WA-649_9420_CA_RPTS_20180222_MRP

EXECUTIVE SUMMARY

The Myers Grocery and White’s Cross Grocery sites are located at 1901 and 1906 Wakelon Road in
Colerain, Bertie County, North Carolina. According to available information, two 2,000 gallon gasoline
USTs were removed from the Myers Grocery site in September 1992. One 4,000-gallon gasoline UST,
one 2,000-gallon gasoline UST, one 1,000-gallon gasoline UST and one 4,000-gallon diesel UST were
removed from the White’s Cross Grocery site in February 1994. In addition, one 1,000-gallon kerosene
UST was abandoned in place. In March 2001, NCDEQ recommended that the two sites (White’s Cross
Grocery and Myers Grocery) be combined into one site. Twenty-four Type II monitoring wells ((M)MW-
1, (M)MW-2, (M)MW-3, (M)MW-5 through (M)MW-11), ((W)MW-1 through (W)MW-7 and (W)MW-9
through (W)MW-15), and two Type III monitoring wells ((M)MWD-4 and (W)MWD-8) were installed at
the sites during previous ground water assessment and corrective action activities.

On February 1, 2018, eight Type II monitoring wells were gauged, purged and sampled. Concentrations
of requested method constituents that exceeded the Maximum Allowable Concentrations specified in
T15A NCAC 2L.0202 were reported in the ground water samples collected from (M)MW-2, (W)MW-1,
(W)MW-12 and (W)MW-15. None of the reported contaminant concentrations exceeded the Gross
Contamination Levels (GCLs).

Contaminant absorbent BioSocks were removed and were not replaced in (M)MW-2, (W)MW-1 and
(W)MW-15 during the February 2018 sampling event.

Based on this information, it is recommended that options to abandon WSW-1 should continue to be
pursued in an effort to lower the risk of the site. If the site risk classification cannot be lowered, semi-
annual ground water sampling activities should continue. The next semi-annual sampling event is
tentatively scheduled for August 2018. Additionally, the BioSocks installed in September 2016, and since
removed from the site, appear to have been marginally effective in reducing contaminant concentrations.
More aggressive means of remediation should be considered in order to reduce the contaminant
concentrations at the site.

TABLE OF CONTENTS

1.0 SITE HISTORY AND CHARACTERIZATION .................................................................... 1
2.0 CURRENT SITE ASSESSMENT ............................................................................................ 1
3.0 GROUND WATER QUALITY ................................................................................................ 2
4.0 CONCLUSIONS AND RECOMMENDATIONS .................................................................... 3
5.0 LIMITATIONS ......................................................................................................................... 3
FIGURES
Figure 1: Site Location Map
Figure 2: Site Map
Figure 3: Water Table Surface Map
Figure 4: Ground Water Quality Map

TABLES
Table 1: Well Construction and Gauging Information
Table 2: Summary of Ground Water Sample Analytical Results

APPENDIX
Appendix A: Laboratory Report – Ground Water Samples

1
1.0 SITE HISTORY AND CHARACTERIZATION
The Myers Grocery and White’s Cross Grocery sites are located at 1901 and 1906 Wakelon Road in
Colerain, Bertie County, North Carolina (Figure 1). According to available information, one 4,000-
gallon gasoline, one 2,000-gallon gasoline, one 1,000-gallon gasoline and one 4,000-gallon diesel
underground storage tanks (USTs) were removed from the White’s Grocery site in February 1994 by
Coastal Environmental Services, Inc. (Coastal). In addition, one 1,000-gallon kerosene UST was
abandoned in place. Two 2,000-gallon gasoline USTs were removed from the Myers Grocery site by
Coastal in September 1992.

In March 2001, NCDEQ recommended that the two sites be combined into one site, and Coastal renamed
the monitoring wells with a prefix of (M) added to the Myers’s facility monitoring wells and a (W) to the
White’s facility monitoring wells. Twenty-two Type II monitoring wells ((M)MW-1, (M)MW-2,
(M)MW-3, (M)MW-6, (M)MW-9, (M)MW-10 through (M)MW-14), ((W)MW-1 through (W)MW-7 and
(W)MW-9 through (W)MW-13), and two Type III monitoring wells ((M)MWD-4 and (W)MWD-8) are
present onsite, having been installed during previous ground water assessment and corrective action
activities.

Although Geological Resources, Inc. (GRI) cannot verify the accuracy of information obtained from
previous reports, for the purposes of this report, it is assumed to be correct. A Site Map showing the
structures on-site and the locations of the monitoring wells is included as Figure 2. Please note that on
July 28, 2010, as requested by NCDEQ, GRI personnel verified with Bertie County Water Department
personnel that municipal water lines run along Meadow Road. Please refer to previous submittals for
further historical information regarding the site.

2.0 CURRENT SITE ASSESSMENT
This report presents the results of ground water sampling and BioSock maintenance activities conducted
in February 2018 at the Myers Grocery and White’s Cross Grocery sites. The activities were conducted
in accordance with GRI proposal number 17-504, which was submitted to NCDEQ on August 25, 2017,
and approved as Task Authorization No. 9420-29 on September 27, 2017. The purpose of the activities
was to obtain current ground water quality data and remove contaminant absorbent BioSocks from the
site.

2
3.0 GROUND WATER QUALITY
Eight Type II monitoring wells ((M)MW-2, (M)MW-3, (M)MW-9, (W)MW-1, (W)MW-3, (W)MW-11,
(W)MW-12 and (W)MW-15) were gauged, purged and sampled on February 1, 2018. The depths to
ground water in the Type II monitoring wells during the February 2018 sampling event ranged from the
top of well casing to 1.50 feet below the tops of well casings. Ground water elevations in the Type II
monitoring wells relative to a temporary benchmark with an assumed elevation of 100.00 feet ranged
from 97.33 to 97.75 feet. Based on this information, ground water flow direction was generally toward
the west with an average hydraulic gradient of less than 0.01 feet per foot. A Water Table Surface Map
for the February 1, 2018, gauging event has been included as Figure 3. Well construction and gauging
information is presented in Table 1.

Laboratory analyses were performed on the ground water samples collected from the monitoring wells
during the February 2018 sampling event for volatile organic compounds using EPA Method 6200B.

Concentrations of one or more individual BTEX constituents, MTBE, naphthalene, 1,2-dichloroethane,
isopropylbenzene, IPE, n-propylbenzene, 1,2,4-trimethylbenzene and/or 1,3,5-trimethylbenzene that
exceeded the Maximum Allowable Concentrations (MACs) specified in T15A NCAC 2L.0202 were
reported in the ground water samples collected from (M)MW-2, (W)MW-1, (W)MW-12 and (W)MW-15.
None of the reported contaminant concentrations exceeded the Gross Contamination Levels (GCLs). A
Ground Water Quality Map based on data from the February 2018 sampling event has been included as
Figure 4. A summary of ground water sample analytical results is presented in Table 2. A complete
laboratory report has been included as Appendix A.

Upon conclusion of the February 2018 sampling event, contaminant absorbent BioSocks were removed
and not replaced in (M)MW-2, (W)MW-1 and (W)MW-15. Since the initial installation of BioSocks at
the site in September 2016, contaminant concentrations in (M)MW-2 have been reduced by 35.02%
(47,270 µg/l in September 2016 to 30,714 µg/l in February 2018); contaminant concentrations in
(W)MW-1 have been reduced by 34.36% (3,494.8 µg/l in September 2016 to 2,293.9 µg/l in February
2018) and contaminant concentrations in (W)MW-15 appear to have increased by 34.73% (3,698.5 µg/l
in September 2016 to 4,983 µg/l in February 2018).

3

4.0 CONCLUSIONS AND RECOMMENDATIONS
 The average depth to ground water during the February 2018 sampling event was 1.14 feet below the
tops of well casings. Ground water flow at the site was toward the west with an average horizontal
hydraulic gradient of less than 0.01 feet per foot.
 Concentrations of one or more individual BTEX constituents, MTBE, naphthalene, 1,2-
dichloroethane, isopropylbenzene, IPE, n-propylbenzene, 1,2,4-trimethylbenzene and/or 1,3,5-
trimethylbenzene that exceeded the MACs were reported in the ground water samples collected from
(M)MW-2, (W)MW-1, (W)MW-12 and (W)MW-15. None of the reported contaminant
concentrations exceeded the GCLs.
 Contaminant absorbent BioSocks were removed and were not replaced in (M)MW-2, (W)MW-1 and
(W)MW-15 following the completion of the February 2018 sampling event. Contaminant
concentrations in (M)MW-2, (W)MW-1 and (W)MW-4 appear to have decreased since the initial
installation of BioSocks in September 2016. Concentrations in (W)MW-15 appear to have increased.
 Based on this information, it is recommended that options to abandon WSW-1 should continue to be
pursued in an effort to lower the risk of the site. If the site risk classification cannot be lowered,
semi-annual ground water sampling activities should continue. The next semi-annual sampling event
is tentatively scheduled for August 2018. Additionally, the BioSocks installed in September 2016,
and since removed from the site, appear to have been marginally effective in reducing contaminant
concentrations. More aggressive means of remediation should be considered in order to reduce the
contaminant concentrations at the site.

5.0 LIMITATIONS
This report has been prepared for the exclusive use of North East Oil Company, Inc. for specific
application to the referenced site in Bertie County, North Carolina. The assessment was conducted based
on the scope of work and level of effort desired by NCDEQ and with resources adequate only for that
scope of work. Our findings have been developed in accordance with generally accepted standards of
environmental practices in the State of North Carolina, available information, and our professional
judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would be
interpreted as being meaningful with respect to parameters indicated in the laboratory report. No

4
additional information can logically be inferred from this data. Please note field data collected prior to
the July 2009 sampling and updated receptor survey event were not obtained under the supervision of
GRI. Although the accuracy of these data cannot be verified, for the purpose of this report GRI assumes
that the information is correct.

FIGURES

TABLES
Date: 02/15/18
07/15/09 100.19 5.30 ---94.89
03/04/10 1.09 ---97.67
04/25/11 2.30 ---96.46
01/19/12 2.59 ---96.17
11/27/12 5.25 ---93.51
07/15/13 1.51 ---97.25
07/15/14 3.44 ---95.32
12/09/15 NM ---NM
07/15/09 99.78 5.10 ---94.68
03/04/10 0.62 ---97.78
04/25/11 2.04 ---96.36
01/19/12 2.31 ---96.09
11/27/12 5.22 ---93.18
07/15/13 1.01 ---97.39
07/15/14 3.23 ---95.17
12/09/15 2.08 ---96.32
09/06/16 3.53 ---94.87
06/22/17 1.97 ---96.43
02/01/18 1.07 ---97.33
07/15/09 99.83 5.10 ---94.73
03/04/10 1.15 ---97.31
04/25/11 2.06 ---96.40
01/19/12 2.32 ---96.14
11/27/12 5.17 ---93.29
07/15/13 1.00 ---97.46
07/15/14 3.18 ---95.28
12/09/15 2.00 ---96.46
09/06/16 3.40 ---95.06
06/22/17 1.93 ---96.53
02/01/18 1.08 ---97.38
07/15/09 99.59 8.83 ---90.76
03/04/10 3.25 ---94.95
04/25/11 4.40 ---93.80
01/19/12 5.40 ---92.80
11/27/12 9.01 ---89.19
07/15/13 4.33 ---93.87
07/15/14 6.39 ---91.81
12/09/15 6.04 ---92.16
09/06/16 7.92 ---90.28
07/15/09 99.78 5.34 ---94.44
03/04/10 1.57 ---96.72
04/25/11 2.07 ---96.22
01/19/12 2.02 ---96.27
11/27/12 5.55 ---92.74
07/15/13 1.31 ---96.98
07/15/14 3.18 ---95.11
12/09/15 NF ---NF
09/06/16 3.23 ---95.06
07/15/09 99.76 5.12 ---94.64
03/04/10 0.55 ---97.90
04/25/11 2.05 ---96.40
01/19/12 2.33 ---96.12
11/27/12 6.14 ---92.31
07/15/13 1.04 ---97.41
07/15/14 3.23 ---95.22
12/09/15 NM ---NM
06/22/17 2.02 ---96.43
02/01/18 1.04 ---97.41
07/15/09 99.56 5.00 ---94.56
03/04/10 0.00 ---98.22
04/25/11 1.88 ---96.34
01/19/12 1.82 ---96.40
11/27/12 5.38 ---92.84
07/15/13 0.50 ---97.72
07/15/14 2.77 ---95.45
12/09/15 1.35 ---96.87
09/06/16 2.70 ---95.52
98.45122-12208/25/93(M) MW-9
98.4603/10/93
2
122-122
03/09/93
122-122
(M) MW-1 98.76
2-122
122-12
98.22
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
MYERS GROCERY AND WHITE'S CROSS GROCERY (INCIDENT NOS. 9420 & 12073)
Free Product
Thickness
(ft.)
Date Water
Level Measured
(mm/dd/yy)
Bottom of
Well
(ft. BGS)
Date
Installed
(mm/dd/yy)
Well Casing
Depth
(ft. BGS)
Ground Water
Elevation
(ft.)
Well ID
Top of Casing
Elevation*
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Screened
Interval
(x to y ft.
BGS)
Facility ID #s: 0-032961/0-025022
08/24/93(M) MW-6
98.203530-35
05/31/94(M) MW-10
98.2912
3008/23/93(M) MWD-4
(M) MW-3
98.40122-12203/09/93(M) MW-2
Page 1 of 4
Date: 02/15/18
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
MYERS GROCERY AND WHITE'S CROSS GROCERY (INCIDENT NOS. 9420 & 12073)
Free Product
Thickness
(ft.)
Date Water
Level Measured
(mm/dd/yy)
Bottom of
Well
(ft. BGS)
Date
Installed
(mm/dd/yy)
Well Casing
Depth
(ft. BGS)
Ground Water
Elevation
(ft.)
Well ID
Top of Casing
Elevation*
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Screened
Interval
(x to y ft.
BGS)
Facility ID #s: 0-032961/0-025022
03/04/10 0.44 ---97.92
04/25/11 2.02 ---96.34
01/19/12 2.32 ---96.04
11/27/12 5.17 ---93.19
07/15/13 1.42 ---96.94
07/15/14 3.18 ---95.18
12/09/15 2.07 ---96.29
09/06/16 3.55 ---94.81
04/25/11 1.85 ---96.37
01/19/12 2.00 ---96.22
11/27/12 4.50 ---93.72
07/15/13 1.69 ---96.53
07/15/14 2.43 ---95.79
12/09/15 1.32 ---96.90
09/06/16 2.11 ---96.11
04/25/11 2.13 ---96.48
01/19/12 2.30 ---96.31
11/27/12 5.06 ---93.55
07/15/13 1.48 ---97.13
07/15/14 3.02 ---95.59
12/09/15 NM ---NM
07/15/09 100.00 5.70 ---94.30
03/04/10 0.67 ---98.38
04/25/11 2.39 ---96.66
01/19/12 2.62 ---96.43
11/27/12 6.03 ---93.02
07/15/13 1.46 ---97.59
07/15/14 3.68 ---95.37
12/09/15 2.48 ---96.57
09/06/16 3.99 ---95.06
06/22/17 2.38 ---96.67
02/01/18 1.35 ---97.70
07/15/09 99.95 4.70 ---95.25
03/04/10 1.11 ---97.52
04/25/11 1.73 ---96.90
01/19/12 2.20 ---96.43
11/27/12 5.32 ---93.31
07/15/13 1.04 ---97.59
07/15/14 3.24 ---95.39
12/09/15 1.99 ---96.64
09/06/16 3.53 ---95.10
07/15/09 100.45 5.10 ---95.35
03/04/10 0.51 ---98.65
04/25/11 1.93 ---97.23
01/19/12 2.57 ---96.59
11/27/12 5.74 ---93.42
07/15/13 1.73 ---97.43
07/15/14 3.37 ---95.79
12/09/15 2.45 ---96.71
09/06/16 3.34 ---95.82
06/22/17 NM ---NM
02/01/18 1.50 ---97.66
07/15/09 100.25 4.44 ---95.81
03/04/10 0.71 ---98.17
04/25/11 1.68 ---97.20
01/19/12 2.50 ---96.38
11/27/12 4.77 ---94.11
07/15/13 1.54 ---97.34
07/15/14 3.64 ---95.24
12/09/15 2.56 ---96.32
09/06/16 4.23 ---94.65
07/15/09 100.11 5.42 ---94.69
03/04/10 0.24 ---98.51
04/25/11 2.08 ---96.67
01/19/12 2.15 ---96.60
11/27/12 5.70 ---93.05
07/15/13 0.84 ---97.91
07/15/14 3.22 ---95.53
12/09/15 1.93 ---96.82
09/06/16 3.65 ---95.10
98.88122-122
99.16122-122
(M) MW-14
98.22152-15202/22/11(M) MW-13
98.61122-12202/22/11
98.36155-15502/02/10(M) MW-12
09/15/95(W) MW-5
99.05122-122
206/13/94 122-12(W) MW-2 98.63
06/13/94(W) MW-4
98.75122-122
06/13/94(W) MW-3
06/13/94(W) MW-1
Page 2 of 4
Date: 02/15/18
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
MYERS GROCERY AND WHITE'S CROSS GROCERY (INCIDENT NOS. 9420 & 12073)
Free Product
Thickness
(ft.)
Date Water
Level Measured
(mm/dd/yy)
Bottom of
Well
(ft. BGS)
Date
Installed
(mm/dd/yy)
Well Casing
Depth
(ft. BGS)
Ground Water
Elevation
(ft.)
Well ID
Top of Casing
Elevation*
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Screened
Interval
(x to y ft.
BGS)
Facility ID #s: 0-032961/0-025022
07/15/09 99.89 5.70 ---94.19
03/04/10 1.40 ---97.47
04/25/11 2.26 ---96.61
01/19/12 2.38 ---96.49
11/27/12 5.91 ---92.96
07/15/13 1.16 ---97.71
07/15/14 3.57 ---95.30
12/09/15 NM NM NM
07/15/09 99.67 4.86 ---94.81
03/04/10 0.78 ---97.58
04/25/11 1.77 ---96.59
01/19/12 1.98 ---96.38
11/27/12 5.52 ---92.84
07/15/13 0.91 ---97.45
07/15/14 3.07 ---95.29
12/09/15 2.02 ---96.34
09/06/16 3.36 ---95.00
07/15/09 100.11 6.35 ---93.76
03/04/10 2.79 ---96.00
04/25/11 1.95 ---96.84
01/19/12 4.70 ---94.09
11/27/12 6.10 ---92.69
07/15/13 1.12 ---97.67
07/15/14 5.98 ---92.81
12/09/15 5.39 ---93.40
09/06/16 3.48 ---95.31
07/15/09 100.13 4.90 ---95.23
03/04/10 NM ---NM
04/25/11 2.31 ---96.51
01/19/12 3.14 ---95.68
11/27/12 6.10 ---92.72
07/15/13 2.70 ---96.12
07/15/14 3.67 ---95.15
12/09/15 NF ---NF
09/06/16 NF NF NF
07/15/09 100.29 NM ---NM
03/04/10 0.17 ---98.74
04/25/11 2.30 ---96.61
01/19/12 2.50 ---96.41
11/27/12 4.76 ---94.15
07/15/13 1.00 ---97.91
07/15/14 NM ---NM
12/09/15 NM ---NM
07/15/09 99.92 4.60 ---95.32
03/04/10 0.24 ---98.37
04/25/11 2.06 ---96.55
01/19/12 2.13 ---96.48
11/27/12 5.14 ---93.47
07/15/13 1.11 ---97.50
07/15/14 3.20 ---95.41
12/09/15 1.88 ---96.73
09/06/16 3.42 ---95.19
06/22/17 1.40 ---97.21
02/01/18 0.86 ---97.75
07/15/09 NF NF ---NF
03/04/10 NF ---NF
04/25/11 2.08 ---96.34
01/19/12 2.76 ---95.66
11/27/12 5.48 ---92.94
07/15/13 1.56 ---96.86
07/15/14 3.44 ---94.98
12/09/15 2.23 ---96.19
09/07/16 3.98 ---94.44
06/22/17 2.06 ---96.36
02/01/18 1.06 ---97.36
5-15
09/15/95(W) MW-6
30
09/18/95(W) MW-10
15
11.3
5-155
5-15
98.87122-122
98.82155-155
5 98.91
98.3615
98.79
12
25-302509/16/95(W) MWD-8
98.42155-15509/19/95(W) MW-12
09/18/95(W) MW-9
09/15/95(W) MW-7
98.6115509/18/95(W) MW-11
Page 3 of 4
Date: 02/15/18
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
MYERS GROCERY AND WHITE'S CROSS GROCERY (INCIDENT NOS. 9420 & 12073)
Free Product
Thickness
(ft.)
Date Water
Level Measured
(mm/dd/yy)
Bottom of
Well
(ft. BGS)
Date
Installed
(mm/dd/yy)
Well Casing
Depth
(ft. BGS)
Ground Water
Elevation
(ft.)
Well ID
Top of Casing
Elevation*
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Screened
Interval
(x to y ft.
BGS)
Facility ID #s: 0-032961/0-025022
07/15/09 100.25 NM ---NM
03/04/10 0.00 ---98.90
04/25/11 2.15 ---96.75
01/19/12 2.34 ---96.56
11/27/12 5.41 ---93.49
07/15/13 0.91 ---97.99
07/15/14 3.36 ---95.54
12/09/15 NM ---NM
03/04/10 0.74 ---98.15
04/25/11 2.37 ---96.52
01/19/12 2.76 ---96.13
11/27/12 5.87 ---93.02
07/15/13 1.52 ---97.37
07/15/14 3.72 ---95.17
12/09/15 2.54 ---96.35
09/06/16 4.12 ---94.77
03/04/10 2.11 ---96.60
04/25/11 2.17 ---96.54
01/19/12 2.48 ---96.23
11/27/12 5.62 ---93.09
07/15/13 1.29 ---97.42
07/15/14 3.52 ---95.19
12/09/15 3.04 ---95.67
09/06/16 3.86 ---94.85
06/22/17 2.20 ---96.51
02/01/18 1.17 ---97.54
Notes:
• Top-of-casing elevations prior to March 2010 were obtained from the report entitled 'Semi-Annual Groundwater Sampling Event October 2004' prepared by
Coastal Environmental Services, Inc. Top-of-casing elevations for the March 4, 2010 gauging data were professionally surveyed by Billy Felton, P.L.S. on
June 2, 2010. Top-of-casing elevations for (M) MW-13 and (M) MW-14 were surveyed by GRI personnel on February 22, 2011.
• NM: Not measured.
• NF: Not found.
15
11.63
2-12
15
98.90(W) MW-13
12
(W) MW-14
209/19/95
12
5-15502/02/10
502/02/10(W) MW-15
98.89
98.71
12.54
5-15
Page 4 of 4
Date: 02/15/18
EPA Method
6010B
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.4 70 70 70 400 400 15 400 10,000
5,000 260,000 84,500 85,500 20,000 6,000 400 25,000 70,000 30,000 28,500 25,000 15,000 NE NE
07/15/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <0.330 <1.00 <1.67 <0.330 <0.330 <0.330 5.13 <100 <100 NR NR <100 NR
03/04/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.200 <0.220 <0.150 <0.180 5.21 NR NR NR NR NR NR
04/25/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.200 <0.220 <0.150 <0.180 9.33 <100 <100 <150 81.3 <100 <170
01/19/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.11 <0.10 <0.10 NR NR NR NR NR NR NR
11/27/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR
07/15/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR
07/16/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR <35 <35 <98 <98 <35 <150
12/09/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/15/09 7,300 25,500 2,740 15,400 1,930 714 <66.0 <200 1,930 289 2,890 850 5.54 5,710 6,940 NR NR 8,900 NR
03/04/10 4,860 17,200 2,720 14,400 1,170 446 <22.0 151 1,450 350 3,290 830 9.44 NR NR NR NR NR NR
04/25/11 3,530 14,900 2,230 11,300 1,090 574 <55.0 130 J 1,280 399 3,480 902 3.78 21,100 13,800 176 <80.0 11,300 723
01/19/12 4,380 11,500 1,830 10,000 865 361 <41 92.7 J 976 193 2,240 566 NR NR NR NR NR NR NR
11/27/12 6,180 26,700 2,520 12,500 1,030 475 <25 101 J 987 287 2,510 601 NR NR NR NR NR NR NR
07/15/13 2,920 13,100 1,530 10,200 562 379 <10 73.5 643 196 2,280 548 NR NR NR NR NR NR NR
07/16/14 4,870 20,500 2,580 13,500 802 499 <10 109 1,000 331 2,750 749 NR 12,800 <3,500 3,400 <98 7,950 J 335
12/09/15 4,850 23,300 2,300 10,500 421 399 <41 76.9 J 522 236 1,980 466 NR NR NR NR NR NR NR
09/06/16 5,550 24,600 2,780 13,000 708 632 <13 131 934 368 2,750 743 NR NR NR NR NR NR NR
06/22/17 2,640 10,700 1,630 7,910 446 321 <25 75.8 J 595 188 2,080 497 NR NR NR NR NR NR NR
02/01/18 3,230 14,000 1,970 10,500 544 470 <25 106 758 263 2,750 735 NR NR NR NR NR NR NR
07/15/09 0.427 J <0.330 <0.670 <1.33 1.08 <1.00 <0.330 <1.00 <1.67 <0.330 <0.330 <0.330 26.7 <100 <100 NR NR <100 NR
03/04/10 4.13 6.21 3.05 16.4 5.92 0.651 J <0.220 0.600 J 13.2 <0.220 5.00 0.651 J 4.80 NR NR NR NR NR NR
04/25/11 1.61 0.589 J 0.880 J 6.16 2.03 <0.500 <0.220 0.297 J 2.74 0.354 J 2.66 0.563 J 11.6 <100 <100 <167 <88.9 <100 <189
01/19/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.11 <0.10 <0.10 NR NR NR NR NR NR NR
11/27/12 <0.10 <0.10 <0.10 <0.22 0.19 J <0.15 <0.10 <0.10 0.12 J <0.10 <0.10 <0.10 NR NR NR NR NR NR NR
07/15/13 0.11 J <0.10 <0.10 <0.22 0.12 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR
07/16/14 0.24 J 1.5 0.29 J 1.5 0.18 J 3.9 B <0.10 <0.10 0.12 J <0.10 0.82 0.16 J NR <35 <35 <99 <99 <35 <150
12/09/15 0.25 J 1.5 0.18 J 0.60 J <0.16 <0.12 <0.16 <0.12 <0.16 <0.16 <0.14 <0.14 NR NR NR NR NR NR NR
09/06/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
06/22/17 <0.13 0.25 J <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
02/01/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
NELeadNEC9-C10 Aromatics2001,2-DichloroethaneXylenesContaminant of Concern

2L Standard (µg/l)IPEFacilty ID #s: 0-032961/0-025022
TABLE 2
MADEP Methods VPH and EPHAnalytical Method
EPA Method 6200B
EthylbenzeneBenzeneTolueneMYERS GROCERY AND WHITE'S CROSS GROCERY (INCIDENT NOS. 9420 & 12073)
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
NaphthaleneIsopropylbenzeneMTBE(M) MW-1 C19-C36 Aliphatics (M) MW-2
(M) MW-3
700
GCL (µg/l)C11-C22 Aromatics 1,3,5-Trimethylbenzenen-PropylbenzeneC9-C18 AliphaticsC5-C8 Aliphatics C9-C12 Aliphatics 1,2,4-TrimethylbenzenePage 1 of 9
Date: 02/15/18
EPA Method
6010B
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.4 70 70 70 400 400 15 400 10,000
5,000 260,000 84,500 85,500 20,000 6,000 400 25,000 70,000 30,000 28,500 25,000 15,000 NE NE NELeadNEC9-C10 Aromatics2001,2-DichloroethaneXylenesContaminant of Concern

2L Standard (µg/l)IPEFacilty ID #s: 0-032961/0-025022
TABLE 2
MADEP Methods VPH and EPHAnalytical Method
EPA Method 6200B
EthylbenzeneBenzeneTolueneMYERS GROCERY AND WHITE'S CROSS GROCERY (INCIDENT NOS. 9420 & 12073)
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
NaphthaleneIsopropylbenzeneMTBEC19-C36 Aliphatics 700
GCL (µg/l)C11-C22 Aromatics 1,3,5-Trimethylbenzenen-PropylbenzeneC9-C18 AliphaticsC5-C8 Aliphatics C9-C12 Aliphatics 1,2,4-Trimethylbenzene07/15/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <0.330 <1.00 <1.67 <0.330 <0.330 <0.330 2.50 J <100 <100 NR NR <100 NR
03/04/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.200 <0.220 <0.150 <0.180 3.50 NR NR NR NR NR NR
04/25/11 <0.140 0.259 J <0.150 0.327 J <0.250 <0.500 <0.220 <0.150 <0.200 <0.220 0.158 J <0.180 3.48 <100 <100 <150 <80.0 <100 <170
01/19/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.11 <0.10 <0.10 NR NR NR NR NR NR NR
11/27/12 <0.10 <0.10 <0.10 <0.22 0.15 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR
07/15/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR
07/16/14 <0.10 0.26 J <0.10 <0.20 <0.10 0.16 JB <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR <35 <35 <99 <99 <35 <150
12/09/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.12 <0.16 <0.16 <0.14 <0.14 NR NR NR NR NR NR NR
09/06/16 <0.13 0.15 J <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
07/15/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <0.330 <1.00 <1.67 <0.330 <0.330 <0.330 7.87 <100 <100 NR NR <100 NR
03/04/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.200 <0.220 <0.150 <0.180 2.96 NR NR NR NR NR NR
04/25/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.200 <0.220 <0.150 <0.180 7.23 <100 <100 <150 <80.0 <100 <170
01/19/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.11 <0.10 <0.10 NR NR NR NR NR NR NR
11/27/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR
07/15/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR
07/16/14 <0.10 0.17 J <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR <35 <35 <99 <99 <35 <150
12/09/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
09/06/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
07/15/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <0.330 <1.00 <1.67 <0.330 <0.330 <0.330 116 <100 <100 NR NR <100 NR
03/04/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.200 <0.220 <0.150 <0.180 15.1 NR NR NR NR NR NR
04/25/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.200 <0.220 <0.150 <0.180 22.1 <100 <100 <150 <80.0 <100 <170
01/19/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.11 <0.10 <0.10 NR NR NR NR NR NR NR
11/27/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR
07/15/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR
07/16/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR <35 <35 <100 <100 <35 <150
12/09/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/22/17 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
02/01/18 0.14 J 0.64 <0.13 0.44 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
07/15/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <0.330 <1.00 <1.67 <0.330 <0.330 <0.330 46.0 <100 <100 NR NR <100 NR
03/04/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.200 <0.220 <0.150 <0.180 3.62 NR NR NR NR NR NR
04/25/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.200 <0.220 <0.150 <0.180 7.12 <100 <100 <150 <80.0 <100 <170
01/19/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.11 <0.10 <0.10 NR NR NR NR NR NR NR
11/27/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR
07/15/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR
07/16/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR <35 <35 <99 <99 <35 <150
12/09/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.12 <0.16 <0.16 <0.14 <0.14 NR NR NR NR NR NR NR
09/06/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
(M) MW-6
(M) MWD-4
(M) MW-9
(M) MW-10
Page 2 of 9
Date: 02/15/18
EPA Method
6010B
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.4 70 70 70 400 400 15 400 10,000
5,000 260,000 84,500 85,500 20,000 6,000 400 25,000 70,000 30,000 28,500 25,000 15,000 NE NE NELeadNEC9-C10 Aromatics2001,2-DichloroethaneXylenesContaminant of Concern

2L Standard (µg/l)IPEFacilty ID #s: 0-032961/0-025022
TABLE 2
MADEP Methods VPH and EPHAnalytical Method
EPA Method 6200B
EthylbenzeneBenzeneTolueneMYERS GROCERY AND WHITE'S CROSS GROCERY (INCIDENT NOS. 9420 & 12073)
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
NaphthaleneIsopropylbenzeneMTBEC19-C36 Aliphatics 700
GCL (µg/l)C11-C22 Aromatics 1,3,5-Trimethylbenzenen-PropylbenzeneC9-C18 AliphaticsC5-C8 Aliphatics C9-C12 Aliphatics 1,2,4-Trimethylbenzene03/04/10 0.174 J <0.190 <0.150 <0.220 <0.250 0.731 J <0.220 <0.150 0.337 J <0.220 0.196 J <0.180 77.7 NR NR NR NR NR NR
04/25/11 2.56 <0.190 0.222 J 0.474 J 1.26 5.95 0.624 J 0.624 J 3.62 <0.220 0.387 J 0.552 J 66.9 <100 <100 154 84.6 <100 <170
01/19/12 0.18 J <0.13 <0.15 <0.30 0.53 0.89 0.38 J <0.10 1.7 <0.11 <0.10 <0.10 NR NR NR NR NR NR NR
11/27/12 <0.10 <0.10 <0.10 <0.22 0.94 <0.15 0.16 J <0.10 2.7 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR
07/15/13 <0.10 <0.10 <0.10 <0.22 0.53 <0.15 <0.10 <0.10 1.4 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR
07/16/14 <0.10 <0.10 <0.10 <0.20 0.50 <0.10 0.19 J <0.10 1.6 <0.10 <0.10 <0.10 NR <35 <35 <99 <99 <35 <150
12/09/15 <0.17 <0.17 <0.15 <0.43 0.51 <0.12 <0.16 <0.12 1.8 <0.16 <0.14 <0.14 NR NR NR NR NR NR NR
09/06/16 0.35 J 1.5 <0.13 0.45 J 0.44 J <0.13 <0.13 <0.13 1.3 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
04/25/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.200 <0.220 <0.150 <0.180 200 <100 <100 <150 <80.0 <100 <170
01/19/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.11 <0.10 <0.10 NR NR NR NR NR NR NR
11/27/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR
07/15/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR
07/16/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR <35 <35 <100 <100 <35 <150
12/09/15 <0.17 0.28 J <0.15 <0.43 <0.16 <0.12 <0.16 <0.12 <0.16 <0.16 <0.14 <0.14 NR NR NR NR NR NR NR
09/06/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
04/25/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.200 <0.220 <0.150 <0.180 56.1 <100 <100 <150 <80.0 <100 <170
01/19/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.11 <0.10 <0.10 NR NR NR NR NR NR NR
11/27/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR
07/15/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR
07/16/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR <35 <35 <98 <98 <35 <150
12/09/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/15/09 254 738 2,090 8,340 <16.5 498 <16.5 215 <83.5 398 2,650 815 41.5 6,760 18,000 NR NR 15,900 NR
03/04/10 175 460 1,020 4,280 <2.50 296 <2.20 119 6.41 J 256 1,930 773 35.6 NR NR NR NR NR NR
04/25/11 138 635 622 2,300 4.98 J 171 <2.20 73.4 4.53 J 189 1,110 330 97.1 2,750 4,010 3,600 <80.0 5,190 554
01/19/12 132 444 957 2,970 4.8 J 323 <3.3 149 2.9 J 359 1,930 667 NR NR NR NR NR NR NR
11/27/12 267 3,000 2,630 10,300 <50 380 <50 133 J <50 385 2,230 618 NR NR NR NR NR NR NR
07/15/13 36.8 80.2 525 1,530 1.5 188 0.36 J 47.1 0.74 85.8 644 201 NR NR NR NR NR NR NR
07/16/14 45.6 234 938 3,070 <0.50 281 <0.50 102 <0.50 236 1,440 401 NR 1,220 J <700 2,080 <99 4,550 374
12/09/15 35.1 314 965 3,160 <4.1 310 <4.1 86.0 <4.0 234 1,670 398 NR NR NR NR NR NR NR
09/06/16 19.8 106 698 2,380 <2.5 291 <2.5 98.9 <2.5 278 1,400 375 NR NR NR NR NR NR NR
06/22/17 10.3 57.9 578 2,010 <2.5 224 B <2.5 59.6 <2.5 152 972 225 NR NR NR NR NR NR NR
02/01/18 14.8 88.1 459 1,590 <2.5 142 <2.5 51.0 <2.5 120 750 197 NR NR NR NR NR NR NR
(M) MW-13
(M) MW-12
(M) MW-14
(W) MW-1
Page 3 of 9
Date: 02/15/18
EPA Method
6010B
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.4 70 70 70 400 400 15 400 10,000
5,000 260,000 84,500 85,500 20,000 6,000 400 25,000 70,000 30,000 28,500 25,000 15,000 NE NE NELeadNEC9-C10 Aromatics2001,2-DichloroethaneXylenesContaminant of Concern

2L Standard (µg/l)IPEFacilty ID #s: 0-032961/0-025022
TABLE 2
MADEP Methods VPH and EPHAnalytical Method
EPA Method 6200B
EthylbenzeneBenzeneTolueneMYERS GROCERY AND WHITE'S CROSS GROCERY (INCIDENT NOS. 9420 & 12073)
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
NaphthaleneIsopropylbenzeneMTBEC19-C36 Aliphatics 700
GCL (µg/l)C11-C22 Aromatics 1,3,5-Trimethylbenzenen-PropylbenzeneC9-C18 AliphaticsC5-C8 Aliphatics C9-C12 Aliphatics 1,2,4-Trimethylbenzene07/15/09 <0.200 <0.330 <0.670 <1.33 0.439 J 4.27 <0.330 4.97 <1.67 3.81 13.6 1.97 7.70 <100 <100 NR NR <100 NR
03/04/10 <0.140 <0.190 1.07 <0.220 0.496 J 3.81 <0.220 5.42 <0.200 6.95 27.2 7.34 10.1 NR NR NR NR NR NR
04/25/11 <0.280 <0.380 0.977 J 1.89 J 0.539 J 10.1 <0.440 12.0 <0.400 24.4 88.2 8.08 13.6 120 <100 273 <80.0 300 <170
01/19/12 <0.13 <0.13 <0.15 <0.30 0.21 J 1.2 <0.16 0.48 J <0.11 <0.11 0.66 <0.10 NR NR NR NR NR NR NR
11/27/12 <0.10 <0.10 0.50 <0.22 0.26 J 6.0 <0.10 5.0 <0.10 5.5 16.3 2.1 NR NR NR NR NR NR NR
07/15/13 <0.10 <0.10 <0.10 <0.22 0.13 J 1.2 <0.10 0.20 J <0.10 <0.10 0.14 J <0.10 NR NR NR NR NR NR NR
07/16/14 <0.10 <0.10 <0.10 <0.20 0.13 J 4.2 <0.10 2.7 <0.10 0.31 J 1.7 <0.10 NR 56.3 J <35 <99 <99 42.1 J <150
12/09/15 <0.17 <0.17 <0.15 <0.43 <0.16 0.33 J <0.16 <0.12 <0.16 <0.16 <0.14 <0.14 NR NR NR NR NR NR NR
09/06/16 <0.13 <0.13 <0.13 <0.31 <0.13 4.2 <0.13 2.1 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
07/15/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <0.330 <1.00 <1.67 <0.330 <0.330 <0.330 19.0 <100 <100 NR NR <100 NR
03/04/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.200 <0.220 <0.150 <0.180 9.25 NR NR NR NR NR NR
04/25/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.200 <0.220 <0.150 <0.180 15.0 <100 <100 152 <80.0 <100 <170
01/19/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.11 <0.10 <0.10 NR NR NR NR NR NR NR
11/27/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR
07/15/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR
07/16/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR <35 <35 <100 <100 <35 <150
12/09/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.12 <0.16 <0.16 <0.14 <0.14 NR NR NR NR NR NR NR
09/06/16 0.35 J 0.90 0.45 J 9.2 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 0.45 J 0.28 J NR NR NR NR NR NR NR
06/22/17 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
02/01/18 <0.13 <0.13 <0.13 <0.25 <0.13 0.60 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
07/15/09 2.79 <0.330 <0.670 <1.33 1.87 <1.00 <0.330 <1.00 <1.67 <0.330 <0.330 <0.330 51.3 <100 <100 NR NR <100 NR
03/04/10 <0.140 <0.190 <0.150 <0.220 1.09 <0.500 <0.220 <0.150 <0.200 <0.220 <0.150 <0.180 6.96 NR NR NR NR NR NR
04/25/11 0.386 J <0.190 <0.150 <0.220 1.87 <0.500 <0.220 <0.150 <0.200 <0.220 <0.150 <0.180 17.4 <100 <100 <150 257 <100 <170
01/19/12 <0.13 <0.13 <0.15 <0.30 1.8 <0.10 <0.16 <0.10 <0.11 <0.11 <0.10 <0.10 NR NR NR NR NR NR NR
11/27/12 <0.10 <0.10 <0.10 <0.22 1.5 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR
07/15/13 7.2 1.5 1.5 28.8 4.7 5.1 <0.10 1.8 <0.10 0.68 8.3 0.33 J NR NR NR NR NR NR NR
07/16/14 3.4 1.2 1.2 23.0 4.3 1.7 <0.10 1.4 <0.10 1.3 9.5 0.42 J NR 38.1 J <35 <99 <99 <35 <150
12/09/15 60.9 9.9 148 731 13.8 27.7 0.39 J 22.6 <0.16 36.1 266 19.1 NR NR NR NR NR NR NR
09/06/16 0.16 J <0.13 <0.13 0.51 J 0.32 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
(W) MW-3
(W) MW-2
(W) MW-4
Page 4 of 9
Date: 02/15/18
EPA Method
6010B
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.4 70 70 70 400 400 15 400 10,000
5,000 260,000 84,500 85,500 20,000 6,000 400 25,000 70,000 30,000 28,500 25,000 15,000 NE NE NELeadNEC9-C10 Aromatics2001,2-DichloroethaneXylenesContaminant of Concern

2L Standard (µg/l)IPEFacilty ID #s: 0-032961/0-025022
TABLE 2
MADEP Methods VPH and EPHAnalytical Method
EPA Method 6200B
EthylbenzeneBenzeneTolueneMYERS GROCERY AND WHITE'S CROSS GROCERY (INCIDENT NOS. 9420 & 12073)
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
NaphthaleneIsopropylbenzeneMTBEC19-C36 Aliphatics 700
GCL (µg/l)C11-C22 Aromatics 1,3,5-Trimethylbenzenen-PropylbenzeneC9-C18 AliphaticsC5-C8 Aliphatics C9-C12 Aliphatics 1,2,4-Trimethylbenzene07/15/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <0.330 <1.00 <1.67 <0.330 <0.330 <0.330 10.5 <100 <100 NR NR <100 NR
03/04/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.200 <0.220 <0.150 <0.180 25.3 NR NR NR NR NR NR
04/25/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.200 <0.220 <0.150 <0.180 28.5 <100 <100 150 111 <100 <170
01/19/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.11 <0.10 <0.10 NR NR NR NR NR NR NR
11/27/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR
07/15/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR
07/16/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR <35 <35 <100 <100 <35 <150
12/09/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.12 <0.16 <0.16 <0.14 <0.14 NR NR NR NR NR NR NR
09/06/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
07/15/09 <0.200 1.28 <0.670 <1.33 <0.330 <1.00 <0.330 <1.00 <1.67 <0.330 <0.330 <0.330 15.6 <100 <100 NR NR <100 NR
03/04/10 <0.140 1.80 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.200 <0.220 <0.150 <0.180 16.5 NR NR NR NR NR NR
04/25/11 <0.140 2.37 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.200 <0.220 <0.150 <0.180 3.77 <100 <100 168 117 <100 <170
01/19/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.11 <0.10 <0.10 NR NR NR NR NR NR NR
11/27/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR
07/15/13 <0.10 0.64 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR
07/16/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR <35 <35 <100 <100 <35 <150
12/09/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/15/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <0.330 <1.00 <1.67 <0.330 <0.330 <0.330 7.81 <100 <100 NR NR <100 NR
03/04/10 <0.140 <0.190 <0.150 <0.220 0.719 J <0.500 <0.220 <0.150 <0.200 <0.220 <0.150 <0.180 4.66 NR NR NR NR NR NR
04/25/11 <0.140 <0.190 <0.150 <0.220 2.43 <0.500 <0.220 <0.150 <0.200 <0.220 <0.150 <0.180 16.0 <100 <100 170 136 <100 <170
01/19/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.11 <0.10 <0.10 NR NR NR NR NR NR NR
11/27/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR
07/15/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR
07/16/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR <35 <35 <98 <98 <35 <150
12/09/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.12 <0.16 <0.16 <0.14 <0.14 NR NR NR NR NR NR NR
09/06/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
07/15/09 <0.200 1.37 <0.670 <1.33 22.2 <1.00 <0.330 <1.00 <1.67 <0.330 <0.330 <0.330 8.20 <100 <100 NR NR <100 NR
03/04/10 <0.140 0.329 J <0.150 10.8 34.7 <0.500 <0.220 <0.150 0.296 J <0.220 3.27 0.956 J 19.0 NR NR NR NR NR NR
04/25/11 0.494 J 13.2 1.80 10.6 2.07 <0.500 <0.220 0.222 J <0.200 0.238 J 1.80 0.634 J 257 <100 <100 163 103 <100 <167
01/19/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.11 <0.10 <0.10 NR NR NR NR NR NR NR
11/27/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR
07/15/13 0.14 J 1.3 0.51 3.0 0.99 <0.15 <0.10 <0.10 <0.10 <0.10 0.19 J <0.10 NR NR NR NR NR NR NR
07/16/14 <0.10 <0.10 <0.10 <0.20 2.7 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR <35 <35 NR NR <35 NR
12/09/15 <0.17 <0.17 <0.15 <0.43 0.69 <0.12 <0.16 <0.12 <0.16 <0.16 <0.14 <0.14 NR NR NR NR NR NR NR
09/06/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
(W) MWD-8
(W) MW-6
(W) MW-7
(W) MW-5
Page 5 of 9
Date: 02/15/18
EPA Method
6010B
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.4 70 70 70 400 400 15 400 10,000
5,000 260,000 84,500 85,500 20,000 6,000 400 25,000 70,000 30,000 28,500 25,000 15,000 NE NE NELeadNEC9-C10 Aromatics2001,2-DichloroethaneXylenesContaminant of Concern

2L Standard (µg/l)IPEFacilty ID #s: 0-032961/0-025022
TABLE 2
MADEP Methods VPH and EPHAnalytical Method
EPA Method 6200B
EthylbenzeneBenzeneTolueneMYERS GROCERY AND WHITE'S CROSS GROCERY (INCIDENT NOS. 9420 & 12073)
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
NaphthaleneIsopropylbenzeneMTBEC19-C36 Aliphatics 700
GCL (µg/l)C11-C22 Aromatics 1,3,5-Trimethylbenzenen-PropylbenzeneC9-C18 AliphaticsC5-C8 Aliphatics C9-C12 Aliphatics 1,2,4-Trimethylbenzene07/15/09 8.48 <0.330 5.13 5.02 50.0 15.8 6.14 11.1 6.52 5.60 2.02 1.33 12.6 180 133 NR NR 122 NR
03/04/10 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NR NR NS NR
04/25/11 0.674 J <0.190 0.217 J <0.220 4.50 0.670 J 0.619 J 0.468 J 1.16 0.263 J <0.150 <0.180 196 <100 <100 174 289 <100 <167
01/19/12 12.2 0.33 J 3.4 1.9 10.4 6.3 2.7 4.2 4.4 2.4 5.0 <0.10 NR NR NR NR NR NR NR
11/27/12 2.8 <0.10 16.1 0.65 J 17.3 19.0 4.2 10.5 6.7 10.9 1.0 <0.10 NR NR NR NR NR NR NR
07/15/13 6.4 0.11 J 7.7 0.32 J 7.7 12.5 2.2 6.6 3.7 5.8 4.9 0.11 J NR NR NR NR NR NR NR
07/16/14 1.1 <0.10 2.3 1.1 J 12.4 8.6 2.3 3.1 4.1 1.9 0.91 <0.10 NR 106 <35 <100 <100 56.0 J <150
12/09/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/04/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.200 <0.220 <0.150 <0.180 7.32 NR NR NR NR NR NR
04/25/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.200 <0.220 <0.150 <0.180 8.49 <100 <100 155 109 <100 <170
01/19/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.11 <0.10 <0.10 NR NR NR NR NR NR NR
11/27/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR
07/15/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR
07/16/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
12/09/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/15/09 0.470 J <0.330 <0.670 <1.33 <0.330 2.93 <0.330 <1.00 <1.67 <0.330 0.705 J <0.330 60.1 <100 <100 NR NR <100 NR
03/04/10 0.477 J <0.190 <0.150 0.274 J <0.250 0.961 J <0.220 <0.150 <0.200 <0.220 0.215 J <0.180 11.2 NR NR NR NR NR NR
04/25/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.200 <0.220 <0.150 <0.180 34.3 <100 <100 <150 124 <100 <170
01/19/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.11 <0.10 <0.10 NR NR NR NR NR NR NR
11/27/12 0.74 <0.10 0.65 1.6 0.18 J 3.1 <0.10 <0.10 <0.10 0.18 J 0.42 J 0.26 J NR NR NR NR NR NR NR
07/15/13 0.23 J <0.10 0.18 J 0.32 J <0.10 0.89 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR
07/16/14 <0.10 <0.10 <0.10 <0.20 <0.10 0.15 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR <35 <35 <100 <100 <35 <150
12/09/15 1.2 <0.17 <0.15 <0.43 <0.16 5.6 <0.16 <0.12 <0.16 <0.16 <0.14 <0.14 NR NR NR NR NR NR NR
09/06/16 1.1 0.43 J 2.6 12.7 0.44 J 0.21 J <0.13 0.23 J <0.13 0.64 2.6 0.67 NR NR NR NR NR NR NR
06/22/17 <0.13 <0.13 <0.13 <0.25 <0.13 0.25 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
02/01/18 0.31 J <0.13 <0.13 <0.25 <0.13 1.3 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
03/04/10 NF NF NF NF NF NF NF NF NF NF NF NF NF NF NF NF NF NF NF
04/25/11 417 47.6 131 754 49.1 5.84 J 8.53 J 10.0 <2.00 16.9 136 18.8 16.3 1,130 1,110 468 154 422 <163
01/19/12 763 97.3 283 1,690 99.0 17.5 6.3 26.4 <2.1 54.7 313 31.1 NR NR NR NR NR NR NR
11/27/12 1,320 187 636 3,280 102 23.2 17.1 43.2 3.1 73.1 440 89.5 NR NR NR NR NR NR NR
07/15/13 8.5 <0.10 0.42 J 2.1 2.8 0.52 0.48 J 0.39 J 0.11 J 0.88 2.5 <0.10 NR NR NR NR NR NR NR
07/16/14 1.3 <0.10 <0.10 0.94 J 1.2 0.12 J 0.18 J <0.10 <0.10 <0.10 0.28 J <0.10 NR <35 <35 <100 <100 <35 <150
12/09/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.12 <0.16 <0.16 <0.14 <0.14 NR NR NR NR NR NR NR
09/07/16 36.6 4.4 6.2 75.1 11.6 1.6 0.92 2.3 0.21 J 4.5 21.1 <0.13 NR NR NR NR NR NR NR
06/22/17 363 59.4 255 1,280 83.3 10.7 4.2 J 13.8 <1.3 32.1 210 36.6 NR NR NR NR NR NR NR
02/01/18 1,140 335 1,070 5,760 169 48.4 8.2 J 59.8 <6.3 144 855 204 NR NR NR NR NR NR NR
(W) MW-9
(W) MW-10
(W) MW-12
(W) MW-11
Page 6 of 9
Date: 02/15/18
EPA Method
6010B
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.4 70 70 70 400 400 15 400 10,000
5,000 260,000 84,500 85,500 20,000 6,000 400 25,000 70,000 30,000 28,500 25,000 15,000 NE NE NELeadNEC9-C10 Aromatics2001,2-DichloroethaneXylenesContaminant of Concern

2L Standard (µg/l)IPEFacilty ID #s: 0-032961/0-025022
TABLE 2
MADEP Methods VPH and EPHAnalytical Method
EPA Method 6200B
EthylbenzeneBenzeneTolueneMYERS GROCERY AND WHITE'S CROSS GROCERY (INCIDENT NOS. 9420 & 12073)
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
NaphthaleneIsopropylbenzeneMTBEC19-C36 Aliphatics 700
GCL (µg/l)C11-C22 Aromatics 1,3,5-Trimethylbenzenen-PropylbenzeneC9-C18 AliphaticsC5-C8 Aliphatics C9-C12 Aliphatics 1,2,4-Trimethylbenzene03/04/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.200 <0.220 <0.150 <0.180 16.7 NR NR NR NR NR NR
04/25/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.200 <0.220 <0.150 <0.180 21.0 <100 <100 152 116 <100 <167
01/19/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.11 <0.10 <0.10 NR NR NR NR NR NR NR
11/27/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR
07/15/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR
07/16/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR <35 <35 <98 <98 <35 <150
12/09/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/04/10 <0.140 <0.190 <0.150 0.505 J 0.413 J <0.500 <0.220 <0.150 <0.200 <0.220 0.189 J <0.180 121 NR NR NR NR NR NR
04/25/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.200 <0.220 <0.150 <0.180 65.3 <100 <100 171 126 <100 <170
01/19/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.11 <0.10 <0.10 NR NR NR NR NR NR NR
11/27/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR
07/15/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR
07/16/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR <35 <35 <100 <100 <35 <150
12/09/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.12 <0.16 <0.16 <0.14 <0.14 NR NR NR NR NR NR NR
09/06/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
03/04/10 2,360 1,600 1,150 9,530 448 50.7 <4.40 88.5 <4.00 186 1,330 334 156 NR NR NR NR NR NR
04/25/11 1,090 947 860 5,440 359 88.6 J <22.0 58.9 J <20.0 132 1,120 267 12.9 4,580 9,710 2,010 129 4,660 204
01/19/12 703 655 804 3,010 191 60.0 4.5 J 72.0 <2.1 167 835 205 NR NR NR NR NR NR NR
11/27/12 1,410 1,740 1,570 8,270 446 81.3 8.6 J 79.4 <5.0 223 1,380 335 NR NR NR NR NR NR NR
07/15/13 462 498 621 3,290 182 76.4 3.0 47.1 1.6 127 695 159 NR NR NR NR NR NR NR
07/16/14 510 460 818 4,730 234 66.5 5.5 J 60.3 2.9 J 182 925 226 NR 1,520 <350 346 <100 3,100 <150
12/09/15 438 940 862 3,260 162 76.2 <4.1 70.5 <4.0 171 806 198 NR NR NR NR NR NR NR
09/06/16 239 79.0 533 2,670 107 70.5 1.6 J 71.7 0.82 J 180 670 144 NR NR NR NR NR NR NR
06/22/17 394 260 890 5,100 141 67.6 <6.3 75.7 <6.3 213 1,350 295 NR NR NR NR NR NR NR
02/01/18 303 340 735 3,420 106 79.0 <2.5 60.2 <2.5 145 760 191 NR NR NR NR NR NR NR
03/04/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.200 <0.220 <0.150 <0.180 <1.50 NR NR NR NR NR NR
04/25/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.200 <0.220 <0.150 <0.180 <1.50 <100 <100 <150 <80.0 <100 <170
01/19/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.11 <0.10 <0.10 NR NR NR NR NR NR NR
07/15/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/04/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.200 <0.220 <0.150 <0.180 <1.50 NR NR NR NR NR NR
04/25/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/19/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
11/27/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/15/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
(W) MW-14
WSW-1
(W) MW-15
WSW-2
(W) MW-13
Page 7 of 9
Date: 02/15/18
EPA Method
6010B
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.4 70 70 70 400 400 15 400 10,000
5,000 260,000 84,500 85,500 20,000 6,000 400 25,000 70,000 30,000 28,500 25,000 15,000 NE NE NELeadNEC9-C10 Aromatics2001,2-DichloroethaneXylenesContaminant of Concern

2L Standard (µg/l)IPEFacilty ID #s: 0-032961/0-025022
TABLE 2
MADEP Methods VPH and EPHAnalytical Method
EPA Method 6200B
EthylbenzeneBenzeneTolueneMYERS GROCERY AND WHITE'S CROSS GROCERY (INCIDENT NOS. 9420 & 12073)
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
NaphthaleneIsopropylbenzeneMTBEC19-C36 Aliphatics 700
GCL (µg/l)C11-C22 Aromatics 1,3,5-Trimethylbenzenen-PropylbenzeneC9-C18 AliphaticsC5-C8 Aliphatics C9-C12 Aliphatics 1,2,4-Trimethylbenzene03/04/10 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
04/25/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/19/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
11/27/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/15/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/04/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.200 <0.220 <0.150 <0.180 4.28 NR NR NR NR NR NR
04/25/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/19/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/15/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/04/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.200 <0.220 <0.150 <0.180 <1.50 NR NR NR NR NR NR
04/25/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.200 <0.220 <0.150 <0.180 <1.50 <100 <100 185 126 <100 <157
01/19/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.11 <0.10 <0.10 NR NR NR NR NR NR NR
07/15/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
12/09/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.12 <0.16 <0.16 <0.14 <0.14 NR NR NR NR NR NR NR
03/04/10 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
04/25/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/19/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
11/27/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/15/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
WSW-7 12/09/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.12 <0.16 <0.16 <0.14 <0.14 NR NR NR NR NR NR NR
01/19/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.11 <0.10 <0.10 NR NR NR NR NR NR NR
07/15/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
12/09/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.12 <0.16 <0.16 <0.14 <0.14 NR NR NR NR NR NR NR
11/27/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR
07/15/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/16/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR <35 <35 <100 <100 <35 <150
11/27/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR
07/15/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/16/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR <35 <35 <98 <98 <35 <150
11/27/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR
07/15/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
11/27/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR
07/15/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/16/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR <35 <35 <97 <97 <35 <150
11/27/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR
07/15/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/16/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR <35 <35 <97 <97 <35 <150
WSW-4
WSW-3
WSW-8
WSW-5
SP-5
SP-3/WSW-5
SP-1/WSW-8
SP-2/WSW-8
WSW-6
SP-4
Page 8 of 9
Date: 02/15/18
EPA Method
6010B
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.4 70 70 70 400 400 15 400 10,000
5,000 260,000 84,500 85,500 20,000 6,000 400 25,000 70,000 30,000 28,500 25,000 15,000 NE NE NELeadNEC9-C10 Aromatics2001,2-DichloroethaneXylenesContaminant of Concern

2L Standard (µg/l)IPEFacilty ID #s: 0-032961/0-025022
TABLE 2
MADEP Methods VPH and EPHAnalytical Method
EPA Method 6200B
EthylbenzeneBenzeneTolueneMYERS GROCERY AND WHITE'S CROSS GROCERY (INCIDENT NOS. 9420 & 12073)
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
NaphthaleneIsopropylbenzeneMTBEC19-C36 Aliphatics 700
GCL (µg/l)C11-C22 Aromatics 1,3,5-Trimethylbenzenen-PropylbenzeneC9-C18 AliphaticsC5-C8 Aliphatics C9-C12 Aliphatics 1,2,4-Trimethylbenzene11/27/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR
07/15/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/16/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR <35 <35 <96 <96 <35 <140
11/27/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR NR
07/15/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
Notes:
• 2L Standard: Maximum allowable concentrations, specified in TI5A NCAC 2L.0202.
• < : Less than the method detection limit specified in the laboratory report.
• Concentrations in bold face type exceeded the 2L Standards.
• NR: Analysis not requested.
• NE: No established standard.
• Please refer to the laboratory report for other compounds which were detected that did not exceed the 2L Standards.
SP-7/WSW-1
• B Indicates analyte found in associated method blank.
• NF: Not found.
• NS: Not sampled.
• J: Estimated value.
• GCL: Gross contamination level.
• Results reported in µg/l (micrograms/liter).
SP-6/WSW-1
Page 9 of 9

APPENDIX

APPENDIX A
Laboratory Report – Ground Water Samples
02/15/18
Technical Report for
GRI (Geological Resources Inc.)
Myer's Grocery & White's Grocery; SR 1001 & Waketon Rd, Colerain, NC
2857
SGS Job Number: FA51525
Sampling Date: 02/01/18
Report to:
GRI (Geological Resources Inc.)
[e-mail]
ATTN: William Regenthal
Total number of pages in report:
Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AK, AR, IA, KY, MA, MS, ND, NH, NV, OK, OR, UT, WA, WV
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone]
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Caitlin Brice, M.S.
General Manager
Orlando, FL 02/15/18
e-Hardcopy 2.0
Automated Report
45
SGS is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
Review standard terms at: http://www.sgs.com/en/terms-and-conditions
The results set forth herein are provided by SGS North America Inc.
1 of 45
FA51525
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................7
3.1: FA51525-1: MMW-2 ....................................................................................................8
3.2: FA51525-2: MMW-3 ....................................................................................................10
3.3: FA51525-3: MMW-9 ....................................................................................................12
3.4: FA51525-4: WMW-1 ....................................................................................................14
3.5: FA51525-5: WMW-3 ....................................................................................................16
3.6: FA51525-6: WMW-11 ..................................................................................................18
3.7: FA51525-7: WMW-12 ..................................................................................................20
3.8: FA51525-8: WMW-15 ..................................................................................................22
Section 4: Misc. Forms ............................................................................................................24
4.1: Chain of Custody ...........................................................................................................25
Section 5: MS Volatiles - QC Data Summaries .....................................................................27
5.1: Method Blank Summary ................................................................................................28
5.2: Blank Spike Summary ...................................................................................................34
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................40 123452 of 45
FA51525
SGS LabLink@184098 08:48 15-Feb-2018
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA51525
Myer's Grocery & White's Grocery; SR 1001 & Waketon Rd, Colerain, NC
Project No: 2857
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA51525-1 02/01/18 09:30 HM 02/02/18 AQ Ground Water MMW-2
FA51525-2 02/01/18 09:39 HM 02/02/18 AQ Ground Water MMW-3
FA51525-3 02/01/18 09:20 HM 02/02/18 AQ Ground Water MMW-9
FA51525-4 02/01/18 10:35 HM 02/02/18 AQ Ground Water WMW-1
FA51525-5 02/01/18 11:11 HM 02/02/18 AQ Ground Water WMW-3
FA51525-6 02/01/18 11:04 HM 02/02/18 AQ Ground Water WMW-11
FA51525-7 02/01/18 10:53 HM 02/02/18 AQ Ground Water WMW-12
FA51525-8 02/01/18 10:44 HM 02/02/18 AQ Ground Water WMW-15
3 of 45
FA515251
Summary of Hits Page 1 of 3
Job Number:FA51525
Account:GRI (Geological Resources Inc.)
Project:Myer's Grocery & White's Grocery; SR 1001 & Waketon Rd, Colerain, NC
Collected:02/01/18
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA51525-1 MMW-2
Benzene 3230 100 25 ug/l SM 6200B
Di-Isopropyl Ether 758 100 25 ug/l SM 6200B
Ethylbenzene 1970 100 25 ug/l SM 6200B
Isopropylbenzene 106 100 25 ug/l SM 6200B
Methyl Tert Butyl Ether 544 100 25 ug/l SM 6200B
Naphthalene 470 100 25 ug/l SM 6200B
n-Propylbenzene 263 100 25 ug/l SM 6200B
Styrene 39.0 J 100 25 ug/l SM 6200B
Toluene 14000 250 63 ug/l SM 6200B
1,2,4-Trimethylbenzene 2750 100 25 ug/l SM 6200B
1,3,5-Trimethylbenzene 735 100 25 ug/l SM 6200B
m,p-Xylene 6730 200 25 ug/l SM 6200B
o-Xylene 3730 100 25 ug/l SM 6200B
Xylene (total)10500 300 50 ug/l SM 6200B
FA51525-2 MMW-3
No hits reported in this sample.
FA51525-3 MMW-9
Benzene 0.14 J 0.50 0.13 ug/l SM 6200B
Toluene 0.64 0.50 0.13 ug/l SM 6200B
m,p-Xylene 0.28 J 1.0 0.13 ug/l SM 6200B
o-Xylene 0.17 J 0.50 0.13 ug/l SM 6200B
Xylene (total)0.44 J 1.5 0.25 ug/l SM 6200B
FA51525-4 WMW-1
Benzene 14.8 10 2.5 ug/l SM 6200B
n-Butylbenzene 11.7 10 2.5 ug/l SM 6200B
sec-Butylbenzene 7.7 J 10 2.5 ug/l SM 6200B
Ethylbenzene 459 10 2.5 ug/l SM 6200B
Isopropylbenzene 51.0 10 2.5 ug/l SM 6200B
p-Isopropyltoluene 4.0 J 10 2.5 ug/l SM 6200B
Naphthalene 142 10 2.5 ug/l SM 6200B
n-Propylbenzene 120 10 2.5 ug/l SM 6200B
Toluene 88.1 10 2.5 ug/l SM 6200B
1,2,4-Trimethylbenzene 750 10 2.5 ug/l SM 6200B
1,3,5-Trimethylbenzene 197 10 2.5 ug/l SM 6200B
m,p-Xylene 997 20 2.5 ug/l SM 6200B
o-Xylene 591 10 2.5 ug/l SM 6200B
Xylene (total)1590 30 5.0 ug/l SM 6200B
4 of 45
FA515252
Summary of Hits Page 2 of 3
Job Number:FA51525
Account:GRI (Geological Resources Inc.)
Project:Myer's Grocery & White's Grocery; SR 1001 & Waketon Rd, Colerain, NC
Collected:02/01/18
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA51525-5 WMW-3
Naphthalene 0.60 0.50 0.13 ug/l SM 6200B
FA51525-6 WMW-11
Benzene 0.31 J 0.50 0.13 ug/l SM 6200B
sec-Butylbenzene 0.18 J 0.50 0.13 ug/l SM 6200B
Naphthalene 1.3 0.50 0.13 ug/l SM 6200B
o-Xylene 0.18 J 0.50 0.13 ug/l SM 6200B
FA51525-7 WMW-12
Benzene 1140 25 6.3 ug/l SM 6200B
o-Chlorotoluene 23.6 J 25 6.3 ug/l SM 6200B
1,2-Dichloroethane 8.2 J 25 6.3 ug/l SM 6200B
Ethylbenzene 1070 25 6.3 ug/l SM 6200B
Isopropylbenzene 59.8 25 6.3 ug/l SM 6200B
Methyl Tert Butyl Ether 169 25 6.3 ug/l SM 6200B
Naphthalene 48.4 25 6.3 ug/l SM 6200B
n-Propylbenzene 144 25 6.3 ug/l SM 6200B
Toluene 335 25 6.3 ug/l SM 6200B
1,2,4-Trimethylbenzene 855 25 6.3 ug/l SM 6200B
1,3,5-Trimethylbenzene 204 25 6.3 ug/l SM 6200B
m,p-Xylene 3880 50 6.3 ug/l SM 6200B
o-Xylene 1880 25 6.3 ug/l SM 6200B
Xylene (total)5760 75 13 ug/l SM 6200B
FA51525-8 WMW-15
Benzene 303 10 2.5 ug/l SM 6200B
n-Butylbenzene 3.3 J 10 2.5 ug/l SM 6200B
sec-Butylbenzene 4.7 J 10 2.5 ug/l SM 6200B
o-Chlorotoluene 21.5 10 2.5 ug/l SM 6200B
Ethylbenzene 735 10 2.5 ug/l SM 6200B
Isopropylbenzene 60.2 10 2.5 ug/l SM 6200B
p-Isopropyltoluene 2.9 J 10 2.5 ug/l SM 6200B
Methyl Tert Butyl Ether 106 10 2.5 ug/l SM 6200B
Naphthalene 79.0 10 2.5 ug/l SM 6200B
n-Propylbenzene 145 10 2.5 ug/l SM 6200B
Toluene 340 10 2.5 ug/l SM 6200B
1,2,4-Trimethylbenzene 760 10 2.5 ug/l SM 6200B
1,3,5-Trimethylbenzene 191 10 2.5 ug/l SM 6200B
m,p-Xylene 2300 50 6.3 ug/l SM 6200B
5 of 45
FA515252
Summary of Hits Page 3 of 3
Job Number:FA51525
Account:GRI (Geological Resources Inc.)
Project:Myer's Grocery & White's Grocery; SR 1001 & Waketon Rd, Colerain, NC
Collected:02/01/18
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
o-Xylene 1130 25 6.3 ug/l SM 6200B
Xylene (total)3420 75 13 ug/l SM 6200B
6 of 45
FA515252
SGS LabLink@184098 08:48 15-Feb-2018
Sample Results
Report of Analysis
Orlando, FL
Section 3
7 of 45
FA515253
SGS LabLink@184098 08:48 15-Feb-2018
Report of Analysis Page 1 of 2
Client Sample ID:MMW-2
Lab Sample ID:FA51525-1 Date Sampled:02/01/18
Matrix:AQ - Ground Water Date Received:02/02/18
Method:SM 6200B Percent Solids:n/a
Project:Myer's Grocery & White's Grocery; SR 1001 & Waketon Rd, Colerain, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0211498.D 200 02/06/18 17:27 TD n/a n/a VA2313
Run #2 A0211520.D 500 02/07/18 14:19 TD n/a n/a VA2314
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 3230 100 25 ug/l
108-86-1 Bromobenzene ND 100 25 ug/l
74-97-5 Bromochloromethane ND 100 25 ug/l
75-27-4 Bromodichloromethane ND 100 25 ug/l
75-25-2 Bromoform ND 100 25 ug/l
104-51-8 n-Butylbenzene ND 100 25 ug/l
135-98-8 sec-Butylbenzene ND 100 25 ug/l
98-06-6 tert-Butylbenzene ND 100 25 ug/l
56-23-5 Carbon Tetrachloride ND 100 25 ug/l
108-90-7 Chlorobenzene ND 100 25 ug/l
75-00-3 Chloroethane ND 100 40 ug/l
67-66-3 Chloroform ND 100 25 ug/l
95-49-8 o-Chlorotoluene ND 100 25 ug/l
106-43-4 p-Chlorotoluene ND 100 25 ug/l
124-48-1 Dibromochloromethane ND 100 25 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 100 49 ug/l
106-93-4 1,2-Dibromoethane ND 100 25 ug/l
75-71-8 Dichlorodifluoromethane ND 100 40 ug/l
95-50-1 1,2-Dichlorobenzene ND 100 25 ug/l
541-73-1 1,3-Dichlorobenzene ND 100 25 ug/l
106-46-7 1,4-Dichlorobenzene ND 100 25 ug/l
75-34-3 1,1-Dichloroethane ND 100 25 ug/l
107-06-2 1,2-Dichloroethane ND 100 25 ug/l
75-35-4 1,1-Dichloroethylene ND 100 25 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 100 25 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 100 25 ug/l
78-87-5 1,2-Dichloropropane ND 100 25 ug/l
142-28-9 1,3-Dichloropropane ND 100 25 ug/l
594-20-7 2,2-Dichloropropane ND 100 25 ug/l
563-58-6 1,1-Dichloropropene ND 100 25 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 100 25 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 100 25 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
8 of 45
FA5152533.1
SGS LabLink@184098 08:48 15-Feb-2018
Report of Analysis Page 2 of 2
Client Sample ID:MMW-2
Lab Sample ID:FA51525-1 Date Sampled:02/01/18
Matrix:AQ - Ground Water Date Received:02/02/18
Method:SM 6200B Percent Solids:n/a
Project:Myer's Grocery & White's Grocery; SR 1001 & Waketon Rd, Colerain, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 758 100 25 ug/l
100-41-4 Ethylbenzene 1970 100 25 ug/l
87-68-3 Hexachlorobutadiene ND 100 25 ug/l
98-82-8 Isopropylbenzene 106 100 25 ug/l
99-87-6 p-Isopropyltoluene ND 100 25 ug/l
74-83-9 Methyl Bromide ND 100 40 ug/l
74-87-3 Methyl Chloride ND 100 40 ug/l
74-95-3 Methylene Bromide ND 100 25 ug/l
75-09-2 Methylene Chloride ND 400 200 ug/l
1634-04-4 Methyl Tert Butyl Ether 544 100 25 ug/l
91-20-3 Naphthalene 470 100 25 ug/l
103-65-1 n-Propylbenzene 263 100 25 ug/l
100-42-5 Styrene 39.0 100 25 ug/l J
630-20-6 1,1,1,2-Tetrachloroethane ND 100 25 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 100 25 ug/l
127-18-4 Tetrachloroethylene ND 100 25 ug/l
108-88-3 Toluene 14000 a 250 63 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 100 25 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 100 25 ug/l
71-55-6 1,1,1-Trichloroethane ND 100 25 ug/l
79-00-5 1,1,2-Trichloroethane ND 100 25 ug/l
79-01-6 Trichloroethylene ND 100 25 ug/l
75-69-4 Trichlorofluoromethane ND 100 40 ug/l
96-18-4 1,2,3-Trichloropropane ND 100 25 ug/l
95-63-6 1,2,4-Trimethylbenzene 2750 100 25 ug/l
108-67-8 1,3,5-Trimethylbenzene 735 100 25 ug/l
75-01-4 Vinyl Chloride ND 100 25 ug/l
m,p-Xylene 6730 200 25 ug/l
95-47-6 o-Xylene 3730 100 25 ug/l
1330-20-7 Xylene (total)10500 300 50 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 94%97%70-130%
17060-07-0 1,2-Dichloroethane-D4 89%95%70-130%
2037-26-5 Toluene-D8 101%98%70-130%
460-00-4 4-Bromofluorobenzene 99%101%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
9 of 45
FA5152533.1
SGS LabLink@184098 08:48 15-Feb-2018
Report of Analysis Page 1 of 2
Client Sample ID:MMW-3
Lab Sample ID:FA51525-2 Date Sampled:02/01/18
Matrix:AQ - Ground Water Date Received:02/02/18
Method:SM 6200B Percent Solids:n/a
Project:Myer's Grocery & White's Grocery; SR 1001 & Waketon Rd, Colerain, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0211499.D 1 02/06/18 17:50 TD n/a n/a VA2313
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 45
FA5152533.2
SGS LabLink@184098 08:48 15-Feb-2018
Report of Analysis Page 2 of 2
Client Sample ID:MMW-3
Lab Sample ID:FA51525-2 Date Sampled:02/01/18
Matrix:AQ - Ground Water Date Received:02/02/18
Method:SM 6200B Percent Solids:n/a
Project:Myer's Grocery & White's Grocery; SR 1001 & Waketon Rd, Colerain, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 95%70-130%
17060-07-0 1,2-Dichloroethane-D4 91%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 45
FA5152533.2
SGS LabLink@184098 08:48 15-Feb-2018
Report of Analysis Page 1 of 2
Client Sample ID:MMW-9
Lab Sample ID:FA51525-3 Date Sampled:02/01/18
Matrix:AQ - Ground Water Date Received:02/02/18
Method:SM 6200B Percent Solids:n/a
Project:Myer's Grocery & White's Grocery; SR 1001 & Waketon Rd, Colerain, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0211500.D 1 02/06/18 18:13 TD n/a n/a VA2313
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 0.14 0.50 0.13 ug/l J
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 45
FA5152533.3
SGS LabLink@184098 08:48 15-Feb-2018
Report of Analysis Page 2 of 2
Client Sample ID:MMW-9
Lab Sample ID:FA51525-3 Date Sampled:02/01/18
Matrix:AQ - Ground Water Date Received:02/02/18
Method:SM 6200B Percent Solids:n/a
Project:Myer's Grocery & White's Grocery; SR 1001 & Waketon Rd, Colerain, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene 0.64 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 0.28 1.0 0.13 ug/l J
95-47-6 o-Xylene 0.17 0.50 0.13 ug/l J
1330-20-7 Xylene (total)0.44 1.5 0.25 ug/l J
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 96%70-130%
17060-07-0 1,2-Dichloroethane-D4 92%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
13 of 45
FA5152533.3
SGS LabLink@184098 08:48 15-Feb-2018
Report of Analysis Page 1 of 2
Client Sample ID:WMW-1
Lab Sample ID:FA51525-4 Date Sampled:02/01/18
Matrix:AQ - Ground Water Date Received:02/02/18
Method:SM 6200B Percent Solids:n/a
Project:Myer's Grocery & White's Grocery; SR 1001 & Waketon Rd, Colerain, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0211521.D 20 02/07/18 14:42 TD n/a n/a VA2314
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 14.8 10 2.5 ug/l
108-86-1 Bromobenzene ND 10 2.5 ug/l
74-97-5 Bromochloromethane ND 10 2.5 ug/l
75-27-4 Bromodichloromethane ND 10 2.5 ug/l
75-25-2 Bromoform ND 10 2.5 ug/l
104-51-8 n-Butylbenzene 11.7 10 2.5 ug/l
135-98-8 sec-Butylbenzene 7.7 10 2.5 ug/l J
98-06-6 tert-Butylbenzene ND 10 2.5 ug/l
56-23-5 Carbon Tetrachloride ND 10 2.5 ug/l
108-90-7 Chlorobenzene ND 10 2.5 ug/l
75-00-3 Chloroethane ND 10 4.0 ug/l
67-66-3 Chloroform ND 10 2.5 ug/l
95-49-8 o-Chlorotoluene ND 10 2.5 ug/l
106-43-4 p-Chlorotoluene ND 10 2.5 ug/l
124-48-1 Dibromochloromethane ND 10 2.5 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 10 4.9 ug/l
106-93-4 1,2-Dibromoethane ND 10 2.5 ug/l
75-71-8 Dichlorodifluoromethane ND 10 4.0 ug/l
95-50-1 1,2-Dichlorobenzene ND 10 2.5 ug/l
541-73-1 1,3-Dichlorobenzene ND 10 2.5 ug/l
106-46-7 1,4-Dichlorobenzene ND 10 2.5 ug/l
75-34-3 1,1-Dichloroethane ND 10 2.5 ug/l
107-06-2 1,2-Dichloroethane ND 10 2.5 ug/l
75-35-4 1,1-Dichloroethylene ND 10 2.5 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 10 2.5 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 10 2.5 ug/l
78-87-5 1,2-Dichloropropane ND 10 2.5 ug/l
142-28-9 1,3-Dichloropropane ND 10 2.5 ug/l
594-20-7 2,2-Dichloropropane ND 10 2.5 ug/l
563-58-6 1,1-Dichloropropene ND 10 2.5 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 10 2.5 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 10 2.5 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
14 of 45
FA5152533.4
SGS LabLink@184098 08:48 15-Feb-2018
Report of Analysis Page 2 of 2
Client Sample ID:WMW-1
Lab Sample ID:FA51525-4 Date Sampled:02/01/18
Matrix:AQ - Ground Water Date Received:02/02/18
Method:SM 6200B Percent Solids:n/a
Project:Myer's Grocery & White's Grocery; SR 1001 & Waketon Rd, Colerain, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 10 2.5 ug/l
100-41-4 Ethylbenzene 459 10 2.5 ug/l
87-68-3 Hexachlorobutadiene ND 10 2.5 ug/l
98-82-8 Isopropylbenzene 51.0 10 2.5 ug/l
99-87-6 p-Isopropyltoluene 4.0 10 2.5 ug/l J
74-83-9 Methyl Bromide ND 10 4.0 ug/l
74-87-3 Methyl Chloride ND 10 4.0 ug/l
74-95-3 Methylene Bromide ND 10 2.5 ug/l
75-09-2 Methylene Chloride ND 40 20 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 10 2.5 ug/l
91-20-3 Naphthalene 142 10 2.5 ug/l
103-65-1 n-Propylbenzene 120 10 2.5 ug/l
100-42-5 Styrene ND 10 2.5 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 10 2.5 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 10 2.5 ug/l
127-18-4 Tetrachloroethylene ND 10 2.5 ug/l
108-88-3 Toluene 88.1 10 2.5 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 10 2.5 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 10 2.5 ug/l
71-55-6 1,1,1-Trichloroethane ND 10 2.5 ug/l
79-00-5 1,1,2-Trichloroethane ND 10 2.5 ug/l
79-01-6 Trichloroethylene ND 10 2.5 ug/l
75-69-4 Trichlorofluoromethane ND 10 4.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 10 2.5 ug/l
95-63-6 1,2,4-Trimethylbenzene 750 10 2.5 ug/l
108-67-8 1,3,5-Trimethylbenzene 197 10 2.5 ug/l
75-01-4 Vinyl Chloride ND 10 2.5 ug/l
m,p-Xylene 997 20 2.5 ug/l
95-47-6 o-Xylene 591 10 2.5 ug/l
1330-20-7 Xylene (total)1590 30 5.0 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 98%70-130%
17060-07-0 1,2-Dichloroethane-D4 96%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
15 of 45
FA5152533.4
SGS LabLink@184098 08:48 15-Feb-2018
Report of Analysis Page 1 of 2
Client Sample ID:WMW-3
Lab Sample ID:FA51525-5 Date Sampled:02/01/18
Matrix:AQ - Ground Water Date Received:02/02/18
Method:SM 6200B Percent Solids:n/a
Project:Myer's Grocery & White's Grocery; SR 1001 & Waketon Rd, Colerain, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0211522.D 1 02/07/18 15:05 TD n/a n/a VA2314
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
16 of 45
FA5152533.5
SGS LabLink@184098 08:48 15-Feb-2018
Report of Analysis Page 2 of 2
Client Sample ID:WMW-3
Lab Sample ID:FA51525-5 Date Sampled:02/01/18
Matrix:AQ - Ground Water Date Received:02/02/18
Method:SM 6200B Percent Solids:n/a
Project:Myer's Grocery & White's Grocery; SR 1001 & Waketon Rd, Colerain, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene 0.60 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 97%70-130%
17060-07-0 1,2-Dichloroethane-D4 95%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
17 of 45
FA5152533.5
SGS LabLink@184098 08:48 15-Feb-2018
Report of Analysis Page 1 of 2
Client Sample ID:WMW-11
Lab Sample ID:FA51525-6 Date Sampled:02/01/18
Matrix:AQ - Ground Water Date Received:02/02/18
Method:SM 6200B Percent Solids:n/a
Project:Myer's Grocery & White's Grocery; SR 1001 & Waketon Rd, Colerain, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0211523.D 1 02/07/18 15:28 TD n/a n/a VA2314
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 0.31 0.50 0.13 ug/l J
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene 0.18 0.50 0.13 ug/l J
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
18 of 45
FA5152533.6
SGS LabLink@184098 08:48 15-Feb-2018
Report of Analysis Page 2 of 2
Client Sample ID:WMW-11
Lab Sample ID:FA51525-6 Date Sampled:02/01/18
Matrix:AQ - Ground Water Date Received:02/02/18
Method:SM 6200B Percent Solids:n/a
Project:Myer's Grocery & White's Grocery; SR 1001 & Waketon Rd, Colerain, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene 1.3 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene 0.18 0.50 0.13 ug/l J
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 97%70-130%
17060-07-0 1,2-Dichloroethane-D4 96%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
19 of 45
FA5152533.6
SGS LabLink@184098 08:48 15-Feb-2018
Report of Analysis Page 1 of 2
Client Sample ID:WMW-12
Lab Sample ID:FA51525-7 Date Sampled:02/01/18
Matrix:AQ - Ground Water Date Received:02/02/18
Method:SM 6200B Percent Solids:n/a
Project:Myer's Grocery & White's Grocery; SR 1001 & Waketon Rd, Colerain, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0211524.D 50 02/07/18 15:51 TD n/a n/a VA2314
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 1140 25 6.3 ug/l
108-86-1 Bromobenzene ND 25 6.3 ug/l
74-97-5 Bromochloromethane ND 25 6.3 ug/l
75-27-4 Bromodichloromethane ND 25 6.3 ug/l
75-25-2 Bromoform ND 25 6.3 ug/l
104-51-8 n-Butylbenzene ND 25 6.3 ug/l
135-98-8 sec-Butylbenzene ND 25 6.3 ug/l
98-06-6 tert-Butylbenzene ND 25 6.3 ug/l
56-23-5 Carbon Tetrachloride ND 25 6.3 ug/l
108-90-7 Chlorobenzene ND 25 6.3 ug/l
75-00-3 Chloroethane ND 25 10 ug/l
67-66-3 Chloroform ND 25 6.3 ug/l
95-49-8 o-Chlorotoluene 23.6 25 6.3 ug/l J
106-43-4 p-Chlorotoluene ND 25 6.3 ug/l
124-48-1 Dibromochloromethane ND 25 6.3 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 25 12 ug/l
106-93-4 1,2-Dibromoethane ND 25 6.3 ug/l
75-71-8 Dichlorodifluoromethane ND 25 10 ug/l
95-50-1 1,2-Dichlorobenzene ND 25 6.3 ug/l
541-73-1 1,3-Dichlorobenzene ND 25 6.3 ug/l
106-46-7 1,4-Dichlorobenzene ND 25 6.3 ug/l
75-34-3 1,1-Dichloroethane ND 25 6.3 ug/l
107-06-2 1,2-Dichloroethane 8.2 25 6.3 ug/l J
75-35-4 1,1-Dichloroethylene ND 25 6.3 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 25 6.3 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 25 6.3 ug/l
78-87-5 1,2-Dichloropropane ND 25 6.3 ug/l
142-28-9 1,3-Dichloropropane ND 25 6.3 ug/l
594-20-7 2,2-Dichloropropane ND 25 6.3 ug/l
563-58-6 1,1-Dichloropropene ND 25 6.3 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 25 6.3 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 25 6.3 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
20 of 45
FA5152533.7
SGS LabLink@184098 08:48 15-Feb-2018
Report of Analysis Page 2 of 2
Client Sample ID:WMW-12
Lab Sample ID:FA51525-7 Date Sampled:02/01/18
Matrix:AQ - Ground Water Date Received:02/02/18
Method:SM 6200B Percent Solids:n/a
Project:Myer's Grocery & White's Grocery; SR 1001 & Waketon Rd, Colerain, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 25 6.3 ug/l
100-41-4 Ethylbenzene 1070 25 6.3 ug/l
87-68-3 Hexachlorobutadiene ND 25 6.3 ug/l
98-82-8 Isopropylbenzene 59.8 25 6.3 ug/l
99-87-6 p-Isopropyltoluene ND 25 6.3 ug/l
74-83-9 Methyl Bromide ND 25 10 ug/l
74-87-3 Methyl Chloride ND 25 10 ug/l
74-95-3 Methylene Bromide ND 25 6.3 ug/l
75-09-2 Methylene Chloride ND 100 50 ug/l
1634-04-4 Methyl Tert Butyl Ether 169 25 6.3 ug/l
91-20-3 Naphthalene 48.4 25 6.3 ug/l
103-65-1 n-Propylbenzene 144 25 6.3 ug/l
100-42-5 Styrene ND 25 6.3 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 25 6.3 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 25 6.3 ug/l
127-18-4 Tetrachloroethylene ND 25 6.3 ug/l
108-88-3 Toluene 335 25 6.3 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 25 6.3 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 25 6.3 ug/l
71-55-6 1,1,1-Trichloroethane ND 25 6.3 ug/l
79-00-5 1,1,2-Trichloroethane ND 25 6.3 ug/l
79-01-6 Trichloroethylene ND 25 6.3 ug/l
75-69-4 Trichlorofluoromethane ND 25 10 ug/l
96-18-4 1,2,3-Trichloropropane ND 25 6.3 ug/l
95-63-6 1,2,4-Trimethylbenzene 855 25 6.3 ug/l
108-67-8 1,3,5-Trimethylbenzene 204 25 6.3 ug/l
75-01-4 Vinyl Chloride ND 25 6.3 ug/l
m,p-Xylene 3880 50 6.3 ug/l
95-47-6 o-Xylene 1880 25 6.3 ug/l
1330-20-7 Xylene (total)5760 75 13 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 97%70-130%
17060-07-0 1,2-Dichloroethane-D4 97%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
21 of 45
FA5152533.7
SGS LabLink@184098 08:48 15-Feb-2018
Report of Analysis Page 1 of 2
Client Sample ID:WMW-15
Lab Sample ID:FA51525-8 Date Sampled:02/01/18
Matrix:AQ - Ground Water Date Received:02/02/18
Method:SM 6200B Percent Solids:n/a
Project:Myer's Grocery & White's Grocery; SR 1001 & Waketon Rd, Colerain, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0211557.D 20 02/08/18 15:56 TD n/a n/a VA2315
Run #2 A0211527.D 50 02/07/18 17:01 TD n/a n/a VA2314
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 303 10 2.5 ug/l
108-86-1 Bromobenzene ND 10 2.5 ug/l
74-97-5 Bromochloromethane ND 10 2.5 ug/l
75-27-4 Bromodichloromethane ND 10 2.5 ug/l
75-25-2 Bromoform ND 10 2.5 ug/l
104-51-8 n-Butylbenzene 3.3 10 2.5 ug/l J
135-98-8 sec-Butylbenzene 4.7 10 2.5 ug/l J
98-06-6 tert-Butylbenzene ND 10 2.5 ug/l
56-23-5 Carbon Tetrachloride ND 10 2.5 ug/l
108-90-7 Chlorobenzene ND 10 2.5 ug/l
75-00-3 Chloroethane ND 10 4.0 ug/l
67-66-3 Chloroform ND 10 2.5 ug/l
95-49-8 o-Chlorotoluene 21.5 10 2.5 ug/l
106-43-4 p-Chlorotoluene ND 10 2.5 ug/l
124-48-1 Dibromochloromethane ND 10 2.5 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 10 4.9 ug/l
106-93-4 1,2-Dibromoethane ND 10 2.5 ug/l
75-71-8 Dichlorodifluoromethane ND 10 4.0 ug/l
95-50-1 1,2-Dichlorobenzene ND 10 2.5 ug/l
541-73-1 1,3-Dichlorobenzene ND 10 2.5 ug/l
106-46-7 1,4-Dichlorobenzene ND 10 2.5 ug/l
75-34-3 1,1-Dichloroethane ND 10 2.5 ug/l
107-06-2 1,2-Dichloroethane ND 10 2.5 ug/l
75-35-4 1,1-Dichloroethylene ND 10 2.5 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 10 2.5 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 10 2.5 ug/l
78-87-5 1,2-Dichloropropane ND 10 2.5 ug/l
142-28-9 1,3-Dichloropropane ND 10 2.5 ug/l
594-20-7 2,2-Dichloropropane ND 10 2.5 ug/l
563-58-6 1,1-Dichloropropene ND 10 2.5 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 10 2.5 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 10 2.5 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
22 of 45
FA5152533.8
SGS LabLink@184098 08:48 15-Feb-2018
Report of Analysis Page 2 of 2
Client Sample ID:WMW-15
Lab Sample ID:FA51525-8 Date Sampled:02/01/18
Matrix:AQ - Ground Water Date Received:02/02/18
Method:SM 6200B Percent Solids:n/a
Project:Myer's Grocery & White's Grocery; SR 1001 & Waketon Rd, Colerain, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 10 2.5 ug/l
100-41-4 Ethylbenzene 735 10 2.5 ug/l
87-68-3 Hexachlorobutadiene ND 10 2.5 ug/l
98-82-8 Isopropylbenzene 60.2 10 2.5 ug/l
99-87-6 p-Isopropyltoluene 2.9 10 2.5 ug/l J
74-83-9 Methyl Bromide ND 10 4.0 ug/l
74-87-3 Methyl Chloride ND 10 4.0 ug/l
74-95-3 Methylene Bromide ND 10 2.5 ug/l
75-09-2 Methylene Chloride ND 40 20 ug/l
1634-04-4 Methyl Tert Butyl Ether 106 10 2.5 ug/l
91-20-3 Naphthalene 79.0 10 2.5 ug/l
103-65-1 n-Propylbenzene 145 10 2.5 ug/l
100-42-5 Styrene ND 10 2.5 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 10 2.5 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 10 2.5 ug/l
127-18-4 Tetrachloroethylene ND 10 2.5 ug/l
108-88-3 Toluene 340 10 2.5 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 10 2.5 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 10 2.5 ug/l
71-55-6 1,1,1-Trichloroethane ND 10 2.5 ug/l
79-00-5 1,1,2-Trichloroethane ND 10 2.5 ug/l
79-01-6 Trichloroethylene ND 10 2.5 ug/l
75-69-4 Trichlorofluoromethane ND 10 4.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 10 2.5 ug/l
95-63-6 1,2,4-Trimethylbenzene 760 10 2.5 ug/l
108-67-8 1,3,5-Trimethylbenzene 191 10 2.5 ug/l
75-01-4 Vinyl Chloride ND 10 2.5 ug/l
m,p-Xylene 2300 a 50 6.3 ug/l
95-47-6 o-Xylene 1130 a 25 6.3 ug/l
1330-20-7 Xylene (total)3420 a 75 13 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 97%97%70-130%
17060-07-0 1,2-Dichloroethane-D4 96%96%70-130%
2037-26-5 Toluene-D8 100%98%70-130%
460-00-4 4-Bromofluorobenzene 101%101%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
23 of 45
FA5152533.8
SGS LabLink@184098 08:48 15-Feb-2018
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Orlando, FL
Section 4
24 of 45
FA515254
FA51525: Chain of Custody
Page 1 of 2
25 of 45
FA5152544.1
Job Number:FA51525 Client:GRI
Date / Time Received:2/2/2018 9:15:00 AM Delivery Method:FX
Project:2857
Airbill #'s:8110 6225 0177
Cooler Information
1. Custody Seals Present
2. Custody Seals Intact
4. Cooler temp verification
3. Temp criteria achieved
5. Cooler media
IR Gun
Ice (Bag)
Trip Blank Information
1. Trip Blank present / cooler
2. Trip Blank listed on COC
2. Samples preserved properly
Sample Information
1. Sample labels present on bottles
5. Sample recvd within HT
4. Condition of sample
3. Sufficient volume/containers recvd for analysis:
Intact
Comments
SM001Rev. Date 05/24/17
SGS Sample Receipt Summary
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
Cooler 1: (2.6);
Cooler 1: (3.0);
3. Type Of TB Received
W or S N/A
6. Dates/Times/IDs on COC match Sample Label
7. VOCs have headspace
8. Bottles received for unspecified tests
9. Compositing instructions clear
10. Voa Soil Kits/Jars received past 48hrs?
11. % Solids Jar received?
Misc. Information
25-Gram 5-GramNumber of Encores:Number of 5035 Field Kits:Number of Lab Filtered Metals:
Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify)
Y or N N/A
Y or N
Therm ID:IR 1; Therm CF:0.4; # of Coolers:1
Y or N N/A
12. Residual Chlorine Present?
Residual Chlorine Test Strip Lot #:
Technician:Reviewer:JORGEC P.H Date:2/2/2018Date:2/2/2018 9:15:00 AM
FA51525: Chain of Custody
Page 2 of 2
26 of 45
FA5152544.1
SGS LabLink@184098 08:48 15-Feb-2018
MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 5
27 of 45
FA515255
Method Blank Summary Page 1 of 2
Job Number:FA51525
Account:GRINCC GRI (Geological Resources Inc.)
Project:Myer's Grocery & White's Grocery; SR 1001 & Waketon Rd, Colerain, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2313-MB A0211485.D 1 02/06/18 TD n/a n/a VA2313
The QC reported here applies to the following samples:Method: SM 6200B
FA51525-1, FA51525-2, FA51525-3
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
28 of 45
FA5152555.1.1
Method Blank Summary Page 2 of 2
Job Number:FA51525
Account:GRINCC GRI (Geological Resources Inc.)
Project:Myer's Grocery & White's Grocery; SR 1001 & Waketon Rd, Colerain, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2313-MB A0211485.D 1 02/06/18 TD n/a n/a VA2313
The QC reported here applies to the following samples:Method: SM 6200B
FA51525-1, FA51525-2, FA51525-3
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
29 of 45
FA5152555.1.1
Method Blank Summary Page 1 of 2
Job Number:FA51525
Account:GRINCC GRI (Geological Resources Inc.)
Project:Myer's Grocery & White's Grocery; SR 1001 & Waketon Rd, Colerain, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2314-MB A0211515.D 1 02/07/18 TD n/a n/a VA2314
The QC reported here applies to the following samples:Method: SM 6200B
FA51525-1, FA51525-4, FA51525-5, FA51525-6, FA51525-7, FA51525-8
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
30 of 45
FA5152555.1.2
Method Blank Summary Page 2 of 2
Job Number:FA51525
Account:GRINCC GRI (Geological Resources Inc.)
Project:Myer's Grocery & White's Grocery; SR 1001 & Waketon Rd, Colerain, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2314-MB A0211515.D 1 02/07/18 TD n/a n/a VA2314
The QC reported here applies to the following samples:Method: SM 6200B
FA51525-1, FA51525-4, FA51525-5, FA51525-6, FA51525-7, FA51525-8
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 96%70-130%
17060-07-0 1,2-Dichloroethane-D4 93%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
31 of 45
FA5152555.1.2
Method Blank Summary Page 1 of 2
Job Number:FA51525
Account:GRINCC GRI (Geological Resources Inc.)
Project:Myer's Grocery & White's Grocery; SR 1001 & Waketon Rd, Colerain, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2315-MB A0211553.D 1 02/08/18 TD n/a n/a VA2315
The QC reported here applies to the following samples:Method: SM 6200B
FA51525-8
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
32 of 45
FA5152555.1.3
Method Blank Summary Page 2 of 2
Job Number:FA51525
Account:GRINCC GRI (Geological Resources Inc.)
Project:Myer's Grocery & White's Grocery; SR 1001 & Waketon Rd, Colerain, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2315-MB A0211553.D 1 02/08/18 TD n/a n/a VA2315
The QC reported here applies to the following samples:Method: SM 6200B
FA51525-8
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 99%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
33 of 45
FA5152555.1.3
Blank Spike Summary Page 1 of 2
Job Number:FA51525
Account:GRINCC GRI (Geological Resources Inc.)
Project:Myer's Grocery & White's Grocery; SR 1001 & Waketon Rd, Colerain, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2313-BS A0211486.D 1 02/06/18 TD n/a n/a VA2313
The QC reported here applies to the following samples:Method: SM 6200B
FA51525-1, FA51525-2, FA51525-3
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 8.1 81 70-130
108-86-1 Bromobenzene 10 8.0 80 70-130
74-97-5 Bromochloromethane 10 7.9 79 70-130
75-27-4 Bromodichloromethane 10 8.5 85 70-130
75-25-2 Bromoform 10 8.0 80 70-130
104-51-8 n-Butylbenzene 10 8.5 85 70-130
135-98-8 sec-Butylbenzene 10 8.6 86 70-130
98-06-6 tert-Butylbenzene 10 8.2 82 70-130
56-23-5 Carbon Tetrachloride 10 9.1 91 70-130
108-90-7 Chlorobenzene 10 8.1 81 70-130
75-00-3 Chloroethane 10 10.4 104 60-140
67-66-3 Chloroform 10 8.1 81 70-130
95-49-8 o-Chlorotoluene 10 8.1 81 70-130
106-43-4 p-Chlorotoluene 10 8.2 82 70-130
124-48-1 Dibromochloromethane 10 8.1 81 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 7.5 75 70-130
106-93-4 1,2-Dibromoethane 10 7.9 79 70-130
75-71-8 Dichlorodifluoromethane 10 9.1 91 60-140
95-50-1 1,2-Dichlorobenzene 10 7.9 79 70-130
541-73-1 1,3-Dichlorobenzene 10 8.1 81 70-130
106-46-7 1,4-Dichlorobenzene 10 8.0 80 70-130
75-34-3 1,1-Dichloroethane 10 8.7 87 70-130
107-06-2 1,2-Dichloroethane 10 8.2 82 70-130
75-35-4 1,1-Dichloroethylene 10 9.0 90 70-130
156-59-2 cis-1,2-Dichloroethylene 10 8.4 84 70-130
156-60-5 trans-1,2-Dichloroethylene 10 9.0 90 70-130
78-87-5 1,2-Dichloropropane 10 8.2 82 70-130
142-28-9 1,3-Dichloropropane 10 7.5 75 70-130
594-20-7 2,2-Dichloropropane 10 8.8 88 70-130
563-58-6 1,1-Dichloropropene 10 8.3 83 70-130
10061-01-5 cis-1,3-Dichloropropene 10 7.7 77 70-130
10061-02-6 trans-1,3-Dichloropropene 10 7.6 76 70-130
108-20-3 Di-Isopropyl Ether 10 8.2 82 70-130
100-41-4 Ethylbenzene 10 8.1 81 70-130
87-68-3 Hexachlorobutadiene 10 8.6 86 70-130
98-82-8 Isopropylbenzene 10 8.6 86 70-130
* = Outside of Control Limits.
34 of 45
FA5152555.2.1
Blank Spike Summary Page 2 of 2
Job Number:FA51525
Account:GRINCC GRI (Geological Resources Inc.)
Project:Myer's Grocery & White's Grocery; SR 1001 & Waketon Rd, Colerain, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2313-BS A0211486.D 1 02/06/18 TD n/a n/a VA2313
The QC reported here applies to the following samples:Method: SM 6200B
FA51525-1, FA51525-2, FA51525-3
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 8.6 86 70-130
74-83-9 Methyl Bromide 10 11.4 114 60-140
74-87-3 Methyl Chloride 10 9.8 98 60-140
74-95-3 Methylene Bromide 10 8.1 81 70-130
75-09-2 Methylene Chloride 10 8.5 85 70-130
1634-04-4 Methyl Tert Butyl Ether 10 8.0 80 70-130
91-20-3 Naphthalene 10 7.3 73 70-130
103-65-1 n-Propylbenzene 10 8.2 82 70-130
100-42-5 Styrene 10 8.2 82 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 8.3 83 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 7.8 78 70-130
127-18-4 Tetrachloroethylene 10 8.4 84 70-130
108-88-3 Toluene 10 8.0 80 70-130
87-61-6 1,2,3-Trichlorobenzene 10 7.7 77 70-130
120-82-1 1,2,4-Trichlorobenzene 10 8.2 82 70-130
71-55-6 1,1,1-Trichloroethane 10 8.4 84 70-130
79-00-5 1,1,2-Trichloroethane 10 7.9 79 70-130
79-01-6 Trichloroethylene 10 8.5 85 70-130
75-69-4 Trichlorofluoromethane 10 9.9 99 60-140
96-18-4 1,2,3-Trichloropropane 10 7.7 77 70-130
95-63-6 1,2,4-Trimethylbenzene 10 8.1 81 70-130
108-67-8 1,3,5-Trimethylbenzene 10 8.4 84 70-130
75-01-4 Vinyl Chloride 10 9.6 96 60-140
m,p-Xylene 20 17.1 86 70-130
95-47-6 o-Xylene 10 8.0 80 70-130
1330-20-7 Xylene (total)30 25.1 84 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
* = Outside of Control Limits.
35 of 45
FA5152555.2.1
Blank Spike Summary Page 1 of 2
Job Number:FA51525
Account:GRINCC GRI (Geological Resources Inc.)
Project:Myer's Grocery & White's Grocery; SR 1001 & Waketon Rd, Colerain, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2314-BS A0211519.D 1 02/07/18 TD n/a n/a VA2314
The QC reported here applies to the following samples:Method: SM 6200B
FA51525-1, FA51525-4, FA51525-5, FA51525-6, FA51525-7, FA51525-8
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 10 100 70-130
108-86-1 Bromobenzene 10 10.3 103 70-130
74-97-5 Bromochloromethane 10 9.8 98 70-130
75-27-4 Bromodichloromethane 10 9.9 99 70-130
75-25-2 Bromoform 10 10.5 105 70-130
104-51-8 n-Butylbenzene 10 10.8 108 70-130
135-98-8 sec-Butylbenzene 10 11.0 110 70-130
98-06-6 tert-Butylbenzene 10 10.3 103 70-130
56-23-5 Carbon Tetrachloride 10 10.2 102 70-130
108-90-7 Chlorobenzene 10 10.3 103 70-130
75-00-3 Chloroethane 10 10.7 107 60-140
67-66-3 Chloroform 10 9.6 96 70-130
95-49-8 o-Chlorotoluene 10 10.4 104 70-130
106-43-4 p-Chlorotoluene 10 10.4 104 70-130
124-48-1 Dibromochloromethane 10 10.2 102 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 9.8 98 70-130
106-93-4 1,2-Dibromoethane 10 10 100 70-130
75-71-8 Dichlorodifluoromethane 10 8.8 88 60-140
95-50-1 1,2-Dichlorobenzene 10 10.4 104 70-130
541-73-1 1,3-Dichlorobenzene 10 10.6 106 70-130
106-46-7 1,4-Dichlorobenzene 10 10.3 103 70-130
75-34-3 1,1-Dichloroethane 10 10.3 103 70-130
107-06-2 1,2-Dichloroethane 10 9.2 92 70-130
75-35-4 1,1-Dichloroethylene 10 10.1 101 70-130
156-59-2 cis-1,2-Dichloroethylene 10 10.3 103 70-130
156-60-5 trans-1,2-Dichloroethylene 10 10.4 104 70-130
78-87-5 1,2-Dichloropropane 10 9.8 98 70-130
142-28-9 1,3-Dichloropropane 10 9.5 95 70-130
594-20-7 2,2-Dichloropropane 10 10 100 70-130
563-58-6 1,1-Dichloropropene 10 9.7 97 70-130
10061-01-5 cis-1,3-Dichloropropene 10 9.4 94 70-130
10061-02-6 trans-1,3-Dichloropropene 10 9.6 96 70-130
108-20-3 Di-Isopropyl Ether 10 9.5 95 70-130
100-41-4 Ethylbenzene 10 10.1 101 70-130
87-68-3 Hexachlorobutadiene 10 10.6 106 70-130
98-82-8 Isopropylbenzene 10 11.1 111 70-130
* = Outside of Control Limits.
36 of 45
FA5152555.2.2
Blank Spike Summary Page 2 of 2
Job Number:FA51525
Account:GRINCC GRI (Geological Resources Inc.)
Project:Myer's Grocery & White's Grocery; SR 1001 & Waketon Rd, Colerain, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2314-BS A0211519.D 1 02/07/18 TD n/a n/a VA2314
The QC reported here applies to the following samples:Method: SM 6200B
FA51525-1, FA51525-4, FA51525-5, FA51525-6, FA51525-7, FA51525-8
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 11.1 111 70-130
74-83-9 Methyl Bromide 10 11.3 113 60-140
74-87-3 Methyl Chloride 10 10.0 100 60-140
74-95-3 Methylene Bromide 10 9.8 98 70-130
75-09-2 Methylene Chloride 10 8.9 89 70-130
1634-04-4 Methyl Tert Butyl Ether 10 9.5 95 70-130
91-20-3 Naphthalene 10 11.7 117 70-130
103-65-1 n-Propylbenzene 10 10.6 106 70-130
100-42-5 Styrene 10 10.7 107 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 10.5 105 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 10.2 102 70-130
127-18-4 Tetrachloroethylene 10 10.6 106 70-130
108-88-3 Toluene 10 10.3 103 70-130
87-61-6 1,2,3-Trichlorobenzene 10 11.4 114 70-130
120-82-1 1,2,4-Trichlorobenzene 10 11.1 111 70-130
71-55-6 1,1,1-Trichloroethane 10 9.6 96 70-130
79-00-5 1,1,2-Trichloroethane 10 10.1 101 70-130
79-01-6 Trichloroethylene 10 10.3 103 70-130
75-69-4 Trichlorofluoromethane 10 9.3 93 60-140
96-18-4 1,2,3-Trichloropropane 10 10.0 100 70-130
95-63-6 1,2,4-Trimethylbenzene 10 10.5 105 70-130
108-67-8 1,3,5-Trimethylbenzene 10 10.9 109 70-130
75-01-4 Vinyl Chloride 10 10.3 103 60-140
m,p-Xylene 20 21.6 108 70-130
95-47-6 o-Xylene 10 10.3 103 70-130
1330-20-7 Xylene (total)30 32.0 107 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 98%70-130%
17060-07-0 1,2-Dichloroethane-D4 95%70-130%
2037-26-5 Toluene-D8 102%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
* = Outside of Control Limits.
37 of 45
FA5152555.2.2
Blank Spike Summary Page 1 of 2
Job Number:FA51525
Account:GRINCC GRI (Geological Resources Inc.)
Project:Myer's Grocery & White's Grocery; SR 1001 & Waketon Rd, Colerain, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2315-BS A0211554.D 1 02/08/18 TD n/a n/a VA2315
The QC reported here applies to the following samples:Method: SM 6200B
FA51525-8
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 9.5 95 70-130
108-86-1 Bromobenzene 10 9.8 98 70-130
74-97-5 Bromochloromethane 10 9.6 96 70-130
75-27-4 Bromodichloromethane 10 9.8 98 70-130
75-25-2 Bromoform 10 9.6 96 70-130
104-51-8 n-Butylbenzene 10 10.3 103 70-130
135-98-8 sec-Butylbenzene 10 10.5 105 70-130
98-06-6 tert-Butylbenzene 10 10.2 102 70-130
56-23-5 Carbon Tetrachloride 10 10.1 101 70-130
108-90-7 Chlorobenzene 10 9.8 98 70-130
75-00-3 Chloroethane 10 8.6 86 60-140
67-66-3 Chloroform 10 9.4 94 70-130
95-49-8 o-Chlorotoluene 10 9.9 99 70-130
106-43-4 p-Chlorotoluene 10 9.9 99 70-130
124-48-1 Dibromochloromethane 10 9.7 97 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 9.1 91 70-130
106-93-4 1,2-Dibromoethane 10 9.7 97 70-130
75-71-8 Dichlorodifluoromethane 10 7.1 71 60-140
95-50-1 1,2-Dichlorobenzene 10 9.8 98 70-130
541-73-1 1,3-Dichlorobenzene 10 10.2 102 70-130
106-46-7 1,4-Dichlorobenzene 10 9.7 97 70-130
75-34-3 1,1-Dichloroethane 10 10 100 70-130
107-06-2 1,2-Dichloroethane 10 9.3 93 70-130
75-35-4 1,1-Dichloroethylene 10 9.9 99 70-130
156-59-2 cis-1,2-Dichloroethylene 10 9.9 99 70-130
156-60-5 trans-1,2-Dichloroethylene 10 10.1 101 70-130
78-87-5 1,2-Dichloropropane 10 9.4 94 70-130
142-28-9 1,3-Dichloropropane 10 9.0 90 70-130
594-20-7 2,2-Dichloropropane 10 9.6 96 70-130
563-58-6 1,1-Dichloropropene 10 9.4 94 70-130
10061-01-5 cis-1,3-Dichloropropene 10 9.0 90 70-130
10061-02-6 trans-1,3-Dichloropropene 10 9.0 90 70-130
108-20-3 Di-Isopropyl Ether 10 9.1 91 70-130
100-41-4 Ethylbenzene 10 9.6 96 70-130
87-68-3 Hexachlorobutadiene 10 10.6 106 70-130
98-82-8 Isopropylbenzene 10 10.4 104 70-130
* = Outside of Control Limits.
38 of 45
FA5152555.2.3
Blank Spike Summary Page 2 of 2
Job Number:FA51525
Account:GRINCC GRI (Geological Resources Inc.)
Project:Myer's Grocery & White's Grocery; SR 1001 & Waketon Rd, Colerain, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2315-BS A0211554.D 1 02/08/18 TD n/a n/a VA2315
The QC reported here applies to the following samples:Method: SM 6200B
FA51525-8
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 10.6 106 70-130
74-83-9 Methyl Bromide 10 9.6 96 60-140
74-87-3 Methyl Chloride 10 8.6 86 60-140
74-95-3 Methylene Bromide 10 9.6 96 70-130
75-09-2 Methylene Chloride 10 8.7 87 70-130
1634-04-4 Methyl Tert Butyl Ether 10 9.2 92 70-130
91-20-3 Naphthalene 10 8.9 89 70-130
103-65-1 n-Propylbenzene 10 10.1 101 70-130
100-42-5 Styrene 10 10.0 100 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 9.9 99 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 9.5 95 70-130
127-18-4 Tetrachloroethylene 10 10.2 102 70-130
108-88-3 Toluene 10 9.7 97 70-130
87-61-6 1,2,3-Trichlorobenzene 10 9.6 96 70-130
120-82-1 1,2,4-Trichlorobenzene 10 10.1 101 70-130
71-55-6 1,1,1-Trichloroethane 10 9.5 95 70-130
79-00-5 1,1,2-Trichloroethane 10 9.6 96 70-130
79-01-6 Trichloroethylene 10 10.0 100 70-130
75-69-4 Trichlorofluoromethane 10 8.2 82 60-140
96-18-4 1,2,3-Trichloropropane 10 9.6 96 70-130
95-63-6 1,2,4-Trimethylbenzene 10 9.9 99 70-130
108-67-8 1,3,5-Trimethylbenzene 10 10.3 103 70-130
75-01-4 Vinyl Chloride 10 8.3 83 60-140
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 101%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
* = Outside of Control Limits.
39 of 45
FA5152555.2.3
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA51525
Account:GRINCC GRI (Geological Resources Inc.)
Project:Myer's Grocery & White's Grocery; SR 1001 & Waketon Rd, Colerain, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA51525-1MS A0211508.D 200 02/06/18 TD n/a n/a VA2313
FA51525-1MSD A0211509.D 200 02/06/18 TD n/a n/a VA2313
FA51525-1 A0211498.D 200 02/06/18 TD n/a n/a VA2313
The QC reported here applies to the following samples:Method: SM 6200B
FA51525-1, FA51525-2, FA51525-3
FA51525-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 3230 2000 5380 108 2000 5230 100 3 70-130/20
108-86-1 Bromobenzene ND 2000 2060 103 2000 2060 103 0 70-130/20
74-97-5 Bromochloromethane ND 2000 1940 97 2000 1900 95 2 70-130/20
75-27-4 Bromodichloromethane ND 2000 1860 93 2000 1900 95 2 70-130/20
75-25-2 Bromoform ND 2000 1600 80 2000 1870 94 16 70-130/20
104-51-8 n-Butylbenzene ND 2000 2180 109 2000 2140 107 2 70-130/20
135-98-8 sec-Butylbenzene ND 2000 2220 111 2000 2170 109 2 70-130/20
98-06-6 tert-Butylbenzene ND 2000 2050 103 2000 2020 101 1 70-130/20
56-23-5 Carbon Tetrachloride ND 2000 2000 100 2000 1880 94 6 70-130/20
108-90-7 Chlorobenzene ND 2000 2050 103 2000 2000 100 2 70-130/20
75-00-3 Chloroethane ND 2000 1750 88 2000 1660 83 5 60-140/20
67-66-3 Chloroform ND 2000 1940 97 2000 1870 94 4 70-130/20
95-49-8 o-Chlorotoluene ND 2000 2140 107 2000 2100 105 2 70-130/20
106-43-4 p-Chlorotoluene ND 2000 2040 102 2000 2030 102 0 70-130/20
124-48-1 Dibromochloromethane ND 2000 1740 87 2000 1900 95 9 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 2000 2000 100 2000 1850 93 8 70-130/20
106-93-4 1,2-Dibromoethane ND 2000 2000 100 2000 2020 101 1 70-130/20
75-71-8 Dichlorodifluoromethane ND 2000 1480 74 2000 1370 69 8 60-140/20
95-50-1 1,2-Dichlorobenzene ND 2000 2040 102 2000 2020 101 1 70-130/20
541-73-1 1,3-Dichlorobenzene ND 2000 2130 107 2000 2080 104 2 70-130/20
106-46-7 1,4-Dichlorobenzene ND 2000 2010 101 2000 1970 99 2 70-130/20
75-34-3 1,1-Dichloroethane ND 2000 2070 104 2000 1960 98 5 70-130/20
107-06-2 1,2-Dichloroethane ND 2000 1790 90 2000 1770 89 1 70-130/20
75-35-4 1,1-Dichloroethylene ND 2000 2030 102 2000 1910 96 6 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 2000 2090 105 2000 2000 100 4 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 2000 2070 104 2000 1960 98 5 70-130/20
78-87-5 1,2-Dichloropropane ND 2000 1940 97 2000 1950 98 1 70-130/20
142-28-9 1,3-Dichloropropane ND 2000 1880 94 2000 1880 94 0 70-130/20
594-20-7 2,2-Dichloropropane ND 2000 1850 93 2000 1770 89 4 70-130/20
563-58-6 1,1-Dichloropropene ND 2000 1950 98 2000 1880 94 4 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 2000 1830 92 2000 1820 91 1 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 2000 1820 91 2000 1840 92 1 70-130/20
108-20-3 Di-Isopropyl Ether 758 2000 2690 97 2000 2630 94 2 70-130/20
100-41-4 Ethylbenzene 1970 2000 4110 107 2000 3950 99 4 70-130/20
87-68-3 Hexachlorobutadiene ND 2000 2090 105 2000 2030 102 3 70-130/20
98-82-8 Isopropylbenzene 106 2000 2330 111 2000 2220 106 5 70-130/20
* = Outside of Control Limits.
40 of 45
FA5152555.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA51525
Account:GRINCC GRI (Geological Resources Inc.)
Project:Myer's Grocery & White's Grocery; SR 1001 & Waketon Rd, Colerain, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA51525-1MS A0211508.D 200 02/06/18 TD n/a n/a VA2313
FA51525-1MSD A0211509.D 200 02/06/18 TD n/a n/a VA2313
FA51525-1 A0211498.D 200 02/06/18 TD n/a n/a VA2313
The QC reported here applies to the following samples:Method: SM 6200B
FA51525-1, FA51525-2, FA51525-3
FA51525-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 2000 2210 111 2000 2210 111 0 70-130/20
74-83-9 Methyl Bromide ND 2000 1870 94 2000 1780 89 5 60-140/20
74-87-3 Methyl Chloride ND 2000 1790 90 2000 1670 84 7 60-140/20
74-95-3 Methylene Bromide ND 2000 1920 96 2000 1900 95 1 70-130/20
75-09-2 Methylene Chloride ND 2000 1820 91 2000 1740 87 4 70-130/20
1634-04-4 Methyl Tert Butyl Ether 544 2000 2480 97 2000 2430 94 2 70-130/20
91-20-3 Naphthalene 470 2000 2520 103 2000 2630 108 4 70-130/20
103-65-1 n-Propylbenzene 263 2000 2390 106 2000 2370 105 1 70-130/20
100-42-5 Styrene 39.0 J 2000 2180 107 2000 2150 106 1 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 2000 2070 104 2000 1980 99 4 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 2000 2100 105 2000 2130 107 1 70-130/20
127-18-4 Tetrachloroethylene ND 2000 2110 106 2000 1980 99 6 70-130/20
108-88-3 Toluene 14200 E 2000 16100 95 2000 15300 55* a 5 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 2000 2010 101 2000 2060 103 2 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 2000 2130 107 2000 2100 105 1 70-130/20
71-55-6 1,1,1-Trichloroethane ND 2000 1890 95 2000 1810 91 4 70-130/20
79-00-5 1,1,2-Trichloroethane ND 2000 2100 105 2000 2050 103 2 70-130/20
79-01-6 Trichloroethylene ND 2000 2010 101 2000 1950 98 3 70-130/20
75-69-4 Trichlorofluoromethane ND 2000 1540 77 2000 1450 73 6 60-140/20
96-18-4 1,2,3-Trichloropropane ND 2000 1980 99 2000 1950 98 2 70-130/20
95-63-6 1,2,4-Trimethylbenzene 2750 2000 4900 108 2000 4800 103 2 70-130/20
108-67-8 1,3,5-Trimethylbenzene 735 2000 2940 110 2000 2880 107 2 70-130/20
75-01-4 Vinyl Chloride ND 2000 1720 86 2000 1660 83 4 60-140/20
m,p-Xylene 6730 4000 11300 114 4000 10900 104 4 70-130/20
95-47-6 o-Xylene 3730 2000 5990 113 2000 5710 99 5 70-130/20
1330-20-7 Xylene (total)10500 6000 17300 113 6000 16600 102 4 70-130/20
CAS No.Surrogate Recoveries MS MSD FA51525-1 Limits
1868-53-7 Dibromofluoromethane 96%95%94%70-130%
17060-07-0 1,2-Dichloroethane-D4 93%91%89%70-130%
2037-26-5 Toluene-D8 102%101%101%70-130%
460-00-4 4-Bromofluorobenzene 98%100%99%70-130%
(a) Outside control limits due to high level in sample relative to spike amount.
* = Outside of Control Limits.
41 of 45
FA5152555.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA51525
Account:GRINCC GRI (Geological Resources Inc.)
Project:Myer's Grocery & White's Grocery; SR 1001 & Waketon Rd, Colerain, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA51525-4MS A0211539.D 20 02/07/18 TD n/a n/a VA2314
FA51525-4MSD A0211540.D 20 02/07/18 TD n/a n/a VA2314
FA51525-4 A0211521.D 20 02/07/18 TD n/a n/a VA2314
The QC reported here applies to the following samples:Method: SM 6200B
FA51525-1, FA51525-4, FA51525-5, FA51525-6, FA51525-7, FA51525-8
FA51525-4 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 14.8 200 225 105 200 220 103 2 70-130/20
108-86-1 Bromobenzene ND 200 220 110 200 214 107 3 70-130/20
74-97-5 Bromochloromethane ND 200 206 103 200 200 100 3 70-130/20
75-27-4 Bromodichloromethane ND 200 194 97 200 183 92 6 70-130/20
75-25-2 Bromoform ND 200 150 75 200 154 77 3 70-130/20
104-51-8 n-Butylbenzene 11.7 200 245 117 200 235 112 4 70-130/20
135-98-8 sec-Butylbenzene 7.7 J 200 240 116 200 231 112 4 70-130/20
98-06-6 tert-Butylbenzene ND 200 219 110 200 213 107 3 70-130/20
56-23-5 Carbon Tetrachloride ND 200 205 103 200 187 94 9 70-130/20
108-90-7 Chlorobenzene ND 200 214 107 200 210 105 2 70-130/20
75-00-3 Chloroethane ND 200 187 94 200 191 96 2 60-140/20
67-66-3 Chloroform ND 200 205 103 200 198 99 3 70-130/20
95-49-8 o-Chlorotoluene ND 200 240 120 200 230 115 4 70-130/20
106-43-4 p-Chlorotoluene ND 200 222 111 200 210 105 6 70-130/20
124-48-1 Dibromochloromethane ND 200 175 88 200 172 86 2 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 200 224 112 200 220 110 2 70-130/20
106-93-4 1,2-Dibromoethane ND 200 214 107 200 213 107 0 70-130/20
75-71-8 Dichlorodifluoromethane ND 200 157 79 200 151 76 4 60-140/20
95-50-1 1,2-Dichlorobenzene ND 200 218 109 200 213 107 2 70-130/20
541-73-1 1,3-Dichlorobenzene ND 200 225 113 200 215 108 5 70-130/20
106-46-7 1,4-Dichlorobenzene ND 200 214 107 200 207 104 3 70-130/20
75-34-3 1,1-Dichloroethane ND 200 213 107 200 208 104 2 70-130/20
107-06-2 1,2-Dichloroethane ND 200 196 98 200 190 95 3 70-130/20
75-35-4 1,1-Dichloroethylene ND 200 207 104 200 202 101 2 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 200 217 109 200 212 106 2 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 200 213 107 200 204 102 4 70-130/20
78-87-5 1,2-Dichloropropane ND 200 205 103 200 203 102 1 70-130/20
142-28-9 1,3-Dichloropropane ND 200 202 101 200 200 100 1 70-130/20
594-20-7 2,2-Dichloropropane ND 200 194 97 200 191 96 2 70-130/20
563-58-6 1,1-Dichloropropene ND 200 205 103 200 194 97 6 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 200 185 93 200 161 81 14 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 200 188 94 200 167 84 12 70-130/20
108-20-3 Di-Isopropyl Ether ND 200 195 98 200 193 97 1 70-130/20
100-41-4 Ethylbenzene 459 200 657 99 200 637 89 3 70-130/20
87-68-3 Hexachlorobutadiene ND 200 217 109 200 213 107 2 70-130/20
98-82-8 Isopropylbenzene 51.0 200 281 115 200 276 113 2 70-130/20
* = Outside of Control Limits.
42 of 45
FA5152555.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA51525
Account:GRINCC GRI (Geological Resources Inc.)
Project:Myer's Grocery & White's Grocery; SR 1001 & Waketon Rd, Colerain, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA51525-4MS A0211539.D 20 02/07/18 TD n/a n/a VA2314
FA51525-4MSD A0211540.D 20 02/07/18 TD n/a n/a VA2314
FA51525-4 A0211521.D 20 02/07/18 TD n/a n/a VA2314
The QC reported here applies to the following samples:Method: SM 6200B
FA51525-1, FA51525-4, FA51525-5, FA51525-6, FA51525-7, FA51525-8
FA51525-4 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene 4.0 J 200 238 117 200 228 112 4 70-130/20
74-83-9 Methyl Bromide ND 200 161 81 200 175 88 8 60-140/20
74-87-3 Methyl Chloride ND 200 154 77 200 148 74 4 60-140/20
74-95-3 Methylene Bromide ND 200 207 104 200 204 102 1 70-130/20
75-09-2 Methylene Chloride ND 200 212 106 200 206 103 3 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 200 196 98 200 196 98 0 70-130/20
91-20-3 Naphthalene 142 200 396 127 200 370 114 7 70-130/20
103-65-1 n-Propylbenzene 120 200 345 113 200 331 106 4 70-130/20
100-42-5 Styrene ND 200 212 106 200 213 107 0 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 200 211 106 200 209 105 1 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 200 220 110 200 217 109 1 70-130/20
127-18-4 Tetrachloroethylene ND 200 221 111 200 210 105 5 70-130/20
108-88-3 Toluene 88.1 200 303 107 200 296 104 2 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 200 217 109 200 219 110 1 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 200 226 113 200 223 112 1 70-130/20
71-55-6 1,1,1-Trichloroethane ND 200 197 99 200 188 94 5 70-130/20
79-00-5 1,1,2-Trichloroethane ND 200 225 113 200 225 113 0 70-130/20
79-01-6 Trichloroethylene ND 200 215 108 200 205 103 5 70-130/20
75-69-4 Trichlorofluoromethane ND 200 166 83 200 159 80 4 60-140/20
96-18-4 1,2,3-Trichloropropane ND 200 208 104 200 207 104 0 70-130/20
95-63-6 1,2,4-Trimethylbenzene 750 200 943 97 200 907 79 4 70-130/20
108-67-8 1,3,5-Trimethylbenzene 197 200 421 112 200 406 105 4 70-130/20
75-01-4 Vinyl Chloride ND 200 195 98 200 190 95 3 60-140/20
m,p-Xylene 997 400 1400 101 400 1360 91 3 70-130/20
95-47-6 o-Xylene 591 200 783 96 200 766 88 2 70-130/20
1330-20-7 Xylene (total)1590 600 2180 98 600 2130 90 2 70-130/20
CAS No.Surrogate Recoveries MS MSD FA51525-4 Limits
1868-53-7 Dibromofluoromethane 97%96%98%70-130%
17060-07-0 1,2-Dichloroethane-D4 96%94%96%70-130%
2037-26-5 Toluene-D8 101%101%100%70-130%
460-00-4 4-Bromofluorobenzene 101%98%99%70-130%
* = Outside of Control Limits.
43 of 45
FA5152555.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA51525
Account:GRINCC GRI (Geological Resources Inc.)
Project:Myer's Grocery & White's Grocery; SR 1001 & Waketon Rd, Colerain, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA51600-4MS A0211570.D 1 02/08/18 TD n/a n/a VA2315
FA51600-4MSD A0211571.D 1 02/08/18 TD n/a n/a VA2315
FA51600-4 a A0211569.D 1 02/08/18 TD n/a n/a VA2315
The QC reported here applies to the following samples:Method: SM 6200B
FA51525-8
FA51600-4 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene ND 10 6.7 67*10 6.4 64*5 70-130/20
108-86-1 Bromobenzene ND 10 7.4 74 10 7.1 71 4 70-130/20
74-97-5 Bromochloromethane ND 10 7.9 79 10 7.6 76 4 70-130/20
75-27-4 Bromodichloromethane 3.9 10 11.8 79 10 10.7 68*10 70-130/20
75-25-2 Bromoform 1.3 10 8.4 71 10 7.4 61*13 70-130/20
104-51-8 n-Butylbenzene ND 10 0.36 4*10 0.37 4*3 70-130/20
135-98-8 sec-Butylbenzene ND 10 ND 0*10 ND 0*nc 70-130/20
98-06-6 tert-Butylbenzene ND 10 ND 0*10 ND 0*nc 70-130/20
56-23-5 Carbon Tetrachloride ND 10 8.6 86 10 7.6 76 12 70-130/20
108-90-7 Chlorobenzene ND 10 8.8 88 10 8.4 84 5 70-130/20
75-00-3 Chloroethane ND 10 11.3 113 10 11.1 111 2 60-140/20
67-66-3 Chloroform 5.9 10 13.5 76 10 12.9 70 5 70-130/20
95-49-8 o-Chlorotoluene ND 10 9.5 95 10 9.1 91 4 70-130/20
106-43-4 p-Chlorotoluene ND 10 7.9 79 10 7.6 76 4 70-130/20
124-48-1 Dibromochloromethane 3.7 10 11.5 78 10 10.3 66*11 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 10 9.3 93 10 9.9 99 6 70-130/20
106-93-4 1,2-Dibromoethane ND 10 7.7 77 10 7.5 75 3 70-130/20
75-71-8 Dichlorodifluoromethane ND 10 9.8 98 10 9.3 93 5 60-140/20
95-50-1 1,2-Dichlorobenzene ND 10 7.8 78 10 7.6 76 3 70-130/20
541-73-1 1,3-Dichlorobenzene ND 10 7.7 77 10 7.4 74 4 70-130/20
106-46-7 1,4-Dichlorobenzene ND 10 7.9 79 10 7.5 75 5 70-130/20
75-34-3 1,1-Dichloroethane ND 10 8.3 83 10 7.9 79 5 70-130/20
107-06-2 1,2-Dichloroethane ND 10 8.1 81 10 7.9 79 2 70-130/20
75-35-4 1,1-Dichloroethylene ND 10 ND 0*10 ND 0*nc 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 10 8.3 83 10 8.3 83 0 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 10 6.7 67*10 6.2 62*8 70-130/20
78-87-5 1,2-Dichloropropane ND 10 7.4 74 10 7.3 73 1 70-130/20
142-28-9 1,3-Dichloropropane ND 10 7.2 72 10 6.9 69*4 70-130/20
594-20-7 2,2-Dichloropropane ND 10 8.2 82 10 7.7 77 6 70-130/20
563-58-6 1,1-Dichloropropene ND 10 ND 0*10 ND 0*nc 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 10 ND 0*10 ND 0*nc 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 10 ND 0*10 ND 0*nc 70-130/20
108-20-3 Di-Isopropyl Ether ND 10 7.5 75 10 7.3 73 3 70-130/20
100-41-4 Ethylbenzene ND 10 2.1 21*10 2.0 20*5 70-130/20
87-68-3 Hexachlorobutadiene ND 10 8.3 83 10 8.0 80 4 70-130/20
98-82-8 Isopropylbenzene ND 10 ND 0*10 ND 0*nc 70-130/20
* = Outside of Control Limits.
44 of 45
FA5152555.3.3
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA51525
Account:GRINCC GRI (Geological Resources Inc.)
Project:Myer's Grocery & White's Grocery; SR 1001 & Waketon Rd, Colerain, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA51600-4MS A0211570.D 1 02/08/18 TD n/a n/a VA2315
FA51600-4MSD A0211571.D 1 02/08/18 TD n/a n/a VA2315
FA51600-4 a A0211569.D 1 02/08/18 TD n/a n/a VA2315
The QC reported here applies to the following samples:Method: SM 6200B
FA51525-8
FA51600-4 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 10 ND 0*10 ND 0*nc 70-130/20
74-83-9 Methyl Bromide ND 10 12.0 120 10 11.2 112 7 60-140/20
74-87-3 Methyl Chloride 0.57 10 11.1 105 10 11.1 105 0 60-140/20
74-95-3 Methylene Bromide ND 10 7.8 78 10 7.6 76 3 70-130/20
75-09-2 Methylene Chloride ND 10 7.7 77 10 7.3 73 5 70-130/20
1634-04-4 Methyl Tert Butyl Ether 0.77 10 8.4 76 10 8.3 75 1 70-130/20
91-20-3 Naphthalene ND 10 ND 0*10 ND 0*nc 70-130/20
103-65-1 n-Propylbenzene ND 10 ND 0*10 ND 0*nc 70-130/20
100-42-5 Styrene ND 10 ND 0*10 ND 0*nc 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 10 8.3 83 10 7.8 78 6 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 10 7.6 76 10 7.6 76 0 70-130/20
127-18-4 Tetrachloroethylene ND 10 8.3 83 10 7.5 75 10 70-130/20
108-88-3 Toluene ND 10 ND 0*10 ND 0*nc 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 10 8.0 80 10 8.2 82 2 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 10 8.1 81 10 8.2 82 1 70-130/20
71-55-6 1,1,1-Trichloroethane ND 10 8.1 81 10 7.7 77 5 70-130/20
79-00-5 1,1,2-Trichloroethane ND 10 7.8 78 10 7.8 78 0 70-130/20
79-01-6 Trichloroethylene ND 10 8.3 83 10 7.8 78 6 70-130/20
75-69-4 Trichlorofluoromethane ND 10 11.4 114 10 10.4 104 9 60-140/20
96-18-4 1,2,3-Trichloropropane ND 10 7.4 74 10 7.6 76 3 70-130/20
95-63-6 1,2,4-Trimethylbenzene ND 10 ND 0*10 ND 0*nc 70-130/20
108-67-8 1,3,5-Trimethylbenzene ND 10 ND 0*10 ND 0*nc 70-130/20
75-01-4 Vinyl Chloride ND 10 ND 0*10 ND 0*nc 60-140/20
CAS No.Surrogate Recoveries MS MSD FA51600-4 Limits
1868-53-7 Dibromofluoromethane 107%105%112%70-130%
17060-07-0 1,2-Dichloroethane-D4 111%108%118%70-130%
2037-26-5 Toluene-D8 59%*72%20%* b 70-130%
460-00-4 4-Bromofluorobenzene 95%98%87%70-130%
(a) Confirmation run.
(b) Outside control limits due to matrix interference.
* = Outside of Control Limits.
45 of 45
FA5152555.3.3