WA-688_9785_CA_MRP_20150827

EXECUTIVE SUMMARY

The former Red Apple Market #21 is located along NC Highway 561 West, in Saint John, Hertford
County, North Carolina. According to available information, two 1,000-gallon gasoline and one 550-
gallon gasoline underground storage tanks (USTs) were removed from the site in October 1992. In
addition, one 550-gallon gasoline UST was closed-in-place in October 1992. The site risk classification
is currently high due to the presence of potable water supply wells within a 1,000-foot radius of the site.

On July 27, 2015, GRI personnel conducted receptor survey update at the site. Three water supply wells
were identified within a 250-foot radius of the source area. Two potable water supply wells were
identified within a 1,000-foot radius of the site. A pond is located approximately 500 feet southwest of
the site.

On July 27, 2015, thirteen monitoring wells were gauged, purged and/or sampled. Concentrations of
requested method constituents that exceeded the Maximum Allowable Concentrations specified in T15A
NCAC 2L.0202 were reported in the ground water samples collected from MW-2R, MW-3R, MW-4R,
MW-5R, MW-9, MW-10 and MW-23. The concentration of benzene reported in the ground water
sample collected from MW-2R exceeded the Gross Contamination Levels (GCLs).

GRI recommends that Mobile Multi-Phase Extraction (MMPE) events and semi-annual ground water
monitoring should continue at the site until contaminant concentrations are reduced to below the GCLs.
Recovery wells could be installed in the vicinity of MW-2R and MW-4R in order to enhance the results
of the MMPE activities. The next monitoring event is tentatively scheduled for January 2016.

TABLE OF CONTENTS

1.0 SITE HISTORY AND CHARACTERIZATION .................................................................... 1
2.0 CURRENT SITE ASSESSMENT ............................................................................................ 1
3.0 UPDATED RECEPTOR SURVEY .......................................................................................... 1
4.0 GROUND WATER QUALITY ................................................................................................ 2
5.0 CONCLUSIONS AND RECOMMENDATIONS .................................................................... 3
6.0 LIMITATIONS ......................................................................................................................... 3

FIGURES
Figure 1: Site Location Map
Figure 2: Site Map
Figure 3: Water Table Surface Map
Figure 4: Ground Water Quality Map

TABLES
Table 1: Adjacent Property Owner Information
Table 2: Water Supply Well Information
Table 3: Well Construction and Gauging Information
Table 4: Summary of Ground Water Sample Analytical Results

APPENDIX
Appendix A: Laboratory Report – Ground Water Samples

1
1.0 SITE HISTORY AND CHARACTERIZATION
The Red Apple Market #21 site is located along NC Highway 561 West in Saint John, Hertford County,
North Carolina (Figure 1). According to available information, two 1,000-gallon gasoline and one 550-
gallon gasoline underground storage tanks (USTs) were removed from the site in October 1992. In
addition, one 550-gallon gasoline UST was closed-in-place in October 1992. Twenty-seven Type II
monitoring wells (MW-1 through MW-6, MW-8 through MW-23, MW-25 and MW-27 through MW-30),
one Type III monitoring well (MWD-7) and three recovery wells (RW-1, RW-2 and RW-3) were installed
at the site during past ground water assessment and remediation activities. Please note, MW-6, MW-11,
MW-12 and MW-13 have been destroyed. A total of 4,381.57 tons of contaminated soil was removed
from the site between May 16 and June 2, 2011. Prior to the May-June 2011 soil excavation, monitoring
wells MW-1 through MW-5, MWD-7 as well as recovery wells RW-1 and RW-3 were abandoned.
Monitoring wells MW-1R through MW-5R were installed following the completion of the May-June
2011 excavation activities. Ground water samples collected from monitoring wells at the site and nearby
water supply wells have exceeded the maximum allowable concentrations (MACs) during past sampling
events. Free product has been reported in MW-2, MW-3, MW-5, MW-2R, MW-3R, MW-4R and MW-
5R.

Please note that certain information contained in this report was obtained under the supervision of
previous consultants. Although Geological Resources, Inc. (GRI) cannot verify the accuracy of
information obtained from previous reports, for the purposes of this report, it is assumed to be correct.
Please refer to previous submittals for further historical information regarding the site.

2.0 CURRENT SITE ASSESSMENT
The purpose of this report is to present the results of updated receptor survey and ground water
monitoring activities conducted on July 27, 2015 at the Red Apple Market #21 site. The activities were
conducted in accordance with GRI proposal number 15-155 which was submitted to NCDENR on March
9, 2015 and approved as Task Authorization No. 9785-062 on April 7, 2015. The purpose of the
activities was to update receptor information and to obtain current ground water quality data for the site.

3.0 UPDATED RECEPTOR SURVEY
On July 27, 2015, GRI personnel conducted an updated receptor survey for the site. Twenty-five water
supply wells (WSW-2, WSW-4, WSW-5, WSW-6 and WSW-8 through WSW-28) were observed within

2
a 1,500-foot radius of the site. Please note, WSW-1, WSW-3 and WSW-7 were not located and are
assumed to have been destroyed. Three water supply wells (WSW-2, WSW-5 and WSW-6) were
identified within a 250-foot radius of the source area. Two potable water supply wells (WSW-6 and
WSW-16) were identified within a 1,000-foot radius of the site. A pond is located approximately 500 feet
southwest of the site. Municipal water is available to the site and the surrounding properties. The site is
not located within a wellhead protection area. A Site Vicinity Map showing the locations of water supply
wells and property boundaries is included as Figure 2. Adjacent property owner information is presented
in Table 1. Water supply well information is presented in Table 2.

4.0 GROUND WATER QUALITY
Thirteen monitoring wells (MW-1R through MW-5R, MW-8, MW-9, MW-10, MW-21, MW-22, MW-
23, MW-25, and MW-30) were gauged, purged and sampled on July 27, 2015. The depths to ground
water in the monitoring wells during the July 2015 sampling event ranged from 12.15 to 16.84 feet below
the tops of well casings. Ground water elevations in the Type II monitoring wells relative to mean sea
level ranged from 39.67 to 42.19 feet. Please note, the depth to water and ground water elevation for
MW-23 appear to be anomalies and were not included in the July 27, 2015 gauging data. Based on this
information, ground water flow for the site during the July 2015 gauging event was generally toward the
southwest. The average horizontal hydraulic gradient across the site was less than 0.01 feet per foot. A
Site Map showing the locations of the monitoring wells and the structures on-site and on surrounding
properties has been included as Figure 3. A Water Table Surface Map for the July 2015 sampling event
has been included as Figure 4. A summary of well construction and gauging information is presented in
Table 3.

Laboratory analyses were performed on the ground water samples collected from the above referenced
monitoring wells during the July 2015 sampling event. The collected ground water samples were
submitted for analyses of volatile organic compounds using EPA Method 6200B.

Concentrations of individual BTEX constituents, MTBE, naphthalene, 1,2-dichloroethane,
isopropylbenzene, n-propylbenzene, 1,3,5-trimethylbenzene and/or 1,2,4-trimethylbenzene that exceeded
the Maximum Allowable Concentrations (MACs) specified in T15A NCAC 2L.0202 were reported in the
ground water samples collected from MW-2R, MW-3R, MW-4R, MW-5R, MW-9, MW-10 and MW-23.
None of the contaminant concentrations exceeded the gross contamination levels (GCLs). A Ground
Water Quality Map based on data from the July 2015 sampling event has been included as Figure 5. A

3
summary of ground water sample analytical results is presented in Table 4. A complete laboratory report
has been included in Appendix A.

The absorbent boom that had been installed in MW-4R following the completion of the October 2014
MMPE event was removed prior to when MW-4R was gauged, purged and sampled on July 27, 2015 and
was not re-installed.

5.0 CONCLUSIONS AND RECOMMENDATIONS
 Twenty-five water supply wells were observed within a 1,500-foot radius of the site during July
2015 updated receptor survey activities. Three water supply wells were identified within a 250-
foot radius of the source area. Two potable water supply wells were identified within a 1,000-
foot radius of the site. A pond is located approximately 500 feet southwest of the site.
 The average depth to ground water in the monitoring wells during the July 2015 sampling event
was 13.95 feet. Ground water flow for the site during the July 2015 gauging event was generally
toward the southwest with an average horizontal hydraulic gradient of less than 0.01 feet per foot.
 Concentrations of individual BTEX constituents, MTBE, naphthalene, 1,2-dichloroethane,
isopropylbenzene, n-propylbenzene, 1,3,5-trimethylbenzene and/or 1,2,4-trimethylbenzene that
exceeded the MACs were reported in the ground water samples collected from MW-2R, MW-3R,
MW-4R, MW-5R, MW-9, MW-10 and MW-23. The concentration of benzene reported in the
ground water sample collected from MW-2R exceeded the GCL.
 The absorbent boom that had been installed in MW-4R following the completion of the October
2014 MMPE event was removed prior to gauging on July 27, 2015. The boom was not replaced
following the completion of the July 2015 sampling activities.
 GRI recommends that Mobile Multi-Phase Extraction (MMPE) events and semi-annual ground
water monitoring should continue at the site until contaminant concentrations are reduced to
below the GCLs. Recovery wells could be installed in the vicinity of MW-2R and MW-4R in
order to enhance the results of the MMPE activities. The next monitoring event is tentatively
scheduled for January 2016.
6.0 LIMITATIONS
This report has been prepared for the exclusive use of Red Apple Markets, Inc. for specific application to
the referenced site in Hertford County, North Carolina. The assessment was conducted based on the
scope of work and level of effort desired by NCDENR and with resources adequate only for that scope of
work. Our findings have been developed in accordance with generally accepted standards of

4
environmental practices in the State of North Carolina, available information, and our professional
judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would be
interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data. Please note that field data collected prior
to the July 2007 sampling and updated receptor survey event was not obtained under the supervision of
GRI. Although the accuracy of this information cannot be verified, for the purpose of this report GRI
assumes that it is correct.

FIGURES

TABLES
Date: 08/18/15 Facility ID #: 0-030290
Parcel ID Number Property Owner Name Mailing Address
5963-35-4820 (Site)St. John Fire Department, Inc.1127 NC Highway 561 West
Aulander, North Carolina 27805
5963-35-5721 Kathleen Dare Maxham 1117 NC Highway 561 West
Aulander, North Carolina 27805
5963-35-2699 St. John Fire Department, Inc.1127 NC Highway 561 West
Aulander, North Carolina 27805
5963-36-3072 Enrico Mineo 1407 W. First Street
Ahoskie, North Carolina 27910
5963-36-4052 Fred L. Liverman 415 N Curtis Street
Ahoskie, North Carolina 27910
5963-35-4976 Cuttiwhiskey Enterprises, Inc.137 Albemarle Avenue
Ahoskie, North Carolina 27910
Notes:
• Parcel ID Numbers are keyed to Figure 2.
TABLE 1
ADJACENT PROPERTY OWNER INFORMATION
RED APPLE MARKET #21 (INCIDENT NO. 9785)
Facility ID #: 0-030290
Well ID.Parcel ID Number Well Owner Mailing Address Well Address
Well Use
(Potable / Non-
Potable
etc.)
Municipal Water
Connected?
Distance from source
area of release (ft.)
WSW-2 5963-35-5721 Kathleen Dare Maxham 1117 NC Highway 561 West
Aulander, North Carolina 27805
1117 NC Highway 561 West
Aulander, North Carolina 27805 Not In Use Yes 170 SE
WSW-4 5963-36-3072 Enrico Mineo 1407 W. First Street
Ahoskie, North Carolina 27910
1124 NC Highway 561 West
Aulander, North Carolina 27805 Not In Use Yes 260 N
WSW-5 5963-36-4052 Fred L. Liverman 415 N Curtis Street
Ahoskie, North Carolina 27910
1122 NC Highway 561 West
Aulander, North Carolina 27805 Not In Use Yes 220 N
WSW-6 5963-36-5001 Sondra R. Salter Post Office Box 147
Sunbury, North Carolina 27979 Not Listed Potable No 200 N
WSW-8 5963-35-5451 Yvonne M. Williams 106 Rountree Lane
Aulander, North Carolina 27805
106 Rountree Lane
Aulander, North Carolina 27805 Not In Use Yes 400 SE
WSW-9 5963-35-8675 Bryan and Sondra R. Salter Post Office Box 147
Sunbury, North Carolina 27979
1111 NC Highway 561 West
Aulander, North Carolina 27805 Not In Use Yes 450 SE
WSW-10 5963-25-7761 Richard and Brenda Spence 1135 NC Highway 561 West
Aulander, North Carolina 27805
1135 NC Highway 561 West
Aulander, North Carolina 27805 Not In Use Yes 560 W
WSW-11 5963-26-9257 Joseph P. and Martha Askew 113 Menola Saint John Road
Ahoskie, North Carolina 27910 Not Listed Not In Use Yes 640 NW
WSW-12 5963-36-4418 Joseph P., Jr. and Cheyrl Askew 113 Menola Saint John Road
Ahoskie, North Carolina 27910
111 Menola Street John Road
Ahoskie, North Carolina 27910 Not In Use Yes 590 N
WSW-13 5963-25-7997 Brenda Overton Edwards 1134 NC Highway 561 West
Aulander, North Carolina 27805
1134 NC Highway 561 West
Aulander, North Carolina 27805 Not In Use Yes 620 NW
WSW-14 5963-25-6976 Brenda E. Piland 1134 NC Highway 561 West
Aulander, North Carolina 27805
1138 NC Highway West
Aulander, North Carolina 27805 Not In Use Yes 700 NW
WSW-15 5963-25-5936 Robert Preston Davis 1140 NC Highway 561 West
Aulander, North Carolina 27805
1140 NC Highway 561 West
Aulander, North Carolina 27805 Not In Use Yes 820 NW
WSW-16 5963-25-3698 Lee Hunter Joyner 1141 NC Highway 561 West
Aulander, North Carolina 27805
1141 NC Highway 561 West
Aulander, North Carolina 27805 Potable No 990 W
TABLE 2
WATER SUPPLY WELL INFORMATION
RED APPLE MARKET #21 (INCIDENT NO. 9785)
Date: 08/18/15
Page 1 of 2
Facility ID #: 0-030290
Well ID.Parcel ID Number Well Owner Mailing Address Well Address
Well Use
(Potable / Non-
Potable
etc.)
Municipal Water
Connected?
Distance from source
area of release (ft.)
TABLE 2
WATER SUPPLY WELL INFORMATION
RED APPLE MARKET #21 (INCIDENT NO. 9785)
Date: 08/18/15
WSW-17 5963-25-3922 Ronald and Kay B. Edwards 1144 NC Highway 561 West
Aulander, North Carolina 27805
1144 NC Highway 561 West
Aulander, North Carolina 27805 Potable No 1,150 NW
WSW-18 5963-26-0382 Ronald and Richward Edwards 1144 NC Highway 561 West
Aulander, North Carolina 27805 Not Listed Potable No 1,250 NW
WSW-19 5963-15-8937 Sarah L. Morris 1204 NC Highway 561 West
Aulander, North Carolina 27805
1154 NC Highway 561 West
Aulander, North Carolina 27805 Not In Use Yes 1,500 NW
WSW-20 5963-15-9569 Joyner Farms, Inc.1147 NC Highway 561 West
Aulander, North Carolina 27805
1147 NC Highway 561 West
Aulander, North Carolina 27805 Non-Potable Yes 1,410 SW
WSW-21 5963-23-9979 Joyner Farms, Inc.1147 NC Highway 561 West
Aulander, North Carolina 27805
118 Mallard Lane
Aulander, North Carolina 27805 Non-Potable Yes 1,100 SW
WSW-22 5963-32-4689 Sondra R. Salter Post Office Box 147
Sunbury, North Carolina 27979
1101 NC Highway 561 West
Aulander, North Carolina 27805 Non-Potable Yes 830' SE
WSW-23 5963-45-3347 Richard and Wanda G. Perry 137 McCaskey Road
Ahoskie, North Carolina 27910
1053 NC Highway 561 West
Aulander, North Carolina 27805 Not In Use Yes 990 SE
WSW-24 5963-45-3835 Stanley and Raymond Jenkins 854 NC Highway 561 West
Aulander, North Carolina 27805
1647 NC Highway 461
Ahoskie, North Carolina 27910 Not In Use Yes 1,080 E
WSW-25 5963-46-4078 St. Johns Baptist Church, Inc. 1644 NC Highway 461
Ahoskie, North Carolina 27910
1645 NC Highway 461
Ahoskie, North Carolina 27910 Not In Use Yes 1,000 NE
WSW-26 5963-46-1178 St. Johns Baptist Church, Inc. 1644 NC Highway 461 West
Ahoskie, North Carolina 27910
1650 NC Highway 461
Ahoskie, North Carolina 27910 Not In Use Yes 750 NE
WSW-27 5963-46-2260 Thornton C. and Devonia A. Askew 1648 NC Highway 461 West
Ahoskie, North Carolina 27910
1648 NC Highway 461
Ahoskie, North Carolina 27910 Not In Use Yes 860 NE
WSW-28 5963-37-2178 Denise Britton Post Office Box 93
Ahoskie, North Carolina 27910
123 Menola Saint John Road
Aulander, North Carolina 27805 Not In Use Yes 1,400 N
Notes:
• Water Supply Wells are keyed to Figure 2.
Page 2 of 2
01/18/07 12.87 0.00 87.13      
06/06/07 13.15 0.00 86.85
06/02/08 14.10 0.00 85.90
12/18/08 16.41 0.00 83.59
03/24/09 14.62 0.00 85.38
06/25/09 15.00 0.00 85.00
09/16/09 15.58 0.02 84.44 Before AFVR
09/16/09 15.64 0.00 84.36 After AFVR
09/21/09 15.66 0.00 84.34
11/17/09 15.42 0.00 84.58 Before AFVR
11/17/09 15.55 0.01 84.46 After AFVR
12/30/09 14.85 0.00 85.15
06/28/10 14.02 0.00 85.98
10/05/10 14.74 0.00 85.26 Abandoned
10/12/11 15.73 0.00 39.03
01/31/12 15.71 0.00 39.05
05/15/12 14.77 0.00 39.99
01/22/13 14.68 0.00 40.08
11/18/13 15.84 0.00 38.92
05/27/14 14.36 0.00 40.40
01/29/15 14.53 0.00 40.23
07/27/15 14.96 0.00 39.80
01/18/07 14.81 3.25 87.58
06/06/07 13.07 0.69 87.12
06/02/08 15.20 2.27 86.35
11/06/08 16.90 2.60 84.93 Before AFVR
11/06/08 15.04 0.16 84.70 After AFVR
12/18/08 15.25 0.69 84.94
03/24/09 16.90 3.54 85.74
06/10/09 15.84 2.12 85.58 Before AFVR
06/10/06 14.29 0.01 85.32 After AFVR
06/25/09 14.90 0.46 85.09
09/16/09 14.85 1.17 85.75 Before AFVR
09/16/09 15.05 0.00 84.55 After AFVR
09/21/09 15.07 0.03 84.56
11/17/09 15.44 0.59 84.67 Before AFVR
11/17/09 14.98 0.02 84.64 After AFVR
12/30/09 14.65 0.33 85.23
06/28/10 15.65 2.04 85.70
10/05/10 15.81 2.79 86.18 Abandoned
10/12/11 14.71 0.00 39.18
01/31/12 14.67 0.22 39.41
05/15/12 13.96 0.23 40.13
12/17/12 15.25 0.75 39.28 Before MMPE
12/21/12 17.94 0.00 35.95 After MMPE
01/22/13 13.85 0.00 40.04
10/07/13 15.00 0.00 38.89 Before MMPE
10/11/13 15.99 0.00 37.90 After MMPE
11/18/13 14.95 0.00 38.94
04/28/14 13.22 0.00 40.67 Before MMPE
05/02/14 16.95 0.00 36.94 After MMPE
05/27/14 13.71 0.00 40.18
10/13/14 14.48 0.00 39.41 Before MMPE
10/17/14 16.70 0.00 37.19 After MMPE
01/29/15 13.86 0.00 40.03
07/27/15 14.18 0.00 39.71
01/18/07 14.02 0.00 86.99
06/06/07 13.86 0.00 87.15
06/02/08 14.77 0.00 86.24
12/18/08 16.27 0.00 84.74
03/24/09 15.90 0.00 85.11
06/25/09 15.80 0.00 85.21
09/16/09 16.72 0.02 84.31 Before AFVR
09/16/09 16.40 0.01 84.62 After AFVR
09/21/09 16.40 0.00 84.61
11/17/09 16.77 0.00 84.24 Before AFVR
11/17/09 16.40 0.01 84.62 After AFVR
12/30/09 13.97 0.00 87.04
06/28/10 15.76 0.00 85.25
10/05/10 15.50 0.00 85.51 Abandoned
10/12/11 14.48 0.00 40.12
01/31/12 15.88 0.00 38.72
05/15/12 14.31 0.00 40.29
12/17/12 14.54 0.00 40.06 Before MMPE
12/21/12 11.85 0.30 43.01 After MMPE
01/22/13 15.09 0.00 39.51
10/07/13 16.20 0.00 38.40 Before MMPE
10/11/13 11.58 0.00 43.02 After MMPE
11/18/13 16.48 0.00 38.12
04/28/14 13.75 0.00 40.85 Before MMPE
05/02/14 10.23 0.00 44.37 After MMPE
05/27/14 16.74 0.00 37.86
10/13/14 15.23 0.00 39.37 Before MMPE
10/17/14 11.74 0.00 42.86 After MMPE
01/29/15 14.62 0.00 39.98
07/27/15 14.61 0.00 39.99
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y
ft. BGS)
20
2010-2010
MW-3 05/07/93 10 10-20 20
10/12/11MW-3R
Ground
Water
Elevation*
(ft.)
27 100.00
Top of
Casing
Elevation*
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
Comments
TABLE 3
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET # 21 (INCIDENT NO. 9785)
Date: 08/04/15 Facility ID # : 0-030290
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Bottom
of Well
(ft. BGS)
MW-1 05/06/93 7 7-27
MW-2 05/07/93 10 10-20
10/12/11MW-1R
101.01
10/12/11MW-2R 10-20
99.60
54.76
54.602010-2010
53.892010
Page 1 of 6
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y
ft. BGS)
Ground
Water
Elevation*
(ft.)
Top of
Casing
Elevation*
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
Comments
TABLE 3
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET # 21 (INCIDENT NO. 9785)
Date: 08/04/15 Facility ID # : 0-030290
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Bottom
of Well
(ft. BGS)
01/18/07 12.69 0.00 87.37
06/14/07 13.06 0.00 87.00
06/02/08 NM NM NM Destroyed
10/12/11 13.28 0.13 40.85
01/31/12 13.12 0.29 41.15
05/15/12 14.13 0.51 40.33
01/22/13 14.22 0.30 40.06
10/07/13 15.16 0.43 39.23 Before MMPE
10/11/13 11.65 0.03 42.40 After MMPE
11/18/13 14.86 0.01 39.17
04/28/14 11.21 0.00 42.81 Before MMPE
05/02/14 11.55 0.45 42.86 After MMPE
05/27/14 13.58 0.00 40.44
10/13/14 15.08 0.02 38.96 Before MMPE
10/17/14 13.64 0.09 40.46 After MMPE
01/29/15 14.15 0.00 39.87
07/27/15 14.00 0.00 40.02
01/18/07 13.02 0.00 87.80
06/06/07 13.23 0.00 87.59
06/02/08 NM NM NM Not Located
12/18/08 NM NM NM Dry
03/24/09 NM NM NM Dry
06/25/09 NM NM NM Dry
09/21/09 15.47 0.00 85.35
12/30/09 14.44 0.00 86.38
06/28/10 13.99 0.00 86.83
10/05/10 14.60 0.00 86.22 Abandoned
10/12/11 14.16 0.02 40.32
01/31/12 15.36 0.00 39.10
05/15/12 14.20 0.00 40.26
12/17/12 14.57 0.00 39.89 Before MMPE
12/21/12 14.10 0.00 40.36 After MMPE
01/22/13 14.45 0.00 40.01
11/18/13 15.44 0.00 39.02
04/28/14 13.97 0.00 40.49 Before MMPE
05/02/14 13.75 0.00 40.71 After MMPE
05/27/14 13.98 0.00 40.48
10/13/14 14.85 0.00 39.61 Before MMPE
10/17/14 14.90 0.00 39.56 After MMPE
01/29/15 14.20 0.00 40.26
07/27/15 14.35 0.00 40.11
MW-6 NA 01/18/07 NA NA NA 100.49 NM NM NM Destroyed
01/18/07 12.35 0.00 87.45
06/06/07 12.43 0.00 87.37
06/02/08 21.80 0.00 78.00
12/18/08 15.27 0.00 84.53
03/24/09 14.55 0.00 85.25
06/25/09 14.85 0.00 84.95
09/21/09 15.52 0.00 84.28
12/30/09 14.70 0.00 85.10
06/28/10 13.87 0.00 85.93
10/05/10 NM NM NM Abandoned
01/18/07 8.59 0.00 92.27
06/06/07 12.87 0.00 87.99
06/02/08 NM NM NM Not Located
12/18/08 17.22 0.00 83.64
03/24/09 4.97 0.00 95.89
06/25/09 16.10 0.00 84.76
09/21/09 17.35 0.00 83.51
12/30/09 6.28 0.00 94.58
06/28/10 14.79 0.00 86.07
10/05/10 12.08 0.00 88.78
10/12/11 16.24 0.00 38.52
01/31/12 11.46 0.00 43.30
05/15/12 13.32 0.00 41.44
11/18/13 15.30 0.00 39.46
05/27/14 12.74 0.00 42.02
01/29/15 9.76 0.00 45.00
07/27/15 12.60 0.00 42.16
35 99.80
100.86
54.76
19
MW-5 NA NA NA
MW-5R
NA
MW-4 NA
MWD-7 02/08/94 30 30-35
100.82
NA NA NA
54.022010-201010/12/11MW-4R
100.06
9-19903/14/94MW-8
54.462010-201010/12/11
Page 2 of 6
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y
ft. BGS)
Ground
Water
Elevation*
(ft.)
Top of
Casing
Elevation*
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
Comments
TABLE 3
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET # 21 (INCIDENT NO. 9785)
Date: 08/04/15 Facility ID # : 0-030290
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Bottom
of Well
(ft. BGS)
01/18/07 7.73 0.00 92.95
06/06/07 9.35 0.00 91.33
06/02/08 8.21 0.00 92.47
12/18/08 11.72 0.00 88.96
03/24/09 11.60 0.00 89.08
06/25/09 11.73 0.00 88.95
09/21/09 12.62 0.00 88.06
12/30/09 12.24 0.00 88.44
06/28/10 12.40 0.00 88.28
10/05/10 12.69 0.00 87.99
10/12/11 10.00 0.00 44.67
01/31/12 10.59 0.00 44.08
05/15/12 9.94 0.00 44.73
12/17/12 10.88 0.00 43.79 Before MMPE
12/21/12 9.41 0.00 45.26 After MMPE
01/22/13 5.34 0.00 49.33
11/18/13 11.49 0.00 43.18
05/27/14 9.64 0.00 45.03
01/29/15 10.94 0.00 43.73
07/27/15 12.48 0.00 42.19
01/18/07 14.26 0.00 86.86
06/06/07 14.38 0.00 86.74
06/02/08 15.50 0.00 85.62
12/18/08 16.62 0.00 84.50
03/24/09 15.99 0.00 85.13
06/25/09 16.16 0.00 84.96
09/21/09 16.85 0.00 84.27
12/30/09 15.98 0.00 85.14
06/28/10 15.45 0.00 85.67
10/05/10 15.97 0.00 85.15
10/12/11 16.40 0.00 38.81
01/31/12 16.05 0.00 39.16
05/15/12 NS NS NS Inaccessable
01/22/13 15.50 0.00 39.71
11/18/13 16.48 0.00 38.73
05/27/14 15.12 0.00 40.09
01/29/15 15.34 0.00 39.87
07/27/15 15.66 0.00 39.55
MW-11 NA 01/18/07 NA NA NA 100.08 NM NM NM Destroyed
MW-12 NA 01/18/07 NA NA NA 99.49 NM NM NM Destroyed
01/18/07 12.72 0.00 87.11
06/06/07 12.83 0.00 87.00 Destroyed
01/18/07 13.78 0.00 87.59
06/06/07 13.93 0.00 87.44
06/02/08 14.90 0.00 86.47
12/18/08 16.49 0.00 84.88
03/24/09 13.73 0.00 87.64
06/25/09 15.85 0.00 85.52
09/21/09 16.60 0.00 84.77
12/30/09 15.92 0.00 85.45
06/28/10 14.92 0.00 86.45
10/05/10 15.83 0.00 85.54
10/12/11 16.28 0.00 39.11
01/31/12 16.00 0.00 39.39
01/22/13 15.44 0.00 39.95
11/18/13 16.22 0.00 39.17
05/27/14 14.91 0.00 40.48
01/29/15 15.18 0.00 40.21
01/18/07 14.32 0.00 87.66
06/06/07 14.43 0.00 87.55
06/02/08 15.47 0.00 86.51
12/18/08 NM NM NM Not Sampled
03/24/09 16.26 0.00 85.72
06/25/09 16.38 0.00 85.60
09/21/09 17.10 0.00 84.88
12/30/09 NM NM NM Not Sampled
06/28/10 15.42 0.00 86.56
10/05/10 16.35 0.00 85.63
10/12/11 16.79 0.00 39.22
01/31/12 16.55 0.00 39.46
11/18/13 16.75 0.00 39.26
05/27/14 15.42 0.00 40.59
01/29/15 15.71 0.00 40.30
22
55.39
MW-15 NA NA
101.98
101.37
NA
56.01
MW-14
100.68
101.12
55.21
21
54.67
MW-13 NA NA NA NA 99.83
04/05/95 12-22
MW-10
9-199
NA
12
1903/14/94MW-9
11-211103/14/94
Page 3 of 6
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y
ft. BGS)
Ground
Water
Elevation*
(ft.)
Top of
Casing
Elevation*
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
Comments
TABLE 3
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET # 21 (INCIDENT NO. 9785)
Date: 08/04/15 Facility ID # : 0-030290
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Bottom
of Well
(ft. BGS)
01/18/07 NM NM NM
06/06/07 13.34 0.00 87.56
06/02/08 NM NM NM NA
12/18/08 NM NM NM Not Sampled
03/24/09 15.31 0.00 85.59
06/25/09 15.31 0.00 85.59
09/21/09 NM NM NM Not Sampled
12/30/09 NM NM NM Not Sampled
06/28/10 NM NM NM Not Sampled
10/05/10 15.28 0.00 85.62
10/12/11 15.70 0.00 39.18
01/31/12 15.46 0.00 39.42
11/18/13 NM NM NM Not Sampled
05/27/14 14.40 0.00 40.48
01/29/15 NM NM NM Not Sampled
01/18/07 NM NM NM
06/06/07 11.93 0.00 87.36
06/02/08 NM NM NM NA
12/18/08 NM NM NM Not Sampled
03/24/09 13.81 0.00 85.48
06/25/09 13.84 0.00 85.45
09/21/09 NM NM NM Not Sampled
12/30/09 NM NM NM Not Sampled
06/28/10 NM NM NM Not Sampled
10/05/10 13.82 0.00 85.47
10/12/11 14.33 0.00 39.28
01/31/12 14.07 0.00 39.54
11/18/13 NM NM NM Not Sampled
05/27/14 12.49 0.00 41.12
01/29/15 NM NM NM Not Sampled
01/18/07 14.09 0.00 87.89
06/06/07 14.38 0.00 87.60
06/02/08 15.24 0.00 86.74
12/18/08 16.68 0.00 85.30
03/24/09 16.04 0.00 85.94
06/25/09 16.19 0.00 85.79
09/21/09 16.92 0.00 85.06
12/30/09 16.01 0.00 85.97
06/28/10 15.38 0.00 86.60
10/05/10 NM NM NM
10/12/11 16.46 0.00 38.83
01/31/12 16.14 0.00 39.15
05/15/12 NS NS NS Inaccessable
11/18/13 16.46 0.00 38.83
05/27/14 15.23 0.00 40.06
01/29/15 15.42 0.00 39.87
01/18/07 13.14 0.00 86.80
06/06/07 13.27 0.00 86.67
06/02/08 14.15 0.00 85.79
12/18/08 15.52 0.00 84.42
03/24/09 14.81 0.00 85.13
06/25/09 15.03 0.00 84.91
09/21/09 15.73 0.00 84.21
12/30/09 14.87 0.00 85.07
06/28/10 14.19 0.00 85.75
10/05/10 NM NM NM
10/12/11 15.30 0.00 38.76
01/31/12 15.01 0.00 39.05
05/15/12 NS NS NS Inaccessable
11/18/13 15.33 0.00 38.73
05/27/14 14.55 0.00 39.51
01/29/15 12.48 0.00 41.58
01/18/07 12.86 0.00 86.93
06/06/07 13.25 0.00 86.54
06/02/08 14.07 0.00 85.72
12/18/08 15.46 0.00 84.33
03/24/09 14.75 0.00 85.04
06/25/09 14.98 0.00 84.81
09/21/09 15.40 0.00 84.39
12/30/09 14.88 0.00 84.91
06/28/10 14.23 0.00 85.56
10/05/10 NM NM NM
10/12/11 15.28 0.00 38.80
01/31/12 15.02 0.00 39.06
05/15/12 14.20 0.00 39.88
11/18/13 15.30 0.00 38.78
05/27/14 NM NM NM Inaccessable
01/29/15 14.22 0.00 39.86
MW-20 04/10/95 10
MW-18 04/07/95 10 22
55.29
NA NA
54.88
MW-17 NA
54.06
MW-19 04/07/95 10
100.90
NA
54.08
99.79
NA NA NA
53.61
99.94
101.98
10-22
MW-16
2210-22
NA
22
99.29
10-22
Page 4 of 6
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y
ft. BGS)
Ground
Water
Elevation*
(ft.)
Top of
Casing
Elevation*
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
Comments
TABLE 3
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET # 21 (INCIDENT NO. 9785)
Date: 08/04/15 Facility ID # : 0-030290
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Bottom
of Well
(ft. BGS)
01/18/07 14.18 0.00 86.51
06/06/07 13.97 0.00 86.72
06/02/08 14.95 0.00 85.74
12/18/08 16.25 0.00 84.44
03/24/09 15.56 0.00 85.13
06/25/09 15.80 0.00 84.89
09/21/09 16.55 0.00 84.14
12/30/09 16.62 0.00 84.07
06/28/10 15.07 0.00 84.93
10/05/10 15.59 0.00 85.10
10/12/11 16.22 0.00 38.62
01/31/12 15.54 0.00 39.30
05/15/12 15.00 0.00 39.84
01/22/13 15.16 0.00 39.68
11/18/13 16.19 0.00 38.65
05/27/14 14.83 0.00 40.01
01/29/15 14.83 0.00 40.01
07/27/15 15.17 0.00 39.67
06/02/08 16.13 0.00 NM
12/18/08 NM NM NM
05/15/12 15.80 0.00 NM
11/18/13 16.88 0.00 NM
05/27/14 NM NM NM Not Sampled
01/29/15 15.58 0.00 NM
07/27/15 16.84 0.00 NM
06/02/08 1.69 0.00 NM
12/18/08 NM NM NM
10/12/11 NM NM NM
05/15/12 0.68 0.00 54.09
11/18/13 1.50 0.00 53.27
05/27/14 2.04 0.00 52.73
01/29/15 0.26 0.00 54.51
07/27/15 1.54 0.00 53.23
03/24/09 12.41 0.00 85.25
06/25/09 12.78 0.00 84.88
09/21/09 13.42 0.00 84.24
12/30/09 12.54 0.00 85.12
06/28/10 11.88 0.00 85.78
10/05/10 12.52 0.00 85.14
10/12/11 12.98 0.00 38.89
01/31/12 12.62 0.00 39.25
05/15/12 11.94 0.00 39.93
11/18/13 12.99 0.00 38.88
05/27/14 11.72 0.00 40.15
01/29/15 11.90 0.00 39.97
07/27/15 12.15 0.00 39.72
03/24/09 16.33 0.00 83.26
06/25/09 13.47 0.00 86.12
09/21/09 NM NM NM Not Sampled
12/30/09 11.74 0.00 87.85
06/28/10 11.10 0.00 88.49
10/05/10 10.50 0.00 89.09
10/12/11 13.03 0.00 40.71
01/31/12 11.45 0.00 42.29
11/18/13 14.23 0.00 39.51
05/27/14 12.05 0.00 41.69
01/29/15 11.21 0.00 42.53
03/24/09 18.06 0.00 82.13
06/25/09 15.00 0.00 85.19
09/21/09 15.65 0.00 84.54
12/30/09 14.96 0.00 85.23
06/28/10 13.96 0.00 86.23
10/05/10 14.68 0.00 85.51
10/12/11 15.25 0.00 39.05
01/31/12 14.89 0.00 39.41
11/18/13 15.19 39.11 39.11
05/27/14 12.53 0.00 41.77
01/29/15 12.60 0.00 41.70
03/24/09 14.55 0.00 85.67
06/25/09 15.20 0.00 85.02
09/21/09 NM NM NM Not Sampled
12/30/09 15.14 0.00 85.08
06/28/10 14.30 0.00 85.92
10/05/10 15.00 0.00 85.22
10/12/11 54.34 NM NM NM Destroyed
2010-2010
53.74
100.19
54.30
100.69
MW-21
51.87
20
03/24/09 10
MW-29 03/24/09 10 10-20 20 100.22
2010-20
54.84
2210-221004/10/95
03/24/09MW-25
54.77
NANANANAMW-23
MW-27
97.66
NM
NMNANANA
10 10-20MW-28 03/24/09
NAMW-22
99.59
Page 5 of 6
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y
ft. BGS)
Ground
Water
Elevation*
(ft.)
Top of
Casing
Elevation*
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
Comments
TABLE 3
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET # 21 (INCIDENT NO. 9785)
Date: 08/04/15 Facility ID # : 0-030290
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Bottom
of Well
(ft. BGS)
03/24/09 13.10 0.00 85.77
06/25/09 13.92 0.00 84.95
09/21/09 14.62 0.00 84.25
12/30/09 13.84 0.00 85.03
06/28/10 13.04 0.00 85.83
10/05/10 13.72 0.00 85.15
10/12/11 14.16 0.00 38.86
01/31/12 13.84 0.00 39.18
05/15/12 13.12 0.00 39.90
11/18/13 14.17 0.00 38.85
05/27/14 12.88 0.00 40.14
01/29/15 13.04 0.00 39.98
07/27/15 13.29 0.00 39.73
Notes:
•  *: Reference point for elevation measurements; assumed elevation 100.00 feet.
•  **: If free product is present in a well, ground water elevation should be calculated by: (Top of Casing Elevation - Depth to Water) +
   (Free Product Thickness x 0.8581)
•  ft BGS : feet below ground surface.
•  NA: Not Available.
•  NM:  Not Measured.
•  Well construction details for monitoring wells installed prior to March 2009 are reproduced from well identification tags, where available.
98.87
03/24/09MW-30
53.02
2010-2010
Page 6 of 6
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 70 6 0.4 70 70 400 400
5,000 260,000 84,500 85,500 20,000 70,000 6,000 400 25,000 30,000 28,500 25,000
01/18/07 46.4 5.51 58.8 28.72 25.7 2.54 34.3 NR NR NR NR NR
06/06/07 68.3 4.56 85.7 32.6 21.6 <0.500 43.9 <0.500 9.60 15.9 36.9 6.60
06/02/08 16.5 1.20 21.2 8.35 38.5 0.320 I 9.23 <1.0 2.98 2.98 6.97 1.54
12/18/08 13 <0.50 10 4.9 14 <1.0 5.9 B <0.75 2.1 J 2.4 J 6.2 1.7 J
03/24/09 44 15 40 23 16 <1.6 19 <1.6 6.8 7.4 4.2 J 2.9 J
06/25/09 6.32 <0.330 7.99 <1.33 10.5 <1.67 3.14 <.0330 1.10 J 1.31 0.840 J <0.330
09/21/09 18.5 <0.190 9.24 1.30 12.7 <0.200 3.10 <0.220 1.17 1.74 0.701 J <0.180
12/30/09 26.1 2.13 5.26 3.14 15.1 <0.200 3.51 <0.220 2.04 1.79 1.87 <0.180
06/28/10 20.1 0.618 J 12.2 2.51 11.4 <0.400 7.66 <0.440 2.38 1.23 J 1.71J 0.464 J
10/05/10 32.6 2.78 16.0 8.47 8.91 <0.200 5.69 <0.220 3.87 3.78 5.51 0.85
10/12/11 <0.13 <0.13 <0.15 <0.30 2.1 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 1.2 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
05/15/12 <0.13 <0.13 <0.15 <0.30 0.16 J <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/22/13 <0.10 <0.10 <0.10 <0.22 1.0 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
11/18/13 <0.10 <0.10 <0.10 <0.22 1.1 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 1.0 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
01/29/15 <0.17 <0.17 <0.15 <0.43 0.80 <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
07/27/15 <0.17 <0.17 <0.15 <0.43 0.91 <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
01/18/07 FP FP FP FP FP FP FP FP FP FP FP FP
06/06/07 FP FP FP FP FP FP FP FP FP FP FP FP
06/02/08 FP FP FP FP FP FP FP FP FP FP FP FP
12/18/08 FP FP FP FP FP FP FP FP FP FP FP FP
03/24/09 FP FP FP FP FP FP FP FP FP FP FP FP
06/25/09 FP FP FP FP FP FP FP FP FP FP FP FP
09/21/09 FP FP FP FP FP FP FP FP FP FP FP FP
12/30/09 FP FP FP FP FP FP FP FP FP FP FP FP
06/28/10 FP FP FP FP FP FP FP FP FP FP FP FP
10/05/10 FP FP FP FP FP FP FP FP FP FP FP FP
10/12/11 9,780 9,700 2,440 10,100 1,220 46.3 J 769 120 146 373 2,390 634
01/31/12 FP FP FP FP FP FP FP FP FP FP FP FP
05/15/12 FP FP FP FP FP FP FP FP FP FP FP FP
01/22/13 3,250 7,990 2,070 11,900 519 14.8 J 2,020 50.7 200 703 4,350 1,440
11/18/13 6,580 7,930 2,100 13,800 731 28.8 J 841 97.9 J 122 397 3,740 878
05/27/14 4,160 4,880 1,400 10,500 657 22.3 J 758 73.2 105 263 3,220 879
01/29/15 4,350 3,670 1,360 7,130 739 29.9 J 555 79.6 99.5 285 2,010 597
07/27/15 6,350 3,210 1,730 7,550 1,090 43.7 J 732 123 114 319 2,250 641
01/18/07 1,940 5.14 34.3 <15.0 3,800 17.0 <25.0 NR NR NR NR NR
06/06/07 3,030 6.18 69.0 7.61 4,880 16.9 40.3 <0.500 13.7 18.0 3.22 2.92
06/02/08 2,500 4.95 126 14.2 5,490 18.3 60.8 9.44 12.8 18.5 6.14 <1.0
12/18/08 1,700 2.1 J 33 2.6 J 4,200 E <1.0 24 B 8.4 9.1 10 1.1 J 1.3 J
03/24/09 2,900 <16 110 140 J 4,900 20 J 69 J <16 20 J 24 J 26 J <16
06/25/09 2,140 10.3 J 56.4 32.9 J 4,110 <33.4 40 J <6.60 <20 11.2 J 19.4 J <6.60
09/21/09 2,180 <7.60 56.2 <8.80 5,040 18.6 J 69.3 <8.80 13.8 J 22.1 J <6.00 <7.20
12/30/09 1,580 2.29 J 41.1 <1.10 4,200 14.5 23.3 6.35 7.99 7.71 <0.750 <0.900
06/28/10 1,780 <9.50 54.0 <11.0 5,040 <10.0 26.2J <11.0 <7.50 <11.0 <7.50 <9.00
10/05/10 1,830 <9.50 47.8 J <11.0 4,010 18.2 J <25.0 <11.0 11.8 J 14.5 J <7.50 <9.00
10/12/11 3.4 6.1 1.7 6.2 0.36 J <0.11 0.46 J <0.16 0.17 J 0.47 J 1.8 0.67
01/31/12 36.6 2.9 17.9 28.4 6.2 <0.11 0.21 J <0.16 1.8 3.5 12.9 3.8
05/15/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/22/13 22.1 2.1 19.1 16.2 8.1 <0.10 0.68 <0.10 1.8 4.1 7.6 3.6
11/18/13 12.6 1.4 17.1 14.0 5.9 <0.10 1.2 <0.10 1.9 4.4 11.9 4.6
05/27/14 4.2 <0.10 0.85 0.74 J 5.9 <0.10 0.27 J <0.10 0.44 J 0.56 0.58 <0.10
01/29/15 3.8 0.28 J 4.7 0.68 J 6.5 <0.16 0.18 J <0.16 0.78 1.5 0.29 J 0.15 J
07/27/15 1.9 0.30 J 1.1 1.0 J 5.5 <0.16 0.28 J <0.16 0.32 J 0.32 J 0.50 0.18 J
01/18/07 14,900 5,650 1,330 4,850 16,100 288 436 NR NR NR NR NR
06/14/07 15,000 8,240 1,710 6,330 14,300 57.0 489 512 66.6 188 1,460 362
06/02/08 NS NS NS NS NS NS NS NS NS NS NS NS
10/12/11 FP FP FP FP FP FP FP FP FP FP FP FP
01/31/12 FP FP FP FP FP FP FP FP FP FP FP FP
05/15/12 FP FP FP FP FP FP FP FP FP FP FP FP
01/22/13 FP FP FP FP FP FP FP FP FP FP FP FP
11/18/13 FP FP FP FP FP FP FP FP FP FP FP FP
05/27/14 792 3,720 1,160 5,660 604 <10 550 22.8 J 95.0 356 2,160 605
01/29/15 170 1,930 1,170 6,160 238 <16 496 <16 125 592 3,230 1,140
07/27/15 236 297 448 2,260 367 <4.0 298 14.8 61.7 215 1,590 445
MW-3
MW-4R IsopropylbenzeneNaphthaleneToluene1,2,4-Trimethylbenzene1,2-DichloroethaneIPEBenzene2L Standard (mg/l)
MW-2
MW-1
MW-4
MW-1R
MW-2R
MW-3R
TABLE 4
SUMMARY OF GROUND WATER SAMPLING RESULTS
RED APPLE MARKET # 21 (INCIDENT NO. 9785)n-Propylbenzene1,3,5-TrimethylbenzeneDate : 08/03/15
Analytical Method EthylbenzeneContaminant of Concern

EPA Method 6210D or EPA Method 6200B
Facility ID # : 0-030290
GCL (mg/l)XylenesMTBEPage 1 of 7
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 70 6 0.4 70 70 400 400
5,000 260,000 84,500 85,500 20,000 70,000 6,000 400 25,000 30,000 28,500 25,000IsopropylbenzeneNaphthaleneToluene1,2,4-Trimethylbenzene1,2-DichloroethaneIPEBenzene2L Standard (mg/l)
TABLE 4
SUMMARY OF GROUND WATER SAMPLING RESULTS
RED APPLE MARKET # 21 (INCIDENT NO. 9785)n-Propylbenzene1,3,5-TrimethylbenzeneDate : 08/03/15
Analytical Method EthylbenzeneContaminant of Concern

EPA Method 6210D or EPA Method 6200B
Facility ID # : 0-030290
GCL (mg/l)XylenesMTBE01/18/07 1,040 76.6 116 109.4 836 <5.00 348 NR NR NR NR NR
06/06/07 1,350 90.1 143 119 1,300 9.78 105 31.1 20.6 41.9 29.0 8.31
06/02/08 NS NS NS NS NS NS NS NS NS NS NS NS
03/24/09 NS NS NS NS NS NS NS NS NS NS NS NS
06/25/09 NS NS NS NS NS NS NS NS NS NS NS NS
09/21/09 403 2.25 J 40.9 37.3 195 3.44 J 61.5 4.47 J 18.1 45.9 19.5 16.4
12/30/09 676 7.35 35.7 12.3 255 3.76 J 43.4 4.58 J 11.6 19.6 4.45 J 3.94 J
06/28/10 817 12.6 J 66.7 55.9 347 <10.0 54.1 <11.0 9.82 J 16.8 J 10.9 J <9.00
10/05/10 308 <19.0 41.1 J 23.0 J 193 <20.0 108 <22.0 24.2 J 46.9 J 29.2 J <18.0
10/12/11 FP FP FP FP FP FP FP FP FP FP FP FP
01/31/12 40.6 2.7 61.4 25.6 156 1.6 42.6 5.2 12.6 31.4 55.6 23.3
05/15/12 871 18.2 134 214.8 93.4 1.7 87.5 2.7 21.4 19.8 111 9.2
01/22/13 143 14.6 114 225 184 1.8 J 128 3.6 22.4 76.2 506 101
11/18/13 34.4 0.45 J 22.7 1.8 99.2 1.2 47.3 1.9 5.7 6.1 13.1 3.1
05/27/14 145 7.8 114 39.9 247 1.9 J 60.7 5.7 15.3 21.5 87.7 11.9
01/29/15 65.8 2.4 28.2 1.5 117 1.1 20.1 2.5 4.8 8.2 7.9 0.26 J
07/27/15 61.2 1.2 J 19.2 10.4 198 1.4 26.1 4.2 6.3 9.6 15.4 1.0 J
01/18/07 NS NS NS NS NS NS NS NS NS NS NS NS
06/06/07 NS NS NS NS NS NS NS NS NS NS NS NS
01/18/07 <1.00 <1.00 <1.00 <3.00 <1.00 <1.00 <1.00 NR NR NR NR NR
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 <0.500 <0.500 <0.500 0.550 <0.500
06/02/08 <1.0 <1.0 <1.0 <3.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
12/18/08 14 <0.50 <0.65 <1.1 13 <1.0 2.1 JB <0.50 <0.75 <0.55 <0.50 <0.65
03/24/09 3.0 J <1.6 <3.0 <5.0 3.6 J <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/30/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/28/10 <0.280 <0.380 <0.300 <0.440 <0.500 <0.400 <1.00 <0.440 <0.300 <0.440 <0.300 <0.360
10/05/10 NS NS NS NS NS NS NS NS NS NS NS NS
01/18/07 <1.00 <1.00 <1.00 <3.00 <1.00 <1.00 <1.00 NR NR NR NR NR
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
06/02/08 NS NS NS NS NS NS NS NS NS NS NS NS
12/18/08 2.3 J <0.50 <0.65 <1.1 <0.50 <1.0 1.2 JB <0.50 <0.75 <0.55 <0.50 <0.65
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/30/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 0.543 J <0.180
06/28/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/05/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 2.30 <0.220 <0.150 <0.220 0.168 J <0.180
10/12/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
05/15/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/18/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
01/29/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
07/27/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.16 0.15 J <0.16 <0.12 <0.16 <0.14 <0.14
01/18/07 53.6 1.48 27.4 56.3 3.67 3.97 18.3 NR NR NR NR NR
06/06/07 56.8 0.960 24.2 53.8 0.690 0.520 14.3 1.42 3.14 6.14 30.1 2.87
06/02/08 33.6 0.640 I 21.7 9.07 2.18 0.800 I 20.5 1.68 4.48 4.51 12.3 0.290 I
12/18/08 40 1.6 J 27 18 <0.50 <1.0 22 B <0.50 6.2 9.7 B 25 3.1 J
03/24/09 68 <1.6 37 23 2.0 J <1.6 28 2.3 J 6.8 13 28 2.1 J
06/25/09 53.4 0.929 J 15.9 20.7 1.04 <1.67 19.5 1.54 4.62 4.64 18.4 1.28
09/21/09 50.7 0.952 J 25.7 18.5 1.85 1.10 23.2 2.42 7.29 9.19 18.4 1.46
12/30/09 71.9 0.903 J 28.4 16.8 <0.250 0.758 J 21.9 1.71 6.49 10.7 20.9 2.06
06/28/10 66.1 <0.950 22.5 15.2 <1.25 <1.00 19.0 <1.10 4.25 J 5.94 9.47 1.11 J
10/05/10 72.6 3.54 74.2 110 <0.250 1.35 33.7 2.95 10.6 22.7 79.8 14.3
10/12/11 37.3 0.41 J 8.2 12.2 0.92 0.76 17.3 2.1 4.5 4.6 8.3 1.0
01/31/12 54.7 0.78 25.0 21.6 1.5 0.98 24.1 2.4 7.1 13.9 21.7 2.6
05/15/12 65.9 0.58 J 15.7 15.0 1.3 0.86 J 15.9 2.4 4.5 7.7 11.6 0.89 J
01/22/13 73.7 2.3 13.9 74.7 0.43 J 0.42 J 13.6 1.2 1.2 2.1 31.8 6.8
11/18/13 183 3.9 53.5 153 0.91 1.2 40.4 4.0 12.0 26.1 96.0 11.9
05/27/14 227 3.7 60.4 158 1.5 1.7 44.1 6.6 12.9 27.9 108 12.2
01/29/15 162 1.7 36.1 71.5 1.3 1.3 32.6 3.8 8.3 18.8 89.3 6.0
07/27/15 120 1.4 43.9 57.7 1.7 1.4 43.5 4.5 9.1 18.1 51.1 5.1
MW-5
MW-5R
MW-8
MW-6
MW-9
MWD-7
Page 2 of 7
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 70 6 0.4 70 70 400 400
5,000 260,000 84,500 85,500 20,000 70,000 6,000 400 25,000 30,000 28,500 25,000IsopropylbenzeneNaphthaleneToluene1,2,4-Trimethylbenzene1,2-DichloroethaneIPEBenzene2L Standard (mg/l)
TABLE 4
SUMMARY OF GROUND WATER SAMPLING RESULTS
RED APPLE MARKET # 21 (INCIDENT NO. 9785)n-Propylbenzene1,3,5-TrimethylbenzeneDate : 08/03/15
Analytical Method EthylbenzeneContaminant of Concern

EPA Method 6210D or EPA Method 6200B
Facility ID # : 0-030290
GCL (mg/l)XylenesMTBE01/18/07 1.84 <1.00 <1.00 <3.00 36.6 1.18 <5.00 NR NR NR NR NR
06/06/07 2.05 <0.500 <0.500 <1.00 28.0 0.630 <5.00 2.50 <0.500 <0.500 <0.500 <0.500
06/02/08 45.2 <1.0 <1.0 1.40 I 42.8 2.15 I 1.98 9.21 0.540 I <1.0 0.380 I <1.0
12/18/08 1.7 J <0.50 <0.65 <1.1 35 <1.0 2.6 JB 12 <0.75 <0.55 0.96 J <0.65
03/24/09 1.4 J <1.6 <3.0 <5.0 49 2.5 J <5.0 12 <1.6 <1.6 <1.6 <1.6
06/25/09 6.42 <0.330 <0.670 <1.33 83.8 3.29 J <1.00 20.7 <1.00 <0.330 <0.330 <0.330
09/21/09 2.03 <0.190 <0.150 <0.220 100 4.02 <0.500 23.4 <0.150 <0.220 <0.150 <0.180
12/30/09 1.13 <0.190 <0.150 <0.220 69.4 2.66 1.41 13.6 <0.150 <0.220 <0.150 <0.180
06/28/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/05/10 0.774 J <0.190 <0.150 <0.220 98.8 5.00 12.3 24.0 <0.150 <0.220 0.506 J <0.180
10/12/11 <0.13 <0.13 <0.15 <0.30 61.8 3.6 0.32 J 18.2 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 1.4 <0.15 <0.30 60.3 3.1 0.14 J 14.4 <0.10 <0.11 <0.10 <0.10
05/15/12 NS NS NS NS NS NS NS NS NS NS NS NS
01/22/13 3.6 <0.20 <0.20 0.38 J 81.8 2.5 0.52 J 9.8 <0.20 <0.20 0.33 J <0.20
11/18/13 0.20 J <0.10 <0.10 <0.22 76.1 3.5 0.61 16.5 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 37.3 1.8 <0.10 7.2 <0.10 <0.10 <0.10 <0.10
01/29/15 0.43 J <0.17 <0.15 <0.43 73.9 3.2 0.74 15.9 <0.12 <0.16 <0.14 <0.14
07/27/15 0.40 J <0.17 <0.15 <0.43 119 4.2 <0.31 21.4 <0.12 <0.16 <0.14 <0.14
01/18/07 NS NS NS NS NS NS NS NS NS NS NS NS
06/06/07 NS NS NS NS NS NS NS NS NS NS NS NS
01/18/07 NS NS NS NS NS NS NS NS NS NS NS NS
06/06/07 NS NS NS NS NS NS NS NS NS NS NS NS
01/18/07 <1.00 <1.00 <1.00 <3.00 <1.00 <1.00 <5.00 NS NR NR NR NR
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
06/02/08 NS NS NS NS NS NS NS NS NS NS NS NS
01/18/07 <1.00 <1.00 <1.00 <3.00 <1.00 <1.00 <5.00 NR NR NR NR NR
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
06/02/08 <1.0 <1.0 <1.0 <3.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
12/18/08 <0.55 <0.50 <0.65 <1.1 <0.50 <1.0 0.86 JB <0.50 <0.75 <0.55 <0.50 <0.65
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/30/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/28/10 1.09 <0.190 <0.150 <0.220 99.8 2.95 <0.500 25.6 <0.150 <0.220 <0.150 <0.180
10/05/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 0.853 J <0.220 <0.150 <0.220 <0.150 <0.180
10/12/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/22/13 <0.10 0.37 J 0.26 J 1.5 J <0.10 <0.10 1.4 <0.10 <0.10 0.14 J 1.0 0.36 J
11/18/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
01/29/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
01/18/07 <1.00 <1.00 <1.00 <3.00 <1.00 <1.00 <5.00 NR NR NR NR NR
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
06/02/08 <1.0 <1.0 <1.0 <3.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
12/18/08 NS NS NS NS NS NS NS NS NS NS NS NS
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/30/09 NS NS NS NS NS NS NS NS NS NS NS NS
06/28/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/05/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/12/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/18/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
01/29/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
01/18/07 NS NS NS NS NS NS NS NS NS NS NS NS
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
06/02/08 NS NS NS NS NS NS NS NS NS NS NS NS
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 NS NS NS NS NS NS NS NS NS NS NS NS
12/30/09 NS NS NS NS NS NS NS NS NS NS NS NS
06/28/10 NS NS NS NS NS NS NS NS NS NS NS NS
10/05/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/12/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/18/13 NS NS NS NS NS NS NS NS NS NS NS NS
05/27/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
01/29/15 NS NS NS NS NS NS NS NS NS NS NS NS
MW-12
MW-13
MW-10
MW-11
MW-14
MW-15
MW-16
Page 3 of 7
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 70 6 0.4 70 70 400 400
5,000 260,000 84,500 85,500 20,000 70,000 6,000 400 25,000 30,000 28,500 25,000IsopropylbenzeneNaphthaleneToluene1,2,4-Trimethylbenzene1,2-DichloroethaneIPEBenzene2L Standard (mg/l)
TABLE 4
SUMMARY OF GROUND WATER SAMPLING RESULTS
RED APPLE MARKET # 21 (INCIDENT NO. 9785)n-Propylbenzene1,3,5-TrimethylbenzeneDate : 08/03/15
Analytical Method EthylbenzeneContaminant of Concern

EPA Method 6210D or EPA Method 6200B
Facility ID # : 0-030290
GCL (mg/l)XylenesMTBE01/18/07 NS NS NS NS NS NS NS NS NS NS NS NS
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
06/02/08 NS NS NS NS NS NS NS NS NS NS NS NS
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 NS NS NS NS NS NS NS NS NS NS NS NS
12/30/09 NS NS NS NS NS NS NS NS NS NS NS NS
06/28/10 NS NS NS NS NS NS NS NS NS NS NS NS
10/05/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/12/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/18/13 NS NS NS NS NS NS NS NS NS NS NS NS
05/27/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
01/29/15 NS NS NS NS NS NS NS NS NS NS NS NS
01/18/07 <1.00 <1.00 <1.00 <3.00 <1.00 <1.00 <5.00 NR NR NR NR NR
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
06/02/08 <1.0 <1.0 <1.0 <3.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
12/18/08 <0.55 <0.50 <0.65 <1.1 <0.50 <1.0 0.59 JB <0.50 <0.75 <0.55 <0.50 <0.65
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/30/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/28/10 <0.140 0.244 J <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/05/10 NS NS NS NS NS NS NS NS NS NS NS NS
10/12/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
05/15/12 NS NS NS NS NS NS NS NS NS NS NS NS
11/18/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
01/29/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
01/18/07 <1.00 <1.00 <1.00 <3.00 <1.00 <1.00 <5.00 NR NR NR NR NR
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
06/02/08 <1.0 <1.0 <1.0 <3.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
12/18/08 <0.55 <0.50 <0.65 <1.1 <0.50 <1.0 <0.50 <0.50 <0.75 <0.55 <0.50 <0.65
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/30/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/28/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/05/10 NS NS NS NS NS NS NS NS NS NS NS NS
10/12/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
05/15/12 NS NS NS NS NS NS NS NS NS NS NS NS
11/18/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
01/29/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
01/18/07 <1.00 <1.00 <1.00 <3.00 <1.00 <1.00 <5.00 NR NR NR NR NR
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
06/02/08 <1.0 <1.0 <1.0 <3.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
12/18/08 <0.55 <0.50 <0.65 <1.1 <0.50 <1.0 <0.50 <0.50 <0.75 <0.55 <0.50 <0.65
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/30/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/28/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/05/10 NS NS NS NS NS NS NS NS NS NS NS NS
10/12/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
05/15/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/18/13 <0.10 <0.10 <0.10 <0.22 0.32 J <0.10 <0.15 0.12 J <0.10 <0.10 <0.10 <0.10
05/27/14 NS NS NS NS NS NS NS NS NS NS NS NS
01/29/15 <0.17 <0.17 <0.15 <0.43 0.34 J <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
MW-17
MW-18
MW-20
MW-19
Page 4 of 7
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 70 6 0.4 70 70 400 400
5,000 260,000 84,500 85,500 20,000 70,000 6,000 400 25,000 30,000 28,500 25,000IsopropylbenzeneNaphthaleneToluene1,2,4-Trimethylbenzene1,2-DichloroethaneIPEBenzene2L Standard (mg/l)
TABLE 4
SUMMARY OF GROUND WATER SAMPLING RESULTS
RED APPLE MARKET # 21 (INCIDENT NO. 9785)n-Propylbenzene1,3,5-TrimethylbenzeneDate : 08/03/15
Analytical Method EthylbenzeneContaminant of Concern

EPA Method 6210D or EPA Method 6200B
Facility ID # : 0-030290
GCL (mg/l)XylenesMTBE01/18/07 <1.00 <1.00 <1.00 <3.00 4.28 <1.00 <5.00 NR NR NR NR NR
06/06/07 <0.500 <0.500 <0.500 <1.00 4.50 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
06/02/08 <1.0 <1.0 <1.0 <3.0 5.26 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
12/18/08 <0.55 <0.50 <0.65 <1.1 4.7 J <1.0 <0.50 <0.50 <0.75 <0.55 <0.50 <0.65
03/24/09 <1.0 <1.6 <3.0 <5.0 4.2 J <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 3.10 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 3.02 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/30/09 <0.140 <0.190 <0.150 <0.220 2.33 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/28/10 <0.140 <0.190 <0.150 <0.220 1.21 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/05/10 <0.140 <0.190 <0.150 <0.220 2.34 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/12/11 <0.13 <0.13 <0.15 <0.30 0.97 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 0.77 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
05/15/12 <0.13 <0.13 <0.15 <0.30 1.1 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/22/13 <0.10 <0.10 <0.10 <0.22 0.24 J <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
11/18/13 <0.10 <0.10 <0.10 <0.22 0.52 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 0.21 J <0.10 <0.10 <0.10 <0.10 <0.10 0.11 J <0.10
01/29/15 <0.17 <0.17 <0.15 <0.43 0.22 J <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
07/27/15 <0.17 <0.17 <0.15 <0.43 0.42 J <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
06/02/08 4.11 <1.0 <1.0 <3.0 52.4 1.78 I <1.0 2.61 <1.0 <1.0 <1.0 <1.0
12/18/08 NS NS NS NS NS NS NS NS NS NS NS NS
05/15/12 <0.13 <0.13 <0.15 <0.30 1.3 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/18/13 2.8 <0.10 0.16 J <0.22 3.1 0.12 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 NS NS NS NS NS NS NS NS NS NS NS NS
01/29/15 <0.17 <0.17 <0.15 <0.43 0.75 <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
07/27/15 <0.17 <0.17 <0.15 <0.43 0.50 <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
06/02/08 81.0 15.6 46.7 162 <1.0 <5.0 38.4 13.5 5.67 10.1 121 57.6
12/18/08 NS NS NS NS NS NS NS NS NS NS NS NS
10/12/11 NS NS NS NS NS NS NS NS NS NS NS NS
05/15/12 104 14.2 60.7 19.5 <0.13 <0.11 19.3 12.5 6.3 11.3 49.0 17.9
11/18/13 63.5 4.7 20.0 13.4 <0.10 <0.10 9.8 11.1 3.5 4.1 12.1 4.2
05/27/14 107 4.3 38.7 45.8 <0.10 <0.10 27.4 16.4 8.2 12.0 41.1 6.5
01/29/15 65.2 0.93 6.4 3.9 <0.16 <0.16 10.3 11.3 3.0 3.8 4.4 0.64
07/27/15 175 2.8 22.8 20.7 <0.33 <0.32 39.4 15.9 10.5 17.1 50.8 3.0
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/30/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/28/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/05/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/12/11 <0.13 <0.13 <0.15 <0.30 0.19 J <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 0.18 J <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
05/15/12 <0.13 <0.13 <0.15 <0.30 0.19 J <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/18/13 <0.10 <0.10 <0.10 <0.22 0.30 J <0.10 <0.15 <0.10 <0.10 <0.10 0.14 J <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 0.56 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
01/29/15 <0.17 <0.17 <0.15 <0.43 0.35 J <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
07/27/15 <0.17 <0.17 <0.15 <0.43 0.39 J <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 NS NS NS NS NS NS NS NS NS NS NS NS
12/30/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/28/10 <0.140 <0.190 <0.150 0.355 J <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 0.159 J <0.180
10/05/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 0.236 J <0.180
10/12/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/18/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
01/29/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/30/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/28/10 <0.140 0.329 J <0.150 0.515 J <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/05/10 <0.140 0.516 J 0.199 J 1.03 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 0.465 J <0.180
10/12/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 0.16 J <0.15 <0.30 1.0 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/18/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
01/29/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
MW-27
MW-23
MW-25
MW-28
MW-21
MW-22
Page 5 of 7
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 70 6 0.4 70 70 400 400
5,000 260,000 84,500 85,500 20,000 70,000 6,000 400 25,000 30,000 28,500 25,000IsopropylbenzeneNaphthaleneToluene1,2,4-Trimethylbenzene1,2-DichloroethaneIPEBenzene2L Standard (mg/l)
TABLE 4
SUMMARY OF GROUND WATER SAMPLING RESULTS
RED APPLE MARKET # 21 (INCIDENT NO. 9785)n-Propylbenzene1,3,5-TrimethylbenzeneDate : 08/03/15
Analytical Method EthylbenzeneContaminant of Concern

EPA Method 6210D or EPA Method 6200B
Facility ID # : 0-030290
GCL (mg/l)XylenesMTBE03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 NS NS NS NS NS NS NS NS NS NS NS NS
12/30/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/28/10 0.572 J 6.18 2.38 15.6 <0.250 <0.200 2.46 J <0.220 0.306 J 0.896 J 8.36 2.02
10/05/10 <0.140 1.00 0.464 J 2.84 <0.250 <0.200 0.841 J <0.220 <0.150 0.248 J 1.81 0.506 J
10/12/11 NS NS NS NS NS NS NS NS NS NS NS NS
03/24/09 <1.0 <1.6 <3.0 <5.0 1.8 J <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 1.15 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 1.23 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/30/09 <0.140 <0.190 <0.150 <0.220 1.14 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/28/10 0.203 J 1.95 0.881 J 5.17 1.44 <0.200 0.674 J <0.220 0.150 J 0.418 J 1.67 0.779 J
10/05/10 <0.140 <0.190 <0.150 <0.220 1.28 <0.200 <0.500 <0.220 <0.150 <0.220 0.169 J <0.180
10/12/11 <0.13 <0.13 <0.15 <0.30 1.2 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
05/15/12 <0.13 <0.13 <0.15 <0.30 0.87 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/18/13 <0.10 <0.10 <0.10 <0.22 0.33 J <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 0.25 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
01/29/15 <0.17 <0.17 <0.15 <0.43 0.27 J <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
07/27/15 <0.17 <0.17 <0.15 <0.43 0.20 J <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
WSW-1 06/02/08 NS NS NS NS NS NS NS NS NS NS NS NS
06/02/08 NS NS NS NS NS NS NS NS NS NS NS NS
03/24/09 NS NS NS NS NS NS NS NS NS NS NS NS
12/30/09 NS NS NS NS NS NS NS NS NS NS NS NS
01/18/07 NS NS NS NS NS NS NS NS NS NS NS NS
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
06/02/08 <1.0 <1.0 <1.0 <3.0 <1.0 <5.0 0.930 I <1.0 <1.0 <1.0 0.330 I <1.0
03/24/09 NS NS NS NS NS NS NS NS NS NS NS NS
12/30/09 NS NS NS NS NS NS NS NS NS NS NS NS
01/18/07 NS NS NS NS NS NS NS NS NS NS NS NS
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
06/02/08 NS NS NS NS NS NS NS NS NS NS NS NS
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/30/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/28/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/05/10 NS NS NS NS NS NS NS NS NS NS NS NS
10/12/11 <0.13 <0.13 <0.15 0.53 J <0.13 <0.11 0.23 J <0.16 <0.10 <0.11 0.33 J <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 0.11 J <0.10
05/15/12 NS NS NS NS NS NS NS NS NS NS NS NS
01/22/13 NS NS NS NS NS NS NS NS NS NS NS NS
11/18/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 0.30 J 0.19 J
01/29/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
01/18/07 NS NS NS NS NS NS NS NS NS NS NS NS
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 2.14 <0.500 <0.500 0.520 <0.500
06/02/08 <1.0 <1.0 <1.0 <3.0 <1.0 <5.0 <1.0 1.75 <1.0 <1.0 <1.0 <1.0
12/18/08 <0.55 <0.50 <0.65 <1.1 <0.50 <1.0 <0.50 29 <0.75 <0.55 <0.50 <0.65
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 26 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 34.3 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 34.4 <0.150 <0.220 <0.150 <0.180
12/30/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 16.1 <0.150 <0.220 <0.150 <0.180
06/28/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 45.0 <0.150 <0.220 <0.150 <0.180
10/05/10 NS NS NS NS NS NS NS NS NS NS NS NS
10/12/11 NS NS NS NS NS NS NS NS NS NS NS NS
01/31/12 NS NS NS NS NS NS NS NS NS NS NS NS
05/15/12 NS NS NS NS NS NS NS NS NS NS NS NS
01/22/13 NS NS NS NS NS NS NS NS NS NS NS NS
05/27/14 NS NS NS NS NS NS NS NS NS NS NS NS
WSW-2
WSW-3
WSW-5
MW-30
WSW-4
MW-29
Page 6 of 7
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 70 6 0.4 70 70 400 400
5,000 260,000 84,500 85,500 20,000 70,000 6,000 400 25,000 30,000 28,500 25,000IsopropylbenzeneNaphthaleneToluene1,2,4-Trimethylbenzene1,2-DichloroethaneIPEBenzene2L Standard (mg/l)
TABLE 4
SUMMARY OF GROUND WATER SAMPLING RESULTS
RED APPLE MARKET # 21 (INCIDENT NO. 9785)n-Propylbenzene1,3,5-TrimethylbenzeneDate : 08/03/15
Analytical Method EthylbenzeneContaminant of Concern

EPA Method 6210D or EPA Method 6200B
Facility ID # : 0-030290
GCL (mg/l)XylenesMTBE06/02/08 NS NS NS NS NS NS NS NS NS NS NS NS
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
06/28/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/05/10 NS NS NS NS NS NS NS NS NS NS NS NS
10/12/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10
05/15/12 NS NS NS NS NS NS NS NS NS NS NS NS
01/22/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
11/18/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
01/29/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
Notes:
• Results reported in µg/l (micrograms per liter).
• NE: Standard not established.
• Concentrations in bold face type exceeded the 2L standards.
• NR: Not requested.
• < : Less than the method detection limit specified in the laboratory report
• I or J: Estimated value.
• V or B: Present in laboratory blank.
• NS: Not sampled.
• E: Estimated value; above laboratory calibration curve.
• A concentration of bromodichloromethane (0.95 µg/l in WSW-6) that exceeded the MACs were reported in the ground water sample collected on
January 29, 2015.
• For other compounds reported which did not exceed the 2L Standards, refer to the laboratory reports.
• GCL : Gross contamination level.
• 2L Standard: as specified in T15A NCAC 2L.0202.
WSW-6
Page 7 of 7

APPENDIX

APPENDIX A
Laboratory Report – Ground Water Samples
08/03/15
Technical Report for
GRI (Geological Resources Inc.)
Ram 21, 1121 NC561 W, Saint John, NC
9785/2486
Accutest Job Number: FA26389
Sampling Date: 07/27/15
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
[e-mail]; [e-mail];
[e-mail]; [e-mail]
ATTN: William Regenthall
Total number of pages in report:
Certifications: FL (E83510), LA (03051), KS (E-10327), IA (366), IL (200063), NC (573), NJ (FL002), SC (96038001)
DoD ELAP (L-A-B L2229), CA (2937), TX (T104704404), PA (68-03573), VA (460177),
AK, AR, GA, KY, MA, NV, OK, UT, WA
This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone] • http://www.accutest.com
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Norm Farmer
Technical Director
Southeast
08/03/15
e-Hardcopy 2.0
Automated Report
49
Accutest Laboratories is the sole authority for authorizing edits or modifications to this
document. Unauthorized modification of this report is strictly prohibited.
1 of 49
FA26389
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................8
3.1: FA26389-1: MW-1R .....................................................................................................9
3.2: FA26389-2: MW-2R .....................................................................................................11
3.3: FA26389-3: MW-3R .....................................................................................................13
3.4: FA26389-4: MW-4R .....................................................................................................15
3.5: FA26389-5: MW-5R .....................................................................................................17
3.6: FA26389-6: MW-8 ........................................................................................................19
3.7: FA26389-7: MW-9 ........................................................................................................21
3.8: FA26389-8: MW-10 ......................................................................................................23
3.9: FA26389-9: MW-21 ......................................................................................................25
3.10: FA26389-10: MW-22 ..................................................................................................27
3.11: FA26389-11: MW-23 ..................................................................................................29
3.12: FA26389-12: MW-25 ..................................................................................................31
3.13: FA26389-13: MW-30 ..................................................................................................33
Section 4: Misc. Forms ............................................................................................................35
4.1: Chain of Custody ...........................................................................................................36
Section 5: GC/MS Volatiles - QC Data Summaries ..............................................................40
5.1: Method Blank Summary ................................................................................................41
5.2: Blank Spike Summary ...................................................................................................44
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................47 123452 of 49
FA26389
Accutest Laboratories
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA26389
Ram 21, 1121 NC561 W, Saint John, NC
Project No: 9785/2486
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA26389-1 07/27/15 12:01 HM 07/28/15 AQ Ground Water MW-1R
FA26389-2 07/27/15 12:10 HM 07/28/15 AQ Ground Water MW-2R
FA26389-3 07/27/15 12:38 HM 07/28/15 AQ Ground Water MW-3R
FA26389-4 07/27/15 12:18 HM 07/28/15 AQ Ground Water MW-4R
FA26389-5 07/27/15 12:29 HM 07/28/15 AQ Ground Water MW-5R
FA26389-6 07/27/15 13:00 HM 07/28/15 AQ Ground Water MW-8
FA26389-7 07/27/15 12:47 HM 07/28/15 AQ Ground Water MW-9
FA26389-8 07/27/15 13:29 HM 07/28/15 AQ Ground Water MW-10
FA26389-9 07/27/15 14:02 HM 07/28/15 AQ Ground Water MW-21
FA26389-10 07/27/15 13:19 HM 07/28/15 AQ Ground Water MW-22
FA26389-11 07/27/15 13:09 HM 07/28/15 AQ Ground Water MW-23
FA26389-12 07/27/15 13:50 HM 07/28/15 AQ Ground Water MW-25
FA26389-13 07/27/15 11:52 HM 07/28/15 AQ Ground Water MW-30
3 of 49
FA26389 1
Summary of Hits Page 1 of 4
Job Number:FA26389
Account:GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Collected:07/27/15
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA26389-1 MW-1R
Methyl Chloride 0.64 0.50 0.16 ug/l SM 6200B
Methyl Tert Butyl Ether 0.91 0.50 0.16 ug/l SM 6200B
FA26389-2 MW-2R
Benzene 6350 100 34 ug/l SM 6200B
n-Butylbenzene 36.1 J 50 14 ug/l SM 6200B
sec-Butylbenzene 21.8 J 50 14 ug/l SM 6200B
1,2-Dichloroethane 123 50 16 ug/l SM 6200B
Di-Isopropyl Ether 43.7 J 50 16 ug/l SM 6200B
Ethylbenzene 1730 50 15 ug/l SM 6200B
Isopropylbenzene 114 50 12 ug/l SM 6200B
p-Isopropyltoluene 14.4 J 50 12 ug/l SM 6200B
Methyl Tert Butyl Ether 1090 50 16 ug/l SM 6200B
Naphthalene 732 50 12 ug/l SM 6200B
n-Propylbenzene 319 50 16 ug/l SM 6200B
Styrene 12.4 J 50 12 ug/l SM 6200B
Toluene 3210 50 17 ug/l SM 6200B
1,2,4-Trimethylbenzene 2250 50 14 ug/l SM 6200B
1,3,5-Trimethylbenzene 641 50 14 ug/l SM 6200B
m,p-Xylene 5160 100 30 ug/l SM 6200B
o-Xylene 2390 50 13 ug/l SM 6200B
Xylene (total)7550 150 43 ug/l SM 6200B
FA26389-3 MW-3R
Benzene 1.9 0.50 0.17 ug/l SM 6200B
Ethylbenzene 1.1 0.50 0.15 ug/l SM 6200B
Isopropylbenzene 0.32 J 0.50 0.12 ug/l SM 6200B
Methyl Chloride 0.84 0.50 0.16 ug/l SM 6200B
Methyl Tert Butyl Ether 5.5 0.50 0.16 ug/l SM 6200B
Naphthalene 0.28 J 0.50 0.12 ug/l SM 6200B
n-Propylbenzene 0.32 J 0.50 0.16 ug/l SM 6200B
Toluene 0.30 J 0.50 0.17 ug/l SM 6200B
1,2,4-Trimethylbenzene 0.50 0.50 0.14 ug/l SM 6200B
1,3,5-Trimethylbenzene 0.18 J 0.50 0.14 ug/l SM 6200B
m,p-Xylene 0.70 J 1.0 0.30 ug/l SM 6200B
o-Xylene 0.31 J 0.50 0.13 ug/l SM 6200B
Xylene (total)1.0 J 1.5 0.43 ug/l SM 6200B
FA26389-4 MW-4R
Benzene 236 13 4.3 ug/l SM 6200B
4 of 49
FA26389 2
Summary of Hits Page 2 of 4
Job Number:FA26389
Account:GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Collected:07/27/15
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
n-Butylbenzene 49.8 13 3.6 ug/l SM 6200B
sec-Butylbenzene 22.2 13 3.5 ug/l SM 6200B
1,2-Dichloroethane 14.8 13 4.1 ug/l SM 6200B
Ethylbenzene 448 13 3.8 ug/l SM 6200B
Isopropylbenzene 61.7 13 3.0 ug/l SM 6200B
p-Isopropyltoluene 13.3 13 3.1 ug/l SM 6200B
Methyl Tert Butyl Ether 367 13 4.1 ug/l SM 6200B
Naphthalene 298 13 3.1 ug/l SM 6200B
n-Propylbenzene 215 13 3.9 ug/l SM 6200B
Toluene 297 13 4.2 ug/l SM 6200B
1,2,4-Trimethylbenzene 1590 50 14 ug/l SM 6200B
1,3,5-Trimethylbenzene 445 13 3.4 ug/l SM 6200B
m,p-Xylene 1710 25 7.4 ug/l SM 6200B
o-Xylene 547 13 3.3 ug/l SM 6200B
Xylene (total)2260 38 11 ug/l SM 6200B
FA26389-5 MW-5R
Benzene 61.2 1.3 0.43 ug/l SM 6200B
n-Butylbenzene 1.1 J 1.3 0.36 ug/l SM 6200B
sec-Butylbenzene 2.5 1.3 0.35 ug/l SM 6200B
1,2-Dichloroethane 4.2 1.3 0.41 ug/l SM 6200B
Di-Isopropyl Ether 1.4 1.3 0.40 ug/l SM 6200B
Ethylbenzene 19.2 1.3 0.38 ug/l SM 6200B
Isopropylbenzene 6.3 1.3 0.30 ug/l SM 6200B
p-Isopropyltoluene 1.7 1.3 0.31 ug/l SM 6200B
Methyl Tert Butyl Ether 198 2.5 0.82 ug/l SM 6200B
Naphthalene 26.1 1.3 0.31 ug/l SM 6200B
n-Propylbenzene 9.6 1.3 0.39 ug/l SM 6200B
Toluene 1.2 J 1.3 0.42 ug/l SM 6200B
1,2,4-Trimethylbenzene 15.4 1.3 0.34 ug/l SM 6200B
1,3,5-Trimethylbenzene 1.0 J 1.3 0.34 ug/l SM 6200B
m,p-Xylene 8.2 2.5 0.74 ug/l SM 6200B
o-Xylene 2.2 1.3 0.33 ug/l SM 6200B
Xylene (total)10.4 3.8 1.1 ug/l SM 6200B
FA26389-6 MW-8
Methyl Chloride 1.0 0.50 0.16 ug/l SM 6200B
Naphthalene 0.15 J 0.50 0.12 ug/l SM 6200B
FA26389-7 MW-9
Benzene 120 2.5 0.86 ug/l SM 6200B
n-Butylbenzene 3.1 0.50 0.14 ug/l SM 6200B
5 of 49
FA26389 2
Summary of Hits Page 3 of 4
Job Number:FA26389
Account:GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Collected:07/27/15
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
sec-Butylbenzene 2.8 0.50 0.14 ug/l SM 6200B
1,2-Dichloroethane 4.5 0.50 0.16 ug/l SM 6200B
Di-Isopropyl Ether 1.4 0.50 0.16 ug/l SM 6200B
Ethylbenzene 43.9 0.50 0.15 ug/l SM 6200B
Isopropylbenzene 9.1 0.50 0.12 ug/l SM 6200B
p-Isopropyltoluene 0.80 0.50 0.12 ug/l SM 6200B
Methyl Tert Butyl Ether 1.7 0.50 0.16 ug/l SM 6200B
Naphthalene 43.5 0.50 0.12 ug/l SM 6200B
n-Propylbenzene 18.1 0.50 0.16 ug/l SM 6200B
Toluene 1.4 0.50 0.17 ug/l SM 6200B
1,2,4-Trimethylbenzene 51.1 2.5 0.68 ug/l SM 6200B
1,3,5-Trimethylbenzene 5.1 0.50 0.14 ug/l SM 6200B
m,p-Xylene 41.5 1.0 0.30 ug/l SM 6200B
o-Xylene 16.3 0.50 0.13 ug/l SM 6200B
Xylene (total)57.7 1.5 0.43 ug/l SM 6200B
FA26389-8 MW-10
Benzene 0.40 J 0.50 0.17 ug/l SM 6200B
1,2-Dichloroethane 21.4 0.50 0.16 ug/l SM 6200B
Di-Isopropyl Ether 4.2 0.50 0.16 ug/l SM 6200B
Methyl Chloride 0.47 J 0.50 0.16 ug/l SM 6200B
Methyl Tert Butyl Ether 119 1.3 0.41 ug/l SM 6200B
FA26389-9 MW-21
Methyl Chloride 0.49 J 0.50 0.16 ug/l SM 6200B
Methyl Tert Butyl Ether 0.42 J 0.50 0.16 ug/l SM 6200B
FA26389-10 MW-22
Methyl Chloride 0.59 0.50 0.16 ug/l SM 6200B
Methyl Tert Butyl Ether 0.50 0.50 0.16 ug/l SM 6200B
FA26389-11 MW-23
Benzene 175 2.5 0.86 ug/l SM 6200B
n-Butylbenzene 1.3 1.0 0.29 ug/l SM 6200B
sec-Butylbenzene 1.6 1.0 0.28 ug/l SM 6200B
Chloroethane 2.2 1.0 0.41 ug/l SM 6200B
1,2-Dichloroethane 15.9 1.0 0.33 ug/l SM 6200B
Ethylbenzene 22.8 1.0 0.30 ug/l SM 6200B
Isopropylbenzene 10.5 1.0 0.24 ug/l SM 6200B
p-Isopropyltoluene 2.1 1.0 0.24 ug/l SM 6200B
Methyl Chloride 1.3 1.0 0.32 ug/l SM 6200B
6 of 49
FA26389 2
Summary of Hits Page 4 of 4
Job Number:FA26389
Account:GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Collected:07/27/15
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
Naphthalene 39.4 1.0 0.24 ug/l SM 6200B
n-Propylbenzene 17.1 1.0 0.31 ug/l SM 6200B
Toluene 2.8 1.0 0.33 ug/l SM 6200B
1,2,4-Trimethylbenzene 50.8 1.0 0.27 ug/l SM 6200B
1,3,5-Trimethylbenzene 3.0 1.0 0.27 ug/l SM 6200B
m,p-Xylene 6.2 2.0 0.59 ug/l SM 6200B
o-Xylene 14.6 1.0 0.27 ug/l SM 6200B
Xylene (total)20.7 3.0 0.86 ug/l SM 6200B
FA26389-12 MW-25
Methyl Chloride 0.52 0.50 0.16 ug/l SM 6200B
Methyl Tert Butyl Ether 0.39 J 0.50 0.16 ug/l SM 6200B
FA26389-13 MW-30
Methyl Chloride 0.46 J 0.50 0.16 ug/l SM 6200B
Methyl Tert Butyl Ether 0.20 J 0.50 0.16 ug/l SM 6200B
7 of 49
FA26389 2
Accutest Laboratories
Sample Results
Report of Analysis
Southeast
Section 3
8 of 49
FA26389 3
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-1R
Lab Sample ID:FA26389-1 Date Sampled:07/27/15
Matrix:AQ - Ground Water Date Received:07/28/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E040052.D 1 07/29/15 TD n/a n/a VE1331
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
9 of 49
FA26389 33.1
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-1R
Lab Sample ID:FA26389-1 Date Sampled:07/27/15
Matrix:AQ - Ground Water Date Received:07/28/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride 0.64 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.91 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 104%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 49
FA26389 33.1
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-2R
Lab Sample ID:FA26389-2 Date Sampled:07/27/15
Matrix:AQ - Ground Water Date Received:07/28/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E040053.D 100 07/29/15 TD n/a n/a VE1331
Run #2 E040066.D 200 07/29/15 TD n/a n/a VE1331
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 6350 a 100 34 ug/l
108-86-1 Bromobenzene ND 50 16 ug/l
74-97-5 Bromochloromethane ND 50 16 ug/l
75-27-4 Bromodichloromethane ND 50 15 ug/l
75-25-2 Bromoform ND 50 11 ug/l
104-51-8 n-Butylbenzene 36.1 50 14 ug/l J
135-98-8 sec-Butylbenzene 21.8 50 14 ug/l J
98-06-6 tert-Butylbenzene ND 50 15 ug/l
56-23-5 Carbon Tetrachloride ND 50 15 ug/l
108-90-7 Chlorobenzene ND 50 16 ug/l
75-00-3 Chloroethane ND 50 21 ug/l
67-66-3 Chloroform ND 50 17 ug/l
95-49-8 o-Chlorotoluene ND 50 15 ug/l
106-43-4 p-Chlorotoluene ND 50 14 ug/l
124-48-1 Dibromochloromethane ND 50 12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 50 20 ug/l
106-93-4 1,2-Dibromoethane ND 50 14 ug/l
75-71-8 Dichlorodifluoromethane ND 50 13 ug/l
95-50-1 1,2-Dichlorobenzene ND 50 13 ug/l
541-73-1 1,3-Dichlorobenzene ND 50 14 ug/l
106-46-7 1,4-Dichlorobenzene ND 50 15 ug/l
75-34-3 1,1-Dichloroethane ND 50 18 ug/l
107-06-2 1,2-Dichloroethane 123 50 16 ug/l
75-35-4 1,1-Dichloroethylene ND 50 17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 50 18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 50 17 ug/l
78-87-5 1,2-Dichloropropane ND 50 17 ug/l
142-28-9 1,3-Dichloropropane ND 50 15 ug/l
594-20-7 2,2-Dichloropropane ND 50 12 ug/l
563-58-6 1,1-Dichloropropene ND 50 16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 50 13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 50 13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 49
FA26389 33.2
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-2R
Lab Sample ID:FA26389-2 Date Sampled:07/27/15
Matrix:AQ - Ground Water Date Received:07/28/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 43.7 50 16 ug/l J
100-41-4 Ethylbenzene 1730 50 15 ug/l
87-68-3 Hexachlorobutadiene ND 50 12 ug/l
98-82-8 Isopropylbenzene 114 50 12 ug/l
99-87-6 p-Isopropyltoluene 14.4 50 12 ug/l J
74-83-9 Methyl Bromide ND 50 18 ug/l
74-87-3 Methyl Chloride ND 50 16 ug/l
74-95-3 Methylene Bromide ND 50 17 ug/l
75-09-2 Methylene Chloride ND 200 100 ug/l
1634-04-4 Methyl Tert Butyl Ether 1090 50 16 ug/l
91-20-3 Naphthalene 732 50 12 ug/l
103-65-1 n-Propylbenzene 319 50 16 ug/l
100-42-5 Styrene 12.4 50 12 ug/l J
630-20-6 1,1,1,2-Tetrachloroethane ND 50 13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 50 14 ug/l
127-18-4 Tetrachloroethylene ND 50 15 ug/l
108-88-3 Toluene 3210 50 17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 50 14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 50 13 ug/l
71-55-6 1,1,1-Trichloroethane ND 50 16 ug/l
79-00-5 1,1,2-Trichloroethane ND 50 14 ug/l
79-01-6 Trichloroethylene ND 50 15 ug/l
75-69-4 Trichlorofluoromethane ND 50 16 ug/l
96-18-4 1,2,3-Trichloropropane ND 50 13 ug/l
95-63-6 1,2,4-Trimethylbenzene 2250 50 14 ug/l
108-67-8 1,3,5-Trimethylbenzene 641 50 14 ug/l
75-01-4 Vinyl Chloride ND 50 13 ug/l
m,p-Xylene 5160 100 30 ug/l
95-47-6 o-Xylene 2390 50 13 ug/l
1330-20-7 Xylene (total)7550 150 43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%101%70-130%
17060-07-0 1,2-Dichloroethane-D4 105%105%70-130%
2037-26-5 Toluene-D8 98%98%70-130%
460-00-4 4-Bromofluorobenzene 100%100%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 49
FA26389 33.2
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-3R
Lab Sample ID:FA26389-3 Date Sampled:07/27/15
Matrix:AQ - Ground Water Date Received:07/28/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E040055.D 1 07/29/15 TD n/a n/a VE1331
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 1.9 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
13 of 49
FA26389 33.3
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-3R
Lab Sample ID:FA26389-3 Date Sampled:07/27/15
Matrix:AQ - Ground Water Date Received:07/28/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene 1.1 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene 0.32 0.50 0.12 ug/l J
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride 0.84 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 5.5 0.50 0.16 ug/l
91-20-3 Naphthalene 0.28 0.50 0.12 ug/l J
103-65-1 n-Propylbenzene 0.32 0.50 0.16 ug/l J
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene 0.30 0.50 0.17 ug/l J
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 0.50 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene 0.18 0.50 0.14 ug/l J
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 0.70 1.0 0.30 ug/l J
95-47-6 o-Xylene 0.31 0.50 0.13 ug/l J
1330-20-7 Xylene (total)1.0 1.5 0.43 ug/l J
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 104%70-130%
17060-07-0 1,2-Dichloroethane-D4 108%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
14 of 49
FA26389 33.3
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-4R
Lab Sample ID:FA26389-4 Date Sampled:07/27/15
Matrix:AQ - Ground Water Date Received:07/28/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E040067.D 25 07/29/15 TD n/a n/a VE1331
Run #2 E040056.D 100 07/29/15 TD n/a n/a VE1331
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 236 13 4.3 ug/l
108-86-1 Bromobenzene ND 13 4.0 ug/l
74-97-5 Bromochloromethane ND 13 4.0 ug/l
75-27-4 Bromodichloromethane ND 13 3.7 ug/l
75-25-2 Bromoform ND 13 2.7 ug/l
104-51-8 n-Butylbenzene 49.8 13 3.6 ug/l
135-98-8 sec-Butylbenzene 22.2 13 3.5 ug/l
98-06-6 tert-Butylbenzene ND 13 3.6 ug/l
56-23-5 Carbon Tetrachloride ND 13 3.8 ug/l
108-90-7 Chlorobenzene ND 13 4.0 ug/l
75-00-3 Chloroethane ND 13 5.2 ug/l
67-66-3 Chloroform ND 13 4.3 ug/l
95-49-8 o-Chlorotoluene ND 13 3.8 ug/l
106-43-4 p-Chlorotoluene ND 13 3.4 ug/l
124-48-1 Dibromochloromethane ND 13 3.1 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 13 4.9 ug/l
106-93-4 1,2-Dibromoethane ND 13 3.5 ug/l
75-71-8 Dichlorodifluoromethane ND 13 3.2 ug/l
95-50-1 1,2-Dichlorobenzene ND 13 3.2 ug/l
541-73-1 1,3-Dichlorobenzene ND 13 3.5 ug/l
106-46-7 1,4-Dichlorobenzene ND 13 3.8 ug/l
75-34-3 1,1-Dichloroethane ND 13 4.5 ug/l
107-06-2 1,2-Dichloroethane 14.8 13 4.1 ug/l
75-35-4 1,1-Dichloroethylene ND 13 4.3 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 13 4.5 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 13 4.2 ug/l
78-87-5 1,2-Dichloropropane ND 13 4.3 ug/l
142-28-9 1,3-Dichloropropane ND 13 3.7 ug/l
594-20-7 2,2-Dichloropropane ND 13 3.0 ug/l
563-58-6 1,1-Dichloropropene ND 13 4.0 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 13 3.3 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 13 3.2 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
15 of 49
FA26389 33.4
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-4R
Lab Sample ID:FA26389-4 Date Sampled:07/27/15
Matrix:AQ - Ground Water Date Received:07/28/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 13 4.0 ug/l
100-41-4 Ethylbenzene 448 13 3.8 ug/l
87-68-3 Hexachlorobutadiene ND 13 3.1 ug/l
98-82-8 Isopropylbenzene 61.7 13 3.0 ug/l
99-87-6 p-Isopropyltoluene 13.3 13 3.1 ug/l
74-83-9 Methyl Bromide ND 13 4.6 ug/l
74-87-3 Methyl Chloride ND 13 4.0 ug/l
74-95-3 Methylene Bromide ND 13 4.3 ug/l
75-09-2 Methylene Chloride ND 50 25 ug/l
1634-04-4 Methyl Tert Butyl Ether 367 13 4.1 ug/l
91-20-3 Naphthalene 298 13 3.1 ug/l
103-65-1 n-Propylbenzene 215 13 3.9 ug/l
100-42-5 Styrene ND 13 3.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 13 3.1 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 13 3.6 ug/l
127-18-4 Tetrachloroethylene ND 13 3.7 ug/l
108-88-3 Toluene 297 13 4.2 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 13 3.4 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 13 3.3 ug/l
71-55-6 1,1,1-Trichloroethane ND 13 4.0 ug/l
79-00-5 1,1,2-Trichloroethane ND 13 3.5 ug/l
79-01-6 Trichloroethylene ND 13 3.7 ug/l
75-69-4 Trichlorofluoromethane ND 13 4.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 13 3.2 ug/l
95-63-6 1,2,4-Trimethylbenzene 1590 a 50 14 ug/l
108-67-8 1,3,5-Trimethylbenzene 445 13 3.4 ug/l
75-01-4 Vinyl Chloride ND 13 3.3 ug/l
m,p-Xylene 1710 25 7.4 ug/l
95-47-6 o-Xylene 547 13 3.3 ug/l
1330-20-7 Xylene (total)2260 38 11 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%103%70-130%
17060-07-0 1,2-Dichloroethane-D4 109%104%70-130%
2037-26-5 Toluene-D8 98%98%70-130%
460-00-4 4-Bromofluorobenzene 100%98%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
16 of 49
FA26389 33.4
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-5R
Lab Sample ID:FA26389-5 Date Sampled:07/27/15
Matrix:AQ - Ground Water Date Received:07/28/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E040057.D 2.5 07/29/15 TD n/a n/a VE1331
Run #2 E040068.D 5 07/29/15 TD n/a n/a VE1331
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 61.2 1.3 0.43 ug/l
108-86-1 Bromobenzene ND 1.3 0.40 ug/l
74-97-5 Bromochloromethane ND 1.3 0.40 ug/l
75-27-4 Bromodichloromethane ND 1.3 0.37 ug/l
75-25-2 Bromoform ND 1.3 0.27 ug/l
104-51-8 n-Butylbenzene 1.1 1.3 0.36 ug/l J
135-98-8 sec-Butylbenzene 2.5 1.3 0.35 ug/l
98-06-6 tert-Butylbenzene ND 1.3 0.36 ug/l
56-23-5 Carbon Tetrachloride ND 1.3 0.38 ug/l
108-90-7 Chlorobenzene ND 1.3 0.40 ug/l
75-00-3 Chloroethane ND 1.3 0.52 ug/l
67-66-3 Chloroform ND 1.3 0.43 ug/l
95-49-8 o-Chlorotoluene ND 1.3 0.38 ug/l
106-43-4 p-Chlorotoluene ND 1.3 0.34 ug/l
124-48-1 Dibromochloromethane ND 1.3 0.31 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 1.3 0.49 ug/l
106-93-4 1,2-Dibromoethane ND 1.3 0.35 ug/l
75-71-8 Dichlorodifluoromethane ND 1.3 0.32 ug/l
95-50-1 1,2-Dichlorobenzene ND 1.3 0.32 ug/l
541-73-1 1,3-Dichlorobenzene ND 1.3 0.35 ug/l
106-46-7 1,4-Dichlorobenzene ND 1.3 0.38 ug/l
75-34-3 1,1-Dichloroethane ND 1.3 0.45 ug/l
107-06-2 1,2-Dichloroethane 4.2 1.3 0.41 ug/l
75-35-4 1,1-Dichloroethylene ND 1.3 0.43 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 1.3 0.45 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 1.3 0.42 ug/l
78-87-5 1,2-Dichloropropane ND 1.3 0.43 ug/l
142-28-9 1,3-Dichloropropane ND 1.3 0.37 ug/l
594-20-7 2,2-Dichloropropane ND 1.3 0.30 ug/l
563-58-6 1,1-Dichloropropene ND 1.3 0.40 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 1.3 0.33 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 1.3 0.32 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
17 of 49
FA26389 33.5
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-5R
Lab Sample ID:FA26389-5 Date Sampled:07/27/15
Matrix:AQ - Ground Water Date Received:07/28/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 1.4 1.3 0.40 ug/l
100-41-4 Ethylbenzene 19.2 1.3 0.38 ug/l
87-68-3 Hexachlorobutadiene ND 1.3 0.31 ug/l
98-82-8 Isopropylbenzene 6.3 1.3 0.30 ug/l
99-87-6 p-Isopropyltoluene 1.7 1.3 0.31 ug/l
74-83-9 Methyl Bromide ND 1.3 0.46 ug/l
74-87-3 Methyl Chloride ND 1.3 0.40 ug/l
74-95-3 Methylene Bromide ND 1.3 0.43 ug/l
75-09-2 Methylene Chloride ND 5.0 2.5 ug/l
1634-04-4 Methyl Tert Butyl Ether 198 a 2.5 0.82 ug/l
91-20-3 Naphthalene 26.1 1.3 0.31 ug/l
103-65-1 n-Propylbenzene 9.6 1.3 0.39 ug/l
100-42-5 Styrene ND 1.3 0.30 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 1.3 0.31 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 1.3 0.36 ug/l
127-18-4 Tetrachloroethylene ND 1.3 0.37 ug/l
108-88-3 Toluene 1.2 1.3 0.42 ug/l J
87-61-6 1,2,3-Trichlorobenzene ND 1.3 0.34 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 1.3 0.33 ug/l
71-55-6 1,1,1-Trichloroethane ND 1.3 0.40 ug/l
79-00-5 1,1,2-Trichloroethane ND 1.3 0.35 ug/l
79-01-6 Trichloroethylene ND 1.3 0.37 ug/l
75-69-4 Trichlorofluoromethane ND 1.3 0.40 ug/l
96-18-4 1,2,3-Trichloropropane ND 1.3 0.32 ug/l
95-63-6 1,2,4-Trimethylbenzene 15.4 1.3 0.34 ug/l
108-67-8 1,3,5-Trimethylbenzene 1.0 1.3 0.34 ug/l J
75-01-4 Vinyl Chloride ND 1.3 0.33 ug/l
m,p-Xylene 8.2 2.5 0.74 ug/l
95-47-6 o-Xylene 2.2 1.3 0.33 ug/l
1330-20-7 Xylene (total)10.4 3.8 1.1 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 109%110%70-130%
17060-07-0 1,2-Dichloroethane-D4 113%113%70-130%
2037-26-5 Toluene-D8 96%95%70-130%
460-00-4 4-Bromofluorobenzene 97%98%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
18 of 49
FA26389 33.5
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-8
Lab Sample ID:FA26389-6 Date Sampled:07/27/15
Matrix:AQ - Ground Water Date Received:07/28/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E040058.D 1 07/29/15 TD n/a n/a VE1331
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
19 of 49
FA26389 33.6
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-8
Lab Sample ID:FA26389-6 Date Sampled:07/27/15
Matrix:AQ - Ground Water Date Received:07/28/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride 1.0 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene 0.15 0.50 0.12 ug/l J
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 105%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
20 of 49
FA26389 33.6
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-9
Lab Sample ID:FA26389-7 Date Sampled:07/27/15
Matrix:AQ - Ground Water Date Received:07/28/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E040059.D 1 07/29/15 TD n/a n/a VE1331
Run #2 E040069.D 5 07/29/15 TD n/a n/a VE1331
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 120 a 2.5 0.86 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene 3.1 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene 2.8 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane 4.5 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
21 of 49
FA26389 33.7
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-9
Lab Sample ID:FA26389-7 Date Sampled:07/27/15
Matrix:AQ - Ground Water Date Received:07/28/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 1.4 0.50 0.16 ug/l
100-41-4 Ethylbenzene 43.9 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene 9.1 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene 0.80 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 1.7 0.50 0.16 ug/l
91-20-3 Naphthalene 43.5 0.50 0.12 ug/l
103-65-1 n-Propylbenzene 18.1 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene 1.4 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 51.1 a 2.5 0.68 ug/l
108-67-8 1,3,5-Trimethylbenzene 5.1 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 41.5 1.0 0.30 ug/l
95-47-6 o-Xylene 16.3 0.50 0.13 ug/l
1330-20-7 Xylene (total)57.7 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 105%104%70-130%
17060-07-0 1,2-Dichloroethane-D4 107%108%70-130%
2037-26-5 Toluene-D8 97%97%70-130%
460-00-4 4-Bromofluorobenzene 100%99%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
22 of 49
FA26389 33.7
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-10
Lab Sample ID:FA26389-8 Date Sampled:07/27/15
Matrix:AQ - Ground Water Date Received:07/28/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E040060.D 1 07/29/15 TD n/a n/a VE1331
Run #2 E040091.D 2.5 07/30/15 TD n/a n/a VE1332
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 0.40 0.50 0.17 ug/l J
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane 21.4 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
23 of 49
FA26389 33.8
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-10
Lab Sample ID:FA26389-8 Date Sampled:07/27/15
Matrix:AQ - Ground Water Date Received:07/28/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 4.2 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride 0.47 0.50 0.16 ug/l J
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 119 a 1.3 0.41 ug/l
91-20-3 Naphthalene ND a 1.3 0.31 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%103%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%108%70-130%
2037-26-5 Toluene-D8 99%98%70-130%
460-00-4 4-Bromofluorobenzene 99%99%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
24 of 49
FA26389 33.8
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-21
Lab Sample ID:FA26389-9 Date Sampled:07/27/15
Matrix:AQ - Ground Water Date Received:07/28/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E040061.D 1 07/29/15 TD n/a n/a VE1331
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
25 of 49
FA26389 33.9
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-21
Lab Sample ID:FA26389-9 Date Sampled:07/27/15
Matrix:AQ - Ground Water Date Received:07/28/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride 0.49 0.50 0.16 ug/l J
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.42 0.50 0.16 ug/l J
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
26 of 49
FA26389 33.9
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-22
Lab Sample ID:FA26389-10 Date Sampled:07/27/15
Matrix:AQ - Ground Water Date Received:07/28/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E040062.D 1 07/29/15 TD n/a n/a VE1331
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
27 of 49
FA26389 33.10
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-22
Lab Sample ID:FA26389-10 Date Sampled:07/27/15
Matrix:AQ - Ground Water Date Received:07/28/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride 0.59 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.50 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 104%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%70-130%
2037-26-5 Toluene-D8 96%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
28 of 49
FA26389 33.10
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-23
Lab Sample ID:FA26389-11 Date Sampled:07/27/15
Matrix:AQ - Ground Water Date Received:07/28/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E040063.D 2 07/29/15 TD n/a n/a VE1331
Run #2 E040092.D 5 07/30/15 TD n/a n/a VE1332
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 175 a 2.5 0.86 ug/l
108-86-1 Bromobenzene ND 1.0 0.32 ug/l
74-97-5 Bromochloromethane ND 1.0 0.32 ug/l
75-27-4 Bromodichloromethane ND 1.0 0.29 ug/l
75-25-2 Bromoform ND 1.0 0.22 ug/l
104-51-8 n-Butylbenzene 1.3 1.0 0.29 ug/l
135-98-8 sec-Butylbenzene 1.6 1.0 0.28 ug/l
98-06-6 tert-Butylbenzene ND 1.0 0.29 ug/l
56-23-5 Carbon Tetrachloride ND 1.0 0.31 ug/l
108-90-7 Chlorobenzene ND 1.0 0.32 ug/l
75-00-3 Chloroethane 2.2 1.0 0.41 ug/l
67-66-3 Chloroform ND 1.0 0.34 ug/l
95-49-8 o-Chlorotoluene ND 1.0 0.30 ug/l
106-43-4 p-Chlorotoluene ND 1.0 0.27 ug/l
124-48-1 Dibromochloromethane ND 1.0 0.25 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 1.0 0.39 ug/l
106-93-4 1,2-Dibromoethane ND 1.0 0.28 ug/l
75-71-8 Dichlorodifluoromethane ND 1.0 0.26 ug/l
95-50-1 1,2-Dichlorobenzene ND 1.0 0.26 ug/l
541-73-1 1,3-Dichlorobenzene ND 1.0 0.28 ug/l
106-46-7 1,4-Dichlorobenzene ND 1.0 0.30 ug/l
75-34-3 1,1-Dichloroethane ND 1.0 0.36 ug/l
107-06-2 1,2-Dichloroethane 15.9 1.0 0.33 ug/l
75-35-4 1,1-Dichloroethylene ND 1.0 0.34 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 1.0 0.36 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 1.0 0.34 ug/l
78-87-5 1,2-Dichloropropane ND 1.0 0.35 ug/l
142-28-9 1,3-Dichloropropane ND 1.0 0.29 ug/l
594-20-7 2,2-Dichloropropane ND 1.0 0.24 ug/l
563-58-6 1,1-Dichloropropene ND 1.0 0.32 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 1.0 0.26 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 1.0 0.25 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
29 of 49
FA26389 33.11
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-23
Lab Sample ID:FA26389-11 Date Sampled:07/27/15
Matrix:AQ - Ground Water Date Received:07/28/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 1.0 0.32 ug/l
100-41-4 Ethylbenzene 22.8 1.0 0.30 ug/l
87-68-3 Hexachlorobutadiene ND 1.0 0.24 ug/l
98-82-8 Isopropylbenzene 10.5 1.0 0.24 ug/l
99-87-6 p-Isopropyltoluene 2.1 1.0 0.24 ug/l
74-83-9 Methyl Bromide ND 1.0 0.36 ug/l
74-87-3 Methyl Chloride 1.3 1.0 0.32 ug/l
74-95-3 Methylene Bromide ND 1.0 0.34 ug/l
75-09-2 Methylene Chloride ND 4.0 2.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 1.0 0.33 ug/l
91-20-3 Naphthalene 39.4 1.0 0.24 ug/l
103-65-1 n-Propylbenzene 17.1 1.0 0.31 ug/l
100-42-5 Styrene ND 1.0 0.24 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 1.0 0.25 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 0.28 ug/l
127-18-4 Tetrachloroethylene ND 1.0 0.30 ug/l
108-88-3 Toluene 2.8 1.0 0.33 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 1.0 0.27 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 1.0 0.26 ug/l
71-55-6 1,1,1-Trichloroethane ND 1.0 0.32 ug/l
79-00-5 1,1,2-Trichloroethane ND 1.0 0.28 ug/l
79-01-6 Trichloroethylene ND 1.0 0.29 ug/l
75-69-4 Trichlorofluoromethane ND 1.0 0.32 ug/l
96-18-4 1,2,3-Trichloropropane ND 1.0 0.25 ug/l
95-63-6 1,2,4-Trimethylbenzene 50.8 1.0 0.27 ug/l
108-67-8 1,3,5-Trimethylbenzene 3.0 1.0 0.27 ug/l
75-01-4 Vinyl Chloride ND 1.0 0.26 ug/l
m,p-Xylene 6.2 2.0 0.59 ug/l
95-47-6 o-Xylene 14.6 1.0 0.27 ug/l
1330-20-7 Xylene (total)20.7 3.0 0.86 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 103%105%70-130%
17060-07-0 1,2-Dichloroethane-D4 109%109%70-130%
2037-26-5 Toluene-D8 95%97%70-130%
460-00-4 4-Bromofluorobenzene 98%98%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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FA26389 33.11
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-25
Lab Sample ID:FA26389-12 Date Sampled:07/27/15
Matrix:AQ - Ground Water Date Received:07/28/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E040064.D 1 07/29/15 TD n/a n/a VE1331
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
31 of 49
FA26389 33.12
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-25
Lab Sample ID:FA26389-12 Date Sampled:07/27/15
Matrix:AQ - Ground Water Date Received:07/28/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride 0.52 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.39 0.50 0.16 ug/l J
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
32 of 49
FA26389 33.12
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-30
Lab Sample ID:FA26389-13 Date Sampled:07/27/15
Matrix:AQ - Ground Water Date Received:07/28/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E040065.D 1 07/29/15 TD n/a n/a VE1331
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
33 of 49
FA26389 33.13
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-30
Lab Sample ID:FA26389-13 Date Sampled:07/27/15
Matrix:AQ - Ground Water Date Received:07/28/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride 0.46 0.50 0.16 ug/l J
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.20 0.50 0.16 ug/l J
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%70-130%
2037-26-5 Toluene-D8 96%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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FA26389 33.13
Accutest Laboratories
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Southeast
Section 4
35 of 49
FA26389 4
FA26389: Chain of Custody
Page 1 of 4
36 of 49
FA26389 44.1
FA26389: Chain of Custody
Page 2 of 4
37 of 49
FA26389 44.1
FA26389: Chain of Custody
Page 3 of 4
38 of 49
FA26389 44.1
FA26389: Chain of Custody
Page 4 of 4
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FA26389 44.1
Accutest Laboratories
GC/MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Southeast
Section 5
40 of 49
FA26389 5
Method Blank Summary Page 1 of 2
Job Number:FA26389
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1331-MB E040047.D 1 07/29/15 TD n/a n/a VE1331
The QC reported here applies to the following samples:Method: SM 6200B
FA26389-1, FA26389-2, FA26389-3, FA26389-4, FA26389-5, FA26389-6, FA26389-7, FA26389-8, FA26389-9,
FA26389-10, FA26389-11, FA26389-12, FA26389-13
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
41 of 49
FA26389 55.1.1
Method Blank Summary Page 2 of 2
Job Number:FA26389
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1331-MB E040047.D 1 07/29/15 TD n/a n/a VE1331
The QC reported here applies to the following samples:Method: SM 6200B
FA26389-1, FA26389-2, FA26389-3, FA26389-4, FA26389-5, FA26389-6, FA26389-7, FA26389-8, FA26389-9,
FA26389-10, FA26389-11, FA26389-12, FA26389-13
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
42 of 49
FA26389 55.1.1
Method Blank Summary Page 1 of 1
Job Number:FA26389
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1332-MB E040093.D 1 07/30/15 TD n/a n/a VE1332
The QC reported here applies to the following samples:Method: SM 6200B
FA26389-8, FA26389-11
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 104%70-130%
17060-07-0 1,2-Dichloroethane-D4 107%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
43 of 49
FA26389 55.1.2
Blank Spike Summary Page 1 of 2
Job Number:FA26389
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1331-BS E040045.D 1 07/29/15 TD n/a n/a VE1331
The QC reported here applies to the following samples:Method: SM 6200B
FA26389-1, FA26389-2, FA26389-3, FA26389-4, FA26389-5, FA26389-6, FA26389-7, FA26389-8, FA26389-9,
FA26389-10, FA26389-11, FA26389-12, FA26389-13
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 10.5 105 70-130
108-86-1 Bromobenzene 10 10.7 107 70-130
74-97-5 Bromochloromethane 10 10.7 107 70-130
75-27-4 Bromodichloromethane 10 11.6 116 70-130
75-25-2 Bromoform 10 11.6 116 70-130
104-51-8 n-Butylbenzene 10 11.5 115 70-130
135-98-8 sec-Butylbenzene 10 11.6 116 70-130
98-06-6 tert-Butylbenzene 10 11.4 114 70-130
56-23-5 Carbon Tetrachloride 10 11.9 119 70-130
108-90-7 Chlorobenzene 10 11.1 111 70-130
75-00-3 Chloroethane 10 12.5 125 60-140
67-66-3 Chloroform 10 11.3 113 70-130
95-49-8 o-Chlorotoluene 10 11.0 110 70-130
106-43-4 p-Chlorotoluene 10 11.1 111 70-130
124-48-1 Dibromochloromethane 10 11.4 114 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 9.6 96 70-130
106-93-4 1,2-Dibromoethane 10 10.8 108 70-130
75-71-8 Dichlorodifluoromethane 10 12.5 125 60-140
95-50-1 1,2-Dichlorobenzene 10 11.1 111 70-130
541-73-1 1,3-Dichlorobenzene 10 11.4 114 70-130
106-46-7 1,4-Dichlorobenzene 10 11.0 110 70-130
75-34-3 1,1-Dichloroethane 10 10.8 108 70-130
107-06-2 1,2-Dichloroethane 10 10.5 105 70-130
75-35-4 1,1-Dichloroethylene 10 10.7 107 70-130
156-59-2 cis-1,2-Dichloroethylene 10 10.4 104 70-130
156-60-5 trans-1,2-Dichloroethylene 10 11.3 113 70-130
78-87-5 1,2-Dichloropropane 10 10.4 104 70-130
142-28-9 1,3-Dichloropropane 10 10.0 100 70-130
594-20-7 2,2-Dichloropropane 10 11.8 118 70-130
563-58-6 1,1-Dichloropropene 10 11.4 114 70-130
10061-01-5 cis-1,3-Dichloropropene 10 11.3 113 70-130
10061-02-6 trans-1,3-Dichloropropene 10 12.1 121 70-130
108-20-3 Di-Isopropyl Ether 10 9.7 97 70-130
100-41-4 Ethylbenzene 10 11.1 111 70-130
87-68-3 Hexachlorobutadiene 10 12.1 121 70-130
98-82-8 Isopropylbenzene 10 11.9 119 70-130
* = Outside of Control Limits.
44 of 49
FA26389 55.2.1
Blank Spike Summary Page 2 of 2
Job Number:FA26389
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1331-BS E040045.D 1 07/29/15 TD n/a n/a VE1331
The QC reported here applies to the following samples:Method: SM 6200B
FA26389-1, FA26389-2, FA26389-3, FA26389-4, FA26389-5, FA26389-6, FA26389-7, FA26389-8, FA26389-9,
FA26389-10, FA26389-11, FA26389-12, FA26389-13
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 11.7 117 70-130
74-83-9 Methyl Bromide 10 13.7 137 60-140
74-87-3 Methyl Chloride 10 11.1 111 60-140
74-95-3 Methylene Bromide 10 10.9 109 70-130
75-09-2 Methylene Chloride 10 9.3 93 70-130
1634-04-4 Methyl Tert Butyl Ether 10 10.8 108 70-130
91-20-3 Naphthalene 10 11.7 117 70-130
103-65-1 n-Propylbenzene 10 11.3 113 70-130
100-42-5 Styrene 10 11.5 115 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 11.7 117 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 9.5 95 70-130
127-18-4 Tetrachloroethylene 10 11.5 115 70-130
108-88-3 Toluene 10 10.7 107 70-130
87-61-6 1,2,3-Trichlorobenzene 10 11.1 111 70-130
120-82-1 1,2,4-Trichlorobenzene 10 11.4 114 70-130
71-55-6 1,1,1-Trichloroethane 10 11.7 117 70-130
79-00-5 1,1,2-Trichloroethane 10 10.1 101 70-130
79-01-6 Trichloroethylene 10 11.2 112 70-130
75-69-4 Trichlorofluoromethane 10 12.6 126 60-140
96-18-4 1,2,3-Trichloropropane 10 10.4 104 70-130
95-63-6 1,2,4-Trimethylbenzene 10 11.4 114 70-130
108-67-8 1,3,5-Trimethylbenzene 10 11.4 114 70-130
75-01-4 Vinyl Chloride 10 13.2 132 60-140
m,p-Xylene 20 22.9 115 70-130
95-47-6 o-Xylene 10 11.4 114 70-130
1330-20-7 Xylene (total)30 34.3 114 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 105%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
* = Outside of Control Limits.
45 of 49
FA26389 55.2.1
Blank Spike Summary Page 1 of 1
Job Number:FA26389
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1332-BS E040082.D 1 07/30/15 TD n/a n/a VE1332
The QC reported here applies to the following samples:Method: SM 6200B
FA26389-8, FA26389-11
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 10.5 105 70-130
1634-04-4 Methyl Tert Butyl Ether 10 11.9 119 70-130
91-20-3 Naphthalene 10 12.2 122 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 104%70-130%
17060-07-0 1,2-Dichloroethane-D4 105%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
* = Outside of Control Limits.
46 of 49
FA26389 55.2.2
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA26389
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA26389-6MS E040072.D 1 07/29/15 TD n/a n/a VE1331
FA26389-6MSD E040073.D 1 07/29/15 TD n/a n/a VE1331
FA26389-6 E040058.D 1 07/29/15 TD n/a n/a VE1331
The QC reported here applies to the following samples:Method: SM 6200B
FA26389-1, FA26389-2, FA26389-3, FA26389-4, FA26389-5, FA26389-6, FA26389-7, FA26389-8, FA26389-9,
FA26389-10, FA26389-11, FA26389-12, FA26389-13
FA26389-6 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene ND 10 10.2 102 10 10 100 2 70-130/20
108-86-1 Bromobenzene ND 10 10.5 105 10 10.4 104 1 70-130/20
74-97-5 Bromochloromethane ND 10 10.7 107 10 10.5 105 2 70-130/20
75-27-4 Bromodichloromethane ND 10 11.1 111 10 10.6 106 5 70-130/20
75-25-2 Bromoform ND 10 9.7 97 10 9.7 97 0 70-130/20
104-51-8 n-Butylbenzene ND 10 10.6 106 10 10.6 106 0 70-130/20
135-98-8 sec-Butylbenzene ND 10 11.1 111 10 10.9 109 2 70-130/20
98-06-6 tert-Butylbenzene ND 10 11.2 112 10 10.9 109 3 70-130/20
56-23-5 Carbon Tetrachloride ND 10 11.7 117 10 10.8 108 8 70-130/20
108-90-7 Chlorobenzene ND 10 10.6 106 10 10.4 104 2 70-130/20
75-00-3 Chloroethane ND 10 8.6 86 10 8.4 84 2 60-140/20
67-66-3 Chloroform ND 10 11.1 111 10 10.8 108 3 70-130/20
95-49-8 o-Chlorotoluene ND 10 10.9 109 10 10.6 106 3 70-130/20
106-43-4 p-Chlorotoluene ND 10 10.8 108 10 10.7 107 1 70-130/20
124-48-1 Dibromochloromethane ND 10 10.4 104 10 10.1 101 3 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 10 9.6 96 10 10 100 4 70-130/20
106-93-4 1,2-Dibromoethane ND 10 10.5 105 10 10.6 106 1 70-130/20
75-71-8 Dichlorodifluoromethane ND 10 9.2 92 10 9.1 91 1 60-140/20
95-50-1 1,2-Dichlorobenzene ND 10 10.9 109 10 10.7 107 2 70-130/20
541-73-1 1,3-Dichlorobenzene ND 10 11.1 111 10 10.9 109 2 70-130/20
106-46-7 1,4-Dichlorobenzene ND 10 10.7 107 10 10.5 105 2 70-130/20
75-34-3 1,1-Dichloroethane ND 10 10.8 108 10 10.4 104 4 70-130/20
107-06-2 1,2-Dichloroethane ND 10 10.7 107 10 10.7 107 0 70-130/20
75-35-4 1,1-Dichloroethylene ND 10 10.8 108 10 10.6 106 2 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 10 9.9 99 10 9.8 98 1 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 10 11.5 115 10 10.9 109 5 70-130/20
78-87-5 1,2-Dichloropropane ND 10 10.2 102 10 10.0 100 2 70-130/20
142-28-9 1,3-Dichloropropane ND 10 9.7 97 10 9.9 99 2 70-130/20
594-20-7 2,2-Dichloropropane ND 10 10.7 107 10 10.3 103 4 70-130/20
563-58-6 1,1-Dichloropropene ND 10 11.2 112 10 10.8 108 4 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 10 10.2 102 10 9.4 94 8 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 10 11.2 112 10 10.5 105 6 70-130/20
108-20-3 Di-Isopropyl Ether ND 10 10.1 101 10 9.9 99 2 70-130/20
100-41-4 Ethylbenzene ND 10 10.8 108 10 10.6 106 2 70-130/20
87-68-3 Hexachlorobutadiene ND 10 10.3 103 10 10.6 106 3 70-130/20
98-82-8 Isopropylbenzene ND 10 11.3 113 10 11.0 110 3 70-130/20
* = Outside of Control Limits.
47 of 49
FA26389 55.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA26389
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA26389-6MS E040072.D 1 07/29/15 TD n/a n/a VE1331
FA26389-6MSD E040073.D 1 07/29/15 TD n/a n/a VE1331
FA26389-6 E040058.D 1 07/29/15 TD n/a n/a VE1331
The QC reported here applies to the following samples:Method: SM 6200B
FA26389-1, FA26389-2, FA26389-3, FA26389-4, FA26389-5, FA26389-6, FA26389-7, FA26389-8, FA26389-9,
FA26389-10, FA26389-11, FA26389-12, FA26389-13
FA26389-6 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 10 11.1 111 10 10.9 109 2 70-130/20
74-83-9 Methyl Bromide ND 10 9.3 93 10 9.4 94 1 60-140/20
74-87-3 Methyl Chloride 1.0 10 9.4 84 10 9.3 83 1 60-140/20
74-95-3 Methylene Bromide ND 10 10.8 108 10 10.7 107 1 70-130/20
75-09-2 Methylene Chloride ND 10 9.5 95 10 9.4 94 1 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 10 10.8 108 10 10.9 109 1 70-130/20
91-20-3 Naphthalene 0.15 J 10 10.8 107 10 11.9 118 10 70-130/20
103-65-1 n-Propylbenzene ND 10 11.0 110 10 10.7 107 3 70-130/20
100-42-5 Styrene ND 10 10.6 106 10 10.4 104 2 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 10 11.3 113 10 10.7 107 5 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 10 9.6 96 10 9.9 99 3 70-130/20
127-18-4 Tetrachloroethylene ND 10 11.1 111 10 10.6 106 5 70-130/20
108-88-3 Toluene ND 10 10.3 103 10 10.0 100 3 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 10 10.2 102 10 11.1 111 8 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 10 10.2 102 10 11.0 110 8 70-130/20
71-55-6 1,1,1-Trichloroethane ND 10 11.8 118 10 11.3 113 4 70-130/20
79-00-5 1,1,2-Trichloroethane ND 10 10.2 102 10 10.3 103 1 70-130/20
79-01-6 Trichloroethylene ND 10 10.7 107 10 10.3 103 4 70-130/20
75-69-4 Trichlorofluoromethane ND 10 9.4 94 10 9.1 91 3 60-140/20
96-18-4 1,2,3-Trichloropropane ND 10 10.4 104 10 10.6 106 2 70-130/20
95-63-6 1,2,4-Trimethylbenzene ND 10 11.0 110 10 10.8 108 2 70-130/20
108-67-8 1,3,5-Trimethylbenzene ND 10 10.9 109 10 10.6 106 3 70-130/20
75-01-4 Vinyl Chloride ND 10 9.9 99 10 9.3 93 6 60-140/20
m,p-Xylene ND 20 22.2 111 20 21.6 108 3 70-130/20
95-47-6 o-Xylene ND 10 11.0 110 10 10.8 108 2 70-130/20
1330-20-7 Xylene (total)ND 30 33.2 111 30 32.3 108 3 70-130/20
CAS No.Surrogate Recoveries MS MSD FA26389-6 Limits
1868-53-7 Dibromofluoromethane 105%104%102%70-130%
17060-07-0 1,2-Dichloroethane-D4 108%109%105%70-130%
2037-26-5 Toluene-D8 99%97%98%70-130%
460-00-4 4-Bromofluorobenzene 99%98%99%70-130%
* = Outside of Control Limits.
48 of 49
FA26389 55.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1
Job Number:FA26389
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA26422-4MS E040100.D 1 07/30/15 TD n/a n/a VE1332
FA26422-4MSD E040101.D 1 07/30/15 TD n/a n/a VE1332
FA26422-4 E040086.D 1 07/30/15 TD n/a n/a VE1332
The QC reported here applies to the following samples:Method: SM 6200B
FA26389-8, FA26389-11
FA26422-4 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene ND 10 10.1 101 10 10.0 100 1 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 10 10.8 108 10 10.5 105 3 70-130/20
91-20-3 Naphthalene ND 10 13.9 139*10 12.3 123 12 70-130/20
CAS No.Surrogate Recoveries MS MSD FA26422-4 Limits
1868-53-7 Dibromofluoromethane 105%104%104%70-130%
17060-07-0 1,2-Dichloroethane-D4 107%105%106%70-130%
2037-26-5 Toluene-D8 99%99%99%70-130%
460-00-4 4-Bromofluorobenzene 98%100%99%70-130%
* = Outside of Control Limits.
49 of 49
FA26389 55.3.2