RA-1897_11583_CA_SCH_20070119_UNKNOWN

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EAsrCo AsT
Environmenta l, P.A.
SITE CHE CK
(15A NCAC 2N 0.0603(b ))
PREPARED IN RESPONSE TO A SUSPECTED LE AKING
COMMERCIAL UNDERGROUND STORAGE TANK SYSTEM
LOCATED AT:
TAYLOR'S BP
10005 SIX FORKS ROAD
RALEIGH, WAKE COUNTY, NORTH CAROLINA
J anuary J 9, 2007
Current Property Owner:
Taylor & Gail Cash
3036 Cranesbill Drive
Raleigh, NC 27613
[phone]
Consul rant:
East Coast Environmental, P.A.
3709 Junction Blvd.
Raleigh, North Carolina 27603
(9 19) 772-0268
Release Discovery Date: March 16, 2001
Cause of Release: Leaking Product Dispensers?
UST Size and Contents: 20,000-Gallon Gasoline UST
Latitude: 350 54.949' N, Longitude: 780 39.022' W
3709 Junction Blvd., Raleigh, NC 27603 [phone] Fax [phone]
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Site Check (l5A NCAC 2N 0.0603(b))
Taylor's BP
I 0005 Six Forks Road, Raleigh, Wake County, North Carolina
Table of Contents
A. BACKGROUND ........................................................................................................ 3
B. SITE GEOLOGY AND BYDROGEOLOGY ......................................................... 4
c. sorLs mvESTIGATION ........................................................................................ 4
c. 1 GeoPROBED SoiL BoRJNGS ....................................................................................... 4
C.3 SOIL SAMPL£NG RESULTS .......................................................................................... 4
D. CONCLUSIONS ........................................................................................................ 6
E. LlMITATIONS .......................................................................................................... 8
ection A Figures
Figure 1
Figu re 2
Section B Tables
Appendices
Site Location Map
Site Map with Soil Sampling Locations
Section C Laboratory Reports
East Coa~1 Environmtntal, P.A.
3709 Junction Blvd.
Raleigh, Nonh Carolina 27603
Phone: [phone] FAX: [phone]
2
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A. BACKGROUND
Site Check (15A NCAC 2N 0.0603(b))
Taylor's BP
10005 Six Forks Road, Raleigh, Wake County, North Carolina
The subject property (hereinafter is referred to as the "Site") is identified as the Taylor's BP and is
located at l0005 Six Forks Road, Raleigh, Wake County, North Carolina. (See Section A, Figure 1 for
Site location.) The Site consists of an approximately 0.93 acre parcel of land currently owned by Taylor
& Gail Cash, and is occupied by Taylor's BP which operates two petroleum Underground Storage Tanks
(USTs) for the retail sale of gasoline, kerosene and diesel fuel.
One or more gasoline releases from UST systems have previously been documented at the Site while
either removing or abandoning in place several old UST systems during the 1990s. In addition, gasoline
related compounds have been detected in an on-Site water supply well which has since been taken out of
use.
This Site check consisted of the installation of a total of 17 Geoprobed soil borings advanced at the
locations inclicated in Section A, Figure 2. Nine borings (SS-1 through SS-9) were advanced adjacent
to the 20,000 and 4,000 gallon USTs to a total depth of 16 feet below land surface so that soi l samples
could be collected from these borings at depth of approximately 15 to 16 feet below land surface. These
soil samples were subsequently placed in Encore sampling devices for submittal to an analytical
laboratory for low boiling point Total Petroleum Hydrocarbon (TPH) analysis by EPA Method 5030.
The soil samples originating from borings SS-6, SS-7, SS-8 and SS-9 nearest the 4,000 gallon
kerosene/diesel UST were also submitted for high boiling point TPH testing by EPA Method 3550.
The soil borings identified as L-1 through L-5 were advanced adjacent to the gasoline product lines to a
total depth of 4 feet below land surface. Samples were collected from these borings at depth of
approximately 3 to 4 feet below land surface and submitted to an analytical laboratory for low boiling
point TPH analysis by EPA Method 5030.
Finally, the soil borings identified as P-.1 through P3 were advanced adjacent to the gasoline and
diesel/kerosene product dispensers to total depths ranging from 8 to 16 feet below land surface.
Samples collected from all of these borings were submitted to an analytical laboratory for sample
specific combination of tests including low boiling point TPH analysis by EPA Method 5030, volati le
organic compounds by EPA 8260, volatile petroleum hydrocarbons by the MADEP-VPH test and for
high boiling point TPH by EPA Method 3550.
East Coast l!nvironmtntal, P.IL
3709 Junction Blvd.
Raleigh, North Carolina 27603
Phone: {919) 772.{)268 FAX: [phone]
3
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Site Check (lSA NCAC 2N 0.0603(b))
Taylor's BP
10005 Six Forks Road, Raleigh, Wake County, North Carolina
B. SITE GEOLOGY AND HYDROGEOLOGY
The Geologic Map of North Carolina 1 locates the Site within injected gneiss of the Raleigh Belt. More
specifically, the Geologic Map of North Carolina describes this injected gneiss as "biotite gneiss and
schist intruded by numerous sills and dikes of granite, pegmatite and aplite; minor borneblende gneiss".
Geoprobed borings advanced at the Site for completion of this Site Check encountered orange-red silty
clay from land surface down to about six feet below. From about six feet down to sixteen feet the
material became more orange-white in color and less clayey. Some white quartz pebbles were also
found towards the bottom of the borings. Neither competent rock nor groundwater was encountered in
any of the borings completed for this Site Check.
C. SOILS INVESTIGATION
C. I Geoprobed Soil Borings
As stated above, ECE mobilized to the Site on January 3, 2007 for the purpose of installing a series of 17
Geoprobed soil borings at the locations indicated in Section A, Figure 2. These activities were initiated
to check for the presence of low and high boiling point TPH by California Method 8015, with EPA
Methods 3550 and 5030 as sample preparation, for volatile organic compounds by EPA Method 8260
and for volatile petroleum hydrocarbons by the MADEP-VPH test.
C.3 Soil Sampling Results
Analytical data for the soil samples collected from borings SS-1 through SS-9, L-1 through L-5 and P-3
and analyzed for the presence of low boiling point TPH by EPA Method 5030 did not indicate the
presence of low boiling point TPH in any sample at levels above the method detection limits.
Analytical data for the soil samples collected from borings SS-6 through SS-9 and P-3 analyzed for the
presence of high boiling point TPH by EPA Method 3550 did show the presence of high boiling point
TPH at levels above the method detection limits in all five samples. Further, soil samples SS-6 and SS-7
detected higb boiling point TPH at levels (51 and 63 mglkg, respectively) in excess of the North
Carolina Department of Environment and Natural Resources action level of 40 mglkg.
I Reference: Geologic Map of North Caroli11a, Department of Natural Resources and Community Development, Division or Land
Resources, 1985 edition.
East Coast Environmental, P.A. 4
3709 Junction Blvd.
Raleigh, North Caroli na 27603
Phone: [phone] FAX: [phone]
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Site Check (lSA NCAC 2N 0.0603(b))
Taylor's BP
10005 Six Forks Road, Raleigh, Wake County, North Carolina
The analytical results for soi l samples P-1 and P-2 collected from under the gasoline product dispensers
detected the presence of numerous compounds targeted by EPA Method 8260 and the MADEP-VPH
test. Many of these compounds were detected at levels in excess of their Soil to Groundwater Maximum
Soil Contaminant Concentrations as set forth in the "Guidelines for Assessment and Corrective Action"
prepared by the North Carolina Underground Storage Tank Section effective July I, 2001 (The
Guidelines. Four constituents (benzene, 1,2,4 trimethyl benzene, C5-C8 aliphatics and C9-ClO
aromatics) were also detected at levels in excess of their Residential Maximum Soi l Contaminant
Concentrations as set forth in the Guidelines. Table 1 in Section B is a summary of these analytical
results displayin g only detected contaminants.
The laboratory analytical report for the soil samples collected by ECE for completion of this Site check
are also presented as an attachment in Section C.
East Coast E11vlronmental, P.A.
3709 Junction Blvd.
Raleigh, North Carolin11 27603
Phone: [phone] FAX: [phone]
5
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D. CONCLUSIONS
Site Check (ISA NCAC lN 0.0603(b))
Taylor's BP
10005 Six Forks Road, Raleigh, Wake County, North Carolina
ECE has completed this Site Check in order to characterize subsurface soil conditions immediately
surrounding two in-use UST systems on the property identified as the Taylor's BP located at I 0005 Six
Forks Road in Raleigh, Wake County, North Carolina.
One or more gasoline releases have already been documented at the Site while either removing or
abandoning in place old UST systems during the 1990s. In addition, gasoline related compounds have
been detected in an on-Site water supply well which has since been taken out of use.
This Site check consisted of the installation of a total of 17 Geoprobed soil borings at the locations
indicated in Section A, Figure 2. Nine borings (SS-1 through SS-9) were advanced adjacent to the in-
use 20,000 and 4,000 gallon USTs to a total depth of 16 feet below land surface. Soil samples were
coll ected from these borings at a depth of approximately 15 to 16 feet below land surface for submittal
to an analytical laboratory for low boiling point Total Petroleum Hydrocarbon (TPH) analysis by EPA
Method 5030. The soil samples originating from the boring nearest the 4,000 gallon kerosene/diesel
UST were also submitted for high boiling point TPH testing by EPA Method 3550.
The soi l borings identified as L-1 through L-5 were advanced adjacent to the gasoline product lines to a
total depth of 4 feet below land surface. Samples were collected from these borings at depth of
approximately 3 to 4 feet below land surface and submjtted to an analytical laboratory for low boiling
point TPH analysis by EPA Method 5030.
Finall y, the soil borings identified as P-1 through P3 were advanced adjacent to the gasoline and
kerosene/diesel product dispensers to total depths ranging from 8 to 16 feet below land surface. Samples
were collected from these borings at varying depths and submitted to the analytical laboratory for sample
specific combination of tests including low boiling point TPH analysis by EPA Method 5030, volatile
organic compounds by EPA 8260, volatile petroleum hydrocarbons by the MADEP-VPH test and/or for
high boiling point TPH by EPA Method 3550.
Data for the EPA 5030 test in the soil samples found detectable TPH levels in two soil samples
identified as P-1 and P-2 as well as several volatile organic compounds by EPA Method 8260. Finally,
the analytical results for the MADEP-VPH testing also detected targeted contaminants at elevated levels.
East Coafi Enviro11mmtal, P.A.
3709 Junction Blvd.
Raleigh, North Carolina 27603
Phone: [phone] FAX: [phone]
6
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Site Check (lSA NCAC 2N 0.0603(b))
Taylor's BP
10005 Six Forks Road, Raleigh, Wake County, North Carolina
Based on the analytical results for soil samples collected for completion of this Site Check, it can be
stated that a release of gasoline has occurred in the vicinity of the gasoline product dispensers. Because
this product dispenser area has a history of gaso line use associated with previously removed and
abandoned in-place UST systems it cannot be detennined with certainty which UST system(s) is the
actual source of these detected gasoline contaminants. However, it should be noted that MTBE was not
detected in either of the two pump island soil samples submitted for the EPA 8260 analysis which
indicates that the source of this gasoline contamination may be one of the old releases already
documented at the Site. Further, the UST systems that are currently operational at the Site have recently
passed tightness testing which indicates that they are l.ikely not the source of the detected gasoline
contaminants.
ECE recommends that Taylor Cash forward a copy of this report to Mr. Bob Davies of the NCDENR-
UST Section, Raleigh Regional Office, 1628 Mail Service Center, Raleigh, NC 27699.
East Coast Envlronml!ntal, P.A.
3709 Junction Blvd.
Raleigh, Nonh Carolina 27603
Phone: [phone] FAX: (919} 712-0468
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E. LIMITATIONS
Site Check (I SA NCAC 2N 0.0603(b))
Taylor's BP
l0005 Six Forks Road, Raleigh, Wake County, North Carolina
This report has been prepared for the exclusive use of Taylor & Gail Cash and/or their designees,
successors or assigns. It has been prepared in accordance with generally accepted environmental
practices. No other warranty, expressed or implied, is made. ECE's conclusions and recommendations
are based on information supplied by others, together with ECE's own site observations. Although ECE
cannot be responsible for the accuracy of data supplied by others, ECE bas no reason to suspect that any
of the information is inaccurate. The observations described herein are based upon conditions readily
visible on the site at the time ofECE's visit(s).
ECE cannot assume responsibility fo r the person(s) in charge of the site, nor otherwise undertake
responsibility for reporting to any local, state or federal public agencies any conditions at the site that
may present a potential danger to public health, safety or the environment. It is the responsibility of the
responsible party to notify the appropriate local, state or federal public agencies as required by law, or
otherwise to disclose, in a timely manner, any information that may be necessary to prevent any danger
to public health, safety or the environment.
D: \ECE\projects\Cash 'sBP\Cash 's BPSiteCheck.doc
East Coast Environmental, P.A.
3709 Junction Blvd.
Raleigh, Nonh Carolina 27603
Phone: [phone] FAX: [phone]
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Site Check (I SA NCAC 2N 0.0603{b))
Taylor's BP
10005 Six Forks Road, Raleigh, Wake Cotmty, North Carolina
Section A
Figures
East Coast Euviroumeutal, P.A.
3709 Junction Blvd.
Kalcigh, North Carolina 27603
Phone: [phone] FAX: (919) 772..{)468
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1:
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East Coast
Environmental,
P.A.
Data use subject to license
C 2004 Delorme XMap® 4.5
www delorme com
Figure 1
Site Location
Map
XMap®4.5
Taylor's BP 10005
Six Forks Road,
Raleigh, NC
Scale 1 12.000
t"'" 1 000 oft Data Zoom 14-0
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--------------------------
Johnston, Scott
From: Johnston, Scott
Sent:
To:
Monday, September 21 , 2009 1:26PM
'Jared Edwards'
Hi Jared,
I have reviewed the soil sampling for the site check appeal at Taylors Conv. Store Inc. number 11583.
It looks like 13 of the 17 the soil samples and associated analyticals would have been necessary in the CSA if the Site
Check was not performed.
Hope this helps and let me know if you need anything else.
Scott
Scott M. Johnston
Hydrogeologist
NCDENR/DWM/UST Section
1
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FIGUR£ 2
Site Map with Soil SaMple and UST SysteM Loco tlons
T o.ylor's BP
10005 Six Forks Roo.d
Ro.leigh, \Jake County, North Carolina
CAD FILE: I PREP. BY: I REV. BY:
cashsiteMap FGT TR'W
£ost Coast
£nvironf2ental. P.A,
37tr.l ..Jt.nctlon Boul tt vord
Rol~loh. North Corollno 27603
[phone] Fox• (919) 772-0~68
DATE: I PROJECT NO.
01/10/07
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Site Check (I SA NCAC 21\' 0.0603(b))
Taylor's BP
10005 Six Forks Road, Raleigh, Wake County, Nonh Carolina
Section B
Tables
E11st Coa.\1 Em•iro11mema/, I'.A.
3709 Junction Blnl.
Raleigh, North Carolina 27603
l'lionc: [phone] FAX: (9\9) 772-04(>8
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Analytical Method > 8260 8260
Sample Contaminant of
lD Concern>
Date Sample 0 ~ . ., 0
Collected Depth 2 c 0
m/ddlyy (ft) u ' c 0
0 .0 c >, 0 >. " ~ .0 " 0
2 0
"' P·1 1/3/07 8' ND ND
P·2 1/3/07 12' 1.7 23
Soil to Groundwater MSCC 0.02 3.3
Residential MSCC 85 626
Industrial/Conunercial MSCC 763 16350
Results arc in mg/kg
Table I
Summary of Analytical Data-Soil
EPA Method 8260
Taylor's BP
10005 Six Forks Road
Raleigh. Wake County, North Carolina
8260 8260 8260 8260 8260
0 c 0
0 c
N 0 0 c N c 0 c 0 "' 0 N "' c >, 0 0 0 >. c c "" c. ~ 0 0 N 0 >, " 0 " c c. " 0 0 ~ 0 0. iii ' " en f--
22 400 170 19 100
33 720 300 44 170
0.0056 7.3 4.6 1.7 1.7
18 3200 1.560 1,564 626
164 82 000 40 000 40 880 16,350
Bold results indicate excccdcnce of Soil to Groundwater MSCC
Bold and shaded results indicate cxccedencc of Residential MSCC
ND-Not Detected
8260 8260 8260 8260 8260 8260
" " 0 c
§ c " 0 " 0 ' ' 0 c c c 0 3 0 0 f-N "' "' >, § 0 0 f->, -"" c ,., ~ -" ~ -5 0 .,
" " >, • 0
' 0 ~ ~ § ' £ " ~ ' .,. ' c. • 0 • c
~ .. N .. "' • >,
' " . " 6. ' z >< -f--f-c
NO 560 5.4 35 98 910
320 960 12 98 170 1700
7.3 7.5 NRS 4.3 0.58 5
782 782 iSRS 626 313 3 129
20,440 20.440 NRS 16,350 8,176 81 760
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Results are in mg!kg
Date
m/dd/yy.'
+
--' ' --,
Table l (Continued)
Summary of Analytical Data-Soil
MADEP-VPH
Taylor's BP
10005 Six Forks Road
Raleigh, Wake County, North Carolina
·"'"'' ,-,--_,'
:m>---"''
Sample Depth (ll)
VPH
72
939
Bold results indicate excccdcnce of Soil to Groundwater MSCC
Bold and shaded results indicate cxccedencc of Residential MSCC
<
N
u
B
VPH
3,300
9,386
" -~ " E 2 <
0
VPH
34
469
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Analytical Method >
Sample Contaminant of Concern >
ID Date
Collected
(m/dd/yy)
SS-1 1/3/07
SS-2 1/3/07
SS-3 1/3/07
SS-4 1/3/07
SS-5 1/3/07
SS-6 1/3/07
SS-7 1/3/07
SS-8 1/3/07
SS-9 1/3/07
L-1 1/3/07
L-2 1/3/07
L-3 1/3/07
L-4 1/3/07
L-5 113/07
P-1 1/3/07
P-2 1/3/07
P-3 1/3/07
NCDENR Action Level
Results arc in mg/kg
NO -i\'ot Detected
NT-Not Tested
Sample
Depth (ft)
15' -16'
15' -16'
15' -16'
15' -16'
15'-16'
15' -16'
15'-16'
15'-16'
15'-16'
3'-4'
3'-4'
3'-4'
3'-4'
3'-4'
7'-8'
II' -12'
7'-8'
Table 1 (Continued)
Summary of Analytical Data-Soil
TPH
Taylor's BP
10005 Six Forks Road
Raleigh, Wake County, North Carolina
EPA 8015 EPA 8015
w/5030 w/3550
c -0 ·-·a 0-0. u 0. 0 000 co:.= 0 0 0 u
·-<r:. :.= </) =-= CJ ·-:-:: 0 ·-oo "'o co~ ~
~:I: -§,:I: 00. ·-0. ...Jl-0:!-
ND NT
ND NT
ND NT
ND NT
ND NT
ND 51
ND 63
ND 30
ND 37
ND NT
ND NT
ND NT
ND NT
ND NT
NT NT
13,000 NT
ND 33
10 40
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Site Check (I SA NCAC 2N 0.0603(b))
Taylor's BP
10005 Six Forks Road, Raleigh, Wake County, North Carolina
Section C
Laboratory Reports
Ea.\/ Cmnt Etn·irollmentaf, P.A.
3709 Junction Blvd.
Raleigh. 1\'orth Carolina 27603
Phone: [phone]l! FAX: [phone]l!
I SG$
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Ms. Diane Byrd
CompuChem
501 Madison Ave.
Cary NC 27513
Report Number: G349-201
Client Project: Cashs BP
Dear Ms. Byrd:
Enclosed arc the results of the analytical services performed under the referenced
project. The samples are certified to meet the requirements of the National
Environmental Laboratory Accreditation Conference Standards. Copies of this report
and supporting data will be retained in our files for a period of five years in the event
they are required for future reference. Any samples submitted to our laboratory will
will be retained for a maximum of thirty (30) days from the date of this report unless
other arrangements are requested.
If there are any questions about the report or the services performed during this project,
please call SGS/Paradigm at [phone]. We will be happy to answer any questions
or concerns which you may have.
Thank you for using SGS/Paradigm Analytical Labs for your analytical services. We look
forward to working with you again on any additional analytical needs which you may have.
Sincerely,
SGS/Paradigm Analytical Laboratories, Inc.
· · ~""£J, ---~~' 1a1tre}!!Y]l_ Laboratory D1rector '-tJ
J. Patrick Weaver
I SG$_
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VPH (Aiiphatics/Aromatics) Laboratory Reporting Form
Client Name: Com uChem
Project Name: ~c,a~s!.!hs~Bc:P __________________ _
Sample Information and Analytical Results
Sample Identification P-1
Sample Matrix Soil
Collection Option (for Soil)' 2
Date Collected 01/03/07
Date Received 01/05/07
Date Extracted 01/03/07
Date Analyzed 01/18/07
Dry Weight 82
Dilution Factor 20
C5-C8 Aliphatics*" 1800 lmo/Kol
Cg-C12 Allphatics'* 4100 lmo/Kol
C9-C10 Aromatics•• 2400imo/Kol
Surrogate% Recovery-PID 160* ..
Surrogate %Recovery-FlO 230* ..
• = Option 1 "Established fill Une on vial, Option 2 =Sampling Device/Brand, or Option 3 c Field weight of soiL •• = Excludes any surrogates or internal standards. •··= High surrogate recovery due to matrix Interference
Lab Info: g349-201-1a Reviewed By: h
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VPH (AIIphatlcs/Aromatlcs) Laboratory Reporting Form
Client Name: Com uChem
Project Name: ~C~•::o•o:h::.s_o:B:;_P __________________ _
Sample Information and Analytical Results
Sample Identification P-2
Sample Matrix Soil
Collection Option (for Soil)" 2
Date Collected 01103/07
Date Received 01105107
Date Extracted 01/03107
Date Analyzed 01110107
Dry Weight 77
Dilution Factor 20
C5-Ca AHphatics .. 3400_lr11glf(gj_
C9-C12 Aliphatics** 6200 (rT1glf<gJ_
C9-C10 Aromatics** 4900 (mg/Kg)
Surrogate% Recovery-PID 220* ..
Surrogate % Recovery-FlO 220***
• = Option 1 = Established fill line on vial, Option 2 " Sampling Device/Brand, or Option 3 = Field weight of soil. •• = Excludes any surrogates or lntemal standards .
... = High surrogate recovery due to matrix Interference
Lab Info: g349-201-2a Reviewed By: W.U..
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Attachment 2
VPH Laboratory Reporting Form
Calibration and QA/QC Information
FID Initial Calioration Date: 01/03/07
Calibration Ranges and Limits
Range
MUL (0711512004)
(~g/L)
C5-C8 Aliphatics 4.4
C9·C12 Aliphatics 3.4
C9-C10 Aromatics 0.13
Calibration Concentration Levels
Range Levels (~g/L)
40
C5-CB 1000
Aliphatics 2000
3000
4000
10
Cg·C12 250
Aliphatics 500
750
1000
10
C9-C10 250
Aromatics 500
750
1000
Calibration Check Date: 01/18/07
Calibration Check
Range Levels (~g/L)
(mg/Kg)
C5-C 8 Aliphatics 2000 200
C9-C12 Aliphatics 500 50
C9-C10 Aromatics 500 50
MDL"' Method Detection Limit
ML = Minimum Limit
PID Initial Calibration Date: 01/03/07
ML KL
(~g/L) (~g/L) (mg/Kg)
14 100 10
11 100 10
0.41 100 10
%RSDorCCC Method of Quantitation
9.7 Calibration Factor
15.00 Calibration Factor
23.10 Calibration Factor
RPD
5.6
3.9
4.5
RPD = Relative Percent Difference
%RSD = Percent Relative Standard Deviation
RL = Reportable Limit CCC " Correlation Coefficient of Curve
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SG$
Attachment 2
VPH Laboratory Reporting Form
Calibration and QA/QC Information
FlO Initial Calibration Date: 01i03i07
Calibration Ranges and Limits
Range IVJUL {07/1512004)
(~giL)
C5-C8 Aliphatics 4.4
C9-C12 Aliphatics 3.4
C9-C10 Aromatics 0.13
Calibration Concentration Levels
Range Levels (~gil)
40
C5·Ce 1000
Aliphatics 2000
3000
4000
10
Ce-Ct2 250
Aliphatics 500
750
1000
10
Ca-Cto 250
Aromatics 500
750
1000
Calibration Check Date: 01110107
Calibration Check
Range Levels (~giL)
(mg/Kg)
C5-C8 Aliphatics 2000 200
C9-C12 Aliphatics 500 50
C9-C10 Aromatics 500 50
MDL = Method Detection Limit
ML = Minimum Limit
Rl = Reportable Limit
PIO Initial Calibration Date: 01i03i07
ML RL
(~giL) (~giL) (mgiKg)
14 100 10
11 100 10
0.41 100 10
%RSDorCCC Method of Quantitatlon
9.7 Calibration Factor
15.00 Calibration Factor
23.10 Calibration Factor
RPD
5.1
0.4
2.4
RPD ,. Relative Percent Difference
%RSD = Percent Relative Standard Deviation
CCC" Correlation Coefficient of Curve
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List of Reporting Abbreviations
and Data Qualifiers
B = Compound also detected in batch blank
BQL = Below Quantitation Limit (RL or MDL)
OF = Dilution Factor
Dup = Duplicate
D = Detected, but RPD is > 40% between results in dual column method.
E = Estimated concentration, exceeds calibration range.
J = Estimated concentration, below calibration range and above MDL
LCS(O) =laboratory Control Spike (Duplicate)
MDL = Method Detection limit
MS(D) = Matrix Spike (Duplicate)
POL = Practical Quantitation limit
I RL = Reporting Limit
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RPD = Relative Percent Difference
mg/kg = milligram per kilogram, ppm, parts per million
ug/kg = micrograms per kilogram, ppb, parts per billion
mg/L = milligram per liter, ppm, parts per million
ug/l = micrograms per liter, ppb, parts per billion
% Rec = Percent Recovery
% soilds = Percent Solids
Special Notes:
1) Metals and mercury samples are digested with a hot block, see the standard
operating procedure document for details.
2) Uncertainty for all reported data is tess than or equal to 30 percent.
Ml34.030606.3
____ liiillliiiiiil _________ _
COMPUCHEM
a division of Liberty Alllll)·tical Corp.
501 Madison Avenue
Cary, NC 27513
q .?'"!"'(-U) I
SUBCONTRACT CHAIN-OF-CUSTODY RECORD
c.~~·r~'" oP B "' r-
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(919) ' X · t91Sl 379-LI{J::, ~q
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#1 Received by:(sig) Date: 1#2 Received n. ll<fC'] #2 Receoed by <•lg)
Name: Time: Name:
Note (1) If "N"Iab snould balch samples to awa•t remarnder of proJect· maximiZing batch srze and m•n•mrzmg OC ral!o. •I "Y" lab snould begrn proceSSIIlg batches now.
Note (21 Samples snoold t:oe stored 60 days ai'ter date report ma•led at no e><tra charge
Nole (31 All lab cop res of data should tle retarned for a mimmum of 3 years.
Note (4) Please cal poml-of-con:act to verify receopt of samples.
Name:
T-TCLP
S-SW-646
~-~~ _600-series
Remarks I Comments
(see Noles 2 & 3)
eha'll .,u tl e-mo.i 1
c 'd;-;.jp.
. J _"C
Revision 0 2-10-99
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CompuChcm
a division of Uberty Analytical Curp.
12-Jan-07
TOM WILL
EAST COAST ENVIRONMENTAL
3709 JUNCTION BLVD.
RALEIGH, NC 27603
Subject:
Report of Data-Project CASH'S BP
Attn.: TOM WILL
Workorder: 12000
Enclosed arc the results of analytical work perfonned in accordance with the referenced
account number.
This report covers sample(s) appearing on the attached listing.
Thank you for selecting CompuChem for your sample analysis. If you should have
questions or require additional analytical services, please contact your representative at
1-800-833-5097.
;-"*""<'rely,
Attachment
TOTAL NUMBER
OF PAGES __
SOl Madison Avenue, Cary, NC 27513 Tel: [phone] r·ax: 919-379-4050
CHAIN OF CUSTODY ~CompuChem 501 Madi<;on Ave. = a division of Liberty Analytical Corp. Cary. NC 2751) ·~~~-~~~~%1~a~~Y~-~~~
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Samples Jl""'::l t\0 days afler ~.;,j ~~ oo extra charge. wiiiio & v.•~ oopy lo""' .p;;, • -------------------
~CompuChem == a division or Liberty Analytical Corp.
CHAIN OF CUSTODY
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FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
P-1
Lab Name: COMPUCHEM Method: 826GB
Lab Code: LIBRTY Case No.: SAS No.' SDG No. ' 12000
Matrix: (soil/water) SOIL Lab Sample ID: 1200016
Sample wt/vol: S.SB(g/mL) G Lab File ID: 1200016A59
Level: (1ow/med) MED
%Moisture: not dec. 18
GC Column: ZB-624 IDo 0.32 (mm)
Date Received: 01/04/07
Date Analyzed: 01/10/07
Dilution Factor: 1.0
Soil Extract Volume: ( 5000} (ul) Soil Aliquot Volume: 25(ul)
CONCENTRATION UNITSo
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
75-71-8---------Dichlorodifluorornethane 1090 u
74-87-3---------Chloromethane 1090 u
75-01-4---------Vinyl Chloride 1090 u
74-83-9---------Bromomethane 1090 u
75-00-3---------Chloroethane 1090 u
75-69-4---------Trichlorofluoromethane 1090 u
75-35-4---------1,1-Dichloroethene 1090 u
75-09-2---------Methylene Chloride 1090 u
156-60-5--------trans-1,2-Dichloroethene 1090 u
1634-04-4-------Methyl-tert-butyl ether --1090 u
75-34-3---------1,1-Dichloroethane 1090 u
108-20-3--------Isopropyl ether 1090 u
594-20-7--------2,2-Dichloropropane 1090 u
156-59-2--------cis-1,2-Dichloroethene 1090 u
74-97-5---------Bromochloromethane 1090 u
67-66-3---------Chloroform 1090 u
71-55-6---------1,1,1-Trichloroethane 1090 u
56-23-5---------Carbon Tetrachloride 1090 u
563-58-6--------1,1-dichloropropene 1090 u
71-43-2---------Benzene 22000
107-06-2--------1,2-Dichloroethane 1090 u
79-01-6---------Trichloroethene 1090 u
78-87-5---------1,2-Dichloropropane 1090 u
74-95-3---------Dibromomethane 1090 u
75-27-4---------Bromodichloromethane 1090 u
108-88-3--------Toluene 240000 E
79-00-5---------1,1,2-Trichloroethane 1090 u
127-18-4--------Tetrachloroethene 1090 u
142-28-9--------1,3-Dichloropropane 1090 u
124-48-1--------Dibromochloromethane 1090 u
106-93-4--------1,2-Dibromoethane 1090 u
108-90-7--------Chlorobenzene 1090 u
630-20-6--------1,1,1,2-Tetrachloroethane 1090 u --
FORM I VOA
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FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
P-1
Lab Name: COMPUCHEM Method: 82608
Lab Code: LIBRTY Case No.: SAS No.: SDG No., 12000
Matrix: {soil/water) SOIL Lab Sample ID: 1200016
Sample wt/vol' 5. 58 (g/mL) G Lab File ID: 1200016A59
Level: (low/med) MED
%Moisture: not dec. 18
Date Received: 01/04/07
Date Analyzed: 01/10/07
GC Column: ZB-624 ro, 0.32 (mml Dilution Factor: 1.0
Soil Extract Volume: ( 5000) (ul) soil Aliquot Volume: 25(ul)
CONCENTRATION UNITS'
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
100-41-4--------Ethylbenzene 130000 E
100-42-5--------Styrene 1090 u
75-25-2---------Bromoform 1090 u
98-82-8---------Isopropyl Benzene 19000
108-86-1--------Bromobenzene 1090 u
96-18-4---------1,2,3-Trichloropropane 1090 u
79-34-5---------1,1,2,2-Tetrachloroethane 1090 u
103-65-1--------n-Propyl Benzene ---75000 E
95-49-8---------2-Chlorotoluene 1090 u
106-43-4--------4-Chlorotoluene 1090 u
108-67-8--------1,3,5-Trimethyl Benzene 1090 u
98-06-6---------tert-Butyl Benzene 1090 u
95-63-6---------1,2,4-Trimethyl Benzene 280000 E
135-98-8--------sec-Butyl Benzene 1090 u
541-73-1--------1,3-Dichlorobenzene 1090 u
106-46-7--------1,4-Dichlorobenzene 1090 u
99-87-6---------p-Isopropyl Toluene 5400
95-50-1---------1,2-Dichlorobenzene 1090 u
104-51-8--------n-Butyl Benzene 35000
96-12-8---------1,2-D~bromo-3-Chloropropane 1090 u
120-82-1--------1,2,4-Trichlorobenzene ~ 1090 u
87-68-3---------Hexachlorobutadiene 1090 u
91-20-3---------Naphthalene 81000 E
87-61-6------1,2,3 Trichlorobenzene 1090 u
1330-20-7 ---Xylene (total) 520000 E
FORM I VOA
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FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
P-1DL
Lab Name: COMPUCHEM Method: 8260B
Lab Code: LIBRTY Case No.: SAS No.: SDG No.: 12000
Matrix: (soil/water} SOIL Lab Sample ID: 1200016
Sample wt/vol: 5. 58 (g/mL) G Lab File ID: 1200016D2A59
Level: llow/med) MED
%Moisture: not dec. 18
Date Received: 01/04/07
Date Analyzed, 01/10/07
GC Column: ZB-624 ID' 0.32 (mm) Dilution Factor: 1.0
Soil Extract Volume: ( 5000) (ul) Soil Aliquot Volume:
CAS NO. COMPOUND
CONCENTRATION UNITS,
(ug/L or ug/Kg) UG/KG
75-71-8---------Dichlorodifluoromethane 27300
74-87-3---------Chloromethane 27300
75-01-4---------Vinyl Chloride 27300
74-83-9---------Bromomethane 27300
75-00-3---------Chloroethane 27300
75-69-4---------Trichlorofluoromethane 27300
75-35-4---------1,1-Dichloroethene 27300
75-09-2---------Methylene Chloride 27300
156-60-5--------trans-1,2-Dichloroethene 27300
1634-04-4-------Methyl-tert-butyl ether --27300
75-34-3---------1,1-Dichloroethane 27300
108-20-3--------Isopropyl ether 27300
594-20-7--------2,2-Dichloropropane 27300
156-59-2--------cis-1,2-Dichloroethene 27300
74-97-5---------Bromochloromethane 27300
67-66-3---------Chloroform 27300
71-55-6---------1,1,1-Trichloroethane 27300
56-23-5---------Carbon Tetrachloride 27300
563-58-6--------1,1-dichloropropene 27300
71-43-2---------Benzene 30000
107-06-2-------.-1,2-Dichloroethane 27300
79-01-6---------Trichloroethene 27300
78-87-5---------1,2-Dichloropropane 27300
74-95-3---------Dibromomethane 27300
u
u
u
u
u u u u u u u u
u
u
u
u
u u u
D u u
u
u
75-27-4---------Bromodichloromethane 27300 ~ 108-88-3--------Toluene 400000
79-00-5---------1,1,2-Trichloroethane 27300 u
127-18-4--------Tetrachloroethene 27300 u
142-28-9--------1,3-Dichloropropane 27300 u
124-48-1--------Dibromochloromethane 27300 u
106-93-4--------1,2-Dibromoethane 27300 u
108-90-7--------Chlorobenzene 27300 u
630-20-6--------1,1,1,2-Tetrachioroethane __ 27300 u
FORM I VOA
Q
1(ul)
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FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
P-1DL
Method: 82608
Lab File ID: 1200016D2A59
% Moisture: not dec. 18
GC Column: ZB-624 In, 0.32 (mm)
Date Received: 01/04/07
Date Analyzed: 01/10/07
Dilution Factor: 1.0
Soil Extract Volume: ( 5000) lull Soil Aliquot Volume:
CAS NO. COMPOUND
CONCENTRATION UNITS,
(ug/L or ug/Kg) UG/KG
100-41-4--------Ethylbenzene 170000
100-42-5--------Styrene 27300
75-25-2---------Bromoform 27300
98-82-8---------Isopropyl Benzene 27300
108-86-1--------Bromobenzene 27300
96-18-4---------1,2,3-Trichloropropane 27300
79-34-5---------1,1,2,2-Tetrachloroethane ___ 27300
103-65-1--------n-Propyl Benzene 100000
95-49-8---------2-Chlorotoluene 27300
106-43-4--------4-Chlorotoluene 27300
108-67-8--------1,3,5-Trimethyl Benzene 27300
98-06-6---------tert-Butyl Benzene 27300
95-63-6---------1,2,4-Tr1methyl Benzene 560000
135-98-8--------sec-Butyl Benzene 27300
541-73-1--------1,3-Dichlorobenzene 27300
106-46-7--------1,4-Dichlorobenzene 27300
99-87-6---------p-Isopropyl Toluene 27300
95-50-1---------1,2-Dichlorobenzene 27300
104-51-8--------n-Butyl Benzene 59000
96-12-8---------1,2-Dibromo-3-Chloropropane 27300
120-82-1--------1,2,4-Trichlorobenzene -27300
87-68-3---------Hexachlorobutadiene 27300
91-20-3---------Naphthalene 98000
87-61-6---------1,2,3-Trichlorobenzene 27300
1330-20-7-------Xylene I total) 910000
FORM I VOA
~ u
u
u
u
u
19 u
u
u
u
D
u
u
u
u
u
D
u u u
1)o u a
Q
1 (ul)
FORM 1 CLIENT SAMPLE NO. I VOLATILE ORGANICS ANALYSIS DATA SHEET
p. 2 I Lab Name: COMPUCHEM
Lab Code: LIBRTY
Method: 8260B
Case No.: I Matrix: (soil/water) SOIL
Sample wt/vol: I Level: (low/med)
5.36(g/mL) G
MED
% Moisture: not dec. 23
I GC Column: ZB-624 m, o.32 (mm)
50001 lull
SAS No.: SDG No. : 12002
Lab Sample ID: 1200201
Lab File ID: 1200201A59
Date Received: 01/04/07
Date Analyzed: 01/10/07
Dilution Factor: 1.0
Soil Aliquot Volume: 25 (ul I 1 Soil Extract Volume: (
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG Q
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75-71-8---------Dichlorodifluoromethane
74-87-3---------Chloromethane
75-01-4---------Vinyl Chloride
74-83-9---------Bromomethane
75-00-3---------Chloroethane
75-69-4.---------Trichlorofluoromethane
75-35-4---------1,1-Dichloroethene
75-09-2---------Methylene Chloride
156-60-5--------trans-1,2-Dichloroethene
1634-04-4-------Methyl-tert-butyl ether --
75-34-3---------1,1-Dichloroethane
108-20-3--------Isopropyl ether
594-20-7--------2,2-Dichloropropane
156-59-2--------cis-1,2-Dichloroethene
74-97-5---------Bromochloromethane
67-66-3---------Chloroform
71-55-6---------1,1,1-Trichloroethane
56-23-5---------Carbon Tetrachloride
563-58-6--------1,1-dichloropropene
71-43-2---------Benzene
107-06-2--------1,2-Dicfiloroethane
79-01-6---------Trichloroethene
78-87-5---------1,2-Dichloropropane
74-95-3---------Dibromomethane
75-27-4---------Bromodichloromethane
108-88-3--------Toluene
79-00-5---------1,1,2-Trichloroethane
127-18-4--------Tetrachloroethene
142-28-9--------1,3-Dichloropropane
124-48-1--------Dibromochloromethane
106-93-4--------1,2-Dibromoethane
108-90-7--------Chlorobenzene
63o'-20-6--------1,1,1,2-TetracfiioroetFlane __
FORM .L VuA
1200 u
1200 u
1200 u
1200 u
1200 u
1200 u
1200 u
1700
1200 u
1200 u
1200 u
1200 u
1200 u
1200 u
1200 u
1200 u
1200 u
1200 u
1200 u
33000
1200 u
1200 u
1200 u
1200 u
1200 u
440000 E
1200 u
1200 u
1200 u
1200 u
1200 u
1200 u
1200 u
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FORM 1
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: COMPUCHEM
Lab Code: LIBRTY
Matrix: (soil/water)
Sample wt/vol:
Level: I low/med)
Case No.:
SOIL
5.36(g/mL) G
MED
Method: 82608
SAS No.:
CLIENT SAMPLE NO.
P-2
SDG No.: 12002
%Moisture: not dec. 23 I GC Column: ZB-624 ID: 0.32 (mm)
Lab Sample ID: 1200201
Lab File ID: 1200201A59
Date Received: 01/04/07
Date Analyzed: 01/10/07
Dilution Factor: 1.0
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Soil Extract Volume: ( 5000) (ul) Soil Aliquot Volume:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
100-41-4--------Ethylbenzene 280000
100-42-5--------Styrene 1200
75-25-2---------Bromoform 1200
98-82-8---------Isopropyl Benzene 44000
108-86-1--------Bromobenzene 1200
96-18-4---------1,2,3-Trichloropropane 1200
79-34-5---------1,1,2,2-Tetrachloroethane 1200
103-65-1--------n-Propyl Benzene ---150000
95-49-8---------2-Chlorotoluene 1200
106-43-4--------4-Chlorotoluene 1200
108-67-8--------1,3,5-Trimethyl Benzene 1200
98-06-6---------tert-Butyl Benzene 1200
95-63-6---------1,2,4-Trimethyl Benzene 430000
135-98-8--------sec-Butyl Benzene 23000
541-73-1--------1,3-Dichlorobenzene 1200
106-46-7--------1,4-Dichlorobenzene 1200
99-87-6---------p-Isopropyl Toluene 12000
95-50-1---------1,2-Dichlorobenzene 1200
104-51-8--------n-Butyl Benzene 70000
96-12-8---------1,2-Dibromo-3-Chloropropane 1200
120-82-1--------1,2,4-Trichlorobenzene --1200
87-68-3---------Hexachlorobutadiene 1200
91-20-3---------Naphthalene 220000
87-61-6---------1,2,3-Trichlorobenzene 1200
1330-20-7-------Xylene (total) 880000
FORM I VOA
25 lul)
Q
E u u
u
u
u
E
u u u
u
E
u
u
u
E
u
u
u
E u
E
I FORM 1
VOLATILE ORGANICS ANALYSIS DATA SHEET
CLIENT SAMPLE NO.
I Lab Name: COMPUCHEM Method: 82608
Lab Code' LIBRTY Case No.: SAS No., SDG No. ' 12002
I Matrix: (soil/water) SOIL Lab Sample ID: 1200201
Sample wt/vol: 5. 36 (g/mL) G
I Level: (low/med) MED
% Moisture: not dec. 23 I GC Column: ZB-624 m, o.32 (mm)
Lab File ID: 1200201D2A59
Date Received: 01/04/07
Date Analyzed: 01/10/07
Dilution Factor: 1.0
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Soil Extract Volume: { 5000) (u1) Soil Aliquot Volume:
CAS NO. COMPOUND
CONCENTRATION UNITS'
(ug/L or ug/Kg) UG/KG
75-71-8---------Dichlorodifluoromethane 40000
74-87-3---------Chloromethane 40000
75-01-4---------Vinyl Chloride 40000
74-83-9---------Bromomethane 40000
75-00-3---------Chloroethane 40000
75-69-4---------Trichlorofluoromethane 40000
75-35-4---------1,1-Dichloroethene 40000
75-09-2---------Methylene Chloride 40000
156-60-5--------trans-1 2-Dichloroethene 40000
1634-04-4-------Methyl-tert-butyl ether ----40000
75-34-3---------1,1-Dichloroethane 40000
108-20-3--------Isopropyl ether 40000
594-20-7--------2,2-Dichloropropane 40000
156-59-2--------cis-1,2-Dichloroethene 40000
74-97-5---------Bromochloromethane 40000
67-66-3---------Chloroform 40000
71-55-6---------1,1,1-Trichloroethane 40000
56-23-5---------carbon Tetrachloride 40000
563-58-6--------1,1-dichloropropene 40000
71-43-2---------Benzene 40000
!07-06-2--------1,2-Dichloroethane 40000
79-01-6---------Trichloroethene 40000
78-87-5---------1,2-Dichloropropane 40000
74-95-3---------Dibromomethane 40000
75-27-4---------Bromodichloromethane 40000
108-88-3--------Toluene 720000
79-00-5---------1,1,2-Trichloroethane 40000
127-18-4--------Tetrachloroethene 40000
142-28-9--------1,3-Dichloropropane 40000
124-48-1--------Dibromochloromethane 40000
106-93-4--------1,2-Dibromoethane 40000
108-90-7--------Chlorobenzene 40000
630-20-6--------1,1,1,2-TetracEioroethane 40000 ---
FuRM I VOA
l (ul I
Q
u
u
u
u u u u u u
u
u u u
u
u
u
u
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u
u u u u
u
fl1
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u u u
u
u u
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I
I
I
I
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I
I
I
I
I
I
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I
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I
I
FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
P-2DL
Lab Name: COMPUCHEM Method: 82608
Lab Code' LIBRTY Case No.: SAS No.' SDG No. ' 12002
Matrix: (soil/water) SOIL Lab Sample ID: 1200201
Sample wt/vol: 5. 36 (g/mL) G Lab File ID: 1200201D2A59
Level: (low/med) MED
% Moisture: not dec. 23
Date Received: 01/04/07
Date Analyzed: 01/10/07
Dilution Factor: 1.0 GC Column: ZB-624 m, 0. 32 (mm)
Soil Extract Volume: ( 5000) lull Soil Aliquot Volume:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
100-41-4--------Ethylbenzene 300000
100-42-5--------Styrene 40000
75-25-2---------Bromoform 40000
98-82-8---------Isopropyl Benzene 40000
108-86-1--------Bromobenzene 40000
96-18-4---------1,2,3-Trichloropropane 40000
79-34-5---------1,1,2,2-Tetrachloroethane 40000
103-65-1--------n-Propyl Benzene --170000
95-49-8---------2-Chlorotoluene 40000
106-43-4--------4-Chlorotoluene 40000
108-67-8--------1,3,5-Trimethyl Benzene 320000
98-06-6---------tert-Butyl Benzene 40000
95-63-6---------1,2,4-Trlmethyl Benzene 960000
135-98-8--------sec-Butyl Benzene 40000
541-73-1--------1,3-Dichlorobenzene 40000
106-46-7--------1,4-Dichlorobenzene 40000
99-87-6---------p-Isopropyl Toluene 40000
95-50-1---------1,2-Dichlorobenzene 40000
104-51-8--------n-Butyl Benzene 98000
96-12-8---------1,2-Dibromo-3-Chloropropane 40000
120-82-1--------1,2,4-Trichlorobenzene -40000
87-68-3---------Hexachlorobutadiene 40000
91-20-3---------Naphthalene 170000
87-61-6---------1,2,3-Trichlorobenzene 40000
1330-20-7-------Xylene (total) 1700000
FORM I VOA
;
u u
u u u
u p
u
u
D u ~ u u u u
0 u
u u ,.,.
u
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Q
1(ul)
FORM 1 CLIENT SAMPLE NO. I GC VOA ORGANICS ANALYSIS DATA SHEET
I Lab Name: COMPUCHEM
Lab Code, LIBRTY Case No.:
I Matrix: (soil/water) SOIL
Sample wt/vol: 5.6 (g/mL)
I Level: (low/med) MED
~Moisture: not dec. 24 I GC Column: RTX-VOLATILES ID: 0.53
1 Soil Extract volume: ( 5000) (ul)
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
9999-99-7-------Gasoline
G
L-1
Contract: 8015B GRO
SAS No.' SDG No. , 12000
(mm)
Lab Sample ID: 1200011
Lab File ID: 055Tl2000ll
Date Received: 01/04/07
Date Analyzed: 01/09/07
Dilution Factor: 1.0
Soil Aliquot Volume: 2SO(uL)
CONCENTRATION UNITS:
(ug/L or ug/Kg) MG/KG Q
5.9l_u __
I
I
FORM I GC VOA
I
I
FORM 1 CLIENT SAMPLE NO. I GC VOA ORGANICS ANALYSIS DATA SHEET
I Lab Name : COMPUCHEM
Lab Code, LIBRTY Case No.: I Matrix: (soil/water) SOIL
Sample wt/vol: 5.6 (g/mLI G I Level: (low/med) MED
% Moisture: not dec. 18
I GC Column: RTX-VOLATILES ID: 0.53
I Soil Extract Volume: ( 5000) (ul)
CAS NO. COMPOUND
L-2
Contract: 8015B GRO
SAS No.: SDG No. : 12000
{mm)
Lab Sample ID: 1200012
Lab File ID: 056Tl200012
Date Received: 01/04/07
Date Analyzed' 01/09/07
Dilution Factor: 1.0
Soil Aliquot Volume: 250(uL)
CONCENTRATION UNITS'
(ug/L or ug/Kg) MG/KG Q
I 9999-99-7-------Gasoline ____________________ _
I
I
I
I
I
I
I
I
I
I
I
I
FORM I GC VOA
FORM 1 CLIENT SAMPLE NO. I GC VOA ORGANICS ANALYSIS DATA SHEET
I Lab Name: COMPUCHEM
Lab Code: LIBRTY Case No.:
I Matrix: (soil/water) SOIL
Sample wt/vol: 5.8 lg/mL)
I Level: (low/med) MED
1 % Moisture: not dec. 22
GC Column: RTX-VOLATILES ID: 0.53 I Soil Extract Volume: (
CAS NO.
5000) lull
COMPOUND
G
L-3
Contract: S015B GRO
SAS No.: SDG No.: 12000
(mm)
Lab Sample ID: 1200013
Lab File ID: 057Tl200013
Date Received: 01/04/07
Date Analyzed: 01/09/07
Dilution Factor: 1.0
Soil Aliquot Volume: 250(uL)
CONCENTRATION UNITS:
(ug/L or ug/Kg) MG/KG Q
I 9999-99-7-------Gasoline ____________________ _ 5. 5]u
I
I
I
I
I
I
I
I
I
I
I
I
---
FORM I GC VOA
FORM l CLIENT SAMPLE NO. I GC VOA ORGANICS ANALYSIS DATA SHEET
I Lab Name: COMPUCHEM
Lab Codeo LIBRTY Case No.:
I Matrix: (soil/water) SOIL
Sample wt/vol: 5.5 (g/mL)
I Level: (low/medl MED
% Moisture: not dec. 18 I GC Column: RTX-VOLATILES ID: 0.53
1 Soil Extract Volume: (
CAS NO.
5000) lull
COMPOUND
I
I
9999-99-7-------Gasoline
I
I
I
I
I
I
I
I
G
L-4
Contract: 8015B GRO
SAS No.' SDG No. ' 12000
lmml
Lab Sample ID: 1200014
Lab File ID: 058Tl200014
Date Received: 01/04/07
Date Analyzed: 01/09/07
Dilution Factor: 1.0
Soil Aliquot Volume: 2SO(uL)
CONCENTRATION UNITSo
(ug/L or ug/Kg) MG/KG Q
FORM I GC VOA
I
I
I
FORM 1 CLIENT SAMPLE NO. I GC VOA ORGANICS ANALYSIS DATA SHEET
I Lab Name: COMPUCHEM
Lab Code: LIBRTY Case No.:
I Matrix: (soil/water) SOIL
Sample wt/vol: 5.5 (g/mL)
I Level: llow/med) MED
% Moisture: not dec. 23 I GC Column: RTX-VOLATILES ID: 0.53
1 Soil Extract volume: (
CAS NO.
5000) (ul)
COMPOUND
I
I
I
I
I
I
I
I
I
I
9999-99-7-------Gasoline
G
L-5
Contract: 8015B GRO
SAS No.: SDG No.: 12000
(mm)
Lab Sample ID: 1200015
Lab File ID: 059Tl200015
Date Received: 01/04/07
Date Analyzed: 01/09/07
Dilution Factor: 1.0
Soil Aliquot Volume: 250(uL)
CONCENTRATION UNITS:
(ug/L or ug/Kg) MG/KG Q
FORM I GC VOA
I
I
I
I FORM 1
GC VOA ORGANICS ANALYSIS DATA SHEET
CLIENT SAMPLE NO.
I T.Jab Name: COMPUCHEM Contract: 8015B
Lab Code, LIBRTY Case No.: SAS No.: SDG No.: 12002 I Matrix: (soil/water) SOIL Lab Sample ID: 1200201
5. 0 (g/mL) G Sample wt/vol:
I % Moisture: 23 decanted: (Y/N) N
Extraction: I Concentrated Extract Volume:
(SepF/Cont/Sonc) P&T
5000(ul)
Lab File ID: 072Tl200201
Date Received: 01/04/07
Date Extracted:
Date Analyzed: 01/11/07
I lnj ection Volume:
GPC Cleanup: (Y/N) N
___ luLl Dilution Factor: 1.0
Sulfur Cleanup: (Y/Nl N
CONCENTRATION UNITS' I
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND (ug/L or ug/Kg) MG/KG Q
9999-99-7-------Gasoline ____________________________ r_3_o_o_ol=====
FORM I GC VOA
FORM 1 CLIENT SAMPLE NO. I GC VOA ORGANICS ANALYSIS DATA SHEET
I Lab Name: COMPUCHEM
Lab Code: LIBRTY Case No.:
I Matrix: (soil/water) SOIL
Sample wt/vol: 5.5 (g/mLI
I Level: (low/med} MED
% Moisture: not dec. 20 I GC Column: RTX-VOLATILES ID: 0.53
1 Soil Extract Volume: {
CAS NO.
5000) lull
COMPOUND
G
?-3
Contract: 8015B GRO
SAS No.: SDG No.: 12000
{mm)
Lab Sample ID: 1200010
Lab File ID: 049Tl200010
Date Received: 01/04/07
Date Analyzed: 01/08/07
Dilution Factor: 1.0
Soil Aliquot Volume: 250(uL)
CONCENTRATION UNITS:
(ug/L or ug/Kg) MG/KG Q
I 9999-99-7-------Gasoline ____________________ _
I
I
I
I
I
I
I
I
I
I
I
I
FORM I GC VOA
I
I
I
I
I
FORM 1 CLIENT SAMPLE NO.
GC VOA ORGANICS ANALYSIS DATA SHEET
Lab Name: COMPUCHEM
Lab Code: LIBRTY Case No.:
Matrix: (soil/water) SOIL
Sample wt/vol: 5.1 (g/mL)
Level: (low/med) MED
% Moisture: not dec. 21
GC Column: RTX-VOLATILES ID: 0.53
G
SS-1
Contract: 80158 GRO
SAS No.:
(mm)
SDG No.' 12000
Lab Sample ID: 1200001
Lab File ID: 040Tl200001
Date Received: 01/04/07
Date Analyzed: 01/08/07
Dilution Factor: 1.0 I Soil Extract volume: (
CAS NO.
5000) lull
COMPOUND
Soil Aliquot Volume: 2SO(uL)
CONCENTRATION UNITSo
(ug/L or ug/Kg) MG/KG Q
I
I
I
I
I
I
I
I
I
I
I
I
I
9999-99-7-------Gasoline ____________________ __ 6+ ---
FORM I GC VOA
I FORM 1
GC VOA ORGANICS ANALYSIS DATA SHEET
CLIENT SAMPLE NO.
I Lab Name: COMPUCHEM Contract: 8015B GRO
SS-2
Lab Code: LIBRTY Case No.: SAS No.: SDG No.: 12000
I Matrix: {soil/water) SOIL Lab Sample ID: 1200002
Sample wt/vol: 5.3 (g/mL) G
I Level: llow/med) MED
%Moisture: not dec. 16 I GC Column: RTX-VOLATILES ID: 0.53
Soil Extract Volume: { 5000) (ul) I
(mm)
Lab File ID: 041Tl200002
Date Received: 01/04/07
Date Analyzed: 01/08/07
Dilution Factor: 1.0
Soil Aliquot Volume: 250(uL)
I
I
I
I
I
I
I
I
I
I
I
I
I
CONCENTRATION UNITS,
CAS NO. COMPOUND (ug/L or ug/Kg) MG/KG Q
9999-99-7-------Gasoline ____________________ _
FORM I GC VOA
FORM 1 CLIENT SAMPLE NO. I GC VOA ORGANICS ANALYSIS DATA SHEET
I Lab Name: COMPUCHEM
Lab Code: LIBRTY Case No.:
I Matrix: {soil/water) SOIL
Sample wt/vol: 5.1 (g/mL)
I Level: (low/med) MED
~ Moisture: not dec. 24 I GC Column: RTX-VOLATILES ID: 0.53
I
I
I
I
I
I
I
I
I
I
I
Soil Extract Volume: { 5000) lull
CAS NO. COMPOUND
9999-99-7-------Gasoline
G
ss-3
Contract: 8015B GRO
SAS No.: SDG No.: 12000
(mm)
Lab Sample ID: 1200003
Lab File ID: 042Tl200003
Date Received: 01/04/07
Date Analyzed: 01/DB/07
Dilution Factor: 1.0
Soil Aliquot Volume: 250(uL)
CONCENTRATION UNITS:
(ug/L or ug/Kg) MG/KG Q
FORM I GC VOA
I
I
I
FORM 1 CLIENT SAMPLE NO. I GC VOA ORGANICS ANALYSIS DATA SHEET
I Lab Name: COMPUCHEM
Lab Code: LIBRTY Case No.:
I Matrix: (soil/water)
Sample wt/vol: I Level: llow/med)
SOIL
4.3 (g/mL) G
MED
~ Moisture: not dec. 15
I GC Column: RTX-VOLATILES ID: 0.53
1 Soil Extract Volume: (
CAS NO.
5000) (ul)
COMPOUND
SS-4
Contract: BOlSB GRO
SAS No.' SDG No., 12000
{mm)
Lab Sample ID: 1200004
Lab File ID: 043Tl200004
Date Received: 01/04/07
Date Analyzed: 01/08/07
Dilution Factor: 1.0
Soil Aliquot Volume: 2SO(uL)
CONCENTRATION UNITS,
(ug/L or ug/Kg) MG/KG Q
I 9999-99-7-------Gasoline ____________________ _ 6.8,U
I
I
I
I
I
I
I
I
I
I
I
I
--
FORM I GC VOA
FORM 1 CLIENT SAMPLE NO. I GC VOA ORGANICS ANALYSIS DATA SHEET
I Lab Name: COMPUCHEM
Lab Code' LIBRTY Case No.:
I Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 lg/mL)
I Level: llow/med) MED
' Moisture: not dec. 19 I •
GC Column: RTX-VOLATILES m, 0.53
1 Soil Extract Volume: { 5000) lull
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
9999-99-7-------Gasoline
G
SS-5
Contract: 8015B GRO
SAS No.: SDG No., 12000
(mm)
Lab Sample ID: 1200005
Lab File ID: 044Tl200005
Date Received: 01/04/07
Date Analyzed: 01/0B/07
Dilution Factor: 1.0
Soil Aliquot Volume: 2SO(uL)
CONCENTRATION UNITS'
(ug/L or ug/Kg) MG/KG Q
FORM I GC VOA
I
I
I
FORM 1 CLIENT SAMPLE NO. I GC VOA ORGANICS ANALYSIS DATA SHEET
I Lab Name: COMPUCHEM
Lab Code, LIBRTY Case No.:
I Matrix: (soil/water) SOIL
Sample wt/vol: 5.3 (g/mL)
I Level: (low/med) MED
% Moisture: not dec. 25
I GC Column: RTX-VOLATILES m, 0.53
1 Soil Extract Volume: (
CAS NO.
5000) (ul)
COMPOUND
I
I
I
I
I
I
I
I
I
I
9999-99-7-------Gasoline
G
SS-6
Contract: 8015B GRO
SAS No.' SDG No. ' 12000
(mm)
Lab Sample ID: 1200006
Lab File ID: 060Tl200006
Date Received: 01/04/07
Date Analyzed: 01/09/07
Dilution Factor: 1.0
Soil Aliquot Volume: 250(uL)
CONCENTRATION UNITS,
(ug/L or ug/Kg) MG/KG Q
ul_u __
FORM I GC VOA
I
I
I
FORM l CLIENT SAMPLE NO. I GC VOA ORGANICS ANALYSIS DATA SHEET
I Lab Name: COMPUCHEM
Lab Code: LIBRTY Case No.:
I Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL)
I Level: (low/med) MED
%Moisture: not dec. 21 I GC Column: RTX-VOLATILES ID: 0.53
1 Soil Extract Volume: (
CAS NO.
5000) (ul)
COMPOUND
I
I
I
I
I
I
I
I
I
I
9999-99-7-------Gasoline
G
SS-7
Contract: 801SB GRO
SAS No.: SDG No. : 12000
(mm)
Lab Sample ID: 1200007
Lab File ID: 046Tl200007
Date Received: 01/04/07
Date Analyzed: 01/08/07
Dilution Factor: 1.0
Soil Aliquot Volume: 2SO(uL)
CONCENTRATION UNITS:
(ug/L or ug/Kg) MG/KG Q
ul_u __ ,
FORM I GC VOA
I
I
I
FORM 1 CLIENT SAMPLE NO. I GC VOA ORGANICS ANALYSIS DATA SHEET
I Lab Name: COMPUCHEM
Lab Code: LIBRTY Case No.:
I Matrix: {soil/water) SOIL
Sample wt/vol: 5.6 (g/mL)
I Level: (low/med) MED
%Moisture: not dec. 16 I GC Column: RTX-VOLATILES ID: 0.53
1 Soil Extract Volume: ( 5000) lull
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
9999-99-7-------Gasoline
G
SS-8
Contract: 80158 GRO
SAS No.' SDG No.: 12000
(mm)
Lab Sample ID: 1200008
Lab File ID: 047Tl200008
Date Received: 01/04/07
Date Analyzed' 01/08/07
Dilution Factor: 1.0
Soil Aliquot Volume: 2SO(uL)
CONCENTRATION UNITS'
(ug/L or ug/Kg) MG/KG Q
s 3l_u __
I
I
FORM I GC VOA
I
I
FORM 1 CLIENT SAMPLE NO. I GC VOA ORGANICS ANALYSIS DATA SHEET
I Lab Name: COMPUCHEM Contract: 80158 GRO
ss-9
Lab Code' LIBRTY Case No.: SAS No.' SDG No., 12000
I Matrix: (soil/water) SOIL Lab Sample ID: 1200009
Sample wt/vol: 5.2 (g/mL) G
I Level: (low/med) MED
Lab File ID: 048T1200009
Date Received: 01/04/07
I %' Moisture: not dec. 19
GC Column: RTX-VOLATILES ID: 0.53
Date Analyzed: 01/08/07
(mm) Dilution Factor: 1.0
1 Soil Extract Volume: ( 5000) lull Soil Aliquot Volume: 250(uL)
CONCENTRATION UNITS,
CAS NO. COMPOUND (ug/L or ug/Kg) MG/KG Q
I 9999-99-7-------Gasoline
I
I
I
I
I
I
I
I
I
I
FORM I GC VOA
I
I
10 EPA SAMPLE NO. I GC EXTRACTABLE ORGANICS ANALYSIS DATA SHEET
I Lab Name: COMPUCHEM Contract: 80158 ORO
P-3
Lab Code: LIBRTY I SAS No.: SDG No.: 12000 Case No.:
Matrix: (soil/water) SOIL
I Sample wt/vol:
% Moisture: 20
20.0 (g/mL) G
Lab Sample ID: 1200010
Lab Pile ID:
decanted: (Y/N) N
I Concentrated Extract Volume: 1000 (uL)
Extraction: (SepF/Cont/Sonc) SONC
Date Received: 01/04/07
Date Extracted:Ol/08/07
Date Analyzed: 01/09/07 I Injection Volume: 1. 0 (uL) Dilution Factor: 1.0
I
I
I
I
I
I
I
I
I
I
I
I
I
GPC Cleanup: (Y/N) N
CAS NO. COMPOUND
Sulfur Cleanup: (Y/N) N
CONCENTRATION UNITS,
(ug/L or ug/Kg) MG/KG Q
~9~9~9~9~-~9~9~-~5~-~-~-~-~-~-~-~D~i~e~s~e~1~====================== _____________ 3_31-----
FORM I PEST
I
I
I
I
1D EPA SAMPLE NO.
GC EXTRACTABLE ORGANICS ANALYSIS DATA SHEET
SS-6
Lab Name: COMPUCHEM Contract: 80158 ORO
Lab Code: LIBRTY Case No.: SAS No.: SDG No.' 12000
Matrix: (soil/water) SOIL
Sample wt/vol: 20. 0 (g/mL) G
Lab Sample ID: 1200006
Lab Pile ID:
% Moisture: 25 decanted: (Y/N) N I Extraction:
Concentrated Extract Volume:
(SepF/Cont/Sonc) SONC
1000 (UL)
Date Received: 01/04/07
Date Extracted:Ol/OB/07
Date Analyzed: 01/08/07 I Injection Volume:
GPC Cleanup: (Y /N) N
I CAS NO.
1.0(uL)
pH'
COMPOUND
Dilution Factor: 1.0
Sulfur Cleanup, (Y/N) N
CONCENTRATION UNITS'
(ug/L or ug/Kg) MG/KG Q
I
I
_:9~9~9~9~-~9~9--~5------~---~-~-~D:i~e~s:e~l~==================== ____________ s_11-----
I
I
I
I
I
I
I
I
I
I
FORM I PEST
I lD
GC EXTRACTABLE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
I Lab Name: COMPUCHEM Contract: 8015B ORO
SS-7
I Lab Code: LIBRTY Case No.:
Matrix: (soil/water) SOIL
SAS No.: SDG No.: 12000
I Sample wt/vol:
% Moisture: 21
20.0 (g/mL) G
decanted, (Y/N) N
Lab Sample ID: 1200007
Lab File ID:
Date Received: 01/04/07
Date Extracted:Ol/08/07
Date Analyzed: 01/08/07
I Extraction: (SepF/Cont/Sonc) SONC
Concentrated Extract Volume: I Injection Volume: 1. 0 (uL)
GPC Cleanup: (Y/N) N
I CAS NO. COMPOUND
1000 (uL)
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) N
CONCENTRATION UNITS'
(ug/L or ug/Kg) MG/KG Q
I
I
~99~9~9~-~9~9~-5~-~-~-~-~-~-~-D:l~-e~s:e~l~===================== ------------6~3~-----1
I
I
I
I
I
I
I
I
I
I
FORM I PEST
I
I
I
I
lD EPA SAMPLE NO.
GC EXTRACTABLE ORGANICS ANALYSIS DATA SHEET
Lab Name: COMPUCHEM
Lab Code: LIBRTY
Matrix: (soil/water)
Sampl_e wt/vol:
% Moisture: 16
SS-8
Contract: 8015B ORO
Case No.:
SOIL
20.0 (g/mL) G
decanted, (Y/N) N
SAS No., SDG No., 12000
Lab Sample ID: 1200008
Lab File ID:
I Extraction: (SepF/Cont/Sonc) SONC
Concentrated Extract Volume: lOOO(uL)
Date Received: 01/04/07
Date Extracted:Ol/08/07
Date Analyzed: 01/08/07 I Injection Volume:
GPC Cleanup: (Y/N) N
I CAS NO.
1. 0 (uL)
pH,
COMPOUND
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) N
CONCENTRATION UNITS,
(ug/L or ug/Kg) MG/KG Q
I
I
~-~9~9~9~9--~9~9--~5~---_-_-__ -_-_-:D:i:e:s~e~l~====================== _____________ 3_o]=====
I
I
I
I
I
I
I
I
I
I
FORM I PEST
I
I
I
I
I
1D EPA SAMPLE NO.
GC EXTRACTABLE ORGANICS ANALYSIS DATA SHEET
SS-9
Lab Name: COMPUCHEM Contract: 8015B ORO
Lab Code: LIBRTY
Matrix: (soil/water)
Sample wt/vol:
%Moisture: 19
Case No.:
SOIL,
20.0 {g/mL) G
decantedo {Y/N) N
Extraction: (SepF/Cont/Sonc) SONC
SAS No.:
Concentrated Extract Volume: 1000{uL)
SDG No. , 12000
Lab Sample ID: 1200009
Lab File ID:
Date Received: 01/04/07
Date Extracted:Ol/08/07
Date Analyzed: 01/08/07 I Injection Volume: l.O{uL) Dilution Factor: 1.0
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GPC Cleanup: {Y/N) N pHo
CAS NO. COMPOUND
Sulfur Cleanup: (Y/N) N
CONCENTRATION UNITS:
{ug/L or ug/Kg) MG/KG Q
-=9~9~9~9~·~9~9~--5~·-·_·_·_·_·_·~D~i~e~s~e~1~====================== _____________ 3_71=====
FORM I PEST