RA-958_6350_CA_MRP_20080304_CAP IMPLEMENTATION

ex
Companies, LLC
"Wfiere 'Exce{{ence .'Meets 'Yaiue"
March 4, 2008
Ms. Caroline E. Davenport
North Carolina Department of Environment and Natural Resources
Division of Waste Management
Unde~·grotmd Storage Tank Section
1628 Mail Service Center
Raleigh, NC 27699
RE: CAP Implementation Monitoring Report
Short Stop
300 W. Main Street, Carrboro
Oa·ange County
Incident Number: 6350
Risk Classification: High
Ranking: H230D
Dear Ms. Davenport:
6711 Peters Creek Road
Suite 201
Roanoke, VA 24019
Telephone: [phone]
Facsimile: 540-563-4921
Enclosed please fmd one copy of the CAP Implementation Groundwater Monitoring Report
completed by Apex Companies, LLC on behalf of Abercrombie Oil Company, Inc. for the
referenced site. If you have any questions regarding the enclosed material, or if additional
material is required, please feel free to contact me at [phone].
Sincerely,
'IZ~
RobertS. Wagner
Project Manager
Enclosure
cc: Mr. Jerry Douglas, Envirorunental Coordinator
Abercrombie Oil Company, Inc.
-<¥ Environmental -<¥ Engineering -<¥ Water Resources ..q,-Industrial Hygiene -<¥
-<¥ Facility Services ~ Construction Services ~
MONITORING REPORT-DATES
REPORT J ~ 0A{J
MONITORING EVENT ------
RECEIPT ~I (£__1) g~~~sEEN,I 1ifiiK
REVIEWER e,A ~
MONITORING REPORT -INFORMATION
INCIDENT NAME ? Hp K. r $ r o P -
lr /36-I{C.~onf.>i€ o iL
INCIDENTJI. /.t: 3!? fP
RANK tL_z-,ttD RISK--'-~~~--
COUNTY ,...;;0:....;;[=--,.-------
MANAGER C.. & Q
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ex
Companies, LLC
"Wiiere 'Exce{(ence :Meets \la(ue"
CAP IMPLEMENTATION
MONITORING REPORT
Short Stop
300 W. Main Street
Carrboro, North Carolina
Incident Number: 6350
Submitted To:
Ms. Caroline E. Davenport
6711 Peters Creek Road
Suite 201
Roanoke, VA 24019
Telephone: [phone]
Facsimile: 540-563-4921
\[o)fG lffV~~:
~\f\l l MAR -6 2008
L ---J
I D(}Jii j\1\'.; r.r' I '·~hJ .. ::.J OFFICE J
---·-+
North Carolina Department of Environment and Natural Resources
Division of Waste Management
Prepared By:
Donald R. Smith
Environmental Scientist
Underground Storage Tank Section
Raleigh Regional Oftice
1628 Mail Service Center
Raleigh, NC 27699
Prepared For:
Mr. Jerry Douglas
Abercrombie Oil Company, Inc.
2930 West Main Street, P.O. Box 1361
Danville, Virginia 24543
Prepared By:
Apex Companies, LLC
6711 Peters Creek Road, Suite 201
Roanoke, Virginia 24019
March 4, 2008
Apex Project No.: 768299.190
Reviewed .By:
@at:
RobertS. Wagner
Project Manager
Reviewed By:
Robert S. WiUiauison
North Carolina Licensed
Geologist #1735
~ Environmental ~ Engineering ~ Water Resources ~ Industrial Hygiene ~
~ Facility Services ~ Construction Services -<1t
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TABLE OF CONTENTS
1.0 INTRODUCrfiON .......................................................................... · ................................. .
2.0 SITE DESCRIPTION ....................................................................................................... 1
3.0 BACKGROUND ............................................................................................................... l
4.0 G.ROUNDWATER MONITORING .............................................................................. 2
5.0 UPDATED RECEPTOR INFORMATION .................................................................. 3
6.0 CAP IMPLEMENTATION MONITORING SUMMARY .......................................... 3
Table 1.
Table 2.
Figure 1.
Figure 2.
Figure 3.
Appendix A
AppendixB
List of Tables
Groundwater Elevation Data
Summary of Groundwater Analytical Results
List of Figures
Site Location Map
Site Plan and Monitoring Well Location Map
Water Table Gradient Map
List of Appendices
Laboratory Certificate oj'Analysis and Chain-ofCustody Records
Historical Groundwater Analytical Data
CAP Implementation Groundwater Monitoring Report
Short Stop
March 4, 2008
Groundwater Incident 116350
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l.Q INTRODUCTION
Apex Companies, LLC has completed Corrective Action Plan (CAP) implementation
groundwater monitoring for the Short Stop facility located at 300 West Main Street in Carrboro
(Orange County), North Carolina (Figure 1). This report was prepared in accordance with North
Carolina Department of Environment and Natural Resources (NCDENR) correspondence dated
December 17, 2007. Data presented in this report documents current and historical groundwater
gauging and groundwater quality data associated with the release. This report, prepared in
accordance with the Underground Storage Tank Section guidelines presented in the NCDENR
Guidelines for Assessment and Corrective Action dated July 1, 2001 , is being delivered to Ms.
Caroline Davenport of the NCDENR Raleigh Regional Office on behalf of Abercrombie Oil
Company, Inc.
2.0 SITE DESCRIPTION
The subject property is located at 300 West Main Street in Carrboro (Orange County),
North Carolina. The facility is operated as a retail gasoline station and convenience store. The
subject site is improved with one slab-on-grade brick building, two dispenser islands covered by
an overhead canopy, and paved access and parking areas. The subject site is served by the
following underground utilities: potable water, telephone, electricity, natural gas, and sanitary
sewer. A site plan illustrating pertinent features of the subject site is provided as Figure 2. The
subject site is zoned for commercial/retail use. The surrounding area is zoned for commercial
and residential use.
3.0 BACKGROUND
On January 15, 1 991, a petroleum release was discovered during the removal of the
undergrm.md storage tank (UST) systems located at the Short Stop Convenience Mart. The
former UST system was previously owned and operated by U-Fill'er-UP, Inc. The approximate
locations of the former UST basins are depicted on Figure 2.
As directed by NCDENR, ENSCI Environmental Inc. (ENSCI) prepared the following
reports associated with the petroleum release at the Short Stop Convenience Mart: Preliminary
Environmental Site Assessment (5/20/93), Limited Site Assessment (6/25/93), Comprehensive
Site Assessment (CSA) (2/17/94), CAP (7/5/94), CSA Addendum (3/8/95), and Quarterly
Groundwater Monitoring Reports (217/96, 5/16/96, 8/1/96). These investigations included the
drilling of eight soil borings (B-1 to B-8), eight Geoprobe soil borings (P-1 to P-4 and D-1 to D-
4), seven Type II groundwater monitoring wells (MW-1, MW-3 to MW-6, MW-8, and MW-9),
and one Type III groundwater monitoring well (MW -7). Monitoring well locations are depicted
on Figure 2.
Monitoring well MW -2 was installed by a contractor other than EN SCI in association
with a confirmed gasoline release at Happy Store #3 18. In addition to the identified release at
Happy Store #3 18, a petroleum release has also been documented at the Onjtes property located
CAP lmplemc11tntion Groundwater Monitoring Report
Shon Siop
Groundwater Incident #6350
March 4, 2008
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adjacent to both the Short Stop Convenience Store and Happy Store #318. According to the
February 17, 1994 CSA prepared by ENSCI, these separate petroleum releases are believed to be
the source(s) of contamination discovered in water supply wells, WW-1 and WW-2 which are
located approximately 200 feet south ofthe Short Stop facility.
Subsequent to the NCDENR approval of the July 5, 1994 CAP, ENSCI installed and
operated a soil vapor extraction (SVE) system in an effort to remediate subsurface. petroleum
impacts. The four SVE wells (SVE-1 through SVE-4) associated with the system are depicted
on Figure 2. ENSCI also installed one groundwater recovery well (RW-1) in accordance with
the July 5, 1994 CAP requirements.
The reports prepared by ENSCI identified the former kerosene UST, the two former
gasoline USTs, and the product dispenser proximal to Main Street as the sources of the release
observed dlU'ing subsurface investigations. In an effort to quantitatively assess current site
conditions, NCDENR requested that anew CSA be performed at the site.
In May 1999, Apex submitted a CSA Addendum docwnenting the installation of four
additional monitoring wells (AEI-MW-10 through AEI-MW-13), groundwater sampling, and
remedial recommendations. Analytical results yielded dissolved-phase petroleum constituents in
excess of the North Carolina Groundwater Quality Standards established in 15A NCAC
2L.0202(g).
4.0 GROUNDWATER MONITORING
In accordance with NCDENR directives, Apex collected .groundwater samples from nine
of the 13 monitoring wells on January 9, 2008. Monitoring well MW-2 was not sampled due to
an insufficient water column. Monitoring wells MW -6 and MW -7 could not be located and
monitoring well MW -12 had an obstruction in it and could not be sampled during this
monitoring event. Prior to purging and sampling, the wells were gauged using a Solinst™
electronic interface probe to measure depth to groundwater and to investigate for the presence of
free-phase petroleum product. Free product was not encountered during the gauging event.
Groundwater elevations as measured on January 9, 2008 are presented in Table 1. Groundwater
monitoring well locations are presented on Figure 2.
Prior to sampling, Apex purged each monitoring well to remove suspended solid material
from the water column and to collect samples representative of aquifer conditions. Groundwater
samples were collected using dedicated, disposable, high density polyethylene bailers and were
transferred directly into the appropriate sample containers immediately upon collection. Clean,
disposable latex gloves were used during all phases of sample collection. The samples were
labeled and stored on ice pending delivery to Air, Water, and Soil Laboratories, Inc. in
Richmond, Virginia. Per NCDENR directives, the monitoring well samples were submitted for
volatile organic compounds (VOCs) and semi-VOCs analysis via U.S. EPA SW-846 method
6210D and 625, respectively. The samples were also analyzed for total lead via method 7421 ,
MADEP volatile petroleum hydrocarbons (VPH) via U.S. EPA SW-846 method 5035, and
MADEP extractable petroleum hydrocarbons (EPH) via U.S. EPA SW-846 method 35508.
CAP Implementation Groundwater Monitoring Report
Short Stop
Ground\vntcr lricidcnl #6350
2 March 4, 2008
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Strict sample security and chain-of-custody documentation were maintained during all phases of
transport. Chain-of-custody documentation and the laboratory Certificates of Analyses are
included as Appendix A.
Analytical results yielded petroleum compounds that exceed 2L Groundwater Quality
Standards in eight of the nine monitoring wells. Monitoring wells MW -8 and MW -13 yielded
maximum methyl tert-butyl ether (MTBE) concentrations of776 micrograms per liter (J.Lg/L) and
489 f.!g/L, respectively. Benzene, naphthalene, lead, trichloroethylene, tetrachloroethylene
(PCE), chloroform, 1,2-Dichloroethane, vinyl chloride, and 1,2-Dichloropropane also exceeded
2L Groundwater Quality Standards in the monitoring wells. PCE and trichloroethylene are
contaminants associated with chemicals commonly used in the dry cleaning process and are not
constituents of the petroleum fuels stored at the subject site. A summary of groundwater
analytical results from the grow1dwater monHoring wells is presented in Table 2. Historical
groundwater analytical data is presented in Appendix B.
Grotmdwater flow at the site was determined by the triangulation method of the relative
groundwater elevations within the monitoring wells. Figure 3 is a water table gradient map
generated from the relative elevations of equilibrated groundwater as measured on January 9,
2008. Relative groundwater elevations predict groundwater flow is to the south.
5.0 UPDATED RECEPTOR INFORMATION
According to records reviewed by Apex, the site and surrounding properties have access
to public utilities, including potable water from a municipal system. Residents in the immediate
vicinity utilize public water for potable water needs.
On January 9, 2008, Apex performed a site reconnaissance to identify any potential
receptors located within a 1,500-foot radius of the subject property. During this and previous
investigations, Apex identified numerous residential and commercial parcels within the 1,500-
foot radius. Personal interviews were conducted with seven property owners during the January
9, 2008 site visit. Each of the seven property owners stated that they obtain potable water from a
municipal system. Apex also spoke via phone with Mr. Greg Moody, owner of the car wash
located approximately 200 feet south of the Short Stop facility, who stated that there are two
supply wells located on his property (WW-1 and WW-2). Currently, both wells are out of use,
but Mr. Moody stated that he will soon begin using one of the wells for water usage at the car
wash. Apex also spoke with Mr. Michael Canova, Code Enforcement Supervisor for the Town
of Carrboro, North Carolina, who sated that he does not know of any other supply wells within
the 1,500-foot survey radius.
6.0 CAP IMPLEMENTATION MONITORING SUMMARY
As requested, Apex has prepared this CAP Implementation Monitoring Report for the
Short Stop facility. Analytical results yielded petroleum compounds that exceed 2L
Groundwater Quality Standards in eight of the nine monitoring wells sampled during this event.
CAP Implementation GI'Oundwater Monitoring Rei>Ort
Short Stop
Groundwalcr lncidenl #6350
3 March 4, 2008
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Two supply wells, WW-1 and WW-2, are located approximately 200 feet south of the site, but
are currently not in use. The owner of the supply wells stated th~t at least one of the wells will
be used in the near future to supply water to the car wash facility.
Based on the presence of petrolewn constituents above 2L Groundwater Quality
Standards and the presence of supply wells in the area, Apex recommends continued monitoring
of the groundwater monitoring wells and sampling of the car wash supply well once active to
determine risk to hwnan health. This report is being delivered to Ms. Caroline Davenport of the
NCDENR on behalf of Abercrombie Oil Company, Inc.
CAP Implementation Groundwater Monitoring Report
Short Stop
Groundwater Incident #6350
4 March 4, 2008
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I FIGURES
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6711 Peters Creek Road
Suite201
Roanoke, Virginia 24019
Telephone: [phone]
Fax:(S40)563-4921
Figure l
Site Location Map
Short Stop
300 West Main Street
Carrboro (Orange CoUDty), North Carolina
PC# 1993-0936
United States Department of the Interior
Geological Survey
7.5 Minute Series Topographic Map
Contour Interval: 20 feet
Scale: 1 inch = 2000 feet
Goodview, Virginia (1967, pbotorevised
1985)
Client: DEQ WCRO
Apex Job #:768299.190
Date: February 2008
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-------~~~~~----~
TABLES
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MW-l Ol/09/08
MW-2 Ol/09/08
MW-3 01/09/08
MW-4 Ol/09/08
MW-5 01/09/08
MW-8 01/09/08
MW-9 01/09/08
AEI-MW-10 01/09/08
AEI-MW-11 01/09/08
AEI-MW-12 01/09/08
AEI-MW-13 01/09/08
Apex
2 NA • Well screen depth unknown.
1 NS ;Not surveyed.
Table l.
Groundwater Elevation Data
96.52 19.78 NA2 76.74
96.10 19.81 NA 76.29
96.50 19.91 88.50-73.50 76.59
95.82 19.49 88.82-71.82 76.33
96.54 20.12 88.54-73.54 76.42
NS3 20.89 NA NA
NS 20.28 NA NA
96.12 19.53 91.12-71.12 76.59
96.59 19.85 91.59-71.59 76.74
96.34 19.75 91.34-71.34 76.59
96.41 20.21 91.41-71.41 76.20
-------------------
Table 2.
Summary of Groundwater Analytical Results
. "'* -2L ..... Gross .. '
Parameter (J.lg/l.) .1\:fW-1 MW-3 MW,-4 MW-5 ··~-8 MW-9 AEI-AEI-AEI-Groundwater Contaminant
<MW;;.to MW-11 MW-13 Standard§' Levels .. (~) . (U2/Lf
MTBE1 26.0 <5 9.7 <5 776 67.8 76.3 <5 489 200 "200,000
Di-isopropyl ether (DIPE) <5 <5 <5 <5 16.0 <5 52.4 8.0 48.4 70 70,000
Benzene <1 <1 <l <] <1 <I 13.0 2.0 <1 1.0 5,000
Ethylbenzene <1 <1 <1 <1 <I <) 4.2 9.5 <1 29 29,000
Isopropyl benzene <1 <1 <l <] <1 <I 3.9 1.5 <1 70 25,000
n-Propylbenzene <1 <1 <1 <1 <1 <I 5.1 2.3 <I 70 30,0()0
tert-Butylbenzene <1 <1 <1 <1 <I <I 1.3 <l <1 70 15,000
1,2,4-Trimethylbenzene <1 <1 <1 <I <l <I <1 2.8 <1 350 28,500
sec-Butylbenzene <1 <I <1 <I <1 <I 3.9 6.2 <1 70 8,500
Naphthalene <I <1 <1 <I <I <1 34.4 2.6 <1 21 15,500
Naphthalene2 <10 <10 <10 <10 <10 <10 34.6 <10 <10 21 15,500
Lead3 4.0 24.0 43.0 236 3.0 13.0 10.0 15.0 7.0 15 15,000
cis-1 ,2-Dichloroethylene <1 <] <1 6.8 40.1 l, 130 <I <I 3.2 NA4 NA
Trichloroethylene <1 <I <1 3.3 465 2,770 <1 <I 18.7 2.8 2,800
Tetrachloroethylene (PCE) <1 <I 7.8 28.5 4,680 44,200 1.5 <1 45.1 m7 700
trans-1,2-Dichloroethylene <l <1 <I <l 6.9 9.1 <l <1 2.2 NA NA
Chloroform <1 <1 <1 <I 3.4 37.7 <l <1 <1 0.00019 190
1, l, I ,2-Tetrachloroethane <1 <I <1 <I <I 56.4 <l <1 <I NA NA
1 ,2-Dichloroethane <1 <] 3.2 <I <I <1 <l <1 2.7 0:38 380
Vinyl chloride <1 <I <1 <I <) 3.8 <1 <1 <1 0.015 15
I, 1-Dichloroethylene <1 <] <1 <I <I 5.6 <I <1 <1 7 7,000
l ,2-Dichloropropane <I <I <1 <1 <I 1.9 <1 <I <l 0.56 560
...
I, 1 ,2-Trichloroethane <1 <1 <1 <1 <1 4.6 <I <I <I NA NA
-------------------
Table 2.
Summary of Groundwater Analytical Results
<100 <100 <100 <100 <100 <tOO 393 223 <100
<100 <100 <100 <100 <100 <100 589 254 <100
C ll-C22 Aromatic <108 <182 NS5 <100 <100 268 <105 <100
<10.8 <18.2 NS <10.5 <10.0
Bold-Values are greater
1 VOCs by U.S. EPA method 62100, reported in micrograms per liter ~L).
' SVOCs by U.S. EPA method 625. reported in micrograms per liter (IJ.g/L).
1 Lead by U.S. EPA method 7421, repOrted in micrograms per liter (j.Lg/L).
• NA "'2L Groundwater Standards & Gross Contaminant Levels not provided.
s NS <Z Not sampled due to insuff~eient water column.
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APPENDIX A
Laboratory Certificate of Analysis and
Chain-of-Custody Records
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AIR
WATER
LABORATORIES, INC!'
2109A Nortb Hamilton Street • Richmond, Vuginia 23230 • Tel: {804) 358.8295 Fax: [phone]
Certificate of Analysis
Final Report
Laboratory-Order ID 08010146
Client Name: APEX Companies, LLC.
6711 Peters Creek Road
Suite 201
Date Issued: January 28, 2008
Roanoke,VA 24019
Submitted To: Robert Wagner
Cllent·Site 1.0.: Short Stop
Laboratory Sample 10 SampleiD
0801 0146·001 010908-190.01/ AE1 ·MW-10
0801 0146-002 010908-190-02/ AE1-MW-11
0801 0146.003 010908-190-03/ MW-1
0801 0146-004 01 0908-190-Q4 I MW -3
08010146-005 0, 0908-190-05 I MW-4
0801 0146-006 010908-190·06/ MW-5
0801 0146·007 01 0908-190·07 I MW -8
08010146-008 010908-190·08/ MW-9 . .
06010146-009 010908-190-09/ AEI-MW-13
Project Number 768299.190
Purchase Order NA
Sample Date Receive Date
January 09, 2008 January 11, 2008
January 09, 2008 January 11, 2008
January 09, 2008 January 11, 2008
January 09, 2008 January 11, 2008
January 09, 2008 January 11. 2008
January 09, 2008 January 11 , 2008
January 09, 2008 January 11, 2008
January 09, 2008 January 11, 2008
January 09, 2Q08 January 11, 2008
On January 11, 2008, nine water samples were recel.ved via courier for analysis in
accordance with the attached Chain-Of-Custody. The samples were received with sample
containers Intact by Ashley McGinley (AWS). Any deviations, discrepancies or Irregularities
observed In sample condition, Including holding times, temperature, containers or
preservatives have been notated on the chain-of-custody.
I
.AIR I WATER I LABORATORIES, INC!
2109A Norlh HamJton Sheet • Richmond, Vzrginia 23230 • Tel: [phone] Fax: [phone] I Certificate·of Analysis
Final Report I Laboratory Order ID 08010146
Client Name: APEX Companies, LLC. Date Received: January 11, 2008
6711 Peters Creek Road Date Issued: January 28, 2008 I Suite 201
Roanoke,VA 24019
Submitted To: Robert Wagner Project Number: 768299.190 I Client Site I.D.: Short Stop Purchase Order: NA
Sample 1.0.: 010908-190-01/ AE1-MW-10 Laboratory Sample I. D.: 08010146·001 I Datemme Sampled: 01/09/08 15:30 Analysis
Parameter Method Sample Results RepUmlt OatefTime Analyst
Lead SW7421 D.010mgiL 0.002 01/1510813:41 OMH 'I
MTBE SMS2100 76.3ug/L 5.0 01122/0815:24 DMB
01-lsopropyl ether (DIPE} SM62100 52.4 ug/L 5.0 01122/08 15:24 OMB
Olchlorodlfluoromethane SM6210D < 1 ugll 1.0 01122/08 15:24 DMB I Chloromethane SM62100 < 1 ugll 1.0 01122108 15:24 DMB
VInyl chloride SM62100 < 1 ugll 1.0 0112210815:24 DMB
Bromomethane SM6210D < 1 ugll-1.0 01122108 15:24 DMB I Chloroethane SM62100 . < 1 ugJl 1.0 01122/08 15:24 DMB
Trichlorofluoromethane SM6210D < 1 ug/L 1.0 01122/08 15:24 DMB
1, 1·Dichloroethytene SM62'10D < 1 ug/L 1.0 01122/08 15:24 DMB I Methylene chloride SM6210D < 4 ug/L 4.0 01122/0815:24 DMB
trans-1 ,2-{)lchloroethylene SM62100 < 1 ugJl 1.0 01122/08 15:24 DMB
1,1-0ichloroethane SM6210D < 1 ug/L 1.0 01122/08 15:24 DMB I 2,2-Dichloropropane SM82100 < 1ug/L 1.0 01122/08 15:24 OMB
cls·1,2-{)lchloroethylene SM62100 < 1 ug/l 1.0 01/22/08 15:24 DMB
Bromochloromethane SM62100 < 1 ugll 1.0 01/22/08 15:24 DMB I Chloroform SM6210D < 1 ug/L 1.0 01/22/08 15:24 DMB
1,1, 1· Trichloroethane SM6210D < 1 ug/L 1.0 01i22/08 15:24 DMB
Carbon tetrachloride SM82100 < 1 ug/L 1.0 01122/08 15:24 DMB .I
_1,1-Dichloropropene SM6210D < 1 ugll 1.0 01122/08 15:24 DMB
Benzene SM62100 13.0 ug/l 1.0 01122/0815:24 DMB
1 ,2-{)lchloroethane SM6210D < 1 ugll 1.0 01/22/0815:24 DMB I Trichloroethylene SM62100 < 1 ug/L 1.0 01122/0815:24 DMB
. 1 ,2-Dlchloropropane SM6210D < 1 ug/L 1.0 01/22/08 15:24 DMB
Dlbromomethane SM6210D < 1 ug/L 1.0 01122/0815:24 DMB I Bromodlchloromethane SM6210D < 1 ugll 1.0 01122/08 15:24 DMB
ci&-1.J.Dichloropropene SM62100 < 1 ugll '1.0 01/22108 15:24 DMB
4-Methyl-2-pentanone (MIBK) SM62100 < 10 ugll 10.0 01/22/0815:24 DMB I Toluene SM62100 < 1 ugiL. 1.0 01/22/08 15:24 DMB
1,1 ,2-Trlchloroethane SM62100 < 1 ug/L 1.0 01/22/08 15:24 DMB
Tetrachloroethylene (PCE) SM82100 1.5 ug/L 1.0 01i22108 15:24 DMB I
t) _ _..,... <'\ -t. AA
I
I AIR
WATER I -LABORATORIES, INC.•
2109A Nortb Hamilton Street • Richmond, Virginia 232.30 • Tel: [phone] Fax: {804) 358-8297
I Certificate of Analysis
I
Final Report
Laboratory Order 10 08010146
Client Name: APEX Companies, LLC. Date Received: January 11 , 2008
I 6711 Peters Creek Road Date Issued: January 28, 2008
Suite 201
Roanoke,VA 24019
I Submitted To: Robert Wagner Project Number: 768299.190
Client Site I.D.: Short Stop Purchase Order: NA
I Sample I.D.: 010908-190·01/ AE1-MW-10 Labo~tory Sample J.D.: 08010146-001
Datefrlme Sampled: 01/09/08 15:30 Analysis
Pan1111eter · Method Sample Results RepUmlt Oatelllme Analyst
I· 1 ,3-Dichloropropana SM62100 < 1 ugll 1.0 0112210815:24 DMB
Olbromochloromethane 5M62100 < 1 ug/L 1.0 01/22108 15:24 DMB
1 ,2-0!bromoethane (EOB) SM6210D < 1 ugll 1.0 01122/08 15:24 DMB
1-Ctllorobeflzene SM6210D < 1 ugll 1.0 0112210815:24 OMB
1, 1.1 ,2-TetrachloroeChane SM6210D < 1 ugiL 1.0 01/22108 15:24 OM8
Ethylbenzene 5M62100 4.2 ugiL 1.0 01/22/0815:24 DMB
I m,p-Xylenea SM6210D < 2 uo/L 2.0 01122/08 15:24 DMB
o-Xytene SM62100 < 1 ug/L 1.0 01122/08 15:24 DMB
Xytenes, Total SM62100 < 3 ug/L 3.0 01122/08 15:24 DMB
I Styrene SM62100 < 1 ug/L 1.0 01122108 15:24 DMB
Bromofonn SM6210D < 1 ug/L 1.0 01/22/08 15:24 DMB
lsopropylbenzene SMS2100 3.9ug/L 1.0 01/22/08 15:24 DMB
I Bromo benzene SM6210D < 1 ugll 1.0 01/2210815:24 DMB
1,1,2,2.-Tetrachklrcethane 5M62100 < 1 ug/L 1.0 01122/08 15:24 OMB
1 ,2,3-Trtct\loropropane SM62100 < 1 ug/L 1.0 01/22108 15:24 DMB
I n.Propytbeozene SM6210D 5.1 ugll 1.0 0112210815:24 DMB
2·Chlorctoluene SM62100 < 1 ug/L 1.0 01122/0815:24 DMB
4-chloc'otoluene SM62100 < 1 ugll 1.0 01/22/08 15:24 OMB
I 1,3,5-Tr1methytbenzene SM62100 < 1 ugiL 1.0 01122/08 15:24 OMS
tert-Butylbenzene SM6210D 1.3 ugll 1.0 01122/08 15:24 OMS
1 ,2,4-Tr1methytbenzene SM6210D < 1 ug/l 1.0 01/22108 15:24 DMB
I sec-Butytbenzene SM62100 3.9 u(1/L 1.0 01/22/08 15:24 DMB
1 ,3-Dichlombenzene SM62100 < 1 ugll 1.0 01122108 15:24 OMB
p-J~propyttoluene SM62100 < 1 ugll 1.0 0112210815:24 OMS
I 1 ,4-0ichlorcbenzene 5M62100 < 1 ugll 1.0 01122108 15:24 DMB
1.2-0ichlorobenzene SM62100 < 1 ugll 1.0 01122108 15:24 DMB
n-Butylbenzene SM6210D < 1 ug/L 1.0 01122/08 15:24 DMB
I 1,2-Dibromo-3-ehloropropane (DBCP) 5M62100 < 4 ugll 4.0 01/22/08 15:24 OMS
1 ,2, 4-Trlctllorcbenzene SM6210D < 1 ugll 1.0 01/22108 15:24 OMB
Hexachlorcbutadlene SM6210D < 1 u9-'L 1.0 01/2210815:24 DMB
I Naphthalene SM6210D 34.4 ugll 1.0 01/22/08 15:24 DMB
1 ,2,3-T rlchtorobenzene SM62100 < 1 ug/L 1.0 01/22108 15:24 OMB
PAn<>? n f AA
I
AIR I WATE R I LABORATORIES,INC;9
2109A North Hamilton Street • Richmond, Virginia 23230 • Tel: (804} 358-8295 fax; [phone]
Certificate of Analysis I
Final Report
Laboratory Order 10 08010146 I
Client Name: APEX Companies, LLC. Date Received: January 11, 2008
6711 Peters Creek Road Date Issued: January 28, 2008 I Suite 201
Roanoke,VA 24019
Submitted To: Robert Wagner Project Number: 768299.190 I Client Site 1.0.: Short Stop Purchase Order: NA
'
Sample 1.0.: 010908-190-01/ AE1-MW-10 Laboratory Sample 1.0.: 06010146..001 I Oate!Time Sampled: 01/09/08 15:30 Analysis
Parameter Method Sample Results Rep Umtt Date/Tlme Analyst
4-Chloro-3-methylphenol EPA625 < 10 ug/L 10.0 01/17/08 1'3:04 JHV I 2-ChLDTOphenol EPA625 < 10 ugll 10,0 01/17108 13:04 JHV
2,4-0ichlorophenol EPA625 < 10 ug/L 10.0 01/17/08 13:04 JHV
2,4-0imelhytphenol EPA625 <10ug/L 10.0 01/17/08 13:04 JHV I 4,6-Dlnltro-2·methylphenol EPA625 < 50 ugll 50.0 01/17108 13:04 JHV
2,4-0inllropheool EPAB25 <50 ugl\. 50.0 01/17108 13;04 JHV
2-Nitrophen?l EPA626 <10ug/L 10.0 01/17/08 13:04 JHV I 4-Nitrophenot EPA625 <50 ugll 50.0 01/17/08 13:04 JHV
Pentachlorophenol EPAB25 < 20 ugll.. 20.0 01/17/08 13:04 JHV
Phenol EPA625 < 10ug/L 10.0 01/17/08 13:04 JHV I 2.4,6-Trlchlorophenol EPAB25 < 10 ug/1.. 10.0 01/17/0813:04 JHV
Acenaphthene EPA625 < 10 ug/L 10.0 01/17/08 13:04 JHV
Acanaphthylene EPAB25 < 10 Ug/l 10.0 01/17/08 13:04 JHV I Anthracene EPAB25 < 10 ug/L 10.0 01111108 13:04 JHV
Benm (a) anthracene EPA625 <10ugll 10.0 01117/08 13:04 JHV
Benzo {b) fluoranthene EPA625 <10ugfl. 10.0 0111710813:04 JHV I Beruro ~)fl~n~ EPA625 < 10 ug/L 10.0 01/17108 13:04 JHV
BenzD (g,h,l) perylene EPAB25 <10ug/L 10.0 01117108 13:04 JHV
· Benz.o (a) pyrene EPA625 < 10ugll 10.0 01/17108 13:04 JHV I 4-Bromophenyl phenyl ether EPA625 < 10 ugll 10.0 01/17/06 13:04 JHV
Butyl benzyl phthalate EPA625 < 10 ug/L 10.0 01117108 13:04 JHV
bls (~·Chloroethoxy) methane EPA625 <10ug/L 10.0 01/17/0813:04 JHV I bls (2-Chloroethyl} ether EPA625 < 10ug/L 10.0 01/17108 13:04 JHV
bls (2-Chlorolsopropyl) ether EPAB25 < 10 ugll 10.0 01/17/0813:04 JHV
4-Chloropheoyl phenyl ether EPA625 < 10 ugJl 10.0 01117108 13:04 JHV I Chrysene EPA625 < 10 ugll. 10.0 01/17/08 13:04 JHV
Dlbenz {a,h) anthracene EPA625 < 10 ug/L 10.0 01/17/08 13:04 JHV
Dl-n-txrtyt phthalate EPA625 < 10 ug/1.. 10.0 01/17/0B 13:04 JHV I , 1,2·Dichlorobenzene EPA625 < 10 ug/l 10.0 01/17/08 13:04 JHV
1,3-Dichlorobenzene EPA625 < 10ugll 10.0 01/17/08 13:04 JHV I
1.4·Dichlorobenzene EPA625 <10ug/L. 10.0 01/17/08 13:04 JHV I!
Dono ~ nf .44
I
I AIR
WATE R I LABORATORIES, INC.•
I
2109A North Hamilton Street • Richmond, Virginia 23230 • Tel: {804) 358..8295 Fax: [phone]
Certificate of Analysis
I Final Report
Laboratory Order ID 08010146
Client Name: APEX Companies, LLC. Date Recelyed: Janua,Y 11, 2008
I 6711 .Peters Creek Road Date Issued: January 28, 2008
Suite 201
I
Roan9ke,VA 24019
Supmltted To: Robert W agner Project Number: 768299.190
Client Site I.D.: Short Stop Purchase Order: NA
I Sample 1.0.: 010908-190-01 / AE1-MW-10 Laboratory Sample J.D.: 08010146-001
Date/Time Sampled: 01/09/08 15:30 Anatysla
Parameter Method Sample Results Rep Umlt OateiTime Analyst
I Dlethyl phthalate EPA625 <10ugll 10.0 01/17/08 13:04 JHV
Dlmothyl phthalate EPA625 < 10 ugll 10.0 01/17/08 13:04 JHV
2,4-Dinltrotoluene EPA625 <10ugll 10.0 01/17/08 13:04 JHV
1.· 2,6-0inltrotoluene EPA625 < 10 ugiL 10.0 01/17/08 13:04 JHV
01-iK>ctyl phthalate EPA625 < 10ug/L 10.0 01/17/0813:04 JHV
bls (2-EthylhexyJ) phthalate EPA625 < 10 ug/1.. 10.0 01/17/0B 13:04 JHV
I Fluoranthena EPA625 < 10 ug/L 10.0 01/17108 13:04 JHV
Fluorene EPA625 < 10 ugll 10.0 01/17108 13:04 JHV
Hexachlorobenzene EPAB25 < 10 ugiL 10.0 01/17/08 1'3:04 JHV
I Hexachlorobutadlane EPA625 <10ugll 10.0 01117/08 13:04 JHV
Hexachlorocyclopentadlene EPA625 <10ug/L 10.0 01/17/08 13:04 JHV
Hexachloroelhane EPA625 < 10ugll 10.0 01/17108 13:04 JHV
I lndeno (1,2.3-od} pyrene EPA625 .<10ug/L 10.0 01/17108 13:04 JHV
lsophorone EPA625 <10ug/L 10.0 01/17/0813:04 .JHV
Naphthalene EPA825 34.6 ugiL 10.0 01/17108 13:04 JHV
I Nitrobenzene EPA625 < 10uglt. 10.0 01117108 13:04 JHV
N-Nitrosodlmethy!amlne EPA625 <10uglt. 10.0 01/17108 13:04 JHV
N-Nitrosodlphenylam!ne EPA625 <10ug/L 10.0 01117/08 13:04 JHV
I N-Nllrollodi·N-p~pylamtna EPA625 < 10 ug/1.. 10.0 01/17/08 13:04 JHV
Phenanthfene EPA625 < 10 ug/L 10.0 01/17/08 13:04 JHV
Pyrena EPA625 < 10ugll 10.0 01/17/0813:04 JHV
I 1.2.4-Trichlorobenzene EPA625 < 10ugll 10.0 01/17/08 13:04 JHV
Benzidine EPA625 <50 ug/L 50.0 01/17/08 13:04 JHV
. 3,3-Dichlorobenzldlne EPAB25 < 1.0 ug!L 10.0 01/17/0B 13:04 JHV
I 2,3,4,6-Tatnu:;hlofophenol EPA625 < 10 ug/l 10.0 01/17108 13:04' JHV
2-Ctlloronaphthalene EPA625 < 10 ugll 10.0 01/17/08 13:04 JHV
C9·C18 Allphatlc H~rocerbons MAOEP see attach 10 I C11-C22 Aromatic Hydrocarbons MAOEP see attach 10
C19-C36 Aliphatic Hydrocarbons MADEP see attach 10
Aliphatic SuiTogate % Recovery MADEP see attach
I Fractionation SuiTogate #1 Recovery MADEP see attach
P::vu" 4 nf .S.d.
AIR WATER
LABORATORIES, INC.•
2109A North Hamilton Street • Richmond, Virginia 23230 • Tel: [phone] fax: [phone]
Certificate of Analysis
Final Report
Laboratory Order ID 08010146
Client Name: APEX Companies, LLC.
6711 Peters Creek Road
Suite 201
Roanoke,VA 24019
Submitted To: Robert Wagne~
Client Site 1.0.: Short Stop
Sample 1.0.: 010908-190-01/ AE1-MW-10
Datemme Sampled: 01/09/08 15:30
Parameter Method
Aromallc Surrogate % Reoovery MAOEP
FracUonalion SurTOgate #2 Recovety MADEP
C5-C8 Allphatlc Hych:ooarbone MADEP
CS.C10 Aromatic Hydrocarbons MADEP
Date Received:
Date Issued:
Project Number:
Purchase Order:
January 11, 2008.
January 28, 2008
768299.190
NA
Laboratory Sample 1.0.: 08010146-001
Analysis
Sample Results . Rep Limit Date/Time Analyst
see attach
aee attach
see attach 10
see attach 1 0
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1-AIR
WATER I INC:-
I
2109A North Hamilton Street • Richmond, Vuginia 23230 • Tel: [phone] Fax: [phone]
Certificate of Analysis
I Final Report
Laboratory Order ID 08010146
Client Name: APEX Companies, LLC. Date Received: January 11, 2008
I 6711 Peters Creek Road Date Issued: January 28, 2008
Sulte201
Roanoke,VA 24019
I Submitted To: Robert Wagner Project Number: 768299.190
Client Site I. D.: Short Stop Purchase Order: NA
I Sample 1.0.: 010908-19()..02/ AE1-MW-11 Laboratory Sample 1.0.: 08010146-002
DateiTime Sampled: 01109/08 14:50 Analysis
Parameter Method Sample Results RepUmlt Date/Time Analyst
I Lead SW7421 0.015 mgiL 0.002 01/15108 13:47 DMH
MTBE SM62100 < 5 ugA. 5.0 01/22/0815:50 DMB
01-lsopropyl ether (OIPE) SM62100 . 8.0 ug/L 5.0 01/2210815:50 DMB I. Dlchlorodlfluoromethane SM62100 < 1 ugiL 1.0 01122108 15:50 DMB
Chloromethane SM82100 <1\lgll.. 1.0 01/22/08 15:50 OMB
Vinyl chloride SM62100 < 1 ug/L 1.0 01/22/0815:50 OMB
I Bromomethane SM6210D < 1 ugll 1.0 0112210815:50 DMB
Ch!oroethene SM62100 < 1 ugiL 1.0 01/22/08 15:50 OMS·
Trlchlorofluoromethane SM62100 < 1ug/L 1.0 01/22108 15:50 DMB
I 1,1-0ichloroethylene SM62100 < 1 ug/1.. 1.0 01122/0815:50 OMB
Methylene chloride SM82100 <4 ug/L 4.0 0112210815:50 OMB
tlans-1,2-0ichloroethylene SM62100 < 1 ug/L 1.0 01122/081.5:50 OMB
I 1,1-Dichloroelhane SM62100 < 1 ugll 1.0 01122/0815:50 DMB
2,2-Dichloropiopane SM6210D <1ugll 1.0 01122108 15:50 DMB
cls-1 ,2-0ichloroethylene SM62100 < 1 ug/L 1.0 01122108 15:50 OMB
I Bromochloromethane SM62100 < 1 ug/L 1.0 01/22108 15:50 DMB
Chloroform SM62100 < 1 ug/l 1.0 0112210815:50 DMB
1,1, 1-Trichloroethane SM62100 < 1 ug/L 1.0 01/22/0815:50 DMB I Calboo tetrachloride SM6210D < 1 ug/L 1.0 0112210815:50 OMB
. 1,1-Dichloropmpene SM82100 < 1 ug/L 1.0 01122/08 15:50 DMB
Benzene SM62100 2.0 ug/L 1.0 01/22108 15:50 DMB
I 1.2-Dichloroethane SM62100 < 1 ugll 1.0 01122/08 15:50 QMB
Trlchloroelhylene SM6210D < 1 ug/L 1.0 0112210815:50 DMB
1,2-Dlchtoropropane SM62100 < 1 ug/L 1.0 . 01/22/0815:50 DMB I Olbromomethane SM6210D < 1ug/L 1.0 01/2210815:50 DMB
Bromodlchloromeltlane SM62100 < 1 ug/L 1.0 01/22/0815:50 OMS
cl&o 1.~Dichloropropene SM62100 < 1 ug/L 1.0 01122108 15:50 OMB
I 4-Methyl-2-pentonone (MIBK) SM62100 < 10ug/L 10.0 01/22Jt)815:50 DMB
Toluene SM62100 < 1 ug/L 1.0 01122/0815:50 DMB
1,1.2· Trichloroethane SM62100 < 1 ug/L 1.0 01/2210815:50 DMB
I Tetrachloroethylene (PCE) SM62100 <1ug/L. 1.0 01/22108 15:50 DMB
Pl:ln~ ~ nf 4!4
I
AIR I WATE R I LABORATORIES, INC~
2109A North Hamilton Street • Richmond, Virginia 23230 • Tel: [phone] Fax: (804) ~-8297
Certificate of AnalysiS I
Final Report
Laboratory Order ID 08010146 I
Client Name: APEX Companies, LLC. Date Received: January 11 , 2008
6711 Peters Creek Road Date Issued: January 28, 2008 I Suite 291
Roanoke,VA 24019
Submitted To: Robert Wagner Project Number: 768299.190 I Client Site I.D.: Short Stop Purchase Order: NA
Sample 1.0.: 010908-190.02/ AE1-MW-11 Laboratory Sampfe I.D.: 0801014~002 I Datefflme Sampled: 01/09/08 14:50 Analysis
Parametar-Method Sample Resulta Rep Umlt Date/Tlme Analyst
1,3-0ichloro~ne SM62100 < 1 ug/1.. 1.0 01122/08 15:50 DMB I Dlbromochloromethane SM6210D < 1 ug/L 1.0 01/22108 15:50 DMB
1,2·Dibromoethane (EDB} SM62100 < 1 ug/1.. 1.0 01/22/08 15:50 . DMB
Chlorobenzena SM6210D < 1 ug/L 1.0 01/22108 16:50 DMB I 1,1,1,2-Tetraehloroethana SMB210D < 1 ugll 1.0 01/22108 15:50 DMB
Ethyl benzene SMB2100 9.5 ug/L 1.0 01122108 15:50 OMB
m,p-Xylenes SM62100 < 2 ug/L 2.0 01/22108 15:50 DMB I o-Xylene SM62100 < 1 ug/L 1.0 01/22108 15:50 DMB
Xylenes. Total SM62100 < 3 ugJL 3.0 01/22108 15:50 OMB
Styrene SM62100 < 1 ug/L 1.0 01/22108 '15:50 DMB I Bromofurm SM6210D < 1 ugll 1.0 01/22/08 15:50 DMB
lsopropylbenzene SM62100 1.5 ug/L 1.0 01/2210815:50 DMB
Bromo benzene SM6210D < 1 ug/L 1.0 01/22108 15:50 DMB I 1.1,2,2·Tetrachloroethane SM6210D < 1 ug/1.. 1.0 01/22108 15:50 DMB
f ,2,3· Trtchloropropane SM6210D < 1 ug/1. 1.0 01/22/08 15:50 DMB
n-Propylbenzene SM6210D 2.3 ugiL 1.0 01122108 15:50 DMB I 2..Chlorotoluene SM6210D < 1 ug/L 1.0 01122/0815:50 DMB
4-Chlorotoluene SM6210D < 1 ug/L 1.0 01122108 15:50 DMB
1,3,5-T rlmelhylbenzooe SM6210D < 1 ugll 1.0 01/22108 15:50 OMB I lert·Butylbenune SM62100 < 1 ug/L 1.0 01/22/08 15:50 OMB
1,2,4-Trlmethylbenzene SM62100 2.8ugll 1.0 01/22/08 15:50 DMB
aeo-Butytbenzene SM6210D 6.2 ug/1.. 1.0 01122/08 15:50 DMB I 1 ,3·Dichlorobenz.ene SM62100 < 1 ug/L 1.0 01122108 15:50 DMB
p-lsopropyltotuene SM6210D < 1 ug/1.. 1.0 01fl2108 15:50 OMB
1,4-0ichlorobenz.ene SM6210D < 1 ugll 1.0 01/22/08 15:50 DMB I 1.2-Diehlorobenzene SM62100 < 1 ug/1.. 1.0 01122/08 15:50 DMB
n-Buty\benzene SM6210D < 1 ug/L 1.0 01/22108 15:50 DMB
1,2-Dibromo-3-ehloropropane (DBCP) SM6210D < 4 ug/L 4.0 01122108 15:50 DMB I 1,2,4-Tr1chlottltMtnzene SM6210D < 1 ugll.. 1.0 01/22108 15:50 DMB
Hexactllorobutadlena SMB2100 < 1 ugll 1.0 0112210815:50 OMB
Naphlhalene SM6210D 2.6ug/L 1.0 01/22/08 15:50 OMB I 1,2,3-Trtchlorobenzene SM62100 < 1 ug/L 1.0 01/22108 15:50 DMB
P~OA 7 of44
I
I AIR
WATER I LABORATORIES, INC!
I
2109A Nortb Hamilton Street • Richmond, VuginiA 23230 • Tel: [phone] Fax: [phone]
Certificate of Analysis
I · Final Report
Laboratory Order 10 08010146
Client Name: APEX Companies, LLC. . Date Received: January 11, 2008
I 6711 Peters Creek Road. Date Issued: January 28, 2008
Suite 201
Roanoke,VA 24019
I Submitted To: Robert Wagner Project Number: 768299.190
Client Site I. D.: Short Stop Purchase Order: NA
I Sample 1.0.: 010908-190-02/ AE1-MW-11 Laboratory Sample 1.0.: 08010146-002
Date/Time Sampled: 01/09/08 14:50 Analysis
Parameter Method Samplo Results RepUmit Date/Time Analyst
I 4-Chloro-3-methylphenol EPA625 < 10ugll 10.0 01/17108 13:37 JHV
2-Chlo.-ophenol EPA625 < 10 ugll 10.0 01/17/0813:37 JHV
2,4-Dichlorophenol EPA625 < 10 ugll 10.0 . 01/17/0813:37 JHV
I. 2,4-Dimelhylphenol EPA625 < 10 ugll 10.0 01/17/0813:37 JHV
4 ,6-Dinltro·2·methylphenol EPA625 < 50ug/L 50.0 01/17/0813:37 JHV
2. 4·Dinltrophenol EPA625 < SOugll 50.0 01/17/0813:37 JHV
I 2-Nitropheool EPA625 < 10ugll 10.0 01/17/0813:37 JHV
4-Nitrophenol EPA625 <50 ugll 50.0 01/17/0813:37 JHV
Penlachlorophenol EPA625 < 20ugll 20.0 01117/0813:37 JHV
I Phenol EPA625 < 10ug/L 10.0 01/17/0813:37 JHV
2,4,6-Trlchlorophenol. EPA625 < 10 ugll 10.0 01117/0813:37 JHV
Acenaphthene EPA625 < 10 ugll 10.0 01/17/08 13:37 JHV
I Acenaphthylene EPA625 < 10 ugll 10.0 01/17/0813:37 JHV
Anthracene EPA625 < 10~gll· 10.0 01/17/08 13:37 JHV
Benzo (a} anthracene EPA625 < 10 ugll 10.0 01/17108 13:37 JHV
I Bento (b) fluoranthene EPA625 <10ugll 10.0 01/17108 13:37 JHV
Benzo (k) fluoranthene EPA625 <10ug/L 10.0 01/1710813:37 JHV
Benzo (g,h,l) peryleoe EPA625 <10ugll 10.0 01/1710813:37 JHV
I Benzo (a) pyreoe EPA625 < 10ugll 10.0 01/17/0813:37 JHV
4-Bromophenyl phenyl ether EPA625 <10ugll 10.0 01/17/08 13:37 JHV
Butyl benz.yl phthalate EPA625 < 10 ugll 10.0 '·01/17/0813:37 JHV
I bls {2-Chloroethoxy) methane EPA625 < 10ugll 10.0 ·01/17/0813:37 JHV
bls (2-Chloroethyl) ether EPA625 < 10 ugll 10.0 01/17/0813:37 JHV
bls {2-Chlorolsopropyl) ether EPA625 < 10ugll 10.0 01/17/0813:37 JHV
I 4-Chlorophenyl phenyl ether EPA625 < 10ugll 10.0 01/17/08 13:37 JHV
Chrysene EPA625 <10ug/L 10.0 01/17108 13:37 JHV
Dlbenz (a~h),anthracene EPA625 < 10 ugll 10.0 01/17/08 13:37 JHV
I DI-n-butyl phthalate EPA625 < 10 ugll 10.0 01/17/0813:37 JHV
1 ,2-Diehlorobenzene EPA625 <10ug/L 10.0 01/17/08 13:37 JHV
1,3-0ichlorobenzene EPA625 < 10ugiL 10.0 01/17/08 13:37 JHV
I 1 ,4-Dichlorobenzene EPA625 < 10ugll 10.0 01/17/08 13:37 JHV
P~nARnf44
AIR
WATER
LABORATORIES, INC!
2109A Nortb Hamilton Street • Richmond, Virginia 23230 • Tel: [phone] Ru: {804) 358-8297
Certificate· of Analysis
Final Report
Laboratory Order 10 08010146
Client Name: APEX Companies, LLC. Date Received: January 11, 2008
6711 Peters Creek Road Date Issued: January 28, 2008
Suite 201
Roanoke.VA 24019
Submitted To: Robert Wagner Project Number: 768299.190
Client Site I.D.: Short Stop Purchase Order: NA
Sample I.D.: 010908-190-02/ AE1 -MW-1 1 Laboratory Sample I. D.: 08010146-002
Date/Time Sampled: 01/09/08 14:50 Analysis
Parameter Method Sample Results RepUmlt DaCe/Time Analyst
Olethyl phthalate EPA625 < 10 ug/L 10.0 01/17108 13:37 JHV
Dimethyl phthalate EPA625 < 10 ugll 10.0 01/17/08 13:37 JHV
2,4-0inltrotoluene EPA625 <10ugll 10.0 01/17108 13:37 JHV
2,6-0inltrotoluene EPA625 < 10ugll 10.0 01/17/0813:37 JHV
01-n-oc:tyi phthalate EPA625 < 10 ugll 10.0 01/17/0813:37 JHV
·bls (2-Ethylhexyt) phthalate EPA625 < 10 ugll 10.0 01/17/08 13:37 JHV
Fluoranthene EPA625 . < 10ugll 10.0 01/17108 13:37 JHV
Fluorene EPA625 <10ugll 10.0 01/17/08 13:37 JHV
Hexachlorobenzene EPA625 < 10 ug/L 10.0 01/17/0813:37 JHV
He)QJdllorobutadlene EPA625 <10ugll 10.0 01/17/08 13:37 JHV
.Hexachlorocyclopentadlene EPA625 < 10 ugll 10.0 01/17108 13:37 JHV
Hexadltoroethane EPA625 <10 ug/L 10.0 01117108 13:37 JHV
lndeno ( 1,2,3-cd) pyrene EPA625 . < 10 ugll 10.0 01/17108 13:37 JHV
taophorone EPA625 < 10 ug/L 10.0 01/17/08 13:37 JHV
Naphthalene EPA625 < 10ugll 10.0 01/17/08 13:37 JHV
Nitrobenzene EPA625 < 10 ugll 10.0 01117/08 13:37 JHV
N-Nitrosodlmethylamlne EPA625 < 10 ugll 10.0 01/1710813:37 JHV
N-Nitrosodlphenylamlne EPA625 < 10 ug/L 10.0 01/17108 13:37 JHV
N-Nitrosodi-N-propylamlne EPA625 < 10 ug/L 10.0 01/17/08 13:37 JHV
Phenanthrene EPA625 < 10 ugJL 10.0 01/17/08 13:37 JHV
Pyrena EPA625 < 10ug/L 10.0 01/17/08 13:37 JHV
1,2,4-Trichlorobenzene EPA625 <10ugll 10.0 01/17108 13:37 JHV
Benzidine EPA625 · <50 ugll 50.0 01117108 13:37 JHV
3,3-0ichlorobenzldlne EPA625 <10 ug/L 10.0 01117/08 13:37 JHV
2,3,4,6-Tetrechlorophenol EPA625 <10ug/L 10.0 01/17/08 13:37 JHV
2-Chloronsphthalene EPA625 < 10 ug/L 10.0 01/17108 13:37 JHV
C9-C18 Aliphatic Hydrocarbons MADEP see attach 10
C11-C22 Aromatic Hydrocarbons MAOEP see attach 10
C19-C36 Aliphatic Hydrocarbon~ MADEP see attach 10
Aliphatic Surrogate % Recovery MADEP see attach
Flltct!Onatlon Surrogate #1 Recovery MADEP see attach
PaQe 9 of 44
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LABORATORIES, INC.•
2109A North Hamilton Sheet • Richmond, Virginia 23230 • Tel: (s04) 358-8295 Ru: [phone] ,
Certificate of Analysis
FlniJI Report
Laboratory Order 10 08010146
Client Name: APEX Companies, LLC.
6711 Peters Creek Road
Suite 201
Roanoke,VA 24019
Submitted To: Robert Wagner
Client Site J.D.: Short Stop
Sample l.D.: 010908-190-02 I AE1-MW-11
Date/Time Sampled: 01/09/08 14:50 ·
Parameter
Aromatic Surrogate % Recovery
FracUonat!on Surrogate #2 Recovery
C5-C8 Aliphatic Hydrocarbons
C9-C10 Aromatic Hydrocarbons
Method
MADEP
MADEP
MADEP
'MADEP
Date Received:
Date ·Issued: ·
January 11 , 2008
January 28, 2008
Project Number: 768299.190
Purcha~e Order: NA
Sample Results
see attach
aee attach
see attach
aaa attach
p,,.. 1 n nf 114
laboratory Sample l.D.:
Analysis
Rep Umlt Oatemme
10
10
08010146-002
Analyst
I
AIR I WATE R I LABORATORIES, INC~
2109A North Ha.m.ilton Street • Richmond, Virginia 23230 • Tel: [phone] Fax: [phone]
Certificate of Analysis I
Final Report I Laboratory Order ID 08010146
Client Name: APEX Companies, LLC .. Date Received: January 11, 2008
6711 Peters Creek Road Date Issued: January 28, 2008 I Suite 201
Roanake,VA 24019
Submitted To: Robert Wagner Project Number: 768299.190 I Client Site I.D.: Short Stop Purchase Order: NA
Sample 1.0.: 010908-190-03 I MW-1 Laboratory Sample I.D.: 08010146-003 I Date/Time Sampled: 01/09/08 14:30 Analysis
Parameter Method Sample Results Rep Umlt Datarnme Analyst
Lead SW7421 0.004mgll 0.002 01/15/0B 13:53 DMH I MTBE SM62100 26.0 ug/L 5.0 0112210816:17 OMB
01-lsopropyl elher (DIPE) SMB2100 < 5 ug/L 5.0 . 01122/08 16:17 OMB
Oicttforodlftuoromelhane SM6210D < 1 ugiL 1.0 01122/0816:17 OMS I Chloromethane SM6210D < 1 ug/~ 1.0 01122/08 16:17 OMB
Vinyl chloride SM62100 < 1 ug/L '1.0 01122108 16:17 DMB
Bromomethane SM6210D < 1 ug/L 1.0 01122/0816:17 OMB I Chloroethane . SM62100 < 1 ug/L 1.0 01122/0816:17 OMB
Trlchlorofluoromethane SM62100 < 1 ugJL 1.0 01/22/06 16:17 DMB
1,1-Dichloroethyfene SM62100 < 1 ug/L. 1.0 01/22J08 18:17 DMB I Methylene chloride SM82100 < 4 ug/L 4.0 01/2210816:17 OMS
trai'IS-1,2-0fchloroethylene SM~2100 < 1 ug/L 1.0 01122/0818:17 . DMB
1, 1-0ichloroethane SM821DO < 1 ug/L 1.0 01122108 16:17 OMB I 2,2-0lchloropropane SM6210D < 1 ug/L 1.0 01122/08 16:17 DMB
cls-1 ,2-0ichloroethylene SM62100 < 1 ug.IL 1.0 01/2210816:17 OMB
Bromochloromeltlane SM62100 < 1 ugiL. 1.0 01/22108 16:17 OMB I Chloroform SM62100 < 1 ugiL 1.0 01122108 16:17 OMB
1, t,1·Trldlloroethane SM62100 < 1 ug/L 1.0 01/2210816:17 OMB
Carbon tetrach/Of'lde SM62100 < 1 ug/L 1.0 Of/22108 16:17 OMB I . 1,1-0fchloropropene SM62100 < 1 ugll 1.0 01122108 16:17 OMB
Benxene SMB2100 < 1 ug/L 1.0 01122/08 16:17 OMS
1 ,2-0\chloroethane SM6210D < 1 ug/L 1.0 01fl2/0B 16:17 OMB I Trlchforoethyfgne SM621DD < 1 ug/L 1.0 01/22/0816:17 OMB
1,2.01chloropropane SM6210D < 1 ug/L 1.0 01/22108 16:17 OMS
Dlbromomelhane SM6210D < 1 ug/L 1.0 0112210816:17 OMB I Bromodlchforomethane SM6210D < 1 ug/L 1.0 0112210816:17 DMB
cls-1,3-0ichloropropene SM6210D < 1 ug/L 1.0 0112210816:17 DMB
4-Methyl-2-penlanooe (MIBK) SM6210D <10ug/L 10.0 01122/08 16:17 DMB I Toluene SM62100 < 1 ugll 1.0 01122/08 16:17 OMB
1,1 ,2-Tr\chloroethane SM62100 < 1 ugiL 1.0 01122108 16:17 OMB
Tetrachloroethy!ena (PCE) SM6210D <1ug/L . 1.0 01/22108 16:17 OMB I
c ... ,. ... "'-t ... f ""
I
I AIR
WATER I LABORATORIES, INC~
I
2109A North Hamilton Street • Richmond, Vir~inia 23230 • Tel: [phone] Fax: [phone]
Certificate of Analysis
I Final Report
Laboratory Order 10 08010146
Client Name: APEX Companies, LLC. Date Received: January 11, 2008
I 6711 Peters Creek Road Date Issued: January 28. 2008
Suite 201
Roanoke,VA 24019
I Submitted To: Robert Wagner Project Number: 768299.190
Client Site I.D.: Short Stop Purchase Order: NA
I Sample 1.0.: 010908--190-03/ MW-1 Laboratory Sample 1.0.: 08010146-003
Date/Time Sampled: 01/09/08 14:30 Analysis
Parameter Method Sample ResultS RepUmlt DateiTlme Analyst
I 1,3-0ichloropropane SM6210D < 1 ug/L 1.0 01122/0816:17 DMB
Dlbromochloromethane SM6210D < 1 ugiL 1.0 01122/0818:17 DMB
1.2-Dibromoethane (EDB) SM62100 < 1 ugiL 1.0 01/2210818:17 OMB
I Chlorobenzene SM62100 < 1 ugiL 1.0 01/2210816:17 OMS
1,1,1.2-Tetrachloroethane SM6210D < 1 ug/L 1.0 01/2210816:17 OMB
Ethylbenzene SM62100 < 1 ug/1.. 1.0 01/22108 16:17 OMS
I m,p-Xylenea SM62100 < 2 ugll. 2.0 01122/0816:17 OMB
o-Xylene SM6210D < 1 ugJL 1.0 01122/0816:17 DMB
Xylenes, Total SM62100 < 3 ugll. 3.0 01/22/0816:17 DMB
I Styrene SM62100 < 1 ug/L 1.0 01/2210816:17 OMB
Bromoform SM82100 < 1 ug/L 1.0 0112210816:17 DMB
laopropylbenzene SM6210D < 1 ugll 1.0 01/2210816:17 OMB
I Bromobenzene SM62100 < 1 ugll.. 1.0 01/22108 16:17 DMB
1, 1.2.2-TenchiOfOethane SM62100 < 1 ug/L 1.0 01122/0816:17 DMB
1,2,3-Trlchloropropane SM6210D < 1 ug/L 1.0 01/2210816:17 DMB
I n·Propylbenzene SM621DD < 1 ugJL 1.0 01122/08 16:17 OMB
2·Chlorotoluene SM6210D < 1 ugJL 1.0 01/2210816:17 DMB
4-Chlorotoluene SM62100 < 1 ugiL 1.0 01/2210816:17 OMB
I 1,3,5-Trlmethylbenzene SM6210D < 1 ug/L 1.0 01122/08 16:17 OMB
tert·Butyfbenzene SM62100 < 1ug/L 1.0 01/2210816:17 OMB
1,2,4-Trlmethylbenzene SM62100 <'I ugiL 1.0 01/22108 16:17 OMB
I sec>Sutylbenzene SM62100 < 1 ug/L 1.0 01/22108 16:17 . OMB
1,3·Dic:hlorobenzene SM62100 < 1 ug/L 1.0 01122/08 16:17 OMB
p-lsopropyftolvene SM62100 < 1 ugll 1.0 . 01/22/08 16:17 OMB
I 1 ,4-Dichlorobenzene SM62100 < 1 ugll 1.0 01/22108 16:17 DMB
1,2-Dichlorobenzene SM621DD < 1 ugll 1.0 01/22/08 16:17 DMB
n·Butylbenzene SM62100 <1ugiL 1.0 01122/08 16:17 DMB
I 1,2-0ibromo-3-chloropropane (DBCP) SM62100 <4 ug/L 4.0 01/22/08 16:17 OMB
1,2,4-Trichlorobenzene . SM62100 < 1 ug/l 1.0 01122/0816:17 OMS
Hexachlorobutadlene SM62100 < 1Ug/L 1.0 01/22/08 16:17 DMB
I Naphthalene SM62100 < 1 ug/L 1.0 01(22/08 16:17 DMB
1,2,3-Trlchlorobenzene SM62100 < 1 ug/1.. 1.0 01/22108 16:17 OMB
P~nA 1? nf 44
I .AIR I WATER I LABORATORIES, INC!
2109A North Hamilton Street • Richmond, Vi:rginia 23230 • Tel: [phone] Fax: [phone]
Certificate of Analysis I
Final Report
Laboratory Order ID 08010146 I
Client Name: APEX Companies, LLC. Date Received: January 11, 2008
6711 Peters Creek Road Date Issued: January 28, 2008 I Suite2Q1
Roanoke,VA 24019
Submitted To: Robert Wagner Project Number: 768299.190 I Client Site I. D.: Short Stop Purchase Order: NA
Sample 1.0.: 010908-190-03/ MW -1 Laboratory Sample 1.0.: 08010146-003 I Date/Time Sampled: 01/09/08 14:30 Analysis
Parameter Method Sample Resulta RepUmlt Datemme Analyst
4-Chloro-3-melhyfphenol EPA625 < 10 ug/l. 10.0 01/17/08 14:10 JHV I 2-Chlomphenol EPA625 < 10 ug/L 10.0 01/17/08 14:10 JHV
2.4-0ichlorophenol EPA625 <1DugiL 10.0 01/17/08 14:10 JHV
2,4-0imethylphenol EPA625 < 10ogJL 10.0 01/11108 14:10 JHV I 4,6-Dinltm-2-methylphenol EPA625 <50 ug/L 50.0 01/17/08 14:10 JHV
2, 4-Dinltmphenol EPA625 < 50ug/L 50.0 01/17/08 14:10 JHV
2-Nitrophen~l EPA625 < 10ugll 10.0 01/17108 14:10 JHV I 4-Nitmphenol EPA625 < 50ug/L 50.0 01/17108 14:10 JHV
Pentachlorophenol EPA625 < 20 ugll 20.0 0111710814:10 JHV
Phenol EPA625 <10ug/L 10.0 01/17/08 14:10 JHV I 2,4,6-Ttlchlorophenol EPA625 < 10 ugll 10.0 01/17/08 14:10 JHV
Acenaphthene EPA625 <10ug/L 10.0 01/17/08 14:10 JHV
Aceoaphthylene EPA625 < 10 ugll 10.0 01/17108 14:10 JHV I Anthracene EPA625 < 10ugll 10.0 01/17/0814:10 JHV
Benzo (a) anthracene EPA625 < 10 ugll 10.0 01/17/08 14:10 JHV
Benzo (b) ftuoranthene EPA625 < 10 ug/L 10.0 01/17/08 14:10 JHV I Benzo (k) fluoranthene EPA625 <10ug/L 10.0 01/17108 14:10 JHV
Benzo (g,h,l} perylene EPA625 < 1oug11.. 10.0 01/1710814:10 JHV
Benzo (a) pyrene EPA625 < 10ug/L 10.0 01/17/0814:10 JHV I . 4-Bmmophenyl phenyl ether EPA625 < 10 ugll 10.0 01/17/08 14:10 JHV
Butyl benzyl phthalate EPA625 < 10 ugll 10.0 01/17/08 14:10 JHV
bls (2-Chloroethoxy) methene EPA625 < 10ug/L 10.0 01/17108 14:10 JHV I bls (2-Chloroethyl) ether EPA625 < 10ug/L 10.0 01/17/08 14:10 JHV
bls (2-Chlorolsopropyt) ether EPA625 < 10ug/L 10.0 01/17/08 14:10 JHV
4-Chlomphenyt phenyl ether EPA625 < 10 ug/L 10.0 01/17/0814:10 JHV I Chryaene EPA625 <10ug/L 10.0 01/17/0814:10 JHV
Dlbenz {e,h) anthracene EPA625 < 10ug/L 10.0 01/17108 14:10 JHV
DI-n-butyl phthalate EPA625 < 10ug/L 10.0 01/17/08 14:10 JHV I 1,2-0lclllorobenzene EPA625 < 10ugJL 10.0 01/17/0814:10 JHV
1,3-Dlchlorobenzene EPA625 < 10ug/L 10.0 01/17/0814:10 JHV
1,4-D/chlombenzene EPA625 < 10 ug/L. 10.0 01/17/0814:10 JHV I
P~oA 13 nf44
I
I AIR
WATER I LABORATORIES, INC.•
I
2109A North Ham~ton Street • Riclunond, Vuginia 23230 • Tel: [phone] Fax: [phone]
Certificate of Analysis
I Final Report
laboratory Order ID 08010146
Client Name: APEX Companies, LLC. Date Received: January 11, 2008
I 6711 Peters Creek Road Date Issued: January 28, 2008
Suite 2Q1
Roanoke,VA 24019
I Submitted To: Robert Wagner Project Number: 768299.190
Client Site 1.0.: Short Stop Purchase Order: NA
I Sample 1.0.: 010908-190-03/ MW-1 Laboratory Sample I.D.: 08010146-003
DateiTime Sampled: 01/09/08 14:30 Analysis
Parameter Method Sample Results Rep Umlt Oate/Tlme Analyst
I Olethyl phthalate EPA625 <1ouwL 10.0 01117/0814:10 JHV
Dimethyl phthalate EPA625 <10ugll 10.0 01117/08 14:10 ·JHV
2,4-0inllrotoluene EPA625 < 10 ugll 10.0 01117108 14:10 JHV
I 2,6-0inltrotoluene EPA62.5 < 10ug/L 10.0 01/17/08 14:10 JHV
01-n-octyl phthalate EPA625 <10ug/L 10.0 01/17/08 14:10 JHV
bls (2-Ethythexyl) phthalate EPA625 < 10ug/L 10.0 01/17/08 14:10 JHV
I Fluoranthene EPA625 < 10ug/L 10.0 01/17/0814:10 JHV
Fluorene EPA625 < 10uWL 10.0 01/17/08 14:10 JHV
Hexachlorobenzene EPA625 < 10 ugJL 10.0 01/17/08 14:10 JHV
I Hexachlorobutadlene EPA625 <10uwL 10.0 01117/08 14:10 JHV
Hexachlorocyclopentadfene EPA625 < 10ugll 10.0 01/17/0814:10 JHV
Hexachloroethane EPA62S <10ug/L 10.0 01/17108 14:10 JHV
I lndeno (1.2,3-<:d) pYfene EPA625 <10ugll 10.0 01/17/0814:10 JHV
lsophorone EPA625 < 10ugfl 10.0 01/17/08 14:10 JHV
Naphthalene EPA625 < 10ug/L 10.0 01/17/0814:10 JHV
I Nitrobenzene EPA625 < 10 ugJL 10.0 01/17/08 14:10 JHV
N-Nitrosodlmethytamlne EPA625 < 10 ug/L 10.0 01/17/0814:10 JHV
N·Nitrosodlphenylamlne EPA625 < 10 ug/L 10.0 01/1710814:10 JHV
I N-Nitrosodi·N-propylamlne EPA625 < 10 ug/L 10.0 01/17108 14:10 JHV
Phenantlvene EPA625 < 10ug/L 10.0 01/17/0814:10 JHV
PYfene EPA625 < 10ugll 10.0 01/17/08 14:10 JHV
I 1,2.4·Trl~lorobenzene EPA625 < 10ug/L 10.0 01117/08 14:10 JHV
Benzidine EPA625 < 50ug/L 50.0 01/17/0614:10 JHV
3,3-0ichlorobenzldlne EPA625 <10ugll 10.0 01/17/08 14:10 JHV
I 2,3,4,6-Tetrachlorop~enol EPA625 < 10ug/L 10.0 01/17/08 14:10 JHV
2-Chloronaphthalene EPA625 < 10ugll 10.0 ,01/17/08 14:10 JHV
C~C18 Aliphatic Hydrocarbons MAOEP saeattach 10
I C11·C22 Aromatic HydrocaJb!lns MAOEP see attach 10
C 19-C36 Aliphatic Hydrocarbons MADEP see attach 10
Aliphatic Surrogate % Recovery MADEP see attach
I Fractionation Surrogate #1 Recovery MADEP see attach
P~n"' 1-i nf .L1
AIR
WATER
LABORATORIES, INC!'
2109A North Hamilton Street • Richmond, Vh·ginia 23230 • Tel: [phone] Fax: [phone]
Certificate of Analysis
Final Report
laboratory Order ID 08010146
Client Name: APEX Companies, LLC.
6711 Peters Creek Road
Suite 201
Roanoke,VA 24019
Submitted To: Robert Wagner
Client Site I.D.: Short Stop
Sample 1.0.: 010908-190-03/ MW-1
Date/Time Sampled: 01/09/08 14:30
Parameter
Aromallc Surrogate % Recovery
Fracllonatlon Surrogate #2 Reoov&f)'
C5-C8 Aliphatic Hydrocarbons
C9-C10 Aromatic Hydrocarbons
Method
MAOEP
MADEP
MADEP
MADEP
Date Received: January 11, 2008
Date Issued: January 28, 2008
Project Number: 768299.190
Purchase Order: NA .
Sample Results
see attach
see attach
see attach
aeeattach
Laboratory Sample 1.0.:
Analysis
Rep Limit OateiTlme
10
10
08010146-003
Analyst
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I AIR
WATER I INC~
2I09A North Hamilton Street • Richmond, Virginia 23230 • Tel: (804} 358-8295 Fax: '(804} 358-S297
I Certificate of Analysis
Final Report
I Laboratory Order 10 08010146
Client Name: APEX Companies, LLC. Date Received: January 11 , 2008
I 6711 Peters Creek Road Date Issued: January 28, 2008
Suite 201
Roanoke,VA 24019
I Submitted To: Robert Wagner Project Number: 768299.190
Client Site 1.0.: Short Stop Purchase Order: NA
I Sample I.D.: '010908-190-04/ MW-3 LaboratOI)' Sample 1.0.: 08010146.004
Oatefrime Sampled: 01/09/08 14:45 Analysts
Pan~mater Method Sample Results Rep limit DatefTime Analyst
I Lead SW7421 0.024 mg/L 0.002 01/15108 14:27 OMH
MTBE SM62100 < 5 ugll 5.0 01122108 16:43 DMB
01-lsopropyl ether {DIPE) SM62100 < 5 ugll 5.0 01/2210816:43 DMB
I Olchl04'odlfluoromethane SM62100 c 1 ugll 1.0 01/22108 16:43 DMB
Chloromethane SM62100 c 1 ug/1.. 1.0 01/2210816:43 DMB
Vln~ chloride SM62100 < 1 ugll 1.0 01122/08 16:43 DMB
I Bromomelhane SM62100 < 1 ug/1.. 1.0 01/22/08 16:43 DMB
Chloroeltlane SM62100 < 1 ug/1.. 1.0 01122103 16:43 OMS
T r1chloronuoromelhane SM62100 < 1 ug/L 1.0 01122108 16:43 . DMB
I 1, 1-Dichloroethytene SM62100 < 1 ug/L 1.0 01122108 16:43 DMB
.Methylene chl?~de SM62100· < 4 ug/L 4.0 01122108 16:43 DMB
trans-1 ,2-Dichlorcelhyleno SM62100 < 1 ug/L 1.0 01/22/08 16:43 DMB
I 1,1-Dichloroethane SM6210D < 1 ug/1.. 1.0 01}22108 16:43 DMB
2 ,2-Dlchloropropane SM6210D < 1 ug/1.. 1.0 01122108 16:43 DMB
cls-1,2·Dichloroethytene SM62100 < 1 ug/1.. 1,0. 01/22/08 16:43 DMB
I Bromochloromethane SM6210D < 1 ug/1.. 1.0 0112210816:43 DMB
Chloroform SM62100 . < 1 ug/1.. 1.0 01122/08 16:43 DMB
1 ,1,1-Trlchloroethane SM62100 < 1 ug/L 1.0 01122/08 16:43 DMB
I Carbon tetrachloride SM62100 < 1 ug/L 1.0 01122/08 16:43 OMS
1,1-0fchloropropene SM6210D <1ug/L 1.0 01122/0816:43 OMS
Benzene SM62100 < 1 ug/L 1.0 01/22/08 16:43 DMB
I 1 ,2-0ichloroethane SM62100 < 1 ug/1.. 1.0 01/22108 16:43 DMB
Trichloroethylene SMS2100 < 1 ug/1.. 1.0 01/22/08 16:43 DMB
1 ,2-Dichloropropane SM62100 < 1 ug/1.. 1.0 01/22/08 16:43 DMB
I Olbromomelhane SM62100 < 1 ug/1.. 1.0 01/22/08 16:43 DMB
Bromodlchforomethane SM62100 < 1 ug/1.. 1.0 01122/08 16:43 DMB
cls-1,3-Dlchloropropene SM62100 < 1 ug/L 1.0 01/22/08 16:43 DMB
I 4-Methyl-2-pentanone (MIBK) ~M62100 < 10 ug/L 10.0 01/22/08 16:43 DMB
Toluene SM62100 < 1 ug/L 1.0 01122/08 16:43 DMB
1,1,2-Trlchloroethane SM62100 < 1 ug/1.. 1.0 01122108 16:43 DMB
I Te~achloroethylene (PCE) SM62100 < 1 ugll 1.0 01/22/08 16;43 DMB
Page 16 of 44
AIR
WATER
LABORATORIES, INC:'
2109A North Hamilton Street " Richmond, Virginia 23230 • Tel: [phone] Fax: [phone]
Certificate of Analysis
Final Report
Laboratory Order ID 08010146
Client Name: APEX Companies, LLC. Date Received: January 11, 2008
6711 Peters Creek Road Date Issued: January 28, 2008.
Suite 201
Roanoke,VA 24019
Submitted To: Robert Wagner Project Number: 768299.190
Client Site I.D.: Short Stop Purchase Order: NA
·Sample 1.0.: 010908.190-04 I MW-3 Laboratory Sample I. D.: 08010146-004
Oatefflme Sampled: 01/09/08 14:45 Analysis
Parameter Method Sample Results RepUmlt Oatelllme Analyst
1,3·Dichloropropane SM62100 < 1 ug/L 1.0 01/22108 16:43 OMB
Olbromochloromethane SM62100 < 1 ug/L 1.0 01122108 16:43 DMB
1,2-Dibromoethane (EOB) SM62100 < 1 ugiL 1.0 01122/0816:43 DMB
Chlorobenzene SM62100 < 1 ugiL 1.0 01122/08 16:43 DMB
1,1,1,2-Tetrachloroethane SM62100 < 1 ug/L 1.0 01122/0816:43 OMB
Elhyfbenzene SM62100 < 1 ugiL 1.0 01122/0816:43 OMB
m,p-Xytenes SM62100 < 2 ugll 2.0 01/22108 16:43 OMB
o-Xylene SM62100 < 1 ugiL 1.0 01122/08 16:43 DMB
Xylenes, Total SM62100 < 3 ugiL 3.0 01122/08 16:43 DMB
Styrene SM62100 < 1 ugll 1.0 01/22108 16:43 OMB
Bromoform SM62100 < 1 ugll 1.0 01122108 16:43 DMB
lsopropylbenzene SM62100 < 1 ugll 1.0 01122108 16:43 DMB
Bromobenzene SM62100 < 1ugiL 1.0 01122108 16:43 DMB
1,1.2,2-Tetrac::hloroethane SM62100 < 1 ugiL 1.0 01122/0816:43 DMB
1,2,3-Ttlchloropropane SM62100 < 1 ugll. 1.0 01/22/08 16:43 DMB
n-Propytbenzene SM82100 < 1 ug/L 1.0 01/22/08 16:43 DMB
2 -Chlorotoluene SM62100 < 1 ugJL 1.0 01122108 18:43 DMB
4-Chlorotoluene SM62100 <1ug/L 1.0 01122/08 16:43 DMB
1,3,5-Trlmethylbenzene SM6210D <1ugll.. 1.0 01/22/08 16:43 OMB
tert-Butylbenzene SM6210D < 1 ug/L 1.0 01122/08 16:43 OMS
1 ,2,4-Trlmethylbenzene SM6210D < 1 ugll. 1.0 01122/08 16:43 OMB
aec-Butyloenzene SM62100 < 1 ugll 1.0 01/22/08 16:43 DMB
1,3-Dichlorobenzene SM62100 < 1 ugll. 1.0 01122108 16:43 OMB
p-lsopropyltoluene SM62100 < 1 ugll 1.0 01122/08 16:43 DMB
1,4-Dichlorobenzene SM62100 < 1 ugll 1.0 01122/08 16:43 DMB
1,2-Dichlorobenzene SM62100 < 1 ugiL 1.0 01/22108 16:43 DMB
n-Butyibenzene SM62100 <.1 ugll. 1.0 01/22108 16:43 DMB
1,2-0ibromo-3-chloropropane (DBCP) SM62100 < 4ug/L 4.0 01/22/08 18:43 OMB
1.2, 4-Trlchlorobenzene SM62100 < 1 ugll 1.0 01/22108 16:43 DMB
Hexachlorobutadlene SM62100 < 1 ugiL 1.0 01/22/08 16:43 DMB
Naphthalene SM6210D < 1 ug/L 1.0 01/22/08 16;43 DMB
1,2,3-Trichlorobenzene SM62100 < 1 ug/L 1.0 01122/08 16:43 OMB
c.,,. .. 1'7 ,..~ AA
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I LABORATORIES, rNc.•
2109A North Hamilton Street • Richmond, Vtrginia 23230 • Tel: (804} 358-8295 Fax: [phone]
I · Certificate of Analysis
Final Report
I Laboratory Order 10 08010146
Client Name: APEX Companies, LLC. Date Received: January 11, 2008
I 6711 Peters Creek Road Date Issued: January 28, 2008
Suite 291
Roanoke, VA 24019
I Submitted To: Robert Wagner Project Number: 768299.190
Client Site I.D.; Short Stop Purc.hase Order: NA
I Sample I.D.: 010908-190-Q4/ MW-3 Laboratory Sample I.D.: 08010146-Q04
Date!Time Sampled: 01/09/08 14:45 Analysis
Parameter Method Sample Results Rep UmJt Date/Time AnalyBt
I 4-Ch\oro-3-methylphenol EPA625 < 10 ugll. 10.0 01{17108 14:42 JHV
2-Chloi'Ophanol EPA625 <10ug/L 10.0 01/17108 14:42 JHV
2,4-0lchlomphenol EPA625 < 10ugll 10.0 01117/08 14:42 JHV
I . 2,4-0imethytphenol EPA625 < 10 ugll 10.0 01/17/08 14:42 JHV
4,6-Dinllro·2-mathytphenol EPA625 <50 ugll 50.0 01/17/08 14:42 JHV
2,4-Dinltrophenol EPA625 <50 ug/L 50.0 01/17/08 14:42 JHV
I 2-Nitrophen.ol EPA625 < 10ugll 10.0 01/17/08 14:42 JHV
4-Nitrophenol EPA625 < 50ug/L 50.0 01/17/08 14:42 JHV
Penlachlorophenol EPA625 < 20 ug/L 20.0 01/17/0814:42 JH~
I Phenol EPA625 < 10 ugiL 10.0 01/17~ 14:42 JHV
2,4,6-Trlchlorophenol EPA625 < 10 ugll 10.0 01/17/0814:42 JHV
Acenaphthene EPA625 <10ug/L . 10.0 01/17/0814:42 JHV
I Aceoaphthytena EPA625 <10ugll 10.0 01/17108 14:42 JHV
Anthrucene EPA625 <10ugiL 10.0 01/1710814:42 JHV
Benzo (a) anthracene ·EPA625 < 10 ug/L 10.0 01/17/08 14:42 JHV
I Benzo (b) lluoranthene EPA625 < 10 ug/L 10.0 01/17/08 14:42 JHV
Benzo (k) lluoranthllt1e EPA625 < 10ug/L 10.0 01/17/0814:42 JHV
Benzo (g,h,l) perytene EPA625 < 10 ug/L 10.0 01117/08 14:42 JHV
I Benzo (a) pyrene EPA625 <10ugll. 10.0 01/1710814:42 JHV
. 4-Bromophenyl phenyl ether EPA625 < 10 ugll· 10.0 01117/0814:42 JHV
Butyl benzyl phthalate EPA625 < 10 ug/L 10.0 01/17108 14:42 JHV
I bls (2·Chloroethoxy) methane EPA825 < 10ugll. 10.0 01117/08 14:42 JHV
bl8 (2-Chloroethyl) ether EPA625 < 10 ug/L 10.0 01/17/0814:42 JHV
bls (2-Chlorolsopropyl) ether EPA625 < 10 ug/L 10.0 01117108 14:42 JHV
I 4-Chlorophenyl phenyl ether EPA625 <10ugiL 10.0 01{17/0814:42 JHV
Chrysene EPA625 <10ug/L 10.0 01/17108 14:42 JHV
Olben% (a,h) anthrucene EPA625 <10ug/L 10.0 01/17108 14:42 JHV
I 01~-butyf phthalate EPA625 <10ug/L 10.0 01/17/08 14:42 JHV
1.2-0lchlorobenzana EPA625 < 10 ugll 10.0 01/17108 14:42 JHV
1,3-0ichlorobenzene EPA625 < 10 ugll 10,0 01/17108 14:42 JHV
I 1 ,4-0lchlorobenzene EPA625 < 10 ugll. 10.0 01/17/08 14:42 JHV
Page 18 of 44
AIR
WATER
lABORATORIES, INC.:' .
2109A North Hamilton Street • RichmonJ, Virginia 23230 • Tel: {804) 358-8295 Fax: [phone]
Certificate of Analysis
Final Report
Laboratory Order ID 08010146
Client Name: APEX Companies, LLC. · Date Received: January 11, 2008
6711 Peters Creek Road Date Issued: January 28, 2008
Suite 201
Roanoke,VA 24019
Submitted To: Robert Wagner Project Number: 768299.190
Cl.lent Site 1.0.: Short Stop Purchase Order: NA
Sample 1.0.: 010908-190-04/ MW-3 Laboratory Sample I. D.: 08010146-004
Date/Time Sampled: 01/09/08 14:45 Analysis
Parameter Method Sample Results Rep Limit Date/Time Analyst
Dlethyl phthalate EPA625 < 10 ugll 10.0 01/17/08 14:42 JHV
Dimethyl phthalate EPA625 < 10 ugll· 10.0 01117/08 14:42 JHV
2,4-Dinltrotoluene EPA625 < 10 ug/L 10.0 01/17/08 14:42 JHV
2,6-Dinlln:lto!uene EPA625 < 10 ug/L 10.0 01/17(08 14:42 JHV
Dl-n-octyt phthalate EPA625 < 10 ugll 10.0 01117108 14:42 JHV
bls {2-Ethylhexyl) phthalate EPA625 < 10 ug/L 10.0 01117/0814:42 JHV
Fluotanlhene EPA625 < 10 ug/L 10.0 01/17/0814:42 JHV
Fluorene EPA625 < 10 ug/L 10.0 01/17/0814:42 JHV
Hexachlorobenzene EPA625 <10ug/L 10.0 01/17/08 14:42 JHV
Hexachlorobutadlene EPA625 < 10 ugll 10.0 01/17/0814:42 JHV
Hexachlorocyclopentadlena EPA625 < 10 ug/L 10.0 01/17/08 14:42 JHV
Hexachloroethane EPAB25 < 10 ug/L 10.0 01/17/0814:42 JHV
lndeno ( 1,2,3-cd) pyrene EPA625 <10ugJL 10.0 01/17/08 14:42 JHV
lsophorone EPA625 < 10ugll 10.0 01/17108 14:42 JHV
Naphthalene EPA625 < 10 ugll 10.0 01/17108 14:42 JHV
Nitrobenzene EPA625 < 10ugll 10.0 01/17108 14:42 JHV
N-Nitrosodlmelhylamlne EPA625 < 10ug/L 10.0 01/17/08 14:42 JHV
N-Nitrosodlphenylamlne EPA625 < 10ug/L 10.0 01/17/0814:42 JHV
N-NIIrosodl-N-propylamlne EPA625 < 10ugiL 10.0 01/17108 14:42 JHV
Phenanthrene EPA625 < 10u9fl 10.0 01/17108 14:42 JHV
Pyrene EPA625 < 10 ug/L 10.0 01/17/0814:42 JHV
1,2,4-Trlchlorobenzene EPA625 < 10 ug/L 10.0 01/17/0814:42 JHV
BenzJdlne EPA625 <50 ug/L 50.0 01/1710814:42 JHV
3 ,3-Dichlorobenzldlne EPA625 < 10 ug/L 10.0 01/17108 14:42 JHV
2,3,4,6-Tetmchlorophenol EPA625 < 10 ugJl 10.0 01/17/0814:42 JHV
2-Chloronaphthalene EPA625 < 10ug/l 10.0 01/17/0814:42 JHV
C9-C18 AllphaUc Hydrocalbons MADEP see attach 10
C11·C22 Aromatic Hydrocarbons MADEP see attach 10
C19-C36 Aliphatic Hydrocarbons MADEP see attach 10
Aliphatic Surrogate % Recovery MAOEP see attach
FracllonaUon Surrogate #1 Recovery MADEP see attac~
c...,.,..._ ... I\-~ AA
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. AIR
WATER
LABORATORJES,I~C~
2109A North Hamilton Street • Richmond, Vtrginia 23230 • Tel: {804) 368-8296 FaJC: [phone]
Certificate of Analysis
Final Report
Laboratory Order ID . 08010146
Client Name: APEX Companies, LLC.
6711 Peters Creek Road
Suite 2Q1
Roanol<e,VA 24019
Submitted To: Robert Wagner
Client Site 1.0.: Short Stop
Sample 1.0.: 010908-190-04/ MW-3
Datefflme Sampled: 01/09/08 14:45
Parameter Method
Aromatic Surrogate % Recovery MADEP
Fractionation Surrogate #2 Recovery MADEP
C5-C8 AllphaUc Hydrocarbons MAOEP
C9-C10 Aromatic Hydrocarbons MADEP
Date Received: January 11, 2008
Date Issued: January 28, 2008
Project Number: 768299.190
Purchase Order: NA
Laboratory Sample 1.0.: 08010146"004
Analysis
Sample Resulls Rep Umlt Date/Tlme Analyst
see attach
see attach
see attach
sea attach
10
10
I
AIR I
WATER I LABORATORIES, INC!
2109A North Hamilton Street • Richmond, Vlr:ginia 23230 • Tel: [phone] Fax: [phone] I Certificate of Analysis
Final Report I Laboratory Order 10 08010146
Client Name: APEX Companies, LLC. Date Received: January 11, 2008
6711 Peters Creek Road Date Issued: January ~8. 2008 I Suite 201
Roanoke,VA 24019
Submitted To: Robert Wagner Project Number: 768299.190 I
Client Site LD.: Short Stop Purchase Order: NA
Sample 1.0.: 010908-190-05 I MW-4 laboratory Sample 1.0.: 08010146-005 I DatefTime Sampled: 01/09/08 14:25 Analysis
Parameter Method Sample Results Rep Umlt Date/Tlme Analyst
Lead SW7421 0.043mg/L 0.002 01/15108 15:17 DMH I MTBE SM62100 · 9.7 ugA. 5.0 01122/08 18:54 DMB
Dl..Jsopropyl ether (DIPE) SM62100 < 5 ugiL 5.0 01122/08 18:54 DMB
Dlchlorodlfluoromethane SM62100 < 1 ugll 1.0 01/22108 18:54 OMB I Chloromethane SM62100 < 1 ugll 1.0 01/22108 18:54 OMB
VInyl chloride SM6210D < 1 ugiL 1.0 01122/08 18:54 DMB
Bromomethane SM82100 < 1 ugll 1.0 01122/08 18:54 DMB I Chloroethane SM62100 < 1 ug/1. 1.0 01122/08 18:54 OMB
lrlchlorofluoromethane SM6~100 < 1 ug/L 1.0 01/22108 18:54 DMB
1,1-Dichloroethylene SM62100 < 1 ug/L 1.0 01/22/08 18:54 DMB I Methylene chloride SM62100 < 4 ugiL 4.0 01/22108 18:54 DMB
trans-1,2-0ichloroethylene SM6210D < 1 ugll 1.0 01/22/08 18:54 OMB
1,1-Dichlcroethane SM62100 < 1 ugiL 1.0 01/22108 18:54 DMB I 2,2-Dichloropropane SM62100 < 1 ugll 1.0 01122/08 18:54 DMB
cls-1,2-Dichloroethylene SM62100 < 1 ugll.. 1.0 01122/0818:54 DMB
Bromochloromethane SM62100 < 1 ug/L 1.0 01/22/08 18:54 DMB I Chloroform SM62100 < 1 ug/L 1.0 01/22/08 18:54 OMS
1,1,1-Trlchloroeltlane SM6210D < 1 ugJl 1.0 01122108 18:54 ·OMS
Carbon tetrachloride SM62100 < 1 ugiL 1.0 01122/08 18:54 DMB I 1, 1-Dichloropropene SM6210D < 1 ugiL 1.0 01122/08 18:54 OMB
Benzene SM6210D < 1 ug/L 1.0 01/22/0818:54 DMB
1,2-Dichloroethane SM6210D 3.2 ugll 1.0 01/22108 18:54 DMB I Trichloroethylene SM62100 < 1 uglt 1.0 01122/08 18:54 OMB
1,2-Dichloropropane SM6210D < 1 ug/L 1.0 01/22/08 18:54 DMB
Dlbromomethane SM6210D < 1 ug/L 1.0 01/22/08 18:54 DMB I Bromodlchloromethane SM6210D < 1 ugll 1.0 01122/08 18:54 DMB
cls-1,3-D!chloropropene SM6210D < 1 ug/L 1.0 01122/08 18:54 OMB
4-Methyl-2-pentanone (MIBK) SM6210D < 10 ug/L 10.0 01/22/08 18:54 DMB I Toluene SM6210D < 1 ugiL 1.0 01122/0818:54 OMB
1.1,2-Trlchloroethane SM6210D < 1 ug/L 1.0 01/22/08 18:54 OMB
Tetrachloroethylene {PCE) SM6210D 7.8 ugiL 1.0 01/22/08 18:54 OMB I
o,.,..,. 'l~ ..,f II A
I
I AIR
WATER I LABORATORIES, INC~
I
2109A North Hamilton Street • Richmond, Virginia 23230 • Tel: [phone] Fax: [phone]
Certificate of Analysis
I Final Report
Laboratory Order 10 08010146
Client Name: APEX Companies, LLC. Date Received: January 11 , 2008
I 6711 Peters Creek Road Date Issued: January 28, 2008
Suite 201
Roanoke,VA 24019
I Submitted To: R~~ert Wagner Project Number: 768299.190
Client SltelD.: Short Stop Purchase Order: NA
I Sample 1.0.: 010908-190-05/ MW-4 Laboratory Sample 1.0.: 08010146..005
DatefTime Sampled: 01/09/08 14:25 Analysis
Parameter Method Sample Results Rep Limit OatWT'Ime Analyst
I 1 ,3-Dichloropropane SM6Z100 < 1 ugiL 1.0 01122108 18:54 OMB
Dlbromochloromethane SM62100 < 1 ug/L 1.0 0112210818:54 DMB
1,2·Dibromoelhane (EDB) SM62100 < 1 ugll 1.0 01122108 18:54 DMB
I Ch!orobenzene SM6210D < 1 ug/L 1.0 01122/08 18:54 DMB
1.1, 1 ,2-Tetrac:Noroethane SM62100 < 1 ugiL 1.0 01122108 18:54 DMB
Ethytbenzene SM62100 < 1 ug/L 1.0 01122/0818:54 OMB
I m,p-Xylenea SM6210D < 2 ug/L 2.0 01/22/08 18:54 DMB
o-Xylane SM62100 < 1 ug/l 1.0 01122108 18:54 OMB
Xytenes, Total SM62100 <3 ug/L• 3.0 01122108 18:54 OMS
I Styrene SM62100 < 1 ug/L 1.0 01122/08 18:54 OMB
Bromoform SM62'100 < 1 ugiL 1.0 01122/0818:54 OMB
I sopropylbenzene SM62100 < 1 ug/L 1.0 01/22/0818:54 DMB
I Bromobenzene SM62100 < 1 ugll. 1.0 01122108 18:54 OMB
1,1,2,2-Tetrachloroelhane SM62100 < 1 ug/L 1.0 0112210818:54 DMB
1,2,3-Trlchloropropane SM6210D < 1 ugll 1.0 01/22108 18:54 DMB
I n·Propylbanzene SM62100 < 1 ugiL 1.0 01/22/()818:54 DMB
2-Chlorotoluane SM62100 < 1 ugll. 1.0 01122/0818:54 DMB
4-Chlorotoluene SM6210D < 1 ug/L 1.0 01122108 18:54 DMB
I 1,3,5-Tnmethylbenzane SM62100 < 1 ug/L 1.0 01122108 18:54 DMB
tert·Butylbenzene SM6210D < 1 ug/L 1.0 01/22108 18:54 DMB
1,2, 4-Trfmethylbenzene SM6210D < 1 ug/L 1.0 01122/08 18:54 DMB
I aao-Butylbenz~ne SM62100 < 1 ug!L 1.0 01/2210818:54 DMB
1,:J:.Oichlorobenzene SM62100 < 1 ug/L 1.0 0112.2108 18:54 DMB
p·lsopropylto.luene SM6210D < 1 ugiL 1.0 01122/08 '18:54 DMB
I 1,4-0ichlorobenzene SM6210D < 1 ugll 1.0 0112210818:54 DMB
1 ,2·Dfchlorobenzene SM6210D < 1 ug/L 1.0 01122/08 18:54 DMB
n-Butylbenzena SM62100 < 1 ugll 1.0 01122/08 18:54 DMB
I · 1,2-0ibromo-3-chloropropane rDBCP> SM62100 <4 ug/L 4.0 01/22/08 18:54 DMB
1,2,4-Trlchlorobanzene SM6210D < 1 ugll 1.0 01122108 18:54 DMB
Hexachlorobutadlene SM6210D < 1 ugll 1.0 01/22/08 18:54 DMB
I Naphthalene SM62100 < 1 ug/L 1.0 01/22/()818:54 OMB
1,2,3-T ri<:hlorobenzene SM62100 < 1 ug/L 1.0 01122/0818:54 OMB
0,...,.._ ')"'l -t. A A
AIR
WATER
LABORATORIES, INC!"
2109A North Hamilton Street • Richmond, Vuginia 23230 • Tel: {804) 358-8295 Fax: (804} 358-8.297
Certificate of Analysis
Final Report
Laboratory Order 10 08010146
Client Name: APEX Companies, LLC. Date Received: January 11, 2008
6711 Peters Creek Road Date Issued: January 28,.2008
Sulte201
Roanoke,VA 24019
Submitted To: Robert Wagner Project Number: 768299.190
.Client Site 1.0.: Short Stop Purchase Order: NA
Sample 1.0.: 010908·190..05/ MW-4 laboratory Sample 1.0.: 0801 014S..005
Datemme Sampled: 01/09/08 14:25 Analysis
Parameter Method Sample Results RepUmlt Oate/Tlme Analyst
4-Chloro-3-methylphenol EPA625 < 10 ugll 10.0 0111710815:15 JHV
2-Chlorophenol EPA625 < 10 ugJL 10.0 01/17/0815:15 JHV
2.4-Dichlorophenol EPA625 < 10ug/L 10.0 01/17/0815:15 JHV
2,4-Dimethylphenol EPA625 < 10ug/L 10.0 01/17/0815:15 JHV
4,6-Dinltro-2-methylphenol EPA625 < 50ug/L 50.0 01117/0815:15 JHV
2,4-:Dinltrophenol EPA625 < 50ug/L 50.0 01/17/0815:15 JHV
2-Nitrophenol EPA625 < 10 ug/L 10.0 01/17/08 15:15 JHV
4-Nltrophenol EPA625 <50 ug/L 50.0 01/17/08 15:15 JHV
Pentachlorophenol EPA625 < 20ug/L 20.0 01/17/0815:15 JHV
Phenol EPA625 < 10 ug/L 10.0 01(17/08 15:15 JHV
.2,4,6-Trlchlorophenol EPA625 < 10 ugll. 10.0 01117/0815:15 JHV
Acenaphthene EPA625 < 10 ugJL 10.0 01/17/08 15:15 JHV
Acenaphthylene EPA625 < 10 ug/L 10.0 01/17/08 15:15 JHV
Anthracene EPA625 < 10ugll 10.0 01/17/08 15:15 JHV
Benzo (a) anthracene EPA625 < 10 ug/L 10.0 01/17/08 15:15 JHV
Benzo (b) fluornnthene EPA625 < 10ug/L 10.0 01/17/0815:15 JHV
Benzo (k) fluoranlhene EPA625 < 10ug!L 10.0 01/17/0815:15 JHV
Benzo (g,h,l) perylene EPA625 < 10 ug/L 10.0 01/17108 15:15 JHV
Benzo (a) pyrene EPA625 <1Dug/L 10.0 01/17/0815:15 JHV
4-Bromophenyl phenyl ether EPA625 <10ug/L 10.0 01117/08 15:15 JHV
Butyl benzyl phthalate EPA625 < 10 ug/L 10.0 01/17/0815:15 JHV
bls (2-Chloroethoxy) methane EPA625 < 1Dug/L 10.0 01/17/08 15:15 JHV
bls (2-Chloroethyl) ether EPA625 < 10 ug/L 10.0 01/17/08 15:15 JHV
bls (2-Chlorolsopropyl) ether EPA625 < 10ug/L 10.0 01/17/08 15:15 JHV
4-Chlorophenyl phenyl ether EPA625 < 10ug/L 10.0 01/17/08 15:15 JHV
Chrysene EPA625 < 10 ug/L 10.0 01/17/08 15:15 JHV
Olbenz (a,h) anthracene EPAS25 < 10ug/L 10.0 01/17/08 15:15 JHV
DI-n-butyl phthalate EPA625 < 10ug/L 10.0 01/17/08 15:15 JHV
1,2·Dichlorober)zene EPA625 < 10ug/L 10.0 01/17/08 15:15 JHV
1.~Dichlorobenzene EPA625 < 10 ug!L 10.0 01/17/0815:15 JHV
1 ,4-Dfchlorobenzene EPA625 < 10 ug/L 10.0 01/17/08 15:15 JHV
Page 23 of 44
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I LABORATORIES, INC.•
I
2109A North Hamilton Street • Richmond, V~.rginia. 23230 • Tel: [phone] Fax: [phone]
Certificate of Analysis
I
Final Report
Laboratory Order 10 08010146
Client Name: APEX Companies, LLC. Date Received: January 11, 2008
I 6711 Peters Creek Road Date Issued: January 28, 2008
Suite 201
Roanoke,VA 24019
I Submitted To: Robert Wagner Project Number: 768299.190
Client Site 1.0 .: Short Stop Purchase Order: NA
I Sample 1.0.: 010908-190-05/ MW-4 Laboratory Sample J.D.: 08010146-005
Date/Time Sampled: 01/09/08 14:25 Analysis
Parameter Method Sample Results Rep Umlt Date/Time Analyst
I orethyi phthalate EPA625 <10ugJL 10.0 01117108 15:15 JHV
Dimethyl phthalate EPA625 < 10 ugJL 10.0 01/1710815:15 JHV
2 ,4-0tnltmtoluene EPA625 < 10 ug,\. 10.0 01 /1710815:15 JHV
I 2,6-Dinltrotoluene · EPA625 <10ug/L 10.0 01/17/08 15:15 JHV
01-n-octyl phthalate EPA625 < 10 ugfL 10.0 01/17/08 15:15 JHV
bls (2-Ethylhexyl) phthalate EPA625 < 10ug/L 10.0 01/17/08 15:15 JHV
I Fluoranthene EPA825 < 10ugfl 10.0 01/17/()8 15:15 JHV
Fluorene EPA625 < 10 ugJL 10.0 01/17/08 15:15 JHV
.Hexachlorobenxene EPA625 <10ugJL 10.0 01/17108 15:15 JHV
I Hexachlorobutadlene EPA625 <10ug/L 10.0 01/17/08 15:15 JHV
. Hexachlorocyclopentadlene EPA625 < 10ug/L 10.0 01/17/08 15:15 JHV
Hexachloroethane EPA625 < 10uglt 10.0 01/17/08 15:15 JHV
I lndeno (1,2,3-cd) pyrene EPA625 <10ugJL 10.0 01/17/08 15:15 JHV
lsophorone EPA625 <10ug/L 10.0 01/17108 15:15 JHV
Naphthalene EPA625 < 10 ugiL 10.0 01/17/08 15:15 JHV
I Nltroben'lene EPA625 < 10 ug/L 10.0 01117/0815:15 JHV
N-Nitrosodlmethyiamlne EPA625 < 10ug/L 10.0 01/17108 15:15 JHV
N-Nitrosodlphenylamlne EPA625 < 10ug/L 10.0 01/17/08 15:15 JHV
I N-Nltrosodi-N-propylamlne EPA625 < 10ugiL 10.0 01/17/08 15:15 JHV
Phenanthrene EPA625 <10ug/L 10.0 01/11/08 15:15 JHV
Pyrene EPA625 <10ugll.. 10.0 01117108 15:15 JHV
I 1 ,2,+ Trlchlorobenzene EPA625 < 10 ug/L 10.0 01/17/0815:15 JHV
Benzidine. EPA625 < 50 ugJL 50.0 01/17108 15:15 JHV
3 ,3-0ichlorobenzldlne EPA625 < 10 ug/L 10.0 01/17/08 15:15 JHV
I 2,3;4,6-Tetrachlorophenol EPA625 < 10ug/L 10.0 01/17/08 15:15 JHV
2-Chloronaphthalene EPA625 <10ug1L 10.0 01/17108 15:15 JHV
C9-C18 Allphetlc Hydrocart)ona MADEP seeauach 10
I C11·C22 Aromatic Hydrocarbons MADEP see attach 10
C19-C36 Aliphatic H~rocarbons MADEP see attach 10
Aliphatic Surrogate % Recovery MADEP see attach
I Frae1lonatlon Surrogate #1 Recovety MADEP see attach
P:m"' ?d nf oild
AIR
WATER
LABORATORIES, INC!
2109A Nortb Hamilton Street • Richmond, Virginia 23230 • Tel: [phone] Fax: [phone]
Certificate of Analysis
Final Report
Laboratory ·order 10 08010146
Client Name: APEX Companies, LLC.
6711 Peters Creek Road
Suite 201
Roanoke,VA 24019
Submitted To: Robert Wagner
Client Site I.D.: Short Stop
Sample t.D.: 010908-190-05/ MW-4
Date/Time Sampled: 01/09/08 14:25
Parameter
Aromatic Surrogate % Recovery
Fractionation Surrogate #2 Recovery
C5-C8 Aliphatic Hydrocarbons
C9-C10 Aromatic Hydrocarbons
Melhod
MADEP
MAOEP
MAOEP
MAOEP
Date Received:
Date Issued:
Project Number:
Purchase Order:
January 11, 2008
January 28, 2008
768299.190
NA
Laboratory Sample 1.0.: 08010146-005
Analysis
~~~~ ~~~~~e ~~
see attach
eee attach
see attach 10
see attach 10
Page 25 of 44
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I AIR
WATER I LABORATORIES, INC.•
I
2109A North Hamilton Street • Richmond, Virginia 23230 • Tel: [phone] Fax: [phone]
Certificate of Analysis
I Final Report
Laboratory Order ID 08010146
Client Name: APEX Companies, LLC. Date Received: January 11, 2008
I 6711 Peters Creek Road Date Issued: January 28, 2008
Suite 201
Roanoke,VA 24019
I Submitted To: Robert Wagner Project Number: 768299.190
Client Site 1.0.: Short Stop Purchase Order: NA
I Sample I.D.: 010908-190-06/ MW-5 laboratory Sample I.D.: 08010146-006
Date/Time Sampled: 01/09/08 14:00 Analysis
Parameter Method Sample Results Rep Umlt DateiTime Analyst
I Lead SW7421 0.236 mgll. 0.002 01/1510815:35 DMH
MTBE SM62100 < 5 ugiL 5.0 01122/08 17:09 OMB
Dl-lsopropyl ether (DIPE) SM62100 < 5 ugll 5.0 01r12.10817:09 DMB
I Dlchlorodlfluoromethane SM6210D < 1 ugll 1.0 01122/08 17:09 OMB
ChiOfomethane SM62100 < 1 ug/L 1.0 01122/08 17:09 OMS
VInyl chloride SM62 100 < 1 ug/1. 1.0 0112210817:09 DMB
I Bromomethane SM6210D ·<1ug/L 1.0 01122/08 17:09 DMB
Chloroethane SM62100 < 1 ug/L 1.0 01122/08 17:09 DMB
Tnchlorofluoromethane · SM62100 < 1 ugll. 1.0 01122/08 17:09 DMB
I 1,1-Dlchloroethytene SM6210D < 1 ugll 1.0 01/22/08 17:09 DMB
.Methylene chloride SM6210D < 4ugll 4.0 . 01/22/08 17:09 OMB
trans-1,2..{llchloroethylone SM62100 < 1 ugJL 1.0 01122108 17;09 DMB
I 1,1-0ichloroethane SM62100 < 1 ugll 1.0 01/22108 17:09 DMB
2,2-0lchloropropane SM62100 < 1 ug/L 1.0 01122/0817:09 DMB
cls-1,2-0ichloroethylene SM6210D 6.8ug/L 1.0 01/22108 17:09 DMB I Bromochloromelttane SM6210D < 1 ugiL 1.0 01/22108 17:09 DMB'
Chloroform SM62100 ·< 1 ugll 1.0 01/22/0817:09 DMB
1,1,1-Trtchloroethane SM62100 < 1 ugll 1.0 01122108 17:09 DMB
I Carbon tetrachloride SM62100 < 1 ugll 1.0 01122108 17:09 DMB
. 1,1-0ichloropropene SM62100 < 1 ug/L 1.0 01/22/0B 17:09 OMB
Benzene SM62100 < 1 ugJL 1.0 01122108 17:09 DMB
I 1.2-0ichloroethane SM62100 < 1 U9IL 1.0 01122/08 17:09 DMB
Trichloroethylene SM62100 3.3 ugJL t.O 01122108 17:09 DMB
1 ,2-Dichloropropane SM6210D < 1 ugJL 1.0 01/22/08 17:09 DMB
I Dlbromomethane SM6210D ·< 1 ugll 1.0 01122108 17:09 DMB
Bromodichloromelttane . SM6210D < 1 ug/L 1.0 01122108 17:09 DMB
c1&-1,3-0ichloropropene SM62100 < 1 ugiL 1.0 01122/08 17:09 DMB
I 4-Methyl-2-pentanone (MI BK) SM62.10D < 10 ug/L 10.0 01122108 17:09 DMB
' Toluene SM62.10D < 1 ugll 1.0 01122/08 17:09 DMB
1,1,2-Trlchloroethane SM6210D < 1 ugll 1.0 01122/08 17:09 DMB
I Tetrachloroethylene (PCE) SM6210D 28.5ugll_ 1.0 01122/08 17:09 DMB
r"'\--• ""' -L • '
I
·AIR I WATE R I LABORATORIES, INC!'
2109A North Ha.m.ilton Street • Richmond, Virginia 23230 • Tel: [phone] Fax: [phone] I Certificate of Analysis
Final ~eport I Laboratory Order ID 08010146
Client Name: APEX Companies, LLC. Date Received: January 11, 20Q8
6711 Peters Creek Road Date Issued: January 28, 2008 I Suite 291 .
Roanoke,VA 24019
Submitted To: Robert Wagner Project Number: 768299.190 I Client Site I. D.: Short Stop Purchase Order: NA
Sample 1.0.: 010908-190-06 / MW-5 Laboratory Sample 1.0.: 08010146-006 I Date/Time Sampled: 01/09/08 14:00 Analysis
Pen~meter Method Sample Results Rep Umlt Data'Time Analyst
1,3-Dichloropropane SM6210D < 1 ug/L 1.0 01/22/08 17:09 DMB I Dlbromochloromethane SM6210D < 1 ug/L 1.0 01/22108 17:09 DMB
1.2-Dibromoethane (EDB) SM62100 < 1 ug/L 1.0 01122108 17:09 DMB
Chlorobenzena SM6210D < 1 ug/L 1.0 01122/08 17:09 DMB I 1,1, 1,2· Tetrachloroethane SM62100 < 1 ugiL 1.0 01/22108 17:09 OMB
Ethytbenzene SM62100 < 1 ug/1.. 1.0 01/22JQ8 17:09 DMB
m,p-Xylenes SM62100 ..; 2 ug/L 2.0 01/2210817:09 DMB I o-Xylena SM62100 < 1 ugll 1.0 01/22108 17:09 DMB
Xyleoes. Total SM6210D < 3 ug/L 3.0 01/22/0817:09 OMS
Styrene SM6210D < 1 Ug/L 1.0 01122/08 17:09 DMB I .Bromoform SM6210D < 1 ug/L 1.0 01122/08 17:09 OMB
lsopropytbenzene SM6210D < 1 ug/L 1.0 01/22108 17:09 DMB
Bromobenzene SM62100 < 1 llg/L 1.0 01122/0817:09 DMB I 1,1 ,2,2-Tetrachloroethane SM62100 < 1 ugll 1.0 01/22108 17:09 DMB
1,2,3-Tr1cnloropropane SM62100 < 1 ug/L 1.0 01122/08 17:09 DMB
n-Propytbenzene SM62100 < 1 ug/L 1.0 01122/08 17:09 OMB I 2-Chlorotoluene SM62100 <1ug/L 1.0 01122108 17:09 DMB
4-Chlorotoluane SM6210D < 1ugll 1.0 01/22/DB 17:09 DMB
1 ,3,5-Trtmethylbenzene SM62100 < 1 ug/L 1.0 01/2210817:09 DMB I tert-Butylbenzene SM621DO < 1 ug/L 1.0 01/22108 17:09 DMB
1,2 .4-Trlmethylbenzene SM62100 < 1 ugll 1.0 01/22108 17:09 DMB
sec-Butyl benzene SM6210D < 1 ugll 1.0 01122/08 17:09 DMB l j '1 ,3-0\chlorobenzene SM6210D < 1 ugll. 1.0 01/22108 17:09 OMS
p-lsopropyltoluene SM62100 < 1 ug/L 1.0 01/22108 17:09 DMB I
1, +Dichlorobenzene SM62100 < 1 ug/L 1.0 01/22108 17:09 DMB I I 1,2-0ichlorobanzene SM62100 < 1 ug/L 1.0 01/22108 17:09 DMB
n-Butylbenzane . SM62100 < 1 ug/L 1.0 01122/08 17:09 OMB
1 ,2-Dibromo-3-chloropropane {DBCP) SM6210D < 4 ug/L 4.0 0112210817:09 DM8 I 1 ,2,4-Trtchlorobenzene SM8210D < 1 ug/L 1.0 . 01122/08 17:09 DMB
Hexachlorobutadlene SM6210D < 1 ug/L 1.0 01122/08 17:09 DMB
Naphtha lime SM62100 < 1 ugfL 1.0 01/2210817:09 DMB I 1,2,3-Tricnlorobenl!ene SM62100 < 1 ug/L 1.0 01122/U8 17:09 DMB
...,_ .,. ..
I AIR I WATE R
I LABORATORIES, INC!'
2109A North Hamilton Street • Richmond, Vugi..nia. 23230 • Tel: [phone] Fax: [phone]
I Certificate of Analysis
Final Report
I Laboratory Order ID 08010146
Client Name: APEX Companies, LLC. Date Received: January 11, 2008
6711 Peters Creek Road Date Issued: January 28, 2008
I Suite 201
Roanoke,VA 24019
Submitted To: Robert Wagner Project Number: 768299.190
I Client Site I.D.: Short Stop Purchase Order: NA
Sample J.D.: 010908-190-06 / MW-5 laboratory Sample 1.0.: 08010146-006
I Date/Time Sampled: 01/09/08 14:00 . Analysis
Parameter Method Sample Results Rep Umlt Oat&'Tlme Analyst
4-Chloro-3-methytphenol EPA625 < 10 ug/L 10.0 01/17/08 15:47 JHV
I 2-Chlorophenol EPA625 <10ugll 10.0 01/17/08 15:47 JHV
2.4-0ichlorophenol EPA625 < 10 ug/L 10.0 01/1710815:47 JHV
2.4-0imethytphenol EPA625 < 10 ug/L 10.0 01/17/0815:-47 JHV
I 4,6-Dinitr0-2-methylphenol EPA625 <50 ugiL 50.0 01/17/0815:47 JHV
2.4-Dinltrophenol EPA625 <50 ug/L 50.0 01/17/0815:47 JHV
2·Nltrophe~ol EPA625 <10ugll 10.0 01/17/08 15:47 JHV
I 4-Nitrophenol EPA825 < 50ugll. 50.0 01/17/08 15:47 JHV
Pentachlorophenol EPA625 < 20 ug/L 20.0 01/1710815:47 JHV
Phenol EPA625 <10ugll 10.0 01/:17/0815:47 JHV
I . 2,4,6-T richlorophenol EPA625 < 10 ugiL 10.0 01/17108 15:47 JHV
Aeenaphthene EPA625 < 10 ug/L 10.0 01/1710815:47 JHV
Acenaphthylene EPA625 < 10 ug/L 10.0 01/17/0815;47 JHV
I Anthracene EPA625 < 10 ugiL 10.0 01/17/0815:47 JHV
Benzo (a) anthracene EPA625 <10ug/L 10.0 01/17/08 15:47 JHV
Benzo (b) ftuoranthan~ EPA625 < 10ug/L '10.0 01/17108 15:47 JHV
I Benzo (k) fluonmthane EPA625 < 10 ug/L 10.0 01/17/0815:~7 JHV
Benzo {g,h,l) perylene EPA625 < 10ug/L 10.0 01/17/08 15:47 JHV
Benzo (a) pyrena EPA625 <10ugiL 10.0 01/17108 15:47 JHV
I . 4-Bromophenyt phenyl ether EPA625 < 10 ug/L 10.0 01117/0815:47 JHV
Butyl benzyl phthalate EPA625 <1<?ug!L 10.0 01/17/0815:47 JHV
bla (2.Chloroelhoxy) methane EPA62S < 10 ug/1.. 10.0 01/17108 15:47 JHV
I bls {2.Chloroethyt) ether EPA625 < 10 ugll 10.0 01/17/08 15:·47 JHV
bla {2-Chlorolaopropyt) ether EPA825 < 10 ug/L 10.0 01/17/08 15:47 JHV
4-Chlorophenyl phenyl ether EPA625 < 10 ug/L 10.0 01/17108 15:47 JHV I· Chrysene EPA625 < 10 ugiL 10.0 o1111ms1s:47 JHV
Dlben:z (a,h) anthracene EPA625 < 10ugll 10.0 01/17/08 15:47 JHV
Dl·n·butyl phthalate EPA625 < 10 ugll 10.0 01/17108 15:47 JHV
I ;
1,2-Dichlorobenzene EPA625 < 10 ug/L 10.0 01/1710815:47 JHV
1,3-Dichlorobenzene EPA625 < 10ug/L 10.0 01/17108 15:47 JHV
1 ,4-Dichlorobenzene EPA625 < 10 ugll 10.0 01/17/08 15:47 JHV
I Page 28of 44
AIR
WATER
LAIIORATORJES, INC~
2109A North Hamilton Street • Richmond, Vugi.ni& 23230 • Tel: [phone] Fax: (804} 358-8297
Certificate of Analysis
Final Reporl
Laboratory Order ID 08010146
Client Name: APEX Companies, LLC.
6711 Peters Creek Road
Suite 201
Roanoke,VA 24019
Submitted To: Robert Wagner
Client Slte.I.D.: Short Stop
Date Received:
Date Issued:
Project Number:
Purchase Order:
January 11, 2008
January 28, 2008
768299.190
NA
Sample J.D.: 01 0908-190-06 / MW-5
Date/Time Sampled: 01/09/08 14:00
l aboratory Sample I. D.: 08010146-006
Analysis
Parameter Method Sample Results Rep Lknlt Oai.B/Time Analyst
Olelhyt phthalate EPAB25 < .10 ug/L 10.0 01/17/08 15:47 JHV
Dimethyl phthalate EPA625 < 10 ugll 10.0 01/17/08 15:47 JHV
2,4-0inltrotoluene EPA625 < 10 ugll 10.0 01/17/08 15:47 JHV
2,6-0lnltrotoluene EPA625 <10ugll 10.0 01/17/08 15:47 JHV
01-n-octyl phthalate EPAB25 < 10 ugiL 10.0 01/17108 15:47 JHV
bla (2-Eihythexyl) phthalate EPA625 <10ugll 10.0 01/17/08 15:47 JHV
Fluoranlhene EPA625 <10ugiL 10.0 01/1710815:47 JHV
Fluorene EPA625 < 10 ugll 10.0 01/17/08 15:47 JHV
HexaChloroben~ene EPA625 <10ugll 10.0 01/17/08 15:47 JHV
Hexachlorobutadlene EPA625 < 10 ugll 10.0 01/17/08 15:47 JHV
. Hexachlorocydopentadlene EPA625 < 10 ug/1.. 10.0 01/17/08 15:47 JHV
Hexachloroethane EPA625 < 10 ugll. 10.0 01/17/0815:47 JHV
lndeno (1,2,3-cd) pyrene EPA625 < 10 ug/.L 10.0 01/17108 15:47 JHV
lsophorone EPA625 < 10 ugiL 10.0 Of/17108 15:47 JHV
Naphthalene EPA625 < 10 ugll 10.0 01{17/08 15:47 JHV
Nitrobenzene EPA625 < 10 ug/L 10.0 01/17/08 15:47 JHV
N-Nitrosodlmethylamlne EPA625 < 10 ug/L 10.0 01{17/0815:47 JHV
N-Nitrosodlphenylamlne EPA625 < 10 ug/L 10.0 01/17108 15:47 JHV
N-Nitrosodl-N-propylamlne EPA625 < 10 ugll 10.0 01/17/08 15:47 JHV
Phenanthrene EPA625 < 10 ug/L 10.0 01/17108 15:47 JHV
Pyrena EPA625 <10ug/L 10.0 01/17108 15:47 JHV
1 ,2,4-Trlchlorobenzene EPA625 < 10ugll 10.0 01/17/08 15:47 JHV
Benzidine EPA625 <50 ugiL 50.0 01/17/08 15:47 JHV
3,3-0ichlorobenzldlne EPA625 < 10 ug/L 10.0 01/17/08 15:47 JHV
2,3,4,6-Tetrachlorophenol EPA625 < 10ugll 10.0 · 01/17/0B 15:47 JHV
2-Chloronaphthalene EPA625 < 10ugll 10.0 01/17/08 15:47 JHV
C5-C8 AJipheUc Hydrocarbons MAOEP see attach 10
C9-C10 Aroma!Jc Hydrocarbons MADEP see attach 10
r"'-•••• """ , ••
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I AIR
WATER I LABORATORJES, INC!'
I 2109A North Hamilton Street" • Richmond, Virginia 23230 • Tel: [phone] Fax: [phone]
Certificate of Analysis
I Ffnal Report
Laboratory Order 10 0801~146
Client Name: APEX Companies, LLC. Date Received: January 11, 2008
I 6711 Peters Creek Road Date Issued: January 28, 2008
Suite 201
Roanoke,VA 24019
I Submitted To: Robert Wagner Project Number: 768299.190
Client Site 1.0.: Short Stop Purchase Order: NA
I Sample 1.0.: . 010908-190-07 I MW-8 Laboratory Sample 1.0.: 08010146-007
Date/Time Sampled: 01/09/08 13:35 Analysis
Parameter Method Sample RBSults RepUmlt Date/Time Analyst
I Lead SW7421 0.003 mg/L 0.002 01/15108 14:48 DMH
MTBE SM6210D naugiL 5.0 01/23108 4:48 DMB
Dl~yf ether (OIPE) SM62100 18.0 ugJl 5.0 01123108 4:48 DMB
I Dlchlorodifluommethane SM6210D < 1 ug/L 1.0 01/23/0813:18 DMB
Chloromethane SM62100 < 1 ugiL 1.0 01/23108 13:18 DMB
VInyl chloride SM62100 < 1 ugJL 1.0 01/23108 13:18 DMB
I Bromomethane SM62100 < 1 ug/L 1.0 01/23108 13:18 DMB
Chloroethane SM621DD < 1 ugiL 1.0 01/23108 13:18 OMS
Trlchlorofluommethane SM6210D < 1 ug/1.. 1.0 01fl3108 13:18 DMB
I 1,1-Dichloroethytene SM62100 <1ug1L 1.0 0112310813:18 DMB
. Melhytene chloride SM6210D < 4 ugn.. 4.0 01123108 13:18 OMB
trans-1,2-Dichloroethylene SM62100 8.9 ugll 1.0 01123108 13:18 DMB
I 1,1-Dichloroethane SM62100 < 1 ugll. 1.0 01/23108 13:18 OMB
2,2-0ichloropropane SM62100 < 1 ugll 1.0 01/23108 13:18 DMB
cls-1 ,2-0ichloroeth)4ene SM62100 40.1 ugll 1.0 01/2310813:18 DMB
I Bromochloromethane SM8210D < 1 ug/L 1.0 01/23108 13:18 OMB
Chloroform SM6210D 3.4 ug/1.. 1.0 01/23108 13:18 OMB
1,1,1-Trichloroothane SM621DD < 1 ugiL 1.0 01/23108 13:18 DMB I. Carbon tetrachloride SM6210D < 1 ugll. 1.0 01/23108 13:18 DMB
1, 1-Dlchloropropene SM62100 < 1 ugll. 1.0 01123108 13:18 DMB
Benzene SM62100 < 1 ugll.. 1.0 01/23/08 13:18 DMB
I · 1,2-Dichloroethane SM8210D < 1 uQIL 1.0 01/23108 13:18 DMB
T rlchloroethytene SM6210D 465 ugiL 1.0 01/23/0813:18 OMB
1,2-Dichloropropane SM82100 < 1 ug/L 1.0 0112310813:18 DMB.
I Dlbromomethane SM62100 <1ug/L 1.0 0112310813:18 OMB
Bromodlchloromethane SM6210D < 1 ug/L 1.0 01/23/08 13:18 DMB
cls-1,l-Oichloropropene SM62100 < 1 ugiL 1.0 0112310813:18 DMB
I 4-Methyt-2-pentanone (MlBK) SM6210D < 10 ugll. 10.0 01123108 13:18 OMB
Toluene SM6210D < 1 ugiL 1.0 01/2310813:18 DMB
1,1,2-Trichloroethane SM62100 <1ug/L . 1.0 01/2310813:18 DMB
I Tetrachloroethylene (PCE) SM62100 4680~ 1.0 01/23108 13:18 DMB
n--... '1n -.& A A
AIR
WATER
LABORATORIES, INC!
2109A North Hamilton Streel • Richmond, Virginia .23230 • Tel: [phone] Fax: [phone]
Certificate of Analysis
Final Report
Laboratory Order 10 08010146
Client Name: APEX Companies, LLC. Date Received: January 11, 2008
6711 Peters Creek Road Date Issued: January 28, 2008
Suite 201
Roanoke,VA 24019
Submitted To: Robert Wagner Project Number: 768299.190
Client Site 1.0.: Short.Stop Purchase Order: NA
Sample 1.0.: 010908-190..07./ MW-8 Laboratory Sample 1.0.: 08010146-007
Date/Time Sampled: 01/09/08 13:35 Analysis
Parameter Method Sample Results Rep Limit Oatel11me Analyst
1,3-0ichloropropsne SM62100 < 1 ugll 1.0 01/23108 13:18 OMB
Olbromochloromethane SM6210D < 1 ugJl 1.0 01123/0813:18 OMB
1,2-0ibromoethane (EOB) SM62100 < 1 ugll 1.0 01123/08 13:18 OMB
Chlorobenzene SM62100 < 1 ugll 1.0 0112310813:18 OMB
1,1,1,2-Teltachloroethane SM82100 < 1 ugiL 1.0 01/23108 13:18 DMB
Ethylbenzene SM62100 < 1 ug/L 1.0 0112310813:18 OMB
m,p-Xytenes SM62100 < 2 ug/L 2.0 01123108 13:18 OMS
o-Xylene SM62100 < 1 ug/L 1.0 01/23108 13:18 DMB
Xylenes, Total SMB2100 <3ug/L · 3.0 01/2310813:18 OMB
Styrene SM62100 < 1 ug/L 1.0 01/23108 13:18 OMS
Bromoform SM62100 < 1 ugiL 1.0 01/23108 13:18 OMB
lsopropylbenzene SM62100 < 1 ug/L 1.0 01123108 '\3:18 OMB
Bromobenzene SM62100 < 1 ugll 1.0 01123/08 13:18 OMB
1,1,2,2-Tetractdoroelhane SM62100 < 1 ugiL 1.0 01/23108 13:18 DMB
1,2,3· T rlchloropropane SM62100 < 1 ugiL 1.0 01/2310813:18 OMB
n-Propylbenzene SM62100 < 1 ug/L 1.0 01123/08 13:18 OMB
2-Chlorotoluefle SM62100 < 1 ug/L 1.0 01123108 13:18 DMB
. 4-Chlorotoluene SM62100 < 1 ug/L 1.0 01/23108 13:18 DMB
1,3, 5· Trlmethylbenz:.ene SM62100 < 1 ug/L 1.0 01/23108 13:18 OMB
tert-Buty(benzene $M62100 < 1 ug/L 1.0 01/23108 13:18 OMS
1,2,4-Trimethylbenzene SM62100 < 1 ugiL. 1.0 01/23/08 13:18 OMB
aeo-Butylbenzene SM62100 < 1 ug/L 1.0 01123/0B 13:18 OMB.
1 ,3-Dichlorobenzene SM6210D < 1 ugll 1.0 01123108 13:18 DMB
p·lsopropyltoluene SM62100 < 1 ug/L 1.0 01/2310813:18 DMB
1 ,4-0ichlorobenzene SM62100 < 1 ug/L· 1.0 01/23108 13:18 OMB
1,2-0ichloroben:zene SM62100 < 1 ugll 1.0 01/23108 13:18 OMB
n.Sutylbenzene SM62100 < 1 ugiL 1.0 01/2310813:18 OMB
1,2-Dibromo-:H:hloropropane (DBCP) SM62100 < 4ug/L 4.0 01/23108 13:18 OMB
1,2,4-Trlchlorobenzene SM62100 < 1 ugiL 1.0 01/23108 13:18 OMB
Hexachlorobutadlene SM62100 < 1 ugll 1.0 01/23108 13:18 DMB
Naphthalene SM6210D < 1 ug/L 1.0 01/23108 13:18 OMB
1,2,3· Trichlorobenzene SM6210D < 1 ugiL 1.0 01/23108 13:18 OMB
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I AIR I WATER
I . LABORATORIES, INC.•
2109A North Hamilton Street • Richmond, Virgini& 23230 • Tel: [phone] Fax: [phone]
I Certificate of Alialysis
Final Report
I Laboratory Order 10 08010146
Client Name: APEX Companies, LLC. Date Received: January 11, 2008
6711 Peters Creek Road Date Issued: January 28, 2008
I Suite 2.01
Roanoke,VA 24019
Submitted To: Robert Wagner Project Number: 768299.190
I Client Site 1.0.: Short Stop Purchase Order: NA
Sample 1.0.: 010908-190·07 / MW-8 Laboratory Sample I.D.: 08010146-007
I Date/Time Sampled: 01/09/08 13:35 Analysis
Parameter Method Sample Results RepUmlt Datemme Analyst
4-Chlo!'o·3-methylphanol EPA625 < 10 ugiL 10.0 01/17/0816:19 JHV I 2-Cillorophenol EPA625 < 10 ugll 10.0 01/17/08 16:19 JHV
2,4-0ichlorophenol EPA625 < 10 ug/L 10.0 01/17/08 16:19 JHV
2,4-Dimethylphenol EPA625 <10ug/L 10.0 01/17/0816:19 JHV I 4,6-0inllro-2-methylphenol EPA625 <50 ugJL 50.0 01/17/0816:19 JHV
2,4-Din ltroptlenol EPA625 <50 ugll 50.0 01/17/08 16:19 JHV
2-Nitrophenol EPA625 < 10 ug/L 10.0 01/17/08 16:19 JHV I· 4-Nltrophenol EPA625 '< 50ugll 50.0 01/17/08 15:19 JHV
Pentachlorophenol EPA625 < 20 ug/L 20.0 01117/08 16:19 JHV
Phenol EPA625 < 10 uglt. 10.0 01/17/08 16:19 . JHV I . 2,4,6-Trlchlorophenol EPA625 < 10 ugll 10.0 01/17/08 16:19 JHV
Acenaphthene EPA625 <10ug/L 10.0 01/17/08 16:19 JHV
Acenaphthylene EPA825 < 10ug/L 10.0 01/17/08 16:19 JHV I Anthracene EPA625 < 10u91\.. 10.0 01/17Kl8 16:19 JHV
Benm (a) anthracene EPA625 < 10 ug/1.. 10.0 01/1710816:19 JHV
Benzo (b) fluoranthene EPA625 <10ug/L 10.0 01/17/0816:19 JHV I Benzo (k) fluoranthene EPA625 < 10 ug/\. 10.0 01/17/08 16:19 JHV
Benzo (g,h,l) perylene EPA625 < 10ug/l 10.0 01/17/0816:19 JHV
Benzo (a) pyrene EPA625 < 10 ug/1.. 10.0 01/17Kl816:19 JHV I . 4-Bromophenyt phenyl ather EPA625 < 10 ug/1.. 10.0 01/17/0816:19 JHV
Butyl benzyl phthalate EPA625 < 10 ugll. 10.0 01/17/08 16:19 JHV
bls {2-Chloroethoxy) methane EPA625 < 10ugll.. 10.0 01/17/08 16:19 JHV I bls (2-Chloroethyl) ether EPA625 <10ug/L 10.0 0111710816:19 JHV
bls {2-Chlorolsopropyt) ether EPA625 < 10 ugJl 10.0 01117108 16:19 JHV
4-Ctdorophenyl phenyl ether EPA625 < 10u91L 10.0 01/17/08 16;19 JHV I Chrysene EPA625 < 10ugll 10.0 01117Kl8 16:19 JHV
Olbenz {a,h) anthracene EPA625 < 10ug/L 10.0 01/17/0816:19 JHV
DI-n-butyl phthalate EPA625 <10ug/L 10.0 01/17/08 16:19 JHV I 1,2-Dichlorobenzene EPA625 < 10 ug/L 10.0 01/1710816:19 JHV
1,3-Dichlorobenzene EPA625 < 10 ug/L 10.0 01/17/08 16:19 JHV
I 1,4-0ichlorobenzene EPA625 <_10 ugll. 10.0 01/17/08 16:19 JHV
Page 32 of 44
I
AIR I
WATER I LABORATORIES, INC~
2109A North Hamilton Street • Richmond, Virginia. 23230 • Tel: [phone] Fax: [phone] I Certificate of Analysis
Final R~port I Laboratory Order ID 08010146
Client Name: APEX Companies, LLC. Date Reeelved: January 11, 2008 I 6711 Peters Creek Road Date Issued: Januaiy 28, 2008
Suite 201
Roanoke,VA 24019 I Submitted To: Robert Wagner Project Number: 768299.190
Client Site l.D.: Short Stop Purchase Order: NA
Sample 1.0.: 010908-190-07/ MW-8 Laboratory Sample 1.0.: 08010146-007 I Date/Time Sampled: 01/09/08 13:35 Analysis
Parameter Method Sample Result& Rep Limit Datemme Analyst I 0\ethy\ phthalate EPA625 <10ugll 10.0 01/17108 16:19 Ji1V
Dimethyl phthalate EPA625 < 10ugll 10.0 01/17/08 16:19 JHV
2,4-Dinltrotoluene EPA625 < 10ug/L 10.0 01/17/08 16:19 JHV I 2,6-0inltrotoluene EPA625 <10ugiL 10.0 01(17/08 16:19 JHV
01-n-octyl phthalate EPA625 < 10ugll 10.0 01117/08 16:19 JHV
bls (2·Ethylhexyt} phthalate EPA625 < 10ugll 10.0 01/17/08 16:1 g JHV I Fluoranthene EPA625 < 10 ugJl. 10.0 01/17/08 16:19 JHV
Fluorene EPAB25 <10ugll 10.0 01117/08 16:19 JHV
HeKachlorobenzene EPA625 '< 10 ug/L 10.0 01117/0816:19 JHV I HeKar:hlorobutadlene EPA625 < 10 ugll 10.0 01/17/08 16:19 JHV
. Hexachlorocyclopent.adlene EPA625 < 10 ugll 10.0 01/17108 1~;19 JHV
Hel<8chloroethane EPA625 <10ugll 10.0 01!17108 16:19 JHV I lndeno (1,2,3-cd) pyrene EPA625 <1Dugll 10.0 01117108 16:19 JHV
lsophorone EPA625 < 10 ugll 10.0 01/17/0816:19 JHV
Naphthalene EPA625 < 10 ug/L 10.0 01/17/08 16:19 JHV I Nitrobenzene EPA625 < 10 ug/L 10.0 01/'17/08 16:19 JHV
N-Nitroaodlmethylamlne EPA625 < 10ugll 10.0 01117/0816:19 JHV
N·Nitrosodlphenylamlne EPA625 < 10ugll 10.0 01/17/08 16:19 JHV I N-Nitrosodi·N-propylamlne EPA625 < 10ugiL 10.0 01/17!08 16:18 JHV
Phenanthrene EPA625 < 10ugll 1o.o 01/17108 16:19 JHV
Pyrene EPA625 < 10 ug/L 10.0 01/17108 16:19 JHV I 1,2,4-Tr1chlorobenzene EPA625 < 10 ugll 10.0 01/17/0816:19 JHV
Benzidine EPA625 <50 ug/L 50.0 01/17/0816:19 JHV
3,3-0ichlorobenzldlne EPA625 <10ug/L 10.0 01/'17/08 16:19 JHV
2,3,4,6-Tetrachlorophenol EPA625 <10ug/L 10.0 01/1710816:19 JHV I 2·Chlorooaphthalene EPA625 <10ugll 10.0 01117/0816:19 JHV
CS.C 18 Aliphatic Hydrocarbons MADEP see attach 10 I C11-C22 Aromatic Hydrocarbons MAOEP see attach 10
Ct9-C36 Aliphatic Hydrocarbons MAOEP see attach 10
Aliphatic Surrogate % Recovety MAOEP see attach I Fractionation Surrogate #1 Recovery MAOEP see attac,h
--...
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AIR
WATER
LABORATORJES,INC: .
2109A North Hamilton Street • Rialunand, Vuginia 23230 • Tel: [phone] Fax: [phone]
Certificate of Analysis
Final Report
Laboratory Order ID 08010146
Client Name; APEX Companies, LLC.
6711 Peters Creek Road
Suite 201
Roanoke,VA 24019
Submitted To: Robert Wagner
Client Site I. D.: Short Stop
Sample I.D.: 010908~190..07 I MW-8
Date/Time Sampled: 01/09/08 13:35
Parameter Method
AromaUc Surrogate % Recovery MADEP
Fract!onaUon Surrogate #2 Recovery MADEP
C5-C8 Allphallc Hydrocarbons MADEP
C9-C10 Aromatic Hydrocarbons MADEP
Date Received: January 11 , 2008
Date Issued: January 28, 2008
Project Number: 768299. 190
Purchase Order: NA
Laboratory Sample 1.0.: 08010146-007
Analysis.
Sample Results Rep Limit Data'Tlme Analyst
see attach
see attach
see attach 10
see attach 10
0---')A ,..6 AA
AIR
WATER
LABORATORIES, INC!
2109A North Hamilton Street • Ric:hmond, Vuginia 23230 • Tel: [phone] Fax: [phone]
Certificate of A~alysis
Final Report
Laboratory Order ID 08010146
Client Name: APEX Companies, LLC. Date Received: January 11 I 2008
6711 Peters Creek Road Date Issued: January 28, 2008
Suite 201
Roanoke,VA 24019
Submitted To: Robert Wagner Project Number: 768299.190
Client Site 1.0.: Short Stop Purchase Order: NA
Sample 1.0.: 010908-190-08/ MW-9 Laboratory Sample I. D.: 08010146-008
Date/Time Sampled: 01/09/08 13:20 Analysis
Parameter Method Sample Results RepUmlt Date/Time Analyst
Lead SW7421 0.013 mgll 0.002 01/15/0814:54 DMH
MTBE SM6210D 67.8 ugJL 5.0 01122108 18:02 DMB
Dl-lsopropyl ether (DIPE} SM62100 < 5 ug/L 5.0 01122/08 16:02 DMB
Dlchlorodlfluoromelhane SM62100 < 1 ugJL ·1.0 01123/08 12:51 DMB
Chloromethane SM62100 < 1 ugll 1.0 01/23108 12:51 DMB
VInyl chloride SMG210D 3.8 ug/L 1.0 01123/08 12:51 DMB
Bromomethane SM62100 < 1 ugJL 1.0 01123108 12:51 DMB
Chloroelhane SM62100 ,<1ug/L 1.0 01123108 12:51 OMB
Ttlchlorofluoromelhane SM62100 < 1 ug/L 1.0 01123/08 12:51 DMB
1,1-Dichloroethylene SM62100 5.6 ugll 1.0 01/23108 12:51 OMS
. Methylene chloride SM62100 <4 ug/1.. 4.0 0112JJ08 12:51 OMS
trans-1,2-Dichloroethylene SM62100 9.1 ug/L 1.0 01123108 12:51 OMB
1,1-Dichloroethane SM62100 < 1 ug/L 1.0 0112310812:51 DMB
2,2-0ichloropropane SM62100 <1ug/L 1.0 01123108 12:51 OMB
cls-1,2-0ichloroethylene SM62100 1130u~. 1.0 01123108 12:51 DMB
Bromochloromethane SM6210D .<1ugll 1.0 01/23108 12:51 DMB
Chloroform SM6210D 37.7 ug/L 1.0 01123108 12:51 OMB
1,1,1-Trichloroethane SM62100 < 1 ug/L 1.0 01123108 12:51 DMB
Carbon tetrachloride SM62100 < 1 ug/L 1.0 01123/08 12:51 DMB
1 1 1·01chloropropene SM62100 < 1 ugll 1.0 01/23108 12:51 DMB
Benzene SM62100 < 1 ugll 1.0 01123/0812:51 DMB
1 12-Dlchloroethane SM62100 < 1ug/L 1.0 0112310812:51 OMB
Trichloroethylene SM62100 2770ug/L 1.0 0112310812:51 OMB
1,2-Dichloropropane SM62100 1.9ug/L 1.0 01123/08 12:51 DMB
Dlbromomethane SM6210D < 1 ug/L 1.0 01123108 12:51 DMB
Bromodlchloromethane SM6210D <1ug/L 1.0 01123/08 12:51 OMB
clo-1 ,3-0ichloropropene SM62100 c:: 1 ug/L 1.0 01/23/08 12:51 DMB
4-Methyl-2-pentenone (MIBK) SM62100 < 10ug/L 10.0 01123108 12:51 DMB
Toluene SM62100 < 1 ug/L 1.0 01123108 12:51 OMB
1,1,2-Trichloroethane SM6210D 4.6ug/L 1.0 01123108 12:51 OMB
Tetrachloroethylene (PCE) SM62100 44200 u~IL 1.0 01123/08 1'2:51 DMB
Page 35 of44
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I AIR
WATE R I INC~
I
2109A North Hamilton Street • Richmond, Vuginia 23230 • Tel: [phone] Fax: [phone]
Certificate of Analysis
I Final Report
Laboratory Order ID 08010146
Client Name; APEX Companies, LLC. Date Reoelved: January 11 r 2008
I 6711 Peters Creek Road Date ls·sued: Janua,.Y 26, 2008
Suite 201
Roanoke,VA 24019
I Submitted To: Robert Wagner Project Number: 768299.190
Client Site 1.0.: Short Stop Purchase Order: NA
I. Sample 1.0.: 010908-190-08/ MW-9 Laboratory Sample I.D.: 08010146-008
DatefTime Sampled: 01/09/08 13:20 Analysis
Parameter Method Sample Results Rep Limit DatefTlme Analyst
I 1 ,3-Dichlompropal)e SM62100 < 1 ugll 1.0 01123108 12:51 OMS
Dlbromochloromethane SM6210D ' < 1 ug/L 1.0 01/23108 12:51 OMS
1,2-Dibromoethane (EDB) SM62100 < 1 ug/L 1.0 01/23/08 12:51 OMB
I Chlorobenzene SM62100 < 1 ug/L 1.0 01/23108 12:51 DMB
1,1,1 ,2-Tetra<:hloroethane SM6210D 56.4 ug/L 1.0 01123108 12:51 DMB
Ethyl benzene SM6210D < 1 u9/l 1.0 01/23108 12:51 DMB
I m,p-Xylenes SM6210D <2ug/L 2.0 01/23/08 12:51 OMB
o-Xylene SM62100 < 1 ugll 1.0 01123108 12:51 OMS
Xylenea, Total SM62100 < 3 ugll 3.0 01123108 12:51 DM8
I Styrene SM6210D .< 1 ugll 1.0 01/23/08 12:51 . DMB
Bromofonn SM62100 < 1 ugll 1.0 01123108 12:51 DMB
Jsopropylbenzene SM62100 < 1 ug/L 1.0 01/23108 12:51 OMB
I Bromobenzene SM62100 < 1 ug/L 1.0 0112310812:51 OMS
1 , 1 ,2.2-T etrac:hloroelhane SM62100 < 1 ug/L 1.0 01/23/0812:51 OMB
1 ,2,3-Tr1chloropropane SM6210D < 1 ug/L 1.0 01123108 12:51 OMS
I n-Propylbenzcne SM62100 <1ug/L 1.0 01123/08 12:51 OMB
2~Chlorotoluene SM62100 < 1 ugll 1.0 01/23/08 12:51 DMB
4-Chlorotoluene SM62100 < 1 ugll. 1.0 01123108 12:51 OMS '
I 1 ,3,5-Trlmethylbenzene SM6210D < 1 ugll 1.0 01123108 12:51 OMS .•.
tert-Butytbenzene SM6210D < 1 ug/L 1.0 . 01/23108 12:51 OMB
1 ,2,4-Trtmethylbenzene SM62100 < 1 ug/L 1.0 01/23108 12:51 DMB
I sec-Butylbenzene SM62100 < 1 ug/L 1.0 01123/08 12:51 OMS
1,3-Dichlorobenzene SM62100 < 1 ug/L 1.0 01/23108 12:51 DMB
p-lsopropyltoluene SM62100 < 1 ug/L 1.0 01/23108 12:51 OMS
I 1 ,4-Dichlorobenzena SM62100 < 1 ug/L 1.0 01/23108 12:51 OMB
1,2-Dichlorobenzene SM6210D < 1 ug/L 1.0 01/23/08 12:51 DMB
n-Butylbenzene SM62100 < 1 ugll 1.0 01/23/08 12:51 OMS
I 1 ,2-Dibromo-3-chloropropane (OBcP) SM62100 < 4 ugll 4.0 01/23/08 12:51 OMS
1 ,2,4-Trtdllorobenzene SM6210D < 'f ugll 1.0 01/23108 12:51 OMB
Hexachlorobutadlene SM6210D < 1 ugll 1.0 01/23/08 12:51 OMS
I Naphthalene SM62100 < 1 ug/L 1.0 01123108 12:51 OMB
1 ,.2,3-Triotllorobonzene SM62100 < 1 ugiL 1.0 01/23108 12:51 OMS
F""\---"",... .,.LA 6
I
I AIR
WATER I LABORATORIES, INC!"
I
2109A North· Hamilton Street • Richmond, VJ.rgi.n.ia 23230 • Tel: [phone] Fax: {804) 358-8297
Certific~te of Analysis
I Final Report
Laboratory Order 10 08010146
CJ!ent Name: APEX Companies, LLC. Date Received: January 11, 2008
I 6711 Peters Creek Road Date Issued: January 28, 2008
Suite 201
Roanoke,VA 24019
I Submitted To: Robert Wagner Project Number: 768299.190
Client Slte I.D.: Short Stop Purchase Order: NA
I Sampl·e I.D.: 010908-19()..()8/ MW-9 Laboratory Sample I.D.: 08010146..()08
Date/Time Sampled: 01/09/08 13:20 Analysis
Paramatar Method Sample Rest~IIS RepUmlt DataiTime Analya.t
I Dlettlyl phthalate EPA625 < 10 ug/L 10.0 01/17108 16:52 JHV
Dimethyl phthalate EPA62S < 10 ugiL 10.0 01/17/08 16:52 JHV
2,4-0inltrotoluene EPA82S < 10 uglt 10.0 01/17108 16:52 JHV
I 2 ,6-0inltrotoluena EPA625 < 10 ug/L 10.0 01117/Ca 16:52 JHV
0\-fH)ctyl phthalate EPA625 < 10 ugll 10.0 . 01/1710816:52 JHV
bla (2-Eihylhaxyf) phthalate EPA625 < 10 ugll 10.0 01/1710816:52 JHV
I Fluornnthene EPA625 < 10 ugll 10.0 01/17/08 16:52 JHV
FltJorene EPA625 < 10 ug/L 10.0 0111710816:52 JHV
Hexachlorobenzene EPA625 <10ug/L 10.0 01117/0816:52 JHV
I Hemchlorobutadlene EPA625 < 10 ug(L 10.0 01/17/08 18:52 JHV
. Hexaohlorocyclopentadlene EPA625 < 10 ug(L 10.0 01/17/08 16:52. JHV
Hexachloroethane EPA625 <10ug/L 10.0 01/17/08 16:52 JHV
I lndeno (1 ,2,3-<XI} pyrene EPA625 <10ug/L 10.0 01/171<>8 16:52 JHV
lsophotone EPA625 < 10 ugll 10.0 01/17/08 16:52 JHV
Naphthalene EPA625 < 10 ug/L 10.0 01/17108 16:52 JHV
I Nitrobenzene EPA625 < 10 ugll 10.0 01117/08 16:52 JHV
N-NitroaodlmeUry1amlne EPA625 <10ug/L 10.0 01117/08 16:52 JHV
N-Nitroeodlphenylamlne EPAB25 .< 10ugiL 10.0 01/17/0816:52 JHV
I N-Nitrosodi-N-propylamlne EPA625 < 10 ug/L 10.0 01/17/0816:52 JHV
Phenanlhrene EPA625 < 10 ugll. 10.0 01/17/08 16:52 JHV
Pyrena EPA625 < 10 ug/L 10.0 01/17/0816:52 JHV
I 1 ,2,4-Tridllorobenzene EPA625 < 10 ug/L 10.0 01/17108 16:52 JHV
Benzidine EPA625 <50 ug/L 50.0 01/17108 16:52 JHV '
3,3-Dichlorobenzldine EPA625 < 10 ug/L 10.0 01/17/0816:52 JHV
I 2,3,4,6-Tetrachlorophenol EPA625 <10ugll 10.0 01/17/08 16:52 JHV
2..Chloronephthalene EPA625 < 10 ug/L 10.0 01/17108 16:52 JHV
C9-C18 Aliphatic Hydrocarbons MAOEP see attach 10
I C11-C22 Aromatic Hydrocarbons MADEP see attach 10
C19-C36 Aliphatic Hydrocarbons MADEP see attach 10
Aliphatic Surrogate % Recovery MAOEP sea attach
I Fractionation Surrogate #1 Recovery MADEP see attach
n.-.. -..,ft -~ A A
AIR
WATER
LABORATORIES, INC!
2109A North Hamilton Street • Richmond, Virginia 23230 • Tel: [phone] Fax: [phone]
Certificate of Analysis
Final Report
Laboratory Order ID 08010146
Client Name: APEX Companies, LLC.
6711 Peters Creek Road
Suite 201
Roanoke,VA 24019
Submitted To: Robert·Wagner
Date Received:
Date Issued:
Project Number:
January 11, 2008
January 28, 2008
768299.190
Client Site 1.0.: Short Stop Purchase Order: NA
Sample 1.0.: 010908--190-08/ MW-9
Date/Time Sampled: 01/09/08 13:20
Parameter
Aromatic Surrogate % Recovery
Ftactlonalion Sutrogate #2 Recovery
C5-C8 Aliphatic Hydrocarbons
C.9-C10 Aromatic Hydrocarbons
Method
MAOEP
MADEP
MADEP
MADEP
Sample Results
see attach
see attach
see attach
see attach
PaQe 39of44
Laboratory Sample I. D.:
Analysis
Rep Umlt Datemme
10
10
08010146-008
Analyst
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I AIR
WATE R I LABORATORIES, INC.•
I
2109A North Hamilton Street • Richmond, Virginia 23230 ~Tel: [phone] Fax: {804) 358-8297
Certificate of Analysis
I Final Report
Laboratory Order ID 08010146
Client Name: APEX Companies, LLC. Date Received: January 11 , 2008
I 6711 Peters Creek Road Date Issued: January 28, 2008
Suite 201
Roanoke,VA 24019
I Submitted To: Robert Wagner ProJect Number: 768299.190
Client Site 1.0.: Short Stop Purchase Order: NA
I Sample J.D.: 010908-190-09 / AEI-MW -13 Laboratory Sample f. D.: 0801 0146-Q09
Dateffime Sampled: 01/09/08 14:50 Analysis
Parameter Method Sample ResultB RepUmlt OataiTime Analyst
I Lead SW7421 0.007 mgll. 0.002 01/15108 15:00 OMH
MTBE SM62100 489 ugiL 5.0 01/23108 4:24 OMS
01-lsD?ropyt eth&r (DIP E) SM62100 48.4 ugll. 6.0 01123108 4:24 OMB
I Olchlorodlftuoromethane SM62100 · < 1 Ug/L 1.0 01123108 4:24 DMB
Chloromethane SM62100 < 1 ugtl 1.0 01/23/()8 4:24 DMB
VInyl chlorld.e SM6210D < 1 ugll.. 1.0 01/23106 4:24 OMS
I · Bromomethane SM62100 < 1 ugiL 1.0 01123108 4:24 OMB
Chloroethane SM62100 ·< 1 ugiL '1.0 01123108 4:24 OMB
T rfchlorofluoromelhane SM6210D < 1 ug/L 1.0 01123108 4:24 OMS
I 1, 1-Dichloroethylene SM62100 <'1 ug/1.. 1.0 01/23108 4:24 DMB
. Methylene chloride SM62100 < 4 ug/L 4.0 01123/08 4;24 DMB
trane-1 ,2-Dfchloroethytane SM62100 2.2 ug/1. 1.0 01123/08 4:24 OMS
I 1,1-Dichloroethane SM6210D < 1 ug/L 1.0 01/23108 4:24 DMB
2,2-Dichloropropane SM62100 < 1 ugll 1.0 01/23108 4:24 DMB
cla-1 ,2-Dichloroethytene SM62100 ' 3.2 ug/L 1.0 01/23108 4:24 DMB
I Bromochloromalhane SM62100 .< 1 ug/L 1.0 01123108 4:24 OMB
Chloroform SM62100 < 1 ugiL 1.0 01/23108 4:24 OMB
1 ; 1,1-T richloroalhane SM6210D < 1 ug/L 1.0 01123108 4:24 DMB
I carbon tetrachloride SM62100 < 1 ugiL 1.0 01/23/()8 4:24 DMB
1 ,1-Dichloropropene SM62100 < 1 ugiL 1.0 01123108 4:24 DMB
Benzene SM82100 < 1 ugll 1.0 01123108 4:24 DMB
I 1,2-Dlchloroethene SM6210D 2.7 ugiL 1.0 01123108 4:24 DMB
Tnchloroethytene SM6210D 18.7 ugiL 1.0 01/23108 4:24 DMB
1 ,2-Dichlorcpropane SM6210D .<1uo/L 1.0 01/23/08 4;24 OMB
I Dlbromomethana SM62100 < 1 ugiL 1.0 01123/08 4:24 OMS
Sromod/chloromethane SM62t00 < 1 ug/L 1.0 01/23/08 4:24 DMB
ci5·1 ,3·Dichloropropene SM62100 < 1 ugll.. 1.0 01/23/08 4:24 DMB
I 4-Methyl-2~entanone (MiBK) SM62100 < 10ugll 10.0 01123/08 4:24 DMB
Toluene SM6210D < 1 ugiL 1.0 01/23108 4:24 DMB
1,1 ,2-Trlchloroethane SM62100 < 1 UQIL 1.0 01/23108 4:24 OMB
I Tetrachloroethylene (PCE) SM62100 45.1 u~ 1.0 01/23108 4:24 DMB
,.., ___ AI"\-· A A
I
AIR I
WATER I LABORATORIES, INC!
2109A North Hamilton Street • Richmond, Vu-gi.n.ia 23230 • Tel: [phone] Fax: (804} 358-8297 I Certificate of Analysis
Final Report I Laboratory Order 10 08010146
Client Name: APEX Companies, LLC. Date Received: January 11, 2008
I 6711 Peters Creek Road Date Issued: January 28, 2008
Suite~01
Roanoke,VA 24019 .I Submitted To: Robert Wagner Project Number: 768299.190
Client Site 1.0.: Short Stop Purchase Order: NA
Sample I.D.: 010908-190-09/ AEI-MW-13 Laboratory Sample 1.0.: 0801 0146-009 I Daterrime Sampled:· 01/09/08 14:50 Analysla ·
Parameter Method Sample Results RepUmlt Date/Time Analyst
1,3-Dichloropropane SM62100 < 1 ugll 1.0 01/23108 4:24 OMB ·I Dlbromochloromethane SM6210D < 1 ugll 1.0 01123108 4:24 DMB
1 ,2-0ibromoelhane (EOB) SM6210D < 1 ugll 1.0 01123108 4:24 DMB
· Chlorobenzene SM62100 < 1 ugiL 1.0 01/23108 4:24 OMS I 1 ,1,1,2·Tetrachloroeth~ne SM62100 < 1 ug/L 1.0 01/23108 4:24 OMS
Ethyl benzene SM62100 < 1 ug/L 1.0 01/23108 4:24 DMB
m,p-Xytenes SM62100 <2ug/L 2.0 01/23108 4:24 OMS I o-Xytene SM6210D < 1 ugll 1.0 01/23108 4:24 DMB
Xytenes. Total SM62100 < 3 ugll 3.0 01/23108 4:24 OMB
S~ene SM8210D < 1 ugiL 1.0 01/23108 4:24 DMB I Bromoform SM6210D < 1 ugiL 1.0 01/23108 4:24 OMB
lsopropylbenzene SM62100 < 1 ugiL 1.0 01/23108 4:24 OMS
Bromobenzene SM6210D · <1ug/L 1.0 01/23108 4:24 DMB I 1,1,2,2· Tetrachloroethane SM6210D < 1 ugiL 1.0 01/23108 4:24 OMB
1,2,3-Trlchloropropane SM6210D < 1 ugiL 1.0 01/23108 4:24 OMS
n·Propylbenzene SM62100 < 1 ug/L 1.0 01/23108 4:24 OMS I 2--Chlorctoluene SM6210D < 1 ug/L 1.0 01123/08 4:24 DMB
4-Chlototoluene SM62100 < 1 ug/L 1.0 01123/08 4:24 OMS
1.3,5-Trlmethylbenzene SM62100 < 1 ugll 1.0 01/23108 4:24 OMS I tert-Butylbenzene SM62100 < 1 ugll 1.0 01123108 4:24 DMB
1,2, 4-Trlmethylbenzene SM62100 < 1 ug/L 1.0 01/23/08 4:24 DMB
seo-Butylbenzene SM6210D <1ug/L 1.0 01/23108 4:24 OMS II 1,3·01chlorobenzene SM62100 < 1 ug/L 1.0 01123108 4:24 DMB
p-lsopropyltoluene SM62100 < 1 ugll 1.0 01/23/08 4:24 DMB
1,4-0ichlorobenzene SM62100 < 1 ug/L 1.0 01123/08 4:24 DMB I~ 1 ,2-Dichlorobenzene SM62100 < 1 ug/L 1.0 01/23108 4:24 OMS
n·Butylbenzer~e SM6210D < 1 Ug/l 1.0 01123108 4:24 DMB
1,2·Dibromo-~chloropropane (OBCP) SM62100 < 4 uglt. 4.0 01/23108 4:24 DMB I' 1,2,4-Trlchlorobenzene SM6210D < 1 ug/l 1.0 01/23108 4:24 DMB
Hexachlorobutadlene SM62100 < 1 ug/1.. 1.0 01/23108 4:24 OMS
Naphthalene SM6210D < 1 ug/L 1.0 01/23108 4:24 DMB I 1,2,3-Trlchlorobenzene SM82100 < 1 ug/L 1.0 01123108 4:24 DMB
n ... __ A ... -~·4
····-·--
I
I AIR
WATE R I LABORATORIES, INC.•
2109A North Hamilton Street • Richmond, Virginia 23230 • Tel: (804) 358~8295 FIIX: [phone]
I Certificate of Analysis
I Final Report
Laboratory Order ID 08010146
Client Name: APEX Companies, LLC. Date Received: January 11, 2008
I 6711 Peters Creek Road Date Issued: Januaiy 28, 2008
Suite ~01
Roanoke,VA 24019
I Submitted To: Robert Wagner Project Number: 768299.190
Client Site I. D.: Short Stop Purchase Order: NA
I Sample 1.0.: 010908-190-09/ AE/-MW-13 Laboratory Sample I.D.: 06010146-009
Datef!lme Sampled: 01/09/08 14:50 Analysis
Parameter Method Sample Results ~ep Limit DateiTime Allalyut
I 4-Chloro-3-methylphenol EPA625 < 10 ugll. 10.0 01/17108 17:23 JHV
2-Chlorophenol EPA625 < 10ug/L 10.0 01/17/08 17:23 JHV
2 ,4-Dichlorophenol EPA625 < 10 ugiL 10.0 01/17/0817:23 JHV
I 2,4-Dtmetnylphenol EPA625 < 10 ugll. 10.0 01/17/08 17:23 JHV
4,6-Dinf(ro-2-methylphenol EPA625 < 50ug/L 50.0 01/17/08 17:23 JHV
2,4-0inltrophenol EPA625 <50 ug/L 50.0 01/17/08 17:23 JHV
I 2-Nlt.rophe!lol EPA625 < 10 ugiL 10.0 01117108 17:23 JHV
4·Nitrophenol EPA625 . <50 ug/L 50.0 01/17/08 17:23 JHv
Pentachlorophenol EPA625 < 20 ug/L 20.0 01/17/08 17:23 JHV
I Phenol EPA625 < 10 ugll 10.0 01/17/08 17:23 JHV
. 2,4,&-Trlchlorophenol EPA625 < 10ug/L 10.0 01/17/08 17:23 JHV
Acenaphthene EPA625 < 10 ug/L 10.0 01/17/08 17:23 JHV
I Acenaphthylene EPA625 < 10 ugll 10.0 01/17108 17:23 JHV
Anthracene EPA625 < 10 ug/L 10.0 01117/0817;23 JHV
Benzo {a) anthracene EPA625 < 10 ugll 10,0 01117/08 17:23 JHV
I Benzo(b)fluo~~~~ EPA625 < 10 ugiL 10.0 01/17/08 17:23 JHV
Benzo (k) fluoranthene EPA625 <10ug,L 10.0 01/17/08 17:23 JHV
Benm (g,h,l) perylene EPA625 < 10 ug/L 10.0 01/17/08 17:23 JHV
I Benm (a) pyrene EPA625 < 10ug/L 10.0 01/1 7/08 17:23 JHV
. 4-Bromophenyl pheoyt ether EPA625 < 10 ugll. 10.0 01/17/0817:23 JHV
Butyl benzyl phthalate EPA625 < 10 ug/L 10.0 01/17/08 17:23 JHV
I bls (2-<:hloroethoxy) methane EPA625 < 10 ugi\. 10.0 01/17/08 17:23 JHV
bls (2-Chloroethyl) ather EPA625 < 10 ug/L 10.0 01/17/08 17:23 JHV
bls (2·Chlorotsopropyl) ether EPA625 <10ug/L 10.0 01/17/08 17:23 JHV
I 4-Chlorophenyl phenyl ether EPA625 < 10 ugiL 10.0 01/1710817:23 JHV
Chrysene EPA625 < 10 ug/L 10.0 01/17/08 17:23 JHV
Dlbenz (a, h) anthracene EPA625 < 10 ug/L 10.0 01/17/08 17:23 JHV
I Dkl·blltyl ph thslate EPA625 · < 10 ug/L 10.0 01/1710817:23 JHV
1,2-Dichlorobenzene EPA625 < 10 ugll. 10.0 01117/08 17:23 JHV
1,3-Dichtorobenzene EPA625 < 10 ug/L 10.0 01/17/08 17:23 JHV
I 1 ,4-0ichlorobenzene EPA625 < 10 ugll, 10.0 01/17108 17:23 JHV
,.,...., __ At'\ -~ A .t
AIR
WATER
LABORATORIES. INC.•
2109A North Hamilton Street • Richmond, VuginiD 23230 • Tel: [phone] Fax: [phone]
Client Name:
Submitted To:
Certifi.:ate of Analysis
Final Report
Laboratory Order 10 08010146
APEX Companies, LLC. Date Received:
6711 Peters Creek Road Date Issued:
Suite 201
· Roanoke,VA 24019
Robert Wagner Project Number:
Client Site I. D.: Short Stop Purchase Order:
January 11 , 2008
January 28, 2008
768299.190
NA
Sample 1.0.: 010908-190-09/ AEI-MW-13 Labcntory Sample 1.0.: 08010146-009
DatefTime Sampled: 01/09/08 14:50 Analysis
Parameter Method Sample Results Rep Umlt Dst&'Tlme Analyst
Dlalhyl phthalate EPA62.5 < 10 ug/L 10.0 01/17/08 17:23 JHV
Dimethyl phthalate EPA625 <10ug/L 10.0 01/17108 17:2.3 JHV
2,4-Dlnltrotoluene EPA625 < 10ugll 10.0 01/17/0817:23 JHV
2,6-Dinltrotoluene EPA625 <10ug/L 10.0 01/17/08 17:23 JHV
0 1-n -<x:ty1 phlhala te EPA625 <10ug/L 10.0 01/1710817:23 JHV
bls (2-Ethylhexyt) phthalate EPA625 <10ug/L 10.0 01/17/08 17:23 JHV
Fluonmthene EPAS25 < 10 ugll 10.0 01/17/08 17:23 JHV
Fluorene EPA625 < 10 ug/\. 10.0 01/17/08 17:23 JHV
Hexachlorobenzene EPA625 < 10 ug/L ·10.0 01117/08 17:23 JHV
Hexachlorobutadlene EPA625 < 10 ug/L 10.0 01/17/0817:23 JHV
. Hexachlorocyclopentadlene EPA625 < 10 ug.ll 10.0 01/17/08 17:23 JHV
Hexachloroethane EPA625 <10ugll 10.0 01/17/08 17:23 JHV
lndeno (1,2,3-<:d) pyrene EPA625 < 10ug.ll 10.0 01/17/08 17:23 JHV
lsophorone EPA625 <10ugfl 10.0 01/17108 17:23 JHV
Naphthalene EPA625 <10ugll 10.0 01/17/08 17:23 JHV
Nltrobeflmne EPA625 < 10 ugt\. 10.0 01/17/08 17:23 JHV
N-Nitroaodlmeth)'lamlne EPA625 < 1 o ug/1. 10.0 01117/08 17:2.3 JHV
N-N\trosodlpheny1amlne EPA625 < 10 ugll 10.0 01/17/08 17:23 JHV
N-Nitrosodi-N-propylamlne EPA625 < 10ugll 10.0 01/17/0817:23 JHV
Phenanthrene EPA625 < 10 ugll 10.0 01/17108 17:23 JHV
Pyrena EPA625 < 10 ug/L 10.0 01117/0817:23 JHV
1,2,4-Trlchlorobenzene EPA625 < 10ug/L 10.0 01117108 17:23 JHV
Benzidine EPA625 < 50ugll 50.0 01/17AJ8 17:23 JHV
3,3-0ichlorobenzldlne EPA625 ·< 10 ug/L 10.0 01/17/08 17:23 JHV
2,3,4,6-Tetr&ctllorophenol EPA625 < 10 ugiL 10.0 01/17/0817:23 JHV
2 -Chloronaphlhalene EPA625 < 10 ug/1.. 10.0 01/17108 17:23 JHV
C9-C18 Aliphatic Hydrocarbons MAOEP see attach 10
C11-C22 Aromatic Hydrocarbons MADEP sea attach 10
C1&-C36 Aliphatic Hydrocarbons MADEP see attach 10
Aliphatic Surrogate % Recovory MADEP see attach
Fractionation Surrogate #1 Recovery MAOEP see attach
o_,..,,... A "l n:l A A
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AIR
WATER
LABORATORIES, rNC:'
2109A Nortb Hamilton Street • Richmond, V~inia 23230 • Tel: [phone] Fax: [phone]
Certifi~ate of Analysis
F/na/ Report
Laboratory Order 10 08010146
Client Name: APEX Companies, LLC.
6711 Peters Creek Road
Suite 201
Roanoke,VA 24019
Submitted To: Robert Wagner
Client Site 1.0.: Short Stop
Date Received:
Date Issued:
January 11, 2008
January 28, 2008
Project Number: 768299.190
Purchase Order: NA
Sample 1.0.: 01090S..190·09/ AEI-MW-13
Date!Time Sampled:. 01/09108 14:50
Laboratory Sample I.D.: . 08010146--009
Parameter Method
Aromatic Surrogate % Recovaty MADEP
Fractionation Surrogate #2 Recovery MADEP
C5-C8 Aliphatic Hydrocarbons MADEP
C9-C10 Aromatic Hydrocarbons MADEP
-~ -,;: --·
Ted Soyars
labo111tofy Manager
Sample Results
see attach
see attach
see attach
see attach
P~n"' .dA nf AA
Analysis
Rep Limit Oa181Tlme
10
10
Analyst
AIR
WATER
LABORATORIES, INC~
2109A North Hamilton Street • Richmond, Virginia 23230 • Tel: [phone] Fa.x: [phone]
Certificate of Analysis
Fins/ Report
Laboratory Order ID 0801 0146
Client Name: Apex Companies, LLC Date Sampled:
6701 Peters Creek Road, Suite 111
Roanoke, VA24019
Date Received:
Date Issued:
Submitted To:
Client Proj I.D.
Robert Wagner
Short Stop
Project Number
Pureba.se Order
Refereoce Method: SW846 method 8l60B
Tentatively ldcntifi~ Compounds:
SimnJe !.p. Compo!Qld
08010146-001 Pentane, 2,2,4·trlmelhyl·
lndane
Benzene, 1 ,2-dlethyl-
Benzene, 1-melhyl·2-(2·propenyt)·
Benzene, 1-elhyenyt-~elhyl·
Benzene, 1 ,2,4,5·tettamelh)'I-
Benzene, 1-ethyenyl-4-ethyl·
Benzene, 2-ethenyl-1 ,4-dlmethyi-
Benzene, 1,2,3,4-tetramethyt-
1H·Indene, 2,3-dlh~ro-4.7-dlmelhyt·
08010146-002 Butane, 2,2·dlmethyl·
Pentane, 2,4·dlmethyl·
Pentane, 2,3·dlmethyl·
Pentane, 2,2,4·trlmethyl·
Hexane, 2,4-dlmelhyi-
Pentane, 2,3,4-trlmathyt·
Pentane, 2,3.~trlmethyt.
lndane
Benzene, 1 ,2-dlethyl·
Benzene, 1-ethenyt-~ethyt·
08010 146.003 No non-target library matches detected above report limit.
08010146.004 No non-target library matchea dotecte<l above report limit.
08010146-00S
08010146~06
080100146-007
08010146.008
080 I 0 146-0il9
No non-target library matches detected above report limit. ·
No non-target library matchee detecte<l above report limit.
No non-target library matches detected above report limit.
No non-target library matches detected above report limit.
No non-target library matchee detected above report limit.
Estimated Cone.
UlzlJ.)
23
287
52
25
164
31 .
30
133
31
24
54
57
31
95
26
45
44
50
47
27
January 09, 2008
January 11, 2008
January 28, 2008
768299.190
NA
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AIR
WATER
LAlBOIIIA,roiUE:S,INC:
2109A North Hamilton St.reot • RichinonJ, Vuginia 23230 • Tel: {804) 358-8295 Fax: [phone]
Client Name:
Submitted To:
Client Proj I.D.
Tentatively ldmtified Compouods·
Sampl;I.D.
08010146-001
0&010146-002
08010146-003
080101%-004
Certificate of Analysis
Final Report
Laboratory Order ID 0801 0146
Apex Companies, LLC ·
6701 Peters Creek Road, Suite 111
Roanoke, VA24019
Robert Wagner
Short Stop
Date Sampled:
Date Received:
Date Issued:
Project Number
Purchase Order
Reference Method: SW84() method 8270C
CQIDil9!!Qd
cyclopentallol, t-methyl-
2-haxanol, 2-methyt...
3-hexanol, 3-methyt...
1,3-dlmethylc)'Ciopentanol
ethylbenzena
2·heptanol, 2-methyl·
lndwlo
benzene, 1 ,3-dlethyt..
benzene, 1 ,2-dlethyl-
benzene, 1 ,2,4,5-tetramllthyt..
1 h-llldene, 2,3-dlhydro-4-melhyl-
benzene, (1-methyl-1-propenyf)·
1 h·lndene, 2,3-dlhydro-1, 1-dlmelhyl·
2-ethyl-2,3-dlhydro-1 h·lndene
1 h·lndene, 2,3-dlhydro-4, 7 -dimethyl-
benzene, (3-methyt.-2-buten~­
dodecanolc acid
2-butanol, 2,3-dlmethyl·
·2-pontanol, 2-melhyl
3-pentanol, 3-methyl-
cyclopentanol, 1-melhyt·
2-hexanol, 2-methyt
ethylbenzene
1-melhlcyc/ohexanol
cyclohexanol, 1,3-dlmelhyl·, cls-
lndane
benzene, 1,3-dlethyt
benzene, 1-elhyt-3·( 1 -methyt ethyl}·
benzene, 1 -melhyi-4·(1-methylpropyl)·
1 h·lndane, 2,3-dlh)dro-5·melhyl-
1 h·lndene, 2.3-dlhydro-1 ,6-dlmethyl·
dodecanoic acid
tetradecanolc acid
9-«tadecenamlde, (ZJ·
n·hexadecanolc acid
9-octadacenamlde, (Z)·
13-docosenamlde, (Z)-
Estimated Cooc.
WiLl·
6.44
7.15 .
10.68
6.29
8.72
7.51
104.71
33.42
14.61
10.41
18.78
45.96
17.36
9.41
6.84
6.34
17.93
.11.19
9.28
17.02
10.28
3.445
17.12
9.34
6.08
30.95
28.18
6.17
6.58
6.16
18.2
11.69
4.52
6.43
6.52
9.23
6.1
January 09,2008
January 11, 2008
January 28, 2008
768299.190
NA
AIR
WATER
LABORATORIES, INC.•
2109A North Hamilton Street • Richmond, Virginia 23230 • Tel: (804} 358-8295 Fax: [phone]
Client Name:
Submitted To:
Client Proj.I.D.
Tentatively ldmlified Compouods:
Sample !.D.
080 I 0 146-00j
08010146-006
08010146.{)07
08010146-008
08010146-009
Laboratory Manager
Certificate of Analysis
Final Report
Laboratory Order 10 08010146
Apex Companies, LLC Date Sampled:
6701 Peters Creek Road, Suite 111
Roanoke, VA 24019
Robert Wagner
Short Stop
Date Received:
Date Issued:
Project Number
Purchase Order
Reference Method: SW846 metbod 8Z70C
&timamd Ccac.
Compound Wl1J
tetrachloroelhylene 20.3
dodacanolc acld 6.S4
n-hexadecanolc acld 5.74
9-<letadecenamlde, (Z)· 4.9
tetrachloroethylene 25.06
n-hexadecanoic add 5.53
9-octadecanamlde, (Z)-11.42
13-docosenamlde, (Z)-11.13
tetrachloroethylene 320,63
dodecanoic acid 21.88
tetradacanolc aclcl 5.31
9·octadecenamlde, (Z)· 5.55
tetrachloroethylene 469.44
ethane, 1, 1,1,2-tetrachloro· 10.189
dodecanoic acid 7.72
9-octadecenamlde, (Z)-8.3
13·docosenamlde, (Z)· 4.23
tetrachloroethylene 11.12
dodecanoic acid 16.5
January 09, 2008
January t 1. 2008
January 28, 2008
768299.190
NA.
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-------------------A ex 8701 Pebn Create Road, &lite 1 t 1
Roanoke, VA 24019 CHAIN OF CUSTODY RECORD f Companies, LLC (540) SG-4920
J08 NO. JOI MAW£ PROJ.ECT liWIACVt ~ ~L PARAioiDUS I
~-....... .....o.\qo Is K...ft STb {) I~-'· 'Uo.,_ , .. V; ~~e:v;~ (l"rrmed) ~~ z----
~~~•N)tUo/ I; :!' ·...: / ct ... .: § ~· w i-~ SloWU DAft TIW( a a P'tln. ST AT!Otl I LDCA1ION I --:., ~~< ..... .,
u .., I lltWAIItCS
0\0'\ot.· \'\0 · o I elct ol \53o ')(. w .., ·c. SUH-MW•\o 8 )< )< )(. X. X.
DUAo6 • \'\o '0'1. l~So A E\. tvt~· " 8 X X X ')( X
o\ o"'IQ.8·1"\o• o'\ \'\lo Mw·\ 8 X X X X X
~\."1.0.1· ,..,. 0 .. 1~45'"' IV\-....1• 3'. i X X X X X
Otoortofl · l'\0 • O$" \'425 ri\W· ~ 8 X "" 1( )<. ~ £r\4 -"" "~!0
D IO'ldl" t<llO •OGr \~60 Mw·S 7 X X ~ )<
'At"""'-tl.• l'\D• 01 \3'lS" N\l.U· 8 8 1-x X )(. X )(
ltno~ae · aQ., • ol • l'l:l.D Mw-'\ e X X )<. X. X
OtDI'o9·l""'.dl )iL \&.1.~() ~~~~ ~~~~ ~~ ~'·A\~·\3 8 X X X )<. X
i
i ' APEX-RoanokE 08010146 O i .... Short Stop o . DUE: 10 Cays ... ! IIIIIIJimiDmll 911 ~i Reed: 01f11108
TOT AU l7t <\ '\ 9 '\ B !
-; .... Q/24) .,...rn-;r irjj~lA ~ 1
• ..._w..r ..,. (~) o.e.rn-........, .., (,..... ...... ,
1-n-cec ® @
,..........,) " lD·.(.')W 1\ .. ~) 0 (f'tWM) ~..W}
..)ft~C. SP-v•~o~ltt1 .hh;\Y\ \~..u
.. .....,.._ lor. (Sllll-•) O.t./T"-•-'-' llr-(SIGttcr1W9) G ..__
® ® NC...· Al\~~6~ o,c.. ~~
( .......... , (l'rlftiW)
~'" WMITt •> ...-r(ecc.......-~: -••" ......,., : TlU.OW •> _....,. _, : ,_ .,,. ....,..,...... -__ \.____ of _4\ __
·-----.--------..... --Jif'-•t·-·· _ ........ ·-··
1.
2.
AIR .
WT.A:~·R. ·wrtU.D···.
2109A North Hamilton Street • Richmond, Virginia 23230 • Tel: (804) I
Sample Conditions Checkl
labiONo.:
Date Cooler Opened:
Are the samples relinquished by aamplel'?
If not. ara custody 5681& used?
3. If yes, are custody seals unbroken and Intact et the date end time of amvel7
4.
5.
6.
7.
8.
9.
10.
11.
12.
Are lhe custody papers filled out completely end correctly?
Do all container labels agree with QJstody papens?
Are lhe samples rscatvod on lea?
Is the temperature blank or reprasantattve sample within eccap!abla Dmlts?
(4 :i: 2 .C)
Are all aamples wlthfn holding lfme forrequastad tests?
Is e sufficient amount of sempla provided to pertonn the tests Indicated?
Are all samples In proper contslneB fur the analyses requested?
· Are all samples apProPriately preserved for the analyses requested?
Are aU volatile organic contaiMl'!l flee of headspace?
·. COMMENTS
il APEX-RoanokE 08010146
~i o: -· *! I I I
Short Stop
IIDIIIHIIRIII!IDiilmD
ru HQ .tilA
0 GY' 0
0 ~ 0
0 D ~
a 0 o ·
GY' D 0
c:Y D 0
~ D 0
Q' 0 0
D' 0 D
cr D 0
cg/ 0 D
e{ 0 0
CUE: 10 Daye
Ra: 01111108
··~·········"· ........ -.
AWS Sample Condllkq Chedcllat_071107 .x1s
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I ~~b·t~f~(§J;]l~(ff; ~J~~.: ,: .,A~h .... ::~·. ~~. ·. :.·.~; .. j ;, .r .,· .. ·-:_~·!,: ...... :j
.=:T'Hrfi.:t:Ao!iR.iN1 riNvrRo'N·MENTAL:·+EsriNG:J.:.
I Clieut AirWatet&Soil Laboratorin(1091) .
2109 N. Hamlltoo Stm:t
I RJchmond, VA 23230
Alln AWSPM
I
Worlc Order:
Project Name:
Project Number:
Receiwd:
ANAL VTICAL REPORT
NRAII68
NC Trust Worlt
08010146
Ol/121011 08:05
Dlluttoa Analysll
. ~~~.e .............................. · ... ~-'!~ ........ ~ ........ '!~~~-.............. ~ ....... ~~~~ ... ~~!~~-..... ~~~-~ ...... ~.t~~-.
I Sample ID: NRA1168-01 (08010146-001 -Water) Sampled: 01/09/08 15:30
MADBPVPH
Methyl tm·Butyl Elbcr 68.1 ug/L 3.00 01116108 23:32 MAD.HPVPH 8012522
B~ 13.5 ug/L 1.00 01/16/08 23:32 MADEPVPH 8012522
ToiiU!De NO ug!L 3.00 o1n6108 23:32 MADEPVPH 8012522 I
Ethylbca%eoe 7.72 uafL 1.00 011\&08 23:32 MADEPVPH 8012522
m,p-Xyleaa ND u&fl. 4.00 0 ln6108 23:32 MADEPVPH 8012522
o-Xy!CDC ND tJ&'L 2.00 0 Itt 6108 23:32 MADEPVPH 8012522
Napbthaleoe 33.5 ug/L 5.00 01 /16108 23:32 MADBPVPH 8012522 I
CS. C8 Aliphatic Hydrocarbans, UoadjusW 441 uafL 100 01116108 23:32 MADEPVPH 8012522
C9 • C12 Aliphatic Hydrocarbo01, Uaadjuall 990 uw'L 100 01/16108 23:32 MADEPVPH 8012S22
C5 • C8 Aliphatic Hydrocarbons 360 u&fl. 100 01/16108 23:32 MADBPVPH 8012522 I
C9 • Cl2 Aliphatic Hydrocarbona 393 uw'L 100 Ollt 610823:32 MADEPVPH 8012522
C9 • CIO Aromatic HydrocatboM 589 uBfL 100 01/16108 23:32 MADEPVPH 8012522
Swr: 2,$-DlbrolfiOiolrmre (FJD) (7()..1 Jmt! 95" 01116108 23:32 MA.DEPYPH 8011522
Surr: 2,5-Dfbromoto/ucne (PID) (7()../JO"l 81" 011/6108 23:32 MADEPYPH 8012521 I
MADEPBPH
C9. Cl II AliphAtic Hydrocarbons ND u~VL 103 0111&'08 20:31 MADBPEPH ~12165
C19 • C36 Aliphatic Hydroembom ND ~ 103 01/16108 20:31 MADBPE.PH 8012165 I
Cll • C2l Aromatic HydroearboDJ 268 ug!L 103 01116108 20:31 MADEPE.PH 8012165
Cit • C2l Aromatic Hydrocarbons, Unadjus 319 u&'L 103 01/16108 20:59 MADEPBPH 8012165
2-Motbylnapblhale~~e 14.7 ug/L 10.3 01116108 20:59 MADBPBPH 8012165
Ac:collphtheno NO ugiL 10.3 01/16108 20:59 MADBPBPH 8012165 I
AcenapbUlyleoc ND ug/L 10.3 01/16108 20:59 MADEPBPH 8012165
A.ntlulce:J)C ND uafL 10.3 01/16108 20:59 MADEPEPH 8012165
BCDZO (a) anlhracCIIc ND ugiL 10.3 01/16108 20:59 MADBPEPH 8012165
Ba!ZO (a) pyn:ae NO uafL 10.3 01 /16108 20:59 MADEPBPH 8o1216s I
Benzo (b) tluol'lnlhenc NO ugiL 10.3 Otn6108 20:59 MADEPBPH 8012165
Btmo (&.bJ} pcrylene NO ug/L IOJ 01116108 20:59 MADBPBPH 80ll16S
BIIIIZO (k) fluoi'III1heoe NO ug/L 10.3 01116108 20:59 MADEPEPH 8012165 I
Cbrylenc ND ug/L 10.3 01116108 20:59 MADBPBPH 8012165
Dibeu (a,b) anth:raeeue NO ug/L 10.3 0 !/16108 20:59 MADEPBPH 8012165
FIUOI'Inlheoe NO ugiL !0.3 01/16108 20:59 MADE.PBPH 8012165
Flu0111ne ND ug/L 10.3 . 01116108 20:59 MADEPEPH 8012165 I
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Indeoo (1,2,3-od) pyrone NO uWI. 10.3 01/16108 20:59 MADEPBPH 8012165
Napblhalene 36.4 ui/L 10.3 01/16108 20:59 MADBPEPH 8012165
PhCD&llthmle ND u&fl. 10.3 01/16108 20:59 MADBPEPH 8012165
Pyrone NO Ua/L 10.3 01116108 20:59 MADBPBPH 8012165
Surr: I·Citlorooctod.:on4! (~14~ 61" 01/16108 20:31 MADEPEPH 8012165
Surr: o·T•rp/Mtry/ (4()..U ()Hj 96 " 01116108 20:59 MADEPEPH 8012165
SIITT; 2-Bl'OmonaphthtJime (40./#f»fJ 114" 01116108 20:59 MADEPEPH 8012165 I
Surr: 2-FluOI'Oblphrrryl (4()..14~ 121" Of/16108 20:59 MA.DEPE.PH 8012165
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Page 2 of 19
Client Air Water&. Soil Labondorie~ (7091)
2109 N. HIIDiiltou S11eet
Richmond, VA 23230
Attn AWSPM
Work Order:
Project N11111e:
Project Number.
Rcc:eived:
ANAL \'TICAL REPORT
NRA1168
NC Trust Wcnk
08010146
0 1/12/08 OB:OS
DDuttoa Aaalyd.s
. ~~~!~~-................................ ~!-~·~ ........ t:i.':~ ........ l!~~~·-.......... -.. -~ -.. -.. ~·~~~ -.. ~~~~-..... -~-"-~-~~-. -... ~-·-t~~-·-
Sample m: NRA1168-02 (08010146-002-Water) Sampled: 01/09/08 14:50
MADEPVPH
Methyl tcrt·Butyl Ether ND usfL 3.00 01117/08 00:03 MADEPVPH 1012522
Benzene 2.11 ug/L 1.00 01117/08 00:03 MADEPVPH 8012522
Toluene l.:Z7 ug/L 3.00 01117/08 00:03 MADEPVPH 8012522
Elhylbemeue 16.0 ugiL 1.00 01117108 00:03 MADEPVPH 8012522
m,p-X yleno ND ugiL 4.00 01117108 00:03 MADEPVPH 8012522
o-Xylene ND ug/L 2.00 01117/08 00:03 MA.DePVPH 8012522
Naphthalene 9.!6 ug/L s.oo Ol/17/08 00:03 MADEPVPH 8012522
CS -C8 Alipb•tic Hydrocarbons, UoadjllltC( , .. ug/L 100 01117/08 00:03 MADEPVPH 8012522
C9-Cl2 Aliphatic Hydrocarbons, UnadjusU 493 uWL 100 01117/08 00:03 MADBPVPH 8012522
C5 • C8 Alipbalic Hydroc:erbolls 789 ugiL 100 01117108 00:03 MADil.PVPH 8012522
C9-Cl:Z Aliphatic Hydroc:arl>ons 223 ug/L tOO 01117/08 00:03 MADEPVPH 8012522
C9-CIO Aromatic Hydrowbona 154 ug/L tOO 01117/08 00:03 MADBPVPH 8012522
Surr: 2.5-Dibromoroluene (FID) (70-13~ 94" 01117108 00:01 MADEPJIPH 8011121
Surr: J,J-Dibromotahwre (PID) (70-13~ 86" 0/117/08 OO:OJ MADEPYPH 8011J11
MADBPBPH
C9 -Cl B Alipbatic Hydrocatboas ND ugiL lOS 01/16108 22:48 MADEPBPH 8012165
Cl9 • C36 Aliphatic Hydrocarboas ND uaiL lOS 01/16108 22:48 MADEPEPH 8012165
Cl1 -C22 Aromatic Hydrocarllons ND uWL lOS 0 tlt 6108 22:48 MADEPEPH 8012165
C11 -C22 Aromatic Hydrocarbons, UnadjUI ND Ua/L lOS 0111610123:16 MADEPEPH 801216.S
2-Methylnapbtbaleoe ND ua/L lO.S 01116108 23:16 MADEPEPH 801216S
Acenapbtbcme ND ug/L tO.S 01/16108 23:16 MADEPEPH 801216S
Acenapblhyleoe ND ug/L to.s 01/16/08 23:16 MADBPEPH 8012165
Anlbraceno ND ua/L 10.5 01116108 23:16 MADEPBPH 8012165
Benzo (a) antbnlceoa ND ug/L 10.5 01116108 23:16 MADEPEPH 8012165
Beozo (a) pym1e ND ug/L tO.S 01116101 23:16 MADEPEPH 801216S
Benzo (b) f!IIOralltbeno ND u&fl.. IO.S 01/16108 23:16 MADEPBPH 80l:ZI6S
Benzo (l,b,i) peryletl(l ND lla/L Ill.$ 01116108 23:16 MADEPI!PH 8012165
Benzo (k) fluon,Qibene NO ua/L 10.5 01/\6108 23:16 MADEPEPH 801216j
Chrylene ND u&fL 10.5 01116108 23:16 MADEPEPH 8012165
DibeiiZ (a,h) anthracene NO ug/L 10.5 01116/08 23:16 MADEPEPH 801216S
Fluol'llllheno ND ug/L 10.5 01116/08 23:16 MADBPEPH 8012165
Fluorene ND ug/L lO.S 01/16108 23:16 MADEPEPH 8012163
lndcno (1,2,J·cd) pym~e ND uaiL IO.S 01116108 23:16 MADEPEPH 8012165
Naphtbaleoe ND uaiL lO.S 01/16/08 23:16 MADEPEPH 8012165
Pbenanthn:Dc ND ug/L lO.S 01/16/08 23:16 MADEPEPH 8012165
PyrCDc NO ug/L 10.5 01116/08 23:16 MADEPEPH 8012165
Surr: J. Chlorooctodtcan' (40-14~ 76" 0/1/MJII 12:4fl MADEPEPH 801216J
Surr: o-Terphtny/ (40-U~ 96" Olll61081J:J6 MADEPEPH BOI1l6J
Surr: 2-Bf'DmONZplrJliDJm• (40-Uon) 111" ()JI/6108 13:16 MA.DEPEPH 80/216J
Surr: 1-F/uoroblpheny/ (40-UO%) 110" 0111610811:16 MADEPEPH 80l216J
Pagc3 of 19
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Client
A tiD
Air Water & Soil Laboratories (7091)
2109 N. Hamilton Stttet
Ricbroond, VA 23230
AWSPM
w orlc Order:
Project N11111e:
Project Number.
llccclved:
NRAil68
NC Trust Work
08010146
01/12108 08:05
Dllut!oa Analylb I ANALYTICAL REPORT
. ~~~ ... ___ .... __ ...... _____ ..... _ .... ~-~~~ ....... -~~-........ l!~~~ .... _ .. _ ..... -~ ...... -~~~~~~ ... ~!~.~~-..... -~-e_t~~~ ...•.. ~.t~~-.
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Sample ID: NRA1168-03 (08010146-003 -Water) Sampled: 01109/08 14:30
MADEPVPH
Methyl tert·Butyl Btber 16.0 usfL
Beoune NO uJIL
Tolucoe ND UWL
Ethytbcmene ND u&fL
m,p-Xyleae ND ugiL
o-Xy\ene ND Ui/L
N1pbthalene ND ug/L
CS-C8 Alipha.cic Hydrocarboas, Unadjuste( NO IJII'L
C9-C12 Aliphatic Hydrocarbooa, UDidjUJtr ND u&fL
CS -C8 Aliphatic Hydroalrbons ND ugiL
C9-C12 Aliphatic Hydrocarbous ND usfL
C9 -.CIO Aromatic Hydrocarbo111 ND ua/L I Surr: 2,S-Dllwonlotoluen• (F/D) (70-1 3~ 104"
.. sUrr: 1,J-Dibromotolll-(PID) (70-JJ~ l OS "
MADBPEPH
I C9 • CIS Aliphatio Hydrocarlxm.l ND ug/L
Cl9-C36 Aliphatic HydroCIUboDB ND ug!L
Cl l • C22 Arumattc HydrocarboDS ND ug/L
Cll • C22 Aromatic Hydrocarboaa, Ul*ljus NO ug/L
I 2-Metbylnapblhaleoe ND ug!L
Ac:enapbtbeDc ND ug/L
Aceoapbthylane NO ug/L
I .
Anthmceoe ND ug/L
Bell7.0 (a) Ill t.bmcetlo ND ug/L
Benm (a} pyn:oe NO ug/L
Bonzo (b} tluom~thcne ND ug/L
I Benzo (s,h,i) perylene ND ug/L
Bemo (It) flUOI'ID1hene ND ug/L
ChrySCIIlC ND ugiL
Dibeu (&,b) a~~lhrac:eno ND ug/L I Fl uotUitbenll NO ug/L
Fluoreo11 ND uJIL
hldcoo ( 1,2,3-cd) pyre:oc ND uaJL
I Niphtbalcue ND u&fL
Pboaldlhrene ND llg/L
Pyreoe NO uaJL
Sllrr: 1-Chlorooctad~ (40-J4cm) 71"
I Surr: o-'T'erphenyl (4fJ..U()'J(I) 9J"
Surr: 1-Bromonaphtha/ens (40-U~ /20"
Surr: 1-FIIIorobipht!IO'I (40-U~ 111"
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3.00 01/17/08 13:19 MADBPVPH 8012728
1.00 01/17108 13:19 MADEPVPH 8012728
3.00 01/J 7.1)8 13:19 MADBPVPH 801272&
1.00 01117/08 13:19 MADEPVPH 8012728
4.00 01/17108 13:19 MADBPVPH 8012728
2.00 01/17108 13:19 MADBPVPH 8012718
5.00 Ot/17108 13:19 MADEPVPH 8012721
100 01/17108 13:19 MADBPVPH 8012721
too 01/17108 13:19 MADBPVPH 8012728
100 01/17/08 13:19 MADEPVPH 8012718
100 01/17108 13:19 MADEP VPH 8012728
100 01/17108 13:19 MADBPVPH 80127211
01/J 7108 JJ: /9 MADEP YPH 1012718
01//7/01 JJ:/9 MADEP YPH 8()12728
104 0111610113:43 MADEPEPH 8012165
104 01116/08 23:43 MADEPEPH 8012165
104 0 1(16108 23 :43 MADEPEPH 80121155
104 01/17/08 00:11 MADBPEPH 8012165
10.4 Ol/17101 00: II MADEPEPH 8012165
10.4 01/17/08 OO:Il MADBP EPH 8012165
10.4 0\/17108 00:11 MADBPBPH 8012165
10.4 01117108 00: II MADEPEPH 1012165
10.4 01117108 00; II MADEPEPH 8012165
10.4 01117101100:11 MADEPBPH 8012165
10,4 01117/08 00:11 MADBPEPH 8012165
10.4 01/(7/08 00:11 MADEPEPH 8012165
10.4 01/17/08 00: II MADEPBPH 8012165
10.4 01/17101 00:11 MADEPEPH 8012165
10.4 01/17108 00: II MADEPEPH 80\l16S
10.4 01117108 00: II MADEPEPH 8012165
10.4 01117108 00:11 MADBPEPH 8012165
10.4 01117108 00:11 MADEPEPH 8012165
10.4 01/17/08 00: II MADEPBPH 8012165
10.4 01117/01 00: II MADEPEPH 8012165
10.4 01/17108 00:11 MADBPEPH 8012165
01116/08 23:43 MAIJEPEPH 80W6S
OJ// 7/08 00: JJ MADEPEPH BOJ216S
01/17108 00: I I MADEPEPH B0/116S
01117/01 00: J I MADEPEPH B0/2165
Pqc 4 of 19
Cliect Air Water & Soil Laboratoria (7091)
2109 N. H1111illo.n Street
Richmond, VA 23230
Attn AWS PM
WockOnfer. NR.AII68
Projec:t tume.: NC TI'\ISt W oz:k
ProjectNu~ 08010146
Rl!c:eived: 01/12108 OI:OS
ANALYTICAL REPORT
DUu don A.nalyala
. ~~.e .. : .............................. ~.~~~ ........ ~.~-........ 1!~ ............... ~ ...... !~~~ ... _D.~~~-~~-..... ~.e.t~~.~ ...... ~.a.t~ ..
Sample ID: NRA1168-4J4 (08010146-004-Water) Sampled: 01/09/08 14:45
MADEPVPH
Melhy1 tert-Buty1 Blher ND ug/L 3.00 01117108 13:49 MADBPVPH 8012728
BeiiUlle NO ug/L 1.00 01117~8 13:49 MADEPVPH 8012128
Toluene NO ug/L 3.00 OI/J7{{)8 13:49 MADEPVPH 8012728
Elhylbeuzcne NO uatL 1.00 01117{{)8 13:49 MADBPVPH 8012728
m,p-Xylcoc NO ui/L 4.00 01117/08 13:49 MADEPVPH .8012728
o-Xyleno NO ~ 2.00 01/17/08 13:49 MADBPVPH 801272B
Naphtha! cue ND u&fl. ~.00 01/t 7/08 13:49 MADBPVPH 8012728
CS • C8 Aliphatic Hydroc&Jbolll, Uuadjui!Cc ND ugiL 100 01117/08 13:49 MADBPVPH 8012728
C9 • C12 Alipbatic HydrociUbooa, Unadjustt ND ugiL 100 01117101 13:49 MADBPVPH 1012728
CS • C8 Aliphatic Hydroc:aJboos ND ~ 100 0 1f1 7/08 t3:(9 MADBPVPH 8012728
C9 • Cl2 Alipba!ic Hydroc:IUboaa ND lt3"L 100 01/17108 13:49 MAOEPVPH 8012728
C9 • ClO Aro~m~tic Hydrocarboos NO ugiL 100 01117108 t3:49 MADBPVPH 801272~
SUJT; 1,5-DibrcHnotolwn• (FJD) (70-JJ(M) Ill " 01/17/fM 13:49 MADEPYPH 8012728
Slu-r: 2,J-Dibromotolum• (PID) (70-1 JO~ 109 ~ 0111 7/CJ8 JJ:49 MADEPYPH 8011728
MADEPBPH
C9-Cl8 Aliphatic Hydrocarbons ND ui/1 108 01117/08 00:38 MADEPBPR 801216S
Cl9 • C36 Aliphatic Hydroc:IUboos ND u~ 108 01117/08 00:38 MADEPEPH 8012165
Cll -C22 Aromatic Hydrocarbons ND ug/L 108 01/17108 00:38 MADBPEPH 801216S
C II -C22 Aromatic Hydrocarllona, Unlldjua ND ug/L 108 01/17/08 01:06 MADBPBPH 801216S
2-Molhylnapb1halane ND uJI{L 10.8 01117/08 01:06 MADEPBPH 801216S
Acenaphtheoe ND ug/L 10.8 01117108 01:06 MADEPEPH 8012165
A.ceoapbthyl&~~e ND ugiL 10.8 01117~8 01:06 MADBPEPH 801216S
Allthraoene ND uatL 10.8 01/17/08 01:06 MADEPEPH 801216S
Bent.D (a) a.nlhnlcene ND ug/L 10.8 01/17/08 01:06 MADBPEPH 8012165
Benzo (1} pyrcne ND uJI{L 10.8 01/17/08 01:06 MADBPEPH 801216~
Benzo (b) f!UOIBDthena ND ufiL 10.8 01/17/08 01:06 MADEPBPH 801216S
Beuzo (J,b,i) perylene ND IIJI/L 10.8 01/17/08 01:06 MADBPEPH BD12165
Benzo (k) fluormtbene ND ugiL 10.8 0 l/17/08 Dl :06 MAOEPEPH 8012165
CbryllCne ND ullfL 10.8 01/17108 01:06 MADEPBPH 801216S
Dibenz ( a,h) IIDihraeeDe ND ullfL 10.8 01/17/08 01:06 MADBPEPH S012165
FIUOBrllbenc ND u;IL 10.8 Ol/17108 01:06 MADEPEPH 801216S
FIU<Il'eDO NO u&fL 10.8 01/17108 01:06 MADBPBPH 8012165
IDdeoo (1,2,3-cd} pyrcnt ND u&fL 10.8 01117108 01 ;06 MADEPBPH 8012165
N~tbaleoc ND ugiL 10.8 01/17108 01:06 MADBPBPH 8012165
PbeJIIIIthrene NO uWI. 10.8 01/17108 01:06 MADEPEPH 8012165
Pyreuc ND uJI{L 10.8 01/17/08 OJ :06 MADBPBPH 8012165
Su1'T: J-Chlorooc~ntl (40-U~ 6.!" 01117/08 00:38 MADEPEPH li01216J
Su": o-T11rpheny/ (40-UO"J 81% OIIJ7/CJ8 01:06 MADEPEPH 8011J6J
Su1'T: J-Brolfl()naphthalllflt (40-UO'J6) 118" 0111 7/CJ8 01:06 MADEPEPH 8012J6J
Surr: 1-Fiuoroblphmy/ ((0-UO"J 115" OIIJ7/CJ8 OJ :06 MADEPEPH 8012165
PageS of 19
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2860 Foil« Cnllghton Road N...,...o, TN 37204 • 800-71111-0DIIO * Fu 811l-n&.:W04
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Client Air Water & Soil Labomaries (7091)
2109 N. Hamiltoo Street
Richmond, VA 23230
A11n AWSPM
Wotlc Order:
Project Nama:
Project Number.
Received:
ANALYTICAL REPORT
NRA1168
NC Trutt Worlt
08010!46
0!112108 08:05
DUudoa Aoal)'lll
. ~~~~-...................... .' ......... ~~-~~ ....... -~ .. -..... '!~ .............. -~ ...... -~~ ... ~~~~-..... ~e-~-~ ...... ~-~~-.
I Sample ID: NRA1168-05 (08010146-005-Water) Sampled: 01/09/0814:25
MADEPVPH
Methyl tert-Butyl Ether 9.19 ugiL
BI!DZIIDII ND
Toluene ND
Bthylbemme ND
Ua/L
uaiL
u8fL I
m.p-Xylene ND
o-Xyhme ND
Napblhllene ND
uJVL
u&fL
ua/L I
C5 -C8 A1ipbatic Hydroc:ubonl, UnadjiiSic( NO uJIL
C9-CJ2 Aliphatic Hydtoc:arboDJ, Unldjustc ND
C5 -C8 Aliphatic Hydrocarbon& ND
C9 -C 12 Aliphatic Hydroc:arllons ND
II&'L
uaiL
ug/L I
C9 -Cl 0 Aromatic Rydroc:arbcns ND u&IL
Surr: 1,5-Dibromotoluea (FID) (70-/JrYI') 106"
· Swr: 1,5-Dif,r,motolum• (PJD) (70-JJrYI') UUH I
MADEPHPH
C9 • Cl8 Aliphatic Hydrocarl:loDS ND
Cl9-C36 AliphAtic Hydrocarbons ND
C11 -C22 Aromatic Hydrocarbon~ NO
Us/L
II&'L
uaiL I
C II -C22 Ammatic Hyctroc:arllool, Unadjus ND
2-MI!Ihylnaphtbaleoe ND
Acenapbthone ND
uaiL
u,&IL
ugiL I
Acmapbthy1ene ND u&fL
Antlneene ND
Benzo (a) aothracene ND
BIIDZAI (a) pyrene NO
uaiL
u,&IL
u&fL I
Balzo (b) flucnn1he:ne ND uJIL
I BC1121l (s,h.i) perylene ND
Beazo (k) fluotiUlcbene NO
ugiL
uafL
ChryiOCle NO uw'L
Dibenz (a,b) utbrKene NO
Fluor&lllbeDc NO
Fluon:ae ND
uw'L
uwt-
u&fL I
Iudeno ( 1 ,2.3-cd) pyrene ND ua/L
Naphthalene ND
PbCIIWI!hrene ND
pyrooo ND I uJIL
uJIL
ucfL
Su": 1-Chloi'O()CtRt/emne (~0-UO'U) 6696
Su": o-Tuplrenyl (~0-U~ 81"
Su": 2-Bromonaphthal•ne (40-UOH) 123"
Sw": 2-Fluoroblplwnyl (40-UOH) 123"
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:too 01117/08 14:20 MADEI'VPH 8012728
1.00 01/17108 14:20 MADBPVPH 1012728
3.00 01/17/08 14:20 MADBPVPH 8012728
1.00 OL/17/08 14:20 MADBPVPH 8012728
4.00 01117/08 14;20 MADBPVPH 8012728
2.00 01/17/08 14:20 MAOEPVPH 8012728
5.00 01/17/08 14:20 MAOEPVPH 8012728
100 Ol/17/08 14:20 MADBPVPH 8012728
100 01117108 14:20 MAOEPVPH 8012728
100 Ol/17/08 14:20 MAOEPVPH 8012718
100 01117108 14:20 MADEPVPH 1012128
100 01117108 14;20 MADEPVPH 8012728
01/17108 U:20 MA.DEP 'YPH 8012728
01/11108 U:20 MA.DEP 'YPH 8012728
182 01117/08 01:33 MADEPEPH 8012165
182 01/17/08 01:33 MADEPEPH 8012165
182 01117108 01:33 MADBPBPH 8012165
182 01/17108 02:00 MADEPBPH 8012165
18.2 0 Ill 7/08 02:00 MADEI'BPH 1!012165
18.2 01117/08 02:00 MADEPBPH 8012165
18.2 01/17/08 02:00 MADBPEPH 8012165
18.2 OJ/17/08 02:00 MADEPBPH 8012165
t8.2 01117108 02:00 MADBPEPH 8012165
18.2 0111 7108 02:00 MADEPBPH 8012165
18.2 01117/08 02:00 MADEPBPH 8012165
18.2 01/17/08 02:00 MADI!PBPH 8012165
18.2 01117/08 02:00 MADEPEPH 8012165
18.2 01117108 02:00 MADEPBPH 8012165
18.2 Ol/17/08 02:00 MADEPBPH 8012165
18.2 01117/08 02:00 MADBPEPH 8012165
18.2 0 1117/08 02:00 MADEPBPH 8012165
18.2 0\1\7108 02..'1)() MADBPBPH 6012165
IS.l 01117/08 02:00 MADEPEPH 8012165
18.2 01/17/08 02:00 MADBPEPH 8012165
IB.l 01117/08 02:00 MADBPBPH 8012165
OJ//1/080/:3J MADEPEPH 8012165
01111108 02:00 MADEPEPH 80/2165
01/1 '1108 01:00 MA.DEPEPH 80/2165
01/17/08 02:00 MADEPEPH 801216$
Page 6 of !9
2880 f'clmr CnJuhiDI Raed N.-11'418, TN 37204 • IIOCHtltl-0980 ' Fax 1116-72&-~<104
Client Air Water & Soil Lahoratoriea (7091)
2109 N. Hamilton Slnlet
R.ichrnond, VA 23230
Attll AWSPM
Work Order;
Project Name:
Project Number:
Received:
ANALYI'ICAL REPORT
NRA1168
NC Trust Work
08010146
01112108 OB:OS
Dllatlou AnaJyt!l
. ~~~e ................................. ~·-~~~ ........ t:J.~~ ........ 1!~~-........ -.... -~.-... -~~~~~ ... ~!~~~-..... -~~~~ ...... ~-~~-.
Sample ID: NRA1168-G6 (08()10146--(106-Water) Sampled: 01/09/08 14:00
MADBPVPH
Methyl tat-Butyl Ether ND ug!L 3.00 ottt7ros 14:51 MADEPVPH 8012728
BellZCIIC NO ugiL 1.00 Olll7ros t4:51 MADEPVPH 8012128
Toluene NO ug!L ).00 01117/08 14:5 I MADBPVPH 8012728 .
Etbylbeu:zcDe ND ug!L 1.00 01117/08 14:51 MADEPVPH 8012728
m,p-Xylooe ND Us/L 4.00 01117/08 14:51 MADEPVPB 801212a
o-Xylme ND uaiL 2.00 01117108 14:51 MADBPVPH 8012728
Naph!haleae ND ugiL s.oo 01/17/08 14:51 MADBPVPH 8012728
CS • C8 Aliphatic Hydrocarbons, U!llldjusleC ND ua/L 100 Oln7/08 14:st MADEPVPH 8012728
C9 • C12 Aliphatic Hydrocarbon&, Unadjusu ND Ua/L tOO 01/17/08 l4:St MADEPVPH 801212!
C5 -CB Alipbatic Hydrocarbous ND u&JL 100 01/17/08 14:.51 MADEPVPH 8012728
C9 • Cl2 Alipbatic Hydroc:arbo01 ND ugiL 100 01117/08 14:St MADBPVPH 8012728
C9-CJ 0 Aromatic Hydrocarbons ND uaiL 100 011!7108 14:.51 MADEPVPH 8012128
Su": 2,$-Dibromotoluene (FID) (70.13(M) /OJ" 01/17/rM U:JI J.UDEPYPH 80/171/J
Surr: 1,5-Dibromotolut:n~ (P!D) (70.1 J~ 109" 01117108 U:SJ MADEJ> 'IPH 80/272/J
Page7ofl9
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Air Water & Soil Labo~ories (7091)
2109 N. Hamilton Street
Richmond, VA 23230
AWSPM
Work. Order:
Project Name:
Project Numba':
Received:
ANALYTICAL REPORT
NRA1168
NC Tnllt Wade
080101.6
01/12108 08:05
Dilution A.Dalyala
. ~~~~ ............................... -~-~~ ........ ~ ....... :t?~ .............. -~ ...... ~~-~~ ... ~~~-~ ...... ~~ ...... ~~ ..
I Sample ID: NRA1168-07 (08010146-007-Wat.er) Sampled: 01/09/0813:35
MADEPVPH
Methyl tert·Butyl Ether 856 u&fl..
Bcozene ND uafL
Toluene ND u&fL I Blhylbenzene ND uafL
UlJ)-Xylcue ND usfL
o-Xyleoe NO usfL
NiphtbalCDCI ND ug/L I
CS • CB Aliphatic Hydrow'bons, Unadjuat« 3590 uaiL
C9-Cl2 Aliphatic Hydroll&l'bons, Unadjusk ND uafL
CS • C8 Aliphatic Hydroc&rbons l7JO ua/L
C9-C12 AliJibetjc Hydroc:arboas NO ugiL I
C9-CIOAnmuticH~ NO ti&'L
Swrr: 2,5·Dibromotoluurt (FID) (10-1 3~ 96"
Sun-: 1,5-Dlbromotolutn• (FID) (70-JJfM) 107" I Sun-: 2,5-Dlbromotolutne (PJD) (70-130") JOO'K
Sun: 2,5-Dibromotofutllt (PJD) (7D-1Jfm) /06"
MADEPEPH
C9-Ct8 Alipbetlc Hyclroccboos ND u&fL I
Cl9 • C36 Alipbatk: H)'droccboaa ND uaJL
Cl 1 • C22 Aromatic Hydrocarbons ND uafL
C\1-C22 Arotaatic Hydrocarbon•, Uolllijus ND ug/L I
2-M.etbylnapbthalene ND u&fL
Ace~~~phtbene ND uaiL
A.cenaphthyleoe ND ua/L
Aothrlccoe ND ugiL I
BOCZD (a) IIDtlnceoe ND Q&IL
BtmlO(a)pyrcoc ND ug/L
Bc:oz.o (b) fluoranlbC!!o ND uaiL
Bmzo (a.b.i) pery1coe ND ugiL I
Bcmo (k) fluomnbeDII ND uaiL
Cb:yiCDC NO us/L
Dibalz (.,h) llltlnceoe ND ullfL I
F!UOIIJithcue ND ullfL
FlUimllll ND us/L
lndc:ao ( 1,2,.3-cd) pymlC ND uafL
Napbthalme ND uafL I
PbciWithrcne NO ugiL
Pyrono ND ugiL
St.il'l": 1-0.Iorooctadecan~ (40.140") 61~
Swrr: o-Twphmyl (4D-Uot4) 89~ I
Sw-r: 1-Bro~len. (40-UO'KV 121"
Swn-: 1·Fiuoroblphuryl (40-UO~ /27" I
I
30.0
1.00
3.00
1.00
•. oo
2.00
5.00
tOOO
\00
1000
100
100
100
100
100
100
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
tO.O
10.0
10.0
10.0
10.0
10.0
10
10
I
10
01/18108 11:33
01/17Al8 15:21
01/17108 15:21
01/17108 15:21
Ol/17108 15:21
01/17108 1S:21
01/17108 15:21
01118108 11:33
01117108 15:21
01/1~ 11:33
01/17108 15:21
01/17108 15:21
0//1710815:11
01//8/0B 11 :JJ
OJ/11/08 15:11
01118108 Jl:JJ
0 ill 7108 02:28
01/17108 02:28
0 Ill 7108 01:28
01/17108 02:5.5
01/17108 02:.5.5
01/17/08 02:5.5
01/17/08 02:.55'
01/17108 02:.55
01117108 02!5.5
01117108 Ol:SS
01/17108 02:5.5
01/17108 02:.55
0 ill 7/08 02:55
OJ/17/tlB 02:.55
01117108 02:55
01/1710802:55
01/17108 02:55
01/17/08 02:55
01/17/08 02:5.5
01/17108 02:SS
01/17108 02:55
OJ//7108 01:28
0/117108 01:55
OJ// 1108 02:55
01/17108 02:SS
MADEPVPH 8013000
MADEPVPH 8012728
MADEPVPH 8012728
MADEPVPH 8012721
MADEPVPH 8012728
MAOEPVPH 8012728
MADEPVPH 8012728
MADl!PVPH 8013000
MADEPVPH 8012728
MADEPVPH 1013000
MADEPVPH 8012728
MADBPVPH 8012728
MADBP Jo'PH 8011728
MADEP Jo'PH 8013000
MADE.P JIPH 8011728
MA.DEPYPH 80/3000
MADEPEPH 801216.5
MADEPEPH 1012165
MADEPBPH 8012165
MADEPBPH 8012165
MADEPEPH 80lll6S
MADEPEPH 8012165
MADBPEPH 801216.5
MADEPEPH 8012165
MADEPEPH 801216.5
MADEPEPH 8012165
MADBPEPH 8012165
MADBPEPH 8012165
MADBPEPH 8012165
MADEPBPH 8012165
MAD5PBPH 8012165
MADEPBPH 1012165
MADEPBPH 801216.5
MADEPEPH 8012165
MADEPEPH 8012165
MADEPEPH 801216.5
MADBPBPH 801216S
MADEPEPH 8011165
MADEPEPH 8(}J116S
MADEPEPH 8011165
MA.DEPEPH 8011165
Page 8 of 19
. .
NO ',o ,.,. 0 • •• : .. •; ,) ... t ..... J,, ··,~:,,;• •,:!•,, ', .... ',,••: ... 0 :•, ', 0 '00::•,'•;.' .. o' • ..:: 0 0 'lo :'',•'. i.·Jl:tf.l,:~rJI~~U~fEH\.'IRqNM~TAL'~STJNO::·i
Client Air Watc:t & Soil Laboratories (7091)
2109 N. Hamilton Street
Richmond, VA 23230
Attn AWSPM
Worlc Order:
Project Name:
Project Number:
Received:
ANALYTICAL REPORT
NRA1t68
NC Tnllt Wodc
080101-46
01/12108 OB:OS
DOadoa Aaaly1U
. ~~~·'· ................................ ~~·-~ ....... -~-~ ........ l!~~ .............. -~ ...... -~~~~ ... ~~!~~~-..... ~e-~-~ ...... ~-~~-.
Sample ID: NRA1168-08 (08010146-008-Water) Sampled: 01/09/0813:20
MADEPVPH
Methyl ten-Butyl Etbcr 663 ug/L 3.00 01117108 IS:$2 MADBPVPH 8012728
8eDUDII ND ugll 1.00 01117108 IS:S2 MADBPVPH 8012728
Toluene NO u&fL 3.00 01117/08 15:S2 MADBPVPH BOt272B
Btbylbenzenc NO uw'L 1.00 01/17108 15:52 MADBPVPH 80127'1.8
m,p-Xyltno ND uw'L 4.00 01117108 I S:52 MADBPVPH 80127'1.1
o-Xylene ND uSfL 2.00 01111108 IS:S2 MADEPVPH 8012728
Naphthalene ND ugll 5.00 01117108 IS:S2 MADEPVPH 8012728
CS • C8 Allpbatic Hydrocarbons, Unadjustee 10800 ugll 5000 50 01/18108 12:03 MADEPVPH 8013000
C9 • C12 Aliphatic Hyd.rocalboos, Unadjusu NO ugiL 100 1 01/17103 15:52 MADEPVPH 8012728
CS • C8 Aliphatic Hydrocarbons 10700 ug/t. sooo so 01/18108 12:03 MADBPVPH 8013000
C9 • Cl2 Allpbatic HydroauboM ND u&fL 100 01117/08 15:52 MADEPVPH 8012728
C9-CIO Aromatic Hydroc:atbo111 ND ug!L 100 01/17108 JS:S2 MADEPVPH 8012728
Surr: 1,5-D/broMQtoluenr (FJD) (7()..130%) 101 " 01/1'1108 I J:JJ !tLADEP J'PH 80/2118
Surr: 1,5-Dibro1Jf0tolu-(FID) (70-13~ 106 " 01//8/08 11:03 MADEI'VPH 8013000
Surr: 1,5-Dibr-omotolumt~ (PID) (7()..1 JiM) 104" 01/1710/J 15:51 MADEP VPH 8012718
Surr: 2,5-DtbromolobJ-(PJD) (70-1 3~ 10!" 01/Ja/08 11~03 MADEP J'PH B0/3000
MADBPEPH
C9 · Cl8 Alipbatic Hydtoearbou ND ug!L 100 01/17108 03:23 MADEPBPH 801216~
Cl9 -C36 Aliphatic Hydtocerooos NO ug!L 100 01/17108 03:23 MADBPBPH 8012165
CII -C22 Aromatic Hydrocarbons NO u&fL 100 01117108 03:23 MADEPEPH 8012165
Cll -C22 Aromatic HydrocarbOilS. Unllljus ND ug/L JOO 01117/08 03:50 MADBPBPH 80\216S
2-Methyblapblbalcne NO ug/L 10.0 Ol/17/08 03:50 MADEPEPH 8012165
Acen'~Jhtblme ND uafL 10.0 01/l7108 03:50 MADBPEPH 8012165
Aoea~tbylcno ND ugiL 10.0 Ol/17/08 03:50 MADEPEPH 8012165
Anthnlcene NO uSfL 10.0 0 l/17108 OJ :SO MADBPEPH 8012165
81111Z0 (11) aathru:eoe NO uSfL 10.0 01/17/08 03:50 MADEPBPH 8012165
Bcnzo (a) pyrene NO . ug/L 10.0 Ol/17/08 03:50 MADBPBPH 801216S
Benzo (b) tluonntbene NO ug/L }0.0 Ol/17/08 03:SO MADBPBPH 8012165
Bcmo (g.b,i) peryleoe ND ug/L 10.0 01117/08 03:50 MADEPEPH 8012165
Benzo (k) fluoraatbc:uo ND ug/L 10.0 0 Ill 7108 03 :SO MADEPEPH 8012165
Cbrysene NO ug/L 10.0 01/I 7108 03:50 MADBPEPH 8012165
Dibenz (a,h) aalhraccne ND ug/L 10.0 01117/08 03:50 MAI>BPEPH 8012165
Fluoranthcno ND u&IL 10.0 Ol/17108 03:SO MADBPBPH 8012165
Fluontno ND ug/L 10.0 o 1/17/08 03 :SO MADBPEPH 8012165
Indeno ( 1 ,2,3-cd) pyre:oe ND ug/L 10.0 01117103 Ol:SO MADBPEPH 801216S
Naphthlllen11 ND uSfL 10.0 01/17/08 03:50 MADEPEPH 8012HiS
Phenaalhreoe ND ug!L 10.0 01117108 Ol:SO MADEPBPH 8012165
Pyrene NO ugll 10.0 01/17/08 03:50 MADBPBPH 8012165
Surr: 1-Chlorooclod«ffne (40-Urm) 67" OJ/17108 03:23 MI.DEPEPH 8012165
Surr: o-Tirphenyl (40-UO") 88" 01/17/08 03:50 MADEPEPH 8012165
Surr: 1-Bromonaph/hQ/ttne (40-140%) [}.0" 01/17108 OJ:JO MA.DEPEPH 801216J
Surr: 1-Piuoroblphenyl (40-/40") /19" 01//7/08 03:50 MA.DEPEPH 8011165
Page 9 oft9
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Client Air Water .t SoU Labor11tories (7091)
2109 N. Hamilton Stteet
Rlcbmoud. VA 23230
Attn AWSPM
Wotk Ordu: NRAII68
Project Namo: NC Trult Work
Project Number: 08010l<t6
Received: 0 lll2108 08:{)5
ANAL \'TICAL REPORT
DUudou Aualyda
. ~~.e ................................. ~':'.~~ ........ ~ ........ t!~~~-............. -~ ...... -~~~~~~ ... ~~~-~~-...... ~.e.t~·o·~ ...... ~~-~~-.
I Sample ID: NRA1168-09 (G8010146-009 • Water) Sampled: 01/09108 14:50
MADEPVPH
Mctbyl tert-Butyl Ether 526 ua/L
Benzene ND
To1ucme ND
Bthylbeuzr:nc ND
uafL
uafL
ug/L I
m,p-Xylenc ND
a-Xylene ND
Naphthalene ND
u&IL
ug/L
ug!L I
C5 • C8 Aliphatic Hydtocarboo&, Unadju.tei 900 uafL
C9-C12 Alipbalic Rydrocadlooa, Uoadjuau ND
CS -C8 Aliphatic Hydtoc:arborila 37~
C9 • C12 Aliphatic Hydrowbooa ND
ugfL
uatL
uafL I
C9 • CIO AroDUitic Hydrocarbona NO
Sllrr: 1,J..Dibro111D101u-(F/D) (1~1 3~ 106"
Sun-: 1,J-DibrolnotolwM (P/D) (10-IJ~ 109H
U&'L I
MADEPEPH
C9-CIS Aliphatic Hydrocarbons ND
C 19 • C36 Aliphatic Hydrocarbon• ND
Cll -C22 Aromatic Hydrocarbim1 ND I ug.IL
ug/L
uafL
C11 -C22 Aromatic HydnlcaJbmll. Uuadjue ND
2-Mo~p~ ND
Aceoapbthene NO
U&'L
u(!L
ug/L I
A.ceoaphthylcne NO ug/L
Anlhrllceae ND
BCDZO (a) mtbtKcno ND
Balzo (1) pyreoe ND
ugiL
ugfL
uafL I
BCIIIZO (b) fluor an thoDe ND llg/L
Beom (i,h,i) pcryleoe ND
Benzo (k) fluorulheno ND I llg./L
ugiL
Cbryteoe ND ug/L
Dibeoz (a.h) 11\thrac:eoe ND
FIIIOrlllllbeno ND
Fl~ ND
ll&iL
llg/L
llg/L I
Indmlo (1,1,3.00) pytme ND ug/L
Nipbthalene ND
PbCDaDthreoe ND
PyreDe ND
ug!L
ug!L
ug/L I
I Surr: J-Chlorooclarkcane (40-UO'X) .S8"
Surr: o-Terplrerryl (40-UO"J .90"
Sri": 2-BromonophthtJ/entl (40-UO"} 117"
Surr: 2-Fiworoblpltt~t~yl (40-Ut:IX) 117H
I
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3.00 01/17/08 16:22 MADBPVPH 8012728
1.00 01/17101 16:22 MADEPVPH 8012728
3.00 01111m 16:22 MADEPVPH 1012728
1.00 01/17108 16:22 MADBPVPR 1012721
4.00 01117/08 16:22 MADEPVPH 1012728
2.00 01/17/08 16:22 MADEPVPH B01272B
.s.oo 01117108 16:22 MADBPVPH 8012728
100 01/17101 16:22 MADBPVPH 8011728
100 01117/0B 16:22 MADEPVPH &01212!
tOO 01117/08 16:22 MADBPVPH 8012728
100 01/17108 16:22 MADEPVPH 8012728
lOO 01117108 16:22 MADBPVPH 8012728
01117108 16:21 MADEP f'PH 8011718
01117108 16:12 MADEP f'PH 8012728
100 01117/08 04:18 MADBPEPH 8012165
100 011l7/08 ~:18 MADBPBPH 8012165
100 01117101 04:18 MADEPEPH 8012165
100 01117101 04:45 MADEPEPH 8012165
10.0 01/17108 04:45 MADEPEPH 8012165
10.0 01/17108 04:45 MADBPBPH 8012165
10.0 01117108 04:45 MADEPBPH 8012165
\0.0 01/17/0B 04:45 MADBPBPH 8012165
10.0 01117/08 04:4~ MADBPEPH 8012165
10.0 01117/08 04:45 MADBPBPH 8012165
10.0 01117/08 04:45 MADEPBPH 8012165
10.0 Olll7108 04:4S MADE'PBPH 8012165
10.0 0!117108 04:4S MADEPBPH 8012165
10.0 01117/08 04:45 MADEPEPH 801216S
10.0 01/17/0B 04:4S MADBPBPH 801216.5
10.0 01117108 04:45 MADBPBPH 8012165
10.0 01/17/08 04:45 MADEPEPH 8012165
10.0 Ol/l7/0B 04:4S MADEPRPH 8012165
10.0 01/17108 04:45 MADEPBPH 8012165
10.0 01117/0B 04:4S MADBP BPH 8012165
10.0 01117/08 04:45 MADRPEPH 8012165
01117108 04:18 MADEPEPH 8011161
01/17108 04:4! MADEPEPH 8012/6J
0//17/08 04:45 MA.DEPEPH 8012/6J
01117/rM 04:45 JMDEPEPH 8012165
Page 10 of 19
~.[f3'sf~~-e~i·®·®·:·:~ ~;~.:, .... ~:-.... _ .. .,, ...... f .. : 3.J·f·~·-.. .:h. ·rr! : .. , ... _.:;, ___ .t; ~;·. . •. ~ ...... ~o;i
.. · :. ·•,•._,,,•f.•·•,.:. ... ••l:"V.U",:•:t'(.'•,!' o •,:,~'4f4•'.'-•:'• "'\•·,.~.-.•t'·:,.• tl '._:, ,,•,: •.i.:~ , :.n:t.E: LEAD~JN' E~VlRQN.~~~T,,&.l'T,!!~TI~Cl -:·;
Client Air Water&; Soil Uboratoria (7091)
2109 N. HamillaD Stree1
Richmond, VA 23230
AnD AWSPM
Wod: Order. NRA 1168
Project Name: NC 'T'rust Worlt
Project Number: 08010146
Received: 0 l/l2108 08:05
SAMPLE EXTRACTION DATA
WIIVol l!Racdon
~~~ ...••.•••••...................... ~~h .......... ~~!':~~ ......... ~~ ..... ~~~'Y_o_l •........••.. ~ •.•••••... ~~---~··········
MADBPE.PH
MADI!PBPH
MADEPBPH
MADEPI!PH
MADI!Pl!PR
MADBPBPH
MADBPBPH
MADI!P EPH
MADBPEPH
MADEPVPH
MADBPVPH
MADBPVPH
MADE7VPH
MADEPVPH
MADEPVPH
MADEPVPH
MADEPVPH
MADEPVPH
MADID' VPH
MADl!PVPH
MADl!PVPH
8012\6S
801216S
801216S
8012165
8012165
8012165
801216S
1012165
8012.511
801lSl2
1012721
8012721
101272&
1012721
1011721
8013000
lllllT.ll
8013000
8012728
NRA116Ul
NRAI168.02
NJtAII68.0l
NRA1168-o4
NRA1161-0.S
NRA1168-o7
NRAII68.08
NRA1168-09
NRA1161-01
NRA 1168.()2
NR.A1\68.03
NR.Al161-04
Nll.AI16J-oS
NRAII68-o6
NRA 1168.()7
NRAI 161-07RB1
NRA 11611.011
NRA! 168.08RB1
NRAI16U9
975.00
9SO.OO
960.00
92.S,OO
550.00
1000.00
1000.00
1000.00
HlO
s.oo
s.oo
s.oo
.s.oo
5.00
.s.oo
5.00
5.00
.s.oo
s.oo
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
5.00
5.00
.s.oo
.s.oo
.s.oo
.s.oo
.s.oo
.s.oo
s.oo
s.oo
s.oo
01/1~8 l3:25
01/U/01 13:25
01/1 SlOB 13:25
01/!~ 13:2S
OIIIS.U 13:25
0111~ 13:25
01/ISIOI 13:2S
0\/15108 13:25
OIAmOI 15:30
OlmiOS 14:50
01109/08 I 4:l0
OltW.118 14;4S
OIA19101 14:25
OIJ09JDI 14:00
01109A11 ll:JS
01109108 13 :3.S
01109101 13:20
Ol/09m 13:20
01~ \~:SO
MSR MADl!P
MSR MAJ>EP
MSil MAOEP
MSR MAJ>EP
MSil MAJ>I!P
MSR MADBP
MSR MADBP
MSR MADI!P
KOM MADEP
KOM MADS.P
KOM MADEP
JCOM MADBP
KOM WADEP
KOM MADI!.P
KOM MADEP
K.OM MADBP
lCOM MADBP
KOM MAJ>EP
KOM MADI!P
Page ll of 19
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~~Sf~ii~fi~i§i'
t::.1j.ji!':~eAil,'fir(·;~;~f./V·I~o~¥eNjAL~T.Ii~JNa~ .•
Client Air Water & Soil Llbotatorics (7091)
2109 N. Hamilton Street
Richmond, VA23230
AIID AWSPM
Work Order:
l'roject Name:
Project Number:
bceived:
PROJECT QUALITY CONTROL DATA
Blank
Allalyta BLink Value Q Unill Q.C. Balch
NllAll68
NCTrustWodt
080\0I-46
01/12108 08:0S
LlbN11111bc:r Allalymf Dallll'lilllo .......................................................................................................................................................................................................................
MADEPVPB
8012522-8LK1
8IIIIZIU& q)_6i0 uaiL 8012522 10l2522·BLKI 01116/08 12:14
ToiiUIU <0.600 uWL 8012522 IOI:z.522·BUC1 01116/D8 12:14
Ethyl~ q)_-46() UWL IOI:z.5ll 1012522-BI.KI 01116108 12:14
m,p--Xylt:oa <O.WO ISJIL 1012.522 1012SD-BLK1 01/16/01 12:14
o-Xylcao <0.1l0 UWL 1012.522 10 12S22-BJJC.I 01/16/DI 12:14
Napblbllcao 3.66 uaiL 10\lm 1012522-8UI Ol/16/01 12:14
cs-ca Allpbatic ~ .. Uudjulte• <50.0 uaJL 8011522 80l:z.522·8UCI 01fl6/0I 12:14
C9 • Cll Aliphatic HydnK-.Irlloaa, Ullllijlllll ~0.0 aWL 1012522 I0\2522·BUI 01116101 12:14
0 • Cl Alipbal:ic BydrocllltloDI ~0.0 uaJL 10\lm 1012522-BU1 . 01/IMlll 12:14
C9 -Cl2 ~ Hydroc:utJaao <50.0 ~aiL 1012m 1012S22·Btx.l 01116101 U:t4
C9 • C\0 Alomlric ~ <50.0 Da/L 1012522 10 1.2S22-BU I 011115101 12:14
S~: J,S·DI~"• (FJD) 97% 8012S22 1012522-BUC.J 01/16/08 12:14
~ta: J,S.J>Ibi'OflttW!w,. (PID) 101% 11012522 IOI:z.522-8LKl 01/16108 12:14
8D1272B-BLK1
Wcdly\ll:rt·Buryl Rlbcr qj_JIIO ~ 8012711 10 1212&-B LX. I 01/17101 II :32
ilcul:lle q),610 ua/L 11012711 10ll7llr-BLKI 01117/011 11:32
Tolualo q),60() ua/L 1012721 10 12721-BU I 01/17108 11:32
Ethyl~ cn.460 Ua/L 8012728 1012718-BUCl 01117108 ll:lJ
m.p-Xytuo <n.WO uw'L 110127111 8012128-BLKl 01117108 11:32
o-Xylello <0.710 uaJL 8012728 8012728-BLK.l 01/17/08 II :32
NapbtbiiiiM <1.6' uafL 8012128 &012728-BUU 01117108 lt:l2
CS -CB Alipbatio Hydtocazboat, UIIICljutlll ~0.0 ISJIL 8012721 10 127l8-BLK.I 01/11108 II :32
C9 • C12 Alipllliic B~ Ullldjull• 1S.S • 1012721 10l2'72t-81.Kl 01117108 11:32
cs -Cl Alipbltie Hydroelrbot!l <SO.O qiL 101272i 101212&-BIJ(.I 01117108 11:32
C9 -C\2 Atlpbali~ H~ 69.4 IIIIL 101212ll 10 12728-BLX.I Ol/17ml 11:32
C9 -C 10 Atom81i~ tfydrowbooa <SO.O uc'L 8012721 &012728-BLK1 01117108 11:32
Sliwr>Ff•: J,J.I>ar-lolwlt• (FID) 106% 8012721 8012728-BLKI 01/17/08 II :32
Stnotpt•: 1,~oiN-(PJD) 107% 8012728 8012728-BLKI 01117108 11:32
8013DOO-BLK1
Mclbylam-BIItyi l!lbet qJ,liO • IOilOOO 1013000-IILK1 01/IIWI 10;19
Bcazmo <0.610 uafL 1013000 10\lOOO-BLKI 01111101 10:19
Toluale q),60() uaiL 8013000 10 I l OQO.BLK.1 01118108 10:19
l!lb:ylbcuellc 0.524 uaJL 8013000 &0 13000-BLK.I 01118108 10:19
m,p-XyleQI: q),840 IIIIL 8013000 8013000-BLK1 01118101 10:19
o-Xyleu <0.710 IIIIL 8013000 8013000-BLKI Ql/181011 I 0:19
NapbllllolCM <1.65 aaiL 8013000 1013000-BLKJ 01118101 10:19
cs. ca Alipbltit: :H~ Ua&Aii~~~~tt <j()_Q 1111'-1013000 IO!JOOO-BLKI Ollll/08 10:19
C9-C1l Alipbatic H)'drocarbo111, UJIIIIti~:P 61.\ uaiL IIOUOOO 80 13()()().BLX.l 01118108 10:19
CS • C& Aliphatic Hydroccbo111 ~o.o ulfl 1013000 1013000-BLIC.l 01/1 8/0a I 0:19
C9 • Cll Alipbatic Hydrocarlloot $4.0 ulfl IIOIJOOO 1!0\3000-BLKI 01/1111111 10:19
P~~&e 12 of 19
C1ieot Arr Wiler & Soil Ltbol'ltorics (709 I)
2109 N. Hamilcon Street
R.icbmoud, VA 23230
A tiD AWSPM
BlankVe!ue
MADEPVPH
8013000-BLK1
C9 • C10 Al'ollladc Hydrcxvboa1
S111T0ifll•: J,J-Dibromotolwro• (FID)
SumJ,ate: J,J-Dibromotolwro• (PID)
MADEPEPH
8012165-BLK1
C9 • Cll Aliphatic Hydlocalbolll
Cl9 • C36 AliphodcH~
Cll • C22 Aramallc: HydmcMbo..., Ualdja
2-M.chylolpbc.leiiC
Accuphtlw:Da
Acel>apllthybe
Alllllrlccoll
~(a)PI~CI
Baazo(a) l')"''aaii
BC!Im (b) llu011111111"""
BCIIm W.,i) payleae
BciiZO (lc) fl~~~:n~~lhene
OuyweDa
Dibc:Dz (a,h) lll!tlncene
Fluonoatht.t>D
FluotCIIO
IDdeno ( 1 ,2,3-cd) pyrcno
NaphtbalCilO
Pblltllmdueae
~
StlmtFifl: /-C1r/OtOOt:tacf«tzNN
Surnlpht: o-T~
&.m>pe: l-BromtNitlpirtlw.to.e
~: J-F1.-oblpMzull
<SO.O
104%
104%
<29.0
<SO.O
<80.0
<1.40
<1.20
<1.20
<1.00
<1.00
<1.00
<1.00
<1.00
<1.10
<1.00
<1.20
<1.00
<1.00
<1.110
<1.)0
<1.00
<1.00
6S%
90%
\\9%
!21%
21N10 Foar CleVhlon Ro.d NNhvtlla, TN 37204' 110().78~80 • Fu 815-721-3404
Worlc Order.
Project N~me:
Projcc:t Number.
lU!ceived:
PROJECT QUALITY CONTROL DATA
Blank • Coat.
Q
us/L
us/L
u&IL
1IW'L
1IW'L
ua/t.
UWL
1IW'L
qll.
qll.
uaJL
uaiL
uaiL
llg/L
llg/L
ugll.
lla/L
uciL
uJIL
uaJL
lli/L
Q.C. Batch
8013000
8013000
1013000
&012165
S01l16S
8012165
1012165
1012165
1011165
1012165
801116J
10!1165
1012165
8012165
1012165
801216.5
8012163
101216J
801li6J
101216.5
IOillfiJ
101216J
1012\fiJ
80\2165
8012163
801216.5
101216.5
NRAII6ll
NC Trust Wotlt
08010146
01/12108 08:0S
LUNumbcr
8013QOO.But I
IOIJOOO.BLKI
8013000-BU:I
IOI216S-BLKI
ID1li65-BLK1
101l16S-BLK1
IOll16S-BU:1
101216S-BLX.I
1012165-BUI
1012165-BLKI
101216J·BLK1
1011165-BLltl
101216~-BLltl
I01l165-BLX.1
801216.5-BUCI
101216S-BLlt1
101216.5-DI...KI
8012165-BLX.I
1012165-BLX.l
101li6S-BLX.l
80\llfiJ-BLX.l
801116S-BUC.I
10lll6S-BUC.1
1011165-BUU
1012 U5.5-But.1
101216.5-BLK.\
8012165-BLKI
01/IIWS 1();19
01/1(1/08 10:19
011111101 10:19
01(16.'08 11:47
01116108 17:47
01116108 18:14
01116.'08 11:1~
01116.'08 18:14
01116108 11;14
011115108 18;14
01/115108 18:14
011115108 18:14
01/16108 18;14
01116108 18:14
Olfl6m8 18:14
01116m8 18:14
0111&'01 18;14
01/1&'01 18:14
01/115108 18:14
01116108 18:14
Ol/16108 18:14
01116108 18:14
01116108 18;14
01116101 17:47
01116108 18:14
01/16108 18:14
0111&'01 18:14
Page 13 of 19
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Client Air Water .t. Soil Laboratories (7091)
2109 N. Hamilton Street
l.licbmood, VA 23230
AWSPM
MADEPVPB
8012522·881
Melby\ lei1-Butyl i!lhct
Bmzt~~e
t'a!UCM
Bthylbe-
m,p-Xy\cmo
o-Xylcus
N~pbdllleae
C5 • CB Allpbltlc Hyc~Jncarbou. U~
C9 • C1liJ~ H~. UDidjlllllld
C9-CIO A.rollllll!c: Hy~
Surrop/1!: 2,S-D/bromo/DJwtNt (FID)
SUrropte: 2,J-D/browtotoinM (PID)
8012728·891
Melbyl!crt·Butyll!lber
~
Tolueaa
Bthylllea:leoe
m,p-Xyteao
o-Xyleae
Napblhal-
C5 • CS Alipbado Hydrocalbcal, Uudj uated
C9 • C12 Al!plwic H~ Ull&djuahld
C9 ·CUI Aroaa1ic Hydroc:utlotll
Swropte: 2.J.D1"'-Il>lwn' (1'1D)
Srm-optt: 2.5-Dibronlo/o/wnc (PJD)
8013000-881
Matllyltmt-Buty! Edler
Bcmllle
Tal~
l!lbylbcazl:ao
m,p-XyleDa
o-Xy!oao
N~pb121&lcaG
C5 • ca Aliphatic Hydtocarboat. u.....vua11ld
C9 • C12 Allpbatlo Hydrocabolla, Ull.ldjusted
C9 • CIO Ammalio Hydrowilon.
~ ..... 2.J..Dl"'-tDiua!• (FJD)
Sufrolt*: 2.5-DI,_~ (PID)
MADEPEPH
so.o
~0
5M
so.o
100
50.0
$0.0
I~
100
so.o
360
360
so.o
so.o
so.o
.so.o
)00
so.o
so.o
uo
100
50.0
40.0
4C.O
50.0
so.o
.so.o
.so.o
100
5a.o
so.o
uo
100
so.o
40.0
40.0
Worlt Order:
Project Name:
Project Numher:
Recoived:
PROJECT QUALITY CONTROL DATA
LCS
Q
57.1
52.7
S4.0
.53.8
Ill
.53 . .5
47.4
167
93.7
.54.7
344
34.5
S3.2
5J.J
S3.6
S.5.0
l12
53.2
50.2
177
80.1
52.7
40.7
41.3
Sl..2
Sl.l
54.1
5.5.6
112
53.4
41.l
176
79.6
.52.9
40.5
4l.S
NRAI168
NC Trust Wor\:
08010146
01112108 OS: OS
114%
10.5%
108%
101%
112%
107%
9.5%
!ILK
94%
109%
96%
96%
106%
107%
107%
110'14
112%
106%
100% II"'
10'14
IDS%
102%
103%
104%
101%
108%
Ill%
112%
107%
96%
Ill%
10'14
106%
101%
104%
Tqol
Rlllp
70· !30
7(J. llO
7(J. uo
70·1l0
70· 130
70· 130
70 -130
70-1]0
70-130
70-130
70·130
70·130
70-llO
70. 130
7(J. 130
70·130
70·130
70·1l0
70·130
70·130
70-130
70-llO
70 ·llO
70-130
70-130
70·130
70·130
70·130
70 • llO
70· no
70-130
70-130
70 ·130
70-130
70-130
70-llO
80!15l2 01/1&'08 \l :35
11112522 01116108 I 1:35
10ll5l2 01116108 11 :3 s
1012$22 01116108 11 :JS
1012.5l2 01116108 11:3S
8012.522 01/1&(18 11:35
1011522 01116108 11:35
80115:l2 01/16101 11:35
8011522 01116108 11:35
8012Sl2 0111&08 II:U
8012Sl2 01116108 u:n
8012S2l 0111&08 11:35
1012721 Oil! Ml8 ~:04
BOil'T.U 01/18108 09:04
8012128 0 Ill &108 09:04
1012728 0 ill &lOS 09:04
10127ll 0111 1.'08 1»:04
8011728 0111&108 09:04
1012728 01118108 09:04
8012721 Olll!WC 09:04
80127ll Olfl 1.'01 09:04
11112721 01/11101 09:04
1012728 01/18108 09;04
1012728 0111&'01 09:04
1013000 0111~ 01:31
IOilOOO 01/19101 01:31
8013000 0111~ 08:31
8013000 01119108 08:31
8013000 Olll9i08 08:31
1013000 01119.'08 01:31
1013000 0111~ 01:31
IOJJOOO 01119108 08:31
8013000 01119J08 08:31
8013000 0111~ 08:31
1013000 01(19108 01:3 I
1013000 01/\9101 01:31
Pqe 14of19
Client Air W.u:r & SoU Laboratories (7091)
2109 N. Hamilton S~
Richmond, VA 23230
Attn AWS PM
MADEPEPH
8012165-881
C9 -CUI Alipbalie K~
Cl9-C36 Aliphatic HydnK:cbaal
Cll -Cl2 Ato~ Hydrocamoaa, Uudj&atcc
2-Me1iryllllpblhlllcuo
Aceaapbtbcuo
Acc.phthylalc
Al1lllra=lo
BIIIIZD (a) llll.thrueno
Ileum <•> ,.._
Beao (t>) lluoruMhene
Belwl ( .. b,Jl pcrylcoc
SciWI (k) flUClftiiiKu
o,_.
Dlbem (a.b) aJilbncc:ue
Fh11xmtbaul
Pluom~e
lDdo:Do ( 1.2.3 .fXI) pyre~~~~
Napht!We~U:~
Pbeuotbmla
Pytao
$l/rtJJFia: J.CJ.tl1rOOC/4tJa:an•
Sllrroplc: o-Tupltmyl
Sllrropltt: 1-Bromor~QP~rrltal•n•
Sltrroptt.: 1-l'luo~~
KnoWII Val.
150
200
4ll
25.0
25.0
25.0
25.0
2S.O
25.0
25.0
25.0
25.0
2S.O
lS.O
25.0
25.0
25.0
2S.O
25.0
25.0
40.0
40.0
40.0
40.0
28110 F_. C'nlghiDn Ro.l NUIMie. TN 37204 ' 800-711!Hlll80 " Fu 615-7~04
Worke>roer.
Pro.i«t Name:
Project NUIIIber:
Received:
NRA1168
NC Trust Wotk
08010146
01112108 08:05
PROJECT QUALITY CONTROL DATA
LCS-Coat.
Allalyud Val Q UDill
141 uaiL 99%
200 Ua/L 100%
392 Ua/L 92%
27.3 uWL 109%
26.3 ua/1.. IDS%
26.1 ua/1.. 107%
l3.S Ua/L 9"%
21.3 ~&11-IS'Mo
IIL6 ua/1. 74%
18.7 Ull'l-7S14
11.7 uw'l 7$%
20.1 ,..,. 1111'1'
22.1 llliL 8814
lB.? u&ll-75%
14.() qlt. 96%
25.8 ua/1. 10314
18.1 uii/L 71%
16.2 UWL 10514
lSJ UWL IOI'Mo
23.8 ua1L 9S%
27.9 70%
37.3 93%
49.6 11414
49J 123%
<40-1<40 8011165 01116108 18:42
40-140 801:1165 01/16101 18:42
40. I <CO 8012165 OIIIIWI 19:09
~-1<$0 8ll1216S 01/16108 19:09
<40-140 8012165 01/16108 19:09
<CO. 140 801216S Olf16A)8 19:09
<CO ·140 1012165 01/IIWII 19:09
44-144 8012165 01111001 19:09
40-140 8012165 OllliWII 19:09
40· 140 101216S 0111~ 19:09
-40-I <CO 11Jili6S 01116101 19:09
40·140 801216S Oln~ 19:09
-40-140 8012165 Gl/1&ol:lll 19:09
-40-140 8012165 01/16101 19:09
<CO-140 IQI216S OJIIIWI 19:09
-40-140 1012165 01/16108 19:09
44-140 84)12165 01116108 19:09
40 -1<40 8012165 0111&o8 19:09
40. l<lO 11012165 01116108 19;09
40-140 8012165 01/16108 19;09
40-140 8012165 01116/08 18:42
40-140 8012165 01/16.()8 19:09
40·140 8012165 01/16108 19:09
40·140 8012165 01116108 19:09
Page IS of19
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CtieDt Air Wiler & Soill.abormories (7091)
2109 N. HamUIDn Stteet
Richmond. VA 23230
Atm · AWSPM
Work Order.
Projcc:t N~:
Project Number.
R.eceived:
PROJECT QUALITY CONTROL DATA
LCSDup
NRA1168
NC Trust Work
08010146
01/12/08 08:05
Splko Tap Simple I =~~-~~. ·-......... -..... -.---~~--~~:-. -~~~~-----~.------~~~~-.. --~~~-~~~--. ~~~-. _RP_~. ~~~~-... -~~---.-. -~~p·Jl-~~~-.• --. ~~ .. .
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8012622-8$01
Methyl tert-l!utyl Ether
Bcru:t:llt:
Toi-
Bthylbcaaot
t~~,p-:X.ylc:no
o-:X.ylcac
C9-CIO~oH~
Swro,atl: l,J-Dt~t#lwlll (117D)
~ l,J.Dl,._~. (PJD)
801272S..BSD1
Mctbyltert-Butyl Edler
Bcllmle
Tal\11:110
l!tbylbcazcqo
ID,p-Xyl~:~~e
o-Xylcno
NapbtUICIIO
C5 • C8 Allpballc Hy~, UllllijllltZd
C9 -Cll Alipbatio Hyd~. Ullllijumd
C9 • C I 0 Aromll:ic: H)ld:>:QQ&toao.
~: l ,J.Dlbra.«IH-(FID)
Srmvplc; 1,J-Dib1'0111Dt0tw... (PJD)
8013000-SSD1
Melby! tat-Bury! Rdlcr
l!elmuo
Tol11110o
Elbytbo:lm:De
na,p-:X.ylcqo
o-Xylcoo
N.,.ldb.Jc:oc
CS-C8 Alipbat!c H~ Uaad,jlllltd
C9 - C 12 Alipbei!Q tlydrocNboaa, UM<!J11Stcc:!
C9-CIO Anii!Wic Hydroc:altlaaa
~: 2.J.Dibn.tuolucltl (FID)
&n-roaar-: 1,5-DIIn-oPiotolwM (PID)
MADEPEPH
n.J
~ 1.7
52.1
Sl.l
109
.52.0
36.9
1.52
10.6
S3.0
286
l06
S3.1
H..5
l6.0
.57J
II!
l5.1
.52.9
173
12.7
S4.1
4l.l
43.0
.53.1
SlJ
53.6
55.0
Ill
53.2
50.2
117
80.1
Sl.7
40.7
41J
l4.D
JO.O
l4.D
50.0
100
50.0
JO.O
Jj()
100
~
360
J60
58.0
.50.0
.50.0
.50.0
100
50.0
50.0
uo
100
.50.0
40.0
-40.0
50.0
.50.0
5().0
50.0
100
.50.0
50.0
Jj()
lCO
50.0
~
-41LG
116% 70 ·130
103% 70-130
106% 70-130
104% 70. 130
109% 70-llO
104% 70 • 130
14% 70 • llO
101% 70-130
II% 70-130
106% ?a-tlO
711% 70-llO
B.S% 70 ·llO
1
l
2
3
3
3
2S
9
IS
l
106% 70. 130 0.1
Ill~ 70 -130 4
1\2% 70. 130 "
liS% 70-130 "
11.5% 10 • llO 3
110% 70. 130 4
106% 70-uo s
lU% 70·130 l
13% 70-130 3
ItO% 7a -130 4
107% 70-130
JOB% 70-130
106% 70-130 2
107% 70-130 1
101% 70-\30 0.9
110% 70-130
112% 70. 130 0.3
106% 10-no o.l
100% 70-130 4
1111% 70· 130 0.4
10% 70. 130 0.7
10,% 70-\30 0.4
102% 70-130
1 Ol% 70 • llO
2j
2S
2S
2S
2S
lS
2S
2S
2.5
2S
2.5
2S
2S
2S
2S
2S
2S
lS
lS
2S
2S
2S
2S
2S
lS
2S
25
l-'
lS
2S
1012SD
IOilSll
1012S'll
IOilSll
1012.522
8012522
80l2Sl2
101:1-'22
8012Sll
1012Sll
1011nl
8012522
1012'n8
1012nl
1011711
10127l8
1012711
8012728
1012721
1012721
1012111
101.2121
1012:711
I0\2'nl
8013000
8013000
1013000
1013000
1013000
1013000
8013000
1013000
1013000
1013000
1013000
10\lOOO
01 n7..0S 07:22
01/17A:J8 07:22
01117Alll 07:22
01117.-ol 07:22
0 1117..0S 07:22
Ol/17ml 07:22
OJ/17ml 07:22
01117108 07:22
OI/1711J8 07:22
01117/118 0'1 :22
01/\7,\)1 07:22
01/17~8 07:22
01117ml 10:19
01117/08 10:19
01117/ll8 10:19
01117~1 10:19
01117.111 10:19
01117,\)1 10:19
Olll7mB 10:19
Ol/17ml 10:19
Ol/17/ll8 10:19
01117JOI 10:19
0\117-01 10:19
01117~8 10:19
01/IR/08 09;04
0111\WB 09;04
0111 !WI 09;04
01118101 09:04
0111 R/08 09:04
01/lR/01 OM4
0111\WS 09:04
01/IRIOI 09:04
01/IRIOI 09:04
01/U/01 09:04
01/18108 09:04
0 I II 8101 09:04
Pqel6ofl9
~xesta·~.9~i ~:~#(i 1t.i.~··'~;., ~·''''· ,,• · .. ~. ':·1~:"·!~'•-o~··~j.r•, .:A·~. ~;~ •... ·~~:, .. l~~j~;~;i~:·:~ .,.. ' :1?:·.·~•:-·.•·~·;; ... .-,.~:·""~~· -~ .. :-. :~r·r" •.. ;:, : .. -:..: :·"!l' :.~ .~:,~ ' ~ .. ·~~!":' ,, ·t~·l·:"· ::-~:. :...:.:~ g'.~.~e: .. '-:~~g~:t~.;.~t:f~l.~q_~~~.N.'t~~,TE~n~q~~
Oient AitWmr& Soil Laboratories (7091)
1109 N. Hamilton Street
Richmond, VA 23230
A tiD AWSPM
NRAll6B
Project Name: NC TIU!It Work
Project Number: 08010146
~i~ 01/12.108 08:05
PROJECT QUALITY CONTROL DATA
LCS Dup -Cout.
Spike TatJct
Q OlDe % 11m. Raq8 RPO l..bnit
8012165-8801
C9 • C18 AlJpha.t!c Hydrocaboas 147 u&fL ISO 98% 40 ·140 0.8 l5
C19 • C36 Aliphadc Hydroc:arboot 19<1 uw'L :KIO 97% <40-140 3 25
Cil • C2l Aromatic Hydrocarboot. Unadjuato :m uw'L <111 88% 40 -140 " .25
2-Mctbylupblhalcae 27.0 uw'L uo 108% 40 -140 .25
AccDipltthao 2.5.9 Ua/L 11.0 104% 40·140 2.5
Aellllphthylocw 26.4 Ui/L 1S.II 106% :40· 140 I .25
Alttlnlli:ZIII 22.4 llf'L 11.G 90% 40 -140 .s .25
Bmm (&) llllllhncaoc IU Ui/L 25.0 19% 40-140 7 2.5
.BeDm (a) pynme 17.S Ua/L n.o ~ .a-140 6 2.5
Bmzo (b) flaanllthalo 17.6 llf'L u.o 70% 40-140 6 2.5
Bazo (J.h.l) pory\eDo 17.4 UWL l$.0 69% 40 ·140 8 25
. Bam (k) ftiiOIUillcDo 11.7 UWL 11.0 75% 40 ·140 1 2.5
<lily.-20.9 uWL 1S.II 83% 40 -1<40 6 2.5
Dibeu (&,b) '-'!lhPco:Pa 17.! u&IL UG 70% 40 -140 7 2S
Fluooa~ 22.6 u&IL 2U 90% 40 -140 6 .25
ftuoraM 2S.I u&IL 11.0 100% 40 ·140 3 1S
lPdo=Do (J,l.J-cd) pyn!Dt: IU u&fL 2l.O 66% 40 -140 9 lS
Nopblbalcnc 26.2 uWL 1.!.0 IDS% 40 -140 D.2 1S
PbcDaatbn:uc 24.1 uJIL 1.!.0 96% 40 -140 s 2S
Pyrcae 22.4 Ua/L 2J.O 90% 40 -1<40 6 .25
Sluropr.; J.CJt/orooctodet:tlnc 24.5 a&fL 40.8 61% 40 -140
~·I).~ lU 11&/L 40.0 90% 40 -140
~'' 1-BrtNrJolltlplrtlt<llm. 47.8 ur/1. 40.0 120% 40 ·140
Swrofr*.·1-F7NOroblpiJenyl 47.4 ur/1. 40.0 !19% 40 .140
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8012165 01/16/08 19:37
8012\65 01116/08 19:37
8012J&s 01/16/08 20:04 I
8012165 01/16/08 ::!0:04
1012165 01/1{.'08 20:04
1012l&s 0111&'01 20:04
1012165 0111 &08 20:04 I
101216S 0111&08 20;04
toJ2J&s 01116/08 20:04
11012165 01/16108 20:04 I
8012165 01116108 20:04
10121&s 01116108 20:04
1012165 01116/08 2():04
801216.5 01116108 2.0:04 I
1012165 01116108 ~:04
8012165 01116/08 20:04
801216.5 ouJMJa 20:04 I 10121&s 01116/0a 20:04
8012165 01116108 20:04
801li6S 01/IMll 20:04
1012165 01116/01 19-.37 I
10l216S OIIIM>a 20:04
8012163 01116/01 20:04
80121&s 01116/0a 20:04 I
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Page 17 of 19
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il.~sf~'iil~~rti·•~1!l~~ ~'{; ..... ~~\ ... , ·:····~ .. ~-,:::'~ ••• 1' .. .!! .. :"·;·::.. ,., .. f::·; .•. • .~··:. ~;~~'" '.: .. :····:_ .... ·.1:.-, ... ,h::•
~~·1,'"'J.'O~~;H: ;.-:·;::.·; .. :.',"-•·•.';.;·.•.,··,;..·.,;._,.: ~--·.":'\' '1>·~'•1-.:·...,. ·...-•)• •• -,,,. ••• ··.r>l ~i·!l:t.~i~.~.!!R·~:.e~a.~b,~€tjt.i:L/!J~t•fi.(.l;·~
Cicot Air Water & Soil LaboratoriQ ('7091}
2l09 N. Hamilton Sucet
Richmood, VA 23230
Attn AWS PM
TestAmenta Na•llvtlle
MADEPBPH
MADBPVPH
Walc:r
Watu
Worlc Order:
Project N~~me:
ProjDct Number:
!Uiceived:
CERTlJ'ICA TION SUMMARY
N/A
N/A
Nclac
X
X
NRAII68
NC Trust Work
080101-46
o 1112103 oa:os
North CArolina
X
X
Page 18of19
29110 ~r Cr.~Qtllon Ro.d Nutwlle, TN 3720<1 • 800-71111-00110 • Fax 111~72&-3o4G4
Climt Air Water & Soil Labomories (7091)
21 09 N. Hamilton Street
Richmond, VA 23230
Attn AWSPM
Wodc On!= NRA 1168
Project N~.me: NC Trust Wad
Project Number. 08010146
Receiwd: 01112108 OB:ru
ND
DATA QUALIFIERS AND DEFINfllONS
Not detected at tho reporting limit (or method detection limit if shown)
METHOD MODIFICATION NOTES
Page 19 of 19
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Test America 111111111 lW£ LU.Oflt IN 04VIIIONiolliNTAI. Tl!lll~G
Nashville, TN COOLERRE NRA1168
Cooler RecalvediO~ ~ 0111212008 a 0805
1. Tracking f. __ l~ 'l_ ~~_2S ____ (Iaat4 digits, FedEx)
Courter. f!5Hil IR Gun ID 10142151
2. Temperature or rep. aampla or limp blank When opened:~ Cel.tua
3. If Item t2llmpwawre Ia o-c or 1 ... , wn the representative ample or t.mp blank frazan? VE8 N0 ••• 0
4. Were cUitOdyaeala on owl• of cooler? YES .. ~ ... NA
If yea, how many andwhere: _____ _.;_ ___________ JJ.;..;;....;A-...;._ __
6. Were the autalntact. algned, end datad COI"'WCIJy? YES .•• NO .. ~
6. Were cuatcdy pap.re ln8ldt cooler? ~ ... NO ... NA
I ctrtffy lf!pt I opened the cpo!tr and anJWttntd aunUoOJ1..§ f!ntla!) _________ _.n~..--~--
7. WeJW cuatody aeaJa on containers: YES ® and Intact YEa ... NO.~
Were th ... algMd and dat8d cofftdly? Vf8 ... No@'
8. Pecking mat"l Uled? ~ Plastic biG Peanuts Vermlcultt. Foam lnurt Paper Ottlw None
8. Coottng proc:esa; e lca.pack Ice (direct c:o!Dc:t) Dry lea Other None
10. Old aU contalnen an1ve In good condition (unbroken)? ~NO ... NA
11. Were all contalnerlobela complar-(1. dllta, algnad, prea.. etc)? ~.NO ••• NA
12. Did all container labela and tap l9fH with custody papere? ~O ... NA
Ua. We11 VOA vlall rec:elwd? ~NO ... NA
b. Was Ulere any obaervab,_ headlpeca pruant In any VOA vial? Y~.NA
14. W.. ttltre a Trip ar.nk In thla cooler? VES·:~ If multiple coolers, e~~quenca •-~-
1 rctr1tfv lttat 1 YOIQidod tht qpo!tr IQd anawtred guuttona 7-1411ntla!l It;)
115a. On prea'd bottlel, did pH tnt atrlps auvgMt ptMifV&tJon re~ehed the com~et pH IBWI? YE8 .• N~
b. Old the bollle tablla lndlcata that the comet preservatiWt were used ~NO ... NA
If preeervatlon ln-t.ouaa wu ~.record atandard ID Of p,..MVatlve uaed here. _____ _
10. W.. rwldual chlollne prMent? YES ••• N~
lcartify that 1 cbeckpd for chlgrtno and QH n per SOP 1nd ll!JWU'Id CI!JntfODJ 1 §.11 ltnth!O tJ25
17. Were custody pape,. properly filled out (Ink. elgned, etc)? @No ... NA
11. Did you algn the w.tody papereln the approprtate place? ~.NO ••• NA
1t. Were c:orNCt c:ordal.,.ra UNCI for the anatysla raq\l~Steei? @.NO ... NA
20. waa eufftclent amount of lllnple Hnt In each container? ~;.NO ... NA
I cuttrv tbtt 1 enttrtd tills pro!tct lntq blMS and antWtfld gyeaUona 1l-2Q llntla!l ciJj}J
I 'lftltv tbnt I gUachfd I ltbt! with tb• ynlqut UMS numbtr tq HCh contalntr llnVall t2
21. Were thwe Non.Confonnanc:e luu .. allogln? YES.~ a PtPE genaratad? ves@.t. __ _
BIS • Broken In shipment
Cooler Reulpt Ponn.doc LF·I
End of Form
R.cvi5cd 9/6107
-------------------~ NRA1168 W.I:ISOIL 01128108 2359
• INC.
CUENT ADDRESS: t
CLIENT PHONE NUMBER:
CLIENT FAX NUMBER: ""v
ls sample for compliance reporting? YES NO
SAMPLER NAME (PRINn:
!! Gl
IIJ E
0 I=
0. 0. .9 0 -(/) (/)
CLIENT SAMPLE 1.0. .s .$
iii ;;;
8. 0 0. E E 8 0 u
4) Cff:IJ\ () \.l\l tJ -ID4
10) /'~
\~-\-f\~-nca.._
\~~~Q
CHAIN OF CUSTODY
PROJECT NAME:
SITE NAME:
PROJECT NUMBER:
P.O. NUMBER:
REGULATORY AUTHORITY:
2109A NORTH HAMILTON STREET
RICHMOND, VIRGINIA 23230
(804) 3$8.8295 PHONE
(804)358-8Zt7 FAX
PAGE OF~
Is samj)le from a chlorinated su~? YES NO PWS 1.0. #:
-=:stQ .. \ 1_~
SAMPLER SIGNATURE: Tum Around Time: ~sJ
NO MATRIX ANALYS'S COMMENTS
Quotei.O.:
./ ./ Dl
../ ./ {.'1
D5
j
COOLER TEMP •c
l.e'llllll a
DATE I TIME I.JMit Ill 0
Laval IV 0 AWSCOC -
-------------------
Historical Groundwater Analytical Results
'h .Di-, 1',2-' . Ethyl-Totill Trichloro-<is-1,2-Tetrachloro-·
Location I Date .Bentene isopropyl benzeo~ • MTBE Tolutne Xylenes Dic~'oro-: ethylene Dichloroethylene · ~tbylene Lead (pg/L) I .. etber_ " (~) (JtgiL) etb~ne (mg/L)1 : (jlg/L), ' ; (j.1g/L) (~/L) '(~) ' (~L). (Ji~). " . ' . (J!I!IL) . -.
BDL5 I ------
09/03/93 . 13.5 ·NS4 ' BDL 3.69 i BDL BQL. BDL NS BDL NS
MW-1 .' 04!22/99 BDL BDL BDL 47,0 BPL, BDL ~DL BDL BDL NS 0.040
.!
09121/07 BDL BDL BDL 26.0 BDL BDL BDL BDL BDL BDL 0.004
. 04/22/93 BDL NS 3.0 BDL lLO TO 19.0 BDL NS BDL NS ..
. llf29195 1.5 NS .BDL 10.0 BDL BDL 8.7 BDL NS BDL NS
..
03/05/96 1.0 NS ;soL '1.2 BDL BDL 5.~ BDL NS BDL NS
MW-4 -
05/15/96 BDL NS BDL BDL BDL I;lDL 2.5 BDi _NS BDL ·NS
04/22/99 BDL 2.3 BDL 11.0 BDL
' BDL 6.1 BDL BDL NS 0.023 '
01/09/08 BDL BDL BDL 9.7 BDL BDL 3.2 BDL BDL 7.8 0.043
----- --.. --
01/21/94 24.0 NS 32.0 79.0 250 570 . 18.Q BD~ NS .BDL NS
" 11129/95 39.0 NS 16.0 96.0 : 2..0 24,0 3.8 Li NS 81.0 NS
03/05/96 BDL NS ' BDL 18.0 BDL BDL ·BDL -16.0 NS 1,500 NS
MW-5 -. .
05115196 ·BDL NS BDL BDL BDL BDL 90.0 34-0 NS 1,300 NS
04/22/99 . BDL 2.0 BDL 6.7 BbL BDL BDL 1.9.0 7 .. 9 · NS 0~051
01/09/08 BDL BDL BDL BDL BDL BDL BDL 3.3 6.8 28.5 0.236
01/05/95
MW-8
4.4 'NS BDL 260 'BDL BDL 30.0 45.0 NS 1,900 NS
01/09/08 BDL 16.0 BDL 776 BDL BDL BDL 465 40.1 4,680 0.003
-------------------
Historical Groundwater Analytical Results (Cont'd.)
" Di-'
; . Benzene .is9propyJ Ethyl-MTBE 'Toluene ~ .~
Location Date (~)' ,etber benzel)e (~L) (JLg!L). .; (~) (J12/L)· ~ ' : ;. ..
01/5/95 3.5 NS L1 1,500 LO
MW-9 ...
01/09/08 BDL BDL BDL 67.8 BDL
MW-10
04~2/99 po ·68.0 30.01 BDL BDL
01/09/08 13.0 52.4 4.2 76.3 BDL
04/22/99 9.0 66.6
MW-11
B'QL BDL BDL
01/09/08 2.0 8.0 9.5 BDL BDL
04122/99 B.DL BDL BDL BDL BDL I
MW-13 ..
01/09/08 BDL 48.4 BDL 489 BDL
, :ZI Groundwater i 0
~Quality-Standard r.o -io ..: 29 ~00 t®Ci : ·. . . {JJ.!/L} .. • 0
, Gross Contaminant :~.00() ' 70,~00 29.,0,00 2oo,ooq 257,500 ~. i Level (f.12/'L}
1 VOCs by U.S. EPA Methods 601 and 602 and/or 6210B,I"CJ))ned m m1crograms per ltter ijLg!L).
1 Lead by U.S. EPA method 7411, reported in milligrams per liter (mg!L).
J NA • 2L Groundwater Standards & Gross Contaminant Levels not provided.
• NS = Not analyzed.
'BDL .. Below Detection limit.
Boldtd ,·alues are those which exceed the 21. Groundwater Quality Standard.
1,2-Total Dfehloro-'{ricbloro-·
Xyle~es ethbe ethylene
(pg/~). (JlgiL) ; (Jlg/L) --
BDL 2~.0 100
BDL BDL 2,770
19.0 BDL BI;>L
BDL BDL BDL
.42.0 E,iDL BDL
BDL BDL BDL
BDL BDL BDL
BDL 2.7 18.7
530 0.38 2.8 .·
87,500 . 380 2,800
'· .. .
cjs-1,2-tetracbloro-· Lead Dichloroethyleoe etbylen~ (mg/L)-(~) (~L), ..
--
NS 5;200 N5-
1,130 44,200 0.013
NS NS 0.()09
BDL 1.5 0.010
. NS NS 0.018 ..
BDL BDL 0.015
..
NS NS 0.015
3.2 45.1 0.007
NA3 ·.0.7 '..;15
'' .. ..
NA· • ' .700 15,000 ..