RA-3823_23187_CA_HRE_20210526_Buy Quick Bahama April 2021 Limited Supply Well Monitoring Event

East Coast Environmental, P.A.
3815 Junction Boulevard Raleigh, NC 27603
[phone]
Eastcoastenv.com

May 26, 2021

Mr. Craig Mcintosh
NC-DEQ-UST Section
Raleigh Regional Office
1628 Mail Service Center
Raleigh, NC 27699-1628

Re: Buy Quick Food Mart - Bahama (Site)
1502 Bahama Road, Bahama, Durham County, North Carolina (WSW-16)
NCDENR-Incident # 23187

Dear Mr. Mcintosh,

Please find attached the analytical results for supply well samples collected from the above listed location
on April 27, 2021. The results for the unfiltered sample collected before the first inline filter showed
MTBE at 1,400-ug/l and IPE at 110-ug/l but no detections in the sample collected between the first and
second in-line carbon filters during this most recent sampling event which indicates no breakthrough after
the first in-line carbon filter.

As stated in our previous monitoring report from August 2020 we now have had sixteen monitoring events
dating back to August 2013 with no detections in samples collected from supply wells WSW-18 and
WSW-25. We believe that based on these historical results the sampling schedule for these two wells
should be dropped back to annual sampling. Your input into this request would be greatly appreciated.
Should you have any questions, or require additional information, please feel free to contact me at your
earliest opportunity.

Finally, we are scheduled to collected samples from 1502 Bahama Road as well as the remaining two
water supply wells during August 2021.

Respectfully,
East Coast Environmental, P.A.
Thomas R. Will, L.G. # 1164
President

102-A Woodwinds Industrial Court
Cary NC, 27511
919.467.3090 919.467.3515Phone:FAX:[TOC_1]ENCO Laboratories, Inc.[TOC]
ENCO Workorder(s): CE06254
Raleigh, NC 27603
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Enclosure(s)
Project Number: 1502 BAHAMA, Project Name/Desc: Buy Quick Food Mart
Attn: Tom Will
East Coast Environmental (EA030)
3815 Junction Blvd.
Bill Scott
Project Manager
Thursday, May 13, 2021
RE: Laboratory Results for
Dear Tom Will,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Thursday, April 29, 2021.
Enclosure(s)
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 1 of 27Page 1 of 27
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SAMPLE SUMMARY/LABORATORY CHRONICLE [TOC_1]Sample Chronical[TOC]
BEFORE FILTER CE06254-01 Sampled:04/27/21 10:35 Received:04/29/21 08:00Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)Preparation
SM 6200B-2011 05/11/21 05/07/21 12:27 05/07/21 17:46EPA 5030B_MS
BEFORE FILTER CE06254-01RE2 Sampled:04/27/21 10:35 Received:04/29/21 08:00Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)Preparation
SM 6200B-2011 05/11/21 05/10/21 15:13 05/10/21 18:21EPA 5030B_MS
AFTER FILTER CE06254-02 Sampled:04/27/21 11:00 Received:04/29/21 08:00Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)Preparation
SM 6200B-2011 05/11/21 05/07/21 12:27 05/07/21 18:14EPA 5030B_MS
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 2 of 27Page 2 of 27
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SAMPLE DETECTION SUMMARY [TOC_1]Detection Summary[TOC]
Lab ID:Client ID:BEFORE FILTER CE06254-01
Analyte MethodUnitsPQLResultsFlag NotesMDL
110 1.0 ug/L SM 6200B-2011 Isopropyl Ether 0.21
Lab ID:Client ID:BEFORE FILTER CE06254-01RE2
Analyte MethodUnitsPQLResultsFlag NotesMDL
1400 10 ug/L SM 6200B-2011D Methyl-tert-Butyl Ether 1.2
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 3 of 27Page 3 of 27
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ANALYTICAL RESULTS
[TOC_1]Analytical Results[TOC]
BEFORE FILTERDescription:Lab Sample ID:CE06254-01 04/29/21 08:00Received:
CE06254Work Order:04/27/21 10:35Sampled:WaterMatrix:
Tom WillSampled By:Project:Buy Quick Food Mart
[TOC_2]BEFORE FILTER[TOC]
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-2011 05/07/21 17:461,1,1,2-Tetrachloroethane [630-20-6]^0.091 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:461,1,1-Trichloroethane [71-55-6]^0.15 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:461,1,2,2-Tetrachloroethane [79-34-5]^0.085 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:461,1,2-Trichloroethane [79-00-5]^0.068 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:461,1-Dichloroethane [75-34-3]^0.050 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:461,1-Dichloroethene [75-35-4]^0.15 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:461,1-Dichloropropene [563-58-6]^0.063 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:461,2,3-Trichlorobenzene [87-61-6]^0.25 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:461,2,3-Trichloropropane [96-18-4]^0.15 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:461,2,4-Trichlorobenzene [120-82-1]^0.097 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:461,2,4-Trimethylbenzene [95-63-6]^0.067 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:461,2-Dibromo-3-chloropropane [96-12-8]^0.48 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:461,2-Dibromoethane [106-93-4]^0.42 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:461,2-Dichlorobenzene [95-50-1]^0.052 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:461,2-Dichloroethane [107-06-2]^0.082 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:461,2-Dichloropropane [78-87-5]^0.098 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:461,3,5-Trimethylbenzene [108-67-8]^0.10 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:461,3-Dichlorobenzene [541-73-1]^0.092 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:461,3-Dichloropropane [142-28-9]^0.15 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:461,4-Dichlorobenzene [106-46-7]^0.10 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:462,2-Dichloropropane [594-20-7]^0.12 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:462-Chlorotoluene [95-49-8]^0.10 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:464-Chlorotoluene [106-43-4]^0.10 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:464-Isopropyltoluene [99-87-6]^0.066 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:46Benzene [71-43-2]^0.050 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:46Bromobenzene [108-86-1]^0.13 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:46Bromochloromethane [74-97-5]^0.11 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:46Bromodichloromethane [75-27-4]^0.10 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:46Bromoform [75-25-2]^0.20 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:46Bromomethane [74-83-9]^0.28 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:46Carbon Tetrachloride [56-23-5]^0.082 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:46Chlorobenzene [108-90-7]^0.069 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:46Chloroethane [75-00-3]^0.18 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:46Chloroform [67-66-3]^0.083 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:46Chloromethane [74-87-3]^0.050 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:46cis-1,2-Dichloroethene [156-59-2]^0.075 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:46cis-1,3-Dichloropropene [10061-01-5]^0.073 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:46Dibromochloromethane [124-48-1]^0.067 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:46Dibromomethane [74-95-3]^0.13 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:46Dichlorodifluoromethane [75-71-8]^0.091 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:46Ethanol [64-17-5]^26 RKY1E07018100ND 1
ug/L SM 6200B-2011 05/07/21 17:46Ethylbenzene [100-41-4]^0.10 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:46Freon 113 [76-13-1]^0.35 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:46Hexachlorobutadiene [87-68-3]^0.15 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:46Isopropyl Ether [108-20-3]^0.21 RKY1E070181.0110 1
ug/L SM 6200B-2011 05/07/21 17:46Isopropylbenzene [98-82-8]^0.13 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:46m,p-Xylenes [108-38-3/106-42-3]^0.18 RKY1E070182.0ND 1
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 4 of 27Page 4 of 27
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ANALYTICAL RESULTS
BEFORE FILTERDescription:Lab Sample ID:CE06254-01 04/29/21 08:00Received:
CE06254Work Order:04/27/21 10:35Sampled:WaterMatrix:
Tom WillSampled By:Project:Buy Quick Food Mart
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-2011 05/07/21 17:46Methylene Chloride [75-09-2]^0.070 RKY1E070182.0ND 1
ug/L SM 6200B-2011 05/10/21 18:21Methyl-tert-Butyl Ether [1634-04-4]^1.2 RKY1E10018101400D 10
ug/L SM 6200B-2011 05/07/21 17:46Naphthalene [91-20-3]^0.086 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:46n-Butyl Benzene [104-51-8]^0.074 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:46n-Propyl Benzene [103-65-1]^0.073 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:46o-Xylene [95-47-6]^0.088 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:46sec-Butylbenzene [135-98-8]^0.053 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:46Styrene [100-42-5]^0.082 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:46tert-Butylbenzene [98-06-6]^0.094 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:46Tetrachloroethene [127-18-4]^0.099 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:46Toluene [108-88-3]^0.053 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:46trans-1,2-Dichloroethene [156-60-5]^0.11 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:46trans-1,3-Dichloropropene [10061-02-6]^0.080 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:46Trichloroethene [79-01-6]^0.13 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:46Trichlorofluoromethane [75-69-4]^0.15 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:46Vinyl chloride [75-01-4]^0.083 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 17:46Xylenes (Total) [1330-20-7]^0.22 RKY1E070181.0ND 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 70-13098 %RKYSM 6200B-2011 05/07/21 17:461E070184950.0 1
4-Bromofluorobenzene 70-130106 %RKYSM 6200B-2011 05/10/21 18:211E100185350.0 1
Dibromofluoromethane 70-13095 %RKYSM 6200B-2011 05/07/21 17:461E070184750.0 1
Dibromofluoromethane 70-130102 %RKYSM 6200B-2011 05/10/21 18:211E100185150.0 1
Toluene-d8 70-130100 %RKYSM 6200B-2011 05/07/21 17:461E070185050.0 1
Toluene-d8 70-130103 %RKYSM 6200B-2011 05/10/21 18:211E100185150.0 1
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 5 of 27Page 5 of 27
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ANALYTICAL RESULTS
AFTER FILTERDescription:Lab Sample ID:CE06254-02 04/29/21 08:00Received:
CE06254Work Order:04/27/21 11:00Sampled:WaterMatrix:
Tom WillSampled By:Project:Buy Quick Food Mart
[TOC_2]AFTER FILTER[TOC]
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-2011 05/07/21 18:141,1,1,2-Tetrachloroethane [630-20-6]^0.091 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:141,1,1-Trichloroethane [71-55-6]^0.15 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:141,1,2,2-Tetrachloroethane [79-34-5]^0.085 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:141,1,2-Trichloroethane [79-00-5]^0.068 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:141,1-Dichloroethane [75-34-3]^0.050 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:141,1-Dichloroethene [75-35-4]^0.15 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:141,1-Dichloropropene [563-58-6]^0.063 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:141,2,3-Trichlorobenzene [87-61-6]^0.25 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:141,2,3-Trichloropropane [96-18-4]^0.15 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:141,2,4-Trichlorobenzene [120-82-1]^0.097 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:141,2,4-Trimethylbenzene [95-63-6]^0.067 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:141,2-Dibromo-3-chloropropane [96-12-8]^0.48 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:141,2-Dibromoethane [106-93-4]^0.42 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:141,2-Dichlorobenzene [95-50-1]^0.052 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:141,2-Dichloroethane [107-06-2]^0.082 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:141,2-Dichloropropane [78-87-5]^0.098 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:141,3,5-Trimethylbenzene [108-67-8]^0.10 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:141,3-Dichlorobenzene [541-73-1]^0.092 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:141,3-Dichloropropane [142-28-9]^0.15 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:141,4-Dichlorobenzene [106-46-7]^0.10 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:142,2-Dichloropropane [594-20-7]^0.12 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:142-Chlorotoluene [95-49-8]^0.10 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:144-Chlorotoluene [106-43-4]^0.10 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:144-Isopropyltoluene [99-87-6]^0.066 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:14Benzene [71-43-2]^0.050 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:14Bromobenzene [108-86-1]^0.13 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:14Bromochloromethane [74-97-5]^0.11 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:14Bromodichloromethane [75-27-4]^0.10 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:14Bromoform [75-25-2]^0.20 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:14Bromomethane [74-83-9]^0.28 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:14Carbon Tetrachloride [56-23-5]^0.082 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:14Chlorobenzene [108-90-7]^0.069 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:14Chloroethane [75-00-3]^0.18 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:14Chloroform [67-66-3]^0.083 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:14Chloromethane [74-87-3]^0.050 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:14cis-1,2-Dichloroethene [156-59-2]^0.075 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:14cis-1,3-Dichloropropene [10061-01-5]^0.073 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:14Dibromochloromethane [124-48-1]^0.067 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:14Dibromomethane [74-95-3]^0.13 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:14Dichlorodifluoromethane [75-71-8]^0.091 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:14Ethanol [64-17-5]^26 RKY1E07018100ND 1
ug/L SM 6200B-2011 05/07/21 18:14Ethylbenzene [100-41-4]^0.10 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:14Freon 113 [76-13-1]^0.35 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:14Hexachlorobutadiene [87-68-3]^0.15 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:14Isopropyl Ether [108-20-3]^0.21 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:14Isopropylbenzene [98-82-8]^0.13 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:14m,p-Xylenes [108-38-3/106-42-3]^0.18 RKY1E070182.0ND 1
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 6 of 27Page 6 of 27
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ANALYTICAL RESULTS
AFTER FILTERDescription:Lab Sample ID:CE06254-02 04/29/21 08:00Received:
CE06254Work Order:04/27/21 11:00Sampled:WaterMatrix:
Tom WillSampled By:Project:Buy Quick Food Mart
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
NotesFlagPQLBatchByAnalyzedMethodMDLResultsUnitsDFAnalyte [CAS Number]
ug/L SM 6200B-2011 05/07/21 18:14Methylene Chloride [75-09-2]^0.070 RKY1E070182.0ND 1
ug/L SM 6200B-2011 05/07/21 18:14Methyl-tert-Butyl Ether [1634-04-4]^0.12 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:14Naphthalene [91-20-3]^0.086 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:14n-Butyl Benzene [104-51-8]^0.074 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:14n-Propyl Benzene [103-65-1]^0.073 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:14o-Xylene [95-47-6]^0.088 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:14sec-Butylbenzene [135-98-8]^0.053 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:14Styrene [100-42-5]^0.082 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:14tert-Butylbenzene [98-06-6]^0.094 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:14Tetrachloroethene [127-18-4]^0.099 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:14Toluene [108-88-3]^0.053 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:14trans-1,2-Dichloroethene [156-60-5]^0.11 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:14trans-1,3-Dichloropropene [10061-02-6]^0.080 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:14Trichloroethene [79-01-6]^0.13 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:14Trichlorofluoromethane [75-69-4]^0.15 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:14Vinyl chloride [75-01-4]^0.083 RKY1E070181.0ND 1
ug/L SM 6200B-2011 05/07/21 18:14Xylenes (Total) [1330-20-7]^0.22 RKY1E070181.0ND 1
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 70-130105 %RKYSM 6200B-2011 05/07/21 18:141E070185250.0 1
Dibromofluoromethane 70-13095 %RKYSM 6200B-2011 05/07/21 18:141E070184850.0 1
Toluene-d8 70-130107 %RKYSM 6200B-2011 05/07/21 18:141E070185450.0 1
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 7 of 27Page 7 of 27
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QUALITY CONTROL DATA [TOC_1]QC Data[TOC]
Volatile Organic Compounds by GCMS - Quality Control
Batch 1E07018 - EPA 5030B_MS
Prepared: 05/07/2021 12:27 Analyzed: 05/07/2021 15:54Blank (1E07018-BLK1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.00.091 U 1,1,1,2-Tetrachloroethane
ug/L1.00.15 U 1,1,1-Trichloroethane
ug/L1.00.085 U 1,1,2,2-Tetrachloroethane
ug/L1.00.068 U 1,1,2-Trichloroethane
ug/L1.00.050 U 1,1-Dichloroethane
ug/L1.00.15 U 1,1-Dichloroethene
ug/L1.00.063 U 1,1-Dichloropropene
ug/L1.00.25 U 1,2,3-Trichlorobenzene
ug/L1.00.15 U 1,2,3-Trichloropropane
ug/L1.00.097 U 1,2,4-Trichlorobenzene
ug/L1.00.067 U 1,2,4-Trimethylbenzene
ug/L1.00.48 U 1,2-Dibromo-3-chloropropane
ug/L1.00.42 U 1,2-Dibromoethane
ug/L1.00.052 U 1,2-Dichlorobenzene
ug/L1.00.082 U 1,2-Dichloroethane
ug/L1.00.098 U 1,2-Dichloropropane
ug/L1.00.10 U 1,3,5-Trimethylbenzene
ug/L1.00.092 U 1,3-Dichlorobenzene
ug/L1.00.15 U 1,3-Dichloropropane
ug/L1.00.10 U 1,4-Dichlorobenzene
ug/L1.00.12 U 2,2-Dichloropropane
ug/L1.00.10 U 2-Chlorotoluene
ug/L1.00.10 U 4-Chlorotoluene
ug/L1.00.066 U 4-Isopropyltoluene
ug/L1.00.050 U Benzene
ug/L1.00.13 U Bromobenzene
ug/L1.00.11 U Bromochloromethane
ug/L1.00.10 U Bromodichloromethane
ug/L1.00.20 U Bromoform
ug/L1.00.28 U Bromomethane
ug/L1.00.082 U Carbon Tetrachloride
ug/L1.00.069 U Chlorobenzene
ug/L1.00.18 U Chloroethane
ug/L1.00.083 U Chloroform
ug/L1.00.050 U Chloromethane
ug/L1.00.075 U cis-1,2-Dichloroethene
ug/L1.00.073 U cis-1,3-Dichloropropene
ug/L1.00.067 U Dibromochloromethane
ug/L1.00.13 U Dibromomethane
ug/L1.00.091 U Dichlorodifluoromethane
ug/L10026U Ethanol
ug/L1.00.10 U Ethylbenzene
ug/L1.00.35 U Freon 113
ug/L1.00.15 U Hexachlorobutadiene
ug/L1.00.21 U Isopropyl Ether
ug/L1.00.13 U Isopropylbenzene
ug/L2.00.18 U m,p-Xylenes
ug/L2.00.070 U Methylene Chloride
ug/L1.00.12 U Methyl-tert-Butyl Ether
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 8 of 27Page 8 of 27
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 1E07018 - EPA 5030B_MS - Continued
Prepared: 05/07/2021 12:27 Analyzed: 05/07/2021 15:54Blank (1E07018-BLK1) Continued
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.00.086 U Naphthalene
ug/L1.00.074 U n-Butyl Benzene
ug/L1.00.073 U n-Propyl Benzene
ug/L1.00.088 U o-Xylene
ug/L1.00.053 U sec-Butylbenzene
ug/L1.00.082 U Styrene
ug/L1.00.094 U tert-Butylbenzene
ug/L1.00.099 U Tetrachloroethene
ug/L1.00.053 U Toluene
ug/L1.00.11 U trans-1,2-Dichloroethene
ug/L1.00.080 U trans-1,3-Dichloropropene
ug/L1.00.13 U Trichloroethene
ug/L1.00.15 U Trichlorofluoromethane
ug/L1.00.083 U Vinyl chloride
ug/L1.00.22 U Xylenes (Total)
ug/L 50.0 70-1304-Bromofluorobenzene 10351
ug/L 50.0 70-130Dibromofluoromethane9347
ug/L 50.0 70-130Toluene-d8 10351
Prepared: 05/07/2021 12:27 Analyzed: 05/07/2021 14:01LCS (1E07018-BS1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 70-1309820 1,1,1,2-Tetrachloroethane
ug/L1.0 20.0 70-13010721 1,1,1-Trichloroethane
ug/L1.0 20.0 70-13010621 1,1,2,2-Tetrachloroethane
ug/L1.0 20.0 70-13011222 1,1,2-Trichloroethane
ug/L1.0 20.0 70-13011824 1,1-Dichloroethane
ug/L1.0 20.0 70-13010521 1,1-Dichloroethene
ug/L1.0 20.0 70-13011022 1,1-Dichloropropene
ug/L1.0 20.0 70-1309820 1,2,3-Trichlorobenzene
ug/L1.0 20.0 70-1309419 1,2,3-Trichloropropane
ug/L1.0 20.0 70-1309519 1,2,4-Trichlorobenzene
ug/L1.0 20.0 70-13010321 1,2,4-Trimethylbenzene
ug/L1.0 20.0 70-1309018 1,2-Dibromo-3-chloropropane
ug/L1.0 20.0 70-1309719 1,2-Dibromoethane
ug/L1.0 20.0 70-13010421 1,2-Dichlorobenzene
ug/L1.0 20.0 70-13010321 1,2-Dichloroethane
ug/L1.0 20.0 70-13011423 1,2-Dichloropropane
ug/L1.0 20.0 70-1309920 1,3,5-Trimethylbenzene
ug/L1.0 20.0 70-13010421 1,3-Dichlorobenzene
ug/L1.0 20.0 70-13010321 1,3-Dichloropropane
ug/L1.0 20.0 70-13010922 1,4-Dichlorobenzene
ug/L1.0 20.0 70-13012625 2,2-Dichloropropane
ug/L1.0 20.0 70-13010421 2-Chlorotoluene
ug/L1.0 20.0 70-13010321 4-Chlorotoluene
ug/L1.0 20.0 70-13010321 4-Isopropyltoluene
ug/L1.0 20.0 70-13011824 Benzene
ug/L1.0 20.0 70-13010220 Bromobenzene
ug/L1.0 20.0 70-13011523 Bromochloromethane
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 9 of 27Page 9 of 27
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 1E07018 - EPA 5030B_MS - Continued
Prepared: 05/07/2021 12:27 Analyzed: 05/07/2021 14:01LCS (1E07018-BS1) Continued
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 70-13011022 Bromodichloromethane
ug/L1.0 20.0 70-13011623 Bromoform
ug/L1.0 20.0 60-14012024 Bromomethane
ug/L1.0 20.0 70-13011222 Carbon Tetrachloride
ug/L1.0 20.0 70-13011022 Chlorobenzene
ug/L1.0 20.0 60-14012725 Chloroethane
ug/L1.0 20.0 70-13010721 Chloroform
ug/L1.0 20.0 60-14011122 Chloromethane
ug/L1.0 20.0 70-1309920 cis-1,2-Dichloroethene
ug/L1.0 20.0 70-13010721 cis-1,3-Dichloropropene
ug/L1.0 20.0 70-13010721 Dibromochloromethane
ug/L1.0 20.0 70-13010521 Dibromomethane
ug/L1.0 20.0 60-14011022 Dichlorodifluoromethane
ug/L100 100 0-200142140 Ethanol
ug/L1.0 20.0 70-13010521 Ethylbenzene
ug/L1.0 40.0 70-13010944 Freon 113
ug/L1.0 20.0 70-13010220 Hexachlorobutadiene
ug/L1.0 20.0 70-13011022 Isopropyl Ether
ug/L1.0 20.0 70-13011122 Isopropylbenzene
ug/L2.0 40.0 70-13011044 m,p-Xylenes
ug/L2.0 20.0 70-13011623 Methylene Chloride
ug/L1.0 20.0 70-13010721 Methyl-tert-Butyl Ether
ug/L1.0 20.0 70-1309419 Naphthalene
ug/L1.0 20.0 70-13010922 n-Butyl Benzene
ug/L1.0 20.0 70-13011523 n-Propyl Benzene
ug/L1.0 20.0 70-13010521 o-Xylene
ug/L1.0 20.0 70-13011022 sec-Butylbenzene
ug/L1.0 20.0 70-13010321 Styrene
ug/L1.0 20.0 70-13010421 tert-Butylbenzene
ug/L1.0 20.0 70-13011423 Tetrachloroethene
ug/L1.0 20.0 70-13010721 Toluene
ug/L1.0 20.0 70-13011222 trans-1,2-Dichloroethene
ug/L1.0 20.0 70-13011022 trans-1,3-Dichloropropene
ug/L1.0 20.0 70-13011423 Trichloroethene
ug/L1.0 20.0 60-14010321 Trichlorofluoromethane
ug/L1.0 20.0 60-14012224 Vinyl chloride
ug/L1.0 60.0 70-13010965 Xylenes (Total)
ug/L 50.0 70-1304-Bromofluorobenzene 10151
ug/L 50.0 70-130Dibromofluoromethane9547
ug/L 50.0 70-130Toluene-d8 10452
Prepared: 05/07/2021 12:27 Analyzed: 05/07/2021 14:30Matrix Spike (1E07018-MS1)
Source: CE06773-05
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 70-1301090.091 U22 1,1,1,2-Tetrachloroethane
ug/L1.0 20.0 70-1301060.15 U21 1,1,1-Trichloroethane
ug/L1.0 20.0 70-1301090.085 U22 1,1,2,2-Tetrachloroethane
ug/L1.0 20.0 70-1301190.068 U24 1,1,2-Trichloroethane
ug/L1.0 20.0 70-1301220.050 U24 1,1-Dichloroethane
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 10 of 27Page 10 of 27
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 1E07018 - EPA 5030B_MS - Continued
Prepared: 05/07/2021 12:27 Analyzed: 05/07/2021 14:30Matrix Spike (1E07018-MS1) Continued
Source: CE06773-05
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 70-1301100.15 U22 1,1-Dichloroethene
ug/L1.0 20.0 70-1301180.063 U24 1,1-Dichloropropene
ug/L1.0 20.0 70-1301040.25 U21 1,2,3-Trichlorobenzene
ug/L1.0 20.0 70-130930.15 U19 1,2,3-Trichloropropane
ug/L1.0 20.0 70-130990.097 U20 1,2,4-Trichlorobenzene
ug/L1.0 20.0 70-1301100.067 U22 1,2,4-Trimethylbenzene
ug/L1.0 20.0 70-130870.48 U17 1,2-Dibromo-3-chloropropane
ug/L1.0 20.0 70-1301020.42 U20 1,2-Dibromoethane
ug/L1.0 20.0 70-1301080.052 U22 1,2-Dichlorobenzene
ug/L1.0 20.0 70-1301050.082 U21 1,2-Dichloroethane
ug/L1.0 20.0 70-1301200.098 U24 1,2-Dichloropropane
ug/L1.0 20.0 70-1301060.10 U21 1,3,5-Trimethylbenzene
ug/L1.0 20.0 70-1301110.092 U22 1,3-Dichlorobenzene
ug/L1.0 20.0 70-1301080.15 U22 1,3-Dichloropropane
ug/L1.0 20.0 70-1301110.10 U22 1,4-Dichlorobenzene
ug/L1.0 20.0 70-1301240.12 U25 2,2-Dichloropropane
ug/L1.0 20.0 70-1301090.10 U22 2-Chlorotoluene
ug/L1.0 20.0 70-1301060.10 U21 4-Chlorotoluene
ug/L1.0 20.0 70-1301140.066 U23 4-Isopropyltoluene
ug/L1.0 20.0 70-1301170.050 U23 Benzene
ug/L1.0 20.0 70-1301140.13 U23 Bromobenzene
ug/L1.0 20.0 70-1301170.11 U23 Bromochloromethane
ug/L1.0 20.0 70-1301160.10 U23 Bromodichloromethane
ug/L1.0 20.0 70-1301140.20 U23 Bromoform
ug/L1.0 20.0 60-1401200.28 U24 Bromomethane
ug/L1.0 20.0 70-1301140.082 U23 Carbon Tetrachloride
ug/L1.0 20.0 70-1301130.069 U23 Chlorobenzene
ug/L1.0 20.0 60-1401200.18 U24 Chloroethane
ug/L1.0 20.0 70-1301160.083 U23 Chloroform
ug/L1.0 20.0 60-1401140.050 U23 Chloromethane
ug/L1.0 20.0 70-1301020.075 U20 cis-1,2-Dichloroethene
ug/L1.0 20.0 70-1301100.073 U22 cis-1,3-Dichloropropene
ug/L1.0 20.0 70-1301120.067 U22 Dibromochloromethane
ug/L1.0 20.0 70-1301100.13 U22 Dibromomethane
ug/L1.0 20.0 60-1401190.091 U24 Dichlorodifluoromethane
ug/L100 100 0-20013826 U140 Ethanol
ug/L1.0 20.0 70-1301120.10 U22 Ethylbenzene
ug/L1.0 40.0 70-1301190.35 U47 Freon 113
ug/L1.0 20.0 70-1301070.15 U21 Hexachlorobutadiene
ug/L1.0 20.0 70-1301190.21 U24 Isopropyl Ether
ug/L1.0 20.0 70-1301180.13 U24 Isopropylbenzene
ug/L2.0 40.0 70-1301190.18 U48 m,p-Xylenes
ug/L2.0 20.0 70-1301180.070 U24 Methylene Chloride
ug/L1.0 20.0 70-1301100.12 U22 Methyl-tert-Butyl Ether
ug/L1.0 20.0 70-130970.086 U19 Naphthalene
ug/L1.0 20.0 70-1301170.074 U23 n-Butyl Benzene
ug/L1.0 20.0 70-1301240.073 U25 n-Propyl Benzene
ug/L1.0 20.0 70-1301120.088 U22 o-Xylene
ug/L1.0 20.0 70-1301210.053 U24 sec-Butylbenzene
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 11 of 27Page 11 of 27
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 1E07018 - EPA 5030B_MS - Continued
Prepared: 05/07/2021 12:27 Analyzed: 05/07/2021 14:30Matrix Spike (1E07018-MS1) Continued
Source: CE06773-05
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 70-1301070.082 U21 Styrene
ug/L1.0 20.0 70-1301100.094 U22 tert-Butylbenzene
ug/L1.0 20.0 70-1301210.099 U24 Tetrachloroethene
ug/L1.0 20.0 70-1301120.053 U22 Toluene
ug/L1.0 20.0 70-1301170.11 U23 trans-1,2-Dichloroethene
ug/L1.0 20.0 70-1301210.080 U24 trans-1,3-Dichloropropene
ug/L1.0 20.0 70-1301170.13 U23 Trichloroethene
ug/L1.0 20.0 60-1401100.15 U22 Trichlorofluoromethane
ug/L1.0 20.0 60-1401270.083 U25 Vinyl chloride
ug/L1.0 60.0 70-1301170.22 U70 Xylenes (Total)
ug/L 50.0 70-1304-Bromofluorobenzene 10754
ug/L 50.0 70-130Dibromofluoromethane9447
ug/L 50.0 70-130Toluene-d8 10351
Prepared: 05/07/2021 12:27 Analyzed: 05/07/2021 14:58Matrix Spike Dup (1E07018-MSD1)
Source: CE06773-05
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 1670-130101 80.091 U20 1,1,1,2-Tetrachloroethane
ug/L1.0 20.0 1870-13098 80.15 U20 1,1,1-Trichloroethane
ug/L1.0 20.0 1670-130109 0.60.085 U22 1,1,2,2-Tetrachloroethane
ug/L1.0 20.0 1870-130116 20.068 U23 1,1,2-Trichloroethane
ug/L1.0 20.0 1970-130111 90.050 U22 1,1-Dichloroethane
ug/L1.0 20.0 2070-130105 50.15 U21 1,1-Dichloroethene
ug/L1.0 20.0 1770-130106 110.063 U21 1,1-Dichloropropene
ug/L1.0 20.0 1770-130100 40.25 U20 1,2,3-Trichlorobenzene
ug/L1.0 20.0 1770-13098 60.15 U20 1,2,3-Trichloropropane
ug/L1.0 20.0 1770-13096 30.097 U19 1,2,4-Trichlorobenzene
ug/L1.0 20.0 1870-130101 80.067 U20 1,2,4-Trimethylbenzene
ug/L1.0 20.0 1870-13088 0.70.48 U18 1,2-Dibromo-3-chloropropane
ug/L1.0 20.0 1570-13098 40.42 U20 1,2-Dibromoethane
ug/L1.0 20.0 1670-130102 60.052 U20 1,2-Dichlorobenzene
ug/L1.0 20.0 1670-130100 50.082 U20 1,2-Dichloroethane
ug/L1.0 20.0 1970-130119 0.20.098 U24 1,2-Dichloropropane
ug/L1.0 20.0 1670-13097 80.10 U19 1,3,5-Trimethylbenzene
ug/L1.0 20.0 1770-130104 70.092 U21 1,3-Dichlorobenzene
ug/L1.0 20.0 1670-130104 40.15 U21 1,3-Dichloropropane
ug/L1.0 20.0 1670-130106 50.10 U21 1,4-Dichlorobenzene
ug/L1.0 20.0 2070-130118 60.12 U24 2,2-Dichloropropane
ug/L1.0 20.0 1670-130101 80.10 U20 2-Chlorotoluene
ug/L1.0 20.0 1670-130103 30.10 U21 4-Chlorotoluene
ug/L1.0 20.0 1770-130102 100.066 U20 4-Isopropyltoluene
ug/L1.0 20.0 1770-130114 30.050 U23 Benzene
ug/L1.0 20.0 1770-130100 130.13 U20 Bromobenzene
ug/L1.0 20.0 1870-130108 70.11 U22 Bromochloromethane
ug/L1.0 20.0 1670-130106 90.10 U21 Bromodichloromethane
ug/L1.0 20.0 4470-130117 20.20 U23 Bromoform
ug/L1.0 20.0 2760-140115 40.28 U23 Bromomethane
ug/L1.0 20.0 1770-130111 30.082 U22 Carbon Tetrachloride
ug/L1.0 20.0 1670-130110 30.069 U22 Chlorobenzene
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 12 of 27Page 12 of 27
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 1E07018 - EPA 5030B_MS - Continued
Prepared: 05/07/2021 12:27 Analyzed: 05/07/2021 14:58Matrix Spike Dup (1E07018-MSD1) Continued
Source: CE06773-05
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 2660-140112 70.18 U22 Chloroethane
ug/L1.0 20.0 1770-130105 90.083 U21 Chloroform
ug/L1.0 20.0 2860-140106 70.050 U21 Chloromethane
ug/L1.0 20.0 1870-13097 50.075 U19 cis-1,2-Dichloroethene
ug/L1.0 20.0 1770-130104 60.073 U21 cis-1,3-Dichloropropene
ug/L1.0 20.0 1670-130109 30.067 U22 Dibromochloromethane
ug/L1.0 20.0 1570-130102 80.13 U20 Dibromomethane
ug/L1.0 20.0 4860-140109 90.091 U22 Dichlorodifluoromethane
ug/L100 100 250-200151 826 U150 Ethanol
ug/L1.0 20.0 1670-130104 70.10 U21 Ethylbenzene
ug/L1.0 40.0 2570-130107 100.35 U43 Freon 113
ug/L1.0 20.0 1970-13097 100.15 U19 Hexachlorobutadiene
ug/L1.0 20.0 3070-130109 90.21 U22 Isopropyl Ether
ug/L1.0 20.0 1670-130110 70.13 U22 Isopropylbenzene
ug/L2.0 40.0 1670-130112 60.18 U45 m,p-Xylenes
ug/L2.0 20.0 1770-130114 40.070 U23 Methylene Chloride
ug/L1.0 20.0 2170-130107 20.12 U21 Methyl-tert-Butyl Ether
ug/L1.0 20.0 1970-13096 0.80.086 U19 Naphthalene
ug/L1.0 20.0 1570-130110 60.074 U22 n-Butyl Benzene
ug/L1.0 20.0 1670-130114 80.073 U23 n-Propyl Benzene
ug/L1.0 20.0 1570-130106 50.088 U21 o-Xylene
ug/L1.0 20.0 1770-130111 90.053 U22 sec-Butylbenzene
ug/L1.0 20.0 2370-130102 50.082 U20 Styrene
ug/L1.0 20.0 2270-130102 70.094 U20 tert-Butylbenzene
ug/L1.0 20.0 2670-130115 50.099 U23 Tetrachloroethene
ug/L1.0 20.0 1770-130109 30.053 U22 Toluene
ug/L1.0 20.0 1970-130113 30.11 U23 trans-1,2-Dichloroethene
ug/L1.0 20.0 1670-130114 60.080 U23 trans-1,3-Dichloropropene
ug/L1.0 20.0 1870-130110 60.13 U22 Trichloroethene
ug/L1.0 20.0 2260-140101 90.15 U20 Trichlorofluoromethane
ug/L1.0 20.0 2760-140116 90.083 U23 Vinyl chloride
ug/L1.0 60.0 1670-130110 60.22 U66 Xylenes (Total)
ug/L 50.0 70-1304-Bromofluorobenzene 10653
ug/L 50.0 70-130Dibromofluoromethane9447
ug/L 50.0 70-130Toluene-d8 10352
Batch 1E08001 - EPA 5030B_MS
Prepared: 05/07/2021 13:00 Analyzed: 05/08/2021 18:28Blank (1E08001-BLK1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.00.091 U 1,1,1,2-Tetrachloroethane
ug/L1.00.15 U 1,1,1-Trichloroethane
ug/L1.00.085 U 1,1,2,2-Tetrachloroethane
ug/L1.00.068 U 1,1,2-Trichloroethane
ug/L1.00.050 U 1,1-Dichloroethane
ug/L1.00.15 U 1,1-Dichloroethene
ug/L1.00.063 U 1,1-Dichloropropene
ug/L1.00.25 U 1,2,3-Trichlorobenzene
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 13 of 27Page 13 of 27
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 1E08001 - EPA 5030B_MS - Continued
Prepared: 05/07/2021 13:00 Analyzed: 05/08/2021 18:28Blank (1E08001-BLK1) Continued
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.00.15 U 1,2,3-Trichloropropane
ug/L1.00.097 U 1,2,4-Trichlorobenzene
ug/L1.00.067 U 1,2,4-Trimethylbenzene
ug/L1.00.48 U 1,2-Dibromo-3-chloropropane
ug/L1.00.42 U 1,2-Dibromoethane
ug/L1.00.052 U 1,2-Dichlorobenzene
ug/L1.00.082 U 1,2-Dichloroethane
ug/L1.00.098 U 1,2-Dichloropropane
ug/L1.00.10 U 1,3,5-Trimethylbenzene
ug/L1.00.092 U 1,3-Dichlorobenzene
ug/L1.00.15 U 1,3-Dichloropropane
ug/L1.00.10 U 1,4-Dichlorobenzene
ug/L1.00.12 U 2,2-Dichloropropane
ug/L1.00.10 U 2-Chlorotoluene
ug/L1.00.10 U 4-Chlorotoluene
ug/L1.00.066 U 4-Isopropyltoluene
ug/L1.00.050 U Benzene
ug/L1.00.13 U Bromobenzene
ug/L1.00.11 U Bromochloromethane
ug/L1.00.10 U Bromodichloromethane
ug/L1.00.20 U Bromoform
ug/L1.00.28 U Bromomethane
ug/L1.00.082 U Carbon Tetrachloride
ug/L1.00.069 U Chlorobenzene
ug/L1.00.18 U Chloroethane
ug/L1.00.083 U Chloroform
ug/L1.00.050 U Chloromethane
ug/L1.00.075 U cis-1,2-Dichloroethene
ug/L1.00.073 U cis-1,3-Dichloropropene
ug/L1.00.067 U Dibromochloromethane
ug/L1.00.13 U Dibromomethane
ug/L1.00.091 U Dichlorodifluoromethane
ug/L10026U Ethanol
ug/L1.00.10 U Ethylbenzene
ug/L1.00.35 U Freon 113
ug/L1.00.15 U Hexachlorobutadiene
ug/L1.00.21 U Isopropyl Ether
ug/L1.00.13 U Isopropylbenzene
ug/L2.00.18 U m,p-Xylenes
ug/L2.00.070 U Methylene Chloride
ug/L1.00.12 U Methyl-tert-Butyl Ether
ug/L1.00.086 U Naphthalene
ug/L1.00.074 U n-Butyl Benzene
ug/L1.00.073 U n-Propyl Benzene
ug/L1.00.088 U o-Xylene
ug/L1.00.053 U sec-Butylbenzene
ug/L1.00.082 U Styrene
ug/L1.00.094 U tert-Butylbenzene
ug/L1.00.099 U Tetrachloroethene
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 14 of 27Page 14 of 27
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 1E08001 - EPA 5030B_MS - Continued
Prepared: 05/07/2021 13:00 Analyzed: 05/08/2021 18:28Blank (1E08001-BLK1) Continued
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.00.053 U Toluene
ug/L1.00.11 U trans-1,2-Dichloroethene
ug/L1.00.080 U trans-1,3-Dichloropropene
ug/L1.00.13 U Trichloroethene
ug/L1.00.15 U Trichlorofluoromethane
ug/L1.00.083 U Vinyl chloride
ug/L1.00.22 U Xylenes (Total)
ug/L 50.0 70-1304-Bromofluorobenzene 11256
ug/L 50.0 70-130Dibromofluoromethane9648
ug/L 50.0 70-130Toluene-d8 10653
Prepared: 05/07/2021 13:00 Analyzed: 05/08/2021 16:36LCS (1E08001-BS1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 70-13010321 1,1,1,2-Tetrachloroethane
ug/L1.0 20.0 70-13011222 1,1,1-Trichloroethane
ug/L1.0 20.0 70-13011122 1,1,2,2-Tetrachloroethane
ug/L1.0 20.0 70-13011924 1,1,2-Trichloroethane
ug/L1.0 20.0 70-13012124 1,1-Dichloroethane
ug/L1.0 20.0 70-13011423 1,1-Dichloroethene
ug/L1.0 20.0 70-13012024 1,1-Dichloropropene
ug/L1.0 20.0 70-1309820 1,2,3-Trichlorobenzene
ug/L1.0 20.0 70-1309820 1,2,3-Trichloropropane
ug/L1.0 20.0 70-1309719 1,2,4-Trichlorobenzene
ug/L1.0 20.0 70-13011423 1,2,4-Trimethylbenzene
ug/L1.0 20.0 70-13010521 1,2-Dibromo-3-chloropropane
ug/L1.0 20.0 70-13010721 1,2-Dibromoethane
ug/L1.0 20.0 70-13010421 1,2-Dichlorobenzene
ug/L1.0 20.0 70-13011623 1,2-Dichloroethane
ug/L1.0 20.0 70-13012325 1,2-Dichloropropane
ug/L1.0 20.0 70-13010721 1,3,5-Trimethylbenzene
ug/L1.0 20.0 70-13010922 1,3-Dichlorobenzene
ug/L1.0 20.0 70-13011423 1,3-Dichloropropane
ug/L1.0 20.0 70-13011122 1,4-Dichlorobenzene
ug/L1.0 20.0 70-13013828 QL-022,2-Dichloropropane
ug/L1.0 20.0 70-13011323 2-Chlorotoluene
ug/L1.0 20.0 70-13011222 4-Chlorotoluene
ug/L1.0 20.0 70-13011022 4-Isopropyltoluene
ug/L1.0 20.0 70-13012024 Benzene
ug/L1.0 20.0 70-13010321 Bromobenzene
ug/L1.0 20.0 70-13010922 Bromochloromethane
ug/L1.0 20.0 70-13011523 Bromodichloromethane
ug/L1.0 20.0 70-13011623 Bromoform
ug/L1.0 20.0 60-1409820 Bromomethane
ug/L1.0 20.0 70-13011924 Carbon Tetrachloride
ug/L1.0 20.0 70-13011022 Chlorobenzene
ug/L1.0 20.0 60-14012926 Chloroethane
ug/L1.0 20.0 70-13011323 Chloroform
ug/L1.0 20.0 60-1409619 Chloromethane
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 15 of 27Page 15 of 27
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 1E08001 - EPA 5030B_MS - Continued
Prepared: 05/07/2021 13:00 Analyzed: 05/08/2021 16:36LCS (1E08001-BS1) Continued
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 70-1309820 cis-1,2-Dichloroethene
ug/L1.0 20.0 70-13011423 cis-1,3-Dichloropropene
ug/L1.0 20.0 70-13011523 Dibromochloromethane
ug/L1.0 20.0 70-13011022 Dibromomethane
ug/L1.0 20.0 60-14010521 Dichlorodifluoromethane
ug/L100 100 0-200160160 Ethanol
ug/L1.0 20.0 70-13011222 Ethylbenzene
ug/L1.0 40.0 70-13011948 Freon 113
ug/L1.0 20.0 70-13010321 Hexachlorobutadiene
ug/L1.0 20.0 70-13012525 Isopropyl Ether
ug/L1.0 20.0 70-13011623 Isopropylbenzene
ug/L2.0 40.0 70-13011847 m,p-Xylenes
ug/L2.0 20.0 70-13011824 Methylene Chloride
ug/L1.0 20.0 70-13012124 Methyl-tert-Butyl Ether
ug/L1.0 20.0 70-13010321 Naphthalene
ug/L1.0 20.0 70-13011824 n-Butyl Benzene
ug/L1.0 20.0 70-13012124 n-Propyl Benzene
ug/L1.0 20.0 70-13011423 o-Xylene
ug/L1.0 20.0 70-13012124 sec-Butylbenzene
ug/L1.0 20.0 70-13010521 Styrene
ug/L1.0 20.0 70-13011222 tert-Butylbenzene
ug/L1.0 20.0 70-13012024 Tetrachloroethene
ug/L1.0 20.0 70-13011423 Toluene
ug/L1.0 20.0 70-13011924 trans-1,2-Dichloroethene
ug/L1.0 20.0 70-13012525 trans-1,3-Dichloropropene
ug/L1.0 20.0 70-13011323 Trichloroethene
ug/L1.0 20.0 60-14011323 Trichlorofluoromethane
ug/L1.0 20.0 60-1408617 Vinyl chloride
ug/L1.0 60.0 70-13011670 Xylenes (Total)
ug/L 50.0 70-1304-Bromofluorobenzene 10754
ug/L 50.0 70-130Dibromofluoromethane9548
ug/L 50.0 70-130Toluene-d8 10352
Prepared: 05/07/2021 13:00 Analyzed: 05/08/2021 17:04Matrix Spike (1E08001-MS1)
Source: CE06773-06
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 70-1301030.091 U21 1,1,1,2-Tetrachloroethane
ug/L1.0 20.0 70-1301100.15 U22 1,1,1-Trichloroethane
ug/L1.0 20.0 70-1301110.085 U22 1,1,2,2-Tetrachloroethane
ug/L1.0 20.0 70-1301130.068 U23 1,1,2-Trichloroethane
ug/L1.0 20.0 70-1301240.050 U25 1,1-Dichloroethane
ug/L1.0 20.0 70-1301150.15 U23 1,1-Dichloroethene
ug/L1.0 20.0 70-1301190.063 U24 1,1-Dichloropropene
ug/L1.0 20.0 70-1301080.25 U22 1,2,3-Trichlorobenzene
ug/L1.0 20.0 70-130960.15 U19 1,2,3-Trichloropropane
ug/L1.0 20.0 70-1301010.097 U20 1,2,4-Trichlorobenzene
ug/L1.0 20.0 70-1301150.067 U23 1,2,4-Trimethylbenzene
ug/L1.0 20.0 70-130980.48 U20 1,2-Dibromo-3-chloropropane
ug/L1.0 20.0 70-1301040.42 U21 1,2-Dibromoethane
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 16 of 27Page 16 of 27
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 1E08001 - EPA 5030B_MS - Continued
Prepared: 05/07/2021 13:00 Analyzed: 05/08/2021 17:04Matrix Spike (1E08001-MS1) Continued
Source: CE06773-06
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 70-1301080.052 U22 1,2-Dichlorobenzene
ug/L1.0 20.0 70-1301140.082 U23 1,2-Dichloroethane
ug/L1.0 20.0 70-1301200.098 U24 1,2-Dichloropropane
ug/L1.0 20.0 70-1301120.10 U22 1,3,5-Trimethylbenzene
ug/L1.0 20.0 70-1301110.092 U22 1,3-Dichlorobenzene
ug/L1.0 20.0 70-1301120.15 U22 1,3-Dichloropropane
ug/L1.0 20.0 70-1301130.10 U23 1,4-Dichlorobenzene
ug/L1.0 20.0 70-1301340.12 U27 QM-072,2-Dichloropropane
ug/L1.0 20.0 70-1301130.10 U23 2-Chlorotoluene
ug/L1.0 20.0 70-1301170.10 U23 4-Chlorotoluene
ug/L1.0 20.0 70-1301140.066 U23 4-Isopropyltoluene
ug/L1.0 20.0 70-1301180.050 U24 Benzene
ug/L1.0 20.0 70-1301010.13 U20 Bromobenzene
ug/L1.0 20.0 70-1301100.11 U22 Bromochloromethane
ug/L1.0 20.0 70-1301160.10 U23 Bromodichloromethane
ug/L1.0 20.0 70-1301190.20 U24 Bromoform
ug/L1.0 20.0 60-140980.28 U20 Bromomethane
ug/L1.0 20.0 70-1301150.082 U23 Carbon Tetrachloride
ug/L1.0 20.0 70-1301110.069 U22 Chlorobenzene
ug/L1.0 20.0 60-1401240.18 U25 Chloroethane
ug/L1.0 20.0 70-1301160.083 U23 Chloroform
ug/L1.0 20.0 60-1401010.050 U20 Chloromethane
ug/L1.0 20.0 70-1301020.075 U20 cis-1,2-Dichloroethene
ug/L1.0 20.0 70-1301130.073 U23 cis-1,3-Dichloropropene
ug/L1.0 20.0 70-1301090.067 U22 Dibromochloromethane
ug/L1.0 20.0 70-1301110.13 U22 Dibromomethane
ug/L1.0 20.0 60-1401040.091 U21 Dichlorodifluoromethane
ug/L100 100 0-20014726 U150 Ethanol
ug/L1.0 20.0 70-1301120.10 U22 Ethylbenzene
ug/L1.0 40.0 70-1301180.35 U47 Freon 113
ug/L1.0 20.0 70-1301050.15 U21 Hexachlorobutadiene
ug/L1.0 20.0 70-1301240.21 U25 Isopropyl Ether
ug/L1.0 20.0 70-1301140.13 U23 Isopropylbenzene
ug/L2.0 40.0 70-1301160.18 U46 m,p-Xylenes
ug/L2.0 20.0 70-1301210.070 U24 Methylene Chloride
ug/L1.0 20.0 70-1301210.12 U24 Methyl-tert-Butyl Ether
ug/L1.0 20.0 70-1301060.086 U21 Naphthalene
ug/L1.0 20.0 70-1301200.074 U24 n-Butyl Benzene
ug/L1.0 20.0 70-1301210.073 U24 n-Propyl Benzene
ug/L1.0 20.0 70-1301120.088 U22 o-Xylene
ug/L1.0 20.0 70-1301230.053 U25 sec-Butylbenzene
ug/L1.0 20.0 70-1301040.082 U21 Styrene
ug/L1.0 20.0 70-1301140.094 U23 tert-Butylbenzene
ug/L1.0 20.0 70-1301200.099 U24 Tetrachloroethene
ug/L1.0 20.0 70-1301120.053 U22 Toluene
ug/L1.0 20.0 70-1301250.11 U25 trans-1,2-Dichloroethene
ug/L1.0 20.0 70-1301230.080 U25 trans-1,3-Dichloropropene
ug/L1.0 20.0 70-1301120.13 U22 Trichloroethene
ug/L1.0 20.0 60-1401120.15 U22 Trichlorofluoromethane
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 17 of 27Page 17 of 27
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 1E08001 - EPA 5030B_MS - Continued
Prepared: 05/07/2021 13:00 Analyzed: 05/08/2021 17:04Matrix Spike (1E08001-MS1) Continued
Source: CE06773-06
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 60-140860.083 U17 Vinyl chloride
ug/L1.0 60.0 70-1301150.22 U69 Xylenes (Total)
ug/L 50.0 70-1304-Bromofluorobenzene 10753
ug/L 50.0 70-130Dibromofluoromethane9949
ug/L 50.0 70-130Toluene-d8 10251
Prepared: 05/07/2021 13:00 Analyzed: 05/08/2021 17:32Matrix Spike Dup (1E08001-MSD1)
Source: CE06773-06
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 1670-130104 10.091 U21 1,1,1,2-Tetrachloroethane
ug/L1.0 20.0 1870-130103 60.15 U21 1,1,1-Trichloroethane
ug/L1.0 20.0 1670-130113 20.085 U23 1,1,2,2-Tetrachloroethane
ug/L1.0 20.0 1870-130123 80.068 U25 1,1,2-Trichloroethane
ug/L1.0 20.0 1970-130114 80.050 U23 1,1-Dichloroethane
ug/L1.0 20.0 2070-130108 70.15 U22 1,1-Dichloroethene
ug/L1.0 20.0 1770-130110 80.063 U22 1,1-Dichloropropene
ug/L1.0 20.0 1770-13098 100.25 U20 1,2,3-Trichlorobenzene
ug/L1.0 20.0 1770-13099 30.15 U20 1,2,3-Trichloropropane
ug/L1.0 20.0 1770-13095 60.097 U19 1,2,4-Trichlorobenzene
ug/L1.0 20.0 1870-130109 60.067 U22 1,2,4-Trimethylbenzene
ug/L1.0 20.0 1870-13098 0.40.48 U20 1,2-Dibromo-3-chloropropane
ug/L1.0 20.0 1570-130109 50.42 U22 1,2-Dibromoethane
ug/L1.0 20.0 1670-130103 40.052 U21 1,2-Dichlorobenzene
ug/L1.0 20.0 1670-130107 60.082 U21 1,2-Dichloroethane
ug/L1.0 20.0 1970-130114 50.098 U23 1,2-Dichloropropane
ug/L1.0 20.0 1670-130102 90.10 U20 1,3,5-Trimethylbenzene
ug/L1.0 20.0 1770-130104 70.092 U21 1,3-Dichlorobenzene
ug/L1.0 20.0 1670-130114 20.15 U23 1,3-Dichloropropane
ug/L1.0 20.0 1670-130106 70.10 U21 1,4-Dichlorobenzene
ug/L1.0 20.0 2070-130125 70.12 U25 2,2-Dichloropropane
ug/L1.0 20.0 1670-130107 50.10 U21 2-Chlorotoluene
ug/L1.0 20.0 1670-130107 90.10 U21 4-Chlorotoluene
ug/L1.0 20.0 1770-130104 90.066 U21 4-Isopropyltoluene
ug/L1.0 20.0 1770-130110 70.050 U22 Benzene
ug/L1.0 20.0 1770-130105 40.13 U21 Bromobenzene
ug/L1.0 20.0 1870-130103 70.11 U21 Bromochloromethane
ug/L1.0 20.0 1670-130109 60.10 U22 Bromodichloromethane
ug/L1.0 20.0 4470-130116 20.20 U23 Bromoform
ug/L1.0 20.0 2760-14092 60.28 U18 Bromomethane
ug/L1.0 20.0 1770-130109 50.082 U22 Carbon Tetrachloride
ug/L1.0 20.0 1670-130111 0.20.069 U22 Chlorobenzene
ug/L1.0 20.0 2660-140118 50.18 U24 Chloroethane
ug/L1.0 20.0 1770-130109 70.083 U22 Chloroform
ug/L1.0 20.0 2860-14094 70.050 U19 Chloromethane
ug/L1.0 20.0 1870-130101 10.075 U20 cis-1,2-Dichloroethene
ug/L1.0 20.0 1770-130103 90.073 U21 cis-1,3-Dichloropropene
ug/L1.0 20.0 1670-130120 100.067 U24 Dibromochloromethane
ug/L1.0 20.0 1570-130102 90.13 U20 Dibromomethane
ug/L1.0 20.0 4860-14099 50.091 U20 Dichlorodifluoromethane
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 18 of 27Page 18 of 27
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 1E08001 - EPA 5030B_MS - Continued
Prepared: 05/07/2021 13:00 Analyzed: 05/08/2021 17:32Matrix Spike Dup (1E08001-MSD1) Continued
Source: CE06773-06
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L100 100 250-200179 2026 U180 Ethanol
ug/L1.0 20.0 1670-130113 0.80.10 U23 Ethylbenzene
ug/L1.0 40.0 2570-130114 30.35 U46 Freon 113
ug/L1.0 20.0 1970-13096 90.15 U19 Hexachlorobutadiene
ug/L1.0 20.0 3070-130120 40.21 U24 Isopropyl Ether
ug/L1.0 20.0 1670-130116 20.13 U23 Isopropylbenzene
ug/L2.0 40.0 1670-130118 20.18 U47 m,p-Xylenes
ug/L2.0 20.0 1770-130115 50.070 U23 Methylene Chloride
ug/L1.0 20.0 2170-130116 40.12 U23 Methyl-tert-Butyl Ether
ug/L1.0 20.0 1970-130103 20.086 U21 Naphthalene
ug/L1.0 20.0 1570-130110 80.074 U22 n-Butyl Benzene
ug/L1.0 20.0 1670-130118 20.073 U24 n-Propyl Benzene
ug/L1.0 20.0 1570-130113 20.088 U23 o-Xylene
ug/L1.0 20.0 1770-130113 80.053 U23 sec-Butylbenzene
ug/L1.0 20.0 2370-130106 20.082 U21 Styrene
ug/L1.0 20.0 2270-130104 100.094 U21 tert-Butylbenzene
ug/L1.0 20.0 2670-130120 0.50.099 U24 Tetrachloroethene
ug/L1.0 20.0 1770-130116 40.053 U23 Toluene
ug/L1.0 20.0 1970-130113 100.11 U23 trans-1,2-Dichloroethene
ug/L1.0 20.0 1670-130130 50.080 U26 trans-1,3-Dichloropropene
ug/L1.0 20.0 1870-130107 50.13 U21 Trichloroethene
ug/L1.0 20.0 2260-140104 70.15 U21 Trichlorofluoromethane
ug/L1.0 20.0 2760-14081 70.083 U16 Vinyl chloride
ug/L1.0 60.0 1670-130116 20.22 U70 Xylenes (Total)
ug/L 50.0 70-1304-Bromofluorobenzene 11759
ug/L 50.0 70-130Dibromofluoromethane9849
ug/L 50.0 70-130Toluene-d8 10553
Batch 1E10018 - EPA 5030B_MS
Prepared: 05/10/2021 14:00 Analyzed: 05/10/2021 16:28Blank (1E10018-BLK1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.00.091 U 1,1,1,2-Tetrachloroethane
ug/L1.00.15 U 1,1,1-Trichloroethane
ug/L1.00.085 U 1,1,2,2-Tetrachloroethane
ug/L1.00.068 U 1,1,2-Trichloroethane
ug/L1.00.050 U 1,1-Dichloroethane
ug/L1.00.15 U 1,1-Dichloroethene
ug/L1.00.063 U 1,1-Dichloropropene
ug/L1.00.25 U 1,2,3-Trichlorobenzene
ug/L1.00.15 U 1,2,3-Trichloropropane
ug/L1.00.097 U 1,2,4-Trichlorobenzene
ug/L1.00.067 U 1,2,4-Trimethylbenzene
ug/L1.00.48 U 1,2-Dibromo-3-chloropropane
ug/L1.00.42 U 1,2-Dibromoethane
ug/L1.00.052 U 1,2-Dichlorobenzene
ug/L1.00.082 U 1,2-Dichloroethane
ug/L1.00.098 U 1,2-Dichloropropane
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 19 of 27Page 19 of 27
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 1E10018 - EPA 5030B_MS - Continued
Prepared: 05/10/2021 14:00 Analyzed: 05/10/2021 16:28Blank (1E10018-BLK1) Continued
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.00.10 U 1,3,5-Trimethylbenzene
ug/L1.00.092 U 1,3-Dichlorobenzene
ug/L1.00.15 U 1,3-Dichloropropane
ug/L1.00.10 U 1,4-Dichlorobenzene
ug/L1.00.12 U 2,2-Dichloropropane
ug/L1.00.10 U 2-Chlorotoluene
ug/L1.00.10 U 4-Chlorotoluene
ug/L1.00.066 U 4-Isopropyltoluene
ug/L1.00.050 U Benzene
ug/L1.00.13 U Bromobenzene
ug/L1.00.11 U Bromochloromethane
ug/L1.00.10 U Bromodichloromethane
ug/L1.00.20 U Bromoform
ug/L1.00.28 U Bromomethane
ug/L1.00.082 U Carbon Tetrachloride
ug/L1.00.069 U Chlorobenzene
ug/L1.00.18 U Chloroethane
ug/L1.00.083 U Chloroform
ug/L1.00.050 U Chloromethane
ug/L1.00.075 U cis-1,2-Dichloroethene
ug/L1.00.073 U cis-1,3-Dichloropropene
ug/L1.00.067 U Dibromochloromethane
ug/L1.00.13 U Dibromomethane
ug/L1.00.091 U Dichlorodifluoromethane
ug/L1.00.10 U Ethylbenzene
ug/L1.00.35 U Freon 113
ug/L1.00.15 U Hexachlorobutadiene
ug/L1.00.21 U Isopropyl Ether
ug/L1.00.13 U Isopropylbenzene
ug/L2.00.18 U m,p-Xylenes
ug/L2.00.070 U Methylene Chloride
ug/L1.00.12 U Methyl-tert-Butyl Ether
ug/L1.00.086 U Naphthalene
ug/L1.00.074 U n-Butyl Benzene
ug/L1.00.073 U n-Propyl Benzene
ug/L1.00.088 U o-Xylene
ug/L1.00.053 U sec-Butylbenzene
ug/L1.00.082 U Styrene
ug/L1.00.094 U tert-Butylbenzene
ug/L1.00.099 U Tetrachloroethene
ug/L1.00.053 U Toluene
ug/L1.00.11 U trans-1,2-Dichloroethene
ug/L1.00.080 U trans-1,3-Dichloropropene
ug/L1.00.13 U Trichloroethene
ug/L1.00.15 U Trichlorofluoromethane
ug/L1.00.083 U Vinyl chloride
ug/L1.00.22 U Xylenes (Total)
ug/L 50.0 70-1304-Bromofluorobenzene 10754
ug/L 50.0 70-130Dibromofluoromethane9950
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 20 of 27Page 20 of 27
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 1E10018 - EPA 5030B_MS - Continued
Prepared: 05/10/2021 14:00 Analyzed: 05/10/2021 16:28Blank (1E10018-BLK1) Continued
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L 50.0 70-130Toluene-d8 10653
Prepared: 05/10/2021 14:00 Analyzed: 05/10/2021 14:36LCS (1E10018-BS1)
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 70-1309419 1,1,1,2-Tetrachloroethane
ug/L1.0 20.0 70-13010220 1,1,1-Trichloroethane
ug/L1.0 20.0 70-13010521 1,1,2,2-Tetrachloroethane
ug/L1.0 20.0 70-13010621 1,1,2-Trichloroethane
ug/L1.0 20.0 70-13011824 1,1-Dichloroethane
ug/L1.0 20.0 70-13010822 1,1-Dichloroethene
ug/L1.0 20.0 70-13011723 1,1-Dichloropropene
ug/L1.0 20.0 70-1309118 1,2,3-Trichlorobenzene
ug/L1.0 20.0 70-1308818 1,2,3-Trichloropropane
ug/L1.0 20.0 70-1308918 1,2,4-Trichlorobenzene
ug/L1.0 20.0 70-13010321 1,2,4-Trimethylbenzene
ug/L1.0 20.0 70-1308717 1,2-Dibromo-3-chloropropane
ug/L1.0 20.0 70-1309619 1,2-Dibromoethane
ug/L1.0 20.0 70-1309920 1,2-Dichlorobenzene
ug/L1.0 20.0 70-13010621 1,2-Dichloroethane
ug/L1.0 20.0 70-13011924 1,2-Dichloropropane
ug/L1.0 20.0 70-13010020 1,3,5-Trimethylbenzene
ug/L1.0 20.0 70-13010020 1,3-Dichlorobenzene
ug/L1.0 20.0 70-13010020 1,3-Dichloropropane
ug/L1.0 20.0 70-13010521 1,4-Dichlorobenzene
ug/L1.0 20.0 70-13012325 2,2-Dichloropropane
ug/L1.0 20.0 70-13010321 2-Chlorotoluene
ug/L1.0 20.0 70-13010120 4-Chlorotoluene
ug/L1.0 20.0 70-13010421 4-Isopropyltoluene
ug/L1.0 20.0 70-13011423 Benzene
ug/L1.0 20.0 70-1309519 Bromobenzene
ug/L1.0 20.0 70-13010521 Bromochloromethane
ug/L1.0 20.0 70-13010822 Bromodichloromethane
ug/L1.0 20.0 70-13011523 Bromoform
ug/L1.0 20.0 60-14010421 Bromomethane
ug/L1.0 20.0 70-13010922 Carbon Tetrachloride
ug/L1.0 20.0 70-13010321 Chlorobenzene
ug/L1.0 20.0 60-14012725 Chloroethane
ug/L1.0 20.0 70-13010621 Chloroform
ug/L1.0 20.0 60-14011022 Chloromethane
ug/L1.0 20.0 70-1309719 cis-1,2-Dichloroethene
ug/L1.0 20.0 70-13010421 cis-1,3-Dichloropropene
ug/L1.0 20.0 70-13010120 Dibromochloromethane
ug/L1.0 20.0 70-13010721 Dibromomethane
ug/L1.0 20.0 60-14010421 Dichlorodifluoromethane
ug/L1.0 20.0 70-13010321 Ethylbenzene
ug/L1.0 40.0 70-13011546 Freon 113
ug/L1.0 20.0 70-1309218 Hexachlorobutadiene
ug/L1.0 20.0 70-13011723 Isopropyl Ether
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 21 of 27Page 21 of 27
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 1E10018 - EPA 5030B_MS - Continued
Prepared: 05/10/2021 14:00 Analyzed: 05/10/2021 14:36LCS (1E10018-BS1) Continued
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 70-13010822 Isopropylbenzene
ug/L2.0 40.0 70-13010944 m,p-Xylenes
ug/L2.0 20.0 70-13011824 Methylene Chloride
ug/L1.0 20.0 70-13010822 Methyl-tert-Butyl Ether
ug/L1.0 20.0 70-1309218 Naphthalene
ug/L1.0 20.0 70-13010822 n-Butyl Benzene
ug/L1.0 20.0 70-13011122 n-Propyl Benzene
ug/L1.0 20.0 70-13010120 o-Xylene
ug/L1.0 20.0 70-13011022 sec-Butylbenzene
ug/L1.0 20.0 70-1309719 Styrene
ug/L1.0 20.0 70-13010220 tert-Butylbenzene
ug/L1.0 20.0 70-13011022 Tetrachloroethene
ug/L1.0 20.0 70-13010421 Toluene
ug/L1.0 20.0 70-13011523 trans-1,2-Dichloroethene
ug/L1.0 20.0 70-13011122 trans-1,3-Dichloropropene
ug/L1.0 20.0 70-13011022 Trichloroethene
ug/L1.0 20.0 60-14010721 Trichlorofluoromethane
ug/L1.0 20.0 60-14010220 Vinyl chloride
ug/L1.0 60.0 70-13010664 Xylenes (Total)
ug/L 50.0 70-1304-Bromofluorobenzene 10251
ug/L 50.0 70-130Dibromofluoromethane9548
ug/L 50.0 70-130Toluene-d8 10552
Prepared: 05/10/2021 14:00 Analyzed: 05/10/2021 15:04Matrix Spike (1E10018-MS1)
Source: CE06773-07
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 70-1301090.091 U22 1,1,1,2-Tetrachloroethane
ug/L1.0 20.0 70-1301160.15 U23 1,1,1-Trichloroethane
ug/L1.0 20.0 70-1301250.085 U25 1,1,2,2-Tetrachloroethane
ug/L1.0 20.0 70-1301220.068 U24 1,1,2-Trichloroethane
ug/L1.0 20.0 70-1301340.050 U27 1,1-Dichloroethane
ug/L1.0 20.0 70-1301220.15 U24 1,1-Dichloroethene
ug/L1.0 20.0 70-1301350.063 U27 1,1-Dichloropropene
ug/L1.0 20.0 70-1301070.25 U21 1,2,3-Trichlorobenzene
ug/L1.0 20.0 70-1301100.15 U22 1,2,3-Trichloropropane
ug/L1.0 20.0 70-1301040.097 U21 1,2,4-Trichlorobenzene
ug/L1.0 20.0 70-1301150.067 U23 1,2,4-Trimethylbenzene
ug/L1.0 20.0 70-1301030.48 U21 1,2-Dibromo-3-chloropropane
ug/L1.0 20.0 70-1301120.42 U22 1,2-Dibromoethane
ug/L1.0 20.0 70-1301130.052 U23 1,2-Dichlorobenzene
ug/L1.0 20.0 70-1301180.082 U24 1,2-Dichloroethane
ug/L1.0 20.0 70-1301280.098 U26 1,2-Dichloropropane
ug/L1.0 20.0 70-1301110.10 U22 1,3,5-Trimethylbenzene
ug/L1.0 20.0 70-1301120.092 U22 1,3-Dichlorobenzene
ug/L1.0 20.0 70-1301150.15 U23 1,3-Dichloropropane
ug/L1.0 20.0 70-1301140.10 U23 1,4-Dichlorobenzene
ug/L1.0 20.0 70-1301400.12 U28 2,2-Dichloropropane
ug/L1.0 20.0 70-1301130.10 U23 2-Chlorotoluene
ug/L1.0 20.0 70-1301140.10 U23 4-Chlorotoluene
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 22 of 27Page 22 of 27
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 1E10018 - EPA 5030B_MS - Continued
Prepared: 05/10/2021 14:00 Analyzed: 05/10/2021 15:04Matrix Spike (1E10018-MS1) Continued
Source: CE06773-07
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 70-1301150.066 U23 4-Isopropyltoluene
ug/L1.0 20.0 70-1301260.050 U25 Benzene
ug/L1.0 20.0 70-1301070.13 U21 Bromobenzene
ug/L1.0 20.0 70-1301210.11 U24 Bromochloromethane
ug/L1.0 20.0 70-1301180.10 U24 Bromodichloromethane
ug/L1.0 20.0 70-1301340.20 U27 Bromoform
ug/L1.0 20.0 60-1401110.28 U22 Bromomethane
ug/L1.0 20.0 70-1301200.082 U24 Carbon Tetrachloride
ug/L1.0 20.0 70-1301160.069 U23 Chlorobenzene
ug/L1.0 20.0 60-1401510.18 U30 Chloroethane
ug/L1.0 20.0 70-1301270.083 U25 Chloroform
ug/L1.0 20.0 60-1401190.050 U24 Chloromethane
ug/L1.0 20.0 70-1301120.075 U22 cis-1,2-Dichloroethene
ug/L1.0 20.0 70-1301170.073 U23 cis-1,3-Dichloropropene
ug/L1.0 20.0 70-1301190.067 U24 Dibromochloromethane
ug/L1.0 20.0 70-1301150.13 U23 Dibromomethane
ug/L1.0 20.0 60-1401140.091 U23 Dichlorodifluoromethane
ug/L1.0 20.0 70-1301150.10 U23 Ethylbenzene
ug/L1.0 40.0 70-1301290.35 U51 Freon 113
ug/L1.0 20.0 70-1301140.15 U23 Hexachlorobutadiene
ug/L1.0 20.0 70-1301350.21 U27 Isopropyl Ether
ug/L1.0 20.0 70-1301190.13 U24 Isopropylbenzene
ug/L2.0 40.0 70-1301190.18 U48 m,p-Xylenes
ug/L2.0 20.0 70-1301290.070 U26 Methylene Chloride
ug/L1.0 20.0 70-1301250.12 U25 Methyl-tert-Butyl Ether
ug/L1.0 20.0 70-1301100.086 U22 Naphthalene
ug/L1.0 20.0 70-1301230.074 U25 n-Butyl Benzene
ug/L1.0 20.0 70-1301270.073 U25 n-Propyl Benzene
ug/L1.0 20.0 70-1301140.088 U23 o-Xylene
ug/L1.0 20.0 70-1301250.053 U25 sec-Butylbenzene
ug/L1.0 20.0 70-1301100.082 U22 Styrene
ug/L1.0 20.0 70-1301130.094 U23 tert-Butylbenzene
ug/L1.0 20.0 70-1301300.099 U26 Tetrachloroethene
ug/L1.0 20.0 70-1301160.053 U23 Toluene
ug/L1.0 20.0 70-1301340.11 U27 trans-1,2-Dichloroethene
ug/L1.0 20.0 70-1301260.080 U25 trans-1,3-Dichloropropene
ug/L1.0 20.0 70-1301190.13 U24 Trichloroethene
ug/L1.0 20.0 60-1401210.15 U24 Trichlorofluoromethane
ug/L1.0 20.0 60-1401150.083 U23 Vinyl chloride
ug/L1.0 60.0 70-1301180.22 U71 Xylenes (Total)
ug/L 50.0 70-1304-Bromofluorobenzene 10552
ug/L 50.0 70-130Dibromofluoromethane10151
ug/L 50.0 70-130Toluene-d8 10552
Prepared: 05/10/2021 14:00 Analyzed: 05/10/2021 15:32Matrix Spike Dup (1E10018-MSD1)
Source: CE06773-07
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 1670-13088 220.091 U18 1,1,1,2-Tetrachloroethane
ug/L1.0 20.0 1870-13097 180.15 U19 1,1,1-Trichloroethane
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 23 of 27Page 23 of 27
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 1E10018 - EPA 5030B_MS - Continued
Prepared: 05/10/2021 14:00 Analyzed: 05/10/2021 15:32Matrix Spike Dup (1E10018-MSD1) Continued
Source: CE06773-07
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 1670-130102 200.085 U20 1,1,2,2-Tetrachloroethane
ug/L1.0 20.0 1870-13097 230.068 U19 1,1,2-Trichloroethane
ug/L1.0 20.0 1970-130109 200.050 U22 1,1-Dichloroethane
ug/L1.0 20.0 2070-13099 200.15 U20 1,1-Dichloroethene
ug/L1.0 20.0 1770-130102 280.063 U20 1,1-Dichloropropene
ug/L1.0 20.0 1770-13091 170.25 U18 1,2,3-Trichlorobenzene
ug/L1.0 20.0 1770-13088 230.15 U18 1,2,3-Trichloropropane
ug/L1.0 20.0 1770-13087 180.097 U17 1,2,4-Trichlorobenzene
ug/L1.0 20.0 1870-13097 170.067 U19 1,2,4-Trimethylbenzene
ug/L1.0 20.0 1870-13088 150.48 U18 1,2-Dibromo-3-chloropropane
ug/L1.0 20.0 1570-13094 180.42 U19 1,2-Dibromoethane
ug/L1.0 20.0 1670-13094 190.052 U19 1,2-Dichlorobenzene
ug/L1.0 20.0 1670-13092 260.082 U18 1,2-Dichloroethane
ug/L1.0 20.0 1970-130105 200.098 U21 1,2-Dichloropropane
ug/L1.0 20.0 1670-13093 180.10 U19 1,3,5-Trimethylbenzene
ug/L1.0 20.0 1770-13094 170.092 U19 1,3-Dichlorobenzene
ug/L1.0 20.0 1670-13096 170.15 U19 1,3-Dichloropropane
ug/L1.0 20.0 1670-13099 140.10 U20 1,4-Dichlorobenzene
ug/L1.0 20.0 2070-130111 230.12 U22 2,2-Dichloropropane
ug/L1.0 20.0 1670-13098 150.10 U20 2-Chlorotoluene
ug/L1.0 20.0 1670-13095 180.10 U19 4-Chlorotoluene
ug/L1.0 20.0 1770-13095 180.066 U19 4-Isopropyltoluene
ug/L1.0 20.0 1770-130104 190.050 U21 Benzene
ug/L1.0 20.0 1770-13089 180.13 U18 Bromobenzene
ug/L1.0 20.0 1870-130102 180.11 U20 Bromochloromethane
ug/L1.0 20.0 1670-13098 190.10 U20 Bromodichloromethane
ug/L1.0 20.0 4470-130104 250.20 U21 Bromoform
ug/L1.0 20.0 2760-14087 240.28 U17 Bromomethane
ug/L1.0 20.0 1770-130102 160.082 U20 Carbon Tetrachloride
ug/L1.0 20.0 1670-13098 170.069 U20 Chlorobenzene
ug/L1.0 20.0 2660-140117 250.18 U23 Chloroethane
ug/L1.0 20.0 1770-130102 220.083 U20 Chloroform
ug/L1.0 20.0 2860-14098 200.050 U20 Chloromethane
ug/L1.0 20.0 1870-13091 200.075 U18 cis-1,2-Dichloroethene
ug/L1.0 20.0 1770-13099 160.073 U20 cis-1,3-Dichloropropene
ug/L1.0 20.0 1670-13098 200.067 U20 Dibromochloromethane
ug/L1.0 20.0 1570-13099 150.13 U20 Dibromomethane
ug/L1.0 20.0 4860-14098 150.091 U20 Dichlorodifluoromethane
ug/L1.0 20.0 1670-13095 190.10 U19 Ethylbenzene
ug/L1.0 40.0 2570-130105 200.35 U42 Freon 113
ug/L1.0 20.0 1970-13088 260.15 U18 Hexachlorobutadiene
ug/L1.0 20.0 3070-130109 210.21 U22 Isopropyl Ether
ug/L1.0 20.0 1670-13097 200.13 U19 Isopropylbenzene
ug/L2.0 40.0 1670-130100 170.18 U40 m,p-Xylenes
ug/L2.0 20.0 1770-130107 180.070 U21 Methylene Chloride
ug/L1.0 20.0 2170-130104 180.12 U21 Methyl-tert-Butyl Ether
ug/L1.0 20.0 1970-13093 170.086 U19 Naphthalene
ug/L1.0 20.0 1570-130100 200.074 U20 n-Butyl Benzene
ug/L1.0 20.0 1670-130104 200.073 U21 n-Propyl Benzene
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 24 of 27Page 24 of 27
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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 1E10018 - EPA 5030B_MS - Continued
Prepared: 05/10/2021 14:00 Analyzed: 05/10/2021 15:32Matrix Spike Dup (1E10018-MSD1) Continued
Source: CE06773-07
FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL
Spike Source %REC RPD
ug/L1.0 20.0 1570-13097 170.088 U19 o-Xylene
ug/L1.0 20.0 1770-130106 160.053 U21 sec-Butylbenzene
ug/L1.0 20.0 2370-13091 190.082 U18 Styrene
ug/L1.0 20.0 2270-13098 140.094 U20 tert-Butylbenzene
ug/L1.0 20.0 2670-13099 280.099 U20 Tetrachloroethene
ug/L1.0 20.0 1770-13098 170.053 U20 Toluene
ug/L1.0 20.0 1970-130107 220.11 U21 trans-1,2-Dichloroethene
ug/L1.0 20.0 1670-130102 210.080 U20 trans-1,3-Dichloropropene
ug/L1.0 20.0 1870-130103 150.13 U21 Trichloroethene
ug/L1.0 20.0 2260-14096 230.15 U19 Trichlorofluoromethane
ug/L1.0 20.0 2760-14089 250.083 U18 Vinyl chloride
ug/L1.0 60.0 1670-13099 170.22 U60 Xylenes (Total)
ug/L 50.0 70-1304-Bromofluorobenzene 10352
ug/L 50.0 70-130Dibromofluoromethane9849
ug/L 50.0 70-130Toluene-d8 10351
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FLAGS/NOTES AND DEFINITIONS [TOC_1]Flags/Notes[TOC]
The sample was analyzed at dilution.
The analyte was detected in the associated method blank.
The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
MRL
E
U
J
D
B
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.PQL
Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.[CALC]
Internal standard outside acceptance limits. Samples results are considered estimated.QI-02
The associated laboratory control sample exhibited high bias; since the result is ND, there is no impact.QL-02
The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
QM-07
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL Page 26 of 27Page 26 of 27
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