MO-29703_48829_CA_O_20221206_Phase II ESA

SUMMIT Engineering, Laboratory & Testing, PC 3575 Centre Circle
Fort Mill, South Carolina 29715
www.SUMMIT-companies.com Phone: [phone]
Fax: [phone]

April 14, 2017

Marlin Bay, LLC
Attention: Keith Rains
310 Spring Crest Drive
Fort Mill, SC 29715

Subject: Limited Phase II Environmental Site Assessment
Miranda Road Site
3701 Miranda Road Charlotte, Mecklenburg County, North Carolina
SUMMIT Project No. 3962.01

Dear Mr. Rains:
SUMMIT ENGINEERING, LABRATORY & TESTING, PC (SUMMIT) is pleased to submit the
following report of our Limited Phase II Environmental Site Assessment (ESA) of the Miranda
Road Site, located at 3701 Miranda Road, Charlotte, Mecklenburg County, North Carolina
(Mecklenburg County Tax IDs: 03315105, 03315225, 03315201).

This report includes a description of the methodology of our investigation and a summary of our
findings and conclusions. If you have any questions regarding our assessment of the subject
property or our conclusions, please do not hesitate to call us at [phone].
Sincerely,
SUMMIT

Patrick W. Lowery, PG Michael D. Zavislak, NRCC-EAC, CIH, PE
Senior Environmental Manager Environmental Department Manager
NC LG No: 2421

SUMMIT’s NC Engineering Firm License No. C-2530

LIMITED PHASE II ENVIRONMENTAL SITE ASSESSMENT

MIRANDA ROAD SITE
CHARLOTTE
MECKLENBURG COUNTY
NORTH CAROLINA SUMMIT PROJECT NO. 3962.01

Marlin Bay, LLC
310 Spring Crest Drive Fort Mill, SC 29715

Prepared By:

SUMMIT ENGINEERING, LABRATORY & TESTING, PC 3575 Centre Circle
Fort Mill, South Carolina 29715
704-504-1717

April 14, 2017
Limited Phase II ESA – Miranda Road Site SUMMIT Project No. 3962.01
Charlotte, North Carolina April 14, 2017

E:\Project Forms\Projects\3962.01 Miranda Road Phase II\3962.01 Miranda Road Site - Phase II ESA.doc i
TABLE OF CONTENTS
1.0 EXECUTIVE SUMMARY ...................................................................................................... 1
2.0 INTRODUCTION .................................................................................................................... 2
2.1. PURPOSE .......................................................................................................................................... 2
2.2. SITE DESCRIPTION ........................................................................................................................ 2
2.3. ASSESSMENT HISTORY ................................................................................................................ 3
2.4. WORK PLAN OBJECTIVES ........................................................................................................... 3
3.0 PROPERTY SETTING ............................................................................................................ 4
3.1. TOPOGRAPHIC SETTING.............................................................................................................. 4
3.2. GEOLOGIC SETTING ..................................................................................................................... 4
3.3. HYDROLOGIC SETTING ............................................................................................................... 5
4.0 SUMMARY OF FIELD ACTIVITIES ..................................................................................... 6
4.1. DRILLING ACTIVITES AND METHODS ..................................................................................... 6
4.2. SAMPLING ....................................................................................................................................... 7
4.3. PACKING AND SHIPMENT ........................................................................................................... 8
4.4. SAMPLING POINT ABANDONMENT ......................................................................................... 8
5.0 SUMMARY OF LABORATORY ANALYSIS ........................................................................ 9
6.0 FINDINGS & CONCLUSIONS ............................................................................................ 10
7.0 QUALIFICATION OF REPORT ........................................................................................... 11
8.0 ADDITIONAL SERVICES .................................................................................................... 12
9.0 REFERENCES ....................................................................................................................... 13

APPENDICES
Appendix I: FIGURES
Appendix II: ANALYTICAL SUMMARY Appendix III: ANALYTICAL RESULTS
Appendix IV: WELL RECORDS/PERMITS

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1.0 EXECUTIVE SUMMARY

On March 31, 2017, SUMMIT Engineering, Laboratory and Testing, PC (SUMMIT) personnel
conducted a Limited Phase II ESA, based on environmental concerns identified in an Phase I ESA,
performed by SUMMIT, dated March 31, 2016. The Phase I ESA identified RECs in connection
with the automotive repair operation located within one (1) parcel of the subject site.

In summary, three (3) groundwater samples were collected from the subject site to identify if the
on-site environmental concerns identified in the Phase I ESA impacted the groundwater quality
beneath the subject site. This assessment focused on the automotive repair operation located at
3701 Miranda Road, and not the entire 35.97 acre site. All collected groundwater samples were
analyzed for the presence of Volatile Organic Compounds (VOCs) by EPA method 8260 and Semi-
Volatile Organic Compounds (SVOCs) by EPA method 8270.

Groundwater samples collected from TMW-3 detected the presence of 1,2-Dichloroethane above its
respected regulatory limits (NCAC 2L). TMW-2 detected the presence of Methyl-tert-butyl ether
below its respective regulatory concentration. No other detections were reported. Based on the
detection of 1,2-Dichloroethane above established regulatory concentrations, SUMMIT concludes
that the environmental concerns identified in the Phase I ESA have impacted the groundwater
quality beneath the subject site.

Due to the limited nature of this assessment, further impacts may exist at the site. Additional
assessment would be recommended in order to collect soil and groundwater quality information
near the septic tank area and further downgradient of the Max Auto Shop. If this assessment was
performed as due diligence prior to purchase or deed transfer, SUMMIT recommends the
perspective owner consider entering the DEQ Brownfields program as a Non-Responsible Party
and completing additional assessment activities under the direction of DEQ Brownfields Program.

Additionally, SUMMIT recommends submitting a copy of this report to North Carolina
Department of Environment Quality.

Limited Phase II ESA – Miranda Road Site SUMMIT Project No. 3962.01 Charlotte, North Carolina April 14, 2017

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2.0 INTRODUCTION
2.1. PURPOSE
SUMMIT was retained by Marline Bay, LLC to perform a Limited Phase II ESA of the Miranda
Road Site, located at 3701 Miranda Road, Charlotte, Mecklenburg County, North Carolina
(Mecklenburg County Tax IDs: 03315105, 03315225, 03315201). The Limited Phase II ESA was
requested in order to assess environmental concerns identified in a Phase I ESA, performed by
SUMMIT ELT, Inc, dated March 31, 2016. This report presents the results of our Limited Phase II
ESA of the Miranda Road Site.

2.2. SITE DESCRIPTION

The subject site is irregular in shape and was noted to be comprised of three (3) contiguous parcels
(Mecklenburg County Parcel IDs: 03315105, 03315225, 03315201) totaling approximately 37.59
acres in area. The site parcels are located along the northern site of Miranda Road and the physical
addresses of 3701 and 3705 Miranda Road correlate with two (2) of the site parcels. The eastern
most parcel (03315225) is generally agricultural with a cell phone tower and pond. Portions of the
property are used for storage of vehicles. The central parcel (03315201) is developed with a cinder
block building along Miranda Road, utilized by Max Auto Shop (3701 Miranda Road). This
building has a single pull through bay and office. The remaining portions of this parcel is
undeveloped agricultural field. The western most parcel (03315105) is developed with a residential
mobile home located along Miranda Road and with agricultural fields in the remaining portions of
the parcel. Two (2) colonial gas high pressure pipelines run north to south through this parcel.
Refer to the Site Location Map shown in Figure 2 of Appendix I for the location of the subject
property.

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2.3. ASSESSMENT HISTORY

SUMMIT completed a Phase I ESA, dated March 31, 2016 for the subject site. The following
Recognized Environmental Conditions (RECs) were identified in the Phase I ESA:

• The historical use of the building located at 3701 Miranda Road as an auto repair facility
was considered a REC.
• A floor drain potentially connected to a septic system was considered to represent a REC.
• Several ASTs and the general housekeeping of the automotive facility was considered to
represent a REC.
• Property owner reported the former use and closure of USTs at the auto repair facility. No
documentation or records of closure could be provided. The former USTs were considered
a REC.

No other site specific or surrounding area assessment history is known at the time of this report.

2.4. WORK PLAN OBJECTIVES

SUMMIT proposed to perform a Limited Phase II ESA according to our understanding of the most
likely potential for impact, in general accordance with ASTM E1903, and in accordance with the
USEPA Field Branches Quality System and Technical Procedures Manual. The proposed scope of
services included the installation and sampling of three (3) temporary monitoring wells in order to
assess the groundwater quality near the automotive shop located on-site. The proposed sampling
locations were placed in accessible locations and in areas that may help identify migrating
contaminants from the area of concern. All samples collected were scheduled to be relinquished to
a NC certified laboratory for analysis of Volatile Organic Compounds (VOCs) by EPA method 8260
and Semi-Volatile Organic Compounds (SVOCs) by EPA method 8270.

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3.0 PROPERTY SETTING

3.1. TOPOGRAPHIC SETTING

The United States Geological Survey (USGS) Charlotte topographic quadrangle map was reviewed
for this report. According to the contour lines on the topographic maps, the site is located on the
side slope of a natural draw that is trending west towards an unnamed tributary. The elevation of
the subject property ranges from approximately 750 feet (along the southeastern property boundary)
to approximately 730 feet (along the northern property boundary) above Mean Sea Level (MSL).
The contour lines indicate the general direction of downward slope is to the north towards an un-
named creek. A pond is located on-site, discharging into the un-named creek that flows north off-
site. The un-named creek flows into Gar Creek. Gar Creek flows into Mountain Island Lake
(Catawba River). Refer to Figure 1 in Appendix I of this report.

3.2. GEOLOGIC SETTING

The property is located in Mecklenburg County, North Carolina, which is located in the south
central Piedmont Physiographic Province. The Piedmont Province generally consists of well-
rounded hills and ridges which are dissected by a well-developed system of draws and streams. The
Piedmont Province is predominantly underlain by metamorphic rock (formed by heat, pressure
and/or chemical action) and igneous rock (formed directly from molten material) which were
initially formed during the Precambrian and Paleozoic eras. The volcanic and sedimentary rocks
deposited in the Piedmont Province during the Precambrian era were the host from the
metamorphism and were changed to gneiss and schist. The more recent Paleozoic era had periods
of igneous emplacement, with at least episodes of regional metamorphism resulting in the majority
of the rock types seen today.

The topography and relief of the Piedmont Province has developed from differential weathering of
the igneous and metamorphic rock. Ridges and hills have been developed on the more easily
weathered and erodible rock. Because of the continued chemical and physical weathering, the
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rocks in the Piedmont Province are now generally covered with a mantle of soil that has weathered
in place from the parent bedrock. These soils vary in thickness and are referred to as residuum or
residual soils. The residuum is typically finer grained and has higher clay content near the surface
because of the advanced weathering. Similarly, the soils typically become coarser grained with
increasing depth because of decreased weathering. As the weathering decreases, the residual soils
generally retain the overall appearance, texture, gradation and foliations of the parent rock.

3.3. HYDROLOGIC SETTING

Based on a review of the United States Geological Survey (USGS) Charlotte topographic
quadrangle map, the inferred groundwater flow direction based on topography appears to be to the
north towards the unnamed tributary of Gar Creek. Refer to Figure 1 in Appendix I for a
topographic map for the subject property.
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4.0 SUMMARY OF FIELD ACTIVITIES

4.1. DRILLING ACTIVITES AND METHODS

Prior to temporary well installation, SUMMIT completed a utility located via NC811. Following
the utility locate submittal, SUMMIT was contacted by a representative of Colonial Pipeline
regarding the two (2) high pressure pipelines within the subject site. Due to the locations of the
pipelines on the downgradient parcel of the subject site, SUMMITs assessment was limited to the
areas immediately surrounding the Max Auto Shop building (within the fence) due to the possibility
of damaging the pipelines with the heavy equipment or drilling augers.

On March 31, 2017, SUMMIT personnel conducted the temporary monitoring well installation
scope of the Limited Phase II ESA. The proposed temporary monitoring well (TMW) locations
were placed in accessible locations within the fenced in portions of the Max Auto Shop as directed
by Colonial Pipeline, and in areas that may help identify migrating contaminants from up-gradient
properties. The locations of the TMW locations can be viewed on the attached Sampling Location
Map, Figure 3, in appendix I.

SUMMIT utilized a CME Hollow Stem Auger drill rig to complete the soil borings and TMW
installation. At each location, a boring was advanced to 40 feet below ground surface (bgs). At
termination depths, the TMWs were constructed within the HSA drill string. The TMWs consisted
of 20 feet of 1-inch Schedule 20 PVC 0.01-inch slotted well screen that was encased in #3 filter
sand and 20-feet of 1-inch Schedule 20 PVC solid riser pipe. A bentonite seal was placed above the
well screen and filter media.

Each boring typically encountered tan/orange fine to medium grained sandy clay and sandy silts.
Soil cuttings generated during TMW installation were spread on-site.

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Groundwater was encountered in all TMWs at approximate depths to water (DTW) ranging from
23 ft bge to 25 ft bgs in the TMWs after installation. New disposable bailer was utilized to purge
the TMW following installation and collect groundwater from each TMW.

Upon completion of the drilling activities, the drilling equipment was decontaminated by the well
driller by use of a steam cleaner or Alconox and tap water wash, tap water rinse, isopropanol rinse
(sampling equipment), and deionized water rinse. Decontamination of the drilling equipment was
performed prior to starting drilling activities, and upon the completion of drilling activities at each
boring/well location.

4.2. SAMPLING

The TMWs were purged of approximately 3 well volumes following installation and allowed to
equilibrate for a minimum of 24 hours prior to sampling. Water elevations were measured
following equilibrium period and prior to sampling. The depth to water measurements are provided
below:

Well ID
Depth to
Water (bgs)
Approximate Surface
Elevation (msl)*
Water Table
Elevation (msl)
TMW-1 30.8 752 721.2
TMW-2 27.8 749 721.2
TMW-3 31.2 752 720.8
All measurements are represented in Feet
MSL – Mean Sea Level * Surface elevations determined Mecklenburg County GIS and field observations. Not surveyed.

Based on the field data it appears that an south to north/northeast hydrologic gradient is present at
the site. The water table elevation ranges from 721 ft msl in the southern and western portion of the
site to 720 ft msl in the northern portion of the site.

Samples were collected utilizing a new disposable bailer on April 4, 2017. Groundwater samples
were containerized in laboratory provided vials and containers, placed on ice and transported to the
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laboratory for analysis. All groundwater samples were analyzed for VOCs (8260) and SVOCs
(8270).

4.3. PACKING AND SHIPMENT

Upon securing the samples in laboratory provided containers, the vial and jar lids were tightly
fastened, and the jars encapsulated in shock-resistant plastic bags. The samples and ice were
double-bagged in large plastic bags, tied off with rubber bands, and packed into a cooler. The
samples were delivered to Pace Analytical, in Huntersville, NC. The vials and jars used for the
collection of the samples at this site were prepared by Pace, and were pre-labeled and contained
analyte-appropriate preservatives. A listing of the preservatives in the sample containers utilized for
the collection of the samples at this site are cataloged in the Chain-Of-Custody record, attached in
Appendix III of this report. The secured samples were relinquished to laboratory on April 4, 2017
for laboratory analysis.

4.4. SAMPLING POINT ABANDONMENT

All boreholes will be abandoned within 60 days of installation in accordance with Mecklenburg
Well requirements. A copy of the well permit can be viewed in Appendix IV of this report.
Limited Phase II ESA – Miranda Road Site SUMMIT Project No. 3962.01 Charlotte, North Carolina April 14, 2017

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5.0 SUMMARY OF LABORATORY ANALYSIS

All samples were relinquished to Pace Analytical on April 4, 2017 for the prescribe analysis. Table
1.0 in Appendix II of this report summarizes all detections. The analytical detections are
summarized below:

• Methyl-tert-butyl ether (MTBE) was detected in groundwater from TMW-2 at 2.4 ug/L,
below NCDEQ reference value of 20 ug/L established in the 15A NCAC 2L standards.

• 1,2-Dichloroethane was detected in groundwater from TMW-3 at 46.5 ug/L, above the
NCDEQ reference value of 0.4 ug/L established in the 15A NCAC 2L standards.

No other detections were identified in the laboratory analysis.

Limited Phase II ESA – Miranda Road Site SUMMIT Project No. 3962.01 Charlotte, North Carolina April 14, 2017

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6.0 FINDINGS & CONCLUSIONS

In summary, three (3) groundwater samples were collected from the subject site to identify if the
on-site environmental concerns identified in the Phase I ESA impacted the groundwater quality
beneath the subject site. This assessment focused on the automotive repair operation located at
3701 Miranda Road, and not the entire 35.97 acre site. All collected groundwater samples were
analyzed for the presence of Volatile Organic Compounds (VOCs) by EPA method 8260 and Semi-
Volatile Organic Compounds (SVOCs) by EPA method 8270.

Groundwater samples collected from TMW-3 detected the presence of 1,2-Dichloroethane above its
respected regulatory limits (NCAC 2L). TMW-2 detected the presence of Methyl-tert-butyl ether
below its respective regulatory concentration. No other detections were reported. Based on the
detection of 1,2-Dichloroethane above established regulatory concentrations, SUMMIT concludes
that the environmental concerns identified in the Phase I ESA have impacted the groundwater
quality beneath the subject site.

Due to the limited nature of this assessment, further impacts may exist at the site. Additional
assessment would be recommended in order to collect soil and groundwater quality information
near the septic tank area and further downgradient of the Max Auto Shop. If this assessment was
performed as due diligence prior to purchase or deed transfer, SUMMIT recommends the
perspective owner consider entering the DEQ Brownfields program as a Non-Responsible Party
and completing additional assessment activities under the direction of DEQ Brownfields Program.

Additionally, SUMMIT recommends submitting a copy of this report to North Carolina
Department of Environment Quality.

Limited Phase II ESA – Miranda Road Site SUMMIT Project No. 3962.01 Charlotte, North Carolina April 14, 2017

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7.0 QUALIFICATION OF REPORT

The Limited Phase II ESA was performed in general accordance with ASTM E1903, and in
accordance with the USEPA Field Branches Quality System and Technical Procedures Manual. The
findings detailed in this report are specific to the conditions in the immediate vicinity of the sample
locations for this particular project.

Limited Phase II ESA – Miranda Road Site SUMMIT Project No. 3962.01 Charlotte, North Carolina April 14, 2017

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8.0 ADDITIONAL SERVICES

This report does not include any environmental assessment of surface water, the determination of
wetlands, the determination of noise impact, the assessment of air quality, the identification of
cultural resources, or the identification of endangered species. These services are beyond the scope
of services of this limited sampling and analysis.

No additional services were provided.
Limited Phase II ESA – Miranda Road Site SUMMIT Project No. 3962.01 Charlotte, North Carolina April 14, 2017

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9.0 REFERENCES

Phase I ESA Report, Mecklenburg County Parcels: 03315105, 0331522, 03315201, by SUMMIT
ELT, Inc, dated March 31, 2016.

United States Geological Survey (USGS) 7.5 minute Topographic Map of the Charlotte
Topographic Quadrangle, 2002.

EPA National Primary Drinking Water Regulations -
http://water.epa.gov/drink/contaminants/index.cfm

15A NCAC 2L Standards –
http://portal.ncdenr.org/web/wq/ps/csu/gwstandards

Limited Phase II ESA – Miranda Road Site SUMMIT Project No. 3962.01
Charlotte, North Carolina April 14, 2017

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APPENDIX I
FIGURES
D:\!Michael!\!SUMMIT!\3962 - Marlin Bay, LLC\3962.01 Meck County Parcels - 03315105, 03315225, 03315201\Environmental\Phase I ESA\Report Files\R-Ph I - Figure 1 Topo.doc SUMMIT ELT, Inc. Project: 3962.01 Figure 1 USGS Topographic Map Miranda Road Site Charlotte, NC Subject Site
D:\!Michael!\!SUMMIT!\3962 - Marlin Bay, LLC\3962.01 Meck County Parcels - 03315105, 03315225, 03315201\Environmental\Phase I ESA\Report Files\R-Ph I - Figure 2 Aerial.doc SUMMIT ELT, Inc. Project: 3962.01 Figure 2 Aerial Photograph Miranda Road Site Charlotte, NC
E:\Project Forms\Projects\3962.01 Miranda Road Phase II\3962.01-Ph I - Figure 3 Sample Location.doc SUMMIT ELT, Inc. Project: 3962.01 Figure 3 Sample Location Map Miranda Road Site Charlotte, NC NTMW-1 TMW-2 TMW-3 Colonial Pipelines Reported Former USTs Reported Septic Tank
Limited Phase II ESA – Miranda Road Site SUMMIT Project No. 3962.01
Charlotte, North Carolina April 14, 2017

E:\Project Forms\Projects\3962.01 Miranda Road Phase II\Appendix II.rtf

APPENDIX II
ANALYTICAL SUMMARY

Miranda Road Site 4/14/2017
3701 Miranda Road, Charlotte, NC SUMMIT Project #: 3962.01
Sample ID Collected Date Matrix Parameter Results Units PQL EPA MCLs NC 2L Standards
TMW-1 4/4/2017 GW VOCs/SVOCs ALL ND ug/L NA NA NA
TMW-2 4/4/2017 GW Methyl-tert-butyl ether 2.4 ug/L 1.0 NA 20
TMW-3 4/4/2017 GW 1,2-Dichloroethane 46.5 ug/L 1.0 5.0 0.4
Notes:
1) NA - Not Applicable
2) NS - Not Sampled
Table 1.0 Summary of Analytical Detections
3) Bolded items were detected above regulatory limits.
Limited Phase II ESA – Miranda Road Site SUMMIT Project No. 3962.01
Charlotte, North Carolina April 14, 2017

E:\Project Forms\Projects\3962.01 Miranda Road Phase II\Appendix III.rtf

APPENDIX III
ANALYTICAL RESULTS

#=CL#
April 10, 2017
LIMS USE: FR - ASHTON BROWN
LIMS OBJECT ID: 92335793
92335793
Project:
Pace Project No.:
RE:
Ashton Brown
3575 Centre Circle
Fort Mill, SC 29718
MIRANDA ROAD
Dear Ashton Brown:
Enclosed are the analytical results for sample(s) received by the laboratory on April 04, 2017. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
[phone]
Enclosures
cc:Michael Zavislak, Summit Engineering
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 29
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92335793
MIRANDA ROAD
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 29
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92335793
MIRANDA ROAD
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92335793001 TMW-1 EPA 8270 74 PASI-CBPJ
EPA 8260 63 PASI-CZDO
92335793002 TMW-2 EPA 8270 74 PASI-CBPJ
EPA 8260 63 PASI-CZDO
92335793003 TMW-3 EPA 8270 74 PASI-CBPJ
EPA 8260 63 PASI-CZDO
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92335793
MIRANDA ROAD
Sample:TMW-1 Lab ID:92335793001 Collected:04/04/17 13:20 Received:04/04/17 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 04/07/17 10:17 83-32-904/06/17 14:0510.0 1
Acenaphthylene ND ug/L 04/07/17 10:17 208-96-804/06/17 14:0510.0 1
Aniline ND ug/L 04/07/17 10:17 62-53-304/06/17 14:0510.0 1
Anthracene ND ug/L 04/07/17 10:17 120-12-704/06/17 14:0510.0 1
Benzo(a)anthracene ND ug/L 04/07/17 10:17 56-55-304/06/17 14:0510.0 1
Benzo(a)pyrene ND ug/L 04/07/17 10:17 50-32-804/06/17 14:0510.0 1
Benzo(b)fluoranthene ND ug/L 04/07/17 10:17 205-99-204/06/17 14:0510.0 1
Benzo(g,h,i)perylene ND ug/L 04/07/17 10:17 191-24-204/06/17 14:0510.0 1
Benzo(k)fluoranthene ND ug/L 04/07/17 10:17 207-08-904/06/17 14:0510.0 1
Benzoic Acid ND ug/L 04/07/17 10:17 65-85-004/06/17 14:0550.0 1
Benzyl alcohol ND ug/L 04/07/17 10:17 100-51-604/06/17 14:0520.0 1
4-Bromophenylphenyl ether ND ug/L 04/07/17 10:17 101-55-304/06/17 14:0510.0 1
Butylbenzylphthalate ND ug/L 04/07/17 10:17 85-68-704/06/17 14:0510.0 1
4-Chloro-3-methylphenol ND ug/L 04/07/17 10:17 59-50-704/06/17 14:0520.0 1
4-Chloroaniline ND ug/L 04/07/17 10:17 106-47-804/06/17 14:0520.0 1
bis(2-Chloroethoxy)methane ND ug/L 04/07/17 10:17 111-91-104/06/17 14:0510.0 1
bis(2-Chloroethyl) ether ND ug/L 04/07/17 10:17 111-44-404/06/17 14:0510.0 1
2-Chloronaphthalene ND ug/L 04/07/17 10:17 91-58-704/06/17 14:0510.0 1
2-Chlorophenol ND ug/L 04/07/17 10:17 95-57-804/06/17 14:0510.0 1
4-Chlorophenylphenyl ether ND ug/L 04/07/17 10:17 7005-72-304/06/17 14:0510.0 1
Chrysene ND ug/L 04/07/17 10:17 218-01-904/06/17 14:0510.0 1
Dibenz(a,h)anthracene ND ug/L 04/07/17 10:17 53-70-304/06/17 14:0510.0 1
Dibenzofuran ND ug/L 04/07/17 10:17 132-64-904/06/17 14:0510.0 1
1,2-Dichlorobenzene ND ug/L 04/07/17 10:17 95-50-104/06/17 14:0510.0 1
1,3-Dichlorobenzene ND ug/L 04/07/17 10:17 541-73-104/06/17 14:0510.0 1
1,4-Dichlorobenzene ND ug/L 04/07/17 10:17 106-46-704/06/17 14:0510.0 1
3,3'-Dichlorobenzidine ND ug/L 04/07/17 10:17 91-94-104/06/17 14:0520.0 1
2,4-Dichlorophenol ND ug/L 04/07/17 10:17 120-83-204/06/17 14:0510.0 1
Diethylphthalate ND ug/L 04/07/17 10:17 84-66-204/06/17 14:0510.0 1
2,4-Dimethylphenol ND ug/L 04/07/17 10:17 105-67-904/06/17 14:0510.0 1
Dimethylphthalate ND ug/L 04/07/17 10:17 131-11-304/06/17 14:0510.0 1
Di-n-butylphthalate ND ug/L 04/07/17 10:17 84-74-204/06/17 14:0510.0 1
4,6-Dinitro-2-methylphenol ND ug/L 04/07/17 10:17 534-52-104/06/17 14:0520.0 1
2,4-Dinitrophenol ND ug/L 04/07/17 10:17 51-28-504/06/17 14:0550.0 1
2,4-Dinitrotoluene ND ug/L 04/07/17 10:17 121-14-204/06/17 14:0510.0 1
2,6-Dinitrotoluene ND ug/L 04/07/17 10:17 606-20-204/06/17 14:0510.0 1
Di-n-octylphthalate ND ug/L 04/07/17 10:17 117-84-004/06/17 14:0510.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 04/07/17 10:17 117-81-704/06/17 14:056.0 1
Fluoranthene ND ug/L 04/07/17 10:17 206-44-004/06/17 14:0510.0 1
Fluorene ND ug/L 04/07/17 10:17 86-73-704/06/17 14:0510.0 1
Hexachloro-1,3-butadiene ND ug/L 04/07/17 10:17 87-68-304/06/17 14:0510.0 1
Hexachlorobenzene ND ug/L 04/07/17 10:17 118-74-104/06/17 14:0510.0 1
Hexachlorocyclopentadiene ND ug/L 04/07/17 10:17 77-47-404/06/17 14:0510.0 1
Hexachloroethane ND ug/L 04/07/17 10:17 67-72-104/06/17 14:0510.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 04/07/17 10:17 193-39-504/06/17 14:0510.0 1
Isophorone ND ug/L 04/07/17 10:17 78-59-104/06/17 14:0510.0 1
1-Methylnaphthalene ND ug/L 04/07/17 10:17 90-12-004/06/17 14:0510.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/10/2017 10:46 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92335793
MIRANDA ROAD
Sample:TMW-1 Lab ID:92335793001 Collected:04/04/17 13:20 Received:04/04/17 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2-Methylnaphthalene ND ug/L 04/07/17 10:17 91-57-604/06/17 14:0510.0 1
2-Methylphenol(o-Cresol)ND ug/L 04/07/17 10:17 95-48-704/06/17 14:0510.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 04/07/17 10:1704/06/17 14:0510.0 1
Naphthalene ND ug/L 04/07/17 10:17 91-20-304/06/17 14:0510.0 1
2-Nitroaniline ND ug/L 04/07/17 10:17 88-74-404/06/17 14:0550.0 1
3-Nitroaniline ND ug/L 04/07/17 10:17 99-09-204/06/17 14:0550.0 1
4-Nitroaniline ND ug/L 04/07/17 10:17 100-01-604/06/17 14:0520.0 1
Nitrobenzene ND ug/L 04/07/17 10:17 98-95-304/06/17 14:0510.0 1
2-Nitrophenol ND ug/L 04/07/17 10:17 88-75-504/06/17 14:0510.0 1
4-Nitrophenol ND ug/L 04/07/17 10:17 100-02-704/06/17 14:0550.0 1
N-Nitrosodimethylamine ND ug/L 04/07/17 10:17 62-75-904/06/17 14:0510.0 1
N-Nitroso-di-n-propylamine ND ug/L 04/07/17 10:17 621-64-704/06/17 14:0510.0 1
N-Nitrosodiphenylamine ND ug/L 04/07/17 10:17 86-30-604/06/17 14:0510.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 04/07/17 10:17 108-60-104/06/17 14:0510.0 1
Pentachlorophenol ND ug/L 04/07/17 10:17 87-86-504/06/17 14:0525.0 1
Phenanthrene ND ug/L 04/07/17 10:17 85-01-804/06/17 14:0510.0 1
Phenol ND ug/L 04/07/17 10:1704/06/17 14:0510.0 1
Pyrene ND ug/L 04/07/17 10:17 129-00-004/06/17 14:0510.0 1
1,2,4-Trichlorobenzene ND ug/L 04/07/17 10:17 120-82-104/06/17 14:0510.0 1
2,4,5-Trichlorophenol ND ug/L 04/07/17 10:17 95-95-404/06/17 14:0510.0 1
2,4,6-Trichlorophenol ND ug/L 04/07/17 10:17 88-06-204/06/17 14:0510.0 1
Surrogates
Nitrobenzene-d5 (S)71 %04/07/17 10:17 4165-60-004/06/17 14:0521-110 1
2-Fluorobiphenyl (S)78 %04/07/17 10:17 321-60-804/06/17 14:0527-110 1
Terphenyl-d14 (S)58 %04/07/17 10:17 1718-51-004/06/17 14:0531-107 1
Phenol-d6 (S)25 %04/07/17 10:17 13127-88-304/06/17 14:0510-110 1
2-Fluorophenol (S)39 %04/07/17 10:17 367-12-404/06/17 14:0512-110 1
2,4,6-Tribromophenol (S)92 %04/07/17 10:17 118-79-604/06/17 14:0527-110 1
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 04/05/17 23:03 67-64-125.0 1
Benzene ND ug/L 04/05/17 23:03 71-43-21.0 1
Bromobenzene ND ug/L 04/05/17 23:03 108-86-11.0 1
Bromochloromethane ND ug/L 04/05/17 23:03 74-97-51.0 1
Bromodichloromethane ND ug/L 04/05/17 23:03 75-27-41.0 1
Bromoform ND ug/L 04/05/17 23:03 75-25-21.0 1
Bromomethane ND ug/L 04/05/17 23:03 74-83-92.0 1
2-Butanone (MEK)ND ug/L 04/05/17 23:03 78-93-35.0 1
Carbon tetrachloride ND ug/L 04/05/17 23:03 56-23-51.0 1
Chlorobenzene ND ug/L 04/05/17 23:03 108-90-71.0 1
Chloroethane ND ug/L 04/05/17 23:03 75-00-31.0 1
Chloroform ND ug/L 04/05/17 23:03 67-66-31.0 1
Chloromethane ND ug/L 04/05/17 23:03 74-87-31.0 1
2-Chlorotoluene ND ug/L 04/05/17 23:03 95-49-81.0 1
4-Chlorotoluene ND ug/L 04/05/17 23:03 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 04/05/17 23:03 96-12-82.0 1
Dibromochloromethane ND ug/L 04/05/17 23:03 124-48-11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/10/2017 10:46 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92335793
MIRANDA ROAD
Sample:TMW-1 Lab ID:92335793001 Collected:04/04/17 13:20 Received:04/04/17 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
1,2-Dibromoethane (EDB)ND ug/L 04/05/17 23:03 106-93-41.0 1
Dibromomethane ND ug/L 04/05/17 23:03 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 04/05/17 23:03 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 04/05/17 23:03 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 04/05/17 23:03 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 04/05/17 23:03 75-71-81.0 1
1,1-Dichloroethane ND ug/L 04/05/17 23:03 75-34-31.0 1
1,2-Dichloroethane ND ug/L 04/05/17 23:03 107-06-21.0 1
1,1-Dichloroethene ND ug/L 04/05/17 23:03 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 04/05/17 23:03 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 04/05/17 23:03 156-60-51.0 1
1,2-Dichloropropane ND ug/L 04/05/17 23:03 78-87-51.0 1
1,3-Dichloropropane ND ug/L 04/05/17 23:03 142-28-91.0 1
2,2-Dichloropropane ND ug/L 04/05/17 23:03 594-20-71.0 1
1,1-Dichloropropene ND ug/L 04/05/17 23:03 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 04/05/17 23:03 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 04/05/17 23:03 10061-02-61.0 1
Diisopropyl ether ND ug/L 04/05/17 23:03 108-20-31.0 1
Ethylbenzene ND ug/L 04/05/17 23:03 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 04/05/17 23:03 87-68-31.0 1
2-Hexanone ND ug/L 04/05/17 23:03 591-78-65.0 1
p-Isopropyltoluene ND ug/L 04/05/17 23:03 99-87-61.0 1
Methylene Chloride ND ug/L 04/05/17 23:03 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 04/05/17 23:03 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 04/05/17 23:03 1634-04-41.0 1
Naphthalene ND ug/L 04/05/17 23:03 91-20-31.0 1
Styrene ND ug/L 04/05/17 23:03 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 04/05/17 23:03 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 04/05/17 23:03 79-34-51.0 1
Tetrachloroethene ND ug/L 04/05/17 23:03 127-18-41.0 1
Toluene ND ug/L 04/05/17 23:03 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 04/05/17 23:03 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 04/05/17 23:03 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 04/05/17 23:03 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 04/05/17 23:03 79-00-51.0 1
Trichloroethene ND ug/L 04/05/17 23:03 79-01-61.0 1
Trichlorofluoromethane ND ug/L 04/05/17 23:03 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 04/05/17 23:03 96-18-41.0 1
Vinyl acetate ND ug/L 04/05/17 23:03 108-05-42.0 1
Vinyl chloride ND ug/L 04/05/17 23:03 75-01-41.0 1
Xylene (Total)ND ug/L 04/05/17 23:03 1330-20-71.0 1
m&p-Xylene ND ug/L 04/05/17 23:03 179601-23-12.0 1
o-Xylene ND ug/L 04/05/17 23:03 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)98 %04/05/17 23:03 460-00-470-130 1
1,2-Dichloroethane-d4 (S)92 %04/05/17 23:03 17060-07-070-130 1
Toluene-d8 (S)99 %04/05/17 23:03 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/10/2017 10:46 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92335793
MIRANDA ROAD
Sample:TMW-2 Lab ID:92335793002 Collected:04/04/17 13:55 Received:04/04/17 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 04/07/17 10:45 83-32-904/06/17 14:0510.0 1
Acenaphthylene ND ug/L 04/07/17 10:45 208-96-804/06/17 14:0510.0 1
Aniline ND ug/L 04/07/17 10:45 62-53-304/06/17 14:0510.0 1
Anthracene ND ug/L 04/07/17 10:45 120-12-704/06/17 14:0510.0 1
Benzo(a)anthracene ND ug/L 04/07/17 10:45 56-55-304/06/17 14:0510.0 1
Benzo(a)pyrene ND ug/L 04/07/17 10:45 50-32-804/06/17 14:0510.0 1
Benzo(b)fluoranthene ND ug/L 04/07/17 10:45 205-99-204/06/17 14:0510.0 1
Benzo(g,h,i)perylene ND ug/L 04/07/17 10:45 191-24-204/06/17 14:0510.0 1
Benzo(k)fluoranthene ND ug/L 04/07/17 10:45 207-08-904/06/17 14:0510.0 1
Benzoic Acid ND ug/L 04/07/17 10:45 65-85-004/06/17 14:0550.0 1
Benzyl alcohol ND ug/L 04/07/17 10:45 100-51-604/06/17 14:0520.0 1
4-Bromophenylphenyl ether ND ug/L 04/07/17 10:45 101-55-304/06/17 14:0510.0 1
Butylbenzylphthalate ND ug/L 04/07/17 10:45 85-68-704/06/17 14:0510.0 1
4-Chloro-3-methylphenol ND ug/L 04/07/17 10:45 59-50-704/06/17 14:0520.0 1
4-Chloroaniline ND ug/L 04/07/17 10:45 106-47-804/06/17 14:0520.0 1
bis(2-Chloroethoxy)methane ND ug/L 04/07/17 10:45 111-91-104/06/17 14:0510.0 1
bis(2-Chloroethyl) ether ND ug/L 04/07/17 10:45 111-44-404/06/17 14:0510.0 1
2-Chloronaphthalene ND ug/L 04/07/17 10:45 91-58-704/06/17 14:0510.0 1
2-Chlorophenol ND ug/L 04/07/17 10:45 95-57-804/06/17 14:0510.0 1
4-Chlorophenylphenyl ether ND ug/L 04/07/17 10:45 7005-72-304/06/17 14:0510.0 1
Chrysene ND ug/L 04/07/17 10:45 218-01-904/06/17 14:0510.0 1
Dibenz(a,h)anthracene ND ug/L 04/07/17 10:45 53-70-304/06/17 14:0510.0 1
Dibenzofuran ND ug/L 04/07/17 10:45 132-64-904/06/17 14:0510.0 1
1,2-Dichlorobenzene ND ug/L 04/07/17 10:45 95-50-104/06/17 14:0510.0 1
1,3-Dichlorobenzene ND ug/L 04/07/17 10:45 541-73-104/06/17 14:0510.0 1
1,4-Dichlorobenzene ND ug/L 04/07/17 10:45 106-46-704/06/17 14:0510.0 1
3,3'-Dichlorobenzidine ND ug/L 04/07/17 10:45 91-94-104/06/17 14:0520.0 1
2,4-Dichlorophenol ND ug/L 04/07/17 10:45 120-83-204/06/17 14:0510.0 1
Diethylphthalate ND ug/L 04/07/17 10:45 84-66-204/06/17 14:0510.0 1
2,4-Dimethylphenol ND ug/L 04/07/17 10:45 105-67-904/06/17 14:0510.0 1
Dimethylphthalate ND ug/L 04/07/17 10:45 131-11-304/06/17 14:0510.0 1
Di-n-butylphthalate ND ug/L 04/07/17 10:45 84-74-204/06/17 14:0510.0 1
4,6-Dinitro-2-methylphenol ND ug/L 04/07/17 10:45 534-52-104/06/17 14:0520.0 1
2,4-Dinitrophenol ND ug/L 04/07/17 10:45 51-28-504/06/17 14:0550.0 1
2,4-Dinitrotoluene ND ug/L 04/07/17 10:45 121-14-204/06/17 14:0510.0 1
2,6-Dinitrotoluene ND ug/L 04/07/17 10:45 606-20-204/06/17 14:0510.0 1
Di-n-octylphthalate ND ug/L 04/07/17 10:45 117-84-004/06/17 14:0510.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 04/07/17 10:45 117-81-704/06/17 14:056.0 1
Fluoranthene ND ug/L 04/07/17 10:45 206-44-004/06/17 14:0510.0 1
Fluorene ND ug/L 04/07/17 10:45 86-73-704/06/17 14:0510.0 1
Hexachloro-1,3-butadiene ND ug/L 04/07/17 10:45 87-68-304/06/17 14:0510.0 1
Hexachlorobenzene ND ug/L 04/07/17 10:45 118-74-104/06/17 14:0510.0 1
Hexachlorocyclopentadiene ND ug/L 04/07/17 10:45 77-47-404/06/17 14:0510.0 1
Hexachloroethane ND ug/L 04/07/17 10:45 67-72-104/06/17 14:0510.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 04/07/17 10:45 193-39-504/06/17 14:0510.0 1
Isophorone ND ug/L 04/07/17 10:45 78-59-104/06/17 14:0510.0 1
1-Methylnaphthalene ND ug/L 04/07/17 10:45 90-12-004/06/17 14:0510.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/10/2017 10:46 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92335793
MIRANDA ROAD
Sample:TMW-2 Lab ID:92335793002 Collected:04/04/17 13:55 Received:04/04/17 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2-Methylnaphthalene ND ug/L 04/07/17 10:45 91-57-604/06/17 14:0510.0 1
2-Methylphenol(o-Cresol)ND ug/L 04/07/17 10:45 95-48-704/06/17 14:0510.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 04/07/17 10:4504/06/17 14:0510.0 1
Naphthalene ND ug/L 04/07/17 10:45 91-20-304/06/17 14:0510.0 1
2-Nitroaniline ND ug/L 04/07/17 10:45 88-74-404/06/17 14:0550.0 1
3-Nitroaniline ND ug/L 04/07/17 10:45 99-09-204/06/17 14:0550.0 1
4-Nitroaniline ND ug/L 04/07/17 10:45 100-01-604/06/17 14:0520.0 1
Nitrobenzene ND ug/L 04/07/17 10:45 98-95-304/06/17 14:0510.0 1
2-Nitrophenol ND ug/L 04/07/17 10:45 88-75-504/06/17 14:0510.0 1
4-Nitrophenol ND ug/L 04/07/17 10:45 100-02-704/06/17 14:0550.0 1
N-Nitrosodimethylamine ND ug/L 04/07/17 10:45 62-75-904/06/17 14:0510.0 1
N-Nitroso-di-n-propylamine ND ug/L 04/07/17 10:45 621-64-704/06/17 14:0510.0 1
N-Nitrosodiphenylamine ND ug/L 04/07/17 10:45 86-30-604/06/17 14:0510.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 04/07/17 10:45 108-60-104/06/17 14:0510.0 1
Pentachlorophenol ND ug/L 04/07/17 10:45 87-86-504/06/17 14:0525.0 1
Phenanthrene ND ug/L 04/07/17 10:45 85-01-804/06/17 14:0510.0 1
Phenol ND ug/L 04/07/17 10:4504/06/17 14:0510.0 1
Pyrene ND ug/L 04/07/17 10:45 129-00-004/06/17 14:0510.0 1
1,2,4-Trichlorobenzene ND ug/L 04/07/17 10:45 120-82-104/06/17 14:0510.0 1
2,4,5-Trichlorophenol ND ug/L 04/07/17 10:45 95-95-404/06/17 14:0510.0 1
2,4,6-Trichlorophenol ND ug/L 04/07/17 10:45 88-06-204/06/17 14:0510.0 1
Surrogates
Nitrobenzene-d5 (S)71 %04/07/17 10:45 4165-60-004/06/17 14:0521-110 1
2-Fluorobiphenyl (S)74 %04/07/17 10:45 321-60-804/06/17 14:0527-110 1
Terphenyl-d14 (S)68 %04/07/17 10:45 1718-51-004/06/17 14:0531-107 1
Phenol-d6 (S)26 %04/07/17 10:45 13127-88-304/06/17 14:0510-110 1
2-Fluorophenol (S)36 %04/07/17 10:45 367-12-404/06/17 14:0512-110 1
2,4,6-Tribromophenol (S)85 %04/07/17 10:45 118-79-604/06/17 14:0527-110 1
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 04/05/17 23:21 67-64-125.0 1
Benzene ND ug/L 04/05/17 23:21 71-43-21.0 1
Bromobenzene ND ug/L 04/05/17 23:21 108-86-11.0 1
Bromochloromethane ND ug/L 04/05/17 23:21 74-97-51.0 1
Bromodichloromethane ND ug/L 04/05/17 23:21 75-27-41.0 1
Bromoform ND ug/L 04/05/17 23:21 75-25-21.0 1
Bromomethane ND ug/L 04/05/17 23:21 74-83-92.0 1
2-Butanone (MEK)ND ug/L 04/05/17 23:21 78-93-35.0 1
Carbon tetrachloride ND ug/L 04/05/17 23:21 56-23-51.0 1
Chlorobenzene ND ug/L 04/05/17 23:21 108-90-71.0 1
Chloroethane ND ug/L 04/05/17 23:21 75-00-31.0 1
Chloroform ND ug/L 04/05/17 23:21 67-66-31.0 1
Chloromethane ND ug/L 04/05/17 23:21 74-87-31.0 1
2-Chlorotoluene ND ug/L 04/05/17 23:21 95-49-81.0 1
4-Chlorotoluene ND ug/L 04/05/17 23:21 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 04/05/17 23:21 96-12-82.0 1
Dibromochloromethane ND ug/L 04/05/17 23:21 124-48-11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/10/2017 10:46 AM
Pace Analytical Services, LLC
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Page 8 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92335793
MIRANDA ROAD
Sample:TMW-2 Lab ID:92335793002 Collected:04/04/17 13:55 Received:04/04/17 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
1,2-Dibromoethane (EDB)ND ug/L 04/05/17 23:21 106-93-41.0 1
Dibromomethane ND ug/L 04/05/17 23:21 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 04/05/17 23:21 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 04/05/17 23:21 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 04/05/17 23:21 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 04/05/17 23:21 75-71-81.0 1
1,1-Dichloroethane ND ug/L 04/05/17 23:21 75-34-31.0 1
1,2-Dichloroethane ND ug/L 04/05/17 23:21 107-06-21.0 1
1,1-Dichloroethene ND ug/L 04/05/17 23:21 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 04/05/17 23:21 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 04/05/17 23:21 156-60-51.0 1
1,2-Dichloropropane ND ug/L 04/05/17 23:21 78-87-51.0 1
1,3-Dichloropropane ND ug/L 04/05/17 23:21 142-28-91.0 1
2,2-Dichloropropane ND ug/L 04/05/17 23:21 594-20-71.0 1
1,1-Dichloropropene ND ug/L 04/05/17 23:21 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 04/05/17 23:21 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 04/05/17 23:21 10061-02-61.0 1
Diisopropyl ether ND ug/L 04/05/17 23:21 108-20-31.0 1
Ethylbenzene ND ug/L 04/05/17 23:21 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 04/05/17 23:21 87-68-31.0 1
2-Hexanone ND ug/L 04/05/17 23:21 591-78-65.0 1
p-Isopropyltoluene ND ug/L 04/05/17 23:21 99-87-61.0 1
Methylene Chloride ND ug/L 04/05/17 23:21 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 04/05/17 23:21 108-10-15.0 1
Methyl-tert-butyl ether 2.4 ug/L 04/05/17 23:21 1634-04-41.0 1
Naphthalene ND ug/L 04/05/17 23:21 91-20-31.0 1
Styrene ND ug/L 04/05/17 23:21 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 04/05/17 23:21 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 04/05/17 23:21 79-34-51.0 1
Tetrachloroethene ND ug/L 04/05/17 23:21 127-18-41.0 1
Toluene ND ug/L 04/05/17 23:21 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 04/05/17 23:21 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 04/05/17 23:21 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 04/05/17 23:21 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 04/05/17 23:21 79-00-51.0 1
Trichloroethene ND ug/L 04/05/17 23:21 79-01-61.0 1
Trichlorofluoromethane ND ug/L 04/05/17 23:21 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 04/05/17 23:21 96-18-41.0 1
Vinyl acetate ND ug/L 04/05/17 23:21 108-05-42.0 1
Vinyl chloride ND ug/L 04/05/17 23:21 75-01-41.0 1
Xylene (Total)ND ug/L 04/05/17 23:21 1330-20-71.0 1
m&p-Xylene ND ug/L 04/05/17 23:21 179601-23-12.0 1
o-Xylene ND ug/L 04/05/17 23:21 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)101 %04/05/17 23:21 460-00-470-130 1
1,2-Dichloroethane-d4 (S)92 %04/05/17 23:21 17060-07-070-130 1
Toluene-d8 (S)100 %04/05/17 23:21 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/10/2017 10:46 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92335793
MIRANDA ROAD
Sample:TMW-3 Lab ID:92335793003 Collected:04/04/17 14:30 Received:04/04/17 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 04/07/17 11:13 83-32-904/06/17 14:0510.0 1
Acenaphthylene ND ug/L 04/07/17 11:13 208-96-804/06/17 14:0510.0 1
Aniline ND ug/L 04/07/17 11:13 62-53-304/06/17 14:0510.0 1
Anthracene ND ug/L 04/07/17 11:13 120-12-704/06/17 14:0510.0 1
Benzo(a)anthracene ND ug/L 04/07/17 11:13 56-55-304/06/17 14:0510.0 1
Benzo(a)pyrene ND ug/L 04/07/17 11:13 50-32-804/06/17 14:0510.0 1
Benzo(b)fluoranthene ND ug/L 04/07/17 11:13 205-99-204/06/17 14:0510.0 1
Benzo(g,h,i)perylene ND ug/L 04/07/17 11:13 191-24-204/06/17 14:0510.0 1
Benzo(k)fluoranthene ND ug/L 04/07/17 11:13 207-08-904/06/17 14:0510.0 1
Benzoic Acid ND ug/L 04/07/17 11:13 65-85-004/06/17 14:0550.0 1
Benzyl alcohol ND ug/L 04/07/17 11:13 100-51-604/06/17 14:0520.0 1
4-Bromophenylphenyl ether ND ug/L 04/07/17 11:13 101-55-304/06/17 14:0510.0 1
Butylbenzylphthalate ND ug/L 04/07/17 11:13 85-68-704/06/17 14:0510.0 1
4-Chloro-3-methylphenol ND ug/L 04/07/17 11:13 59-50-704/06/17 14:0520.0 1
4-Chloroaniline ND ug/L 04/07/17 11:13 106-47-804/06/17 14:0520.0 1
bis(2-Chloroethoxy)methane ND ug/L 04/07/17 11:13 111-91-104/06/17 14:0510.0 1
bis(2-Chloroethyl) ether ND ug/L 04/07/17 11:13 111-44-404/06/17 14:0510.0 1
2-Chloronaphthalene ND ug/L 04/07/17 11:13 91-58-704/06/17 14:0510.0 1
2-Chlorophenol ND ug/L 04/07/17 11:13 95-57-804/06/17 14:0510.0 1
4-Chlorophenylphenyl ether ND ug/L 04/07/17 11:13 7005-72-304/06/17 14:0510.0 1
Chrysene ND ug/L 04/07/17 11:13 218-01-904/06/17 14:0510.0 1
Dibenz(a,h)anthracene ND ug/L 04/07/17 11:13 53-70-304/06/17 14:0510.0 1
Dibenzofuran ND ug/L 04/07/17 11:13 132-64-904/06/17 14:0510.0 1
1,2-Dichlorobenzene ND ug/L 04/07/17 11:13 95-50-104/06/17 14:0510.0 1
1,3-Dichlorobenzene ND ug/L 04/07/17 11:13 541-73-104/06/17 14:0510.0 1
1,4-Dichlorobenzene ND ug/L 04/07/17 11:13 106-46-704/06/17 14:0510.0 1
3,3'-Dichlorobenzidine ND ug/L 04/07/17 11:13 91-94-104/06/17 14:0520.0 1
2,4-Dichlorophenol ND ug/L 04/07/17 11:13 120-83-204/06/17 14:0510.0 1
Diethylphthalate ND ug/L 04/07/17 11:13 84-66-204/06/17 14:0510.0 1
2,4-Dimethylphenol ND ug/L 04/07/17 11:13 105-67-904/06/17 14:0510.0 1
Dimethylphthalate ND ug/L 04/07/17 11:13 131-11-304/06/17 14:0510.0 1
Di-n-butylphthalate ND ug/L 04/07/17 11:13 84-74-204/06/17 14:0510.0 1
4,6-Dinitro-2-methylphenol ND ug/L 04/07/17 11:13 534-52-104/06/17 14:0520.0 1
2,4-Dinitrophenol ND ug/L 04/07/17 11:13 51-28-504/06/17 14:0550.0 1
2,4-Dinitrotoluene ND ug/L 04/07/17 11:13 121-14-204/06/17 14:0510.0 1
2,6-Dinitrotoluene ND ug/L 04/07/17 11:13 606-20-204/06/17 14:0510.0 1
Di-n-octylphthalate ND ug/L 04/07/17 11:13 117-84-004/06/17 14:0510.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 04/07/17 11:13 117-81-704/06/17 14:056.0 1
Fluoranthene ND ug/L 04/07/17 11:13 206-44-004/06/17 14:0510.0 1
Fluorene ND ug/L 04/07/17 11:13 86-73-704/06/17 14:0510.0 1
Hexachloro-1,3-butadiene ND ug/L 04/07/17 11:13 87-68-304/06/17 14:0510.0 1
Hexachlorobenzene ND ug/L 04/07/17 11:13 118-74-104/06/17 14:0510.0 1
Hexachlorocyclopentadiene ND ug/L 04/07/17 11:13 77-47-404/06/17 14:0510.0 1
Hexachloroethane ND ug/L 04/07/17 11:13 67-72-104/06/17 14:0510.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 04/07/17 11:13 193-39-504/06/17 14:0510.0 1
Isophorone ND ug/L 04/07/17 11:13 78-59-104/06/17 14:0510.0 1
1-Methylnaphthalene ND ug/L 04/07/17 11:13 90-12-004/06/17 14:0510.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/10/2017 10:46 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92335793
MIRANDA ROAD
Sample:TMW-3 Lab ID:92335793003 Collected:04/04/17 14:30 Received:04/04/17 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
2-Methylnaphthalene ND ug/L 04/07/17 11:13 91-57-604/06/17 14:0510.0 1
2-Methylphenol(o-Cresol)ND ug/L 04/07/17 11:13 95-48-704/06/17 14:0510.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 04/07/17 11:1304/06/17 14:0510.0 1
Naphthalene ND ug/L 04/07/17 11:13 91-20-304/06/17 14:0510.0 1
2-Nitroaniline ND ug/L 04/07/17 11:13 88-74-404/06/17 14:0550.0 1
3-Nitroaniline ND ug/L 04/07/17 11:13 99-09-204/06/17 14:0550.0 1
4-Nitroaniline ND ug/L 04/07/17 11:13 100-01-604/06/17 14:0520.0 1
Nitrobenzene ND ug/L 04/07/17 11:13 98-95-304/06/17 14:0510.0 1
2-Nitrophenol ND ug/L 04/07/17 11:13 88-75-504/06/17 14:0510.0 1
4-Nitrophenol ND ug/L 04/07/17 11:13 100-02-704/06/17 14:0550.0 1
N-Nitrosodimethylamine ND ug/L 04/07/17 11:13 62-75-904/06/17 14:0510.0 1
N-Nitroso-di-n-propylamine ND ug/L 04/07/17 11:13 621-64-704/06/17 14:0510.0 1
N-Nitrosodiphenylamine ND ug/L 04/07/17 11:13 86-30-604/06/17 14:0510.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 04/07/17 11:13 108-60-104/06/17 14:0510.0 1
Pentachlorophenol ND ug/L 04/07/17 11:13 87-86-504/06/17 14:0525.0 1
Phenanthrene ND ug/L 04/07/17 11:13 85-01-804/06/17 14:0510.0 1
Phenol ND ug/L 04/07/17 11:1304/06/17 14:0510.0 1
Pyrene ND ug/L 04/07/17 11:13 129-00-004/06/17 14:0510.0 1
1,2,4-Trichlorobenzene ND ug/L 04/07/17 11:13 120-82-104/06/17 14:0510.0 1
2,4,5-Trichlorophenol ND ug/L 04/07/17 11:13 95-95-404/06/17 14:0510.0 1
2,4,6-Trichlorophenol ND ug/L 04/07/17 11:13 88-06-204/06/17 14:0510.0 1
Surrogates
Nitrobenzene-d5 (S)76 %04/07/17 11:13 4165-60-004/06/17 14:0521-110 1
2-Fluorobiphenyl (S)77 %04/07/17 11:13 321-60-804/06/17 14:0527-110 1
Terphenyl-d14 (S)83 %04/07/17 11:13 1718-51-004/06/17 14:0531-107 1
Phenol-d6 (S)31 %04/07/17 11:13 13127-88-304/06/17 14:0510-110 1
2-Fluorophenol (S)43 %04/07/17 11:13 367-12-404/06/17 14:0512-110 1
2,4,6-Tribromophenol (S)89 %04/07/17 11:13 118-79-604/06/17 14:0527-110 1
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 04/05/17 23:38 67-64-125.0 1
Benzene ND ug/L 04/05/17 23:38 71-43-21.0 1
Bromobenzene ND ug/L 04/05/17 23:38 108-86-11.0 1
Bromochloromethane ND ug/L 04/05/17 23:38 74-97-51.0 1
Bromodichloromethane ND ug/L 04/05/17 23:38 75-27-41.0 1
Bromoform ND ug/L 04/05/17 23:38 75-25-21.0 1
Bromomethane ND ug/L 04/05/17 23:38 74-83-92.0 1
2-Butanone (MEK)ND ug/L 04/05/17 23:38 78-93-35.0 1
Carbon tetrachloride ND ug/L 04/05/17 23:38 56-23-51.0 1
Chlorobenzene ND ug/L 04/05/17 23:38 108-90-71.0 1
Chloroethane ND ug/L 04/05/17 23:38 75-00-31.0 1
Chloroform ND ug/L 04/05/17 23:38 67-66-31.0 1
Chloromethane ND ug/L 04/05/17 23:38 74-87-31.0 1
2-Chlorotoluene ND ug/L 04/05/17 23:38 95-49-81.0 1
4-Chlorotoluene ND ug/L 04/05/17 23:38 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 04/05/17 23:38 96-12-82.0 1
Dibromochloromethane ND ug/L 04/05/17 23:38 124-48-11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/10/2017 10:46 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 29
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92335793
MIRANDA ROAD
Sample:TMW-3 Lab ID:92335793003 Collected:04/04/17 14:30 Received:04/04/17 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260 MSV Low Level
1,2-Dibromoethane (EDB)ND ug/L 04/05/17 23:38 106-93-41.0 1
Dibromomethane ND ug/L 04/05/17 23:38 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 04/05/17 23:38 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 04/05/17 23:38 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 04/05/17 23:38 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 04/05/17 23:38 75-71-81.0 1
1,1-Dichloroethane ND ug/L 04/05/17 23:38 75-34-31.0 1
1,2-Dichloroethane 46.5 ug/L 04/05/17 23:38 107-06-21.0 1
1,1-Dichloroethene ND ug/L 04/05/17 23:38 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 04/05/17 23:38 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 04/05/17 23:38 156-60-51.0 1
1,2-Dichloropropane ND ug/L 04/05/17 23:38 78-87-51.0 1
1,3-Dichloropropane ND ug/L 04/05/17 23:38 142-28-91.0 1
2,2-Dichloropropane ND ug/L 04/05/17 23:38 594-20-71.0 1
1,1-Dichloropropene ND ug/L 04/05/17 23:38 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 04/05/17 23:38 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 04/05/17 23:38 10061-02-61.0 1
Diisopropyl ether ND ug/L 04/05/17 23:38 108-20-31.0 1
Ethylbenzene ND ug/L 04/05/17 23:38 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 04/05/17 23:38 87-68-31.0 1
2-Hexanone ND ug/L 04/05/17 23:38 591-78-65.0 1
p-Isopropyltoluene ND ug/L 04/05/17 23:38 99-87-61.0 1
Methylene Chloride ND ug/L 04/05/17 23:38 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 04/05/17 23:38 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 04/05/17 23:38 1634-04-41.0 1
Naphthalene ND ug/L 04/05/17 23:38 91-20-31.0 1
Styrene ND ug/L 04/05/17 23:38 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 04/05/17 23:38 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 04/05/17 23:38 79-34-51.0 1
Tetrachloroethene ND ug/L 04/05/17 23:38 127-18-41.0 1
Toluene ND ug/L 04/05/17 23:38 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 04/05/17 23:38 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 04/05/17 23:38 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 04/05/17 23:38 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 04/05/17 23:38 79-00-51.0 1
Trichloroethene ND ug/L 04/05/17 23:38 79-01-61.0 1
Trichlorofluoromethane ND ug/L 04/05/17 23:38 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 04/05/17 23:38 96-18-41.0 1
Vinyl acetate ND ug/L 04/05/17 23:38 108-05-42.0 1
Vinyl chloride ND ug/L 04/05/17 23:38 75-01-41.0 1
Xylene (Total)ND ug/L 04/05/17 23:38 1330-20-71.0 1
m&p-Xylene ND ug/L 04/05/17 23:38 179601-23-12.0 1
o-Xylene ND ug/L 04/05/17 23:38 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)97 %04/05/17 23:38 460-00-470-130 1
1,2-Dichloroethane-d4 (S)94 %04/05/17 23:38 17060-07-070-130 1
Toluene-d8 (S)100 %04/05/17 23:38 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/10/2017 10:46 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92335793
MIRANDA ROAD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
355323
EPA 8260
EPA 8260
8260 MSV Low Level
Associated Lab Samples:92335793001, 92335793002, 92335793003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1971008
Associated Lab Samples:92335793001, 92335793002, 92335793003
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 04/05/17 17:32
1,1,1-Trichloroethane ug/L ND 1.0 04/05/17 17:32
1,1,2,2-Tetrachloroethane ug/L ND 1.0 04/05/17 17:32
1,1,2-Trichloroethane ug/L ND 1.0 04/05/17 17:32
1,1-Dichloroethane ug/L ND 1.0 04/05/17 17:32
1,1-Dichloroethene ug/L ND 1.0 04/05/17 17:32
1,1-Dichloropropene ug/L ND 1.0 04/05/17 17:32
1,2,3-Trichlorobenzene ug/L ND 1.0 04/05/17 17:32
1,2,3-Trichloropropane ug/L ND 1.0 04/05/17 17:32
1,2,4-Trichlorobenzene ug/L ND 1.0 04/05/17 17:32
1,2-Dibromo-3-chloropropane ug/L ND 2.0 04/05/17 17:32
1,2-Dibromoethane (EDB)ug/L ND 1.0 04/05/17 17:32
1,2-Dichlorobenzene ug/L ND 1.0 04/05/17 17:32
1,2-Dichloroethane ug/L ND 1.0 04/05/17 17:32
1,2-Dichloropropane ug/L ND 1.0 04/05/17 17:32
1,3-Dichlorobenzene ug/L ND 1.0 04/05/17 17:32
1,3-Dichloropropane ug/L ND 1.0 04/05/17 17:32
1,4-Dichlorobenzene ug/L ND 1.0 04/05/17 17:32
2,2-Dichloropropane ug/L ND 1.0 04/05/17 17:32
2-Butanone (MEK)ug/L ND 5.0 04/05/17 17:32
2-Chlorotoluene ug/L ND 1.0 04/05/17 17:32
2-Hexanone ug/L ND 5.0 04/05/17 17:32
4-Chlorotoluene ug/L ND 1.0 04/05/17 17:32
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 04/05/17 17:32
Acetone ug/L ND 25.0 04/05/17 17:32
Benzene ug/L ND 1.0 04/05/17 17:32
Bromobenzene ug/L ND 1.0 04/05/17 17:32
Bromochloromethane ug/L ND 1.0 04/05/17 17:32
Bromodichloromethane ug/L ND 1.0 04/05/17 17:32
Bromoform ug/L ND 1.0 04/05/17 17:32
Bromomethane ug/L ND 2.0 04/05/17 17:32
Carbon tetrachloride ug/L ND 1.0 04/05/17 17:32
Chlorobenzene ug/L ND 1.0 04/05/17 17:32
Chloroethane ug/L ND 1.0 04/05/17 17:32
Chloroform ug/L ND 1.0 04/05/17 17:32
Chloromethane ug/L ND 1.0 04/05/17 17:32
cis-1,2-Dichloroethene ug/L ND 1.0 04/05/17 17:32
cis-1,3-Dichloropropene ug/L ND 1.0 04/05/17 17:32
Dibromochloromethane ug/L ND 1.0 04/05/17 17:32
Dibromomethane ug/L ND 1.0 04/05/17 17:32
Dichlorodifluoromethane ug/L ND 1.0 04/05/17 17:32
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92335793
MIRANDA ROAD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1971008
Associated Lab Samples:92335793001, 92335793002, 92335793003
Matrix:Water
Analyzed
Diisopropyl ether ug/L ND 1.0 04/05/17 17:32
Ethylbenzene ug/L ND 1.0 04/05/17 17:32
Hexachloro-1,3-butadiene ug/L ND 1.0 04/05/17 17:32
m&p-Xylene ug/L ND 2.0 04/05/17 17:32
Methyl-tert-butyl ether ug/L ND 1.0 04/05/17 17:32
Methylene Chloride ug/L ND 2.0 04/05/17 17:32
Naphthalene ug/L ND 1.0 04/05/17 17:32
o-Xylene ug/L ND 1.0 04/05/17 17:32
p-Isopropyltoluene ug/L ND 1.0 04/05/17 17:32
Styrene ug/L ND 1.0 04/05/17 17:32
Tetrachloroethene ug/L ND 1.0 04/05/17 17:32
Toluene ug/L ND 1.0 04/05/17 17:32
trans-1,2-Dichloroethene ug/L ND 1.0 04/05/17 17:32
trans-1,3-Dichloropropene ug/L ND 1.0 04/05/17 17:32
Trichloroethene ug/L ND 1.0 04/05/17 17:32
Trichlorofluoromethane ug/L ND 1.0 04/05/17 17:32
Vinyl acetate ug/L ND 2.0 04/05/17 17:32
Vinyl chloride ug/L ND 1.0 04/05/17 17:32
Xylene (Total)ug/L ND 1.0 04/05/17 17:32
1,2-Dichloroethane-d4 (S)%91 70-130 04/05/17 17:32
4-Bromofluorobenzene (S)%98 70-130 04/05/17 17:32
Toluene-d8 (S)%101 70-130 04/05/17 17:32
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1971009LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 51.350 103 70-130
1,1,1-Trichloroethane ug/L 49.950 100 70-130
1,1,2,2-Tetrachloroethane ug/L 53.550 107 70-130
1,1,2-Trichloroethane ug/L 52.350 105 70-130
1,1-Dichloroethane ug/L 47.050 94 70-130
1,1-Dichloroethene ug/L 50.450 101 70-132
1,1-Dichloropropene ug/L 48.950 98 70-130
1,2,3-Trichlorobenzene ug/L 54.950 110 70-135
1,2,3-Trichloropropane ug/L 55.550 111 70-130
1,2,4-Trichlorobenzene ug/L 55.150 110 70-134
1,2-Dibromo-3-chloropropane ug/L 53.250 106 70-130
1,2-Dibromoethane (EDB)ug/L 56.950 114 70-130
1,2-Dichlorobenzene ug/L 54.750 109 70-130
1,2-Dichloroethane ug/L 46.350 93 70-130
1,2-Dichloropropane ug/L 52.250 104 70-130
1,3-Dichlorobenzene ug/L 54.450 109 70-130
1,3-Dichloropropane ug/L 56.450 113 70-130
1,4-Dichlorobenzene ug/L 54.150 108 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/10/2017 10:46 AM
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Page 14 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92335793
MIRANDA ROAD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1971009LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 49.150 98 58-145
2-Butanone (MEK)ug/L 109100 109 70-145
2-Chlorotoluene ug/L 54.650 109 70-130
2-Hexanone ug/L 120100 120 70-144
4-Chlorotoluene ug/L 54.350 109 70-130
4-Methyl-2-pentanone (MIBK)ug/L 111100 111 70-140
Acetone ug/L 114100 114 50-175
Benzene ug/L 52.450 105 70-130
Bromobenzene ug/L 53.950 108 70-130
Bromochloromethane ug/L 48.050 96 70-130
Bromodichloromethane ug/L 55.150 110 70-130
Bromoform ug/L 46.850 94 70-130
Bromomethane ug/L 52.650 105 54-130
Carbon tetrachloride ug/L 55.850 112 70-132
Chlorobenzene ug/L 54.950 110 70-130
Chloroethane ug/L 43.650 87 64-134
Chloroform ug/L 48.450 97 70-130
Chloromethane ug/L 50.650 101 64-130
cis-1,2-Dichloroethene ug/L 45.950 92 70-131
cis-1,3-Dichloropropene ug/L 53.050 106 70-130
Dibromochloromethane ug/L 50.950 102 70-130
Dibromomethane ug/L 54.250 108 70-131
Dichlorodifluoromethane ug/L 39.950 80 56-130
Diisopropyl ether ug/L 50.150 100 70-130
Ethylbenzene ug/L 52.950 106 70-130
Hexachloro-1,3-butadiene ug/L 54.750 109 70-130
m&p-Xylene ug/L 106100 106 70-130
Methyl-tert-butyl ether ug/L 48.950 98 70-130
Methylene Chloride ug/L 49.150 98 63-130
Naphthalene ug/L 54.050 108 70-138
o-Xylene ug/L 52.550 105 70-130
p-Isopropyltoluene ug/L 51.950 104 70-130
Styrene ug/L 53.750 107 70-130
Tetrachloroethene ug/L 54.350 109 70-130
Toluene ug/L 51.150 102 70-130
trans-1,2-Dichloroethene ug/L 48.750 97 70-130
trans-1,3-Dichloropropene ug/L 53.050 106 70-132
Trichloroethene ug/L 54.050 108 70-130
Trichlorofluoromethane ug/L 51.250 102 62-133
Vinyl acetate ug/L 105100 105 66-157
Vinyl chloride ug/L 38.250 76 50-150
Xylene (Total)ug/L 159150 106 70-130
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/10/2017 10:46 AM
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Page 15 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92335793
MIRANDA ROAD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1971010MATRIX SPIKE SAMPLE:
MSSpike
Result
92335641016
1,1,1,2-Tetrachloroethane ug/L 20.820 104 70-130ND
1,1,1-Trichloroethane ug/L 20.720 103 70-130ND
1,1,2,2-Tetrachloroethane ug/L 21.420 107 70-130ND
1,1,2-Trichloroethane ug/L 21.120 106 70-130ND
1,1-Dichloroethane ug/L 19.320 97 70-130ND
1,1-Dichloroethene ug/L 21.720 108 70-166ND
1,1-Dichloropropene ug/L 19.820 99 70-130ND
1,2,3-Trichlorobenzene ug/L 21.220 106 70-130ND
1,2,3-Trichloropropane ug/L 22.320 112 70-130ND
1,2,4-Trichlorobenzene ug/L 20.820 104 70-130ND
1,2-Dibromo-3-chloropropane ug/L 21.120 105 70-130ND
1,2-Dibromoethane (EDB)ug/L 22.020 110 70-130ND
1,2-Dichlorobenzene ug/L 21.820 109 70-130ND
1,2-Dichloroethane ug/L 18.420 92 70-130ND
1,2-Dichloropropane ug/L 20.720 103 70-130ND
1,3-Dichlorobenzene ug/L 22.020 110 70-130ND
1,3-Dichloropropane ug/L 21.920 110 70-130ND
1,4-Dichlorobenzene ug/L 21.420 106 70-130ND
2,2-Dichloropropane ug/L 17.620 88 70-130ND
2-Butanone (MEK)ug/L 42.940 107 70-130ND
2-Chlorotoluene ug/L 22.420 112 70-130ND
2-Hexanone ug/L 47.640 119 70-130ND
4-Chlorotoluene ug/L 22.020 110 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 43.640 109 70-130ND
Acetone ug/L 46.140 115 70-130ND
Benzene ug/L 21.320 107 70-148ND
Bromobenzene ug/L 21.520 107 70-130ND
Bromochloromethane ug/L 20.520 103 70-130ND
Bromodichloromethane ug/L 21.920 110 70-130ND
Bromoform ug/L 18.620 93 70-130ND
Bromomethane ug/L 17.820 89 70-130ND
Carbon tetrachloride ug/L 23.320 116 70-130ND
Chlorobenzene ug/L 22.520 112 70-146ND
Chloroethane ug/L 18.420 92 70-130ND
Chloroform ug/L 18.620 93 70-130ND
Chloromethane ug/L 22.120 110 70-130ND
cis-1,2-Dichloroethene ug/L 19.020 95 70-130ND
cis-1,3-Dichloropropene ug/L 19.520 97 70-130ND
Dibromochloromethane ug/L 20.120 101 70-130ND
Dibromomethane ug/L 21.620 108 70-130ND
Dichlorodifluoromethane ug/L 18.020 90 70-130ND
Diisopropyl ether ug/L 20.020 100 70-130ND
Ethylbenzene ug/L 22.620 113 70-130ND
Hexachloro-1,3-butadiene ug/L 22.120 111 70-130ND
m&p-Xylene ug/L 44.840 112 70-130ND
Methyl-tert-butyl ether ug/L 19.520 94 70-1300.00075J mg/L
Methylene Chloride ug/L 19.620 98 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/10/2017 10:46 AM
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Page 16 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92335793
MIRANDA ROAD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1971010MATRIX SPIKE SAMPLE:
MSSpike
Result
92335641016
Naphthalene ug/L 20.520 102 70-130ND
o-Xylene ug/L 22.120 111 70-130ND
p-Isopropyltoluene ug/L 20.820 104 70-130ND
Styrene ug/L 21.320 106 70-130ND
Tetrachloroethene ug/L 22.420 112 70-130ND
Toluene ug/L 22.020 110 70-155ND
trans-1,2-Dichloroethene ug/L 19.820 99 70-130ND
trans-1,3-Dichloropropene ug/L 19.920 100 70-130ND
Trichloroethene ug/L 22.720 114 69-151ND
Trichlorofluoromethane ug/L 22.820 114 70-130ND
Vinyl acetate ug/L 33.340 83 70-130ND
Vinyl chloride ug/L 16.820 84 70-130ND
1,2-Dichloroethane-d4 (S)%93 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92335775001
1971011SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L NDND
1,1,1-Trichloroethane ug/L NDND
1,1,2,2-Tetrachloroethane ug/L NDND
1,1,2-Trichloroethane ug/L NDND
1,1-Dichloroethane ug/L NDND
1,1-Dichloroethene ug/L NDND
1,1-Dichloropropene ug/L NDND
1,2,3-Trichlorobenzene ug/L NDND
1,2,3-Trichloropropane ug/L NDND
1,2,4-Trichlorobenzene ug/L NDND
1,2-Dibromo-3-chloropropane ug/L NDND
1,2-Dibromoethane (EDB)ug/L NDND
1,2-Dichlorobenzene ug/L NDND
1,2-Dichloroethane ug/L NDND
1,2-Dichloropropane ug/L NDND
1,3-Dichlorobenzene ug/L NDND
1,3-Dichloropropane ug/L NDND
1,4-Dichlorobenzene ug/L NDND
2,2-Dichloropropane ug/L NDND
2-Butanone (MEK)ug/L NDND
2-Chlorotoluene ug/L NDND
2-Hexanone ug/L NDND
4-Chlorotoluene ug/L NDND
4-Methyl-2-pentanone (MIBK)ug/L NDND
Acetone ug/L NDND
Benzene ug/L NDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/10/2017 10:46 AM
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[phone]
Page 17 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92335793
MIRANDA ROAD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92335775001
1971011SAMPLE DUPLICATE:
Bromobenzene ug/L NDND
Bromochloromethane ug/L NDND
Bromodichloromethane ug/L NDND
Bromoform ug/L NDND
Bromomethane ug/L NDND
Carbon tetrachloride ug/L NDND
Chlorobenzene ug/L NDND
Chloroethane ug/L NDND
Chloroform ug/L NDND
Chloromethane ug/L NDND
cis-1,2-Dichloroethene ug/L NDND
cis-1,3-Dichloropropene ug/L NDND
Dibromochloromethane ug/L NDND
Dibromomethane ug/L NDND
Dichlorodifluoromethane ug/L NDND
Diisopropyl ether ug/L NDND
Ethylbenzene ug/L NDND
Hexachloro-1,3-butadiene ug/L NDND
m&p-Xylene ug/L NDND
Methyl-tert-butyl ether ug/L NDND
Methylene Chloride ug/L NDND
Naphthalene ug/L NDND
o-Xylene ug/L NDND
p-Isopropyltoluene ug/L NDND
Styrene ug/L NDND
Tetrachloroethene ug/L NDND
Toluene ug/L NDND
trans-1,2-Dichloroethene ug/L NDND
trans-1,3-Dichloropropene ug/L NDND
Trichloroethene ug/L NDND
Trichlorofluoromethane ug/L NDND
Vinyl acetate ug/L NDND
Vinyl chloride ug/L NDND
Xylene (Total)ug/L NDND
1,2-Dichloroethane-d4 (S)%92 193
4-Bromofluorobenzene (S)%100 199
Toluene-d8 (S)%101 0100
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/10/2017 10:46 AM
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Page 18 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92335793
MIRANDA ROAD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
355594
EPA 3510
EPA 8270
8270 Water MSSV
Associated Lab Samples:92335793001, 92335793002, 92335793003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1972638
Associated Lab Samples:92335793001, 92335793002, 92335793003
Matrix:Water
Analyzed
1,2,4-Trichlorobenzene ug/L ND 10.0 04/07/17 08:53
1,2-Dichlorobenzene ug/L ND 10.0 04/07/17 08:53
1,3-Dichlorobenzene ug/L ND 10.0 04/07/17 08:53
1,4-Dichlorobenzene ug/L ND 10.0 04/07/17 08:53
1-Methylnaphthalene ug/L ND 10.0 04/07/17 08:53
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 04/07/17 08:53
2,4,5-Trichlorophenol ug/L ND 10.0 04/07/17 08:53
2,4,6-Trichlorophenol ug/L ND 10.0 04/07/17 08:53
2,4-Dichlorophenol ug/L ND 10.0 04/07/17 08:53
2,4-Dimethylphenol ug/L ND 10.0 04/07/17 08:53
2,4-Dinitrophenol ug/L ND 50.0 04/07/17 08:53
2,4-Dinitrotoluene ug/L ND 10.0 04/07/17 08:53
2,6-Dinitrotoluene ug/L ND 10.0 04/07/17 08:53
2-Chloronaphthalene ug/L ND 10.0 04/07/17 08:53
2-Chlorophenol ug/L ND 10.0 04/07/17 08:53
2-Methylnaphthalene ug/L ND 10.0 04/07/17 08:53
2-Methylphenol(o-Cresol)ug/L ND 10.0 04/07/17 08:53
2-Nitroaniline ug/L ND 50.0 04/07/17 08:53
2-Nitrophenol ug/L ND 10.0 04/07/17 08:53
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 04/07/17 08:53
3,3'-Dichlorobenzidine ug/L ND 20.0 04/07/17 08:53
3-Nitroaniline ug/L ND 50.0 04/07/17 08:53
4,6-Dinitro-2-methylphenol ug/L ND 20.0 04/07/17 08:53
4-Bromophenylphenyl ether ug/L ND 10.0 04/07/17 08:53
4-Chloro-3-methylphenol ug/L ND 20.0 04/07/17 08:53
4-Chloroaniline ug/L ND 20.0 04/07/17 08:53
4-Chlorophenylphenyl ether ug/L ND 10.0 04/07/17 08:53
4-Nitroaniline ug/L ND 20.0 04/07/17 08:53
4-Nitrophenol ug/L ND 50.0 04/07/17 08:53
Acenaphthene ug/L ND 10.0 04/07/17 08:53
Acenaphthylene ug/L ND 10.0 04/07/17 08:53
Aniline ug/L ND 10.0 04/07/17 08:53
Anthracene ug/L ND 10.0 04/07/17 08:53
Benzo(a)anthracene ug/L ND 10.0 04/07/17 08:53
Benzo(a)pyrene ug/L ND 10.0 04/07/17 08:53
Benzo(b)fluoranthene ug/L ND 10.0 04/07/17 08:53
Benzo(g,h,i)perylene ug/L ND 10.0 04/07/17 08:53
Benzo(k)fluoranthene ug/L ND 10.0 04/07/17 08:53
Benzoic Acid ug/L ND 50.0 04/07/17 08:53
Benzyl alcohol ug/L ND 20.0 04/07/17 08:53
bis(2-Chloroethoxy)methane ug/L ND 10.0 04/07/17 08:53
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/10/2017 10:46 AM
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Page 19 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92335793
MIRANDA ROAD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1972638
Associated Lab Samples:92335793001, 92335793002, 92335793003
Matrix:Water
Analyzed
bis(2-Chloroethyl) ether ug/L ND 10.0 04/07/17 08:53
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 04/07/17 08:53
Butylbenzylphthalate ug/L ND 10.0 04/07/17 08:53
Chrysene ug/L ND 10.0 04/07/17 08:53
Di-n-butylphthalate ug/L ND 10.0 04/07/17 08:53
Di-n-octylphthalate ug/L ND 10.0 04/07/17 08:53
Dibenz(a,h)anthracene ug/L ND 10.0 04/07/17 08:53
Dibenzofuran ug/L ND 10.0 04/07/17 08:53
Diethylphthalate ug/L ND 10.0 04/07/17 08:53
Dimethylphthalate ug/L ND 10.0 04/07/17 08:53
Fluoranthene ug/L ND 10.0 04/07/17 08:53
Fluorene ug/L ND 10.0 04/07/17 08:53
Hexachloro-1,3-butadiene ug/L ND 10.0 04/07/17 08:53
Hexachlorobenzene ug/L ND 10.0 04/07/17 08:53
Hexachlorocyclopentadiene ug/L ND 10.0 04/07/17 08:53
Hexachloroethane ug/L ND 10.0 04/07/17 08:53
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 04/07/17 08:53
Isophorone ug/L ND 10.0 04/07/17 08:53
N-Nitroso-di-n-propylamine ug/L ND 10.0 04/07/17 08:53
N-Nitrosodimethylamine ug/L ND 10.0 04/07/17 08:53
N-Nitrosodiphenylamine ug/L ND 10.0 04/07/17 08:53
Naphthalene ug/L ND 10.0 04/07/17 08:53
Nitrobenzene ug/L ND 10.0 04/07/17 08:53
Pentachlorophenol ug/L ND 25.0 04/07/17 08:53
Phenanthrene ug/L ND 10.0 04/07/17 08:53
Phenol ug/L ND 10.0 04/07/17 08:53
Pyrene ug/L ND 10.0 04/07/17 08:53
2,4,6-Tribromophenol (S)%38 27-110 04/07/17 08:53
2-Fluorobiphenyl (S)%76 27-110 04/07/17 08:53
2-Fluorophenol (S)%19 12-110 04/07/17 08:53
Nitrobenzene-d5 (S)%72 21-110 04/07/17 08:53
Phenol-d6 (S)%21 10-110 04/07/17 08:53
Terphenyl-d14 (S)%100 31-107 04/07/17 08:53
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1972639LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1972640
1,2,4-Trichlorobenzene ug/L 35.250 70 31-1207135.5 1 30
1,2-Dichlorobenzene ug/L 35.750 71 38-1206733.5 6 30
1,3-Dichlorobenzene ug/L 33.050 66 30-1226532.3 2 30
1,4-Dichlorobenzene ug/L 34.250 68 37-1206432.1 6 30
1-Methylnaphthalene ug/L 39.750 79 34-1138241.2 4 30
2,2'-Oxybis(1-chloropropane)ug/L 41.350 83 18-1207638.0 8 30
2,4,5-Trichlorophenol ug/L 37.150 74 43-1136431.8 15 30
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/10/2017 10:46 AM
Pace Analytical Services, LLC
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Page 20 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92335793
MIRANDA ROAD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1972639LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1972640
2,4,6-Trichlorophenol ug/L 42.150 84 42-1206834.2 21 30
2,4-Dichlorophenol ug/L 40.050 80 30-1207336.5 9 30
2,4-Dimethylphenol ug/L 43.950 88 29-1118542.6 3 30
2,4-Dinitrophenol ug/L 157 R12506319-1323690.1 54 30
2,4-Dinitrotoluene ug/L 52.450 105 58-12810452.1 1 30
2,6-Dinitrotoluene ug/L 54.450 109 54-12910853.9 1 30
2-Chloronaphthalene ug/L 42.250 84 43-1178241.1 3 30
2-Chlorophenol ug/L 39.550 79 37-1206733.7 16 30
2-Methylnaphthalene ug/L 41.550 83 33-1208542.5 2 30
2-Methylphenol(o-Cresol)ug/L 32.050 64 31-1205929.5 8 30
2-Nitroaniline ug/L 78.2100 78 48-1217979.1 1 30
2-Nitrophenol ug/L 49.050 98 25-1168643.2 13 30
3&4-Methylphenol(m&p Cresol)ug/L 27.250 54 23-1204522.6 19 30
3,3'-Dichlorobenzidine ug/L 86.9100 87 10-1548888.1 1 30
3-Nitroaniline ug/L 83.4100 83 43-1158484.2 1 30
4,6-Dinitro-2-methylphenol ug/L 78.0 R11007844-1245252.1 40 30
4-Bromophenylphenyl ether ug/L 42.450 85 34-1138240.8 4 30
4-Chloro-3-methylphenol ug/L 80.8100 81 31-1108080.3 1 30
4-Chloroaniline ug/L 76.9100 77 20-1207878.1 2 30
4-Chlorophenylphenyl ether ug/L 37.850 76 34-1167537.5 1 30
4-Nitroaniline ug/L 86.8100 87 46-1288888.4 2 30
4-Nitrophenol ug/L 76.0250 30 11-1202459.2 25 30
Acenaphthene ug/L 42.850 86 48-1148241.2 4 30
Acenaphthylene ug/L 42.650 85 48-1128140.7 5 30
Aniline ug/L 25.850 52 26-1204723.5 9 30
Anthracene ug/L 42.150 84 57-1188341.7 1 30
Benzo(a)anthracene ug/L 41.950 84 56-1218442.1 0 30
Benzo(a)pyrene ug/L 40.650 81 55-1277939.4 3 30
Benzo(b)fluoranthene ug/L 39.650 79 53-1287839.0 2 30
Benzo(g,h,i)perylene ug/L 41.750 83 54-1258542.4 2 30
Benzo(k)fluoranthene ug/L 39.150 78 51-1237738.3 2 30
Benzoic Acid ug/L 62.3250 25 10-1201741.9J 30
Benzyl alcohol ug/L 71.7100 72 27-1206464.3 11 30
bis(2-Chloroethoxy)methane ug/L 39.850 80 32-1208039.8 0 30
bis(2-Chloroethyl) ether ug/L 44.950 90 33-1118542.3 6 30
bis(2-Ethylhexyl)phthalate ug/L 54.850 110 50-14510451.9 5 30
Butylbenzylphthalate ug/L 54.650 109 54-13810452.2 4 30
Chrysene ug/L 41.550 83 58-1278341.7 0 30
Di-n-butylphthalate ug/L 50.150 100 56-1259849.0 2 30
Di-n-octylphthalate ug/L 58.350 117 50-13411155.3 5 30
Dibenz(a,h)anthracene ug/L 42.650 85 53-1298341.3 3 30
Dibenzofuran ug/L 41.150 82 45-1208241.0 0 30
Diethylphthalate ug/L 45.650 91 53-1209145.4 0 30
Dimethylphthalate ug/L 45.650 91 55-1168843.8 4 30
Fluoranthene ug/L 41.750 83 57-1258442.2 1 30
Fluorene ug/L 40.950 82 53-1188140.4 1 30
Hexachloro-1,3-butadiene ug/L 32.950 66 23-1206834.2 4 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/10/2017 10:46 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 29
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92335793
MIRANDA ROAD
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1972639LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1972640
Hexachlorobenzene ug/L 45.250 90 49-1168743.3 4 30
Hexachlorocyclopentadiene ug/L 29.450 59 26-1585427.1 8 30
Hexachloroethane ug/L 33.050 66 30-1146532.7 1 30
Indeno(1,2,3-cd)pyrene ug/L 43.050 86 55-1288542.7 1 30
Isophorone ug/L 46.350 93 31-1189446.9 1 30
N-Nitroso-di-n-propylamine ug/L 40.250 80 32-1197437.0 8 30
N-Nitrosodimethylamine ug/L 28.250 56 13-1205226.2 8 30
N-Nitrosodiphenylamine ug/L 44.150 88 43-1208542.5 4 30
Naphthalene ug/L 39.050 78 32-1207838.8 0 30
Nitrobenzene ug/L 41.350 83 33-1108743.7 6 30
Pentachlorophenol ug/L 101100 101 10-1377979.4 24 30
Phenanthrene ug/L 40.850 82 57-1178240.8 0 30
Phenol ug/L 18.650 37 10-1203316.3 13 30
Pyrene ug/L 39.050 78 55-1227437.1 5 30
2,4,6-Tribromophenol (S)%106 27-11089
2-Fluorobiphenyl (S)%80 27-11078
2-Fluorophenol (S)%44 12-11036
Nitrobenzene-d5 (S)%75 21-11078
Phenol-d6 (S)%33 10-11028
Terphenyl-d14 (S)%82 31-10778
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/10/2017 10:46 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 29
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92335793
MIRANDA ROAD
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/10/2017 10:46 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 29
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92335793
MIRANDA ROAD
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92335793001 355594 355702TMW-1 EPA 3510 EPA 8270
92335793002 355594 355702TMW-2 EPA 3510 EPA 8270
92335793003 355594 355702TMW-3 EPA 3510 EPA 8270
92335793001 355323TMW-1 EPA 8260
92335793002 355323TMW-2 EPA 8260
92335793003 355323TMW-3 EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/10/2017 10:46 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 29
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Limited Phase II ESA – Miranda Road Site SUMMIT Project No. 3962.01
Charlotte, North Carolina April 14, 2017

E:\Project Forms\Projects\3962.01 Miranda Road Phase II\Appendix IV.rtf

APPENDIX IV
WELL RECORDS
WELL PERMITS
SIP Form – revised 2/15/11
Mecklenburg County Health Department Groundwater & Wastewater Services 700 N. Tryon St., Suite 211 Charlotte, NC 28202
Phone: [phone] Fax: [phone] http://groundwater.charmeck.org
Permit Issuance Date: _______________
Permit Number: ____________________ 
SUBSURFACE INVESTIGATION PERMIT
I. Well Owner Information
Name: ___________________________________
Attn: _____________________________________
Phone #: _____________________
Address 1: ________________________________
Address 2: ________________________________
City: __________________________ State: _______ Zip: _____________
II. Agent Information (if applicable)

Name: ___________________________________
Attn: _____________________________________
Phone #: _____________________
Address 1: ________________________________
Address 2: ________________________________
City: __________________________ State: _______ Zip: _____________
III. Site Information

Site Name; ________________________________
Parcel ID Number: _____________________
Address: ________________________________
City: __________________________ State: _______ Zip: _____________

General Conditions of This Permit:
• This permit shall be VALID for a period not to exceed twelve (12) months from the date of issuance.
• This permit is VALID for the site specified aboveDQGmust be on-site during the course of the investigation
and made available to a Department representative upon request.
• A North Carolina Certified Well Contrator must perform any well contractor activities associated with this permit.
• All wells shall be constructed and abandoned to the standards of Chapter VI, Section V and Section VIof the Mecklenburg County Groundwater Well Regulations.
• All temporary wells, including those installed using Direct Push Technology, must be abandoned
to the standards of Chapter VI, Section VI of the Mecklenburg County Groundwater Well Regulations.
• Registration information for all wells must be submitted to the Department within thirty (30) days of well completion. If water samples are collected, it is recommended that the well NOT be registered until the
analytical results are received.

Owner
3/2/2017
70002411
Marlin Bay, LLC
Keith Rains
803-493-5393
310 sprincrest drive
Fort Mill SC 29715
Miranda Road Tracts
03315201
NC