of Casing (feet) Free Product Thickness (ft.) Ground Water Elevation (ft.) Comments 03/01/07 3.32 0.00 97.04 08/13/07 DRY 0.00 NM 03/12/09 NM 0.00 NM 08/25/09 DRY 0.00 NM 12/08/11 10.17 0.00 90.19 06/13/12 6.98 0.00 93.38 03/07/13 4.33 0.00 96.03 10/02/13 9.19 0.00 91.17 04/02/14 3.41 0.00 96.95 09/30/14 5.98 0.00 94.38 04/01/15 1.87 0.00 98.49 01/11/16 2.60 0.00 97.76 07/15/20 8.45 0.00 91.91 03/04/21 2.85 0.00 97.51 12/14/21 11.42 0.00 88.94 01/11/23 11.79 0.00 88.57 03/01/07 2.63 0.00 97.91 08/13/07 DRY 0.00 NM 03/12/09 DRY 0.00 NM 08/25/09 DRY 0.00 NM 12/08/11 DRY 0.00 NM 06/13/12 7.07 0.00 93.47 03/07/13 2.60 0.00 97.94 10/02/13 DRY 0.00 NM 01/11/16 1.98 0.00 98.56 10/05/16 8.49 0.00 92.05 06/26/17 2.12 0.00 98.42 04/11/18 2.06 0.00 98.48 07/15/20 DRY DRY DRY 03/04/21 2.89 0.00 97.65 12/14/21 DRY DRY DRY 01/11/23 DRY DRY DRY 12/08/11 10.96 0.00 89.90 06/13/12 8.00 0.17 93.01 01/23/13 7.81 0.10 93.13 Before AFVR 01/23/13 10.05 0.00 90.81 After AFVR 03/07/13 5.66 0.44 95.58 08/27/13 5.73 0.25 95.34 Before AFVR 08/27/13 10.17 0.00 90.69 After AFVR 10/02/13 9.88 0.00 90.98 04/02/14 3.39 0.04 97.50 09/30/14 7.07 0.03 93.82 04/01/15 2.16 0.00 98.70 01/11/16 2.97 0.00 97.89 10/05/16 8.11 0.00 92.75 06/26/17 4.00 0.00 96.86 04/11/18 3.47 0.00 97.39 01/08/19 3.26 0.00 97.60 10/03/19 10.88 0.00 89.98 07/15/20 9.24 0.00 91.62 03/04/21 3.68 0.00 97.18 12/14/21 12.12 0.00 88.74 01/11/23 12.65 0.00 88.21 03/01/07 2.85 0.00 97.77 08/13/07 DRY 0.00 NM 03/12/09 DRY 0.00 NM 08/25/09 DRY 0.00 NM 12/08/11 DRY 0.00 NM 06/13/12 7.38 0.00 93.24 03/07/13 3.22 0.00 97.40 10/02/13 DRY 0.00 NM 01/11/16 1.87 0.00 98.75 01/11/23 DRY DRY DRY 03/01/07 3.70 0.00 97.01 08/13/07 DRY 0.00 NM 03/12/09 DRY 0.00 NM 08/25/09 DRY 0.00 NM 12/08/11 10.02 0.00 90.69 06/13/12 6.86 0.00 93.85 03/07/13 1.90 0.00 98.81 10/02/13 9.44 0.00 91.27 04/02/14 1.60 0.00 99.11 09/30/14 6.57 0.00 94.14 04/01/15 0.93 0.00 99.78 01/11/23 DRY DRY DRY 03/01/07 16.71 0.00 83.69 08/13/07 19.68 0.00 80.72 03/12/09 21.73 0.00 78.67 08/25/09 21.07 0.00 79.33 12/08/11 19.30 0.00 81.10 06/13/12 18.50 0.00 81.90 03/07/13 17.39 0.00 83.01 10/02/13 18.25 0.00 82.15 04/02/14 15.71 0.00 84.69 09/30/14 17.85 0.00 82.55 04/01/15 15.22 0.00 85.18 01/11/23 20.06 0.00 80.34 TABLE 5 WELL CONSTRUCTION AND GAUGING INFORMATION PEELE'S SERVICE STATION (INCIDENT NO. 10000) Facility ID # : 00-0-0000013895 100.36155 - 15501/26/93MW-1 100.54122 - 12201/27/93MW-2 100.86177 - 17712/08/11MW-2R 100.62122 - 12201/27/93MW-3 100.71155 - 15505/14/93MW-4 100.403530 - 353005/18/93MW-5 Page 1 of 3 Date: 02/08/2023 Well ID Date Installed (m/dd/yy) Date Water Level Measured (m/dd/yy) Well Casing Depth (ft. BGS) Screened Interval (x to y ft. BGS) Bottom of Well (ft. BGS) Top of Casing Elevation (ft.) Depth to Water from Top of Casing (feet) Free Product Thickness (ft.) Ground Water Elevation (ft.) Comments TABLE 5 WELL CONSTRUCTION AND GAUGING INFORMATION PEELE'S SERVICE STATION (INCIDENT NO. 10000) Facility ID # : 00-0-0000013895 03/01/07 4.52 0.00 95.58 08/13/07 11.32 0.00 88.78 03/12/09 DRY 0.00 DRY 08/25/09 12.37 0.00 87.73 12/08/11 10.70 0.00 89.40 06/13/12 7.74 0.00 92.36 03/07/13 5.68 0.00 94.42 10/02/13 NM 0.00 NM 01/11/23 DRY DRY DRY 08/25/09 12.05 0.00 88.27 12/08/11 11.03 0.00 89.29 06/13/12 8.38 0.00 91.94 03/07/13 5.52 0.00 94.80 10/02/13 9.89 0.00 90.43 01/11/23 DRY DRY DRY 03/01/07 2.76 0.00 97.47 08/13/07 10.70 0.00 89.53 03/12/09 NM 0.00 NM 08/25/09 10.55 0.00 89.68 12/08/11 9.60 0.00 90.63 06/13/12 5.97 0.00 94.26 03/07/13 2.60 0.00 97.63 10/02/13 8.73 0.00 91.50 04/02/14 3.12 0.00 97.11 09/30/14 5.37 0.00 94.86 04/01/15 2.19 0.00 98.04 01/11/23 NM 0.00 NM Not Located 03/01/07 3.16 0.00 97.13 08/13/07 10.74 0.00 89.55 03/12/09 DRY 0.00 DRY 08/25/09 10.60 0.00 89.69 12/08/11 9.52 0.00 90.77 06/13/12 6.58 0.00 93.71 03/07/13 4.16 0.00 96.13 10/02/13 NM 0.00 NM 01/11/23 11.11 0.00 89.18 08/25/09 13.00 0.00 87.25 12/08/11 10.86 0.00 89.39 06/13/12 8.28 0.00 91.97 03/07/13 6.84 0.00 93.41 10/02/13 9.58 0.00 90.67 04/02/14 3.09 0.00 97.16 09/30/14 7.67 0.00 92.58 04/01/15 2.29 0.00 97.96 01/11/23 NM 0.00 NM Not Located 03/01/07 5.93 0.00 94.33 08/13/07 11.97 0.00 88.29 03/12/09 15.51 0.00 84.75 08/25/09 14.19 0.00 86.07 12/08/11 11.88 0.00 88.38 06/13/12 9.51 0.00 90.75 03/07/13 7.53 0.00 92.73 10/02/13 10.40 0.00 89.86 04/02/14 4.64 0.00 95.62 09/30/14 8.86 0.00 91.40 04/01/15 3.70 0.00 96.56 01/11/16 4.40 0.00 95.86 10/05/16 10.54 0.00 89.72 06/26/17 5.93 0.00 94.33 04/11/18 4.86 0.00 95.40 01/08/19 4.75 0.00 95.51 10/03/19 11.60 0.00 88.66 07/15/20 10.01 0.00 90.25 03/04/21 5.40 0.00 94.86 12/14/21 12.41 0.00 87.85 01/11/23 13.64 0.00 86.62 100.25144 - 14402/16/94MW-10 100.29155 - 15505/19/93MW-9 100.10155 - 15505/17/93MW-6 100.32122.5 - 122.505/17/93MW-7 100.23155 - 15505/19/93MW-8 100.26144 - 14402/16/94MW-11 Page 2 of 3 Date: 02/08/2023 Well ID Date Installed (m/dd/yy) Date Water Level Measured (m/dd/yy) Well Casing Depth (ft. BGS) Screened Interval (x to y ft. BGS) Bottom of Well (ft. BGS) Top of Casing Elevation (ft.) Depth to Water from Top of Casing (feet) Free Product Thickness (ft.) Ground Water Elevation (ft.) Comments TABLE 5 WELL CONSTRUCTION AND GAUGING INFORMATION PEELE'S SERVICE STATION (INCIDENT NO. 10000) Facility ID # : 00-0-0000013895 03/01/07 3.61 0.00 96.89 08/13/07 11.10 0.00 89.40 03/12/09 13.44 0.00 87.06 08/25/09 NM 0.00 NM 12/08/11 10.17 0.00 90.33 06/13/12 7.30 0.00 93.20 03/07/13 4.98 0.00 95.52 10/02/13 NM 0.00 NM 01/11/23 NM 0.00 NM Not Located 03/01/07 4.50 0.00 95.79 08/13/07 11.04 0.00 89.25 03/12/09 13.80 0.00 86.49 08/25/09 NM 0.00 NM 12/08/11 10.72 0.00 89.57 06/13/12 7.57 0.00 92.72 03/07/13 5.67 0.00 94.62 10/02/13 NM 0.00 NM 01/11/23 NM 0.00 NM Not Located 08/25/09 NM NM Not Located 12/08/11 NM NM Not Located 06/13/12 NM NM Not Located 03/07/13 NM NM Not Located 10/02/13 NM NM Not Located 04/02/14 5.78 0.00 95.63 09/30/14 10.23 0.00 91.18 04/01/15 4.89 0.00 96.52 01/11/16 5.67 0.00 95.74 10/05/16 10.28 0.00 91.13 06/26/17 6.47 0.00 94.94 07/15/20 NM NM Not Located 03/04/21 6.49 0.00 94.92 12/14/21 DRY DRY DRY 01/11/23 DRY DRY DRY 08/25/09 NM NM Not Located 12/08/11 NM NM Not Located 06/13/12 NM NM Not Located 03/07/13 NM NM Not Located 10/02/13 NM NM Not Located 04/02/14 5.13 0.00 95.47 09/30/14 NM NM Not Located 04/01/15 4.48 0.00 96.12 01/11/16 4.91 0.00 95.69 07/15/20 10.09 0.00 90.51 01/11/23 13.78 0.00 86.82 08/25/09 NM NM Not Located 12/08/11 NM NM Not Located 06/13/12 NM NM Not Located 03/07/13 NM NM Not Located 10/02/13 NM NM Not Located 01/11/23 NM 0.00 NM Not Located 03/01/07 2.09 0.00 98.57 08/13/07 12.71 0.00 87.95 03/12/09 14.78 0.00 85.88 08/25/09 NM 0.00 NM 12/08/11 13.29 0.00 87.37 06/13/12 3.12 0.00 97.54 03/07/13 1.04 0.00 99.62 10/02/13 11.08 0.00 89.58 04/02/14 1.04 0.00 99.62 09/30/14 1.78 0.00 98.88 04/01/15 NM NM NM Under Puddle 01/11/23 5.43 0.00 95.23 03/01/07 8.37 0.00 92.51 08/13/07 12.93 0.00 87.95 03/12/09 17.02 0.00 83.86 08/25/09 NM 0.00 NM 12/08/11 14.45 0.00 86.43 06/13/12 11.92 0.00 88.96 03/07/13 10.25 0.00 90.63 10/02/13 11.41 0.00 89.47 04/02/14 6.63 0.00 94.25 09/30/14 10.88 0.00 90.00 04/01/15 5.54 0.00 95.34 01/11/23 15.02 0.00 85.86 Notes: • * Top-of-casing elevation and well construction data is reproduced from the July 2005 monitoring report prepared by CES Engineering, PC; elevations relative to a temporary benchmark with an assumed datum of 100.00 feet; data reported in feet. • ** : If free product is present in a well, ground water elevation calculated by: [Top of Casing Elevation - Depth to Water] - [free product thickness x 0.8581] • ft BGS : feet below ground surface • NA: Not available. • NM: Not measured; well not located. 100.60188 - 18 100.50144 - 14402/16/94MW-12 100.29188 - 18804/27/95MW-13 101.41188 - 18804/27/95MW-14 804/27/95MW-15 100.87188 - 18804/27/95MW-16 155 - 15508/16/95MW-17 100.66 100.88155 - 15508/16/95MW-18 Page 3 of 3 EPA Method 6010B Well ID Date Collected (mm/dd/yy) 1 600 600 500 20 6 70 400 400 15 400 700 10,000 200 5,000 260,000 80,000 50,000 20,000 6,000 70,000 28,500 25,000 15,000 NE NE NE NE 03/01/07 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 <1.00 NR NR NR NR NR NR NR 08/13/07 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 03/12/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 08/25/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 12/08/11 29.9 0.91 21.2 4.0 0.18 J 48.6 0.32 J 18.5 0.16 J NR NR NR NR NR 06/13/12 10.3 2.2 6.3 113 <0.13 54.7 <0.11 130 17.6 NR NR NR NR NR 03/07/13 4.6 2.7 4.3 215 <0.10 49.4 <0.10 162 30.7 NR NR NR NR NR 10/02/13 36.2 13.1 26.6 1,020 0.35 J 228 <0.10 973 214 NR NR NR NR NR 04/02/14 0.77 1.0 2.1 86.1 <0.10 33.4 <0.10 71.7 11.9 NR NR NR NR NR 09/30/14 1.9 J 3.4 J 5.7 326 <1.0 88.7 <1.0 331 56.6 NR NR NR NR NR 04/01/15 <0.17 <0.17 0.29 J 7.1 <0.16 3.3 <0.16 6.6 0.70 NR NR NR NR NR 01/11/16 <0.13 <0.13 <0.13 0.71 J <0.13 0.41 J <0.13 0.95 0.24 J NR NR NR NR NR 07/15/20 1.2 J 2.7 18.6 194 <0.31 192 <0.31 428 15.2 NR NR NR NR NR 03/11/21 <0.13 <0.13 0.43 J 3.3 <0.13 3.1 <0.13 2.3 0.48 J NR NR NR NR NR 12/14/21 <3.1 <3.1 <3.1 <6.3 <3.1 17.0 <3.1 3.4 J <3.1 NR NR NR NR NR 01/11/23 4.6 0.76 6.4 3.6 <0.13 16.9 <0.13 8.5 0.39 J NR NR NR NR NR 03/01/07 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 <1.00 NR NR NR NR NR NR NR 08/13/07 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 03/12/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 08/25/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 06/13/12 27.1 22.4 29.7 652 <1.3 60.7 <1.1 278 57.3 NR NR NR NR NR 03/07/13 1.7 3.1 1.1 21.7 <0.10 0.49 J <0.10 4.3 1.3 NR NR NR NR NR 10/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 01/11/16 2.8 0.23 J 1.0 3.6 <0.13 0.43 J <0.13 1.5 <0.13 NR NR NR NR NR 10/05/16 13.0 5.1 18.4 211 <0.31 87.2 <0.31 202 18.1 NR NR NR NR NR 06/26/17 0.23 J 0.35 J 0.45 J 6.7 <0.13 1.0 <0.13 6.1 0.38 J NR NR NR NR NR 04/11/18 <0.13 <0.13 <0.13 0.78 J <0.13 0.28 J <0.13 0.91 <0.13 NR NR NR NR NR 07/15/20 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 03/11/21 <0.13 <0.13 <0.13 <0.25 <0.13 0.18 J <0.13 <0.13 <0.13 NR NR NR NR NR 01/11/23 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 12/08/11 147 2,300 1,310 12,250 <6.5 670 <5.4 2,770 756 NR NR NR NR NR 06/13/12 FP FP FP FP FP FP FP FP FP FP FP FP FP FP 10/02/13 729 4,320 1,010 19,210 <25 814 <25 3,640 900 NR NR NR NR NR 04/02/14 FP FP FP FP FP FP FP FP FP FP FP FP FP FP 09/30/14 FP FP FP FP FP FP FP FP FP FP FP FP FP FP 04/01/15 26.2 399 88.6 1,720 <4.1 109 <4.0 641 201 NR NR NR NR NR 01/11/16 8.9 55.6 22.7 180 <0.13 23 <0.13 70.3 23.5 NR NR NR NR NR 10/05/16 332 2,160 420 4,960 <6.3 378 <6.3 1,260 409 NR NR NR NR NR 06/26/17 15.6 129 39.7 303 <0.13 34.1 <0.13 119 31.3 NR NR NR NR NR 04/11/18 39.6 221 160 3,650 <3.1 178 <3.1 650 218 NR NR NR NR NR 01/08/19 36.5 200 181 3,330 <3.1 194 <3.1 664 191 NR NR NR NR NR 10/03/19 46.1 208 247 4,980 <3.1 267 <3.1 780 209 NR NR NR NR NR 07/15/20 858 2,980 166 7,820 <13 208 <13 863 328 NR NR NR NR NR 03/11/21 15.9 152 63.0 996 <1.3 56.8 <1.3 240 86.9 NR NR NR NR NR 12/14/21 8.2 J 16.7 6.4 J 24.0 J <3.1 49.1 <3.1 16.4 <3.1 NR NR NR NR NR 01/11/23 74.1 88.2 21.2 1,270 <3.1 8.8 J <3.1 160 60.1 NR NR NR NR NR 03/01/07 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 <1.00 NR NR NR NR NR NR NR 08/13/07 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 03/12/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 08/25/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 12/08/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 06/13/12 1.4 2.8 8.3 117 <0.33 10.1 <0.27 63.2 23.7 NR NR NR NR NR 03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR 10/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 01/11/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 0.14 J <0.13 NR NR NR NR NR 01/11/23 NS NS NS NS NS NS NS NS NS NS NS NS NS NS TABLE 6 SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS PEELE'S SERVICE STATION (INCIDENT NO. 10000) Date: 02/08/2023 Analytical Method  C9 - C 2 2 A r o m a t i c s MACs (μg/l) Na p h t h a l e n e IP E 1, 2 , 4 - Tr i m e t h y l b e n z e n e 1, 3 , 5 - Tr i m e t h y l b e n z e n e C9 - C 1 8 A l i p h a t i c s C1 9 - C 3 6 A l i p h a t i c s C5 - C 8 A l i p h a t i c s Le a d Facility ID #: 00-0-0000013895 EPA Method 6200B MADEP Methods EPH & VPH Xy l e n e s MT B E GCL (μg/l) Et h y l b e n z e n e Be n z e n e To l u e n e Contaminant of Concern  MW-1 MW-2 MW-2R MW-3 Page 1 of 6 EPA Method 6010B Well ID Date Collected (mm/dd/yy) 1 600 600 500 20 6 70 400 400 15 400 700 10,000 200 5,000 260,000 80,000 50,000 20,000 6,000 70,000 28,500 25,000 15,000 NE NE NE NE TABLE 6 SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS PEELE'S SERVICE STATION (INCIDENT NO. 10000) Date: 02/08/2023 Analytical Method  C9 - C 2 2 A r o m a t i c s MACs (μg/l) Na p h t h a l e n e IP E 1, 2 , 4 - Tr i m e t h y l b e n z e n e 1, 3 , 5 - Tr i m e t h y l b e n z e n e C9 - C 1 8 A l i p h a t i c s C1 9 - C 3 6 A l i p h a t i c s C5 - C 8 A l i p h a t i c s Le a d Facility ID #: 00-0-0000013895 EPA Method 6200B MADEP Methods EPH & VPH Xy l e n e s MT B E GCL (μg/l) Et h y l b e n z e n e Be n z e n e To l u e n e Contaminant of Concern  03/01/07 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 <1.00 NR NR NR NR NR NR NR 08/13/07 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 03/12/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 08/25/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 12/08/11 <0.13 0.80 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 06/13/12 <0.13 <0.13 <0.15 <0.30 <0.13 0.10 J <0.11 <0.10 <0.10 NR NR NR NR NR 03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR 10/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR 04/02/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/30/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 04/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR NR 01/11/23 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 03/01/07 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 <1.00 NR NR NR NR NR NR NR 08/13/07 1.72 <1.0 <1.0 <3.0 3.47 <1.0 0.16 I NR NR NR NR NR NR NR 03/12/09 2.0 J <0.70 1.2 J 2.7 J 3.6 J 4.0 JB <1.0 2.2 J 0.54 J 77.9 <100 <200 <100 <200 08/25/09 3.53 <0.330 <0.670 <1.33 4.68 <1.00 <1.67 <0.330 <0.330 103 <100 <195.2 <95.2 <195.2 12/08/11 <0.13 <0.13 <0.15 <0.30 0.26 J <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 06/13/12 0.31 J <0.13 <0.15 <0.30 <0.13 0.28 J <0.11 <0.10 <0.10 NR NR NR NR NR 03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR 10/02/13 <0.10 <0.10 <0.10 <0.22 0.68 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR 04/02/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/30/14 <0.10 <0.10 <0.10 <0.20 0.61 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 04/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR NR 01/11/23 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR 03/01/07 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 <1.00 NR NR NR NR NR NR NR 08/13/07 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 <5 NR NR NR NR NR NR NR 03/12/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 08/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.67 <0.330 <0.330 2.85 <100 <100 NR <100 12/08/11 <0.13 3.8 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 06/13/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR 10/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 01/11/23 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 08/25/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 12/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 06/13/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR 10/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR 01/11/23 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 03/01/07 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 <1.00 NR NR NR NR NR NR NR 08/13/07 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 <5.0 NR NR NR NR NR NR NR 03/12/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 08/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.67 <0.330 <0.330 3.02 <100 <100 NR <100 12/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 06/13/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR 10/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR 04/02/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/30/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 04/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR NR 01/11/23 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 03/01/07 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 <1.00 NR NR NR NR NR NR NR 09/07/07 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 <5.0 NR NR NR NR NR NR NR 03/12/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 08/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.67 <0.330 <0.330 3.12 <100 <100 NR <100 12/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 06/13/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR 10/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 01/11/23 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 NS NS NS NS NS MW-4 MW-5 MW-6 MW-7 MW-8 MW-9 Page 2 of 6 EPA Method 6010B Well ID Date Collected (mm/dd/yy) 1 600 600 500 20 6 70 400 400 15 400 700 10,000 200 5,000 260,000 80,000 50,000 20,000 6,000 70,000 28,500 25,000 15,000 NE NE NE NE TABLE 6 SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS PEELE'S SERVICE STATION (INCIDENT NO. 10000) Date: 02/08/2023 Analytical Method  C9 - C 2 2 A r o m a t i c s MACs (μg/l) Na p h t h a l e n e IP E 1, 2 , 4 - Tr i m e t h y l b e n z e n e 1, 3 , 5 - Tr i m e t h y l b e n z e n e C9 - C 1 8 A l i p h a t i c s C1 9 - C 3 6 A l i p h a t i c s C5 - C 8 A l i p h a t i c s Le a d Facility ID #: 00-0-0000013895 EPA Method 6200B MADEP Methods EPH & VPH Xy l e n e s MT B E GCL (μg/l) Et h y l b e n z e n e Be n z e n e To l u e n e Contaminant of Concern  08/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.67 <0.330 <0.330 5.60 <100 <100 NR <100 12/08/11 <0.13 5.9 0.33 J 0.73 J <0.13 <0.10 <0.11 0.21 J <0.10 NR NR NR NR NR 06/13/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR 10/02/13 <0.10 <0.10 <0.10 0.16 J <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR 04/02/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/30/14 <0.10 <0.10 <0.10 <0.20 <0.10 0.27 J <0.10 0.21 J <0.10 NR NR NR NR NR 04/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR NR 01/11/23 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 03/01/07 3.58 108 136 1,629 10.6 61.4 15.3 NR NR NR NR NR NR NR 08/13/07 14.2 187 736 9,010 31.3 428 11.2 NR NR NR NR NR NR NR 03/12/09 7.3 <0.70 <0.50 1.9 J 3.2 J 1.7 JB <1.0 0.72 J 1.2 J 2.8 J 176 133 <100 166 08/25/09 7.44 <0.330 1.62 J 7.99 <0.330 2.51 <1.67 1.90 0.332 J 11.6 111 296 <97.1 220 12/08/11 35.8 1.4 218 1,710 1.4 348 1.4 987 354 NR NR NR NR NR 06/13/12 10.6 2.3 J 64.0 429 <0.65 133 <0.54 443 104 NR NR NR NR NR 03/07/13 14.8 2.4 99.9 618 0.32 J 262 <0.10 796 130 NR NR NR NR NR 10/02/13 16.4 4.2 J 147 800 <2.5 248 <2.5 1,020 80.5 NR NR NR NR NR 04/02/14 13.1 3.2 125 916 0.31 J 242 <0.10 911 177 NR NR NR NR NR 09/30/14 6.7 0.61 J 27.9 172 <0.50 135 <0.50 194 20.9 NR NR NR NR NR 04/01/15 1.9 J 1.1 J 28.2 210 <0.82 87.0 <0.80 191 29.2 NR NR NR NR NR 01/11/16 3.4 J 4.0 J 150 1,080 <2.5 476 <2.5 1,420 318 NR NR NR NR NR 10/05/16 1.3 0.14 J 19 12.6 <0.13 38.6 <0.13 83.9 3.3 NR NR NR NR NR 06/26/17 2.7 0.86 87.7 518 0.19 J 294 <0.13 1,130 198 NR NR NR NR NR 04/11/18 11.2 J <3.1 129 1,030 <3.1 339 <3.1 1,610 317 NR NR NR NR NR 01/08/19 26.4 2.9 J 121 896 <2.5 413 <2.5 1,850 445 NR NR NR NR NR 10/03/19 21.3 J 7.1 J 108 522 <6.3 350 <6.3 1,360 299 NR NR NR NR NR 07/15/20 16.5 J 6.6 J 60.6 393 <6.3 259 <6.3 1,650 359 NR NR NR NR NR 03/11/21 4.6 <0.25 29.9 194 <0.25 154 <0.25 707 163 NR NR NR NR NR 12/14/21 7.9 J <3.1 49.1 245 <3.1 210 <3.1 944 243 NR NR NR NR NR 01/11/23 7.6 <0.13 5.3 2.0 <0.13 38.6 <0.13 12.4 0.52 NR NR NR NR NR 03/01/07 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 <1.00 NR NR NR NR NR NR NR 08/13/07 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 <5 NR NR NR NR NR NR NR 03/12/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <1.0 <0.70 <0.50 8.8 <100 <100 NR <100 08/25/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 12/08/11 <0.13 139 <0.15 <0.30 <0.13 0.17 J <0.11 <0.10 <0.10 NR NR NR NR NR 06/13/12 <0.65 <0.64 <0.73 <1.5 <0.65 <0.50 <0.54 <0.50 <0.50 NR NR NR NR NR 03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 0.16 J <0.10 <0.10 <0.10 NR NR NR NR NR 10/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 01/11/23 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 03/01/07 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 <1.00 NR NR NR NR NR NR NR 08/13/07 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 <5.0 NR NR NR NR NR NR NR 03/12/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 08/25/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 12/08/11 <0.13 11.0 0.27 J <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 06/13/12 <0.13 1.0 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR 10/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 01/11/23 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 12/08/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 06/13/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 10/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 04/02/14 0.76 <0.10 <0.10 <0.20 2.2 1.8 2.1 <0.10 <0.10 NR NR NR NR NR 09/30/14 2.5 0.15 J <0.10 1.3 J 2.0 4.2 1.7 <0.10 0.10 J NR NR NR NR NR 04/01/15 <0.17 <0.17 <0.15 <0.43 0.72 <0.12 0.64 <0.14 <0.14 NR NR NR NR NR 01/11/16 2.2 <0.13 0.18 J 1.1 J 0.45 J 8.0 0.64 <0.13 <0.13 NR NR NR NR NR 10/05/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR 06/26/17 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR 07/15/20 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 03/11/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 NS NS NS NS NS 01/11/23 NS NS NS NS NS NS NS NS NS NS NS NS NS NS MW-10 MW-11 MW-12 MW-13 MW-14 Page 3 of 6 EPA Method 6010B Well ID Date Collected (mm/dd/yy) 1 600 600 500 20 6 70 400 400 15 400 700 10,000 200 5,000 260,000 80,000 50,000 20,000 6,000 70,000 28,500 25,000 15,000 NE NE NE NE TABLE 6 SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS PEELE'S SERVICE STATION (INCIDENT NO. 10000) Date: 02/08/2023 Analytical Method  C9 - C 2 2 A r o m a t i c s MACs (μg/l) Na p h t h a l e n e IP E 1, 2 , 4 - Tr i m e t h y l b e n z e n e 1, 3 , 5 - Tr i m e t h y l b e n z e n e C9 - C 1 8 A l i p h a t i c s C1 9 - C 3 6 A l i p h a t i c s C5 - C 8 A l i p h a t i c s Le a d Facility ID #: 00-0-0000013895 EPA Method 6200B MADEP Methods EPH & VPH Xy l e n e s MT B E GCL (μg/l) Et h y l b e n z e n e Be n z e n e To l u e n e Contaminant of Concern  12/08/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 06/13/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 10/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 04/02/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/30/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 04/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR NR 01/11/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR 07/15/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR 01/11/23 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR 12/08/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 06/13/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 10/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 01/11/23 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 03/01/07 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 <1.00 NR NR NR NR NR NR NR 08/13/07 <1.0 <1.0 <1.0 <3.0 <1.0 1.45 <5 NR NR NR NR NR NR NR 03/12/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <1.0 <0.70 <0.50 NR NR NR NR NR 08/25/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 12/08/11 <0.13 <0.13 <0.15 0.36 J <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 06/13/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR 10/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 0.16 J <0.10 <0.10 <0.10 NR NR NR NR NR 04/02/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/30/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 04/01/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 01/11/23 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR 03/01/07 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 <1.00 NR NR NR NR NR NR NR 08/13/07 <1.0 <1.0 <1.0 <3.0 1.34 <1.0 <5 NR NR NR NR NR NR NR 03/12/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <1.0 <0.70 <0.50 <2.0 <100 <200 <100 <200 08/25/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 12/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 06/13/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 0.21 J <0.10 <0.10 <0.10 NR NR NR NR NR 10/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR 04/02/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/30/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 04/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR NR 01/11/23 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR 06/13/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 10/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 01/11/23 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 03/12/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <1.0 <0.70 <0.50 NR NR NR NR NR 08/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.67 <0.330 <0.330 NR NR NR NR NR 12/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 06/13/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR 10/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR 04/02/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/30/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 04/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR NR 01/11/23 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR 08/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.67 <0.330 <0.330 NR NR NR NR NR 12/08/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 06/13/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 10/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 04/02/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 09/30/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 04/01/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 01/11/23 06/13/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 10/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 04/02/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 09/30/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 04/01/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS WSW-5 Destroyed MW-15 MW-16 MW-17 MW-18 WSW-1 WSW-2 WSW-3 Page 4 of 6 EPA Method 6010B Well ID Date Collected (mm/dd/yy) 1 600 600 500 20 6 70 400 400 15 400 700 10,000 200 5,000 260,000 80,000 50,000 20,000 6,000 70,000 28,500 25,000 15,000 NE NE NE NE TABLE 6 SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS PEELE'S SERVICE STATION (INCIDENT NO. 10000) Date: 02/08/2023 Analytical Method  C9 - C 2 2 A r o m a t i c s MACs (μg/l) Na p h t h a l e n e IP E 1, 2 , 4 - Tr i m e t h y l b e n z e n e 1, 3 , 5 - Tr i m e t h y l b e n z e n e C9 - C 1 8 A l i p h a t i c s C1 9 - C 3 6 A l i p h a t i c s C5 - C 8 A l i p h a t i c s Le a d Facility ID #: 00-0-0000013895 EPA Method 6200B MADEP Methods EPH & VPH Xy l e n e s MT B E GCL (μg/l) Et h y l b e n z e n e Be n z e n e To l u e n e Contaminant of Concern  08/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.67 <0.330 <0.330 NR NR NR NR NR 12/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 06/13/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR 10/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR 04/02/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/30/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 04/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR NR 03/01/07 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 08/13/07 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 <5.0 NR NR NR NR NR NR NR 03/12/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <1.0 <0.70 <0.50 NR NR NR NR NR 08/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.67 <0.330 <0.330 NR NR NR NR NR 12/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 06/13/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR 10/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR 04/02/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/30/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 04/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR NR 03/01/07 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 08/13/07 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 <5 NR NR NR NR NR NR NR 03/12/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <1.0 <0.70 <0.50 NR NR NR NR NR 08/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.67 <0.330 <0.330 NR NR NR NR NR 12/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 06/13/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR 10/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR 04/02/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/30/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 04/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR NR 03/01/07 <0.500 <0.500 <0.500 <1.500 <0.500 <5.00 <0.500 NR <0.500 NR NR NR NR NR 08/13/07 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 03/12/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 08/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.67 <0.330 <0.330 NR NR NR NR NR 12/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 06/13/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR 10/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR 04/02/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/30/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 04/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR NR 01/11/23 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR 06/13/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 10/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 04/02/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 09/30/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 08/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.67 <0.330 <0.330 NR NR NR NR NR 12/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 06/13/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR 03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR 10/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR 04/02/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 09/30/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS 04/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR NR 04/02/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR 05/07/15 <1.0 <5.0 <1.0 <3.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 NR NR NR NR 01/06/16 <1.00 <5.00 <1.00 <3.00 <1.00 <5.00 <1.00 <1.00 <1.00 <1.00 NR NR NR NR 11/02/16 <1.00 <5.00 <1.00 <3.00 <1.00 <5.00 <1.00 <1.00 <1.00 <1.00 NR NR NR NR 07/17/17 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 <1.00 <1.00 <1.00 <1.00 NR NR NR NR 05/22/18 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 <1.00 <1.00 <1.00 <1.00 NR NR NR NR 03/11/19 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 <1.00 <1.00 <1.00 <1.00 NR NR NR NR 01/11/23 WSW-56 WSW-6 WSW-7 WSW-8 WSW-55 Destroyed WSW-41/ DW-3 WSW-62 Page 5 of 6 EPA Method 6010B Well ID Date Collected (mm/dd/yy) 1 600 600 500 20 6 70 400 400 15 400 700 10,000 200 5,000 260,000 80,000 50,000 20,000 6,000 70,000 28,500 25,000 15,000 NE NE NE NE TABLE 6 SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS PEELE'S SERVICE STATION (INCIDENT NO. 10000) Date: 02/08/2023 Analytical Method  C9 - C 2 2 A r o m a t i c s MACs (μg/l) Na p h t h a l e n e IP E 1, 2 , 4 - Tr i m e t h y l b e n z e n e 1, 3 , 5 - Tr i m e t h y l b e n z e n e C9 - C 1 8 A l i p h a t i c s C1 9 - C 3 6 A l i p h a t i c s C5 - C 8 A l i p h a t i c s Le a d Facility ID #: 00-0-0000013895 EPA Method 6200B MADEP Methods EPH & VPH Xy l e n e s MT B E GCL (μg/l) Et h y l b e n z e n e Be n z e n e To l u e n e Contaminant of Concern  05/07/15 <1.0 <5.0 <1.0 <3.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 NR NR NR NR 01/06/16 <1.00 <5.00 <1.00 <3.00 <1.00 <5.00 <1.00 <1.00 <1.00 <1.00 NR NR NR NR 11/02/16 <1.00 <5.00 <1.00 <3.00 <1.00 <5.00 <1.00 <1.00 <1.00 <1.00 NR NR NR NR 07/17/17 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 <1.00 <1.00 <1.00 <1.00 NR NR NR NR 05/22/18 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 <1.00 <1.00 <1.00 <1.00 NR NR NR NR 03/11/19 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 <1.00 <1.00 <1.00 <1.00 NR NR NR NR 12/14/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR 01/11/23 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR Notes: • Results reported in µg/L (micrograms per liter). • NS: Not sampled; well dry, insufficient water to sample or not located. • NE: Standard not established. • For other compounds reported which did not exceed the 2L Standards, refer to the laboratory reports. • I or J: Estimated value between the MDL and PQL . • Concentrations in bold face type exceeded the 2L standard. • < : Less than the method detection limit specified in the laboratory report. • NR : Analysis not requested. • 2L Standard : Maximum allowable concentrations as specified in T15A NCAC 2L.0202. • GCL : Gross contamination level as specified in T15A NCAC 2L.0202. Trip Blank Page 6 of 6 APPENDICES APPENDIX A State Correspondence ROY COOPER Governor ELIZABETH S. BISER Secretary MICHAEL SCOTT Director North Carolina Department of Environmental Quality | Division of Waste Management | UST Section Washington Regional Office | 943 Washington Square Mall | Washington, NC 27889 | (252) 946-6481 January 25, 2022 North East Oil Company, Inc. ATTN: Ms. Bea Harrison Post Office Box 1386 Ahoskie, North Carolina 27910 Re: Notice of Regulatory Requirements 15A NCAC 2L .0407 Risk-based Assessment and Corrective Action for Petroleum Underground Storage Tanks Acknowledgement of Report Receipt Peele’s Service Station 2675 Old US Highway 64, Jamesville Martin County Incident Number: 10000 Risk Classification: High Ranking: H 405 R Dear Ms. Harrison: The Division of Waste Management (DWM) Underground Storage Tank (UST) Section received the Groundwater Monitoring Report dated January 20, 2022. The report has been reviewed and will be maintained in the Washington Regional Office. The report indicates continued levels of groundwater contamination. The subject incident has been determined by the Department, in response to North Carolina General Statute (NCGS) 143-215.94E(e4), to be of sufficiently high priority to allow funding by the State Trust Fund Program. Therefore, you are directed to proceed with assessment. Specifically, you are required to: · Continue to monitor groundwater quality on an annual schedule. Submit the results of the groundwater sampling activities in a monitoring report to this office within 30 days of receiving the analytical results. · During the next monitoring event, conduct a comprehensive sampling of monitoring wells and water supply wells and perform a Contamination Fate and Transport Model. Effective October 1, 2004, the Department requires that all work following the submittal of the Limited Site Assessment Report (Title 15A NCAC 2L .0405) be preapproved if State Trust Fund reimbursement is anticipated. To comply with this requirement, a completed Preapproval/Claim Authorization Form, encompassing the required remedial activities, must be received in this office within 14 days of the date of this letter. Upon completion of the preapproved activities, you should submit your claim promptly. Reimbursement funds are budgeted based on completed preapprovals, but lengthy delays in reimbursement can occur if claims are not submitted immediately following work completion. 2516 Received JAN 25 2022 Because a release or discharge has been confirmed, a Licensed Geologist or a Professional Engineer, certified by the State of North Carolina, is required to prepare and certify all reports submitted to the Department in accordance with Title 15A NCAC 2L .0103(e) and 2L .0111(b). Please note that before you sell, transfer, or request a “No Further Action” determination for a property that has not been remediated to below “unrestricted use” standards, you must file a Notice of Residual Petroleum ("Notice") with the Register of Deeds in the county where the property is located (NCGS 143B-279.9 and 143B-279.11). Failure to comply with the State's rules in the manner and time specified may result in the assessment of civil penalties and/or the use of other enforcement mechanisms. If you have any questions regarding the actions or the rules mentioned in this letter, please contact me at the address or telephone number listed below. If you have any questions regarding trust fund eligibility or reimbursement, please contact the UST Section Trust Fund Branch at (919) 733-8486. Sincerely, Allison Ward Hydrogeologist Washington Regional Office cc: GRI, William Regenthal, P.G.via email Simonsen Law Firm, Mr. Lars Simonsen, PO Box 848, Edenton, NC WaRO 2516 Received JAN 04 2023 APPENDIX B Laboratory Report – Ground Water Samples 01/19/23 Technical Report for GRI (Geological Resources Inc.) Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC 2516 SGS Job Number: FC1878 Sampling Date: 01/11/23 Report to: GRI 3502 Hayes Rd Monroe, NC 28110 carriekennedy@geologicalresourcesinc.com; jjr@geologicalresourcesinc.com; wlr@geologicalresourcesinc.com ATTN: William Regenthall Total number of pages in report: Certifications: FL(E83510), LA(03051), KS(E-10327), NC(573), NJ(FL002), NY(12022), SC(96038001) DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177), AL, AK, AR, CT, IA, KY, MA, MI. MS, ND, NH, NV, OK, OR, IL, UT, VT, WA, WI, WV This report shall not be reproduced, except in its entirety, without the written approval of SGS. Test results relate only to samples analyzed. SGS North America Inc. 4405 Vineland Road Suite C-15 Orlando, FL 32811 tel: 407-425-6700 fax: 407-425-0707 Test results contained within this data package meet the requirements of the National Environmental Laboratory Accreditation Program and/or state specific certification programs as applicable. Client Service contact: Muna Mohammed 407-425-6700 Norm Farmer Technical Director Orlando, FL 01/19/23 e-Hardcopy 2.0 Automated Report 44 SGS is the sole authority for authorizing edits or modifications to this document. Unauthorized modification of this report is strictly prohibited. Review standard terms at: http://www.sgs.com/en/terms-and-conditions The results set forth herein are provided by SGS North America Inc. Please share your ideas about how we can serve you better at: EHS.US.CustomerCare@sgs.com 1 of 44 FC1878 Table of Contents -1- Sections: Section 1: Sample Summary ...................................................................................................3 Section 2: Summary of Hits ....................................................................................................4 Section 3: Sample Results ........................................................................................................6 3.1: FC1878-1: TRIP BLANK .............................................................................................7 3.2: FC1878-2: MW-18 ........................................................................................................9 3.3: FC1878-3: MW-17 ........................................................................................................11 3.4: FC1878-4: MW-15 ........................................................................................................13 3.5: FC1878-5: MW-11 ........................................................................................................15 3.6: FC1878-6: MW-9 ..........................................................................................................17 3.7: FC1878-7: MW-1 ..........................................................................................................19 3.8: FC1878-8: MW-2R .......................................................................................................21 3.9: FC1878-9: MW-5 ..........................................................................................................23 3.10: FC1878-10: WSW-41 .................................................................................................25 3.11: FC1878-11: WSW-2 ....................................................................................................27 Section 4: Misc. Forms ............................................................................................................29 4.1: Chain of Custody ...........................................................................................................30 Section 5: MS Volatiles - QC Data Summaries .....................................................................32 5.1: Method Blank Summary ................................................................................................33 5.2: Blank Spike Summary ...................................................................................................37 5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................41 1 2 3 4 5 2 of 44 FC1878 SGS North America Inc. Sample Summary GRI (Geological Resources Inc.) Job No:FC1878 Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC Project No: 2516 Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID This report contains results reported as ND = Not detected. The following applies: Organics ND = Not detected above the MDL FC1878-1 01/11/23 08:08 JB 01/13/23 AQ Trip Blank Water TRIP BLANK FC1878-2 01/11/23 09:54 JB 01/13/23 AQ Ground Water MW-18 FC1878-3 01/11/23 10:12 JB 01/13/23 AQ Ground Water MW-17 FC1878-4 01/11/23 10:26 JB 01/13/23 AQ Ground Water MW-15 FC1878-5 01/11/23 10:41 JB 01/13/23 AQ Ground Water MW-11 FC1878-6 01/11/23 10:52 JB 01/13/23 AQ Ground Water MW-9 FC1878-7 01/11/23 11:05 JB 01/13/23 AQ Ground Water MW-1 FC1878-8 01/11/23 11:16 JB 01/13/23 AQ Ground Water MW-2R FC1878-9 01/11/23 11:33 JB 01/13/23 AQ Ground Water MW-5 FC1878-10 01/11/23 11:40 JB 01/13/23 AQ Ground Water WSW-41 FC1878-11 01/11/23 11:47 JB 01/13/23 AQ Ground Water WSW-2 3 of 44 FC1878 1 Summary of Hits Page 1 of 2 Job Number:FC1878 Account:GRI (Geological Resources Inc.) Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC Collected:01/11/23 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method FC1878-1 TRIP BLANK No hits reported in this sample. FC1878-2 MW-18 No hits reported in this sample. FC1878-3 MW-17 No hits reported in this sample. FC1878-4 MW-15 No hits reported in this sample. FC1878-5 MW-11 Benzene 7.6 0.50 0.13 ug/l SM 6200B n-Butylbenzene 3.3 0.50 0.13 ug/l SM 6200B sec-Butylbenzene 4.9 0.50 0.13 ug/l SM 6200B tert-Butylbenzene 0.21 J 0.50 0.13 ug/l SM 6200B Chloroethane 0.35 J 0.50 0.20 ug/l SM 6200B Ethylbenzene 5.3 0.50 0.13 ug/l SM 6200B Isopropylbenzene 7.9 0.50 0.13 ug/l SM 6200B p-Isopropyltoluene 1.4 0.50 0.13 ug/l SM 6200B Methyl Chloride 0.21 J 0.50 0.20 ug/l SM 6200B Naphthalene 38.6 0.50 0.13 ug/l SM 6200B n-Propylbenzene 10.8 0.50 0.13 ug/l SM 6200B 1,2,4-Trimethylbenzene 12.4 0.50 0.13 ug/l SM 6200B 1,3,5-Trimethylbenzene 0.52 0.50 0.13 ug/l SM 6200B m,p-Xylene 1.9 1.0 0.13 ug/l SM 6200B Xylene (total)2.0 1.5 0.25 ug/l SM 6200B FC1878-6 MW-9 No hits reported in this sample. FC1878-7 MW-1 Benzene 4.6 0.50 0.13 ug/l SM 6200B n-Butylbenzene 1.2 0.50 0.13 ug/l SM 6200B sec-Butylbenzene 3.2 0.50 0.13 ug/l SM 6200B tert-Butylbenzene 0.16 J 0.50 0.13 ug/l SM 6200B Ethylbenzene 6.4 0.50 0.13 ug/l SM 6200B 4 of 44 FC1878 2 Summary of Hits Page 2 of 2 Job Number:FC1878 Account:GRI (Geological Resources Inc.) Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC Collected:01/11/23 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method Isopropylbenzene 2.5 0.50 0.13 ug/l SM 6200B p-Isopropyltoluene 0.63 0.50 0.13 ug/l SM 6200B Naphthalene 16.9 0.50 0.13 ug/l SM 6200B n-Propylbenzene 3.6 0.50 0.13 ug/l SM 6200B Toluene 0.76 0.50 0.13 ug/l SM 6200B 1,2,4-Trimethylbenzene 8.5 0.50 0.13 ug/l SM 6200B 1,3,5-Trimethylbenzene 0.39 J 0.50 0.13 ug/l SM 6200B m,p-Xylene 2.2 1.0 0.13 ug/l SM 6200B o-Xylene 1.4 0.50 0.13 ug/l SM 6200B Xylene (total)3.6 1.5 0.25 ug/l SM 6200B FC1878-8 MW-2R Benzene 74.1 13 3.1 ug/l SM 6200B Ethylbenzene 21.2 13 3.1 ug/l SM 6200B Naphthalene 8.8 J 13 3.1 ug/l SM 6200B Toluene 88.2 13 3.1 ug/l SM 6200B 1,2,4-Trimethylbenzene 160 13 3.1 ug/l SM 6200B 1,3,5-Trimethylbenzene 60.1 13 3.1 ug/l SM 6200B m,p-Xylene 540 25 3.1 ug/l SM 6200B o-Xylene 735 13 3.1 ug/l SM 6200B Xylene (total)1270 38 6.3 ug/l SM 6200B FC1878-9 MW-5 No hits reported in this sample. FC1878-10 WSW-41 Trichloroethylene 0.29 J 0.50 0.13 ug/l SM 6200B FC1878-11 WSW-2 No hits reported in this sample. 5 of 44 FC1878 2 SGS North America Inc. Sample Results Report of Analysis Orlando, FL Section 3 6 of 44 FC1878 3 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID:TRIP BLANK Lab Sample ID:FC1878-1 Date Sampled:01/11/23 Matrix:AQ - Trip Blank Water Date Received:01/13/23 Method:SM 6200B Percent Solids:n/a Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 E110927.D 1 01/16/23 12:34 KW n/a n/a VE2639 Run #2 Purge Volume Run #1 10.0 ml Run #2 VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.13 ug/l 108-86-1 Bromobenzene ND 0.50 0.13 ug/l 74-97-5 Bromochloromethane ND 0.50 0.13 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l 75-25-2 Bromoform ND 0.50 0.13 ug/l 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane ND 0.50 0.20 ug/l 67-66-3 Chloroform ND 0.50 0.13 ug/l 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l 75-71-8 Dichlorodifluoromethane a ND 0.50 0.20 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l 75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l 563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 7 of 44 FC1878 3 3. 1 SGS North America Inc. Report of Analysis Page 2 of 2 Client Sample ID:TRIP BLANK Lab Sample ID:FC1878-1 Date Sampled:01/11/23 Matrix:AQ - Trip Blank Water Date Received:01/13/23 Method:SM 6200B Percent Solids:n/a Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l 100-41-4 Ethylbenzene ND 0.50 0.13 ug/l 87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l 74-83-9 Methyl Bromide ND 0.50 0.20 ug/l 74-87-3 Methyl Chloride ND 0.50 0.20 ug/l 74-95-3 Methylene Bromide ND 0.50 0.13 ug/l 75-09-2 Methylene Chloride ND 2.0 1.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l 91-20-3 Naphthalene ND 0.50 0.13 ug/l 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l 100-42-5 Styrene ND 0.50 0.13 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l 108-88-3 Toluene ND 0.50 0.13 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l 71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l 79-01-6 Trichloroethylene ND 0.50 0.13 ug/l 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l m,p-Xylene ND 1.0 0.13 ug/l 95-47-6 o-Xylene ND 0.50 0.13 ug/l 1330-20-7 Xylene (total)ND 1.5 0.25 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 96%70-130% 17060-07-0 1,2-Dichloroethane-D4 101%70-130% 2037-26-5 Toluene-D8 105%70-130% 460-00-4 4-Bromofluorobenzene 107%70-130% (a) Associated ECC outside of control limits high, sample is ND. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 8 of 44 FC1878 3 3. 1 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID:MW-18 Lab Sample ID:FC1878-2 Date Sampled:01/11/23 Matrix:AQ - Ground Water Date Received:01/13/23 Method:SM 6200B Percent Solids:n/a Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 E110928.D 1 01/16/23 12:56 KW n/a n/a VE2639 Run #2 Purge Volume Run #1 10.0 ml Run #2 VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.13 ug/l 108-86-1 Bromobenzene ND 0.50 0.13 ug/l 74-97-5 Bromochloromethane ND 0.50 0.13 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l 75-25-2 Bromoform ND 0.50 0.13 ug/l 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane ND 0.50 0.20 ug/l 67-66-3 Chloroform ND 0.50 0.13 ug/l 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l 75-71-8 Dichlorodifluoromethane a ND 0.50 0.20 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l 75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l 563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 9 of 44 FC1878 3 3. 2 SGS North America Inc. Report of Analysis Page 2 of 2 Client Sample ID:MW-18 Lab Sample ID:FC1878-2 Date Sampled:01/11/23 Matrix:AQ - Ground Water Date Received:01/13/23 Method:SM 6200B Percent Solids:n/a Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l 100-41-4 Ethylbenzene ND 0.50 0.13 ug/l 87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l 74-83-9 Methyl Bromide ND 0.50 0.20 ug/l 74-87-3 Methyl Chloride ND 0.50 0.20 ug/l 74-95-3 Methylene Bromide ND 0.50 0.13 ug/l 75-09-2 Methylene Chloride ND 2.0 1.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l 91-20-3 Naphthalene ND 0.50 0.13 ug/l 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l 100-42-5 Styrene ND 0.50 0.13 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l 108-88-3 Toluene ND 0.50 0.13 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l 71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l 79-01-6 Trichloroethylene ND 0.50 0.13 ug/l 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l m,p-Xylene ND 1.0 0.13 ug/l 95-47-6 o-Xylene ND 0.50 0.13 ug/l 1330-20-7 Xylene (total)ND 1.5 0.25 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 97%70-130% 17060-07-0 1,2-Dichloroethane-D4 103%70-130% 2037-26-5 Toluene-D8 105%70-130% 460-00-4 4-Bromofluorobenzene 109%70-130% (a) Associated ECC outside of control limits high, sample is ND. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 10 of 44 FC1878 3 3. 2 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID:MW-17 Lab Sample ID:FC1878-3 Date Sampled:01/11/23 Matrix:AQ - Ground Water Date Received:01/13/23 Method:SM 6200B Percent Solids:n/a Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 E110929.D 1 01/16/23 13:20 KW n/a n/a VE2639 Run #2 Purge Volume Run #1 10.0 ml Run #2 VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.13 ug/l 108-86-1 Bromobenzene ND 0.50 0.13 ug/l 74-97-5 Bromochloromethane ND 0.50 0.13 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l 75-25-2 Bromoform ND 0.50 0.13 ug/l 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane ND 0.50 0.20 ug/l 67-66-3 Chloroform ND 0.50 0.13 ug/l 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l 75-71-8 Dichlorodifluoromethane a ND 0.50 0.20 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l 75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l 563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 11 of 44 FC1878 3 3. 3 SGS North America Inc. Report of Analysis Page 2 of 2 Client Sample ID:MW-17 Lab Sample ID:FC1878-3 Date Sampled:01/11/23 Matrix:AQ - Ground Water Date Received:01/13/23 Method:SM 6200B Percent Solids:n/a Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l 100-41-4 Ethylbenzene ND 0.50 0.13 ug/l 87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l 74-83-9 Methyl Bromide ND 0.50 0.20 ug/l 74-87-3 Methyl Chloride ND 0.50 0.20 ug/l 74-95-3 Methylene Bromide ND 0.50 0.13 ug/l 75-09-2 Methylene Chloride ND 2.0 1.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l 91-20-3 Naphthalene ND 0.50 0.13 ug/l 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l 100-42-5 Styrene ND 0.50 0.13 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l 108-88-3 Toluene ND 0.50 0.13 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l 71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l 79-01-6 Trichloroethylene ND 0.50 0.13 ug/l 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l m,p-Xylene ND 1.0 0.13 ug/l 95-47-6 o-Xylene ND 0.50 0.13 ug/l 1330-20-7 Xylene (total)ND 1.5 0.25 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 95%70-130% 17060-07-0 1,2-Dichloroethane-D4 104%70-130% 2037-26-5 Toluene-D8 104%70-130% 460-00-4 4-Bromofluorobenzene 109%70-130% (a) Associated ECC outside of control limits high, sample is ND. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 12 of 44 FC1878 3 3. 3 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID:MW-15 Lab Sample ID:FC1878-4 Date Sampled:01/11/23 Matrix:AQ - Ground Water Date Received:01/13/23 Method:SM 6200B Percent Solids:n/a Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 E110930.D 1 01/16/23 13:43 KW n/a n/a VE2639 Run #2 Purge Volume Run #1 10.0 ml Run #2 VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.13 ug/l 108-86-1 Bromobenzene ND 0.50 0.13 ug/l 74-97-5 Bromochloromethane ND 0.50 0.13 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l 75-25-2 Bromoform ND 0.50 0.13 ug/l 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane ND 0.50 0.20 ug/l 67-66-3 Chloroform ND 0.50 0.13 ug/l 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l 75-71-8 Dichlorodifluoromethane a ND 0.50 0.20 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l 75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l 563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 13 of 44 FC1878 3 3. 4 SGS North America Inc. Report of Analysis Page 2 of 2 Client Sample ID:MW-15 Lab Sample ID:FC1878-4 Date Sampled:01/11/23 Matrix:AQ - Ground Water Date Received:01/13/23 Method:SM 6200B Percent Solids:n/a Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l 100-41-4 Ethylbenzene ND 0.50 0.13 ug/l 87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l 74-83-9 Methyl Bromide ND 0.50 0.20 ug/l 74-87-3 Methyl Chloride ND 0.50 0.20 ug/l 74-95-3 Methylene Bromide ND 0.50 0.13 ug/l 75-09-2 Methylene Chloride ND 2.0 1.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l 91-20-3 Naphthalene ND 0.50 0.13 ug/l 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l 100-42-5 Styrene ND 0.50 0.13 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l 108-88-3 Toluene ND 0.50 0.13 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l 71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l 79-01-6 Trichloroethylene ND 0.50 0.13 ug/l 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l m,p-Xylene ND 1.0 0.13 ug/l 95-47-6 o-Xylene ND 0.50 0.13 ug/l 1330-20-7 Xylene (total)ND 1.5 0.25 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 97%70-130% 17060-07-0 1,2-Dichloroethane-D4 107%70-130% 2037-26-5 Toluene-D8 100%70-130% 460-00-4 4-Bromofluorobenzene 109%70-130% (a) Associated ECC outside of control limits high, sample is ND. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 14 of 44 FC1878 3 3. 4 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID:MW-11 Lab Sample ID:FC1878-5 Date Sampled:01/11/23 Matrix:AQ - Ground Water Date Received:01/13/23 Method:SM 6200B Percent Solids:n/a Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 E110972.D 1 01/17/23 18:35 KW n/a n/a VE2640 Run #2 Purge Volume Run #1 10.0 ml Run #2 VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene 7.6 0.50 0.13 ug/l 108-86-1 Bromobenzene ND 0.50 0.13 ug/l 74-97-5 Bromochloromethane ND 0.50 0.13 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l 75-25-2 Bromoform ND 0.50 0.13 ug/l 104-51-8 n-Butylbenzene 3.3 0.50 0.13 ug/l 135-98-8 sec-Butylbenzene 4.9 0.50 0.13 ug/l 98-06-6 tert-Butylbenzene 0.21 0.50 0.13 ug/l J 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane 0.35 0.50 0.20 ug/l J 67-66-3 Chloroform ND 0.50 0.13 ug/l 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l 75-71-8 Dichlorodifluoromethane a ND 0.50 0.20 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l 75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l 563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 15 of 44 FC1878 3 3. 5 SGS North America Inc. Report of Analysis Page 2 of 2 Client Sample ID:MW-11 Lab Sample ID:FC1878-5 Date Sampled:01/11/23 Matrix:AQ - Ground Water Date Received:01/13/23 Method:SM 6200B Percent Solids:n/a Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l 100-41-4 Ethylbenzene 5.3 0.50 0.13 ug/l 87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l 98-82-8 Isopropylbenzene 7.9 0.50 0.13 ug/l 99-87-6 p-Isopropyltoluene 1.4 0.50 0.13 ug/l 74-83-9 Methyl Bromide ND 0.50 0.20 ug/l 74-87-3 Methyl Chloride 0.21 0.50 0.20 ug/l J 74-95-3 Methylene Bromide ND 0.50 0.13 ug/l 75-09-2 Methylene Chloride ND 2.0 1.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l 91-20-3 Naphthalene 38.6 0.50 0.13 ug/l 103-65-1 n-Propylbenzene 10.8 0.50 0.13 ug/l 100-42-5 Styrene ND 0.50 0.13 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l 108-88-3 Toluene ND 0.50 0.13 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l 71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l 79-01-6 Trichloroethylene ND 0.50 0.13 ug/l 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l 95-63-6 1,2,4-Trimethylbenzene 12.4 0.50 0.13 ug/l 108-67-8 1,3,5-Trimethylbenzene 0.52 0.50 0.13 ug/l 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l m,p-Xylene 1.9 1.0 0.13 ug/l 95-47-6 o-Xylene ND 0.50 0.13 ug/l 1330-20-7 Xylene (total)2.0 1.5 0.25 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 98%70-130% 17060-07-0 1,2-Dichloroethane-D4 104%70-130% 2037-26-5 Toluene-D8 95%70-130% 460-00-4 4-Bromofluorobenzene 109%70-130% (a) Associated CCV outside control limits high, sample is ND. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 16 of 44 FC1878 3 3. 5 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID:MW-9 Lab Sample ID:FC1878-6 Date Sampled:01/11/23 Matrix:AQ - Ground Water Date Received:01/13/23 Method:SM 6200B Percent Solids:n/a Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 E110974.D 1 01/17/23 19:21 KW n/a n/a VE2640 Run #2 Purge Volume Run #1 10.0 ml Run #2 VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.13 ug/l 108-86-1 Bromobenzene ND 0.50 0.13 ug/l 74-97-5 Bromochloromethane ND 0.50 0.13 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l 75-25-2 Bromoform ND 0.50 0.13 ug/l 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane ND 0.50 0.20 ug/l 67-66-3 Chloroform ND 0.50 0.13 ug/l 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l 75-71-8 Dichlorodifluoromethane a ND 0.50 0.20 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l 75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l 563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 17 of 44 FC1878 3 3. 6 SGS North America Inc. Report of Analysis Page 2 of 2 Client Sample ID:MW-9 Lab Sample ID:FC1878-6 Date Sampled:01/11/23 Matrix:AQ - Ground Water Date Received:01/13/23 Method:SM 6200B Percent Solids:n/a Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l 100-41-4 Ethylbenzene ND 0.50 0.13 ug/l 87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l 74-83-9 Methyl Bromide ND 0.50 0.20 ug/l 74-87-3 Methyl Chloride ND 0.50 0.20 ug/l 74-95-3 Methylene Bromide ND 0.50 0.13 ug/l 75-09-2 Methylene Chloride ND 2.0 1.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l 91-20-3 Naphthalene ND 0.50 0.13 ug/l 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l 100-42-5 Styrene ND 0.50 0.13 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l 108-88-3 Toluene ND 0.50 0.13 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l 71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l 79-01-6 Trichloroethylene ND 0.50 0.13 ug/l 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l m,p-Xylene ND 1.0 0.13 ug/l 95-47-6 o-Xylene ND 0.50 0.13 ug/l 1330-20-7 Xylene (total)ND 1.5 0.25 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 96%70-130% 17060-07-0 1,2-Dichloroethane-D4 101%70-130% 2037-26-5 Toluene-D8 101%70-130% 460-00-4 4-Bromofluorobenzene 110%70-130% (a) Associated CCV outside control limits high, sample is ND. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 18 of 44 FC1878 3 3. 6 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID:MW-1 Lab Sample ID:FC1878-7 Date Sampled:01/11/23 Matrix:AQ - Ground Water Date Received:01/13/23 Method:SM 6200B Percent Solids:n/a Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 E110975.D 1 01/17/23 19:43 KW n/a n/a VE2640 Run #2 Purge Volume Run #1 10.0 ml Run #2 VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene 4.6 0.50 0.13 ug/l 108-86-1 Bromobenzene ND 0.50 0.13 ug/l 74-97-5 Bromochloromethane ND 0.50 0.13 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l 75-25-2 Bromoform ND 0.50 0.13 ug/l 104-51-8 n-Butylbenzene 1.2 0.50 0.13 ug/l 135-98-8 sec-Butylbenzene 3.2 0.50 0.13 ug/l 98-06-6 tert-Butylbenzene 0.16 0.50 0.13 ug/l J 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane ND 0.50 0.20 ug/l 67-66-3 Chloroform ND 0.50 0.13 ug/l 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l 75-71-8 Dichlorodifluoromethane a ND 0.50 0.20 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l 75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l 563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 19 of 44 FC1878 3 3. 7 SGS North America Inc. Report of Analysis Page 2 of 2 Client Sample ID:MW-1 Lab Sample ID:FC1878-7 Date Sampled:01/11/23 Matrix:AQ - Ground Water Date Received:01/13/23 Method:SM 6200B Percent Solids:n/a Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l 100-41-4 Ethylbenzene 6.4 0.50 0.13 ug/l 87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l 98-82-8 Isopropylbenzene 2.5 0.50 0.13 ug/l 99-87-6 p-Isopropyltoluene 0.63 0.50 0.13 ug/l 74-83-9 Methyl Bromide ND 0.50 0.20 ug/l 74-87-3 Methyl Chloride ND 0.50 0.20 ug/l 74-95-3 Methylene Bromide ND 0.50 0.13 ug/l 75-09-2 Methylene Chloride ND 2.0 1.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l 91-20-3 Naphthalene 16.9 0.50 0.13 ug/l 103-65-1 n-Propylbenzene 3.6 0.50 0.13 ug/l 100-42-5 Styrene ND 0.50 0.13 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l 108-88-3 Toluene 0.76 0.50 0.13 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l 71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l 79-01-6 Trichloroethylene ND 0.50 0.13 ug/l 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l 95-63-6 1,2,4-Trimethylbenzene 8.5 0.50 0.13 ug/l 108-67-8 1,3,5-Trimethylbenzene 0.39 0.50 0.13 ug/l J 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l m,p-Xylene 2.2 1.0 0.13 ug/l 95-47-6 o-Xylene 1.4 0.50 0.13 ug/l 1330-20-7 Xylene (total)3.6 1.5 0.25 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 96%70-130% 17060-07-0 1,2-Dichloroethane-D4 104%70-130% 2037-26-5 Toluene-D8 96%70-130% 460-00-4 4-Bromofluorobenzene 108%70-130% (a) Associated CCV outside control limits high, sample is ND. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 20 of 44 FC1878 3 3. 7 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID:MW-2R Lab Sample ID:FC1878-8 Date Sampled:01/11/23 Matrix:AQ - Ground Water Date Received:01/13/23 Method:SM 6200B Percent Solids:n/a Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 E110976.D 25 01/17/23 20:06 KW n/a n/a VE2640 Run #2 Purge Volume Run #1 10.0 ml Run #2 VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene 74.1 13 3.1 ug/l 108-86-1 Bromobenzene ND 13 3.1 ug/l 74-97-5 Bromochloromethane ND 13 3.1 ug/l 75-27-4 Bromodichloromethane ND 13 3.1 ug/l 75-25-2 Bromoform ND 13 3.1 ug/l 104-51-8 n-Butylbenzene ND 13 3.1 ug/l 135-98-8 sec-Butylbenzene ND 13 3.1 ug/l 98-06-6 tert-Butylbenzene ND 13 3.1 ug/l 56-23-5 Carbon Tetrachloride ND 13 3.1 ug/l 108-90-7 Chlorobenzene ND 13 3.1 ug/l 75-00-3 Chloroethane ND 13 5.0 ug/l 67-66-3 Chloroform ND 13 3.1 ug/l 95-49-8 o-Chlorotoluene ND 13 3.1 ug/l 106-43-4 p-Chlorotoluene ND 13 3.1 ug/l 124-48-1 Dibromochloromethane ND 13 3.1 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 13 6.2 ug/l 106-93-4 1,2-Dibromoethane ND 13 3.1 ug/l 75-71-8 Dichlorodifluoromethane a ND 13 5.0 ug/l 95-50-1 1,2-Dichlorobenzene ND 13 3.1 ug/l 541-73-1 1,3-Dichlorobenzene ND 13 3.1 ug/l 106-46-7 1,4-Dichlorobenzene ND 13 3.1 ug/l 75-34-3 1,1-Dichloroethane ND 13 3.1 ug/l 107-06-2 1,2-Dichloroethane ND 13 3.1 ug/l 75-35-4 1,1-Dichloroethylene ND 13 3.1 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 13 3.1 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 13 3.1 ug/l 78-87-5 1,2-Dichloropropane ND 13 3.1 ug/l 142-28-9 1,3-Dichloropropane ND 13 3.1 ug/l 594-20-7 2,2-Dichloropropane ND 13 3.1 ug/l 563-58-6 1,1-Dichloropropene ND 13 3.1 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 13 3.1 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 13 3.1 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 21 of 44 FC1878 3 3. 8 SGS North America Inc. Report of Analysis Page 2 of 2 Client Sample ID:MW-2R Lab Sample ID:FC1878-8 Date Sampled:01/11/23 Matrix:AQ - Ground Water Date Received:01/13/23 Method:SM 6200B Percent Solids:n/a Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether ND 13 3.1 ug/l 100-41-4 Ethylbenzene 21.2 13 3.1 ug/l 87-68-3 Hexachlorobutadiene ND 13 3.1 ug/l 98-82-8 Isopropylbenzene ND 13 3.1 ug/l 99-87-6 p-Isopropyltoluene ND 13 3.1 ug/l 74-83-9 Methyl Bromide ND 13 5.0 ug/l 74-87-3 Methyl Chloride ND 13 5.0 ug/l 74-95-3 Methylene Bromide ND 13 3.1 ug/l 75-09-2 Methylene Chloride ND 50 25 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 13 3.1 ug/l 91-20-3 Naphthalene 8.8 13 3.1 ug/l J 103-65-1 n-Propylbenzene ND 13 3.1 ug/l 100-42-5 Styrene ND 13 3.1 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 13 3.1 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 13 3.1 ug/l 127-18-4 Tetrachloroethylene ND 13 3.1 ug/l 108-88-3 Toluene 88.2 13 3.1 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 13 3.1 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 13 3.1 ug/l 71-55-6 1,1,1-Trichloroethane ND 13 3.1 ug/l 79-00-5 1,1,2-Trichloroethane ND 13 3.1 ug/l 79-01-6 Trichloroethylene ND 13 3.1 ug/l 75-69-4 Trichlorofluoromethane ND 13 5.0 ug/l 96-18-4 1,2,3-Trichloropropane ND 13 3.1 ug/l 95-63-6 1,2,4-Trimethylbenzene 160 13 3.1 ug/l 108-67-8 1,3,5-Trimethylbenzene 60.1 13 3.1 ug/l 75-01-4 Vinyl Chloride ND 13 3.1 ug/l m,p-Xylene 540 25 3.1 ug/l 95-47-6 o-Xylene 735 13 3.1 ug/l 1330-20-7 Xylene (total)1270 38 6.3 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 95%70-130% 17060-07-0 1,2-Dichloroethane-D4 101%70-130% 2037-26-5 Toluene-D8 102%70-130% 460-00-4 4-Bromofluorobenzene 110%70-130% (a) Associated CCV outside control limits high, sample is ND. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 22 of 44 FC1878 3 3. 8 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID:MW-5 Lab Sample ID:FC1878-9 Date Sampled:01/11/23 Matrix:AQ - Ground Water Date Received:01/13/23 Method:SM 6200B Percent Solids:n/a Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 E110977.D 1 01/17/23 20:28 KW n/a n/a VE2640 Run #2 Purge Volume Run #1 10.0 ml Run #2 VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.13 ug/l 108-86-1 Bromobenzene ND 0.50 0.13 ug/l 74-97-5 Bromochloromethane ND 0.50 0.13 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l 75-25-2 Bromoform ND 0.50 0.13 ug/l 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane ND 0.50 0.20 ug/l 67-66-3 Chloroform ND 0.50 0.13 ug/l 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l 75-71-8 Dichlorodifluoromethane a ND 0.50 0.20 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l 75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l 563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 23 of 44 FC1878 3 3. 9 SGS North America Inc. Report of Analysis Page 2 of 2 Client Sample ID:MW-5 Lab Sample ID:FC1878-9 Date Sampled:01/11/23 Matrix:AQ - Ground Water Date Received:01/13/23 Method:SM 6200B Percent Solids:n/a Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l 100-41-4 Ethylbenzene ND 0.50 0.13 ug/l 87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l 74-83-9 Methyl Bromide ND 0.50 0.20 ug/l 74-87-3 Methyl Chloride ND 0.50 0.20 ug/l 74-95-3 Methylene Bromide ND 0.50 0.13 ug/l 75-09-2 Methylene Chloride ND 2.0 1.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l 91-20-3 Naphthalene ND 0.50 0.13 ug/l 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l 100-42-5 Styrene ND 0.50 0.13 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l 108-88-3 Toluene ND 0.50 0.13 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l 71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l 79-01-6 Trichloroethylene ND 0.50 0.13 ug/l 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l m,p-Xylene ND 1.0 0.13 ug/l 95-47-6 o-Xylene ND 0.50 0.13 ug/l 1330-20-7 Xylene (total)ND 1.5 0.25 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 96%70-130% 17060-07-0 1,2-Dichloroethane-D4 104%70-130% 2037-26-5 Toluene-D8 100%70-130% 460-00-4 4-Bromofluorobenzene 110%70-130% (a) Associated CCV outside control limits high, sample is ND. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 24 of 44 FC1878 3 3. 9 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID:WSW-41 Lab Sample ID:FC1878-10 Date Sampled:01/11/23 Matrix:AQ - Ground Water Date Received:01/13/23 Method:SM 6200B Percent Solids:n/a Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 E110978.D 1 01/17/23 20:51 KW n/a n/a VE2640 Run #2 Purge Volume Run #1 10.0 ml Run #2 VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.13 ug/l 108-86-1 Bromobenzene ND 0.50 0.13 ug/l 74-97-5 Bromochloromethane ND 0.50 0.13 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l 75-25-2 Bromoform ND 0.50 0.13 ug/l 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane ND 0.50 0.20 ug/l 67-66-3 Chloroform ND 0.50 0.13 ug/l 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l 75-71-8 Dichlorodifluoromethane a ND 0.50 0.20 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l 75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l 563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 25 of 44 FC1878 3 3. 1 0 SGS North America Inc. Report of Analysis Page 2 of 2 Client Sample ID:WSW-41 Lab Sample ID:FC1878-10 Date Sampled:01/11/23 Matrix:AQ - Ground Water Date Received:01/13/23 Method:SM 6200B Percent Solids:n/a Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l 100-41-4 Ethylbenzene ND 0.50 0.13 ug/l 87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l 74-83-9 Methyl Bromide ND 0.50 0.20 ug/l 74-87-3 Methyl Chloride ND 0.50 0.20 ug/l 74-95-3 Methylene Bromide ND 0.50 0.13 ug/l 75-09-2 Methylene Chloride ND 2.0 1.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l 91-20-3 Naphthalene ND 0.50 0.13 ug/l 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l 100-42-5 Styrene ND 0.50 0.13 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l 108-88-3 Toluene ND 0.50 0.13 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l 71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l 79-01-6 Trichloroethylene 0.29 0.50 0.13 ug/l J 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l m,p-Xylene ND 1.0 0.13 ug/l 95-47-6 o-Xylene ND 0.50 0.13 ug/l 1330-20-7 Xylene (total)ND 1.5 0.25 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 97%70-130% 17060-07-0 1,2-Dichloroethane-D4 105%70-130% 2037-26-5 Toluene-D8 101%70-130% 460-00-4 4-Bromofluorobenzene 110%70-130% (a) Associated CCV outside control limits high, sample is ND. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 26 of 44 FC1878 3 3. 1 0 SGS North America Inc. Report of Analysis Page 1 of 2 Client Sample ID:WSW-2 Lab Sample ID:FC1878-11 Date Sampled:01/11/23 Matrix:AQ - Ground Water Date Received:01/13/23 Method:SM 6200B Percent Solids:n/a Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 E110979.D 1 01/17/23 21:13 KW n/a n/a VE2640 Run #2 Purge Volume Run #1 10.0 ml Run #2 VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.13 ug/l 108-86-1 Bromobenzene ND 0.50 0.13 ug/l 74-97-5 Bromochloromethane ND 0.50 0.13 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l 75-25-2 Bromoform ND 0.50 0.13 ug/l 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane ND 0.50 0.20 ug/l 67-66-3 Chloroform ND 0.50 0.13 ug/l 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l 75-71-8 Dichlorodifluoromethane a ND 0.50 0.20 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l 75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l 563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 27 of 44 FC1878 3 3. 1 1 SGS North America Inc. Report of Analysis Page 2 of 2 Client Sample ID:WSW-2 Lab Sample ID:FC1878-11 Date Sampled:01/11/23 Matrix:AQ - Ground Water Date Received:01/13/23 Method:SM 6200B Percent Solids:n/a Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l 100-41-4 Ethylbenzene ND 0.50 0.13 ug/l 87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l 74-83-9 Methyl Bromide ND 0.50 0.20 ug/l 74-87-3 Methyl Chloride ND 0.50 0.20 ug/l 74-95-3 Methylene Bromide ND 0.50 0.13 ug/l 75-09-2 Methylene Chloride ND 2.0 1.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l 91-20-3 Naphthalene ND 0.50 0.13 ug/l 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l 100-42-5 Styrene ND 0.50 0.13 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l 108-88-3 Toluene ND 0.50 0.13 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l 71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l 79-01-6 Trichloroethylene ND 0.50 0.13 ug/l 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l m,p-Xylene ND 1.0 0.13 ug/l 95-47-6 o-Xylene ND 0.50 0.13 ug/l 1330-20-7 Xylene (total)ND 1.5 0.25 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 96%70-130% 17060-07-0 1,2-Dichloroethane-D4 106%70-130% 2037-26-5 Toluene-D8 102%70-130% 460-00-4 4-Bromofluorobenzene 112%70-130% (a) Associated CCV outside control limits high, sample is ND. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 28 of 44 FC1878 3 3. 1 1 SGS North America Inc. Misc. Forms Custody Documents and Other Forms Includes the following where applicable: Chain of Custody Orlando, FL Section 4 29 of 44 FC1878 4 FC1878: Chain of Custody Page 1 of 2 30 of 44 FC1878 4 4. 1 Job Number:FC1878 Client:GRI Date / Time Received:1/13/2023 9:45:00 AM Delivery Method:FX Project:PEELE'S SERVICE STATION Airbill #'s: Cooler Information 1. Custody Seals Present 2. Custody Seals Intact 4. Cooler temp verification 3. Temp criteria achieved 5. Cooler media IR Gun Ice (Bag) Trip Blank Information 1. Trip Blank present / cooler 2. Trip Blank listed on COC 2. Samples preserved properly Sample Information 1. Sample labels present on bottles 5. Sample recvd within HT 4. Condition of sample 3. Sufficient volume/containers recvd for analysis: Intact Comments SM001Rev. Date 05/24/17 SGS Sample Receipt Summary Cooler Temps (Raw Measured) °C: Cooler Temps (Corrected) °C: Cooler 1: (0.4); Cooler 1: (0.6); 3. Type Of TB Received W or S N/A 6. Dates/Times/IDs on COC match Sample Label 7. VOCs have headspace 8. Bottles received for unspecified tests 9. Compositing instructions clear 10. Voa Soil Kits/Jars received past 48hrs? 11. % Solids Jar received? Misc. Information 25-Gram 5-GramNumber of Encores:Number of 5035 Field Kits:Number of Lab Filtered Metals: Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify) Y or N N/A Y or N Therm ID:IR 1; Therm CF:0.2; # of Coolers:1 Y or N N/A 12. Residual Chlorine Present? Residual Chlorine Test Strip Lot #: Technician:Reviewer:NATHANS Date:Date:1/13/2023 9:45:00 AM FC1878: Chain of Custody Page 2 of 2 31 of 44 FC1878 4 4. 1 SGS North America Inc. MS Volatiles QC Data Summaries Includes the following where applicable: Method Blank Summaries Blank Spike Summaries Matrix Spike and Duplicate Summaries Orlando, FL Section 5 32 of 44 FC1878 5 Method Blank Summary Page 1 of 2 Job Number:FC1878 Account:GRINCC GRI (Geological Resources Inc.) Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VE2639-MB E110926.D 1 01/16/23 KW n/a n/a VE2639 The QC reported here applies to the following samples:Method: SM 6200B FC1878-1, FC1878-2, FC1878-3, FC1878-4 CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.13 ug/l 108-86-1 Bromobenzene ND 0.50 0.13 ug/l 74-97-5 Bromochloromethane ND 0.50 0.13 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l 75-25-2 Bromoform ND 0.50 0.13 ug/l 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane ND 0.50 0.20 ug/l 67-66-3 Chloroform ND 0.50 0.13 ug/l 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l 75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l 75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l 563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l 108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l 100-41-4 Ethylbenzene ND 0.50 0.13 ug/l 87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l 33 of 44 FC1878 5 5. 1 . 1 Method Blank Summary Page 2 of 2 Job Number:FC1878 Account:GRINCC GRI (Geological Resources Inc.) Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VE2639-MB E110926.D 1 01/16/23 KW n/a n/a VE2639 The QC reported here applies to the following samples:Method: SM 6200B FC1878-1, FC1878-2, FC1878-3, FC1878-4 CAS No.Compound Result RL MDL Units Q 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l 74-83-9 Methyl Bromide ND 0.50 0.20 ug/l 74-87-3 Methyl Chloride ND 0.50 0.20 ug/l 74-95-3 Methylene Bromide ND 0.50 0.13 ug/l 75-09-2 Methylene Chloride ND 2.0 1.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l 91-20-3 Naphthalene ND 0.50 0.13 ug/l 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l 100-42-5 Styrene ND 0.50 0.13 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l 108-88-3 Toluene ND 0.50 0.13 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l 71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l 79-01-6 Trichloroethylene ND 0.50 0.13 ug/l 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l m,p-Xylene ND 1.0 0.13 ug/l 95-47-6 o-Xylene ND 0.50 0.13 ug/l 1330-20-7 Xylene (total)ND 1.5 0.25 ug/l CAS No.Surrogate Recoveries Limits 1868-53-7 Dibromofluoromethane 96%70-130% 17060-07-0 1,2-Dichloroethane-D4 101%70-130% 2037-26-5 Toluene-D8 104%70-130% 460-00-4 4-Bromofluorobenzene 108%70-130% 34 of 44 FC1878 5 5. 1 . 1 Method Blank Summary Page 1 of 2 Job Number:FC1878 Account:GRINCC GRI (Geological Resources Inc.) Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VE2640-MB E110958.D 1 01/17/23 KW n/a n/a VE2640 The QC reported here applies to the following samples:Method: SM 6200B FC1878-5, FC1878-6, FC1878-7, FC1878-8, FC1878-9, FC1878-10, FC1878-11 CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.13 ug/l 108-86-1 Bromobenzene ND 0.50 0.13 ug/l 74-97-5 Bromochloromethane ND 0.50 0.13 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l 75-25-2 Bromoform ND 0.50 0.13 ug/l 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane ND 0.50 0.20 ug/l 67-66-3 Chloroform ND 0.50 0.13 ug/l 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l 75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l 75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l 563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l 108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l 100-41-4 Ethylbenzene ND 0.50 0.13 ug/l 87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l 35 of 44 FC1878 5 5. 1 . 2 Method Blank Summary Page 2 of 2 Job Number:FC1878 Account:GRINCC GRI (Geological Resources Inc.) Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VE2640-MB E110958.D 1 01/17/23 KW n/a n/a VE2640 The QC reported here applies to the following samples:Method: SM 6200B FC1878-5, FC1878-6, FC1878-7, FC1878-8, FC1878-9, FC1878-10, FC1878-11 CAS No.Compound Result RL MDL Units Q 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l 74-83-9 Methyl Bromide ND 0.50 0.20 ug/l 74-87-3 Methyl Chloride ND 0.50 0.20 ug/l 74-95-3 Methylene Bromide ND 0.50 0.13 ug/l 75-09-2 Methylene Chloride ND 2.0 1.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l 91-20-3 Naphthalene ND 0.50 0.13 ug/l 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l 100-42-5 Styrene ND 0.50 0.13 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l 108-88-3 Toluene ND 0.50 0.13 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l 71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l 79-01-6 Trichloroethylene ND 0.50 0.13 ug/l 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l m,p-Xylene ND 1.0 0.13 ug/l 95-47-6 o-Xylene ND 0.50 0.13 ug/l 1330-20-7 Xylene (total)ND 1.5 0.25 ug/l CAS No.Surrogate Recoveries Limits 1868-53-7 Dibromofluoromethane 96%70-130% 17060-07-0 1,2-Dichloroethane-D4 102%70-130% 2037-26-5 Toluene-D8 103%70-130% 460-00-4 4-Bromofluorobenzene 109%70-130% 36 of 44 FC1878 5 5. 1 . 2 Blank Spike Summary Page 1 of 2 Job Number:FC1878 Account:GRINCC GRI (Geological Resources Inc.) Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VE2639-BS E110924.D 1 01/16/23 KW n/a n/a VE2639 The QC reported here applies to the following samples:Method: SM 6200B FC1878-1, FC1878-2, FC1878-3, FC1878-4 Spike BSP BSP CAS No.Compound ug/l ug/l %Limits 71-43-2 Benzene 10 9.5 95 70-130 108-86-1 Bromobenzene 10 8.9 89 70-130 74-97-5 Bromochloromethane 10 10.3 103 70-130 75-27-4 Bromodichloromethane 10 10.1 101 70-130 75-25-2 Bromoform 10 10.5 105 70-130 104-51-8 n-Butylbenzene 10 9.5 95 70-130 135-98-8 sec-Butylbenzene 10 10.4 104 70-130 98-06-6 tert-Butylbenzene 10 10.0 100 70-130 56-23-5 Carbon Tetrachloride 10 11.9 119 70-130 108-90-7 Chlorobenzene 10 9.8 98 70-130 75-00-3 Chloroethane 10 8.2 82 60-140 67-66-3 Chloroform 10 9.7 97 70-130 95-49-8 o-Chlorotoluene 10 9.7 97 70-130 106-43-4 p-Chlorotoluene 10 9.9 99 70-130 124-48-1 Dibromochloromethane 10 9.9 99 70-130 96-12-8 1,2-Dibromo-3-chloropropane 10 9.4 94 70-130 106-93-4 1,2-Dibromoethane 10 10.1 101 70-130 75-71-8 Dichlorodifluoromethane 10 9.0 90 60-140 95-50-1 1,2-Dichlorobenzene 10 9.8 98 70-130 541-73-1 1,3-Dichlorobenzene 10 9.8 98 70-130 106-46-7 1,4-Dichlorobenzene 10 9.3 93 70-130 75-34-3 1,1-Dichloroethane 10 9.9 99 70-130 107-06-2 1,2-Dichloroethane 10 9.7 97 70-130 75-35-4 1,1-Dichloroethylene 10 9.9 99 70-130 156-59-2 cis-1,2-Dichloroethylene 10 10 100 70-130 156-60-5 trans-1,2-Dichloroethylene 10 9.7 97 70-130 78-87-5 1,2-Dichloropropane 10 9.2 92 70-130 142-28-9 1,3-Dichloropropane 10 9.2 92 70-130 594-20-7 2,2-Dichloropropane 10 9.5 95 70-130 563-58-6 1,1-Dichloropropene 10 9.7 97 70-130 10061-01-5 cis-1,3-Dichloropropene 10 9.9 99 70-130 10061-02-6 trans-1,3-Dichloropropene 10 10.8 108 70-130 108-20-3 Di-Isopropyl Ether 10 9.9 99 70-130 100-41-4 Ethylbenzene 10 9.7 97 70-130 87-68-3 Hexachlorobutadiene 10 9.2 92 70-130 98-82-8 Isopropylbenzene 10 10.2 102 70-130 * = Outside of Control Limits. 37 of 44 FC1878 5 5. 2 . 1 Blank Spike Summary Page 2 of 2 Job Number:FC1878 Account:GRINCC GRI (Geological Resources Inc.) Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VE2639-BS E110924.D 1 01/16/23 KW n/a n/a VE2639 The QC reported here applies to the following samples:Method: SM 6200B FC1878-1, FC1878-2, FC1878-3, FC1878-4 Spike BSP BSP CAS No.Compound ug/l ug/l %Limits 99-87-6 p-Isopropyltoluene 10 10.2 102 70-130 74-83-9 Methyl Bromide 10 7.7 77 60-140 74-87-3 Methyl Chloride 10 8.4 84 60-140 74-95-3 Methylene Bromide 10 9.5 95 70-130 75-09-2 Methylene Chloride 10 9.7 97 70-130 1634-04-4 Methyl Tert Butyl Ether 10 9.9 99 70-130 91-20-3 Naphthalene 10 10.4 104 70-130 103-65-1 n-Propylbenzene 10 9.8 98 70-130 100-42-5 Styrene 10 9.6 96 70-130 630-20-6 1,1,1,2-Tetrachloroethane 10 10.1 101 70-130 79-34-5 1,1,2,2-Tetrachloroethane 10 9.8 98 70-130 127-18-4 Tetrachloroethylene 10 9.8 98 70-130 108-88-3 Toluene 10 9.5 95 70-130 87-61-6 1,2,3-Trichlorobenzene 10 9.7 97 70-130 120-82-1 1,2,4-Trichlorobenzene 10 9.9 99 70-130 71-55-6 1,1,1-Trichloroethane 10 9.8 98 70-130 79-00-5 1,1,2-Trichloroethane 10 9.8 98 70-130 79-01-6 Trichloroethylene 10 9.4 94 70-130 75-69-4 Trichlorofluoromethane 10 8.3 83 60-140 96-18-4 1,2,3-Trichloropropane 10 9.1 91 70-130 95-63-6 1,2,4-Trimethylbenzene 10 10.2 102 70-130 108-67-8 1,3,5-Trimethylbenzene 10 9.7 97 70-130 75-01-4 Vinyl Chloride 10 8.0 80 60-140 m,p-Xylene 20 19.7 99 70-130 95-47-6 o-Xylene 10 10.4 104 70-130 1330-20-7 Xylene (total)30 30.1 100 70-130 CAS No.Surrogate Recoveries BSP Limits 1868-53-7 Dibromofluoromethane 100%70-130% 17060-07-0 1,2-Dichloroethane-D4 101%70-130% 2037-26-5 Toluene-D8 100%70-130% 460-00-4 4-Bromofluorobenzene 100%70-130% * = Outside of Control Limits. 38 of 44 FC1878 5 5. 2 . 1 Blank Spike Summary Page 1 of 2 Job Number:FC1878 Account:GRINCC GRI (Geological Resources Inc.) Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VE2640-BS E110956.D 1 01/17/23 KW n/a n/a VE2640 The QC reported here applies to the following samples:Method: SM 6200B FC1878-5, FC1878-6, FC1878-7, FC1878-8, FC1878-9, FC1878-10, FC1878-11 Spike BSP BSP CAS No.Compound ug/l ug/l %Limits 71-43-2 Benzene 10 9.4 94 70-130 108-86-1 Bromobenzene 10 9.1 91 70-130 74-97-5 Bromochloromethane 10 10.3 103 70-130 75-27-4 Bromodichloromethane 10 10.1 101 70-130 75-25-2 Bromoform 10 9.8 98 70-130 104-51-8 n-Butylbenzene 10 9.1 91 70-130 135-98-8 sec-Butylbenzene 10 9.8 98 70-130 98-06-6 tert-Butylbenzene 10 9.7 97 70-130 56-23-5 Carbon Tetrachloride 10 11.0 110 70-130 108-90-7 Chlorobenzene 10 9.6 96 70-130 75-00-3 Chloroethane 10 8.6 86 60-140 67-66-3 Chloroform 10 9.6 96 70-130 95-49-8 o-Chlorotoluene 10 9.9 99 70-130 106-43-4 p-Chlorotoluene 10 10.1 101 70-130 124-48-1 Dibromochloromethane 10 9.7 97 70-130 96-12-8 1,2-Dibromo-3-chloropropane 10 9.4 94 70-130 106-93-4 1,2-Dibromoethane 10 10.1 101 70-130 75-71-8 Dichlorodifluoromethane 10 9.1 91 60-140 95-50-1 1,2-Dichlorobenzene 10 9.8 98 70-130 541-73-1 1,3-Dichlorobenzene 10 9.8 98 70-130 106-46-7 1,4-Dichlorobenzene 10 9.3 93 70-130 75-34-3 1,1-Dichloroethane 10 9.9 99 70-130 107-06-2 1,2-Dichloroethane 10 9.6 96 70-130 75-35-4 1,1-Dichloroethylene 10 9.0 90 70-130 156-59-2 cis-1,2-Dichloroethylene 10 10.1 101 70-130 156-60-5 trans-1,2-Dichloroethylene 10 9.5 95 70-130 78-87-5 1,2-Dichloropropane 10 9.3 93 70-130 142-28-9 1,3-Dichloropropane 10 9.2 92 70-130 594-20-7 2,2-Dichloropropane 10 8.9 89 70-130 563-58-6 1,1-Dichloropropene 10 9.1 91 70-130 10061-01-5 cis-1,3-Dichloropropene 10 9.8 98 70-130 10061-02-6 trans-1,3-Dichloropropene 10 10.5 105 70-130 108-20-3 Di-Isopropyl Ether 10 10.2 102 70-130 100-41-4 Ethylbenzene 10 9.5 95 70-130 87-68-3 Hexachlorobutadiene 10 8.2 82 70-130 98-82-8 Isopropylbenzene 10 9.6 96 70-130 * = Outside of Control Limits. 39 of 44 FC1878 5 5. 2 . 2 Blank Spike Summary Page 2 of 2 Job Number:FC1878 Account:GRINCC GRI (Geological Resources Inc.) Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VE2640-BS E110956.D 1 01/17/23 KW n/a n/a VE2640 The QC reported here applies to the following samples:Method: SM 6200B FC1878-5, FC1878-6, FC1878-7, FC1878-8, FC1878-9, FC1878-10, FC1878-11 Spike BSP BSP CAS No.Compound ug/l ug/l %Limits 99-87-6 p-Isopropyltoluene 10 9.6 96 70-130 74-83-9 Methyl Bromide 10 8.7 87 60-140 74-87-3 Methyl Chloride 10 9.0 90 60-140 74-95-3 Methylene Bromide 10 9.7 97 70-130 75-09-2 Methylene Chloride 10 9.6 96 70-130 1634-04-4 Methyl Tert Butyl Ether 10 9.8 98 70-130 91-20-3 Naphthalene 10 10.5 105 70-130 103-65-1 n-Propylbenzene 10 9.4 94 70-130 100-42-5 Styrene 10 9.6 96 70-130 630-20-6 1,1,1,2-Tetrachloroethane 10 10.1 101 70-130 79-34-5 1,1,2,2-Tetrachloroethane 10 10.1 101 70-130 127-18-4 Tetrachloroethylene 10 9.1 91 70-130 108-88-3 Toluene 10 9.5 95 70-130 87-61-6 1,2,3-Trichlorobenzene 10 9.4 94 70-130 120-82-1 1,2,4-Trichlorobenzene 10 9.4 94 70-130 71-55-6 1,1,1-Trichloroethane 10 9.4 94 70-130 79-00-5 1,1,2-Trichloroethane 10 10 100 70-130 79-01-6 Trichloroethylene 10 9.1 91 70-130 75-69-4 Trichlorofluoromethane 10 8.6 86 60-140 96-18-4 1,2,3-Trichloropropane 10 9.3 93 70-130 95-63-6 1,2,4-Trimethylbenzene 10 10.1 101 70-130 108-67-8 1,3,5-Trimethylbenzene 10 9.5 95 70-130 75-01-4 Vinyl Chloride 10 8.2 82 60-140 m,p-Xylene 20 19.1 96 70-130 95-47-6 o-Xylene 10 10.2 102 70-130 1330-20-7 Xylene (total)30 29.4 98 70-130 CAS No.Surrogate Recoveries BSP Limits 1868-53-7 Dibromofluoromethane 99%70-130% 17060-07-0 1,2-Dichloroethane-D4 101%70-130% 2037-26-5 Toluene-D8 101%70-130% 460-00-4 4-Bromofluorobenzene 104%70-130% * = Outside of Control Limits. 40 of 44 FC1878 5 5. 2 . 2 Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2 Job Number:FC1878 Account:GRINCC GRI (Geological Resources Inc.) Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FC1874-4MS E110934.D 10 01/16/23 KW n/a n/a VE2639 FC1874-4MSD E110935.D 10 01/16/23 KW n/a n/a VE2639 FC1874-4 E110933.D 10 01/16/23 KW n/a n/a VE2639 The QC reported here applies to the following samples:Method: SM 6200B FC1878-1, FC1878-2, FC1878-3, FC1878-4 FC1874-4 Spike MS MS Spike MSD MSD Limits CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD 71-43-2 Benzene 357 100 474 117 100 472 115 0 70-130/20 108-86-1 Bromobenzene ND 100 97.7 98 100 101 101 3 70-130/20 74-97-5 Bromochloromethane ND 100 105 105 100 108 108 3 70-130/20 75-27-4 Bromodichloromethane ND 100 109 109 100 111 111 2 70-130/20 75-25-2 Bromoform ND 100 94.2 94 100 99.8 100 6 70-130/20 104-51-8 n-Butylbenzene ND 100 115 115 100 118 118 3 70-130/20 135-98-8 sec-Butylbenzene ND 100 125 125 100 130 130 4 70-130/20 98-06-6 tert-Butylbenzene 2.3 J 100 122 120 100 125 123 2 70-130/20 56-23-5 Carbon Tetrachloride ND 100 132 132*100 135 135*2 70-130/20 108-90-7 Chlorobenzene ND 100 108 108 100 109 109 1 70-130/20 75-00-3 Chloroethane ND 100 107 107 100 118 118 10 60-140/20 67-66-3 Chloroform ND 100 112 112 100 112 112 0 70-130/20 95-49-8 o-Chlorotoluene ND 100 115 115 100 115 115 0 70-130/20 106-43-4 p-Chlorotoluene ND 100 112 112 100 114 114 2 70-130/20 124-48-1 Dibromochloromethane ND 100 95.8 96 100 100 100 4 70-130/20 96-12-8 1,2-Dibromo-3-chloropropane ND 100 103 103 100 101 101 2 70-130/20 106-93-4 1,2-Dibromoethane ND 100 106 106 100 108 108 2 70-130/20 75-71-8 Dichlorodifluoromethane ND 100 114 114 100 138 138 19 60-140/20 95-50-1 1,2-Dichlorobenzene ND 100 105 105 100 107 107 2 70-130/20 541-73-1 1,3-Dichlorobenzene ND 100 108 108 100 111 111 3 70-130/20 106-46-7 1,4-Dichlorobenzene ND 100 103 103 100 106 106 3 70-130/20 75-34-3 1,1-Dichloroethane ND 100 115 115 100 114 114 1 70-130/20 107-06-2 1,2-Dichloroethane 29.0 100 137 108 100 134 105 2 70-130/20 75-35-4 1,1-Dichloroethylene ND 100 123 123 100 121 121 2 70-130/20 156-59-2 cis-1,2-Dichloroethylene ND 100 110 110 100 112 112 2 70-130/20 156-60-5 trans-1,2-Dichloroethylene ND 100 114 114 100 113 113 1 70-130/20 78-87-5 1,2-Dichloropropane ND 100 106 106 100 107 107 1 70-130/20 142-28-9 1,3-Dichloropropane ND 100 100 100 100 99.5 100 1 70-130/20 594-20-7 2,2-Dichloropropane ND 100 108 108 100 108 108 0 70-130/20 563-58-6 1,1-Dichloropropene ND 100 115 115 100 115 115 0 70-130/20 10061-01-5 cis-1,3-Dichloropropene ND 100 103 103 100 105 105 2 70-130/20 10061-02-6 trans-1,3-Dichloropropene ND 100 111 111 100 111 111 0 70-130/20 108-20-3 Di-Isopropyl Ether 31.1 100 145 114 100 146 115 1 70-130/20 100-41-4 Ethylbenzene 13.9 100 128 114 100 128 114 0 70-130/20 87-68-3 Hexachlorobutadiene ND 100 108 108 100 108 108 0 70-130/20 98-82-8 Isopropylbenzene 5.7 100 123 117 100 125 119 2 70-130/20 * = Outside of Control Limits. 41 of 44 FC1878 5 5. 3 . 1 Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2 Job Number:FC1878 Account:GRINCC GRI (Geological Resources Inc.) Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FC1874-4MS E110934.D 10 01/16/23 KW n/a n/a VE2639 FC1874-4MSD E110935.D 10 01/16/23 KW n/a n/a VE2639 FC1874-4 E110933.D 10 01/16/23 KW n/a n/a VE2639 The QC reported here applies to the following samples:Method: SM 6200B FC1878-1, FC1878-2, FC1878-3, FC1878-4 FC1874-4 Spike MS MS Spike MSD MSD Limits CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD 99-87-6 p-Isopropyltoluene ND 100 120 120 100 124 124 3 70-130/20 74-83-9 Methyl Bromide ND 100 94.8 95 100 97.1 97 2 60-140/20 74-87-3 Methyl Chloride ND 100 103 103 100 125 125 19 60-140/20 74-95-3 Methylene Bromide ND 100 105 105 100 105 105 0 70-130/20 75-09-2 Methylene Chloride ND 100 113 113 100 110 110 3 70-130/20 1634-04-4 Methyl Tert Butyl Ether ND 100 103 103 100 105 105 2 70-130/20 91-20-3 Naphthalene 9.0 100 122 113 100 122 113 0 70-130/20 103-65-1 n-Propylbenzene 5.4 100 124 119 100 125 120 1 70-130/20 100-42-5 Styrene ND 100 106 106 100 109 109 3 70-130/20 630-20-6 1,1,1,2-Tetrachloroethane ND 100 106 106 100 108 108 2 70-130/20 79-34-5 1,1,2,2-Tetrachloroethane ND 100 109 109 100 110 110 1 70-130/20 127-18-4 Tetrachloroethylene ND 100 108 108 100 110 110 2 70-130/20 108-88-3 Toluene 41.8 100 153 111 100 153 111 0 70-130/20 87-61-6 1,2,3-Trichlorobenzene ND 100 103 103 100 101 101 2 70-130/20 120-82-1 1,2,4-Trichlorobenzene ND 100 107 107 100 106 106 1 70-130/20 71-55-6 1,1,1-Trichloroethane ND 100 114 114 100 115 115 1 70-130/20 79-00-5 1,1,2-Trichloroethane ND 100 105 105 100 107 107 2 70-130/20 79-01-6 Trichloroethylene ND 100 110 110 100 110 110 0 70-130/20 75-69-4 Trichlorofluoromethane ND 100 113 113 100 130 130 14 60-140/20 96-18-4 1,2,3-Trichloropropane ND 100 97.6 98 100 99.4 99 2 70-130/20 95-63-6 1,2,4-Trimethylbenzene 37.7 100 158 120 100 162 124 3 70-130/20 108-67-8 1,3,5-Trimethylbenzene 6.1 100 119 113 100 121 115 2 70-130/20 75-01-4 Vinyl Chloride ND 100 112 112 100 124 124 10 60-140/20 m,p-Xylene 28.4 200 263 117 200 264 118 0 70-130/20 95-47-6 o-Xylene 40.3 100 161 121 100 162 122 1 70-130/20 1330-20-7 Xylene (total)68.8 300 424 118 300 426 119 0 70-130/20 CAS No.Surrogate Recoveries MS MSD FC1874-4 Limits 1868-53-7 Dibromofluoromethane 99%99%94%70-130% 17060-07-0 1,2-Dichloroethane-D4 102%100%105%70-130% 2037-26-5 Toluene-D8 102%100%106%70-130% 460-00-4 4-Bromofluorobenzene 103%102%110%70-130% * = Outside of Control Limits. 42 of 44 FC1878 5 5. 3 . 1 Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2 Job Number:FC1878 Account:GRINCC GRI (Geological Resources Inc.) Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch LA86707-1MS E110965.D 25 01/17/23 KW n/a n/a VE2640 LA86707-1MSD E110966.D 25 01/17/23 KW n/a n/a VE2640 LA86707-1 E110964.D 25 01/17/23 KW n/a n/a VE2640 The QC reported here applies to the following samples:Method: SM 6200B FC1878-5, FC1878-6, FC1878-7, FC1878-8, FC1878-9, FC1878-10, FC1878-11 LA86707-1 Spike MS MS Spike MSD MSD Limits CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD 71-43-2 Benzene 1240 250 1580 136* a 250 1540 120 3 70-130/20 108-86-1 Bromobenzene ND 250 243 97 250 256 102 5 70-130/20 74-97-5 Bromochloromethane ND 250 263 105 250 274 110 4 70-130/20 75-27-4 Bromodichloromethane ND 250 252 101 250 260 104 3 70-130/20 75-25-2 Bromoform ND 250 179 72 250 198 79 10 70-130/20 104-51-8 n-Butylbenzene 15.4 250 289 109 250 300 114 4 70-130/20 135-98-8 sec-Butylbenzene 15.3 250 313 119 250 325 124 4 70-130/20 98-06-6 tert-Butylbenzene ND 250 287 115 250 297 119 3 70-130/20 56-23-5 Carbon Tetrachloride ND 250 270 108 250 286 114 6 70-130/20 108-90-7 Chlorobenzene ND 250 267 107 250 277 111 4 70-130/20 75-00-3 Chloroethane ND 250 255 102 250 289 116 13 60-140/20 67-66-3 Chloroform 14.9 250 277 105 250 285 108 3 70-130/20 95-49-8 o-Chlorotoluene ND 250 268 107 250 277 111 3 70-130/20 106-43-4 p-Chlorotoluene ND 250 270 108 250 279 112 3 70-130/20 124-48-1 Dibromochloromethane ND 250 208 83 250 221 88 6 70-130/20 96-12-8 1,2-Dibromo-3-chloropropane ND 250 214 86 250 225 90 5 70-130/20 106-93-4 1,2-Dibromoethane ND 250 249 100 250 263 105 5 70-130/20 75-71-8 Dichlorodifluoromethane ND 250 281 112 250 328 131 15 60-140/20 95-50-1 1,2-Dichlorobenzene ND 250 253 101 250 267 107 5 70-130/20 541-73-1 1,3-Dichlorobenzene ND 250 259 104 250 272 109 5 70-130/20 106-46-7 1,4-Dichlorobenzene ND 250 249 100 250 262 105 5 70-130/20 75-34-3 1,1-Dichloroethane ND 250 273 109 250 278 111 2 70-130/20 107-06-2 1,2-Dichloroethane ND 250 252 101 250 257 103 2 70-130/20 75-35-4 1,1-Dichloroethylene ND 250 295 118 250 291 116 1 70-130/20 156-59-2 cis-1,2-Dichloroethylene ND 250 268 107 250 284 114 6 70-130/20 156-60-5 trans-1,2-Dichloroethylene ND 250 274 110 250 278 111 1 70-130/20 78-87-5 1,2-Dichloropropane ND 250 251 100 250 261 104 4 70-130/20 142-28-9 1,3-Dichloropropane ND 250 233 93 250 242 97 4 70-130/20 594-20-7 2,2-Dichloropropane ND 250 259 104 250 261 104 1 70-130/20 563-58-6 1,1-Dichloropropene ND 250 280 112 250 287 115 2 70-130/20 10061-01-5 cis-1,3-Dichloropropene ND 250 238 95 250 251 100 5 70-130/20 10061-02-6 trans-1,3-Dichloropropene ND 250 249 100 250 259 104 4 70-130/20 108-20-3 Di-Isopropyl Ether 11.3 J 250 283 109 250 286 110 1 70-130/20 100-41-4 Ethylbenzene 362 250 666 122 250 664 121 0 70-130/20 87-68-3 Hexachlorobutadiene ND 250 253 101 250 268 107 6 70-130/20 98-82-8 Isopropylbenzene 145 250 446 120 250 455 124 2 70-130/20 * = Outside of Control Limits. 43 of 44 FC1878 5 5. 3 . 2 Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2 Job Number:FC1878 Account:GRINCC GRI (Geological Resources Inc.) Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch LA86707-1MS E110965.D 25 01/17/23 KW n/a n/a VE2640 LA86707-1MSD E110966.D 25 01/17/23 KW n/a n/a VE2640 LA86707-1 E110964.D 25 01/17/23 KW n/a n/a VE2640 The QC reported here applies to the following samples:Method: SM 6200B FC1878-5, FC1878-6, FC1878-7, FC1878-8, FC1878-9, FC1878-10, FC1878-11 LA86707-1 Spike MS MS Spike MSD MSD Limits CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD 99-87-6 p-Isopropyltoluene 6.4 J 250 291 114 250 307 120 5 70-130/20 74-83-9 Methyl Bromide ND 250 215 86 250 243 97 12 60-140/20 74-87-3 Methyl Chloride ND 250 257 103 250 295 118 14 60-140/20 74-95-3 Methylene Bromide ND 250 248 99 250 261 104 5 70-130/20 75-09-2 Methylene Chloride ND 250 253 101 250 254 102 0 70-130/20 1634-04-4 Methyl Tert Butyl Ether 180 250 443 105 250 438 103 1 70-130/20 91-20-3 Naphthalene 723 250 1000 111 250 1010 115 1 70-130/20 103-65-1 n-Propylbenzene 139 250 437 119 250 441 121 1 70-130/20 100-42-5 Styrene ND 250 257 103 250 270 108 5 70-130/20 630-20-6 1,1,1,2-Tetrachloroethane ND 250 253 101 250 262 105 3 70-130/20 79-34-5 1,1,2,2-Tetrachloroethane ND 250 251 100 250 258 103 3 70-130/20 127-18-4 Tetrachloroethylene ND 250 264 106 250 280 112 6 70-130/20 108-88-3 Toluene 6.8 J 250 268 104 250 278 108 4 70-130/20 87-61-6 1,2,3-Trichlorobenzene ND 250 240 96 250 254 102 6 70-130/20 120-82-1 1,2,4-Trichlorobenzene ND 250 254 102 250 263 105 3 70-130/20 71-55-6 1,1,1-Trichloroethane ND 250 280 112 250 290 116 4 70-130/20 79-00-5 1,1,2-Trichloroethane ND 250 245 98 250 253 101 3 70-130/20 79-01-6 Trichloroethylene ND 250 263 105 250 274 110 4 70-130/20 75-69-4 Trichlorofluoromethane ND 250 261 104 250 304 122 15 60-140/20 96-18-4 1,2,3-Trichloropropane ND 250 234 94 250 241 96 3 70-130/20 95-63-6 1,2,4-Trimethylbenzene 9.8 J 250 288 111 250 302 117 5 70-130/20 108-67-8 1,3,5-Trimethylbenzene 4.7 J 250 272 107 250 282 111 4 70-130/20 75-01-4 Vinyl Chloride ND 250 236 94 250 274 110 15 60-140/20 m,p-Xylene 24.6 J 500 572 109 500 589 113 3 70-130/20 95-47-6 o-Xylene 342 250 655 125 250 652 124 0 70-130/20 1330-20-7 Xylene (total)366 750 1230 115 750 1240 117 1 70-130/20 CAS No.Surrogate Recoveries MS MSD LA86707-1 Limits 1868-53-7 Dibromofluoromethane 100%98%95%70-130% 17060-07-0 1,2-Dichloroethane-D4 103%96%101%70-130% 2037-26-5 Toluene-D8 100%98%102%70-130% 460-00-4 4-Bromofluorobenzene 103%103%109%70-130% (a) Outside control limits due to high level in sample relative to spike amount. * = Outside of Control Limits. 44 of 44 FC1878 5 5. 3 . 2 APPENDIX C Contaminant Mass Calculations Area ID Well ID Area (ft²) Average Well Depth (ft.) Average Depth to Water (ft.) Water Column Height (ft) Volume (ft³) Volume (L) Effective Porosity Effective Volume (L) MW-1 MW-2R MW-11 Area Date Well Benzene (μ/L) Toluene (μ/L) Ethylbenzene (μ/L) Xylenes (μ/L) MTBE (μ/L) Naphthalene (μ/L) Total (μ/L) DTW (ft.) Average Water Column Height (ft.) Total Average Mass (g)Percent Red.To Date Red. MW-1 0.00 0.00 0.29 7.10 0.00 3.30 10.69 1.87 MW-2R 26.20 399.00 88.60 1720.00 0.00 109.00 2342.80 2.16 MW-11 1.9 1.1 28.2 210 0 87 328.20 3.70 Avg.9.37 133.37 39.03 645.70 0.00 66.43 893.90 2.58 MW-1 1.20 2.7 18.6 194 0.00 192 1.20 8.45 MW-2R 858.00 2980.00 166.00 7820.00 0.00 208.00 12032.00 9.24 MW-11 16.50 6.60 60.60 393.00 0.00 259.00 735.70 10.01 Avg.291.90 1493.30 113.30 4106.50 0.00 233.50 4256.30 9.23 MW-1 0.00 0.00 0.43 3.30 0.00 3.10 6.83 2.85 MW-2R 15.90 152.00 63.00 996.00 0.00 56.80 1283.70 3.68 MW-11 4.60 0.00 29.90 194.00 0.00 154.00 382.50 5.40 Avg.6.83 50.67 31.11 397.77 0.00 71.30 557.68 3.98 MW-1 0.00 0.00 0.00 0.00 0.00 17.00 17.00 11.42 MW-2R 8.20 16.70 6.40 24.00 0.00 49.10 104.40 12.12 MW-11 7.90 0.00 49.10 245.00 0.00 210.00 512.00 12.41 Avg.5.37 16.70 18.50 89.67 0.00 92.03 222.27 11.98 MW-1 4.6 0.76 6.4 3.6 0.00 16.9 32.26 11.79 MW-2R 74.1 88.2 21.2 1270 0.00 8.8 J 1453.50 12.65 MW-11 7.6 <0.13 5.3 2 0.00 38.6 53.50 13.64 Avg.28.77 88.96 10.97 425.20 0.00 27.75 581.64 12.698.35 Date Average Water Column Height (ft.) 04/01/15 12.62 07/15/20 5.97 03/11/21 11.22 12/14/21 3.22 01/11/23 2.51 Notes: • April 1, 2015 was the first sampling event with out free product in MW-2R; therful used as the baseline sampling event. • Area of the contaminant plume is calculated from Figure 6 • Height of the water column is calculated by subtracting the average depth to water from the average well depth of the referenced monitoring wells • Volume of the contaminant plume is calculated by multiplying the area of the plume by the average height of the water column during each sampling event • Effective porosity is assumed based on the sub-surface soil profile obtained from well construction records and soil boring logs • Total mass was calculated by multiplying the total contaminant concentrations for the sampling event with effective volume • Contaminant mass cannot be calculated in wells containing FP; therefore, the total contaminant mass is based on the known concentrations in the area for each sampling event. • When areas couldn’t be sampled, the last known concentrations were used in the calculations. 25.52 88.6%93.7% 45%75.4% 52.04 -103.9%87.1% Percent Reduction Compared to Previous Event --- 12/14/21 3.22 Area 1 01/11/23 2.51 07/15/20 5.97 1 15.26,301.9 2.58 12.62 450,406 12.62 906.38 -125.1%-125.1% APPENDIX C CONTAMINANT MASS CALCULATIONS PEELE'S SERVICE STATION (INCIDENT NO. 10000) 03/11/21 Baseline Event 11.22 402.72 223.38 75.4% ------04/01/15 79,530 0.202,252,031 44.5% Total Contaminant Mass (g) 402.72 Percent Reduction To Date --- 52.04 -103.9%87% 25.52 94%88.6% 906.38 -125.1%-125% 223.38 APPENDIX D; Water Supply Well Abandonment Agreement Letters 3502 Hayes Road • Monroe, North Carolina 28110 113 West Firetower Road, Suite G • Winterville, North Carolina 28590 Phone (704) 845-4010 • (888) 870-4133 • Fax (704) 845-4012 January 9, 2023 Evangeline M Patterson 3759 Brennan Avenue Norfolk, Virginia 23502 Re: Water Supply Abandonment Agreement Peele’s Service Station Jamesville, Martin County, North Carolina Parcel No. 0100696 Incident #10000 GRI Project No. 2516 Dear Ms. Patterson: Geological Resources, Inc. (GRI) Is currently monitoring the active incident #10000 located at 2675 Old US Highway 64. Concentrations of petroleum contaminants that exceed the North Carolina Department of Environmental Quality (NCDEQ) maximum allowable concentrations were reported in ground water samples collected from the associated monitoring well. Based on this information, GRI proposes to abandon the water supply well within 250 feet of the source area, to lower the NCDEQ risk classification of the release. It is GRI’s understanding that you are the owner of the property (2717 Old US Highway 64) identified as Parcel No. 0100696 and that water supply well (WSW-1) is located on this property. On behalf of the former owners (Peele’s Service Station) of the 2675 Old US Highway 64 site, GRI is requesting your permission to abandon the water supply well (WSW-1). Costs associated with the abandonment of your water supply well will be covered by the responsible party. We would greatly appreciate a response, even if you elect not to abandon your water supply well at this time at this time. Your cooperation in this matter will be greatly appreciated. If you have any questions, please feel free to contact me at (704) 845-4010. Sincerely, Ethan Rogerson, GIT Project Manager Water Supply Well Abandonment 2717 Old US Highway 64 Page 2 of 2 3502 Hayes Road • Monroe, North Carolina 28110 113 West Firetower Road, Suite G • Winterville, North Carolina 28590 Phone (704) 845-4010 • (888) 870-4133 • Fax (704) 845-4012 Yes, I agree to allow my water supply well to be abandon. No, I do not agree to allow my water supply well to be abandon. Signature Date (For Martin County Parcel No. 0100696) Evangeline M. Patterson ___________________________ Phone Number WSW-1 3502 Hayes Road • Monroe, North Carolina 28110 113 West Firetower Road, Suite G • Winterville, North Carolina 28590 Phone (704) 845-4010 • (888) 870-4133 • Fax (704) 845-4012 January 24, 2023 Evangeline M Patterson 3759 Brennan Avenue Norfolk, Virginia 23502 Re: Water Supply Abandonment Agreement Peele’s Service Station Jamesville, Martin County, North Carolina Parcel No. 0100696 Incident #10000 GRI Project No. 2516 Dear Ms. Patterson: Geological Resources, Inc. (GRI) Is currently monitoring the active incident #10000 located at 2675 Old US Highway 64. Concentrations of petroleum contaminants that exceed the North Carolina Department of Environmental Quality (NCDEQ) maximum allowable concentrations were reported in ground water samples collected from the associated monitoring well. Based on this information, GRI proposes to abandon the water supply well within 250 feet of the source area, to lower the NCDEQ risk classification of the release. It is GRI’s understanding that you are the owner of the property (2717 Old US Highway 64) identified as Parcel No. 0100696 and that water supply well (WSW-1) is located on this property. On behalf of the former owners (Peele’s Service Station) of the 2675 Old US Highway 64 site, GRI is requesting your permission to abandon the water supply well (WSW-1). Costs associated with the abandonment of your water supply well will be covered by the responsible party. We would greatly appreciate a response, even if you elect not to abandon your water supply well at this time at this time. Your cooperation in this matter will be greatly appreciated. If you have any questions, please feel free to contact me at (704) 845-4010. Sincerely, Ethan Rogerson, GIT Project Manager Water Supply Well Abandonment 2717 Old US Highway 64 Page 2 of 2 3502 Hayes Road • Monroe, North Carolina 28110 113 West Firetower Road, Suite G • Winterville, North Carolina 28590 Phone (704) 845-4010 • (888) 870-4133 • Fax (704) 845-4012 Yes, I agree to allow my water supply well to be abandon. No, I do not agree to allow my water supply well to be abandon. Signature Date (For Martin County Parcel No. 0100696) Evangeline M. Patterson ___________________________ Phone Number WSW-1 3502 Hayes Road • Monroe, North Carolina 28110 113 West Firetower Road, Suite G • Winterville, North Carolina 28590 Phone (704) 845-4010 • (888) 870-4133 • Fax (704) 845-4012 January 31, 2023 Evangeline M Patterson 3759 Brennan Avenue Norfolk, Virginia 23502 Re: Water Supply Abandonment Agreement Peele’s Service Station Jamesville, Martin County, North Carolina Parcel No. 0100696 Incident #10000 GRI Project No. 2516 Dear Ms. Patterson: Geological Resources, Inc. (GRI) Is currently monitoring the active incident #10000 located at 2675 Old US Highway 64. Concentrations of petroleum contaminants that exceed the North Carolina Department of Environmental Quality (NCDEQ) maximum allowable concentrations were reported in ground water samples collected from the associated monitoring well. Based on this information, GRI proposes to abandon the water supply well within 250 feet of the source area, to lower the NCDEQ risk classification of the release. It is GRI’s understanding that you are the owner of the property (2717 Old US Highway 64) identified as Parcel No. 0100696 and that water supply well (WSW-1) is located on this property. On behalf of the former owners (Peele’s Service Station) of the 2675 Old US Highway 64 site, GRI is requesting your permission to abandon the water supply well (WSW-1). Costs associated with the abandonment of your water supply well will be covered by the responsible party. We would greatly appreciate a response, even if you elect not to abandon your water supply well at this time at this time. Your cooperation in this matter will be greatly appreciated. If you have any questions, please feel free to contact me at (704) 845-4010. Sincerely, Ethan Rogerson, GIT Project Manager Water Supply Well Abandonment 2717 Old US Highway 64 Page 2 of 2 3502 Hayes Road • Monroe, North Carolina 28110 113 West Firetower Road, Suite G • Winterville, North Carolina 28590 Phone (704) 845-4010 • (888) 870-4133 • Fax (704) 845-4012 Yes, I agree to allow my water supply well to be abandon. No, I do not agree to allow my water supply well to be abandon. Signature Date (For Martin County Parcel No. 0100696) Evangeline M. Patterson ___________________________ Phone Number WSW-1 ROY COOPER Governor ELIZABETH S. BISER Secretary MICHAEL SCOTT Director North Carolina Department of Environmental Quality | Division of Waste Management | UST Section Washington Regional Office | 943 Washington Square Mall | Washington, NC 27889 | (252) 946-6481 April 25, 2023 North East Oil Company, Inc. ATTN: Ms. Bea Harrison Post Office Box 1386 Ahoskie, North Carolina 27910 Re: Notice of Regulatory Requirements 15A NCAC 2L .0407 Risk-based Assessment and Corrective Action for Petroleum Underground Storage Tanks Acknowledgement of Report Receipt Peele’s Service Station 2675 Old US Highway 64, Jamesville Martin County Incident Number: 10000 Risk Classification: High Ranking: H 405 R Dear Ms. Harrison: The Division of Waste Management (DWM) Underground Storage Tank (UST) Section received the Groundwater Monitoring Report dated February 13, 2023. The report has been reviewed and will be maintained in the Washington Regional Office. The report indicates continued levels of groundwater contamination in three monitoring wells. The subject incident has been determined by the Department, in response to North Carolina General Statute (NCGS) 143-215.94E(e4), to be of sufficiently high priority to allow funding by the State Trust Fund Program. Therefore, you are directed to proceed with assessment. Specifically, you are required to: • Continue to monitor groundwater quality on a semi-annual schedule. Submit the results of the groundwater sampling activities in a monitoring report to this office within 30 days of receiving the analytical results. • Install nutrient socks in necessary monitoring wells to assist with natural attenuation. • During the next sampling event, if water levels allow; conduct a comprehensive sampling of monitoring wells and water supply wells and perform a Contamination Fate and Transport Model. If water levels are not high enough, sample MW-1, MW-2R, MW-11, WSW-2, WSW-41. Effective October 1, 2004, the Department requires that all work following the submittal of the Limited Site Assessment Report (Title 15A NCAC 2L .0405) be preapproved if State Trust Fund reimbursement is anticipated. To comply with this requirement, a completed Preapproval/Claim Authorization Form, encompassing the required remedial activities, must be received in this office within 14 days of the date of this letter. Upon completion of the preapproved activities, you should submit your claim promptly. Reimbursement funds are budgeted based on completed preapprovals, but lengthy delays in reimbursement can occur if claims are not submitted immediately following work completion. Because a release or discharge has been confirmed, a Licensed Geologist or a Professional Engineer, certified by the State of North Carolina, is required to prepare and certify all reports submitted to the Department in accordance with Title 15A NCAC 2L .0103(e) and 2L .0111(b). Please note that before you sell, transfer, or request a “No Further Action” determination for a property that has not been remediated to below “unrestricted use” standards, you must file a Notice of Residual Petroleum ("Notice") with the Register of Deeds in the county where the property is located (NCGS 143B-279.9 and 143B-279.11). Failure to comply with the State's rules in the manner and time specified may result in the assessment of civil penalties and/or the use of other enforcement mechanisms. If you have any questions regarding the actions or the rules mentioned in this letter, please contact me at the address or telephone number listed below. If you have any questions regarding trust fund eligibility or reimbursement, please contact the UST Section Trust Fund Branch at (919) 733-8486. Sincerely, Allison Ward Hydrogeologist Washington Regional Office cc: GRI, Ethan Rogerson, via email Simonsen Law Firm, Mr. Lars Simonsen, PO Box 848, Edenton, NC WaRO