Loading...
HomeMy WebLinkAboutMO-88905_96941_CA_UST-12_20230120Aboveground & Underground Storage Tank Closure Report D’Arrigo Property 901 Dr. Martin Luther King Jr. Way Gastonia, North Carolina 28054 Facility ID No. 00-0-0000047507 Prepared for: John D’Arrigo 901 Dr. Martin Luther King Jr. Way Gastonia, North Carolina 28054 January 20, 2023 Blue Ridge Project Number: 22-6232.1 Prepared by: Blue Ridge Environmental Services, Inc. 2315 Kings Rd. Extension Shelby, North Carolina 28152 (O) 704.482.2111 (F) 704.482.4335 BRESI@BlueRidge-ESI.com 2315 Kings Road Extension Shelby, North Carolina 28152 (O) 704.482.2111 (F) 704.482.4335 Email: BRESI@BlueRidge-ESI.com January 20, 2023 Mr. Brad Newton N.C. Department of Environmental Quality Underground Storage Tank Section 610 East Center Ave Suite 301 Mooresville, North Carolina 28115 RE: Aboveground & Underground Storage Tank Closure Report D’Arrigo Property 901 Dr. Martin Luther King Jr. Way Gastonia, Gaston County, North Carolina 28054 Facility I.D: 00-0-0000047507 Incident No. None Blue Ridge Project No. 22-6232.1 Dear Mr. Newton: Blue Ridge is pleased to submit the Aboveground & Underground Storage Tank Closure Report for the D’Arrigo Property Site. If you have any questions regarding our recommendations, please contact the undersigned at 704-482-2111 or KenP@BlueRidge-ESI.com. Sincerely, Blue Ridge Environmental Services, Inc. Kenneth A. Pimienta Senior Project Manager 2315 Kings Road Extension Shelby, North Carolina 28152 Phone: (704) 482-2111 Fax: (704) 482-4335 Email: BRESI@BlueRidge-ESI.com ABOVEGROUND & UNDERGROUND STORAGE TANK CLOSURE REPORT Blue Ridge Project No.: 22-6232.1 A. Site Information 1. Site Identification Date of Report: January 20, 2023 Site Risk: N/A Facility I.D: 00-0-0000047507 UST Incident Number: N/A Site Name: D’Arrigo Property (Site) Site Street Address: 901 Dr. Martin Luther King Jr. Way (Figure 1) City/Town: Gastonia Zip Code: 28054 County: Gaston Description of Geographical Data Point: UST Basin Location Method (GPS, topographical map, other): GPS Latitude: 35.276217 Longitude: -81.182291 2. Information about Contacts Associated with the Leaking UST System UST Owner: John D’Arrigo Tel: (704) 417-6788 Address: 901 Dr. Martin Luther King Jr. Way, Gastonia, NC 28054 Email: John@dcginc.us UST Operator: Unknown Tel: Not Applicable (N/A) Address: 901 Dr. Martin Luther King Jr. Way, Gastonia, NC 28054 Email: None Property Owner: D’Arrigo Construction Group INC. Tel: (724) 869-7117 Address: 901 Dr. Martin Luther King Jr. Way, Gastonia, NC 28054 Email: John@dcginc.us Consultant: Blue Ridge Environmental Services, Inc. Tel: (704) 482-2111 Address: 2315 Kings Rd. Ext., Shelby, NC 28152 Email: BRESI@BlueRidge-ESI.com Analytical Laboratory: Pace Analytical Services, LLC. State Certification No.: 329 Tel: (803) 791-9700 Address: 106 Vantage Point Drive, Columbia, SC 29172 AST/UST Closure Report January 20, 2023 D’Arrigo Property Page 2 Gastonia, North Carolina 28054 Blue Ridge Project No. 22-6232.1 3. Information about the Release Date Discovered: N/A Estimated Quantity of Release: N/A Cause of Release: N/A Source of Release (e.g., Dispenser/Piping/UST): N/A Sizes and Contents of Tanks or Other Containment from which the Release Occurred: N/A   4. Certification I, Cliff R. Lundgren, a Licensed Geologist for Blue Ridge Environmental Services, Inc., do certify that the information contained in this report is correct and accurate to the best of my knowledge. Cliff R. Lundgren, P.G. Senior Consultant/President Blue Ridge Environmental Services, Inc. is licensed to practice geology in North Carolina. The certification number of the company or corporation is: C-272 AST/UST Closure Report January 20, 2023 D’Arrigo Property Page 3 Gastonia, North Carolina 28054 Blue Ridge Project No. 22-6232.1 B. Executive Summary The former Underground Storage Tank (UST) and former Aboveground Storage Tank (AST) systems located at 901 Dr. Martin Luther King Jr. Way (Site) in Gastonia, NC were owned by Mr. John D’Arrigo. Mr. D’Arrigo never operated the USTs that were discovered at the Site or the former ASTs. Several onsite structures have been demolished and removed from the property and the Site currently contains a single story office building with an adjoining warehouse consisting of Gaston County Parcel ID 305893. The property borders are surrounded by a chain link fence in all directions. The AST system and all associated components were removed from the Site between June and August 2022. Blue Ridge personnel was not onsite during disassembly and removal of the ASTs. The former AST system consisted of five (5) approximately 20,000-gallon diesel steel ASTs and one (1) approximately 600,000-gallon heating oil steel AST. The UST system consisted of two (2) 550-gallon and one (1) 3,000-gallon heating oil USTs, located in three (3) individual tank basins. The USTs and ASTs are believed to have been installed circa 1975, which is the year the Site was constructed. Under the direct supervision of Blue Ridge, the three (3) USTs were excavated and removed from the Site on October 14, 2022 with very minor odor and no visual staining observe during the removal. Only the soils above and adjacent deemed necessary to remove the USTs were excavated during the tank removals. The final dimensions of the UST basins containing UST #1 and UST #2 each were 10 feet long X 8 feet wide X 6 feet deep, while the final dimension of UST #3 were 24 feet long x 8 feet wide x 7.5 feet deep. Please note that the copper product lines of UST #1 and UST #2 ran beneath the adjacent building, while UST #3 did not provide evidence of any product lines. The UST basin excavations were absent of odor or staining. The ASTs and USTs are believed to have been installed circa 1975, which is the year the Site was constructed. Upon removal, the USTs appeared to be in good condition with no holes, minor pitting or corrosion observed (see photos in Appendix A). No groundwater, bedrock or free product was encountered during the excavation of the UST system. Soil samples were collected within 2 feet beneath the bottom of the USTs and within 2 feet beneath the ground surface where the former ASTs once reside. Minor petroleum odors and minor staining was noted beneath and immediately surrounding the AST loading rack during the AST closure activities. As a precaution, the property owner requested the over-excavation and removal of the potentially petroleum impacted soils surrounding the AST loading rack. The over-excavation activities were conducted under the direct supervision of Blue Ridge on October 19, 2022. When no obvious evidence of potential contamination remained based on field observations/screening with a handheld photoionization detector (PID) for VOCs, the AST over-excavation activities were halted. One (1) bottom and four (4) sidewall confirmation soil samples were subsequently collected from the excavation area. The final dimensions of the AST over-excavation area were approximately 18’ long X 8’ wide X 7’ deep. Approximately 31.50 tons of potentially impacted AST/UST Closure Report January 20, 2023 D’Arrigo Property Page 4 Gastonia, North Carolina 28054 Blue Ridge Project No. 22-6232.1 soil immediately adjacent to the former AST loading rack were removed and transported to Environmental Soil Inc. of Lattimore, North Carolina for proper off-site disposal. Analysis from the seventeen (17) soil samples (SS-1 through SS-12, SW-1 through SW-4 and B-5) collected in association with the former AST system revealed detectable concentrations of TPH-DRO found to be present below the North Carolina Action Level for TPH-DRO of 100 mg/kg in fifteen (15) soil samples (SS-1 through SS-3, SS-6 through SS- 12, SW-1 through SW-4 and B-5) collected. Furthermore, a detectable concentration of TPH- GRO below the North Carolina Action Level of 50 mg/kg was reported in the soil sample collected from SS-8. No concentrations of TPH-DRO or TPH-GRO were reported in the soil samples collected from SS-4 and SS-5. No violations of the North Carolina Action Level for TPH-DRO and/or TPH -GRO were reported from the soil samples collected in association with AST #1 through AST #6. Analysis from three (3) (T-1, T-2 and T-3S) of the four (4) soil samples collected (T-1, T-2, T- 3N and T-3S) during the UST closure activities beneath the USTs, revealed detectable concentrations of TPH-DRO found to be present below the North Carolina Action Level for TPH-DRO. No concentrations of TPH-GRO were found to be present in the four (4) soil samples collected. No violations of the North Carolina Action Level for TPH-DRO and/or TPH -GRO were reported from the soil samples collected in association with UST #1 through UST #3. Based on the information obtained during the UST and AST closure activities, Blue Ridge recommends a “No Further Action” (NFA) status be assigned to the Site. This UST-12 Closure Report has been submitted to the North Carolina Department of Environmental Quality (NCDEQ) Mooresville Regional Office for review. AST/UST Closure Report January 20, 2023 D’Arrigo Property Page 5 Gastonia, North Carolina 28054 Blue Ridge Project No. 22-6232.1 C. Table of Contents A. Site Information ................................................................................................................... 1 1. Site Identification ............................................................................................................................. 1 2. Information about Contacts Associated with the Leaking UST System ............................................ 1 3. Information about the Release ......................................................................................................... 2 4. Certification ..................................................................................................................................... 2 B. Executive Summary ............................................................................................................ 3 C. Table of Contents ................................................................................................................ 5 D. Site History and Characterization ..................................................................................... 7 1. UST Owner/Operator Information ..................................................................................................... 7 2. UST/AST System and Other Release Information ............................................................................ 7 3. AST / Non-UST Spills and Release Information ................................................................................ 7 4. Release Information for Current UST Closure .................................................................................. 8 5. Site Characteristics ........................................................................................................................... 8 6. Summary of Assessment & Corrective Actions ................................................................................. 8 E. Closure Procedures ........................................................................................................... 9 1. Preparations for Closure ...................................................................................................... 9 2. Procedures for Closure ........................................................................................................ 9 3. Residual Material and Tank Disposal Handling .................................................................... 9 4. Soil Excavation Activities .................................................................................................... 10 F. Site Investigation ................................................................................................................... 11 1. Field Screening Information ............................................................................................... 11 2. Soil Sampling Information .................................................................................................. 12 3. Document groundwater and surface water information ...................................................... 12 4. Quality control measure information ................................................................................... 13 5. Soil and Groundwater Investigation Results ....................................................................... 13 G. Conclusions and Recommendations ................................................................................... 14 AST/UST Closure Report January 20, 2023 D’Arrigo Property Page 6 Gastonia, North Carolina 28054 Blue Ridge Project No. 22-6232.1 Figures 1. Site Vicinity Map 2. Site Map 3. Site Detail Plan Tables 1. Site History - UST/AST System and Other Release Information 2. Site History - UST/AST Owner/Operator and Other Responsible Party Information 3. Summary of Soil Analytical Laboratory Results Appendices A. UST Closure Photographs B. UST-3 Form – Notice of Intent: UST Permanent Closure or Change-in-Service C. Fire Department Permit D. UST-2B Form – Site Investigation Report for Permanent Closure or Change-in-Service of Unregistered UST E. UST Disposal Certificate F. Residual Fuel Disposal Manifest G. Soil Disposal Manifests H. Quality Assurance/Quality Control Procedures Drilling and Field Activities Protocol I. Laboratory Analytical Data and Chain of Custody AST/UST Closure Report January 20, 2023 D’Arrigo Property Page 7 Gastonia, North Carolina 28054 Blue Ridge Project No. 22-6232.1 D. Site History and Characterization 1. UST Owner/Operator Information The former Underground Storage Tank (UST) and former Aboveground Storage Tanks (AST) systems located at 901 Dr. Martin Luther King Jr. Way (Site) in Gastonia, NC were owned by Mr. John D’Arrigo. Mr. D’Arrigo never operated the USTs that were discovered at the Site or the former ASTs. The UST/AST former operator is unknown. Refer to Table 2: Site History - UST/AST Owner/Operator and Other Responsible Party Information for additional information regarding the USTs and ASTs. 2. UST/AST System and Other Release Information The AST system and all associated components were removed from the Site between June and August 2022. Blue Ridge personnel was not onsite during disassembly and removal of the ASTs. The former AST system consisted of five (5) approximately 20,000-gallon diesel steel ASTs and one (1) approximately 600,000-gallon heating oil steel AST. The UST system consisted of two (2) 550-gallon and one (1) 3,000-gallon heating oil USTs, located in three (3) individual tank basins. The ASTs and USTs are believed to have been installed circa 1975, which is the year the Site was constructed. The UST systems and all associated components were removed from the Site October 14, 2022 under the direct supervision of Blue Ridge. The location of the former USTs, ASTs, system components and soil samples are illustrated on Figures 2 & 3, respectively. Please refer to Tables 1 – 3 for additional information regarding the USTs and ASTs and soil sampling data. Describe any past releases at this site No previous release information was found on the North Carolina Regional Underground Storage Tanks (RUST) database. 3. AST / Non-UST Spills and Release Information There is no applicable AST or non-UST spill or release information for this Site. Please refer to Table 1: Site History - UST/AST System and Other Release Information for additional information regarding ASTs. AST/UST Closure Report January 20, 2023 D’Arrigo Property Page 8 Gastonia, North Carolina 28054 Blue Ridge Project No. 22-6232.1 4. Release Information for Current UST/AST Closure Based on the information obtained during the recent UST/AST closure activities, a release has not been confirmed and additional soil and groundwater assessment is not warranted. 5. Site Characteristics  Status of the facility at this present time (active / inactive): Several on-site structures have been demolished and removed from the property and the Site currently contains a single story office building with an adjoining warehouse. The property borders are surrounded by a chain link fence in all directions. A UST system status change for the three (3) USTs to “Permanently Closed” is requested by means of this report and the attached UST-2B Form – Site Investigation Report for Permanent Closure or Change in Service of Unregistered USTs, also sent to the Raleigh Central Office on January 20, 2023.  Describe surrounding property use: Primarily commercial properties currently surround the Site.  Water supply wells associated with this site or adjacent properties: No water supply wells (WSWs) were evident on the subject property and public water is available to the Site and surrounding properties. No obvious signs of WSWs were observed on the Site or surrounding properties.  Surface Water Bodies on or Within the Vicinity of the Site: There were no surface water bodies observed within the immediate vicinity of the Site. 6. Summary of Assessment and Corrective Actions Blue Ridge personnel was not onsite during disassembly and removal of the ASTs. Minor petroleum odors and minor staining was noted beneath and immediately surrounding the AST loading rack during the AST removal activities. As a precaution, the property owner requested the over-excavation and removal of the potentially petroleum impacted soils surrounding the AST loading rack. Over-excavation and removal of potentially petroleum contaminated soils adjacent to the former AST loading rack was conducted under the direct supervision of Blue Ridge during the UST/AST system closure activities on October 19, 2022. When no obvious evidence of potential contamination remained based on field observations/screening with a handheld photoionization detector (PID) for VOCs, the AST over-excavation AST/UST Closure Report January 20, 2023 D’Arrigo Property Page 9 Gastonia, North Carolina 28054 Blue Ridge Project No. 22-6232.1 activities were halted. One (1) bottom and four (4) sidewall confirmation soil samples were subsequently collected from the excavation area. Approximately 31.50 tons of potentially impacted soil immediately adjacent to the former AST loading rack were removed, stock-piled and transported for proper off-site disposal. Please refer to Appendix G for the Soil Disposal Manifests. E. Closure Procedures 1. Preparations for Closure Prior to initiating closure activities, a UST-3 Form: Notice of Intent: UST Permanent Closure or Change in Service, dated June 14, 2022, was submitted to NCDEQ, DWM. A copy of the UST-3 Form is included as Appendix B. The North Carolina One Call Center was contacted and requested that the local utility services conduct an Electromagnetic (EM) Survey in the area of concern at the Site to determine the orientation and location of underground utility lines. 2. Procedures for Closure The six (6) ASTs and all associated components were removed from the Site between June and August 2022, while the three (3) USTs were removed from the Site October 2022. Blue Ridge personnel was not onsite during disassembly and removal of the ASTs. The six (6) ASTs were empty prior to conducting field activities and minute residual liquid remaining in the tanks was extracted. Prior to conducting field activities, the three (3) USTs also were checked and pumped any fuel/residual material. A total of approximately 2,070 gallons of residual heating oil, diesel fuel and residual petroleum based water was removed from the ASTs and USTs and disposed of at Zero Waste Recycling, LLC of Charlotte, NC on September 22, 2022. Please refer to Appendix F - Residual Fuel Disposal Manifests. Prior to removal of the USTs, the tanks were purged of volatile organic compounds (VOCs) utilizing dry ice until rendered inert. Upon removal, the USTs appeared to be in good condition with no holes, minor pitting or corrosion observed (see photos in Appendix A). No groundwater or bedrock was encountered during the UST removal. The location of the former AST and UST system components is illustrated on Figures 2 and 3, respectively. Photographs from the closure activities at the Site are included as Appendix A. The UST-2B Form – Site Investigation Report for Permanent Closure or Change in Service of Unregistered USTs is included as Appendix D. 3. Residual Material and Tank Disposal Handling  Describe the storage, sampling and disposal of the residual material and tanks: A total of approximately 2,070 gallons of residual heating oil, diesel fuel and residual petroleum based water was removed from the ASTs and USTs and disposed of at AST/UST Closure Report January 20, 2023 D’Arrigo Property Page 10 Gastonia, North Carolina 28054 Blue Ridge Project No. 22-6232.1 Zero Waste Recycling, LLC of Charlotte, NC on September 22, 2022. During closure activities, the USTs were rendered inert with dry ice. The three (3) removed USTs and six (6) removed ASTs were loaded and transported to Foss Recycling located in Gastonia, North Carolina. The UST Disposal Certificates and Residual Fuel Disposal Manifests are included as Appendix E and F, respectively. Upon removal, the USTs appeared to be in good condition with no holes, minor pitting or corrosion observed. 4. Soil Excavation Activities  Describe excavation procedures noting the condition of the soils and the dimensions of the excavation in relation to the system, piping and/or pumps: The six (6) ASTs were removed from the Site prior to the removal of the USTs. Blue Ridge personnel was not onsite during disassembly and removal of the ASTs. Minor petroleum odors and minor staining was noted beneath and immediately surrounding the AST loading rack during the AST closure activities. As a precaution, the property owner requested the over-excavation and removal of the potentially petroleum impacted soils surrounding the AST loading rack. The over-excavation activities were conducted under the direct supervision of Blue Ridge on October 19, 2022. When no obvious evidence of potential contamination remained based on field observations/screening with a handheld photoionization detector (PID) for VOCs, the AST over-excavation activities were halted. One (1) bottom and four (4) sidewall confirmation soil samples were subsequently collected from the excavation area. The final dimensions of the AST over-excavation area were approximately 18’ long X 8’ wide X 7’ deep. The remaining three (3) USTs were excavated and removed on October 14, 2022 with very minor odor and no visual staining observed. Only the soils above and adjacent deemed necessary to remove the USTs were excavated during the tank removals. The final dimensions of the UST basins containing UST #1 and UST #2 each were 10 feet long X 8 feet wide X 6 feet deep, while the final dimension of UST #3 were 24 feet long x 8 feet wide x 7.5 feet deep. The UST basin excavations were absent of odor or staining. No groundwater, bedrock or free product was encountered during the excavation of the USTs. Please note the copper product lines of UST #1 and UST #2 ran beneath the adjacent building, while UST #3 did not provide evidence of any product lines. The location of the former UST basin is illustrated on Figures 2 & 3, respectively.  Depth of tank(s) from land surface to top and base of tank: The tops of the UST # 1 and UST #2 were approximately 2 feet bgl and the base of the USTs was at approximately 6 feet bgl. The top of UST #3 was approximately 1.5 feet bgl and the base of the UST was at approximately 6 feet bgl. AST/UST Closure Report January 20, 2023 D’Arrigo Property Page 11 Gastonia, North Carolina 28054 Blue Ridge Project No. 22-6232.1  Soil type(s) encountered: Grayish brown loose gravel surrounded UST #1, while UST #2 and #3 were immediately surrounded by a reddish orange, friable micaceous minor clayey silt. Soils located beneath the former ASTs also consisted of a reddish orange, friable micaceous minor clayey silt.  Type and source of backfill used: The excavation was backfilled using the overburden material, tamped and tracked in with the excavator.  Note if groundwater, free product, or bedrock was encountered: Groundwater was not encountered during the tank removal activities; therefore, it was not necessary to install a monitoring well. No free product or bedrock was encountered during the excavation of the USTs.  Describe the method of temporary storage, sampling, and treatment/disposal of soil: Blue Ridge personnel was not onsite during disassembly and removal of the ASTs. Over-excavation and removal of potentially petroleum contaminated soils adjacent to the former AST loading rack was conducted under the direct supervision of Blue Ridge on October 19, 2022. When no obvious evidence of potential contamination remained based on field observations/screening the over-excavation activities were halted and one (1) bottom and four (4) sidewall confirmation soil samples were subsequently collected. Approximately 31.50 tons of potentially impacted soil immediately adjacent to the former AST loading rack were removed and transported to Environmental Soil Inc. of Lattimore, North Carolina for proper off-site disposal. Please refer to Appendix G for the Soil Disposal Manifests. F. Site Investigation 1. Field Screening Information  Physical characteristics of the soil samples, as observed during collection: The soils encountered during the UST/AST Closure activities were primarily described as a reddish orange, friable micaceous minor clayey silt to the excavation termination depth.  Field instrumentation used to screen soils: PID utilized for screening of VOCs.  Field instrument calibration procedures: Page 2 of Appendix H. AST/UST Closure Report January 20, 2023 D’Arrigo Property Page 12 Gastonia, North Carolina 28054 Blue Ridge Project No. 22-6232.1  Screening results: PID readings of VOCs were detected in soil samples collected during the closure activities. See Table 3 for field screening VOCs noted during the UST/AST closure activities. 2. Soil Sampling Information  Lithological description of excavation: Grayish brown loose gravel surrounded UST #1, while UST #2 and #3 were immediately surrounded by a reddish orange, friable micaceous minor clayey silt. Soils located beneath the former ASTs also consisted of a reddish orange, friable micaceous minor clayey silt.  Type of samples (from excavation, stockpiled soil, etc.): Soil samples were collected from native soil in the UST basins beneath the bottom of the tanks. Please note the USTs were absent of any product piping and/or dispensers. In addition, soil samples were also collected beneath the former AST locations and beneath the associated product piping.  Soil sampling collection procedures (split spoon, grab, hand auger, etc.): Soil samples collected from the UST basins were obtained by grab sample collection from the excavator bucket teeth using clean nitrile gloves and the soil samples collected from the former AST locations were obtained using a stainless-steel hand auger.  Location of samples: See Figure 3 – Site Detail Plan.  Depth of soil samples below land surface: Soil samples were collected from the tank basins within 2-feet beneath the bottom of the USTs at depths ranging from of 6.5 feet to 8-feet bgl. In addition, soil samples were also collected within 2-feet beneath the former AST locations.  Time/Date of sampling: Soil samples were collected from September 8 through October 19, 2022. See Chain-of-Custody Form in Appendix I for sample times.  Sample identification: See Figure 3 & Table 3 and attached Chain-of-Custody Form in Appendix I.  Method(s) of soil sample analysis: EPA Method 8015C with 5030B prep method for Total Petroleum Hydrocarbons – Gasoline Range Organics (TPH-GRO) and EPA Method 8015C with 3550C prep method for Total Petroleum Hydrocarbons – Diesel Range Organics (TPH-DRO). See Table 3 and attached Chain-of-Custody Form in Appendix I. 3. Groundwater and Surface Water Information  Location of water samples: Groundwater or surface water samples were not collected during the UST closure activities. UST Closure Report January 18, 2023 D’Arrigo Property Page 13 Gastonia, North Carolina 28054 Blue Ridge Project No. 22-6232.1  Field Measurements: N/A  Sample collection procedures: N/A  Time/Date Collected: N/A  Sample Identification: N/A  Method(s) of water sample analysis: N/A 4. Quality Control Measure Information  Sampling handling procedures including sample preservation techniques and sample transport procedures: See QA/QC in Appendix H.  Decontamination procedures: See QA/QC in Appendix H.  Time and Date Samples were submitted to lab: See attached Chain-of-Custody Form in Appendix I. 5. Soil and Groundwater Investigation Results  All the target constituents were analyzed at low level detection limits and an “estimated” results, “J” value was reported by the laboratory. The “J” value indicates a concentration greater than the laboratory limit of quantitation (LOQ) and less than the detection limit (DL). Details and the reported “J” value can be found in the laboratory analytical report included as Appendix I.  Analysis from three (3) (T-1, T-2 and T-3S) of the four (4) soil samples collected (T-1, T-2, T-3N and T-3S) during the UST closure activities beneath the USTs, revealed detectable concentrations of TPH-DRO found to be present below the North Carolina Action Level for TPH-DRO. No concentrations of TPH-GRO were found to be present in the four (4) soil samples collected.  Analysis from the seventeen (17) soil samples (SS-1 through SS-12, SW-1 through SW-4 and B-5) collected in association with the former AST system revealed detectable concentrations of TPH-DRO found to be present below the North Carolina Action Level for TPH-DRO of 100 mg/kg in fifteen (15) soil samples (SS-1 through SS- 3, SS-6 through SS-12, SW-1 through SW-4 and B-5) collected. Furthermore, a detectable concentration of TPH-GRO below the North Carolina Action Level of 50 mg/kg was reported in the soil sample collected from SS-8. No concentrations of TPH- DRO or TPH-GRO were reported in the soil samples collected from SS-4 and SS-5.  Refer to Table 3 and Figure 3 for detailed information regarding soil sampling results. A copy of the laboratory analytical data and chain of custody is included as Appendix I. UST Closure Report January 18, 2023 D’Arrigo Property Page 14 Gastonia, North Carolina 28054 Blue Ridge Project No. 22-6232.1 G. Conclusions and Recommendations The former UST and former AST systems located at 901 Dr. Martin Luther King Jr. Way (Site) in Gastonia, NC were owned by Mr. John D’Arrigo. Mr. D’Arrigo never operated the USTs that were discovered at the Site or the former ASTs. Several onsite structures have been demolished and removed from the property and the Site currently contains a single story office building with an adjoining warehouse consisting of Gaston County Parcel ID 305893. The property borders are surrounded by a chain link fence in all directions. The AST system and all associated components were removed from the Site between June and August 2022. Blue Ridge personnel was not onsite during disassembly and removal of the ASTs. The former AST system consisted of five (5) approximately 20,000-gallon diesel steel ASTs and one (1) approximately 600,000-gallon heating oil steel AST. The UST system consisted of two (2) 550-gallon and one (1) 3,000-gallon heating oil USTs, located in three (3) individual tank basins. The USTs and ASTs are believed to have been installed circa 1975, which is the year the Site was constructed. Under the direct supervision of Blue Ridge, the three (3) USTs were excavated and removed from the Site on October 14, 2022 with very minor odor and no visual staining observe during the removal. Only the soils above and adjacent deemed necessary to remove the USTs were excavated during the tank removals. The final dimensions of the UST basins containing UST #1 and UST #2 each were 10 feet long X 8 feet wide X 6 feet deep, while the final dimension of UST #3 were 24 feet long x 8 feet wide x 7.5 feet deep. Please note that the copper product lines of UST #1 and UST #2 ran beneath the adjacent building, while UST #3 did not provide evidence of any product lines. The UST basin excavations were absent of odor or staining. The ASTs and USTs are believed to have been installed circa 1975, which is the year the Site was constructed. Upon removal, the USTs appeared to be in good condition with no holes, minor pitting or corrosion observed (see photos in Appendix A). No groundwater, bedrock or free product was encountered during the excavation of the UST system. Soil samples were collected within 2 feet beneath the bottom of the USTs and within 2 feet beneath the ground surface where the former ASTs once reside. Minor petroleum odors and minor staining was noted beneath and immediately surrounding the AST loading rack during the AST closure activities. As a precaution, the property owner requested the over-excavation and removal of the potentially petroleum impacted soils surrounding the AST loading rack. The over-excavation activities were conducted under the direct supervision of Blue Ridge on October 19, 2022. When no obvious evidence of potential contamination remained based on field observations/screening with a handheld photoionization detector (PID) for VOCs, the AST over-excavation activities were halted. One (1) bottom and four (4) sidewall confirmation soil samples were subsequently collected from the excavation area. The final dimensions of the AST over-excavation area were approximately 18’ long X 8’ wide X 7’ deep. Approximately 31.50 tons of potentially impacted soil immediately adjacent to the former AST loading rack were removed and transported to UST Closure Report January 18, 2023 D’Arrigo Property Page 15 Gastonia, North Carolina 28054 Blue Ridge Project No. 22-6232.1 Environmental Soil Inc. of Lattimore, North Carolina for proper off-site disposal. Analysis from the seventeen (17) soil samples (SS-1 through SS-12, SW-1 through SW-4 and B-5) collected in association with the former AST system revealed detectable concentrations of TPH-DRO found to be present below the North Carolina Action Level for TPH-DRO of 100 mg/kg in fifteen (15) soil samples (SS-1 through SS-3, SS-6 through SS- 12, SW-1 through SW-4 and B-5) collected. Furthermore, a detectable concentration of TPH- GRO below the North Carolina Action Level of 50 mg/kg was reported in the soil sample collected from SS-8. No concentrations of TPH-DRO or TPH-GRO were reported in the soil samples collected from SS-4 and SS-5. No violations of the North Carolina Action Level for TPH-DRO and/or TPH -GRO were reported from the soil samples collected in association with AST #1 through AST #6. Analysis from three (3) (T-1, T-2 and T-3S) of the four (4) soil samples collected (T-1, T-2, T- 3N and T-3S) during the UST closure activities beneath the USTs, revealed detectable concentrations of TPH-DRO found to be present below the North Carolina Action Level for TPH-DRO. No concentrations of TPH-GRO were found to be present in the four (4) soil samples collected. No violations of the North Carolina Action Level for TPH-DRO and/or TPH -GRO were reported from the soil samples collected in association with UST #1 through UST #3. Based on the information obtained during the UST and AST closure activities, Blue Ridge recommends a “No Further Action” (NFA) status be assigned to the Site. This UST-12 Closure Report has been submitted to the North Carolina Department of Environmental Quality (NCDEQ) Mooresville Regional Office for review. If you have any questions regarding this matter, please do not hesitate to contact us at (704) 482-2111. Respectfully Submitted, Blue Ridge Environmental Services, Inc. Kenneth A. Pimienta Senior Project Manager Cliff R. Lundgren, P.G. Senior Consultant/ President N.C. Registration No.1359 cc: Mr. John D’Arrigo FIGURES Figure 1 SITE VICINITY MAP North Client: Project: Location: Blue Ridge Project No. : Date: 1/9/23 John D’Arrigo D’Arrigo Property 901 Dr. Martin Luther King Jr. Way Gastonia, North Carolina 28054 22-6232.1 MW-14 AST #1 AST #2 AST #3 AST #4 AST #5 UST #3 UST #2 UST #1Concrete AST #6 Gravel AST Dirt Burm AST Underground PipingAST Loading Rack Warehouse Building Office Building Former Building Location ID GAL CONTENTS DIM AST #1 20,000 #2 Heating Oil 12' x 53' 4" AST #2 20,000 #2 Heating Oil 12' x 53' 4" AST #3 20,000 #2 Heating Oil 12' x 53' 4" AST #4 20,000 #2 Heating Oil 12' x 53' 4" AST #5 20,000 #2 Heating Oil 12' x 53' 4" AST #6 600,000 #2 Heating Oil N/A SidewalkSidewalkSidewalkAsphalt & Dirt Asphalt Grass & Dirt Former Retaining Wall AST #1 MW-14 AST #1 AST #2 AST #3 AST #4 AST #5 UST #3 UST #2 UST #1Concrete AST #6 Gravel AST Dirt Burm AST Underground Piping AST Loading Rack Warehouse Building Office Building Former Building Location ID GAL CONTENTS DIM AST #1 20,000 #2 Heating Oil 12' x 53' 4" AST #2 20,000 #2 Heating Oil 12' x 53' 4" AST #3 20,000 #2 Heating Oil 12' x 53' 4" AST #4 20,000 #2 Heating Oil 12' x 53' 4" AST #5 20,000 #2 Heating Oil 12' x 53' 4" AST #6 600,000 #2 Heating Oil N/A SidewalkSidewalkSidewalkAsphalt & Dirt Asphalt Grass & Dirt AST #1 SW-1 TPH-DRO: 9.3 TPH-GRO: < 3.9 SW-2 TPH-DRO: 8.3 TPH-GRO: < 4.1 SW-3 TPH-DRO: 7.1 J TPH-GRO: < 3.7 SW-4 TPH-DRO: 8.8 TPH-GRO: < 3.9 SS-5 TPH-DRO: < 4.4 TPH-GRO: < 5.5 SS-6 TPH-DRO: 23 TPH-GRO: < 3.5 SS-7 TPH-DRO: 30 TPH-GRO: < 3.4 SS-8 TPH-DRO: 15 TPH-GRO: 13 SS-9 TPH-DRO: 32 TPH-GRO: < 4 SS-10 TPH-DRO: 27 TPH-GRO: < 3.2 SS-11 TPH-DRO: 6 J TPH-GRO: < 3 SS-12 TPH-DRO: 9.3 TPH-GRO: < 3.2 SS-1 TPH-DRO: 11 TPH-GRO: < 8.8 SS-2 TPH-DRO: 37 TPH-GRO: < 4.5 SS-3 TPH-DRO: 59 TPH-GRO: < 5.9 SS-4 TPH-DRO: < 4.4 TPH-GRO: < 4.6 T-1 TPH-DRO: 5.5 J TPH-GRO: < 4 T-2 TPH-DRO: 4.8 J TPH-GRO: < 4.1 T-3N TPH-DRO: < 4.1 TPH-GRO: < 3.8 T-3S TPH-DRO: 5 TPH-GRO: < 3.9 B-5 TPH-DRO: 9.2 TPH-GRO: < 3.4 TABLES Revision Date:1/4/2023 Incident Number: None UST ID Number Current / Most- Recent Contents Previous Contents Capacity (in gallons) Construction Details Tank Dimensions Description of Piping and Pumps Date Tank Installed Status of UST Release associated with this UST System? 1 #2 Heating Oil #2 Heating Oil 550 Single Wall Steel 46" x 74" None Unknown Removed No 2 #2 Heating Oil #2 Heating Oil 550 Single Wall Steel 46" x 74" None Unknown Removed No 3 #2 Heating Oil #2 Heating Oil 3,000 Single Wall Steel 64" x 18' None Unknown Removed No AST ID Number Current/Last Contents Previous Contents Capacity (in gallons) Construction Details Tank Dimensions (in feet) Description of Piping and Pumps Date Tank Installed Status of the AST Release associated with this AST System? 1 Diesel Diesel 20,000 Single Wall Steel N/A Steel Unknown Removed No 2 Diesel Diesel 20,000 Single Wall Steel N/A Steel Unknown Removed No 3 Diesel Diesel 20,000 Single Wall Steel N/A Steel Unknown Removed No 4 Diesel Diesel 20,000 Single Wall Steel N/A Steel Unknown Removed No 5 Diesel Diesel 20,000 Single Wall Steel N/A Steel Unknown Removed No 6 #2 Heating Oil #2 Heating Oil 600,000 Single Double Wall Steel N/A Steel Unknown Removed No Incident Number Material Released Date of Release None N/A N/A N/A: Not Applicable Blue Ridge Project No. 22-6232.1 Description of Release N/A Table 1 Site History - UST/AST System and Other Release Information D’Arrigo Property 901 Dr. Martin Luther King Jr. Way Gastonia, Gaston Co., North Carolina 28054 Facility I.D: 00-0-0000047507 Rev Date: 1/4/23 Incident Number: None UST ID Number Tank #1 through Tank #3 Facility ID Number None City State Zip Telephone Number Gastonia NC 28054 (704) 417-6788 City State Zip Telephone Number N/A N/A N/A N/A Incident Number 16471 Date Incident Occurred 4/30/1996 Date Incident Reported 6/26/1996 Date Incident Closed 3/8/2019 City State Zip Telephone Number Gastonia NC 28054 (704) 824-6714 N/A: Not Applicable 859 North Marietta Street Street Address N/A Other Incidents Onsite or Commingled/In Close Proximity Name of Responsible Party for Other Incident PSNC Energy Street Address Street Address 901 Dr. Martin Luther King Jr. Way Name of Operator Dates of Operation Unknown 1975 - Unknown Date Blue Ridge Project No. 22-6232.1 Name of Owner Dates of Operation Mr. John D’Arrigo Never Operated Facility I.D: 00-0-0000047507 Table 2 Site History - UST/AST Owner/Operator and Other Responsible Party Information D’Arrigo Property 901 Dr. Martin Luther King Jr. Way Gastonia, Gaston Co., North Carolina 28054 EPA METHOD 8015C with 3550C Prep EPA METHOD 8015C with 5030B Prep Field Screening Sample ID Date Collected Source Area Sample Interval Depth (ft.) Incident Phase SS-1 09/08/22 Former AST Area 1 3 AST Closure 11 < 8.8 1.7 SS-2 09/08/22 Former AST Area 1 3 AST Closure 37 < 4.5 2.3 SS-3 09/08/22 Former AST Area 1 3 AST Closure 59 < 5.9 1.8 SS-4 09/08/22 Former AST Area 1 3 AST Closure < 4.4 < 4.6 1.2 SS-5 09/08/22 Former AST Area 1 3 AST Closure < 4.4 < 5.5 1.3 SS-6 09/08/22 Former AST Area 2 2 AST Closure 23 < 3.5 2.1 SS-7 09/08/22 Former AST Area 2 2 AST Closure 30 < 3.4 1.1 SS-8 09/08/22 Former AST Area 2 2 AST Closure 15 13 3.7 SS-9 09/08/22 Former AST Area 2 2 AST Closure 32 < 4 1.6 SS-10 09/08/22 Former AST Area 2 2 AST Closure 27 < 3.2 1.3 SS-11 10/19/22 Piping 3 AST Closure 6 J < 3 6.4 SS-12 10/19/22 Piping 3 AST Closure 9.3 < 3.2 7.6 T-1 10/14/22 UST-1 7 UST Closure 5.5 J < 4 0.3 Summary of Soil Analytical Laboratory Results & Field Screening Table 3 Contaminant of Concern (mg/Kg)TPH- DROBlue Ridge Project No. 22-6232.1 Facility I.D: None Gastonia, Gaston Co., North Carolina 28054 901 Dr. Martin Luther King Jr. Way D’Arrigo Property Analytical Method TPH- GROPID Reading (ppm) EPA METHOD 8015C with 3550C Prep EPA METHOD 8015C with 5030B Prep Field Screening Sample ID Date Collected Source Area Sample Interval Depth (ft.) Incident Phase Summary of Soil Analytical Laboratory Results & Field Screening Table 3 Contaminant of Concern (mg/Kg)TPH- DROBlue Ridge Project No. 22-6232.1 Facility I.D: None Gastonia, Gaston Co., North Carolina 28054 901 Dr. Martin Luther King Jr. Way D’Arrigo Property Analytical Method TPH- GROPID Reading (ppm)T-2 10/14/22 UST-2 6.5 UST Closure 4.8 J < 4.1 0.3 T-3N 10/14/22 UST-3 8 UST Closure < 4.1 < 3.8 0.7 T-3S 10/14/22 UST-3 8 UST Closure 5 < 3.9 0.0 SW-1 10/19/22 South Sidewall 5 UST Closure 9.3 < 3.9 4.0 SW-2 10/19/22 West Sidewall 5 UST Closure 8.3 < 4.1 4.0 SW-3 10/19/22 North Sidewall 5 UST Closure 7.1 J < 3.7 0.0 SW-4 10/19/22 East Sidewall 5 UST Closure 8.8 < 3.9 0.0 B-5 10/19/22 Bottom 7 UST Closure 9.2 < 3.4 6.7 100 50 DRO - Diesel Range Organics < : Less than laboratory detection limit. mg/kg - milligrams per kilogram GRO - Gasoline Range Organics Concentrations in Bold Exceed Action Level J - Estimated Result <LOQ and >DL ppm - Parts Per Million PID - Photoionization Detector --- = Not Applicable/Not Present/Not Measured North Carolina Action Level (mg/kg) TPH - Total Petroleum Hydrocarbons APPENDICES APPENDIX A UST Closure Report January 17, 2023 D’Arrigo Property Page 1 Gastonia, Gaston Co., NC Blue Ridge Project No. 22-6232.1 1. View of UST #1 once UST was uncovered. 2. View of UST #2. Note the basin which contained UST #1 is shown to the right of the photograph. UST Closure Report January 17, 2023 D’Arrigo Property Page 2 Gastonia, Gaston Co., NC Blue Ridge Project No. 22-6232.1 4. View of UST #3 once removed from the excavation. 3. Additional view of UST #2. UST Closure Report January 17, 2023 D’Arrigo Property Page 3 Gastonia, Gaston Co., NC Blue Ridge Project No. 22-6232.1 5. View of excavation area that contained UST #3. 6. View of excavation area that contained UST #3 once excavation was backfilled. UST Closure Report January 17, 2023 D’Arrigo Property Page 4 Gastonia, Gaston Co., NC Blue Ridge Project No. 22-6232.1 7. View of UST #1 once removed from the excavation area. 8. View of excavation area that contained UST #2. UST Closure Report January 17, 2023 D’Arrigo Property Page 5 Gastonia, Gaston Co., NC Blue Ridge Project No. 22-6232.1 9. View of former AST loading rack area shown with the concrete footers. 10. View of former AST loading rack area excavation. UST Closure Report January 17, 2023 D’Arrigo Property Page 6 Gastonia, Gaston Co., NC Blue Ridge Project No. 22-6232.1 12. View of former location of AST #1 through AST #5 . 11. View of the former location of AST #6. APPENDIX B APPENDIX C APPENDIX D APPENDIX E www.elite-envirosvc.com • info@elite-envirosvc.com • Office 803.818-5288 • Mobile 704.914.8568 Elite Environmental Services, Inc. • 322 Clarendon Estates Drive • Clover, SC 29710 CERTIFICATE OF CLOSURE (AST) Aboveground Storage Tank Be it known the five tanks located at: 901 Dr. Martin Luther King Jr. Way Gastonia, NC 28054 (5) tanks of which contained waste gasoline with the following capacities of twenty thousand gallons, the tanks contained residual material that was removed and then tank was removed per API standards on 06.30.2022 By: __________________________________ Position: ______Vice President ____________________ Contractor: Elite Environmental Services 322 Clarendon Estates Drive Clover, SC 29710 Metal Recycler: Foss Metal Recyclers Hwy 321 Gastonia, NC Elite Environmental Services, Inc. Project No. 101443 Original to Customer, copy to file www.elite-envirosvc.com • info@elite-envirosvc.com • Office 803.818-5288 • Mobile 704.914.8568 Elite Environmental Services, Inc. • 322 Clarendon Estates Drive • Clover, SC 29710 CERTIFICATE OF CLOSURE (AST) Aboveground Storage Tank Be it known the one tank located at: 901 Dr. Martin Luther King Jr. Way Gastonia, NC 28054 (1) tank of which contained waste fuel oil with the following capacity of six hundred thousand gallons, the tank contained residual material that was removed and then tank was removed per API standards on 08.19.2022 By: __________________________________ Position: ______Vice President ____________________ Contractor: Elite Environmental Services 322 Clarendon Estates Drive Clover, SC 29710 Metal Recycler: Foss Metal Recyclers Hwy 321 Gastonia, NC Elite Environmental Services, Inc. Project No. 101443 Original to Customer, copy to file www.elite-envirosvc.com • info@elite-envirosvc.com • Office 803.818-5288 • Mobile 704.914.8568 Elite Environmental Services, Inc. • 322 Clarendon Estates Drive • Clover, SC 29710 CERTIFICATE OF CLOSURE (UST) Underground Storage Tank Be it known the five tanks located at: 901 Dr. Martin Luther King Jr. Way Gastonia, NC 28054 (5) tanks of which contained waste fuel oil with the following capacities of five hundred and fifty gallons, the tanks contained residual material that was removed and then tank was removed per API standards on 10.14.2022 and 10.20.2022 By: __________________________________ Position: ______Vice President ____________________ Contractor: Elite Environmental Services 322 Clarendon Estates Drive Clover, SC 29710 Metal Recycler: Foss Metal Recyclers Hwy 321 Gastonia, NC Elite Environmental Services, Inc. Project No. 101443 Original to Customer, copy to file www.elite-envirosvc.com • info@elite-envirosvc.com • Office 803.818-5288 • Mobile 704.914.8568 Elite Environmental Services, Inc. • 322 Clarendon Estates Drive • Clover, SC 29710 CERTIFICATE OF CLOSURE (UST) Underground Storage Tank Be it known the one tank located at: 901 Dr. Martin Luther King Jr. Way Gastonia, NC 28054 (1) tank of which contained waste fuel oil with the following capacities of three thousand gallons, the tanks contained residual material that was removed and then tank was removed per API standards on 10.14.2022 By: __________________________________ Position: ______Vice President ____________________ Contractor: Elite Environmental Services 322 Clarendon Estates Drive Clover, SC 29710 Metal Recycler: Foss Metal Recyclers Hwy 321 Gastonia, NC Elite Environmental Services, Inc. Project No. 101443 Original to Customer, copy to file APPENDIX F APPENDIX G APPENDIX H Page 1 2315 Kings Road Extension Shelby, North Carolina 28152 (O) 704.482.2111 (F) 704.482.4335 Email: BRESI@BlueRidge-ESI.com Blue Ridge Environmental Services, Inc. Quality Assurance/Quality Control Procedures Drilling and Field Activities Protocol Pre-Drilling Protocol Blue Ridge will contact a commercial utilities location service a minimum of 48 hours (per location service requirements) prior to mobilization of the drill crew to the project site. It will be the responsibility of the utilities location service to locate and delineate (by marking the ground surface), to the extent possible, buried or underground utilities which may be encountered during or impeded by drilling activities. This should include but may not be limited to: electrical power services, private and/or municipal water and sewer services, telecommunication services, natural gas services, and/or other public or municipal utilities. Borehole locations will not be made closer than 36" from surface delineated utilities. If closer proximity to delineated utilities is required, bore hole advancement will be conducted by hand auger boring protocol. Prior to commencement of drilling, the augers, down hole equipment and associated tools will be cleaned in a designated decontamination control area using a steam cleaner or high-pressure washer. Bulk soil material which may remain inside or outside of the augers or tools will be removed. Augers will also be pressure washed between each successive bore hole to remove any soil material from the preceding boring. Before raising the drill rig mast, Blue Ridge drilling personnel will observe over-head conditions for the presence of aerial mounted utilities, tree limbs, canopies, awnings, building overhangs or other structural impedances to normal drill rig operations. Drill Protocol and Techniques Bore holes utilized in sub-surface intrusive investigations will be advanced using a trailer mounted Simco 2400 SK-1 drill rig equipped with 4.5 inch outside diameter solid stem augers or 3.25-inch inner diameter hollow stem augers. Where warranted, shallow boring hole advancement may require utilization of a steel hand auger equipped with a 3" inside diameter barrel. Page 2 2315 Kings Road Extension Shelby, North Carolina 28152 (O) 704.482.2111 (F) 704.482.4335 Email: BRESI@BlueRidge-ESI.com Soil Sampling Collection and Analysis The sample preparation area at each bore hole location will be located as reasonably possible away from running motors or where discharged vapors, exhaust and/or fumes may come in contact with the sample. Towels, field meters, sample jars and other equipment will be placed such that they do not come into contact with soil or other materials which may contaminate the sampled soils. Unless specified by the client or by project requirements, soil samples will be collected at approximately 5- foot intervals. Soil samples will be retrieved according to one of two sampling protocols (dependent upon project or client requirements): (1) by split barrel sampling protocol or (2) from bulk soil material retrieved from the solid stem auger following flight advancement. In an effort to reduce cross contamination of samples, soil samples which are to be submitted for chemical analysis will only be handled by the geologist using fresh, manufacturer clean, latex examination gloves. Following retrieval, the soil sample from each interval will be split into roughly equal portions with one portion subjected to field examination and classification by Blue Ridge geologic personnel and the remaining portion placed into a glass sample container to await selection for chemical analysis. Samples which are to be submitted for volatile constituent analysis will be thermally isolated by being placed into the plastic ice chest. After the sample is retrieved from the bore hole and placed into the sample container, the project name, sampling interval, data and time will be noted on the container. Soil Screening and Photoionization Detector Soil samples collected from each sampling interval will be subjected to on site screening by head space analytical method utilizing a Photovac brand portable photoionization detector (PID). Prior to the soil screening, the PID will be calibrated in the field to 98.9 parts per million (ppm) using isobutylene calibration gas per manufacturer's standards. Soil screening will be conducted by placing a spilt portion of each sample collected from the specified sampling interval into a resealable plastic bag. The bag is then placed aside to allow the head space air above the sample to equilibrate. Following the anticipated equilibration interval, the probe of the PID is inserted through the side of the sample bag and the resulting levels of volatile organic vapors recorded. PID levels are recorded in parts per million (ppm) and may be an indication of the relative concentration of volatile organic compounds in the soil. Page 3 2315 Kings Road Extension Shelby, North Carolina 28152 (O) 704.482.2111 (F) 704.482.4335 Email: BRESI@blueridge-esi.com Monitoring Well Construction Protocol Monitoring well bore hole advancement will be conducted utilizing 3.25 inch inside diameter hollow stem auger. For typical monitoring well construction, the bore hole will be advanced through the vadose zone (over burden soil) into the saturated zone to approximately 10 feet below the water table thereby allowing approximately 10 feet of hydrostatic head within the well. The boring will be converted into a groundwater monitoring well by the emplacement of 2 inch inside diameter schedule 40 PVC pipe (well screen and riser). The well screen will have a manufacturer machine cut 0.010-inch slot width and will be emplaced so the top of the well screen will be located above the anticipated seasonal high-water table. The annular space surrounding the well screen will be backfilled utilizing an FX-2 filter sand (45 to 55 mm grain size) to approximately 2 feet above the top of the well screen. The filter pack will be isolated by the emplacement of approximately 2 feet of bentonite pellets and the bentonite seal will then be hydrated and allowed to seal. Following the bentonite seal hydration, the remaining annular space will be backfilled to the surface grade utilizing a neat Portland Type II cement or similar type grout. Typically, the wells will be completed at grade level inside a traffic rated steel vault and the well sealed, using a water-tight locking pressure cap. Where it is possible, the well vault will be raised above the existing surface grade approximately 1 inch to promote surface water run-off and reduce the potential for standing water above the well head. Monitoring Well Development Blue Ridge will allow an anticipated time interval for the well bore to stabilize following construction. The monitoring well will then be developed by hand bailing utilizing a fresh manufacturer clean polyvinyl bailer. Well development will be conducted until: approximately 5 well volumes of water have been removed, the water is relatively silt and sediment "free", or until essentially dry. Well development should be performed to accomplish the following: 1) To remove silt and sediment which may have entered the well during construction activities. 2) To remove mud cake and "smeared material@ on the bore hole walls from drilling. 3) To seat and grade the filter pack. 4) To promote hydraulic conductivity into the well bore. Monitoring Well Gauging Static water levels within each monitoring well will be measured. Measurements will be made from the top of the casing (riser) and recorded to the nearest 0.01 foot. Blue Ridge will electronically measure for the presence of free product in suspect wells. Where free product Page 4 2315 Kings Road Extension Shelby, North Carolina 28152 (O) 704.482.2111 (F) 704.482.4335 Email: BRESI@blueridge-esi.com is indicated to be present, the depth to the top of the product layer and the depth to the top of the water will be recorded. Measurement will be made from the top of the well casing (riser) and recorded to the nearest 0.01 foot. Monitoring wells will be gauged before performing sample collection events at other times that may be required and warranted. The water level indicator and the oil/water interface probe will be cleaned with a solution of laboratory grade soap (Alconox) and distilled water, rinsed with distilled water, rinsed with methanol alcohol and finally rinsed with deionized water both before the first well is checked and between successive wells. Bailers used to inspect the water surface will also be cleaned between successive wells using a solution of 5% tri-sodium phosphate and water. Groundwater Sampling Whenever possible, prior to conducting the initial sample collection event for any given monitoring well, Blue Ridge will allow for the well to stabilize following monitoring well development. Before conducting each sampling event, an attempt will be made to purge each well of a minimum of three volumes of water or until the well becomes essentially dry. All wells will then be allowed to recharge in part or in whole prior to sampling. Groundwater samples will be collected by Blue Ridge personnel utilizing disposable manufacturer clean polyvinyl bailers equipped with a bottom ball check valve. An inert string will be used to lower the bailer to the water surface. The string will be replaced between successive samples. The sample will be collected by gently lowering the bailer into the water, thereby reducing degasification and/or volatilization of the sample. After the bailer is lowered into the water, the sample will be allowed to stabilize for approximately three seconds, allowing the ball valve to close. Care will be taken not to overfill the bailer, allowing inspection of the water surface upon removal of the bailer from the well. Once the bailer is removed, water samples will be transferred to glass vials in such a manner as to reduce volatilization. To reduce the potential of sample cross contamination, Blue Ridge personnel will don fresh disposable latex examination gloves between each monitoring well sampling point and whenever contact with groundwater is possible. Transportation of Samples to Laboratory Before drilling activities are initiated, a plastic ice chest will be prepared for temporary soil and water sample storage. Preparation will include placing ice packs into the ice chest for thermal isolation in an attempt to preserve sample integrity. The cooler will be pre-chilled using blue ice, ice packs or similar items to provide thermal isolation of the sample materials. The maximum holding time for samples to be tested for volatile organics is 14 days. Therefore, samples will be delivered to the laboratory and analyzed by the laboratory within this time frame. The laboratory has been consulted regarding holding times. If the samples are taken directly to the lab from the drill site, they will be held in the same pre-chilled cooler. Page 5 2315 Kings Road Extension Shelby, North Carolina 28152 (O) 704.482.2111 (F) 704.482.4335 Email: BRESI@blueridge-esi.com If the samples cannot be taken directly to the lab, they will be taken to Blue Ridge's office, where the sample containers will be transferred immediately from the cooler to the assigned refrigerator, until such time that they can be taken to the lab. When the samples are scheduled to be delivered to the lab, they will be transferred from the refrigerator to a pre-chilled cooler until delivery to the lab has been made. Blue Ridge Chain of Custody Protocol For each set of samples collected from the specified project site, Blue Ridge will enter all samples, containers, and ice chests into standard chain of custody protocol. A chain of custody form will be established for each sampling event a includes the following information: (1) project name and location, (2) sampling personnel, (3) project management personnel, (4) sample identification numbers, (5) sample collection date and time, (6) sample matrix {soil or water}, (7) sample description, (8) preservatives utilized, (9) number of containers, (10) requested parameters, (11) miscellaneous field or laboratory remarks, (12) and transference records. The chain of custody form will accompany the samples through each phase of the delivery process. APPENDIX I The electronic signature above is the equivalent of a handwritten signature. This report shall not be reproduced,except in its entirety,without the written approval of Pace Analytical Services,LLC. Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.) 106 Vantage Point Drive West Columbia,SC 29172 Tel:803-791-9700 Fax:803-791-9111 www.pacelabs.com Report of Analysis Blue Ridge Environmental Services 2315 Kings Road Ext. Shelby,NC 28152 Attention:Cliff Lundgren Project Name:D'Arrigo Property (ASTs) Project Number:22-6232.1 Lot Number:XI12035 Date Completed:09/30/2022 09/30/2022 9:50 AM Approved and released by: Project Manager II:Edward Barnett Page 1 of 21 PACE ANALYTICAL SERVICES,LLC SC DHEC No:32010001 NELAC No:E87653 NC DENR No:329 NC Field Parameters No:5639 Pace Analytical Services,LLC (formerly Shealy Environmetal Services,Inc.) 106 Vantage Point Drive West Columbia,SC 29172 (803)791-9700 Fax (803)791-9111 www.pacelabs.com Case Narrative Blue Ridge Environmental Services Lot Number:XI12035 This Report of Analysis contains the analytical result(s)for the sample(s)listed on the Sample Summary following this Case Narrative.The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report.Where sampling is conducted by the client,results relate to the accuracy of the information provided,and as the samples are received. Sample receipt,sample analysis,and data review have been performed in accordance with the most current approved The NELAC Institute (TNI)standards,the Pace Analytical Services,LLC ("Pace") Laboratory Quality Manual,standard operating procedures (SOPs),and Pace policies.Any exceptions to the TNI standards,the Laboratory Quality Manual,SOPs or policies are qualified on the results page or discussed below. Pace is a TNI accredited laboratory;however,the following analyses are currently not listed on our TNI scope of accreditation:Drinking Water:VOC (excluding BTEX,MTBE,Naphthalene,&1,2- dichloroethane)EPA 524.2,E.coli and Total coliforms SM 9223 B-2004,Solid Chemical Material:TOC Walkley-Black,Biological Tissue:All,Non-Potable Water:SGT-HEM EPA 1664B,Silica EPA 200.7, Boron,Calcium,Silicon,Strontium EPA 200.8,Bicarbonate,Carbonate,and Hydroxide Alkalinity SM 2320 B-2011,SM 9221 C E-2006 &SM 9222D-2006,Strontium SW-846 6010D,VOC SM 6200 B-2011,Fecal Coliform Colilert-18. Where applicable,all soil sample results (including LOQ and DL if requested)are corrected for dry weight unless flagged with a "W"qualifier. If you have any questions regarding this report,please contact the Pace Project Manager listed on the cover page. TPH-GRO Insufficient sample volume was provided to perform matrix spike/matrix spike duplicate (MS/MSD)for analytical batch 54633.An LCS/LCSD was run in lieu of an MS/MSD. TPH-DRO Surrogate recovered marginally high in sample XI12035-009.As the sample could not be reanalyzed in hold the initial data has been reported. Page 2 of 21 PACE ANALYTICAL SERVICES, LLC Sample Summary Blue Ridge Environmental Services Lot Number: XI12035 Sample Number Sample ID Matrix Date Sampled Date Received 001 09/08/2022 0845SS-1 Solid 09/12/2022 002 09/08/2022 0858SS-2 Solid 09/12/2022 003 09/08/2022 0916SS-3 Solid 09/12/2022 004 09/08/2022 0927SS-4 Solid 09/12/2022 005 09/08/2022 0939SS-5 Solid 09/12/2022 006 09/08/2022 0951SS-6 Solid 09/12/2022 007 09/08/2022 1006SS-7 Solid 09/12/2022 008 09/08/2022 1020SS-8 Solid 09/12/2022 009 09/08/2022 1031SS-9 Solid 09/12/2022 010 09/08/2022 1045SS-10 Solid 09/12/2022 (10 samples) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 3 of 21 PACE ANALYTICAL SERVICES, LLC Detection Summary Blue Ridge Environmental Services Lot Number: XI12035 Sample Sample ID Matrix Parameter Method Result Q Units Page 001 SS-1 Solid TPH-DRO 8015C 5.6 J mg/kg 5 002 SS-2 Solid TPH-DRO 8015C 37 mg/kg 6 003 SS-3 Solid TPH-DRO 8015C 59 mg/kg 7 006 SS-6 Solid TPH-DRO 8015C 23 mg/kg 10 007 SS-7 Solid TPH-DRO 8015C 30 mg/kg 11 008 SS-8 Solid TPH-DRO 8015C 15 mg/kg 12 008 SS-8 Solid TPH-GRO 8015C 13 mg/kg 12 009 SS-9 Solid TPH-DRO 8015C 32 Q mg/kg 13 010 SS-10 Solid TPH-DRO 8015C 27 mg/kg 14 (9 detections) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 4 of 21 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: Blue Ridge Environmental Services SS-1 XI12035-001 09/08/2022 0845 09/12/2022 Solid % Solids:59.0 09/13/2022 2135 TPH - DRO Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3550C 8015C 1 09/16/2022 1455 NCM 09/15/2022 1501 54268 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL TPH-DRO 8015C 5.6 J 1mg/Kg5.511 AcceptanceRun 1 Surrogate Q % Recovery Limits o - Terphenyl 97 55-120 TPH - GRO Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8015C 1 09/20/2022 1342 ECB 54633 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL TPH-GRO 8015C ND 1mg/Kg8.818 AcceptanceRun 1 Surrogate Q % Recovery Limits Bromofluorobenzene 141 23-179 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 5 of 21 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: Blue Ridge Environmental Services SS-2 XI12035-002 09/08/2022 0858 09/12/2022 Solid % Solids:77.8 09/13/2022 2135 TPH - DRO Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3550C 8015C 1 09/16/2022 1504 NCM 09/15/2022 1501 54268 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL TPH-DRO 8015C 37 1mg/Kg4.28.6 AcceptanceRun 1 Surrogate Q % Recovery Limits o - Terphenyl 104 55-120 TPH - GRO Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8015C 1 09/20/2022 1407 ECB 54633 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL TPH-GRO 8015C ND 1mg/Kg4.59.0 AcceptanceRun 1 Surrogate Q % Recovery Limits Bromofluorobenzene 143 23-179 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 6 of 21 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: Blue Ridge Environmental Services SS-3 XI12035-003 09/08/2022 0916 09/12/2022 Solid % Solids:73.0 09/13/2022 2135 TPH - DRO Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3550C 8015C 1 09/16/2022 1513 NCM 09/15/2022 1501 54268 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL TPH-DRO 8015C 59 1mg/Kg4.59.1 AcceptanceRun 1 Surrogate Q % Recovery Limits o - Terphenyl 107 55-120 TPH - GRO Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8015C 1 09/20/2022 1432 ECB 54633 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL TPH-GRO 8015C ND 1mg/Kg5.912 AcceptanceRun 1 Surrogate Q % Recovery Limits Bromofluorobenzene 133 23-179 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 7 of 21 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: Blue Ridge Environmental Services SS-4 XI12035-004 09/08/2022 0927 09/12/2022 Solid % Solids:74.5 09/13/2022 2135 TPH - DRO Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3550C 8015C 1 09/16/2022 1521 NCM 09/15/2022 1501 54268 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL TPH-DRO 8015C ND 1mg/Kg4.48.9 AcceptanceRun 1 Surrogate Q % Recovery Limits o - Terphenyl 111 55-120 TPH - GRO Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8015C 1 09/20/2022 1457 ECB 54633 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL TPH-GRO 8015C ND 1mg/Kg4.69.2 AcceptanceRun 1 Surrogate Q % Recovery Limits Bromofluorobenzene 135 23-179 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 8 of 21 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: Blue Ridge Environmental Services SS-5 XI12035-005 09/08/2022 0939 09/12/2022 Solid % Solids:74.8 09/13/2022 2135 TPH - DRO Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3550C 8015C 1 09/16/2022 1530 NCM 09/15/2022 1501 54268 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL TPH-DRO 8015C ND 1mg/Kg4.48.9 AcceptanceRun 1 Surrogate Q % Recovery Limits o - Terphenyl 110 55-120 TPH - GRO Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8015C 1 09/20/2022 1522 ECB 54633 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL TPH-GRO 8015C ND 1mg/Kg5.511 AcceptanceRun 1 Surrogate Q % Recovery Limits Bromofluorobenzene 135 23-179 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 9 of 21 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: Blue Ridge Environmental Services SS-6 XI12035-006 09/08/2022 0951 09/12/2022 Solid % Solids:87.2 09/13/2022 2135 TPH - DRO Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3550C 8015C 1 09/16/2022 1539 NCM 09/15/2022 1501 54268 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL TPH-DRO 8015C 23 1mg/Kg3.87.7 AcceptanceRun 1 Surrogate Q % Recovery Limits o - Terphenyl 113 55-120 TPH - GRO Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8015C 1 09/20/2022 1547 ECB 54633 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL TPH-GRO 8015C ND 1mg/Kg3.57.1 AcceptanceRun 1 Surrogate Q % Recovery Limits Bromofluorobenzene 132 23-179 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 10 of 21 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: Blue Ridge Environmental Services SS-7 XI12035-007 09/08/2022 1006 09/12/2022 Solid % Solids:87.0 09/13/2022 2135 TPH - DRO Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3550C 8015C 1 09/28/2022 1832 NCM 09/20/2022 1451 54659 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL TPH-DRO 8015C 30 1mg/Kg3.87.7 AcceptanceRun 1 Surrogate Q % Recovery Limits o - Terphenyl 105 55-120 TPH - GRO Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8015C 1 09/20/2022 1612 ECB 54633 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL TPH-GRO 8015C ND 1mg/Kg3.46.9 AcceptanceRun 1 Surrogate Q % Recovery Limits Bromofluorobenzene 135 23-179 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 11 of 21 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: Blue Ridge Environmental Services SS-8 XI12035-008 09/08/2022 1020 09/12/2022 Solid % Solids:78.7 09/21/2022 2203 TPH - DRO Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3550C 8015C 1 09/28/2022 1841 NCM 09/20/2022 1451 54659 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL TPH-DRO 8015C 15 1mg/Kg4.18.4 AcceptanceRun 1 Surrogate Q % Recovery Limits o - Terphenyl 101 55-120 TPH - GRO Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8015C 1 09/20/2022 1637 ECB 54633 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL TPH-GRO 8015C 13 1mg/Kg3.77.5 AcceptanceRun 1 Surrogate Q % Recovery Limits Bromofluorobenzene 136 23-179 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 12 of 21 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: Blue Ridge Environmental Services SS-9 XI12035-009 09/08/2022 1031 09/12/2022 Solid % Solids:77.5 09/20/2022 2102 TPH - DRO Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3550C 8015C 1 09/28/2022 1849 NCM 09/20/2022 1451 54659 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL TPH-DRO 8015C 32 Q 1mg/Kg4.28.6 AcceptanceRun 1 Surrogate Q % Recovery Limits o - Terphenyl N 121 55-120 TPH - GRO Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8015C 1 09/20/2022 1702 ECB 54633 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL TPH-GRO 8015C ND 1mg/Kg4.08.1 AcceptanceRun 1 Surrogate Q % Recovery Limits Bromofluorobenzene 140 23-179 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 13 of 21 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: Blue Ridge Environmental Services SS-10 XI12035-010 09/08/2022 1045 09/12/2022 Solid % Solids:85.8 09/21/2022 2203 TPH - DRO Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3550C 8015C 1 09/28/2022 1858 NCM 09/20/2022 1451 54659 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL TPH-DRO 8015C 27 1mg/Kg3.87.7 AcceptanceRun 1 Surrogate Q % Recovery Limits o - Terphenyl 105 55-120 TPH - GRO Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8015C 1 09/20/2022 1727 ECB 54633 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL TPH-GRO 8015C ND 1mg/Kg3.26.3 AcceptanceRun 1 Surrogate Q % Recovery Limits Bromofluorobenzene 131 23-179 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 14 of 21 QC Summary 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 15 of 21 TPH - DRO - MB Batch:Prep Method: Prep Date: Sample ID:XQ54268-001 54268 3550C 09/15/2022 1501Analytical Method:8015C Matrix:Solid Parameter Result Q LOQ DL Units Analysis DateDil TPH-DRO ND 09/16/2022 12196.7 3.3 mg/kg1 Surrogate Q % Rec Acceptance Limit o - Terphenyl 115 55-120 TPH - DRO - LCS Batch:Prep Method: Prep Date: Sample ID:XQ54268-002 54268 3550C 09/15/2022 1501Analytical Method:8015C Matrix:Solid Parameter Result Q % Rec Spike Amount Analysis Date %Rec LimitDil(mg/kg)(mg/kg) TPH-DRO 89 09/16/2022 12271078370-1301 Surrogate Q % Rec Acceptance Limit o - Terphenyl 111 55-120 TPH - DRO - MB Batch:Prep Method: Prep Date: Sample ID:XQ54659-001 54659 3550C 09/20/2022 1451Analytical Method:8015C Matrix:Solid Parameter Result Q LOQ DL Units Analysis DateDil TPH-DRO ND 09/28/2022 18166.7 3.3 mg/kg1 Surrogate Q % Rec Acceptance Limit o - Terphenyl 109 55-120 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% + = RPD is out of criteria _DL = Detection Limit * = RSD is out of criteria 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 16 of 21 TPH - DRO - LCS Batch:Prep Method: Prep Date: Sample ID:XQ54659-002 54659 3550C 09/20/2022 1451Analytical Method:8015C Matrix:Solid Parameter Result Q % Rec Spike Amount Analysis Date %Rec LimitDil(mg/kg)(mg/kg) TPH-DRO 83 09/28/2022 18241008370-1301 Surrogate Q % Rec Acceptance Limit o - Terphenyl 98 55-120 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% + = RPD is out of criteria _DL = Detection Limit * = RSD is out of criteria 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 17 of 21 TPH - GRO - MB Batch:Prep Method: Sample ID:XQ54633-001 54633 5030B Analytical Method:8015C Matrix:Solid Parameter Result Q LOQ DL Units Analysis DateDil TPH-GRO ND 09/20/2022 12345.0 2.5 mg/kg1 Surrogate Q % Rec Acceptance Limit Bromofluorobenzene 124 23-179 TPH - GRO - LCS Batch:Prep Method: Sample ID:XQ54633-002 54633 5030B Analytical Method:8015C Matrix:Solid Parameter Result Q % Rec Spike Amount Analysis Date %Rec LimitDil(mg/kg)(mg/kg) TPH-GRO 55 09/20/2022 11441105070-1301 Surrogate Q % Rec Acceptance Limit Bromofluorobenzene 126 23-179 TPH - GRO - LCSD Batch:Prep Method: Sample ID:XQ54633-003 54633 5030B Analytical Method:8015C Matrix:Solid Parameter Result Q % Rec Spike Amount Analysis Date% RPD %Rec Limit % RPD LimitDil(mg/kg)(mg/kg) TPH-GRO 55 09/20/2022 12091105070-1300.36 201 Surrogate Q % Rec Acceptance Limit Bromofluorobenzene 118 23-179 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% + = RPD is out of criteria _DL = Detection Limit * = RSD is out of criteria 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 18 of 21 Chain of Custody and Miscellaneous Documents 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 19 of 21 PACE ANALYTICAL SERVICES, LLC 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 21 of 21 The electronic signature above is the equivalent of a handwritten signature. This report shall not be reproduced,except in its entirety,without the written approval of Pace Analytical Services,LLC. Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.) 106 Vantage Point Drive West Columbia,SC 29172 Tel:803-791-9700 Fax:803-791-9111 www.pacelabs.com Report of Analysis Blue Ridge Environmental Services 2315 Kings Road Ext. Shelby,NC 28152 Attention:Cliff Lundgren Project Name:DArrigo Property Project Number:22-6232.1 Lot Number:XJ18078 Date Completed:11/17/2022 11/17/2022 12:19 PM Approved and released by: Project Manager II:Edward Barnett Page 1 of 14 PACE ANALYTICAL SERVICES,LLC SC DHEC No:32010001 NELAC No:E87653 NC DENR No:329 NC Field Parameters No:5639 Pace Analytical Services,LLC (formerly Shealy Environmetal Services,Inc.) 106 Vantage Point Drive West Columbia,SC 29172 (803)791-9700 Fax (803)791-9111 www.pacelabs.com Case Narrative Blue Ridge Environmental Services Lot Number:XJ18078 This Report of Analysis contains the analytical result(s)for the sample(s)listed on the Sample Summary following this Case Narrative.The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report.Where sampling is conducted by the client,results relate to the accuracy of the information provided,and as the samples are received. Sample receipt,sample analysis,and data review have been performed in accordance with the most current approved The NELAC Institute (TNI)standards,the Pace Analytical Services,LLC ("Pace") Laboratory Quality Manual,standard operating procedures (SOPs),and Pace policies.Any exceptions to the TNI standards,the Laboratory Quality Manual,SOPs or policies are qualified on the results page or discussed below. Pace is a TNI accredited laboratory;however,the following analyses are currently not listed on our TNI scope of accreditation:Drinking Water:VOC (excluding BTEX,MTBE,Naphthalene,&1,2- dichloroethane)EPA 524.2,E.coli and Total coliforms SM 9223 B-2004,Solid Chemical Material:TOC Walkley-Black,Biological Tissue:All,Non-Potable Water:SGT-HEM EPA 1664B,Silica EPA 200.7, Boron,Calcium,Silicon,Strontium EPA 200.8,Bicarbonate,Carbonate,and Hydroxide Alkalinity SM 2320 B-2011,SM 9221 C E-2006 &SM 9222D-2006,Strontium SW-846 6010D,VOC SM 6200 B-2011,Fecal Coliform Colilert-18. Where applicable,all soil sample results (including LOQ and DL if requested)are corrected for dry weight unless flagged with a "W"qualifier. If you have any questions regarding this report,please contact the Pace Project Manager listed on the cover page. TPH-DRO Samples XJ18078-001,XJ18078-002,XJ18078-003 and XJ18078-004 were reanalyzed outside of analytical holding time due to LCS recovery out of range as well as surrogate recovery in the samples and Method Blank.The reanalysis confirmed the initial results and the in-hold data has been reported. TPH-GRO Insufficient sample volume was provided to perform matrix spike/matrix spike duplicate (MS/MSD)for analytical batch 57957.An LCS/LCSD was run in lieu of an MS/MSD. Page 2 of 14 PACE ANALYTICAL SERVICES, LLC Sample Summary Blue Ridge Environmental Services Lot Number: XJ18078 Sample Number Sample ID Matrix Date Sampled Date Received 001 10/14/2022 1119T-1 Solid 10/18/2022 002 10/14/2022 1045T-2 Solid 10/18/2022 003 10/14/2022 1138T-3N Solid 10/18/2022 004 10/14/2022 1151T-3S Solid 10/18/2022 (4 samples) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 3 of 14 PACE ANALYTICAL SERVICES, LLC Detection Summary Blue Ridge Environmental Services Lot Number: XJ18078 Sample Sample ID Matrix Parameter Method Result Q Units Page 001 T-1 Solid TPH-DRO 8015C 5.5 JQL mg/kg 5 002 T-2 Solid TPH-DRO 8015C 4.8 JQL mg/kg 6 004 T-3S Solid TPH-DRO 8015C 5 JL mg/kg 8 (3 detections) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 4 of 14 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: Blue Ridge Environmental Services T-1 XJ18078-001 10/14/2022 1119 10/18/2022 Solid % Solids:75.5 10/20/2022 2207 TPH - DRO Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3550C 8015C 1 11/14/2022 1333 NCM 10/24/2022 0000 57913 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL TPH-DRO 8015C 5.5 JQL 1mg/Kg4.38.6 AcceptanceRun 1 Surrogate Q % Recovery Limits o - Terphenyl N 45 55-120 TPH - GRO Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8015C 1 10/24/2022 1757 ECB 57957 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL TPH-GRO 8015C ND 1mg/Kg4.08.0 AcceptanceRun 1 Surrogate Q % Recovery Limits Bromofluorobenzene 139 23-179 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 5 of 14 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: Blue Ridge Environmental Services T-2 XJ18078-002 10/14/2022 1045 10/18/2022 Solid % Solids:74.7 10/20/2022 2207 TPH - DRO Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3550C 8015C 1 11/14/2022 1341 NCM 10/24/2022 0000 57913 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL TPH-DRO 8015C 4.8 JQL 1mg/Kg4.38.8 AcceptanceRun 1 Surrogate Q % Recovery Limits o - Terphenyl N 37 55-120 TPH - GRO Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8015C 1 10/24/2022 1822 ECB 57957 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL TPH-GRO 8015C ND 1mg/Kg4.18.2 AcceptanceRun 1 Surrogate Q % Recovery Limits Bromofluorobenzene 149 23-179 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 6 of 14 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: Blue Ridge Environmental Services T-3N XJ18078-003 10/14/2022 1138 10/18/2022 Solid % Solids:79.8 10/20/2022 2207 TPH - DRO Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3550C 8015C 1 11/14/2022 1349 NCM 10/24/2022 0000 57913 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL TPH-DRO 8015C ND L 1mg/Kg4.18.3 AcceptanceRun 1 Surrogate Q % Recovery Limits o - Terphenyl 61 55-120 TPH - GRO Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8015C 1 10/24/2022 1847 ECB 57957 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL TPH-GRO 8015C ND 1mg/Kg3.87.7 AcceptanceRun 1 Surrogate Q % Recovery Limits Bromofluorobenzene 140 23-179 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 7 of 14 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: Blue Ridge Environmental Services T-3S XJ18078-004 10/14/2022 1151 10/18/2022 Solid % Solids:79.1 10/20/2022 2207 TPH - DRO Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3550C 8015C 1 11/14/2022 1358 NCM 10/24/2022 0000 57913 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL TPH-DRO 8015C 5.0 JL 1mg/Kg4.08.2 AcceptanceRun 1 Surrogate Q % Recovery Limits o - Terphenyl 86 55-120 TPH - GRO Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8015C 1 10/24/2022 1912 ECB 57957 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL TPH-GRO 8015C ND 1mg/Kg3.97.8 AcceptanceRun 1 Surrogate Q % Recovery Limits Bromofluorobenzene 143 23-179 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 8 of 14 QC Summary 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 9 of 14 TPH - DRO - MB Batch:Prep Method: Prep Date: Sample ID:XQ57913-001 57913 3550C 10/24/2022 0000Analytical Method:8015C Matrix:Solid Parameter Result Q LOQ DL Units Analysis DateDil TPH-DRO ND 11/14/2022 12516.7 3.3 mg/kg1 Surrogate Q % Rec Acceptance Limit o - Terphenyl N 46 55-120 TPH - DRO - LCS Batch:Prep Method: Prep Date: Sample ID:XQ57913-002 57913 3550C 10/24/2022 0000Analytical Method:8015C Matrix:Solid Parameter Result Q % Rec Spike Amount Analysis Date %Rec LimitDil(mg/kg)(mg/kg) TPH-DRO 42 11/14/2022 1259N518370-1301 Surrogate Q % Rec Acceptance Limit o - Terphenyl N 53 55-120 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% + = RPD is out of criteria _DL = Detection Limit * = RSD is out of criteria 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 10 of 14 TPH - GRO - MB Batch:Prep Method: Sample ID:XQ57957-001 57957 5030B Analytical Method:8015C Matrix:Solid Parameter Result Q LOQ DL Units Analysis DateDil TPH-GRO ND 10/24/2022 15255.0 2.5 mg/kg1 Surrogate Q % Rec Acceptance Limit Bromofluorobenzene 123 23-179 TPH - GRO - LCS Batch:Prep Method: Sample ID:XQ57957-002 57957 5030B Analytical Method:8015C Matrix:Solid Parameter Result Q % Rec Spike Amount Analysis Date %Rec LimitDil(mg/kg)(mg/kg) TPH-GRO 54 10/24/2022 14351075070-1301 Surrogate Q % Rec Acceptance Limit Bromofluorobenzene 116 23-179 TPH - GRO - LCSD Batch:Prep Method: Sample ID:XQ57957-003 57957 5030B Analytical Method:8015C Matrix:Solid Parameter Result Q % Rec Spike Amount Analysis Date% RPD %Rec Limit % RPD LimitDil(mg/kg)(mg/kg) TPH-GRO 53 10/24/2022 15001065070-1301.3 201 Surrogate Q % Rec Acceptance Limit Bromofluorobenzene 118 23-179 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% + = RPD is out of criteria _DL = Detection Limit * = RSD is out of criteria 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 11 of 14 Chain of Custody and Miscellaneous Documents 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 12 of 14 PACE ANALYTICAL SERVICES, LLC 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 13 of 14 PACE ANALYTICAL SERVICES, LLC 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 14 of 14 The electronic signature above is the equivalent of a handwritten signature. This report shall not be reproduced,except in its entirety,without the written approval of Pace Analytical Services,LLC. Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.) 106 Vantage Point Drive West Columbia,SC 29172 Tel:803-791-9700 Fax:803-791-9111 www.pacelabs.com Report of Analysis Blue Ridge Environmental Services 2315 Kings Road Ext. Shelby,NC 28152 Attention:Cliff Lundgren Project Name:DArrigo Property Project Number:22-6232.1 Lot Number:XJ20090 Date Completed:11/15/2022 11/15/2022 2:11 PM Approved and released by: Project Manager II:Edward Barnett Page 1 of 18 PACE ANALYTICAL SERVICES,LLC SC DHEC No:32010001 NELAC No:E87653 NC DENR No:329 NC Field Parameters No:5639 Pace Analytical Services,LLC (formerly Shealy Environmetal Services,Inc.) 106 Vantage Point Drive West Columbia,SC 29172 (803)791-9700 Fax (803)791-9111 www.pacelabs.com Case Narrative Blue Ridge Environmental Services Lot Number:XJ20090 This Report of Analysis contains the analytical result(s)for the sample(s)listed on the Sample Summary following this Case Narrative.The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report.Where sampling is conducted by the client,results relate to the accuracy of the information provided,and as the samples are received. Sample receipt,sample analysis,and data review have been performed in accordance with the most current approved The NELAC Institute (TNI)standards,the Pace Analytical Services,LLC ("Pace") Laboratory Quality Manual,standard operating procedures (SOPs),and Pace policies.Any exceptions to the TNI standards,the Laboratory Quality Manual,SOPs or policies are qualified on the results page or discussed below. Pace is a TNI accredited laboratory;however,the following analyses are currently not listed on our TNI scope of accreditation:Drinking Water:VOC (excluding BTEX,MTBE,Naphthalene,&1,2- dichloroethane)EPA 524.2,E.coli and Total coliforms SM 9223 B-2004,Solid Chemical Material:TOC Walkley-Black,Biological Tissue:All,Non-Potable Water:SGT-HEM EPA 1664B,Silica EPA 200.7, Boron,Calcium,Silicon,Strontium EPA 200.8,Bicarbonate,Carbonate,and Hydroxide Alkalinity SM 2320 B-2011,SM 9221 C E-2006 &SM 9222D-2006,Strontium SW-846 6010D,VOC SM 6200 B-2011,Fecal Coliform Colilert-18. Where applicable,all soil sample results (including LOQ and DL if requested)are corrected for dry weight unless flagged with a "W"qualifier. If you have any questions regarding this report,please contact the Pace Project Manager listed on the cover page. TPH-GRO Insufficient sample volume was provided to perform matrix spike/matrix spike duplicate (MS/MSD)for analytical batch 57957.An LCS/LCSD was run in lieu of an MS/MSD. Surrogate recovery for the following sample was outside the upper control limit:XJ20090-001.This sample did not contain any target analytes;therefore,re-extraction and/or re-analysis was not performed. Page 2 of 18 PACE ANALYTICAL SERVICES, LLC Sample Summary Blue Ridge Environmental Services Lot Number: XJ20090 Sample Number Sample ID Matrix Date Sampled Date Received 001 10/19/2022 1116SW-1 Solid 10/20/2022 002 10/19/2022 1122SW-2 Solid 10/20/2022 003 10/19/2022 1127SW-3 Solid 10/20/2022 004 10/19/2022 1138SW-4 Solid 10/20/2022 005 10/19/2022 1142B-5 Solid 10/20/2022 006 10/19/2022 1203SS-11 Solid 10/20/2022 007 10/19/2022 1249SS-12 Solid 10/20/2022 (7 samples) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 3 of 18 PACE ANALYTICAL SERVICES, LLC Detection Summary Blue Ridge Environmental Services Lot Number: XJ20090 Sample Sample ID Matrix Parameter Method Result Q Units Page 001 SW-1 Solid TPH-DRO 8015C 9.3 mg/kg 5 002 SW-2 Solid TPH-DRO 8015C 8.3 mg/kg 6 003 SW-3 Solid TPH-DRO 8015C 7.1 J mg/kg 7 004 SW-4 Solid TPH-DRO 8015C 14 mg/kg 8 005 B-5 Solid TPH-DRO 8015C 9.2 mg/kg 9 006 SS-11 Solid TPH-DRO 8015C 6 J mg/kg 10 007 SS-12 Solid TPH-DRO 8015C 9.3 mg/kg 11 (7 detections) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 4 of 18 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: Blue Ridge Environmental Services SW-1 XJ20090-001 10/19/2022 1116 10/20/2022 Solid % Solids:79.3 10/26/2022 0048 TPH - DRO Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3550C 8015C 1 11/14/2022 1423 NCM 10/23/2022 1300 57877 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL TPH-DRO 8015C 9.3 1mg/Kg4.18.4 AcceptanceRun 1 Surrogate Q % Recovery Limits o - Terphenyl 101 55-120 TPH - GRO Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8015C 1 10/24/2022 1938 ECB 57957 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL TPH-GRO 8015C ND Q 1mg/Kg3.97.7 AcceptanceRun 1 Surrogate Q % Recovery Limits Bromofluorobenzene N 185 23-179 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 5 of 18 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: Blue Ridge Environmental Services SW-2 XJ20090-002 10/19/2022 1122 10/20/2022 Solid % Solids:79.4 10/26/2022 0048 TPH - DRO Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3550C 8015C 1 11/14/2022 1449 NCM 10/23/2022 1300 57877 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL TPH-DRO 8015C 8.3 1mg/Kg4.18.3 AcceptanceRun 1 Surrogate Q % Recovery Limits o - Terphenyl 94 55-120 TPH - GRO Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8015C 1 10/24/2022 2002 ECB 57957 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL TPH-GRO 8015C ND 1mg/Kg4.18.2 AcceptanceRun 1 Surrogate Q % Recovery Limits Bromofluorobenzene 143 23-179 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 6 of 18 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: Blue Ridge Environmental Services SW-3 XJ20090-003 10/19/2022 1127 10/20/2022 Solid % Solids:79.8 10/26/2022 0048 TPH - DRO Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3550C 8015C 1 11/14/2022 1457 NCM 10/23/2022 1300 57877 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL TPH-DRO 8015C 7.1 J 1mg/Kg4.18.3 AcceptanceRun 1 Surrogate Q % Recovery Limits o - Terphenyl 91 55-120 TPH - GRO Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8015C 1 10/24/2022 2027 ECB 57957 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL TPH-GRO 8015C ND 1mg/Kg3.77.5 AcceptanceRun 1 Surrogate Q % Recovery Limits Bromofluorobenzene 139 23-179 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 7 of 18 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: Blue Ridge Environmental Services SW-4 XJ20090-004 10/19/2022 1138 10/20/2022 Solid % Solids:75.4 10/26/2022 0048 TPH - DRO Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3550C 8015C 1 11/14/2022 1505 NCM 10/23/2022 1300 57877 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL TPH-DRO 8015C 14 1mg/Kg4.38.8 AcceptanceRun 1 Surrogate Q % Recovery Limits o - Terphenyl 91 55-120 TPH - GRO Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8015C 1 10/24/2022 2052 ECB 57957 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL TPH-GRO 8015C ND 1mg/Kg3.97.9 AcceptanceRun 1 Surrogate Q % Recovery Limits Bromofluorobenzene 144 23-179 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 8 of 18 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: Blue Ridge Environmental Services B-5 XJ20090-005 10/19/2022 1142 10/20/2022 Solid % Solids:81.6 10/26/2022 0048 TPH - DRO Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3550C 8015C 1 11/14/2022 1514 NCM 10/23/2022 1300 57877 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL TPH-DRO 8015C 9.2 1mg/Kg4.08.1 AcceptanceRun 1 Surrogate Q % Recovery Limits o - Terphenyl 82 55-120 TPH - GRO Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8015C 1 10/24/2022 2117 ECB 57957 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL TPH-GRO 8015C ND 1mg/Kg3.46.9 AcceptanceRun 1 Surrogate Q % Recovery Limits Bromofluorobenzene 141 23-179 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 9 of 18 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: Blue Ridge Environmental Services SS-11 XJ20090-006 10/19/2022 1203 10/20/2022 Solid % Solids:89.1 10/26/2022 0048 TPH - DRO Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3550C 8015C 1 11/14/2022 1522 NCM 10/23/2022 1300 57877 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL TPH-DRO 8015C 6.0 J 1mg/Kg3.77.5 AcceptanceRun 1 Surrogate Q % Recovery Limits o - Terphenyl 97 55-120 TPH - GRO Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8015C 1 10/24/2022 2142 ECB 57957 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL TPH-GRO 8015C ND 1mg/Kg3.06.0 AcceptanceRun 1 Surrogate Q % Recovery Limits Bromofluorobenzene 136 23-179 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 10 of 18 Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: Blue Ridge Environmental Services SS-12 XJ20090-007 10/19/2022 1249 10/20/2022 Solid % Solids:87.5 10/26/2022 0048 TPH - DRO Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3550C 8015C 1 11/14/2022 1531 NCM 10/23/2022 1300 57877 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL TPH-DRO 8015C 9.3 1mg/Kg3.77.6 AcceptanceRun 1 Surrogate Q % Recovery Limits o - Terphenyl 101 55-120 TPH - GRO Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8015C 1 10/24/2022 2207 ECB 57957 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL TPH-GRO 8015C ND 1mg/Kg3.26.4 AcceptanceRun 1 Surrogate Q % Recovery Limits Bromofluorobenzene 133 23-179 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 11 of 18 QC Summary 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 12 of 18 TPH - DRO - MB Batch:Prep Method: Prep Date: Sample ID:XQ57877-001 57877 3550C 10/23/2022 1300Analytical Method:8015C Matrix:Solid Parameter Result Q LOQ DL Units Analysis DateDil TPH-DRO ND 11/14/2022 14066.7 3.3 mg/kg1 Surrogate Q % Rec Acceptance Limit o - Terphenyl 93 55-120 TPH - DRO - LCS Batch:Prep Method: Prep Date: Sample ID:XQ57877-002 57877 3550C 10/23/2022 1300Analytical Method:8015C Matrix:Solid Parameter Result Q % Rec Spike Amount Analysis Date %Rec LimitDil(mg/kg)(mg/kg) TPH-DRO 73 11/14/2022 1415878370-1301 Surrogate Q % Rec Acceptance Limit o - Terphenyl 91 55-120 TPH - DRO - MS Batch:Prep Method: Prep Date: Sample ID:XJ20090-001MS 57877 3550C 10/23/2022 1300Analytical Method:8015C Matrix:Solid Parameter Result Q % Rec Spike Amount Analysis Date %Rec Limit Sample Amount Dil(mg/kg)(mg/kg)(mg/kg) TPH-DRO 99 11/14/2022 14328510070-1309.3 1 Surrogate Q % Rec Acceptance Limit o - Terphenyl 76 55-120 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% + = RPD is out of criteria _DL = Detection Limit * = RSD is out of criteria 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 13 of 18 TPH - DRO - MSD Batch:Prep Method: Prep Date: Sample ID:XJ20090-001MD 57877 3550C 10/23/2022 1300Analytical Method:8015C Matrix:Solid Parameter Result Q % Rec Spike Amount Analysis Date% RPD %Rec Limit % RPD Limit Sample Amount Dil(mg/kg)(mg/kg)(mg/kg) TPH-DRO 92 11/14/2022 14407910070-1306.7 209.3 1 Surrogate Q % Rec Acceptance Limit o - Terphenyl 70 55-120 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% + = RPD is out of criteria _DL = Detection Limit * = RSD is out of criteria 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 14 of 18 TPH - GRO - MB Batch:Prep Method: Sample ID:XQ57957-001 57957 5030B Analytical Method:8015C Matrix:Solid Parameter Result Q LOQ DL Units Analysis DateDil TPH-GRO ND 10/24/2022 15255.0 2.5 mg/kg1 Surrogate Q % Rec Acceptance Limit Bromofluorobenzene 123 23-179 TPH - GRO - LCS Batch:Prep Method: Sample ID:XQ57957-002 57957 5030B Analytical Method:8015C Matrix:Solid Parameter Result Q % Rec Spike Amount Analysis Date %Rec LimitDil(mg/kg)(mg/kg) TPH-GRO 54 10/24/2022 14351075070-1301 Surrogate Q % Rec Acceptance Limit Bromofluorobenzene 116 23-179 TPH - GRO - LCSD Batch:Prep Method: Sample ID:XQ57957-003 57957 5030B Analytical Method:8015C Matrix:Solid Parameter Result Q % Rec Spike Amount Analysis Date% RPD %Rec Limit % RPD LimitDil(mg/kg)(mg/kg) TPH-GRO 53 10/24/2022 15001065070-1301.3 201 Surrogate Q % Rec Acceptance Limit Bromofluorobenzene 118 23-179 Note:Calculations are performed before rounding to avoid round-off errors in calculated results LOQ = Limit of Quantitation ND = Not detected at or above the DL J = Estimated result < LOQ and > DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% + = RPD is out of criteria _DL = Detection Limit * = RSD is out of criteria 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 15 of 18 Chain of Custody and Miscellaneous Documents 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 16 of 18 PACE ANALYTICAL SERVICES, LLC 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) Page 17 of 18