WA-688_9785_CA_MRP_20150212

EXECUTIVE SUMMARY

The former Red Apple Market #21 is located along NC Highway 561 West, in Saint John, Hertford
County, North Carolina (Figure 1). According to information obtained from the file and a Semi-Annual
Ground Water Monitoring Report dated November 18, 2004, prepared by CES Engineering, PC (CES),
the site previously operated as a petroleum retail facility. Two 1,000-gallon gasoline USTs and one 550-
gallon gasoline UST were removed from the site in October 1992. In addition, one 550-gallon gasoline
UST was closed-in-place in October 1992. The site risk classification is currently high due to the
presence of potable water supply wells within a 1,000-foot radius of the site.

On January 29, 2015, twenty monitoring wells and two water supply wells were gauged, purged and/or
sampled. Concentrations of requested method constituents that exceeded the Maximum Allowable
Concentrations specified in T15A NCAC 2L.0202 were reported in the ground water samples collected
from MW-2R, MW-3R, MW-4R, MW-5R, MW-9, MW-10 and MW-23. A concentration of
bromodichloromethane that exceeded the MAC was reported in the ground water sample collected from
WSW-6. None of the contaminant concentrations exceeded the gross contamination levels.

The total volatile organic compound (VOC) concentrations reported in monitoring wells MW-2R, MW-
3R, MW-4R and MW-5R in the May 2014 and January 2015 ground water sampling events were
35,466.62 g/l and 28,219.14 g/l, respectively. Based on this information, total VOC concentrations in
monitoring wells MW-2R, MW-3R, MW-4R and MW-5R have been reduced by approximately 20.4% by
completing the Mobile Multi-Phase Extraction (MMPE) activities conducted in October 2014.

GRI recommends that MMPE events and semi-annual ground water monitoring should continue at the
site until contaminant concentrations are reduced. Recovery wells could be installed in the vicinity of
MW-2R and MW-4R in order to enhance the results of the MMPE activities. The next monitoring event
is tentatively scheduled for July 2015.

TABLE OF CONTENTS

1.0 SITE HISTORY AND CHARACTERIZATION .................................................................... 1
2.0 CURRENT SITE ASSESSMENT ............................................................................................ 1
3.0 GROUND WATER QUALITY ................................................................................................ 1
4.0 CORRECTIVE ACTION EVALUATION .............................................................................. 2
5.0 CONCLUSIONS AND RECOMMENDATIONS .................................................................... 4
6.0 LIMITATIONS ......................................................................................................................... 5

FIGURES
Figure 1: Site Location Map
Figure 2: Site Map
Figure 3: Water Table Surface Map
Figure 4: Ground Water Quality Map
Figure 5: Benzene Isoconcentration Map
Figure 6: MTBE Isoconcentration Map
Figure 7: Naphthalene Isoconcentration Map
Figure 8: 1,2,-Dichloroethane Isoconcentration Map

TABLES
Table 1: Well Construction and Gauging Information
Table 2: Summary of Ground Water Sample Analytical Results

APPENDICES
Appendix A: Laboratory Report – Ground Water Samples
Appendix B: Graphs of Individual VOC Concentrations vs. Time
Appendix C: Graphs of Total VOC Concentrations vs. Depths to Ground Water

1
1.0 SITE HISTORY AND CHARACTERIZATION
The Red Apple Market #21 site is located along NC Highway 561 West in Saint John, Hertford County,
North Carolina (Figure 1). According to available information, two 1,000-gallon gasoline and one 550-
gallon gasoline underground storage tanks (USTs) were removed from the site in October 1992. In
addition, one 550-gallon gasoline UST was closed-in-place in October 1992. Twenty-seven Type II
monitoring wells (MW-1 through MW-6, MW-8 through MW-23, MW-25 and MW-27 through MW-30),
one Type III monitoring well (MWD-7) and three recovery wells (RW-1 through RW-3) were installed at
the site during past ground water assessment and remediation activities. Please note, monitoring wells
MW-6, MW-11, MW-12 and MW-13 have been destroyed. A total of 4,381.57 tons of contaminated soil
was removed from the site between May 16 and June 2, 2011. Prior to the May-June 2011 soil
excavation, monitoring wells MW-1 through MW-5, MWD-7 as well as recovery wells RW-1 and RW-3
were abandoned. Monitoring wells MW-1R through MW-5R were installed following the completion of
the May-June 2011 excavation activities. Ground water samples collected from monitoring wells at the
site and nearby water supply wells have exceeded the maximum allowable concentrations (MACs) during
past sampling events. Free product has been reported in monitoring wells MW-2, MW-3, MW-5, MW-
2R, MW-3R, MW-4R and MW-5R.

Please note that certain information contained in this report was obtained under the supervision of
previous consultants. Although Geological Resources, Inc. (GRI) cannot verify the accuracy of
information obtained from previous reports, for the purposes of this report, it is assumed to be correct.
Please refer to previous submittals for further historical information regarding the site.

2.0 CURRENT SITE ASSESSMENT
The purpose of this report is to present the results of ground water assessment activities conducted on
January 29, 2015 at the Red Apple Market #21 site. The activities were conducted in accordance with
GRI proposal number 14-624 which was submitted to NCDENR on October 15, 2014 and approved as
Task Authorization No. 9785-061 on January 12, 2015. .

3.0 GROUND WATER QUALITY
Twenty monitoring wells (MW-1R through MW-5R, MW-8, MW-9, MW-10, MW-14, MW-15, MW-20
through MW-23, MW-25, MW-27, MW-28 and MW-30) and two water supply wells (WSW-4 and
WSW-6) were gauged, purged and/or sampled on January 29, 2015. Please note, monitoring wells MW-

2
16 and MW-17 were inaccessible and WSW-5 was inactive, therefore, these wells were not sampled. The
depths to ground water in the monitoring wells during the January 2015 sampling event ranged from 9.76
to 15.58 feet below the tops of well casings. Ground water elevations in the Type II monitoring wells
relative to mean sea level ranged from 39.86 to 45.00 feet. Please note, the depth to water and ground
water elevation for MW-23 appear to be anomalies and were not included in the January 29, 2015
gauging data. Based on this information, ground water flow for the site during the January 2015 gauging
event was convergent toward the vicinity of the May-June 2011 excavation area. The average horizontal
hydraulic gradient across the site was approximately 0.01 feet per foot. A Site Map showing the locations
of the monitoring wells and the structures on-site and on surrounding properties has been included as
Figure 2. A Water Table Surface Map for the January 2015 sampling event has been included as Figure
3. A summary of well construction and gauging information is presented in Table 1.

Laboratory analyses were performed on the ground water samples collected from the referenced
monitoring wells during the January 2015 sampling event. The collected ground water samples were
submitted for analyses of volatile organic compounds (VOCs) using EPA Method 6200B.

Concentrations of individual BTEX constituents, MTBE, naphthalene, 1,2-dichloroethane,
isopropylbenzene, n-propylbenzene, 1,3,5-trimethylbenzene and/or 1,2,4-trimethylbenzene that exceeded
the Maximum Allowable Concentrations (MACs) specified in T15A NCAC 2L.0202 were reported in the
ground water samples collected from MW-2R, MW-3R, MW-4R, MW-5R, MW-9, MW-10 and MW-23.
A concentration of bromodichloromethane that exceeded the MAC was reported in the ground water
sample collected from WSW-6. None of the contaminant concentrations exceeded the gross
contamination levels (GCLs). A Ground Water Quality Map based on data from the January 2015
sampling event has been included as Figure 4. Contaminant specific isoconcentration maps for benzene,
MTBE, naphthalene and 1,2-dichloroethane are included as Figures 5 through 8, respectively. A
summary of ground water sample analytical results is presented in Table 2. A complete laboratory report
has been included in Appendix A. Please note that the absorbent boom that had been installed in MW-
4R following the completion of the October 2014 MMPE event was reinstalled in MW-4R after the well
was gauged, purged and sampled on January 29, 2015.

4.0 CORRECTIVE ACTION EVALUATION
In accordance with the System Enhancement Report dated May 14, 2010, Soil and Ground Water
Monitoring Report dated November 19, 2010, and the NCDENR correspondence dated June 10, 2010,

3
soil excavation activities were conducted as the new method for corrective action for this incident. Please
note that a pump and treat remediation system reportedly operated at the site from February 1999 to
September 2005 and October 2008 to May 2010. Between May 26 and June 2, 2011, a total of 4,381.57
tons of contaminated soil was removed from the site and transported to a permitted disposal facility.

Following the completion of the May-June 2011 excavation activities, four mobile multi-phase extraction
(MMPE) events have been conducted at the site on MW-2R, MW-3R, MW-4R, MW-5R and/or MW-9.
The MMPE events were conducted between December 2012 and October 2014. A total of 26,887 gallons
of contaminated ground water has been removed by the MMPE events. Approximately 27.36 gallons of
liquid and vapor phase free product have been removed by the MMPE events conducted between
December 2012 and October 2014.

Based on a comparison of ground water quality data obtained from the October 2010 and January 2015
sampling events, the total VOC concentrations (including BTEX constituents MTBE, and naphthalene)
from monitoring wells MW-1/1R, MW-3/3R and MW-5/5R have been significantly reduced as a result of
the soil excavation and dewatering activities conducted in 2011 as well as the MMPE events conducted
between December 2012 and October 2014. A comparison of data between October 2010 and January
2015 indicates a contaminant reduction of approximately 98.9% in MW-1/1R (from 74.45 g/l in October
2010 to 0.80 g/l in January 2015); approximately 99.7% in MW-3/3R (from 5,888 g/l in October 2010
to 16.14 g/l in January 2015), and approximately 65.1% in MW-5/5R (from 673 g/l in October 2010 to
235 g/l in January). Please note, MW-2 contained a free product thickness of 2.04 feet during the
October 2010 sampling event. MW-4 was not located during the October 2010 sampling event. After the
excavation activities, MW-2R and MW-4R have periodically contained free product. The contaminant
concentrations in all wells should continue to naturally attenuate and reduce over time since the secondary
source has been removed.

The MMPE events have been conducted at the site in order to recover free product and reduce
contaminant concentrations, with the most recent event being conducted on monitoring wells MW-2R,
MW-3R, MW-4R and MW-5R between October 13 and 17, 2014. Based on a comparison of ground
water quality data obtained from the May 2014 and January 2015 sampling events, the total VOC
concentrations (including BTEX constituents, MTBE, and naphthalene) from monitoring wells MW-
2/2R, MW-3/3R, MW-4/4R and MW-5/5R have been reduced as a result of the MMPE activities. A
comparison of data between May 2014 and January 2015 indicates a contaminant reduction of
approximately 20.3% in MW-2R (from 22,355 g/l in May 2014 to 17,804 g/l in January 2015),

4
approximately 18.6 % in MW-4R (from 12,486 g/l in May 2014 to 10,164 g/l in January 2015) and
approximately 61.8% in MW-5R (from 614 g/l in May 2014 to 235 g/l in January 2015). Contaminant
concentrations increased in MW-3R approximately 43.9% (from 11 g/l in May 2014 to 16 g/l in
January 2015) likely due to the MMPE activities drawing contaminants from underneath the site building.
No free product was observed at the site during the January 2015 sampling event. Graphs showing
variations in individual BTEX constituents, MTBE and naphthalene concentrations versus time and
variations in total VOCs versus depths to ground water in each of the affected wells have been included as
Appendices B and C, respectively.

5.0 CONCLUSIONS AND RECOMMENDATIONS
 The average depth to ground water in the monitoring wells during the January 2015 sampling
event was 13.56 feet. Ground water flow for the site during the January 2015 gauging event was
generally convergent toward the vicinity of the May-June 2011 excavation area. The average
horizontal hydraulic gradient across the site was approximately 0.01 feet per foot.
 Concentrations of individual BTEX constituents, MTBE, naphthalene, 1,2-dichloroethane,
isopropylbenzene, n-propylbenzene, 1,3,5-trimethylbenzene and/or 1,2,4-trimethylbenzene that
exceeded the MACs were reported in the ground water samples collected from MW-2R, MW-3R,
MW-4R, MW-5R, MW-9, MW-10 and MW-23. None of the contaminant concentrations
exceeded the GCL.
 A concentration of bromodichloromethane that exceeded the MAC was reported in the ground
water sample collected from WSW-6 during the January 2015 sampling event.
Bromodichloromethane is a common water treatment chemical. An evaluation should be made
on the sample collection source during the next sampling event to determine if municipal water is
being sampled at the WSW-6 spigot. An attempt should be made to sample WSW-6 at the
wellhead. Additionally, receptor information should be updated for this incident.
 Total VOC concentrations in monitoring wells MW-2R, MW-3R, MW-4R and MW-5R have
been reduced by approximately 20.4% by completing the October 2014 MMPE activities.
Furthermore, monitoring well MW-4R had measurable free product prior to the MMPE event.
Free product was removed from the well and total VOC concentrations were significantly
reduced.
 The absorbent boom that had been installed in MW-4R following the completion of the October
2014 MMPE event was removed prior to gauging on January 29, 2015. The boom was replaced

5
following the completion of the January 2015 sampling activities. Absorbent booms should
continue to be used, as needed at the site until free product is no longer present.
 Based on these results, GRI recommends that additional MMPE events should be conducted at
the site in order reduce contaminant concentrations. Additionally, recovery wells could be
installed in the vicinity of MW-2R and MW-4R in order to enhance the results of the MMPE
activities. Semi-annual ground water monitoring should continue at the site until contaminant
concentrations are reduced. The next semi-annual ground water monitoring event is tentatively
scheduled for July 2015.
6.0 LIMITATIONS
This report has been prepared for the exclusive use of Red Apple Markets, Inc. for specific application to
the referenced site in Hertford County, North Carolina. The assessment was conducted based on the
scope of work and level of effort desired by NCDENR and with resources adequate only for that scope of
work. Our findings have been developed in accordance with generally accepted standards of
environmental practices in the State of North Carolina, available information, and our professional
judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would be
interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data. Please note that field data collected prior
to the July 2007 sampling and updated receptor survey event was not obtained under the supervision of
GRI. Although the accuracy of this information cannot be verified, for the purpose of this report GRI
assumes that it is correct.

FIGURES

TABLES
01/18/07 12.87 0.00 87.13      
06/06/07 13.15 0.00 86.85
06/02/08 14.10 0.00 85.90
12/18/08 16.41 0.00 83.59
03/24/09 14.62 0.00 85.38
06/25/09 15.00 0.00 85.00
09/16/09 15.58 0.02 84.44 Before AFVR
09/16/09 15.64 0.00 84.36 After AFVR
09/21/09 15.66 0.00 84.34
11/17/09 15.42 0.00 84.58 Before AFVR
11/17/09 15.55 0.01 84.46 After AFVR
12/30/09 14.85 0.00 85.15
06/28/10 14.02 0.00 85.98
10/05/10 14.74 0.00 85.26 Abandoned
10/12/11 15.73 0.00 39.03
01/31/12 15.71 0.00 39.05
05/15/12 14.77 0.00 39.99
01/22/13 14.68 0.00 40.08
11/18/13 15.84 0.00 38.92
05/27/14 14.36 0.00 40.40
01/29/15 14.53 0.00 40.23
01/18/07 14.81 3.25 87.58
06/06/07 13.07 0.69 87.12
06/02/08 15.20 2.27 86.35
11/06/08 16.90 2.60 84.93 Before AFVR
11/06/08 15.04 0.16 84.70 After AFVR
12/18/08 15.25 0.69 84.94
03/24/09 16.90 3.54 85.74
06/10/09 15.84 2.12 85.58 Before AFVR
06/10/06 14.29 0.01 85.32 After AFVR
06/25/09 14.90 0.46 85.09
09/16/09 14.85 1.17 85.75 Before AFVR
09/16/09 15.05 0.00 84.55 After AFVR
09/21/09 15.07 0.03 84.56
11/17/09 15.44 0.59 84.67 Before AFVR
11/17/09 14.98 0.02 84.64 After AFVR
12/30/09 14.65 0.33 85.23
06/28/10 15.65 2.04 85.70
10/05/10 15.81 2.79 86.18 Abandoned
10/12/11 14.71 0.00 39.18
01/31/12 14.67 0.22 39.41
05/15/12 13.96 0.23 40.13
12/17/12 15.25 0.75 39.28 Before MMPE
12/21/12 17.94 0.00 35.95 After MMPE
01/22/13 13.85 0.00 40.04
10/07/13 15.00 0.00 38.89 Before MMPE
10/11/13 15.99 0.00 37.90 After MMPE
11/18/13 14.95 0.00 38.94
04/28/14 13.22 0.00 40.67 Before MMPE
05/02/14 16.95 0.00 36.94 After MMPE
05/27/14 13.71 0.00 40.18
10/13/14 14.48 0.00 39.41 Before MMPE
10/17/14 16.70 0.00 37.19 After MMPE
01/29/15 13.86 0.00 40.03
01/18/07 14.02 0.00 86.99
06/06/07 13.86 0.00 87.15
06/02/08 14.77 0.00 86.24
12/18/08 16.27 0.00 84.74
03/24/09 15.90 0.00 85.11
06/25/09 15.80 0.00 85.21
09/16/09 16.72 0.02 84.31 Before AFVR
09/16/09 16.40 0.01 84.62 After AFVR
09/21/09 16.40 0.00 84.61
11/17/09 16.77 0.00 84.24 Before AFVR
11/17/09 16.40 0.01 84.62 After AFVR
12/30/09 13.97 0.00 87.04
06/28/10 15.76 0.00 85.25
10/05/10 15.50 0.00 85.51 Abandoned
10/12/11 14.48 0.00 40.12
01/31/12 15.88 0.00 38.72
05/15/12 14.31 0.00 40.29
12/17/12 14.54 0.00 40.06 Before MMPE
12/21/12 11.85 0.30 43.01 After MMPE
01/22/13 15.09 0.00 39.51
10/07/13 16.20 0.00 38.40 Before MMPE
10/11/13 11.58 0.00 43.02 After MMPE
11/18/13 16.48 0.00 38.12
04/28/14 13.75 0.00 40.85 Before MMPE
05/02/14 10.23 0.00 44.37 After MMPE
05/27/14 16.74 0.00 37.86
10/13/14 15.23 0.00 39.37 Before MMPE
10/17/14 11.74 0.00 42.86 After MMPE
01/29/15 14.62 0.00 39.98
54.76
53.89
MW-3R 10/12/11 10 10-20 20 54.60
MW-2R
101.01
99.60
MW-1 05/06/93 7 7-27
MW-2 05/07/93 10 10-20
MW-1R 10/12/11
Comments
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET # 21 (INCIDENT NO. 9785)
Date: 02/02/15 Facility ID # : 0-030290
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Bottom
of Well
(ft. BGS)
Ground
Water
Elevation*
(ft.)
27 100.00
Top of
Casing
Elevation*
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
10/12/11 10 10-20 20
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y
ft. BGS)
10 10-20 20
20
MW-3 05/07/93 10 10-20 20
Page 1 of 5
Comments
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET # 21 (INCIDENT NO. 9785)
Date: 02/02/15 Facility ID # : 0-030290
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Bottom
of Well
(ft. BGS)
Ground
Water
Elevation*
(ft.)
Top of
Casing
Elevation*
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y
ft. BGS)
01/18/07 12.69 0.00 87.37
06/14/07 13.06 0.00 87.00
06/02/08 NM NM NM Destroyed
10/12/11 13.28 0.13 40.85
01/31/12 13.12 0.29 41.15
05/15/12 14.13 0.51 40.33
01/22/13 14.22 0.30 40.06
10/07/13 15.16 0.43 39.23 Before MMPE
10/11/13 11.65 0.03 42.40 After MMPE
11/18/13 14.86 0.01 39.17
04/28/14 11.21 0.00 42.81 Before MMPE
05/02/14 11.55 0.45 42.86 After MMPE
05/27/14 13.58 0.00 40.44
10/13/14 15.08 0.02 38.96 Before MMPE
10/17/14 13.64 0.09 40.46 After MMPE
01/29/15 14.15 0.00 39.87
01/18/07 13.02 0.00 87.80
06/06/07 13.23 0.00 87.59
06/02/08 NM NM NM Not Located
12/18/08 NM NM NM Dry
03/24/09 NM NM NM Dry
06/25/09 NM NM NM Dry
09/21/09 15.47 0.00 85.35
12/30/09 14.44 0.00 86.38
06/28/10 13.99 0.00 86.83
10/05/10 14.60 0.00 86.22 Abandoned
10/12/11 14.16 0.02 40.32
01/31/12 15.36 0.00 39.10
05/15/12 14.20 0.00 40.26
12/17/12 14.57 0.00 39.89 Before MMPE
12/21/12 14.10 0.00 40.36 After MMPE
01/22/13 14.45 0.00 40.01
11/18/13 15.44 0.00 39.02
04/28/14 13.97 0.00 40.49 Before MMPE
05/02/14 13.75 0.00 40.71 After MMPE
05/27/14 13.98 0.00 40.48
10/13/14 14.85 0.00 39.61 Before MMPE
10/17/14 14.90 0.00 39.56 After MMPE
01/29/15 14.20 0.00 40.26
MW-6 NA 01/18/07 NA NA NA 100.49 NM NM NM Destroyed
01/18/07 12.35 0.00 87.45
06/06/07 12.43 0.00 87.37
06/02/08 21.80 0.00 78.00
12/18/08 15.27 0.00 84.53
03/24/09 14.55 0.00 85.25
06/25/09 14.85 0.00 84.95
09/21/09 15.52 0.00 84.28
12/30/09 14.70 0.00 85.10
06/28/10 13.87 0.00 85.93
10/05/10 NM NM NM Abandoned
01/18/07 8.59 0.00 92.27
06/06/07 12.87 0.00 87.99
06/02/08 NM NM NM Not Located
12/18/08 17.22 0.00 83.64
03/24/09 4.97 0.00 95.89
06/25/09 16.10 0.00 84.76
09/21/09 17.35 0.00 83.51
12/30/09 6.28 0.00 94.58
06/28/10 14.79 0.00 86.07
10/05/10 12.08 0.00 88.78
10/12/11 16.24 0.00 38.52
01/31/12 11.46 0.00 43.30
05/15/12 13.32 0.00 41.44
11/18/13 15.30 0.00 39.46
05/27/14 12.74 0.00 42.02
01/29/15 9.76 0.00 45.00
01/18/07 7.73 0.00 92.95
06/06/07 9.35 0.00 91.33
06/02/08 8.21 0.00 92.47
12/18/08 11.72 0.00 88.96
03/24/09 11.60 0.00 89.08
06/25/09 11.73 0.00 88.95
09/21/09 12.62 0.00 88.06
12/30/09 12.24 0.00 88.44
06/28/10 12.40 0.00 88.28
10/05/10 12.69 0.00 87.99
10/12/11 10.00 0.00 44.67
01/31/12 10.59 0.00 44.08
05/15/12 9.94 0.00 44.73
12/17/12 10.88 0.00 43.79 Before MMPE
12/21/12 9.41 0.00 45.26 After MMPE
01/22/13 5.34 0.00 49.33
11/18/13 11.49 0.00 43.18
05/27/14 9.64 0.00 45.03
01/29/15 10.94 0.00 43.73
MWD-7 02/08/94 30 30-35
MW-5R 10/12/11 10 10-20 20
10 10-20 20
NA 100.82
MW-4 NA NA NA NA 100.06
54.02MW-4R 10/12/11
54.46
MW-5 NA NA NA
MW-8 03/14/94 9 9-19 19
54.76
35 99.80
100.86
MW-9 03/14/94 9 199-19
54.67
100.68
Page 2 of 5
Comments
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET # 21 (INCIDENT NO. 9785)
Date: 02/02/15 Facility ID # : 0-030290
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Bottom
of Well
(ft. BGS)
Ground
Water
Elevation*
(ft.)
Top of
Casing
Elevation*
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y
ft. BGS)
01/18/07 14.26 0.00 86.86
06/06/07 14.38 0.00 86.74
06/02/08 15.50 0.00 85.62
12/18/08 16.62 0.00 84.50
03/24/09 15.99 0.00 85.13
06/25/09 16.16 0.00 84.96
09/21/09 16.85 0.00 84.27
12/30/09 15.98 0.00 85.14
06/28/10 15.45 0.00 85.67
10/05/10 15.97 0.00 85.15
10/12/11 16.40 0.00 38.81
01/31/12 16.05 0.00 39.16
05/15/12 NS NS NS Inaccessable
01/22/13 15.50 0.00 39.71
11/18/13 16.48 0.00 38.73
05/27/14 15.12 0.00 40.09
01/29/15 15.34 0.00 39.87
MW-11 NA 01/18/07 NA NA NA 100.08 NM NM NM Destroyed
MW-12 NA 01/18/07 NA NA NA 99.49 NM NM NM Destroyed
01/18/07 12.72 0.00 87.11
06/06/07 12.83 0.00 87.00 Destroyed
01/18/07 13.78 0.00 87.59
06/06/07 13.93 0.00 87.44
06/02/08 14.90 0.00 86.47
12/18/08 16.49 0.00 84.88
03/24/09 13.73 0.00 87.64
06/25/09 15.85 0.00 85.52
09/21/09 16.60 0.00 84.77
12/30/09 15.92 0.00 85.45
06/28/10 14.92 0.00 86.45
10/05/10 15.83 0.00 85.54
10/12/11 16.28 0.00 39.11
01/31/12 16.00 0.00 39.39
01/22/13 15.44 0.00 39.95
11/18/13 16.22 0.00 39.17
05/27/14 14.91 0.00 40.48
01/29/15 15.18 0.00 40.21
01/18/07 14.32 0.00 87.66
06/06/07 14.43 0.00 87.55
06/02/08 15.47 0.00 86.51
12/18/08 NM NM NM Not Sampled
03/24/09 16.26 0.00 85.72
06/25/09 16.38 0.00 85.60
09/21/09 17.10 0.00 84.88
12/30/09 NM NM NM Not Sampled
06/28/10 15.42 0.00 86.56
10/05/10 16.35 0.00 85.63
10/12/11 16.79 0.00 39.22
01/31/12 16.55 0.00 39.46
11/18/13 16.75 0.00 39.26
05/27/14 15.42 0.00 40.59
01/29/15 15.71 0.00 40.30
01/18/07 NM NM NM
06/06/07 13.34 0.00 87.56
06/02/08 NM NM NM NA
12/18/08 NM NM NM Not Sampled
03/24/09 15.31 0.00 85.59
06/25/09 15.31 0.00 85.59
09/21/09 NM NM NM Not Sampled
12/30/09 NM NM NM Not Sampled
06/28/10 NM NM NM Not Sampled
10/05/10 15.28 0.00 85.62
10/12/11 15.70 0.00 39.18
01/31/12 15.46 0.00 39.42
11/18/13 NM NM NM Not Sampled
05/27/14 14.40 0.00 40.48
01/29/15 NM NM NM Not Sampled
01/18/07 NM NM NM
06/06/07 11.93 0.00 87.36
06/02/08 NM NM NM NA
12/18/08 NM NM NM Not Sampled
03/24/09 13.81 0.00 85.48
06/25/09 13.84 0.00 85.45
09/21/09 NM NM NM Not Sampled
12/30/09 NM NM NM Not Sampled
06/28/10 NM NM NM Not Sampled
10/05/10 13.82 0.00 85.47
10/12/11 14.33 0.00 39.28
01/31/12 14.07 0.00 39.54
11/18/13 NM NM NM Not Sampled
05/27/14 12.49 0.00 41.12
01/29/15 NM NM NM Not Sampled
MW-16
NA NA NA
53.61
NA NA
99.29
100.90
12-22
NA NA
56.01
MW-13 NA NA NA NA 99.83
MW-10 03/14/94 11 11-21 21
55.21
101.12
MW-14 04/05/95 12 22
55.39
MW-15 NA NA
101.98
101.37
NA NA
54.88
MW-17 NA
Page 3 of 5
Comments
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET # 21 (INCIDENT NO. 9785)
Date: 02/02/15 Facility ID # : 0-030290
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Bottom
of Well
(ft. BGS)
Ground
Water
Elevation*
(ft.)
Top of
Casing
Elevation*
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y
ft. BGS)
01/18/07 14.09 0.00 87.89
06/06/07 14.38 0.00 87.60
06/02/08 15.24 0.00 86.74
12/18/08 16.68 0.00 85.30
03/24/09 16.04 0.00 85.94
06/25/09 16.19 0.00 85.79
09/21/09 16.92 0.00 85.06
12/30/09 16.01 0.00 85.97
06/28/10 15.38 0.00 86.60
10/05/10 NM NM NM
10/12/11 16.46 0.00 38.83
01/31/12 16.14 0.00 39.15
05/15/12 NS NS NS Inaccessable
11/18/13 16.46 0.00 38.83
05/27/14 15.23 0.00 40.06
01/29/15 15.42 0.00 39.87
01/18/07 13.14 0.00 86.80
06/06/07 13.27 0.00 86.67
06/02/08 14.15 0.00 85.79
12/18/08 15.52 0.00 84.42
03/24/09 14.81 0.00 85.13
06/25/09 15.03 0.00 84.91
09/21/09 15.73 0.00 84.21
12/30/09 14.87 0.00 85.07
06/28/10 14.19 0.00 85.75
10/05/10 NM NM NM
10/12/11 15.30 0.00 38.76
01/31/12 15.01 0.00 39.05
05/15/12 NS NS NS Inaccessable
11/18/13 15.33 0.00 38.73
05/27/14 14.55 0.00 39.51
01/29/15 12.48 0.00 41.58
01/18/07 12.86 0.00 86.93
06/06/07 13.25 0.00 86.54
06/02/08 14.07 0.00 85.72
12/18/08 15.46 0.00 84.33
03/24/09 14.75 0.00 85.04
06/25/09 14.98 0.00 84.81
09/21/09 15.40 0.00 84.39
12/30/09 14.88 0.00 84.91
06/28/10 14.23 0.00 85.56
10/05/10 NM NM NM
10/12/11 15.28 0.00 38.80
01/31/12 15.02 0.00 39.06
05/15/12 14.20 0.00 39.88
11/18/13 15.30 0.00 38.78
05/27/14 NM NM NM Inaccessable
01/29/15 14.22 0.00 39.86
01/18/07 14.18 0.00 86.51
06/06/07 13.97 0.00 86.72
06/02/08 14.95 0.00 85.74
12/18/08 16.25 0.00 84.44
03/24/09 15.56 0.00 85.13
06/25/09 15.80 0.00 84.89
09/21/09 16.55 0.00 84.14
12/30/09 16.62 0.00 84.07
06/28/10 15.07 0.00 84.93
10/05/10 15.59 0.00 85.10
10/12/11 16.22 0.00 38.62
01/31/12 15.54 0.00 39.30
05/15/12 15.00 0.00 39.84
01/22/13 15.16 0.00 39.68
11/18/13 16.19 0.00 38.65
05/27/14 14.83 0.00 40.01
01/29/15 14.83 0.00 40.01
06/02/08 16.13 0.00 NM
12/18/08 NM NM NM
05/15/12 15.80 0.00 NM
11/18/13 16.88 0.00 NM
05/27/14 NM NM NM Not Sampled
01/29/15 15.58 0.00 NM
06/02/08 1.69 0.00 NM
12/18/08 NM NM NM
10/12/11 NM NM NM
05/15/12 0.68 0.00 54.09
11/18/13 1.50 0.00 53.27
05/27/14 2.04 0.00 52.73
01/29/15 0.26 0.00 54.51
2210-22
54.08
MW-21 04/10/95 10 10-22 22
99.79
99.94
101.98
10-22
10-22 22
54.06
NM
NA NA
NA NA
54.77
MW-18 04/07/95 10 22
55.29
MW-19 04/07/95 10
MW-20 04/10/95 10
100.69
MW-22 NA NA NM
MW-23 NA NA
54.84
Page 4 of 5
Comments
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET # 21 (INCIDENT NO. 9785)
Date: 02/02/15 Facility ID # : 0-030290
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Bottom
of Well
(ft. BGS)
Ground
Water
Elevation*
(ft.)
Top of
Casing
Elevation*
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y
ft. BGS)
03/24/09 12.41 0.00 85.25
06/25/09 12.78 0.00 84.88
09/21/09 13.42 0.00 84.24
12/30/09 12.54 0.00 85.12
06/28/10 11.88 0.00 85.78
10/05/10 12.52 0.00 85.14
10/12/11 12.98 0.00 38.89
01/31/12 12.62 0.00 39.25
05/15/12 11.94 0.00 39.93
11/18/13 12.99 0.00 38.88
05/27/14 11.72 0.00 40.15
01/29/15 11.90 0.00 39.97
03/24/09 99.59 16.33 0.00 83.26
06/25/09 13.47 0.00 86.12
09/21/09 NM NM NM Not Sampled
12/30/09 11.74 0.00 87.85
06/28/10 11.10 0.00 88.49
10/05/10 10.50 0.00 89.09
10/12/11 13.03 0.00 40.71
01/31/12 11.45 0.00 42.29
11/18/13 14.23 0.00 39.51
05/27/14 12.05 0.00 41.69
01/29/15 11.21 0.00 42.53
03/24/09 18.06 0.00 82.13
06/25/09 15.00 0.00 85.19
09/21/09 15.65 0.00 84.54
12/30/09 14.96 0.00 85.23
06/28/10 13.96 0.00 86.23
10/05/10 14.68 0.00 85.51
10/12/11 15.25 0.00 39.05
01/31/12 14.89 0.00 39.41
11/18/13 15.19 39.11 39.11
05/27/14 12.53 0.00 41.77
01/29/15 12.60 0.00 41.70
03/24/09 14.55 0.00 85.67
06/25/09 15.20 0.00 85.02
09/21/09 NM NM NM Not Sampled
12/30/09 15.14 0.00 85.08
06/28/10 14.30 0.00 85.92
10/05/10 15.00 0.00 85.22
10/12/11 54.34 NM NM NM Destroyed
03/24/09 13.10 0.00 85.77
06/25/09 13.92 0.00 84.95
09/21/09 14.62 0.00 84.25
12/30/09 13.84 0.00 85.03
06/28/10 13.04 0.00 85.83
10/05/10 13.72 0.00 85.15
10/12/11 14.16 0.00 38.86
01/31/12 13.84 0.00 39.18
05/15/12 13.12 0.00 39.90
11/18/13 14.17 0.00 38.85
05/27/14 12.88 0.00 40.14
01/29/15 13.04 0.00 39.98
Notes:
•  *: Reference point for elevation measurements; assumed elevation 100.00 feet.
•  **: If free product is present in a well, ground water elevation should be calculated by: (Top of Casing Elevation - Depth to Water) +
   (Free Product Thickness x 0.8581)
•  ft BGS : feet below ground surface.
•  NA: Not Available.
•  NM:  Not Measured.
•  Well construction details for monitoring wells installed prior to March 2009 are reproduced from well identification tags, where available.
MW-27
MW-28 03/24/09 10 10-20 20
03/24/09 10 20
MW-30 03/24/09
97.66
10-20
MW-29 03/24/09 10 10-20 20 100.22
MW-25 03/24/09 10 10-20 20
51.87
53.74
10 10-20 20
53.02
98.87
100.19
54.30
Page 5 of 5
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 70 6 0.4 70 70 400 400
5,000 260,000 84,500 85,500 20,000 70,000 6,000 400 25,000 30,000 28,500 25,000
01/18/07 46.4 5.51 58.8 28.72 25.7 2.54 34.3 NR NR NR NR NR
06/06/07 68.3 4.56 85.7 32.6 21.6 <0.500 43.9 <0.500 9.60 15.9 36.9 6.60
06/02/08 16.5 1.20 21.2 8.35 38.5 0.320 I 9.23 <1.0 2.98 2.98 6.97 1.54
12/18/08 13 <0.50 10 4.9 14 <1.0 5.9 B <0.75 2.1 J 2.4 J 6.2 1.7 J
03/24/09 44 15 40 23 16 <1.6 19 <1.6 6.8 7.4 4.2 J 2.9 J
06/25/09 6.32 <0.330 7.99 <1.33 10.5 <1.67 3.14 <.0330 1.10 J 1.31 0.840 J <0.330
09/21/09 18.5 <0.190 9.24 1.30 12.7 <0.200 3.10 <0.220 1.17 1.74 0.701 J <0.180
12/30/09 26.1 2.13 5.26 3.14 15.1 <0.200 3.51 <0.220 2.04 1.79 1.87 <0.180
06/28/10 20.1 0.618 J 12.2 2.51 11.4 <0.400 7.66 <0.440 2.38 1.23 J 1.71J 0.464 J
10/05/10 32.6 2.78 16.0 8.47 8.91 <0.200 5.69 <0.220 3.87 3.78 5.51 0.85
10/12/11 <0.13 <0.13 <0.15 <0.30 2.1 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 1.2 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
05/15/12 <0.13 <0.13 <0.15 <0.30 0.16 J <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/22/13 <0.10 <0.10 <0.10 <0.22 1.0 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
11/18/13 <0.10 <0.10 <0.10 <0.22 1.1 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 1.0 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
01/29/15 <0.17 <0.17 <0.15 <0.43 0.80 <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
01/18/07 FP FP FP FP FP FP FP FP FP FP FP FP
06/06/07 FP FP FP FP FP FP FP FP FP FP FP FP
06/02/08 FP FP FP FP FP FP FP FP FP FP FP FP
12/18/08 FP FP FP FP FP FP FP FP FP FP FP FP
03/24/09 FP FP FP FP FP FP FP FP FP FP FP FP
06/25/09 FP FP FP FP FP FP FP FP FP FP FP FP
09/21/09 FP FP FP FP FP FP FP FP FP FP FP FP
12/30/09 FP FP FP FP FP FP FP FP FP FP FP FP
06/28/10 FP FP FP FP FP FP FP FP FP FP FP FP
10/05/10 FP FP FP FP FP FP FP FP FP FP FP FP
10/12/11 9,780 9,700 2,440 10,100 1,220 46.3 J 769 120 146 373 2,390 634
01/31/12 FP FP FP FP FP FP FP FP FP FP FP FP
05/15/12 FP FP FP FP FP FP FP FP FP FP FP FP
01/22/13 3,250 7,990 2,070 11,900 519 14.8 J 2,020 50.7 200 703 4,350 1,440
11/18/13 6,580 7,930 2,100 13,800 731 28.8 J 841 97.9 J 122 397 3,740 878
05/27/14 4,160 4,880 1,400 10,500 657 22.3 J 758 73.2 105 263 3,220 879
01/29/15 4,350 3,670 1,360 7,130 739 29.9 J 555 79.6 99.5 285 2,010 597
01/18/07 1,940 5.14 34.3 <15.0 3,800 17.0 <25.0 NR NR NR NR NR
06/06/07 3,030 6.18 69.0 7.61 4,880 16.9 40.3 <0.500 13.7 18.0 3.22 2.92
06/02/08 2,500 4.95 126 14.2 5,490 18.3 60.8 9.44 12.8 18.5 6.14 <1.0
12/18/08 1,700 2.1 J 33 2.6 J 4,200 E <1.0 24 B 8.4 9.1 10 1.1 J 1.3 J
03/24/09 2,900 <16 110 140 J 4,900 20 J 69 J <16 20 J 24 J 26 J <16
06/25/09 2,140 10.3 J 56.4 32.9 J 4,110 <33.4 40 J <6.60 <20 11.2 J 19.4 J <6.60
09/21/09 2,180 <7.60 56.2 <8.80 5,040 18.6 J 69.3 <8.80 13.8 J 22.1 J <6.00 <7.20
12/30/09 1,580 2.29 J 41.1 <1.10 4,200 14.5 23.3 6.35 7.99 7.71 <0.750 <0.900
06/28/10 1,780 <9.50 54.0 <11.0 5,040 <10.0 26.2J <11.0 <7.50 <11.0 <7.50 <9.00
10/05/10 1,830 <9.50 47.8 J <11.0 4,010 18.2 J <25.0 <11.0 11.8 J 14.5 J <7.50 <9.00
10/12/11 3.4 6.1 1.7 6.2 0.36 J <0.11 0.46 J <0.16 0.17 J 0.47 J 1.8 0.67
01/31/12 36.6 2.9 17.9 28.4 6.2 <0.11 0.21 J <0.16 1.8 3.5 12.9 3.8
05/15/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/22/13 22.1 2.1 19.1 16.2 8.1 <0.10 0.68 <0.10 1.8 4.1 7.6 3.6
11/18/13 12.6 1.4 17.1 14.0 5.9 <0.10 1.2 <0.10 1.9 4.4 11.9 4.6
05/27/14 4.2 <0.10 0.85 0.74 J 5.9 <0.10 0.27 J <0.10 0.44 J 0.56 0.58 <0.10
01/29/15 3.8 0.28 J 4.7 0.68 J 6.5 <0.16 0.18 J <0.16 0.78 1.5 0.29 J 0.15 J
01/18/07 14,900 5,650 1,330 4,850 16,100 288 436 NR NR NR NR NR
06/14/07 15,000 8,240 1,710 6,330 14,300 57.0 489 512 66.6 188 1,460 362
06/02/08 NS NS NS NS NS NS NS NS NS NS NS NS
10/12/11 FP FP FP FP FP FP FP FP FP FP FP FP
01/31/12 FP FP FP FP FP FP FP FP FP FP FP FP
05/15/12 FP FP FP FP FP FP FP FP FP FP FP FP
01/22/13 FP FP FP FP FP FP FP FP FP FP FP FP
11/18/13 FP FP FP FP FP FP FP FP FP FP FP FP
05/27/14 792 3,720 1,160 5,660 604 <10 550 22.8 J 95.0 356 2,160 605
01/29/15 170 1,930 1,170 6,160 238 <16 496 <16 125 592 3,230 1,140
01/18/07 1,040 76.6 116 109.4 836 <5.00 348 NR NR NR NR NR
06/06/07 1,350 90.1 143 119 1,300 9.78 105 31.1 20.6 41.9 29.0 8.31
06/02/08 NS NS NS NS NS NS NS NS NS NS NS NS
03/24/09 NS NS NS NS NS NS NS NS NS NS NS NS
06/25/09 NS NS NS NS NS NS NS NS NS NS NS NS
09/21/09 403 2.25 J 40.9 37.3 195 3.44 J 61.5 4.47 J 18.1 45.9 19.5 16.4
12/30/09 676 7.35 35.7 12.3 255 3.76 J 43.4 4.58 J 11.6 19.6 4.45 J 3.94 J
06/28/10 817 12.6 J 66.7 55.9 347 <10.0 54.1 <11.0 9.82 J 16.8 J 10.9 J <9.00
10/05/10 308 <19.0 41.1 J 23.0 J 193 <20.0 108 <22.0 24.2 J 46.9 J 29.2 J <18.0BenzeneMW-3
MW-5
2L Standard (mg/l)IsopropylbenzeneNaphthaleneToluene1,2,4-Trimethylbenzene1,2-DichloroethaneIPEMW-2
MW-1R
MW-1
MW-4
TABLE 2
SUMMARY OF GROUND WATER SAMPLING RESULTS
RED APPLE MARKET # 21 (INCIDENT NO. 9785)n-Propylbenzene1,3,5-TrimethylbenzeneDate : 02/09/15
Analytical Method EthylbenzeneContaminant of Concern

EPA Method 6210D or EPA Method 6200B
MW-2R
MW-3R
MW-4R
Facility ID # : 0-030290
GCL (mg/l)XylenesMTBEPage 1 of 6
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 70 6 0.4 70 70 400 400
5,000 260,000 84,500 85,500 20,000 70,000 6,000 400 25,000 30,000 28,500 25,000Benzene2L Standard (mg/l)IsopropylbenzeneNaphthaleneToluene1,2,4-Trimethylbenzene1,2-DichloroethaneIPETABLE 2
SUMMARY OF GROUND WATER SAMPLING RESULTS
RED APPLE MARKET # 21 (INCIDENT NO. 9785)n-Propylbenzene1,3,5-TrimethylbenzeneDate : 02/09/15
Analytical Method EthylbenzeneContaminant of Concern

EPA Method 6210D or EPA Method 6200B
Facility ID # : 0-030290
GCL (mg/l)XylenesMTBE10/12/11 FP FP FP FP FP FP FP FP FP FP FP FP
01/31/12 40.6 2.7 61.4 25.6 156 1.6 42.6 5.2 12.6 31.4 55.6 23.3
05/15/12 871 18.2 134 214.8 93.4 1.7 87.5 2.7 21.4 19.8 111 9.2
01/22/13 143 14.6 114 225 184 1.8 J 128 3.6 22.4 76.2 506 101
11/18/13 34.4 0.45 J 22.7 1.8 99.2 1.2 47.3 1.9 5.7 6.1 13.1 3.1
05/27/14 145 7.8 114 39.9 247 1.9 J 60.7 5.7 15.3 21.5 87.7 11.9
01/29/15 65.8 2.4 28.2 1.5 117 1.1 20.1 2.5 4.8 8.2 7.9 0.26 J
01/18/07 NS NS NS NS NS NS NS NS NS NS NS NS
06/06/07 NS NS NS NS NS NS NS NS NS NS NS NS
01/18/07 <1.00 <1.00 <1.00 <3.00 <1.00 <1.00 <1.00 NR NR NR NR NR
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 <0.500 <0.500 <0.500 0.550 <0.500
06/02/08 <1.0 <1.0 <1.0 <3.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
12/18/08 14 <0.50 <0.65 <1.1 13 <1.0 2.1 JB <0.50 <0.75 <0.55 <0.50 <0.65
03/24/09 3.0 J <1.6 <3.0 <5.0 3.6 J <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/30/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/28/10 <0.280 <0.380 <0.300 <0.440 <0.500 <0.400 <1.00 <0.440 <0.300 <0.440 <0.300 <0.360
10/05/10 NS NS NS NS NS NS NS NS NS NS NS NS
01/18/07 <1.00 <1.00 <1.00 <3.00 <1.00 <1.00 <1.00 NR NR NR NR NR
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
06/02/08 NS NS NS NS NS NS NS NS NS NS NS NS
12/18/08 2.3 J <0.50 <0.65 <1.1 <0.50 <1.0 1.2 JB <0.50 <0.75 <0.55 <0.50 <0.65
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/30/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 0.543 J <0.180
06/28/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/05/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 2.30 <0.220 <0.150 <0.220 0.168 J <0.180
10/12/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
05/15/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/18/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
01/29/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
01/18/07 53.6 1.48 27.4 56.3 3.67 3.97 18.3 NR NR NR NR NR
06/06/07 56.8 0.960 24.2 53.8 0.690 0.520 14.3 1.42 3.14 6.14 30.1 2.87
06/02/08 33.6 0.640 I 21.7 9.07 2.18 0.800 I 20.5 1.68 4.48 4.51 12.3 0.290 I
12/18/08 40 1.6 J 27 18 <0.50 <1.0 22 B <0.50 6.2 9.7 B 25 3.1 J
03/24/09 68 <1.6 37 23 2.0 J <1.6 28 2.3 J 6.8 13 28 2.1 J
06/25/09 53.4 0.929 J 15.9 20.7 1.04 <1.67 19.5 1.54 4.62 4.64 18.4 1.28
09/21/09 50.7 0.952 J 25.7 18.5 1.85 1.10 23.2 2.42 7.29 9.19 18.4 1.46
12/30/09 71.9 0.903 J 28.4 16.8 <0.250 0.758 J 21.9 1.71 6.49 10.7 20.9 2.06
06/28/10 66.1 <0.950 22.5 15.2 <1.25 <1.00 19.0 <1.10 4.25 J 5.94 9.47 1.11 J
10/05/10 72.6 3.54 74.2 110 <0.250 1.35 33.7 2.95 10.6 22.7 79.8 14.3
10/12/11 37.3 0.41 J 8.2 12.2 0.92 0.76 17.3 2.1 4.5 4.6 8.3 1.0
01/31/12 54.7 0.78 25.0 21.6 1.5 0.98 24.1 2.4 7.1 13.9 21.7 2.6
05/15/12 65.9 0.58 J 15.7 15.0 1.3 0.86 J 15.9 2.4 4.5 7.7 11.6 0.89 J
01/22/13 73.7 2.3 13.9 74.7 0.43 J 0.42 J 13.6 1.2 1.2 2.1 31.8 6.8
11/18/13 183 3.9 53.5 153 0.91 1.2 40.4 4.0 12.0 26.1 96.0 11.9
05/27/14 227 3.7 60.4 158 1.5 1.7 44.1 6.6 12.9 27.9 108 12.2
01/29/15 162 1.7 36.1 71.5 1.3 1.3 32.6 3.8 8.3 18.8 89.3 6.0
01/18/07 1.84 <1.00 <1.00 <3.00 36.6 1.18 <5.00 NR NR NR NR NR
06/06/07 2.05 <0.500 <0.500 <1.00 28.0 0.630 <5.00 2.50 <0.500 <0.500 <0.500 <0.500
06/02/08 45.2 <1.0 <1.0 1.40 I 42.8 2.15 I 1.98 9.21 0.540 I <1.0 0.380 I <1.0
12/18/08 1.7 J <0.50 <0.65 <1.1 35 <1.0 2.6 JB 12 <0.75 <0.55 0.96 J <0.65
03/24/09 1.4 J <1.6 <3.0 <5.0 49 2.5 J <5.0 12 <1.6 <1.6 <1.6 <1.6
06/25/09 6.42 <0.330 <0.670 <1.33 83.8 3.29 J <1.00 20.7 <1.00 <0.330 <0.330 <0.330
09/21/09 2.03 <0.190 <0.150 <0.220 100 4.02 <0.500 23.4 <0.150 <0.220 <0.150 <0.180
12/30/09 1.13 <0.190 <0.150 <0.220 69.4 2.66 1.41 13.6 <0.150 <0.220 <0.150 <0.180
06/28/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/05/10 0.774 J <0.190 <0.150 <0.220 98.8 5.00 12.3 24.0 <0.150 <0.220 0.506 J <0.180
10/12/11 <0.13 <0.13 <0.15 <0.30 61.8 3.6 0.32 J 18.2 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 1.4 <0.15 <0.30 60.3 3.1 0.14 J 14.4 <0.10 <0.11 <0.10 <0.10
05/15/12 NS NS NS NS NS NS NS NS NS NS NS NS
01/22/13 3.6 <0.20 <0.20 0.38 J 81.8 2.5 0.52 J 9.8 <0.20 <0.20 0.33 J <0.20
11/18/13 0.20 J <0.10 <0.10 <0.22 76.1 3.5 0.61 16.5 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 37.3 1.8 <0.10 7.2 <0.10 <0.10 <0.10 <0.10
01/29/15 0.43 J <0.17 <0.15 <0.43 73.9 3.2 0.74 15.9 <0.12 <0.16 <0.14 <0.14
MW-8
MW-6
MWD-7
MW-5R
MW-9
MW-10
Page 2 of 6
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 70 6 0.4 70 70 400 400
5,000 260,000 84,500 85,500 20,000 70,000 6,000 400 25,000 30,000 28,500 25,000Benzene2L Standard (mg/l)IsopropylbenzeneNaphthaleneToluene1,2,4-Trimethylbenzene1,2-DichloroethaneIPETABLE 2
SUMMARY OF GROUND WATER SAMPLING RESULTS
RED APPLE MARKET # 21 (INCIDENT NO. 9785)n-Propylbenzene1,3,5-TrimethylbenzeneDate : 02/09/15
Analytical Method EthylbenzeneContaminant of Concern

EPA Method 6210D or EPA Method 6200B
Facility ID # : 0-030290
GCL (mg/l)XylenesMTBE01/18/07 NS NS NS NS NS NS NS NS NS NS NS NS
06/06/07 NS NS NS NS NS NS NS NS NS NS NS NS
01/18/07 NS NS NS NS NS NS NS NS NS NS NS NS
06/06/07 NS NS NS NS NS NS NS NS NS NS NS NS
01/18/07 <1.00 <1.00 <1.00 <3.00 <1.00 <1.00 <5.00 NS NR NR NR NR
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
06/02/08 NS NS NS NS NS NS NS NS NS NS NS NS
01/18/07 <1.00 <1.00 <1.00 <3.00 <1.00 <1.00 <5.00 NR NR NR NR NR
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
06/02/08 <1.0 <1.0 <1.0 <3.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
12/18/08 <0.55 <0.50 <0.65 <1.1 <0.50 <1.0 0.86 JB <0.50 <0.75 <0.55 <0.50 <0.65
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/30/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/28/10 1.09 <0.190 <0.150 <0.220 99.8 2.95 <0.500 25.6 <0.150 <0.220 <0.150 <0.180
10/05/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 0.853 J <0.220 <0.150 <0.220 <0.150 <0.180
10/12/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/22/13 <0.10 0.37 J 0.26 J 1.5 J <0.10 <0.10 1.4 <0.10 <0.10 0.14 J 1.0 0.36 J
11/18/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
01/29/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
01/18/07 <1.00 <1.00 <1.00 <3.00 <1.00 <1.00 <5.00 NR NR NR NR NR
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
06/02/08 <1.0 <1.0 <1.0 <3.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
12/18/08 NS NS NS NS NS NS NS NS NS NS NS NS
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/30/09 NS NS NS NS NS NS NS NS NS NS NS NS
06/28/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/05/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/12/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/18/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
01/29/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
01/18/07 NS NS NS NS NS NS NS NS NS NS NS NS
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
06/02/08 NS NS NS NS NS NS NS NS NS NS NS NS
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 NS NS NS NS NS NS NS NS NS NS NS NS
12/30/09 NS NS NS NS NS NS NS NS NS NS NS NS
06/28/10 NS NS NS NS NS NS NS NS NS NS NS NS
10/05/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/12/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/18/13 NS NS NS NS NS NS NS NS NS NS NS NS
05/27/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
01/29/15 NS NS NS NS NS NS NS NS NS NS NS NS
01/18/07 NS NS NS NS NS NS NS NS NS NS NS NS
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
06/02/08 NS NS NS NS NS NS NS NS NS NS NS NS
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 NS NS NS NS NS NS NS NS NS NS NS NS
12/30/09 NS NS NS NS NS NS NS NS NS NS NS NS
06/28/10 NS NS NS NS NS NS NS NS NS NS NS NS
10/05/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/12/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/18/13 NS NS NS NS NS NS NS NS NS NS NS NS
05/27/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
01/29/15 NS NS NS NS NS NS NS NS NS NS NS NS
MW-14
MW-15
MW-16
MW-17
MW-13
MW-11
MW-12
Page 3 of 6
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 70 6 0.4 70 70 400 400
5,000 260,000 84,500 85,500 20,000 70,000 6,000 400 25,000 30,000 28,500 25,000Benzene2L Standard (mg/l)IsopropylbenzeneNaphthaleneToluene1,2,4-Trimethylbenzene1,2-DichloroethaneIPETABLE 2
SUMMARY OF GROUND WATER SAMPLING RESULTS
RED APPLE MARKET # 21 (INCIDENT NO. 9785)n-Propylbenzene1,3,5-TrimethylbenzeneDate : 02/09/15
Analytical Method EthylbenzeneContaminant of Concern

EPA Method 6210D or EPA Method 6200B
Facility ID # : 0-030290
GCL (mg/l)XylenesMTBE01/18/07 <1.00 <1.00 <1.00 <3.00 <1.00 <1.00 <5.00 NR NR NR NR NR
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
06/02/08 <1.0 <1.0 <1.0 <3.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
12/18/08 <0.55 <0.50 <0.65 <1.1 <0.50 <1.0 0.59 JB <0.50 <0.75 <0.55 <0.50 <0.65
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/30/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/28/10 <0.140 0.244 J <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/05/10 NS NS NS NS NS NS NS NS NS NS NS NS
10/12/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
05/15/12 NS NS NS NS NS NS NS NS NS NS NS NS
11/18/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
01/29/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
01/18/07 <1.00 <1.00 <1.00 <3.00 <1.00 <1.00 <5.00 NR NR NR NR NR
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
06/02/08 <1.0 <1.0 <1.0 <3.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
12/18/08 <0.55 <0.50 <0.65 <1.1 <0.50 <1.0 <0.50 <0.50 <0.75 <0.55 <0.50 <0.65
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/30/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/28/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/05/10 NS NS NS NS NS NS NS NS NS NS NS NS
10/12/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
05/15/12 NS NS NS NS NS NS NS NS NS NS NS NS
11/18/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
01/29/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
01/18/07 <1.00 <1.00 <1.00 <3.00 <1.00 <1.00 <5.00 NR NR NR NR NR
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
06/02/08 <1.0 <1.0 <1.0 <3.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
12/18/08 <0.55 <0.50 <0.65 <1.1 <0.50 <1.0 <0.50 <0.50 <0.75 <0.55 <0.50 <0.65
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/30/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/28/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/05/10 NS NS NS NS NS NS NS NS NS NS NS NS
10/12/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
05/15/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/18/13 <0.10 <0.10 <0.10 <0.22 0.32 J <0.10 <0.15 0.12 J <0.10 <0.10 <0.10 <0.10
05/27/14 NS NS NS NS NS NS NS NS NS NS NS NS
01/29/15 <0.17 <0.17 <0.15 <0.43 0.34 J <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
01/18/07 <1.00 <1.00 <1.00 <3.00 4.28 <1.00 <5.00 NR NR NR NR NR
06/06/07 <0.500 <0.500 <0.500 <1.00 4.50 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
06/02/08 <1.0 <1.0 <1.0 <3.0 5.26 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
12/18/08 <0.55 <0.50 <0.65 <1.1 4.7 J <1.0 <0.50 <0.50 <0.75 <0.55 <0.50 <0.65
03/24/09 <1.0 <1.6 <3.0 <5.0 4.2 J <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 3.10 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 3.02 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/30/09 <0.140 <0.190 <0.150 <0.220 2.33 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/28/10 <0.140 <0.190 <0.150 <0.220 1.21 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/05/10 <0.140 <0.190 <0.150 <0.220 2.34 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/12/11 <0.13 <0.13 <0.15 <0.30 0.97 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 0.77 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
05/15/12 <0.13 <0.13 <0.15 <0.30 1.1 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/22/13 <0.10 <0.10 <0.10 <0.22 0.24 J <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
11/18/13 <0.10 <0.10 <0.10 <0.22 0.52 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 0.21 J <0.10 <0.10 <0.10 <0.10 <0.10 0.11 J <0.10
01/29/15 <0.17 <0.17 <0.15 <0.43 0.22 J <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
MW-19
MW-18
MW-21
MW-20
Page 4 of 6
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 70 6 0.4 70 70 400 400
5,000 260,000 84,500 85,500 20,000 70,000 6,000 400 25,000 30,000 28,500 25,000Benzene2L Standard (mg/l)IsopropylbenzeneNaphthaleneToluene1,2,4-Trimethylbenzene1,2-DichloroethaneIPETABLE 2
SUMMARY OF GROUND WATER SAMPLING RESULTS
RED APPLE MARKET # 21 (INCIDENT NO. 9785)n-Propylbenzene1,3,5-TrimethylbenzeneDate : 02/09/15
Analytical Method EthylbenzeneContaminant of Concern

EPA Method 6210D or EPA Method 6200B
Facility ID # : 0-030290
GCL (mg/l)XylenesMTBE06/02/08 4.11 <1.0 <1.0 <3.0 52.4 1.78 I <1.0 2.61 <1.0 <1.0 <1.0 <1.0
12/18/08 NS NS NS NS NS NS NS NS NS NS NS NS
05/15/12 <0.13 <0.13 <0.15 <0.30 1.3 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/18/13 2.8 <0.10 0.16 J <0.22 3.1 0.12 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 NS NS NS NS NS NS NS NS NS NS NS NS
01/29/15 <0.17 <0.17 <0.15 <0.43 0.75 <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
06/02/08 81.0 15.6 46.7 162 <1.0 <5.0 38.4 13.5 5.67 10.1 121 57.6
12/18/08 NS NS NS NS NS NS NS NS NS NS NS NS
10/12/11 NS NS NS NS NS NS NS NS NS NS NS NS
05/15/12 104 14.2 60.7 19.5 <0.13 <0.11 19.3 12.5 6.3 11.3 49.0 17.9
11/18/13 63.5 4.7 20.0 13.4 <0.10 <0.10 9.8 11.1 3.5 4.1 12.1 4.2
05/27/14 107 4.3 38.7 45.8 <0.10 <0.10 27.4 16.4 8.2 12.0 41.1 6.5
01/29/15 65.2 0.93 6.4 3.9 <0.16 <0.16 10.3 11.3 3.0 3.8 4.4 0.64
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/30/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/28/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/05/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/12/11 <0.13 <0.13 <0.15 <0.30 0.19 J <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 0.18 J <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
05/15/12 <0.13 <0.13 <0.15 <0.30 0.19 J <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/18/13 <0.10 <0.10 <0.10 <0.22 0.30 J <0.10 <0.15 <0.10 <0.10 <0.10 0.14 J <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 0.56 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
01/29/15 <0.17 <0.17 <0.15 <0.43 0.35 J <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 NS NS NS NS NS NS NS NS NS NS NS NS
12/30/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/28/10 <0.140 <0.190 <0.150 0.355 J <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 0.159 J <0.180
10/05/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 0.236 J <0.180
10/12/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/18/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
01/29/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/30/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/28/10 <0.140 0.329 J <0.150 0.515 J <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/05/10 <0.140 0.516 J 0.199 J 1.03 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 0.465 J <0.180
10/12/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 0.16 J <0.15 <0.30 1.0 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/18/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
01/29/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 NS NS NS NS NS NS NS NS NS NS NS NS
12/30/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/28/10 0.572 J 6.18 2.38 15.6 <0.250 <0.200 2.46 J <0.220 0.306 J 0.896 J 8.36 2.02
10/05/10 <0.140 1.00 0.464 J 2.84 <0.250 <0.200 0.841 J <0.220 <0.150 0.248 J 1.81 0.506 J
10/12/11 NS NS NS NS NS NS NS NS NS NS NS NS
03/24/09 <1.0 <1.6 <3.0 <5.0 1.8 J <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 1.15 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 1.23 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/30/09 <0.140 <0.190 <0.150 <0.220 1.14 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/28/10 0.203 J 1.95 0.881 J 5.17 1.44 <0.200 0.674 J <0.220 0.150 J 0.418 J 1.67 0.779 J
10/05/10 <0.140 <0.190 <0.150 <0.220 1.28 <0.200 <0.500 <0.220 <0.150 <0.220 0.169 J <0.180
10/12/11 <0.13 <0.13 <0.15 <0.30 1.2 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
05/15/12 <0.13 <0.13 <0.15 <0.30 0.87 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/18/13 <0.10 <0.10 <0.10 <0.22 0.33 J <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 0.25 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
01/29/15 <0.17 <0.17 <0.15 <0.43 0.27 J <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
MW-29
MW-22
MW-28
MW-25
MW-30
MW-23
MW-27
Page 5 of 6
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 70 6 0.4 70 70 400 400
5,000 260,000 84,500 85,500 20,000 70,000 6,000 400 25,000 30,000 28,500 25,000Benzene2L Standard (mg/l)IsopropylbenzeneNaphthaleneToluene1,2,4-Trimethylbenzene1,2-DichloroethaneIPETABLE 2
SUMMARY OF GROUND WATER SAMPLING RESULTS
RED APPLE MARKET # 21 (INCIDENT NO. 9785)n-Propylbenzene1,3,5-TrimethylbenzeneDate : 02/09/15
Analytical Method EthylbenzeneContaminant of Concern

EPA Method 6210D or EPA Method 6200B
Facility ID # : 0-030290
GCL (mg/l)XylenesMTBEWSW-1 06/02/08 NS NS NS NS NS NS NS NS NS NS NS NS
06/02/08 NS NS NS NS NS NS NS NS NS NS NS NS
03/24/09 NS NS NS NS NS NS NS NS NS NS NS NS
12/30/09 NS NS NS NS NS NS NS NS NS NS NS NS
01/18/07 NS NS NS NS NS NS NS NS NS NS NS NS
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
06/02/08 <1.0 <1.0 <1.0 <3.0 <1.0 <5.0 0.930 I <1.0 <1.0 <1.0 0.330 I <1.0
03/24/09 NS NS NS NS NS NS NS NS NS NS NS NS
12/30/09 NS NS NS NS NS NS NS NS NS NS NS NS
01/18/07 NS NS NS NS NS NS NS NS NS NS NS NS
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
06/02/08 NS NS NS NS NS NS NS NS NS NS NS NS
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/30/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/28/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/05/10 NS NS NS NS NS NS NS NS NS NS NS NS
10/12/11 <0.13 <0.13 <0.15 0.53 J <0.13 <0.11 0.23 J <0.16 <0.10 <0.11 0.33 J <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 0.11 J <0.10
05/15/12 NS NS NS NS NS NS NS NS NS NS NS NS
01/22/13 NS NS NS NS NS NS NS NS NS NS NS NS
11/18/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 0.30 J 0.19 J
01/29/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
01/18/07 NS NS NS NS NS NS NS NS NS NS NS NS
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 2.14 <0.500 <0.500 0.520 <0.500
06/02/08 <1.0 <1.0 <1.0 <3.0 <1.0 <5.0 <1.0 1.75 <1.0 <1.0 <1.0 <1.0
12/18/08 <0.55 <0.50 <0.65 <1.1 <0.50 <1.0 <0.50 29 <0.75 <0.55 <0.50 <0.65
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 26 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 34.3 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 34.4 <0.150 <0.220 <0.150 <0.180
12/30/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 16.1 <0.150 <0.220 <0.150 <0.180
06/28/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 45.0 <0.150 <0.220 <0.150 <0.180
10/05/10 NS NS NS NS NS NS NS NS NS NS NS NS
10/12/11 NS NS NS NS NS NS NS NS NS NS NS NS
01/31/12 NS NS NS NS NS NS NS NS NS NS NS NS
05/15/12 NS NS NS NS NS NS NS NS NS NS NS NS
01/22/13 NS NS NS NS NS NS NS NS NS NS NS NS
05/27/14 NS NS NS NS NS NS NS NS NS NS NS NS
06/02/08 NS NS NS NS NS NS NS NS NS NS NS NS
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
06/28/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/05/10 NS NS NS NS NS NS NS NS NS NS NS NS
10/12/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10
05/15/12 NS NS NS NS NS NS NS NS NS NS NS NS
01/22/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
11/18/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
01/29/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
Notes:
• Results reported in µg/l (micrograms per liter).
• NE: Standard not established.
• Concentrations in bold face type exceeded the 2L standards.
• NR: Not requested.
• < : Less than the method detection limit specified in the laboratory report
• I or J: Estimated value.
• V or B: Present in laboratory blank.
• NS: Not sampled.
• E: Estimated value; above laboratory calibration curve.
• A concentration of bromodichloromethane (0.95 µg/l in WSW-6) that exceeded the MACs were reported in the ground water sample collected on
January 29, 2015.
• For other compounds reported which did not exceed the 2L Standards, refer to the laboratory reports.
• GCL : Gross contamination level.
• 2L Standard: as specified in T15A NCAC 2L.0202.
WSW-2
WSW-3
WSW-4
WSW-5
WSW-6
Page 6 of 6

APPENDICES

APPENDIX A
Laboratory Report – Ground Water Samples

02/06/15
Technical Report for
GRI (Geological Resources Inc.)
Ram 21, 1121 NC561 W, Saint John, NC
9785/2486
Accutest Job Number: FA21787
Sampling Date: 01/29/15
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
[e-mail]; [e-mail];
[e-mail]; [e-mail]
ATTN: William Regenthall
Total number of pages in report:
Certifications: FL (E83510), LA (03051), KS (E-10327), IA (366), IL (200063), NC (573), NJ (FL002), SC (96038001)
DoD ELAP (L-A-B L2229), CA (2937), TX (T104704404), PA (68-03573), VA (460177),
AK, AR, GA, KY, MA, NV, OK, UT, WA
This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone] • http://www.accutest.com
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Norm Farmer
Technical Director
Southeast
02/06/15
e-Hardcopy 2.0
Automated Report
84
Accutest Laboratories is the sole authority for authorizing edits or modifications to this
document. Unauthorized modification of this report is strictly prohibited.
1 of 84
FA21787
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................5
Section 3: Sample Results ........................................................................................................10
3.1: FA21787-1: MW-1R .....................................................................................................11
3.2: FA21787-2: MW-2R .....................................................................................................13
3.3: FA21787-3: MW-3R .....................................................................................................15
3.4: FA21787-4: MW-4R .....................................................................................................17
3.5: FA21787-5: MW-5R .....................................................................................................19
3.6: FA21787-6: MW-8 ........................................................................................................21
3.7: FA21787-7: MW-9 ........................................................................................................23
3.8: FA21787-8: MW-10 ......................................................................................................25
3.9: FA21787-9: MW-14 ......................................................................................................27
3.10: FA21787-10: MW-15 ..................................................................................................29
3.11: FA21787-11: MW-18 ..................................................................................................31
3.12: FA21787-12: MW-19 ..................................................................................................33
3.13: FA21787-13: MW-20 ..................................................................................................35
3.14: FA21787-14: MW-21 ..................................................................................................37
3.15: FA21787-15: MW-22 ..................................................................................................39
3.16: FA21787-16: MW-23 ..................................................................................................41
3.17: FA21787-17: MW-25 ..................................................................................................43
3.18: FA21787-18: MW-27 ..................................................................................................45
3.19: FA21787-19: MW-28 ..................................................................................................47
3.20: FA21787-20: MW-30 ..................................................................................................49
3.21: FA21787-21: WSW-4 .................................................................................................51
3.22: FA21787-22: WSW-6 .................................................................................................53
Section 4: Misc. Forms ............................................................................................................55
4.1: Chain of Custody ...........................................................................................................56
Section 5: GC/MS Volatiles - QC Data Summaries ..............................................................60
5.1: Method Blank Summary ................................................................................................61
5.2: Blank Spike Summary ...................................................................................................69
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................77 123452 of 84
FA21787
Accutest Laboratories
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA21787
Ram 21, 1121 NC561 W, Saint John, NC
Project No: 9785/2486
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA21787-1 01/29/15 14:31 JH 01/30/15 AQ Ground Water MW-1R
FA21787-2 01/29/15 14:42 JH 01/30/15 AQ Ground Water MW-2R
FA21787-3 01/29/15 14:53 JH 01/30/15 AQ Ground Water MW-3R
FA21787-4 01/29/15 15:14 JH 01/30/15 AQ Ground Water MW-4R
FA21787-5 01/29/15 15:05 JH 01/30/15 AQ Ground Water MW-5R
FA21787-6 01/29/15 12:08 JH 01/30/15 AQ Ground Water MW-8
FA21787-7 01/29/15 12:59 JH 01/30/15 AQ Ground Water MW-9
FA21787-8 01/29/15 11:30 JH 01/30/15 AQ Ground Water MW-10
FA21787-9 01/29/15 12:34 JH 01/30/15 AQ Ground Water MW-14
FA21787-10 01/29/15 12:45 JH 01/30/15 AQ Ground Water MW-15
FA21787-11 01/29/15 10:58 JH 01/30/15 AQ Ground Water MW-18
FA21787-12 01/29/15 11:19 JH 01/30/15 AQ Ground Water MW-19
FA21787-13 01/29/15 13:10 JH 01/30/15 AQ Ground Water MW-20
3 of 84
FA21787 1
Accutest Laboratories
Sample Summary
(continued)
GRI (Geological Resources Inc.)
Job No:FA21787
Ram 21, 1121 NC561 W, Saint John, NC
Project No: 9785/2486
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA21787-14 01/29/15 13:21 JH 01/30/15 AQ Ground Water MW-21
FA21787-15 01/29/15 11:52 JH 01/30/15 AQ Ground Water MW-22
FA21787-16 01/29/15 12:23 JH 01/30/15 AQ Ground Water MW-23
FA21787-17 01/29/15 13:35 JH 01/30/15 AQ Ground Water MW-25
FA21787-18 01/29/15 14:07 JH 01/30/15 AQ Ground Water MW-27
FA21787-19 01/29/15 14:18 JH 01/30/15 AQ Ground Water MW-28
FA21787-20 01/29/15 13:50 JH 01/30/15 AQ Ground Water MW-30
FA21787-21 01/29/15 11:40 JH 01/30/15 AQ Water WSW-4
FA21787-22 01/29/15 11:06 JH 01/30/15 AQ Water WSW-6
4 of 84
FA21787 1
Summary of Hits Page 1 of 5
Job Number:FA21787
Account:GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Collected:01/29/15
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA21787-1 MW-1R
Methyl Tert Butyl Ether 0.80 0.50 0.16 ug/l SM 6200B
FA21787-2 MW-2R
Benzene 4350 50 17 ug/l SM 6200B
n-Butylbenzene 35.2 J 50 14 ug/l SM 6200B
sec-Butylbenzene 21.6 J 50 14 ug/l SM 6200B
1,2-Dichloroethane 79.6 50 16 ug/l SM 6200B
Di-Isopropyl Ether 29.9 J 50 16 ug/l SM 6200B
Ethylbenzene 1360 50 15 ug/l SM 6200B
Isopropylbenzene 99.5 50 12 ug/l SM 6200B
p-Isopropyltoluene 16.2 J 50 12 ug/l SM 6200B
Methyl Tert Butyl Ether 739 50 16 ug/l SM 6200B
Naphthalene 555 50 12 ug/l SM 6200B
n-Propylbenzene 285 50 16 ug/l SM 6200B
Toluene 3670 50 17 ug/l SM 6200B
1,2,4-Trimethylbenzene 2010 50 14 ug/l SM 6200B
1,3,5-Trimethylbenzene 597 50 14 ug/l SM 6200B
m,p-Xylene 4660 100 30 ug/l SM 6200B
o-Xylene 2470 50 13 ug/l SM 6200B
Xylene (total)7130 150 43 ug/l SM 6200B
FA21787-3 MW-3R
Benzene 3.8 0.50 0.17 ug/l SM 6200B
n-Butylbenzene 0.26 J 0.50 0.14 ug/l SM 6200B
sec-Butylbenzene 0.28 J 0.50 0.14 ug/l SM 6200B
Ethylbenzene 4.7 0.50 0.15 ug/l SM 6200B
Isopropylbenzene 0.78 0.50 0.12 ug/l SM 6200B
Methyl Tert Butyl Ether 6.5 0.50 0.16 ug/l SM 6200B
Naphthalene 0.18 J 0.50 0.12 ug/l SM 6200B
n-Propylbenzene 1.5 0.50 0.16 ug/l SM 6200B
Toluene 0.28 J 0.50 0.17 ug/l SM 6200B
1,2,4-Trimethylbenzene 0.29 J 0.50 0.14 ug/l SM 6200B
1,3,5-Trimethylbenzene 0.15 J 0.50 0.14 ug/l SM 6200B
m,p-Xylene 0.53 J 1.0 0.30 ug/l SM 6200B
o-Xylene 0.16 J 0.50 0.13 ug/l SM 6200B
Xylene (total)0.68 J 1.5 0.43 ug/l SM 6200B
FA21787-4 MW-4R
Benzene 170 50 17 ug/l SM 6200B
n-Butylbenzene 121 50 14 ug/l SM 6200B
5 of 84
FA21787 2
Summary of Hits Page 2 of 5
Job Number:FA21787
Account:GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Collected:01/29/15
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
sec-Butylbenzene 64.0 50 14 ug/l SM 6200B
Ethylbenzene 1170 50 15 ug/l SM 6200B
Isopropylbenzene 125 50 12 ug/l SM 6200B
p-Isopropyltoluene 28.7 J 50 12 ug/l SM 6200B
Methyl Tert Butyl Ether 238 50 16 ug/l SM 6200B
Naphthalene 496 50 12 ug/l SM 6200B
n-Propylbenzene 592 50 16 ug/l SM 6200B
Toluene 1930 50 17 ug/l SM 6200B
1,2,4-Trimethylbenzene 3230 50 14 ug/l SM 6200B
1,3,5-Trimethylbenzene 1140 50 14 ug/l SM 6200B
m,p-Xylene 4510 100 30 ug/l SM 6200B
o-Xylene 1650 50 13 ug/l SM 6200B
Xylene (total)6160 150 43 ug/l SM 6200B
FA21787-5 MW-5R
Benzene 65.8 1.3 0.43 ug/l SM 6200B
n-Butylbenzene 0.69 0.50 0.14 ug/l SM 6200B
sec-Butylbenzene 2.6 0.50 0.14 ug/l SM 6200B
tert-Butylbenzene 0.36 J 0.50 0.15 ug/l SM 6200B
1,2-Dichloroethane 2.5 0.50 0.16 ug/l SM 6200B
Di-Isopropyl Ether 1.1 0.50 0.16 ug/l SM 6200B
Ethylbenzene 28.2 0.50 0.15 ug/l SM 6200B
Isopropylbenzene 4.8 0.50 0.12 ug/l SM 6200B
p-Isopropyltoluene 1.3 0.50 0.12 ug/l SM 6200B
Methyl Tert Butyl Ether 117 1.3 0.41 ug/l SM 6200B
Naphthalene 20.1 0.50 0.12 ug/l SM 6200B
n-Propylbenzene 8.2 0.50 0.16 ug/l SM 6200B
Toluene 2.4 0.50 0.17 ug/l SM 6200B
1,2,4-Trimethylbenzene 7.9 0.50 0.14 ug/l SM 6200B
1,3,5-Trimethylbenzene 0.26 J 0.50 0.14 ug/l SM 6200B
m,p-Xylene 0.90 J 1.0 0.30 ug/l SM 6200B
o-Xylene 0.59 0.50 0.13 ug/l SM 6200B
Xylene (total)1.5 1.5 0.43 ug/l SM 6200B
FA21787-6 MW-8
No hits reported in this sample.
FA21787-7 MW-9
Benzene 162 2.5 0.86 ug/l SM 6200B
n-Butylbenzene 5.7 0.50 0.14 ug/l SM 6200B
sec-Butylbenzene 3.6 0.50 0.14 ug/l SM 6200B
1,2-Dichloroethane 3.8 0.50 0.16 ug/l SM 6200B
6 of 84
FA21787 2
Summary of Hits Page 3 of 5
Job Number:FA21787
Account:GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Collected:01/29/15
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
Di-Isopropyl Ether 1.3 0.50 0.16 ug/l SM 6200B
Ethylbenzene 36.1 0.50 0.15 ug/l SM 6200B
Isopropylbenzene 8.3 0.50 0.12 ug/l SM 6200B
p-Isopropyltoluene 1.4 0.50 0.12 ug/l SM 6200B
Methyl Tert Butyl Ether 1.3 0.50 0.16 ug/l SM 6200B
Naphthalene 32.6 0.50 0.12 ug/l SM 6200B
n-Propylbenzene 18.8 0.50 0.16 ug/l SM 6200B
Toluene 1.7 0.50 0.17 ug/l SM 6200B
1,2,4-Trimethylbenzene 89.3 2.5 0.68 ug/l SM 6200B
1,3,5-Trimethylbenzene 6.0 0.50 0.14 ug/l SM 6200B
m,p-Xylene 52.8 1.0 0.30 ug/l SM 6200B
o-Xylene 18.7 0.50 0.13 ug/l SM 6200B
Xylene (total)71.5 1.5 0.43 ug/l SM 6200B
FA21787-8 MW-10
Benzene 0.43 J 0.50 0.17 ug/l SM 6200B
1,2-Dichloroethane 15.9 0.50 0.16 ug/l SM 6200B
Di-Isopropyl Ether 3.2 0.50 0.16 ug/l SM 6200B
Methyl Tert Butyl Ether 73.9 1.0 0.33 ug/l SM 6200B
Naphthalene 0.74 0.50 0.12 ug/l SM 6200B
FA21787-9 MW-14
No hits reported in this sample.
FA21787-10 MW-15
No hits reported in this sample.
FA21787-11 MW-18
No hits reported in this sample.
FA21787-12 MW-19
No hits reported in this sample.
FA21787-13 MW-20
Methyl Tert Butyl Ether 0.34 J 0.50 0.16 ug/l SM 6200B
FA21787-14 MW-21
Methyl Tert Butyl Ether 0.22 J 0.50 0.16 ug/l SM 6200B
7 of 84
FA21787 2
Summary of Hits Page 4 of 5
Job Number:FA21787
Account:GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Collected:01/29/15
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA21787-15 MW-22
Methyl Tert Butyl Ether 0.75 0.50 0.16 ug/l SM 6200B
FA21787-16 MW-23
Benzene 65.2 1.0 0.34 ug/l SM 6200B
n-Butylbenzene 0.47 J 0.50 0.14 ug/l SM 6200B
sec-Butylbenzene 0.67 0.50 0.14 ug/l SM 6200B
Chloroethane 1.1 0.50 0.21 ug/l SM 6200B
1,2-Dichloroethane 11.3 0.50 0.16 ug/l SM 6200B
Ethylbenzene 6.4 0.50 0.15 ug/l SM 6200B
Isopropylbenzene 3.0 0.50 0.12 ug/l SM 6200B
p-Isopropyltoluene 1.4 0.50 0.12 ug/l SM 6200B
Methyl Chloride 0.57 0.50 0.16 ug/l SM 6200B
Naphthalene 10.3 0.50 0.12 ug/l SM 6200B
n-Propylbenzene 3.8 0.50 0.16 ug/l SM 6200B
Toluene 0.93 0.50 0.17 ug/l SM 6200B
1,2,4-Trimethylbenzene 4.4 0.50 0.14 ug/l SM 6200B
1,3,5-Trimethylbenzene 0.64 0.50 0.14 ug/l SM 6200B
m,p-Xylene 1.1 1.0 0.30 ug/l SM 6200B
o-Xylene 2.8 0.50 0.13 ug/l SM 6200B
Xylene (total)3.9 1.5 0.43 ug/l SM 6200B
FA21787-17 MW-25
Methyl Tert Butyl Ether 0.35 J 0.50 0.16 ug/l SM 6200B
FA21787-18 MW-27
No hits reported in this sample.
FA21787-19 MW-28
No hits reported in this sample.
FA21787-20 MW-30
Methyl Tert Butyl Ether 0.27 J 0.50 0.16 ug/l SM 6200B
FA21787-21 WSW-4
No hits reported in this sample.
8 of 84
FA21787 2
Summary of Hits Page 5 of 5
Job Number:FA21787
Account:GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Collected:01/29/15
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA21787-22 WSW-6
Bromodichloromethane 0.95 0.50 0.15 ug/l SM 6200B
Bromoform 0.61 0.50 0.11 ug/l SM 6200B
Chloroform 0.67 0.50 0.17 ug/l SM 6200B
Dibromochloromethane 1.2 0.50 0.12 ug/l SM 6200B
9 of 84
FA21787 2
Accutest Laboratories
Sample Results
Report of Analysis
Southeast
Section 3
10 of 84
FA21787 3
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-1R
Lab Sample ID:FA21787-1 Date Sampled:01/29/15
Matrix:AQ - Ground Water Date Received:01/30/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E036171.D 1 02/03/15 TD n/a n/a VE1204
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 84
FA21787 33.1
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-1R
Lab Sample ID:FA21787-1 Date Sampled:01/29/15
Matrix:AQ - Ground Water Date Received:01/30/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.80 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%70-130%
2037-26-5 Toluene-D8 96%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 84
FA21787 33.1
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-2R
Lab Sample ID:FA21787-2 Date Sampled:01/29/15
Matrix:AQ - Ground Water Date Received:01/30/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0192086.D 100 02/04/15 TD n/a n/a VA1632
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 4350 50 17 ug/l
108-86-1 Bromobenzene ND 50 16 ug/l
74-97-5 Bromochloromethane ND 50 16 ug/l
75-27-4 Bromodichloromethane ND 50 15 ug/l
75-25-2 Bromoform ND 50 11 ug/l
104-51-8 n-Butylbenzene 35.2 50 14 ug/l J
135-98-8 sec-Butylbenzene 21.6 50 14 ug/l J
98-06-6 tert-Butylbenzene ND 50 15 ug/l
56-23-5 Carbon Tetrachloride ND 50 15 ug/l
108-90-7 Chlorobenzene ND 50 16 ug/l
75-00-3 Chloroethane ND 50 21 ug/l
67-66-3 Chloroform ND 50 17 ug/l
95-49-8 o-Chlorotoluene ND 50 15 ug/l
106-43-4 p-Chlorotoluene ND 50 14 ug/l
124-48-1 Dibromochloromethane ND 50 12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 50 20 ug/l
106-93-4 1,2-Dibromoethane ND 50 14 ug/l
75-71-8 Dichlorodifluoromethane ND 50 13 ug/l
95-50-1 1,2-Dichlorobenzene ND 50 13 ug/l
541-73-1 1,3-Dichlorobenzene ND 50 14 ug/l
106-46-7 1,4-Dichlorobenzene ND 50 15 ug/l
75-34-3 1,1-Dichloroethane ND 50 18 ug/l
107-06-2 1,2-Dichloroethane 79.6 50 16 ug/l
75-35-4 1,1-Dichloroethylene ND 50 17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 50 18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 50 17 ug/l
78-87-5 1,2-Dichloropropane ND 50 17 ug/l
142-28-9 1,3-Dichloropropane ND 50 15 ug/l
594-20-7 2,2-Dichloropropane ND 50 12 ug/l
563-58-6 1,1-Dichloropropene ND 50 16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 50 13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 50 13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
13 of 84
FA21787 33.2
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-2R
Lab Sample ID:FA21787-2 Date Sampled:01/29/15
Matrix:AQ - Ground Water Date Received:01/30/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 29.9 50 16 ug/l J
100-41-4 Ethylbenzene 1360 50 15 ug/l
87-68-3 Hexachlorobutadiene ND 50 12 ug/l
98-82-8 Isopropylbenzene 99.5 50 12 ug/l
99-87-6 p-Isopropyltoluene 16.2 50 12 ug/l J
74-83-9 Methyl Bromide ND 50 18 ug/l
74-87-3 Methyl Chloride ND 50 16 ug/l
74-95-3 Methylene Bromide ND 50 17 ug/l
75-09-2 Methylene Chloride ND 200 100 ug/l
1634-04-4 Methyl Tert Butyl Ether 739 50 16 ug/l
91-20-3 Naphthalene 555 50 12 ug/l
103-65-1 n-Propylbenzene 285 50 16 ug/l
100-42-5 Styrene ND 50 12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 50 13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 50 14 ug/l
127-18-4 Tetrachloroethylene ND 50 15 ug/l
108-88-3 Toluene 3670 50 17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 50 14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 50 13 ug/l
71-55-6 1,1,1-Trichloroethane ND 50 16 ug/l
79-00-5 1,1,2-Trichloroethane ND 50 14 ug/l
79-01-6 Trichloroethylene ND 50 15 ug/l
75-69-4 Trichlorofluoromethane ND 50 16 ug/l
96-18-4 1,2,3-Trichloropropane ND 50 13 ug/l
95-63-6 1,2,4-Trimethylbenzene 2010 50 14 ug/l
108-67-8 1,3,5-Trimethylbenzene 597 50 14 ug/l
75-01-4 Vinyl Chloride ND 50 13 ug/l
m,p-Xylene 4660 100 30 ug/l
95-47-6 o-Xylene 2470 50 13 ug/l
1330-20-7 Xylene (total)7130 150 43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 105%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
14 of 84
FA21787 33.2
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-3R
Lab Sample ID:FA21787-3 Date Sampled:01/29/15
Matrix:AQ - Ground Water Date Received:01/30/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E036172.D 1 02/03/15 TD n/a n/a VE1204
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 3.8 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene 0.26 0.50 0.14 ug/l J
135-98-8 sec-Butylbenzene 0.28 0.50 0.14 ug/l J
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
15 of 84
FA21787 33.3
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-3R
Lab Sample ID:FA21787-3 Date Sampled:01/29/15
Matrix:AQ - Ground Water Date Received:01/30/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene 4.7 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene 0.78 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 6.5 0.50 0.16 ug/l
91-20-3 Naphthalene 0.18 0.50 0.12 ug/l J
103-65-1 n-Propylbenzene 1.5 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene 0.28 0.50 0.17 ug/l J
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 0.29 0.50 0.14 ug/l J
108-67-8 1,3,5-Trimethylbenzene 0.15 0.50 0.14 ug/l J
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 0.53 1.0 0.30 ug/l J
95-47-6 o-Xylene 0.16 0.50 0.13 ug/l J
1330-20-7 Xylene (total)0.68 1.5 0.43 ug/l J
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
16 of 84
FA21787 33.3
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-4R
Lab Sample ID:FA21787-4 Date Sampled:01/29/15
Matrix:AQ - Ground Water Date Received:01/30/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E036166.D 100 02/03/15 TD n/a n/a VE1204
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 170 50 17 ug/l
108-86-1 Bromobenzene ND 50 16 ug/l
74-97-5 Bromochloromethane ND 50 16 ug/l
75-27-4 Bromodichloromethane ND 50 15 ug/l
75-25-2 Bromoform ND 50 11 ug/l
104-51-8 n-Butylbenzene 121 50 14 ug/l
135-98-8 sec-Butylbenzene 64.0 50 14 ug/l
98-06-6 tert-Butylbenzene ND 50 15 ug/l
56-23-5 Carbon Tetrachloride ND 50 15 ug/l
108-90-7 Chlorobenzene ND 50 16 ug/l
75-00-3 Chloroethane ND 50 21 ug/l
67-66-3 Chloroform ND 50 17 ug/l
95-49-8 o-Chlorotoluene ND 50 15 ug/l
106-43-4 p-Chlorotoluene ND 50 14 ug/l
124-48-1 Dibromochloromethane ND 50 12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 50 20 ug/l
106-93-4 1,2-Dibromoethane ND 50 14 ug/l
75-71-8 Dichlorodifluoromethane ND 50 13 ug/l
95-50-1 1,2-Dichlorobenzene ND 50 13 ug/l
541-73-1 1,3-Dichlorobenzene ND 50 14 ug/l
106-46-7 1,4-Dichlorobenzene ND 50 15 ug/l
75-34-3 1,1-Dichloroethane ND 50 18 ug/l
107-06-2 1,2-Dichloroethane ND 50 16 ug/l
75-35-4 1,1-Dichloroethylene ND 50 17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 50 18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 50 17 ug/l
78-87-5 1,2-Dichloropropane ND 50 17 ug/l
142-28-9 1,3-Dichloropropane ND 50 15 ug/l
594-20-7 2,2-Dichloropropane ND 50 12 ug/l
563-58-6 1,1-Dichloropropene ND 50 16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 50 13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 50 13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
17 of 84
FA21787 33.4
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-4R
Lab Sample ID:FA21787-4 Date Sampled:01/29/15
Matrix:AQ - Ground Water Date Received:01/30/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 50 16 ug/l
100-41-4 Ethylbenzene 1170 50 15 ug/l
87-68-3 Hexachlorobutadiene ND 50 12 ug/l
98-82-8 Isopropylbenzene 125 50 12 ug/l
99-87-6 p-Isopropyltoluene 28.7 50 12 ug/l J
74-83-9 Methyl Bromide ND 50 18 ug/l
74-87-3 Methyl Chloride ND 50 16 ug/l
74-95-3 Methylene Bromide ND 50 17 ug/l
75-09-2 Methylene Chloride ND 200 100 ug/l
1634-04-4 Methyl Tert Butyl Ether 238 50 16 ug/l
91-20-3 Naphthalene 496 50 12 ug/l
103-65-1 n-Propylbenzene 592 50 16 ug/l
100-42-5 Styrene ND 50 12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 50 13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 50 14 ug/l
127-18-4 Tetrachloroethylene ND 50 15 ug/l
108-88-3 Toluene 1930 50 17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 50 14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 50 13 ug/l
71-55-6 1,1,1-Trichloroethane ND 50 16 ug/l
79-00-5 1,1,2-Trichloroethane ND 50 14 ug/l
79-01-6 Trichloroethylene ND 50 15 ug/l
75-69-4 Trichlorofluoromethane ND 50 16 ug/l
96-18-4 1,2,3-Trichloropropane ND 50 13 ug/l
95-63-6 1,2,4-Trimethylbenzene 3230 50 14 ug/l
108-67-8 1,3,5-Trimethylbenzene 1140 50 14 ug/l
75-01-4 Vinyl Chloride ND 50 13 ug/l
m,p-Xylene 4510 100 30 ug/l
95-47-6 o-Xylene 1650 50 13 ug/l
1330-20-7 Xylene (total)6160 150 43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 96%70-130%
17060-07-0 1,2-Dichloroethane-D4 101%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
18 of 84
FA21787 33.4
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-5R
Lab Sample ID:FA21787-5 Date Sampled:01/29/15
Matrix:AQ - Ground Water Date Received:01/30/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E036163.D 1 02/03/15 TD n/a n/a VE1204
Run #2 E036180.D 2.5 02/03/15 TD n/a n/a VE1204
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 65.8 a 1.3 0.43 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene 0.69 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene 2.6 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene 0.36 0.50 0.15 ug/l J
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane 2.5 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
19 of 84
FA21787 33.5
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-5R
Lab Sample ID:FA21787-5 Date Sampled:01/29/15
Matrix:AQ - Ground Water Date Received:01/30/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 1.1 0.50 0.16 ug/l
100-41-4 Ethylbenzene 28.2 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene 4.8 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene 1.3 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 117 a 1.3 0.41 ug/l
91-20-3 Naphthalene 20.1 0.50 0.12 ug/l
103-65-1 n-Propylbenzene 8.2 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene 2.4 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 7.9 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene 0.26 0.50 0.14 ug/l J
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 0.90 1.0 0.30 ug/l J
95-47-6 o-Xylene 0.59 0.50 0.13 ug/l
1330-20-7 Xylene (total)1.5 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 99%98%70-130%
17060-07-0 1,2-Dichloroethane-D4 105%101%70-130%
2037-26-5 Toluene-D8 97%98%70-130%
460-00-4 4-Bromofluorobenzene 100%99%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
20 of 84
FA21787 33.5
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-8
Lab Sample ID:FA21787-6 Date Sampled:01/29/15
Matrix:AQ - Ground Water Date Received:01/30/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E036173.D 1 02/03/15 TD n/a n/a VE1204
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
21 of 84
FA21787 33.6
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-8
Lab Sample ID:FA21787-6 Date Sampled:01/29/15
Matrix:AQ - Ground Water Date Received:01/30/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
22 of 84
FA21787 33.6
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-9
Lab Sample ID:FA21787-7 Date Sampled:01/29/15
Matrix:AQ - Ground Water Date Received:01/30/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0192077.D 1 02/04/15 TD n/a n/a VA1632
Run #2 A0192057.D 5 02/03/15 TD n/a n/a VA1631
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 162 a 2.5 0.86 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene 5.7 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene 3.6 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane 3.8 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
23 of 84
FA21787 33.7
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-9
Lab Sample ID:FA21787-7 Date Sampled:01/29/15
Matrix:AQ - Ground Water Date Received:01/30/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 1.3 0.50 0.16 ug/l
100-41-4 Ethylbenzene 36.1 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene 8.3 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene 1.4 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 1.3 0.50 0.16 ug/l
91-20-3 Naphthalene 32.6 0.50 0.12 ug/l
103-65-1 n-Propylbenzene 18.8 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene 1.7 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 89.3 a 2.5 0.68 ug/l
108-67-8 1,3,5-Trimethylbenzene 6.0 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 52.8 1.0 0.30 ug/l
95-47-6 o-Xylene 18.7 0.50 0.13 ug/l
1330-20-7 Xylene (total)71.5 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%98%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%105%70-130%
2037-26-5 Toluene-D8 100%100%70-130%
460-00-4 4-Bromofluorobenzene 102%102%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
24 of 84
FA21787 33.7
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-10
Lab Sample ID:FA21787-8 Date Sampled:01/29/15
Matrix:AQ - Ground Water Date Received:01/30/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0192078.D 1 02/04/15 TD n/a n/a VA1632
Run #2 A0192089.D 2 02/04/15 TD n/a n/a VA1632
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 0.43 0.50 0.17 ug/l J
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane 15.9 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
25 of 84
FA21787 33.8
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-10
Lab Sample ID:FA21787-8 Date Sampled:01/29/15
Matrix:AQ - Ground Water Date Received:01/30/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 3.2 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 73.9 a 1.0 0.33 ug/l
91-20-3 Naphthalene 0.74 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 98%97%70-130%
17060-07-0 1,2-Dichloroethane-D4 98%100%70-130%
2037-26-5 Toluene-D8 101%100%70-130%
460-00-4 4-Bromofluorobenzene 99%103%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
26 of 84
FA21787 33.8
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-14
Lab Sample ID:FA21787-9 Date Sampled:01/29/15
Matrix:AQ - Ground Water Date Received:01/30/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0192079.D 1 02/04/15 TD n/a n/a VA1632
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
27 of 84
FA21787 33.9
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-14
Lab Sample ID:FA21787-9 Date Sampled:01/29/15
Matrix:AQ - Ground Water Date Received:01/30/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 97%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
28 of 84
FA21787 33.9
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-15
Lab Sample ID:FA21787-10 Date Sampled:01/29/15
Matrix:AQ - Ground Water Date Received:01/30/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0192080.D 1 02/04/15 TD n/a n/a VA1632
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
29 of 84
FA21787 33.10
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-15
Lab Sample ID:FA21787-10 Date Sampled:01/29/15
Matrix:AQ - Ground Water Date Received:01/30/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 97%70-130%
17060-07-0 1,2-Dichloroethane-D4 99%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 104%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
30 of 84
FA21787 33.10
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-18
Lab Sample ID:FA21787-11 Date Sampled:01/29/15
Matrix:AQ - Ground Water Date Received:01/30/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0192081.D 1 02/04/15 TD n/a n/a VA1632
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
31 of 84
FA21787 33.11
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-18
Lab Sample ID:FA21787-11 Date Sampled:01/29/15
Matrix:AQ - Ground Water Date Received:01/30/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 98%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
32 of 84
FA21787 33.11
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-19
Lab Sample ID:FA21787-12 Date Sampled:01/29/15
Matrix:AQ - Ground Water Date Received:01/30/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0192082.D 1 02/04/15 TD n/a n/a VA1632
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
33 of 84
FA21787 33.12
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-19
Lab Sample ID:FA21787-12 Date Sampled:01/29/15
Matrix:AQ - Ground Water Date Received:01/30/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 98%70-130%
17060-07-0 1,2-Dichloroethane-D4 101%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
34 of 84
FA21787 33.12
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-20
Lab Sample ID:FA21787-13 Date Sampled:01/29/15
Matrix:AQ - Ground Water Date Received:01/30/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0192083.D 1 02/04/15 TD n/a n/a VA1632
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
35 of 84
FA21787 33.13
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-20
Lab Sample ID:FA21787-13 Date Sampled:01/29/15
Matrix:AQ - Ground Water Date Received:01/30/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.34 0.50 0.16 ug/l J
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
36 of 84
FA21787 33.13
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-21
Lab Sample ID:FA21787-14 Date Sampled:01/29/15
Matrix:AQ - Ground Water Date Received:01/30/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0192084.D 1 02/04/15 TD n/a n/a VA1632
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
37 of 84
FA21787 33.14
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-21
Lab Sample ID:FA21787-14 Date Sampled:01/29/15
Matrix:AQ - Ground Water Date Received:01/30/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.22 0.50 0.16 ug/l J
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 97%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
38 of 84
FA21787 33.14
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-22
Lab Sample ID:FA21787-15 Date Sampled:01/29/15
Matrix:AQ - Ground Water Date Received:01/30/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0192085.D 1 02/04/15 TD n/a n/a VA1632
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
39 of 84
FA21787 33.15
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-22
Lab Sample ID:FA21787-15 Date Sampled:01/29/15
Matrix:AQ - Ground Water Date Received:01/30/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.75 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 98%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 103%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
40 of 84
FA21787 33.15
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-23
Lab Sample ID:FA21787-16 Date Sampled:01/29/15
Matrix:AQ - Ground Water Date Received:01/30/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0192064.D 1 02/03/15 TD n/a n/a VA1631
Run #2 A0192088.D 2 02/04/15 TD n/a n/a VA1632
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 65.2 a 1.0 0.34 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene 0.47 0.50 0.14 ug/l J
135-98-8 sec-Butylbenzene 0.67 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane 1.1 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane 11.3 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
41 of 84
FA21787 33.16
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-23
Lab Sample ID:FA21787-16 Date Sampled:01/29/15
Matrix:AQ - Ground Water Date Received:01/30/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene 6.4 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene 3.0 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene 1.4 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride 0.57 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene 10.3 0.50 0.12 ug/l
103-65-1 n-Propylbenzene 3.8 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene 0.93 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 4.4 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene 0.64 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 1.1 1.0 0.30 ug/l
95-47-6 o-Xylene 2.8 0.50 0.13 ug/l
1330-20-7 Xylene (total)3.9 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 98%98%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%107%70-130%
2037-26-5 Toluene-D8 97%97%70-130%
460-00-4 4-Bromofluorobenzene 102%101%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
42 of 84
FA21787 33.16
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-25
Lab Sample ID:FA21787-17 Date Sampled:01/29/15
Matrix:AQ - Ground Water Date Received:01/30/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E036197.D 1 02/04/15 TD n/a n/a VE1205
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride a ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
43 of 84
FA21787 33.17
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-25
Lab Sample ID:FA21787-17 Date Sampled:01/29/15
Matrix:AQ - Ground Water Date Received:01/30/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.35 0.50 0.16 ug/l J
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 97%70-130%
17060-07-0 1,2-Dichloroethane-D4 97%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
(a) Associated BS recovery outside control limits.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
44 of 84
FA21787 33.17
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-27
Lab Sample ID:FA21787-18 Date Sampled:01/29/15
Matrix:AQ - Ground Water Date Received:01/30/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E036198.D 1 02/04/15 TD n/a n/a VE1205
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride a ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
45 of 84
FA21787 33.18
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-27
Lab Sample ID:FA21787-18 Date Sampled:01/29/15
Matrix:AQ - Ground Water Date Received:01/30/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 98%70-130%
17060-07-0 1,2-Dichloroethane-D4 99%70-130%
2037-26-5 Toluene-D8 93%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
(a) Associated BS recovery outside control limits.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
46 of 84
FA21787 33.18
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-28
Lab Sample ID:FA21787-19 Date Sampled:01/29/15
Matrix:AQ - Ground Water Date Received:01/30/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E036199.D 1 02/04/15 TD n/a n/a VE1205
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride a ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
47 of 84
FA21787 33.19
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-28
Lab Sample ID:FA21787-19 Date Sampled:01/29/15
Matrix:AQ - Ground Water Date Received:01/30/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 101%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
(a) Associated BS recovery outside control limits.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
48 of 84
FA21787 33.19
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-30
Lab Sample ID:FA21787-20 Date Sampled:01/29/15
Matrix:AQ - Ground Water Date Received:01/30/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E036200.D 1 02/04/15 TD n/a n/a VE1205
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride a ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
49 of 84
FA21787 33.20
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-30
Lab Sample ID:FA21787-20 Date Sampled:01/29/15
Matrix:AQ - Ground Water Date Received:01/30/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.27 0.50 0.16 ug/l J
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
(a) Associated BS recovery outside control limits.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
50 of 84
FA21787 33.20
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:WSW-4
Lab Sample ID:FA21787-21 Date Sampled:01/29/15
Matrix:AQ - Water Date Received:01/30/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E036201.D 1 02/04/15 TD n/a n/a VE1205
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride a ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
51 of 84
FA21787 33.21
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:WSW-4
Lab Sample ID:FA21787-21 Date Sampled:01/29/15
Matrix:AQ - Water Date Received:01/30/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
(a) Associated BS recovery outside control limits.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
52 of 84
FA21787 33.21
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:WSW-6
Lab Sample ID:FA21787-22 Date Sampled:01/29/15
Matrix:AQ - Water Date Received:01/30/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E036202.D 1 02/04/15 TD n/a n/a VE1205
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane 0.95 0.50 0.15 ug/l
75-25-2 Bromoform 0.61 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride a ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform 0.67 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane 1.2 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
53 of 84
FA21787 33.22
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:WSW-6
Lab Sample ID:FA21787-22 Date Sampled:01/29/15
Matrix:AQ - Water Date Received:01/30/15
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
2037-26-5 Toluene-D8 96%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
(a) Associated BS recovery outside control limits.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
54 of 84
FA21787 33.22
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Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Southeast
Section 4
55 of 84
FA21787 4
FA21787: Chain of Custody
Page 1 of 4
56 of 84
FA21787 44.1
FA21787: Chain of Custody
Page 2 of 4
57 of 84
FA21787 44.1
FA21787: Chain of Custody
Page 3 of 4
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FA21787 44.1
FA21787: Chain of Custody
Page 4 of 4
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Accutest Laboratories
GC/MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Southeast
Section 5
60 of 84
FA21787 5
Method Blank Summary Page 1 of 2
Job Number:FA21787
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1204-MB E036160.D 1 02/03/15 TD n/a n/a VE1204
The QC reported here applies to the following samples:Method: SM 6200B
FA21787-1, FA21787-3, FA21787-4, FA21787-5, FA21787-6
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
61 of 84
FA21787 55.1.1
Method Blank Summary Page 2 of 2
Job Number:FA21787
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1204-MB E036160.D 1 02/03/15 TD n/a n/a VE1204
The QC reported here applies to the following samples:Method: SM 6200B
FA21787-1, FA21787-3, FA21787-4, FA21787-5, FA21787-6
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
62 of 84
FA21787 55.1.1
Method Blank Summary Page 1 of 2
Job Number:FA21787
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1631-MB A0192049.D 1 02/03/15 TD n/a n/a VA1631
The QC reported here applies to the following samples:Method: SM 6200B
FA21787-7, FA21787-16
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
63 of 84
FA21787 55.1.2
Method Blank Summary Page 2 of 2
Job Number:FA21787
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1631-MB A0192049.D 1 02/03/15 TD n/a n/a VA1631
The QC reported here applies to the following samples:Method: SM 6200B
FA21787-7, FA21787-16
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 97%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
64 of 84
FA21787 55.1.2
Method Blank Summary Page 1 of 2
Job Number:FA21787
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1632-MB A0192075.D 1 02/04/15 TD n/a n/a VA1632
The QC reported here applies to the following samples:Method: SM 6200B
FA21787-2, FA21787-7, FA21787-8, FA21787-9, FA21787-10, FA21787-11, FA21787-12, FA21787-13, FA21787-14,
FA21787-15, FA21787-16
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
65 of 84
FA21787 55.1.3
Method Blank Summary Page 2 of 2
Job Number:FA21787
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1632-MB A0192075.D 1 02/04/15 TD n/a n/a VA1632
The QC reported here applies to the following samples:Method: SM 6200B
FA21787-2, FA21787-7, FA21787-8, FA21787-9, FA21787-10, FA21787-11, FA21787-12, FA21787-13, FA21787-14,
FA21787-15, FA21787-16
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 94%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
66 of 84
FA21787 55.1.3
Method Blank Summary Page 1 of 2
Job Number:FA21787
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1205-MB E036194.D 1 02/04/15 TD n/a n/a VE1205
The QC reported here applies to the following samples:Method: SM 6200B
FA21787-17, FA21787-18, FA21787-19, FA21787-20, FA21787-21, FA21787-22
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
67 of 84
FA21787 55.1.4
Method Blank Summary Page 2 of 2
Job Number:FA21787
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1205-MB E036194.D 1 02/04/15 TD n/a n/a VE1205
The QC reported here applies to the following samples:Method: SM 6200B
FA21787-17, FA21787-18, FA21787-19, FA21787-20, FA21787-21, FA21787-22
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 97%70-130%
17060-07-0 1,2-Dichloroethane-D4 101%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
68 of 84
FA21787 55.1.4
Blank Spike Summary Page 1 of 2
Job Number:FA21787
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1204-BS E036167.D 1 02/03/15 TD n/a n/a VE1204
The QC reported here applies to the following samples:Method: SM 6200B
FA21787-1, FA21787-3, FA21787-4, FA21787-5, FA21787-6
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 9.5 95 70-130
108-86-1 Bromobenzene 10 9.0 90 70-130
74-97-5 Bromochloromethane 10 9.2 92 70-130
75-27-4 Bromodichloromethane 10 9.5 95 70-130
75-25-2 Bromoform 10 8.3 83 70-130
104-51-8 n-Butylbenzene 10 8.2 82 70-130
135-98-8 sec-Butylbenzene 10 10.2 102 70-130
98-06-6 tert-Butylbenzene 10 9.8 98 70-130
56-23-5 Carbon Tetrachloride 10 11.3 113 70-130
108-90-7 Chlorobenzene 10 9.5 95 70-130
75-00-3 Chloroethane 10 8.6 86 60-140
67-66-3 Chloroform 10 9.5 95 70-130
95-49-8 o-Chlorotoluene 10 9.6 96 70-130
106-43-4 p-Chlorotoluene 10 10.0 100 70-130
124-48-1 Dibromochloromethane 10 8.6 86 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 7.9 79 70-130
106-93-4 1,2-Dibromoethane 10 9.1 91 70-130
75-71-8 Dichlorodifluoromethane 10 8.8 88 60-140
95-50-1 1,2-Dichlorobenzene 10 9.5 95 70-130
541-73-1 1,3-Dichlorobenzene 10 9.9 99 70-130
106-46-7 1,4-Dichlorobenzene 10 8.9 89 70-130
75-34-3 1,1-Dichloroethane 10 9.4 94 70-130
107-06-2 1,2-Dichloroethane 10 9.3 93 70-130
75-35-4 1,1-Dichloroethylene 10 10.6 106 70-130
156-59-2 cis-1,2-Dichloroethylene 10 9.5 95 70-130
156-60-5 trans-1,2-Dichloroethylene 10 9.7 97 70-130
78-87-5 1,2-Dichloropropane 10 9.4 94 70-130
142-28-9 1,3-Dichloropropane 10 9.0 90 70-130
594-20-7 2,2-Dichloropropane 10 10.2 102 70-130
563-58-6 1,1-Dichloropropene 10 10.3 103 70-130
10061-01-5 cis-1,3-Dichloropropene 10 9.2 92 70-130
10061-02-6 trans-1,3-Dichloropropene 10 9.5 95 70-130
108-20-3 Di-Isopropyl Ether 10 9.1 91 70-130
100-41-4 Ethylbenzene 10 9.4 94 70-130
87-68-3 Hexachlorobutadiene 10 9.0 90 70-130
98-82-8 Isopropylbenzene 10 8.9 89 70-130
* = Outside of Control Limits.
69 of 84
FA21787 55.2.1
Blank Spike Summary Page 2 of 2
Job Number:FA21787
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1204-BS E036167.D 1 02/03/15 TD n/a n/a VE1204
The QC reported here applies to the following samples:Method: SM 6200B
FA21787-1, FA21787-3, FA21787-4, FA21787-5, FA21787-6
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 8.5 85 70-130
74-83-9 Methyl Bromide 10 7.5 75 60-140
74-87-3 Methyl Chloride 10 8.2 82 60-140
74-95-3 Methylene Bromide 10 9.2 92 70-130
75-09-2 Methylene Chloride 10 8.8 88 70-130
1634-04-4 Methyl Tert Butyl Ether 10 9.0 90 70-130
91-20-3 Naphthalene 10 8.3 83 70-130
103-65-1 n-Propylbenzene 10 10.3 103 70-130
100-42-5 Styrene 10 8.4 84 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 9.4 94 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 8.3 83 70-130
127-18-4 Tetrachloroethylene 10 9.7 97 70-130
108-88-3 Toluene 10 9.1 91 70-130
87-61-6 1,2,3-Trichlorobenzene 10 8.4 84 70-130
120-82-1 1,2,4-Trichlorobenzene 10 8.6 86 70-130
71-55-6 1,1,1-Trichloroethane 10 9.7 97 70-130
79-00-5 1,1,2-Trichloroethane 10 8.9 89 70-130
79-01-6 Trichloroethylene 10 9.7 97 70-130
75-69-4 Trichlorofluoromethane 10 8.5 85 60-140
96-18-4 1,2,3-Trichloropropane 10 8.6 86 70-130
95-63-6 1,2,4-Trimethylbenzene 10 9.0 90 70-130
108-67-8 1,3,5-Trimethylbenzene 10 10.6 106 70-130
75-01-4 Vinyl Chloride 10 8.2 82 60-140
m,p-Xylene 20 19.7 99 70-130
95-47-6 o-Xylene 10 10.0 100 70-130
1330-20-7 Xylene (total)30 29.7 99 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 98%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
* = Outside of Control Limits.
70 of 84
FA21787 55.2.1
Blank Spike Summary Page 1 of 2
Job Number:FA21787
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1631-BS A0192047.D 1 02/03/15 TD n/a n/a VA1631
The QC reported here applies to the following samples:Method: SM 6200B
FA21787-7, FA21787-16
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 8.6 86 70-130
108-86-1 Bromobenzene 10 8.7 87 70-130
74-97-5 Bromochloromethane 10 8.3 83 70-130
75-27-4 Bromodichloromethane 10 8.9 89 70-130
75-25-2 Bromoform 10 8.2 82 70-130
104-51-8 n-Butylbenzene 10 8.8 88 70-130
135-98-8 sec-Butylbenzene 10 9.7 97 70-130
98-06-6 tert-Butylbenzene 10 9.4 94 70-130
56-23-5 Carbon Tetrachloride 10 8.9 89 70-130
108-90-7 Chlorobenzene 10 9.1 91 70-130
75-00-3 Chloroethane 10 8.9 89 60-140
67-66-3 Chloroform 10 8.5 85 70-130
95-49-8 o-Chlorotoluene 10 9.3 93 70-130
106-43-4 p-Chlorotoluene 10 9.6 96 70-130
124-48-1 Dibromochloromethane 10 8.7 87 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 7.7 77 70-130
106-93-4 1,2-Dibromoethane 10 8.7 87 70-130
75-71-8 Dichlorodifluoromethane 10 9.2 92 60-140
95-50-1 1,2-Dichlorobenzene 10 9.2 92 70-130
541-73-1 1,3-Dichlorobenzene 10 9.5 95 70-130
106-46-7 1,4-Dichlorobenzene 10 8.7 87 70-130
75-34-3 1,1-Dichloroethane 10 8.3 83 70-130
107-06-2 1,2-Dichloroethane 10 8.9 89 70-130
75-35-4 1,1-Dichloroethylene 10 9.1 91 70-130
156-59-2 cis-1,2-Dichloroethylene 10 8.5 85 70-130
156-60-5 trans-1,2-Dichloroethylene 10 8.6 86 70-130
78-87-5 1,2-Dichloropropane 10 8.8 88 70-130
142-28-9 1,3-Dichloropropane 10 8.5 85 70-130
594-20-7 2,2-Dichloropropane 10 8.6 86 70-130
563-58-6 1,1-Dichloropropene 10 9.2 92 70-130
10061-01-5 cis-1,3-Dichloropropene 10 8.5 85 70-130
10061-02-6 trans-1,3-Dichloropropene 10 9.1 91 70-130
108-20-3 Di-Isopropyl Ether 10 8.2 82 70-130
100-41-4 Ethylbenzene 10 8.6 86 70-130
87-68-3 Hexachlorobutadiene 10 8.8 88 70-130
98-82-8 Isopropylbenzene 10 9.5 95 70-130
* = Outside of Control Limits.
71 of 84
FA21787 55.2.2
Blank Spike Summary Page 2 of 2
Job Number:FA21787
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1631-BS A0192047.D 1 02/03/15 TD n/a n/a VA1631
The QC reported here applies to the following samples:Method: SM 6200B
FA21787-7, FA21787-16
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 9.5 95 70-130
74-83-9 Methyl Bromide 10 10.1 101 60-140
74-87-3 Methyl Chloride 10 10.4 104 60-140
74-95-3 Methylene Bromide 10 8.6 86 70-130
75-09-2 Methylene Chloride 10 9.2 92 70-130
1634-04-4 Methyl Tert Butyl Ether 10 8.0 80 70-130
91-20-3 Naphthalene 10 8.7 87 70-130
103-65-1 n-Propylbenzene 10 9.8 98 70-130
100-42-5 Styrene 10 8.6 86 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 8.8 88 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 8.3 83 70-130
127-18-4 Tetrachloroethylene 10 8.9 89 70-130
108-88-3 Toluene 10 9.3 93 70-130
87-61-6 1,2,3-Trichlorobenzene 10 8.8 88 70-130
120-82-1 1,2,4-Trichlorobenzene 10 8.7 87 70-130
71-55-6 1,1,1-Trichloroethane 10 8.4 84 70-130
79-00-5 1,1,2-Trichloroethane 10 8.7 87 70-130
79-01-6 Trichloroethylene 10 9.0 90 70-130
75-69-4 Trichlorofluoromethane 10 10 100 60-140
96-18-4 1,2,3-Trichloropropane 10 8.6 86 70-130
95-63-6 1,2,4-Trimethylbenzene 10 8.7 87 70-130
108-67-8 1,3,5-Trimethylbenzene 10 8.8 88 70-130
75-01-4 Vinyl Chloride 10 10.0 100 60-140
m,p-Xylene 20 18.0 90 70-130
95-47-6 o-Xylene 10 9.3 93 70-130
1330-20-7 Xylene (total)30 27.3 91 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 99%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
* = Outside of Control Limits.
72 of 84
FA21787 55.2.2
Blank Spike Summary Page 1 of 2
Job Number:FA21787
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1632-BS A0192076.D 1 02/04/15 TD n/a n/a VA1632
The QC reported here applies to the following samples:Method: SM 6200B
FA21787-2, FA21787-7, FA21787-8, FA21787-9, FA21787-10, FA21787-11, FA21787-12, FA21787-13, FA21787-14,
FA21787-15, FA21787-16
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 8.3 83 70-130
108-86-1 Bromobenzene 10 8.3 83 70-130
74-97-5 Bromochloromethane 10 8.2 82 70-130
75-27-4 Bromodichloromethane 10 8.4 84 70-130
75-25-2 Bromoform 10 7.2 72 70-130
104-51-8 n-Butylbenzene 10 8.4 84 70-130
135-98-8 sec-Butylbenzene 10 9.1 91 70-130
98-06-6 tert-Butylbenzene 10 8.8 88 70-130
56-23-5 Carbon Tetrachloride 10 8.3 83 70-130
108-90-7 Chlorobenzene 10 9.0 90 70-130
75-00-3 Chloroethane 10 11.5 115 60-140
67-66-3 Chloroform 10 8.4 84 70-130
95-49-8 o-Chlorotoluene 10 8.7 87 70-130
106-43-4 p-Chlorotoluene 10 9.0 90 70-130
124-48-1 Dibromochloromethane 10 8.0 80 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 7.3 73 70-130
106-93-4 1,2-Dibromoethane 10 8.4 84 70-130
75-71-8 Dichlorodifluoromethane 10 11.3 113 60-140
95-50-1 1,2-Dichlorobenzene 10 8.8 88 70-130
541-73-1 1,3-Dichlorobenzene 10 9.1 91 70-130
106-46-7 1,4-Dichlorobenzene 10 8.3 83 70-130
75-34-3 1,1-Dichloroethane 10 8.1 81 70-130
107-06-2 1,2-Dichloroethane 10 8.6 86 70-130
75-35-4 1,1-Dichloroethylene 10 8.6 86 70-130
156-59-2 cis-1,2-Dichloroethylene 10 8.5 85 70-130
156-60-5 trans-1,2-Dichloroethylene 10 8.2 82 70-130
78-87-5 1,2-Dichloropropane 10 8.5 85 70-130
142-28-9 1,3-Dichloropropane 10 8.3 83 70-130
594-20-7 2,2-Dichloropropane 10 8.1 81 70-130
563-58-6 1,1-Dichloropropene 10 8.9 89 70-130
10061-01-5 cis-1,3-Dichloropropene 10 8.0 80 70-130
10061-02-6 trans-1,3-Dichloropropene 10 8.7 87 70-130
108-20-3 Di-Isopropyl Ether 10 7.9 79 70-130
100-41-4 Ethylbenzene 10 8.3 83 70-130
87-68-3 Hexachlorobutadiene 10 8.3 83 70-130
98-82-8 Isopropylbenzene 10 9.1 91 70-130
* = Outside of Control Limits.
73 of 84
FA21787 55.2.3
Blank Spike Summary Page 2 of 2
Job Number:FA21787
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1632-BS A0192076.D 1 02/04/15 TD n/a n/a VA1632
The QC reported here applies to the following samples:Method: SM 6200B
FA21787-2, FA21787-7, FA21787-8, FA21787-9, FA21787-10, FA21787-11, FA21787-12, FA21787-13, FA21787-14,
FA21787-15, FA21787-16
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 8.8 88 70-130
74-83-9 Methyl Bromide 10 12.8 128 60-140
74-87-3 Methyl Chloride 10 13.0 130 60-140
74-95-3 Methylene Bromide 10 8.4 84 70-130
75-09-2 Methylene Chloride 10 9.0 90 70-130
1634-04-4 Methyl Tert Butyl Ether 10 7.7 77 70-130
91-20-3 Naphthalene 10 7.7 77 70-130
103-65-1 n-Propylbenzene 10 9.0 90 70-130
100-42-5 Styrene 10 8.1 81 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 8.4 84 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 7.7 77 70-130
127-18-4 Tetrachloroethylene 10 8.4 84 70-130
108-88-3 Toluene 10 9.0 90 70-130
87-61-6 1,2,3-Trichlorobenzene 10 7.9 79 70-130
120-82-1 1,2,4-Trichlorobenzene 10 8.1 81 70-130
71-55-6 1,1,1-Trichloroethane 10 8.1 81 70-130
79-00-5 1,1,2-Trichloroethane 10 8.6 86 70-130
79-01-6 Trichloroethylene 10 8.7 87 70-130
75-69-4 Trichlorofluoromethane 10 12.6 126 60-140
96-18-4 1,2,3-Trichloropropane 10 8.0 80 70-130
95-63-6 1,2,4-Trimethylbenzene 10 8.1 81 70-130
108-67-8 1,3,5-Trimethylbenzene 10 8.1 81 70-130
75-01-4 Vinyl Chloride 10 12.7 127 60-140
m,p-Xylene 20 17.2 86 70-130
95-47-6 o-Xylene 10 8.9 89 70-130
1330-20-7 Xylene (total)30 26.1 87 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%70-130%
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
* = Outside of Control Limits.
74 of 84
FA21787 55.2.3
Blank Spike Summary Page 1 of 2
Job Number:FA21787
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1205-BS E036206.D 1 02/04/15 TD n/a n/a VE1205
The QC reported here applies to the following samples:Method: SM 6200B
FA21787-17, FA21787-18, FA21787-19, FA21787-20, FA21787-21, FA21787-22
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 11.1 111 70-130
108-86-1 Bromobenzene 10 10.3 103 70-130
74-97-5 Bromochloromethane 10 10.9 109 70-130
75-27-4 Bromodichloromethane 10 10.9 109 70-130
75-25-2 Bromoform 10 9.7 97 70-130
104-51-8 n-Butylbenzene 10 9.7 97 70-130
135-98-8 sec-Butylbenzene 10 10.8 108 70-130
98-06-6 tert-Butylbenzene 10 10.6 106 70-130
56-23-5 Carbon Tetrachloride 10 13.1 131*70-130
108-90-7 Chlorobenzene 10 10.2 102 70-130
75-00-3 Chloroethane 10 9.4 94 60-140
67-66-3 Chloroform 10 11.0 110 70-130
95-49-8 o-Chlorotoluene 10 10.5 105 70-130
106-43-4 p-Chlorotoluene 10 10.5 105 70-130
124-48-1 Dibromochloromethane 10 9.9 99 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 10 100 70-130
106-93-4 1,2-Dibromoethane 10 10.6 106 70-130
75-71-8 Dichlorodifluoromethane 10 10.5 105 60-140
95-50-1 1,2-Dichlorobenzene 10 10.1 101 70-130
541-73-1 1,3-Dichlorobenzene 10 10.2 102 70-130
106-46-7 1,4-Dichlorobenzene 10 10.1 101 70-130
75-34-3 1,1-Dichloroethane 10 11.0 110 70-130
107-06-2 1,2-Dichloroethane 10 11.1 111 70-130
75-35-4 1,1-Dichloroethylene 10 11.9 119 70-130
156-59-2 cis-1,2-Dichloroethylene 10 10.8 108 70-130
156-60-5 trans-1,2-Dichloroethylene 10 11.3 113 70-130
78-87-5 1,2-Dichloropropane 10 10.9 109 70-130
142-28-9 1,3-Dichloropropane 10 10.5 105 70-130
594-20-7 2,2-Dichloropropane 10 12.1 121 70-130
563-58-6 1,1-Dichloropropene 10 11.4 114 70-130
10061-01-5 cis-1,3-Dichloropropene 10 11.4 114 70-130
10061-02-6 trans-1,3-Dichloropropene 10 10.9 109 70-130
108-20-3 Di-Isopropyl Ether 10 11.3 113 70-130
100-41-4 Ethylbenzene 10 10.8 108 70-130
87-68-3 Hexachlorobutadiene 10 10.3 103 70-130
98-82-8 Isopropylbenzene 10 9.4 94 70-130
* = Outside of Control Limits.
75 of 84
FA21787 55.2.4
Blank Spike Summary Page 2 of 2
Job Number:FA21787
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1205-BS E036206.D 1 02/04/15 TD n/a n/a VE1205
The QC reported here applies to the following samples:Method: SM 6200B
FA21787-17, FA21787-18, FA21787-19, FA21787-20, FA21787-21, FA21787-22
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 9.2 92 70-130
74-83-9 Methyl Bromide 10 8.7 87 60-140
74-87-3 Methyl Chloride 10 9.7 97 60-140
74-95-3 Methylene Bromide 10 10.8 108 70-130
75-09-2 Methylene Chloride 10 9.9 99 70-130
1634-04-4 Methyl Tert Butyl Ether 10 11.4 114 70-130
91-20-3 Naphthalene 10 10.5 105 70-130
103-65-1 n-Propylbenzene 10 10.7 107 70-130
100-42-5 Styrene 10 9.9 99 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 10.4 104 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 10.1 101 70-130
127-18-4 Tetrachloroethylene 10 10.9 109 70-130
108-88-3 Toluene 10 10.6 106 70-130
87-61-6 1,2,3-Trichlorobenzene 10 10.0 100 70-130
120-82-1 1,2,4-Trichlorobenzene 10 10.0 100 70-130
71-55-6 1,1,1-Trichloroethane 10 11.2 112 70-130
79-00-5 1,1,2-Trichloroethane 10 10.4 104 70-130
79-01-6 Trichloroethylene 10 10.9 109 70-130
75-69-4 Trichlorofluoromethane 10 10.1 101 60-140
96-18-4 1,2,3-Trichloropropane 10 10.3 103 70-130
95-63-6 1,2,4-Trimethylbenzene 10 10.6 106 70-130
108-67-8 1,3,5-Trimethylbenzene 10 12.4 124 70-130
75-01-4 Vinyl Chloride 10 9.8 98 60-140
m,p-Xylene 20 21.9 110 70-130
95-47-6 o-Xylene 10 10.7 107 70-130
1330-20-7 Xylene (total)30 32.6 109 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 101%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
* = Outside of Control Limits.
76 of 84
FA21787 55.2.4
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA21787
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA21825-1MS A0192055.D 10 02/03/15 TD n/a n/a VA1631
FA21825-1MSD A0192056.D 10 02/03/15 TD n/a n/a VA1631
FA21825-1 A0192050.D 10 02/03/15 TD n/a n/a VA1631
The QC reported here applies to the following samples:Method: SM 6200B
FA21787-7, FA21787-16
FA21825-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene ND 100 76.0 76 100 91.0 91 18 70-130/20
108-86-1 Bromobenzene ND 100 75.7 76 100 92.8 93 20 70-130/20
74-97-5 Bromochloromethane ND 100 76.1 76 100 91.2 91 18 70-130/20
75-27-4 Bromodichloromethane ND 100 77.5 78 100 86.2 86 11 70-130/20
75-25-2 Bromoform ND 100 67.5 68*100 73.8 74 9 70-130/20
104-51-8 n-Butylbenzene ND 100 77.4 77 100 96.5 97 22*70-130/20
135-98-8 sec-Butylbenzene ND 100 82.6 83 100 103 103 22*70-130/20
98-06-6 tert-Butylbenzene ND 100 80.8 81 100 101 101 22*70-130/20
56-23-5 Carbon Tetrachloride ND 100 78.4 78 100 88.4 88 12 70-130/20
108-90-7 Chlorobenzene ND 100 80.2 80 100 96.8 97 19 70-130/20
75-00-3 Chloroethane ND 100 87.2 87 100 96.7 97 10 60-140/20
67-66-3 Chloroform ND 100 81.8 82 100 97.2 97 17 70-130/20
95-49-8 o-Chlorotoluene ND 100 87.7 88 100 107 107 20 70-130/20
106-43-4 p-Chlorotoluene ND 100 82.4 82 100 101 101 20 70-130/20
124-48-1 Dibromochloromethane ND 100 73.3 73 100 82.2 82 11 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 100 71.7 72 100 85.1 85 17 70-130/20
106-93-4 1,2-Dibromoethane ND 100 78.5 79 100 93.6 94 18 70-130/20
75-71-8 Dichlorodifluoromethane ND 100 84.7 85 100 99.8 100 16 60-140/20
95-50-1 1,2-Dichlorobenzene ND 100 81.8 82 100 101 101 21*70-130/20
541-73-1 1,3-Dichlorobenzene ND 100 82.9 83 100 102 102 21*70-130/20
106-46-7 1,4-Dichlorobenzene ND 100 76.4 76 100 93.3 93 20 70-130/20
75-34-3 1,1-Dichloroethane ND 100 75.2 75 100 89.8 90 18 70-130/20
107-06-2 1,2-Dichloroethane ND 100 80.9 81 100 95.7 96 17 70-130/20
75-35-4 1,1-Dichloroethylene ND 100 80.0 80 100 99.2 99 21*70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 100 76.7 77 100 93.0 93 19 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 100 75.5 76 100 89.8 90 17 70-130/20
78-87-5 1,2-Dichloropropane ND 100 77.8 78 100 92.4 92 17 70-130/20
142-28-9 1,3-Dichloropropane ND 100 76.7 77 100 92.2 92 18 70-130/20
594-20-7 2,2-Dichloropropane ND 100 75.2 75 100 89.5 90 17 70-130/20
563-58-6 1,1-Dichloropropene ND 100 81.1 81 100 97.8 98 19 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 100 74.4 74 100 79.0 79 6 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 100 81.4 81 100 89.6 90 10 70-130/20
108-20-3 Di-Isopropyl Ether ND 100 74.7 75 100 89.0 89 17 70-130/20
100-41-4 Ethylbenzene 30.5 100 97.9 67*100 119 89 19 70-130/20
87-68-3 Hexachlorobutadiene ND 100 75.5 76 100 96.5 97 24*70-130/20
98-82-8 Isopropylbenzene 3.0 J 100 84.2 81 100 103 100 20 70-130/20
* = Outside of Control Limits.
77 of 84
FA21787 55.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA21787
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA21825-1MS A0192055.D 10 02/03/15 TD n/a n/a VA1631
FA21825-1MSD A0192056.D 10 02/03/15 TD n/a n/a VA1631
FA21825-1 A0192050.D 10 02/03/15 TD n/a n/a VA1631
The QC reported here applies to the following samples:Method: SM 6200B
FA21787-7, FA21787-16
FA21825-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene 1.7 J 100 81.7 80 100 101 99 21*70-130/20
74-83-9 Methyl Bromide ND 100 98.7 99 100 112 112 13 60-140/20
74-87-3 Methyl Chloride ND 100 96.8 97 100 115 115 17 60-140/20
74-95-3 Methylene Bromide ND 100 79.3 79 100 92.5 93 15 70-130/20
75-09-2 Methylene Chloride ND 100 86.8 87 100 104 104 18 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 100 72.2 72 100 87.0 87 19 70-130/20
91-20-3 Naphthalene 3.0 J 100 76.6 74 100 95.7 93 22*70-130/20
103-65-1 n-Propylbenzene 8.1 100 88.7 81 100 108 100 20 70-130/20
100-42-5 Styrene ND 100 74.4 74 100 89.9 90 19 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 100 77.2 77 100 91.9 92 17 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 100 75.0 75 100 91.1 91 19 70-130/20
127-18-4 Tetrachloroethylene ND 100 76.1 76 100 91.5 92 18 70-130/20
108-88-3 Toluene 27.7 100 101 73 100 123 95 20 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 100 75.2 75 100 95.2 95 23*70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 100 76.0 76 100 95.4 95 23*70-130/20
71-55-6 1,1,1-Trichloroethane ND 100 75.2 75 100 90.6 91 19 70-130/20
79-00-5 1,1,2-Trichloroethane ND 100 203 203*100 247 247*20 70-130/20
79-01-6 Trichloroethylene ND 100 79.8 80 100 94.6 95 17 70-130/20
75-69-4 Trichlorofluoromethane ND 100 93.9 94 100 109 109 15 60-140/20
96-18-4 1,2,3-Trichloropropane ND 100 77.4 77 100 92.9 93 18 70-130/20
95-63-6 1,2,4-Trimethylbenzene 90.1 100 139 49*100 171 81 21*70-130/20
108-67-8 1,3,5-Trimethylbenzene 97.0 100 143 46*100 175 78 20 70-130/20
75-01-4 Vinyl Chloride ND 100 89.5 90 100 108 108 19 60-140/20
m,p-Xylene 129 200 253 62*200 307 89 19 70-130/20
95-47-6 o-Xylene 80.4 100 141 61*100 172 92 20 70-130/20
1330-20-7 Xylene (total)210 300 394 61*300 479 90 19 70-130/20
CAS No.Surrogate Recoveries MS MSD FA21825-1 Limits
1868-53-7 Dibromofluoromethane 102%101%98%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%102%102%70-130%
2037-26-5 Toluene-D8 100%102%101%70-130%
460-00-4 4-Bromofluorobenzene 99%101%106%70-130%
* = Outside of Control Limits.
78 of 84
FA21787 55.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA21787
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA21787-4MS E036178.D 100 02/03/15 TD n/a n/a VE1204
FA21787-4MSD E036179.D 100 02/03/15 TD n/a n/a VE1204
FA21787-4 E036166.D 100 02/03/15 TD n/a n/a VE1204
The QC reported here applies to the following samples:Method: SM 6200B
FA21787-1, FA21787-3, FA21787-4, FA21787-5, FA21787-6
FA21787-4 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 170 1000 877 71 1000 858 69*2 70-130/20
108-86-1 Bromobenzene ND 1000 706 71 1000 685 69*3 70-130/20
74-97-5 Bromochloromethane ND 1000 705 71 1000 689 69*2 70-130/20
75-27-4 Bromodichloromethane ND 1000 703 70 1000 648 65*8 70-130/20
75-25-2 Bromoform ND 1000 499 50*1000 469 47*6 70-130/20
104-51-8 n-Butylbenzene 121 1000 745 62*1000 710 59*5 70-130/20
135-98-8 sec-Butylbenzene 64.0 1000 856 79 1000 817 75 5 70-130/20
98-06-6 tert-Butylbenzene ND 1000 792 79 1000 760 76 4 70-130/20
56-23-5 Carbon Tetrachloride ND 1000 852 85 1000 773 77 10 70-130/20
108-90-7 Chlorobenzene ND 1000 754 75 1000 740 74 2 70-130/20
75-00-3 Chloroethane ND 1000 818 82 1000 757 76 8 60-140/20
67-66-3 Chloroform ND 1000 767 77 1000 748 75 3 70-130/20
95-49-8 o-Chlorotoluene ND 1000 853 85 1000 818 82 4 70-130/20
106-43-4 p-Chlorotoluene ND 1000 780 78 1000 751 75 4 70-130/20
124-48-1 Dibromochloromethane ND 1000 594 59*1000 549 55*8 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 1000 681 68*1000 653 65*4 70-130/20
106-93-4 1,2-Dibromoethane ND 1000 724 72 1000 712 71 2 70-130/20
75-71-8 Dichlorodifluoromethane ND 1000 978 98 1000 923 92 6 60-140/20
95-50-1 1,2-Dichlorobenzene ND 1000 751 75 1000 734 73 2 70-130/20
541-73-1 1,3-Dichlorobenzene ND 1000 776 78 1000 753 75 3 70-130/20
106-46-7 1,4-Dichlorobenzene ND 1000 702 70 1000 680 68*3 70-130/20
75-34-3 1,1-Dichloroethane ND 1000 720 72 1000 707 71 2 70-130/20
107-06-2 1,2-Dichloroethane ND 1000 741 74 1000 724 72 2 70-130/20
75-35-4 1,1-Dichloroethylene ND 1000 828 83 1000 795 80 4 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 1000 728 73 1000 720 72 1 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 1000 742 74 1000 711 71 4 70-130/20
78-87-5 1,2-Dichloropropane ND 1000 740 74 1000 722 72 2 70-130/20
142-28-9 1,3-Dichloropropane ND 1000 712 71 1000 708 71 1 70-130/20
594-20-7 2,2-Dichloropropane ND 1000 784 78 1000 761 76 3 70-130/20
563-58-6 1,1-Dichloropropene ND 1000 810 81 1000 774 77 5 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 1000 685 69*1000 613 61*11 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 1000 712 71 1000 645 65*10 70-130/20
108-20-3 Di-Isopropyl Ether ND 1000 718 72 1000 707 71 2 70-130/20
100-41-4 Ethylbenzene 1170 1000 1720 55*1000 1680 51*2 70-130/20
87-68-3 Hexachlorobutadiene ND 1000 707 71 1000 688 69*3 70-130/20
98-82-8 Isopropylbenzene 125 1000 799 67*1000 782 66*2 70-130/20
* = Outside of Control Limits.
79 of 84
FA21787 55.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA21787
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA21787-4MS E036178.D 100 02/03/15 TD n/a n/a VE1204
FA21787-4MSD E036179.D 100 02/03/15 TD n/a n/a VE1204
FA21787-4 E036166.D 100 02/03/15 TD n/a n/a VE1204
The QC reported here applies to the following samples:Method: SM 6200B
FA21787-1, FA21787-3, FA21787-4, FA21787-5, FA21787-6
FA21787-4 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene 28.7 J 1000 691 66*1000 664 64*4 70-130/20
74-83-9 Methyl Bromide ND 1000 795 80 1000 767 77 4 60-140/20
74-87-3 Methyl Chloride ND 1000 883 88 1000 882 88 0 60-140/20
74-95-3 Methylene Bromide ND 1000 753 75 1000 727 73 4 70-130/20
75-09-2 Methylene Chloride ND 1000 684 68*1000 663 66*3 70-130/20
1634-04-4 Methyl Tert Butyl Ether 238 1000 923 69*1000 912 67*1 70-130/20
91-20-3 Naphthalene 496 1000 1150 65*1000 1120 62*3 70-130/20
103-65-1 n-Propylbenzene 592 1000 1260 67*1000 1200 61*5 70-130/20
100-42-5 Styrene ND 1000 652 65*1000 649 65*0 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 1000 720 72 1000 694 69*4 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 1000 692 69*1000 666 67*4 70-130/20
127-18-4 Tetrachloroethylene ND 1000 738 74 1000 721 72 2 70-130/20
108-88-3 Toluene 1930 1000 2420 49*1000 2370 44*2 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 1000 668 67*1000 673 67*1 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 1000 672 67*1000 680 68*1 70-130/20
71-55-6 1,1,1-Trichloroethane ND 1000 740 74 1000 709 71 4 70-130/20
79-00-5 1,1,2-Trichloroethane ND 1000 748 75 1000 753 75 1 70-130/20
79-01-6 Trichloroethylene ND 1000 767 77 1000 743 74 3 70-130/20
75-69-4 Trichlorofluoromethane ND 1000 949 95 1000 878 88 8 60-140/20
96-18-4 1,2,3-Trichloropropane ND 1000 694 69*1000 681 68*2 70-130/20
95-63-6 1,2,4-Trimethylbenzene 3230 1000 3130 -10* a 1000 3020 -21* a 4 70-130/20
108-67-8 1,3,5-Trimethylbenzene 1140 1000 1650 51*1000 1590 45*4 70-130/20
75-01-4 Vinyl Chloride ND 1000 867 87 1000 855 86 1 60-140/20
m,p-Xylene 4510 2000 5270 38* a 2000 5160 33* a 2 70-130/20
95-47-6 o-Xylene 1650 1000 2210 56*1000 2160 51*2 70-130/20
1330-20-7 Xylene (total)6160 3000 7480 44* a 3000 7320 39* a 2 70-130/20
CAS No.Surrogate Recoveries MS MSD FA21787-4 Limits
1868-53-7 Dibromofluoromethane 99%98%96%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%104%101%70-130%
2037-26-5 Toluene-D8 98%99%99%70-130%
460-00-4 4-Bromofluorobenzene 100%98%101%70-130%
(a) Outside control limits due to high level in sample relative to spike amount.
* = Outside of Control Limits.
80 of 84
FA21787 55.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA21787
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA21787-20MS E036207.D 1 02/04/15 TD n/a n/a VE1205
FA21787-20MSD E036208.D 1 02/04/15 TD n/a n/a VE1205
FA21787-20 E036200.D 1 02/04/15 TD n/a n/a VE1205
The QC reported here applies to the following samples:Method: SM 6200B
FA21787-17, FA21787-18, FA21787-19, FA21787-20, FA21787-21, FA21787-22
FA21787-20 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene ND 10 7.9 79 10 7.8 78 1 70-130/20
108-86-1 Bromobenzene ND 10 7.5 75 10 7.4 74 1 70-130/20
74-97-5 Bromochloromethane ND 10 7.9 79 10 7.9 79 0 70-130/20
75-27-4 Bromodichloromethane ND 10 7.9 79 10 7.8 78 1 70-130/20
75-25-2 Bromoform ND 10 7.1 71 10 7.1 71 0 70-130/20
104-51-8 n-Butylbenzene ND 10 6.9 69*10 6.8 68*1 70-130/20
135-98-8 sec-Butylbenzene ND 10 7.7 77 10 7.6 76 1 70-130/20
98-06-6 tert-Butylbenzene ND 10 7.6 76 10 7.5 75 1 70-130/20
56-23-5 Carbon Tetrachloride ND 10 9.2 92 10 9.1 91 1 70-130/20
108-90-7 Chlorobenzene ND 10 7.5 75 10 7.4 74 1 70-130/20
75-00-3 Chloroethane ND 10 9.5 95 10 9.1 91 4 60-140/20
67-66-3 Chloroform ND 10 7.8 78 10 7.8 78 0 70-130/20
95-49-8 o-Chlorotoluene ND 10 7.6 76 10 7.5 75 1 70-130/20
106-43-4 p-Chlorotoluene ND 10 7.6 76 10 7.6 76 0 70-130/20
124-48-1 Dibromochloromethane ND 10 7.2 72 10 7.1 71 1 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 10 7.2 72 10 7.2 72 0 70-130/20
106-93-4 1,2-Dibromoethane ND 10 7.7 77 10 7.8 78 1 70-130/20
75-71-8 Dichlorodifluoromethane ND 10 10.7 107 10 10.4 104 3 60-140/20
95-50-1 1,2-Dichlorobenzene ND 10 7.4 74 10 7.4 74 0 70-130/20
541-73-1 1,3-Dichlorobenzene ND 10 7.5 75 10 7.4 74 1 70-130/20
106-46-7 1,4-Dichlorobenzene ND 10 7.4 74 10 7.3 73 1 70-130/20
75-34-3 1,1-Dichloroethane ND 10 7.9 79 10 7.8 78 1 70-130/20
107-06-2 1,2-Dichloroethane ND 10 7.9 79 10 8.0 80 1 70-130/20
75-35-4 1,1-Dichloroethylene ND 10 8.4 84 10 8.1 81 4 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 10 7.8 78 10 7.7 77 1 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 10 8.0 80 10 7.9 79 1 70-130/20
78-87-5 1,2-Dichloropropane ND 10 7.8 78 10 7.9 79 1 70-130/20
142-28-9 1,3-Dichloropropane ND 10 7.7 77 10 7.6 76 1 70-130/20
594-20-7 2,2-Dichloropropane ND 10 8.5 85 10 8.3 83 2 70-130/20
563-58-6 1,1-Dichloropropene ND 10 8.1 81 10 8.0 80 1 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 10 8.0 80 10 8.0 80 0 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 10 7.9 79 10 7.8 78 1 70-130/20
108-20-3 Di-Isopropyl Ether ND 10 8.2 82 10 8.2 82 0 70-130/20
100-41-4 Ethylbenzene ND 10 7.9 79 10 7.7 77 3 70-130/20
87-68-3 Hexachlorobutadiene ND 10 7.3 73 10 7.1 71 3 70-130/20
98-82-8 Isopropylbenzene ND 10 6.8 68*10 6.6 66*3 70-130/20
* = Outside of Control Limits.
81 of 84
FA21787 55.3.3
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA21787
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA21787-20MS E036207.D 1 02/04/15 TD n/a n/a VE1205
FA21787-20MSD E036208.D 1 02/04/15 TD n/a n/a VE1205
FA21787-20 E036200.D 1 02/04/15 TD n/a n/a VE1205
The QC reported here applies to the following samples:Method: SM 6200B
FA21787-17, FA21787-18, FA21787-19, FA21787-20, FA21787-21, FA21787-22
FA21787-20 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 10 6.5 65*10 6.4 64*2 70-130/20
74-83-9 Methyl Bromide ND 10 9.2 92 10 8.8 88 4 60-140/20
74-87-3 Methyl Chloride ND 10 10 100 10 9.8 98 2 60-140/20
74-95-3 Methylene Bromide ND 10 7.8 78 10 7.9 79 1 70-130/20
75-09-2 Methylene Chloride ND 10 7.2 72 10 7.1 71 1 70-130/20
1634-04-4 Methyl Tert Butyl Ether 0.27 J 10 8.3 80 10 8.5 82 2 70-130/20
91-20-3 Naphthalene ND 10 7.6 76 10 7.6 76 0 70-130/20
103-65-1 n-Propylbenzene ND 10 7.7 77 10 7.6 76 1 70-130/20
100-42-5 Styrene ND 10 7.1 71 10 7.0 70 1 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 10 7.7 77 10 7.6 76 1 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 10 7.5 75 10 7.6 76 1 70-130/20
127-18-4 Tetrachloroethylene ND 10 7.8 78 10 7.6 76 3 70-130/20
108-88-3 Toluene ND 10 7.7 77 10 7.5 75 3 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 10 7.2 72 10 7.2 72 0 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 10 7.3 73 10 7.2 72 1 70-130/20
71-55-6 1,1,1-Trichloroethane ND 10 8.0 80 10 7.9 79 1 70-130/20
79-00-5 1,1,2-Trichloroethane ND 10 7.7 77 10 7.6 76 1 70-130/20
79-01-6 Trichloroethylene ND 10 7.8 78 10 7.7 77 1 70-130/20
75-69-4 Trichlorofluoromethane ND 10 10.1 101 10 10.0 100 1 60-140/20
96-18-4 1,2,3-Trichloropropane ND 10 7.6 76 10 7.6 76 0 70-130/20
95-63-6 1,2,4-Trimethylbenzene ND 10 7.6 76 10 7.6 76 0 70-130/20
108-67-8 1,3,5-Trimethylbenzene ND 10 9.1 91 10 9.0 90 1 70-130/20
75-01-4 Vinyl Chloride ND 10 10.3 103 10 10.1 101 2 60-140/20
m,p-Xylene ND 20 15.9 80 20 15.6 78 2 70-130/20
95-47-6 o-Xylene ND 10 7.8 78 10 7.7 77 1 70-130/20
1330-20-7 Xylene (total)ND 30 23.8 79 30 23.4 78 2 70-130/20
CAS No.Surrogate Recoveries MS MSD FA21787-20 Limits
1868-53-7 Dibromofluoromethane 99%99%99%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%100%103%70-130%
2037-26-5 Toluene-D8 98%97%99%70-130%
460-00-4 4-Bromofluorobenzene 99%98%101%70-130%
* = Outside of Control Limits.
82 of 84
FA21787 55.3.3
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA21787
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA21787-2MS A0192098.D 100 02/04/15 TD n/a n/a VA1632
FA21787-2MSD A0192099.D 100 02/04/15 TD n/a n/a VA1632
FA21787-2 A0192086.D 100 02/04/15 TD n/a n/a VA1632
The QC reported here applies to the following samples:Method: SM 6200B
FA21787-2, FA21787-7, FA21787-8, FA21787-9, FA21787-10, FA21787-11, FA21787-12, FA21787-13, FA21787-14,
FA21787-15, FA21787-16
FA21787-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 4350 1000 5490 114 1000 5790 144* a 5 70-130/20
108-86-1 Bromobenzene ND 1000 1050 105 1000 1130 113 7 70-130/20
74-97-5 Bromochloromethane ND 1000 1050 105 1000 1100 110 5 70-130/20
75-27-4 Bromodichloromethane ND 1000 1100 110 1000 1130 113 3 70-130/20
75-25-2 Bromoform ND 1000 973 97 1000 977 98 0 70-130/20
104-51-8 n-Butylbenzene 35.2 J 1000 1120 108 1000 1220 118 9 70-130/20
135-98-8 sec-Butylbenzene 21.6 J 1000 1170 115 1000 1300 128 11 70-130/20
98-06-6 tert-Butylbenzene ND 1000 1130 113 1000 1250 125 10 70-130/20
56-23-5 Carbon Tetrachloride ND 1000 1090 109 1000 1150 115 5 70-130/20
108-90-7 Chlorobenzene ND 1000 1120 112 1000 1180 118 5 70-130/20
75-00-3 Chloroethane ND 1000 884 88 1000 858 86 3 60-140/20
67-66-3 Chloroform ND 1000 1110 111 1000 1150 115 4 70-130/20
95-49-8 o-Chlorotoluene ND 1000 1200 120 1000 1290 129 7 70-130/20
106-43-4 p-Chlorotoluene ND 1000 1160 116 1000 1260 126 8 70-130/20
124-48-1 Dibromochloromethane ND 1000 1050 105 1000 1090 109 4 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 1000 1110 111 1000 1110 111 0 70-130/20
106-93-4 1,2-Dibromoethane ND 1000 1100 110 1000 1140 114 4 70-130/20
75-71-8 Dichlorodifluoromethane ND 1000 871 87 1000 914 91 5 60-140/20
95-50-1 1,2-Dichlorobenzene ND 1000 1160 116 1000 1230 123 6 70-130/20
541-73-1 1,3-Dichlorobenzene ND 1000 1180 118 1000 1250 125 6 70-130/20
106-46-7 1,4-Dichlorobenzene ND 1000 1070 107 1000 1140 114 6 70-130/20
75-34-3 1,1-Dichloroethane ND 1000 1040 104 1000 1100 110 6 70-130/20
107-06-2 1,2-Dichloroethane 79.6 1000 1210 113 1000 1270 119 5 70-130/20
75-35-4 1,1-Dichloroethylene ND 1000 1100 110 1000 1150 115 4 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 1000 1070 107 1000 1120 112 5 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 1000 1040 104 1000 1080 108 4 70-130/20
78-87-5 1,2-Dichloropropane ND 1000 1070 107 1000 1120 112 5 70-130/20
142-28-9 1,3-Dichloropropane ND 1000 1070 107 1000 1140 114 6 70-130/20
594-20-7 2,2-Dichloropropane ND 1000 1020 102 1000 1070 107 5 70-130/20
563-58-6 1,1-Dichloropropene ND 1000 1130 113 1000 1200 120 6 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 1000 994 99 1000 1060 106 6 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 1000 1130 113 1000 1160 116 3 70-130/20
108-20-3 Di-Isopropyl Ether 29.9 J 1000 1040 101 1000 1110 108 7 70-130/20
100-41-4 Ethylbenzene 1360 1000 2440 108 1000 2600 124 6 70-130/20
87-68-3 Hexachlorobutadiene ND 1000 1060 106 1000 1110 111 5 70-130/20
98-82-8 Isopropylbenzene 99.5 1000 1260 116 1000 1360 126 8 70-130/20
* = Outside of Control Limits.
83 of 84
FA21787 55.3.4
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA21787
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA21787-2MS A0192098.D 100 02/04/15 TD n/a n/a VA1632
FA21787-2MSD A0192099.D 100 02/04/15 TD n/a n/a VA1632
FA21787-2 A0192086.D 100 02/04/15 TD n/a n/a VA1632
The QC reported here applies to the following samples:Method: SM 6200B
FA21787-2, FA21787-7, FA21787-8, FA21787-9, FA21787-10, FA21787-11, FA21787-12, FA21787-13, FA21787-14,
FA21787-15, FA21787-16
FA21787-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene 16.2 J 1000 1140 112 1000 1260 124 10 70-130/20
74-83-9 Methyl Bromide ND 1000 963 96 1000 973 97 1 60-140/20
74-87-3 Methyl Chloride ND 1000 1010 101 1000 1050 105 4 60-140/20
74-95-3 Methylene Bromide ND 1000 1100 110 1000 1130 113 3 70-130/20
75-09-2 Methylene Chloride ND 1000 1200 120 1000 1250 125 4 70-130/20
1634-04-4 Methyl Tert Butyl Ether 739 1000 1770 103 1000 1860 112 5 70-130/20
91-20-3 Naphthalene 555 1000 1660 111 1000 1760 121 6 70-130/20
103-65-1 n-Propylbenzene 285 1000 1440 116 1000 1580 130 9 70-130/20
100-42-5 Styrene ND 1000 1050 105 1000 1120 112 6 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 1000 1090 109 1000 1150 115 5 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 1000 1040 104 1000 1120 112 7 70-130/20
127-18-4 Tetrachloroethylene ND 1000 1070 107 1000 1130 113 5 70-130/20
108-88-3 Toluene 3670 1000 4690 102 1000 4950 128 5 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 1000 1030 103 1000 1120 112 8 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 1000 1060 106 1000 1150 115 8 70-130/20
71-55-6 1,1,1-Trichloroethane ND 1000 1070 107 1000 1120 112 5 70-130/20
79-00-5 1,1,2-Trichloroethane ND 1000 1140 114 1000 1180 118 3 70-130/20
79-01-6 Trichloroethylene ND 1000 1100 110 1000 1140 114 4 70-130/20
75-69-4 Trichlorofluoromethane ND 1000 987 99 1000 1020 102 3 60-140/20
96-18-4 1,2,3-Trichloropropane ND 1000 1090 109 1000 1170 117 7 70-130/20
95-63-6 1,2,4-Trimethylbenzene 2010 1000 3040 103 1000 3310 130 9 70-130/20
108-67-8 1,3,5-Trimethylbenzene 597 1000 1640 104 1000 1790 119 9 70-130/20
75-01-4 Vinyl Chloride ND 1000 915 92 1000 973 97 6 60-140/20
m,p-Xylene 4660 2000 6860 110 2000 7310 133* a 6 70-130/20
95-47-6 o-Xylene 2470 1000 3650 118 1000 3900 143* a 7 70-130/20
1330-20-7 Xylene (total)7130 3000 10500 112 3000 11200 136* a 6 70-130/20
CAS No.Surrogate Recoveries MS MSD FA21787-2 Limits
1868-53-7 Dibromofluoromethane 103%102%99%70-130%
17060-07-0 1,2-Dichloroethane-D4 105%103%105%70-130%
2037-26-5 Toluene-D8 101%100%99%70-130%
460-00-4 4-Bromofluorobenzene 99%99%101%70-130%
(a) Outside control limits due to high level in sample relative to spike amount.
* = Outside of Control Limits.
84 of 84
FA21787 55.3.4

APPENDIX B
Graphs of Individual VOC Concentrations vs. Time

APPENDIX B
SUMMARY OF GROUND WATER QUALITY DATA
RED APPLE MARKET #21
Date Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene
MAC 1 600 600 500 20 6
01/18/07 46.4 5.51 58.8 28.72 25.7 34.3
06/06/07 68.3 4.56 85.7 32.6 21.6 43.9
06/02/08 16.5 1.20 21.2 8.35 38.5 9.23
12/18/08 13 <0.50 10 4.9 14 5.9
03/24/09 44 15 40 23 16 19
06/25/09 6.32 <0.330 7.99 <1.33 10.5 3.14
09/21/09 18.5 <0.190 9.24 1.30 12.7 3.10
12/30/09 26.1 2.13 5.26 3.14 15.1 3.51
06/28/10 20.1 0.62 12.2 2.51 11.4 7.66
10/05/10 32.6 2.78 16.0 8.47 8.91 5.69
10/12/11 <0.13 <0.13 <0.15 <0.30 2.1 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 1.2 <0.10
05/15/12 <0.13 <0.13 <0.15 <0.30 0.16 <0.10
01/22/13 <0.10 <0.10 <0.10 <0.22 1.0 <0.15
11/18/13 <0.10 <0.10 <0.10 <0.22 1.1 <0.15
05/27/14 <0.10 <0.10 <0.10 <0.20 1.0 <0.10
01/29/15 <0.17 <0.17 <0.15 <0.43 0.80 <0.12
Date Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene
MAC 1 600 600 500 20 6
01/18/07 FP FP FP FP FP FP
06/06/07 FP FP FP FP FP FP
06/02/08 FP FP FP FP FP FP
12/18/08 FP FP FP FP FP FP
03/24/09 FP FP FP FP FP FP
06/25/09 FP FP FP FP FP FP
09/21/09 FP FP FP FP FP FP
12/30/09 FP FP FP FP FP FP
06/28/10 FP FP FP FP FP FP
10/05/10 FP FP FP FP FP FP
10/12/11 9,780 9,700 2,440 10,100 1,220 769
01/31/12 FP FP FP FP FP FP
05/15/12 FP FP FP FP FP FP
01/22/13 3,250 7,990 2,070 11,900 519 2,020
11/18/13 6,580 7,930 2,100 13,800 731 841
05/27/14 4,160 4,880 1,400 10,500 657 758
01/29/15 4,350 3,670 1,360 7,130 739 555
Date Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene
MAC 1 600 600 500 20 6
01/18/07 1,940 5.14 34.3 <15.0 3,800 <25.0
06/06/07 3,030 6.18 69.0 7.61 4,880 40.3
06/02/08 2,500 4.95 126 14.2 5,490 60.8
12/18/08 1,700 2.1 33 2.6 4,200 24
03/24/09 2,900 <16 110 140 4,900 69
06/25/09 2,140 10.3 56.4 32.9 4,110 40
09/21/09 2,180 <7.60 56.2 <8.80 5,040 69.3
12/30/09 1,580 2.29 41.1 <1.10 4,200 23.3
06/28/10 1,780 <9.50 54.0 <11.0 5,040 26.2
10/05/10 1,830 <9.50 47.8 <11.0 4,010 <25.0
10/12/11 3.4 6.1 1.7 6.2 0.36 0.46
01/31/12 36.6 2.9 17.9 28.4 6.2 0.21
05/15/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10
01/22/13 22.1 2.1 19.1 16.2 8.1 0.68
11/18/13 12.6 1.4 17.1 14.0 5.9 1.2
05/27/14 4.2 <0.10 0.85 0.74 J 5.9 0.27
01/29/15 3.8 0.28 4.7 0.68 6.5 0.18
Date Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene
MAC 1 600 600 500 20 6
01/18/07 14,900 5,650 1,330 4,850 16,100 436
06/14/07 15,000 8,240 1,710 6,330 14,300 489
06/02/08 NS NS NS NS NS NS
10/12/11 FP FP FP FP FP FP
01/31/12 FP FP FP FP FP FP
05/15/12 FP FP FP FP FP FP
01/22/13 FP FP FP FP FP FP
11/18/13 FP FP FP FP FP FP
05/27/14 792 3,720 1,160 5,660 604 550.0
01/29/15 170 1,930 1,170 6,160 238 496
MW-1/MW-1R
MW-2/MW-2R
MW-3/MW-3R
MW-4/MW-4R
Note:
Concentrations in mg/L.Page 1 of 2
APPENDIX B
SUMMARY OF GROUND WATER QUALITY DATA
RED APPLE MARKET #21
Date Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene
MAC 1 600 600 500 20 6
01/18/07 1,040 76.6 116 109.4 836 348
06/06/07 1,350 90.1 143 119 1,300 105
06/02/08 NS NS NS NS NS NS
12/18/08 NS NS NS NS NS NS
03/24/09 NS NS NS NS NS NS
06/25/09 NS NS NS NS NS NS
09/21/09 403 2.25 40.9 37.3 195 61.5
12/30/09 676 7.35 35.7 12.3 255 43.4
06/28/10 817 12.60 66.7 55.9 347 54.1
10/05/10 308 <19.0 41.1 23.0 193 108
10/12/11 FP FP FP FP FP FP
01/31/12 40.6 2.7 61.4 25.6 156 42.6
05/15/12 871 18.2 134 214.8 93.4 87.5
01/22/13 143 14.6 114 225 184 128
11/18/13 34.4 0.45 22.7 1.8 99.2 47.3
05/27/14 145 7.8 114 39.9 247 60.7
01/29/15 65.8 2.4 28.2 1.5 117 20.1
MW-9
Date Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene
MAC 1 600 600 500 20 6
01/18/07 53.6 1.48 27.4 56.3 3.67 18.3
06/06/07 56.8 0.960 24.2 53.8 0.690 14.3
06/02/08 33.6 0.640 21.7 9.07 2.18 20.5
12/18/08 40 1.600 27 18 <0.50 22
03/24/09 68 <1.6 37 23 2.0 28
06/25/09 53.4 0.929 15.9 20.7 1.04 19.5
09/21/09 50.7 0.952 25.7 18.5 1.85 23.2
12/30/09 71.9 0.903 28.4 16.8 <0.250 21.9
06/28/10 66.1 <0.950 22.5 15.2 <1.25 19.0
10/05/10 72.6 3.54 74.2 110 <0.250 33.7
10/12/11 37.3 0.41 8.2 12.2 0.92 17.3
01/31/12 54.7 0.78 25.0 21.6 1.5 24.1
05/15/12 65.9 0.58 15.7 15.0 1.3 15.9
01/22/13 73.7 2.3 13.9 74.7 0.43 13.6
11/18/13 183 3.9 53.5 153 0.91 40.4
05/27/14 227 3.7 60.4 158 1.5 44.1
01/29/15 162 1.7 36.1 71.5 1.3 32.6
MW-5/MW-5R
Note:
Concentrations in mg/L.Page 2 of 2
0
100
200
300
400
500
600
700
MAC 01/18/07 06/06/07 06/02/08 12/18/08 03/24/09 06/25/09 09/21/09 12/30/09 06/28/10 10/05/10 10/12/11 01/31/12 05/15/12 01/22/13 11/18/13 05/27/14 01/29/15Concentration (ug/L)Sample Date
Ground Water Quality Chart -MW-1/MW-1R
Red Apple Market #21
Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene
0
2000
4000
6000
8000
10000
12000
14000
16000
MAC 01/18/07 06/06/07 06/02/08 12/18/08 03/24/09 06/25/09 09/21/09 12/30/09 06/28/10 10/05/10 10/12/11 01/31/12 05/15/12 01/22/13 11/18/13 05/27/14 01/29/15Concentration (ug/L)Sample Date
Ground Water Quality Chart -MW-2/MW-2R
Red Apple Market #21
Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene
3.54 ft.
FP
0.69 ft.
FP
2.27 ft.
FP
0.69 ft.
FP
0.23 ft.
FP
3.25 ft.
FP
0.46 ft.
FP
0.03 ft.
FP
0.33 ft.
FP
2.79 ft.
FP
2.04 ft.
FP
0.22 ft.
FP
0
1000
2000
3000
4000
5000
6000
MAC 01/18/07 06/06/07 06/02/08 12/18/08 03/24/09 06/25/09 09/21/09 12/30/09 06/28/10 10/05/10 10/12/11 01/31/12 05/15/12 01/22/13 11/18/13 05/27/14 01/29/15Concentration (ug/L)Sample Date
Ground Water Quality Chart -MW-3/MW-3R
Red Apple Market #21
Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene
0
2000
4000
6000
8000
10000
12000
14000
16000
18000
MAC 01/18/07 06/14/07 06/02/08 10/12/11 01/31/12 05/15/12 01/22/13 11/18/13 05/27/14 01/29/15Concentration (ug/L)Sample Date
Ground Water Quality Chart -MW-4/MW-4R
Red Apple Market #21
Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene
0.13 ft.
FPNS 0.29 ft.
FP
0.51 ft.
FP
0.30 ft.
FP
0.01 ft.
FP
0
200
400
600
800
1000
1200
1400
1600
MAC 01/18/07 06/06/07 06/02/08 12/18/08 03/24/09 06/25/09 09/21/09 12/30/09 06/28/10 10/05/10 10/12/11 01/31/12 05/15/12 01/22/13 11/18/13 05/27/14 01/29/15Concentration (ug/L)Sample Date
Ground Water Quality Chart -MW-5/MW-5R
Red Apple Market #21
Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene
NS NS NS NS 0.02 ft.
FP
0
100
200
300
400
500
600
700
MAC 01/18/07 06/06/07 06/02/08 12/18/08 03/24/09 06/25/09 09/21/09 12/30/09 06/28/10 10/05/10 10/12/11 01/31/12 05/15/12 01/22/13 11/18/13 05/27/14 01/29/15Concentration (ug/L)Sample Date
Ground Water Quality Chart -MW-9
Red Apple Market #21
Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene

APPENDIX C
Graphs of Total VOC Concentrations vs. Depths to Ground Water

APPENDIX C
TOTAL VOC'S vs DEPTH TO WATER
RED APPLE MARKET #21
TOTAL VOC'S INCLUDE BTEX, MTBE AND NAPHTHALENE
MW-1/1R
Date Total VOC's Depth to Water
01/18/07 199.43 12.87
06/06/07 256.66 13.15
06/02/08 94.98 14.10
12/18/08 41.90 16.41
03/24/09 157.00 14.62
06/25/09 27.95 15.00
09/21/09 44.84 15.66
12/30/09 55.24 14.85
06/28/10 54.488 14.02
10/05/10 74.45 14.74
10/12/11 2.1 15.73
01/31/12 1.2 15.71
05/15/12 0.16 14.77
01/22/13 1 14.68
11/18/13 1.1 15.84
05/27/14 1 14.36
01/29/15 0.8 14.53
MW-2/2R
Date Total VOC's Depth to Water
01/18/07 FP 14.81
06/06/07 FP 13.07
06/02/08 FP 15.20
12/18/08 FP 15.25
03/24/09 FP 16.90
06/25/09 FP 14.90
09/21/09 FP 15.07
12/30/09 FP 14.65
06/28/10 FP 15.65
10/05/10 FP 15.81
10/12/11 34,009 14.71
01/31/12 FP 14.67
05/15/12 FP 13.96
01/22/13 27,749 13.85
11/18/13 31,982 14.95
05/27/14 22,355 13.71
01/29/15 17,804 13.86
MW-3/3R
Date Total VOC's Depth to Water
01/18/07 5,779.44 14.02
06/06/07 8,033.09 13.86
06/02/08 8195.95 14.77
12/18/08 5937.70 16.27
03/24/09 8,050.00 15.90
06/25/09 6,349.60 15.80
09/21/09 7,345.50 16.40
12/30/09 5,846.69 13.97
06/28/10 6,900.20 15.76
10/05/10 5,887.80 15.50
10/12/11 18.22 14.48
01/31/12 92.21 15.88
05/15/12 0.00 14.31
01/22/13 68.28 15.09
11/18/13 52.20 16.48
05/27/14 11.22 16.74
01/29/15 16.14 14.62
Note:
Concentrations in mg/L; Depths to water reported in feet.Page 1 of 2
APPENDIX C
TOTAL VOC'S vs DEPTH TO WATER
RED APPLE MARKET #21
TOTAL VOC'S INCLUDE BTEX, MTBE AND NAPHTHALENE
MW-4/4R
Date Total VOC's Depth to Water
01/18/07 43266 12.69
06/14/07 46069 13.06
06/02/08 0.00 NM
10/12/11 0.00 13.28
01/31/12 0.00 13.12
05/15/12 0.00 14.13
01/22/13 0.00 14.22
11/18/13 0.00 14.86
05/27/14 12,486.00 13.58
01/29/15 10,164.00 14.15
MW-5/5R
Date Total VOC's Depth to Water
01/18/07 2,526.0 13.02
06/06/07 3,107.10 13.23
06/02/08 0.00 NM
12/18/08 0.00 NM
03/24/09 0.00 NM
06/25/09 0.00 NM
09/21/09 739.95 15.47
12/30/09 1,029.75 14.44
06/28/10 1,353.30 13.99
10/05/10 673.10 14.60
10/12/11 0.00 14.16
01/31/12 328.90 15.36
05/15/12 1,418.90 14.20
01/22/13 808.60 14.45
11/18/13 205.85 15.44
05/27/14 614.40 13.98
01/29/15 235.00 14.20
MW-9
Date Total VOC's Depth to Water
01/18/07 160.75 7.73
06/06/07 150.75 9.35
06/02/08 87.69 8.21
12/18/08 86.60 11.72
03/24/09 158.00 11.60
06/25/09 111.47 11.73
09/21/09 120.90 12.62
12/30/09 139.90 12.24
06/28/10 122.80 12.40
10/05/10 294.04 12.69
10/12/11 76.33 10.00
01/31/12 127.68 10.59
05/15/12 114.38 9.94
01/22/13 178.63 5.34
11/18/13 434.71 11.49
05/27/14 494.70 9.64
01/29/15 305.20 10.94
Note:
Concentrations in mg/L; Depths to water reported in feet.Page 2 of 2
0.00
2.00
4.00
6.00
8.00
10.00
12.00
14.00
16.00
18.00
0
50
100
150
200
250
300
Depth to Water (ft.)Total VOC's Concentration (ug/L)Sample Date
Ground Water Quality vs. Depth to Water
Red Apple Market #21 -MW-1/MW-1R
Total VOC's
Depth to Water
0.00
2.00
4.00
6.00
8.00
10.00
12.00
14.00
16.00
18.00
0
5,000
10,000
15,000
20,000
25,000
30,000
35,000
40,000
Depth to Water (ft.)Total VOC's Concentration (ug/L)Sample Date
Ground Water Quality vs. Depth to Water
Red Apple Market #21 -MW-2MW-/2R
Total VOC's
Depth to Water
FPFPFPFPFPFPFPFP FP FP FPFP
0.00
2.00
4.00
6.00
8.00
10.00
12.00
14.00
16.00
18.00
0
1,000
2,000
3,000
4,000
5,000
6,000
7,000
8,000
9,000
Depth to Water (ft.)Total VOC's Concentration (ug/L)Sample Date
Ground Water Quality vs. Depth to Water
Red Apple Market #21 -MW-3/MW-3R
Total VOC's
Depth to Water
0.00
2.00
4.00
6.00
8.00
10.00
12.00
14.00
16.00
0
5,000
10,000
15,000
20,000
25,000
30,000
35,000
40,000
45,000
50,000
Depth to Water (ft.)Total VOC's Concentration (ug/L)Sample Date
Ground Water Quality vs. Depth to Water
Red Apple Market #21 -MW-4/MW-4R
Total VOC's
Depth to Water
NS FP FP FP FP FP
0.00
2.00
4.00
6.00
8.00
10.00
12.00
14.00
16.00
18.00
0
500
1,000
1,500
2,000
2,500
3,000
3,500
Depth to Water (ft.)Total VOC's Concentration (ug/L)Sample Date
Ground Water Quality vs. Depth to Water
Red Apple Market #21 -MW5
Total VOC's
Depth to Water
NS NS NS NS FP
0.00
2.00
4.00
6.00
8.00
10.00
12.00
14.00
0
100
200
300
400
500
600
Depth to Water (ft.)Total VOC's Concentration (ug/L)Sample Date
Ground Water Quality vs. Depth to Water
Red Apple Market #21 -MW9
Total VOC's
Depth to Water