RA-29471_48615_CA_LSA_20220915

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]

September 15, 2022

Mr. John Maloy
NCDEQ-UST Section
Raleigh Regional Office
1628 Mail Service Center
Raleigh, NC 27699-1628

Re: Phase I Limited Site Assessment Report
Flash Market #370
1390 Northwest Maynard Road
Cary, Wake County
North Carolina
Facility ID Number: 0-035687
Incident Number: 48615
GRI Project No: 6117

Dear Mr. Maloy,

Please find enclosed the referenced report for the abovementioned site.
If you have any questions, please contact Laura Minor at 704-845-4010.

Sincerely,
Geological Resources, Inc.

Leslie Maxtone-Graham
Administrative Assistant

Enclosure

Cc: Mr. Scott Gordon; Transit Energy Group, file

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
Engineering Certification: C-2727 • Geology Certification: C-127
Phase I Limited Site Assessment Report
Flash Market #370
1390 Northwest Maynard Road
Cary, Wake County
North Carolina
Facility ID Number: 0-035687
Incident Number: 48615
GRI Project Number: 6117

Prepared for:

Mr. Scott Gordon, NC Remediation Manager
Transit Energy Group
501 River Street, Floor 3
Greenville, SC 29602

September 15, 2022

Laura Minor
Project Manager
Xavier T. Farmer, G.I.T.
Report Writer

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase I Limited Site Assessment Report
Prepared on: September 15, 2022 Flash Market #370
Project Manager: Laura Minor GRI Project No. 6117
i
EXECUTIVE SUMMARY
The Flash Market #370 site is located at 1390 Northwest Maynard Road in Cary, Wake County, North
Carolina. The property operates as a petroleum retail facility and convenience store. The site is covered
by concrete and asphalt. There are one 17,000-gallon gasoline and one 10,000-gallon gasoline USTs
currently in use at the site with six associated gasoline dispenser islands. The surrounding properties are
commercial or residential.

On June 2, 2022, a non-passing spill bucket integrity test was reported. GRI conducted a site check at the
subject site on July 6, 2022. One monitoring well (MW-1) was installed adjacent to the tank #2 spill bucket,
the suspected source of contamination. Soil samples were collected at 10-foot intervals during the
installation of monitoring well MW-1. The concentration of MTBE reported in soil sample SS-1-10’ and
SS-1-30’ exceeded the soil-to-water MCC. A ground water sample was collected from MW-1. The
concentrations of benzene, MTBE, naphthalene, TAA, TBA, C5-C8 aliphatics, and C9-C10 aromatics
reported in the ground water sample collected from MW-1 exceeded the MACs. No free product was
noted at the site. Site Check results identified a release at the site and a LSA was required.

A receptor survey was conducted on September 7, 2022. No water supply wells were identified within a
1,500-foot radius of the site. Public water is available to the subject site and to all surrounding properties.
Two surface water bodies were identified within a 500-foot radius of the site. Coles Branch, a class C/NSW
water, was identified about 250 feet southeast of the site. A retention pond was identified about 400 feet
northeast of the site.

The reported contaminant concentrations do not exceed ten times the NCDEQ surface water standards.
Based on the lack of receptors other than surface water bodies, the availability of municipal water to all
properties in the area, and relatively low ground water contaminant concentrations, GRI recommends the
site be classified as Low Risk and the incident closed after filing a Notice of Residual Petroleum.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase I Limited Site Assessment Report
Prepared on: September 15, 2022 Flash Market #370
Project Manager: Laura Minor GRI Project No. 6117
ii
SITE INFORMATION
1. Site Identification
 Flash Market #370 (Facility ID 0-035687)
 Incident Number 48615 – (Risk Ranking Undetermined)
 Location of Source Area: 1390 Northwest Maynard Road
Cary, NC 27513
Wake County (Figures 1 and 2A)
35.788162°N, 78.809742°W (Topographical Map)
2. Information about Contacts Associated with the Leaking UST System
UST/AST Owner
Flash Market, LLC (Table 1)
501 River Street Floor 3
Greenville, SC 29602
[e-mail]
704-221-3405

UST/AST Operator
Flash Market, LLC (Table 1)
501 River Street Floor 3
Greenville, SC 29602
[e-mail]
704-221-3405

Property Owner
Getty Leasing, Inc.
292 Madison Avenue Floor 9
New York, NY, 11017
Email Unknown
Phone No. Unknown

Property Occupant
Rose Oil Company, Inc
613 US Highway 158 Bypass
Henderson, NC 27537
[e-mail]
252-438-7141

Consultant/Contractor
Geological Resources, Inc.
3502 Hayes Road
Monroe, NC 28110
[e-mail]
704-845-4010

Analytical Laboratory
Waypoint Analytical, LLC
449 Springbrook Road
Charlotte, NC 2821
State Certification No. 402
704-529-6364
3. Information about Release
 Release was discovered on July 20, 2022
 An unknown amount of product was released from the leaking UST System via the non-passing spill
bucket
 One (1) 17,000-gallon gasoline and one (1) 10,000-gallon gasoline USTs are in use at the site (Table 2)

Certification:

I, John M. Brown, a Licensed Geologist for Geological Resources, Inc., do certify that the information
contained in this report is correct and accurate to the best of my knowledge.

Geological Resources, Inc. is licensed to practice geology and engineering in North Carolina. The
certification numbers of the corporation are C-127 and C-2727, respectively.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase I Limited Site Assessment Report
Prepared on: September 15, 2022 Flash Market #370
Project Manager: Laura Minor GRI Project No. 6117
iii
ACRONYMS
ACM: Asbestos Containing Materials
AFVR: Aggressive Fluid-Vapor Recovery
ARR: Acknowledgement of Report Receipt
AS: Air Sparging
AST: Aboveground Storage Tank
ASTM: American Society for Testing and
Materials
BGS: Below Ground Surface
CAP: Corrective Action Plan
CFR: Code of Federal Regulations
CSA: Comprehensive Site Assessment
DPE: Dual Phase Extraction
DRO: Total Petroleum Hydrocarbons Diesel
Range Organics
DWM: Division of Waste Management
DWR: Department of Water Resources
EPA: Environmental Protection Agency
EPH: Extractible Petroleum Hydrocarbons
ESA: Environmental Site Assessment
GCL: Gross Contamination Level
GRI: Geological Resources, Inc.
GRO: Total Petroleum Hydrocarbons
Gasoline Range Organics
LSA: Limited Site Assessment
MAC: Maximum Allowable Concentration as
specified in T15A NCAC 2L.0202
MADEP: Massachusetts Department of
Environmental Protection
MCC: Maximum Contaminant Concentrations
MMPE: Mobile Multi-Phase Extraction
NAPL: Non-Aqueous Phase Liquid, “Free
Product”
NCDEQ: North Carolina Department of
Environmental Quality
NCDOT: North Carolina Department of
Transportation
NFA: Notice of No Further Action
NORR: Notice of Regulatory Requirements
NOV: Notice of Violation
NPDES: National Pollutant Discharge
Elimination System
NRP: Notice of Residual Petroleum
O&M: Operation and Maintenance
PAHs: Polynuclear Aromatic Hydrocarbons
PCA: Pre-Construction Assessment
RAL: Regulatory Action Level
SCLs: Soil Cleanup Level
SPCC: Spill Prevention Control and
Countermeasures
SVE: Soil Vapor Extraction
SVOCs: Semi-Volatile Organic Compounds
SWAP: Source Water Assessment and
Protection
SWPPP: Stormwater Pollution Prevention Plan
TCLP: Toxicity Characteristic Leaching
Procedure (EPA Method SW-846 1311)
TOC: Top of Casing
TPH: Total Petroleum Hydrocarbons
USGS: United States Geological Survey
UST: Underground Storage Tank
UVF: Ultraviolet Fluorescence
VOCs: Volatile Organic Compounds
VPH: Volatile Petroleum Hydrocarbons

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase I Limited Site Assessment Report
Prepared on: September 15, 2022 Flash Market #370
Project Manager: Laura Minor GRI Project No. 6117
TABLE OF CONTENTS

EXECUTIVE SUMMARY ....................................................................................................................... i
SITE INFORMATION ............................................................................................................................ ii
ACRONYMS ..................................................................................................................................... ivii
1. RISK CHARACTERIZATION .....................................................................................................1
2. RECEPTOR INFORMATION .....................................................................................................3
3. SITE GEOLOGY AND HYDROGEOLOGY ...................................................................................4
4. SITE INVESTIGATION .............................................................................................................5
5. CONCLUSIONS AND RECOMMENDATIONS ............................................................................7
6. LIMITATIONS ........................................................................................................................7

FIGURES
Figure 1: Site Location Map
Figure 2A: Site Vicinity Map
Figure 2B: Zoning Map
Figure 3: Site Map
Figure 4: Soil Quality Map
Figure 5: Ground Water Quality Map

TABLES
Table 1: UST Owner/Operator Information
Table 2: UST System Information
Table 3: Land Use Information
Table 4: Receptor Information
Table 5: Adjacent Property Owner Information
Table 6: Well Construction and Gauging Information
Table 7: Summary of Soil Sample Analytical Results
Table 8: Summary of Ground Water Sample Analytical Results

APPENDICES
Appendix A: Wake County Property Cards
Appendix B: Well Construction Records and Subsurface Logs
Appendix C: State Correspondence
Appendix D: Laboratory Analytical Reports

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase I Limited Site Assessment Report
Prepared on: September 15, 2022 Flash Market #370
Project Manager: Laura Minor GRI Project No. 6117
1
1. RISK CHARACTERIZATION
Limited Site Assessment Risk Classification and Land Use Form
Part I – Groundwater/Surface Water/Vapor Impacts
High Risk
1. Has the release contaminated any water supply well including any well used for non-drinking
purposes? NO

2. Is a water supply well used for drinking water located within 1,000 feet of the source area of the
release? NO

3. Is a water supply well not used for drinking water (e.g., irrigation, washing cars, industrial cooling
water, filling swimming pools) located within 250 feet of the source area of the release?
NO

4. Does ground water within 500 feet of the source area of the release have the potential for future
use (there is no other source of water supply other than the groundwater)? NO

Public water is available to the site and surrounding properties.

5. Do vapors from the release pose a threat of explosion because of accumulation of the vapors in a
confined space or pose any other serious threat to public health, public safety or the
environment?
NO

6. Are there any other factors that would cause the release to pose an imminent danger to public
health, public safety, or the environment? NO
If YES, explain:

Intermediate Risk
7. Is a surface water body located within 500 feet of the source area of the release? YES

A small creek is located approximately 300 feet southwest of the site. A retention pond is located
approximately 350 feet northwest of the site.

If YES, does the maximum groundwater contaminant concentration exceed the surface water
quality standards and criteria found in 15A NCAC 2B .0200 by a factor of 10?
NO
8. Is the source area of the release located within an approved or planned wellhead protection area
as defined in 42 USC 300h-7(e)? NO

9. Is the release located in the Coastal Plain physiographic region as designated on a map entitled
“Geology of North Carolina” published by the Department in 1985? NO

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase I Limited Site Assessment Report
Prepared on: September 15, 2022 Flash Market #370
Project Manager: Laura Minor GRI Project No. 6117
2
10. If YES, is the source area of the release located in an area in which there is recharge to an
unconfined or semi-confined deeper aquifer that is being used or may be used as a source of
drinking water? N/A
If YES, describe.
11. Do the levels of ground water contamination for any contaminant exceed the gross contamination
levels established by the Department? NO

Part II - Land Use
Property Containing Source Area of Release
The questions below pertain to the property containing the source area of the release.
1. Does the property contain one or more primary or secondary residences (permanent or
temporary)? NO
Explain:
The subject property is an active convenience store and petroleum retail facility.

2. Does the property contain a school, daycare center, hospital, playground, park, recreation area,
church, nursing home, or other place of public assembly? NO
Explain:

The subject property is an active convenience store and petroleum retail facility.

3. Does the property contain a commercial (e.g., retail, warehouse, office/business space, etc.) or
industrial (e.g., manufacturing, utilities, industrial research and development,
chemical/petroleum bulk storage, etc.) enterprise, an inactive commercial or industrial
enterprise, or is the land undeveloped? YES
Explain:

The subject property is an active convenience store and petroleum retail facility.

4. Do children visit the property? YES
Explain:

The site is currently a convenience store and children would likely visit the property.

5. Is access to the property reliably restricted consistent with its use (e.g., by fences, security
personnel or both)? NO
Explain:
The property is easily accessible to pedestrian and vehicular traffic.
6. Do pavement, buildings, or other structures cap the contaminated soil? YES
Explain:
The site is currently covered with concrete and asphalt.

If yes, what mechanisms are in place or can be put into place to ensure that the contaminated soil

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase I Limited Site Assessment Report
Prepared on: September 15, 2022 Flash Market #370
Project Manager: Laura Minor GRI Project No. 6117
3
will remain capped in the foreseeable future?
The site is expected to remain in operation as an active convenience store and petroleum retail
facility in the near future.
7. What is the zoning status of the property?
According to the City of Cary Official Zoning Map, the site is zoned GCCU (General Commercial
Conditional Use).
8. Is the use of the property likely to change in the next 20 years? NO
Explain:

The subject property is currently an active convenience store and petroleum retail facility and
likely remain a convenience store in the near future.
Property Surrounding Source Area of Release
The questions below pertain to the area within 1,500 feet of the source area of the release (excludes
property containing source area of the release):

9. What is the distance from the source area of the release to the nearest primary or secondary
residence (permanent or temporary)?

The closest primary residence is 306 Cole Canyon Court located approximately 300 feet north of
the UST basin.

10. What is the distance from the source area of the release to the nearest school, daycare center,
hospital, playground, park, recreation area, church, nursing home or other place of public
assembly?

Black Creek Greenway is located approximately 200 feet north of the UST basin.

11. What is the zoning status of properties in the surrounding area?

According to the City of Cary Official Zoning Map, the surrounding areas are zoned Commercial
(GC and GCCU), Office/institutional (OI/OICU), Industrial (I/ICU) and Residential (R8/R8CU,
R12/R12CU, R20, R40, RMF/RMF-C).

12. Briefly characterize the use and activities of the land in the surrounding area.

The area surrounding the site is a mixture of commercial, public/institutional and residential.
Land use information has been included as Table 3. A zoning map has been included as Figure 2B.

2. RECEPTOR INFORMATION
1. Water Supply Wells:
A receptor survey was conducted on September 7, 2022. No water supply wells were identified
within 1500 feet of the site. A Site Location Map is provided as Figure 1 and a Site Vicinity Map

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase I Limited Site Assessment Report
Prepared on: September 15, 2022 Flash Market #370
Project Manager: Laura Minor GRI Project No. 6117
4
showing property boundaries for the site and surrounding properties has been included as Figure
2A. Receptor information has been provided in Table 4.

2. Public Water Supplies:
Are public water supplies available within 1,500 feet of the source area of the release? YES
If yes, where is the location of the nearest public water lines and the source(s) of the public water
supply. Explain:
Municipal water is available to the site and the surrounding properties. Water lines run along the
public streets in the area. Public water is supplied by the City of Cary.

3. Surface Water:
Identify all surface water bodies (e.g., ditch, pond, stream, lake, river) within 1,500 feet of the
source area of the release. This information must be shown on the USGS topographic map.
Two surface water bodies were identified within a 500-foot radius of the site. A small stream was
identified about 250 feet southeast of the site. A retention pond was also identified about 400
feet northeast of the site.

4. Wellhead Protection Areas:
Identify all planned or approved wellhead protection areas in the vicinity of the source area. This
information must be shown on the USGS topographic map. Wellhead protection areas are defined
in 42 USC 300h-7(e).
On September 12, 2022, GRI personnel accessed the NCDEQ SWAP Program’s website to identify
wellhead protection areas in the vicinity of the subject site. The site is not located within a
wellhead protection area.

5. Deep Aquifers in the Coastal Plain Physiographic Region:
The site is not located in the Coastal Plain Physiographic Region.
6. Subsurface Structures:
No structures with basements were observed in the vicinity of the source area. The water main
and other underground utilities run along Northwest Maynard Road and several underground
utility lines were observed on the property.

7. Property Owners and Occupants:
The names and addresses of the owners of properties adjacent to the site are presented in Table
5. Property boundaries are shown on Figure 2A. Property cards for the adjacent property owners
are attached as Appendix B.
3. SITE GEOLOGY AND HYDROGEOLOGY
According to the 1985 Geologic Map of North Carolina, the site is located in the Carolina Slate Belt. The
bedrock is generally described as metamorphosed argillite, mudstone, volcanic sandstone, conglomerate,
and volcanic rock. The soil samples collected during well installation activities were tan, gray and red clay.
The depth to ground water during the July 2022 gauging event was 23.71 feet below the top of well casing.
Copies of the well construction record and subsurface log have been included as Appendix C. A Site Map

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase I Limited Site Assessment Report
Prepared on: September 15, 2022 Flash Market #370
Project Manager: Laura Minor GRI Project No. 6117
5
is included as Figure 3. Well construction and gauging information is presented in Table 6. A photo of the
monitoring well is shown below:

4. SITE INVESTIGATION
On July 2, 2022, a non-passing spill bucket integrity test was reported and on July 6, 2022, GRI conducted
a site check at the subject site. A soil boring was advanced adjacent to the spill bucket to a depth of
approximately 30 feet BGS and soil samples were collected from the borings (SB-1-10’, SB-1-20’, and SB-
1-30’).

Soil boring SB-1 was completed as monitoring well MW-1 by a North Carolina licensed well contractor on
July 6, 2022, to assess the identified release at the site. MW-1 was installed to a total depth of 30 feet
BGS with a 15-foot screened interval set to bracket the water table at the time of installation. Based on
the soil and ground water sample analytic results, a LSA was recommended. A copy of the NORR requiring
an LSA has been included as Appendix D.

Monitoring well MW-1 was gauged on July 6, 2022. The depth to ground water was 23.71 feet. Gauging
data from the July 2022 gauging event has been included in Table 6. A summary of the current gauging
data is shown below:

Well ID
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(ft.)
Groundwater
Elevation
(ft.)
MW-1 15 - 30 30 100.00 23.71 76.29

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase I Limited Site Assessment Report
Prepared on: September 15, 2022 Flash Market #370
Project Manager: Laura Minor GRI Project No. 6117
6
1. Soil Sampling:
Soil samples (SB-1-10’, SB-1-20’, and SB-1-30’) were collected on July 6, 2022, during Site Check
activities. Samples SB-1-10’ and SB-1-30’ were submitted for laboratory analyses of and VOCs by EPA
Method 8260, and VPH by the MADEP method. Soil sample SB-1-20’ was submitted for VPH only by
the MADEP method. The applicable soil-to-water MCCs were below the concentrations of MTBE
reported in the soil samples collected from SB-1-10’ and SB-1-30’. No free product was noted at the
site. A Soil Quality Map has been included as Figure 4. A summary of the soil sample analytical results
is presented in Table 7. A copy of the laboratory analytical report from the July 2022 soil sampling
event has been included as Appendix D. A copy of the soil sample analytical results is shown below:
Sample ID Sample Depth (ft-BGS) Benzene Toluene Ethylbenzene Total Xylenes MTBE Naphthalene Soil to Water MCC (mg/kg) 0.0072 5.4 8 6 0.085 0.2
Residential SCLs (mg/kg) 12 1,250 60.3 3,120 156 5.5
SB-1-10’ 10 0.002 J 0.001 J 0.001 J 0.009 J 0.234 <0.001
SB-1-20’ 20 NR NR NR NR NR NR
SB-1-30’ 30 <0.0008 <0.001 <0.0008 0.0008 J 2.24 <0.001

2. Ground Water Sampling:
On July 6, 2022, MW-1 was gauged, purged, and sampled in accordance with NCDEQ guidelines. The
ground water sample was submitted for analysis of VOCs by EPA Method 6200B, EDB by EPA Method
504.1, total lead by EPA Method 3030C and VPH by the MADEP Method. The concentrations of
benzene, MTBE, naphthalene, TAA, TBA, C5-C8 aliphatics, and C9-C10 aromatics reported in the
ground water sample collected from MW-1 were below the MACs. All contaminant concentrations
were below the GCLs and below ten times the surface water standards. No free product was observed
at the site. A Ground Water Quality Map has been included as Figure 6. A summary of the ground
water analytical data has been included in Table 8. A copy of the laboratory analytical report has been
included as Appendix E. A summary of the current ground water sampling data is shown below:

Contaminant of
Concern
 Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene Well
ID
MAC (µg/l) 1 600 600 500 20 6
GCL (µg/l) 5,000 260,000 84,500 85,500 20,000 6,000
MW-1 99.2 40 40.9 210 3550 8.01

3. Quality Control:
The soil and ground water samples were immediately placed in laboratory-supplied containers after
collection, which were then placed in iced coolers. New disposable bailers were used to sample the

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase I Limited Site Assessment Report
Prepared on: September 15, 2022 Flash Market #370
Project Manager: Laura Minor GRI Project No. 6117
7
monitoring well and new nitrile gloves were worn during soil and ground water sampling. Samples
were logged using proper chain-of-custody procedures. The samples were transported to a North
Carolina certified laboratory for analysis. A laboratory supplied trip blank was included in the sample
cooler. No detectable concentrations of requested method constituents were reported in the trip
blank.

5. CONCLUSIONS AND RECOMMENDATIONS
 The site is an active convenience store and petroleum retail facility. Land use in the area consists
of commercial, residential, office and public/institutional properties.
 A receptor survey was conducted on September 7, 2022. No water supply wells were identified
within a 1,500-foot radius of the site. Public water is available to the subject site and to all
surrounding properties.
 Two surface water bodies were identified within a 500-foot radius of the site. Coles Branch, a
Class C/NSW water, is located approximately 300 feet southeast of the site. A retention pond is
located about 350 feet northeast of the site.
 On July 6, 2022, one monitoring well was installed. Soil samples were collected at 10-foot intervals
during the installation of monitoring well MW-1. The concentration of MTBE reported in soil
samples SB-1-10’ and SB-1-30’ exceeded the soil-to-water MCC.
 On July 6, 2022, a ground water sample was collected from MW-1. The MACs were below the
concentrations of benzene, MTBE, naphthalene, TAA, TBA, C5-C8 aliphatics, and C9-C10 aromatics
reported in the ground water sample collected from MW-1.
 The reported contaminant concentrations do not exceed ten times the NCDEQ surface water
standards. Based on the lack of receptors other than surface water bodies, the availability of
municipal water to all properties in the area, and relatively low ground water contaminant
concentrations, GRI recommends the site be classified as Low Risk and the incident closed after
filing a Notice of Residual Petroleum.

6. LIMITATIONS
This report has been prepared for the exclusive use of Transit Energy Group and Mr. Scott Gordon for
specific application to the referenced site in Wake County, North Carolina. The assessment was conducted
based on the scope of work and level of effort specified by NCDEQ and with resources adequate only for
that scope of work. Our findings have been developed in accordance with generally accepted standards
of geology and hydrogeology practices in the State of North Carolina, available information and our
professional judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would
be interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data.

FIGURES
SITE LOCATIONFigure 1 Site Location Flash Market #3701390 NW Maynard RoadCary, North CarolinaWake CountyIncident No. PendingGRI Project No. 6117500 M2000 FTDate: 06/18/2022 Location: 35.788162° N -78.809742° W Dad
SITE
0754712134
0754629493
0754611587
0754612835 0754615887
0754621154
0754615675
0754622295
MAYNARD RDBAYOAK DRC A S T A L IA D R
JO E L C TCONTESSA DRSPRING BUD DRD U T C H E S S D R
BELROSE DR
PHAUFF CTSILVER
L
I
NI
NG LNCALM WINDS CT
HOWLAND AVECOLE VALLEY DRBRAINTREE CT
RAVENDALE PL
HUNTSWORTH PLR
O
S
E S
K
Y
C
T
OLDE WEATHERSTONE WAY
ORCHARD PARK DRCOLE STREAM CTPAINTED FALL WAY DAVENBURY W AYSOLANO DR
FOREST WIND WAY
DOGWOOD FOREST DR
MAYNARD CROSSING CT
T H E N S IA C TOZONE CTSEABREEZE CTSMALLWOOD CTM A R S E N A L N
WEYDALE WAY
G A Y L E C IR
VERMEL CTABBEYDALE DRA D V E N T U R E T R L
C
OL
E
CA
N
Y
ON

C
T
BELROSE DRCol
es
Br
an
chFIGURE 2A: SITE VICINITY MAPFLASH MARKET #3701390 NW MAYNARD ROADCARY, WAKE COUNTYNORTH CAROLINAINCIDENT NO. 48615GRI PROJECT NO. 6117
PREPARED BY:GEOLOGICAL RESOURCES, INC.AUGUST 10, 2022
1,500-FOOT RADIUS
1,000-FOOT RADIUS 500-FOOT RADIUS
³
250-FOOT RADIUS
0 300150Feet
1 inch = 300 feet
1
LEGEND
Wake_Streets_2019_06
Wake_HydroLines_2011_10
Wake_MajorStreams_2011_10
Wake_HydroPolys_2011_10
Adjacent Properties
Wake_Property_2019_06
SITEMAYNARD RDBAYOAK DRC A S T A L IA D R
JO E L C TCONTESSA DRSPRING BUD DRD U T C H E S S D R
BELROSE DR
PHAUFF CTSILVER
L
I
NI
NG LNCALM WINDS CT
HOWLAND AVECOLE VALLEY DRBRAINTREE CT
RAVENDALE PL
HUNTSWORTH PLR
O
S
E S
K
Y
C
T
OLDE WEATHERSTONE WAY
ORCHARD PARK DRCOLE STREAM CTPAINTED FALL WAY DAVENBURY W AYSOLANO DR
FOREST WIND WAY
DOGWOOD FOREST DR
MAYNARD CROSSING CT
T H E N S IA C TOZONE CTSEABREEZE CTSMALLWOOD CTM A R S E N A L N
WEYDALE WAY
G A Y L E C IR
VERMEL CTABBEYDALE DRA D V E N T U R E T R L
C
OL
E
CA
N
Y
ON

C
T
BELROSE DRCol
es
Br
an
chFIGURE 2B:ZONING MAPFLASH MARKET #3701390 NW MAYNARD ROADCARY, WAKE COUNTYNORTH CAROLINAINCIDENT NO. 48615GRI PROJECT NO. 6117
PREPARED BY:GEOLOGICAL RESOURCES, INC.AUGUST 10, 2022
1,500-FOOT RADIUS
1,000-FOOT RADIUS 500-FOOT RADIUS
³
250-FOOT RADIUS
0 300150Feet
1 inch = 300 feet
1
LEGEND
Wake_Streets_2019_06
Wake_HydroLines_2011_10
Wake_MajorStreams_2011_10
Wake_HydroPolys_2011_10
ZONING - PDDMINOR
ZONING - CARY
ZONING - CARY
ZONING - I
ZONING -R/R
ZONING -OICU
ZONING -R20
ZONING - R40
ZONING - PDDMAJOR
ZONING - RMF-C
ZONING - R12CU
ZONING - R8CU
ZONING - ICU
ZONING - GCCU
Wake_Property_2019_06

TABLES
UST ID Number 1A-1 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 1A-1 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 1A-1 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 1A-1 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 1A-1 Facility ID Number
Owner or Operator?
Owner/Operator
501 River Street, Floor 3, Greenville, SC 29602 864-626-5553
00-0-0000035687
Name of Owner or Operator Dates of Ownership / Operation
Flash Market LLC 7/29/2022 - Current
Address Telephone Number
613 US Highway 158 Bypass, Henderson, NC 27537 252-438-7141
UST OWNER/OPERATOR INFORMATION
FLASH MARKET #370 (INCIDENT NO. 48615)
00-0-0000035687
Name of Owner or Operator Dates of Ownership / Operation
TABLE 1
00-0-0000035687
Name of Owner or Operator Dates of Ownership / Operation
Laws Enterprises, Inc.8/26/2004 - 12/18/2008
Rose Oil Company, Inc.1/1/1997 - 8/26/2004
Address Telephone Number
Address Telephone Number
Unknown Unknown
00-0-0000035687
Name of Owner or Operator Dates of Ownership / Operation
Tirath, Inc.12/18/2008 - 3/2/2016
Address Telephone Number
Unknown Unknown
613 US Highway 158 Bypass, Henderson, NC 27537 252-438-7141
00-0-0000035687
Name of Owner or Operator Dates of Ownership / Operation
Rose Oil Company, Inc.3/2/2016 - 7/29/2022
Address Telephone Number
Date: 08/02/22 Facility ID #: 00-0-0000035687
Was Release
Associated
with UST
System?
(Yes / No)
1A Gasoline NA 10,000 06/01/1997 Single Wall FRP 8' x 26' 8"Single Wall FRP Current No
1 Gasoline NA 17,000 06/01/1997 Single Wall FRP 10' 6" x 31'Single Wall FRP Current No
Capacity
(gallons)
Date
Installed
Construction
Details
Tank
Dimensions
Description of
Associated
Product Piping
and
Pumps
Status
of
UST
TABLE 2
UST SYSTEM INFORMATION
FLASH MARKET #370 (INCIDENT NO. 48615)
UST
ID
No.
Current
or Most
Recent
Contents
Previous
Contents
Date: 09/12/22 Facility ID # : 00-0-0000035687
Map ID No.Land Use Feature Zoning Description Address
Distance from
Source Area
(feet)
1 Black Creek Greenway GCCU Greenway/Walking Trail N/A ~230 N
2 Weatherstone Elementary PDDMajor Elementary School 1000 Olde Weatherstone Way ~1200 NW
Industrial I/ICU N/A N/A N/A
General Commercial/
Conditional Use GC/GCCU N/A N/A N/A
Office and Institutional/
Conditional Use OI/OICU N/A N/A N/A
Mixed Use District MXD N/A N/A N/A
Residential Multi-Familty RMF-C N/A N/A N/A
Residential District/
Conditional Use R8/R8CU N/A N/A N/A
Residential District/
Conditional Use R12/R12CU N/A N/A N/A
Residential District R20 N/A N/A N/A
Residential District R40 N/A N/A N/A
Planned Development District PDDMajor N/A N/A N/A
Planned Development District PDDMinor N/A N/A N/A
Resource/Recreation District R/R N/A N/A N/A
Note:
• Properties are keyed to Figure 2B.
TABLE 3
LAND USE INFORMATION
FLASH MARKET #370 (INCIDENT NO. 48615)
Facility ID # : 00-0-0000035687
Well ID.Parcel ID No.Well Owner Mailing Address Well Address Well Status
(Active/In-Active)
Well Use
(Potable / Non-
Potable
etc.)
Municpal
Water
Available
Yes/No
Connected
to
Municipal
Water
Yes/No
Distance
from source
area of
release
(ft.)
Receptor
ID
Latitude/ Longitude
of Any Significant
Points
Up or Down-
Gradient
Distance
from
the source
area
of release
(ft.)
n/a 35.788802°N,
78.808116°W Down 300
n/a 35.787500°N,
78.808060°W Down 350
Notes:
• Receptors are shown on Figure 2A.
• n/a: not applicable.
Small intermittent Stream Approx. 250' southeast of site n/a none
Retention pond Approx. 400' NE of UST basin n/a retain stormwater
Description Location Contact/Phone Number Usage
TABLE 4
RECEPTOR INFORMATION
FLASH MARKET #370 (INCIDENT NO. 48615)
Date: 09/12/22
Well Construction Details
(Depth, Screened Interval, Type of Well, ect.)
Date: 09/12/22 Facility ID #: 0-035687
PIN Number Property Owner Name Property Owner Address
754615887 Getty Leasing, inc.292 Madison Avenue, Floor 9
New York NY, 10017-6376
754615675 Atlantic Avenue Tire LD Co., LLC 1380 NW Maynard Road
Cary, NC 27513-8721
754712134 MAA TANC, Inc.
MAA Schindler #010119
6815 Poplar Avenue, Suite 500
Germantown, TN 38138-0612
754612835 BSN Real Estate, LLC 507 Catlin Road
Cary NC 27519-5984
754621154 Paul Norman Ferris and Maria S
Ferris Trustee
114 Rose Sky Court
Cary, NC 27513-3580
754629493 Coles Creek Homeowners Assn., Inc.
PPM, INC
11010 Raven Ridge Road
Raleigh, NC 27614-8837
Note:
• Properties are keyed to Figure 2A.
TABLE 5
ADJACENT PROPERTY OWNER INFORMATION
FLASH MARKET #370 (INCIDENT NO. 48615)
Date: 09/13/22 Facility ID # : 00-0-0000035687
Well ID
Date
Installed
(m/dd/yy)
Date Water
Level
Measured
(m/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(feet)
Free Product
Thickness
(ft.)
Ground
Water
Elevation (ft.)
Comments
MW-1 07/06/22 07/06/22 15 15-30 30 100.00 23.71 ---76.29
TABLE 6
WELL CONSTRUCTION AND GAUGING INFORMATION
FLASH MARKET #370 (INCIDENT NO. 48615)
Date: 08/02/22
Sample IDDate Collected (mm/dd/yy)Sample Depth(ft-BGS)BenzeneTolueneEthylbenzeneXylenesMTBENaphthaleneC5 - C8 AliphaticsC9-C12 Aliphaticsc9-C10 Aromatics0.0072 5.4 8 6 0.085 0.2 68 540 31
12 1,250 60.3 3,120 156 5.5 625 1,560 469
59.4 18,600 297 46,700 1,810 27 9,340 23,300 7,000
SS-1-10'07/06/22 10 0.002 J 0.001 J 0.001 J 0.009 J 0.234 <0.001 <1.96 <7.36 <1.01
SS-1-20'07/06/22 20 NR NR NR NR NR NR <2.89 <10.8 <1.48
SS-1-30'07/06/22 30 <0.0008 <0.001 <0.0008 0.0008 J 2.24 <0.001 <1.92 <7.21 <0.986
Notes:
• Results reported in mg/kg (milligrams per kilograms)
• ft-BGS: feet below ground surface
• < : Less than the method detection limit specified in the laboratory report
• MCCs: Maximum Contaminant Concentrations (soils)
• SCLs: Soil Cleanup Levels.
• Concentrations in bold face type exceed the soil-to-water MCC
• Concentrations in italic type exceed the residential SCL
• NE: Not Established
• NR: Not Requested
MADEP VPH/EPH
Soil to Water MCC (mg/kg)
Residential SCLs (mg/kg)
Industrial/Commercial Soil
Cleanup Levels (mg/kg)
Facility ID #: 00-0-0000035687
TABLE 7
SUMMARY OF SOIL SAMPLE ANALYTICAL RESULTS
FLASH MARKET #370 (INCIDENT NO. 48615)
Analytical Method EPA 8260B
Date: 09/13/22
Facility ID #: 00-0-0000035687
EPA
504.1 SW-6020B
Well
ID
Date Sampled
(mm/dd/yy)
1 600 600 500 20 6 40 10 70 0.02 15 400 700 200
510 110 1300 670 15000 120 NE NE 200,000 1.0 NC 1,250 1,800 40,000
5,000 260,000 80,000 50,000 20,000 6,000 40,000 10,000 70,000 50 15,000 NE NE NE
MW-1 07/06/22 99.2 40 40.9 210 3,550 8.01 1,210 2,640 5.59 <0.00345 <0.500 846 164 308
Notes:
• Nearest stream is Coles Branch, a desinated Class C/NSW water.
• Results reported in micrograms per liter (µg/l).
• MAC: Maximum Allowable Concentration as specified in T15A NCAC 2L.0202.
• < : Less than the method detection limit specified in the laboratory report.
• GCL: Gross contamination level.
• Concentrations in bold face type exceed the MAC
• Concentrations in italic type exceed the GCL
• J: Estimated value.
• NE: Not established.
• NR: Not requested.
• Refer to laboratory report for other detectable concentrations which did not exceed the MACs.
10 x 2B (μg/l)tert-Amyl alcohol(TAA)tert-Butyl alcohol(TBA)Lead• NC: Not calculated; the 10 x 2B Standard for Lead is a calculated value determined by the water hardness. The average hardness for the state of NC is 46 ppm and was used to
calculate this value.
TABLE 8
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
FLASH MARKET #370 (INCIDENT NO. 48615)
Analytical Method EPA 602 MADEP VPH
Contaminant of Concern
MTBEC5-C8 AliphaticsMAC (μg/l)
GCL (μg/l)NaphthaleneC9-C12 AliphaticsC9-C10 Aromatics1,2-Dibromoethane(EDB)Di-isopropyl etherBenzeneEthylbenzeneXylenesToluene

APPENDICES

APPENDIX A
Wake County Property Cards

APPENDIX B
Well Construction Record and Subsurface Log
Geological Resources, Inc.Phone:[phone]
3502 Hayes Road Fax:[phone]
Monroe, NC 28110
Project Flash Market #370 Project #6117
Address 1390 NW Maynard Road, Cary NC
Boring Number MW-1 Date Drilled 07/06/22
Sample Method Grab Drilling Method 6.25 SSA
Completion Details Well installed at 30' with 15' screen, 15' riser, flush mounted
Driller Matt Steele License #4548A Log By AJ Discepolo
Boring Lab Sample PID GW USCS
Depth Sample Type ppm depth class From To Color Moisture Odor
0
2
0.0 3.0 Gray/tan
4 3.0 23.0 CLAY Red
6
8
10 SB-1-10'grab 10'CL Red moist

12
14
16

18
20 SB-2-20'grab 20'CL Red moist
22
q 23.0 30.0 Tan moist
24
26
28

30 SB-3-30'grab 30'CL Tan moist
32
34
35
Depth (feet)
SUBSURFACE LOG
Soil Type
LITHOLOGY
Fine SAND
CLAY
CLAY
CLAY
CLAY
WELL CONSTRUCTION RECORD
This form can be used for single or multiple wells
Form GW-1 North Carolina Department of Environment and Natural Resources – Division of Water 5HVRXUFHV Revised AXJXVW 2013
1. Well Contractor Information:

Well Contractor Name

NC Well Contractor Certification Number

Company Name 2. Well Construction Permit #: List all applicable well permits (i.e. County, State, Variance, ,QMHFWLRQetc.) 3. Well Use (check well use): Water Supply Well: □Agricultural □Municipal/Public □Geothermal (Heating/Cooling Supply) □Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared) □Irrigation
Non-Water Supply Well: □Monitoring □Recovery
Injection Well: □Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier □Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop) □Tracer □Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks)
4. Date Well(s) Completed: ____________ Well ID#______________________ 5a. Well Location:
Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip
County Parcel Identification No. (PIN) 5b. Latitude and Longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) N W
6. Is (are) the well(s): □Permanent or □Temporary

7. Is this a repair to an existing well: □Yes or □No If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form.
8. Number of wells constructed: For multiple injection or non-water supply wells ONLY with the same construction, you can submit one form. 9. Total well depth below land surface: (ft.) For multiple wells list all depths if different (example- 3@200’ and 2@100′) 10. Static water level below top of casing: (ft.) If water level is above casing, use “+” 11. Borehole diameter: (in.) 12. Well construction method: (i.e. auger, rotary, cable, direct push, etc.) FOR WATER SUPPLY WELLS ONLY: 13a. Yield (gpm) Method of test: 13b. Disinfection type: Amount:

14. WATER ZONES
FROM TO DESCRIPTION
ft. ft.
ft. ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable) FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
17. SCREEN FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
18. GROUT
FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
ft. ft.
ft. ft.
ft. ft.
19. SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
ft. ft.
ft. ft.
20. DRILLING LOG (attach additional sheets if necessary) FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
21. REMARKS

22. Certification:
Signature of Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner.
23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well construction details. You may also attach additional pages if necessary. SUBMITTAL INSTUCTIONS 24a. For All Wells: Submit this form within 30 days of completion of well construction to the following: Division of Water Resources, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells ONLY: In addition to sending the form to the address in
24a above, also submit a copy of this form within 30 days of completion of well construction to the following: Division of Water Resources, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells:
Also submit one copy of this form within 30 days of completion ofwell construction to the county health department of the county whereconstructed.
For Internal Use ONLY:

APPENDIX C
State Correspondence

APPENDIX D
Laboratory Analytical Report

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

7/20/2022
Geological Resources, Inc. Laura Minor
3502 Hayes Road Monroe, NC, 28110
Ref: Analytical Testing
Lab Report Number: 22-189-0051 Client Project Description: Flash Market #370
GRI #6117
Dear Laura Minor:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 7/8/2022 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love Project Manager
Page 1 of 50
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202237735State ProgramNorth Carolina
12/31/2022402State ProgramNorth Carolina
07/31/202299012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Page 1 of 1 00016/22-189-0051
Page 2 of 50
Report Number:
Sample Summary Table
Client Project Description:
22-189-0051
Flash Market #370
GRI #6117
Lab No Client Sample ID Matrix Date Collected Date Received
07/06/2022 08:50Aqueous 93939 MW-1 07/08/2022 11:45
07/06/2022 07:17Solids 93940 SB-1-10'07/08/2022 11:45
07/06/2022 08:28Solids 93941 SB-2-20'07/08/2022 11:45
07/06/2022 08:32Aqueous 93942 Trip Blank 07/08/2022 11:45
07/06/2022 08:38Solids 93943 SB-3-30'07/08/2022 11:45
Page 3 of 50
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-189-0051
Report Limit
Project:Flash Market #370
V 93939MW-1
54.5 07/14/2022 23:346200BAcetoneµg/L 1.80
99.2 07/14/2022 23:346200BBenzeneµg/L 0.180
2.86 07/14/2022 23:346200Bn-Butylbenzene µg/L 0.180
1.35 07/14/2022 23:346200Bsec-Butyl benzene µg/L 0.200
5.59 07/14/2022 23:346200BDi-Isopropyl Ether (DIPE)µg/L 0.500
J66.7 07/14/2022 23:346200BEthanolµg/L 42.0
40.9 07/14/2022 23:346200BEthylbenzeneµg/L 0.170
J0.829 07/14/2022 23:346200BEthyl Tertiary Butyl Ether (ETBE)µg/L 0.059
5.24 07/14/2022 23:346200B2-Hexanone µg/L 0.380
6.89 07/14/2022 23:346200BIsopropylbenzeneµg/L 0.180
0.826 07/14/2022 23:346200B4-Isopropyl toluene µg/L 0.089
23.7 07/14/2022 23:346200BMethyl Ethyl Ketone (MEK)µg/L 0.710
3550 07/15/2022 18:146200BMethyl tert-butyl ether (MTBE)µg/L 14.0
3.78 07/14/2022 23:346200B4-Methyl-2-Pentanone µg/L 0.078
8.01 07/14/2022 23:346200BNaphthaleneµg/L 0.470
11.0 07/14/2022 23:346200Bn-Propylbenzene µg/L 0.190
2640 07/15/2022 18:146200Btert-Butyl Alcohol (TBA)µg/L 160
1210 07/15/2022 18:146200Btert-Amyl Alcohol (TAA)µg/L 190
69.0 07/14/2022 23:346200Btert-Amyl Methyl Ether (TAME)µg/L 0.280
40.0 07/14/2022 23:346200BTolueneµg/L 0.220
95.7 07/14/2022 23:346200B1,2,4-Trimethylbenzene µg/L 0.190
26.4 07/14/2022 23:346200B1,3,5-Trimethylbenzene µg/L 0.180
66.9 07/14/2022 23:346200Bo-Xylene µg/L 0.210
143 07/14/2022 23:346200Bm,p-Xylene µg/L 0.420
210 07/14/2022 23:346200BXylene (Total)µg/L 0.210
846 07/14/2022 23:34CALCULATIONAliphatic C5-C8 (Adjusted)µg/L 115
164 07/14/2022 18:59CALCULATIONAliphatics C9-C12 (Adjusted)µg/L 25.8
308 07/14/2022 18:59CALCULATIONAromatic C9-C10 (Adjusted)µg/L 4.02
985 07/15/2022 08:41MADEP-VPH Aliphatic C5-C8 µg/L 115
723 07/14/2022 18:59MADEP-VPH Aliphatic C9-C12 µg/L 25.8
308 07/14/2022 18:59MADEP-VPH Aromatic C9-C10 µg/L 4.02
V 93940SB-1-10'
0.200 07/12/2022 14:008260DAcetonemg/Kg - dry 0.003
J0.002 07/12/2022 14:008260DBenzenemg/Kg - dry 0.0008
J0.002 07/12/2022 14:008260DBromomethanemg/Kg - dry 0.002
J0.002 07/12/2022 14:008260DCarbon Disulfide mg/Kg - dry 0.0009
Page 4 of 50
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-189-0051
Report Limit
Project:Flash Market #370
V 93940SB-1-10'
J0.001 07/12/2022 14:008260DEthylbenzenemg/Kg - dry 0.0008
J0.007 07/12/2022 14:008260D2-Hexanone mg/Kg - dry 0.0009
0.098 07/12/2022 14:008260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0009
0.234 07/12/2022 14:008260DMethyl tert-butyl ether (MTBE)mg/Kg - dry 0.0009
J0.001 07/12/2022 14:008260DToluenemg/Kg - dry 0.0009
J0.004 07/12/2022 14:008260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0007
J0.001 07/12/2022 14:008260D1,3,5-Trimethylbenzene mg/Kg - dry 0.0008
J0.002 07/12/2022 14:008260Do-Xylene mg/Kg - dry 0.0007
J0.006 07/12/2022 14:008260Dm,p-Xylene mg/Kg - dry 0.001
J0.009 07/12/2022 14:008260DXylene (Total)mg/Kg - dry 0.0007
29.5 07/15/2022 10:33SW-DRYWT Moisture %
V 93942Trip Blank
J2.21 07/14/2022 19:426200BAcetoneµg/L 1.80
V 93943SB-3-30'
0.123 07/12/2022 14:278260DAcetonemg/Kg - dry 0.003
J0.001 07/12/2022 14:278260DDi-Isopropyl Ether (DIPE)mg/Kg - dry 0.001
J0.018 07/12/2022 14:278260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0009
2.24 07/14/2022 12:178260DMethyl tert-butyl ether (MTBE)mg/Kg - dry 0.022
J0.001 07/12/2022 14:278260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0007
J0.0008 07/12/2022 14:278260Do-Xylene mg/Kg - dry 0.0007
J0.0008 07/12/2022 14:278260DXylene (Total)mg/Kg - dry 0.0007
31.2 07/15/2022 10:33SW-DRYWT Moisture %
Page 5 of 50

Client: Geological Resources, Inc. CASE NARRATIVE
Project: Flash Market #370 Lab Report Number: 22-189-0051
Date: 7/20/2022
EDB and DBCP by Microextraction GC/ECD Method EPA-504.1 Analyte: 1,2-Dibromoethane QC Batch No: V21440/V21417
Confirmation column CCV above range for this Analyte. No hits in samples. No further action taken. Volatile Organic Compounds - GC/MS Method 6200B Analyte: tert-Amyl alcohol
QC Batch No: V21339/V21408 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.

Page 6 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-189-0051
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #6117 Received : 07/08/2022
Flash Market #370
Report Date : 07/20/2022
Sample ID :
Lab No :
Sampled:MW-1
93939 Matrix:
7/6/2022 8:50
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.500 µg/L 0.500 1.00Lead 1 07/14/22 13:55 6020BEDV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 7 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-189-0051
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #6117 Received : 07/08/2022
Flash Market #370
Report Date : 07/20/2022
Sample ID :
Lab No :
Sampled:MW-1
93939 Matrix:
7/6/2022 8:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V21337 07/14/22 09:00 V21408 07/15/22 09:00
54.5 µg/L 1.80 10.0Acetone 1 07/14/22 23:34 V21339JLB
99.2 µg/L 0.180 0.500Benzene 1 07/14/22 23:34 V21339JLB
<0.210 µg/L 0.210 0.500Bromobenzene 1 07/14/22 23:34 V21339JLB
<0.420 µg/L 0.420 1.00Bromochloromethane 1 07/14/22 23:34 V21339JLB
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 07/14/22 23:34 V21339JLB
<1.50 µg/L 1.50 5.00Bromoform 1 07/14/22 23:34 V21339JLB
<0.280 µg/L 0.280 1.00Bromomethane 1 07/14/22 23:34 V21339JLB
2.86 µg/L 0.180 0.500n-Butylbenzene 1 07/14/22 23:34 V21339JLB
1.35 µg/L 0.200 0.500
sec-Butyl benzene 1 07/14/22 23:34 V21339JLB
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 07/14/22 23:34 V21339JLB
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 07/14/22 23:34 V21339JLB
<0.190 µg/L 0.190 0.500Chlorobenzene 1 07/14/22 23:34 V21339JLB
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 07/14/22 23:34 V21339JLB
<0.430 µg/L 0.430 1.00Chloroethane 1 07/14/22 23:34 V21339JLB
<0.220 µg/L 0.220 0.500Chloroform 1 07/14/22 23:34 V21339JLB
<0.220 µg/L 0.220 0.500
Chloromethane 1 07/14/22 23:34 V21339JLB
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 07/14/22 23:34 V21339JLB
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 07/14/22 23:34 V21339JLB
5.59 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 07/14/22 23:34 V21339JLB
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 07/14/22 23:34 V21339JLB
<0.230 µg/L 0.230 0.500Dibromomethane 1 07/14/22 23:34 V21339JLB
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 07/14/22 23:34 V21339JLB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 8 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-189-0051
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #6117 Received : 07/08/2022
Flash Market #370
Report Date : 07/20/2022
Sample ID :
Lab No :
Sampled:MW-1
93939 Matrix:
7/6/2022 8:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V21337 07/14/22 09:00 V21408 07/15/22 09:00
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 07/14/22 23:34 V21339JLB
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 07/14/22 23:34 V21339JLB
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 07/14/22 23:34 V21339JLB
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 07/14/22 23:34 V21339JLB
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 07/14/22 23:34 V21339JLB
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 07/14/22 23:34 V21339JLB
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 07/14/22 23:34 V21339JLB
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 07/14/22 23:34 V21339JLB
<0.190 µg/L 0.190 0.500
1,2-Dichloropropane 1 07/14/22 23:34 V21339JLB
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 07/14/22 23:34 V21339JLB
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 07/14/22 23:34 V21339JLB
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 07/14/22 23:34 V21339JLB
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 07/14/22 23:34 V21339JLB
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 07/14/22 23:34 V21339JLB
66.7 J µg/L 42.0 200Ethanol 1 07/14/22 23:34 V21339JLB
40.9 µg/L 0.170 0.500
Ethylbenzene 1 07/14/22 23:34 V21339JLB
0.829 J µg/L 0.059 10.0Ethyl Tertiary Butyl Ether (ETBE)1 07/14/22 23:34 V21339JLB
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 07/14/22 23:34 V21339JLB
5.24 µg/L 0.380 1.002-Hexanone 1 07/14/22 23:34 V21339JLB
6.89 µg/L 0.180 0.500Isopropylbenzene 1 07/14/22 23:34 V21339JLB
0.826 µg/L 0.089 0.5004-Isopropyl toluene 1 07/14/22 23:34 V21339JLB
23.7 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 07/14/22 23:34 V21339JLB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 9 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-189-0051
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #6117 Received : 07/08/2022
Flash Market #370
Report Date : 07/20/2022
Sample ID :
Lab No :
Sampled:MW-1
93939 Matrix:
7/6/2022 8:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V21337 07/14/22 09:00 V21408 07/15/22 09:00
3550 µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 07/15/22 18:14 V21409JLB
3.78 µg/L 0.078 1.004-Methyl-2-Pentanone 1 07/14/22 23:34 V21339JLB
<0.330 µg/L 0.330 2.00Methylene Chloride 1 07/14/22 23:34 V21339JLB
8.01 µg/L 0.470 1.00Naphthalene 1 07/14/22 23:34 V21339JLB
11.0 µg/L 0.190 0.500n-Propylbenzene 1 07/14/22 23:34 V21339JLB
<0.220 µg/L 0.220 0.500Styrene 1 07/14/22 23:34 V21339JLB
2640 µg/L 160 1000tert-Butyl Alcohol (TBA)100 07/15/22 18:14 V21409JLB
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 07/14/22 23:34 V21339JLB
1210 µg/L 190 1000
tert-Amyl Alcohol (TAA)100 07/15/22 18:14 V21409JLB
69.0 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 07/14/22 23:34 V21339JLB
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 07/14/22 23:34 V21339JLB
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 07/14/22 23:34 V21339JLB
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 07/14/22 23:34 V21339JLB
40.0 µg/L 0.220 0.500Toluene 1 07/14/22 23:34 V21339JLB
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 07/14/22 23:34 V21339JLB
<0.310 µg/L 0.310 0.500
1,2,4-Trichlorobenzene 1 07/14/22 23:34 V21339JLB
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 07/14/22 23:34 V21339JLB
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 07/14/22 23:34 V21339JLB
<0.180 µg/L 0.180 0.500Trichloroethene 1 07/14/22 23:34 V21339JLB
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 07/14/22 23:34 V21339JLB
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 07/14/22 23:34 V21339JLB
95.7 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 07/14/22 23:34 V21339JLB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 10 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-189-0051
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #6117 Received : 07/08/2022
Flash Market #370
Report Date : 07/20/2022
Sample ID :
Lab No :
Sampled:MW-1
93939 Matrix:
7/6/2022 8:50
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V21337 07/14/22 09:00 V21408 07/15/22 09:00
26.4 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 07/14/22 23:34 V21339JLB
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 07/14/22 23:34 V21339JLB
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 07/14/22 23:34 V21339JLB
66.9 µg/L 0.210 0.500o-Xylene 1 07/14/22 23:34 V21339JLB
143 µg/L 0.420 1.00m,p-Xylene 1 07/14/22 23:34 V21339JLB
210 µg/L 0.210 0.500Xylene (Total)1 07/14/22 23:34 V21339
Surrogate: 4-Bromofluorobenzene 96.8 Limits: 70-130%07/14/22 23:341 JLB V21339
Surrogate: Dibromofluoromethane 99.2 Limits: 70-130%07/14/22 23:341 JLB V21339
Surrogate: 1,2-Dichloroethane - d4 97.0 Limits: 70-130%07/14/22 23:341 JLB V21339
Surrogate: Toluene-d8 100 Limits: 70-130%07/14/22 23:341 JLB V21339
Surrogate: 4-Bromofluorobenzene 99.4 Limits: 70-130%07/15/22 18:14100 JLB V21409
Surrogate: Dibromofluoromethane 96.6 Limits: 70-130%07/15/22 18:14100 JLB V21409
Surrogate: 1,2-Dichloroethane - d4 97.8 Limits: 70-130%07/15/22 18:14100 JLB V21409
Surrogate: Toluene-d8 99.0 Limits: 70-130%07/15/22 18:14100 JLB V21409
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
EPA-504.1(PREP)
EPA-504.1 Prep Batch(es):V21417 07/18/22 13:00
<0.00345 µg/L 0.00345 0.02091,2-Dibromoethane 1 07/18/22 14:04 V21440JC1
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 11 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-189-0051
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #6117 Received : 07/08/2022
Flash Market #370
Report Date : 07/20/2022
Sample ID :
Lab No :
Sampled:MW-1
93939 Matrix:
7/6/2022 8:50
Aqueous
Analytical Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
CALCULATION
846 µg/L 115 500Aliphatic C5-C8 (Adjusted)1 07/14/22 23:34
164 µg/L 25.8 50.0Aliphatics C9-C12 (Adjusted)1 07/14/22 18:59
308 µg/L 4.02 50.0Aromatic C9-C10 (Adjusted)1 07/14/22 18:59
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V21307 07/14/22 08:00
985 µg/L 115 500Aliphatic C5-C8 10 07/15/22 08:41 V21308TBL
723 µg/L 25.8 50.0Aliphatic C9-C12 1 07/14/22 18:59 V21308TBL
308 µg/L 4.02 50.0Aromatic C9-C10 1 07/14/22 18:59 V21308TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)93.8 Limits: 70-130%07/14/22 18:591 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)90.0 Limits: 70-130%07/14/22 18:591 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)94.1 Limits: 70-130%07/15/22 08:4110 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)83.9 Limits: 70-130%07/15/22 08:4110 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 12 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-189-0051
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #6117 Received : 07/08/2022
Flash Market #370
Report Date : 07/20/2022
Sample ID :
Lab No :
Sampled:SB-1-10'
93940 Matrix:
7/6/2022 7:17
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
29.5 %Moisture 1 07/15/22 10:33 SW-DRYWTADC
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 13 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-189-0051
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #6117 Received : 07/08/2022
Flash Market #370
Report Date : 07/20/2022
Sample ID :
Lab No :
Sampled:SB-1-10'
93940 Matrix:
7/6/2022 7:17
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V21179 07/12/22 08:00
0.200 mg/Kg - dry 0.003 0.028Acetone 1 07/12/22 14:00 V21180TBL
<0.001 mg/Kg - dry 0.001 0.028Acrolein 1 07/12/22 14:00 V21180TBL
<0.001 mg/Kg - dry 0.001 0.028Acrylonitrile 1 07/12/22 14:00 V21180TBL
0.002 J mg/Kg - dry 0.0008 0.007Benzene 1 07/12/22 14:00 V21180TBL
<0.0007 mg/Kg - dry 0.0007 0.007Bromobenzene 1 07/12/22 14:00 V21180TBL
<0.001 mg/Kg - dry 0.001 0.007Bromochloromethane 1 07/12/22 14:00 V21180TBL
<0.001 mg/Kg - dry 0.001 0.007Bromodichloromethane 1 07/12/22 14:00 V21180TBL
<0.001 mg/Kg - dry 0.001 0.007Bromoform 1 07/12/22 14:00 V21180TBL
0.002 J
mg/Kg - dry 0.002 0.014
Bromomethane 1 07/12/22 14:00 V21180TBL
<0.0007 mg/Kg - dry 0.0007 0.007n-Butylbenzene 1 07/12/22 14:00 V21180TBL
<0.0008 mg/Kg - dry 0.0008 0.007sec-Butyl benzene 1 07/12/22 14:00 V21180TBL
<0.0007 mg/Kg - dry 0.0007 0.007tert-Butyl benzene 1 07/12/22 14:00 V21180TBL
0.002 J mg/Kg - dry 0.0009 0.007Carbon Disulfide 1 07/12/22 14:00 V21180TBL
<0.002 mg/Kg - dry 0.002 0.007Carbon Tetrachloride 1 07/12/22 14:00 V21180TBL
<0.0010 mg/Kg - dry 0.0010 0.007Chlorobenzene 1 07/12/22 14:00 V21180TBL
<0.001 mg/Kg - dry 0.001 0.007
Chlorodibromomethane 1 07/12/22 14:00 V21180TBL
<0.001 mg/Kg - dry 0.001 0.014Chloroethane 1 07/12/22 14:00 V21180TBL
<0.001 mg/Kg - dry 0.001 0.007Chloroform 1 07/12/22 14:00 V21180TBL
<0.0009 mg/Kg - dry 0.0009 0.014Chloromethane 1 07/12/22 14:00 V21180TBL
<0.0007 mg/Kg - dry 0.0007 0.0072-Chlorotoluene 1 07/12/22 14:00 V21180TBL
<0.0006 mg/Kg - dry 0.0006 0.0074-Chlorotoluene 1 07/12/22 14:00 V21180TBL
<0.001 mg/Kg - dry 0.001 0.007Di-Isopropyl Ether (DIPE)1 07/12/22 14:00 V21180TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 14 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-189-0051
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #6117 Received : 07/08/2022
Flash Market #370
Report Date : 07/20/2022
Sample ID :
Lab No :
Sampled:SB-1-10'
93940 Matrix:
7/6/2022 7:17
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V21179 07/12/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0141,2-Dibromo-3-Chloropropane 1 07/12/22 14:00 V21180TBL
<0.0008 mg/Kg - dry 0.0008 0.0071,2-Dibromoethane 1 07/12/22 14:00 V21180TBL
<0.0008 mg/Kg - dry 0.0008 0.007Dibromomethane 1 07/12/22 14:00 V21180TBL
<0.0004 mg/Kg - dry 0.0004 0.0071,2-Dichlorobenzene 1 07/12/22 14:00 V21180TBL
<0.0005 mg/Kg - dry 0.0005 0.0071,3-Dichlorobenzene 1 07/12/22 14:00 V21180TBL
<0.0009 mg/Kg - dry 0.0009 0.0071,4-Dichlorobenzene 1 07/12/22 14:00 V21180TBL
<0.001 mg/Kg - dry 0.001 0.014Dichlorodifluoromethane 1 07/12/22 14:00 V21180TBL
<0.001 mg/Kg - dry 0.001 0.0071,1-Dichloroethane 1 07/12/22 14:00 V21180TBL
<0.001 mg/Kg - dry 0.001 0.007
1,2-Dichloroethane 1 07/12/22 14:00 V21180TBL
<0.001 mg/Kg - dry 0.001 0.0071,1-Dichloroethene 1 07/12/22 14:00 V21180TBL
<0.001 mg/Kg - dry 0.001 0.007cis-1,2-Dichloroethene 1 07/12/22 14:00 V21180TBL
<0.001 mg/Kg - dry 0.001 0.007trans-1,2-Dichloroethene 1 07/12/22 14:00 V21180TBL
<0.0006 mg/Kg - dry 0.0006 0.0071,2-Dichloropropane 1 07/12/22 14:00 V21180TBL
<0.0008 mg/Kg - dry 0.0008 0.0071,3-Dichloropropane 1 07/12/22 14:00 V21180TBL
<0.001 mg/Kg - dry 0.001 0.0072,2-Dichloropropane 1 07/12/22 14:00 V21180TBL
<0.001 mg/Kg - dry 0.001 0.007
1,1-Dichloropropene 1 07/12/22 14:00 V21180TBL
<0.0008 mg/Kg - dry 0.0008 0.007cis-1,3-Dichloropropene 1 07/12/22 14:00 V21180TBL
<0.001 mg/Kg - dry 0.001 0.007trans-1,3-Dichloropropene 1 07/12/22 14:00 V21180TBL
0.001 J mg/Kg - dry 0.0008 0.007Ethylbenzene 1 07/12/22 14:00 V21180TBL
<0.001 mg/Kg - dry 0.001 0.070Ethyl Tertiary Butyl Ether (ETBE)1 07/12/22 14:00 V21180TBL
<0.001 mg/Kg - dry 0.001 0.014Hexachlorobutadiene 1 07/12/22 14:00 V21180TBL
<0.0009 mg/Kg - dry 0.0009 0.014n-Hexane 1 07/12/22 14:00 V21180TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 15 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-189-0051
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #6117 Received : 07/08/2022
Flash Market #370
Report Date : 07/20/2022
Sample ID :
Lab No :
Sampled:SB-1-10'
93940 Matrix:
7/6/2022 7:17
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V21179 07/12/22 08:00
0.007 J mg/Kg - dry 0.0009 0.0282-Hexanone 1 07/12/22 14:00 V21180TBL
<0.0007 mg/Kg - dry 0.0007 0.007Isopropylbenzene 1 07/12/22 14:00 V21180TBL
<0.001 mg/Kg - dry 0.001 0.0074-Isopropyl toluene 1 07/12/22 14:00 V21180TBL
0.098 mg/Kg - dry 0.0009 0.028Methyl Ethyl Ketone (MEK)1 07/12/22 14:00 V21180TBL
0.234 mg/Kg - dry 0.0009 0.007Methyl tert-butyl ether (MTBE)1 07/12/22 14:00 V21180TBL
<0.021 mg/Kg - dry 0.021 0.0284-Methyl-2-Pentanone 1 07/12/22 14:00 V21180TBL
<0.002 mg/Kg - dry 0.002 0.014Methylene Chloride 1 07/12/22 14:00 V21180TBL
<0.001 mg/Kg - dry 0.001 0.014Naphthalene 1 07/12/22 14:00 V21180TBL
<0.0008 mg/Kg - dry 0.0008 0.007
n-Propylbenzene 1 07/12/22 14:00 V21180TBL
<0.002 mg/Kg - dry 0.002 0.007Styrene 1 07/12/22 14:00 V21180TBL
<0.001 mg/Kg - dry 0.001 0.0071,1,1,2-Tetrachloroethane 1 07/12/22 14:00 V21180TBL
<0.0005 mg/Kg - dry 0.0005 0.0071,1,2,2-Tetrachloroethane 1 07/12/22 14:00 V21180TBL
<0.001 mg/Kg - dry 0.001 0.007Tetrachloroethene 1 07/12/22 14:00 V21180TBL
0.001 J mg/Kg - dry 0.0009 0.007Toluene 1 07/12/22 14:00 V21180TBL
<0.0008 mg/Kg - dry 0.0008 0.0141,2,3-Trichlorobenzene 1 07/12/22 14:00 V21180TBL
<0.0009 mg/Kg - dry 0.0009 0.014
1,2,4-Trichlorobenzene 1 07/12/22 14:00 V21180TBL
<0.002 mg/Kg - dry 0.002 0.0071,1,1-Trichloroethane 1 07/12/22 14:00 V21180TBL
<0.0007 mg/Kg - dry 0.0007 0.0071,1,2-Trichloroethane 1 07/12/22 14:00 V21180TBL
<0.001 mg/Kg - dry 0.001 0.007Trichloroethene 1 07/12/22 14:00 V21180TBL
<0.002 mg/Kg - dry 0.002 0.014Trichlorofluoromethane 1 07/12/22 14:00 V21180TBL
<0.001 mg/Kg - dry 0.001 0.0071,2,3-Trichloropropane 1 07/12/22 14:00 V21180TBL
0.004 J mg/Kg - dry 0.0007 0.0071,2,4-Trimethylbenzene 1 07/12/22 14:00 V21180TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 16 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-189-0051
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #6117 Received : 07/08/2022
Flash Market #370
Report Date : 07/20/2022
Sample ID :
Lab No :
Sampled:SB-1-10'
93940 Matrix:
7/6/2022 7:17
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V21179 07/12/22 08:00
0.001 J mg/Kg - dry 0.0008 0.0071,3,5-Trimethylbenzene 1 07/12/22 14:00 V21180TBL
<0.0007 mg/Kg - dry 0.0007 0.014Vinyl Acetate 1 07/12/22 14:00 V21180TBL
<0.0007 mg/Kg - dry 0.0007 0.014Vinyl Chloride 1 07/12/22 14:00 V21180TBL
0.002 J mg/Kg - dry 0.0007 0.007o-Xylene 1 07/12/22 14:00 V21180TBL
0.006 J mg/Kg - dry 0.001 0.014m,p-Xylene 1 07/12/22 14:00 V21180TBL
0.009 J mg/Kg - dry 0.0007 0.007Xylene (Total)1 07/12/22 14:00 V21180KCC
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%07/12/22 14:001 TBL V21180
Surrogate: Dibromofluoromethane 106 Limits: 84-123%07/12/22 14:001 TBL V21180
Surrogate: Toluene-d8 94.1 Limits: 76-129%07/12/22 14:001 TBL V21180
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 17 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-189-0051
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #6117 Received : 07/08/2022
Flash Market #370
Report Date : 07/20/2022
Sample ID :
Lab No :
Sampled:SB-1-10'
93940 Matrix:
7/6/2022 7:17
Solids
Analytical Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
CALCULATION
<1.96 mg/Kg - dry 12.9Aliphatic C5-C8 (Adjusted)100 07/13/22 15:07
<7.36 mg/Kg - dry 12.9Aliphatics C9-C12 (Adjusted)100 07/13/22 15:07
<1.01 mg/Kg - dry 1.01 12.9Aromatic C9-C10 (Adjusted)100 07/13/22 15:07
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V21222 07/13/22 08:00
<1.96 mg/Kg - dry 1.96 12.9Aliphatic C5-C8 100 07/13/22 15:07 V21223TBL
<7.36 mg/Kg - dry 7.36 12.9Aliphatic C9-C12 100 07/13/22 15:07 V21223TBL
<1.01 mg/Kg - dry 1.01 12.9Aromatic C9-C10 100 07/13/22 15:07 V21223TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)76.9 Limits: 70-130%07/13/22 15:07100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)80.8 Limits: 70-130%07/13/22 15:07100 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 18 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-189-0051
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #6117 Received : 07/08/2022
Flash Market #370
Report Date : 07/20/2022
Sample ID :
Lab No :
Sampled:SB-2-20'
93941 Matrix:
7/6/2022 8:28
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V21222 07/13/22 08:00
<2.89 mg/Kg 2.89 19.0Aliphatic C5-C8 100 07/13/22 15:31 V21223TBL
<10.8 mg/Kg 10.8 19.0Aliphatic C9-C12 100 07/13/22 15:31 V21223TBL
<1.48 mg/Kg 1.48 19.0Aromatic C9-C10 100 07/13/22 15:31 V21223TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)96.3 Limits: 70-130%07/13/22 15:31100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)102 Limits: 70-130%07/13/22 15:31100 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 19 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-189-0051
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #6117 Received : 07/08/2022
Flash Market #370
Report Date : 07/20/2022
Sample ID :
Lab No :
Sampled:Trip Blank
93942 Matrix:
7/6/2022 8:32
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V21337 07/14/22 09:00
2.21 J µg/L 1.80 10.0Acetone 1 07/14/22 19:42 V21339JLB
<0.180 µg/L 0.180 0.500Benzene 1 07/14/22 19:42 V21339JLB
<0.210 µg/L 0.210 0.500Bromobenzene 1 07/14/22 19:42 V21339JLB
<0.420 µg/L 0.420 1.00Bromochloromethane 1 07/14/22 19:42 V21339JLB
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 07/14/22 19:42 V21339JLB
<1.50 µg/L 1.50 5.00Bromoform 1 07/14/22 19:42 V21339JLB
<0.280 µg/L 0.280 1.00Bromomethane 1 07/14/22 19:42 V21339JLB
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 07/14/22 19:42 V21339JLB
<0.200 µg/L 0.200 0.500
sec-Butyl benzene 1 07/14/22 19:42 V21339JLB
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 07/14/22 19:42 V21339JLB
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 07/14/22 19:42 V21339JLB
<0.190 µg/L 0.190 0.500Chlorobenzene 1 07/14/22 19:42 V21339JLB
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 07/14/22 19:42 V21339JLB
<0.430 µg/L 0.430 1.00Chloroethane 1 07/14/22 19:42 V21339JLB
<0.220 µg/L 0.220 0.500Chloroform 1 07/14/22 19:42 V21339JLB
<0.220 µg/L 0.220 0.500
Chloromethane 1 07/14/22 19:42 V21339JLB
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 07/14/22 19:42 V21339JLB
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 07/14/22 19:42 V21339JLB
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 07/14/22 19:42 V21339JLB
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 07/14/22 19:42 V21339JLB
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 07/14/22 19:42 V21339JLB
<0.230 µg/L 0.230 0.500Dibromomethane 1 07/14/22 19:42 V21339JLB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 20 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-189-0051
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #6117 Received : 07/08/2022
Flash Market #370
Report Date : 07/20/2022
Sample ID :
Lab No :
Sampled:Trip Blank
93942 Matrix:
7/6/2022 8:32
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V21337 07/14/22 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 07/14/22 19:42 V21339JLB
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 07/14/22 19:42 V21339JLB
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 07/14/22 19:42 V21339JLB
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 07/14/22 19:42 V21339JLB
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 07/14/22 19:42 V21339JLB
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 07/14/22 19:42 V21339JLB
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 07/14/22 19:42 V21339JLB
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 07/14/22 19:42 V21339JLB
<0.180 µg/L 0.180 0.500
trans-1,2-Dichloroethene 1 07/14/22 19:42 V21339JLB
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 07/14/22 19:42 V21339JLB
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 07/14/22 19:42 V21339JLB
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 07/14/22 19:42 V21339JLB
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 07/14/22 19:42 V21339JLB
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 07/14/22 19:42 V21339JLB
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 07/14/22 19:42 V21339JLB
<42.0 µg/L 42.0 200
Ethanol 1 07/14/22 19:42 V21339JLB
<0.170 µg/L 0.170 0.500Ethylbenzene 1 07/14/22 19:42 V21339JLB
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 07/14/22 19:42 V21339JLB
<0.380 µg/L 0.380 1.002-Hexanone 1 07/14/22 19:42 V21339JLB
<0.180 µg/L 0.180 0.500Isopropylbenzene 1 07/14/22 19:42 V21339JLB
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 07/14/22 19:42 V21339JLB
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 07/14/22 19:42 V21339JLB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 21 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-189-0051
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #6117 Received : 07/08/2022
Flash Market #370
Report Date : 07/20/2022
Sample ID :
Lab No :
Sampled:Trip Blank
93942 Matrix:
7/6/2022 8:32
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V21337 07/14/22 09:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 07/14/22 19:42 V21339JLB
<0.078 µg/L 0.078 1.004-Methyl-2-Pentanone 1 07/14/22 19:42 V21339JLB
<0.330 µg/L 0.330 2.00Methylene Chloride 1 07/14/22 19:42 V21339JLB
<0.470 µg/L 0.470 1.00Naphthalene 1 07/14/22 19:42 V21339JLB
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 07/14/22 19:42 V21339JLB
<0.220 µg/L 0.220 0.500Styrene 1 07/14/22 19:42 V21339JLB
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 07/14/22 19:42 V21339JLB
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 07/14/22 19:42 V21339JLB
<0.220 µg/L 0.220 0.500
Tetrachloroethene 1 07/14/22 19:42 V21339JLB
<0.220 µg/L 0.220 0.500Toluene 1 07/14/22 19:42 V21339JLB
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 07/14/22 19:42 V21339JLB
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 07/14/22 19:42 V21339JLB
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 07/14/22 19:42 V21339JLB
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 07/14/22 19:42 V21339JLB
<0.180 µg/L 0.180 0.500Trichloroethene 1 07/14/22 19:42 V21339JLB
<0.180 µg/L 0.180 0.500
Trichlorofluoromethane 1 07/14/22 19:42 V21339JLB
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 07/14/22 19:42 V21339JLB
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 07/14/22 19:42 V21339JLB
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 07/14/22 19:42 V21339JLB
<1.00 µg/L 1.00 5.00Vinyl Acetate 1 07/14/22 19:42 V21339JLB
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 07/14/22 19:42 V21339JLB
<0.210 µg/L 0.210 0.500o-Xylene 1 07/14/22 19:42 V21339JLB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 22 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-189-0051
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #6117 Received : 07/08/2022
Flash Market #370
Report Date : 07/20/2022
Sample ID :
Lab No :
Sampled:Trip Blank
93942 Matrix:
7/6/2022 8:32
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V21337 07/14/22 09:00
<0.420 µg/L 0.420 1.00m,p-Xylene 1 07/14/22 19:42 V21339JLB
<0.21 µg/L 0.210 0.500Xylene (Total)1 07/14/22 19:42 V21339
Surrogate: 4-Bromofluorobenzene 97.2 Limits: 70-130%07/14/22 19:421 JLB V21339
Surrogate: Dibromofluoromethane 96.6 Limits: 70-130%07/14/22 19:421 JLB V21339
Surrogate: 1,2-Dichloroethane - d4 96.6 Limits: 70-130%07/14/22 19:421 JLB V21339
Surrogate: Toluene-d8 99.4 Limits: 70-130%07/14/22 19:421 JLB V21339
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 23 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-189-0051
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #6117 Received : 07/08/2022
Flash Market #370
Report Date : 07/20/2022
Sample ID :
Lab No :
Sampled:SB-3-30'
93943 Matrix:
7/6/2022 8:38
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
31.2 %Moisture 1 07/15/22 10:33 SW-DRYWTADC
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 24 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-189-0051
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #6117 Received : 07/08/2022
Flash Market #370
Report Date : 07/20/2022
Sample ID :
Lab No :
Sampled:SB-3-30'
93943 Matrix:
7/6/2022 8:38
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V21179 07/12/22 08:00 V21287 07/14/22 08:00
0.123 mg/Kg - dry 0.003 0.029Acetone 1 07/12/22 14:27 V21180TBL
<0.001 mg/Kg - dry 0.001 0.029Acrolein 1 07/12/22 14:27 V21180TBL
<0.001 mg/Kg - dry 0.001 0.029Acrylonitrile 1 07/12/22 14:27 V21180TBL
<0.0008 mg/Kg - dry 0.0008 0.007Benzene 1 07/12/22 14:27 V21180TBL
<0.0007 mg/Kg - dry 0.0007 0.007Bromobenzene 1 07/12/22 14:27 V21180TBL
<0.001 mg/Kg - dry 0.001 0.007Bromochloromethane 1 07/12/22 14:27 V21180TBL
<0.001 mg/Kg - dry 0.001 0.007Bromodichloromethane 1 07/12/22 14:27 V21180TBL
<0.001 mg/Kg - dry 0.001 0.007Bromoform 1 07/12/22 14:27 V21180TBL
<0.002 mg/Kg - dry 0.002 0.014
Bromomethane 1 07/12/22 14:27 V21180TBL
<0.0007 mg/Kg - dry 0.0007 0.007n-Butylbenzene 1 07/12/22 14:27 V21180TBL
<0.0008 mg/Kg - dry 0.0008 0.007sec-Butyl benzene 1 07/12/22 14:27 V21180TBL
<0.0007 mg/Kg - dry 0.0007 0.007tert-Butyl benzene 1 07/12/22 14:27 V21180TBL
<0.0009 mg/Kg - dry 0.0009 0.007Carbon Disulfide 1 07/12/22 14:27 V21180TBL
<0.002 mg/Kg - dry 0.002 0.007Carbon Tetrachloride 1 07/12/22 14:27 V21180TBL
<0.0010 mg/Kg - dry 0.0010 0.007Chlorobenzene 1 07/12/22 14:27 V21180TBL
<0.001 mg/Kg - dry 0.001 0.007
Chlorodibromomethane 1 07/12/22 14:27 V21180TBL
<0.001 mg/Kg - dry 0.001 0.014Chloroethane 1 07/12/22 14:27 V21180TBL
<0.001 mg/Kg - dry 0.001 0.007Chloroform 1 07/12/22 14:27 V21180TBL
<0.0009 mg/Kg - dry 0.0009 0.014Chloromethane 1 07/12/22 14:27 V21180TBL
<0.0007 mg/Kg - dry 0.0007 0.0072-Chlorotoluene 1 07/12/22 14:27 V21180TBL
<0.0006 mg/Kg - dry 0.0006 0.0074-Chlorotoluene 1 07/12/22 14:27 V21180TBL
0.001 J mg/Kg - dry 0.001 0.007Di-Isopropyl Ether (DIPE)1 07/12/22 14:27 V21180TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 25 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-189-0051
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #6117 Received : 07/08/2022
Flash Market #370
Report Date : 07/20/2022
Sample ID :
Lab No :
Sampled:SB-3-30'
93943 Matrix:
7/6/2022 8:38
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V21179 07/12/22 08:00 V21287 07/14/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0141,2-Dibromo-3-Chloropropane 1 07/12/22 14:27 V21180TBL
<0.0009 mg/Kg - dry 0.0009 0.0071,2-Dibromoethane 1 07/12/22 14:27 V21180TBL
<0.0008 mg/Kg - dry 0.0008 0.007Dibromomethane 1 07/12/22 14:27 V21180TBL
<0.0005 mg/Kg - dry 0.0005 0.0071,2-Dichlorobenzene 1 07/12/22 14:27 V21180TBL
<0.0006 mg/Kg - dry 0.0006 0.0071,3-Dichlorobenzene 1 07/12/22 14:27 V21180TBL
<0.0009 mg/Kg - dry 0.0009 0.0071,4-Dichlorobenzene 1 07/12/22 14:27 V21180TBL
<0.002 mg/Kg - dry 0.002 0.014Dichlorodifluoromethane 1 07/12/22 14:27 V21180TBL
<0.001 mg/Kg - dry 0.001 0.0071,1-Dichloroethane 1 07/12/22 14:27 V21180TBL
<0.002 mg/Kg - dry 0.002 0.007
1,2-Dichloroethane 1 07/12/22 14:27 V21180TBL
<0.001 mg/Kg - dry 0.001 0.0071,1-Dichloroethene 1 07/12/22 14:27 V21180TBL
<0.001 mg/Kg - dry 0.001 0.007cis-1,2-Dichloroethene 1 07/12/22 14:27 V21180TBL
<0.001 mg/Kg - dry 0.001 0.007trans-1,2-Dichloroethene 1 07/12/22 14:27 V21180TBL
<0.0006 mg/Kg - dry 0.0006 0.0071,2-Dichloropropane 1 07/12/22 14:27 V21180TBL
<0.0008 mg/Kg - dry 0.0008 0.0071,3-Dichloropropane 1 07/12/22 14:27 V21180TBL
<0.001 mg/Kg - dry 0.001 0.0072,2-Dichloropropane 1 07/12/22 14:27 V21180TBL
<0.001 mg/Kg - dry 0.001 0.007
1,1-Dichloropropene 1 07/12/22 14:27 V21180TBL
<0.0008 mg/Kg - dry 0.0008 0.007cis-1,3-Dichloropropene 1 07/12/22 14:27 V21180TBL
<0.001 mg/Kg - dry 0.001 0.007trans-1,3-Dichloropropene 1 07/12/22 14:27 V21180TBL
<0.0008 mg/Kg - dry 0.0008 0.007Ethylbenzene 1 07/12/22 14:27 V21180TBL
<0.001 mg/Kg - dry 0.001 0.072Ethyl Tertiary Butyl Ether (ETBE)1 07/12/22 14:27 V21180TBL
<0.001 mg/Kg - dry 0.001 0.014Hexachlorobutadiene 1 07/12/22 14:27 V21180TBL
<0.0010 mg/Kg - dry 0.0010 0.014n-Hexane 1 07/12/22 14:27 V21180TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 26 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-189-0051
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #6117 Received : 07/08/2022
Flash Market #370
Report Date : 07/20/2022
Sample ID :
Lab No :
Sampled:SB-3-30'
93943 Matrix:
7/6/2022 8:38
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V21179 07/12/22 08:00 V21287 07/14/22 08:00
<0.0009 mg/Kg - dry 0.0009 0.0292-Hexanone 1 07/12/22 14:27 V21180TBL
<0.0007 mg/Kg - dry 0.0007 0.007Isopropylbenzene 1 07/12/22 14:27 V21180TBL
<0.001 mg/Kg - dry 0.001 0.0074-Isopropyl toluene 1 07/12/22 14:27 V21180TBL
0.018 J mg/Kg - dry 0.0009 0.029Methyl Ethyl Ketone (MEK)1 07/12/22 14:27 V21180TBL
2.24 mg/Kg - dry 0.022 0.181Methyl tert-butyl ether (MTBE)50 07/14/22 12:17 V21288TBL
<0.021 mg/Kg - dry 0.021 0.0294-Methyl-2-Pentanone 1 07/12/22 14:27 V21180TBL
<0.002 mg/Kg - dry 0.002 0.014Methylene Chloride 1 07/12/22 14:27 V21180TBL
<0.001 mg/Kg - dry 0.001 0.014Naphthalene 1 07/12/22 14:27 V21180TBL
<0.0008 mg/Kg - dry 0.0008 0.007
n-Propylbenzene 1 07/12/22 14:27 V21180TBL
<0.002 mg/Kg - dry 0.002 0.007Styrene 1 07/12/22 14:27 V21180TBL
<0.001 mg/Kg - dry 0.001 0.0071,1,1,2-Tetrachloroethane 1 07/12/22 14:27 V21180TBL
<0.0005 mg/Kg - dry 0.0005 0.0071,1,2,2-Tetrachloroethane 1 07/12/22 14:27 V21180TBL
<0.001 mg/Kg - dry 0.001 0.007Tetrachloroethene 1 07/12/22 14:27 V21180TBL
<0.0010 mg/Kg - dry 0.0010 0.007Toluene 1 07/12/22 14:27 V21180TBL
<0.0008 mg/Kg - dry 0.0008 0.0141,2,3-Trichlorobenzene 1 07/12/22 14:27 V21180TBL
<0.0009 mg/Kg - dry 0.0009 0.014
1,2,4-Trichlorobenzene 1 07/12/22 14:27 V21180TBL
<0.002 mg/Kg - dry 0.002 0.0071,1,1-Trichloroethane 1 07/12/22 14:27 V21180TBL
<0.0007 mg/Kg - dry 0.0007 0.0071,1,2-Trichloroethane 1 07/12/22 14:27 V21180TBL
<0.001 mg/Kg - dry 0.001 0.007Trichloroethene 1 07/12/22 14:27 V21180TBL
<0.003 mg/Kg - dry 0.003 0.014Trichlorofluoromethane 1 07/12/22 14:27 V21180TBL
<0.001 mg/Kg - dry 0.001 0.0071,2,3-Trichloropropane 1 07/12/22 14:27 V21180TBL
0.001 J mg/Kg - dry 0.0007 0.0071,2,4-Trimethylbenzene 1 07/12/22 14:27 V21180TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 27 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-189-0051
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #6117 Received : 07/08/2022
Flash Market #370
Report Date : 07/20/2022
Sample ID :
Lab No :
Sampled:SB-3-30'
93943 Matrix:
7/6/2022 8:38
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V21179 07/12/22 08:00 V21287 07/14/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.0071,3,5-Trimethylbenzene 1 07/12/22 14:27 V21180TBL
<0.0007 mg/Kg - dry 0.0007 0.014Vinyl Acetate 1 07/12/22 14:27 V21180TBL
<0.0007 mg/Kg - dry 0.0007 0.014Vinyl Chloride 1 07/12/22 14:27 V21180TBL
0.0008 J mg/Kg - dry 0.0007 0.007o-Xylene 1 07/12/22 14:27 V21180TBL
<0.001 mg/Kg - dry 0.001 0.014m,p-Xylene 1 07/12/22 14:27 V21180TBL
0.0008 J mg/Kg - dry 0.0007 0.007Xylene (Total)1 07/12/22 14:27 V21180KCC
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%07/12/22 14:271 TBL V21180
Surrogate: Dibromofluoromethane 104 Limits: 84-123%07/12/22 14:271 TBL V21180
Surrogate: Toluene-d8 94.2 Limits: 76-129%07/12/22 14:271 TBL V21180
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%07/14/22 12:1750 TBL V21288
Surrogate: Dibromofluoromethane 103 Limits: 70-130%07/14/22 12:1750 TBL V21288
Surrogate: Toluene-d8 93.8 Limits: 76-129%07/14/22 12:1750 TBL V21288
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 28 of 50
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-189-0051
00087
Geological Resources, Inc.
3502 Hayes Road
Laura Minor
Monroe
Danyale Love
Project Manager
GRI #6117 Received : 07/08/2022
Flash Market #370
Report Date : 07/20/2022
Sample ID :
Lab No :
Sampled:SB-3-30'
93943 Matrix:
7/6/2022 8:38
Solids
Analytical Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
CALCULATION
<1.92 mg/Kg - dry 1.92 12.7Aliphatic C5-C8 (Adjusted)1 07/12/22 14:27
<7.21 mg/Kg - dry 12.7Aliphatics C9-C12 (Adjusted)100 07/13/22 15:54
<0.986 mg/Kg - dry 0.986 12.7Aromatic C9-C10 (Adjusted)100 07/13/22 15:54
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V21222 07/13/22 08:00
<1.92 mg/Kg - dry 1.92 12.7Aliphatic C5-C8 100 07/13/22 15:54 V21223TBL
<7.21 mg/Kg - dry 7.21 12.7Aliphatic C9-C12 100 07/13/22 15:54 V21223TBL
<0.986 mg/Kg - dry 0.986 12.7Aromatic C9-C10 100 07/13/22 15:54 V21223TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)83.1 Limits: 70-130%07/13/22 15:54100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)82.5 Limits: 70-130%07/13/22 15:54100 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Page 29 of 50
Quality Control Data
22-189-0051Report No:
Project Description:
Client ID:Geological Resources, Inc.
Flash Market #370
QC Prep Batch Method:
Metals Analyses
6020B
V21310QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3005A
QC Prep:V21216
Associated Lab Samples: 93939
LRB-V21216 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
07/14/22 13:421.000.500<0.500µg/LLead
LCS-V21216Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
99.098.7100µg/LLead 80-120
V 93939-MS-V21216 V 93939-MSD-V21216Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
98.6 99.098.6100100< 0.500µg/LLead 99.0 75-125 0.0 20.0
V 93939-PDS-V21216Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
07/14/22 14:1410451.8µg/LLead
Page 1 of 19Date:07/20/2022 04:15 PM
Page 30 of 50
Quality Control Data
22-189-0051Report No:
Project Description:
Client ID:Geological Resources, Inc.
Flash Market #370
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V21339QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V21337
Associated Lab Samples: 93939, 93942
LRB-V21337 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/14/22 18:2410.01.80<1.80µg/LAcetone
07/14/22 18:240.5000.180<0.180µg/LBenzene
07/14/22 18:240.5000.210<0.210µg/LBromobenzene
07/14/22 18:241.000.420<0.420µg/LBromochloromethane
07/14/22 18:240.5000.160<0.160µg/LBromodichloromethane
07/14/22 18:245.001.50<1.50µg/LBromoform
07/14/22 18:241.000.280<0.280µg/LBromomethane
07/14/22 18:240.5000.180<0.180µg/Ln-Butylbenzene
07/14/22 18:240.5000.200<0.200µg/Lsec-Butyl benzene
07/14/22 18:242.000.920<0.920µg/Ltert-Butyl benzene
07/14/22 18:240.5000.180<0.180µg/LCarbon Tetrachloride
07/14/22 18:240.5000.190<0.190µg/LChlorobenzene
07/14/22 18:240.5000.190<0.190µg/LChlorodibromomethane
07/14/22 18:241.000.430<0.430µg/LChloroethane
07/14/22 18:240.5000.220<0.220µg/LChloroform
07/14/22 18:240.5000.220<0.220µg/LChloromethane
07/14/22 18:240.5000.200<0.200µg/L2-Chlorotoluene
07/14/22 18:240.5000.200<0.200µg/L4-Chlorotoluene
07/14/22 18:240.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
07/14/22 18:242.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
07/14/22 18:240.5000.200<0.200µg/L1,2-Dibromoethane
07/14/22 18:240.5000.230<0.230µg/LDibromomethane
07/14/22 18:240.5000.220<0.220µg/L1,2-Dichlorobenzene
07/14/22 18:240.5000.190<0.190µg/L1,3-Dichlorobenzene
07/14/22 18:240.5000.210<0.210µg/L1,4-Dichlorobenzene
07/14/22 18:245.001.20<1.20µg/LDichlorodifluoromethane
07/14/22 18:240.5000.240<0.240µg/L1,1-Dichloroethane
Page 2 of 19Date:07/20/2022 04:15 PM
Page 31 of 50
Quality Control Data
22-189-0051Report No:
Project Description:
Client ID:Geological Resources, Inc.
Flash Market #370
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V21339QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V21337
Associated Lab Samples: 93939, 93942
LRB-V21337 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/14/22 18:240.5000.150<0.150µg/L1,2-Dichloroethane
07/14/22 18:240.5000.150<0.150µg/L1,1-Dichloroethene
07/14/22 18:240.5000.200<0.200µg/Lcis-1,2-Dichloroethene
07/14/22 18:240.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
07/14/22 18:240.5000.190<0.190µg/L1,2-Dichloropropane
07/14/22 18:240.5000.130<0.130µg/L1,3-Dichloropropane
07/14/22 18:242.000.210<0.210µg/L2,2-Dichloropropane
07/14/22 18:240.5000.200<0.200µg/L1,1-Dichloropropene
07/14/22 18:240.5000.210<0.210µg/Lcis-1,3-Dichloropropene
07/14/22 18:240.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
07/14/22 18:2420042.0<42.0µg/LEthanol
07/14/22 18:240.5000.170<0.170µg/LEthylbenzene
07/14/22 18:2410.00.059<0.059µg/LEthyl Tertiary Butyl Ether (ETBE)
07/14/22 18:243.000.350<0.350µg/LHexachlorobutadiene
07/14/22 18:241.000.380<0.380µg/L2-Hexanone
07/14/22 18:240.5000.180<0.180µg/LIsopropylbenzene
07/14/22 18:240.5000.089<0.089µg/L4-Isopropyl toluene
07/14/22 18:245.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
07/14/22 18:241.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
07/14/22 18:241.000.078<0.078µg/L4-Methyl-2-Pentanone
07/14/22 18:242.000.330<0.330µg/LMethylene Chloride
07/14/22 18:241.000.470<0.470µg/LNaphthalene
07/14/22 18:240.5000.190<0.190µg/Ln-Propylbenzene
07/14/22 18:240.5000.220<0.220µg/LStyrene
07/14/22 18:2410.00.350<0.350µg/Ltert-Butyl formate (TBF)
07/14/22 18:2410.00.280<0.280µg/Ltert-Amyl Methyl Ether (TAME)
07/14/22 18:240.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
Page 3 of 19Date:07/20/2022 04:15 PM
Page 32 of 50
Quality Control Data
22-189-0051Report No:
Project Description:
Client ID:Geological Resources, Inc.
Flash Market #370
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V21339QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V21337
Associated Lab Samples: 93939, 93942
LRB-V21337 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/14/22 18:240.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
07/14/22 18:240.5000.220<0.220µg/LTetrachloroethene
07/14/22 18:240.5000.220<0.220µg/LToluene
07/14/22 18:240.5000.380<0.380µg/L1,2,3-Trichlorobenzene
07/14/22 18:240.5000.310<0.310µg/L1,2,4-Trichlorobenzene
07/14/22 18:240.5000.160<0.160µg/L1,1,1-Trichloroethane
07/14/22 18:240.5000.096<0.096µg/L1,1,2-Trichloroethane
07/14/22 18:240.5000.180<0.180µg/LTrichloroethene
07/14/22 18:240.5000.180<0.180µg/LTrichlorofluoromethane
07/14/22 18:240.5000.270<0.270µg/L1,2,3-Trichloropropane
07/14/22 18:240.5000.190<0.190µg/L1,2,4-Trimethylbenzene
07/14/22 18:240.5000.180<0.180µg/L1,3,5-Trimethylbenzene
07/14/22 18:245.001.00<1.00µg/LVinyl Acetate
07/14/22 18:240.5000.170<0.170µg/LVinyl Chloride
07/14/22 18:240.5000.210<0.210µg/Lo-Xylene
07/14/22 18:241.000.420<0.420µg/Lm,p-Xylene
07/14/22 18:244-Bromofluorobenzene (S)99.6 70-130
07/14/22 18:24Dibromofluoromethane (S)98.2 70-130
07/14/22 18:241,2-Dichloroethane - d4 (S)98.0 70-130
07/14/22 18:24Toluene-d8 (S)99.4 70-130
LCS-V21337 LCSD-V21337Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
39.7 99.299.739.940.0µg/LAcetone 40-160 0.5 20.0
19.5 97.510420.720.0µg/LBenzene 70-130 5.9 20.0
Page 4 of 19Date:07/20/2022 04:15 PM
Page 33 of 50
Quality Control Data
22-189-0051Report No:
Project Description:
Client ID:Geological Resources, Inc.
Flash Market #370
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V21339QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V21337
LCS-V21337 LCSD-V21337Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
19.6 98.010120.220.0µg/LBromobenzene 70-130 3.0 20.0
19.7 98.510220.320.0µg/LBromochloromethane 70-130 3.0 20.0
20.6 10310420.720.0µg/LBromodichloromethane 70-130 0.4 20.0
23.1 11611523.020.0µg/LBromoform 70-130 0.4 20.0
19.5 97.594.018.820.0µg/LBromomethane 60-140 3.6 20.0
19.8 99.010420.720.0µg/Ln-Butylbenzene 70-130 4.4 20.0
19.9 99.510420.720.0µg/Lsec-Butyl benzene 70-130 3.9 20.0
20.2 10110320.620.0µg/Ltert-Butyl benzene 70-130 1.9 20.0
20.5 10310320.520.0µg/LCarbon Tetrachloride 70-130 0.0 20.0
20.4 10210721.320.0µg/LChlorobenzene 70-130 4.3 20.0
21.3 10711422.720.0µg/LChlorodibromomethane 70-130 6.3 20.0
19.0 95.096.519.320.0µg/LChloroethane 60-140 1.5 20.0
20.1 10110521.020.0µg/LChloroform 70-130 4.3 20.0
19.1 95.599.019.820.0µg/LChloromethane 60-140 3.5 20.0
19.9 99.510320.520.0µg/L2-Chlorotoluene 70-130 2.9 20.0
19.8 99.010120.220.0µg/L4-Chlorotoluene 70-130 2.0 20.0
19.9 99.510420.720.0µg/LDi-Isopropyl Ether (DIPE)70-130 3.9 20.0
17.7 88.598.519.720.0µg/L1,2-Dibromo-3-Chloropropane 70-130 10.6 20.0
20.7 10410521.020.0µg/L1,2-Dibromoethane 70-130 1.4 20.0
20.1 10199.519.920.0µg/LDibromomethane 70-130 1.0 20.0
20.9 10510420.820.0µg/L1,2-Dichlorobenzene 70-130 0.4 20.0
19.8 99.010420.720.0µg/L1,3-Dichlorobenzene 70-130 4.4 20.0
19.3 96.510020.020.0µg/L1,4-Dichlorobenzene 70-130 3.5 20.0
20.1 10110821.520.0µg/LDichlorodifluoromethane 60-140 6.7 20.0
19.9 99.510420.820.0µg/L1,1-Dichloroethane 70-130 4.4 20.0
18.7 93.597.019.420.0µg/L1,2-Dichloroethane 70-130 3.6 20.0
Page 5 of 19Date:07/20/2022 04:15 PM
Page 34 of 50
Quality Control Data
22-189-0051Report No:
Project Description:
Client ID:Geological Resources, Inc.
Flash Market #370
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V21339QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V21337
LCS-V21337 LCSD-V21337Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
20.0 10010320.520.0µg/L1,1-Dichloroethene 70-130 2.4 20.0
20.2 10110621.220.0µg/Lcis-1,2-Dichloroethene 70-130 4.8 20.0
20.4 10210921.720.0µg/Ltrans-1,2-Dichloroethene 70-130 6.1 20.0
18.8 94.010120.120.0µg/L1,2-Dichloropropane 70-130 6.6 20.0
20.1 10110721.420.0µg/L1,3-Dichloropropane 70-130 6.2 20.0
19.9 99.510621.220.0µg/L2,2-Dichloropropane 70-130 6.3 20.0
19.9 99.510320.520.0µg/L1,1-Dichloropropene 70-130 2.9 20.0
20.3 10210721.420.0µg/Lcis-1,3-Dichloropropene 70-130 5.2 20.0
20.3 10210721.420.0µg/Ltrans-1,3-Dichloropropene 70-130 5.2 20.0
575 115105526500µg/LEthanol 60-140 8.9 20.0
19.8 99.010220.420.0µg/LEthylbenzene 70-130 2.9 20.0
42.5 10611043.840.0µg/LEthyl Tertiary Butyl Ether (ETBE)70-130 3.0 20.0
20.5 10310821.620.0µg/LHexachlorobutadiene 70-130 5.2 20.0
19.9 99.510120.220.0µg/L2-Hexanone 60-140 1.4 20.0
19.9 99.510220.320.0µg/LIsopropylbenzene 70-130 1.9 20.0
20.5 10310721.320.0µg/L4-Isopropyl toluene 70-130 3.8 20.0
22.4 11294.518.920.0µg/LMethyl Ethyl Ketone (MEK)60-140 16.9 20.0
20.6 10310521.020.0µg/LMethyl tert-butyl ether (MTBE)70-130 1.9 20.0
19.8 99.010520.920.0µg/L4-Methyl-2-Pentanone 60-140 5.4 20.0
20.0 10010420.720.0µg/LMethylene Chloride 70-130 3.4 20.0
18.2 91.094.518.920.0µg/LNaphthalene 70-130 3.7 20.0
19.8 99.010320.620.0µg/Ln-Propylbenzene 70-130 3.9 20.0
20.7 10410821.520.0µg/LStyrene 70-130 3.7 20.0
49.1 12312248.840.0µg/Ltert-Butyl formate (TBF)40-140 0.6 20.0
43.0 10810943.540.0µg/Ltert-Amyl Methyl Ether (TAME)40-140 1.1 20.0
21.0 10510621.220.0µg/L1,1,1,2-Tetrachloroethane 70-130 0.9 20.0
Page 6 of 19Date:07/20/2022 04:15 PM
Page 35 of 50
Quality Control Data
22-189-0051Report No:
Project Description:
Client ID:Geological Resources, Inc.
Flash Market #370
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V21339QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V21337
LCS-V21337 LCSD-V21337Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
20.8 10410120.220.0µg/L1,1,2,2-Tetrachloroethane 70-130 2.9 20.0
19.8 99.010420.720.0µg/LTetrachloroethene 70-130 4.4 20.0
19.3 96.510020.020.0µg/LToluene 70-130 3.5 20.0
19.5 97.510420.720.0µg/L1,2,3-Trichlorobenzene 70-130 5.9 20.0
19.7 98.510120.220.0µg/L1,2,4-Trichlorobenzene 70-130 2.5 20.0
20.5 10310621.120.0µg/L1,1,1-Trichloroethane 70-130 2.8 20.0
21.0 10510420.820.0µg/L1,1,2-Trichloroethane 70-130 0.9 20.0
19.7 98.510320.520.0µg/LTrichloroethene 70-130 3.9 20.0
20.1 10110621.220.0µg/LTrichlorofluoromethane 60-140 5.3 20.0
19.4 97.010320.520.0µg/L1,2,3-Trichloropropane 70-130 5.5 20.0
19.8 99.010020.020.0µg/L1,2,4-Trimethylbenzene 70-130 1.0 20.0
19.9 99.510420.720.0µg/L1,3,5-Trimethylbenzene 70-130 3.9 20.0
23.6 11812725.320.0µg/LVinyl Acetate 60-140 6.9 20.0
19.0 95.010220.420.0µg/LVinyl Chloride 60-140 7.1 20.0
20.1 10110320.620.0µg/Lo-Xylene 70-130 2.4 20.0
40.7 10210642.340.0µg/Lm,p-Xylene 70-130 3.8 20.0
99.099.44-Bromofluorobenzene (S)70-130
99.8102Dibromofluoromethane (S)70-130
98.498.61,2-Dichloroethane - d4 (S)70-130
99.4101Toluene-d8 (S)70-130
Page 7 of 19Date:07/20/2022 04:15 PM
Page 36 of 50
Quality Control Data
22-189-0051Report No:
Project Description:
Client ID:Geological Resources, Inc.
Flash Market #370
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V21409QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V21408
Associated Lab Samples: 93939
LRB-V21408 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/15/22 13:431.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
07/15/22 13:4310.01.60<1.60µg/Ltert-Butyl Alcohol (TBA)
07/15/22 13:4310.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
07/15/22 13:434-Bromofluorobenzene (S)100 70-130
07/15/22 13:43Dibromofluoromethane (S)96.6 70-130
07/15/22 13:431,2-Dichloroethane - d4 (S)98.4 70-130
07/15/22 13:43Toluene-d8 (S)98.8 70-130
LCS-V21408 LCSD-V21408Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
20.8 10410220.420.0µg/LMethyl tert-butyl ether (MTBE)70-130 1.9 20.0
43.6 10910642.240.0µg/Ltert-Butyl Alcohol (TBA)40-140 3.2 20.0
19.3 96.511322.520.0µg/Ltert-Amyl Alcohol (TAA)40-140 15.3 20.0
98.899.04-Bromofluorobenzene (S)70-130
99.699.8Dibromofluoromethane (S)70-130
99.096.41,2-Dichloroethane - d4 (S)70-130
98.699.2Toluene-d8 (S)70-130
Page 8 of 19Date:07/20/2022 04:15 PM
Page 37 of 50
Quality Control Data
22-189-0051Report No:
Project Description:
Client ID:Geological Resources, Inc.
Flash Market #370
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V21180QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V21179
Associated Lab Samples: 93940, 93943
LRB-V21179 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/12/22 12:080.0200.002<0.002mg/KgAcetone
07/12/22 12:080.0200.001<0.001mg/KgAcrolein
07/12/22 12:080.0200.0008<0.0008mg/KgAcrylonitrile
07/12/22 12:080.0050.0006<0.0006mg/KgBenzene
07/12/22 12:080.0050.0005<0.0005mg/KgBromobenzene
07/12/22 12:080.0050.0008<0.0008mg/KgBromochloromethane
07/12/22 12:080.0050.001<0.001mg/KgBromodichloromethane
07/12/22 12:080.0050.001<0.001mg/KgBromoform
07/12/22 12:080.0100.001<0.001mg/KgBromomethane
07/12/22 12:080.0050.0005<0.0005mg/Kgn-Butylbenzene
07/12/22 12:080.0050.0006<0.0006mg/Kgsec-Butyl benzene
07/12/22 12:080.0050.0005<0.0005mg/Kgtert-Butyl benzene
07/12/22 12:080.0050.0006<0.0006mg/KgCarbon Disulfide
07/12/22 12:080.0050.001<0.001mg/KgCarbon Tetrachloride
07/12/22 12:080.0050.0007<0.0007mg/KgChlorobenzene
07/12/22 12:080.0050.0009<0.0009mg/KgChlorodibromomethane
07/12/22 12:080.0100.0009<0.0009mg/KgChloroethane
07/12/22 12:080.0050.001<0.001mg/KgChloroform
07/12/22 12:080.0100.0006<0.0006mg/KgChloromethane
07/12/22 12:080.0050.0005<0.0005mg/Kg2-Chlorotoluene
07/12/22 12:080.0050.0004<0.0004mg/Kg4-Chlorotoluene
07/12/22 12:080.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
07/12/22 12:080.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
07/12/22 12:080.0050.0006<0.0006mg/Kg1,2-Dibromoethane
07/12/22 12:080.0050.0006<0.0006mg/KgDibromomethane
07/12/22 12:080.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
07/12/22 12:080.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 9 of 19Date:07/20/2022 04:15 PM
Page 38 of 50
Quality Control Data
22-189-0051Report No:
Project Description:
Client ID:Geological Resources, Inc.
Flash Market #370
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V21180QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V21179
Associated Lab Samples: 93940, 93943
LRB-V21179 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/12/22 12:080.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
07/12/22 12:080.0100.001<0.001mg/KgDichlorodifluoromethane
07/12/22 12:080.0050.0008<0.0008mg/Kg1,1-Dichloroethane
07/12/22 12:080.0050.001<0.001mg/Kg1,2-Dichloroethane
07/12/22 12:080.0050.0007<0.0007mg/Kg1,1-Dichloroethene
07/12/22 12:080.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
07/12/22 12:080.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
07/12/22 12:080.0050.0004<0.0004mg/Kg1,2-Dichloropropane
07/12/22 12:080.0050.0006<0.0006mg/Kg1,3-Dichloropropane
07/12/22 12:080.0050.001<0.001mg/Kg2,2-Dichloropropane
07/12/22 12:080.0050.0008<0.0008mg/Kg1,1-Dichloropropene
07/12/22 12:080.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
07/12/22 12:080.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
07/12/22 12:080.0050.0006<0.0006mg/KgEthylbenzene
07/12/22 12:080.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
07/12/22 12:080.0100.0008<0.0008mg/KgHexachlorobutadiene
07/12/22 12:080.0100.0007<0.0007mg/Kgn-Hexane
07/12/22 12:080.0200.0006<0.0006mg/Kg2-Hexanone
07/12/22 12:080.0050.0005<0.0005mg/KgIsopropylbenzene
07/12/22 12:080.0050.001<0.001mg/Kg4-Isopropyl toluene
07/12/22 12:080.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
07/12/22 12:080.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
07/12/22 12:080.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
07/12/22 12:080.0100.001<0.001mg/KgMethylene Chloride
07/12/22 12:080.0100.0010<0.0010mg/KgNaphthalene
07/12/22 12:080.0050.0005<0.0005mg/Kgn-Propylbenzene
07/12/22 12:080.0050.001<0.001mg/KgStyrene
Page 10 of 19Date:07/20/2022 04:15 PM
Page 39 of 50
Quality Control Data
22-189-0051Report No:
Project Description:
Client ID:Geological Resources, Inc.
Flash Market #370
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V21180QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V21179
Associated Lab Samples: 93940, 93943
LRB-V21179 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/12/22 12:080.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
07/12/22 12:080.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
07/12/22 12:080.0050.0009<0.0009mg/KgTetrachloroethene
07/12/22 12:080.0050.0007<0.0007mg/KgToluene
07/12/22 12:080.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
07/12/22 12:080.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
07/12/22 12:080.0050.001<0.001mg/Kg1,1,1-Trichloroethane
07/12/22 12:080.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
07/12/22 12:080.0050.0009<0.0009mg/KgTrichloroethene
07/12/22 12:080.0100.002<0.002mg/KgTrichlorofluoromethane
07/12/22 12:080.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
07/12/22 12:080.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
07/12/22 12:080.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
07/12/22 12:080.0100.0005<0.0005mg/KgVinyl Acetate
07/12/22 12:080.0100.0005<0.0005mg/KgVinyl Chloride
07/12/22 12:080.0050.0005<0.0005mg/Kgo-Xylene
07/12/22 12:080.0100.001<0.001mg/Kgm,p-Xylene
07/12/22 12:084-Bromofluorobenzene (S)101 70-130
07/12/22 12:08Dibromofluoromethane (S)103 84-123
07/12/22 12:08Toluene-d8 (S)95.8 76-129
LCS-V21179 LCSD-V21179Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.094 94.996.40.0960.100mg/KgAcetone 29-198 1.5 20
0.093 93.089.90.0890.100mg/KgAcrolein 70-130 3.3 20
Page 11 of 19Date:07/20/2022 04:15 PM
Page 40 of 50
Quality Control Data
22-189-0051Report No:
Project Description:
Client ID:Geological Resources, Inc.
Flash Market #370
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V21180QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V21179
LCS-V21179 LCSD-V21179Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.113 1131120.1120.100mg/KgAcrylonitrile 65-134 0.8 20
0.052 1051080.0540.050mg/KgBenzene 74-127 2.8 20
0.048 96.699.00.0490.050mg/KgBromobenzene 73-125 2.4 20
0.055 1111140.0560.050mg/KgBromochloromethane 72-134 2.3 20
0.052 1051060.0520.050mg/KgBromodichloromethane 75-122 0.9 20
0.048 96.096.60.0480.050mg/KgBromoform 66-135 0.6 20
0.051 1031060.0530.050mg/KgBromomethane 20-180 3.0 20
0.049 98.01020.0510.050mg/Kgn-Butylbenzene 65-135 4.0 20
0.046 93.897.60.0480.050mg/Kgsec-Butyl benzene 66-131 3.9 20
0.046 93.295.40.0470.050mg/Kgtert-Butyl benzene 67-132 2.3 20
0.052 1061120.0560.050mg/KgCarbon Disulfide 61-129 5.8 20
0.050 1011050.0520.050mg/KgCarbon Tetrachloride 64-143 3.5 20
0.049 99.01030.0510.050mg/KgChlorobenzene 74-118 3.7 20
0.047 95.896.40.0480.050mg/KgChlorodibromomethane 73-122 0.6 20
0.052 1051120.0560.050mg/KgChloroethane 33-149 6.2 20
0.052 1041080.0530.050mg/KgChloroform 73-127 3.0 20
0.045 91.297.00.0480.050mg/KgChloromethane 45-143 6.1 20
0.047 95.698.40.0490.050mg/Kg2-Chlorotoluene 67-124 2.8 20
0.047 95.898.40.0490.050mg/Kg4-Chlorotoluene 71-126 2.6 20
0.058 1161170.0580.050mg/KgDi-Isopropyl Ether (DIPE)59-159 1.1 20
0.047 94.490.00.0450.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 4.7 20
0.049 98.898.60.0490.050mg/Kg1,2-Dibromoethane 70-132 0.2 20
0.053 1081090.0540.050mg/KgDibromomethane 74-133 0.9 20
0.048 96.296.80.0480.050mg/Kg1,2-Dichlorobenzene 72-123 0.6 20
0.048 96.499.00.0490.050mg/Kg1,3-Dichlorobenzene 71-120 2.6 20
0.048 96.098.40.0490.050mg/Kg1,4-Dichlorobenzene 71-123 2.4 20
Page 12 of 19Date:07/20/2022 04:15 PM
Page 41 of 50
Quality Control Data
22-189-0051Report No:
Project Description:
Client ID:Geological Resources, Inc.
Flash Market #370
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V21180QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V21179
LCS-V21179 LCSD-V21179Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.040 81.084.20.0420.050mg/KgDichlorodifluoromethane 26-146 3.8 20
0.055 1101130.0560.050mg/Kg1,1-Dichloroethane 74-127 2.5 20
0.055 1111110.0550.050mg/Kg1,2-Dichloroethane 68-128 0.3 20
0.054 1081130.0560.050mg/Kg1,1-Dichloroethene 67-149 4.5 20
0.055 1111150.0570.050mg/Kgcis-1,2-Dichloroethene 76-134 3.1 20
0.055 1101150.0570.050mg/Kgtrans-1,2-Dichloroethene 73-132 4.6 20
0.055 1101120.0550.050mg/Kg1,2-Dichloropropane 73-130 1.2 20
0.050 1011020.0510.050mg/Kg1,3-Dichloropropane 75-124 0.9 20
0.053 1061110.0550.050mg/Kg2,2-Dichloropropane 50-142 4.5 20
0.052 1041140.0560.050mg/Kg1,1-Dichloropropene 71-130 8.6 20
0.054 1091110.0550.050mg/Kgcis-1,3-Dichloropropene 71-125 1.6 20
0.054 1101110.0550.050mg/Kgtrans-1,3-Dichloropropene 68-123 1.6 20
0.048 96.61010.0500.050mg/KgEthylbenzene 74-128 4.0 20
0.113 1131120.1120.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 0.8 20
0.046 92.094.40.0470.050mg/KgHexachlorobutadiene 64-125 2.5 20
0.053 1061160.0570.050mg/Kgn-Hexane 70-130 8.8 20
0.051 1031030.0510.050mg/Kg2-Hexanone 61-157 0.3 20
0.043 87.892.20.0460.050mg/KgIsopropylbenzene 68-126 4.8 20
0.047 95.098.20.0490.050mg/Kg4-Isopropyl toluene 68-129 3.3 20
0.053 1081060.0520.050mg/KgMethyl Ethyl Ketone (MEK)63-149 1.8 20
0.052 1061060.0530.050mg/KgMethyl tert-butyl ether (MTBE)70-130 0.5 20
0.058 1161150.0570.050mg/Kg4-Methyl-2-Pentanone 57-162 1.2 20
0.055 1111130.0560.050mg/KgMethylene Chloride 74-129 1.7 20
0.047 94.291.00.0450.050mg/KgNaphthalene 57-157 3.4 20
0.048 97.01000.0500.050mg/Kgn-Propylbenzene 67-130 3.4 20
0.049 99.41020.0500.050mg/KgStyrene 77-121 2.3 20
Page 13 of 19Date:07/20/2022 04:15 PM
Page 42 of 50
Quality Control Data
22-189-0051Report No:
Project Description:
Client ID:Geological Resources, Inc.
Flash Market #370
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V21180QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V21179
LCS-V21179 LCSD-V21179Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.050 1001000.0500.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 0.3 20
0.047 94.895.00.0470.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 0.2 20
0.052 1051110.0550.050mg/KgTetrachloroethene 68-130 5.1 20
0.052 1051090.0540.050mg/KgToluene 71-129 4.1 20
0.048 96.494.20.0470.050mg/Kg1,2,3-Trichlorobenzene 68-130 2.3 20
0.048 97.298.20.0490.050mg/Kg1,2,4-Trichlorobenzene 66-125 1.0 20
0.051 1021070.0530.050mg/Kg1,1,1-Trichloroethane 67-131 4.0 20
0.047 94.295.80.0470.050mg/Kg1,1,2-Trichloroethane 70-133 1.6 20
0.053 1071110.0550.050mg/KgTrichloroethene 75-133 3.8 20
0.053 1061140.0560.050mg/KgTrichlorofluoromethane 44-146 7.0 20
0.048 97.695.60.0470.050mg/Kg1,2,3-Trichloropropane 60-137 2.0 20
0.048 96.098.60.0490.050mg/Kg1,2,4-Trimethylbenzene 69-129 2.6 20
0.047 94.498.60.0490.050mg/Kg1,3,5-Trimethylbenzene 69-128 4.3 20
0.047 95.093.80.0460.050mg/KgVinyl Acetate 60-140 1.2 20
0.050 1011060.0530.050mg/KgVinyl Chloride 48-147 5.2 20
0.047 95.499.60.0490.050mg/Kgo-Xylene 74-126 4.3 20
0.095 95.599.20.0990.100mg/Kgm,p-Xylene 75-124 3.8 20
99.898.24-Bromofluorobenzene (S)70-130
103103Dibromofluoromethane (S)84-123
95.096.4Toluene-d8 (S)76-129
Page 14 of 19Date:07/20/2022 04:15 PM
Page 43 of 50
Quality Control Data
22-189-0051Report No:
Project Description:
Client ID:Geological Resources, Inc.
Flash Market #370
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V21288QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V21287
Associated Lab Samples: 93943
LRB-V21287 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/14/22 11:490.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
07/14/22 11:494-Bromofluorobenzene (S)101 70-130
07/14/22 11:49Dibromofluoromethane (S)101 70-130
07/14/22 11:49Toluene-d8 (S)94.6 76-129
LCS-V21287 LCSD-V21287Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.049 99.499.00.0490.050mg/KgMethyl tert-butyl ether (MTBE)70-130 0.4 20
98.698.44-Bromofluorobenzene (S)70-130
105103Dibromofluoromethane (S)70-130
95.094.8Toluene-d8 (S)76-129
Page 15 of 19Date:07/20/2022 04:15 PM
Page 44 of 50
Quality Control Data
22-189-0051Report No:
Project Description:
Client ID:Geological Resources, Inc.
Flash Market #370
QC Prep Batch Method:
EDB and DBCP by Microextraction GC/ECD
EPA-504.1
V21440QC Analytical Batch(es):
Analysis Method:
Analysis Description:
EPA-504.1(PREP)
QC Prep:V21417
Associated Lab Samples: 93939
LRB-V21417 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
07/18/22 12:570.02000.00330<0.00330µg/L1,2-Dibromoethane
LCS-V21417 LCSD-V21417Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.277 1111070.2670.250µg/L1,2-Dibromoethane 70-130 3.6 20.0
V 93965-DUP-V21417Duplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 07/18/22 15:340.0<0.0210< 0.0210µg/L1,2-Dibromoethane
V 93939-MS-V21417Matrix Spike
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
0.255 95.80.266< 0.00351µg/L1,2-Dibromoethane 70-130
Page 16 of 19Date:07/20/2022 04:15 PM
Page 45 of 50
Quality Control Data
22-189-0051Report No:
Project Description:
Client ID:Geological Resources, Inc.
Flash Market #370
QC Prep Batch Method:
Massachusetts VPH
MADEP-VPH
V21223QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAVPH (Prep)
QC Prep:V21222
Associated Lab Samples: 93940, 93941, 93943
LRB-V21222 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/13/22 14:438.001.22<1.22mg/KgAliphatic C5-C8
07/13/22 14:438.004.56<4.56mg/KgAliphatic C9-C12
07/13/22 14:438.000.624<0.624mg/KgAromatic C9-C10
07/13/22 14:432,5-Dibromotoluene (FID) (S)100 70-130
07/13/22 14:432,5-Dibromotoluene (PID) (S)84.4 70-130
LCS-V21222 LCSD-V21222Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
36.2 11311436.632.0mg/KgAliphatic C5-C8 70-130 1.0 50
38.6 12111837.932.0mg/KgAliphatic C9-C12 70-130 1.8 50
12.6 11811912.710.7mg/KgAromatic C9-C10 70-130 0.7 50
77.390.72,5-Dibromotoluene (FID) (S)70-130
76.182.82,5-Dibromotoluene (PID) (S)70-130
Page 17 of 19Date:07/20/2022 04:15 PM
Page 46 of 50
Quality Control Data
22-189-0051Report No:
Project Description:
Client ID:Geological Resources, Inc.
Flash Market #370
QC Prep Batch Method:
Massachusetts VPH
MADEP-VPH
V21308QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAVPH (Prep)
QC Prep:V21307
Associated Lab Samples: 93939
LRB-V21307 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/14/22 18:3550.011.5<11.5µg/LAliphatic C5-C8
07/14/22 18:3550.025.8<25.8µg/LAliphatic C9-C12
07/14/22 18:3550.04.02<4.02µg/LAromatic C9-C10
07/14/22 18:352,5-Dibromotoluene (FID) (S)95.4 70-130
07/14/22 18:352,5-Dibromotoluene (PID) (S)91.0 70-130
LCS-V21307 LCSD-V21307Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
294 98.096.0288300µg/LAliphatic C5-C8 70-130 2.0 50.0
318 106106318300µg/LAliphatic C9-C12 70-130 0.0 50.0
102 102105105100µg/LAromatic C9-C10 70-130 2.8 50.0
79.979.32,5-Dibromotoluene (FID) (S)70-130
77.577.82,5-Dibromotoluene (PID) (S)70-130
Page 18 of 19Date:07/20/2022 04:15 PM
Page 47 of 50
Quality Control Data
22-189-0051Report No:
Project Description:
Client ID:Geological Resources, Inc.
Flash Market #370
Dry Weight Determination
SW-DRYWT
V21320QC Analytical Batch:
Analysis Method:
Analysis Description:
V 93768-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 07/15/22 10:330.920.921.1%Moisture
V 94001-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 07/15/22 10:330.423.924.0%Moisture
Page 19 of 19Date:07/20/2022 04:15 PM
Page 48 of 50
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:22-189-0051
Geological Resources, Inc.
00087
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 1.3
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
ü
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Sample SP-2-2 missing jar for % solids. Results can not be reported as dry
weight.
Signature:Adam Crouch Date & Time:07/08/2022 18:43:37
Special precautions or instructions included?
Comments:
Page 49 of 50
Page 50 of 50