MO-29548_48687_CA_IAR_20221021

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]

October 21, 2022

Mr. Brad Newton
NCDEQ-UST Section
Mooresville Regional Office
610 East Center Ave.
Mooresville, NC 28115

Re: Initial Abatement Action Report
August 2022
Riverside Grocery
107 Riverside Drive
McAdenville, Gaston County
North Carolina
Facility ID Number: 00-0-0000015989
Incident Number: Pending
GRI Project Number: 6171

Dear Mr. Newton,

Please find enclosed the referenced report for the above-mentioned site.
If you have any questions, please contact Eric Eubanks at 704-845-4010.

Sincerely,
Geological Resources, Inc.

Leslie Maxtone-Graham
Administrative Assistant

Enclosure

Cc. Mr. Donald McGinnis, file

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
Engineering Certification: C-2727 • Geology Certification: C-127
Initial Abatement Action Report
August 2022
Riverside Grocery
107 Riverside Drive
McAdenville, Gaston County
North Carolina 28101
Facility ID Number: 00-0-0000015989
Incident Number: Pending
GRI Project Number: 6171

Prepared for:

Mr. Donald McGinnis
Riverside Grocery
107 Riverside Drive
McAdenville, North Carolina 28101

October 11, 2022

Eric Eubanks, P.G.
Project Manager
Xavier T. Farmer, G.I.T.
Report Writer

_____________________________________________________________________________________
Prepared by: Geological Resources, Inc. Initial Abatement Action Report
Prepared on: October 11, 2022 Riverside Grocery
Project Manager: Eric Eubanks, P.G. GRI Project No. 6171
i
EXECUTIVE SUMMARY
Riverside Grocery is a former petroleum retail facility and convenience store. The site is located at 107
Riverside Drive in McAdenville, Gaston County, North Carolina. The adjoining properties are commercial
and residential. Municipal water is available to the site. The site had one UST basin southeast of the
canopy which contained one 6,000-gallon gasoline, one 4,000-gallon gasoline and one 4,000-gallon diesel
USTs. These USTs were removed from the site on August 30, 2022.

During tank removal activities, petroleum contamination was noted beneath the product piping and the
dispenser island. Ground water not encountered in the UST basin. UST closure soil samples were
collected beneath the USTs, product piping, the dispenser island, and from each truckload of excavated
soil. The collected soil samples were submitted for on-site analysis of TPH-GRO and TPH-DRO using UVF
technology. Based on the field observations and UVF field screening results, over-excavation activities
were conducted beneath the dispenser island and beneath the product lines during UST system removal.

Following over-excavation activities, confirmation soil samples were collected from beneath the dispenser
island and product piping. The collected confirmation samples were submitted for laboratory analysis for
VOCs using EPA Method 8260D, SVOCs by EPA Method 8270D, and VPH and EPH by the MADEP Methods.
The reported concentrations of TPH-GRO, TPH-DRO, one or more individual BTEX constituents,
naphthalene, n-butylbenzene, n-propylbenzene, sec-butylbenzene, isopropylbenzene, 4-
isopropyltolunene, 1,2,4-trimethylbenzene, 1,3,5-trimethylbenzene, 1-methylnaphthalene, 2-
methylnaphthalene, C5-C8 aliphatics, C9-C12 aliphatics, C9-C18 aliphatics, C9-C10 aromatics and/or C11-
C22 aromatics reported in confirmation samples OE-PP-1-14’, OE-DI-1-14’, and OE-DI-2-14 were above
the RALs or soil-to-water MCCs.

Based on these results, a release has occurred at the site. A Limited Site Assessment should be conducted
to determine the risk classification of the site.

_____________________________________________________________________________________
Prepared by: Geological Resources, Inc. Initial Abatement Action Report
Prepared on: October 11, 2022 Riverside Grocery
Project Manager: Eric Eubanks, P.G. GRI Project No. 6171
iii
ACRONYMS
ACM: Asbestos Containing Materials
AFVR: Aggressive Fluid-Vapor Recovery
ARR: Acknowledgement of Report Receipt
AS: Air Sparging
AST: Aboveground Storage Tank
ASTM: American Society for Testing and
Materials
BGS: Below Ground Surface
CAP: Corrective Action Plan
CFR: Code of Federal Regulations
CSA: Comprehensive Site Assessment
DPE: Dual Phase Extraction
DRO: Total Petroleum Hydrocarbons Diesel
Range Organics
DWM: Division of Waste Management
DWR: Department of Water Resources
EPA: Environmental Protection Agency
EPH: Extractible Petroleum Hydrocarbons
ESA: Environmental Site Assessment
GCL: Gross Contamination Level
GRI: Geological Resources, Inc.
GRO: Total Petroleum Hydrocarbons
Gasoline Range Organics
LSA: Limited Site Assessment
MAC: Maximum Allowable Concentration as
specified in T15A NCAC 2L.0202
MADEP: Massachusetts Department of
Environmental Protection
MCC: Maximum Contaminant
Concentrations
MMPE: Mobile Multi-Phase Extraction
NAPL: Non-Aqueous Phase Liquid, “Free
Product”
NCDEQ: North Carolina Department of
Environmental Quality
NCDOT: North Carolina Department of
Transportation
NFA: Notice of No Further Action
NORR: Notice of Regulatory Requirements
NOV: Notice of Violation
NPDES: National Pollutant Discharge
Elimination System
NRP: Notice of Residual Petroleum
O&M: Operation and Maintenance
PAHs: Polynuclear Aromatic Hydrocarbons
PCA: Pre-Construction Assessment
RAL: Regulatory Action Level
SCLs: Soil Cleanup Level
SPCC: Spill Prevention Control and
Countermeasures
SVE: Soil Vapor Extraction
SVOCs: Semi-Volatile Organic Compounds
SWPPP: Stormwater Pollution Prevention Plan
TCLP: Toxicity Characteristic Leaching
Procedure (EPA Method SW-846 1311)
TOC: Top of Casing
TPH: Total Petroleum Hydrocarbons
USGS: United States Geological Survey
UST: Underground Storage Tank
UVF: Ultraviolet Fluorescence
VOCs: Volatile Organic Compounds
VPH: Volatile Petroleum Hydrocarbons

_____________________________________________________________________________________
Prepared by: Geological Resources, Inc. Initial Abatement Action Report
Prepared on: October 11, 2022 Riverside Grocery
Project Manager: Eric Eubanks, P.G. GRI Project No. 6171
TABLE OF CONTENTS

EXECUTIVE SUMMARY ....................................................................................................................... i
SITE INFORMATION ............................................................................................................................ ii
ACRONYMS ....................................................................................................................................... iii
A. SITE HISTORY AND CHARACTERIZATION ...................................................................................1
B. SITE CHECK ..............................................................................................................................2
C. UST CLOSURE ..........................................................................................................................2
D. FREE PRODUCT INVESTIGATION AND RECOVERY REPORT .........................................................4
E. GROUND WATER INVESTIGATION ............................................................................................4
F. INITIAL RESPONSE AND ABATEMENT ACTION ...........................................................................4
G. EXCAVATION OF CONTAMINATED SOIL ....................................................................................5
H. SOIL AND GROUNDWATER SAMPLE RESULTS ...........................................................................6
I. SUMMARY AND CONCLUSIONS ................................................................................................7
J. LIMITATIONS ...........................................................................................................................7
FIGURES
Figure 1: Site Location Map
Figure 2: Site Map
Figure 3: Soil Sample Location Map
Figure 4: Soil Quality Map

TABLES
Table 1: UST Owner/Operator Information
Table 2: UST System Information
Table 3: Summary of Soil Sample Analytical Results – Field Data
Table 4: Summary of Soil Sample Analytical Results

APPENDICES
Appendix A: 24-Hour Release and UST Leak Reporting Form (UST-61)
Appendix B: Notice of Intent form (UST-3)
Appendix C: Site Investigation Report for Permanent Closure or Change-in-Service of UST (UST-2A)
Appendix D: Health and Safety Plan
Appendix E: UST Disposal Manifests
Appendix F: Fluid Disposal Manifest
Appendix G: Soil Disposal Manifests
Appendix H: UVF Field Screening Results
Appendix I: Laboratory Analytical Reports

____________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Initial Abatement Action Report
Prepared on: October 11, 2022 Riverside Grocery
Project Manager: Eric Eubanks, P.G. GRI Project No. 6171
1
A. SITE HISTORY AND CHARACTERIZATION
1. UST Owner and Operator Information:
In accordance with the Initial Abatement Action Report guidelines, the UST owner and operator
information has been summarized in Table 1.
2. UST System Information:
In accordance with the Initial Abatement Action Report guidelines, the UST system information has been
summarized in Table 2. A copy of the Registered Tank Report is shown below:

3. Non-UST Information:
No ASTs are located at the site.
4. Comprehensive Description of the Release:
GRI personnel conducted analysis of TPH-GRO and TPH-DRO using UVF technology. Based on the results
of the soil samples collected during UST removal activities, a release was documented at the site. A 24-
Hour Release and UST Leak Reporting Form (UST-61) was submitted to the Mooresville Regional office of
the NCDEQ on September 6, 2022 (Appendix A).

GRI conducted UST removal activities at the site on August 30, 2022. The site had one UST basin southeast
of the canopy, which contained one 6,000-gallon gasoline, one 4,000-gallon gasoline, and one 4,000-
gallon diesel USTs. Petroleum odors were noted in the soil beneath the product piping and the dispenser
island.
5. Description of the Site Characteristics:
The Riverside Grocery site is a former petroleum retail facility and convenience store located at 107
Riverside Drive in McAdenville, Gaston County, North Carolina (Figure 1). The site is bordered to the
southwest by Riverside Drive. A site map is included as Figure 2.

____________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Initial Abatement Action Report
Prepared on: October 11, 2022 Riverside Grocery
Project Manager: Eric Eubanks, P.G. GRI Project No. 6171
2
6. Summary of Initial Abatement Actions, Assessment Activities, and Corrective Actions:
Prior to closure, the appropriate officials were notified by GRI (i.e., Fire Marshal and NCDEQ). A copy of
the UST-3 Notice of Intent Form is included as Appendix B. One 6,000-gallon gasoline, one 4,000-gallon
gasoline, and one 4,000-gallon diesel USTs, a dispenser island, and product piping were removed from the
site on August 30, 2022. Petroleum contamination was noted below product piping and below the
dispenser island. Over-excavation of the product lines and beneath the dispenser island was conducted
due to strong petroleum odors and field screening results. Ground water was not encountered in the UST
basin. A copy of the Site Investigation Report for Permanent Closure or Change-in-Service of UST (UST-
2A) Form has been included as Appendix C. A copy of the site-specific health and safety plan used during
UST closure activities is included as Appendix D.

B. SITE CHECK
A site check was not part of the initial abatement activities.

C. UST CLOSURE
1. Preparation for Closure:
Donald McGinnis contracted GRI to supervise UST closure activities of 6,000-gallon gasoline UST, 4,000-
gallon gasoline UST and 4,000-gallon diesel UST as well as associated dispensers and product piping from
the site. Prior to closure activities, GRI personnel notified the City of McAdenville Fire Department. A
Notice of Intent: UST Permanent Closure or Change-in-Service (UST-3 Form) Form was submitted to the
NCDEQ Mooresville Regional office on August 9, 2022, and is included as Appendix B. A copy of the Site
Investigation Report for Permanent Closure or Change-in-Service of UST Form (UST-2A Form) is included
as Appendix C. A copy of the site-specific health and safety plan is included as Appendix D.

2. Closure Procedure:
Between August 30 and August 31, 2022, one 6,000-gallon gasoline UST, one 4,000-gallon gasoline UST
and one 4,000-gallon diesel UST as well as associated dispensers and product piping were removed from
the site. The USTs were located in the UST basin southeast of the canopy. The 6,000-gallon UST measured
8 feet in diameter by 16 feet in length and the 4,000-gallon USTs measured 5 feet 4 inches in diameter by
24 feet in length. All of the USTs were visually inspected and appeared to be in fair condition with minor
corrosion and pitting. All of the USTs were constructed of steel. A disposal manifest for the USTs removed
in August 2022 is included as Appendix E. The USTs were transported off site for proper disposal. Photos
of the 4,000-gallon USTs and 6,000-gallon UST are shown below:

____________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Initial Abatement Action Report
Prepared on: October 11, 2022 Riverside Grocery
Project Manager: Eric Eubanks, P.G. GRI Project No. 6171
3

3. Residual Material:
Prior to the initiation of the UST closure activities, the USTs were emptied. Product and residual liquid
were removed from the 6,000-gallon gasoline, 4,000-gallon gasoline and 4,000-gallon diesel USTs. A total
of 81 gallons of petroleum contacted water was vacuumed out of the USTs and properly disposed of at a
permitted disposal facility. A copy of the disposal manifest for the fluids recovered during the pump out
event is provided as Appendix F.
4. Release Information:
Soil samples were collected during UST closure activities in August 2022 from under the three USTs,
product piping and dispensers. The samples were analyzed for TPH-GRO and TPH-DRO by UVF methods
onsite. The concentrations of GRO and DRO in samples taken from under the product piping (PP-1-4’) and
dispensers (DI-1-4’ and DI-2-4’) exceeded the action levels. Based on this information, over excavation
activities were conducted in those areas.
5. Soil Excavation Activities:
Based on the observations and direction of GRI staff, 127.46 tons of contaminated soil were removed
from the site during the August 2022 UST closure activities. The over-excavation of the product piping
and dispensers was extended downward due to strong odors and field screening results following the

____________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Initial Abatement Action Report
Prepared on: October 11, 2022 Riverside Grocery
Project Manager: Eric Eubanks, P.G. GRI Project No. 6171
4
removal of USTs. The excavation boundaries are shown on Figure 2. Soil disposal manifests are included
as Appendix G.
6. Site Investigation:
Soil samples were collected from the base of the UST basins (1-G-1-12’, 1G-2-12’, 2-D-1-10’ through 2-D-
3-10’, 3-G-1-10’ through 3-G-3-10’), from beneath the dispenser islands (DI-1-4’ and DI-2-4’) and from
beneath the product piping (PP-1-4’) and were analyzed on-site for GRO and DRO using UVF methods.
Based on the field observations and UVF results, over-excavation activities were conducted along the
product piping and beneath the dispensers.

Following over-excavation of the UST basins, confirmation soil samples were collected from beneath the
product piping (OE-PP-1-14’) and dispensers (OE-DI-1-14’, OE-DI-2-14’) were submitted for on-site
analysis for TPH-GRO and TPH-DRO. Since the field screening soil sample results were above the RALs,
soil samples OE-PP-1-14’, OE-DI-1-14’, and OE-DI-2-14’ were submitted to Waypoint Analytical (Waypoint)
for laboratory analyses of VOCs using EPA Method 8260D, SVOCs using EPA Method 8270D and VPH and
EPH by the MADEP Methods.

Soil samples collected from below the UST components and soil samples collected from truck loads 1
through 7, represents contaminated soil removal during initial abatement activities and was submitted
for on-site analysis for TPH-GRO and TPH-DRO. All soil samples were collected using either a hand auger
or directly from the bucket of the excavator. Soil sample locations are shown on Figure 3. A copy of the
field screening results is included as Appendix H.

D. FREE PRODUCT INVESTIGATION AND RECOVERY REPORT
Free product was not encountered during the August 2022 UST closure activities.

E. GROUND WATER INVESTIGATION
Ground water was not encountered during the August 2022 UST closure activities.

F. INITIAL RESPONSE AND ABATEMENT ACTION
1. Initial Response Actions:
One 6,000-gallon gasoline UST, one 4,000-gallon gasoline UST and one 4,000-gallon diesel UST, associated
dispensers and product piping were removed from the site between August 30 and August 31, 2022.
Based on the field observations, over excavation activities were conducted under the product piping and
dispensers. Ground water was not encountered in the UST basin.
• Source Control Actions: One 6,000-gallon gasoline UST, one 4,000-gallon gasoline UST and one 4,000-
gallon diesel UST, associated dispensers and product piping were removed from the site between
August 30 and August 31, 2022.
• Contaminant Migration Control Measures: The release was to the sub-surface; therefore, no

____________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Initial Abatement Action Report
Prepared on: October 11, 2022 Riverside Grocery
Project Manager: Eric Eubanks, P.G. GRI Project No. 6171
5
contaminant migration control measures were necessary.
• Measures Taken to Mitigate Fire/Safety Hazards: Prior to closure, the appropriate officials were
notified (i.e., Fire Marshal). Free product was not encountered during closure activities.
• Measures Taken to Identify and Mitigate Pollution Hazards: The release was to the sub-surface;
therefore, no migration control measures were necessary.
2. Initial Abatement Actions:
• Contaminated Soil Storage/Treatment and/or Disposal: Between August 30 and August 31, 2022,
GRI conducted the soil excavation activities. Contaminated soil was loaded into dump trucks and
transported to a permitted facility for disposal.

G. EXCAVATION OF CONTAMINATED SOIL
1. Extent of Soil Contamination:
Over-excavation activities were conducted along the product piping and beneath the dispensers. The
over-excavation was extended in all directions due to strong odors and field screening results
following the removal of USTs. A total of 127.46 tons of contaminated soil was transported offsite to
a permitted disposal facility during the August 2022 UST closure activities. Photos of the excavation
area are shown below:

2. Excavation Process:
The excavation activities were conducted using a track-mounted excavator. GRI conducted the
excavation activities and directed the equipment operators as to what to excavate. Photos showing
the excavation in progress are shown below:

____________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Initial Abatement Action Report
Prepared on: October 11, 2022 Riverside Grocery
Project Manager: Eric Eubanks, P.G. GRI Project No. 6171
6

3. Sampling Description:
All soil samples were collected directly from the bucket of the excavator or using a hand auger by GRI
personnel. Samples were collected with clean, disposable nitrile gloves, immediately placed in
laboratory-supplied glassware and placed on ice.

H. SOIL AND GROUNDWATER SAMPLE RESULTS
• Soil:
The reported concentrations of TPH-GRO, TPH-DRO, one or more individual BTEX constituents,
naphthalene, n-butylbenzene, n-propylbenzene, sec-butylbenzene, isopropylbenzene, 4-
isopropyltolunene, 1,2,4-trimethylbenzene, 1,3,5-trimethylbenzene, 1-methylnaphthalene, 2-
methylnaphthalene, C5-C8 aliphatics, C9-C12 aliphatics, C9-C18 aliphatics, C9-C10 aromatics and/or C11-
C22 aromatics reported in confirmation samples OE-PP-1-14’, OE-DI-1-14’, and OE-DI-2-14 were above
the RALs or soil-to-water MCCs. A summary of soil sample analytical results is presented as Table 4. A Soil
Quality Map has been included as Figure 4. Copies of the laboratory reports are included as Appendix I.
A summary of the soil sampling data from the August 2022 UST closure activities is show below:

____________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Initial Abatement Action Report
Prepared on: October 11, 2022 Riverside Grocery
Project Manager: Eric Eubanks, P.G. GRI Project No. 6171
7 Sample ID Sample Depth (ft-BGS) Gasoline-Range TPH Diesel-Range TPH Benzene Toluene Ethylbenzene Total Xylenes RAL (mg/kg) 50 100 NE NE NE NE
Soil to Water MCC (mg/kg) NE NE 0.0072 5.4 8.0 6.0
Residential SCLs (mg/kg) NE NE 12 1,250 60 3,120
OE-PP-1-14' 14 153 114 <0.018 18 11.3 58.5
OE-DI-1-14' 14 191 189 <0.019 2.93 7.60 43.5
OE-DI-2-14' 14 262 227 <0.018 2.11 7.20 41.3

• Ground Water:
Ground water was not encountered during the August 2022 UST closure activities.

I. SUMMARY AND CONCLUSIONS
• One 6,000-gallon gasoline UST, one 4,000-gallon gasoline UST and one 4,000-gallon diesel UST,
associated dispensers and product piping were removed from the site between August 30, 2022, and
August 31, 2022.
• A total of 127.46 tons of contaminated soil was removed during the August 2022 UST closure
activities.
• No free product was noted in the UST basin during closure activities.
• Ground water was not encountered during the August 2022 UST closure activities.
• The reported concentrations of TPH-GRO, TPH-DRO, one or more individual BTEX constituents,
naphthalene, n-butylbenzene, n-propylbenzene, sec-butylbenzene, isopropylbenzene, 4-
isopropyltolunene, 1,2,4-trimethylbenzene, 1,3,5-trimethylbenzene, 1-methylnaphthalene, 2-
methylnaphthalene, C5-C8 aliphatics, C9-C12 aliphatics, C9-C18 aliphatics, C9-C10 aromatics and/or
C11-C22 aromatics reported in confirmation samples OE-PP-1-14’, OE-DI-1-14’, and OE-DI-2-14 were
above the RALs or soil-to-water MCCs.
• Based on these results, a release has occurred at the site. A Limited Site Assessment should be
conducted to determine the site risk classification of the incident.
J. LIMITATIONS
This report has been prepared for the exclusive use of Mr. Donald McGinnis for specific application to the
referenced site in Gaston County, North Carolina. The assessment was conducted based on the scope of
work and level of effort desired by the NCDEQ and with resources adequate only for that scope of work.
Our findings have been developed in accordance with generally accepted standards of environmental
practices in the State of North Carolina, available information, and our professional judgment. No other
warranty is expressed or implied.

The data that is presented in this report is indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would

____________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Initial Abatement Action Report
Prepared on: October 11, 2022 Riverside Grocery
Project Manager: Eric Eubanks, P.G. GRI Project No. 6171
8
be interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from this data.

FIGURES
SITE LOCATION
Figure 1
Site Location
Riverside Grocery
107 Riverside Drive
McAdenville, North Carolina
Gaston County
Incident No. Pending
GRI Project No. 6171500 M
2000 FT
Date: 08/23/2022 Location: 35.260433° N -81.072897° W
D
a
d

TABLES
UST ID Number 1 through 3 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 1 through 3 Facility ID Number
Owner or Operator?
Owner/Operator
Address Telephone Number
Unknown Unknown
Name of Owner or Operator Dates of Ownership / Operation
00-0-0000015989
United Oil of the Carolinas
Name of Owner or Operator Dates of Ownership / Operation
TABLE 1
UST OWNER/OPERATOR INFORMATION
RIVERSIDE GROCERY (INCIDENT NO. PENDING)
00-0-0000015989
05/08/1986 - 02/26/2003
Donald McGinnis 02/26/2003 - 08/30/2022
Address Telephone Number
852 Mark Wilson Road, Mt. Holly, NC 28120 980-210-4894
Page 1 of 1
Date: 09/06/22
Was Release
Associated
with UST
System?
(Yes / No)
1 Gasoline Gasoline 4,000 5/11/1965
Single Wall
Steel/FRP 5' 4" x 24' Single Wall FRP
Removed
08/30/22 Yes
2 Diesel Diesel 4,000 5/11/1965
Single Wall
Steel/FRP 5' 4" x 24' Single Wall FRP
Removed
08/30/22 Yes
3 Gasoline Gasoline 6,000 5/7/1981
Single Wall
Steel/FRP 8' x 16' Single Wall FRP
Removed
08/30/22 Yes
Tank
Dimensions
Description of
Associated
Product Piping
and
Pumps
Status
of
UST
TABLE 2
UST SYSTEM INFORMATION
RIVERSIDE GROCERY (INCIDENT NO. PENDING)
Facility ID #: 0-015989
UST
ID
No.
Current
or Most
Recent
Contents
Previous
Contents
Capacity
(gallons)
Date
Installed
Construction
Details
Page 1 of 1
Date: 09/06/22 Facility ID #: 0-015989
Sample ID
Date
Collected
(mm/dd/yy)
Sample
Location
Sample
Depth
(ft-BGS)
50 100
1-G-1-12’08/30/22 12 <10 ---
1-G-2-12’08/30/22 12 <10 ---
2-D-1-10’08/30/22 10 <10 22.6
2-D-2-10’08/30/22 10 <10 8.4
2-D-3-10’08/30/22 10 <10 6.4
3-D-1-10’08/30/22 10 <10 ---
3-D-2-10’08/30/22 10 <10 ---
3-D-3-10’08/30/22 10 <10 ---
DI-1-4’08/30/22 4 486 227
DI-2-4’08/30/22 4 155 118
PP-1-4'08/30/22 Product Piping 4 1,284 644
OE-PP-1-14’08/31/22 14 153 114
OE-DI-1-14’08/31/22 14 191 189
OE-DI-2-14’08/31/22 14 262 227
Truck-1 08/30/22 ---343 217
Truck-2 08/30/22 ---290 199
Truck-3 08/31/22 ---133.2 152
Truck-4 08/31/22 ---153.2 169
Truck-5 08/31/22 ---194 169.2
Truck-6 08/31/22 ---186 176
Truck-7 08/31/22 ---171.2 195.6
UST Basin
Dispenser Island
Overexcavation
Area
TABLE 3
Diesel-Range TPHRIVERSIDE GROCERY (INCIDENT NO. PENDING)
Analytical Method 
• Concentrations in bold face type indicate the reported concentrations exceeded
the RALs
Notes:
• Results reported in mg/kg; samples analyzed onsite by UVF
• ft-BGS: feet below ground surface
• RAL: Regulatory Action Level
• < : Less than the UFV method detection limit
RAL (mg/kg)
Contaminant of Concern Gasoline-Range TPHUVF
SUMMARY OF SOIL SAMPLE ANALYTICAL RESULTS - FIELD DATA
Stockpile
Page 1 of 1
Date: 10/11/22 Facility ID #: 0-015989
Sample ID
Date
Collected
(mm/dd/yy)
Sample
Location
Sample
Depth
(ft-BGS)
50 100 NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE
NE NE 0.0072 5.4 8.0 6.0 0.085 0.2 2.4 2.2 1.3 0.12 1.4 6.6 6.6 0.054 1.5 68 540 31 68 NE 31
NE NE 12 1,250 60 3,120 156 5.5 782 1,560 1,560 1,560 1,560 156 156 22.8 62.5 625 1,560 469 1,560 31,200 469
OE-PP-1-14'08/30/22 Product Piping 14 153 114 <0.018 18 11.3 58.5 <0.019 17.2 4.10 1.67 2.23 0.634 10.3 67.1 20.5 2.06 3.99 257 25.0 369 30.6 J <14.5 29.7 J
OE-DI-1-14'08/30/22 14 191 189 <0.019 2.93 7.60 43.5 <0.020 29.2 6.65 2.62 2.71 1.16 13.0 96.5 28.4 2.58 5.13 648 594 936 69.0 <14.2 42.2 J
OE-DI-2-14'08/30/22 14 262 227 <0.018 2.11 7.20 41.3 <0.020 27.0 5.74 2.66 2.88 1.04 14.1 94.3 27.8 1.53 3.06 445 389 417 55.5 J <14.6 48.6 J
Notes:
• Results reported in mg/kg (milligrams per kilogram).
• Trip blank results reported in μg/L (micrograms per liter).
• RAL: Regulatory Action Level (soil).
• MCC: Maximum Contaminant Concentrations (soil).
• NE: Not Established.
• NR: Analysis
was not • Concentrations in bold face type indicate the Soil-to-Water MCCs were below the reported concentrations.
• Concentrations in italic face type indicate the SCLs were below the reported concentrations.
• < : Less than the method detection limit specified in the laboratory report.
• Please note that corresponding field samples may have been labeled differently than samples submitted to the laboratory for analysis.
• J0: Calibration verification outside of acceptable limits. Result is estimated.
• J3: The associated batch QC was outside the established quality control range for precision.
• J4: The associated batch QC was outside the established quality control range for accuracy.
• J5: The sample matrix interfered with the ability to make any accurate determination; spike value is high.
• J6: The sample matrix interfered with the ability to make any accurate determination; spike value is low.
• B: The same analyte is found in the associated blank.
TABLE 4
SUMMARY OF SOIL SAMPLE ANALYTICAL RESULTS - LABORATORY ANALYTICAL DATA
RIVERSIDE GROCERY (INCIDENT NO. PENDING)Adjusted C19-C36 AliphaticsAdjusted C11-C22 AromaticsMADEP VPH MADEP EPH
BenzeneTolueneEthylbenzeneMTBENaphthalenen-ButylbenzeneAdjusted C5-C8 AliphaticsAdjusted C9-C12 AliphaticsUnadjusted C9-C10 AromaticsAdjusted C9-C18 Aliphatics1,3,5-Trimethylbenzene1-Methylnaphthalene2-MethylnaphthaleneAnalytical Method →
UVF/EPA Methods
5030/8015B and
3550/8015B
Contaminant of Concern →Gasoline-Range TPHDiesel-Range TPHsec-ButylbenzeneIsopropylbenzene1,2,4-TrimethylbenzeneEPA Methods 8260B and 8270D
XylenesRAL (mg/kg)
Soil-to-Water MCCs (mg/kg)
Residential SCLs (mg/kg)
Dispenser
Islands n-Propylbenzene4-Isopropyltoluene(p-isopropyltoluene)Page 1 of 1

APPENDICES

APPENDIX A
24-Hour Release and UST Leak Reporting Form (UST-61)

UST-61 24-Hour Release and UST Leak Reporting Form.
For Releases
in NC
This form should be completed and submitted to the UST Section’s regional office following a known or suspected release from an underground storage tank (UST) system. This form is required to be submitted within 24 hours of discovery of a known or
suspected release
(DWM USE ONLY) Incident # ________ Risk (H,I,L,U)_______ Received On ________ Received By ________
Reported by (circle one): Phone, Fax or Report Region _______
Suspected Contamination? (Y/N) ________ Confirmed GW Contamination? (Y/N) ______ Confirmed Soil Contamination ?(Y/N) ______
Samples Taken?(Y/N) ______ Free Product? (Y/N) _____ If Yes, State Greatest Thickness ______________
Facility ID Number ______________ Date Leak Discovered ___________ Comm/Non-Commercial? ________
Reg/Non-regulated? _____________
INCIDENT DESCRIPTION
Incident Name:
Address: County:
City/Town: Zip Code: Regional Office (circle one): Asheville, Mooresville, Fayetteville, Raleigh, Washington, Wilmington, Winston-Salem
Latitude (decimal degrees): Longitude (decimal degrees) : Obtained by:
Briefly describe suspected or confirmed release: (including but not limited to: nature of release, date of release, amount
of release, amount of free product present and recovery efforts, initial responses conducted, impacts to receptors)  GPS
 Topographic map
 GIS Address matching
 Other
 Unknown
Describe location:

HOW RELEASE WAS DISCOVERED (Release Code)
(Check one)
 Release Detection Equipment or Methods
 During UST Closure/Removal
 Property Transfer
 Visual/Odor
 Water in Tank
 Water Supply Well Contamination
 Groundwater Contamination
 Surface Water Contamination
 Other (specify) _______________

SOURCE OF CONTAMINATION
Source of Release (Check primary source) Cause of Release (Check primary cause) Type of Release (Check one) Product Type Released (Check primary product type released)

 Tank
 Piping
 Dispenser
 Submersible Turbine Pump
 Delivery Problem
 Spill Bucket
 Other
 Unknown
Definitions presented on reverse

 Spill
 Overfill
 Corrosion
 Physical/Mechanical
Damage
 Install Problem
 Other
 Unknown
Definitions presented on reverse

 Petroleum
 Non-Petroleum
 Both
Location
(Check one)
 Facility
 Residence
 Other

 Gasoline/ Diesel/
Kerosene
 Heating Oil
 Other Petroleum
Products
 Metals
 Other Inorganics
 Other Organics

 Diesel/Veg. Oil
Blend
 Vegetable Oil 100%
 E10 – E20
 E21 – E84
 E85 – E99
 Ethanol 100%
 E01 – E09
Ownership
1. Municipal 2. Military 3. Unknown 4. Private 5. Federal 6. County 7. State Operation Type 1. Public Service 2. Agricultural 3. Residential 4. Education/Relig. 5. Industrial 6. Commercial 7. Mining
UST Form 61 (02/19) Page 1 of 2

Riverside Grocery
107 Riverside Drive
McAdenville
Gaston
0-15989
8/30/22CommReg
Y NYYN
28101
35.260433 -81.072897
xPetroleum contaminated soil was encountered during UST removal
activities. Soil collected from beneath the product piping and
dispenser islands exceeded the RALs for TPH-GRO and TPH-DRO.
Overexcavation activities were conducted beneath the dispensers
and product piping to a depth of 14' BGS, whereupon weathered
bedrock was encountered. Ground water was not encountered.
x
x
x
x
x
x
x

IMPACT ON DRINKING WATER SUPPLIES
Water Supply Wells Affected? 1. Yes 2. No 3. Unknown Number of Water Supply Wells Affected __________________
Water Supply Wells Contaminated: (Include Users Names, Addresses and Phone Numbers. Attach additional sheet if necessary) 1. 2. 3.
UST SYSTEM OWNER UST Owner/Company
Point of Contact Address
City State Zip Code Telephone Number
UST SYSTEM OPERATOR
UST Operator/Company Address
City State Zip Code Telephone Number
LANDOWNER AT LOCATION OF UST INCIDENT
Landowner Address
City State Zip Code Telephone Number
Draw Sketch of Area (showing two major road intersections) or Attach Map
Person Reporting Incident Company Telephone Number
Title Address Date
UST Form 61 (02/19) Page 2 of 2
Definitions of Sources Tank: means the tank that stores the product and is part of the underground storage tank system Piping: means the piping and connectors running from the tank or submersible turbine pump to the dispenser or other end-use equipment (Vent, vapor recovery, or fill lines are excluded.) Dispenser: includes the dispenser and the equipment used to connect the dispenser to the piping (e.g., a release from a suction pump or from components located above the shear valve) Submersible Turbine Pump (STP) Area includes the submersible turbine pump head (typically located in the tank sump), the line leak detector, and the piping that connects the submersible turbine pump to the tank Delivery Problem: identifies releases that occurred during product delivery to the tank. (Typical causes associated with this source are spills and overfills.)
Other: serves as the option to use when the release source is known but does not fit into one of the preceding categories (e.g., for releases from vent lines, vapor recovery lines, and fill lines) Unknown: identifies releases for which the source has not been determined Definitions of Causes
Spill: use this cause when a spill occurs (e.g., when the delivery hose is disconnected from the tank fill pipe or when the nozzle is removed from the dispenser) Overfill: use when an overfill occurs (e.g., overfills may occur from the fill pipe at the tank or when the nozzle fails to shut off at the dispenser) Physical or Mechanical Damage: use for all types of physical or mechanical damage, except corrosion (e.g., puncture of tank or piping, loose fittings, broken components, and components that have changed dimension) Corrosion: use when a metal tank, piping, or other component has a release due to corrosion (e.g., for steel, corrosion takes the form of rust) Installation Problem: use when the problem is determined to have occurred specifically because the UST system was not installed properly Other: use this option when the cause is known but does not fit into one of the preceding categories (e.g., putting regulated substances into monitoring wells) Unknown: use when the cause has not been determined
Donald McGinnis 852 Mark Wilson Drive
Mt. Holly NC 28120 980-210-4894
Riverside Grocery 107 Riverside Drive
McAdenville NC 28101 980-210-4894
Donald McGinnis
Mt. Holly NC
852 Mark Wilson Drive
28120 980-210-4894
Riverside Grocery
Eric M. Eubanks, P.G.
Staff Scientist
Geological Resources, Inc.
3502 Hayes Rd. Monroe, NC 28110
704-845-4010
9/6/2022

APPENDIX B
Notice of Intent form (UST-3)
UST-3 Notice of Intent: UST Permanent Closure or Change-in-Service
Return completed form to:
The DWM Regional Office located in the area where the facility is located. Also send a copy to the Central Office in Raleigh.
SEE MAP ON THE BACK OF THIS FORM FOR THE CENTRAL AND REGIONAL OFFICE ADDRESSES.
STATE USE ONLY

I.D. #_____________________

Date Received______________
INSTRUCTIONS (READ THIS FIRST)
Complete and return a UST-3 form at least thirty (30) days prior to closure or change-in-service activities.
Completed UST closure or change-in-service site assessment reports, along with a copy of the UST-2A and/or 2B forms, should be submitted
to the appropriate Division of Waste Management (DWM) Regional Office within thirty (30) days following closure activities. The UST-2 form
should also be submitted to the Central Office in Raleigh so that the status of the tanks may be changed to permanently closed and your
tank fee account can be closed out. Note: Tank fees may be due for unregistered tanks.
UST closure and change-in-service site assessments must be completed in accordance with the latest version of the Guidelines for Site
Checks, Tank Closure and Initial Response. The guidelines can be obtained at https://deq.nc.gov/about/divisions/waste-management/ust.
Note: To close tanks in place you must obtain prior approval from the DWM Regional office located in the region where the facility is located.
You must make sure that USTs removed from your property are disposed of properly. When choosing a closure contractor, ask where the
tank(s) will be taken for disposal. Usually, USTs are cleaned and cut up for scrap metal. This is dangerous work and must be performed
by a qualified company. Tanks disposed of illegally in fields or other dumpsites can leak petroleum products and sludge into the environment.
If your tanks are disposed of improperly, you could be held responsible for the cleanup of any environmental damage that occurs.
I. OWNERSHIP OF TANKS II. LOCATION
Owner Name (Corporation, Individual, Public Agency, or Other Entity)

Facility Name or Company

Street Address

Facility ID # (If known)

City

County

Street Address

State

Zip Code

City

County

Zip Code

Phone Number

Email

Phone Number

III. CONTACT PERSONNEL
Name:

Company Name:

Job Title:

Phone Number:

IV. TANK REMOVAL, CLOSURE IN PLACE, CHANGE-IN SERVICE
1. Contact local fire marshal.
2. Plan entire closure event.
3. Conduct Site Soil Assessment.
4. If removing tanks or closing in place, refer to
API Publication 2015 Cleaning Petroleum
Storage Tanks and 1604 Removal and
Disposal of Used Underground Petroleum
Storage Tanks.
5. Provide a sketch locating piping, tanks and
soil sampling locations.
6. Submit a closure report in the format of UST-
12 (including the form UST-2) within thirty
(30) days following the site investigation.
7. If a release from the tanks has occurred, the
site assessment portion of the tank closure
must be conducted under the supervision of
a P.E. or L.G., with all closure site assessment
reports bearing the signature and seal of the
P.E. or L.G. If a release has not occurred, the
supervision, signature or seal of a P.E. or L.G.
is not required.
8. Keep closure records for three (3) years.
V. WORK TO BE PERFORMED BY
Contractor Name:

Contractor Company Name:

Address:

City:

State:

Zip Code:

Phone No:

Primary Consultant Name:

Primary Consultant Company Name:

Consultant Phone No:

VI. TANKS SCHEDULED FOR CLOSURE OR CHANGE-IN-SERVICE

Tank ID No.

Size in Gallons

Last Contents
Proposed Activity
Closure Change-In-Service
Removal Abandonment in Place * New Contents Stored

* Prior written approval to abandon a tank in place must be received from a DWM Regional Office.
VII. OWNER OR OWNER’S AUTHORIZED REPRESENTATIVE
Has a release from a UST system occurred at this location? Yes No Unknown
I understand that I can be held responsible for environmental damage resulting from the improper disposal of my USTs.
Print name and official title:
Signature Date Signed

SCHEDULED REMOVAL DATE

Notify your DWM Regional Office
48 hours before this date if
scheduled removal date changes
UST-3 Rev 6/2022
NC Gaston
NC

APPENDIX C
Site Investigation Report for Permanent Closure or Change-in-Service of UST (UST-2A)
UST-2A Site Investigation Report for Permanent Closure or Change-in-
Service of
REGISTERED UST

Return completed form to:
NC DEQ / DWM / UST SECTION
1646 MAIL SERVICE CENTER
RALEIGH, NC 27699-1646
ATTN: REGISTRATION & PERMITTING

phone [phone] fax [phone] http://www.wastenotnc.org/

STATE USE ONLY: Facility ID #

Date Received

INSTRUCTIONS (READ THIS FIRST)
1. UST permanent closure or change in service must be completed in accordance with the latest version of the Guidelines for Site Checks, Tank
Closure and Initial Response and Abatement. The guidelines can be obtained at http://deq.nc.gov/about/divisions/waste-management/waste-
management-permit-guidance/underground-storage-tanks-section.
2. Permanent closure: Complete all sections of this form.
3. Change-in-service: Where a UST system will be converted from storing a regulated substance to a non-regulated substance, complete sections I, II, III, IV, and VI
4. For more than 5 registered UST systems, attach additional forms as needed
5. Tank Fee Refund: An annual tank fee may be refunded for a tank for which a tank fee was not required. An owner or operator must submit
a written request and include: (1) contact information, (2) federal identification # or SSN, and (3) a copy of UST-2 form. The annual tank
fee will be prorated based on the date of permanent closure.
6. UNREGISTERED USTs use Form UST-2B
I. OWNERSHIP OF TANKS II. LOCATION OF TANKS
Owner Name (Corporation, Individual, Public Agency, or Other Entity)

Facility Name or Company

Street Address

Facility ID # (If known)

City County Street Address
State

Zip Code

City

County

Zip Code

Phone Number
Phone Number

III. CONTACT PERSONNEL
Contact for Facility:

Job Title:

Phone #:

Closure Contractor Name:

Closure Contractor Company:

Address:

Phone #

Primary Consultant Name:

Primary Consultant Company:

Address:

Phone #

IV. UST INFORMATION FOR REGISTERED UST SYSTEMS
UNREGISTERED USTs use Form UST-2B V. EXCAVATION CONDITION
Tank ID
No.
Size in
Gallons
Last
Contents
Last
Use
Date
Permanent
Close Date Method of Permanent Closure:
Indicate REMOVED or enter fill
material, such as foam/ concrete/ sand
Change-in-
Service
Date
Water in excavation Free product
Notable
odor or
visible soil
contaminatio
n
Yes No Yes No Yes No

VI. CERTIFICATION
I certify under penalty of law that I have personally examined and am familiar with the information submitted in this and all attached documents and that
based on my inquiry of those individuals immediately responsible for obtaining the information, I believe that the submitted information is true accurate and complete.
Print name and official title of owner or owner’s authorized representative

Signature Date Signed

NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY, DIVISION OF WASTE MANAGEMENT, UST SECTION
1646 MAIL SERVICE CENTER, RALEIGH, NC 27699-1646 PHONE [phone] FAX [phone] http://www.wastenotnc.org/ 1/2016

Donald McGinnis
852 Mark Wilson Road
Mount Holly Gaston
North Carolina 28120
980-210-4894
Riverside Grocery
00-0-0000015989
107 Riverside Drive
McAdenville 28101Gaston
980-210-4894
Donald McGinnis Owner 980-210-4894
Justin Radford Geological Resources, Inc.3502 Hayes Road, Monroe, NC 28110704-845-4010
Eric Eubanks Geological Resources, Inc.3502 Hayes Road, Monroe, NC 28110704-845-4010
1 4,000 Gasoline Unknown8/30/2022 REMOVED 8/30/2022
2 4,000 Diesel Unknown8/30/2022 8/30/2022
3 6,000 Gasoline Unknown8/30/2022 8/30/2022
REMOVED
REMOVED
Donald McGinnis, Owner
9/8/2022

APPENDIX D
Health and Safety Plan

1
GEOLOGICAL RESOURCES, INC.
Site-Specific Health and Safety Plan

1.0 General Information:
a. Project name: Riverside Grocery
b. Location: 107 Riverside Drive, McAdenville, Gaston County, NC
c. GRI Job #: 6171

2.0 Project Organization:
a. Site Supervisor/H&S Officer: Eric Eubanks 919-455-4577
b. Project Manager: Eric Eubanks 919-455-4577
c. Subcontractor(s):

3.0 Safety Plan Preparation:
a. Prepared by & date: Eric Eubanks, 08/24/22
b. Reviewed/approved by & date: Joanna Alley, 8/24/22

4.0 Site History and Description:
a. Type of site (i.e., spill, leaking UST system, etc.): Former petroleum retail
facility
b. Site/project description: The site is a former petroleum retail station.
Current activities include USTs/canopy/product piping removal activities.

5.0 Potential Hazards:
Physical Hazards: (check)
X Slips X Overhead X Explosion X Sun burn x Electricity
X Trips utilities X Noise Cold Weather X Pressurized
line/vessels
X Falls X Underground X Pinch points X Hot Weather
X Fire utilities X Burns X Crush

Chemical Hazards: (check)
X Gasoline Used Oil
X Diesel Solvents
Kerosene Antifreeze
New Oil Acid (sample preservative)

Equipment/Vehicular/Other: (i.e., Geoprobe, drill rig, back hoe, track hoe, traffic, skid steer etc.)
GRI trucks, excavator, bobcat, dump trucks for soil disposal/backfill

Biological Hazards: (i.e., toxic insects, spiders, poisonous plants, poisonous snakes, aggressive dogs)
Spiders, ants in grass

6.0 Site Organization and Safety Control: (Evaluate the need for site control to protect persons from
exposure to hazardous conditions; i.e. work permits, cones, barricade tape, exclusion zones, etc.)
a. Work area(s) identified: __Entire site _________________________________________

2
b. Work area marked _____ Yes ___X__ No
c. Work area barricaded _____ Yes __X___ No
d. Support area established: ___n/a_____________________________________________
e. Entry and escape routes identified: __n/a ______________________________________
f. Rally point identified: _____ Yes __X__ No Location:____________________________
g. Emergency shut-off for water identified _____ Yes __X___ No
h. Emergency fuel shut-off identified _____ Yes __X___ No
i. Site map attached: _____ Yes _____ No
**Emergency Response Procedures**
Action (i.e. shut off all power equipment) Assemble at rally point
Call 911 for medical or utilities emergency Do NOT enter confined spaces
Discuss what to do if …..cut product line, water line, cable/electric line

7.0 Job Activities in Work Plan:
X UST Removal X Soil Sampling Manual FP Recovery
X Soil Excavation System O&M Other (specify)
Powered Drilling MMPE/AFVR __________________
Hand Augering _ Water sampling __________________
8.0 Required Education and/or Training:
X OSHA 40 hr X Annual 8 hr Refresher OSHA Site Supervisor

9.0 Air Monitoring:
If, in the opinion of the site supervisor, petroleum hydrocarbon vapor concentrations are excessive, site
activities will cease until petroleum hydrocarbon vapor concentrations diminish to acceptable levels.

10.0 Equipment:
FID/PID X Combustible gas indicator Interface Probe
O2 meter Other Water level meter

11.0 Personnel Protection Equipment:
X Hard hat Rubber boots Respirator X Hearing
X Safety glasses X Work gloves X Sun screen protection
X Steel toe boots X First aid kit Repellent X Nitrile
Tyvek suit X Fire extinguisher Dust mask gloves

12.0 Decontamination Procedures: (evaluate need for decon, describe procedures)
Use new nitrile gloves between soil samples.

3
13.0 Emergency Contacts:
a. Local Assistance:
Site Phone Fire Department 911
Police 911 Ambulance 911
Water Department Sanitary Sewer
Natural Gas Power Company

Nearest Hospital with Emergency Room (directions attached)
Name CaroMont Regional Medical Center
Address 2525 Court Dr
Gastonia, NC 28054
Number [phone]

b. National or Regional Sources of Assistance:
1) Geological Resources, Inc. [phone]
2) Chemtrec (24 Hours) [phone]
3) Bureau of Explosives (24 Hours) [phone]
4) National Response Center, NRC [phone]
(Oil/Hazardous Substances)
5) DOT, Off. Of Haz. Operations [phone]

14.0 Signatures:

This plan has been reviewed by all on-site personnel and all provisions are clear (signatures
required).

Project Manager: 8/24/22
Site Supervisor:
Other personnel:

4
15.0 Amendments:

a. Site-Specific Health and Safety Plans are based on information available at the time of plan
preparation. Unexpected conditions may arise. It is important that personal protective
measures be thoroughly assessed prior to and during the planned activities. Unplanned
activities and/or changes in the hazard status should initiate a review of this plan and may
result in major changes to it.
b. Changes in the hazard status or unplanned activities are to be submitted on “Amendment to
the Site-Specific Health and Safety Plan” which is included bellow.
c. Amendment must be approved by the Project Manager prior to implementation of the
amendment.

AMENDMENT TO THE SITE-SPECIFIC HEALTH AND SAFETY PLAN

A. Changes in field activities or hazards:

B. Proposed amendment:

C. Approval:

Proposed by: ___________________________________date ______________________

Approved by: ___________________________________date _____________________

Amendment number: ____________________________

Amendment effective date: _______________________

APPENDIX E
UST Disposal Manifests

APPENDIX F
Fluids Disposal Manifest

APPENDIX G
Soil Disposal Manifests

APPENDIX H
UVF Field Screening Results

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
Engineering Certification: C-2727 • Geology Certification: C-127
UVF Trilogy Analytical Report

Samples Collected: August 30, 2022
Samples Analyzed: August 31, 2022
Site Name: Riverside Grocery
Site Address: 107 Riverside Drive, McAdenville, NC
GRI Project Number: 6171

September 6, 2022

Eric M. Eubanks, P.G.
Operator

Technical Procedures
Sample Collection and Handling
Soil samples may be collected using any acceptable procedure. Sampler must use a clean pair of nitrile
gloves for each sample collected. The sample will be placed in a clean, sealable bag (ziplock). Once
collected, the sample must be analyzed immediately or placed on ice. The sample may be kept on ice for
up to 48 hours prior to UVF analyses. If the sample cannot be analyzed within 48 hours, the sample may
be extracted and kept at 4 degrees C for up to 14 days. Proper chain-of-custody procedures must be
followed.
Calibration
The UFV Trilogy has standard calibrations stored for the following analysis:
 GRO
 DRO
 Total PAH
 Target PAH
 Heavy PAH
Prior to use, calibration standards are used to perform a 5-point verification on the factory stored
calibrations for GRO and DRO. The calibration standards used are as follows:
GRO
 0.5 ppm
 1 ppm
 3 ppm
 5 ppm
 10 ppm
DRO
 0.1 ppm
 0.5 ppm
 1 ppm
 3 ppm
 5 ppm
Operation
Sample Extraction
 5mg of soil are weighed into a clean extraction jar
 Methanol is added to the extraction jar to create a 2x or 4x dilution
o 2x Dilution: 10 mL of methanol
o 4x Dilution: 20 mL of methanol
 The extraction jar is shaken for several minutes to thoroughly mix the soil with solvent
(methanol)
 The mixture is allowed to settle for several minutes
 A clean syringe is used to draw liquid from the extraction jar
 A clean filter is attached to the end of the syringe and the liquid dispensed through the filter
into a clean test tube
 This liquid is referred to as the extraction
Dilution Preparation
 An adjustable micropipette is used to precisely measure out the amount of extract needed for
the dilution
Technical Procedures
 The measured out amount of the extract is added to a clean test tube and methanol is added
dilute the extract. Examples of dilutions are shown below:

Extract Amount
500 μL
200 μL
100 μL
50 μL
25 μL

Add Solvent to the
5 mL line
5 mL line
5 mL line
5 mL line
5 mL line
2x Extract
Dilution Factor
20x
50x
100x
200x
400x
4x Extract
Dilution Factor
40x
100x
200x
400x
800x

Sample Analyzation
 The dilution is shaken to thoroughly mix, then poured into a clean glass cuvette
 The desired module is inserted into the UVF Trilogy and the corresponding factory calibration is
selected
 “Measure Fluorescence” is pressed on the touchscreen and the reading is recorded
 The reading should be between the concentrations of the calibration standards (GRO: 0.5-10
ppm; DRO 0.1-5 ppm)
o Reading below the calibration standard range are recorded as below the detection limit
 Detection Limit = (lower range of calibration standards range) x dilution factor
(i.e. a GRO sample with a 100x dilution factor has a detection limit of 50 ppm)
o Readings above the calibration standard range should be further diluted and reanalyzed
o Negative readings are an indication of quenching (see below)
 The reading is multiplied by the dilution factor to calculate the final concentration
 Check suspected contaminated samples for quenching by running additional dilutions
o According to the siteLAB Quick Reference Guide:
“Quenching” can occur when the detector is swamped by too many hydrocarbons or
organic interferences, producing low or negative concentrations. Test the sample at
multiple dilutions to confirm results are linear and accurate.”
QA/QC
Calibration
 The UFV Trilogy will be calibrated daily prior to use
 The calibration results will be saved and entered into the calibration log
Method Blank
 A method blank of methanol will be analyzed following calibration and following the last sample
analyzed for each site
Duplicates
 One duplicate will be analyzed for every 20 samples
 The duplicate will be prepared from the extract of the sample and diluted to the same factor as
the sample analyzed
Project Name:Date Collected:
Project Number:Date Analysed:
Project Manager:Operator:
Sample ID Matrix
Dilution
Factor x
GRO
Output
(ppm)
=GRO Value
(mg/Kg)
Dilution
Factor x
DRO
Output
(ppm)
=DRO Value
(mg/Kg)
1-G-1-12'Soil 20 <0.5 <10 ---------
1-G-2-12'Soil 20 <0.5 <10 ---------
2-D-1-10'Soil 20 <0.5 <10 20 1.13 22.6
2-D-2-10'Soil 20 <0.5 <10 20 0.42 8.4
2-D-3-10'Soil 20 <0.5 <10 20 0.32 6.4
3-D-1-10'Soil 20 <0.5 <10 ---------
3-G-2-10'Soil 20 <0.5 <10 ---------
3-G-3-10'Soil 20 <0.5 <10 ---------
DI-1-4'Soil 100 4.86 486 100 2.27 227
DI-2-4'Soil 100 1.55 155 100 1.18 118
Truck-1 Soil 100 3.43 343 100 2.17 217
Truck-2 Soil 100 2.9 290 100 1.99 199
Truck-3 Soil 40 3.33 133.2 40 3.8 152
Truck-4 Soil 40 3.83 153.2 40 4.22 168.8
Truck-5 Soil 40 4.85 194 40 4.23 169.2
Truck-6 Soil 40 4.65 186 40 4.4 176
Truck-7 Soil 40 4.28 171.2 40 4.89 195.6
PP-1-4'Soil 200 6.42 1,284 200 3.22 644
OE-PP-1-14'Soil 100 1.53 153 100 1.14 114
OE-DI-1-14'Soil 100 1.91 191 100 1.89 189
OE-DI-2-14'Soil 100 2.62 262 100 2.27 227
UVF Analytical Report
siteLAB UVF Trilogy
8/31/2022
8/30/2022
Eric Eubanks
Riverside Grocery
6171
Eric Eubanks
Site:
Riverside Grocery
Report Date:
9/6/2022
Page:
1 of 1

APPENDIX I
Laboratory Analytical Reports

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

9/12/2022
Geological Resources, Inc. Eric Eubanks
3502 Hayes Road Monroe, NC, 28110
Ref: Analytical Testing
Lab Report Number: 22-244-0001 Client Project Description: Riverside Grocery
GRI #6171
Dear Eric Eubanks:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 9/1/2022 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love Project Manager
Page 1 of 60
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202337735State ProgramNorth Carolina
12/31/2022402State ProgramNorth Carolina
07/31/202299012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Page 1 of 1 00016/22-244-0001
Page 2 of 60
Report Number:
Sample Summary Table
Client Project Description:
22-244-0001
Riverside Grocery
GRI #6171
Lab No Client Sample ID Matrix Date Collected Date Received
08/30/2022 17:15Solids 98378 OE-PP-1-14'09/01/2022
08/30/2022 17:25Solids 98379 OE-DI-1-14'09/01/2022
08/30/2022 17:35Solids 98380 OE-DI-2-14'09/01/2022
Page 3 of 60
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-244-0001
Report Limit
Project:Riverside Grocery
V 98378OE-PP-1-14'
4.10 09/02/2022 15:558260Dn-Butylbenzene mg/Kg - dry 0.015
1.67 09/02/2022 15:558260Dsec-Butyl benzene mg/Kg - dry 0.017
11.3 09/02/2022 15:558260DEthylbenzenemg/Kg - dry 0.018
4.07 09/02/2022 15:558260Dn-Hexane mg/Kg - dry 0.020
2.23 09/02/2022 15:558260DIsopropylbenzenemg/Kg - dry 0.014
0.634 09/02/2022 15:558260D4-Isopropyl toluene mg/Kg - dry 0.041
17.2 09/02/2022 16:228260DNaphthalenemg/Kg - dry 0.314
10.3 09/02/2022 15:558260Dn-Propylbenzene mg/Kg - dry 0.017
18.0 09/02/2022 16:228260DToluenemg/Kg - dry 0.209
67.1 09/02/2022 16:228260D1,2,4-Trimethylbenzene mg/Kg - dry 0.155
20.5 09/02/2022 16:228260D1,3,5-Trimethylbenzene mg/Kg - dry 0.172
18.0 09/02/2022 16:228260Do-Xylene mg/Kg - dry 0.158
40.5 09/02/2022 16:228260Dm,p-Xylene mg/Kg - dry 0.400
58.5 09/02/2022 16:228260DXylene (Total)mg/Kg - dry 0.158
2.06 09/07/2022 16:558270E1-Methylnaphthalene mg/Kg - dry 0.125
3.99 09/07/2022 16:558270E2-Methylnaphthalene mg/Kg - dry 0.118
4.03 09/07/2022 16:558270ENaphthalenemg/Kg - dry 0.170
257 09/02/2022 15:55CALCULATIONAliphatic C5-C8 (Adjusted)mg/Kg - dry 1.66
25.0 09/02/2022 15:55CALCULATIONAliphatics C9-C12 (Adjusted)mg/Kg - dry 6.22
369 09/02/2022 16:42CALCULATIONAromatic C9-C10 (Adjusted)mg/Kg - dry 0.851
J29.7 09/07/2022 16:55CALCULATIONAromatic C11-C22 (Adjusted)mg/Kg - dry 16.8
J30.6 09/09/2022 20:17MADEP-EPH Aliphatic C9-C18 mg/Kg - dry 10.9
J33.7 09/09/2022 20:17MADEP-EPH Aromatic C11-C22 mg/Kg - dry 16.8
275 09/02/2022 16:42MADEP-VPH Aliphatic C5-C8 mg/Kg - dry 1.66
464 09/02/2022 16:42MADEP-VPH Aliphatic C9-C12 mg/Kg - dry 6.22
369 09/02/2022 16:42MADEP-VPH Aromatic C9-C10 mg/Kg - dry 0.851
15.7 09/07/2022 10:07SW-DRYWT Moisture %
V 98379OE-DI-1-14'
6.65 09/02/2022 16:508260Dn-Butylbenzene mg/Kg - dry 0.016
2.62 09/02/2022 16:508260Dsec-Butyl benzene mg/Kg - dry 0.018
7.60 09/02/2022 16:508260DEthylbenzenemg/Kg - dry 0.019
2.36 09/02/2022 16:508260Dn-Hexane mg/Kg - dry 0.021
2.71 09/02/2022 16:508260DIsopropylbenzenemg/Kg - dry 0.015
1.16 09/02/2022 16:508260D4-Isopropyl toluene mg/Kg - dry 0.043
29.2 09/02/2022 17:178260DNaphthalenemg/Kg - dry 0.329
13.0 09/02/2022 16:508260Dn-Propylbenzene mg/Kg - dry 0.017
Page 4 of 60
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-244-0001
Report Limit
Project:Riverside Grocery
V 98379OE-DI-1-14'
2.93 09/02/2022 16:508260DToluenemg/Kg - dry 0.021
96.5 09/02/2022 17:178260D1,2,4-Trimethylbenzene mg/Kg - dry 0.162
28.4 09/02/2022 17:178260D1,3,5-Trimethylbenzene mg/Kg - dry 0.179
14.7 09/02/2022 17:178260Do-Xylene mg/Kg - dry 0.166
28.8 09/02/2022 17:178260Dm,p-Xylene mg/Kg - dry 0.418
43.5 09/02/2022 17:178260DXylene (Total)mg/Kg - dry 0.166
2.58 09/07/2022 17:178270E1-Methylnaphthalene mg/Kg - dry 0.123
5.13 09/07/2022 17:178270E2-Methylnaphthalene mg/Kg - dry 0.116
5.99 09/07/2022 17:178270ENaphthalenemg/Kg - dry 0.167
648 09/02/2022 16:50CALCULATIONAliphatic C5-C8 (Adjusted)mg/Kg - dry 1.67
594 09/02/2022 16:50CALCULATIONAliphatics C9-C12 (Adjusted)mg/Kg - dry 31.4
936 09/02/2022 17:53CALCULATIONAromatic C9-C10 (Adjusted)mg/Kg - dry 4.30
J42.2 09/07/2022 17:17CALCULATIONAromatic C11-C22 (Adjusted)mg/Kg - dry 16.4
69.0 09/09/2022 20:53MADEP-EPH Aliphatic C9-C18 mg/Kg - dry 10.7
J48.1 09/09/2022 20:53MADEP-EPH Aromatic C11-C22 mg/Kg - dry 16.4
651 09/02/2022 17:30MADEP-VPH Aliphatic C5-C8 mg/Kg - dry 1.67
1580 09/02/2022 17:53MADEP-VPH Aliphatic C9-C12 mg/Kg - dry 31.4
936 09/02/2022 17:53MADEP-VPH Aromatic C9-C10 mg/Kg - dry 4.30
14.0 09/07/2022 10:07SW-DRYWT Moisture %
V 98380OE-DI-2-14'
5.74 09/02/2022 17:448260Dn-Butylbenzene mg/Kg - dry 0.015
2.66 09/02/2022 17:448260Dsec-Butyl benzene mg/Kg - dry 0.018
7.20 09/02/2022 17:448260DEthylbenzenemg/Kg - dry 0.018
2.20 09/02/2022 17:448260Dn-Hexane mg/Kg - dry 0.021
2.88 09/02/2022 17:448260DIsopropylbenzenemg/Kg - dry 0.014
1.04 09/02/2022 17:448260D4-Isopropyl toluene mg/Kg - dry 0.042
27.0 09/02/2022 18:128260DNaphthalenemg/Kg - dry 0.322
14.1 09/02/2022 18:128260Dn-Propylbenzene mg/Kg - dry 0.175
2.11 09/02/2022 17:448260DToluenemg/Kg - dry 0.021
94.3 09/02/2022 18:128260D1,2,4-Trimethylbenzene mg/Kg - dry 0.159
27.8 09/02/2022 18:128260D1,3,5-Trimethylbenzene mg/Kg - dry 0.175
14.1 09/02/2022 18:128260Do-Xylene mg/Kg - dry 0.162
27.2 09/02/2022 18:128260Dm,p-Xylene mg/Kg - dry 0.411
41.3 09/02/2022 18:128260DXylene (Total)mg/Kg - dry 0.162
1.53 09/07/2022 17:408270E1-Methylnaphthalene mg/Kg - dry 0.126
3.06 09/07/2022 17:408270E2-Methylnaphthalene mg/Kg - dry 0.119
Page 5 of 60
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-244-0001
Report Limit
Project:Riverside Grocery
V 98380OE-DI-2-14'
4.16 09/07/2022 17:408270ENaphthalenemg/Kg - dry 0.172
445 09/02/2022 17:44CALCULATIONAliphatic C5-C8 (Adjusted)mg/Kg - dry 1.57
389 09/02/2022 17:44CALCULATIONAliphatics C9-C12 (Adjusted)mg/Kg - dry 29.4
417 09/02/2022 19:05CALCULATIONAromatic C9-C10 (Adjusted)mg/Kg - dry 4.02
J48.6 09/07/2022 17:40CALCULATIONAromatic C11-C22 (Adjusted)mg/Kg - dry 17.0
J55.5 09/09/2022 21:29MADEP-EPH Aliphatic C9-C18 mg/Kg - dry 11.0
J52.8 09/09/2022 21:29MADEP-EPH Aromatic C11-C22 mg/Kg - dry 17.0
447 09/02/2022 18:17MADEP-VPH Aliphatic C5-C8 mg/Kg - dry 1.57
855 09/02/2022 19:05MADEP-VPH Aliphatic C9-C12 mg/Kg - dry 29.4
417 09/02/2022 19:05MADEP-VPH Aromatic C9-C10 mg/Kg - dry 4.02
16.4 09/07/2022 10:07SW-DRYWT Moisture %
Page 6 of 60

Client: Geological Resources, Inc. CASE NARRATIVE
Project: Riverside Grocery Lab Report Number: 22-244-0001
Date: 9/12/2022
Volatile Organic Compounds - GC/MS Method 8260D Analyte: Naphthalene QC Batch No: V23470/V23469
CCV result is above control limits but within method parameters. Results are reported but considered estimated.

Page 7 of 60
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-244-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #6171 Received : 09/01/2022
Riverside Grocery
Report Date : 09/12/2022
Sample ID :
Lab No :
Sampled:OE-PP-1-14'
98378 Matrix:
8/30/2022 17:15
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
15.7 %Moisture 1 09/07/22 10:07 SW-DRYWTAMB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 8 of 60
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-244-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #6171 Received : 09/01/2022
Riverside Grocery
Report Date : 09/12/2022
Sample ID :
Lab No :
Sampled:OE-PP-1-14'
98378 Matrix:
8/30/2022 17:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8260D Prep Batch(es):V23469 09/02/22 08:00
<0.076 mg/Kg - dry 0.076 0.634Acetone 50 09/02/22 15:55 V23470TBL
<0.038 mg/Kg - dry 0.038 0.634Acrolein 50 09/02/22 15:55 V23470TBL
<0.023 mg/Kg - dry 0.023 0.634Acrylonitrile 50 09/02/22 15:55 V23470TBL
<0.018 mg/Kg - dry 0.018 0.158Benzene 50 09/02/22 15:55 V23470TBL
<0.015 mg/Kg - dry 0.015 0.158Bromobenzene 50 09/02/22 15:55 V23470TBL
<0.025 mg/Kg - dry 0.025 0.158Bromochloromethane 50 09/02/22 15:55 V23470TBL
<0.037 mg/Kg - dry 0.037 0.158Bromodichloromethane 50 09/02/22 15:55 V23470TBL
<0.032 mg/Kg - dry 0.032 0.158Bromoform 50 09/02/22 15:55 V23470TBL
<0.057 mg/Kg - dry 0.057 0.317
Bromomethane 50 09/02/22 15:55 V23470TBL
4.10 mg/Kg - dry 0.015 0.158n-Butylbenzene 50 09/02/22 15:55 V23470TBL
1.67 mg/Kg - dry 0.017 0.158sec-Butyl benzene 50 09/02/22 15:55 V23470TBL
<0.015 mg/Kg - dry 0.015 0.158tert-Butyl benzene 50 09/02/22 15:55 V23470TBL
<0.020 mg/Kg - dry 0.020 0.158Carbon Disulfide 50 09/02/22 15:55 V23470TBL
<0.050 mg/Kg - dry 0.050 0.158Carbon Tetrachloride 50 09/02/22 15:55 V23470TBL
<0.021 mg/Kg - dry 0.021 0.158Chlorobenzene 50 09/02/22 15:55 V23470TBL
<0.028 mg/Kg - dry 0.028 0.158
Chlorodibromomethane 50 09/02/22 15:55 V23470TBL
<0.028 mg/Kg - dry 0.028 0.317Chloroethane 50 09/02/22 15:55 V23470TBL
<0.033 mg/Kg - dry 0.033 0.158Chloroform 50 09/02/22 15:55 V23470TBL
<0.020 mg/Kg - dry 0.020 0.317Chloromethane 50 09/02/22 15:55 V23470TBL
<0.016 mg/Kg - dry 0.016 0.1582-Chlorotoluene 50 09/02/22 15:55 V23470TBL
<0.012 mg/Kg - dry 0.012 0.1584-Chlorotoluene 50 09/02/22 15:55 V23470TBL
<0.023 mg/Kg - dry 0.023 0.158Di-Isopropyl Ether (DIPE)50 09/02/22 15:55 V23470TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 9 of 60
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-244-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #6171 Received : 09/01/2022
Riverside Grocery
Report Date : 09/12/2022
Sample ID :
Lab No :
Sampled:OE-PP-1-14'
98378 Matrix:
8/30/2022 17:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8260D Prep Batch(es):V23469 09/02/22 08:00
<0.013 mg/Kg - dry 0.013 0.3171,2-Dibromo-3-Chloropropane 50 09/02/22 15:55 V23470TBL
<0.018 mg/Kg - dry 0.018 0.1581,2-Dibromoethane 50 09/02/22 15:55 V23470TBL
<0.031 mg/Kg - dry 0.031 0.158Dibromomethane 50 09/02/22 15:55 V23470TBL
<0.009 mg/Kg - dry 0.009 0.1581,2-Dichlorobenzene 50 09/02/22 15:55 V23470TBL
<0.012 mg/Kg - dry 0.012 0.1581,3-Dichlorobenzene 50 09/02/22 15:55 V23470TBL
<0.019 mg/Kg - dry 0.019 0.1581,4-Dichlorobenzene 50 09/02/22 15:55 V23470TBL
<0.041 mg/Kg - dry 0.041 0.317Dichlorodifluoromethane 50 09/02/22 15:55 V23470TBL
<0.026 mg/Kg - dry 0.026 0.1581,1-Dichloroethane 50 09/02/22 15:55 V23470TBL
<0.043 mg/Kg - dry 0.043 0.158
1,2-Dichloroethane 50 09/02/22 15:55 V23470TBL
<0.023 mg/Kg - dry 0.023 0.1581,1-Dichloroethene 50 09/02/22 15:55 V23470TBL
<0.025 mg/Kg - dry 0.025 0.158cis-1,2-Dichloroethene 50 09/02/22 15:55 V23470TBL
<0.033 mg/Kg - dry 0.033 0.158trans-1,2-Dichloroethene 50 09/02/22 15:55 V23470TBL
<0.013 mg/Kg - dry 0.013 0.1581,2-Dichloropropane 50 09/02/22 15:55 V23470TBL
<0.017 mg/Kg - dry 0.017 0.1581,3-Dichloropropane 50 09/02/22 15:55 V23470TBL
<0.040 mg/Kg - dry 0.040 0.1582,2-Dichloropropane 50 09/02/22 15:55 V23470TBL
<0.024 mg/Kg - dry 0.024 0.158
1,1-Dichloropropene 50 09/02/22 15:55 V23470TBL
<0.017 mg/Kg - dry 0.017 0.158cis-1,3-Dichloropropene 50 09/02/22 15:55 V23470TBL
<0.025 mg/Kg - dry 0.025 0.158trans-1,3-Dichloropropene 50 09/02/22 15:55 V23470TBL
11.3 mg/Kg - dry 0.018 0.158Ethylbenzene 50 09/02/22 15:55 V23470TBL
<0.026 mg/Kg - dry 0.026 3.18Ethyl Tertiary Butyl Ether (ETBE)50 09/02/22 15:55 V23470TBL
<0.025 mg/Kg - dry 0.025 0.317Hexachlorobutadiene 50 09/02/22 15:55 V23470TBL
4.07 mg/Kg - dry 0.020 0.317n-Hexane 50 09/02/22 15:55 V23470TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 10 of 60
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-244-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #6171 Received : 09/01/2022
Riverside Grocery
Report Date : 09/12/2022
Sample ID :
Lab No :
Sampled:OE-PP-1-14'
98378 Matrix:
8/30/2022 17:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8260D Prep Batch(es):V23469 09/02/22 08:00
<0.019 mg/Kg - dry 0.019 0.6342-Hexanone 50 09/02/22 15:55 V23470TBL
2.23 mg/Kg - dry 0.014 0.158Isopropylbenzene 50 09/02/22 15:55 V23470TBL
0.634 mg/Kg - dry 0.041 0.1584-Isopropyl toluene 50 09/02/22 15:55 V23470TBL
<0.020 mg/Kg - dry 0.020 0.634Methyl Ethyl Ketone (MEK)50 09/02/22 15:55 V23470TBL
<0.019 mg/Kg - dry 0.019 0.158Methyl tert-butyl ether (MTBE)50 09/02/22 15:55 V23470TBL
<0.475 mg/Kg - dry 0.475 0.6344-Methyl-2-Pentanone 50 09/02/22 15:55 V23470TBL
<0.046 mg/Kg - dry 0.046 0.158Methylene Chloride 50 09/02/22 15:55 V23470TBL
17.2 mg/Kg - dry 0.314 3.18Naphthalene 500 09/02/22 16:22 V23470TBL
10.3 mg/Kg - dry 0.017 0.158
n-Propylbenzene 50 09/02/22 15:55 V23470TBL
<0.045 mg/Kg - dry 0.045 0.158Styrene 50 09/02/22 15:55 V23470TBL
<0.033 mg/Kg - dry 0.033 0.1581,1,1,2-Tetrachloroethane 50 09/02/22 15:55 V23470TBL
<0.010 mg/Kg - dry 0.010 0.1581,1,2,2-Tetrachloroethane 50 09/02/22 15:55 V23470TBL
<0.028 mg/Kg - dry 0.028 0.158Tetrachloroethene 50 09/02/22 15:55 V23470TBL
18.0 mg/Kg - dry 0.209 1.59Toluene 500 09/02/22 16:22 V23470TBL
<0.017 mg/Kg - dry 0.017 0.3171,2,3-Trichlorobenzene 50 09/02/22 15:55 V23470TBL
<0.020 mg/Kg - dry 0.020 0.317
1,2,4-Trichlorobenzene 50 09/02/22 15:55 V23470TBL
<0.045 mg/Kg - dry 0.045 0.1581,1,1-Trichloroethane 50 09/02/22 15:55 V23470TBL
<0.014 mg/Kg - dry 0.014 0.1581,1,2-Trichloroethane 50 09/02/22 15:55 V23470TBL
<0.029 mg/Kg - dry 0.029 0.158Trichloroethene 50 09/02/22 15:55 V23470TBL
<0.066 mg/Kg - dry 0.066 0.317Trichlorofluoromethane 50 09/02/22 15:55 V23470TBL
<0.022 mg/Kg - dry 0.022 0.1581,2,3-Trichloropropane 50 09/02/22 15:55 V23470TBL
67.1 mg/Kg - dry 0.155 1.591,2,4-Trimethylbenzene 500 09/02/22 16:22 V23470TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 11 of 60
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-244-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #6171 Received : 09/01/2022
Riverside Grocery
Report Date : 09/12/2022
Sample ID :
Lab No :
Sampled:OE-PP-1-14'
98378 Matrix:
8/30/2022 17:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8260D Prep Batch(es):V23469 09/02/22 08:00
20.5 mg/Kg - dry 0.172 1.591,3,5-Trimethylbenzene 500 09/02/22 16:22 V23470TBL
<0.014 mg/Kg - dry 0.014 0.317Vinyl Acetate 50 09/02/22 15:55 V23470TBL
<0.015 mg/Kg - dry 0.015 0.317Vinyl Chloride 50 09/02/22 15:55 V23470TBL
18.0 mg/Kg - dry 0.158 1.59o-Xylene 500 09/02/22 16:22 V23470TBL
40.5 mg/Kg - dry 0.400 3.18m,p-Xylene 500 09/02/22 16:22 V23470TBL
58.5 mg/Kg - dry 0.158 1.59Xylene (Total)500 09/02/22 16:22 V23470
Surrogate: 4-Bromofluorobenzene 95.5 Limits: 70-130%09/02/22 15:5550 TBL V23470
Surrogate: Dibromofluoromethane 88.8 Limits: 70-130%09/02/22 15:5550 TBL V23470
Surrogate: Toluene-d8 98.1 Limits: 76-129%09/02/22 15:5550 TBL V23470
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%09/02/22 16:22500 TBL V23470
Surrogate: Dibromofluoromethane 97.2 Limits: 70-130%09/02/22 16:22500 TBL V23470
Surrogate: Toluene-d8 102 Limits: 76-129%09/02/22 16:22500 TBL V23470
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V23506 09/06/22 10:25
<0.137 mg/Kg - dry 0.137 0.784Acenaphthene 1 09/07/22 16:55 V23553JMV
<0.124 mg/Kg - dry 0.124 0.784Acenaphthylene 1 09/07/22 16:55 V23553JMV
<0.180 mg/Kg - dry 0.180 0.784Aniline 1 09/07/22 16:55 V23553JMV
<0.169 mg/Kg - dry 0.169 0.784Anthracene 1 09/07/22 16:55 V23553JMV
<0.164 mg/Kg - dry 0.164 0.784Benzo(a)anthracene 1 09/07/22 16:55 V23553JMV
<0.174 mg/Kg - dry 0.174 0.784Benzo(a)pyrene 1 09/07/22 16:55 V23553JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 12 of 60
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-244-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #6171 Received : 09/01/2022
Riverside Grocery
Report Date : 09/12/2022
Sample ID :
Lab No :
Sampled:OE-PP-1-14'
98378 Matrix:
8/30/2022 17:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V23506 09/06/22 10:25
<0.173 mg/Kg - dry 0.173 0.784Benzo(b)fluoranthene 1 09/07/22 16:55 V23553JMV
<0.161 mg/Kg - dry 0.161 0.784Benzo(g,h,i)perylene 1 09/07/22 16:55 V23553JMV
<0.162 mg/Kg - dry 0.162 0.784Benzo(k)fluoranthene 1 09/07/22 16:55 V23553JMV
<0.688 mg/Kg - dry 0.688 2.37Benzoic Acid 1 09/07/22 16:55 V23553JMV
<0.124 mg/Kg - dry 0.124 0.784Benzyl alcohol 1 09/07/22 16:55 V23553JMV
<0.139 mg/Kg - dry 0.139 0.784Bis(2-Chloroethoxy)methane 1 09/07/22 16:55 V23553JMV
<0.126 mg/Kg - dry 0.126 0.784Bis(2-Chloroethyl)ether 1 09/07/22 16:55 V23553JMV
<0.161 mg/Kg - dry 0.161 0.391Bis(2-Chloroisopropyl)ether 1 09/07/22 16:55 V23553JMV
<0.142 mg/Kg - dry 0.142 0.784
Bis(2-ethylhexyl)phthalate 1 09/07/22 16:55 V23553JMV
<0.129 mg/Kg - dry 0.129 0.7844-Bromophenyl phenyl ether 1 09/07/22 16:55 V23553JMV
<0.134 mg/Kg - dry 0.134 0.391Butyl benzyl phthalate 1 09/07/22 16:55 V23553JMV
<0.109 mg/Kg - dry 0.109 0.7844-Chloro-3-methylphenol 1 09/07/22 16:55 V23553JMV
<0.132 mg/Kg - dry 0.132 0.3914-Chloroaniline 1 09/07/22 16:55 V23553JMV
<0.137 mg/Kg - dry 0.137 0.7842-Chloronaphthalene 1 09/07/22 16:55 V23553JMV
<0.116 mg/Kg - dry 0.116 0.7842-Chlorophenol 1 09/07/22 16:55 V23553JMV
<0.149 mg/Kg - dry 0.149 1.19
4-Chlorophenyl phenyl ether 1 09/07/22 16:55 V23553JMV
<0.168 mg/Kg - dry 0.168 0.784Chrysene 1 09/07/22 16:55 V23553JMV
<0.272 mg/Kg - dry 0.272 0.784Dibenz(a,h)anthracene 1 09/07/22 16:55 V23553JMV
<0.141 mg/Kg - dry 0.141 0.784Dibenzofuran 1 09/07/22 16:55 V23553JMV
<0.112 mg/Kg - dry 0.112 0.7841,2-Dichlorobenzene 1 09/07/22 16:55 V23553JMV
<0.115 mg/Kg - dry 0.115 0.7841,3-Dichlorobenzene 1 09/07/22 16:55 V23553JMV
<0.115 mg/Kg - dry 0.115 0.3911,4-Dichlorobenzene 1 09/07/22 16:55 V23553JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 13 of 60
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-244-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #6171 Received : 09/01/2022
Riverside Grocery
Report Date : 09/12/2022
Sample ID :
Lab No :
Sampled:OE-PP-1-14'
98378 Matrix:
8/30/2022 17:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V23506 09/06/22 10:25
<0.174 mg/Kg - dry 0.174 0.7843,3'-Dichlorobenzidine 1 09/07/22 16:55 V23553JMV
<0.113 mg/Kg - dry 0.113 0.7842,4-Dichlorophenol 1 09/07/22 16:55 V23553JMV
<0.213 mg/Kg - dry 0.213 0.784Diethyl phthalate 1 09/07/22 16:55 V23553JMV
<0.206 mg/Kg - dry 0.206 0.784Dimethyl phthalate 1 09/07/22 16:55 V23553JMV
<0.128 mg/Kg - dry 0.128 0.3912,4-Dimethylphenol 1 09/07/22 16:55 V23553JMV
<0.126 mg/Kg - dry 0.126 0.784Di-n-butyl phthalate 1 09/07/22 16:55 V23553JMV
<0.284 mg/Kg - dry 0.284 1.784,6-Dinitro-2-methylphenol 1 09/07/22 16:55 V23553JMV
<0.616 mg/Kg - dry 0.616 1.782,4-Dinitrophenol 1 09/07/22 16:55 V23553JMV
<0.114 mg/Kg - dry 0.114 0.784
2,4-Dinitrotoluene 1 09/07/22 16:55 V23553JMV
<0.128 mg/Kg - dry 0.128 0.7842,6-Dinitrotoluene 1 09/07/22 16:55 V23553JMV
<0.169 mg/Kg - dry 0.169 0.391Di-n-Octyl Phthalate 1 09/07/22 16:55 V23553JMV
<0.145 mg/Kg - dry 0.145 0.784Fluoranthene 1 09/07/22 16:55 V23553JMV
<0.151 mg/Kg - dry 0.151 0.784Fluorene 1 09/07/22 16:55 V23553JMV
<0.125 mg/Kg - dry 0.125 0.784Hexachlorobenzene 1 09/07/22 16:55 V23553JMV
<0.115 mg/Kg - dry 0.115 0.784Hexachlorobutadiene 1 09/07/22 16:55 V23553JMV
<0.186 mg/Kg - dry 0.186 0.784
Hexachlorocyclopentadiene 1 09/07/22 16:55 V23553JMV
<0.094 mg/Kg - dry 0.094 0.784Hexachloroethane 1 09/07/22 16:55 V23553JMV
<0.212 mg/Kg - dry 0.212 0.784Indeno(1,2,3-cd)pyrene 1 09/07/22 16:55 V23553JMV
<0.226 mg/Kg - dry 0.226 0.784Isophorone 1 09/07/22 16:55 V23553JMV
2.06 mg/Kg - dry 0.125 0.7841-Methylnaphthalene 1 09/07/22 16:55 V23553JMV
3.99 mg/Kg - dry 0.118 0.7842-Methylnaphthalene 1 09/07/22 16:55 V23553JMV
<0.115 mg/Kg - dry 0.115 0.7842-Methylphenol 1 09/07/22 16:55 V23553JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 14 of 60
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-244-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #6171 Received : 09/01/2022
Riverside Grocery
Report Date : 09/12/2022
Sample ID :
Lab No :
Sampled:OE-PP-1-14'
98378 Matrix:
8/30/2022 17:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V23506 09/06/22 10:25
<0.100 mg/Kg - dry 0.100 0.7843&4 Methylphenol 1 09/07/22 16:55 V23553JMV
4.03 mg/Kg - dry 0.170 0.784Naphthalene 1 09/07/22 16:55 V23553JMV
<0.114 mg/Kg - dry 0.114 0.7842-Nitroaniline 1 09/07/22 16:55 V23553JMV
<0.142 mg/Kg - dry 0.142 0.7843-Nitroaniline 1 09/07/22 16:55 V23553JMV
<0.110 mg/Kg - dry 0.110 0.3914-Nitroaniline 1 09/07/22 16:55 V23553JMV
<0.137 mg/Kg - dry 0.137 0.391Nitrobenzene 1 09/07/22 16:55 V23553JMV
<0.105 mg/Kg - dry 0.105 0.7842-Nitrophenol 1 09/07/22 16:55 V23553JMV
<0.138 mg/Kg - dry 0.138 0.7844-Nitrophenol 1 09/07/22 16:55 V23553JMV
<0.311 mg/Kg - dry 0.311 0.784
N-Nitrosodimethylamine 1 09/07/22 16:55 V23553JMV
<0.214 mg/Kg - dry 0.214 0.784N-Nitrosodiphenylamine 1 09/07/22 16:55 V23553JMV
<0.139 mg/Kg - dry 0.139 0.784N-Nitroso-di-n-propylamine 1 09/07/22 16:55 V23553JMV
<0.411 mg/Kg - dry 0.411 1.19Pentachlorophenol 1 09/07/22 16:55 V23553JMV
<0.246 mg/Kg - dry 0.246 0.784Phenanthrene 1 09/07/22 16:55 V23553JMV
<0.132 mg/Kg - dry 0.132 0.784Phenol 1 09/07/22 16:55 V23553JMV
<0.158 mg/Kg - dry 0.158 0.784Pyrene 1 09/07/22 16:55 V23553JMV
<0.093 mg/Kg - dry 0.093 0.391
Pyridine 1 09/07/22 16:55 V23553JMV
<0.126 mg/Kg - dry 0.126 0.7841,2,4-Trichlorobenzene 1 09/07/22 16:55 V23553JMV
<0.114 mg/Kg - dry 0.114 0.7842,4,5-Trichlorophenol 1 09/07/22 16:55 V23553JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 15 of 60
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-244-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #6171 Received : 09/01/2022
Riverside Grocery
Report Date : 09/12/2022
Sample ID :
Lab No :
Sampled:OE-PP-1-14'
98378 Matrix:
8/30/2022 17:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V23506 09/06/22 10:25
<0.114 mg/Kg - dry 0.114 0.7842,4,6-Trichlorophenol 1 09/07/22 16:55 V23553JMV
8270ESurrogate: Phenol-d5 90.1 Limits: 34-121%09/07/22 16:551 JMV
Surrogate: 2-Fluorobiphenyl 95.8 Limits: 44-115%09/07/22 16:551 JMV V23553
Surrogate: 2-Fluorophenol 96.7 Limits: 35-115%09/07/22 16:551 JMV V23553
Surrogate: Nitrobenzene-d5 79.0 Limits: 37-122%09/07/22 16:551 JMV V23553
Surrogate: 4-Terphenyl-d14 116 Limits: 54-127%09/07/22 16:551 JMV V23553
Surrogate: 2,4,6-Tribromophenol 115 Limits: 39-132%09/07/22 16:551 JMV V23553
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 16 of 60
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-244-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #6171 Received : 09/01/2022
Riverside Grocery
Report Date : 09/12/2022
Sample ID :
Lab No :
Sampled:OE-PP-1-14'
98378 Matrix:
8/30/2022 17:15
Solids
Analytical Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
CALCULATION
257 mg/Kg - dry 1.66 10.9Aliphatic C5-C8 (Adjusted)100 09/02/22 15:55
25.0 mg/Kg - dry 6.22 10.9Aliphatics C9-C12 (Adjusted)100 09/02/22 15:55
369 mg/Kg - dry 0.851 10.9Aromatic C9-C10 (Adjusted)100 09/02/22 16:42
29.7 J mg/Kg - dry 16.8 59.4Aromatic C11-C22 (Adjusted)1 09/07/22 16:55
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):V23573 09/07/22 13:15
30.6 J mg/Kg - dry 10.9 59.4Aliphatic C9-C18 1 09/09/22 20:17 V23694JLK
<14.5 mg/Kg - dry 14.5 59.4Aliphatic C19-C36 1 09/09/22 20:17 V23694JLK
33.7 J mg/Kg - dry 16.8 59.4Aromatic C11-C22 1 09/09/22 20:17 V23694JLK
MADEP-EPHSurrogate: 2-Bromonaphthalene 98.3 Limits: 40-140%09/09/22 20:171 JLK
MADEP-EPHSurrogate: Chlorooctadecane 74.0 Limits: 40-140%09/09/22 20:171 JLK
MADEP-EPHSurrogate: OTP Surrogate 81.0 Limits: 40-140%09/09/22 20:171 JLK
Surrogate: 2-Fluorobiphenyl 96.3 Limits: 40-140%09/09/22 20:171 JLK V23694
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V23447 09/02/22 08:00
275 mg/Kg - dry 1.66 10.9Aliphatic C5-C8 100 09/02/22 16:42 V23448TBL
464 mg/Kg - dry 6.22 10.9Aliphatic C9-C12 100 09/02/22 16:42 V23448TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 17 of 60
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-244-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #6171 Received : 09/01/2022
Riverside Grocery
Report Date : 09/12/2022
Sample ID :
Lab No :
Sampled:OE-PP-1-14'
98378 Matrix:
8/30/2022 17:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V23447 09/02/22 08:00
369 mg/Kg - dry 0.851 10.9Aromatic C9-C10 100 09/02/22 16:42 V23448TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)104 Limits: 70-130%09/02/22 16:42100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)91.0 Limits: 70-130%09/02/22 16:42100 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 18 of 60
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-244-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #6171 Received : 09/01/2022
Riverside Grocery
Report Date : 09/12/2022
Sample ID :
Lab No :
Sampled:OE-DI-1-14'
98379 Matrix:
8/30/2022 17:25
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
14.0 %Moisture 1 09/07/22 10:07 SW-DRYWTAMB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 19 of 60
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-244-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #6171 Received : 09/01/2022
Riverside Grocery
Report Date : 09/12/2022
Sample ID :
Lab No :
Sampled:OE-DI-1-14'
98379 Matrix:
8/30/2022 17:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8260D Prep Batch(es):V23469 09/02/22 08:00
<0.079 mg/Kg - dry 0.079 0.665Acetone 50 09/02/22 16:50 V23470TBL
<0.040 mg/Kg - dry 0.040 0.665Acrolein 50 09/02/22 16:50 V23470TBL
<0.025 mg/Kg - dry 0.025 0.665Acrylonitrile 50 09/02/22 16:50 V23470TBL
<0.019 mg/Kg - dry 0.019 0.166Benzene 50 09/02/22 16:50 V23470TBL
<0.016 mg/Kg - dry 0.016 0.166Bromobenzene 50 09/02/22 16:50 V23470TBL
<0.026 mg/Kg - dry 0.026 0.166Bromochloromethane 50 09/02/22 16:50 V23470TBL
<0.039 mg/Kg - dry 0.039 0.166Bromodichloromethane 50 09/02/22 16:50 V23470TBL
<0.033 mg/Kg - dry 0.033 0.166Bromoform 50 09/02/22 16:50 V23470TBL
<0.060 mg/Kg - dry 0.060 0.332
Bromomethane 50 09/02/22 16:50 V23470TBL
6.65 mg/Kg - dry 0.016 0.166n-Butylbenzene 50 09/02/22 16:50 V23470TBL
2.62 mg/Kg - dry 0.018 0.166sec-Butyl benzene 50 09/02/22 16:50 V23470TBL
<0.016 mg/Kg - dry 0.016 0.166tert-Butyl benzene 50 09/02/22 16:50 V23470TBL
<0.021 mg/Kg - dry 0.021 0.166Carbon Disulfide 50 09/02/22 16:50 V23470TBL
<0.052 mg/Kg - dry 0.052 0.166Carbon Tetrachloride 50 09/02/22 16:50 V23470TBL
<0.022 mg/Kg - dry 0.022 0.166Chlorobenzene 50 09/02/22 16:50 V23470TBL
<0.029 mg/Kg - dry 0.029 0.166
Chlorodibromomethane 50 09/02/22 16:50 V23470TBL
<0.029 mg/Kg - dry 0.029 0.332Chloroethane 50 09/02/22 16:50 V23470TBL
<0.034 mg/Kg - dry 0.034 0.166Chloroform 50 09/02/22 16:50 V23470TBL
<0.020 mg/Kg - dry 0.020 0.332Chloromethane 50 09/02/22 16:50 V23470TBL
<0.016 mg/Kg - dry 0.016 0.1662-Chlorotoluene 50 09/02/22 16:50 V23470TBL
<0.013 mg/Kg - dry 0.013 0.1664-Chlorotoluene 50 09/02/22 16:50 V23470TBL
<0.024 mg/Kg - dry 0.024 0.166Di-Isopropyl Ether (DIPE)50 09/02/22 16:50 V23470TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 20 of 60
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-244-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #6171 Received : 09/01/2022
Riverside Grocery
Report Date : 09/12/2022
Sample ID :
Lab No :
Sampled:OE-DI-1-14'
98379 Matrix:
8/30/2022 17:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8260D Prep Batch(es):V23469 09/02/22 08:00
<0.014 mg/Kg - dry 0.014 0.3321,2-Dibromo-3-Chloropropane 50 09/02/22 16:50 V23470TBL
<0.019 mg/Kg - dry 0.019 0.1661,2-Dibromoethane 50 09/02/22 16:50 V23470TBL
<0.032 mg/Kg - dry 0.032 0.166Dibromomethane 50 09/02/22 16:50 V23470TBL
<0.010 mg/Kg - dry 0.010 0.1661,2-Dichlorobenzene 50 09/02/22 16:50 V23470TBL
<0.012 mg/Kg - dry 0.012 0.1661,3-Dichlorobenzene 50 09/02/22 16:50 V23470TBL
<0.020 mg/Kg - dry 0.020 0.1661,4-Dichlorobenzene 50 09/02/22 16:50 V23470TBL
<0.043 mg/Kg - dry 0.043 0.332Dichlorodifluoromethane 50 09/02/22 16:50 V23470TBL
<0.027 mg/Kg - dry 0.027 0.1661,1-Dichloroethane 50 09/02/22 16:50 V23470TBL
<0.045 mg/Kg - dry 0.045 0.166
1,2-Dichloroethane 50 09/02/22 16:50 V23470TBL
<0.024 mg/Kg - dry 0.024 0.1661,1-Dichloroethene 50 09/02/22 16:50 V23470TBL
<0.026 mg/Kg - dry 0.026 0.166cis-1,2-Dichloroethene 50 09/02/22 16:50 V23470TBL
<0.034 mg/Kg - dry 0.034 0.166trans-1,2-Dichloroethene 50 09/02/22 16:50 V23470TBL
<0.014 mg/Kg - dry 0.014 0.1661,2-Dichloropropane 50 09/02/22 16:50 V23470TBL
<0.018 mg/Kg - dry 0.018 0.1661,3-Dichloropropane 50 09/02/22 16:50 V23470TBL
<0.042 mg/Kg - dry 0.042 0.1662,2-Dichloropropane 50 09/02/22 16:50 V23470TBL
<0.025 mg/Kg - dry 0.025 0.166
1,1-Dichloropropene 50 09/02/22 16:50 V23470TBL
<0.017 mg/Kg - dry 0.017 0.166cis-1,3-Dichloropropene 50 09/02/22 16:50 V23470TBL
<0.026 mg/Kg - dry 0.026 0.166trans-1,3-Dichloropropene 50 09/02/22 16:50 V23470TBL
7.60 mg/Kg - dry 0.019 0.166Ethylbenzene 50 09/02/22 16:50 V23470TBL
<0.027 mg/Kg - dry 0.027 3.33Ethyl Tertiary Butyl Ether (ETBE)50 09/02/22 16:50 V23470TBL
<0.026 mg/Kg - dry 0.026 0.332Hexachlorobutadiene 50 09/02/22 16:50 V23470TBL
2.36 mg/Kg - dry 0.021 0.332n-Hexane 50 09/02/22 16:50 V23470TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 21 of 60
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-244-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #6171 Received : 09/01/2022
Riverside Grocery
Report Date : 09/12/2022
Sample ID :
Lab No :
Sampled:OE-DI-1-14'
98379 Matrix:
8/30/2022 17:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8260D Prep Batch(es):V23469 09/02/22 08:00
<0.020 mg/Kg - dry 0.020 0.6652-Hexanone 50 09/02/22 16:50 V23470TBL
2.71 mg/Kg - dry 0.015 0.166Isopropylbenzene 50 09/02/22 16:50 V23470TBL
1.16 mg/Kg - dry 0.043 0.1664-Isopropyl toluene 50 09/02/22 16:50 V23470TBL
<0.021 mg/Kg - dry 0.021 0.665Methyl Ethyl Ketone (MEK)50 09/02/22 16:50 V23470TBL
<0.020 mg/Kg - dry 0.020 0.166Methyl tert-butyl ether (MTBE)50 09/02/22 16:50 V23470TBL
<0.498 mg/Kg - dry 0.498 0.6654-Methyl-2-Pentanone 50 09/02/22 16:50 V23470TBL
<0.048 mg/Kg - dry 0.048 0.166Methylene Chloride 50 09/02/22 16:50 V23470TBL
29.2 mg/Kg - dry 0.329 3.33Naphthalene 500 09/02/22 17:17 V23470TBL
13.0 mg/Kg - dry 0.017 0.166
n-Propylbenzene 50 09/02/22 16:50 V23470TBL
<0.047 mg/Kg - dry 0.047 0.166Styrene 50 09/02/22 16:50 V23470TBL
<0.034 mg/Kg - dry 0.034 0.1661,1,1,2-Tetrachloroethane 50 09/02/22 16:50 V23470TBL
<0.010 mg/Kg - dry 0.010 0.1661,1,2,2-Tetrachloroethane 50 09/02/22 16:50 V23470TBL
<0.029 mg/Kg - dry 0.029 0.166Tetrachloroethene 50 09/02/22 16:50 V23470TBL
2.93 mg/Kg - dry 0.021 0.166Toluene 50 09/02/22 16:50 V23470TBL
<0.017 mg/Kg - dry 0.017 0.3321,2,3-Trichlorobenzene 50 09/02/22 16:50 V23470TBL
<0.021 mg/Kg - dry 0.021 0.332
1,2,4-Trichlorobenzene 50 09/02/22 16:50 V23470TBL
<0.047 mg/Kg - dry 0.047 0.1661,1,1-Trichloroethane 50 09/02/22 16:50 V23470TBL
<0.015 mg/Kg - dry 0.015 0.1661,1,2-Trichloroethane 50 09/02/22 16:50 V23470TBL
<0.030 mg/Kg - dry 0.030 0.166Trichloroethene 50 09/02/22 16:50 V23470TBL
<0.069 mg/Kg - dry 0.069 0.332Trichlorofluoromethane 50 09/02/22 16:50 V23470TBL
<0.023 mg/Kg - dry 0.023 0.1661,2,3-Trichloropropane 50 09/02/22 16:50 V23470TBL
96.5 mg/Kg - dry 0.162 1.661,2,4-Trimethylbenzene 500 09/02/22 17:17 V23470TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 22 of 60
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-244-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #6171 Received : 09/01/2022
Riverside Grocery
Report Date : 09/12/2022
Sample ID :
Lab No :
Sampled:OE-DI-1-14'
98379 Matrix:
8/30/2022 17:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8260D Prep Batch(es):V23469 09/02/22 08:00
28.4 mg/Kg - dry 0.179 1.661,3,5-Trimethylbenzene 500 09/02/22 17:17 V23470TBL
<0.015 mg/Kg - dry 0.015 0.332Vinyl Acetate 50 09/02/22 16:50 V23470TBL
<0.015 mg/Kg - dry 0.015 0.332Vinyl Chloride 50 09/02/22 16:50 V23470TBL
14.7 mg/Kg - dry 0.166 1.66o-Xylene 500 09/02/22 17:17 V23470TBL
28.8 mg/Kg - dry 0.418 3.33m,p-Xylene 500 09/02/22 17:17 V23470TBL
43.5 mg/Kg - dry 0.166 1.66Xylene (Total)500 09/02/22 17:17 V23470
Surrogate: 4-Bromofluorobenzene 95.5 Limits: 70-130%09/02/22 16:5050 TBL V23470
Surrogate: Dibromofluoromethane 91.1 Limits: 70-130%09/02/22 16:5050 TBL V23470
Surrogate: Toluene-d8 98.4 Limits: 76-129%09/02/22 16:5050 TBL V23470
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%09/02/22 17:17500 TBL V23470
Surrogate: Dibromofluoromethane 94.1 Limits: 70-130%09/02/22 17:17500 TBL V23470
Surrogate: Toluene-d8 104 Limits: 76-129%09/02/22 17:17500 TBL V23470
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V23506 09/06/22 10:25
<0.134 mg/Kg - dry 0.134 0.767Acenaphthene 1 09/07/22 17:17 V23553JMV
<0.122 mg/Kg - dry 0.122 0.767Acenaphthylene 1 09/07/22 17:17 V23553JMV
<0.176 mg/Kg - dry 0.176 0.767Aniline 1 09/07/22 17:17 V23553JMV
<0.166 mg/Kg - dry 0.166 0.767Anthracene 1 09/07/22 17:17 V23553JMV
<0.161 mg/Kg - dry 0.161 0.767Benzo(a)anthracene 1 09/07/22 17:17 V23553JMV
<0.170 mg/Kg - dry 0.170 0.767Benzo(a)pyrene 1 09/07/22 17:17 V23553JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 23 of 60
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-244-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #6171 Received : 09/01/2022
Riverside Grocery
Report Date : 09/12/2022
Sample ID :
Lab No :
Sampled:OE-DI-1-14'
98379 Matrix:
8/30/2022 17:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V23506 09/06/22 10:25
<0.169 mg/Kg - dry 0.169 0.767Benzo(b)fluoranthene 1 09/07/22 17:17 V23553JMV
<0.158 mg/Kg - dry 0.158 0.767Benzo(g,h,i)perylene 1 09/07/22 17:17 V23553JMV
<0.159 mg/Kg - dry 0.159 0.767Benzo(k)fluoranthene 1 09/07/22 17:17 V23553JMV
<0.674 mg/Kg - dry 0.674 2.33Benzoic Acid 1 09/07/22 17:17 V23553JMV
<0.122 mg/Kg - dry 0.122 0.767Benzyl alcohol 1 09/07/22 17:17 V23553JMV
<0.137 mg/Kg - dry 0.137 0.767Bis(2-Chloroethoxy)methane 1 09/07/22 17:17 V23553JMV
<0.124 mg/Kg - dry 0.124 0.767Bis(2-Chloroethyl)ether 1 09/07/22 17:17 V23553JMV
<0.158 mg/Kg - dry 0.158 0.383Bis(2-Chloroisopropyl)ether 1 09/07/22 17:17 V23553JMV
<0.139 mg/Kg - dry 0.139 0.767
Bis(2-ethylhexyl)phthalate 1 09/07/22 17:17 V23553JMV
<0.126 mg/Kg - dry 0.126 0.7674-Bromophenyl phenyl ether 1 09/07/22 17:17 V23553JMV
<0.131 mg/Kg - dry 0.131 0.383Butyl benzyl phthalate 1 09/07/22 17:17 V23553JMV
<0.107 mg/Kg - dry 0.107 0.7674-Chloro-3-methylphenol 1 09/07/22 17:17 V23553JMV
<0.130 mg/Kg - dry 0.130 0.3834-Chloroaniline 1 09/07/22 17:17 V23553JMV
<0.134 mg/Kg - dry 0.134 0.7672-Chloronaphthalene 1 09/07/22 17:17 V23553JMV
<0.114 mg/Kg - dry 0.114 0.7672-Chlorophenol 1 09/07/22 17:17 V23553JMV
<0.146 mg/Kg - dry 0.146 1.16
4-Chlorophenyl phenyl ether 1 09/07/22 17:17 V23553JMV
<0.165 mg/Kg - dry 0.165 0.767Chrysene 1 09/07/22 17:17 V23553JMV
<0.267 mg/Kg - dry 0.267 0.767Dibenz(a,h)anthracene 1 09/07/22 17:17 V23553JMV
<0.138 mg/Kg - dry 0.138 0.767Dibenzofuran 1 09/07/22 17:17 V23553JMV
<0.109 mg/Kg - dry 0.109 0.7671,2-Dichlorobenzene 1 09/07/22 17:17 V23553JMV
<0.113 mg/Kg - dry 0.113 0.7671,3-Dichlorobenzene 1 09/07/22 17:17 V23553JMV
<0.113 mg/Kg - dry 0.113 0.3831,4-Dichlorobenzene 1 09/07/22 17:17 V23553JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 24 of 60
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-244-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #6171 Received : 09/01/2022
Riverside Grocery
Report Date : 09/12/2022
Sample ID :
Lab No :
Sampled:OE-DI-1-14'
98379 Matrix:
8/30/2022 17:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V23506 09/06/22 10:25
<0.170 mg/Kg - dry 0.170 0.7673,3'-Dichlorobenzidine 1 09/07/22 17:17 V23553JMV
<0.111 mg/Kg - dry 0.111 0.7672,4-Dichlorophenol 1 09/07/22 17:17 V23553JMV
<0.209 mg/Kg - dry 0.209 0.767Diethyl phthalate 1 09/07/22 17:17 V23553JMV
<0.202 mg/Kg - dry 0.202 0.767Dimethyl phthalate 1 09/07/22 17:17 V23553JMV
<0.125 mg/Kg - dry 0.125 0.3832,4-Dimethylphenol 1 09/07/22 17:17 V23553JMV
<0.124 mg/Kg - dry 0.124 0.767Di-n-butyl phthalate 1 09/07/22 17:17 V23553JMV
<0.279 mg/Kg - dry 0.279 1.744,6-Dinitro-2-methylphenol 1 09/07/22 17:17 V23553JMV
<0.604 mg/Kg - dry 0.604 1.742,4-Dinitrophenol 1 09/07/22 17:17 V23553JMV
<0.112 mg/Kg - dry 0.112 0.767
2,4-Dinitrotoluene 1 09/07/22 17:17 V23553JMV
<0.125 mg/Kg - dry 0.125 0.7672,6-Dinitrotoluene 1 09/07/22 17:17 V23553JMV
<0.166 mg/Kg - dry 0.166 0.383Di-n-Octyl Phthalate 1 09/07/22 17:17 V23553JMV
<0.143 mg/Kg - dry 0.143 0.767Fluoranthene 1 09/07/22 17:17 V23553JMV
<0.148 mg/Kg - dry 0.148 0.767Fluorene 1 09/07/22 17:17 V23553JMV
<0.123 mg/Kg - dry 0.123 0.767Hexachlorobenzene 1 09/07/22 17:17 V23553JMV
<0.113 mg/Kg - dry 0.113 0.767Hexachlorobutadiene 1 09/07/22 17:17 V23553JMV
<0.182 mg/Kg - dry 0.182 0.767
Hexachlorocyclopentadiene 1 09/07/22 17:17 V23553JMV
<0.092 mg/Kg - dry 0.092 0.767Hexachloroethane 1 09/07/22 17:17 V23553JMV
<0.208 mg/Kg - dry 0.208 0.767Indeno(1,2,3-cd)pyrene 1 09/07/22 17:17 V23553JMV
<0.222 mg/Kg - dry 0.222 0.767Isophorone 1 09/07/22 17:17 V23553JMV
2.58 mg/Kg - dry 0.123 0.7671-Methylnaphthalene 1 09/07/22 17:17 V23553JMV
5.13 mg/Kg - dry 0.116 0.7672-Methylnaphthalene 1 09/07/22 17:17 V23553JMV
<0.112 mg/Kg - dry 0.112 0.7672-Methylphenol 1 09/07/22 17:17 V23553JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 25 of 60
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-244-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #6171 Received : 09/01/2022
Riverside Grocery
Report Date : 09/12/2022
Sample ID :
Lab No :
Sampled:OE-DI-1-14'
98379 Matrix:
8/30/2022 17:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V23506 09/06/22 10:25
<0.098 mg/Kg - dry 0.098 0.7673&4 Methylphenol 1 09/07/22 17:17 V23553JMV
5.99 mg/Kg - dry 0.167 0.767Naphthalene 1 09/07/22 17:17 V23553JMV
<0.112 mg/Kg - dry 0.112 0.7672-Nitroaniline 1 09/07/22 17:17 V23553JMV
<0.139 mg/Kg - dry 0.139 0.7673-Nitroaniline 1 09/07/22 17:17 V23553JMV
<0.108 mg/Kg - dry 0.108 0.3834-Nitroaniline 1 09/07/22 17:17 V23553JMV
<0.134 mg/Kg - dry 0.134 0.383Nitrobenzene 1 09/07/22 17:17 V23553JMV
<0.103 mg/Kg - dry 0.103 0.7672-Nitrophenol 1 09/07/22 17:17 V23553JMV
<0.136 mg/Kg - dry 0.136 0.7674-Nitrophenol 1 09/07/22 17:17 V23553JMV
<0.305 mg/Kg - dry 0.305 0.767
N-Nitrosodimethylamine 1 09/07/22 17:17 V23553JMV
<0.210 mg/Kg - dry 0.210 0.767N-Nitrosodiphenylamine 1 09/07/22 17:17 V23553JMV
<0.137 mg/Kg - dry 0.137 0.767N-Nitroso-di-n-propylamine 1 09/07/22 17:17 V23553JMV
<0.403 mg/Kg - dry 0.403 1.16Pentachlorophenol 1 09/07/22 17:17 V23553JMV
<0.241 mg/Kg - dry 0.241 0.767Phenanthrene 1 09/07/22 17:17 V23553JMV
<0.130 mg/Kg - dry 0.130 0.767Phenol 1 09/07/22 17:17 V23553JMV
<0.155 mg/Kg - dry 0.155 0.767Pyrene 1 09/07/22 17:17 V23553JMV
<0.092 mg/Kg - dry 0.092 0.383
Pyridine 1 09/07/22 17:17 V23553JMV
<0.124 mg/Kg - dry 0.124 0.7671,2,4-Trichlorobenzene 1 09/07/22 17:17 V23553JMV
<0.111 mg/Kg - dry 0.111 0.7672,4,5-Trichlorophenol 1 09/07/22 17:17 V23553JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 26 of 60
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-244-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #6171 Received : 09/01/2022
Riverside Grocery
Report Date : 09/12/2022
Sample ID :
Lab No :
Sampled:OE-DI-1-14'
98379 Matrix:
8/30/2022 17:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V23506 09/06/22 10:25
<0.112 mg/Kg - dry 0.112 0.7672,4,6-Trichlorophenol 1 09/07/22 17:17 V23553JMV
8270ESurrogate: Phenol-d5 92.8 Limits: 34-121%09/07/22 17:171 JMV
Surrogate: 2-Fluorobiphenyl 90.4 Limits: 44-115%09/07/22 17:171 JMV V23553
Surrogate: 2-Fluorophenol 98.2 Limits: 35-115%09/07/22 17:171 JMV V23553
Surrogate: Nitrobenzene-d5 76.6 Limits: 37-122%09/07/22 17:171 JMV V23553
Surrogate: 4-Terphenyl-d14 114 Limits: 54-127%09/07/22 17:171 JMV V23553
Surrogate: 2,4,6-Tribromophenol 114 Limits: 39-132%09/07/22 17:171 JMV V23553
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 27 of 60
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-244-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #6171 Received : 09/01/2022
Riverside Grocery
Report Date : 09/12/2022
Sample ID :
Lab No :
Sampled:OE-DI-1-14'
98379 Matrix:
8/30/2022 17:25
Solids
Analytical Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
CALCULATION
648 mg/Kg - dry 1.67 11.0Aliphatic C5-C8 (Adjusted)100 09/02/22 16:50
594 mg/Kg - dry 31.4 55.1Aliphatics C9-C12 (Adjusted)50 09/02/22 16:50
936 mg/Kg - dry 4.30 55.1Aromatic C9-C10 (Adjusted)500 09/02/22 17:53
42.2 J mg/Kg - dry 16.4 57.9Aromatic C11-C22 (Adjusted)1 09/07/22 17:17
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):V23573 09/07/22 13:15
69.0 mg/Kg - dry 10.7 57.9Aliphatic C9-C18 1 09/09/22 20:53 V23694JLK
<14.2 mg/Kg - dry 14.2 57.9Aliphatic C19-C36 1 09/09/22 20:53 V23694JLK
48.1 J mg/Kg - dry 16.4 57.9Aromatic C11-C22 1 09/09/22 20:53 V23694JLK
MADEP-EPHSurrogate: 2-Bromonaphthalene 110 Limits: 40-140%09/09/22 20:531 JLK
MADEP-EPHSurrogate: Chlorooctadecane 78.9 Limits: 40-140%09/09/22 20:531 JLK
MADEP-EPHSurrogate: OTP Surrogate 87.9 Limits: 40-140%09/09/22 20:531 JLK
Surrogate: 2-Fluorobiphenyl 103 Limits: 40-140%09/09/22 20:531 JLK V23694
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V23447 09/02/22 08:00
651 mg/Kg - dry 1.67 11.0Aliphatic C5-C8 100 09/02/22 17:30 V23448TBL
1580 mg/Kg - dry 31.4 55.1Aliphatic C9-C12 500 09/02/22 17:53 V23448TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 28 of 60
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-244-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #6171 Received : 09/01/2022
Riverside Grocery
Report Date : 09/12/2022
Sample ID :
Lab No :
Sampled:OE-DI-1-14'
98379 Matrix:
8/30/2022 17:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V23447 09/02/22 08:00
936 mg/Kg - dry 4.30 55.1Aromatic C9-C10 500 09/02/22 17:53 V23448TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)114 Limits: 70-130%09/02/22 17:30100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)79.7 Limits: 70-130%09/02/22 17:30100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)106 Limits: 70-130%09/02/22 17:53500 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)107 Limits: 70-130%09/02/22 17:53500 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 29 of 60
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-244-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #6171 Received : 09/01/2022
Riverside Grocery
Report Date : 09/12/2022
Sample ID :
Lab No :
Sampled:OE-DI-2-14'
98380 Matrix:
8/30/2022 17:35
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
16.4 %Moisture 1 09/07/22 10:07 SW-DRYWTAMB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 30 of 60
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-244-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #6171 Received : 09/01/2022
Riverside Grocery
Report Date : 09/12/2022
Sample ID :
Lab No :
Sampled:OE-DI-2-14'
98380 Matrix:
8/30/2022 17:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8260D Prep Batch(es):V23469 09/02/22 08:00
<0.078 mg/Kg - dry 0.078 0.653Acetone 50 09/02/22 17:44 V23470TBL
<0.039 mg/Kg - dry 0.039 0.653Acrolein 50 09/02/22 17:44 V23470TBL
<0.024 mg/Kg - dry 0.024 0.653Acrylonitrile 50 09/02/22 17:44 V23470TBL
<0.018 mg/Kg - dry 0.018 0.162Benzene 50 09/02/22 17:44 V23470TBL
<0.016 mg/Kg - dry 0.016 0.162Bromobenzene 50 09/02/22 17:44 V23470TBL
<0.026 mg/Kg - dry 0.026 0.162Bromochloromethane 50 09/02/22 17:44 V23470TBL
<0.038 mg/Kg - dry 0.038 0.162Bromodichloromethane 50 09/02/22 17:44 V23470TBL
<0.032 mg/Kg - dry 0.032 0.162Bromoform 50 09/02/22 17:44 V23470TBL
<0.059 mg/Kg - dry 0.059 0.326
Bromomethane 50 09/02/22 17:44 V23470TBL
5.74 mg/Kg - dry 0.015 0.162n-Butylbenzene 50 09/02/22 17:44 V23470TBL
2.66 mg/Kg - dry 0.018 0.162sec-Butyl benzene 50 09/02/22 17:44 V23470TBL
<0.016 mg/Kg - dry 0.016 0.162tert-Butyl benzene 50 09/02/22 17:44 V23470TBL
<0.020 mg/Kg - dry 0.020 0.162Carbon Disulfide 50 09/02/22 17:44 V23470TBL
<0.051 mg/Kg - dry 0.051 0.162Carbon Tetrachloride 50 09/02/22 17:44 V23470TBL
<0.021 mg/Kg - dry 0.021 0.162Chlorobenzene 50 09/02/22 17:44 V23470TBL
<0.028 mg/Kg - dry 0.028 0.162
Chlorodibromomethane 50 09/02/22 17:44 V23470TBL
<0.029 mg/Kg - dry 0.029 0.326Chloroethane 50 09/02/22 17:44 V23470TBL
<0.034 mg/Kg - dry 0.034 0.162Chloroform 50 09/02/22 17:44 V23470TBL
<0.020 mg/Kg - dry 0.020 0.326Chloromethane 50 09/02/22 17:44 V23470TBL
<0.016 mg/Kg - dry 0.016 0.1622-Chlorotoluene 50 09/02/22 17:44 V23470TBL
<0.012 mg/Kg - dry 0.012 0.1624-Chlorotoluene 50 09/02/22 17:44 V23470TBL
<0.023 mg/Kg - dry 0.023 0.162Di-Isopropyl Ether (DIPE)50 09/02/22 17:44 V23470TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 31 of 60
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-244-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #6171 Received : 09/01/2022
Riverside Grocery
Report Date : 09/12/2022
Sample ID :
Lab No :
Sampled:OE-DI-2-14'
98380 Matrix:
8/30/2022 17:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8260D Prep Batch(es):V23469 09/02/22 08:00
<0.014 mg/Kg - dry 0.014 0.3261,2-Dibromo-3-Chloropropane 50 09/02/22 17:44 V23470TBL
<0.019 mg/Kg - dry 0.019 0.1621,2-Dibromoethane 50 09/02/22 17:44 V23470TBL
<0.032 mg/Kg - dry 0.032 0.162Dibromomethane 50 09/02/22 17:44 V23470TBL
<0.010 mg/Kg - dry 0.010 0.1621,2-Dichlorobenzene 50 09/02/22 17:44 V23470TBL
<0.012 mg/Kg - dry 0.012 0.1621,3-Dichlorobenzene 50 09/02/22 17:44 V23470TBL
<0.019 mg/Kg - dry 0.019 0.1621,4-Dichlorobenzene 50 09/02/22 17:44 V23470TBL
<0.043 mg/Kg - dry 0.043 0.326Dichlorodifluoromethane 50 09/02/22 17:44 V23470TBL
<0.026 mg/Kg - dry 0.026 0.1621,1-Dichloroethane 50 09/02/22 17:44 V23470TBL
<0.044 mg/Kg - dry 0.044 0.162
1,2-Dichloroethane 50 09/02/22 17:44 V23470TBL
<0.023 mg/Kg - dry 0.023 0.1621,1-Dichloroethene 50 09/02/22 17:44 V23470TBL
<0.025 mg/Kg - dry 0.025 0.162cis-1,2-Dichloroethene 50 09/02/22 17:44 V23470TBL
<0.034 mg/Kg - dry 0.034 0.162trans-1,2-Dichloroethene 50 09/02/22 17:44 V23470TBL
<0.014 mg/Kg - dry 0.014 0.1621,2-Dichloropropane 50 09/02/22 17:44 V23470TBL
<0.017 mg/Kg - dry 0.017 0.1621,3-Dichloropropane 50 09/02/22 17:44 V23470TBL
<0.041 mg/Kg - dry 0.041 0.1622,2-Dichloropropane 50 09/02/22 17:44 V23470TBL
<0.024 mg/Kg - dry 0.024 0.162
1,1-Dichloropropene 50 09/02/22 17:44 V23470TBL
<0.017 mg/Kg - dry 0.017 0.162cis-1,3-Dichloropropene 50 09/02/22 17:44 V23470TBL
<0.026 mg/Kg - dry 0.026 0.162trans-1,3-Dichloropropene 50 09/02/22 17:44 V23470TBL
7.20 mg/Kg - dry 0.018 0.162Ethylbenzene 50 09/02/22 17:44 V23470TBL
<0.027 mg/Kg - dry 0.027 3.27Ethyl Tertiary Butyl Ether (ETBE)50 09/02/22 17:44 V23470TBL
<0.025 mg/Kg - dry 0.025 0.326Hexachlorobutadiene 50 09/02/22 17:44 V23470TBL
2.20 mg/Kg - dry 0.021 0.326n-Hexane 50 09/02/22 17:44 V23470TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 32 of 60
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-244-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #6171 Received : 09/01/2022
Riverside Grocery
Report Date : 09/12/2022
Sample ID :
Lab No :
Sampled:OE-DI-2-14'
98380 Matrix:
8/30/2022 17:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8260D Prep Batch(es):V23469 09/02/22 08:00
<0.020 mg/Kg - dry 0.020 0.6532-Hexanone 50 09/02/22 17:44 V23470TBL
2.88 mg/Kg - dry 0.014 0.162Isopropylbenzene 50 09/02/22 17:44 V23470TBL
1.04 mg/Kg - dry 0.042 0.1624-Isopropyl toluene 50 09/02/22 17:44 V23470TBL
<0.021 mg/Kg - dry 0.021 0.653Methyl Ethyl Ketone (MEK)50 09/02/22 17:44 V23470TBL
<0.020 mg/Kg - dry 0.020 0.162Methyl tert-butyl ether (MTBE)50 09/02/22 17:44 V23470TBL
<0.490 mg/Kg - dry 0.490 0.6534-Methyl-2-Pentanone 50 09/02/22 17:44 V23470TBL
<0.047 mg/Kg - dry 0.047 0.162Methylene Chloride 50 09/02/22 17:44 V23470TBL
27.0 mg/Kg - dry 0.322 3.27Naphthalene 500 09/02/22 18:12 V23470TBL
14.1 mg/Kg - dry 0.175 1.63
n-Propylbenzene 500 09/02/22 18:12 V23470TBL
<0.046 mg/Kg - dry 0.046 0.162Styrene 50 09/02/22 17:44 V23470TBL
<0.034 mg/Kg - dry 0.034 0.1621,1,1,2-Tetrachloroethane 50 09/02/22 17:44 V23470TBL
<0.010 mg/Kg - dry 0.010 0.1621,1,2,2-Tetrachloroethane 50 09/02/22 17:44 V23470TBL
<0.029 mg/Kg - dry 0.029 0.162Tetrachloroethene 50 09/02/22 17:44 V23470TBL
2.11 mg/Kg - dry 0.021 0.162Toluene 50 09/02/22 17:44 V23470TBL
<0.017 mg/Kg - dry 0.017 0.3261,2,3-Trichlorobenzene 50 09/02/22 17:44 V23470TBL
<0.020 mg/Kg - dry 0.020 0.326
1,2,4-Trichlorobenzene 50 09/02/22 17:44 V23470TBL
<0.046 mg/Kg - dry 0.046 0.1621,1,1-Trichloroethane 50 09/02/22 17:44 V23470TBL
<0.015 mg/Kg - dry 0.015 0.1621,1,2-Trichloroethane 50 09/02/22 17:44 V23470TBL
<0.029 mg/Kg - dry 0.029 0.162Trichloroethene 50 09/02/22 17:44 V23470TBL
<0.068 mg/Kg - dry 0.068 0.326Trichlorofluoromethane 50 09/02/22 17:44 V23470TBL
<0.023 mg/Kg - dry 0.023 0.1621,2,3-Trichloropropane 50 09/02/22 17:44 V23470TBL
94.3 mg/Kg - dry 0.159 1.631,2,4-Trimethylbenzene 500 09/02/22 18:12 V23470TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 33 of 60
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-244-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #6171 Received : 09/01/2022
Riverside Grocery
Report Date : 09/12/2022
Sample ID :
Lab No :
Sampled:OE-DI-2-14'
98380 Matrix:
8/30/2022 17:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8260D Prep Batch(es):V23469 09/02/22 08:00
27.8 mg/Kg - dry 0.175 1.631,3,5-Trimethylbenzene 500 09/02/22 18:12 V23470TBL
<0.015 mg/Kg - dry 0.015 0.326Vinyl Acetate 50 09/02/22 17:44 V23470TBL
<0.015 mg/Kg - dry 0.015 0.326Vinyl Chloride 50 09/02/22 17:44 V23470TBL
14.1 mg/Kg - dry 0.162 1.63o-Xylene 500 09/02/22 18:12 V23470TBL
27.2 mg/Kg - dry 0.411 3.27m,p-Xylene 500 09/02/22 18:12 V23470TBL
41.3 mg/Kg - dry 0.162 1.63Xylene (Total)500 09/02/22 18:12 V23470
Surrogate: 4-Bromofluorobenzene 95.1 Limits: 70-130%09/02/22 17:4450 TBL V23470
Surrogate: Dibromofluoromethane 85.5 Limits: 70-130%09/02/22 17:4450 TBL V23470
Surrogate: Toluene-d8 101 Limits: 76-129%09/02/22 17:4450 TBL V23470
Surrogate: 4-Bromofluorobenzene 99.6 Limits: 70-130%09/02/22 18:12500 TBL V23470
Surrogate: Dibromofluoromethane 92.1 Limits: 70-130%09/02/22 18:12500 TBL V23470
Surrogate: Toluene-d8 102 Limits: 76-129%09/02/22 18:12500 TBL V23470
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V23506 09/06/22 10:25
<0.138 mg/Kg - dry 0.138 0.789Acenaphthene 1 09/07/22 17:40 V23553JMV
<0.125 mg/Kg - dry 0.125 0.789Acenaphthylene 1 09/07/22 17:40 V23553JMV
<0.181 mg/Kg - dry 0.181 0.789Aniline 1 09/07/22 17:40 V23553JMV
<0.171 mg/Kg - dry 0.171 0.789Anthracene 1 09/07/22 17:40 V23553JMV
<0.166 mg/Kg - dry 0.166 0.789Benzo(a)anthracene 1 09/07/22 17:40 V23553JMV
<0.175 mg/Kg - dry 0.175 0.789Benzo(a)pyrene 1 09/07/22 17:40 V23553JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 34 of 60
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-244-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #6171 Received : 09/01/2022
Riverside Grocery
Report Date : 09/12/2022
Sample ID :
Lab No :
Sampled:OE-DI-2-14'
98380 Matrix:
8/30/2022 17:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V23506 09/06/22 10:25
<0.174 mg/Kg - dry 0.174 0.789Benzo(b)fluoranthene 1 09/07/22 17:40 V23553JMV
<0.162 mg/Kg - dry 0.162 0.789Benzo(g,h,i)perylene 1 09/07/22 17:40 V23553JMV
<0.163 mg/Kg - dry 0.163 0.789Benzo(k)fluoranthene 1 09/07/22 17:40 V23553JMV
<0.693 mg/Kg - dry 0.693 2.39Benzoic Acid 1 09/07/22 17:40 V23553JMV
<0.125 mg/Kg - dry 0.125 0.789Benzyl alcohol 1 09/07/22 17:40 V23553JMV
<0.141 mg/Kg - dry 0.141 0.789Bis(2-Chloroethoxy)methane 1 09/07/22 17:40 V23553JMV
<0.127 mg/Kg - dry 0.127 0.789Bis(2-Chloroethyl)ether 1 09/07/22 17:40 V23553JMV
<0.162 mg/Kg - dry 0.162 0.394Bis(2-Chloroisopropyl)ether 1 09/07/22 17:40 V23553JMV
<0.143 mg/Kg - dry 0.143 0.789
Bis(2-ethylhexyl)phthalate 1 09/07/22 17:40 V23553JMV
<0.130 mg/Kg - dry 0.130 0.7894-Bromophenyl phenyl ether 1 09/07/22 17:40 V23553JMV
<0.135 mg/Kg - dry 0.135 0.394Butyl benzyl phthalate 1 09/07/22 17:40 V23553JMV
<0.110 mg/Kg - dry 0.110 0.7894-Chloro-3-methylphenol 1 09/07/22 17:40 V23553JMV
<0.133 mg/Kg - dry 0.133 0.3944-Chloroaniline 1 09/07/22 17:40 V23553JMV
<0.138 mg/Kg - dry 0.138 0.7892-Chloronaphthalene 1 09/07/22 17:40 V23553JMV
<0.117 mg/Kg - dry 0.117 0.7892-Chlorophenol 1 09/07/22 17:40 V23553JMV
<0.150 mg/Kg - dry 0.150 1.20
4-Chlorophenyl phenyl ether 1 09/07/22 17:40 V23553JMV
<0.169 mg/Kg - dry 0.169 0.789Chrysene 1 09/07/22 17:40 V23553JMV
<0.275 mg/Kg - dry 0.275 0.789Dibenz(a,h)anthracene 1 09/07/22 17:40 V23553JMV
<0.142 mg/Kg - dry 0.142 0.789Dibenzofuran 1 09/07/22 17:40 V23553JMV
<0.112 mg/Kg - dry 0.112 0.7891,2-Dichlorobenzene 1 09/07/22 17:40 V23553JMV
<0.116 mg/Kg - dry 0.116 0.7891,3-Dichlorobenzene 1 09/07/22 17:40 V23553JMV
<0.116 mg/Kg - dry 0.116 0.3941,4-Dichlorobenzene 1 09/07/22 17:40 V23553JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 35 of 60
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-244-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #6171 Received : 09/01/2022
Riverside Grocery
Report Date : 09/12/2022
Sample ID :
Lab No :
Sampled:OE-DI-2-14'
98380 Matrix:
8/30/2022 17:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V23506 09/06/22 10:25
<0.175 mg/Kg - dry 0.175 0.7893,3'-Dichlorobenzidine 1 09/07/22 17:40 V23553JMV
<0.114 mg/Kg - dry 0.114 0.7892,4-Dichlorophenol 1 09/07/22 17:40 V23553JMV
<0.215 mg/Kg - dry 0.215 0.789Diethyl phthalate 1 09/07/22 17:40 V23553JMV
<0.208 mg/Kg - dry 0.208 0.789Dimethyl phthalate 1 09/07/22 17:40 V23553JMV
<0.129 mg/Kg - dry 0.129 0.3942,4-Dimethylphenol 1 09/07/22 17:40 V23553JMV
<0.127 mg/Kg - dry 0.127 0.789Di-n-butyl phthalate 1 09/07/22 17:40 V23553JMV
<0.287 mg/Kg - dry 0.287 1.794,6-Dinitro-2-methylphenol 1 09/07/22 17:40 V23553JMV
<0.622 mg/Kg - dry 0.622 1.792,4-Dinitrophenol 1 09/07/22 17:40 V23553JMV
<0.115 mg/Kg - dry 0.115 0.789
2,4-Dinitrotoluene 1 09/07/22 17:40 V23553JMV
<0.129 mg/Kg - dry 0.129 0.7892,6-Dinitrotoluene 1 09/07/22 17:40 V23553JMV
<0.171 mg/Kg - dry 0.171 0.394Di-n-Octyl Phthalate 1 09/07/22 17:40 V23553JMV
<0.147 mg/Kg - dry 0.147 0.789Fluoranthene 1 09/07/22 17:40 V23553JMV
<0.153 mg/Kg - dry 0.153 0.789Fluorene 1 09/07/22 17:40 V23553JMV
<0.126 mg/Kg - dry 0.126 0.789Hexachlorobenzene 1 09/07/22 17:40 V23553JMV
<0.116 mg/Kg - dry 0.116 0.789Hexachlorobutadiene 1 09/07/22 17:40 V23553JMV
<0.187 mg/Kg - dry 0.187 0.789
Hexachlorocyclopentadiene 1 09/07/22 17:40 V23553JMV
<0.094 mg/Kg - dry 0.094 0.789Hexachloroethane 1 09/07/22 17:40 V23553JMV
<0.214 mg/Kg - dry 0.214 0.789Indeno(1,2,3-cd)pyrene 1 09/07/22 17:40 V23553JMV
<0.228 mg/Kg - dry 0.228 0.789Isophorone 1 09/07/22 17:40 V23553JMV
1.53 mg/Kg - dry 0.126 0.7891-Methylnaphthalene 1 09/07/22 17:40 V23553JMV
3.06 mg/Kg - dry 0.119 0.7892-Methylnaphthalene 1 09/07/22 17:40 V23553JMV
<0.116 mg/Kg - dry 0.116 0.7892-Methylphenol 1 09/07/22 17:40 V23553JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 36 of 60
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-244-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #6171 Received : 09/01/2022
Riverside Grocery
Report Date : 09/12/2022
Sample ID :
Lab No :
Sampled:OE-DI-2-14'
98380 Matrix:
8/30/2022 17:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V23506 09/06/22 10:25
<0.101 mg/Kg - dry 0.101 0.7893&4 Methylphenol 1 09/07/22 17:40 V23553JMV
4.16 mg/Kg - dry 0.172 0.789Naphthalene 1 09/07/22 17:40 V23553JMV
<0.115 mg/Kg - dry 0.115 0.7892-Nitroaniline 1 09/07/22 17:40 V23553JMV
<0.143 mg/Kg - dry 0.143 0.7893-Nitroaniline 1 09/07/22 17:40 V23553JMV
<0.111 mg/Kg - dry 0.111 0.3944-Nitroaniline 1 09/07/22 17:40 V23553JMV
<0.138 mg/Kg - dry 0.138 0.394Nitrobenzene 1 09/07/22 17:40 V23553JMV
<0.106 mg/Kg - dry 0.106 0.7892-Nitrophenol 1 09/07/22 17:40 V23553JMV
<0.139 mg/Kg - dry 0.139 0.7894-Nitrophenol 1 09/07/22 17:40 V23553JMV
<0.314 mg/Kg - dry 0.314 0.789
N-Nitrosodimethylamine 1 09/07/22 17:40 V23553JMV
<0.216 mg/Kg - dry 0.216 0.789N-Nitrosodiphenylamine 1 09/07/22 17:40 V23553JMV
<0.141 mg/Kg - dry 0.141 0.789N-Nitroso-di-n-propylamine 1 09/07/22 17:40 V23553JMV
<0.415 mg/Kg - dry 0.415 1.20Pentachlorophenol 1 09/07/22 17:40 V23553JMV
<0.248 mg/Kg - dry 0.248 0.789Phenanthrene 1 09/07/22 17:40 V23553JMV
<0.133 mg/Kg - dry 0.133 0.789Phenol 1 09/07/22 17:40 V23553JMV
<0.160 mg/Kg - dry 0.160 0.789Pyrene 1 09/07/22 17:40 V23553JMV
<0.094 mg/Kg - dry 0.094 0.394
Pyridine 1 09/07/22 17:40 V23553JMV
<0.127 mg/Kg - dry 0.127 0.7891,2,4-Trichlorobenzene 1 09/07/22 17:40 V23553JMV
<0.115 mg/Kg - dry 0.115 0.7892,4,5-Trichlorophenol 1 09/07/22 17:40 V23553JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 37 of 60
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-244-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #6171 Received : 09/01/2022
Riverside Grocery
Report Date : 09/12/2022
Sample ID :
Lab No :
Sampled:OE-DI-2-14'
98380 Matrix:
8/30/2022 17:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V23506 09/06/22 10:25
<0.115 mg/Kg - dry 0.115 0.7892,4,6-Trichlorophenol 1 09/07/22 17:40 V23553JMV
8270ESurrogate: Phenol-d5 94.6 Limits: 34-121%09/07/22 17:401 JMV
Surrogate: 2-Fluorobiphenyl 64.7 Limits: 44-115%09/07/22 17:401 JMV V23553
Surrogate: 2-Fluorophenol 100 Limits: 35-115%09/07/22 17:401 JMV V23553
Surrogate: Nitrobenzene-d5 74.9 Limits: 37-122%09/07/22 17:401 JMV V23553
Surrogate: 4-Terphenyl-d14 101 Limits: 54-127%09/07/22 17:401 JMV V23553
Surrogate: 2,4,6-Tribromophenol 102 Limits: 39-132%09/07/22 17:401 JMV V23553
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 38 of 60
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-244-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #6171 Received : 09/01/2022
Riverside Grocery
Report Date : 09/12/2022
Sample ID :
Lab No :
Sampled:OE-DI-2-14'
98380 Matrix:
8/30/2022 17:35
Solids
Analytical Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
CALCULATION
445 mg/Kg - dry 1.57 10.3Aliphatic C5-C8 (Adjusted)100 09/02/22 17:44
389 mg/Kg - dry 29.4 51.6Aliphatics C9-C12 (Adjusted)50 09/02/22 17:44
417 mg/Kg - dry 4.02 51.6Aromatic C9-C10 (Adjusted)500 09/02/22 19:05
48.6 J mg/Kg - dry 17.0 59.9Aromatic C11-C22 (Adjusted)1 09/07/22 17:40
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):V23573 09/07/22 13:15
55.5 J mg/Kg - dry 11.0 59.9Aliphatic C9-C18 1 09/09/22 21:29 V23694JLK
<14.6 mg/Kg - dry 14.6 59.9Aliphatic C19-C36 1 09/09/22 21:29 V23694JLK
52.8 J mg/Kg - dry 17.0 59.9Aromatic C11-C22 1 09/09/22 21:29 V23694JLK
MADEP-EPHSurrogate: 2-Bromonaphthalene 119 Limits: 40-140%09/09/22 21:291 JLK
MADEP-EPHSurrogate: Chlorooctadecane 79.5 Limits: 40-140%09/09/22 21:291 JLK
MADEP-EPHSurrogate: OTP Surrogate 93.0 Limits: 40-140%09/09/22 21:291 JLK
Surrogate: 2-Fluorobiphenyl 116 Limits: 40-140%09/09/22 21:291 JLK V23694
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V23447 09/02/22 08:00
447 mg/Kg - dry 1.57 10.3Aliphatic C5-C8 100 09/02/22 18:17 V23448TBL
855 mg/Kg - dry 29.4 51.6Aliphatic C9-C12 500 09/02/22 19:05 V23448TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 39 of 60
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-244-0001
00087
Geological Resources, Inc.
3502 Hayes Road
Eric Eubanks
Monroe
Danyale Love
Project Manager
GRI #6171 Received : 09/01/2022
Riverside Grocery
Report Date : 09/12/2022
Sample ID :
Lab No :
Sampled:OE-DI-2-14'
98380 Matrix:
8/30/2022 17:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V23447 09/02/22 08:00
417 mg/Kg - dry 4.02 51.6Aromatic C9-C10 500 09/02/22 19:05 V23448TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)119 Limits: 70-130%09/02/22 18:17100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)98.3 Limits: 70-130%09/02/22 18:17100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)110 Limits: 70-130%09/02/22 19:05500 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)103 Limits: 70-130%09/02/22 19:05500 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 40 of 60
Quality Control Data
22-244-0001Report No:
Project Description:
Client ID:Geological Resources, Inc.
Riverside Grocery
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V23470QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V23469
Associated Lab Samples: 98378, 98379, 98380
LRB-V23469 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/02/22 11:230.0200.002<0.002mg/KgAcetone
09/02/22 11:230.0200.001<0.001mg/KgAcrolein
09/02/22 11:230.0200.0008<0.0008mg/KgAcrylonitrile
09/02/22 11:230.0050.0006<0.0006mg/KgBenzene
09/02/22 11:230.0050.0005<0.0005mg/KgBromobenzene
09/02/22 11:230.0050.0008<0.0008mg/KgBromochloromethane
09/02/22 11:230.0050.001<0.001mg/KgBromodichloromethane
09/02/22 11:230.0050.001<0.001mg/KgBromoform
09/02/22 11:230.0100.001<0.001mg/KgBromomethane
09/02/22 11:230.0050.0005<0.0005mg/Kgn-Butylbenzene
09/02/22 11:230.0050.0006<0.0006mg/Kgsec-Butyl benzene
09/02/22 11:230.0050.0005<0.0005mg/Kgtert-Butyl benzene
09/02/22 11:230.0050.0006<0.0006mg/KgCarbon Disulfide
09/02/22 11:230.0050.001<0.001mg/KgCarbon Tetrachloride
09/02/22 11:230.0050.0007<0.0007mg/KgChlorobenzene
09/02/22 11:230.0050.0009<0.0009mg/KgChlorodibromomethane
09/02/22 11:230.0100.0009<0.0009mg/KgChloroethane
09/02/22 11:230.0050.001<0.001mg/KgChloroform
09/02/22 11:230.0100.0006<0.0006mg/KgChloromethane
09/02/22 11:230.0050.0005<0.0005mg/Kg2-Chlorotoluene
09/02/22 11:230.0050.0004<0.0004mg/Kg4-Chlorotoluene
09/02/22 11:230.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
09/02/22 11:230.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
09/02/22 11:230.0050.0006<0.0006mg/Kg1,2-Dibromoethane
09/02/22 11:230.0050.0010<0.0010mg/KgDibromomethane
09/02/22 11:230.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
09/02/22 11:230.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 1 of 18Date:09/12/2022 03:59 PM
Page 41 of 60
Quality Control Data
22-244-0001Report No:
Project Description:
Client ID:Geological Resources, Inc.
Riverside Grocery
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V23470QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V23469
Associated Lab Samples: 98378, 98379, 98380
LRB-V23469 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/02/22 11:230.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
09/02/22 11:230.0100.001<0.001mg/KgDichlorodifluoromethane
09/02/22 11:230.0050.0008<0.0008mg/Kg1,1-Dichloroethane
09/02/22 11:230.0050.001<0.001mg/Kg1,2-Dichloroethane
09/02/22 11:230.0050.0007<0.0007mg/Kg1,1-Dichloroethene
09/02/22 11:230.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
09/02/22 11:230.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
09/02/22 11:230.0050.0004<0.0004mg/Kg1,2-Dichloropropane
09/02/22 11:230.0050.0006<0.0006mg/Kg1,3-Dichloropropane
09/02/22 11:230.0050.001<0.001mg/Kg2,2-Dichloropropane
09/02/22 11:230.0050.0008<0.0008mg/Kg1,1-Dichloropropene
09/02/22 11:230.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
09/02/22 11:230.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
09/02/22 11:230.0050.0006<0.0006mg/KgEthylbenzene
09/02/22 11:230.1000.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
09/02/22 11:230.0100.0008<0.0008mg/KgHexachlorobutadiene
09/02/22 11:230.0100.0007<0.0007mg/Kgn-Hexane
09/02/22 11:230.0200.0006<0.0006mg/Kg2-Hexanone
09/02/22 11:230.0050.0005<0.0005mg/KgIsopropylbenzene
09/02/22 11:230.0050.001<0.001mg/Kg4-Isopropyl toluene
09/02/22 11:230.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
09/02/22 11:230.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
09/02/22 11:230.0050.001<0.001mg/KgMethylene Chloride
09/02/22 11:230.0100.0010<0.0010mg/KgNaphthalene
09/02/22 11:230.0050.0005<0.0005mg/Kgn-Propylbenzene
09/02/22 11:230.0050.001<0.001mg/KgStyrene
09/02/22 11:230.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
Page 2 of 18Date:09/12/2022 03:59 PM
Page 42 of 60
Quality Control Data
22-244-0001Report No:
Project Description:
Client ID:Geological Resources, Inc.
Riverside Grocery
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V23470QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V23469
Associated Lab Samples: 98378, 98379, 98380
LRB-V23469 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/02/22 11:230.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
09/02/22 11:230.0050.0009<0.0009mg/KgTetrachloroethene
09/02/22 11:230.0050.0007<0.0007mg/KgToluene
09/02/22 11:230.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
09/02/22 11:230.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
09/02/22 11:230.0050.001<0.001mg/Kg1,1,1-Trichloroethane
09/02/22 11:230.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
09/02/22 11:230.0050.0009<0.0009mg/KgTrichloroethene
09/02/22 11:230.0100.002<0.002mg/KgTrichlorofluoromethane
09/02/22 11:230.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
09/02/22 11:230.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
09/02/22 11:230.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
09/02/22 11:230.0100.0005<0.0005mg/KgVinyl Acetate
09/02/22 11:230.0100.0005<0.0005mg/KgVinyl Chloride
09/02/22 11:230.0050.0005<0.0005mg/Kgo-Xylene
09/02/22 11:230.0100.001<0.001mg/Kgm,p-Xylene
09/02/22 11:234-Bromofluorobenzene (S)110 70-130
09/02/22 11:23Dibromofluoromethane (S)102 70-130
09/02/22 11:23Toluene-d8 (S)104 76-129
LCS-V23469 LCSD-V23469Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.087 87.195.20.0950.100mg/KgAcetone 29-198 8.8 20
0.096 96.397.80.0970.100mg/KgAcrolein 70-130 1.5 20
0.103 1031080.1080.100mg/KgAcrylonitrile 65-134 4.7 20
Page 3 of 18Date:09/12/2022 03:59 PM
Page 43 of 60
Quality Control Data
22-244-0001Report No:
Project Description:
Client ID:Geological Resources, Inc.
Riverside Grocery
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V23470QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V23469
LCS-V23469 LCSD-V23469Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.044 89.489.40.0440.050mg/KgBenzene 74-127 0.0 20
0.046 93.091.40.0450.050mg/KgBromobenzene 73-125 1.7 20
0.047 94.094.20.0470.050mg/KgBromochloromethane 72-134 0.2 20
0.046 92.093.80.0460.050mg/KgBromodichloromethane 75-122 1.9 20
0.048 96.21000.0500.050mg/KgBromoform 66-135 4.0 20
0.048 97.495.80.0470.050mg/KgBromomethane 20-180 1.6 20
0.049 98.097.20.0480.050mg/Kgn-Butylbenzene 65-135 0.8 20
0.045 91.290.80.0450.050mg/Kgsec-Butyl benzene 66-131 0.4 20
0.044 89.688.20.0440.050mg/Kgtert-Butyl benzene 67-132 1.5 20
0.044 88.490.60.0450.050mg/KgCarbon Disulfide 61-129 2.4 20
0.042 84.487.80.0430.050mg/KgCarbon Tetrachloride 64-143 3.9 20
0.045 91.292.80.0460.050mg/KgChlorobenzene 74-118 1.7 20
0.047 95.697.40.0480.050mg/KgChlorodibromomethane 73-122 1.8 20
0.047 94.894.20.0470.050mg/KgChloroethane 33-149 0.6 20
0.045 90.491.60.0450.050mg/KgChloroform 73-127 1.3 20
0.049 98.893.40.0460.050mg/KgChloromethane 45-143 5.6 20
0.046 92.692.20.0460.050mg/Kg2-Chlorotoluene 67-124 0.4 20
0.046 92.692.20.0460.050mg/Kg4-Chlorotoluene 71-126 0.4 20
0.046 93.093.00.0460.050mg/KgDi-Isopropyl Ether (DIPE)59-159 0.0 20
0.052 1041110.0550.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 6.8 20
0.048 96.01010.0500.050mg/Kg1,2-Dibromoethane 70-132 5.0 20
0.047 94.495.40.0470.050mg/KgDibromomethane 74-133 1.0 20
0.047 94.696.20.0480.050mg/Kg1,2-Dichlorobenzene 72-123 1.6 20
0.048 97.695.20.0470.050mg/Kg1,3-Dichlorobenzene 71-120 2.4 20
0.047 95.292.40.0460.050mg/Kg1,4-Dichlorobenzene 71-123 2.9 20
0.043 87.487.80.0430.050mg/KgDichlorodifluoromethane 26-146 0.4 20
Page 4 of 18Date:09/12/2022 03:59 PM
Page 44 of 60
Quality Control Data
22-244-0001Report No:
Project Description:
Client ID:Geological Resources, Inc.
Riverside Grocery
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V23470QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V23469
LCS-V23469 LCSD-V23469Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.044 89.290.20.0450.050mg/Kg1,1-Dichloroethane 74-127 1.1 20
0.044 88.891.00.0450.050mg/Kg1,2-Dichloroethane 68-128 2.4 20
0.042 84.887.00.0430.050mg/Kg1,1-Dichloroethene 67-149 2.5 20
0.044 88.288.80.0440.050mg/Kgcis-1,2-Dichloroethene 76-134 0.6 20
0.045 90.691.20.0450.050mg/Kgtrans-1,2-Dichloroethene 73-132 0.6 20
0.045 91.290.60.0450.050mg/Kg1,2-Dichloropropane 73-130 0.6 20
0.046 93.897.80.0480.050mg/Kg1,3-Dichloropropane 75-124 4.1 20
0.041 83.486.00.0430.050mg/Kg2,2-Dichloropropane 50-142 3.0 20
0.044 89.289.80.0440.050mg/Kg1,1-Dichloropropene 71-130 0.6 20
0.046 93.294.00.0470.050mg/Kgcis-1,3-Dichloropropene 71-125 0.8 20
0.046 93.894.80.0470.050mg/Kgtrans-1,3-Dichloropropene 68-123 1.0 20
0.044 89.491.00.0450.050mg/KgEthylbenzene 74-128 1.7 20
0.096 96.899.50.0990.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 2.7 20
0.046 92.294.60.0470.050mg/KgHexachlorobutadiene 64-125 2.5 20
0.048 97.692.40.0460.050mg/Kgn-Hexane 70-130 5.4 20
0.049 99.81110.0550.050mg/Kg2-Hexanone 61-157 10.6 20
0.045 91.090.80.0450.050mg/KgIsopropylbenzene 68-126 0.2 20
0.045 91.891.60.0450.050mg/Kg4-Isopropyl toluene 68-129 0.2 20
0.046 93.497.60.0480.050mg/KgMethyl Ethyl Ketone (MEK)63-149 4.3 20
0.046 93.297.00.0480.050mg/KgMethyl tert-butyl ether (MTBE)70-130 3.9 20
0.041 83.882.20.0410.050mg/KgMethylene Chloride 74-129 1.9 20
0.045 90.094.60.0470.050mg/KgNaphthalene 57-157 4.9 20
0.046 93.092.80.0460.050mg/Kgn-Propylbenzene 67-130 0.2 20
0.047 95.097.20.0480.050mg/KgStyrene 77-121 2.2 20
0.046 93.894.40.0470.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 0.6 20
0.049 98.21010.0500.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 2.4 20
Page 5 of 18Date:09/12/2022 03:59 PM
Page 45 of 60
Quality Control Data
22-244-0001Report No:
Project Description:
Client ID:Geological Resources, Inc.
Riverside Grocery
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V23470QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V23469
LCS-V23469 LCSD-V23469Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.044 89.687.80.0430.050mg/KgTetrachloroethene 68-130 2.0 20
0.044 88.889.00.0440.050mg/KgToluene 71-129 0.2 20
0.055 1101110.0550.050mg/Kg1,2,3-Trichlorobenzene 68-130 0.5 20
0.053 1081100.0540.050mg/Kg1,2,4-Trichlorobenzene 66-125 1.8 20
0.045 90.085.60.0420.050mg/Kg1,1,1-Trichloroethane 67-131 5.0 20
0.046 93.297.40.0480.050mg/Kg1,1,2-Trichloroethane 70-133 4.4 20
0.045 91.886.40.0430.050mg/KgTrichloroethene 75-133 6.0 20
0.043 86.487.80.0430.050mg/KgTrichlorofluoromethane 44-146 1.6 20
0.048 97.81020.0510.050mg/Kg1,2,3-Trichloropropane 60-137 4.5 20
0.046 93.491.60.0450.050mg/Kg1,2,4-Trimethylbenzene 69-129 1.9 20
0.045 91.690.00.0450.050mg/Kg1,3,5-Trimethylbenzene 69-128 1.7 20
0.049 98.81050.0520.050mg/KgVinyl Acetate 60-140 6.4 20
0.047 94.890.40.0450.050mg/KgVinyl Chloride 48-147 4.7 20
0.045 90.291.00.0450.050mg/Kgo-Xylene 74-126 0.8 20
0.091 91.490.60.0900.100mg/Kgm,p-Xylene 75-124 0.8 20
10198.64-Bromofluorobenzene (S)70-130
101102Dibromofluoromethane (S)70-130
101101Toluene-d8 (S)76-129
Page 6 of 18Date:09/12/2022 03:59 PM
Page 46 of 60
Quality Control Data
22-244-0001Report No:
Project Description:
Client ID:Geological Resources, Inc.
Riverside Grocery
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V23553QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V23506
Associated Lab Samples: 98378, 98379, 98380
LRB-V23506 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/06/22 16:390.6610.116<0.116mg/KgAcenaphthene
09/06/22 16:390.6610.105<0.105mg/KgAcenaphthylene
09/06/22 16:390.6610.152<0.152mg/KgAniline
09/06/22 16:390.6610.143<0.143mg/KgAnthracene
09/06/22 16:390.6610.139<0.139mg/KgBenzo(a)anthracene
09/06/22 16:390.6610.147<0.147mg/KgBenzo(a)pyrene
09/06/22 16:390.6610.146<0.146mg/KgBenzo(b)fluoranthene
09/06/22 16:390.6610.136<0.136mg/KgBenzo(g,h,i)perylene
09/06/22 16:390.6610.137<0.137mg/KgBenzo(k)fluoranthene
09/06/22 16:392.000.580<0.580mg/KgBenzoic Acid
09/06/22 16:390.6610.105<0.105mg/KgBenzyl alcohol
09/06/22 16:390.6610.118<0.118mg/KgBis(2-Chloroethoxy)methane
09/06/22 16:390.6610.107<0.107mg/KgBis(2-Chloroethyl)ether
09/06/22 16:390.3310.136<0.136mg/KgBis(2-Chloroisopropyl)ether
09/06/22 16:390.6610.120<0.120mg/KgBis(2-ethylhexyl)phthalate
09/06/22 16:390.6610.109<0.109mg/Kg4-Bromophenyl phenyl ether
09/06/22 16:390.3310.113<0.113mg/KgButyl benzyl phthalate
09/06/22 16:390.6610.092<0.092mg/Kg4-Chloro-3-methylphenol
09/06/22 16:390.3310.112<0.112mg/Kg4-Chloroaniline
09/06/22 16:390.6610.116<0.116mg/Kg2-Chloronaphthalene
09/06/22 16:390.6610.098<0.098mg/Kg2-Chlorophenol
09/06/22 16:391.000.126<0.126mg/Kg4-Chlorophenyl phenyl ether
09/06/22 16:390.6610.142<0.142mg/KgChrysene
09/06/22 16:390.6610.230<0.230mg/KgDibenz(a,h)anthracene
09/06/22 16:390.6610.119<0.119mg/KgDibenzofuran
09/06/22 16:390.6610.094<0.094mg/Kg1,2-Dichlorobenzene
09/06/22 16:390.6610.097<0.097mg/Kg1,3-Dichlorobenzene
Page 7 of 18Date:09/12/2022 03:59 PM
Page 47 of 60
Quality Control Data
22-244-0001Report No:
Project Description:
Client ID:Geological Resources, Inc.
Riverside Grocery
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V23553QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V23506
Associated Lab Samples: 98378, 98379, 98380
LRB-V23506 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/06/22 16:390.3310.097<0.097mg/Kg1,4-Dichlorobenzene
09/06/22 16:390.6610.147<0.147mg/Kg3,3'-Dichlorobenzidine
09/06/22 16:390.6610.095<0.095mg/Kg2,4-Dichlorophenol
09/06/22 16:390.6610.180<0.180mg/KgDiethyl phthalate
09/06/22 16:390.6610.174<0.174mg/KgDimethyl phthalate
09/06/22 16:390.3310.108<0.108mg/Kg2,4-Dimethylphenol
09/06/22 16:390.6610.107<0.107mg/KgDi-n-butyl phthalate
09/06/22 16:391.500.240<0.240mg/Kg4,6-Dinitro-2-methylphenol
09/06/22 16:391.500.520<0.520mg/Kg2,4-Dinitrophenol
09/06/22 16:390.6610.096<0.096mg/Kg2,4-Dinitrotoluene
09/06/22 16:390.6610.108<0.108mg/Kg2,6-Dinitrotoluene
09/06/22 16:390.3310.143<0.143mg/KgDi-n-Octyl Phthalate
09/06/22 16:390.6610.123<0.123mg/KgFluoranthene
09/06/22 16:390.6610.128<0.128mg/KgFluorene
09/06/22 16:390.6610.106<0.106mg/KgHexachlorobenzene
09/06/22 16:390.6610.097<0.097mg/KgHexachlorobutadiene
09/06/22 16:390.6610.157<0.157mg/KgHexachlorocyclopentadiene
09/06/22 16:390.6610.079<0.079mg/KgHexachloroethane
09/06/22 16:390.6610.179<0.179mg/KgIndeno(1,2,3-cd)pyrene
09/06/22 16:390.6610.191<0.191mg/KgIsophorone
09/06/22 16:390.6610.106<0.106mg/Kg1-Methylnaphthalene
09/06/22 16:390.6610.100<0.100mg/Kg2-Methylnaphthalene
09/06/22 16:390.6610.097<0.097mg/Kg2-Methylphenol
09/06/22 16:390.6610.085<0.085mg/Kg3&4 Methylphenol
09/06/22 16:390.6610.144<0.144mg/KgNaphthalene
09/06/22 16:390.6610.096<0.096mg/Kg2-Nitroaniline
09/06/22 16:390.6610.120<0.120mg/Kg3-Nitroaniline
Page 8 of 18Date:09/12/2022 03:59 PM
Page 48 of 60
Quality Control Data
22-244-0001Report No:
Project Description:
Client ID:Geological Resources, Inc.
Riverside Grocery
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V23553QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V23506
Associated Lab Samples: 98378, 98379, 98380
LRB-V23506 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/06/22 16:390.3310.093<0.093mg/Kg4-Nitroaniline
09/06/22 16:390.3310.116<0.116mg/KgNitrobenzene
09/06/22 16:390.6610.088<0.088mg/Kg2-Nitrophenol
09/06/22 16:390.6610.117<0.117mg/Kg4-Nitrophenol
09/06/22 16:390.6610.263<0.263mg/KgN-Nitrosodimethylamine
09/06/22 16:390.6610.181<0.181mg/KgN-Nitrosodiphenylamine
09/06/22 16:390.6610.118<0.118mg/KgN-Nitroso-di-n-propylamine
09/06/22 16:391.000.347<0.347mg/KgPentachlorophenol
09/06/22 16:390.6610.208<0.208mg/KgPhenanthrene
09/06/22 16:390.6610.112<0.112mg/KgPhenol
09/06/22 16:390.6610.134<0.134mg/KgPyrene
09/06/22 16:390.3310.079<0.079mg/KgPyridine
09/06/22 16:390.6610.107<0.107mg/Kg1,2,4-Trichlorobenzene
09/06/22 16:390.6610.096<0.096mg/Kg2,4,5-Trichlorophenol
09/06/22 16:390.6610.096<0.096mg/Kg2,4,6-Trichlorophenol
09/06/22 16:392-Fluorobiphenyl (S)98.8 44-115
09/06/22 16:392-Fluorophenol (S)97.0 35-115
09/06/22 16:39Nitrobenzene-d5 (S)80.2 37-122
09/06/22 16:394-Terphenyl-d14 (S)111 54-127
09/06/22 16:392,4,6-Tribromophenol (S)110 39-132
09/06/22 16:39Phenol-d5 (S)88.0 34-121
LCS-V23506Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
94.61.581.67mg/KgAcenaphthene 40-123
94.01.571.67mg/KgAcenaphthylene 32-132
Page 9 of 18Date:09/12/2022 03:59 PM
Page 49 of 60
Quality Control Data
22-244-0001Report No:
Project Description:
Client ID:Geological Resources, Inc.
Riverside Grocery
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V23553QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V23506
LCS-V23506Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1212.021.67mg/KgAniline 12-197
94.61.581.67mg/KgAnthracene 47-123
1001.671.67mg/KgBenzo(a)anthracene 49-126
1161.931.67mg/KgBenzo(a)pyrene 45-129
1071.781.67mg/KgBenzo(b)fluoranthene 45-132
98.81.651.67mg/KgBenzo(g,h,i)perylene 43-134
1001.671.67mg/KgBenzo(k)fluoranthene 47-132
44.60.7461.67mg/KgBenzoic Acid 10-83
1011.691.67mg/KgBenzyl alcohol 29-122
76.61.281.67mg/KgBis(2-Chloroethoxy)methane 36-121
80.81.351.67mg/KgBis(2-Chloroethyl)ether 31-120
79.61.331.67mg/KgBis(2-Chloroisopropyl)ether 33-131
1061.771.67mg/KgBis(2-ethylhexyl)phthalate 51-133
1041.731.67mg/Kg4-Bromophenyl phenyl ether 46-124
92.21.541.67mg/KgButyl benzyl phthalate 48-132
85.01.421.67mg/Kg4-Chloro-3-methylphenol 45-122
71.21.191.67mg/Kg4-Chloroaniline 17-106
95.21.591.67mg/Kg2-Chloronaphthalene 41-114
96.41.611.67mg/Kg2-Chlorophenol 34-121
98.81.651.67mg/Kg4-Chlorophenyl phenyl ether 45-121
1041.741.67mg/KgChrysene 50-124
96.41.611.67mg/KgDibenz(a,h)anthracene 45-134
94.61.581.67mg/KgDibenzofuran 44-120
94.61.581.67mg/Kg1,2-Dichlorobenzene 33-117
95.81.601.67mg/Kg1,3-Dichlorobenzene 30-115
93.41.561.67mg/Kg1,4-Dichlorobenzene 31-115
79.01.321.67mg/Kg3,3'-Dichlorobenzidine 22-121
Page 10 of 18Date:09/12/2022 03:59 PM
Page 50 of 60
Quality Control Data
22-244-0001Report No:
Project Description:
Client ID:Geological Resources, Inc.
Riverside Grocery
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V23553QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V23506
LCS-V23506Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
88.01.471.67mg/Kg2,4-Dichlorophenol 40-122
96.41.611.67mg/KgDiethyl phthalate 50-124
97.61.631.67mg/KgDimethyl phthalate 48-124
89.81.501.67mg/Kg2,4-Dimethylphenol 30-127
1041.731.67mg/KgDi-n-butyl phthalate 51-128
89.21.491.67mg/Kg4,6-Dinitro-2-methylphenol 29-132
79.01.321.67mg/Kg2,4-Dinitrophenol 27-129
1081.801.67mg/Kg2,4-Dinitrotoluene 48-126
1041.741.67mg/Kg2,6-Dinitrotoluene 46-124
1071.791.67mg/KgDi-n-Octyl Phthalate 45-140
97.61.631.67mg/KgFluoranthene 50-127
95.21.591.67mg/KgFluorene 43-125
1021.711.67mg/KgHexachlorobenzene 45-122
95.21.591.67mg/KgHexachlorobutadiene 32-123
79.61.331.67mg/KgHexachlorocyclopentadiene 32-117
85.01.421.67mg/KgHexachloroethane 28-117
97.61.631.67mg/KgIndeno(1,2,3-cd)pyrene 45-133
65.81.101.67mg/KgIsophorone 30-122
82.61.381.67mg/Kg1-Methylnaphthalene 40-119
79.01.321.67mg/Kg2-Methylnaphthalene 38-122
94.61.581.67mg/Kg2-Methylphenol 32-122
81.41.361.67mg/Kg3&4 Methylphenol 34-119
79.61.331.67mg/KgNaphthalene 35-123
84.41.411.67mg/Kg2-Nitroaniline 44-127
81.41.361.67mg/Kg3-Nitroaniline 33-119
89.81.501.67mg/Kg4-Nitroaniline 63-147
71.21.191.67mg/KgNitrobenzene 34-122
Page 11 of 18Date:09/12/2022 03:59 PM
Page 51 of 60
Quality Control Data
22-244-0001Report No:
Project Description:
Client ID:Geological Resources, Inc.
Riverside Grocery
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V23553QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V23506
LCS-V23506Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
82.01.371.67mg/Kg2-Nitrophenol 36-123
79.61.331.67mg/Kg4-Nitrophenol 30-132
68.21.141.67mg/KgN-Nitrosodimethylamine 10-146
1161.931.67mg/KgN-Nitrosodiphenylamine 38-127
83.81.401.67mg/KgN-Nitroso-di-n-propylamine 36-120
1121.871.67mg/KgPentachlorophenol 25-133
95.21.591.67mg/KgPhenanthrene 50-121
87.41.461.67mg/KgPhenol 34-121
1041.731.67mg/KgPyrene 47-127
58.00.9701.67mg/KgPyridine 10-80
85.61.431.67mg/Kg1,2,4-Trichlorobenzene 34-118
97.61.631.67mg/Kg2,4,5-Trichlorophenol 41-124
94.61.581.67mg/Kg2,4,6-Trichlorophenol 39-126
97.62-Fluorobiphenyl (S)44-115
97.82-Fluorophenol (S)35-115
68.8Nitrobenzene-d5 (S)37-122
1104-Terphenyl-d14 (S)54-127
1112,4,6-Tribromophenol (S)39-132
89.4Phenol-d5 (S)34-121
V 98392-MS-V23506 V 98392-MSD-V23506Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.62 97.01.631.671.67<0.116mg/KgAcenaphthene 97.6 40-123 0.6 20
1.60 95.81.601.671.67<0.105mg/KgAcenaphthylene 95.8 32-132 0.0 20
2.16 1292.251.671.67<0.152mg/KgAniline 135 12-197 4.0 20
Page 12 of 18Date:09/12/2022 03:59 PM
Page 52 of 60
Quality Control Data
22-244-0001Report No:
Project Description:
Client ID:Geological Resources, Inc.
Riverside Grocery
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V23553QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V23506
V 98392-MS-V23506 V 98392-MSD-V23506Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.60 95.81.611.671.67<0.143mg/KgAnthracene 96.4 47-123 0.6 20
1.67 1001.701.671.67<0.139mg/KgBenzo(a)anthracene 102 49-126 1.7 20
1.96 1172.011.671.67<0.147mg/KgBenzo(a)pyrene 120 45-129 2.5 20
1.71 1021.771.671.67<0.146mg/KgBenzo(b)fluoranthene 106 45-132 3.4 20
1.66 99.41.721.671.67<0.136mg/KgBenzo(g,h,i)perylene 103 43-134 3.5 20
1.73 1041.771.671.67<0.137mg/KgBenzo(k)fluoranthene 106 47-132 2.2 20
0.893 53.40.9271.671.67<0.580mg/KgBenzoic Acid 55.5 10-83 3.7 20
1.72 1031.741.671.67<0.105mg/KgBenzyl alcohol 104 29-122 1.1 20
1.36 81.41.351.671.67<0.118mg/KgBis(2-Chloroethoxy)methane 80.8 36-121 0.7 20
1.38 82.61.411.671.67<0.107mg/KgBis(2-Chloroethyl)ether 84.4 31-120 2.1 20
1.37 82.01.401.671.67<0.136mg/KgBis(2-Chloroisopropyl)ether 83.8 33-131 2.1 20
1.76 1051.801.671.67<0.120mg/KgBis(2-ethylhexyl)phthalate 108 51-133 2.2 20
1.72 1031.731.671.67<0.109mg/Kg4-Bromophenyl phenyl ether 104 46-124 0.5 20
1.49 89.21.521.671.67<0.113mg/KgButyl benzyl phthalate 91.0 48-132 1.9 20
1.49 89.21.481.671.67<0.092mg/Kg4-Chloro-3-methylphenol 88.6 45-122 0.6 20
1.30 77.81.321.671.67<0.112mg/Kg4-Chloroaniline 79.0 17-106 1.5 20
1.63 97.61.611.671.67<0.116mg/Kg2-Chloronaphthalene 96.4 41-114 1.2 20
1.67 1001.721.671.67<0.098mg/Kg2-Chlorophenol 103 34-121 2.9 20
1.69 1011.681.671.67<0.126mg/Kg4-Chlorophenyl phenyl ether 101 45-121 0.5 20
1.72 1031.781.671.67<0.142mg/KgChrysene 107 50-124 3.4 20
1.60 95.81.691.671.67<0.230mg/KgDibenz(a,h)anthracene 101 45-134 5.4 20
1.65 98.81.611.671.67<0.119mg/KgDibenzofuran 96.4 44-120 2.4 20
1.59 95.21.641.671.67<0.094mg/Kg1,2-Dichlorobenzene 98.2 33-117 3.0 20
1.56 93.41.601.671.67<0.097mg/Kg1,3-Dichlorobenzene 95.8 30-115 2.5 20
1.52 91.01.551.671.67<0.097mg/Kg1,4-Dichlorobenzene 92.8 31-115 1.9 20
1.38 82.61.421.671.67<0.147mg/Kg3,3'-Dichlorobenzidine 85.0 22-121 2.8 20
Page 13 of 18Date:09/12/2022 03:59 PM
Page 53 of 60
Quality Control Data
22-244-0001Report No:
Project Description:
Client ID:Geological Resources, Inc.
Riverside Grocery
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V23553QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V23506
V 98392-MS-V23506 V 98392-MSD-V23506Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.51 90.41.541.671.67<0.095mg/Kg2,4-Dichlorophenol 92.2 40-122 1.9 20
1.67 1001.641.671.67<0.180mg/KgDiethyl phthalate 98.2 50-124 1.8 20
1.71 1021.711.671.67<0.174mg/KgDimethyl phthalate 102 48-124 0.0 30
1.56 93.41.561.671.67<0.108mg/Kg2,4-Dimethylphenol 93.4 30-127 0.0 20
1.68 1011.681.671.67<0.107mg/KgDi-n-butyl phthalate 101 51-128 0.0 20
1.60 95.81.591.671.67<0.240mg/Kg4,6-Dinitro-2-methylphenol 95.2 29-132 0.6 20
1.52 91.01.591.671.67<0.520mg/Kg2,4-Dinitrophenol 95.2 27-129 4.5 20
1.90 1141.871.671.67<0.096mg/Kg2,4-Dinitrotoluene 112 48-126 1.5 20
1.81 1081.831.671.67<0.108mg/Kg2,6-Dinitrotoluene 110 46-124 1.0 20
1.79 1071.861.671.67<0.143mg/KgDi-n-Octyl Phthalate 111 45-140 3.8 20
1.61 96.41.631.671.67<0.123mg/KgFluoranthene 97.6 50-127 1.2 20
1.64 98.21.611.671.67<0.128mg/KgFluorene 96.4 43-125 1.8 20
1.70 1021.761.671.67<0.106mg/KgHexachlorobenzene 105 45-122 3.4 20
1.58 94.61.591.671.67<0.097mg/KgHexachlorobutadiene 95.2 32-123 0.6 20
1.28 76.61.281.671.67<0.157mg/KgHexachlorocyclopentadiene 76.6 32-117 0.0 20
1.36 81.41.451.671.67<0.079mg/KgHexachloroethane 86.8 28-117 6.4 20
1.65 98.81.701.671.67<0.179mg/KgIndeno(1,2,3-cd)pyrene 102 45-133 2.9 20
1.17 70.01.161.671.67<0.191mg/KgIsophorone 69.4 30-122 0.8 20
1.40 83.81.401.671.67<0.106mg/Kg1-Methylnaphthalene 83.8 40-119 0.0 20
1.35 80.81.381.671.67<0.100mg/Kg2-Methylnaphthalene 82.6 38-122 2.1 20
1.65 98.81.601.671.67<0.097mg/Kg2-Methylphenol 95.8 32-122 3.0 20
1.43 85.61.471.671.67<0.085mg/Kg3&4 Methylphenol 88.0 34-119 2.7 20
1.36 81.41.371.671.67<0.144mg/KgNaphthalene 82.0 35-123 0.7 20
1.49 89.21.441.671.67<0.096mg/Kg2-Nitroaniline 86.2 44-127 3.4 20
1.45 86.81.421.671.67<0.120mg/Kg3-Nitroaniline 85.0 33-119 2.0 20
1.60 95.81.571.671.67<0.093mg/Kg4-Nitroaniline 94.0 63-147 1.8 20
Page 14 of 18Date:09/12/2022 03:59 PM
Page 54 of 60
Quality Control Data
22-244-0001Report No:
Project Description:
Client ID:Geological Resources, Inc.
Riverside Grocery
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V23553QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V23506
V 98392-MS-V23506 V 98392-MSD-V23506Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.21 72.41.231.671.67<0.116mg/KgNitrobenzene 73.6 34-122 1.6 20
1.44 86.21.451.671.67<0.088mg/Kg2-Nitrophenol 86.8 32-123 0.6 20
1.39 83.21.411.671.67<0.117mg/Kg4-Nitrophenol 84.4 30-132 1.4 20
1.15 68.81.201.671.67<0.263mg/KgN-Nitrosodimethylamine 71.8 10-146 4.2 30
1.94 1161.941.671.67<0.181mg/KgN-Nitrosodiphenylamine 116 38-127 0.0 20
1.44 86.21.491.671.67<0.118mg/KgN-Nitroso-di-n-propylamine 89.2 36-120 3.4 20
1.95 1171.981.671.67<0.347mg/KgPentachlorophenol 119 25-133 1.5 20
1.59 95.21.601.671.67<0.208mg/KgPhenanthrene 95.8 50-121 0.6 20
1.54 92.21.571.671.67<0.112mg/KgPhenol 94.0 34-121 1.9 20
1.69 1011.751.671.67<0.134mg/KgPyrene 105 47-127 3.4 20
1.10 65.81.111.671.67<0.079mg/KgPyridine 66.4 10-80 0.9 20
1.47 88.01.441.671.67<0.107mg/Kg1,2,4-Trichlorobenzene 86.2 34-118 2.0 20
1.69 1011.751.671.67<0.096mg/Kg2,4,5-Trichlorophenol 105 41-124 3.4 20
1.64 98.21.631.671.67<0.096mg/Kg2,4,6-Trichlorophenol 97.6 39-126 0.6 20
97.62-Fluorobiphenyl (S)95.2 44-115
1002-Fluorophenol (S)101 35-115
71.8Nitrobenzene-d5 (S)70.0 37-122
1084-Terphenyl-d14 (S)108 54-127
1132,4,6-Tribromophenol (S)113 39-132
90.7Phenol-d5 (S)90.3 34-121
Page 15 of 18Date:09/12/2022 03:59 PM
Page 55 of 60
Quality Control Data
22-244-0001Report No:
Project Description:
Client ID:Geological Resources, Inc.
Riverside Grocery
QC Prep Batch Method:
Massachusetts EPH
MADEP-EPH
V23694QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAEPH (Prep)
QC Prep:V23573
Associated Lab Samples: 98378, 98379, 98380
LRB-V23573 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/09/22 16:0350.09.20<9.20mg/KgAliphatic C9-C18
09/09/22 16:0350.012.2<12.2mg/KgAliphatic C19-C36
09/09/22 16:0350.014.2<14.2mg/KgAromatic C11-C22
09/09/22 16:032-Fluorobiphenyl (S)99.5 40-140
09/09/22 16:032-Bromonaphthalene (S)101 40-140
09/09/22 16:03Chlorooctadecane (S)72.0 40-140
09/09/22 16:03OTP Surrogate (S)86.5 40-140
LCS-V23573 LCSD-V23573Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
46.0 76.681.048.660.0mg/KgAliphatic C9-C18 40-140 5.4 50
68.8 86.094.275.480.0mg/KgAliphatic C19-C36 40-140 9.1 50
173 102104176170mg/KgAromatic C11-C22 40-140 1.7 50
10497.52-Fluorobiphenyl (S)40-140
1071042-Bromonaphthalene (S)40-140
73.081.0Chlorooctadecane (S)40-140
90.591.5OTP Surrogate (S)40-140
Page 16 of 18Date:09/12/2022 03:59 PM
Page 56 of 60
Quality Control Data
22-244-0001Report No:
Project Description:
Client ID:Geological Resources, Inc.
Riverside Grocery
QC Prep Batch Method:
Massachusetts VPH
MADEP-VPH
V23448QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAVPH (Prep)
QC Prep:V23447
Associated Lab Samples: 98378, 98379, 98380
LRB-V23447 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/02/22 14:208.001.22<1.22mg/KgAliphatic C5-C8
09/02/22 14:208.004.56<4.56mg/KgAliphatic C9-C12
09/02/22 14:208.000.624<0.624mg/KgAromatic C9-C10
09/02/22 14:202,5-Dibromotoluene (FID) (S)75.5 70-130
09/02/22 14:202,5-Dibromotoluene (PID) (S)79.9 70-130
LCS-V23447 LCSD-V23447Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
30.2 94.392.129.532.0mg/KgAliphatic C5-C8 70-130 2.3 50
31.9 99.696.530.932.0mg/KgAliphatic C9-C12 70-130 3.1 50
9.92 92.785.29.1210.7mg/KgAromatic C9-C10 70-130 8.4 50
83.083.32,5-Dibromotoluene (FID) (S)70-130
85.681.32,5-Dibromotoluene (PID) (S)70-130
Page 17 of 18Date:09/12/2022 03:59 PM
Page 57 of 60
Quality Control Data
22-244-0001Report No:
Project Description:
Client ID:Geological Resources, Inc.
Riverside Grocery
Dry Weight Determination
SW-DRYWT
V23534QC Analytical Batch:
Analysis Method:
Analysis Description:
V 98367-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 09/07/22 10:070.614.614.5%Moisture
V 98374-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 09/07/22 10:070.017.617.6%Moisture
Page 18 of 18Date:09/12/2022 03:59 PM
Page 58 of 60
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:22-244-0001
Geological Resources, Inc.
00087
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT 15 1.4C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
ü
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Danyale Love Date & Time:09/01/2022 11:31:10
Special precautions or instructions included?
Comments:
Page 59 of 60
Page 60 of 60